FA-1322_29012_CA_MRP_20230505

ENVIRONMENTAL | CIVIL | G EOTECHNICAL

MONITORING REPORT STARFLITE FOOD STORE #272 1416 FAYETTEVILLE ROAD ROCKINGHAM, RICHMOND COUNTY, NC NCDEQ INCIDENT NO. 29012 RISK CLASSIFICATION: I130D

MAY 5, 2023 NCDEQ CONTRACT NO. N122019D TASK AUTHORIZATION NO. 04 CATLIN PROJECT NO. 221072 PREPARED FOR: MR. HASSAN OSMAN NCDEQ, DWM, UST SECTION 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 PREPARED BY: CATLIN ENGINEERS AND SCIENTISTS 220 OLD DAIRY ROAD WILMINGTON, NC 28405 [phone]
CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585
CORPORATE LICENSURE NO. FOR GEOLOGY SERVICES C-118

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023
TABLE OF CONTENTS
PAGE
1.0 SITE INFORMATION 1
2.0 EXECUTIVE SUMMARY 2
3.0 SCOPE OF SERVICES 2
4.0 SITE HISTORY AND CHARACTERIZATION 3
4.1 UST OWNER AND OPERATOR INFORMATION 3 4.2 UST INFORMATION 3 4.3 CONTAMINANT SOURCE INVENTORY 3 4.4 SITE CHARACTERISTICS 4 4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE 4 4.6 RECEPTOR INFORMATION 4 4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES 4
5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY 5
5.1 SOIL AND BEDROCK 5
5.2 HYDROGEOLOGY 6
6.0 SITE ASSESSMENT INFORMATION 6
6.1 GAUGING DATA 7 6.2 SAMPLING DATA 7 6.3 SUMMARY OF GROUNDWATER INFORMATION 8 6.4 EVALUATION OF ASSESSMENT INFORMATION 9
7.0 CONCLUSIONS AND RECOMMENDATIONS 9
8.0 STATEMENTS AND CERTIFICATION 10
9.0 LIMITATIONS 10
10.0 REFERENCES 11

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023
TABLES
TABLE 1 SITE HISTORY – UST AND OTHER RELEASE INFORMATION
TABLE 2 PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
TABLE 3 WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
TABLE 4 SUMMARY OF GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B
TABLE 5 SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS – STANDARD METHOD 6200B
FIGURES FIGURE 1 SITE VICINITY MAP
FIGURE 2 POTENTIAL RECEPTOR MAP
FIGURE 3 SITE MAP
FIGURE 4 GROUNDWATER ELEVATION – MARCH 1, 2023
FIGURE 5 MONITORING WELL GROUNDWATER SAMPLE ANALYTICAL RESULTS –
MARCH 1, 2023
FIGURE 6 ESTIMATED HORIZONTAL EXTENT OF BENZENE – MARCH 1, 2023

APPENDICES APPENDIX A HISTORICAL DATA
APPENDIX B SITE PHOTOGRAPHS
APPENDIX C DAILY ACTIVITIES LOG AND FIELD DATA SHEETS
APPENDIX D LABORATORY ANALYTICAL REPORT AND CHAIN OF CUSTODY DOCUMENT

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 1 May 2023
1.0 SITE INFORMATION
Site Identification
Date: 05/05/2023 Site Risk/Priority Rank: I130D
UST Number: FA-1322 Incident Number: 29012
Site Name: Starflite Food Store #272 Facility ID: 0-03830
Site Location: 1416 Fayetteville Road
Nearest City/Town: Rockingham County: Richmond
Description of Geographical Data Point: Former gasoline UST basin
Location Method: Google Earth
Latitude (decimal degrees): 34.94534° Longitude (decimal degrees): -79.75491°
Contacts Information
UST Owner: Marshall Oil Group, LLC (dissolved)
Address: PO Box 1128, Wake Forest, NC 27588 Phone: Not Applicable
UST Operator: Marshall Oil Group, LLC (dissolved)
Address: PO Box 1128, Wake Forest, NC 27588 Phone: Not Applicable
Property Owner: R & S Patel, LLC
Address: 808 Hillcrest Drive, Rockingham, NC 28379-2503 Phone: Unknown
Property Occupant: JD Convenience Mart/El Super Taco
Address: 1416 Fayetteville Road, Rockingham, NC Phone: [phone]
Consultant: CATLIN Engineers and Scientists
Address: 220 Old Dairy Rd., Wilmington, NC 28405 Phone: [phone]
Corporate Licensure No. For Engineering Services: C-0585
Corporate Geology License No.: C-118
Analytical Laboratory: Con-Test Analytical Laboratory State Certification: NC 652, NC-DW 25703
Address: 39 Spruce St., E. Longmeadow, MA 01028 Phone: [phone]
Release Information
Date Discovered: 08/01/2002
Estimated Quantity of Release: Unknown
Cause of Release: Leak in the UST system
Source of Release: UST system or associated fitting(s)
Sizes and contents of UST system(s) from which the release occurred:
• One 1,000-gallon UST
• Three 4,000-gallon gasoline USTs
• Four 10,000-gallon gasoline USTs
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 2 May 2023
2.0 EXECUTIVE SUMMARY
The Starflite Food Store #272 site is located at 1416 Fayetteville Road,
Rockingham, Richmond County, North Carolina. Nine underground storage tanks
(USTs) were previously operated at the site. One 1,000-gallon, one 10,000-gallon, and three 4,000-gallon USTs were removed from the site in 1988. Four 10,000-gallon USTs were abandoned in place in 2009. A petroleum release was discovered through soil and groundwater sample analyses associated with a planned property
transaction.
The purpose of this report is to document the latest groundwater sampling event. On March 1, 2023, CATLIN Engineers and Scientists (CATLIN) personnel measured groundwater at an average of three feet deep in the shallow wells and 28 feet deep
in the deep well on-site. Groundwater samples from five monitoring wells were
collected. The samples were submitted for laboratory analysis of volatile organic compounds (VOCs) per Standard Method (SM) 6200B plus ethylene dibromide (EDB), methyl tert-butyl ether (MTBE) and diisopropyl ether (DIPE).
Laboratory results did not indicate any dissolved petroleum constituents above their
respective laboratory reporting limits in the sample from MW-4. Several VOCs were detected in the MW-1, MW-2, MW-3, and MW-5D samples at concentrations greater than those established in Title 15A of the North Carolina Administrative Code, Subchapter 2L (2L GWQS), but below Gross Contaminant Levels (GCL).
The groundwater sample collected during this event from monitoring well MW-2 revealed contaminant concentrations generally higher than those detected during the October 2022 sampling event; however, those in MW-1 have decreased. Benzene concentrations have remained below GCL in samples from MW-2 since
2021. This monitoring sampling event is the third consecutive event with no GCL exceedances. CATLIN recommends the site be a candidate for No Further Action (NFA) status with a Notice of Residual Petroleum (NRP) for groundwater.
3.0 SCOPE OF SERVICES The scope of services for this report was performed in general accordance with CATLIN proposal number 221072.4P, dated January 4, 2023. Services were
authorized by the North Carolina Department of Environmental Quality’s (NCDEQ’s) Task Authorization (TA) #04, approved on January 4, 2023, and Contract Number N122019D.
The approved scope of services for this Task Authorization included to:
• Collect groundwater samples from five monitoring wells (MW-1, MW-2, MW-3, MW-4, and MW-5D);
• Analyze six water samples (five monitoring well samples and one trip blank) according to SM 6200B (including EDB, MTBE, and DIPE); and,
• Prepare and submit a monitoring report summarizing the findings.
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 3 May 2023
The scope of services was conducted in accordance with the approved TA.
4.0 SITE HISTORY AND CHARACTERIZATION

The Starflite Food Store #272 site is located at 1416 Fayetteville Road, Rockingham, Richmond County, North Carolina (Figures 1 and 2). Summarized available historical sampling and gauging data from previous consultants are provided in Appendix A. Site photographs are presented in Appendix B.
4.1 UST OWNER AND OPERATOR INFORMATION Marshall Oil Group, LLC (Marshall Oil) reportedly owned the nine USTs historically operated on-site. A former retail petroleum facility and
convenience store, Starflite Food Store #272, operated the tanks. Marshall
Oil dissolved in 2010 and the site was subsequently accepted into the North Carolina UST Section Trust Fund Branch State Lead Program (S&ME, 2020). Available information regarding UST owners/operators and is presented on
Table 1.
4.2 UST INFORMATION Four 4,000-gallon gasoline USTs and one 1,000-gallon UST (unknown
contents) were installed at the site in 1966. One 10,000-gallon UST was
installed in 1971. The tanks were operated for petroleum retail sales until their removal in July 1988. No closure report was provided (S&ME, 2020). One 10,000-gallon kerosene UST was installed in October 1981 and three
10,000-gallon gasoline USTs were installed in October 1988. Marshall Oil
purchased the property in January 1996. Historical files do not fully clarify the ownership/operation history of the tanks versus the property. However, previous reports and site notes indicate that all tanks were at some point owned by Marshall Oil (S&ME, 2020; NCDENR 2013).
Between 2007 and 2008, the property was foreclosed on and purchased by Mr. Jeffrey Barnhardt. He received permission from then North Carolina Department of Environment and Natural Resources (NCDENR, now NCDEQ) to have the UST system removed. In February 2009, at the advice of the City
of Rockingham, Mr. Barnhardt instead abandoned the USTs in place by filling them with sand and capping the fill ports with concrete (S&ME, 2020). Available UST system information is presented in Table 1 and the approximate former UST basin location is illustrated on Figure 3.
4.3 CONTAMINANT SOURCE INVENTORY An on-site release was discovered in August 2002 during soil and groundwater sampling associated with a potential real estate sale. Soil
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 4 May 2023
sample analytical results revealed total petroleum hydrocarbons (TPH) gasoline range organics (GRO) and diesel range organics (DRO) above State Action Levels. Multiple targeted analytes were reported at
concentrations above their respective 2L GWQS in the groundwater samples
(EMS, 2003; S&ME, 2020). 4.4 SITE CHARACTERISTICS
The property is owned by R & S Patel, LLC and the former Starflite Food
Store is now occupied by the El Super Taco restaurant and JD Mart Convenience Store, which does not sell petroleum. The parcel is comprised of the store building and a concrete lot.
4.5 OWNERS AND OCCUPANTS OF ADJOINING/NEARBY PROPERTIES AND LAND USE Properties in the site vicinity are mostly commercial and residential. Eastside Cemetery is to the east (across Eastside Drive). A retail petroleum facility
(Shell) and convenience store is across the parking lot to the west. A retail
store operates on the parcel adjoining the site to the south. US Route 1 bounds the site to the north. A residence and the Richmond County water Department are located to the north (across US Route 1).
4.6 RECEPTOR INFORMATION
Conducting a receptor survey was outside the scope of this monitoring event. A review of historical files available on the NCDEQ Waste Management Online Database (aka Laserfiche) indicates that the last receptor survey for
the Former Starflite Food Store #272 site was conducted in 2013 by
Crawford Environmental Services (CES, 2013). According to previous reports, municipal water is available to the site vicinity. No water supply wells were identified within 1,000 feet of the site and no
surface water bodies were noted within 500 feet (CES, 2013; S&ME, 2020). Potential receptors are illustrated on Figure 2 and receptor information is shown on Table 2.
4.7 PREVIOUS INVESTIGATIONS AND REMEDIAL ACTIVITIES The release was discovered in 2002 during sampling conducted for a potential real estate transaction. The soil samples contained TPH GRO up to 4,100 milligrams per kilograms (mg/kg) and up to 71 mg/kg TPH DRO.
Groundwater sample analytical results also revealed several targeted analytes at concentrations above their 2L GWQS (ATC, 2002). A Limited Site Assessment (LSA) was conducted in April 2003. Soil samples were obtained from approximately five feet below land surface (BLS) at
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CATLIN Project No. 221072 5 May 2023
multiple locations across the site. Laboratory analytical results revealed several VOC concentrations above their respective Soil-to-Groundwater (STGW) maximum soil contaminant concentrations (MSCC). The C9-C22
aromatics concentration was reported above its Residential MSCC (EMS,
2003). However, all soil samples were collected from below the water table (measured at two feet BLS) and therefore, do not likely reflect vadose zone soil conditions (S&ME, 2020).
To date, four shallow monitoring wells (MW-1 through MW-4) and one deep
monitoring well (MW-5D) have been installed on-site. Four sampling events were conducted between 2003 and 2020 (in 2003, 2013, 2018, and 2020). Historically, the greatest petroleum constituent concentrations have been reported in samples from MW-2. Multiple VOC concentrations above
2L GWQS have been reported in samples from MW-1, MW-2, MW-3, and
MW-5D. Benzene had persisted above its GCL in samples from MW-2. No other constituents have been reported above GCL. No VOCs have been detected above their laboratory reporting limits in samples from MW-4 (S&ME, 2020).

CATLIN conducted a groundwater monitoring event in July 2021. Monitoring wells MW-1, MW-2, MW-3, and MW-5D were sampled. Several petroleum constituents were reported above their 2L GWQS in all the monitoring well samples. Benzene was reported above its GCL in the sample from MW-2.
The contaminant concentrations in MW-2 had fluctuated since the previous
sampling event (CATLIN, 2021). In June 2022, CATLIN oversaw a mobile multi-phase extraction (MMPE) event at the site utilizing monitoring well MW-2 as the extraction point. A total
of 4,638 gallons of impacted groundwater were removed (CATLIN, 2022A).
CATLIN conducted subsequent groundwater monitoring events in July and October 2022. During both events, laboratory analysis revealed multiple petroleum compounds above their 2L GWQS in the samples from MW-1,
MW-2, MW-3, and MW-5D; however, none were above GCL. The
contaminant concentrations in MW-2 had decreased since the July 2021 event, including benzene being brought below GCL (CATLIN, 2022A; 2022B).
Summarized historical data prepared by S&ME, Inc. (S&ME) (2020) are
presented in Appendix A. Site photographs are provided in Appendix B. 5.0 REGIONAL AND SITE GEOLOGY AND HYDROGEOLOGY
5.1 SOIL AND BEDROCK
As defined in the Geologic Map of North Carolina, published by the North Carolina Department of Natural Resources and Community Development (1985), the site lies within the Coastal Plain physiographic province.
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 6 May 2023
The North Carolina Coastal Plain is approximately 90 to 150 miles wide from
the Atlantic Ocean westward to its boundary with the Piedmont province.
Two natural subdivisions of the Coastal Plain were described by Stuckey (1965): the Tidewater region and the Inner Coastal Plain. The project area is located within the Inner Coastal Plain, which is an area of erosional
topography (Horton and Zullo, 1991).
The Coastal Plain comprises a wedge-shaped sequence of stratified marine and non-marine sedimentary rocks deposited on crystalline basement. The sedimentary sequences range in age from Recent to lower Cretaceous
(Narkunas, 1980). According to the 1985 Geologic Map of North Carolina,
locally cross-bedded, sand, sandstone, and mudstone (of the Middendorf formation) crop out in the site area. Boring logs provided in EMS (2003) indicate that the site is underlain by
sandy clay and clayey sand to approximately 30 feet BLS. Quartz bearing
clayey sands were observed from 35 to 50 feet BLS. Clay (approximately 2 feet thick) and siltstone (approximately 15 feet thick) layers were encountered at further depths.
5.2 HYDROGEOLOGY

Groundwater - The 2020 Visual Hydrogeologic Framework (VHF) – North Carolina Hydrogeological Database identified sufficient boreholes near the site to draw a cross-section. According to the VHF, the Black Creek aquifer
extends to approximately 70 feet BLS. A confining unit (approximately 10 feet
thick) is projected to be present below the Black Creek aquifer. The crystalline basement is expected to be encountered at 80 feet BLS in the site vicinity.
Surface Water – No surface water bodies were identified within 500 feet of
the site (S&ME, 2020). 6.0 SITE ASSESSMENT INFORMATION
CATLIN conducted field activities on March 1, 2023 in general accordance with the
approved TA and pre-prepared Health and Safety Plan (HASP). Upon arrival at the site, potential hazards were evaluated before beginning field work and are documented on a Daily Activities Log, included in Appendix C. Photographs from the site visit are included in Appendix B.
CATLIN personnel gauged and collected groundwater samples for laboratory analysis of VOCs per SM 6200B from five monitoring wells (MW-1, MW-2, MW-3, MW-4, and MW-5D). Well locations and site features are shown on Figure 3 and well construction details are presented on Table 3.

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 7 May 2023
6.1 GAUGING DATA Historical gauging results report depth to water ranging from 1.17 feet below
top of casing (BTOC) (MW-4) to 4.89 feet BTOC (MW-2) in the shallow wells.
Depth to water has historically ranged from 30.19 feet BTOC to 39.46 BTOC in the deep well (MW-5D) (S&ME, 2020; CATLIN, 2022A). During recent monitoring events, the calculated groundwater flow direction was towards the north/northeast (CATLIN, 2021).

During the March 2023 event, CATLIN personnel measured depth to water using an electronic water interface probe. To prevent cross contamination, the probe and cabling were decontaminated according to the manufacturer’s recommendations between use in each well. Gauging data were recorded on
an electronic groundwater sampling form using a tablet device. Gauging
procedures were performed in general accordance with NCDENR and NCDEQ Guidelines and Environmental Protection Agency (EPA) Region 4 Operating Procedures.
Depth to water ranged from 2.85 feet BTOC (MW-4) to 3.23 feet BTOC
(MW-2) in the shallow wells. Depth to water in MW-5D was 28.24 feet BTOC. The depths to water measured in MW-1 and MW-4 were above their respective screened intervals. Based on groundwater elevations calculated for this monitoring period, groundwater flow direction is towards the north.
Monitoring well gauging results for events conducted by CATLIN are presented in Table 3. Groundwater elevation and flow direction are illustrated on Figure 4 and groundwater sampling forms are provided in Appendix C.
6.2 SAMPLING DATA Following gauging, the monitoring wells were sampled in general accordance with NCDENR and NCDEQ Guidelines and EPA Region 4 Operating Procedures. Prior to obtaining representative groundwater samples, each
monitoring well was purged by removing a minimum of three well volumes using a new, disposable bailer. Monitoring well groundwater field parameter data were measured at one-minute intervals using an In-Situ Aqua TROLL 600 Multiparameter Sonde (Aqua TROLL). Conductivity, pH, oxidation reduction potential (ORP), dissolved oxygen, and temperature
measurements were recorded utilizing the VuSitu mobile application (version 1.17.12). The Aqua TROLL was decontaminated according to the manufacturer’s recommendations between use at each monitoring well. Groundwater parameter data were transferred from the VuSitu mobile application to the electronic groundwater sampling forms. Copies of the
groundwater sampling forms are available in Appendix C.
After a minimum of three well volumes were removed (or the well was bailed dry), a groundwater sample was collected from the well and poured into appropriate laboratory provided glassware, labeled, and placed on ice in an
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 8 May 2023
insulated cooler. A laboratory-provided trip blank was maintained in the cooler for the duration of the event.
The groundwater samples and laboratory-provided trip blank were submitted
to Con-Test Analytical Laboratory (Certification NC 652 and NC-DW 25703) in East Longmeadow, Massachusetts, under proper chain of custody (COC) protocol and analyzed per SM 6200B (including EDB, MTBE, and DIPE). The laboratory analytical data and COC are included in Appendix D.
6.3 SUMMARY OF GROUNDWATER INFORMATION Historically, samples from monitoring well MW-2 have contained the highest petroleum constituent concentrations. Light non-aqueous phase liquid
(LNAPL; aka free-phase product) has never been detected at the site. During
the previous sampling event conducted by CATLIN (October 2022), multiple constituents were detected at concentrations exceeding their 2L GWQS in samples from MW-1, MW-2, MW-3, and MW-5D. Benzene has been previously reported above its GCL in samples from MW-2; however, it has
been below GCL since July 2022. Historical information prepared by other
consultants is included in Appendix A. The latest groundwater sampling laboratory results for SM 6200B analysis are summarized in Table 4. Historical results for events conducted by
CATLIN are in Table 5. Monitoring well sample analytical results are illustrated on Figure 5. A copy of the complete laboratory report and COC documentation are in Appendix D. Monitoring Wells
During the March 2023 monitoring event, five monitoring well groundwater samples (MW-1, MW-2, MW-3, MW-4, and MW-5D) were collected and submitted for analysis via SM 6200B (including EDB, MTBE, and DIPE). No analyte concentrations were detected above GCL in any of the monitoring
well samples. Laboratory analysis detected an estimated concentration (“J”-value) of acetone in the MW-4 sample; however, this is likely a laboratory artifact and was also detected in the laboratory-provided trip blank sample. Analytical results reported the following constituents at concentrations above their 2L GWQS in samples MW-1, MW-2, MW-3, and MW-5D:
• MW-1: benzene, isopropylbenzene, naphthalene, and n-propylbenzene;
• MW-2: benzene, EDB, ethylbenzene, naphthalene, n-propylbenzene,
toluene, and total xylenes;
• MW-3: benzene, ethylbenzene, isopropylbenzene, naphthalene, and n-propylbenzene; and
• MW-5D: benzene, MTBE, and naphthalene.

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 9 May 2023
Trip Blank One laboratory-provided trip blank sample was submitted for analysis per SM
6200B (including EDB, MTBE, and DIPE). An estimated concentration (“J”-
value) of acetone (a common laboratory artifact) was detected; however, it was well below 2L GWQS. No other targeted analytes were detected. 6.4 EVALUATION OF ASSESSMENT INFORMATION

Extent of Contamination Benzene was historically reported above its GCL in samples from MW-2. No GCL exceedances have been revealed since July 2021. Several petroleum
constituents were still detected above their respective 2L GWQS in
monitoring wells MW-1, MW-2, MW-3, and MW-5D. Summarized monitoring well groundwater sample analytical results are illustrated on Figure 5. The estimated horizontal extent of benzene is shown on Figure 6.
The highest concentrations of benzene, toluene, ethylbenzene, and total
xylenes (BTEX) have historically been reported in samples from MW-2. The BTEX concentrations in MW-2 have increased since the previous monitoring event (but are still well below GCL), while those in MW-1 have decreased (CATLIN, 2022B).

Cleanup Levels Achieved
Soil – Soil samples obtained in 2002 revealed several VOCs above STGW MSCC and one targeted analyte above Residential MSCC. However, soil
samples were collected from below the water table and are likely not
reflective of vadose zone soil conditions.
Groundwater – Groundwater contaminant concentrations are above 2L GWQS, but below GCL at the site.

LNAPL – LNAPL was not measured during this monitoring period. LNAPL has not been historically observed at the site. 7.0 CONCLUSIONS AND RECOMMENDATIONS

Conclusions Groundwater monitoring findings for this period are summarized below:
• Five monitoring wells (MW-1, MW-2, MW-3, MW-4, and MW-5D) were sampled.
• Groundwater flow direction was calculated to be towards the north.
• No targeted analytes were above their reporting limits in the sample from MW-4.
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 10 May 2023
•Several petroleum constituents above their 2L GWQS were reported in thesamples from MW-1, MW-2, MW-3, and MW-5D.
•No targeted analytes were detected above GCL.
•The MW-2 BTEX concentrations have increased since the previous samplingevent (but are still well below GCL), while those in MW-1 have decreased.
Recommendations
CATLIN recommends the site be a candidate for NFA status with a NRP for groundwater.
8.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. April 28, 2023 Will this report be submitted after the established due date? YES
This report was submitted on May 5, 2023.
2 Was any required information from the above template missing from this report? YES
No cross sections are provided.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved in the Corrective Action Plan not be met? NA
No CAP has been submitted for this site.
4 Does any known or suspected source zone soil contamination or free product remain outside of the assessed area that could be inhibiting natural attenuation? NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a potential new release from a separate onsite or offsite source? NO
6 Certification:
I, Benjamin J. Ashba, a Licensed Geologist for CATLIN Engineers and Scientists, do certify
that the information contained in this report is correct and accurate to the best of my knowledge.
CATLIN Engineers and Scientists is licensed to practice geology in North Carolina.
The certification number of the company or corporation is C-118.
9.0 LIMITATIONS
The groundwater samples analyzed as part of this investigation only provide isolated data points and may not represent conditions at every location in the project area.
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 11 May 2023
Analyses and conclusions of this report, being based on interpolation between data points at the project area, may not be completely representative of all site conditions. Conclusions and recommendations of this investigation and report are
based on the best available data in an effort to comply with current regulatory
requirements. 10.0 REFERENCES
ATC Associates of North Carolina, P.C., Baseline Environmental Assessment,
Starflite, 1416 Fayetteville Road, Rockingham, North Carolina, NCDENR
Facility Identification No. 0-003830, ATEC Project Number 45.03451.0025, September 3, 2002.
CATLIN Engineers and Scientists, Monitoring Report, Starflite Food Store #272,
1416 Fayetteville Road, Rockingham, Richmond County, North Carolina,
NCDEQ Incident No. 29012, Risk Classification: I130D, August 6, 2021.
CATLIN Engineers and Scientists, Monitoring Report, Starflite Food Store #272,
1416 Fayetteville Road, Rockingham, Richmond County, North Carolina, NCDEQ Incident No. 29012, Risk Classification: I130D, August 25, 2022(A).
CATLIN Engineers and Scientists, Monitoring Report, Starflite Food Store #272,
1416 Fayetteville Road, Rockingham, Richmond County, North Carolina,
NCDEQ Incident No. 29012, Risk Classification: I130D, December 7, 2022(B).
Crawford Environmental Services, Inc., Groundwater Monitoring Report: August
2013, Starflite Food Store #272, 1416 Fayetteville Road, Rockingham,
Richmond County, North Carolina, Incident Number 7351, August 26, 2013.
EMS Environmental, Inc., Limited Site Assessment – Phase I and II, Starflite Food
Store #272, NCDENR Incident No. 29012, EMS Project #7351, April 16, 2003.
Horton, J. Wright, Jr. and Victor A. Zullo, An Introduction to the Geology of the
Carolinas: The Geology of the Carolinas, pp 1-11.
Narkunas, J., Groundwater Evaluation in the Central Coastal Plain of North
Carolina, North Carolina Department of Natural Resources and Community Development, 1980, pp 119.
NCDEQ, Division of Water Resources, 2020 Visual Hydrogeologic Framework,
North Carolina Hydrogeological Database, ncwater.org/?page=350, accessed August 3, 2021.
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Corrective Action Guidelines, January 19,
2021.
NCDENR, Division of Waste Management, Ken Currie – Fayetteville Regional Office, Recommendation of Site for State Lead Cleanup, January 16, 2013.
NCDENR, UST Section, North Carolina Department of Environment and Natural Resources, Division of Waste Management, Guidelines for Sampling,
December 1, 2013.
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 12 May 2023
NCDEQ, UST Section, North Carolina Department of Environmental Quality, Division of Waste Management, Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement, January 19, 2021.
North Carolina Department of Natural Resources and Community Development,
Geological Map of North Carolina, 1985.
S&ME, Inc., Groundwater Monitoring Report, Starflite Food Store 272, Incident
#29012, 1416 Fayetteville Road, Rockingham, Richmond County, NC, S&ME Project No. 4305-18-100B, June 2, 2020.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and
Ecosystem Support Division, Athens Georgia, Operating Procedure – Field
Equipment Cleaning and Decontamination at the FEC, Striggow, B., U.S. EPA Report No. SESDPROC-206-R3, Effective Date December 18, 2015.
U.S. Environmental Protection Agency, Science and Ecosystem Support Division,
Athens Georgia, Operating Procedure – Groundwater Level and Well Depth
Measurement, Striggow, B., U.S. EPA Report No. SESDPROC-105-R3, Effective Date November 3, 2016.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure –
Groundwater Sampling, Striggow, B., U.S. EPA Report No. SESDPROC-
301-R4, Effective Date April 26, 2017.
U.S. EPA, Region 4, U.S. Environmental Protection Agency, Science and Ecosystem Support Division, Athens Georgia, Operating Procedure – In Situ Water Quality Monitoring, Chief, Field Services Branch, U.S. EPA Report No.
SESDPROC-111-R4, Effective Date March 14, 2018.
Winner, M.D, Jr., and Coble, R.W., Hydrogeologic Framework of the North Carolina
Coastal Plain Aquifer System: U.S. Geological Survey Open File Report 87-
690, 1989, pp 155.

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TABLES
Page 1 of 1
TABLE 1
SITE HISTORY — UST AND OTHER RELEASE INFORMATION
Incident Name and No.: Starflite Food Store #272 - 29012
UST ID
Number
Name of
Owner/
Operator
Dates of
Ownership
Dates of
Operation
Last
Contents
Previous
Contents
Capacity
(gal)
Construction
Details
Tank
Dimensions
(inches)
Installation
Date
(mm/dd/yy)
Date
Removed
(mm/dd/yy)
1 Unknown Unknown Gasoline Gasoline 4,000 Unknown Unknown XX/XX/66 07/01/88
2 Unknown Unknown Gasoline Gasoline 4,000 Unknown Unknown XX/XX/66 07/01/88
3 Unknown Unknown Gasoline Gasoline 4,000 Unknown Unknown XX/XX/66 07/01/88
4 Unknown Unknown Unknown Unknown 1,000 Unknown Unknown XX/XX/66 07/01/88
5 Unknown Unknown Gasoline Gasoline 10,000 Unknown Unknown XX/XX/71 07/01/88
6 Unknown Unknown Gasoline Gasoline 10,000 Unknown Unknown 10/24/88 AIP 02/29/09
7 Unknown Unknown Gasoline Gasoline 10,000 Unknown Unknown 10/24/88 AIP 02/29/09
8 Unknown Unknown Gasoline Gasoline 10,000 Unknown Unknown 10/24/88 AIP 02/29/09
9 Unknown Unknown Kerosene Kerosene 10,000 Unknown Unknown 10/26/81 AIP 02/29/09
Incident
Number
Material
Released
Date Release
Discovered
(mm/dd/yy)
29012 Gasoline
(assumed)08/16/02
XX = Exact date unknown.
AIP = Abandoned in Place; USTs were filled with sand.
Description of the Release
On August 16 2002, TPH discovered in soils and groundwater during assessment associated with a planned property
transaction.
Marshall Oil
Group, LLC
(Dissolved)
NCDEQ; 29012_Starflite Food Store #272; T1_Site History
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023
Page 1 of 1
TABLE 2
Incident Name and No.: Starflite Food Store #272 - 29012
Well ID Property
Address
Parcel
Number
Owner Name
(Last, First MI)
Owner Mailing
Address Well Use
Distance/
Direction
from
Source Area
(ft.)
Comment
Receptor
ID Location Contact
Distance/
Direction from
Source Area (ft.)
ft. = feet
Description
No known water supply wells within 1,000 ft.
No known water bodies or other receptors within 500 ft.
PUBLIC AND PRIVATE WATER SUPPLY WELLS AND OTHER RECEPTOR INFORMATION
NCDEQ; 29012_Starflite Food Store #272; T2_Receptor Info
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023
Page 1 of 1
TABLE 3
WELL CONSTRUCTION AND HISTORICAL WATER LEVEL GAUGING DATA
Incident Name and No.: Starflite Food Store #272 - 29012
Well ID
Date
Installed
(mm/dd/yy)*
Date Water
Level
Measured
(mm/dd/yy)
Well
Diameter
(inches)
Well
Casing
Depth
(ft. BLS)*
Screened
Interval
(x to y ft.
BLS)*
Bottom
of Well
(ft. BLS)*
Top of
Casing
Elevation*
(ft.)
Free-Phase
Product
Thickness**
Depth to
Groundwater
from Top of
Casing (ft.)
Groundwater
Elevation (ft.)Comments
07/07/21 NMT 3.15 301.29 Ɨ
06/27/22 NMT 3.17 301.27 Ɨ
07/28/22 NMT 2.76 301.68 Ɨ
10/31/22 NMT 3.90 300.54 Ɨ
03/01/23 NMT 3.11 301.33 Ɨ
07/07/21 NMT 4.22 301.41
06/27/22 NMT 4.02 301.61
07/28/22 NMT 3.38 302.25
10/31/22 NMT 4.89 300.74
03/01/23 NMT 3.23 302.40
07/07/21 NMT 3.13 301.16
06/27/22 NMT 3.26 301.03
07/28/22 NMT 2.87 301.42 Ɨ
10/31/22 NMT 3.81 300.48
03/01/23 NMT 3.16 301.13
07/28/22 NMT 2.85 302.15 Ɨ
10/31/22 NMT 4.04 300.96
03/01/23 NMT 2.85 302.15 Ɨ
07/07/21 NMT 30.19 274.20 Type III; Ɨ
06/27/22 NMT 30.72 273.67 Type III; Ɨ
07/28/22 NMT 30.22 274.17 Type III; Ɨ
10/31/22 NMT 29.56 274.83 Type III; Ɨ
03/01/23 NMT 28.24 276.15 Type III; Ɨ
NMT = No Measurable Thickness
Ɨ = Water level was measured above the screened interval.
304.44
305.00
MW-1
304.29183-1832.0
03/06/03 2.0 3
52.003/06/03
3-13 13 305.63
** = if free-phase product is present in a well, ground water elevation should be calculated by : [top of casing elevation - depth to water]+ [free product thickness xspecific gravity of the fuel type]
* = Data obtained from S&ME (2020).
ft. BLS = feet Below Land Surface
304.396661-66616.0/2.003/07/03MW-5D
205-20
MW-4 03/06/03
03/06/03MW-3
MW-2
2.0 3 3-18 18
NCDEQ; 29012_Starflite Food Store #272; T3_Well Construction & Gauging
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023
Page 1 of 1
TABLE 4
SUMMARY OF GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Starflite Food Store #272 - 29012
Date
Collected
03/01/23 <40 100 <34 45 24 <3.2 ƚ <4.0 290 120 <2.5 <3.4 400 370 <3.0 15 11 <3.0 <19.9 J*BMDL
03/01/23 <20 1,900 <17 30 15 2.8 J <2.0 890 59 4.1 J <1.7 360 160 2.8 J 1,600 400 120 2,120 BMDL
03/01/23 <20 56 <17 41 25 <1.6 ƚ <2.0 850 150 2.6 J 12 680 420 <1.5 7.8 50 21 98 BMDL
03/01/23 3.6 J <0.18 <1.7 <0.15 <0.13 <0.16 ƚ <0.20 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
03/01/23 9.0 J 4.1 19 <0.15 0.67 <0.16 ƚ 1.3 0.53 4.7 <0.13 38 10 0.25 J <0.15 <0.22 0.48 J <0.15 <0.80 J*BMDL
03/01/23 2.8 J <0.18 <1.7 <0.15 <0.13 <0.16 ƚ <0.20 <0.22 <0.15 <0.13 <0.17 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit
Bold results indicate concentrations above 2L GWQS.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than method detection limit
ƚ = The method detection limit is above the 2L GWQS.
* = The value represents the sum of the reported practical quantitation limit of one analyte and the detected concentration of the other analyte.
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).n-PropylbenzeneDiisopropyl Ether (DIPE)11,700
25
20,000
20 Styrene70,000
70Naphthalene Methyl tert-Butyl Ether (MTBE)Isopropylbenzene (Cumene)p-Isopropyltoluene(p-Cymene)MW-5D
MW-3
MW-2
MW-1
Well/
Sample
ID
MW-4
Trip
Blank
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
5,900
70
5,000
1
4,000,000
4,000
Contaminant of
Concern
Acetone n-Butylbenzenesec-Butylbenzene Ethylbenzene2-Butanone (MEK)1,2-Dibromoethane (EDB)Benzene All Other SM 6200B AnalytesVaries
VariesTotal XylenesToluene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene50,000
500
260,000
600
8,800
70
28,500
400
24,100
400
70,000
70
80,000
600
30,500
70
50
0.02
6,000
6
26,100
70
NCDEQ; 29012_Starflite Food Store #272; T4_GW Results
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023
Page 1 of 1
TABLE 5
SUMMARY OF HISTORICAL GROUNDWATER LABORATORY RESULTS — STANDARD METHOD 6200B
Incident Name and No.: Starflite Food Store #272 - 29012
Date
Collected
07/07/21 <24 72 BMDL 51 24 1.9 J 4.8 J BMDL <3.2 ƚ <1.5 910 97 <0.90 <1.7 BMDL 430 300 BMDL 12 6.9 <1.0 19.2 J BMDL
07/28/22 <20 120 <16 52 29 2.4 J <1.7 BMDL <3.1 ƚ <1.3 1,000 130 2.0 J 4.1 J <2.3 560 380 BMDL 16 5.0 6.8 22.8 J BMDL
10/31/22 <41 110 <32 55 26 <2.6 <3.4 BMDL <6.2 ƚ <2.6 1,200 120 <1.9 <3.4 <4.7 600 390 <2.1 18 7.2 J <2.3 22.2 J BMDL
03/01/23 <40 100 <34 45 24 <2.8 <2.8 <3.2 ƚ <6.1 ƚ <4.0 290 120 <2.5 <3.4 <3.5 400 370 <3.0 15 11 <3.0 <19.9 J*BMDL
07/07/21 <240 9,100 BMDL 39 J <10 <9.0 <19 BMDL <32 ƚ <15 1,600 85 <9.0 <17 BMDL 640 200 BMDL 3,600 1,100 220 4,330 BMDL
07/28/22 <200 2,300 <160 210 69 <13 <17 BMDL <31 ƚ <13 1,300 170 38 J <17 <23 ƚ 1,000 490 BMDL 2,700 2,600 650 4,400 BMDL
10/31/22 <20 780 <16 28 13 <1.3 <1.7 BMDL <3.1 ƚ <1.3 720 53 3.9 J <1.7 <2.3 390 150 1.7 J 610 430 120 1,540 BMDL
03/01/23 <20 1,900 <17 30 15 <1.4 <1.4 2.8 J <3.0 ƚ <2.0 890 59 4.1 J <1.7 <1.8 360 160 2.8 J 1,600 400 120 2,120 BMDL
07/07/21 <47 22 BMDL 52 25 <1.8 <3.8 BMDL <6.4 ƚ <3.0 1,000 110 6.4 J 5.2 J BMDL 650 340 BMDL 5.4 J 350 40 199.2 J BMDL
07/28/22 <20 45 <16 120 22 <1.3 <1.7 BMDL <3.1 ƚ <1.3 910 120 3.8 J 14 <2.3 670 340 BMDL 9.9 160 64 155 BMDL
10/31/22 <20 35 <16 38 21 <1.3 <1.7 BMDL <3.1 ƚ <1.3 1,000 120 3.2 J 10 <2.3 730 340 <1.1 6.4 180 72 149.4 BMDL
03/01/23 <20 56 <17 41 25 <1.4 <1.4 <1.6 ƚ <3.0 ƚ <2.0 850 150 2.6 J 12 <1.8 680 420 <1.5 7.8 50 21 98 BMDL
07/28/22 3.7 J <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 BMDL <0.31 <0.13 <0.21 <0.11 <0.097 <0.17 <0.23 <0.24 <0.086 BMDL <0.22 <0.20 <0.11 <0.69 BMDL
10/31/22 <2.0 <0.20 <1.6 <0.15 <0.11 <0.13 <0.17 BMDL <0.31 <0.13 <0.21 <0.11 <0.097 <0.17 <0.23 <0.24 <0.086 <0.11 <0.22 <0.20 <0.11 <0.69 BMDL
03/01/23 3.6 J <0.18 <1.7 <0.15 <0.13 <0.14 <0.14 <0.16 ƚ <0.30 <0.20 <0.22 <0.15 <0.13 <0.17 <0.18 <0.38 <0.12 <0.15 <0.22 <0.20 <0.15 <0.73 BMDL
07/07/21 2.8 J 0.34 J BMDL <0.14 <0.10 <0.090 <0.19 BMDL 0.59 0.49 J <0.090 0.10 J <0.090 32 BMDL <0.15 <0.080 BMDL <0.11 <0.10 <0.10 <0.27 BMDL
07/28/22 5.5 J 1.1 4.2 J <0.15 0.22 J <0.13 <0.17 BMDL <0.31 0.34 J <0.21 1.1 <0.097 13 0.31 J 5.8 L <0.086 BMDL <0.22 0.29 J <0.11 <0.69 BMDL
10/31/22 16 J 3.4 13 <0.15 0.45 J <0.13 <0.17 BMDL <0.31 1.2 0.40 J 3.3 <0.097 39 <0.23 12 0.14 J <0.11 <0.22 <0.20 <0.11 <0.69 BMDL
03/01/23 9.0 J 4.1 19 <0.15 0.67 <0.14 <0.14 <0.16 ƚ <0.30 1.3 0.53 4.7 <0.13 38 <0.18 10 0.25 J <0.15 <0.22 0.48 J <0.15 <0.80 J*BMDL
All results in micrograms per liter (µg/L).
BMDL = Below Method Detection Limit
Bold results indicate concentrations above 2L GWQS.
Shaded results indicate concentrations above GCL.
GCL = Gross Contaminant Level
2L GWQS = NCAC T15A:02L Groundwater Quality Standards
< = Less than method detection limit
ƚ = The method detection limit is above the 2L GWQS.
* = The value represents the sum of the reported practical quantitation limit of one analyte and the detected concentration of the other analyte.
J = Detected but below the Reporting Limit (lowest calibration standard); result is an estimated concentration (CLP J-Flag).
L = Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side (L-04 Flag).
MW-3
MW-4
MW-5D
GCL (µg/L)
2L GWQS (µg/L)
6,000,000
6,000
5,000
1
5,900
70
8,800
70
4,000,000
4,000 Ethylbenzenetert-Butylbenzene
14,750
70
70,000
70
400
0.4
70,000
70
80,000
600
50
0.02
MW-1
MW-2 Isopropylbenzene (Cumene)Chloroform 1,2-Dichloroethane Contaminant of
Concern
Acetone Benzene n-Butylbenzenesec-Butylbenzene 2-Butanone (MEK)Well/
Sample
ID Diisopropyl Ether (DIPE)1,2-Dibromoethane (EDB)24,100
400 All Other SM 6200B Analytesp-Isopropyltoluene(p-Cymene)Methyl tert-Butyl Ether (MTBE)Naphthalenen-PropylbenzeneTolueneMethylene Chloride5,000
5
50,000
500
Varies
Varies
260,000
600
28,500
400 1,3,5-TrimethylbenzeneTotal Xylenes1,2,4-TrimethylbenzeneStyrene70,000
70
30,500
70
11,700
25
20,000
20
6,000
6
26,100
70
NCDEQ; 29012_Starflite Food Store #272; T5_Historical GW Results
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

FIGURES
FIGUREPROJECTTITLE
1SITE VICINITY MAP
SITE LOCATION
FAYETTEVIL
L
E
R
D EASTSIDE
DR
Copyright:© 2013 National Geographic Society, i-cubed
2,000 0 2,000 4,0001,000
Feet
³
STARFLITE FOODSTORE #272
1416 FAYETTEVILLE RDROCKINGHAM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072MAY 2023 AS SHOWN KMC/BJA
FIGUREPROJECTTITLE
2POTENTIAL RECEPTOR MAP
SITE LOCATION
1 ,5 0 0 F EET RADIUS
500F E E T RADIUS
FAYETTEVILLE RDEASTSIDE
DR
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
500 0 500 1,000250
Feet
³
STARFLITE FOODSTORE #2721416 FAYETTEVILLE RDROCKINGHAM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072AS SHOWN KMC/BJAMAY 2023
FIGUREPROJECTTITLE
3SITE MAP
!>
!>
!>
!(>!>FAYETTEVILLE R
D
EASTSIDE
DR
MW-5DMW-1
MW-3
MW-4
MW-2
10,000-GAL. GASOLINE USTs (CLOSED IN PLACE)10,000-GAL. KEROSENE UST(CLOSED IN PLACE)
FORMERPUMP ISLANDS
FORMER KEROSENEDISPENSER
Source: Esri, Maxar, Earthstar Geographics, and the GIS User Community
30 0 30 6015
Feet
³
STARFLITE FOODSTORE #272
1416 FAYETTEVILLE RDROCKINGHAM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072AS SHOWN KMC/BJA
NOTE: Well and tank locations were obtained from previous
reports prepared by other consultants and are approximate.
Parcel Boundary
LEGEND
Monitoring Well(Type II)!>
Approximate Location of UST System
Monitoring Well(Deep)((>
MAY 2023
FIGUREPROJECTTITLE
4GRO U NDW ATER EL EV ATIO N –MARCH 1, 2023
!>
!>
!>
!(>!>
<FAYETTEVILLE R
D
EASTSIDE
DR
MW-5D*(276.15)
MW-1(301.33)
MW-3(301.13)
MW-4(302.15)MW-2(302.40)
302.00
301.75
302.25
301.50
301.25
Sourc e: Esri, Ma xa r, Ea rthsta r Geogra p hic s, a nd the GIS U ser Com m unity
30 0 30 6015
Feet
³
STARFL ITE FO O DSTO RE #2721416 FAYETTEV IL L E RDRO CKINGHAM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072AS SHO W N KMC/BJA
PROJECTPROJECT
NO TES: 1. W ell a nd ta nk loc a tions were obta ined from p revious rep orts p rep a red by other c onsulta nts a nd a re a p p roxim a te.2. * = Deep well; eleva tion not used for c ontouring p urp oses.3. The ground wa ter eleva tion c ontour interva l is 0.25 feet.
Pa rc el Bound a ry
LEGEND
Ap p roxim a te L oc a tion of U ST System
Ga uged Monitoring W ell (Deep )
!(>
Ga uged Monitoring W ell (Typ e II)
!>
Ground wa ter FlowDirec tion
Ground wa ter Contour<Ground wa ter Eleva tion (Feet)
(##)
MAY 2023
FIGUREPROJECTTITLE
5
MONIT OR ING W ELLGR OU NDW AT ER SAMP LEANALYT ICAL R ESU LT S –MAR CH 1, 2023
!>
!>
!>
!(>!>FAYETTEVILLE RD
EASTSIDE
DR
MW-5D*MW-1
MW-3
MW-4
MW-2
???
??ESTIMATED HORIZONTALEXTENT OF 2L GWQSEXCEEDANCES
Source: Esri, Maxar, Earthstar Geographics, and the GIS U ser Com m unity
30 0 30 6015
Feet
³
ST AR FLIT E FOODST OR E #2721416 FAYET T EV ILLE R DR OCKINGH AM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072AS SH OW N KMC/BJA
NOT ES: 1. W ell and tank locations were obtained from previous reports prepared by other consultants and are approxim ate.2. * = Deep well; analytical results not used for contouring purposes
P arcel Boundary
LEGEND
Sam pled Monitoring W ell (T ype II)
!>
Approxim ate Location of U ST System
Sam pled Monitoring W ell (Deep)!(>
SUMMARY OF GROUNDWATER LABORATORY RESULTS - STANDARD METHOD 6200BIncident Name and No.: Starflite Food Store #272 - 29012
DateCollected
03/01/23 100 <3.2 ƚ 290 120 <3.4 400 370 15 <19.9 J*03/01/23 1,900 2.8 J 890 59 <1.7 360 160 1,600 2,12003/01/23 56 <1.6 ƚ 850 150 12 680 420 7.8 9803/01/23 <0.18<0.16 ƚ<0.22 <0.15 <0.17 <0.38 <0.12 <0.22 <0.7303/01/23 4.1 <0.16 ƚ 0.53 4.7 38 10 0.25 J <0.22 <0.80 J*
All results in m icrogram s per liter (µg/L).R efer to T able 4 for all results and notes. Bold results are above 2L GW Q S. T otal XylenesEthylbenz eneIsopropylbenz ene (Cum ene)Benz ene
50,000500260,000 60026,100 706,000 6 T oluene n-P ropylbenz eneNaphthalene 1,2-Dibrom oethane (EDB)500.02 Methyl tert-Butyl Ether (MT BE)
20,000 20GCL (µg/L)2L GWQS (µg/L)
Contaminant of Concern
MW -1MW -2MW -3
MW -5D
Well/ Sample ID
MW -4
80,000600 30,500 705,000 1
MAY 2023
FIGUREPROJECTTITLE
6EST IMAT ED HO RIZ O NT ALEX T ENT O F BENZ ENE –MARCH 1, 2023
!>
!>
!>
!(>!>FAYETTEVILLE RDEASTSIDE
DR
MW-5D*(4.1)
MW-1(100)
MW-3(56)
MW-4(<0.18)
MW-2(1,900)(1)(10)
(100)
???
??(1,000)
Source: Esri, Ma xa r, Ea rthsta r Geogra phics, a n d the GIS U ser Com m un ity
30 0 30 6015
Feet
³
ST ARFL IT E FO O DST O RE #2721416 FAYET T EV IL L E RDRO CKINGHAM, NC
INCIDENT NO.JOB NO.DATE SCALE DRAWN BY/CHECKED BY29012221072AS SHO WN KMC/BJA
NO T ES: 1. Well a n d ta n k loca tion s were obta in ed from previous reports prepa red by other con sulta n ts a n d a re a pproxim a te.2. * = Deep well; a n a lytica l results n ot used for con tourin g purposes3. 2L GWQS for Ben zen e is 1 μg/L .
Pa rcel Boun da ry
LEGEND
Approxim a te L oca tionof U ST System
Sa m pled Mon itorin g Well (Deep)!(>
Sa m pled Mon itorin g Well (T ype II)
!>
Ben zen e Estim a ted Isocon cen tra tion
Ben zen e Con cen tra tion (μg/L )
(##)
MAY 2023

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

APPENDICES

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

APPENDIX A HISTORICAL DATA
TABLE 3
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Starflite Food Store 272 (Incident No.: 29012, UST #: FA-1322)
1416 Fayetteville Road, Rockingham, Richmond County, North Carolina
S&ME Project No. 4305-18-100B
UST Facility ID # 0-00-000003830
Method
504.1
Method
6010
Well
ID
Date
Collected
Chloromethane2/11/2003 NA NA NA 2,100 BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL 1,000 BDL BDL 8,200 BDL BDL 470 NR BDL BDL 5,780 390 170 BDL BDL 46 13 11 BDL 8.7
7/3/2013 NA NA NA 384 BDL BDL 50.5 27.6 2.4 NR 1.0 BDL BDL BDL BDL 1,490 150 BDL 71.7 638 354 45.8 NR 88.6 15 107.2 NA NA NA NA NA NA NA NA NA
8/28/2018 <10 <400 <1,000 150 <100 <100 52 25 <10 NR <10 <10 <10 <10 <10 1,300 120 <10 8.6 J 530 350 21 NR 17 <10 39.2 NA NA NA NA NA NA NA NA NA
4/14/2020 <5 <200 56 J 62 <50 <50 40 21 <5 4.8 J <5 <5 <5 <5 <5 860 87 <5 4.3 J 450 290 10 <5 13 1.7 J 30.9 NA NA NA NA NA NA NA NA NA
3/21/2003 NA NA NA 6,300 *BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL 1,900 BDL BDL BDL BDL BDL 11,000 NR BDL BDL 8,700 540 BDL 14 47 88 58 33.48 BDL 8.56
7/3/2013
8/28/2018 1,200 <1,000 <2,500 8,800 *<250 <250 150 44 <25 NR <25 <25 <25 <25 <25 2,900 220 28 8.0 J 1,500 570 9,800 NR 2,800 580 11,000 NA NA NA NA NA NA NA NA NA
4/14/2020 <25 <1,000 <2,500 5,500 *<250 <250 44 17 J <25 <50 <25 <25 <25 <25 <25 1,400 81 <25 <25 640 210 4,600 <25 930 180 4,600 NA NA NA NA NA NA NA NA NA
3/21/2003 NA NA NA 1,200 BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL 1,800 BDL BDL 8,600 BDL BDL BDL NR BDL BDL BDL 750 48 BDL BDL 6.6 22 22.23 BDL 6.16
7/3/2013 NA NA NA 3,580 BDL BDL BDL 1,530 BDL NR BDL BDL BDL BDL BDL 456 29.8 BDL BDL 821 66.1 6,380 NR 1,740 625 7,570 NA NA NA NA NA NA NA NA NA
8/28/2018 <10 200 J <1,000 100 <100 <100 89 27 <10 NR <10 <10 <10 <10 46.9 1,300 140 12 32 720 400 25 NR 1,600 330 1,163 NA NA NA NA NA NA NA NA NA
4/14/2020 <10 <400 <1,000 65 <100 <100 64 24 <10 <20 <10 <10 <10 <10 <10 1,300 120 10 15 700 360 14 <10 1,300 200 873 NA NA NA NA NA NA NA NA NA
3/21/2003 BDL BDL NA BDL BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL BDL BDL 2.2 BDL BDL BDL BDL
7/3/2013 BDL BDL NA BDL BDL BDL BDL BDL BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL NR BDL BDL BDL NA NA NA NA NA NA NA NA NA
8/28/2018 <0.5 <20 <50 <0.5 <5.0 <5.0 <0.5 <0.5 <0.5 NR <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NR <0.5 <0.5 <1.0 NA NA NA NA NA NA NA NA NA
4/14/2020 <0.5 <20 <50 <0.5 <5.0 <5.0 <0.5 <0.5 <0.5 NR <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.37 J <0.5 <0.5 <1.0 NA NA NA NA NA NA NA NA NA
3/21/2003 NA NA BDL 9.6 BDL BDL BDL BDL BDL NR BDL BDL 11 BDL BDL 6 BDL BDL 11 BDL BDL BDL NR BDL BDL 9.5 BDL BDL BDL BDL 24 1.8 0.11 BDL BDL
7/3/2013
8/28/2018 3 390 9.8 J 7.4 5.3 5.1 0.28 J 1.4 0.19 J NR <0.5 0.38 J <0.5 2.7 1.3 1.5 11 <0.5 64 32 0.48 J <0.5 NR 1.9 0.49 J 2.43 NA NA NA NA NA NA NA NA NA
4/14/2020 1.7 330 7.6 J 4.7 7.9 <5 <0.5 0.77 <0.5 <1 <0.5 <0.5 <0.5 1.9 1.0 0.59 5.4 <0.5 56 11 0.27J <0.5 <0.5 0.7 0.16 J 0.65 J NA NA NA NA NA NA NA NA NA
128 10 6,000 1 4,000 100 70 70 70 3 50 0.03 70 70 0.4 600 70 25 20 6 70 600 2,000 400 400 500 6 100 30 0.02 15 400 700 10,000 200
128,000 10,000 6,000,000 5,000 4,000,000 100,000 6,900 8,500 15,000 3,000 50,000 30 70,000 70,000 400 84,500 25,000 11,700 20,000 6,000 30,000 260,000 2,000,000 28,500 25,000 85,500 6,000 100,000 30,000 50 15,000 NE NE NE NE
NE NE 4,500,000 16 450,000 110,000 NE NE NE 52 82 1.5 8.1 1,400 NE 35 180 NE 4,500 35 490 3,800 NE 50 35 77 35 NE NE 1.8 NE 1.7 0.15 NE 32
NE NE 19,000,000 69 1,900,000 470,000 NE NE NE 220 340 25 36 5,900 NE 150 750 NE 20,000 150 2,000 16,000 NE 210 150 320 150 NE NE 7.7 NE 7 1 NE 130
Notes:
Analytes that are not shown for the method were not detected.NA: Analysis for sample not requested.
Concentrations are reported in micrograms per liter (µg/L).BDL : Not detected above laboratory detection limits.
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202 J : Estimated concentration (value between the laboratory method reporting limit and laboratory method detection limits).
Concentrations exceeding the laboratory's detection limits are shown in BOLD fields.NE: Value not established
GCL - Gross Contaminantion Level VISL: Vapor Intrusion Screening Level (Groundwater Screening Level) (February 2018)
Value Exceeds the 2L Standard
Value* Exceeds Gross Contamination Levels
MW-2
MW-3
MW-4
MW-5D
VISL-Non-Residential
2L Standard
GCL
VISL-Residential C9-C18 AliphaticC9-C22 AromaticsMW-1 n-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneNaphthalene2,4-DimethylphenolC5-C8 AliphaticAnalytical Method →MADEP VPH/EPH
Contaminant of Concern →tert-Amyl Methyl Ethertert-Butyl AlcoholBenzene2-Butanone4 Methyl-2-pentanonen-Butylbenzenesec-ButylbenzeneChlorobenzenevinyl chlorideChloroformDiisopropyl ether(Isopropyl ether)tert-ButylbenzenePhenolNot Located; Not Sampled
Not Located; Not Sampled Trichlorofluoromethane Volatile Organic Compounds by Method 6200 or equivalent
C19-C36 AliphaticsAcetoneSemi-Volatile Organic
Compounds by Method 625
EDB1,2-dichloroethaneEthylbenzeneIsopropylbenzenep-IsopropyltolueneMethyl tert-butyl etherNaphthaleneTotal XylenesLeadAPPENDIX A
HISTORICAL DATA (S&ME, 2020)
NCDEQ; 29012_Starflite Food Store #272
CATLIN Project No. 221072
CATLIN Engineers and Scientists
May 2023

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

APPENDIX B SITE PHOTOGRAPHS
APPENDIX B SITE PHOTOGRAPHS – MARCH 1, 2023
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023
View of the site facing southwest.

View of MW-1, facing northeast.
APPENDIX B SITE PHOTOGRAPHS – MARCH 1, 2023
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023
View of MW-2, facing southeast.

View of MW-3, facing northeast.
APPENDIX B SITE PHOTOGRAPHS – MARCH 1, 2023
NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023
View of MW-4, facing south.

View of MW-5D, facing northeast.

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

APPENDIX C

DAILY ACTIVITIES LOG
AND FIELD DATA SHEETS

CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-1 16.89
3.11 2.756
NMT 8.269
20 13.782
2
Method:Bailer Purge Start Time:12:01
Required Bails for 3 Well Volumes:35 Purge Stop Time:12:12
Required Bails for 5 Well Volumes:58 Was Well Purged Dry?no
Number of Bails Removed:35 Sample Time:12:12
Groundwater Removed (gal):8.4
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
12:00 296.53 4.19 12.26 -130.65 28.94
12:01 296.66 3.48 12.25 -113.20 28.62
12:02 296.93 3.55 12.23 -108.23 28.47
12:03 297.03 3.61 12.19 -105.13 28.47
12:04 297.06 3.48 12.17 -103.45 28.53
12:05 297.12 3.48 12.16 -102.36 28.66
12:06 296.71 3.37 12.12 -101.77 28.83
12:07 298.35 3.35 12.08 -102.09 29.05
12:08 297.99 3.38 12.04 -102.16 29.25
12:09 297.89 3.32 12.03 -101.44 29.36
12:10 298.26 3.45 12.00 -103.59 29.50
12:11 297.11 3.50 12.03 -104.32 29.55
Laboratory: Con-Test Analysis:
NCDEQ-Hassan Osman
Monitoring Well Information
Nate Newman
3/1/2023
Starflite Food Store #272
221072
6200B
Laboratory Analysis Information
Geochemical Parameters
Depth to Water (ft below TOC)
mild turbidity light gray
Aqua Troll 600
Turbidity and Additional
Sampling Notes
GROUNDWATER SAMPLING FORM
Water Column (ft below TOC)
One Well Volume (gal)
Three Well Volumes (gal)
Five Well Volumes (gal)
Well Data
Well ID
Depth to Product (ft below TOC)
Total Well Depth (ft)
Purging Information Information
Volume of Groundwater in Well
Well Diameter (inches)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-2 9.77
3.23 1.594
NMT 4.783
13 7.972
2
Method:Bailer Purge Start Time:13:23
Required Bails for 3 Well Volumes:20 Purge Stop Time:13:30
Required Bails for 5 Well Volumes:34 Was Well Purged Dry?YES
Number of Bails Removed:17 Sample Time:13:33
Groundwater Removed (gal):4.1
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
13:23 276.49 5.82 12.27 -104.46 27.69
13:24 277.29 3.08 12.30 -112.99 27.42
13:25 255.50 3.17 12.28 -113.14 27.41
13:26 272.90 3.42 12.25 -111.93 27.42
13:27 268.55 3.71 12.24 -110.96 27.42
13:28 253.02 4.23 12.23 -110.55 27.48
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
moderate turbidity gray.
bailed dry at roughly 17
bails
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Starflite Food Store #272 Nate Newman
221072 3/1/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-3 14.84
3.16 2.422
NMT 7.266
18 12.109
2
Method:Bailer Purge Start Time:13:02
Required Bails for 3 Well Volumes:31 Purge Stop Time:13:12
Required Bails for 5 Well Volumes:51 Was Well Purged Dry?No
Number of Bails Removed:31 Sample Time:13:12
Groundwater Removed (gal):7.4
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
13:02 282.53 3.53 12.25 -100.67 28.45
13:03 300.69 3.43 12.25 -101.59 28.34
13:04 298.88 3.67 12.21 -100.13 28.37
13:05 295.93 3.73 12.16 -97.92 28.49
13:06 294.77 3.61 12.11 -96.51 28.63
13:07 292.19 3.63 12.06 -96.00 28.81
13:08 296.58 3.36 12.02 -96.55 29.03
13:09 295.85 3.22 12.01 -95.92 29.11
13:10 293.68 3.11 11.99 -96.62 29.21
13:11 204.83 5.41 11.98 -96.62 29.26
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
moderate turbidity light gray
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Starflite Food Store #272 Nate Newman
221072 3/1/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-4 15.15
2.85 2.472
NMT 7.417
18 12.362
2
Method:Bailer Purge Start Time:13:47
Required Bails for 3 Well Volumes:31 Purge Stop Time:13:58
Required Bails for 5 Well Volumes:52 Was Well Purged Dry?No
Number of Bails Removed:31 Sample Time:13:58
Groundwater Removed (gal):7.4
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
13:46 156.67 4.93 12.23 -58.92 27.70
13:47 250.03 3.52 12.30 -64.56 27.10
13:48 248.94 3.46 12.27 -68.75 27.06
13:49 258.61 3.39 12.25 -72.21 27.03
13:50 260.33 3.35 12.21 -73.73 27.26
13:51 262.93 3.29 12.16 -73.87 27.46
13:52 261.88 3.23 12.11 -74.24 27.70
13:53 261.44 3.12 12.08 -74.32 27.93
13:54 259.56 3.02 12.07 -72.74 27.98
13:55 257.26 2.93 12.05 -71.24 28.12
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
high turbidity orange/brown
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Starflite Food Store #272 Nate Newman
221072 3/1/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)
CATLIN PROJECT: SAMPLED BY:
CATLIN PROJECT # : DATE SAMPLED:
CLIENT'S NAME:
MW-5D 37.76
28.24 6.162
NMT 18.487
66 30.812
2
Method:Bailer Purge Start Time:11:31
Required Bails for 3 Well Volumes:78 Purge Stop Time:11:43
Required Bails for 5 Well Volumes:129 Was Well Purged Dry?YES
Number of Bails Removed:25 Sample Time:11:55
Groundwater Removed (gal):6.0
Equipment Used:
Time
pH
(Standard Units)
ORP
(mV)
Specific
Cond.
(µS/cm)
Dissolved
Oxygen
(mg/L)
Temperature
(Co)
11:31 83.10 4.95 11.88 -77.93 32.09
11:32 85.72 4.08 11.89 -90.73 32.12
11:33 93.37 3.84 11.97 -105.45 32.11
11:34 83.87 3.61 12.15 -128.84 32.07
11:35 104.54 3.82 12.33 -134.10 32.02
11:36 112.04 3.42 12.40 -139.50 31.94
11:37 118.12 3.25 12.50 -148.21 31.87
11:38 123.39 3.44 12.61 -157.94 31.75
11:39 139.56 3.54 12.61 -158.04 31.58
11:40 141.49 3.52 12.71 -167.66 31.57
Laboratory: Con-Test Analysis:6200B
Depth to Product (ft below TOC)Three Well Volumes (gal)
Total Well Depth (ft) Five Well Volumes (gal)
Well Diameter (inches)
Purging Information Information
Geochemical Parameters
Aqua Troll 600
Turbidity and Additional
Sampling Notes
incredibly slow recharge.
bailed dry at roughly 25
bails. clear
Laboratory Analysis Information
Depth to Water (ft below TOC) One Well Volume (gal)
GROUNDWATER SAMPLING FORM
Starflite Food Store #272 Nate Newman
221072 3/1/2023
NCDEQ-Hassan Osman
Monitoring Well Information
Well Data Volume of Groundwater in Well
Well ID Water Column (ft below TOC)

NCDEQ; 29012_Starflite Food Store #272 CATLIN Engineers and Scientists
CATLIN Project No. 221072 May 2023

APPENDIX D

LABORATORY ANALYTICAL REPORT AND
CHAIN OF CUSTODY DOCUMENT

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 17, 2023
Sean O’Neil
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
Project Location: Rockingham, NC
Client Job Number:
Project Number: 221072
Laboratory Work Order Number: 23C0255
Enclosed are results of analyses for samples as received by the laboratory on March 2, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kaitlyn A. Feliciano
Project Manager
Page 1 of 30
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 6
Sample Results 7
23C0255-01 7
23C0255-02 9
23C0255-03 11
23C0255-04 13
23C0255-05 15
23C0255-06 17
Sample Preparation Information 19
QC Data 20
Volatile Organic Compounds by GC/MS 20
B333130 20
B333306 24
Flag/Qualifier Summary 25
Certifications 26
Chain of Custody/Sample Receipt 28
Page 2 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/17/2023
CATLIN Engineers & Scientists
1044 Washington Street
Raleigh, NC 27605
ATTN: Sean O’Neil
221072
23C0255
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Rockingham, NC
230301-5
MW-1 23C0255-01 Ground Water SM21-23 6200B
MW-2 23C0255-02 Ground Water SM21-23 6200B
MW-3 23C0255-03 Ground Water SM21-23 6200B
MW-4 23C0255-04 Ground Water SM21-23 6200B
MW-5D 23C0255-05 Ground Water SM21-23 6200B
Trip Blank 23C0255-06 Ground Water SM21-23 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-01MW-1
DL
1,2,4-Trimethylbenzene 11 10 g/L SM21-23 6200B4.0
Benzene 100 10 g/L SM21-23 6200B3.7
Ethylbenzene 290 10 g/L SM21-23 6200B4.4
Isopropylbenzene (Cumene)120 10 g/L SM21-23 6200B3.0
m+p Xylene 15 20 g/L SM21-23 6200BJ9.8
Naphthalene 400 10 g/L SM21-23 6200B7.6
n-Butylbenzene 45 10 g/L SM21-23 6200B3.0
n-Propylbenzene 370 10 g/L SM21-23 6200B2.5
sec-Butylbenzene 24 10 g/L SM21-23 6200B2.5
Toluene 15 10 g/L SM21-23 6200B4.5
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-02MW-2
DL
1,2,4-Trimethylbenzene 400 5.0 g/L SM21-23 6200B2.0
1,2-Dibromoethane (EDB)2.8 5.0 g/L SM21-23 6200BJ1.6
1,3,5-Trimethylbenzene 120 5.0 g/L SM21-23 6200B1.5
Benzene 1900 5.0 g/L SM21-23 6200B1.8
Ethylbenzene 890 5.0 g/L SM21-23 6200B2.2
Isopropylbenzene (Cumene)59 5.0 g/L SM21-23 6200B1.5
m+p Xylene 1500 10 g/L SM21-23 6200B4.9
Naphthalene 360 5.0 g/L SM21-23 6200B3.8
n-Butylbenzene 30 5.0 g/L SM21-23 6200B1.5
n-Propylbenzene 160 5.0 g/L SM21-23 6200B1.2
o-Xylene 620 5.0 g/L SM21-23 6200B2.4
p-Isopropyltoluene (p-Cymene)4.1 5.0 g/L SM21-23 6200BJ1.3
sec-Butylbenzene 15 5.0 g/L SM21-23 6200B1.3
Styrene 2.8 5.0 g/L SM21-23 6200BJ1.5
Toluene 1600 100 g/L SM21-23 6200B45
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-03MW-3
DL
1,2,4-Trimethylbenzene 50 5.0 g/L SM21-23 6200B2.0
1,3,5-Trimethylbenzene 21 5.0 g/L SM21-23 6200B1.5
Benzene 56 5.0 g/L SM21-23 6200B1.8
Ethylbenzene 850 5.0 g/L SM21-23 6200B2.2
Isopropylbenzene (Cumene)150 5.0 g/L SM21-23 6200B1.5
m+p Xylene 89 10 g/L SM21-23 6200B4.9
Methyl tert-Butyl Ether (MTBE)12 5.0 g/L SM21-23 6200B1.7
Naphthalene 680 5.0 g/L SM21-23 6200B3.8
n-Butylbenzene 41 5.0 g/L SM21-23 6200B1.5
n-Propylbenzene 420 5.0 g/L SM21-23 6200B1.2
o-Xylene 9.0 5.0 g/L SM21-23 6200B2.4
p-Isopropyltoluene (p-Cymene)2.6 5.0 g/L SM21-23 6200BJ1.3
sec-Butylbenzene 25 5.0 g/L SM21-23 6200B1.3
Toluene 7.8 5.0 g/L SM21-23 6200B2.2
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-04MW-4
DL
Acetone 3.6 50 g/L SM21-23 6200BJ2.0
Page 4 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-05MW-5D
DL
1,2,4-Trimethylbenzene 0.48 0.50 g/L SM21-23 6200BJ0.20
2-Butanone (MEK)19 5.0 g/L SM21-23 6200B1.7
Acetone 9.0 50 g/L SM21-23 6200BJ2.0
Benzene 4.1 0.50 g/L SM21-23 6200B0.18
Diisopropyl Ether (DIPE)1.3 0.50 g/L SM21-23 6200B0.20
Ethylbenzene 0.53 0.50 g/L SM21-23 6200B0.22
Isopropylbenzene (Cumene)4.7 0.50 g/L SM21-23 6200B0.15
m+p Xylene 0.56 1.0 g/L SM21-23 6200BJ0.49
Methyl tert-Butyl Ether (MTBE)38 0.50 g/L SM21-23 6200B0.17
Naphthalene 10 0.50 g/L SM21-23 6200B0.38
n-Propylbenzene 0.25 0.50 g/L SM21-23 6200BJ0.12
sec-Butylbenzene 0.67 0.50 g/L SM21-23 6200B0.13
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
23C0255-06Trip Blank
DL
Acetone 2.8 50 g/L SM21-23 6200BJ2.0
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 5 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 23C0255-01,02+03 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-23 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2,2-Dichloropropane
23C0255-01[MW-1], 23C0255-02[MW-2], 23C0255-03[MW-3], 23C0255-04[MW-4], 23C0255-05[MW-5D], 23C0255-06[Trip Blank], B333130-BLK1, B333130-BS1,
B333130-BSD1, S084140-CCV1
Vinyl Acetate
23C0255-01[MW-1], 23C0255-02[MW-2], 23C0255-03[MW-3], 23C0255-04[MW-4], 23C0255-05[MW-5D], 23C0255-06[Trip Blank], B333130-BLK1, B333130-BS1,
B333130-BSD1, S084140-CCV1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
23C0255-01[MW-1], 23C0255-02[MW-2], 23C0255-03[MW-3]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Meghan E. Kelley
Reporting Specialist
Page 6 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/1/2023 12:12
[TOC_2]23C0255-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 3/4/23 12:56 EEHg/L40 3/3/23SM21-23 6200B20Acetone
100 10 3/4/23 12:56 EEHg/L3.7 3/3/23SM21-23 6200B20Benzene
ND 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B20Bromobenzene
ND 10 3/4/23 12:56 EEHg/L5.7 3/3/23SM21-23 6200B20Bromochloromethane
ND 10 3/4/23 12:56 EEHg/L3.2 3/3/23SM21-23 6200B20Bromodichloromethane
ND 10 3/4/23 12:56 EEHg/L8.2 3/3/23SM21-23 6200B20Bromoform
ND 40 3/4/23 12:56 EEHg/L26 3/3/23SM21-23 6200B20Bromomethane
ND 100 3/4/23 12:56 EEHg/L34 3/3/23SM21-23 6200B202-Butanone (MEK)
45 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B20n-Butylbenzene
24 10 3/4/23 12:56 EEHg/L2.5 3/3/23SM21-23 6200B20sec-Butylbenzene
ND 10 3/4/23 12:56 EEHg/L2.8 3/3/23SM21-23 6200B20tert-Butylbenzene
ND 10 3/4/23 12:56 EEHg/L3.3 3/3/23SM21-23 6200B20Carbon Tetrachloride
ND 10 3/4/23 12:56 EEHg/L2.4 3/3/23SM21-23 6200B20Chlorobenzene
ND 1000 3/4/23 12:56 EEHg/L410 3/3/23SM21-23 6200B20Ethanol
ND 10 3/4/23 12:56 EEHg/L4.0 3/3/23SM21-23 6200B20Chlorodibromomethane
ND 10 3/4/23 12:56 EEHg/L6.8 3/3/23SM21-23 6200B20Chloroethane
ND 10 3/4/23 12:56 EEHg/L2.8 3/3/23SM21-23 6200B20Chloroform
ND 12 3/4/23 12:56 EEHg/L10 3/3/23SM21-23 6200B20Chloromethane
ND 10 3/4/23 12:56 EEHg/L3.1 3/3/23SM21-23 6200B202-Chlorotoluene
ND 10 3/4/23 12:56 EEHg/L3.1 3/3/23SM21-23 6200B204-Chlorotoluene
ND 10 3/4/23 12:56 EEHg/L3.2 3/3/23SM21-23 6200B201,2-Dibromoethane (EDB)
ND 10 3/4/23 12:56 EEHg/L2.6 3/3/23SM21-23 6200B201,2-Dichlorobenzene
ND 10 3/4/23 12:56 EEHg/L2.7 3/3/23SM21-23 6200B201,3-Dichlorobenzene
ND 10 3/4/23 12:56 EEHg/L2.6 3/3/23SM21-23 6200B201,4-Dichlorobenzene
ND 10 3/4/23 12:56 EEHg/L3.2 3/3/23SM21-23 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 3/4/23 12:56 EEHg/L2.7 3/3/23SM21-23 6200B201,1-Dichloroethane
ND 20 3/4/23 12:56 EEHg/L6.1 3/3/23SM21-23 6200B201,2-Dichloroethane
ND 10 3/4/23 12:56 EEHg/L2.8 3/3/23SM21-23 6200B201,1-Dichloroethylene
ND 10 3/4/23 12:56 EEHg/L2.8 3/3/23SM21-23 6200B20cis-1,2-Dichloroethylene
ND 10 3/4/23 12:56 EEHg/L3.4 3/3/23SM21-23 6200B20trans-1,2-Dichloroethylene
ND 10 3/4/23 12:56 EEHg/L3.9 3/3/23SM21-23 6200B201,2-Dichloropropane
ND 10 3/4/23 12:56 EEHg/L2.3 3/3/23SM21-23 6200B201,3-Dichloropropane
ND 10 3/4/23 12:56 EEHg/L7.0 3/3/23SM21-23 6200B20L-042,2-Dichloropropane
ND 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B201,1-Dichloropropene
ND 10 3/4/23 12:56 EEHg/L3.3 3/3/23SM21-23 6200B20cis-1,3-Dichloropropene
ND 10 3/4/23 12:56 EEHg/L2.8 3/3/23SM21-23 6200B20trans-1,3-Dichloropropene
ND 10 3/4/23 12:56 EEHg/L4.0 3/3/23SM21-23 6200B20Diisopropyl Ether (DIPE)
290 10 3/4/23 12:56 EEHg/L4.4 3/3/23SM21-23 6200B20Ethylbenzene
ND 100 3/4/23 12:56 EEHg/L24 3/3/23SM21-23 6200B202-Hexanone (MBK)
120 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B20Isopropylbenzene (Cumene)
ND 10 3/4/23 12:56 EEHg/L2.5 3/3/23SM21-23 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 3/4/23 12:56 EEHg/L3.4 3/3/23SM21-23 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 3/4/23 12:56 EEHg/L3.5 3/3/23SM21-23 6200B20Methylene Chloride
ND 100 3/4/23 12:56 EEHg/L26 3/3/23SM21-23 6200B204-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 7 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 3/1/2023 12:12
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
400 10 3/4/23 12:56 EEHg/L7.6 3/3/23SM21-23 6200B20Naphthalene
370 10 3/4/23 12:56 EEHg/L2.5 3/3/23SM21-23 6200B20n-Propylbenzene
ND 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B20Styrene
ND 10 3/4/23 12:56 EEHg/L2.7 3/3/23SM21-23 6200B201,1,2,2-Tetrachloroethane
ND 10 3/4/23 12:56 EEHg/L3.4 3/3/23SM21-23 6200B20Tetrachloroethylene
15 10 3/4/23 12:56 EEHg/L4.5 3/3/23SM21-23 6200B20Toluene
ND 20 3/4/23 12:56 EEHg/L6.8 3/3/23SM21-23 6200B201,2,3-Trichlorobenzene
ND 10 3/4/23 12:56 EEHg/L6.0 3/3/23SM21-23 6200B201,2,4-Trichlorobenzene
ND 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B201,1,1-Trichloroethane
ND 10 3/4/23 12:56 EEHg/L3.8 3/3/23SM21-23 6200B201,1,2-Trichloroethane
ND 10 3/4/23 12:56 EEHg/L3.5 3/3/23SM21-23 6200B20Trichloroethylene
ND 10 3/4/23 12:56 EEHg/L3.1 3/3/23SM21-23 6200B20Trichlorofluoromethane (Freon 11)
ND 10 3/4/23 12:56 EEHg/L5.5 3/3/23SM21-23 6200B201,2,3-Trichloropropane
11 10 3/4/23 12:56 EEHg/L4.0 3/3/23SM21-23 6200B201,2,4-Trimethylbenzene
ND 10 3/4/23 12:56 EEHg/L3.0 3/3/23SM21-23 6200B201,3,5-Trimethylbenzene
ND 400 3/4/23 12:56 EEHg/L33 3/3/23SM21-23 6200B20L-04Vinyl Acetate
ND 10 3/4/23 12:56 EEHg/L4.7 3/3/23SM21-23 6200B20Vinyl Chloride
15 20 3/4/23 12:56 EEHg/L9.8 3/3/23SM21-23 6200B20Jm+p Xylene
ND 10 3/4/23 12:56 EEHg/L4.9 3/3/23SM21-23 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.4 3/4/23 12:5670-130
Toluene-d8 101 3/4/23 12:5670-130
4-Bromofluorobenzene 106 3/4/23 12:5670-130
Page 8 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:33
[TOC_2]23C0255-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 3/4/23 13:25 EEHg/L20 3/3/23SM21-23 6200B10Acetone
1900 5.0 3/4/23 13:25 EEHg/L1.8 3/3/23SM21-23 6200B10Benzene
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B10Bromobenzene
ND 5.0 3/4/23 13:25 EEHg/L2.8 3/3/23SM21-23 6200B10Bromochloromethane
ND 5.0 3/4/23 13:25 EEHg/L1.6 3/3/23SM21-23 6200B10Bromodichloromethane
ND 5.0 3/4/23 13:25 EEHg/L4.1 3/3/23SM21-23 6200B10Bromoform
ND 20 3/4/23 13:25 EEHg/L13 3/3/23SM21-23 6200B10Bromomethane
ND 50 3/4/23 13:25 EEHg/L17 3/3/23SM21-23 6200B102-Butanone (MEK)
30 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B10n-Butylbenzene
15 5.0 3/4/23 13:25 EEHg/L1.3 3/3/23SM21-23 6200B10sec-Butylbenzene
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B10tert-Butylbenzene
ND 5.0 3/4/23 13:25 EEHg/L1.6 3/3/23SM21-23 6200B10Carbon Tetrachloride
ND 5.0 3/4/23 13:25 EEHg/L1.2 3/3/23SM21-23 6200B10Chlorobenzene
ND 500 3/4/23 13:25 EEHg/L200 3/3/23SM21-23 6200B10Ethanol
ND 5.0 3/4/23 13:25 EEHg/L2.0 3/3/23SM21-23 6200B10Chlorodibromomethane
ND 5.0 3/4/23 13:25 EEHg/L3.4 3/3/23SM21-23 6200B10Chloroethane
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B10Chloroform
ND 6.0 3/4/23 13:25 EEHg/L5.0 3/3/23SM21-23 6200B10Chloromethane
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B102-Chlorotoluene
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B104-Chlorotoluene
2.8 5.0 3/4/23 13:25 EEHg/L1.6 3/3/23SM21-23 6200B10J1,2-Dibromoethane (EDB)
ND 5.0 3/4/23 13:25 EEHg/L1.3 3/3/23SM21-23 6200B101,2-Dichlorobenzene
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B101,3-Dichlorobenzene
ND 5.0 3/4/23 13:25 EEHg/L1.3 3/3/23SM21-23 6200B101,4-Dichlorobenzene
ND 5.0 3/4/23 13:25 EEHg/L1.6 3/3/23SM21-23 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B101,1-Dichloroethane
ND 10 3/4/23 13:25 EEHg/L3.0 3/3/23SM21-23 6200B101,2-Dichloroethane
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B101,1-Dichloroethylene
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B10cis-1,2-Dichloroethylene
ND 5.0 3/4/23 13:25 EEHg/L1.7 3/3/23SM21-23 6200B10trans-1,2-Dichloroethylene
ND 5.0 3/4/23 13:25 EEHg/L1.9 3/3/23SM21-23 6200B101,2-Dichloropropane
ND 5.0 3/4/23 13:25 EEHg/L1.2 3/3/23SM21-23 6200B101,3-Dichloropropane
ND 5.0 3/4/23 13:25 EEHg/L3.5 3/3/23SM21-23 6200B10L-042,2-Dichloropropane
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B101,1-Dichloropropene
ND 5.0 3/4/23 13:25 EEHg/L1.6 3/3/23SM21-23 6200B10cis-1,3-Dichloropropene
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B10trans-1,3-Dichloropropene
ND 5.0 3/4/23 13:25 EEHg/L2.0 3/3/23SM21-23 6200B10Diisopropyl Ether (DIPE)
890 5.0 3/4/23 13:25 EEHg/L2.2 3/3/23SM21-23 6200B10Ethylbenzene
ND 50 3/4/23 13:25 EEHg/L12 3/3/23SM21-23 6200B102-Hexanone (MBK)
59 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B10Isopropylbenzene (Cumene)
4.1 5.0 3/4/23 13:25 EEHg/L1.3 3/3/23SM21-23 6200B10Jp-Isopropyltoluene (p-Cymene)
ND 5.0 3/4/23 13:25 EEHg/L1.7 3/3/23SM21-23 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 3/4/23 13:25 EEHg/L1.8 3/3/23SM21-23 6200B10Methylene Chloride
ND 50 3/4/23 13:25 EEHg/L13 3/3/23SM21-23 6200B104-Methyl-2-pentanone (MIBK)
Page 9 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-02
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:33
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
360 5.0 3/4/23 13:25 EEHg/L3.8 3/3/23SM21-23 6200B10Naphthalene
160 5.0 3/4/23 13:25 EEHg/L1.2 3/3/23SM21-23 6200B10n-Propylbenzene
2.8 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B10JStyrene
ND 5.0 3/4/23 13:25 EEHg/L1.4 3/3/23SM21-23 6200B101,1,2,2-Tetrachloroethane
ND 5.0 3/4/23 13:25 EEHg/L1.7 3/3/23SM21-23 6200B10Tetrachloroethylene
1600 100 3/7/23 14:57 MFFg/L45 3/6/23SM21-23 6200B200Toluene
ND 10 3/4/23 13:25 EEHg/L3.4 3/3/23SM21-23 6200B101,2,3-Trichlorobenzene
ND 5.0 3/4/23 13:25 EEHg/L3.0 3/3/23SM21-23 6200B101,2,4-Trichlorobenzene
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B101,1,1-Trichloroethane
ND 5.0 3/4/23 13:25 EEHg/L1.9 3/3/23SM21-23 6200B101,1,2-Trichloroethane
ND 5.0 3/4/23 13:25 EEHg/L1.7 3/3/23SM21-23 6200B10Trichloroethylene
ND 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 3/4/23 13:25 EEHg/L2.8 3/3/23SM21-23 6200B101,2,3-Trichloropropane
400 5.0 3/4/23 13:25 EEHg/L2.0 3/3/23SM21-23 6200B101,2,4-Trimethylbenzene
120 5.0 3/4/23 13:25 EEHg/L1.5 3/3/23SM21-23 6200B101,3,5-Trimethylbenzene
ND 200 3/4/23 13:25 EEHg/L17 3/3/23SM21-23 6200B10L-04Vinyl Acetate
ND 5.0 3/4/23 13:25 EEHg/L2.4 3/3/23SM21-23 6200B10Vinyl Chloride
1500 10 3/4/23 13:25 EEHg/L4.9 3/3/23SM21-23 6200B10m+p Xylene
620 5.0 3/4/23 13:25 EEHg/L2.4 3/3/23SM21-23 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.4 3/4/23 13:2570-130
1,2-Dichloroethane-d4 111 3/7/23 14:5770-130
Toluene-d8 99.0 3/4/23 13:2570-130
Toluene-d8 103 3/7/23 14:5770-130
4-Bromofluorobenzene 106 3/4/23 13:2570-130
4-Bromofluorobenzene 95.6 3/7/23 14:5770-130
Page 10 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:12
[TOC_2]23C0255-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 3/4/23 13:52 EEHg/L20 3/3/23SM21-23 6200B10Acetone
56 5.0 3/4/23 13:52 EEHg/L1.8 3/3/23SM21-23 6200B10Benzene
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B10Bromobenzene
ND 5.0 3/4/23 13:52 EEHg/L2.8 3/3/23SM21-23 6200B10Bromochloromethane
ND 5.0 3/4/23 13:52 EEHg/L1.6 3/3/23SM21-23 6200B10Bromodichloromethane
ND 5.0 3/4/23 13:52 EEHg/L4.1 3/3/23SM21-23 6200B10Bromoform
ND 20 3/4/23 13:52 EEHg/L13 3/3/23SM21-23 6200B10Bromomethane
ND 50 3/4/23 13:52 EEHg/L17 3/3/23SM21-23 6200B102-Butanone (MEK)
41 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B10n-Butylbenzene
25 5.0 3/4/23 13:52 EEHg/L1.3 3/3/23SM21-23 6200B10sec-Butylbenzene
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B10tert-Butylbenzene
ND 5.0 3/4/23 13:52 EEHg/L1.6 3/3/23SM21-23 6200B10Carbon Tetrachloride
ND 5.0 3/4/23 13:52 EEHg/L1.2 3/3/23SM21-23 6200B10Chlorobenzene
ND 500 3/4/23 13:52 EEHg/L200 3/3/23SM21-23 6200B10Ethanol
ND 5.0 3/4/23 13:52 EEHg/L2.0 3/3/23SM21-23 6200B10Chlorodibromomethane
ND 5.0 3/4/23 13:52 EEHg/L3.4 3/3/23SM21-23 6200B10Chloroethane
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B10Chloroform
ND 6.0 3/4/23 13:52 EEHg/L5.0 3/3/23SM21-23 6200B10Chloromethane
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B102-Chlorotoluene
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B104-Chlorotoluene
ND 5.0 3/4/23 13:52 EEHg/L1.6 3/3/23SM21-23 6200B101,2-Dibromoethane (EDB)
ND 5.0 3/4/23 13:52 EEHg/L1.3 3/3/23SM21-23 6200B101,2-Dichlorobenzene
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B101,3-Dichlorobenzene
ND 5.0 3/4/23 13:52 EEHg/L1.3 3/3/23SM21-23 6200B101,4-Dichlorobenzene
ND 5.0 3/4/23 13:52 EEHg/L1.6 3/3/23SM21-23 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B101,1-Dichloroethane
ND 10 3/4/23 13:52 EEHg/L3.0 3/3/23SM21-23 6200B101,2-Dichloroethane
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B101,1-Dichloroethylene
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B10cis-1,2-Dichloroethylene
ND 5.0 3/4/23 13:52 EEHg/L1.7 3/3/23SM21-23 6200B10trans-1,2-Dichloroethylene
ND 5.0 3/4/23 13:52 EEHg/L1.9 3/3/23SM21-23 6200B101,2-Dichloropropane
ND 5.0 3/4/23 13:52 EEHg/L1.2 3/3/23SM21-23 6200B101,3-Dichloropropane
ND 5.0 3/4/23 13:52 EEHg/L3.5 3/3/23SM21-23 6200B10L-042,2-Dichloropropane
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B101,1-Dichloropropene
ND 5.0 3/4/23 13:52 EEHg/L1.6 3/3/23SM21-23 6200B10cis-1,3-Dichloropropene
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B10trans-1,3-Dichloropropene
ND 5.0 3/4/23 13:52 EEHg/L2.0 3/3/23SM21-23 6200B10Diisopropyl Ether (DIPE)
850 5.0 3/4/23 13:52 EEHg/L2.2 3/3/23SM21-23 6200B10Ethylbenzene
ND 50 3/4/23 13:52 EEHg/L12 3/3/23SM21-23 6200B102-Hexanone (MBK)
150 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B10Isopropylbenzene (Cumene)
2.6 5.0 3/4/23 13:52 EEHg/L1.3 3/3/23SM21-23 6200B10Jp-Isopropyltoluene (p-Cymene)
12 5.0 3/4/23 13:52 EEHg/L1.7 3/3/23SM21-23 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 3/4/23 13:52 EEHg/L1.8 3/3/23SM21-23 6200B10Methylene Chloride
ND 50 3/4/23 13:52 EEHg/L13 3/3/23SM21-23 6200B104-Methyl-2-pentanone (MIBK)
Page 11 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:12
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
680 5.0 3/4/23 13:52 EEHg/L3.8 3/3/23SM21-23 6200B10Naphthalene
420 5.0 3/4/23 13:52 EEHg/L1.2 3/3/23SM21-23 6200B10n-Propylbenzene
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B10Styrene
ND 5.0 3/4/23 13:52 EEHg/L1.4 3/3/23SM21-23 6200B101,1,2,2-Tetrachloroethane
ND 5.0 3/4/23 13:52 EEHg/L1.7 3/3/23SM21-23 6200B10Tetrachloroethylene
7.8 5.0 3/4/23 13:52 EEHg/L2.2 3/3/23SM21-23 6200B10Toluene
ND 10 3/4/23 13:52 EEHg/L3.4 3/3/23SM21-23 6200B101,2,3-Trichlorobenzene
ND 5.0 3/4/23 13:52 EEHg/L3.0 3/3/23SM21-23 6200B101,2,4-Trichlorobenzene
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B101,1,1-Trichloroethane
ND 5.0 3/4/23 13:52 EEHg/L1.9 3/3/23SM21-23 6200B101,1,2-Trichloroethane
ND 5.0 3/4/23 13:52 EEHg/L1.7 3/3/23SM21-23 6200B10Trichloroethylene
ND 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 3/4/23 13:52 EEHg/L2.8 3/3/23SM21-23 6200B101,2,3-Trichloropropane
50 5.0 3/4/23 13:52 EEHg/L2.0 3/3/23SM21-23 6200B101,2,4-Trimethylbenzene
21 5.0 3/4/23 13:52 EEHg/L1.5 3/3/23SM21-23 6200B101,3,5-Trimethylbenzene
ND 200 3/4/23 13:52 EEHg/L17 3/3/23SM21-23 6200B10L-04Vinyl Acetate
ND 5.0 3/4/23 13:52 EEHg/L2.4 3/3/23SM21-23 6200B10Vinyl Chloride
89 10 3/4/23 13:52 EEHg/L4.9 3/3/23SM21-23 6200B10m+p Xylene
9.0 5.0 3/4/23 13:52 EEHg/L2.4 3/3/23SM21-23 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.4 3/4/23 13:5270-130
Toluene-d8 99.1 3/4/23 13:5270-130
4-Bromofluorobenzene 106 3/4/23 13:5270-130
Page 12 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:58
[TOC_2]23C0255-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.6 50 3/4/23 8:48 EEHg/L2.0 3/3/23SM21-23 6200B1JAcetone
ND 0.50 3/4/23 8:48 EEHg/L0.18 3/3/23SM21-23 6200B1Benzene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B1Bromobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.28 3/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 3/4/23 8:48 EEHg/L0.16 3/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 3/4/23 8:48 EEHg/L0.41 3/3/23SM21-23 6200B1Bromoform
ND 2.0 3/4/23 8:48 EEHg/L1.3 3/3/23SM21-23 6200B1Bromomethane
ND 5.0 3/4/23 8:48 EEHg/L1.7 3/3/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B1n-Butylbenzene
ND 0.50 3/4/23 8:48 EEHg/L0.13 3/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 3/4/23 8:48 EEHg/L0.16 3/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 3/4/23 8:48 EEHg/L0.12 3/3/23SM21-23 6200B1Chlorobenzene
ND 50 3/4/23 8:48 EEHg/L20 3/3/23SM21-23 6200B1Ethanol
ND 0.50 3/4/23 8:48 EEHg/L0.20 3/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 3/4/23 8:48 EEHg/L0.34 3/3/23SM21-23 6200B1Chloroethane
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B1Chloroform
ND 0.60 3/4/23 8:48 EEHg/L0.50 3/3/23SM21-23 6200B1Chloromethane
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 3/4/23 8:48 EEHg/L0.16 3/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/4/23 8:48 EEHg/L0.13 3/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.13 3/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.16 3/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 3/4/23 8:48 EEHg/L0.30 3/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/4/23 8:48 EEHg/L0.17 3/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/4/23 8:48 EEHg/L0.19 3/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 3/4/23 8:48 EEHg/L0.12 3/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 3/4/23 8:48 EEHg/L0.35 3/3/23SM21-23 6200B1L-042,2-Dichloropropane
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 3/4/23 8:48 EEHg/L0.16 3/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 3/4/23 8:48 EEHg/L0.20 3/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/4/23 8:48 EEHg/L0.22 3/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 3/4/23 8:48 EEHg/L1.2 3/3/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/4/23 8:48 EEHg/L0.13 3/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/4/23 8:48 EEHg/L0.17 3/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/4/23 8:48 EEHg/L0.18 3/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 3/4/23 8:48 EEHg/L1.3 3/3/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
Page 13 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/1/2023 13:58
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/4/23 8:48 EEHg/L0.38 3/3/23SM21-23 6200B1Naphthalene
ND 0.50 3/4/23 8:48 EEHg/L0.12 3/3/23SM21-23 6200B1n-Propylbenzene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B1Styrene
ND 0.50 3/4/23 8:48 EEHg/L0.14 3/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/4/23 8:48 EEHg/L0.17 3/3/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 3/4/23 8:48 EEHg/L0.22 3/3/23SM21-23 6200B1Toluene
ND 1.0 3/4/23 8:48 EEHg/L0.34 3/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.30 3/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 3/4/23 8:48 EEHg/L0.19 3/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 3/4/23 8:48 EEHg/L0.17 3/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/4/23 8:48 EEHg/L0.28 3/3/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 3/4/23 8:48 EEHg/L0.20 3/3/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 3/4/23 8:48 EEHg/L0.15 3/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 3/4/23 8:48 EEHg/L1.7 3/3/23SM21-23 6200B1L-04Vinyl Acetate
ND 0.50 3/4/23 8:48 EEHg/L0.24 3/3/23SM21-23 6200B1Vinyl Chloride
ND 1.0 3/4/23 8:48 EEHg/L0.49 3/3/23SM21-23 6200B1m+p Xylene
ND 0.50 3/4/23 8:48 EEHg/L0.24 3/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.1 3/4/23 8:4870-130
Toluene-d8 99.7 3/4/23 8:4870-130
4-Bromofluorobenzene 105 3/4/23 8:4870-130
Page 14 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-05
Field Sample #: MW-5D
Sample Matrix: Ground Water
Sampled: 3/1/2023 11:55
[TOC_2]23C0255-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
9.0 50 3/4/23 12:00 EEHg/L2.0 3/3/23SM21-23 6200B1JAcetone
4.1 0.50 3/4/23 12:00 EEHg/L0.18 3/3/23SM21-23 6200B1Benzene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B1Bromobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.28 3/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 3/4/23 12:00 EEHg/L0.16 3/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 3/4/23 12:00 EEHg/L0.41 3/3/23SM21-23 6200B1Bromoform
ND 2.0 3/4/23 12:00 EEHg/L1.3 3/3/23SM21-23 6200B1Bromomethane
19 5.0 3/4/23 12:00 EEHg/L1.7 3/3/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B1n-Butylbenzene
0.67 0.50 3/4/23 12:00 EEHg/L0.13 3/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 3/4/23 12:00 EEHg/L0.16 3/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 3/4/23 12:00 EEHg/L0.12 3/3/23SM21-23 6200B1Chlorobenzene
ND 50 3/4/23 12:00 EEHg/L20 3/3/23SM21-23 6200B1Ethanol
ND 0.50 3/4/23 12:00 EEHg/L0.20 3/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 3/4/23 12:00 EEHg/L0.34 3/3/23SM21-23 6200B1Chloroethane
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B1Chloroform
ND 0.60 3/4/23 12:00 EEHg/L0.50 3/3/23SM21-23 6200B1Chloromethane
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 3/4/23 12:00 EEHg/L0.16 3/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/4/23 12:00 EEHg/L0.13 3/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.13 3/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.16 3/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 3/4/23 12:00 EEHg/L0.30 3/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/4/23 12:00 EEHg/L0.17 3/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/4/23 12:00 EEHg/L0.19 3/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 3/4/23 12:00 EEHg/L0.12 3/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 3/4/23 12:00 EEHg/L0.35 3/3/23SM21-23 6200B1L-042,2-Dichloropropane
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 3/4/23 12:00 EEHg/L0.16 3/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B1trans-1,3-Dichloropropene
1.3 0.50 3/4/23 12:00 EEHg/L0.20 3/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
0.53 0.50 3/4/23 12:00 EEHg/L0.22 3/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 3/4/23 12:00 EEHg/L1.2 3/3/23SM21-23 6200B12-Hexanone (MBK)
4.7 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/4/23 12:00 EEHg/L0.13 3/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
38 0.50 3/4/23 12:00 EEHg/L0.17 3/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/4/23 12:00 EEHg/L0.18 3/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 3/4/23 12:00 EEHg/L1.3 3/3/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
Page 15 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-05
Field Sample #: MW-5D
Sample Matrix: Ground Water
Sampled: 3/1/2023 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
10 0.50 3/4/23 12:00 EEHg/L0.38 3/3/23SM21-23 6200B1Naphthalene
0.25 0.50 3/4/23 12:00 EEHg/L0.12 3/3/23SM21-23 6200B1Jn-Propylbenzene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B1Styrene
ND 0.50 3/4/23 12:00 EEHg/L0.14 3/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/4/23 12:00 EEHg/L0.17 3/3/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 3/4/23 12:00 EEHg/L0.22 3/3/23SM21-23 6200B1Toluene
ND 1.0 3/4/23 12:00 EEHg/L0.34 3/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.30 3/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 3/4/23 12:00 EEHg/L0.19 3/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 3/4/23 12:00 EEHg/L0.17 3/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/4/23 12:00 EEHg/L0.28 3/3/23SM21-23 6200B11,2,3-Trichloropropane
0.48 0.50 3/4/23 12:00 EEHg/L0.20 3/3/23SM21-23 6200B1J1,2,4-Trimethylbenzene
ND 0.50 3/4/23 12:00 EEHg/L0.15 3/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 3/4/23 12:00 EEHg/L1.7 3/3/23SM21-23 6200B1L-04Vinyl Acetate
ND 0.50 3/4/23 12:00 EEHg/L0.24 3/3/23SM21-23 6200B1Vinyl Chloride
0.56 1.0 3/4/23 12:00 EEHg/L0.49 3/3/23SM21-23 6200B1Jm+p Xylene
ND 0.50 3/4/23 12:00 EEHg/L0.24 3/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.7 3/4/23 12:0070-130
Toluene-d8 100 3/4/23 12:0070-130
4-Bromofluorobenzene 106 3/4/23 12:0070-130
Page 16 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-06
Field Sample #: Trip Blank
Sample Matrix: Ground Water
Sampled: 3/1/2023 00:00
[TOC_2]23C0255-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
2.8 50 3/4/23 7:26 EEHg/L2.0 3/3/23SM21-23 6200B1JAcetone
ND 0.50 3/4/23 7:26 EEHg/L0.18 3/3/23SM21-23 6200B1Benzene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B1Bromobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.28 3/3/23SM21-23 6200B1Bromochloromethane
ND 0.50 3/4/23 7:26 EEHg/L0.16 3/3/23SM21-23 6200B1Bromodichloromethane
ND 0.50 3/4/23 7:26 EEHg/L0.41 3/3/23SM21-23 6200B1Bromoform
ND 2.0 3/4/23 7:26 EEHg/L1.3 3/3/23SM21-23 6200B1Bromomethane
ND 5.0 3/4/23 7:26 EEHg/L1.7 3/3/23SM21-23 6200B12-Butanone (MEK)
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B1n-Butylbenzene
ND 0.50 3/4/23 7:26 EEHg/L0.13 3/3/23SM21-23 6200B1sec-Butylbenzene
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B1tert-Butylbenzene
ND 0.50 3/4/23 7:26 EEHg/L0.16 3/3/23SM21-23 6200B1Carbon Tetrachloride
ND 0.50 3/4/23 7:26 EEHg/L0.12 3/3/23SM21-23 6200B1Chlorobenzene
ND 50 3/4/23 7:26 EEHg/L20 3/3/23SM21-23 6200B1Ethanol
ND 0.50 3/4/23 7:26 EEHg/L0.20 3/3/23SM21-23 6200B1Chlorodibromomethane
ND 0.50 3/4/23 7:26 EEHg/L0.34 3/3/23SM21-23 6200B1Chloroethane
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B1Chloroform
ND 0.60 3/4/23 7:26 EEHg/L0.50 3/3/23SM21-23 6200B1Chloromethane
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B12-Chlorotoluene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B14-Chlorotoluene
ND 0.50 3/4/23 7:26 EEHg/L0.16 3/3/23SM21-23 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/4/23 7:26 EEHg/L0.13 3/3/23SM21-23 6200B11,2-Dichlorobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B11,3-Dichlorobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.13 3/3/23SM21-23 6200B11,4-Dichlorobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.16 3/3/23SM21-23 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethane
ND 1.0 3/4/23 7:26 EEHg/L0.30 3/3/23SM21-23 6200B11,2-Dichloroethane
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B11,1-Dichloroethylene
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/4/23 7:26 EEHg/L0.17 3/3/23SM21-23 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/4/23 7:26 EEHg/L0.19 3/3/23SM21-23 6200B11,2-Dichloropropane
ND 0.50 3/4/23 7:26 EEHg/L0.12 3/3/23SM21-23 6200B11,3-Dichloropropane
ND 0.50 3/4/23 7:26 EEHg/L0.35 3/3/23SM21-23 6200B1L-042,2-Dichloropropane
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B11,1-Dichloropropene
ND 0.50 3/4/23 7:26 EEHg/L0.16 3/3/23SM21-23 6200B1cis-1,3-Dichloropropene
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B1trans-1,3-Dichloropropene
ND 0.50 3/4/23 7:26 EEHg/L0.20 3/3/23SM21-23 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/4/23 7:26 EEHg/L0.22 3/3/23SM21-23 6200B1Ethylbenzene
ND 5.0 3/4/23 7:26 EEHg/L1.2 3/3/23SM21-23 6200B12-Hexanone (MBK)
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/4/23 7:26 EEHg/L0.13 3/3/23SM21-23 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/4/23 7:26 EEHg/L0.17 3/3/23SM21-23 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/4/23 7:26 EEHg/L0.18 3/3/23SM21-23 6200B1Methylene Chloride
ND 5.0 3/4/23 7:26 EEHg/L1.3 3/3/23SM21-23 6200B14-Methyl-2-pentanone (MIBK)
Page 17 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/2/2023
Work Order: 23C0255Sample Description:Project Location: Rockingham, NC
Sample ID: 23C0255-06
Field Sample #: Trip Blank
Sample Matrix: Ground Water
Sampled: 3/1/2023 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/4/23 7:26 EEHg/L0.38 3/3/23SM21-23 6200B1Naphthalene
ND 0.50 3/4/23 7:26 EEHg/L0.12 3/3/23SM21-23 6200B1n-Propylbenzene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B1Styrene
ND 0.50 3/4/23 7:26 EEHg/L0.14 3/3/23SM21-23 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/4/23 7:26 EEHg/L0.17 3/3/23SM21-23 6200B1Tetrachloroethylene
ND 0.50 3/4/23 7:26 EEHg/L0.22 3/3/23SM21-23 6200B1Toluene
ND 1.0 3/4/23 7:26 EEHg/L0.34 3/3/23SM21-23 6200B11,2,3-Trichlorobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.30 3/3/23SM21-23 6200B11,2,4-Trichlorobenzene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B11,1,1-Trichloroethane
ND 0.50 3/4/23 7:26 EEHg/L0.19 3/3/23SM21-23 6200B11,1,2-Trichloroethane
ND 0.50 3/4/23 7:26 EEHg/L0.17 3/3/23SM21-23 6200B1Trichloroethylene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/4/23 7:26 EEHg/L0.28 3/3/23SM21-23 6200B11,2,3-Trichloropropane
ND 0.50 3/4/23 7:26 EEHg/L0.20 3/3/23SM21-23 6200B11,2,4-Trimethylbenzene
ND 0.50 3/4/23 7:26 EEHg/L0.15 3/3/23SM21-23 6200B11,3,5-Trimethylbenzene
ND 20 3/4/23 7:26 EEHg/L1.7 3/3/23SM21-23 6200B1L-04Vinyl Acetate
ND 0.50 3/4/23 7:26 EEHg/L0.24 3/3/23SM21-23 6200B1Vinyl Chloride
ND 1.0 3/4/23 7:26 EEHg/L0.49 3/3/23SM21-23 6200B1m+p Xylene
ND 0.50 3/4/23 7:26 EEHg/L0.24 3/3/23SM21-23 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.2 3/4/23 7:2670-130
Toluene-d8 102 3/4/23 7:2670-130
4-Bromofluorobenzene 104 3/4/23 7:2670-130
Page 18 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B333130 03/03/230.25 5.0023C0255-01 [MW-1]
B333130 03/03/230.5 5.0023C0255-02 [MW-2]
B333130 03/03/230.5 5.0023C0255-03 [MW-3]
B333130 03/03/235 5.0023C0255-04 [MW-4]
B333130 03/03/235 5.0023C0255-05 [MW-5D]
B333130 03/03/235 5.0023C0255-06 [Trip Blank]
Prep Method: SW-846 5030B-SM21-23 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B333306 03/06/230.025 5.0023C0255-02RE1 [MW-2]
[TOC_1]Sample Preparation Information[TOC]
Page 19 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B333130 - SW-846 5030B
[TOC_3]B333130[TOC]
Blank (B333130-BLK1) Prepared: 03/03/23 Analyzed: 03/04/23
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50 L-04ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 20 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B333130 - SW-846 5030B
Blank (B333130-BLK1) Prepared: 03/03/23 Analyzed: 03/04/23
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 81.920.5
g/L 25.0 70-130Surrogate: Toluene-d8 99.424.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.2
LCS (B333130-BS1) Prepared: 03/03/23 Analyzed: 03/04/23
Acetone g/L50 100 70-13082.082.0
Benzene g/L0.50 10.0 70-13089.88.98
Bromobenzene g/L0.50 10.0 70-13010110.1
Bromochloromethane g/L0.50 10.0 70-13094.59.45
Bromodichloromethane g/L0.50 10.0 70-13097.89.78
Bromoform g/L0.50 10.0 70-13010810.8
Bromomethane g/L2.0 10.0 60-14010210.2
2-Butanone (MEK)g/L5.0 100 70-13091.291.2
n-Butylbenzene g/L0.50 10.0 70-13087.58.75
sec-Butylbenzene g/L0.50 10.0 70-13092.09.20
tert-Butylbenzene g/L0.50 10.0 70-13095.59.55
Carbon Tetrachloride g/L0.50 10.0 70-13095.79.57
Chlorobenzene g/L0.50 10.0 70-13010510.5
Ethanol g/L50 100 70-13086.286.2
Chlorodibromomethane g/L0.50 10.0 70-13010510.5
Chloroethane g/L0.50 10.0 60-14099.49.94
Chloroform g/L0.50 10.0 70-13088.38.83
Chloromethane g/L0.60 10.0 60-14088.58.85
2-Chlorotoluene g/L0.50 10.0 70-13093.39.33
4-Chlorotoluene g/L0.50 10.0 70-13010210.2
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010210.2
1,2-Dichlorobenzene g/L0.50 10.0 70-13098.29.82
1,3-Dichlorobenzene g/L0.50 10.0 70-13095.49.54
1,4-Dichlorobenzene g/L0.50 10.0 70-13092.99.29
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14082.28.22
1,1-Dichloroethane g/L0.50 10.0 70-13088.38.83
1,2-Dichloroethane g/L0.50 10.0 70-13085.58.55
1,1-Dichloroethylene g/L0.50 10.0 70-13093.09.30
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13089.38.93
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13087.78.77
1,2-Dichloropropane g/L0.50 10.0 70-13093.99.39
1,3-Dichloropropane g/L0.50 10.0 70-13096.79.67
2,2-Dichloropropane g/L0.50 10.0 L-0470-13064.7 *6.47
1,1-Dichloropropene g/L0.50 10.0 70-13088.38.83
cis-1,3-Dichloropropene g/L0.50 10.0 70-13091.39.13
trans-1,3-Dichloropropene g/L0.50 10.0 70-13091.39.13
Page 21 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B333130 - SW-846 5030B
LCS (B333130-BS1) Prepared: 03/03/23 Analyzed: 03/04/23
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13090.09.00
Ethylbenzene g/L0.50 10.0 70-13010210.2
2-Hexanone (MBK)g/L5.0 100 70-13091.891.8
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010410.4
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13091.69.16
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13089.18.91
Methylene Chloride g/L5.0 10.0 70-13089.28.92
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13093.693.6
Naphthalene g/L0.50 10.0 70-13087.38.73
n-Propylbenzene g/L0.50 10.0 70-13010210.2
Styrene g/L0.50 10.0 70-13010710.7
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13091.69.16
Tetrachloroethylene g/L0.50 10.0 70-13010410.4
Toluene g/L0.50 10.0 70-13096.69.66
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13092.59.25
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13091.19.11
1,1,1-Trichloroethane g/L0.50 10.0 70-13090.99.09
1,1,2-Trichloroethane g/L0.50 10.0 70-13010210.2
Trichloroethylene g/L0.50 10.0 70-13010010.0
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13097.19.71
1,2,3-Trichloropropane g/L0.50 10.0 70-13098.19.81
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13093.09.30
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010210.2
Vinyl Acetate g/L20 100 L-0470-13055.3 *55.3
Vinyl Chloride g/L0.50 10.0 60-14010510.5
m+p Xylene g/L1.0 20.0 70-13010220.4
o-Xylene g/L0.50 10.0 70-13010310.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 82.620.7
g/L 25.0 70-130Surrogate: Toluene-d8 99.024.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10726.6
LCS Dup (B333130-BSD1) Prepared: 03/03/23 Analyzed: 03/04/23
Acetone g/L50 100 2570-13085.2 3.8385.2
Benzene g/L0.50 10.0 2570-13092.5 2.969.25
Bromobenzene g/L0.50 10.0 2570-130101 0.39610.1
Bromochloromethane g/L0.50 10.0 2570-13095.1 0.6339.51
Bromodichloromethane g/L0.50 10.0 2570-13095.3 2.599.53
Bromoform g/L0.50 10.0 2570-130112 4.0911.2
Bromomethane g/L2.0 10.0 2560-140113 9.6711.3
2-Butanone (MEK)g/L5.0 100 2570-13088.8 2.6488.8
n-Butylbenzene g/L0.50 10.0 2570-13088.4 1.028.84
sec-Butylbenzene g/L0.50 10.0 2570-13094.2 2.369.42
tert-Butylbenzene g/L0.50 10.0 2570-13095.6 0.1059.56
Carbon Tetrachloride g/L0.50 10.0 2570-13098.5 2.889.85
Chlorobenzene g/L0.50 10.0 2570-130108 2.9910.8
Ethanol g/L50 100 2570-130103 17.7103
Chlorodibromomethane g/L0.50 10.0 2570-130106 1.3310.6
Chloroethane g/L0.50 10.0 2560-140102 2.7810.2
Chloroform g/L0.50 10.0 2570-13091.4 3.459.14
Chloromethane g/L0.60 10.0 2560-14088.2 0.3408.82
2-Chlorotoluene g/L0.50 10.0 2570-13094.1 0.8549.41
4-Chlorotoluene g/L0.50 10.0 2570-130101 0.78710.1
Page 22 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B333130 - SW-846 5030B
LCS Dup (B333130-BSD1) Prepared: 03/03/23 Analyzed: 03/04/23
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130106 2.9810.6
1,2-Dichlorobenzene g/L0.50 10.0 2570-13097.9 0.3069.79
1,3-Dichlorobenzene g/L0.50 10.0 2570-13096.8 1.469.68
1,4-Dichlorobenzene g/L0.50 10.0 2570-13094.0 1.189.40
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14094.8 14.29.48
1,1-Dichloroethane g/L0.50 10.0 2570-13093.2 5.409.32
1,2-Dichloroethane g/L0.50 10.0 2570-13089.5 4.578.95
1,1-Dichloroethylene g/L0.50 10.0 2570-13096.8 4.009.68
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13094.3 5.459.43
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13089.2 1.708.92
1,2-Dichloropropane g/L0.50 10.0 2570-13093.3 0.6419.33
1,3-Dichloropropane g/L0.50 10.0 2570-13098.1 1.449.81
2,2-Dichloropropane g/L0.50 10.0 25 L-0470-13065.6 1.38*6.56
1,1-Dichloropropene g/L0.50 10.0 2570-13092.8 4.979.28
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13094.5 3.449.45
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13090.6 0.7709.06
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13093.6 3.929.36
Ethylbenzene g/L0.50 10.0 2570-130104 2.6210.4
2-Hexanone (MBK)g/L5.0 100 2570-13096.7 5.1196.7
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130107 2.3710.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13094.2 2.809.42
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13093.1 4.399.31
Methylene Chloride g/L5.0 10.0 2570-13091.0 2.009.10
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13096.4 3.0096.4
Naphthalene g/L0.50 10.0 2570-13090.8 3.939.08
n-Propylbenzene g/L0.50 10.0 2570-130106 4.5310.6
Styrene g/L0.50 10.0 2570-130112 4.3911.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13094.9 3.549.49
Tetrachloroethylene g/L0.50 10.0 2570-130108 3.6910.8
Toluene g/L0.50 10.0 2570-130101 4.7510.1
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130102 9.2810.2
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13095.1 4.309.51
1,1,1-Trichloroethane g/L0.50 10.0 2570-13095.5 4.949.55
1,1,2-Trichloroethane g/L0.50 10.0 2570-130102 0.29510.2
Trichloroethylene g/L0.50 10.0 2570-130105 4.4710.5
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130105 8.0110.5
1,2,3-Trichloropropane g/L0.50 10.0 2570-130103 5.1610.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13094.0 1.079.40
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130107 4.4910.7
Vinyl Acetate g/L20 100 25 L-0470-13052.0 6.09*52.0
Vinyl Chloride g/L0.50 10.0 2560-140103 2.2110.3
m+p Xylene g/L1.0 20.0 2570-130106 3.7021.2
o-Xylene g/L0.50 10.0 2570-130107 3.8210.7
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 86.221.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.924.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10726.6
Page 23 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B333306 - SW-846 5030B
[TOC_3]B333306[TOC]
Blank (B333306-BLK1) Prepared: 03/06/23 Analyzed: 03/07/23
Toluene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11127.6
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.723.7
LCS (B333306-BS1) Prepared: 03/06/23 Analyzed: 03/07/23
Toluene g/L0.50 10.0 70-13097.99.79
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10827.0
g/L 25.0 70-130Surrogate: Toluene-d8 10325.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.024.5
LCS Dup (B333306-BSD1) Prepared: 03/06/23 Analyzed: 03/07/23
Toluene g/L0.50 10.0 2570-13098.6 0.7129.86
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11228.1
g/L 25.0 70-130Surrogate: Toluene-d8 10125.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.424.4
Page 24 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
Page 25 of 30
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-23 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
652North Carolina Div. of Water QualityNC 12/31/2023
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