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Home My WebLink AboutNCD980602163_19911231_Warren County PCB Landfill_SERB C_Monthly Inspections and Leachate Monitoring, Semi-Annual Sampling - 1991-OCR------------------------------- ,,._STAT["'~ c1 .,.,.,10,,.,,~ ft;~_: .. ~ ,__ , I , t c' , ~ -~ 'r,. t~~'g 't SIIJ-i', .......... 1,,,... ,'~Qu,,M"~ State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary December 31, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Larry Rose, Hydrogeological Technician Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the December inspection is enclosed for your review. The landfill appears to be in good condition at the present time. There was no evidence of recent groundhog activity. The leg traps set for groundhogs resulted in the capture of a gray fox. Apparently the fox was trying to aid the efforts of controlling the groundhog population at the site and inadvertently stepped in the trap. Since we have no quarrel with a valuable ally, it was set free. The existing burrow entrances should be sealed by filling with soil and the remaining traps can be removed. Control efforts may be needed again this coming Spring. Because of freezing weather conditions and the possibility of damaging the pump, the leachate sump was not pumped. If you have any questions, please call this office at (919) 733-0692. cc: Jim Coffey Attachment • j . --l. Entrance Road 2. Monitoring Wells Casings, locks J. ... . , . · Fences, gates, locks Landfill fence, gate, locks Air Vent ~-Landfill Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Ero~ion, vegetation 10. Irrigation Syst~ Influent Piping Pump Sprinkler Units NAME LJJR.l<-r Ro~E NO POTENTIAL PROBLEM PROBLEM OBSERVATIONS .✓ -v V v v • V ✓ .-,.--. ........ ______ _ .: PCi3 _LANDFILL MONTHLY REPORT (CONT. uATE / 2 .-1-0 =JI NAME lA12.e..y f2o<E . ,.--._ ·: Pumping Data. . . Pumping -Times -L lz-1'1Cfft1;[E;. 11Jo 7 Pw.,ping Volume ____ ....:,_ ___________ _ Irrigatjon Data. Irrif;°a.ting Times lTriga.ting yo1ume" ·' _______________ _;__ J I f ~C> I J..l/ '].. 'fr/ s" l . 4r/ 2-5 // • , l ~- 1 -State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary December 2, 1991 MEMORANDUM TO: Mr. James Rhodes, Deputy Secretary Department of Administration FROM: Larry Rose, Hydrogeological Technician f/2.- Solid Waste Section William L. Meyer Director RE: Results of the Sample Analysis from the PCB Landfill Sampling Episode Attached are copies of the results of the sample analysis from the PCB Landfill sampling episode conducted in October. All samples were analyzed at the State Public Health Laboratory. The results of all tests (ground water, surface water, and stream sediment samples) were below the detection limits. There is no evidence of any contamination from the landfill at this time. If you have any questions concerning the landfill, please contact our office at (919) 733-0692. cc: Bill Meyer Dennis w. Retzlaff Attachment An Equal Opportunity Affinnatlve Acdon Employer ' State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary December 2, 1991 MEMORANDUM TO: FROM: fll- RE: Mr. James Rhodes, Deputy Secretary Department of Administration Larry Rose, Hydrogeological Technician Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the November inspection is enclosed for your review. Overall, the landfill site appears to be in good condition. Efforts to eliminate groundhogs within the fenced portion of the site are continuing. The leachate sump was pumped and measurements were taken on the pumping rate and volume. If you have any questions, please call this office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affinnatlve Action Employer .:~, PCO LA.rl.Df !LL i"iui\J.'liU lU.::.PORT 1. Entrance Road 2. Monitoring Wells Casings, locks · Fences, gates, locks .) . Landfill fence, gate, locks 1, • Air Vent ~-Landfill Cover 6. 7. B. .. 10. Erosion, vegetation Subsidence Leachate Detection System Water in sump Leachate Collection System Access Pipe Pump Piping Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation Irrigation Syste~ Influent Piping Pump Sprinkler Units NAME Le..,,.,.,.'-f Ko~<-·-----++------------ NO POTENTIAL PROBLEM PROBLEM . . v' ✓ ✓ v ✓ V ✓ OBSERVATIONS .: PCi3 LANDFILL MONTHLY REPORT (cmrr. uATE _____ /_/_.-_~__._7_-_Cj'--1 _____ NAME L~ l(.:,,e : Pumping Data Pumping-Times PUJ.,ping Volume ;>S--1 ~~ -t ~5'"" = · It,, S-.. e:,,/tL 1 Irrigat1bn Data Irri£;°a.ting Times .. , ... -~-~-t,'. ~;J /_nt._~-----·------ Irrigating yolume ·' _________________ _ • G:?-~r;:;:J '.,.i.::: ~ :'.0 :; ~ :0 H :;G '.~:'. U... ccc:.::-t:: \ L.i.. L [0 :; S :-: :: : -;: Oa: ~: / / -~ ?~ 9/ S i. : ~ ~; ;i :-:: ~ : f' L° 8 _ _:.____.:::::...._ ______ _ LF Oi.5tdc,:: ---------Si.t~ O~s::.! ------------( m ~ ~ l c. -ind u ~., s ~ ~ L --d ! :-:: ~) P;:::iL: .7. ------Co•.:.:i.:y: J../AR.R~N Sic! A!1:!ss:__________ Sic~ Ccnc1cc: A~~:!~La:i.ons: 2~~ = PolyvLnyl~ht~rLd!; GS= G~tvanlz!! S:a~l; S = St!;l; SS = S:aLnlas; S:!al Ty?: o E SLz~ of 0a?:i Eco~ T0p of 5 C LC<•l? -Ci;:.r.g c~s :.ng Ct!~~:-Ca5 ~::.5 Fi!<!': o~ H-:£3h~ Ci::-:-.:-::a n: i Si:a:i.,-H:-i.J . i.:, :'!~ :-a,~::.~-c i:i;i.~ :-o 1..! C-?-:; :-J 3,,,:i:0.:1 : . .J ~.; .l ::~ = ~,J'~ ':~ :" i;;n~:: 0'.!:~:-ElEV~T!o.A> I/ 1 I I/ 'i.'2-/ 39 %,2~ I l f. '31 2 3~' 11 251/ q1."-f~ II 3 I II II 2.~' l/2.. 25';5 'f 2. ,'S''f t ., r I 3// 2.£5 J) io,2s , . . . -~'-... ' I ~ .#".'~~~ r ~••'No,,, ~ '~.:I !5/111-(. ~.-\ ,~ .r.::~ . 0 -~.., (,O I r::, ~ :-, .. ,;,,.,, .. .,. _ _,,,<] fl!J.I (,llJ,,V,ll .. ~j,~ ·' ¾~.~ State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary October 30, 1991 MEMORANDUM TO: FROM: t~ RE: Mr. James Rhodes, Deputy Secretary Department of Administration Bobby Lutfy, Hydrogeologist Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the October inspection is enclosed for your review. The ground water monitoring wells and the four stream locations were sampled on October 28 and 29. The leachate sump was pumped and a sample of the leachate was taken. The maintenance needs at the landfill have been promptly attended to by the Department of Transportation. The grass has recently been mowed. The grass within the well fences has been trimmed back, which made sampling of the monitoring wells much easier. Traps have been set to control the groundhogs at the site. Repairs have been made to the leachate collection pump and the fitting on the influent pi~ing. Overall, the landfill site appears to be in generally good condition at this time . The results of the ground and surface water sampling analysis will be forwarded to you when they are received by the .Solid Waste Section. If you have any questions concerning the PCB Landfill, you may contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Employer .. .. \... PCI) LAJ-4Df ILL h UL\i'i-!Ll'. H...El'O i<.T 1. Entrance Road 2. Monitoring Wells Casings, locks · Fences, gates, locks J . Landfill fence, gate, locks ,; . Air Vent ). Landfill Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation 10. Irrigation Syste~ Influent Piping Pump Sprinkler Units NAME /Jc.'£/!t NO POTENTIAL PROBLEM PROBLEM v . . V V OBSERVATIONS .: PC .3 LANDFILL MONTHLY REPORT (CONT. uATE _ __,_/_<O...,,_, /4_~_-.... 8_+_~ __ 9..._/4_u ...... 11 ____ NAME __ B ____ ,&13=-· __ r __ l_·.,.,_-;;_F+-~-r-/4 __ L_A1e_t2 ... Y...a..-: __ ~_-_--'~ c:.~ .1 I I : Pumping Data Pumping -Times Pw.,ping Volume .Abet.·!-IO iJ aa.((c.·J>'\ s Irrigatjbn Data .:. .! Irri~ating Times Irrigating yolume H. t . Department of Human Resource& ·~-"v.;)t,.✓im11\· of Health Service& SAMPLE ANALYSES REQUEST State Laboratory of Public Hea P. 0. Box 280 306 N. Wilmington Str Raleigh, 276 C'-I 2-Slte Number __________________ Field Sample Number---------------- Name of Site fC B l /: Site Location ___ ,5 __ 4_...___l.;;..t_o_L/ ________ _ Collected By L; I<(.)~ //3. Lut5 ID# o, 2(051 Date Collected ___,/.:.a::{)e--__,2:c.,f#-=f_,_I._ ___ Time Type of Sample: 7 B_L Environmental ___ Groundwater ( 1) ~ Surface Water (2) __ Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments Upskeet""' <.£~d e I MOY 2 ! ·n ' I INORGANIC CHEMISTRY \ ) Extractable11 Total \, I Parameter Re1ult11 m1i/ 1 Parameter Re11ult11 mg/ 1 Paf amc.Js..r..-/" Re11ult11 mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ fluoride _TOC __ Silver __ Iron ----__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Resulu mg/1 _P&T:GC/MS __ Acid:B/N Exe. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls Parameter ~DB __ PCB's __ Petroleum __ Endrin __ Lindane Date Received _/_0_-_'~---:.9_-_...9_1;....· _,<3 __ .;..;~;;....._ _____ _ Date Extracted _I _0_-_3...,0 ___ ·· .... 'J .... l .... 1" ..... ~--J'M ........ ....._ _____ _ Results mg/ 1 Parameter Resulti; mg/ 1 __ Methoxychlor -<LJ, 000/-nnhl _ Toxaphene 7 , _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter Rei;ults PCi/ 1 __ Gross Alpha __ Gross Beta Date Reported _________________ _ Date Analyzed /1-/S-:9/-VP Reported By S13874 -------------------Lab Number __________________ _ OHS 3191 (Revised 7185) Solid and Hazardous Waste (Review 7187) . , N. C. D,~partment of Human Resource& ' Dlvli1on of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hea P. 0 . Box 280 306 N. Wilmington Sm Raleigh, 276 Site Number ----------------Field Sample Number __ C_(,_( ) ___________ _ Name of Site fC B (_ /: Site Location ___ .5_1<_. __ l_t_o_Y ________ _ Collected By L~ ftCJ~ / /3. l (,{ti; ID# Type of Sample: o, ?-(057 Date Collected --'l.'""'{)'---=z .. f_:9__,__,_I ____ Time /Jl ..,,._, /0_'/S Environmental ___ Groundwater ( 1) ___ Surface Water (2) V Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Re INORGANIC CHEMISTRY Extractable, Total Parameter Re11uh1 mail 1 Parameter Re1ult11 mg/ 1 Parameter Result, mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride __ Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ fluoride _Toe __ Silver __ Iron ----__ Lead -- --__ Manganese ----__ Mercury ----__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ I Parameter Results mg/ I _P&T:GC/MS ~DB __ Methoxychlor --Acid:B/N Exe. __ PCB's -<0,/0 'PPl;!j,,_, __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin --2,4,5-TP (silvex) --__ Lindanc -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls __ Gross Alpha __ (MPN) Coliform Colonies/lOOmls __ Gross Beta -------- Dace Received ___.;.J_0_·-_;)._9--'----'-9_1....;/3....;o...;· ....;ti)~-------Date Reported ________________ _ Date Extracted /0 -31 -9 / VP Reported By DHS 3191 (Revised 7185) Solid and Hazardous Wane (Review 7187) Date Analyzed /I-Ji'-9/--yp S13'·)7s Lab Number -------°'------------ ., , , N. C. @cpartment of Human Resources Drvlilon of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hea. P. 0 . Box 280 306 N. Wilmington Sm Raleigh, 276 Site Number ------------------Field Sample Number __ '7_G._l_t./_-___________ _ Name of Site fC B L f:.' Site Location ____ 5-';g"""· __ l __ t_o_tf ________ _ Collected By L ~ /?CJ~ / 6 · Lu~ ID# Type of Sample: 0'-2:(oS1 Date Collected __,i..,.(?_-_,Z::;;.,,~--j_,__I.._ __ _ Time Environmental ___ Groundwater (1) ~Surface Water (2) __ Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Re Comments clown s/recvv, INORGANIC CHEMISTRY Extractable11 Total Parameter Re11ult11 mii/1 Parameter Re11ult11 mg/ I Parameter Result11 mg/I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride _TOC __ Silver __ Iron ----__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results ma:/ I I Parameter Result,; mg/ I _ P&. T:GC/MS ~DB __ Methoxychlor __ Acid:B/N Ext. __ PCB's <t:, • ODO I .DDm .__ Toxaphene 71 _TOX __ Petroleum -2,4-D --__ Endrin --2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Rei;ults PCi/ I __ (MF) Coliform Colonies/lOOmls --Gross Alpha --(MPN) Coliform Colonies/ lOOmls __ Gross Beta -------- Date Received _J_0_-_,,,2. ___ 9 ___ -_<} ___ 1_JS __ d) ________ Date Reported ________________ _ Date Extracted _J_o _____ -3_0_· .... -9..,.1_16"""-,L~-',JM'---,.__ ______ Date Analyzed -.L./,.__/--=-=/f'c.--_fL..:..l _:YP..L.L ________ _ Reported By Lab Number _ .. S ._.·,1_...:"..,,.;o..._8.._7.&..:116J" ___________ _ DHS 3191 (Revised 7/85) Solid and Huardous Waa1e (Review 7187) '• N. C. Department of Human Resources ' Dl-vlii~n of Health Service, SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0 . Box 280• 306 N. Wilmington Sm Ralei11h, 276 Site Number _________________ Field Sample Number _w_li>_l5 ____________ _ Name of Site fC B l /:.' Site Location __ ,...5;.:i2.c::.· __ l-=t;._;:_o_t./...:._ ________ _ Collected By L ~ f?o~ / J5 · L ""t/j lDII Type of Sample: 0 w 2(0 57 Date Collected __,l.....,~_--=z~?._:fl--J-I __ _ Environmental ___ Groundwater (1) ___ Surface Water (2) _.lL soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) RC Comments d o vJr1 sfv--ea<b INORGANIC CHEMISTRY Extractable11 Total Parameter Re11ult11 m1i/ l Parameter Re11ult11 mg/ l Parameter Re1ult11 mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _Toe __ Silver __ Iron -- --_Lead ----__ Manganese ----__ Mercury ----__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY I Parameter Re1ult11 mg/ l Parameter Result11 mg/ I Parameter Results mg/ I _P&T:GC/MS -v!DB __ Methoxychlor __ Acid:B/N Ext. __ PCB's <0,70p,,:m-t-__ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin --2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Resulu PCi/ I __ (MF) Coliform Colonies/lOOmls __ Gross Alpha __ ( MPN) Coliform Colonies/ 1 OOmls __ Gross Beta -------- Date Received _._f_0_·-_;2-----"9_-_9 ____ /_,(]_£2. _____ _ Dace Reported __________________ _ Dace Extracted / 0 -J'/-9/-V P Reported By Date Analyzed ..L/...L.'/_-~/JC..Y:_-_.'7:u/'--~..¥,..L'P~-------- Lab Number ___ S,=)_.1._3_B_7_7 ________ _ DHS 3191 (Rcvi6CJ 7/85) SoliJ and Huardous Waste (Review 7 /87) N. ¢. [)epartment of Human Resources • .. •; D!vlz1!1.'>n of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0 . Box 280· 306 N. Wilmington Sm Raleigh, 276 Site Number _________________ Field Sample Number __ {,_'_C._l _"-___________ _ Name of Site fC 8 {_ f:: Site Location _ _.,,_-s_g __ l_t_o_V ________ _ Collected By L ~ f?o~ / 15 · l l<fEj ID# Type of Sample: o, 2(0 57 Date Collected ___ i __ {}_-___ 2__,,,__=/ ....... I _____ Time _</_._· i./-_o_ Environmental ___ Groundwater (1) ~ Surface Water (2) __ Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments UT Ups fr ea. ,N\ S;,.,. ,,.,..r;,/-e_ INORGANIC CHEMISTRY Extractable, Total Parameter Re1ult1 mii/ 1 Parameter Re111ulu mg/1 Parameter Re111ult1 mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _Toe __ Silver __ Iron ----__ Lead -- --__ Manganese -- --__ Mercury ----__ Nitrate -- --__ Selenium -- -ORGANIC CHEMISTRY Parameter Resulu mg/1 Parameter Result• m.:/ l Parameter Results mg/ 1 _P&T:GC/MS -v!;DB __ Methoxychlor __ Acid:B/N Ext. __ PCB's <o, ooo 11f.-rrL __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin __ 2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/l00mls __ Gross Alpha --( MPN) Coliform Colonies/ l OOmls __ Gross Beta -------- I o -.;J. 0 -9 I .£' & Date Received _____ / ______ X_:J , _______ Date Reported __________________ _ Date Extracted JO -3 0 -91 J/J;aM, Reported By Date Analyzed ..... / .... '/__,-/'7Y.T'3f"-"'lf'2~(.,:-"0~nlt'e_"'1i1""',,-----------$1J8'78 -------------------Lab Number __________________ _ OHS 3191 (Revised 7/85) Solid anJ Hazardous Waatc (Review 7187) .. N. C. Department of Human Resources ' Divlilo'n of Health Serviceli SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0. Box 280 306 N. Wilmin11ton Sm Raleigh, 276 Site Number ------------------Field Sample Number __ C._G,,_· _1_'1 ___________ _ Name of Site fC B L /: Site Location ----~;..;t.Z""'· __ l...::t_;...o_tf...;.._ _______ _ Collected By L ~ f?o~ / I)· L (,(ffj ID/I 0 G 2(0 57 Date Collected _-Jf.u.:tZ:....-~2.:::.,'J,..._:1-+--lc-__ _ Time o/' _''-fo Type of Sample: Environmental ___ Groundwater ( 1) ___ Surface Water (2) --iL Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments LA p s-J-r~,,vi_ INORGANIC CHEMISTRY Extractable11 Total Parameter Re1ult11 mii/ l Parameter Re11ult11 mg/ l Parameter Results mg/ l __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _TOC __ Silver __ Iron ----__ Lead ----__ Manganese ----__ Mercury ----__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Resultll mg/1 Parameter Results mg/ 1 Parameter Results mg/ 1 _ P& T:GC/MS ~DB __ Methoxychlor __ Acid:B/N Ext. __ PCB's <0,10 ~ __ Toxaphene I I _TOX __ Petroleum _2,4-0 --__ Endrin --2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls __ Gross Alpha __ (MPN) Coliform Colonies/lOOmls __ Gross Beta -------- Date Received ~/_0_-..2_9.:....._·_-~9_;___;,J3.;.;:;._£}_..;;;..;:. _____ _ Date Reported __________________ _ Date Extracted -,,~J .... ~_,-3,__,._'/_-_,_f-1../ __ '1/io:;....,&.P _______ _ Date Analyzed ..,.l,_...'/_-.L,.J..,.F_-~9c....Li:....16..L..:.P ________ _ 913879 Reported By -------------------Lab Number __________________ _ OHS 3191 (Revised 71B5) SoliJ and Hazardous Wu1e (Review 71B7) I N: C. Department of Human Resources ' Div!-tl6n of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hea P. 0. Box 28( 306 N. Wilmington Str Raleigh, 276 Site Number ________________ Field Sample Number _..;;;6...:·ec,~/~G'------------ Name of Slee fC B L /: Site Location ___ ,5;..:iZ~• __ l-=6:....:..o_V.,:._ _______ _ Collected By L., f?o,;:,,c. / I)· Lu~ ID# Type of Sample: 0, 2( O 57 Date Collected __.lu:tZ'---__,z::::..,·~F----f~I.__ __ _ T. lJ:3,o 1me ____ _ Environmental ___ Groundwater ( 1) ✓ Surface Water (2) __ Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid ( 6) __ Sludge (7) __ Other (8) l< T Comment1 l>v u.J t1. slv f!1 (V\ .SC 7 ' ~ INORGANIC CHEMISTRY Extractable, Parameter Re1ult1 mi/ 1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury __ Selenium __ Silver -- -- ---- -- Parameter Results mg/ 1 _P&T:GC/MS __ Acid:B/N Ext. _TOX ---- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls -- -- Dace Received / O -,,2 7 -CJ I /3 £2 Date Extracted / 0-go-9/--VfJcTM Reported By OHS 3191 (Revised 7/BS) Solid anc.l Huardous Waate (Review 7187) Total Parameter Re11ult11 mg/ 1 Parameter Re11ult1 mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _ms __ Fluoride _TOC __ Iron --__ Lead --__ Manganese --__ Mercury -- __ Nitrate --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ I Parameter Results mg/ I ~DB __ Mechoxychlor __ PCB's < tJ , oo o/ ,Ql/1"' __ Toxaphene , ~ __ Petroleum _2,4-D __ Endrin --2,4,5-TP (silvex) __ Lindane -- RADIOCHEMISTRY Parameter Results PCi/ I __ Gross Alpha __ Gross Beta -- -- Date Reported _________________ _ Date Analyzed -1-J//½:-~/~Y-=-_.Z'-4'/_jl;.L..L,p ________ _ S13880 Lab Number __________________ _ I ,, ... N. C. ,Department of Human Resources · · [)(vla'ion uf Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0. Box 280· 306 N. Wilmington Sm Raleigh, 276 Site Number ________________ Field Sample Number __ &_'-_f C/~---------- Name of Site fC 8 l J:.' Site Location ___ .5::..:t?.~· __ l..:t:....;;..o_'-1...:.... _______ _ Collected By L ~ f?v;;;.c. / J5 · L U~ ID// Type of Sample: tJ 6-?::( 0 51 Date Collected -....1lui::();....-_,Z~,,__=f~"-I __ _ 0~3 0 Time_ .... z __ _ Environmental __ Groundwater ( 1) __ Surface Water (2) _£Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Other (8) UT Comments Pown.sfreo.. n INORGANIC CHEMISTRY Extractable, Total Parameter Re11ult11 m1i/l Parameter Re11ult11 mg/ I Parameter Re11ult11 mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _TOC __ Silver __ Iron ----__ Lead -- --__ Manganese ----__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Re11ulta m1i/ I _ P&. T:GC/MS __ Acid:B/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls --(MPN) Coliform Colonies/lOOmls Parameter ~DB __ PCB's __ Petroleum __ Endrin __ Lindane Date Received / 0 -;l_ 9 -9 / /3 if} Date Extracted /O-3/-9/YP Results mg/ I < CJ I LO f?/?rt1.... Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ I __ Methoxychlor __ Toxaphene _2,4-D --2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 Date Reported _________________ _ Date Analyzed ... /:;.../;._-_/.'-"'y..l<.--..... 9'-"I_Y,¥-LP ________ _ Reported By ----------------Lab Number __ S.;;;...~_1_3_8_·8_1 _________ _ DHS 3191 (Revised 7/85) Solid anJ Huardous Wute (Review 7/87) .. N. C. Department of Human Resources Dlvlalon of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Type of Sample: Environmental ___ Groundwater ( 1) ___ Surface Water (2) ~Soil (3) __ Other (4) Concentrate __ Solid (5) __ Liquid ( 6) __ Sludge (7) __ Other (8) Time_~_O_._''f: ___ ~ __ _s . -e.. t.Q LF. INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results mg/1 _P&T:GC/MS ~B __ Methoxychlor __ Acid:B/N Ext. CB's <o,[O .pp.m..-__ Toxaphene 1 _TOX __ Petroleum _2,4,D --__ Endrin __ 2,4,5,TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls __ Gross Alpha __ (MPN) Coliform Colonies/lOOmls __ Gross Beta -------- Date Received __,_/_0_-_:2._CJ_-_9_/_,<3c....::::....::£}....:...._ _______ Date Reported __ ...J./"-"0'-l-~~~/~9::...../L..-________ _ Date Analyzed -"'/_,,,/'--=--_./'::---"".S'------L.9 ..... /_1/p.L..,L ________ _ 913872 Lab Number __________________ _ Date ExtracteM ~!-v = Reported By ~ o{;_ ~ -= DHS3!91 (Revi a 7/85) ~ 5 P Solid and Hazardous Waste (Review 7187) ~7 / 0 7 z_. -· 7' r 3: g'-g j N. C. Department of Human Resources Dlvlalon of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0 . Box 2804 7 306 N. Wilmington Street Raleigh, 27611 9~-// Site Number ___ .::::> ______ ..,.-_______ Field Sample Number ____ O_o_S_.;..3_--r-_· _o _______ _ Name of Site Pc 8 la. hit I I Site Location __ S_R __ J _6_o_Lf-_...:;w_,.__ci_r-...;.r_e_,...;. .. _a_k..,_l1-h.~,,_ J Collected By Type of Sample: L lA. TF Y ID# 0 S9 Date Collected / 0 -;;; f-1 I Time /I : I 5" Environmental Concentrate Comments __ Groundwater (1) __ Solid (5) Lea Chlf.le I rt-Pk.en. f __ Surface Water (2) ~ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable, Total Parameter Results mg/ l Parameter Results mg/ l Parameter Results mg/1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _Toe __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ l Parameter Results mg/ l Parameter Results mg/1 _P&T:GC/MS ~B __ Methoxychlor __ Acid:B/N Ext. __ PCB's <0,000 Lf/21tt.. __ Toxaphene _TOX __ Petroleum _2,4,D --__ Endrin __ 2,4,5,TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls __ Gross Alpha __ (MPN) Coliform Colonies/lOOmls __ Gross Beta ---- ---- Date Received _/_0_-_~_9_-_°t_J_IJ_·_JJJ _______ _ Date Reported __________________ _ Date Extracted ...,J:_0~-.-3"-0_-.... 9. ..... 1/_Y)......._70....j..><JM~,....__ ______ _ Date Analyzed //-/S-Vyp Reported By ~1~ci73 Lab Number ____ -__ -_o ____________ _ OHS 3191 (Revised 7185) Solid and Hazardous Waste (Review 7/87) Chain of Custodv Record '"': . . Hazardous ~aste Hacerials Location of Sara?ling: Generator Company's Name Address __ Storage Facility Other: !Ja {--reV'I __ Transporter Tre~cment Facility __ 0isposa 1 Fae i l icy ._/'iand f i 11 Telephone ~ o l lec tor's Name _____ t ____ oh;...b....,v,_·' __,_[_VL...;..;...f...:..£~-~--- -Signa tu re/ :,at;.e Sampled ID --i. f --f f Time Sampled _ _;... ________ ,_ ___ _ ~pe of Process Generating Waste -~ ie ld !nforma tion . I :.c:ld Sample ~o. ~ai~ of Possession: .. nae e r. it le incVusiJe dates signature title inclusive dates .".csu~ts · reported . ~ ,<to.~«-~ title 1 dat~ ' lnsc=uctions: Complete all applicable. information including signatures, and submit ~ith analysis request forms. .. Location of Sampling: Company's Name Address Chain of Custodv Record Hazardous Waste Hacerials Generator _Storage Facility Ocher: __ Transporter __ Disposal facility Telephone / Tre~tment Facility VLandfill '.: o l lec tor's Name -----/S----.;)_b_b-1,y_· __.L=vt..::..f_!~--...:...---- 1. 7 Telephone (7/y ) 73s~ o 6,7.;;J.__ -signature ID~ .:i._ 9 -Cf J :,a~e Sampled Time Sampled_-----------,,------ :: i:> e Of process Gener at i ng Waste _. __ ._f _o.:.>'_'_. c_· __ w~· ;..a._~_/4 _ __,;;;D;..'...;' s:1f,./~?o;;.S""-:.:.:...I _Jl...fi~~:...;C:;.:<_· ;_.(,o/7----------- -~ ie ld !nforma cion :.ald Sampte ~o. 5 3 ,39 ~a~~ of Possession: .. title incL6sive7 daces signature t.i c le inclusive dates :.csu~ts · reported signature title date lnst=uccions: Complete all applicable. information including signatures, and submit ~ich analysis request forms. .. . ' '1. C. Department of Human Resources )!vi,ion of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0 . Box 2804 7 306 N. Wilmington Street Raleigh, 27611 ,ite Number 93 L c>i. V\.Jt, · r I Field Sample Number Oo 7 1 </71 \Jame of Site Pc& ::::ollccted By L UT~Y ID# rypc of Sample: Environmental Concentrate __ Groundwater (1) __ Solid (5) __ Surface Water (2) ~ Liquid (6) __ Soil (3) __ Other (4) __ Sludge (7) __ Other (8) o s-c; Site Location s /(_ !6ot.f l! 2a.. ir -re .;.--, Ge., ,__·fv / Date Collected !cJ-,;i_Cf -C/r Time ( r: rs- Comments l e0-ch..t?.../e k -H~e.-tT INORGANIC CHEMISTRY Extract.ables Total Parameter Results mg/ 1 Parameter Results mg/1 Parameter Results mg/ 1 __ Arsenic / Arsenic ~ a _ o \ _i:5 ii Ver L.. o . c.'.;J __ Barium ✓Barium O.A l.9 /4' 4-j ~ _..LSulfates __ Cadmium /cadmium L o .cc5 / o _ le~ ~ _line __ Chromium v Chloride ·1 I _!::_ Ph b .. C/ l __ Lead V Chromium L.o.c.1 __rtanducci vity IJ.~r-, --..."l"--9"'-.c.:..... __ Mercury ~ L.. O.C~J ~ms b-:Jf. I __ Copper __ Selenium 19,luoride a .en __ TOC r3ij.,; 1' .... .,_ .,_-t--00 \.r~ """- __ Silver __ Iron ~~. ~o L,/ .4/ /4.t:Ji" : +-v . f z {~- --~Lead L-o -cc-6 ~ //f1,,u1h.es i'·..-..,i,..,._ 3:.,. -~ 'c ~Manganese . o . ~✓...., ,/ ---- --~ercury L o.ccCJ-. -- --__ Nitrate L... \ .Qo -- --~eleni u ~ ~c .cc'q -- ORGANIC CHEMISTRY Parameter Results mg/ 1 _P&T:GC/MS __ Acid:B/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lO0mls Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane )ace Received _________________ _ Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/1 __ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 Date Reported __________________ _ )ate Extracted ------------------Date Analyzed -r-i-r-:--r-.,......,~------------- Lab Number O 1'-Jodo OCT 30 --; i leported By )HS 3191 (ReviscJ 7185) olid and Hazardous Waste (Review 7/87) Chain of Custodv Record Hazardous ~aste P.aterials Location of Sa@?ling: Generator Company's Name Address ~olleccor's Name :,a t;e Sampled __ ._Storage Facility Ocher: __ Transporter Tre~cmenc Facility __ Disposal Fae i l icy VLand f i 11 Telephone Telephone ~<~f_r~f~l--'~Z~-5~3;;.._-_o~~.....L.r ~-2.;::_ ___ _ Time Sampled_...;_ _______ _,,--___ _ ::?e of Process Generating Waste · fo ;,<(c t..la_.s/4. U,!fd?v..s ... I r;._c, l ty ~ield Information Coo l I . 77. L-i -/l e., f Ja_ A p ie " :.cld Sample Xo. ~=~~ of Possession: .. title inclusile dates signature title inclusive daces date ? !nst=uccions: Complete all applicable. information including signatures, and submit ~ith analysis request forms. .. ' . . ' _.,, 1--; -· N. C .. Dcpartment of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 2804 7 306 N. Wilmington Street Raleigh, 27611 Site Number _...,;1/L...;J""----------------Field Sample Number ___ ~_,_<!?____.,··'!£,..:::....· _________ _ Name of Site -~B-~__,;B ___ L_t:'___________ Site Location __ ..... 5.:..:a.:,,...._/-=·t;._;;_o_tf~--------- Collected By L~ /(c;~ / &. lutfj ID# 06, 2(057 Date Collected __./.=p_---=2~~=--=f,__,_I __ _ Type of Sample: Environmental _L Groundwater ( 1) Concentrate __ Solid (5) __ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) Comments INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride _TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Resulu mg/1 _P&T:GC/MS __ Acid:B/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lOOmls Parameter ~DB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter Results mg/ 1 __ Methoxychlor ~'-J.OlJOI -Toxaphene --r7 _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter __ Gross Alpha __ Gross Beta Results PCi/ 1 Date Received -l-''::..H~...µ1...1--=~~-'-----------Date Reported __ _,c./._,'/'-----<-0_---"'?~./ _________ _ Date Extracted £P-'-4'-=:;.:..L-JL.J.--L4-~TM.._:__-=. ______ _ Date Analyzed _,,_/,_Q,_-_.;:;_~...::;.~.L.,_--,L,9,c_L_J6-L-1.p _______ _ Reported By ~ Lab Number _____ 9_1_3_8_6_~1 _____ _ OHS 3191 (Revi 7185) Solid and Hazardous Waste (Review 7187) . •N. C~ I.'>~partment of Human Resources ... ' Divliion of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Hea, P. 0. Box 280 306 N. Wilmington Sm Ralei11h, 276 q1J ·-d ,/~ .Site Number --../-I-JI<.,~---------------Fie! Sample Number ---,"2 ...... ~-_,-,___ __________ _ Name of Site fC B L /:' Site Location _ _.-._'S __ i< __ l"--t_o_tf ________ _ Collected By L~ f?Q~ / I). Lutq ID# 06, 2(o5l Date Collected ___..l_(Z_-~2_·'8'_=/_ .... I ___ Time .J. ·1 I £ Type of Sample: Environmental ~ Groundwater ( 1) Concentrate __ Solid (5) __ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable, Parameter Re1ult11 mKI 1 Parameter Re1ult11 mg/ 1 __ Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium __ Chromium __ Chloride __ Lead __ Chromium __ Mercury __ Copper __ Selenium __ Fluoride __ Silver __ Iron --__ Lead --__ Manganese --__ Mercury --__ Nitrate --__ Selenium ORGANIC CHEMISTRY Parameter Re1ult1 mg/ 1 Parameter Re1ults mg/ 1 _ P&. T:GC/MS Comments Total Parameter __ Silver __ Sulfates __ Zinc _Ph __ Conductivity _TDS _Toe -- -- -- -- -- -- Parameter -v!DB --Methoxychlor __ Acid:B/N Ext. __ PCB's <o. o o o /,1!PM __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin --2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Re1ult1 mg/ 1 Results mg/ 1 Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lOOmls --( M PN) Coliform Colonies/ 1 OOmls __ Gross Alpha __ Gross Beta Date Received -~-J-,J&a..L...,r...:.......:__::;~:......:..;..i,... ________ Date Reported _________________ _ Date Extracted / Date Analyzed JO-.;J 9 -9/J(p Reported By --------------Lab Number 913862 OHS 3191 (Rcvi~<l 7/85) Solid 1&nd Huardous Waatc (Review 7187) ' ' , .. N. Q.' qepartment of Human Resource& Dlvlalon of Health Service& SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0 . Box 280 306 N. Wilmington Sm Raleigh, 276 .Site Number ___ __,q"-=J'-. ------------Field Sample Number ..M'2""'k"'-'-/..;;D'-------------- Name of Site -~fi_t:.";;_.;::B..__ __ l_/:_-,--_________ Site Location ___ .5:..:.i<::,,,,,..._l.:;;.t....:o;__tf,;___ _______ _ Collected By L .. f?u~ I&. L ut1 m11 06, ?:f osr Date Collected l(Z-Z'ff--11 Type of Sample: Environmental Concentrate Comments v ___ Groundwater ( 1) __ Solid (5) r;w-3 __ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable11 Total Parameter Re11ult11 m1i/ 1 Parameter Re11ult11 mg/ 1 Parameter Re11ult11 mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _Toe __ Silver __ Iron -- --__ Lead -- --__ Manganese ----__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Re11ulu mg/ 1 _P&T:GC/MS __ Acid:B/N Exe. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls Parameter -v!;DB __ PCB's __ Petroleum __ Endrin __ Lindane l o IJ Date Received -"--+""rl-..'-'-'--+-'-~---::::::;i:;;.:,_....:..1 _______ _ Date Extracted ....,l __ CJ_-__ ~'---"CJ'-----9 .... J'---'::0......_7?,+ . ...,Cfl\'-'-I\...._ _____ _ Reported By OHS 3191 (Rcvi&cJ 7/85) Solid and Huardous Waatc (Review 7187) Results mi/ 1 Parameter Results mg/ 1 __ Methoxychlor <o,ooo/ f72'4\.-__ Toxaphene -2,4-D --2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter __ Gross Alpha __ Gross Beta Results PCi/ 1 Date Reported _________________ _ Date Analyzed __./_,,t:J,e;,__-=.;J..,,_9i<..--LZ.!...1/_1t)?~:;,___ ______ _ o_:.1~.of-3 Lab Number ______ __;::;__'L6_Ci _________ _ .>N. t :. O~partment of Human Resources • Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Heal P. 0 . Box 280- 306 N. Wilmington Sm Raleigh, 276 ,Site Number _..,,f..::;J_-_____________ Field Sample Number __,,/a""-"'"----'/'--·-/ __________ _ Name of Site fC B L /:' Site Location ___ .5:..:tZ.:i.· __ l-=t:....:;..o_L/..;._ _______ _ Collected By L ~ I<~~ / IJ · L "'i-F; lD# Type of Sample: 0 C, 2( 051 Date Collected ___,fi'"""/Z_-_,2:::c..·.;..cg-_:1_1.__ __ _ ~ :JS-Time -~-'----- Environmental \/" Groundwater ( 1) Concentrate __ Solid (5) __ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) Comments INORGANIC CHEMISTRY Extractable11 Parameter Re1ult11 mii/1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury __ Selenium __ Silver -------- -- Parameter Re1ult11 mg/ l _ P&.T:GC/MS __ Acid:8/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/lOOmls __ (MPN) Coliform Colonies/lOOmls Total Parameter Re11ult1 mg/ 1 Parameter Resulu mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _ms __ fluoride _TOC __ Iron --__ Lead --__ Manganese --__ Mercury --__ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~DB __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/ l Parameter Results mg/ 1 __ Methoxychlor <o.o oo~ __ Toxaphene _2,4-D --2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter __ Gross Alpha __ Gross Beta Results PCi/ 1 Date Reported _________________ _ Date Extracted _._=-. ....... ....&...-......... _...._.µ.4_..,._ ______ Date Analyzed _l_.ooe.._-_.,~:..::....:;9_-..L-9..L'I_J(PIJC-L. ________ _ 91386 /IJ Reported By -------------------Lab Number _________ ••---------- OHS 3191 (Revised 7185) Solid and Hazardous Waste (Review 7187) ·• •. l.oc·uion of Sara?ling: :ompany's Narue \ddress .. _. _ -_ • -4.l ~ ._. ~ I • .,. (. C l J. '1 1 S Ccncrar.or _Scorace Facility Ocher: _Transporr.cr __ Disposal facility l F /PEp-r OF ffet11'vr517lA7/l!Jfd.1cph.onc Trca crncnt L1c V Landfi 11 a lt'f ·7.3 :2 -o ~ q '2 Tc l c phone -1CL~_).._~~=--;7 _______ _ :,at; c Sampled ___ l tP __ -___ 2..;;fl ___ --_q.f _________ _ Time Samp 1 ed _ _;_ ________ -,-__ . 1~e of Process Ceneratinc Wascc ·teld lnformacion !cld Sampte Xo. ,6 10 l/ydt'P66<??f?G:IC&-?µ,bf · cir.le c.iclc r. i. c le i11clu!ii.vc date!> csu~cs · reported j}& C. i. c. l C d.itc nsc:-ucci.ons: Comjlletc all applicable. information incluciinc si~nacurcs, and subiui.r. ,,_. i ch .: n i1 l y:. i. s r c 'I u cs t:. f o nu:. • .. f,J 0 :....:.., 0 o-: CJ u IJ .... u ,n 01 0 11 1J ..... (/) U- .J 11 ,, m ,,., "' u . .-, l/) ~ I N ' C - 11 11 <I! 0 u u m JJ r:: 0 ,,....u ') r' 11 SI u 'U ..... I l/l ·-· C: "' 1/1 ,n ,n 11 1, .,.., -,1 .-(. 01 tJ . .-, (/) >, u r:: :·, 0 u ~ ,,,, J.I .. , r: ,, 01 i:i.. --• 11 11 u (/) ,,, ,n 1' ~•·' r: ·-· ,,, LI V1 II (n (/) -~ _, 11 11 JJ (/) II (/) OI 11 11 V1 ' m 0 I l/) 0 1\1 'D .... ~· () -· .c: u ..... , :,., r:: ·-· > >, _, 0 n. II r J .--. Cu •n e 0 ·-· u m •-1 ~-11 I .I .r.i .0 --i: n. ::' .v. (J .... IJ (/) IJ_, 0 a. C f-J i: Q I.J I.LJ .r:: I.I n. 11 C l I.LI 0 1\1 "-1 ·~·· l/) lu 0 11 o. >, I-' ,,, J.I r; 11 r: 1_: () u J.I .r: "0 .. , 01 ::i; .... , 0 I I 'II ,u r,, ,,,, r: •P•' '" ,11 u 1, 11 JI :) 0 '10 C .. , in "' u '>O c; .. , ,n m u _, 1, 11 C: C . .-, 110 r: •• 1 "t1 r: m tJ (f) I.• '\I 1• ,,, :?- \J 01 JJ :, 0 1., 11 C: C ..... ,, 11 J.I :1 0 \, 11 r.: r:: .... ~ ~ ... ~ ·- ~ tr---~ t'--- ~ ~ -::. ~ ::: ~ (/) ';;fJ (j"" :j-.., -.. ~ \<"I -"'" c-l N V) t"'-- ' ~ tl't t-4 t'lc) ti -0 c,,... ~ .. ~ ~ ~ ~ ~ < ~ ~ ~ :: ... .::. . ~ ~ ::t-- V) VJ V) 'l. C. Department of Human Resources )lvialon of Health Services SAMPLE ANALYSES REQUEST Scace Laboratory of Public Heal ch P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 ,ice Number -~---------------Field Sample Number __ 7-+-..... /-'R-'-~o:;___--,--------~ '-lame of Si Ce _;P,__, .....1.C--'.'--!' p_).,___~Lu..V....::.v..:..i..1 r_;;f----:.(.....:..;.....1../...:..I_____ Site Location SR. I bO t/ (U cl' e I-' f7 t,1 , (~,G.{,(jt, <f--v -,ltf; I . IO# 0 5'1 Date Collected /0 /zlc;; Time //(J--Q (/ ::::ollected By a-1 1 fype of Sample: Environmental Concentrate Comments ___ Groundwater (1) __ Solid (5) f~~a:111 , ft' B ___ Surface Water (2) __ Liquid (6) __ Soil (3) __ Sludge (7) I ___:d_ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractable& Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ .Arsenic 1Arsenic s: {)_, Q / LS il ver L_;'ef~ __ Barium ._/Barium Q. s-1:J ~Sulfates __ Cadmium 2cadmium S::QL Q(~ ,,;;-Zinc ,-2 l' __ Chromium •i :hlori~e .,, i/.ph ~-] __ Lead Chromium <:'Q.Q { =:;: Conductivity i ·)., P..c ·~ :l--~~-0..: __ Mercury --h,L.Copper ~D-.::: <::;; _ms &,._. , .. ,) ~ '-- __ Selenium ==2{luoride Q .'.3: I _TOC __ Silver ' Iron j:_/ .. 5,;.j ~i-:.~ui::::.:1 diS~ --_iLLead j. Ci t. ;.:z .....--Al'. I<:./; I,<, I +y:. 5So --_.LManganese Q .. .55 <--------s.:. J ; .; ii.A.. '-t l' --__i_.:( Mercury L_,::::i • ~e,C 3-., -- --fNicrace .L.... \~ QO ---- --__ Selenium < Q ,. c2. {2 ,::;--- ORGANIC CHEMISTRY Parameter Results mg/ 1 _P&T:GC/MS __ Acid:B/N Ext. _TOX -- -- MICROBIOLOGY Parameter __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lOOmls Parameter _EDB __ PCB's __ Petroleum __ Endrin __ Lindane )ace Received _________________ _ )ace Extracted _________________ _ Results mg/ 1 Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ 1 __ Mechoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 Dace Reported __________________ _ Date Analyzed -7""'".-:---.,--:---------------- '.leported By 0 I o22S OCT 7 :,:; 1 1 -------------------Lab Number _________ .:.__~-------- )HS J 191 ( ReviscJ 7185) olid and Hazardous Waste (Review 7187) Chain of Custodv Record Hazardous Waste P.ctcrials !.ocation of Sampling: Generator __ Transporter Company's Name .-\ddress __ Storage Facility Ocher: P c-_·~ I r r)f. , _ -....2. 1,%,1 Ci. rz " __ Disposal facility Telephone IOV 2 0 191 1 __ Treatment Facility La.n.oif'/1',i::i ;::: ::~1~ ,; ~-.: ~olleccor's Name /;,/,fy L,:._ -fr; Telephone _._(..._?I __.7)._?r---3_3_0 ___ -.... f ..... 7_.;;Z=-. __ -si gnature __ :,at;e Sampled /() /c7-/91 . · · . , , Time Sampled ---+./...,/_0-_,Q..._, -----.-----/ 7 ' , ~?e of Process Generating Waste ~ield Information :.c:ld Sample ~o. 7 /f?C ~ai~ of Possession: signature ' I) . \! l) ,, ; I , I daces title inclusive da t es title inclusive dates title date · 1 !nsc=uccions: Complete all applicable. information including signatures, and submit ~ich analysis request forms. .,; ,., . N. C. Dt:partment of Human Resources Divlalc;m of H~~lth Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0 . Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number ----------------Field Sample Number __ O'-'{...,,)...,5..___.l/-._4-.........,0....__ _______ _ Name of Site />c _g l{lnd-ft ' f ( Site Location __ s_· .;_R-_....:...{..:;..6_0 ...1.'f: _ _..:;..M_ct=..!..r..:..v-_:~:;.:.Yl~(o:;_~_;_t ....:..." -7..t-- Collected By /!,ot>h f LIA +47 ID# _O_S--<f__,_ __ Date Collected / 0 -7 -1 f Time l I ! Z)o Type of Sample: Environmental ~e __ Groundwater (1) __ Solid (5) __ Surface Water (2) V Liquid (6) __ Soil (3) __ Other (4) __ Sludge (7) __ Other (8) Comments L' V\. +kt e.. ""' +- INORGANIC CHEMISTRY Extractable& Total Parameter Results mg/ l Parameter Results mg/ l Parameter Results mg/ l __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _ms __ Selenium __ Fluoride _TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results mg/ l Parameter Results mg/ l _P&T:GC/MS _EDB __ Methoxychlor __ Acid:B/N Ext. --1.LPCB•s __ Toxaphene _TOX __ Petroleum < 0 d>OO / ,P/2-A =-2,4-D --__ Endrin __ 2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ l __ (MF) Coliform Colonies/lO0mls __ Gross Alpha __ (MPN) Coliform Colonies/lO0mls __ Gross Beta -------- Date Received lo -7-q; II A f>el5~· D"e Extrnct<~.. ·C/f"Ye 1JJG Reported By . c;(? OHS 3191 (Revised 7/85) Date Reported / () ....-dz:::~ ? / PC$s-, Date Analyzed /0-~3-9/ 1/P S136J1 Lab Number __________________ _ Solid and Haza rdous Waste (Review 7187) Location of Sampling: Company's Name Address S. R.. Chain of Custodv Record Hazardous Waste Materials Generator __ Storage Facility Ocher: __ Transporter __ Disposal Facility Telephone Tre~tment Facility L.-/(a nd f i 11 ~ o l lec co r ' s Name _......._/],_c,_. b_b....,ff---· ___.L=-LA_-f-_£;_,,,____._ ___ _ Telephone (Cflo/) IJJJ-Ob 1/L -signature :,a~e Sampled i0 -?-17 11 :oo Time Sampled_~....;_-------,.----- ::pe Of Pr oce S S Gener at i ng Wa SC e _-__ -_r_o_)(_,_'-_w __ ~_s-_l-e._ .. ?...;r:...;:f-'r;;..S::.ol.;.;f___:fi.;_~~..j.-(_,< '7-1~----------- ~ield Information :.cld Sample ~o. DOS:4-L/ b ~=~~ of Possession: signature title inclusive dates signature title inclusive dates .".csu ~ ts reported signature title date lnst=uctions: Complete all applicable information including signatures, and submit ~ith analysis request forms. . ,, State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary October 1, 1991 William L. Meyer Director MEMORANDUM TO: Mr. James Rhodes, Deputy Secretary Department of Administration FROM: Larry Rose, Hydrogeological Technician µ_. Solid Waste Section RE: The PCB Landfill Monthly Inspection The PCB Landfill Monthly Report for the October inspection is enclosed for your review. Burrowing activities of what appear to be resident groundhogs continue to be a problem at the landfill. Three active den entrances were found within the fenced perimeter during this inspection and control measures should be taken to prevent possible damage to the liner system. The pump was repaired since the last inspection, allowing the leachate to be pumped during an earlier routine visit this month; however, it failed during the scheduled inspection and is in need of repair again. Excluding the minor problems discussed, the overall condition of the landfill seems to be good. If you have any questions, please call this office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Employer .... ... .... .. \.,_ Pco LAflDf ILL hUL,l HLY h..i.:J:'Oi:U' 1. Entrance Road 2. Monitoring Wells Casings, locks · Fences, gates, locks .) . Landfill fence, gate, locks fj • Air Vent ,. .) . Landfill Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface lmpoundment Erosion, vegetation 10 . Irrigation Syste~ Influent Piping Pump Sprinkler Units . NAME L ,11,r-Ln y I O ~,., ------'---------'------- NO PROBLEM ✓ / V v l.,·/ t,/ / V ✓ ./ It ✓ -17 / --- t/ ✓ ,/ ✓ ✓ (,/ POTENTIAL PROBLEM ✓ ·✓ OBSERVATIONS c:./x/J<lc .EO J-::'; //;N6 .: PC3 LANDFILL MONTHLY REPORT (CONT. uATE 1-3o -91 NAME L,? ;-y 1 -----= ....... -"----------. ..,, ; Pumping Data Pumping -Times Irrigatjbn Data Irrit·a·ting Times Irrigating Volume I \ . l __ \ " .. ---------------------------------- 9-3o-9/ .. Lt,--, 1/' ,.e C ,,{~ l l( L/3 '-f ' 3/'f I c; --,_ l/i/ ,, L/ I J. ,, f.,, 1I I ,, ., N. C. Department of Human Resources Dlv~ion of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number _-1,.9_;;3'----------------Field Sample Number ___ -=5''---lf'------''f_-_.S--=-------- Name of Site ?CB Lp Site Location SR /wO 'f Warren U)(.,(~7, Collected By &b~f k ·ffr ID# _...::;;(!)_S----J-9_· _ Date Collected _,.LC/_---'-/i_,_/_---'qL.L; ___ Time IO" '/:0 Type of Sample: Environmental Concentrate Comments __ Groundwater ( 1) __ Solid ( 5) Le4c/44/e Sa._,._,p/e., "'' __ Surface Water (2) ~Liquid (6) __ Soil (3) __ Sludge (7) __ Other (4) __ Other (8) INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride _TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium --- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 _P&T:GC/MS ~DB __ Methoxychlor __ Acid:B/N Ext. CB's <o, 000/-f'l»!J, __ Toxaphene _TOX __ Petroleum _2,4-0 --__ Endrin __ 2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/lO0mls __ Gross Alpha __ (MPN) Coliform Colonies/lOOmls __ Gross Beta ---- ---- Date Received -'----'-----''---L.._..___._ __________ Date Reported __ __,,_9_--=e<:..i.....3"'----.L.9__,_J ________ _ Date Analyzed _.q,__-....,/'--''7'----;...9 f~:161'-1---P _________ _ Reported By Lab Number ____ 9~1=.J=-.:.:~·=--•0~0-=--------- DHS319l(Rev· 7/85) Solid and Hazar ous Waste (Review 7187) Purpose: Enforcement and compliance with the N. C. Solid and Hazardous Waste Management Rules. Preparation A sample analyses request form (OHS 3191) must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one (1) container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate. Do not submit an analysis request sheet with no parameters indicated. Equivalent measurements: ppm= µg/ml = mg/1 =µgi g= mg/kg ppb = µg/1 = µg/lO00g = µg/kg DEFINITIONS/INSTRUCTIONS Site Number -A twelve,digit site/location identifier, assigned only by the district field representative. Field Sample Number -A six,digit sample identifier which is pre,printed on the sample label. Name of Site -Name of landfill, facility, etc. Site Location -Address, street number, state road, etc. Collected By -Name and ID of sample collector. Date and Time Collected -Self,explanatory. Environmental -A sample of a naturally occurring substance such as groundwater, surface water or soils which may be contaminated. Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed wastes. Comments -Lists details regarding sample or sample point, including but limited to, phase separation, and/ or od9rs. · lnorpnic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. Extractables are only performed on a solid or semi,solid. For routine landfill samples, check all parameters in the second and third columns. Organic Chemistry -Check { ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the space provided. Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for either of these. Distribution: 1. Original to State Laboratory of Public Health Environmental Sciences Branch P. 0. Box 28047 Raleigh, NC 27611 2. Lab sends copy to Solid and Hazardous Waste Management Branch. 3. Solid and Hazardous Waste Management Branch sends copy to field person. Disposition: This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History. Additional forms may be ordered from: Solid and Hazardous Waste Management Branch Division of Health Services P. 0. Box 2091 Raleigh, NC 27602,2091 l...ll<il.11 Ol ~USC.OU\" P.ecorG Hazardous ~aste P.aterials !.ocat ion of Samp l.ing: Genera tor __ Transporter Tre~cment Facility Company's Name Address __ Storage Facility Other: __ Disposal facilicy }r8 Landfill Telephone Collector's Name __ £_o_b_b_ 1 o#-y ___ L---'4.._f._.£;.._1 .,._1 _ ___..._ __ _ -signature :,at;.e Sampled ___ e,:...f-___,;f..._(_.:__q ........ / _______ _ Time Samp 1 ed -------:/ .... 0_·_' 'f_o __ -r----- ::p e of Process Gener at i ng Waste _. __ ..:.?;_C_-_6"--_l_a._0....,d;;:.-..:.h..:.•..:.! !'-/ ________________ _ ~ield Information ··::.cld Sampte ~o. ~=i~ of Possession: . . . ?it le signature title inclusive dates signature c i c le inclusive dates title date lnsc=uctions: Complete all applicable information including signatures, and submit ~ich analysis request forms. ... /~;:'srAri~~ t:--1,···1 ·· ,,,~. ~1' ) '·t-'I'. ~ ~~'' ¼:·-~~,t,9 State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary August 29,1991 MEMORANDUM TO: Mr. James Rhodes, Deputy Secretary Department of Administration FROM: Larry Rose, Hydrogeological Technician Solid Waste Section RE: The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the August inspection is enclosed for your review. The inspection for this month found the site in good condition with only minor problems that need attention. The pump could not be started, therefore the leachate collection system was not pumped. In addition, there appears to be a groundhog den located within the fenced perimeter of the landfill. Because burrowing activities could cause both erosion problems and damage to the liner system, efforts should be made to control the establishment of any permanent dens. If you have any questions or comments concerning the PCB landfill, please call this office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Employer • ~co LAfjDf ILL i'iUl·\il !L:t lU:f'O r<.T l . Entrance Road 2. Monitoring Wells Casings, locks · Fences, gates, locks J. Landfill fence, gate, locks i,. Air Vent ~-Landfill Cover 6. 7. Erosion, vegetation Subsidence Leachate Detection System Water in sump Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface lmpoundment Erosion, vegetation 10 . Irrigation Syste~ Influent Piping Pump Sprinkle r Units NO POTENTIAL PROBLEM PROBLEM v .....----- V OBSERVATIONS .: PC.3 LANDFILL MONTHLY REPORT (CONT. uATE ___ %._(/_-_2_9_~_,_1_1 ___________ NAME __ L_n_~-~~7'---ll~,~u~s-~---'---------- : Pumping Data Pumping -Times Pm.,ping Volume------"---------------,-- Irrigati cm Data Irrilia.ting Times Irrigating Volume JAMES G. MARTIN GOVERNOR THOMAS J. HARRELSON SECRETARY STATE OF NORTH CAROLINA DEPARTMENT OF TRANSPORTATION P.O. BOX 25201 RALEIGH 27611-5201 July 26, 1991 MEMORANDUM TO: Mr. W. D. Campbell, P.E. M~Maintenance & Equipment FROM: Cameron W. Lee, Jr., P.E. State Operation Engineer 1UUL 29 1991 DIVISION OF HIGHWAYS WILLIAM G. MARLEY, JR, P.E STATE HIGHWAY ADMINISTRATOR Branch SUBJECT: PCB Land Fill Agreement -Warren County Enclosed is a revised agreement for our Department to perform certain maintenance activities at the PCB Land Fill in Warren County. The maintenance of the mechanical equipment, included in the original agreement, has been deleted from our responsibility. If the revised agreement is satisfactory, please forward to Secretary Harrelson for signature. After which, the agreement should be sent to Mr. Laird Davison in the Department of Environment, Health and Natural Resources. Mr. Davison will have the agreement signed by Secretary Cobey. Division Engineer Earl Stegall estimates the annual cost to maintain the land fill in acc ordance with the agreement to be $10,000. Earl has reques ted funds to cover this work and be allocated to the Warren County Secondary Road Maintenance account. We understand the wo rk is currently being done within their existing budget. Let me know if you have questions. CWLjr:amc Enclosure cc: Mr. Larry Goode, P.E. Mr. Earl Stegall, P.E. Mr. Laird Davison, (EHNR) Mr. Tommy Cline (SPO) An Equal Opportunity/ Affirmative Action Employer ' \ ~:W.rc'.~ J$j',.··1· ., .,,~ ~1 ~tJ~~ MSIIJ} ., ........ ~~,• . '.lit(~-"'"--j ···~~~~ .. JP State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary July 26, 1991 MEMORANDUM TO: Mr. James Rhodes, Deputy Secretary Department of Administration FROM: Larry Rose, Hydrogeological Technician -;/K- Solid Waste Section RE: The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the July inspection is enclosed for your review. The leachate swnp was pwnped and measurements were taken on the pwnping rate and volwne. Overall, the landfill site appears to be in good condition at this time. If you have any questions concerning the PCB Landfill, please call this office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity AlfllTT\c1tlve Action Employer . \. .- PCO LAN.Of I LL i"i\.Jh i'HLl:' Ki.:J?ORT 7_,z (, -C/1 l . Entrance Road 2. Monitoring Wells Casings, locks -Fence s , gates, locks .). Landfill fence, gate, locks !;. Air Vent ). Landfill Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8 . Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface lmpoundment Erosion, vegetation 1 0 . I rrigation Syst~ Influent Piping Pump Sprinkler Units NAME~_t _A_,t:.._,2,,_'f~Q_c_z_c_1-r/ _____ 6'_1,_.;..J..,,.,y_,;_k~r_:;.,e-;-','1'--- NO POTENTIAL PROBLEM PROBLEM ... ✓ ✓ v ✓ ✓ -✓ ✓ ✓ ./ OBSERVATIONS ::_ PCB LANDFILL MONTHLY REPORT (CONT. iJATE . 7--~, -Cf f NAME -------~'----------------'----..;;._ __ ·: Pumping Data Pumping -Times O q:3 I :zt, .,f,',S"t>: /J. {i)/,'jt-f,'57> -l.'Z 0,·t>L l'.3 ·. II~"' -Q._ M1,,, . ~c.. Pm,ping Volumf} /2-S fit1/s., 4,~ ,.L /'klitt} {~o.f _/:,../( f f..roH-1-c ) (j) r:, (;..! v T 'j I.rrigatibn Data Irriga.ting Times 1---~--'!-~~~e -. ( 7, -i.. JJ ~~ J - Irrigating Volume · , _______________ _ / I If 42 J 39 /"L ,, ~-. ~ 31 f v 1 ,,if' ,:2,7:r;.1 I~ ;:J •' I -·· ~ --~ . ~ .' ;,o ·t?, ~~ . / State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary June, 27 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Larry Rose, Hydrogeological Technician Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the June inspection is enclosed for your review. The leachate sump was pumped and measurements were taken on the pumping rate and volume. The grass at the site has recently been mowed. Overall, the landfill site appears to be in good condition at this time. If you have any questions concerning the PCB Landfill, please call this office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Employer .. .. -------------------------~ ---> ..._..,.u.r .U.J.. nvh J.nLl ,~x-U.r..J.· ~ .# 1.1ATJ~ _........;0--.... ;l.__.;7_---::'1./ _________ _ 1. Entrance Road 2. Monitoring Wells Casings, locks · Fences, gates, locks J. Landfill fence, gate, locks L.. Air Vent . 5. Land£ il 1 Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface lmpoundment Erosion, vegetation 10. Irrigation Syst~ Influent Piping Pump Sprinkler Units NAME._~~---+--~~£__._ __ NO POTENTIAL PROBLEM PROBLEM . . ·v ✓ ii ✓ r/ V V: L( OBSERVATIONS ' ; :.·. PC.3 _LANDFILL MONTHLY REPORT (CONT. iJATE · 6 "';i. Z-11 NAME __ L_/i_l'<.._/'<... __ 'f __ ~ __ s_.t_· ____ _ ·: Pumping Data Pumping-Times ' PUL,ping Volume ---=-/"-'/O:a;....,.,3".,,,_.,.?l .... ./""'1 __________ ~_ Irrigaticm Data Irriga·t:ing Times Irrigating Volume ·' ________________ _ ' .•.. . ' N. C. Department of Human Resources Division of Health Services SAMPLE ANALYSES REQUEST State Laboratory of Public Health P. 0. Box 28047 306 N. Wilmington Street Raleigh, 27611 Site Number __ -________________ Field Sample Number ___ 5'_3=-----'i .... "=------------ Name of Site .fe a b½df,'11 SiteLocation 5(< /4;,tJ'f ..... ~,--:<1;·-·;/;~ArTc,;u . µc__ ~ 7-,'-t t ~t i/. 7 Collected By _l_· ,_R_o_~~f ______ ID# -~O_t,_·2.~-Date Collected 5 -3Q -9 i <>-Ti~ I {: t° /;::_, \ Type of Sample: / ---? il 1 JUNl 219Ti Environmental Concentrate Co,ments . / __ Groundwater ( 1) __ Solid ( 5) __ Surface Water (2) __ Liquid (6) __ Soil (3) ~ Other (4) Lt:.,4c.t1,+ -rt. __ Sludge (7) __ Other (8) L tz.Acl-tA 7 E 54-MPJE 8(z<'?M ~UT PtU/ INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride _TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --__ Mercury -- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/ 1 _P&T:GC/MS EDB __ Methoxychlor __ Acid:B/N Ext. ~PCB's <01 """ L __ Toxaphene _TOX __ Petroleum _2,4-D --__ Endrin __ 2,4,5-TP (silvex) --__ Lindane -- MICROBIOLOGY RADIOCHEMISTRY Parameter Parameter Results PCi/ 1 __ (MF) Coliform Colonies/l00mls __ Gross Alpha __ (MPN) Coliform Colonies/lO0mls __ Gross Beta ---- ---- Date Received _!,j,_✓_-_3~·-~0-----~v/__,_/_rJv_k:J_, ____ Date Reported ___ 0=-· -----=-/-=0'-------'9--'-/ _______ _ Date Analyzed ..._t,_--"----_t'/ ...... ·_,_/__.:V.__P._ ________ _ Q'?-1~·.lso Lab Number ...... ,\. J Date Ernactea F ;ge W~ Reported By · /U DHS 3191 (Revise /85) J=F? / / 9 {) c} Solid and Hazardous Waste (Review 7 /87) 0 Purpose: Preparation Enforcement and compliance with the N. C. Solid and Hazardous Waste Management Rules. A sample analyses request form (OHS 3191) must be completed for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one ( 1) container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The collector must then write the site and sample number on the duplicate. Do not submit an analysis request sheet with no parameters indicated. Equivalent measurements: ppm= µg/ml = mg/1 =µgi g= mg/kg ppb = µg/1 = µg/lOOOg = µg/kg DEFINITIONS/INSTRUCTIONS Site Number -A twelve-digit site/location identifier, assigned only by the district field representative. Field Sample Number -A six-digit sample identifier which is pre-printed on the sample label. Name of Site -Name of landfill, facility, etc. Site Location -Address, street number, state road, etc. Collected By -Name and ID of sample collector. Date and Time Collected -Self-explanatory. Environmental -A sample of a naturally occurring substance such as groundwater, surface water or soils which may be contaminated. Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed wastes. Comments -Lists details regarding sample or sample point, including but limited to, phase separation, and/ or od<;>rs. ' Inorpnic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. Extractables are only performed on a solid or semi-solid. For routine landfill samples, check all parameters in the second and third columns. Organic Chemistry -Check ( ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the space provided. Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for either of these. Distribution: 1. Original to State Laboratory of Public Health Environmental Sciences Branch P. 0. Box 2804 7 Raleigh, NC 27611 2. Lab sends copy to Solid and Hazardous Waste Management Branch. 3. Solid and Hazardous Waste Management Branch sends copy to field person. Disposition: This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section of the Records Disposition Schedule as published by the North Carolina Division of Archives and History. Additional forms may be ordered from: Solid and Hazardous Waste Management Branch Division of Health Services P. 0. Box 2091 Raleigh, NC 27602-2091 Hazardous Waste 1-!atcrials ~ !.ocat ion of Sampling: Ccncrator _Scorace Facility Ocher: ~ I N i"'lf:.J1T :":F A 0 j'l.u1,J1j ·7~.117,1.,,,...,, ~ompany • 5 aroe ¢I ,.. !:::'. /T V1r1 f7 \ddrcss @ t-t:16H 4/C ? :olleccor's Name ~ f<.c~ -signature ~Transporter _Disposal Facility Telephone :,ar;e Sampled ____ _-s __ --__ 3._c>_-_';i,.__1 _________ _ Time Trc~tment Facili1 .....-,Landfill ::pc of Process Cenerating Waste · f'cl3 1-i11z44-J)ou..,S Wll"5'TG L /1::..,;bj:: N '------------------'-------=-----------,---------- ·ield Information hJo T / /W,,,i, Q / .:.cld Sample Xo. ~ai~ of Possession: t t le -inclusive daces signature ~~ itl inclusive dates signature title inclusive daces ported /?Md signature date nsc=uccions: Complete all applicabl~ information including signatures, and submit ~ich analysis request forms. State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary May 30, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Larry Rose, Hydrogeological Technician Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the May inspection is enclosed for your review. The leachate sump was pumped and a leachate sample was taken at this time. The maintenance needs mentioned in April's report have been addressed with the repair of the hinge on the outer casing of Well# 1 and the addition of soil cover over burrow holes in the landfill cap. Generally, the landfill site appears to be in good condition at this time. If you have any questions concerning the PCB Landfill, please contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affinnattve Acdon Employer ,,. f 1. Entranc~ Road 2. Monitoring Wells Casings, locks · Fences, gates, locks J. Landfill fence, gate, locks ~-Landfill Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation 10. Irrigation Syst~ Influent Piping Pump Sprinkler Units NAME L~ ~ NO ~TI.AL PROBLE.~ PROBLEM OBSERVATIONS ✓ v' v --- ✓ v I ,/ I . . , : PC2, LANDFILL MONTHLY REPORT (CONT • : Pumping Data Pumping -Times Pm,ping Volume Irrigation Data Irriga.ting Times ..1 rA/1. r ___ .......,.._c:.,_ ____________ _ Irrigating Volume ·' _________________ ...:...__ I ./ L ,A r -e I~ n, ~ ,.,J / H ..:f_ • _ ,,t/";f,~~ 1,uol,,-IO /,;,£d I, ,,,,.,.J l{).t /eY ,~/,),., ov/tv C~?1''":_5 cf tucfl # 3 ,_ t/;1l) tJO/~ ~-~ State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary April 30, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Bobby Lutfy, Hydrogeologist Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the April inspection is enclosed for your review. The ground water monitoring wells and the four stream locations were sampled on April 24th. The leachate sump was pumped and measurements were taken on the pump down rate and recharge rate during pumping. A leachate sample was taken at this time. The maintenance needs mentioned in last month's report have not yet been addressed. (The hinge on the outer casing of Well# 1 is broken and needs to be repaired. The burrow holes in the landfill cap need to be repaired and measures need to be taken to prevent further damag~ by burrowing animals.) The grass at the site has recently been mowed. overall, the landfill site appears to be in generally good condition at this time. If you have any questions concerning the PCB Landfill, you may contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affinnadve Action Employer Pco LANDf ILL i"lUl{fhL:l'. KEPORT l . Entrance Road 2 . Monitoring Wells Casings, locks · Fences, gates, locks J. Landfill fence, gate, locks !.. Air Vent 5 . Landfill Cover 6. Erosion, vegetation Subsidence Leachate Detection System Water in sump 7. Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation 10 . Irrigation Syst~ Influent Piping Pump Sprinkler Units NAME /JolJ B'i l 1-1 TP.i /2,1-~IJ.'/ fZ:os; f:.. I NO POTENTIAL PROBLEM PROBLEM OBSERVATIONS ... fYl <i /.e 1,,(J (.,s.a..,,J l,, .... ...,.Qvls. i,1 /cu,dh't I c .. 1p .: PC13 I-WDFILL MONTHLY REPORT (C01'1T. : Pumping Data Pumping -Times 1; '-I & -10(1 0 IP Irrigatibn Dat.a Irriia.ting Times ,,. Irrigating Volume · , ________________ _ • t . N. C. Ocpanmcnf of Human R.uourcu . 0lvltlon of Huhh Scrvlc« . SAMPLE ANALYSES REQUEST S1111c Labor;,tory of l'ubli( I'. 0 . llu, 306 N. W1lmin1,1u ll..l.:11(h Slee Number ----------,,..--------Field Sample Number __ o_o-.:...~_--=3:;.__;c:;_3_· _____ _ N11me of Site -~P_.;;;c_:,B~~L_C{,~h,.;;.;d_f,~•..,__/ !.________ Sicc LOCllCion __ _,,(;J:___Cl_.;..Y_V-...:e....:.1r1_;___..=.(]:,_..__~....:.V)...L.7l-,C--. -. - Collected Dy _ .. l ~!A~I :...F-1-i ------ID/I _b_S'_q __ Dlltc: Collccccd </-;;l,_.5. -<// Time /(' So Type of Sample: Conuncnt11 Environmenul ___ Groundwater (1) ___ Surface Water (2) __ Soil (3) Concenrr.&h: __ Solid (5) 0 Ltf.bi f I c ff/"\ e .,.f --f:o -~ V Ocher (4) V Liquid (6) ___ Sluditc (7) ___ Ocher (8) INORGANIC CHEMISTRY EJLcnu:ublc• Pillrilmcccr Rc•ulu mii/ l __ Arsenic __ fiarium __ Cadmium _Chromium --U:IIU __ Mer..:ury __ Sdc:nium _Silver ---------- P.lramctcr Rc1ult1 mirl 1 __ P&T:GC/MS --Acid:ll/N Exe. _TOX --- MICROBIOLOGY Par.lmetcr --(MF) Coliform Colonia./ 100mb --(MPN) Coliform Colonic,/ 100mh, Pillrilmctcr R.c11ulc¥ m~/ l __ Arsenic __ Barium __ Ctdmium __ Chloride __ Chromium __ Copper __ fluoride __ Iron __ Lead _·_ Mangan~se __ Mercury __ Nicrace __ Sc:lenium ORGANIC CHEMlSTllY ' Pitrilmch:r _EDU Vi•cu•s __ Pccroleum __ En<lrin __ Lindane - llc1mlt11 m~/ l <~,()()(){_ Par.uncccr __ Gro:.:. Alpha __ Gro:.s lk1a Tot.-1 P;,,.r.-,ncu:r __ Stlv.:r __ Suif11tc:; __ Zinc __ Ph __ C,mduccivicy __ TL)S __ TOC -- -- -- --- ---- Para1n.:1i.:r __ M.:1ho~yddor __ Tux;1pla.:n.: --2,·H) --L,4,'1 -TP (silvn:) -- H.ADlOCH!:MlSTH. Y llc .. ult11 m1 llt:1>ult1> m~ Dace Received L/ -Q, b:: er I '?(/~ Date Rcponc:d _ _._.. C.__-_,,c../_,~""-------'~'--...:...~-------- DiltC Extract~=: ~WGz,, D.cc A,uly,cJ Reported nv t--.,..,5'-"""''-r--.i:;;£__..;~_;;.--=;.....---------Lab Number ---,9...-?l.,,....,.1h4"°''1.~s~---- f)!l'i ]IC)l (llr d7/llS) ~ ... l;I .... ,,,,, .. ,'I., •.• 'llr .. i .. , .. ,11n1 rI ~ //~ 7 ~ s=-1s-fl-VP -· ' Haz~rdous Waste Materials !.ocation of Sarapling: :ompany's Naroe \ddress Generator _Transporter _Scoraee Facility __ Disposal Facility Ocher: Telephone :o 1 lec cor • s Name _ __.&_b=h~'--I __ L:;;..;vi..:.f.:-:..£;~------ -s /gna cure Treatment Facility /Landfill :,at;.e Sampled ___ 4 ___ -_.;?_-'-'S"'_· _-.... CZ...::'/ _______ _ Time S amp 1 ed __,;....;...........:/i~/_~1_.S_o ___ -w-___ _ . ~pe of Process Generating Waste 'ield lnformation :.cld Sample ~o. IJOS3 t/3 ~ai~ of Possession: sifnacure iklus i vc dates 1/JC ~. c77Z signature inclusive dates signature title date nsc:uctions: Complete all applicable information including signatures, and submit ~ich analysis request forms. GRou:;o '.-IAT2:l ~10~; I "I'OlI:~G '.,":'.L.L OOCt..''.·12:'.-iT..\T ION SHC:c:T Dat2: ~-2-tf-'f/ Si ::e Na:::-:: PCB La u/f; _I I Pa:~it f:(2.~15~?--_-_--:=._-:=_ __ C O lj r1 t y : Wa Y-r-e. t'I Site Des::.: -Tc~,·c. {µc..sle v.-~pd.>,A ( Distdct: ( 'nun ic .-ir.du;;. / sa'n i.. -c.2:.:0) ---------Site A.::dr-as s :sg /('pO lf 1 Af/-o,,J Site Contact: _________ _ Abb:e~iations: PVG = Polyvinylchloride; GS= Galvanized S:eel; S = Steal; SS = Stainless Stael Type o t Size of DeiJ':h froM Tnp ot Stick,1? dl C:ising Ca.3ing Outer Casing Fee:: of Height Co;-;-.::ien·':s f Standi:-,g , in~~t' out~r i nr.~ :-oute: to B0ttor!! CO ~.;a~ C 7: Wate: inn~c Ol!ter ,7,1>5 /~l( 1<. en£ r.) D 12. '/ f y--'( /I I I / I ~ J Pvc b 5"/,Y> 'ti I 0 I ro. '6 . .JI a. Iv (7c:J B,,-..,·/rev·S\ ,11..,,i_,,1 _,,,,,_ • .,_.., q,., (J , ; I 110 ~ds. ) , pvc-'f ~ '-/ 1.0 I I '11 -:J l!' ., lz, --A_,,,.., 1-3:J. I 1 ~na. -q y /' ,,~ '4~ I, ; I ,; ,(p 3 eve_ tf r '-/D,tj ;).o,D ~, C'f --1ft:q ,, ' iv JfU1..,,. L 1 ~ /t,, 'f-bo,:/s iJ,S' V V (/ ; I I · 1 5o .£ . .,: Ir '+ PVc.. 5 1/--' 3 'i. 'b /~, I J.(), 1 /{ ~ /4 -~ I ,.-, ,. ,nA~A ~ ,J!, I r r r . gr::, 13.gy LLI. TF v' U-a.rQ.y tco5.c.. • .N. C. ~:partmcnt of Human Rcaourcu . DJ~t.lon of HC1&hh Servlcu SAMPLE ANALYSES REQUEST State Labor.itory of Public He P. 0. Uox lt 306 N. W1lminl(ton S, R,lci1ih, 2 "i Slee Number ________________ Field Sample Number __.5~3...:Y;...· :-I __________ _ Name of Site fc.. e La i1dft ·, I Site Location .... S"'Re..,;:__.wl(p=o_.'f_,_A:<...:+f~·kvi!::...:..L ______ _ Collected Dy _L __ u_t...,f,...--,+--+/_t __ (_<)_-s_~ ___ ID/I OS'( /o 6l. Dllte Collected ....;"-..,..f ..;...-.:;.3-...;i'f:..::'-;;.::Cr;,-r .J,...I ____ _ Type of Sample: Environmental V Groundwater ( 1) __ Surface Water (2) __ Soil (3) __ Other (4) Conccntr.tte __ Solid (5) __ Liquid (6) ___ Sluditc (7) __ Ocher (8) Timi: /2 : 2 0 I -I°fA> lJ Colll.m ¼ INORGANIC CHEMISTRY Eur1u:ublc• Tot.&l P.&rameter Rc•ulu mic/ 1 P.&ramctcr Re111ult111 mg/ 1 P;.,.ramcu:r Rc:liUlllll mi:/ I __ Arsenic __ Arsenic __ Silver __ Barium __ 0arium __ Sulfocc:s __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride: __ Ph __ Leud __ Chromium __ Con<lucciviry __ Mercury __ Copper __ TDS __ $dc:nium __ fluoride _TOC _Silver __ Iron ----__ Lead ----__ Manganese ----__ Mercury ----__ Nicracc. ----__ Selenium -- ORGANIC CHEMlSTllY P.&ramctcr Rc•u!u m"/ 1 --P&T:GC/MS __ Acid:B/N Exe. _TOX ---- MICROBIOLOGY Parameter __ (MF) Coliform Colonia;/ 100mls --(MPN) Coliform Colonie1i/lOOmls Date Reccived 'J.:~ 2,S-q/ IJA f'CEJ?s Date Extracted S-'il-9/-,t'P,wG P.&r.&mctc.:r _EDll _iL PCB's __ Pccroleum __ Enc.Jrin __ Lindane llc11ulc111 m.:/ l <0,0007 Para1nc1cr __ Gross Alpha __ Gross &'.la Para1nctcr H.c1iulc11 mi:/ l __ Mccho(<ychlor __ Tox.iplicnc -2,4-D __ 2,4,.5-TP (silvcx) -- H.ADlOCHEMlSTR Y Dace Reported __ ....;:5"==-----'/:.__::C:>,:;o,_-_..!:,'f--1..f _______ _ Date Analyzcc.l ..:S:-"'---Lt~~~-9..L.L-/YJ-LJ.P _________ _ Lab Number ___ :w:9=1 .... 1....,,.='-'~=4;;,;.;' 4!4----------Reported By ~ :e_ ~ [)!IS JJ()J (llrvi ~ ,-JL.r7, t'/ I'/ •. 1, I .... "I, ... '" .•.•. II,,.; .... , ·111ni fft I I ...,., '-f (f -9 I I $ts-s- · ,N. C. Otp11rrmcnr of Human Ruourcu . D\vlalon of HC11hh Scrvlcca SAMPLE ANALYSES REQUEST S1111c Laboratory of Public Ht P. 0 . Box 28 306 N. W ilminKton S1 R.lc,.ih, 27 Site Number -----------------Field Sample Number ______ 5_3_~_-z... __________ _ Name of Site ec l3 G ,odf,·lf Collected Dy Lu -/ fy / 11. o 5,t_ Type of Sample: Site Location ,512. 16 0 'I , /l{/z,,,., ID/I Q!i"CJ /o~2 011teCollccccd l.f -z..L(-91 Time /.1S-o i Environmental V ___ Groundwater (1) ___ Surface Water (2) __ Soil (3) __ Ocher (4) Concentrtlte __ Solid (5) ___ Liquid (6) ___ SluJitc (7) ___ Ocher (8) w-.2. INORGANIC CHEMISTRY Elltr1u:table11 Parameter Rc11ulu mii/ l __ Arsenic _Barium __ Cadmium __ Chromium __ Lc11d __ Mercury __ Selenium __ Silver ---------- Parameter Rc11ulta mii/ l _P&T:GC/MS __ Acid:B/N Exe. _TOX ---- MICROBIOLOGY Parameter --(MF) Coliform Colonia;/ lOOmls --(MPN) Coliform Colonies/ lOOmls Pllran1eter H.e11ulc11 mic/ 1 __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoride __ Iron _Lc11d __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMlSTllY Parilmcccr _EDB /pews __ Petroleum __ Endrin __ Lindanc Rc11ulc11 mii:/ l <().0 007 Paran\clcr __ Gro:;s Alpha --Gro:.:; Bela Tocal Par;,r.mctcr Rcliulc11 mi,:/ l __ Silver __ Sulfates __ Zinc __ Ph __ Conduccivicy __ TDS __ TOC -- -- -- -- -- -- Paran\clcr llci;ultb mi,:/ l __ Mcchol_(ychlor __ Toxaphcnc --2A-D --2,4,.5-TP (silvex) -- llADIOCHEMlSTR Y llcbulc,; PCi/ 1 Date Received _ ___._lf_,.a::.~ ............ 5"_-_.q_.,J__,_IJ~Au.... _______ _ Date Reported ________________ _ Date Extracted S'-8'-1/ 1//;1/JG Reported By ------------------Lab Number f)ll'i Jl'>I (llrviml 7/R'i) ... l;t '•~-ul,,uPfl .•.. ·nr,,i,-u,?/H?l · ,N. C. Dcparrmcnr of Human RcaourcC6 . Dlvlalon of Huhh Scrvlcca SAMPLE ANALYSES REQUEST S1111c Labor.iwry of Public He P. 0 . Hux 281 306 N. Wilmini,mn Sc ll.ilc11ih, 27 Site Number ----------------Field Sample Number _...;:;5_.,3""--"'Z_,3~---------- Name of Site Pc B l « ttdf I I Collected Dy Lulfy /te_o~c. Sltc Location 5 Fl. i 6 0 Y ID/I Off /ptL Date: Collected '/-2 '-I -q I Type of Sample:: Environmental -✓--Groundwater ( 1) ___ Surface: Water (2) __ Soil (3) __ Other (4) Concentr.&te __ Solid (5) ___ Liquid (6) __ SluJKc (7) __ Other (8) ·-3 INORGANIC CHEMISTRY E:iu:nu:ublc• P.aramctcr Rc1ulu mii/ l Parameter Re11ulcti mg/ l __ Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium __ Chromium __ Chloride: __ Lc11d __ Chromium __ Mercury __ Copper __ Sdenium __ fluoride: _Silver __ Iron --__ Lead --__ Manganese --__ Mercury --__ Nitrate --__ Selenium ORGANIC CHEMISTllY Parameter Rc1ulta mii/ l Paran\cter Raulc11 mJt/ l _P&T:GC/MS EDll __ Acid:B/N Exe. V pcn·s <o.oooL -TOX __ Petroleum --__ Endrin --__ Lindanc: MICROBIOLOGY Con;lmentll Toe.al Parameter __ Silver __ Sulfoces __ Zinc __ Ph __ Conduccivicy __ T DS _TOC ---- -------- Paran\elcr __ Mccho~ychlor __ Toxaphcnc _2,•l-D __ 2,4,5-TP (silv~x) -- llADIOCHEMISTR Y Time J..,' 2-S Reliuhti mi,:/1 Rci;ulu; mi,:/ l Parameter Paran\cccr llcbulci; PCi/ 1 __ ( MF) Coliform Colonia./ lOOmls --( M PN) Coliform Colonic:,/ l OOmls Dace Received __ lf __ . ___ D....,.s....._-..... 9 ..... t-A .... A...._ ________ _ Date: Extracted S--f;-f/:::VetJJG Reported nv n11s Jl<)J (llrviiCll 7/ll~) t'• t;' , •.• ,,. I \II~'"'·••'• •fl,."i,-u, .,,H?l __ Gross Alpha __ Gro:.s Bcca Dace Rc:porccd _________________ _ Date: Analyzed .S-/.S-'1 /1/P 911-14''6 Lab Number · ·· N. C. Dcputmcnt of Human Rcaourca . f?lvlllon of Huhn Scrvlcu SAMPLE ANALYSES REQUEST S11,1c Labor .. cory of Public 1-1< P. 0 .1.ka 2/J 306 N. Wilmin"mn S, ll.1le11th, 21 Site Number ________________ Field Sample Number _~_-3_F_f..,__ _________ _ Name of Site Pc 13 lo. V\.d(i I/ Site Location 5 R I fo tJ 'f ; d,1:/2?1 Collected Dy Lu 1(1.1 I R 0 ~ e ID/I 0 5f !tJ G:;. Date Collected c/--,d_ <J--1 I Time 1/"'__s 0 '? l Type of Sample: Environmental Concentr.&te vi' Groundwater ( 1) Solid (5) W- Surface: Water (2) Liquid (6) Soil (3) Sluditc (7) Other (4) Ochc:r (8) INORGANIC CHEMISTRY Extr1u:ublc• Parameter Rc•ulu mat/ I Parameter Re11ult11 mg/1 __ Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium _Chromium __ Chloride __ Lead __ Chromium __ Mc:n:ury __ Copper __ Sdcnium __ fluoride: _Silver __ Iron -_Lead --__ Manganese --__ Mercury --__ Nicrate. --__ Selenium ORGANIC CHEMISTRY Parameter Re,ulc. mat/ l Parameter Rc,mlt11 mg/ 1 _P&T:GC/MS _EDD __ Acid:B/N Ext. V PCB's <o,OOO/ _TOX __ Pccrolc:um --__ En<lrin --__ Lindanc: MICROBIOLOGY Parameter __ ( MF) Coliform Colonia;/ lOOmls --(MPN) Coliform Colonics/lOOmls Par.uncrcr __ Gro:.s Alpha __ Gro:.s Dcca Total Paranu:u:r Rcliuh11 mi:/ l __ Silver __ Sulfates __ Zinc __ Ph __ Conducciviry __ TOS __ TOC ------ -- -- -- Paran\ctcr U.cc;ulh mi:/ I --Mcrhonchlor __ T o x.iphcnl' -2A-D __ 2,4,.5-TP (silvcx) -- llADIOCHEMISTR Y Date Received __ y_._-...,2..,.S:.__-9...._{_ .. A...,_IJ+---------Dace Reponcd ________________ _ Date Extracted $: ?-1[1'f:Ju.J6 Dace AnalyzcJ S"-/S--1/ j/P Reported By ---------------Lab Number ____ S_l_1_11_1._\_7 _____ _ ()!IS JI C)J (llrviml 7/RS) ,. I; ' , •~. II' I, .... , .. , ...• 'fl t"Vi~u,, IH?l . _N. C. Dcp11rtmcnr of Human Reoourcu . D.lvlalon of HC11lth Servlcu SAMPLE ANALYSES REQUEST Stutc Laboracory of Public He P. 0. Uox 281 306 N. Wilmin~con Sc R.lc111h, 27, Site Number ________________ Field Sample Number ~5..:a3 .... t'"""~------------ Name of Site f.c.e La. ndf:; I I Site Location .5~ I 60 1/ ,4/-/c?'vl Collected Dy ~ Li../ .f1y ( fl~~~ I DI/ o5·c; /4c,, ? Date Collected L/ -~-</ -~1 I Type of Sample: Environmenul ___ Groundwater ( 1) ✓ Surface Water (2) __ Soil (3) __ Other (4) Concentr,ue __ Solid (5) __ Liquid (6) ___ Sluditc (7) __ Ocher (8) Reus INORGANIC CHEMISTllY Extr1u:table1 P.&rameter Rc•ulu mil/ l __ Arsenic __ Barium _Cadmium __ Chromium __ Lc11d __ Mercury __ Sdenium _silver ---------- Parameter Re1ult1 mit/ 1 _P&T:GC/MS __ Acid:8/N Ext. _TOX ---- MICROBIOLOGY Parameter __ (MF) Coliform Colonia./lOOmls -(MPN) Coliform Colonie,/lOOmls P.&rameter Re11ulc111 mK/ l __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoride __ Iron __ Lead __ Manganese __ Mercury __ Nitrate __ Selenium ORGANIC CHEMISTRY P.&r;amch:r _EDD ~PCB's __ Petroleum __ Endrin __ Lindarn: llc111ult11 m~/ l <o ,t,1>ol Paran\ctcr __ Gross Alpha --Gro:.s Bela Total P,ramctcr __ Silver __ Sulfates __ Zinc __ Ph __ Cnnduccivicy __ TDS _TOC -------- ---- Paran\ctcr __ Mccho~ychlor __ Toxaphcnc _2,·~-D --2,4,5-TP (silvcx) -- H.ADIOCHEMISTR Y T. 3 'S-O 1mc ___ _ Rcliult11 mi;/ l Rci;ulci; mi:/ l Date Received __ ff_-.... a:_s ___ , 9~1 __,A .... A....._ ______ _ Date Rcporccd ________________ _ Date Extracted 5 -Y---Cf(:/J?,.WG Reported By ------------------ ()!IS Jl'>I (llrviml 7/fl~) •· I; I 'l~.1, I ,.u 1'f/., •. , 'fl,-vi.-,~ .,IH7) Dace Analyzed S-JS--9/1/P Lab Number ____ 9_. _i_l_._1'.?t:.....t\.::..: 8.::.· _____ _ N. C. Department of Human RcaourCC6 . Dlvlllon of Health Servlcu SAMPLE ANALYSES REQUEST State Laboratory of Public Heald P. 0. Box 2804'i 306 N. WilminKcon Scree Riilci1ih, 27611 Site Number ________________ Field Sample Number ....:=:S-=3;...:...W..;:t-;;._ __________ _ Name of Site ec B La nd(/ II Site LocatiOI' .;12, /lo '( 1 11/:&-n Collected Dy Lu·~/1 /t<o1L ID/I oSifc><>''J-Date Collected <f-.:i._'f -cu Type of Sample: Environmental ___ Groundwater (I) V Surface Water (2) __ Soil (3) __ Other (4) Concentr,te __ Solid (5) __ Liquid (6) __ Sludlle ( 7) __ Other (8) INORGANIC CHEMISTRY Extractable• Parameter Re•ulu m.i/ l P;uameter Re .. ultli mg/ l __ Arsenic __ Arsenic __ Barium __ Barium __ Cadmium __ Cadmium __ Chromium __ Chloride __ Lend __ Chromium __ Mercury __ Copper __ Selenium __ fluoride __ Silver __ Iron --__ Lead --__ Manganese --__ Mercury --__ Nitrate --__ Selenium ORGANIC CHEMISTRY Parameter Reaulta m.i/ 1 Parameter lle11ult11 m.:/ 1 _P&T:GC/MS EDB __ Acid:B/N Ext. L/pcn·s <O,Q(l_O l _TOX --Petroleum --__ Endrin --__ Lindane MICROBIOLOGY Commcnt11 Total Parameter __ Silver __ Sulfates __ Zinc __ Ph __ Conductivity __ TDS _TOC ------ -- -- -- Parameter --Mdhonchlor __ T oxaphenc -2,4,D --2,4,5,TP (silvex) -- RADIOCHEMISTRY Time .... x2 .... 1<_,'_S_o __ Reliulc" mg/ 1 Rci;ulb mi:/ I Parameter Paran\ctcr llci;uhi; PCi/ 1 __ (MF) Coliform Colonies/ lOOmls __ (MPN) Coliform Colonies/lOOmls __ Gross Alpha __ Gross Ikea Date Received __ 'f...._, .... J:-S:._,q..,_,.l.___&..,4...,(d_,__ _______ Date Reported ______________ _ Date Extracted S:Y-f/11P,;rt,I6 _________ Dace Analyzed ..;::S-:.--,_/.S:--'---..te.9...:../~~~7'~--------- Reporred Dy ----------------Lab Number _____ 9_1_1_11_· i_¼_9 ______ _ £)HS 3191 (Rrvi,cd 7/flS) (' l;I ''-··'''"'"""-;-•• ·n,..vi~w ?/H?) N. C, Ocp1mmcnr of Human Rcaourcu . Dlvlalon of Huhh Scrvlcca SAMPLE ANALYSES REQUEST S11,1c Labora1ury u( l'ublu: I'. 0 . LI..,• 306 N. Wilrninl(IUI ll..lcil(h, Site Number ________________ Fidd Sample Number __,.S"""'3~g_7..._ ________ _ N1&mc of She PC t3 L a.,.cf A I I Slee Loc1&cion .5 Ii:. 1 G O if . /1,£/c,,, L _Jr / n ,. ,..r~ 1 ,, ? , I_;).., I-~/> 7 /c-Collcctcd Dy -,c:,o.11Y:i.....L'-c"'y ... · ____ ,<-_c_,;_,,..____ ID/I !-CL:t /Qb L D1&te Collected __ -,-___ -, _ ___..1 .... _____ Ti me'-' • ~ Type of Sample: Environmcnul __ Groundwater (1) ✓ Surface Water (2) __ Soil (3) __ Other (4) Conccntr.ate __ Solid (5) __ Liquid (6) ___ Sludllc (7) __ Ocher (8) U T Uj' INORGANIC CHEMISTRY E.uriu:c.blc• P.&ramctcr Rc•ulu mit/ l __ Ar:.enic __ llarium __ Cadmium __ Chromium --Lc11J __ Mcn:ury _._Sdenium _Silver ---------- P.&rametcr Rc,ulu mii/ l _J>&T:GC/MS __ Acid:ll/N Exe. _TOX ---- MICROBIOLOCY Pilramctcr -( MF) Coliform Colonia./ lOOml:; -(MPN) Coliform Colonic,/IOOmls Parameter Rc11ulc11 mK/ l __ Arsenic __ 0arium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoriJe __ Iron _Lead _·_ Mangan~sc __ Mercury __ Nicracc . ___ Selenium ORGANIC CHEMlSTllY - Parameter EDU l71'CU's --Pccroleum --En<lrin --Lindane llc11ult11 m~/ l <o.ooo/ Paran\clcr __ Gro:.s Alpha __ Gro:.:. lk1a Con_uncnt11 Total P;.ra1nctcr llcaull11 mt __ Silver __ Sul(ucc:; __ Zinc __ Ph __ C<inducciviry __ TUS __ -roe -- ---- -- -- -- Par.unctcr llcbUltb m~ __ Mccho:<yddor __ Tox;1pl1.:n.: --2,•f-D --2,'l,S-TI' (silvcx) -- llADlOCHEMISTll Y llcbulra PCi/ l D,uc Received ff -().S>9 J AA Dace Rcpurtl·d ________________ _ Date Excracccd S -Y....9/J/73 y/6 Rcporrcd Oy Lab Number l"\I IS l 11) I (llrvi~cil 7/11~) ,. I; l S1111c L1boraiory o( l'ubli,: N. C. Ocparrmcnr of Human Ruourcu . . Dlv!.lon of Huhh Scrvlcu SAMPLE ANALYSES REQUEST I'. 0. Liu• 306 N. Wdmini,;101 H..lc11(h, Site Number Fidd Sllmplc Number 5"3 <g<l N1Lmc of Slee fC ,:3 t. ct ~,I l,_ I(__ Slee Location ,f 12 /f:,{.)L/ Al~ ' > , Collccccd Dy l.11 lf7 I tfc~JL 7 ID/I <>~<j /vG 1. Type of Sample: Environmcnul ___ Groundwater (1) ✓ Surface Water (2) __ Soil (3) __ Ocher (4) Conccncr.ace __ Solid (5) Liquid (6) ---Sluditc (7) ___ Other (8) D11cc: Collected ll T £) S INORGANIC CHEMISTRY Eunu:tablc• P.&rilmc:u~r U.caulu mic/ l __ Aocnic __ fiarium __ Cadmium _Chromium --Lc:11J __ Mcr..:ury _·_sdc:nium _Silver --------- Piirilmctcr Rc,ulta miil 1 _P&T:GC/MS __ Acid:8/N Exe. _TOX ---- MICROBIOLOGY Par.amc:tc:r --( MF) Coliform Colonia./ lOOmls -(MPN) Coliform Colonic,/lOOmls Pi&ramctc:r U.c11ulc11 mK/ l __ Ar:;cnic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoride: __ Iron _Lead _·_ Manganese __ Mercury __ Nicracc . ___ Selenium ORGANIC CHEMISTllY - Pilri&O\Ctcr _EDll ...J.L PCB's __ Pccroleum __ Enurin __ Lindanc: llc11ult111 m~/ l <o. ot:>Ol Para1nc1cr __ Gro:.s Alpha --Cro:.:; Bela lf-~Lf-q I Timc .:,:,S- ConuncnCti Total Para1ncu:r llc•ult,. m~ __ Silva __ Sulfoccs __ Zinc __ Ph __ C,mduccivicy __ TDS __ -roe ---- -- -- -- -- Par.unct.cr llc1>ulc1> m~ __ Mccho~ycldor __ Tox.iphcnc __ l,•f-D --L,'1,5-TP (silvcx) -- llADlOCt-11:MlSTll Y llc1,ulc. PCi/ l Dace Received _.._I./...,-).......,S.._-..... q1..1l..._-i.,..Au.A..L..-_______ _ Dace: Rcporccd _______________ _ Date Extr1tccc:d ... S-~-/i .... 'O_J/. ___ '/_--vP""-'-· __________ _ Reported Oy ----------------- ri11s ll'>I (llrvi~,17/1!~) •· Ii• ,1 ... ,,1,,u•'U, .. •• 'fl,-,,i_.u,-,/1-C{\ Do&cc AnalyzcJ .... 5:--LL.=S'-:....-_, ..L-t~r-::lt?>½---..,.------- 9111:\ 5 1 Lab Number N. G, Ocparrmcnr of Human Ruourcu . Dlvt.lon of Hcahh Scrvlcu SAMPLE ANALYSES REQUEST S11,1c Laboracory of Public I'. 0. Liu• 306 N. Wilrninl(10, H.,dc11Lh Site Number ----------------Field Sample Number __ S...;;.3_$5_:.Cj ________ _ Site Location .51'< /f:, 0 'I ; /-1{~ N1&mcofS1tc ec. <3 L4nlf1 If Collected Dy Lul/1 / Kos.-:. Type of Sample:: ID/I OS 'I /£>{, 2 01&tc: Collected Y -,.)__ \ f -")/ Tim~'.' .S,J ' Con:uncnu Environmenul ___ Groundwater ( 1) ___ Surface: W1&tcr (2) Solid (5) ___ Liquid (6) ___ Sludllc (7) ___ Ocher (8) RC. ll s· -i edr :n €AA f ✓ Soil (3) __ Ocher (4) Eunu:ublc• Pilrilmc,cr ltc,ulu mli[/l __ Arsenic _l}uium __ Cadmium __ Chromium __ Lc:11d __ Mercury __ $dcnium _Silver --------- Parameter Rc,uli. mli[/ l --P& T:GC/MS __ Acid:8/N Exe. _TQX ---- MlCRO8lOLOGY INORGANIC CHEMISTRY Total Pilranu!lcr llc11ulh mK/ 1 Para,ncu:r __ Arsenic __ Silver __ Barium __ Sulfuccs __ Cadmium __ Zinc __ Chloride __ Ph __ Chromium __ Cllnducc1viry __ Copper __ TUS __ fluoride _TOC __ Iron -- __ Lend -- _·_ Mangan~sc -- __ Mercury -- __ Nicracc . -- __ Selenium -- ORGANIC CHEMlSTllY - Parilmch:r llc11ulc11 m~/ l Pari\nu:ll:r _EDD __ Mcdlll~yddor _iL..pcu·s <o,Ln __ 'fc,x;1pl1cnc __ Petroleum _2.-f-D __ EnJrin --2,4,S-TP (silvcx) __ Lindanc -- llADlOCHEMISTH. Y lle11ult11 m1 llt:bUlcb IHI Parilmcrcr Paran\clcr llc,.ulci; PCa/ l --( MF) Coliform Colonia./ lOOmls --(MPN) Coliform Colonici/ lOOmls D,ue Received lf -J... S -CJ/ II.fl Dace Extracccd S'-/3-9/1/P Reported Oy ------------------ n11s ll'>l (ltrvi~cil 7/RS) •·• &; I 'I.,,, I,,,. ,,1., .. , •f1~.,j,.,.,,//l7\ __ Gro:.s Alpha --Gro:.s lkla Dace Rcponcd _______________ _ D.&cc: AnalyicJ S -/S -9/1(p Lab Number 911-4 52 S1111c Labor .. tory o( Public.: N. C. Ocpurmcnr of Human Rcaourcei . Dlvlaluo of Hulth Scrvlcu SAMPLE ANALYSES REQUEST I'. 0 . Liu" 306 N. Wilmini.1..:rn H.,lc11ih, Sltc Number ----------------Field Sllmple Number ....,5,:;;..w3'--+-yo=----------- Name o( Slte Pc t3 l,l.,,d'(/I SitcLocu.tion 5,z /too '{ J ~[/41,,, Collected Dy f_1,,1 ~f"f / ~ .. ; e. ID/I. o[9 /0 ' l Du.te Collected 3/:--::>.. '-f -11 Type of Sample: Environmental ___ Groundwater (1) ___ Surface Water (2) 1/ Soil (3) __ Ocher (4) Conccntr.&tc __ Solid (5) Liquid (6) ___ SluJjlc (7) ___ Ocher (8) Conuncnu s ~~cvt,f INORGANIC CHEMISTRY Euriu:ublc• Tot.-1 P.arilmcu:r ltc.ulu mitl l P;aran,etcr Rc.-ulh mi,:/1 P.-r.-1ncu:r llcault11 mi; __ Arsenic __ Arsenic __ Silva __ Jluium __ Llarium __ Sulfuci::; __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride __ Ph __ Lc11d __ Chromium __ C,inc.luccivicy __ Men:ury __ Copper __ TDS _._Sdenium __ fluoride __ TOC _Silver __ lron ---__ Lead -- --__ Manganese ----__ Mercury ----__ Nitrate . ----__ Selenium -- ORGANIC CHEMlSTllY P.aramcccr Rc•ulu mi[/ l Pilr.amctcr _ P&. T:GC/MS EDll --Acid:8/N Exe. /l'CB's _TQX __ Pccrolc.-um --__ EnJrin --__ Lindanc MICRODlOLOGY Parilmctcr --( MF) Coliform Colonia./ lOOmls --(MPN) Coliform Colonic,/lOOmls O;ue Received ___ f/ .... --l'.i:--J'::;.._' .:..q /'--... f!~ft:..__ ______ _ Diltc ExcraCled ..;;!(-~-.:.:/3~-..;.1.'-1/_.1/p~----------- Rcporccd lly Oll'i ) t l)J {lltvi~nl 1/ll~) ..... ' llc.-ullti m.:/ l <OtlO Par.-1nc1cr __ Gro:.!i Alpl1a -. _ Gro:.!i l.kLa Par.tn\clcr llcbuhb m~ __ Mccho!'ycltlor __ Tox;1plH:n.: _l,·~-D __ l!•.S-TP (sil11cx) -- H.ADIOCl·lEMISTll Y llcoulh PCi/ 1 Dace RcporccJ ________________ _ Dace AnalyzcJ ...,$-_-.._/-=S-:-=---:.!-9~/.·-:!:Jl;._.Pi.... _______ _ Lab Number ___ 9_l _l_. 1_:l_S_, 3 ______ _ N. C. Dcp11rrmcnr of Human Ruourcu Dlvltlon of Huhh Scrvlcu SAMPLE ANALYSES REQUEST S1111c Labor .. tory of l'ublic I'. 0. Uux 306 N. Wil111inb1u1 l\.,lc11th, Site Number ________________ Fidd Sample Number _:,_·-__ 3 .... 9 .... I ___________ _ Name of Site ..:.fi .... c:::: ___ B __ Lg......,.__vi_d-,_'.(,.__._1_.I(..__ ________ Slee Loc11tion .51< /t,o Y J llftuY> Collected Dy LIA .f f'y / f?.os-c. ID/I o .;-q /v(:l Date Collccccd if-~ Y -JI Type of Sample: Environmental Con:uncnt11 ___ Groundwntcr ( 1) ___ Surface Water (2) c../ Soil (3) __ Solid (5) __ Liquid (6) ___ Slud1£c ( 7) ___ Ocher (8) UTU 5 -5Aft-~01.f __ Ocher (4) E:r.cnu:ublc11 Piir.uncccr Rc11ulu mic/ l --Arsenic _0arium _Cadmium __ Chromium --Lc11d __ Mcn:ury __ Sdcnium _Silver --------- Pi&ramcter Rc11ulu m1t/ l --P& T:GC/MS __ Acid:8/N Exe. -TOX ---- MICROBIOLOGY Pariimcter --( MF) Coliform Colonia;/ lOOmls -( M PN) Coliform Colonie,/ l OOmls INORGANIC CHEMISTRY P .. ranu:tcr U.clluh,; mi,:/ l __ Arsenic __ Barium __ Cadmium __ Chloride __ Chromium __ Copper __ fluoride __ Iron __ Lead ._._Manganese __ Mercury __ Nicrace. __ Selenium ORGANIC CHEMISTllY - Pi&ri&mcccr _EDU ✓ l'CB's --Pccroicum __ EnJrin --Lindanc - H.c11ult11 mii;/ l <O,LO Para1nc1cr __ Gro:.s Alpha __ Gro:.s Ikea Total Para,ncu:r __ Silva __ Sulfuccs __ Zinc __ Ph __ Cnnducciviry __ TDS _TOC -- -- -- -- -- -- Par.unch::r __ Mc1ho~yddor __ 'fox;1phcnL· _2,•~-D --2."•.'.i-TP (silvcx) -- llADlOCHt::MISTll Y llcaul111 m~ llcr,ultr, mi: OiUC Received 1/ ~ J.S -C/ I 111/ Date: Rcportnl ________________ _ Dace Extracted S;-13---9/jp Reported fly nll'i Jl'>I (llrvi1,nl 7/flS) ... Ii ' f .... ,, I '"" ,,., .•.•. n ,.,,i,.w, IH?l Dace AnalyzcJ S -/S'-9/1/P Lab Number 9111lS4 N, C. Dcpurmcnr of Human Ruourcu Dlvi.lon of Hcahh Scrvlcu SAMPLE ANALYSES REQUEST S1111c Lo1boro1tory of Public I'. 0. Liu~ )06 N. W1lmin,;1u1 H.,ilc11ih, Site Number ________________ Field Sample Number --=5~3:c..'t.L.;;:.Z _________ _ Name of Slee ..;P.,...:C:;...:,D..__...;.L._.a,,_~.-::;;+P~l_f ________ Slee Locacion SfZ /tt, O L/ . A{&;-,,,, Collected Dy Lu ./ I y /a l>L, e ID/I C">;i'j / c,(, l Dace Collected c-f -.:2 'f -q I Type of Sample: Environmenul ___ Groundwater (1) ___ Surface W11cer (2) v Soil (J) __ Other (4) Conccntr.&tc: __ Solid (5) ___ Liquid (6) ___ Sludilc (7) __ Ocher (8) Comment• U ID 5-~Ju~ <l-"1--f INORGANIC CHEMISTRY Euriu:'--'blc• Toc .. l P.&ramctcr Rc•ulu mii/ l P.&ramctcr Hc11uh11 mi,:/ 1 P .. r .. ,nclcr __ Ar:.c:nic __ Ar:.cnic __ Silver _lluium __ 13arium __ Sulfocc:; __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride __ Ph __ Lc11J __ Chromium __ CllnJuccivicy __ Mcr.:ury __ Copper __ TUS __ Sdcnium __ fluoride: __ ·roe _Silver __ Iron ----__ Lead ----__ Manganese ----__ Mercury ----__ Nicracc . ----__ Selenium -- ORGANIC CHEMISTllY -- P.&ramctcr Rc•uh.t1 mr.c/1 P;ar,&n\cccr llt:11ulc11 m.:/ 1 Par.unctcr __ P& T:GC/MS _EDD __ Mc1ho~yclilor --Acid:8/N Exe. ~PCB's <0,/0 __ 'fux.ipl11:nc _TOX __ Pccrolc:um __ 2,•H ) --__ En<lrin --2.'L.'.i-TP (silvcx) ---__ Lindanc -- MICRODlOLOGY H.ADlOCHEMISTll Y Rc.ul111 m~ llc1>ullb m~ Par;amcrcr P.ar .. n\clcr llcbu(c., PCi/ l --( MF) Coliform Colonic,;/ lOOml:. -(MPN) Coliform Colonic,/lOOml:. O;uc R.ecc:ivc:d __ 1/ ..... -__ ~.......,,.>r'--, fi....:.l_~lf....;.A_;__ ______ _ Dace Exrraccc:d ... 5;._-.,_./3-.-.7..i.(_16.&...\.P __________ _ Rcporred Oy ()l('i Jll)J (llr~i~,I 7/A~) •· I: t '1 .. • ,, I,,,. ,._, ...• · fl r,•i""'" '? IH?l __ Gro:.s Alpha --Gro:.s lk1a Dace: Rcpom.·d _______________ _ Dace Analyzed _.,;)""'c--'-_.1../._.S:~---LZJ./_~~'P=---------- Lab Number 91111 S S Hazardous Waste ~acerials !.ocacion of Sampling: Generator _Scoracc Facility Ocher: _Transporter _Disposal facility :ompany's Name /!?8 L.F,~/i)e,a f 0 1 /'. /ldm/1'1 ,· Telephone \ddress 5R.. i4'Q4 . j}I/m, 7 'i- : o l lec tor's Name _L_u..,f ... ~ ... Y.__ ... J__.& ... -< .... i;_' >£ ____ _... ___ _ -signature _Treatment .Facility ~Landfill(jc-.B :,at;e Sampled (f: J.Lf~1 j Time Sampled_..;_, _______ _,, ___ _ LF ::pe of Process Genera ting Was ce · Pc 13 ---------------------,---------- 'ield Information 53 'l 2. 5 .3 '6 '{ 53 ~S 53g17 ~ai~ of Possession: ive dates · t.itle inclusive daces signature title inclusive dates cSU!CS ren t.LA -~·~·(}f{V title date · nsc:uctions: Complete all applicable information including signatures, and submit ~ith analysis request. forms. DEPARTMENT OF ADMINISTRATION PC 6Q . ' STATE PROPERTY OFFICE w, '!!!~ Id DATE, 7-11-cv FRrM:];i/2~~ ( l NOTE AND FILE t l PER OUR CONVERSATION t NOTE AND RETURN TO ME -( I PER YOUR REQUEST _ RETURN lllnt ll>RE DETAILS _ FOR YOUR APPROVAL SEE NE ABOUT THIS FOR YOUR INFORMATION PLEASE ANSWER -FOR YOUR CCMMENTS t t PREPARE REPLY fOR MY SIGNAlllRE l SIGNAlllRE () TAKE APPROPRIATE ACTION () INVESTIGATE I RETURN ( ) RUSH -IIIE>IATE ACTION ( ) SET UP FILE CtJA 3-I£~ q I -/4, -;;;,~ ~ 1 C(,Y\L p::, c lct v·. ·-fy, ... James G. Martin, Governor William W. Cobey, Jr., Secretary February 28, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Bobby Lutfy, Hydrogeologist B~ Solid Waste Section The PCB Landfill Monthly Inspection The PCB Landfill Monthly Report for the February inspection is enclosed for your review. The landfill appears to be in generally good condition. The sprinkler system was repaired on February 13th. D.O.T. has also restricted the access to the left of the main gate. The leachate pump will be put in operating order prior to next month's landfill inspection. I met with Mr. Glenwood Rose and Mr. Clarence Thompson of the Warren County Department of Transportation maintenance department at the PCB Landfill site to show them the new sprinkler system. We discussed the need to flag the sprinkler system in such a way as to avoid damage to the system by mowing equipment. Other maintenance issues at the PCB Landfill site were also discussed. The D.O.T. has been very responsive to maintenance needs at the site. They have continued to do a good job of keeping up the site and performing maintenance tasks as required at the PCB Landfill. If you have any questions concerning the PCB landfi~_r1.fs~,ftJ contact our office at (919) 733-0692. .<\I.I~!~ I \ \ cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Emr!~r James G. Martin, Governor William W. Cobey, Jr., Secretary March 21, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Bobby Lutfy, Hydrogeologist !3L Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the March inspection is enclosed for your review. A leachate level measurement system was installed in order to determine if the pump is pumping all the leachate out of the leachate collection system and to determine the recharge rate of leachate into the collection system. The leachate pump was repaired by D.O.T., and the leachate collection system was pt:_-r:ped-~-·~>:1, ':-.i,..J~'..C<e " A couple of maintenance needs were observed during this month 's inspection. The hinge on the outer casing of Well# 1 is broken and needs to be repaired. Moles, or some other small animals, have been burrowing in the landfill cap. Some effort needs to be made to eradicate these animals and repair the burrow holes. The Solid Waste Section is glad to see that the Department of Administration, as the (new) Permit Holder for the PCB Landfill, has taken steps to establish a maintenance and operations fund for the facility. Needed repairs to the sprinkler system were made this past month. We hope additional funds will be made available to fence in the leachate holding pond and to purchase a leachate storage tank this coming fiscal year. If there is any way our Section can provide more effective service to the Department of Administration in the inspection and monitoring of the PCB Landfill, please let us know. If you have any questions concerning the PCB Landfill, you may contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmadve Action Employer .... .. . .. Pea LAN.Of ILL i-11.Jhi'HLr H..E.PO?-.T -...· j,ATJ~ ~rn.._..!.J_ti..:..:R..;....c ___ H.,____o<_o_,.J--, _t_CJ_Cf_l -- l . Entrance Road 2. Monitoring Wells Casings, locks .) . 5 . 6. 7. 8. 10. · Fences, gates, locks Landfill fence, gate, locks Air Vent Landfill Cover Erosion, vegetation Subsidence Leachate Detection System Water in sump Leachate Collection System Access Pipe Pump Piping Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation Irrigation Syst~ Influent Piping Pump Sprinkler Units NO PROBLEM v ~ v ... ~ POTENTIAL PROBLEM v OBSERVATIONS f/l"''j~ ol t,,,../.e.r c~.s,·..,_J t.or w~ II#/ ,:S b,..fei,,, l'lf ol<, /,..ol~s; <t...,,J h"'r.-ow.r ,.,,, /11.r.J C:11 c"'e : Pumping Data Pumping-Times Irrigatibn Data Irriia.ting Times Irrigating Volume .: PC:3 LANDFILL MONTHLY REPORT (CONT. Sc..'"'r'1'.s ~ ~-"' ~-G ,.\.o .Q\k..-srs~~. t. 1 State of North Carolina . Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary February 28, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of Administration Bobby Lutfy, Hydrogeologist Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the February inspection is enclosed for your review. The landfill appears to be in generally good condition. The sprinkler system was repaired on February 13th. D.O.T. has also restricted the access to the left of the main gate. The leachate pwnp will be put in operating order prior to next month's landfill inspection. I met with Mr. Glenwood Rose and Mr. Clarence Thompson of the Warren County Department of Transportation maintenance department at the PCB Landfill site to show them the new sprinkler system. We discussed the need to flag the sprinkler system in such a way as to avoid damage to the system by mowing equipment. Other maintenance issues at the PCB Landfill site were also discussed. The D.O.T. has been very responsive to maintenance needs at the site. They have continued to do a good job of keeping up the site and performing maintenance tasks as required at the PCB Landfill. If you have any questions concerning the PCB landfill please contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Ea Oooo nltv Affirmative Action EmolOVPr PCO WDf ILL i'iUl\l'liLY KEPORT 1 . Entrance Road 2. Monitoring Wells Casings, locks _). · Fences, gates, locks Landfill fence, gate, locks Air Vent . ). Landfill Cover 6. 7. Erosion, vegetation Subsidence Leachate Detection System Water in sump Leachate Collection System Access Pipe Pump Piping 8. Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation 10 . Irrigation Syst~ Influent Piping Pump Sprinkler Units NAME 2o&g y Ll1TPf _/4A-~12y 7 POTENTIAL Ro..se NO PROBLEM PROBLEM v V . . OBSERVATIONS /9<.c.ess 7b /f!.p,j. o/' /"lq ,·., [Jtf k .,..e.s+.-,·c,../ec/ Sr<• "'~lr..-$,,S~ ....... "'--.~ ' ~e."' -'~F '~"d :.-PCB LANDFILL MONTHLY REPORT (CONT. i.JATE ~ g I l'f 9/ NAME __ L_i._-17--+---./'----'Rc-'----o...;...se. __ ..;a._ __ : Pumping Data Pumping -Times PUL,ping Volume -----.----'-------------,-- Irrigatibn Data Irriia"t:ing Times Irrigating Volume .- .. .• #~ (% t State of North Carolina Department of Environment, Health, and Natural Resources Division of Solid Waste Management P.O. Box 27687 · Raleigh, North Carolina 27611-7687 James G. Martin, Governor William W. Cobey, Jr., Secretary January 24, 1991 MEMORANDUM TO: FROM: RE: Mr. James Rhodes, Deputy Secretary Department of A<1ninistration Bobby Lutfy, Hydrogeologist BL Solid Waste Section The PCB Landfill Monthly Inspection William L. Meyer Director The PCB Landfill Monthly Report for the January inspection is enclosed for your review. The landfill appears to be in generally good condition. Once again, the leachate collection pump could not be started, so no leachate was pumped. The concrete pads for the new sprinkler system were at the site, but the system has not yet been repaired. It is my understanding that these repairs are scheduled to be made as soon as the weather permits. Since the logging was done at the front of the site this past year, several points of possible access to the site have been opened up. Over recent -months it appears that hunters have been entering the site just to the left of the cable across the entrance road. Some effort needs to be made to further restrict access to the site. If you have any questions concerning the PCB landfill please contact our office at (919) 733-0692. cc: Jim Coffey Attachment An Equal Opportunity Affirmative Action Employer l . Entrance Road 2 . Monitoring Wells Casings, locks · Fences, gates, locks .). Landfill fence, gate, locks L.. Air Vent . S . Land£ il 1 Cover Erosion, vegetation Subsidence 6. Leachate Detection System Water in sump 7. Leachate Collection System Ac cess Pipe Pump Piping 8 . Treatment Works Influent Piping Sand Filter Carbon Filter Effluent Piping Surface Impoundment Erosion, vegetation 10 . I rrigation Syst~ Influent Piping Pump Sprinkler Units NO POTENTIAL PROBLEM PROBLEM v I, ✓ .. · PCI3 Lm DFILL MONTHLY REPORT (cmrr. : Pumping Data Pumping -Times Pur.,ping Volume Irrigatibn Data Irriia"t:ing Times Irrigating Volume ---------'----------------:- ___, -