WA-1411_16616_CA_MRP_20110209

February 01, 2011
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9286253
9286253
Project:
Pace Project No.:
RE:
Linda Blalock
NCDENR-UST Section
1637 Mail Service Center
Raleigh, NC 276991637
Cofield Service Center #16616
Dear Linda Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on January 21, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ashley Nifong
[e-mail]
Project Manager
Enclosures
cc:Chris Hanley, Agra Environmental, Inc.
Raj Shah, Agra Environmental, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9286253001 MW1 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-CJMW
EPA 625 58 PASI-CPPM
SM 6200B 64 PASI-CTLS
9286253002 MW2 MADEP EPH 7 PASI-CCAH
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-CJMW
EPA 625 58 PASI-CPPM
SM 6200B 64 PASI-CTLS
9286253003 MW3 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-CJMW
EPA 625 58 PASI-CPPM
SM 6200B 64 PASI-CTLS
9286253004 MW4 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-CJMW
EPA 625 58 PASI-CPPM
SM 6200B 64 PASI-CTLS
9286253005 WSW1 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-CJMW
EPA 625 58 PASI-CPPM
SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
HITS ONLY
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9286253002 MW2
Aliphatic (C05-C08)130 ug/L 01/25/11 23:01 N2100MADEP VPH
Lead 7.5 ug/L 01/24/11 21:505.0EPA 200.7
Benzene 8.4 ug/L 01/27/11 16:480.50SM 6200B
1,2-Dichloroethane 9.0 ug/L 01/27/11 16:480.50SM 6200B
Diisopropyl ether 1.6 ug/L 01/27/11 16:480.50SM 6200B
Ethylbenzene 2.4 ug/L 01/27/11 16:480.50SM 6200B
Isopropylbenzene (Cumene)1.2 ug/L 01/27/11 16:480.50SM 6200B
Naphthalene 3.9 ug/L 01/27/11 16:482.0SM 6200B
n-Propylbenzene 0.72 ug/L 01/27/11 16:480.50SM 6200B
1,2,4-Trimethylbenzene 3.9 ug/L 01/27/11 16:480.50SM 6200B
m&p-Xylene 7.8 ug/L 01/27/11 16:481.0SM 6200B
o-Xylene 7.4 ug/L 01/27/11 16:480.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW1 Lab ID:9286253001 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 01/28/11 04:59 N201/26/11 14:15114
Aliphatic (C19-C36)ND ug/L 1 01/28/11 04:59 N201/26/11 14:15114
Aromatic (C11-C22)ND ug/L 1 01/28/11 04:59 N201/26/11 14:15114
Nonatriacontane (S)76 %1 01/28/11 04:59 7194-86-701/26/11 14:1540-140
o-Terphenyl (S)79 %1 01/28/11 04:59 84-15-101/26/11 14:1540-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 01/25/11 22:35 N2100
Aliphatic (C09-C12)ND ug/L 1 01/25/11 22:35 N2100
Aromatic (C09-C10)ND ug/L 1 01/25/11 22:35 N2100
2,5-Dibromotoluene (PID)(S)100 %1 01/25/11 22:3570-130
2,5-Dibromotoluene (FID)(S)96 %1 01/25/11 22:3570-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 01/24/11 21:47 7439-92-101/22/11 09:305.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 01/28/11 17:58 83-32-901/26/11 09:455.0
Acenaphthylene ND ug/L 1 01/28/11 17:58 208-96-801/26/11 09:455.0
Anthracene ND ug/L 1 01/28/11 17:58 120-12-701/26/11 09:455.0
Benzo(a)anthracene ND ug/L 1 01/28/11 17:58 56-55-301/26/11 09:455.0
Benzo(a)pyrene ND ug/L 1 01/28/11 17:58 50-32-801/26/11 09:455.0
Benzo(b)fluoranthene ND ug/L 1 01/28/11 17:58 205-99-201/26/11 09:455.0
Benzo(g,h,i)perylene ND ug/L 1 01/28/11 17:58 191-24-201/26/11 09:455.0
Benzo(k)fluoranthene ND ug/L 1 01/28/11 17:58 207-08-901/26/11 09:455.0
4-Bromophenylphenyl ether ND ug/L 1 01/28/11 17:58 101-55-301/26/11 09:455.0
Butylbenzylphthalate ND ug/L 1 01/28/11 17:58 85-68-701/26/11 09:455.0
4-Chloro-3-methylphenol ND ug/L 1 01/28/11 17:58 59-50-701/26/11 09:455.0
bis(2-Chloroethoxy)methane ND ug/L 1 01/28/11 17:58 111-91-101/26/11 09:4510.0
bis(2-Chloroethyl) ether ND ug/L 1 01/28/11 17:58 111-44-401/26/11 09:455.0
bis(2-Chloroisopropyl) ether ND ug/L 1 01/28/11 17:58 108-60-101/26/11 09:455.0
2-Chloronaphthalene ND ug/L 1 01/28/11 17:58 91-58-701/26/11 09:455.0
2-Chlorophenol ND ug/L 1 01/28/11 17:58 95-57-801/26/11 09:455.0
4-Chlorophenylphenyl ether ND ug/L 1 01/28/11 17:58 7005-72-301/26/11 09:455.0
Chrysene ND ug/L 1 01/28/11 17:58 218-01-901/26/11 09:455.0
Dibenz(a,h)anthracene ND ug/L 1 01/28/11 17:58 53-70-301/26/11 09:455.0
3,3'-Dichlorobenzidine ND ug/L 1 01/28/11 17:58 91-94-101/26/11 09:4525.0
2,4-Dichlorophenol ND ug/L 1 01/28/11 17:58 120-83-201/26/11 09:455.0
Diethylphthalate ND ug/L 1 01/28/11 17:58 84-66-201/26/11 09:455.0
2,4-Dimethylphenol ND ug/L 1 01/28/11 17:58 105-67-901/26/11 09:4510.0
Dimethylphthalate ND ug/L 1 01/28/11 17:58 131-11-301/26/11 09:455.0
Di-n-butylphthalate ND ug/L 1 01/28/11 17:58 84-74-201/26/11 09:455.0
4,6-Dinitro-2-methylphenol ND ug/L 1 01/28/11 17:58 534-52-101/26/11 09:4520.0
2,4-Dinitrophenol ND ug/L 1 01/28/11 17:58 51-28-501/26/11 09:4550.0
2,4-Dinitrotoluene ND ug/L 1 01/28/11 17:58 121-14-201/26/11 09:455.0
2,6-Dinitrotoluene ND ug/L 1 01/28/11 17:58 606-20-201/26/11 09:455.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 5 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW1 Lab ID:9286253001 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 01/28/11 17:58 117-84-001/26/11 09:455.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 01/28/11 17:58 117-81-701/26/11 09:455.0
Fluoranthene ND ug/L 1 01/28/11 17:58 206-44-001/26/11 09:455.0
Fluorene ND ug/L 1 01/28/11 17:58 86-73-701/26/11 09:455.0
Hexachloro-1,3-butadiene ND ug/L 1 01/28/11 17:58 87-68-301/26/11 09:455.0
Hexachlorobenzene ND ug/L 1 01/28/11 17:58 118-74-101/26/11 09:455.0
Hexachlorocyclopentadiene ND ug/L 1 01/28/11 17:58 77-47-401/26/11 09:4510.0
Hexachloroethane ND ug/L 1 01/28/11 17:58 67-72-101/26/11 09:455.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 01/28/11 17:58 193-39-501/26/11 09:455.0
Isophorone ND ug/L 1 01/28/11 17:58 78-59-101/26/11 09:4510.0
Naphthalene ND ug/L 1 01/28/11 17:58 91-20-301/26/11 09:455.0
Nitrobenzene ND ug/L 1 01/28/11 17:58 98-95-301/26/11 09:455.0
2-Nitrophenol ND ug/L 1 01/28/11 17:58 88-75-501/26/11 09:455.0
4-Nitrophenol ND ug/L 1 01/28/11 17:58 100-02-701/26/11 09:4550.0
N-Nitrosodimethylamine ND ug/L 1 01/28/11 17:58 62-75-901/26/11 09:455.0
N-Nitroso-di-n-propylamine ND ug/L 1 01/28/11 17:58 621-64-701/26/11 09:455.0
N-Nitrosodiphenylamine ND ug/L 1 01/28/11 17:58 86-30-601/26/11 09:4510.0
Pentachlorophenol ND ug/L 1 01/28/11 17:58 87-86-501/26/11 09:4525.0
Phenanthrene ND ug/L 1 01/28/11 17:58 85-01-801/26/11 09:455.0
Phenol ND ug/L 1 01/28/11 17:58 108-95-201/26/11 09:455.0
Pyrene ND ug/L 1 01/28/11 17:58 129-00-001/26/11 09:455.0
1,2,4-Trichlorobenzene ND ug/L 1 01/28/11 17:58 120-82-101/26/11 09:455.0
2,4,6-Trichlorophenol ND ug/L 1 01/28/11 17:58 88-06-201/26/11 09:4510.0
Nitrobenzene-d5 (S)57 %1 01/28/11 17:58 4165-60-001/26/11 09:4510-120
2-Fluorobiphenyl (S)65 %1 01/28/11 17:58 321-60-801/26/11 09:4515-120
Terphenyl-d14 (S)75 %1 01/28/11 17:58 1718-51-001/26/11 09:4511-131
Phenol-d6 (S)29 %1 01/28/11 17:58 13127-88-301/26/11 09:4510-120
2-Fluorophenol (S)40 %1 01/28/11 17:58 367-12-401/26/11 09:4510-120
2,4,6-Tribromophenol (S)75 %1 01/28/11 17:58 118-79-601/26/11 09:4510-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 01/26/11 04:47 71-43-20.50
Bromobenzene ND ug/L 1 01/26/11 04:47 108-86-10.50
Bromochloromethane ND ug/L 1 01/26/11 04:47 74-97-50.50
Bromodichloromethane ND ug/L 1 01/26/11 04:47 75-27-40.50
Bromoform ND ug/L 1 01/26/11 04:47 75-25-20.50
Bromomethane ND ug/L 1 01/26/11 04:47 74-83-95.0
n-Butylbenzene ND ug/L 1 01/26/11 04:47 104-51-80.50
sec-Butylbenzene ND ug/L 1 01/26/11 04:47 135-98-80.50
tert-Butylbenzene ND ug/L 1 01/26/11 04:47 98-06-60.50
Carbon tetrachloride ND ug/L 1 01/26/11 04:47 56-23-50.50
Chlorobenzene ND ug/L 1 01/26/11 04:47 108-90-70.50
Chloroethane ND ug/L 1 01/26/11 04:47 75-00-31.0
Chloroform ND ug/L 1 01/26/11 04:47 67-66-30.50
Chloromethane ND ug/L 1 01/26/11 04:47 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/26/11 04:47 95-49-80.50
4-Chlorotoluene ND ug/L 1 01/26/11 04:47 106-43-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 6 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW1 Lab ID:9286253001 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2-Dibromo-3-chloropropane ND ug/L 1 01/26/11 04:47 96-12-81.0
Dibromochloromethane ND ug/L 1 01/26/11 04:47 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 01/26/11 04:47 106-93-40.50
Dibromomethane ND ug/L 1 01/26/11 04:47 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 01/26/11 04:47 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 01/26/11 04:47 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 01/26/11 04:47 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 01/26/11 04:47 75-71-80.50
1,1-Dichloroethane ND ug/L 1 01/26/11 04:47 75-34-30.50
1,2-Dichloroethane ND ug/L 1 01/26/11 04:47 107-06-20.50
1,1-Dichloroethene ND ug/L 1 01/26/11 04:47 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 01/26/11 04:47 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 01/26/11 04:47 156-60-50.50
1,2-Dichloropropane ND ug/L 1 01/26/11 04:47 78-87-50.50
1,3-Dichloropropane ND ug/L 1 01/26/11 04:47 142-28-90.50
2,2-Dichloropropane ND ug/L 1 01/26/11 04:47 594-20-70.50
1,1-Dichloropropene ND ug/L 1 01/26/11 04:47 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 01/26/11 04:47 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 01/26/11 04:47 10061-02-60.50
Diisopropyl ether ND ug/L 1 01/26/11 04:47 108-20-30.50
Ethylbenzene ND ug/L 1 01/26/11 04:47 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 01/26/11 04:47 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 01/26/11 04:47 98-82-80.50
Methylene Chloride ND ug/L 1 01/26/11 04:47 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 01/26/11 04:47 1634-04-40.50
Naphthalene ND ug/L 1 01/26/11 04:47 91-20-32.0
n-Propylbenzene ND ug/L 1 01/26/11 04:47 103-65-10.50
Styrene ND ug/L 1 01/26/11 04:47 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 01/26/11 04:47 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 01/26/11 04:47 79-34-50.50
Tetrachloroethene ND ug/L 1 01/26/11 04:47 127-18-40.50
Toluene ND ug/L 1 01/26/11 04:47 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 01/26/11 04:47 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 01/26/11 04:47 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 01/26/11 04:47 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 01/26/11 04:47 79-00-50.50
Trichloroethene ND ug/L 1 01/26/11 04:47 79-01-60.50
Trichlorofluoromethane ND ug/L 1 01/26/11 04:47 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/26/11 04:47 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 01/26/11 04:47 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 01/26/11 04:47 108-67-80.50
Vinyl chloride ND ug/L 1 01/26/11 04:47 75-01-41.0
m&p-Xylene ND ug/L 1 01/26/11 04:47 179601-23-11.0
o-Xylene ND ug/L 1 01/26/11 04:47 95-47-60.50
1,2-Dichloroethane-d4 (S)120 %1 01/26/11 04:47 17060-07-070-130
Dibromofluoromethane (S)113 %1 01/26/11 04:47 1868-53-770-130
4-Bromofluorobenzene (S)101 %1 01/26/11 04:47 460-00-470-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 7 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW1 Lab ID:9286253001 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene-d8 (S)101 %1 01/26/11 04:47 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 8 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW2 Lab ID:9286253002 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 01/31/11 22:48 N201/26/11 14:15114
Aliphatic (C19-C36)ND ug/L 1 01/31/11 22:48 N201/26/11 14:15114
Aromatic (C11-C22)ND ug/L 1 01/31/11 22:48 N201/26/11 14:15114
Nonatriacontane (S)76 %1 01/31/11 22:48 7194-86-701/26/11 14:1540-140
o-Terphenyl (S)66 %1 01/31/11 22:48 84-15-101/26/11 14:1540-140
2-Fluorobiphenyl (S)91 %1 01/31/11 22:48 321-60-801/26/11 14:1540-140
2-Bromonaphthalene (S)95 %1 01/31/11 22:48 580-13-201/26/11 14:1540-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)130 ug/L 1 01/25/11 23:01 N2100
Aliphatic (C09-C12)ND ug/L 1 01/25/11 23:01 N2100
Aromatic (C09-C10)ND ug/L 1 01/25/11 23:01 N2100
2,5-Dibromotoluene (PID)(S)107 %1 01/25/11 23:0170-130
2,5-Dibromotoluene (FID)(S)101 %1 01/25/11 23:0170-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 7.5 ug/L 1 01/24/11 21:50 7439-92-101/22/11 09:305.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 01/28/11 18:26 83-32-901/26/11 09:455.9
Acenaphthylene ND ug/L 1 01/28/11 18:26 208-96-801/26/11 09:455.9
Anthracene ND ug/L 1 01/28/11 18:26 120-12-701/26/11 09:455.9
Benzo(a)anthracene ND ug/L 1 01/28/11 18:26 56-55-301/26/11 09:455.9
Benzo(a)pyrene ND ug/L 1 01/28/11 18:26 50-32-801/26/11 09:455.9
Benzo(b)fluoranthene ND ug/L 1 01/28/11 18:26 205-99-201/26/11 09:455.9
Benzo(g,h,i)perylene ND ug/L 1 01/28/11 18:26 191-24-201/26/11 09:455.9
Benzo(k)fluoranthene ND ug/L 1 01/28/11 18:26 207-08-901/26/11 09:455.9
4-Bromophenylphenyl ether ND ug/L 1 01/28/11 18:26 101-55-301/26/11 09:455.9
Butylbenzylphthalate ND ug/L 1 01/28/11 18:26 85-68-701/26/11 09:455.9
4-Chloro-3-methylphenol ND ug/L 1 01/28/11 18:26 59-50-701/26/11 09:455.9
bis(2-Chloroethoxy)methane ND ug/L 1 01/28/11 18:26 111-91-101/26/11 09:4511.8
bis(2-Chloroethyl) ether ND ug/L 1 01/28/11 18:26 111-44-401/26/11 09:455.9
bis(2-Chloroisopropyl) ether ND ug/L 1 01/28/11 18:26 108-60-101/26/11 09:455.9
2-Chloronaphthalene ND ug/L 1 01/28/11 18:26 91-58-701/26/11 09:455.9
2-Chlorophenol ND ug/L 1 01/28/11 18:26 95-57-801/26/11 09:455.9
4-Chlorophenylphenyl ether ND ug/L 1 01/28/11 18:26 7005-72-301/26/11 09:455.9
Chrysene ND ug/L 1 01/28/11 18:26 218-01-901/26/11 09:455.9
Dibenz(a,h)anthracene ND ug/L 1 01/28/11 18:26 53-70-301/26/11 09:455.9
3,3'-Dichlorobenzidine ND ug/L 1 01/28/11 18:26 91-94-101/26/11 09:4529.4
2,4-Dichlorophenol ND ug/L 1 01/28/11 18:26 120-83-201/26/11 09:455.9
Diethylphthalate ND ug/L 1 01/28/11 18:26 84-66-201/26/11 09:455.9
2,4-Dimethylphenol ND ug/L 1 01/28/11 18:26 105-67-901/26/11 09:4511.8
Dimethylphthalate ND ug/L 1 01/28/11 18:26 131-11-301/26/11 09:455.9
Di-n-butylphthalate ND ug/L 1 01/28/11 18:26 84-74-201/26/11 09:455.9
4,6-Dinitro-2-methylphenol ND ug/L 1 01/28/11 18:26 534-52-101/26/11 09:4523.5
2,4-Dinitrophenol ND ug/L 1 01/28/11 18:26 51-28-501/26/11 09:4558.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 9 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW2 Lab ID:9286253002 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 01/28/11 18:26 121-14-201/26/11 09:455.9
2,6-Dinitrotoluene ND ug/L 1 01/28/11 18:26 606-20-201/26/11 09:455.9
Di-n-octylphthalate ND ug/L 1 01/28/11 18:26 117-84-001/26/11 09:455.9
bis(2-Ethylhexyl)phthalate ND ug/L 1 01/28/11 18:26 117-81-701/26/11 09:455.9
Fluoranthene ND ug/L 1 01/28/11 18:26 206-44-001/26/11 09:455.9
Fluorene ND ug/L 1 01/28/11 18:26 86-73-701/26/11 09:455.9
Hexachloro-1,3-butadiene ND ug/L 1 01/28/11 18:26 87-68-301/26/11 09:455.9
Hexachlorobenzene ND ug/L 1 01/28/11 18:26 118-74-101/26/11 09:455.9
Hexachlorocyclopentadiene ND ug/L 1 01/28/11 18:26 77-47-401/26/11 09:4511.8
Hexachloroethane ND ug/L 1 01/28/11 18:26 67-72-101/26/11 09:455.9
Indeno(1,2,3-cd)pyrene ND ug/L 1 01/28/11 18:26 193-39-501/26/11 09:455.9
Isophorone ND ug/L 1 01/28/11 18:26 78-59-101/26/11 09:4511.8
Naphthalene ND ug/L 1 01/28/11 18:26 91-20-301/26/11 09:455.9
Nitrobenzene ND ug/L 1 01/28/11 18:26 98-95-301/26/11 09:455.9
2-Nitrophenol ND ug/L 1 01/28/11 18:26 88-75-501/26/11 09:455.9
4-Nitrophenol ND ug/L 1 01/28/11 18:26 100-02-701/26/11 09:4558.8
N-Nitrosodimethylamine ND ug/L 1 01/28/11 18:26 62-75-901/26/11 09:455.9
N-Nitroso-di-n-propylamine ND ug/L 1 01/28/11 18:26 621-64-701/26/11 09:455.9
N-Nitrosodiphenylamine ND ug/L 1 01/28/11 18:26 86-30-601/26/11 09:4511.8
Pentachlorophenol ND ug/L 1 01/28/11 18:26 87-86-501/26/11 09:4529.4
Phenanthrene ND ug/L 1 01/28/11 18:26 85-01-801/26/11 09:455.9
Phenol ND ug/L 1 01/28/11 18:26 108-95-201/26/11 09:455.9
Pyrene ND ug/L 1 01/28/11 18:26 129-00-001/26/11 09:455.9
1,2,4-Trichlorobenzene ND ug/L 1 01/28/11 18:26 120-82-101/26/11 09:455.9
2,4,6-Trichlorophenol ND ug/L 1 01/28/11 18:26 88-06-201/26/11 09:4511.8
Nitrobenzene-d5 (S)60 %1 01/28/11 18:26 4165-60-001/26/11 09:4510-120
2-Fluorobiphenyl (S)62 %1 01/28/11 18:26 321-60-801/26/11 09:4515-120
Terphenyl-d14 (S)70 %1 01/28/11 18:26 1718-51-001/26/11 09:4511-131
Phenol-d6 (S)31 %1 01/28/11 18:26 13127-88-301/26/11 09:4510-120
2-Fluorophenol (S)41 %1 01/28/11 18:26 367-12-401/26/11 09:4510-120
2,4,6-Tribromophenol (S)80 %1 01/28/11 18:26 118-79-601/26/11 09:4510-137
6200B MSV Analytical Method: SM 6200B
Benzene 8.4 ug/L 1 01/27/11 16:48 71-43-20.50
Bromobenzene ND ug/L 1 01/27/11 16:48 108-86-10.50
Bromochloromethane ND ug/L 1 01/27/11 16:48 74-97-50.50
Bromodichloromethane ND ug/L 1 01/27/11 16:48 75-27-40.50
Bromoform ND ug/L 1 01/27/11 16:48 75-25-20.50
Bromomethane ND ug/L 1 01/27/11 16:48 74-83-95.0
n-Butylbenzene ND ug/L 1 01/27/11 16:48 104-51-80.50
sec-Butylbenzene ND ug/L 1 01/27/11 16:48 135-98-80.50
tert-Butylbenzene ND ug/L 1 01/27/11 16:48 98-06-60.50
Carbon tetrachloride ND ug/L 1 01/27/11 16:48 56-23-50.50
Chlorobenzene ND ug/L 1 01/27/11 16:48 108-90-70.50
Chloroethane ND ug/L 1 01/27/11 16:48 75-00-31.0
Chloroform ND ug/L 1 01/27/11 16:48 67-66-30.50
Chloromethane ND ug/L 1 01/27/11 16:48 74-87-31.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 10 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW2 Lab ID:9286253002 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 01/27/11 16:48 95-49-80.50
4-Chlorotoluene ND ug/L 1 01/27/11 16:48 106-43-40.50
1,2-Dibromo-3-chloropropane ND ug/L 1 01/27/11 16:48 96-12-81.0
Dibromochloromethane ND ug/L 1 01/27/11 16:48 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 01/27/11 16:48 106-93-40.50
Dibromomethane ND ug/L 1 01/27/11 16:48 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 01/27/11 16:48 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 01/27/11 16:48 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 01/27/11 16:48 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 01/27/11 16:48 75-71-80.50
1,1-Dichloroethane ND ug/L 1 01/27/11 16:48 75-34-30.50
1,2-Dichloroethane 9.0 ug/L 1 01/27/11 16:48 107-06-20.50
1,1-Dichloroethene ND ug/L 1 01/27/11 16:48 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 01/27/11 16:48 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 01/27/11 16:48 156-60-50.50
1,2-Dichloropropane ND ug/L 1 01/27/11 16:48 78-87-50.50
1,3-Dichloropropane ND ug/L 1 01/27/11 16:48 142-28-90.50
2,2-Dichloropropane ND ug/L 1 01/27/11 16:48 594-20-70.50
1,1-Dichloropropene ND ug/L 1 01/27/11 16:48 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 01/27/11 16:48 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 01/27/11 16:48 10061-02-60.50
Diisopropyl ether 1.6 ug/L 1 01/27/11 16:48 108-20-30.50
Ethylbenzene 2.4 ug/L 1 01/27/11 16:48 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 01/27/11 16:48 87-68-32.0
Isopropylbenzene (Cumene)1.2 ug/L 1 01/27/11 16:48 98-82-80.50
Methylene Chloride ND ug/L 1 01/27/11 16:48 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 01/27/11 16:48 1634-04-40.50
Naphthalene 3.9 ug/L 1 01/27/11 16:48 91-20-32.0
n-Propylbenzene 0.72 ug/L 1 01/27/11 16:48 103-65-10.50
Styrene ND ug/L 1 01/27/11 16:48 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 01/27/11 16:48 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 01/27/11 16:48 79-34-50.50
Tetrachloroethene ND ug/L 1 01/27/11 16:48 127-18-40.50
Toluene ND ug/L 1 01/27/11 16:48 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 01/27/11 16:48 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 01/27/11 16:48 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 01/27/11 16:48 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 01/27/11 16:48 79-00-50.50
Trichloroethene ND ug/L 1 01/27/11 16:48 79-01-60.50
Trichlorofluoromethane ND ug/L 1 01/27/11 16:48 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/27/11 16:48 96-18-40.50
1,2,4-Trimethylbenzene 3.9 ug/L 1 01/27/11 16:48 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 01/27/11 16:48 108-67-80.50
Vinyl chloride ND ug/L 1 01/27/11 16:48 75-01-41.0
m&p-Xylene 7.8 ug/L 1 01/27/11 16:48 179601-23-11.0
o-Xylene 7.4 ug/L 1 01/27/11 16:48 95-47-60.50
1,2-Dichloroethane-d4 (S)105 %1 01/27/11 16:48 17060-07-070-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 11 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW2 Lab ID:9286253002 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Dibromofluoromethane (S)102 %1 01/27/11 16:48 1868-53-770-130
4-Bromofluorobenzene (S)101 %1 01/27/11 16:48 460-00-470-130
Toluene-d8 (S)100 %1 01/27/11 16:48 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 12 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW3 Lab ID:9286253003 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 01/28/11 05:34 N201/26/11 14:15116
Aliphatic (C19-C36)ND ug/L 1 01/28/11 05:34 N201/26/11 14:15116
Aromatic (C11-C22)ND ug/L 1 01/28/11 05:34 N201/26/11 14:15116
Nonatriacontane (S)76 %1 01/28/11 05:34 7194-86-701/26/11 14:1540-140
o-Terphenyl (S)78 %1 01/28/11 05:34 84-15-101/26/11 14:1540-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 01/25/11 23:25 N2100
Aliphatic (C09-C12)ND ug/L 1 01/25/11 23:25 N2100
Aromatic (C09-C10)ND ug/L 1 01/25/11 23:25 N2100
2,5-Dibromotoluene (PID)(S)110 %1 01/25/11 23:2570-130
2,5-Dibromotoluene (FID)(S)111 %1 01/25/11 23:2570-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 01/24/11 21:54 7439-92-101/22/11 09:305.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 01/28/11 18:54 83-32-901/26/11 09:455.7
Acenaphthylene ND ug/L 1 01/28/11 18:54 208-96-801/26/11 09:455.7
Anthracene ND ug/L 1 01/28/11 18:54 120-12-701/26/11 09:455.7
Benzo(a)anthracene ND ug/L 1 01/28/11 18:54 56-55-301/26/11 09:455.7
Benzo(a)pyrene ND ug/L 1 01/28/11 18:54 50-32-801/26/11 09:455.7
Benzo(b)fluoranthene ND ug/L 1 01/28/11 18:54 205-99-201/26/11 09:455.7
Benzo(g,h,i)perylene ND ug/L 1 01/28/11 18:54 191-24-201/26/11 09:455.7
Benzo(k)fluoranthene ND ug/L 1 01/28/11 18:54 207-08-901/26/11 09:455.7
4-Bromophenylphenyl ether ND ug/L 1 01/28/11 18:54 101-55-301/26/11 09:455.7
Butylbenzylphthalate ND ug/L 1 01/28/11 18:54 85-68-701/26/11 09:455.7
4-Chloro-3-methylphenol ND ug/L 1 01/28/11 18:54 59-50-701/26/11 09:455.7
bis(2-Chloroethoxy)methane ND ug/L 1 01/28/11 18:54 111-91-101/26/11 09:4511.4
bis(2-Chloroethyl) ether ND ug/L 1 01/28/11 18:54 111-44-401/26/11 09:455.7
bis(2-Chloroisopropyl) ether ND ug/L 1 01/28/11 18:54 108-60-101/26/11 09:455.7
2-Chloronaphthalene ND ug/L 1 01/28/11 18:54 91-58-701/26/11 09:455.7
2-Chlorophenol ND ug/L 1 01/28/11 18:54 95-57-801/26/11 09:455.7
4-Chlorophenylphenyl ether ND ug/L 1 01/28/11 18:54 7005-72-301/26/11 09:455.7
Chrysene ND ug/L 1 01/28/11 18:54 218-01-901/26/11 09:455.7
Dibenz(a,h)anthracene ND ug/L 1 01/28/11 18:54 53-70-301/26/11 09:455.7
3,3'-Dichlorobenzidine ND ug/L 1 01/28/11 18:54 91-94-101/26/11 09:4528.4
2,4-Dichlorophenol ND ug/L 1 01/28/11 18:54 120-83-201/26/11 09:455.7
Diethylphthalate ND ug/L 1 01/28/11 18:54 84-66-201/26/11 09:455.7
2,4-Dimethylphenol ND ug/L 1 01/28/11 18:54 105-67-901/26/11 09:4511.4
Dimethylphthalate ND ug/L 1 01/28/11 18:54 131-11-301/26/11 09:455.7
Di-n-butylphthalate ND ug/L 1 01/28/11 18:54 84-74-201/26/11 09:455.7
4,6-Dinitro-2-methylphenol ND ug/L 1 01/28/11 18:54 534-52-101/26/11 09:4522.7
2,4-Dinitrophenol ND ug/L 1 01/28/11 18:54 51-28-501/26/11 09:4556.8
2,4-Dinitrotoluene ND ug/L 1 01/28/11 18:54 121-14-201/26/11 09:455.7
2,6-Dinitrotoluene ND ug/L 1 01/28/11 18:54 606-20-201/26/11 09:455.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 13 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW3 Lab ID:9286253003 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 01/28/11 18:54 117-84-001/26/11 09:455.7
bis(2-Ethylhexyl)phthalate ND ug/L 1 01/28/11 18:54 117-81-701/26/11 09:455.7
Fluoranthene ND ug/L 1 01/28/11 18:54 206-44-001/26/11 09:455.7
Fluorene ND ug/L 1 01/28/11 18:54 86-73-701/26/11 09:455.7
Hexachloro-1,3-butadiene ND ug/L 1 01/28/11 18:54 87-68-301/26/11 09:455.7
Hexachlorobenzene ND ug/L 1 01/28/11 18:54 118-74-101/26/11 09:455.7
Hexachlorocyclopentadiene ND ug/L 1 01/28/11 18:54 77-47-401/26/11 09:4511.4
Hexachloroethane ND ug/L 1 01/28/11 18:54 67-72-101/26/11 09:455.7
Indeno(1,2,3-cd)pyrene ND ug/L 1 01/28/11 18:54 193-39-501/26/11 09:455.7
Isophorone ND ug/L 1 01/28/11 18:54 78-59-101/26/11 09:4511.4
Naphthalene ND ug/L 1 01/28/11 18:54 91-20-301/26/11 09:455.7
Nitrobenzene ND ug/L 1 01/28/11 18:54 98-95-301/26/11 09:455.7
2-Nitrophenol ND ug/L 1 01/28/11 18:54 88-75-501/26/11 09:455.7
4-Nitrophenol ND ug/L 1 01/28/11 18:54 100-02-701/26/11 09:4556.8
N-Nitrosodimethylamine ND ug/L 1 01/28/11 18:54 62-75-901/26/11 09:455.7
N-Nitroso-di-n-propylamine ND ug/L 1 01/28/11 18:54 621-64-701/26/11 09:455.7
N-Nitrosodiphenylamine ND ug/L 1 01/28/11 18:54 86-30-601/26/11 09:4511.4
Pentachlorophenol ND ug/L 1 01/28/11 18:54 87-86-501/26/11 09:4528.4
Phenanthrene ND ug/L 1 01/28/11 18:54 85-01-801/26/11 09:455.7
Phenol ND ug/L 1 01/28/11 18:54 108-95-201/26/11 09:455.7
Pyrene ND ug/L 1 01/28/11 18:54 129-00-001/26/11 09:455.7
1,2,4-Trichlorobenzene ND ug/L 1 01/28/11 18:54 120-82-101/26/11 09:455.7
2,4,6-Trichlorophenol ND ug/L 1 01/28/11 18:54 88-06-201/26/11 09:4511.4
Nitrobenzene-d5 (S)51 %1 01/28/11 18:54 4165-60-001/26/11 09:4510-120
2-Fluorobiphenyl (S)54 %1 01/28/11 18:54 321-60-801/26/11 09:4515-120
Terphenyl-d14 (S)73 %1 01/28/11 18:54 1718-51-001/26/11 09:4511-131
Phenol-d6 (S)30 %1 01/28/11 18:54 13127-88-301/26/11 09:4510-120
2-Fluorophenol (S)41 %1 01/28/11 18:54 367-12-401/26/11 09:4510-120
2,4,6-Tribromophenol (S)75 %1 01/28/11 18:54 118-79-601/26/11 09:4510-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 01/26/11 05:10 71-43-20.50
Bromobenzene ND ug/L 1 01/26/11 05:10 108-86-10.50
Bromochloromethane ND ug/L 1 01/26/11 05:10 74-97-50.50
Bromodichloromethane ND ug/L 1 01/26/11 05:10 75-27-40.50
Bromoform ND ug/L 1 01/26/11 05:10 75-25-20.50
Bromomethane ND ug/L 1 01/26/11 05:10 74-83-95.0
n-Butylbenzene ND ug/L 1 01/26/11 05:10 104-51-80.50
sec-Butylbenzene ND ug/L 1 01/26/11 05:10 135-98-80.50
tert-Butylbenzene ND ug/L 1 01/26/11 05:10 98-06-60.50
Carbon tetrachloride ND ug/L 1 01/26/11 05:10 56-23-50.50
Chlorobenzene ND ug/L 1 01/26/11 05:10 108-90-70.50
Chloroethane ND ug/L 1 01/26/11 05:10 75-00-31.0
Chloroform ND ug/L 1 01/26/11 05:10 67-66-30.50
Chloromethane ND ug/L 1 01/26/11 05:10 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/26/11 05:10 95-49-80.50
4-Chlorotoluene ND ug/L 1 01/26/11 05:10 106-43-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 14 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW3 Lab ID:9286253003 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2-Dibromo-3-chloropropane ND ug/L 1 01/26/11 05:10 96-12-81.0
Dibromochloromethane ND ug/L 1 01/26/11 05:10 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 01/26/11 05:10 106-93-40.50
Dibromomethane ND ug/L 1 01/26/11 05:10 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 01/26/11 05:10 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 01/26/11 05:10 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 01/26/11 05:10 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 01/26/11 05:10 75-71-80.50
1,1-Dichloroethane ND ug/L 1 01/26/11 05:10 75-34-30.50
1,2-Dichloroethane ND ug/L 1 01/26/11 05:10 107-06-20.50
1,1-Dichloroethene ND ug/L 1 01/26/11 05:10 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 01/26/11 05:10 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 01/26/11 05:10 156-60-50.50
1,2-Dichloropropane ND ug/L 1 01/26/11 05:10 78-87-50.50
1,3-Dichloropropane ND ug/L 1 01/26/11 05:10 142-28-90.50
2,2-Dichloropropane ND ug/L 1 01/26/11 05:10 594-20-70.50
1,1-Dichloropropene ND ug/L 1 01/26/11 05:10 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 01/26/11 05:10 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 01/26/11 05:10 10061-02-60.50
Diisopropyl ether ND ug/L 1 01/26/11 05:10 108-20-30.50
Ethylbenzene ND ug/L 1 01/26/11 05:10 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 01/26/11 05:10 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 01/26/11 05:10 98-82-80.50
Methylene Chloride ND ug/L 1 01/26/11 05:10 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 01/26/11 05:10 1634-04-40.50
Naphthalene ND ug/L 1 01/26/11 05:10 91-20-32.0
n-Propylbenzene ND ug/L 1 01/26/11 05:10 103-65-10.50
Styrene ND ug/L 1 01/26/11 05:10 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 01/26/11 05:10 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 01/26/11 05:10 79-34-50.50
Tetrachloroethene ND ug/L 1 01/26/11 05:10 127-18-40.50
Toluene ND ug/L 1 01/26/11 05:10 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 01/26/11 05:10 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 01/26/11 05:10 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 01/26/11 05:10 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 01/26/11 05:10 79-00-50.50
Trichloroethene ND ug/L 1 01/26/11 05:10 79-01-60.50
Trichlorofluoromethane ND ug/L 1 01/26/11 05:10 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/26/11 05:10 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 01/26/11 05:10 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 01/26/11 05:10 108-67-80.50
Vinyl chloride ND ug/L 1 01/26/11 05:10 75-01-41.0
m&p-Xylene ND ug/L 1 01/26/11 05:10 179601-23-11.0
o-Xylene ND ug/L 1 01/26/11 05:10 95-47-60.50
1,2-Dichloroethane-d4 (S)98 %1 01/26/11 05:10 17060-07-070-130
Dibromofluoromethane (S)98 %1 01/26/11 05:10 1868-53-770-130
4-Bromofluorobenzene (S)100 %1 01/26/11 05:10 460-00-470-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 15 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW3 Lab ID:9286253003 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene-d8 (S)97 %1 01/26/11 05:10 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 16 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW4 Lab ID:9286253004 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15122
Aliphatic (C19-C36)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15122
Aromatic (C11-C22)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15122
Nonatriacontane (S)80 %1 01/28/11 06:10 7194-86-701/26/11 14:1540-140
o-Terphenyl (S)71 %1 01/28/11 06:10 84-15-101/26/11 14:1540-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 01/25/11 23:51 N2100
Aliphatic (C09-C12)ND ug/L 1 01/25/11 23:51 N2100
Aromatic (C09-C10)ND ug/L 1 01/25/11 23:51 N2100
2,5-Dibromotoluene (PID)(S)100 %1 01/25/11 23:5170-130
2,5-Dibromotoluene (FID)(S)97 %1 01/25/11 23:5170-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 01/24/11 21:57 7439-92-101/22/11 09:305.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 01/28/11 19:22 83-32-901/26/11 09:455.7
Acenaphthylene ND ug/L 1 01/28/11 19:22 208-96-801/26/11 09:455.7
Anthracene ND ug/L 1 01/28/11 19:22 120-12-701/26/11 09:455.7
Benzo(a)anthracene ND ug/L 1 01/28/11 19:22 56-55-301/26/11 09:455.7
Benzo(a)pyrene ND ug/L 1 01/28/11 19:22 50-32-801/26/11 09:455.7
Benzo(b)fluoranthene ND ug/L 1 01/28/11 19:22 205-99-201/26/11 09:455.7
Benzo(g,h,i)perylene ND ug/L 1 01/28/11 19:22 191-24-201/26/11 09:455.7
Benzo(k)fluoranthene ND ug/L 1 01/28/11 19:22 207-08-901/26/11 09:455.7
4-Bromophenylphenyl ether ND ug/L 1 01/28/11 19:22 101-55-301/26/11 09:455.7
Butylbenzylphthalate ND ug/L 1 01/28/11 19:22 85-68-701/26/11 09:455.7
4-Chloro-3-methylphenol ND ug/L 1 01/28/11 19:22 59-50-701/26/11 09:455.7
bis(2-Chloroethoxy)methane ND ug/L 1 01/28/11 19:22 111-91-101/26/11 09:4511.5
bis(2-Chloroethyl) ether ND ug/L 1 01/28/11 19:22 111-44-401/26/11 09:455.7
bis(2-Chloroisopropyl) ether ND ug/L 1 01/28/11 19:22 108-60-101/26/11 09:455.7
2-Chloronaphthalene ND ug/L 1 01/28/11 19:22 91-58-701/26/11 09:455.7
2-Chlorophenol ND ug/L 1 01/28/11 19:22 95-57-801/26/11 09:455.7
4-Chlorophenylphenyl ether ND ug/L 1 01/28/11 19:22 7005-72-301/26/11 09:455.7
Chrysene ND ug/L 1 01/28/11 19:22 218-01-901/26/11 09:455.7
Dibenz(a,h)anthracene ND ug/L 1 01/28/11 19:22 53-70-301/26/11 09:455.7
3,3'-Dichlorobenzidine ND ug/L 1 01/28/11 19:22 91-94-101/26/11 09:4528.7
2,4-Dichlorophenol ND ug/L 1 01/28/11 19:22 120-83-201/26/11 09:455.7
Diethylphthalate ND ug/L 1 01/28/11 19:22 84-66-201/26/11 09:455.7
2,4-Dimethylphenol ND ug/L 1 01/28/11 19:22 105-67-901/26/11 09:4511.5
Dimethylphthalate ND ug/L 1 01/28/11 19:22 131-11-301/26/11 09:455.7
Di-n-butylphthalate ND ug/L 1 01/28/11 19:22 84-74-201/26/11 09:455.7
4,6-Dinitro-2-methylphenol ND ug/L 1 01/28/11 19:22 534-52-101/26/11 09:4523.0
2,4-Dinitrophenol ND ug/L 1 01/28/11 19:22 51-28-501/26/11 09:4557.5
2,4-Dinitrotoluene ND ug/L 1 01/28/11 19:22 121-14-201/26/11 09:455.7
2,6-Dinitrotoluene ND ug/L 1 01/28/11 19:22 606-20-201/26/11 09:455.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 17 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW4 Lab ID:9286253004 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 01/28/11 19:22 117-84-001/26/11 09:455.7
bis(2-Ethylhexyl)phthalate ND ug/L 1 01/28/11 19:22 117-81-701/26/11 09:455.7
Fluoranthene ND ug/L 1 01/28/11 19:22 206-44-001/26/11 09:455.7
Fluorene ND ug/L 1 01/28/11 19:22 86-73-701/26/11 09:455.7
Hexachloro-1,3-butadiene ND ug/L 1 01/28/11 19:22 87-68-301/26/11 09:455.7
Hexachlorobenzene ND ug/L 1 01/28/11 19:22 118-74-101/26/11 09:455.7
Hexachlorocyclopentadiene ND ug/L 1 01/28/11 19:22 77-47-401/26/11 09:4511.5
Hexachloroethane ND ug/L 1 01/28/11 19:22 67-72-101/26/11 09:455.7
Indeno(1,2,3-cd)pyrene ND ug/L 1 01/28/11 19:22 193-39-501/26/11 09:455.7
Isophorone ND ug/L 1 01/28/11 19:22 78-59-101/26/11 09:4511.5
Naphthalene ND ug/L 1 01/28/11 19:22 91-20-301/26/11 09:455.7
Nitrobenzene ND ug/L 1 01/28/11 19:22 98-95-301/26/11 09:455.7
2-Nitrophenol ND ug/L 1 01/28/11 19:22 88-75-501/26/11 09:455.7
4-Nitrophenol ND ug/L 1 01/28/11 19:22 100-02-701/26/11 09:4557.5
N-Nitrosodimethylamine ND ug/L 1 01/28/11 19:22 62-75-901/26/11 09:455.7
N-Nitroso-di-n-propylamine ND ug/L 1 01/28/11 19:22 621-64-701/26/11 09:455.7
N-Nitrosodiphenylamine ND ug/L 1 01/28/11 19:22 86-30-601/26/11 09:4511.5
Pentachlorophenol ND ug/L 1 01/28/11 19:22 87-86-501/26/11 09:4528.7
Phenanthrene ND ug/L 1 01/28/11 19:22 85-01-801/26/11 09:455.7
Phenol ND ug/L 1 01/28/11 19:22 108-95-201/26/11 09:455.7
Pyrene ND ug/L 1 01/28/11 19:22 129-00-001/26/11 09:455.7
1,2,4-Trichlorobenzene ND ug/L 1 01/28/11 19:22 120-82-101/26/11 09:455.7
2,4,6-Trichlorophenol ND ug/L 1 01/28/11 19:22 88-06-201/26/11 09:4511.5
Nitrobenzene-d5 (S)64 %1 01/28/11 19:22 4165-60-001/26/11 09:4510-120
2-Fluorobiphenyl (S)71 %1 01/28/11 19:22 321-60-801/26/11 09:4515-120
Terphenyl-d14 (S)82 %1 01/28/11 19:22 1718-51-001/26/11 09:4511-131
Phenol-d6 (S)34 %1 01/28/11 19:22 13127-88-301/26/11 09:4510-120
2-Fluorophenol (S)47 %1 01/28/11 19:22 367-12-401/26/11 09:4510-120
2,4,6-Tribromophenol (S)74 %1 01/28/11 19:22 118-79-601/26/11 09:4510-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 01/26/11 05:33 71-43-20.50
Bromobenzene ND ug/L 1 01/26/11 05:33 108-86-10.50
Bromochloromethane ND ug/L 1 01/26/11 05:33 74-97-50.50
Bromodichloromethane ND ug/L 1 01/26/11 05:33 75-27-40.50
Bromoform ND ug/L 1 01/26/11 05:33 75-25-20.50
Bromomethane ND ug/L 1 01/26/11 05:33 74-83-95.0
n-Butylbenzene ND ug/L 1 01/26/11 05:33 104-51-80.50
sec-Butylbenzene ND ug/L 1 01/26/11 05:33 135-98-80.50
tert-Butylbenzene ND ug/L 1 01/26/11 05:33 98-06-60.50
Carbon tetrachloride ND ug/L 1 01/26/11 05:33 56-23-50.50
Chlorobenzene ND ug/L 1 01/26/11 05:33 108-90-70.50
Chloroethane ND ug/L 1 01/26/11 05:33 75-00-31.0
Chloroform ND ug/L 1 01/26/11 05:33 67-66-30.50
Chloromethane ND ug/L 1 01/26/11 05:33 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/26/11 05:33 95-49-80.50
4-Chlorotoluene ND ug/L 1 01/26/11 05:33 106-43-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 18 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW4 Lab ID:9286253004 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2-Dibromo-3-chloropropane ND ug/L 1 01/26/11 05:33 96-12-81.0
Dibromochloromethane ND ug/L 1 01/26/11 05:33 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 01/26/11 05:33 106-93-40.50
Dibromomethane ND ug/L 1 01/26/11 05:33 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 01/26/11 05:33 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 01/26/11 05:33 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 01/26/11 05:33 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 01/26/11 05:33 75-71-80.50
1,1-Dichloroethane ND ug/L 1 01/26/11 05:33 75-34-30.50
1,2-Dichloroethane ND ug/L 1 01/26/11 05:33 107-06-20.50
1,1-Dichloroethene ND ug/L 1 01/26/11 05:33 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 01/26/11 05:33 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 01/26/11 05:33 156-60-50.50
1,2-Dichloropropane ND ug/L 1 01/26/11 05:33 78-87-50.50
1,3-Dichloropropane ND ug/L 1 01/26/11 05:33 142-28-90.50
2,2-Dichloropropane ND ug/L 1 01/26/11 05:33 594-20-70.50
1,1-Dichloropropene ND ug/L 1 01/26/11 05:33 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 01/26/11 05:33 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 01/26/11 05:33 10061-02-60.50
Diisopropyl ether ND ug/L 1 01/26/11 05:33 108-20-30.50
Ethylbenzene ND ug/L 1 01/26/11 05:33 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 01/26/11 05:33 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 01/26/11 05:33 98-82-80.50
Methylene Chloride ND ug/L 1 01/26/11 05:33 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 01/26/11 05:33 1634-04-40.50
Naphthalene ND ug/L 1 01/26/11 05:33 91-20-32.0
n-Propylbenzene ND ug/L 1 01/26/11 05:33 103-65-10.50
Styrene ND ug/L 1 01/26/11 05:33 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 01/26/11 05:33 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 01/26/11 05:33 79-34-50.50
Tetrachloroethene ND ug/L 1 01/26/11 05:33 127-18-40.50
Toluene ND ug/L 1 01/26/11 05:33 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 01/26/11 05:33 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 01/26/11 05:33 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 01/26/11 05:33 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 01/26/11 05:33 79-00-50.50
Trichloroethene ND ug/L 1 01/26/11 05:33 79-01-60.50
Trichlorofluoromethane ND ug/L 1 01/26/11 05:33 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/26/11 05:33 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 01/26/11 05:33 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 01/26/11 05:33 108-67-80.50
Vinyl chloride ND ug/L 1 01/26/11 05:33 75-01-41.0
m&p-Xylene ND ug/L 1 01/26/11 05:33 179601-23-11.0
o-Xylene ND ug/L 1 01/26/11 05:33 95-47-60.50
1,2-Dichloroethane-d4 (S)119 %1 01/26/11 05:33 17060-07-070-130
Dibromofluoromethane (S)116 %1 01/26/11 05:33 1868-53-770-130
4-Bromofluorobenzene (S)100 %1 01/26/11 05:33 460-00-470-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 19 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:MW4 Lab ID:9286253004 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene-d8 (S)100 %1 01/26/11 05:33 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 20 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:WSW1 Lab ID:9286253005 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15100
Aliphatic (C19-C36)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15100
Aromatic (C11-C22)ND ug/L 1 01/28/11 06:10 N201/26/11 14:15100
Nonatriacontane (S)70 %1 01/28/11 06:10 7194-86-701/26/11 14:1540-140
o-Terphenyl (S)79 %1 01/28/11 06:10 84-15-101/26/11 14:1540-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 01/26/11 00:15 N2100
Aliphatic (C09-C12)ND ug/L 1 01/26/11 00:15 N2100
Aromatic (C09-C10)ND ug/L 1 01/26/11 00:15 N2100
2,5-Dibromotoluene (PID)(S)116 %1 01/26/11 00:1570-130
2,5-Dibromotoluene (FID)(S)115 %1 01/26/11 00:1570-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 01/24/11 22:00 7439-92-101/22/11 09:305.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 01/28/11 19:50 83-32-901/26/11 09:455.0
Acenaphthylene ND ug/L 1 01/28/11 19:50 208-96-801/26/11 09:455.0
Anthracene ND ug/L 1 01/28/11 19:50 120-12-701/26/11 09:455.0
Benzo(a)anthracene ND ug/L 1 01/28/11 19:50 56-55-301/26/11 09:455.0
Benzo(a)pyrene ND ug/L 1 01/28/11 19:50 50-32-801/26/11 09:455.0
Benzo(b)fluoranthene ND ug/L 1 01/28/11 19:50 205-99-201/26/11 09:455.0
Benzo(g,h,i)perylene ND ug/L 1 01/28/11 19:50 191-24-201/26/11 09:455.0
Benzo(k)fluoranthene ND ug/L 1 01/28/11 19:50 207-08-901/26/11 09:455.0
4-Bromophenylphenyl ether ND ug/L 1 01/28/11 19:50 101-55-301/26/11 09:455.0
Butylbenzylphthalate ND ug/L 1 01/28/11 19:50 85-68-701/26/11 09:455.0
4-Chloro-3-methylphenol ND ug/L 1 01/28/11 19:50 59-50-701/26/11 09:455.0
bis(2-Chloroethoxy)methane ND ug/L 1 01/28/11 19:50 111-91-101/26/11 09:4510.0
bis(2-Chloroethyl) ether ND ug/L 1 01/28/11 19:50 111-44-401/26/11 09:455.0
bis(2-Chloroisopropyl) ether ND ug/L 1 01/28/11 19:50 108-60-101/26/11 09:455.0
2-Chloronaphthalene ND ug/L 1 01/28/11 19:50 91-58-701/26/11 09:455.0
2-Chlorophenol ND ug/L 1 01/28/11 19:50 95-57-801/26/11 09:455.0
4-Chlorophenylphenyl ether ND ug/L 1 01/28/11 19:50 7005-72-301/26/11 09:455.0
Chrysene ND ug/L 1 01/28/11 19:50 218-01-901/26/11 09:455.0
Dibenz(a,h)anthracene ND ug/L 1 01/28/11 19:50 53-70-301/26/11 09:455.0
3,3'-Dichlorobenzidine ND ug/L 1 01/28/11 19:50 91-94-101/26/11 09:4525.0
2,4-Dichlorophenol ND ug/L 1 01/28/11 19:50 120-83-201/26/11 09:455.0
Diethylphthalate ND ug/L 1 01/28/11 19:50 84-66-201/26/11 09:455.0
2,4-Dimethylphenol ND ug/L 1 01/28/11 19:50 105-67-901/26/11 09:4510.0
Dimethylphthalate ND ug/L 1 01/28/11 19:50 131-11-301/26/11 09:455.0
Di-n-butylphthalate ND ug/L 1 01/28/11 19:50 84-74-201/26/11 09:455.0
4,6-Dinitro-2-methylphenol ND ug/L 1 01/28/11 19:50 534-52-101/26/11 09:4520.0
2,4-Dinitrophenol ND ug/L 1 01/28/11 19:50 51-28-501/26/11 09:4550.0
2,4-Dinitrotoluene ND ug/L 1 01/28/11 19:50 121-14-201/26/11 09:455.0
2,6-Dinitrotoluene ND ug/L 1 01/28/11 19:50 606-20-201/26/11 09:455.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 21 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:WSW1 Lab ID:9286253005 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 01/28/11 19:50 117-84-001/26/11 09:455.0
bis(2-Ethylhexyl)phthalate ND ug/L 1 01/28/11 19:50 117-81-701/26/11 09:455.0
Fluoranthene ND ug/L 1 01/28/11 19:50 206-44-001/26/11 09:455.0
Fluorene ND ug/L 1 01/28/11 19:50 86-73-701/26/11 09:455.0
Hexachloro-1,3-butadiene ND ug/L 1 01/28/11 19:50 87-68-301/26/11 09:455.0
Hexachlorobenzene ND ug/L 1 01/28/11 19:50 118-74-101/26/11 09:455.0
Hexachlorocyclopentadiene ND ug/L 1 01/28/11 19:50 77-47-401/26/11 09:4510.0
Hexachloroethane ND ug/L 1 01/28/11 19:50 67-72-101/26/11 09:455.0
Indeno(1,2,3-cd)pyrene ND ug/L 1 01/28/11 19:50 193-39-501/26/11 09:455.0
Isophorone ND ug/L 1 01/28/11 19:50 78-59-101/26/11 09:4510.0
Naphthalene ND ug/L 1 01/28/11 19:50 91-20-301/26/11 09:455.0
Nitrobenzene ND ug/L 1 01/28/11 19:50 98-95-301/26/11 09:455.0
2-Nitrophenol ND ug/L 1 01/28/11 19:50 88-75-501/26/11 09:455.0
4-Nitrophenol ND ug/L 1 01/28/11 19:50 100-02-701/26/11 09:4550.0
N-Nitrosodimethylamine ND ug/L 1 01/28/11 19:50 62-75-901/26/11 09:455.0
N-Nitroso-di-n-propylamine ND ug/L 1 01/28/11 19:50 621-64-701/26/11 09:455.0
N-Nitrosodiphenylamine ND ug/L 1 01/28/11 19:50 86-30-601/26/11 09:4510.0
Pentachlorophenol ND ug/L 1 01/28/11 19:50 87-86-501/26/11 09:4525.0
Phenanthrene ND ug/L 1 01/28/11 19:50 85-01-801/26/11 09:455.0
Phenol ND ug/L 1 01/28/11 19:50 108-95-201/26/11 09:455.0
Pyrene ND ug/L 1 01/28/11 19:50 129-00-001/26/11 09:455.0
1,2,4-Trichlorobenzene ND ug/L 1 01/28/11 19:50 120-82-101/26/11 09:455.0
2,4,6-Trichlorophenol ND ug/L 1 01/28/11 19:50 88-06-201/26/11 09:4510.0
Nitrobenzene-d5 (S)59 %1 01/28/11 19:50 4165-60-001/26/11 09:4510-120
2-Fluorobiphenyl (S)64 %1 01/28/11 19:50 321-60-801/26/11 09:4515-120
Terphenyl-d14 (S)75 %1 01/28/11 19:50 1718-51-001/26/11 09:4511-131
Phenol-d6 (S)32 %1 01/28/11 19:50 13127-88-301/26/11 09:4510-120
2-Fluorophenol (S)44 %1 01/28/11 19:50 367-12-401/26/11 09:4510-120
2,4,6-Tribromophenol (S)69 %1 01/28/11 19:50 118-79-601/26/11 09:4510-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 01/27/11 17:11 71-43-20.50
Bromobenzene ND ug/L 1 01/27/11 17:11 108-86-10.50
Bromochloromethane ND ug/L 1 01/27/11 17:11 74-97-50.50
Bromodichloromethane ND ug/L 1 01/27/11 17:11 75-27-40.50
Bromoform ND ug/L 1 01/27/11 17:11 75-25-20.50
Bromomethane ND ug/L 1 01/27/11 17:11 74-83-95.0
n-Butylbenzene ND ug/L 1 01/27/11 17:11 104-51-80.50
sec-Butylbenzene ND ug/L 1 01/27/11 17:11 135-98-80.50
tert-Butylbenzene ND ug/L 1 01/27/11 17:11 98-06-60.50
Carbon tetrachloride ND ug/L 1 01/27/11 17:11 56-23-50.50
Chlorobenzene ND ug/L 1 01/27/11 17:11 108-90-70.50
Chloroethane ND ug/L 1 01/27/11 17:11 75-00-31.0
Chloroform ND ug/L 1 01/27/11 17:11 67-66-30.50
Chloromethane ND ug/L 1 01/27/11 17:11 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/27/11 17:11 95-49-80.50
4-Chlorotoluene ND ug/L 1 01/27/11 17:11 106-43-40.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 22 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:WSW1 Lab ID:9286253005 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
1,2-Dibromo-3-chloropropane ND ug/L 1 01/27/11 17:11 96-12-81.0
Dibromochloromethane ND ug/L 1 01/27/11 17:11 124-48-10.50
1,2-Dibromoethane (EDB)ND ug/L 1 01/27/11 17:11 106-93-40.50
Dibromomethane ND ug/L 1 01/27/11 17:11 74-95-30.50
1,2-Dichlorobenzene ND ug/L 1 01/27/11 17:11 95-50-10.50
1,3-Dichlorobenzene ND ug/L 1 01/27/11 17:11 541-73-10.50
1,4-Dichlorobenzene ND ug/L 1 01/27/11 17:11 106-46-70.50
Dichlorodifluoromethane ND ug/L 1 01/27/11 17:11 75-71-80.50
1,1-Dichloroethane ND ug/L 1 01/27/11 17:11 75-34-30.50
1,2-Dichloroethane ND ug/L 1 01/27/11 17:11 107-06-20.50
1,1-Dichloroethene ND ug/L 1 01/27/11 17:11 75-35-40.50
cis-1,2-Dichloroethene ND ug/L 1 01/27/11 17:11 156-59-20.50
trans-1,2-Dichloroethene ND ug/L 1 01/27/11 17:11 156-60-50.50
1,2-Dichloropropane ND ug/L 1 01/27/11 17:11 78-87-50.50
1,3-Dichloropropane ND ug/L 1 01/27/11 17:11 142-28-90.50
2,2-Dichloropropane ND ug/L 1 01/27/11 17:11 594-20-70.50
1,1-Dichloropropene ND ug/L 1 01/27/11 17:11 563-58-60.50
cis-1,3-Dichloropropene ND ug/L 1 01/27/11 17:11 10061-01-50.50
trans-1,3-Dichloropropene ND ug/L 1 01/27/11 17:11 10061-02-60.50
Diisopropyl ether ND ug/L 1 01/27/11 17:11 108-20-30.50
Ethylbenzene ND ug/L 1 01/27/11 17:11 100-41-40.50
Hexachloro-1,3-butadiene ND ug/L 1 01/27/11 17:11 87-68-32.0
Isopropylbenzene (Cumene)ND ug/L 1 01/27/11 17:11 98-82-80.50
Methylene Chloride ND ug/L 1 01/27/11 17:11 75-09-22.0
Methyl-tert-butyl ether ND ug/L 1 01/27/11 17:11 1634-04-40.50
Naphthalene ND ug/L 1 01/27/11 17:11 91-20-32.0
n-Propylbenzene ND ug/L 1 01/27/11 17:11 103-65-10.50
Styrene ND ug/L 1 01/27/11 17:11 100-42-50.50
1,1,1,2-Tetrachloroethane ND ug/L 1 01/27/11 17:11 630-20-60.50
1,1,2,2-Tetrachloroethane ND ug/L 1 01/27/11 17:11 79-34-50.50
Tetrachloroethene ND ug/L 1 01/27/11 17:11 127-18-40.50
Toluene ND ug/L 1 01/27/11 17:11 108-88-30.50
1,2,3-Trichlorobenzene ND ug/L 1 01/27/11 17:11 87-61-62.0
1,2,4-Trichlorobenzene ND ug/L 1 01/27/11 17:11 120-82-12.0
1,1,1-Trichloroethane ND ug/L 1 01/27/11 17:11 71-55-60.50
1,1,2-Trichloroethane ND ug/L 1 01/27/11 17:11 79-00-50.50
Trichloroethene ND ug/L 1 01/27/11 17:11 79-01-60.50
Trichlorofluoromethane ND ug/L 1 01/27/11 17:11 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/27/11 17:11 96-18-40.50
1,2,4-Trimethylbenzene ND ug/L 1 01/27/11 17:11 95-63-60.50
1,3,5-Trimethylbenzene ND ug/L 1 01/27/11 17:11 108-67-80.50
Vinyl chloride ND ug/L 1 01/27/11 17:11 75-01-41.0
m&p-Xylene ND ug/L 1 01/27/11 17:11 179601-23-11.0
o-Xylene ND ug/L 1 01/27/11 17:11 95-47-60.50
1,2-Dichloroethane-d4 (S)105 %1 01/27/11 17:11 17060-07-070-130
Dibromofluoromethane (S)102 %1 01/27/11 17:11 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 01/27/11 17:11 460-00-470-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 23 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Sample:WSW1 Lab ID:9286253005 Collected:01/19/11 16:30 Received:01/21/11 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene-d8 (S)102 %1 01/27/11 17:11 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 24 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/12498
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555892
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N201/31/11 20:25
Aliphatic (C19-C36)ug/L ND 100 N201/31/11 20:25
Aromatic (C11-C22)ug/L ND 100 N201/31/11 20:25
2-Bromonaphthalene (S)%97 40-140 01/31/11 20:25
2-Fluorobiphenyl (S)%94 40-140 01/31/11 20:25
Nonatriacontane (S)%91 40-140 01/31/11 20:25
o-Terphenyl (S)%80 40-140 01/31/11 20:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555893LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
555894
Aliphatic (C09-C18)ug/L 226 N23007540-14084252 11 50
Aliphatic (C19-C36)ug/L 304 N24007640-140108432 35 50
Aromatic (C11-C22)ug/L 686 N28508140-14090766 11 50
2-Bromonaphthalene (S)%84 40-14088
2-Fluorobiphenyl (S)%90 40-14094
Nonatriacontane (S)%89 40-14099
o-Terphenyl (S)%73 40-14084
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 25 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/4668
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555263
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 100 N201/25/11 15:56
Aliphatic (C09-C12)ug/L ND 100 N201/25/11 15:56
Aromatic (C09-C10)ug/L ND 100 N201/25/11 15:56
2,5-Dibromotoluene (FID)(S)%102 70-130 01/25/11 15:56
2,5-Dibromotoluene (PID)(S)%106 70-130 01/25/11 15:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555264LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
555265
Aliphatic (C05-C08)ug/L 297 N23009970-13093280 6 25
Aliphatic (C09-C12)ug/L 351 N230011730-130116349 1 25
Aromatic (C09-C10)ug/L 104 N210010470-130102102 2 25
2,5-Dibromotoluene (FID)(S)%110 70-130102
2,5-Dibromotoluene (PID)(S)%118 70-130110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 26 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/7762
SM 3030C
EPA 200.7
200.7 MET 3030C
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:554590
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Matrix:Water
Analyzed
Lead ug/L ND 5.0 01/24/11 21:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
554591LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 527500 105 85-115
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
554592MATRIX SPIKE SAMPLE:
MSSpike
Result
9286246001
Lead ug/L 556500 107 70-13021.0
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
554594MATRIX SPIKE SAMPLE:
MSSpike
Result
9286070001
Lead ug/L 493500 98 70-130ND
Parameter Units
Dup
Result QualifiersRPDResult
9286246002
554593SAMPLE DUPLICATE:
Lead ug/L 35.8 1132.1
Parameter Units
Dup
Result QualifiersRPDResult
9286218001
554595SAMPLE DUPLICATE:
Lead ug/L 6.7 57.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 27 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/12489
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555657
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 01/27/11 15:55
2,4,6-Trichlorophenol ug/L ND 10.0 01/27/11 15:55
2,4-Dichlorophenol ug/L ND 5.0 01/27/11 15:55
2,4-Dimethylphenol ug/L ND 10.0 01/27/11 15:55
2,4-Dinitrophenol ug/L ND 50.0 01/27/11 15:55
2,4-Dinitrotoluene ug/L ND 5.0 01/27/11 15:55
2,6-Dinitrotoluene ug/L ND 5.0 01/27/11 15:55
2-Chloronaphthalene ug/L ND 5.0 01/27/11 15:55
2-Chlorophenol ug/L ND 5.0 01/27/11 15:55
2-Nitrophenol ug/L ND 5.0 01/27/11 15:55
3,3'-Dichlorobenzidine ug/L ND 25.0 01/27/11 15:55
4,6-Dinitro-2-methylphenol ug/L ND 20.0 01/27/11 15:55
4-Bromophenylphenyl ether ug/L ND 5.0 01/27/11 15:55
4-Chloro-3-methylphenol ug/L ND 5.0 01/27/11 15:55
4-Chlorophenylphenyl ether ug/L ND 5.0 01/27/11 15:55
4-Nitrophenol ug/L ND 50.0 01/27/11 15:55
Acenaphthene ug/L ND 5.0 01/27/11 15:55
Acenaphthylene ug/L ND 5.0 01/27/11 15:55
Anthracene ug/L ND 5.0 01/27/11 15:55
Benzo(a)anthracene ug/L ND 5.0 01/27/11 15:55
Benzo(a)pyrene ug/L ND 5.0 01/27/11 15:55
Benzo(b)fluoranthene ug/L ND 5.0 01/27/11 15:55
Benzo(g,h,i)perylene ug/L ND 5.0 01/27/11 15:55
Benzo(k)fluoranthene ug/L ND 5.0 01/27/11 15:55
bis(2-Chloroethoxy)methane ug/L ND 10.0 01/27/11 15:55
bis(2-Chloroethyl) ether ug/L ND 5.0 01/27/11 15:55
bis(2-Chloroisopropyl) ether ug/L ND 5.0 01/27/11 15:55
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 01/27/11 15:55
Butylbenzylphthalate ug/L ND 5.0 01/27/11 15:55
Chrysene ug/L ND 5.0 01/27/11 15:55
Di-n-butylphthalate ug/L ND 5.0 01/27/11 15:55
Di-n-octylphthalate ug/L ND 5.0 01/27/11 15:55
Dibenz(a,h)anthracene ug/L ND 5.0 01/27/11 15:55
Diethylphthalate ug/L ND 5.0 01/27/11 15:55
Dimethylphthalate ug/L ND 5.0 01/27/11 15:55
Fluoranthene ug/L ND 5.0 01/27/11 15:55
Fluorene ug/L ND 5.0 01/27/11 15:55
Hexachloro-1,3-butadiene ug/L ND 5.0 01/27/11 15:55
Hexachlorobenzene ug/L ND 5.0 01/27/11 15:55
Hexachlorocyclopentadiene ug/L ND 10.0 01/27/11 15:55
Hexachloroethane ug/L ND 5.0 01/27/11 15:55
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 01/27/11 15:55
Isophorone ug/L ND 10.0 01/27/11 15:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 28 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555657
Associated Lab Samples:9286253001, 9286253002, 9286253003, 9286253004, 9286253005
Matrix:Water
Analyzed
N-Nitroso-di-n-propylamine ug/L ND 5.0 01/27/11 15:55
N-Nitrosodimethylamine ug/L ND 5.0 01/27/11 15:55
N-Nitrosodiphenylamine ug/L ND 10.0 01/27/11 15:55
Naphthalene ug/L ND 5.0 01/27/11 15:55
Nitrobenzene ug/L ND 5.0 01/27/11 15:55
Pentachlorophenol ug/L ND 25.0 01/27/11 15:55
Phenanthrene ug/L ND 5.0 01/27/11 15:55
Phenol ug/L ND 5.0 01/27/11 15:55
Pyrene ug/L ND 5.0 01/27/11 15:55
2,4,6-Tribromophenol (S)%73 10-137 01/27/11 15:55
2-Fluorobiphenyl (S)%63 15-120 01/27/11 15:55
2-Fluorophenol (S)%41 10-120 01/27/11 15:55
Nitrobenzene-d5 (S)%63 10-120 01/27/11 15:55
Phenol-d6 (S)%27 10-120 01/27/11 15:55
Terphenyl-d14 (S)%79 11-131 01/27/11 15:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555658LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 31.850 64 44-142
2,4,6-Trichlorophenol ug/L 38.450 77 37-144
2,4-Dichlorophenol ug/L 41.350 83 1-191
2,4-Dimethylphenol ug/L 39.750 79 32-119
2,4-Dinitrophenol ug/L 15.5J250 6 1-181
2,4-Dinitrotoluene ug/L 40.050 80 39-139
2,6-Dinitrotoluene ug/L 40.750 81 50-158
2-Chloronaphthalene ug/L 38.450 77 60-118
2-Chlorophenol ug/L 36.450 73 23-134
2-Nitrophenol ug/L 35.150 70 29-182
3,3'-Dichlorobenzidine ug/L 72.5100 72 1-262
4,6-Dinitro-2-methylphenol ug/L 50.1100 50 1-181
4-Bromophenylphenyl ether ug/L 36.950 74 53-127
4-Chloro-3-methylphenol ug/L 88.1100 88 22-147
4-Chlorophenylphenyl ether ug/L 38.250 76 25-158
4-Nitrophenol ug/L 66.3250 27 1-132
Acenaphthene ug/L 40.450 81 47-145
Acenaphthylene ug/L 39.750 79 33-145
Anthracene ug/L 41.150 82 1-166
Benzo(a)anthracene ug/L 41.750 83 33-143
Benzo(a)pyrene ug/L 38.650 77 17-163
Benzo(b)fluoranthene ug/L 40.150 80 24-159
Benzo(g,h,i)perylene ug/L 40.050 80 1-219
Benzo(k)fluoranthene ug/L 39.950 80 11-162
bis(2-Chloroethoxy)methane ug/L 34.950 70 33-184
bis(2-Chloroethyl) ether ug/L 35.550 71 12-158
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 29 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555658LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroisopropyl) ether ug/L 32.050 64 36-166
bis(2-Ethylhexyl)phthalate ug/L 36.650 73 8-158
Butylbenzylphthalate ug/L 37.350 75 1-152
Chrysene ug/L 40.950 82 17-168
Di-n-butylphthalate ug/L 37.850 76 1-118
Di-n-octylphthalate ug/L 32.550 65 4-146
Dibenz(a,h)anthracene ug/L 40.550 81 1-227
Diethylphthalate ug/L 38.650 77 1-114
Dimethylphthalate ug/L 37.650 75 1-112
Fluoranthene ug/L 42.250 84 26-137
Fluorene ug/L 41.950 84 59-121
Hexachloro-1,3-butadiene ug/L 27.350 55 24-116
Hexachlorobenzene ug/L 38.550 77 1-152
Hexachlorocyclopentadiene ug/L 26.350 53 25-150
Hexachloroethane ug/L 26.850 54 40-113
Indeno(1,2,3-cd)pyrene ug/L 40.050 80 1-171
Isophorone ug/L 41.450 83 21-196
N-Nitroso-di-n-propylamine ug/L 41.350 83 1-230
N-Nitrosodimethylamine ug/L 24.550 49 25-150
N-Nitrosodiphenylamine ug/L 39.050 78 25-150
Naphthalene ug/L 35.150 70 21-133
Nitrobenzene ug/L 35.350 71 35-180
Pentachlorophenol ug/L 76.6100 77 14-176
Phenanthrene ug/L 40.650 81 54-120
Phenol ug/L 17.950 36 5-112
Pyrene ug/L 42.250 84 52-115
2,4,6-Tribromophenol (S)%83 10-137
2-Fluorobiphenyl (S)%69 15-120
2-Fluorophenol (S)%44 10-120
Nitrobenzene-d5 (S)%70 10-120
Phenol-d6 (S)%32 10-120
Terphenyl-d14 (S)%79 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
555659MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286246005
555660
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 74 44-14276 3100ND73.8 75.7
2,4,6-Trichlorophenol ug/L 100 83 37-14487 4100ND83.3 86.8
2,4-Dichlorophenol ug/L 100 96 1-191100 4100ND95.7 99.8
2,4-Dimethylphenol ug/L 100 93 32-11996 3100ND92.8 95.5
2,4-Dinitrophenol ug/L 500 59 1-18177 27500ND294385
2,4-Dinitrotoluene ug/L 100 89 39-13995 6100ND88.8 94.6
2,6-Dinitrotoluene ug/L 100 86 50-15891 6100ND85.9 91.4
2-Chloronaphthalene ug/L 100 82 60-11884 3100ND81.5 84.1
2-Chlorophenol ug/L 100 81 23-13491 11100ND81.2 90.9
2-Nitrophenol ug/L 100 74 29-18282 11100ND73.5 82.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 30 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
555659MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286246005
555660
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3,3'-Dichlorobenzidine ug/L 200 82 1-26285 4200ND164171
4,6-Dinitro-2-methylphenol ug/L 200 67 1-18182 20200ND135165
4-Bromophenylphenyl ether ug/L 100 77 53-12780 4100ND76.5 79.8
4-Chloro-3-methylphenol ug/L 200 101 22-147105 4200ND202211
4-Chlorophenylphenyl ether ug/L 100 81 25-15884 4100ND81.1 84.1
4-Nitrophenol ug/L 500 72 1-13274 3500ND358370
Acenaphthene ug/L 100 86 47-14587 1100ND85.6 86.6
Acenaphthylene ug/L 100 83 33-14586 5100ND82.5 86.3
Anthracene ug/L 100 85 1-16688 3100ND85.0 87.7
Benzo(a)anthracene ug/L 100 87 33-14390 3100ND86.9 89.9
Benzo(a)pyrene ug/L 100 81 17-16383 3100ND80.5 83.2
Benzo(b)fluoranthene ug/L 100 83 24-15987 5100ND82.9 86.7
Benzo(g,h,i)perylene ug/L 100 87 1-21987 1100ND87.0 86.5
Benzo(k)fluoranthene ug/L 100 84 11-16285 1100ND84.1 85.3
bis(2-Chloroethoxy)methane ug/L 100 74 33-18478 5100ND74.1 78.0
bis(2-Chloroethyl) ether ug/L 100 71 12-15880 12100ND70.6 79.9
bis(2-Chloroisopropyl) ether ug/L 100 64 36-16672 11100ND64.4 71.5
bis(2-Ethylhexyl)phthalate ug/L 100 76 8-15883 8100ND76.0 82.7
Butylbenzylphthalate ug/L 100 75 1-15281 8100ND74.5 80.9
Chrysene ug/L 100 85 17-16888 3100ND85.5 88.0
Di-n-butylphthalate ug/L 100 81 1-11884 4100ND81.0 84.4
Di-n-octylphthalate ug/L 100 73 4-14678 6100ND73.5 77.9
Dibenz(a,h)anthracene ug/L 100 88 1-22788 0100ND87.8 88.2
Diethylphthalate ug/L 100 82 1-11485 4100ND81.9 85.2
Dimethylphthalate ug/L 100 79 1-11282 4100ND79.2 82.1
Fluoranthene ug/L 100 98 26-13795 3100ND98.0 94.7
Fluorene ug/L 100 89 59-12191 2100ND88.7 90.6
Hexachloro-1,3-butadiene ug/L 100 69 24-11667 3100ND69.1 67.3
Hexachlorobenzene ug/L 100 79 1-15283 4100ND79.3 82.9
Hexachlorocyclopentadiene ug/L 100 66 25-15070 5100ND66.2 69.8
Hexachloroethane ug/L 100 62 40-11362 1100ND61.6 62.2
Indeno(1,2,3-cd)pyrene ug/L 100 87 1-17187 1100ND86.5 87.2
Isophorone ug/L 100 81 21-19689 10100ND80.5 89.0
N-Nitroso-di-n-propylamine ug/L 100 72 1-23091 24100ND71.6 91.2
N-Nitrosodimethylamine ug/L 100 59 25-15069 15100ND59.4 68.7
N-Nitrosodiphenylamine ug/L 100 80 25-15084 4100ND79.9 83.5
Naphthalene ug/L 100 77 21-13380 3100ND77.5 79.8
Nitrobenzene ug/L 100 74 35-18075 2100ND73.8 75.5
Pentachlorophenol ug/L 200 80 14-17690 13200ND159181
Phenanthrene ug/L 100 84 54-12087 3100ND84.4 87.1
Phenol ug/L 100 60 5-11272 18100ND59.5 71.6
Pyrene ug/L 100 79 52-11587 9100ND79.5 86.7
2,4,6-Tribromophenol (S)%93 10-13797
2-Fluorobiphenyl (S)%73 15-12075
2-Fluorophenol (S)%59 10-12067
Nitrobenzene-d5 (S)%73 10-12076
Phenol-d6 (S)%50 10-12061
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 31 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
555659MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286246005
555660
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Terphenyl-d14 (S)%76 11-13184
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 32 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/13833
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9286253001, 9286253003, 9286253004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555205
Associated Lab Samples:9286253001, 9286253003, 9286253004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/26/11 00:35
1,1,1-Trichloroethane ug/L ND 0.50 01/26/11 00:35
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/26/11 00:35
1,1,2-Trichloroethane ug/L ND 0.50 01/26/11 00:35
1,1-Dichloroethane ug/L ND 0.50 01/26/11 00:35
1,1-Dichloroethene ug/L ND 0.50 01/26/11 00:35
1,1-Dichloropropene ug/L ND 0.50 01/26/11 00:35
1,2,3-Trichlorobenzene ug/L ND 2.0 01/26/11 00:35
1,2,3-Trichloropropane ug/L ND 0.50 01/26/11 00:35
1,2,4-Trichlorobenzene ug/L ND 2.0 01/26/11 00:35
1,2,4-Trimethylbenzene ug/L ND 0.50 01/26/11 00:35
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/26/11 00:35
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/26/11 00:35
1,2-Dichlorobenzene ug/L ND 0.50 01/26/11 00:35
1,2-Dichloroethane ug/L ND 0.50 01/26/11 00:35
1,2-Dichloropropane ug/L ND 0.50 01/26/11 00:35
1,3,5-Trimethylbenzene ug/L ND 0.50 01/26/11 00:35
1,3-Dichlorobenzene ug/L ND 0.50 01/26/11 00:35
1,3-Dichloropropane ug/L ND 0.50 01/26/11 00:35
1,4-Dichlorobenzene ug/L ND 0.50 01/26/11 00:35
2,2-Dichloropropane ug/L ND 0.50 01/26/11 00:35
2-Chlorotoluene ug/L ND 0.50 01/26/11 00:35
4-Chlorotoluene ug/L ND 0.50 01/26/11 00:35
Benzene ug/L ND 0.50 01/26/11 00:35
Bromobenzene ug/L ND 0.50 01/26/11 00:35
Bromochloromethane ug/L ND 0.50 01/26/11 00:35
Bromodichloromethane ug/L ND 0.50 01/26/11 00:35
Bromoform ug/L ND 0.50 01/26/11 00:35
Bromomethane ug/L ND 5.0 01/26/11 00:35
Carbon tetrachloride ug/L ND 0.50 01/26/11 00:35
Chlorobenzene ug/L ND 0.50 01/26/11 00:35
Chloroethane ug/L ND 1.0 01/26/11 00:35
Chloroform ug/L ND 0.50 01/26/11 00:35
Chloromethane ug/L ND 1.0 01/26/11 00:35
cis-1,2-Dichloroethene ug/L ND 0.50 01/26/11 00:35
cis-1,3-Dichloropropene ug/L ND 0.50 01/26/11 00:35
Dibromochloromethane ug/L ND 0.50 01/26/11 00:35
Dibromomethane ug/L ND 0.50 01/26/11 00:35
Dichlorodifluoromethane ug/L ND 0.50 01/26/11 00:35
Diisopropyl ether ug/L ND 0.50 01/26/11 00:35
Ethylbenzene ug/L ND 0.50 01/26/11 00:35
Hexachloro-1,3-butadiene ug/L ND 2.0 01/26/11 00:35
Isopropylbenzene (Cumene)ug/L ND 0.50 01/26/11 00:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 33 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555205
Associated Lab Samples:9286253001, 9286253003, 9286253004
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 01/26/11 00:35
Methyl-tert-butyl ether ug/L ND 0.50 01/26/11 00:35
Methylene Chloride ug/L ND 2.0 01/26/11 00:35
n-Butylbenzene ug/L ND 0.50 01/26/11 00:35
n-Propylbenzene ug/L ND 0.50 01/26/11 00:35
Naphthalene ug/L ND 2.0 01/26/11 00:35
o-Xylene ug/L ND 0.50 01/26/11 00:35
sec-Butylbenzene ug/L ND 0.50 01/26/11 00:35
Styrene ug/L ND 0.50 01/26/11 00:35
tert-Butylbenzene ug/L ND 0.50 01/26/11 00:35
Tetrachloroethene ug/L ND 0.50 01/26/11 00:35
Toluene ug/L ND 0.50 01/26/11 00:35
trans-1,2-Dichloroethene ug/L ND 0.50 01/26/11 00:35
trans-1,3-Dichloropropene ug/L ND 0.50 01/26/11 00:35
Trichloroethene ug/L ND 0.50 01/26/11 00:35
Trichlorofluoromethane ug/L ND 1.0 01/26/11 00:35
Vinyl chloride ug/L ND 1.0 01/26/11 00:35
1,2-Dichloroethane-d4 (S)%117 70-130 01/26/11 00:35
4-Bromofluorobenzene (S)%97 70-130 01/26/11 00:35
Dibromofluoromethane (S)%114 70-130 01/26/11 00:35
Toluene-d8 (S)%99 70-130 01/26/11 00:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555206LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.550 89 60-140
1,1,1-Trichloroethane ug/L 45.650 91 60-140
1,1,2,2-Tetrachloroethane ug/L 47.150 94 60-140
1,1,2-Trichloroethane ug/L 50.950 102 60-140
1,1-Dichloroethane ug/L 47.450 95 60-140
1,1-Dichloroethene ug/L 43.750 87 60-140
1,1-Dichloropropene ug/L 51.450 103 60-140
1,2,3-Trichlorobenzene ug/L 45.950 92 60-140
1,2,3-Trichloropropane ug/L 48.050 96 60-140
1,2,4-Trichlorobenzene ug/L 42.250 84 60-140
1,2,4-Trimethylbenzene ug/L 50.050 100 60-140
1,2-Dibromo-3-chloropropane ug/L 50.450 101 60-140
1,2-Dibromoethane (EDB)ug/L 51.850 104 60-140
1,2-Dichlorobenzene ug/L 50.750 101 60-140
1,2-Dichloroethane ug/L 47.750 95 60-140
1,2-Dichloropropane ug/L 47.850 96 60-140
1,3,5-Trimethylbenzene ug/L 50.050 100 60-140
1,3-Dichlorobenzene ug/L 50.750 101 60-140
1,3-Dichloropropane ug/L 52.650 105 60-140
1,4-Dichlorobenzene ug/L 45.450 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 34 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555206LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 44.150 88 60-140
2-Chlorotoluene ug/L 54.550 109 60-140
4-Chlorotoluene ug/L 54.850 110 60-140
Benzene ug/L 48.650 97 60-140
Bromobenzene ug/L 48.650 97 60-140
Bromochloromethane ug/L 49.850 100 60-140
Bromodichloromethane ug/L 47.550 95 60-140
Bromoform ug/L 49.350 99 60-140
Bromomethane ug/L 58.350 117 60-140
Carbon tetrachloride ug/L 44.750 89 60-140
Chlorobenzene ug/L 45.350 91 60-140
Chloroethane ug/L 45.450 91 60-140
Chloroform ug/L 46.150 92 60-140
Chloromethane ug/L 46.550 93 60-140
cis-1,2-Dichloroethene ug/L 47.250 94 60-140
cis-1,3-Dichloropropene ug/L 48.150 96 60-140
Dibromochloromethane ug/L 48.950 98 60-140
Dibromomethane ug/L 47.050 94 60-140
Dichlorodifluoromethane ug/L 40.150 80 60-140
Diisopropyl ether ug/L 54.650 109 60-140
Ethylbenzene ug/L 50.250 100 60-140
Hexachloro-1,3-butadiene ug/L 46.350 93 60-140
Isopropylbenzene (Cumene)ug/L 49.050 98 60-140
m&p-Xylene ug/L 110100 110 60-140
Methyl-tert-butyl ether ug/L 52.950 106 60-140
Methylene Chloride ug/L 46.250 92 60-140
n-Butylbenzene ug/L 48.450 97 60-140
n-Propylbenzene ug/L 53.350 107 60-140
Naphthalene ug/L 46.450 93 60-140
o-Xylene ug/L 48.750 97 60-140
sec-Butylbenzene ug/L 49.850 100 60-140
Styrene ug/L 49.350 99 60-140
tert-Butylbenzene ug/L 49.050 98 60-140
Tetrachloroethene ug/L 45.450 91 60-140
Toluene ug/L 48.450 97 60-140
trans-1,2-Dichloroethene ug/L 46.550 93 60-140
trans-1,3-Dichloropropene ug/L 56.850 114 60-140
Trichloroethene ug/L 50.050 100 60-140
Trichlorofluoromethane ug/L 48.150 96 60-140
Vinyl chloride ug/L 55.350 111 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 70-130
Dibromofluoromethane (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 35 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
556848MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286251003
556849
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 106 60-14096 1020ND21.2 19.2
1,1,1-Trichloroethane ug/L 20 108 60-140109 120ND21.6 21.8
1,1,2,2-Tetrachloroethane ug/L 20 120 60-140102 1720ND24.1 20.4
1,1,2-Trichloroethane ug/L 20 108 60-14097 1120ND21.6 19.4
1,1-Dichloroethane ug/L 20 114 60-140115 120ND22.8 22.9
1,1-Dichloroethene ug/L 20 121 60-140119 220ND24.3 23.8
1,1-Dichloropropene ug/L 20 115 60-140112 320ND23.0 22.5
1,2,3-Trichlorobenzene ug/L 20 104 60-14086 1920ND20.8 17.2
1,2,3-Trichloropropane ug/L 20 103 60-14092 1220ND20.7 18.4
1,2,4-Trichlorobenzene ug/L 20 100 60-14080 2220ND20.0 15.9
1,2,4-Trimethylbenzene ug/L 20 118 60-14097 2020ND23.5 19.3
1,2-Dibromo-3-chloropropane ug/L 20 118 60-14092 2420ND23.6 18.5
1,2-Dibromoethane (EDB)ug/L 20 117 60-140101 1520ND23.4 20.2
1,2-Dichlorobenzene ug/L 20 118 60-140101 1620ND23.6 20.2
1,2-Dichloroethane ug/L 20 102 60-140109 720ND20.4 21.9
1,2-Dichloropropane ug/L 20 115 60-140104 1020ND23.1 20.9
1,3,5-Trimethylbenzene ug/L 20 116 60-14098 1620ND23.1 19.7
1,3-Dichlorobenzene ug/L 20 119 60-140105 1320ND23.8 20.9
1,3-Dichloropropane ug/L 20 120 60-140104 1420ND24.0 20.8
1,4-Dichlorobenzene ug/L 20 105 60-14093 1220ND21.0 18.5
2,2-Dichloropropane ug/L 20 70 60-14070 120ND14.0 13.9
2-Chlorotoluene ug/L 20 127 60-140111 1320ND25.3 22.2
4-Chlorotoluene ug/L 20 133 60-140116 1420ND26.6 23.2
Benzene ug/L 20 112 60-14097 1520ND22.4 19.4
Bromobenzene ug/L 20 114 60-140101 1320ND22.9 20.1
Bromochloromethane ug/L 20 115 60-140113 220ND23.1 22.5
Bromodichloromethane ug/L 20 103 60-14096 720ND20.5 19.1
Bromoform ug/L 20 106 60-14092 1420ND21.2 18.5
Bromomethane ug/L 20 98 60-140101 320ND19.7 20.2
Carbon tetrachloride ug/L 20 104 60-14099 520ND20.8 19.8
Chlorobenzene ug/L 20 110 60-14097 1220ND22.0 19.5
Chloroethane ug/L 20 103 60-140107 420ND20.5 21.3
Chloroform ug/L 20 104 60-140104 120ND20.7 20.8
Chloromethane ug/L 20 113 60-140113 020ND22.6 22.5
cis-1,2-Dichloroethene ug/L 20 112 60-140111 120ND22.4 22.2
cis-1,3-Dichloropropene ug/L 20 84 60-14074 1220ND16.7 14.9
Dibromochloromethane ug/L 20 105 60-14092 1320ND21.0 18.4
Dibromomethane ug/L 20 110 60-14098 1220ND22.0 19.6
Dichlorodifluoromethane ug/L 20 109 60-140113 420ND21.8 22.7
Diisopropyl ether ug/L 20 124 60-140115 720ND24.8 23.0
Ethylbenzene ug/L 20 117 60-140104 1220ND23.5 20.9
Hexachloro-1,3-butadiene ug/L 20 97 60-14080 1820ND19.3 16.0
Isopropylbenzene (Cumene)ug/L 20 110 60-14095 1420ND21.9 19.0
m&p-Xylene ug/L 40 129 60-140114 1240ND51.5 45.6
Methyl-tert-butyl ether ug/L 20 116 60-140106 920ND23.5 21.4
Methylene Chloride ug/L 20 123 60-140126 320ND24.5 25.3
n-Butylbenzene ug/L 20 100 60-14084 1720ND20.0 16.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 36 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
556848MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286251003
556849
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 129 60-140111 1520ND25.8 22.3
Naphthalene ug/L R12010660-14077 3220ND21.3 15.4
o-Xylene ug/L 20 109 60-14095 1320ND21.8 19.1
sec-Butylbenzene ug/L 20 115 60-14098 1620ND23.1 19.6
Styrene ug/L 20 112 60-14097 1520ND22.4 19.3
tert-Butylbenzene ug/L 20 115 60-140100 1420ND22.9 19.9
Tetrachloroethene ug/L 20 104 60-14095 920ND20.9 19.0
Toluene ug/L 20 106 60-14098 820ND21.3 19.7
trans-1,2-Dichloroethene ug/L 20 113 60-140115 120ND22.7 22.9
trans-1,3-Dichloropropene ug/L 20 93 60-14084 1020ND18.7 16.9
Trichloroethene ug/L 20 112 60-140100 1220ND22.5 20.0
Trichlorofluoromethane ug/L 20 99 60-140102 320ND19.9 20.5
Vinyl chloride ug/L 20 131 60-140130 120ND26.2 26.0
1,2-Dichloroethane-d4 (S)%91 70-130107
4-Bromofluorobenzene (S)%98 70-13098
Dibromofluoromethane (S)%96 70-130106
Toluene-d8 (S)%97 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 37 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/13849
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9286253002, 9286253005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555735
Associated Lab Samples:9286253002, 9286253005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 01/27/11 15:39
1,1,1-Trichloroethane ug/L ND 0.50 01/27/11 15:39
1,1,2,2-Tetrachloroethane ug/L ND 0.50 01/27/11 15:39
1,1,2-Trichloroethane ug/L ND 0.50 01/27/11 15:39
1,1-Dichloroethane ug/L ND 0.50 01/27/11 15:39
1,1-Dichloroethene ug/L ND 0.50 01/27/11 15:39
1,1-Dichloropropene ug/L ND 0.50 01/27/11 15:39
1,2,3-Trichlorobenzene ug/L ND 2.0 01/27/11 15:39
1,2,3-Trichloropropane ug/L ND 0.50 01/27/11 15:39
1,2,4-Trichlorobenzene ug/L ND 2.0 01/27/11 15:39
1,2,4-Trimethylbenzene ug/L ND 0.50 01/27/11 15:39
1,2-Dibromo-3-chloropropane ug/L ND 1.0 01/27/11 15:39
1,2-Dibromoethane (EDB)ug/L ND 0.50 01/27/11 15:39
1,2-Dichlorobenzene ug/L ND 0.50 01/27/11 15:39
1,2-Dichloroethane ug/L ND 0.50 01/27/11 15:39
1,2-Dichloropropane ug/L ND 0.50 01/27/11 15:39
1,3,5-Trimethylbenzene ug/L ND 0.50 01/27/11 15:39
1,3-Dichlorobenzene ug/L ND 0.50 01/27/11 15:39
1,3-Dichloropropane ug/L ND 0.50 01/27/11 15:39
1,4-Dichlorobenzene ug/L ND 0.50 01/27/11 15:39
2,2-Dichloropropane ug/L ND 0.50 01/27/11 15:39
2-Chlorotoluene ug/L ND 0.50 01/27/11 15:39
4-Chlorotoluene ug/L ND 0.50 01/27/11 15:39
Benzene ug/L ND 0.50 01/27/11 15:39
Bromobenzene ug/L ND 0.50 01/27/11 15:39
Bromochloromethane ug/L ND 0.50 01/27/11 15:39
Bromodichloromethane ug/L ND 0.50 01/27/11 15:39
Bromoform ug/L ND 0.50 01/27/11 15:39
Bromomethane ug/L ND 5.0 01/27/11 15:39
Carbon tetrachloride ug/L ND 0.50 01/27/11 15:39
Chlorobenzene ug/L ND 0.50 01/27/11 15:39
Chloroethane ug/L ND 1.0 01/27/11 15:39
Chloroform ug/L ND 0.50 01/27/11 15:39
Chloromethane ug/L ND 1.0 01/27/11 15:39
cis-1,2-Dichloroethene ug/L ND 0.50 01/27/11 15:39
cis-1,3-Dichloropropene ug/L ND 0.50 01/27/11 15:39
Dibromochloromethane ug/L ND 0.50 01/27/11 15:39
Dibromomethane ug/L ND 0.50 01/27/11 15:39
Dichlorodifluoromethane ug/L ND 0.50 01/27/11 15:39
Diisopropyl ether ug/L ND 0.50 01/27/11 15:39
Ethylbenzene ug/L ND 0.50 01/27/11 15:39
Hexachloro-1,3-butadiene ug/L ND 2.0 01/27/11 15:39
Isopropylbenzene (Cumene)ug/L ND 0.50 01/27/11 15:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 38 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:555735
Associated Lab Samples:9286253002, 9286253005
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 01/27/11 15:39
Methyl-tert-butyl ether ug/L ND 0.50 01/27/11 15:39
Methylene Chloride ug/L ND 2.0 01/27/11 15:39
n-Butylbenzene ug/L ND 0.50 01/27/11 15:39
n-Propylbenzene ug/L ND 0.50 01/27/11 15:39
Naphthalene ug/L ND 2.0 01/27/11 15:39
o-Xylene ug/L ND 0.50 01/27/11 15:39
sec-Butylbenzene ug/L ND 0.50 01/27/11 15:39
Styrene ug/L ND 0.50 01/27/11 15:39
tert-Butylbenzene ug/L ND 0.50 01/27/11 15:39
Tetrachloroethene ug/L ND 0.50 01/27/11 15:39
Toluene ug/L ND 0.50 01/27/11 15:39
trans-1,2-Dichloroethene ug/L ND 0.50 01/27/11 15:39
trans-1,3-Dichloropropene ug/L ND 0.50 01/27/11 15:39
Trichloroethene ug/L ND 0.50 01/27/11 15:39
Trichlorofluoromethane ug/L ND 1.0 01/27/11 15:39
Vinyl chloride ug/L ND 1.0 01/27/11 15:39
1,2-Dichloroethane-d4 (S)%125 70-130 01/27/11 15:39
4-Bromofluorobenzene (S)%99 70-130 01/27/11 15:39
Dibromofluoromethane (S)%117 70-130 01/27/11 15:39
Toluene-d8 (S)%101 70-130 01/27/11 15:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555736LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.850 96 60-140
1,1,1-Trichloroethane ug/L 48.450 97 60-140
1,1,2,2-Tetrachloroethane ug/L 53.550 107 60-140
1,1,2-Trichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethane ug/L 49.950 100 60-140
1,1-Dichloroethene ug/L 53.250 106 60-140
1,1-Dichloropropene ug/L 49.350 99 60-140
1,2,3-Trichlorobenzene ug/L 49.850 100 60-140
1,2,3-Trichloropropane ug/L 46.950 94 60-140
1,2,4-Trichlorobenzene ug/L 46.250 92 60-140
1,2,4-Trimethylbenzene ug/L 64.550 129 60-140
1,2-Dibromo-3-chloropropane ug/L 49.350 99 60-140
1,2-Dibromoethane (EDB)ug/L 50.250 100 60-140
1,2-Dichlorobenzene ug/L 54.050 108 60-140
1,2-Dichloroethane ug/L 47.150 94 60-140
1,2-Dichloropropane ug/L 50.850 102 60-140
1,3,5-Trimethylbenzene ug/L 53.250 106 60-140
1,3-Dichlorobenzene ug/L 54.350 109 60-140
1,3-Dichloropropane ug/L 52.850 106 60-140
1,4-Dichlorobenzene ug/L 48.150 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 39 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
555736LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.050 98 60-140
2-Chlorotoluene ug/L 57.850 116 60-140
4-Chlorotoluene ug/L 60.750 121 60-140
Benzene ug/L 48.150 96 60-140
Bromobenzene ug/L 51.050 102 60-140
Bromochloromethane ug/L 50.350 101 60-140
Bromodichloromethane ug/L 49.050 98 60-140
Bromoform ug/L 49.250 98 60-140
Bromomethane ug/L 48.650 97 60-140
Carbon tetrachloride ug/L 49.450 99 60-140
Chlorobenzene ug/L 47.250 94 60-140
Chloroethane ug/L 46.250 92 60-140
Chloroform ug/L 46.850 94 60-140
Chloromethane ug/L 45.050 90 60-140
cis-1,2-Dichloroethene ug/L 48.650 97 60-140
cis-1,3-Dichloropropene ug/L 48.750 97 60-140
Dibromochloromethane ug/L 47.650 95 60-140
Dibromomethane ug/L 49.050 98 60-140
Dichlorodifluoromethane ug/L 48.250 96 60-140
Diisopropyl ether ug/L 52.250 104 60-140
Ethylbenzene ug/L 52.550 105 60-140
Hexachloro-1,3-butadiene ug/L 51.450 103 60-140
Isopropylbenzene (Cumene)ug/L 51.650 103 60-140
m&p-Xylene ug/L 117100 117 60-140
Methyl-tert-butyl ether ug/L 49.150 98 60-140
Methylene Chloride ug/L 55.950 112 60-140
n-Butylbenzene ug/L 52.050 104 60-140
n-Propylbenzene ug/L 57.950 116 60-140
Naphthalene ug/L 47.550 95 60-140
o-Xylene ug/L 51.550 103 60-140
sec-Butylbenzene ug/L 53.950 108 60-140
Styrene ug/L 51.650 103 60-140
tert-Butylbenzene ug/L 52.850 106 60-140
Tetrachloroethene ug/L 48.350 97 60-140
Toluene ug/L 48.050 96 60-140
trans-1,2-Dichloroethene ug/L 49.650 99 60-140
trans-1,3-Dichloropropene ug/L 47.650 95 60-140
Trichloroethene ug/L 50.150 100 60-140
Trichlorofluoromethane ug/L 45.850 92 60-140
Vinyl chloride ug/L 59.350 119 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%98 70-130
Dibromofluoromethane (S)%98 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 40 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
557939MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286418002
557940
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 60-140101 020ND20.2 20.3
1,1,1-Trichloroethane ug/L 20 112 60-140112 020ND22.4 22.3
1,1,2,2-Tetrachloroethane ug/L 20 113 60-140112 120ND22.5 22.3
1,1,2-Trichloroethane ug/L 20 100 60-140105 520ND20.0 21.1
1,1-Dichloroethane ug/L 20 113 60-140112 120ND22.6 22.5
1,1-Dichloroethene ug/L 20 119 60-140116 220ND23.8 23.2
1,1-Dichloropropene ug/L 20 105 60-140106 020ND21.1 21.1
1,2,3-Trichlorobenzene ug/L 20 84 60-14087 320ND16.9 17.4
1,2,3-Trichloropropane ug/L 20 102 60-140100 120ND20.3 20.0
1,2,4-Trichlorobenzene ug/L 20 74 60-14076 220ND14.9 15.1
1,2,4-Trimethylbenzene ug/L 20 101 60-140103 120ND20.3 20.5
1,2-Dibromo-3-chloropropane ug/L 20 92 60-14096 420ND18.4 19.2
1,2-Dibromoethane (EDB)ug/L 20 99 60-140101 120ND19.9 20.2
1,2-Dichlorobenzene ug/L 20 106 60-140108 220ND21.1 21.6
1,2-Dichloroethane ug/L 20 108 60-140109 120ND21.5 21.8
1,2-Dichloropropane ug/L 20 110 60-140103 720ND22.0 20.6
1,3,5-Trimethylbenzene ug/L 20 103 60-140103 020ND20.7 20.7
1,3-Dichlorobenzene ug/L 20 109 60-140111 220ND21.8 22.2
1,3-Dichloropropane ug/L 20 106 60-140105 120ND21.2 21.1
1,4-Dichlorobenzene ug/L 20 100 60-14099 020ND19.9 19.9
2,2-Dichloropropane ug/L 20 82 60-14083 120ND16.4 16.6
2-Chlorotoluene ug/L 20 113 60-140114 020ND22.7 22.7
4-Chlorotoluene ug/L 20 122 60-140123 120ND24.5 24.7
Benzene ug/L 20 103 60-140104 120ND20.6 20.9
Bromobenzene ug/L 20 103 60-140106 320ND20.6 21.3
Bromochloromethane ug/L 20 109 60-140111 220ND21.7 22.2
Bromodichloromethane ug/L 20 101 60-140103 220ND20.2 20.7
Bromoform ug/L 20 97 60-14097 020ND19.5 19.4
Bromomethane ug/L 20 94 60-14097 220ND18.9 19.3
Carbon tetrachloride ug/L 20 107 60-140109 120ND21.5 21.8
Chlorobenzene ug/L 20 101 60-140101 020ND20.3 20.2
Chloroethane ug/L 20 108 60-140108 020ND21.6 21.7
Chloroform ug/L 20 104 60-140105 120ND20.9 21.1
Chloromethane ug/L 20 105 60-140107 320ND20.9 21.5
cis-1,2-Dichloroethene ug/L 20 107 60-140106 120ND21.3 21.2
cis-1,3-Dichloropropene ug/L 20 70 60-14073 420ND14.1 14.6
Dibromochloromethane ug/L 20 96 60-14096 020ND19.1 19.2
Dibromomethane ug/L 20 111 60-140100 1120ND22.3 20.0
Dichlorodifluoromethane ug/L 20 106 60-140108 220ND21.1 21.6
Diisopropyl ether ug/L 20 104 60-140106 220ND20.8 21.1
Ethylbenzene ug/L 20 107 60-140107 020ND21.4 21.4
Hexachloro-1,3-butadiene ug/L 20 83 60-14086 320ND16.6 17.1
Isopropylbenzene (Cumene)ug/L 20 96 60-14098 220ND19.3 19.6
m&p-Xylene ug/L 40 120 60-140120 040ND47.8 47.9
Methyl-tert-butyl ether ug/L 20 96 60-14099 220ND19.3 19.8
Methylene Chloride ug/L 20 127 60-140125 120ND25.3 25.1
n-Butylbenzene ug/L 20 90 60-14092 220ND18.0 18.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 41 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
557939MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286418002
557940
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 117 60-140116 020ND23.3 23.3
Naphthalene ug/L 20 68 60-14070 320ND13.6 14.0
o-Xylene ug/L 20 94 60-14095 120ND18.7 18.9
sec-Butylbenzene ug/L 20 102 60-140103 120ND20.4 20.6
Styrene ug/L 20 97 60-14099 320ND19.4 19.9
tert-Butylbenzene ug/L 20 100 60-140101 120ND20.1 20.2
Tetrachloroethene ug/L 20 93 60-14095 220ND18.6 19.0
Toluene ug/L 20 99 60-140104 520ND19.8 20.7
trans-1,2-Dichloroethene ug/L 20 108 60-140109 120ND21.7 21.8
trans-1,3-Dichloropropene ug/L 20 86 60-14091 620ND17.2 18.3
Trichloroethene ug/L 20 106 60-140105 020ND21.1 21.1
Trichlorofluoromethane ug/L 20 107 60-140107 020ND21.5 21.5
Vinyl chloride ug/L 20 117 60-140119 220ND23.3 23.8
1,2-Dichloroethane-d4 (S)%103 70-130104
4-Bromofluorobenzene (S)%99 70-130100
Dibromofluoromethane (S)%102 70-130103
Toluene-d8 (S)%97 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 42 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The lab does not hold NELAC accreditation for this parameter.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 43 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9286253
Cofield Service Center #16616
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9286253001 OEXT/12498 GCSV/9131MW1MADEP EPH MADEP EPH
9286253002 OEXT/12498 GCSV/9131MW2MADEP EPH MADEP EPH
9286253003 OEXT/12498 GCSV/9131MW3MADEP EPH MADEP EPH
9286253004 OEXT/12498 GCSV/9131MW4MADEP EPH MADEP EPH
9286253005 OEXT/12498 GCSV/9131WSW1MADEP EPH MADEP EPH
9286253001 GCV/4668MW1MADEP VPH
9286253002 GCV/4668MW2MADEP VPH
9286253003 GCV/4668MW3MADEP VPH
9286253004 GCV/4668MW4MADEP VPH
9286253005 GCV/4668WSW1MADEP VPH
9286253001 MPRP/7762 ICP/7166MW1SM 3030C EPA 200.7
9286253002 MPRP/7762 ICP/7166MW2SM 3030C EPA 200.7
9286253003 MPRP/7762 ICP/7166MW3SM 3030C EPA 200.7
9286253004 MPRP/7762 ICP/7166MW4SM 3030C EPA 200.7
9286253005 MPRP/7762 ICP/7166WSW1SM 3030C EPA 200.7
9286253001 OEXT/12489 MSSV/4547MW1EPA 625 EPA 625
9286253002 OEXT/12489 MSSV/4547MW2EPA 625 EPA 625
9286253003 OEXT/12489 MSSV/4547MW3EPA 625 EPA 625
9286253004 OEXT/12489 MSSV/4547MW4EPA 625 EPA 625
9286253005 OEXT/12489 MSSV/4547WSW1EPA 625 EPA 625
9286253001 MSV/13833MW1SM 6200B
9286253002 MSV/13849MW2SM 6200B
9286253003 MSV/13833MW3SM 6200B
9286253004 MSV/13833MW4SM 6200B
9286253005 MSV/13849WSW1SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 02/01/2011 04:04 PM Page 44 of 44
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]