RA-682_3873_CA_MRP_20230317

FGHGHFGHFG
FALCON ENGINEERING, INC. / 1210 TRINITY ROAD, SUITE 110 CARY, NC 27513 / P: 919-871-0800 / WWW.FALCONENGINEERS.COM
March 17, 2023
Scott Ryals
NCDEQ Underground Storage Tank Section
217 West Jones Street
Raleigh, North Carolina 27603
Re: Soil Sampling Letter Report
Former MS Solomon Yard
965 Blalock Dairy Road
Roxboro, Person County, North Carolina 27574
UST Incident Number: 3873
Project No: G22036.05

Scott,

Falcon has completed the requested soil sampling at the Former MS Solomon Yard UST (Incident No. 3873).
Falcon collected ten soil samples (samples S1 through S10) via hand auger on February 14, 2003. Hand augers
were performed to a depth of five feet below ground surface (BGS). Falcon staff bagged composite soil samples
of each hand auger in approximately 2.5-foot sections and scanned them with a Photoionization detector (PID).
PID scans of the ten soil samples did not register above 0.2 parts per million. Samples were taken from the first
2.5 feet BGS and analyzed for semi-volatile organic compounds via method 8270.
Nine contaminants were identified in sample S4 (Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene,
Benzo(g,h,i)perylene, Benzo(k)fluoranthene, Chrysene, Fluoranthene, Indeno(1,2,3-cd)pyrene, and Pyrene. The
nine contaminants were “J-flagged” indicating they are estimated values. Ben-zo(a)pyrene was identified at
0.321J mg/kg. (milligrams per kilogram) which is above the soil-to-groundwater MSCC (Maximum Soil
Contaminant Concentration) of 0.096 mg/kg and the Residential MSCC of 0.088 mg/kg but below the
Industrial/Commercial MSCCs of 0.78 mg/kg. The remining eight contaminants were below their respective
Soil-to-Groundwater, Residential and Industrial/commercial MSCCs. Constituents above method detection
limits were not identified in the remaining nine soil samples. Please see the attached Table B-3: Summary of
Soil Sampling Results, USGS Topographic Map, Site Map, Hand Auger Map, Photographs, and Laboratory
Data.
SOIL SAMPLIN LETTER REPORT

NC DEQ UST SECTION / MS SOLOMON YARD NO. 3873/ G22036.05 / MARCH 17, 2023 2

Sampling was in general accordance with the NC Department of Environmental Quality (DEQ) Division of
Waste Management’s (DWM) “Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement
for UST Releases” (May 17, 2021 Version Change 11–2021) guidance document. The sampling strategy was
derived based upon the project scope and objectives as outlined above. The sample was sent to Waypoint
Analytical for analysis. Appropriate sterile containers were received by Falcon from Waypoint prior to
beginning the fieldwork. Sample containers were labeled appropriately.
A Minirae 3000 PID was used to field screen samples for volatile organics to determine if a release had occurred.
A composite sample of the first 2.5 feet was collected for analysis. The PID was calibrated per manufacturer
instructions prior to use. Representative samples were placed in a sealed plastic bag for approximately 10
minutes to allow soil hydrocarbons to reach equilibrium within the headspace prior to scanning with the PID.
One sample per boring was collected from the depth of the proposed cut or from the section above the depth
of cut with the highest PID reading.
To avoid cross contamination, a new unused pair of non-powdered nitrile gloves was worn while extracting
each sample. Samples were placed in the appropriate laboratory provided containers. The labels on each
container were then completed so that each provided the date and time of sampling, method of analysis, sample
collector, preservative used and sampling location identification. Samples were placed in an ice-filled cooler and
transported to the lab. Appropriate chain-of-custody procedures, including the completion of necessary forms,
were followed.
Please review and advise us if you have any questions or concerns. We appreciate this opportunity to provide
services to you and look forward to partnering with you on future projects. If you have any questions, please
give Falcon a call at [phone].
Sincerely,
FALCON ENGINEERING, INC.

Christopher J. Burkhardt Jeremy R. Hamm, PE Environmental Services Manager Geotechnical Services Manager
Enclosures:
Site Location Map, Hand Auger Location Map, Photographs, Laboratory Data
SOIL SAMPLIN LETTER REPORT

NC DEQ UST SECTION / MS SOLOMON YARD NO. 3873/ G22036.05 / MARCH 17, 2023 3

TABLE B-3: SUMMARY OF SOIL SAMPLING RESULTS
Revision Date: Incident Number and Name: 3873 Former MS Solomon Yard Facility ID#: Unknown

Analytical Method (e.g., VOC by EPA 8260) -> 8270 8270 8270 8270 8270 8270 8270 8270 8270
Contaminant of Concern -> Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Fluoranthene Indeno(1,2,3-cd)pyrene Pyrene Sample ID
Date Collected (mm/dd/yy)
Source Area (e.g., Tank Pit)
Sample Depth (ft BGS)
Incident Phase (IAA, LSA, etc.)
S1 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S2 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S34 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S4 02/14/2023 YARD 0-2.5 LSA 0.288J 0.321J 0.527J 0.263J 0.183J 0.288J 0.432J 0.285J 0.423J
S5 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S6 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S7 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S8 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S9 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
S10 02/14/2023 YARD 0-2.5 LSA < < < < < < < < <
Minimum Reporting Limit (mg/kg) 0.169 0.179 0.177 0.165 0.166 0.172 0.149 0.218 0.463
Soil to Groundwater MSCC (mg/kg) 0.35 0.096 1.2 6400 12 39 290 3.4 270
Residential MSCC (mg/kg) 0.88 0.088 0.88 469 9 88 620 0.88 469
Industrial/Commercial MSCC (mg/kg) 8 0.78 8 12264 78 780 16400 8 12264
Detection limits for contaminants not detected are indicated by a < symbol (e.g., < 1, 10, 42) MSCC = maximum soil contaminant concentration ft. BGS = feet below ground surface Results are reported in mg/kg. (milligrams per kilogram) J= estimated value Bold = concentration is above the Soil to Groundwater MSCC
Former MS Solomon Yard
Soil Sampling
USGS Topo Map “Hurdle Mills, NC” 2022
Project No.:G22036.05Date: March 2023Source: USGS TopoView Website: https://ngmdb.usgs.gov/topoview/
Former MS Solomon Yard
Soil Sampling
Site Map
Project No.:G22036.05Date: March 2023Source:Person County GIS website:https://www.personcountync.gov/government/departments-a-h/gis
Former MS Solomon Yard
Soil Sampling
Hand Auger Map
Project No.:G22036.05Date: March 2023Source:Google Earth 2022 Aerial Photograph
Former MS Solomon Yard
Soil Sampling
Site Photographs
Project No.:G22036.05Date: March 2023
Photograph No: 1: General view looking east toward the site.
Photograph No: 2: General view looking south toward the site.
Former MS Solomon Yard
Soil Sampling
Site Photographs
Project No.:G22036.05Date: March 2023
Photograph No: 3: General view looking north toward the site.
Photograph No: General view of the pond.

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

2/27/2023
Falcon Engineering Christopher Burkhardt
1210 Trinity Road Suite 110
Cary, NC, 27513
Ref: Analytical Testing Lab Report Number: 23-047-0008
Client Project Description: Solomon
Dear Christopher Burkhardt:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 2/16/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 68
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/23-047-0008
Page 2 of 68
Report Number:
Sample Summary Table
Client Project Description:
23-047-0008
Solomon
Lab No Client Sample ID Matrix Date Collected Date Received
02/14/2023 14:28Solids 99875 S1 02/16/2023 11:30
02/14/2023 14:31Solids 99876 S2 02/16/2023 11:30
02/14/2023 14:36Solids 99877 S3 02/16/2023 11:30
02/14/2023 14:40Solids 99878 S4 02/16/2023 11:30
02/14/2023 14:44Solids 99879 S5 02/16/2023 11:30
02/14/2023 14:49Solids 99880 S6 02/16/2023 11:30
02/14/2023 14:52Solids 99881 S7 02/16/2023 11:30
02/14/2023 14:55Solids 99882 S8 02/16/2023 11:30
02/14/2023 14:59Solids 99883 S9 02/16/2023 11:30
02/14/2023 15:01Solids 99884 S10 02/16/2023 11:30
Page 3 of 68
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-047-0008
Report Limit
Project:Solomon
V 99875S1
18.5 02/16/2023 16:10SW-DRYWT Moisture %
V 99876S2
19.1 02/16/2023 16:10SW-DRYWT Moisture %
V 99877S3
27.8 02/16/2023 16:10SW-DRYWT Moisture %
V 99878S4
J0.288 02/22/2023 19:148270EBenzo(a)anthracene mg/Kg - dry 0.169
J0.321 02/22/2023 19:148270EBenzo(a)pyrene mg/Kg - dry 0.179
J0.527 02/22/2023 19:148270EBenzo(b)fluoranthene mg/Kg - dry 0.177
J0.263 02/22/2023 19:148270EBenzo(g,h,i)perylene mg/Kg - dry 0.165
J0.183 02/22/2023 19:148270EBenzo(k)fluoranthene mg/Kg - dry 0.166
J0.288 02/22/2023 19:148270EChrysenemg/Kg - dry 0.172
J0.432 02/22/2023 19:148270EFluoranthenemg/Kg - dry 0.149
J0.285 02/22/2023 19:148270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.218
J0.423 02/22/2023 19:148270EPyrenemg/Kg - dry 0.163
17.9 02/16/2023 16:10SW-DRYWT Moisture %
V 99879S5
13.1 02/16/2023 16:10SW-DRYWT Moisture %
V 99880S6
14.9 02/17/2023 10:20SW-DRYWT Moisture %
V 99881S7
15.4 02/17/2023 10:20SW-DRYWT Moisture %
V 99882S8
20.0 02/17/2023 10:20SW-DRYWT Moisture %
V 99883S9
19.8 02/17/2023 10:20SW-DRYWT Moisture %
V 99884S10
13.5 02/17/2023 10:20SW-DRYWT Moisture %
Page 4 of 68

Client: Falcon Engineering CASE NARRATIVE
Project: Solomon Lab Report Number: 23-047-0008
Date: 2/24/2023
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 99866 (SB-8-25') Analyte: 2,4-Dinitrophenol
QC Batch No: V30112/V30032 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 99866 (SB-8-25')
Analyte: 3,3`-Dichlorobenzidine QC Batch No: V30112/V30032
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 99866 (SB-8-25') Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V30112/V30032 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Aniline
QC Batch No: V30112/V30032 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Sample 99866 (SB-8-25')
Analyte: Benzoic Acid QC Batch No: V30112/V30032
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.

Page 5 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S1
99875 Matrix:
2/14/2023 14:28
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.5 %Moisture 1 02/16/23 16:10 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S1
99875 Matrix:
2/14/2023 14:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.142 mg/Kg - dry 0.142 0.809Acenaphthene 1 02/22/23 18:06 V30112JMV
<0.128 mg/Kg - dry 0.128 0.809
Acenaphthylene 1 02/22/23 18:06 V30112JMV
<0.186 mg/Kg - dry 0.186 0.809Aniline 1 02/22/23 18:06 V30112JMV
<0.175 mg/Kg - dry 0.175 0.809Anthracene 1 02/22/23 18:06 V30112JMV
<0.170 mg/Kg - dry 0.170 0.809Benzo(a)anthracene 1 02/22/23 18:06 V30112JMV
<0.180 mg/Kg - dry 0.180 0.809Benzo(a)pyrene 1 02/22/23 18:06 V30112JMV
<0.179 mg/Kg - dry 0.179 0.809Benzo(b)fluoranthene 1 02/22/23 18:06 V30112JMV
<0.166 mg/Kg - dry 0.166 0.809Benzo(g,h,i)perylene 1 02/22/23 18:06 V30112JMV
<0.168 mg/Kg - dry 0.168 0.809
Benzo(k)fluoranthene 1 02/22/23 18:06 V30112JMV
<0.711 mg/Kg - dry 0.711 2.45Benzoic Acid 1 02/22/23 18:06 V30112JMV
<0.128 mg/Kg - dry 0.128 0.809Benzyl alcohol 1 02/22/23 18:06 V30112JMV
<0.144 mg/Kg - dry 0.144 0.809Bis(2-Chloroethoxy)methane 1 02/22/23 18:06 V30112JMV
<0.131 mg/Kg - dry 0.131 0.809Bis(2-Chloroethyl)ether 1 02/22/23 18:06 V30112JMV
<0.166 mg/Kg - dry 0.166 0.404Bis(2-Chloroisopropyl)ether 1 02/22/23 18:06 V30112JMV
<0.147 mg/Kg - dry 0.147 0.809Bis(2-ethylhexyl)phthalate 1 02/22/23 18:06 V30112JMV
<0.133 mg/Kg - dry 0.133 0.8094-Bromophenyl phenyl ether 1 02/22/23 18:06 V30112JMV
<0.138 mg/Kg - dry 0.138 0.404Butyl benzyl phthalate 1 02/22/23 18:06 V30112JMV
<0.113 mg/Kg - dry 0.113 0.8094-Chloro-3-methylphenol 1 02/22/23 18:06 V30112JMV
<0.137 mg/Kg - dry 0.137 0.4044-Chloroaniline 1 02/22/23 18:06 V30112JMV
<0.142 mg/Kg - dry 0.142 0.8092-Chloronaphthalene 1 02/22/23 18:06 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8092-Chlorophenol 1 02/22/23 18:06 V30112JMV
<0.154 mg/Kg - dry 0.154 1.234-Chlorophenyl phenyl ether 1 02/22/23 18:06 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S1
99875 Matrix:
2/14/2023 14:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.174 mg/Kg - dry 0.174 0.809Chrysene 1 02/22/23 18:06 V30112JMV
<0.282 mg/Kg - dry 0.282 0.809
Dibenz(a,h)anthracene 1 02/22/23 18:06 V30112JMV
<0.146 mg/Kg - dry 0.146 0.809Dibenzofuran 1 02/22/23 18:06 V30112JMV
<0.115 mg/Kg - dry 0.115 0.8091,2-Dichlorobenzene 1 02/22/23 18:06 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8091,3-Dichlorobenzene 1 02/22/23 18:06 V30112JMV
<0.119 mg/Kg - dry 0.119 0.4041,4-Dichlorobenzene 1 02/22/23 18:06 V30112JMV
<0.180 mg/Kg - dry 0.180 0.8093,3'-Dichlorobenzidine 1 02/22/23 18:06 V30112JMV
<0.117 mg/Kg - dry 0.117 0.8092,4-Dichlorophenol 1 02/22/23 18:06 V30112JMV
<0.220 mg/Kg - dry 0.220 0.809
Diethyl phthalate 1 02/22/23 18:06 V30112JMV
<0.213 mg/Kg - dry 0.213 0.809Dimethyl phthalate 1 02/22/23 18:06 V30112JMV
<0.132 mg/Kg - dry 0.132 0.4042,4-Dimethylphenol 1 02/22/23 18:06 V30112JMV
<0.131 mg/Kg - dry 0.131 0.809Di-n-butyl phthalate 1 02/22/23 18:06 V30112JMV
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 02/22/23 18:06 V30112JMV
<0.638 mg/Kg - dry 0.638 1.842,4-Dinitrophenol 1 02/22/23 18:06 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8092,4-Dinitrotoluene 1 02/22/23 18:06 V30112JMV
<0.132 mg/Kg - dry 0.132 0.8092,6-Dinitrotoluene 1 02/22/23 18:06 V30112JMV
<0.175 mg/Kg - dry 0.175 0.404Di-n-Octyl Phthalate 1 02/22/23 18:06 V30112JMV
<0.150 mg/Kg - dry 0.150 0.809Fluoranthene 1 02/22/23 18:06 V30112JMV
<0.157 mg/Kg - dry 0.157 0.809Fluorene 1 02/22/23 18:06 V30112JMV
<0.130 mg/Kg - dry 0.130 0.809Hexachlorobenzene 1 02/22/23 18:06 V30112JMV
<0.119 mg/Kg - dry 0.119 0.809Hexachlorobutadiene 1 02/22/23 18:06 V30112JMV
<0.192 mg/Kg - dry 0.192 0.809Hexachlorocyclopentadiene 1 02/22/23 18:06 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S1
99875 Matrix:
2/14/2023 14:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.097 mg/Kg - dry 0.097 0.809Hexachloroethane 1 02/22/23 18:06 V30112JMV
<0.219 mg/Kg - dry 0.219 0.809
Indeno(1,2,3-cd)pyrene 1 02/22/23 18:06 V30112JMV
<0.234 mg/Kg - dry 0.234 0.809Isophorone 1 02/22/23 18:06 V30112JMV
<0.130 mg/Kg - dry 0.130 0.8091-Methylnaphthalene 1 02/22/23 18:06 V30112JMV
<0.122 mg/Kg - dry 0.122 0.8092-Methylnaphthalene 1 02/22/23 18:06 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8092-Methylphenol 1 02/22/23 18:06 V30112JMV
<0.104 mg/Kg - dry 0.104 0.8093&4 Methylphenol 1 02/22/23 18:06 V30112JMV
<0.176 mg/Kg - dry 0.176 0.809Naphthalene 1 02/22/23 18:06 V30112JMV
<0.118 mg/Kg - dry 0.118 0.809
2-Nitroaniline 1 02/22/23 18:06 V30112JMV
<0.147 mg/Kg - dry 0.147 0.8093-Nitroaniline 1 02/22/23 18:06 V30112JMV
<0.114 mg/Kg - dry 0.114 0.4044-Nitroaniline 1 02/22/23 18:06 V30112JMV
<0.142 mg/Kg - dry 0.142 0.404Nitrobenzene 1 02/22/23 18:06 V30112JMV
<0.108 mg/Kg - dry 0.108 0.8092-Nitrophenol 1 02/22/23 18:06 V30112JMV
<0.143 mg/Kg - dry 0.143 0.8094-Nitrophenol 1 02/22/23 18:06 V30112JMV
<0.322 mg/Kg - dry 0.322 0.809N-Nitrosodimethylamine 1 02/22/23 18:06 V30112JMV
<0.222 mg/Kg - dry 0.222 0.809N-Nitrosodiphenylamine 1 02/22/23 18:06 V30112JMV
<0.144 mg/Kg - dry 0.144 0.809N-Nitroso-di-n-propylamine 1 02/22/23 18:06 V30112JMV
<0.425 mg/Kg - dry 0.425 1.23Pentachlorophenol 1 02/22/23 18:06 V30112JMV
<0.255 mg/Kg - dry 0.255 0.809Phenanthrene 1 02/22/23 18:06 V30112JMV
<0.137 mg/Kg - dry 0.137 0.809Phenol 1 02/22/23 18:06 V30112JMV
<0.164 mg/Kg - dry 0.164 0.809Pyrene 1 02/22/23 18:06 V30112JMV
<0.097 mg/Kg - dry 0.097 0.404Pyridine 1 02/22/23 18:06 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S1
99875 Matrix:
2/14/2023 14:28
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.131 mg/Kg - dry 0.131 0.8091,2,4-Trichlorobenzene 1 02/22/23 18:06 V30112JMV
<0.118 mg/Kg - dry 0.118 0.809
2,4,5-Trichlorophenol 1 02/22/23 18:06 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8092,4,6-Trichlorophenol 1 02/22/23 18:06 V30112JMV
8270ESurrogate: Phenol-d5 44.7 Limits: 34-121%02/22/23 18:061 JMV
Surrogate: 2-Fluorobiphenyl 50.2 Limits: 44-115%02/22/23 18:061 JMV V30112
Surrogate: 2-Fluorophenol 43.2 Limits: 35-115%02/22/23 18:061 JMV V30112
Surrogate: Nitrobenzene-d5 41.3 Limits: 37-122%02/22/23 18:061 JMV V30112
Surrogate: 4-Terphenyl-d14 61.7 Limits: 54-127%02/22/23 18:061 JMV V30112
Surrogate: 2,4,6-Tribromophenol 55.3 Limits: 39-132%02/22/23 18:061 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S2
99876 Matrix:
2/14/2023 14:31
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.1 %Moisture 1 02/16/23 16:10 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S2
99876 Matrix:
2/14/2023 14:31
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.143 mg/Kg - dry 0.143 0.815Acenaphthene 1 02/22/23 18:29 V30112JMV
<0.129 mg/Kg - dry 0.129 0.815
Acenaphthylene 1 02/22/23 18:29 V30112JMV
<0.187 mg/Kg - dry 0.187 0.815Aniline 1 02/22/23 18:29 V30112JMV
<0.176 mg/Kg - dry 0.176 0.815Anthracene 1 02/22/23 18:29 V30112JMV
<0.171 mg/Kg - dry 0.171 0.815Benzo(a)anthracene 1 02/22/23 18:29 V30112JMV
<0.181 mg/Kg - dry 0.181 0.815Benzo(a)pyrene 1 02/22/23 18:29 V30112JMV
<0.180 mg/Kg - dry 0.180 0.815Benzo(b)fluoranthene 1 02/22/23 18:29 V30112JMV
<0.168 mg/Kg - dry 0.168 0.815Benzo(g,h,i)perylene 1 02/22/23 18:29 V30112JMV
<0.169 mg/Kg - dry 0.169 0.815
Benzo(k)fluoranthene 1 02/22/23 18:29 V30112JMV
<0.716 mg/Kg - dry 0.716 2.47Benzoic Acid 1 02/22/23 18:29 V30112JMV
<0.129 mg/Kg - dry 0.129 0.815Benzyl alcohol 1 02/22/23 18:29 V30112JMV
<0.145 mg/Kg - dry 0.145 0.815Bis(2-Chloroethoxy)methane 1 02/22/23 18:29 V30112JMV
<0.132 mg/Kg - dry 0.132 0.815Bis(2-Chloroethyl)ether 1 02/22/23 18:29 V30112JMV
<0.168 mg/Kg - dry 0.168 0.407Bis(2-Chloroisopropyl)ether 1 02/22/23 18:29 V30112JMV
<0.148 mg/Kg - dry 0.148 0.815Bis(2-ethylhexyl)phthalate 1 02/22/23 18:29 V30112JMV
<0.134 mg/Kg - dry 0.134 0.8154-Bromophenyl phenyl ether 1 02/22/23 18:29 V30112JMV
<0.139 mg/Kg - dry 0.139 0.407Butyl benzyl phthalate 1 02/22/23 18:29 V30112JMV
<0.114 mg/Kg - dry 0.114 0.8154-Chloro-3-methylphenol 1 02/22/23 18:29 V30112JMV
<0.138 mg/Kg - dry 0.138 0.4074-Chloroaniline 1 02/22/23 18:29 V30112JMV
<0.143 mg/Kg - dry 0.143 0.8152-Chloronaphthalene 1 02/22/23 18:29 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8152-Chlorophenol 1 02/22/23 18:29 V30112JMV
<0.155 mg/Kg - dry 0.155 1.244-Chlorophenyl phenyl ether 1 02/22/23 18:29 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S2
99876 Matrix:
2/14/2023 14:31
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.175 mg/Kg - dry 0.175 0.815Chrysene 1 02/22/23 18:29 V30112JMV
<0.284 mg/Kg - dry 0.284 0.815
Dibenz(a,h)anthracene 1 02/22/23 18:29 V30112JMV
<0.147 mg/Kg - dry 0.147 0.815Dibenzofuran 1 02/22/23 18:29 V30112JMV
<0.116 mg/Kg - dry 0.116 0.8151,2-Dichlorobenzene 1 02/22/23 18:29 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8151,3-Dichlorobenzene 1 02/22/23 18:29 V30112JMV
<0.120 mg/Kg - dry 0.120 0.4071,4-Dichlorobenzene 1 02/22/23 18:29 V30112JMV
<0.181 mg/Kg - dry 0.181 0.8153,3'-Dichlorobenzidine 1 02/22/23 18:29 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8152,4-Dichlorophenol 1 02/22/23 18:29 V30112JMV
<0.222 mg/Kg - dry 0.222 0.815
Diethyl phthalate 1 02/22/23 18:29 V30112JMV
<0.215 mg/Kg - dry 0.215 0.815Dimethyl phthalate 1 02/22/23 18:29 V30112JMV
<0.133 mg/Kg - dry 0.133 0.4072,4-Dimethylphenol 1 02/22/23 18:29 V30112JMV
<0.132 mg/Kg - dry 0.132 0.815Di-n-butyl phthalate 1 02/22/23 18:29 V30112JMV
<0.296 mg/Kg - dry 0.296 1.854,6-Dinitro-2-methylphenol 1 02/22/23 18:29 V30112JMV
<0.642 mg/Kg - dry 0.642 1.852,4-Dinitrophenol 1 02/22/23 18:29 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8152,4-Dinitrotoluene 1 02/22/23 18:29 V30112JMV
<0.133 mg/Kg - dry 0.133 0.8152,6-Dinitrotoluene 1 02/22/23 18:29 V30112JMV
<0.176 mg/Kg - dry 0.176 0.407Di-n-Octyl Phthalate 1 02/22/23 18:29 V30112JMV
<0.152 mg/Kg - dry 0.152 0.815Fluoranthene 1 02/22/23 18:29 V30112JMV
<0.158 mg/Kg - dry 0.158 0.815Fluorene 1 02/22/23 18:29 V30112JMV
<0.131 mg/Kg - dry 0.131 0.815Hexachlorobenzene 1 02/22/23 18:29 V30112JMV
<0.120 mg/Kg - dry 0.120 0.815Hexachlorobutadiene 1 02/22/23 18:29 V30112JMV
<0.194 mg/Kg - dry 0.194 0.815Hexachlorocyclopentadiene 1 02/22/23 18:29 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S2
99876 Matrix:
2/14/2023 14:31
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.097 mg/Kg - dry 0.097 0.815Hexachloroethane 1 02/22/23 18:29 V30112JMV
<0.221 mg/Kg - dry 0.221 0.815
Indeno(1,2,3-cd)pyrene 1 02/22/23 18:29 V30112JMV
<0.236 mg/Kg - dry 0.236 0.815Isophorone 1 02/22/23 18:29 V30112JMV
<0.131 mg/Kg - dry 0.131 0.8151-Methylnaphthalene 1 02/22/23 18:29 V30112JMV
<0.123 mg/Kg - dry 0.123 0.8152-Methylnaphthalene 1 02/22/23 18:29 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8152-Methylphenol 1 02/22/23 18:29 V30112JMV
<0.104 mg/Kg - dry 0.104 0.8153&4 Methylphenol 1 02/22/23 18:29 V30112JMV
<0.177 mg/Kg - dry 0.177 0.815Naphthalene 1 02/22/23 18:29 V30112JMV
<0.119 mg/Kg - dry 0.119 0.815
2-Nitroaniline 1 02/22/23 18:29 V30112JMV
<0.148 mg/Kg - dry 0.148 0.8153-Nitroaniline 1 02/22/23 18:29 V30112JMV
<0.115 mg/Kg - dry 0.115 0.4074-Nitroaniline 1 02/22/23 18:29 V30112JMV
<0.143 mg/Kg - dry 0.143 0.407Nitrobenzene 1 02/22/23 18:29 V30112JMV
<0.109 mg/Kg - dry 0.109 0.8152-Nitrophenol 1 02/22/23 18:29 V30112JMV
<0.144 mg/Kg - dry 0.144 0.8154-Nitrophenol 1 02/22/23 18:29 V30112JMV
<0.325 mg/Kg - dry 0.325 0.815N-Nitrosodimethylamine 1 02/22/23 18:29 V30112JMV
<0.223 mg/Kg - dry 0.223 0.815N-Nitrosodiphenylamine 1 02/22/23 18:29 V30112JMV
<0.145 mg/Kg - dry 0.145 0.815N-Nitroso-di-n-propylamine 1 02/22/23 18:29 V30112JMV
<0.428 mg/Kg - dry 0.428 1.24Pentachlorophenol 1 02/22/23 18:29 V30112JMV
<0.257 mg/Kg - dry 0.257 0.815Phenanthrene 1 02/22/23 18:29 V30112JMV
<0.138 mg/Kg - dry 0.138 0.815Phenol 1 02/22/23 18:29 V30112JMV
<0.165 mg/Kg - dry 0.165 0.815Pyrene 1 02/22/23 18:29 V30112JMV
<0.097 mg/Kg - dry 0.097 0.407Pyridine 1 02/22/23 18:29 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S2
99876 Matrix:
2/14/2023 14:31
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.132 mg/Kg - dry 0.132 0.8151,2,4-Trichlorobenzene 1 02/22/23 18:29 V30112JMV
<0.118 mg/Kg - dry 0.118 0.815
2,4,5-Trichlorophenol 1 02/22/23 18:29 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8152,4,6-Trichlorophenol 1 02/22/23 18:29 V30112JMV
8270ESurrogate: Phenol-d5 81.1 Limits: 34-121%02/22/23 18:291 JMV
Surrogate: 2-Fluorobiphenyl 80.8 Limits: 44-115%02/22/23 18:291 JMV V30112
Surrogate: 2-Fluorophenol 82.6 Limits: 35-115%02/22/23 18:291 JMV V30112
Surrogate: Nitrobenzene-d5 74.9 Limits: 37-122%02/22/23 18:291 JMV V30112
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%02/22/23 18:291 JMV V30112
Surrogate: 2,4,6-Tribromophenol 89.2 Limits: 39-132%02/22/23 18:291 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S3
99877 Matrix:
2/14/2023 14:36
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.8 %Moisture 1 02/16/23 16:10 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S3
99877 Matrix:
2/14/2023 14:36
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.160 mg/Kg - dry 0.160 0.914Acenaphthene 1 02/22/23 18:52 V30112JMV
<0.145 mg/Kg - dry 0.145 0.914
Acenaphthylene 1 02/22/23 18:52 V30112JMV
<0.210 mg/Kg - dry 0.210 0.914Aniline 1 02/22/23 18:52 V30112JMV
<0.198 mg/Kg - dry 0.198 0.914Anthracene 1 02/22/23 18:52 V30112JMV
<0.192 mg/Kg - dry 0.192 0.914Benzo(a)anthracene 1 02/22/23 18:52 V30112JMV
<0.203 mg/Kg - dry 0.203 0.914Benzo(a)pyrene 1 02/22/23 18:52 V30112JMV
<0.202 mg/Kg - dry 0.202 0.914Benzo(b)fluoranthene 1 02/22/23 18:52 V30112JMV
<0.188 mg/Kg - dry 0.188 0.914Benzo(g,h,i)perylene 1 02/22/23 18:52 V30112JMV
<0.189 mg/Kg - dry 0.189 0.914
Benzo(k)fluoranthene 1 02/22/23 18:52 V30112JMV
<0.803 mg/Kg - dry 0.803 2.77Benzoic Acid 1 02/22/23 18:52 V30112JMV
<0.145 mg/Kg - dry 0.145 0.914Benzyl alcohol 1 02/22/23 18:52 V30112JMV
<0.163 mg/Kg - dry 0.163 0.914Bis(2-Chloroethoxy)methane 1 02/22/23 18:52 V30112JMV
<0.148 mg/Kg - dry 0.148 0.914Bis(2-Chloroethyl)ether 1 02/22/23 18:52 V30112JMV
<0.188 mg/Kg - dry 0.188 0.457Bis(2-Chloroisopropyl)ether 1 02/22/23 18:52 V30112JMV
<0.166 mg/Kg - dry 0.166 0.914Bis(2-ethylhexyl)phthalate 1 02/22/23 18:52 V30112JMV
<0.150 mg/Kg - dry 0.150 0.9144-Bromophenyl phenyl ether 1 02/22/23 18:52 V30112JMV
<0.156 mg/Kg - dry 0.156 0.457Butyl benzyl phthalate 1 02/22/23 18:52 V30112JMV
<0.127 mg/Kg - dry 0.127 0.9144-Chloro-3-methylphenol 1 02/22/23 18:52 V30112JMV
<0.155 mg/Kg - dry 0.155 0.4574-Chloroaniline 1 02/22/23 18:52 V30112JMV
<0.160 mg/Kg - dry 0.160 0.9142-Chloronaphthalene 1 02/22/23 18:52 V30112JMV
<0.136 mg/Kg - dry 0.136 0.9142-Chlorophenol 1 02/22/23 18:52 V30112JMV
<0.174 mg/Kg - dry 0.174 1.394-Chlorophenyl phenyl ether 1 02/22/23 18:52 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S3
99877 Matrix:
2/14/2023 14:36
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.196 mg/Kg - dry 0.196 0.914Chrysene 1 02/22/23 18:52 V30112JMV
<0.318 mg/Kg - dry 0.318 0.914
Dibenz(a,h)anthracene 1 02/22/23 18:52 V30112JMV
<0.164 mg/Kg - dry 0.164 0.914Dibenzofuran 1 02/22/23 18:52 V30112JMV
<0.130 mg/Kg - dry 0.130 0.9141,2-Dichlorobenzene 1 02/22/23 18:52 V30112JMV
<0.134 mg/Kg - dry 0.134 0.9141,3-Dichlorobenzene 1 02/22/23 18:52 V30112JMV
<0.135 mg/Kg - dry 0.135 0.4571,4-Dichlorobenzene 1 02/22/23 18:52 V30112JMV
<0.203 mg/Kg - dry 0.203 0.9143,3'-Dichlorobenzidine 1 02/22/23 18:52 V30112JMV
<0.132 mg/Kg - dry 0.132 0.9142,4-Dichlorophenol 1 02/22/23 18:52 V30112JMV
<0.249 mg/Kg - dry 0.249 0.914
Diethyl phthalate 1 02/22/23 18:52 V30112JMV
<0.240 mg/Kg - dry 0.240 0.914Dimethyl phthalate 1 02/22/23 18:52 V30112JMV
<0.149 mg/Kg - dry 0.149 0.4572,4-Dimethylphenol 1 02/22/23 18:52 V30112JMV
<0.148 mg/Kg - dry 0.148 0.914Di-n-butyl phthalate 1 02/22/23 18:52 V30112JMV
<0.332 mg/Kg - dry 0.332 2.084,6-Dinitro-2-methylphenol 1 02/22/23 18:52 V30112JMV
<0.720 mg/Kg - dry 0.720 2.082,4-Dinitrophenol 1 02/22/23 18:52 V30112JMV
<0.133 mg/Kg - dry 0.133 0.9142,4-Dinitrotoluene 1 02/22/23 18:52 V30112JMV
<0.149 mg/Kg - dry 0.149 0.9142,6-Dinitrotoluene 1 02/22/23 18:52 V30112JMV
<0.198 mg/Kg - dry 0.198 0.457Di-n-Octyl Phthalate 1 02/22/23 18:52 V30112JMV
<0.170 mg/Kg - dry 0.170 0.914Fluoranthene 1 02/22/23 18:52 V30112JMV
<0.177 mg/Kg - dry 0.177 0.914Fluorene 1 02/22/23 18:52 V30112JMV
<0.146 mg/Kg - dry 0.146 0.914Hexachlorobenzene 1 02/22/23 18:52 V30112JMV
<0.135 mg/Kg - dry 0.135 0.914Hexachlorobutadiene 1 02/22/23 18:52 V30112JMV
<0.217 mg/Kg - dry 0.217 0.914Hexachlorocyclopentadiene 1 02/22/23 18:52 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S3
99877 Matrix:
2/14/2023 14:36
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.109 mg/Kg - dry 0.109 0.914Hexachloroethane 1 02/22/23 18:52 V30112JMV
<0.247 mg/Kg - dry 0.247 0.914
Indeno(1,2,3-cd)pyrene 1 02/22/23 18:52 V30112JMV
<0.264 mg/Kg - dry 0.264 0.914Isophorone 1 02/22/23 18:52 V30112JMV
<0.146 mg/Kg - dry 0.146 0.9141-Methylnaphthalene 1 02/22/23 18:52 V30112JMV
<0.138 mg/Kg - dry 0.138 0.9142-Methylnaphthalene 1 02/22/23 18:52 V30112JMV
<0.134 mg/Kg - dry 0.134 0.9142-Methylphenol 1 02/22/23 18:52 V30112JMV
<0.117 mg/Kg - dry 0.117 0.9143&4 Methylphenol 1 02/22/23 18:52 V30112JMV
<0.199 mg/Kg - dry 0.199 0.914Naphthalene 1 02/22/23 18:52 V30112JMV
<0.133 mg/Kg - dry 0.133 0.914
2-Nitroaniline 1 02/22/23 18:52 V30112JMV
<0.166 mg/Kg - dry 0.166 0.9143-Nitroaniline 1 02/22/23 18:52 V30112JMV
<0.129 mg/Kg - dry 0.129 0.4574-Nitroaniline 1 02/22/23 18:52 V30112JMV
<0.160 mg/Kg - dry 0.160 0.457Nitrobenzene 1 02/22/23 18:52 V30112JMV
<0.122 mg/Kg - dry 0.122 0.9142-Nitrophenol 1 02/22/23 18:52 V30112JMV
<0.162 mg/Kg - dry 0.162 0.9144-Nitrophenol 1 02/22/23 18:52 V30112JMV
<0.364 mg/Kg - dry 0.364 0.914N-Nitrosodimethylamine 1 02/22/23 18:52 V30112JMV
<0.250 mg/Kg - dry 0.250 0.914N-Nitrosodiphenylamine 1 02/22/23 18:52 V30112JMV
<0.163 mg/Kg - dry 0.163 0.914N-Nitroso-di-n-propylamine 1 02/22/23 18:52 V30112JMV
<0.480 mg/Kg - dry 0.480 1.39Pentachlorophenol 1 02/22/23 18:52 V30112JMV
<0.288 mg/Kg - dry 0.288 0.914Phenanthrene 1 02/22/23 18:52 V30112JMV
<0.155 mg/Kg - dry 0.155 0.914Phenol 1 02/22/23 18:52 V30112JMV
<0.185 mg/Kg - dry 0.185 0.914Pyrene 1 02/22/23 18:52 V30112JMV
<0.109 mg/Kg - dry 0.109 0.457Pyridine 1 02/22/23 18:52 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S3
99877 Matrix:
2/14/2023 14:36
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.148 mg/Kg - dry 0.148 0.9141,2,4-Trichlorobenzene 1 02/22/23 18:52 V30112JMV
<0.133 mg/Kg - dry 0.133 0.914
2,4,5-Trichlorophenol 1 02/22/23 18:52 V30112JMV
<0.133 mg/Kg - dry 0.133 0.9142,4,6-Trichlorophenol 1 02/22/23 18:52 V30112JMV
8270ESurrogate: Phenol-d5 76.0 Limits: 34-121%02/22/23 18:521 JMV
Surrogate: 2-Fluorobiphenyl 74.9 Limits: 44-115%02/22/23 18:521 JMV V30112
Surrogate: 2-Fluorophenol 77.2 Limits: 35-115%02/22/23 18:521 JMV V30112
Surrogate: Nitrobenzene-d5 69.5 Limits: 37-122%02/22/23 18:521 JMV V30112
Surrogate: 4-Terphenyl-d14 94.6 Limits: 54-127%02/22/23 18:521 JMV V30112
Surrogate: 2,4,6-Tribromophenol 85.0 Limits: 39-132%02/22/23 18:521 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S4
99878 Matrix:
2/14/2023 14:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.9 %Moisture 1 02/16/23 16:10 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S4
99878 Matrix:
2/14/2023 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.141 mg/Kg - dry 0.141 0.803Acenaphthene 1 02/22/23 19:14 V30112JMV
<0.127 mg/Kg - dry 0.127 0.803
Acenaphthylene 1 02/22/23 19:14 V30112JMV
<0.185 mg/Kg - dry 0.185 0.803Aniline 1 02/22/23 19:14 V30112JMV
<0.174 mg/Kg - dry 0.174 0.803Anthracene 1 02/22/23 19:14 V30112JMV
0.288 J mg/Kg - dry 0.169 0.803Benzo(a)anthracene 1 02/22/23 19:14 V30112JMV
0.321 J mg/Kg - dry 0.179 0.803Benzo(a)pyrene 1 02/22/23 19:14 V30112JMV
0.527 J mg/Kg - dry 0.177 0.803Benzo(b)fluoranthene 1 02/22/23 19:14 V30112JMV
0.263 J mg/Kg - dry 0.165 0.803Benzo(g,h,i)perylene 1 02/22/23 19:14 V30112JMV
0.183 J
mg/Kg - dry 0.166 0.803
Benzo(k)fluoranthene 1 02/22/23 19:14 V30112JMV
<0.706 mg/Kg - dry 0.706 2.44Benzoic Acid 1 02/22/23 19:14 V30112JMV
<0.127 mg/Kg - dry 0.127 0.803Benzyl alcohol 1 02/22/23 19:14 V30112JMV
<0.143 mg/Kg - dry 0.143 0.803Bis(2-Chloroethoxy)methane 1 02/22/23 19:14 V30112JMV
<0.130 mg/Kg - dry 0.130 0.803Bis(2-Chloroethyl)ether 1 02/22/23 19:14 V30112JMV
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 02/22/23 19:14 V30112JMV
<0.146 mg/Kg - dry 0.146 0.803Bis(2-ethylhexyl)phthalate 1 02/22/23 19:14 V30112JMV
<0.132 mg/Kg - dry 0.132 0.8034-Bromophenyl phenyl ether 1 02/22/23 19:14 V30112JMV
<0.137 mg/Kg - dry 0.137 0.401Butyl benzyl phthalate 1 02/22/23 19:14 V30112JMV
<0.112 mg/Kg - dry 0.112 0.8034-Chloro-3-methylphenol 1 02/22/23 19:14 V30112JMV
<0.136 mg/Kg - dry 0.136 0.4014-Chloroaniline 1 02/22/23 19:14 V30112JMV
<0.141 mg/Kg - dry 0.141 0.8032-Chloronaphthalene 1 02/22/23 19:14 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8032-Chlorophenol 1 02/22/23 19:14 V30112JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 02/22/23 19:14 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S4
99878 Matrix:
2/14/2023 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
0.288 J mg/Kg - dry 0.172 0.803Chrysene 1 02/22/23 19:14 V30112JMV
<0.280 mg/Kg - dry 0.280 0.803
Dibenz(a,h)anthracene 1 02/22/23 19:14 V30112JMV
<0.144 mg/Kg - dry 0.144 0.803Dibenzofuran 1 02/22/23 19:14 V30112JMV
<0.114 mg/Kg - dry 0.114 0.8031,2-Dichlorobenzene 1 02/22/23 19:14 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8031,3-Dichlorobenzene 1 02/22/23 19:14 V30112JMV
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 02/22/23 19:14 V30112JMV
<0.179 mg/Kg - dry 0.179 0.8033,3'-Dichlorobenzidine 1 02/22/23 19:14 V30112JMV
<0.116 mg/Kg - dry 0.116 0.8032,4-Dichlorophenol 1 02/22/23 19:14 V30112JMV
<0.219 mg/Kg - dry 0.219 0.803
Diethyl phthalate 1 02/22/23 19:14 V30112JMV
<0.211 mg/Kg - dry 0.211 0.803Dimethyl phthalate 1 02/22/23 19:14 V30112JMV
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 02/22/23 19:14 V30112JMV
<0.130 mg/Kg - dry 0.130 0.803Di-n-butyl phthalate 1 02/22/23 19:14 V30112JMV
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 02/22/23 19:14 V30112JMV
<0.633 mg/Kg - dry 0.633 1.832,4-Dinitrophenol 1 02/22/23 19:14 V30112JMV
<0.117 mg/Kg - dry 0.117 0.8032,4-Dinitrotoluene 1 02/22/23 19:14 V30112JMV
<0.131 mg/Kg - dry 0.131 0.8032,6-Dinitrotoluene 1 02/22/23 19:14 V30112JMV
<0.174 mg/Kg - dry 0.174 0.401Di-n-Octyl Phthalate 1 02/22/23 19:14 V30112JMV
0.432 J mg/Kg - dry 0.149 0.803Fluoranthene 1 02/22/23 19:14 V30112JMV
<0.155 mg/Kg - dry 0.155 0.803Fluorene 1 02/22/23 19:14 V30112JMV
<0.129 mg/Kg - dry 0.129 0.803Hexachlorobenzene 1 02/22/23 19:14 V30112JMV
<0.118 mg/Kg - dry 0.118 0.803Hexachlorobutadiene 1 02/22/23 19:14 V30112JMV
<0.191 mg/Kg - dry 0.191 0.803Hexachlorocyclopentadiene 1 02/22/23 19:14 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S4
99878 Matrix:
2/14/2023 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.096 mg/Kg - dry 0.096 0.803Hexachloroethane 1 02/22/23 19:14 V30112JMV
0.285 J
mg/Kg - dry 0.218 0.803
Indeno(1,2,3-cd)pyrene 1 02/22/23 19:14 V30112JMV
<0.232 mg/Kg - dry 0.232 0.803Isophorone 1 02/22/23 19:14 V30112JMV
<0.129 mg/Kg - dry 0.129 0.8031-Methylnaphthalene 1 02/22/23 19:14 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8032-Methylnaphthalene 1 02/22/23 19:14 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8032-Methylphenol 1 02/22/23 19:14 V30112JMV
<0.103 mg/Kg - dry 0.103 0.8033&4 Methylphenol 1 02/22/23 19:14 V30112JMV
<0.175 mg/Kg - dry 0.175 0.803Naphthalene 1 02/22/23 19:14 V30112JMV
<0.117 mg/Kg - dry 0.117 0.803
2-Nitroaniline 1 02/22/23 19:14 V30112JMV
<0.146 mg/Kg - dry 0.146 0.8033-Nitroaniline 1 02/22/23 19:14 V30112JMV
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 02/22/23 19:14 V30112JMV
<0.141 mg/Kg - dry 0.141 0.401Nitrobenzene 1 02/22/23 19:14 V30112JMV
<0.108 mg/Kg - dry 0.108 0.8032-Nitrophenol 1 02/22/23 19:14 V30112JMV
<0.142 mg/Kg - dry 0.142 0.8034-Nitrophenol 1 02/22/23 19:14 V30112JMV
<0.320 mg/Kg - dry 0.320 0.803N-Nitrosodimethylamine 1 02/22/23 19:14 V30112JMV
<0.220 mg/Kg - dry 0.220 0.803N-Nitrosodiphenylamine 1 02/22/23 19:14 V30112JMV
<0.143 mg/Kg - dry 0.143 0.803N-Nitroso-di-n-propylamine 1 02/22/23 19:14 V30112JMV
<0.422 mg/Kg - dry 0.422 1.22Pentachlorophenol 1 02/22/23 19:14 V30112JMV
<0.253 mg/Kg - dry 0.253 0.803Phenanthrene 1 02/22/23 19:14 V30112JMV
<0.136 mg/Kg - dry 0.136 0.803Phenol 1 02/22/23 19:14 V30112JMV
0.423 J mg/Kg - dry 0.163 0.803Pyrene 1 02/22/23 19:14 V30112JMV
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 02/22/23 19:14 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S4
99878 Matrix:
2/14/2023 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.130 mg/Kg - dry 0.130 0.8031,2,4-Trichlorobenzene 1 02/22/23 19:14 V30112JMV
<0.117 mg/Kg - dry 0.117 0.803
2,4,5-Trichlorophenol 1 02/22/23 19:14 V30112JMV
<0.117 mg/Kg - dry 0.117 0.8032,4,6-Trichlorophenol 1 02/22/23 19:14 V30112JMV
8270ESurrogate: Phenol-d5 86.5 Limits: 34-121%02/22/23 19:141 JMV
Surrogate: 2-Fluorobiphenyl 88.0 Limits: 44-115%02/22/23 19:141 JMV V30112
Surrogate: 2-Fluorophenol 86.2 Limits: 35-115%02/22/23 19:141 JMV V30112
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%02/22/23 19:141 JMV V30112
Surrogate: 4-Terphenyl-d14 98.2 Limits: 54-127%02/22/23 19:141 JMV V30112
Surrogate: 2,4,6-Tribromophenol 87.4 Limits: 39-132%02/22/23 19:141 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S5
99879 Matrix:
2/14/2023 14:44
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 02/16/23 16:10 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S5
99879 Matrix:
2/14/2023 14:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.133 mg/Kg - dry 0.133 0.760Acenaphthene 1 02/22/23 19:37 V30112JMV
<0.120 mg/Kg - dry 0.120 0.760
Acenaphthylene 1 02/22/23 19:37 V30112JMV
<0.174 mg/Kg - dry 0.174 0.760Aniline 1 02/22/23 19:37 V30112JMV
<0.164 mg/Kg - dry 0.164 0.760Anthracene 1 02/22/23 19:37 V30112JMV
<0.159 mg/Kg - dry 0.159 0.760Benzo(a)anthracene 1 02/22/23 19:37 V30112JMV
<0.169 mg/Kg - dry 0.169 0.760Benzo(a)pyrene 1 02/22/23 19:37 V30112JMV
<0.168 mg/Kg - dry 0.168 0.760Benzo(b)fluoranthene 1 02/22/23 19:37 V30112JMV
<0.156 mg/Kg - dry 0.156 0.760Benzo(g,h,i)perylene 1 02/22/23 19:37 V30112JMV
<0.157 mg/Kg - dry 0.157 0.760
Benzo(k)fluoranthene 1 02/22/23 19:37 V30112JMV
<0.667 mg/Kg - dry 0.667 2.30Benzoic Acid 1 02/22/23 19:37 V30112JMV
<0.120 mg/Kg - dry 0.120 0.760Benzyl alcohol 1 02/22/23 19:37 V30112JMV
<0.135 mg/Kg - dry 0.135 0.760Bis(2-Chloroethoxy)methane 1 02/22/23 19:37 V30112JMV
<0.123 mg/Kg - dry 0.123 0.760Bis(2-Chloroethyl)ether 1 02/22/23 19:37 V30112JMV
<0.156 mg/Kg - dry 0.156 0.379Bis(2-Chloroisopropyl)ether 1 02/22/23 19:37 V30112JMV
<0.138 mg/Kg - dry 0.138 0.760Bis(2-ethylhexyl)phthalate 1 02/22/23 19:37 V30112JMV
<0.125 mg/Kg - dry 0.125 0.7604-Bromophenyl phenyl ether 1 02/22/23 19:37 V30112JMV
<0.130 mg/Kg - dry 0.130 0.379Butyl benzyl phthalate 1 02/22/23 19:37 V30112JMV
<0.106 mg/Kg - dry 0.106 0.7604-Chloro-3-methylphenol 1 02/22/23 19:37 V30112JMV
<0.128 mg/Kg - dry 0.128 0.3794-Chloroaniline 1 02/22/23 19:37 V30112JMV
<0.133 mg/Kg - dry 0.133 0.7602-Chloronaphthalene 1 02/22/23 19:37 V30112JMV
<0.113 mg/Kg - dry 0.113 0.7602-Chlorophenol 1 02/22/23 19:37 V30112JMV
<0.144 mg/Kg - dry 0.144 1.154-Chlorophenyl phenyl ether 1 02/22/23 19:37 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S5
99879 Matrix:
2/14/2023 14:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.163 mg/Kg - dry 0.163 0.760Chrysene 1 02/22/23 19:37 V30112JMV
<0.264 mg/Kg - dry 0.264 0.760
Dibenz(a,h)anthracene 1 02/22/23 19:37 V30112JMV
<0.136 mg/Kg - dry 0.136 0.760Dibenzofuran 1 02/22/23 19:37 V30112JMV
<0.108 mg/Kg - dry 0.108 0.7601,2-Dichlorobenzene 1 02/22/23 19:37 V30112JMV
<0.112 mg/Kg - dry 0.112 0.7601,3-Dichlorobenzene 1 02/22/23 19:37 V30112JMV
<0.112 mg/Kg - dry 0.112 0.3791,4-Dichlorobenzene 1 02/22/23 19:37 V30112JMV
<0.169 mg/Kg - dry 0.169 0.7603,3'-Dichlorobenzidine 1 02/22/23 19:37 V30112JMV
<0.110 mg/Kg - dry 0.110 0.7602,4-Dichlorophenol 1 02/22/23 19:37 V30112JMV
<0.207 mg/Kg - dry 0.207 0.760
Diethyl phthalate 1 02/22/23 19:37 V30112JMV
<0.200 mg/Kg - dry 0.200 0.760Dimethyl phthalate 1 02/22/23 19:37 V30112JMV
<0.124 mg/Kg - dry 0.124 0.3792,4-Dimethylphenol 1 02/22/23 19:37 V30112JMV
<0.123 mg/Kg - dry 0.123 0.760Di-n-butyl phthalate 1 02/22/23 19:37 V30112JMV
<0.276 mg/Kg - dry 0.276 1.734,6-Dinitro-2-methylphenol 1 02/22/23 19:37 V30112JMV
<0.598 mg/Kg - dry 0.598 1.732,4-Dinitrophenol 1 02/22/23 19:37 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7602,4-Dinitrotoluene 1 02/22/23 19:37 V30112JMV
<0.124 mg/Kg - dry 0.124 0.7602,6-Dinitrotoluene 1 02/22/23 19:37 V30112JMV
<0.164 mg/Kg - dry 0.164 0.379Di-n-Octyl Phthalate 1 02/22/23 19:37 V30112JMV
<0.141 mg/Kg - dry 0.141 0.760Fluoranthene 1 02/22/23 19:37 V30112JMV
<0.147 mg/Kg - dry 0.147 0.760Fluorene 1 02/22/23 19:37 V30112JMV
<0.121 mg/Kg - dry 0.121 0.760Hexachlorobenzene 1 02/22/23 19:37 V30112JMV
<0.112 mg/Kg - dry 0.112 0.760Hexachlorobutadiene 1 02/22/23 19:37 V30112JMV
<0.180 mg/Kg - dry 0.180 0.760Hexachlorocyclopentadiene 1 02/22/23 19:37 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S5
99879 Matrix:
2/14/2023 14:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.091 mg/Kg - dry 0.091 0.760Hexachloroethane 1 02/22/23 19:37 V30112JMV
<0.205 mg/Kg - dry 0.205 0.760
Indeno(1,2,3-cd)pyrene 1 02/22/23 19:37 V30112JMV
<0.219 mg/Kg - dry 0.219 0.760Isophorone 1 02/22/23 19:37 V30112JMV
<0.121 mg/Kg - dry 0.121 0.7601-Methylnaphthalene 1 02/22/23 19:37 V30112JMV
<0.115 mg/Kg - dry 0.115 0.7602-Methylnaphthalene 1 02/22/23 19:37 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7602-Methylphenol 1 02/22/23 19:37 V30112JMV
<0.097 mg/Kg - dry 0.097 0.7603&4 Methylphenol 1 02/22/23 19:37 V30112JMV
<0.165 mg/Kg - dry 0.165 0.760Naphthalene 1 02/22/23 19:37 V30112JMV
<0.111 mg/Kg - dry 0.111 0.760
2-Nitroaniline 1 02/22/23 19:37 V30112JMV
<0.138 mg/Kg - dry 0.138 0.7603-Nitroaniline 1 02/22/23 19:37 V30112JMV
<0.107 mg/Kg - dry 0.107 0.3794-Nitroaniline 1 02/22/23 19:37 V30112JMV
<0.133 mg/Kg - dry 0.133 0.379Nitrobenzene 1 02/22/23 19:37 V30112JMV
<0.102 mg/Kg - dry 0.102 0.7602-Nitrophenol 1 02/22/23 19:37 V30112JMV
<0.134 mg/Kg - dry 0.134 0.7604-Nitrophenol 1 02/22/23 19:37 V30112JMV
<0.302 mg/Kg - dry 0.302 0.760N-Nitrosodimethylamine 1 02/22/23 19:37 V30112JMV
<0.208 mg/Kg - dry 0.208 0.760N-Nitrosodiphenylamine 1 02/22/23 19:37 V30112JMV
<0.135 mg/Kg - dry 0.135 0.760N-Nitroso-di-n-propylamine 1 02/22/23 19:37 V30112JMV
<0.399 mg/Kg - dry 0.399 1.15Pentachlorophenol 1 02/22/23 19:37 V30112JMV
<0.239 mg/Kg - dry 0.239 0.760Phenanthrene 1 02/22/23 19:37 V30112JMV
<0.128 mg/Kg - dry 0.128 0.760Phenol 1 02/22/23 19:37 V30112JMV
<0.154 mg/Kg - dry 0.154 0.760Pyrene 1 02/22/23 19:37 V30112JMV
<0.091 mg/Kg - dry 0.091 0.379Pyridine 1 02/22/23 19:37 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S5
99879 Matrix:
2/14/2023 14:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.123 mg/Kg - dry 0.123 0.7601,2,4-Trichlorobenzene 1 02/22/23 19:37 V30112JMV
<0.110 mg/Kg - dry 0.110 0.760
2,4,5-Trichlorophenol 1 02/22/23 19:37 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7602,4,6-Trichlorophenol 1 02/22/23 19:37 V30112JMV
8270ESurrogate: Phenol-d5 83.8 Limits: 34-121%02/22/23 19:371 JMV
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 44-115%02/22/23 19:371 JMV V30112
Surrogate: 2-Fluorophenol 86.8 Limits: 35-115%02/22/23 19:371 JMV V30112
Surrogate: Nitrobenzene-d5 77.8 Limits: 37-122%02/22/23 19:371 JMV V30112
Surrogate: 4-Terphenyl-d14 97.0 Limits: 54-127%02/22/23 19:371 JMV V30112
Surrogate: 2,4,6-Tribromophenol 88.0 Limits: 39-132%02/22/23 19:371 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S6
99880 Matrix:
2/14/2023 14:49
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.9 %Moisture 1 02/17/23 10:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S6
99880 Matrix:
2/14/2023 14:49
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.136 mg/Kg - dry 0.136 0.776Acenaphthene 1 02/22/23 19:59 V30112JMV
<0.123 mg/Kg - dry 0.123 0.776
Acenaphthylene 1 02/22/23 19:59 V30112JMV
<0.178 mg/Kg - dry 0.178 0.776Aniline 1 02/22/23 19:59 V30112JMV
<0.168 mg/Kg - dry 0.168 0.776Anthracene 1 02/22/23 19:59 V30112JMV
<0.163 mg/Kg - dry 0.163 0.776Benzo(a)anthracene 1 02/22/23 19:59 V30112JMV
<0.172 mg/Kg - dry 0.172 0.776Benzo(a)pyrene 1 02/22/23 19:59 V30112JMV
<0.171 mg/Kg - dry 0.171 0.776Benzo(b)fluoranthene 1 02/22/23 19:59 V30112JMV
<0.159 mg/Kg - dry 0.159 0.776Benzo(g,h,i)perylene 1 02/22/23 19:59 V30112JMV
<0.160 mg/Kg - dry 0.160 0.776
Benzo(k)fluoranthene 1 02/22/23 19:59 V30112JMV
<0.681 mg/Kg - dry 0.681 2.35Benzoic Acid 1 02/22/23 19:59 V30112JMV
<0.123 mg/Kg - dry 0.123 0.776Benzyl alcohol 1 02/22/23 19:59 V30112JMV
<0.138 mg/Kg - dry 0.138 0.776Bis(2-Chloroethoxy)methane 1 02/22/23 19:59 V30112JMV
<0.125 mg/Kg - dry 0.125 0.776Bis(2-Chloroethyl)ether 1 02/22/23 19:59 V30112JMV
<0.159 mg/Kg - dry 0.159 0.387Bis(2-Chloroisopropyl)ether 1 02/22/23 19:59 V30112JMV
<0.141 mg/Kg - dry 0.141 0.776Bis(2-ethylhexyl)phthalate 1 02/22/23 19:59 V30112JMV
<0.128 mg/Kg - dry 0.128 0.7764-Bromophenyl phenyl ether 1 02/22/23 19:59 V30112JMV
<0.132 mg/Kg - dry 0.132 0.387Butyl benzyl phthalate 1 02/22/23 19:59 V30112JMV
<0.108 mg/Kg - dry 0.108 0.7764-Chloro-3-methylphenol 1 02/22/23 19:59 V30112JMV
<0.131 mg/Kg - dry 0.131 0.3874-Chloroaniline 1 02/22/23 19:59 V30112JMV
<0.136 mg/Kg - dry 0.136 0.7762-Chloronaphthalene 1 02/22/23 19:59 V30112JMV
<0.115 mg/Kg - dry 0.115 0.7762-Chlorophenol 1 02/22/23 19:59 V30112JMV
<0.148 mg/Kg - dry 0.148 1.184-Chlorophenyl phenyl ether 1 02/22/23 19:59 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S6
99880 Matrix:
2/14/2023 14:49
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.166 mg/Kg - dry 0.166 0.776Chrysene 1 02/22/23 19:59 V30112JMV
<0.270 mg/Kg - dry 0.270 0.776
Dibenz(a,h)anthracene 1 02/22/23 19:59 V30112JMV
<0.139 mg/Kg - dry 0.139 0.776Dibenzofuran 1 02/22/23 19:59 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7761,2-Dichlorobenzene 1 02/22/23 19:59 V30112JMV
<0.114 mg/Kg - dry 0.114 0.7761,3-Dichlorobenzene 1 02/22/23 19:59 V30112JMV
<0.114 mg/Kg - dry 0.114 0.3871,4-Dichlorobenzene 1 02/22/23 19:59 V30112JMV
<0.172 mg/Kg - dry 0.172 0.7763,3'-Dichlorobenzidine 1 02/22/23 19:59 V30112JMV
<0.112 mg/Kg - dry 0.112 0.7762,4-Dichlorophenol 1 02/22/23 19:59 V30112JMV
<0.211 mg/Kg - dry 0.211 0.776
Diethyl phthalate 1 02/22/23 19:59 V30112JMV
<0.204 mg/Kg - dry 0.204 0.776Dimethyl phthalate 1 02/22/23 19:59 V30112JMV
<0.126 mg/Kg - dry 0.126 0.3872,4-Dimethylphenol 1 02/22/23 19:59 V30112JMV
<0.125 mg/Kg - dry 0.125 0.776Di-n-butyl phthalate 1 02/22/23 19:59 V30112JMV
<0.282 mg/Kg - dry 0.282 1.764,6-Dinitro-2-methylphenol 1 02/22/23 19:59 V30112JMV
<0.611 mg/Kg - dry 0.611 1.762,4-Dinitrophenol 1 02/22/23 19:59 V30112JMV
<0.113 mg/Kg - dry 0.113 0.7762,4-Dinitrotoluene 1 02/22/23 19:59 V30112JMV
<0.126 mg/Kg - dry 0.126 0.7762,6-Dinitrotoluene 1 02/22/23 19:59 V30112JMV
<0.168 mg/Kg - dry 0.168 0.387Di-n-Octyl Phthalate 1 02/22/23 19:59 V30112JMV
<0.144 mg/Kg - dry 0.144 0.776Fluoranthene 1 02/22/23 19:59 V30112JMV
<0.150 mg/Kg - dry 0.150 0.776Fluorene 1 02/22/23 19:59 V30112JMV
<0.124 mg/Kg - dry 0.124 0.776Hexachlorobenzene 1 02/22/23 19:59 V30112JMV
<0.114 mg/Kg - dry 0.114 0.776Hexachlorobutadiene 1 02/22/23 19:59 V30112JMV
<0.184 mg/Kg - dry 0.184 0.776Hexachlorocyclopentadiene 1 02/22/23 19:59 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S6
99880 Matrix:
2/14/2023 14:49
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.093 mg/Kg - dry 0.093 0.776Hexachloroethane 1 02/22/23 19:59 V30112JMV
<0.210 mg/Kg - dry 0.210 0.776
Indeno(1,2,3-cd)pyrene 1 02/22/23 19:59 V30112JMV
<0.224 mg/Kg - dry 0.224 0.776Isophorone 1 02/22/23 19:59 V30112JMV
<0.124 mg/Kg - dry 0.124 0.7761-Methylnaphthalene 1 02/22/23 19:59 V30112JMV
<0.117 mg/Kg - dry 0.117 0.7762-Methylnaphthalene 1 02/22/23 19:59 V30112JMV
<0.114 mg/Kg - dry 0.114 0.7762-Methylphenol 1 02/22/23 19:59 V30112JMV
<0.099 mg/Kg - dry 0.099 0.7763&4 Methylphenol 1 02/22/23 19:59 V30112JMV
<0.169 mg/Kg - dry 0.169 0.776Naphthalene 1 02/22/23 19:59 V30112JMV
<0.113 mg/Kg - dry 0.113 0.776
2-Nitroaniline 1 02/22/23 19:59 V30112JMV
<0.141 mg/Kg - dry 0.141 0.7763-Nitroaniline 1 02/22/23 19:59 V30112JMV
<0.109 mg/Kg - dry 0.109 0.3874-Nitroaniline 1 02/22/23 19:59 V30112JMV
<0.136 mg/Kg - dry 0.136 0.387Nitrobenzene 1 02/22/23 19:59 V30112JMV
<0.104 mg/Kg - dry 0.104 0.7762-Nitrophenol 1 02/22/23 19:59 V30112JMV
<0.137 mg/Kg - dry 0.137 0.7764-Nitrophenol 1 02/22/23 19:59 V30112JMV
<0.309 mg/Kg - dry 0.309 0.776N-Nitrosodimethylamine 1 02/22/23 19:59 V30112JMV
<0.212 mg/Kg - dry 0.212 0.776N-Nitrosodiphenylamine 1 02/22/23 19:59 V30112JMV
<0.138 mg/Kg - dry 0.138 0.776N-Nitroso-di-n-propylamine 1 02/22/23 19:59 V30112JMV
<0.407 mg/Kg - dry 0.407 1.18Pentachlorophenol 1 02/22/23 19:59 V30112JMV
<0.244 mg/Kg - dry 0.244 0.776Phenanthrene 1 02/22/23 19:59 V30112JMV
<0.131 mg/Kg - dry 0.131 0.776Phenol 1 02/22/23 19:59 V30112JMV
<0.157 mg/Kg - dry 0.157 0.776Pyrene 1 02/22/23 19:59 V30112JMV
<0.093 mg/Kg - dry 0.093 0.387Pyridine 1 02/22/23 19:59 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S6
99880 Matrix:
2/14/2023 14:49
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.125 mg/Kg - dry 0.125 0.7761,2,4-Trichlorobenzene 1 02/22/23 19:59 V30112JMV
<0.113 mg/Kg - dry 0.113 0.776
2,4,5-Trichlorophenol 1 02/22/23 19:59 V30112JMV
<0.113 mg/Kg - dry 0.113 0.7762,4,6-Trichlorophenol 1 02/22/23 19:59 V30112JMV
8270ESurrogate: Phenol-d5 86.5 Limits: 34-121%02/22/23 19:591 JMV
Surrogate: 2-Fluorobiphenyl 88.6 Limits: 44-115%02/22/23 19:591 JMV V30112
Surrogate: 2-Fluorophenol 88.6 Limits: 35-115%02/22/23 19:591 JMV V30112
Surrogate: Nitrobenzene-d5 83.8 Limits: 37-122%02/22/23 19:591 JMV V30112
Surrogate: 4-Terphenyl-d14 98.2 Limits: 54-127%02/22/23 19:591 JMV V30112
Surrogate: 2,4,6-Tribromophenol 87.1 Limits: 39-132%02/22/23 19:591 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S7
99881 Matrix:
2/14/2023 14:52
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.4 %Moisture 1 02/17/23 10:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S7
99881 Matrix:
2/14/2023 14:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.137 mg/Kg - dry 0.137 0.780Acenaphthene 1 02/23/23 13:19 V30112JMV
<0.124 mg/Kg - dry 0.124 0.780
Acenaphthylene 1 02/23/23 13:19 V30112JMV
<0.179 mg/Kg - dry 0.179 0.780Aniline 1 02/23/23 13:19 V30112JMV
<0.169 mg/Kg - dry 0.169 0.780Anthracene 1 02/23/23 13:19 V30112JMV
<0.164 mg/Kg - dry 0.164 0.780Benzo(a)anthracene 1 02/23/23 13:19 V30112JMV
<0.173 mg/Kg - dry 0.173 0.780Benzo(a)pyrene 1 02/23/23 13:19 V30112JMV
<0.172 mg/Kg - dry 0.172 0.780Benzo(b)fluoranthene 1 02/23/23 13:19 V30112JMV
<0.160 mg/Kg - dry 0.160 0.780Benzo(g,h,i)perylene 1 02/23/23 13:19 V30112JMV
<0.161 mg/Kg - dry 0.161 0.780
Benzo(k)fluoranthene 1 02/23/23 13:19 V30112JMV
<0.685 mg/Kg - dry 0.685 2.36Benzoic Acid 1 02/23/23 13:19 V30112JMV
<0.124 mg/Kg - dry 0.124 0.780Benzyl alcohol 1 02/23/23 13:19 V30112JMV
<0.139 mg/Kg - dry 0.139 0.780Bis(2-Chloroethoxy)methane 1 02/23/23 13:19 V30112JMV
<0.126 mg/Kg - dry 0.126 0.780Bis(2-Chloroethyl)ether 1 02/23/23 13:19 V30112JMV
<0.160 mg/Kg - dry 0.160 0.390Bis(2-Chloroisopropyl)ether 1 02/23/23 13:19 V30112JMV
<0.141 mg/Kg - dry 0.141 0.780Bis(2-ethylhexyl)phthalate 1 02/23/23 13:19 V30112JMV
<0.128 mg/Kg - dry 0.128 0.7804-Bromophenyl phenyl ether 1 02/23/23 13:19 V30112JMV
<0.133 mg/Kg - dry 0.133 0.390Butyl benzyl phthalate 1 02/23/23 13:19 V30112JMV
<0.109 mg/Kg - dry 0.109 0.7804-Chloro-3-methylphenol 1 02/23/23 13:19 V30112JMV
<0.132 mg/Kg - dry 0.132 0.3904-Chloroaniline 1 02/23/23 13:19 V30112JMV
<0.137 mg/Kg - dry 0.137 0.7802-Chloronaphthalene 1 02/23/23 13:19 V30112JMV
<0.116 mg/Kg - dry 0.116 0.7802-Chlorophenol 1 02/23/23 13:19 V30112JMV
<0.148 mg/Kg - dry 0.148 1.184-Chlorophenyl phenyl ether 1 02/23/23 13:19 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S7
99881 Matrix:
2/14/2023 14:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.167 mg/Kg - dry 0.167 0.780Chrysene 1 02/23/23 13:19 V30112JMV
<0.271 mg/Kg - dry 0.271 0.780
Dibenz(a,h)anthracene 1 02/23/23 13:19 V30112JMV
<0.140 mg/Kg - dry 0.140 0.780Dibenzofuran 1 02/23/23 13:19 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7801,2-Dichlorobenzene 1 02/23/23 13:19 V30112JMV
<0.115 mg/Kg - dry 0.115 0.7801,3-Dichlorobenzene 1 02/23/23 13:19 V30112JMV
<0.115 mg/Kg - dry 0.115 0.3901,4-Dichlorobenzene 1 02/23/23 13:19 V30112JMV
<0.173 mg/Kg - dry 0.173 0.7803,3'-Dichlorobenzidine 1 02/23/23 13:19 V30112JMV
<0.113 mg/Kg - dry 0.113 0.7802,4-Dichlorophenol 1 02/23/23 13:19 V30112JMV
<0.212 mg/Kg - dry 0.212 0.780
Diethyl phthalate 1 02/23/23 13:19 V30112JMV
<0.205 mg/Kg - dry 0.205 0.780Dimethyl phthalate 1 02/23/23 13:19 V30112JMV
<0.127 mg/Kg - dry 0.127 0.3902,4-Dimethylphenol 1 02/23/23 13:19 V30112JMV
<0.126 mg/Kg - dry 0.126 0.780Di-n-butyl phthalate 1 02/23/23 13:19 V30112JMV
<0.283 mg/Kg - dry 0.283 1.774,6-Dinitro-2-methylphenol 1 02/23/23 13:19 V30112JMV
<0.614 mg/Kg - dry 0.614 1.772,4-Dinitrophenol 1 02/23/23 13:19 V30112JMV
<0.114 mg/Kg - dry 0.114 0.7802,4-Dinitrotoluene 1 02/23/23 13:19 V30112JMV
<0.127 mg/Kg - dry 0.127 0.7802,6-Dinitrotoluene 1 02/23/23 13:19 V30112JMV
<0.169 mg/Kg - dry 0.169 0.390Di-n-Octyl Phthalate 1 02/23/23 13:19 V30112JMV
<0.145 mg/Kg - dry 0.145 0.780Fluoranthene 1 02/23/23 13:19 V30112JMV
<0.151 mg/Kg - dry 0.151 0.780Fluorene 1 02/23/23 13:19 V30112JMV
<0.125 mg/Kg - dry 0.125 0.780Hexachlorobenzene 1 02/23/23 13:19 V30112JMV
<0.115 mg/Kg - dry 0.115 0.780Hexachlorobutadiene 1 02/23/23 13:19 V30112JMV
<0.185 mg/Kg - dry 0.185 0.780Hexachlorocyclopentadiene 1 02/23/23 13:19 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S7
99881 Matrix:
2/14/2023 14:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.093 mg/Kg - dry 0.093 0.780Hexachloroethane 1 02/23/23 13:19 V30112JMV
<0.211 mg/Kg - dry 0.211 0.780
Indeno(1,2,3-cd)pyrene 1 02/23/23 13:19 V30112JMV
<0.225 mg/Kg - dry 0.225 0.780Isophorone 1 02/23/23 13:19 V30112JMV
<0.125 mg/Kg - dry 0.125 0.7801-Methylnaphthalene 1 02/23/23 13:19 V30112JMV
<0.118 mg/Kg - dry 0.118 0.7802-Methylnaphthalene 1 02/23/23 13:19 V30112JMV
<0.114 mg/Kg - dry 0.114 0.7802-Methylphenol 1 02/23/23 13:19 V30112JMV
<0.100 mg/Kg - dry 0.100 0.7803&4 Methylphenol 1 02/23/23 13:19 V30112JMV
<0.170 mg/Kg - dry 0.170 0.780Naphthalene 1 02/23/23 13:19 V30112JMV
<0.114 mg/Kg - dry 0.114 0.780
2-Nitroaniline 1 02/23/23 13:19 V30112JMV
<0.141 mg/Kg - dry 0.141 0.7803-Nitroaniline 1 02/23/23 13:19 V30112JMV
<0.110 mg/Kg - dry 0.110 0.3904-Nitroaniline 1 02/23/23 13:19 V30112JMV
<0.137 mg/Kg - dry 0.137 0.390Nitrobenzene 1 02/23/23 13:19 V30112JMV
<0.104 mg/Kg - dry 0.104 0.7802-Nitrophenol 1 02/23/23 13:19 V30112JMV
<0.138 mg/Kg - dry 0.138 0.7804-Nitrophenol 1 02/23/23 13:19 V30112JMV
<0.310 mg/Kg - dry 0.310 0.780N-Nitrosodimethylamine 1 02/23/23 13:19 V30112JMV
<0.213 mg/Kg - dry 0.213 0.780N-Nitrosodiphenylamine 1 02/23/23 13:19 V30112JMV
<0.139 mg/Kg - dry 0.139 0.780N-Nitroso-di-n-propylamine 1 02/23/23 13:19 V30112JMV
<0.410 mg/Kg - dry 0.410 1.18Pentachlorophenol 1 02/23/23 13:19 V30112JMV
<0.245 mg/Kg - dry 0.245 0.780Phenanthrene 1 02/23/23 13:19 V30112JMV
<0.132 mg/Kg - dry 0.132 0.780Phenol 1 02/23/23 13:19 V30112JMV
<0.158 mg/Kg - dry 0.158 0.780Pyrene 1 02/23/23 13:19 V30112JMV
<0.093 mg/Kg - dry 0.093 0.390Pyridine 1 02/23/23 13:19 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S7
99881 Matrix:
2/14/2023 14:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.126 mg/Kg - dry 0.126 0.7801,2,4-Trichlorobenzene 1 02/23/23 13:19 V30112JMV
<0.113 mg/Kg - dry 0.113 0.780
2,4,5-Trichlorophenol 1 02/23/23 13:19 V30112JMV
<0.114 mg/Kg - dry 0.114 0.7802,4,6-Trichlorophenol 1 02/23/23 13:19 V30112JMV
8270ESurrogate: Phenol-d5 89.8 Limits: 34-121%02/23/23 13:191 JMV
Surrogate: 2-Fluorobiphenyl 89.8 Limits: 44-115%02/23/23 13:191 JMV V30112
Surrogate: 2-Fluorophenol 90.7 Limits: 35-115%02/23/23 13:191 JMV V30112
Surrogate: Nitrobenzene-d5 84.4 Limits: 37-122%02/23/23 13:191 JMV V30112
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%02/23/23 13:191 JMV V30112
Surrogate: 2,4,6-Tribromophenol 95.2 Limits: 39-132%02/23/23 13:191 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S8
99882 Matrix:
2/14/2023 14:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 02/17/23 10:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S8
99882 Matrix:
2/14/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.145 mg/Kg - dry 0.145 0.825Acenaphthene 1 02/23/23 13:42 V30112JMV
<0.131 mg/Kg - dry 0.131 0.825
Acenaphthylene 1 02/23/23 13:42 V30112JMV
<0.190 mg/Kg - dry 0.190 0.825Aniline 1 02/23/23 13:42 V30112JMV
<0.178 mg/Kg - dry 0.178 0.825Anthracene 1 02/23/23 13:42 V30112JMV
<0.173 mg/Kg - dry 0.173 0.825Benzo(a)anthracene 1 02/23/23 13:42 V30112JMV
<0.183 mg/Kg - dry 0.183 0.825Benzo(a)pyrene 1 02/23/23 13:42 V30112JMV
<0.182 mg/Kg - dry 0.182 0.825Benzo(b)fluoranthene 1 02/23/23 13:42 V30112JMV
<0.170 mg/Kg - dry 0.170 0.825Benzo(g,h,i)perylene 1 02/23/23 13:42 V30112JMV
<0.171 mg/Kg - dry 0.171 0.825
Benzo(k)fluoranthene 1 02/23/23 13:42 V30112JMV
<0.725 mg/Kg - dry 0.725 2.50Benzoic Acid 1 02/23/23 13:42 V30112JMV
<0.131 mg/Kg - dry 0.131 0.825Benzyl alcohol 1 02/23/23 13:42 V30112JMV
<0.147 mg/Kg - dry 0.147 0.825Bis(2-Chloroethoxy)methane 1 02/23/23 13:42 V30112JMV
<0.133 mg/Kg - dry 0.133 0.825Bis(2-Chloroethyl)ether 1 02/23/23 13:42 V30112JMV
<0.170 mg/Kg - dry 0.170 0.412Bis(2-Chloroisopropyl)ether 1 02/23/23 13:42 V30112JMV
<0.150 mg/Kg - dry 0.150 0.825Bis(2-ethylhexyl)phthalate 1 02/23/23 13:42 V30112JMV
<0.136 mg/Kg - dry 0.136 0.8254-Bromophenyl phenyl ether 1 02/23/23 13:42 V30112JMV
<0.141 mg/Kg - dry 0.141 0.412Butyl benzyl phthalate 1 02/23/23 13:42 V30112JMV
<0.115 mg/Kg - dry 0.115 0.8254-Chloro-3-methylphenol 1 02/23/23 13:42 V30112JMV
<0.140 mg/Kg - dry 0.140 0.4124-Chloroaniline 1 02/23/23 13:42 V30112JMV
<0.145 mg/Kg - dry 0.145 0.8252-Chloronaphthalene 1 02/23/23 13:42 V30112JMV
<0.122 mg/Kg - dry 0.122 0.8252-Chlorophenol 1 02/23/23 13:42 V30112JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 02/23/23 13:42 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S8
99882 Matrix:
2/14/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.177 mg/Kg - dry 0.177 0.825Chrysene 1 02/23/23 13:42 V30112JMV
<0.287 mg/Kg - dry 0.287 0.825
Dibenz(a,h)anthracene 1 02/23/23 13:42 V30112JMV
<0.148 mg/Kg - dry 0.148 0.825Dibenzofuran 1 02/23/23 13:42 V30112JMV
<0.118 mg/Kg - dry 0.118 0.8251,2-Dichlorobenzene 1 02/23/23 13:42 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8251,3-Dichlorobenzene 1 02/23/23 13:42 V30112JMV
<0.121 mg/Kg - dry 0.121 0.4121,4-Dichlorobenzene 1 02/23/23 13:42 V30112JMV
<0.183 mg/Kg - dry 0.183 0.8253,3'-Dichlorobenzidine 1 02/23/23 13:42 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8252,4-Dichlorophenol 1 02/23/23 13:42 V30112JMV
<0.225 mg/Kg - dry 0.225 0.825
Diethyl phthalate 1 02/23/23 13:42 V30112JMV
<0.217 mg/Kg - dry 0.217 0.825Dimethyl phthalate 1 02/23/23 13:42 V30112JMV
<0.135 mg/Kg - dry 0.135 0.4122,4-Dimethylphenol 1 02/23/23 13:42 V30112JMV
<0.133 mg/Kg - dry 0.133 0.825Di-n-butyl phthalate 1 02/23/23 13:42 V30112JMV
<0.300 mg/Kg - dry 0.300 1.884,6-Dinitro-2-methylphenol 1 02/23/23 13:42 V30112JMV
<0.650 mg/Kg - dry 0.650 1.882,4-Dinitrophenol 1 02/23/23 13:42 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8252,4-Dinitrotoluene 1 02/23/23 13:42 V30112JMV
<0.135 mg/Kg - dry 0.135 0.8252,6-Dinitrotoluene 1 02/23/23 13:42 V30112JMV
<0.178 mg/Kg - dry 0.178 0.412Di-n-Octyl Phthalate 1 02/23/23 13:42 V30112JMV
<0.153 mg/Kg - dry 0.153 0.825Fluoranthene 1 02/23/23 13:42 V30112JMV
<0.160 mg/Kg - dry 0.160 0.825Fluorene 1 02/23/23 13:42 V30112JMV
<0.132 mg/Kg - dry 0.132 0.825Hexachlorobenzene 1 02/23/23 13:42 V30112JMV
<0.122 mg/Kg - dry 0.122 0.825Hexachlorobutadiene 1 02/23/23 13:42 V30112JMV
<0.196 mg/Kg - dry 0.196 0.825Hexachlorocyclopentadiene 1 02/23/23 13:42 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S8
99882 Matrix:
2/14/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.099 mg/Kg - dry 0.099 0.825Hexachloroethane 1 02/23/23 13:42 V30112JMV
<0.223 mg/Kg - dry 0.223 0.825
Indeno(1,2,3-cd)pyrene 1 02/23/23 13:42 V30112JMV
<0.238 mg/Kg - dry 0.238 0.825Isophorone 1 02/23/23 13:42 V30112JMV
<0.132 mg/Kg - dry 0.132 0.8251-Methylnaphthalene 1 02/23/23 13:42 V30112JMV
<0.125 mg/Kg - dry 0.125 0.8252-Methylnaphthalene 1 02/23/23 13:42 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8252-Methylphenol 1 02/23/23 13:42 V30112JMV
<0.106 mg/Kg - dry 0.106 0.8253&4 Methylphenol 1 02/23/23 13:42 V30112JMV
<0.180 mg/Kg - dry 0.180 0.825Naphthalene 1 02/23/23 13:42 V30112JMV
<0.120 mg/Kg - dry 0.120 0.825
2-Nitroaniline 1 02/23/23 13:42 V30112JMV
<0.150 mg/Kg - dry 0.150 0.8253-Nitroaniline 1 02/23/23 13:42 V30112JMV
<0.116 mg/Kg - dry 0.116 0.4124-Nitroaniline 1 02/23/23 13:42 V30112JMV
<0.145 mg/Kg - dry 0.145 0.412Nitrobenzene 1 02/23/23 13:42 V30112JMV
<0.111 mg/Kg - dry 0.111 0.8252-Nitrophenol 1 02/23/23 13:42 V30112JMV
<0.146 mg/Kg - dry 0.146 0.8254-Nitrophenol 1 02/23/23 13:42 V30112JMV
<0.328 mg/Kg - dry 0.328 0.825N-Nitrosodimethylamine 1 02/23/23 13:42 V30112JMV
<0.226 mg/Kg - dry 0.226 0.825N-Nitrosodiphenylamine 1 02/23/23 13:42 V30112JMV
<0.147 mg/Kg - dry 0.147 0.825N-Nitroso-di-n-propylamine 1 02/23/23 13:42 V30112JMV
<0.433 mg/Kg - dry 0.433 1.25Pentachlorophenol 1 02/23/23 13:42 V30112JMV
<0.260 mg/Kg - dry 0.260 0.825Phenanthrene 1 02/23/23 13:42 V30112JMV
<0.140 mg/Kg - dry 0.140 0.825Phenol 1 02/23/23 13:42 V30112JMV
<0.167 mg/Kg - dry 0.167 0.825Pyrene 1 02/23/23 13:42 V30112JMV
<0.099 mg/Kg - dry 0.099 0.412Pyridine 1 02/23/23 13:42 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S8
99882 Matrix:
2/14/2023 14:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.133 mg/Kg - dry 0.133 0.8251,2,4-Trichlorobenzene 1 02/23/23 13:42 V30112JMV
<0.120 mg/Kg - dry 0.120 0.825
2,4,5-Trichlorophenol 1 02/23/23 13:42 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8252,4,6-Trichlorophenol 1 02/23/23 13:42 V30112JMV
8270ESurrogate: Phenol-d5 81.7 Limits: 34-121%02/23/23 13:421 JMV
Surrogate: 2-Fluorobiphenyl 81.3 Limits: 44-115%02/23/23 13:421 JMV V30112
Surrogate: 2-Fluorophenol 84.1 Limits: 35-115%02/23/23 13:421 JMV V30112
Surrogate: Nitrobenzene-d5 75.3 Limits: 37-122%02/23/23 13:421 JMV V30112
Surrogate: 4-Terphenyl-d14 89.8 Limits: 54-127%02/23/23 13:421 JMV V30112
Surrogate: 2,4,6-Tribromophenol 82.9 Limits: 39-132%02/23/23 13:421 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S9
99883 Matrix:
2/14/2023 14:59
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 02/17/23 10:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S9
99883 Matrix:
2/14/2023 14:59
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.144 mg/Kg - dry 0.144 0.824Acenaphthene 1 02/23/23 14:04 V30112JMV
<0.130 mg/Kg - dry 0.130 0.824
Acenaphthylene 1 02/23/23 14:04 V30112JMV
<0.189 mg/Kg - dry 0.189 0.824Aniline 1 02/23/23 14:04 V30112JMV
<0.178 mg/Kg - dry 0.178 0.824Anthracene 1 02/23/23 14:04 V30112JMV
<0.173 mg/Kg - dry 0.173 0.824Benzo(a)anthracene 1 02/23/23 14:04 V30112JMV
<0.183 mg/Kg - dry 0.183 0.824Benzo(a)pyrene 1 02/23/23 14:04 V30112JMV
<0.182 mg/Kg - dry 0.182 0.824Benzo(b)fluoranthene 1 02/23/23 14:04 V30112JMV
<0.169 mg/Kg - dry 0.169 0.824Benzo(g,h,i)perylene 1 02/23/23 14:04 V30112JMV
<0.170 mg/Kg - dry 0.170 0.824
Benzo(k)fluoranthene 1 02/23/23 14:04 V30112JMV
<0.723 mg/Kg - dry 0.723 2.49Benzoic Acid 1 02/23/23 14:04 V30112JMV
<0.130 mg/Kg - dry 0.130 0.824Benzyl alcohol 1 02/23/23 14:04 V30112JMV
<0.147 mg/Kg - dry 0.147 0.824Bis(2-Chloroethoxy)methane 1 02/23/23 14:04 V30112JMV
<0.133 mg/Kg - dry 0.133 0.824Bis(2-Chloroethyl)ether 1 02/23/23 14:04 V30112JMV
<0.169 mg/Kg - dry 0.169 0.412Bis(2-Chloroisopropyl)ether 1 02/23/23 14:04 V30112JMV
<0.149 mg/Kg - dry 0.149 0.824Bis(2-ethylhexyl)phthalate 1 02/23/23 14:04 V30112JMV
<0.135 mg/Kg - dry 0.135 0.8244-Bromophenyl phenyl ether 1 02/23/23 14:04 V30112JMV
<0.140 mg/Kg - dry 0.140 0.412Butyl benzyl phthalate 1 02/23/23 14:04 V30112JMV
<0.115 mg/Kg - dry 0.115 0.8244-Chloro-3-methylphenol 1 02/23/23 14:04 V30112JMV
<0.139 mg/Kg - dry 0.139 0.4124-Chloroaniline 1 02/23/23 14:04 V30112JMV
<0.144 mg/Kg - dry 0.144 0.8242-Chloronaphthalene 1 02/23/23 14:04 V30112JMV
<0.122 mg/Kg - dry 0.122 0.8242-Chlorophenol 1 02/23/23 14:04 V30112JMV
<0.157 mg/Kg - dry 0.157 1.254-Chlorophenyl phenyl ether 1 02/23/23 14:04 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S9
99883 Matrix:
2/14/2023 14:59
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.177 mg/Kg - dry 0.177 0.824Chrysene 1 02/23/23 14:04 V30112JMV
<0.286 mg/Kg - dry 0.286 0.824
Dibenz(a,h)anthracene 1 02/23/23 14:04 V30112JMV
<0.148 mg/Kg - dry 0.148 0.824Dibenzofuran 1 02/23/23 14:04 V30112JMV
<0.117 mg/Kg - dry 0.117 0.8241,2-Dichlorobenzene 1 02/23/23 14:04 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8241,3-Dichlorobenzene 1 02/23/23 14:04 V30112JMV
<0.121 mg/Kg - dry 0.121 0.4121,4-Dichlorobenzene 1 02/23/23 14:04 V30112JMV
<0.183 mg/Kg - dry 0.183 0.8243,3'-Dichlorobenzidine 1 02/23/23 14:04 V30112JMV
<0.119 mg/Kg - dry 0.119 0.8242,4-Dichlorophenol 1 02/23/23 14:04 V30112JMV
<0.224 mg/Kg - dry 0.224 0.824
Diethyl phthalate 1 02/23/23 14:04 V30112JMV
<0.216 mg/Kg - dry 0.216 0.824Dimethyl phthalate 1 02/23/23 14:04 V30112JMV
<0.134 mg/Kg - dry 0.134 0.4122,4-Dimethylphenol 1 02/23/23 14:04 V30112JMV
<0.133 mg/Kg - dry 0.133 0.824Di-n-butyl phthalate 1 02/23/23 14:04 V30112JMV
<0.299 mg/Kg - dry 0.299 1.874,6-Dinitro-2-methylphenol 1 02/23/23 14:04 V30112JMV
<0.648 mg/Kg - dry 0.648 1.872,4-Dinitrophenol 1 02/23/23 14:04 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8242,4-Dinitrotoluene 1 02/23/23 14:04 V30112JMV
<0.134 mg/Kg - dry 0.134 0.8242,6-Dinitrotoluene 1 02/23/23 14:04 V30112JMV
<0.178 mg/Kg - dry 0.178 0.412Di-n-Octyl Phthalate 1 02/23/23 14:04 V30112JMV
<0.153 mg/Kg - dry 0.153 0.824Fluoranthene 1 02/23/23 14:04 V30112JMV
<0.159 mg/Kg - dry 0.159 0.824Fluorene 1 02/23/23 14:04 V30112JMV
<0.132 mg/Kg - dry 0.132 0.824Hexachlorobenzene 1 02/23/23 14:04 V30112JMV
<0.121 mg/Kg - dry 0.121 0.824Hexachlorobutadiene 1 02/23/23 14:04 V30112JMV
<0.195 mg/Kg - dry 0.195 0.824Hexachlorocyclopentadiene 1 02/23/23 14:04 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S9
99883 Matrix:
2/14/2023 14:59
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.098 mg/Kg - dry 0.098 0.824Hexachloroethane 1 02/23/23 14:04 V30112JMV
<0.223 mg/Kg - dry 0.223 0.824
Indeno(1,2,3-cd)pyrene 1 02/23/23 14:04 V30112JMV
<0.238 mg/Kg - dry 0.238 0.824Isophorone 1 02/23/23 14:04 V30112JMV
<0.132 mg/Kg - dry 0.132 0.8241-Methylnaphthalene 1 02/23/23 14:04 V30112JMV
<0.124 mg/Kg - dry 0.124 0.8242-Methylnaphthalene 1 02/23/23 14:04 V30112JMV
<0.121 mg/Kg - dry 0.121 0.8242-Methylphenol 1 02/23/23 14:04 V30112JMV
<0.105 mg/Kg - dry 0.105 0.8243&4 Methylphenol 1 02/23/23 14:04 V30112JMV
<0.179 mg/Kg - dry 0.179 0.824Naphthalene 1 02/23/23 14:04 V30112JMV
<0.120 mg/Kg - dry 0.120 0.824
2-Nitroaniline 1 02/23/23 14:04 V30112JMV
<0.149 mg/Kg - dry 0.149 0.8243-Nitroaniline 1 02/23/23 14:04 V30112JMV
<0.116 mg/Kg - dry 0.116 0.4124-Nitroaniline 1 02/23/23 14:04 V30112JMV
<0.144 mg/Kg - dry 0.144 0.412Nitrobenzene 1 02/23/23 14:04 V30112JMV
<0.110 mg/Kg - dry 0.110 0.8242-Nitrophenol 1 02/23/23 14:04 V30112JMV
<0.145 mg/Kg - dry 0.145 0.8244-Nitrophenol 1 02/23/23 14:04 V30112JMV
<0.327 mg/Kg - dry 0.327 0.824N-Nitrosodimethylamine 1 02/23/23 14:04 V30112JMV
<0.225 mg/Kg - dry 0.225 0.824N-Nitrosodiphenylamine 1 02/23/23 14:04 V30112JMV
<0.147 mg/Kg - dry 0.147 0.824N-Nitroso-di-n-propylamine 1 02/23/23 14:04 V30112JMV
<0.432 mg/Kg - dry 0.432 1.25Pentachlorophenol 1 02/23/23 14:04 V30112JMV
<0.259 mg/Kg - dry 0.259 0.824Phenanthrene 1 02/23/23 14:04 V30112JMV
<0.139 mg/Kg - dry 0.139 0.824Phenol 1 02/23/23 14:04 V30112JMV
<0.167 mg/Kg - dry 0.167 0.824Pyrene 1 02/23/23 14:04 V30112JMV
<0.099 mg/Kg - dry 0.099 0.412Pyridine 1 02/23/23 14:04 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S9
99883 Matrix:
2/14/2023 14:59
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.133 mg/Kg - dry 0.133 0.8241,2,4-Trichlorobenzene 1 02/23/23 14:04 V30112JMV
<0.120 mg/Kg - dry 0.120 0.824
2,4,5-Trichlorophenol 1 02/23/23 14:04 V30112JMV
<0.120 mg/Kg - dry 0.120 0.8242,4,6-Trichlorophenol 1 02/23/23 14:04 V30112JMV
8270ESurrogate: Phenol-d5 83.8 Limits: 34-121%02/23/23 14:041 JMV
Surrogate: 2-Fluorobiphenyl 85.0 Limits: 44-115%02/23/23 14:041 JMV V30112
Surrogate: 2-Fluorophenol 85.3 Limits: 35-115%02/23/23 14:041 JMV V30112
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%02/23/23 14:041 JMV V30112
Surrogate: 4-Terphenyl-d14 95.8 Limits: 54-127%02/23/23 14:041 JMV V30112
Surrogate: 2,4,6-Tribromophenol 86.2 Limits: 39-132%02/23/23 14:041 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S10
99884 Matrix:
2/14/2023 15:01
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.5 %Moisture 1 02/17/23 10:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S10
99884 Matrix:
2/14/2023 15:01
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.134 mg/Kg - dry 0.134 0.763Acenaphthene 1 02/23/23 14:27 V30112JMV
<0.121 mg/Kg - dry 0.121 0.763
Acenaphthylene 1 02/23/23 14:27 V30112JMV
<0.175 mg/Kg - dry 0.175 0.763Aniline 1 02/23/23 14:27 V30112JMV
<0.165 mg/Kg - dry 0.165 0.763Anthracene 1 02/23/23 14:27 V30112JMV
<0.160 mg/Kg - dry 0.160 0.763Benzo(a)anthracene 1 02/23/23 14:27 V30112JMV
<0.169 mg/Kg - dry 0.169 0.763Benzo(a)pyrene 1 02/23/23 14:27 V30112JMV
<0.168 mg/Kg - dry 0.168 0.763Benzo(b)fluoranthene 1 02/23/23 14:27 V30112JMV
<0.157 mg/Kg - dry 0.157 0.763Benzo(g,h,i)perylene 1 02/23/23 14:27 V30112JMV
<0.158 mg/Kg - dry 0.158 0.763
Benzo(k)fluoranthene 1 02/23/23 14:27 V30112JMV
<0.670 mg/Kg - dry 0.670 2.31Benzoic Acid 1 02/23/23 14:27 V30112JMV
<0.121 mg/Kg - dry 0.121 0.763Benzyl alcohol 1 02/23/23 14:27 V30112JMV
<0.136 mg/Kg - dry 0.136 0.763Bis(2-Chloroethoxy)methane 1 02/23/23 14:27 V30112JMV
<0.123 mg/Kg - dry 0.123 0.763Bis(2-Chloroethyl)ether 1 02/23/23 14:27 V30112JMV
<0.157 mg/Kg - dry 0.157 0.381Bis(2-Chloroisopropyl)ether 1 02/23/23 14:27 V30112JMV
<0.138 mg/Kg - dry 0.138 0.763Bis(2-ethylhexyl)phthalate 1 02/23/23 14:27 V30112JMV
<0.126 mg/Kg - dry 0.126 0.7634-Bromophenyl phenyl ether 1 02/23/23 14:27 V30112JMV
<0.130 mg/Kg - dry 0.130 0.381Butyl benzyl phthalate 1 02/23/23 14:27 V30112JMV
<0.106 mg/Kg - dry 0.106 0.7634-Chloro-3-methylphenol 1 02/23/23 14:27 V30112JMV
<0.129 mg/Kg - dry 0.129 0.3814-Chloroaniline 1 02/23/23 14:27 V30112JMV
<0.134 mg/Kg - dry 0.134 0.7632-Chloronaphthalene 1 02/23/23 14:27 V30112JMV
<0.113 mg/Kg - dry 0.113 0.7632-Chlorophenol 1 02/23/23 14:27 V30112JMV
<0.145 mg/Kg - dry 0.145 1.164-Chlorophenyl phenyl ether 1 02/23/23 14:27 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S10
99884 Matrix:
2/14/2023 15:01
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.164 mg/Kg - dry 0.164 0.763Chrysene 1 02/23/23 14:27 V30112JMV
<0.265 mg/Kg - dry 0.265 0.763
Dibenz(a,h)anthracene 1 02/23/23 14:27 V30112JMV
<0.137 mg/Kg - dry 0.137 0.763Dibenzofuran 1 02/23/23 14:27 V30112JMV
<0.109 mg/Kg - dry 0.109 0.7631,2-Dichlorobenzene 1 02/23/23 14:27 V30112JMV
<0.112 mg/Kg - dry 0.112 0.7631,3-Dichlorobenzene 1 02/23/23 14:27 V30112JMV
<0.112 mg/Kg - dry 0.112 0.3811,4-Dichlorobenzene 1 02/23/23 14:27 V30112JMV
<0.169 mg/Kg - dry 0.169 0.7633,3'-Dichlorobenzidine 1 02/23/23 14:27 V30112JMV
<0.110 mg/Kg - dry 0.110 0.7632,4-Dichlorophenol 1 02/23/23 14:27 V30112JMV
<0.208 mg/Kg - dry 0.208 0.763
Diethyl phthalate 1 02/23/23 14:27 V30112JMV
<0.201 mg/Kg - dry 0.201 0.763Dimethyl phthalate 1 02/23/23 14:27 V30112JMV
<0.124 mg/Kg - dry 0.124 0.3812,4-Dimethylphenol 1 02/23/23 14:27 V30112JMV
<0.123 mg/Kg - dry 0.123 0.763Di-n-butyl phthalate 1 02/23/23 14:27 V30112JMV
<0.277 mg/Kg - dry 0.277 1.734,6-Dinitro-2-methylphenol 1 02/23/23 14:27 V30112JMV
<0.601 mg/Kg - dry 0.601 1.732,4-Dinitrophenol 1 02/23/23 14:27 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7632,4-Dinitrotoluene 1 02/23/23 14:27 V30112JMV
<0.124 mg/Kg - dry 0.124 0.7632,6-Dinitrotoluene 1 02/23/23 14:27 V30112JMV
<0.165 mg/Kg - dry 0.165 0.381Di-n-Octyl Phthalate 1 02/23/23 14:27 V30112JMV
<0.142 mg/Kg - dry 0.142 0.763Fluoranthene 1 02/23/23 14:27 V30112JMV
<0.147 mg/Kg - dry 0.147 0.763Fluorene 1 02/23/23 14:27 V30112JMV
<0.122 mg/Kg - dry 0.122 0.763Hexachlorobenzene 1 02/23/23 14:27 V30112JMV
<0.112 mg/Kg - dry 0.112 0.763Hexachlorobutadiene 1 02/23/23 14:27 V30112JMV
<0.181 mg/Kg - dry 0.181 0.763Hexachlorocyclopentadiene 1 02/23/23 14:27 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S10
99884 Matrix:
2/14/2023 15:01
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.091 mg/Kg - dry 0.091 0.763Hexachloroethane 1 02/23/23 14:27 V30112JMV
<0.206 mg/Kg - dry 0.206 0.763
Indeno(1,2,3-cd)pyrene 1 02/23/23 14:27 V30112JMV
<0.220 mg/Kg - dry 0.220 0.763Isophorone 1 02/23/23 14:27 V30112JMV
<0.122 mg/Kg - dry 0.122 0.7631-Methylnaphthalene 1 02/23/23 14:27 V30112JMV
<0.115 mg/Kg - dry 0.115 0.7632-Methylnaphthalene 1 02/23/23 14:27 V30112JMV
<0.112 mg/Kg - dry 0.112 0.7632-Methylphenol 1 02/23/23 14:27 V30112JMV
<0.098 mg/Kg - dry 0.098 0.7633&4 Methylphenol 1 02/23/23 14:27 V30112JMV
<0.166 mg/Kg - dry 0.166 0.763Naphthalene 1 02/23/23 14:27 V30112JMV
<0.111 mg/Kg - dry 0.111 0.763
2-Nitroaniline 1 02/23/23 14:27 V30112JMV
<0.138 mg/Kg - dry 0.138 0.7633-Nitroaniline 1 02/23/23 14:27 V30112JMV
<0.107 mg/Kg - dry 0.107 0.3814-Nitroaniline 1 02/23/23 14:27 V30112JMV
<0.134 mg/Kg - dry 0.134 0.381Nitrobenzene 1 02/23/23 14:27 V30112JMV
<0.102 mg/Kg - dry 0.102 0.7632-Nitrophenol 1 02/23/23 14:27 V30112JMV
<0.135 mg/Kg - dry 0.135 0.7634-Nitrophenol 1 02/23/23 14:27 V30112JMV
<0.304 mg/Kg - dry 0.304 0.763N-Nitrosodimethylamine 1 02/23/23 14:27 V30112JMV
<0.209 mg/Kg - dry 0.209 0.763N-Nitrosodiphenylamine 1 02/23/23 14:27 V30112JMV
<0.136 mg/Kg - dry 0.136 0.763N-Nitroso-di-n-propylamine 1 02/23/23 14:27 V30112JMV
<0.401 mg/Kg - dry 0.401 1.16Pentachlorophenol 1 02/23/23 14:27 V30112JMV
<0.240 mg/Kg - dry 0.240 0.763Phenanthrene 1 02/23/23 14:27 V30112JMV
<0.129 mg/Kg - dry 0.129 0.763Phenol 1 02/23/23 14:27 V30112JMV
<0.154 mg/Kg - dry 0.154 0.763Pyrene 1 02/23/23 14:27 V30112JMV
<0.091 mg/Kg - dry 0.091 0.381Pyridine 1 02/23/23 14:27 V30112JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 68
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27513
23-047-0008
00122
Suite 110
Falcon Engineering
1210 Trinity Road
Christopher Burkhardt
Cary
Received : 02/16/2023
Solomon
Report Date : 02/27/2023
Sample ID :
Lab No :
Sampled:S10
99884 Matrix:
2/14/2023 15:01
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30032 02/22/23 11:00
<0.123 mg/Kg - dry 0.123 0.7631,2,4-Trichlorobenzene 1 02/23/23 14:27 V30112JMV
<0.111 mg/Kg - dry 0.111 0.763
2,4,5-Trichlorophenol 1 02/23/23 14:27 V30112JMV
<0.111 mg/Kg - dry 0.111 0.7632,4,6-Trichlorophenol 1 02/23/23 14:27 V30112JMV
8270ESurrogate: Phenol-d5 88.9 Limits: 34-121%02/23/23 14:271 JMV
Surrogate: 2-Fluorobiphenyl 91.0 Limits: 44-115%02/23/23 14:271 JMV V30112
Surrogate: 2-Fluorophenol 89.2 Limits: 35-115%02/23/23 14:271 JMV V30112
Surrogate: Nitrobenzene-d5 86.1 Limits: 37-122%02/23/23 14:271 JMV V30112
Surrogate: 4-Terphenyl-d14 100 Limits: 54-127%02/23/23 14:271 JMV V30112
Surrogate: 2,4,6-Tribromophenol 90.1 Limits: 39-132%02/23/23 14:271 JMV V30112
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
Associated Lab Samples: 99875, 99876, 99877, 99878, 99879, 99880, 99881, 99882, 99883, 99884
LRB-V30032 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/22/23 15:510.6600.116<0.116mg/KgAcenaphthene
02/22/23 15:510.6600.105<0.105mg/KgAcenaphthylene
02/22/23 15:510.6600.152<0.152mg/KgAniline
02/22/23 15:510.6600.143<0.143mg/KgAnthracene
02/22/23 15:510.6600.139<0.139mg/KgBenzo(a)anthracene
02/22/23 15:510.6600.147<0.147mg/KgBenzo(a)pyrene
02/22/23 15:510.6600.146<0.146mg/KgBenzo(b)fluoranthene
02/22/23 15:510.6600.136<0.136mg/KgBenzo(g,h,i)perylene
02/22/23 15:510.6600.137<0.137mg/KgBenzo(k)fluoranthene
02/22/23 15:512.000.580<0.580mg/KgBenzoic Acid
02/22/23 15:510.6600.105<0.105mg/KgBenzyl alcohol
02/22/23 15:510.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
02/22/23 15:510.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
02/22/23 15:510.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
02/22/23 15:510.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
02/22/23 15:510.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
02/22/23 15:510.3300.113<0.113mg/KgButyl benzyl phthalate
02/22/23 15:510.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
02/22/23 15:510.3300.112<0.112mg/Kg4-Chloroaniline
02/22/23 15:510.6600.116<0.116mg/Kg2-Chloronaphthalene
02/22/23 15:510.6600.098<0.098mg/Kg2-Chlorophenol
02/22/23 15:511.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
02/22/23 15:510.6600.142<0.142mg/KgChrysene
02/22/23 15:510.6600.230<0.230mg/KgDibenz(a,h)anthracene
02/22/23 15:510.6600.119<0.119mg/KgDibenzofuran
02/22/23 15:510.6600.094<0.094mg/Kg1,2-Dichlorobenzene
02/22/23 15:510.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 1 of 11Date:02/27/2023 10:52 AM
Page 56 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
Associated Lab Samples: 99875, 99876, 99877, 99878, 99879, 99880, 99881, 99882, 99883, 99884
LRB-V30032 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/22/23 15:510.3300.097<0.097mg/Kg1,4-Dichlorobenzene
02/22/23 15:510.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
02/22/23 15:510.6600.095<0.095mg/Kg2,4-Dichlorophenol
02/22/23 15:510.6600.180<0.180mg/KgDiethyl phthalate
02/22/23 15:510.6600.174<0.174mg/KgDimethyl phthalate
02/22/23 15:510.3300.108<0.108mg/Kg2,4-Dimethylphenol
02/22/23 15:510.6600.107<0.107mg/KgDi-n-butyl phthalate
02/22/23 15:511.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
02/22/23 15:511.500.520<0.520mg/Kg2,4-Dinitrophenol
02/22/23 15:510.6600.096<0.096mg/Kg2,4-Dinitrotoluene
02/22/23 15:510.6600.108<0.108mg/Kg2,6-Dinitrotoluene
02/22/23 15:510.3300.143<0.143mg/KgDi-n-Octyl Phthalate
02/22/23 15:510.6600.123<0.123mg/KgFluoranthene
02/22/23 15:510.6600.128<0.128mg/KgFluorene
02/22/23 15:510.6600.106<0.106mg/KgHexachlorobenzene
02/22/23 15:510.6600.097<0.097mg/KgHexachlorobutadiene
02/22/23 15:510.6600.157<0.157mg/KgHexachlorocyclopentadiene
02/22/23 15:510.6600.079<0.079mg/KgHexachloroethane
02/22/23 15:510.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
02/22/23 15:510.6600.191<0.191mg/KgIsophorone
02/22/23 15:510.6600.106<0.106mg/Kg1-Methylnaphthalene
02/22/23 15:510.6600.100<0.100mg/Kg2-Methylnaphthalene
02/22/23 15:510.6600.097<0.097mg/Kg2-Methylphenol
02/22/23 15:510.6600.084<0.084mg/Kg3&4 Methylphenol
02/22/23 15:510.6600.144<0.144mg/KgNaphthalene
02/22/23 15:510.6600.096<0.096mg/Kg2-Nitroaniline
02/22/23 15:510.6600.120<0.120mg/Kg3-Nitroaniline
Page 2 of 11Date:02/27/2023 10:52 AM
Page 57 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
Associated Lab Samples: 99875, 99876, 99877, 99878, 99879, 99880, 99881, 99882, 99883, 99884
LRB-V30032 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
02/22/23 15:510.3300.093<0.093mg/Kg4-Nitroaniline
02/22/23 15:510.3300.116<0.116mg/KgNitrobenzene
02/22/23 15:510.6600.088<0.088mg/Kg2-Nitrophenol
02/22/23 15:510.6600.117<0.117mg/Kg4-Nitrophenol
02/22/23 15:510.6600.263<0.263mg/KgN-Nitrosodimethylamine
02/22/23 15:510.6600.181<0.181mg/KgN-Nitrosodiphenylamine
02/22/23 15:510.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
02/22/23 15:511.000.347<0.347mg/KgPentachlorophenol
02/22/23 15:510.6600.208<0.208mg/KgPhenanthrene
02/22/23 15:510.6600.112<0.112mg/KgPhenol
02/22/23 15:510.6600.134<0.134mg/KgPyrene
02/22/23 15:510.3300.079<0.079mg/KgPyridine
02/22/23 15:510.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
02/22/23 15:510.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
02/22/23 15:510.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
02/22/23 15:512-Fluorobiphenyl (S)88.0 44-115
02/22/23 15:512-Fluorophenol (S)90.0 35-115
02/22/23 15:51Nitrobenzene-d5 (S)82.6 37-122
02/22/23 15:514-Terphenyl-d14 (S)100 54-127
02/22/23 15:512,4,6-Tribromophenol (S)85.2 39-132
02/22/23 15:51Phenol-d5 (S)87.0 34-121
LCS-V30032Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.01.571.67mg/KgAcenaphthene 40-123
93.41.561.67mg/KgAcenaphthylene 32-132
Page 3 of 11Date:02/27/2023 10:52 AM
Page 58 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
LCS-V30032Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
235*3.931.67mg/KgAniline 12-197
98.21.641.67mg/KgAnthracene 47-123
96.41.611.67mg/KgBenzo(a)anthracene 49-126
1101.841.67mg/KgBenzo(a)pyrene 45-129
98.81.651.67mg/KgBenzo(b)fluoranthene 45-132
99.41.661.67mg/KgBenzo(g,h,i)perylene 43-134
1001.671.67mg/KgBenzo(k)fluoranthene 47-132
38.00.6361.67mg/KgBenzoic Acid 10-83
95.21.591.67mg/KgBenzyl alcohol 29-122
89.81.501.67mg/KgBis(2-Chloroethoxy)methane 36-121
92.21.541.67mg/KgBis(2-Chloroethyl)ether 31-120
1031.721.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1081.801.67mg/KgBis(2-ethylhexyl)phthalate 51-133
96.41.611.67mg/Kg4-Bromophenyl phenyl ether 46-124
1131.891.67mg/KgButyl benzyl phthalate 48-132
79.61.331.67mg/Kg4-Chloro-3-methylphenol 45-122
80.81.351.67mg/Kg4-Chloroaniline 17-106
95.21.591.67mg/Kg2-Chloronaphthalene 41-114
93.41.561.67mg/Kg2-Chlorophenol 34-121
90.41.511.67mg/Kg4-Chlorophenyl phenyl ether 45-121
98.21.641.67mg/KgChrysene 50-124
98.21.641.67mg/KgDibenz(a,h)anthracene 45-134
91.61.531.67mg/KgDibenzofuran 44-120
85.61.431.67mg/Kg1,2-Dichlorobenzene 33-117
81.41.361.67mg/Kg1,3-Dichlorobenzene 30-115
83.21.391.67mg/Kg1,4-Dichlorobenzene 31-115
75.41.261.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 4 of 11* QC Fail Date:02/27/2023 10:52 AM
Page 59 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
LCS-V30032Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.01.371.67mg/Kg2,4-Dichlorophenol 40-122
94.61.581.67mg/KgDiethyl phthalate 50-124
92.81.551.67mg/KgDimethyl phthalate 48-124
89.21.491.67mg/Kg2,4-Dimethylphenol 30-127
1071.781.67mg/KgDi-n-butyl phthalate 51-128
50.90.8511.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
36.70.6141.67mg/Kg2,4-Dinitrophenol 27-129
95.81.601.67mg/Kg2,4-Dinitrotoluene 48-126
96.41.611.67mg/Kg2,6-Dinitrotoluene 46-124
1071.781.67mg/KgDi-n-Octyl Phthalate 45-140
93.41.561.67mg/KgFluoranthene 50-127
93.41.561.67mg/KgFluorene 43-125
96.41.611.67mg/KgHexachlorobenzene 45-122
76.61.281.67mg/KgHexachlorobutadiene 32-123
46.10.7701.67mg/KgHexachlorocyclopentadiene 32-117
81.41.361.67mg/KgHexachloroethane 28-117
97.01.621.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
80.21.341.67mg/KgIsophorone 30-122
83.21.391.67mg/Kg1-Methylnaphthalene 40-119
78.41.311.67mg/Kg2-Methylnaphthalene 38-122
97.61.631.67mg/Kg2-Methylphenol 32-122
83.81.401.67mg/Kg3&4 Methylphenol 34-119
82.01.371.67mg/KgNaphthalene 35-123
96.41.611.67mg/Kg2-Nitroaniline 44-127
91.61.531.67mg/Kg3-Nitroaniline 33-119
85.61.431.67mg/Kg4-Nitroaniline 63-147
86.81.451.67mg/KgNitrobenzene 34-122
Page 5 of 11Date:02/27/2023 10:52 AM
Page 60 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
LCS-V30032Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2-Nitrophenol 36-123
1051.751.67mg/Kg4-Nitrophenol 30-132
82.01.371.67mg/KgN-Nitrosodimethylamine 10-146
1202.001.67mg/KgN-Nitrosodiphenylamine 38-127
91.01.521.67mg/KgN-Nitroso-di-n-propylamine 36-120
1051.751.67mg/KgPentachlorophenol 25-133
97.01.621.67mg/KgPhenanthrene 50-121
98.81.651.67mg/KgPhenol 34-121
1021.711.67mg/KgPyrene 47-127
59.50.9951.67mg/KgPyridine 10-80
77.21.291.67mg/Kg1,2,4-Trichlorobenzene 34-118
89.81.501.67mg/Kg2,4,5-Trichlorophenol 41-124
89.21.491.67mg/Kg2,4,6-Trichlorophenol 39-126
94.62-Fluorobiphenyl (S)44-115
97.82-Fluorophenol (S)35-115
81.4Nitrobenzene-d5 (S)37-122
1044-Terphenyl-d14 (S)54-127
92.12,4,6-Tribromophenol (S)39-132
93.9Phenol-d5 (S)34-121
V 99866-MS-V30032 V 99866-MSD-V30032Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.38 82.61.471.671.67<0.116mg/KgAcenaphthene 88.0 40-123 6.3 20
1.38 82.61.461.671.67<0.105mg/KgAcenaphthylene 87.4 32-132 5.6 20
2.51 1502.831.671.67<0.152mg/KgAniline 169 12-197 11.9 20
Page 6 of 11Date:02/27/2023 10:52 AM
Page 61 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
V 99866-MS-V30032 V 99866-MSD-V30032Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.45 86.81.581.671.67<0.143mg/KgAnthracene 94.6 47-123 8.5 20
1.41 84.41.541.671.67<0.139mg/KgBenzo(a)anthracene 92.2 49-126 8.8 20
1.60 95.81.751.671.67<0.147mg/KgBenzo(a)pyrene 105 45-129 8.9 20
1.46 87.41.591.671.67<0.146mg/KgBenzo(b)fluoranthene 95.2 45-132 8.5 20
1.46 87.41.591.671.67<0.136mg/KgBenzo(g,h,i)perylene 95.2 43-134 8.5 20
1.44 86.21.561.671.67<0.137mg/KgBenzo(k)fluoranthene 93.4 47-132 8.0 20
1.31 78.41.401.671.67<0.580mg/KgBenzoic Acid 83.8*10-83 6.6 20
1.46 87.41.541.671.67<0.105mg/KgBenzyl alcohol 92.2 29-122 5.3 20
1.34 80.21.421.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 85.0 36-121 5.7 20
1.34 80.21.381.671.67<0.107mg/KgBis(2-Chloroethyl)ether 82.6 31-120 2.9 20
1.53 91.61.551.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 92.8 33-131 1.2 20
1.60 95.81.741.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 104 51-133 8.3 20
1.45 86.81.571.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 94.0 46-124 7.9 20
1.67 1001.821.671.67<0.113mg/KgButyl benzyl phthalate 109 48-132 8.5 20
1.20 71.81.271.671.67<0.092mg/Kg4-Chloro-3-methylphenol 76.0 45-122 5.6 20
1.18 70.61.281.671.67<0.112mg/Kg4-Chloroaniline 76.6 17-106 8.1 20
1.40 83.81.471.671.67<0.116mg/Kg2-Chloronaphthalene 88.0 41-114 4.8 20
1.38 82.61.421.671.67<0.098mg/Kg2-Chlorophenol 85.0 34-121 2.8 20
1.32 79.01.431.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 85.6 45-121 8.0 20
1.46 87.41.561.671.67<0.142mg/KgChrysene 93.4 50-124 6.6 20
1.43 85.61.561.671.67<0.230mg/KgDibenz(a,h)anthracene 93.4 45-134 8.6 20
1.35 80.81.461.671.67<0.119mg/KgDibenzofuran 87.4 44-120 7.8 20
1.23 73.61.281.671.67<0.094mg/Kg1,2-Dichlorobenzene 76.6 33-117 3.9 20
1.21 72.41.221.671.67<0.097mg/Kg1,3-Dichlorobenzene 73.0 30-115 0.8 20
1.19 71.21.251.671.67<0.097mg/Kg1,4-Dichlorobenzene 74.8 31-115 4.9 20
0.847 50.71.091.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 65.2 22-121 25.0*20
Page 7 of 11* QC Fail Date:02/27/2023 10:52 AM
Page 62 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
V 99866-MS-V30032 V 99866-MSD-V30032Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.19 71.21.301.671.67<0.095mg/Kg2,4-Dichlorophenol 77.8 40-122 8.8 20
1.41 84.41.511.671.67<0.180mg/KgDiethyl phthalate 90.4 50-124 6.8 20
1.37 82.01.461.671.67<0.174mg/KgDimethyl phthalate 87.4 48-124 6.3 30
1.29 77.21.411.671.67<0.108mg/Kg2,4-Dimethylphenol 84.4 30-127 8.8 20
1.57 94.01.741.671.67<0.107mg/KgDi-n-butyl phthalate 104 51-128 10.2 20
0.769 46.00.9701.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 58.0 29-132 23.1*20
0.615 36.80.8071.671.67<0.520mg/Kg2,4-Dinitrophenol 48.3 27-129 27.0*20
1.41 84.41.531.671.67<0.096mg/Kg2,4-Dinitrotoluene 91.6 48-126 8.1 20
1.42 85.01.521.671.67<0.108mg/Kg2,6-Dinitrotoluene 91.0 46-124 6.8 20
1.56 93.41.691.671.67<0.143mg/KgDi-n-Octyl Phthalate 101 45-140 8.0 20
1.41 84.41.531.671.67<0.123mg/KgFluoranthene 91.6 50-127 8.1 20
1.36 81.41.471.671.67<0.128mg/KgFluorene 88.0 43-125 7.7 20
1.41 84.41.551.671.67<0.106mg/KgHexachlorobenzene 92.8 45-122 9.4 20
1.12 67.01.171.671.67<0.097mg/KgHexachlorobutadiene 70.0 32-123 4.3 20
0.740 44.30.7431.671.67<0.157mg/KgHexachlorocyclopentadiene 44.4 32-117 0.4 20
1.25 74.81.271.671.67<0.079mg/KgHexachloroethane 76.0 28-117 1.5 20
1.42 85.01.531.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 91.6 45-133 7.4 20
1.18 70.61.261.671.67<0.191mg/KgIsophorone 75.4 30-122 6.5 20
1.25 74.81.331.671.67<0.106mg/Kg1-Methylnaphthalene 79.6 40-119 6.2 20
1.24 74.21.301.671.67<0.100mg/Kg2-Methylnaphthalene 77.8 38-122 4.7 20
1.36 81.41.431.671.67<0.097mg/Kg2-Methylphenol 85.6 32-122 5.0 20
1.23 73.61.291.671.67<0.085mg/Kg3&4 Methylphenol 77.2 34-119 4.7 20
1.30 77.81.361.671.67<0.144mg/KgNaphthalene 81.4 35-123 4.5 20
1.42 85.01.501.671.67<0.096mg/Kg2-Nitroaniline 89.8 44-127 5.4 20
1.32 79.01.441.671.67<0.120mg/Kg3-Nitroaniline 86.2 33-119 8.6 20
1.25 74.81.371.671.67<0.093mg/Kg4-Nitroaniline 82.0 63-147 9.1 20
Page 8 of 11* QC Fail Date:02/27/2023 10:52 AM
Page 63 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30112QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30032
V 99866-MS-V30032 V 99866-MSD-V30032Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.24 74.21.311.671.67<0.116mg/KgNitrobenzene 78.4 34-122 5.4 20
1.18 70.61.231.671.67<0.088mg/Kg2-Nitrophenol 73.6 32-123 4.1 20
1.54 92.21.641.671.67<0.117mg/Kg4-Nitrophenol 98.2 30-132 6.2 20
1.17 70.01.241.671.67<0.263mg/KgN-Nitrosodimethylamine 74.2 10-146 5.8 30
1.73 1041.931.671.67<0.181mg/KgN-Nitrosodiphenylamine 116 38-127 10.9 20
1.35 80.81.421.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 85.0 36-120 5.0 20
1.60 95.81.771.671.67<0.347mg/KgPentachlorophenol 106 25-133 10.0 20
1.45 86.81.581.671.67<0.208mg/KgPhenanthrene 94.6 50-121 8.5 20
1.42 85.01.461.671.67<0.112mg/KgPhenol 87.4 34-121 2.7 20
1.51 90.41.631.671.67<0.134mg/KgPyrene 97.6 47-127 7.6 20
0.168 10.00.1781.671.67<0.079mg/KgPyridine 10.6 10-80 5.7 20
1.14 68.21.201.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 71.8 34-118 5.1 20
1.32 79.01.391.671.67<0.096mg/Kg2,4,5-Trichlorophenol 83.2 41-124 5.1 20
1.33 79.61.421.671.67<0.096mg/Kg2,4,6-Trichlorophenol 85.0 39-126 6.5 20
81.42-Fluorobiphenyl (S)85.6 44-115
85.62-Fluorophenol (S)88.2 35-115
71.8Nitrobenzene-d5 (S)74.8 37-122
92.24-Terphenyl-d14 (S)98.8 54-127
79.32,4,6-Tribromophenol (S)86.7 39-132
81.1Phenol-d5 (S)85.5 34-121
Page 9 of 11Date:02/27/2023 10:52 AM
Page 64 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
Dry Weight Determination
SW-DRYWT
V29838QC Analytical Batch:
Analysis Method:
Analysis Description:
V 99877-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/16/23 16:101.028.127.8%Moisture
V 99878-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/16/23 16:101.117.717.9%Moisture
Page 10 of 11Date:02/27/2023 10:52 AM
Page 65 of 68
Quality Control Data
23-047-0008Report No:
Project Description:
Client ID:Falcon Engineering
Solomon
Dry Weight Determination
SW-DRYWT
V29848QC Analytical Batch:
Analysis Method:
Analysis Description:
V 99880-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/17/23 10:205.215.714.9%Moisture
V 99881-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 02/17/23 10:203.914.815.4%Moisture
Page 11 of 11Date:02/27/2023 10:52 AM
Page 66 of 68
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-047-0008
Falcon Engineering
00122
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.3C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:02/16/2023 12:15:57
Special precautions or instructions included?
Comments:
Page 67 of 68
Page 68 of 68