MO-28738_47974_CA_IAR_20211115_Initial Abatement Report

Initial Abatement Action Report Appendix A
Report Formats
Initial Abatement Action Report
In addition to reporting initial response and abatement actions and assessment actions and presenting initial site
characterization, this newly -created Initial Abatement Action Report must fulfill the requirements, when a release
has been discovered, for the following individual reports:
❑ Site Check Report (Section C)
❑ UST Closure Report (UST-12) with UST-2 Form (Section D)
❑ Post -Excavation Soil Contamination Assessment Report (Section H)
❑ Product Recovery Report (Section E)
Check the applicable report(s). Complete Sections A-L, as required, including the sections specifically designated
for the reports you have indicated. The Initial Abatement Action Report must be submitted to the appropriate
regional office within 90 days following discovery of release.
A. Site Information
1. Site Identification
©Date of Report: November 15, 2021
'Facility I.D.: Not Applicable UST Incident Number (if known): 47974
Site Name: Revocable Trust of Sharon Saville Parker Property
©Site Street Address: 6342 Deveron Drive
li'City/Town: Charlotte Zip Code: 28211-4612 County: Mecklenburg
©Description of Geographical Data Point (e.g., diesel fill port): Former UST location
Location Method (GPS, topographical map, other): GPS
'Latitude (decimal degrees): 35.161163 Longitude (decimal degrees):-80.772062
2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city,
state, zip code and mailing address, if different).
BUST Owner: Revocable Trust of Sharon Saville Parker
Address: c/o Jessica Parker, 212 W. Friendly Ave., Greensboro, NC 27401 Tel.:
®UST Operator: Unknown
Address: Tel:
©Property Owner: Carol T. Miller
Address: 6342 Deveron Drive, Charlotte, NC 28211 Tel.: [phone]
L='Property Occupant: Carol T. Miller
Address: 6342 Deveron Drive, Charlotte, NC 28211 Tel.: [phone]
1---'Consultant/Contractor: Harmon Environmental, PA
Address: 615 Bruce Thomas Road, Monroe, NC 28112 Tel: [phone]
Analytical Laboratory: Pace Analytical Services, LLC State Certification No.: 375
Address: 9800 Kincey Ave., Suite 100, Huntersville, NC 28078 Tel: [phone]
3. Information about Release
�--'Date Discovered: July 21, 2021
''Estimated Quantity of Release: Unknown
'Cause of Release: Holes and aittina in the tank
©Source of Release (Dispenser/Piping/UST): UST-1
-Sizes and contents of UST system(s) from which the release occurred): 550-gallon heating oil tank
4. Certification (The title page must display the seal and signature of the certifying P.E. or L.G. and the
name and certification number of the company or corporation, if applicable (See 1 SA NCAC 2L
.0103(e)].)
I, Richard L. Harmon, a Professional Engine /Licensed Geologist (c cle one) for (firm or company of employment), do
certify that the information contained in this repo ,jo the best of my knowledge.
3.
(Please Affix Seal and Signature)
Harmon Environmental, PA (Name of company or ccrpot*ationjI AA Censea.jo pia 'ce geolog ngineering (circle
one or both) in North Carolina The certification nuniqiothe c9mnany or rorporati C-323
<�: U1� e✓1 .
Initial Abatement Report ��`:Y Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property "- 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
B. Site History and Characterization
1. Provide UST owner and operator information.
ree List the names, addresses, telephone numbers, and dates of ownership/operation of all previous UST
owners and operators of the UST system(s). Present in table form (Use Reporting Table B-2, Site
History, UST Owner/Operator Information, from the Guidelines, Appendix B.).
See attached Table B-2.
2. Provide UST information (inclusive of all USTs, currently and historically in place at facility). For each
UST, provide the following information in table form (Use Reporting Table 13-1, Site History, UST/AST
System Information, from the Guidelines, Appendix B.):
o Tank identification number (keyed to a site map showing the locations of all UST systems);
© Last contents of tank;
© Previous contents of tank (if any);
© Capacity of tank in gallons;
© Construction (material and structure);
o Tank dimensions;
© Installation date;
Description of piping and pump(s) associated with each UST;
Status of UST (in use or not in use, closed in place, closed by removal; date of last use, date of
closure); and
© Indication that a release was or was not associated with the tank or associated piping or pump(s).
Provide discussion to supplement Table 13-1 and the UST location map in order to clarify the spatial and
historical relationships among tanks and between tanks and piping and dispensers. Provide information
about any historical compliance issues.
See attached Table B-1. Harmon Environmental, PA and DeBruhl Environmental Excavating.
Inc. were contracted to remove a 550-gallon residential heating oil tank (UST-1) and excavate
petroleum -impacted soil. The Initial Abatement activities were conducted on October 25 and
October 26. 2021. Incident Number 47974 has been assigned to this site.
3. Provide non -UST information.
List, describe, and indicate location of ASTs and associated piping and pump(s) currently and
historically in place at facility) and describe historical releases. For each AST, present the information
in table form (Use Reporting Table B-1, Site History, UST/AST System Information, from the
Guidelines, Appendix B.); and
List, describe, and indicate location and date of spills which have occurred at facility.
See attached Table B-1. This table summarizes the Incidences at this site prior to October 25,
2021. With the exception of UST-1, no releases have been documented at this site.
4. Provide a comprehensive description of the release, including date discovered, cause and source (including
tank identification number and contents), and the relationship of historical UST releases, non -UST releases,
and off -site releases (indicate incident number) to contamination from current release.
Incident Number 47974 has been assigned to the release associated with UST -I. This release was
discovered on July 21, 2021 by Cedar Rock Environmental PC. This UST was reportedly closed
in place with Plowable concrete material. The site was subsequently closed with a Notice of
Residual Petroleum. After acquiring the proper on September 27, 2021, the Millers requested
Harmon Environmental. PA and DeBruhl Environmental Excavating. Inc. remove the UST.
excavated the petroleum -impacted soil, and request the North Carolina Department of
Environmental, Quality remove the Notice of Residual Petroleum from the property.
5. Provide a brief description of site characteristics (including status of facility (active or inactive), land use of
site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface
cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
Initial Abatement Report 2 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
The site is located in an established residential community in Charlotte. North Carolina. The
topography of this site slopes toward the southeast draining toward an unnamed tributya of
McAlpine Creek. The vegetation on site consists primarily of grass and ornamental shrubber.
Based on the Soil Survey of Mecklenburg County published by the United States Department of
Agriculture. Natural Resources Conservation Service (USDA NRCS) in 2019, the soil type
associated with this region of Mecklenburg County as the Cecil -Urban land (CuB). The depth to
bedrock. the depth to groundwater and the groundwater flow direction at the site have not been
determined.
6. Summarize initial abatement actions, assessment activities, and corrective actions performed to date and list
all reports previously submitted.
DeBruhl Environmental Excavating, Inc. under the oversight of Harmon Environmental. PA
personnel, excavated approximately 39.32 tons of petroleum -impacted soil from the site. This soil
was transported to the Environmental Soil. Inc. permitted land application site in Lattimore.
North Carolina for ppropriate disposal.
C. Site Check Report (if applicable)
Incorporate the minimum requirements of a Site Check Report, as outlined in the Guidelines, Appendix A, p.
43, if a site check revealed a release and initiated the initial response and abatement action.
l . Present and summarize the results of tank and line tightness testing (Refer to Section L, Appendix A,
Tightness testing results and supporting documentation). If theses tightness testing results did not indicate
a release, and if, instead, environmental contamination was the basis for suspecting a release, describe the
environmental contamination.
2. Describe the site check procedure. (For guidance refer to the Guidelines, Section 4.3, Site Check
Requirements). Reference site and sample location maps provided in Section J, Figures, and summaries of
soil and groundwater analytical results provided in Section K, Tables. Explain how the selection of sample
types and locations was influenced by the nature of the stored substance, the type of initial alarm or cause
for suspicion, the type of backfiil, the depth to groundwater, and other factors appropriate for identifying
the presence and source of a release. Describe the condition of the UST system (i.e., pitting, holes, etc.)
where it can be observed.
3. If a release is determined, document initial response actions (submittal of 24-Hour Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions;
4. Document any soil excavation activities in Section H, Excavation of Contaminated Soil.
5. Document site investigation.
Describe field screening, including:
© Physical characteristics of the soil samples, as observed during collection;
© Field instrumentation used to screen soils;
© Field instrument calibration procedures; and
Screening results (Refer to table provided in Section K.).
Document soil sampling information (Refer to figures, tables, and appendices provided in Sections J,
K, and L.), including:
Lithological descriptions from logs for borings, excavations;
Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
Sample collection procedures (grab, split spoon, hand auger, etc.);
w Location of soil samples;
© Depth of soil samples ( feet below land surface);
o Time/date collected;
o Sample identification; and
© Method(s) of soil sample analysis.
® Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
o Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
© Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
r-j Sample collection procedures (grab, bailer, etc.);
Initial Abatement Report 3 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Time/date collected.
© Sample identification; and
Method(s) of water sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
o Decontamination procedures;
© Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
® Describe soil and groundwater investigation results, including:
o Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K. and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
6. Present conclusions and recommendations, referencing maps and cross -sections in Section J, as follows:
® Describe source and estimated extent of soil contamination (If there are multiple sources of release,
then describe the extent of contamination from each source);
o Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
o Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
® Describe source(s) and estimated extent of any groundwater or surface water contamination;
o Describe source(s) and estimated thickness and extent of any free product;
o Indicate what initial response and abatement actions are required; and
Discuss the need for further investigation or remediation.
This section is not applicable. UST-1 was a non-commercial, non -regulated heating oil tank.
D. UST Closure Report following UST-12 Format) and Site Investigation Report for Permanent Closure or
Change -in -Service of UST (UST-2 Form) (if applicable).
Incorporate the minimum requirements of a UST Closure Report, as outlined in Appendix A, p.55, and
complete the UST-2 Form, found in Appendix A, p. 60 of the Guidelines), if UST closure indicated a release
and initiated the initial response and abatement action.
1. Describe preparations for closure including steps taken to notify authorities, permits obtained, and steps
taken to clean and purge the tanks.
2. Describe the closure procedure (For guidance, refer to the Guidelines, Section 5.), referencing site and
sampling location maps and cross -sections presented in Section J of this report. Clearly state how the
selection of sample types and locations was influenced by the nature of the stored substance, the type of
initial alarm or cause for suspicion, the type of backfill, the depth to groundwater, and other factors
appropriate for identifying the presence and source of a release. If presence of groundwater or bedrock
require the installation and sampling of monitoring well(s), describe the process.
3. Note the amount of residual material pumped from the tank and describe the storage, sampling and disposal
of the residual material and the disposal of the tank, pumps and piping (Refer to appendices with disposal
manifests and certificate of tank disposal in Section L.).
4. If a release is determined, document initial response actions (submittal of 24-Hour Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions.
5. Document any soil excavation activities in Section H, Excavation of Contaminated Soil.
6. Document site investigation.
Describe field screening, including:
Physical characteristics of the soil samples, as observed during collection;
Initial Abatement Report 4 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Field instrumentation used to screen soils;
Field instrument calibration procedures; and
Screening results (Refer to table provided in Section J.).
Document soil sampling information (Refer to figures, tables, and appendices provided in Sections J,
K and L.), including:
© Lithological descriptions from logs for borings, excavations;
© Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
o Sample collection procedures (grab, split spoon, hand auger, etc.);
o Location of soil samples;
© Depth of soil samples (feet below land surface);
o Time/date collected;
© Sample identification; and
o Method(s) of soil sample analysis.
Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
o Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
© Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
o Sample collection procedures (grab, bailer, etc.);
© Time/date collected.
o Sample identification; and
© Method(s) of water sample analysis.
© Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L, including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
Decontamination procedures;
o Time and date samples were submitted to lab; and
o Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil and groundwater investigation results, including:
Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
® Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
7. Present conclusions and recommendations, referencing maps and cross -sections in Section J as follows:
Describe source and estimated extent of soil contamination, referencing maps and cross -sections in
Section J (If there are multiple sources of release, then describe the extent of contamination from each
source.);
Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
a Describe source(s) and estimated extent of any groundwater or surface water contamination;
Describe source(s) and estimated thickness and extent of any free product;
Indicate what initial response and abatement actions are required; and
Discuss the need for further investigation or remediation.
This section is not applicable. UST-1 was a non-commercial, non -regulated heating oil tank.
E. Free Product Investigation and Recovery Report (if applicable)
Discuss the status of free product at the site, as follows:
1. If free product is, or has been, present at the site, describe its current and historical status (product distribution,
thickness, recovery activities). Refer to tables in Section K: Table B-7, Monitoring and Remediation Well
Construction Information; and Table B-8A, Free Product Recovery Information; Table B-813, Cumulative Volume
Initial Abatement Report 5 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
of Free Product Recovered from Site; and Table B-9, Current and Historical Groundwater Elevations and Free
Product Thickness. Also refer to map(s) showing extent of free product in Section J;
2. Identify any on -site or off -site effluent discharges, treatment used, effluent quality, permitting actions taken, and
location of such discharges and identify the disposition of recovered free product (refer to attached product
disposal manifests);
3. Document the performance, total cost, and cost per gallon to date of each method of free product recovery used at
site. Justify why the technology is or was used; and
4. Provide conclusions and recommendations concerning historical, current, and future recovery activities, including:
tFO Any proposal to change the current method of free product recovery to a better or more cost-effective
technology;
A justification for continued product recovery, if planned; and
Any determination that free product has been eliminated from the site with a recommendation to reclassify
the risk posed by the release, if applicable.
This section is not applicable. No free product was observed during the initial abatement process.
F. Groundwater and Surface Water Investigation (if applicable)
1. If groundwater or bedrock was encountered in pits, trenches or shallow boring during site check, UST
system closure, or initial abatement investigation, if monitoring or water supply wells were found to be
contaminated, or if surface water is present nearby, then indicate actions taken to investigate suspected
contamination from a release (e.g., installation of monitoring wells, groundwater or surface sampling and
analysis).
2. Document groundwater investigation (or, if applicable, refer to groundwater investigations under Section
C, Site Check Report, or Section D, UST Closure Report), as follows:
5nl Present groundwater and surface water sampling information (Refer to tables and appendices provided
in Sections K and L.), including:
© Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
o Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
© Sample collection procedures (grab, bailer, etc.);
Time/date collected.
© Sample identification; and
© Method(s) of water sample analysis.
© Document quality -control measure information (Refer to tables and appendices provided in Sections K
and L), including:
© Sample handling procedures including sample preservation techniques and sample transport
procedures;
o Decontamination procedures;
o Time and date samples were submitted to lab; and
© Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
© Describe groundwater or surface water investigation results, including:
© Presentation of analytical results (Refer to table(s) provided in Section K and to appendix with
laboratory analytical results provided in Section L.) and discussion of the results in relation to the
cleanup levels (groundwater quality or surface water quality standards); and
o Discussion of the effect of quality control sample results on the interpretation of groundwater or
surface water analytical results.
This section is not applicable. Groundwater was not encountered during the initial abatement
process.
G. Initial Response and Abatement Action
1. Describe initial response actions performed within 24 hours of discovery of the release, including:
n Submittal of 24-Hour Release Report and UST Leak Reporting Form (UST-61);
Action to prevent further release and to determine source of the release;
Identification and mitigation of hazards due to exposure to pollutants (e.g. Responsible party must
identify and sample water supply wells at risk of impact by the release and provide supply of alternate
water, if wells are impacted.); and
Initial Abatement Report 6 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
G: Identification and mitigation of hazards due to fire, explosion, and vapor hazards.
DeBruhl Environmental Excavatioe. Inc. under the oversight of Harmon Environmental. PA
personnel, excavated approximately 39.32 tons of petroleum -impacted soil from the site. This soil
was transported to the Environmental Soil, Inc. permitted land application site for appropriate
disposal. Pollution hazards associated with former UST-1 were mitigated by removing the
petroleum -impacted soil associated with the former UST.
Describe initial abatement actions performed, including:
© Completion of investigation to confirm presence and determine source of the release;
© Investigation and recovery of free product;
® Continued mitigation and monitoring of fire, explosion, and vapor hazards;
o Remediation of hazards posed by exposed contaminated soil;
® Submittal of 20-Day Report summarizing the progress of the initial actions performed within the 20-
day period following discovery of the release; and
r� Soil excavation activities (Document in Section H, Excavation of Contaminated soil.).
DeBruhl Environmental Excavating, Inc. under the oversight of Harmon Environmental. PA
personnel excavated approximately 39.32 tons of petroleum -impacted soil from the site. This soil
was transported to the Environmental Soil. Inc. permitted land application site in Lattimore.
North Carolina for appropriate disposal.
H. Excavation of Contaminated Soil
1. Describe source and estimated extent of soil contamination determined in initial investigations (e.g., site
check, UST system closure), referencing maps and cross -sections in Section J and tables presenting soil
sampling information and results in Section K (If there are multiple sources of release, then describe the
extent of contamination from each source.), including:
Sampling location and depths; locations of tanks, piping dispensers, sumps, areas of staining (indicate
if above or below tank); utility lines; potential receptors; buildings; relationship of area(s) of
contaminated soil to groundwater and bedrock; and
If part or all of UST system was removed, indicate dimensions of resulting pits and trenches.
This section is not applicable. UST -I was a non-commercial, non -regulated heating oil tank.
Describe excavation process, referencing maps and cross -sections in Section J, tables presenting soil
sampling information and results in section K and disposal manifests and geological logs in Section J, as
follows:
o Describe type of equipment used (e.g., back hoe, track hoe, dump truck);
© Describe field screening, if used to determine limits of excavation, including:
o Physical characteristics of the soil samples, as observed during collection;
© Field instrumentation used to screen soils;
o Field instrument calibration procedures;
© Screening results (Refer to table provided in Section K.);
® Indicate the final dimensions of the excavation(s);
© Indicate the volume (in cubic yards) and weight (in tons) of soil excavated from each excavation (show
calculations);
Describe relationship of final excavation pit to former UST system, to groundwater, to bedrock, and to
structures; and
© Indicate if the excavation operation ceased on encountering clean soil, groundwater, or bedrock OR if
excavation ceased 5 feet from tank(s), dispenser(s), and/or piping and at a depth of 17 feet below land
surface.
The Detroleum-impacted soil was excavated using a Caterpillar® 426B backho_e operated by Mr.
Randy DeBruhl of DeBruhl Environmental Excavating. Inc. and loaded directly into Mack
Granite® quad -axle dump trucks for transport to the Environmental Soils. Inc. permitted land
application site in Lattimore. North Carolina for appropriate disposal. The final dimensions of
the UST excavation measured approximately 14 eet long by approximately 9 feet wide and up to
Initial Abatement Report 7 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
14 feet deep. The excavation was terminated when field screening results indicated clean soil was
encountered. The total volume of petroleum -impacted soil removed in conjunction with this Initial
Abatement proiect was approximately 39.32 tons. Based on the Soil Survey of Mecklenburg
County published by the USDA NRCS in 2014, the soil We associated with this region of
Mecklenburg County is the Cecil -Urban land (CuB). The depth to bedrock the depth to
groundwater and the groundwater flow direction at the site have not been determined.
Describe post -excavation confirmation soil sampling , referencing maps and cross -sections in Section J,
tables presenting soil sampling information and results in Section K, and geological logs in Section L as
follows:
5-1 Describe sample location and depth, and methods of collection and analysis for each excavation;
© Note if multiple excavations were performed sequentially in an area of contaminated soil„ i.e., if
confirmatory sampling following primary excavation indicated that contaminated soil remained, so that
further excavation was performed and a second set of confirmatory samples was collected and
analyzed; and
If contaminated soil was allowed to remain after final excavation, indicate precisely the location and
depth of the residual contamination and explain why it was not removed, i.e., why it was not
economically and/or technologically feasible to excavate it
Document Soil Investigation.
Provide soil sampling information for all samples collected following excavation and during previous
investigations. Refer to table provided in Section K: Table B-3, Summary of Soil Sampling Results; to
figures, in Section J; and to appendices, in Section L. Information should include
o Lithological descriptions from logs for borings, excavations;
© Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
© Sample collection procedures (grab, split spoon, hand auger, etc.);
© Location of soil samples;
© Depth of soil samples (feet below land surface);
o Time/date collected;
Sample identification;
r� Indication of phase of sampling: site check; closure, IAA, etc.; and
o Method(s) of soil sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
® Decontamination procedures;
© Time and date samples were submitted to lab; and
® Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
© Describe soil investigation results, including:
o Presentation of analytical results for soil samples (Refer to table provided in Section K and to appendix
with laboratory analytical results provided in Section L.);
© Discussion of the results in relation to the appropriate cleanup levels, identifying the samples that
exceed the lower of:
(a) the residential MSCCs or
(b) the soil -to -groundwater MSCCs.
Discussion of effect of quality control sample results on the interpretation of soil analytical results.
On October 26, 2021, DeBruhl Environmental Excavating, Inc. removed approximately 39.32 tons
of petroleum -impacted soil associated with a former 550-gallon heating oil UST. In conjunction
with the excavation activities, one confirmatory soil sample BOTI (6) was collected from
immediately beneath the UST and five confirmatory soil samples BOT204). SW(9), EW(11),
NW() and WW(8) were collected by Harmon Environmental. PA personnel, from the base and
side walls of the excavation at the locations depicted on Figure 3. Soil sample BOT204) was
collected from the base of the excavation at a depth of approximately 14 feet below grade. Soil
sample SW(9) was collected from the south wall of the excavation at a depth of approximately 9
feet below grade. Soil sample EWO1) was collected from the east wall of the excavation at a
depth of pproximately 11 feet below grade. Soil sample NW(9) was collected from the north wall
Initial Abatement Report 8 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
of the excavation at a depth of approximately 9 feet below grade and soil sample WW(8) was
collected from the west wall of the excavation at a depth of pproximately 8feel below grade.
These six soil samples were analyzed by Pace Analytical Services. LLC of Huntersville, North
Carolina for analysis. Soil sample BOTI j6) was analyzed for gasoline range organic compounds
(GRO) and diesel range organic compounds (DRO) in accordance with SW-846 Method 801 SC
Soil samples BOT204). SW(9), EW(11), NW(9) and WW(8) were analyzed for volatile organic
compounds (VOCs) by SW-846 Method 8260D: semi -volatile organic compounds (Semi-VOCs) in
accordance with SW-846 Method 8270E BN/A and, volatile petroleum hydrocarbon (VPH1
compounds and extractable petroleum hydrocarbon (EPH) compounds by Massachusetts
Methods. A copy of the laboratory report is presented in Appendix J and a copy of the Chain -off
Custody Record is included in Appendix I. As indicated by these results. no targeted compounds
were detected in the BOT2(14), SW(9), EW(11), NW(9) and SWO samples at concentrations
exceeding the respective analytical method detection limits.
5. Describe disposal of contaminated soil, referencing tables presenting soil sampling information and results
in Section K and disposal manifests in Section L as follows:
Y__, Indicate volume and weight of contaminated soil removed from each excavation at site;
r-i Describe construction of any stockpile of contaminated soil, describe collection and analysis of
stockpile samples;
Indicate if soil was treated onsite (Reference permit in Section L.);
Indicate if soil was transported offsite for disposal and, if so, by whom and to what destination; and
r Confirm that excavation was back -filled with clean soil.
On October 26, 2021, approximately 39.32 tons of petroleum -impacted soil was excavated from
the vicinity of a former 550-gallon UST basin at the site. As excavated, the impacted soil was
loaded directly into dump trucks and transported to the Environmental Soils. Inc. permitted land
application site in Lattimore, North Carolina for appropriate disposal. A copy of the manifest is
presented in Appendix H. The excavation was backfilled with clean soil from a local quarry.
6. Present conclusions, as follows;
® Briefly summarize excavation process;
© Describe extent of final excavation(s) and collection of confirmatory samples;
o Indicate if excavation ceased on encountering groundwater or bedrock; and
E, Indicate whether soil contaminant levels in exceedance of the lowest MSCCs remain in the
excavation(s), further excavation being determined infeasible by the UST Section, or soil contaminant
levels in final excavation confirmatory soil samples were equal to below the lowest MSCCs
1. Conclusions
1. If soil contaminant levels in exceedance of the lowest MSCCs remain in the excavation(s) (further
excavation being determined infeasible by the UST Section), if groundwater or bedrock has been
encountered in proximity to contamination, or if free product is present, it should be concluded that a
Limited Site Assessment must be performed and a report submitted within 120 days of discovery of the
release; but
2. If soil contaminant levels in final excavation confirmatory soil samples were equal to or below the lowest
MSCCs and if groundwater, bedrock, and free product were not encountered in the excavation(s), then no
further action should be requested.
On October 26. 2021. DeBruhl Environmental Excavating. Inc. removed approximately 39.32 tons
of petroleum -impacted soil associated with a former 550-gallon heating oil UST. In conjunction
with the excavation activities, one confirmatory soil sample BOTI (6) was collected from
immediately beneath the UST and five confirmatory soil samples BOT2(14). SW(9). EW01),
NW(9) and WW(8) were collected by Harmon Environmental, PA personnel, from the base and
side walls of the excavation at the locations depicted on Figure 3. Soil sample BOT2(14) was
collected from the base of the excavation at a depth of approximately 14 feet below grade. Soil
sample SW(9) was collected from the south wall of the excavation at a depth of approximately 9
feet below grade. Soil sample EW(11) was collected from the east wall of the excavation at a
nth of approximately 11 feet below grade. Soil sample NW(9) was collected from the north wall
of the excavation at a depth of pproximately 9 feet below grade and soil sample WW(8) was
Initial Abatement Report 9 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
collected from the west wall of the excavation at a depth of anoroximately 8 feet below grade
These six soil samples were analyzed by Pace Analytical Services. LLC of Huntersville, North
Carolina for analysis. Soil sample BOTI (6) was analyzed for gasoline range organic compounds
(GRO) and diesel range organic compounds (DRO) in accordance with SW-846 Method 8015C.
Soil samples BOT204), SW(9), EW(11), NW(9) and WW(8) were analyzed for volatile or anic
compounds (VOCs) by SW-846 Method 8260D: semi -volatile organic compounds (Semi-VOCs) in
accordance with SW-846 Method 8270E BN/A and, volatile Petroleum hydrocarbon (VPHJ
compounds and extractable petroleum hydrocarbon (EPH) compounds by Massachusetts
Methods. A copy of the laboratory report is presented in Appendix J and a copy of the Chain -of -
Custody Record is included in Appendix I. As indicated by these results, no targeted compounds
were detected in the BOT2(14), SW(9), EW01), NW(9) and SW(8) samples at concentrations
exceeding the respective analytical method detection limits. Based on these results, Harmon
Environmental, PA recommends the DEQ issue a no -further -action letter for this incident and
assist with the removal of the Notice of Residual Petroleum from the site.
J. Figures
Provide the following:
1. A topographic map illustrating the area within 1500-foot radius of the source of the release, showing:
Topographic contours;
Site location;
® Buildings;
© Adjacent streets, roads, highways (identified by street names and numbers);
o Surface water bodies;
o Groundwater flow direction (if determined); and
North arrow and scale.
See Figure 1
A site map* and cross -sections illustrating the UST system(s)/excavation area(s), drawn to scale, showing:
Buildings and property boundaries;
© Underground utilities, such as sewer lines and other conduits; basements; and vaults;
© Water supply wells, surface water bodies
o Location and orientation of current and former UST(s), pumps; product lines, sumps, etc.;
© Length, diameter and volume of current and former UST(s);
© Type of material(s) stored in UST(s) (currently and formerly); and
o Names or descriptions of properties adjacent to the site; and
o North arrow and scale.
Figure 2 presents a scaled drawing of the residence and property boundaries. Soil sample locations,
sample designations sample depths and the frnal limits of the excavation are depicted on Figure 3. No
groundwater sampling activities were conducted in conjunction with this project. As a result, this
ire does not present groundwater monitoring locations or groundwater flow direction. The final
limits of the excavation an approximate scale and a north arrow are presented on Figure 3.
3. Map(s)* and geological cross -sections, drawn to scale, depicting all soil analytical results obtained to date
and final confirmatory sample results, to include:
RE; Description of soil and bedrock lithology (as determined by investigation to date);
© Location and orientation of UST(s), pumps, piping, sumps, etc.(current and former);
Soil sample identification (unique letter and/or numerical code), location, and depth;
Soil sample analytical results;
Final limits of each stage of excavation for each excavation on site**; and
Two geological cross -sections, drawn across the contaminated area and intersecting at right angles,
showing the vertical distribution of the contaminants in the unsaturated zone. (Indicate vertical and
horizontal scale, orientation of each section, location of water table, soil types and lithology, all
borings and sample locations represented by the sections, and soil analytical results for each
represented sample, and show sections as labeled lines on the map.)
Initial Abatement Report 10 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental com

Initial Abatement Action Report Appendix A
Report Formats
Figure 3 presents a scaled drawing of the area immediate surrounding the excavation. This
figure presents the locations, sample designations, depths and analytical results associated with
the soil samples collected during this excavation project. A north arrow and an approximate
scale are presented on this figure. No geologic cross -sections have been prepared in conjunction
with this project. A description of the soil types encountered during this excavation is discussed in
response to Question B.S. of this form. A Geologic Log of the excavation is presented in Appendix
4. Map(s)* and geological cross -sections, drawn to scale, depicting the groundwater and surface water
analytical results,** to include;
o Location and orientation of UST(s), pumps, piping, sumps, etc.(current and former);
Groundwater sample identification (unique letter and/or numerical code referencing monitoring or
water supply well)and location;
Surface water sample identification (unique letter and/or numerical code) and location; and
Groundwater and surface water sample analytical results.
No groundwater or surface water samples were collected in conjunction with this initial
abatement project.
5. A free product map* showing thickness (infect) and extent of free product** using contour lines; and
No free product was observed during this initial abatement project.
6. A potential receptor map that clearly identifies water supply wells (municipal or public/private wells, etc.) and
other potential receptors (surface water bodies, basements, utilities, etc.) which are at risk.
*Note: If possible, use a single base map to prepare site plans using a map scale of 1 inch = 40 feet (or a
smaller scale for large sites, if necessary). Maps and figures should include conventional symbols, notations,
labeling, legends, scales, and north arrows and should conform to generally accepted practices of map
presentation such as those enumerated in the USGS Geological Survey pamphlet, "Topographic Maps."
** If applicable
A receptor survey was not conducted in coniunction with this initial abatement project.
K. Tables
Provide the following:
1. Site History (Complete Tables 13-1 and B-2 from Guidelines, Appendix B);
Tables B-1 and B-2 are attached.
2. Public and Private Water Supply Well and Other Receptor Information (Complete Table B-5 from
Guidelines, Appendix B);
A receptor survey was not conducted in conjunction with this initial abatement proiect.
3. Field Screening Results;
This table was not used in this project.
4. Summary of Soil Sampling Results (Complete Table B-3 from Guidelines, Appendix B);
See Table B-3 attached.
5. Summary of Groundwater and Surface Water Sampling Results* (Complete Table B-4 from Guidelines,
Appendix B)*;
This table is not applicable to this project.
Initial Abatement Report 11 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
6. Monitoring and Remediation Well Construction Information (Complete Table B-7 from Guidelines, Appendix
B)*;
This table is not applicable to this project.
7. Free Product Recovery Information (Complete Table 13-8A from Guidelines, Appendix B)*;
This table is not applicable to this project.
8. Cumulative Volume of Free Product Recovered from Site (Complete Table 13-813 from Guidelines, Appendix
B)*;
This table is not applicable to this project.
9. Current and Historical Groundwater Elevations and Free Product Thickness (Complete Table B-9 from
Guidelines, Appendix B)*.
* If applicable
This table is not applicable to this project.
L. Appendices
Provide the following:*
Appendix A
Tightness testing results and supporting documentation*
Appendix B
Notification of Intent: UST Permanent Closure or Change -in -Service (UST-3 Form)
Appendix C
Site Investigation Report for Permanent Closure or Change -in -Service of UST (UST-2
Form)*
Appendix D
Site Specific Health and Safety Plan (HASP)
Appendix E
Certificate of UST disposal*
Appendix F
Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature)*
Appendix G
Standard procedures (sampling, field equipment decontamination, field screening, etc.)
Appendix H
Soil, water, free product, and sludge disposal manifests and soil treatment permits*
Appendix I
Complete chain -of -custody records
Appendix J
Copy of all laboratory analytical records
Appendix K
Photographs of site check, closure, and excavation activities (optional)
Appendix L
Geologic logs for excavation(s)/borings (related to IAA investigation only)
Appendix M
Monitoring Well Construction Forms (for all wells constructed to date)
* If applicable
Initial Abatement Report 12 Harmon Environmental, PA
Revocable Trust of Sharon Saville Parker Property 615 Bruce Thomas Road
6342 Deveron Drive Monroe, North Carolina 28112
Charlotte, North Carolina 28211 www.harmonenvironmental com

Figures

APPROXIMATE SCALE IN FEET
0 2000 4000
SOURCE: TOPO! 2003 NATIONAL GEOGRAPHIC
FIGURE 1
HARMON ENVIRONMENTAL, PA SITE LOCATION MAP
615 BRUCE THOMAS ROAD REVOCABLE TRUST OF SHARON SAVILLE PARKER
MONROE, NORTH CAROLINA PROPERTY
harmonenvironmental.com 6342 DEVERON DRIVE o
CHARLOTTE. NORTH CAROLINA

LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
PAVED AND GRAVEL SURFACES
O APPROXIMATE LOCATION OF
EXCAVATION
APPROXIMATE LOCATION OF
i_, FORMER UNDERGROUND APPROXIMATE SCALE IN FEET
STORAGETANK
APPROXIMATE LOCATION OF
FENCE
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
harmonenvironmental.com
40 80
SOURCE: MECKLENBURG COUNTY GIS AND FIELD MEASUREMENTS
SITE LAYOUT MAP
REVOCABLE TRUST OF SHARON SAVILLE PARKER
PROPERTY
6342 DEVERON DRIVE
CHARLOTTE, NORTH CAROLINA

EW(11)
NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE ANALYTICAL
METHOD DETECTION LIMITS
Q
a
4e
sw(g)
NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE ANALYTICAL
/ METHOD DETECTION LIMITS
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
PAVED AND GRAVEL SURFACES
a APPROXIMATE LOCATION OF
EXCAVATION
APPROXIMATE LOCATION OF
FORMER UNDERGROUND
STORAGETANK
APPROXIMATE LOCATION OF
FENCE
• APPROXIMATE LOCATION OF
SOIL SAMPLE
(8) APPROXIMATE DEPTH OF SOIL
SAMPLE IN FEET BELOW GRADE
MG/KG MILLIGRAMS PER KILOGRAM
HARMON ENVIRONMENTAL, PA
615 BRUCE THOMAS ROAD
MONROE, NORTH CAROLINA 28112
harmonenvironmental.com
NW(9)
NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE ANALYTICAL
METHOD DETECTION LIMITS
CC
F�R/O
CFR
OqO
BOTI (6)
GRO 224 MG/KG
DRO 10,100 MG/KG
BOT2(14)
NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE ANALYTICAL
METHOD DETECTION LIMITS
WW(8)
NO TARGETED COMPOUNDS
DETECTED AT CONCENTRATIONS
EXCEEDING THE RESPECTIVE ANALYTICAL
METHOD DETECTION LIMITS
NOTES:
SOIL SAMPLE BOTI (6) WAS COLLECTED BY HARMON ENVIRONMENTAL.
PA PERSONNEL AND ANALYZED BY PACE ANALYTICAL SERVICES, LLC
FOR GASOLINE AND DIESEL RANGE ORGANIC COMPOUNDS BY SW-846
METHOD 8015C FOLLOWING SAMPLE PREPARATION IN ACCORDANCE
WITH SW-846 METHOD 5030E AND METHOD 3546, RESPECTIVELY.
SOIL SAMPLE BOT2(14), SW(9), EW(II), NW(9), AND WW(8) WERE
COLLECTED BY HARMON ENVIRONMENTAL, PA PERSONNEL AND
ANALIZED BY PACE ANALYTICAL SERVICES, LLC FOR VOLATILE ORGANIC
COMPOUNDS BY SW-846 METHOD 82601): SEMI -VOLATILE ORGANIC
COMPOUNDS BY SW-86 METHOD 8270E BN/A, AND VOLATILE AND
EXTRACTABLE PETROLEUM HYDROCARBON COMPOUNDS BY
MASSACHUSETTS METHODS.
APPROXIMATE SCALE IN FEET
0 40 80
SOURCE: MECKLENBURG COUNTY GIS AND FIELD MEASUREMENTS
SITE LAYOUT MAP WITH ANALYTICAL RESULTS
REVOCABLE TRUST OF SHARON SAVILLE PARKER
PROPERTY
6342 DEVERON DRIVE

Tables

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System Information
Revision Date: 11/11/2021 Incident Number and Name: 47974/Sharon Saville Parker Property
UST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pum s
Date Tank
Installed
Status of
UST ***
Was release
associated
with the UST
S stem?
UST-1
Heating Oil
Heating
Oil
550
Gallons
Single
Wall Steel
48 in by
74 in
Copper
Feed and
Return
Unknown
Removed
10/26/21
Yes
Add additional records as necessan,
Description
Was release
AST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
AST ***
with the AST
Pumps
System?
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-2: Site History - UST Owner and Operator Information
Revision Date: 1 1/1 1/2021 Incident Number and Name: 47974/Sharon Saville Parker Pro ert
UST ID Number
UST-1
Facility ID Number
I N/A
Name of Owner
Dates of Ownership
mm/dd/ to mm/dd/
Unknown
Street Address
City
State
Zip
Telephone Number
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Unknown
Street Address
City
State
Zip
Telephone Number
UST ID Number
Facility ID Number
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
Street Address
City
State
Zip
Telephone Number
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Unknown
Street Address
City
State
Zip
Tele hone Number
Add additional records as necessary

Table B-3: Summary of Soil Sampling Results
Revision Date: 11/11/2021 Incident Number and Name: 47974/Sharon Saville Parker Property
Analytical Method
8015
8015
8260B
8270
VPH&EPH
Contaminant of Concern
V
O
>
v
Oj
E
°.'
a
n=
>
Sample
ID
Date
Collected
Source
Area
Sample
Depth
Incident
Phase
BOT1(6)
10/26/2021
UST Basin
6
Initial Abatement
10,100
224
No Targeted Compounds Detected
BOT2(14)
10/26/2021
UST Basin
14
Intital Abatement
SW(9)
10/26/2021
UST Basin
9
Initital Abatement
EW(11)
10/26/2021
UST Basin
11
Initial Abatement
NW(9)
10/26/2021
UST Basin
9
Initial Abatement
WV(8)
1 10/26/20211
UST Basin
1 8
1 Initial Abatement
DEQ Action Level
100
50
Soil to Groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
Industrial/Commerical MSCC (mg/kg)
Notes: MSCC = Maximum Soil Contaminant Concentration
Sample Depth presented in feet below ground surface
Results presented in milligrams per kilogram (mg/kg)
DRO = Diesel Range Organic Compounds
GRO = Gasolline Range Organic Compounds
NA = Not Applicable

Appendix A
Tightness Testing results and Supporting Documentation
(This Appendix is not applicable to this project)

Appendix B
Notification of Intent: UST Permanent Closure or
Change -in -Service (UST-3 Form)
(This Appendix is not applicable to this project)

Appendix C
Site Investigation Report for Permanent Closure
Or Change -in -Services of UST (UST-2 Form)
(This Appendix is not applicable to this project)

Appendix D
Site Specific Health and Safety Plan

Site Specific Health and Safety Plan
for
Site Assessment Activities
at
6342 Deveron Drive, Charlotte, North Carolina
October 14, 2021
Prepared By:
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
704-292-4527
Harmonenvironmental. com
This document is confidential and is to be used by designated project personnel. Reproduction of
this document is strictly prohibited unless approved in writing by Harmon Environmental, PA.

Signatures of Approval
Project Manager
Date
Corporate Health and Safety Coordinator
Date
Site Health and Safety Manager
Date

Plan Acceptance
I have been permitted the opportunity to read this Health and Safety Plan for Site Assessment
Activities at 6342 Deveron Drive, Charlotte, North Carolina, and have been briefed by the Site
Safety Manager or an appropriately designated alternate on its content. All questions and
comments I have asked or stated regarding this Plan have been satisfactorily addressed. I
understand the contents of this Plan and agree to abide by its requirements.
Each person entering exclusion zones defined in Section 5.4 of this Plan shall sign below.
ISigure Printed Narppe Company Date

Table of Contents
Section
Title
Page No.
1.0
General Information
1
2.0
Project Organization
2
3.0
Site Description
2
4.0
Site Safety Control
2
5.0
Hazard Assessment/Personnel Protection
3
6.0
Decontaminating Procedures
4
7.0
Emergency Procedures
4
Figure Site Layout Map
Appendix A Exposure Limits of Chemical Hazardous
Appendix B Route to Hospital

1.0 General information
1.1 Site Safety Plan Preparation:
Plan Prepared By: R. Harmon
Date Plan Approved: October 14, 2021
1.2 Site Information:
Site Name: 6432 Deveron Drive Charlotte, NC
Site Location: 6432 Deveron Drive, Charlotte, NC
Site Contact: None
Site Status: Open (X ) Closed( )
Limited Access( ) Fenced( )
Existing Site Information:
Detailed ( ) Sketch ( )
Preliminary (X) None ( )
Facility EPA I.D. No.:N/A
1.3 Hazardous Materials Information:
State/Form of Hazardous Materials:
Gas ( ) Liquid( Soil (X)
Groundwater (X) Sludge( Solid( )
Material Hazards:
Corrosive( Volatile (X) Ignitable ( )
Toxic ( ) Reactive ( ) Explosive ( )
Radioactive () Unknown () Flammable ( )
1.4 Scope of Work:
Excavate petroleum -impacted soil from the vicinity of a former residential heating
oil underground storage tank. The excavated soil will be loaded directly onto trucks
for transport to a licensed disposal facility. Following completion of the
excavation, soil samples will be collected, and the excavation will be backfilled
with clean soil imported from off -site.
Health and Safety Plan 1 Harmon Environmental, PA
6342 Deveron Drive 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
October 14, 2021 704-292-4527

2.0 Project Organization
Project Manager:
Corporate Health and Safety Coordinator:
Site Health and Safety Manager:
Technical Support:
Harmon Environmental Project No. 896-01
3.0 Site Description
Richard Harmon
Richard Harmon
Richard Harmon
DeBruhl Environmental Excavating, Inc.
The site consists of a residential property with a former heating oil underground storage tank.
4.0 Site Safety Controls
4.1 Site Map:
See attached figure
4.2 Perimeter Control:
No perimeter control is in place at the site.
4.3 Command Post Area:
The command post will be established outside of the exclusion zone at the subject site. A telephone
will be available at the command post area.
4.4 Exclusion Zones:
During the excavation activities, the exclusion zone shall be defined as a 15-foot radius around the
open excavation.
4.5 Decontamination Area:
Decontamination of the excavation equipment will be performed on -site.
5.0 Hazard AssessmenVPersonnel Protection
5.1 General
Primary routes of potential exposure are through inhalation of dust, ingestion, and skin contact
with impacted soil and/or groundwater. Hazards include the physical hazard associated with
excavation, drilling and well advancement activities. Due to the outdoor location of the project
and expected hazards, moderate health risks are anticipated.
Health and Safety Plan 2 Harmon Environmental, PA
6342 Deveron Drive 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
October 14, 2021 704-292-4527

5.2 Health and Safety Training Requirements
All field personnel (including Subcontractors) must have appropriate hazardous waste site health
and safety training in accordance with OSHA 1910.120 regulations prior to initiating on -site
activities. The Site Safety Manager must have an additional 8 hours of specific site management
training.
5.3 Personnel Protection
General Level of Protection:
A ( ) B ( ) C ( ) D modified ( ) D (X)
Level D:
For all personnel participating in the excavation and sampling activities, the following equipment
is required as a minimum:
• Chemical resistant outer gloves
• Steel toe and shank boots
• Standard work clothing (long -sleeve shirt and long pants)
• Hard hat and safety glasses.
• Ear protection (when noise levels preclude normal conversation)
5.4 Upgrading and Downgrading of Personnel Protection:
Upgrading and downgrading of personnel protection levels will be implemented if deemed
necessary by the Site Safety Manager. Any upgrades will be based on observed site conditions.
Under no circumstances will downgrading be permitted by any field personnel without the consent
of the Site Safety Manager.
6.0 Decontamination Procedures
• Boots, boot covers, and gloves will be cleaned with phosphate -free soap and tap
water.
• Disposable coverings and equipment will be cleaned with phosphate -free soap and
tap water, then disposed of as normal trash.
Health and Safety Plan 3 Harmon Environmental, PA
6342 Deveron Drive 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
October 14, 2021 704-292-4527

• Sampling equipment will be cleaned with phosphate -free soap, and tap water,
followed by a distilled water rinse.
7.0 Emergency Procedure
7.1 Field Communications: Hand signals when distressed; working in noisy
environment; or wearing respirators.
Thumbs up
Thumbs Down
Hands on wrist
Hands on Throat
OK
Not OK
Exit Exclusion Zone
Cannot Breathe
7.2 In the Event of Personnel Exposure:
Skin Contact: Flush with water, remove impacted clothing. Secure Medical
Attention
Inhalation: Move person away from exclusion zone, administer first aid and
CPR as necessary. Secure medical attention.
Ingestion: Secure medical attention.
Eye Contact: Irrigate with water. Secure medical attention.
7.3 Personnel Injury:
In the event a personnel injury occurs, decontaminate individual if injury is not life
threatening. If decontamination is not feasible, wrap the victim in a blanket,
administer first aid or CPR as necessary, contact the local rescue squad, and
hospital.
All injuries, exposures, or spills are to be documented by the Site Safety Manager
and reported to the Project Manager within 24 hours. Such documentation is to be
kept on file at Harmon Environmental, PA for future reference.
7.4 Heat Stress:
In the event of heat stress, move the victim out of the heat to a cool area on site.
Place the victim in shock position with their feet elevated. Cool the victim by
spraying with water or using wet towels and fanning. Secure medical attention.
Health and Safety Plan 4 Harmon Environmental, PA
6342 Deveron Drive 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
October 14, 2021 704-292-4527

7.5 First Aid Equipment:
A first aid kit is located within the support vehicles on -site. Potable water is available on -site.
7.6 Route to Hospital
See Appendix B
7.7 Emergency Information:
Service
Phone
Ambulance
911
Fire Department
911
Police
911
Hospital (Novant)
[phone]
Charlotte Poison Control
[phone]
North Carolina Department of Environment,
[phone]
Health and Natural Resources
Region IV EPA
[phone]
DeBruhl Environmental Excavating, Inc.
[phone]
Harmon Environmental, PA
[phone]
896-01.H&S
Health and Safety Plan 5 Harmon Environmental, PA
6342 Deveron Drive 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
October 14, 2021 704-292-4527

Figures

Polaris 3G Map — Mecklenburg County, North Carolina
Date Printed: 10/14/2021 4:35:02 PM

Appendix A
Exposure Limits of Chemical Hazards

)NOCO -- DIESEL kUhL 1NU. [ - IJMazl, rUl- iL,
)NOCO -- DIESEL FUEL NO. 2 - DIESEL FUEL
tTERIAL SAFETY DATA SHEET
;N: 9140002865296
Lnufacturer's CAGE: 15445
in No. Indicator: A
in Number/Trade Name: DIESEL FUEL NO. 2
General Information
:em Name: DIESEL FUEL
)mpany's Name: CONOCO INC
)mpany's Street: 600 N DAIRY ASHFORD RD RM 3012
)mpany's P. 0. Box: 4784
)mpany's City: HOUSTON
)mpany's State: TX
)mpany's Country: US
=pany's Zip Code: 77210-4784
)mpany's Emerg Ph #: 713-293-5550/800-424-9300
Dmpany's Info Ph #: 713-293-5550
scord No. For Safety Entry: 029
Dt Safety Entries This Stk#: 093
-.atus: SMU
ste MSDS Prepared: 14AUG91
sfety Data Review Date: 24JUN92
apply Item Manager: KY
SDS Serial Number: BMZTT
uecification Number: VV-F-800
pec Type, Grade, Class: GRADE DF-2
azard Characteristic Code: F4
Ingredients/Identity Information
roprietary: NO
ngredient: PETROLEUM MID -DISTILLATE (DIESEL MARINE FUEL)
ngredient Sequence Number: 01
ercent: 100 %
IOSH (RTECS) Number: 1004302PE
AS Number: 68476-34-6
SHA PEL: 5 MG/M3 AS OIL MIST
CGIH TLV: 5 MG/M3 AS OIL MIST
ther Recommended Limit: NONE SPECIFIED
Physical/Chemical Characteristics
.ppearance And Odor: CLEAR OR LIGHT YELLOW LIQUID, AROMATIC ODOR
oiling Point: 350 - 680F
Ielting Point: NOT GIVEN
'apor Pressure (MM Hg/70 F): 1 MMHG
vapor Density (Air=1): > 1
Specific Gravity: 0.85 - 0.93
)ecomposition Temperature: NOT GIVEN
:vaporation Rate And Ref: NIL
solubility In Water: INSOLUBLE
?ercent Volatiles By Volume: NIL
;orrosion Rate (IPY): UNKNOWN
Fire and Explosion Hazard Data
-lash Point: 130F,54C
?lash Point Method: TCC
ittp://msds.pdc.comell.edu/msds/siri/msds/h/q 194/g436.htm1 10

1 "f'� r Vl J
Lower Explosive Limit: 0.4
7pper Explosive Limit: 6 %
Extinguishing Media: WATER SPRAY, FOAM, DRY CHEMICAL CAARBON DIOXIDE
Special Fire Fighting Proc: USE WATER TO KEEP FIRE -EXPOSED CONTAINERS
OOL. IF LEAK OR SPILL HAS NOT IGNITIED, USE WATER SPRAY TO DISPERSE THE
VAPORS AND TO PROVIDE PROTECTION.
Jnusual Fire And Expl Hazrds: PRODUCTS OF COMBUSTION MAY CONTAIN CARBON
MONOXIDE, CARBON DIOXIDE AND OTHER TOXIC MATERILS. DO NOT ENTER ENCLOSED OR
ONFINED SPACE WITHOUT PROPER PPE.
Reactivity Data
Stability: YES
�ond To Avoid (Stability): AVOID HEAT AND FLAME
Materials To Avoid: INCOMATIBLE WITH OXIDIZING MATERIALS.
Health Hazard Data
Precautions for Safe Handling and Use
Control Measures
Transportation Data
Disposal Data
---------------------------------------------------------------------------
Label Data
Sabel Required: YES
Technical Review Date: 24JUN92
MFR Label Number: NONE
Label Status: G
:�ommon Name: DIESEL FUEL NO. 2
�hronic Hazard: NO
Signal Word: CAUTION!
kcute Health Hazard -Slight: X
7ontact Hazard -Slight: X
Fire Hazard -Slight: X
Reactivity Hazard -None: X
Special Hazard Precautions: STORE IN WELL VENTILATED AREEA. KEEP CONTAINER
TIGHTLY CLOSED. STORE IN ACCORDANCE WITH NATIONAL FIRE PROTECTION ASSN
REGULATIONS. FIRST AID: INHALATION: REMOVE TO FRESH AIR. IF NOT BREATHING,
3IVE ARTIFICIAL RESPIRATION. IF BREATHING IS DIFFICULT, GIVE OXYGEN. CALL A
PHYSICIAN. SKIN: FLUSH SKIN WITH WATER AFTER CONTACT. REMOVE CONTAMINATED
;LOTHING. EYES: IMMEDIATELY FLUSH WITH WATER FOR 15 MINUTES. CALL A
PHYSICIAN. INGESTION: DO NOT INDUCE VOMITING. IMMEDIATELY GIVE TWO GLASSES
DF WATER. NEVER GIVE ANYTHING TO IF UNCONCIOUS. CALL MD
Protect Eye: Y
Protect Skin: Y
Label Name: CONOCO INC
Label Street: 600 N DAIRY ASHFORD RD RM 3012
Label P.O. Box: 4784
Label City: HOUSTON
Label State: TX
Label Zip Code: 77210-4784
http://msds.pdc.comell.edu/msds/sirilmsds/h/q 194/g436.html 10/14/200'

rage S of .i
,abet Country: us
:abel Emergency Number: 713-293-5550/800-424-9300
tp://msds.pdc.comell.edu/msds/siri/msds/h/q 194/g436.html 10/14/2001

Appendix B
Route to Hospital

10/14/21, 4:23 PM 6342 Deveron Dr, Charlotte, NC 28211 to Hospital, Hawthorne Lane, Charlotte, NC - Google Maps
Go gle Maps 6342 Deveron Dr, Charlotte, NC 28211 to Hospital, Drive 5.4 miles, 14 min
Hawthorne Lane, Charlotte, NC
�..
RIYOLUTI;M V:;IMORE
':ES: DLL'C PAFA. .. (R ,�..
WCU END - r.ospRM
EROJ*N•LL
Eu Gs'In,Rs,�'
APn1n Ml3RA :RrNnsS
`�SL,iwa
:. _
J9
j
Meaprume.©
�
YOOTIiSIDE
PARE
-
�u r,e^i Rardc;<
�r
�.
q
SED6Ef:ELD _
GlfCpR AN 1•F - Y CASTDVER
`Ly
... ��
pAh
y^ + Q
!
+
y
ILL OE
VILLA4E
F�+�.
_ EREEDDAA
PEPDAVV.
EVID
ROAD
f
'fKVER-
`` y
COTSWOID
i
e
G:.s�t+T rf, J
�
� e `� f
CVLLIND'MOuD
S
i
MIYwSPMA
pCLAWSIII PM*
ClAW3ON P .. ` ' WEP4
{PA G,3 yn
` OLFAIID SOUTH
•
vM1AaE . _
yys
vEas! AA3rAltnP.vg Hp�
8
scn:o. �Pun�aapr
i
!
AwNTfouD
�
f'�
cA�owuoD
4
E
4 y
N-a1wnM
y
FDPESi
i
■
ff
~,SO. PAR* '^"'^•�
PPOVIDEN
PMN
�
$
..i cj DAF^:LM WNNS
:ReM 7
-!: aM �',I
■���■ EASDfORFST
r
1, :.....,r
y
STONENAVEN 9
r
, r.,.,,.,M "COIe:G31PPlr Q �7 g
r: Go gle tii
~a pasuRM
_. Rpa
N1r�yl:ie
ep'�
Map data 02021 Google 2000 ft ■ ■
6342 Deveron Dr
Charlotte, NC 28211
Take Glenridge Rd to Rama Rd
2 min (0.3 mi)
t 1. Head northeast on Deveron Dr toward Glenridge
Rd
'l 2. Turn left onto Glenridge Rd
r* 3. Turn right onto Deveron Dr
118ft
0.2 mi
384 ft
Take Randolph Rd to N Caswell Rd
10 min (5.0 mi)
41 4. Turn left at the 1 st cross street onto Rama Rd
0.2 mi
t 5. Continue onto Sardis Rd
F+ 6. Turn right onto Randolph Rd
S Pass by Jack in the Box (on the right in 1.3 mi)
0.5 mi
4.3 mi
https://www.google.com/maps/dir/6342+Deveron+Dr,+Charlotte,+NC+28211 /Hospital,+Hawthome+Lane,+Charlotte,+NC/@35.1834539,-80.8116789,1... 1 /2

10/14/21, 4:23 PM 6342 Deveron Dr, Charlotte, NC 28211 to Hospital, Hawthorne Lane, Charlotte, NC - Google Maps
Continue on N Caswell Rd to your destination
f+ 7. Turn right onto N Caswell Rd
+1 8. Turn left
F+ 9. Turn right
10. Turn left
4D Destination will be on the right
Hospital
200 Hawthorne Ln, Charlotte, NC 28204
These directions are for planning purposes only.
You may find that construction projects, traffic,
weather, or other events may cause conditions to
differ from the map results, and you should plan
your route accordingly. You must obey all signs or
notices regarding your route.
1 min (0.1 mi)
387 ft
135 ft
46 ft
75 ft
https://www.google.com/maps/d ir/6342+Deveron+Dr,+Charlotte,+NC+28211 /Hospital,+Hawthome+Lane,+Charlotte,+NC/@35.1834539,-80.8116789,1... 2/2

Appendix E
Certification of UST Disposal

UST Disposal Company
4921 Hoover Drive
Charlotte, NC 28269
704-599-0770
CERTIFICATE OF TANK DISPOSAL
Certificate Number: 20121035
Contractor:
DeBruhl Environmental Excavating, Inc
4921 Hoover Drive
Charlotte, NC 28269
TYPE OF TANK SIZE
UST 46" x 74"
Date: 11/4/2021
Address:
6342 Devron Dr
Charlotte, NC 28211
GALLONS
550
UST Disposal Company certifies that the above mentioned tank has been properly
disposed of and the contents and sludge processed in full compliance with local, state and
federal regulations.
UST Disposal Company
4921 Hoover Drive
Charlotte, NC 28269

Appendix F
Groundwater Field Measurements
(This Appendix is not applicable to this project)

Appendix G
Standard Procedures

Standard Procedures
Soil Sampling in Conjunction with UST Removal
For safety reasons, soil samples associated with UST closures are typically collected
using the bucket of the excavator as the sampling equipment. To accomplish this task,
Harmon Environmental, PA sampling personnel direct the excavation contractor to
extract a sample from a pre -defined location on the base or side -wall of the excavation.
This soil sample is then brought to the surface of the ground and staged at a safe location
for screening and sampling.
Typically a sample aliquot is collected from the bucket of the excavation equipment and
placed directly into a zipper seal bag for field screening with a Multi -Rae® photoionizing
organic vapor detector (PID), or equivalent, calibrated to an isobutylene standard. New
latex gloves, or equivalent, are worn throughout the collection of the screening sample.
Each zipper seal bag is labeled with a sample designation, time, date, approximate depth
and sampler's initials at the time of collected.
Based on the results of the field screening activities, Harmon Environmental, PA field
personnel may opt to collect a sample aliquot from the excavator bucket for laboratory
analyses. Prior to collecting a sample, new latex gloves, or equivalent, are donned, and
the laboratory supplied sample bottles are labeled. Each soil sample is then collected
directly from the excavator bucket and placed directly into the pre -labeled glassware
provided by the laboratory. These samples are then placed in a cooler on ice pending
delivery under chain -of -custody protocol to the analyzing laboratory.
The depth of each sample, the location of each sample, the time of sample collection, the
field screening results and any deviations from these standard protocols are documented
in the field notes prepared in conjunction with each project.

Appendix H
Soil, Water, Free -Product and Sludge Disposal Manifests
And Soil Treatment Permits

�� P.CiBOX 235
K_�UI�/��YN��T�| SOILS, INC.ENVIRONMENTAL /r��- ^���/^-^�' uv��LATT|K8ORE.N.C28O89
704'434-0075
NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL
APPROVAL#MAN|FEST#
LOCATION OF SOIL:
TRANSPORTER:
T|k4E: TRUCK#
DATE: LICENSE#_-__�
DRIVER SIGNATURE
T|K4E� - - TRUCK#
DATE: - - -- LICENSE #
DRIVER SIGNATURE
TIME. -
DATE:
DRIVER S|GNATURE__
GROSS WT.___
TAREVVT.____
NET WT.
`
- GR(}S8VVT. _-
LBS.
TAREVVT. -_
- LB5.
NET WT.
LBS,
_ TRUCK #___' __ _ GROSS WT. __-_LBS.
_ L|CENSE#_-- TAREVVT.-_______-_
LBG.
TIME: _- --TRUCK#---------GROSSUVT.--__' --LBS.
DATE: _- _- -_-' L|CEN8E#'_--__--� TAREVVT. LBS.
DRIVER SIGNATURE. --. _ ���_- NETVVT. LBS.
TOTAL. NET VVT _
TOTALEOU|V'TONS _
INSPECTED & ACCEPTED BYENVIRONMENTAL SOILS, INC.

DEBRUHL ENVIRONMENTAL EXCAVATING, INC.
4921 HOOVER DRIVE
CHARLOTTE, NC 28269
704-598-2681 - OFFICE
NON -HAZARDOUS WASTE MANIFEST
DATE %� c:' 2 � / zo `z j LOAD NUMBER `
ENVIRONMENTAL CONSULTANT: Harmon Environmental
Contact: Rick Harmon Phone: [phone]
GENERATOR: C jr,:� j
Address:6 34.1- "A�
Contact: L,q,.a( lvt;l ��.r Phone: -7v4- - ,S"77 -476`'
TRANSPORTER: DeBruhl Environmental Excavating, Inc,
Contact: Randy DeBruhl Phone: [phone]
DESTINATION: Environmental Soils, Inc., Dedicated Land Application Site
CLASS & TYPE OF CONTAMINATE IN SOIL: Class II- petroleum
WASTE ORIGINATION POINT: 63 4 z -V12.\1 00 ") b t ` 4:,f"'` �' It'—' ,V'(-'
COUNTY: Mecklenburg SOURCE OF CONTAMNTION: UST
f-Q- �D D�
TRUCK#:2 VOLUME:��/fib
DRIVER SIGNATURE: z'_ DATE:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:
In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in
question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of
Waste Constituents. I certify that I ant familiar with the source of contamination of the
soil and further certify the source, to the best of my knowledge, contains no contaminants
other than that listed above.
Signature- t ' ) ��L _ Date
Company Name __Title

DEBRUHL ENVIRONMENTAL EXCAVATING, INC.
4921 HOOVER DRIVE
CHARLOTTE, NC 28269
704-598-2681 - OFFICE
NON -HAZARDOUS WASTE MANIFEST
DATE_ / 0 / Z,/2a al-1 LOAD NUMBER ..)
ENVIRONMENTAL CONSULTANT: Harmon Environmental
Contact: Rick Hannon Phone: [phone]
GENERATOR: Cjr,L, j
Address:W.3 4 z- fir+ lAe
Contact:LA,,,( y� ; l r�,,, Phone: -7u f - ,s 77 -4 76
TRANSPORTER: DeBruhl Environmental Excavating, Inc.
Contact: Randy DeBruhl Phone: [phone] i
DESTINATION: Environmental Soils, Inc., Dedicated Land Application Site
CLASS & TYPE OF CONTAMINATE IN SOIL: Class II- petroleum
WASTE ORIGINATION POINT: 63 4 --'— _ ? ,1 pv "J D r , CAP, L tlZ , Al (.
COUNTY: Mecklenburg SOURCE OF CONTMMT TION: UST
TRUCK#: M G �l. VOL UM '�6 L
DRIVER SIGNATURE: J� / DATE: J G, Z U, Z I
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:
In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in
question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of
Waste Constituents. I certify that I am familiar with the source of contamination of the
soil and further certify the source, to the best of my knowledge, contains no contaminants
other than that listed above,
Signature f,�(� ' �'� Date ;, b 1 7'1 j
Company Name 57 _____—Title

F-t4VIRONMENTAL SOILS, INC. ENVIRONMENTAL SOILS, INC.
P.O. BOX 295 P.O. BOX 295
LATTIMORE, N.C. 28089-0489 LATTIMORE, N.C. 28089-0489
704/434-0075 704/434-0075
[phone] FAX
[phone] FAX
Job Name: Job Name:
I
Truck# kw�- (
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons: 11 eAr
PUBLIC WEIGHM A -
LICENSE EXPIRES JUNE
Weighed by: MATT RICE
INVALID UNLESS SIGNED
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt.:
Tons:
PUBLIC WEIGHNIA-
LICENSE EXPIRES JUNE
Weighed by: MATT RILT
r.
—A'75171:.c:nc� 7 7-TE
ENVIRONMENTAL SOILS, INC.
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
[phone] FAX
Job Name:
Truck#
6 lb
'�G lb KEYED
l
Gross Wgt.: .44' b
Tare Wgt:
Net Wgt.:
Tons:

Appendix I
Completed Chain -of -Custody Records

CHAIN -OF -CUSTODY Analytical Request Document
PaceAnalytical'
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
pany: Billigg Information:
pI- "y'�-4�, %I—f,-r-t�,t.�cwi��i�Ct►;��/JVl
less:/.r �j,t,) ,/� 4,1
� 7 L J ��L C�1 t i+�GLi1�� L� i7�_.nr� e-4^
Copy To: Si 90! io o/Address:
Customer Project Name/Number: State: County/City: Time one Collected:
( /��. J PT [ ] MT ( J CT (VJ ET
Phone -;a ZA t' ---t 3-L'4 Site/Facility IDN: Compliance Monitoring?
Email `-10 t , [ 1 Yes jy No
Cqllected By (pr'n ):
Purchase Order N:
DW PWS ID N:
Quote M
DW Location Code:
Collected By (�ignature):
Turnaround Date Required:
Imme late y —Packed on Ice:
7l`', rN,
[ .j Yes [ J No
Sample Disposal:
Rush:
Field Filtered (if applicable):
[ Dispose as appropriate I J Return
[ [ Same Day [ ] Next Day
[ J Yes ( ] No X-4%
I 1 Archive: _
[ ] 2 Day [ ] 3 Day [ ] 4 Day ( ] 5 Day
( I Hold:
(Expedite Charges Apply)
Analysis:
• Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SQ, Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
LABUSI�Wo# : 92569202 nberor
111111111111111111111111
92569202
Container.
' • Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zi ic acetate,
(6) methanol, (7) sodium bisutfate, (8) sodium thiasulfate, (9) hexane, (A) ascorbic acid, (8) ammonium ulfate,
(C) ammonium hydroxide, (D) TSP. (U) Unpreserved, (0) Other
AnalvseS Lab Profile/tine-
Comp / Collected (or Res M of S
Customer Sample ID Matrix ` Grab Composite Start) Composite End Cl Ctns
c
Date I Time Date I Time
-au Jattlt]1C —celpt In
x11St:
Custody Seals Present/
ntact YC�?NA
Custody Signatures Pr c
•ent ,y.'N NA
Collector Signature P
sent `N NA
Bottles Intact
L:N NA
Correct Bottles
!Y, -N NA
Sufficient Volume
:Y,N NA
Samples Received on i
Y-N NA
VOA - Headspace Accept
ble Y N„UA-'
USDA Regulated Soils
Y N tLw
Samples in Holding Tim.
Y..N NA
Residual Chlorine Pres
nt Y N NA
Cl Strips:
-
Sample pN Acceptable
_
N ta".
pH Strips:
Sulfide Present
Y N NA
Lead Acetate Strips:
.
r_
LTui USE ONLY:
Lab Sample N / Comment;:
h`4Lti L o,-, I -SLy I i.I ke I I 1 [4 1 1 1 '>' I k I I I I I I I Y I I
Customer Remarks / Special Conditions / Possible Hazards:
Type of Ice Used:
Wet Blue Dry None
Packing Material bled:
Radchem sample(s) screened (<500 cpm): Y N f A
Relinqu' d by/Co
any:(Signature)
Date/Time:
-20240
Received by/Company:(Signaturer
linquishe.,%by/Co
pa^ng: (Signature)
Date/TJ1i�me.
R� J
Received b)t�Company: (Signature)
N
LL 2�
L
linqui ed by/Company:(Signature)
Date/Time:
Received by/Company:(Signature)
SHORT HOLDS PRESENT (<72 hours): Y,I - N,,-,' N/A
Lab Tracking It:
6392
iamples received
via:
FEDEX UPS Client Courier t Pace Courier'
Date/Time:
MTJL LAB USE ONLY
�7
Table It:
Pale /Time:
Acctnum:
�] (
b/11-% , ,'
Template:
��
Prelogin:
PM:
Date/Time:
PB:
Lab Sample Tempeu cure Info:
Temp Blank Rece ed: Y NA
Therm ID#: c
Cooler 1 Temp Ul on Receipt:
Cooler 1 Therm rr. Factor: T
Cooler 1 Correct Temp: 7,_
Comments:
Trip Blank Receive : Y N NA
HCL McOH TSP Other
Non Conformance( ): page
YES / NO of:--

Appendix J
Analytical Results

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 10, 2021
Mr. Rick Harmon
Harmon Environmental
615 Bruce Thomas Road
Monroe, NC 28112
RE: Project: 896-01
Pace Project No.: 92569202
Dear Mr. Harmon:
Enclosed are the analytical results for sample(s) received by the laboratory on October 27, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 63

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 896-01
Pace Project No.: 92569202
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
896-01
92569202
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92569202001
BOT 1 (6)
EPA 8015C Modified
AP2
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
SW-846
KDF
1
PASI-C
92569202002
BOT 2 (14)
MADEP EPH
AEG
8
PAN
MADEP VPH
CL
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92569202003
SW (9)
MADEP EPH
AEG
8
PAN
MADEP VPH
CL
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
92569202004
EW (11)
MADEP EPH
AEG
8
PAN
MADEP VPH
CL
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
92569202005
NW (9)
MADEP EPH
AEG
8
PAN
MADEP VPH
CL
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
92569202006
WW (8)
MADEP EPH
AEG
8
PAN
MADEP VPH
CL
5
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
CL
70
PASI-C
SW-846
KDF
1
PASI-C
SM 2540G
CMK
1
PAN
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: 896-01
Pace Project No.: 92569202
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92569202001
BOT 1 (6)
EPA 8015C Modified
Diesel Range Organics(C10-C28)
10100
mg/kg
183
10/29/21 12:36
EPA 8015C Modified
Gas Range Organics (C6-C10)
224
mg/kg
11.7
10/30/21 02:07
SW-846
Percent Moisture
31.8
%
0.10
10/28/21 15:52
N2
92569202002
BOT 2 (14)
SW-846
Percent Moisture
22.4
%
0.10
10/28/21 15:52
N2
SM 2540G
Total Solids
78.8
%
11/01/21 15:56
92569202003
SW (9)
SW-846
Percent Moisture
30.0
%
0.10
10/28/21 15:52
N2
SM 2540G
Total Solids
71.8
%
11/01/21 15:56
92569202004
EW (11)
SW-846
Percent Moisture
27.8
%
0.10
10/28/21 15:52
N2
SM 2540G
Total Solids
73.0
%
11/02/21 09:51
92569202005
NW (9)
SW-846
Percent Moisture
31.5
%
0.10
10/28/21 15:52
N2
SM 2540G
Total Solids
68.9
%
11/02/21 09:51
92569202006
WW (8)
SW-846
Percent Moisture
19.2
%
0.10
10/28/21 15:52
N2
SM 2540G
Total Solids
81.3
%
11/02/21 09:51
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Date: November 10, 2021
NW (9) (Lab ID: 92569202005)
• TPH by Method MADEPE - Dilution due to matrix impact during extraction procedure
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: MADEP EPH
Description: TPH by Method MADEPE
Client: Harmon Environmental
Date: November 10, 2021
General Information:
5 samples were analyzed for MADEP EPH by Pace National Mt. Juliet. All samples were received in acceptable condition with any
exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this
report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 1768646
E: Analyte concentration exceeded the calibration range. The reported result is estimated.
• MS (Lab ID: R3727687-7)
• Aliphatic (C09-C18)
• MSD (Lab ID: R3727687-8)
• Aliphatic (C09-C18)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Harmon Environmental
Date: November 10, 2021
General Information:
1 sample was analyzed for EPA 8015C Modified by Pace Analytical Services Charlotte. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 656006
SO: Surrogate recovery outside laboratory control limits.
- DUP (Lab ID: 3439083)
- n-Pentacosane (S)
S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-
analysis).
- MS (Lab ID: 3439082)
- n-Pentacosane (S)
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
- BOT 1 (6) (Lab ID: 92569202001)
- n-Pentacosane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Harmon Environmental
Date: November 10, 2021
Additional Comments:
PROJECT NARRATIVE
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8015C Modified
Description: Gasoline Range Organics
Client: Harmon Environmental
Date: November 10, 2021
General Information:
1 sample was analyzed for EPA 8015C Modified by Pace Analytical Services Charlotte. All samples were received in acceptable
condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached
at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 655959
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• BOT 1 (6) (Lab ID: 92569202001)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: MADEP VPH
Description: VPH NC Soil
Client: Harmon Environmental
Date: November 10, 2021
General Information:
5 samples were analyzed for MADEP VPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end
of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP VPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 10 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Harmon Environmental
Date: November 10, 2021
General Information:
5 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 655833
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3438174)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• BOT 2 (14) (Lab ID: 92569202002)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• DUP (Lab ID: 3438177)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• EW (11) (Lab ID: 92569202004)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• LCS (Lab ID: 3438175)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• MS (Lab ID: 3438176)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• NW (9) (Lab ID: 92569202005)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• SW (9) (Lab ID: 92569202003)
• 2,4-Dinitrophenol
• 4,6-Dinitro-2-methyl phenol
• WW (8) (Lab ID: 92569202006)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Harmon Environmental
Date: November 10, 2021
QC Batch: 655833
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• 2,4-Dinitrophenol
• Hexachloro-1,3-butadiene
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 12 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Harmon Environmental
Date: November 10, 2021
General Information:
5 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of
this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
QC Batch: 655937
IK: The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be
considered an estimated value.
• BLANK (Lab ID: 3438825)
• Bromomethane
• BOT 2 (14) (Lab ID: 92569202002)
• Bromomethane
• DUP (Lab ID: 3438827)
• Bromomethane
• EW (11) (Lab ID: 92569202004)
• Bromomethane
• LCS (Lab ID: 3438826)
• Bromomethane
• MS (Lab ID: 3438828)
• Bromomethane
- NW (9) (Lab ID: 92569202005)
• Bromomethane
• SW (9) (Lab ID: 92569202003)
• Bromomethane
• WW (8) (Lab ID: 92569202006)
• Bromomethane
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 13 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: EPA 8260D
Description: 8260D/5035A/5030B Volatiles
Client: Harmon Environmental
Date: November 10, 2021
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 14 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 896-01
Pace Project No.: 92569202
Method: SM 2540G
Description: Total Solids 2540 G-2011
Client: Harmon Environmental
Date: November 10, 2021
General Information:
5 samples were analyzed for SM 2540G by Pace National Mt. Juliet. All samples were received in acceptable condition with any
exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this
report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 15 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: BOT 1 (6) Lab ID: 92569202001 Collected: 10/26/21 08:35 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
Diesel Range Organics(C10-C28)
10100 mg/kg 183 25 10/28/21 15:25
10/29/21 12:36
Surrogates
n-Pentacosane (S)
0 % 32-130 25 10/28/21 15:25
10/29/21 12:36 629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gas Range Organics (C6-C10)
224 mg/kg 11.7 1 10/28/21 15:58
10/30/21 02:07
Surrogates
4-Bromofluorobenzene (S)
182 % 66-131 1 10/28/21 15:58
10/30/21 02:07 460-00-4 S5
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
31.8 % 0.10 1
10/28/21 15:52 N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: BOT 2 (14) Lab ID: 92569202002 Collected: 10/26/21 09:20 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
TPH by Method MADEPE
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Total Extractable Hydrocarbons
Surrogates
o-Terphenyl(S)
1-Chloro-octadecane (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-CO8)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
ND
mg/kg
8.25
1
11/03/2109:23
11/06/2112:12
ND
mg/kg
8.25
1
11/03/2109:23
11/06/2112:12
ND
mg/kg
8.25
1
11/03/2109:23
11/06/2120:19
ND
mg/kg
8.25
1
11/03/2109:23
11/06/2112:12
TPH-TEH
51.1
%
40.0-140
1
11/03/2109:23
11/06/2120:19
84-15-1
64.5
%
40.0-140
1
11/03/2109:23
11/06/2112:12
3386-33-2
68.9
%
40.0-140
1
11/03/2109:23
11/06/2120:19
321-60-8
68.5
%
40.0-140
1
11/03/2109:23
11/06/2120:19
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
Pace Analytical
Services - Charlotte
ND
mg/kg
3.8
1
10/28/21 13:52
10/28/21 15:42
ND
mg/kg
3.8
1
10/28/21 13:52
10/28/21 15:42
ND
mg/kg
3.8
1
10/28/21 13:52
10/28/21 15:42
99
%
70-130
1
10/28/21 13:52
10/28/21 15:42
460-00-4
99
%
70-130
1
10/28/21 13:52
10/28/21 15:42
460-00-4
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
83-32-9
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
208-96-8
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
62-53-3
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
120-12-7
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
56-55-3
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
50-32-8
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
205-99-2
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
191-24-2
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
207-08-9
ND
ug/kg
2110
1
10/28/2115:17
10/29/2118:44
65-85-0
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
100-51-6
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
101-55-3
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
85-68-7
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
59-50-7
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
106-47-8
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
111-91-1
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
111-44-4
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
91-58-7
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
95-57-8
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
7005-72-3
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
218-01-9
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
53-70-3
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
132-64-9
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: BOT 2 (14) Lab ID: 92569202002 Collected: 10/26/21 09:20 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
91-94-1
2,4-Dichlorophenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
120-83-2
Diethylphthalate
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
84-66-2
2,4-Dimethylphenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
105-67-9
Dimethylphthalate
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
131-11-3
Di-n-butylphthalate
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2110
1
10/28/2115:17
10/29/2118:44
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
606-20-2
Di-n-octylphthalate
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
117-81-7
Fluoranthene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
206-44-0
Fluorene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
87-68-3
Hexachlorobenzene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
77-47-4
Hexachloroethane
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
193-39-5
Isophorone
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
78-59-1
1-Methylnaphthalene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
90-12-0
2-Methylnaphthalene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
422
1
10/28/21 15:17
10/29/21 18:44
15831-10-4
Naphthalene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
91-20-3
2-Nitroaniline
ND
ug/kg
2110
1
10/28/2115:17
10/29/2118:44
88-74-4
3-Nitroaniline
ND
ug/kg
2110
1
10/28/2115:17
10/29/2118:44
99-09-2
4-Nitroaniline
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
100-01-6
Nitrobenzene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
98-95-3
2-Nitrophenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
88-75-5
4-Nitrophenol
ND
ug/kg
2110
1
10/28/2115:17
10/29/2118:44
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
108-60-1
Pentachlorophenol
ND
ug/kg
845
1
10/28/2115:17
10/29/2118:44
87-86-5
Phenanthrene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
85-01-8
Phenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
108-95-2
Pyrene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
129-00-0
Pyridine
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
422
1
10/28/2115:17
10/29/2118:44
88-06-2
REPORT OF LABORATORY ANALYSIS
IL
IL
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: BOT 2 (14) Lab ID: 92569202002 Collected: 10/26/21 09:20 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
35
%
21-130
1
10/28/21 15:17
10/29/21 18:44
4165-60-0
2-Fluorobiphenyl (S)
35
%
19-130
1
10/28/21 15:17
10/29/21 18:44
321-60-8
Terphenyl-d14 (S)
46
%
15-130
1
10/28/21 15:17
10/29/21 18:44
1718-51-0
Phenol-d6 (S)
36
%
18-130
1
10/28/21 15:17
10/29/21 18:44
13127-88-3
2-Fluorophenol (S)
34
%
18-130
1
10/28/21 15:17
10/29/21 18:44
367-12-4
2,4,6-Tribromophenol (S)
36
%
18-130
1
10/28/21 15:17
10/29/21 18:44
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
155
1
10/28/21 13:24
10/28/21 17:02
67-64-1
Benzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
71-43-2
Bromobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
108-86-1
Bromochloromethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
74-97-5
Bromodichloromethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
75-27-4
Bromoform
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
75-25-2
Bromomethane
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
74-83-9
2-Butanone (MEK)
ND
ug/kg
155
1
10/28/21 13:24
10/28/21 17:02
78-93-3
n-Butylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
104-51-8
sec-Butylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
135-98-8
tert-Butyl benzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
98-06-6
Carbon tetrachloride
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
56-23-5
Chlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
108-90-7
Chloroethane
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
75-00-3
Chloroform
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
67-66-3
Chloromethane
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
74-87-3
2-Chlorotoluene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
95-49-8
4-Chlorotoluene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
96-12-8
Dibromochloromethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
106-93-4
Dibromomethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: BOT 2 (14) Lab ID: 92569202002 Collected: 10/26/21 09:20 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
10061-02-6
Diisopropyl ether
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
108-20-3
Ethylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
87-68-3
2-Hexanone
ND
ug/kg
77.7
1
10/28/21 13:24
10/28/21 17:02
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
99-87-6
Methylene Chloride
ND
ug/kg
31.1
1
10/28/21 13:24
10/28/21 17:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
77.7
1
10/28/21 13:24
10/28/21 17:02
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
1634-04-4
Naphthalene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
91-20-3
n-Propylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
103-65-1
Styrene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
79-34-5
Tetrachloroethene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
127-18-4
Toluene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
79-00-5
Trichloroethene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
108-67-8
Vinyl acetate
ND
ug/kg
77.7
1
10/28/21 13:24
10/28/21 17:02
108-05-4
Vinyl chloride
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
75-01-4
Xylene (Total)
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
1330-20-7
m&p-Xylene
ND
ug/kg
15.5
1
10/28/21 13:24
10/28/21 17:02
179601-23-1
o-Xylene
ND
ug/kg
7.8
1
10/28/21 13:24
10/28/21 17:02
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
10/28/21 13:24
10/28/21 17:02
2037-26-5
4-Bromofluorobenzene (S)
100
%
69-134
1
10/28/21 13:24
10/28/21 17:02
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
10/28/21 13:24
10/28/21 17:02
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
22.4
%
0.10
1
10/28/21 15:52
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
78.8
%
1
11/01/21 15:50
11/01/21 15:56
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /10/2021 04:50 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 20 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: SW (9) Lab ID: 92569202003 Collected: 10/26/21 09:30 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
TPH by Method MADEPE
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Total Extractable Hydrocarbons
Surrogates
o-Terphenyl(S)
1-Chloro-octadecane (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-008)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
ND
mg/kg
9.06
1
11/03/2109:23
11/06/2112:34
ND
mg/kg
9.06
1
11/03/2109:23
11/06/2112:34
ND
mg/kg
9.06
1
11/03/2109:23
11/06/2120:41
ND
mg/kg
9.06
1
11/03/2109:23
11/06/2112:34
TPH-TEH
46.2
%
40.0-140
1
11/03/2109:23
11/06/2120:41
84-15-1
52.3
%
40.0-140
1
11/03/2109:23
11/06/2112:34
3386-33-2
78.9
%
40.0-140
1
11/03/2109:23
11/06/2120:41
321-60-8
78.4
%
40.0-140
1
11/03/2109:23
11/06/2120:41
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
Pace Analytical
Services - Charlotte
ND
mg/kg
4.6
1
10/28/2113:52
10/28/2116:11
ND
mg/kg
4.6
1
10/28/2113:52
10/28/2116:11
ND
mg/kg
4.6
1
10/28/2113:52
10/28/2116:11
100
%
70-130
1
10/28/2113:52
10/28/2116:11
460-00-4
99
%
70-130
1
10/28/2113:52
10/28/2116:11
460-00-4
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
83-32-9
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
208-96-8
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
62-53-3
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
120-12-7
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
56-55-3
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
50-32-8
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
205-99-2
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
191-24-2
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
207-08-9
ND
ug/kg
2370
1
10/28/2115:17
10/29/2119:15
65-85-0
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
100-51-6
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
101-55-3
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
85-68-7
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
59-50-7
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
106-47-8
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
111-91-1
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
111-44-4
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
91-58-7
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
95-57-8
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
7005-72-3
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
218-01-9
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
53-70-3
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
132-64-9
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: SW (9) Lab ID: 92569202003 Collected: 10/26/21 09:30 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
91-94-1
2,4-Dichlorophenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
120-83-2
Diethylphthalate
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
84-66-2
2,4-Dimethylphenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
105-67-9
Dimethylphthalate
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
131-11-3
Di-n-butylphthalate
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2370
1
10/28/2115:17
10/29/2119:15
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
606-20-2
Di-n-octylphthalate
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
117-81-7
Fluoranthene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
206-44-0
Fluorene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
87-68-3
Hexachlorobenzene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
77-47-4
Hexachloroethane
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
193-39-5
Isophorone
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
78-59-1
1-Methylnaphthalene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
90-12-0
2-Methylnaphthalene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
474
1
10/28/21 15:17
10/29/21 19:15
15831-10-4
Naphthalene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
91-20-3
2-Nitroaniline
ND
ug/kg
2370
1
10/28/2115:17
10/29/2119:15
88-74-4
3-Nitroaniline
ND
ug/kg
2370
1
10/28/2115:17
10/29/2119:15
99-09-2
4-Nitroaniline
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
100-01-6
Nitrobenzene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
98-95-3
2-Nitrophenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
88-75-5
4-Nitrophenol
ND
ug/kg
2370
1
10/28/2115:17
10/29/2119:15
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
108-60-1
Pentachlorophenol
ND
ug/kg
949
1
10/28/2115:17
10/29/2119:15
87-86-5
Phenanthrene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
85-01-8
Phenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
108-95-2
Pyrene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
129-00-0
Pyridine
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
474
1
10/28/2115:17
10/29/2119:15
88-06-2
REPORT OF LABORATORY ANALYSIS
IL
IL
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: SW (9) Lab ID: 92569202003 Collected: 10/26/21 09:30 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
40
%
21-130
1
10/28/21 15:17
10/29/21 19:15
4165-60-0
2-Fluorobiphenyl (S)
38
%
19-130
1
10/28/21 15:17
10/29/21 19:15
321-60-8
Terphenyl-d14 (S)
44
%
15-130
1
10/28/21 15:17
10/29/21 19:15
1718-51-0
Phenol-d6 (S)
37
%
18-130
1
10/28/21 15:17
10/29/21 19:15
13127-88-3
2-Fluorophenol (S)
36
%
18-130
1
10/28/21 15:17
10/29/21 19:15
367-12-4
2,4,6-Tribromophenol (S)
38
%
18-130
1
10/28/21 15:17
10/29/21 19:15
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
175
1
10/28/21 13:24
10/28/21 17:20
67-64-1
Benzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
71-43-2
Bromobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
108-86-1
Bromochloromethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
74-97-5
Bromodichloromethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
75-27-4
Bromoform
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
75-25-2
Bromomethane
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
74-83-9
2-Butanone (MEK)
ND
ug/kg
175
1
10/28/21 13:24
10/28/21 17:20
78-93-3
n-Butylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
104-51-8
sec-Butylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
135-98-8
tert-Butyl benzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
98-06-6
Carbon tetrachloride
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
56-23-5
Chlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
108-90-7
Chloroethane
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
75-00-3
Chloroform
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
67-66-3
Chloromethane
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
74-87-3
2-Chlorotoluene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
95-49-8
4-Chlorotoluene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
96-12-8
Dibromochloromethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
106-93-4
Dibromomethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
106-46-7
Dichlorodifluoromethane
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: SW (9) Lab ID: 92569202003 Collected: 10/26/21 09:30 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
10061-02-6
Diisopropyl ether
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
108-20-3
Ethylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
87-68-3
2-Hexanone
ND
ug/kg
87.3
1
10/28/21 13:24
10/28/21 17:20
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
99-87-6
Methylene Chloride
ND
ug/kg
34.9
1
10/28/21 13:24
10/28/21 17:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
87.3
1
10/28/21 13:24
10/28/21 17:20
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
1634-04-4
Naphthalene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
91-20-3
n-Propylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
103-65-1
Styrene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
79-34-5
Tetrachloroethene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
127-18-4
Toluene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
79-00-5
Trichloroethene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
79-01-6
Trichlorofluoromethane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
108-67-8
Vinyl acetate
ND
ug/kg
87.3
1
10/28/21 13:24
10/28/21 17:20
108-05-4
Vinyl chloride
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
75-01-4
Xylene (Total)
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
1330-20-7
m&p-Xylene
ND
ug/kg
17.5
1
10/28/21 13:24
10/28/21 17:20
179601-23-1
o-Xylene
ND
ug/kg
8.7
1
10/28/21 13:24
10/28/21 17:20
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
10/28/21 13:24
10/28/21 17:20
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
10/28/21 13:24
10/28/21 17:20
460-00-4
1,2-Dichloroethane-d4 (S)
107
%
70-130
1
10/28/21 13:24
10/28/21 17:20
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
30.0
%
0.10
1
10/28/21 15:52
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
71.8
%
1
11/01/21 15:50
11/01/21 15:56
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /10/2021 04:50 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 24 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: EW (11) Lab ID: 92569202004 Collected: 10/26/21 09:36 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
TPH by Method MADEPE
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Total Extractable Hydrocarbons
Surrogates
o-Terphenyl(S)
1-Chloro-octadecane (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-008)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
ND
mg/kg
8.90
1
11/03/2109:23
11/06/2112:56
ND
mg/kg
8.90
1
11/03/2109:23
11/06/2112:56
ND
mg/kg
8.90
1
11/03/2109:23
11/06/2121:03
ND
mg/kg
8.90
1
11/03/2109:23
11/06/2121:03
TPH-TEH
51.2
%
40.0-140
1
11/03/2109:23
11/06/2121:03
84-15-1
63.3
%
40.0-140
1
11/03/2109:23
11/06/2112:56
3386-33-2
72.5
%
40.0-140
1
11/03/2109:23
11/06/2121:03
321-60-8
72.1
%
40.0-140
1
11/03/2109:23
11/06/2121:03
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
Pace Analytical
Services - Charlotte
ND
mg/kg
4.4
1
10/28/21 13:52
10/28/21 16:39
ND
mg/kg
4.4
1
10/28/21 13:52
10/28/21 16:39
ND
mg/kg
4.4
1
10/28/21 13:52
10/28/21 16:39
96
%
70-130
1
10/28/21 13:52
10/28/21 16:39
460-00-4
99
%
70-130
1
10/28/21 13:52
10/28/21 16:39
460-00-4
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
83-32-9
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
208-96-8
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
62-53-3
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
120-12-7
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
56-55-3
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
50-32-8
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
205-99-2
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
191-24-2
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
207-08-9
ND
ug/kg
2310
1
10/28/2115:17
10/29/2119:46
65-85-0
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
100-51-6
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
101-55-3
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
85-68-7
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
59-50-7
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
106-47-8
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
111-91-1
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
111-44-4
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
91-58-7
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
95-57-8
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
7005-72-3
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
218-01-9
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
53-70-3
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
132-64-9
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: EW (11) Lab ID: 92569202004 Collected: 10/26/21 09:36 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
91-94-1
2,4-Dichlorophenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
120-83-2
Diethylphthalate
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
84-66-2
2,4-Dimethylphenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
105-67-9
Dimethylphthalate
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
131-11-3
Di-n-butylphthalate
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2310
1
10/28/2115:17
10/29/2119:46
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
606-20-2
Di-n-octylphthalate
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
117-81-7
Fluoranthene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
206-44-0
Fluorene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
87-68-3
Hexachlorobenzene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
77-47-4
Hexachloroethane
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
193-39-5
Isophorone
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
78-59-1
1-Methylnaphthalene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
90-12-0
2-Methylnaphthalene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
462
1
10/28/21 15:17
10/29/21 19:46
15831-10-4
Naphthalene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
91-20-3
2-Nitroaniline
ND
ug/kg
2310
1
10/28/2115:17
10/29/2119:46
88-74-4
3-Nitroaniline
ND
ug/kg
2310
1
10/28/2115:17
10/29/2119:46
99-09-2
4-Nitroaniline
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
100-01-6
Nitrobenzene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
98-95-3
2-Nitrophenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
88-75-5
4-Nitrophenol
ND
ug/kg
2310
1
10/28/2115:17
10/29/2119:46
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
108-60-1
Pentachlorophenol
ND
ug/kg
923
1
10/28/2115:17
10/29/2119:46
87-86-5
Phenanthrene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
85-01-8
Phenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
108-95-2
Pyrene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
129-00-0
Pyridine
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
462
1
10/28/2115:17
10/29/2119:46
88-06-2
REPORT OF LABORATORY ANALYSIS
IL
IL
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: EW (11) Lab ID: 92569202004 Collected: 10/26/21 09:36 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
47
%
21-130
1
10/28/21 15:17
10/29/21 19:46
4165-60-0
2-Fluorobiphenyl (S)
47
%
19-130
1
10/28/21 15:17
10/29/21 19:46
321-60-8
Terphenyl-d14 (S)
49
%
15-130
1
10/28/21 15:17
10/29/21 19:46
1718-51-0
Phenol-d6 (S)
46
%
18-130
1
10/28/21 15:17
10/29/21 19:46
13127-88-3
2-Fluorophenol (S)
45
%
18-130
1
10/28/21 15:17
10/29/21 19:46
367-12-4
2,4,6-Tribromophenol (S)
48
%
18-130
1
10/28/21 15:17
10/29/21 19:46
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
177
1
10/28/21 13:24
10/28/21 17:39
67-64-1
Benzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
71-43-2
Bromobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
108-86-1
Bromochloromethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
74-97-5
Bromodichloromethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
75-27-4
Bromoform
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
75-25-2
Bromomethane
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
74-83-9
2-Butanone (MEK)
ND
ug/kg
177
1
10/28/21 13:24
10/28/21 17:39
78-93-3
n-Butylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
104-51-8
sec-Butylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
135-98-8
tert-Butyl benzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
98-06-6
Carbon tetrachloride
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
56-23-5
Chlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
108-90-7
Chloroethane
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
75-00-3
Chloroform
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
67-66-3
Chloromethane
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
74-87-3
2-Chlorotoluene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
95-49-8
4-Chlorotoluene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
96-12-8
Dibromochloromethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
106-93-4
Dibromomethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
106-46-7
Dichlorodifluoromethane
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: EW (11) Lab ID: 92569202004 Collected: 10/26/21 09:36 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
10061-02-6
Diisopropyl ether
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
108-20-3
Ethylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
87-68-3
2-Hexanone
ND
ug/kg
88.5
1
10/28/21 13:24
10/28/21 17:39
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
99-87-6
Methylene Chloride
ND
ug/kg
35.4
1
10/28/21 13:24
10/28/21 17:39
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
88.5
1
10/28/21 13:24
10/28/21 17:39
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
1634-04-4
Naphthalene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
91-20-3
n-Propylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
103-65-1
Styrene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
79-34-5
Tetrachloroethene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
127-18-4
Toluene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
79-00-5
Trichloroethene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
79-01-6
Trichlorofluoromethane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
108-67-8
Vinyl acetate
ND
ug/kg
88.5
1
10/28/21 13:24
10/28/21 17:39
108-05-4
Vinyl chloride
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
75-01-4
Xylene (Total)
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
1330-20-7
m&p-Xylene
ND
ug/kg
17.7
1
10/28/21 13:24
10/28/21 17:39
179601-23-1
o-Xylene
ND
ug/kg
8.9
1
10/28/21 13:24
10/28/21 17:39
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
10/28/21 13:24
10/28/21 17:39
2037-26-5
4-Bromofluorobenzene (S)
99
%
69-134
1
10/28/21 13:24
10/28/21 17:39
460-00-4
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
10/28/21 13:24
10/28/21 17:39
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
27.8
%
0.10
1
10/28/21 15:52
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
73.0
%
1
11/02/21 09:43
11/02/21 09:51
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /10/2021 04:50 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 28 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: NW (9) Lab ID: 92569202005 Collected: 10/26/21 09:40 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
TPH by Method MADEPE
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Total Extractable Hydrocarbons
Surrogates
o-Terphenyl(S)
1-Chloro-octadecane (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-008)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
ND
mg/kg
26.6
2.81
11/03/2109:23
11/06/2113:18
ND
mg/kg
26.6
2.81
11/03/2109:23
11/06/2113:18
ND
mg/kg
26.6
2.81
11/03/2109:23
11/06/2121:25
ND
mg/kg
26.6
2.81
11/03/2109:23
11/06/2113:18
TPH-TEH
57.6
%
40.0-140
2.81
11/03/2109:23
11/06/2121:25
84-15-1
61.3
%
40.0-140
2.81
11/03/2109:23
11/06/2113:18
3386-33-2
80.0
%
40.0-140
2.81
11/03/2109:23
11/06/2121:25
321-60-8
79.3
%
40.0-140
2.81
11/03/2109:23
11/06/2121:25
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
Pace Analytical
Services - Charlotte
ND
mg/kg
4.9
1
10/28/21 13:52
10/28/21 17:07
ND
mg/kg
4.9
1
10/28/21 13:52
10/28/21 17:07
ND
mg/kg
4.9
1
10/28/21 13:52
10/28/21 17:07
97
%
70-130
1
10/28/21 13:52
10/28/21 17:07
460-00-4
96
%
70-130
1
10/28/21 13:52
10/28/21 17:07
460-00-4
Analytical Method: EPA 8270E Preparation Method: EPA
3546
Pace Analytical
Services - Charlotte
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
83-32-9
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
208-96-8
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
62-53-3
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
120-12-7
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
56-55-3
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
50-32-8
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
205-99-2
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
191-24-2
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
207-08-9
ND
ug/kg
2410
1
10/28/2115:17
10/29/2120:16
65-85-0
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
100-51-6
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
101-55-3
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
85-68-7
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
59-50-7
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
106-47-8
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
111-91-1
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
111-44-4
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
91-58-7
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
95-57-8
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
7005-72-3
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
218-01-9
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
53-70-3
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
132-64-9
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: NW (9) Lab ID: 92569202005 Collected: 10/26/21 09:40 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
91-94-1
2,4-Dichlorophenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
120-83-2
Diethylphthalate
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
84-66-2
2,4-Dimethylphenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
105-67-9
Dimethylphthalate
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
131-11-3
Di-n-butylphthalate
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2410
1
10/28/2115:17
10/29/2120:16
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
606-20-2
Di-n-octylphthalate
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
117-81-7
Fluoranthene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
206-44-0
Fluorene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
87-68-3
Hexachlorobenzene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
77-47-4
Hexachloroethane
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
193-39-5
Isophorone
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
78-59-1
1-Methylnaphthalene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
90-12-0
2-Methylnaphthalene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
482
1
10/28/21 15:17
10/29/21 20:16
15831-10-4
Naphthalene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
91-20-3
2-Nitroaniline
ND
ug/kg
2410
1
10/28/2115:17
10/29/2120:16
88-74-4
3-Nitroaniline
ND
ug/kg
2410
1
10/28/2115:17
10/29/2120:16
99-09-2
4-Nitroaniline
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
100-01-6
Nitrobenzene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
98-95-3
2-Nitrophenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
88-75-5
4-Nitrophenol
ND
ug/kg
2410
1
10/28/2115:17
10/29/2120:16
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
108-60-1
Pentachlorophenol
ND
ug/kg
964
1
10/28/2115:17
10/29/2120:16
87-86-5
Phenanthrene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
85-01-8
Phenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
108-95-2
Pyrene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
129-00-0
Pyridine
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
482
1
10/28/2115:17
10/29/2120:16
88-06-2
REPORT OF LABORATORY ANALYSIS
IL
IL
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: NW (9) Lab ID: 92569202005 Collected: 10/26/21 09:40 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
48
%
21-130
1
10/28/21 15:17
10/29/21 20:16
4165-60-0
2-Fluorobiphenyl (S)
47
%
19-130
1
10/28/21 15:17
10/29/21 20:16
321-60-8
Terphenyl-d14 (S)
46
%
15-130
1
10/28/21 15:17
10/29/21 20:16
1718-51-0
Phenol-d6 (S)
46
%
18-130
1
10/28/21 15:17
10/29/21 20:16
13127-88-3
2-Fluorophenol (S)
45
%
18-130
1
10/28/21 15:17
10/29/21 20:16
367-12-4
2,4,6-Tribromophenol (S)
46
%
18-130
1
10/28/21 15:17
10/29/21 20:16
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
200
1
10/28/21 13:24
10/28/21 17:57
67-64-1
Benzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
71-43-2
Bromobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
108-86-1
Bromochloromethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
74-97-5
Bromodichloromethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
75-27-4
Bromoform
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
75-25-2
Bromomethane
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
74-83-9
2-Butanone (MEK)
ND
ug/kg
200
1
10/28/21 13:24
10/28/21 17:57
78-93-3
n-Butylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
104-51-8
sec-Butylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
135-98-8
tert-Butyl benzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
98-06-6
Carbon tetrachloride
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
56-23-5
Chlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
108-90-7
Chloroethane
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
75-00-3
Chloroform
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
67-66-3
Chloromethane
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
74-87-3
2-Chlorotoluene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
95-49-8
4-Chlorotoluene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
96-12-8
Dibromochloromethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
106-93-4
Dibromomethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
106-46-7
Dichlorodifluoromethane
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
75-71-8
1,1-Dichloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
75-34-3
1,2-Dichloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
107-06-2
1,1-Dichloroethene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
156-60-5
1,2-Dichloropropane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
78-87-5
1,3-Dichloropropane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
142-28-9
2,2-Dichloropropane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
594-20-7
1,1-Dichloropropene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: NW (9) Lab ID: 92569202005 Collected: 10/26/21 09:40 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
10061-02-6
Diisopropyl ether
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
108-20-3
Ethylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
87-68-3
2-Hexanone
ND
ug/kg
100
1
10/28/21 13:24
10/28/21 17:57
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
98-82-8
p-Isopropyltoluene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
99-87-6
Methylene Chloride
ND
ug/kg
40.1
1
10/28/21 13:24
10/28/21 17:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
100
1
10/28/21 13:24
10/28/21 17:57
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
1634-04-4
Naphthalene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
91-20-3
n-Propylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
103-65-1
Styrene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
79-34-5
Tetrachloroethene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
127-18-4
Toluene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
79-00-5
Trichloroethene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
79-01-6
Trichlorofluoromethane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
108-67-8
Vinyl acetate
ND
ug/kg
100
1
10/28/21 13:24
10/28/21 17:57
108-05-4
Vinyl chloride
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
75-01-4
Xylene (Total)
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
1330-20-7
m&p-Xylene
ND
ug/kg
20.0
1
10/28/21 13:24
10/28/21 17:57
179601-23-1
o-Xylene
ND
ug/kg
10.0
1
10/28/21 13:24
10/28/21 17:57
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
10/28/21 13:24
10/28/21 17:57
2037-26-5
4-Bromofluorobenzene (S)
100
%
69-134
1
10/28/21 13:24
10/28/21 17:57
460-00-4
1,2-Dichloroethane-d4 (S)
106
%
70-130
1
10/28/21 13:24
10/28/21 17:57
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
31.5
%
0.10
1
10/28/21 15:52
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
68.9
%
1
11/02/21 09:43
11/02/21 09:51
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /10/2021 04:50 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 32 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: WW (8) Lab ID: 92569202006 Collected: 10/26/21 10:45 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
TPH by Method MADEPE
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Total Extractable Hydrocarbons
Surrogates
o-Terphenyl(S)
1-Chloro-octadecane (S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
VPH NC Soil
Aliphatic (C05-008)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Surrogates
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
8270E MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methyl phenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
1,2-Dichlorobenzene
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
ND
mg/kg
8.00
1
11/03/2109:23
11/06/2113:40
ND
mg/kg
8.00
1
11/03/2109:23
11/06/2113:40
ND
mg/kg
8.00
1
11/03/2109:23
11/06/2121:47
ND
mg/kg
8.00
1
11/03/2109:23
11/06/2113:40
TPH-TEH
62.5
%
40.0-140
1
11/03/2109:23
11/06/2121:47
84-15-1
71.2
%
40.0-140
1
11/03/2109:23
11/06/2113:40
3386-33-2
77.7
%
40.0-140
1
11/03/2109:23
11/06/2121:47
321-60-8
77.5
%
40.0-140
1
11/03/2109:23
11/06/2121:47
580-13-2
Analytical Method: MADEP VPH Preparation Method:
MADEP VPH
Pace Analytical
Services - Charlotte
ND
mg/kg
3.7
1
10/28/21 13:52
10/28/21 17:36
ND
mg/kg
3.7
1
10/28/21 13:52
10/28/21 17:36
ND
mg/kg
3.7
1
10/28/21 13:52
10/28/21 17:36
100
%
70-130
1
10/28/21 13:52
10/28/21 17:36
460-00-4
99
%
70-130
1
10/28/21 13:52
10/28/21 17:36
460-00-4
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
83-32-9
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
208-96-8
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
62-53-3
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
120-12-7
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
56-55-3
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
50-32-8
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
205-99-2
ND
ug/kg
412
1
10/28/21 15:17
11 /01 /21 06:31
191-24-2
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
207-08-9
ND
ug/kg
2060
1
10/28/21 15:17
11/01/2106:31
65-85-0
ND
ug/kg
825
1
10/28/21 15:17
11 /01 /21 06:31
100-51-6
ND
ug/kg
412
1
10/28/21 15:17
11 /01 /21 06:31
101-55-3
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
85-68-7
ND
ug/kg
825
1
10/28/21 15:17
11/01/2106:31
59-50-7
ND
ug/kg
825
1
10/28/21 15:17
11/01/2106:31
106-47-8
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
111-91-1
ND
ug/kg
412
1
10/28/21 15:17
11 /01 /21 06:31
111-44-4
ND
ug/kg
412
1
10/28/21 15:17
11 /01 /21 06:31
91-58-7
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
95-57-8
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
7005-72-3
ND
ug/kg
412
1
10/28/21 15:17
11 /01 /21 06:31
218-01-9
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
53-70-3
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
132-64-9
ND
ug/kg
412
1
10/28/21 15:17
11/01/2106:31
95-50-1
REPORT OF LABORATORY ANALYSIS
N2
N2
N2
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: WW (8) Lab ID: 92569202006 Collected: 10/26/21 10:45 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
1,3-Dichlorobenzene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
825
1
10/28/2115:17
11/01/2106:31
91-94-1
2,4-Dichlorophenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
120-83-2
Diethylphthalate
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
84-66-2
2,4-Dimethylphenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
105-67-9
Dimethylphthalate
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
131-11-3
Di-n-butylphthalate
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
825
1
10/28/2115:17
11/01/2106:31
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2060
1
10/28/2115:17
11/01/2106:31
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
606-20-2
Di-n-octylphthalate
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
117-81-7
Fluoranthene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
206-44-0
Fluorene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
87-68-3
Hexachlorobenzene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
77-47-4
Hexachloroethane
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
193-39-5
Isophorone
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
78-59-1
1-Methylnaphthalene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
90-12-0
2-Methylnaphthalene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
412
1
10/28/21 15:17
11/01/21 06:31
15831-10-4
Naphthalene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
91-20-3
2-Nitroaniline
ND
ug/kg
2060
1
10/28/2115:17
11/01/2106:31
88-74-4
3-Nitroaniline
ND
ug/kg
2060
1
10/28/2115:17
11/01/2106:31
99-09-2
4-Nitroaniline
ND
ug/kg
825
1
10/28/2115:17
11/01/2106:31
100-01-6
Nitrobenzene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
98-95-3
2-Nitrophenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
88-75-5
4-Nitrophenol
ND
ug/kg
2060
1
10/28/2115:17
11/01/2106:31
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
108-60-1
Pentachlorophenol
ND
ug/kg
825
1
10/28/2115:17
11/01/2106:31
87-86-5
Phenanthrene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
85-01-8
Phenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
108-95-2
Pyrene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
129-00-0
Pyridine
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
412
1
10/28/2115:17
11/01/2106:31
88-06-2
REPORT OF LABORATORY ANALYSIS
IL
v1
v1
IL
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: WW (8) Lab ID: 92569202006 Collected: 10/26/21 10:45 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical
Services - Charlotte
Surrogates
Nitrobenzene-d5 (S)
35
%
21-130
1
10/28/21 15:17
11/01/21 06:31
4165-60-0
2-Fluorobiphenyl (S)
39
%
19-130
1
10/28/21 15:17
11/01/21 06:31
321-60-8
Terphenyl-d14 (S)
53
%
15-130
1
10/28/21 15:17
11/01/21 06:31
1718-51-0
Phenol-d6 (S)
35
%
18-130
1
10/28/21 15:17
11/01/21 06:31
13127-88-3
2-Fluorophenol (S)
35
%
18-130
1
10/28/21 15:17
11/01/21 06:31
367-12-4
2,4,6-Tribromophenol (S)
40
%
18-130
1
10/28/21 15:17
11/01/21 06:31
118-79-6
8260D/5035A/5030B Volatiles
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical
Services - Charlotte
Acetone
ND
ug/kg
152
1
10/28/21 13:24
10/28/21 18:16
67-64-1
Benzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
71-43-2
Bromobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
108-86-1
Bromochloromethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
74-97-5
Bromodichloromethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
75-27-4
Bromoform
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
75-25-2
Bromomethane
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
74-83-9
2-Butanone (MEK)
ND
ug/kg
152
1
10/28/21 13:24
10/28/21 18:16
78-93-3
n-Butylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
104-51-8
sec-Butylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
135-98-8
tert-Butyl benzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
98-06-6
Carbon tetrachloride
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
56-23-5
Chlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
108-90-7
Chloroethane
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
75-00-3
Chloroform
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
67-66-3
Chloromethane
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
74-87-3
2-Chlorotoluene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
95-49-8
4-Chlorotoluene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
96-12-8
Dibromochloromethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
106-93-4
Dibromomethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
563-58-6
REPORT OF LABORATORY ANALYSIS
IK
Qual
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 896-01
Pace Project No.: 92569202
Sample: WW (8) Lab ID: 92569202006 Collected: 10/26/21 10:45 Received: 10/27/21 12:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A/5030B Volatiles
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
10061-02-6
Diisopropyl ether
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
108-20-3
Ethylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
87-68-3
2-Hexanone
ND
ug/kg
75.8
1
10/28/21 13:24
10/28/21 18:16
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
99-87-6
Methylene Chloride
ND
ug/kg
30.3
1
10/28/21 13:24
10/28/21 18:16
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
75.8
1
10/28/21 13:24
10/28/21 18:16
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
1634-04-4
Naphthalene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
91-20-3
n-Propylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
103-65-1
Styrene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
79-34-5
Tetrachloroethene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
127-18-4
Toluene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
79-00-5
Trichloroethene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
79-01-6
Trichlorofluoromethane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
108-67-8
Vinyl acetate
ND
ug/kg
75.8
1
10/28/21 13:24
10/28/21 18:16
108-05-4
Vinyl chloride
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
75-01-4
Xylene (Total)
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
1330-20-7
m&p-Xylene
ND
ug/kg
15.2
1
10/28/21 13:24
10/28/21 18:16
179601-23-1
o-Xylene
ND
ug/kg
7.6
1
10/28/21 13:24
10/28/21 18:16
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
10/28/21 13:24
10/28/21 18:16
2037-26-5
4-Bromofluorobenzene (S)
100
%
69-134
1
10/28/21 13:24
10/28/21 18:16
460-00-4
1,2-Dichloroethane-d4 (S)
106
%
70-130
1
10/28/21 13:24
10/28/21 18:16
17060-07-0
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
19.2
%
0.10
1
10/28/21 15:52
N2
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids
81.3
%
1
11/02/21 09:43
11/02/21 09:51
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 11 /10/2021 04:50 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 36 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 1768646
Analysis Method: MADEP EPH
QC Batch Method: MA DEP/NJ DEP
Analysis Description: TPH
by Method MADEPE
Laboratory: Pace
National - Mt.
Juliet
Associated Lab Samples: 92569202002, 92569202003,
92569202004, 92569202005, 92569202006
METHOD BLANK: R3727687-1
Matrix: Solid
Associated Lab Samples: 92569202002, 92569202003,
92569202004, 92569202005, 92569202006
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aliphatic (C09-C18)
mg/kg
ND 6.50
11/05/21 11:00
Aliphatic (C19-C36)
mg/kg
ND 6.50
11/05/21 11:00
Total Extractable Hydrocarbons
mg/kg
ND 6.50
11/05/21 11:00
1-Chloro-octadecane (S)
%
73.9 40.0-140
11/05/21 11:00
METHOD BLANK: R3727687-4
Matrix: Solid
Associated Lab Samples: 92569202002, 92569202003,
92569202004, 92569202005, 92569202006
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Aromatic (C11-C22)
mg/kg
ND 6.50
11/05/21 12:13
Total Extractable Hydrocarbons
mg/kg
ND 6.50
11/05/21 12:13
o-Terphenyl (S)
%
70.7 40.0-140
11/05/21 12:13
2-Fluorobiphenyl (S)
%
83.3 40.0-140
11/05/21 12:13
2-Bromonaphthalene (S)
%
82.7 40.0-140
11/05/21 12:13
LABORATORY CONTROL SAMPLE & LCSD:
R3727687-2 R3727687-3
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
39.9 22.6 23.7
56.6 59.4
40.0-140 4.75
25
Aliphatic (C19-C36)
mg/kg
53.2 36.6 37.4
68.8 70.3
40.0-140 2.16
25
1-Chloro-octadecane (S)
%
72.4 74.4
40.0-140
LABORATORY CONTROL SAMPLE & LCSD:
R3727687-5 R3727687-6
Spike LCS LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result
% Rec % Rec
Limits RPD
RPD Qualifiers
Aromatic (C11-C22)
mg/kg
113 76.2 78.4
67.4 69.4
40.0-140 2.85
25
o-Terphenyl (S)
%
64.3 65.8
40.0-140
2-Fluorobiphenyl (S)
%
77.3 79.3
40.0-140
2-Bromonaphthalene (S)
%
77.1 79.1
40.0-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
R3727687-7
R3727687-8
MS
MSD
L1423679-01
Spike
Spike
MS MSD
MS
MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result Result
% Rec
% Rec Limits RPD Qual
Aliphatic (C09-C18)
mg/kg
739
44.6
44.3
749 774
22.7
78.9 40.0-140 3.25 E,P6
Aliphatic (C19-C36)
mg/kg
4.59
59.5
59.0
39.2 33.5
58.2
48.9 40.0-140 15.8
1-Chloro-octadecane (S)
%
68.4
59.2 40.0-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 655959
Analysis Method:
EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description:
Gasoline Range Organics
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202001
METHOD BLANK: 3438907
Matrix: Solid
Associated Lab Samples: 92569202001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
6.0 10/29/21 16:44
4-Bromofluorobenzene (S)
%
87 66-131
10/29/21 16:44
LABORATORY CONTROL SAMPLE:
3438908
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.7 40.2
81 70-130
4-Bromofluorobenzene (S)
%
89 66-131
MATRIX SPIKE SAMPLE:
3438910
92569213001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 88.8
79.2 87
70-145
4-Bromofluorobenzene (S)
%
86
66-131
SAMPLE DUPLICATE: 3438909
92569162035 Dup
Parameter
Units
Result Result
RPD Qualifiers
Gas Range Organics (C6-C10)
mg/kg
2.8J
ND
4-Bromofluorobenzene (S)
%
89
86
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 655957 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
METHOD BLANK: 3438887
Matrix:
Solid
Associated Lab Samples: 92569202002, 92569202003,
92569202004, 92569202005, 92569202006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
2.5
10/28/21 14:45 N2
Aromatic (C09-C10)
mg/kg
ND
2.5
10/28/21 14:45 N2
4-Bromofluorobenzene (FID) (S)
%
102
70-130
10/28/21 14:45
4-Bromofluorobenzene (PID) (S)
%
103
70-130
10/28/21 14:45
LABORATORY CONTROL SAMPLE & LCSD:
3438888
3438889
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg 14.9
13.7 13.2
92
89
70-130 3 25 N2
Aromatic (C09-C10)
mg/kg 5
5.4 5.2
109
104
70-130 5 25 N2
4-Bromofluorobenzene (FID) (S)
%
103
103
70-130
4-Bromofluorobenzene (PID) (S)
%
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 63

lacieAnalyfica('
www,pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 655937 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A/5030B Analysis Description: 8260D 5035A 5030E
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
METHOD BLANK: 3438825
Matrix:
Solid
Associated Lab Samples: 92569202002,
92569202003, 92569202004, 92569202005, 92569202006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,1,1-Trichloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,1,2-Trichloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,1-Dichloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,1-Dichloroethene
ug/kg
ND
5.0
10/28/21 13:20
1,1-Dichloropropene
ug/kg
ND
5.0
10/28/21 13:20
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
1,2,3-Trichloropropane
ug/kg
ND
5.0
10/28/21 13:20
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
1,2,4-Trimethyl benzene
ug/kg
ND
5.0
10/28/21 13:20
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
10/28/21 13:20
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
10/28/21 13:20
1,2-Dichlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
1,2-Dichloroethane
ug/kg
ND
5.0
10/28/21 13:20
1,2-Dichloropropane
ug/kg
ND
5.0
10/28/21 13:20
1,3,5-Trimethyl benzene
ug/kg
ND
5.0
10/28/21 13:20
1,3-Dichlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
1,3-Dichloropropane
ug/kg
ND
5.0
10/28/21 13:20
1,4-Dichlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
2,2-Dichloropropane
ug/kg
ND
5.0
10/28/21 13:20
2-Butanone (MEK)
ug/kg
ND
100
10/28/21 13:20
2-Chlorotoluene
ug/kg
ND
5.0
10/28/21 13:20
2-Hexanone
ug/kg
ND
50.0
10/28/21 13:20
4-Chlorotoluene
ug/kg
ND
5.0
10/28/21 13:20
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
10/28/21 13:20
Acetone
ug/kg
ND
100
10/28/21 13:20
Benzene
ug/kg
ND
5.0
10/28/21 13:20
Bromobenzene
ug/kg
ND
5.0
10/28/21 13:20
Bromochloromethane
ug/kg
ND
5.0
10/28/21 13:20
Bromodichloromethane
ug/kg
ND
5.0
10/28/21 13:20
Bromoform
ug/kg
ND
5.0
10/28/21 13:20
Bromomethane
ug/kg
ND
10.0
10/28/21 13:20 IK
Carbon tetrachloride
ug/kg
ND
5.0
10/28/21 13:20
Chlorobenzene
ug/kg
ND
5.0
10/28/21 13:20
Chloroethane
ug/kg
ND
10.0
10/28/21 13:20
Chloroform
ug/kg
ND
5.0
10/28/21 13:20
Chloromethane
ug/kg
ND
10.0
10/28/21 13:20
cis- 1,2-Dichloroethene
ug/kg
ND
5.0
10/28/21 13:20
cis- 1,3-Dichloropropene
ug/kg
ND
5.0
10/28/21 13:20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
METHOD BLANK: 3438825 Matrix: Solid
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromochloromethane
ug/kg
ND
5.0
10/28/21 13:20
Dibromomethane
ug/kg
ND
5.0
10/28/21 13:20
Dichlorodifluoromethane
ug/kg
ND
10.0
10/28/21 13:20
Diisopropyl ether
ug/kg
ND
5.0
10/28/21 13:20
Ethylbenzene
ug/kg
ND
5.0
10/28/21 13:20
Hexachloro-1,3-butadiene
ug/kg
ND
10.0
10/28/21 13:20
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
10/28/21 13:20
m&p-Xylene
ug/kg
ND
10.0
10/28/21 13:20
Methyl-tert-butyl ether
ug/kg
ND
5.0
10/28/21 13:20
Methylene Chloride
ug/kg
ND
20.0
10/28/21 13:20
n-Butylbenzene
ug/kg
ND
5.0
10/28/21 13:20
n-Propylbenzene
ug/kg
ND
5.0
10/28/21 13:20
Naphthalene
ug/kg
ND
5.0
10/28/21 13:20
o-Xylene
ug/kg
ND
5.0
10/28/21 13:20
p-Isopropyltoluene
ug/kg
ND
5.0
10/28/21 13:20
sec-Butylbenzene
ug/kg
ND
5.0
10/28/21 13:20
Styrene
ug/kg
ND
5.0
10/28/21 13:20
tert-Butyl benzene
ug/kg
ND
5.0
10/28/21 13:20
Tetrachloroethene
ug/kg
ND
5.0
10/28/21 13:20
Toluene
ug/kg
ND
5.0
10/28/21 13:20
trans-1,2-Dichloroethene
ug/kg
ND
5.0
10/28/21 13:20
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
10/28/21 13:20
Trichloroethene
ug/kg
ND
5.0
10/28/21 13:20
Trichlorofluoromethane
ug/kg
ND
5.0
10/28/21 13:20
Vinyl acetate
ug/kg
ND
50.0
10/28/21 13:20
Vinyl chloride
ug/kg
ND
10.0
10/28/21 13:20
Xylene (Total)
ug/kg
ND
10.0
10/28/21 13:20
1,2-Dichloroethane-d4 (S)
%
110
70-130
10/28/21 13:20
4-Bromofluorobenzene (S)
%
100
69-134
10/28/21 13:20
Toluene-d8 (S)
%
98
70-130
10/28/21 13:20
Qualifiers
LABORATORY CONTROL SAMPLE:
3438826
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
1250
1230
98
70-130
1,1,1-Trichloroethane
ug/kg
1250
1240
99
70-130
1,1,2,2-Tetrachloroethane
ug/kg
1250
1240
99
70-130
1,1,2-Trichloroethane
ug/kg
1250
1230
98
70-130
1,1-Dichloroethane
ug/kg
1250
1320
105
70-130
1,1-Dichloroethene
ug/kg
1250
1350
108
70-130
1,1-Dichloropropene
ug/kg
1250
1260
101
70-130
1,2,3-Trichlorobenzene
ug/kg
1250
1290
103
65-130
1,2,3-Trichloropropane
ug/kg
1250
1260
100
70-130
1,2,4-Trichlorobenzene
ug/kg
1250
1270
101
68-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
LABORATORY CONTROL SAMPLE:
Parameter
3438826
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trimethylbenzene
ug/kg
1250
1270
101
70-130
1,2-Dibromo-3-chloropropane
ug/kg
1250
1380
110
70-130
1,2-Dibromoethane (EDB)
ug/kg
1250
1250
100
70-130
1,2-Dichlorobenzene
ug/kg
1250
1220
98
70-130
1,2-Dichloroethane
ug/kg
1250
1180
94
63-130
1,2-Dichloropropane
ug/kg
1250
1280
102
70-130
1,3,5-Trimethylbenzene
ug/kg
1250
1280
103
70-130
1,3-Dichlorobenzene
ug/kg
1250
1220
98
70-130
1,3-Dichloropropane
ug/kg
1250
1220
97
70-130
1,4-Dichlorobenzene
ug/kg
1250
1210
97
70-130
2,2-Dichloropropane
ug/kg
1250
1250
100
66-130
2-Butanone (MEK)
ug/kg
2500
2550
102
70-130
2-Chlorotoluene
ug/kg
1250
1290
103
70-130
2-Hexanone
ug/kg
2500
2590
104
70-130
4-Chlorotoluene
ug/kg
1250
1240
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
2500
2530
101
70-130
Acetone
ug/kg
2500
2310
92
69-130
Benzene
ug/kg
1250
1250
100
70-130
Bromobenzene
ug/kg
1250
1270
102
70-130
Bromochloromethane
ug/kg
1250
1290
103
70-130
Bromodichloromethane
ug/kg
1250
1220
97
69-130
Bromoform
ug/kg
1250
1290
103
70-130
Bromomethane
ug/kg
1250
1440
115
52-130IK
Carbon tetrachloride
ug/kg
1250
1280
103
70-130
Chlorobenzene
ug/kg
1250
1200
96
70-130
Chloroethane
ug/kg
1250
1430
114
65-130
Chloroform
ug/kg
1250
1260
100
70-130
Chloromethane
ug/kg
1250
1260
101
55-130
cis-1,2-Dichloroethene
ug/kg
1250
1290
103
70-130
cis-1,3-Dichloropropene
ug/kg
1250
1260
101
70-130
Dibromochloromethane
ug/kg
1250
1280
103
70-130
Dibromomethane
ug/kg
1250
1260
101
70-130
Dichlorodifluoromethane
ug/kg
1250
1270
102
45-156
Diisopropyl ether
ug/kg
1250
1230
98
70-130
Ethylbenzene
ug/kg
1250
1150
92
70-130
Hexachloro-1,3-butadiene
ug/kg
1250
1290
103
66-130
Isopropylbenzene (Cumene)
ug/kg
1250
1250
100
70-130
m&p-Xylene
ug/kg
2500
2420
97
70-130
Methyl-tert-butyl ether
ug/kg
1250
1200
96
70-130
Methylene Chloride
ug/kg
1250
1150
92
65-130
n-Butylbenzene
ug/kg
1250
1290
103
67-130
n-Propylbenzene
ug/kg
1250
1260
101
70-130
Naphthalene
ug/kg
1250
1250
100
70-130
o-Xylene
ug/kg
1250
1210
97
70-130
p-Isopropyltoluene
ug/kg
1250
1270
102
67-130
sec-Butylbenzene
ug/kg
1250
1260
101
69-130
Styrene
ug/kg
1250
1280
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
LABORATORY CONTROL SAMPLE:
Parameter
3438826
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
tert-Butyl benzene
ug/kg
1250
1210
97
67-130
Tetrachloroethene
ug/kg
1250
1250
100
70-130
Toluene
ug/kg
1250
1200
96
70-130
trans-1,2-Dichloroethene
ug/kg
1250
1350
108
70-130
trans- 1,3-Dichloropropene
ug/kg
1250
1230
98
68-130
Trichloroethene
ug/kg
1250
1240
99
70-130
Trichlorofluoromethane
ug/kg
1250
1240
99
70-130
Vinyl acetate
ug/kg
2500
2590
104
70-130
Vinyl chloride
ug/kg
1250
1340
107
61-130
Xylene (Total)
ug/kg
3750
3640
97
70-130
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
%
98
69-134
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
3438828
Units
92569202006
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
757
673
89
70-131
1,1,1-Trichloroethane
ug/kg
ND
757
677
89
65-133
1,1,2,2-Tetrachloroethane
ug/kg
ND
757
674
89
66-130
1,1,2-Trichloroethane
ug/kg
ND
757
667
88
66-133
1,1-Dichloroethane
ug/kg
ND
757
697
92
65-130
1,1-Dichloroethene
ug/kg
ND
757
717
95
10-158
1,1-Dichloropropene
ug/kg
ND
757
721
95
68-133
1,2,3-Trichlorobenzene
ug/kg
ND
757
596
79
27-138
1,2,3-Trichloropropane
ug/kg
ND
757
669
88
67-130
1,2,4-Trichlorobenzene
ug/kg
ND
757
737
97
51-134
1,2,4-Trimethylbenzene
ug/kg
ND
757
926
122
63-136
1,2-Dibromo-3-chloropropane
ug/kg
ND
757
654
86
32-130
1,2-Dibromoethane (EDB)
ug/kg
ND
757
678
89
70-130
1,2-Dichlorobenzene
ug/kg
ND
757
727
96
69-130
1,2-Dichloroethane
ug/kg
ND
757
622
82
59-130
1,2-Dichloropropane
ug/kg
ND
757
713
94
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
757
812
107
65-137
1,3-Dichlorobenzene
ug/kg
ND
757
712
94
70-130
1,3-Dichloropropane
ug/kg
ND
757
678
89
70-130
1,4-Dichlorobenzene
ug/kg
ND
757
721
95
68-130
2,2-Dichloropropane
ug/kg
ND
757
649
86
32-130
2-Butanone (MEK)
ug/kg
ND
1510
1100
73
10-136
2-Chlorotoluene
ug/kg
ND
757
752
99
69-141
2-Hexanone
ug/kg
ND
1510
1140
75
10-144
4-Chlorotoluene
ug/kg
ND
757
729
96
70-132
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
1510
1260
83
25-143
Acetone
ug/kg
ND
1510
712
47
10-130
Benzene
ug/kg
ND
757
709
94
67-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
MATRIX SPIKE SAMPLE:
Parameter
3438828
Units
92569202006
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromobenzene
ug/kg
ND
757
722
95
70-130
Bromochloromethane
ug/kg
ND
757
654
86
69-134
Bromodichloromethane
ug/kg
ND
757
630
83
64-130
Bromoform
ug/kg
ND
757
613
81
62-130
Bromomethane
ug/kg
ND
757
334
44
20-1761K
Carbon tetrachloride
ug/kg
ND
757
690
91
65-140
Chlorobenzene
ug/kg
ND
757
706
93
70-130
Chloroethane
ug/kg
ND
757
122
16
10-130
Chloroform
ug/kg
ND
757
672
89
63-130
Chloromethane
ug/kg
ND
757
623
82
58-130
cis-1,2-Dichloroethene
ug/kg
ND
757
690
91
66-130
cis-1,3-Dichloropropene
ug/kg
ND
757
666
88
67-130
Dibromochloromethane
ug/kg
ND
757
635
84
67-130
Dibromomethane
ug/kg
ND
757
657
87
63-131
Dichlorodifluoromethane
ug/kg
ND
757
599
79
44-180
Diisopropyl ether
ug/kg
ND
757
648
86
63-130
Ethylbenzene
ug/kg
ND
757
703
93
66-130
Hexachloro-1,3-butadiene
ug/kg
ND
757
786
104
64-150
Isopropylbenzene (Cumene)
ug/kg
ND
757
763
101
69-135
m&p-Xylene
ug/kg
ND
1510
1510
99
60-133
Methyl-tert-butyl ether
ug/kg
ND
757
610
81
65-130
Methylene Chloride
ug/kg
ND
757
608
80
61-130
n-Butylbenzene
ug/kg
ND
757
840
111
65-140
n-Propylbenzene
ug/kg
ND
757
771
102
67-140
Naphthalene
ug/kg
ND
757
683
90
15-145
o-Xylene
ug/kg
ND
757
729
96
66-133
p-Isopropyltoluene
ug/kg
ND
757
790
104
56-147
sec-Butylbenzene
ug/kg
ND
757
766
101
65-139
Styrene
ug/kg
ND
757
723
95
70-132
tert-Butyl benzene
ug/kg
ND
757
729
96
62-135
Tetrachloroethene
ug/kg
ND
757
744
98
70-135
Toluene
ug/kg
ND
757
697
92
67-130
trans-1,2-Dichloroethene
ug/kg
ND
757
723
95
69-130
trans- 1,3-Dichloropropene
ug/kg
ND
757
635
84
62-130
Trichloroethene
ug/kg
ND
757
710
94
70-135
Trichlorofluoromethane
ug/kg
ND
757
87.8
12
10-130
Vinyl acetate
ug/kg
ND
1510
1280
85
53-130
Vinyl chloride
ug/kg
ND
757
636
84
61-148
Xylene (Total)
ug/kg
ND
2280
2240
98
63-132
1,2-Dichloroethane-d4 (S)
%
117
70-130
4-Bromofluorobenzene (S)
%
99
69-134
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 45 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
SAMPLE DUPLICATE: 3438827
Parameter
Units
92568803008
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
ND
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
ND
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
SAMPLE DUPLICATE: 3438827
Parameter
Units
92568803008
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
108
109
4-Bromofluorobenzene (S)
%
100
99
Toluene-d8 (S)
%
99
98
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 47 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 656006
Analysis Method:
EPA 8015C Modified
QC Batch Method: EPA 3546
Analysis Description:
8015 Solid GCSV
Laboratory:
Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202001
METHOD BLANK: 3439080
Matrix: Solid
Associated Lab Samples: 92569202001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
5.0 10/29/21 10:37
n-Pentacosane (S)
%
72 32-130
10/29/21 10:37
LABORATORY CONTROL SAMPLE:
3439081
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.4 41.9
63 47-130
n-Pentacosane (S)
%
59 32-130
MATRIX SPIKE SAMPLE:
3439082
92569213001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 85.6
30.9 34
10-133
n-Pentacosane(S)
%
25
32-130 S2
SAMPLE DUPLICATE: 3439083
92569213002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
ND
n-Pentacosane (S)
%
34
22 SO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 655833 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
METHOD BLANK: 3438174 Matrix: Solid
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
333
10/29/21 11:14
1,2-Dichlorobenzene
ug/kg
ND
333
10/29/21 11:14
1,3-Dichlorobenzene
ug/kg
ND
333
10/29/21 11:14
1,4-Dichlorobenzene
ug/kg
ND
333
10/29/21 11:14
1-Methylnaphthalene
ug/kg
ND
333
10/29/21 11:14
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
333
10/29/21 11:14
2,4,5-Trichlorophenol
ug/kg
ND
333
10/29/21 11:14
2,4,6-Trichlorophenol
ug/kg
ND
333
10/29/21 11:14
2,4-Dichlorophenol
ug/kg
ND
333
10/29/21 11:14
2,4-Dimethylphenol
ug/kg
ND
333
10/29/21 11:14
2,4-Dinitrophenol
ug/kg
ND
1670
10/29/21 11:14
2,4-Dinitrotoluene
ug/kg
ND
333
10/29/21 11:14
2,6-Dinitrotoluene
ug/kg
ND
333
10/29/21 11:14
2-Chloronaphthalene
ug/kg
ND
333
10/29/21 11:14
2-Chlorophenol
ug/kg
ND
333
10/29/21 11:14
2-Methylnaphthalene
ug/kg
ND
333
10/29/21 11:14
2-Methylphenol(o-Cresol)
ug/kg
ND
333
10/29/21 11:14
2-Nitroaniline
ug/kg
ND
1670
10/29/21 11:14
2-Nitrophenol
ug/kg
ND
333
10/29/21 11:14
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
333
10/29/21 11:14
3,3'-Dichlorobenzidine
ug/kg
ND
667
10/29/21 11:14
3-Nitroaniline
ug/kg
ND
1670
10/29/21 11:14
4,6-Dinitro-2-methyl phenol
ug/kg
ND
667
10/29/21 11:14
4-Bromophenylphenyl ether
ug/kg
ND
333
10/29/21 11:14
4-ChIoro-3-methyl phenol
ug/kg
ND
667
10/29/21 11:14
4-Chloroaniline
ug/kg
ND
667
10/29/21 11:14
4-Chlorophenylphenyl ether
ug/kg
ND
333
10/29/21 11:14
4-Nitroaniline
ug/kg
ND
667
10/29/21 11:14
4-Nitrophenol
ug/kg
ND
1670
10/29/21 11:14
Acenaphthene
ug/kg
ND
333
10/29/21 11:14
Acenaphthylene
ug/kg
ND
333
10/29/21 11:14
Aniline
ug/kg
ND
333
10/29/21 11:14
Anthracene
ug/kg
ND
333
10/29/21 11:14
Benzo(a)anthracene
ug/kg
ND
333
10/29/21 11:14
Benzo(a)pyrene
ug/kg
ND
333
10/29/21 11:14
Benzo(b)fluoranthene
ug/kg
ND
333
10/29/21 11:14
Benzo(g,h,i)perylene
ug/kg
ND
333
10/29/21 11:14
Benzo(k)fluoranthene
ug/kg
ND
333
10/29/21 11:14
Benzoic Acid
ug/kg
ND
1670
10/29/21 11:14
Benzyl alcohol
ug/kg
ND
667
10/29/21 11:14
v1
IL
IL
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
METHOD BLANK: 3438174 Matrix: Solid
Associated Lab Samples: 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroethoxy)methane
ug/kg
ND
333
10/29/21 11:14
bis(2-Chloroethyl) ether
ug/kg
ND
333
10/29/21 11:14
bis(2-Ethylhexyl)phthalate
ug/kg
ND
333
10/29/21 11:14
Butylbenzylphthalate
ug/kg
ND
333
10/29/21 11:14
Chrysene
ug/kg
ND
333
10/29/21 11:14
Di-n-butylphthalate
ug/kg
ND
333
10/29/21 11:14
Di-n-octylphthalate
ug/kg
ND
333
10/29/21 11:14
Dibenz(a,h)anthracene
ug/kg
ND
333
10/29/21 11:14
Dibenzofuran
ug/kg
ND
333
10/29/21 11:14
Diethylphthalate
ug/kg
ND
333
10/29/21 11:14
Dimethylphthalate
ug/kg
ND
333
10/29/21 11:14
Fluoranthene
ug/kg
ND
333
10/29/21 11:14
Fluorene
ug/kg
ND
333
10/29/21 11:14
Hexachloro-1,3-butadiene
ug/kg
ND
333
10/29/21 11:14
Hexachlorobenzene
ug/kg
ND
333
10/29/21 11:14
Hexachlorocyclopentadiene
ug/kg
ND
333
10/29/21 11:14
Hexachloroethane
ug/kg
ND
333
10/29/21 11:14
Indeno(1,2,3-cd)pyrene
ug/kg
ND
333
10/29/21 11:14
Isophorone
ug/kg
ND
333
10/29/21 11:14
N-Nitroso-di-n-propylamine
ug/kg
ND
333
10/29/21 11:14
N-Nitrosodimethylamine
ug/kg
ND
333
10/29/21 11:14
N-Nitrosodiphenylamine
ug/kg
ND
333
10/29/21 11:14
Naphthalene
ug/kg
ND
333
10/29/21 11:14
Nitrobenzene
ug/kg
ND
333
10/29/21 11:14
Pentachlorophenol
ug/kg
ND
667
10/29/21 11:14
Phenanthrene
ug/kg
ND
333
10/29/21 11:14
Phenol
ug/kg
ND
333
10/29/21 11:14
Pyrene
ug/kg
ND
333
10/29/21 11:14
Pyridine
ug/kg
ND
333
10/29/21 11:14
2,4,6-Tribromophenol (S)
%
79
18-130
10/29/21 11:14
2-Fluorobiphenyl (S)
%
73
19-130
10/29/21 11:14
2-Fluorophenol (S)
%
62
18-130
10/29/21 11:14
Nitrobenzene-d5 (S)
%
64
21-130
10/29/21 11:14
Phenol-d6 (S)
%
66
18-130
10/29/21 11:14
Terphenyl-d14 (S)
%
113
15-130
10/29/21 11:14
Qualifiers
LABORATORY CONTROL SAMPLE:
3438175
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1640
1100
67
47-130
1,2-Dichlorobenzene
ug/kg
1640
1050
64
49-130
1,3-Dichlorobenzene
ug/kg
1640
1050
64
48-130
1,4-Dichlorobenzene
ug/kg
1640
1100
67
49-130
1-Methylnaphthalene
ug/kg
1640
1230
75
54-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
LABORATORY CONTROL SAMPLE:
Parameter
3438175
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2'-Oxybis(1-chloropropane)
ug/kg
1640
1160
71
38-130
2,4,5-Trichlorophenol
ug/kg
1640
1700
103
49-130
2,4,6-Trichlorophenol
ug/kg
1640
1550
94
50-130
2,4-Dichlorophenol
ug/kg
1640
1210
73
51-130
2,4-Dimethylphenol
ug/kg
1640
1290
78
53-130
2,4-Dinitrophenol
ug/kg
8220
10300
126
39-130 v1
2,4-Dinitrotoluene
ug/kg
1640
1980
120
53-130
2,6-Dinitrotoluene
ug/kg
1640
1880
114
55-130
2-Chloronaphthalene
ug/kg
1640
1490
90
48-130
2-Chlorophenol
ug/kg
1640
1080
66
54-130
2-Methylnaphthalene
ug/kg
1640
1200
73
57-130
2-Methylphenol(o-Cresol)
ug/kg
1640
1180
72
50-130
2-Nitroaniline
ug/kg
3290
3290
100
49-130
2-Nitrophenol
ug/kg
1640
1140
69
50-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1640
1230
75
50-130
3,3'-Dichlorobenzidine
ug/kg
3290
3010
91
47-130IL
3-Nitroaniline
ug/kg
3290
3410
104
45-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
3290
4010
122
50-142 v1
4-Bromophenylphenyl ether
ug/kg
1640
1700
103
55-130
4-ChIoro-3-methyl phenol
ug/kg
3290
3000
91
52-130
4-Chloroaniline
ug/kg
3290
2340
71
49-130
4-Chlorophenylphenyl ether
ug/kg
1640
1840
112
53-130
4-Nitroaniline
ug/kg
3290
3500
106
51-130
4-Nitrophenol
ug/kg
8220
9710
118
40-130
Acenaphthene
ug/kg
1640
1590
97
56-130
Acenaphthylene
ug/kg
1640
1640
100
58-130
Aniline
ug/kg
1640
987
60
44-130
Anthracene
ug/kg
1640
1620
99
60-130
Benzo(a)anthracene
ug/kg
1640
1890
115
59-130
Benzo(a)pyrene
ug/kg
1640
1880
114
57-130
Benzo(b)fluoranthene
ug/kg
1640
1890
115
54-130
Benzo(g,h,i)perylene
ug/kg
1640
1990
121
59-130
Benzo(k)fluoranthene
ug/kg
1640
1900
115
54-130
Benzoic Acid
ug/kg
8220
6010
73
19-130
Benzyl alcohol
ug/kg
3290
2450
74
50-130
bis(2-Chloroethoxy)methane
ug/kg
1640
1120
68
55-130
bis(2-Chloroethyl) ether
ug/kg
1640
1140
69
53-130
bis(2-Ethylhexyl)phthalate
ug/kg
1640
1600
97
58-130
Butylbenzylphthalate
ug/kg
1640
1650
100
46-138
Chrysene
ug/kg
1640
1900
115
57-130
Di-n-butylphthalate
ug/kg
1640
1540
93
57-130
Di-n-octylphthalate
ug/kg
1640
1660
101
57-130
Dibenz(a,h)anthracene
ug/kg
1640
1970
120
60-130
Dibenzofuran
ug/kg
1640
1780
109
54-130
Diethylphthalate
ug/kg
1640
1810
110
55-130
Dimethylphthalate
ug/kg
1640
1780
108
57-130
Fluoranthene
ug/kg
1640
1680
102
57-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
LABORATORY CONTROL SAMPLE:
3438175
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Fluorene
ug/kg
1640
1670
102
56-130
Hexachloro-1,3-butadiene
ug/kg
1640
1170
71
41-130
Hexachlorobenzene
ug/kg
1640
1590
97
53-130
Hexachlorocyclopentadiene
ug/kg
1640
1160
70
23-130
Hexachloroethane
ug/kg
1640
1010
62
48-130
Indeno(1,2,3-cd)pyrene
ug/kg
1640
2080
126
61-130
Isophorone
ug/kg
1640
1260
77
49-130
N-Nitroso-di-n-propylamine
ug/kg
1640
1240
75
52-130
N-Nitrosodimethylamine
ug/kg
1640
1040
63
45-130
N-Nitrosodiphenylamine
ug/kg
1640
1550
94
56-130
Naphthalene
ug/kg
1640
1090
66
56-130
Nitrobenzene
ug/kg
1640
1120
68
50-130
Pentachlorophenol
ug/kg
3290
3260
99
33-130
Phenanthrene
ug/kg
1640
1610
98
60-130
Phenol
ug/kg
1640
1260
76
54-130
Pyrene
ug/kg
1640
1740
106
61-130
Pyridine
ug/kg
1640
901
55
35-130
2,4,6-Tribromophenol (S)
%
91
18-130
2-Fluorobiphenyl (S)
%
77
19-130
2-Fluorophenol (S)
%
57
18-130
Nitrobenzene-d5(S)
%
60
21-130
Phenol-d6 (S)
%
64
18-130
Terphenyl-d14(S)
%
103
15-130
MATRIX SPIKE SAMPLE:
3438176
92569091005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
1970
1360
69
22-130
1,2-Dichlorobenzene
ug/kg
ND
1970
1340
68
23-130
1,3-Dichlorobenzene
ug/kg
ND
1970
1300
66
26-130
1,4-Dichlorobenzene
ug/kg
ND
1970
1340
68
27-130
1-Methylnaphthalene
ug/kg
ND
1970
1420
72
30-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1970
1430
72
30-130
2,4,5-Trichlorophenol
ug/kg
ND
1970
1830
93
26-130
2,4,6-Trichlorophenol
ug/kg
ND
1970
1730
87
23-130
2,4-Dichlorophenol
ug/kg
ND
1970
1460
74
29-130
2,4-Dimethylphenol
ug/kg
ND
1970
1520
77
13-130
2,4-Dinitrophenol
ug/kg
ND
9880
10300
104
10-131 v1
2,4-Dinitrotoluene
ug/kg
ND
1970
2090
106
28-130
2,6-Dinitrotoluene
ug/kg
ND
1970
2040
103
36-130
2-Chloronaphthalene
ug/kg
ND
1970
1660
84
27-130
2-Chlorophenol
ug/kg
ND
1970
1320
67
29-130
2-Methylnaphthalene
ug/kg
ND
1970
1400
71
29-130
2-Methylphenol(o-Cresol)
ug/kg
ND
1970
1420
72
20-130
2-Nitroaniline
ug/kg
ND
3960
3530
89
29-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
MATRIX SPIKE SAMPLE:
3438176
92569091005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Nitrophenol
ug/kg
ND
1970
1420
72
26-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
1970
1440
73
10-176
3,3'-Dichlorobenzidine
ug/kg
ND
3960
3160
80
15-130IL
3-Nitroaniline
ug/kg
ND
3960
3650
92
28-130IL
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3960
4210
106
15-132 v1
4-Bromophenylphenyl ether
ug/kg
ND
1970
1750
89
35-130
4-Chloro-3-methylphenol
ug/kg
ND
3960
3320
84
30-130
4-Chloroaniline
ug/kg
ND
3960
2740
69
28-130
4-Chlorophenylphenyl ether
ug/kg
ND
1970
1930
98
32-130
4-Nitroaniline
ug/kg
ND
3960
3650
92
30-130
4-Nitrophenol
ug/kg
ND
9880
10200
103
17-130
Acenaphthene
ug/kg
ND
1970
1690
86
29-130
Acenaphthylene
ug/kg
ND
1970
1750
89
31-130
Aniline
ug/kg
ND
1970
1130
57
10-130
Anthracene
ug/kg
ND
1970
1660
84
33-130
Benzo(a)anthracene
ug/kg
ND
1970
1890
96
32-130
Benzo(a)pyrene
ug/kg
ND
1970
1930
97
32-130
Benzo(b)fluoranthene
ug/kg
ND
1970
1900
96
33-130
Benzo(g,h,i)perylene
ug/kg
ND
1970
1990
101
28-130
Benzo(k)fluoranthene
ug/kg
ND
1970
1960
99
31-130
Benzoic Acid
ug/kg
ND
9880
6840
69
10-130
Benzyl alcohol
ug/kg
ND
3960
2860
72
31-130
bis(2-Chloroethoxy)methane
ug/kg
ND
1970
1360
69
30-130
bis(2-Chloroethyl) ether
ug/kg
ND
1970
1380
70
68-130
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1970
1670
85
40-130
Butylbenzylphthalate
ug/kg
ND
1970
1690
86
40-130
Chrysene
ug/kg
ND
1970
1920
97
30-130
Di-n-butylphthalate
ug/kg
ND
1970
1580
80
41-130
Di-n-octylphthalate
ug/kg
ND
1970
1730
88
42-130
Dibenz(a,h)anthracene
ug/kg
ND
1970
1970
100
27-130
Dibenzofuran
ug/kg
ND
1970
1830
92
32-130
Diethylphthalate
ug/kg
ND
1970
1910
97
40-130
Dimethylphthalate
ug/kg
ND
1970
1930
97
37-130
Fluoranthene
ug/kg
ND
1970
1700
86
26-130
Fluorene
ug/kg
ND
1970
1780
90
31-130
Hexachloro-1,3-butadiene
ug/kg
ND
1970
1460
74
20-130
Hexachlorobenzene
ug/kg
ND
1970
1630
83
29-130
Hexachlorocyclopentadiene
ug/kg
ND
1970
1400
71
10-130
Hexachloroethane
ug/kg
ND
1970
1250
63
21-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1970
2080
105
28-130
Isophorone
ug/kg
ND
1970
1440
73
32-130
N-Nitroso-di-n-propylamine
ug/kg
ND
1970
1430
73
31-130
N-Nitrosodimethylamine
ug/kg
ND
1970
1270
64
20-130
N-Nitrosodiphenylamine
ug/kg
ND
1970
1610
81
32-130
Naphthalene
ug/kg
ND
1970
1350
68
30-130
Nitrobenzene
ug/kg
ND
1970
1390
70
25-130
Pentachlorophenol
ug/kg
ND
3960
3380
86
10-130
Results presented on this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
MATRIX SPIKE SAMPLE:
Parameter
3438176
Units
92569091005
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Phenanthrene
ug/kg
ND
1970
1680
85
34-130
Phenol
ug/kg
ND
1970
1470
75
14-130
Pyrene
ug/kg
ND
1970
1740
88
31-130
Pyridine
ug/kg
ND
1970
362J
18
10-130
2,4,6-Tribromophenol (S)
%
86
18-130
2-Fluorobiphenyl (S)
%
69
19-130
2-Fluorophenol (S)
%
62
18-130
Nitrobenzene-d5(S)
%
66
21-130
Phenol-d6 (S)
%
68
18-130
Terphenyl-d14 (S)
%
93
15-130
SAMPLE DUPLICATE: 3438177
Parameter
Units
92569091006
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Bromophenylphenyl ether
ug/kg
ND
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
4-Chloroaniline
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
RPD Qualifiers
v1
IL
IL
v1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
SAMPLE DUPLICATE: 3438177
Parameter
Units
92569091006
Result
Dup
Result
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
Pyridine
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
72
75
2-Fluorobiphenyl (S)
%
61
66
2-Fluorophenol (S)
%
62
69
Nitrobenzene-d5 (S)
%
69
71
Phenol-d6 (S)
%
65
72
Terphenyl-d14 (S)
%
85
86
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 656032 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92569202001, 92569202002, 92569202003, 92569202004, 92569202005, 92569202006
SAMPLE DUPLICATE: 3439228
92569162024 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 23.1 23.5 2 N2
SAMPLE DUPLICATE: 3439229
92569290005 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 19.5 19.2 1 N2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC.
Page 56 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 1766758 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92569202002, 92569202003
METHOD BLANK: R3724182-1
Matrix:
Solid
Associated Lab Samples: 92569202002, 92569202003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Solids
%
0.00100
11/01/21 15:56
LABORATORY CONTROL SAMPLE:
R3724182-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Solids
%
50.0
50.0
99.9 85.0-115
SAMPLE DUPLICATE: R3724182-3
L1424123-07 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 91.7 92.0 0.406
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 896-01
Pace Project No.: 92569202
QC Batch: 1766760 Analysis Method: SM 2540G
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Laboratory: Pace National - Mt. Juliet
Associated Lab Samples: 92569202004, 92569202005, 92569202006
METHOD BLANK: R3724726-1
Matrix:
Solid
Associated Lab Samples: 92569202004, 92569202005,
92569202006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Solids
%
0.00100
11/02/21 09:51
LABORATORY CONTROL SAMPLE:
R3724726-2
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Solids
%
50.0
50.0
100 85.0-115
SAMPLE DUPLICATE: R3724726-3
92569202004 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 73.0 74.7 2.30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 896-01
Pace Project No.: 92569202
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92569202005
Ill TPH by Method MADEPE - Dilution due to matrix impact during extraction procedure
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
P6 Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 896-01
Pace Project No.: 92569202
ANALYTE QUALIFIERS
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /10/2021 04:50 PM without the written consent of Pace Analytical Services, LLC. Page 60 of 63

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
896-01
92569202
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92569202002
BOT 2 (14)
MA DEP/NJ DEP
1768646
MADEP EPH
1768646
92569202003
SW (9)
MA DEP/NJ DEP
1768646
MADEP EPH
1768646
92569202004
EW (11)
MA DEP/NJ DEP
1768646
MADEP EPH
1768646
92569202005
NW (9)
MA DEP/NJ DEP
1768646
MADEP EPH
1768646
92569202006
WW (8)
MA DEP/NJ DEP
1768646
MADEP EPH
1768646
92569202001
BOT 1 (6)
EPA 3546
656006
EPA 8015C Modified
656144
92569202001
BOT 1 (6)
EPA 5030B
655959
EPA 8015C Modified
656244
92569202002
BOT 2 (14)
MADEP VPH
655957
MADEP VPH
656020
92569202003
SW (9)
MADEP VPH
655957
MADEP VPH
656020
92569202004
EW (11)
MADEP VPH
655957
MADEP VPH
656020
92569202005
NW (9)
MADEP VPH
655957
MADEP VPH
656020
92569202006
WW (8)
MADEP VPH
655957
MADEP VPH
656020
92569202002
BOT 2 (14)
EPA 3546
655833
EPA 8270E
656166
92569202003
SW (9)
EPA 3546
655833
EPA 8270E
656166
92569202004
EW (11)
EPA 3546
655833
EPA 8270E
656166
92569202005
NW (9)
EPA 3546
655833
EPA 8270E
656166
92569202006
WW (8)
EPA 3546
655833
EPA 8270E
656166
92569202002
BOT 2 (14)
EPA 5035A/5030B
655937
EPA 8260D
655977
92569202003
SW (9)
EPA 5035A/5030B
655937
EPA 8260D
655977
92569202004
EW (11)
EPA 5035A/5030B
655937
EPA 8260D
655977
92569202005
NW (9)
EPA 5035A/5030B
655937
EPA 8260D
655977
92569202006
WW (8)
EPA 5035A/5030B
655937
EPA 8260D
655977
92569202001
BOT 1 (6)
SW-846
656032
92569202002
BOT 2 (14)
SW-846
656032
92569202003
SW (9)
SW-846
656032
92569202004
EW (11)
SW-846
656032
92569202005
NW (9)
SW-846
656032
92569202006
WW (8)
SW-846
656032
92569202002
BOT 2 (14)
SM 2540 G
1766758
SM 2540G
1766758
92569202003
SW (9)
SM 2540 G
1766758
SM 2540G
1766758
92569202004
EW (11)
SM 2540 G
1766760
SM 2540G
1766760
92569202005
NW (9)
SM 2540 G
1766760
SM 2540G
1766760
92569202006
WW (8)
SM 2540 G
1766760
SM 2540G
1766760
Date: 11/10/2021 04:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 61 of 63

I
0
c
m
3
m
13
a
v
m
v
A
2
ro
2
v
0
3
A
n
Q
v
w
c
4A
n
rY
�
3
rT
o
0
3
�
w
C
n
�
a
�
�
3
m n
IZ
n n
�O
N
II1
6
3
3
N
3
a
m v
n. A
w
c'
n
s
a
Itemu
BP4U-125 mL Nam
c Unpreserved (N/A) (CI-)
SP3U-250 mL Mast
I
is Unpreserved (NfA)
BP2U-500 mL Plas
iC Unpreserved IN1/IA)
BPJU-1 liter Plastic
Unpreserved (N/A)
BMS-125 mL Plastic
I
H2SO4 (pH < 2) I-)
VP3N-2SO mL plastic
HNO3 (pH < 2)
OP47-125 mL Plasi
a 2N Acetate & Na H (>9}
BP4C-125 mL Plast
C NaOH (pH > 12) Cl-)(
—
WGFU-wide-maut
ed Glass jar Unpreserved
AG lU-1 liter Amber
Unpreserved (N/A) (CM)
ZKAG1H-1
liter Amber
HO (pH < 2)
AG3U-250 mL AmLer
Unpreserved (N{A) (Cl-)_
AG IS-1 liter Ambe
H2504 (pH < 2)
AG35-250 mL Amber
H2SO4 (pH < 2)
AG3A(DG3A)-250
nL Amber NH4Cl (N/A)jCI-)
DG9H-40 mL VOA
qC1 (N/A)
V69T-40 mL VOA I
la2521331 (N/A) j
VG9U-10 m1 VOA
np (N/A)
OG9P-40 mL VOA
3PO4 (N/A) '
VOAK 46 vials pwr
it)-5035 kit (N/A)
J
.J.i
i,-r
W
"�
',J`/
V/GK (3 via1S per
it)-VPH/Gas kit (N/M
SPST-125 ml Sterl
e Plastic (N/A — lab)I
SP27-250 mL Stet
le Plastic (N/A — lab)
ZzzBP3A-25O
mL Plasi
is INH2)2SO4 (93-9
7)
AGOU-100 mL Aml
ler Unpreserved vial} (N/A)
VSGU-20 mL Scint
Ilail4n vlals (N/A)
DGSIU-40 mi. Amb
l
r Unpreserved vials (N/A)
i
C ;
ro n
ell
CL
m 3
a Iv
CL
� O
S �
IM
rn o
n Cr
CD G
,8 x
01 '13
n =
tD y
w 3
IM
tofD
O
o f
CD
-o a
N O
01
.01-r 0
O 3
3
M
O
M
Co
aD
to
IL
�+ o
O G O
r"t c o c
63 a �
W - 0 z
2
d
z
f' a m 3
n fD
o �
v

Appendix K
Photographs of Site Check, Closure and Excavation
(This Appendix was not used)

Appendix L
Geologic Log of the Excavation

EXCAVATION LOG
BORING/WELL NO.: UST EXCAVATION
PROJECT NAME: S.S. PARKER PROPERTY
PROJECT NO.: 896-01
HARMON ENVIRONMENTAL, PA
CONTRACTOR: DEBRUHL ENV. EXCAV.
OPERATOR: RANDY DEBRUHL
615 BRUCE THOMAS ROAD
METHOD: BACKHOE
MONROE, NORTH CAROLINA 28112
DATE: OCTOBER 25&26, 2021
704-292-4527
ELEVATION: NO MEASURED
harmonenvironmental.com
DEPTH
SAMPLING
SAMPLE
REMARKS/
(FEET)
METHOD
DESCRIPTION
COMMENTS
BACKHOE
RED AND BLUE MOTTLED MICACEOUS SILT
6.0
TAN AND ORANGE MOTTLED SILT
14.0
EXCAVATION TERMINATED AT 14.0 FEET

Appendix M
Monitor Well Construction Forms
(This Appendix is not applicable to this project)

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, December 6, 2021 8:14 AM
To: Rick Harmon
Subject: RE: [External] Re: Revocable Trust Of Sharon Saville Parker Property - Revocable Trust Of Sharon
Saville Parker Property - Incident #47974
Thanks!
Trudy
From: Rick Harmon [maiIto: [e-mail]]
Sent: Monday, December 6, 2021 8:11 AM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Re: Revocable Trust Of Sharon Saville Parker Property - Revocable Trust Of Sharon Saville Parker
Property - Incident #47974
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.
Per you request.
Richard Harmon, P.G.
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
harmonenvironmental. com
On Monday, December 6, 2021, 08:05:31 AM EST, Beverly, Trudy <trudy.beverly(@-ncdenr.gov> wrote:
Hey Rick,
Unfortunately, I left the cd for the report in my office and I'm working remotely today. Please email me a copy of the
report.
Thank you,
Trudy
�E
Ikpirlrrxn[o1 Lmironmentul 4uaWty�
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.BeverlyPncdenr.gov

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https: / /deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-males
File Review Procedures:
https: / /deq.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httl2s://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https: //files.nc.gov/ncdeg/Waste°/n20Management/DWM/UST/WhatsNew/Final-Electronic-Document-Submittal-Policypdf
https: //files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/UST%20file%20names%20for%20Laserfiche.docx