26061- Brownfields Assessment Report - Piedmont Plating

Via Email
May 18, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Ms. Carolyn Minnich

Re: Brownfields Assessment Report
Piedmont Plating & Anodizing
Distribution Street & Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 26061-22-060
H&H Project No. H&A-002

Dear Carolyn:

Please find the enclosed Brownfields Assessment Report prepared for the Piedmont Plating & Anodizing
Brownfields property located in Charlotte, Mecklenburg County. The assessment activities were
completed pursuant to the North Carolina Department of Environmental Quality approved Brownfields
Assessment Work Plan dated April 13, 2023.

Should you have questions or need additional information, please do not hesitate to contact us.

Sincerely,
Hart & Hickman, PC
Loryn Smith Ralph McGee, PG
Project Environmental Scientist Senior Project Manager

Enclosures:

cc: Mr. Christopher Kirchner, Hoffman & Associates (Via Email)
Mr. David Roberts, Hoffman & Associates (Via Email)
Mr. Teddy Chapman, 6 Summit Capital, LLC (Via Email)
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Brownfields Assessment Report
Piedmont Plating & Anodizing
Distribution Street & Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 26061-22-060
H&H Job No. H&A-002

Table of Contents

1.0 Introduction and Background ...............................................................................................1 
1.1 Site Background Information ................................................................................................2 
1.2 Previous Assessment Activities .............................................................................................3 
2.0 Brownfields Assessment Activities ......................................................................................10 
3.0 Receptor Survey ....................................................................................................................12 
4.0 Soil Assessment Activities .....................................................................................................15 
4.1 Soil Sampling Activities ......................................................................................................15 
4.2 Soil Sampling Analytical Results ........................................................................................18 
5.0 Groundwater Assessment Activities ....................................................................................21 
5.1 Groundwater Sampling Activities .......................................................................................21 
5.2 Groundwater Sampling Analytical Results .........................................................................24 
6.0 Sub-Slab Soil Gas Assessment Activities ............................................................................26 
6.1 Sub-Slab Soil Gas Sampling Activities ...............................................................................26 
6.2 Sub-Slab Soil Gas Sampling Results ...................................................................................28 
6.3 Vapor Intrusion Evaluation .................................................................................................28 
7.0 Quality Assurance – Quality Control ..................................................................................31 
7.1 Trip Blank ............................................................................................................................31 
7.2 Field Duplicates ...................................................................................................................31 
7.3 Investigation Derived Waste ...............................................................................................32 
8.0 Summary and Conclusions ..................................................................................................33 

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List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Sub-Slab Soil Gas Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Sample Location Map
Figure 4 Receptor Survey Map
Figure 5 Shallow Groundwater Potentiometric Map

List of Appendices

Appendix A Receptor Survey Form
Appendix B Boring Logs & Well Abandonment Records
Appendix C Laboratory Analytical Reports
Appendix D Groundwater and Sub-Slab Soil Gas Sampling Forms
Appendix E DEQ Risk Calculators

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Piedmont Plating & Anodizing
Distribution Street & Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 26061-22-060
H&H Job No. H&A-002

1.0 Introduction and Background

Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report for the Piedmont
Plating and Anodizing Brownfields property (Brownfields Project No. 26061-22-060) located at
2401 Distribution Street and 2322, 2400, 2402, 2404, and 2406 Dunavant Street in Charlotte,
Mecklenburg County, North Carolina (Site). The Site consists of four contiguous parcels
(Mecklenburg County Parcel Identification Nos. [PIN] 12104204, 12104215, 12104216, and
12104244) that collectively total approximately 2.6 acres of land located in a rapidly densifying
area of the South End neighborhood approximately 2.5 miles southwest of uptown Charlotte. A
Site location map is provided as Figure 1, and the Site and surrounding area are shown in
Figure 2.

The Site was developed in the early 1960s with one approximate 25,800 square foot (sq ft)
warehouse building (2401 Distribution Street), one approximate 18,500 sq ft multi-tenant
warehouse building (2322 Dunavant Street), one approximately 3,600 sq ft warehouse building
(2400 Dunavant Street), and one approximately 11,400 sq ft multi-tenant warehouse building
(2402/2406 Dunavant Street). Remaining portions of the Site are improved with asphalt-paved
access drives, parking areas, and landscaping. The Site buildings are currently occupied as
follows:

 The 2401 Distribution Street Site building is currently vacant.

 The 2322 Dunavant Street Site building is occupied by The Dunavant Restaurant, Barton
Malow Construction (offices), and a vacant tenant space.

 The 2400 Dunavant Street Site building is currently vacant, and the adjoining 2402-2406
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Dunavant Street Site building consists of a vacant tenant space (2402 Dunavant Street)
and SL Laser (a laser equipment supplier; 2406 Dunavant Street).

Proposed redevelopment of the Brownfields property includes razing the existing Site buildings
for construction of multi-story high density residential apartment building over a podium-style
parking deck with limited retail and amenity spaces at ground level. No residential units are
currently planned for ground level components of the proposed apartment building.

1.1 Site Background Information

As early as the 1930s, the Site consisted of undeveloped vegetated land. The Site was cleared
and graded in the 1950s, but remained undeveloped vacant land until the current warehouse
buildings were constructed in the early 1960s. The Site buildings were historically occupied as
follows:

 The 2401 Distribution Street Site building was occupied by Colora Knits Inc. (hosiery
manufacturers) and Gold Seal Manufacturing Company Inc. in the early 1960s and
Mielco Industries (auto parts manufacturing) in the mid-1980s until the early 1990s. The
2401 Distribution Street Site building was then occupied by various distribution, retail,
and commercial office tenants from the 1990s until the late 2010s.

 The 2322 Dunavant Street Site building was occupied by Piedmont Plating & Anodizing
Company from the early 1960s until the early to mid-1970s, when Southern Aluminum
Finishing Company acquired the property and continued plating and anodizing operations
until 2014. The warehouse building was renovated for commercial uses and has been
operated as a restaurant since 2018.

 The 2400 and 2402/2406 Dunavant Street Site building was occupied by a dairy
equipment manufacturer in 1961 until the 1990s, and a lithographic printer from 1983
until 2016. The Site buildings have since been renovated for commercial uses and have
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been occupied by a retail home furnishings business and a laser equipment supplier since
2017/2018.

Historical operations at the Site have consisted of hosiery manufacturing, auto parts
manufacturing, metal plating and anodizing, equipment manufacturing, and lithographic printing.
In more recent years, the Site buildings have been occupied by various retail and commercial
tenants.

1.2 Previous Assessment Activities

H&H reviewed several reports prepared by others to obtain additional information associated
with previous environmental assessments completed for each Site parcel. A brief summary of
the previous environmental reports is provided below.

2401 Distribution Street
Partner Engineering North Carolina, PLLC (Partner) conducted a Phase I ESA for the 2401
Distribution Street Site parcel in April 2021. According to information provided in the report,
the Site was occupied by Parker Medical Associates for manufacturing athletic protective guards
and other resin/fiberglass-based products, Dance Style Studios for custom dancewear design, and
Friendship Trays for food preparation and distribution. Historically, the Site building was
occupied by Colora Knits Inc. for hosiery manufacturing and Gold Seal Manufacturing Company
Inc., Boise Cascade Office Supply Overflow, Mielco Industries Auto Parts Manufacturing (1984-
1991), and Parker Medical Products and a commercial kitchen (1991-2020s).

Results of groundwater assessments completed at the north-northeast adjacent Crayton Printing
Brownfields property identified tetrachloroethylene (PCE), trichloroethylene (TCE), and vinyl
chloride at concentrations above the North Carolina Department of Environmental Quality
(DEQ) 2L Groundwater Quality Standards (2L Standards) in samples collected in close
proximity and topographically upgradient of the 2401 Distribution Street Site parcel. Results of
the Phase I ESA identified the potential for impact from historical on-Site operations and from
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known impacts in groundwater identified on the north-northeast adjacent Crayton Printing
Brownfields property as environmental concerns in connection with the Site.

Following the completion of the Phase I ESA for 2401 Distribution Street, Partner completed a
Phase II Subsurface Investigation in May 2021 which included the collection of one groundwater
sample and three near slab exterior soil gas samples for laboratory analysis. Each sample was
collected adjacent to the northern and topographically upgradient side of the 2401 Distribution
Street Site building. The May 2021 Phase II sample locations are shown in Figure 3.

Groundwater sample laboratory analytical results indicated that TCE (up to 3.4 micrograms per
liter [µg/L]) was detected at concentrations slightly above the DEQ 2L Standard of 3.0 µg/L and
the DEQ Residential Vapor Intrusion Groundwater Screening Level (GWSL) of 1.0 µg/L. In
addition, low levels of PCE (up to 6.2 micrograms per cubic meter [µg/m3]), TCE (3.6 µg/m3),
and vinyl chloride (0.59 µg/m3) were detected in soil gas at concentrations above the laboratory
method detection limits, but below their respective DEQ Vapor Intrusion Sub-slab and Exterior
Soil Gas Screening Levels (SGSLs).

2322 Dunavant Street
In November 2021, Partner conducted a Phase I ESA for the 2322 Dunavant Street Site parcels
(Parcels 12104216 and 12104244). According to information provided in the report, the Site was
occupied by Barton Marlow for office space, The Dunavant (restaurant), and a vacant tenant
space. Historically, the Site was occupied by Piedmont Plating & Anodizing Company from
1961 until 1973, when the Southern Aluminum Finishing Company reportedly acquired the Site
for similar operations until 2014.

According to information provided in the Partner Phase I ESA report, operations at the Site
consisted of anodizing aluminum, which is generally described as an electrochemical oxidation
process that consists of immersing metal into multiple chemical baths (primarily sulfuric acid) to
convert the metal surface into a decorative, durable, and corrosive-resistance product. Limited
information was available pertaining to chemical use and hazardous waste generation, storage,
and handling procedures.
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Partner also reviewed a prior Phase I ESA prepared by ERM and dated October 2007. At the
time of the ERM report, the 2322 Dunavant Street Site building was occupied by the Southern
Aluminum Finishing facility. During the Site reconnaissance, the Site contact stated that plating
process wastewater generated during the anodizing processes is treated on-Site prior to
discharging to the municipal sanitary sewer system. During the pretreatment process, a caustic
solution was added to neutralize the wastewater pH levels, and a flocculating agent was added to
promote solids to settle within wastewater clarifying tanks. The wastewater would then cycle
through three 500-gallon process tanks prior to being discharged. Sludge collected from the
clarifier was pumped into a filter press and dried prior to disposal into an on-Site dumpster.

ERM also identified numerous aboveground storage tanks (ASTs) at the facility which contained
the wastewater pretreatment system, clarifier, backup tank for the wastewater pretreatment
system, hydrochloric acid, and electrolytic coloring solutions. Four to five dip tanks associated
with the anodizing process were also identified within the Site building. ERM did not identify
other ASTs, underground storage tanks (USTs), or other items of environmental concern at the
Site. Based on this information, ERM did not recommend additional assessment activities.
However, results of the Partner Phase I ESA identified on-Site historical aluminum plating and
anodizing operations as an environmental concern in connection with the 2322 Dunavant Street
Site parcels. Partner also identified the known chlorinated solvent impacts in groundwater
identified at the adjacent Crayton Brownfields Property (discussed above) as an environmental
concern.

Following the completion of the Phase I ESA for 2322 Dunavant Street, Partner completed a
Phase II Subsurface Investigation in November 2021 which included the collection of three soil
samples and two exterior soil gas samples for laboratory analysis. Partner attempted to install
temporary groundwater monitoring wells for the collection of groundwater samples, but drilling
refusal was encountered prior to reaching the water table and no groundwater samples were
collected. The November 2021 Phase II sample locations are shown in Figure 3.

Results of the soil sampling activities did not identify compounds at concentrations above the
laboratory method detection limits. Results of the exterior soil gas sampling activities indicated
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the presence of 1,3-butadiene (24.8 µg/m3) and benzene (22.8 µg/m3) at concentrations above
their respective DEQ Residential Vapor Intrusion SGSLs, but below the DEQ Non-Residential
Vapor Intrusion SGSLs.

2400 Dunavant Street
In April 2022, Partner conducted a Phase I ESA for the 2400 Dunavant Street Site parcel.
According to information provided in the report, the Site was occupied by Mrs. Howard Fine
Furnishings and Interiors (home goods storage), SL-Laser Systems (laser equipment calibration),
and a vacant tenant space. Historically, the Site was occupied by a dairy equipment
manufacturer in the 1960s, an outwear manufacturer (knitting) in the early 1970s, a lithographic
printer from at least 1983 until 2016, and other various office and warehouse occupants. Results
of the Phase I ESA identified the potential for impacts from an undocumented release associated
with historical Site operations as an environmental concern in connection with the Site.

Following the completion of the Phase I ESA for 2400 Dunavant Street, Partner completed a
Phase II Subsurface Investigation in May 2022 which included the collection of three soil
samples and two sub-slab soil gas samples for laboratory analysis. The two sub-slab soil gas
samples were collected within the former lithographic printer tenant space. Partner attempted to
install temporary groundwater monitoring wells for the collection of groundwater samples, but
drilling refusal was encountered prior to reaching the water table and no groundwater samples
were collected. The May 2022 Phase II sample locations are shown in Figure 3.

Soil sample results did not identify compounds at concentrations above the DEQ PSRGs or
background levels in the case of metals. Results of sub-slab soil gas sampling completed within
the tenant space for the former printing operations identified benzene (up to 21.8 µg/m3) and
1,1,2,2-trichloroethane (4.24 µg/m3) at concentrations above their respective DEQ Residential
Vapor Intrusion SGSLs but below the DEQ Non-Residential Vapor Intrusion SGSLs. In
addition, low levels of TCE (11.7 µg/m3) and PCE (4.24 µg/m3) were detected at concentrations
above the laboratory reporting limits but below the DEQ Vapor Intrusion SGSLs in one sub-slab
soil gas sample.
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2023 Phase I ESA
In March 2023, H&H completed a Phase I ESA for the Site. Results of the Phase I ESA
identified the following environmental concerns:

 The 2401 Distribution Street Site building was historically occupied by the Colora Knits
Inc. (hosiery manufacturers) and Gold Seal Manufacturing as early as the 1960s and
Mielco Industries (auto parts manufacturing) from the mid-1980s until the early 1990s.
Operations such as hosiery and auto parts manufacturing may have included use of dyes,
solvents, and/or petroleum products.

The 2322 Dunavant Street Site building was occupied by Piedmont Plating & Anodizing
Company from the early 1960s until the early to mid-1970s, when the Southern
Aluminum Finishing Company acquired the Site building and continued similar metal
plating and anodizing operations. Metal plating and anodizing operations may have
included the use of various chemicals and solvents.

The 2400 Dunavant Street Site building was occupied by a dairy equipment manufacturer
in the 1960s, an outwear manufacturer (knitting) in the early 1970s, a lithographic printer
from at least 1983 until 2016, and other various office and warehouse occupants.
Manufacturing operations such as dairy equipment and knitting as well as printing
operations commonly use dyes, solvents, and/or petroleum products.

Limited information is available pertaining to the use of potentially hazardous materials
or generation, storage, and management practices associated with hazardous waste for the
historical on-Site manufacturing, metal plating and anodizing, and printing operations.
The Site buildings have recently been renovated and there is no obvious evidence of
environmentally sensitive systems remaining at the Site (tanks, separators, drains, sumps,
storage areas, etc.). However, based on the types and duration of historical operations
conducted within the Site buildings, results of the Phase I ESA indicated that the
potential for impact from undocumented releases represents an environmental concern
that warrants further evaluation.
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As discussed above, Partner completed Limited Phase II Investigations for each Site
parcel in May 2021, November 2021, and May 2022. Phase II assessments completed at
the Site included the collection of soil, groundwater, and soil gas samples for laboratory
analysis to evaluate subsurface conditions for potential impacts associated with historical
on-Site and nearby off-Site uses. A low level of TCE (3.4 µg/L) was detected in a
groundwater sample collected in the northern and upgradient portion of the Site at a
concentration exceeding the 2L Standard (and DEQ Residential Vapor Intrusion GWSL).
Results of the Phase I ESA identified the presence of TCE in groundwater at
concentrations above the 2L Standard as an environmental concern in connection with the
Site.

 The Site is located in a historically industrial and commercial use area of Charlotte.
Operations on nearby properties have included dry cleaning facilities, photofinishing, a
printing facility, and other manufacturing and industrial uses. In addition, several release
incidents are listed in the environmental databases for multiple nearby off-Site properties.
Results of groundwater assessment activities previously completed for the adjacent
property to the north have identified PCE, TCE, and vinyl chloride at concentrations
above the 2L Standards in monitoring wells located approximately 60 to 330 ft north-
northeast and cross-gradient to upgradient to the subject Site. Results of the Phase I ESA
identified the potential for impact to the Site from documented and undocumented
releases associated with historical operations on nearby off-Site properties as an
environmental concern in connection with the Site.

To address environmental concerns associated with historical on-Site and off-Site operations, 6
Summit Capital, LLC elected to enter the Site into the DEQ Brownfields Redevelopment Section
on August 29, 2022, and received a letter of eligibility on February 7, 2023. Hoffman &
Associates is under contract to acquire the Site from 6 Summit Capital, LLC and intends to
submit an updated Brownfields Property Application to be identified as the Prospective
Developer and complete the Brownfields agreement process. A kick-off/data gap meeting with
the DEQ Brownfields Redevelopment Section, 6 Summit Capital, LLC, Hoffman & Associates,
and H&H was held on April 12, 2023, to discuss prior Site history, proposed redevelopment
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plans, and data gaps. To address data gaps and DEQ Brownfields requests for additional
assessment, H&H prepared a Brownfields Assessment Work Plan (Work Plan) for DEQ review
and approval. The Work Plan received DEQ-approval in an email dated April 13, 2023.

Brownfields assessment activities were completed in accordance with the DEQ-approved Work
Plan to further evaluate the potential for impacts and assist with the management of Site media
during proposed redevelopment. A summary of the Brownfields assessment activities is
provided in the following sections.
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2.0 Brownfields Assessment Activities

Brownfields assessment activities were completed in April 2023 and included the collection of
soil, groundwater, and sub-slab soil gas samples to evaluate for potential impacts associated with
historical on-Site and nearby off-Site operations and potential risks associated with planned
redevelopment. In addition, a receptor survey was completed to obtain information about land
use, water supply, basements, underground utilities, drains, and surface water bodies in the
vicinity of the Site.

As part of the assessment activities, soil borings were advanced adjacent to the former railroad
spurs and loading docks located in the central portion of the Site, near former ASTs associated
with historical metal plating operations in eastern portions of the Site, and within the 2322
Dunavant Street Site building in the former wastewater treatment system area associated with the
former plating operations. H&H also completed groundwater assessment activities to evaluate
current groundwater conditions in areas of the Site where assessment activities have not
previously been completed. To evaluate the potential for structural vapor intrusion into the
proposed buildings and to further establish baseline soil gas concentrations, H&H collected sub-
slab soil gas samples within each Site building.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. The private utility locator also
utilized ground penetrating radar (GPR) survey techniques to identify and mark utilities. In
addition, H&H directed the drilling contractor to hand clear each boring to a depth of
approximately 5 feet below the ground surface (ft bgs) to further screen the boring locations for
the presence of subsurface utilities prior to utilizing mechanical drilling equipment.

The Brownfields assessment activities were conducted in general accordance with the DEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of
Contaminated Sites (Guidelines) dated September 2022, the DEQ Division of Waste
Management (DWM) Vapor Intrusion Guidance (VI Guidance) dated September 2022, the most
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recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Laboratory
Services and Applies Science Division (LSASD) Field Branches Quality System and Technical
Procedures guidance, the DEQ Brownfields Program Environmental Site Assessment Work Plan
Minimum Requirements Checklist dated March 2023, and the DEQ-approved Work Plan.

A summary of receptor survey results is provided in Section 3.0, details of the soil, groundwater,
and vapor intrusion assessment activities are provided in Section 4.0 through Section 6.0. A
description of the quality assurance and quality control measures is provided in Section 7.0, and
a summary and conclusions based on results of the assessment activities are provided in
Section 8.0.
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3.0 Receptor Survey

In April 2023, H&H conducted a receptor survey at the Site and surrounding area. Receptor
survey activities included an intensive pedestrian and vehicular survey for possible potable water
supply wells, springs, and surface water intakes used as a source of water within a 1,500 ft radius
of the Site. H&H also reviewed the online Mecklenburg County Well Information System for
potential wells in the area and utilized the online DEQ Source Water Assessment Program
(SWAP) to identify potential potable water sources for properties located within a 1,500 ft radius
of the Site.

In addition, H&H identified the locations of main underground and aboveground utilities and
land use and zoning in the area of the Site using available Mecklenburg County online resources.
A receptor survey map is provided as Figure 4, and a copy of the completed DEQ Brownfields
Property Receptor Survey form is provided as Appendix A. Results of the receptor survey
activities are summarized below.

Zoning
The Brownfields property is zoned as transit-oriented development (TOD-UC and TOD-NC).
Adjacent properties to the northeast, southeast, southwest, and northwest are also zoned as
transit-oriented development (TOD-UC and TOD-NC).

Municipal Water Availability
Municipal water supplied by the City of Charlotte is available to the Site and surrounding area.
H&H did not identify sources of public drinking water within 1,500 ft of the Site based on the
review of information available on Mecklenburg County Well Information System Maps, DEQ
SWAP, and the Annual Water Quality Report published by the City of Charlotte. The City of
Charlotte obtains raw water from Lake Norman and Mountain Island Lake which are located
approximately fifteen miles northwest of the Site at the closest point to Mountain Island Lake.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the
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Site to identify potential water supply wells. H&H also utilized the DEQ SWAP geographic
information system map and Mecklenburg County Well Information System maps to identify
potential potable water supply wells located within a 1,500 ft radius of the Site. According to
information obtained from online resources, no active or inactive water supply wells are located
within the 1,500 ft radius of the Site. H&H was unable to visually confirm the presence of water
supply or irrigation wells located near the Brownfields property due to access restrictions.

According to Mecklenburg County well regulations, no water supply well permit will be
approved for any use if the well is proposed within 1,000 feet of known groundwater
contamination. Due to the presence of documented groundwater impacts on multiple properties
surrounding the Site, no water supply wells should be present in the area. This is consistent with
information obtained from the Mecklenburg County Well Information System maps which
indicated that no wells are located in the Site area.

Surface Water Bodies
An unnamed tributary of Irwin Creek is located approximately 230 ft northwest of the Site
(Figure 1). Based on the DEQ Surface Water Classification system, Irwin Creek is a Class C
surface water body. A Class C surface water body is defined as “waters protected for uses such
as secondary recreation, fishing, wildlife, fish consumption, aquatic life including propagation,
survival and maintenance of biological integrity, and agriculture. Secondary recreation includes
wading, boating, and other uses involving human body contact with water where such activities
take place in an infrequent, unorganized, or incidental manner”. Based on information obtained
from the DEQ Division of Water Resources (DWR) Surface Water Classifications geographic
information system map, the subject Site is not located within a protected water supply
watershed area.

Subsurface Utilities and Structures
H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities located
on the Site and conducted a visual reconnaissance in the Site area to identify potential subsurface
structures within 100 ft of the subject Site. H&H observed evidence of subsurface utilities
including sanitary sewer, storm sewer, municipal water, communications, electrical, and natural
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gas on the Site and nearby adjacent properties. Overhead electrical lines were observed along
the northern and southeastern property boundaries. Overhead electrical lines were also observed
between the 2322 and 2400 Dunavant Street buildings. H&H did not observe structures with
potential basements within a 1,500 ft radius of the Site during the visual reconnaissance.

Approximate locations of subsurface and overhead utilities located in the immediate vicinity of
the Site are shown in Figure 4.
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4.0 Soil Assessment Activities

In April 2023, under the direction of H&H, Innovative Environmental Technologies (IET)
advanced ten (10) soil borings at the Site to evaluate for potential impacts in areas of potential
concern and in areas that may be disturbed during planned redevelopment and grading activities.
It should be noted that H&H attempted to advance BF-SB-10 within the 2322 Dunavant Street
building. However, a soil sample could not be collected at this location due to an existing gravel
layer beneath the building slab which sluffed and backfilled the borehole at each attempt to
advance the soil boring. Soil boring locations are shown in Figure 3.

Soil borings were advanced utilizing a decontaminated stainless-steel hand auger or a
track-mounted direct push technology (DPT) drill rig. During boring advancement, continuous
soil samples were collected from the center of the hand auger bucket or from acetate lined
macrocore DPT sleeves. The soil samples were logged for lithologic description, observed for
obvious evidence of staining and unusual odors, and field screened for the presence of volatile
organic vapors using a calibrated photoionization detector (PID). Obvious evidence of staining,
odors, or elevated PID readings were not observed by field personnel during soil boring
advancement. Boring logs including lithologic descriptions and field screening results for each
soil boring are provided in Appendix B.

A discussion of the soil sampling activities and results is provided in the following sections.

4.1 Soil Sampling Activities

H&H collected ten (10) soil samples for laboratory analysis from ten (10) soil borings (BF-SB-1
through BF-SB-9 and BF-SB-11). As previously noted, no soil sample was collected at the BF-
SB-10 soil boring advanced within the 2322 Dunavant Street Site building due to the presence of
gravel beneath the building slab. Soil samples for laboratory analysis were collected as
described below and locations of the soil borings are shown in Figure 3.

 One soil sample (BF-SB-1) was collected adjacent to the southwestern side of 2401
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Distribution Street Site building to evaluate soil conditions near the western Site
boundary. The soil boring was advanced to approximately 5 ft bgs. Because field
screening results did not indicate obvious evidence of potential impacts, a soil sample
was collected from apparent native soil at the 4-6 ft depth interval. The soil sample was
submitted for analysis of volatile organic compounds (VOCs) by EPA Method 8260,
semi-volatile organic compounds (SVOCs) by EPA Method 8270, and Resource
Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA
Methods 6020/7471/7199.

 One soil sample (BF-SB-2) was advanced north of the 2401 Distribution Street Site
building to evaluate soil conditions along the northern Site boundary. The soil boring
was advanced to approximately 5 ft below ground surface (bgs) and because field
screening results did not indicate obvious evidence of potential impacts, a sample was
collected from a shallow depth interval (0-2 ft bgs). The soil sample was submitted for
analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA
metals plus hexavalent chromium by EPA Methods 6020/7471/7199.

 Four shallow soil borings (BF-SB-3 through BF-SB-6) were advanced to approximately 5
ft bgs between former loading docks and the former railroad spurs located in the central
portion of the Site. Because field screening results did not indicate obvious evidence of
potential impacts, each soil sample was collected from the 0-2 ft bgs depth interval to
evaluate soil conditions at the surface based on historical uses in the central portion of the
Site. The soil samples were submitted for analysis of VOCs by EPA Method 8260,
SVOCs by EPA Method 8270, and RCRA metals plus hexavalent chromium by EPA
Methods 6020/7471/7199.

 Two soil borings (BF-SB-7 and BF-SB-8) were advanced to approximately 8 ft bgs near
the eastern corner of the 2322 Dunavant Street Site building where former metal plating
related ASTs were historically staged. Results of field screening did not identify obvious
evidence of potential impacts in either soil boring. Therefore, the BF-SB-7 soil sample
was collected from 2-4 ft bgs and BF-SB-8 soil sample was collected from 0-2 ft bgs to
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evaluate the potential for impact at varying depths in this area of the Site. The soil
samples were submitted for analysis of VOCs by EPA Method 8260, SVOCs by EPA
Method 8270, RCRA metals plus hexavalent chromium, copper, aluminum, nickel, and
zinc by EPA Methods 6020/7471/7199, and cyanide by EPA Method 4500.

 One soil boring (BF-SB-9) was advanced to approximately 8 ft bgs within the 2322
Dunavant Street Site building in the area of the former wastewater treatment system. No
obvious evidence of impacts was observed during field screening. Therefore, a soil
sample was collected from a shallow depth interval just beneath the slab to evaluate the
potential for impact based on historical use in this area of the building. The soil sample
was submitted for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method
8270, RCRA metals plus hexavalent chromium, copper, aluminum, nickel, and zinc by
EPA Methods 6020/7471/7199, and cyanide by EPA Method 4500.

 One soil boring (BF-SB-11) was advanced to approximately 6 ft bgs near the southern
corner of the 2400-2406 Dunavant Street Site building to evaluate soil conditions near the
southeastern Site boundary. Because field screening results did not indicate obvious
evidence of potential impacts, a soil sample was collected from apparent native soil at the
4-6 ft depth interval. The soil sample was submitted for analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, and RCRA metals plus hexavalent
chromium by EPA Methods 6020/7471/7199.

Soil samples BF-SB-1 and BF-SB-11 were collected from apparent native soil along Distribution
Street and Dunavant Street in areas that appear to be undisturbed by historical uses. Therefore,
H&H considers metals concentrations detected in these two soil samples to be representative of
naturally occurring background levels in Site soil.

The soil samples selected for laboratory analysis were placed in dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Pace Analytical
(Pace), under standard chain of custody protocols for the laboratory analyses listed above.
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Following sampling activities, the soil borings were abandoned and the surfaces were repaired
similar to pre-drilling conditions, or the borings were converted into temporary monitoring wells
as discussed further in Section 5.0 below. In addition, soil sample locations were estimated
using a hand-held global positioning system (GPS) unit for exterior locations or were estimated
by measuring distances from known benchmarks (windows, walls, doorframes, etc.) for the
interior locations.

4.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is presented in Table 1 and a copy of the
laboratory analytical report and chain of custody record is provided in Appendix C. The
laboratory analytical results were compared to the most recent versions of the DEQ PSRGs dated
January 2023. In addition to the PSRGs, metals results were compared to published
concentrations for naturally occurring metals as well as Site-specific background levels
established using data from BF-SB-1 and BF-SB-11. A discussion of the laboratory analytical
results in comparison to the regulatory screening levels and background levels for metals is
included below.

VOCs
Laboratory analytical results indicate that no VOCs were detected at concentrations above the
DEQ Residential or Industrial/Commercial PSRGs in soil samples collected at the Site. Trace
levels of methylene chloride (up to 0.165 C9 mg/kg) were detected above the DEQ Protection of
Groundwater PSRGs of 0.025 mg/kg in several soil samples. Note that C9 designation indicates
that methylene chloride has been identified by the laboratory as a common laboratory introduced
contaminant and its presence in the soil samples is not representative of conditions at the Site. A
trace level of TCE (0.029 mg/kg) was also detected at a concentration slightly above the DEQ
Protection of Groundwater PSRG of 0.021 mg/kg in the BF-SB-6 soil sample collected in the
central portion of the Site.

Laboratory analytical results also indicated trace levels of 1,2,4-trimethylbenzene (up to 0.0178
mg/kg), 4-methyl-2-pentanone (0.0484 J mg/kg), naphthalene (up to 0.0198 mg/kg), cis-1,2-
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dichloroethene (0.0134 J mg/kg), and n-propylbenzene (0.0039 J mg/kg) at concentrations above
the laboratory method detection limits, but below DEQ PSRGs in select soil samples. Note that
the J-Flag designation indicates that the compound was detected at a concentration above the
laboratory method detection limit, but below the laboratory reporting limit resulting in a
laboratory estimated concentration. No other VOCs were detected at concentrations above
laboratory method detection limits in the soil samples collected at the Site.

SVOCs
Laboratory analytical results indicate that several polycyclic aromatic hydrocarbons (PAHs)
were detected at concentrations above the laboratory method detection limits in the BF-SB-6 soil
collected in the central portion of the Site. The compounds benzo(a)anthracene (53 mg/kg),
benzo(a)pyrene (48.5 mg/kg), benzo(b)fluoranthene (64 mg/kg), benzo(k)fluoranthene (22.8
mg/kg), indeno(1,2,3-cd)pyrene (29.8 mg/kg), and naphthalene (12.6 mg/kg) were detected at
concentrations above the DEQ Residential and/or Industrial/Commercial PSRGs.
Benzo(a)pyrene was also detected in BF-SB-8/BF-SB-DUP (up to 0.323 J mg/kg; former metal
plating area) at a concentration exceeding the DEQ Residential PSRG but below the DEQ
Industrial/Commercial PSRG. No other SVOCs were detected at concentrations above
laboratory method detection limits in the soil samples collected at the Site.

Metals
As expected, several metals were detected at concentrations above laboratory method detection
limits in the soil samples collected at the Site. Concentrations of arsenic (up to 2.9 mg/kg) were
detected above the DEQ Residential PSRG of 0.68 mg/kg in several soil samples collected from
the Site. The concentrations of arsenic detected is Site soil samples are consistent with Site-
specific background levels and well within the published range for naturally occurring levels.

Hexavalent chromium was detected at concentrations ranging from 0.856 mg/kg – 2.09 mg/kg in
background soil samples BF-SB-1 and BF-SB-11. The hexavalent chromium concentration
detected in soil sample BF-SB-6 (26.4 mg/kg) exceeds the DEQ Industrial/Commercial PSRG
and upper limit of the Site-specific range. Hexavalent chromium was also detected in BF-SB 4,
BF-SB-5, and BF-SB-8 (up to 4.89 mg/kg) at a concentration exceeding the DEQ Residential
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and/or DEQ Protection of Groundwater PSRGs and the upper limit of the Site-specific range.
Concentrations of hexavalent chromium detected in the remaining soil samples are within the
background range. No other metals were detected at concentrations above the DEQ PSRGs or
background concentrations.

Although below the DEQ PSRGs, trivalent chromium was detected in BF-SB-1 (154 mg/kg) and
in BF-SB-5 (119 mg/kg) at concentrations above the “Rule of 20” for toxicity characteristics of
100 mg/kg. Therefore, H&H requested the laboratory analyze BF-SB-1 and BF-SB-5 for
chromium using Toxicity Characteristic Leaching Potential (TCLP) methods to determine if the
leachate concentration was greater than the EPA maximum concentration for toxicity
characteristic criteria 5.0 milligrams per liter (mg/L). Results of TCLP analysis indicate that
chromium was not detected concentrations above the laboratory method detection limit in the
leachate samples and confirms chromium concentrations in the soil samples are not present at
characteristically hazardous levels.

Cyanide
Laboratory analytical results identified trace levels of cyanide (up to 0.42 mg/kg) at
concentrations well below the DEQ Residential PSRG of 5 mg/kg in soil samples collected in
historical plating operational areas of the Site. Note that trace levels of cyanide (up to 0.24 J
mg/kg) were also detected in both background soil samples (BF-SB-1 and BF-SB-11).

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5.0 Groundwater Assessment Activities

In April 2023, H&H provided oversight during the installation of eight (8) temporary
groundwater monitoring wells (BF-TMW-1 through BF-TMW-8) at the Site. Groundwater
samples were collected for laboratory analysis from each temporary monitoring well to evaluate
the current groundwater conditions in areas of the Site where previous assessment activities have
not been completed and to delineate the extent of chlorinated solvent impacts identified near the
northern Site boundary during previous sampling activities completed by Partner. Locations of
the temporary monitoring wells are depicted in Figure 3 and are described further below.

 Two temporary monitoring wells (BF-TMW-1 and BF-TMW-2) were installed in the
western and downgradient portion of the Site;
 Three temporary monitoring wells (BF-TMW-3, BF-TMW-4, and BF-TMW-6) were
installed in upgradient portions of the Site, along the northern Site boundary and
downgradient of historical off-Site operations;
 One temporary monitoring well (BF-TMW-5) was installed in the central portion of the
Site;
 One upgradient temporary monitoring well (BF-TWM-7) was installed in the eastern
portion of the Site, near the former metal plating wastewater AST staging area; and
 One upgradient temporary monitoring well (BF-TMW-8) was installed in the southern
portion of the Site.

5.1 Groundwater Sampling Activities

The temporary monitoring wells were installed utilizing DPT and hollow stem auger drilling
techniques to advance borings until sufficient groundwater was encountered. Due to shallow
refusal at the BF-TMW-4 location along the northern Site boundary, the temporary well boring
was advanced using air rotary drilling methods. Continuous soil samples were collected from
the temporary monitoring well boring cuttings and logged for lithologic description, observed for
obvious evidence of staining and unusual odors, and field screened for the presence of volatile
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organic vapors using a calibrated PID. Field screening results did not indicate obvious evidence
of potential impacts in samples collected from the temporary well borings.

Temporary monitoring wells were constructed of 1-inch diameter PVC with 5 to 15 ft of pre-
packed well screen set to bracket the water table and 1-inch diameter PVC well casing to the
ground surface. Temporary monitoring wells were installed to depths ranging from
approximately 7 to 22 ft bgs. A filter sand pack was installed from the bottom of each temporary
well boring to approximately 2 ft above each well screen and a hydrated bentonite seal was then
installed above the filter sand pack. Temporary monitoring well boring logs with well
construction details are provided in Appendix B.

Following installation of the temporary monitoring wells, the wells were allowed to equilibrate
to static conditions and a decontaminated electronic water level indicator was used to measure
the depth to the water table relative to the ground surface and the tops of the well casings. H&H
surveyed the temporary well elevations with a Spectra SP96 surveying instrument, which has an
elevation accuracy level of approximately 2 centimeters. The depth to groundwater
measurements and the temporary well elevations were then used to calculate the water table
elevations at each temporary well location and the water table elevations were used to estimate
the groundwater flow direction at the Site.

Groundwater in northern portions of the Site generally flows from northeast to west.
Groundwater in the eastern portion of the Site generally flows toward the west across the Site. A
tabular summary of well construction details and groundwater elevation data is provided as
Table 2, and the water table potentiometric surface and estimated groundwater flow direction are
shown in Figure 5.

Once depth to water and surveying measurements were collected, the temporary wells were
developed by removing a minimum of 3 to 5 volumes and until field parameters have stabilized
(pH± 0.1 Standard Units [SU] and conductivity varies no more than 5%). Following
development, temporary monitoring wells were allowed to equilibrate to static conditions.
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After development, groundwater samples were collected utilizing low flow/low stress purging
techniques using a peristaltic and dedicated polyethylene tubing. During sampling, the intake
point of the sample tubing was placed in the approximate mid-portion of the screened interval of
the well, and groundwater was removed at a rate no greater than 200 milliliters per minute
(mL/min). H&H utilized calibrated water quality meters to collect measurements of pH,
temperature, dissolved oxygen, oxidation reduction potential, turbidity, and specific conductivity
at three- to five-minute intervals during the purging process. Purging was considered complete
when the field parameters stabilized (pH ± 0.1 SU, conductivity varied no more than 5%, and
turbidity was less than 10 Nephelometric Turbidity Units [NTUs]). Note that select wells were
pumped dry during the purging process and were allowed to recover to static conditions prior to
collecting groundwater samples for laboratory analysis. Groundwater sampling forms completed
by sampling personnel are provided in Appendix D.

Once groundwater parameters stabilized, groundwater samples submitted for analysis of SVOCs
and RCRA metals were collected directly into laboratory supplied glassware directly from the
sample tubing discharge. The groundwater samples for VOC analysis were collected directly
into laboratory supplied sample containers using the “soda straw” method to eliminate the
potential for volatile compound loss through the pump head. The sample containers were
labeled with the sample identification, date, time, and requested analysis, and placed in a
laboratory supplied cooler with ice.

Groundwater samples BF-TMW-1 through BF-TMW-6 were delivered to Pace under standard
chain of custody protocols for analyses of VOCs by EPA Method 8260, SVOCs by EPA Method
8270, and RCRA metals by EPA Method 6020/7470. Groundwater samples BF-TMW-7 and
BF-TMW-8 were delivered to Pace under standard chain of custody protocols for analyses of
VOCs by EPA Method 8260, SVOCs by EPA Method 8270, RCRA metals plus copper,
aluminum, nickel, and zinc by EPA Method 6020/7470, and cyanide by EPA Method 4500.

Note that turbidity was measured at 73.80 NTUs in BF-TMW-8 at the time of sample collection.
H&H collected a field-filtered and unfiltered sample from BF-TMW-8 for metals analysis and
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requested the laboratory place the filtered sample on hold. Based on the results of the unfiltered
BF-TMW-8 groundwater sample, the filtered groundwater sample was not analyzed.

The groundwater sample locations were estimated using a hand-held GPS unit. Following
sampling activities, the temporary monitoring wells were abandoned by a licensed well driller
and the surfaces were repaired similar to pre-drilling conditions. Driller provided temporary
monitoring well abandonment records are provided in Appendix B.

5.2 Groundwater Sampling Analytical Results

A tabular summary of the groundwater sample laboratory analytical results is presented in
Table 3 and a copy of the laboratory analytical report and chain of custody record is provided in
Appendix C. Groundwater analytical data were compared to the 2L Standards dated April 2022
and the DEQ Residential and Non-Residential Vapor Intrusion Groundwater Screening Levels
(GWSLs) dated January 2023.

Organic Compounds
Laboratory analytical results indicate that TCE (up to 19.2 µg/L) was detected in upgradient
groundwater samples BF-TMW-4, BF-TMW-6, and BF-TMW-7 (and its duplicate groundwater
sample BF-GW-DUP1) at concentrations above the DEQ 2L Standard of 3.0 µg/L and/or the
DEQ Residential and Non-Residential Vapor Intrusion GWSLs of 1.0 µg/L and 4.4 µg/L,
respectively. Groundwater sampling results also identified a concentration of TCE (12.2 µg/L)
above the 2L Standard and Vapor Intrusion GWSLs in the BF-TWM-5 groundwater sample
collected in the central portion of the Site. TCE was not detected at concentrations above the
laboratory method detection limits in groundwater samples collected in the southwestern portion
of the Site (BF-TMW-1), the northwestern portion of the Site (BF-TMW-2), or the southeastern
portion of the Site (BF-TMW-8).

Low levels of PCE (up to 6.4 µg/L) were detected above the 2L Standard of 0.7 µg/L but below
the DEQ Vapor Intrusion GWSLs in the upgradient BF-TMW-4 groundwater sample and in the
and BF-TMW-5 groundwater sample collected in the central portion of the Site. PCE was not
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detected at concentrations above the 2L Standard or Vapor Intrusion GWSLs in the remaining
groundwater samples collected at the Site.

Low levels of chloroform (up to 1.8 µg/L) were detected at concentrations above the DEQ
Residential Vapor Intrusion GWSL of 1.0 µg/L, but below the DEQ Non-Residential Vapor
Intrusion GWSL of 3.6 µg/L and well below the DEQ 2L Standard of 70 µg/L. Note that
chloroform is a byproduct of the drinking water treatment process and its presence in Site
groundwater may be attributable to leaking municipal water lines and not an environmental
release.

Trace levels of 1,1-dichloroethene (up to 0.86 J µg/L) and cis-1,2-dichloroethene (up to 0.88 J
µg/L) were detected in select groundwater samples at concentrations above the laboratory
method detection limits, but below the 2L Standards and the DEQ Vapor Intrusion GWSLs. No
other organic compounds were detected at concentrations above the laboratory method detection
limits in the groundwater samples collected at the Site.

Inorganic Compounds
Low levels of arsenic (up to 0.50 J µg/L), barium (up to 49.6 µg/L), cadmium (up to 0.083 J
µg/L), total chromium (up to 5.7 µg/L), copper (up to 1.7 J µg/L), lead (up to 4.6 µg/L), nickel
(up to 4.2 µg/L), selenium (up to 0.47 J µg/L), and zinc (up to 2.8 J µg/L) were detected at
concentrations above the laboratory method detection limits, but below the 2L Standards in
groundwater samples collected at the Site. No other metals were detected at concentrations
above the laboratory method detection limits in groundwater.

Laboratory analytical results indicate that cyanide was not detected at concentrations above the
laboratory method detection limits in groundwater samples collected in the area of historical
plating operations (BF-TMW-7) or in background sample BF-TMW-8 collected in the
southeastern portion of the Site. This is consistent with soil sample data which did not identify
the presence of cyanide at concentrations above the DEQ Protection of Groundwater PSRG in
these areas.

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6.0 Sub-Slab Soil Gas Assessment Activities

To evaluate the potential for structural vapor intrusion into the proposed buildings and to
establish baseline soil gas concentrations beneath the existing Site buildings, H&H installed and
sampled temporary sub-slab soil gas sampling points within each existing Site building between
April 17 and April 20, 2023. The sub-slab soil gas sampling point locations are shown in
Figure 3, and the soil gas sampling activities and results are described below.

6.1 Sub-Slab Soil Gas Sampling Activities

H&H installed eleven (11) sub-slab soil gas sample points (BF-SSV-1 through BF-SSV-11)
within the existing Site buildings using a rotary hammer drill and 1½-inch diameter drill bit to
advance a pilot hole into the concrete slab to a depth of approximately 1¾ inches below the
surface. A drill guide was then placed in the pilot hole and a 5/8-inch diameter drill bit was
utilized to advance the boring through the concrete slab and approximately 6-inches into the
underlying soil. Following concrete borehole advancement, loose concrete cuttings were
removed from each boring using a bottlebrush. A Cox-Colvin Vapor Pin™ (vapor pin) assembly
(brass sampling point and silicone sleeve) was then seated in the borehole using an
installation/extraction tool and hammer. Upon installation of the vapor pin assembly, dedicated
Teflon® sample tubing was connected to the barbed end of the sample point. Each sub-slab soil
gas point was allowed to equilibrate for a minimum of 2-hours after installation and prior to
sample collection.

Each sub-slab soil gas sample was collected utilizing a laboratory supplied 1-liter Summa®
canister connected to an air-flow regulator calibrated by the laboratory to collect the soil gas
samples at a rate of approximately 100 mL/min. Prior to the collection of the soil gas samples,
“shut-in” tests were conducted on the sampling train and helium leak checks were conducted at
each sampling point. A description of the shut-in test and helium leak testing procedures is
provided below.

The shut-in test was conducted by connecting the flow regulator and vacuum gauge to the
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Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once
the sampling train was “closed”, the sample valve on the Summa® canister was opened and the
reading on the vacuum gauge was recorded. The Summa® canister sample valve was then
closed, and the vacuum gauge was observed to ensure no vacuum loss occurred. If the vacuum
reading remained the same, the shut-in test was considered successful. If vacuum loss occurred,
the flow regulator and/or brass cap was reseated, and the shut-in test was repeated until the
vacuum reading remained stable. Each Summa® canister passed the shut-in test.

Following a successful shut-in test, the Summa® canister was connected to the Teflon® sample
tubing using a brass nut and ferrule assembly to create an airtight seal and a leak check was
performed on the sampling point. The leak check was performed by constructing a shroud over
the sampling point and sample train and flooding the shroud with helium gas. Helium
concentrations inside the shroud were measured using a calibrated helium gas detector and
maintained at concentrations greater than 10%. Once helium concentrations stabilized within the
shroud, the sample tubing was purged outside of the shroud using a syringe and a three-way
valve to collect purged soil gas into a Tedlar® bag. The purged soil gas was then analyzed using
the helium gas detector to ensure that helium concentrations in the soil gas sample were less than
10% of the helium concentrations measured within the shroud. Each sub-slab soil gas sampling
point passed the helium leak check criteria.

Following successful leak checks, the sub-slab soil gas samples were collected by opening the
intake valve on the Summa® canister. Vacuum readings on the Summa® canisters were recorded
prior to and following the sampling period to ensure adequate sample volume was collected. A
vacuum of approximately 5 inches of mercury or more was maintained within each Summa®
canister at the conclusion of the sampling activities in accordance with DEQ DWM Vapor
Intrusion guidance. Following sample collection, the Summa® canisters were shipped to
Waypoint Analytical under standard chain-of-custody protocols for analysis of VOCs by EPA
Method TO-15. Upon receipt of the samples, the laboratory recorded the final received vacuum
pressure for each Summa® canister.

After sampling was completed, the sample locations were estimated by measuring from known
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benchmarks within the Site building (e.g., exterior walls, doorframes, etc.). The sample
locations were permanently abandoned, and the surfaces were repaired similar to pre-drilling
conditions.

6.2 Sub-Slab Soil Gas Sampling Results

A tabular summary of the sub-slab soil gas sample laboratory analytical results is provided as
Table 4. The analytical results were compared to the DEQ Residential and Non-Residential
Vapor Intrusion SGSLs dated January 2023. A copy of the laboratory analytical report and chain
of custody record is provided in Appendix C.

As shown in Table 4, laboratory analytical results indicate that several compounds were detected
at concentrations above the laboratory method detection limits in each sub-slab soil gas sample.
Low levels of the petroleum related compound naphthalene (up to 5.59 micrograms per cubic
meter [µg/m3]) were detected at concentrations above the DEQ Residential Vapor Intrusion
SGSL in several sub-slab soil gas samples (BF-SSV-1, BF-SSV-2, BF-SSV-4, BF-SSV-5, BF-
SSV-7, BF-SSV-8/ BF-SG-DUP, BF-SSV-9, and BF-SSV-11). No other compounds were
detected at concentrations exceeding the DEQ Vapor Intrusion SGSLs in the April 2023 sub-slab
soil gas samples collected at the Site.

Low levels of the chlorinated solvents PCE (up to 31.3 µg/m3) and TCE (up to 9.43 µg/m3) were
detected at concentrations above the laboratory method detection limits, but below the DEQ
Vapor Intrusion SGSLs in select sub-slab soil gas samples collected at the Site.

6.3 Vapor Intrusion Evaluation

The DEQ Vapor Intrusion SGSLs are very conservative and based upon a Target Cancer Risk
(TCR) of 1 x 10-6 for potential carcinogenic effects and a Target Hazard Quotient (THQ) of 0.2
for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not
typically warranted if the calculated cumulative lifetime incremental carcinogenic risk (LICR) is
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1 x 10-4 or less and the acceptable level for non-carcinogenic risk is a calculated cumulative
hazard index (HI) of 1.0 or less. Note that the HI is the sum of THQs for each detected analyte.

H&H utilized the DEQ Risk Calculator (January 2023) assuming residential and non-residential
land use scenarios to further evaluate potential cumulative risks for the soil gas to indoor air
vapor intrusion pathway for the proposed and existing Site buildings. To model the potential for
vapor intrusion under a hypothetical “worst-case” scenario for each existing Site building, H&H
conservatively calculated the cumulative risks using the highest concentration of any compound
detected in any sub-slab soil gas sample collected within each existing Site building including
the sub-slab soil gas samples collected by H&H (April 2023) and those previously collected by
Partner (May 2022). Risk calculator results are summarized in the table below. Copies of the
completed risk calculators are provided in Appendix E.

As shown in the table above, hypothetical worst-case scenario soil gas to indoor air risk
calculator results are acceptable for both residential (proposed use) and non-residential uses
(current use). Although results of assessment activities completed at the Site do not indicate a
potential vapor intrusion risk at unacceptable levels, H&H understands that a vapor intrusion
mitigation system will be installed during construction of the proposed buildings out of an
abundance of caution.

Brownfields assessment results indicate that a trace level of TCE was detected at a concentration
Evaluation Area Land Use
Scenario
Calculated
Cumulative
LICR
Calculated
Cumulative HI
Exceedance of
Acceptable
Levels?
2401 Distribution Street Residential 3.8 x 10-6 0.27 No
Non-Residential 2.8 x 10-7 0.021 No
2322 Dunavant Street Residential 2.6 x 10-6 0.20 No
Non-Residential 1.9 x 10-7 0.016 No
2400-2406 Distribution
Street
Residential 2.1 x 10-5 0.68 No
Non-Residential 1.6 x 10-6 0.054 No
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exceeding the DEQ Protection of Groundwater PSRG in one soil sample (BF-SB-6) collected
from the former loading docks and railroad spurs in the central portion of the Site. As noted
above, TCE (up to 19.2 µg/L) was detected at concentrations exceeding the DEQ Vapor
Intrusion GWSLs in four groundwater samples located in upgradient and central portions of the
Site (BF-TMW-4 through BF-TMW-7/BF-GW-DUP1). Results of the sub-slab soil gas
sampling activities indicate low levels of TCE (up to 9.43 µg/m3) at concentrations above the
laboratory method detection limits, but below the DEQ Vapor Intrusion SGSLs in several sub-
slab soil gas samples collected from each existing Site building. It should also be noted that TCE
(11.2 µg/m3) was detected above the laboratory method detection limits but below the DEQ
Vapor Intrusion SGSLs within the 2402 Dunavant Street Site building during previous sampling
activities completed by Partner in May 2022 (see Table 4).

Based on the results of exterior soil gas and sub-slab soil gas assessment activities completed at
the Site, the TCE detections in groundwater do not appear to pose a potential vapor intrusion
concern at unacceptable levels. Section 4.3 of the DWM Vapor Intrusion Guidance (March 2018
- Version 2) states as follows: "If soil gas and/or indoor air data has already been collected, using
screening levels for those media are more appropriate, however, groundwater data may still be
used to screen other areas of the site that may need to be investigated for potential VI."
Therefore, consistent with the Vapor Intrusion Guidance, the soil gas sampling results are more
appropriate for evaluating vapor intrusion risks at the Site, and utilizing the groundwater results
to impose additional sampling requirements related to TCE would not follow the conceptual Site
model, generally accepted industry practices, or the vapor intrusion guidance established by
DEQ.

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7.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location and following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis. One
trip blank was submitted for analysis of VOCs by EPA Method 8260. In addition, H&H
collected duplicate soil, groundwater, and sub-slab soil gas samples to evaluate the ability of the
laboratory to reproduce sample results. Duplicate samples were submitted to the laboratory for
the same analysis as the corresponding parent sample.

7.1 Trip Blank

The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. One trip blank accompanied the field VOC soil and groundwater samples and was
submitted for laboratory analysis of VOCs by EPA Method 8260. No VOC constituents were
identified above laboratory method detection limits in the trip blank. Laboratory analytical
results of the trip blank are included in the laboratory analytical report provided in Appendix C.

7.2 Field Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater
samples were collected directly into individual laboratory supplied sample containers using
sampling methodologies described in previous sections. The duplicate sub-slab soil gas sample
was collected concurrently with the parent sample using a laboratory supplied T-fitting which
allows for collection of two sub-slab soil gas samples from one sampling point simultaneously.
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The samples were analyzed for the same parameters as the parent samples, and the analytical
results were compared with those of the parent samples. The analytical results of the parent
samples and the duplicate samples were used to evaluate the cumulative precision of the
analytical method, sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1 for soil, Table 3 for groundwater, and Table 4 for sub-slab soil gas).
Review of the duplicate sample results for the soil, groundwater, and sub-slab soil gas samples
did not indicate significant variability compared with the results of the parent samples.

7.3 Investigation Derived Waste

Investigation derived waste (IDW) generated at the Site was containerized in 55-gallon drums
and staged on-Site. After the completion of the Site assessment activities, H&H collected IDW
samples from the containers for disposal characterization purposes. The IDW samples were
analyzed for TCLP VOCs by EPA Method 8260, TCLP SVOCs by EPA Method 8270, and
TCLP RCRA metals by EPA Method 6070/7471. As expected, laboratory analytical results
indicate that no compounds were detected at characteristically hazardous levels and the IDW was
transported off-Site for disposal as non-hazardous waste.

A copy of the IDW sample laboratory analytical report is provided in Appendix C.
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8.0 Summary and Conclusions

H&H completed Brownfields assessment activities at the Piedmont Plating & Anodizing
Company Brownfields property located at Distribution Street and Dunavant Street in Charlotte,
Mecklenburg County, North Carolina. The assessment activities were completed in general
accordance with the DEQ Brownfields approved Work Plan dated April 13, 2023. Brownfields
assessment activities included collection of soil, groundwater, and sub-slab soil gas samples for
laboratory analysis to further evaluate potential risks and to assist in management of Site media
during future redevelopment activities. In addition, a receptor survey was completed at the Site
and in the nearby area to obtain information about land use, water supply, basements,
underground utilities, drains, and surface water bodies in the vicinity of the Site. A brief
summary of the Brownfields assessment activities is provided below.

 The results of the receptor survey indicated that the Site is located in a transit-oriented
development (TOD-UC and TOD-NC) use area of Charlotte. No private water supply or
irrigation wells were identified on properties within 1,500 ft of the Site. Surface water
features were not observed at the Site.

 Results of soil assessment activities did not identify areas of impacts with the exception
of one soil sample (BF-SB-6) collected near the former loading docks and railroad spur
located in the central portion of the Site. Laboratory analytical results indicate that a
trace level of TCE was detected in the BF-SB-6 soil sample at a concentration above the
DEQ Protection of Groundwater PSRG, but below the DEQ Residential PSRG. Higher
levels of several PAHs and hexavalent chromium were detected in the BF-SB-6 soil
sample at concentrations above the DEQ Residential and/or Industrial/Commercial
PSRGs.

Lower levels of PAHs consistent with ubiquitous conditions in urban settings were
detected at concentrations above the DEQ Residential PSRGs but below the DEQ
Industrial/Commercial PSRGs in a soil sample collected near the former plating AST
staging area in the northeastern portion of the Site. No other compounds were detected at
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concentrations above the DEQ PSRGs in soil samples collected in former metal plating
operational areas at the Site.

 Results of the groundwater assessment activities identified PCE and/or TCE at
concentrations above the 2L Standards in upgradient samples collected in northeastern
and northern portions of the Site, and a sample collected in the central portion of the Site.
The concentrations of TCE also exceeded the DEQ Residential and/or Non-Residential
Vapor Intrusion GWSLs.

Results of the groundwater sampling activities indicate that the highest concentration of
TCE was detected in the northeastern and upgradient portion of the Site at the BF-
TWM-7 well location with concentrations decreasing to the west and concentrations
below the laboratory method detection limits in samples collected in southern portions of
the Site. Based on results of the groundwater sampling activities, the source of TCE is
attributed to an off-Site release (or releases) located east-northeast of the Site and impacts
in groundwater above the DEQ 2L Standard and DEQ Vapor Intrusion GWSLs are
limited to the northeastern, north-central, central portions of the Site.

 Results of sub-slab soil gas sampling activities completed within the existing Site
buildings identified naphthalene at concentrations exceeding the DEQ Vapor Intrusion
Residential SGSL. PCE and TCE were detected in several sub-slab soil gas samples at
concentrations above the laboratory method detection limits, but below the DEQ Vapor
Intrusion SGSLs. Results of cumulative risk calculations utilizing the highest
concentration of any compound detected in any sub-slab soil gas sample collected during
any sampling event indicate that there is no unacceptable risk of potential vapor intrusion
for a residential or non-residential use at the Site.

In summary, results of soil assessment activities indicate that soil impacts appear to be limited in
extent to areas near the 2322 Dunavant Street Site building (former AST staging area and the
loading dock/former rail spur). Based on results of soil assessment activities completed at the
Site, soil disturbed during redevelopment can be managed pursuant to a DEQ-approved EMP.
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Results of groundwater sampling activities indicate chlorinated solvent impacts at concentrations
above the applicable regulatory screening levels appear to be attributable to an off-Site source or
sources located east-northeast of the Site and impacts are limited in extent to upgradient portions
of the Site to the central portion of the Site. In the event groundwater is encountered during
future redevelopment activities, it can be managed in accordance with a DEQ-approved EMP.
Risks associated with the use of impacted groundwater at the Site will be addressed through the
implementation of a groundwater use restriction in the pending Brownfields Agreement.

Although hypothetical worst-case risk calculator results for the soil gas to indoor air vapor
intrusion pathways do not exceed unacceptable risk levels for residential and non-residential
uses, H&H understands that a vapor intrusion mitigations system approved by DEQ will be
installed during construction of proposed building. Based on review of the DEQ Brownfields
draft Minimum Mitigation and Sampling Requirements for Reuse memorandum dated February
2023, the vapor intrusion mitigation system requirements are within Matrix 2 with a cumulative
worst-case LICR <1x10-4 and a cumulative worst-case HI between 0.1 and 1.0 with detectable
levels of TCE in Site media.

Table 1 Summary of Soil Analytical Data Piedmont Plating & Anodizing Distribution Street & Dunavant Street Charlotte, North CarolinaH&H Job No. H&A-002Evaluation Area Background Northern Site BoundarySample IDBF-SB-1 BF-SB-2 BF-SB-3 BF-SB-4 BF-SB-5 BF-SB-6Date4/18/20234/18/2023 4/18/2023Sample Type Depth (ft bgs)4-6 0-2 0-2 0-2 0-2 0-2UnitsVOCs (8260D)1,2,4-Trimethylbenzene<0.0064 <0.006 <0.0084 <0.00680.0082 0.0178 63 370 12-- -- -- 4-Methyl-2-pentanone (MIBK)<0.0104 <0.0098 <0.0097 <0.0110.0484 J<0.01447,000 30,000 0.45-- -- -- Methylene Chloride0.048 C9 0.0648 C9 0.0534 0.165 C9 0.050 C9 0.11158 650 0.025-- -- -- Naphthalene0.0072 J, C8 0.007 J, C8<0.0053 <0.0060 <0.00350.0198 2.1 8.8 0.39-- -- -- Trichloroethene<0.0087 <0.0082 <0.0081 <0.0092 <0.00540.0290.87 4 0.021-- -- -- cis-1,2-Dichloroethene<0.0037 <0.0035 <0.0034 <0.0039 <0.00230.0134 J 13 78 0.41-- -- -- n-Propylbenzene<0.0038 <0.0036 <0.0036 <0.00410.0039 J<0.0053780 5,100 2.6-- -- -- SVOCs (8270E)1-Methylnaphthalene<0.127 <0.139 <0.143 <0.149 <0.1502.81 J 18 73 0.11-- -- --2-Methylnaphthalene<0.145 <0.159 <0.163 <0.169 <0.1715.08 48 600 3.1-- -- --Acenaphthene<0.127 <0.139 <0.143 <0.149 <0.15024.2 720 9,000 16-- -- --Anthracene<0.118 <0.130 <0.133 <0.139 <0.14030.5 3,600 45,000 1,300-- -- --Benzo(a)anthracene<0.121 <0.132 <0.136 <0.141 <0.142531210.35------Benzo(a)pyrene<0.125<0.137<0.141<0.146<0.14748.50.112.10.12-- -- --Benzo(b)fluoranthene<0.121 <0.132 <0.136 <0.141 <0.142641.1211.2------Benzo(g,h,i)perylene<0.140<0.154<0.158<0.164<0.16630.9NENENE------Benzo(k)fluoranthene<0.127<0.139<0.143<0.149<0.15022.81121012------Chrysene<0.131<0.144<0.148<0.154<0.15551.91102,10036------Dibenzofuran<0.130<0.143<0.147<0.153<0.154101623010------Fluoranthene<0.124<0.136<0.139<0.145<0.1461064806,000670------Fluorene<0.127<0.139<0.143<0.149<0.15021.34806,000.0110------Indeno(1,2,3-cd)pyrene<0.142<0.156<0.160<0.167<0.16829.81.1213.9------Naphthalene<0.123<0.135<0.138<0.144<0.14512.62.190.39------Phenanthrene<0.118<0.130<0.133<0.139<0.140116NENENE------Pyrene<0.147<0.161<0.165<0.172<0.17391.83604,500440------Metals (6020B/7470A/7199)Aluminum26,800 P6, R1NA NA NA NA NA16,000 230,000 110,000--18,900 - 26,800 7,000 - 100,000Arsenic0.51 J 1.2 2.9 1.1 1.9 2.2 0.68 3.0 5.8--0.51 - 2.4 1.0 - 18Barium158 93.5 118 69.8 118 151 3,100 47,000 580.0--22.1 - 158 50 - 1,000Cadmium 0.067 J 0.049 J 0.067 J<0.099 <0.0350.58 1.4 20 3-- <0.037 - 0.067 1.0 - 10Chromium (Total)154 M1 76.9 60.1 58.2 119 68.6 NE NE NE--80.6 - 154 7.0 - 300Chromium (VI)2.09<0.3151.944.892.3726.40.316.53.8--0.856 - 2.09NSChromium (III)15276.958.253.311742.223,000350,000360,000--79.7 - 152NSCopper69.6 M1NANANANANA6309,300700--27.8 - 69.63.0 - 100Lead0.7420.912.17.214.629.6400800250--0.74 - 9.7ND - 50Mercury <0.0190.019 J<0.00930.0310.013 J0.021 J4.770NE--<0.019 - 0.0270.03 - 0.52Nickel90.7NANANANANA3104,700130.0--10.3 - 90.7ND - 150Selenium<0.520.36 J0.16 J0.22 J0.43 J0.61781,2002.1--<0.52 - 0.63<0.1 - 0.8Silver<0.52<0.232.9<0.25<0.25<0.23781,2003.4--<0.52 - 2.9ND - 5.0 Zinc99.2 M1NANANANANA4,70070,0001,200--20.4 - 99.225 - 124Cyanide (4500)Cyanide 0.16 J, R1NA NA NA NA NA53114-- -- --Metals (6010 D TCLP) (mg/L)Chromium<0.0043 NA NA NA <0.0043 NA -- -- --5 mg/L-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics dated November 2004.3) Site-specific background metals data taken from soil samples BF-SB-1 and BF-SB-11, collected from the Site.4) Background metal ranges for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils; Al concentrations taken from eastern U.S. Soils.Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise specified.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the Residential PSRGs and background values in the case of metals. Underlined values exceed Industrial/Commercial PSRG.Italicized values exceed the Protection of Groundwater PSRGs.Trivalent chromium concentrations are calculated.VOCs = volatile organic compounds; SVOC = semi-volatile organic compounds; TCLP = Toxic Characteristic Leaching Procedure; ft bgs= feet below ground surfaceNS = not specified; NE = not established; -- = not applicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.M1 = Matrix spike exceeded the quality control limits; R1 = Relative percent difference in compound was outside control limits; C8 = Result may be biased high due to carryover from previously analyzed sample.P6 = Matrix spike recovery exceeded laboratory control limits due to high parent sample concentration; C9 = Common laboratory contaminant; B = analyte detected in associated laboratory method blank.Industrial/ Commercial PSRGs (1)Site-Specific Raqnge(3)Published Range (4)Grabmg/kgFormer Loading Docks & Railroad SpursBackground MetalsProtection of Groundwater PSRGs(1)Maximum Concentration for TCLP (2)Screening Criteria4/19/2023Residential PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Hoffman & Associates/H&A‐002 2401 Distribution St/Brownfields Assessment/Tables/Data Tables_Piedmont Plating_LESTable 1 (Page 1 of 2)Hart & Hickman, PC
Table 1 Summary of Soil Analytical Data Piedmont Plating & Anodizing Distribution Street & Dunavant Street Charlotte, North CarolinaH&H Job No. H&A-002Evaluation Area Interior Former Plating AreaBackgrund Sample IDBF-SB-7BF-SB-9 BF-SB-11Date4/17/20234/20/2023 4/17/2023Sample Type Depth (ft bgs)2-40-2 4-6UnitsVOCs (8260D)1,2,4-Trimethylbenzene<0.0062 <0.0068 <0.0066 <0.0042 <0.003863 370 12-- -- -- 4-Methyl-2-pentanone (MIBK)<0.01 <0.011 <0.0106 <0.0069 <0.00627,000 30,000 0.45-- -- -- Methylene Chloride0.0471 C9 0.0416 J, C9 0.0524 C9 0.032 C9 0.0264 C958 650 0.025-- -- -- Naphthalene<0.0055 <0.006 <0.0058 <0.0037 <0.00342.1 8.8 0.39-- -- -- Trichloroethene<0.0084 <0.0092 <0.0089 <0.0057 <0.00520.87 4 0.021-- -- -- cis-1,2-Dichloroethene<0.0035 <0.0039 <0.0038 <0.0024 <0.002213 78 0.41-- -- -- n-Propylbenzene<0.0051 <0.0041 <0.0039 <0.0025 <0.0023780 5,100 2.6-- -- -- SVOCs (8270E)1-Methylnaphthalene<0.141 <0.143 <0.183 <0.154 <0.14818 73 0.11-- -- --2-Methylnaphthalene<0.161 <0.162 <0.165 <0.175 <0.16948 600 3.1-- -- --Acenaphthene<0.141 <0.143 <0.145 <0.154 <0.148720 9,000 16-- -- --Anthracene<0.132 <0.133 <0.135 <0.143 <0.1383,600 45,000 1,300-- -- --Benzo(a)anthracene<0.1340.167 J 0.366 J<0.146 <0.1411 21 0.35-- -- --Benzo(a)pyrene<0.1390.146 J 0.323 J<0.151 <0.1460.11 2.1 0.12-- -- --Benzo(b)fluoranthene<0.1340.209 J 0.471<0.146 <0.1411.1 21 1.2-- -- --Benzo(g,h,i)perylene<0.156 <0.1580.230 J<0.170 <0.164NE NE NE-- -- --Benzo(k)fluoranthene<0.141 <0.1430.182 J<0.154 <0.14811 210 12-- -- --Chrysene<0.1460.168 J 0.360 J<0.159 <0.153110 2,100 36-- -- --Dibenzofuran<0.145 <0.146 <0.148 <0.158 <0.15216 230 10-- -- --Fluoranthene<0.1380.255 J 0.628 0.176 J<0.144480 6,000 670-- -- --Fluorene<0.141 <0.143 <0.145 <0.154 <0.148480 6,000 110-- -- --Indeno(1,2,3-cd)pyrene<0.159 <0.1600.212 J<0.172 <0.1661.1 21 3.9-- -- --Naphthalene<0.137 <0.138 <0.140 <0.148 <0.1432.1 9 0.39-- -- --Phenanthrene<0.1320.148 J 0.5 0.156 J<0.138NE NE NE-- -- --Pyrene<0.1630.255 J 0.642<0.178 <0.171360 4,500 440-- -- --Metals (6020B/7470A/7199)Aluminum16,300 17,800 20,500 24,100 18,900 16,000 230,000 110,000--18,900 - 26,800 7,000 - 100,000Arsenic2.2 2.4 2.0 2.3 2.4 0.68 3.0 5.8--0.51 - 2.4 1.0 - 18Barium18.0 43.7 49.4 100 22.1 3,100 47,000 580.0--22.1 - 158 50 - 1,000Cadmium <0.0900.070 J 0.066 J 0.17<0.0371.4 20 3-- <0.037 - 0.067 1.0 - 10Chromium (Total)57.9 27.9 77.1 73.2 80.6 NE NE NE--80.6 - 154 7.0 - 300Chromium (VI)0.577 J2.301.75 1.38 0.856 J 0.31 6.5 3.8--0.856 - 2.09 NSChromium (III)57.3 25.6 75.4 71.8 79.7 23,000 350,000 360,000--79.7 - 152 NSCopper20.9 22.0 40.7 46.5 27.8 630 9,300 700--27.8 - 69.6 3.0 - 100Lead7.9 14.4 38.2 21.9 9.7 400 800 250--0.74 - 9.7 ND - 50Mercury 0.034 0.026 0.045 0.047 0.027 4.7 70 NE-- <0.019 - 0.027 0.03 - 0.52Nickel7.4 7.0 15.7 20.2 10.3 310 4,700 130.0--10.3 - 90.7 ND - 150Selenium0.51 J 0.63 0.53 J 0.62 J 0.63 J 78 1,200 2.1-- <0.52 - 0.63<0.1 - 0.8Silver<0.25 <0.24 <0.25 <0.27 <0.2678 1,200 3.4-- <0.52 - 2.9 ND - 5.0 Zinc16.6 33.2 33.8 37.5 20.4 4,700 70,000 1,200--20.4 - 99.2 25 - 124Cyanide (4500)Cyanide0.42 0.27 J 0.33 J, B 0.26 J 0.24 J 5 31 14-- -- --Metals (6010 D TCLP) (mg/L)ChromiumNA NA NA NA NA -- -- --5 mg/L-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics dated November 2004.3) Site-specific background metals data taken from soil samples BF-SB-1 and BF-SB-11, collected from the Site.4) Background metal ranges for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils; Al concentrations taken from eastern U.S. Soils.Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise specified.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the Residential PSRGs and background values in the case of metals. Underlined values exceed Residential PSRG.Italicized values exceed the Protection of Groundwater PSRGs.Trivalent chromium concentrations are calculated.VOCs = volatile organic compounds; SVOC = semi-volatile organic compounds; TCLP = Toxic Characteristic Leaching Procedure; ft bgs= feet below ground surfaceNS = not specified; NE = not established; -- = not applicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.M1 = Matrix spike exceeded the quality control limits; R1 = Relative percent difference in compound was outside control limits; C8 = Result may be biased high due to carryover from previously analyzed sample.P6 = Matrix spike recovery exceeded laboratory control limits due to high parent sample concentration; C9 = Common laboratory contaminant; B = analyte detected in associated laboratory method blank.mg/kgResidential PSRGs (1)Industrial/ Commercial PSRGs (1)Protection of Groundwater PSRGs(1)Maximum Concentration for TCLP (2)4/18/2023GrabScreening Criteria Background Metals0-2BF-SB-8/BF-SB- DUPFormer Plating AST AreaSite-Specific Range (3)Published Range (4)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Hoffman & Associates/H&A‐002 2401 Distribution St/Brownfields Assessment/Tables/Data Tables_Piedmont Plating_LESTable 1 (Page 2 of 2)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation Data Piedmont Plating & AnodizingDistribution Street & Dunavant StreetCharlotte, North CarolinaH&H Job No. H&A-002Well IDTotal Well Depth (ft bgs)Screen Length (ft) Screen Interval (ft bgs)TOC Elevation (ft MSL)1Depth to Groundwater (ft below TOC)Groundwater Elevation (ft MSL)2BF-TMW-115105-15717.245.21712.03BF-TMW-27.552.5-7.5715.452.32713.13BF-TMW-3752-7713.371.11712.26BF-TMW-413103-13717.249.51707.73BF-TMW-515105-15716.834.45712.38BF-TMW-615105-15734.399.25725.14BF-TMW-722157-22732.169.20722.96BF-TMW-820155-20734.399.94724.46Notes:1) The top of casing (TOC) elevations were surveyed by H&H using a Spectra SP85 survying instrument.2) Groundwater elevations calculated using surveyed TOC elevations.The Spectra SP85 has an accuracy of approximately 2 centimeters.Depth to groundwater measurements collected by H&H on April 24, 2023.TMW = temporary monitoring well; ft bgs = feet below ground surface; MSL = mean sea levelhttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Hoffman & Associates/H&A‐002 2401 Distribution St/Brownfields Assessment/Tables/Data Tables_Piedmont Plating_LES5/15/2023Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Groundwater Analytical Data Piedmont Plating & Anodizing Distribution Street & Dunavant Street Charlotte, North CarolinaH&H Job No. H&A-002Evaluation AreaSite CenterSample IDBF-TMW-1 BF-TMW-2 BF-TMW-3 BF-TMW-4 BF-TMW-5 BF-TMW-6 BF-TMW-8Date4/19/2023 4/21/2023 4/20/2023 4/21/2023 4/20/2023UnitsVOCs (8260D)1,1-Dichloroethene<0.35 <0.35 <0.35 <0.35 <0.35 <0.350.75 J 0.86 J<0.35350 39 160Chloroform<0.43 <0.43 <0.430.44 J 1.31.80.57 J0.57 J0.80 J700.813.6Tetrachloroethene<0.29<0.290.58 J1.86.4<0.29<0.29<0.29<0.290.71248Trichloroethene<0.38<0.380.57 J2.212.28.518.719.2<0.38314.4cis-1,2-Dichloroethene0.77 J<0.38 <0.380.88 J 0.46 J<0.380.45 J 0.51 J<0.3870 50 210SVOCs (8270E)------Metals (6020/7470)AluminumNA NA NA NA NA NA342 349 231 ---- --Arsenic0.25 J 0.50 J 0.37 J 0.22 J 0.16 J 0.13 J 0.19 J 0.18 J 0.098 J 10-- --Barium28.5 41.0 37.4 37.6 49.6 45.7 33.6 36.6 33.4 700-- --Cadmium<0.060<0.0600.083 J<0.060<0.20<0.060<0.060<0.060<0.0602----Chromium1.10.64 J1.35.71.9<0.500.73 J0.79 J1.210----CopperNANANANANANA1.3 J1.3 J1.7 J1,000----Lead<0.077<0.0774.6<0.0770.35 J0.078 J0.081 J<0.077<0.07715----NickelNANANANANANA3.33.34.2100----Selenium0.12 J0.47 J0.21 J0.14 J0.16 J0.36 J0.27 J0.25 J0.076 J20----Silver<0.070<0.070<0.070<0.070<0.070<0.070<0.070<0.070<0.07020----Mercury<0.12<0.12<0.12<0.12<0.12<0.12<0.12<0.12<0.1210.180.75ZincNANANANANANA<2.7<2.72.8 J1,000----Cyanide (4500)Cyanide NA NA NA NA NA NA <0.0060 <0.0060 <0.006070-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.2) DEQ Vapor Intrusion Groundwater Screening Levels (GWSLs) dated January 2023.Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the 2L Standard.Underlined values exceed the DEQ Residential Vapor Intrusion GWSLs. Italicized values exceed the DEQ Non-Residential GWSLs. NE = not established; -- = not applicable; BDL = below the laboratory method detection limits; NA = not analyzedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. BF-TMW-7/BF-GW-DUP1ALL BDL4/21/20234/18/2023Upgradient DowngradientUpgradientµg/LScreening Criteria 2L Standards (1) Residential GWSLs (2)Non-Residential GWSLs (2)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Hoffman & Associates/H&A‐002 2401 Distribution St/Brownfields Assessment/Tables/Data Tables_Piedmont Plating_LES5/15/2023Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Sub-Slab Soil Gas Analytical Data Piedmont Plating & Anodizing Distribution Street & Dunavant Street Charlotte, North CarolinaH&H Job No. H&A-002Evaluation AreaSample IDBF-SSV-1 BF-SSV-2 BF-SSV-3 BF-SSV-4 BF-SSV-5 BF-SSV-6 BF-SSV-7 BF-SSV-9 BF-SSV-10 BF-SSV-11 SG-1* SG-2*Sample Date4/17/20234/17/2023 4/17/2023 4/20/2023 4/17/2023Sample Type UnitsVOCs (TO-15)1,1,2,2-Tetrachloroethane<0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <0.104 <1.374.241.6 211,1,2-Trichloro-1,2,2-trifluoroethane<0.561 <0.561 <0.5610.567 J<0.561 <0.561 <0.561 <0.561 <0.561 <0.561 <0.561 <0.561 <1.53 <1.5335,000 440,0001,2,4-Trimethylbenzene<0.1106.33 5.11 51.7 4.96 7.20 5.5 5.18 5.11 14.6<0.11032.0 24.2 16.9 420 5,3001,2-Dichlorobenzene<0.096 <0.096 <0.0960.661 J<0.096 <0.096 <0.096 <0.096 <0.096 <0.096 <0.0960.841 J<1.20 <1.201,400 18,0001,3,5-Trimethylbenzene<0.2360.550 J<0.23612.2<0.2360.619 J<0.236 <0.236 <0.2363.11<0.23612.4 6.38 4.52 420 5,3001,4-Dichlorobenzene<0.186 <0.186 <0.1861.42 J<0.186 <0.186 <0.186 <0.186 <0.186 <0.186 <0.1861.95 J<1.20 <1.208.5 1101,4-Dioxane<0.435 <0.435 <0.435 <0.435 <0.435 <0.4350.673 J<0.435 <0.4350.493 J<0.435 <0.435 <0.721 <0.72119 2502-Hexanone<0.285 <0.285 <0.285 <0.285 <0.285 <0.285 <0.2850.688 J 0.679 J<0.285 <0.285 <0.285 <5.115.69 210 2,6002-Propanol5.05 B 3.62 J, B4.98 B39.64.20 J, B5.50 B22.7 B11.1 B11.2 B16.2 B15.6 B52.8 J<3.073.291,40018,0002,2,4-TrimethylpentaneNANANANANANANANANANANANA44.340.8NENE4-Ethyltoluene<0.1284.594.5013.6<0.1285.594.674.564.558.18<0.12812.822.215.8NENE4-Methyl-2-pentanone (MIBK)<0.121<0.1210.421 J0.643 J<0.121<0.1210.507 J0.696 J0.630 J1.32 J2.834.51<5.12<5.1221,000260,000Acetone12.87.48 B18.527.413.113.871.130.029.144.823.936.342.525.7NENEBenzene0.450 J0.268 J0.964 J1.83 B0.482 J0.396 J0.606 J0.360 J0.351 J0.415 J0.383 J5.6721.814.312160Carbon disulfide2.85 J0.333 J5.09 J1.89 J<0.0600.479 J, B0.999 J0.632 J0.607 J5.01 J1.13 J1.10 J2.0121.54,90061,000Chlorobenzene<0.107<0.107<0.1070.768 J<0.107<0.107<0.107<0.107<0.107<0.107<0.1072.71<0.924<0.9243504,400Chloroform1.90 J<0.0860.580 J2.42 J<0.0860.585 J0.507 J<0.086<0.0860.795 J1.35 J1.47 J<0.973<0.9734.153Chloromethane<0.067<0.067<0.067<0.067<0.067<0.067<0.067<0.067<0.067<0.067<0.0670.774 J1.141.036307,900Cyclohexane<0.161<0.161<0.161<0.1612.41 J<0.161<0.161<0.161<0.1612.02 J<0.1612.44 J<0.6895.8242,000530,000Dichlorodifluoromethane2.872.752.622.782.592.772.682.752.692.43 J40.23.56<1.702.387008,800EthanolNANANANANANANANANANANANA16.1 J16.3 JNENEEthyl acetate<0.136<0.136<0.1360.742 J<0.136<0.136<0.136<0.136<0.136<0.136<0.1365.69NANA4906,100Ethylbenzene<0.106<0.106<0.1068.03<0.106<0.1060.668 J<0.106<0.106<0.106<0.10614.826.217.437490Heptane<0.143<0.143<0.1431.40 J0.295 J0.467 J1.07 J<0.143<0.1430.381 J0.536 J5.9011.909.612,80035,000Methyl Ethyl Ketone (MEK)1.35 J3.052.234.361.42 J1.562.8318.818.84.682.749.455.043.9835,000440,000Methylene Chloride11.73.709.863.6213.318.79.692.752.578.455.9430.8<0.694<0.6943,40053,000Naphthalene4.835.59<0.1835.394.93<0.1834.794.804.834.79<0.1834.94<3.30<3.302.836n-Hexane0.377 J<0.0470.285 J2.540.345 J0.296 J0.877 J0.285 J0.260 J0.807 J0.440 J40.522.738.14,90061,000Propene<0.242<0.242<0.2425.31<0.242<0.2422.77<0.242<0.242<0.242<0.2427.56<2.15<2.1521,000260,000Styrene<0.124<0.124<0.1246.78<0.124<0.124<0.124<0.124<0.1245.47<0.1248.39<0.851<0.8517,00088,000Tetrachloroethene31.30.488 J0.624 J<0.1810.820 J19.63.22 J0.827 J0.827 J1.08 J5.673.76<1.364.242803,500Tetrahydrofuran0.238 J0.990 J0.377 J<0.107<0.1070.669 J1.33 J20.020.11.990.867 J0.468 J<0.590<0.59014,000180,000Toluene1.00 J0.388 J0.795 J18.61.39 J1.25 J3.321.45 J1.41 J1.63 J0.904 J60.514993.835,000440,000Trichloroethene9.43<0.199<0.199<0.199<0.1998.382.25<0.199<0.199<0.199<0.199<0.199<1.0711.714180Trichlorofluoromethane2.37 J1.60 J1.69 J1.60 J1.56 J1.93 J1.93 J1.69 J1.58 J1.42 J1.69 J3.991.601.53NENEm&p-Xylene4.89 J<0.2175.6532.05.03 J4.98 J7.225.45 J5.38 J5.35 J4.90 J54.410163.37008,800o-Xylene<0.157<0.1570.712 J16.7<0.1570.655 J1.61 J0.503 J0.503 J1.54 J<0.15726.737.323.17008,800Xylene (total)4.89 J<0.1576.36 J48.75.03 J5.64 J8.83 J5.95 J5.88 J6.89 J4.90 J81.1138.386.47008,800DEQ Cumulative Risk Calculator (2)Residential Worst-Case LICR Residential Worst-Case Non-Carcinogenic HINon-Residential Worst-Case LICR Non-Residential Worst-Case Non-Carcinogenic HI1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023.2) DEQ Cumulative Risk Calculator dated January 2023.*Sub-slab soil gas points installed and sampled by Partner Engineering on May 12, 2022. Compound concentrations reported to the laboratory reporting limits (RDL).Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits, unless otherwise specified.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the table above.Bold values indicate an exceedance of Residential SGSLs. VOCs = volatile organic compounds; NE = not established; NA = not analyzed J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration; B = Analyte detected in method blank<1.00.27Acceptable Risk Levels2.6 x 10-60.202.1 x 10-50.68 2.8 x 10-71.9 x 10-71.6 x 10-60.0210.0160.0544/18/20233.8 x 10-62322 Dunavant Street<1.0 x 10-42400-2406 Dunavant Street5/12/2022Sub-Slab Soil Gasµg/m3Residential SGSLs (1)Non-Residential SGSLs (1)Screening Criteria4/20/2023BF-SSV-8 / BF-SG-DUP4/17/20232401 Distribution Streethttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Hoffman & Associates/H&A‐002 2401 Distribution St/Brownfields Assessment/Tables/Data Tables_Piedmont Plating_LES5/15/2023Table 4 (Page 1 of 1)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed June, 2022.
SITE LOCATION MAP
PIEDMONT PLATING & ANODIZING
DISTRIBUTION STREET & DUNAVANT STREET CHARLOTTE, NORTH CAROLINA
DATE: 5-15-23
JOB NO: H&A-002
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT02,000 4,000
SCALE IN FEET
SITE
Path: C:\Users\sperry\OneDrive - Hart & Hickman\My Documents\ArcGIS\PROJECTS\H&A-002\H&A-002 Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2022
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. H&A-002
DATE: 5-15-23
FIGURE NO. 2
PIEDMONT PLATING & ANODIZING
DISTRIBUTION STREET & DUNAVANT STREET
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
SITE AND BROWNFIELDS PROPERTYBOUNDARY
PARCEL LINE
POLE-MOUNTED TRANSFORMER
DUMPSTER
GREASE TRAP
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROMMECKLENBURG COUNTY GIS, 2023.
2. BPN: BROWNFIELDS PROPERTY NUMBER
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyDUNAVANT STREETDISTRIBUTION STREETPARKER MEDICAL ASSOCIATES(2400 DISTRIBUTION STREET)
B&G LIEBERMAN(2412-2420 DISTRIBUTION STREET)
GRIER INTERIORS(2326-2328 DISTRIBUTION STREET)
UNDER CONSTRUCTION(CRAYTON PRINTING
BROWNFIELDS PROPERTY
[BPN: 24025-20-060])
JUNCTION 1504 LUXURYAPARTMENT COMPLEX(1504 MAINLINE BOULEVARD)(SOUTH END TRANSIT
BROWNFIELDS PROPERTY
[BPN: 10036-06-060]
COXSCHEPP CONSTRUCTION(2408-2410 DUNAVANT STREET)
PARKING LOT
(2401 DISTRIBUTION STREET)
(2322 DUNAVANT STREET)
(2400 DUNAVANT STREET)
(2402-2406 DUNAVANT STREET)
REVISION NO. 0
JOB NO. H&A-002
DATE: 5-15-23
FIGURE NO. 3
PIEDMONT PLATING & ANODIZINGDISTRIBUTION STREET & DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
PROPOSED RETAIL SPACE
PROPOSED LOBBY SPACE
PROPOSED UTILITY SPACE
PROPOSED PARKING AREA
PRIOR TEMPORARY MONITORINGWELL LOCATION
PRIOR SOIL BORING LOCATION
PRIOR SOIL GAS SAMPLE LOCATION
TEMPORARY MONITORING WELLLOCATION
CO-LOCATED TEMPORARYMONITORING WELL AND SOIL BORINGLOCATION
SUB-SLAB GAS SAMPLE LOCATION
SOIL BORING LOCATION
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2022.
2. PRIOR SAMPLE LOCATIONS OBTAINED FROM PHASE II SUBSURFACE INVESTIGATION REPORTS PREPARED BY PARTNER ENGINEERING DATED MAY 2021, DECEMBER 2021, AND MAY 2022.
3. *GROUNDWATER SAMPLE NOT COLLECTED DUE TO DRILL RIG REFUSAL PRIOR TO ENCOUNTERING GROUNDWATER.
4. **SOIL SAMPLE BF-SB-10 COULD NOT BE
COLLECTED DUE TO A GRAVEL LAYER BENEATH BUILDING SLAB AT THIS LOCATION.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyDUNAVANT STREETDISTRIBUTION STREETSG-1SG-2
SG-1
SG-2
SG-3 B-1
SG-1
SG-2
TMW-1*
B-1*
B-2*
B-3*
BF-SSV-1
BF-SSV-2
BF-SSV-8
BF-TWM-1/SB-1
BF-TMW-3/SB-2
BF-TMW-4
BF-SB-10**
BF-SB-8BF-SB-9
BF-SSV-7
BF-SSV-9
BF-SSV-10
BF-SSV-11
BF-SSV-6
BF-SSV-5
BF-SB-3
BF-SB-5
BF-SB-4
BF-SB-6
BF-SSV-4
BF-SSV-3
BF-TMW-6
BF-TMW-7/BF-SB-7
BF-TWM-2
FORMER RAILROAD SPURS
BF-TMW-5
BF-TMW-8/SB-11
B
E
A
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S

B
VDU
N
A
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ST
DUN
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FAI
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A
V
DIANA DRDISTRIBUTION STRECEPTOR SURVEY MAP
PIEDMONT PLATING & ANODIZINGDISTRIBUTION STREET & DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 4
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 400 800
SCALE IN FEET
N
DATE: 5-15-23
JOB NO. H&A-002
NOTES:
1. PARCEL AND ZONING DATA AND AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, 2023.
1,500 FOOT RADIUS LEGEND
SOURCE PROPERTY BOUNDARY
SURFACE WATER FEATURE
MIXED USED ZONING
BUSINESS ZONING
INDUSTRIAL ZONING
TRANSIT ORIENTED DEVELOPMENT ZONING
RESIDENTIAL ZONING
S:\AAA-Master Projects\Hoffman & Associates\H&A-002 2401 Distribution St\Brownfields Assessment\Figures\RECEPTOR_SURVEY.mxdALLIANCE CENTER FOR EDUCATION(2705 BALTIMORE AVENUE)
INSET1" = 150'
TITLE
PROJECT
DUNAVANT STREETDISTRIBUTION STREETGAS LINE
SANITARY SEWER
WATER LINE
OVERHEAD ELECTRIC LINE
SS
GAS
W
O/H
PARCEL BOUNDARY LINE
O/H
O/H
O/H
O/H
O/H
SSSSSSSSSSSSSSSSSSSSSS
SSSSSSSSSS SSSSSSO/H
O/H
GASGASGASGASGASGAS
GAS
GAS
WW WWWWW
W W
WGASWWWWWW COMMUNICATION
(722.96)
(725.14)
(707.73)
(724.46)
(712.38)
(712.03)
(713.13)
(712.26)7237217197177157137237
2
1
7
1
9
7
1
7
7
1
5
7
1
3
REVISION NO. 0
JOB NO. H&A-002
DATE: 4-26-23
FIGURE NO. 5
PIEDMONT PLATING & ANODIZING
DISTRIBUTION STREET & DUNAVANT STREET
CHARLOTTE, NORTH CAROLINA
SHALLOW GROUNDWATERPOTENTIOMETRIC MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
PROPOSED RETAIL SPACE
PROPOSED LOBBY SPACE
PROPOSED UTILITY SPACE
PROPOSED PARKING AREA
TEMPORARY MONITORING WELL LOCATION
CO-LOCATED TEMPORARY MONITORING WELLAND SOIL BORING LOCATION
GROUNDWATER ELEVATION (FT MSL)
GROUNDWATER ELEVATION CONTOUR (FT MSL)(DASHED WHERE INFERRED)
INFERRED GROUNDWATER FLOW DIRECTION
NOTES:
1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2023.
2. DEPTH TO GROUNDWATER MEASUREMENTS WERE COLLECTED BY H&H ON 4/24/23.
3. WELL LOCATIONS AND ELEVATIONS WERE MEASURED BY H&H USING A SPECTRA SP85 SURVEYING INSTRUMENT.
4. BF-TMW-4 WAS INSTALLED IN BEDROCK USING
AIR ROTARY DRILLING TECHNIQUES. THE POTENTIOMETRIC SURFACE IN THIS WELL IS
UNDER HYDROSTATIC PRESSURE AND WAS NOT USED FOR CONTOURING.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 GeologyDUNAVANT STREETDISTRIBUTION STREETBF-TMW-6
BF-TMW-7/BF-SB-7
BF-TWM-2
BF-TMW-5
BF-TWM-1/SB-1
BF-TMW-3/SB-2
BF-TMW-4
BF-TMW-8/SB-11
723
(725.14)S:\AAA-Master Projects\Hoffman & Associates\H&A-002 2401 Distribution St\Brownfields Assessment\Figures\H&A-002-BF_SAMPLE.dwg, FIG 5, 5/15/2023 3:04:41 PM, shaynes
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/hoffman & associates/h&a-002 2401
distribution st/brownfields assessment/report/26061- draft brownfields assessment report - piedmont plating.doc

Appendix A

Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Piedmont Plating & Anodizing
Address:Distribution Street and Dunavant Street
City:Charlotte
County:Mecklenburg
Brownfields Project Number: 26061-22-060
Property and Building Characteristics
a. Provide occupancy and use information.
The 2322 Dunavant Street Site building is occupied by Barton Malow, The Dunavant, and a vacant tenant space
The 2400 Dunavant Street Site building is unoccupied
The 2402-2406 Dunavant Street Site building is occupied by SL Laser and a vacant tenant space
The 2401 Distribution Street building is constructed as a one-story office building.
The 2322 Dunavant Street building is constructed as a one-story office and restaurant building.
The 2400 Dunavant Street building is constructed as a one-story warehouse building.
The 2402-2402 Dunavant Street building is constructed as a one-story warehouse building.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The 2401 Distribution Street building foundation consists of a slab-above-grade.
The 2322 Dunavant Street building foundation consists of a slab-above-grade.
The 2400 Dunavant Street building foundation consists of a slab-above-grade.
The 2402-2406 Dunavant Street building foundation consists of a slab-above-grade.
The 2401 Distribution Street building has a forced air- not ducted HVAC system.
The 2322 Dunavant Street building has a forced air- not ducted HVAC system.
The 2400 Dunavant Street building has a forced air- ducted HVAC system.
The 2404-2406 Dunavant Street building has a forced air- ducted HVAC system.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No subslab ventilation systems are currently in place. It is unknown if a moisture barrier is currently in-place
beneath the Site buildings.
The Brownfields property will be developed with high
density apartments and a parking garage.% of property that is grassed areas (unpaved)
% of property that is agricultural crops
% of property that is paved
Size of Property (acres)
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design considerations (e.g. positive pressure?).
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information requested below. Distances are measured from
the site property boundary unless otherwise indicated by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
~2.6
~5
0
~30
The 2401 Distrubution Street Site building is vacant
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If numerous buildings are on-site, consult with
your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
0
~65
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
East
South
Southwest
West
Northwest
N----
N----
N----
Utilities
Is there a septic system on-site? (Y or N) No
Please provide the utility providers for the subject property
a. Natural Gas: Piedmont Natural Gas (underground)
b. Sewer: Charlotte Water (underground)
c. Electricity: Duke Energy (above and below ground)
d. Other: Communication (underground)
For surrounding properties, please complete the following table with available information.
N----
Y On-Site NE/SE
N----
Y On-Site NW
Y On-Site SE
Y On-Site SE
Y On-Site NW/SE
Is there a residence within 1,000 ft of the Property?
Is a sanitary sewer within 100 ft of the Property boundary?
Is a buried electrical cable main within 100 ft of Property boundary?
Is a water line main within 100 ft of Property boundary?
NA
NA
NA
Transit Oriented District - Transit (TOD-TR)
Transit Oriented District - Transit (TOD-TR)
Transit Oriented District - Transit (TOD-TR)
Transit Oriented District - Transit (TOD-TR)
For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction material, and diameter of the utilities. In addition, please
provide the following information on utility providers. If additional assessment is required, the public utility locators should be contacted. This information can then be added
to a site map.
Y/N *
NA
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If specific receptors are present, please
provide addresses of the facilities.
Proposed Usage
Is a storm water pipe within 100 ft of the Property boundary?
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject property.
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance (ft)
--
--
Current Use/Occupant
Is a school or daycare center within 1,000 ft of the Property?
DirectionUtility/Potential Receptor
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Transit Oriented District - Transit (TOD-TR)NA
Transit Oriented District - Transit (TOD-TR)NA
Is there a basement within 1,000 ft of the Property
Distance (ft) Address
--
Zoning/Land Use
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
Charlotte Water
N -- -- --
N -- ----
N -- ----
Surface Water & Wetlands
Unnamed Tributary of Irwin Creek
No
b. List the uses of the water body.
c. What is the source of the water for the water body?
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
impoundments)
If no on-site surface water features, what is the nearest
surface water body?
Are there any wetlands present on the property? If no
wetlands on-site, are wetlands suspected on adjoining
properties?
a. Is the water body naturally developed or man-made?
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the Property.
No
Are there surface water features on the property? (If yes,
please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the water providers name.
Distance (ft) Direction
Provide Information regarding Surface Water and Wetlands
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
AddressY/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield survey within 1,500 ft of the property
boundaries should be completed to determine if water supply or irrigation wells may be present. Information from applicable databases can and should be utilized; however,
should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please
attach a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
Rev. 09/2015 Page 3 of 3
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distribution st/brownfields assessment/report/26061- draft brownfields assessment report - piedmont plating.doc
Appendix B

Boring Logs & Well Abandonment Records
NOTES: Hand Auger to 5 ft bgs; Direct Push Technology to 7 ft bgs; Hollow Stem Auger to 16 ft bgs.
BF-SB-1 soil sample collected from 4-6 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
BF-TMW-1 groundwater sample analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
Well No.
Page:
WELL LOG
BF-TMW-1/BF-SB-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
04/18/2023
04/18/2023
IET
Hand Auger, Direct Push, Hollow Stem
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
16
6
Grab, Direct Push
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') Asphalt
(6') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, tan/brown
(10') SILT (ML); some clay, medium plasticity, medium stiff, moist, brown
(16') Boring terminated
0.4
0.2
1.3
1.7
1.7
4.2
1.8
1.9
0
5
10
15
20
25
30
16
1
0.100
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
(1') SILT (ML); medium stiff, moist, tan/brown
BF- SB-1
DP
GR
8.32
9.51
NOTES: Hand Auger to 5 ft bgs; Direct Push Technology to 7 ft bgs.
BF-SB-2 soil sample collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
BF-TMW-3 groundwater sample analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant Steet, Charlotte, NC
WELL LOG
Boring No.
Page:
BF-TMW-3/BF-SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
0
5
10
(0') Asphalt
(1') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, dark gray/green
(4.5') Lean CLAY (CL); medium plasticity, medium stiff, wet, tan/brown, with brick layer
(5') Lean CLAY (CL); medium plasticity, medium stiff, wet, tan/brown
1.5
3.0
2.1
0
5
10
GR
DP
(7') Boring terminated
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
TimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleSample Type(3') Lean CLAY (CL); medium plasticity, medium stiff, wet, tan/brown
04/19/2023
04/19/2023
IET
Hand Auger, Direct Push
Power Probe 9510
Ann Marie Lindley
7
3.25
7
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
Grab, Direct Push
BF-
SB-2
4.93
1.69
NOTES: BF-SB-3 collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Hart & Hickman
Hand Auger
Hand Auger
Ann Marie Lindley
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(3') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown with graymottling
0.0
0.0
0.0
0
5
10
(1') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown
BF- SB-3GR
Grab
(5') Boring terminated
NOTES: BF-SB-4 collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Hart & Hickman
Hand Auger
Hand Auger
Ann Marie Lindley
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt/Brick 0.8
3.1
3.4
0
5
10
(1') Lean CLAY (CL); medium plasticity, medium stiff, moist, greenish-gray and tan
GR
Grab
(5') Boring terminated
BF- SB-4
NOTES: BF-SB-5 collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Hart & Hickman
Hand Auger
Hand Auger
Ann Marie Lindley
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') ORGANIC SOIL (OL); Grass
(4') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, orange/tan
0.6
0.5
0.4
0
5
10
(1') SILT (ML); some clay, medium stiff, moist, tan/brown/red with mottling
BF- SB-5GR
Grab
(5') Boring terminated
NOTES: BF-SB-6 collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, and Hexavalent Chromium.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Hart & Hickman
Hand Auger
Hand Auger
Ann Marie Lindley
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(3') SILT (ML); some clay, medium stiff, moist, tan/reddish-brown with gray mottling
0.5
0.0
0.1
0
5
10
(1.5') SILT (ML); medium stiff, moist, brown, with mica
BF- SB-6
(2.5') SILT (ML); some clay, medium stiff, moist, reddish-brown
Grab
GR
(5') Boring terminated
NOTES: Hand Auger to 5 ft bgs; Direct Push Technology to 9 ft bgs; Hollow Stem Auger to 25 ft bgs.
BF-SB-7 soil sample collected from 2-4 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, Hexavalent Chromium, and Cyanide.
BF-TMW-7 groundwater sample analyzed for VOCs, SVOCs, RCRA Metals, and Cyanide.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
Well No.
Page:
WELL LOG
BF-TMW-7/BF-SB-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
04/17/2023
04/17/2023
IET
Hand Auger, Direct Push, Hollow Stem
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25
3.25
Grab
9.14
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') Asphalt
(2') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-tan,
mottling
(7') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, tan
(9') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, white/tan
(12') SILT (ML); some clay, trace sand, medium stiff, moist, tan/brown/white
(25') Boring terminated
1.0
0.7
0.6
0.8
0.9
0.7
0.0
0.7
0.5
0.2
0.0
1.3
BF-
0
5
10
15
20
25
30
25
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
(15') SILT (ML); some clay, trace sand, medium stiff, moist, reddish-brown
(16') Lean CLAY (CL); some silt, medium stiff, moist, brown
(20') SILT (ML); some clay, medium stiff, moist, brown
(18') Lean CLAY (CL); some silt, trace sand, medium stiff, moist, brown with mottling
SB-7
11.67
NOTES: BF-SB-8/BF-SB-DUP collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, Hexavalent Chromium and Cyanide.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-8/BF-SB-DUP
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Drilling Company
Hand Auger; Direct Push
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab, Direct Push
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(1.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-brown
(3') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-tan
(7') SILT (ML); some clay, medium stiff, moist, white/gray
0.5
0.8
0.2
1.0
BF-SB-8
0
5
10
GR
DP
BF-SB-DUP1
(8') Boring terminated
NOTES: BF-SB-9 collected from 0-2 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, Hexavalent Chromium and Cyanide.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant Steet, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-9
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
Drilling Company Hand
Hand Auger; Direct Push
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Concrete
(0.5') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, dark reddish-brown
(4') Poorly graded GRAVEL (GP)
(5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, light
reddish-brown
0.2
0.5
0.6
0.5
0
5
10
GR
DP
Grab, Direct Push
(8') Boring terminated
BF- SB-9
NOTES:Hand Auger to 5 ft bgs; Direct Push Technology to 10 ft bgs; Hollow Stem Auger to 25 ft bgs.
BF-SB-11 soil sample collected from 4-6 ft bgs and analyzed for VOCs, SVOCs, RCRA Metals, Hexavalent Chromium, and Cyanide.
BF-TMW-8 groundwater sample analyzed for VOCs, SVOCs, RCRA Metals, and Cyanide.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant
Street, Charlotte, NC
WELL LOG
Well No.
Page:
BF-TMW-8/BF-SB-11
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
04/17/2023
04/17/2023
IET
Hand Auger, Direct Push, Hollow Stem
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25
8.85
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') Asphalt
(1') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-brown
(7') SILT (ML); some clay, medium stiff, moist, yellow/tan
(9') As Above: with black mottling
(10') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, tan
(12') SILT (ML); some clay, medium stiff, moist, brown
(16') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist,
reddish-brown/tan
(20') Lean CLAY (CL); medium plasticity, medium stiff, moist, brown
(25') Boring terminated
0.0
0.0
0.5
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.2
0.0
1.3
BF-SB-11
0
5
10
15
20
25
30
25
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DP
GR
HS
6.00Grab, Direct Push, Hollow Stem
17.6
NOTES: Hand Auger to 5 ft bgs; Direct Push Technology to 7 ft bgs.
BF-TMW-2 analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002
Distribution Street and Dunavant Steet, Charlotte, NC
BORING LOG
Boring No.
Page:
BF-TMW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/17/2023
4/17/2023
IET
Hand Auger; Direct Push
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
7.50
3.25
0
5
10
(0') Asphalt
(1') SILT (ML); some fine gravel, medium stiff, moist, reddish-brown/tan
(4') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown
(5') Lean CLAY (CL); some silt, some fine gravel, medium plasticity,
medium stiff, moist, brown
0.3
0.7
0.1
1.3
0
5
10
GR
DP
Grab, Direct Push
(7.5') Boring terminated
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
7.50
2
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
TimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleSample Type5.56
4.11
NOTES: Switched to air rotary at 5 feet.
BF-TMW-4 analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002Distribution Street and Dunavant
Street, Charlotte, NC
Well No.
Page:
WELL LOG
BF-TMW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
04/19/2023
04/20/2023
IET
Hand Auger, Hollow Stem Auger (HSA)
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
13
6.00
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
(6') SILT (ML); some clay, soft, moist, brown
(13') Boring terminated
0.8
1.2
1.3
0
5
10
15
13
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
(0') Asphalt
(1') SILT (ML); some clay, some gravel, medium stiff, moist, brown
GR
HSA
Grab, HSA
(5') HSA refusal. Switched to air rotary.
6 - 13' Void encountered100% Recovery0% Recovery9.13
12.64
NOTES: BF-TMW-5 analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002Distribution Street and Dunavant
Street, Charlotte, NC
Well No.
Page:
WELL LOG
BF-TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15
6.00
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15 (15') Boring terminated
1.0
2.3
0.3
0
5
10
15
(0') Asphalt
(1') Lean CLAY (CL); some silt, trace sand, medium plasticity,
medium stiff, moist, tan/gray
GR
HSA
Grab
(5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, tan/brown, mica
(6') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, tan/brown
15
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
04/17/2023
04/17/2023
IET
Hand Auger, Hollow Stem
Power Probe 9510
Ann Marie Lindley
(4') Lean CLAY (CL); some silt, trace sand, medium plasticity, medium stiff, moist, gray
(10') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown
2.1
1.1
1.3
4.6
0.9
6.31
4.35
NOTES: BF-TMW-6 analyzed for VOCs, SVOCs, and RCRA Metals.
generated using GroundLogs.online
Client:
Project:
Address:
Hoffman & Associates
H&A-002Distribution Street and Dunavant
Street, Charlotte, NC
Well No.
Page:
WELL LOG
BF-TMW-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
04/18/2023
04/18/2023
IET
Hand Auger, Hollow Stem Auger (HSA)
Power Probe 9510
Ann Marie Lindley
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15
6.00
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15 (15') Boring terminated
8.1
2.2
2.0
0
5
10
15
15
1
0.100
Sch 40 PVC Slotted
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
(0') Asphalt
(1.5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, reddish-
brown
GR
HSA
Grab, HSA
(5') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, gray/brown
(7') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, tan/brown 2.6
1.9
1.0
0.5
1.6
11.92
9.99
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
ertification:
ture of Certified Well Contracto
Terry White
3287-A one
1/2
IET
Sip 70003135
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2401 Distribution St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 22 80 51 59
TMW-1
16
4
5.51
6
10
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
8.Certification:
Signature of Certified Well Con
Terry White
3287-A one
1/4
IET
Sip 70003135
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2401 Distribution St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 22 80 51 59
TMW-2
7.5
4
2.26
2.5
5
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
rtification:
ture of Certified Well Contracto
Terry White
3287-A one
1/4
IET
Sip 70003135
15LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2401 Distribution St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 22 80 51 59
TMW-3
7
4
1.69
2
5
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Certification:
nature of Certified Well Contrac
Terry White
3287-A one
1
IET
Sip 70003135
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2401 Distribution St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 22 80 51 59
TMW-4
13
4
9.15
3
10
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
rtification:
ure of Certified Well Contractor
Terry White
3287-A one
3/4
IET
Sip 70003135
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2401 Distribution St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 22 80 51 59
TMW-5
15
4
4.34
5
10
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Certification:
nature of Certified Well Contrac
Terry White
3287-A one
1
IET
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2322 Dunavant St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 20 80 51 57
TMW-6
15
4
9.13
5
10
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Certification:
gnature of Certified Well Contra
Terry White
3287-A one
1
IET
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2322 Dunavant St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 20 80 51 57
TMW-7
22
4
8.85
7
15
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
fication:
e of Certified Well Contractor or
Terry White
3287-A one
1
IET
25LB
4/28/2023
Bentonite holes from bottom to top. Capped with concrete.
Piedmont Plating & Anodizing Company
2322 Dunavant St. Charlotte 28203 5/1/2023
Mecklenburg
35 12 20 80 51 57
TMW-8
20
4
9.73
5
15
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/hoffman & associates/h&a-002 2401
distribution st/brownfields assessment/report/26061- draft brownfields assessment report - piedmont plating.doc
Appendix C

Laboratory Analytical Reports
#=CL#
May 15, 2023
LIMS USE: FR - LORYN SMITH
LIMS OBJECT ID: 92663594
92663594
Project:
Pace Project No.:
RE:
Loryn Smith
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
H&A-002
Dear Loryn Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
This report was revised on May 11, 2023, to report 6010D TCLP chormium on Pace samples 92663594001 and
92663594003.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 169
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92663594
H&A-002
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 169
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92663594
H&A-002
Pace Analytical Services National
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 169
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID Matrix Date Collected Date Received
92663594001 BF-SB-1 Solid 04/18/23 16:15 04/21/23 12:15
92663594002 BF-SB-2 Solid 04/19/23 14:45 04/21/23 12:15
92663594003 BF-SB-3 Solid 04/19/23 16:05 04/21/23 12:15
92663594004 BF-SB-4 Solid 04/19/23 14:50 04/21/23 12:15
92663594005 BF-SB-5 Solid 04/18/23 16:10 04/21/23 12:15
92663594006 BF-SB-6 Solid 04/18/23 16:05 04/21/23 12:15
92663594007 BF-SB-7 Solid 04/17/23 16:45 04/21/23 12:15
92663594008 BF-SB-8 Solid 04/18/23 15:30 04/21/23 12:15
92663594009 BF-SB-9 Solid 04/20/23 17:30 04/21/23 12:15
92663594010 BF-SB-11 Solid 04/17/23 13:20 04/21/23 12:15
92663594011 BF-TMW-1 Water 04/21/23 09:05 04/21/23 12:15
92663594012 BF-TMW-2 Water 04/21/23 09:05 04/21/23 12:15
92663594013 BF-TMW-3 Water 04/19/23 15:50 04/21/23 12:15
92663594014 BF-TMW-4 Water 04/21/23 10:25 04/21/23 12:15
92663594015 BF-TMW-5 Water 04/20/23 14:25 04/21/23 12:15
92663594016 BF-TMW-6 Water 04/21/23 08:25 04/21/23 12:15
92663594017 BF-TMW-7 Water 04/18/23 15:30 04/21/23 12:15
92663594018 BF-TMW-8 Water 04/20/23 09:55 04/21/23 12:15
92663594019 BF-SB-DUP Solid 04/18/23 00:00 04/21/23 12:15
92663594020 BF-GW-DUP Water 04/18/23 00:00 04/21/23 12:15
92663594022 TRIP BLANK Water 04/20/23 00:00 04/21/23 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 169
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92663594001 BF-SB-1 EPA 6010D 1 PASI-MDM
EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AANM
92663594002 BF-SB-2 EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92663594003 BF-SB-3 EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92663594004 BF-SB-4 EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92663594005 BF-SB-5 EPA 6010D 1 PASI-MDM
EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 169
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7199 1 PANSET
92663594006 BF-SB-6 EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
92663594007 BF-SB-7 EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AANM
92663594008 BF-SB-8 EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AANM
92663594009 BF-SB-9 EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AANM
92663594010 BF-SB-11 EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 169
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AEGC
92663594011 BF-TMW-1 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594012 BF-TMW-2 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594013 BF-TMW-3 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594014 BF-TMW-4 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594015 BF-TMW-5 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594016 BF-TMW-6 EPA 6020B 7 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92663594017 BF-TMW-7 EPA 6020B 11 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
SM 4500-CN-E-2011 1 PASI-AANM
92663594018 BF-TMW-8 EPA 6020B 11 PASI-AKRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
SM 4500-CN-E-2011 1 PASI-AANM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 169
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92663594019 BF-SB-DUP EPA 6020B 11 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANSET
SM 4500-CN-E-2011 1 PASI-AEGC
92663594020 BF-GW-DUP EPA 6020B 11 PASI-ACRW, KRL
EPA 7470A 1 PASI-ABM
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
SM 4500-CN-E-2011 1 PASI-AANM
92663594022 TRIP BLANK EPA 8260D 63 PASI-CCL
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-1 Lab ID: 92663594001 Collected: 04/18/23 16:15 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3015A
Leachate Method/Date: EPA 1311; 05/04/23 14:05
Pace Analytical Services - Minneapolis
6010D MET ICP, TCLP MICRO
Chromium ND mg/L 05/05/23 16:00 7440-47-305/05/23 13:270.10 0.0043 1
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 26800 mg/kg 04/28/23 09:31 7429-90-5 P6,R104/26/23 11:0431.5 6.4 1
Arsenic 0.51J mg/kg 04/27/23 15:32 7440-38-204/26/23 11:040.52 0.15 1
Barium 158 mg/kg 04/27/23 15:32 7440-39-304/26/23 11:040.31 0.079 1
Cadmium 0.067J mg/kg 04/27/23 15:32 7440-43-904/26/23 11:040.084 0.031 1
Chromium 154 mg/kg 04/27/23 15:32 7440-47-3 M104/26/23 11:042.1 0.41 1
Copper 69.6 mg/kg 04/27/23 15:32 7440-50-8 M104/26/23 11:041.0 0.32 1
Lead 0.74 mg/kg 04/27/23 15:32 7439-92-104/26/23 11:040.52 0.098 1
Nickel 90.7 mg/kg 04/27/23 15:32 7440-02-004/26/23 11:040.52 0.24 1
Selenium ND mg/kg 04/27/23 15:32 7782-49-204/26/23 11:040.52 0.11 1
Silver ND mg/kg 04/27/23 15:32 7440-22-404/26/23 11:040.52 0.21 1
Zinc 99.2 mg/kg 04/27/23 15:32 7440-66-6 M104/26/23 11:045.2 1.2 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury ND mg/kg 04/28/23 08:57 7439-97-604/26/23 11:070.019 0.0083 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 12:23 83-32-904/26/23 15:21362 127 1
Acenaphthylene ND ug/kg 04/27/23 12:23 208-96-804/26/23 15:21362 127 1
Aniline ND ug/kg 04/27/23 12:23 62-53-304/26/23 15:21362 141 1
Anthracene ND ug/kg 04/27/23 12:23 120-12-704/26/23 15:21362 118 1
Benzo(a)anthracene ND ug/kg 04/27/23 12:23 56-55-304/26/23 15:21362 121 1
Benzo(a)pyrene ND ug/kg 04/27/23 12:23 50-32-804/26/23 15:21362 125 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 12:23 205-99-204/26/23 15:21362 121 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 12:23 191-24-204/26/23 15:21362 140 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 12:23 207-08-904/26/23 15:21362 127 1
Benzoic Acid ND ug/kg 04/27/23 12:23 65-85-004/26/23 15:211810 777 1
Benzyl alcohol ND ug/kg 04/27/23 12:23 100-51-604/26/23 15:21723 274 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 12:23 101-55-304/26/23 15:21362 139 1
Butylbenzylphthalate ND ug/kg 04/27/23 12:23 85-68-704/26/23 15:21362 152 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 12:23 59-50-704/26/23 15:21723 254 1
4-Chloroaniline ND ug/kg 04/27/23 12:23 106-47-804/26/23 15:21723 284 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 12:23 111-91-104/26/23 15:21362 150 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 12:23 111-44-404/26/23 15:21362 136 1
2-Chloronaphthalene ND ug/kg 04/27/23 12:23 91-58-704/26/23 15:21362 144 1
2-Chlorophenol ND ug/kg 04/27/23 12:23 95-57-804/26/23 15:21362 136 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 12:23 7005-72-304/26/23 15:21362 135 1
Chrysene ND ug/kg 04/27/23 12:23 218-01-904/26/23 15:21362 131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-1 Lab ID: 92663594001 Collected: 04/18/23 16:15 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenz(a,h)anthracene ND ug/kg 04/27/23 12:23 53-70-304/26/23 15:21362 139 1
Dibenzofuran ND ug/kg 04/27/23 12:23 132-64-904/26/23 15:21362 130 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 12:23 95-50-104/26/23 15:21362 130 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 12:23 541-73-104/26/23 15:21362 128 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 12:23 106-46-704/26/23 15:21362 138 1
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 12:23 91-94-104/26/23 15:21723 244 1
2,4-Dichlorophenol ND ug/kg 04/27/23 12:23 120-83-204/26/23 15:21362 141 1
Diethylphthalate ND ug/kg 04/27/23 12:23 84-66-204/26/23 15:21362 133 1
2,4-Dimethylphenol ND ug/kg 04/27/23 12:23 105-67-904/26/23 15:21362 150 1
Dimethylphthalate ND ug/kg 04/27/23 12:23 131-11-304/26/23 15:21362 131 1
Di-n-butylphthalate ND ug/kg 04/27/23 12:23 84-74-204/26/23 15:21362 122 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 12:23 534-52-104/26/23 15:21723 337 1
2,4-Dinitrophenol ND ug/kg 04/27/23 12:23 51-28-504/26/23 15:211810 1120 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 12:23 121-14-204/26/23 15:21362 139 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 12:23 606-20-204/26/23 15:21362 133 1
Di-n-octylphthalate ND ug/kg 04/27/23 12:23 117-84-004/26/23 15:21362 142 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 12:23 117-81-704/26/23 15:21362 140 1
Fluoranthene ND ug/kg 04/27/23 12:23 206-44-004/26/23 15:21362 124 1
Fluorene ND ug/kg 04/27/23 12:23 86-73-704/26/23 15:21362 127 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 12:23 87-68-304/26/23 15:21362 157 1
Hexachlorobenzene ND ug/kg 04/27/23 12:23 118-74-104/26/23 15:21362 141 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 12:23 77-47-404/26/23 15:21362 207 1
Hexachloroethane ND ug/kg 04/27/23 12:23 67-72-104/26/23 15:21362 138 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 12:23 193-39-504/26/23 15:21362 142 1
Isophorone ND ug/kg 04/27/23 12:23 78-59-104/26/23 15:21362 161 1
1-Methylnaphthalene ND ug/kg 04/27/23 12:23 90-12-004/26/23 15:21362 127 1
2-Methylnaphthalene ND ug/kg 04/27/23 12:23 91-57-604/26/23 15:21362 145 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 12:23 95-48-704/26/23 15:21362 148 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 12:23 15831-10-404/26/23 15:21362 146 1
Naphthalene ND ug/kg 04/27/23 12:23 91-20-304/26/23 15:21362 123 1
2-Nitroaniline ND ug/kg 04/27/23 12:23 88-74-404/26/23 15:211810 296 1
3-Nitroaniline ND ug/kg 04/27/23 12:23 99-09-204/26/23 15:211810 284 1
4-Nitroaniline ND ug/kg 04/27/23 12:23 100-01-604/26/23 15:21723 275 1
Nitrobenzene ND ug/kg 04/27/23 12:23 98-95-304/26/23 15:21362 168 1
2-Nitrophenol ND ug/kg 04/27/23 12:23 88-75-504/26/23 15:21362 157 1
4-Nitrophenol ND ug/kg 04/27/23 12:23 100-02-704/26/23 15:211810 699 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 12:23 62-75-904/26/23 15:21362 122 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 12:23 621-64-704/26/23 15:21362 136 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 12:23 86-30-604/26/23 15:21362 128 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 12:23 108-60-104/26/23 15:21362 172 1
Pentachlorophenol ND ug/kg 04/27/23 12:23 87-86-504/26/23 15:21723 354 1
Phenanthrene ND ug/kg 04/27/23 12:23 85-01-804/26/23 15:21362 118 1
Phenol ND ug/kg 04/27/23 12:23 108-95-204/26/23 15:21362 161 1
Pyrene ND ug/kg 04/27/23 12:23 129-00-004/26/23 15:21362 147 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-1 Lab ID: 92663594001 Collected: 04/18/23 16:15 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Pyridine ND ug/kg 04/27/23 12:23 110-86-104/26/23 15:21362 114 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 12:23 120-82-104/26/23 15:21362 142 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 12:23 95-95-404/26/23 15:21362 165 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 12:23 88-06-204/26/23 15:21362 149 1
Surrogates
Nitrobenzene-d5 (S)46 %04/27/23 12:23 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)50 %04/27/23 12:23 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)63 %04/27/23 12:23 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)44 %04/27/23 12:23 13127-88-304/26/23 15:2110-130 1
2-Fluorophenol (S)44 %04/27/23 12:23 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)55 %04/27/23 12:23 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 18:53 67-64-104/25/23 14:47216 69.2 1
Benzene ND ug/kg 04/25/23 18:53 71-43-204/25/23 14:4710.8 4.3 1
Bromobenzene ND ug/kg 04/25/23 18:53 108-86-104/25/23 14:4710.8 3.5 1
Bromochloromethane ND ug/kg 04/25/23 18:53 74-97-504/25/23 14:4710.8 3.2 1
Bromodichloromethane ND ug/kg 04/25/23 18:53 75-27-404/25/23 14:4710.8 4.2 1
Bromoform ND ug/kg 04/25/23 18:53 75-25-204/25/23 14:4710.8 3.8 1
Bromomethane ND ug/kg 04/25/23 18:53 74-83-9 IK04/25/23 14:4743.1 33.4 1
2-Butanone (MEK)ND ug/kg 04/25/23 18:53 78-93-304/25/23 14:47216 51.7 1
n-Butylbenzene ND ug/kg 04/25/23 18:53 104-51-804/25/23 14:4710.8 6.8 1
sec-Butylbenzene ND ug/kg 04/25/23 18:53 135-98-804/25/23 14:4710.8 4.7 1
tert-Butylbenzene ND ug/kg 04/25/23 18:53 98-06-604/25/23 14:4710.8 3.8 1
Carbon tetrachloride ND ug/kg 04/25/23 18:53 56-23-504/25/23 14:4710.8 4.0 1
Chlorobenzene ND ug/kg 04/25/23 18:53 108-90-704/25/23 14:4710.8 6.2 1
Chloroethane ND ug/kg 04/25/23 18:53 75-00-304/25/23 14:4721.6 8.3 1
Chloroform ND ug/kg 04/25/23 18:53 67-66-304/25/23 14:4710.8 9.0 1
Chloromethane ND ug/kg 04/25/23 18:53 74-87-304/25/23 14:4721.6 9.1 1
2-Chlorotoluene ND ug/kg 04/25/23 18:53 95-49-804/25/23 14:4710.8 3.8 1
4-Chlorotoluene ND ug/kg 04/25/23 18:53 106-43-404/25/23 14:4710.8 6.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 18:53 96-12-804/25/23 14:4710.8 4.2 1
Dibromochloromethane ND ug/kg 04/25/23 18:53 124-48-104/25/23 14:4710.8 6.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 18:53 106-93-404/25/23 14:4710.8 4.7 1
Dibromomethane ND ug/kg 04/25/23 18:53 74-95-304/25/23 14:4710.8 2.3 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 18:53 95-50-104/25/23 14:4710.8 3.9 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 18:53 541-73-104/25/23 14:4710.8 3.3 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 18:53 106-46-704/25/23 14:4710.8 2.8 1
Dichlorodifluoromethane ND ug/kg 04/25/23 18:53 75-71-804/25/23 14:4721.6 11.0 1
1,1-Dichloroethane ND ug/kg 04/25/23 18:53 75-34-304/25/23 14:4710.8 4.4 1
1,2-Dichloroethane ND ug/kg 04/25/23 18:53 107-06-204/25/23 14:4710.8 7.1 1
1,1-Dichloroethene ND ug/kg 04/25/23 18:53 75-35-404/25/23 14:4710.8 4.4 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 18:53 156-59-204/25/23 14:4710.8 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-1 Lab ID: 92663594001 Collected: 04/18/23 16:15 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
trans-1,2-Dichloroethene ND ug/kg 04/25/23 18:53 156-60-504/25/23 14:4710.8 9.2 1
1,2-Dichloropropane ND ug/kg 04/25/23 18:53 78-87-504/25/23 14:4710.8 3.2 1
1,3-Dichloropropane ND ug/kg 04/25/23 18:53 142-28-904/25/23 14:4710.8 3.4 1
2,2-Dichloropropane ND ug/kg 04/25/23 18:53 594-20-7 v204/25/23 14:4710.8 8.2 1
1,1-Dichloropropene ND ug/kg 04/25/23 18:53 563-58-604/25/23 14:4710.8 5.2 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 18:53 10061-01-504/25/23 14:4710.8 2.9 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 18:53 10061-02-604/25/23 14:4710.8 3.7 1
Diisopropyl ether ND ug/kg 04/25/23 18:53 108-20-304/25/23 14:4710.8 2.9 1
Ethylbenzene ND ug/kg 04/25/23 18:53 100-41-404/25/23 14:4710.8 5.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 18:53 87-68-304/25/23 14:4721.6 17.6 1
2-Hexanone ND ug/kg 04/25/23 18:53 591-78-604/25/23 14:47108 10.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 18:53 98-82-804/25/23 14:4710.8 3.7 1
p-Isopropyltoluene ND ug/kg 04/25/23 18:53 99-87-604/25/23 14:4710.8 5.3 1
Methylene Chloride 48.0 ug/kg 04/25/23 18:53 75-09-2 C904/25/23 14:4743.1 29.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 18:53 108-10-104/25/23 14:47108 10.4 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 18:53 1634-04-4 v204/25/23 14:4710.8 4.0 1
Naphthalene 7.2J ug/kg 04/25/23 18:53 91-20-3 C804/25/23 14:4710.8 5.7 1
n-Propylbenzene ND ug/kg 04/25/23 18:53 103-65-104/25/23 14:4710.8 3.8 1
Styrene ND ug/kg 04/25/23 18:53 100-42-504/25/23 14:4710.8 2.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 18:53 630-20-604/25/23 14:4710.8 4.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 18:53 79-34-504/25/23 14:4710.8 2.8 1
Tetrachloroethene ND ug/kg 04/25/23 18:53 127-18-404/25/23 14:4710.8 3.4 1
Toluene ND ug/kg 04/25/23 18:53 108-88-304/25/23 14:4710.8 7.4 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 18:53 87-61-604/25/23 14:4710.8 8.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 18:53 120-82-104/25/23 14:4710.8 9.1 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 18:53 71-55-604/25/23 14:4710.8 5.6 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 18:53 79-00-504/25/23 14:4710.8 3.6 1
Trichloroethene ND ug/kg 04/25/23 18:53 79-01-604/25/23 14:4710.8 8.7 1
Trichlorofluoromethane ND ug/kg 04/25/23 18:53 75-69-404/25/23 14:4710.8 5.9 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 18:53 96-18-404/25/23 14:4710.8 5.5 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 18:53 95-63-604/25/23 14:4710.8 6.4 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 18:53 108-67-804/25/23 14:4710.8 3.6 1
Vinyl acetate ND ug/kg 04/25/23 18:53 108-05-404/25/23 14:47108 22.2 1
Vinyl chloride ND ug/kg 04/25/23 18:53 75-01-4 v204/25/23 14:4721.6 5.5 1
Xylene (Total)ND ug/kg 04/25/23 18:53 1330-20-704/25/23 14:4721.6 6.1 1
m&p-Xylene ND ug/kg 04/25/23 18:53 179601-23-104/25/23 14:4721.6 7.4 1
o-Xylene ND ug/kg 04/25/23 18:53 95-47-604/25/23 14:4710.8 4.8 1
Surrogates
Toluene-d8 (S)99 %04/25/23 18:53 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 18:53 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)96 %04/25/23 18:53 17060-07-004/25/23 14:4770-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-1 Lab ID: 92663594001 Collected: 04/18/23 16:15 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 9.6 %04/21/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 89.2 %04/27/23 16:5904/27/23 16:441
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.09 mg/kg 05/01/23 13:37 18540-29-904/30/23 06:541.12 0.286 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.16J mg/kg 04/27/23 19:10 57-12-5 R104/26/23 17:140.32 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-2 Lab ID: 92663594002 Collected: 04/19/23 14:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.2 mg/kg 04/27/23 15:46 7440-38-204/26/23 11:040.57 0.16 1
Barium 93.5 mg/kg 04/27/23 15:46 7440-39-304/26/23 11:040.34 0.086 1
Cadmium 0.049J mg/kg 04/27/23 15:46 7440-43-904/26/23 11:040.092 0.034 1
Chromium 76.9 mg/kg 04/27/23 15:46 7440-47-304/26/23 11:042.3 0.44 1
Lead 20.9 mg/kg 04/27/23 15:46 7439-92-104/26/23 11:040.57 0.11 1
Selenium 0.36J mg/kg 04/27/23 15:46 7782-49-204/26/23 11:040.57 0.12 1
Silver ND mg/kg 04/27/23 15:46 7440-22-404/26/23 11:040.57 0.23 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.019J mg/kg 04/28/23 09:02 7439-97-604/26/23 11:070.023 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 12:51 83-32-904/26/23 15:21396 139 1
Acenaphthylene ND ug/kg 04/27/23 12:51 208-96-804/26/23 15:21396 139 1
Aniline ND ug/kg 04/27/23 12:51 62-53-304/26/23 15:21396 155 1
Anthracene ND ug/kg 04/27/23 12:51 120-12-704/26/23 15:21396 130 1
Benzo(a)anthracene ND ug/kg 04/27/23 12:51 56-55-304/26/23 15:21396 132 1
Benzo(a)pyrene ND ug/kg 04/27/23 12:51 50-32-804/26/23 15:21396 137 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 12:51 205-99-204/26/23 15:21396 132 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 12:51 191-24-204/26/23 15:21396 154 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 12:51 207-08-904/26/23 15:21396 139 1
Benzoic Acid ND ug/kg 04/27/23 12:51 65-85-004/26/23 15:211980 852 1
Benzyl alcohol ND ug/kg 04/27/23 12:51 100-51-604/26/23 15:21793 300 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 12:51 101-55-304/26/23 15:21396 153 1
Butylbenzylphthalate ND ug/kg 04/27/23 12:51 85-68-704/26/23 15:21396 167 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 12:51 59-50-704/26/23 15:21793 279 1
4-Chloroaniline ND ug/kg 04/27/23 12:51 106-47-804/26/23 15:21793 311 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 12:51 111-91-104/26/23 15:21396 165 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 12:51 111-44-404/26/23 15:21396 149 1
2-Chloronaphthalene ND ug/kg 04/27/23 12:51 91-58-704/26/23 15:21396 157 1
2-Chlorophenol ND ug/kg 04/27/23 12:51 95-57-804/26/23 15:21396 149 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 12:51 7005-72-304/26/23 15:21396 148 1
Chrysene ND ug/kg 04/27/23 12:51 218-01-904/26/23 15:21396 144 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 12:51 53-70-304/26/23 15:21396 153 1
Dibenzofuran ND ug/kg 04/27/23 12:51 132-64-904/26/23 15:21396 143 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 12:51 95-50-104/26/23 15:21396 143 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 12:51 541-73-104/26/23 15:21396 141 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 12:51 106-46-704/26/23 15:21396 151 1
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 12:51 91-94-104/26/23 15:21793 268 1
2,4-Dichlorophenol ND ug/kg 04/27/23 12:51 120-83-204/26/23 15:21396 155 1
Diethylphthalate ND ug/kg 04/27/23 12:51 84-66-204/26/23 15:21396 145 1
2,4-Dimethylphenol ND ug/kg 04/27/23 12:51 105-67-904/26/23 15:21396 165 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-2 Lab ID: 92663594002 Collected: 04/19/23 14:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/23 12:51 131-11-304/26/23 15:21396 144 1
Di-n-butylphthalate ND ug/kg 04/27/23 12:51 84-74-204/26/23 15:21396 133 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 12:51 534-52-104/26/23 15:21793 370 1
2,4-Dinitrophenol ND ug/kg 04/27/23 12:51 51-28-504/26/23 15:211980 1230 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 12:51 121-14-204/26/23 15:21396 153 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 12:51 606-20-204/26/23 15:21396 145 1
Di-n-octylphthalate ND ug/kg 04/27/23 12:51 117-84-004/26/23 15:21396 156 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 12:51 117-81-704/26/23 15:21396 154 1
Fluoranthene ND ug/kg 04/27/23 12:51 206-44-004/26/23 15:21396 136 1
Fluorene ND ug/kg 04/27/23 12:51 86-73-704/26/23 15:21396 139 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 12:51 87-68-304/26/23 15:21396 172 1
Hexachlorobenzene ND ug/kg 04/27/23 12:51 118-74-104/26/23 15:21396 155 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 12:51 77-47-404/26/23 15:21396 227 1
Hexachloroethane ND ug/kg 04/27/23 12:51 67-72-104/26/23 15:21396 151 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 12:51 193-39-504/26/23 15:21396 156 1
Isophorone ND ug/kg 04/27/23 12:51 78-59-104/26/23 15:21396 177 1
1-Methylnaphthalene ND ug/kg 04/27/23 12:51 90-12-004/26/23 15:21396 139 1
2-Methylnaphthalene ND ug/kg 04/27/23 12:51 91-57-604/26/23 15:21396 159 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 12:51 95-48-704/26/23 15:21396 162 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 12:51 15831-10-404/26/23 15:21396 160 1
Naphthalene ND ug/kg 04/27/23 12:51 91-20-304/26/23 15:21396 135 1
2-Nitroaniline ND ug/kg 04/27/23 12:51 88-74-404/26/23 15:211980 324 1
3-Nitroaniline ND ug/kg 04/27/23 12:51 99-09-204/26/23 15:211980 311 1
4-Nitroaniline ND ug/kg 04/27/23 12:51 100-01-604/26/23 15:21793 302 1
Nitrobenzene ND ug/kg 04/27/23 12:51 98-95-304/26/23 15:21396 184 1
2-Nitrophenol ND ug/kg 04/27/23 12:51 88-75-504/26/23 15:21396 172 1
4-Nitrophenol ND ug/kg 04/27/23 12:51 100-02-704/26/23 15:211980 766 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 12:51 62-75-904/26/23 15:21396 133 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 12:51 621-64-704/26/23 15:21396 149 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 12:51 86-30-604/26/23 15:21396 141 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 12:51 108-60-104/26/23 15:21396 189 1
Pentachlorophenol ND ug/kg 04/27/23 12:51 87-86-504/26/23 15:21793 388 1
Phenanthrene ND ug/kg 04/27/23 12:51 85-01-804/26/23 15:21396 130 1
Phenol ND ug/kg 04/27/23 12:51 108-95-204/26/23 15:21396 177 1
Pyrene ND ug/kg 04/27/23 12:51 129-00-004/26/23 15:21396 161 1
Pyridine ND ug/kg 04/27/23 12:51 110-86-104/26/23 15:21396 125 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 12:51 120-82-104/26/23 15:21396 156 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 12:51 95-95-404/26/23 15:21396 181 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 12:51 88-06-204/26/23 15:21396 163 1
Surrogates
Nitrobenzene-d5 (S)61 %04/27/23 12:51 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)60 %04/27/23 12:51 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)80 %04/27/23 12:51 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)58 %04/27/23 12:51 13127-88-304/26/23 15:2110-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-2 Lab ID: 92663594002 Collected: 04/19/23 14:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)58 %04/27/23 12:51 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)70 %04/27/23 12:51 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 19:12 67-64-104/25/23 14:47203 65.1 1
Benzene ND ug/kg 04/25/23 19:12 71-43-204/25/23 14:4710.1 4.0 1
Bromobenzene ND ug/kg 04/25/23 19:12 108-86-104/25/23 14:4710.1 3.3 1
Bromochloromethane ND ug/kg 04/25/23 19:12 74-97-504/25/23 14:4710.1 3.0 1
Bromodichloromethane ND ug/kg 04/25/23 19:12 75-27-404/25/23 14:4710.1 3.9 1
Bromoform ND ug/kg 04/25/23 19:12 75-25-204/25/23 14:4710.1 3.6 1
Bromomethane ND ug/kg 04/25/23 19:12 74-83-9 IK04/25/23 14:4740.6 31.4 1
2-Butanone (MEK)ND ug/kg 04/25/23 19:12 78-93-304/25/23 14:47203 48.7 1
n-Butylbenzene ND ug/kg 04/25/23 19:12 104-51-804/25/23 14:4710.1 6.4 1
sec-Butylbenzene ND ug/kg 04/25/23 19:12 135-98-804/25/23 14:4710.1 4.5 1
tert-Butylbenzene ND ug/kg 04/25/23 19:12 98-06-604/25/23 14:4710.1 3.6 1
Carbon tetrachloride ND ug/kg 04/25/23 19:12 56-23-504/25/23 14:4710.1 3.8 1
Chlorobenzene ND ug/kg 04/25/23 19:12 108-90-704/25/23 14:4710.1 5.8 1
Chloroethane ND ug/kg 04/25/23 19:12 75-00-304/25/23 14:4720.3 7.8 1
Chloroform ND ug/kg 04/25/23 19:12 67-66-304/25/23 14:4710.1 8.5 1
Chloromethane ND ug/kg 04/25/23 19:12 74-87-304/25/23 14:4720.3 8.5 1
2-Chlorotoluene ND ug/kg 04/25/23 19:12 95-49-804/25/23 14:4710.1 3.6 1
4-Chlorotoluene ND ug/kg 04/25/23 19:12 106-43-404/25/23 14:4710.1 5.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 19:12 96-12-804/25/23 14:4710.1 3.9 1
Dibromochloromethane ND ug/kg 04/25/23 19:12 124-48-104/25/23 14:4710.1 5.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 19:12 106-93-404/25/23 14:4710.1 4.5 1
Dibromomethane ND ug/kg 04/25/23 19:12 74-95-304/25/23 14:4710.1 2.2 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 19:12 95-50-104/25/23 14:4710.1 3.7 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 19:12 541-73-104/25/23 14:4710.1 3.1 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 19:12 106-46-704/25/23 14:4710.1 2.6 1
Dichlorodifluoromethane ND ug/kg 04/25/23 19:12 75-71-804/25/23 14:4720.3 10.3 1
1,1-Dichloroethane ND ug/kg 04/25/23 19:12 75-34-304/25/23 14:4710.1 4.2 1
1,2-Dichloroethane ND ug/kg 04/25/23 19:12 107-06-204/25/23 14:4710.1 6.7 1
1,1-Dichloroethene ND ug/kg 04/25/23 19:12 75-35-404/25/23 14:4710.1 4.2 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 19:12 156-59-204/25/23 14:4710.1 3.5 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 19:12 156-60-504/25/23 14:4710.1 8.6 1
1,2-Dichloropropane ND ug/kg 04/25/23 19:12 78-87-504/25/23 14:4710.1 3.0 1
1,3-Dichloropropane ND ug/kg 04/25/23 19:12 142-28-904/25/23 14:4710.1 3.2 1
2,2-Dichloropropane ND ug/kg 04/25/23 19:12 594-20-7 v204/25/23 14:4710.1 7.7 1
1,1-Dichloropropene ND ug/kg 04/25/23 19:12 563-58-604/25/23 14:4710.1 4.9 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 19:12 10061-01-504/25/23 14:4710.1 2.8 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 19:12 10061-02-604/25/23 14:4710.1 3.5 1
Diisopropyl ether ND ug/kg 04/25/23 19:12 108-20-304/25/23 14:4710.1 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-2 Lab ID: 92663594002 Collected: 04/19/23 14:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/25/23 19:12 100-41-404/25/23 14:4710.1 4.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 19:12 87-68-304/25/23 14:4720.3 16.6 1
2-Hexanone ND ug/kg 04/25/23 19:12 591-78-604/25/23 14:47101 9.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 19:12 98-82-804/25/23 14:4710.1 3.4 1
p-Isopropyltoluene ND ug/kg 04/25/23 19:12 99-87-604/25/23 14:4710.1 5.0 1
Methylene Chloride 64.8 ug/kg 04/25/23 19:12 75-09-2 C904/25/23 14:4740.6 27.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 19:12 108-10-104/25/23 14:47101 9.8 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 19:12 1634-04-4 v204/25/23 14:4710.1 3.8 1
Naphthalene 7.0J ug/kg 04/25/23 19:12 91-20-3 C804/25/23 14:4710.1 5.3 1
n-Propylbenzene ND ug/kg 04/25/23 19:12 103-65-104/25/23 14:4710.1 3.6 1
Styrene ND ug/kg 04/25/23 19:12 100-42-504/25/23 14:4710.1 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 19:12 630-20-604/25/23 14:4710.1 3.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 19:12 79-34-504/25/23 14:4710.1 2.7 1
Tetrachloroethene ND ug/kg 04/25/23 19:12 127-18-404/25/23 14:4710.1 3.2 1
Toluene ND ug/kg 04/25/23 19:12 108-88-304/25/23 14:4710.1 7.0 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 19:12 87-61-604/25/23 14:4710.1 8.2 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 19:12 120-82-104/25/23 14:4710.1 8.5 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 19:12 71-55-604/25/23 14:4710.1 5.3 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 19:12 79-00-504/25/23 14:4710.1 3.4 1
Trichloroethene ND ug/kg 04/25/23 19:12 79-01-604/25/23 14:4710.1 8.2 1
Trichlorofluoromethane ND ug/kg 04/25/23 19:12 75-69-404/25/23 14:4710.1 5.6 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 19:12 96-18-404/25/23 14:4710.1 5.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 19:12 95-63-604/25/23 14:4710.1 6.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 19:12 108-67-804/25/23 14:4710.1 3.4 1
Vinyl acetate ND ug/kg 04/25/23 19:12 108-05-404/25/23 14:47101 20.9 1
Vinyl chloride ND ug/kg 04/25/23 19:12 75-01-4 v204/25/23 14:4720.3 5.2 1
Xylene (Total)ND ug/kg 04/25/23 19:12 1330-20-704/25/23 14:4720.3 5.8 1
m&p-Xylene ND ug/kg 04/25/23 19:12 179601-23-104/25/23 14:4720.3 6.9 1
o-Xylene ND ug/kg 04/25/23 19:12 95-47-604/25/23 14:4710.1 4.5 1
Surrogates
Toluene-d8 (S)100 %04/25/23 19:12 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)99 %04/25/23 19:12 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)97 %04/25/23 19:12 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.5 %04/21/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.0 %04/27/23 16:5904/27/23 16:441
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-2 Lab ID: 92663594002 Collected: 04/19/23 14:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/01/23 13:43 18540-29-904/30/23 06:541.23 0.315 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-3 Lab ID: 92663594003 Collected: 04/19/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.9 mg/kg 04/27/23 15:49 7440-38-204/26/23 11:040.57 0.16 1
Barium 118 mg/kg 04/27/23 15:49 7440-39-304/26/23 11:040.34 0.085 1
Cadmium 0.067J mg/kg 04/27/23 15:49 7440-43-904/26/23 11:040.091 0.033 1
Chromium 60.1 mg/kg 04/27/23 15:49 7440-47-304/26/23 11:042.3 0.44 1
Lead 12.1 mg/kg 04/27/23 15:49 7439-92-104/26/23 11:040.57 0.11 1
Selenium 0.16J mg/kg 04/27/23 15:49 7782-49-204/26/23 11:040.57 0.12 1
Silver 2.9 mg/kg 04/27/23 15:49 7440-22-404/26/23 11:040.57 0.23 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury ND mg/kg 04/28/23 09:04 7439-97-604/26/23 11:070.021 0.0093 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 14:13 83-32-904/26/23 15:21407 143 1
Acenaphthylene ND ug/kg 04/27/23 14:13 208-96-804/26/23 15:21407 143 1
Aniline ND ug/kg 04/27/23 14:13 62-53-304/26/23 15:21407 159 1
Anthracene ND ug/kg 04/27/23 14:13 120-12-704/26/23 15:21407 133 1
Benzo(a)anthracene ND ug/kg 04/27/23 14:13 56-55-304/26/23 15:21407 136 1
Benzo(a)pyrene ND ug/kg 04/27/23 14:13 50-32-804/26/23 15:21407 141 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 14:13 205-99-204/26/23 15:21407 136 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 14:13 191-24-204/26/23 15:21407 158 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 14:13 207-08-904/26/23 15:21407 143 1
Benzoic Acid ND ug/kg 04/27/23 14:13 65-85-004/26/23 15:212030 874 1
Benzyl alcohol ND ug/kg 04/27/23 14:13 100-51-604/26/23 15:21814 308 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 14:13 101-55-304/26/23 15:21407 157 1
Butylbenzylphthalate ND ug/kg 04/27/23 14:13 85-68-704/26/23 15:21407 171 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 14:13 59-50-704/26/23 15:21814 286 1
4-Chloroaniline ND ug/kg 04/27/23 14:13 106-47-804/26/23 15:21814 319 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 14:13 111-91-104/26/23 15:21407 169 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 14:13 111-44-404/26/23 15:21407 153 1
2-Chloronaphthalene ND ug/kg 04/27/23 14:13 91-58-704/26/23 15:21407 162 1
2-Chlorophenol ND ug/kg 04/27/23 14:13 95-57-804/26/23 15:21407 153 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 14:13 7005-72-304/26/23 15:21407 152 1
Chrysene ND ug/kg 04/27/23 14:13 218-01-904/26/23 15:21407 148 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 14:13 53-70-304/26/23 15:21407 157 1
Dibenzofuran ND ug/kg 04/27/23 14:13 132-64-904/26/23 15:21407 147 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 14:13 95-50-104/26/23 15:21407 147 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 14:13 541-73-104/26/23 15:21407 144 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 14:13 106-46-704/26/23 15:21407 155 1
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 14:13 91-94-104/26/23 15:21814 275 1
2,4-Dichlorophenol ND ug/kg 04/27/23 14:13 120-83-204/26/23 15:21407 159 1
Diethylphthalate ND ug/kg 04/27/23 14:13 84-66-204/26/23 15:21407 149 1
2,4-Dimethylphenol ND ug/kg 04/27/23 14:13 105-67-904/26/23 15:21407 169 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-3 Lab ID: 92663594003 Collected: 04/19/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/23 14:13 131-11-304/26/23 15:21407 148 1
Di-n-butylphthalate ND ug/kg 04/27/23 14:13 84-74-204/26/23 15:21407 137 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 14:13 534-52-104/26/23 15:21814 380 1
2,4-Dinitrophenol ND ug/kg 04/27/23 14:13 51-28-504/26/23 15:212030 1260 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 14:13 121-14-204/26/23 15:21407 157 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 14:13 606-20-204/26/23 15:21407 149 1
Di-n-octylphthalate ND ug/kg 04/27/23 14:13 117-84-004/26/23 15:21407 160 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 14:13 117-81-704/26/23 15:21407 158 1
Fluoranthene ND ug/kg 04/27/23 14:13 206-44-004/26/23 15:21407 139 1
Fluorene ND ug/kg 04/27/23 14:13 86-73-704/26/23 15:21407 143 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 14:13 87-68-304/26/23 15:21407 176 1
Hexachlorobenzene ND ug/kg 04/27/23 14:13 118-74-104/26/23 15:21407 159 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 14:13 77-47-404/26/23 15:21407 233 1
Hexachloroethane ND ug/kg 04/27/23 14:13 67-72-104/26/23 15:21407 155 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 14:13 193-39-504/26/23 15:21407 160 1
Isophorone ND ug/kg 04/27/23 14:13 78-59-104/26/23 15:21407 181 1
1-Methylnaphthalene ND ug/kg 04/27/23 14:13 90-12-004/26/23 15:21407 143 1
2-Methylnaphthalene ND ug/kg 04/27/23 14:13 91-57-604/26/23 15:21407 163 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 14:13 95-48-704/26/23 15:21407 166 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 14:13 15831-10-404/26/23 15:21407 164 1
Naphthalene ND ug/kg 04/27/23 14:13 91-20-304/26/23 15:21407 138 1
2-Nitroaniline ND ug/kg 04/27/23 14:13 88-74-404/26/23 15:212030 333 1
3-Nitroaniline ND ug/kg 04/27/23 14:13 99-09-204/26/23 15:212030 319 1
4-Nitroaniline ND ug/kg 04/27/23 14:13 100-01-604/26/23 15:21814 309 1
Nitrobenzene ND ug/kg 04/27/23 14:13 98-95-304/26/23 15:21407 189 1
2-Nitrophenol ND ug/kg 04/27/23 14:13 88-75-504/26/23 15:21407 176 1
4-Nitrophenol ND ug/kg 04/27/23 14:13 100-02-704/26/23 15:212030 787 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 14:13 62-75-904/26/23 15:21407 137 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 14:13 621-64-704/26/23 15:21407 153 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 14:13 86-30-604/26/23 15:21407 144 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 14:13 108-60-104/26/23 15:21407 194 1
Pentachlorophenol ND ug/kg 04/27/23 14:13 87-86-504/26/23 15:21814 398 1
Phenanthrene ND ug/kg 04/27/23 14:13 85-01-804/26/23 15:21407 133 1
Phenol ND ug/kg 04/27/23 14:13 108-95-204/26/23 15:21407 181 1
Pyrene ND ug/kg 04/27/23 14:13 129-00-004/26/23 15:21407 165 1
Pyridine ND ug/kg 04/27/23 14:13 110-86-104/26/23 15:21407 128 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 14:13 120-82-104/26/23 15:21407 160 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 14:13 95-95-404/26/23 15:21407 186 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 14:13 88-06-204/26/23 15:21407 168 1
Surrogates
Nitrobenzene-d5 (S)53 %04/27/23 14:13 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)45 %04/27/23 14:13 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)59 %04/27/23 14:13 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)49 %04/27/23 14:13 13127-88-304/26/23 15:2110-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-3 Lab ID: 92663594003 Collected: 04/19/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)45 %04/27/23 14:13 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)53 %04/27/23 14:13 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 19:30 67-64-104/25/23 14:47200 64.4 1
Benzene ND ug/kg 04/25/23 19:30 71-43-204/25/23 14:4710.0 4.0 1
Bromobenzene ND ug/kg 04/25/23 19:30 108-86-104/25/23 14:4710.0 3.3 1
Bromochloromethane ND ug/kg 04/25/23 19:30 74-97-504/25/23 14:4710.0 3.0 1
Bromodichloromethane ND ug/kg 04/25/23 19:30 75-27-404/25/23 14:4710.0 3.9 1
Bromoform ND ug/kg 04/25/23 19:30 75-25-204/25/23 14:4710.0 3.5 1
Bromomethane ND ug/kg 04/25/23 19:30 74-83-9 IK04/25/23 14:4740.1 31.1 1
2-Butanone (MEK)ND ug/kg 04/25/23 19:30 78-93-304/25/23 14:47200 48.1 1
n-Butylbenzene ND ug/kg 04/25/23 19:30 104-51-804/25/23 14:4710.0 6.3 1
sec-Butylbenzene ND ug/kg 04/25/23 19:30 135-98-804/25/23 14:4710.0 4.4 1
tert-Butylbenzene ND ug/kg 04/25/23 19:30 98-06-604/25/23 14:4710.0 3.6 1
Carbon tetrachloride ND ug/kg 04/25/23 19:30 56-23-504/25/23 14:4710.0 3.7 1
Chlorobenzene ND ug/kg 04/25/23 19:30 108-90-704/25/23 14:4710.0 5.8 1
Chloroethane ND ug/kg 04/25/23 19:30 75-00-304/25/23 14:4720.0 7.7 1
Chloroform ND ug/kg 04/25/23 19:30 67-66-304/25/23 14:4710.0 8.4 1
Chloromethane ND ug/kg 04/25/23 19:30 74-87-304/25/23 14:4720.0 8.4 1
2-Chlorotoluene ND ug/kg 04/25/23 19:30 95-49-804/25/23 14:4710.0 3.5 1
4-Chlorotoluene ND ug/kg 04/25/23 19:30 106-43-404/25/23 14:4710.0 5.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 19:30 96-12-804/25/23 14:4710.0 3.9 1
Dibromochloromethane ND ug/kg 04/25/23 19:30 124-48-104/25/23 14:4710.0 5.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 19:30 106-93-404/25/23 14:4710.0 4.4 1
Dibromomethane ND ug/kg 04/25/23 19:30 74-95-304/25/23 14:4710.0 2.1 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 19:30 95-50-104/25/23 14:4710.0 3.6 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 19:30 541-73-104/25/23 14:4710.0 3.1 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 19:30 106-46-704/25/23 14:4710.0 2.6 1
Dichlorodifluoromethane ND ug/kg 04/25/23 19:30 75-71-804/25/23 14:4720.0 10.2 1
1,1-Dichloroethane ND ug/kg 04/25/23 19:30 75-34-304/25/23 14:4710.0 4.1 1
1,2-Dichloroethane ND ug/kg 04/25/23 19:30 107-06-204/25/23 14:4710.0 6.6 1
1,1-Dichloroethene ND ug/kg 04/25/23 19:30 75-35-404/25/23 14:4710.0 4.1 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 19:30 156-59-204/25/23 14:4710.0 3.4 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 19:30 156-60-504/25/23 14:4710.0 8.5 1
1,2-Dichloropropane ND ug/kg 04/25/23 19:30 78-87-504/25/23 14:4710.0 3.0 1
1,3-Dichloropropane ND ug/kg 04/25/23 19:30 142-28-904/25/23 14:4710.0 3.1 1
2,2-Dichloropropane ND ug/kg 04/25/23 19:30 594-20-7 v204/25/23 14:4710.0 7.6 1
1,1-Dichloropropene ND ug/kg 04/25/23 19:30 563-58-604/25/23 14:4710.0 4.8 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 19:30 10061-01-504/25/23 14:4710.0 2.7 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 19:30 10061-02-604/25/23 14:4710.0 3.4 1
Diisopropyl ether ND ug/kg 04/25/23 19:30 108-20-304/25/23 14:4710.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-3 Lab ID: 92663594003 Collected: 04/19/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/25/23 19:30 100-41-404/25/23 14:4710.0 4.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 19:30 87-68-304/25/23 14:4720.0 16.4 1
2-Hexanone ND ug/kg 04/25/23 19:30 591-78-604/25/23 14:47100 9.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 19:30 98-82-804/25/23 14:4710.0 3.4 1
p-Isopropyltoluene ND ug/kg 04/25/23 19:30 99-87-604/25/23 14:4710.0 4.9 1
Methylene Chloride 53.4 ug/kg 04/25/23 19:30 75-09-2 C904/25/23 14:4740.1 27.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 19:30 108-10-104/25/23 14:47100 9.7 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 19:30 1634-04-4 v204/25/23 14:4710.0 3.7 1
Naphthalene ND ug/kg 04/25/23 19:30 91-20-304/25/23 14:4710.0 5.3 1
n-Propylbenzene ND ug/kg 04/25/23 19:30 103-65-104/25/23 14:4710.0 3.6 1
Styrene ND ug/kg 04/25/23 19:30 100-42-504/25/23 14:4710.0 2.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 19:30 630-20-604/25/23 14:4710.0 3.8 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 19:30 79-34-504/25/23 14:4710.0 2.6 1
Tetrachloroethene ND ug/kg 04/25/23 19:30 127-18-404/25/23 14:4710.0 3.2 1
Toluene ND ug/kg 04/25/23 19:30 108-88-304/25/23 14:4710.0 6.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 19:30 87-61-604/25/23 14:4710.0 8.1 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 19:30 120-82-104/25/23 14:4710.0 8.4 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 19:30 71-55-604/25/23 14:4710.0 5.2 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 19:30 79-00-504/25/23 14:4710.0 3.3 1
Trichloroethene ND ug/kg 04/25/23 19:30 79-01-604/25/23 14:4710.0 8.1 1
Trichlorofluoromethane ND ug/kg 04/25/23 19:30 75-69-404/25/23 14:4710.0 5.5 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 19:30 96-18-404/25/23 14:4710.0 5.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 19:30 95-63-604/25/23 14:4710.0 6.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 19:30 108-67-804/25/23 14:4710.0 3.4 1
Vinyl acetate ND ug/kg 04/25/23 19:30 108-05-404/25/23 14:47100 20.6 1
Vinyl chloride ND ug/kg 04/25/23 19:30 75-01-4 v204/25/23 14:4720.0 5.1 1
Xylene (Total)ND ug/kg 04/25/23 19:30 1330-20-704/25/23 14:4720.0 5.7 1
m&p-Xylene ND ug/kg 04/25/23 19:30 179601-23-104/25/23 14:4720.0 6.9 1
o-Xylene ND ug/kg 04/25/23 19:30 95-47-604/25/23 14:4710.0 4.4 1
Surrogates
Toluene-d8 (S)100 %04/25/23 19:30 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)101 %04/25/23 19:30 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)95 %04/25/23 19:30 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.4 %04/21/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.7 %04/27/23 16:5904/27/23 16:441
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-3 Lab ID: 92663594003 Collected: 04/19/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.94 mg/kg 05/01/23 13:48 18540-29-904/30/23 06:541.21 0.308 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-4 Lab ID: 92663594004 Collected: 04/19/23 14:50 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.1 mg/kg 04/27/23 15:52 7440-38-204/26/23 11:040.62 0.18 1
Barium 69.8 mg/kg 04/27/23 15:52 7440-39-304/26/23 11:040.37 0.092 1
Cadmium ND mg/kg 04/27/23 15:52 7440-43-904/26/23 11:040.099 0.036 1
Chromium 58.2 mg/kg 04/27/23 15:52 7440-47-304/26/23 11:042.5 0.48 1
Lead 7.2 mg/kg 04/27/23 15:52 7439-92-104/26/23 11:040.62 0.11 1
Selenium 0.22J mg/kg 04/27/23 15:52 7782-49-204/26/23 11:040.62 0.13 1
Silver ND mg/kg 04/27/23 15:52 7440-22-404/26/23 11:040.62 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.031 mg/kg 04/28/23 09:05 7439-97-604/26/23 11:070.021 0.0092 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 14:41 83-32-904/26/23 15:21423 149 1
Acenaphthylene ND ug/kg 04/27/23 14:41 208-96-804/26/23 15:21423 149 1
Aniline ND ug/kg 04/27/23 14:41 62-53-304/26/23 15:21423 166 1
Anthracene ND ug/kg 04/27/23 14:41 120-12-704/26/23 15:21423 139 1
Benzo(a)anthracene ND ug/kg 04/27/23 14:41 56-55-304/26/23 15:21423 141 1
Benzo(a)pyrene ND ug/kg 04/27/23 14:41 50-32-804/26/23 15:21423 146 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 14:41 205-99-204/26/23 15:21423 141 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 14:41 191-24-204/26/23 15:21423 164 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 14:41 207-08-904/26/23 15:21423 149 1
Benzoic Acid ND ug/kg 04/27/23 14:41 65-85-004/26/23 15:212120 910 1
Benzyl alcohol ND ug/kg 04/27/23 14:41 100-51-604/26/23 15:21847 321 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 14:41 101-55-304/26/23 15:21423 163 1
Butylbenzylphthalate ND ug/kg 04/27/23 14:41 85-68-704/26/23 15:21423 178 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 14:41 59-50-704/26/23 15:21847 298 1
4-Chloroaniline ND ug/kg 04/27/23 14:41 106-47-804/26/23 15:21847 332 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 14:41 111-91-104/26/23 15:21423 176 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 14:41 111-44-404/26/23 15:21423 159 1
2-Chloronaphthalene ND ug/kg 04/27/23 14:41 91-58-704/26/23 15:21423 168 1
2-Chlorophenol ND ug/kg 04/27/23 14:41 95-57-804/26/23 15:21423 159 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 14:41 7005-72-304/26/23 15:21423 158 1
Chrysene ND ug/kg 04/27/23 14:41 218-01-904/26/23 15:21423 154 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 14:41 53-70-304/26/23 15:21423 163 1
Dibenzofuran ND ug/kg 04/27/23 14:41 132-64-904/26/23 15:21423 153 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 14:41 95-50-104/26/23 15:21423 153 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 14:41 541-73-104/26/23 15:21423 150 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 14:41 106-46-704/26/23 15:21423 162 1
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 14:41 91-94-104/26/23 15:21847 286 1
2,4-Dichlorophenol ND ug/kg 04/27/23 14:41 120-83-204/26/23 15:21423 166 1
Diethylphthalate ND ug/kg 04/27/23 14:41 84-66-204/26/23 15:21423 155 1
2,4-Dimethylphenol ND ug/kg 04/27/23 14:41 105-67-904/26/23 15:21423 176 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-4 Lab ID: 92663594004 Collected: 04/19/23 14:50 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/23 14:41 131-11-304/26/23 15:21423 154 1
Di-n-butylphthalate ND ug/kg 04/27/23 14:41 84-74-204/26/23 15:21423 142 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 14:41 534-52-104/26/23 15:21847 395 1
2,4-Dinitrophenol ND ug/kg 04/27/23 14:41 51-28-504/26/23 15:212120 1310 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 14:41 121-14-204/26/23 15:21423 163 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 14:41 606-20-204/26/23 15:21423 155 1
Di-n-octylphthalate ND ug/kg 04/27/23 14:41 117-84-004/26/23 15:21423 167 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 14:41 117-81-704/26/23 15:21423 164 1
Fluoranthene ND ug/kg 04/27/23 14:41 206-44-004/26/23 15:21423 145 1
Fluorene ND ug/kg 04/27/23 14:41 86-73-704/26/23 15:21423 149 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 14:41 87-68-304/26/23 15:21423 183 1
Hexachlorobenzene ND ug/kg 04/27/23 14:41 118-74-104/26/23 15:21423 166 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 14:41 77-47-404/26/23 15:21423 243 1
Hexachloroethane ND ug/kg 04/27/23 14:41 67-72-104/26/23 15:21423 162 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 14:41 193-39-504/26/23 15:21423 167 1
Isophorone ND ug/kg 04/27/23 14:41 78-59-104/26/23 15:21423 189 1
1-Methylnaphthalene ND ug/kg 04/27/23 14:41 90-12-004/26/23 15:21423 149 1
2-Methylnaphthalene ND ug/kg 04/27/23 14:41 91-57-604/26/23 15:21423 169 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 14:41 95-48-704/26/23 15:21423 173 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 14:41 15831-10-404/26/23 15:21423 171 1
Naphthalene ND ug/kg 04/27/23 14:41 91-20-304/26/23 15:21423 144 1
2-Nitroaniline ND ug/kg 04/27/23 14:41 88-74-404/26/23 15:212120 346 1
3-Nitroaniline ND ug/kg 04/27/23 14:41 99-09-204/26/23 15:212120 332 1
4-Nitroaniline ND ug/kg 04/27/23 14:41 100-01-604/26/23 15:21847 322 1
Nitrobenzene ND ug/kg 04/27/23 14:41 98-95-304/26/23 15:21423 196 1
2-Nitrophenol ND ug/kg 04/27/23 14:41 88-75-504/26/23 15:21423 183 1
4-Nitrophenol ND ug/kg 04/27/23 14:41 100-02-704/26/23 15:212120 819 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 14:41 62-75-904/26/23 15:21423 142 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 14:41 621-64-704/26/23 15:21423 159 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 14:41 86-30-604/26/23 15:21423 150 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 14:41 108-60-104/26/23 15:21423 201 1
Pentachlorophenol ND ug/kg 04/27/23 14:41 87-86-504/26/23 15:21847 414 1
Phenanthrene ND ug/kg 04/27/23 14:41 85-01-804/26/23 15:21423 139 1
Phenol ND ug/kg 04/27/23 14:41 108-95-204/26/23 15:21423 189 1
Pyrene ND ug/kg 04/27/23 14:41 129-00-004/26/23 15:21423 172 1
Pyridine ND ug/kg 04/27/23 14:41 110-86-104/26/23 15:21423 133 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 14:41 120-82-104/26/23 15:21423 167 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 14:41 95-95-404/26/23 15:21423 194 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 14:41 88-06-204/26/23 15:21423 174 1
Surrogates
Nitrobenzene-d5 (S)64 %04/27/23 14:41 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)54 %04/27/23 14:41 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)78 %04/27/23 14:41 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)63 %04/27/23 14:41 13127-88-304/26/23 15:2110-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-4 Lab ID: 92663594004 Collected: 04/19/23 14:50 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)58 %04/27/23 14:41 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)66 %04/27/23 14:41 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 19:49 67-64-104/25/23 14:47228 73.2 1
Benzene ND ug/kg 04/25/23 19:49 71-43-204/25/23 14:4711.4 4.5 1
Bromobenzene ND ug/kg 04/25/23 19:49 108-86-104/25/23 14:4711.4 3.7 1
Bromochloromethane ND ug/kg 04/25/23 19:49 74-97-504/25/23 14:4711.4 3.4 1
Bromodichloromethane ND ug/kg 04/25/23 19:49 75-27-404/25/23 14:4711.4 4.4 1
Bromoform ND ug/kg 04/25/23 19:49 75-25-204/25/23 14:4711.4 4.0 1
Bromomethane ND ug/kg 04/25/23 19:49 74-83-9 IK04/25/23 14:4745.6 35.4 1
2-Butanone (MEK)ND ug/kg 04/25/23 19:49 78-93-304/25/23 14:47228 54.8 1
n-Butylbenzene ND ug/kg 04/25/23 19:49 104-51-804/25/23 14:4711.4 7.2 1
sec-Butylbenzene ND ug/kg 04/25/23 19:49 135-98-804/25/23 14:4711.4 5.0 1
tert-Butylbenzene ND ug/kg 04/25/23 19:49 98-06-604/25/23 14:4711.4 4.1 1
Carbon tetrachloride ND ug/kg 04/25/23 19:49 56-23-504/25/23 14:4711.4 4.3 1
Chlorobenzene ND ug/kg 04/25/23 19:49 108-90-704/25/23 14:4711.4 6.5 1
Chloroethane ND ug/kg 04/25/23 19:49 75-00-304/25/23 14:4722.8 8.8 1
Chloroform ND ug/kg 04/25/23 19:49 67-66-304/25/23 14:4711.4 9.5 1
Chloromethane ND ug/kg 04/25/23 19:49 74-87-304/25/23 14:4722.8 9.6 1
2-Chlorotoluene ND ug/kg 04/25/23 19:49 95-49-804/25/23 14:4711.4 4.0 1
4-Chlorotoluene ND ug/kg 04/25/23 19:49 106-43-404/25/23 14:4711.4 6.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 19:49 96-12-804/25/23 14:4711.4 4.4 1
Dibromochloromethane ND ug/kg 04/25/23 19:49 124-48-104/25/23 14:4711.4 6.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 19:49 106-93-404/25/23 14:4711.4 5.0 1
Dibromomethane ND ug/kg 04/25/23 19:49 74-95-304/25/23 14:4711.4 2.4 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 19:49 95-50-104/25/23 14:4711.4 4.1 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 19:49 541-73-104/25/23 14:4711.4 3.5 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 19:49 106-46-704/25/23 14:4711.4 3.0 1
Dichlorodifluoromethane ND ug/kg 04/25/23 19:49 75-71-804/25/23 14:4722.8 11.6 1
1,1-Dichloroethane ND ug/kg 04/25/23 19:49 75-34-304/25/23 14:4711.4 4.7 1
1,2-Dichloroethane ND ug/kg 04/25/23 19:49 107-06-204/25/23 14:4711.4 7.6 1
1,1-Dichloroethene ND ug/kg 04/25/23 19:49 75-35-404/25/23 14:4711.4 4.7 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 19:49 156-59-204/25/23 14:4711.4 3.9 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 19:49 156-60-504/25/23 14:4711.4 9.7 1
1,2-Dichloropropane ND ug/kg 04/25/23 19:49 78-87-504/25/23 14:4711.4 3.4 1
1,3-Dichloropropane ND ug/kg 04/25/23 19:49 142-28-904/25/23 14:4711.4 3.6 1
2,2-Dichloropropane ND ug/kg 04/25/23 19:49 594-20-7 v204/25/23 14:4711.4 8.6 1
1,1-Dichloropropene ND ug/kg 04/25/23 19:49 563-58-604/25/23 14:4711.4 5.5 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 19:49 10061-01-504/25/23 14:4711.4 3.1 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 19:49 10061-02-604/25/23 14:4711.4 3.9 1
Diisopropyl ether ND ug/kg 04/25/23 19:49 108-20-304/25/23 14:4711.4 3.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-4 Lab ID: 92663594004 Collected: 04/19/23 14:50 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/25/23 19:49 100-41-404/25/23 14:4711.4 5.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 19:49 87-68-304/25/23 14:4722.8 18.7 1
2-Hexanone ND ug/kg 04/25/23 19:49 591-78-604/25/23 14:47114 11.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 19:49 98-82-804/25/23 14:4711.4 3.9 1
p-Isopropyltoluene ND ug/kg 04/25/23 19:49 99-87-604/25/23 14:4711.4 5.6 1
Methylene Chloride 165 ug/kg 04/25/23 19:49 75-09-2 C904/25/23 14:4745.6 31.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 19:49 108-10-104/25/23 14:47114 11.0 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 19:49 1634-04-4 v204/25/23 14:4711.4 4.3 1
Naphthalene ND ug/kg 04/25/23 19:49 91-20-304/25/23 14:4711.4 6.0 1
n-Propylbenzene ND ug/kg 04/25/23 19:49 103-65-104/25/23 14:4711.4 4.1 1
Styrene ND ug/kg 04/25/23 19:49 100-42-504/25/23 14:4711.4 3.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 19:49 630-20-604/25/23 14:4711.4 4.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 19:49 79-34-504/25/23 14:4711.4 3.0 1
Tetrachloroethene ND ug/kg 04/25/23 19:49 127-18-404/25/23 14:4711.4 3.6 1
Toluene ND ug/kg 04/25/23 19:49 108-88-304/25/23 14:4711.4 7.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 19:49 87-61-604/25/23 14:4711.4 9.2 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 19:49 120-82-104/25/23 14:4711.4 9.6 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 19:49 71-55-604/25/23 14:4711.4 5.9 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 19:49 79-00-504/25/23 14:4711.4 3.8 1
Trichloroethene ND ug/kg 04/25/23 19:49 79-01-604/25/23 14:4711.4 9.2 1
Trichlorofluoromethane ND ug/kg 04/25/23 19:49 75-69-404/25/23 14:4711.4 6.3 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 19:49 96-18-404/25/23 14:4711.4 5.8 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 19:49 95-63-604/25/23 14:4711.4 6.8 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 19:49 108-67-804/25/23 14:4711.4 3.8 1
Vinyl acetate ND ug/kg 04/25/23 19:49 108-05-404/25/23 14:47114 23.5 1
Vinyl chloride ND ug/kg 04/25/23 19:49 75-01-4 v204/25/23 14:4722.8 5.8 1
Xylene (Total)ND ug/kg 04/25/23 19:49 1330-20-704/25/23 14:4722.8 6.5 1
m&p-Xylene ND ug/kg 04/25/23 19:49 179601-23-104/25/23 14:4722.8 7.8 1
o-Xylene ND ug/kg 04/25/23 19:49 95-47-604/25/23 14:4711.4 5.0 1
Surrogates
Toluene-d8 (S)100 %04/25/23 19:49 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 19:49 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)97 %04/25/23 19:49 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.0 %04/21/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.8 %04/27/23 16:5904/27/23 16:441
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-4 Lab ID: 92663594004 Collected: 04/19/23 14:50 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 4.89 mg/kg 05/01/23 13:53 18540-29-904/30/23 06:541.29 0.328 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-5 Lab ID: 92663594005 Collected: 04/18/23 16:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3015A
Leachate Method/Date: EPA 1311; 05/04/23 14:05
Pace Analytical Services - Minneapolis
6010D MET ICP, TCLP MICRO
Chromium ND mg/L 05/05/23 16:01 7440-47-305/05/23 13:270.10 0.0043 1
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.9 mg/kg 04/27/23 16:01 7440-38-204/26/23 11:040.60 0.17 1
Barium 118 mg/kg 04/27/23 16:01 7440-39-304/26/23 11:040.36 0.090 1
Cadmium ND mg/kg 04/27/23 16:01 7440-43-904/26/23 11:040.096 0.035 1
Chromium 119 mg/kg 04/27/23 16:01 7440-47-304/26/23 11:042.4 0.47 1
Lead 14.6 mg/kg 04/27/23 16:01 7439-92-104/26/23 11:040.60 0.11 1
Selenium 0.43J mg/kg 04/27/23 16:01 7782-49-204/26/23 11:040.60 0.13 1
Silver ND mg/kg 04/27/23 16:01 7440-22-404/26/23 11:040.60 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.013J mg/kg 04/28/23 09:10 7439-97-604/26/23 11:070.023 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 15:08 83-32-904/26/23 15:21427 150 1
Acenaphthylene ND ug/kg 04/27/23 15:08 208-96-804/26/23 15:21427 150 1
Aniline ND ug/kg 04/27/23 15:08 62-53-304/26/23 15:21427 167 1
Anthracene ND ug/kg 04/27/23 15:08 120-12-704/26/23 15:21427 140 1
Benzo(a)anthracene ND ug/kg 04/27/23 15:08 56-55-304/26/23 15:21427 142 1
Benzo(a)pyrene ND ug/kg 04/27/23 15:08 50-32-804/26/23 15:21427 147 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 15:08 205-99-204/26/23 15:21427 142 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 15:08 191-24-204/26/23 15:21427 166 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 15:08 207-08-904/26/23 15:21427 150 1
Benzoic Acid ND ug/kg 04/27/23 15:08 65-85-004/26/23 15:212130 917 1
Benzyl alcohol ND ug/kg 04/27/23 15:08 100-51-604/26/23 15:21854 323 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 15:08 101-55-304/26/23 15:21427 164 1
Butylbenzylphthalate ND ug/kg 04/27/23 15:08 85-68-704/26/23 15:21427 180 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 15:08 59-50-704/26/23 15:21854 300 1
4-Chloroaniline ND ug/kg 04/27/23 15:08 106-47-804/26/23 15:21854 335 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 15:08 111-91-104/26/23 15:21427 177 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 15:08 111-44-404/26/23 15:21427 160 1
2-Chloronaphthalene ND ug/kg 04/27/23 15:08 91-58-704/26/23 15:21427 169 1
2-Chlorophenol ND ug/kg 04/27/23 15:08 95-57-804/26/23 15:21427 160 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 15:08 7005-72-304/26/23 15:21427 159 1
Chrysene ND ug/kg 04/27/23 15:08 218-01-904/26/23 15:21427 155 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 15:08 53-70-304/26/23 15:21427 164 1
Dibenzofuran ND ug/kg 04/27/23 15:08 132-64-904/26/23 15:21427 154 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 15:08 95-50-104/26/23 15:21427 154 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 15:08 541-73-104/26/23 15:21427 151 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-5 Lab ID: 92663594005 Collected: 04/18/23 16:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,4-Dichlorobenzene ND ug/kg 04/27/23 15:08 106-46-704/26/23 15:21427 163 1
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 15:08 91-94-104/26/23 15:21854 288 1
2,4-Dichlorophenol ND ug/kg 04/27/23 15:08 120-83-204/26/23 15:21427 167 1
Diethylphthalate ND ug/kg 04/27/23 15:08 84-66-204/26/23 15:21427 157 1
2,4-Dimethylphenol ND ug/kg 04/27/23 15:08 105-67-904/26/23 15:21427 177 1
Dimethylphthalate ND ug/kg 04/27/23 15:08 131-11-304/26/23 15:21427 155 1
Di-n-butylphthalate ND ug/kg 04/27/23 15:08 84-74-204/26/23 15:21427 144 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 15:08 534-52-104/26/23 15:21854 398 1
2,4-Dinitrophenol ND ug/kg 04/27/23 15:08 51-28-504/26/23 15:212130 1320 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 15:08 121-14-204/26/23 15:21427 164 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 15:08 606-20-204/26/23 15:21427 157 1
Di-n-octylphthalate ND ug/kg 04/27/23 15:08 117-84-004/26/23 15:21427 168 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 15:08 117-81-704/26/23 15:21427 166 1
Fluoranthene ND ug/kg 04/27/23 15:08 206-44-004/26/23 15:21427 146 1
Fluorene ND ug/kg 04/27/23 15:08 86-73-704/26/23 15:21427 150 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 15:08 87-68-304/26/23 15:21427 185 1
Hexachlorobenzene ND ug/kg 04/27/23 15:08 118-74-104/26/23 15:21427 167 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 15:08 77-47-404/26/23 15:21427 245 1
Hexachloroethane ND ug/kg 04/27/23 15:08 67-72-104/26/23 15:21427 163 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 15:08 193-39-504/26/23 15:21427 168 1
Isophorone ND ug/kg 04/27/23 15:08 78-59-104/26/23 15:21427 190 1
1-Methylnaphthalene ND ug/kg 04/27/23 15:08 90-12-004/26/23 15:21427 150 1
2-Methylnaphthalene ND ug/kg 04/27/23 15:08 91-57-604/26/23 15:21427 171 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 15:08 95-48-704/26/23 15:21427 175 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 15:08 15831-10-404/26/23 15:21427 172 1
Naphthalene ND ug/kg 04/27/23 15:08 91-20-304/26/23 15:21427 145 1
2-Nitroaniline ND ug/kg 04/27/23 15:08 88-74-404/26/23 15:212130 349 1
3-Nitroaniline ND ug/kg 04/27/23 15:08 99-09-204/26/23 15:212130 335 1
4-Nitroaniline ND ug/kg 04/27/23 15:08 100-01-604/26/23 15:21854 325 1
Nitrobenzene ND ug/kg 04/27/23 15:08 98-95-304/26/23 15:21427 198 1
2-Nitrophenol ND ug/kg 04/27/23 15:08 88-75-504/26/23 15:21427 185 1
4-Nitrophenol ND ug/kg 04/27/23 15:08 100-02-704/26/23 15:212130 825 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 15:08 62-75-904/26/23 15:21427 144 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 15:08 621-64-704/26/23 15:21427 160 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 15:08 86-30-604/26/23 15:21427 151 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 15:08 108-60-104/26/23 15:21427 203 1
Pentachlorophenol ND ug/kg 04/27/23 15:08 87-86-504/26/23 15:21854 418 1
Phenanthrene ND ug/kg 04/27/23 15:08 85-01-804/26/23 15:21427 140 1
Phenol ND ug/kg 04/27/23 15:08 108-95-204/26/23 15:21427 190 1
Pyrene ND ug/kg 04/27/23 15:08 129-00-004/26/23 15:21427 173 1
Pyridine ND ug/kg 04/27/23 15:08 110-86-104/26/23 15:21427 135 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 15:08 120-82-104/26/23 15:21427 168 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 15:08 95-95-404/26/23 15:21427 195 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 15:08 88-06-204/26/23 15:21427 176 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-5 Lab ID: 92663594005 Collected: 04/18/23 16:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)58 %04/27/23 15:08 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)50 %04/27/23 15:08 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)79 %04/27/23 15:08 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)53 %04/27/23 15:08 13127-88-304/26/23 15:2110-130 1
2-Fluorophenol (S)48 %04/27/23 15:08 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)57 %04/27/23 15:08 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 20:07 67-64-104/25/23 14:47134 43.2 1
Benzene ND ug/kg 04/25/23 20:07 71-43-204/25/23 14:476.7 2.7 1
Bromobenzene ND ug/kg 04/25/23 20:07 108-86-104/25/23 14:476.7 2.2 1
Bromochloromethane ND ug/kg 04/25/23 20:07 74-97-504/25/23 14:476.7 2.0 1
Bromodichloromethane ND ug/kg 04/25/23 20:07 75-27-404/25/23 14:476.7 2.6 1
Bromoform ND ug/kg 04/25/23 20:07 75-25-204/25/23 14:476.7 2.4 1
Bromomethane ND ug/kg 04/25/23 20:07 74-83-9 IK04/25/23 14:4726.9 20.8 1
2-Butanone (MEK)ND ug/kg 04/25/23 20:07 78-93-304/25/23 14:47134 32.3 1
n-Butylbenzene ND ug/kg 04/25/23 20:07 104-51-804/25/23 14:476.7 4.2 1
sec-Butylbenzene ND ug/kg 04/25/23 20:07 135-98-804/25/23 14:476.7 3.0 1
tert-Butylbenzene ND ug/kg 04/25/23 20:07 98-06-604/25/23 14:476.7 2.4 1
Carbon tetrachloride ND ug/kg 04/25/23 20:07 56-23-504/25/23 14:476.7 2.5 1
Chlorobenzene ND ug/kg 04/25/23 20:07 108-90-704/25/23 14:476.7 3.9 1
Chloroethane ND ug/kg 04/25/23 20:07 75-00-304/25/23 14:4713.4 5.2 1
Chloroform ND ug/kg 04/25/23 20:07 67-66-304/25/23 14:476.7 5.6 1
Chloromethane ND ug/kg 04/25/23 20:07 74-87-304/25/23 14:4713.4 5.6 1
2-Chlorotoluene ND ug/kg 04/25/23 20:07 95-49-804/25/23 14:476.7 2.4 1
4-Chlorotoluene ND ug/kg 04/25/23 20:07 106-43-404/25/23 14:476.7 3.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 20:07 96-12-804/25/23 14:476.7 2.6 1
Dibromochloromethane ND ug/kg 04/25/23 20:07 124-48-104/25/23 14:476.7 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 20:07 106-93-404/25/23 14:476.7 3.0 1
Dibromomethane ND ug/kg 04/25/23 20:07 74-95-304/25/23 14:476.7 1.4 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 20:07 95-50-104/25/23 14:476.7 2.4 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 20:07 541-73-104/25/23 14:476.7 2.1 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 20:07 106-46-704/25/23 14:476.7 1.7 1
Dichlorodifluoromethane ND ug/kg 04/25/23 20:07 75-71-804/25/23 14:4713.4 6.8 1
1,1-Dichloroethane ND ug/kg 04/25/23 20:07 75-34-304/25/23 14:476.7 2.8 1
1,2-Dichloroethane ND ug/kg 04/25/23 20:07 107-06-204/25/23 14:476.7 4.5 1
1,1-Dichloroethene ND ug/kg 04/25/23 20:07 75-35-404/25/23 14:476.7 2.8 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 20:07 156-59-204/25/23 14:476.7 2.3 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 20:07 156-60-504/25/23 14:476.7 5.7 1
1,2-Dichloropropane ND ug/kg 04/25/23 20:07 78-87-504/25/23 14:476.7 2.0 1
1,3-Dichloropropane ND ug/kg 04/25/23 20:07 142-28-904/25/23 14:476.7 2.1 1
2,2-Dichloropropane ND ug/kg 04/25/23 20:07 594-20-7 v204/25/23 14:476.7 5.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-5 Lab ID: 92663594005 Collected: 04/18/23 16:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 20:07 563-58-604/25/23 14:476.7 3.2 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 20:07 10061-01-504/25/23 14:476.7 1.8 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 20:07 10061-02-604/25/23 14:476.7 2.3 1
Diisopropyl ether ND ug/kg 04/25/23 20:07 108-20-304/25/23 14:476.7 1.8 1
Ethylbenzene ND ug/kg 04/25/23 20:07 100-41-404/25/23 14:476.7 3.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 20:07 87-68-304/25/23 14:4713.4 11.0 1
2-Hexanone ND ug/kg 04/25/23 20:07 591-78-604/25/23 14:4767.2 6.5 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 20:07 98-82-804/25/23 14:476.7 2.3 1
p-Isopropyltoluene ND ug/kg 04/25/23 20:07 99-87-604/25/23 14:476.7 3.3 1
Methylene Chloride 50.0 ug/kg 04/25/23 20:07 75-09-2 C904/25/23 14:4726.9 18.4 1
4-Methyl-2-pentanone (MIBK)48.4J ug/kg 04/25/23 20:07 108-10-104/25/23 14:4767.2 6.5 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 20:07 1634-04-4 v204/25/23 14:476.7 2.5 1
Naphthalene ND ug/kg 04/25/23 20:07 91-20-304/25/23 14:476.7 3.5 1
n-Propylbenzene 3.9J ug/kg 04/25/23 20:07 103-65-104/25/23 14:476.7 2.4 1
Styrene ND ug/kg 04/25/23 20:07 100-42-504/25/23 14:476.7 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 20:07 630-20-604/25/23 14:476.7 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 20:07 79-34-504/25/23 14:476.7 1.8 1
Tetrachloroethene ND ug/kg 04/25/23 20:07 127-18-404/25/23 14:476.7 2.1 1
Toluene ND ug/kg 04/25/23 20:07 108-88-304/25/23 14:476.7 4.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 20:07 87-61-604/25/23 14:476.7 5.4 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 20:07 120-82-104/25/23 14:476.7 5.6 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 20:07 71-55-604/25/23 14:476.7 3.5 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 20:07 79-00-504/25/23 14:476.7 2.2 1
Trichloroethene ND ug/kg 04/25/23 20:07 79-01-604/25/23 14:476.7 5.4 1
Trichlorofluoromethane ND ug/kg 04/25/23 20:07 75-69-404/25/23 14:476.7 3.7 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 20:07 96-18-404/25/23 14:476.7 3.4 1
1,2,4-Trimethylbenzene 8.2 ug/kg 04/25/23 20:07 95-63-604/25/23 14:476.7 4.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 20:07 108-67-804/25/23 14:476.7 2.3 1
Vinyl acetate ND ug/kg 04/25/23 20:07 108-05-404/25/23 14:4767.2 13.8 1
Vinyl chloride ND ug/kg 04/25/23 20:07 75-01-4 v204/25/23 14:4713.4 3.4 1
Xylene (Total)ND ug/kg 04/25/23 20:07 1330-20-704/25/23 14:4713.4 3.8 1
m&p-Xylene ND ug/kg 04/25/23 20:07 179601-23-104/25/23 14:4713.4 4.6 1
o-Xylene ND ug/kg 04/25/23 20:07 95-47-604/25/23 14:476.7 3.0 1
Surrogates
Toluene-d8 (S)101 %04/25/23 20:07 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 20:07 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)97 %04/25/23 20:07 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.9 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-5 Lab ID: 92663594005 Collected: 04/18/23 16:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.8 %04/27/23 16:5904/27/23 16:441
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.37 mg/kg 05/01/23 14:09 18540-29-904/30/23 06:541.29 0.328 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-6 Lab ID: 92663594006 Collected: 04/18/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.2 mg/kg 04/27/23 16:04 7440-38-204/26/23 11:040.57 0.16 1
Barium 151 mg/kg 04/27/23 16:04 7440-39-304/26/23 11:040.34 0.085 1
Cadmium 0.58 mg/kg 04/27/23 16:04 7440-43-904/26/23 11:040.091 0.033 1
Chromium 68.6 mg/kg 04/27/23 16:04 7440-47-304/26/23 11:042.3 0.44 1
Lead 29.6 mg/kg 04/27/23 16:04 7439-92-104/26/23 11:040.57 0.11 1
Selenium 0.61 mg/kg 04/27/23 16:04 7782-49-204/26/23 11:040.57 0.12 1
Silver ND mg/kg 04/27/23 16:04 7440-22-404/26/23 11:040.57 0.23 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.021J mg/kg 04/28/23 09:12 7439-97-604/26/23 11:070.022 0.0097 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene 24200 ug/kg 04/27/23 18:24 83-32-904/26/23 15:214110 1440 10
Acenaphthylene ND ug/kg 04/27/23 18:24 208-96-804/26/23 15:214110 1440 10
Aniline ND ug/kg 04/27/23 18:24 62-53-304/26/23 15:214110 1610 10
Anthracene 30500 ug/kg 04/27/23 18:24 120-12-704/26/23 15:214110 1340 10
Benzo(a)anthracene 53000 ug/kg 04/28/23 09:17 56-55-304/26/23 15:2120500 6850 50
Benzo(a)pyrene 45800 ug/kg 04/28/23 09:17 50-32-804/26/23 15:2120500 7100 50
Benzo(b)fluoranthene 64000 ug/kg 04/28/23 09:17 205-99-204/26/23 15:2120500 6850 50
Benzo(g,h,i)perylene 30900 ug/kg 04/27/23 18:24 191-24-204/26/23 15:214110 1590 10
Benzo(k)fluoranthene 22800 ug/kg 04/27/23 18:24 207-08-904/26/23 15:214110 1440 10
Benzoic Acid ND ug/kg 04/27/23 18:24 65-85-004/26/23 15:2120500 8830 10
Benzyl alcohol ND ug/kg 04/27/23 18:24 100-51-604/26/23 15:218220 3110 10
4-Bromophenylphenyl ether ND ug/kg 04/27/23 18:24 101-55-304/26/23 15:214110 1580 10
Butylbenzylphthalate ND ug/kg 04/27/23 18:24 85-68-704/26/23 15:214110 1730 10
4-Chloro-3-methylphenol ND ug/kg 04/27/23 18:24 59-50-704/26/23 15:218220 2890 10
4-Chloroaniline ND ug/kg 04/27/23 18:24 106-47-804/26/23 15:218220 3220 10
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 18:24 111-91-104/26/23 15:214110 1710 10
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 18:24 111-44-404/26/23 15:214110 1540 10
2-Chloronaphthalene ND ug/kg 04/27/23 18:24 91-58-704/26/23 15:214110 1630 10
2-Chlorophenol ND ug/kg 04/27/23 18:24 95-57-804/26/23 15:214110 1540 10
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 18:24 7005-72-304/26/23 15:214110 1530 10
Chrysene 51900 ug/kg 04/28/23 09:17 218-01-904/26/23 15:2120500 7470 50
Dibenz(a,h)anthracene ND ug/kg 04/27/23 18:24 53-70-304/26/23 15:214110 1580 10
Dibenzofuran 10000 ug/kg 04/27/23 18:24 132-64-904/26/23 15:214110 1480 10
1,2-Dichlorobenzene ND ug/kg 04/27/23 18:24 95-50-104/26/23 15:214110 1480 10
1,3-Dichlorobenzene ND ug/kg 04/27/23 18:24 541-73-104/26/23 15:214110 1460 10
1,4-Dichlorobenzene ND ug/kg 04/27/23 18:24 106-46-704/26/23 15:214110 1570 10
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 18:24 91-94-104/26/23 15:218220 2780 10
2,4-Dichlorophenol ND ug/kg 04/27/23 18:24 120-83-204/26/23 15:214110 1610 10
Diethylphthalate ND ug/kg 04/27/23 18:24 84-66-204/26/23 15:214110 1510 10
2,4-Dimethylphenol ND ug/kg 04/27/23 18:24 105-67-904/26/23 15:214110 1710 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-6 Lab ID: 92663594006 Collected: 04/18/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 04/27/23 18:24 131-11-304/26/23 15:214110 1490 10
Di-n-butylphthalate ND ug/kg 04/27/23 18:24 84-74-204/26/23 15:214110 1380 10
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 18:24 534-52-104/26/23 15:218220 3830 10
2,4-Dinitrophenol ND ug/kg 04/27/23 18:24 51-28-504/26/23 15:2120500 12700 10
2,4-Dinitrotoluene ND ug/kg 04/27/23 18:24 121-14-204/26/23 15:214110 1580 10
2,6-Dinitrotoluene ND ug/kg 04/27/23 18:24 606-20-204/26/23 15:214110 1510 10
Di-n-octylphthalate ND ug/kg 04/27/23 18:24 117-84-004/26/23 15:214110 1620 10
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 18:24 117-81-704/26/23 15:214110 1590 10
Fluoranthene 106000 ug/kg 04/28/23 09:17 206-44-004/26/23 15:2120500 7030 50
Fluorene 21300 ug/kg 04/27/23 18:24 86-73-704/26/23 15:214110 1440 10
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 18:24 87-68-304/26/23 15:214110 1780 10
Hexachlorobenzene ND ug/kg 04/27/23 18:24 118-74-104/26/23 15:214110 1610 10
Hexachlorocyclopentadiene ND ug/kg 04/27/23 18:24 77-47-404/26/23 15:214110 2350 10
Hexachloroethane ND ug/kg 04/27/23 18:24 67-72-104/26/23 15:214110 1570 10
Indeno(1,2,3-cd)pyrene 29800 ug/kg 04/27/23 18:24 193-39-504/26/23 15:214110 1620 10
Isophorone ND ug/kg 04/27/23 18:24 78-59-104/26/23 15:214110 1830 10
1-Methylnaphthalene 2810J ug/kg 04/27/23 18:24 90-12-004/26/23 15:214110 1440 10
2-Methylnaphthalene 5080 ug/kg 04/27/23 18:24 91-57-604/26/23 15:214110 1640 10
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 18:24 95-48-704/26/23 15:214110 1680 10
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 18:24 15831-10-404/26/23 15:214110 1660 10
Naphthalene 12600 ug/kg 04/27/23 18:24 91-20-304/26/23 15:214110 1390 10
2-Nitroaniline ND ug/kg 04/27/23 18:24 88-74-404/26/23 15:2120500 3360 10
3-Nitroaniline ND ug/kg 04/27/23 18:24 99-09-204/26/23 15:2120500 3220 10
4-Nitroaniline ND ug/kg 04/27/23 18:24 100-01-604/26/23 15:218220 3130 10
Nitrobenzene ND ug/kg 04/27/23 18:24 98-95-304/26/23 15:214110 1910 10
2-Nitrophenol ND ug/kg 04/27/23 18:24 88-75-504/26/23 15:214110 1780 10
4-Nitrophenol ND ug/kg 04/27/23 18:24 100-02-704/26/23 15:2120500 7940 10
N-Nitrosodimethylamine ND ug/kg 04/27/23 18:24 62-75-904/26/23 15:214110 1380 10
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 18:24 621-64-704/26/23 15:214110 1540 10
N-Nitrosodiphenylamine ND ug/kg 04/27/23 18:24 86-30-604/26/23 15:214110 1460 10
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 18:24 108-60-104/26/23 15:214110 1950 10
Pentachlorophenol ND ug/kg 04/27/23 18:24 87-86-504/26/23 15:218220 4020 10
Phenanthrene 116000 ug/kg 04/28/23 09:17 85-01-804/26/23 15:2120500 6720 50
Phenol ND ug/kg 04/27/23 18:24 108-95-204/26/23 15:214110 1830 10
Pyrene 91800 ug/kg 04/28/23 09:17 129-00-004/26/23 15:2120500 8340 50
Pyridine ND ug/kg 04/27/23 18:24 110-86-104/26/23 15:214110 1290 10
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 18:24 120-82-104/26/23 15:214110 1620 10
2,4,5-Trichlorophenol ND ug/kg 04/27/23 18:24 95-95-404/26/23 15:214110 1880 10
2,4,6-Trichlorophenol ND ug/kg 04/27/23 18:24 88-06-204/26/23 15:214110 1690 10
Surrogates
Nitrobenzene-d5 (S)0 %04/27/23 18:24 4165-60-0 D3,S404/26/23 15:2110-130 10
2-Fluorobiphenyl (S)0 %04/27/23 18:24 321-60-8 S404/26/23 15:2110-130 10
Terphenyl-d14 (S)0 %04/27/23 18:24 1718-51-0 S404/26/23 15:2110-130 10
Phenol-d6 (S)0 %04/27/23 18:24 13127-88-3 S404/26/23 15:2110-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-6 Lab ID: 92663594006 Collected: 04/18/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %04/27/23 18:24 367-12-4 S404/26/23 15:2110-130 10
2,4,6-Tribromophenol (S)0 %04/27/23 18:24 118-79-6 S404/26/23 15:2110-131 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 20:25 67-64-104/25/23 14:47299 95.8 1
Benzene ND ug/kg 04/25/23 20:25 71-43-204/25/23 14:4714.9 5.9 1
Bromobenzene ND ug/kg 04/25/23 20:25 108-86-104/25/23 14:4714.9 4.9 1
Bromochloromethane ND ug/kg 04/25/23 20:25 74-97-504/25/23 14:4714.9 4.4 1
Bromodichloromethane ND ug/kg 04/25/23 20:25 75-27-404/25/23 14:4714.9 5.8 1
Bromoform ND ug/kg 04/25/23 20:25 75-25-204/25/23 14:4714.9 5.3 1
Bromomethane ND ug/kg 04/25/23 20:25 74-83-9 IK04/25/23 14:4759.7 46.3 1
2-Butanone (MEK)ND ug/kg 04/25/23 20:25 78-93-304/25/23 14:47299 71.6 1
n-Butylbenzene ND ug/kg 04/25/23 20:25 104-51-804/25/23 14:4714.9 9.4 1
sec-Butylbenzene ND ug/kg 04/25/23 20:25 135-98-804/25/23 14:4714.9 6.6 1
tert-Butylbenzene ND ug/kg 04/25/23 20:25 98-06-604/25/23 14:4714.9 5.3 1
Carbon tetrachloride ND ug/kg 04/25/23 20:25 56-23-504/25/23 14:4714.9 5.6 1
Chlorobenzene ND ug/kg 04/25/23 20:25 108-90-704/25/23 14:4714.9 8.6 1
Chloroethane ND ug/kg 04/25/23 20:25 75-00-304/25/23 14:4729.9 11.5 1
Chloroform ND ug/kg 04/25/23 20:25 67-66-304/25/23 14:4714.9 12.5 1
Chloromethane ND ug/kg 04/25/23 20:25 74-87-304/25/23 14:4729.9 12.5 1
2-Chlorotoluene ND ug/kg 04/25/23 20:25 95-49-804/25/23 14:4714.9 5.3 1
4-Chlorotoluene ND ug/kg 04/25/23 20:25 106-43-404/25/23 14:4714.9 8.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 20:25 96-12-804/25/23 14:4714.9 5.8 1
Dibromochloromethane ND ug/kg 04/25/23 20:25 124-48-104/25/23 14:4714.9 8.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 20:25 106-93-404/25/23 14:4714.9 6.6 1
Dibromomethane ND ug/kg 04/25/23 20:25 74-95-304/25/23 14:4714.9 3.2 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 20:25 95-50-104/25/23 14:4714.9 5.4 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 20:25 541-73-104/25/23 14:4714.9 4.6 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 20:25 106-46-704/25/23 14:4714.9 3.9 1
Dichlorodifluoromethane ND ug/kg 04/25/23 20:25 75-71-804/25/23 14:4729.9 15.2 1
1,1-Dichloroethane ND ug/kg 04/25/23 20:25 75-34-304/25/23 14:4714.9 6.1 1
1,2-Dichloroethane ND ug/kg 04/25/23 20:25 107-06-204/25/23 14:4714.9 9.9 1
1,1-Dichloroethene ND ug/kg 04/25/23 20:25 75-35-404/25/23 14:4714.9 6.1 1
cis-1,2-Dichloroethene 13.4J ug/kg 04/25/23 20:25 156-59-204/25/23 14:4714.9 5.1 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 20:25 156-60-504/25/23 14:4714.9 12.7 1
1,2-Dichloropropane ND ug/kg 04/25/23 20:25 78-87-504/25/23 14:4714.9 4.5 1
1,3-Dichloropropane ND ug/kg 04/25/23 20:25 142-28-904/25/23 14:4714.9 4.7 1
2,2-Dichloropropane ND ug/kg 04/25/23 20:25 594-20-7 v204/25/23 14:4714.9 11.3 1
1,1-Dichloropropene ND ug/kg 04/25/23 20:25 563-58-604/25/23 14:4714.9 7.2 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 20:25 10061-01-504/25/23 14:4714.9 4.1 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 20:25 10061-02-604/25/23 14:4714.9 5.1 1
Diisopropyl ether ND ug/kg 04/25/23 20:25 108-20-304/25/23 14:4714.9 4.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-6 Lab ID: 92663594006 Collected: 04/18/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 04/25/23 20:25 100-41-404/25/23 14:4714.9 7.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 20:25 87-68-304/25/23 14:4729.9 24.4 1
2-Hexanone ND ug/kg 04/25/23 20:25 591-78-604/25/23 14:47149 14.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 20:25 98-82-804/25/23 14:4714.9 5.1 1
p-Isopropyltoluene ND ug/kg 04/25/23 20:25 99-87-604/25/23 14:4714.9 7.3 1
Methylene Chloride 111 ug/kg 04/25/23 20:25 75-09-2 C904/25/23 14:4759.7 40.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 20:25 108-10-104/25/23 14:47149 14.4 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 20:25 1634-04-4 v204/25/23 14:4714.9 5.6 1
Naphthalene 19.8 ug/kg 04/25/23 20:25 91-20-304/25/23 14:4714.9 7.9 1
n-Propylbenzene ND ug/kg 04/25/23 20:25 103-65-104/25/23 14:4714.9 5.3 1
Styrene ND ug/kg 04/25/23 20:25 100-42-504/25/23 14:4714.9 3.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 20:25 630-20-604/25/23 14:4714.9 5.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 20:25 79-34-504/25/23 14:4714.9 3.9 1
Tetrachloroethene ND ug/kg 04/25/23 20:25 127-18-404/25/23 14:4714.9 4.7 1
Toluene ND ug/kg 04/25/23 20:25 108-88-304/25/23 14:4714.9 10.3 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 20:25 87-61-604/25/23 14:4714.9 12.1 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 20:25 120-82-104/25/23 14:4714.9 12.5 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 20:25 71-55-604/25/23 14:4714.9 7.8 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 20:25 79-00-504/25/23 14:4714.9 5.0 1
Trichloroethene 29.0 ug/kg 04/25/23 20:25 79-01-604/25/23 14:4714.9 12.0 1
Trichlorofluoromethane ND ug/kg 04/25/23 20:25 75-69-404/25/23 14:4714.9 8.2 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 20:25 96-18-404/25/23 14:4714.9 7.6 1
1,2,4-Trimethylbenzene 17.8 ug/kg 04/25/23 20:25 95-63-604/25/23 14:4714.9 8.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 20:25 108-67-804/25/23 14:4714.9 5.0 1
Vinyl acetate ND ug/kg 04/25/23 20:25 108-05-404/25/23 14:47149 30.7 1
Vinyl chloride ND ug/kg 04/25/23 20:25 75-01-4 v204/25/23 14:4729.9 7.6 1
Xylene (Total)ND ug/kg 04/25/23 20:25 1330-20-704/25/23 14:4729.9 8.5 1
m&p-Xylene ND ug/kg 04/25/23 20:25 179601-23-104/25/23 14:4729.9 10.2 1
o-Xylene ND ug/kg 04/25/23 20:25 95-47-604/25/23 14:4714.9 6.6 1
Surrogates
Toluene-d8 (S)100 %04/25/23 20:25 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)99 %04/25/23 20:25 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)99 %04/25/23 20:25 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.1 %04/21/23 17:16 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.2 %04/27/23 16:5904/27/23 16:441
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-6 Lab ID: 92663594006 Collected: 04/18/23 16:05 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 26.4 mg/kg 05/01/23 14:19 18540-29-904/30/23 06:541.25 0.318 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-7 Lab ID: 92663594007 Collected: 04/17/23 16:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 16300 mg/kg 04/28/23 09:46 7429-90-504/26/23 11:0436.1 7.3 1
Arsenic 2.2 mg/kg 04/27/23 16:07 7440-38-204/26/23 11:040.60 0.17 1
Barium 18.0 mg/kg 04/27/23 16:07 7440-39-304/26/23 11:040.36 0.090 1
Cadmium ND mg/kg 04/27/23 16:07 7440-43-904/26/23 11:040.096 0.035 1
Chromium 57.9 mg/kg 04/27/23 16:07 7440-47-304/26/23 11:042.4 0.47 1
Copper 20.9 mg/kg 04/27/23 16:07 7440-50-804/26/23 11:041.2 0.37 1
Lead 7.9 mg/kg 04/27/23 16:07 7439-92-104/26/23 11:040.60 0.11 1
Nickel 7.4 mg/kg 04/27/23 16:07 7440-02-004/26/23 11:040.60 0.28 1
Selenium 0.51J mg/kg 04/27/23 16:07 7782-49-204/26/23 11:040.60 0.13 1
Silver ND mg/kg 04/27/23 16:07 7440-22-404/26/23 11:040.60 0.25 1
Zinc 16.6 mg/kg 04/27/23 16:07 7440-66-604/26/23 11:046.0 1.4 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.034 mg/kg 04/28/23 09:13 7439-97-604/26/23 11:070.023 0.0099 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 13:19 83-32-904/26/23 15:21403 141 1
Acenaphthylene ND ug/kg 04/27/23 13:19 208-96-804/26/23 15:21403 141 1
Aniline ND ug/kg 04/27/23 13:19 62-53-304/26/23 15:21403 157 1
Anthracene ND ug/kg 04/27/23 13:19 120-12-704/26/23 15:21403 132 1
Benzo(a)anthracene ND ug/kg 04/27/23 13:19 56-55-304/26/23 15:21403 134 1
Benzo(a)pyrene ND ug/kg 04/27/23 13:19 50-32-804/26/23 15:21403 139 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 13:19 205-99-204/26/23 15:21403 134 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 13:19 191-24-204/26/23 15:21403 156 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 13:19 207-08-904/26/23 15:21403 141 1
Benzoic Acid ND ug/kg 04/27/23 13:19 65-85-004/26/23 15:212010 865 1
Benzyl alcohol ND ug/kg 04/27/23 13:19 100-51-604/26/23 15:21805 305 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 13:19 101-55-304/26/23 15:21403 155 1
Butylbenzylphthalate ND ug/kg 04/27/23 13:19 85-68-704/26/23 15:21403 170 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 13:19 59-50-704/26/23 15:21805 283 1
4-Chloroaniline ND ug/kg 04/27/23 13:19 106-47-804/26/23 15:21805 316 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 13:19 111-91-104/26/23 15:21403 167 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 13:19 111-44-404/26/23 15:21403 151 1
2-Chloronaphthalene ND ug/kg 04/27/23 13:19 91-58-704/26/23 15:21403 160 1
2-Chlorophenol ND ug/kg 04/27/23 13:19 95-57-804/26/23 15:21403 151 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 13:19 7005-72-304/26/23 15:21403 150 1
Chrysene ND ug/kg 04/27/23 13:19 218-01-904/26/23 15:21403 146 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 13:19 53-70-304/26/23 15:21403 155 1
Dibenzofuran ND ug/kg 04/27/23 13:19 132-64-904/26/23 15:21403 145 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 13:19 95-50-104/26/23 15:21403 145 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 13:19 541-73-104/26/23 15:21403 143 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 13:19 106-46-704/26/23 15:21403 154 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-7 Lab ID: 92663594007 Collected: 04/17/23 16:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 13:19 91-94-104/26/23 15:21805 272 1
2,4-Dichlorophenol ND ug/kg 04/27/23 13:19 120-83-204/26/23 15:21403 157 1
Diethylphthalate ND ug/kg 04/27/23 13:19 84-66-204/26/23 15:21403 148 1
2,4-Dimethylphenol ND ug/kg 04/27/23 13:19 105-67-904/26/23 15:21403 167 1
Dimethylphthalate ND ug/kg 04/27/23 13:19 131-11-304/26/23 15:21403 146 1
Di-n-butylphthalate ND ug/kg 04/27/23 13:19 84-74-204/26/23 15:21403 135 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 13:19 534-52-104/26/23 15:21805 376 1
2,4-Dinitrophenol ND ug/kg 04/27/23 13:19 51-28-504/26/23 15:212010 1240 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 13:19 121-14-204/26/23 15:21403 155 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 13:19 606-20-204/26/23 15:21403 148 1
Di-n-octylphthalate ND ug/kg 04/27/23 13:19 117-84-004/26/23 15:21403 159 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 13:19 117-81-704/26/23 15:21403 156 1
Fluoranthene ND ug/kg 04/27/23 13:19 206-44-004/26/23 15:21403 138 1
Fluorene ND ug/kg 04/27/23 13:19 86-73-704/26/23 15:21403 141 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 13:19 87-68-304/26/23 15:21403 174 1
Hexachlorobenzene ND ug/kg 04/27/23 13:19 118-74-104/26/23 15:21403 157 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 13:19 77-47-404/26/23 15:21403 231 1
Hexachloroethane ND ug/kg 04/27/23 13:19 67-72-104/26/23 15:21403 154 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 13:19 193-39-504/26/23 15:21403 159 1
Isophorone ND ug/kg 04/27/23 13:19 78-59-104/26/23 15:21403 179 1
1-Methylnaphthalene ND ug/kg 04/27/23 13:19 90-12-004/26/23 15:21403 141 1
2-Methylnaphthalene ND ug/kg 04/27/23 13:19 91-57-604/26/23 15:21403 161 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 13:19 95-48-704/26/23 15:21403 165 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 13:19 15831-10-404/26/23 15:21403 162 1
Naphthalene ND ug/kg 04/27/23 13:19 91-20-304/26/23 15:21403 137 1
2-Nitroaniline ND ug/kg 04/27/23 13:19 88-74-404/26/23 15:212010 329 1
3-Nitroaniline ND ug/kg 04/27/23 13:19 99-09-204/26/23 15:212010 316 1
4-Nitroaniline ND ug/kg 04/27/23 13:19 100-01-604/26/23 15:21805 306 1
Nitrobenzene ND ug/kg 04/27/23 13:19 98-95-304/26/23 15:21403 187 1
2-Nitrophenol ND ug/kg 04/27/23 13:19 88-75-504/26/23 15:21403 174 1
4-Nitrophenol ND ug/kg 04/27/23 13:19 100-02-704/26/23 15:212010 778 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 13:19 62-75-904/26/23 15:21403 135 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 13:19 621-64-704/26/23 15:21403 151 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 13:19 86-30-604/26/23 15:21403 143 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 13:19 108-60-104/26/23 15:21403 192 1
Pentachlorophenol ND ug/kg 04/27/23 13:19 87-86-504/26/23 15:21805 394 1
Phenanthrene ND ug/kg 04/27/23 13:19 85-01-804/26/23 15:21403 132 1
Phenol ND ug/kg 04/27/23 13:19 108-95-204/26/23 15:21403 179 1
Pyrene ND ug/kg 04/27/23 13:19 129-00-004/26/23 15:21403 163 1
Pyridine ND ug/kg 04/27/23 13:19 110-86-104/26/23 15:21403 127 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 13:19 120-82-104/26/23 15:21403 159 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 13:19 95-95-404/26/23 15:21403 184 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 13:19 88-06-204/26/23 15:21403 166 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-7 Lab ID: 92663594007 Collected: 04/17/23 16:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)58 %04/27/23 13:19 4165-60-004/26/23 15:2110-130 1
2-Fluorobiphenyl (S)54 %04/27/23 13:19 321-60-804/26/23 15:2110-130 1
Terphenyl-d14 (S)78 %04/27/23 13:19 1718-51-004/26/23 15:2110-130 1
Phenol-d6 (S)55 %04/27/23 13:19 13127-88-304/26/23 15:2110-130 1
2-Fluorophenol (S)53 %04/27/23 13:19 367-12-404/26/23 15:2110-130 1
2,4,6-Tribromophenol (S)66 %04/27/23 13:19 118-79-604/26/23 15:2110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 20:44 67-64-104/25/23 14:47208 66.6 1
Benzene ND ug/kg 04/25/23 20:44 71-43-204/25/23 14:4710.4 4.1 1
Bromobenzene ND ug/kg 04/25/23 20:44 108-86-104/25/23 14:4710.4 3.4 1
Bromochloromethane ND ug/kg 04/25/23 20:44 74-97-504/25/23 14:4710.4 3.1 1
Bromodichloromethane ND ug/kg 04/25/23 20:44 75-27-404/25/23 14:4710.4 4.0 1
Bromoform ND ug/kg 04/25/23 20:44 75-25-204/25/23 14:4710.4 3.7 1
Bromomethane ND ug/kg 04/25/23 20:44 74-83-9 IK04/25/23 14:4741.5 32.2 1
2-Butanone (MEK)ND ug/kg 04/25/23 20:44 78-93-304/25/23 14:47208 49.8 1
n-Butylbenzene ND ug/kg 04/25/23 20:44 104-51-804/25/23 14:4710.4 6.5 1
sec-Butylbenzene ND ug/kg 04/25/23 20:44 135-98-804/25/23 14:4710.4 4.6 1
tert-Butylbenzene ND ug/kg 04/25/23 20:44 98-06-604/25/23 14:4710.4 3.7 1
Carbon tetrachloride ND ug/kg 04/25/23 20:44 56-23-504/25/23 14:4710.4 3.9 1
Chlorobenzene ND ug/kg 04/25/23 20:44 108-90-704/25/23 14:4710.4 6.0 1
Chloroethane ND ug/kg 04/25/23 20:44 75-00-304/25/23 14:4720.8 8.0 1
Chloroform ND ug/kg 04/25/23 20:44 67-66-304/25/23 14:4710.4 8.7 1
Chloromethane ND ug/kg 04/25/23 20:44 74-87-304/25/23 14:4720.8 8.7 1
2-Chlorotoluene ND ug/kg 04/25/23 20:44 95-49-804/25/23 14:4710.4 3.7 1
4-Chlorotoluene ND ug/kg 04/25/23 20:44 106-43-404/25/23 14:4710.4 5.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 20:44 96-12-804/25/23 14:4710.4 4.0 1
Dibromochloromethane ND ug/kg 04/25/23 20:44 124-48-104/25/23 14:4710.4 5.8 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 20:44 106-93-404/25/23 14:4710.4 4.6 1
Dibromomethane ND ug/kg 04/25/23 20:44 74-95-304/25/23 14:4710.4 2.2 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 20:44 95-50-104/25/23 14:4710.4 3.7 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 20:44 541-73-104/25/23 14:4710.4 3.2 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 20:44 106-46-704/25/23 14:4710.4 2.7 1
Dichlorodifluoromethane ND ug/kg 04/25/23 20:44 75-71-804/25/23 14:4720.8 10.6 1
1,1-Dichloroethane ND ug/kg 04/25/23 20:44 75-34-304/25/23 14:4710.4 4.3 1
1,2-Dichloroethane ND ug/kg 04/25/23 20:44 107-06-204/25/23 14:4710.4 6.9 1
1,1-Dichloroethene ND ug/kg 04/25/23 20:44 75-35-404/25/23 14:4710.4 4.3 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 20:44 156-59-204/25/23 14:4710.4 3.5 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 20:44 156-60-504/25/23 14:4710.4 8.8 1
1,2-Dichloropropane ND ug/kg 04/25/23 20:44 78-87-504/25/23 14:4710.4 3.1 1
1,3-Dichloropropane ND ug/kg 04/25/23 20:44 142-28-904/25/23 14:4710.4 3.2 1
2,2-Dichloropropane ND ug/kg 04/25/23 20:44 594-20-7 v204/25/23 14:4710.4 7.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-7 Lab ID: 92663594007 Collected: 04/17/23 16:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 20:44 563-58-604/25/23 14:4710.4 5.0 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 20:44 10061-01-504/25/23 14:4710.4 2.8 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 20:44 10061-02-604/25/23 14:4710.4 3.6 1
Diisopropyl ether ND ug/kg 04/25/23 20:44 108-20-304/25/23 14:4710.4 2.8 1
Ethylbenzene ND ug/kg 04/25/23 20:44 100-41-404/25/23 14:4710.4 4.8 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 20:44 87-68-304/25/23 14:4720.8 17.0 1
2-Hexanone ND ug/kg 04/25/23 20:44 591-78-604/25/23 14:47104 10.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 20:44 98-82-804/25/23 14:4710.4 3.5 1
p-Isopropyltoluene ND ug/kg 04/25/23 20:44 99-87-604/25/23 14:4710.4 5.1 1
Methylene Chloride 47.1 ug/kg 04/25/23 20:44 75-09-2 C904/25/23 14:4741.5 28.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 20:44 108-10-104/25/23 14:47104 10.0 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 20:44 1634-04-4 v204/25/23 14:4710.4 3.9 1
Naphthalene ND ug/kg 04/25/23 20:44 91-20-304/25/23 14:4710.4 5.5 1
n-Propylbenzene ND ug/kg 04/25/23 20:44 103-65-104/25/23 14:4710.4 3.7 1
Styrene ND ug/kg 04/25/23 20:44 100-42-504/25/23 14:4710.4 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 20:44 630-20-604/25/23 14:4710.4 4.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 20:44 79-34-504/25/23 14:4710.4 2.7 1
Tetrachloroethene ND ug/kg 04/25/23 20:44 127-18-404/25/23 14:4710.4 3.3 1
Toluene ND ug/kg 04/25/23 20:44 108-88-304/25/23 14:4710.4 7.2 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 20:44 87-61-604/25/23 14:4710.4 8.4 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 20:44 120-82-104/25/23 14:4710.4 8.7 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 20:44 71-55-604/25/23 14:4710.4 5.4 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 20:44 79-00-504/25/23 14:4710.4 3.4 1
Trichloroethene ND ug/kg 04/25/23 20:44 79-01-604/25/23 14:4710.4 8.4 1
Trichlorofluoromethane ND ug/kg 04/25/23 20:44 75-69-404/25/23 14:4710.4 5.7 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 20:44 96-18-404/25/23 14:4710.4 5.3 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 20:44 95-63-604/25/23 14:4710.4 6.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 20:44 108-67-804/25/23 14:4710.4 3.5 1
Vinyl acetate ND ug/kg 04/25/23 20:44 108-05-404/25/23 14:47104 21.4 1
Vinyl chloride ND ug/kg 04/25/23 20:44 75-01-4 v204/25/23 14:4720.8 5.3 1
Xylene (Total)ND ug/kg 04/25/23 20:44 1330-20-704/25/23 14:4720.8 5.9 1
m&p-Xylene ND ug/kg 04/25/23 20:44 179601-23-104/25/23 14:4720.8 7.1 1
o-Xylene ND ug/kg 04/25/23 20:44 95-47-604/25/23 14:4710.4 4.6 1
Surrogates
Toluene-d8 (S)101 %04/25/23 20:44 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 20:44 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)97 %04/25/23 20:44 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.5 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-7 Lab ID: 92663594007 Collected: 04/17/23 16:45 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.1 %04/27/23 16:5904/27/23 16:441
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.577J mg/kg 05/01/23 14:24 18540-29-9 J04/30/23 06:541.20 0.307 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.42 mg/kg 04/27/23 19:15 57-12-504/26/23 17:140.30 0.15 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-8 Lab ID: 92663594008 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 17800 mg/kg 04/28/23 09:49 7429-90-504/26/23 11:0434.7 7.0 1
Arsenic 2.4 mg/kg 04/27/23 16:10 7440-38-204/26/23 11:040.58 0.17 1
Barium 43.7 mg/kg 04/27/23 16:10 7440-39-304/26/23 11:040.35 0.087 1
Cadmium 0.070J mg/kg 04/27/23 16:10 7440-43-904/26/23 11:040.092 0.034 1
Chromium 27.9 mg/kg 04/27/23 16:10 7440-47-304/26/23 11:042.3 0.45 1
Copper 22.0 mg/kg 04/27/23 16:10 7440-50-804/26/23 11:041.2 0.35 1
Lead 14.4 mg/kg 04/27/23 16:10 7439-92-104/26/23 11:040.58 0.11 1
Nickel 7.0 mg/kg 04/27/23 16:10 7440-02-004/26/23 11:040.58 0.27 1
Selenium 0.63 mg/kg 04/27/23 16:10 7782-49-204/26/23 11:040.58 0.12 1
Silver ND mg/kg 04/27/23 16:10 7440-22-404/26/23 11:040.58 0.24 1
Zinc 33.2 mg/kg 04/27/23 16:10 7440-66-604/26/23 11:045.8 1.4 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.026 mg/kg 04/28/23 09:15 7439-97-604/26/23 11:070.020 0.0089 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 15:38 83-32-904/26/23 15:38406 143 1
Acenaphthylene ND ug/kg 04/27/23 15:38 208-96-804/26/23 15:38406 143 1
Aniline ND ug/kg 04/27/23 15:38 62-53-304/26/23 15:38406 159 1
Anthracene ND ug/kg 04/27/23 15:38 120-12-704/26/23 15:38406 133 1
Benzo(a)anthracene 167J ug/kg 04/27/23 15:38 56-55-304/26/23 15:38406 135 1
Benzo(a)pyrene 146J ug/kg 04/27/23 15:38 50-32-804/26/23 15:38406 140 1
Benzo(b)fluoranthene 209J ug/kg 04/27/23 15:38 205-99-204/26/23 15:38406 135 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 15:38 191-24-204/26/23 15:38406 158 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 15:38 207-08-904/26/23 15:38406 143 1
Benzoic Acid ND ug/kg 04/27/23 15:38 65-85-004/26/23 15:382030 873 1
Benzyl alcohol ND ug/kg 04/27/23 15:38 100-51-604/26/23 15:38812 308 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 15:38 101-55-304/26/23 15:38406 156 1
Butylbenzylphthalate ND ug/kg 04/27/23 15:38 85-68-704/26/23 15:38406 171 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 15:38 59-50-704/26/23 15:38812 286 1
4-Chloroaniline ND ug/kg 04/27/23 15:38 106-47-804/26/23 15:38812 319 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 15:38 111-91-104/26/23 15:38406 169 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 15:38 111-44-404/26/23 15:38406 153 1
2-Chloronaphthalene ND ug/kg 04/27/23 15:38 91-58-704/26/23 15:38406 161 1
2-Chlorophenol ND ug/kg 04/27/23 15:38 95-57-804/26/23 15:38406 153 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 15:38 7005-72-304/26/23 15:38406 151 1
Chrysene 168J ug/kg 04/27/23 15:38 218-01-904/26/23 15:38406 148 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 15:38 53-70-304/26/23 15:38406 156 1
Dibenzofuran ND ug/kg 04/27/23 15:38 132-64-904/26/23 15:38406 146 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 15:38 95-50-104/26/23 15:38406 146 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 15:38 541-73-104/26/23 15:38406 144 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 15:38 106-46-7 L204/26/23 15:38406 155 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-8 Lab ID: 92663594008 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 15:38 91-94-104/26/23 15:38812 274 1
2,4-Dichlorophenol ND ug/kg 04/27/23 15:38 120-83-204/26/23 15:38406 159 1
Diethylphthalate ND ug/kg 04/27/23 15:38 84-66-204/26/23 15:38406 149 1
2,4-Dimethylphenol ND ug/kg 04/27/23 15:38 105-67-904/26/23 15:38406 169 1
Dimethylphthalate ND ug/kg 04/27/23 15:38 131-11-304/26/23 15:38406 148 1
Di-n-butylphthalate ND ug/kg 04/27/23 15:38 84-74-204/26/23 15:38406 137 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 15:38 534-52-104/26/23 15:38812 379 1
2,4-Dinitrophenol ND ug/kg 04/27/23 15:38 51-28-504/26/23 15:382030 1260 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 15:38 121-14-204/26/23 15:38406 156 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 15:38 606-20-204/26/23 15:38406 149 1
Di-n-octylphthalate ND ug/kg 04/27/23 15:38 117-84-004/26/23 15:38406 160 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 15:38 117-81-704/26/23 15:38406 158 1
Fluoranthene 255J ug/kg 04/27/23 15:38 206-44-004/26/23 15:38406 139 1
Fluorene ND ug/kg 04/27/23 15:38 86-73-704/26/23 15:38406 143 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 15:38 87-68-304/26/23 15:38406 176 1
Hexachlorobenzene ND ug/kg 04/27/23 15:38 118-74-104/26/23 15:38406 159 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 15:38 77-47-404/26/23 15:38406 233 1
Hexachloroethane ND ug/kg 04/27/23 15:38 67-72-104/26/23 15:38406 155 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 15:38 193-39-504/26/23 15:38406 160 1
Isophorone ND ug/kg 04/27/23 15:38 78-59-104/26/23 15:38406 181 1
1-Methylnaphthalene ND ug/kg 04/27/23 15:38 90-12-004/26/23 15:38406 143 1
2-Methylnaphthalene ND ug/kg 04/27/23 15:38 91-57-604/26/23 15:38406 162 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 15:38 95-48-704/26/23 15:38406 166 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 15:38 15831-10-404/26/23 15:38406 164 1
Naphthalene ND ug/kg 04/27/23 15:38 91-20-304/26/23 15:38406 138 1
2-Nitroaniline ND ug/kg 04/27/23 15:38 88-74-404/26/23 15:382030 332 1
3-Nitroaniline ND ug/kg 04/27/23 15:38 99-09-204/26/23 15:382030 319 1
4-Nitroaniline ND ug/kg 04/27/23 15:38 100-01-604/26/23 15:38812 309 1
Nitrobenzene ND ug/kg 04/27/23 15:38 98-95-304/26/23 15:38406 188 1
2-Nitrophenol ND ug/kg 04/27/23 15:38 88-75-504/26/23 15:38406 176 1
4-Nitrophenol ND ug/kg 04/27/23 15:38 100-02-704/26/23 15:382030 785 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 15:38 62-75-904/26/23 15:38406 137 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 15:38 621-64-704/26/23 15:38406 153 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 15:38 86-30-604/26/23 15:38406 144 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 15:38 108-60-104/26/23 15:38406 193 1
Pentachlorophenol ND ug/kg 04/27/23 15:38 87-86-504/26/23 15:38812 398 1
Phenanthrene 148J ug/kg 04/27/23 15:38 85-01-804/26/23 15:38406 133 1
Phenol ND ug/kg 04/27/23 15:38 108-95-204/26/23 15:38406 181 1
Pyrene 255J ug/kg 04/27/23 15:38 129-00-004/26/23 15:38406 165 1
Pyridine ND ug/kg 04/27/23 15:38 110-86-104/26/23 15:38406 128 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 15:38 120-82-104/26/23 15:38406 160 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 15:38 95-95-404/26/23 15:38406 186 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 15:38 88-06-204/26/23 15:38406 167 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-8 Lab ID: 92663594008 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)66 %04/27/23 15:38 4165-60-004/26/23 15:3810-130 1
2-Fluorobiphenyl (S)68 %04/27/23 15:38 321-60-804/26/23 15:3810-130 1
Terphenyl-d14 (S)86 %04/27/23 15:38 1718-51-004/26/23 15:3810-130 1
Phenol-d6 (S)58 %04/27/23 15:38 13127-88-304/26/23 15:3810-130 1
2-Fluorophenol (S)58 %04/27/23 15:38 367-12-404/26/23 15:3810-130 1
2,4,6-Tribromophenol (S)76 %04/27/23 15:38 118-79-604/26/23 15:3810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 21:02 67-64-104/25/23 14:47229 73.4 1
Benzene ND ug/kg 04/25/23 21:02 71-43-204/25/23 14:4711.4 4.6 1
Bromobenzene ND ug/kg 04/25/23 21:02 108-86-104/25/23 14:4711.4 3.7 1
Bromochloromethane ND ug/kg 04/25/23 21:02 74-97-504/25/23 14:4711.4 3.4 1
Bromodichloromethane ND ug/kg 04/25/23 21:02 75-27-404/25/23 14:4711.4 4.4 1
Bromoform ND ug/kg 04/25/23 21:02 75-25-204/25/23 14:4711.4 4.0 1
Bromomethane ND ug/kg 04/25/23 21:02 74-83-9 IK04/25/23 14:4745.8 35.5 1
2-Butanone (MEK)ND ug/kg 04/25/23 21:02 78-93-304/25/23 14:47229 54.9 1
n-Butylbenzene ND ug/kg 04/25/23 21:02 104-51-804/25/23 14:4711.4 7.2 1
sec-Butylbenzene ND ug/kg 04/25/23 21:02 135-98-804/25/23 14:4711.4 5.0 1
tert-Butylbenzene ND ug/kg 04/25/23 21:02 98-06-604/25/23 14:4711.4 4.1 1
Carbon tetrachloride ND ug/kg 04/25/23 21:02 56-23-504/25/23 14:4711.4 4.3 1
Chlorobenzene ND ug/kg 04/25/23 21:02 108-90-704/25/23 14:4711.4 6.6 1
Chloroethane ND ug/kg 04/25/23 21:02 75-00-304/25/23 14:4722.9 8.8 1
Chloroform ND ug/kg 04/25/23 21:02 67-66-304/25/23 14:4711.4 9.6 1
Chloromethane ND ug/kg 04/25/23 21:02 74-87-304/25/23 14:4722.9 9.6 1
2-Chlorotoluene ND ug/kg 04/25/23 21:02 95-49-804/25/23 14:4711.4 4.0 1
4-Chlorotoluene ND ug/kg 04/25/23 21:02 106-43-404/25/23 14:4711.4 6.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 21:02 96-12-804/25/23 14:4711.4 4.4 1
Dibromochloromethane ND ug/kg 04/25/23 21:02 124-48-104/25/23 14:4711.4 6.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 21:02 106-93-404/25/23 14:4711.4 5.0 1
Dibromomethane ND ug/kg 04/25/23 21:02 74-95-304/25/23 14:4711.4 2.4 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 21:02 95-50-104/25/23 14:4711.4 4.1 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 21:02 541-73-104/25/23 14:4711.4 3.5 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 21:02 106-46-704/25/23 14:4711.4 3.0 1
Dichlorodifluoromethane ND ug/kg 04/25/23 21:02 75-71-804/25/23 14:4722.9 11.6 1
1,1-Dichloroethane ND ug/kg 04/25/23 21:02 75-34-304/25/23 14:4711.4 4.7 1
1,2-Dichloroethane ND ug/kg 04/25/23 21:02 107-06-204/25/23 14:4711.4 7.6 1
1,1-Dichloroethene ND ug/kg 04/25/23 21:02 75-35-404/25/23 14:4711.4 4.7 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 21:02 156-59-204/25/23 14:4711.4 3.9 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 21:02 156-60-504/25/23 14:4711.4 9.7 1
1,2-Dichloropropane ND ug/kg 04/25/23 21:02 78-87-504/25/23 14:4711.4 3.4 1
1,3-Dichloropropane ND ug/kg 04/25/23 21:02 142-28-904/25/23 14:4711.4 3.6 1
2,2-Dichloropropane ND ug/kg 04/25/23 21:02 594-20-7 v204/25/23 14:4711.4 8.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-8 Lab ID: 92663594008 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 21:02 563-58-604/25/23 14:4711.4 5.5 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 21:02 10061-01-504/25/23 14:4711.4 3.1 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 21:02 10061-02-604/25/23 14:4711.4 3.9 1
Diisopropyl ether ND ug/kg 04/25/23 21:02 108-20-304/25/23 14:4711.4 3.1 1
Ethylbenzene ND ug/kg 04/25/23 21:02 100-41-404/25/23 14:4711.4 5.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 21:02 87-68-304/25/23 14:4722.9 18.7 1
2-Hexanone ND ug/kg 04/25/23 21:02 591-78-604/25/23 14:47114 11.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 21:02 98-82-804/25/23 14:4711.4 3.9 1
p-Isopropyltoluene ND ug/kg 04/25/23 21:02 99-87-604/25/23 14:4711.4 5.6 1
Methylene Chloride 41.6J ug/kg 04/25/23 21:02 75-09-2 C904/25/23 14:4745.8 31.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 21:02 108-10-104/25/23 14:47114 11.0 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 21:02 1634-04-4 v204/25/23 14:4711.4 4.3 1
Naphthalene ND ug/kg 04/25/23 21:02 91-20-304/25/23 14:4711.4 6.0 1
n-Propylbenzene ND ug/kg 04/25/23 21:02 103-65-104/25/23 14:4711.4 4.1 1
Styrene ND ug/kg 04/25/23 21:02 100-42-504/25/23 14:4711.4 3.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 21:02 630-20-604/25/23 14:4711.4 4.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 21:02 79-34-504/25/23 14:4711.4 3.0 1
Tetrachloroethene ND ug/kg 04/25/23 21:02 127-18-404/25/23 14:4711.4 3.6 1
Toluene ND ug/kg 04/25/23 21:02 108-88-304/25/23 14:4711.4 7.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 21:02 87-61-604/25/23 14:4711.4 9.2 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 21:02 120-82-104/25/23 14:4711.4 9.6 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 21:02 71-55-604/25/23 14:4711.4 5.9 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 21:02 79-00-504/25/23 14:4711.4 3.8 1
Trichloroethene ND ug/kg 04/25/23 21:02 79-01-604/25/23 14:4711.4 9.2 1
Trichlorofluoromethane ND ug/kg 04/25/23 21:02 75-69-404/25/23 14:4711.4 6.3 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 21:02 96-18-404/25/23 14:4711.4 5.8 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 21:02 95-63-604/25/23 14:4711.4 6.8 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 21:02 108-67-804/25/23 14:4711.4 3.8 1
Vinyl acetate ND ug/kg 04/25/23 21:02 108-05-404/25/23 14:47114 23.5 1
Vinyl chloride ND ug/kg 04/25/23 21:02 75-01-4 v204/25/23 14:4722.9 5.8 1
Xylene (Total)ND ug/kg 04/25/23 21:02 1330-20-704/25/23 14:4722.9 6.5 1
m&p-Xylene ND ug/kg 04/25/23 21:02 179601-23-104/25/23 14:4722.9 7.8 1
o-Xylene ND ug/kg 04/25/23 21:02 95-47-604/25/23 14:4711.4 5.1 1
Surrogates
Toluene-d8 (S)100 %04/25/23 21:02 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 21:02 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)98 %04/25/23 21:02 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.2 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-8 Lab ID: 92663594008 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 68.3 %04/27/23 16:5904/27/23 16:441
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 2.30 mg/kg 05/01/23 14:29 18540-29-904/30/23 06:541.46 0.373 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.27J mg/kg 04/27/23 19:16 57-12-504/26/23 17:140.37 0.18 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-9 Lab ID: 92663594009 Collected: 04/20/23 17:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 24100 mg/kg 04/28/23 09:52 7429-90-504/26/23 11:0439.4 8.0 1
Arsenic 2.3 mg/kg 04/27/23 16:13 7440-38-204/26/23 11:040.66 0.19 1
Barium 100 mg/kg 04/27/23 16:13 7440-39-304/26/23 11:040.39 0.099 1
Cadmium 0.17 mg/kg 04/27/23 16:13 7440-43-904/26/23 11:040.11 0.039 1
Chromium 73.2 mg/kg 04/27/23 16:13 7440-47-304/26/23 11:042.6 0.51 1
Copper 46.5 mg/kg 04/27/23 16:13 7440-50-804/26/23 11:041.3 0.40 1
Lead 21.9 mg/kg 04/27/23 16:13 7439-92-104/26/23 11:040.66 0.12 1
Nickel 20.2 mg/kg 04/27/23 16:13 7440-02-004/26/23 11:040.66 0.30 1
Selenium 0.62J mg/kg 04/27/23 16:13 7782-49-204/26/23 11:040.66 0.14 1
Silver ND mg/kg 04/27/23 16:13 7440-22-404/26/23 11:040.66 0.27 1
Zinc 37.5 mg/kg 04/27/23 16:13 7440-66-604/26/23 11:046.6 1.5 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.047 mg/kg 04/28/23 09:17 7439-97-604/26/23 11:070.023 0.0098 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 16:05 83-32-904/26/23 15:38437 154 1
Acenaphthylene ND ug/kg 04/27/23 16:05 208-96-804/26/23 15:38437 154 1
Aniline ND ug/kg 04/27/23 16:05 62-53-304/26/23 15:38437 171 1
Anthracene ND ug/kg 04/27/23 16:05 120-12-704/26/23 15:38437 143 1
Benzo(a)anthracene ND ug/kg 04/27/23 16:05 56-55-304/26/23 15:38437 146 1
Benzo(a)pyrene ND ug/kg 04/27/23 16:05 50-32-804/26/23 15:38437 151 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 16:05 205-99-204/26/23 15:38437 146 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 16:05 191-24-204/26/23 15:38437 170 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 16:05 207-08-904/26/23 15:38437 154 1
Benzoic Acid ND ug/kg 04/27/23 16:05 65-85-004/26/23 15:382190 940 1
Benzyl alcohol ND ug/kg 04/27/23 16:05 100-51-604/26/23 15:38875 331 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 16:05 101-55-304/26/23 15:38437 168 1
Butylbenzylphthalate ND ug/kg 04/27/23 16:05 85-68-704/26/23 15:38437 184 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 16:05 59-50-704/26/23 15:38875 307 1
4-Chloroaniline ND ug/kg 04/27/23 16:05 106-47-804/26/23 15:38875 343 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 16:05 111-91-104/26/23 15:38437 182 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 16:05 111-44-404/26/23 15:38437 164 1
2-Chloronaphthalene ND ug/kg 04/27/23 16:05 91-58-704/26/23 15:38437 174 1
2-Chlorophenol ND ug/kg 04/27/23 16:05 95-57-804/26/23 15:38437 164 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 16:05 7005-72-304/26/23 15:38437 163 1
Chrysene ND ug/kg 04/27/23 16:05 218-01-904/26/23 15:38437 159 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 16:05 53-70-304/26/23 15:38437 168 1
Dibenzofuran ND ug/kg 04/27/23 16:05 132-64-904/26/23 15:38437 158 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 16:05 95-50-104/26/23 15:38437 158 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 16:05 541-73-104/26/23 15:38437 155 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 16:05 106-46-7 L204/26/23 15:38437 167 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-9 Lab ID: 92663594009 Collected: 04/20/23 17:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 16:05 91-94-104/26/23 15:38875 296 1
2,4-Dichlorophenol ND ug/kg 04/27/23 16:05 120-83-204/26/23 15:38437 171 1
Diethylphthalate ND ug/kg 04/27/23 16:05 84-66-204/26/23 15:38437 160 1
2,4-Dimethylphenol ND ug/kg 04/27/23 16:05 105-67-904/26/23 15:38437 182 1
Dimethylphthalate ND ug/kg 04/27/23 16:05 131-11-304/26/23 15:38437 159 1
Di-n-butylphthalate ND ug/kg 04/27/23 16:05 84-74-204/26/23 15:38437 147 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 16:05 534-52-104/26/23 15:38875 408 1
2,4-Dinitrophenol ND ug/kg 04/27/23 16:05 51-28-504/26/23 15:382190 1350 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 16:05 121-14-204/26/23 15:38437 168 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 16:05 606-20-204/26/23 15:38437 160 1
Di-n-octylphthalate ND ug/kg 04/27/23 16:05 117-84-004/26/23 15:38437 172 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 16:05 117-81-704/26/23 15:38437 170 1
Fluoranthene 176J ug/kg 04/27/23 16:05 206-44-004/26/23 15:38437 150 1
Fluorene ND ug/kg 04/27/23 16:05 86-73-704/26/23 15:38437 154 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 16:05 87-68-304/26/23 15:38437 190 1
Hexachlorobenzene ND ug/kg 04/27/23 16:05 118-74-104/26/23 15:38437 171 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 16:05 77-47-404/26/23 15:38437 250 1
Hexachloroethane ND ug/kg 04/27/23 16:05 67-72-104/26/23 15:38437 167 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 16:05 193-39-504/26/23 15:38437 172 1
Isophorone ND ug/kg 04/27/23 16:05 78-59-104/26/23 15:38437 195 1
1-Methylnaphthalene ND ug/kg 04/27/23 16:05 90-12-004/26/23 15:38437 154 1
2-Methylnaphthalene ND ug/kg 04/27/23 16:05 91-57-604/26/23 15:38437 175 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 16:05 95-48-704/26/23 15:38437 179 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 16:05 15831-10-404/26/23 15:38437 176 1
Naphthalene ND ug/kg 04/27/23 16:05 91-20-304/26/23 15:38437 148 1
2-Nitroaniline ND ug/kg 04/27/23 16:05 88-74-404/26/23 15:382190 358 1
3-Nitroaniline ND ug/kg 04/27/23 16:05 99-09-204/26/23 15:382190 343 1
4-Nitroaniline ND ug/kg 04/27/23 16:05 100-01-604/26/23 15:38875 333 1
Nitrobenzene ND ug/kg 04/27/23 16:05 98-95-304/26/23 15:38437 203 1
2-Nitrophenol ND ug/kg 04/27/23 16:05 88-75-504/26/23 15:38437 190 1
4-Nitrophenol ND ug/kg 04/27/23 16:05 100-02-704/26/23 15:382190 845 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 16:05 62-75-904/26/23 15:38437 147 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 16:05 621-64-704/26/23 15:38437 164 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 16:05 86-30-604/26/23 15:38437 155 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 16:05 108-60-104/26/23 15:38437 208 1
Pentachlorophenol ND ug/kg 04/27/23 16:05 87-86-504/26/23 15:38875 428 1
Phenanthrene 156J ug/kg 04/27/23 16:05 85-01-804/26/23 15:38437 143 1
Phenol ND ug/kg 04/27/23 16:05 108-95-204/26/23 15:38437 195 1
Pyrene ND ug/kg 04/27/23 16:05 129-00-004/26/23 15:38437 178 1
Pyridine ND ug/kg 04/27/23 16:05 110-86-104/26/23 15:38437 138 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 16:05 120-82-104/26/23 15:38437 172 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 16:05 95-95-404/26/23 15:38437 200 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 16:05 88-06-204/26/23 15:38437 180 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-9 Lab ID: 92663594009 Collected: 04/20/23 17:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)67 %04/27/23 16:05 4165-60-004/26/23 15:3810-130 1
2-Fluorobiphenyl (S)70 %04/27/23 16:05 321-60-804/26/23 15:3810-130 1
Terphenyl-d14 (S)83 %04/27/23 16:05 1718-51-004/26/23 15:3810-130 1
Phenol-d6 (S)60 %04/27/23 16:05 13127-88-304/26/23 15:3810-130 1
2-Fluorophenol (S)59 %04/27/23 16:05 367-12-404/26/23 15:3810-130 1
2,4,6-Tribromophenol (S)69 %04/27/23 16:05 118-79-604/26/23 15:3810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 21:20 67-64-104/25/23 14:47142 45.6 1
Benzene ND ug/kg 04/25/23 21:20 71-43-204/25/23 14:477.1 2.8 1
Bromobenzene ND ug/kg 04/25/23 21:20 108-86-104/25/23 14:477.1 2.3 1
Bromochloromethane ND ug/kg 04/25/23 21:20 74-97-504/25/23 14:477.1 2.1 1
Bromodichloromethane ND ug/kg 04/25/23 21:20 75-27-404/25/23 14:477.1 2.7 1
Bromoform ND ug/kg 04/25/23 21:20 75-25-204/25/23 14:477.1 2.5 1
Bromomethane ND ug/kg 04/25/23 21:20 74-83-9 IK04/25/23 14:4728.4 22.0 1
2-Butanone (MEK)ND ug/kg 04/25/23 21:20 78-93-304/25/23 14:47142 34.1 1
n-Butylbenzene ND ug/kg 04/25/23 21:20 104-51-804/25/23 14:477.1 4.5 1
sec-Butylbenzene ND ug/kg 04/25/23 21:20 135-98-804/25/23 14:477.1 3.1 1
tert-Butylbenzene ND ug/kg 04/25/23 21:20 98-06-604/25/23 14:477.1 2.5 1
Carbon tetrachloride ND ug/kg 04/25/23 21:20 56-23-504/25/23 14:477.1 2.7 1
Chlorobenzene ND ug/kg 04/25/23 21:20 108-90-704/25/23 14:477.1 4.1 1
Chloroethane ND ug/kg 04/25/23 21:20 75-00-304/25/23 14:4714.2 5.5 1
Chloroform ND ug/kg 04/25/23 21:20 67-66-304/25/23 14:477.1 5.9 1
Chloromethane ND ug/kg 04/25/23 21:20 74-87-304/25/23 14:4714.2 6.0 1
2-Chlorotoluene ND ug/kg 04/25/23 21:20 95-49-804/25/23 14:477.1 2.5 1
4-Chlorotoluene ND ug/kg 04/25/23 21:20 106-43-404/25/23 14:477.1 4.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 21:20 96-12-804/25/23 14:477.1 2.8 1
Dibromochloromethane ND ug/kg 04/25/23 21:20 124-48-104/25/23 14:477.1 4.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 21:20 106-93-404/25/23 14:477.1 3.1 1
Dibromomethane ND ug/kg 04/25/23 21:20 74-95-304/25/23 14:477.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 21:20 95-50-104/25/23 14:477.1 2.6 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 21:20 541-73-104/25/23 14:477.1 2.2 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 21:20 106-46-704/25/23 14:477.1 1.8 1
Dichlorodifluoromethane ND ug/kg 04/25/23 21:20 75-71-804/25/23 14:4714.2 7.2 1
1,1-Dichloroethane ND ug/kg 04/25/23 21:20 75-34-304/25/23 14:477.1 2.9 1
1,2-Dichloroethane ND ug/kg 04/25/23 21:20 107-06-204/25/23 14:477.1 4.7 1
1,1-Dichloroethene ND ug/kg 04/25/23 21:20 75-35-404/25/23 14:477.1 2.9 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 21:20 156-59-204/25/23 14:477.1 2.4 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 21:20 156-60-504/25/23 14:477.1 6.0 1
1,2-Dichloropropane ND ug/kg 04/25/23 21:20 78-87-504/25/23 14:477.1 2.1 1
1,3-Dichloropropane ND ug/kg 04/25/23 21:20 142-28-904/25/23 14:477.1 2.2 1
2,2-Dichloropropane ND ug/kg 04/25/23 21:20 594-20-7 v204/25/23 14:477.1 5.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-9 Lab ID: 92663594009 Collected: 04/20/23 17:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 21:20 563-58-604/25/23 14:477.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 21:20 10061-01-504/25/23 14:477.1 1.9 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 21:20 10061-02-604/25/23 14:477.1 2.4 1
Diisopropyl ether ND ug/kg 04/25/23 21:20 108-20-304/25/23 14:477.1 1.9 1
Ethylbenzene ND ug/kg 04/25/23 21:20 100-41-404/25/23 14:477.1 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 21:20 87-68-304/25/23 14:4714.2 11.6 1
2-Hexanone ND ug/kg 04/25/23 21:20 591-78-604/25/23 14:4771.1 6.9 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 21:20 98-82-804/25/23 14:477.1 2.4 1
p-Isopropyltoluene ND ug/kg 04/25/23 21:20 99-87-604/25/23 14:477.1 3.5 1
Methylene Chloride 32.0 ug/kg 04/25/23 21:20 75-09-2 C904/25/23 14:4728.4 19.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 21:20 108-10-104/25/23 14:4771.1 6.9 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 21:20 1634-04-4 v204/25/23 14:477.1 2.7 1
Naphthalene ND ug/kg 04/25/23 21:20 91-20-304/25/23 14:477.1 3.7 1
n-Propylbenzene ND ug/kg 04/25/23 21:20 103-65-104/25/23 14:477.1 2.5 1
Styrene ND ug/kg 04/25/23 21:20 100-42-504/25/23 14:477.1 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 21:20 630-20-604/25/23 14:477.1 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 21:20 79-34-504/25/23 14:477.1 1.9 1
Tetrachloroethene ND ug/kg 04/25/23 21:20 127-18-404/25/23 14:477.1 2.2 1
Toluene ND ug/kg 04/25/23 21:20 108-88-304/25/23 14:477.1 4.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 21:20 87-61-604/25/23 14:477.1 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 21:20 120-82-104/25/23 14:477.1 6.0 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 21:20 71-55-604/25/23 14:477.1 3.7 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 21:20 79-00-504/25/23 14:477.1 2.4 1
Trichloroethene ND ug/kg 04/25/23 21:20 79-01-604/25/23 14:477.1 5.7 1
Trichlorofluoromethane ND ug/kg 04/25/23 21:20 75-69-404/25/23 14:477.1 3.9 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 21:20 96-18-404/25/23 14:477.1 3.6 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 21:20 95-63-604/25/23 14:477.1 4.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 21:20 108-67-804/25/23 14:477.1 2.4 1
Vinyl acetate ND ug/kg 04/25/23 21:20 108-05-404/25/23 14:4771.1 14.6 1
Vinyl chloride ND ug/kg 04/25/23 21:20 75-01-4 v204/25/23 14:4714.2 3.6 1
Xylene (Total)ND ug/kg 04/25/23 21:20 1330-20-704/25/23 14:4714.2 4.1 1
m&p-Xylene ND ug/kg 04/25/23 21:20 179601-23-104/25/23 14:4714.2 4.9 1
o-Xylene ND ug/kg 04/25/23 21:20 95-47-604/25/23 14:477.1 3.1 1
Surrogates
Toluene-d8 (S)99 %04/25/23 21:20 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 21:20 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)97 %04/25/23 21:20 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.5 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-9 Lab ID: 92663594009 Collected: 04/20/23 17:30 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.8 %04/27/23 17:1504/27/23 17:001
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.38 mg/kg 05/01/23 14:35 18540-29-904/30/23 06:541.27 0.323 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.26J mg/kg 04/27/23 19:16 57-12-504/26/23 17:140.40 0.20 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-11 Lab ID: 92663594010 Collected: 04/17/23 13:20 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 18900 mg/kg 04/28/23 10:01 7429-90-504/26/23 11:0437.9 7.7 1
Arsenic 2.4 mg/kg 04/27/23 16:16 7440-38-204/26/23 11:040.63 0.18 1
Barium 22.1 mg/kg 04/27/23 16:16 7440-39-304/26/23 11:040.38 0.095 1
Cadmium ND mg/kg 04/27/23 16:16 7440-43-904/26/23 11:040.10 0.037 1
Chromium 80.6 mg/kg 04/27/23 16:16 7440-47-304/26/23 11:042.5 0.49 1
Copper 27.8 mg/kg 04/27/23 16:16 7440-50-804/26/23 11:041.3 0.39 1
Lead 9.7 mg/kg 04/27/23 16:16 7439-92-104/26/23 11:040.63 0.12 1
Nickel 10.3 mg/kg 04/27/23 16:16 7440-02-004/26/23 11:040.63 0.29 1
Selenium 0.63J mg/kg 04/27/23 16:16 7782-49-204/26/23 11:040.63 0.13 1
Silver ND mg/kg 04/27/23 16:16 7440-22-404/26/23 11:040.63 0.26 1
Zinc 20.4 mg/kg 04/27/23 16:16 7440-66-604/26/23 11:046.3 1.5 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.027 mg/kg 04/28/23 09:18 7439-97-604/26/23 11:070.021 0.0093 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 16:33 83-32-904/26/23 15:38422 148 1
Acenaphthylene ND ug/kg 04/27/23 16:33 208-96-804/26/23 15:38422 148 1
Aniline ND ug/kg 04/27/23 16:33 62-53-304/26/23 15:38422 165 1
Anthracene ND ug/kg 04/27/23 16:33 120-12-704/26/23 15:38422 138 1
Benzo(a)anthracene ND ug/kg 04/27/23 16:33 56-55-304/26/23 15:38422 141 1
Benzo(a)pyrene ND ug/kg 04/27/23 16:33 50-32-804/26/23 15:38422 146 1
Benzo(b)fluoranthene ND ug/kg 04/27/23 16:33 205-99-204/26/23 15:38422 141 1
Benzo(g,h,i)perylene ND ug/kg 04/27/23 16:33 191-24-204/26/23 15:38422 164 1
Benzo(k)fluoranthene ND ug/kg 04/27/23 16:33 207-08-904/26/23 15:38422 148 1
Benzoic Acid ND ug/kg 04/27/23 16:33 65-85-004/26/23 15:382110 906 1
Benzyl alcohol ND ug/kg 04/27/23 16:33 100-51-604/26/23 15:38843 319 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 16:33 101-55-304/26/23 15:38422 162 1
Butylbenzylphthalate ND ug/kg 04/27/23 16:33 85-68-704/26/23 15:38422 178 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 16:33 59-50-704/26/23 15:38843 296 1
4-Chloroaniline ND ug/kg 04/27/23 16:33 106-47-804/26/23 15:38843 331 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 16:33 111-91-104/26/23 15:38422 175 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 16:33 111-44-404/26/23 15:38422 158 1
2-Chloronaphthalene ND ug/kg 04/27/23 16:33 91-58-704/26/23 15:38422 167 1
2-Chlorophenol ND ug/kg 04/27/23 16:33 95-57-804/26/23 15:38422 158 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 16:33 7005-72-304/26/23 15:38422 157 1
Chrysene ND ug/kg 04/27/23 16:33 218-01-904/26/23 15:38422 153 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 16:33 53-70-304/26/23 15:38422 162 1
Dibenzofuran ND ug/kg 04/27/23 16:33 132-64-904/26/23 15:38422 152 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 16:33 95-50-104/26/23 15:38422 152 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 16:33 541-73-104/26/23 15:38422 149 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 16:33 106-46-7 L204/26/23 15:38422 161 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-11 Lab ID: 92663594010 Collected: 04/17/23 13:20 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 16:33 91-94-104/26/23 15:38843 285 1
2,4-Dichlorophenol ND ug/kg 04/27/23 16:33 120-83-204/26/23 15:38422 165 1
Diethylphthalate ND ug/kg 04/27/23 16:33 84-66-204/26/23 15:38422 155 1
2,4-Dimethylphenol ND ug/kg 04/27/23 16:33 105-67-904/26/23 15:38422 175 1
Dimethylphthalate ND ug/kg 04/27/23 16:33 131-11-304/26/23 15:38422 153 1
Di-n-butylphthalate ND ug/kg 04/27/23 16:33 84-74-204/26/23 15:38422 142 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 16:33 534-52-104/26/23 15:38843 394 1
2,4-Dinitrophenol ND ug/kg 04/27/23 16:33 51-28-504/26/23 15:382110 1300 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 16:33 121-14-204/26/23 15:38422 162 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 16:33 606-20-204/26/23 15:38422 155 1
Di-n-octylphthalate ND ug/kg 04/27/23 16:33 117-84-004/26/23 15:38422 166 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 16:33 117-81-704/26/23 15:38422 164 1
Fluoranthene ND ug/kg 04/27/23 16:33 206-44-004/26/23 15:38422 144 1
Fluorene ND ug/kg 04/27/23 16:33 86-73-704/26/23 15:38422 148 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 16:33 87-68-304/26/23 15:38422 183 1
Hexachlorobenzene ND ug/kg 04/27/23 16:33 118-74-104/26/23 15:38422 165 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 16:33 77-47-404/26/23 15:38422 241 1
Hexachloroethane ND ug/kg 04/27/23 16:33 67-72-104/26/23 15:38422 161 1
Indeno(1,2,3-cd)pyrene ND ug/kg 04/27/23 16:33 193-39-504/26/23 15:38422 166 1
Isophorone ND ug/kg 04/27/23 16:33 78-59-104/26/23 15:38422 188 1
1-Methylnaphthalene ND ug/kg 04/27/23 16:33 90-12-004/26/23 15:38422 148 1
2-Methylnaphthalene ND ug/kg 04/27/23 16:33 91-57-604/26/23 15:38422 169 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 16:33 95-48-704/26/23 15:38422 172 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 16:33 15831-10-404/26/23 15:38422 170 1
Naphthalene ND ug/kg 04/27/23 16:33 91-20-304/26/23 15:38422 143 1
2-Nitroaniline ND ug/kg 04/27/23 16:33 88-74-404/26/23 15:382110 345 1
3-Nitroaniline ND ug/kg 04/27/23 16:33 99-09-204/26/23 15:382110 331 1
4-Nitroaniline ND ug/kg 04/27/23 16:33 100-01-604/26/23 15:38843 321 1
Nitrobenzene ND ug/kg 04/27/23 16:33 98-95-304/26/23 15:38422 195 1
2-Nitrophenol ND ug/kg 04/27/23 16:33 88-75-504/26/23 15:38422 183 1
4-Nitrophenol ND ug/kg 04/27/23 16:33 100-02-704/26/23 15:382110 815 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 16:33 62-75-904/26/23 15:38422 142 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 16:33 621-64-704/26/23 15:38422 158 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 16:33 86-30-604/26/23 15:38422 149 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 16:33 108-60-104/26/23 15:38422 201 1
Pentachlorophenol ND ug/kg 04/27/23 16:33 87-86-504/26/23 15:38843 413 1
Phenanthrene ND ug/kg 04/27/23 16:33 85-01-804/26/23 15:38422 138 1
Phenol ND ug/kg 04/27/23 16:33 108-95-204/26/23 15:38422 188 1
Pyrene ND ug/kg 04/27/23 16:33 129-00-004/26/23 15:38422 171 1
Pyridine ND ug/kg 04/27/23 16:33 110-86-104/26/23 15:38422 133 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 16:33 120-82-104/26/23 15:38422 166 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 16:33 95-95-404/26/23 15:38422 193 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 16:33 88-06-204/26/23 15:38422 174 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-11 Lab ID: 92663594010 Collected: 04/17/23 13:20 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)66 %04/27/23 16:33 4165-60-004/26/23 15:3810-130 1
2-Fluorobiphenyl (S)69 %04/27/23 16:33 321-60-804/26/23 15:3810-130 1
Terphenyl-d14 (S)88 %04/27/23 16:33 1718-51-004/26/23 15:3810-130 1
Phenol-d6 (S)58 %04/27/23 16:33 13127-88-304/26/23 15:3810-130 1
2-Fluorophenol (S)57 %04/27/23 16:33 367-12-404/26/23 15:3810-130 1
2,4,6-Tribromophenol (S)64 %04/27/23 16:33 118-79-604/26/23 15:3810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 21:39 67-64-104/25/23 14:47128 41.2 1
Benzene ND ug/kg 04/25/23 21:39 71-43-204/25/23 14:476.4 2.6 1
Bromobenzene ND ug/kg 04/25/23 21:39 108-86-104/25/23 14:476.4 2.1 1
Bromochloromethane ND ug/kg 04/25/23 21:39 74-97-504/25/23 14:476.4 1.9 1
Bromodichloromethane ND ug/kg 04/25/23 21:39 75-27-404/25/23 14:476.4 2.5 1
Bromoform ND ug/kg 04/25/23 21:39 75-25-204/25/23 14:476.4 2.3 1
Bromomethane ND ug/kg 04/25/23 21:39 74-83-9 IK04/25/23 14:4725.7 19.9 1
2-Butanone (MEK)ND ug/kg 04/25/23 21:39 78-93-304/25/23 14:47128 30.8 1
n-Butylbenzene ND ug/kg 04/25/23 21:39 104-51-804/25/23 14:476.4 4.0 1
sec-Butylbenzene ND ug/kg 04/25/23 21:39 135-98-804/25/23 14:476.4 2.8 1
tert-Butylbenzene ND ug/kg 04/25/23 21:39 98-06-604/25/23 14:476.4 2.3 1
Carbon tetrachloride ND ug/kg 04/25/23 21:39 56-23-504/25/23 14:476.4 2.4 1
Chlorobenzene ND ug/kg 04/25/23 21:39 108-90-704/25/23 14:476.4 3.7 1
Chloroethane ND ug/kg 04/25/23 21:39 75-00-304/25/23 14:4712.8 5.0 1
Chloroform ND ug/kg 04/25/23 21:39 67-66-304/25/23 14:476.4 5.4 1
Chloromethane ND ug/kg 04/25/23 21:39 74-87-304/25/23 14:4712.8 5.4 1
2-Chlorotoluene ND ug/kg 04/25/23 21:39 95-49-804/25/23 14:476.4 2.3 1
4-Chlorotoluene ND ug/kg 04/25/23 21:39 106-43-404/25/23 14:476.4 3.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 21:39 96-12-804/25/23 14:476.4 2.5 1
Dibromochloromethane ND ug/kg 04/25/23 21:39 124-48-104/25/23 14:476.4 3.6 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 21:39 106-93-404/25/23 14:476.4 2.8 1
Dibromomethane ND ug/kg 04/25/23 21:39 74-95-304/25/23 14:476.4 1.4 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 21:39 95-50-104/25/23 14:476.4 2.3 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 21:39 541-73-104/25/23 14:476.4 2.0 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 21:39 106-46-704/25/23 14:476.4 1.7 1
Dichlorodifluoromethane ND ug/kg 04/25/23 21:39 75-71-804/25/23 14:4712.8 6.5 1
1,1-Dichloroethane ND ug/kg 04/25/23 21:39 75-34-304/25/23 14:476.4 2.6 1
1,2-Dichloroethane ND ug/kg 04/25/23 21:39 107-06-204/25/23 14:476.4 4.3 1
1,1-Dichloroethene ND ug/kg 04/25/23 21:39 75-35-404/25/23 14:476.4 2.6 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 21:39 156-59-204/25/23 14:476.4 2.2 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 21:39 156-60-504/25/23 14:476.4 5.5 1
1,2-Dichloropropane ND ug/kg 04/25/23 21:39 78-87-504/25/23 14:476.4 1.9 1
1,3-Dichloropropane ND ug/kg 04/25/23 21:39 142-28-904/25/23 14:476.4 2.0 1
2,2-Dichloropropane ND ug/kg 04/25/23 21:39 594-20-7 v204/25/23 14:476.4 4.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-11 Lab ID: 92663594010 Collected: 04/17/23 13:20 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 21:39 563-58-604/25/23 14:476.4 3.1 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 21:39 10061-01-504/25/23 14:476.4 1.7 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 21:39 10061-02-604/25/23 14:476.4 2.2 1
Diisopropyl ether ND ug/kg 04/25/23 21:39 108-20-304/25/23 14:476.4 1.7 1
Ethylbenzene ND ug/kg 04/25/23 21:39 100-41-404/25/23 14:476.4 3.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 21:39 87-68-304/25/23 14:4712.8 10.5 1
2-Hexanone ND ug/kg 04/25/23 21:39 591-78-604/25/23 14:4764.2 6.2 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 21:39 98-82-804/25/23 14:476.4 2.2 1
p-Isopropyltoluene ND ug/kg 04/25/23 21:39 99-87-604/25/23 14:476.4 3.2 1
Methylene Chloride 26.4 ug/kg 04/25/23 21:39 75-09-2 C904/25/23 14:4725.7 17.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 21:39 108-10-104/25/23 14:4764.2 6.2 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 21:39 1634-04-4 v204/25/23 14:476.4 2.4 1
Naphthalene ND ug/kg 04/25/23 21:39 91-20-304/25/23 14:476.4 3.4 1
n-Propylbenzene ND ug/kg 04/25/23 21:39 103-65-104/25/23 14:476.4 2.3 1
Styrene ND ug/kg 04/25/23 21:39 100-42-504/25/23 14:476.4 1.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 21:39 630-20-604/25/23 14:476.4 2.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 21:39 79-34-504/25/23 14:476.4 1.7 1
Tetrachloroethene ND ug/kg 04/25/23 21:39 127-18-404/25/23 14:476.4 2.0 1
Toluene ND ug/kg 04/25/23 21:39 108-88-304/25/23 14:476.4 4.4 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 21:39 87-61-604/25/23 14:476.4 5.2 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 21:39 120-82-104/25/23 14:476.4 5.4 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 21:39 71-55-604/25/23 14:476.4 3.3 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 21:39 79-00-504/25/23 14:476.4 2.1 1
Trichloroethene ND ug/kg 04/25/23 21:39 79-01-604/25/23 14:476.4 5.2 1
Trichlorofluoromethane ND ug/kg 04/25/23 21:39 75-69-404/25/23 14:476.4 3.5 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 21:39 96-18-404/25/23 14:476.4 3.2 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 21:39 95-63-604/25/23 14:476.4 3.8 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 21:39 108-67-804/25/23 14:476.4 2.2 1
Vinyl acetate ND ug/kg 04/25/23 21:39 108-05-404/25/23 14:4764.2 13.2 1
Vinyl chloride ND ug/kg 04/25/23 21:39 75-01-4 v204/25/23 14:4712.8 3.3 1
Xylene (Total)ND ug/kg 04/25/23 21:39 1330-20-704/25/23 14:4712.8 3.7 1
m&p-Xylene ND ug/kg 04/25/23 21:39 179601-23-104/25/23 14:4712.8 4.4 1
o-Xylene ND ug/kg 04/25/23 21:39 95-47-604/25/23 14:476.4 2.8 1
Surrogates
Toluene-d8 (S)100 %04/25/23 21:39 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)100 %04/25/23 21:39 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)96 %04/25/23 21:39 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.9 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-11 Lab ID: 92663594010 Collected: 04/17/23 13:20 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.7 %04/27/23 17:1504/27/23 17:001
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.856J mg/kg 05/01/23 14:40 18540-29-9 J04/30/23 06:541.27 0.324 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.24J mg/kg 05/01/23 15:52 57-12-505/01/23 12:360.38 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-1 Lab ID: 92663594011 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.25J ug/L 04/24/23 22:24 7440-38-204/23/23 16:541.0 0.087 1
Barium 28.5 ug/L 04/24/23 22:24 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:24 7440-43-904/23/23 16:540.20 0.060 1
Chromium 1.1 ug/L 04/24/23 22:24 7440-47-304/23/23 16:541.0 0.50 1
Lead ND ug/L 04/24/23 22:24 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.12J ug/L 04/24/23 22:24 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:24 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:15 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 20:54 83-32-904/25/23 17:1010.0 2.0 1
Acenaphthylene ND ug/L 04/26/23 20:54 208-96-804/25/23 17:1010.0 2.0 1
Aniline ND ug/L 04/26/23 20:54 62-53-304/25/23 17:1010.0 1.6 1
Anthracene ND ug/L 04/26/23 20:54 120-12-704/25/23 17:1010.0 2.3 1
Benzo(a)anthracene ND ug/L 04/26/23 20:54 56-55-304/25/23 17:1010.0 2.7 1
Benzo(a)pyrene ND ug/L 04/26/23 20:54 50-32-804/25/23 17:1010.0 2.8 1
Benzo(b)fluoranthene ND ug/L 04/26/23 20:54 205-99-204/25/23 17:1010.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 20:54 191-24-204/25/23 17:1010.0 2.8 1
Benzo(k)fluoranthene ND ug/L 04/26/23 20:54 207-08-904/25/23 17:1010.0 2.7 1
Benzoic Acid ND ug/L 04/26/23 20:54 65-85-004/25/23 17:1050.0 22.0 1
Benzyl alcohol ND ug/L 04/26/23 20:54 100-51-604/25/23 17:1020.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 20:54 101-55-304/25/23 17:1010.0 1.8 1
Butylbenzylphthalate ND ug/L 04/26/23 20:54 85-68-704/25/23 17:1010.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 20:54 59-50-704/25/23 17:1010.0 3.3 1
4-Chloroaniline ND ug/L 04/26/23 20:54 106-47-804/25/23 17:1020.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 20:54 111-91-104/25/23 17:1010.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 20:54 111-44-404/25/23 17:1010.0 1.9 1
2-Chloronaphthalene ND ug/L 04/26/23 20:54 91-58-704/25/23 17:1010.0 1.7 1
2-Chlorophenol ND ug/L 04/26/23 20:54 95-57-804/25/23 17:1010.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 20:54 7005-72-304/25/23 17:1010.0 2.0 1
Chrysene ND ug/L 04/26/23 20:54 218-01-904/25/23 17:1010.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 20:54 53-70-304/25/23 17:1010.0 3.0 1
Dibenzofuran ND ug/L 04/26/23 20:54 132-64-904/25/23 17:1010.0 2.1 1
1,2-Dichlorobenzene ND ug/L 04/26/23 20:54 95-50-104/25/23 17:1010.0 1.8 1
1,3-Dichlorobenzene ND ug/L 04/26/23 20:54 541-73-104/25/23 17:1010.0 1.6 1
1,4-Dichlorobenzene ND ug/L 04/26/23 20:54 106-46-704/25/23 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 20:54 91-94-104/25/23 17:1020.0 8.1 1
2,4-Dichlorophenol ND ug/L 04/26/23 20:54 120-83-204/25/23 17:1010.0 1.4 1
Diethylphthalate ND ug/L 04/26/23 20:54 84-66-204/25/23 17:1010.0 2.0 1
2,4-Dimethylphenol ND ug/L 04/26/23 20:54 105-67-904/25/23 17:1010.0 1.7 1
Dimethylphthalate ND ug/L 04/26/23 20:54 131-11-304/25/23 17:1010.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-1 Lab ID: 92663594011 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 20:54 84-74-204/25/23 17:1010.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 20:54 534-52-104/25/23 17:1020.0 7.8 1
2,4-Dinitrophenol ND ug/L 04/26/23 20:54 51-28-504/25/23 17:1050.0 26.0 1
2,4-Dinitrotoluene ND ug/L 04/26/23 20:54 121-14-204/25/23 17:1010.0 1.6 1
2,6-Dinitrotoluene ND ug/L 04/26/23 20:54 606-20-204/25/23 17:1010.0 1.7 1
Di-n-octylphthalate ND ug/L 04/26/23 20:54 117-84-004/25/23 17:1010.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 20:54 117-81-704/25/23 17:106.0 3.7 1
Fluoranthene ND ug/L 04/26/23 20:54 206-44-004/25/23 17:1010.0 2.2 1
Fluorene ND ug/L 04/26/23 20:54 86-73-704/25/23 17:1010.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 20:54 87-68-304/25/23 17:1010.0 1.8 1
Hexachlorobenzene ND ug/L 04/26/23 20:54 118-74-104/25/23 17:1010.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 20:54 77-47-404/25/23 17:1010.0 1.6 1
Hexachloroethane ND ug/L 04/26/23 20:54 67-72-104/25/23 17:1010.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 20:54 193-39-504/25/23 17:1010.0 2.9 1
Isophorone ND ug/L 04/26/23 20:54 78-59-104/25/23 17:1010.0 1.7 1
1-Methylnaphthalene ND ug/L 04/26/23 20:54 90-12-004/25/23 17:1010.0 2.0 1
2-Methylnaphthalene ND ug/L 04/26/23 20:54 91-57-604/25/23 17:1010.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 20:54 95-48-704/25/23 17:1010.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 20:54 15831-10-404/25/23 17:1010.0 1.2 1
Naphthalene ND ug/L 04/26/23 20:54 91-20-304/25/23 17:1010.0 2.1 1
2-Nitroaniline ND ug/L 04/26/23 20:54 88-74-404/25/23 17:1020.0 3.0 1
3-Nitroaniline ND ug/L 04/26/23 20:54 99-09-204/25/23 17:1020.0 3.8 1
4-Nitroaniline ND ug/L 04/26/23 20:54 100-01-604/25/23 17:1020.0 5.1 1
Nitrobenzene ND ug/L 04/26/23 20:54 98-95-304/25/23 17:1010.0 1.9 1
2-Nitrophenol ND ug/L 04/26/23 20:54 88-75-504/25/23 17:1010.0 1.4 1
4-Nitrophenol ND ug/L 04/26/23 20:54 100-02-704/25/23 17:1050.0 6.6 1
N-Nitrosodimethylamine ND ug/L 04/26/23 20:54 62-75-904/25/23 17:1010.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 20:54 621-64-704/25/23 17:1010.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 20:54 86-30-604/25/23 17:1010.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 20:54 108-60-104/25/23 17:1010.0 1.2 1
Pentachlorophenol ND ug/L 04/26/23 20:54 87-86-504/25/23 17:1020.0 3.8 1
Phenanthrene ND ug/L 04/26/23 20:54 85-01-804/25/23 17:1010.0 2.0 1
Phenol ND ug/L 04/26/23 20:54 108-95-204/25/23 17:1010.0 1.4 1
Pyrene ND ug/L 04/26/23 20:54 129-00-004/25/23 17:1010.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 20:54 120-82-104/25/23 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 20:54 95-95-404/25/23 17:1010.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 20:54 88-06-204/25/23 17:1010.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)57 %04/26/23 20:54 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)51 %04/26/23 20:54 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)73 %04/26/23 20:54 1718-51-004/25/23 17:1019-191 1
Phenol-d6 (S)35 %04/26/23 20:54 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)41 %04/26/23 20:54 367-12-404/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)59 %04/26/23 20:54 118-79-604/25/23 17:1010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-1 Lab ID: 92663594011 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/26/23 11:30 67-64-125.0 5.1 1
Benzene ND ug/L 04/26/23 11:30 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/26/23 11:30 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/26/23 11:30 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/26/23 11:30 75-27-41.0 0.31 1
Bromoform ND ug/L 04/26/23 11:30 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/26/23 11:30 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/26/23 11:30 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/26/23 11:30 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/26/23 11:30 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/26/23 11:30 75-00-31.0 0.65 1
Chloroform ND ug/L 04/26/23 11:30 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/26/23 11:30 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/26/23 11:30 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/26/23 11:30 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/26/23 11:30 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/26/23 11:30 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/26/23 11:30 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/26/23 11:30 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/26/23 11:30 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/26/23 11:30 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/26/23 11:30 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/26/23 11:30 75-71-8 IK,M1,
v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/26/23 11:30 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/26/23 11:30 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/26/23 11:30 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.77J ug/L 04/26/23 11:30 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/26/23 11:30 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/26/23 11:30 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/26/23 11:30 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/26/23 11:30 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/26/23 11:30 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/26/23 11:30 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/26/23 11:30 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/26/23 11:30 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/26/23 11:30 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 11:30 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/26/23 11:30 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/26/23 11:30 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/26/23 11:30 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/26/23 11:30 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/26/23 11:30 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/26/23 11:30 91-20-31.0 0.64 1
Styrene ND ug/L 04/26/23 11:30 100-42-51.0 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-1 Lab ID: 92663594011 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,1,2-Tetrachloroethane ND ug/L 04/26/23 11:30 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/26/23 11:30 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/26/23 11:30 127-18-41.0 0.29 1
Toluene ND ug/L 04/26/23 11:30 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/26/23 11:30 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 11:30 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/26/23 11:30 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/26/23 11:30 79-00-51.0 0.32 1
Trichloroethene ND ug/L 04/26/23 11:30 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/26/23 11:30 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/26/23 11:30 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/26/23 11:30 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/26/23 11:30 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/26/23 11:30 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/26/23 11:30 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/26/23 11:30 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %04/26/23 11:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %04/26/23 11:30 17060-07-070-130 1
Toluene-d8 (S)100 %04/26/23 11:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-2 Lab ID: 92663594012 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.50J ug/L 04/24/23 22:27 7440-38-204/23/23 16:541.0 0.087 1
Barium 41.0 ug/L 04/24/23 22:27 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:27 7440-43-904/23/23 16:540.20 0.060 1
Chromium 0.64J ug/L 04/24/23 22:27 7440-47-304/23/23 16:541.0 0.50 1
Lead ND ug/L 04/24/23 22:27 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.47J ug/L 04/24/23 22:27 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:27 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:17 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 21:19 83-32-904/25/23 17:1010.0 2.0 1
Acenaphthylene ND ug/L 04/26/23 21:19 208-96-804/25/23 17:1010.0 2.0 1
Aniline ND ug/L 04/26/23 21:19 62-53-304/25/23 17:1010.0 1.6 1
Anthracene ND ug/L 04/26/23 21:19 120-12-704/25/23 17:1010.0 2.3 1
Benzo(a)anthracene ND ug/L 04/26/23 21:19 56-55-304/25/23 17:1010.0 2.7 1
Benzo(a)pyrene ND ug/L 04/26/23 21:19 50-32-804/25/23 17:1010.0 2.8 1
Benzo(b)fluoranthene ND ug/L 04/26/23 21:19 205-99-204/25/23 17:1010.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 21:19 191-24-204/25/23 17:1010.0 2.8 1
Benzo(k)fluoranthene ND ug/L 04/26/23 21:19 207-08-904/25/23 17:1010.0 2.7 1
Benzoic Acid ND ug/L 04/26/23 21:19 65-85-004/25/23 17:1050.0 22.0 1
Benzyl alcohol ND ug/L 04/26/23 21:19 100-51-604/25/23 17:1020.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 21:19 101-55-304/25/23 17:1010.0 1.8 1
Butylbenzylphthalate ND ug/L 04/26/23 21:19 85-68-704/25/23 17:1010.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 21:19 59-50-704/25/23 17:1010.0 3.3 1
4-Chloroaniline ND ug/L 04/26/23 21:19 106-47-804/25/23 17:1020.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 21:19 111-91-104/25/23 17:1010.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 21:19 111-44-404/25/23 17:1010.0 1.9 1
2-Chloronaphthalene ND ug/L 04/26/23 21:19 91-58-704/25/23 17:1010.0 1.7 1
2-Chlorophenol ND ug/L 04/26/23 21:19 95-57-804/25/23 17:1010.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 21:19 7005-72-304/25/23 17:1010.0 2.0 1
Chrysene ND ug/L 04/26/23 21:19 218-01-904/25/23 17:1010.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 21:19 53-70-304/25/23 17:1010.0 3.0 1
Dibenzofuran ND ug/L 04/26/23 21:19 132-64-904/25/23 17:1010.0 2.1 1
1,2-Dichlorobenzene ND ug/L 04/26/23 21:19 95-50-104/25/23 17:1010.0 1.8 1
1,3-Dichlorobenzene ND ug/L 04/26/23 21:19 541-73-104/25/23 17:1010.0 1.6 1
1,4-Dichlorobenzene ND ug/L 04/26/23 21:19 106-46-704/25/23 17:1010.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 21:19 91-94-104/25/23 17:1020.0 8.1 1
2,4-Dichlorophenol ND ug/L 04/26/23 21:19 120-83-204/25/23 17:1010.0 1.4 1
Diethylphthalate ND ug/L 04/26/23 21:19 84-66-204/25/23 17:1010.0 2.0 1
2,4-Dimethylphenol ND ug/L 04/26/23 21:19 105-67-904/25/23 17:1010.0 1.7 1
Dimethylphthalate ND ug/L 04/26/23 21:19 131-11-304/25/23 17:1010.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-2 Lab ID: 92663594012 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 21:19 84-74-204/25/23 17:1010.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 21:19 534-52-104/25/23 17:1020.0 7.8 1
2,4-Dinitrophenol ND ug/L 04/26/23 21:19 51-28-504/25/23 17:1050.0 26.0 1
2,4-Dinitrotoluene ND ug/L 04/26/23 21:19 121-14-204/25/23 17:1010.0 1.6 1
2,6-Dinitrotoluene ND ug/L 04/26/23 21:19 606-20-204/25/23 17:1010.0 1.7 1
Di-n-octylphthalate ND ug/L 04/26/23 21:19 117-84-004/25/23 17:1010.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 21:19 117-81-704/25/23 17:106.0 3.7 1
Fluoranthene ND ug/L 04/26/23 21:19 206-44-004/25/23 17:1010.0 2.2 1
Fluorene ND ug/L 04/26/23 21:19 86-73-704/25/23 17:1010.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 21:19 87-68-304/25/23 17:1010.0 1.8 1
Hexachlorobenzene ND ug/L 04/26/23 21:19 118-74-104/25/23 17:1010.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 21:19 77-47-404/25/23 17:1010.0 1.6 1
Hexachloroethane ND ug/L 04/26/23 21:19 67-72-104/25/23 17:1010.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 21:19 193-39-504/25/23 17:1010.0 2.9 1
Isophorone ND ug/L 04/26/23 21:19 78-59-104/25/23 17:1010.0 1.7 1
1-Methylnaphthalene ND ug/L 04/26/23 21:19 90-12-004/25/23 17:1010.0 2.0 1
2-Methylnaphthalene ND ug/L 04/26/23 21:19 91-57-604/25/23 17:1010.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 21:19 95-48-704/25/23 17:1010.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 21:19 15831-10-404/25/23 17:1010.0 1.2 1
Naphthalene ND ug/L 04/26/23 21:19 91-20-304/25/23 17:1010.0 2.1 1
2-Nitroaniline ND ug/L 04/26/23 21:19 88-74-404/25/23 17:1020.0 3.0 1
3-Nitroaniline ND ug/L 04/26/23 21:19 99-09-204/25/23 17:1020.0 3.8 1
4-Nitroaniline ND ug/L 04/26/23 21:19 100-01-604/25/23 17:1020.0 5.1 1
Nitrobenzene ND ug/L 04/26/23 21:19 98-95-304/25/23 17:1010.0 1.9 1
2-Nitrophenol ND ug/L 04/26/23 21:19 88-75-504/25/23 17:1010.0 1.4 1
4-Nitrophenol ND ug/L 04/26/23 21:19 100-02-704/25/23 17:1050.0 6.6 1
N-Nitrosodimethylamine ND ug/L 04/26/23 21:19 62-75-904/25/23 17:1010.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 21:19 621-64-704/25/23 17:1010.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 21:19 86-30-604/25/23 17:1010.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 21:19 108-60-104/25/23 17:1010.0 1.2 1
Pentachlorophenol ND ug/L 04/26/23 21:19 87-86-504/25/23 17:1020.0 3.8 1
Phenanthrene ND ug/L 04/26/23 21:19 85-01-804/25/23 17:1010.0 2.0 1
Phenol ND ug/L 04/26/23 21:19 108-95-204/25/23 17:1010.0 1.4 1
Pyrene ND ug/L 04/26/23 21:19 129-00-004/25/23 17:1010.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 21:19 120-82-104/25/23 17:1010.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 21:19 95-95-404/25/23 17:1010.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 21:19 88-06-204/25/23 17:1010.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)82 %04/26/23 21:19 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)74 %04/26/23 21:19 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)95 %04/26/23 21:19 1718-51-004/25/23 17:1019-191 1
Phenol-d6 (S)46 %04/26/23 21:19 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)35 %04/26/23 21:19 367-12-404/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)54 %04/26/23 21:19 118-79-604/25/23 17:1010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-2 Lab ID: 92663594012 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/26/23 11:12 67-64-125.0 5.1 1
Benzene ND ug/L 04/26/23 11:12 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/26/23 11:12 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/26/23 11:12 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/26/23 11:12 75-27-41.0 0.31 1
Bromoform ND ug/L 04/26/23 11:12 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/26/23 11:12 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/26/23 11:12 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/26/23 11:12 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/26/23 11:12 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/26/23 11:12 75-00-31.0 0.65 1
Chloroform ND ug/L 04/26/23 11:12 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/26/23 11:12 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/26/23 11:12 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/26/23 11:12 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/26/23 11:12 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/26/23 11:12 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/26/23 11:12 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/26/23 11:12 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/26/23 11:12 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/26/23 11:12 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/26/23 11:12 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/26/23 11:12 75-71-8 IK,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/26/23 11:12 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/26/23 11:12 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/26/23 11:12 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/26/23 11:12 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/26/23 11:12 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/26/23 11:12 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/26/23 11:12 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/26/23 11:12 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/26/23 11:12 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/26/23 11:12 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/26/23 11:12 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/26/23 11:12 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/26/23 11:12 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 11:12 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/26/23 11:12 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/26/23 11:12 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/26/23 11:12 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/26/23 11:12 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/26/23 11:12 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/26/23 11:12 91-20-31.0 0.64 1
Styrene ND ug/L 04/26/23 11:12 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/26/23 11:12 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-2 Lab ID: 92663594012 Collected: 04/21/23 09:05 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 04/26/23 11:12 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/26/23 11:12 127-18-41.0 0.29 1
Toluene ND ug/L 04/26/23 11:12 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/26/23 11:12 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 11:12 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/26/23 11:12 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/26/23 11:12 79-00-51.0 0.32 1
Trichloroethene ND ug/L 04/26/23 11:12 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/26/23 11:12 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/26/23 11:12 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/26/23 11:12 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/26/23 11:12 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/26/23 11:12 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/26/23 11:12 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/26/23 11:12 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)100 %04/26/23 11:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %04/26/23 11:12 17060-07-070-130 1
Toluene-d8 (S)104 %04/26/23 11:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-3 Lab ID: 92663594013 Collected: 04/19/23 15:50 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.37J ug/L 04/24/23 22:31 7440-38-204/23/23 16:541.0 0.087 1
Barium 37.4 ug/L 04/24/23 22:31 7440-39-304/23/23 16:541.0 0.21 1
Cadmium 0.083J ug/L 04/24/23 22:31 7440-43-904/23/23 16:540.20 0.060 1
Chromium 1.3 ug/L 04/24/23 22:31 7440-47-304/23/23 16:541.0 0.50 1
Lead 4.6 ug/L 04/24/23 22:31 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.21J ug/L 04/24/23 22:31 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:31 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:19 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 14:32 83-32-904/25/23 14:418.3 1.7 1
Acenaphthylene ND ug/L 04/26/23 14:32 208-96-804/25/23 14:418.3 1.6 1
Aniline ND ug/L 04/26/23 14:32 62-53-304/25/23 14:418.3 1.4 1
Anthracene ND ug/L 04/26/23 14:32 120-12-704/25/23 14:418.3 1.9 1
Benzo(a)anthracene ND ug/L 04/26/23 14:32 56-55-304/25/23 14:418.3 2.2 1
Benzo(a)pyrene ND ug/L 04/26/23 14:32 50-32-804/25/23 14:418.3 2.3 1
Benzo(b)fluoranthene ND ug/L 04/26/23 14:32 205-99-204/25/23 14:418.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 14:32 191-24-204/25/23 14:418.3 2.4 1
Benzo(k)fluoranthene ND ug/L 04/26/23 14:32 207-08-904/25/23 14:418.3 2.3 1
Benzoic Acid ND ug/L 04/26/23 14:32 65-85-004/25/23 14:4141.7 18.3 1
Benzyl alcohol ND ug/L 04/26/23 14:32 100-51-604/25/23 14:4116.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 14:32 101-55-304/25/23 14:418.3 1.5 1
Butylbenzylphthalate ND ug/L 04/26/23 14:32 85-68-704/25/23 14:418.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 14:32 59-50-704/25/23 14:418.3 2.8 1
4-Chloroaniline ND ug/L 04/26/23 14:32 106-47-804/25/23 14:4116.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 14:32 111-91-104/25/23 14:418.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 14:32 111-44-404/25/23 14:418.3 1.6 1
2-Chloronaphthalene ND ug/L 04/26/23 14:32 91-58-704/25/23 14:418.3 1.4 1
2-Chlorophenol ND ug/L 04/26/23 14:32 95-57-804/25/23 14:418.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 14:32 7005-72-304/25/23 14:418.3 1.7 1
Chrysene ND ug/L 04/26/23 14:32 218-01-904/25/23 14:418.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 14:32 53-70-304/25/23 14:418.3 2.5 1
Dibenzofuran ND ug/L 04/26/23 14:32 132-64-904/25/23 14:418.3 1.8 1
1,2-Dichlorobenzene ND ug/L 04/26/23 14:32 95-50-1 R104/25/23 14:418.3 1.5 1
1,3-Dichlorobenzene ND ug/L 04/26/23 14:32 541-73-1 R104/25/23 14:418.3 1.3 1
1,4-Dichlorobenzene ND ug/L 04/26/23 14:32 106-46-7 R104/25/23 14:418.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 14:32 91-94-104/25/23 14:4116.7 6.8 1
2,4-Dichlorophenol ND ug/L 04/26/23 14:32 120-83-204/25/23 14:418.3 1.2 1
Diethylphthalate ND ug/L 04/26/23 14:32 84-66-204/25/23 14:418.3 1.7 1
2,4-Dimethylphenol ND ug/L 04/26/23 14:32 105-67-9 v204/25/23 14:418.3 1.4 1
Dimethylphthalate ND ug/L 04/26/23 14:32 131-11-304/25/23 14:418.3 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-3 Lab ID: 92663594013 Collected: 04/19/23 15:50 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 14:32 84-74-204/25/23 14:418.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 14:32 534-52-104/25/23 14:4116.7 6.5 1
2,4-Dinitrophenol ND ug/L 04/26/23 14:32 51-28-504/25/23 14:4141.7 21.7 1
2,4-Dinitrotoluene ND ug/L 04/26/23 14:32 121-14-204/25/23 14:418.3 1.4 1
2,6-Dinitrotoluene ND ug/L 04/26/23 14:32 606-20-204/25/23 14:418.3 1.4 1
Di-n-octylphthalate ND ug/L 04/26/23 14:32 117-84-004/25/23 14:418.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 14:32 117-81-704/25/23 14:415.0 3.1 1
Fluoranthene ND ug/L 04/26/23 14:32 206-44-004/25/23 14:418.3 1.8 1
Fluorene ND ug/L 04/26/23 14:32 86-73-704/25/23 14:418.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 14:32 87-68-304/25/23 14:418.3 1.5 1
Hexachlorobenzene ND ug/L 04/26/23 14:32 118-74-104/25/23 14:418.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 14:32 77-47-404/25/23 14:418.3 1.3 1
Hexachloroethane ND ug/L 04/26/23 14:32 67-72-104/25/23 14:418.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 14:32 193-39-504/25/23 14:418.3 2.4 1
Isophorone ND ug/L 04/26/23 14:32 78-59-104/25/23 14:418.3 1.4 1
1-Methylnaphthalene ND ug/L 04/26/23 14:32 90-12-004/25/23 14:418.3 1.7 1
2-Methylnaphthalene ND ug/L 04/26/23 14:32 91-57-604/25/23 14:418.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 14:32 95-48-704/25/23 14:418.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 14:32 15831-10-404/25/23 14:418.3 1.0 1
Naphthalene ND ug/L 04/26/23 14:32 91-20-304/25/23 14:418.3 1.7 1
2-Nitroaniline ND ug/L 04/26/23 14:32 88-74-404/25/23 14:4116.7 2.5 1
3-Nitroaniline ND ug/L 04/26/23 14:32 99-09-204/25/23 14:4116.7 3.1 1
4-Nitroaniline ND ug/L 04/26/23 14:32 100-01-604/25/23 14:4116.7 4.2 1
Nitrobenzene ND ug/L 04/26/23 14:32 98-95-304/25/23 14:418.3 1.6 1
2-Nitrophenol ND ug/L 04/26/23 14:32 88-75-504/25/23 14:418.3 1.2 1
4-Nitrophenol ND ug/L 04/26/23 14:32 100-02-704/25/23 14:4141.7 5.5 1
N-Nitrosodimethylamine ND ug/L 04/26/23 14:32 62-75-904/25/23 14:418.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 14:32 621-64-704/25/23 14:418.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 14:32 86-30-604/25/23 14:418.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 14:32 108-60-104/25/23 14:418.3 0.96 1
Pentachlorophenol ND ug/L 04/26/23 14:32 87-86-504/25/23 14:4116.7 3.1 1
Phenanthrene ND ug/L 04/26/23 14:32 85-01-804/25/23 14:418.3 1.7 1
Phenol ND ug/L 04/26/23 14:32 108-95-204/25/23 14:418.3 1.1 1
Pyrene ND ug/L 04/26/23 14:32 129-00-004/25/23 14:418.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 14:32 120-82-1 R104/25/23 14:418.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 14:32 95-95-404/25/23 14:418.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 14:32 88-06-204/25/23 14:418.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)53 %04/26/23 14:32 4165-60-004/25/23 14:4110-138 1
2-Fluorobiphenyl (S)46 %04/26/23 14:32 321-60-804/25/23 14:4110-130 1
Terphenyl-d14 (S)93 %04/26/23 14:32 1718-51-004/25/23 14:4119-191 1
Phenol-d6 (S)30 %04/26/23 14:32 13127-88-304/25/23 14:4110-130 1
2-Fluorophenol (S)39 %04/26/23 14:32 367-12-404/25/23 14:4110-130 1
2,4,6-Tribromophenol (S)65 %04/26/23 14:32 118-79-604/25/23 14:4110-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-3 Lab ID: 92663594013 Collected: 04/19/23 15:50 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 07:24 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 07:24 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 07:24 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 07:24 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 07:24 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 07:24 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 07:24 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 07:24 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 07:24 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 07:24 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 07:24 75-00-31.0 0.65 1
Chloroform ND ug/L 04/28/23 07:24 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 07:24 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 07:24 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 07:24 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 07:24 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 07:24 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 07:24 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 07:24 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 07:24 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 07:24 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 07:24 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 07:24 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 07:24 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 07:24 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 07:24 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/28/23 07:24 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 07:24 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 07:24 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 07:24 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 07:24 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 07:24 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 07:24 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 07:24 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 07:24 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 07:24 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 07:24 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 07:24 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/28/23 07:24 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 07:24 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 07:24 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 07:24 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 07:24 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 07:24 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 07:24 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-3 Lab ID: 92663594013 Collected: 04/19/23 15:50 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 07:24 79-34-51.0 0.22 1
Tetrachloroethene 0.58J ug/L 04/28/23 07:24 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 07:24 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 07:24 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 07:24 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 07:24 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 07:24 79-00-51.0 0.32 1
Trichloroethene 0.57J ug/L 04/28/23 07:24 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 07:24 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 07:24 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 07:24 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 07:24 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 07:24 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 07:24 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 07:24 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %04/28/23 07:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %04/28/23 07:24 17060-07-070-130 1
Toluene-d8 (S)102 %04/28/23 07:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-4 Lab ID: 92663594014 Collected: 04/21/23 10:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.22J ug/L 04/24/23 22:35 7440-38-204/23/23 16:541.0 0.087 1
Barium 37.6 ug/L 04/24/23 22:35 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:35 7440-43-904/23/23 16:540.20 0.060 1
Chromium 5.7 ug/L 04/24/23 22:35 7440-47-304/23/23 16:541.0 0.50 1
Lead ND ug/L 04/24/23 22:35 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.14J ug/L 04/24/23 22:35 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:35 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:26 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 21:44 83-32-904/25/23 17:108.7 1.7 1
Acenaphthylene ND ug/L 04/26/23 21:44 208-96-804/25/23 17:108.7 1.7 1
Aniline ND ug/L 04/26/23 21:44 62-53-304/25/23 17:108.7 1.4 1
Anthracene ND ug/L 04/26/23 21:44 120-12-704/25/23 17:108.7 2.0 1
Benzo(a)anthracene ND ug/L 04/26/23 21:44 56-55-304/25/23 17:108.7 2.3 1
Benzo(a)pyrene ND ug/L 04/26/23 21:44 50-32-804/25/23 17:108.7 2.4 1
Benzo(b)fluoranthene ND ug/L 04/26/23 21:44 205-99-204/25/23 17:108.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 21:44 191-24-204/25/23 17:108.7 2.5 1
Benzo(k)fluoranthene ND ug/L 04/26/23 21:44 207-08-904/25/23 17:108.7 2.4 1
Benzoic Acid ND ug/L 04/26/23 21:44 65-85-004/25/23 17:1043.5 19.1 1
Benzyl alcohol ND ug/L 04/26/23 21:44 100-51-604/25/23 17:1017.4 2.5 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 21:44 101-55-304/25/23 17:108.7 1.5 1
Butylbenzylphthalate ND ug/L 04/26/23 21:44 85-68-704/25/23 17:108.7 2.7 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 21:44 59-50-704/25/23 17:108.7 2.9 1
4-Chloroaniline ND ug/L 04/26/23 21:44 106-47-804/25/23 17:1017.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 21:44 111-91-104/25/23 17:108.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 21:44 111-44-404/25/23 17:108.7 1.7 1
2-Chloronaphthalene ND ug/L 04/26/23 21:44 91-58-704/25/23 17:108.7 1.5 1
2-Chlorophenol ND ug/L 04/26/23 21:44 95-57-804/25/23 17:108.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 21:44 7005-72-304/25/23 17:108.7 1.7 1
Chrysene ND ug/L 04/26/23 21:44 218-01-904/25/23 17:108.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 21:44 53-70-304/25/23 17:108.7 2.6 1
Dibenzofuran ND ug/L 04/26/23 21:44 132-64-904/25/23 17:108.7 1.8 1
1,2-Dichlorobenzene ND ug/L 04/26/23 21:44 95-50-104/25/23 17:108.7 1.6 1
1,3-Dichlorobenzene ND ug/L 04/26/23 21:44 541-73-104/25/23 17:108.7 1.4 1
1,4-Dichlorobenzene ND ug/L 04/26/23 21:44 106-46-704/25/23 17:108.7 1.5 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 21:44 91-94-104/25/23 17:1017.4 7.1 1
2,4-Dichlorophenol ND ug/L 04/26/23 21:44 120-83-204/25/23 17:108.7 1.2 1
Diethylphthalate ND ug/L 04/26/23 21:44 84-66-204/25/23 17:108.7 1.8 1
2,4-Dimethylphenol ND ug/L 04/26/23 21:44 105-67-904/25/23 17:108.7 1.5 1
Dimethylphthalate ND ug/L 04/26/23 21:44 131-11-304/25/23 17:108.7 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-4 Lab ID: 92663594014 Collected: 04/21/23 10:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 21:44 84-74-204/25/23 17:108.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 21:44 534-52-104/25/23 17:1017.4 6.8 1
2,4-Dinitrophenol ND ug/L 04/26/23 21:44 51-28-504/25/23 17:1043.5 22.6 1
2,4-Dinitrotoluene ND ug/L 04/26/23 21:44 121-14-204/25/23 17:108.7 1.4 1
2,6-Dinitrotoluene ND ug/L 04/26/23 21:44 606-20-204/25/23 17:108.7 1.5 1
Di-n-octylphthalate ND ug/L 04/26/23 21:44 117-84-004/25/23 17:108.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 21:44 117-81-704/25/23 17:105.2 3.2 1
Fluoranthene ND ug/L 04/26/23 21:44 206-44-004/25/23 17:108.7 1.9 1
Fluorene ND ug/L 04/26/23 21:44 86-73-704/25/23 17:108.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 21:44 87-68-304/25/23 17:108.7 1.5 1
Hexachlorobenzene ND ug/L 04/26/23 21:44 118-74-104/25/23 17:108.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 21:44 77-47-404/25/23 17:108.7 1.4 1
Hexachloroethane ND ug/L 04/26/23 21:44 67-72-104/25/23 17:108.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 21:44 193-39-504/25/23 17:108.7 2.5 1
Isophorone ND ug/L 04/26/23 21:44 78-59-104/25/23 17:108.7 1.4 1
1-Methylnaphthalene ND ug/L 04/26/23 21:44 90-12-004/25/23 17:108.7 1.8 1
2-Methylnaphthalene ND ug/L 04/26/23 21:44 91-57-604/25/23 17:108.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 21:44 95-48-704/25/23 17:108.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 21:44 15831-10-404/25/23 17:108.7 1.1 1
Naphthalene ND ug/L 04/26/23 21:44 91-20-304/25/23 17:108.7 1.8 1
2-Nitroaniline ND ug/L 04/26/23 21:44 88-74-404/25/23 17:1017.4 2.6 1
3-Nitroaniline ND ug/L 04/26/23 21:44 99-09-204/25/23 17:1017.4 3.3 1
4-Nitroaniline ND ug/L 04/26/23 21:44 100-01-604/25/23 17:1017.4 4.4 1
Nitrobenzene ND ug/L 04/26/23 21:44 98-95-304/25/23 17:108.7 1.6 1
2-Nitrophenol ND ug/L 04/26/23 21:44 88-75-504/25/23 17:108.7 1.2 1
4-Nitrophenol ND ug/L 04/26/23 21:44 100-02-704/25/23 17:1043.5 5.7 1
N-Nitrosodimethylamine ND ug/L 04/26/23 21:44 62-75-904/25/23 17:108.7 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 21:44 621-64-704/25/23 17:108.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 21:44 86-30-604/25/23 17:108.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 21:44 108-60-104/25/23 17:108.7 1.0 1
Pentachlorophenol ND ug/L 04/26/23 21:44 87-86-504/25/23 17:1017.4 3.3 1
Phenanthrene ND ug/L 04/26/23 21:44 85-01-804/25/23 17:108.7 1.7 1
Phenol ND ug/L 04/26/23 21:44 108-95-204/25/23 17:108.7 1.2 1
Pyrene ND ug/L 04/26/23 21:44 129-00-004/25/23 17:108.7 1.9 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 21:44 120-82-104/25/23 17:108.7 1.5 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 21:44 95-95-404/25/23 17:108.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 21:44 88-06-204/25/23 17:108.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)86 %04/26/23 21:44 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)76 %04/26/23 21:44 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)101 %04/26/23 21:44 1718-51-004/25/23 17:1019-191 1
Phenol-d6 (S)52 %04/26/23 21:44 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)65 %04/26/23 21:44 367-12-404/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)89 %04/26/23 21:44 118-79-604/25/23 17:1010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-4 Lab ID: 92663594014 Collected: 04/21/23 10:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 08:00 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 08:00 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 08:00 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 08:00 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 08:00 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 08:00 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 08:00 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 08:00 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 08:00 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 08:00 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 08:00 75-00-31.0 0.65 1
Chloroform 0.44J ug/L 04/28/23 08:00 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 08:00 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 08:00 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 08:00 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 08:00 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 08:00 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 08:00 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 08:00 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 08:00 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 08:00 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 08:00 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 08:00 75-71-8 IH,M1,
v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 08:00 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 08:00 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 08:00 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.88J ug/L 04/28/23 08:00 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 08:00 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 08:00 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 08:00 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 08:00 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 08:00 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 08:00 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 08:00 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 08:00 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 08:00 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 08:00 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 08:00 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/28/23 08:00 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 08:00 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 08:00 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 08:00 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 08:00 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 08:00 100-42-51.0 0.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-4 Lab ID: 92663594014 Collected: 04/21/23 10:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 08:00 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 08:00 79-34-51.0 0.22 1
Tetrachloroethene 1.8 ug/L 04/28/23 08:00 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 08:00 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 08:00 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 08:00 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 08:00 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 08:00 79-00-51.0 0.32 1
Trichloroethene 2.2 ug/L 04/28/23 08:00 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 08:00 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 08:00 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 08:00 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 08:00 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 08:00 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 08:00 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 08:00 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %04/28/23 08:00 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %04/28/23 08:00 17060-07-070-130 1
Toluene-d8 (S)103 %04/28/23 08:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-5 Lab ID: 92663594015 Collected: 04/20/23 14:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.16J ug/L 04/24/23 22:39 7440-38-204/23/23 16:541.0 0.087 1
Barium 49.6 ug/L 04/24/23 22:39 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:39 7440-43-904/23/23 16:540.20 0.060 1
Chromium 1.9 ug/L 04/24/23 22:39 7440-47-304/23/23 16:541.0 0.50 1
Lead 0.35J ug/L 04/24/23 22:39 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.16J ug/L 04/24/23 22:39 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:39 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:29 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 22:10 83-32-904/25/23 17:108.7 1.7 1
Acenaphthylene ND ug/L 04/26/23 22:10 208-96-804/25/23 17:108.7 1.7 1
Aniline ND ug/L 04/26/23 22:10 62-53-304/25/23 17:108.7 1.4 1
Anthracene ND ug/L 04/26/23 22:10 120-12-704/25/23 17:108.7 2.0 1
Benzo(a)anthracene ND ug/L 04/26/23 22:10 56-55-304/25/23 17:108.7 2.3 1
Benzo(a)pyrene ND ug/L 04/26/23 22:10 50-32-804/25/23 17:108.7 2.4 1
Benzo(b)fluoranthene ND ug/L 04/26/23 22:10 205-99-204/25/23 17:108.7 2.3 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 22:10 191-24-204/25/23 17:108.7 2.5 1
Benzo(k)fluoranthene ND ug/L 04/26/23 22:10 207-08-904/25/23 17:108.7 2.4 1
Benzoic Acid ND ug/L 04/26/23 22:10 65-85-004/25/23 17:1043.5 19.1 1
Benzyl alcohol ND ug/L 04/26/23 22:10 100-51-604/25/23 17:1017.4 2.5 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 22:10 101-55-304/25/23 17:108.7 1.5 1
Butylbenzylphthalate ND ug/L 04/26/23 22:10 85-68-704/25/23 17:108.7 2.7 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 22:10 59-50-704/25/23 17:108.7 2.9 1
4-Chloroaniline ND ug/L 04/26/23 22:10 106-47-804/25/23 17:1017.4 3.2 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 22:10 111-91-104/25/23 17:108.7 1.6 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 22:10 111-44-404/25/23 17:108.7 1.7 1
2-Chloronaphthalene ND ug/L 04/26/23 22:10 91-58-704/25/23 17:108.7 1.5 1
2-Chlorophenol ND ug/L 04/26/23 22:10 95-57-804/25/23 17:108.7 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 22:10 7005-72-304/25/23 17:108.7 1.7 1
Chrysene ND ug/L 04/26/23 22:10 218-01-904/25/23 17:108.7 2.4 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 22:10 53-70-304/25/23 17:108.7 2.6 1
Dibenzofuran ND ug/L 04/26/23 22:10 132-64-904/25/23 17:108.7 1.8 1
1,2-Dichlorobenzene ND ug/L 04/26/23 22:10 95-50-104/25/23 17:108.7 1.6 1
1,3-Dichlorobenzene ND ug/L 04/26/23 22:10 541-73-104/25/23 17:108.7 1.4 1
1,4-Dichlorobenzene ND ug/L 04/26/23 22:10 106-46-704/25/23 17:108.7 1.5 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 22:10 91-94-104/25/23 17:1017.4 7.1 1
2,4-Dichlorophenol ND ug/L 04/26/23 22:10 120-83-204/25/23 17:108.7 1.2 1
Diethylphthalate ND ug/L 04/26/23 22:10 84-66-204/25/23 17:108.7 1.8 1
2,4-Dimethylphenol ND ug/L 04/26/23 22:10 105-67-904/25/23 17:108.7 1.5 1
Dimethylphthalate ND ug/L 04/26/23 22:10 131-11-304/25/23 17:108.7 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-5 Lab ID: 92663594015 Collected: 04/20/23 14:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 22:10 84-74-204/25/23 17:108.7 1.9 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 22:10 534-52-104/25/23 17:1017.4 6.8 1
2,4-Dinitrophenol ND ug/L 04/26/23 22:10 51-28-504/25/23 17:1043.5 22.6 1
2,4-Dinitrotoluene ND ug/L 04/26/23 22:10 121-14-204/25/23 17:108.7 1.4 1
2,6-Dinitrotoluene ND ug/L 04/26/23 22:10 606-20-204/25/23 17:108.7 1.5 1
Di-n-octylphthalate ND ug/L 04/26/23 22:10 117-84-004/25/23 17:108.7 3.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 22:10 117-81-704/25/23 17:105.2 3.2 1
Fluoranthene ND ug/L 04/26/23 22:10 206-44-004/25/23 17:108.7 1.9 1
Fluorene ND ug/L 04/26/23 22:10 86-73-704/25/23 17:108.7 1.8 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 22:10 87-68-304/25/23 17:108.7 1.5 1
Hexachlorobenzene ND ug/L 04/26/23 22:10 118-74-104/25/23 17:108.7 1.9 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 22:10 77-47-404/25/23 17:108.7 1.4 1
Hexachloroethane ND ug/L 04/26/23 22:10 67-72-104/25/23 17:108.7 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 22:10 193-39-504/25/23 17:108.7 2.5 1
Isophorone ND ug/L 04/26/23 22:10 78-59-104/25/23 17:108.7 1.4 1
1-Methylnaphthalene ND ug/L 04/26/23 22:10 90-12-004/25/23 17:108.7 1.8 1
2-Methylnaphthalene ND ug/L 04/26/23 22:10 91-57-604/25/23 17:108.7 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 22:10 95-48-704/25/23 17:108.7 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 22:10 15831-10-404/25/23 17:108.7 1.1 1
Naphthalene ND ug/L 04/26/23 22:10 91-20-304/25/23 17:108.7 1.8 1
2-Nitroaniline ND ug/L 04/26/23 22:10 88-74-404/25/23 17:1017.4 2.6 1
3-Nitroaniline ND ug/L 04/26/23 22:10 99-09-204/25/23 17:1017.4 3.3 1
4-Nitroaniline ND ug/L 04/26/23 22:10 100-01-604/25/23 17:1017.4 4.4 1
Nitrobenzene ND ug/L 04/26/23 22:10 98-95-304/25/23 17:108.7 1.6 1
2-Nitrophenol ND ug/L 04/26/23 22:10 88-75-504/25/23 17:108.7 1.2 1
4-Nitrophenol ND ug/L 04/26/23 22:10 100-02-704/25/23 17:1043.5 5.7 1
N-Nitrosodimethylamine ND ug/L 04/26/23 22:10 62-75-904/25/23 17:108.7 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 22:10 621-64-704/25/23 17:108.7 1.2 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 22:10 86-30-604/25/23 17:108.7 2.6 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 22:10 108-60-104/25/23 17:108.7 1.0 1
Pentachlorophenol ND ug/L 04/26/23 22:10 87-86-504/25/23 17:1017.4 3.3 1
Phenanthrene ND ug/L 04/26/23 22:10 85-01-804/25/23 17:108.7 1.7 1
Phenol ND ug/L 04/26/23 22:10 108-95-204/25/23 17:108.7 1.2 1
Pyrene ND ug/L 04/26/23 22:10 129-00-004/25/23 17:108.7 1.9 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 22:10 120-82-104/25/23 17:108.7 1.5 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 22:10 95-95-404/25/23 17:108.7 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 22:10 88-06-204/25/23 17:108.7 1.3 1
Surrogates
Nitrobenzene-d5 (S)55 %04/26/23 22:10 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)50 %04/26/23 22:10 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)96 %04/26/23 22:10 1718-51-004/25/23 17:1019-191 1
Phenol-d6 (S)34 %04/26/23 22:10 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)43 %04/26/23 22:10 367-12-404/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)84 %04/26/23 22:10 118-79-604/25/23 17:1010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-5 Lab ID: 92663594015 Collected: 04/20/23 14:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 08:19 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 08:19 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 08:19 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 08:19 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 08:19 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 08:19 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 08:19 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 08:19 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 08:19 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 08:19 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 08:19 75-00-31.0 0.65 1
Chloroform 1.3 ug/L 04/28/23 08:19 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 08:19 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 08:19 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 08:19 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 08:19 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 08:19 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 08:19 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 08:19 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 08:19 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 08:19 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 08:19 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 08:19 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 08:19 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 08:19 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 08:19 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.46J ug/L 04/28/23 08:19 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 08:19 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 08:19 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 08:19 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 08:19 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 08:19 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 08:19 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 08:19 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 08:19 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 08:19 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 08:19 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 08:19 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/28/23 08:19 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 08:19 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 08:19 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 08:19 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 08:19 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 08:19 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 08:19 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-5 Lab ID: 92663594015 Collected: 04/20/23 14:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 08:19 79-34-51.0 0.22 1
Tetrachloroethene 6.4 ug/L 04/28/23 08:19 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 08:19 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 08:19 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 08:19 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 08:19 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 08:19 79-00-51.0 0.32 1
Trichloroethene 12.2 ug/L 04/28/23 08:19 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 08:19 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 08:19 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 08:19 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 08:19 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 08:19 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 08:19 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 08:19 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %04/28/23 08:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %04/28/23 08:19 17060-07-070-130 1
Toluene-d8 (S)102 %04/28/23 08:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-6 Lab ID: 92663594016 Collected: 04/21/23 08:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Arsenic 0.13J ug/L 04/24/23 22:43 7440-38-204/23/23 16:541.0 0.087 1
Barium 45.7 ug/L 04/24/23 22:43 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:43 7440-43-904/23/23 16:540.20 0.060 1
Chromium ND ug/L 04/24/23 22:43 7440-47-304/23/23 16:541.0 0.50 1
Lead 0.078J ug/L 04/24/23 22:43 7439-92-104/23/23 16:541.0 0.077 1
Selenium 0.36J ug/L 04/24/23 22:43 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:43 7440-22-404/23/23 16:540.40 0.070 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 15:31 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 22:35 83-32-904/25/23 17:109.1 1.8 1
Acenaphthylene ND ug/L 04/26/23 22:35 208-96-804/25/23 17:109.1 1.8 1
Aniline ND ug/L 04/26/23 22:35 62-53-304/25/23 17:109.1 1.5 1
Anthracene ND ug/L 04/26/23 22:35 120-12-704/25/23 17:109.1 2.1 1
Benzo(a)anthracene ND ug/L 04/26/23 22:35 56-55-304/25/23 17:109.1 2.4 1
Benzo(a)pyrene ND ug/L 04/26/23 22:35 50-32-804/25/23 17:109.1 2.5 1
Benzo(b)fluoranthene ND ug/L 04/26/23 22:35 205-99-204/25/23 17:109.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 22:35 191-24-204/25/23 17:109.1 2.6 1
Benzo(k)fluoranthene ND ug/L 04/26/23 22:35 207-08-904/25/23 17:109.1 2.5 1
Benzoic Acid ND ug/L 04/26/23 22:35 65-85-004/25/23 17:1045.5 20.0 1
Benzyl alcohol ND ug/L 04/26/23 22:35 100-51-604/25/23 17:1018.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 22:35 101-55-304/25/23 17:109.1 1.6 1
Butylbenzylphthalate ND ug/L 04/26/23 22:35 85-68-704/25/23 17:109.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 22:35 59-50-704/25/23 17:109.1 3.0 1
4-Chloroaniline ND ug/L 04/26/23 22:35 106-47-804/25/23 17:1018.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 22:35 111-91-104/25/23 17:109.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 22:35 111-44-404/25/23 17:109.1 1.7 1
2-Chloronaphthalene ND ug/L 04/26/23 22:35 91-58-704/25/23 17:109.1 1.6 1
2-Chlorophenol ND ug/L 04/26/23 22:35 95-57-804/25/23 17:109.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 22:35 7005-72-304/25/23 17:109.1 1.8 1
Chrysene ND ug/L 04/26/23 22:35 218-01-904/25/23 17:109.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 22:35 53-70-304/25/23 17:109.1 2.7 1
Dibenzofuran ND ug/L 04/26/23 22:35 132-64-904/25/23 17:109.1 1.9 1
1,2-Dichlorobenzene ND ug/L 04/26/23 22:35 95-50-104/25/23 17:109.1 1.6 1
1,3-Dichlorobenzene ND ug/L 04/26/23 22:35 541-73-104/25/23 17:109.1 1.5 1
1,4-Dichlorobenzene ND ug/L 04/26/23 22:35 106-46-704/25/23 17:109.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 22:35 91-94-104/25/23 17:1018.2 7.4 1
2,4-Dichlorophenol ND ug/L 04/26/23 22:35 120-83-204/25/23 17:109.1 1.3 1
Diethylphthalate ND ug/L 04/26/23 22:35 84-66-204/25/23 17:109.1 1.9 1
2,4-Dimethylphenol ND ug/L 04/26/23 22:35 105-67-904/25/23 17:109.1 1.5 1
Dimethylphthalate ND ug/L 04/26/23 22:35 131-11-304/25/23 17:109.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-6 Lab ID: 92663594016 Collected: 04/21/23 08:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 04/26/23 22:35 84-74-204/25/23 17:109.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 22:35 534-52-104/25/23 17:1018.2 7.1 1
2,4-Dinitrophenol ND ug/L 04/26/23 22:35 51-28-504/25/23 17:1045.5 23.6 1
2,4-Dinitrotoluene ND ug/L 04/26/23 22:35 121-14-204/25/23 17:109.1 1.5 1
2,6-Dinitrotoluene ND ug/L 04/26/23 22:35 606-20-204/25/23 17:109.1 1.6 1
Di-n-octylphthalate ND ug/L 04/26/23 22:35 117-84-004/25/23 17:109.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 22:35 117-81-704/25/23 17:105.5 3.4 1
Fluoranthene ND ug/L 04/26/23 22:35 206-44-004/25/23 17:109.1 2.0 1
Fluorene ND ug/L 04/26/23 22:35 86-73-704/25/23 17:109.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 22:35 87-68-304/25/23 17:109.1 1.6 1
Hexachlorobenzene ND ug/L 04/26/23 22:35 118-74-104/25/23 17:109.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 22:35 77-47-404/25/23 17:109.1 1.4 1
Hexachloroethane ND ug/L 04/26/23 22:35 67-72-104/25/23 17:109.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 22:35 193-39-504/25/23 17:109.1 2.6 1
Isophorone ND ug/L 04/26/23 22:35 78-59-104/25/23 17:109.1 1.5 1
1-Methylnaphthalene ND ug/L 04/26/23 22:35 90-12-004/25/23 17:109.1 1.8 1
2-Methylnaphthalene ND ug/L 04/26/23 22:35 91-57-604/25/23 17:109.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 22:35 95-48-704/25/23 17:109.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 22:35 15831-10-404/25/23 17:109.1 1.1 1
Naphthalene ND ug/L 04/26/23 22:35 91-20-304/25/23 17:109.1 1.9 1
2-Nitroaniline ND ug/L 04/26/23 22:35 88-74-404/25/23 17:1018.2 2.7 1
3-Nitroaniline ND ug/L 04/26/23 22:35 99-09-204/25/23 17:1018.2 3.4 1
4-Nitroaniline ND ug/L 04/26/23 22:35 100-01-604/25/23 17:1018.2 4.6 1
Nitrobenzene ND ug/L 04/26/23 22:35 98-95-304/25/23 17:109.1 1.7 1
2-Nitrophenol ND ug/L 04/26/23 22:35 88-75-504/25/23 17:109.1 1.3 1
4-Nitrophenol ND ug/L 04/26/23 22:35 100-02-704/25/23 17:1045.5 6.0 1
N-Nitrosodimethylamine ND ug/L 04/26/23 22:35 62-75-904/25/23 17:109.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 22:35 621-64-704/25/23 17:109.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 22:35 86-30-604/25/23 17:109.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 22:35 108-60-104/25/23 17:109.1 1.0 1
Pentachlorophenol ND ug/L 04/26/23 22:35 87-86-504/25/23 17:1018.2 3.4 1
Phenanthrene ND ug/L 04/26/23 22:35 85-01-804/25/23 17:109.1 1.8 1
Phenol ND ug/L 04/26/23 22:35 108-95-204/25/23 17:109.1 1.2 1
Pyrene ND ug/L 04/26/23 22:35 129-00-004/25/23 17:109.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 22:35 120-82-104/25/23 17:109.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 22:35 95-95-404/25/23 17:109.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 22:35 88-06-204/25/23 17:109.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)92 %04/26/23 22:35 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)85 %04/26/23 22:35 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)97 %04/26/23 22:35 1718-51-004/25/23 17:1019-191 1
Phenol-d6 (S)31 %04/26/23 22:35 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)9 %04/26/23 22:35 367-12-4 S004/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)12 %04/26/23 22:35 118-79-604/25/23 17:1010-164 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-6 Lab ID: 92663594016 Collected: 04/21/23 08:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 08:37 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 08:37 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 08:37 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 08:37 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 08:37 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 08:37 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 08:37 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 08:37 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 08:37 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 08:37 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 08:37 75-00-31.0 0.65 1
Chloroform 1.8 ug/L 04/28/23 08:37 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 08:37 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 08:37 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 08:37 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 08:37 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 08:37 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 08:37 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 08:37 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 08:37 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 08:37 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 08:37 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 08:37 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 08:37 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 08:37 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 08:37 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/28/23 08:37 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 08:37 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 08:37 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 08:37 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 08:37 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 08:37 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 08:37 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 08:37 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 08:37 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 08:37 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 08:37 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 08:37 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/28/23 08:37 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 08:37 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 08:37 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 08:37 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 08:37 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 08:37 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 08:37 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-6 Lab ID: 92663594016 Collected: 04/21/23 08:25 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 08:37 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/28/23 08:37 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 08:37 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 08:37 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 08:37 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 08:37 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 08:37 79-00-51.0 0.32 1
Trichloroethene 8.5 ug/L 04/28/23 08:37 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 08:37 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 08:37 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 08:37 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 08:37 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 08:37 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 08:37 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 08:37 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)98 %04/28/23 08:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %04/28/23 08:37 17060-07-070-130 1
Toluene-d8 (S)105 %04/28/23 08:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-7 Lab ID: 92663594017 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Aluminum 342 ug/L 04/24/23 22:47 7429-90-504/23/23 16:5420.0 7.4 1
Arsenic 0.19J ug/L 04/24/23 22:47 7440-38-204/23/23 16:541.0 0.087 1
Barium 33.6 ug/L 04/24/23 22:47 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:47 7440-43-904/23/23 16:540.20 0.060 1
Chromium 0.73J ug/L 04/24/23 22:47 7440-47-304/23/23 16:541.0 0.50 1
Copper 1.3J ug/L 04/24/23 22:47 7440-50-804/23/23 16:542.0 1.1 1
Lead 0.081J ug/L 04/24/23 22:47 7439-92-104/23/23 16:541.0 0.077 1
Nickel 3.3 ug/L 04/24/23 22:47 7440-02-004/23/23 16:541.0 0.42 1
Selenium 0.27J ug/L 04/24/23 22:47 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:47 7440-22-404/23/23 16:540.40 0.070 1
Zinc ND ug/L 04/24/23 22:47 7440-66-604/23/23 16:5410.0 2.7 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 19:08 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/23/23 16:32 83-32-904/22/23 11:548.3 1.7 1
Acenaphthylene ND ug/L 04/23/23 16:32 208-96-804/22/23 11:548.3 1.6 1
Aniline ND ug/L 04/23/23 16:32 62-53-304/22/23 11:548.3 1.4 1
Anthracene ND ug/L 04/23/23 16:32 120-12-704/22/23 11:548.3 1.9 1
Benzo(a)anthracene ND ug/L 04/23/23 16:32 56-55-304/22/23 11:548.3 2.2 1
Benzo(a)pyrene ND ug/L 04/23/23 16:32 50-32-804/22/23 11:548.3 2.3 1
Benzo(b)fluoranthene ND ug/L 04/23/23 16:32 205-99-204/22/23 11:548.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 04/23/23 16:32 191-24-204/22/23 11:548.3 2.4 1
Benzo(k)fluoranthene ND ug/L 04/23/23 16:32 207-08-904/22/23 11:548.3 2.3 1
Benzoic Acid ND ug/L 04/23/23 16:32 65-85-004/22/23 11:5441.7 18.3 1
Benzyl alcohol ND ug/L 04/23/23 16:32 100-51-604/22/23 11:5416.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 04/23/23 16:32 101-55-304/22/23 11:548.3 1.5 1
Butylbenzylphthalate ND ug/L 04/23/23 16:32 85-68-704/22/23 11:548.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 04/23/23 16:32 59-50-704/22/23 11:548.3 2.8 1
4-Chloroaniline ND ug/L 04/23/23 16:32 106-47-804/22/23 11:5416.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/23/23 16:32 111-91-104/22/23 11:548.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 04/23/23 16:32 111-44-404/22/23 11:548.3 1.6 1
2-Chloronaphthalene ND ug/L 04/23/23 16:32 91-58-704/22/23 11:548.3 1.4 1
2-Chlorophenol ND ug/L 04/23/23 16:32 95-57-804/22/23 11:548.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/23/23 16:32 7005-72-304/22/23 11:548.3 1.7 1
Chrysene ND ug/L 04/23/23 16:32 218-01-904/22/23 11:548.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 04/23/23 16:32 53-70-304/22/23 11:548.3 2.5 1
Dibenzofuran ND ug/L 04/23/23 16:32 132-64-904/22/23 11:548.3 1.8 1
1,2-Dichlorobenzene ND ug/L 04/23/23 16:32 95-50-104/22/23 11:548.3 1.5 1
1,3-Dichlorobenzene ND ug/L 04/23/23 16:32 541-73-104/22/23 11:548.3 1.3 1
1,4-Dichlorobenzene ND ug/L 04/23/23 16:32 106-46-704/22/23 11:548.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 04/23/23 16:32 91-94-104/22/23 11:5416.7 6.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-7 Lab ID: 92663594017 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dichlorophenol ND ug/L 04/23/23 16:32 120-83-204/22/23 11:548.3 1.2 1
Diethylphthalate ND ug/L 04/23/23 16:32 84-66-204/22/23 11:548.3 1.7 1
2,4-Dimethylphenol ND ug/L 04/23/23 16:32 105-67-9 v204/22/23 11:548.3 1.4 1
Dimethylphthalate ND ug/L 04/23/23 16:32 131-11-304/22/23 11:548.3 1.8 1
Di-n-butylphthalate ND ug/L 04/23/23 16:32 84-74-204/22/23 11:548.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 04/23/23 16:32 534-52-104/22/23 11:5416.7 6.5 1
2,4-Dinitrophenol ND ug/L 04/23/23 16:32 51-28-504/22/23 11:5441.7 21.7 1
2,4-Dinitrotoluene ND ug/L 04/23/23 16:32 121-14-204/22/23 11:548.3 1.4 1
2,6-Dinitrotoluene ND ug/L 04/23/23 16:32 606-20-204/22/23 11:548.3 1.4 1
Di-n-octylphthalate ND ug/L 04/23/23 16:32 117-84-004/22/23 11:548.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/23/23 16:32 117-81-704/22/23 11:545.0 3.1 1
Fluoranthene ND ug/L 04/23/23 16:32 206-44-004/22/23 11:548.3 1.8 1
Fluorene ND ug/L 04/23/23 16:32 86-73-704/22/23 11:548.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 04/23/23 16:32 87-68-304/22/23 11:548.3 1.5 1
Hexachlorobenzene ND ug/L 04/23/23 16:32 118-74-104/22/23 11:548.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 04/23/23 16:32 77-47-404/22/23 11:548.3 1.3 1
Hexachloroethane ND ug/L 04/23/23 16:32 67-72-104/22/23 11:548.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/23/23 16:32 193-39-504/22/23 11:548.3 2.4 1
Isophorone ND ug/L 04/23/23 16:32 78-59-104/22/23 11:548.3 1.4 1
1-Methylnaphthalene ND ug/L 04/23/23 16:32 90-12-004/22/23 11:548.3 1.7 1
2-Methylnaphthalene ND ug/L 04/23/23 16:32 91-57-604/22/23 11:548.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/23/23 16:32 95-48-704/22/23 11:548.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/23/23 16:32 15831-10-404/22/23 11:548.3 1.0 1
Naphthalene ND ug/L 04/23/23 16:32 91-20-304/22/23 11:548.3 1.7 1
2-Nitroaniline ND ug/L 04/23/23 16:32 88-74-404/22/23 11:5416.7 2.5 1
3-Nitroaniline ND ug/L 04/23/23 16:32 99-09-204/22/23 11:5416.7 3.1 1
4-Nitroaniline ND ug/L 04/23/23 16:32 100-01-604/22/23 11:5416.7 4.2 1
Nitrobenzene ND ug/L 04/23/23 16:32 98-95-304/22/23 11:548.3 1.6 1
2-Nitrophenol ND ug/L 04/23/23 16:32 88-75-504/22/23 11:548.3 1.2 1
4-Nitrophenol ND ug/L 04/23/23 16:32 100-02-704/22/23 11:5441.7 5.5 1
N-Nitrosodimethylamine ND ug/L 04/23/23 16:32 62-75-904/22/23 11:548.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/23/23 16:32 621-64-704/22/23 11:548.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 04/23/23 16:32 86-30-604/22/23 11:548.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/23/23 16:32 108-60-104/22/23 11:548.3 0.96 1
Pentachlorophenol ND ug/L 04/23/23 16:32 87-86-504/22/23 11:5416.7 3.1 1
Phenanthrene ND ug/L 04/23/23 16:32 85-01-804/22/23 11:548.3 1.7 1
Phenol ND ug/L 04/23/23 16:32 108-95-204/22/23 11:548.3 1.1 1
Pyrene ND ug/L 04/23/23 16:32 129-00-004/22/23 11:548.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 04/23/23 16:32 120-82-104/22/23 11:548.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 04/23/23 16:32 95-95-404/22/23 11:548.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/23/23 16:32 88-06-204/22/23 11:548.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)24 %04/23/23 16:32 4165-60-004/22/23 11:5410-138 1
2-Fluorobiphenyl (S)20 %04/23/23 16:32 321-60-804/22/23 11:5410-130 1
Terphenyl-d14 (S)53 %04/23/23 16:32 1718-51-004/22/23 11:5419-191 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-7 Lab ID: 92663594017 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Phenol-d6 (S)10 %04/23/23 16:32 13127-88-304/22/23 11:5410-130 1
2-Fluorophenol (S)15 %04/23/23 16:32 367-12-404/22/23 11:5410-130 1
2,4,6-Tribromophenol (S)31 %04/23/23 16:32 118-79-604/22/23 11:5410-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 08:55 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 08:55 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 08:55 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 08:55 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 08:55 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 08:55 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 08:55 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 08:55 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 08:55 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 08:55 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 08:55 75-00-31.0 0.65 1
Chloroform 0.57J ug/L 04/28/23 08:55 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 08:55 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 08:55 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 08:55 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 08:55 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 08:55 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 08:55 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 08:55 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 08:55 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 08:55 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 08:55 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 08:55 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 08:55 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 08:55 107-06-21.0 0.32 1
1,1-Dichloroethene 0.75J ug/L 04/28/23 08:55 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.45J ug/L 04/28/23 08:55 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 08:55 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 08:55 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 08:55 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 08:55 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 08:55 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 08:55 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 08:55 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 08:55 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 08:55 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 08:55 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 08:55 591-78-65.0 0.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-7 Lab ID: 92663594017 Collected: 04/18/23 15:30 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
p-Isopropyltoluene ND ug/L 04/28/23 08:55 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 08:55 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 08:55 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 08:55 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 08:55 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 08:55 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 08:55 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 08:55 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/28/23 08:55 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 08:55 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 08:55 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 08:55 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 08:55 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 08:55 79-00-51.0 0.32 1
Trichloroethene 18.7 ug/L 04/28/23 08:55 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 08:55 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 08:55 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 08:55 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 08:55 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 08:55 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 08:55 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 08:55 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)95 %04/28/23 08:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)113 %04/28/23 08:55 17060-07-070-130 1
Toluene-d8 (S)102 %04/28/23 08:55 2037-26-570-130 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide ND mg/L 04/24/23 19:57 57-12-504/24/23 16:480.0080 0.0060 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-8 Lab ID: 92663594018 Collected: 04/20/23 09:55 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Aluminum 231 ug/L 04/24/23 22:51 7429-90-504/23/23 16:5420.0 7.4 1
Arsenic 0.098J ug/L 04/24/23 22:51 7440-38-204/23/23 16:541.0 0.087 1
Barium 33.4 ug/L 04/24/23 22:51 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 22:51 7440-43-904/23/23 16:540.20 0.060 1
Chromium 1.2 ug/L 04/24/23 22:51 7440-47-304/23/23 16:541.0 0.50 1
Copper 1.7J ug/L 04/24/23 22:51 7440-50-804/23/23 16:542.0 1.1 1
Lead ND ug/L 04/24/23 22:51 7439-92-104/23/23 16:541.0 0.077 1
Nickel 4.2 ug/L 04/24/23 22:51 7440-02-004/23/23 16:541.0 0.42 1
Selenium 0.076J ug/L 04/24/23 22:51 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 22:51 7440-22-404/23/23 16:540.40 0.070 1
Zinc 2.8J ug/L 04/24/23 22:51 7440-66-604/23/23 16:5410.0 2.7 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 19:10 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/26/23 23:00 83-32-904/25/23 17:108.3 1.7 1
Acenaphthylene ND ug/L 04/26/23 23:00 208-96-804/25/23 17:108.3 1.6 1
Aniline ND ug/L 04/26/23 23:00 62-53-304/25/23 17:108.3 1.4 1
Anthracene ND ug/L 04/26/23 23:00 120-12-704/25/23 17:108.3 1.9 1
Benzo(a)anthracene ND ug/L 04/26/23 23:00 56-55-304/25/23 17:108.3 2.2 1
Benzo(a)pyrene ND ug/L 04/26/23 23:00 50-32-804/25/23 17:108.3 2.3 1
Benzo(b)fluoranthene ND ug/L 04/26/23 23:00 205-99-204/25/23 17:108.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 04/26/23 23:00 191-24-204/25/23 17:108.3 2.4 1
Benzo(k)fluoranthene ND ug/L 04/26/23 23:00 207-08-904/25/23 17:108.3 2.3 1
Benzoic Acid ND ug/L 04/26/23 23:00 65-85-004/25/23 17:1041.7 18.3 1
Benzyl alcohol ND ug/L 04/26/23 23:00 100-51-604/25/23 17:1016.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 04/26/23 23:00 101-55-304/25/23 17:108.3 1.5 1
Butylbenzylphthalate ND ug/L 04/26/23 23:00 85-68-704/25/23 17:108.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 04/26/23 23:00 59-50-704/25/23 17:108.3 2.8 1
4-Chloroaniline ND ug/L 04/26/23 23:00 106-47-804/25/23 17:1016.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/26/23 23:00 111-91-104/25/23 17:108.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 04/26/23 23:00 111-44-404/25/23 17:108.3 1.6 1
2-Chloronaphthalene ND ug/L 04/26/23 23:00 91-58-704/25/23 17:108.3 1.4 1
2-Chlorophenol ND ug/L 04/26/23 23:00 95-57-804/25/23 17:108.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/26/23 23:00 7005-72-304/25/23 17:108.3 1.7 1
Chrysene ND ug/L 04/26/23 23:00 218-01-904/25/23 17:108.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 04/26/23 23:00 53-70-304/25/23 17:108.3 2.5 1
Dibenzofuran ND ug/L 04/26/23 23:00 132-64-904/25/23 17:108.3 1.8 1
1,2-Dichlorobenzene ND ug/L 04/26/23 23:00 95-50-104/25/23 17:108.3 1.5 1
1,3-Dichlorobenzene ND ug/L 04/26/23 23:00 541-73-104/25/23 17:108.3 1.3 1
1,4-Dichlorobenzene ND ug/L 04/26/23 23:00 106-46-704/25/23 17:108.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 04/26/23 23:00 91-94-104/25/23 17:1016.7 6.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-8 Lab ID: 92663594018 Collected: 04/20/23 09:55 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dichlorophenol ND ug/L 04/26/23 23:00 120-83-204/25/23 17:108.3 1.2 1
Diethylphthalate ND ug/L 04/26/23 23:00 84-66-204/25/23 17:108.3 1.7 1
2,4-Dimethylphenol ND ug/L 04/26/23 23:00 105-67-904/25/23 17:108.3 1.4 1
Dimethylphthalate ND ug/L 04/26/23 23:00 131-11-304/25/23 17:108.3 1.8 1
Di-n-butylphthalate ND ug/L 04/26/23 23:00 84-74-204/25/23 17:108.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 04/26/23 23:00 534-52-104/25/23 17:1016.7 6.5 1
2,4-Dinitrophenol ND ug/L 04/26/23 23:00 51-28-504/25/23 17:1041.7 21.7 1
2,4-Dinitrotoluene ND ug/L 04/26/23 23:00 121-14-204/25/23 17:108.3 1.4 1
2,6-Dinitrotoluene ND ug/L 04/26/23 23:00 606-20-204/25/23 17:108.3 1.4 1
Di-n-octylphthalate ND ug/L 04/26/23 23:00 117-84-004/25/23 17:108.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/26/23 23:00 117-81-704/25/23 17:105.0 3.1 1
Fluoranthene ND ug/L 04/26/23 23:00 206-44-004/25/23 17:108.3 1.8 1
Fluorene ND ug/L 04/26/23 23:00 86-73-704/25/23 17:108.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 04/26/23 23:00 87-68-304/25/23 17:108.3 1.5 1
Hexachlorobenzene ND ug/L 04/26/23 23:00 118-74-104/25/23 17:108.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 04/26/23 23:00 77-47-404/25/23 17:108.3 1.3 1
Hexachloroethane ND ug/L 04/26/23 23:00 67-72-104/25/23 17:108.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/26/23 23:00 193-39-504/25/23 17:108.3 2.4 1
Isophorone ND ug/L 04/26/23 23:00 78-59-104/25/23 17:108.3 1.4 1
1-Methylnaphthalene ND ug/L 04/26/23 23:00 90-12-004/25/23 17:108.3 1.7 1
2-Methylnaphthalene ND ug/L 04/26/23 23:00 91-57-604/25/23 17:108.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/26/23 23:00 95-48-704/25/23 17:108.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/26/23 23:00 15831-10-404/25/23 17:108.3 1.0 1
Naphthalene ND ug/L 04/26/23 23:00 91-20-304/25/23 17:108.3 1.7 1
2-Nitroaniline ND ug/L 04/26/23 23:00 88-74-404/25/23 17:1016.7 2.5 1
3-Nitroaniline ND ug/L 04/26/23 23:00 99-09-204/25/23 17:1016.7 3.1 1
4-Nitroaniline ND ug/L 04/26/23 23:00 100-01-604/25/23 17:1016.7 4.2 1
Nitrobenzene ND ug/L 04/26/23 23:00 98-95-304/25/23 17:108.3 1.6 1
2-Nitrophenol ND ug/L 04/26/23 23:00 88-75-504/25/23 17:108.3 1.2 1
4-Nitrophenol ND ug/L 04/26/23 23:00 100-02-704/25/23 17:1041.7 5.5 1
N-Nitrosodimethylamine ND ug/L 04/26/23 23:00 62-75-904/25/23 17:108.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/26/23 23:00 621-64-704/25/23 17:108.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 04/26/23 23:00 86-30-604/25/23 17:108.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/26/23 23:00 108-60-104/25/23 17:108.3 0.96 1
Pentachlorophenol ND ug/L 04/26/23 23:00 87-86-504/25/23 17:1016.7 3.1 1
Phenanthrene ND ug/L 04/26/23 23:00 85-01-804/25/23 17:108.3 1.7 1
Phenol ND ug/L 04/26/23 23:00 108-95-204/25/23 17:108.3 1.1 1
Pyrene ND ug/L 04/26/23 23:00 129-00-004/25/23 17:108.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 04/26/23 23:00 120-82-104/25/23 17:108.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 04/26/23 23:00 95-95-404/25/23 17:108.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/26/23 23:00 88-06-204/25/23 17:108.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)102 %04/26/23 23:00 4165-60-004/25/23 17:1010-138 1
2-Fluorobiphenyl (S)94 %04/26/23 23:00 321-60-804/25/23 17:1010-130 1
Terphenyl-d14 (S)107 %04/26/23 23:00 1718-51-004/25/23 17:1019-191 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-8 Lab ID: 92663594018 Collected: 04/20/23 09:55 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Phenol-d6 (S)55 %04/26/23 23:00 13127-88-304/25/23 17:1010-130 1
2-Fluorophenol (S)49 %04/26/23 23:00 367-12-404/25/23 17:1010-130 1
2,4,6-Tribromophenol (S)66 %04/26/23 23:00 118-79-604/25/23 17:1010-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 09:14 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 09:14 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 09:14 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 09:14 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 09:14 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 09:14 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 09:14 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 09:14 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 09:14 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 09:14 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 09:14 75-00-31.0 0.65 1
Chloroform 0.80J ug/L 04/28/23 09:14 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 09:14 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 09:14 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 09:14 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 09:14 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 09:14 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 09:14 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 09:14 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 09:14 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 09:14 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 09:14 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 09:14 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 09:14 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 09:14 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 09:14 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/28/23 09:14 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 09:14 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 09:14 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 09:14 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 09:14 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 09:14 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 09:14 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 09:14 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 09:14 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 09:14 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 09:14 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 09:14 591-78-65.0 0.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-TMW-8 Lab ID: 92663594018 Collected: 04/20/23 09:55 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
p-Isopropyltoluene ND ug/L 04/28/23 09:14 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 09:14 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 09:14 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 09:14 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 09:14 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 09:14 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 09:14 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 09:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/28/23 09:14 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 09:14 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 09:14 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 09:14 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 09:14 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 09:14 79-00-51.0 0.32 1
Trichloroethene ND ug/L 04/28/23 09:14 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 09:14 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 09:14 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 09:14 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 09:14 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 09:14 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 09:14 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 09:14 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)95 %04/28/23 09:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %04/28/23 09:14 17060-07-070-130 1
Toluene-d8 (S)104 %04/28/23 09:14 2037-26-570-130 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide ND mg/L 04/24/23 19:58 57-12-504/24/23 16:480.0080 0.0060 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-DUP Lab ID: 92663594019 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Aluminum 20500 mg/kg 04/28/23 10:04 7429-90-504/26/23 11:0436.7 7.5 1
Arsenic 2.0 mg/kg 04/27/23 16:19 7440-38-204/26/23 11:040.61 0.18 1
Barium 49.4 mg/kg 04/27/23 16:19 7440-39-304/26/23 11:040.37 0.092 1
Cadmium 0.066J mg/kg 04/27/23 16:19 7440-43-904/26/23 11:040.098 0.036 1
Chromium 77.1 mg/kg 04/27/23 16:19 7440-47-304/26/23 11:042.4 0.48 1
Copper 40.7 mg/kg 04/27/23 16:19 7440-50-804/26/23 11:041.2 0.37 1
Lead 38.2 mg/kg 04/27/23 16:19 7439-92-104/26/23 11:040.61 0.11 1
Nickel 15.7 mg/kg 04/27/23 16:19 7440-02-004/26/23 11:040.61 0.28 1
Selenium 0.53J mg/kg 04/27/23 16:19 7782-49-204/26/23 11:040.61 0.13 1
Silver ND mg/kg 04/27/23 16:19 7440-22-404/26/23 11:040.61 0.25 1
Zinc 33.8 mg/kg 04/27/23 16:19 7440-66-604/26/23 11:046.1 1.4 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.045 mg/kg 04/28/23 09:20 7439-97-604/26/23 11:070.021 0.0093 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/27/23 17:01 83-32-904/26/23 15:38412 145 1
Acenaphthylene ND ug/kg 04/27/23 17:01 208-96-804/26/23 15:38412 145 1
Aniline ND ug/kg 04/27/23 17:01 62-53-304/26/23 15:38412 161 1
Anthracene ND ug/kg 04/27/23 17:01 120-12-704/26/23 15:38412 135 1
Benzo(a)anthracene 366J ug/kg 04/27/23 17:01 56-55-304/26/23 15:38412 137 1
Benzo(a)pyrene 323J ug/kg 04/27/23 17:01 50-32-804/26/23 15:38412 142 1
Benzo(b)fluoranthene 471 ug/kg 04/27/23 17:01 205-99-204/26/23 15:38412 137 1
Benzo(g,h,i)perylene 230J ug/kg 04/27/23 17:01 191-24-204/26/23 15:38412 160 1
Benzo(k)fluoranthene 182J ug/kg 04/27/23 17:01 207-08-904/26/23 15:38412 145 1
Benzoic Acid ND ug/kg 04/27/23 17:01 65-85-004/26/23 15:382060 885 1
Benzyl alcohol ND ug/kg 04/27/23 17:01 100-51-604/26/23 15:38823 312 1
4-Bromophenylphenyl ether ND ug/kg 04/27/23 17:01 101-55-304/26/23 15:38412 158 1
Butylbenzylphthalate ND ug/kg 04/27/23 17:01 85-68-704/26/23 15:38412 173 1
4-Chloro-3-methylphenol ND ug/kg 04/27/23 17:01 59-50-704/26/23 15:38823 289 1
4-Chloroaniline ND ug/kg 04/27/23 17:01 106-47-804/26/23 15:38823 323 1
bis(2-Chloroethoxy)methane ND ug/kg 04/27/23 17:01 111-91-104/26/23 15:38412 171 1
bis(2-Chloroethyl) ether ND ug/kg 04/27/23 17:01 111-44-404/26/23 15:38412 155 1
2-Chloronaphthalene ND ug/kg 04/27/23 17:01 91-58-704/26/23 15:38412 163 1
2-Chlorophenol ND ug/kg 04/27/23 17:01 95-57-804/26/23 15:38412 155 1
4-Chlorophenylphenyl ether ND ug/kg 04/27/23 17:01 7005-72-304/26/23 15:38412 153 1
Chrysene 360J ug/kg 04/27/23 17:01 218-01-904/26/23 15:38412 150 1
Dibenz(a,h)anthracene ND ug/kg 04/27/23 17:01 53-70-304/26/23 15:38412 158 1
Dibenzofuran ND ug/kg 04/27/23 17:01 132-64-904/26/23 15:38412 148 1
1,2-Dichlorobenzene ND ug/kg 04/27/23 17:01 95-50-104/26/23 15:38412 148 1
1,3-Dichlorobenzene ND ug/kg 04/27/23 17:01 541-73-104/26/23 15:38412 146 1
1,4-Dichlorobenzene ND ug/kg 04/27/23 17:01 106-46-7 L204/26/23 15:38412 157 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-DUP Lab ID: 92663594019 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND ug/kg 04/27/23 17:01 91-94-104/26/23 15:38823 278 1
2,4-Dichlorophenol ND ug/kg 04/27/23 17:01 120-83-204/26/23 15:38412 161 1
Diethylphthalate ND ug/kg 04/27/23 17:01 84-66-204/26/23 15:38412 151 1
2,4-Dimethylphenol ND ug/kg 04/27/23 17:01 105-67-904/26/23 15:38412 171 1
Dimethylphthalate ND ug/kg 04/27/23 17:01 131-11-304/26/23 15:38412 150 1
Di-n-butylphthalate ND ug/kg 04/27/23 17:01 84-74-204/26/23 15:38412 138 1
4,6-Dinitro-2-methylphenol ND ug/kg 04/27/23 17:01 534-52-104/26/23 15:38823 384 1
2,4-Dinitrophenol ND ug/kg 04/27/23 17:01 51-28-504/26/23 15:382060 1270 1
2,4-Dinitrotoluene ND ug/kg 04/27/23 17:01 121-14-204/26/23 15:38412 158 1
2,6-Dinitrotoluene ND ug/kg 04/27/23 17:01 606-20-204/26/23 15:38412 151 1
Di-n-octylphthalate ND ug/kg 04/27/23 17:01 117-84-004/26/23 15:38412 162 1
bis(2-Ethylhexyl)phthalate ND ug/kg 04/27/23 17:01 117-81-704/26/23 15:38412 160 1
Fluoranthene 628 ug/kg 04/27/23 17:01 206-44-004/26/23 15:38412 141 1
Fluorene ND ug/kg 04/27/23 17:01 86-73-704/26/23 15:38412 145 1
Hexachloro-1,3-butadiene ND ug/kg 04/27/23 17:01 87-68-304/26/23 15:38412 178 1
Hexachlorobenzene ND ug/kg 04/27/23 17:01 118-74-104/26/23 15:38412 161 1
Hexachlorocyclopentadiene ND ug/kg 04/27/23 17:01 77-47-404/26/23 15:38412 236 1
Hexachloroethane ND ug/kg 04/27/23 17:01 67-72-104/26/23 15:38412 157 1
Indeno(1,2,3-cd)pyrene 212J ug/kg 04/27/23 17:01 193-39-504/26/23 15:38412 162 1
Isophorone ND ug/kg 04/27/23 17:01 78-59-104/26/23 15:38412 183 1
1-Methylnaphthalene ND ug/kg 04/27/23 17:01 90-12-004/26/23 15:38412 145 1
2-Methylnaphthalene ND ug/kg 04/27/23 17:01 91-57-604/26/23 15:38412 165 1
2-Methylphenol(o-Cresol)ND ug/kg 04/27/23 17:01 95-48-704/26/23 15:38412 168 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/27/23 17:01 15831-10-404/26/23 15:38412 166 1
Naphthalene ND ug/kg 04/27/23 17:01 91-20-304/26/23 15:38412 140 1
2-Nitroaniline ND ug/kg 04/27/23 17:01 88-74-404/26/23 15:382060 337 1
3-Nitroaniline ND ug/kg 04/27/23 17:01 99-09-204/26/23 15:382060 323 1
4-Nitroaniline ND ug/kg 04/27/23 17:01 100-01-604/26/23 15:38823 313 1
Nitrobenzene ND ug/kg 04/27/23 17:01 98-95-304/26/23 15:38412 191 1
2-Nitrophenol ND ug/kg 04/27/23 17:01 88-75-504/26/23 15:38412 178 1
4-Nitrophenol ND ug/kg 04/27/23 17:01 100-02-704/26/23 15:382060 796 1
N-Nitrosodimethylamine ND ug/kg 04/27/23 17:01 62-75-904/26/23 15:38412 138 1
N-Nitroso-di-n-propylamine ND ug/kg 04/27/23 17:01 621-64-704/26/23 15:38412 155 1
N-Nitrosodiphenylamine ND ug/kg 04/27/23 17:01 86-30-604/26/23 15:38412 146 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/27/23 17:01 108-60-104/26/23 15:38412 196 1
Pentachlorophenol ND ug/kg 04/27/23 17:01 87-86-504/26/23 15:38823 403 1
Phenanthrene 500 ug/kg 04/27/23 17:01 85-01-804/26/23 15:38412 135 1
Phenol ND ug/kg 04/27/23 17:01 108-95-204/26/23 15:38412 183 1
Pyrene 642 ug/kg 04/27/23 17:01 129-00-004/26/23 15:38412 167 1
Pyridine ND ug/kg 04/27/23 17:01 110-86-104/26/23 15:38412 130 1
1,2,4-Trichlorobenzene ND ug/kg 04/27/23 17:01 120-82-104/26/23 15:38412 162 1
2,4,5-Trichlorophenol ND ug/kg 04/27/23 17:01 95-95-404/26/23 15:38412 188 1
2,4,6-Trichlorophenol ND ug/kg 04/27/23 17:01 88-06-204/26/23 15:38412 170 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-DUP Lab ID: 92663594019 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Nitrobenzene-d5 (S)64 %04/27/23 17:01 4165-60-004/26/23 15:3810-130 1
2-Fluorobiphenyl (S)62 %04/27/23 17:01 321-60-804/26/23 15:3810-130 1
Terphenyl-d14 (S)82 %04/27/23 17:01 1718-51-004/26/23 15:3810-130 1
Phenol-d6 (S)58 %04/27/23 17:01 13127-88-304/26/23 15:3810-130 1
2-Fluorophenol (S)56 %04/27/23 17:01 367-12-404/26/23 15:3810-130 1
2,4,6-Tribromophenol (S)73 %04/27/23 17:01 118-79-604/26/23 15:3810-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/25/23 21:57 67-64-104/25/23 14:47221 70.8 1
Benzene ND ug/kg 04/25/23 21:57 71-43-204/25/23 14:4711.0 4.4 1
Bromobenzene ND ug/kg 04/25/23 21:57 108-86-104/25/23 14:4711.0 3.6 1
Bromochloromethane ND ug/kg 04/25/23 21:57 74-97-504/25/23 14:4711.0 3.3 1
Bromodichloromethane ND ug/kg 04/25/23 21:57 75-27-404/25/23 14:4711.0 4.3 1
Bromoform ND ug/kg 04/25/23 21:57 75-25-204/25/23 14:4711.0 3.9 1
Bromomethane ND ug/kg 04/25/23 21:57 74-83-9 IK04/25/23 14:4744.1 34.2 1
2-Butanone (MEK)ND ug/kg 04/25/23 21:57 78-93-304/25/23 14:47221 53.0 1
n-Butylbenzene ND ug/kg 04/25/23 21:57 104-51-804/25/23 14:4711.0 7.0 1
sec-Butylbenzene ND ug/kg 04/25/23 21:57 135-98-804/25/23 14:4711.0 4.9 1
tert-Butylbenzene ND ug/kg 04/25/23 21:57 98-06-604/25/23 14:4711.0 3.9 1
Carbon tetrachloride ND ug/kg 04/25/23 21:57 56-23-504/25/23 14:4711.0 4.1 1
Chlorobenzene ND ug/kg 04/25/23 21:57 108-90-704/25/23 14:4711.0 6.3 1
Chloroethane ND ug/kg 04/25/23 21:57 75-00-304/25/23 14:4722.1 8.5 1
Chloroform ND ug/kg 04/25/23 21:57 67-66-304/25/23 14:4711.0 9.2 1
Chloromethane ND ug/kg 04/25/23 21:57 74-87-304/25/23 14:4722.1 9.3 1
2-Chlorotoluene ND ug/kg 04/25/23 21:57 95-49-804/25/23 14:4711.0 3.9 1
4-Chlorotoluene ND ug/kg 04/25/23 21:57 106-43-404/25/23 14:4711.0 6.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/25/23 21:57 96-12-804/25/23 14:4711.0 4.3 1
Dibromochloromethane ND ug/kg 04/25/23 21:57 124-48-104/25/23 14:4711.0 6.2 1
1,2-Dibromoethane (EDB)ND ug/kg 04/25/23 21:57 106-93-404/25/23 14:4711.0 4.9 1
Dibromomethane ND ug/kg 04/25/23 21:57 74-95-304/25/23 14:4711.0 2.4 1
1,2-Dichlorobenzene ND ug/kg 04/25/23 21:57 95-50-104/25/23 14:4711.0 4.0 1
1,3-Dichlorobenzene ND ug/kg 04/25/23 21:57 541-73-104/25/23 14:4711.0 3.4 1
1,4-Dichlorobenzene ND ug/kg 04/25/23 21:57 106-46-704/25/23 14:4711.0 2.9 1
Dichlorodifluoromethane ND ug/kg 04/25/23 21:57 75-71-804/25/23 14:4722.1 11.2 1
1,1-Dichloroethane ND ug/kg 04/25/23 21:57 75-34-304/25/23 14:4711.0 4.5 1
1,2-Dichloroethane ND ug/kg 04/25/23 21:57 107-06-204/25/23 14:4711.0 7.3 1
1,1-Dichloroethene ND ug/kg 04/25/23 21:57 75-35-404/25/23 14:4711.0 4.5 1
cis-1,2-Dichloroethene ND ug/kg 04/25/23 21:57 156-59-204/25/23 14:4711.0 3.8 1
trans-1,2-Dichloroethene ND ug/kg 04/25/23 21:57 156-60-504/25/23 14:4711.0 9.4 1
1,2-Dichloropropane ND ug/kg 04/25/23 21:57 78-87-504/25/23 14:4711.0 3.3 1
1,3-Dichloropropane ND ug/kg 04/25/23 21:57 142-28-904/25/23 14:4711.0 3.4 1
2,2-Dichloropropane ND ug/kg 04/25/23 21:57 594-20-7 v204/25/23 14:4711.0 8.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-DUP Lab ID: 92663594019 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND ug/kg 04/25/23 21:57 563-58-604/25/23 14:4711.0 5.3 1
cis-1,3-Dichloropropene ND ug/kg 04/25/23 21:57 10061-01-504/25/23 14:4711.0 3.0 1
trans-1,3-Dichloropropene ND ug/kg 04/25/23 21:57 10061-02-604/25/23 14:4711.0 3.8 1
Diisopropyl ether ND ug/kg 04/25/23 21:57 108-20-304/25/23 14:4711.0 3.0 1
Ethylbenzene ND ug/kg 04/25/23 21:57 100-41-404/25/23 14:4711.0 5.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/25/23 21:57 87-68-304/25/23 14:4722.1 18.0 1
2-Hexanone ND ug/kg 04/25/23 21:57 591-78-604/25/23 14:47110 10.6 1
Isopropylbenzene (Cumene)ND ug/kg 04/25/23 21:57 98-82-804/25/23 14:4711.0 3.8 1
p-Isopropyltoluene ND ug/kg 04/25/23 21:57 99-87-604/25/23 14:4711.0 5.4 1
Methylene Chloride 52.4 ug/kg 04/25/23 21:57 75-09-2 C904/25/23 14:4744.1 30.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/25/23 21:57 108-10-104/25/23 14:47110 10.6 1
Methyl-tert-butyl ether ND ug/kg 04/25/23 21:57 1634-04-4 v204/25/23 14:4711.0 4.1 1
Naphthalene ND ug/kg 04/25/23 21:57 91-20-304/25/23 14:4711.0 5.8 1
n-Propylbenzene ND ug/kg 04/25/23 21:57 103-65-104/25/23 14:4711.0 3.9 1
Styrene ND ug/kg 04/25/23 21:57 100-42-504/25/23 14:4711.0 2.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/25/23 21:57 630-20-604/25/23 14:4711.0 4.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/25/23 21:57 79-34-504/25/23 14:4711.0 2.9 1
Tetrachloroethene ND ug/kg 04/25/23 21:57 127-18-404/25/23 14:4711.0 3.5 1
Toluene ND ug/kg 04/25/23 21:57 108-88-304/25/23 14:4711.0 7.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/25/23 21:57 87-61-604/25/23 14:4711.0 8.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/25/23 21:57 120-82-104/25/23 14:4711.0 9.3 1
1,1,1-Trichloroethane ND ug/kg 04/25/23 21:57 71-55-604/25/23 14:4711.0 5.7 1
1,1,2-Trichloroethane ND ug/kg 04/25/23 21:57 79-00-504/25/23 14:4711.0 3.7 1
Trichloroethene ND ug/kg 04/25/23 21:57 79-01-604/25/23 14:4711.0 8.9 1
Trichlorofluoromethane ND ug/kg 04/25/23 21:57 75-69-404/25/23 14:4711.0 6.1 1
1,2,3-Trichloropropane ND ug/kg 04/25/23 21:57 96-18-404/25/23 14:4711.0 5.6 1
1,2,4-Trimethylbenzene ND ug/kg 04/25/23 21:57 95-63-604/25/23 14:4711.0 6.6 1
1,3,5-Trimethylbenzene ND ug/kg 04/25/23 21:57 108-67-804/25/23 14:4711.0 3.7 1
Vinyl acetate ND ug/kg 04/25/23 21:57 108-05-404/25/23 14:47110 22.7 1
Vinyl chloride ND ug/kg 04/25/23 21:57 75-01-4 v204/25/23 14:4722.1 5.6 1
Xylene (Total)ND ug/kg 04/25/23 21:57 1330-20-704/25/23 14:4722.1 6.3 1
m&p-Xylene ND ug/kg 04/25/23 21:57 179601-23-104/25/23 14:4722.1 7.5 1
o-Xylene ND ug/kg 04/25/23 21:57 95-47-604/25/23 14:4711.0 4.9 1
Surrogates
Toluene-d8 (S)100 %04/25/23 21:57 2037-26-504/25/23 14:4770-130 1
4-Bromofluorobenzene (S)99 %04/25/23 21:57 460-00-404/25/23 14:4770-130 1
1,2-Dichloroethane-d4 (S)95 %04/25/23 21:57 17060-07-004/25/23 14:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.3 %04/21/23 17:16 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-SB-DUP Lab ID: 92663594019 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.9 %04/27/23 17:1504/27/23 17:001
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.75 mg/kg 05/01/23 14:45 18540-29-904/30/23 06:541.27 0.323 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide 0.33J mg/kg 05/01/23 15:53 57-12-5 B05/01/23 12:360.37 0.19 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-GW-DUP Lab ID: 92663594020 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Aluminum 349 ug/L 04/24/23 23:02 7429-90-504/23/23 16:5420.0 7.4 1
Arsenic 0.18J ug/L 04/24/23 23:02 7440-38-204/23/23 16:541.0 0.087 1
Barium 36.6 ug/L 04/26/23 13:58 7440-39-304/23/23 16:541.0 0.21 1
Cadmium ND ug/L 04/24/23 23:02 7440-43-904/23/23 16:540.20 0.060 1
Chromium 0.79J ug/L 04/24/23 23:02 7440-47-304/23/23 16:541.0 0.50 1
Copper 1.3J ug/L 04/24/23 23:02 7440-50-804/23/23 16:542.0 1.1 1
Lead ND ug/L 04/24/23 23:02 7439-92-104/23/23 16:541.0 0.077 1
Nickel 3.3 ug/L 04/24/23 23:02 7440-02-004/23/23 16:541.0 0.42 1
Selenium 0.25J ug/L 04/24/23 23:02 7782-49-204/23/23 16:542.0 0.072 1
Silver ND ug/L 04/24/23 23:02 7440-22-404/23/23 16:540.40 0.070 1
Zinc ND ug/L 04/24/23 23:02 7440-66-604/23/23 16:5410.0 2.7 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 04/29/23 19:13 7439-97-604/27/23 18:120.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 04/23/23 16:58 83-32-904/22/23 11:548.3 1.7 1
Acenaphthylene ND ug/L 04/23/23 16:58 208-96-804/22/23 11:548.3 1.6 1
Aniline ND ug/L 04/23/23 16:58 62-53-304/22/23 11:548.3 1.4 1
Anthracene ND ug/L 04/23/23 16:58 120-12-704/22/23 11:548.3 1.9 1
Benzo(a)anthracene ND ug/L 04/23/23 16:58 56-55-304/22/23 11:548.3 2.2 1
Benzo(a)pyrene ND ug/L 04/23/23 16:58 50-32-804/22/23 11:548.3 2.3 1
Benzo(b)fluoranthene ND ug/L 04/23/23 16:58 205-99-204/22/23 11:548.3 2.2 1
Benzo(g,h,i)perylene ND ug/L 04/23/23 16:58 191-24-204/22/23 11:548.3 2.4 1
Benzo(k)fluoranthene ND ug/L 04/23/23 16:58 207-08-904/22/23 11:548.3 2.3 1
Benzoic Acid ND ug/L 04/23/23 16:58 65-85-004/22/23 11:5441.7 18.3 1
Benzyl alcohol ND ug/L 04/23/23 16:58 100-51-604/22/23 11:5416.7 2.4 1
4-Bromophenylphenyl ether ND ug/L 04/23/23 16:58 101-55-304/22/23 11:548.3 1.5 1
Butylbenzylphthalate ND ug/L 04/23/23 16:58 85-68-704/22/23 11:548.3 2.6 1
4-Chloro-3-methylphenol ND ug/L 04/23/23 16:58 59-50-704/22/23 11:548.3 2.8 1
4-Chloroaniline ND ug/L 04/23/23 16:58 106-47-804/22/23 11:5416.7 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 04/23/23 16:58 111-91-104/22/23 11:548.3 1.5 1
bis(2-Chloroethyl) ether ND ug/L 04/23/23 16:58 111-44-404/22/23 11:548.3 1.6 1
2-Chloronaphthalene ND ug/L 04/23/23 16:58 91-58-704/22/23 11:548.3 1.4 1
2-Chlorophenol ND ug/L 04/23/23 16:58 95-57-804/22/23 11:548.3 1.0 1
4-Chlorophenylphenyl ether ND ug/L 04/23/23 16:58 7005-72-304/22/23 11:548.3 1.7 1
Chrysene ND ug/L 04/23/23 16:58 218-01-904/22/23 11:548.3 2.3 1
Dibenz(a,h)anthracene ND ug/L 04/23/23 16:58 53-70-304/22/23 11:548.3 2.5 1
Dibenzofuran ND ug/L 04/23/23 16:58 132-64-904/22/23 11:548.3 1.8 1
1,2-Dichlorobenzene ND ug/L 04/23/23 16:58 95-50-104/22/23 11:548.3 1.5 1
1,3-Dichlorobenzene ND ug/L 04/23/23 16:58 541-73-104/22/23 11:548.3 1.3 1
1,4-Dichlorobenzene ND ug/L 04/23/23 16:58 106-46-704/22/23 11:548.3 1.4 1
3,3'-Dichlorobenzidine ND ug/L 04/23/23 16:58 91-94-104/22/23 11:5416.7 6.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-GW-DUP Lab ID: 92663594020 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dichlorophenol ND ug/L 04/23/23 16:58 120-83-204/22/23 11:548.3 1.2 1
Diethylphthalate ND ug/L 04/23/23 16:58 84-66-204/22/23 11:548.3 1.7 1
2,4-Dimethylphenol ND ug/L 04/23/23 16:58 105-67-9 v204/22/23 11:548.3 1.4 1
Dimethylphthalate ND ug/L 04/23/23 16:58 131-11-304/22/23 11:548.3 1.8 1
Di-n-butylphthalate ND ug/L 04/23/23 16:58 84-74-204/22/23 11:548.3 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 04/23/23 16:58 534-52-104/22/23 11:5416.7 6.5 1
2,4-Dinitrophenol ND ug/L 04/23/23 16:58 51-28-504/22/23 11:5441.7 21.7 1
2,4-Dinitrotoluene ND ug/L 04/23/23 16:58 121-14-204/22/23 11:548.3 1.4 1
2,6-Dinitrotoluene ND ug/L 04/23/23 16:58 606-20-204/22/23 11:548.3 1.4 1
Di-n-octylphthalate ND ug/L 04/23/23 16:58 117-84-004/22/23 11:548.3 3.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 04/23/23 16:58 117-81-704/22/23 11:545.0 3.1 1
Fluoranthene ND ug/L 04/23/23 16:58 206-44-004/22/23 11:548.3 1.8 1
Fluorene ND ug/L 04/23/23 16:58 86-73-704/22/23 11:548.3 1.7 1
Hexachloro-1,3-butadiene ND ug/L 04/23/23 16:58 87-68-304/22/23 11:548.3 1.5 1
Hexachlorobenzene ND ug/L 04/23/23 16:58 118-74-104/22/23 11:548.3 1.8 1
Hexachlorocyclopentadiene ND ug/L 04/23/23 16:58 77-47-404/22/23 11:548.3 1.3 1
Hexachloroethane ND ug/L 04/23/23 16:58 67-72-104/22/23 11:548.3 1.2 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/23/23 16:58 193-39-504/22/23 11:548.3 2.4 1
Isophorone ND ug/L 04/23/23 16:58 78-59-104/22/23 11:548.3 1.4 1
1-Methylnaphthalene ND ug/L 04/23/23 16:58 90-12-004/22/23 11:548.3 1.7 1
2-Methylnaphthalene ND ug/L 04/23/23 16:58 91-57-604/22/23 11:548.3 1.6 1
2-Methylphenol(o-Cresol)ND ug/L 04/23/23 16:58 95-48-704/22/23 11:548.3 1.6 1
3&4-Methylphenol(m&p Cresol)ND ug/L 04/23/23 16:58 15831-10-404/22/23 11:548.3 1.0 1
Naphthalene ND ug/L 04/23/23 16:58 91-20-304/22/23 11:548.3 1.7 1
2-Nitroaniline ND ug/L 04/23/23 16:58 88-74-404/22/23 11:5416.7 2.5 1
3-Nitroaniline ND ug/L 04/23/23 16:58 99-09-204/22/23 11:5416.7 3.1 1
4-Nitroaniline ND ug/L 04/23/23 16:58 100-01-604/22/23 11:5416.7 4.2 1
Nitrobenzene ND ug/L 04/23/23 16:58 98-95-304/22/23 11:548.3 1.6 1
2-Nitrophenol ND ug/L 04/23/23 16:58 88-75-504/22/23 11:548.3 1.2 1
4-Nitrophenol ND ug/L 04/23/23 16:58 100-02-704/22/23 11:5441.7 5.5 1
N-Nitrosodimethylamine ND ug/L 04/23/23 16:58 62-75-904/22/23 11:548.3 1.6 1
N-Nitroso-di-n-propylamine ND ug/L 04/23/23 16:58 621-64-704/22/23 11:548.3 1.1 1
N-Nitrosodiphenylamine ND ug/L 04/23/23 16:58 86-30-604/22/23 11:548.3 2.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/23/23 16:58 108-60-104/22/23 11:548.3 0.96 1
Pentachlorophenol ND ug/L 04/23/23 16:58 87-86-504/22/23 11:5416.7 3.1 1
Phenanthrene ND ug/L 04/23/23 16:58 85-01-804/22/23 11:548.3 1.7 1
Phenol ND ug/L 04/23/23 16:58 108-95-204/22/23 11:548.3 1.1 1
Pyrene ND ug/L 04/23/23 16:58 129-00-004/22/23 11:548.3 1.8 1
1,2,4-Trichlorobenzene ND ug/L 04/23/23 16:58 120-82-104/22/23 11:548.3 1.4 1
2,4,5-Trichlorophenol ND ug/L 04/23/23 16:58 95-95-404/22/23 11:548.3 1.2 1
2,4,6-Trichlorophenol ND ug/L 04/23/23 16:58 88-06-204/22/23 11:548.3 1.3 1
Surrogates
Nitrobenzene-d5 (S)38 %04/23/23 16:58 4165-60-004/22/23 11:5410-138 1
2-Fluorobiphenyl (S)34 %04/23/23 16:58 321-60-804/22/23 11:5410-130 1
Terphenyl-d14 (S)54 %04/23/23 16:58 1718-51-004/22/23 11:5419-191 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-GW-DUP Lab ID: 92663594020 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Phenol-d6 (S)16 %04/23/23 16:58 13127-88-304/22/23 11:5410-130 1
2-Fluorophenol (S)22 %04/23/23 16:58 367-12-404/22/23 11:5410-130 1
2,4,6-Tribromophenol (S)46 %04/23/23 16:58 118-79-604/22/23 11:5410-164 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 09:32 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 09:32 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 09:32 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 09:32 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 09:32 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 09:32 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 09:32 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 09:32 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 09:32 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 09:32 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 09:32 75-00-31.0 0.65 1
Chloroform 0.57J ug/L 04/28/23 09:32 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 09:32 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 09:32 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 09:32 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 09:32 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 09:32 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 09:32 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 09:32 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 09:32 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 09:32 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 09:32 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 09:32 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 09:32 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 09:32 107-06-21.0 0.32 1
1,1-Dichloroethene 0.86J ug/L 04/28/23 09:32 75-35-41.0 0.35 1
cis-1,2-Dichloroethene 0.51J ug/L 04/28/23 09:32 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 09:32 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 09:32 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 09:32 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 09:32 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 09:32 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 09:32 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 09:32 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 09:32 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 09:32 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 09:32 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 09:32 591-78-65.0 0.48 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: BF-GW-DUP Lab ID: 92663594020 Collected: 04/18/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
p-Isopropyltoluene ND ug/L 04/28/23 09:32 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 09:32 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 09:32 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 09:32 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 09:32 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 09:32 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 09:32 630-20-61.0 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 09:32 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/28/23 09:32 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 09:32 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 09:32 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 09:32 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 09:32 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 09:32 79-00-51.0 0.32 1
Trichloroethene 19.2 ug/L 04/28/23 09:32 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 09:32 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 09:32 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 09:32 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 09:32 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 09:32 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 09:32 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 09:32 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)97 %04/28/23 09:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %04/28/23 09:32 17060-07-070-130 1
Toluene-d8 (S)104 %04/28/23 09:32 2037-26-570-130 1
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
4500CNE Cyanide, Total
Cyanide ND mg/L 04/24/23 20:02 57-12-504/24/23 16:480.0080 0.0060 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: TRIP BLANK Lab ID: 92663594022 Collected: 04/20/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 04/28/23 01:36 67-64-125.0 5.1 1
Benzene ND ug/L 04/28/23 01:36 71-43-21.0 0.34 1
Bromobenzene ND ug/L 04/28/23 01:36 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 04/28/23 01:36 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 04/28/23 01:36 75-27-41.0 0.31 1
Bromoform ND ug/L 04/28/23 01:36 75-25-21.0 0.34 1
Bromomethane ND ug/L 04/28/23 01:36 74-83-92.0 1.7 1
2-Butanone (MEK)ND ug/L 04/28/23 01:36 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 04/28/23 01:36 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 04/28/23 01:36 108-90-71.0 0.28 1
Chloroethane ND ug/L 04/28/23 01:36 75-00-31.0 0.65 1
Chloroform ND ug/L 04/28/23 01:36 67-66-31.0 0.43 1
Chloromethane ND ug/L 04/28/23 01:36 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/28/23 01:36 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 04/28/23 01:36 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/28/23 01:36 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 04/28/23 01:36 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/28/23 01:36 106-93-41.0 0.27 1
Dibromomethane ND ug/L 04/28/23 01:36 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 04/28/23 01:36 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 04/28/23 01:36 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 04/28/23 01:36 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 04/28/23 01:36 75-71-8 IH,v11.0 0.35 1
1,1-Dichloroethane ND ug/L 04/28/23 01:36 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 04/28/23 01:36 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 04/28/23 01:36 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/28/23 01:36 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/28/23 01:36 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 04/28/23 01:36 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 04/28/23 01:36 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 04/28/23 01:36 594-20-71.0 0.39 1
1,1-Dichloropropene ND ug/L 04/28/23 01:36 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/28/23 01:36 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/28/23 01:36 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 04/28/23 01:36 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 04/28/23 01:36 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/28/23 01:36 87-68-32.0 1.5 1
2-Hexanone ND ug/L 04/28/23 01:36 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 04/28/23 01:36 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 04/28/23 01:36 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 04/28/23 01:36 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 04/28/23 01:36 1634-04-41.0 0.42 1
Naphthalene ND ug/L 04/28/23 01:36 91-20-31.0 0.64 1
Styrene ND ug/L 04/28/23 01:36 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/28/23 01:36 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 169
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663594
H&A-002
Sample: TRIP BLANK Lab ID: 92663594022 Collected: 04/20/23 00:00 Received: 04/21/23 12:15 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 04/28/23 01:36 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 04/28/23 01:36 127-18-41.0 0.29 1
Toluene ND ug/L 04/28/23 01:36 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/28/23 01:36 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/28/23 01:36 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/28/23 01:36 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 04/28/23 01:36 79-00-51.0 0.32 1
Trichloroethene ND ug/L 04/28/23 01:36 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 04/28/23 01:36 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/28/23 01:36 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 04/28/23 01:36 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 04/28/23 01:36 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 04/28/23 01:36 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 04/28/23 01:36 179601-23-12.0 0.71 1
o-Xylene ND ug/L 04/28/23 01:36 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)94 %04/28/23 01:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %04/28/23 01:36 17060-07-070-130 1
Toluene-d8 (S)104 %04/28/23 01:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 101 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770880
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4001963
Associated Lab Samples:92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 04/29/23 14:300.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4001964LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 97 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4001965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662338001
4001966
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 96 75-12597 1 252.5ND 2.4 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770883
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92663594017, 92663594018, 92663594020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4001980
Associated Lab Samples:92663594017, 92663594018, 92663594020
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 04/29/23 18:120.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4001981LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4001982MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662485001
4001983
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 82 75-12583 2 252.5ND 2.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
877601
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4627360
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.019 04/28/23 08:540.0082
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4627361LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.470.44 109 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4627362MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594001
4627363
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.487 105 80-120108 12 200.531ND 0.51 0.58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
879481
EPA 3015A
EPA 6010D
6010D MET ICP, TCLP MICRO
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples: 92663594001, 92663594005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4635722
Associated Lab Samples:92663594001, 92663594005
Matrix: Water
AnalyzedMDL
Chromium mg/L ND 0.10 05/05/23 15:340.0043
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4635362
Associated Lab Samples:92663594001, 92663594005
Matrix: Water
AnalyzedMDL
Chromium mg/L ND 0.10 05/05/23 15:360.0043
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4635723LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium mg/L 5.15 103 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4635724MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10649808001
4635725
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium mg/L 5 101 75-12599 2 205ND5.1 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769799
EPA 3010A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016, 92663594017,
92663594018, 92663594020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3996539
Associated Lab Samples: 92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016, 92663594017,
92663594018, 92663594020
Matrix: Water
AnalyzedMDL
Aluminum ug/L 8.0J 20.0 04/24/23 20:507.4
Arsenic ug/L ND 1.0 04/24/23 20:500.087
Barium ug/L ND 1.0 04/24/23 20:500.21
Cadmium ug/L ND 0.20 04/24/23 20:500.060
Chromium ug/L ND 1.0 04/24/23 20:500.50
Copper ug/L ND 2.0 04/24/23 20:501.1
Lead ug/L ND 1.0 04/24/23 20:500.077
Nickel ug/L ND 1.0 04/24/23 20:500.42
Selenium ug/L ND 2.0 04/24/23 20:500.072
Silver ug/L ND 0.40 04/24/23 20:500.070
Zinc ug/L ND 10.0 04/24/23 20:502.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3996540LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum ug/L 25502500 102 80-120
Arsenic ug/L 49.650 99 80-120
Barium ug/L 49.850 100 80-120
Cadmium ug/L 51.650 103 80-120
Chromium ug/L 52.050 104 80-120
Copper ug/L 52.450 105 80-120
Lead ug/L 50.550 101 80-120
Nickel ug/L 51.950 104 80-120
Selenium ug/L 50.350 101 80-120
Silver ug/L 25.725 103 80-120
Zinc ug/L 53.250 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3996541MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92661765001
3996542
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum ug/L 2500 100 75-125101 1 20250035.5 2550 2560
Arsenic ug/L 50 98 75-12597 1 2050ND49.1 48.8
Barium ug/L 50 98 75-12599 0 205013.0 62.0 62.3
Cadmium ug/L 50 102 75-125102 0 2050ND51.0 51.2
Chromium ug/L 50 103 75-125103 0 20501.2 52.8 52.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3996541MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92661765001
3996542
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper ug/L 50 105 75-125106 1 2050ND52.7 53.4
Lead ug/L 50 100 75-125100 0 2050ND50.2 50.3
Nickel ug/L 50 103 75-125105 1 20501.9 53.4 54.2
Selenium ug/L 50 99 75-125100 1 20500.089J 49.5 50.2
Silver ug/L 25 102 75-125101 0 2025ND25.4 25.4
Zinc ug/L 50 101 75-125104 2 2050ND52.2 53.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
877600
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4627356
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
Aluminum mg/kg ND 28.1 04/28/23 09:255.7
Arsenic mg/kg ND 0.47 04/27/23 15:260.13
Barium mg/kg ND 0.28 04/27/23 15:260.070
Cadmium mg/kg ND 0.075 04/27/23 15:260.028
Chromium mg/kg ND 1.9 04/27/23 15:260.36
Copper mg/kg ND 0.94 04/27/23 15:260.29
Lead mg/kg ND 0.47 04/27/23 15:260.087
Nickel mg/kg ND 0.47 04/27/23 15:260.22
Selenium mg/kg ND 0.47 04/27/23 15:260.098
Silver mg/kg ND 0.47 04/27/23 15:260.19
Zinc mg/kg ND 4.7 04/27/23 15:261.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4627357LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum mg/kg 918917 100 80-120
Arsenic mg/kg 41.945.9 91 80-120
Barium mg/kg 44.645.9 97 80-120
Cadmium mg/kg 42.945.9 94 80-120
Chromium mg/kg 44.145.9 96 80-120
Copper mg/kg 45.845.9 100 80-120
Lead mg/kg 44.545.9 97 80-120
Nickel mg/kg 44.745.9 97 80-120
Selenium mg/kg 42.245.9 92 80-120
Silver mg/kg 22.322.9 97 80-120
Zinc mg/kg 44.045.9 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4627358MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594001
4627359
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Aluminum mg/kg P6,R1102058775-125-78 23 2010702680032700 25900
Arsenic mg/kg 50.9 89 75-12591 7 2053.30.51J 45.7 48.9
Barium mg/kg 50.9 108 75-125118 4 2053.3158 213 221
Cadmium mg/kg 50.9 91 75-12594 7 2053.30.067J 46.5 50.0
Chromium mg/kg M150.9 115 75-12551 16 2053.3154 213 182
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4627358MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594001
4627359
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper mg/kg M150.9 107 75-125142 16 2053.369.6 124 145
Lead mg/kg 50.9 90 75-12595 10 2053.30.74 46.8 51.5
Nickel mg/kg 50.9 98 75-12586 3 2053.390.7 141 136
Selenium mg/kg 50.9 90 75-12592 7 2053.3ND 45.8 49.3
Silver mg/kg 25.5 92 75-12595 8 2026.7ND 23.5 25.5
Zinc mg/kg M150.9 101 75-12567 11 2053.399.2 150 135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770278
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3998742
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/25/23 16:441.9
1,1,1-Trichloroethane ug/kg ND 5.0 04/25/23 16:442.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/25/23 16:441.3
1,1,2-Trichloroethane ug/kg ND 5.0 04/25/23 16:441.7
1,1-Dichloroethane ug/kg ND 5.0 04/25/23 16:442.1
1,1-Dichloroethene ug/kg ND 5.0 04/25/23 16:442.1
1,1-Dichloropropene ug/kg ND 5.0 04/25/23 16:442.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/25/23 16:444.0
1,2,3-Trichloropropane ug/kg ND 5.0 04/25/23 16:442.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/25/23 16:444.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/25/23 16:443.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/25/23 16:441.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/25/23 16:442.2
1,2-Dichlorobenzene ug/kg ND 5.0 04/25/23 16:441.8
1,2-Dichloroethane ug/kg ND 5.0 04/25/23 16:443.3
1,2-Dichloropropane ug/kg ND 5.0 04/25/23 16:441.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/25/23 16:441.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/25/23 16:441.6
1,3-Dichloropropane ug/kg ND 5.0 04/25/23 16:441.6
1,4-Dichlorobenzene ug/kg ND 5.0 04/25/23 16:441.3
2,2-Dichloropropane ug/kg ND 5.0 v204/25/23 16:443.8
2-Butanone (MEK)ug/kg ND 100 04/25/23 16:4424.0
2-Chlorotoluene ug/kg ND 5.0 04/25/23 16:441.8
2-Hexanone ug/kg ND 50.0 04/25/23 16:444.8
4-Chlorotoluene ug/kg ND 5.0 04/25/23 16:442.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/25/23 16:444.8
Acetone ug/kg ND 100 04/25/23 16:4432.1
Benzene ug/kg ND 5.0 04/25/23 16:442.0
Bromobenzene ug/kg ND 5.0 04/25/23 16:441.6
Bromochloromethane ug/kg ND 5.0 04/25/23 16:441.5
Bromodichloromethane ug/kg ND 5.0 04/25/23 16:441.9
Bromoform ug/kg ND 5.0 04/25/23 16:441.8
Bromomethane ug/kg ND 20.0 IK04/25/23 16:4415.5
Carbon tetrachloride ug/kg ND 5.0 04/25/23 16:441.9
Chlorobenzene ug/kg ND 5.0 04/25/23 16:442.9
Chloroethane ug/kg ND 10.0 04/25/23 16:443.9
Chloroform ug/kg ND 5.0 04/25/23 16:444.2
Chloromethane ug/kg ND 10.0 04/25/23 16:444.2
cis-1,2-Dichloroethene ug/kg ND 5.0 04/25/23 16:441.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 110 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3998742
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
cis-1,3-Dichloropropene ug/kg ND 5.0 04/25/23 16:441.4
Dibromochloromethane ug/kg ND 5.0 04/25/23 16:442.8
Dibromomethane ug/kg ND 5.0 04/25/23 16:441.1
Dichlorodifluoromethane ug/kg ND 10.0 04/25/23 16:445.1
Diisopropyl ether ug/kg ND 5.0 04/25/23 16:441.4
Ethylbenzene ug/kg ND 5.0 04/25/23 16:442.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 04/25/23 16:448.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/25/23 16:441.7
m&p-Xylene ug/kg ND 10.0 04/25/23 16:443.4
Methyl-tert-butyl ether ug/kg ND 5.0 v204/25/23 16:441.9
Methylene Chloride ug/kg ND 20.0 04/25/23 16:4413.7
n-Butylbenzene ug/kg ND 5.0 04/25/23 16:443.2
n-Propylbenzene ug/kg ND 5.0 04/25/23 16:441.8
Naphthalene ug/kg ND 5.0 04/25/23 16:442.6
o-Xylene ug/kg ND 5.0 04/25/23 16:442.2
p-Isopropyltoluene ug/kg ND 5.0 04/25/23 16:442.5
sec-Butylbenzene ug/kg ND 5.0 04/25/23 16:442.2
Styrene ug/kg ND 5.0 04/25/23 16:441.3
tert-Butylbenzene ug/kg ND 5.0 04/25/23 16:441.8
Tetrachloroethene ug/kg ND 5.0 04/25/23 16:441.6
Toluene ug/kg ND 5.0 04/25/23 16:443.4
trans-1,2-Dichloroethene ug/kg ND 5.0 04/25/23 16:444.2
trans-1,3-Dichloropropene ug/kg ND 5.0 04/25/23 16:441.7
Trichloroethene ug/kg ND 5.0 04/25/23 16:444.0
Trichlorofluoromethane ug/kg ND 5.0 04/25/23 16:442.8
Vinyl acetate ug/kg ND 50.0 04/25/23 16:4410.3
Vinyl chloride ug/kg ND 10.0 v204/25/23 16:442.5
Xylene (Total)ug/kg ND 10.0 04/25/23 16:442.8
1,2-Dichloroethane-d4 (S)%97 70-130 04/25/23 16:44
4-Bromofluorobenzene (S)%100 70-130 04/25/23 16:44
Toluene-d8 (S)%101 70-130 04/25/23 16:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3998743LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 412500 82 70-130
1,1,1-Trichloroethane ug/kg 393500 79 70-130
1,1,2,2-Tetrachloroethane ug/kg 431500 86 70-130
1,1,2-Trichloroethane ug/kg 399500 80 70-130
1,1-Dichloroethane ug/kg 405500 81 70-130
1,1-Dichloroethene ug/kg 406500 81 70-130
1,1-Dichloropropene ug/kg 409500 82 70-130
1,2,3-Trichlorobenzene ug/kg 413500 83 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3998743LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,3-Trichloropropane ug/kg 400500 80 70-130
1,2,4-Trichlorobenzene ug/kg 425500 85 70-130
1,2,4-Trimethylbenzene ug/kg 424500 85 70-130
1,2-Dibromo-3-chloropropane ug/kg 408500 82 67-130
1,2-Dibromoethane (EDB)ug/kg 416500 83 70-130
1,2-Dichlorobenzene ug/kg 402500 80 70-130
1,2-Dichloroethane ug/kg 421500 84 70-130
1,2-Dichloropropane ug/kg 409500 82 70-130
1,3,5-Trimethylbenzene ug/kg 418500 84 70-130
1,3-Dichlorobenzene ug/kg 430500 86 70-130
1,3-Dichloropropane ug/kg 401500 80 70-130
1,4-Dichlorobenzene ug/kg 412500 82 70-130
2,2-Dichloropropane ug/kg 358 v250072 67-130
2-Butanone (MEK)ug/kg 8221000 82 66-130
2-Chlorotoluene ug/kg 425500 85 70-130
2-Hexanone ug/kg 8951000 89 70-130
4-Chlorotoluene ug/kg 418500 84 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 8411000 84 70-130
Acetone ug/kg 8781000 88 67-130
Benzene ug/kg 398500 80 70-130
Bromobenzene ug/kg 414500 83 70-130
Bromochloromethane ug/kg 454500 91 70-130
Bromodichloromethane ug/kg 400500 80 70-130
Bromoform ug/kg 415500 83 70-130
Bromomethane ug/kg 512 IK500102 53-175
Carbon tetrachloride ug/kg 415500 83 70-130
Chlorobenzene ug/kg 426500 85 70-130
Chloroethane ug/kg 394500 79 70-135
Chloroform ug/kg 392500 78 70-130
Chloromethane ug/kg 421500 84 64-130
cis-1,2-Dichloroethene ug/kg 427500 85 70-130
cis-1,3-Dichloropropene ug/kg 405500 81 70-130
Dibromochloromethane ug/kg 410500 82 70-130
Dibromomethane ug/kg 443500 89 70-130
Dichlorodifluoromethane ug/kg 417500 83 63-145
Diisopropyl ether ug/kg 390500 78 68-130
Ethylbenzene ug/kg 382500 76 70-130
Hexachloro-1,3-butadiene ug/kg 400500 80 70-130
Isopropylbenzene (Cumene)ug/kg 411500 82 70-130
m&p-Xylene ug/kg 7901000 79 70-130
Methyl-tert-butyl ether ug/kg 379 v250076 70-130
Methylene Chloride ug/kg 392500 78 67-130
n-Butylbenzene ug/kg 403500 81 70-130
n-Propylbenzene ug/kg 407500 81 70-130
Naphthalene ug/kg 431500 86 70-130
o-Xylene ug/kg 404500 81 70-130
p-Isopropyltoluene ug/kg 427500 85 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 112 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3998743LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/kg 409500 82 70-130
Styrene ug/kg 405500 81 70-130
tert-Butylbenzene ug/kg 460500 92 64-130
Tetrachloroethene ug/kg 434500 87 70-130
Toluene ug/kg 408500 82 70-130
trans-1,2-Dichloroethene ug/kg 406500 81 70-130
trans-1,3-Dichloropropene ug/kg 393500 79 70-130
Trichloroethene ug/kg 416500 83 70-130
Trichlorofluoromethane ug/kg 403500 81 70-130
Vinyl acetate ug/kg 8401000 84 70-134
Vinyl chloride ug/kg 348 v250070 68-130
Xylene (Total)ug/kg 11901500 80 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3998744MATRIX SPIKE SAMPLE:
MSSpike
Result
92663455001
1,1,1,2-Tetrachloroethane ug/kg 66606030 110 58-140ND
1,1,1-Trichloroethane ug/kg 70506030 117 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 69306030 115 52-139ND
1,1,2-Trichloroethane ug/kg 69306030 115 56-140ND
1,1-Dichloroethane ug/kg 67806030 112 58-145ND
1,1-Dichloroethene ug/kg 71406030 118 57-158ND
1,1-Dichloropropene ug/kg 70006030 116 58-151ND
1,2,3-Trichlorobenzene ug/kg 63806030 106 48-149ND
1,2,3-Trichloropropane ug/kg 62306030 103 54-132ND
1,2,4-Trichlorobenzene ug/kg 64906030 108 51-151ND
1,2,4-Trimethylbenzene ug/kg 295006030 101 38-17023300
1,2-Dibromo-3-chloropropane ug/kg 60006030 100 44-134ND
1,2-Dibromoethane (EDB)ug/kg 65506030 109 60-138ND
1,2-Dichlorobenzene ug/kg 63106030 105 59-147ND
1,2-Dichloroethane ug/kg 67206030 111 57-139ND
1,2-Dichloropropane ug/kg 69306030 115 62-145ND
1,3,5-Trimethylbenzene ug/kg 126006030 106 47-1596210
1,3-Dichlorobenzene ug/kg 66106030 110 58-144ND
1,3-Dichloropropane ug/kg 64406030 107 60-142ND
1,4-Dichlorobenzene ug/kg 63206030 105 57-143ND
2,2-Dichloropropane ug/kg 6910 v36030115 37-144ND
2-Butanone (MEK)ug/kg 1590012100 132 28-146ND
2-Chlorotoluene ug/kg 71106030 118 55-158ND
2-Hexanone ug/kg 1320012100 109 44-141ND
4-Chlorotoluene ug/kg 65106030 108 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 2040012100 102 50-1388090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 113 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3998744MATRIX SPIKE SAMPLE:
MSSpike
Result
92663455001
Acetone ug/kg 16500 M112100137 20-136ND
Benzene ug/kg 143006030 109 60-1457690
Bromobenzene ug/kg 64906030 107 59-145ND
Bromochloromethane ug/kg 71306030 118 57-143ND
Bromodichloromethane ug/kg 64806030 107 53-133ND
Bromoform ug/kg 62706030 104 48-133ND
Bromomethane ug/kg 1620 IK603027 10-167ND
Carbon tetrachloride ug/kg 63106030 105 57-147ND
Chlorobenzene ug/kg 67906030 113 61-144ND
Chloroethane ug/kg 10806030 18 10-153ND
Chloroform ug/kg 74706030 124 58-141ND
Chloromethane ug/kg 88006030 146 54-165ND
cis-1,2-Dichloroethene ug/kg 71406030 118 59-144ND
cis-1,3-Dichloropropene ug/kg 67906030 112 56-137ND
Dibromochloromethane ug/kg 64006030 106 53-139ND
Dibromomethane ug/kg 70706030 117 60-136ND
Dichlorodifluoromethane ug/kg 89206030 148 49-177ND
Diisopropyl ether ug/kg 65806030 109 53-136ND
Ethylbenzene ug/kg 165006030 88 53-15011200
Hexachloro-1,3-butadiene ug/kg 95706030 159 42-186ND
Isopropylbenzene (Cumene)ug/kg 88406030 109 62-1542280
m&p-Xylene ug/kg 7520012100 64 49-15667400
Methyl-tert-butyl ether ug/kg 6130 v36030102 54-133ND
Methylene Chloride ug/kg 78906030 131 50-153ND
n-Butylbenzene ug/kg 93306030 114 44-1742440
n-Propylbenzene ug/kg 99506030 101 52-1573860
Naphthalene ug/kg 504006030 100 37-15044400
o-Xylene ug/kg 409006030 74 54-15036400
p-Isopropyltoluene ug/kg 105006030 141 50-1641980
sec-Butylbenzene ug/kg 74706030 124 58-161ND
Styrene ug/kg 73706030 122 60-148ND
tert-Butylbenzene ug/kg 67306030 111 44-151ND
Tetrachloroethene ug/kg 62906030 104 53-151ND
Toluene ug/kg 71300 E,M16030453 52-14844000
trans-1,2-Dichloroethene ug/kg 66606030 110 60-148ND
trans-1,3-Dichloropropene ug/kg 64506030 107 55-133ND
Trichloroethene ug/kg 68806030 114 60-148ND
Trichlorofluoromethane ug/kg 13106030 22 10-154ND
Vinyl acetate ug/kg 1330012100 110 50-149ND
Vinyl chloride ug/kg 6120 v36030101 57-157ND
Xylene (Total)ug/kg 11600018100 68 52-153104000
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663465001
3998745SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 157 1 300.16 mg/kg
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg 114 2 300.12 mg/kg
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg 51.0J 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg 11.3 30 300.0084 mg/kg
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 11.3 3 300.011 mg/kg
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg 7.0 5 300.0066 mg/kg
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663465001
3998745SAMPLE DUPLICATE:
m&p-Xylene ug/kg 48.1 5 300.046 mg/kg
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 34.6 C930ND
n-Butylbenzene ug/kg 25.8 3 300.027 mg/kg
n-Propylbenzene ug/kg 18.1 1 300.018 mg/kg
Naphthalene ug/kg 87.2 2 300.086 mg/kg
o-Xylene ug/kg 43.8 7 300.041 mg/kg
p-Isopropyltoluene ug/kg 99.5 5 300.11 mg/kg
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg 3.8J 30ND
Toluene ug/kg 39.8 18 300.033 mg/kg
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 91.9 6 300.087 mg/kg
1,2-Dichloroethane-d4 (S)%9494
4-Bromofluorobenzene (S)%98100
Toluene-d8 (S)%101101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770365
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663594011, 92663594012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3999229
Associated Lab Samples:92663594011, 92663594012
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/26/23 07:220.31
1,1,1-Trichloroethane ug/L ND 1.0 04/26/23 07:220.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/26/23 07:220.22
1,1,2-Trichloroethane ug/L ND 1.0 04/26/23 07:220.32
1,1-Dichloroethane ug/L ND 1.0 04/26/23 07:220.37
1,1-Dichloroethene ug/L ND 1.0 04/26/23 07:220.35
1,1-Dichloropropene ug/L ND 1.0 04/26/23 07:220.43
1,2,3-Trichlorobenzene ug/L ND 1.0 04/26/23 07:220.81
1,2,3-Trichloropropane ug/L ND 1.0 04/26/23 07:220.26
1,2,4-Trichlorobenzene ug/L ND 1.0 04/26/23 07:220.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/26/23 07:220.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/26/23 07:220.27
1,2-Dichlorobenzene ug/L ND 1.0 04/26/23 07:220.34
1,2-Dichloroethane ug/L ND 1.0 04/26/23 07:220.32
1,2-Dichloropropane ug/L ND 1.0 04/26/23 07:220.36
1,3-Dichlorobenzene ug/L ND 1.0 04/26/23 07:220.34
1,3-Dichloropropane ug/L ND 1.0 04/26/23 07:220.28
1,4-Dichlorobenzene ug/L ND 1.0 04/26/23 07:220.33
2,2-Dichloropropane ug/L ND 1.0 04/26/23 07:220.39
2-Butanone (MEK)ug/L ND 5.0 04/26/23 07:224.0
2-Chlorotoluene ug/L ND 1.0 04/26/23 07:220.32
2-Hexanone ug/L ND 5.0 04/26/23 07:220.48
4-Chlorotoluene ug/L ND 1.0 04/26/23 07:220.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/26/23 07:222.7
Acetone ug/L ND 25.0 04/26/23 07:225.1
Benzene ug/L ND 1.0 04/26/23 07:220.34
Bromobenzene ug/L ND 1.0 04/26/23 07:220.29
Bromochloromethane ug/L ND 1.0 04/26/23 07:220.47
Bromodichloromethane ug/L ND 1.0 04/26/23 07:220.31
Bromoform ug/L ND 1.0 04/26/23 07:220.34
Bromomethane ug/L ND 2.0 04/26/23 07:221.7
Carbon tetrachloride ug/L ND 1.0 04/26/23 07:220.33
Chlorobenzene ug/L ND 1.0 04/26/23 07:220.28
Chloroethane ug/L ND 1.0 04/26/23 07:220.65
Chloroform ug/L ND 1.0 04/26/23 07:220.43
Chloromethane ug/L ND 1.0 04/26/23 07:220.54
cis-1,2-Dichloroethene ug/L ND 1.0 04/26/23 07:220.38
cis-1,3-Dichloropropene ug/L ND 1.0 04/26/23 07:220.36
Dibromochloromethane ug/L ND 1.0 04/26/23 07:220.36
Dibromomethane ug/L ND 1.0 04/26/23 07:220.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3999229
Associated Lab Samples:92663594011, 92663594012
Matrix: Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 IK,v104/26/23 07:220.35
Diisopropyl ether ug/L ND 1.0 04/26/23 07:220.31
Ethylbenzene ug/L ND 1.0 04/26/23 07:220.30
Hexachloro-1,3-butadiene ug/L ND 2.0 04/26/23 07:221.5
m&p-Xylene ug/L ND 2.0 04/26/23 07:220.71
Methyl-tert-butyl ether ug/L ND 1.0 04/26/23 07:220.42
Methylene Chloride ug/L ND 5.0 04/26/23 07:222.0
Naphthalene ug/L ND 1.0 04/26/23 07:220.64
o-Xylene ug/L ND 1.0 04/26/23 07:220.34
p-Isopropyltoluene ug/L ND 1.0 04/26/23 07:220.41
Styrene ug/L ND 1.0 04/26/23 07:220.29
Tetrachloroethene ug/L ND 1.0 04/26/23 07:220.29
Toluene ug/L ND 1.0 04/26/23 07:220.24
trans-1,2-Dichloroethene ug/L ND 1.0 04/26/23 07:220.40
trans-1,3-Dichloropropene ug/L ND 1.0 04/26/23 07:220.36
Trichloroethene ug/L ND 1.0 04/26/23 07:220.38
Trichlorofluoromethane ug/L ND 1.0 04/26/23 07:220.30
Vinyl acetate ug/L ND 2.0 04/26/23 07:221.3
Vinyl chloride ug/L ND 1.0 04/26/23 07:220.39
Xylene (Total)ug/L ND 1.0 04/26/23 07:220.34
1,2-Dichloroethane-d4 (S)%102 70-130 04/26/23 07:22
4-Bromofluorobenzene (S)%102 70-130 04/26/23 07:22
Toluene-d8 (S)%101 70-130 04/26/23 07:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3999230LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.420 107 70-130
1,1,1-Trichloroethane ug/L 20.320 101 70-130
1,1,2,2-Tetrachloroethane ug/L 21.120 105 70-130
1,1,2-Trichloroethane ug/L 22.020 110 70-130
1,1-Dichloroethane ug/L 20.220 101 70-130
1,1-Dichloroethene ug/L 19.720 99 70-130
1,1-Dichloropropene ug/L 22.020 110 70-130
1,2,3-Trichlorobenzene ug/L 21.620 108 70-130
1,2,3-Trichloropropane ug/L 20.120 100 70-130
1,2,4-Trichlorobenzene ug/L 20.820 104 70-130
1,2-Dibromo-3-chloropropane ug/L 19.620 98 70-131
1,2-Dibromoethane (EDB)ug/L 22.120 110 70-130
1,2-Dichlorobenzene ug/L 21.520 107 70-130
1,2-Dichloroethane ug/L 20.820 104 70-130
1,2-Dichloropropane ug/L 22.220 111 70-130
1,3-Dichlorobenzene ug/L 21.420 107 70-130
1,3-Dichloropropane ug/L 20.620 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3999230LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 21.620 108 70-130
2,2-Dichloropropane ug/L 18.320 91 68-135
2-Butanone (MEK)ug/L 38.940 97 70-134
2-Chlorotoluene ug/L 21.120 106 70-130
2-Hexanone ug/L 41.740 104 70-131
4-Chlorotoluene ug/L 21.520 108 70-130
4-Methyl-2-pentanone (MIBK)ug/L 40.940 102 70-130
Acetone ug/L 41.440 103 70-133
Benzene ug/L 20.820 104 70-130
Bromobenzene ug/L 20.720 103 70-130
Bromochloromethane ug/L 21.920 110 70-130
Bromodichloromethane ug/L 21.320 107 70-130
Bromoform ug/L 19.420 97 70-130
Bromomethane ug/L 16.020 80 45-151
Carbon tetrachloride ug/L 20.820 104 70-130
Chlorobenzene ug/L 21.320 106 70-130
Chloroethane ug/L 21.420 107 39-152
Chloroform ug/L 20.420 102 70-130
Chloromethane ug/L 22.720 114 58-130
cis-1,2-Dichloroethene ug/L 20.520 103 70-130
cis-1,3-Dichloropropene ug/L 21.520 108 70-130
Dibromochloromethane ug/L 20.720 103 70-130
Dibromomethane ug/L 21.420 107 70-130
Dichlorodifluoromethane ug/L 25.6 IK,v120128 54-133
Diisopropyl ether ug/L 20.620 103 70-130
Ethylbenzene ug/L 21.320 107 70-130
Hexachloro-1,3-butadiene ug/L 22.720 114 70-135
m&p-Xylene ug/L 42.340 106 70-130
Methyl-tert-butyl ether ug/L 20.020 100 70-130
Methylene Chloride ug/L 22.020 110 66-130
Naphthalene ug/L 21.120 105 70-130
o-Xylene ug/L 20.620 103 70-130
p-Isopropyltoluene ug/L 21.820 109 70-130
Styrene ug/L 21.020 105 70-130
Tetrachloroethene ug/L 19.320 96 70-130
Toluene ug/L 20.320 101 70-130
trans-1,2-Dichloroethene ug/L 21.120 106 70-130
trans-1,3-Dichloropropene ug/L 21.220 106 70-130
Trichloroethene ug/L 20.920 104 70-130
Trichlorofluoromethane ug/L 20.220 101 62-130
Vinyl acetate ug/L 40.540 101 70-144
Vinyl chloride ug/L 18.120 90 62-130
Xylene (Total)ug/L 62.860 105 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3999232MATRIX SPIKE SAMPLE:
MSSpike
Result
92663594011
1,1,1,2-Tetrachloroethane ug/L 23.120 116 70-141ND
1,1,1-Trichloroethane ug/L 24.320 122 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.920 114 69-142ND
1,1,2-Trichloroethane ug/L 24.120 120 70-138ND
1,1-Dichloroethane ug/L 23.820 119 70-150ND
1,1-Dichloroethene ug/L 24.220 121 70-156ND
1,1-Dichloropropene ug/L 26.520 132 70-150ND
1,2,3-Trichlorobenzene ug/L 21.720 108 70-148ND
1,2,3-Trichloropropane ug/L 21.320 107 70-140ND
1,2,4-Trichlorobenzene ug/L 20.920 104 70-146ND
1,2-Dibromo-3-chloropropane ug/L 20.620 103 68-146ND
1,2-Dibromoethane (EDB)ug/L 23.420 117 70-138ND
1,2-Dichlorobenzene ug/L 22.420 112 70-141ND
1,2-Dichloroethane ug/L 23.020 115 69-143ND
1,2-Dichloropropane ug/L 23.720 119 68-156ND
1,3-Dichlorobenzene ug/L 22.720 114 70-143ND
1,3-Dichloropropane ug/L 22.620 113 70-138ND
1,4-Dichlorobenzene ug/L 22.120 110 70-142ND
2,2-Dichloropropane ug/L 24.320 122 52-170ND
2-Butanone (MEK)ug/L 46.140 115 60-157ND
2-Chlorotoluene ug/L 22.820 114 70-147ND
2-Hexanone ug/L 43.640 109 68-146ND
4-Chlorotoluene ug/L 22.820 114 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 44.040 110 70-141ND
Acetone ug/L 51.040 127 58-157ND
Benzene ug/L 23.620 118 70-142ND
Bromobenzene ug/L 21.720 108 70-143ND
Bromochloromethane ug/L 25.620 128 70-146ND
Bromodichloromethane ug/L 22.820 114 70-139ND
Bromoform ug/L 21.220 106 64-140ND
Bromomethane ug/L 9.820 49 28-192ND
Carbon tetrachloride ug/L 25.420 127 70-148ND
Chlorobenzene ug/L 23.120 115 70-141ND
Chloroethane ug/L 26.620 133 58-191ND
Chloroform ug/L 24.220 121 70-148ND
Chloromethane ug/L 24.120 120 43-162ND
cis-1,2-Dichloroethene ug/L 25.220 122 68-1510.77J
cis-1,3-Dichloropropene ug/L 23.620 118 70-139ND
Dibromochloromethane ug/L 22.820 114 70-144ND
Dibromomethane ug/L 23.720 119 70-139ND
Dichlorodifluoromethane ug/L 35.5 IK,M1,v120177 39-171ND
Diisopropyl ether ug/L 23.020 115 67-142ND
Ethylbenzene ug/L 23.820 119 70-143ND
Hexachloro-1,3-butadiene ug/L 23.220 116 64-163ND
m&p-Xylene ug/L 46.840 117 70-144ND
Methyl-tert-butyl ether ug/L 22.020 110 65-143ND
Methylene Chloride ug/L 22.520 112 62-149ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3999232MATRIX SPIKE SAMPLE:
MSSpike
Result
92663594011
Naphthalene ug/L 21.420 107 67-147ND
o-Xylene ug/L 22.720 113 70-145ND
p-Isopropyltoluene ug/L 23.620 118 70-147ND
Styrene ug/L 22.920 114 70-143ND
Tetrachloroethene ug/L 22.720 113 70-145ND
Toluene ug/L 22.920 115 70-142ND
trans-1,2-Dichloroethene ug/L 24.020 120 70-151ND
trans-1,3-Dichloropropene ug/L 22.720 113 70-139ND
Trichloroethene ug/L 23.920 119 62-146ND
Trichlorofluoromethane ug/L 26.120 130 63-153ND
Vinyl acetate ug/L 46.040 115 61-162ND
Vinyl chloride ug/L 22.120 110 61-163ND
Xylene (Total)ug/L 69.560 116 70-143ND
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594012
3999231SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594012
3999231SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L 0.61J 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND IK,v130ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L 1.3 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L 1.8 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.49J 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%107103
4-Bromofluorobenzene (S)%102100
Toluene-d8 (S)%103104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770981
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92663594013, 92663594014, 92663594015, 92663594016, 92663594017, 92663594018, 92663594020,
92663594022
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002511
Associated Lab Samples: 92663594013, 92663594014, 92663594015, 92663594016, 92663594017, 92663594018, 92663594020,
92663594022
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 04/28/23 00:230.31
1,1,1-Trichloroethane ug/L ND 1.0 04/28/23 00:230.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 04/28/23 00:230.22
1,1,2-Trichloroethane ug/L ND 1.0 04/28/23 00:230.32
1,1-Dichloroethane ug/L ND 1.0 04/28/23 00:230.37
1,1-Dichloroethene ug/L ND 1.0 04/28/23 00:230.35
1,1-Dichloropropene ug/L ND 1.0 04/28/23 00:230.43
1,2,3-Trichlorobenzene ug/L ND 1.0 04/28/23 00:230.81
1,2,3-Trichloropropane ug/L ND 1.0 04/28/23 00:230.26
1,2,4-Trichlorobenzene ug/L ND 1.0 04/28/23 00:230.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 04/28/23 00:230.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 04/28/23 00:230.27
1,2-Dichlorobenzene ug/L ND 1.0 04/28/23 00:230.34
1,2-Dichloroethane ug/L ND 1.0 04/28/23 00:230.32
1,2-Dichloropropane ug/L ND 1.0 04/28/23 00:230.36
1,3-Dichlorobenzene ug/L ND 1.0 04/28/23 00:230.34
1,3-Dichloropropane ug/L ND 1.0 04/28/23 00:230.28
1,4-Dichlorobenzene ug/L ND 1.0 04/28/23 00:230.33
2,2-Dichloropropane ug/L ND 1.0 04/28/23 00:230.39
2-Butanone (MEK)ug/L ND 5.0 04/28/23 00:234.0
2-Chlorotoluene ug/L ND 1.0 04/28/23 00:230.32
2-Hexanone ug/L ND 5.0 04/28/23 00:230.48
4-Chlorotoluene ug/L ND 1.0 04/28/23 00:230.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 04/28/23 00:232.7
Acetone ug/L ND 25.0 04/28/23 00:235.1
Benzene ug/L ND 1.0 04/28/23 00:230.34
Bromobenzene ug/L ND 1.0 04/28/23 00:230.29
Bromochloromethane ug/L ND 1.0 04/28/23 00:230.47
Bromodichloromethane ug/L ND 1.0 04/28/23 00:230.31
Bromoform ug/L ND 1.0 04/28/23 00:230.34
Bromomethane ug/L ND 2.0 04/28/23 00:231.7
Carbon tetrachloride ug/L ND 1.0 04/28/23 00:230.33
Chlorobenzene ug/L ND 1.0 04/28/23 00:230.28
Chloroethane ug/L ND 1.0 04/28/23 00:230.65
Chloroform ug/L ND 1.0 04/28/23 00:230.43
Chloromethane ug/L ND 1.0 04/28/23 00:230.54
cis-1,2-Dichloroethene ug/L ND 1.0 04/28/23 00:230.38
cis-1,3-Dichloropropene ug/L ND 1.0 04/28/23 00:230.36
Dibromochloromethane ug/L ND 1.0 04/28/23 00:230.36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4002511
Associated Lab Samples: 92663594013, 92663594014, 92663594015, 92663594016, 92663594017, 92663594018, 92663594020,
92663594022
Matrix: Water
AnalyzedMDL
Dibromomethane ug/L ND 1.0 04/28/23 00:230.39
Dichlorodifluoromethane ug/L ND 1.0 IH,v104/28/23 00:230.35
Diisopropyl ether ug/L ND 1.0 04/28/23 00:230.31
Ethylbenzene ug/L ND 1.0 04/28/23 00:230.30
Hexachloro-1,3-butadiene ug/L ND 2.0 04/28/23 00:231.5
m&p-Xylene ug/L ND 2.0 04/28/23 00:230.71
Methyl-tert-butyl ether ug/L ND 1.0 04/28/23 00:230.42
Methylene Chloride ug/L ND 5.0 04/28/23 00:232.0
Naphthalene ug/L ND 1.0 04/28/23 00:230.64
o-Xylene ug/L ND 1.0 04/28/23 00:230.34
p-Isopropyltoluene ug/L ND 1.0 04/28/23 00:230.41
Styrene ug/L ND 1.0 04/28/23 00:230.29
Tetrachloroethene ug/L ND 1.0 04/28/23 00:230.29
Toluene ug/L ND 1.0 04/28/23 00:230.24
trans-1,2-Dichloroethene ug/L ND 1.0 04/28/23 00:230.40
trans-1,3-Dichloropropene ug/L ND 1.0 04/28/23 00:230.36
Trichloroethene ug/L ND 1.0 04/28/23 00:230.38
Trichlorofluoromethane ug/L ND 1.0 04/28/23 00:230.30
Vinyl acetate ug/L ND 2.0 04/28/23 00:231.3
Vinyl chloride ug/L ND 1.0 04/28/23 00:230.39
Xylene (Total)ug/L ND 1.0 04/28/23 00:230.34
1,2-Dichloroethane-d4 (S)%107 70-130 04/28/23 00:23
4-Bromofluorobenzene (S)%96 70-130 04/28/23 00:23
Toluene-d8 (S)%103 70-130 04/28/23 00:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002512LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.920 109 70-130
1,1,1-Trichloroethane ug/L 18.420 92 70-130
1,1,2,2-Tetrachloroethane ug/L 24.620 123 70-130
1,1,2-Trichloroethane ug/L 23.420 117 70-130
1,1-Dichloroethane ug/L 18.720 93 70-130
1,1-Dichloroethene ug/L 17.620 88 70-130
1,1-Dichloropropene ug/L 19.820 99 70-130
1,2,3-Trichlorobenzene ug/L 23.420 117 70-130
1,2,3-Trichloropropane ug/L 23.020 115 70-130
1,2,4-Trichlorobenzene ug/L 21.920 110 70-130
1,2-Dibromo-3-chloropropane ug/L 22.720 114 70-131
1,2-Dibromoethane (EDB)ug/L 22.720 113 70-130
1,2-Dichlorobenzene ug/L 23.220 116 70-130
1,2-Dichloroethane ug/L 21.320 107 70-130
1,2-Dichloropropane ug/L 20.920 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002512LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 22.920 115 70-130
1,3-Dichloropropane ug/L 22.420 112 70-130
1,4-Dichlorobenzene ug/L 22.720 113 70-130
2,2-Dichloropropane ug/L 15.620 78 68-135
2-Butanone (MEK)ug/L 42.340 106 70-134
2-Chlorotoluene ug/L 23.020 115 70-130
2-Hexanone ug/L 46.340 116 70-131
4-Chlorotoluene ug/L 23.320 117 70-130
4-Methyl-2-pentanone (MIBK)ug/L 45.940 115 70-130
Acetone ug/L 39.940 100 70-133
Benzene ug/L 19.220 96 70-130
Bromobenzene ug/L 22.520 112 70-130
Bromochloromethane ug/L 18.720 94 70-130
Bromodichloromethane ug/L 21.220 106 70-130
Bromoform ug/L 20.720 104 70-130
Bromomethane ug/L 15.320 77 45-151
Carbon tetrachloride ug/L 19.020 95 70-130
Chlorobenzene ug/L 22.820 114 70-130
Chloroethane ug/L 18.420 92 39-152
Chloroform ug/L 20.220 101 70-130
Chloromethane ug/L 18.420 92 58-130
cis-1,2-Dichloroethene ug/L 19.520 97 70-130
cis-1,3-Dichloropropene ug/L 20.620 103 70-130
Dibromochloromethane ug/L 21.920 109 70-130
Dibromomethane ug/L 19.320 97 70-130
Dichlorodifluoromethane ug/L 23.9 IH,v120120 54-133
Diisopropyl ether ug/L 19.920 99 70-130
Ethylbenzene ug/L 22.420 112 70-130
Hexachloro-1,3-butadiene ug/L 22.620 113 70-135
m&p-Xylene ug/L 45.040 112 70-130
Methyl-tert-butyl ether ug/L 17.420 87 70-130
Methylene Chloride ug/L 21.120 106 66-130
Naphthalene ug/L 23.220 116 70-130
o-Xylene ug/L 22.320 111 70-130
p-Isopropyltoluene ug/L 23.620 118 70-130
Styrene ug/L 22.220 111 70-130
Tetrachloroethene ug/L 20.520 103 70-130
Toluene ug/L 20.820 104 70-130
trans-1,2-Dichloroethene ug/L 19.120 96 70-130
trans-1,3-Dichloropropene ug/L 21.120 106 70-130
Trichloroethene ug/L 19.720 99 70-130
Trichlorofluoromethane ug/L 18.020 90 62-130
Vinyl acetate ug/L 40.940 102 70-144
Vinyl chloride ug/L 14.920 74 62-130
Xylene (Total)ug/L 67.260 112 70-130
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 125 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4002512LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4002514MATRIX SPIKE SAMPLE:
MSSpike
Result
92663594014
1,1,1,2-Tetrachloroethane ug/L 20.320 102 70-141ND
1,1,1-Trichloroethane ug/L 21.620 108 70-150ND
1,1,2,2-Tetrachloroethane ug/L 22.020 110 69-142ND
1,1,2-Trichloroethane ug/L 21.620 108 70-138ND
1,1-Dichloroethane ug/L 22.620 113 70-150ND
1,1-Dichloroethene ug/L 24.220 121 70-156ND
1,1-Dichloropropene ug/L 22.020 110 70-150ND
1,2,3-Trichlorobenzene ug/L 18.120 90 70-148ND
1,2,3-Trichloropropane ug/L 21.520 107 70-140ND
1,2,4-Trichlorobenzene ug/L 17.120 86 70-146ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 68-146ND
1,2-Dibromoethane (EDB)ug/L 20.620 103 70-138ND
1,2-Dichlorobenzene ug/L 20.320 102 70-141ND
1,2-Dichloroethane ug/L 22.520 113 69-143ND
1,2-Dichloropropane ug/L 21.420 107 68-156ND
1,3-Dichlorobenzene ug/L 20.020 100 70-143ND
1,3-Dichloropropane ug/L 20.720 104 70-138ND
1,4-Dichlorobenzene ug/L 20.020 100 70-142ND
2,2-Dichloropropane ug/L 19.220 96 52-170ND
2-Butanone (MEK)ug/L 51.440 119 60-157ND
2-Chlorotoluene ug/L 20.520 102 70-147ND
2-Hexanone ug/L 44.240 111 68-146ND
4-Chlorotoluene ug/L 20.220 101 70-142ND
4-Methyl-2-pentanone (MIBK)ug/L 42.840 107 70-141ND
Acetone ug/L 47.740 119 58-157ND
Benzene ug/L 21.620 108 70-142ND
Bromobenzene ug/L 20.020 100 70-143ND
Bromochloromethane ug/L 20.920 104 70-146ND
Bromodichloromethane ug/L 20.320 101 70-139ND
Bromoform ug/L 18.420 92 64-140ND
Bromomethane ug/L 16.020 80 28-192ND
Carbon tetrachloride ug/L 21.220 106 70-148ND
Chlorobenzene ug/L 20.920 105 70-141ND
Chloroethane ug/L 28.720 144 58-191ND
Chloroform ug/L 22.520 110 70-1480.44J
Chloromethane ug/L 26.320 131 43-162ND
cis-1,2-Dichloroethene ug/L 23.020 111 68-1510.88J
cis-1,3-Dichloropropene ug/L 19.420 97 70-139ND
Dibromochloromethane ug/L 18.920 95 70-144ND
Dibromomethane ug/L 19.820 99 70-139ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4002514MATRIX SPIKE SAMPLE:
MSSpike
Result
92663594014
Dichlorodifluoromethane ug/L 39.1 IH,M1,v120195 39-171ND
Diisopropyl ether ug/L 21.720 109 67-142ND
Ethylbenzene ug/L 20.320 101 70-143ND
Hexachloro-1,3-butadiene ug/L 19.420 97 64-163ND
m&p-Xylene ug/L 40.340 101 70-144ND
Methyl-tert-butyl ether ug/L 18.720 94 65-143ND
Methylene Chloride ug/L 22.120 110 62-149ND
Naphthalene ug/L 19.020 95 67-147ND
o-Xylene ug/L 20.220 101 70-145ND
p-Isopropyltoluene ug/L 19.920 99 70-147ND
Styrene ug/L 20.120 101 70-143ND
Tetrachloroethene ug/L 20.020 91 70-1451.8
Toluene ug/L 21.320 106 70-142ND
trans-1,2-Dichloroethene ug/L 23.020 115 70-151ND
trans-1,3-Dichloropropene ug/L 18.720 93 70-139ND
Trichloroethene ug/L 22.620 102 62-1462.2
Trichlorofluoromethane ug/L 25.020 125 63-153ND
Vinyl acetate ug/L 38.940 97 61-162ND
Vinyl chloride ug/L 21.020 105 61-163ND
Xylene (Total)ug/L 60.560 101 70-143ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594013
4002513SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 127 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594013
4002513SAMPLE DUPLICATE:
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND IH,v130ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 0.55J 300.58J
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 300.57J
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%108107
4-Bromofluorobenzene (S)%9696
Toluene-d8 (S)%104102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769745
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663594017, 92663594020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3996395
Associated Lab Samples:92663594017, 92663594020
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 04/23/23 11:501.7
1,2-Dichlorobenzene ug/L ND 10.0 04/23/23 11:501.8
1,3-Dichlorobenzene ug/L ND 10.0 04/23/23 11:501.6
1,4-Dichlorobenzene ug/L ND 10.0 04/23/23 11:501.7
1-Methylnaphthalene ug/L ND 10.0 04/23/23 11:502.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 04/23/23 11:501.2
2,4,5-Trichlorophenol ug/L ND 10.0 04/23/23 11:501.4
2,4,6-Trichlorophenol ug/L ND 10.0 04/23/23 11:501.6
2,4-Dichlorophenol ug/L ND 10.0 04/23/23 11:501.4
2,4-Dimethylphenol ug/L ND 10.0 v204/23/23 11:501.7
2,4-Dinitrophenol ug/L ND 50.0 04/23/23 11:5026.0
2,4-Dinitrotoluene ug/L ND 10.0 04/23/23 11:501.6
2,6-Dinitrotoluene ug/L ND 10.0 04/23/23 11:501.7
2-Chloronaphthalene ug/L ND 10.0 04/23/23 11:501.7
2-Chlorophenol ug/L ND 10.0 04/23/23 11:501.2
2-Methylnaphthalene ug/L ND 10.0 04/23/23 11:501.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 04/23/23 11:501.9
2-Nitroaniline ug/L ND 20.0 04/23/23 11:503.0
2-Nitrophenol ug/L ND 10.0 04/23/23 11:501.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 04/23/23 11:501.2
3,3'-Dichlorobenzidine ug/L ND 20.0 04/23/23 11:508.1
3-Nitroaniline ug/L ND 20.0 04/23/23 11:503.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/23/23 11:507.8
4-Bromophenylphenyl ether ug/L ND 10.0 04/23/23 11:501.8
4-Chloro-3-methylphenol ug/L ND 10.0 04/23/23 11:503.3
4-Chloroaniline ug/L ND 20.0 04/23/23 11:503.6
4-Chlorophenylphenyl ether ug/L ND 10.0 04/23/23 11:502.0
4-Nitroaniline ug/L ND 20.0 04/23/23 11:505.1
4-Nitrophenol ug/L ND 50.0 04/23/23 11:506.6
Acenaphthene ug/L ND 10.0 04/23/23 11:502.0
Acenaphthylene ug/L ND 10.0 04/23/23 11:502.0
Aniline ug/L ND 10.0 04/23/23 11:501.6
Anthracene ug/L ND 10.0 04/23/23 11:502.3
Benzo(a)anthracene ug/L ND 10.0 04/23/23 11:502.7
Benzo(a)pyrene ug/L ND 10.0 04/23/23 11:502.8
Benzo(b)fluoranthene ug/L ND 10.0 04/23/23 11:502.6
Benzo(g,h,i)perylene ug/L ND 10.0 04/23/23 11:502.8
Benzo(k)fluoranthene ug/L ND 10.0 04/23/23 11:502.7
Benzoic Acid ug/L ND 50.0 04/23/23 11:5022.0
Benzyl alcohol ug/L ND 20.0 04/23/23 11:502.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3996395
Associated Lab Samples:92663594017, 92663594020
Matrix: Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/23/23 11:501.8
bis(2-Chloroethyl) ether ug/L ND 10.0 04/23/23 11:501.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 04/23/23 11:503.7
Butylbenzylphthalate ug/L ND 10.0 04/23/23 11:503.1
Chrysene ug/L ND 10.0 04/23/23 11:502.8
Di-n-butylphthalate ug/L ND 10.0 04/23/23 11:502.2
Di-n-octylphthalate ug/L ND 10.0 04/23/23 11:503.9
Dibenz(a,h)anthracene ug/L ND 10.0 04/23/23 11:503.0
Dibenzofuran ug/L ND 10.0 04/23/23 11:502.1
Diethylphthalate ug/L ND 10.0 04/23/23 11:502.0
Dimethylphthalate ug/L ND 10.0 04/23/23 11:502.1
Fluoranthene ug/L ND 10.0 04/23/23 11:502.2
Fluorene ug/L ND 10.0 04/23/23 11:502.1
Hexachloro-1,3-butadiene ug/L ND 10.0 04/23/23 11:501.8
Hexachlorobenzene ug/L ND 10.0 04/23/23 11:502.2
Hexachlorocyclopentadiene ug/L ND 10.0 04/23/23 11:501.6
Hexachloroethane ug/L ND 10.0 04/23/23 11:501.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 04/23/23 11:502.9
Isophorone ug/L ND 10.0 04/23/23 11:501.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 04/23/23 11:501.3
N-Nitrosodimethylamine ug/L ND 10.0 04/23/23 11:501.9
N-Nitrosodiphenylamine ug/L ND 10.0 04/23/23 11:503.0
Naphthalene ug/L ND 10.0 04/23/23 11:502.1
Nitrobenzene ug/L ND 10.0 04/23/23 11:501.9
Pentachlorophenol ug/L ND 20.0 04/23/23 11:503.8
Phenanthrene ug/L ND 10.0 04/23/23 11:502.0
Phenol ug/L ND 10.0 04/23/23 11:501.4
Pyrene ug/L ND 10.0 04/23/23 11:502.2
2,4,6-Tribromophenol (S)%88 10-164 04/23/23 11:50
2-Fluorobiphenyl (S)%62 10-130 04/23/23 11:50
2-Fluorophenol (S)%59 10-130 04/23/23 11:50
Nitrobenzene-d5 (S)%76 10-138 04/23/23 11:50
Phenol-d6 (S)%46 10-130 04/23/23 11:50
Terphenyl-d14 (S)%90 19-191 04/23/23 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3996396LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 30.150 60 11-130
1,2-Dichlorobenzene ug/L 25.850 52 10-130
1,3-Dichlorobenzene ug/L 24.350 49 10-130
1,4-Dichlorobenzene ug/L 25.050 50 10-130
1-Methylnaphthalene ug/L 38.550 77 23-130
2,2'-Oxybis(1-chloropropane)ug/L 34.550 69 21-135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 130 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3996396LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 44.650 89 38-147
2,4,6-Trichlorophenol ug/L 43.150 86 34-142
2,4-Dichlorophenol ug/L 43.850 88 36-136
2,4-Dimethylphenol ug/L 66.0 v350132 38-134
2,4-Dinitrophenol ug/L 182250 73 10-169
2,4-Dinitrotoluene ug/L 43.150 86 44-154
2,6-Dinitrotoluene ug/L 44.050 88 44-156
2-Chloronaphthalene ug/L 38.650 77 25-130
2-Chlorophenol ug/L 39.450 79 29-130
2-Methylnaphthalene ug/L 36.150 72 23-130
2-Methylphenol(o-Cresol)ug/L 40.050 80 31-130
2-Nitroaniline ug/L 79.3100 79 39-145
2-Nitrophenol ug/L 44.750 89 29-142
3&4-Methylphenol(m&p Cresol)ug/L 37.650 75 30-130
3,3'-Dichlorobenzidine ug/L 81.1100 81 44-158
3-Nitroaniline ug/L 81.3100 81 45-152
4,6-Dinitro-2-methylphenol ug/L 90.7100 91 39-158
4-Bromophenylphenyl ether ug/L 43.350 87 47-147
4-Chloro-3-methylphenol ug/L 83.3100 83 40-138
4-Chloroaniline ug/L 71.0100 71 35-130
4-Chlorophenylphenyl ether ug/L 40.150 80 36-139
4-Nitroaniline ug/L 77.4100 77 46-157
4-Nitrophenol ug/L 132250 53 17-130
Acenaphthene ug/L 39.750 79 34-135
Acenaphthylene ug/L 40.750 81 35-137
Aniline ug/L 13.950 28 25-130
Anthracene ug/L 38.950 78 47-146
Benzo(a)anthracene ug/L 41.450 83 48-160
Benzo(a)pyrene ug/L 41.250 82 47-165
Benzo(b)fluoranthene ug/L 41.550 83 49-171
Benzo(g,h,i)perylene ug/L 40.050 80 46-166
Benzo(k)fluoranthene ug/L 43.150 86 55-162
Benzoic Acid ug/L 101250 40 10-130
Benzyl alcohol ug/L 75.0100 75 29-132
bis(2-Chloroethoxy)methane ug/L 40.250 80 33-136
bis(2-Chloroethyl) ether ug/L 38.550 77 30-142
bis(2-Ethylhexyl)phthalate ug/L 44.550 89 46-173
Butylbenzylphthalate ug/L 45.550 91 53-169
Chrysene ug/L 41.450 83 54-152
Di-n-butylphthalate ug/L 43.050 86 49-161
Di-n-octylphthalate ug/L 44.450 89 50-166
Dibenz(a,h)anthracene ug/L 41.150 82 46-166
Dibenzofuran ug/L 40.150 80 37-136
Diethylphthalate ug/L 41.550 83 45-149
Dimethylphthalate ug/L 40.750 81 43-145
Fluoranthene ug/L 42.050 84 50-153
Fluorene ug/L 41.150 82 42-142
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3996396LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 25.950 52 10-130
Hexachlorobenzene ug/L 42.750 85 44-138
Hexachlorocyclopentadiene ug/L 33.950 68 10-130
Hexachloroethane ug/L 23.250 46 10-130
Indeno(1,2,3-cd)pyrene ug/L 41.550 83 46-166
Isophorone ug/L 42.950 86 36-135
N-Nitroso-di-n-propylamine ug/L 41.150 82 33-140
N-Nitrosodimethylamine ug/L 35.550 71 24-130
N-Nitrosodiphenylamine ug/L 42.050 84 46-144
Naphthalene ug/L 33.550 67 20-130
Nitrobenzene ug/L 40.050 80 33-133
Pentachlorophenol ug/L 89.6100 90 21-163
Phenanthrene ug/L 41.650 83 47-146
Phenol ug/L 27.350 55 19-130
Pyrene ug/L 43.050 86 53-155
2,4,6-Tribromophenol (S)%128 10-164
2-Fluorobiphenyl (S)%93 10-130
2-Fluorophenol (S)%77 10-130
Nitrobenzene-d5 (S)%102 10-138
Phenol-d6 (S)%63 10-130
Terphenyl-d14 (S)%110 19-191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 132 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770122
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016, 92663594018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3997898
Associated Lab Samples:92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016, 92663594018
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 04/26/23 12:461.7
1,2-Dichlorobenzene ug/L ND 10.0 04/26/23 12:461.8
1,3-Dichlorobenzene ug/L ND 10.0 04/26/23 12:461.6
1,4-Dichlorobenzene ug/L ND 10.0 04/26/23 12:461.7
1-Methylnaphthalene ug/L ND 10.0 04/26/23 12:462.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 04/26/23 12:461.2
2,4,5-Trichlorophenol ug/L ND 10.0 04/26/23 12:461.4
2,4,6-Trichlorophenol ug/L ND 10.0 04/26/23 12:461.6
2,4-Dichlorophenol ug/L ND 10.0 04/26/23 12:461.4
2,4-Dimethylphenol ug/L ND 10.0 v204/26/23 12:461.7
2,4-Dinitrophenol ug/L ND 50.0 04/26/23 12:4626.0
2,4-Dinitrotoluene ug/L ND 10.0 04/26/23 12:461.6
2,6-Dinitrotoluene ug/L ND 10.0 04/26/23 12:461.7
2-Chloronaphthalene ug/L ND 10.0 04/26/23 12:461.7
2-Chlorophenol ug/L ND 10.0 04/26/23 12:461.2
2-Methylnaphthalene ug/L ND 10.0 04/26/23 12:461.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 04/26/23 12:461.9
2-Nitroaniline ug/L ND 20.0 04/26/23 12:463.0
2-Nitrophenol ug/L ND 10.0 04/26/23 12:461.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 04/26/23 12:461.2
3,3'-Dichlorobenzidine ug/L ND 20.0 04/26/23 12:468.1
3-Nitroaniline ug/L ND 20.0 04/26/23 12:463.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 04/26/23 12:467.8
4-Bromophenylphenyl ether ug/L ND 10.0 04/26/23 12:461.8
4-Chloro-3-methylphenol ug/L ND 10.0 04/26/23 12:463.3
4-Chloroaniline ug/L ND 20.0 04/26/23 12:463.6
4-Chlorophenylphenyl ether ug/L ND 10.0 04/26/23 12:462.0
4-Nitroaniline ug/L ND 20.0 04/26/23 12:465.1
4-Nitrophenol ug/L ND 50.0 04/26/23 12:466.6
Acenaphthene ug/L ND 10.0 04/26/23 12:462.0
Acenaphthylene ug/L ND 10.0 04/26/23 12:462.0
Aniline ug/L ND 10.0 04/26/23 12:461.6
Anthracene ug/L ND 10.0 04/26/23 12:462.3
Benzo(a)anthracene ug/L ND 10.0 04/26/23 12:462.7
Benzo(a)pyrene ug/L ND 10.0 04/26/23 12:462.8
Benzo(b)fluoranthene ug/L ND 10.0 04/26/23 12:462.6
Benzo(g,h,i)perylene ug/L ND 10.0 04/26/23 12:462.8
Benzo(k)fluoranthene ug/L ND 10.0 04/26/23 12:462.7
Benzoic Acid ug/L ND 50.0 04/26/23 12:4622.0
Benzyl alcohol ug/L ND 20.0 04/26/23 12:462.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3997898
Associated Lab Samples:92663594011, 92663594012, 92663594013, 92663594014, 92663594015, 92663594016, 92663594018
Matrix: Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/26/23 12:461.8
bis(2-Chloroethyl) ether ug/L ND 10.0 04/26/23 12:461.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 04/26/23 12:463.7
Butylbenzylphthalate ug/L ND 10.0 04/26/23 12:463.1
Chrysene ug/L ND 10.0 04/26/23 12:462.8
Di-n-butylphthalate ug/L ND 10.0 04/26/23 12:462.2
Di-n-octylphthalate ug/L ND 10.0 04/26/23 12:463.9
Dibenz(a,h)anthracene ug/L ND 10.0 04/26/23 12:463.0
Dibenzofuran ug/L ND 10.0 04/26/23 12:462.1
Diethylphthalate ug/L ND 10.0 04/26/23 12:462.0
Dimethylphthalate ug/L ND 10.0 04/26/23 12:462.1
Fluoranthene ug/L ND 10.0 04/26/23 12:462.2
Fluorene ug/L ND 10.0 04/26/23 12:462.1
Hexachloro-1,3-butadiene ug/L ND 10.0 04/26/23 12:461.8
Hexachlorobenzene ug/L ND 10.0 04/26/23 12:462.2
Hexachlorocyclopentadiene ug/L ND 10.0 04/26/23 12:461.6
Hexachloroethane ug/L ND 10.0 04/26/23 12:461.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 04/26/23 12:462.9
Isophorone ug/L ND 10.0 04/26/23 12:461.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 04/26/23 12:461.3
N-Nitrosodimethylamine ug/L ND 10.0 04/26/23 12:461.9
N-Nitrosodiphenylamine ug/L ND 10.0 04/26/23 12:463.0
Naphthalene ug/L ND 10.0 04/26/23 12:462.1
Nitrobenzene ug/L ND 10.0 04/26/23 12:461.9
Pentachlorophenol ug/L ND 20.0 04/26/23 12:463.8
Phenanthrene ug/L ND 10.0 04/26/23 12:462.0
Phenol ug/L ND 10.0 04/26/23 12:461.4
Pyrene ug/L ND 10.0 04/26/23 12:462.2
2,4,6-Tribromophenol (S)%71 10-164 04/26/23 12:46
2-Fluorobiphenyl (S)%54 10-130 04/26/23 12:46
2-Fluorophenol (S)%47 10-130 04/26/23 12:46
Nitrobenzene-d5 (S)%64 10-138 04/26/23 12:46
Phenol-d6 (S)%39 10-130 04/26/23 12:46
Terphenyl-d14 (S)%76 19-191 04/26/23 12:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3997899LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 22.750 45 11-130
1,2-Dichlorobenzene ug/L 22.450 45 10-130
1,3-Dichlorobenzene ug/L 21.650 43 10-130
1,4-Dichlorobenzene ug/L 21.650 43 10-130
1-Methylnaphthalene ug/L 26.450 53 23-130
2,2'-Oxybis(1-chloropropane)ug/L 28.750 57 21-135
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3997899LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 39.450 79 38-147
2,4,6-Trichlorophenol ug/L 39.250 78 34-142
2,4-Dichlorophenol ug/L 39.250 78 36-136
2,4-Dimethylphenol ug/L 59.7 v350119 38-134
2,4-Dinitrophenol ug/L 187250 75 10-169
2,4-Dinitrotoluene ug/L 40.350 81 44-154
2,6-Dinitrotoluene ug/L 39.550 79 44-156
2-Chloronaphthalene ug/L 27.150 54 25-130
2-Chlorophenol ug/L 35.350 71 29-130
2-Methylnaphthalene ug/L 24.950 50 23-130
2-Methylphenol(o-Cresol)ug/L 37.150 74 31-130
2-Nitroaniline ug/L 71.9100 72 39-145
2-Nitrophenol ug/L 39.150 78 29-142
3&4-Methylphenol(m&p Cresol)ug/L 34.050 68 30-130
3,3'-Dichlorobenzidine ug/L 72.4100 72 44-158
3-Nitroaniline ug/L 75.4100 75 45-152
4,6-Dinitro-2-methylphenol ug/L 86.9100 87 39-158
4-Bromophenylphenyl ether ug/L 37.750 75 47-147
4-Chloro-3-methylphenol ug/L 77.2100 77 40-138
4-Chloroaniline ug/L 67.5100 67 35-130
4-Chlorophenylphenyl ether ug/L 34.450 69 36-139
4-Nitroaniline ug/L 71.3100 71 46-157
4-Nitrophenol ug/L 127250 51 17-130
Acenaphthene ug/L 31.950 64 34-135
Acenaphthylene ug/L 32.250 64 35-137
Aniline ug/L 21.450 43 25-130
Anthracene ug/L 35.550 71 47-146
Benzo(a)anthracene ug/L 39.150 78 48-160
Benzo(a)pyrene ug/L 39.550 79 47-165
Benzo(b)fluoranthene ug/L 40.750 81 49-171
Benzo(g,h,i)perylene ug/L 38.450 77 46-166
Benzo(k)fluoranthene ug/L 42.950 86 55-162
Benzoic Acid ug/L 105250 42 10-130
Benzyl alcohol ug/L 68.1100 68 29-132
bis(2-Chloroethoxy)methane ug/L 37.650 75 33-136
bis(2-Chloroethyl) ether ug/L 34.350 69 30-142
bis(2-Ethylhexyl)phthalate ug/L 40.450 81 46-173
Butylbenzylphthalate ug/L 42.150 84 53-169
Chrysene ug/L 39.250 78 54-152
Di-n-butylphthalate ug/L 39.450 79 49-161
Di-n-octylphthalate ug/L 38.050 76 50-166
Dibenz(a,h)anthracene ug/L 39.150 78 46-166
Dibenzofuran ug/L 33.850 68 37-136
Diethylphthalate ug/L 38.650 77 45-149
Dimethylphthalate ug/L 37.350 75 43-145
Fluoranthene ug/L 38.850 78 50-153
Fluorene ug/L 35.950 72 42-142
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3997899LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 22.150 44 10-130
Hexachlorobenzene ug/L 38.050 76 44-138
Hexachlorocyclopentadiene ug/L 21.750 43 10-130
Hexachloroethane ug/L 21.650 43 10-130
Indeno(1,2,3-cd)pyrene ug/L 39.050 78 46-166
Isophorone ug/L 38.750 77 36-135
N-Nitroso-di-n-propylamine ug/L 37.950 76 33-140
N-Nitrosodimethylamine ug/L 32.350 65 24-130
N-Nitrosodiphenylamine ug/L 37.550 75 46-144
Naphthalene ug/L 24.950 50 20-130
Nitrobenzene ug/L 34.350 69 33-133
Pentachlorophenol ug/L 83.4100 83 21-163
Phenanthrene ug/L 37.950 76 47-146
Phenol ug/L 26.150 52 19-130
Pyrene ug/L 42.250 84 53-155
2,4,6-Tribromophenol (S)%99 10-164
2-Fluorobiphenyl (S)%69 10-130
2-Fluorophenol (S)%60 10-130
Nitrobenzene-d5 (S)%79 10-138
Phenol-d6 (S)%49 10-130
Terphenyl-d14 (S)%93 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3997900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594013
3997901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R183.3 27 10-13042 44 3083.3ND 22.2 34.6
1,2-Dichlorobenzene ug/L R183.3 27 10-13040 41 3083.3ND 22.1 33.6
1,3-Dichlorobenzene ug/L R183.3 23 10-13038 49 3083.3ND 19.4 32.0
1,4-Dichlorobenzene ug/L R183.3 24 10-13039 50 3083.3ND 19.7 32.7
1-Methylnaphthalene ug/L 83.3 52 10-13152 1 3083.3ND 43.0 43.6
2,2'-Oxybis(1-chloropropane)ug/L 83.3 60 11-14353 13 3083.3ND 50.1 44.2
2,4,5-Trichlorophenol ug/L 83.3 85 10-17084 1 3083.3ND 70.7 69.7
2,4,6-Trichlorophenol ug/L 83.3 85 10-16675 12 3083.3ND 70.6 62.8
2,4-Dichlorophenol ug/L 83.3 81 10-15376 7 3083.3ND 67.7 63.2
2,4-Dimethylphenol ug/L v1,v383.3 124 20-147104 18 3083.3ND 104 86.5
2,4-Dinitrophenol ug/L 417 82 10-17291 10 30417ND340 377
2,4-Dinitrotoluene ug/L 83.3 87 30-16494 8 3083.3ND 72.8 78.5
2,6-Dinitrotoluene ug/L 83.3 84 31-16384 0 3083.3ND 70.2 70.1
2-Chloronaphthalene ug/L 83.3 62 15-13454 13 3083.3ND 51.3 45.0
2-Chlorophenol ug/L 83.3 74 10-13967 10 3083.3ND 61.8 55.8
2-Methylnaphthalene ug/L 83.3 47 12-13048 3 3083.3ND 39.3 40.3
2-Methylphenol(o-Cresol) ug/L 83.3 76 19-13267 12 3083.3ND 63.2 55.9
2-Nitroaniline ug/L 167 75 23-15472 4 30167ND126 120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3997900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594013
3997901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 83.3 82 10-15978 5 3083.3ND 68.3 64.8
3&4-Methylphenol(m&p
Cresol)ug/L 83.3 70 13-13663 9 3083.3ND 58.0 52.9
3,3'-Dichlorobenzidine ug/L 167 68 10-17885 23 30167ND113 142
3-Nitroaniline ug/L 167 78 20-16687 11 30167ND130 145
4,6-Dinitro-2-methylphenol ug/L v11679810-187103 5 30167ND163 171
4-Bromophenylphenyl ether ug/L 83.3 83 31-15778 6 3083.3ND 69.0 64.8
4-Chloro-3-methylphenol ug/L 167 78 27-14678 0 30167ND130 130
4-Chloroaniline ug/L 167 63 13-14365 4 30167ND105 109
4-Chlorophenylphenyl ether ug/L 83.3 74 23-14970 5 3083.3ND 61.6 58.5
4-Nitroaniline ug/L 167 79 24-17188 11 30167ND132 147
4-Nitrophenol ug/L 417 54 10-13057 5 30417ND224 236
Acenaphthene ug/L 83.3 70 21-14763 11 3083.3ND 58.5 52.2
Acenaphthylene ug/L 83.3 71 19-15063 12 3083.3ND 58.9 52.3
Aniline ug/L 83.3 42 10-13048 14 3083.3ND 35.2 40.4
Anthracene ug/L 83.3 79 36-15278 1 3083.3ND 65.5 64.8
Benzo(a)anthracene ug/L 83.3 88 42-16386 3 3083.3ND 73.5 71.6
Benzo(a)pyrene ug/L 83.3 91 40-16986 5 3083.3ND 75.6 71.6
Benzo(b)fluoranthene ug/L 83.3 93 40-17785 8 3083.3ND 77.2 71.2
Benzo(g,h,i)perylene ug/L 83.3 88 38-17491 3 3083.3ND 73.0 75.5
Benzo(k)fluoranthene ug/L 83.3 95 41-17186 9 3083.3ND 78.8 71.9
Benzoic Acid ug/L 417 46 10-13040 13 30417ND192 168
Benzyl alcohol ug/L 167 70 18-14166 6 30167ND117 109
bis(2-Chloroethoxy)methane ug/L 83.3 76 19-14669 9 3083.3ND 63.2 57.5
bis(2-Chloroethyl) ether ug/L 83.3 72 19-15165 10 3083.3ND 60.2 54.3
bis(2-Ethylhexyl)phthalate ug/L 83.3 95 42-16892 3 3083.3ND 78.9 76.5
Butylbenzylphthalate ug/L 83.3 99 42-17793 6 3083.3ND 82.4 77.9
Chrysene ug/L 83.3 89 43-15986 4 3083.3ND 74.2 71.6
Di-n-butylphthalate ug/L 83.3 89 42-16092 4 3083.3ND 74.0 76.8
Di-n-octylphthalate ug/L 83.3 98 42-171100 3 3083.3ND 81.5 83.7
Dibenz(a,h)anthracene ug/L 83.3 89 40-17193 5 3083.3ND 74.2 77.7
Dibenzofuran ug/L 83.3 73 23-14767 8 3083.3ND 60.7 56.2
Diethylphthalate ug/L 83.3 82 33-15787 7 3083.3ND 68.1 72.7
Dimethylphthalate ug/L 83.3 79 27-15480 1 3083.3ND 66.2 67.0
Fluoranthene ug/L 83.3 87 42-15792 6 3083.3ND 72.8 77.0
Fluorene ug/L 83.3 78 25-15574 5 3083.3ND 64.8 61.7
Hexachloro-1,3-butadiene ug/L 83.3 19 10-13037 3083.3ND 15.7J 31.2
Hexachlorobenzene ug/L 83.3 84 32-14580 4 3083.3ND 69.9 66.9
Hexachlorocyclopentadiene ug/L 83.3 30 10-13039 25 3083.3ND 25.0 32.1
Hexachloroethane ug/L 83.3 19 10-13037 3083.3ND 15.8J 30.9
Indeno(1,2,3-cd)pyrene ug/L 83.3 90 39-17493 3 3083.3ND 75.0 77.4
Isophorone ug/L 83.3 78 19-14673 7 3083.3ND 64.6 60.4
N-Nitroso-di-n-propylamine ug/L 83.3 77 20-15068 12 3083.3ND 64.1 56.9
N-Nitrosodimethylamine ug/L 83.3 67 13-13058 14 3083.3ND 56.0 48.4
N-Nitrosodiphenylamine ug/L 83.3 83 33-14979 5 3083.3ND 69.4 66.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3997900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594013
3997901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 83.3 40 10-12847 18 3083.3ND 33.0 39.5
Nitrobenzene ug/L 83.3 72 19-14568 5 3083.3ND 60.1 57.0
Pentachlorophenol ug/L v11679810-18898 0 30167ND163 163
Phenanthrene ug/L 83.3 84 38-15082 2 3083.3ND 70.1 68.6
Phenol ug/L 83.3 52 10-13045 13 3083.3ND 43.0 37.7
Pyrene ug/L 83.3 93 42-16382 12 3083.3ND 77.2 68.5
2,4,6-Tribromophenol (S) %102 10-16495
2-Fluorobiphenyl (S)%70 10-13058
2-Fluorophenol (S)%57 10-13046
Nitrobenzene-d5 (S)%77 10-13867
Phenol-d6 (S)%46 10-13037
Terphenyl-d14 (S)%95 19-19180
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770544
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3999982
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 325 04/27/23 07:46128
1,2-Dichlorobenzene ug/kg ND 325 04/27/23 07:46117
1,3-Dichlorobenzene ug/kg ND 325 04/27/23 07:46115
1,4-Dichlorobenzene ug/kg ND 325 04/27/23 07:46124
1-Methylnaphthalene ug/kg ND 325 04/27/23 07:46114
2,2'-Oxybis(1-chloropropane)ug/kg ND 325 04/27/23 07:46154
2,4,5-Trichlorophenol ug/kg ND 325 04/27/23 07:46149
2,4,6-Trichlorophenol ug/kg ND 325 04/27/23 07:46134
2,4-Dichlorophenol ug/kg ND 325 04/27/23 07:46127
2,4-Dimethylphenol ug/kg ND 325 04/27/23 07:46135
2,4-Dinitrophenol ug/kg ND 1620 04/27/23 07:461000
2,4-Dinitrotoluene ug/kg ND 325 04/27/23 07:46125
2,6-Dinitrotoluene ug/kg ND 325 04/27/23 07:46119
2-Chloronaphthalene ug/kg ND 325 04/27/23 07:46129
2-Chlorophenol ug/kg ND 325 04/27/23 07:46122
2-Methylnaphthalene ug/kg ND 325 04/27/23 07:46130
2-Methylphenol(o-Cresol)ug/kg ND 325 04/27/23 07:46133
2-Nitroaniline ug/kg ND 1620 04/27/23 07:46266
2-Nitrophenol ug/kg ND 325 04/27/23 07:46141
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 04/27/23 07:46131
3,3'-Dichlorobenzidine ug/kg ND 649 04/27/23 07:46219
3-Nitroaniline ug/kg ND 1620 04/27/23 07:46255
4,6-Dinitro-2-methylphenol ug/kg ND 649 04/27/23 07:46303
4-Bromophenylphenyl ether ug/kg ND 325 04/27/23 07:46125
4-Chloro-3-methylphenol ug/kg ND 649 04/27/23 07:46228
4-Chloroaniline ug/kg ND 649 04/27/23 07:46255
4-Chlorophenylphenyl ether ug/kg ND 325 04/27/23 07:46121
4-Nitroaniline ug/kg ND 649 04/27/23 07:46247
4-Nitrophenol ug/kg ND 1620 04/27/23 07:46628
Acenaphthene ug/kg ND 325 04/27/23 07:46114
Acenaphthylene ug/kg ND 325 04/27/23 07:46114
Aniline ug/kg ND 325 04/27/23 07:46127
Anthracene ug/kg ND 325 04/27/23 07:46106
Benzo(a)anthracene ug/kg ND 325 04/27/23 07:46108
Benzo(a)pyrene ug/kg ND 325 04/27/23 07:46112
Benzo(b)fluoranthene ug/kg ND 325 04/27/23 07:46108
Benzo(g,h,i)perylene ug/kg ND 325 04/27/23 07:46126
Benzo(k)fluoranthene ug/kg ND 325 04/27/23 07:46114
Benzoic Acid ug/kg ND 1620 04/27/23 07:46697
Benzyl alcohol ug/kg ND 649 04/27/23 07:46246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3999982
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 325 04/27/23 07:46135
bis(2-Chloroethyl) ether ug/kg ND 325 04/27/23 07:46122
bis(2-Ethylhexyl)phthalate ug/kg ND 325 04/27/23 07:46126
Butylbenzylphthalate ug/kg ND 325 04/27/23 07:46137
Chrysene ug/kg ND 325 04/27/23 07:46118
Di-n-butylphthalate ug/kg ND 325 04/27/23 07:46109
Di-n-octylphthalate ug/kg ND 325 04/27/23 07:46128
Dibenz(a,h)anthracene ug/kg ND 325 04/27/23 07:46125
Dibenzofuran ug/kg ND 325 04/27/23 07:46117
Diethylphthalate ug/kg ND 325 04/27/23 07:46119
Dimethylphthalate ug/kg ND 325 04/27/23 07:46118
Fluoranthene ug/kg ND 325 04/27/23 07:46111
Fluorene ug/kg ND 325 04/27/23 07:46114
Hexachloro-1,3-butadiene ug/kg ND 325 04/27/23 07:46141
Hexachlorobenzene ug/kg ND 325 04/27/23 07:46127
Hexachlorocyclopentadiene ug/kg ND 325 04/27/23 07:46186
Hexachloroethane ug/kg ND 325 04/27/23 07:46124
Indeno(1,2,3-cd)pyrene ug/kg ND 325 04/27/23 07:46128
Isophorone ug/kg ND 325 04/27/23 07:46145
N-Nitroso-di-n-propylamine ug/kg ND 325 04/27/23 07:46122
N-Nitrosodimethylamine ug/kg ND 325 04/27/23 07:46109
N-Nitrosodiphenylamine ug/kg ND 325 04/27/23 07:46115
Naphthalene ug/kg ND 325 04/27/23 07:46110
Nitrobenzene ug/kg ND 325 04/27/23 07:46150
Pentachlorophenol ug/kg ND 649 04/27/23 07:46318
Phenanthrene ug/kg ND 325 04/27/23 07:46106
Phenol ug/kg ND 325 04/27/23 07:46145
Pyrene ug/kg ND 325 04/27/23 07:46132
Pyridine ug/kg ND 325 04/27/23 07:46102
2,4,6-Tribromophenol (S)%70 10-131 04/27/23 07:46
2-Fluorobiphenyl (S)%67 10-130 04/27/23 07:46
2-Fluorophenol (S)%65 10-130 04/27/23 07:46
Nitrobenzene-d5 (S)%69 10-130 04/27/23 07:46
Phenol-d6 (S)%67 10-130 04/27/23 07:46
Terphenyl-d14 (S)%78 10-130 04/27/23 07:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3999983LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 8191670 49 43-130
1,2-Dichlorobenzene ug/kg 8231670 49 43-130
1,3-Dichlorobenzene ug/kg 8021670 48 43-130
1,4-Dichlorobenzene ug/kg 8111670 49 44-130
1-Methylnaphthalene ug/kg 9331670 56 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 140 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3999983LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 7711670 46 29-130
2,4,5-Trichlorophenol ug/kg 11301670 68 47-130
2,4,6-Trichlorophenol ug/kg 10701670 64 47-130
2,4-Dichlorophenol ug/kg 9331670 56 45-130
2,4-Dimethylphenol ug/kg 13301670 80 45-130
2,4-Dinitrophenol ug/kg 65208330 78 27-140
2,4-Dinitrotoluene ug/kg 13401670 80 46-130
2,6-Dinitrotoluene ug/kg 13401670 81 48-130
2-Chloronaphthalene ug/kg 9111670 55 46-130
2-Chlorophenol ug/kg 8501670 51 43-130
2-Methylnaphthalene ug/kg 8931670 54 47-130
2-Methylphenol(o-Cresol)ug/kg 9091670 55 42-130
2-Nitroaniline ug/kg 23103330 69 41-130
2-Nitrophenol ug/kg 9701670 58 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 9461670 57 39-130
3,3'-Dichlorobenzidine ug/kg 25603330 77 41-130
3-Nitroaniline ug/kg 23903330 72 37-130
4,6-Dinitro-2-methylphenol ug/kg 29303330 88 38-141
4-Bromophenylphenyl ether ug/kg 12501670 75 47-130
4-Chloro-3-methylphenol ug/kg 21903330 66 44-130
4-Chloroaniline ug/kg 17203330 52 41-130
4-Chlorophenylphenyl ether ug/kg 11201670 67 45-130
4-Nitroaniline ug/kg 24203330 73 42-130
4-Nitrophenol ug/kg 65808330 79 39-131
Acenaphthene ug/kg 10401670 62 49-130
Acenaphthylene ug/kg 10401670 62 50-130
Aniline ug/kg 7221670 43 38-130
Anthracene ug/kg 12401670 75 49-130
Benzo(a)anthracene ug/kg 13901670 83 51-130
Benzo(a)pyrene ug/kg 15001670 90 51-130
Benzo(b)fluoranthene ug/kg 15001670 90 49-130
Benzo(g,h,i)perylene ug/kg 16501670 99 48-140
Benzo(k)fluoranthene ug/kg 14901670 89 51-130
Benzoic Acid ug/kg 36708330 44 22-130
Benzyl alcohol ug/kg 17603330 53 43-130
bis(2-Chloroethoxy)methane ug/kg 8371670 50 43-130
bis(2-Chloroethyl) ether ug/kg 7871670 47 42-130
bis(2-Ethylhexyl)phthalate ug/kg 14901670 89 43-130
Butylbenzylphthalate ug/kg 15101670 91 44-131
Chrysene ug/kg 14001670 84 51-130
Di-n-butylphthalate ug/kg 13901670 84 46-130
Di-n-octylphthalate ug/kg 15101670 90 45-130
Dibenz(a,h)anthracene ug/kg 16601670 100 48-130
Dibenzofuran ug/kg 10601670 64 10-130
Diethylphthalate ug/kg 13301670 80 48-130
Dimethylphthalate ug/kg 12801670 77 48-130
Fluoranthene ug/kg 13501670 81 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 141 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3999983LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11901670 71 48-130
Hexachloro-1,3-butadiene ug/kg 7801670 47 39-130
Hexachlorobenzene ug/kg 13101670 78 47-130
Hexachlorocyclopentadiene ug/kg 7721670 46 17-130
Hexachloroethane ug/kg 7821670 47 40-130
Indeno(1,2,3-cd)pyrene ug/kg 16501670 99 50-130
Isophorone ug/kg 9721670 58 41-130
N-Nitroso-di-n-propylamine ug/kg 9231670 55 36-130
N-Nitrosodimethylamine ug/kg 8411670 50 34-130
N-Nitrosodiphenylamine ug/kg 13001670 78 48-130
Naphthalene ug/kg 8621670 52 46-130
Nitrobenzene ug/kg 8471670 51 39-130
Pentachlorophenol ug/kg 28103330 84 42-130
Phenanthrene ug/kg 13701670 82 50-130
Phenol ug/kg 9001670 54 42-130
Pyrene ug/kg 14501670 87 50-130
Pyridine ug/kg 7001670 42 26-130
2,4,6-Tribromophenol (S)%77 10-131
2-Fluorobiphenyl (S)%48 10-130
2-Fluorophenol (S)%44 10-130
Nitrobenzene-d5 (S)%47 10-130
Phenol-d6 (S)%47 10-130
Terphenyl-d14 (S)%82 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3999984MATRIX SPIKE SAMPLE:
MSSpike
Result
92662899005
1,2,4-Trichlorobenzene ug/kg 10602100 50 16-130ND
1,2-Dichlorobenzene ug/kg 10702100 51 19-130ND
1,3-Dichlorobenzene ug/kg 10402100 49 19-130ND
1,4-Dichlorobenzene ug/kg 10502100 50 20-130ND
1-Methylnaphthalene ug/kg 11502100 55 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 10102100 48 10-130ND
2,4,5-Trichlorophenol ug/kg 13002100 62 19-130ND
2,4,6-Trichlorophenol ug/kg 12902100 61 18-130ND
2,4-Dichlorophenol ug/kg 11402100 54 16-130ND
2,4-Dimethylphenol ug/kg 16302100 78 10-130ND
2,4-Dinitrophenol ug/kg 779010500 74 10-143ND
2,4-Dinitrotoluene ug/kg 14902100 71 19-130ND
2,6-Dinitrotoluene ug/kg 15102100 72 22-130ND
2-Chloronaphthalene ug/kg 11202100 53 18-130ND
2-Chlorophenol ug/kg 11002100 52 20-130ND
2-Methylnaphthalene ug/kg 11202100 53 18-130ND
2-Methylphenol(o-Cresol)ug/kg 11502100 55 13-130ND
2-Nitroaniline ug/kg 26604200 63 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 142 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3999984MATRIX SPIKE SAMPLE:
MSSpike
Result
92662899005
2-Nitrophenol ug/kg 12102100 58 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 11602100 55 13-130ND
3,3'-Dichlorobenzidine ug/kg 28404200 68 10-130ND
3-Nitroaniline ug/kg 26804200 64 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 33804200 80 10-144ND
4-Bromophenylphenyl ether ug/kg 13902100 66 18-130ND
4-Chloro-3-methylphenol ug/kg 25504200 61 16-130ND
4-Chloroaniline ug/kg 21204200 50 17-130ND
4-Chlorophenylphenyl ether ug/kg 13002100 62 17-130ND
4-Nitroaniline ug/kg 27704200 66 21-130ND
4-Nitrophenol ug/kg 703010500 67 13-131ND
Acenaphthene ug/kg 12702100 61 20-130ND
Acenaphthylene ug/kg 12702100 60 21-130ND
Aniline ug/kg 8142100 39 10-130ND
Anthracene ug/kg 13902100 66 19-130ND
Benzo(a)anthracene ug/kg 14702100 70 17-130ND
Benzo(a)pyrene ug/kg 16702100 79 14-130ND
Benzo(b)fluoranthene ug/kg 16502100 79 11-134ND
Benzo(g,h,i)perylene ug/kg 18302100 87 12-130ND
Benzo(k)fluoranthene ug/kg 16602100 79 15-130ND
Benzoic Acid ug/kg 459010500 44 10-130ND
Benzyl alcohol ug/kg 21304200 51 20-130ND
bis(2-Chloroethoxy)methane ug/kg 10502100 50 16-130ND
bis(2-Chloroethyl) ether ug/kg 10202100 48 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 15402100 73 11-130ND
Butylbenzylphthalate ug/kg 16002100 76 10-130ND
Chrysene ug/kg 14802100 70 17-130ND
Di-n-butylphthalate ug/kg 15002100 71 16-130ND
Di-n-octylphthalate ug/kg 15302100 73 16-130ND
Dibenz(a,h)anthracene ug/kg 17602100 84 13-130ND
Dibenzofuran ug/kg 12802100 61 19-130ND
Diethylphthalate ug/kg 14902100 71 22-130ND
Dimethylphthalate ug/kg 14502100 69 23-130ND
Fluoranthene ug/kg 14602100 70 14-130ND
Fluorene ug/kg 13802100 66 19-130ND
Hexachloro-1,3-butadiene ug/kg 10102100 48 12-130ND
Hexachlorobenzene ug/kg 14202100 67 17-130ND
Hexachlorocyclopentadiene ug/kg 9692100 46 10-130ND
Hexachloroethane ug/kg 10302100 49 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 18202100 87 13-130ND
Isophorone ug/kg 12202100 58 17-130ND
N-Nitroso-di-n-propylamine ug/kg 11502100 55 10-130ND
N-Nitrosodimethylamine ug/kg 10502100 50 16-130ND
N-Nitrosodiphenylamine ug/kg 14602100 70 19-130ND
Naphthalene ug/kg 11102100 53 18-130ND
Nitrobenzene ug/kg 10902100 52 15-130ND
Pentachlorophenol ug/kg 31204200 74 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3999984MATRIX SPIKE SAMPLE:
MSSpike
Result
92662899005
Phenanthrene ug/kg 15202100 72 17-130ND
Phenol ug/kg 11202100 53 15-130ND
Pyrene ug/kg 15702100 75 31-130ND
Pyridine ug/kg 6022100 29 10-130ND
2,4,6-Tribromophenol (S)%66 10-131
2-Fluorobiphenyl (S)%47 10-130
2-Fluorophenol (S)%45 10-130
Nitrobenzene-d5 (S)%47 10-130
Phenol-d6 (S)%45 10-130
Terphenyl-d14 (S)%69 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662945001
3999985SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662945001
3999985SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6364
2-Fluorobiphenyl (S)%5658
2-Fluorophenol (S)%5658
Nitrobenzene-d5 (S)%5962
Phenol-d6 (S)%5861
Terphenyl-d14 (S)%7366
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770548
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4000003
Associated Lab Samples:92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 326 04/27/23 15:36128
1,2-Dichlorobenzene ug/kg ND 326 04/27/23 15:36117
1,3-Dichlorobenzene ug/kg ND 326 04/27/23 15:36115
1,4-Dichlorobenzene ug/kg ND 326 04/27/23 15:36124
1-Methylnaphthalene ug/kg ND 326 04/27/23 15:36114
2,2'-Oxybis(1-chloropropane)ug/kg ND 326 04/27/23 15:36155
2,4,5-Trichlorophenol ug/kg ND 326 04/27/23 15:36149
2,4,6-Trichlorophenol ug/kg ND 326 04/27/23 15:36134
2,4-Dichlorophenol ug/kg ND 326 04/27/23 15:36127
2,4-Dimethylphenol ug/kg ND 326 04/27/23 15:36135
2,4-Dinitrophenol ug/kg ND 1630 04/27/23 15:361010
2,4-Dinitrotoluene ug/kg ND 326 04/27/23 15:36125
2,6-Dinitrotoluene ug/kg ND 326 04/27/23 15:36119
2-Chloronaphthalene ug/kg ND 326 04/27/23 15:36129
2-Chlorophenol ug/kg ND 326 04/27/23 15:36122
2-Methylnaphthalene ug/kg ND 326 04/27/23 15:36130
2-Methylphenol(o-Cresol)ug/kg ND 326 04/27/23 15:36133
2-Nitroaniline ug/kg ND 1630 04/27/23 15:36266
2-Nitrophenol ug/kg ND 326 04/27/23 15:36141
3&4-Methylphenol(m&p Cresol)ug/kg ND 326 04/27/23 15:36131
3,3'-Dichlorobenzidine ug/kg ND 651 04/27/23 15:36220
3-Nitroaniline ug/kg ND 1630 04/27/23 15:36256
4,6-Dinitro-2-methylphenol ug/kg ND 651 04/27/23 15:36304
4-Bromophenylphenyl ether ug/kg ND 326 04/27/23 15:36125
4-Chloro-3-methylphenol ug/kg ND 651 04/27/23 15:36229
4-Chloroaniline ug/kg ND 651 04/27/23 15:36256
4-Chlorophenylphenyl ether ug/kg ND 326 04/27/23 15:36121
4-Nitroaniline ug/kg ND 651 04/27/23 15:36248
4-Nitrophenol ug/kg ND 1630 04/27/23 15:36630
Acenaphthene ug/kg ND 326 04/27/23 15:36114
Acenaphthylene ug/kg ND 326 04/27/23 15:36114
Aniline ug/kg ND 326 04/27/23 15:36127
Anthracene ug/kg ND 326 04/27/23 15:36107
Benzo(a)anthracene ug/kg ND 326 04/27/23 15:36109
Benzo(a)pyrene ug/kg ND 326 04/27/23 15:36112
Benzo(b)fluoranthene ug/kg ND 326 04/27/23 15:36109
Benzo(g,h,i)perylene ug/kg ND 326 04/27/23 15:36126
Benzo(k)fluoranthene ug/kg ND 326 04/27/23 15:36114
Benzoic Acid ug/kg ND 1630 04/27/23 15:36700
Benzyl alcohol ug/kg ND 651 04/27/23 15:36247
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4000003
Associated Lab Samples:92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 326 04/27/23 15:36135
bis(2-Chloroethyl) ether ug/kg ND 326 04/27/23 15:36122
bis(2-Ethylhexyl)phthalate ug/kg ND 326 04/27/23 15:36126
Butylbenzylphthalate ug/kg ND 326 04/27/23 15:36137
Chrysene ug/kg ND 326 04/27/23 15:36118
Di-n-butylphthalate ug/kg ND 326 04/27/23 15:36110
Di-n-octylphthalate ug/kg ND 326 04/27/23 15:36128
Dibenz(a,h)anthracene ug/kg ND 326 04/27/23 15:36125
Dibenzofuran ug/kg ND 326 04/27/23 15:36117
Diethylphthalate ug/kg ND 326 04/27/23 15:36119
Dimethylphthalate ug/kg ND 326 04/27/23 15:36118
Fluoranthene ug/kg ND 326 04/27/23 15:36112
Fluorene ug/kg ND 326 04/27/23 15:36114
Hexachloro-1,3-butadiene ug/kg ND 326 04/27/23 15:36141
Hexachlorobenzene ug/kg ND 326 04/27/23 15:36127
Hexachlorocyclopentadiene ug/kg ND 326 04/27/23 15:36187
Hexachloroethane ug/kg ND 326 04/27/23 15:36124
Indeno(1,2,3-cd)pyrene ug/kg ND 326 04/27/23 15:36128
Isophorone ug/kg ND 326 04/27/23 15:36145
N-Nitroso-di-n-propylamine ug/kg ND 326 04/27/23 15:36122
N-Nitrosodimethylamine ug/kg ND 326 04/27/23 15:36110
N-Nitrosodiphenylamine ug/kg ND 326 04/27/23 15:36115
Naphthalene ug/kg ND 326 04/27/23 15:36111
Nitrobenzene ug/kg ND 326 04/27/23 15:36151
Pentachlorophenol ug/kg ND 651 04/27/23 15:36319
Phenanthrene ug/kg ND 326 04/27/23 15:36107
Phenol ug/kg ND 326 04/27/23 15:36145
Pyrene ug/kg ND 326 04/27/23 15:36132
Pyridine ug/kg ND 326 04/27/23 15:36103
2,4,6-Tribromophenol (S)%65 10-131 04/27/23 15:36
2-Fluorobiphenyl (S)%64 10-130 04/27/23 15:36
2-Fluorophenol (S)%65 10-130 04/27/23 15:36
Nitrobenzene-d5 (S)%69 10-130 04/27/23 15:36
Phenol-d6 (S)%70 10-130 04/27/23 15:36
Terphenyl-d14 (S)%77 10-130 04/27/23 15:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4000004LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 7391660 45 43-130
1,2-Dichlorobenzene ug/kg 7171660 43 43-130
1,3-Dichlorobenzene ug/kg 7101660 43 43-130
1,4-Dichlorobenzene ug/kg 722 L2166043 44-130
1-Methylnaphthalene ug/kg 8731660 53 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4000004LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 7041660 42 29-130
2,4,5-Trichlorophenol ug/kg 9881660 59 47-130
2,4,6-Trichlorophenol ug/kg 9781660 59 47-130
2,4-Dichlorophenol ug/kg 8421660 51 45-130
2,4-Dimethylphenol ug/kg 12101660 73 45-130
2,4-Dinitrophenol ug/kg 51808310 62 27-140
2,4-Dinitrotoluene ug/kg 11001660 66 46-130
2,6-Dinitrotoluene ug/kg 11301660 68 48-130
2-Chloronaphthalene ug/kg 8351660 50 46-130
2-Chlorophenol ug/kg 7641660 46 43-130
2-Methylnaphthalene ug/kg 8251660 50 47-130
2-Methylphenol(o-Cresol)ug/kg 8021660 48 42-130
2-Nitroaniline ug/kg 20303320 61 41-130
2-Nitrophenol ug/kg 8851660 53 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 8591660 52 39-130
3,3'-Dichlorobenzidine ug/kg 20403320 61 41-130
3-Nitroaniline ug/kg 19703320 59 37-130
4,6-Dinitro-2-methylphenol ug/kg 23403320 70 38-141
4-Bromophenylphenyl ether ug/kg 10801660 65 47-130
4-Chloro-3-methylphenol ug/kg 20703320 62 44-130
4-Chloroaniline ug/kg 16403320 49 41-130
4-Chlorophenylphenyl ether ug/kg 10301660 62 45-130
4-Nitroaniline ug/kg 19603320 59 42-130
4-Nitrophenol ug/kg 52108310 63 39-131
Acenaphthene ug/kg 9931660 60 49-130
Acenaphthylene ug/kg 9751660 59 50-130
Aniline ug/kg 6571660 40 38-130
Anthracene ug/kg 10401660 63 49-130
Benzo(a)anthracene ug/kg 11501660 69 51-130
Benzo(a)pyrene ug/kg 11801660 71 51-130
Benzo(b)fluoranthene ug/kg 11601660 70 49-130
Benzo(g,h,i)perylene ug/kg 12401660 75 48-140
Benzo(k)fluoranthene ug/kg 11501660 70 51-130
Benzoic Acid ug/kg 36808310 44 22-130
Benzyl alcohol ug/kg 16103320 49 43-130
bis(2-Chloroethoxy)methane ug/kg 7671660 46 43-130
bis(2-Chloroethyl) ether ug/kg 6991660 42 42-130
bis(2-Ethylhexyl)phthalate ug/kg 11601660 70 43-130
Butylbenzylphthalate ug/kg 11801660 71 44-131
Chrysene ug/kg 11601660 70 51-130
Di-n-butylphthalate ug/kg 11101660 67 46-130
Di-n-octylphthalate ug/kg 11701660 71 45-130
Dibenz(a,h)anthracene ug/kg 13301660 80 48-130
Dibenzofuran ug/kg 10001660 60 10-130
Diethylphthalate ug/kg 11001660 66 48-130
Dimethylphthalate ug/kg 10801660 65 48-130
Fluoranthene ug/kg 10801660 65 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4000004LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 10401660 63 48-130
Hexachloro-1,3-butadiene ug/kg 6791660 41 39-130
Hexachlorobenzene ug/kg 10501660 63 47-130
Hexachlorocyclopentadiene ug/kg 6041660 36 17-130
Hexachloroethane ug/kg 6961660 42 40-130
Indeno(1,2,3-cd)pyrene ug/kg 12401660 74 50-130
Isophorone ug/kg 9801660 59 41-130
N-Nitroso-di-n-propylamine ug/kg 8901660 54 36-130
N-Nitrosodimethylamine ug/kg 7571660 46 34-130
N-Nitrosodiphenylamine ug/kg 11001660 66 48-130
Naphthalene ug/kg 8001660 48 46-130
Nitrobenzene ug/kg 7691660 46 39-130
Pentachlorophenol ug/kg 21003320 63 42-130
Phenanthrene ug/kg 11401660 69 50-130
Phenol ug/kg 8061660 49 42-130
Pyrene ug/kg 11501660 69 50-130
Pyridine ug/kg 6491660 39 26-130
2,4,6-Tribromophenol (S)%57 10-131
2-Fluorobiphenyl (S)%44 10-130
2-Fluorophenol (S)%39 10-130
Nitrobenzene-d5 (S)%42 10-130
Phenol-d6 (S)%42 10-130
Terphenyl-d14 (S)%64 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4000005MATRIX SPIKE SAMPLE:
MSSpike
Result
92662497011
1,2,4-Trichlorobenzene ug/kg 9652130 45 16-130ND
1,2-Dichlorobenzene ug/kg 9122130 43 19-130ND
1,3-Dichlorobenzene ug/kg 8812130 41 19-130ND
1,4-Dichlorobenzene ug/kg 8842130 41 20-130ND
1-Methylnaphthalene ug/kg 10502130 49 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 7732130 36 10-130ND
2,4,5-Trichlorophenol ug/kg 11002130 52 19-130ND
2,4,6-Trichlorophenol ug/kg 11102130 52 18-130ND
2,4-Dichlorophenol ug/kg 10702130 50 16-130ND
2,4-Dimethylphenol ug/kg 11502130 54 10-130ND
2,4-Dinitrophenol ug/kg ND10700 12 10-143ND
2,4-Dinitrotoluene ug/kg 10502130 49 19-130ND
2,6-Dinitrotoluene ug/kg 10802130 51 22-130ND
2-Chloronaphthalene ug/kg 10602130 50 18-130ND
2-Chlorophenol ug/kg 9472130 44 20-130ND
2-Methylnaphthalene ug/kg 9992130 47 18-130ND
2-Methylphenol(o-Cresol)ug/kg 8962130 42 13-130ND
2-Nitroaniline ug/kg 2000J4270 47 18-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 149 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4000005MATRIX SPIKE SAMPLE:
MSSpike
Result
92662497011
2-Nitrophenol ug/kg 9582130 45 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 9132130 43 13-130ND
3,3'-Dichlorobenzidine ug/kg 16904270 40 10-130ND
3-Nitroaniline ug/kg 1980J4270 46 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 9414270 22 10-144ND
4-Bromophenylphenyl ether ug/kg 11202130 53 18-130ND
4-Chloro-3-methylphenol ug/kg 21004270 49 16-130ND
4-Chloroaniline ug/kg 17304270 40 17-130ND
4-Chlorophenylphenyl ether ug/kg 10602130 50 17-130ND
4-Nitroaniline ug/kg 19104270 45 21-130ND
4-Nitrophenol ug/kg 444010700 42 13-131ND
Acenaphthene ug/kg 10902130 51 20-130ND
Acenaphthylene ug/kg 11202130 52 21-130ND
Aniline ug/kg 6662130 31 10-130ND
Anthracene ug/kg 10702130 50 19-130ND
Benzo(a)anthracene ug/kg 11102130 49 17-130ND
Benzo(a)pyrene ug/kg 12002130 51 14-130ND
Benzo(b)fluoranthene ug/kg 12002130 50 11-134ND
Benzo(g,h,i)perylene ug/kg 13002130 57 12-130ND
Benzo(k)fluoranthene ug/kg 12502130 56 15-130ND
Benzoic Acid ug/kg ND M1107008 10-130ND
Benzyl alcohol ug/kg 17604270 41 20-130ND
bis(2-Chloroethoxy)methane ug/kg 8482130 40 16-130ND
bis(2-Chloroethyl) ether ug/kg 8102130 38 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 11002130 52 11-130ND
Butylbenzylphthalate ug/kg 11802130 55 10-130ND
Chrysene ug/kg 11402130 50 17-130ND
Di-n-butylphthalate ug/kg 10102130 47 16-130ND
Di-n-octylphthalate ug/kg 9552130 45 16-130ND
Dibenz(a,h)anthracene ug/kg 12402130 58 13-130ND
Dibenzofuran ug/kg 11102130 52 19-130ND
Diethylphthalate ug/kg 10202130 48 22-130ND
Dimethylphthalate ug/kg 10202130 48 23-130ND
Fluoranthene ug/kg 10202130 44 14-130ND
Fluorene ug/kg 11002130 52 19-130ND
Hexachloro-1,3-butadiene ug/kg 9192130 43 12-130ND
Hexachlorobenzene ug/kg 11202130 53 17-130ND
Hexachlorocyclopentadiene ug/kg 420J2130 20 10-130ND
Hexachloroethane ug/kg 8362130 39 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 13002130 58 13-130ND
Isophorone ug/kg 9022130 42 17-130ND
N-Nitroso-di-n-propylamine ug/kg 8692130 41 10-130ND
N-Nitrosodimethylamine ug/kg 8112130 38 16-130ND
N-Nitrosodiphenylamine ug/kg 11402130 53 19-130ND
Naphthalene ug/kg 9742130 46 18-130ND
Nitrobenzene ug/kg 9022130 42 15-130ND
Pentachlorophenol ug/kg 16804270 39 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4000005MATRIX SPIKE SAMPLE:
MSSpike
Result
92662497011
Phenanthrene ug/kg 11502130 52 17-130ND
Phenol ug/kg 9732130 46 15-130ND
Pyrene ug/kg 13702130 59 31-130ND
Pyridine ug/kg 7762130 36 10-130ND
2,4,6-Tribromophenol (S)%45 10-131
2-Fluorobiphenyl (S)%43 10-130
2-Fluorophenol (S)%36 10-130
Nitrobenzene-d5 (S)%38 10-130
Phenol-d6 (S)%37 10-130
Terphenyl-d14 (S)%55 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662497013
4000006SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30143J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662497013
4000006SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg 174J 30380
Benzo(a)anthracene ug/kg 595 D653301020
Benzo(a)pyrene ug/kg 685 D63630987
Benzo(b)fluoranthene ug/kg 935 D636301350
Benzo(g,h,i)perylene ug/kg 563 28 30743
Benzo(k)fluoranthene ug/kg 369J 301420
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg 718 D643301110
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30199J
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 1140 D651301930
Fluorene ug/kg ND 30136J
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg 498 30 30674
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30131J
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg 916 D666301820
Phenol ug/kg ND 30ND
Pyrene ug/kg 1240 D656302200
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6962
2-Fluorobiphenyl (S)%6663
2-Fluorophenol (S)%4545
Nitrobenzene-d5 (S)%6057
Phenol-d6 (S)%4847
Terphenyl-d14 (S)%7774
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769680
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663521005
3996202SAMPLE DUPLICATE:
Percent Moisture %12.9 N2152514.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663577003
3996203SAMPLE DUPLICATE:
Percent Moisture %18.0 N2232514.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2049689
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3918599-1
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008
Matrix: Solid
AnalyzedMDL
Total Solids %0.00100 04/27/23 16:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3918599-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1608802-46
R3918599-3SAMPLE DUPLICATE:
Total Solids %91.1 0.833 1091.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2049735
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples: 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3918602-1
Associated Lab Samples:92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
Total Solids %0.00300 04/27/23 17:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3918602-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594009
R3918602-3SAMPLE DUPLICATE:
Total Solids %81.2 3.01 1078.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 155 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2049527
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3919549-1
Associated Lab Samples: 92663594001, 92663594002, 92663594003, 92663594004, 92663594005, 92663594006, 92663594007,
92663594008, 92663594009, 92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 05/01/23 12:020.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3919549-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.4510.0 94.5 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3919549-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1608457-02
R3919549-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 20.0 99.0 75.0-125104 4.49 2020.0ND 19.8 20.7
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3919549-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1608457-02
Chromium, Hexavalent mg/kg 688641 107 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1608272-100
R3919549-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 1.31 R1148208.72
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92663594005
R3919549-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 1.95 19.3 202.37
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 156 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
770563
SM 4500-CN-E-2011
SM 4500-CN-E-2011
4500CNE Cyanide, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92663594001, 92663594007, 92663594008, 92663594009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4000119
Associated Lab Samples:92663594001, 92663594007, 92663594008, 92663594009
Matrix: Solid
AnalyzedMDL
Cyanide mg/kg ND 0.30 04/27/23 19:120.15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4000120LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 2.92.9 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4000121MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663594001
4000122
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg R12.9 91 80-12096 18 103.30.16J 2.8 3.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 157 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
771487
SM 4500-CN-E-2011
SM 4500-CN-E-2011
4500CNE Cyanide, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92663594010, 92663594019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4004652
Associated Lab Samples:92663594010, 92663594019
Matrix: Solid
AnalyzedMDL
Cyanide mg/kg ND 0.26 05/01/23 15:430.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4004653LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/kg 2.62.6 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4004654MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92664567001
4004655
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/kg M1,R133280-12069 27 1032.6 3.6 4.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 158 of 169
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663594
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769952
SM 4500-CN-E-2011
SM 4500-CN-E-2011
4500CNE Cyanide, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92663594017, 92663594018, 92663594020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3997191
Associated Lab Samples:92663594017, 92663594018, 92663594020
Matrix: Water
AnalyzedMDL
Cyanide mg/L ND 0.0080 04/24/23 19:440.0060
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3997192LABORATORY CONTROL SAMPLE:
LCSSpike
Cyanide mg/L 0.100.1 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3997193MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663628002
3997194
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L 0.1 91 80-12089 2 100.1ND 0.095 0.093
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3997195MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663480001
3997196
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Cyanide mg/L M1,R10.1 57 80-12072 20 100.10.011 0.068 0.083
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 159 of 169
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92663594
H&A-002
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Result may be biased high due to carryover from previously analyzed sample.C8
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Analyte concentration exceeded the calibration range. The reported result is estimated.E
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 160 of 169
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92663594
H&A-002
ANALYTE QUALIFIERS
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 169
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663594001 879481 879576BF-SB-1 EPA 3015A EPA 6010D
92663594005 879481 879576BF-SB-5 EPA 3015A EPA 6010D
92663594011 769799 769813BF-TMW-1 EPA 3010A EPA 6020B
92663594012 769799 769813BF-TMW-2 EPA 3010A EPA 6020B
92663594013 769799 769813BF-TMW-3 EPA 3010A EPA 6020B
92663594014 769799 769813BF-TMW-4 EPA 3010A EPA 6020B
92663594015 769799 769813BF-TMW-5 EPA 3010A EPA 6020B
92663594016 769799 769813BF-TMW-6 EPA 3010A EPA 6020B
92663594017 769799 769813BF-TMW-7 EPA 3010A EPA 6020B
92663594018 769799 769813BF-TMW-8 EPA 3010A EPA 6020B
92663594020 769799 769813BF-GW-DUP EPA 3010A EPA 6020B
92663594001 877600 877943BF-SB-1 EPA 3050B EPA 6020B
92663594002 877600 877943BF-SB-2 EPA 3050B EPA 6020B
92663594003 877600 877943BF-SB-3 EPA 3050B EPA 6020B
92663594004 877600 877943BF-SB-4 EPA 3050B EPA 6020B
92663594005 877600 877943BF-SB-5 EPA 3050B EPA 6020B
92663594006 877600 877943BF-SB-6 EPA 3050B EPA 6020B
92663594007 877600 877943BF-SB-7 EPA 3050B EPA 6020B
92663594008 877600 877943BF-SB-8 EPA 3050B EPA 6020B
92663594009 877600 877943BF-SB-9 EPA 3050B EPA 6020B
92663594010 877600 877943BF-SB-11 EPA 3050B EPA 6020B
92663594019 877600 877943BF-SB-DUP EPA 3050B EPA 6020B
92663594011 770880 771045BF-TMW-1 EPA 7470A EPA 7470A
92663594012 770880 771045BF-TMW-2 EPA 7470A EPA 7470A
92663594013 770880 771045BF-TMW-3 EPA 7470A EPA 7470A
92663594014 770880 771045BF-TMW-4 EPA 7470A EPA 7470A
92663594015 770880 771045BF-TMW-5 EPA 7470A EPA 7470A
92663594016 770880 771045BF-TMW-6 EPA 7470A EPA 7470A
92663594017 770883 771043BF-TMW-7 EPA 7470A EPA 7470A
92663594018 770883 771043BF-TMW-8 EPA 7470A EPA 7470A
92663594020 770883 771043BF-GW-DUP EPA 7470A EPA 7470A
92663594001 877601 877741BF-SB-1 EPA 7471B EPA 7471B
92663594002 877601 877741BF-SB-2 EPA 7471B EPA 7471B
92663594003 877601 877741BF-SB-3 EPA 7471B EPA 7471B
92663594004 877601 877741BF-SB-4 EPA 7471B EPA 7471B
92663594005 877601 877741BF-SB-5 EPA 7471B EPA 7471B
92663594006 877601 877741BF-SB-6 EPA 7471B EPA 7471B
92663594007 877601 877741BF-SB-7 EPA 7471B EPA 7471B
92663594008 877601 877741BF-SB-8 EPA 7471B EPA 7471B
92663594009 877601 877741BF-SB-9 EPA 7471B EPA 7471B
92663594010 877601 877741BF-SB-11 EPA 7471B EPA 7471B
92663594019 877601 877741BF-SB-DUP EPA 7471B EPA 7471B
92663594011 770122 770421BF-TMW-1 EPA 3510C EPA 8270E
92663594012 770122 770421BF-TMW-2 EPA 3510C EPA 8270E
92663594013 770122 770421BF-TMW-3 EPA 3510C EPA 8270E
92663594014 770122 770421BF-TMW-4 EPA 3510C EPA 8270E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 162 of 169
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663594015 770122 770421BF-TMW-5 EPA 3510C EPA 8270E
92663594016 770122 770421BF-TMW-6 EPA 3510C EPA 8270E
92663594017 769745 769790BF-TMW-7 EPA 3510C EPA 8270E
92663594018 770122 770421BF-TMW-8 EPA 3510C EPA 8270E
92663594020 769745 769790BF-GW-DUP EPA 3510C EPA 8270E
92663594001 770544 770746BF-SB-1 EPA 3546 EPA 8270E
92663594002 770544 770746BF-SB-2 EPA 3546 EPA 8270E
92663594003 770544 770746BF-SB-3 EPA 3546 EPA 8270E
92663594004 770544 770746BF-SB-4 EPA 3546 EPA 8270E
92663594005 770544 770746BF-SB-5 EPA 3546 EPA 8270E
92663594006 770544 770746BF-SB-6 EPA 3546 EPA 8270E
92663594007 770544 770746BF-SB-7 EPA 3546 EPA 8270E
92663594008 770548 770784BF-SB-8 EPA 3546 EPA 8270E
92663594009 770548 770784BF-SB-9 EPA 3546 EPA 8270E
92663594010 770548 770784BF-SB-11 EPA 3546 EPA 8270E
92663594019 770548 770784BF-SB-DUP EPA 3546 EPA 8270E
92663594001 770278 770390BF-SB-1 EPA 5035A/5030B EPA 8260D
92663594002 770278 770390BF-SB-2 EPA 5035A/5030B EPA 8260D
92663594003 770278 770390BF-SB-3 EPA 5035A/5030B EPA 8260D
92663594004 770278 770390BF-SB-4 EPA 5035A/5030B EPA 8260D
92663594005 770278 770390BF-SB-5 EPA 5035A/5030B EPA 8260D
92663594006 770278 770390BF-SB-6 EPA 5035A/5030B EPA 8260D
92663594007 770278 770390BF-SB-7 EPA 5035A/5030B EPA 8260D
92663594008 770278 770390BF-SB-8 EPA 5035A/5030B EPA 8260D
92663594009 770278 770390BF-SB-9 EPA 5035A/5030B EPA 8260D
92663594010 770278 770390BF-SB-11 EPA 5035A/5030B EPA 8260D
92663594019 770278 770390BF-SB-DUP EPA 5035A/5030B EPA 8260D
92663594011 770365BF-TMW-1 EPA 8260D
92663594012 770365BF-TMW-2 EPA 8260D
92663594013 770981BF-TMW-3 EPA 8260D
92663594014 770981BF-TMW-4 EPA 8260D
92663594015 770981BF-TMW-5 EPA 8260D
92663594016 770981BF-TMW-6 EPA 8260D
92663594017 770981BF-TMW-7 EPA 8260D
92663594018 770981BF-TMW-8 EPA 8260D
92663594020 770981BF-GW-DUP EPA 8260D
92663594022 770981TRIP BLANK EPA 8260D
92663594001 769680BF-SB-1 SW-846
92663594002 769680BF-SB-2 SW-846
92663594003 769680BF-SB-3 SW-846
92663594004 769680BF-SB-4 SW-846
92663594005 769680BF-SB-5 SW-846
92663594006 769680BF-SB-6 SW-846
92663594007 769680BF-SB-7 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 163 of 169
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663594
H&A-002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663594008 769680BF-SB-8 SW-846
92663594009 769680BF-SB-9 SW-846
92663594010 769680BF-SB-11 SW-846
92663594019 769680BF-SB-DUP SW-846
92663594001 2049689 2049689BF-SB-1 SM 2540 G SM 2540G
92663594002 2049689 2049689BF-SB-2 SM 2540 G SM 2540G
92663594003 2049689 2049689BF-SB-3 SM 2540 G SM 2540G
92663594004 2049689 2049689BF-SB-4 SM 2540 G SM 2540G
92663594005 2049689 2049689BF-SB-5 SM 2540 G SM 2540G
92663594006 2049689 2049689BF-SB-6 SM 2540 G SM 2540G
92663594007 2049689 2049689BF-SB-7 SM 2540 G SM 2540G
92663594008 2049689 2049689BF-SB-8 SM 2540 G SM 2540G
92663594009 2049735 2049735BF-SB-9 SM 2540 G SM 2540G
92663594010 2049735 2049735BF-SB-11 SM 2540 G SM 2540G
92663594019 2049735 2049735BF-SB-DUP SM 2540 G SM 2540G
92663594001 2049527 2049527BF-SB-1 3060A EPA 7199
92663594002 2049527 2049527BF-SB-2 3060A EPA 7199
92663594003 2049527 2049527BF-SB-3 3060A EPA 7199
92663594004 2049527 2049527BF-SB-4 3060A EPA 7199
92663594005 2049527 2049527BF-SB-5 3060A EPA 7199
92663594006 2049527 2049527BF-SB-6 3060A EPA 7199
92663594007 2049527 2049527BF-SB-7 3060A EPA 7199
92663594008 2049527 2049527BF-SB-8 3060A EPA 7199
92663594009 2049527 2049527BF-SB-9 3060A EPA 7199
92663594010 2049527 2049527BF-SB-11 3060A EPA 7199
92663594019 2049527 2049527BF-SB-DUP 3060A EPA 7199
92663594001 770563 770666BF-SB-1 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594007 770563 770666BF-SB-7 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594008 770563 770666BF-SB-8 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594009 770563 770666BF-SB-9 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594010 771487 771570BF-SB-11 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594019 771487 771570BF-SB-DUP SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594017 769952 770037BF-TMW-7 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594018 769952 770037BF-TMW-8 SM 4500-CN-E-2011 SM 4500-CN-E-2011
92663594020 769952 770037BF-GW-DUP SM 4500-CN-E-2011 SM 4500-CN-E-2011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/15/2023 04:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 164 of 169
Page 165 of 169
Page 166 of 169
Page 167 of 169
Page 168 of 169
Page 169 of 169

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/9/2023
Hart & Hickman (Charlotte) Loryn Smith
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-114-0003 Client Project Description: H&A-002
Dear Loryn Smith:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/24/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 68
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-114-0003
Page 2 of 68
Report Number:
Sample Summary Table
Client Project Description:
23-114-0003
H&A-002
Lab No Client Sample ID Matrix Date Collected Date Received
04/20/2023Air 94707 BF-SSV-DUP 04/24/2023 10:40
04/20/2023 16:13Air 94708 BF-SSV-8 04/24/2023 10:40
04/18/2023 09:25Air 94709 BF-SSV-3 04/24/2023 10:40
04/20/2023 16:33Air 94710 BF-SSV-7 04/24/2023 10:40
04/17/2023 16:55Air 94711 BF-SSV-1 04/24/2023 10:40
04/17/2023 15:50Air 94712 BF-SSV-10 04/24/2023 10:40
04/18/2023 08:55Air 94713 BF-SSV-2 04/24/2023 10:40
04/17/2023 16:27Air 94714 BF-SSV-5 04/24/2023 10:40
04/17/2023 15:00Air 94715 BF-SSV-9 04/24/2023 10:40
04/17/2023 15:20Air 94716 BF-SSV-6 04/24/2023 10:40
04/17/2023 14:00Air 94717 BF-SSV-11 04/24/2023 10:40
04/18/2023 11:00Air 94718 BF-SSV-4 04/24/2023 10:40
Page 3 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94707BF-SSV-DUP
29.1 05/04/2023 22:53TO-15 Acetone µg/m3 0.202
J0.351 05/04/2023 22:53TO-15 Benzene µg/m3 0.073
J0.607 05/04/2023 22:53TO-15 Carbon Disulfide µg/m3 0.060
2.69 05/04/2023 22:53TO-15 Dichlorodifluoromethane µg/m3 0.134
4.55 05/04/2023 22:53TO-15 4-Ethyltoluene µg/m3 0.128
J0.260 05/04/2023 22:53TO-15 n-Hexane µg/m3 0.047
J0.679 05/04/2023 22:53TO-15 2-Hexanone µg/m3 0.285
B11.2 05/04/2023 22:53TO-15 Isopropyl Alcohol µg/m3 0.139
18.8 05/04/2023 22:53TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.630 05/04/2023 22:53TO-15 4-Methyl-2-Pentanone µg/m3 0.121
2.57 05/04/2023 22:53TO-15 Methylene Chloride µg/m3 0.488
4.83 05/04/2023 22:53TO-15 Naphthalene µg/m3 0.183
J0.827 05/04/2023 22:53TO-15 Tetrachloroethene µg/m3 0.181
20.1 05/04/2023 22:53TO-15 Tetrahydrofuran µg/m3 0.107
J1.41 05/04/2023 22:53TO-15 Toluene µg/m3 0.090
J1.58 05/04/2023 22:53TO-15 Trichlorofluoromethane µg/m3 0.130
5.11 05/04/2023 22:53TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.503 05/04/2023 22:53TO-15 o-Xylene µg/m3 0.157
J5.38 05/04/2023 22:53TO-15 m,p-Xylene µg/m3 0.217
J5.88 05/04/2023 22:53TO-15 Xylene (Total)µg/m3 0.157
V 94708BF-SSV-8
30.0 05/04/2023 23:58TO-15 Acetone µg/m3 0.202
J0.360 05/04/2023 23:58TO-15 Benzene µg/m3 0.073
J0.632 05/04/2023 23:58TO-15 Carbon Disulfide µg/m3 0.060
2.75 05/04/2023 23:58TO-15 Dichlorodifluoromethane µg/m3 0.134
4.56 05/04/2023 23:58TO-15 4-Ethyltoluene µg/m3 0.128
J0.285 05/04/2023 23:58TO-15 n-Hexane µg/m3 0.047
J0.688 05/04/2023 23:58TO-15 2-Hexanone µg/m3 0.285
B11.1 05/04/2023 23:58TO-15 Isopropyl Alcohol µg/m3 0.139
18.8 05/04/2023 23:58TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.696 05/04/2023 23:58TO-15 4-Methyl-2-Pentanone µg/m3 0.121
2.75 05/04/2023 23:58TO-15 Methylene Chloride µg/m3 0.488
4.80 05/04/2023 23:58TO-15 Naphthalene µg/m3 0.183
J0.827 05/04/2023 23:58TO-15 Tetrachloroethene µg/m3 0.181
20.0 05/04/2023 23:58TO-15 Tetrahydrofuran µg/m3 0.107
J1.45 05/04/2023 23:58TO-15 Toluene µg/m3 0.090
Page 4 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94708BF-SSV-8
J1.69 05/04/2023 23:58TO-15 Trichlorofluoromethane µg/m3 0.130
5.18 05/04/2023 23:58TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.503 05/04/2023 23:58TO-15 o-Xylene µg/m3 0.157
J5.45 05/04/2023 23:58TO-15 m,p-Xylene µg/m3 0.217
J5.95 05/04/2023 23:58TO-15 Xylene (Total)µg/m3 0.157
V 94709BF-SSV-3
18.5 05/05/2023 00:49TO-15 Acetone µg/m3 0.202
J0.964 05/05/2023 00:49TO-15 Benzene µg/m3 0.073
J5.09 05/05/2023 00:49TO-15 Carbon Disulfide µg/m3 0.060
J0.580 05/05/2023 00:49TO-15 Chloroform µg/m3 0.086
2.62 05/05/2023 00:49TO-15 Dichlorodifluoromethane µg/m3 0.134
4.50 05/05/2023 00:49TO-15 4-Ethyltoluene µg/m3 0.128
J0.285 05/05/2023 00:49TO-15 n-Hexane µg/m3 0.047
B4.98 05/05/2023 00:49TO-15 Isopropyl Alcohol µg/m3 0.139
2.23 05/05/2023 00:49TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.421 05/05/2023 00:49TO-15 4-Methyl-2-Pentanone µg/m3 0.121
9.86 05/05/2023 00:49TO-15 Methylene Chloride µg/m3 0.488
J0.624 05/05/2023 00:49TO-15 Tetrachloroethene µg/m3 0.181
J0.377 05/05/2023 00:49TO-15 Tetrahydrofuran µg/m3 0.107
J0.795 05/05/2023 00:49TO-15 Toluene µg/m3 0.090
J1.69 05/05/2023 00:49TO-15 Trichlorofluoromethane µg/m3 0.130
5.11 05/05/2023 00:49TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.712 05/05/2023 00:49TO-15 o-Xylene µg/m3 0.157
5.65 05/05/2023 00:49TO-15 m,p-Xylene µg/m3 0.217
J6.36 05/05/2023 00:49TO-15 Xylene (Total)µg/m3 0.157
V 94710BF-SSV-7
71.1 05/05/2023 01:42TO-15 Acetone µg/m3 0.202
J0.606 05/05/2023 01:42TO-15 Benzene µg/m3 0.073
J0.999 05/05/2023 01:42TO-15 Carbon Disulfide µg/m3 0.060
J0.507 05/05/2023 01:42TO-15 Chloroform µg/m3 0.086
2.68 05/05/2023 01:42TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.673 05/05/2023 01:42TO-15 1,4-Dioxane µg/m3 0.435
J0.668 05/05/2023 01:42TO-15 Ethylbenzene µg/m3 0.106
4.67 05/05/2023 01:42TO-15 4-Ethyltoluene µg/m3 0.128
J1.07 05/05/2023 01:42TO-15 Heptane µg/m3 0.143
J0.877 05/05/2023 01:42TO-15 n-Hexane µg/m3 0.047
Page 5 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94710BF-SSV-7
B22.7 05/05/2023 01:42TO-15 Isopropyl Alcohol µg/m3 0.139
2.83 05/05/2023 01:42TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.507 05/05/2023 01:42TO-15 4-Methyl-2-Pentanone µg/m3 0.121
9.69 05/05/2023 01:42TO-15 Methylene Chloride µg/m3 0.488
4.79 05/05/2023 01:42TO-15 Naphthalene µg/m3 0.183
2.77 05/05/2023 01:42TO-15 Propene µg/m3 0.242
J3.22 05/05/2023 01:42TO-15 Tetrachloroethene µg/m3 0.181
J1.33 05/05/2023 01:42TO-15 Tetrahydrofuran µg/m3 0.107
3.32 05/05/2023 01:42TO-15 Toluene µg/m3 0.090
2.25 05/05/2023 01:42TO-15 Trichloroethene µg/m3 0.199
J1.93 05/05/2023 01:42TO-15 Trichlorofluoromethane µg/m3 0.130
5.48 05/05/2023 01:42TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J1.61 05/05/2023 01:42TO-15 o-Xylene µg/m3 0.157
7.22 05/05/2023 01:42TO-15 m,p-Xylene µg/m3 0.217
J8.83 05/05/2023 01:42TO-15 Xylene (Total)µg/m3 0.157
V 94711BF-SSV-1
12.8 05/05/2023 02:45TO-15 Acetone µg/m3 0.202
J0.450 05/05/2023 02:45TO-15 Benzene µg/m3 0.073
J2.85 05/05/2023 02:45TO-15 Carbon Disulfide µg/m3 0.060
J1.90 05/05/2023 02:45TO-15 Chloroform µg/m3 0.086
2.87 05/05/2023 02:45TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.377 05/05/2023 02:45TO-15 n-Hexane µg/m3 0.047
B5.05 05/05/2023 02:45TO-15 Isopropyl Alcohol µg/m3 0.139
J1.35 05/05/2023 02:45TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
11.7 05/05/2023 02:45TO-15 Methylene Chloride µg/m3 0.488
4.83 05/05/2023 02:45TO-15 Naphthalene µg/m3 0.183
31.3 05/05/2023 02:45TO-15 Tetrachloroethene µg/m3 0.181
J0.238 05/05/2023 02:45TO-15 Tetrahydrofuran µg/m3 0.107
J1.00 05/05/2023 02:45TO-15 Toluene µg/m3 0.090
9.43 05/05/2023 02:45TO-15 Trichloroethene µg/m3 0.199
J2.37 05/05/2023 02:45TO-15 Trichlorofluoromethane µg/m3 0.130
J4.89 05/05/2023 02:45TO-15 m,p-Xylene µg/m3 0.217
J4.89 05/05/2023 02:45TO-15 Xylene (Total)µg/m3 0.157
V 94712BF-SSV-10
23.9 05/05/2023 03:36TO-15 Acetone µg/m3 0.202
J0.383 05/05/2023 03:36TO-15 Benzene µg/m3 0.073
Page 6 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94712BF-SSV-10
J1.13 05/05/2023 03:36TO-15 Carbon Disulfide µg/m3 0.060
J1.35 05/05/2023 03:36TO-15 Chloroform µg/m3 0.086
40.2 05/05/2023 03:36TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.536 05/05/2023 03:36TO-15 Heptane µg/m3 0.143
J0.440 05/05/2023 03:36TO-15 n-Hexane µg/m3 0.047
B15.6 05/05/2023 03:36TO-15 Isopropyl Alcohol µg/m3 0.139
2.74 05/05/2023 03:36TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
2.83 05/05/2023 03:36TO-15 4-Methyl-2-Pentanone µg/m3 0.121
5.94 05/05/2023 03:36TO-15 Methylene Chloride µg/m3 0.488
5.67 05/05/2023 03:36TO-15 Tetrachloroethene µg/m3 0.181
J0.867 05/05/2023 03:36TO-15 Tetrahydrofuran µg/m3 0.107
J0.904 05/05/2023 03:36TO-15 Toluene µg/m3 0.090
J1.69 05/05/2023 03:36TO-15 Trichlorofluoromethane µg/m3 0.130
J4.90 05/05/2023 03:36TO-15 m,p-Xylene µg/m3 0.217
J4.90 05/05/2023 03:36TO-15 Xylene (Total)µg/m3 0.157
V 94713BF-SSV-2
B7.48 05/05/2023 04:29TO-15 Acetone µg/m3 0.202
J0.268 05/05/2023 04:29TO-15 Benzene µg/m3 0.073
J0.333 05/05/2023 04:29TO-15 Carbon Disulfide µg/m3 0.060
2.75 05/05/2023 04:29TO-15 Dichlorodifluoromethane µg/m3 0.134
4.59 05/05/2023 04:29TO-15 4-Ethyltoluene µg/m3 0.128
JB3.62 05/05/2023 04:29TO-15 Isopropyl Alcohol µg/m3 0.139
3.05 05/05/2023 04:29TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
3.70 05/05/2023 04:29TO-15 Methylene Chloride µg/m3 0.488
5.59 05/05/2023 04:29TO-15 Naphthalene µg/m3 0.183
J0.488 05/05/2023 04:29TO-15 Tetrachloroethene µg/m3 0.181
J0.990 05/05/2023 04:29TO-15 Tetrahydrofuran µg/m3 0.107
J0.388 05/05/2023 04:29TO-15 Toluene µg/m3 0.090
J1.60 05/05/2023 04:29TO-15 Trichlorofluoromethane µg/m3 0.130
6.33 05/05/2023 04:29TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.550 05/05/2023 04:29TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
V 94714BF-SSV-5
13.1 05/05/2023 05:22TO-15 Acetone µg/m3 0.202
J0.482 05/05/2023 05:22TO-15 Benzene µg/m3 0.073
J2.41 05/05/2023 05:22TO-15 Cyclohexane µg/m3 0.161
2.59 05/05/2023 05:22TO-15 Dichlorodifluoromethane µg/m3 0.134
Page 7 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94714BF-SSV-5
J0.295 05/05/2023 05:22TO-15 Heptane µg/m3 0.143
J0.345 05/05/2023 05:22TO-15 n-Hexane µg/m3 0.047
JB4.20 05/05/2023 05:22TO-15 Isopropyl Alcohol µg/m3 0.139
J1.42 05/05/2023 05:22TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
13.3 05/05/2023 05:22TO-15 Methylene Chloride µg/m3 0.488
4.93 05/05/2023 05:22TO-15 Naphthalene µg/m3 0.183
J0.820 05/05/2023 05:22TO-15 Tetrachloroethene µg/m3 0.181
J1.39 05/05/2023 05:22TO-15 Toluene µg/m3 0.090
J1.56 05/05/2023 05:22TO-15 Trichlorofluoromethane µg/m3 0.130
4.96 05/05/2023 05:22TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J5.03 05/05/2023 05:22TO-15 m,p-Xylene µg/m3 0.217
J5.03 05/05/2023 05:22TO-15 Xylene (Total)µg/m3 0.157
V 94715BF-SSV-9
44.8 05/05/2023 06:15TO-15 Acetone µg/m3 0.202
J0.415 05/05/2023 06:15TO-15 Benzene µg/m3 0.073
J5.01 05/05/2023 06:15TO-15 Carbon Disulfide µg/m3 0.060
J0.795 05/05/2023 06:15TO-15 Chloroform µg/m3 0.086
J2.02 05/05/2023 06:15TO-15 Cyclohexane µg/m3 0.161
J2.43 05/05/2023 06:15TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.493 05/05/2023 06:15TO-15 1,4-Dioxane µg/m3 0.435
8.18 05/05/2023 06:15TO-15 4-Ethyltoluene µg/m3 0.128
J0.381 05/05/2023 06:15TO-15 Heptane µg/m3 0.143
J0.807 05/05/2023 06:15TO-15 n-Hexane µg/m3 0.047
B16.2 05/05/2023 06:15TO-15 Isopropyl Alcohol µg/m3 0.139
4.68 05/05/2023 06:15TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J1.32 05/05/2023 06:15TO-15 4-Methyl-2-Pentanone µg/m3 0.121
8.45 05/05/2023 06:15TO-15 Methylene Chloride µg/m3 0.488
4.79 05/05/2023 06:15TO-15 Naphthalene µg/m3 0.183
5.47 05/05/2023 06:15TO-15 Styrene µg/m3 0.124
J1.08 05/05/2023 06:15TO-15 Tetrachloroethene µg/m3 0.181
1.99 05/05/2023 06:15TO-15 Tetrahydrofuran µg/m3 0.107
J1.63 05/05/2023 06:15TO-15 Toluene µg/m3 0.090
J1.42 05/05/2023 06:15TO-15 Trichlorofluoromethane µg/m3 0.130
14.6 05/05/2023 06:15TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
3.11 05/05/2023 06:15TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
J1.54 05/05/2023 06:15TO-15 o-Xylene µg/m3 0.157
Page 8 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94715BF-SSV-9
J5.35 05/05/2023 06:15TO-15 m,p-Xylene µg/m3 0.217
J6.89 05/05/2023 06:15TO-15 Xylene (Total)µg/m3 0.157
V 94716BF-SSV-6
13.8 05/09/2023 14:18TO-15 Acetone µg/m3 0.202
J0.396 05/09/2023 14:18TO-15 Benzene µg/m3 0.073
JB0.479 05/09/2023 14:18TO-15 Carbon Disulfide µg/m3 0.060
J0.585 05/09/2023 14:18TO-15 Chloroform µg/m3 0.086
2.77 05/09/2023 14:18TO-15 Dichlorodifluoromethane µg/m3 0.134
5.59 05/09/2023 14:18TO-15 4-Ethyltoluene µg/m3 0.128
J0.467 05/09/2023 14:18TO-15 Heptane µg/m3 0.143
J0.296 05/09/2023 14:18TO-15 n-Hexane µg/m3 0.047
B5.50 05/09/2023 14:18TO-15 Isopropyl Alcohol µg/m3 0.139
1.56 05/09/2023 14:18TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
18.7 05/09/2023 14:18TO-15 Methylene Chloride µg/m3 0.488
19.6 05/09/2023 14:18TO-15 Tetrachloroethene µg/m3 0.181
J0.669 05/09/2023 14:18TO-15 Tetrahydrofuran µg/m3 0.107
J1.25 05/09/2023 14:18TO-15 Toluene µg/m3 0.090
8.38 05/09/2023 14:18TO-15 Trichloroethene µg/m3 0.199
J1.93 05/09/2023 14:18TO-15 Trichlorofluoromethane µg/m3 0.130
7.20 05/09/2023 14:18TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
J0.619 05/09/2023 14:18TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
J0.655 05/09/2023 14:18TO-15 o-Xylene µg/m3 0.157
J4.98 05/09/2023 14:18TO-15 m,p-Xylene µg/m3 0.217
J5.64 05/09/2023 14:18TO-15 Xylene (Total)µg/m3 0.157
V 94717BF-SSV-11
36.3 05/05/2023 17:30TO-15 Acetone µg/m3 0.202
5.67 05/05/2023 17:30TO-15 Benzene µg/m3 0.073
J1.10 05/05/2023 17:30TO-15 Carbon Disulfide µg/m3 0.060
2.71 05/05/2023 17:30TO-15 Chlorobenzene µg/m3 0.107
J1.47 05/05/2023 17:30TO-15 Chloroform µg/m3 0.086
J0.774 05/05/2023 17:30TO-15 Chloromethane µg/m3 0.067
J2.44 05/05/2023 17:30TO-15 Cyclohexane µg/m3 0.161
J0.841 05/05/2023 17:30TO-15 1,2-Dichlorobenzene µg/m3 0.096
J1.95 05/05/2023 17:30TO-15 1,4-Dichlorobenzene µg/m3 0.186
3.56 05/05/2023 17:30TO-15 Dichlorodifluoromethane µg/m3 0.134
5.69 05/05/2023 17:30TO-15 Ethyl Acetate µg/m3 0.136
Page 9 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94717BF-SSV-11
14.8 05/05/2023 17:30TO-15 Ethylbenzene µg/m3 0.106
12.8 05/05/2023 17:30TO-15 4-Ethyltoluene µg/m3 0.128
5.90 05/05/2023 17:30TO-15 Heptane µg/m3 0.143
40.5 05/05/2023 17:30TO-15 n-Hexane µg/m3 0.047
J52.8 05/09/2023 00:19TO-15 Isopropyl Alcohol µg/m3 2.78
9.45 05/05/2023 17:30TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
4.51 05/05/2023 17:30TO-15 4-Methyl-2-Pentanone µg/m3 0.121
30.8 05/05/2023 17:30TO-15 Methylene Chloride µg/m3 0.488
4.94 05/05/2023 17:30TO-15 Naphthalene µg/m3 0.183
7.56 05/05/2023 17:30TO-15 Propene µg/m3 0.242
8.39 05/05/2023 17:30TO-15 Styrene µg/m3 0.124
3.76 05/05/2023 17:30TO-15 Tetrachloroethene µg/m3 0.181
J0.468 05/05/2023 17:30TO-15 Tetrahydrofuran µg/m3 0.107
60.5 05/05/2023 17:30TO-15 Toluene µg/m3 0.090
3.99 05/05/2023 17:30TO-15 Trichlorofluoromethane µg/m3 0.130
32.0 05/05/2023 17:30TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
12.4 05/05/2023 17:30TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
26.7 05/05/2023 17:30TO-15 o-Xylene µg/m3 0.157
54.4 05/05/2023 17:30TO-15 m,p-Xylene µg/m3 0.217
81.1 05/05/2023 17:30TO-15 Xylene (Total)µg/m3 0.157
V 94718BF-SSV-4
27.4 05/05/2023 18:20TO-15 Acetone µg/m3 0.202
B1.83 05/05/2023 18:20TO-15 Benzene µg/m3 0.073
J1.89 05/05/2023 18:20TO-15 Carbon Disulfide µg/m3 0.060
J0.768 05/05/2023 18:20TO-15 Chlorobenzene µg/m3 0.107
J2.42 05/05/2023 18:20TO-15 Chloroform µg/m3 0.086
J0.661 05/05/2023 18:20TO-15 1,2-Dichlorobenzene µg/m3 0.096
J1.42 05/05/2023 18:20TO-15 1,4-Dichlorobenzene µg/m3 0.186
2.78 05/05/2023 18:20TO-15 Dichlorodifluoromethane µg/m3 0.134
J0.742 05/05/2023 18:20TO-15 Ethyl Acetate µg/m3 0.136
8.03 05/05/2023 18:20TO-15 Ethylbenzene µg/m3 0.106
13.6 05/05/2023 18:20TO-15 4-Ethyltoluene µg/m3 0.128
J0.567 05/05/2023 18:20TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561
J1.40 05/05/2023 18:20TO-15 Heptane µg/m3 0.143
2.54 05/05/2023 18:20TO-15 n-Hexane µg/m3 0.047
39.6 05/05/2023 18:20TO-15 Isopropyl Alcohol µg/m3 0.139
Page 10 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-114-0003
Report Limit
Project:H&A-002
V 94718BF-SSV-4
4.36 05/05/2023 18:20TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224
J0.643 05/05/2023 18:20TO-15 4-Methyl-2-Pentanone µg/m3 0.121
3.62 05/05/2023 18:20TO-15 Methylene Chloride µg/m3 0.488
5.39 05/05/2023 18:20TO-15 Naphthalene µg/m3 0.183
5.31 05/05/2023 18:20TO-15 Propene µg/m3 0.242
6.78 05/05/2023 18:20TO-15 Styrene µg/m3 0.124
18.6 05/05/2023 18:20TO-15 Toluene µg/m3 0.090
J1.60 05/05/2023 18:20TO-15 Trichlorofluoromethane µg/m3 0.130
51.7 05/05/2023 18:20TO-15 1,2,4-Trimethylbenzene µg/m3 0.110
12.2 05/05/2023 18:20TO-15 1,3,5-Trimethylbenzene µg/m3 0.236
16.7 05/05/2023 18:20TO-15 o-Xylene µg/m3 0.157
32.0 05/05/2023 18:20TO-15 m,p-Xylene µg/m3 0.217
48.7 05/05/2023 18:20TO-15 Xylene (Total)µg/m3 0.157
Page 11 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-DUP
94707 Matrix:
4/20/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
29.1 µg/m3 0.202 4.75Acetone 1 05/04/23 22:53 V32829ENM
0.351 J
µg/m3 0.073 1.60
Benzene 1 05/04/23 22:53 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/04/23 22:53 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/04/23 22:53 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/04/23 22:53 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/04/23 22:53 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/04/23 22:53 V32829ENM
0.607 J µg/m3 0.060 6.23Carbon Disulfide 1 05/04/23 22:53 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/04/23 22:53 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/04/23 22:53 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/04/23 22:53 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/04/23 22:53 V32829ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 05/04/23 22:53 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/04/23 22:53 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/04/23 22:53 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/04/23 22:53 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/04/23 22:53 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/04/23 22:53 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/04/23 22:53 V32829ENM
2.69 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/04/23 22:53 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/04/23 22:53 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/04/23 22:53 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-DUP
94707 Matrix:
4/20/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/04/23 22:53 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/04/23 22:53 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/04/23 22:53 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/04/23 22:53 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/04/23 22:53 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/04/23 22:53 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/04/23 22:53 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/04/23 22:53 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/04/23 22:53 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/04/23 22:53 V32829ENM
4.55 µg/m3 0.128 2.464-Ethyltoluene 1 05/04/23 22:53 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/04/23 22:53 V32829ENM
<0.143 µg/m3 0.143 2.05Heptane 1 05/04/23 22:53 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/04/23 22:53 V32829ENM
0.260 J µg/m3 0.047 1.76n-Hexane 1 05/04/23 22:53 V32829ENM
0.679 J µg/m3 0.285 2.052-Hexanone 1 05/04/23 22:53 V32829ENM
11.2 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/04/23 22:53 V32829ENM
18.8 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/04/23 22:53 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/04/23 22:53 V32829ENM
0.630 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/04/23 22:53 V32829ENM
2.57 µg/m3 0.488 1.74Methylene Chloride 1 05/04/23 22:53 V32829ENM
4.83 µg/m3 0.183 2.62Naphthalene 1 05/04/23 22:53 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-DUP
94707 Matrix:
4/20/2023 0:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/04/23 22:53 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/04/23 22:53 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/04/23 22:53 V32829ENM
0.827 J µg/m3 0.181 3.39Tetrachloroethene 1 05/04/23 22:53 V32829ENM
20.1 µg/m3 0.107 1.47Tetrahydrofuran 1 05/04/23 22:53 V32829ENM
1.41 J µg/m3 0.090 1.88Toluene 1 05/04/23 22:53 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/04/23 22:53 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/04/23 22:53 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/04/23 22:53 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/04/23 22:53 V32829ENM
1.58 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/04/23 22:53 V32829ENM
5.11 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/04/23 22:53 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/04/23 22:53 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/04/23 22:53 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/04/23 22:53 V32829ENM
0.503 J µg/m3 0.157 2.17o-Xylene 1 05/04/23 22:53 V32829ENM
5.38 J µg/m3 0.217 5.65m,p-Xylene 1 05/04/23 22:53 V32829ENM
5.88 J µg/m3 0.157 2.17Xylene (Total)1 05/04/23 22:53 V32829
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%05/04/23 22:531 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-8
94708 Matrix:
4/20/2023 16:13
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
30.0 µg/m3 0.202 4.75Acetone 1 05/04/23 23:58 V32829ENM
0.360 J
µg/m3 0.073 1.60
Benzene 1 05/04/23 23:58 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/04/23 23:58 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/04/23 23:58 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/04/23 23:58 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/04/23 23:58 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/04/23 23:58 V32829ENM
0.632 J µg/m3 0.060 6.23Carbon Disulfide 1 05/04/23 23:58 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/04/23 23:58 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/04/23 23:58 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/04/23 23:58 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/04/23 23:58 V32829ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 05/04/23 23:58 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/04/23 23:58 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/04/23 23:58 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/04/23 23:58 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/04/23 23:58 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/04/23 23:58 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/04/23 23:58 V32829ENM
2.75 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/04/23 23:58 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/04/23 23:58 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/04/23 23:58 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-8
94708 Matrix:
4/20/2023 16:13
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/04/23 23:58 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/04/23 23:58 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/04/23 23:58 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/04/23 23:58 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/04/23 23:58 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/04/23 23:58 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/04/23 23:58 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/04/23 23:58 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/04/23 23:58 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/04/23 23:58 V32829ENM
4.56 µg/m3 0.128 2.464-Ethyltoluene 1 05/04/23 23:58 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/04/23 23:58 V32829ENM
<0.143 µg/m3 0.143 2.05Heptane 1 05/04/23 23:58 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/04/23 23:58 V32829ENM
0.285 J µg/m3 0.047 1.76n-Hexane 1 05/04/23 23:58 V32829ENM
0.688 J µg/m3 0.285 2.052-Hexanone 1 05/04/23 23:58 V32829ENM
11.1 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/04/23 23:58 V32829ENM
18.8 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/04/23 23:58 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/04/23 23:58 V32829ENM
0.696 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/04/23 23:58 V32829ENM
2.75 µg/m3 0.488 1.74Methylene Chloride 1 05/04/23 23:58 V32829ENM
4.80 µg/m3 0.183 2.62Naphthalene 1 05/04/23 23:58 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-8
94708 Matrix:
4/20/2023 16:13
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/04/23 23:58 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/04/23 23:58 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/04/23 23:58 V32829ENM
0.827 J µg/m3 0.181 3.39Tetrachloroethene 1 05/04/23 23:58 V32829ENM
20.0 µg/m3 0.107 1.47Tetrahydrofuran 1 05/04/23 23:58 V32829ENM
1.45 J µg/m3 0.090 1.88Toluene 1 05/04/23 23:58 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/04/23 23:58 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/04/23 23:58 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/04/23 23:58 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/04/23 23:58 V32829ENM
1.69 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/04/23 23:58 V32829ENM
5.18 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/04/23 23:58 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/04/23 23:58 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/04/23 23:58 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/04/23 23:58 V32829ENM
0.503 J µg/m3 0.157 2.17o-Xylene 1 05/04/23 23:58 V32829ENM
5.45 J µg/m3 0.217 5.65m,p-Xylene 1 05/04/23 23:58 V32829ENM
5.95 J µg/m3 0.157 2.17Xylene (Total)1 05/04/23 23:58 V32829
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/04/23 23:581 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-3
94709 Matrix:
4/18/2023 9:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
18.5 µg/m3 0.202 4.75Acetone 1 05/05/23 00:49 V32829ENM
0.964 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 00:49 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 00:49 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 00:49 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 00:49 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 00:49 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 00:49 V32829ENM
5.09 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 00:49 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 00:49 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 00:49 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 00:49 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 00:49 V32829ENM
0.580 J µg/m3 0.086 2.44Chloroform 1 05/05/23 00:49 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 00:49 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 00:49 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 00:49 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 00:49 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 00:49 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 00:49 V32829ENM
2.62 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 00:49 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 00:49 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 00:49 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-3
94709 Matrix:
4/18/2023 9:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 00:49 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 00:49 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 00:49 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 00:49 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 00:49 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 00:49 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 00:49 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 00:49 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 00:49 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 00:49 V32829ENM
4.50 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 00:49 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 00:49 V32829ENM
<0.143 µg/m3 0.143 2.05Heptane 1 05/05/23 00:49 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 00:49 V32829ENM
0.285 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 00:49 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 00:49 V32829ENM
4.98 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 00:49 V32829ENM
2.23 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 00:49 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 00:49 V32829ENM
0.421 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 00:49 V32829ENM
9.86 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 00:49 V32829ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 05/05/23 00:49 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-3
94709 Matrix:
4/18/2023 9:25
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 00:49 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 00:49 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 00:49 V32829ENM
0.624 J µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 00:49 V32829ENM
0.377 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 00:49 V32829ENM
0.795 J µg/m3 0.090 1.88Toluene 1 05/05/23 00:49 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 00:49 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 00:49 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 00:49 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 00:49 V32829ENM
1.69 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 00:49 V32829ENM
5.11 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 00:49 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 00:49 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 00:49 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 00:49 V32829ENM
0.712 J µg/m3 0.157 2.17o-Xylene 1 05/05/23 00:49 V32829ENM
5.65 µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 00:49 V32829ENM
6.36 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 00:49 V32829
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/05/23 00:491 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-7
94710 Matrix:
4/20/2023 16:33
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
71.1 µg/m3 0.202 4.75Acetone 1 05/05/23 01:42 V32829ENM
0.606 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 01:42 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 01:42 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 01:42 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 01:42 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 01:42 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 01:42 V32829ENM
0.999 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 01:42 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 01:42 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 01:42 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 01:42 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 01:42 V32829ENM
0.507 J µg/m3 0.086 2.44Chloroform 1 05/05/23 01:42 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 01:42 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 01:42 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 01:42 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 01:42 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 01:42 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 01:42 V32829ENM
2.68 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 01:42 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 01:42 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 01:42 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-7
94710 Matrix:
4/20/2023 16:33
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 01:42 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 01:42 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 01:42 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 01:42 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 01:42 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 01:42 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 01:42 V32829ENM
0.673 J µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 01:42 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 01:42 V32829ENM
0.668 J µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 01:42 V32829ENM
4.67 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 01:42 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 01:42 V32829ENM
1.07 J µg/m3 0.143 2.05Heptane 1 05/05/23 01:42 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 01:42 V32829ENM
0.877 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 01:42 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 01:42 V32829ENM
22.7 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 01:42 V32829ENM
2.83 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 01:42 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 01:42 V32829ENM
0.507 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 01:42 V32829ENM
9.69 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 01:42 V32829ENM
4.79 µg/m3 0.183 2.62Naphthalene 1 05/05/23 01:42 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-7
94710 Matrix:
4/20/2023 16:33
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
2.77 µg/m3 0.242 0.860Propene 1 05/05/23 01:42 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 01:42 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 01:42 V32829ENM
3.22 J µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 01:42 V32829ENM
1.33 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 01:42 V32829ENM
3.32 µg/m3 0.090 1.88Toluene 1 05/05/23 01:42 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 01:42 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 01:42 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 01:42 V32829ENM
2.25 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 01:42 V32829ENM
1.93 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 01:42 V32829ENM
5.48 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 01:42 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 01:42 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 01:42 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 01:42 V32829ENM
1.61 J µg/m3 0.157 2.17o-Xylene 1 05/05/23 01:42 V32829ENM
7.22 µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 01:42 V32829ENM
8.83 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 01:42 V32829
Surrogate: 4-Bromofluorobenzene 93.6 Limits: 70-130%05/05/23 01:421 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-1
94711 Matrix:
4/17/2023 16:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
12.8 µg/m3 0.202 4.75Acetone 1 05/05/23 02:45 V32829ENM
0.450 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 02:45 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 02:45 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 02:45 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 02:45 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 02:45 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 02:45 V32829ENM
2.85 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 02:45 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 02:45 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 02:45 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 02:45 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 02:45 V32829ENM
1.90 J µg/m3 0.086 2.44Chloroform 1 05/05/23 02:45 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 02:45 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 02:45 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 02:45 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 02:45 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 02:45 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 02:45 V32829ENM
2.87 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 02:45 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 02:45 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 02:45 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-1
94711 Matrix:
4/17/2023 16:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 02:45 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 02:45 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 02:45 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 02:45 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 02:45 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 02:45 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 02:45 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 02:45 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 02:45 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 02:45 V32829ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 02:45 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 02:45 V32829ENM
<0.143 µg/m3 0.143 2.05Heptane 1 05/05/23 02:45 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 02:45 V32829ENM
0.377 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 02:45 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 02:45 V32829ENM
5.05 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 02:45 V32829ENM
1.35 J µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 02:45 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 02:45 V32829ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 02:45 V32829ENM
11.7 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 02:45 V32829ENM
4.83 µg/m3 0.183 2.62Naphthalene 1 05/05/23 02:45 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-1
94711 Matrix:
4/17/2023 16:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 02:45 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 02:45 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 02:45 V32829ENM
31.3 µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 02:45 V32829ENM
0.238 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 02:45 V32829ENM
1.00 J µg/m3 0.090 1.88Toluene 1 05/05/23 02:45 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 02:45 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 02:45 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 02:45 V32829ENM
9.43 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 02:45 V32829ENM
2.37 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 02:45 V32829ENM
<0.110 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 02:45 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 02:45 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 02:45 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 02:45 V32829ENM
<0.157 µg/m3 0.157 2.17o-Xylene 1 05/05/23 02:45 V32829ENM
4.89 J µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 02:45 V32829ENM
4.89 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 02:45 V32829
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%05/05/23 02:451 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-10
94712 Matrix:
4/17/2023 15:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
23.9 µg/m3 0.202 4.75Acetone 1 05/05/23 03:36 V32829ENM
0.383 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 03:36 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 03:36 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 03:36 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 03:36 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 03:36 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 03:36 V32829ENM
1.13 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 03:36 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 03:36 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 03:36 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 03:36 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 03:36 V32829ENM
1.35 J µg/m3 0.086 2.44Chloroform 1 05/05/23 03:36 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 03:36 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 03:36 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 03:36 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 03:36 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 03:36 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 03:36 V32829ENM
40.2 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 03:36 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 03:36 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 03:36 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-10
94712 Matrix:
4/17/2023 15:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 03:36 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 03:36 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 03:36 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 03:36 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 03:36 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 03:36 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 03:36 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 03:36 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 03:36 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 03:36 V32829ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 03:36 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 03:36 V32829ENM
0.536 J µg/m3 0.143 2.05Heptane 1 05/05/23 03:36 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 03:36 V32829ENM
0.440 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 03:36 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 03:36 V32829ENM
15.6 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 03:36 V32829ENM
2.74 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 03:36 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 03:36 V32829ENM
2.83 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 03:36 V32829ENM
5.94 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 03:36 V32829ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 05/05/23 03:36 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-10
94712 Matrix:
4/17/2023 15:50
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 03:36 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 03:36 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 03:36 V32829ENM
5.67 µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 03:36 V32829ENM
0.867 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 03:36 V32829ENM
0.904 J µg/m3 0.090 1.88Toluene 1 05/05/23 03:36 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 03:36 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 03:36 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 03:36 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 03:36 V32829ENM
1.69 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 03:36 V32829ENM
<0.110 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 03:36 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 03:36 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 03:36 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 03:36 V32829ENM
<0.157 µg/m3 0.157 2.17o-Xylene 1 05/05/23 03:36 V32829ENM
4.90 J µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 03:36 V32829ENM
4.90 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 03:36 V32829
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%05/05/23 03:361 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-2
94713 Matrix:
4/18/2023 8:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
7.48 B µg/m3 0.202 4.75Acetone 1 05/05/23 04:29 V32829ENM
0.268 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 04:29 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 04:29 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 04:29 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 04:29 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 04:29 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 04:29 V32829ENM
0.333 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 04:29 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 04:29 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 04:29 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 04:29 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 04:29 V32829ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 05/05/23 04:29 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 04:29 V32829ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 04:29 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 04:29 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 04:29 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 04:29 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 04:29 V32829ENM
2.75 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 04:29 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 04:29 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 04:29 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-2
94713 Matrix:
4/18/2023 8:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 04:29 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 04:29 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 04:29 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 04:29 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 04:29 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 04:29 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 04:29 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 04:29 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 04:29 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 04:29 V32829ENM
4.59 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 04:29 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 04:29 V32829ENM
<0.143 µg/m3 0.143 2.05Heptane 1 05/05/23 04:29 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 04:29 V32829ENM
<0.047 µg/m3 0.047 1.76n-Hexane 1 05/05/23 04:29 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 04:29 V32829ENM
3.62 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 04:29 V32829ENM
3.05 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 04:29 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 04:29 V32829ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 04:29 V32829ENM
3.70 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 04:29 V32829ENM
5.59 µg/m3 0.183 2.62Naphthalene 1 05/05/23 04:29 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-2
94713 Matrix:
4/18/2023 8:55
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 04:29 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 04:29 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 04:29 V32829ENM
0.488 J µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 04:29 V32829ENM
0.990 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 04:29 V32829ENM
0.388 J µg/m3 0.090 1.88Toluene 1 05/05/23 04:29 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 04:29 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 04:29 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 04:29 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 04:29 V32829ENM
1.60 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 04:29 V32829ENM
6.33 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 04:29 V32829ENM
0.550 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 04:29 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 04:29 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 04:29 V32829ENM
<0.157 µg/m3 0.157 2.17o-Xylene 1 05/05/23 04:29 V32829ENM
<0.217 µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 04:29 V32829ENM
<0.157 µg/m3 0.157 2.17Xylene (Total)1 05/05/23 04:29 V32829
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/05/23 04:291 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-5
94714 Matrix:
4/17/2023 16:27
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
13.1 µg/m3 0.202 4.75Acetone 1 05/05/23 05:22 V32829ENM
0.482 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 05:22 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 05:22 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 05:22 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 05:22 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 05:22 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 05:22 V32829ENM
<0.060 µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 05:22 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 05:22 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 05:22 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 05:22 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 05:22 V32829ENM
<0.086 µg/m3 0.086 2.44Chloroform 1 05/05/23 05:22 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 05:22 V32829ENM
2.41 J µg/m3 0.161 3.44Cyclohexane 1 05/05/23 05:22 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 05:22 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 05:22 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 05:22 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 05:22 V32829ENM
2.59 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 05:22 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 05:22 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 05:22 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-5
94714 Matrix:
4/17/2023 16:27
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 05:22 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 05:22 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 05:22 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 05:22 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 05:22 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 05:22 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 05:22 V32829ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 05:22 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 05:22 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 05:22 V32829ENM
<0.128 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 05:22 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 05:22 V32829ENM
0.295 J µg/m3 0.143 2.05Heptane 1 05/05/23 05:22 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 05:22 V32829ENM
0.345 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 05:22 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 05:22 V32829ENM
4.20 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 05:22 V32829ENM
1.42 J µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 05:22 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 05:22 V32829ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 05:22 V32829ENM
13.3 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 05:22 V32829ENM
4.93 µg/m3 0.183 2.62Naphthalene 1 05/05/23 05:22 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-5
94714 Matrix:
4/17/2023 16:27
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 05:22 V32829ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/05/23 05:22 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 05:22 V32829ENM
0.820 J µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 05:22 V32829ENM
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 05:22 V32829ENM
1.39 J µg/m3 0.090 1.88Toluene 1 05/05/23 05:22 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 05:22 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 05:22 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 05:22 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 05:22 V32829ENM
1.56 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 05:22 V32829ENM
4.96 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 05:22 V32829ENM
<0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 05:22 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 05:22 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 05:22 V32829ENM
<0.157 µg/m3 0.157 2.17o-Xylene 1 05/05/23 05:22 V32829ENM
5.03 J µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 05:22 V32829ENM
5.03 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 05:22 V32829
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%05/05/23 05:221 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-9
94715 Matrix:
4/17/2023 15:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
44.8 µg/m3 0.202 4.75Acetone 1 05/05/23 06:15 V32829ENM
0.415 J
µg/m3 0.073 1.60
Benzene 1 05/05/23 06:15 V32829ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 06:15 V32829ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 06:15 V32829ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 06:15 V32829ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 06:15 V32829ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 06:15 V32829ENM
5.01 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 06:15 V32829ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 06:15 V32829ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 06:15 V32829ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 06:15 V32829ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 06:15 V32829ENM
0.795 J µg/m3 0.086 2.44Chloroform 1 05/05/23 06:15 V32829ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 06:15 V32829ENM
2.02 J µg/m3 0.161 3.44Cyclohexane 1 05/05/23 06:15 V32829ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 06:15 V32829ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 06:15 V32829ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 06:15 V32829ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 06:15 V32829ENM
2.43 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 06:15 V32829ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 06:15 V32829ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 06:15 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-9
94715 Matrix:
4/17/2023 15:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 06:15 V32829ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 06:15 V32829ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 06:15 V32829ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 06:15 V32829ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 06:15 V32829ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 06:15 V32829ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 06:15 V32829ENM
0.493 J µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 06:15 V32829ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 06:15 V32829ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 06:15 V32829ENM
8.18 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 06:15 V32829ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 06:15 V32829ENM
0.381 J µg/m3 0.143 2.05Heptane 1 05/05/23 06:15 V32829ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 06:15 V32829ENM
0.807 J µg/m3 0.047 1.76n-Hexane 1 05/05/23 06:15 V32829ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 06:15 V32829ENM
16.2 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 06:15 V32829ENM
4.68 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 06:15 V32829ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 06:15 V32829ENM
1.32 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 06:15 V32829ENM
8.45 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 06:15 V32829ENM
4.79 µg/m3 0.183 2.62Naphthalene 1 05/05/23 06:15 V32829ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-9
94715 Matrix:
4/17/2023 15:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32828 05/04/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/05/23 06:15 V32829ENM
5.47 µg/m3 0.124 2.13
Styrene 1 05/05/23 06:15 V32829ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 06:15 V32829ENM
1.08 J µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 06:15 V32829ENM
1.99 µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 06:15 V32829ENM
1.63 J µg/m3 0.090 1.88Toluene 1 05/05/23 06:15 V32829ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 06:15 V32829ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 06:15 V32829ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 06:15 V32829ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 06:15 V32829ENM
1.42 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 06:15 V32829ENM
14.6 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 06:15 V32829ENM
3.11 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 06:15 V32829ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 06:15 V32829ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 06:15 V32829ENM
1.54 J µg/m3 0.157 2.17o-Xylene 1 05/05/23 06:15 V32829ENM
5.35 J µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 06:15 V32829ENM
6.89 J µg/m3 0.157 2.17Xylene (Total)1 05/05/23 06:15 V32829
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/05/23 06:151 ENM V32829
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-6
94716 Matrix:
4/17/2023 15:20
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32965 05/09/23 09:00
13.8 µg/m3 0.202 4.75Acetone 1 05/09/23 14:18 V32966ENM
0.396 J
µg/m3 0.073 1.60
Benzene 1 05/09/23 14:18 V32966ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/09/23 14:18 V32966ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/09/23 14:18 V32966ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/09/23 14:18 V32966ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/09/23 14:18 V32966ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/09/23 14:18 V32966ENM
0.479 JB µg/m3 0.060 6.23Carbon Disulfide 1 05/09/23 14:18 V32966ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/09/23 14:18 V32966ENM
<0.107 µg/m3 0.107 2.30Chlorobenzene 1 05/09/23 14:18 V32966ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/09/23 14:18 V32966ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/09/23 14:18 V32966ENM
0.585 J µg/m3 0.086 2.44Chloroform 1 05/09/23 14:18 V32966ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/09/23 14:18 V32966ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/09/23 14:18 V32966ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/09/23 14:18 V32966ENM
<0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/09/23 14:18 V32966ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/09/23 14:18 V32966ENM
<0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/09/23 14:18 V32966ENM
2.77 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/09/23 14:18 V32966ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/09/23 14:18 V32966ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/09/23 14:18 V32966ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-6
94716 Matrix:
4/17/2023 15:20
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32965 05/09/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/09/23 14:18 V32966ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/09/23 14:18 V32966ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/09/23 14:18 V32966ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/09/23 14:18 V32966ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/09/23 14:18 V32966ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/09/23 14:18 V32966ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/09/23 14:18 V32966ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/09/23 14:18 V32966ENM
<0.136 µg/m3 0.136 1.80
Ethyl Acetate 1 05/09/23 14:18 V32966ENM
<0.106 µg/m3 0.106 2.17Ethylbenzene 1 05/09/23 14:18 V32966ENM
5.59 µg/m3 0.128 2.464-Ethyltoluene 1 05/09/23 14:18 V32966ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/09/23 14:18 V32966ENM
0.467 J µg/m3 0.143 2.05Heptane 1 05/09/23 14:18 V32966ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/09/23 14:18 V32966ENM
0.296 J µg/m3 0.047 1.76n-Hexane 1 05/09/23 14:18 V32966ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/09/23 14:18 V32966ENM
5.50 B µg/m3 0.139 4.92Isopropyl Alcohol 1 05/09/23 14:18 V32966ENM
1.56 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/09/23 14:18 V32966ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/09/23 14:18 V32966ENM
<0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/09/23 14:18 V32966ENM
18.7 µg/m3 0.488 1.74Methylene Chloride 1 05/09/23 14:18 V32966ENM
<0.183 µg/m3 0.183 2.62Naphthalene 1 05/09/23 14:18 V32966ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-6
94716 Matrix:
4/17/2023 15:20
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32965 05/09/23 09:00
<0.242 µg/m3 0.242 0.860Propene 1 05/09/23 14:18 V32966ENM
<0.124 µg/m3 0.124 2.13
Styrene 1 05/09/23 14:18 V32966ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/09/23 14:18 V32966ENM
19.6 µg/m3 0.181 3.39Tetrachloroethene 1 05/09/23 14:18 V32966ENM
0.669 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/09/23 14:18 V32966ENM
1.25 J µg/m3 0.090 1.88Toluene 1 05/09/23 14:18 V32966ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/09/23 14:18 V32966ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/09/23 14:18 V32966ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/09/23 14:18 V32966ENM
8.38 µg/m3 0.199 2.15Trichloroethene 1 05/09/23 14:18 V32966ENM
1.93 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/09/23 14:18 V32966ENM
7.20 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/09/23 14:18 V32966ENM
0.619 J µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/09/23 14:18 V32966ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/09/23 14:18 V32966ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/09/23 14:18 V32966ENM
0.655 J µg/m3 0.157 2.17o-Xylene 1 05/09/23 14:18 V32966ENM
4.98 J µg/m3 0.217 5.65m,p-Xylene 1 05/09/23 14:18 V32966ENM
5.64 J µg/m3 0.157 2.17Xylene (Total)1 05/09/23 14:18 V32966
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%05/05/23 16:281 ENM V32879
Surrogate: 4-Bromofluorobenzene 96.4 Limits: 70-130%05/09/23 14:181 ENM V32966
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-11
94717 Matrix:
4/17/2023 14:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00 V32929 05/08/23 09:00
36.3 µg/m3 0.202 4.75Acetone 1 05/05/23 17:30 V32879ENM
5.67 µg/m3 0.073 1.60
Benzene 1 05/05/23 17:30 V32879ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 17:30 V32879ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 17:30 V32879ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 17:30 V32879ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 17:30 V32879ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 17:30 V32879ENM
1.10 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 17:30 V32879ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 17:30 V32879ENM
2.71 µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 17:30 V32879ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 17:30 V32879ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 17:30 V32879ENM
1.47 J µg/m3 0.086 2.44Chloroform 1 05/05/23 17:30 V32879ENM
0.774 J µg/m3 0.067 1.03Chloromethane 1 05/05/23 17:30 V32879ENM
2.44 J µg/m3 0.161 3.44Cyclohexane 1 05/05/23 17:30 V32879ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 17:30 V32879ENM
0.841 J µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 17:30 V32879ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 17:30 V32879ENM
1.95 J µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 17:30 V32879ENM
3.56 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 17:30 V32879ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 17:30 V32879ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 17:30 V32879ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-11
94717 Matrix:
4/17/2023 14:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00 V32929 05/08/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 17:30 V32879ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 17:30 V32879ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 17:30 V32879ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 17:30 V32879ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 17:30 V32879ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 17:30 V32879ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 17:30 V32879ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 17:30 V32879ENM
5.69 µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 17:30 V32879ENM
14.8 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 17:30 V32879ENM
12.8 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 17:30 V32879ENM
<0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 17:30 V32879ENM
5.90 µg/m3 0.143 2.05Heptane 1 05/05/23 17:30 V32879ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 17:30 V32879ENM
40.5 µg/m3 0.047 1.76n-Hexane 1 05/05/23 17:30 V32879ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 17:30 V32879ENM
52.8 J µg/m3 2.78 98.3Isopropyl Alcohol 20 05/09/23 00:19 V32931ENM
9.45 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 17:30 V32879ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 17:30 V32879ENM
4.51 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 17:30 V32879ENM
30.8 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 17:30 V32879ENM
4.94 µg/m3 0.183 2.62Naphthalene 1 05/05/23 17:30 V32879ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-11
94717 Matrix:
4/17/2023 14:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00 V32929 05/08/23 09:00
7.56 µg/m3 0.242 0.860Propene 1 05/05/23 17:30 V32879ENM
8.39 µg/m3 0.124 2.13
Styrene 1 05/05/23 17:30 V32879ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 17:30 V32879ENM
3.76 µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 17:30 V32879ENM
0.468 J µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 17:30 V32879ENM
60.5 µg/m3 0.090 1.88Toluene 1 05/05/23 17:30 V32879ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 17:30 V32879ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 17:30 V32879ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 17:30 V32879ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 17:30 V32879ENM
3.99 µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 17:30 V32879ENM
32.0 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 17:30 V32879ENM
12.4 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 17:30 V32879ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 17:30 V32879ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 17:30 V32879ENM
26.7 µg/m3 0.157 2.17o-Xylene 1 05/05/23 17:30 V32879ENM
54.4 µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 17:30 V32879ENM
81.1 µg/m3 0.157 2.17Xylene (Total)1 05/05/23 17:30 V32879
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%05/05/23 17:301 ENM V32879
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/09/23 00:1920 ENM V32931
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-4
94718 Matrix:
4/18/2023 11:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00
27.4 µg/m3 0.202 4.75Acetone 1 05/05/23 18:20 V32879ENM
1.83 B
µg/m3 0.073 1.60
Benzene 1 05/05/23 18:20 V32879ENM
<0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/05/23 18:20 V32879ENM
<0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/05/23 18:20 V32879ENM
<0.153 µg/m3 0.153 5.17Bromoform 1 05/05/23 18:20 V32879ENM
<0.115 µg/m3 0.115 1.94Bromomethane 1 05/05/23 18:20 V32879ENM
<0.328 µg/m3 0.328 1.111,3-Butadiene 1 05/05/23 18:20 V32879ENM
1.89 J µg/m3 0.060 6.23Carbon Disulfide 1 05/05/23 18:20 V32879ENM
<0.155 µg/m3 0.155 3.15
Carbon Tetrachloride 1 05/05/23 18:20 V32879ENM
0.768 J µg/m3 0.107 2.30Chlorobenzene 1 05/05/23 18:20 V32879ENM
<0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/05/23 18:20 V32879ENM
<0.164 µg/m3 0.164 1.32Chloroethane 1 05/05/23 18:20 V32879ENM
2.42 J µg/m3 0.086 2.44Chloroform 1 05/05/23 18:20 V32879ENM
<0.067 µg/m3 0.067 1.03Chloromethane 1 05/05/23 18:20 V32879ENM
<0.161 µg/m3 0.161 3.44Cyclohexane 1 05/05/23 18:20 V32879ENM
<0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/05/23 18:20 V32879ENM
0.661 J µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/05/23 18:20 V32879ENM
<0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/05/23 18:20 V32879ENM
1.42 J µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/05/23 18:20 V32879ENM
2.78 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/05/23 18:20 V32879ENM
<0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/05/23 18:20 V32879ENM
<0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/05/23 18:20 V32879ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-4
94718 Matrix:
4/18/2023 11:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00
<0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/05/23 18:20 V32879ENM
<0.095 µg/m3 0.095 1.98
cis-1,2-Dichloroethene 1 05/05/23 18:20 V32879ENM
<0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/05/23 18:20 V32879ENM
<0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/05/23 18:20 V32879ENM
<0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/05/23 18:20 V32879ENM
<0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/05/23 18:20 V32879ENM
<0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/05/23 18:20 V32879ENM
<0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/05/23 18:20 V32879ENM
0.742 J
µg/m3 0.136 1.80
Ethyl Acetate 1 05/05/23 18:20 V32879ENM
8.03 µg/m3 0.106 2.17Ethylbenzene 1 05/05/23 18:20 V32879ENM
13.6 µg/m3 0.128 2.464-Ethyltoluene 1 05/05/23 18:20 V32879ENM
0.567 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/05/23 18:20 V32879ENM
1.40 J µg/m3 0.143 2.05Heptane 1 05/05/23 18:20 V32879ENM
<0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/05/23 18:20 V32879ENM
2.54 µg/m3 0.047 1.76n-Hexane 1 05/05/23 18:20 V32879ENM
<0.285 µg/m3 0.285 2.052-Hexanone 1 05/05/23 18:20 V32879ENM
39.6 µg/m3 0.139 4.92Isopropyl Alcohol 1 05/05/23 18:20 V32879ENM
4.36 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/05/23 18:20 V32879ENM
<0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/05/23 18:20 V32879ENM
0.643 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/05/23 18:20 V32879ENM
3.62 µg/m3 0.488 1.74Methylene Chloride 1 05/05/23 18:20 V32879ENM
5.39 µg/m3 0.183 2.62Naphthalene 1 05/05/23 18:20 V32879ENM
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-114-0003
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Loryn Smith
Charlotte
Received : 04/24/2023
H&A-002
Report Date : 05/09/2023
Sample ID :
Lab No :
Sampled:BF-SSV-4
94718 Matrix:
4/18/2023 11:00
Air
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
TO-15 Prep
TO-15 Prep Batch(es):V32871 05/05/23 09:00
5.31 µg/m3 0.242 0.860Propene 1 05/05/23 18:20 V32879ENM
6.78 µg/m3 0.124 2.13
Styrene 1 05/05/23 18:20 V32879ENM
<0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/05/23 18:20 V32879ENM
<0.181 µg/m3 0.181 3.39Tetrachloroethene 1 05/05/23 18:20 V32879ENM
<0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 05/05/23 18:20 V32879ENM
18.6 µg/m3 0.090 1.88Toluene 1 05/05/23 18:20 V32879ENM
<0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/05/23 18:20 V32879ENM
<0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/05/23 18:20 V32879ENM
<0.087 µg/m3 0.087 2.73
1,1,2-Trichloroethane 1 05/05/23 18:20 V32879ENM
<0.199 µg/m3 0.199 2.15Trichloroethene 1 05/05/23 18:20 V32879ENM
1.60 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/05/23 18:20 V32879ENM
51.7 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/05/23 18:20 V32879ENM
12.2 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/05/23 18:20 V32879ENM
<0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/05/23 18:20 V32879ENM
<0.127 µg/m3 0.127 1.28Vinyl Chloride 1 05/05/23 18:20 V32879ENM
16.7 µg/m3 0.157 2.17o-Xylene 1 05/05/23 18:20 V32879ENM
32.0 µg/m3 0.217 5.65m,p-Xylene 1 05/05/23 18:20 V32879ENM
48.7 µg/m3 0.157 2.17Xylene (Total)1 05/05/23 18:20 V32879
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%05/05/23 18:201 ENM V32879
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32829QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32828
Associated Lab Samples: 94707, 94708, 94709, 94710, 94711, 94712, 94713, 94714, 94715
LRB-V32828 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 11:304.750.2020.992µg/m3Acetone
05/04/23 11:301.600.073<0.073µg/m3Benzene
05/04/23 11:3010.40.147<0.147µg/m3Benzyl Chloride
05/04/23 11:303.350.150<0.150µg/m3Bromodichloromethane
05/04/23 11:305.170.153<0.153µg/m3Bromoform
05/04/23 11:301.940.115<0.115µg/m3Bromomethane
05/04/23 11:301.110.328<0.328µg/m31,3-Butadiene
05/04/23 11:306.230.060<0.060µg/m3Carbon Disulfide
05/04/23 11:303.150.155<0.155µg/m3Carbon Tetrachloride
05/04/23 11:302.300.107<0.107µg/m3Chlorobenzene
05/04/23 11:304.260.208<0.208µg/m3Chlorodibromomethane
05/04/23 11:301.320.164<0.164µg/m3Chloroethane
05/04/23 11:302.440.086<0.086µg/m3Chloroform
05/04/23 11:301.030.067<0.067µg/m3Chloromethane
05/04/23 11:303.440.161<0.161µg/m3Cyclohexane
05/04/23 11:303.840.151<0.151µg/m31,2-Dibromoethane
05/04/23 11:303.010.096<0.096µg/m31,2-Dichlorobenzene
05/04/23 11:3012.00.174<0.174µg/m31,3-Dichlorobenzene
05/04/23 11:303.010.186<0.186µg/m31,4-Dichlorobenzene
05/04/23 11:302.470.134<0.134µg/m3Dichlorodifluoromethane
05/04/23 11:302.020.101<0.101µg/m31,1-Dichloroethane
05/04/23 11:302.020.129<0.129µg/m31,2-Dichloroethane
05/04/23 11:301.980.107<0.107µg/m31,1-Dichloroethene
05/04/23 11:301.980.095<0.095µg/m3cis-1,2-Dichloroethene
05/04/23 11:301.980.108<0.108µg/m3trans-1,2-Dichloroethene
05/04/23 11:302.310.205<0.205µg/m31,2-Dichloropropane
05/04/23 11:303.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane
Page 1 of 16Date:05/09/2023 04:27 PM
Page 48 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32829QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32828
Associated Lab Samples: 94707, 94708, 94709, 94710, 94711, 94712, 94713, 94714, 94715
LRB-V32828 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 11:302.270.178<0.178µg/m3cis-1,3-Dichloropropene
05/04/23 11:302.270.178<0.178µg/m3trans-1,3-Dichloropropene
05/04/23 11:301.800.435<0.435µg/m31,4-Dioxane
05/04/23 11:301.800.136<0.136µg/m3Ethyl Acetate
05/04/23 11:302.170.106<0.106µg/m3Ethylbenzene
05/04/23 11:302.460.128<0.128µg/m34-Ethyltoluene
05/04/23 11:303.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
05/04/23 11:302.050.143<0.143µg/m3Heptane
05/04/23 11:305.330.330<0.330µg/m3Hexachlorobutadiene
05/04/23 11:301.760.047<0.047µg/m3n-Hexane
05/04/23 11:302.050.285<0.285µg/m32-Hexanone
05/04/23 11:304.920.1392.37µg/m3Isopropyl Alcohol
05/04/23 11:301.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
05/04/23 11:301.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE)
05/04/23 11:302.050.121<0.121µg/m34-Methyl-2-Pentanone
05/04/23 11:301.740.488<0.488µg/m3Methylene Chloride
05/04/23 11:302.620.183<0.183µg/m3Naphthalene
05/04/23 11:300.8600.242<0.242µg/m3Propene
05/04/23 11:302.130.124<0.124µg/m3Styrene
05/04/23 11:303.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
05/04/23 11:303.390.181<0.181µg/m3Tetrachloroethene
05/04/23 11:301.470.107<0.107µg/m3Tetrahydrofuran
05/04/23 11:301.880.090<0.090µg/m3Toluene
05/04/23 11:303.710.209<0.209µg/m31,2,4-Trichlorobenzene
05/04/23 11:302.730.144<0.144µg/m31,1,1-Trichloroethane
05/04/23 11:302.730.087<0.087µg/m31,1,2-Trichloroethane
05/04/23 11:302.150.199<0.199µg/m3Trichloroethene
Page 2 of 16Date:05/09/2023 04:27 PM
Page 49 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32829QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32828
Associated Lab Samples: 94707, 94708, 94709, 94710, 94711, 94712, 94713, 94714, 94715
LRB-V32828 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/04/23 11:302.810.130<0.130µg/m3Trichlorofluoromethane
05/04/23 11:302.460.110<0.110µg/m31,2,4-Trimethylbenzene
05/04/23 11:302.460.236<0.236µg/m31,3,5-Trimethylbenzene
05/04/23 11:301.760.224<0.224µg/m3Vinyl Acetate
05/04/23 11:301.280.127<0.127µg/m3Vinyl Chloride
05/04/23 11:302.170.157<0.157µg/m3o-Xylene
05/04/23 11:305.650.217<0.217µg/m3m,p-Xylene
05/04/23 11:304-Bromofluorobenzene (S)91.0 70-130
LCS-V32828Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
89.010.611.9µg/m3Acetone 70-130
81.813.116.0µg/m3Benzene 70-130
90.723.525.9µg/m3Benzyl Chloride 70-130
79.726.733.5µg/m3Bromodichloromethane 70-130
84.943.951.7µg/m3Bromoform 70-130
83.516.219.4µg/m3Bromomethane 70-130
81.09.0011.1µg/m31,3-Butadiene 70-130
87.813.715.6µg/m3Carbon Disulfide 70-130
82.526.031.5µg/m3Carbon Tetrachloride 70-130
88.220.323.0µg/m3Chlorobenzene 70-130
87.037.142.6µg/m3Chlorodibromomethane 70-130
81.010.713.2µg/m3Chloroethane 70-130
82.720.224.4µg/m3Chloroform 70-130
86.38.8910.3µg/m3Chloromethane 70-130
77.313.317.2µg/m3Cyclohexane 70-130
Page 3 of 16Date:05/09/2023 04:27 PM
Page 50 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32829QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32828
LCS-V32828Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.433.238.4µg/m31,2-Dibromoethane 70-130
93.328.130.1µg/m31,2-Dichlorobenzene 70-130
89.326.930.1µg/m31,3-Dichlorobenzene 70-130
91.027.430.1µg/m31,4-Dichlorobenzene 70-130
85.821.224.7µg/m3Dichlorodifluoromethane 70-130
85.617.320.2µg/m31,1-Dichloroethane 70-130
81.616.520.2µg/m31,2-Dichloroethane 70-130
85.316.919.8µg/m31,1-Dichloroethene 70-130
87.317.319.8µg/m3cis-1,2-Dichloroethene 70-130
87.317.319.8µg/m3trans-1,2-Dichloroethene 70-130
80.918.723.1µg/m31,2-Dichloropropane 70-130
86.030.135.0µg/m31,2-Dichlorotetrafluoroethane 70-130
83.218.922.7µg/m3cis-1,3-Dichloropropene 70-130
83.218.922.7µg/m3trans-1,3-Dichloropropene 70-130
80.514.518.0µg/m31,4-Dioxane 70-130
81.614.718.0µg/m3Ethyl Acetate 70-130
87.018.921.7µg/m3Ethylbenzene 70-130
86.521.324.6µg/m34-Ethyltoluene 70-130
85.932.938.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
82.917.020.5µg/m3Heptane 70-130
91.348.753.3µg/m3Hexachlorobutadiene 70-130
86.915.317.6µg/m3n-Hexane 70-130
85.317.520.5µg/m32-Hexanone 70-130
93.411.512.3µg/m3Isopropyl Alcohol 70-130
83.712.414.8µg/m3Methyl Ethyl Ketone (MEK)70-130
84.415.218.0µg/m3Methyl tert-butyl ether (MTBE)70-130
82.416.920.5µg/m34-Methyl-2-Pentanone 70-130
Page 4 of 16Date:05/09/2023 04:27 PM
Page 51 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32829QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32828
LCS-V32828Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.714.417.4µg/m3Methylene Chloride 70-130
90.023.626.2µg/m3Naphthalene 70-130
86.27.438.61µg/m3Propene 70-130
89.219.021.3µg/m3Styrene 70-130
89.530.734.3µg/m31,1,2,2-Tetrachloroethane 70-130
84.628.733.9µg/m3Tetrachloroethene 70-130
82.912.214.7µg/m3Tetrahydrofuran 70-130
83.515.718.8µg/m3Toluene 70-130
92.734.437.1µg/m31,2,4-Trichlorobenzene 70-130
81.622.327.3µg/m31,1,1-Trichloroethane 70-130
87.123.827.3µg/m31,1,2-Trichloroethane 70-130
83.222.426.9µg/m3Trichloroethene 70-130
86.424.328.1µg/m3Trichlorofluoromethane 70-130
90.622.324.6µg/m31,2,4-Trimethylbenzene 70-130
89.822.124.6µg/m31,3,5-Trimethylbenzene 70-130
88.015.517.6µg/m3Vinyl Acetate 70-130
85.110.912.8µg/m3Vinyl Chloride 70-130
91.719.921.7µg/m3o-Xylene 70-130
84.736.843.4µg/m3m,p-Xylene 70-130
1024-Bromofluorobenzene (S)70-130
Page 5 of 16Date:05/09/2023 04:27 PM
Page 52 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32879QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32871
Associated Lab Samples: 94717, 94718
LRB-V32871 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/05/23 10:304.750.2021.88µg/m3Acetone
05/05/23 10:301.600.0730.514µg/m3Benzene
05/05/23 10:3010.40.147<0.147µg/m3Benzyl Chloride
05/05/23 10:303.350.150<0.150µg/m3Bromodichloromethane
05/05/23 10:305.170.153<0.153µg/m3Bromoform
05/05/23 10:301.940.115<0.115µg/m3Bromomethane
05/05/23 10:301.110.328<0.328µg/m31,3-Butadiene
05/05/23 10:306.230.060<0.060µg/m3Carbon Disulfide
05/05/23 10:303.150.155<0.155µg/m3Carbon Tetrachloride
05/05/23 10:302.300.107<0.107µg/m3Chlorobenzene
05/05/23 10:304.260.208<0.208µg/m3Chlorodibromomethane
05/05/23 10:301.320.164<0.164µg/m3Chloroethane
05/05/23 10:302.440.086<0.086µg/m3Chloroform
05/05/23 10:301.030.067<0.067µg/m3Chloromethane
05/05/23 10:303.440.161<0.161µg/m3Cyclohexane
05/05/23 10:303.840.151<0.151µg/m31,2-Dibromoethane
05/05/23 10:303.010.096<0.096µg/m31,2-Dichlorobenzene
05/05/23 10:3012.00.174<0.174µg/m31,3-Dichlorobenzene
05/05/23 10:303.010.186<0.186µg/m31,4-Dichlorobenzene
05/05/23 10:302.470.134<0.134µg/m3Dichlorodifluoromethane
05/05/23 10:302.020.101<0.101µg/m31,1-Dichloroethane
05/05/23 10:302.020.129<0.129µg/m31,2-Dichloroethane
05/05/23 10:301.980.107<0.107µg/m31,1-Dichloroethene
05/05/23 10:301.980.095<0.095µg/m3cis-1,2-Dichloroethene
05/05/23 10:301.980.108<0.108µg/m3trans-1,2-Dichloroethene
05/05/23 10:302.310.205<0.205µg/m31,2-Dichloropropane
05/05/23 10:303.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane
Page 6 of 16Date:05/09/2023 04:27 PM
Page 53 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32879QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32871
Associated Lab Samples: 94717, 94718
LRB-V32871 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/05/23 10:302.270.178<0.178µg/m3cis-1,3-Dichloropropene
05/05/23 10:302.270.178<0.178µg/m3trans-1,3-Dichloropropene
05/05/23 10:301.800.435<0.435µg/m31,4-Dioxane
05/05/23 10:301.800.136<0.136µg/m3Ethyl Acetate
05/05/23 10:302.170.106<0.106µg/m3Ethylbenzene
05/05/23 10:302.460.128<0.128µg/m34-Ethyltoluene
05/05/23 10:303.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
05/05/23 10:302.050.143<0.143µg/m3Heptane
05/05/23 10:305.330.330<0.330µg/m3Hexachlorobutadiene
05/05/23 10:301.760.047<0.047µg/m3n-Hexane
05/05/23 10:302.050.285<0.285µg/m32-Hexanone
05/05/23 10:304.920.1392.35µg/m3Isopropyl Alcohol
05/05/23 10:301.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
05/05/23 10:301.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE)
05/05/23 10:302.050.121<0.121µg/m34-Methyl-2-Pentanone
05/05/23 10:301.740.488<0.488µg/m3Methylene Chloride
05/05/23 10:302.620.183<0.183µg/m3Naphthalene
05/05/23 10:300.8600.242<0.242µg/m3Propene
05/05/23 10:302.130.124<0.124µg/m3Styrene
05/05/23 10:303.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
05/05/23 10:303.390.181<0.181µg/m3Tetrachloroethene
05/05/23 10:301.470.107<0.107µg/m3Tetrahydrofuran
05/05/23 10:301.880.0900.569µg/m3Toluene
05/05/23 10:303.710.209<0.209µg/m31,2,4-Trichlorobenzene
05/05/23 10:302.730.144<0.144µg/m31,1,1-Trichloroethane
05/05/23 10:302.730.087<0.087µg/m31,1,2-Trichloroethane
05/05/23 10:302.150.199<0.199µg/m3Trichloroethene
Page 7 of 16Date:05/09/2023 04:27 PM
Page 54 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32879QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32871
Associated Lab Samples: 94717, 94718
LRB-V32871 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/05/23 10:302.810.130<0.130µg/m3Trichlorofluoromethane
05/05/23 10:302.460.110<0.110µg/m31,2,4-Trimethylbenzene
05/05/23 10:302.460.236<0.236µg/m31,3,5-Trimethylbenzene
05/05/23 10:301.760.224<0.224µg/m3Vinyl Acetate
05/05/23 10:301.280.127<0.127µg/m3Vinyl Chloride
05/05/23 10:302.170.157<0.157µg/m3o-Xylene
05/05/23 10:305.650.217<0.217µg/m3m,p-Xylene
05/05/23 10:304-Bromofluorobenzene (S)97.4 70-130
LCS-V32871Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.111.211.9µg/m3Acetone 70-130
87.514.016.0µg/m3Benzene 70-130
94.224.425.9µg/m3Benzyl Chloride 70-130
84.428.333.5µg/m3Bromodichloromethane 70-130
91.847.551.7µg/m3Bromoform 70-130
88.617.219.4µg/m3Bromomethane 70-130
91.810.211.1µg/m31,3-Butadiene 70-130
91.014.215.6µg/m3Carbon Disulfide 70-130
87.627.631.5µg/m3Carbon Tetrachloride 70-130
90.820.923.0µg/m3Chlorobenzene 70-130
89.238.042.6µg/m3Chlorodibromomethane 70-130
87.111.513.2µg/m3Chloroethane 70-130
87.721.424.4µg/m3Chloroform 70-130
93.99.6810.3µg/m3Chloromethane 70-130
83.114.317.2µg/m3Cyclohexane 70-130
Page 8 of 16Date:05/09/2023 04:27 PM
Page 55 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32879QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32871
LCS-V32871Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.033.838.4µg/m31,2-Dibromoethane 70-130
97.329.330.1µg/m31,2-Dichlorobenzene 70-130
95.328.730.1µg/m31,3-Dichlorobenzene 70-130
96.028.930.1µg/m31,4-Dichlorobenzene 70-130
91.422.624.7µg/m3Dichlorodifluoromethane 70-130
89.618.120.2µg/m31,1-Dichloroethane 70-130
87.617.720.2µg/m31,2-Dichloroethane 70-130
89.317.719.8µg/m31,1-Dichloroethene 70-130
90.417.919.8µg/m3cis-1,2-Dichloroethene 70-130
90.918.019.8µg/m3trans-1,2-Dichloroethene 70-130
87.820.323.1µg/m31,2-Dichloropropane 70-130
90.231.635.0µg/m31,2-Dichlorotetrafluoroethane 70-130
90.720.622.7µg/m3cis-1,3-Dichloropropene 70-130
90.720.622.7µg/m3trans-1,3-Dichloropropene 70-130
88.315.918.0µg/m31,4-Dioxane 70-130
84.415.218.0µg/m3Ethyl Acetate 70-130
90.719.721.7µg/m3Ethylbenzene 70-130
91.022.424.6µg/m34-Ethyltoluene 70-130
88.734.038.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
89.718.420.5µg/m3Heptane 70-130
10354.953.3µg/m3Hexachlorobutadiene 70-130
90.315.917.6µg/m3n-Hexane 70-130
89.718.420.5µg/m32-Hexanone 70-130
10112.412.3µg/m3Isopropyl Alcohol 70-130
86.412.814.8µg/m3Methyl Ethyl Ketone (MEK)70-130
90.516.318.0µg/m3Methyl tert-butyl ether (MTBE)70-130
89.218.320.5µg/m34-Methyl-2-Pentanone 70-130
Page 9 of 16Date:05/09/2023 04:27 PM
Page 56 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32879QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32871
LCS-V32871Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.715.117.4µg/m3Methylene Chloride 70-130
96.925.426.2µg/m3Naphthalene 70-130
94.58.148.61µg/m3Propene 70-130
93.419.921.3µg/m3Styrene 70-130
82.728.434.3µg/m31,1,2,2-Tetrachloroethane 70-130
98.833.533.9µg/m3Tetrachloroethene 70-130
89.113.114.7µg/m3Tetrahydrofuran 70-130
91.417.218.8µg/m3Toluene 70-130
10438.737.1µg/m31,2,4-Trichlorobenzene 70-130
86.823.727.3µg/m31,1,1-Trichloroethane 70-130
87.123.827.3µg/m31,1,2-Trichloroethane 70-130
91.424.626.9µg/m3Trichloroethene 70-130
88.925.028.1µg/m3Trichlorofluoromethane 70-130
93.923.124.6µg/m31,2,4-Trimethylbenzene 70-130
92.622.824.6µg/m31,3,5-Trimethylbenzene 70-130
90.916.017.6µg/m3Vinyl Acetate 70-130
91.411.712.8µg/m3Vinyl Chloride 70-130
89.419.421.7µg/m3o-Xylene 70-130
86.837.743.4µg/m3m,p-Xylene 70-130
1014-Bromofluorobenzene (S)70-130
Page 10 of 16Date:05/09/2023 04:27 PM
Page 57 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32931QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32929
Associated Lab Samples: 94717
LRB-V32929 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/08/23 11:014.920.1392.24µg/m3Isopropyl Alcohol
05/08/23 11:014-Bromofluorobenzene (S)93.0 70-130
LCS-V32929Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.711.912.3µg/m3Isopropyl Alcohol 70-130
1024-Bromofluorobenzene (S)70-130
Page 11 of 16Date:05/09/2023 04:27 PM
Page 58 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32966QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32965
Associated Lab Samples: 94716
LRB-V32965 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/09/23 11:284.750.2021.27µg/m3Acetone
05/09/23 11:281.600.073<0.073µg/m3Benzene
05/09/23 11:2810.40.147<0.147µg/m3Benzyl Chloride
05/09/23 11:283.350.150<0.150µg/m3Bromodichloromethane
05/09/23 11:285.170.153<0.153µg/m3Bromoform
05/09/23 11:281.940.115<0.115µg/m3Bromomethane
05/09/23 11:281.110.328<0.328µg/m31,3-Butadiene
05/09/23 11:286.230.0601.37µg/m3Carbon Disulfide
05/09/23 11:283.150.155<0.155µg/m3Carbon Tetrachloride
05/09/23 11:282.300.107<0.107µg/m3Chlorobenzene
05/09/23 11:284.260.208<0.208µg/m3Chlorodibromomethane
05/09/23 11:281.320.164<0.164µg/m3Chloroethane
05/09/23 11:282.440.086<0.086µg/m3Chloroform
05/09/23 11:281.030.067<0.067µg/m3Chloromethane
05/09/23 11:283.440.161<0.161µg/m3Cyclohexane
05/09/23 11:283.840.151<0.151µg/m31,2-Dibromoethane
05/09/23 11:283.010.096<0.096µg/m31,2-Dichlorobenzene
05/09/23 11:2812.00.174<0.174µg/m31,3-Dichlorobenzene
05/09/23 11:283.010.186<0.186µg/m31,4-Dichlorobenzene
05/09/23 11:282.470.134<0.134µg/m3Dichlorodifluoromethane
05/09/23 11:282.020.101<0.101µg/m31,1-Dichloroethane
05/09/23 11:282.020.129<0.129µg/m31,2-Dichloroethane
05/09/23 11:281.980.107<0.107µg/m31,1-Dichloroethene
05/09/23 11:281.980.095<0.095µg/m3cis-1,2-Dichloroethene
05/09/23 11:281.980.108<0.108µg/m3trans-1,2-Dichloroethene
05/09/23 11:282.310.205<0.205µg/m31,2-Dichloropropane
05/09/23 11:283.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane
Page 12 of 16Date:05/09/2023 04:27 PM
Page 59 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32966QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32965
Associated Lab Samples: 94716
LRB-V32965 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/09/23 11:282.270.178<0.178µg/m3cis-1,3-Dichloropropene
05/09/23 11:282.270.178<0.178µg/m3trans-1,3-Dichloropropene
05/09/23 11:281.800.435<0.435µg/m31,4-Dioxane
05/09/23 11:281.800.136<0.136µg/m3Ethyl Acetate
05/09/23 11:282.170.106<0.106µg/m3Ethylbenzene
05/09/23 11:282.460.128<0.128µg/m34-Ethyltoluene
05/09/23 11:283.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane
05/09/23 11:282.050.143<0.143µg/m3Heptane
05/09/23 11:285.330.330<0.330µg/m3Hexachlorobutadiene
05/09/23 11:281.760.047<0.047µg/m3n-Hexane
05/09/23 11:282.050.285<0.285µg/m32-Hexanone
05/09/23 11:284.920.1392.43µg/m3Isopropyl Alcohol
05/09/23 11:281.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK)
05/09/23 11:281.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE)
05/09/23 11:282.050.121<0.121µg/m34-Methyl-2-Pentanone
05/09/23 11:281.740.488<0.488µg/m3Methylene Chloride
05/09/23 11:282.620.183<0.183µg/m3Naphthalene
05/09/23 11:280.8600.242<0.242µg/m3Propene
05/09/23 11:282.130.124<0.124µg/m3Styrene
05/09/23 11:283.430.104<0.104µg/m31,1,2,2-Tetrachloroethane
05/09/23 11:283.390.1811.23µg/m3Tetrachloroethene
05/09/23 11:281.470.107<0.107µg/m3Tetrahydrofuran
05/09/23 11:281.880.090<0.090µg/m3Toluene
05/09/23 11:283.710.209<0.209µg/m31,2,4-Trichlorobenzene
05/09/23 11:282.730.144<0.144µg/m31,1,1-Trichloroethane
05/09/23 11:282.730.087<0.087µg/m31,1,2-Trichloroethane
05/09/23 11:282.150.199<0.199µg/m3Trichloroethene
Page 13 of 16Date:05/09/2023 04:27 PM
Page 60 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32966QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32965
Associated Lab Samples: 94716
LRB-V32965 Matrix: AIRLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/09/23 11:282.810.130<0.130µg/m3Trichlorofluoromethane
05/09/23 11:282.460.110<0.110µg/m31,2,4-Trimethylbenzene
05/09/23 11:282.460.236<0.236µg/m31,3,5-Trimethylbenzene
05/09/23 11:281.760.224<0.224µg/m3Vinyl Acetate
05/09/23 11:281.280.127<0.127µg/m3Vinyl Chloride
05/09/23 11:282.170.157<0.157µg/m3o-Xylene
05/09/23 11:285.650.217<0.217µg/m3m,p-Xylene
05/09/23 11:284-Bromofluorobenzene (S)97.2 70-130
LCS-V32965Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.111.811.9µg/m3Acetone 70-130
95.615.316.0µg/m3Benzene 70-130
10326.625.9µg/m3Benzyl Chloride 70-130
98.833.133.5µg/m3Bromodichloromethane 70-130
10956.351.7µg/m3Bromoform 70-130
94.818.419.4µg/m3Bromomethane 70-130
10111.211.1µg/m31,3-Butadiene 70-130
10115.815.6µg/m3Carbon Disulfide 70-130
95.230.031.5µg/m3Carbon Tetrachloride 70-130
10223.423.0µg/m3Chlorobenzene 70-130
10143.142.6µg/m3Chlorodibromomethane 70-130
96.212.713.2µg/m3Chloroethane 70-130
95.023.224.4µg/m3Chloroform 70-130
11111.410.3µg/m3Chloromethane 70-130
88.915.317.2µg/m3Cyclohexane 70-130
Page 14 of 16Date:05/09/2023 04:27 PM
Page 61 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32966QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32965
LCS-V32965Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.938.038.4µg/m31,2-Dibromoethane 70-130
11233.630.1µg/m31,2-Dichlorobenzene 70-130
11133.430.1µg/m31,3-Dichlorobenzene 70-130
11233.630.1µg/m31,4-Dichlorobenzene 70-130
10626.224.7µg/m3Dichlorodifluoromethane 70-130
97.519.720.2µg/m31,1-Dichloroethane 70-130
93.518.920.2µg/m31,2-Dichloroethane 70-130
96.919.219.8µg/m31,1-Dichloroethene 70-130
98.419.519.8µg/m3cis-1,2-Dichloroethene 70-130
10019.819.8µg/m3trans-1,2-Dichloroethene 70-130
10123.423.1µg/m31,2-Dichloropropane 70-130
10637.235.0µg/m31,2-Dichlorotetrafluoroethane 70-130
10122.922.7µg/m3cis-1,3-Dichloropropene 70-130
10122.922.7µg/m3trans-1,3-Dichloropropene 70-130
10318.518.0µg/m31,4-Dioxane 70-130
92.216.618.0µg/m3Ethyl Acetate 70-130
10122.021.7µg/m3Ethylbenzene 70-130
10024.724.6µg/m34-Ethyltoluene 70-130
96.637.038.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130
11022.620.5µg/m3Heptane 70-130
12767.953.3µg/m3Hexachlorobutadiene 70-130
96.517.017.6µg/m3n-Hexane 70-130
98.020.120.5µg/m32-Hexanone 70-130
10412.812.3µg/m3Isopropyl Alcohol 70-130
95.914.214.8µg/m3Methyl Ethyl Ketone (MEK)70-130
96.117.318.0µg/m3Methyl tert-butyl ether (MTBE)70-130
10020.620.5µg/m34-Methyl-2-Pentanone 70-130
Page 15 of 16Date:05/09/2023 04:27 PM
Page 62 of 68
Quality Control Data
23-114-0003Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
H&A-002
QC Prep Batch Method:
Volatile Organic Compounds in Air- GC/MS
TO-15
V32966QC Analytical Batch(es):
Analysis Method:
Analysis Description:
TO-15 Prep
QC Prep:V32965
LCS-V32965Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.816.517.4µg/m3Methylene Chloride 70-130
10728.026.2µg/m3Naphthalene 70-130
1129.638.61µg/m3Propene 70-130
10121.621.3µg/m3Styrene 70-130
95.332.734.3µg/m31,1,2,2-Tetrachloroethane 70-130
11037.433.9µg/m3Tetrachloroethene 70-130
95.914.114.7µg/m3Tetrahydrofuran 70-130
98.418.518.8µg/m3Toluene 70-130
11944.037.1µg/m31,2,4-Trichlorobenzene 70-130
92.625.327.3µg/m31,1,1-Trichloroethane 70-130
98.927.027.3µg/m31,1,2-Trichloroethane 70-130
10628.626.9µg/m3Trichloroethene 70-130
96.427.128.1µg/m3Trichlorofluoromethane 70-130
10325.424.6µg/m31,2,4-Trimethylbenzene 70-130
10626.124.6µg/m31,3,5-Trimethylbenzene 70-130
93.116.417.6µg/m3Vinyl Acetate 70-130
10613.612.8µg/m3Vinyl Chloride 70-130
10122.021.7µg/m3o-Xylene 70-130
96.742.043.4µg/m3m,p-Xylene 70-130
1034-Bromofluorobenzene (S)70-130
Page 16 of 16Date:05/09/2023 04:27 PM
Page 63 of 68
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-114-0003
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:N/A
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:04/24/2023 11:10:46
Special precautions or instructions included?
Comments:
Page 64 of 68
Page 65 of 68
Page 66 of 68
Page 67 of 68
Page 68 of 68
#=CL#
May 09, 2023
LIMS USE: FR - LORYN SMITH
LIMS OBJECT ID: 92663572
92663572
Project:
Pace Project No.:
RE:
Loryn Smith
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
H&A-002
Dear Loryn Smith:
Enclosed are the analytical results for sample(s) received by the laboratory on April 21, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92663572
H&A-002
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 18
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92663572
H&A-002
Lab ID Sample ID Matrix Date Collected Date Received
92663572001 IDW Solid 04/21/23 11:10 04/21/23 12:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92663572
H&A-002
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92663572001 IDW EPA 6010D 7 PASI-MIP
EPA 7470A 1 PASI-MLMW
EPA 8270E 18 PASI-CPKS
EPA 8260D 14 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663572
H&A-002
Sample: IDW Lab ID: 92663572001 Collected: 04/21/23 11:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3015A
Leachate Method/Date: EPA 1311; 05/07/23 18:00
Pace Analytical Services - Minneapolis
6010D MET ICP, TCLP MICRO
Arsenic ND mg/L 05/09/23 13:04 7440-38-205/08/23 13:350.20 0.0091 1
Barium 0.50 mg/L 05/09/23 13:04 7440-39-305/08/23 13:350.10 0.0067 1
Cadmium 0.0045J mg/L 05/09/23 13:04 7440-43-905/08/23 13:350.030 0.0019 1
Chromium 0.0050J mg/L 05/09/23 13:04 7440-47-305/08/23 13:350.10 0.0043 1
Lead ND mg/L 05/09/23 13:04 7439-92-105/08/23 13:350.10 0.010 1
Selenium 0.016J mg/L 05/09/23 13:04 7782-49-2 B05/08/23 13:350.20 0.0069 1
Silver ND mg/L 05/09/23 13:04 7440-22-405/08/23 13:350.10 0.0041 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 05/07/23 18:00
Pace Analytical Services - Minneapolis
7470A Mercury, TCLP
Mercury ND ug/L 05/09/23 12:00 7439-97-605/08/23 12:570.60 0.29 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 05/03/23 13:42 Initial pH: 4.83; Final pH: 5
Pace Analytical Services - Charlotte
8270E TCLP RVE
1,4-Dichlorobenzene ND ug/L 05/07/23 14:07 106-46-705/06/23 12:3050.0 2.1 1
2,4-Dinitrotoluene ND ug/L 05/07/23 14:07 121-14-205/06/23 12:3050.0 1.2 1
Hexachloro-1,3-butadiene ND ug/L 05/07/23 14:07 87-68-305/06/23 12:3050.0 2.0 1
Hexachlorobenzene ND ug/L 05/07/23 14:07 118-74-105/06/23 12:3050.0 1.7 1
Hexachloroethane ND ug/L 05/07/23 14:07 67-72-105/06/23 12:3050.0 2.0 1
2-Methylphenol(o-Cresol)ND ug/L 05/07/23 14:07 95-48-705/06/23 12:3050.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 05/07/23 14:07 15831-10-405/06/23 12:3050.0 1.2 1
Nitrobenzene ND ug/L 05/07/23 14:07 98-95-305/06/23 12:3050.0 2.1 1
Pentachlorophenol ND ug/L 05/07/23 14:07 87-86-505/06/23 12:30100 2.2 1
Pyridine ND ug/L 05/07/23 14:07 110-86-1 L2,v105/06/23 12:3050.0 3.4 1
2,4,5-Trichlorophenol ND ug/L 05/07/23 14:07 95-95-405/06/23 12:3050.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 05/07/23 14:07 88-06-205/06/23 12:3050.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)113 %05/07/23 14:07 4165-60-005/06/23 12:3010-138 1
2-Fluorobiphenyl (S)86 %05/07/23 14:07 321-60-805/06/23 12:3010-130 1
Terphenyl-d14 (S)112 %05/07/23 14:07 1718-51-005/06/23 12:3019-191 1
Phenol-d6 (S)56 %05/07/23 14:07 13127-88-305/06/23 12:3010-130 1
2-Fluorophenol (S)69 %05/07/23 14:07 367-12-405/06/23 12:3010-130 1
2,4,6-Tribromophenol (S)102 %05/07/23 14:07 118-79-605/06/23 12:3010-164 1
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311; 05/04/23 12:47
Pace Analytical Services - Charlotte
8260D MSV TCLP
Benzene ND ug/L 05/06/23 08:46 71-43-2100 59.8 20
2-Butanone (MEK)ND ug/L 05/06/23 08:46 78-93-3200 158 20
Carbon tetrachloride ND ug/L 05/06/23 08:46 56-23-5 M1100 44.2 20
Chlorobenzene ND ug/L 05/06/23 08:46 108-90-7100 36.0 20
Chloroform ND ug/L 05/06/23 08:46 67-66-3100 56.2 20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92663572
H&A-002
Sample: IDW Lab ID: 92663572001 Collected: 04/21/23 11:10 Received: 04/21/23 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311; 05/04/23 12:47
Pace Analytical Services - Charlotte
8260D MSV TCLP
1,4-Dichlorobenzene ND ug/L 05/06/23 08:46 106-46-7100 38.2 20
1,2-Dichloroethane ND ug/L 05/06/23 08:46 107-06-2100 26.0 20
1,1-Dichloroethene ND ug/L 05/06/23 08:46 75-35-4100 43.0 20
Tetrachloroethene ND ug/L 05/06/23 08:46 127-18-4100 35.6 20
Trichloroethene ND ug/L 05/06/23 08:46 79-01-6100 37.0 20
Vinyl chloride ND ug/L 05/06/23 08:46 75-01-4100 36.2 20
Surrogates
1,2-Dichloroethane-d4 (S)103 %05/06/23 08:46 17060-07-070-130 20
Toluene-d8 (S)102 %05/06/23 08:46 2037-26-570-130 20
4-Bromofluorobenzene (S)99 %05/06/23 08:46 460-00-470-130 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
879852
EPA 7470A
EPA 7470A
7470A Mercury TCLP
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples: 92663572001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4637791
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.60 05/09/23 11:420.29
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4637265
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.60 05/09/23 12:030.29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4637792LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 17.315 115 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4637793MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10651147001
4637794
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L M11511880-120125 6 2015ND17.8 18.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
879850
EPA 3015A
EPA 6010D
6010D MET ICP, TCLP MICRO
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples: 92663572001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4637769
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
Arsenic mg/L 0.012J 0.20 05/09/23 12:360.0091
Barium mg/L 0.0087J 0.10 05/09/23 12:360.0067
Cadmium mg/L ND 0.030 05/09/23 12:360.0019
Chromium mg/L ND 0.10 05/09/23 12:360.0043
Lead mg/L ND 0.10 05/09/23 12:360.010
Selenium mg/L 0.0082J 0.20 05/09/23 12:360.0069
Silver mg/L ND 0.10 05/09/23 12:360.0041
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4637265
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
Arsenic mg/L ND 0.20 05/09/23 12:380.0091
Barium mg/L ND 0.10 05/09/23 12:380.0067
Cadmium mg/L ND 0.030 05/09/23 12:380.0019
Chromium mg/L ND 0.10 05/09/23 12:380.0043
Lead mg/L ND 0.10 05/09/23 12:380.010
Selenium mg/L 0.011J 0.20 05/09/23 12:380.0069
Silver mg/L ND 0.10 05/09/23 12:380.0041
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4637770LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 5.05 100 80-120
Barium mg/L 5.05 100 80-120
Cadmium mg/L 5.25 103 80-120
Chromium mg/L 5.05 100 80-120
Lead mg/L 5.15 101 80-120
Selenium mg/L 5.15 102 80-120
Silver mg/L 2.52.5 99 80-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4637771MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
10651147001
4637772
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/L 5 100 75-12599 1 205ND5.0 5.0
Barium mg/L 5 98 75-12598 0 2050.45 5.3 5.3
Cadmium mg/L 5 101 75-125101 0 205ND5.1 5.0
Chromium mg/L 5 100 75-12599 0 205ND5.0 5.0
Lead mg/L 5 100 75-125100 0 205ND5.0 5.0
Selenium mg/L 5 102 75-125102 1 205ND5.1 5.1
Silver mg/L 2.5 101 75-125100 0 202.5ND 2.5 2.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
772683
EPA 8260D
EPA 8260D
8260D MSV TCLP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663572001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4011097
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
1,1-Dichloroethene ug/L ND 5.0 05/06/23 01:422.2
1,2-Dichloroethane ug/L ND 5.0 05/06/23 01:421.3
1,4-Dichlorobenzene ug/L ND 5.0 05/06/23 01:421.9
2-Butanone (MEK)ug/L ND 10.0 05/06/23 01:427.9
Benzene ug/L ND 5.0 05/06/23 01:423.0
Carbon tetrachloride ug/L ND 5.0 05/06/23 01:422.2
Chlorobenzene ug/L ND 5.0 05/06/23 01:421.8
Chloroform ug/L ND 5.0 05/06/23 01:422.8
Tetrachloroethene ug/L ND 5.0 05/06/23 01:421.8
Trichloroethene ug/L ND 5.0 05/06/23 01:421.8
Vinyl chloride ug/L ND 5.0 05/06/23 01:421.8
1,2-Dichloroethane-d4 (S)%100 70-130 05/06/23 01:42
4-Bromofluorobenzene (S)%102 70-130 05/06/23 01:42
Toluene-d8 (S)%102 70-130 05/06/23 01:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4011096LABORATORY CONTROL SAMPLE:
LCSSpike
1,1-Dichloroethene ug/L 21.320 106 70-130
1,2-Dichloroethane ug/L 21.820 109 70-130
1,4-Dichlorobenzene ug/L 20.720 103 70-130
2-Butanone (MEK)ug/L 43.340 108 70-134
Benzene ug/L 22.520 112 70-130
Carbon tetrachloride ug/L 22.620 113 70-130
Chlorobenzene ug/L 21.020 105 70-130
Chloroform ug/L 18.320 91 70-130
Tetrachloroethene ug/L 20.420 102 70-130
Trichloroethene ug/L 22.920 114 70-130
Vinyl chloride ug/L 16.720 83 62-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4011098MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92663572001
4011099
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 20 121 70-156127 3020NDND ND
1,2-Dichloroethane ug/L 20 109 69-143128 3020NDND ND
1,4-Dichlorobenzene ug/L 20 124 70-142128 3020NDND ND
2-Butanone (MEK)ug/L 40 104 60-157108 3040NDND ND
Benzene ug/L 20 129 70-142122 3020NDND ND
Carbon tetrachloride ug/L M12021770-148227 3020NDND 45.4J
Chlorobenzene ug/L 20 125 70-141137 3020NDND ND
Chloroform ug/L 20 132 70-148131 3020NDND ND
Tetrachloroethene ug/L 20 101 70-14599 3020NDND ND
Trichloroethene ug/L 20 105 62-14695 3020NDND ND
Vinyl chloride ug/L 20 91 61-16381 3020NDND ND
1,2-Dichloroethane-d4 (S) %104 70-130107
4-Bromofluorobenzene (S) %97 70-130100
Toluene-d8 (S)%102 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
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Huntersville, NC 28078
[phone]
Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
772816
EPA 3510C
EPA 8270E
8270E TCLP MSSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92663572001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4007523
Associated Lab Samples:92663572001
Matrix: Water
AnalyzedMDL
1,4-Dichlorobenzene ug/L ND 50.0 05/07/23 11:112.1
2,4,5-Trichlorophenol ug/L ND 50.0 05/07/23 11:111.4
2,4,6-Trichlorophenol ug/L ND 50.0 05/07/23 11:111.5
2,4-Dinitrotoluene ug/L ND 50.0 05/07/23 11:111.2
2-Methylphenol(o-Cresol)ug/L ND 50.0 05/07/23 11:111.2
3&4-Methylphenol(m&p Cresol)ug/L ND 50.0 05/07/23 11:111.2
Hexachloro-1,3-butadiene ug/L ND 50.0 05/07/23 11:112.0
Hexachlorobenzene ug/L ND 50.0 05/07/23 11:111.7
Hexachloroethane ug/L ND 50.0 05/07/23 11:112.0
Nitrobenzene ug/L ND 50.0 05/07/23 11:112.1
Pentachlorophenol ug/L ND 100 05/07/23 11:112.2
Pyridine ug/L ND 50.0 v105/07/23 11:113.4
2,4,6-Tribromophenol (S)%96 10-164 05/07/23 11:11
2-Fluorobiphenyl (S)%77 10-130 05/07/23 11:11
2-Fluorophenol (S)%74 10-130 05/07/23 11:11
Nitrobenzene-d5 (S)%107 10-138 05/07/23 11:11
Phenol-d6 (S)%63 10-130 05/07/23 11:11
Terphenyl-d14 (S)%104 19-191 05/07/23 11:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4011884LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 332500 66 10-130
2,4,5-Trichlorophenol ug/L 496500 99 38-147
2,4,6-Trichlorophenol ug/L 515500 103 34-142
2,4-Dinitrotoluene ug/L 503500 101 44-154
2-Methylphenol(o-Cresol)ug/L 485500 97 31-130
3&4-Methylphenol(m&p Cresol)ug/L 456500 91 30-130
Hexachloro-1,3-butadiene ug/L 444500 89 10-130
Hexachlorobenzene ug/L 426500 85 44-138
Hexachloroethane ug/L 361500 72 10-130
Nitrobenzene ug/L 516500 103 33-133
Pentachlorophenol ug/L 9041000 90 21-163
Pyridine ug/L 68.7 L2,v150014 16-130
2,4,6-Tribromophenol (S)%93 10-164
2-Fluorobiphenyl (S)%88 10-130
2-Fluorophenol (S)%74 10-130
Nitrobenzene-d5 (S)%108 10-138
Phenol-d6 (S)%63 10-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92663572
H&A-002
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4011884LABORATORY CONTROL SAMPLE:
LCSSpike
Terphenyl-d14 (S)%105 19-191
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
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Huntersville, NC 28078
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Page 13 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92663572
H&A-002
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92663572
H&A-002
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92663572001 879850 879912IDWEPA 3015A EPA 6010D
92663572001 879852 880028IDWEPA 7470A EPA 7470A
92663572001 772816 772919IDWEPA 3510C EPA 8270E
92663572001 772683IDWEPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/09/2023 06:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 18
Page 16 of 18
Page 17 of 18
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https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/hoffman & associates/h&a-002 2401
distribution st/brownfields assessment/report/26061- draft brownfields assessment report - piedmont plating.doc
Appendix D

Groundwater and Sub-Slab Soil Gas Sampling Forms

Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERS500 mL1000 mL1500 mL2000 mL2500 mL100 mL/min100 mL/min100 mL/min100 mL/min100 mL/minPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERS4/18/23Pace LES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23
Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft:________________ Depth to Water (ft:___________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:_______________ ftWeather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERSPaceLES4/21/23YSI PP (ES#1363), Hach2100Q (ES#1836)
&Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes:________________________________________________________________________________________________________________________________________________________________________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WH&A-002Ann Marie Lindley60s, sunnyBF-SSV-15995SS Temp Conc4.5Gravel NAFull4/17/23164569Syringe 1 L10.80 ppm Yes14308BF-SSV-211376SS Temp Conc4.5Gravel NAFull4/18/23084554Syringe 1 L10.80 ppm Yes6569BF-SSV-311357SS Temp Conc4.5Gravel NAFull4/18/23092058Syringe 1 L10.4225 ppmYes16216BF-SSV-415813SS Temp Conc4.5Gravel NAFull4/18/23105067Syringe 1 L10.60 ppm Yes16240BF-SSV-511365SS Temp Conc4.5Gravel NAFull4/17/23163569Syringe 1 L11.0875 ppmYes16204BF-SSV-613711SS Temp Conc4.5Gravel NAFull4/17/23152569Syringe 1 L10.40 ppm Yes13142
&Žƌŵ^sͲϭSub-Slab / Soil Gas Vapor Installation Field FormProject No.:__________________ Sampler:______________________Weather:____________________________________________________________Surface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 4/21/2022" Hg = inches of mercury; ppm = parts per millionNotes: ____________________________________________________Sample ID TypeVapor Monitoring Point Construction Helium Leak TestEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)͗ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WH&A-002Ann Marie Lindley60s, sunnyBF-SSV-713691SS Temp Conc4.5Gravel NAFull4/20/23162070 Syringe 1 L10.30 ppm Yes13122BF-SSV-811355SS Temp Conc4.5Gravel NAFull4/20/23160570 Syringe 1 L10.40 ppm Yes16233BF-SSV-DUP13700SS Temp Conc4.5Gravel NAFull4/20/23160570 Syringe 1 L10.40 ppm Yes16233BF-SSV-913697SS Temp Conc4.5Gravel NAFull4/17/23150067Syringe 1 L10.60 ppm Yes14314BF-SSV-1013693SS Temp Conc4.5Gravel NAFull4/17/23154569Syringe 1 L10.70 ppm Yes14327BF-SSV-115992SS Temp Conc4.5Gravel NAFull4/17/23140065Syringe 1 L12.70 ppm Yes16218____________________________________________________________________________________________________________________________________________________________
&Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormDate Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercuryNotes:_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WProject No.: H&A-002 Sampler: Ann Marie LindleyWeather: 60s, sunnyBF-SSV-11L59954/17/2310100 mL/min1700-14693535143081704-51655-2869BF-SSV-21L0855-27.5113764/18/23100900-2054495449100 mL/min65690907-5BF-SSV-30925-281L113574/18/23105823582316216100 mL/min0930-190937-5BF-SSV-41100-27.51L158134/18/23101105-196726672616240100 mL/min1111-5BF-SSV-51627-281L113654/17/23101632-2069356935100 mL/min162041638-5BF-SSV-61L1520-284/17/2313711101525-216931693113142100 mL/min1533-5
&Žƌŵ^sͲϮSub-Slab / Soil Gas Vapor Sampling Field FormDate Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 6/18/2020" Hg = inches of mercury^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sample ID^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗Sampling Information Indoor ParametersOutdoor ParametersSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͗͘ͰhƐĞƌƐͰŵǀĂǁƚĞƌͰƌŽƉďŽdžͰLJKƚŚĞƌͰ&ŽƌŵĚŝƚƐͰ/YͲ^^sͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϭ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WBF-SSV-71L136914/20/2310100 mL/min1638-18.58526--131221644-51633-2870BF-SSV-81L1613-27113554/20/23101618-18852670--100 mL/min162331624-5BF-SSV-DUP1613-271L137004/20/2310852670--16233100 mL/min1618-181624-5BF-SSV-91500-271L136974/17/23101505-186731673114314100 mL/min1512-5BF-SSV-101550-291L136934/17/23101555-1969316931100 mL/min143271602-5BF-SSV-111L1400-274/17/235992101405-186530653016218100 mL/min1411-5Notes:____________________________________________________________________________________________________________________________________________________________________________________________________Project No.: H&A-002 Sampler: Ann Marie LindleyWeather: 60s, sunny
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/hoffman & associates/h&a-002 2401
distribution st/brownfields assessment/report/26061- draft brownfields assessment report - piedmont plating.doc
Appendix E

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Soil Gas- 2401 Distribution Street
North Carolina Department of Environmental Quality
Risk Calculator
Former Piedmont Plating & Anodizing Company
Distribution Street & Dunavant Street
Division of Waste Management - Brownfields Program
H&A-002
January 2023
November 2022 EPA RSL Table
Prepared By:Loryn Smith
Ralph McGee
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas- 2401 Distribution Street
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas- 2401 Distribution Street
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: H&A-002Exposure Unit ID: Soil Gas- 2401 Distribution StreetDescription of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes:CAS NumberChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion27.467-64-1Acetoneug/m31.8371-43-2Benzeneug/m35.0975-15-0Carbon Disulfideug/m30.768108-90-7Chlorobenzeneug/m32.4267-66-3Chloroformug/m32.41110-82-7Cyclohexaneug/m30.66195-50-1Dichlorobenzene, 1,2-ug/m31.42106-46-7Dichlorobenzene, 1,4-ug/m32.8775-71-8Dichlorodifluoromethaneug/m30.742141-78-6Ethyl Acetateug/m38.03100-41-4Ethylbenzeneug/m30.99109-99-9~Tetrahydrofuranug/m31.4142-82-5Heptane, N-ug/m32.54110-54-3Hexane, N-ug/m339.667-63-0Isopropanolug/m34.3678-93-3Methyl Ethyl Ketone (2-Butanone)ug/m30.643108-10-1Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m313.375-09-2Methylene Chlorideug/m35.5991-20-3~Naphthaleneug/m35.31115-07-1Propyleneug/m36.78100-42-5Styreneug/m331.3127-18-4Tetrachloroethyleneug/m318.6108-88-3Tolueneug/m30.56776-13-1Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m39.4379-01-6Trichloroethyleneug/m32.3775-69-4Trichlorofluoromethaneug/m351.795-63-6Trimethylbenzene, 1,2,4-ug/m312.2108-67-8Trimethylbenzene, 1,3,5-ug/m348.71330-20-7Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas- 2401 Distribution Street
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.8E-06 2.7E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.8E-07 2.1E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas- 2401 Distribution Street
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 27.4 0.822 --
71-43-2 Benzene 1.83 0.0549 3.6E-01 6.3E+00 1.5E-07 1.8E-03
75-15-0 Carbon Disulfide 5.09 0.1527 -1.5E+02 2.1E-04
108-90-7 Chlorobenzene 0.768 0.02304 -1.0E+01 4.4E-04
67-66-3 Chloroform 2.42 0.0726 1.2E-01 2.0E+01 5.9E-07 7.1E-04
110-82-7 Cyclohexane 2.41 0.0723 -1.3E+03 1.2E-05
95-50-1 Dichlorobenzene, 1,2-0.661 0.01983 -4.2E+01 9.5E-05
106-46-7 Dichlorobenzene, 1,4-1.42 0.0426 2.6E-01 1.7E+02 1.7E-07 5.1E-05
75-71-8 Dichlorodifluoromethane 2.87 0.0861 -2.1E+01 8.3E-04
141-78-6 Ethyl Acetate 0.742 0.02226 -1.5E+01 3.0E-04
100-41-4 Ethylbenzene 8.03 0.2409 1.1E+00 2.1E+02 2.1E-07 2.3E-04
109-99-9 ~Tetrahydrofuran 0.99 0.0297 -4.2E+02 1.4E-05
142-82-5 Heptane, N-1.4 0.042 -8.3E+01 1.0E-04
110-54-3 Hexane, N-2.54 0.0762 -1.5E+02 1.0E-04
67-63-0 Isopropanol 39.6 1.188 -4.2E+01 5.7E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)4.36 0.1308 -1.0E+03 2.5E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 0.643 0.01929 -6.3E+02 6.2E-06
75-09-2 Methylene Chloride 13.3 0.399 1.0E+02 1.3E+02 3.9E-09 6.4E-04
91-20-3 ~Naphthalene 5.59 0.1677 8.3E-02 6.3E-01 2.0E-06 5.4E-02
115-07-1 Propylene 5.31 0.1593 -6.3E+02 5.1E-05
100-42-5 Styrene 6.78 0.2034 -2.1E+02 2.0E-04
127-18-4 Tetrachloroethylene 31.3 0.939 1.1E+01 8.3E+00 8.7E-08 2.3E-02
108-88-3 Toluene 18.6 0.558 -1.0E+03 1.1E-04
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.567 0.01701 -1.0E+03 3.3E-06
79-01-6 Trichloroethylene 9.43 0.2829 4.8E-01 4.2E-01 5.9E-07 1.4E-01
75-69-4 Trichlorofluoromethane 2.37 0.0711 --
95-63-6 Trimethylbenzene, 1,2,4-51.7 1.551 -1.3E+01 2.5E-02
108-67-8 Trimethylbenzene, 1,3,5-12.2 0.366 -1.3E+01 5.8E-03
1330-20-7 Xylenes 48.7 1.461 -2.1E+01 1.4E-02
Cumulative: 3.8E-06 2.7E-01
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas- 2401 Distribution Street
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 27.4 0.274 --
71-43-2 Benzene 1.83 0.0183 1.6E+00 2.6E+01 1.2E-08 1.4E-04
75-15-0 Carbon Disulfide 5.09 0.0509 -6.1E+02 1.7E-05
108-90-7 Chlorobenzene 0.768 0.00768 -4.4E+01 3.5E-05
67-66-3 Chloroform 2.42 0.0242 5.3E-01 8.6E+01 4.5E-08 5.6E-05
110-82-7 Cyclohexane 2.41 0.0241 -5.3E+03 9.2E-07
95-50-1 Dichlorobenzene, 1,2-0.661 0.00661 -1.8E+02 7.5E-06
106-46-7 Dichlorobenzene, 1,4-1.42 0.0142 1.1E+00 7.0E+02 1.3E-08 4.1E-06
75-71-8 Dichlorodifluoromethane 2.87 0.0287 -8.8E+01 6.6E-05
141-78-6 Ethyl Acetate 0.742 0.00742 -6.1E+01 2.4E-05
100-41-4 Ethylbenzene 8.03 0.0803 4.9E+00 8.8E+02 1.6E-08 1.8E-05
109-99-9 ~Tetrahydrofuran 0.99 0.0099 -1.8E+03 1.1E-06
142-82-5 Heptane, N-1.4 0.014 -3.5E+02 8.0E-06
110-54-3 Hexane, N-2.54 0.0254 -6.1E+02 8.3E-06
67-63-0 Isopropanol 39.6 0.396 -1.8E+02 4.5E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)4.36 0.0436 -4.4E+03 2.0E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 0.643 0.00643 -2.6E+03 4.9E-07
75-09-2 Methylene Chloride 13.3 0.133 1.2E+03 5.3E+02 1.1E-10 5.1E-05
91-20-3 ~Naphthalene 5.59 0.0559 3.6E-01 2.6E+00 1.5E-07 4.3E-03
115-07-1 Propylene 5.31 0.0531 -2.6E+03 4.0E-06
100-42-5 Styrene 6.78 0.0678 -8.8E+02 1.5E-05
127-18-4 Tetrachloroethylene 31.3 0.313 4.7E+01 3.5E+01 6.6E-09 1.8E-03
108-88-3 Toluene 18.6 0.186 -4.4E+03 8.5E-06
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.567 0.00567 -4.4E+03 2.6E-07
79-01-6 Trichloroethylene 9.43 0.0943 3.0E+00 1.8E+00 3.2E-08 1.1E-02
75-69-4 Trichlorofluoromethane 2.37 0.0237 --
95-63-6 Trimethylbenzene, 1,2,4-51.7 0.517 -5.3E+01 2.0E-03
108-67-8 Trimethylbenzene, 1,3,5-12.2 0.122 -5.3E+01 4.6E-04
1330-20-7 Xylenes 48.7 0.487 -8.8E+01 1.1E-03
Cumulative: 2.8E-07 2.1E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Loryn Smith
Ralph McGee
Soil Gas - 2322 Dunavant Street
North Carolina Department of Environmental Quality
Risk Calculator
Former Piedmont Plating & Anodizing Company
Distribution Street & Dunavant Street
Division of Waste Management - Brownfields Program
H&A-002
January 2023
November 2022 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2322 Dunavant Street
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2322 Dunavant Street
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: H&A-002Exposure Unit ID: Soil Gas - 2322 Dunavant StreetDescription of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes:CAS NumberChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion71.167-64-1Acetoneug/m30.60671-43-2Benzeneug/m35.0175-15-0Carbon Disulfideug/m30.79567-66-3Chloroformug/m32.02110-82-7Cyclohexaneug/m32.7775-71-8Dichlorodifluoromethaneug/m30.673123-91-1Dioxane, 1,4-ug/m30.668100-41-4Ethylbenzeneug/m320.1109-99-9~Tetrahydrofuranug/m31.07142-82-5Heptane, N-ug/m30.877110-54-3Hexane, N-ug/m30.688591-78-6Hexanone, 2-ug/m322.767-63-0Isopropanolug/m318.878-93-3Methyl Ethyl Ketone (2-Butanone)ug/m31.32108-10-1Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m318.775-09-2Methylene Chlorideug/m34.8391-20-3~Naphthaleneug/m32.77115-07-1Propyleneug/m35.47100-42-5Styreneug/m319.6127-18-4Tetrachloroethyleneug/m33.32108-88-3Tolueneug/m38.3879-01-6Trichloroethyleneug/m31.9375-69-4Trichlorofluoromethaneug/m314.695-63-6Trimethylbenzene, 1,2,4-ug/m33.11108-67-8Trimethylbenzene, 1,3,5-ug/m38.831330-20-7Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2322 Dunavant Street
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.6E-06 2.0E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.9E-07 1.6E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2322 Dunavant Street
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 71.1 2.133 --
71-43-2 Benzene 0.606 0.01818 3.6E-01 6.3E+00 5.1E-08 5.8E-04
75-15-0 Carbon Disulfide 5.01 0.1503 -1.5E+02 2.1E-04
67-66-3 Chloroform 0.795 0.02385 1.2E-01 2.0E+01 2.0E-07 2.3E-04
110-82-7 Cyclohexane 2.02 0.0606 -1.3E+03 9.7E-06
75-71-8 Dichlorodifluoromethane 2.77 0.0831 -2.1E+01 8.0E-04
123-91-1 Dioxane, 1,4-0.673 0.02019 5.6E-01 6.3E+00 3.6E-08 6.5E-04
100-41-4 Ethylbenzene 0.668 0.02004 1.1E+00 2.1E+02 1.8E-08 1.9E-05
109-99-9 ~Tetrahydrofuran 20.1 0.603 -4.2E+02 2.9E-04
142-82-5 Heptane, N-1.07 0.0321 -8.3E+01 7.7E-05
110-54-3 Hexane, N-0.877 0.02631 -1.5E+02 3.6E-05
591-78-6 Hexanone, 2-0.688 0.02064 -6.3E+00 6.6E-04
67-63-0 Isopropanol 22.7 0.681 -4.2E+01 3.3E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)18.8 0.564 -1.0E+03 1.1E-04
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 1.32 0.0396 -6.3E+02 1.3E-05
75-09-2 Methylene Chloride 18.7 0.561 1.0E+02 1.3E+02 5.5E-09 9.0E-04
91-20-3 ~Naphthalene 4.83 0.1449 8.3E-02 6.3E-01 1.8E-06 4.6E-02
115-07-1 Propylene 2.77 0.0831 -6.3E+02 2.7E-05
100-42-5 Styrene 5.47 0.1641 -2.1E+02 1.6E-04
127-18-4 Tetrachloroethylene 19.6 0.588 1.1E+01 8.3E+00 5.4E-08 1.4E-02
108-88-3 Toluene 3.32 0.0996 -1.0E+03 1.9E-05
79-01-6 Trichloroethylene 8.38 0.2514 4.8E-01 4.2E-01 5.3E-07 1.2E-01
75-69-4 Trichlorofluoromethane 1.93 0.0579 --
95-63-6 Trimethylbenzene, 1,2,4-14.6 0.438 -1.3E+01 7.0E-03
108-67-8 Trimethylbenzene, 1,3,5-3.11 0.0933 -1.3E+01 1.5E-03
1330-20-7 Xylenes 8.83 0.2649 -2.1E+01 2.5E-03
Cumulative: 2.6E-06 2.0E-01
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2322 Dunavant Street
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 71.1 0.711 --
71-43-2 Benzene 0.606 0.00606 1.6E+00 2.6E+01 3.9E-09 4.6E-05
75-15-0 Carbon Disulfide 5.01 0.0501 -6.1E+02 1.6E-05
67-66-3 Chloroform 0.795 0.00795 5.3E-01 8.6E+01 1.5E-08 1.9E-05
110-82-7 Cyclohexane 2.02 0.0202 -5.3E+03 7.7E-07
75-71-8 Dichlorodifluoromethane 2.77 0.0277 -8.8E+01 6.3E-05
123-91-1 Dioxane, 1,4-0.673 0.00673 2.5E+00 2.6E+01 2.7E-09 5.1E-05
100-41-4 Ethylbenzene 0.668 0.00668 4.9E+00 8.8E+02 1.4E-09 1.5E-06
109-99-9 ~Tetrahydrofuran 20.1 0.201 -1.8E+03 2.3E-05
142-82-5 Heptane, N-1.07 0.0107 -3.5E+02 6.1E-06
110-54-3 Hexane, N-0.877 0.00877 -6.1E+02 2.9E-06
591-78-6 Hexanone, 2-0.688 0.00688 -2.6E+01 5.2E-05
67-63-0 Isopropanol 22.7 0.227 -1.8E+02 2.6E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)18.8 0.188 -4.4E+03 8.6E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 1.32 0.0132 -2.6E+03 1.0E-06
75-09-2 Methylene Chloride 18.7 0.187 1.2E+03 5.3E+02 1.5E-10 7.1E-05
91-20-3 ~Naphthalene 4.83 0.0483 3.6E-01 2.6E+00 1.3E-07 3.7E-03
115-07-1 Propylene 2.77 0.0277 -2.6E+03 2.1E-06
100-42-5 Styrene 5.47 0.0547 -8.8E+02 1.2E-05
127-18-4 Tetrachloroethylene 19.6 0.196 4.7E+01 3.5E+01 4.2E-09 1.1E-03
108-88-3 Toluene 3.32 0.0332 -4.4E+03 1.5E-06
79-01-6 Trichloroethylene 8.38 0.0838 3.0E+00 1.8E+00 2.8E-08 9.6E-03
75-69-4 Trichlorofluoromethane 1.93 0.0193 --
95-63-6 Trimethylbenzene, 1,2,4-14.6 0.146 -5.3E+01 5.6E-04
108-67-8 Trimethylbenzene, 1,3,5-3.11 0.0311 -5.3E+01 1.2E-04
1330-20-7 Xylenes 8.83 0.0883 -8.8E+01 2.0E-04
Cumulative: 1.9E-07 1.6E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Soil Gas - 2400-2406 Dunavant Street
North Carolina Department of Environmental Quality
Risk Calculator
Former Piedmont Plating & Anodizing Company
Distribution Street & Dunavant Street
Division of Waste Management - Brownfields Program
H&A-002
January 2023
November 2022 EPA RSL Table
Prepared By:Loryn Smith
Ralph McGee
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2400-2406 Dunavant Street
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2400-2406 Dunavant Street
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: H&A-002Exposure Unit ID: Soil Gas - 2400-2406 Dunavant StreetDescription of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes:CAS NumberChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion42.567-64-1Acetoneug/m321.871-43-2Benzeneug/m321.575-15-0Carbon Disulfideug/m32.71108-90-7Chlorobenzeneug/m31.1467-66-3Chloroformug/m35.82110-82-7Cyclohexaneug/m30.84195-50-1Dichlorobenzene, 1,2-ug/m31.95106-46-7Dichlorobenzene, 1,4-ug/m340.275-71-8Dichlorodifluoromethaneug/m35.69141-78-6Ethyl Acetateug/m326.2100-41-4Ethylbenzeneug/m30.867109-99-9~Tetrahydrofuranug/m39.45142-82-5Heptane, N-ug/m35.69591-78-6Hexanone, 2-ug/m352.867-63-0Isopropanolug/m330.878-93-3Methyl Ethyl Ketone (2-Butanone)ug/m34.51108-10-1Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m34.9475-09-2Methylene Chlorideug/m340.591-20-3~Naphthaleneug/m37.56115-07-1Propyleneug/m38.39100-42-5Styreneug/m34.2479-34-5Tetrachloroethane, 1,1,2,2-ug/m35.67127-18-4Tetrachloroethyleneug/m3149108-88-3Tolueneug/m311.779-01-6Trichloroethyleneug/m33.9975-69-4Trichlorofluoromethaneug/m33295-63-6Trimethylbenzene, 1,2,4-ug/m312.4108-67-8Trimethylbenzene, 1,3,5-ug/m3138.31330-20-7Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2400-2406 Dunavant Street
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.1E-05 6.8E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.6E-06 5.4E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2400-2406 Dunavant Street
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 42.5 1.275 --
71-43-2 Benzene 21.8 0.654 3.6E-01 6.3E+00 1.8E-06 2.1E-02
75-15-0 Carbon Disulfide 21.5 0.645 -1.5E+02 8.8E-04
108-90-7 Chlorobenzene 2.71 0.0813 -1.0E+01 1.6E-03
67-66-3 Chloroform 1.14 0.0342 1.2E-01 2.0E+01 2.8E-07 3.3E-04
110-82-7 Cyclohexane 5.82 0.1746 -1.3E+03 2.8E-05
95-50-1 Dichlorobenzene, 1,2-0.841 0.02523 -4.2E+01 1.2E-04
106-46-7 Dichlorobenzene, 1,4-1.95 0.0585 2.6E-01 1.7E+02 2.3E-07 7.0E-05
75-71-8 Dichlorodifluoromethane 40.2 1.206 -2.1E+01 1.2E-02
141-78-6 Ethyl Acetate 5.69 0.1707 -1.5E+01 2.3E-03
100-41-4 Ethylbenzene 26.2 0.786 1.1E+00 2.1E+02 7.0E-07 7.5E-04
109-99-9 ~Tetrahydrofuran 0.867 0.02601 -4.2E+02 1.2E-05
142-82-5 Heptane, N-9.45 0.2835 -8.3E+01 6.8E-04
591-78-6 Hexanone, 2-5.69 0.1707 -6.3E+00 5.5E-03
67-63-0 Isopropanol 52.8 1.584 -4.2E+01 7.6E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)30.8 0.924 -1.0E+03 1.8E-04
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 4.51 0.1353 -6.3E+02 4.3E-05
75-09-2 Methylene Chloride 4.94 0.1482 1.0E+02 1.3E+02 1.5E-09 2.4E-04
91-20-3 ~Naphthalene 40.5 1.215 8.3E-02 6.3E-01 1.5E-05 3.9E-01
115-07-1 Propylene 7.56 0.2268 -6.3E+02 7.2E-05
100-42-5 Styrene 8.39 0.2517 -2.1E+02 2.4E-04
79-34-5 Tetrachloroethane, 1,1,2,2-4.24 0.1272 4.8E-02 -2.6E-06
127-18-4 Tetrachloroethylene 5.67 0.1701 1.1E+01 8.3E+00 1.6E-08 4.1E-03
108-88-3 Toluene 149 4.47 -1.0E+03 8.6E-04
79-01-6 Trichloroethylene 11.7 0.351 4.8E-01 4.2E-01 7.3E-07 1.7E-01
75-69-4 Trichlorofluoromethane 3.99 0.1197 --
95-63-6 Trimethylbenzene, 1,2,4-32 0.96 -1.3E+01 1.5E-02
108-67-8 Trimethylbenzene, 1,3,5-12.4 0.372 -1.3E+01 5.9E-03
1330-20-7 Xylenes 138.3 4.149 -2.1E+01 4.0E-02
Cumulative: 2.1E-05 6.8E-01
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: H&A-002
Exposure Unit ID: Soil Gas - 2400-2406 Dunavant Street
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 42.5 0.425 --
71-43-2 Benzene 21.8 0.218 1.6E+00 2.6E+01 1.4E-07 1.7E-03
75-15-0 Carbon Disulfide 21.5 0.215 -6.1E+02 7.0E-05
108-90-7 Chlorobenzene 2.71 0.0271 -4.4E+01 1.2E-04
67-66-3 Chloroform 1.14 0.0114 5.3E-01 8.6E+01 2.1E-08 2.7E-05
110-82-7 Cyclohexane 5.82 0.0582 -5.3E+03 2.2E-06
95-50-1 Dichlorobenzene, 1,2-0.841 0.00841 -1.8E+02 9.6E-06
106-46-7 Dichlorobenzene, 1,4-1.95 0.0195 1.1E+00 7.0E+02 1.7E-08 5.6E-06
75-71-8 Dichlorodifluoromethane 40.2 0.402 -8.8E+01 9.2E-04
141-78-6 Ethyl Acetate 5.69 0.0569 -6.1E+01 1.9E-04
100-41-4 Ethylbenzene 26.2 0.262 4.9E+00 8.8E+02 5.3E-08 6.0E-05
109-99-9 ~Tetrahydrofuran 0.867 0.00867 -1.8E+03 9.9E-07
142-82-5 Heptane, N-9.45 0.0945 -3.5E+02 5.4E-05
591-78-6 Hexanone, 2-5.69 0.0569 -2.6E+01 4.3E-04
67-63-0 Isopropanol 52.8 0.528 -1.8E+02 6.0E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)30.8 0.308 -4.4E+03 1.4E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 4.51 0.0451 -2.6E+03 3.4E-06
75-09-2 Methylene Chloride 4.94 0.0494 1.2E+03 5.3E+02 4.0E-11 1.9E-05
91-20-3 ~Naphthalene 40.5 0.405 3.6E-01 2.6E+00 1.1E-06 3.1E-02
115-07-1 Propylene 7.56 0.0756 -2.6E+03 5.8E-06
100-42-5 Styrene 8.39 0.0839 -8.8E+02 1.9E-05
79-34-5 Tetrachloroethane, 1,1,2,2-4.24 0.0424 2.1E-01 - 2.0E-07
127-18-4 Tetrachloroethylene 5.67 0.0567 4.7E+01 3.5E+01 1.2E-09 3.2E-04
108-88-3 Toluene 149 1.49 -4.4E+03 6.8E-05
79-01-6 Trichloroethylene 11.7 0.117 3.0E+00 1.8E+00 3.9E-08 1.3E-02
75-69-4 Trichlorofluoromethane 3.99 0.0399 --
95-63-6 Trimethylbenzene, 1,2,4-32 0.32 -5.3E+01 1.2E-03
108-67-8 Trimethylbenzene, 1,3,5-12.4 0.124 -5.3E+01 4.7E-04
1330-20-7 Xylenes 138.3 1.383 -8.8E+01 3.2E-03
Cumulative: 1.6E-06 5.4E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator