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HomeMy WebLinkAboutMO-29269_48436_CA_WSW_20211129_WSW Sample Results for 15103 Cramur DriveCHARLOTTE Laboratory Analysis Report W tj E R Report Date: 11/29/2021 12:01 Environmental Laboratory Services LOCATION: GWO-96858 CHAIN OF CUSTODY #: 211117018 LOC ID: G-PRIV SAMPLE DATE -TIME: 11/17/2021 10:35 SAMPLE DESCRIPTION: Grab Parameter Result Units RL Method Start Date / Time Analyst Sample ID: A109856 A109856 Pesticide/PCB Extraction 3510C LLE 11/18/2021 12:54 SLT A109856 Continuous Liq-Liq Extraction Completed 3520C 11/22/2021 07:54 WMC A109856 1,1,1,2-Tetrachloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1,1-Trichloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1,2,2-Tetrachloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1,2-Trichloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1-Dichloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1-Dichloroethylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,1-Dichloropropene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2,3-Trichlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2,3-Trichloropropane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2,4-Trichlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2,4-Tri methyl benzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2-Dibromo-3-chloropropane (DCP)* < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2-Dibromoethane (EDB)* < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2-Dichloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,2-Dichloropropane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,3,5-Tri methyl benzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 1,3-Dichloropropane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 2,2-Dichloropropane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Benzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Bromobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Bromochloromethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Bromodichloromethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Bromoform < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Bromomethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Carbon Tetrachloride < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Chlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Chlorodibromomethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Chloroethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Chloroform < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Chloromethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Cis-1,2-Dichloroethylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Cis-1,3-Dichloropropene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Dibromomethane < ug/L 0.5 EPA524.2 11/18/2021 12:51 MLL A109856 Dichlorodifluoromethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Dichloromethane (methylene chloride) < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Ethylbenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Fluorotrichloromethane < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Hexachlorobutadiene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 lsopropyl benzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 m&p-Xylene < ug/L 1.0 EPA 524.2 11/18/2021 12:51 MLL A109856 m-Dichlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Methyl-t-butyl ether (MTBE) < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Naphthalene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 n-Butylbenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 n-Propylbenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 o-Chlorotoluene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 o-Dichlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 o-Xylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 p-Chlorotoluene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 p-Dichlorobenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL Page 1 of 4 CHARLOTTE Laboratory Analysis Report Wb,TER Report Date: 11/29/2021 12:01 Environmental Laboratory Services LOCATION: GWO-96858 CHAIN OF CUSTODY #: 211117018 LOC ID: G-PRIV SAMPLE DATE -TIME: 11/17/2021 10:35 SAMPLE DESCRIPTION: Grab Parameter Result Units RL Method Start Date / Time Analyst A109856 p-Isopropyltoluene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Sec -Butyl benzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Styrene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Tert-Butylbenzene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Tetrachloroethylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL AI09856 Toluene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Trans-1,2-Dichloroethylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Trans-1,3-Dichloropropene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MILL A109856 Trichloroethylene < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 Vinyl Chloride < ug/L 0.5 EPA 524.2 11/18/2021 12:51 MLL A109856 4,4'- DDD < ug/L 0.10 SW846 8081B 11/19/2021 12:38 SLT A109856 4,4'- DDE < ug/L 0.10 SW846 8081B 11/19/2021 12:38 SLT A109856 4,4'- DDT < ug/L 0.10 SW846 8081B 11/19/2021 12:38 SLT A109856 Aldrin < ug/L 0.05 SW846 8081 B 11/19/2021 12:38 SLT AI09856 alpha-BHC < ug/L 0.10 SW8468081B 11/19/2021 12:38 SLT A109856 beta-BHC < ug/L 0.10 SW846 8081B 11/19/2021 12:38 SLT A109856 Chlordane (Technical) < 0.40 ug/L 0.40 SW846 8081 B 11/22/2021 13:34 SLT A109856 delta-BHC < ug/L 0.05 SW8468081B 11/19/2021 12:38 SLT A109856 Dieldrin < ug/L 0.10 SW8468081B 11/19/2021 12:38 SLT A109856 Endosuifan I < ug/L 0.05 SW846 8081 B 11/19/2021 12:38 SLT A109856 Endosuifan II < ug/L 0.10 SW846 8081 B 11/19/2021 12:38 SLT A109856 Endosuifan sulfate < ug/L 0.10 SW846 8081 B 11/19/2021 12:38 SLT A109856 Endrin < ug/L 0.10 SW846 8081 B 11/19/2021 12:38 SLT A109856 Endrin aldehyde < ug/L 0.10 SW846 8081 B 11/19/2021 12:38 SLT A109856 gamma-BHC (Lindane) < ug/L 0.05 SW846 8081 B 11/19/2021 12:38 SLT A109856 Heptachlor < ug/L 0.05 SW8468081B 11/19/2021 12:38 SLT A109856 Heptachlor epoxide < ug/L 0.10 SW846 8081B 11/19/2021 12:38 SLT A109856 Methoxychlor < ug/L 0.10 SW846 8081 B 11/19/2021 12:38 SLT A109856 Toxaphene < 1.0 ug/L 1.0 SW846 8081 B 11/19/2021 12:34 SLT A109856 1,2,4,5 Tetrachlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 1,2,4-Trichlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 1,2-Dichlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109866 1,3-Dichlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 1,4-Dichlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 1-Chloronaphthalene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,3,4,6-Tetrachlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,3-Dichloraniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4,5-Trichlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4,6-Trichlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4-Dichlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4-Dimethylphenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4-Dinitrophenol < ug/L 20 SW846 8270E 11/22/2021 17:03 WMC A109856 2,4-Dinitrotoluene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,6-Dichlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2,6-Dinitrotoluene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Chloronaphthalene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Chlorophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Methyl naphthalene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Methylphenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Nitroaniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 2-Nitrophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 3,3'-Dichlorobenzidine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 3-Nitroaniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC Page 2 of 4 CHARLOTTE Laboratory Analysis Report W6TER Report Date: 11/29/2021 12:01 Environmental Laboratory Services LOCATION: GWO-96858 CHAIN OF CUSTODY #: 211117018 LOC ID: G-PRIV SAMPLE DATE -TIME: 11/17/2021 10:35 SAMPLE DESCRIPTION: Grab Parameter Result Units RL Method Start Date / Time Analyst A109856 4,6-Dinitro-2-methylphenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Bromophenyl-phenylether < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Chloro-3-methylphenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Chloroaniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Chlorophenyl-phenylether < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Methylphenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Nitroaniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 4-Nitrophenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Acenaphthene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Acenaphthylene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Acetophenone < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Alpha-Terpineol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Aniline < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Anthracene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzidine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzo [g,h,i] perylene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzo(a) anthracene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzo[a]pyrene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzo[b]fluoranthene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzo[k]fluoranthene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzoic acid < ug/L 25 SW846 8270E 11/22/2021 17:03 WMC A109856 Benzyl alcohol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 bis(2-Chloroethoxy)methane < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Bis(2-chloroethyl) ether < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 bis(2-chloroisopropyl) ether < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 bis(2-Ethylhexyl)phthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Butylbenzylphthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Carbazole < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Chrysene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Dibenz[a,h]anthracene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Dibenzofuran < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Diethylphthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Dimethylphthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Di-n-butylphthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Di-n-octylphthalate < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Diphenylhydrazine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Fluoranthene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Fluorene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Hexachlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Hexachlorobutadiene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Hexachlorocyclopentadiene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Hexachloroethane < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 lndeno[1,2,3-cd]pyrene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC AI09856 lsophorone < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC AI09856 Napthalene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 n-Decane < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Nitrobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 N-Nitrosodimethylamine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 n-Nitroso-di-n-propylamine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 N-Nitrosodiphenylamine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 n-Octadecane < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Pentachlorobenzene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Pentachlorophenol < ug/L 10 SW846 8270E 11/22/2021 17:03 WMC Page 3 of 4 CHARLOTTE Laboratory Analysis Report WtReport Date: 11/29/2021 12:01 jTER Environmental Laboratory Services LOCATION: GWO-96858 CHAIN OF CUSTODY #: 211117018 LOC ID: G-PRIV SAMPLE DATE -TIME: 11/17/2021 10:35 SAMPLE DESCRIPTION: Grab Parameter Result Units RL Method Start Date / Time Analyst A109856 Phenanthrene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Phenol < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Pyrene < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Pyridine < ug/L 5 SW846 8270E 11/22/2021 17:03 WMC A109856 Nitrate 1.2 mg/L 0.05 EPA353.2-93 11/18/2021 14:16 MSC A109856 Nitrate/Nitrite 1.2 mg/L 0.05 EPA353.2-93 11/18/2021 14:16 MSC A109856 Nitrite <0.05 mg/L 0.05 EPA353.2-93 11/18/2021 13:22 MSC A109856 E. Coli-PA Absent P/A SM 9223B 11/17/2021 15:21 KAH A109856 Total Coliform- P/A Absent P/A SM 9223B 11/17/2021 15:21 KAH Comment: 524: EPA 524.2 is not an approved method for 1,2-dibromo-3-chloropropane (DBCP) and 1,2-dibromoethane (EDB). Gina H. Kimble, Laboratory Supervisor: .'° `" The results contained in this report are specific to the samples listed above. CHARLOTTE WATER -Environmental Laboratory Services 4222 Westmont Drive, Charlotte, North Carolina 28217 N.C. Certification 192, N.C.DHHS Certification 37417, EPA Cert 01215 Page 4 of 4 CHARLOTTE-MECKLENBURG UTILITY DEPARTMENT ENVIRONMENTAL LABORATORY SERVICES CHAIN OF CUSTODY RECORD 4222 Westmont Drive, Charlotte, NC 28217 (704) 336 - 2854 or (704) 622 - 7280 CHARIDTTE- COC #; CHAR 0 KLEHsUA� NC DENR Certification No.192; NC DHHS Certification No. 37417; US EPA Certification No. 01215 CHA8 OU E-MECKL'ENZURG z�1117 / ! PAGE 1 OF 1 LITY UTIDECAR—EN 0L CLIENT: Mecklenburg County, LUESA- Groundwater & Wastewater Services Send REPORT To: Send INVOICE To: Sa Ied By (Print Na FACILITY: Groundwater (POTABLE WATER) Heather Ray Jeremy Michael -iT / C{ ADDRESS: 15915 Cramur Or 3205 Freedom Drive, Suite 8000 3205 Freedom Drive, Suite 8000 W tnessed By (Print & Sign Nam - If Applicable): LAB CODE: REAL PRIG NEW TNC MPL PME AMB LM OTHER Charlotte, NC 28208 Charlotte, NC 28208 (circle one) IN Sample Collection logo mm�IN�NI� Chemical Preservative 04= =,E:m ME I ME NEON III IIIIIIE a, 'at ME OMNI�'eom�r�� IN =ii��i1�IIIJIini;lEMEMEN III Instructions: Complete all yellow shaded areas. Blue areas are for LAB USE ONLY. Relinq ' h y: (Sig re) Receiv by: (Signature) Date: Military Time: For each parameter requested, circle the "x" to verify your request. l 17 f L3a Relinquished by: (Signature) R ceived by: (Signature) Date: MilitaryTime: Nutrients include: Nitrate/Nitrite, TKN, Total Phosphours, Ammonia Itemize Metals Here: Relinquished by: (Signature) Received by: (Signature) Date: Military Time: For Composite samples, record the autosampler BEGIN and END date/time. For Grab samples, record the collection time as the BEGIN date/time only. Relinquished by: (Signature) Received by: (Signature) Date: Military Time: Comments: —3-DAY TAT REQUESTED— Form Revision U8; Ettective April 1, 202 LaD GooeS: KCAL = Neal tSiaie; i-Kiv = t'nvate Well; INtvv = riew t-ermlttea vven; i Ivl = i ransient ivon-UOmmunity; AlvlC7 = AmDlerlt; uvl = L"dna00 CHARLOTTE WATER - Environmental Laboratory Services Sample Receipt Checklist Completed by Initials: Date/Time: &J J-I / / 5c/ COC#: 21111701 Sample Matrix: Wastewater ElDrinking Water DCryptolGiardia (LT2) Other: Field Analysis/Information Only (No cooler) CustodySeal(s) Intact?: Yes E]No F_-_JN/A Type of Ice Used: Wet Blue Shipping Container Intact: Yes E]No [§N/A Dry Ice ONone Thermal Preservation: *Sample Temperature measured immediately after removal from cooler. *Notify management immediately of any sample that did not meet temperature requirements or frozen. *If multiple parameters, in additional to BacT are collected for a site, a receipt temperature for the BacT plus another bottle must be measured and recorded on the COC. Requirements: DW: <_ WC WW: <_ WC BacT: <_ 10°C LT2 Crypto/Giardia: <_ 20°C LT2 E. coli: <_ 10°C Do sample receipt temperatures meet requirements (including requirement by downward trend)? EYes []No, explain below. Downward trend required to meet requirement? DYes * At time of receipt into the laboratory, the allowed downward trend may be applied to meet temperature requirement. Initial temperature from the sample collector becomes critical. If samples are received next day, receipt temperatures must meet requirements listed above. Chemical Preservation: Note: *If samples are not preserved correctly, notify Personnel. Do not check BacT, TOC, VOA, THM and HAA. All containers needing preservation are found to be in EPA compliance? F�]`l'es E]No F]N/A If no, explain. *If the pH of a metals(excluding H is incorrect these steps are followed: *If the pH of any other chemically preserved sample is incorrect 1. On COC, document sample pH prior to adding additional preservative. (not including metals), follow these steps: 2. Document "pH NOT MET" on container. 1. Notify immediately of sample incorrectly preserved. Qualify Date/time of preservation will be captured on the lid, when additional sample not properly preserved on the COC and in LIMS. HNO3 Acid is added to achieve pH < 2. No comment in LIMS required. Option: Substitute a correctly preserved bottle. Document on COC & notify personnel. Write "DO NOT USE" on the incorrectly preserved bottle. No comment in LIMS requires when a sample with correct preservative is substituted. COC Properly Filled Out? ®Yes E]No If no, explain. COC Correction sent to Project Manager? Yes RNo ®N/A Do sample labels agree with the COC? ®Yes E]No If no, explain. All sample bottles accounted for? ®Yes No Samples Arrived within Hold Time? P-4l'es RNo, & notify Project Mgr. Correct Bottles Used? MYes E]No VOA Vials have Zero Headspace (< 6 mm)? ❑Yes RNo DN/A *Bubbles should be no larger than: If no, notify Laboratory Section Supervisor. Short Hold Analyses (< 48 hrs.)? D (es No Rush Turn Around Time (TAT)? Yes — If yes, notify Laboratory Section(s). If yes, notify Project Manager Addition Information Comments: Preliminary COC Review (Optional): Initials: Date: REC-100_FORM_Sample_Rec_Checldist EFF030521 This printed copy is an UNCONTROLLED copy of the online CONTROLLED document.