WA-27689_38813_CA_MRP_20230428

ENVIRONMENTAL | CIVIL | GEOTECHNICAL

MONITORING REPORT US 17 COUNTRY STORE 1383 US HIGHWAY 17 SOUTH ELIZABETH CITY, PASQUOTANK COUNTY, NC NCDEQ INCIDENT NO. 38813 RISK CLASSIFICATION: I140D

APRIL 28, 2023 NCDEQ CONTRACT NO. N122019D TASK AUTHORIZATION NO. 06 CATLIN PROJECT NO. 220209 PREPARED FOR: MR. HASSAN OSMAN NCDEQ, DWM, UST SECTION 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 PREPARED BY: CATLIN ENGINEERS AND SCIENTISTS 220 OLD DAIRY ROAD WILMINGTON, NC 28405 [phone]
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585
CORPORATE LICENSURE NO. FOR GEOLOGY SERVICES C-118

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023
TABLE OF CONTENTS
PAGE
1.0 SITE INFORMATION 1
2.0 EXECUTIVE SUMMARY 2
3.0 SCOPE OF SERVICES 2
4.0 SITE HISTORY AND CHARACTERIZATION 3
4.1 UST OWNER AND OPERATOR INFORMATION 3 4.2 UST INFORMATION 3 4.3 CONTAMINANT SOURCE INVENTORY 4 4.4 SITE CHARACTERISTICS 4 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE 4 4.6 RECEPTOR INFORMATION 5 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES 5
5.0 SITE GEOLOGY AND HYDROGEOLOGY 6
5.1 SOIL AND BEDROCK 6
5.2 HYDROGEOLOGY 7
6.0 SITE ASSESSMENT INFORMATION 7
6.1 MONITORING WELL INSTALLATION 8 6.2 GAUGING DATA 8 6.3 SAMPLING DATA 9 6.4 SUMMARY OF GROUNDWATER INFORMATION 9 6.5 EVALUATION OF ASSESSMENT INFORMATION 10
7.0 CONCLUSIONS AND RECOMMENDATIONS 11
8.0 LIMITATIONS 11
9.0 STATEMENTS AND CERTIFICATION 12
10.0 REFERENCES 12

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023
TABLES
TABLE 1 SITE HISTORY – UST AND OTHER RELEASE INFORMATION
TABLE 2 PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
TABLE 3 WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
TABLE 4 SUMMARY OF GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B
TABLE 5 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B
TABLE 6 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – EPA METHOD 625
TABLE 7 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – MADEP EPH/VPH
FIGURES
FIGURE 1 SITE VICINITY MAP
FIGURE 2 POTENTIAL RECEPTOR MAP
FIGURE 3 SITE MAP
FIGURE 4 GROUNDWATER ELEVATION – MARCH 29, 2023
FIGURE 5 MONITORING WELL GROUNDWATER SAMPLE ANALYTICAL RESULTS –
MARCH 29, 2023
APPENDICES APPENDIX A HISTORICAL DATA
APPENDIX B SITE PHOTOGRAPHS
APPENDIX C JOB HAZARD ANALYSES AND FIELD DATA SHEETS
APPENDIX D WELL LOG AND WELL CONSTRUCTION RECORD
APPENDIX E LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 1 April 2023
1.0 SITE INFORMATION
Site Identification
Date: 04/28/2023 Site Risk/Priority Rank: I140D
UST Number: WA-27689 Incident Number: 38813
Site Name: US 17 Country Store Facility ID: 00-01670
Site Location: 1383 US Hwy 17 S
Nearest City/Town: Elizabeth City County: Pasquotank
Description of Geographical Data Point: Former 10,000-gal diesel UST basin
Location Method: Google Earth
Latitude (decimal degrees): 36.259624 ° Longitude (decimal degrees): -76.302518°
Contacts Information
UST Owner: Hollowell Oil Company (Dissolved)
Address: N/A Phone: N/A
UST Operator: Hubert D. Ambrose (Deceased)
Address: N/A Phone: N/A
Property Owner: Ghanshyam R. Patel
Address: 109 Golf Club Dr., Elizabeth City, NC 27909 Phone: [phone]
Property Occupant: Unknown Resident/Renter
Address: 1382 US Hwy 17 S, Elizabeth City, NC 27909 Phone: N/A
Consultant: CATLIN Engineers and Scientists (CATLIN)
Address: 220 Old Dairy Rd., Wilmington, NC 28405 Phone: [phone]
Analytical Laboratory: Con-Test Analytical Laboratory State Certification: NC 652, NC-DW 25703
Address: 39 Spruce St., E. Longmeadow, MA 01028 Phone: [phone]
Release Information
Date Discovered: 08/13/2015
Estimated Quantity of Release: Unknown
Cause of Release: Leak in the UST system(s)
Source of Release: UST system or associated fitting(s)
Sizes and contents of UST system(s) from which the release occurred:
• One 10,000-gallon gasoline (UST 1)
• Two 10,000-gallon diesel (UST 4 & 6)
• One 6,000-gallon gasoline (UST 2)
• One 2,000-gallon kerosene (UST 3)
• One 2,000-gallon diesel (UST 5)
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CATLIN Project No. 220209 2 April 2023
2.0 EXECUTIVE SUMMARY The US 17 Country Store site is located at 1383 US Highway 17 South, Elizabeth
City, Pasquotank County, North Carolina. Six underground storage tanks (USTs)
historically operated at the site. One 2,000-gallon diesel UST was previously abandoned in place in 1996. One 6,000-gallon gasoline, one 10,000-gallon gasoline, two 10,000-gallon diesel, and one 2,000-gallon kerosene USTs were removed from the site in June 2022.
The purpose of this report is to document the latest well installation and groundwater
sampling activities. On March 21 and 22, 2023, CATLIN Engineers and Scientists (CATLIN) personnel advanced one boring to 30 feet below land surface (BLS) for the construction of a Type III monitoring well (TMW-01).
On March 29, 2023, CATLIN returned to the site for gauging and sampling activities.
Groundwater was measured at approximately two feet deep across the site. Light non-aqueous phase liquid (LNAPL; aka free-phase product) was not measured in any of the monitoring wells. Groundwater samples from five monitoring wells were collected and submitted for laboratory analysis of volatile organic compounds
(VOCs) per Standard Method (SM) 6200B plus ethylene dibromide (EDB), methyl
tert-butyl ether (MTBE), and diisopropyl ether (DIPE). Laboratory results did not indicate any dissolved petroleum constituents above the concentrations established in Title 15A of the North Carolina Administrative Code,
Subchapter 2L, Section .0202 Groundwater Quality Standards (2L GWQS) in the
samples from MW-02 and TMW-01. Multiple targeted analytes were reported in the MW-04 sample at concentrations above 2L GWQS, but below the Gross Contaminant Levels (GCL). Only benzene was above 2L GWQS in the MW-01 and MW-03 samples.
The VOC concentrations reported in the MW-01, MW-02, and MW-03 samples during this monitoring event are generally lower than those from the previous event (November 2022), while those in MW-04 have fluctuated.
CATLIN recommends to:
• Evaluate passive remedial and/or enhanced natural attenuation options.
• Continue period monitoring (sampling).
• Make additional efforts to obtain access and sample water supply well WSW-1. 3.0 SCOPE OF SERVICES
The scope of services for this report were performed in general accordance with CATLIN proposal number 220209.6P, dated January 24, 2023. Services were authorized by NCDEQ’s Task Authorization (TA) #06, dated January 25, 2023, and Contract Number N122019D.
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 3 April 2023
The approved scope of services for this Task Authorization included to:
• Install one Type III monitoring well and survey the top of casing (TOC)
elevation;
• Collect groundwater samples from five monitoring wells (MW-01 through MW-04 and TMW-01) and one water supply well (WSW-1)
• Analyze seven water samples (five monitoring wells, one water supply well, and one trip blank) per SM 6200B (plus EDB, MTBE, and DIPE); and
• Prepare and submit a monitoring report summarizing the findings.

Access was not granted for water supply well WSW-1; therefore, this well was not sampled. The remaining scope of services was conducted in general accordance with the approved TA.
4.0 SITE HISTORY AND CHARACTERIZATION
The US 17 Country Store site is located at 1383 US Highway 17 South, Elizabeth City, Pasquotank County, North Carolina (Figures 1 and 2). Summarized historical sampling and gauging data from previous consultants are provided in Appendix A.
Site photographs are presented in Appendix B.
4.1 UST OWNER AND OPERATOR INFORMATION Hollowell Oil Company owned the six USTs historically operated on-site. The
tanks were operated by Hubert Ambrose for petroleum retail sales. Hollowell
Oil Co. is dissolved (1993) and Hubert Ambrose is deceased (2018). The site was accepted into the North Carolina UST Section Trust Fund Branch State Lead Program in April 2020 (NCDEQ, 2020).
Available information regarding UST owners/operators is presented on
Table 1. 4.2 UST INFORMATION
Historically, one 2,000-gallon diesel UST operated on-site until April 1996.
Due to existing structures placed over top of the tank, it was abandoned in place by other parties in May 1996 (CE&S, 1996). A 10,000-gallon gasoline UST and 6,000-gallon gasoline UST were installed
in 1982, a 10,000-gallon diesel UST was installed in 1984, and a 2,000-
gallon kerosene UST and a 10,000-gallon diesel USTs were installed in 1988. These five USTs presumably operated until their temporary closure in 2008 (NCDEQ, 2020). These tanks were removed by CATLIN in June 2022 (CATLIN, 2022A).
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CATLIN Project No. 220209 4 April 2023
Available UST system information is presented in Table 1 and the approximate former UST system locations are illustrated on Figure 2.
4.3 CONTAMINANT SOURCE INVENTORY An on-site release was discovered in August 2015 during site assessment activities. Groundwater analytical results revealed multiple VOCs at
concentrations greater than their 2L GWQS and benzene up to 9,090
micrograms per liter (μg/L), which is above its GCL of 5,000 μg/L (ECES, 2015). 4.4 SITE CHARACTERISTICS

The site previously operated as a country store and retail gas station. The property was passed to Hubert Ambrose’s heirs in 2018 (NCDEQ, 2020). Currently, the property is owned by Ghanshyam Patel and occupied by Automotive Solutions (a vehicle repair service).

The parcel has three structures: the former store building, a repair garage (Automotive Solutions), and a small vacant building located on the northeast portion of the property. During recent site activities, it appeared that the former store was in the process of being remodeled and there was a
residential dwelling upstairs. The terrain includes concrete, gravel parking
surfaces, and grassy areas. The open, parking area is leased to commercial truck drivers for parking their personal vehicles and semi-trucks. During recent site activities, a number of the monitoring well concrete pads
were found to be damaged. The damaged concrete pads were removed and
replaced with larger and thicker concrete pads. Site photographs are presented in Appendix B. 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES
AND LAND USE
Properties in the site vicinity are mostly businesses and agricultural land. The site is bound by US Highway 17 South to the west and Simpson Ditch Road to the north. A gas station (Exxon) and convenience store are located to the
north (across Simpson Ditch Road). The adjoining property to the east is
owned by the Freeway Tabernacle Church and the property to the south is a business (B&S Enterprises, Inc.). Agricultural land is located to the north and west (across US Highway 17 South).
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 5 April 2023
4.6 RECEPTOR INFORMATION CATLIN conducted the most recent receptor survey for the US 17 Country
Store site in November 2022. Potential receptors located within 1,500 feet of
the subject site are illustrated on Figure 2 and pertinent receptor information from CATLIN (2022B) is described below and presented on Table 2. Based on utility data obtained from the Pasquotank County GIS map, public
water is available to properties within 1,500 feet of the site. One non-potable
well is located approximately 300 feet northwest from the source area, in an agricultural field across US Highway 17. The well appears to be used for irrigation; however, there is a spigot and hose at the well. There is concern that seasonal farm workers may drink water from the well.

A drainage ditch is located approximately 395 feet northwest of the site. No perennial surface water bodies were identified within 1,500 feet of the site; the nearest one is an unnamed tributary of the Little River, located 4,260 feet northwest of the site.
4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES In April 1996, Coastal Engineers & Surveying (CE&S) conducted groundwater sampling in the vicinity of a 2,000-gallon diesel UST. A
temporary monitoring well was installed near the tank and groundwater
samples were collected for analysis per Environmental Protection Agency (EPA) Method 602/625. No analytes were reported above the laboratory detection limits. The UST was abandoned in place in May 1996 by Roger Turner & Sons, Inc. (CE&S, 1996).

In August 2015, Eastern Carolina Environmental Services, Inc. (ECES) conducted a groundwater investigation and receptor survey. No water supply wells or surface water bodies were identified within 1,000 feet of the site. Eight temporary monitoring wells were installed and groundwater samples
were collected for analysis per SM 6200B. Laboratory analytical results
revealed multiple analytes above their 2L GWQS in all samples, and benzene exceeding its GCL. Based on these results, an intermediate risk classification was assigned (ECES, 2015).
On behalf of NCDEQ, CATLIN conducted soil sampling activities in June
2021. Fourteen soil borings (SB-01 through SB-14) were advanced via direct push technology (DPT) in the vicinity of the remaining USTs. Soil samples were collected from each at approximately four feet BLS for waste characterization and analysis for total petroleum hydrocarbons (TPH)
gasoline range organics (GRO) and diesel range organics (DRO) per
ultraviolet florescence (UVF) methods. Laboratory analytical results indicated TPH GRO and/or DRO concentrations above State Action Levels in multiple
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CATLIN Project No. 220209 6 April 2023
samples, up to 3,774 milligrams per kilogram (mg/kg) TPH GRO and 20,678 mg/kg TPH DRO. However, the samples collected in the vicinity of the southern gasoline UST (UST 1) were below State Action Levels (CATLIN,
2021).
CATLIN conducted UST closure activities in June 2022. The five remaining USTs (Tanks 1 through 4 and Tank 6) were closed by removal. A total of 450.41 tons of contaminated soil were excavated and disposed. Groundwater
was encountered during the excavation activities and a LNAPL sheen was
observed. Approximately 625 gallons of non-hazardous fluids were pumped from the tanks. No soil or groundwater samples were collected due to the prior soil assessment and waste characterization analyses (CATLIN, 2022A).
A Limited Site Assessment (LSA) was performed by CATLIN in October and
November 2022. Four Type II monitoring wells (MW-01 through MW-04) were installed. Groundwater samples were collected from the monitoring wells and analyzed for VOCs via SM 6200B (including EDB, MTBE, and DIPE), semi-VOCs via EPA Method 625, and extractable petroleum
hydrocarbons (EPH)/volatile petroleum hydrocarbons (VPH) via
Massachusetts Department of Environmental Protection (MADEP) methods. Benzene was reported above 2L GWQS in all four monitoring well samples. Multiple semi-VOCs and MADEP analytical fractions were reported in the MW-02, MW-03, and MW-04 samples above 2L GWQS. However, no
contaminants were above GCL. One water supply well (WSW-1) that
appeared to be used for watering crops was identified approximately 300 feet northwest of the site, and a drainage ditch runs along the northwest site boundary (CATLIN, 2022B).
Portions of summarized historical sampling data from previous consultants
are provided in Appendix A. 5.0 SITE GEOLOGY AND HYDROGEOLOGY
5.1 SOIL AND BEDROCK As defined in the Geologic Map of North Carolina, published by the North Carolina Department of Natural Resources and Community Development (1985), the site lies within the Coastal Plain physiographic province.
Two natural subdivisions of the Coastal Plain were described by Stuckey (1965): the Tidewater region and the Tidewater. The project area is located within the Inner Coastal Plain, which is an area of constructional topography (Horton and Zullo, 1991).

The Coastal Plain comprises a wedge-shaped sequence of stratified marine and non-marine sedimentary rocks deposited on crystalline basement. The
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 7 April 2023
sedimentary sequences range in age from Recent to lower Cretaceous (Narkunas, 1980).
The site is underlain by undivided surficial deposits within the Coastal Plain.
According to the 1985 Geologic Map of North Carolina, sand, clay, gravel, and peat are exposed in the site area. According to monitoring well boring logs from CATLIN (2022B), tan, clayey
sand underlies the site to approximately three feet BLS. Sandy clay and/or
clayey sand was encountered from three to eight feet BLS. Gray sand was observed up to 30 feet BLS during the installation of TMW-01 during this event.
5.2 HYDROGEOLOGY
Groundwater – The Coastal Plain groundwater system consists of aquifers comprised of permeable sands, gravels, and limestones separated by confining units of less permeable sediment. According to Winner, Jr. and
Coble (1989), the surficial aquifer consists primarily of fine sands, clays,
shells, peat beds, and scattered deposits of coarse-grained material in the form of relic beach ridges and floodplain alluvium. The areal extent of the surficial aquifer in the Coastal Plain is approximately 25,000 square miles with an average thickness of 35 feet. The average estimated hydraulic
conductivity is 29 feet per day (Winner, Jr. and Coble, 1989).
The 2020 VHF identified three boreholes near the site to draw a cross-section: Elizabeth City RO Test, E 11I; PA-T2-62, F 10Q; and DWR Perquimans Test, F 13W. According to the VHF, the surficial aquifer extends
to approximately 260 feet BLS. The Yorktown confining unit (approximately
10 feet thick) and associated aquifer are projected to underlie the surficial aquifer to 470 feet BLS. The Castle Hayne, Beaufort, Upper Cape Fear, and Lower Cape Fear aquifers are modeled to be present at further depths.
Surface Water – A drainage ditch is located approximately 395 feet northwest
of the site. No perennial surface water bodies were identified within 1,500 feet of the site. 6.0 SITE ASSESSMENT INFORMATION

Field activities included installing one Type III monitoring well (TMW-01) and obtaining groundwater samples from five monitoring wells (MW-01 through MW-04 and TMW-01) and attempt to obtain an access agreement for sampling one water supply well (WSW-1). CATLIN conducted field activities on in general accordance
with the approved TA and pre-prepared Health and Safety Plan (HASP). Daily safety
briefings detailing hazards identified in the task specific job hazard analysis (JHA)
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CATLIN Project No. 220209 8 April 2023
sheets were conducted prior to initiating field work. The JHAs and field data sheets are included in Appendix C.
6.1 MONITORING WELL INSTALLATION
On March 21 and 22, 2023, one boring was advanced to 30 feet BLS for monitoring well construction by a North Carolina Certified Well Contractor, utilizing hollow stem augers and mud rotary tooling with a Diedrich D-50 drill
rig. Cuttings generated during drilling activities were spread on-site.
The well (TMW-01) was constructed of new, threaded PVC casing and screen. No glues or cements were used in joining PVC components. New nitrile gloves were worn while handling all well materials. The monitoring well
was constructed with a pointed PVC sediment trap, five feet of 2-inch
diameter, 0.010-inch slotted PVC well screen, 25 feet of 2-inch diameter inner casing PVC, and 20 feet of 4-inch diameter outer casing PVC to the surface. The annular space was filled with coarse sand packed to approximately three feet above the well screen and bentonite chips were
packed to within 20 feet of the ground surface. The bentonite chips were
poured from the surface while simultaneously pouring water to facilitate hydration. The remaining 20 feet was filled with Portland cement poured from the surface.
The well was finished with a concrete pad and flush-mount steel wellhead
and locking well cap. After installation, the monitoring well was developed by over-pumping. The TOC elevation was measured using traditional survey methods (Rod and Level). The survey forms are included in Appendix C.
Monitoring well construction information is summarized on Table 3 and a site
map with monitoring well locations are illustrated on Figure 3. Site photographs are presented in Appendix B. The well log and Well Construction Record were submitted to NCDEQ on April 4, 2023; copies are provided in Appendix D.
6.2 GAUGING DATA During the March 2023 event, CATLIN personnel measured depth to water in five monitoring wells using an electronic water interface probe. To prevent
cross contamination, the probe and cabling were decontaminated according
to manufacturer’s recommendations between use in each well. Gauging data were recorded on an electronic groundwater sampling form using a tablet device. Gauging procedures were performed in general accordance with North Carolina Department of Environmental and Natural Resources
(NCDENR) and NCDEQ Guidelines, and EPA Region 4 Operating Procedures.
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CATLIN Project No. 220209 9 April 2023
Depth to water ranged from 0.99 feet below top of casing (BTOC) (MW-01) to 2.77 feet BTOC (MW-04) in the Type II wells. Depth to water in Type III well TMW-01 was 2.98 feet BTOC. The depths to water in MW-01, MW-03, MW-04, and TMW-01 were above their respective screen intervals. LNAPL
was not encountered during this monitoring event. Based on groundwater
elevations calculated for this monitoring period, groundwater flow direction is towards the west.
Monitoring well gauging results for events conducted by CATLIN are
presented in Table 3. Groundwater elevations and flow direction are
illustrated on Figure 4. Groundwater sampling forms with gauging data are provided in Appendix C.
6.3 SAMPLING DATA
Following gauging, the wells were sampled in general accordance with NCDEQ Guidelines and EPA Region 4 Operating Procedures. Prior to obtaining a representative groundwater sample, each monitoring well was purged by removing a minimum of three well volumes using a new,
disposable bailer. Groundwater field parameter data were measured at one-minute intervals using an In-Situ Aqua TROLL 600 Multiparameter Sonde (Aqua TROLL). Conductivity, pH, oxidation reduction potential (ORP), dissolved oxygen, and temperature measurements were recorded utilizing the VuSitu mobile application (version 1.17.12). The Aqua TROLL was
decontaminated according to manufacturer’s recommendations and rinsed with distilled water between use at each monitoring well. Groundwater parameter data were transferred from the VuSitu mobile application to the electronic groundwater sampling forms. Copies of the groundwater sampling forms are available in Appendix C.
Once a minimum of three well volumes were removed (or the well was bailed dry), groundwater samples were collected from the bailers and poured into appropriate, laboratory-provided, pre-preserved glassware, labeled, and placed on ice in an insulated cooler.
The groundwater samples and laboratory-provided trip blank were submitted to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC) protocol and analyzed per SM 6200B (including EDB, MTBE, and DIPE). The
laboratory analytical data and COC are included in Appendix E.
6.4 SUMMARY OF GROUNDWATER INFORMATION
The latest groundwater sampling laboratory results for SM 6200B analysis
are summarized in Table 4 and illustrated on Figure 5. Historical results for
events conducted by CATLIN are in Tables 6 and 7. A copy of the complete laboratory report and COC documentation are in Appendix E.
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 10 April 2023
Monitoring Wells
During the March 2023 sampling event, five monitoring well groundwater samples (MW-01 through MW-04 and TMW-01) were collected and
submitted for analysis via SM 6200B (including EDB, MTBE, and DIPE. No
analyte concentrations were detected above GCL in any of the monitoring well samples. Analytical results reported the following VOCs at concentrations above their 2L GWQS in the MW-01, MW-03, and MW-04 samples:
•MW-01 and MW-03: benzene; and
•MW-04: benzene, isopropylbenzene, MTBE, naphthalene, and n-propylbenzene.
Water Supply Well
A groundwater sample was not obtained from water supply well WSW-1. The property owner could not be reached through mail, and no one was present on site at the time of sampling activities.
Trip Blank
A laboratory-provided trip blank was submitted for analysis per SM 6200B. No targeted analytes were detected in the trip blank sample.
6.5 EVALUATION OF ASSESSMENT INFORMATION
Extent of Contamination
Benzene was above its 2L GWQS in the samples from MW-01 and MW-03. Multiple petroleum constituents were detected above their respective 2L GWQS in the sample from MW-04. However, no constituents were reported above GCL. A summary of monitoring well groundwater sample analytical results are illustrated on Figure 5. The dissolved phase contaminant plume is
horizontally delineated to the south and is vertically delineated.
The highest contaminant concentrations have historically been reported in samples from MW-03 and MW-04. The concentrations in samples obtained from MW-01, MW-02, and MW-03 appear to be decreasing in relation to the
concentrations historically reported, while those in MW-04 have fluctuated.
Cleanup Levels Achieved
Soil – Approximately 450.41 of impacted soil have been removed from the
site (CATLIN, 2022A). Soil samples obtained in 2021 indicate that TPH concentrations are above State Action Levels, up to 3,774 mg/kg TPH GRO and 20,678 mg/kg TPH DRO (CATLIN, 2021).
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 11 April 2023
Groundwater – Groundwater contaminant concentrations are above 2L GWQS, but below GCL at the site.
LNAPL – LNAPL was not measured during this monitoring period. LNAPL
has never been detected at the site.
7.0 CONCLUSIONS AND RECOMMENDATIONS
Conclusions
Groundwater monitoring findings for this period are summarized below:
•One Type III monitoring well (TMW-01) was installed to 30 feet BLS.
•Damaged concrete well pads were removed and replaced.
•Groundwater samples were collected from MW-01 through MW-04 andTMW-01 and analyzed per SM 6200B (including EDB, MTBE, and DIPE).
•Access was not granted to sample water supply well WSW-1.
•Multiple contaminants were detected in the MW-04 sample at concentrationsabove their 2L GWQS.
•Only benzene was above its 2L GWQS in the MW-01 and MW-03 samples.
•No constituents were reported above their respective GCL.
Recommendations
CATLIN recommends to:
•Evaluate passive remedial and/or enhanced natural attenuation options.
•Continue period monitoring (sampling).
•Make additional efforts to obtain access and sample water supply wellWSW-1.
8.0 LIMITATIONS
The soil and groundwater samples analyzed as part of this investigation only provide isolated data points and may not represent conditions at every location in the project area. Analyses and conclusions of this report, being based on interpolation of data
points at the project area, may not be completely representative of all site
conditions. Conclusions and recommendations of this investigation and report are based on the best available data in an effort to comply with current regulatory requirements.
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CATLIN Project No. 220209 12 April 2023
9.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. April 28, 2023
Will this report be submitted after the established due date? NO
2 Was any required information from the above template missing from this report? YES
No cross sections are provided
3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? NA
No CAP has been submitted for this site.
4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? NO
6 Certification:
I, Benjamin J. Ashba, a Licensed Geologist for CATLIN Engineers and Scientists, do certify that the information contained in this report is correct and accurate to the best of my knowledge.
CATLIN Engineers and Scientists is licensed to practice geology in North Carolina. The certification number of the company or corporation is C-118.
10.0 REFERENCES
CATLIN Engineers and Scientists, Letter Report, US 17 Country Store, 851 Halls
Creek Road, Elizabeth City, NC 27909, Incident Number: 38813, Risk
Classification: I140D, July 30, 2021.
CATLIN Engineers and Scientists, UST Closure Report, US 17 Country Store, 1383
US Highway 17 South, Elizabeth City, Pasquotank County, North Carolina,
NCDEQ Incident No: 38813, Risk Classification: I140D, July 20, 2022(A).
CATLIN Engineers and Scientists, Limited Site Assessment Report, US 17 Country
Store, 1383 US Highway 17 South, Elizabeth City, Pasquotank County, North Carolina, NCDEQ Incident No: 38813, Risk Classification: I140D, December
22, 2022(B).
Coastal Engineering and Surveying, Re: Country Store, Hwy 17 South, Elizabeth
City, UST Closure File 2099-Posquotank, June 21, 1996.
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CATLIN Project No. 220209 13 April 2023
County of Pasquotank, North Carolina, Zoning Ordinance, June 12, 2021.
Eastern Carolina Environmental Services, Inc., Ground-Water Investigation and Receptor Survey, Hubert Ambrose Property – 1383 US Highway 17 South,
Elizabeth City, Pasquotank County, North Carolina, August 25, 2015.
Horton, J. Wright and Zullo, Vicor A., The Geology of the Carolinas, 1991.
Narkunas, James, Groundwater Evaluation in the Central Coastal Plain of North
Carolina, January 1, 1980.
NCDENR, UST Section, North Carolina Department of Environmental Quality,
Division of Environmental Management, Underground Storage Tank Closure
Report, July 26, 1996.
NCDENR, UST Section, North Carolina Department of Environmental Quality, Division of Environmental Management, UST-3 Form, Notice of Intent: UST Permanent Closure or Change-in-Service, May 15, 1996.
NCDENR, UST Section, North Carolina Department of Environmental Quality,
Division of Environmental Management, UST-2 Form, Site Investigation
Report for Permanent Closure or Change-in-Service of UST, June 24, 1996.
NCDEQ, Division of Water Resources, 2020 Visual Hydrogeologic Framework, North Carolina Hydrogeological Database, ncwater.org/?page=350,
accessed November 15, 2022.
NCDEQ, Division of Waste Management, Document Management System (Laserfiche), Miscellaneous (documents associated with Incident No. 18221), accessed November 2020-April 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality,
Division of Waste Management, Guidelines for Sampling, UST Section, North
Carolina Department of Environment and Natural Resources, December 1, 2013.
NCDEQ, UST Section, North Carolina Department of Environment Quality, Division of Waste Management, Guidelines for Site Checks, Tank Closure, and Initial
Response and Abatement for Petroleum and Hazardous Substance UST
Releases, Petroleum Non-UST Releases, January 19, 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, UST Section Assessment Guidelines, Petroleum and Hazardous Substance UST Releases, Petroleum Non-UST
Releases, January 19, 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Memorandum, Recommendation for State
Lead Cleanup, Incident Name: US 17 Country Store, Incident# (UST#): 38813 (WA-27689), March 30, 2020.
NCDEQ, UST Section, North Carolina Department of Environmental Quality,
Division of Waste Management, State Lead Acceptance, US 17 Country
Store, 1383 US Hwy 17 South, Elizabeth City, Pasquotank County, North
Carolina, Incident Numbers: 38813, Risk Classification: Intermediate, September 8, 2020.
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 14 April 2023
Rhodes, Thomas S., and Conrad, Stephen G., 1985, Geologic Map of North Carolina: Department of Natural Resources and Community Development, Division of Land Resources, and the NC Geological Survey, compiled by
Brown, Philip M., et al, and Parker, John M. III, and in association with the
State Geologic Map Advisory Committee, scale 1:500,000.
Pasquotank County, North Carolina, https://www.pasquotankcountync.org/, December 2022.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and
Ecosystem Support Division, Athens Georgia, Guidance – Design and
Installation of Monitoring Wells, Striggow, B., US. EPA Report No. SESGUID-101-R0, Effective Date February 18, 2008.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Field
Equipment Cleaning and Decontamination at the FEC, Striggow, B., U.S.
EPA Report No. SESDPROC-206-R3, Effective Date December 18, 2015.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – Groundwater Level and Well Depth Measurement, Striggow, B., U.S. EPA
Report No. SESDPROC-105-R3, Effective Date November 3, 2016.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure –
Groundwater Sampling, Striggow, B., U.S. EPA Report No. SESDPROC-301-R4, Effective Date April 26, 2017.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – In Situ
Water Quality Monitoring, Chief, Field Services Branch, U.S. EPA Report No. SESDPROC-111-R4, Effective Date March 14, 2018.
Winner M.D, Jr. and Coble R.W., Hydrogeologic Framework of the North Carolina
Coastal Plain Aquifer System, 1996.
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023
TABLES
Page 1 of 1
TABLE 1
SITE HISTORY — UST AND OTHER RELEASE INFORMATION
Incident Name and No.: US 17 Country Store - 38813
UST ID
Number
Name of Owner/
Operator
Last
Contents
Previous
Contents
Capacity
(gal)
Construction
Details
Tank
Dimensions
(feet)
Installation
Date
(mm/dd/yy)
Date
Removed
(mm/dd/yy)
1 Gasoline Gasoline 10,000 Single Wall
Steel 22.75 x 8.5 04/22/82 06/21/22
2 Gasoline Gasoline 6,000 Single Wall
Steel 16 x 8 04/22/82 06/21/22
3 Kerosene Kerosene 2,000 Single Wall
Steel 12 x 5.4 04/22/88 06/21/22
4 Diesel Diesel 10,000 Single Wall
Steel 26 x 8 04/22/88 06/21/22
5*Diesel Diesel 2,000 Steel 12 x 4.5 04/22/82 AIP 05/28/96
6 Diesel Diesel 10,000 Single Wall
Steel 26.5 x 8 01/01/84 06/21/22
Incident
Number
Material
Released
Date Release
Discovered
(mm/dd/yy)
38813 Petroleum 08/13/15
Information on UST 5 obtained from C&S (1996).
Information on release obtained from ECE (2015) and NCDEQ (2020).
* = Tank system was not associated with the release.
gal = gallons
XX = Exact date unknown.
AIP = Abandoned In Place
Hollowell Oil Co.
(dissolved) /
Hubert D.
Ambrose
(deceased)
Description of the Release
Groundwater contamination was discovered during site assessment activities in August 2015.
Dates of Ownership/
Operation
(mm/dd/yy)
01/01/84 - 11/06/08
04/22/82 - 04/XX/96
04/22/82 - 11/06/08
04/22/88 - 11/06/08
NCDEQ; 38813_US 17 Country Store; T1_Site History
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 2
Incident Name and No.: US 17 Country Store - 38813
Well ID Property Address Parcel ID Owner Name Owner Mailing
Address Well Use
Distance/
Direction
from
Source Area
(ft.)
Comment
WSW-1
Intersection of US
Hwy 17 & Foreman
Bundy Rd
7992 03444414 Yeng K Choo &
Ann Kuan Tan
2507 Dan & Mary
Street, Elizabeth City,
NC 27909
Active
Non-
Potable
300 / NW
Appeared to be
used for watering
crops.
Receptor
ID Location Contact
Distance/
Direction from
Source Area (ft.)
Drainage Ditch Parrallel to US 17 —Northwest Site
Boundary
Information obtained from a field survey conducted on November 9, 2022, receptor survey letters sent to properties within 1,000 feet.
ft. = feet
Drainage ditch along the site boundary, suspected to intersect with
the water table.
Description
PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
NCDEQ; 38813_US 17 Country Store; T2_Receptor Info
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 3
WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
Incident Name and No.: US 17 Country Store - 38813
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Diameter
(inches)
Well
Casing
Depth
(ft. BLS)
Screened
Interval
(x to y ft.
BLS)
Bottom
of Well
(ft. BLS)
Top of
Casing
Elevation
(ft.)
Free-Phase
Product
Thickness*
Depth to
Groundwater
from Top of
Casing (ft.)
Groundwater
Elevation (ft.)Comments
11/09/22 NMT 4.64 95.36
03/29/23 NMT 0.99 99.01 Ɨ
11/09/22 NMT 5.13 94.98
03/29/23 NMT 1.87 98.24
11/09/22 NMT 5.05 95.03
03/29/23 NMT 2.76 97.32 Ɨ
11/09/22 NMT 5.04 95.03
03/29/23 NMT 2.77 97.30 Ɨ
TMW-01 03/22/23 03/29/23 4.0/2.0 25.0 25.0-30.0 30.0 100.14 NMT 2.98 97.16 Type III; Ɨ
ft. BLS = feet Below Land Surface
NMT = No Measurable Thickness
Ɨ = Water level was measured above the screened interval.
10/25/22
10/25/22
10/25/22
MW-04
MW-03
MW-02
MW-01 100.0014.04.0-14.04.02.0
2.0 1.5 1.5-11.5 11.5 100.11
100.0814.04.0-14.04.02.0
* = if free-phase product is present in a well, ground water elevation should be calculated by : [top of casing elevation - depth to water]+ [free product thickness x
specific gravity of the fuel type]
2.0 4.0 4.0-14.0 14.0 100.0710/25/22
NCDEQ; 38813_US 17 Country Store; T3_Well Construction & Gauging
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 4
SUMMARY OF GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: US 17 Country Store - 38813
Date
Collected
(mm/dd/yy)
03/29/23 <2.0 4.1 <1.7 0.25 J 0.87 <0.14 <0.20 3.4 0.81 4.9 <0.38 1.0 <0.22 0.38 J <0.15 <0.73 BMDL
03/29/23 <4.0 <0.37 <3.4 0.82 J 1.2 <0.28 <0.40 <0.44 0.72 J <0.34 <0.76 0.98 J <0.45 <0.40 <0.30 <1.47 BMDL
03/29/23 <8.0 2.1 <6.7 0.60 J <0.51 <0.57 <0.81 2.4 1.9 J 5.1 <1.5 3.4 <0.89 <0.80 0.64 J <2.97 BMDL
03/29/23 <20 780 24 J 24 17 2.3 J 13 350 83 430 79 L 220 16 35 <1.5 32.5 J BMDL
03/29/23 12 J 0.76 <1.7 1.4 0.55 <0.14 <0.20 3.8 1.1 3.9 1.4 L 2.5 6.4 13 1.1 8.60 BMDL
03/29/23 <2.0 <0.18 <1.7 <0.15 <0.13 <0.14 <0.20 <0.22 <0.15 <0.17 <0.38 <0.12 <0.22 <0.20 <0.15 <0.73 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit (refer to analytical report for a complete list of analytes and detection limits)
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than method detection limit
J = Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag).
L = Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side (L-04 Flag).
MW-01
Well/
Sample
ID
28,500
400
24,100
400
50,000
500
80,000
600
Trip Blank
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
5,000
1
4,000,000
4,000
5,900
70
8,800
70
14,750
70
70,000
70
TMW-01
Varies
Varies
30,500
70
20,000
20
6,000
6
26,100
70
260,000
600
MW-04
MW-03
MW-02 Total Xylenes All Other SM 6200B Analytes1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenesec-Butylbenzene Contaminant of
Concern
Acetone Benzene 2-Butanone (MEK)n-ButylbenzeneMethyl tert-Butyl Ether (MTBE)Naphthalene n-PropylbenzeneToluene tert-Butylbenzene Diisopropyl Ether (DIPE)EthylbenzeneIsopropylbenzene (Cumene)NCDEQ; 38813_US 17 Country Store; T4_GW Results (SM 6200B)
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 5
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: US 17 Country Store - 38813
Date
Collected
(mm/dd/yy)
11/09/22 5.6 J 19 <3.2 1.1 1.1 <0.26 <0.26 <0.26 9.5 1.9 <0.19 17 3.1 3.4 0.58 J 1.6 0.36 J 5.9 BMDL
03/29/23 <2.0 4.1 <1.7 0.25 J 0.87 <0.14 <0.13 <0.20 3.4 0.81 <0.13 4.9 <0.38 1.0 <0.22 0.38 J <0.15 <0.73 BMDL
11/09/22 <4.1 140 <3.2 8.8 13 0.50 J 0.58 J 0.32 J 5.1 18 <0.19 48 7.5 24 1.4 <0.40 <0.23 <2.46 J*BMDL
03/29/23 <4.0 <0.37 <3.4 0.82 J 1.2 <0.28 <0.26 <0.40 <0.44 0.72 J <0.25 <0.34 <0.76 0.98 J <0.45 <0.40 <0.30 <1.47 BMDL
11/09/22 <10 96 <8.1 14 7.8 <0.64 <0.65 7.6 130 36 3.7 38 51 83 69 390 120 560 BMDL
03/29/23 <8.0 2.1 <6.7 0.60 J <0.51 <0.57 <0.51 <0.81 2.4 1.9 J <0.51 5.1 <1.5 3.4 <0.89 <0.80 0.64 J <2.97 BMDL
11/09/22 <8.1 180 16 J 25 17 2.4 <0.52 2.7 250 120 1.0 J 12 91 320 4.9 54 1.6 J 23 BMDL
03/29/23 <20 780 24 J 24 17 2.3 J <1.3 13 350 83 <1.3 430 79 L 220 16 35 <1.5 32.5 J BMDL
03/29/23 12 J 0.76 <1.7 1.4 0.55 <0.14 <0.13 <0.20 3.8 1.1 <0.13 3.9 1.4 L 2.5 6.4 13 1.1 8.60 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than method detection limit
* = The value represents the sum of the reported practical quantitation limit of one analyte and the detected concentration of the other analyte.
J = Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag).
L = Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side (L-04 Flag).p-Isopropyltoluene (p-Cymene)Contaminant of
Concern
Acetone Benzene 2-Butanone (MEK)n-Butylbenzenesec-Butylbenzene Well/
Sample
ID
tert-Butylbenzene 1,4-Dichlorobenzene Diisopropyl Ether (DIPE)EthylbenzeneIsopropylbenzene (Cumene)Total Xylenes All Other SM 6200B AnalytesMethyl tert-Butyl Ether (MTBE)Naphthalene n-PropylbenzeneToluene 1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneVaries
Varies
30,500
70
11,700
25
20,000
20
6,000
6
26,100
70
260,000
600
80,000
600
28,500
400
24,100
400
50,000
500
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
5,000
1
4,000,000
4,000
5,900
70
8,800
70
14,750
70
405
6
70,000
70
TMW-01
MW-04
MW-03
MW-02
MW-01
NCDEQ; 38813_US 17 Country Store; T5_Historical GW (SM 6200B)
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
Date
Collected
(mm/dd/yy)
11/09/22 <0.567 <0.503 <0.457 <0.767 <0.568 <0.672 <0.755 <0.523 <0.519 <0.249 <0.500 <0.669 BMDL
11/09/22 3.80 J 0.689 J <0.464 <0.780 8.53 4.70 J 78.5 13 <0.527 2.09 J <0.508 2.26 J BMDL
11/09/22 <0.561 <0.498 <0.452 2.50 J <0.562 15.2 13.9 <0.518 0.984 J <0.246 0.789 J <0.662 BMDL
11/09/22 <0.580 <0.514 0.469 J <0.784 0.950 J 68.8 90.9 <0.535 <0.530 1.71 J <0.511 <0.684 BMDL
All results in micrograms per liter (µg/L).
EPA = Environmental Protection Agency
BMDL = Below Method Detection Limit
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
NE = Not Established
< = Less than method detection limit
J = Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag).
Varies
Varies
GCL (µg/L)
2L GWQS (µg/L)
1,950
80
2,000
2,000
845
300
6,000
6
NE
NE
100,000
100
400,000
400
30,000
30
NE
NE
12,000
30
550
200
TABLE 6
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — EPA METHOD 625
Incident Name and No.: US 17 Country Store - 38813
MW-04
MW-03
200
200PyreneContaminant of
Concern
Well/
Sample
ID AcenaphtheneAnthraceneFluoreneNaphthalene2-MethylnaphthalenePhenanthreneAll Other EPA 625 AnalytesMW-01
MW-02 3/4-MethylphenolPhenol2-Methylphenol2,4-DimethylphenolDiethylphthalateNCDEQ; 38813_US 17 Country Store; T6_Historical GW (EPA 625)
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023
Page 1 of 1
TABLE 7
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — MADEP EPH/VPH
Incident Name and No.: US 17 Country Store - 38813
Date
Collected
(mm/dd/yy)
11/09/22 100 <95 <95 210 <200 <200 210 <300 <95 <295 ƚ
2,100 610 1,800 340 210 580 340 2,310 610 2,380
440 H,S 180 H,S 800 H,S 340 210 580 340 650 H,S 180 H,S 1,380 H,S
11/09/22 150 <96 230 1,400 730 1,700 1,400 880 <96 1,930
170 <98 270 2,300 900 1,900 2,300 1,070 <98 2,170
240 H <99 H 230 H 2,300 900 1,900 2,300 1,140 H <99 H 2,130 H
All results in micrograms per liter (µg/L).
MADEP = Massachusetts Department of Environmental Protection
EPH = Extractable Petroleum Hydrocarbon
VPH = Volatile Petroleum Hydrocarbon
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than method detection limit
NE = Not Established
ƚ = The method detection limit is above the 2L GWQS.
H = Sample was extracted past the recommended holding time (H-06 Flag).
S = Sample was re-extracted outside of holding time since surrogate standard recovery was outside of control limits. Data from analysis
performed outside of holding time is also reported since surrogate recovery is acceptable (S-10 Flag).
** = Sample was run twice for EPH analysis due to laboratory issues (See H and S Flags). Refer to the analytical report for all flags and the
case narrative summary.C9-C22 AromaticsWell/
Sample
ID
Method EPH Analytical Fractions VPH Analytical
Fractions
Combined MADEP
EPH/VPH Fractions
Contaminant of
Concern
C9-C18 AliphaticC19-C36 AliphaticC11-C22 AromaticC5-C8 AliphaticC9-C12 AliphaticNE
200 C9-C10 AromaticC5-C8 AliphaticsC9-C18 AliphaticsC19-C36 AliphaticsMW-01
GCL (µg/L)
2L GWQS (µg/L)
NE
700
NE
10,000
MW-03
11/09/22MW-04**
11/09/22MW-02**
NE
200
NE
400
NE
700
NE
200
NE
400
NE
700
NE
10,000
NCDEQ; 38813_US 17 Country Store; T7_Historical GW (MADEP)
CATLIN Project No. 220209
CATLIN Engineers and Scientists
April 2023

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

FIGURES
FIGUREPROJECTTITLE
1SITE VICINITY MAP
SITE LOCATIONUS HWY 17 SFOREMAN BUNDY RD
Copyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
US 17 COUNTRY STORE1383 US HWY 17 SOUTHELIZABETH CITY, NC
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220209APRIL 2023 AS SHOWN KMC/BJA
INCIDENT NO.
38813
FIGUREPROJECTTITLE
2POTENTIAL RECEPTOR MAP
!(W
SITE LOCATIONUS HWY 17 SFOREMAN BUNDY RD
1 ,5 0 0 F EET RADIUS
500F E E T RADIUS
WSW-1
DRAINAGE DITCHDRAINAGE DITCH
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
US 17 COUNTRY STORE1383 US HWY 17 SOUTHELIZABETH CITY, NC
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220209APRIL 2023 AS SHOWN KMC/BJAINCIDENT NO.38813
LEGEND
Active Non-Potable
Water Supply Well!(W
FIGUREPROJECTTITLE
3
!>
!>
!>
!>
!(>
FORMER COUNTRY STOREUS HIGHWAY 17 S2,000-GALKEROSENE UST
KEROSENE DISPENSER
DISPENSERS
DIESELDISPENSERS
10,000-GALDIESEL UST
10,000-GALGASOLINEUST
DISPENSERS
6,000-GALGASOLINE UST
!(V
!(V
2,000-GAL DIESEL UST(ABANDONED IN PLACE)
10,000-GALDIESEL UST
MW-01
MW-02
MW-03
MW-04TMW-01
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
³
30 0 30 6015
Feet
NOTES: 1. UST system components and utility locations provided bySEPI Geohpysical Investigation (2021) and are approximate.2. Well locations were obtained from field activities conducted by CATLIN on October 25, 2022 and March 22, 2023.
Parcel Boundary
Assumed Supply
Lines
UST System ElectricalComponent
LEGEND
Vent(s)!(V
Vent Lines (Removed)
Telephone Lines
Unknown Lines
SITE MAPUS 17 COUNTRY STORE1383 US HWY 17 SOUTHELIZABETH CITY, NC
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220209APRIL 2023 AS SHOWN KMC/BJA
INCIDENT NO.
38813
Approximate Location
of Former UST System
Assumed Supply Lines (Abandoned in Place)
MonitoringWell (Type II)!>
Excavation Limits
MonitoringWell (Type III)((>
FIGUREPROJECTTITLE
4
!>
!>
!>
!>
!(><US HIGHWAY 17 S!(V
!(V
MW-01(99.01)
MW-02(98.24)
MW-03(97.32)
MW-04(97.30)
TMW-01*(97.16)98.7598.5098.2598.0097.7597.50Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
³
30 0 30 6015
Feet
NOTES: 1. UST system components and utility locations provided bySEPI Geohpysical Investigation (2021) and are approximate.2. Well locations were obtained from field activities conducted by CATLIN on October 25, 2022 and March 22, 2023.3. The groundwater elevation contour interval is 0.25 feet. * = Deep well; elevation not used for contouring purposes.
GROUNDWATER ELEVATION –MARCH 29, 2023
US 17 COUNTRY STORE1383 US HWY 17 SOUTHELIZABETH CITY, NC
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220209APRIL 2023 AS SHOWN KMC/BJAINCIDENT NO.38813
Parcel Boundary
Assumed Supply Lines
UST System ElectricalComponent
LEGEND
Vent(s)!(V
Vent Lines (Removed)
Approximate Location of Former UST System
Assumed Supply Lines (Abandoned in Place)
Gauged MonitoringWell (Type II)!>
Gauged Monitoring Well (Type III)!(>
Groundwater Contour
Groundwater Flow Direction
<Groundwater Elevation (Feet)(##)
FIGUREPROJECTTITLE
5
!>
!>
!>
!>
!(>
!(V
!(V
MW-01
MW-02
MW-03
MW-04TMW-01*
ESTIMATED HORIZONTAL EXTENT OF 2L GWQS EXCEEDANCES
??
?????Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
³
30 0 30 6015
Feet
NOTES: 1. UST system components and utility locations provided bySEPI Geohpysical Investigation (2021) and are approximate.2. Well locations were obtained from field activities conducted by CATLIN on October 25, 2022 and March 22, 2023.3. * = Deep well; analytical results not used for contouring purposes
Parcel Boundary
Assumed Supply Lines
UST System ElectricalComponent
LEGEND
Vent(s)!(V
Vent Lines (Removed)
MONITORING WELLGROUNDWATER SAMPLEANALYTICAL RESULTS –MARCH 29, 2023
US 17 COUNTRY STORE1383 US HWY 17 SOUTHELIZABETH CITY, NC
JOB NO.DATE SCALE DRAWN BY/CHECKED BY220209APRIL 2023 AS SHOWN KMC/BJAINCIDENT NO.38813
Approximate Location of Former UST System
Assumed Supply Lines (Abandoned in Place)
Sampled MonitoringWell (Type II)!>
Sampled Monitoring Well (Type III)!(>
Incident Name and No.: US 17 Country Store - 38813
DateCollected
03/29/23 4.1 0.81 4.9 <0.38 1.003/29/23 <0.37 0.72 J <0.34 <0.76 0.98 J03/29/23 2.1 1.9 J 5.1 <1.5 3.403/29/23 780 83 430 79 L 22003/29/23 0.76 1.1 3.9 1.4 L 2.5
All results in micrograms per liter (µg/L).Refer to Table 4 for all results and notes.Bold results are above 2L GWQS.
MW-04
MW-02MW-03
SUMMARY OF GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200B
Contaminant of Concern
Benzene Naphthalene n-PropylbenzeneIsopropylbenzene (Cumene)Methyl tert-Butyl Ether (MTBE)Well/ SampleIDMW-01
TMW-01 GCL (µg/L)2L GWQS (µg/L) 5,0001 6,0006 26,1007020,0002030,50070

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDICES

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDIX A HISTORICAL DATA
APPENDIX A HISTORICAL DATA (ECES, 2015)
NCDEQ; 38813_US 17 Country Store CATLIN Project No. 220209 CATLIN Engineers and Scientists April 2023
APPENDIX A HISTORICAL DATA (ECES, 2015)
NCDEQ; 38813_US 17 Country Store CATLIN Project No. 220209 CATLIN Engineers and Scientists April 2023

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDIX B SITE PHOTOGRAPHS
APPENDIX B SITE PHOTOGRAPHS – MARCH 21 AND 22, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store Site / Drill Rig Facing East
US 17 Country Store
Site Facing Southeast
APPENDIX B SITE PHOTOGRAPHS – MARCH 21 AND 22, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store Site Facing Southwest
US 17 Country Store Drilling TMW-01
Facing East
APPENDIX B SITE PHOTOGRAPHS – MARCH 21 AND 22, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
Drilling TMW-01
US 17 Country Store
Developing TMW-01
APPENDIX B SITE PHOTOGRAPHS – MARCH 21 AND 22, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
Finished TMW-01 Facing Southeast
US 17 Country Store Damaged MW-03 Facing Southwest
APPENDIX B SITE PHOTOGRAPHS – MARCH 21 AND 22, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store Damaged MW-02 Facing Northeast
US 17 Country Store Damaged MW-02
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
Site Facing East
US 17 Country Store MW-01
Facing Southeast
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store MW-01 Sampling
US 17 Country Store MW-01 Well Cap & Lock
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
MW-02
After Rehab
US 17 Country Store
MW-02 After Rehab
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
MW-03
After Rehab
US 17 Country Store
MW-02 After Rehab
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store MW-04
US 17 Country Store MW-04
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store
MW-04 (Right)
US 17 Country Store TMW-01 (Left)
APPENDIX B SITE PHOTOGRAPHS – MARCH 29, 2023
NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists CATLIN Project No. 220209 April 2023

US 17 Country Store WSW-1
US 17 Country Store WSW-1

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDIX C
JOB HAZARD ANALYSES
AND FIELD DATA SHEETS
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Drill Rig N/A
tools and materials N/A
Drill Rig N/A
Drill Rig 85 dBA
Exposure Potential
Likely
Likely
Likely
Start Stop
10:45 14:45
14:45 14:50
14:50 17:30
17:30 18:00
7:00 7:30
7:30 7:45
7:45 12:30
12:30
Date and Time:
3/21/23 @ 14:50
3/22/23 @ 07:45
3/21/23 @ 14:50
3/22/23 @ 07:45
3/21/23 @ 14:50
3/22/23 @ 07:45
Tommy Chalmers / CATLIN
Cameron Stratton / CATLIN
Equipment Used:PPE D/Water Level Indicator/Sampling Supplies/Generator/Pressure Washer
PERSONNEL ONSITE
Name and Company (Print)Signature
Trevor Mizelle / CATLIN
Cleaned up equipment and departed site.
Snakes surroundings
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
DAILY TASK
Vehicle # 50
Mileage:Start: End:
Travel from Wilmington office to site on March 21, 2023.
On-site Health and Safety Meeting covering proper PPE, weather concerns, equipment and road safety.
Set up, drilled TMW-01 to 20' w/ mud rotary and taking split spoons.Changed to HSA and drilled to 20'. Grout and set outside casing.
Travel from site ot hotel.
Travel from hotel to site on March 22, 2023.
Drilled out casing set yesterday with mud rotary. Continued down to 30' taking split spoons. Set Type III MW @
30' w/ 5' screen. Survey new well with existing well MW-01. Take pics of wells and located destroyed wells.
On-site Health and Safety Meeting covering proper PPE, weather concerns, equipment and road safety.
Insect bites and stings surroundings
Drill Rig Operations Likely
Heavy Lifting/ Moving Likely
Rolling or Pinching Objects Likely
Noise Likely
Biological Hazards
Name of Biological Hazard Source
Cold Weather Operations Unlikely
Heat (ambient)Likely
Slips/Trips/Falls Likely
NAPHTHALENE ppm
* Gas and/or Diesel
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
ETHYL BENZENE ppm
Date(s) this JHA
Conducted:
3/21/23 & 3/22/23
Employee Certifying this JHA
Print Name: Benjamin J. Ashba, P.G.Signature:
Weather:Sunny, 70's
Potential Chemicals Concentration
BENZENE ppm
Site-Specific Job Hazard Analysis
Operational Phase Task/Operation Location Where Task/Operation Performed
Monitoring Soil Borings/Well Installations Lancaster Store, Elizabeth City, NC
Page 1 of 1
CLIENT'S CATLIN
NAME:PROJECT:CATLIN PROJECT #:PHASE:
INSTRUMENT #:ELEVATION (TBM):DATE:3/22/2023 ROD #:UNITS (FT./M):
TOP
BOTTOM5.665.105.365.135.665.10
FIELD NOTES BY:DATE:3/22/2023 INSTRUMENT BY:
NOTES REDUCED BY:DATE:4/19/2023 ROD PERSON:
HI - (-) = ELEV.* A sketch must be provided with the level notes.
T. Mizelle T. Mizelle
S. Miller C. Stratton
0.00
(+) = MID at TBM or BM (TOP - BOTTOM) * 100 = DISTANCE
TBM + (+) = HI (TOP + BOTTOM)/2 = MID (-)
105.38 0.00
30 0 105.38
29 0
28 0 105.38 0.00
0.00
27 0 105.38 0.00
105.38 0.00
26 0 105.38
25 0
24 0 105.38 0.00
0.00
23 0 105.38 0.00
105.38 0.00
22 0 105.38
21 0
20 0 105.38 0.00
0.00
19 0 105.38 0.00
105.38 0.00
18 0 105.38
17 0
16 0 105.38 0.00
0.00
15 0 105.38 0.00
105.38 0.00
14 0 105.38
13 0
12 0 105.38 0.00
0.00
11 0 105.38 0.00
105.38 0.00
10 0 105.38
9 0
8 0 105.38 0.00
0.00
7 0 105.38 0.00
105.38 0.00
6 0 105.38
5 0
MW-01
4 0 105.38 0.00
5.25 TMW-01
3 0 56 5.38 105.38 100.00 5.38
100.00 5.38 MW-01
2 71 23 5.24 105.38 100.14
HI ELEV. (feet)CHECK (T+B)/2 NOTES
1 0 56 5.38 105.38
100.00
POINT ANGLE
(degrees)
DISTANCE
(feet)MID (-)(+)
REDUCED LEVEL NOTES
US 17 Country Store220209
BENCH MARK DESC.:MW-01
NCDEQ - SLP
Source Exposure Limit
Groundwater and/or soil vapor 0.5 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 20 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 100 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 50 ppm TLV-TWA ACGIH
Groundwater and/or soil vapor 10 ppm TLV-TWA ACGIH
Source Exposure Limit
atmosphere N/A
atmosphere N/A
surroundings N/A
Roads N/A
Exposure Potential
Likely
Unlikely
Unlikely
Start Stop
11:45 12:30
12:30 12:45
12:45 18:15
18:15 18:30
18:30 18:45
Date and Time:
3/29/23 @ 12:45
ETHYL BENZENE
NAPHTHALENE ppm
Physical Hazards
Name of Physical Hazard Exposure Level/ Potential
* Gas and/or Diesel
Sunny and 70s
Site-Specific Job Hazard Analysis
Location Where Task/Operation Performed
Lancaster Store, Elizabeth City, NC
Task/Operation
Gauge and Sample Wells
Employee Certifying this JHA
Print Name: Sean O'Neil, P.E.Signature:
Operational Phase
Monitoring
Date(s) this JHA
Conducted:
03/29/2023
Weather:
Mob and Travel to Site.
Located, opened, gauged, photographed, and sampled monitoring wells. Spoke with property owner. Rehabbed
MW-2 and MW-3.
Attempted WSW access but was unable (no residence or office on site).
Depart site and drove to hotel.
Chemical Hazards
Potential Chemicals Concentration
BENZENE ppm
ppm
TOLUENE ppm
XYLENE, ALL ISOMERS ppm
METHYL TERT-BUTYL ETHER ppm
Traffic Likely
Biological Hazards
Name of Biological Hazard Source
Poison Plants (Ivy, Oak, and/or Sumac)surroundings
Van #59 Mileage:
On-Site Health and Safety briefing
Cold Weather Operations Unlikely - 60s out
Heat (ambient)Unlikely - 60s out
Slips/Trips/Falls Likely
Insect bites and stings surroundings
Start: End:
DAILY TASK
Snakes surroundings
PERSONNEL ONSITE
Name and Company (Print)Signature
Nathaniel Newman / CATLIN
Equipment Used:PPE D/Interface Probe/Sampling Supplies/Aqua Troll 600/Bailers
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
MW-01 13.01
0.99 2.123
NMT 6.370
14 10.616
2
Method:Bailer Purge Start Time:15:11
Required Bails for 3 Well Volumes:27 Purge Stop Time:15:20
Required Bails for 5 Well Volumes:45 Was Well Purged Dry?No
Number of Bails Removed:27 Sample Time:15:20
Groundwater Removed (gal):6.5
Equipment Used:
Time
Specific
Cond.
(µS/cm)
pH
(Standard
Units)
ORP
(mV)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
15:08 0.00 12.72 -75.35 8.44 23.67
15:09 1380.70 12.49 -58.85 4.79 24.00
15:10 1462.94 12.47 -55.80 3.17 24.10
15:11 1521.78 12.45 -52.51 3.26 24.26
15:12 1544.44 12.42 -50.64 3.46 24.39
15:13 924.12 12.42 -49.88 3.59 24.54
15:14 1580.59 12.42 -49.58 3.69 24.63
15:15 1497.01 12.42 -49.17 3.72 24.72
15:16 1571.88 12.42 -48.66 3.86 24.66
Laboratory:ConTest Analysis:
GROUNDWATER SAMPLING FORM
Water Column (ft below TOC)
One Well Volume (gal)
Three Well Volumes (gal)
Five Well Volumes (gal)
Monitoring Well Information
Well Data
Well ID
Depth to Product (ft below TOC)
Total Well Depth (ft)
Nate Newman
3/29/2023
US 17 Country Store
220209
Volume of Groundwater in Well
NCDEQ - SLP
Aqua Troll 600
Turbidity and Additional
Sampling Notes
Well Diameter (inches)
Depth to Water (ft below TOC)
6200B
Laboratory Analysis Information
Geochemical Parameters
Moderate turbidity; light brown.
Purging Information Information
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
MW-02 9.63
1.87 1.572
NMT 4.715
11.5 7.858
2
Method:Bailer Purge Start Time:15:55
Required Bails for 3 Well Volumes:20 Purge Stop Time:16:01
Required Bails for 5 Well Volumes:33 Was Well Purged Dry?No
Number of Bails Removed:20 Sample Time:16:01
Groundwater Removed (gal):4.8
Equipment Used:
Time
Specific
Cond.
(µS/cm)
pH
(Standard
Units)
ORP
(mV)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
15:52 1.23 13.29 -61.06 8.06 26.21
15:53 1783.98 12.84 -219.11 5.16 24.45
15:54 1821.60 12.72 -168.67 3.55 24.30
15:55 1809.94 12.62 -138.39 3.48 24.43
15:56 1747.79 12.54 -120.53 3.45 24.56
15:57 1789.37 12.48 -109.63 3.26 24.73
15:58 1788.75 12.44 -103.25 3.25 24.80
15:59 1203.88 12.47 -100.98 3.23 24.98
16:00 3.66 12.53 -98.95 8.04 24.99
16:01 3.39 12.56 -88.70 8.33 24.98
Laboratory:ConTest Analysis:
GROUNDWATER SAMPLING FORM
US 17 Country Store Nate Newman
220209 3/29/2023
NCDEQ - SLP
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
Depth to Water (ft below TOC)One Well Volume (gal)
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft)Five Well Volumes (gal)
Bottom at 11.4. Moderate turbidity; brown.
Laboratory Analysis Information
6200B
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
MW-03 11.24
2.76 1.834
NMT 5.503
14 9.172
2
Method:Bailer Purge Start Time:13:50
Required Bails for 3 Well Volumes:19 Purge Stop Time:14:00
Required Bails for 5 Well Volumes:39 Was Well Purged Dry?No
Number of Bails Removed:19 Sample Time:14:00
Groundwater Removed (gal):4.6
Equipment Used:
Time
Specific
Cond.
(µS/cm)
pH
(Standard
Units)
ORP
(mV)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
13:52 0.00 13.46 230.72 8.28 26.43
13:53 0.00 13.00 99.67 7.99 26.72
13:54 1880.51 12.52 -19.09 4.31 25.39
13:55 746.84 12.52 -47.30 4.14 25.33
13:56 1890.70 12.48 -63.01 3.64 25.42
13:57 1823.92 12.43 -71.01 3.69 25.61
13:58 1793.43 12.40 -73.65 3.61 25.77
Laboratory:ConTest Analysis:
GROUNDWATER SAMPLING FORM
US 17 Country Store Nate Newman
220209 3/29/2023
NCDEQ - SLP
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
Depth to Water (ft below TOC)One Well Volume (gal)
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft)Five Well Volumes (gal)
Moderate turbidity; gray.
Laboratory Analysis Information
6200B
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
MW-04 11.23
2.77 1.833
NMT 5.498
14 9.164
2
Method:Bailer Purge Start Time:14:51
Required Bails for 3 Well Volumes:23 Purge Stop Time:14:58
Required Bails for 5 Well Volumes:39 Was Well Purged Dry?No
Number of Bails Removed:23 Sample Time:14:58
Groundwater Removed (gal):5.5
Equipment Used:
Time
Specific
Cond.
(µS/cm)
pH
(Standard
Units)
ORP
(mV)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
14:48 0.00 195.59 8.42 25.71
14:49 532.51 12.32 -141.21 4.44 25.59
14:50 501.06 12.26 -137.78 2.95 25.69
14:51 505.01 12.22 -135.04 2.91 25.80
14:52 510.54 12.20 -131.86 2.99 25.90
14:53 518.66 12.18 -129.74 3.11 25.99
14:54 514.85 12.17 -124.99 2.87 26.04
Laboratory:ConTest Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft)Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
High turbidity; gray/black.
Laboratory Analysis Information
Depth to Water (ft below TOC)One Well Volume (gal)
GROUNDWATER SAMPLING FORM
US 17 Country Store Nate Newman
220209 3/29/2023
NCDEQ - SLP
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT:SAMPLED BY:
CATLIN PROJECT # :DATE SAMPLED:
CLIENT'S NAME:
TMW-01 27.02
2.98 4.410
NMT 13.229
30 22.048
2
Method:Bailer Purge Start Time:15:29
Required Bails for 3 Well Volumes:56 Purge Stop Time:15:47
Required Bails for 5 Well Volumes:92 Was Well Purged Dry?No
Number of Bails Removed:56 Sample Time:15:47
Groundwater Removed (gal):13.4
Equipment Used:
Time
Specific
Cond.
(µS/cm)
pH
(Standard
Units)
ORP
(mV)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
15:26 1.45 12.63 -17.70 8.37 24.79
15:27 2789.94 13.76 -194.53 7.23 26.40
15:28 2729.80 13.76 -194.00 4.81 26.78
15:29 2840.40 13.78 -188.84 4.72 27.16
15:30 3022.22 13.79 -186.47 4.52 27.50
15:31 3028.73 13.80 -184.81 4.44 27.74
15:32 2894.79 13.80 -184.71 4.22 27.96
15:33 2654.88 13.78 -183.95 4.08 28.15
15:34 2372.01 13.76 -182.64 4.04 28.28
15:35 2054.65 13.74 -180.65 4.03 28.38
15:36 1810.31 13.71 -177.39 3.92 28.44
15:37 1474.74 13.65 -173.28 3.98 28.49
15:38 1226.10 13.61 -169.46 3.88 28.53
15:39 1009.26 13.55 -164.00 3.95 28.55
15:40 846.84 13.48 -157.77 3.99 28.56
15:41 692.61 13.42 -152.28 3.86 28.56
15:42 666.23 13.43 -149.32 3.77 28.64
15:43 613.48 13.39 -143.58 3.75 28.61
Laboratory:ConTest Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft)Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
Clear
Laboratory Analysis Information
Depth to Water (ft below TOC)One Well Volume (gal)
GROUNDWATER SAMPLING FORM
US 17 Country Store Nate Newman
220209 3/29/2023
NCDEQ - SLP
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDIX D

WELL LOG AND
WELL CONSTRUCTION RECORD

30.0
5.0
8.0
13.0
18.0
22.4
27.4
5
14
7
9
5
8
2
7
7
1
3
2
4
13
7
5
6
5
3
11
5
2
6
4
30.0 4" Sch. 40 PVC25.0
20.0
30.0
0.0
20.0
22.0
30.02" Sch. 40 PVC2" Slot .010Sch. 40 PVCM
M
Sat.
Sat.
Sat.
Sat.
5.0
7.5
5.0
7.5
29.4
FILL
(CH) - Gray, Highly Plastic CLAY. Strong HCO
(SP) - Gray, F. SAND. Strong HCO from 8.0-10.0' BLS
Mod. HCO from 13.0-15.0' BLS
BORING TERMINATED AT ELEVATION 70.1 ft in F.
SAND
95.1
92.6
95.1
92.6
70.7
193.6
145.4
13.7
3.6
141.9
42.8
DRILL MACHINE:Diedrich D-50 METHOD:MUD ROTRAY/HSA
COUNTY:PASQUOTANK
2795238 924304
T.O.C. ELEV.:
TOTAL DEPTH:
WELL DEPTH:
NC
SHEET
3.4
NM
DEPTH
1
100.14
30.0
30.0
0 HOUR DTW:
24 HOUR DTW:END DATE:3/22/23
OF1
BORING LOCATION:~3' NE of MW-04
BLOW COUNT
0.5ft
START DATE:3/21/23
0.5ft
WELL ID:
STATE:
TMW-01NORTHING:
LOGGED BY:
DRILLER:
CREW:
0.5ft0.5ft
EASTING:
PROJECT NO.:220209
SYSTEM:NCSP NAD 83 (USft)
US 17 COUNTRY STOREPROJECT:T. MIZELLE
D. T. Chalmers, JR
C. STRATTON
LOCATION:ELIZABETH CITY
ENVIRONMENTAL, CIVILGEOTECHNICAL
Wilmington, Raleigh, Washington,Charleston
CATLIN BORING LOG 220209_NCDEQ SLP US 17 COUNTRY STORE.GPJ CATLIN.GDT 4/4/23Concrete Bentonite Pellets #2 Medium Sand
0.0
WELL LOG
WELL
DETAIL
SOIL AND ROCK
DESCRIPTIONLAB.DEPTH
MOIS
0.0 LAND SURFACE
LOG ELEVATION
100.1
OVA
(ppm)
220209
03/22/23
MUD ROTRAY/HSA
4146A
3.41
TMW-01
-76.3025
D. T. Chalmers, JR
36.25986
PASQUOTANK
1
X
4/4/2023
10.25
Surface Pour
CATLIN Engineers and Scientists
X
2 Slot .010
1383 US HWY 17 SOUTH, ELIZABETH CITY, NC 27909
Bent. Pellets22
PVC
25
20N/A
22 30 Torpedo Sand
30.0
X 20
25 30 PVC
2
Sch. 40
0
0 4 Sch. 40
Sch. 40 PVC
Well ID#:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
(if well field, one lat/long is sufficient)
N
6. Is (are) the well(s):
Yes
TemporaryPermanent or
or No7. Is this a repair to an existing well:
8. Number of wells constructed:
For multiple injection or non-water supply wells ONLY with the same construction, youcan submit one form.
9. Total well depth below land surface:
For multiple wells list all depths in different (example- 3@200' and 2@100')
W
(ft.)10. Static water level below top of casing:
If water level is above casing, use "+"
11. Borehole diameter:
MATERIAL
FROM
Residential Water Supply (shared)
Adapted from Form GW-1
ft.
ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.
ft.
(ft.)
(in.)
ft.
ft.ft.
ft.
ft.
ft.in.
in.
ft.
ft.
ft.ft.
ft.
ft.
13b. Disinfection type:
22. Certification:
Revised 2-22-2016
ft.NDEQ-US 17 COUNTRY STORE
TO DIAMETER THICKNESS MATERIAL
FROM17. SCREEN DIAMETER SLOT SIZE MATERIALTHICKNESS
FROM TO MATERIAL
ft.ft.
ft.
ft.
FROM TO
18. GROUT
MATERIAL
19. SAND/GRAVEL PACK (if applicable)
1. Well Contractor Information:
This form can be used for single or multiple wells
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:List all applicable well permits (i.e. County, State, Variance, Injection, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural
Non-Water Supply Well:
Monitoring
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Irrigation
15. INNER CASING OR TUBING (geothermal closed-loop)
Municipal/Public
Residential Water Supply (single)
ft.
ft.ft.
ft.ft.
ft.
ft.ft.
ft.
TO
EMPLACEMENT METHOD & AMOUNT
in.
in.
in.
EMPLACEMENT METHOD
Recovery
Injection Well:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of
this record has been provided to the well owner.
If this is a repair, fill out known well construction information and explain the nature ofthe repair under #21 remarks section or on the back of this form.
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
13a. Yield (gpm)
FOR WATER SUPPLY WELLS ONLY:
Method of test:
Amount:
For Internal Use ONLY:
14. WATER ZONES
FROM TO DESCRIPTION
FROM TO
24c. For Water Sypply & Injection Wells:Also submit one copy of this form within 30 days of completion of wellconstruction to the county health department of the county where constructed.
DIAMETER THICKNESS
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
21. REMARKS
20. DRILLING LOG (attach additional sheets if necessary)
5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees:
Signature of Certified Well Contractor Date
24a. For All Wells: Submit this form within 30 days of completion of wellconstruction to the following:
SUBMITTAL INSTRUCTIONS
Division of Water Resources, Information Processing Unit,1617 Mail Service Center, Raleigh, NC 27699-1617
Division of Water Resources, Underground Injection Control Program,1636 Mail Service Center, Raleigh, NC 27699-1636
16. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
North Carolina Department of Environment and Natural Resources - Division of Water Resources
24b. For Injection Wells ONLY: In addition to sending the form to theaddress in 24a above, also submit a copy of this form within 30 days ofcompletion of well construction to the following:
WELL CONSTRUCTION RECORD
23. Site diagram or additional well details:
Aquifer Recharge Groundwater Remediation
Stormwater Drainage
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling Return)
Salinity Barrier
Subsidence Control
Tracer
Other (explain under #21 Remarks)
4. Date Well(s) Completed:
5a. Well Location:SEE
ATTAC
H
E
D
Surface Pour
Surface Pour020
N/A
00-0-0000001670

NCDEQ; 38813_US 17 Country Store CATLIN Engineers and Scientists
CATLIN Project No. 220209 April 2023

APPENDIX E

LABORATORY ANALYTICAL REPORT AND
CHAIN OF CUSTODY DOCUMENT

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 5, 2023
Ben Ashba
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
Project Location: Elizabeth City, NC
Client Job Number:
Project Number: 220209
Laboratory Work Order Number: 23C3558
Enclosed are results of analyses for samples as received by the laboratory on March 31, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Page 1 of 30
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
23C3558-01 8
23C3558-02 10
23C3558-03 12
23C3558-04 14
23C3558-05 16
23C3558-06 18
Sample Preparation Information 20
QC Data 21
Volatile Organic Compounds by GC/MS 21
B335888 21
Flag/Qualifier Summary 25
Certifications 26
Chain of Custody/Sample Receipt 28
Page 2 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/5/2023
CATLIN Engineers & Scientists
220 Old Dairy Road
Wilmington, NC 28405
ATTN: Ben Ashba
220209
23C3558
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Elizabeth City, NC
230330-3
Trip Blank 23C3558-01 Ground Water SM21-23 6200B
MW-01 23C3558-02 Ground Water SM21-23 6200B
MW-02 23C3558-03 Ground Water SM21-23 6200B
MW-03 23C3558-04 Ground Water SM21-23 6200B
MW-04 23C3558-05 Ground Water SM21-23 6200B
TMW-01 23C3558-06 Ground Water SM21-23 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:23C3558-01Trip Blank
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C3558-02MW-01
DL
1,2,4-Trimethylbenzene 0.38 0.50 g/L SM21-23 6200BJ0.20
Benzene 4.1 0.50 g/L SM21-23 6200B0.18
Ethylbenzene 3.4 0.50 g/L SM21-23 6200B0.22
Isopropylbenzene (Cumene)0.81 0.50 g/L SM21-23 6200B0.15
Methyl tert-Butyl Ether (MTBE)4.9 0.50 g/L SM21-23 6200B0.17
n-Butylbenzene 0.25 0.50 g/L SM21-23 6200BJ0.15
n-Propylbenzene 1.0 0.50 g/L SM21-23 6200B0.12
sec-Butylbenzene 0.87 0.50 g/L SM21-23 6200B0.13
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C3558-03MW-02
DL
Isopropylbenzene (Cumene)0.72 1.0 g/L SM21-23 6200BJ0.30
n-Butylbenzene 0.82 1.0 g/L SM21-23 6200BJ0.30
n-Propylbenzene 0.98 1.0 g/L SM21-23 6200BJ0.25
sec-Butylbenzene 1.2 1.0 g/L SM21-23 6200B0.25
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C3558-04MW-03
DL
1,3,5-Trimethylbenzene 0.64 2.0 g/L SM21-23 6200BJ0.60
Benzene 2.1 2.0 g/L SM21-23 6200B0.74
Ethylbenzene 2.4 2.0 g/L SM21-23 6200B0.88
Isopropylbenzene (Cumene)1.9 2.0 g/L SM21-23 6200BJ0.60
Methyl tert-Butyl Ether (MTBE)5.1 2.0 g/L SM21-23 6200B0.68
n-Butylbenzene 0.60 2.0 g/L SM21-23 6200BJ0.60
n-Propylbenzene 3.4 2.0 g/L SM21-23 6200B0.50
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C3558-05MW-04
DL
1,2,4-Trimethylbenzene 35 5.0 g/L SM21-23 6200B2.0
2-Butanone (MEK)24 50 g/L SM21-23 6200BJ17
Benzene 780 5.0 g/L SM21-23 6200B1.8
Diisopropyl Ether (DIPE)13 5.0 g/L SM21-23 6200B2.0
Ethylbenzene 350 5.0 g/L SM21-23 6200B2.2
Isopropylbenzene (Cumene)83 5.0 g/L SM21-23 6200B1.5
m+p Xylene 30 10 g/L SM21-23 6200B4.9
Methyl tert-Butyl Ether (MTBE)430 5.0 g/L SM21-23 6200B1.7
Naphthalene 79 5.0 g/L SM21-23 6200BL-04 3.8
n-Butylbenzene 24 5.0 g/L SM21-23 6200B1.5
n-Propylbenzene 220 5.0 g/L SM21-23 6200B1.2
o-Xylene 2.5 5.0 g/L SM21-23 6200BJ2.4
sec-Butylbenzene 17 5.0 g/L SM21-23 6200B1.3
tert-Butylbenzene 2.3 5.0 g/L SM21-23 6200BJ1.4
Toluene 16 5.0 g/L SM21-23 6200B2.2
Page 5 of 30
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C3558-06TMW-01
DL
1,2,4-Trimethylbenzene 13 0.50 g/L SM21-23 6200B0.20
1,3,5-Trimethylbenzene 1.1 0.50 g/L SM21-23 6200B0.15
Acetone 12 50 g/L SM21-23 6200BJ2.0
Benzene 0.76 0.50 g/L SM21-23 6200B0.18
Ethylbenzene 3.8 0.50 g/L SM21-23 6200B0.22
Isopropylbenzene (Cumene)1.1 0.50 g/L SM21-23 6200B0.15
m+p Xylene 5.7 1.0 g/L SM21-23 6200B0.49
Methyl tert-Butyl Ether (MTBE)3.9 0.50 g/L SM21-23 6200B0.17
Naphthalene 1.4 0.50 g/L SM21-23 6200BL-04 0.38
n-Butylbenzene 1.4 0.50 g/L SM21-23 6200B0.15
n-Propylbenzene 2.5 0.50 g/L SM21-23 6200B0.12
o-Xylene 2.9 0.50 g/L SM21-23 6200B0.24
sec-Butylbenzene 0.55 0.50 g/L SM21-23 6200B0.13
Toluene 6.4 0.50 g/L SM21-23 6200B0.22
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 23C3558-03+04 due to matrix interference.
For method 6200B elevated reporting limits for sample 23C3558-05 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-23 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
4-Methyl-2-pentanone (MIBK)
23C3558-01[Trip Blank], 23C3558-02[MW-01], 23C3558-03[MW-02], 23C3558-04[MW-03], 23C3558-05[MW-04], 23C3558-06[TMW-01], B335888-BLK1,
B335888-BS1, B335888-BSD1, S085445-CCV1
Naphthalene
23C3558-01[Trip Blank], 23C3558-02[MW-01], 23C3558-03[MW-02], 23C3558-04[MW-03], 23C3558-05[MW-04], 23C3558-06[TMW-01], B335888-BLK1,
B335888-BS1, B335888-BSD1, S085445-CCV1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Bromomethane
B335888-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
23C3558-05[MW-04]
Elevated reporting limit due to matrix interference.
Analyte & Samples(s) Qualified:
RL-12
23C3558-03[MW-02], 23C3558-04[MW-03]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 7 of 30
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-01
Field Sample #: Trip Blank
Sample Matrix: Ground Water
Sampled: 3/29/2023 00:00
[TOC_2]23C3558-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/3/23 22:53 MFFg/L2.0 4/3/23SM21-23 6200B1Acetone
ND 0.50 4/3/23 22:53 MFFg/L0.18 4/3/23SM21-23 6200B1Benzene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B1Bromobenzene
ND 0.50 4/3/23 22:53 MFFg/L0.28 4/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 4/3/23 22:53 MFFg/L0.16 4/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 4/3/23 22:53 MFFg/L0.41 4/3/23SM21-23 6200B1Bromoform
ND 2.0 4/3/23 22:53 MFFg/L1.3 4/3/23SM21-23 6200B1Bromomethane
ND 5.0 4/3/23 22:53 MFFg/L1.7 4/3/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B1n-Butylbenzene
ND 0.50 4/3/23 22:53 MFFg/L0.13 4/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 4/3/23 22:53 MFFg/L0.16 4/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 4/3/23 22:53 MFFg/L0.12 4/3/23SM21-23 6200B1Chlorobenzene
ND 50 4/3/23 22:53 MFFg/L20 4/3/23SM21-23 6200B1Ethanol
ND 0.50 4/3/23 22:53 MFFg/L0.20 4/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 4/3/23 22:53 MFFg/L0.34 4/3/23SM21-23 6200B1Chloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B1Chloroform
ND 0.60 4/3/23 22:53 MFFg/L0.50 4/3/23SM21-23 6200B1Chloromethane
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 4/3/23 22:53 MFFg/L0.16 4/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/3/23 22:53 MFFg/L0.13 4/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 4/3/23 22:53 MFFg/L0.13 4/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 4/3/23 22:53 MFFg/L0.16 4/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.30 4/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/3/23 22:53 MFFg/L0.17 4/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/3/23 22:53 MFFg/L0.19 4/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 4/3/23 22:53 MFFg/L0.12 4/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 4/3/23 22:53 MFFg/L0.35 4/3/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 4/3/23 22:53 MFFg/L0.16 4/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 4/3/23 22:53 MFFg/L0.20 4/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 4/3/23 22:53 MFFg/L0.22 4/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 4/3/23 22:53 MFFg/L1.2 4/3/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/3/23 22:53 MFFg/L0.13 4/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 4/3/23 22:53 MFFg/L0.17 4/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/3/23 22:53 MFFg/L0.18 4/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 4/3/23 22:53 MFFg/L1.3 4/3/23SM21-23 6200B1L-044-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 8 of 30
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-01
Field Sample #: Trip Blank
Sample Matrix: Ground Water
Sampled: 3/29/2023 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/3/23 22:53 MFFg/L0.38 4/3/23SM21-23 6200B1L-04Naphthalene
ND 0.50 4/3/23 22:53 MFFg/L0.12 4/3/23SM21-23 6200B1n-Propylbenzene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B1Styrene
ND 0.50 4/3/23 22:53 MFFg/L0.14 4/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.17 4/3/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 4/3/23 22:53 MFFg/L0.22 4/3/23SM21-23 6200B1Toluene
ND 1.0 4/3/23 22:53 MFFg/L0.34 4/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 1.0 4/3/23 22:53 MFFg/L0.30 4/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.19 4/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 4/3/23 22:53 MFFg/L0.17 4/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/3/23 22:53 MFFg/L0.28 4/3/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 4/3/23 22:53 MFFg/L0.20 4/3/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 4/3/23 22:53 MFFg/L0.15 4/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 4/3/23 22:53 MFFg/L1.7 4/3/23SM21-23 6200B1Vinyl Acetate
ND 0.50 4/3/23 22:53 MFFg/L0.24 4/3/23SM21-23 6200B1Vinyl Chloride
ND 1.0 4/3/23 22:53 MFFg/L0.49 4/3/23SM21-23 6200B1m+p Xylene
ND 0.50 4/3/23 22:53 MFFg/L0.24 4/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 4/3/23 22:5370-130
Toluene-d8 99.0 4/3/23 22:5370-130
4-Bromofluorobenzene 88.9 4/3/23 22:5370-130
Page 9 of 30
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-02
Field Sample #: MW-01
Sample Matrix: Ground Water
Sampled: 3/29/2023 15:20
[TOC_2]23C3558-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 4/4/23 5:42 MFFg/L2.0 4/3/23SM21-23 6200B1Acetone
4.1 0.50 4/4/23 5:42 MFFg/L0.18 4/3/23SM21-23 6200B1Benzene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B1Bromobenzene
ND 0.50 4/4/23 5:42 MFFg/L0.28 4/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 4/4/23 5:42 MFFg/L0.16 4/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 4/4/23 5:42 MFFg/L0.41 4/3/23SM21-23 6200B1Bromoform
ND 2.0 4/4/23 5:42 MFFg/L1.3 4/3/23SM21-23 6200B1Bromomethane
ND 5.0 4/4/23 5:42 MFFg/L1.7 4/3/23SM21-23 6200B12-Butanone (MEK)
0.25 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B1Jn-Butylbenzene
0.87 0.50 4/4/23 5:42 MFFg/L0.13 4/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 4/4/23 5:42 MFFg/L0.16 4/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 4/4/23 5:42 MFFg/L0.12 4/3/23SM21-23 6200B1Chlorobenzene
ND 50 4/4/23 5:42 MFFg/L20 4/3/23SM21-23 6200B1Ethanol
ND 0.50 4/4/23 5:42 MFFg/L0.20 4/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 4/4/23 5:42 MFFg/L0.34 4/3/23SM21-23 6200B1Chloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B1Chloroform
ND 0.60 4/4/23 5:42 MFFg/L0.50 4/3/23SM21-23 6200B1Chloromethane
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 4/4/23 5:42 MFFg/L0.16 4/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/4/23 5:42 MFFg/L0.13 4/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 4/4/23 5:42 MFFg/L0.13 4/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 4/4/23 5:42 MFFg/L0.16 4/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.30 4/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/4/23 5:42 MFFg/L0.17 4/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/4/23 5:42 MFFg/L0.19 4/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 4/4/23 5:42 MFFg/L0.12 4/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 4/4/23 5:42 MFFg/L0.35 4/3/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 4/4/23 5:42 MFFg/L0.16 4/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 4/4/23 5:42 MFFg/L0.20 4/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
3.4 0.50 4/4/23 5:42 MFFg/L0.22 4/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 4/4/23 5:42 MFFg/L1.2 4/3/23SM21-23 6200B12-Hexanone (MBK)
0.81 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/4/23 5:42 MFFg/L0.13 4/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
4.9 0.50 4/4/23 5:42 MFFg/L0.17 4/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/4/23 5:42 MFFg/L0.18 4/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 4/4/23 5:42 MFFg/L1.3 4/3/23SM21-23 6200B1L-044-Methyl-2-pentanone (MIBK)
Page 10 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-02
Field Sample #: MW-01
Sample Matrix: Ground Water
Sampled: 3/29/2023 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 4/4/23 5:42 MFFg/L0.38 4/3/23SM21-23 6200B1L-04Naphthalene
1.0 0.50 4/4/23 5:42 MFFg/L0.12 4/3/23SM21-23 6200B1n-Propylbenzene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B1Styrene
ND 0.50 4/4/23 5:42 MFFg/L0.14 4/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.17 4/3/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 4/4/23 5:42 MFFg/L0.22 4/3/23SM21-23 6200B1Toluene
ND 1.0 4/4/23 5:42 MFFg/L0.34 4/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 1.0 4/4/23 5:42 MFFg/L0.30 4/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.19 4/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 4/4/23 5:42 MFFg/L0.17 4/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/4/23 5:42 MFFg/L0.28 4/3/23SM21-23 6200B11,2,3-Trichloropropane
0.38 0.50 4/4/23 5:42 MFFg/L0.20 4/3/23SM21-23 6200B1J1,2,4-Trimethylbenzene
ND 0.50 4/4/23 5:42 MFFg/L0.15 4/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 4/4/23 5:42 MFFg/L1.7 4/3/23SM21-23 6200B1Vinyl Acetate
ND 0.50 4/4/23 5:42 MFFg/L0.24 4/3/23SM21-23 6200B1Vinyl Chloride
ND 1.0 4/4/23 5:42 MFFg/L0.49 4/3/23SM21-23 6200B1m+p Xylene
ND 0.50 4/4/23 5:42 MFFg/L0.24 4/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 4/4/23 5:4270-130
Toluene-d8 98.0 4/4/23 5:4270-130
4-Bromofluorobenzene 89.4 4/4/23 5:4270-130
Page 11 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-03
Field Sample #: MW-02
Sample Matrix: Ground Water
Sampled: 3/29/2023 16:01
[TOC_2]23C3558-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-12 Volatile Organic Compounds by GC/MS
ND 100 4/4/23 6:09 MFFg/L4.0 4/3/23SM21-23 6200B2Acetone
ND 1.0 4/4/23 6:09 MFFg/L0.37 4/3/23SM21-23 6200B2Benzene
ND 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B2Bromobenzene
ND 1.0 4/4/23 6:09 MFFg/L0.57 4/3/23SM21-23 6200B2Bromochloromethane
ND 1.0 4/4/23 6:09 MFFg/L0.32 4/3/23SM21-23 6200B2Bromodichloromethane
ND 1.0 4/4/23 6:09 MFFg/L0.82 4/3/23SM21-23 6200B2Bromoform
ND 4.0 4/4/23 6:09 MFFg/L2.6 4/3/23SM21-23 6200B2Bromomethane
ND 10 4/4/23 6:09 MFFg/L3.4 4/3/23SM21-23 6200B22-Butanone (MEK)
0.82 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B2Jn-Butylbenzene
1.2 1.0 4/4/23 6:09 MFFg/L0.25 4/3/23SM21-23 6200B2sec-Butylbenzene
ND 1.0 4/4/23 6:09 MFFg/L0.28 4/3/23SM21-23 6200B2tert-Butylbenzene
ND 1.0 4/4/23 6:09 MFFg/L0.33 4/3/23SM21-23 6200B2Carbon Tetrachloride
ND 1.0 4/4/23 6:09 MFFg/L0.24 4/3/23SM21-23 6200B2Chlorobenzene
ND 100 4/4/23 6:09 MFFg/L41 4/3/23SM21-23 6200B2Ethanol
ND 1.0 4/4/23 6:09 MFFg/L0.40 4/3/23SM21-23 6200B2Chlorodibromomethane
ND 1.0 4/4/23 6:09 MFFg/L0.68 4/3/23SM21-23 6200B2Chloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.28 4/3/23SM21-23 6200B2Chloroform
ND 1.2 4/4/23 6:09 MFFg/L1.0 4/3/23SM21-23 6200B2Chloromethane
ND 1.0 4/4/23 6:09 MFFg/L0.31 4/3/23SM21-23 6200B22-Chlorotoluene
ND 1.0 4/4/23 6:09 MFFg/L0.31 4/3/23SM21-23 6200B24-Chlorotoluene
ND 1.0 4/4/23 6:09 MFFg/L0.32 4/3/23SM21-23 6200B21,2-Dibromoethane (EDB)
ND 1.0 4/4/23 6:09 MFFg/L0.26 4/3/23SM21-23 6200B21,2-Dichlorobenzene
ND 1.0 4/4/23 6:09 MFFg/L0.27 4/3/23SM21-23 6200B21,3-Dichlorobenzene
ND 1.0 4/4/23 6:09 MFFg/L0.26 4/3/23SM21-23 6200B21,4-Dichlorobenzene
ND 1.0 4/4/23 6:09 MFFg/L0.32 4/3/23SM21-23 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 4/4/23 6:09 MFFg/L0.27 4/3/23SM21-23 6200B21,1-Dichloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.61 4/3/23SM21-23 6200B21,2-Dichloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.28 4/3/23SM21-23 6200B21,1-Dichloroethylene
ND 1.0 4/4/23 6:09 MFFg/L0.28 4/3/23SM21-23 6200B2cis-1,2-Dichloroethylene
ND 1.0 4/4/23 6:09 MFFg/L0.34 4/3/23SM21-23 6200B2trans-1,2-Dichloroethylene
ND 1.0 4/4/23 6:09 MFFg/L0.39 4/3/23SM21-23 6200B21,2-Dichloropropane
ND 1.0 4/4/23 6:09 MFFg/L0.23 4/3/23SM21-23 6200B21,3-Dichloropropane
ND 1.0 4/4/23 6:09 MFFg/L0.70 4/3/23SM21-23 6200B22,2-Dichloropropane
ND 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B21,1-Dichloropropene
ND 1.0 4/4/23 6:09 MFFg/L0.33 4/3/23SM21-23 6200B2cis-1,3-Dichloropropene
ND 1.0 4/4/23 6:09 MFFg/L0.28 4/3/23SM21-23 6200B2trans-1,3-Dichloropropene
ND 1.0 4/4/23 6:09 MFFg/L0.40 4/3/23SM21-23 6200B2Diisopropyl Ether (DIPE)
ND 1.0 4/4/23 6:09 MFFg/L0.44 4/3/23SM21-23 6200B2Ethylbenzene
ND 10 4/4/23 6:09 MFFg/L2.4 4/3/23SM21-23 6200B22-Hexanone (MBK)
0.72 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B2JIsopropylbenzene (Cumene)
ND 1.0 4/4/23 6:09 MFFg/L0.25 4/3/23SM21-23 6200B2p-Isopropyltoluene (p-Cymene)
ND 1.0 4/4/23 6:09 MFFg/L0.34 4/3/23SM21-23 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 4/4/23 6:09 MFFg/L0.35 4/3/23SM21-23 6200B2Methylene Chloride
ND 10 4/4/23 6:09 MFFg/L2.6 4/3/23SM21-23 6200B2L-044-Methyl-2-pentanone (MIBK)
Page 12 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-03
Field Sample #: MW-02
Sample Matrix: Ground Water
Sampled: 3/29/2023 16:01
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-12 Volatile Organic Compounds by GC/MS
ND 1.0 4/4/23 6:09 MFFg/L0.76 4/3/23SM21-23 6200B2L-04Naphthalene
0.98 1.0 4/4/23 6:09 MFFg/L0.25 4/3/23SM21-23 6200B2Jn-Propylbenzene
ND 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B2Styrene
ND 1.0 4/4/23 6:09 MFFg/L0.27 4/3/23SM21-23 6200B21,1,2,2-Tetrachloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.34 4/3/23SM21-23 6200B2Tetrachloroethylene
ND 1.0 4/4/23 6:09 MFFg/L0.45 4/3/23SM21-23 6200B2Toluene
ND 2.0 4/4/23 6:09 MFFg/L0.68 4/3/23SM21-23 6200B21,2,3-Trichlorobenzene
ND 2.0 4/4/23 6:09 MFFg/L0.60 4/3/23SM21-23 6200B21,2,4-Trichlorobenzene
ND 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B21,1,1-Trichloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.38 4/3/23SM21-23 6200B21,1,2-Trichloroethane
ND 1.0 4/4/23 6:09 MFFg/L0.35 4/3/23SM21-23 6200B2Trichloroethylene
ND 1.0 4/4/23 6:09 MFFg/L0.31 4/3/23SM21-23 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 4/4/23 6:09 MFFg/L0.55 4/3/23SM21-23 6200B21,2,3-Trichloropropane
ND 1.0 4/4/23 6:09 MFFg/L0.40 4/3/23SM21-23 6200B21,2,4-Trimethylbenzene
ND 1.0 4/4/23 6:09 MFFg/L0.30 4/3/23SM21-23 6200B21,3,5-Trimethylbenzene
ND 40 4/4/23 6:09 MFFg/L3.3 4/3/23SM21-23 6200B2Vinyl Acetate
ND 1.0 4/4/23 6:09 MFFg/L0.47 4/3/23SM21-23 6200B2Vinyl Chloride
ND 2.0 4/4/23 6:09 MFFg/L0.98 4/3/23SM21-23 6200B2m+p Xylene
ND 1.0 4/4/23 6:09 MFFg/L0.49 4/3/23SM21-23 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 110 4/4/23 6:0970-130
Toluene-d8 99.3 4/4/23 6:0970-130
4-Bromofluorobenzene 91.0 4/4/23 6:0970-130
Page 13 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-04
Field Sample #: MW-03
Sample Matrix: Ground Water
Sampled: 3/29/2023 14:00
[TOC_2]23C3558-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-12 Volatile Organic Compounds by GC/MS
ND 200 4/4/23 6:37 MFFg/L8.0 4/3/23SM21-23 6200B4Acetone
2.1 2.0 4/4/23 6:37 MFFg/L0.74 4/3/23SM21-23 6200B4Benzene
ND 2.0 4/4/23 6:37 MFFg/L0.59 4/3/23SM21-23 6200B4Bromobenzene
ND 2.0 4/4/23 6:37 MFFg/L1.1 4/3/23SM21-23 6200B4Bromochloromethane
ND 2.0 4/4/23 6:37 MFFg/L0.63 4/3/23SM21-23 6200B4Bromodichloromethane
ND 2.0 4/4/23 6:37 MFFg/L1.6 4/3/23SM21-23 6200B4Bromoform
ND 8.0 4/4/23 6:37 MFFg/L5.3 4/3/23SM21-23 6200B4Bromomethane
ND 20 4/4/23 6:37 MFFg/L6.7 4/3/23SM21-23 6200B42-Butanone (MEK)
0.60 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B4Jn-Butylbenzene
ND 2.0 4/4/23 6:37 MFFg/L0.51 4/3/23SM21-23 6200B4sec-Butylbenzene
ND 2.0 4/4/23 6:37 MFFg/L0.57 4/3/23SM21-23 6200B4tert-Butylbenzene
ND 2.0 4/4/23 6:37 MFFg/L0.65 4/3/23SM21-23 6200B4Carbon Tetrachloride
ND 2.0 4/4/23 6:37 MFFg/L0.48 4/3/23SM21-23 6200B4Chlorobenzene
ND 200 4/4/23 6:37 MFFg/L81 4/3/23SM21-23 6200B4Ethanol
ND 2.0 4/4/23 6:37 MFFg/L0.80 4/3/23SM21-23 6200B4Chlorodibromomethane
ND 2.0 4/4/23 6:37 MFFg/L1.4 4/3/23SM21-23 6200B4Chloroethane
ND 2.0 4/4/23 6:37 MFFg/L0.56 4/3/23SM21-23 6200B4Chloroform
ND 2.4 4/4/23 6:37 MFFg/L2.0 4/3/23SM21-23 6200B4Chloromethane
ND 2.0 4/4/23 6:37 MFFg/L0.62 4/3/23SM21-23 6200B42-Chlorotoluene
ND 2.0 4/4/23 6:37 MFFg/L0.62 4/3/23SM21-23 6200B44-Chlorotoluene
ND 2.0 4/4/23 6:37 MFFg/L0.64 4/3/23SM21-23 6200B41,2-Dibromoethane (EDB)
ND 2.0 4/4/23 6:37 MFFg/L0.52 4/3/23SM21-23 6200B41,2-Dichlorobenzene
ND 2.0 4/4/23 6:37 MFFg/L0.55 4/3/23SM21-23 6200B41,3-Dichlorobenzene
ND 2.0 4/4/23 6:37 MFFg/L0.51 4/3/23SM21-23 6200B41,4-Dichlorobenzene
ND 2.0 4/4/23 6:37 MFFg/L0.64 4/3/23SM21-23 6200B4Dichlorodifluoromethane (Freon 12)
ND 2.0 4/4/23 6:37 MFFg/L0.55 4/3/23SM21-23 6200B41,1-Dichloroethane
ND 2.0 4/4/23 6:37 MFFg/L1.2 4/3/23SM21-23 6200B41,2-Dichloroethane
ND 2.0 4/4/23 6:37 MFFg/L0.56 4/3/23SM21-23 6200B41,1-Dichloroethylene
ND 2.0 4/4/23 6:37 MFFg/L0.56 4/3/23SM21-23 6200B4cis-1,2-Dichloroethylene
ND 2.0 4/4/23 6:37 MFFg/L0.69 4/3/23SM21-23 6200B4trans-1,2-Dichloroethylene
ND 2.0 4/4/23 6:37 MFFg/L0.77 4/3/23SM21-23 6200B41,2-Dichloropropane
ND 2.0 4/4/23 6:37 MFFg/L0.46 4/3/23SM21-23 6200B41,3-Dichloropropane
ND 2.0 4/4/23 6:37 MFFg/L1.4 4/3/23SM21-23 6200B42,2-Dichloropropane
ND 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B41,1-Dichloropropene
ND 2.0 4/4/23 6:37 MFFg/L0.65 4/3/23SM21-23 6200B4cis-1,3-Dichloropropene
ND 2.0 4/4/23 6:37 MFFg/L0.57 4/3/23SM21-23 6200B4trans-1,3-Dichloropropene
ND 2.0 4/4/23 6:37 MFFg/L0.81 4/3/23SM21-23 6200B4Diisopropyl Ether (DIPE)
2.4 2.0 4/4/23 6:37 MFFg/L0.88 4/3/23SM21-23 6200B4Ethylbenzene
ND 20 4/4/23 6:37 MFFg/L4.8 4/3/23SM21-23 6200B42-Hexanone (MBK)
1.9 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B4JIsopropylbenzene (Cumene)
ND 2.0 4/4/23 6:37 MFFg/L0.51 4/3/23SM21-23 6200B4p-Isopropyltoluene (p-Cymene)
5.1 2.0 4/4/23 6:37 MFFg/L0.68 4/3/23SM21-23 6200B4Methyl tert-Butyl Ether (MTBE)
ND 20 4/4/23 6:37 MFFg/L0.71 4/3/23SM21-23 6200B4Methylene Chloride
ND 20 4/4/23 6:37 MFFg/L5.3 4/3/23SM21-23 6200B4L-044-Methyl-2-pentanone (MIBK)
Page 14 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-04
Field Sample #: MW-03
Sample Matrix: Ground Water
Sampled: 3/29/2023 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-12 Volatile Organic Compounds by GC/MS
ND 2.0 4/4/23 6:37 MFFg/L1.5 4/3/23SM21-23 6200B4L-04Naphthalene
3.4 2.0 4/4/23 6:37 MFFg/L0.50 4/3/23SM21-23 6200B4n-Propylbenzene
ND 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B4Styrene
ND 2.0 4/4/23 6:37 MFFg/L0.55 4/3/23SM21-23 6200B41,1,2,2-Tetrachloroethane
ND 2.0 4/4/23 6:37 MFFg/L0.67 4/3/23SM21-23 6200B4Tetrachloroethylene
ND 2.0 4/4/23 6:37 MFFg/L0.89 4/3/23SM21-23 6200B4Toluene
ND 4.0 4/4/23 6:37 MFFg/L1.4 4/3/23SM21-23 6200B41,2,3-Trichlorobenzene
ND 4.0 4/4/23 6:37 MFFg/L1.2 4/3/23SM21-23 6200B41,2,4-Trichlorobenzene
ND 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B41,1,1-Trichloroethane
ND 2.0 4/4/23 6:37 MFFg/L0.76 4/3/23SM21-23 6200B41,1,2-Trichloroethane
ND 2.0 4/4/23 6:37 MFFg/L0.70 4/3/23SM21-23 6200B4Trichloroethylene
ND 2.0 4/4/23 6:37 MFFg/L0.62 4/3/23SM21-23 6200B4Trichlorofluoromethane (Freon 11)
ND 2.0 4/4/23 6:37 MFFg/L1.1 4/3/23SM21-23 6200B41,2,3-Trichloropropane
ND 2.0 4/4/23 6:37 MFFg/L0.80 4/3/23SM21-23 6200B41,2,4-Trimethylbenzene
0.64 2.0 4/4/23 6:37 MFFg/L0.60 4/3/23SM21-23 6200B4J1,3,5-Trimethylbenzene
ND 80 4/4/23 6:37 MFFg/L6.7 4/3/23SM21-23 6200B4Vinyl Acetate
ND 2.0 4/4/23 6:37 MFFg/L0.95 4/3/23SM21-23 6200B4Vinyl Chloride
ND 4.0 4/4/23 6:37 MFFg/L2.0 4/3/23SM21-23 6200B4m+p Xylene
ND 2.0 4/4/23 6:37 MFFg/L0.97 4/3/23SM21-23 6200B4o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 4/4/23 6:3770-130
Toluene-d8 99.9 4/4/23 6:3770-130
4-Bromofluorobenzene 89.8 4/4/23 6:3770-130
Page 15 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-05
Field Sample #: MW-04
Sample Matrix: Ground Water
Sampled: 3/29/2023 14:58
[TOC_2]23C3558-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 4/4/23 7:04 MFFg/L20 4/3/23SM21-23 6200B10Acetone
780 5.0 4/4/23 7:04 MFFg/L1.8 4/3/23SM21-23 6200B10Benzene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B10Bromobenzene
ND 5.0 4/4/23 7:04 MFFg/L2.8 4/3/23SM21-23 6200B10Bromochloromethane
ND 5.0 4/4/23 7:04 MFFg/L1.6 4/3/23SM21-23 6200B10Bromodichloromethane
ND 5.0 4/4/23 7:04 MFFg/L4.1 4/3/23SM21-23 6200B10Bromoform
ND 20 4/4/23 7:04 MFFg/L13 4/3/23SM21-23 6200B10Bromomethane
24 50 4/4/23 7:04 MFFg/L17 4/3/23SM21-23 6200B10J2-Butanone (MEK)
24 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B10n-Butylbenzene
17 5.0 4/4/23 7:04 MFFg/L1.3 4/3/23SM21-23 6200B10sec-Butylbenzene
2.3 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B10Jtert-Butylbenzene
ND 5.0 4/4/23 7:04 MFFg/L1.6 4/3/23SM21-23 6200B10Carbon Tetrachloride
ND 5.0 4/4/23 7:04 MFFg/L1.2 4/3/23SM21-23 6200B10Chlorobenzene
ND 500 4/4/23 7:04 MFFg/L200 4/3/23SM21-23 6200B10Ethanol
ND 5.0 4/4/23 7:04 MFFg/L2.0 4/3/23SM21-23 6200B10Chlorodibromomethane
ND 5.0 4/4/23 7:04 MFFg/L3.4 4/3/23SM21-23 6200B10Chloroethane
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B10Chloroform
ND 6.0 4/4/23 7:04 MFFg/L5.0 4/3/23SM21-23 6200B10Chloromethane
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B102-Chlorotoluene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B104-Chlorotoluene
ND 5.0 4/4/23 7:04 MFFg/L1.6 4/3/23SM21-23 6200B101,2-Dibromoethane (EDB)
ND 5.0 4/4/23 7:04 MFFg/L1.3 4/3/23SM21-23 6200B101,2-Dichlorobenzene
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B101,3-Dichlorobenzene
ND 5.0 4/4/23 7:04 MFFg/L1.3 4/3/23SM21-23 6200B101,4-Dichlorobenzene
ND 5.0 4/4/23 7:04 MFFg/L1.6 4/3/23SM21-23 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B101,1-Dichloroethane
ND 5.0 4/4/23 7:04 MFFg/L3.0 4/3/23SM21-23 6200B101,2-Dichloroethane
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B101,1-Dichloroethylene
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B10cis-1,2-Dichloroethylene
ND 5.0 4/4/23 7:04 MFFg/L1.7 4/3/23SM21-23 6200B10trans-1,2-Dichloroethylene
ND 5.0 4/4/23 7:04 MFFg/L1.9 4/3/23SM21-23 6200B101,2-Dichloropropane
ND 5.0 4/4/23 7:04 MFFg/L1.2 4/3/23SM21-23 6200B101,3-Dichloropropane
ND 5.0 4/4/23 7:04 MFFg/L3.5 4/3/23SM21-23 6200B102,2-Dichloropropane
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B101,1-Dichloropropene
ND 5.0 4/4/23 7:04 MFFg/L1.6 4/3/23SM21-23 6200B10cis-1,3-Dichloropropene
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B10trans-1,3-Dichloropropene
13 5.0 4/4/23 7:04 MFFg/L2.0 4/3/23SM21-23 6200B10Diisopropyl Ether (DIPE)
350 5.0 4/4/23 7:04 MFFg/L2.2 4/3/23SM21-23 6200B10Ethylbenzene
ND 50 4/4/23 7:04 MFFg/L12 4/3/23SM21-23 6200B102-Hexanone (MBK)
83 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B10Isopropylbenzene (Cumene)
ND 5.0 4/4/23 7:04 MFFg/L1.3 4/3/23SM21-23 6200B10p-Isopropyltoluene (p-Cymene)
430 5.0 4/4/23 7:04 MFFg/L1.7 4/3/23SM21-23 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 4/4/23 7:04 MFFg/L1.8 4/3/23SM21-23 6200B10Methylene Chloride
ND 50 4/4/23 7:04 MFFg/L13 4/3/23SM21-23 6200B10L-044-Methyl-2-pentanone (MIBK)
Page 16 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-05
Field Sample #: MW-04
Sample Matrix: Ground Water
Sampled: 3/29/2023 14:58
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
79 5.0 4/4/23 7:04 MFFg/L3.8 4/3/23SM21-23 6200B10L-04Naphthalene
220 5.0 4/4/23 7:04 MFFg/L1.2 4/3/23SM21-23 6200B10n-Propylbenzene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B10Styrene
ND 5.0 4/4/23 7:04 MFFg/L1.4 4/3/23SM21-23 6200B101,1,2,2-Tetrachloroethane
ND 5.0 4/4/23 7:04 MFFg/L1.7 4/3/23SM21-23 6200B10Tetrachloroethylene
16 5.0 4/4/23 7:04 MFFg/L2.2 4/3/23SM21-23 6200B10Toluene
ND 10 4/4/23 7:04 MFFg/L3.4 4/3/23SM21-23 6200B101,2,3-Trichlorobenzene
ND 10 4/4/23 7:04 MFFg/L3.0 4/3/23SM21-23 6200B101,2,4-Trichlorobenzene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B101,1,1-Trichloroethane
ND 5.0 4/4/23 7:04 MFFg/L1.9 4/3/23SM21-23 6200B101,1,2-Trichloroethane
ND 5.0 4/4/23 7:04 MFFg/L1.7 4/3/23SM21-23 6200B10Trichloroethylene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 4/4/23 7:04 MFFg/L2.8 4/3/23SM21-23 6200B101,2,3-Trichloropropane
35 5.0 4/4/23 7:04 MFFg/L2.0 4/3/23SM21-23 6200B101,2,4-Trimethylbenzene
ND 5.0 4/4/23 7:04 MFFg/L1.5 4/3/23SM21-23 6200B101,3,5-Trimethylbenzene
ND 200 4/4/23 7:04 MFFg/L17 4/3/23SM21-23 6200B10Vinyl Acetate
ND 5.0 4/4/23 7:04 MFFg/L2.4 4/3/23SM21-23 6200B10Vinyl Chloride
30 10 4/4/23 7:04 MFFg/L4.9 4/3/23SM21-23 6200B10m+p Xylene
2.5 5.0 4/4/23 7:04 MFFg/L2.4 4/3/23SM21-23 6200B10Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 4/4/23 7:0470-130
Toluene-d8 98.4 4/4/23 7:0470-130
4-Bromofluorobenzene 90.4 4/4/23 7:0470-130
Page 17 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-06
Field Sample #: TMW-01
Sample Matrix: Ground Water
Sampled: 3/29/2023 15:47
[TOC_2]23C3558-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
12 50 4/4/23 0:15 MFFg/L2.0 4/3/23SM21-23 6200B1JAcetone
0.76 0.50 4/4/23 0:15 MFFg/L0.18 4/3/23SM21-23 6200B1Benzene
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B1Bromobenzene
ND 0.50 4/4/23 0:15 MFFg/L0.28 4/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 4/4/23 0:15 MFFg/L0.16 4/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 4/4/23 0:15 MFFg/L0.41 4/3/23SM21-23 6200B1Bromoform
ND 2.0 4/4/23 0:15 MFFg/L1.3 4/3/23SM21-23 6200B1Bromomethane
ND 5.0 4/4/23 0:15 MFFg/L1.7 4/3/23SM21-23 6200B12-Butanone (MEK)
1.4 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B1n-Butylbenzene
0.55 0.50 4/4/23 0:15 MFFg/L0.13 4/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 4/4/23 0:15 MFFg/L0.16 4/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 4/4/23 0:15 MFFg/L0.12 4/3/23SM21-23 6200B1Chlorobenzene
ND 50 4/4/23 0:15 MFFg/L20 4/3/23SM21-23 6200B1Ethanol
ND 0.50 4/4/23 0:15 MFFg/L0.20 4/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 4/4/23 0:15 MFFg/L0.34 4/3/23SM21-23 6200B1Chloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B1Chloroform
ND 0.60 4/4/23 0:15 MFFg/L0.50 4/3/23SM21-23 6200B1Chloromethane
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 4/4/23 0:15 MFFg/L0.16 4/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 4/4/23 0:15 MFFg/L0.13 4/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 4/4/23 0:15 MFFg/L0.13 4/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 4/4/23 0:15 MFFg/L0.16 4/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.30 4/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 4/4/23 0:15 MFFg/L0.17 4/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 4/4/23 0:15 MFFg/L0.19 4/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 4/4/23 0:15 MFFg/L0.12 4/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 4/4/23 0:15 MFFg/L0.35 4/3/23SM21-23 6200B12,2-Dichloropropane
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 4/4/23 0:15 MFFg/L0.16 4/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 4/4/23 0:15 MFFg/L0.20 4/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
3.8 0.50 4/4/23 0:15 MFFg/L0.22 4/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 4/4/23 0:15 MFFg/L1.2 4/3/23SM21-23 6200B12-Hexanone (MBK)
1.1 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 4/4/23 0:15 MFFg/L0.13 4/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
3.9 0.50 4/4/23 0:15 MFFg/L0.17 4/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 4/4/23 0:15 MFFg/L0.18 4/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 4/4/23 0:15 MFFg/L1.3 4/3/23SM21-23 6200B1L-044-Methyl-2-pentanone (MIBK)
Page 18 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/31/2023
Work Order: 23C3558Sample Description:Project Location: Elizabeth City, NC
Sample ID: 23C3558-06
Field Sample #: TMW-01
Sample Matrix: Ground Water
Sampled: 3/29/2023 15:47
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
1.4 0.50 4/4/23 0:15 MFFg/L0.38 4/3/23SM21-23 6200B1L-04Naphthalene
2.5 0.50 4/4/23 0:15 MFFg/L0.12 4/3/23SM21-23 6200B1n-Propylbenzene
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B1Styrene
ND 0.50 4/4/23 0:15 MFFg/L0.14 4/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.17 4/3/23SM21-23 6200B1Tetrachloroethylene
6.4 0.50 4/4/23 0:15 MFFg/L0.22 4/3/23SM21-23 6200B1Toluene
ND 1.0 4/4/23 0:15 MFFg/L0.34 4/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 1.0 4/4/23 0:15 MFFg/L0.30 4/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.19 4/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 4/4/23 0:15 MFFg/L0.17 4/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 4/4/23 0:15 MFFg/L0.28 4/3/23SM21-23 6200B11,2,3-Trichloropropane
13 0.50 4/4/23 0:15 MFFg/L0.20 4/3/23SM21-23 6200B11,2,4-Trimethylbenzene
1.1 0.50 4/4/23 0:15 MFFg/L0.15 4/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 4/4/23 0:15 MFFg/L1.7 4/3/23SM21-23 6200B1Vinyl Acetate
ND 0.50 4/4/23 0:15 MFFg/L0.24 4/3/23SM21-23 6200B1Vinyl Chloride
5.7 1.0 4/4/23 0:15 MFFg/L0.49 4/3/23SM21-23 6200B1m+p Xylene
2.9 0.50 4/4/23 0:15 MFFg/L0.24 4/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 4/4/23 0:1570-130
Toluene-d8 99.3 4/4/23 0:1570-130
4-Bromofluorobenzene 86.7 4/4/23 0:1570-130
Page 19 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B335888 04/03/235 5.0023C3558-01 [Trip Blank]
B335888 04/03/235 5.0023C3558-02 [MW-01]
B335888 04/03/232.5 5.0023C3558-03 [MW-02]
B335888 04/03/231.25 5.0023C3558-04 [MW-03]
B335888 04/03/230.5 5.0023C3558-05 [MW-04]
B335888 04/03/235 5.0023C3558-06 [TMW-01]
[TOC_1]Sample Preparation Information[TOC]
Page 20 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B335888 - SW-846 5030B
[TOC_3]B335888[TOC]
Blank (B335888-BLK1) Prepared & Analyzed: 04/03/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0 L-04ND
Naphthalene g/L0.50 L-04ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 21 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B335888 - SW-846 5030B
Blank (B335888-BLK1) Prepared & Analyzed: 04/03/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10726.8
g/L 25.0 70-130Surrogate: Toluene-d8 10425.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 86.721.7
LCS (B335888-BS1) Prepared & Analyzed: 04/03/23
Acetone g/L50 100 70-130114114
Benzene g/L0.50 10.0 70-13096.89.68
Bromobenzene g/L0.50 10.0 70-13090.09.00
Bromochloromethane g/L0.50 10.0 70-13010610.6
Bromodichloromethane g/L0.50 10.0 70-13097.29.72
Bromoform g/L0.50 10.0 70-13087.48.74
Bromomethane g/L2.0 10.0 60-14014014.0
2-Butanone (MEK)g/L5.0 100 70-130104104
n-Butylbenzene g/L0.50 10.0 70-13083.88.38
sec-Butylbenzene g/L0.50 10.0 70-13089.18.91
tert-Butylbenzene g/L0.50 10.0 70-13092.89.28
Carbon Tetrachloride g/L0.50 10.0 70-13089.98.99
Chlorobenzene g/L0.50 10.0 70-13095.89.58
Ethanol g/L50 100 70-13091.891.8
Chlorodibromomethane g/L0.50 10.0 70-13089.48.94
Chloroethane g/L0.50 10.0 60-14093.39.33
Chloroform g/L0.50 10.0 70-13095.19.51
Chloromethane g/L0.60 10.0 60-14091.59.15
2-Chlorotoluene g/L0.50 10.0 70-13092.89.28
4-Chlorotoluene g/L0.50 10.0 70-13089.78.97
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13095.29.52
1,2-Dichlorobenzene g/L0.50 10.0 70-13094.29.42
1,3-Dichlorobenzene g/L0.50 10.0 70-13096.19.61
1,4-Dichlorobenzene g/L0.50 10.0 70-13096.29.62
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14010710.7
1,1-Dichloroethane g/L0.50 10.0 70-13092.79.27
1,2-Dichloroethane g/L0.50 10.0 70-13010310.3
1,1-Dichloroethylene g/L0.50 10.0 70-13010410.4
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13096.29.62
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13088.08.80
1,2-Dichloropropane g/L0.50 10.0 70-13010010.0
1,3-Dichloropropane g/L0.50 10.0 70-13095.99.59
2,2-Dichloropropane g/L0.50 10.0 70-13077.87.78
1,1-Dichloropropene g/L0.50 10.0 70-13093.99.39
cis-1,3-Dichloropropene g/L0.50 10.0 70-13090.49.04
trans-1,3-Dichloropropene g/L0.50 10.0 70-13094.79.47
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B335888 - SW-846 5030B
LCS (B335888-BS1) Prepared & Analyzed: 04/03/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010510.5
Ethylbenzene g/L0.50 10.0 70-13095.29.52
2-Hexanone (MBK)g/L5.0 100 70-13095.395.3
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13091.09.10
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13086.28.62
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13094.59.45
Methylene Chloride g/L5.0 10.0 70-13097.89.78
4-Methyl-2-pentanone (MIBK)g/L5.0 100 L-0470-13067.5 *67.5
Naphthalene g/L0.50 10.0 L-0470-13052.2 *5.22
n-Propylbenzene g/L0.50 10.0 70-13084.68.46
Styrene g/L0.50 10.0 70-13090.69.06
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13087.38.73
Tetrachloroethylene g/L0.50 10.0 70-13099.89.98
Toluene g/L0.50 10.0 70-13095.09.50
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13073.87.38
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13078.97.89
1,1,1-Trichloroethane g/L0.50 10.0 70-13097.99.79
1,1,2-Trichloroethane g/L0.50 10.0 70-13095.49.54
Trichloroethylene g/L0.50 10.0 70-13099.39.93
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13010210.2
1,2,3-Trichloropropane g/L0.50 10.0 70-13011011.0
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13090.29.02
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13085.08.50
Vinyl Acetate g/L20 100 70-13084.684.6
Vinyl Chloride g/L0.50 10.0 60-14098.49.84
m+p Xylene g/L1.0 20.0 70-13094.819.0
o-Xylene g/L0.50 10.0 70-13090.99.09
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10426.0
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.824.0
LCS Dup (B335888-BSD1) Prepared & Analyzed: 04/03/23
Acetone g/L50 100 2570-130103 10.4103
Benzene g/L0.50 10.0 2570-130100 3.4510.0
Bromobenzene g/L0.50 10.0 2570-13094.2 4.569.42
Bromochloromethane g/L0.50 10.0 2570-130109 3.0710.9
Bromodichloromethane g/L0.50 10.0 2570-13098.5 1.339.85
Bromoform g/L0.50 10.0 2570-13086.6 0.9208.66
Bromomethane g/L2.0 10.0 25 L-0760-140154 9.47*15.4
2-Butanone (MEK)g/L5.0 100 2570-13096.2 7.8596.2
n-Butylbenzene g/L0.50 10.0 2570-13086.4 3.068.64
sec-Butylbenzene g/L0.50 10.0 2570-13093.3 4.619.33
tert-Butylbenzene g/L0.50 10.0 2570-13097.9 5.359.79
Carbon Tetrachloride g/L0.50 10.0 2570-13092.8 3.179.28
Chlorobenzene g/L0.50 10.0 2570-13097.8 2.079.78
Ethanol g/L50 100 2570-13088.4 3.7588.4
Chlorodibromomethane g/L0.50 10.0 2570-13090.2 0.8919.02
Chloroethane g/L0.50 10.0 2560-14096.9 3.799.69
Chloroform g/L0.50 10.0 2570-13098.8 3.829.88
Chloromethane g/L0.60 10.0 2560-14095.0 3.759.50
2-Chlorotoluene g/L0.50 10.0 2570-13089.2 3.968.92
4-Chlorotoluene g/L0.50 10.0 2570-13091.1 1.559.11
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B335888 - SW-846 5030B
LCS Dup (B335888-BSD1) Prepared & Analyzed: 04/03/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13091.2 4.299.12
1,2-Dichlorobenzene g/L0.50 10.0 2570-13097.9 3.859.79
1,3-Dichlorobenzene g/L0.50 10.0 2570-13096.8 0.7269.68
1,4-Dichlorobenzene g/L0.50 10.0 2570-13094.2 2.109.42
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-140111 3.7711.1
1,1-Dichloroethane g/L0.50 10.0 2570-13096.4 3.919.64
1,2-Dichloroethane g/L0.50 10.0 2570-130102 1.3610.2
1,1-Dichloroethylene g/L0.50 10.0 2570-130107 2.9410.7
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13098.4 2.269.84
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13091.0 3.359.10
1,2-Dichloropropane g/L0.50 10.0 2570-13099.8 0.3009.98
1,3-Dichloropropane g/L0.50 10.0 2570-13096.1 0.2089.61
2,2-Dichloropropane g/L0.50 10.0 2570-13083.2 6.718.32
1,1-Dichloropropene g/L0.50 10.0 2570-130101 7.2910.1
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13092.3 2.089.23
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13090.9 4.099.09
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130107 2.0810.7
Ethylbenzene g/L0.50 10.0 2570-13097.5 2.399.75
2-Hexanone (MBK)g/L5.0 100 2570-13089.1 6.7389.1
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13092.2 1.319.22
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13088.0 2.078.80
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13094.1 0.4249.41
Methylene Chloride g/L5.0 10.0 2570-130105 7.0110.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 25 L-0470-13062.4 7.88*62.4
Naphthalene g/L0.50 10.0 25 L-0470-13052.5 0.573*5.25
n-Propylbenzene g/L0.50 10.0 2570-13087.7 3.608.77
Styrene g/L0.50 10.0 2570-13089.1 1.678.91
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13085.7 1.858.57
Tetrachloroethylene g/L0.50 10.0 2570-130101 1.2910.1
Toluene g/L0.50 10.0 2570-13097.5 2.609.75
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13073.4 0.5437.34
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13077.8 1.407.78
1,1,1-Trichloroethane g/L0.50 10.0 2570-13098.7 0.8149.87
1,1,2-Trichloroethane g/L0.50 10.0 2570-13093.0 2.559.30
Trichloroethylene g/L0.50 10.0 2570-130101 1.9910.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130106 3.8510.6
1,2,3-Trichloropropane g/L0.50 10.0 2570-130103 6.3110.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13093.9 4.029.39
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13088.9 4.498.89
Vinyl Acetate g/L20 100 2570-13083.0 1.8083.0
Vinyl Chloride g/L0.50 10.0 2560-140104 5.9210.4
m+p Xylene g/L1.0 20.0 2570-13094.0 0.84718.8
o-Xylene g/L0.50 10.0 2570-13091.7 0.8769.17
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10426.0
g/L 25.0 70-130Surrogate: Toluene-d8 99.124.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 93.023.3
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
Elevated reporting limit due to matrix interference.RL-12
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 26 of 30
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
652North Carolina Div. of Water QualityNC 12/31/2023
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