WS-1257_30594_CA_LAB_20140731

#=CL#
July 31, 2014
LIMS USE: FR - ALEX CHINERY
LIMS OBJECT ID: 92210650
92210650
Project:
Pace Project No.:
RE:
Alex Chinery
Terracon
2020E Starita Road
Charlotte, NC 28206
JOHNSON'S GROCERY
Dear Alex Chinery:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92210650001 MW-2 SM 6200B 63 PASI-CMCK
92210650002 MW-3 SM 6200B 63 PASI-CMCK
92210650003 MW-4 SM 6200B 63 PASI-CMCK
92210650004 WSW-1 SM 6200B 63 PASI-CMCK
92210650005 WSW-3 SM 6200B 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92210650001 MW-2
Benzene 67.4 ug/L 07/29/14 07:190.50SM 6200B
Ethylbenzene 73.4 ug/L 07/29/14 07:190.50SM 6200B
Isopropylbenzene (Cumene)8.6 ug/L 07/29/14 07:190.50SM 6200B
Methyl-tert-butyl ether 1.6 ug/L 07/29/14 07:190.50SM 6200B
Naphthalene 19.1 ug/L 07/29/14 07:192.0SM 6200B
n-Propylbenzene 22.2 ug/L 07/29/14 07:190.50SM 6200B
Toluene 550 ug/L 07/30/14 20:452.5SM 6200B
1,2,4-Trimethylbenzene 168 ug/L 07/29/14 07:190.50SM 6200B
1,3,5-Trimethylbenzene 60.5 ug/L 07/29/14 07:190.50SM 6200B
m&p-Xylene 251 ug/L 07/29/14 07:191.0SM 6200B
o-Xylene 114 ug/L 07/29/14 07:190.50SM 6200B
92210650003 MW-4
Benzene 46.4 ug/L 07/29/14 12:015.0SM 6200B
Ethylbenzene 72.8 ug/L 07/29/14 12:015.0SM 6200B
Isopropylbenzene (Cumene)31.6 ug/L 07/29/14 12:015.0SM 6200B
Naphthalene 27.8 ug/L 07/29/14 12:0120.0SM 6200B
n-Propylbenzene 115 ug/L 07/29/14 12:015.0SM 6200B
Toluene 142 ug/L 07/29/14 12:015.0SM 6200B
1,2,4-Trimethylbenzene 621 ug/L 07/29/14 12:015.0SM 6200B
1,3,5-Trimethylbenzene 253 ug/L 07/29/14 12:015.0SM 6200B
m&p-Xylene 286 ug/L 07/29/14 12:0110.0SM 6200B
o-Xylene 114 ug/L 07/29/14 12:015.0SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Method:
Client:Terracon
SM 6200B
Date:July 31, 2014
Description:6200B MSV
General Information:
5 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/27747
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92210819004
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 1251134)
• Dichlorodifluoromethane
• MSD (Lab ID: 1251135)
• Dichlorodifluoromethane
QC Batch: MSV/27748
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92210726007
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MSD (Lab ID: 1251621)
• Dichlorodifluoromethane
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Method:
Client:Terracon
SM 6200B
Date:July 31, 2014
Description:6200B MSV
Analyte Comments:
QC Batch: MSV/27748
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• MW-4 (Lab ID: 92210650003)
• 1,1-Dichloroethane
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-2 Lab ID:92210650001 Collected:07/24/14 13:10 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 67.4 ug/L 07/29/14 07:19 71-43-20.50 1
Bromobenzene ND ug/L 07/29/14 07:19 108-86-10.50 1
Bromochloromethane ND ug/L 07/29/14 07:19 74-97-50.50 1
Bromodichloromethane ND ug/L 07/29/14 07:19 75-27-40.50 1
Bromoform ND ug/L 07/29/14 07:19 75-25-20.50 1
Bromomethane ND ug/L 07/29/14 07:19 74-83-95.0 1
n-Butylbenzene ND ug/L 07/29/14 07:19 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/29/14 07:19 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/29/14 07:19 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/29/14 07:19 56-23-50.50 1
Chlorobenzene ND ug/L 07/29/14 07:19 108-90-70.50 1
Chloroethane ND ug/L 07/29/14 07:19 75-00-31.0 1
Chloroform ND ug/L 07/29/14 07:19 67-66-30.50 1
Chloromethane ND ug/L 07/29/14 07:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/29/14 07:19 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/29/14 07:19 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/29/14 07:19 96-12-81.0 1
Dibromochloromethane ND ug/L 07/29/14 07:19 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/29/14 07:19 106-93-40.50 1
Dibromomethane ND ug/L 07/29/14 07:19 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/29/14 07:19 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/29/14 07:19 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/29/14 07:19 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/29/14 07:19 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/29/14 07:19 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/29/14 07:19 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/29/14 07:19 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/29/14 07:19 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/29/14 07:19 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/29/14 07:19 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/29/14 07:19 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/29/14 07:19 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/29/14 07:19 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/29/14 07:19 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/29/14 07:19 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/29/14 07:19 108-20-30.50 1
Ethylbenzene 73.4 ug/L 07/29/14 07:19 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/29/14 07:19 87-68-32.0 1
Isopropylbenzene (Cumene)8.6 ug/L 07/29/14 07:19 98-82-80.50 1
Methylene Chloride ND ug/L 07/29/14 07:19 75-09-22.0 1
Methyl-tert-butyl ether 1.6 ug/L 07/29/14 07:19 1634-04-40.50 1
Naphthalene 19.1 ug/L 07/29/14 07:19 91-20-32.0 1
n-Propylbenzene 22.2 ug/L 07/29/14 07:19 103-65-10.50 1
Styrene ND ug/L 07/29/14 07:19 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/29/14 07:19 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/29/14 07:19 79-34-50.50 1
Tetrachloroethene ND ug/L 07/29/14 07:19 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-2 Lab ID:92210650001 Collected:07/24/14 13:10 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 550 ug/L 07/30/14 20:45 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 07/29/14 07:19 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/29/14 07:19 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/29/14 07:19 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/29/14 07:19 79-00-50.50 1
Trichloroethene ND ug/L 07/29/14 07:19 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/29/14 07:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/29/14 07:19 96-18-40.50 1
1,2,4-Trimethylbenzene 168 ug/L 07/29/14 07:19 95-63-60.50 1
1,3,5-Trimethylbenzene 60.5 ug/L 07/29/14 07:19 108-67-80.50 1
Vinyl chloride ND ug/L 07/29/14 07:19 75-01-41.0 1
m&p-Xylene 251 ug/L 07/29/14 07:19 179601-23-11.0 1
o-Xylene 114 ug/L 07/29/14 07:19 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %07/29/14 07:19 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %07/29/14 07:19 460-00-470-130 1
Toluene-d8 (S)100 %07/29/14 07:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-3 Lab ID:92210650002 Collected:07/24/14 10:55 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/29/14 13:08 71-43-20.50 1
Bromobenzene ND ug/L 07/29/14 13:08 108-86-10.50 1
Bromochloromethane ND ug/L 07/29/14 13:08 74-97-50.50 1
Bromodichloromethane ND ug/L 07/29/14 13:08 75-27-40.50 1
Bromoform ND ug/L 07/29/14 13:08 75-25-20.50 1
Bromomethane ND ug/L 07/29/14 13:08 74-83-95.0 1
n-Butylbenzene ND ug/L 07/29/14 13:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/29/14 13:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/29/14 13:08 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/29/14 13:08 56-23-50.50 1
Chlorobenzene ND ug/L 07/29/14 13:08 108-90-70.50 1
Chloroethane ND ug/L 07/29/14 13:08 75-00-31.0 1
Chloroform ND ug/L 07/29/14 13:08 67-66-30.50 1
Chloromethane ND ug/L 07/29/14 13:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/29/14 13:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/29/14 13:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/29/14 13:08 96-12-81.0 1
Dibromochloromethane ND ug/L 07/29/14 13:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/29/14 13:08 106-93-40.50 1
Dibromomethane ND ug/L 07/29/14 13:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/29/14 13:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/29/14 13:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/29/14 13:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/29/14 13:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/29/14 13:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/29/14 13:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/29/14 13:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/29/14 13:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/29/14 13:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/29/14 13:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/29/14 13:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/29/14 13:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/29/14 13:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/29/14 13:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/29/14 13:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/29/14 13:08 108-20-30.50 1
Ethylbenzene ND ug/L 07/29/14 13:08 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/29/14 13:08 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/29/14 13:08 98-82-80.50 1
Methylene Chloride ND ug/L 07/29/14 13:08 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/29/14 13:08 1634-04-40.50 1
Naphthalene ND ug/L 07/29/14 13:08 91-20-32.0 1
n-Propylbenzene ND ug/L 07/29/14 13:08 103-65-10.50 1
Styrene ND ug/L 07/29/14 13:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/29/14 13:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/29/14 13:08 79-34-50.50 1
Tetrachloroethene ND ug/L 07/29/14 13:08 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-3 Lab ID:92210650002 Collected:07/24/14 10:55 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/29/14 13:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/29/14 13:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/29/14 13:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/29/14 13:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/29/14 13:08 79-00-50.50 1
Trichloroethene ND ug/L 07/29/14 13:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/29/14 13:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/29/14 13:08 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/29/14 13:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/29/14 13:08 108-67-80.50 1
Vinyl chloride ND ug/L 07/29/14 13:08 75-01-41.0 1
m&p-Xylene ND ug/L 07/29/14 13:08 179601-23-11.0 1
o-Xylene ND ug/L 07/29/14 13:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %07/29/14 13:08 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %07/29/14 13:08 460-00-470-130 1
Toluene-d8 (S)99 %07/29/14 13:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-4 Lab ID:92210650003 Collected:07/24/14 11:40 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 46.4 ug/L 07/29/14 12:01 71-43-25.0 10
Bromobenzene ND ug/L 07/29/14 12:01 108-86-15.0 10
Bromochloromethane ND ug/L 07/29/14 12:01 74-97-55.0 10
Bromodichloromethane ND ug/L 07/29/14 12:01 75-27-45.0 10
Bromoform ND ug/L 07/29/14 12:01 75-25-25.0 10
Bromomethane ND ug/L 07/29/14 12:01 74-83-950.0 10
n-Butylbenzene ND ug/L 07/29/14 12:01 104-51-85.0 10
sec-Butylbenzene ND ug/L 07/29/14 12:01 135-98-85.0 10
tert-Butylbenzene ND ug/L 07/29/14 12:01 98-06-65.0 10
Carbon tetrachloride ND ug/L 07/29/14 12:01 56-23-55.0 10
Chlorobenzene ND ug/L 07/29/14 12:01 108-90-75.0 10
Chloroethane ND ug/L 07/29/14 12:01 75-00-310.0 10
Chloroform ND ug/L 07/29/14 12:01 67-66-35.0 10
Chloromethane ND ug/L 07/29/14 12:01 74-87-310.0 10
2-Chlorotoluene ND ug/L 07/29/14 12:01 95-49-85.0 10
4-Chlorotoluene ND ug/L 07/29/14 12:01 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 07/29/14 12:01 96-12-810.0 10
Dibromochloromethane ND ug/L 07/29/14 12:01 124-48-15.0 10
1,2-Dibromoethane (EDB)ND ug/L 07/29/14 12:01 106-93-45.0 10
Dibromomethane ND ug/L 07/29/14 12:01 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 07/29/14 12:01 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 07/29/14 12:01 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 07/29/14 12:01 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 07/29/14 12:01 75-71-85.0 10
1,1-Dichloroethane ND ug/L 07/29/14 12:01 75-34-3 D35.0 10
1,2-Dichloroethane ND ug/L 07/29/14 12:01 107-06-25.0 10
1,1-Dichloroethene ND ug/L 07/29/14 12:01 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 07/29/14 12:01 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 07/29/14 12:01 156-60-55.0 10
1,2-Dichloropropane ND ug/L 07/29/14 12:01 78-87-55.0 10
1,3-Dichloropropane ND ug/L 07/29/14 12:01 142-28-95.0 10
2,2-Dichloropropane ND ug/L 07/29/14 12:01 594-20-75.0 10
1,1-Dichloropropene ND ug/L 07/29/14 12:01 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 07/29/14 12:01 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 07/29/14 12:01 10061-02-65.0 10
Diisopropyl ether ND ug/L 07/29/14 12:01 108-20-35.0 10
Ethylbenzene 72.8 ug/L 07/29/14 12:01 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 07/29/14 12:01 87-68-320.0 10
Isopropylbenzene (Cumene)31.6 ug/L 07/29/14 12:01 98-82-85.0 10
Methylene Chloride ND ug/L 07/29/14 12:01 75-09-220.0 10
Methyl-tert-butyl ether ND ug/L 07/29/14 12:01 1634-04-45.0 10
Naphthalene 27.8 ug/L 07/29/14 12:01 91-20-320.0 10
n-Propylbenzene 115 ug/L 07/29/14 12:01 103-65-15.0 10
Styrene ND ug/L 07/29/14 12:01 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 07/29/14 12:01 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 07/29/14 12:01 79-34-55.0 10
Tetrachloroethene ND ug/L 07/29/14 12:01 127-18-45.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:MW-4 Lab ID:92210650003 Collected:07/24/14 11:40 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 142 ug/L 07/29/14 12:01 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 07/29/14 12:01 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 07/29/14 12:01 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 07/29/14 12:01 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 07/29/14 12:01 79-00-55.0 10
Trichloroethene ND ug/L 07/29/14 12:01 79-01-65.0 10
Trichlorofluoromethane ND ug/L 07/29/14 12:01 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 07/29/14 12:01 96-18-45.0 10
1,2,4-Trimethylbenzene 621 ug/L 07/29/14 12:01 95-63-65.0 10
1,3,5-Trimethylbenzene 253 ug/L 07/29/14 12:01 108-67-85.0 10
Vinyl chloride ND ug/L 07/29/14 12:01 75-01-410.0 10
m&p-Xylene 286 ug/L 07/29/14 12:01 179601-23-110.0 10
o-Xylene 114 ug/L 07/29/14 12:01 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S)102 %07/29/14 12:01 17060-07-070-130 10
4-Bromofluorobenzene (S)100 %07/29/14 12:01 460-00-470-130 10
Toluene-d8 (S)100 %07/29/14 12:01 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:WSW-1 Lab ID:92210650004 Collected:07/24/14 12:15 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/28/14 23:52 71-43-20.50 1
Bromobenzene ND ug/L 07/28/14 23:52 108-86-10.50 1
Bromochloromethane ND ug/L 07/28/14 23:52 74-97-50.50 1
Bromodichloromethane ND ug/L 07/28/14 23:52 75-27-40.50 1
Bromoform ND ug/L 07/28/14 23:52 75-25-20.50 1
Bromomethane ND ug/L 07/28/14 23:52 74-83-95.0 1
n-Butylbenzene ND ug/L 07/28/14 23:52 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/28/14 23:52 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/28/14 23:52 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/28/14 23:52 56-23-50.50 1
Chlorobenzene ND ug/L 07/28/14 23:52 108-90-70.50 1
Chloroethane ND ug/L 07/28/14 23:52 75-00-31.0 1
Chloroform ND ug/L 07/28/14 23:52 67-66-30.50 1
Chloromethane ND ug/L 07/28/14 23:52 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/28/14 23:52 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/28/14 23:52 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/28/14 23:52 96-12-81.0 1
Dibromochloromethane ND ug/L 07/28/14 23:52 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/28/14 23:52 106-93-40.50 1
Dibromomethane ND ug/L 07/28/14 23:52 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/28/14 23:52 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/28/14 23:52 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/28/14 23:52 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/28/14 23:52 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/28/14 23:52 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/28/14 23:52 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/28/14 23:52 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/28/14 23:52 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/28/14 23:52 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/28/14 23:52 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/28/14 23:52 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/28/14 23:52 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/28/14 23:52 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/28/14 23:52 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/28/14 23:52 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/28/14 23:52 108-20-30.50 1
Ethylbenzene ND ug/L 07/28/14 23:52 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/28/14 23:52 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/28/14 23:52 98-82-80.50 1
Methylene Chloride ND ug/L 07/28/14 23:52 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/28/14 23:52 1634-04-40.50 1
Naphthalene ND ug/L 07/28/14 23:52 91-20-32.0 1
n-Propylbenzene ND ug/L 07/28/14 23:52 103-65-10.50 1
Styrene ND ug/L 07/28/14 23:52 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/28/14 23:52 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/28/14 23:52 79-34-50.50 1
Tetrachloroethene ND ug/L 07/28/14 23:52 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:WSW-1 Lab ID:92210650004 Collected:07/24/14 12:15 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/28/14 23:52 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/28/14 23:52 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/28/14 23:52 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/28/14 23:52 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/28/14 23:52 79-00-50.50 1
Trichloroethene ND ug/L 07/28/14 23:52 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/28/14 23:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/28/14 23:52 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/28/14 23:52 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/28/14 23:52 108-67-80.50 1
Vinyl chloride ND ug/L 07/28/14 23:52 75-01-41.0 1
m&p-Xylene ND ug/L 07/28/14 23:52 179601-23-11.0 1
o-Xylene ND ug/L 07/28/14 23:52 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %07/28/14 23:52 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %07/28/14 23:52 460-00-470-130 1
Toluene-d8 (S)99 %07/28/14 23:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:WSW-3 Lab ID:92210650005 Collected:07/24/14 14:05 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 07/29/14 00:08 71-43-20.50 1
Bromobenzene ND ug/L 07/29/14 00:08 108-86-10.50 1
Bromochloromethane ND ug/L 07/29/14 00:08 74-97-50.50 1
Bromodichloromethane ND ug/L 07/29/14 00:08 75-27-40.50 1
Bromoform ND ug/L 07/29/14 00:08 75-25-20.50 1
Bromomethane ND ug/L 07/29/14 00:08 74-83-95.0 1
n-Butylbenzene ND ug/L 07/29/14 00:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 07/29/14 00:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 07/29/14 00:08 98-06-60.50 1
Carbon tetrachloride ND ug/L 07/29/14 00:08 56-23-50.50 1
Chlorobenzene ND ug/L 07/29/14 00:08 108-90-70.50 1
Chloroethane ND ug/L 07/29/14 00:08 75-00-31.0 1
Chloroform ND ug/L 07/29/14 00:08 67-66-30.50 1
Chloromethane ND ug/L 07/29/14 00:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/29/14 00:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 07/29/14 00:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 07/29/14 00:08 96-12-81.0 1
Dibromochloromethane ND ug/L 07/29/14 00:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 07/29/14 00:08 106-93-40.50 1
Dibromomethane ND ug/L 07/29/14 00:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 07/29/14 00:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 07/29/14 00:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 07/29/14 00:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 07/29/14 00:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 07/29/14 00:08 75-34-30.50 1
1,2-Dichloroethane ND ug/L 07/29/14 00:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 07/29/14 00:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 07/29/14 00:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 07/29/14 00:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 07/29/14 00:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 07/29/14 00:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 07/29/14 00:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 07/29/14 00:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 07/29/14 00:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 07/29/14 00:08 10061-02-60.50 1
Diisopropyl ether ND ug/L 07/29/14 00:08 108-20-30.50 1
Ethylbenzene ND ug/L 07/29/14 00:08 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 07/29/14 00:08 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 07/29/14 00:08 98-82-80.50 1
Methylene Chloride ND ug/L 07/29/14 00:08 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 07/29/14 00:08 1634-04-40.50 1
Naphthalene ND ug/L 07/29/14 00:08 91-20-32.0 1
n-Propylbenzene ND ug/L 07/29/14 00:08 103-65-10.50 1
Styrene ND ug/L 07/29/14 00:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 07/29/14 00:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 07/29/14 00:08 79-34-50.50 1
Tetrachloroethene ND ug/L 07/29/14 00:08 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Sample:WSW-3 Lab ID:92210650005 Collected:07/24/14 14:05 Received:07/24/14 15:58 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 07/29/14 00:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 07/29/14 00:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 07/29/14 00:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 07/29/14 00:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 07/29/14 00:08 79-00-50.50 1
Trichloroethene ND ug/L 07/29/14 00:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 07/29/14 00:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/29/14 00:08 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 07/29/14 00:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 07/29/14 00:08 108-67-80.50 1
Vinyl chloride ND ug/L 07/29/14 00:08 75-01-41.0 1
m&p-Xylene ND ug/L 07/29/14 00:08 179601-23-11.0 1
o-Xylene ND ug/L 07/29/14 00:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %07/29/14 00:08 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %07/29/14 00:08 460-00-470-130 1
Toluene-d8 (S)99 %07/29/14 00:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27747
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92210650004, 92210650005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1251132
Associated Lab Samples:92210650004, 92210650005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/28/14 23:35
1,1,1-Trichloroethane ug/L ND 0.50 07/28/14 23:35
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/28/14 23:35
1,1,2-Trichloroethane ug/L ND 0.50 07/28/14 23:35
1,1-Dichloroethane ug/L ND 0.50 07/28/14 23:35
1,1-Dichloroethene ug/L ND 0.50 07/28/14 23:35
1,1-Dichloropropene ug/L ND 0.50 07/28/14 23:35
1,2,3-Trichlorobenzene ug/L ND 2.0 07/28/14 23:35
1,2,3-Trichloropropane ug/L ND 0.50 07/28/14 23:35
1,2,4-Trichlorobenzene ug/L ND 2.0 07/28/14 23:35
1,2,4-Trimethylbenzene ug/L ND 0.50 07/28/14 23:35
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/28/14 23:35
1,2-Dibromoethane (EDB)ug/L ND 0.50 07/28/14 23:35
1,2-Dichlorobenzene ug/L ND 0.50 07/28/14 23:35
1,2-Dichloroethane ug/L ND 0.50 07/28/14 23:35
1,2-Dichloropropane ug/L ND 0.50 07/28/14 23:35
1,3,5-Trimethylbenzene ug/L ND 0.50 07/28/14 23:35
1,3-Dichlorobenzene ug/L ND 0.50 07/28/14 23:35
1,3-Dichloropropane ug/L ND 0.50 07/28/14 23:35
1,4-Dichlorobenzene ug/L ND 0.50 07/28/14 23:35
2,2-Dichloropropane ug/L ND 0.50 07/28/14 23:35
2-Chlorotoluene ug/L ND 0.50 07/28/14 23:35
4-Chlorotoluene ug/L ND 0.50 07/28/14 23:35
Benzene ug/L ND 0.50 07/28/14 23:35
Bromobenzene ug/L ND 0.50 07/28/14 23:35
Bromochloromethane ug/L ND 0.50 07/28/14 23:35
Bromodichloromethane ug/L ND 0.50 07/28/14 23:35
Bromoform ug/L ND 0.50 07/28/14 23:35
Bromomethane ug/L ND 5.0 07/28/14 23:35
Carbon tetrachloride ug/L ND 0.50 07/28/14 23:35
Chlorobenzene ug/L ND 0.50 07/28/14 23:35
Chloroethane ug/L ND 1.0 07/28/14 23:35
Chloroform ug/L ND 0.50 07/28/14 23:35
Chloromethane ug/L ND 1.0 07/28/14 23:35
cis-1,2-Dichloroethene ug/L ND 0.50 07/28/14 23:35
cis-1,3-Dichloropropene ug/L ND 0.50 07/28/14 23:35
Dibromochloromethane ug/L ND 0.50 07/28/14 23:35
Dibromomethane ug/L ND 0.50 07/28/14 23:35
Dichlorodifluoromethane ug/L ND 0.50 07/28/14 23:35
Diisopropyl ether ug/L ND 0.50 07/28/14 23:35
Ethylbenzene ug/L ND 0.50 07/28/14 23:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1251132
Associated Lab Samples:92210650004, 92210650005
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 07/28/14 23:35
Isopropylbenzene (Cumene)ug/L ND 0.50 07/28/14 23:35
m&p-Xylene ug/L ND 1.0 07/28/14 23:35
Methyl-tert-butyl ether ug/L ND 0.50 07/28/14 23:35
Methylene Chloride ug/L ND 2.0 07/28/14 23:35
n-Butylbenzene ug/L ND 0.50 07/28/14 23:35
n-Propylbenzene ug/L ND 0.50 07/28/14 23:35
Naphthalene ug/L ND 2.0 07/28/14 23:35
o-Xylene ug/L ND 0.50 07/28/14 23:35
sec-Butylbenzene ug/L ND 0.50 07/28/14 23:35
Styrene ug/L ND 0.50 07/28/14 23:35
tert-Butylbenzene ug/L ND 0.50 07/28/14 23:35
Tetrachloroethene ug/L ND 0.50 07/28/14 23:35
Toluene ug/L ND 0.50 07/28/14 23:35
trans-1,2-Dichloroethene ug/L ND 0.50 07/28/14 23:35
trans-1,3-Dichloropropene ug/L ND 0.50 07/28/14 23:35
Trichloroethene ug/L ND 0.50 07/28/14 23:35
Trichlorofluoromethane ug/L ND 1.0 07/28/14 23:35
Vinyl chloride ug/L ND 1.0 07/28/14 23:35
1,2-Dichloroethane-d4 (S)%101 70-130 07/28/14 23:35
4-Bromofluorobenzene (S)%101 70-130 07/28/14 23:35
Toluene-d8 (S)%99 70-130 07/28/14 23:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1251133LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 59.750 119 60-140
1,1,1-Trichloroethane ug/L 60.950 122 60-140
1,1,2,2-Tetrachloroethane ug/L 51.450 103 60-140
1,1,2-Trichloroethane ug/L 54.450 109 60-140
1,1-Dichloroethane ug/L 51.350 103 60-140
1,1-Dichloroethene ug/L 60.350 121 60-140
1,1-Dichloropropene ug/L 60.750 121 60-140
1,2,3-Trichlorobenzene ug/L 54.450 109 60-140
1,2,3-Trichloropropane ug/L 54.750 109 60-140
1,2,4-Trichlorobenzene ug/L 55.550 111 60-140
1,2,4-Trimethylbenzene ug/L 56.450 113 60-140
1,2-Dibromo-3-chloropropane ug/L 51.950 104 60-140
1,2-Dibromoethane (EDB)ug/L 55.650 111 60-140
1,2-Dichlorobenzene ug/L 53.750 107 60-140
1,2-Dichloroethane ug/L 55.250 110 60-140
1,2-Dichloropropane ug/L 51.050 102 60-140
1,3,5-Trimethylbenzene ug/L 55.850 112 60-140
1,3-Dichlorobenzene ug/L 53.650 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1251133LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 53.550 107 60-140
1,4-Dichlorobenzene ug/L 52.850 106 60-140
2,2-Dichloropropane ug/L 56.450 113 60-140
2-Chlorotoluene ug/L 53.050 106 60-140
4-Chlorotoluene ug/L 53.950 108 60-140
Benzene ug/L 52.350 105 60-140
Bromobenzene ug/L 52.650 105 60-140
Bromochloromethane ug/L 57.550 115 60-140
Bromodichloromethane ug/L 67.150 134 60-140
Bromoform ug/L 57.650 115 60-140
Bromomethane ug/L 41.450 83 60-140
Carbon tetrachloride ug/L 68.450 137 60-140
Chlorobenzene ug/L 53.350 107 60-140
Chloroethane ug/L 48.450 97 60-140
Chloroform ug/L 60.350 121 60-140
Chloromethane ug/L 49.850 100 60-140
cis-1,2-Dichloroethene ug/L 58.050 116 60-140
cis-1,3-Dichloropropene ug/L 52.950 106 60-140
Dibromochloromethane ug/L 62.050 124 60-140
Dibromomethane ug/L 58.450 117 60-140
Dichlorodifluoromethane ug/L 62.550 125 60-140
Diisopropyl ether ug/L 50.850 102 60-140
Ethylbenzene ug/L 53.650 107 60-140
Hexachloro-1,3-butadiene ug/L 55.650 111 60-140
Isopropylbenzene (Cumene)ug/L 59.550 119 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 53.650 107 60-140
Methylene Chloride ug/L 55.850 112 60-140
n-Butylbenzene ug/L 57.350 115 60-140
n-Propylbenzene ug/L 55.150 110 60-140
Naphthalene ug/L 55.550 111 60-140
o-Xylene ug/L 51.950 104 60-140
sec-Butylbenzene ug/L 57.250 114 60-140
Styrene ug/L 59.150 118 60-140
tert-Butylbenzene ug/L 57.850 116 60-140
Tetrachloroethene ug/L 57.850 116 60-140
Toluene ug/L 53.750 107 60-140
trans-1,2-Dichloroethene ug/L 57.650 115 60-140
trans-1,3-Dichloropropene ug/L 53.150 106 60-140
Trichloroethene ug/L 52.950 106 60-140
Trichlorofluoromethane ug/L 59.350 119 60-140
Vinyl chloride ug/L 53.950 108 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1251134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92210819004
1251135
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140117 320ND22.9 23.5
1,1,1-Trichloroethane ug/L 20 126 60-140124 120ND25.1 24.9
1,1,2,2-Tetrachloroethane ug/L 20 99 60-140107 820ND19.8 21.4
1,1,2-Trichloroethane ug/L 20 109 60-140114 520ND21.7 22.9
1,1-Dichloroethane ug/L 20 107 60-140109 220ND21.5 21.8
1,1-Dichloroethene ug/L 20 132 60-140129 220ND26.4 25.9
1,1-Dichloropropene ug/L 20 129 60-140126 220ND25.9 25.3
1,2,3-Trichlorobenzene ug/L 20 108 60-140111 220ND21.7 22.2
1,2,3-Trichloropropane ug/L 20 106 60-140112 520ND21.3 22.4
1,2,4-Trichlorobenzene ug/L 20 110 60-140112 220ND22.0 22.3
1,2,4-Trimethylbenzene ug/L 20 113 60-140116 220ND22.7 23.1
1,2-Dibromo-3-chloropropane ug/L 20 97 60-140104 720ND19.4 20.8
1,2-Dibromoethane (EDB)ug/L 20 109 60-140114 520ND21.7 22.8
1,2-Dichlorobenzene ug/L 20 109 60-140112 320ND21.7 22.4
1,2-Dichloroethane ug/L 20 111 60-140116 420ND22.2 23.2
1,2-Dichloropropane ug/L 20 103 60-140108 520ND20.7 21.6
1,3,5-Trimethylbenzene ug/L 20 112 60-140116 320ND22.5 23.2
1,3-Dichlorobenzene ug/L 20 108 60-140112 320ND21.7 22.3
1,3-Dichloropropane ug/L 20 104 60-140110 620ND20.8 22.0
1,4-Dichlorobenzene ug/L 20 108 60-140111 320ND21.5 22.2
2,2-Dichloropropane ug/L 20 107 60-140107 020ND21.4 21.4
2-Chlorotoluene ug/L 20 109 60-140114 420ND21.8 22.8
4-Chlorotoluene ug/L 20 109 60-140111 220ND21.8 22.2
Benzene ug/L 20 108 60-140112 320ND21.7 22.4
Bromobenzene ug/L 20 107 60-140110 320ND21.3 22.1
Bromochloromethane ug/L 20 118 60-140123 420ND23.6 24.7
Bromodichloromethane ug/L 20 128 60-140136 620ND25.6 27.3
Bromoform ug/L 20 107 60-140111 320ND21.4 22.1
Bromomethane ug/L 20 110 60-140110 020ND21.9 22.0
Carbon tetrachloride ug/L 20 139 60-140135 320ND27.8 27.0
Chlorobenzene ug/L 20 107 60-140111 320ND21.4 22.2
Chloroethane ug/L 20 109 60-140116 620ND21.8 23.2
Chloroform ug/L 20 126 60-140129 220ND25.2 25.7
Chloromethane ug/L 20 114 60-140115 020ND22.9 23.0
cis-1,2-Dichloroethene ug/L 20 121 60-140124 320ND24.1 24.9
cis-1,3-Dichloropropene ug/L 20 101 60-140106 420ND20.3 21.2
Dibromochloromethane ug/L 20 117 60-140122 420ND23.4 24.4
Dibromomethane ug/L 20 115 60-140119 420ND23.0 23.8
Dichlorodifluoromethane ug/L M02015460-140151 220ND30.9 30.1
Diisopropyl ether ug/L 20 102 60-140106 520ND20.3 21.3
Ethylbenzene ug/L 20 107 60-140110 320ND21.4 22.0
Hexachloro-1,3-butadiene ug/L 20 116 60-140115 120ND23.3 23.0
Isopropylbenzene (Cumene)ug/L 20 119 60-140121 120ND23.9 24.2
m&p-Xylene ug/L 40 102 60-140106 440ND40.9 42.4
Methyl-tert-butyl ether ug/L 20 106 60-140111 520ND21.1 22.2
Methylene Chloride ug/L 20 106 60-140110 320ND21.2 21.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1251134MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92210819004
1251135
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 117 60-140115 220ND23.4 23.0
n-Propylbenzene ug/L 20 114 60-140113 120ND22.8 22.6
Naphthalene ug/L 20 107 60-140113 520ND21.5 22.5
o-Xylene ug/L 20 103 60-140106 320ND20.6 21.2
sec-Butylbenzene ug/L 20 118 60-140116 220ND23.7 23.1
Styrene ug/L 20 114 60-140119 420ND22.8 23.7
tert-Butylbenzene ug/L 20 118 60-140118 020ND23.6 23.7
Tetrachloroethene ug/L 20 117 60-140115 120ND23.4 23.1
Toluene ug/L 20 111 60-140114 220ND22.2 22.7
trans-1,2-Dichloroethene ug/L 20 123 60-140123 020ND24.6 24.5
trans-1,3-Dichloropropene ug/L 20 101 60-140105 420ND20.3 21.1
Trichloroethene ug/L 20 111 60-140112 120ND22.1 22.4
Trichlorofluoromethane ug/L 20 134 60-140130 320ND26.9 26.0
Vinyl chloride ug/L 20 121 60-140118 320ND24.2 23.5
1,2-Dichloroethane-d4 (S)%102 70-130102
4-Bromofluorobenzene (S)%101 70-130103
Toluene-d8 (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/27748
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92210650001, 92210650002, 92210650003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1251156
Associated Lab Samples:92210650001, 92210650002, 92210650003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/29/14 07:02
1,1,1-Trichloroethane ug/L ND 0.50 07/29/14 07:02
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/29/14 07:02
1,1,2-Trichloroethane ug/L ND 0.50 07/29/14 07:02
1,1-Dichloroethane ug/L ND 0.50 07/29/14 07:02
1,1-Dichloroethene ug/L ND 0.50 07/29/14 07:02
1,1-Dichloropropene ug/L ND 0.50 07/29/14 07:02
1,2,3-Trichlorobenzene ug/L ND 2.0 07/29/14 07:02
1,2,3-Trichloropropane ug/L ND 0.50 07/29/14 07:02
1,2,4-Trichlorobenzene ug/L ND 2.0 07/29/14 07:02
1,2,4-Trimethylbenzene ug/L ND 0.50 07/29/14 07:02
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/29/14 07:02
1,2-Dibromoethane (EDB)ug/L ND 0.50 07/29/14 07:02
1,2-Dichlorobenzene ug/L ND 0.50 07/29/14 07:02
1,2-Dichloroethane ug/L ND 0.50 07/29/14 07:02
1,2-Dichloropropane ug/L ND 0.50 07/29/14 07:02
1,3,5-Trimethylbenzene ug/L ND 0.50 07/29/14 07:02
1,3-Dichlorobenzene ug/L ND 0.50 07/29/14 07:02
1,3-Dichloropropane ug/L ND 0.50 07/29/14 07:02
1,4-Dichlorobenzene ug/L ND 0.50 07/29/14 07:02
2,2-Dichloropropane ug/L ND 0.50 07/29/14 07:02
2-Chlorotoluene ug/L ND 0.50 07/29/14 07:02
4-Chlorotoluene ug/L ND 0.50 07/29/14 07:02
Benzene ug/L ND 0.50 07/29/14 07:02
Bromobenzene ug/L ND 0.50 07/29/14 07:02
Bromochloromethane ug/L ND 0.50 07/29/14 07:02
Bromodichloromethane ug/L ND 0.50 07/29/14 07:02
Bromoform ug/L ND 0.50 07/29/14 07:02
Bromomethane ug/L ND 5.0 07/29/14 07:02
Carbon tetrachloride ug/L ND 0.50 07/29/14 07:02
Chlorobenzene ug/L ND 0.50 07/29/14 07:02
Chloroethane ug/L ND 1.0 07/29/14 07:02
Chloroform ug/L ND 0.50 07/29/14 07:02
Chloromethane ug/L ND 1.0 07/29/14 07:02
cis-1,2-Dichloroethene ug/L ND 0.50 07/29/14 07:02
cis-1,3-Dichloropropene ug/L ND 0.50 07/29/14 07:02
Dibromochloromethane ug/L ND 0.50 07/29/14 07:02
Dibromomethane ug/L ND 0.50 07/29/14 07:02
Dichlorodifluoromethane ug/L ND 0.50 07/29/14 07:02
Diisopropyl ether ug/L ND 0.50 07/29/14 07:02
Ethylbenzene ug/L ND 0.50 07/29/14 07:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1251156
Associated Lab Samples:92210650001, 92210650002, 92210650003
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 07/29/14 07:02
Isopropylbenzene (Cumene)ug/L ND 0.50 07/29/14 07:02
m&p-Xylene ug/L ND 1.0 07/29/14 07:02
Methyl-tert-butyl ether ug/L ND 0.50 07/29/14 07:02
Methylene Chloride ug/L ND 2.0 07/29/14 07:02
n-Butylbenzene ug/L ND 0.50 07/29/14 07:02
n-Propylbenzene ug/L ND 0.50 07/29/14 07:02
Naphthalene ug/L ND 2.0 07/29/14 07:02
o-Xylene ug/L ND 0.50 07/29/14 07:02
sec-Butylbenzene ug/L ND 0.50 07/29/14 07:02
Styrene ug/L ND 0.50 07/29/14 07:02
tert-Butylbenzene ug/L ND 0.50 07/29/14 07:02
Tetrachloroethene ug/L ND 0.50 07/29/14 07:02
Toluene ug/L ND 0.50 07/29/14 07:02
trans-1,2-Dichloroethene ug/L ND 0.50 07/29/14 07:02
trans-1,3-Dichloropropene ug/L ND 0.50 07/29/14 07:02
Trichloroethene ug/L ND 0.50 07/29/14 07:02
Trichlorofluoromethane ug/L ND 1.0 07/29/14 07:02
Vinyl chloride ug/L ND 1.0 07/29/14 07:02
1,2-Dichloroethane-d4 (S)%102 70-130 07/29/14 07:02
4-Bromofluorobenzene (S)%100 70-130 07/29/14 07:02
Toluene-d8 (S)%99 70-130 07/29/14 07:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1251157LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 57.050 114 60-140
1,1,1-Trichloroethane ug/L 60.350 121 60-140
1,1,2,2-Tetrachloroethane ug/L 50.150 100 60-140
1,1,2-Trichloroethane ug/L 53.750 107 60-140
1,1-Dichloroethane ug/L 49.850 100 60-140
1,1-Dichloroethene ug/L 58.950 118 60-140
1,1-Dichloropropene ug/L 58.750 117 60-140
1,2,3-Trichlorobenzene ug/L 52.250 104 60-140
1,2,3-Trichloropropane ug/L 52.250 104 60-140
1,2,4-Trichlorobenzene ug/L 53.850 108 60-140
1,2,4-Trimethylbenzene ug/L 53.950 108 60-140
1,2-Dibromo-3-chloropropane ug/L 49.450 99 60-140
1,2-Dibromoethane (EDB)ug/L 53.950 108 60-140
1,2-Dichlorobenzene ug/L 51.350 103 60-140
1,2-Dichloroethane ug/L 54.550 109 60-140
1,2-Dichloropropane ug/L 50.250 100 60-140
1,3,5-Trimethylbenzene ug/L 53.250 106 60-140
1,3-Dichlorobenzene ug/L 51.350 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1251157LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.550 103 60-140
1,4-Dichlorobenzene ug/L 50.950 102 60-140
2,2-Dichloropropane ug/L 52.350 105 60-140
2-Chlorotoluene ug/L 52.150 104 60-140
4-Chlorotoluene ug/L 51.550 103 60-140
Benzene ug/L 51.150 102 60-140
Bromobenzene ug/L 50.350 101 60-140
Bromochloromethane ug/L 55.250 110 60-140
Bromodichloromethane ug/L 66.150 132 60-140
Bromoform ug/L 54.950 110 60-140
Bromomethane ug/L 45.550 91 60-140
Carbon tetrachloride ug/L 66.750 133 60-140
Chlorobenzene ug/L 51.050 102 60-140
Chloroethane ug/L 47.950 96 60-140
Chloroform ug/L 59.650 119 60-140
Chloromethane ug/L 50.250 100 60-140
cis-1,2-Dichloroethene ug/L 57.150 114 60-140
cis-1,3-Dichloropropene ug/L 51.550 103 60-140
Dibromochloromethane ug/L 59.550 119 60-140
Dibromomethane ug/L 56.450 113 60-140
Dichlorodifluoromethane ug/L 66.850 134 60-140
Diisopropyl ether ug/L 49.250 98 60-140
Ethylbenzene ug/L 50.750 101 60-140
Hexachloro-1,3-butadiene ug/L 52.850 106 60-140
Isopropylbenzene (Cumene)ug/L 56.550 113 60-140
m&p-Xylene ug/L 98.1100 98 60-140
Methyl-tert-butyl ether ug/L 51.750 103 60-140
Methylene Chloride ug/L 53.750 107 60-140
n-Butylbenzene ug/L 54.750 109 60-140
n-Propylbenzene ug/L 52.550 105 60-140
Naphthalene ug/L 53.450 107 60-140
o-Xylene ug/L 49.850 100 60-140
sec-Butylbenzene ug/L 54.050 108 60-140
Styrene ug/L 56.250 112 60-140
tert-Butylbenzene ug/L 55.150 110 60-140
Tetrachloroethene ug/L 54.650 109 60-140
Toluene ug/L 52.150 104 60-140
trans-1,2-Dichloroethene ug/L 56.050 112 60-140
trans-1,3-Dichloropropene ug/L 52.150 104 60-140
Trichloroethene ug/L 51.650 103 60-140
Trichlorofluoromethane ug/L 59.450 119 60-140
Vinyl chloride ug/L 53.550 107 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1251620MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92210726007
1251621
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 60-140117 920ND21.4 23.4
1,1,1-Trichloroethane ug/L 20 110 60-140123 1120ND22.0 24.5
1,1,2,2-Tetrachloroethane ug/L 20 98 60-140107 920ND19.6 21.4
1,1,2-Trichloroethane ug/L 20 106 60-140113 620ND21.3 22.6
1,1-Dichloroethane ug/L 20 99 60-140108 920ND19.8 21.6
1,1-Dichloroethene ug/L 20 109 60-140117 720ND21.9 23.5
1,1-Dichloropropene ug/L 20 116 60-140128 1020ND23.1 25.6
1,2,3-Trichlorobenzene ug/L 20 99 60-140111 1220ND19.8 22.2
1,2,3-Trichloropropane ug/L 20 102 60-140111 920ND20.3 22.1
1,2,4-Trichlorobenzene ug/L 20 102 60-140113 1020ND20.4 22.7
1,2,4-Trimethylbenzene ug/L 20 105 60-140116 1020ND21.0 23.2
1,2-Dibromo-3-chloropropane ug/L 20 94 60-140103 820ND18.9 20.5
1,2-Dibromoethane (EDB)ug/L 20 104 60-140112 820ND20.7 22.5
1,2-Dichlorobenzene ug/L 20 101 60-140111 920ND20.1 22.1
1,2-Dichloroethane ug/L 20 105 60-140112 720ND21.0 22.4
1,2-Dichloropropane ug/L 20 100 60-140110 1020ND19.9 22.1
1,3,5-Trimethylbenzene ug/L 20 104 60-140115 1020ND20.8 22.9
1,3-Dichlorobenzene ug/L 20 101 60-140112 1120ND20.1 22.4
1,3-Dichloropropane ug/L 20 101 60-140111 1020ND20.2 22.2
1,4-Dichlorobenzene ug/L 20 100 60-140111 1020ND20.1 22.2
2,2-Dichloropropane ug/L 20 113 60-140129 1320ND22.6 25.7
2-Chlorotoluene ug/L 20 101 60-140114 1220ND20.2 22.7
4-Chlorotoluene ug/L 20 101 60-140112 1020ND20.2 22.4
Benzene ug/L 20 102 60-140113 1020ND20.4 22.5
Bromobenzene ug/L 20 102 60-140110 820ND20.3 21.9
Bromochloromethane ug/L 20 113 60-140122 820ND22.6 24.5
Bromodichloromethane ug/L 20 122 60-140136 1120ND24.4 27.2
Bromoform ug/L 20 102 60-140114 1120ND20.4 22.7
Bromomethane ug/L 20 79 60-14094 1720ND15.9 18.8
Carbon tetrachloride ug/L 20 118 60-140138 1620ND23.6 27.6
Chlorobenzene ug/L 20 101 60-140111 1020ND20.1 22.3
Chloroethane ug/L 20 101 60-140108 620ND20.2 21.5
Chloroform ug/L 20 116 60-140129 1120ND23.2 25.8
Chloromethane ug/L 20 102 60-140111 920ND20.3 22.2
cis-1,2-Dichloroethene ug/L 20 115 60-140123 720ND22.9 24.6
cis-1,3-Dichloropropene ug/L 20 100 60-140112 1120ND19.9 22.3
Dibromochloromethane ug/L 20 110 60-140120 820ND22.1 24.0
Dibromomethane ug/L 20 109 60-140120 1020ND21.7 24.0
Dichlorodifluoromethane ug/L M02013060-140145 1020ND26.1 28.9
Diisopropyl ether ug/L 20 98 60-140106 820ND19.6 21.2
Ethylbenzene ug/L 20 99 60-140111 1120ND19.9 22.1
Hexachloro-1,3-butadiene ug/L 20 106 60-140115 820ND21.2 23.0
Isopropylbenzene (Cumene)ug/L 20 109 60-140122 1220ND21.7 24.4
m&p-Xylene ug/L 40 95 60-140106 1140ND38.0 42.5
Methyl-tert-butyl ether ug/L 20 101 60-140112 7208.9 29.1 31.3
Methylene Chloride ug/L 20 89 60-14097 820ND17.9 19.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1251620MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92210726007
1251621
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 108 60-140119 920ND21.6 23.7
n-Propylbenzene ug/L 20 104 60-140116 1120ND20.7 23.2
Naphthalene ug/L 20 100 60-140112 1120ND20.1 22.5
o-Xylene ug/L 20 95 60-140106 1120ND19.0 21.1
sec-Butylbenzene ug/L 20 106 60-140118 1020ND21.2 23.5
Styrene ug/L 20 108 60-140120 1020ND21.7 24.1
tert-Butylbenzene ug/L 20 105 60-140118 1120ND21.1 23.5
Tetrachloroethene ug/L 20 105 60-140117 1120ND20.9 23.4
Toluene ug/L 20 103 60-140115 1120ND20.6 23.1
trans-1,2-Dichloroethene ug/L 20 112 60-140122 920ND22.4 24.4
trans-1,3-Dichloropropene ug/L 20 98 60-140108 1020ND19.6 21.6
Trichloroethene ug/L 20 100 60-140111 1120ND20.0 22.2
Trichlorofluoromethane ug/L 20 112 60-140123 1020ND22.3 24.7
Vinyl chloride ug/L 20 108 60-140119 1020ND21.6 23.9
1,2-Dichloroethane-d4 (S)%101 70-13098
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92210650
JOHNSON'S GROCERY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92210650001 MSV/27748MW-2 SM 6200B
92210650002 MSV/27748MW-3 SM 6200B
92210650003 MSV/27748MW-4 SM 6200B
92210650004 MSV/27747WSW-1 SM 6200B
92210650005 MSV/27747WSW-3 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/31/2014 01:23 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 30
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