WS-2441_3320_CA_LAB_20190628

07/05/19
Technical Report for
ATC Group Services LLC
Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
SGS Job Number: FA65658
Sampling Date: 06/28/19
Report to:
ATC Group Services LLC
7606 Whitehall Executive Center Dr Suite 800
Charlotte, NC 28273
[e-mail]; [e-mail]
ATTN: Andrew Deppensmith
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 07/05/19
e-Hardcopy 2.0
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Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
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1 of 32
FA65658
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................5
3.1: FA65658-1: MW-1 ........................................................................................................6
3.2: FA65658-2: MW-2 ........................................................................................................8
3.3: FA65658-3: WSW-1 .....................................................................................................10
3.4: FA65658-4: WSW-2 .....................................................................................................12
3.5: FA65658-5: WSW-3 .....................................................................................................14
3.6: FA65658-6: WSW-4 .....................................................................................................16
3.7: FA65658-7: FB-1 ..........................................................................................................18
Section 4: Misc. Forms ............................................................................................................20
4.1: Chain of Custody ...........................................................................................................21
Section 5: MS Volatiles - QC Data Summaries .....................................................................23
5.1: Method Blank Summary ................................................................................................24
5.2: Blank Spike Summary ...................................................................................................27
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................30 123452 of 32
FA65658
SGS North America Inc.
Sample Summary
ATC Group Services LLC
Job No:FA65658
Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA65658-1 06/28/19 11:45 AR 07/02/19 AQ Ground Water MW-1
FA65658-2 06/28/19 11:30 AR 07/02/19 AQ Ground Water MW-2
FA65658-3 06/28/19 12:20 AR 07/02/19 AQ Water WSW-1
FA65658-4 06/28/19 12:50 AR 07/02/19 AQ Water WSW-2
FA65658-5 06/28/19 13:05 AR 07/02/19 AQ Water WSW-3
FA65658-6 06/28/19 13:45 AR 07/02/19 AQ Water WSW-4
FA65658-7 06/28/19 11:15 AR 07/02/19 AQ Field Blank Water FB-1
3 of 32
FA656581
Summary of Hits Page 1 of 1
Job Number:FA65658
Account:ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Collected:06/28/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA65658-1 MW-1
Benzene 8.0 0.50 0.13 ug/l SM 6200B
2-Butanone (MEK)12.7 2.5 1.3 ug/l SM 6200B
sec-Butylbenzene 0.53 0.50 0.13 ug/l SM 6200B
Ethylbenzene 10.8 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 2.2 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.23 J 0.50 0.13 ug/l SM 6200B
Naphthalene 0.62 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 1.3 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.68 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.3 1.0 0.13 ug/l SM 6200B
Xylene (total)1.3 J 1.5 0.25 ug/l SM 6200B
FA65658-2 MW-2
No hits reported in this sample.
FA65658-3 WSW-1
No hits reported in this sample.
FA65658-4 WSW-2
No hits reported in this sample.
FA65658-5 WSW-3
Tetrachloroethylene 0.25 J 0.50 0.13 ug/l SM 6200B
FA65658-6 WSW-4
No hits reported in this sample.
FA65658-7 FB-1
No hits reported in this sample.
4 of 32
FA656582
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
5 of 32
FA656583
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA65658-1 Date Sampled:06/28/19
Matrix:AQ - Ground Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218479.D 1 07/03/19 11:54 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene 8.0 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)12.7 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.53 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 of 32
FA6565833.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA65658-1 Date Sampled:06/28/19
Matrix:AQ - Ground Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene 10.8 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene 2.2 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.23 0.50 0.13 ug/l J
91-20-3 Naphthalene 0.62 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.3 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.68 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.3 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)1.3 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 32
FA6565833.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA65658-2 Date Sampled:06/28/19
Matrix:AQ - Ground Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218480.D 1 07/03/19 12:17 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 32
FA6565833.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA65658-2 Date Sampled:06/28/19
Matrix:AQ - Ground Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 32
FA6565833.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-1
Lab Sample ID:FA65658-3 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218481.D 1 07/03/19 12:39 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 32
FA6565833.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-1
Lab Sample ID:FA65658-3 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 32
FA6565833.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA65658-4 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218482.D 1 07/03/19 13:02 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 32
FA6565833.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA65658-4 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 32
FA6565833.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-3
Lab Sample ID:FA65658-5 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218483.D 1 07/03/19 13:25 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 32
FA6565833.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-3
Lab Sample ID:FA65658-5 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.25 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 32
FA6565833.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA65658-6 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218484.D 1 07/03/19 13:48 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 32
FA6565833.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA65658-6 Date Sampled:06/28/19
Matrix:AQ - Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 32
FA6565833.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:FB-1
Lab Sample ID:FA65658-7 Date Sampled:06/28/19
Matrix:AQ - Field Blank Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0218478.D 1 07/03/19 11:31 AB n/a n/a VA2583
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 32
FA6565833.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:FB-1
Lab Sample ID:FA65658-7 Date Sampled:06/28/19
Matrix:AQ - Field Blank Water Date Received:07/02/19
Method:SM 6200B Percent Solids:n/a
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 32
FA6565833.7
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
20 of 32
FA656584
FA65658: Chain of Custody
Page 1 of 2
21 of 32
FA6565844.1
Job Number:FA65658 Client:ATC
Date / Time Received:7/2/2019 8:50:00 AM Delivery Method:FX
Project:163 SERVICE & GROCERY
Airbill #'s:1009 6377 3945
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.2);
Cooler 1: (1.6);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH Date:Date:7/2/2019 8:50:00 AM
FA65658: Chain of Custody
Page 2 of 2
22 of 32
FA6565844.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
23 of 32
FA656585
Method Blank Summary Page 1 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-MB A0218477.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 10 2.0 ug/l
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
78-93-3 2-Butanone (MEK)ND 2.5 1.3 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
64-17-5 Ethyl Alcohol ND 100 65 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
24 of 32
FA6565855.1.1
Method Blank Summary Page 2 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-MB A0218477.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 5.0 1.0 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
108-05-4 Vinyl Acetate ND 5.0 1.0 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
25 of 32
FA6565855.1.1
Method Blank Summary Page 3 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-MB A0218477.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 103%70-130%
26 of 32
FA6565855.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-BS A0218475.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 60.2 120 70-130
71-43-2 Benzene 10 9.6 96 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 8.9 89 70-130
75-27-4 Bromodichloromethane 10 8.8 88 70-130
75-25-2 Bromoform 10 8.1 81 70-130
78-93-3 2-Butanone (MEK)50 53.1 106 70-130
104-51-8 n-Butylbenzene 10 9.2 92 70-130
135-98-8 sec-Butylbenzene 10 9.2 92 70-130
98-06-6 tert-Butylbenzene 10 8.9 89 70-130
56-23-5 Carbon Tetrachloride 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 12.5 125 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.1 91 70-130
124-48-1 Dibromochloromethane 10 8.7 87 70-130
106-93-4 1,2-Dibromoethane 10 9.4 94 70-130
75-71-8 Dichlorodifluoromethane 10 10.2 102 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130
106-46-7 1,4-Dichlorobenzene 10 9.3 93 70-130
75-34-3 1,1-Dichloroethane 10 9.9 99 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.9 99 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.5 95 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130
78-87-5 1,2-Dichloropropane 10 9.5 95 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 10.5 105 70-130
563-58-6 1,1-Dichloropropene 10 9.3 93 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.5 85 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
108-20-3 Di-Isopropyl Ether 10 9.1 91 70-130
64-17-5 Ethyl Alcohol 500 597 119 70-130
100-41-4 Ethylbenzene 10 9.7 97 70-130
* = Outside of Control Limits.
27 of 32
FA6565855.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-BS A0218475.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 49.1 98 70-130
98-82-8 Isopropylbenzene 10 9.5 95 70-130
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 12.6 126 60-140
74-87-3 Methyl Chloride 10 12.4 124 60-140
75-09-2 Methylene Chloride 10 9.2 92 70-130
108-10-1 4-Methyl-2-pentanone (MIBK)50 50.8 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.1 91 70-130
91-20-3 Naphthalene 10 8.2 82 70-130
103-65-1 n-Propylbenzene 10 9.1 91 70-130
100-42-5 Styrene 10 8.7 87 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.7 87 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 10.3 103 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.6 86 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.6 86 70-130
71-55-6 1,1,1-Trichloroethane 10 9.8 98 70-130
79-00-5 1,1,2-Trichloroethane 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 9.4 94 70-130
75-69-4 Trichlorofluoromethane 10 13.4 134 60-140
96-18-4 1,2,3-Trichloropropane 10 9.0 90 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.6 86 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.9 89 70-130
108-05-4 Vinyl Acetate 50 41.0 82 70-130
75-01-4 Vinyl Chloride 10 12.4 124 60-140
m,p-Xylene 20 17.9 90 70-130
95-47-6 o-Xylene 10 8.8 88 70-130
1330-20-7 Xylene (total)30 26.7 89 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 100%70-130%
* = Outside of Control Limits.
28 of 32
FA6565855.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2583-BS A0218475.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
29 of 32
FA6565855.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA65658-1MS A0218488.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1MSD A0218489.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1 A0218479.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
FA65658-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 250 275 110 250 213 85 25*70-130/20
71-43-2 Benzene 8.0 50 60.3 105 50 59.7 103 1 70-130/20
108-86-1 Bromobenzene ND 50 51.5 103 50 51.5 103 0 70-130/20
74-97-5 Bromochloromethane ND 50 49.8 100 50 48.1 96 3 70-130/20
75-27-4 Bromodichloromethane ND 50 44.8 90 50 44.2 88 1 70-130/20
75-25-2 Bromoform ND 50 29.5 59*50 29.6 59*0 70-130/20
78-93-3 2-Butanone (MEK)12.7 250 249 95 250 261 99 5 70-130/20
104-51-8 n-Butylbenzene ND 50 51.8 104 50 51.1 102 1 70-130/20
135-98-8 sec-Butylbenzene 0.53 50 51.2 101 50 51.0 101 0 70-130/20
98-06-6 tert-Butylbenzene ND 50 48.5 97 50 48.5 97 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50 52.4 105 50 51.1 102 3 70-130/20
108-90-7 Chlorobenzene ND 50 52.5 105 50 51.7 103 2 70-130/20
75-00-3 Chloroethane ND 50 54.5 109 50 51.3 103 6 60-140/20
67-66-3 Chloroform ND 50 54.2 108 50 53.0 106 2 70-130/20
95-49-8 o-Chlorotoluene ND 50 54.3 109 50 54.1 108 0 70-130/20
106-43-4 p-Chlorotoluene ND 50 49.7 99 50 49.6 99 0 70-130/20
124-48-1 Dibromochloromethane ND 50 37.7 75 50 36.7 73 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 50.1 100 50 49.7 99 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 43.2 86 50 43.3 87 0 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 51.7 103 50 51.2 102 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 53.8 108 50 53.2 106 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 51.4 103 50 50.6 101 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 55.9 112 50 55.1 110 1 70-130/20
107-06-2 1,2-Dichloroethane ND 50 50.7 101 50 50.3 101 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 57.1 114 50 55.6 111 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 52.9 106 50 52.3 105 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 53.6 107 50 52.9 106 1 70-130/20
78-87-5 1,2-Dichloropropane ND 50 52.8 106 50 52.3 105 1 70-130/20
142-28-9 1,3-Dichloropropane ND 50 48.5 97 50 48.2 96 1 70-130/20
594-20-7 2,2-Dichloropropane ND 50 57.0 114 50 54.4 109 5 70-130/20
563-58-6 1,1-Dichloropropene ND 50 52.5 105 50 51.9 104 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 40.7 81 50 41.0 82 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 44.5 89 50 45.2 90 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 49.8 100 50 49.0 98 2 70-130/20
64-17-5 Ethyl Alcohol ND 2500 3160 126 2500 3240 130 3 70-130/20
100-41-4 Ethylbenzene 10.8 50 64.3 107 50 63.7 106 1 70-130/20
* = Outside of Control Limits.
30 of 32
FA6565855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA65658-1MS A0218488.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1MSD A0218489.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1 A0218479.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
FA65658-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 250 232 93 250 241 96 4 70-130/20
98-82-8 Isopropylbenzene 2.2 50 54.4 104 50 53.7 103 1 70-130/20
99-87-6 p-Isopropyltoluene ND 50 50.0 100 50 50.1 100 0 70-130/20
74-83-9 Methyl Bromide ND 50 53.5 107 50 50.3 101 6 60-140/20
74-87-3 Methyl Chloride ND 50 51.6 103 50 50.9 102 1 60-140/20
75-09-2 Methylene Chloride ND 50 53.2 106 50 51.7 103 3 70-130/20
108-10-1 4-Methyl-2-pentanone (MIBK)ND 250 253 101 250 260 104 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.23 J 50 49.9 99 50 49.2 98 1 70-130/20
91-20-3 Naphthalene 0.62 50 45.9 91 50 46.1 91 0 70-130/20
103-65-1 n-Propylbenzene 1.3 50 51.6 101 50 51.3 100 1 70-130/20
100-42-5 Styrene ND 50 47.2 94 50 46.9 94 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 47.9 96 50 47.2 94 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 53.3 107 50 52.4 105 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 57.1 114 50 56.0 112 2 70-130/20
108-88-3 Toluene ND 50 53.8 108 50 53.1 106 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 46.4 93 50 46.8 94 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 47.0 94 50 46.3 93 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 55.1 110 50 53.6 107 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 52.8 106 50 51.4 103 3 70-130/20
79-01-6 Trichloroethylene ND 50 53.1 106 50 52.3 105 2 70-130/20
75-69-4 Trichlorofluoromethane ND 50 59.2 118 50 56.1 112 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 49.2 98 50 49.2 98 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 0.68 50 49.1 97 50 48.9 96 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 49.3 99 50 49.1 98 0 70-130/20
108-05-4 Vinyl Acetate ND 250 201 80 250 209 84 4 70-130/20
75-01-4 Vinyl Chloride ND 50 54.1 108 50 52.5 105 3 60-140/20
m,p-Xylene 1.3 100 101 100 100 100 99 1 70-130/20
95-47-6 o-Xylene ND 50 48.7 97 50 47.9 96 2 70-130/20
1330-20-7 Xylene (total)1.3 J 150 150 99 150 148 98 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA65658-1 Limits
1868-53-7 Dibromofluoromethane 101%100%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%100%103%70-130%
2037-26-5 Toluene-D8 100%99%92%70-130%
* = Outside of Control Limits.
31 of 32
FA6565855.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA65658
Account:ATCNCC ATC Group Services LLC
Project:Service & Grocery; 5087 NC Hwy 163, West Jefferson, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA65658-1MS A0218488.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1MSD A0218489.D 5 07/03/19 AB n/a n/a VA2583
FA65658-1 A0218479.D 1 07/03/19 AB n/a n/a VA2583
The QC reported here applies to the following samples:Method: SM 6200B
FA65658-1, FA65658-2, FA65658-3, FA65658-4, FA65658-5, FA65658-6, FA65658-7
CAS No.Surrogate Recoveries MS MSD FA65658-1 Limits
460-00-4 4-Bromofluorobenzene 99%100%100%70-130%
* = Outside of Control Limits.
32 of 32
FA6565855.3.1