WS-1257_30594_CA_SCH_20150323

LETTER REPORT
Johnsons Grocery Store (Incident #30594)
5870 NC Highway 268
Dobson, Surry County, North Carolina
March 23, 2015
Terracon Project No. 71149156
Prepared for:
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Raleigh, North Carolina
Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina
Terracon Consultants, Inc. 2020-E Starita Road Charlotte, NC 28206
P 704-509-1777 F 704-509-1888 terracon.com
March 23, 2015
Mr. Herb Berger
North Carolina Department of Environment and Natural Resources
Division of Waste Management
1637 Mail Service Center
Raleigh, North Carolina 27699-1637
Email:[e-mail]
Re: Letter Report
Johnsons Grocery Store
5870 NC Highway 268
Dobson, Surry County, North Carolina
UST Incident Number: 30594
Terracon Project No. 71149156
Dear Mr. Berger:
Terracon Consultants, Inc. (Terracon) is pleased to submit this Letter Report for the above
referenced property. This report has been prepared in general accordance with North Carolina
Department of Environment and Natural Resources (NCDENR), UST Section Guidelines for
Assessment and Corrective Action for UST Releases,dated July 15, 2008, revised December 2013
and Task Authorization No. 02, approved on November 19, 2014.
Terracon personnel mobilized to the site on January 12, 2015 to conduct a 96-hour Mobile Multi-
Phase Extraction (MMPE) event at monitoring wells MW-1 and MW-5 which contained the highest
levels of petroleum constituents or free product based on recent and historic groundwater sampling
events conducted on the site. The locations of the monitoring wells are depicted on Figure 1,
Terracon was unable to locate well MW-5 and subsequently MMPE activities were only conducted
utilizing well MW-1. Depth to water was 24.78 feet below ground surface prior to commencement of
MMPE activities with approximately 1.94 feet of free product.
The MMPE event was conducted by ZAVA Industrial Inc. from January 12, 2015 to January 16, 2015.
According to ZAVA’s field report dated January 16, 2015, a total of 1,784 gallons of water was
recovered from the well and mass balance calculations indicated total VOC emissions removed from
the well equated to 24.52 gallons. Zava’s field report for the MMPE event is included as Attachment
A. Photographs of the MMPE event are provided in Appendix B.
Johnson’s Grocery Store
Dobson, North Carolina
Project Number 71149156
Incident No. 30594
March 23, 2015
In addition to the MMPE event, Terracon oversaw the advancement of two soil borings (GP-6 and
GP-7) by Probe Technology, Inc. to an approximate depth of 30 feet below ground surface (bgs)
utilizing a Geoprobe® drill rig equipped with a hollow stem rotary auger. The down-hole drilling
equipment was decontaminated prior to advancing each boring. Soils collected from the borings
were screened for organic vapors using a photoionization detector (PID). Soil Samples GP-6(20-25)
and GP-7(20-25) were submitted to Pace Analytical in Huntersville, a North Carolina-approved
laboratory for analysis of risk-based parameters including EPA Methods 8260 and 8270, MADEP
EPH and MADEP VPH. The borings were subsequently converted to Type II groundwater monitoring
wells MW-6 and MW-7. The proposed locations of wells MW-6 and MW-7 were inaccessible and
were adjusted in the field due to the presence of an approximately 25 foot elevation change sloping
towards an intermittent drainage feature along the northern property boundary. The locations of
monitoring wells MW-6 and MW-7 are depicted on Figure 1.
According to the laboratory analytical report, benzene was detected in samples GP-7(20-25) at 9.6
micrograms per kilogram (µg/kg) in excess of the Soil-to-Water Maximum Soil Contaminant
Concentration (MSCC) of 5.6 µg/kg. Additional analytes were detected at concentrations below their
respective Soil-to-Water MSCCs. A copy of laboratory analytical report is included in Appendix C.
Terracon recommends the on-site groundwater monitoring wells be sampled in April 2015 to
evaluate the effectiveness of the MMPE event.
If you have any questions regarding this report or the assessment activities, please contact us at
704-509-1777.
Sincerely,
Terracon Consultants, Inc.
S. Alex Chinery, EI Christopher L. Corbitt, PG
Environmental Staff Professional Senior Project Manager
Attachments: Figure 1
Appendix A – MMPE Field Report by ZAVA Industrial Inc.
Appendix B – MMPE Event Photographs
Appendix C – Laboratory Analytical Reports
Appendix D – Boring Logs and Well Construction Records
Johnson’s Grocery Store
Dobson, North Carolina
Project Number 71149156
Incident No. 30594
March 23, 2015
In addition to the MMPE event, Terracon oversaw the advancement of two soil borings (GP-6 and
GP-7) by Probe Technology, Inc. to an approximate depth of 30 feet below ground surface (bgs)
utilizing a Geoprobe® drill rig equipped with a hollow stem rotary auger. The down-hole drilling
equipment was decontaminated prior to advancing each boring. Soils collected from the borings
were screened for organic vapors using a photoionization detector (PID). Soil Samples GP-6(20-25)
and GP-7(20-25) were submitted to Pace Analytical in Huntersville, a North Carolina-approved
laboratory for analysis of risk-based parameters including EPA Methods 8260 and 8270, MADEP
EPH and MADEP VPH. The borings were subsequently converted to Type II groundwater monitoring
wells MW-6 and MW-7. The locations of monitoring wells MW-6 and MW-7 are depicted on Figure 1.
According to the laboratory analytical report, benzene was detected in samples GP-7(20-25) at 9.6
micrograms per kilogram (µg/kg) in excess of the Soil-to-Water Maximum Soil Contaminant
Concentration (MSCC) of 5.6 µg/kg. Additional analytes were detected at concentrations below their
respective Soil-to-Water MSCCs. A copy of laboratory analytical report is included in Appendix C.
Terracon recommends the on-site groundwater monitoring wells be sampled in April 2015 to
evaluate the effectiveness of the MMPE event.
If you have any questions regarding this report or the assessment activities, please contact us at
704-509-1777.
Sincerely,
Terracon Consultants, Inc.
S. Alex Chinery, EI Christopher L. Corbitt, PG
Environmental Staff Professional Senior Project Manager
Attachments: Figure 1
Appendix A – MMPE Field Report by ZAVA Industrial Inc.
Appendix B – MMPE Event Photographs
Appendix C – Laboratory Analytical Reports
Appendix D – Boring Logs and Well Construction Records
FIGURE
1
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTIONPURPOSES 2020-E Starita Road
Charlotte, NC
Former Johnson’s Grocery
5870 NC Highway 268
Dobson, NC
SITE PLANProject Manager:
Drawn by:
Checked by:
Approved by:
SAC Project No.
File Name:
Date:
Scale:
71149156
SAC
March 2015CLC
2CLC
1” ~ 60’
denotes approximate site
boundary
denotes groundwater
monitoring well.
MW-5
(Not Located)
MW-4
MW-1
MW-2
MW-3
MW-6
MW-7
APPENDIX A
MMPE FIELD REPORT
APPENDIX B
MMPE EVENT PHOTOGRAPHS
Project No. 71149156
Date Photos Taken: January 12, 2015
Johnsons Grocery Store – Dobson, North Carolina
Alleged location of monitoring well MW-5Photo 1
View of tanker with vacuum hose inserted into well MW-1Photo 2
Project No. 71149156
Date Photos Taken: January 12, 2015
Johnsons Grocery Store – Dobson, North Carolina
View of MMPE trailer and tankerPhoto 3
View of the installation of monitoring well MW-7Photo 4
APPENDIX C
LABORATORY ANALYTICAL REPORT
#=CL#
January 16, 2015
LIMS USE: FR - ALEX CHINERY
LIMS OBJECT ID: 92232897
92232897
Project:
Pace Project No.:
RE:
Alex Chinery
Terracon
2020E Starita Road
Charlotte, NC 28206
Johnson Grocery 71149156
Dear Alex Chinery:
Enclosed are the analytical results for sample(s) received by the laboratory on January 12, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Lab ID Sample ID Matrix Date Collected Date Received
92232897001 GP-6 (20-25)Solid 01/12/15 13:14 01/12/15 16:50
92232897002 GP-7 (20-25)Solid 01/12/15 10:24 01/12/15 16:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Lab ID Sample ID Method
Analytes
ReportedAnalysts
92232897001 GP-6 (20-25)MADEP EPH 7RES
MADEP VPH 5BFW
EPA 8270 74BPJ
EPA 8260 70DLK
ASTM D2974-87 1SLJ
92232897002 GP-7 (20-25)MADEP EPH 7RES
MADEP VPH 5BFW
EPA 8270 74RES
EPA 8260 70DLK
ASTM D2974-87 1SLJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-6 (20-25)Lab ID:92232897001 Collected:01/12/15 13:14 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 01/15/15 21:47 N201/15/15 07:2014.1 14.1 1
Aliphatic (C19-C36)15.3 mg/kg 01/15/15 21:47 N201/15/15 07:2014.1 14.1 1
Aromatic (C11-C22)ND mg/kg 01/15/15 21:47 N201/15/15 07:2014.1 14.1 1
Surrogates
Nonatriacontane (S)96 %01/15/15 21:47 7194-86-701/15/15 07:2040-140 1
o-Terphenyl (S)59 %01/15/15 21:47 84-15-101/15/15 07:2040-140 1
2-Fluorobiphenyl (S)71 %01/15/15 21:47 321-60-801/15/15 07:2040-140 1
2-Bromonaphthalene (S)78 %01/15/15 21:47 580-13-201/15/15 07:2040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 01/13/15 17:25 N201/13/15 10:553.0 3.0 1
Aliphatic (C09-C12)ND mg/kg 01/13/15 17:25 N201/13/15 10:553.0 3.0 1
Aromatic (C09-C10)ND mg/kg 01/13/15 17:25 N201/13/15 10:553.0 3.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)93 %01/13/15 17:25 460-00-401/13/15 10:5570-130 1
4-Bromofluorobenzene (PID) (S)89 %01/13/15 17:25 460-00-401/13/15 10:5570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/16/15 15:57 83-32-901/14/15 13:014640107010
Acenaphthylene ND ug/kg 01/16/15 15:57 208-96-801/14/15 13:014640110010
Aniline ND ug/kg 01/16/15 15:57 62-53-301/14/15 13:014640125010
Anthracene ND ug/kg 01/16/15 15:57 120-12-701/14/15 13:014640104010
Benzo(a)anthracene ND ug/kg 01/16/15 15:57 56-55-301/14/15 13:01464085810
Benzo(a)pyrene ND ug/kg 01/16/15 15:57 50-32-801/14/15 13:01464088710
Benzo(b)fluoranthene ND ug/kg 01/16/15 15:57 205-99-201/14/15 13:01464080210
Benzo(g,h,i)perylene ND ug/kg 01/16/15 15:57 191-24-201/14/15 13:014640118010
Benzo(k)fluoranthene ND ug/kg 01/16/15 15:57 207-08-901/14/15 13:01464091510
Benzoic Acid ND ug/kg 01/16/15 15:57 65-85-001/14/15 13:012320084410
Benzyl alcohol ND ug/kg 01/16/15 15:57 100-51-601/14/15 13:01929092910
4-Bromophenylphenyl ether ND ug/kg 01/16/15 15:57 101-55-301/14/15 13:01464084410
Butylbenzylphthalate ND ug/kg 01/16/15 15:57 85-68-701/14/15 13:01464098510
4-Chloro-3-methylphenol ND ug/kg 01/16/15 15:57 59-50-701/14/15 13:01929095710
4-Chloroaniline ND ug/kg 01/16/15 15:57 106-47-801/14/15 13:0123200129010
bis(2-Chloroethoxy)methane ND ug/kg 01/16/15 15:57 111-91-101/14/15 13:014640108010
bis(2-Chloroethyl) ether ND ug/kg 01/16/15 15:57 111-44-401/14/15 13:014640118010
bis(2-Chloroisopropyl) ether ND ug/kg 01/16/15 15:57 108-60-101/14/15 13:014640124010
2-Chloronaphthalene ND ug/kg 01/16/15 15:57 91-58-701/14/15 13:01464091510
2-Chlorophenol ND ug/kg 01/16/15 15:57 95-57-801/14/15 13:014640127010
4-Chlorophenylphenyl ether ND ug/kg 01/16/15 15:57 7005-72-301/14/15 13:01464095710
Chrysene ND ug/kg 01/16/15 15:57 218-01-901/14/15 13:01464061910
Dibenz(a,h)anthracene ND ug/kg 01/16/15 15:57 53-70-301/14/15 13:01464098510
Dibenzofuran ND ug/kg 01/16/15 15:57 132-64-901/14/15 13:01464076010
1,2-Dichlorobenzene ND ug/kg 01/16/15 15:57 95-50-101/14/15 13:014640124010
1,3-Dichlorobenzene ND ug/kg 01/16/15 15:57 541-73-101/14/15 13:014640106010
1,4-Dichlorobenzene ND ug/kg 01/16/15 15:57 106-46-701/14/15 13:014640131010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-6 (20-25)Lab ID:92232897001 Collected:01/12/15 13:14 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 01/16/15 15:57 91-94-101/14/15 13:0123200101010
2,4-Dichlorophenol ND ug/kg 01/16/15 15:57 120-83-201/14/15 13:014640101010
Diethylphthalate ND ug/kg 01/16/15 15:57 84-66-201/14/15 13:01464071810
2,4-Dimethylphenol ND ug/kg 01/16/15 15:57 105-67-901/14/15 13:014640183010
Dimethylphthalate ND ug/kg 01/16/15 15:57 131-11-301/14/15 13:01464094310
Di-n-butylphthalate ND ug/kg 01/16/15 15:57 84-74-201/14/15 13:01464076010
4,6-Dinitro-2-methylphenol ND ug/kg 01/16/15 15:57 534-52-101/14/15 13:01929092910
2,4-Dinitrophenol ND ug/kg 01/16/15 15:57 51-28-501/14/15 13:012320076010
2,4-Dinitrotoluene ND ug/kg 01/16/15 15:57 121-14-201/14/15 13:01464087210
2,6-Dinitrotoluene 4070J ug/kg 01/16/15 15:57 606-20-201/14/15 13:01464097110
Di-n-octylphthalate ND ug/kg 01/16/15 15:57 117-84-001/14/15 13:01464097110
bis(2-Ethylhexyl)phthalate ND ug/kg 01/16/15 15:57 117-81-701/14/15 13:014640127010
Fluoranthene ND ug/kg 01/16/15 15:57 206-44-001/14/15 13:01464067510
Fluorene ND ug/kg 01/16/15 15:57 86-73-701/14/15 13:01464095710
Hexachloro-1,3-butadiene ND ug/kg 01/16/15 15:57 87-68-301/14/15 13:01464080210
Hexachlorobenzene ND ug/kg 01/16/15 15:57 118-74-101/14/15 13:01464059110
Hexachlorocyclopentadiene ND ug/kg 01/16/15 15:57 77-47-401/14/15 13:01464085810
Hexachloroethane ND ug/kg 01/16/15 15:57 67-72-101/14/15 13:014640122010
Indeno(1,2,3-cd)pyrene ND ug/kg 01/16/15 15:57 193-39-501/14/15 13:01464095710
Isophorone ND ug/kg 01/16/15 15:57 78-59-101/14/15 13:014640104010
1-Methylnaphthalene ND ug/kg 01/16/15 15:57 90-12-001/14/15 13:014640121010
2-Methylnaphthalene ND ug/kg 01/16/15 15:57 91-57-601/14/15 13:01464099910
2-Methylphenol(o-Cresol)ND ug/kg 01/16/15 15:57 95-48-701/14/15 13:014640141010
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/16/15 15:5701/14/15 13:014640183010
Naphthalene ND ug/kg 01/16/15 15:57 91-20-301/14/15 13:014640114010
2-Nitroaniline ND ug/kg 01/16/15 15:57 88-74-401/14/15 13:0123200144010
3-Nitroaniline ND ug/kg 01/16/15 15:57 99-09-201/14/15 13:0123200127010
4-Nitroaniline ND ug/kg 01/16/15 15:57 100-01-601/14/15 13:019290131010
Nitrobenzene ND ug/kg 01/16/15 15:57 98-95-301/14/15 13:014640127010
2-Nitrophenol ND ug/kg 01/16/15 15:57 88-75-501/14/15 13:014640113010
4-Nitrophenol ND ug/kg 01/16/15 15:57 100-02-701/14/15 13:012320083010
N-Nitrosodimethylamine ND ug/kg 01/16/15 15:57 62-75-901/14/15 13:014640151010
N-Nitroso-di-n-propylamine ND ug/kg 01/16/15 15:57 621-64-701/14/15 13:01464088710
N-Nitrosodiphenylamine ND ug/kg 01/16/15 15:57 86-30-601/14/15 13:014640138010
Pentachlorophenol ND ug/kg 01/16/15 15:57 87-86-501/14/15 13:012320084410
Phenanthrene ND ug/kg 01/16/15 15:57 85-01-801/14/15 13:01464077410
Phenol ND ug/kg 01/16/15 15:57 108-95-201/14/15 13:014640139010
Pyrene ND ug/kg 01/16/15 15:57 129-00-001/14/15 13:01464078810
1,2,4-Trichlorobenzene ND ug/kg 01/16/15 15:57 120-82-101/14/15 13:01464090110
2,4,5-Trichlorophenol ND ug/kg 01/16/15 15:57 95-95-401/14/15 13:014640144010
2,4,6-Trichlorophenol ND ug/kg 01/16/15 15:57 88-06-201/14/15 13:014640103010
Surrogates
Nitrobenzene-d5 (S)0 %01/16/15 15:57 4165-60-0 D3,S401/14/15 13:0123-110 10
2-Fluorobiphenyl (S)0 %01/16/15 15:57 321-60-801/14/15 13:0130-110 10
Terphenyl-d14 (S)0 %01/16/15 15:57 1718-51-001/14/15 13:0128-110 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-6 (20-25)Lab ID:92232897001 Collected:01/12/15 13:14 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)0 %01/16/15 15:57 13127-88-301/14/15 13:0122-110 10
2-Fluorophenol (S)0 %01/16/15 15:57 367-12-401/14/15 13:0113-110 10
2,4,6-Tribromophenol (S)0 %01/16/15 15:57 118-79-601/14/15 13:0127-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 82.8J ug/kg 01/14/15 15:48 67-64-110310.3 1
Benzene 2.2J ug/kg 01/14/15 15:48 71-43-25.1 1.6 1
Bromobenzene ND ug/kg 01/14/15 15:48 108-86-15.1 2.1 1
Bromochloromethane ND ug/kg 01/14/15 15:48 74-97-55.1 1.7 1
Bromodichloromethane ND ug/kg 01/14/15 15:48 75-27-45.1 1.9 1
Bromoform ND ug/kg 01/14/15 15:48 75-25-25.1 2.4 1
Bromomethane ND ug/kg 01/14/15 15:48 74-83-910.3 2.6 1
2-Butanone (MEK)30.2J ug/kg 01/14/15 15:48 78-93-31033.0 1
n-Butylbenzene ND ug/kg 01/14/15 15:48 104-51-85.1 1.8 1
sec-Butylbenzene ND ug/kg 01/14/15 15:48 135-98-85.1 1.6 1
tert-Butylbenzene ND ug/kg 01/14/15 15:48 98-06-65.1 2.1 1
Carbon tetrachloride ND ug/kg 01/14/15 15:48 56-23-55.1 2.7 1
Chlorobenzene ND ug/kg 01/14/15 15:48 108-90-75.1 1.9 1
Chloroethane ND ug/kg 01/14/15 15:48 75-00-310.3 2.5 1
Chloroform ND ug/kg 01/14/15 15:48 67-66-35.1 1.6 1
Chloromethane ND ug/kg 01/14/15 15:48 74-87-310.3 2.5 1
2-Chlorotoluene ND ug/kg 01/14/15 15:48 95-49-85.1 1.7 1
4-Chlorotoluene ND ug/kg 01/14/15 15:48 106-43-45.1 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/14/15 15:48 96-12-85.1 3.7 1
Dibromochloromethane ND ug/kg 01/14/15 15:48 124-48-15.1 1.8 1
1,2-Dibromoethane (EDB)ND ug/kg 01/14/15 15:48 106-93-45.1 1.8 1
Dibromomethane ND ug/kg 01/14/15 15:48 74-95-35.1 2.6 1
1,2-Dichlorobenzene ND ug/kg 01/14/15 15:48 95-50-15.1 1.9 1
1,3-Dichlorobenzene ND ug/kg 01/14/15 15:48 541-73-15.1 2.1 1
1,4-Dichlorobenzene ND ug/kg 01/14/15 15:48 106-46-75.1 1.7 1
Dichlorodifluoromethane ND ug/kg 01/14/15 15:48 75-71-810.3 3.7 1
1,1-Dichloroethane ND ug/kg 01/14/15 15:48 75-34-35.1 1.5 1
1,2-Dichloroethane ND ug/kg 01/14/15 15:48 107-06-25.1 2.3 1
1,1-Dichloroethene ND ug/kg 01/14/15 15:48 75-35-45.1 1.8 1
cis-1,2-Dichloroethene ND ug/kg 01/14/15 15:48 156-59-25.1 1.4 1
trans-1,2-Dichloroethene ND ug/kg 01/14/15 15:48 156-60-55.1 1.9 1
1,2-Dichloropropane ND ug/kg 01/14/15 15:48 78-87-55.1 1.7 1
1,3-Dichloropropane ND ug/kg 01/14/15 15:48 142-28-95.1 1.9 1
2,2-Dichloropropane ND ug/kg 01/14/15 15:48 594-20-75.1 1.7 1
1,1-Dichloropropene ND ug/kg 01/14/15 15:48 563-58-65.1 1.5 1
cis-1,3-Dichloropropene ND ug/kg 01/14/15 15:48 10061-01-55.1 1.8 1
trans-1,3-Dichloropropene ND ug/kg 01/14/15 15:48 10061-02-65.1 1.5 1
Diisopropyl ether ND ug/kg 01/14/15 15:48 108-20-35.1 1.7 1
Ethylbenzene ND ug/kg 01/14/15 15:48 100-41-45.1 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-6 (20-25)Lab ID:92232897001 Collected:01/12/15 13:14 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene ND ug/kg 01/14/15 15:48 87-68-35.1 2.1 1
2-Hexanone ND ug/kg 01/14/15 15:48 591-78-651.3 4.0 1
Isopropylbenzene (Cumene)ND ug/kg 01/14/15 15:48 98-82-85.1 1.9 1
p-Isopropyltoluene ND ug/kg 01/14/15 15:48 99-87-65.1 1.7 1
Methylene Chloride ND ug/kg 01/14/15 15:48 75-09-220.5 3.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/14/15 15:48 108-10-151.3 3.8 1
Methyl-tert-butyl ether ND ug/kg 01/14/15 15:48 1634-04-45.1 1.5 1
Naphthalene ND ug/kg 01/14/15 15:48 91-20-35.1 1.2 1
n-Propylbenzene ND ug/kg 01/14/15 15:48 103-65-15.1 1.7 1
Styrene ND ug/kg 01/14/15 15:48 100-42-55.1 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/14/15 15:48 630-20-65.1 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/14/15 15:48 79-34-55.1 1.9 1
Tetrachloroethene ND ug/kg 01/14/15 15:48 127-18-45.1 1.7 1
Toluene ND ug/kg 01/14/15 15:48 108-88-35.1 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 01/14/15 15:48 87-61-65.1 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 01/14/15 15:48 120-82-15.1 1.6 1
1,1,1-Trichloroethane ND ug/kg 01/14/15 15:48 71-55-65.1 1.8 1
1,1,2-Trichloroethane ND ug/kg 01/14/15 15:48 79-00-55.1 2.2 1
Trichloroethene ND ug/kg 01/14/15 15:48 79-01-65.1 2.2 1
Trichlorofluoromethane ND ug/kg 01/14/15 15:48 75-69-45.1 2.3 1
1,2,3-Trichloropropane ND ug/kg 01/14/15 15:48 96-18-45.1 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 01/14/15 15:48 95-63-65.1 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 01/14/15 15:48 108-67-85.1 1.8 1
Vinyl acetate ND ug/kg 01/14/15 15:48 108-05-451.3 9.0 1
Vinyl chloride ND ug/kg 01/14/15 15:48 75-01-410.3 1.8 1
Xylene (Total)ND ug/kg 01/14/15 15:48 1330-20-710.3 3.7 1
m&p-Xylene ND ug/kg 01/14/15 15:48 179601-23-110.3 3.7 1
o-Xylene ND ug/kg 01/14/15 15:48 95-47-65.1 1.9 1
Surrogates
Toluene-d8 (S)99 %01/14/15 15:48 2037-26-570-130 1
4-Bromofluorobenzene (S)83 %01/14/15 15:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %01/14/15 15:48 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.9 %01/14/15 08:110.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-7 (20-25)Lab ID:92232897002 Collected:01/12/15 10:24 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 01/15/15 22:19 N201/15/15 07:2012.9 12.9 1
Aliphatic (C19-C36)ND mg/kg 01/15/15 22:19 N201/15/15 07:2012.9 12.9 1
Aromatic (C11-C22)ND mg/kg 01/15/15 22:19 N201/15/15 07:2012.9 12.9 1
Surrogates
Nonatriacontane (S)67 %01/15/15 22:19 7194-86-701/15/15 07:2040-140 1
o-Terphenyl (S)57 %01/15/15 22:19 84-15-101/15/15 07:2040-140 1
2-Fluorobiphenyl (S)68 %01/15/15 22:19 321-60-801/15/15 07:2040-140 1
2-Bromonaphthalene (S)75 %01/15/15 22:19 580-13-201/15/15 07:2040-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)5.7 mg/kg 01/13/15 17:51 N201/13/15 10:552.5 2.5 1
Aliphatic (C09-C12)ND mg/kg 01/13/15 17:51 N201/13/15 10:552.5 2.5 1
Aromatic (C09-C10)ND mg/kg 01/13/15 17:51 N201/13/15 10:552.5 2.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)97 %01/13/15 17:51 460-00-401/13/15 10:5570-130 1
4-Bromofluorobenzene (PID) (S)92 %01/13/15 17:51 460-00-401/13/15 10:5570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 01/16/15 15:29 83-32-901/14/15 13:01425097810
Acenaphthylene ND ug/kg 01/16/15 15:29 208-96-801/14/15 13:014250100010
Aniline ND ug/kg 01/16/15 15:29 62-53-301/14/15 13:014250115010
Anthracene ND ug/kg 01/16/15 15:29 120-12-701/14/15 13:01425095210
Benzo(a)anthracene ND ug/kg 01/16/15 15:29 56-55-301/14/15 13:01425078510
Benzo(a)pyrene ND ug/kg 01/16/15 15:29 50-32-801/14/15 13:01425081110
Benzo(b)fluoranthene ND ug/kg 01/16/15 15:29 205-99-201/14/15 13:01425073410
Benzo(g,h,i)perylene ND ug/kg 01/16/15 15:29 191-24-201/14/15 13:014250108010
Benzo(k)fluoranthene ND ug/kg 01/16/15 15:29 207-08-901/14/15 13:01425083710
Benzoic Acid ND ug/kg 01/16/15 15:29 65-85-001/14/15 13:012120077210
Benzyl alcohol ND ug/kg 01/16/15 15:29 100-51-601/14/15 13:01849084910
4-Bromophenylphenyl ether ND ug/kg 01/16/15 15:29 101-55-301/14/15 13:01425077210
Butylbenzylphthalate ND ug/kg 01/16/15 15:29 85-68-701/14/15 13:01425090110
4-Chloro-3-methylphenol ND ug/kg 01/16/15 15:29 59-50-701/14/15 13:01849087510
4-Chloroaniline ND ug/kg 01/16/15 15:29 106-47-801/14/15 13:0121200118010
bis(2-Chloroethoxy)methane ND ug/kg 01/16/15 15:29 111-91-101/14/15 13:01425099110
bis(2-Chloroethyl) ether ND ug/kg 01/16/15 15:29 111-44-401/14/15 13:014250108010
bis(2-Chloroisopropyl) ether ND ug/kg 01/16/15 15:29 108-60-101/14/15 13:014250113010
2-Chloronaphthalene ND ug/kg 01/16/15 15:29 91-58-701/14/15 13:01425083710
2-Chlorophenol ND ug/kg 01/16/15 15:29 95-57-801/14/15 13:014250116010
4-Chlorophenylphenyl ether ND ug/kg 01/16/15 15:29 7005-72-301/14/15 13:01425087510
Chrysene ND ug/kg 01/16/15 15:29 218-01-901/14/15 13:01425056610
Dibenz(a,h)anthracene ND ug/kg 01/16/15 15:29 53-70-301/14/15 13:01425090110
Dibenzofuran ND ug/kg 01/16/15 15:29 132-64-901/14/15 13:01425069510
1,2-Dichlorobenzene ND ug/kg 01/16/15 15:29 95-50-101/14/15 13:014250113010
1,3-Dichlorobenzene ND ug/kg 01/16/15 15:29 541-73-101/14/15 13:01425096510
1,4-Dichlorobenzene ND ug/kg 01/16/15 15:29 106-46-701/14/15 13:014250120010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-7 (20-25)Lab ID:92232897002 Collected:01/12/15 10:24 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 01/16/15 15:29 91-94-101/14/15 13:012120092710
2,4-Dichlorophenol ND ug/kg 01/16/15 15:29 120-83-201/14/15 13:01425092710
Diethylphthalate ND ug/kg 01/16/15 15:29 84-66-201/14/15 13:01425065610
2,4-Dimethylphenol ND ug/kg 01/16/15 15:29 105-67-901/14/15 13:014250167010
Dimethylphthalate ND ug/kg 01/16/15 15:29 131-11-301/14/15 13:01425086210
Di-n-butylphthalate ND ug/kg 01/16/15 15:29 84-74-201/14/15 13:01425069510
4,6-Dinitro-2-methylphenol ND ug/kg 01/16/15 15:29 534-52-101/14/15 13:01849084910
2,4-Dinitrophenol ND ug/kg 01/16/15 15:29 51-28-501/14/15 13:012120069510
2,4-Dinitrotoluene ND ug/kg 01/16/15 15:29 121-14-201/14/15 13:01425079810
2,6-Dinitrotoluene ND ug/kg 01/16/15 15:29 606-20-201/14/15 13:01425088810
Di-n-octylphthalate ND ug/kg 01/16/15 15:29 117-84-001/14/15 13:01425088810
bis(2-Ethylhexyl)phthalate ND ug/kg 01/16/15 15:29 117-81-701/14/15 13:014250116010
Fluoranthene ND ug/kg 01/16/15 15:29 206-44-001/14/15 13:01425061810
Fluorene ND ug/kg 01/16/15 15:29 86-73-701/14/15 13:01425087510
Hexachloro-1,3-butadiene ND ug/kg 01/16/15 15:29 87-68-301/14/15 13:01425073410
Hexachlorobenzene ND ug/kg 01/16/15 15:29 118-74-101/14/15 13:01425054110
Hexachlorocyclopentadiene ND ug/kg 01/16/15 15:29 77-47-401/14/15 13:01425078510
Hexachloroethane ND ug/kg 01/16/15 15:29 67-72-101/14/15 13:014250112010
Indeno(1,2,3-cd)pyrene ND ug/kg 01/16/15 15:29 193-39-501/14/15 13:01425087510
Isophorone ND ug/kg 01/16/15 15:29 78-59-101/14/15 13:01425095210
1-Methylnaphthalene ND ug/kg 01/16/15 15:29 90-12-001/14/15 13:014250111010
2-Methylnaphthalene ND ug/kg 01/16/15 15:29 91-57-601/14/15 13:01425091410
2-Methylphenol(o-Cresol)ND ug/kg 01/16/15 15:29 95-48-701/14/15 13:014250129010
3&4-Methylphenol(m&p Cresol)ND ug/kg 01/16/15 15:2901/14/15 13:014250167010
Naphthalene ND ug/kg 01/16/15 15:29 91-20-301/14/15 13:014250104010
2-Nitroaniline ND ug/kg 01/16/15 15:29 88-74-401/14/15 13:0121200131010
3-Nitroaniline ND ug/kg 01/16/15 15:29 99-09-201/14/15 13:0121200116010
4-Nitroaniline ND ug/kg 01/16/15 15:29 100-01-601/14/15 13:018490120010
Nitrobenzene ND ug/kg 01/16/15 15:29 98-95-301/14/15 13:014250116010
2-Nitrophenol ND ug/kg 01/16/15 15:29 88-75-501/14/15 13:014250103010
4-Nitrophenol ND ug/kg 01/16/15 15:29 100-02-701/14/15 13:012120075910
N-Nitrosodimethylamine ND ug/kg 01/16/15 15:29 62-75-901/14/15 13:014250138010
N-Nitroso-di-n-propylamine ND ug/kg 01/16/15 15:29 621-64-701/14/15 13:01425081110
N-Nitrosodiphenylamine ND ug/kg 01/16/15 15:29 86-30-601/14/15 13:014250126010
Pentachlorophenol ND ug/kg 01/16/15 15:29 87-86-501/14/15 13:012120077210
Phenanthrene ND ug/kg 01/16/15 15:29 85-01-801/14/15 13:01425070810
Phenol ND ug/kg 01/16/15 15:29 108-95-201/14/15 13:014250127010
Pyrene ND ug/kg 01/16/15 15:29 129-00-001/14/15 13:01425072110
1,2,4-Trichlorobenzene ND ug/kg 01/16/15 15:29 120-82-101/14/15 13:01425082410
2,4,5-Trichlorophenol ND ug/kg 01/16/15 15:29 95-95-401/14/15 13:014250131010
2,4,6-Trichlorophenol ND ug/kg 01/16/15 15:29 88-06-201/14/15 13:01425094010
Surrogates
Nitrobenzene-d5 (S)0 %01/16/15 15:29 4165-60-0 D3,S401/14/15 13:0123-110 10
2-Fluorobiphenyl (S)0 %01/16/15 15:29 321-60-801/14/15 13:0130-110 10
Terphenyl-d14 (S)0 %01/16/15 15:29 1718-51-001/14/15 13:0128-110 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-7 (20-25)Lab ID:92232897002 Collected:01/12/15 10:24 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
Phenol-d6 (S)0 %01/16/15 15:29 13127-88-301/14/15 13:0122-110 10
2-Fluorophenol (S)0 %01/16/15 15:29 367-12-401/14/15 13:0113-110 10
2,4,6-Tribromophenol (S)0 %01/16/15 15:29 118-79-601/14/15 13:0127-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 01/14/15 16:08 67-64-110710.7 1
Benzene 9.6 ug/kg 01/14/15 16:08 71-43-25.3 1.7 1
Bromobenzene ND ug/kg 01/14/15 16:08 108-86-15.3 2.1 1
Bromochloromethane ND ug/kg 01/14/15 16:08 74-97-55.3 1.8 1
Bromodichloromethane ND ug/kg 01/14/15 16:08 75-27-45.3 2.0 1
Bromoform ND ug/kg 01/14/15 16:08 75-25-25.3 2.5 1
Bromomethane ND ug/kg 01/14/15 16:08 74-83-910.7 2.7 1
2-Butanone (MEK)ND ug/kg 01/14/15 16:08 78-93-31073.1 1
n-Butylbenzene ND ug/kg 01/14/15 16:08 104-51-85.3 1.9 1
sec-Butylbenzene ND ug/kg 01/14/15 16:08 135-98-85.3 1.7 1
tert-Butylbenzene ND ug/kg 01/14/15 16:08 98-06-65.3 2.1 1
Carbon tetrachloride ND ug/kg 01/14/15 16:08 56-23-55.3 2.8 1
Chlorobenzene ND ug/kg 01/14/15 16:08 108-90-75.3 2.0 1
Chloroethane ND ug/kg 01/14/15 16:08 75-00-310.7 2.6 1
Chloroform ND ug/kg 01/14/15 16:08 67-66-35.3 1.7 1
Chloromethane ND ug/kg 01/14/15 16:08 74-87-310.7 2.6 1
2-Chlorotoluene ND ug/kg 01/14/15 16:08 95-49-85.3 1.8 1
4-Chlorotoluene ND ug/kg 01/14/15 16:08 106-43-45.3 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/14/15 16:08 96-12-85.3 3.8 1
Dibromochloromethane ND ug/kg 01/14/15 16:08 124-48-15.3 1.9 1
1,2-Dibromoethane (EDB)ND ug/kg 01/14/15 16:08 106-93-45.3 1.9 1
Dibromomethane ND ug/kg 01/14/15 16:08 74-95-35.3 2.7 1
1,2-Dichlorobenzene ND ug/kg 01/14/15 16:08 95-50-15.3 2.0 1
1,3-Dichlorobenzene ND ug/kg 01/14/15 16:08 541-73-15.3 2.1 1
1,4-Dichlorobenzene ND ug/kg 01/14/15 16:08 106-46-75.3 1.8 1
Dichlorodifluoromethane ND ug/kg 01/14/15 16:08 75-71-810.7 3.8 1
1,1-Dichloroethane ND ug/kg 01/14/15 16:08 75-34-35.3 1.6 1
1,2-Dichloroethane ND ug/kg 01/14/15 16:08 107-06-25.3 2.3 1
1,1-Dichloroethene ND ug/kg 01/14/15 16:08 75-35-45.3 1.9 1
cis-1,2-Dichloroethene ND ug/kg 01/14/15 16:08 156-59-25.3 1.5 1
trans-1,2-Dichloroethene ND ug/kg 01/14/15 16:08 156-60-55.3 2.0 1
1,2-Dichloropropane ND ug/kg 01/14/15 16:08 78-87-55.3 1.8 1
1,3-Dichloropropane ND ug/kg 01/14/15 16:08 142-28-95.3 2.0 1
2,2-Dichloropropane ND ug/kg 01/14/15 16:08 594-20-75.3 1.8 1
1,1-Dichloropropene ND ug/kg 01/14/15 16:08 563-58-65.3 1.6 1
cis-1,3-Dichloropropene ND ug/kg 01/14/15 16:08 10061-01-55.3 1.9 1
trans-1,3-Dichloropropene ND ug/kg 01/14/15 16:08 10061-02-65.3 1.6 1
Diisopropyl ether ND ug/kg 01/14/15 16:08 108-20-35.3 1.8 1
Ethylbenzene ND ug/kg 01/14/15 16:08 100-41-45.3 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Sample:GP-7 (20-25)Lab ID:92232897002 Collected:01/12/15 10:24 Received:01/12/15 16:50 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Hexachloro-1,3-butadiene ND ug/kg 01/14/15 16:08 87-68-35.3 2.1 1
2-Hexanone ND ug/kg 01/14/15 16:08 591-78-653.4 4.2 1
Isopropylbenzene (Cumene)ND ug/kg 01/14/15 16:08 98-82-85.3 2.0 1
p-Isopropyltoluene 10.4 ug/kg 01/14/15 16:08 99-87-65.3 1.8 1
Methylene Chloride ND ug/kg 01/14/15 16:08 75-09-221.3 3.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/14/15 16:08 108-10-153.4 3.9 1
Methyl-tert-butyl ether ND ug/kg 01/14/15 16:08 1634-04-45.3 1.6 1
Naphthalene ND ug/kg 01/14/15 16:08 91-20-35.3 1.3 1
n-Propylbenzene ND ug/kg 01/14/15 16:08 103-65-15.3 1.8 1
Styrene ND ug/kg 01/14/15 16:08 100-42-55.3 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/14/15 16:08 630-20-65.3 2.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/14/15 16:08 79-34-55.3 2.0 1
Tetrachloroethene ND ug/kg 01/14/15 16:08 127-18-45.3 1.8 1
Toluene 2.6J ug/kg 01/14/15 16:08 108-88-35.3 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 01/14/15 16:08 87-61-65.3 2.3 1
1,2,4-Trichlorobenzene ND ug/kg 01/14/15 16:08 120-82-15.3 1.7 1
1,1,1-Trichloroethane ND ug/kg 01/14/15 16:08 71-55-65.3 1.9 1
1,1,2-Trichloroethane ND ug/kg 01/14/15 16:08 79-00-55.3 2.2 1
Trichloroethene ND ug/kg 01/14/15 16:08 79-01-65.3 2.2 1
Trichlorofluoromethane ND ug/kg 01/14/15 16:08 75-69-45.3 2.3 1
1,2,3-Trichloropropane ND ug/kg 01/14/15 16:08 96-18-45.3 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 01/14/15 16:08 95-63-65.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 01/14/15 16:08 108-67-85.3 1.9 1
Vinyl acetate ND ug/kg 01/14/15 16:08 108-05-453.4 9.4 1
Vinyl chloride ND ug/kg 01/14/15 16:08 75-01-410.7 1.9 1
Xylene (Total)ND ug/kg 01/14/15 16:08 1330-20-710.7 3.8 1
m&p-Xylene ND ug/kg 01/14/15 16:08 179601-23-110.7 3.8 1
o-Xylene ND ug/kg 01/14/15 16:08 95-47-65.3 2.0 1
Surrogates
Toluene-d8 (S)97 %01/14/15 16:08 2037-26-570-130 1
4-Bromofluorobenzene (S)87 %01/14/15 16:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %01/14/15 16:08 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.3 %01/14/15 08:110.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/8909
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92232897001, 92232897002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1368683
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N201/13/15 11:21
Aliphatic (C09-C12)mg/kg ND 2.5 N201/13/15 11:21
Aromatic (C09-C10)mg/kg ND 2.5 N201/13/15 11:21
4-Bromofluorobenzene (FID) (S)%96 70-130 01/13/15 11:21
4-Bromofluorobenzene (PID) (S)%93 70-130 01/13/15 11:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1368684LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1368685
Aliphatic (C05-C08)mg/kg 14.1 N2159470-1308913.3 6 25
Aliphatic (C09-C12)mg/kg 13.6 N2159130-1309113.7 1 25
Aromatic (C09-C10)mg/kg 4.8 N259670-130934.7 3 25
4-Bromofluorobenzene (FID) (S)%93 70-13093
4-Bromofluorobenzene (PID) (S)%93 70-13093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/29987
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92232897001, 92232897002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1369776
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.6 01/14/15 12:10
1,1,1-Trichloroethane ug/kg ND 4.6 01/14/15 12:10
1,1,2,2-Tetrachloroethane ug/kg ND 4.6 01/14/15 12:10
1,1,2-Trichloroethane ug/kg ND 4.6 01/14/15 12:10
1,1-Dichloroethane ug/kg ND 4.6 01/14/15 12:10
1,1-Dichloroethene ug/kg ND 4.6 01/14/15 12:10
1,1-Dichloropropene ug/kg ND 4.6 01/14/15 12:10
1,2,3-Trichlorobenzene ug/kg ND 4.6 01/14/15 12:10
1,2,3-Trichloropropane ug/kg ND 4.6 01/14/15 12:10
1,2,4-Trichlorobenzene ug/kg ND 4.6 01/14/15 12:10
1,2,4-Trimethylbenzene ug/kg ND 4.6 01/14/15 12:10
1,2-Dibromo-3-chloropropane ug/kg ND 4.6 01/14/15 12:10
1,2-Dibromoethane (EDB)ug/kg ND 4.6 01/14/15 12:10
1,2-Dichlorobenzene ug/kg ND 4.6 01/14/15 12:10
1,2-Dichloroethane ug/kg ND 4.6 01/14/15 12:10
1,2-Dichloropropane ug/kg ND 4.6 01/14/15 12:10
1,3,5-Trimethylbenzene ug/kg ND 4.6 01/14/15 12:10
1,3-Dichlorobenzene ug/kg ND 4.6 01/14/15 12:10
1,3-Dichloropropane ug/kg ND 4.6 01/14/15 12:10
1,4-Dichlorobenzene ug/kg ND 4.6 01/14/15 12:10
2,2-Dichloropropane ug/kg ND 4.6 01/14/15 12:10
2-Butanone (MEK)ug/kg ND 92.1 01/14/15 12:10
2-Chlorotoluene ug/kg ND 4.6 01/14/15 12:10
2-Hexanone ug/kg ND 46.0 01/14/15 12:10
4-Chlorotoluene ug/kg ND 4.6 01/14/15 12:10
4-Methyl-2-pentanone (MIBK)ug/kg ND 46.0 01/14/15 12:10
Acetone ug/kg ND 92.1 01/14/15 12:10
Benzene ug/kg ND 4.6 01/14/15 12:10
Bromobenzene ug/kg ND 4.6 01/14/15 12:10
Bromochloromethane ug/kg ND 4.6 01/14/15 12:10
Bromodichloromethane ug/kg ND 4.6 01/14/15 12:10
Bromoform ug/kg ND 4.6 01/14/15 12:10
Bromomethane ug/kg ND 9.2 01/14/15 12:10
Carbon tetrachloride ug/kg ND 4.6 01/14/15 12:10
Chlorobenzene ug/kg ND 4.6 01/14/15 12:10
Chloroethane ug/kg ND 9.2 01/14/15 12:10
Chloroform ug/kg ND 4.6 01/14/15 12:10
Chloromethane ug/kg ND 9.2 01/14/15 12:10
cis-1,2-Dichloroethene ug/kg ND 4.6 01/14/15 12:10
cis-1,3-Dichloropropene ug/kg ND 4.6 01/14/15 12:10
Dibromochloromethane ug/kg ND 4.6 01/14/15 12:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1369776
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 4.6 01/14/15 12:10
Dichlorodifluoromethane ug/kg ND 9.2 01/14/15 12:10
Diisopropyl ether ug/kg ND 4.6 01/14/15 12:10
Ethylbenzene ug/kg ND 4.6 01/14/15 12:10
Hexachloro-1,3-butadiene ug/kg ND 4.6 01/14/15 12:10
Isopropylbenzene (Cumene)ug/kg ND 4.6 01/14/15 12:10
m&p-Xylene ug/kg ND 9.2 01/14/15 12:10
Methyl-tert-butyl ether ug/kg ND 4.6 01/14/15 12:10
Methylene Chloride ug/kg ND 18.4 01/14/15 12:10
n-Butylbenzene ug/kg ND 4.6 01/14/15 12:10
n-Propylbenzene ug/kg ND 4.6 01/14/15 12:10
Naphthalene ug/kg ND 4.6 01/14/15 12:10
o-Xylene ug/kg ND 4.6 01/14/15 12:10
p-Isopropyltoluene ug/kg ND 4.6 01/14/15 12:10
sec-Butylbenzene ug/kg ND 4.6 01/14/15 12:10
Styrene ug/kg ND 4.6 01/14/15 12:10
tert-Butylbenzene ug/kg ND 4.6 01/14/15 12:10
Tetrachloroethene ug/kg ND 4.6 01/14/15 12:10
Toluene ug/kg ND 4.6 01/14/15 12:10
trans-1,2-Dichloroethene ug/kg ND 4.6 01/14/15 12:10
trans-1,3-Dichloropropene ug/kg ND 4.6 01/14/15 12:10
Trichloroethene ug/kg ND 4.6 01/14/15 12:10
Trichlorofluoromethane ug/kg ND 4.6 01/14/15 12:10
Vinyl acetate ug/kg ND 46.0 01/14/15 12:10
Vinyl chloride ug/kg ND 9.2 01/14/15 12:10
Xylene (Total)ug/kg ND 9.2 01/14/15 12:10
1,2-Dichloroethane-d4 (S)%103 70-132 01/14/15 12:10
4-Bromofluorobenzene (S)%92 70-130 01/14/15 12:10
Toluene-d8 (S)%103 70-130 01/14/15 12:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369777LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.945.8 109 74-137
1,1,1-Trichloroethane ug/kg 47.345.8 103 67-140
1,1,2,2-Tetrachloroethane ug/kg 47.445.8 104 72-141
1,1,2-Trichloroethane ug/kg 51.245.8 112 78-138
1,1-Dichloroethane ug/kg 48.345.8 105 69-134
1,1-Dichloroethene ug/kg 44.845.8 98 67-138
1,1-Dichloropropene ug/kg 49.845.8 109 69-139
1,2,3-Trichlorobenzene ug/kg 49.245.8 107 70-146
1,2,3-Trichloropropane ug/kg 50.145.8 109 69-144
1,2,4-Trichlorobenzene ug/kg 47.445.8 104 68-148
1,2,4-Trimethylbenzene ug/kg 49.345.8 108 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369777LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 48.545.8 106 65-140
1,2-Dibromoethane (EDB)ug/kg 51.945.8 113 77-135
1,2-Dichlorobenzene ug/kg 48.045.8 105 77-141
1,2-Dichloroethane ug/kg 47.845.8 104 65-137
1,2-Dichloropropane ug/kg 49.645.8 108 72-136
1,3,5-Trimethylbenzene ug/kg 49.145.8 107 76-133
1,3-Dichlorobenzene ug/kg 47.645.8 104 74-138
1,3-Dichloropropane ug/kg 50.845.8 111 71-139
1,4-Dichlorobenzene ug/kg 48.545.8 106 76-138
2,2-Dichloropropane ug/kg 47.345.8 103 68-137
2-Butanone (MEK)ug/kg 97.091.6 106 58-147
2-Chlorotoluene ug/kg 45.345.8 99 73-139
2-Hexanone ug/kg 10191.6 111 62-145
4-Chlorotoluene ug/kg 48.145.8 105 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 10591.6 114 64-149
Acetone ug/kg 92.291.6 101 53-153
Benzene ug/kg 52.045.8 114 73-135
Bromobenzene ug/kg 51.345.8 112 75-133
Bromochloromethane ug/kg 46.545.8 101 73-134
Bromodichloromethane ug/kg 46.545.8 101 71-135
Bromoform ug/kg 47.945.8 105 66-141
Bromomethane ug/kg 60.745.8 133 53-160
Carbon tetrachloride ug/kg 47.745.8 104 60-145
Chlorobenzene ug/kg 48.745.8 106 78-130
Chloroethane ug/kg 55.945.8 122 64-149
Chloroform ug/kg 44.245.8 97 70-134
Chloromethane ug/kg 54.045.8 118 52-150
cis-1,2-Dichloroethene ug/kg 49.345.8 108 70-133
cis-1,3-Dichloropropene ug/kg 49.945.8 109 68-134
Dibromochloromethane ug/kg 46.845.8 102 71-138
Dibromomethane ug/kg 49.245.8 108 74-130
Dichlorodifluoromethane ug/kg 52.8 F345.8 115 40-160
Diisopropyl ether ug/kg 44.645.8 97 69-141
Ethylbenzene ug/kg 50.445.8 110 75-133
Hexachloro-1,3-butadiene ug/kg 45.845.8 100 68-143
Isopropylbenzene (Cumene)ug/kg 50.745.8 111 76-143
m&p-Xylene ug/kg 10091.6 109 75-136
Methyl-tert-butyl ether ug/kg 43.945.8 96 68-144
Methylene Chloride ug/kg 48.745.8 106 45-154
n-Butylbenzene ug/kg 48.445.8 106 72-137
n-Propylbenzene ug/kg 48.445.8 106 76-136
Naphthalene ug/kg 51.845.8 113 68-151
o-Xylene ug/kg 48.245.8 105 76-141
p-Isopropyltoluene ug/kg 48.145.8 105 76-140
sec-Butylbenzene ug/kg 48.645.8 106 79-139
Styrene ug/kg 50.745.8 111 79-137
tert-Butylbenzene ug/kg 44.345.8 97 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369777LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 42.145.8 92 71-138
Toluene ug/kg 50.745.8 111 74-131
trans-1,2-Dichloroethene ug/kg 47.445.8 104 67-135
trans-1,3-Dichloropropene ug/kg 52.345.8 114 65-146
Trichloroethene ug/kg 53.645.8 117 67-135
Trichlorofluoromethane ug/kg 56.6 F345.8 124 59-144
Vinyl acetate ug/kg 61.6 F391.6 67 40-160
Vinyl chloride ug/kg 50.045.8 109 56-141
Xylene (Total)ug/kg 148137 108 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1370674MATRIX SPIKE SAMPLE:
MSSpike
Result
92232780037
1,1,1,2-Tetrachloroethane ug/kg 22.222.4 99 70-130ND
1,1,1-Trichloroethane ug/kg 22.622.4 101 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 25.222.4 113 70-130ND
1,1,2-Trichloroethane ug/kg 23.822.4 106 70-130ND
1,1-Dichloroethane ug/kg 24.822.4 111 70-130ND
1,1-Dichloroethene ug/kg 23.922.4 107 49-180ND
1,1-Dichloropropene ug/kg 24.622.4 110 70-130ND
1,2,3-Trichlorobenzene ug/kg 21.022.4 94 70-130ND
1,2,3-Trichloropropane ug/kg 21.822.4 97 70-130ND
1,2,4-Trichlorobenzene ug/kg 19.822.4 88 70-130ND
1,2,4-Trimethylbenzene ug/kg 22.422.4 100 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 23.822.4 106 70-130ND
1,2-Dibromoethane (EDB)ug/kg 23.622.4 105 70-130ND
1,2-Dichlorobenzene ug/kg 21.422.4 95 70-130ND
1,2-Dichloroethane ug/kg 24.522.4 109 70-130ND
1,2-Dichloropropane ug/kg 23.422.4 104 70-130ND
1,3,5-Trimethylbenzene ug/kg 22.622.4 101 70-130ND
1,3-Dichlorobenzene ug/kg 21.122.4 94 70-130ND
1,3-Dichloropropane ug/kg 22.622.4 101 70-130ND
1,4-Dichlorobenzene ug/kg 21.222.4 95 70-130ND
2,2-Dichloropropane ug/kg 21.822.4 97 70-130ND
2-Butanone (MEK)ug/kg 58.3J44.8 130 70-130ND
2-Chlorotoluene ug/kg 21.522.4 96 70-130ND
2-Hexanone ug/kg 41.5J44.8 93 70-130ND
4-Chlorotoluene ug/kg 22.222.4 99 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 44.4J44.8 99 70-130ND
Acetone ug/kg 46.6J44.8 104 70-130ND
Benzene ug/kg 24.222.4 108 50-166ND
Bromobenzene ug/kg 23.822.4 106 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1370674MATRIX SPIKE SAMPLE:
MSSpike
Result
92232780037
Bromochloromethane ug/kg 23.122.4 103 70-130ND
Bromodichloromethane ug/kg 21.022.4 94 70-130ND
Bromoform ug/kg 19.822.4 89 70-130ND
Bromomethane ug/kg 22.822.4 102 70-130ND
Carbon tetrachloride ug/kg 21.222.4 95 70-130ND
Chlorobenzene ug/kg 22.422.4 100 43-169ND
Chloroethane ug/kg 29.3 M022.4 131 70-130ND
Chloroform ug/kg 22.422.4 100 70-130ND
Chloromethane ug/kg 27.122.4 121 70-130ND
cis-1,2-Dichloroethene ug/kg 25.022.4 112 70-130ND
cis-1,3-Dichloropropene ug/kg 21.922.4 98 70-130ND
Dibromochloromethane ug/kg 19.122.4 85 70-130ND
Dibromomethane ug/kg 22.122.4 99 70-130ND
Dichlorodifluoromethane ug/kg 27.722.4 124 70-130ND
Diisopropyl ether ug/kg 23.222.4 104 70-130ND
Ethylbenzene ug/kg 23.422.4 105 70-130ND
Hexachloro-1,3-butadiene ug/kg 20.022.4 89 70-130ND
Isopropylbenzene (Cumene)ug/kg 23.122.4 103 70-130ND
m&p-Xylene ug/kg 46.444.8 103 70-130ND
Methyl-tert-butyl ether ug/kg 22.622.4 101 70-130ND
Methylene Chloride ug/kg 26.522.4 118 70-130ND
n-Butylbenzene ug/kg 22.222.4 99 70-130ND
n-Propylbenzene ug/kg 22.722.4 101 70-130ND
Naphthalene ug/kg 21.922.4 98 70-130ND
o-Xylene ug/kg 22.322.4 100 70-130ND
p-Isopropyltoluene ug/kg 22.122.4 99 70-130ND
sec-Butylbenzene ug/kg 23.422.4 104 70-130ND
Styrene ug/kg 22.622.4 101 70-130ND
tert-Butylbenzene ug/kg 20.522.4 91 70-130ND
Tetrachloroethene ug/kg 20.622.4 86 70-130ND
Toluene ug/kg 23.522.4 105 52-163ND
trans-1,2-Dichloroethene ug/kg 24.722.4 110 70-130ND
trans-1,3-Dichloropropene ug/kg 22.822.4 102 70-130ND
Trichloroethene ug/kg 22.622.4 101 49-167ND
Trichlorofluoromethane ug/kg 29.8 M022.4 133 70-130ND
Vinyl acetate ug/kg 52.7J44.8 118 70-130ND
Vinyl chloride ug/kg 26.922.4 120 70-130ND
1,2-Dichloroethane-d4 (S)%116 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92232780039
1370687SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92232780039
1370687SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 3011.4J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92232780039
1370687SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg 27.5 R1623052.5
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%114 6112
4-Bromofluorobenzene (S)%93 493
Toluene-d8 (S)%99 1102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/32273
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92232897001, 92232897002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1369865
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 01/15/15 16:35
1,2-Dichlorobenzene ug/kg ND 330 01/15/15 16:35
1,3-Dichlorobenzene ug/kg ND 330 01/15/15 16:35
1,4-Dichlorobenzene ug/kg ND 330 01/15/15 16:35
1-Methylnaphthalene ug/kg ND 330 01/15/15 16:35
2,4,5-Trichlorophenol ug/kg ND 330 01/15/15 16:35
2,4,6-Trichlorophenol ug/kg ND 330 01/15/15 16:35
2,4-Dichlorophenol ug/kg ND 330 01/15/15 16:35
2,4-Dimethylphenol ug/kg ND 330 01/15/15 16:35
2,4-Dinitrophenol ug/kg ND 1650 01/15/15 16:35
2,4-Dinitrotoluene ug/kg ND 330 01/15/15 16:35
2,6-Dinitrotoluene ug/kg ND 330 01/15/15 16:35
2-Chloronaphthalene ug/kg ND 330 01/15/15 16:35
2-Chlorophenol ug/kg ND 330 01/15/15 16:35
2-Methylnaphthalene ug/kg ND 330 01/15/15 16:35
2-Methylphenol(o-Cresol)ug/kg ND 330 01/15/15 16:35
2-Nitroaniline ug/kg ND 1650 01/15/15 16:35
2-Nitrophenol ug/kg ND 330 01/15/15 16:35
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 01/15/15 16:35
3,3'-Dichlorobenzidine ug/kg ND 1650 01/15/15 16:35
3-Nitroaniline ug/kg ND 1650 01/15/15 16:35
4,6-Dinitro-2-methylphenol ug/kg ND 660 01/15/15 16:35
4-Bromophenylphenyl ether ug/kg ND 330 01/15/15 16:35
4-Chloro-3-methylphenol ug/kg ND 660 01/15/15 16:35
4-Chloroaniline ug/kg ND 1650 01/15/15 16:35
4-Chlorophenylphenyl ether ug/kg ND 330 01/15/15 16:35
4-Nitroaniline ug/kg ND 660 01/15/15 16:35
4-Nitrophenol ug/kg ND 1650 01/15/15 16:35
Acenaphthene ug/kg ND 330 01/15/15 16:35
Acenaphthylene ug/kg ND 330 01/15/15 16:35
Aniline ug/kg ND 330 01/15/15 16:35
Anthracene ug/kg ND 330 01/15/15 16:35
Benzo(a)anthracene ug/kg ND 330 01/15/15 16:35
Benzo(a)pyrene ug/kg ND 330 01/15/15 16:35
Benzo(b)fluoranthene ug/kg ND 330 01/15/15 16:35
Benzo(g,h,i)perylene ug/kg ND 330 01/15/15 16:35
Benzo(k)fluoranthene ug/kg ND 330 01/15/15 16:35
Benzoic Acid ug/kg ND 1650 01/15/15 16:35
Benzyl alcohol ug/kg ND 660 01/15/15 16:35
bis(2-Chloroethoxy)methane ug/kg ND 330 01/15/15 16:35
bis(2-Chloroethyl) ether ug/kg ND 330 01/15/15 16:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1369865
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 01/15/15 16:35
bis(2-Ethylhexyl)phthalate ug/kg ND 330 01/15/15 16:35
Butylbenzylphthalate ug/kg ND 330 01/15/15 16:35
Chrysene ug/kg ND 330 01/15/15 16:35
Di-n-butylphthalate ug/kg ND 330 01/15/15 16:35
Di-n-octylphthalate ug/kg ND 330 01/15/15 16:35
Dibenz(a,h)anthracene ug/kg ND 330 01/15/15 16:35
Dibenzofuran ug/kg ND 330 01/15/15 16:35
Diethylphthalate ug/kg ND 330 01/15/15 16:35
Dimethylphthalate ug/kg ND 330 01/15/15 16:35
Fluoranthene ug/kg ND 330 01/15/15 16:35
Fluorene ug/kg ND 330 01/15/15 16:35
Hexachloro-1,3-butadiene ug/kg ND 330 01/15/15 16:35
Hexachlorobenzene ug/kg ND 330 01/15/15 16:35
Hexachlorocyclopentadiene ug/kg ND 330 01/15/15 16:35
Hexachloroethane ug/kg ND 330 01/15/15 16:35
Indeno(1,2,3-cd)pyrene ug/kg ND 330 01/15/15 16:35
Isophorone ug/kg ND 330 01/15/15 16:35
N-Nitroso-di-n-propylamine ug/kg ND 330 01/15/15 16:35
N-Nitrosodimethylamine ug/kg ND 330 01/15/15 16:35
N-Nitrosodiphenylamine ug/kg ND 330 01/15/15 16:35
Naphthalene ug/kg ND 330 01/15/15 16:35
Nitrobenzene ug/kg ND 330 01/15/15 16:35
Pentachlorophenol ug/kg ND 1650 01/15/15 16:35
Phenanthrene ug/kg ND 330 01/15/15 16:35
Phenol ug/kg ND 330 01/15/15 16:35
Pyrene ug/kg ND 330 01/15/15 16:35
2,4,6-Tribromophenol (S)%44 27-110 01/15/15 16:35
2-Fluorobiphenyl (S)%47 30-110 01/15/15 16:35
2-Fluorophenol (S)%46 13-110 01/15/15 16:35
Nitrobenzene-d5 (S)%54 23-110 01/15/15 16:35
Phenol-d6 (S)%50 22-110 01/15/15 16:35
Terphenyl-d14 (S)%61 28-110 01/15/15 16:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369866LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11801670 71 36-120
1,2-Dichlorobenzene ug/kg 11101670 67 41-120
1,3-Dichlorobenzene ug/kg 1050 L016706366-120
1,4-Dichlorobenzene ug/kg 11101670 66 42-120
1-Methylnaphthalene ug/kg 12701670 76 40-120
2,4,5-Trichlorophenol ug/kg 12801670 77 37-120
2,4,6-Trichlorophenol ug/kg 12001670 72 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369866LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 12301670 74 33-120
2,4-Dimethylphenol ug/kg 13401670 81 36-120
2,4-Dinitrophenol ug/kg 59908330 72 22-121
2,4-Dinitrotoluene ug/kg 14401670 86 60-120
2,6-Dinitrotoluene ug/kg 14401670 86 54-120
2-Chloronaphthalene ug/kg 11201670 67 41-120
2-Chlorophenol ug/kg 12501670 75 39-120
2-Methylnaphthalene ug/kg 12601670 75 26-120
2-Methylphenol(o-Cresol)ug/kg 14001670 84 41-120
2-Nitroaniline ug/kg 28403330 85 45-120
2-Nitrophenol ug/kg 12901670 77 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 14101670 85 35-120
3,3'-Dichlorobenzidine ug/kg 26003330 78 16-125
3-Nitroaniline ug/kg 24103330 72 45-120
4,6-Dinitro-2-methylphenol ug/kg 25803330 77 46-120
4-Bromophenylphenyl ether ug/kg 12001670 72 36-120
4-Chloro-3-methylphenol ug/kg 28703330 86 37-120
4-Chloroaniline ug/kg 22903330 69 35-120
4-Chlorophenylphenyl ether ug/kg 12901670 78 30-120
4-Nitroaniline ug/kg 26103330 78 48-120
4-Nitrophenol ug/kg 85308330 102 43-120
Acenaphthene ug/kg 12901670 78 46-120
Acenaphthylene ug/kg 12301670 74 46-120
Aniline ug/kg 10501670 63 33-120
Anthracene ug/kg 12301670 74 63-120
Benzo(a)anthracene ug/kg 12901670 78 61-120
Benzo(a)pyrene ug/kg 12601670 76 59-120
Benzo(b)fluoranthene ug/kg 12401670 74 55-120
Benzo(g,h,i)perylene ug/kg 12201670 73 57-120
Benzo(k)fluoranthene ug/kg 11301670 68 56-120
Benzoic Acid ug/kg 55508330 67 13-120
Benzyl alcohol ug/kg 27403330 82 34-120
bis(2-Chloroethoxy)methane ug/kg 11601670 70 21-120
bis(2-Chloroethyl) ether ug/kg 12501670 75 25-120
bis(2-Chloroisopropyl) ether ug/kg 10201670 61 13-120
bis(2-Ethylhexyl)phthalate ug/kg 14201670 85 56-123
Butylbenzylphthalate ug/kg 14101670 84 57-120
Chrysene ug/kg 13001670 78 64-120
Di-n-butylphthalate ug/kg 13201670 79 58-120
Di-n-octylphthalate ug/kg 15301670 92 47-121
Dibenz(a,h)anthracene ug/kg 12501670 75 56-120
Dibenzofuran ug/kg 12301670 74 43-120
Diethylphthalate ug/kg 13601670 82 55-120
Dimethylphthalate ug/kg 13001670 78 54-120
Fluoranthene ug/kg 13101670 79 61-120
Fluorene ug/kg 13501670 81 51-120
Hexachloro-1,3-butadiene ug/kg 12401670 75 22-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1369866LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 11201670 67 53-120
Hexachlorocyclopentadiene ug/kg 8501670 51 18-150
Hexachloroethane ug/kg 11801670 71 39-120
Indeno(1,2,3-cd)pyrene ug/kg 12901670 78 58-120
Isophorone ug/kg 13101670 79 38-120
N-Nitroso-di-n-propylamine ug/kg 14801670 89 30-120
N-Nitrosodimethylamine ug/kg 11001670 66 32-120
N-Nitrosodiphenylamine ug/kg 12401670 74 50-120
Naphthalene ug/kg 11701670 70 38-120
Nitrobenzene ug/kg 12801670 77 37-120
Pentachlorophenol ug/kg 21903330 66 10-120
Phenanthrene ug/kg 11701670 70 62-120
Phenol ug/kg 11801670 71 37-120
Pyrene ug/kg 12901670 77 63-120
2,4,6-Tribromophenol (S)%75 27-110
2-Fluorobiphenyl (S)%70 30-110
2-Fluorophenol (S)%70 13-110
Nitrobenzene-d5 (S)%75 23-110
Phenol-d6 (S)%76 22-110
Terphenyl-d14 (S)%72 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/32295
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92232897001, 92232897002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1370617
Associated Lab Samples:92232897001, 92232897002
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N201/16/15 08:59
Aliphatic (C19-C36)mg/kg ND 10.0 N201/16/15 08:59
Aromatic (C11-C22)mg/kg ND 10.0 N201/16/15 08:59
2-Bromonaphthalene (S)%79 40-140 01/16/15 08:59
2-Fluorobiphenyl (S)%62 40-140 01/16/15 08:59
Nonatriacontane (S)%79 40-140 01/16/15 08:59
o-Terphenyl (S)%63 40-140 01/16/15 08:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1370618LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
1370619
Aliphatic (C09-C18)mg/kg ND N2106140-14059ND 50
Aliphatic (C19-C36)mg/kg ND N213.3 71 40-14066ND 50
Aromatic (C11-C22)mg/kg 18.2 N228.3 64 40-1407220.4 11 50
2-Bromonaphthalene (S)%77 40-14094
2-Fluorobiphenyl (S)%64 40-14083
Nonatriacontane (S)%78 40-14069
o-Terphenyl (S)%65 40-14070
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7415
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92232897001, 92232897002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92232794001
1369041SAMPLE DUPLICATE:
Percent Moisture %33.6 4 2535.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92232897002
1369042SAMPLE DUPLICATE:
Percent Moisture %23.8 7 2522.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
The lab does not hold TNI accreditation for this parameter.N2
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92232897
Johnson Grocery 71149156
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92232897001 OEXT/32295 GCSV/20088GP-6 (20-25)MADEP EPH MADEP EPH
92232897002 OEXT/32295 GCSV/20088GP-7 (20-25)MADEP EPH MADEP EPH
92232897001 GCV/8909 GCV/8912GP-6 (20-25)MADEP VPH MADEP VPH
92232897002 GCV/8909 GCV/8912GP-7 (20-25)MADEP VPH MADEP VPH
92232897001 OEXT/32273 MSSV/10195GP-6 (20-25)EPA 3546 EPA 8270
92232897002 OEXT/32273 MSSV/10195GP-7 (20-25)EPA 3546 EPA 8270
92232897001 MSV/29987GP-6 (20-25)EPA 8260
92232897002 MSV/29987GP-7 (20-25)EPA 8260
92232897001 PMST/7415GP-6 (20-25)ASTM D2974-87
92232897002 PMST/7415GP-7 (20-25)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 01/16/2015 05:34 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 30
Page 29 of 30
Page 30 of 30
APPENDIX D
BORING LOGS AND WELL CONSTRUCTION RECORDS
SOIL BORING LOG
PROJECT NAME: Johnson Grocery (Incident # 30594)SOIL BORING I.D.: MW-6
PROJECT NO.: 711479156 DATE(S) DRILLED: January 12, 2015
PROJECT LOCATION:5870 NC Highway 268 DRILLING CONTR.: Probe Technology
Greensboro, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2 inches
CLIENT: North Carolina Department of Environment and Natrual Resources SAMPLING METHOD/INTERVAL: 5-Foot
LOGGED BY: Alex Chinery REMARKS: BGS = below grade surface
DESCRIPTIVE LOG
SAMPLE SAMPLE BLOWS PID/FID DEPTH
INTERVAL REC. (IN.)PER 6"(ppm)(FT)DESCRIPTION OF SOIL
0-5 NA 0.4 0.0
1.0
2.0
3.0
4.0
5-10 NA 0.4 5.0
6.0
7.0
8.0
9.0
10-15 NA 3.7 10.0
11.0
12.0
13.0
14.0
15-20 NA 0.3 15.0
Odors 16.0
17.0
18.0
19.0
20-25 NA 28.9 20.0
Odors 21.0
22.0
23.0
24.0
25-30 NA -25.0
26.0
27.0
28.0
29.0
30.0
31.0
32.0
33.0
34.0
35.0
36.0
37.0
38.0
39.0
40.0
41.0
42.0
43.0
Odors
No
Light brown/tan sandy clay
No
No
Red/Brown sandy clay
Petroleum/Organic
No
Groundwater encountered
Petroleum/Organic
Dark brown sandy clay
Boring terminated at 35 feet
DRILLING METHODS
AR - AIR ROTARY SAMPLING METHODS
CFA - CONTINUOUS FLIGHT AUGER SS - SPLIT SPOONDC - DRIVEN CASING ST - SHELBY TUBEHA - HAND AUGER GP - GEOPROBE HSA -
HOLLOW STEM AUGERMD - MUD DRILLING * - Sample collected for analysisRC - ROCK CORING ND = <1 ppmWR - WATER ROTARY
SOIL BORING LOG
PROJECT NAME: Johnson Grocery (Incident # 30594)SOIL BORING I.D.: MW-7
PROJECT NO.: 711479156 DATE(S) DRILLED: January 12, 2015
PROJECT LOCATION:5870 NC Highway 268 DRILLING CONTR.: Probe Technology
Greensboro, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2 inches
CLIENT: North Carolina Department of Environment and Natrual Resources SAMPLING METHOD/INTERVAL: 5-Foot
LOGGED BY: Alex Chinery REMARKS: BGS = below grade surface
DESCRIPTIVE LOG
SAMPLE SAMPLE BLOWS PID/FID DEPTH
INTERVAL REC. (IN.)PER 6"(ppm)(FT)DESCRIPTION OF SOIL
0-5 NA 0.4 0.0
1.0
2.0
3.0
4.0
5-10 NA 0.4 5.0
6.0
7.0
8.0
9.0
10-15 NA 3.7 10.0
11.0
12.0
13.0
14.0
15-20 NA 0.3 15.0
16.0
17.0
18.0
19.0
20-25 NA 28.9 20.0
Odors 21.0
22.0
23.0
24.0
25-30 NA -25.0
26.0
27.0
28.0
29.0
30.0
31.0
32.0
33.0
34.0
35.0
36.0
37.0
38.0
39.0
40.0
41.0
42.0
43.0
Odors
No
Brown sandy clay
No
Red/Brown sand clay
No
No
Grey/Tan silty clay and Partially weathered rock (PWR)
Boring terminated at 35 feet
Petroleum/Organic
Dark grey/brown sandy clay
Groundwater encountered
No
DRILLING METHODS
AR - AIR ROTARY SAMPLING METHODS
CFA - CONTINUOUS FLIGHT AUGER SS - SPLIT SPOONDC - DRIVEN CASING ST - SHELBY TUBEHA - HAND AUGER GP - GEOPROBE HSA -
HOLLOW STEM AUGERMD - MUD DRILLING * - Sample collected for analysisRC - ROCK CORING ND = <1 ppmWR - WATER ROTARY
Resources ugust
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.
For multiple wells list all depths if different (example- 3@200’ and 2@100
If water level is above casing, use “+”
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.

_______________
Terry White, JR
3287-B
Terra Sonic International dba Probe Technology
✔
1/12/15 MW-6, MW-7
Piedmont Tobacco
5870 NC Hwy 268
Surry
36 20 33.84 80 39 24.53
✔
✔
2
35
28
8.5
auger
28 35 silty sand
0 20 2 Sch40 PVC
20 35 2 0.010 Sch40 PVC
0 16 neat cement pour
16 18 bentonite pour through augers
18 35 silica sand pour through augers
See consultants log
1/15/15Mike Tynan Digitally signed by Mike Tynan
DN: cn=Mike Tynan, o, ou,
email=[e-mail], c=US
Date: 2015.01.15 07:59:25 -05'00'