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NCD980602163_19900515_Warren County PCB Landfill_SERB C_Re Trip Summary and Lab Data for 18 Apr 1990 Sampling-OCR
15 May 1990 MEMORANDUM: To: From: Re: File Charlotte Jesneck, Hydrogeologist Superfund Section PCB Landfill, Warren County Trip Summary and Laboratory Data For 18 April 1990 Sampling On 18 April 1990, Bruce Nicholson and I traveled to the PCB landfill in Warren County to conduct sampling of grass and soil on the landfill cap. The purpose of the sampling was to assist the Solid Waste Section in obtaining background information on the landfill cap before leachate extraction, treatment, and spray irrigation recommences. The landfill was staked at 50 feet intervals as depicted in the attached sketch. The landfill was then divided into four quadrants. Samples of grass and surface soil were collected near each staked point and composited within quadrants. This approach yielded four grass composite samples and four soil composite samples. In addition to these samples, samples were collected from the leachate collection pond sediment and the charcoal filter. The leachate collection pond did not have enough liquid to take a water sample. The soil samples form the landfill cap were collected using stainless steel scoops and composited in a precleaned stainless steel bucket. The bucket was decontaminated between composites by washing with alconox and deionized water, rinsing with deionized water, rinsing with isopropyl alcohol, and again rinsing with deionized water. The scoops were discarded between quadrants. The grass samples were composited in a bucket lined with aluminum foil. The foil was discarded between composites. Polyvinyl chloride gloves were worn while collecting samples. The gloves were discarded between quadrants and the other samples collected. All samples we placed in glass jars precleaned for organic samples. The samples were stored on ice until delivered to the laboratory the next morning. All of the samples were analyzed for PCBs and Base/Neutral and Acid Extractables. The table below identifies the field sample numbers, the Superfund Section identification numbers, the laboratory identification numbers, and the time of collection for each sample location: Field# Superfund # Lab# Location Time Collected A-G-1 12064 905009 Quadrant A 11 :50 -12: 10 Composite, Grass A-S-1_ 12065 905010 Quadrant A 11:50 -12:10 Composite, Soil B-G-1 12066 905011 Quadrant B 11:15 -11:30 Composite, Grass B-S-1 12067 905012 Quadrant B 11:15 -11:30 Composite, Soil C-G-1 12068 905013 Quadrant C 15:00 -15:15 Composite, Grass C-S-1 12069 905014 Quadrant C 15:00 -15:15 Composite, Soil D-G-1 12070 905015 Quadrant D 14:40 -14 :55 Composite, I Grass D-S-1 12071 905016 Quadrant D 14:40 -14 :55 Composite, Soil 2 12072 905017 Leachate Pond 15:30 Sediment 3 12073 905018 Charcoal Filter 15:30 The analytical data sheets are attached. Sample 2, the sediment from the leachate pond, was the only sample with a detectable concentration of PCBs. PCBs (#1260 PCB) · were detected at a level of 0.27 ppm in this sample. attachments cc: Lee Crosby Bobby Lufty cv /jo /Memos.cv x.. + >< I l/\ 11 0 ~ "' ( 3 -;J ---:, " p -f ~ (" ., 0 0 0 ;:s :::, i--+-n t,, ~ ' - V\ <> .,,. I.A u R> 0 ( :f ,s;:;-, $' ~ ~ ( "' >' C' ~ ' :;; ,:-~ -L \' ~ -f I T(-1i r i ) ("' (' + ;<. y + .L ,<. ..._ __.:.., ..,.. X ..... _l... ·~z + ..... J.... l -'-.J-...... -)<-x-x-x-:-x -)< I -x-:X-1 I .L + .J_ ;,(.. ,<._ ..!,.-..I-J.... -6 ....... +-+ X I i I I >< + + L J;) ( 0 .L .... .... +- 0 C ::, -+- ..:.-- 6 -+- .L :.- -\-' __,._ -I- _J ~ ""b ., 0 X. t---~ $:! 0 -::;-~ _,_ r> --0 0 ~ v Q r-- ~ ,"- ----- ".:" -; :; (" :> c<: ........., ,,_,___ --."\ ; --::, C :::. I'-\ _,_ ~ ---~ < ~ ~ =-(__;' ' . : 5'::i p>:' 5 V fl-P (' {'v ,1 J N. C. D~partment of Human Resources Division cf Health Services SAMPLE ANALYSES REQUEST Collected By l{-,, C /:) ..5 ~ /-, , , f\ Type of Sample: Environmental __ Groundwater (1) __ Surface Water (2) __ Soil (3)- --Other (4) ID# Concentrate S <; ✓ c 1 0 ~ ~'--S6Iid (5) __ Liquid (6) __ Sludge (7) __ Other (8) Comments PI e o s Q JJ o IC l\ o )', o /1 s / , I £ ; c <: + , 1 (-f h e --r P ;" -" 0 n vi St1 m ;}e_ ) Q ? + , o r, a 1 <1 -z.._.,e fo r -)-/2 e.. o ! ), e rs ' · I I ~-n cd ,· c r,{ ) P J, INORGANIC CHEMISTRY Extractables Parameter Results mg/ I __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury __ Selenium __ Silver -- -- ' --- -- -- Parameter Results mg/I ~T:GC/MS 1d:B/N Ext. LTOX . J ( J,._ / n r o h a---z..c-, c_ u c ,· Lr /\lorob:nZou/l~r1V1 1L nc,'c A ,/ 'iv« .... ,, '71, I C,1\u o ).e1--c01Y1/)()u"1I < wh1c h."":19h T < /-.r ,,,/ rJ O I h k :.,),I\/ _MICRO.BIOLOGY _, J ' . / 1 1...-t \. Lt t 7 ..) / _ _;:. Parameter __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lO0mls Date Received APR 1 9 1990 fJJ.9 p j Total Parameter Results mg/I Parameter Results mg/ 1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _TDS __ Fluoride -------__ TOC _·_Iron -- __ lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB'.s __ Petroleum __ Endrin __ Lindane Results mg/ I Parameter Results mg/I __ Methoxychlor < rh Lo pPM._ __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- Parameter RADIOCHEMISTRY Results PCi/ 1 __ Gross Alpha __ Gross Beta Date Reported__ ..)--'-;L--f O,.., ~s-BJJr, Date Analyzed l/-~3-901/p 5-/-CJo/3fJ sosoo1-J1 Lab Number _________ ...; _______ _ ~-· '(.JS ?:me __, F ' N. C. Osepartment of Human Resources Di-vision of Health Services ,5 u ~j>-P r SAMPLE ANALYSES REQUEST Seate Laboratory of Public Heal P. 0. Box 280• 306 N. Wilmington Sere Site Number Raleigh, 276 ;Ve, o 'l~o ~-O:l 16 3 Field Sample Number _/:__~_--=6:__::<2::..._ ... _s~------- N f S. I} \....:'_ r' ·), /_. . . / /'' , I 1 S. L . c/ .-... , / ' . -! ;'1 /, ; ) ame O ICC ---'r--=--'-=---'-=---(·•_. c....-'_,,1_··e-· ~· -·-'---'---------1te oca.t1on ' ,,.,., · . .-:, 1 ·', /'! ,. : ., ., r r ' v) Ir: r1 () -/ ( Date Collected '7 / ) ?{ ) Cj C Time A //,1 Collected By }/<,, 1r /c ·, .A1, · 1\ Type of Sample: 4/ 10# ------'--'--- Environmental ___ Groundwater ( 1) ✓ Surface Water (2) __ Soil (3)- --Other (4) Co~~~--~~ __ Solid (5) __ Liquid (6) __ Sludge (7) Other (8) A -S j_ q)~ It ~ Comments /)1 ;:., ,·, . [ I 1:: 0 S Q (._; (, ./ '-! , , · 1' INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph ___ Lead __ Chromium __ ConduGiviry , --Mercury __ Copper _TDS ' __ Selenium , __ Flue.ride -------__ TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury --·····- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/1 Parameter Results mg/ 1 Parameter ~T:GC/MS ~B __ Methoxychlor 1d:B/N Ext. __ PCB'.s <ollopP-~ __ Toxaphene _TOX __ Petroleum _2,4-D L CJ". i o ro h,.•r.-z.D, c. ,, .. ·J __ Endrin __ 2,4,5-TP (silvex) ,/ ( 1-d oroOi:llZ-O~N.:;r.:,L .. ,~:,1\ __ Lindane -- ,/ c .. ?;~ ~;"' ·re, r-/()1 e r-CL-~11.'-..·:' J r.,}< ,,_ 1--. /(_ 1--. ": 1 9 11 t-,, ~ .. ,.,., ,_, () ,,, A;,1,"'1)yfICROBIOLOGY RADIOCHEMISTRY _,, -'! L·t /\ i_/ /~,' _) /_:;.. Results mg/ 1 ---- Results mg/ 1 Parameter 1 Parameter R es ults PCi/1 __ (MF) Coliform Colonies/ lO0mls __ (MPN) Coliform Colonies/lO0mls Date Rectived APR 1 g 1990 81) --pe/3 ;- Date Extracted L/--,23--901/P [WA 4--JS-C/O AA ' Reported By OHS 31 91 ( Revised 7/85) __ Gross Alpha __ Gross Be ta Date Reported A PG/3-'s {3/J Dare Analyzed L/-2,3-C/Ojlp 5-J-1or,f) Qn-:-:-0 -~ fJ ~7-.. .... ~: .• ,?J ..,,._ .. Lab Number N. C. Di;parcmenc of Human Resources Division of H.:alch Services >= r 4- S u 1;>-P r f"\ J f \j 7[ SAMPLE ANALYSES REQUEST Site Number Scace Laboratory of Public Hcal1 P. 0 . Box 280~ 306 N. Wilmington Sere Raleigh, 2761 /1/(., n l ?{o -=t%::O;, /{;, -=-~ Field Sample Number __ l _o-_·c_,_fc_b _______ _ ·-·~f-','.7'-'-'-'-.'·."-. .:.;:; '----',-,"'-'--'---·-'-'·.....,:1...,_'_1\_(_)_.f'_! _· ,_1 -,l ID# __ .,_/.:....' I ~1·_' --DaStieteCLoolcleac~tieodn ~-/.,/· ,)so,,:;,-/,/ /la~,c('.",/ h1, r ,T,,im,.,ei ff M' ! ci, Collected By if, Ir/, .5 }. /; A --...; f Cl --(__ ' ti Type of Sample: 8--6 . .-, j tyu..J e ~ Name of Sicc En vironmen ta! ___ Groundwater (1 ) ___ Surface Water (2) __ Soil (3)_ __ Ocher (4) Concentrate ( I ---rrtS-> ✓ ~ (5) __ Liquid (6) __ Sludge (7) __ Ocher (8) Comments , I ( ;\ , , ; , ·? . ; ·s ., } Q { f--, ct ,i o ) i; -z....e fo r / f)! '2_ C, /) i: (S INORGANIC CHEMISTRY Extractables Parameter Results mg/ 1 __ Arsenic __ Barium __ Cadmium ___ Chromium ___ Lead __ Mercury '_._Selenium __ Silver -- --- ·. ---· -.. -- -- Parameter Results mg/1 ~T:GC/MS Acid:B/N Ext. -. TO,X. . J L (../'\/o r ukc2c-,c.:,,,·. L ( I\ Jo r o b, 1, 2-0 ._,,,n·~ rt1 ,-l ,1 l , · J '.· , d 1~~-i~1C·//~ C ,.-(C ~/1''•,'ro,/, ·,_,,: f · 1,· f'\ fV\' \J ,, ..,.... I i-, . ,.,.',I() ; >·' '.,\,1 ,j, tl I )yfICROBIOLOGY j .• .'' ._ t '\ LI I l.. ' ~) ,' -~ Parameter 1 --(MF) Coliform Colonies/l00mls --(MPN) Coliform Colonies/l00mls APR 1 9 1990 B ,(\ Date Received IY Date ExcractedPf/3..J...3-9oyp 5/JIA Reported By OHS 3 191 (Revised 7185) , .... I: I ·-J LI-a--...:-.... \Y/_,.,..,,. /0 ,..,.;.-.,, 7 /P,,7) Total Parameter Results mg/1 Parameter Results mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph 1--Chromium __ Conductivity __ Copper _TDS __ Fluoride -------__ TOC __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB's __ Petroleum __ Endrin __ Lindane lJ -J_y 90 flA Results mg/ 1 <o.lOPJ2.~ Paran,eter __ Gross Alpha __ Gross Beta Parameter Resul cs mg/ 1 __ Methoxychlor __ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/ 1 Date Reported ...-,,,=-,,..------..,.-,-,-.,.---------1'Cl3's BPA Date Analyzed Lj-:23-90-YP S-J-'fo BfJ. Lab Number "-,§ __ , _, 15- 'N. C. Department of Human Resources Division of Health Services Su j)..P f' I SAMPLE ANALYSES REQUEST State Labo ratory of Public Heal P. 0. Box 280 306 N. Wilmingwn Sm Raleigh, 276 _!...:.A:.......Fe,""'' '----"--'0_0_·1-=-~-=-o-~_,,_·O_,_;=-=J .__:..:/{;::...,~'_,,.._S __ Field Sample Number __ \_~_· _,,C~J--l.b-~'---7'---------Site Number Name of Site --'f-~_-..:::C'--'....:;-·'==--·)---'!=~'-l,=-·•'-. .,_l'.c-'(...:.·_,-'-f-'-!--'-~-·,_;_;) _________ Site Locarion c_/,,.,. . s (; ·' /). ,: -r h.,/., ~ r' r: i :· ;) Collected By l{J /;;-_<, A/r ,-r\ Type of Sample: 01 / <-JJ. oJc, 1D# -----'--'---Date Collected ~ ) ~ / fr, Time I() -Id j 1 fi)cu)g~ Environmental ___ Groundwater ( 1) . -/Surface Water (2) _V_ S 'oil (3)_ __ Other (4) Concentrate __ Solid (5 ) ___ Liquid (6) __ Sludge (7) ___ Other (8) Comments ,, / ( /'-: s; ,; ,·' f'o f INORGANIC CHEMISTRY Extractables Parameter Results mg/1 __ Arsenic __ Barium __ Cadmium __ Chromium __ Lead __ Mercury 1 __ Selenium c; l i=~I vcr I /-- --··-· -- -- Parameter Results mg/I ~T:GC/MS Acid:B/N Ext. _TOX . , L ( J"l i n r e ,L,,r""2c-? c. a ,i J L r /\ I(; r o G-: n Zc~/-{ ,, rr,:, c Ct l,·J r, ..... .., "" ·t , Fy · , ,/ (,<. 1) l.i C, / i, ('. ,.-C:; _:.,,,,n,, ·,' f\,./, - • I ' \..·l I ~ i../ ! -... _) / __:., Parameter ' __ (MF) Coliform Colonies/l00mls __ (MPN) Coliform Colonies/lO0mls APR 1 9 1990 {3f) Date Receiverl Date ExtracteJl;ff...L/()1/p jj()JA Reported By OHS 3 I 91 ( Revised 7185) ("' .l : l --J u ____ .J-.. -\'{/ ____ ro __ : ____ -, IC:'\ Total Parameter Results mg/1 Parameter Results mg/1 __ Arsenic __ Silver __ . Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conduccrvicy __ Copper _TDS ,--Fluoride . --------__ TOC ___ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCBls __ Petroleum __ Endrin __ Lindane Results mg/1 -<o,Jo 'f2/2.rr-._,, 7- Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/1 __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 Date Reported --,.,-----------------JC-f:;s 6µA Date Analyzed 'f-23-C/OJ/p -:f-J-9D BlJ Lab Number QI) r;:· n .,~ r_;, ,._., '-.. ,_JJ V _.., ."1,, - N. C. Dep.arcment of Human Resources D~vision of Health Services ~.s ~A ..,,., f· Suf-Pr SAMPLE ANALYSES REQUEST State laboratory of Public Hea· P. 0 . Box 280 306 N. Wilmington Sm Site Number Name of Site 11v· n °lv,1 ~,o-, u-~ I ':l !.) . ;., z --'-/--=--t=G"'--'....,. __ ..c,.o_C.. __ ~ __ .-.--'--~==--~/0:~·-··_-_> __ Field Sample Number ~_(_.)._L __ ({ __ -________ _ Raleigh, 276 0 ( ;':'_ / . ,. . / ,{'. ! ! ·....._. f ._) '-' C i I' ,' ,.'. I ' · If.. ) ; . , Collected By • (1 I' I tr 5 I: /1 , r\ !_JI ID# --~' ~/ ___ Dace Collected Type of Sample: Environmental {[-b--) Concel)t~a~e. "- ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (J)_ __ Other (4) . 1 .. , r.; S-~ Sdtr&-(5) __ Liquid (6) __ Sludge (7) __ Other (8) t ; c--: +, _l {-fhf1e -~ 1 C -/)~rs INORGANIC CHEMISTRY Extractables Parameter Results mg/1 ___ Arsenic __ Barium __ Cadmium l~Chrnmium ____ Lead __ Mercury __ Sdenium -·--Silver --I -- ---~-·- -- -- Parameter Results mg/1 ~T:GC/MS Acid:B/N Ext. _TOX . . £. C .{" j n r u h,,,i-z.o : c_ u c,·J L_( /\ i 0 r C-b '.' f1 Z.O l.,J+'<) r r,: , L c1 l, · ,A '," c-?1~~.-•c,!li, ('. ,.-CC~1/N<1n,/< '' r-.:. .,_ ,N•f,(.f's ,.C,h, , ,. r , ,, , ) r: ; 0 ·-' A,'.· J, /1, i "MICROBIOLOGY I . I I l..·l I I.. (..f ',_,. ._) ,' _;, Parameter ' --(MF) Coliform Colonies/l00mls --(MPN) Coliform Colonies/l00mls Total Parameter Results mg/1 Parameter Results mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Cond"J:::vicy __ Copper __ TDS __ Fluoride --------__ TOC __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 Parameter Results mg/ 1 __ Merhm:·1chlor <oiLO-P/2~-__ T oxap!:ene I-__ 2,4-D __ 2,4 ,5-TP (silvex) -- RADIOCHE\1ISTRY Parameter __ Gross Alpha __ Gross Beta Results PCi/1 Date Received ~"'7"".A,-P_R_l_g_1900 __ {3_[J _______ _ Dare ExrractJtfJ.3-90\/P Dace Reported ~-,,---------~-------pee,~ 6 ,v It Dace Analyzed Y -2,3-90-YP 5-(-CJuM Reported By Lab Number DHS 3191 (Revised 7185) , .. I · I --J tJ ____ J ___ ,v, ___ ,n 'N. C. Gcrartmem of Human Resources Division of Health Services :~¾~ .. 5 v 1P--P· r SAMPLE ANALYSES REQUEST Seate Laboratory of Public Hca P. 0. Box 28( 306 N. Wilmington Ser Raleigh, 2 7c Site Number /1 0. V1 .::;&1,/ l...,,..., /j-....... .) ) d O (, c; _ __,/'--! tLl:....'_..,,,C"",'----"-Q.,____ _ __;1 l:c...1.=.:.... __ r:;;?(i; __ , .. __ --",'==--~.;;..;!&;=-,--•, _."':_> ___ Field Sam pie Number _______ (9 __ / ________ _ .(J (. ,/'_·_., ,i . c·., ·1,._ .-.-'./ ('' I ] S ,· / < JI J Name: of Sire __:._..::.-'---"--~-'-=-"--'-''-'---'--'--'--'"'--'--.L,_,;'-----------ire Loca,ion 7,,,..,., _., ,:; v • /l ,: r ID# __ lJ-'--, --'-/-~ Date Collected -'--f j ) ?{ } 9(: h/, rr " r: lnr) Type of Sample: C --5-I . q~J c, ~ Environmental ___ Groundwater ( 1) ~ Surface Water (2) ~ Soil (3)- --Other (4) Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Ocher (8) /) r I(") o <, "' ' I I :· 11 c,) ;cu fp ri. INORGANIC CHEMISTRY Comments ,< /'. ( /::_, ,..,. ·,· :? Extractables Total Parameter Results mg/ 1 Parameter Results mg/1 Paran1eter __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS ' __ Selenium I __ Fluoride . --------__ TOC __ Si lver 1--lron -- --1-Lead -- --__ Manganese -- --· -__ Mercury --..... --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/ 1 Parameter Results mg/1 Parameter ~T:GC/MS ~B __ Methoxychlor td:B/N Ext. __ PCB's < a LO:r>Qrr\_. __ Toxaphene _TOX . . __ Petroleum r, _2,4-D L ( J'\ i () r'U h;.-,~-z.c , c. u c,-J __ Endrin __ 2,4,5-TP (silvex) L_t /\!urob'.'t1Z..Ot,J/~rr,1 ,L ,1t,,,\ __ Lindane --., VCt 0\0/1 F?': / ' ·" C-<;,u o!),cv-ccf\1f!i:JJ'\ . ./, . ' Time \-3 P/Yl I Results mg/ 1 Results mg/ 1 . ,_ "· /'Y\ ; ':j ii t' . -.. _ ,. ,-~-· _. '--;-r:,~· _; "~· _·_;~:\,~;~, J~• "-'-(\fc' i' .,,,_.M~I~C~Rr-,-,-O-"-B_I_O---,'--L_O_G_Y ________ --,-___ -,--____ R_A_D_I_O_C_H_E_M_IS_T_R_,Y ______ _ I Pa ram~~~~ ~, ' "' 1 '/ _, : _::.-Parameter Results PCi/ 1 --(MF) Coliform Colonies/lO0mls --(MPN) Coliform Colonies/lO0mls APR 1 g 1990 /3/) Reported By DHS 3191 ( R~vised 7 /85) __ Gross Alpha __ Gross Beta Dace Reported~-~~-----~~~-------Pa8 :'J--ISNJf Date Analyzed L/-,23-901(p S-f -CjtJ6/) Lab Number N. C. E)eparcmenc of Human Resources Division of Health Services S§Zp ►:' ,5 u 1/>-f) (' SAMPLE ANALYSES REQUEST Site Number Scace Laboratory of Public Heal P. 0 . Box 280' 306 N . Wilmington Sere Raleigh, 276 -'--'/tf'------""G"-"-'Q'--_"1....::~-L.-,_· -~--.,O--'-;l~/4~L_:, _::_-> __ Field Sample Number -+-} __,_~______.{...:...)_7'-------'(,;;._) ______ _ /7 _,-·) / _ j ,f'-'J) <-;I /J e )•/ . Name of Site ----';_·.c.:·•-_.,_;i .)::__.....:'--=-c...(.c..··1---'-''\__,_-'-'-. '-' --'--'--.-~' -'-'---------Site Loca;ion ,--·~-~.,..·-•-----'.---=-:,_,_c_; •.c..'-'i-,.'-'-/1_,c.~· -'-1_....;'v....=.,-c.,-'r-',-''-' ..:..'''-· .:...f .:...n:..!.ri..:__ __ _ ID# 4 / Da1e Collected . '7 / J 8' / 90 Time /-3 f (?'.' D-(; -_ I q)u.-d 7> m~s Type of Sample: Environmental ___ Groundwater ( 1) ___ Surface Water (2) __ Soil (3)- --Other (4) Concentrat~ c s· t</ ~l;d~ (~) __ Liquid ( 6) __ Sludge (7) __ Other (8) Comments (1 ✓· ,;.. I \. I \ 1·1 ·,• J -I' ) (' '· I, } c 1---!-, ci " o . u -z_..,e_ re i ·-/ ): e_ o 1 A e rs INORGANIC CHEMISTRY Extractables I Total Parameter Results mg/I Parameter Results mg/ I I Parameter Results mg/I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates __ Cadmium __ Cadmium __ Zinc __ Chromium __ Chloride _Ph __ Lead __ Chromium __ Conduc:ivity __ Mercury __ Copper _TDS __ Selenium __ Fluoride . -------__ TOC __ Silver __ Iron -- --__ Lead -- --__ Manganese -- --· -__ Mercury --...... --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/I ::; ;:..-;· ~.:c.~ I'.'~ ;,9 ~\/ 1, .~ ,-)',;:i: 0 ICROBIOLOGY . i . • ~-l ·• l..t ( '7" -> / _-., Parameter · --(MF) Coliform Colonies/l00mls --(MPN) Coliform Colonies/lOOmls Parameter _J;.DB _\.,,/"_pprcB'.s __ Petroleum __ Endrin __ Lindane . APR 1 9 Date Received Dace Extractfo~-901/P 1990 ~,G Reported By Df-lS 3191 (Revised 7185) Results mg/I Parameter Results mg/I __ Methoxychlor <IJ, !()OD,,..,__ ___ Toxaphene _____ ,, ____ 2,4-D __ 2,4,5-TP (silvex) RADIOCHEMISTRY Parameter Results PCi/1 __ Gross Alpha __ Gross Beta Date Reported --------~~-------- ?03~ 13 ~·A; Dace Analyzed Lf-,2-3-C/Oyp .f'-1----9oA(J Lab Number • N. C. Department of Human Resources Qi vis ion of Hc:alch Services :::,--== . ---~ r~ ,5 u JJ> --P r SAMPLE ANALYSES REQUEST Scare Laboratory of Public He, P. 0. Box 28( 306 N. Wilmington Ser Site Number Name o f Sire / Raleigh, 27t --'-J1-'--V-'e,""'' ~Q,____,-_,V.~~1_L'_· -~-~_,_;;_·l--'7,~·1~/i--'L~·~-~-~---Field Sample Number -~j -~ __ 0_7 _________ _ '.(} \r·.. ,,),. / } .{' ' / ) . . ~ I . .,, .... J I •. t:' )., / --~ c:., ,, ' .. I. I Site Location ;,-,..,· .:, '·' c', /1 c· / 1/C, r _f' f' r) } (~ /I if /) < j } ... Collected By / . .-:, r · ::t · ' 11 ., ' , (1, IDF.' __ !.../--'.--'-/ __ Dare Collected . w / ) :€{ ) 9(> -t-I I Time ____ _ T ype of Sample: 0-5-I. €;)~ D a-~ Environmental ___ Groundwa ter ( 1) 7 Surface Water (2) __ Soil (3)- --Other (4) Concentrate __ So lid (5) __ Liquid (6) __ Sludge (7) __ Ocher (8) ;'\ f'/ <::a s [' .' i ,.. ' ' l 1 ['_-,-• .L. t-f-/i1'·(,0 "" r v, C ') ;,·;• i.-i '" ,,, // c., .__,t.. ,: • /c_ ) c f-+ , o ;, o ) u c--e f'o r I f/2e_ oi)e r.s , I i : . n c d , c rl: I P vi. INORGANIC CHEMISTRY Extractables Total Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/I __ Arsenic __ Arsenic __ Silver __ Barium __ Barium __ Sulfates ___ Cadmium __ Cadmium __ Zinc __ Chromium __ Chlo ride _Ph ___ Lead __ Chromium __ Conductivity __ Mercury __ Copper _TDS 1--Scleni um __ Fluoride -------__ TOC __ Silver __ Iron -- --__ Lead -- ---__ Manganes e -- ---__ Mercury --···-- --__ Nitrate -- --__ Selenium -- ORGANIC CHEMISTRY Parameter Results mg/I ~T:GC/MS Acid:B/N Ext. --,-TOX . .. . j ~ ( ..{'\ / r~ !'() L0~'2c 1·c. u (;·c L ( /\ / C: r o 0,' n l-Ov/-{~ rr,:: l c1 ( ,· ( A ,/ c1"'t~~,"·'c.~?f;I ( ir C~,-~r~•,.,•ri,J(, --(MF) C oliform Colonies/l 00mls __ (MPN) Coli form Colonies/l 00mls Parameter ~B __ PCB'.s __ Petroleum __ Endrin __ Lindane Dace Received APR 1 g 1900 .,!3/). Date Extrac re~3-'101/p /]!!} lf,2,5'-?0 AA R e ported By DHS 3191 (Revised 7185) Results mg/I Parameter Results mg/ I __ Methoxychlor -<a,LO ~-__ Toxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Parameter Results PCi/ 1 __ Gross Alpha __ Gross Beta Date Reporte~ J 13/Jlt Dare Analyzed ~~#-90-vP 5'-.)~1of,[) Q')r:·0·11 ,1·• Lab Number ._,,.__ .. ii· ..,,'t) r N. C. Dep.arcmenr of Human Resources Di lli s ion cf Health Services ,5 u 1J> -f,· r State Laboratory of Public Heal, SAMPLE ANALYSES REQUEST P. 0 . Box 280~ 306 N. Wilmington Sere Sire Number Raleigh, 2761 Field Sample Number __ .:....\ _1 .:::.0.....:.· -""'{)"""\ _7..:...._._d-________ _ './: (_ .. ·\ / , ·.\ ·1,. ,. ./ .,r'_, . I ,1. :::_/ : , ,,.. )1· / ;· Name of Site __;_....:c'--;.....J...;='--''=-'-'--'-"--'-''-'--'-~-'--''-----------Site Location ,-c'-·-'-•·r~. ·_-"<;-';"-'-_; c.:..',:+/..:..;._. ~-·....:.·~_.:..::::...1/..c:,C•,__;__r L( ::..." --I.1'7:.!_'._..!.. r--': r1c..2...._ __ _ 'f. } ; ' . Collected By i. .·, Ir ii?_"", ()/i · (\ ID# __ lJ-'-, ....... /_' __ Date Collected . Y J } f-5 ) 9 (; I I 1 Time-3 ~f..-W~- S ~J Type of Sample: 5 Cl W\ r /_e_ 0--;;tJ_ c....dt_~ (J~ Enviro nmental Concentrate ___ Groundwater ( l) Solid (5) __ Surface Water (2) Liquid (6) J.L_ ~) 5 ec!i' mt ¥t + __ Sludge (7) __ Other (4) Other (8) ;f C.i C I ' .. / ,· n ') . ,.J ). P / . Comments ., /· _,· 1 ~:-/ ·,+ i ... I / '· 'i ' ) .I \ INORGANIC CHEMISTRY Extractables Parameter Results mg/I __ Arsenic __ Barium __ Cadmium __ Chromium ___ Lead __ Mercury 1--Selenium __ Silver -- -- ---~ ... -- -- Parameter Results mg/1 ~T:GC/MS td:B/N Ext. ZTOX ' · ,. J" i <) ru ,~:.,n--z.c-; ( (; 1,·J L< /\ / (;-( 0 be 11 z.o,.){0 rr., 1 C c, , ,· ii\ ' ~ c.?,:~,.,_ ·,c, ~IA C v· C ~,~1/)1) ,_: 0,./ ( ·\.~,· ~ . c '"'· rn .. ~ Ii I , ;, , • ,.· .• ,,; ; ,,1 ,:\, .J, ,11}1ICROBIOLOGY ' ,'' • '-:. I ~ Lt { l ... -~ ,' _:::, Parameter -' __ (MF) Coliform Colonies/lO0mls __ (MPN) Coliform Colonies/lOOmls ,81) Total Parameter Results mg/1 Parameter Results mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _TDS __ Fluoride ---------__ TOC - __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B __ PCB'.s __ Petroleum __ Endrin __ Lindane Results mg/1 Qt ::i...7_ pp.rr< :i<f# J ;i.i:~ o -P e.P. 1 Param.eter __ Gross Alpha __ Gross Beta Parameter Results mg/I __ Methoxychlor __ T oxaphene _2,4-D __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Result; PCi/1 Date Receive>p. APR 1 9 1900 Date Excracteo ~;?3' 70-yp Reported By 6.lllfJ Lfr25'-CJo A8 DHS 3191 (Rrvised 7/85) .-. •• 1 1 f • I \VI -• ff', -, /0..,\ 0N. C. 0epartment o f Human Resources Division of Health Services ~w r ,5 \.) 1J>-P · (' SAMPLE ANALYSES REQUEST Sire Number Scace Laboratory of Public Hea P. 0. Box 280 306 N. Wilmington Sm Raleigh, 276 //:!.,·,,'/. () CiV.-. ~10-, I/' --2 ~-0 7 '::? ----'--''----"''-""•~,___1....cO'-i.i....._· 1 __ i;;;-u::_, ... ~·~'~--'IC~···,_ .. _> ___ Field Sample Number ________ 0 _________ _ r--,,: ... /1''1 ! ,.,;_ .. ,.. ___ ;, _.r J'l~ ; Name of Site , '--· i ' , __ <-1 i\ r -· ' : Site Loca~ion 1 ·" · -' '·-' ,, , r, .:, 1 /(, r ," r7 :· ,-: r"\ ~//-'-'-.•:-'--'., 1_··-"/.'-, ·=:,~1_\.'-/-_, '--'-''-'------ID# __ l.J_/~/_ 1 __ Date Collected . 0 ,/) f?) 90 Time 3 /? Wl Collected By Type of Sample: ~ I 5l\ M, pl ( 3 l~~ p-fe/t-) Environmental ___ G roundwa ter ( 1) ___ Surface Water (2) __ Soil (3)- _j_[_ Oth-cr ( 4) lJ~ f u a.I Concentrate __ Solid (5) __ Liquid (6) __ Sludge (7) __ Ocher (8) Comments / / ' / :._ / \ .,-·' I I ~-' . ./' 1 } f' ' -~ I Q r-, , o 11 {./ • <1 -z_.e_ ro r f h e_ o :I /2 e rs ' I I ,· lJ r ) ; ( (). i p J , , e ; INORGANIC CHEMISTRY Extractables Parameter Results mg/ 1 __ Arsenic ___ Barium ___ Cadmium __ Chromium ___ Lead ___ Mercury __ Seleniu m ___ Silver -- -- ---...... -- -- Parameter Results mg/ 1 ~T:GC/MS Acid:B/N Ext. \ / ~°;~ i n t' r.,: ,l, F 7.c ,(. (1 r ;J L ( /\ !c ro iJ:117-ovH~rr.,, c n t,>A , .. ., ........ c.?,~ -,-: 'o ~Ii, t: (·' C ~ ;,./J,)-.J r,,/ { ' . , . ,'-' • 1...-t ~ 1..1 /'-/ _) /_--;, Parameter · __ (MF) Coliform Colonies/lO0mls --(MPN) Coliform Colonies/lO0mls Date Received APR 1 g 1990 6b _ Reported By DHS 3 19 1 ( Revised 7185) Total Parameter Results mg/ 1 Parameter Results mg/1 __ Arsenic __ Silver __ Barium __ Sulfates __ Cadmium __ Zinc __ Chloride _Ph __ Chromium __ Conductivity __ Copper _TOS __ Fluoride -------__ TOC ------ __ Iron -- __ Lead -- __ Manganese -- __ Mercury -- __ Nitrate -- __ Selenium -- ORGANIC CHEMISTRY Parameter ~B _\_PCB's __ Petroleum __ Endrin __ Lindane Results mg/1 </._, QpprYG Parameter __ Gross Alpha __ Gross Beta Parameter Results mg/ I __ Methoxychlor __ Toxaphene _2,4-0 __ 2,4,5-TP (silvex) -- RADIOCHEMISTRY Results PCi/1 Date Reported ~=-=-=7""""------=----------1)(!,,!3:5 8/vl+ Date Analyzed' Lf-30-q(!VP .:[-..1-9tJ81Y Lab Number Cnain of Cus:::od'-" Reco-::-d E2z2rdous ~2ste H.ateria.ls ~oc2:icJ o: S2..mpling: Generator Transporter Irea~~~t Faci.l __ Storage Facility Other: Disposal ?acility {Zandfi.ll ---------------------------- '.: ~p2;y's" N 2.IDe __ ~f---=C::::.1___..!..hL' _L_c,,~· ...1.l'.1L._J.:'.c)L 1 ..J.j_"...!...1 _· L/ .:-T ________ l el e ;rn one( ____ ) _______ -7 __ _ A.d dress \V C,1 1 f -:._ 11\ { ( ------~_____.:::'.~_!__-'-"'-"-+:---->=----'----,---------------------------- Collector 1 s Na.me _ _;:[:=:::.._~,i.<J/='A.-'L/--"-G,.__Jti.-'-'-. ..:..' l.,--=--7 _J+!/4_,\::...;:,Ju--=---:c=-/4,._,,Vi:....:..L='-'· ___ T ele_::iho~e( ___ ) _______ _ Y /. ) r,_.) f ~1incrn1re .:-. Date Sc.:::uled -;,,; / Time Sa.mp led -------'--+-"--=--+, ------------ 10 11 J/1 ✓ , ')a /) 1, a -;-; ,,J t rl} l i<.12. st e £.CD d I sp OJ Cf ( --¥--'""'-'-.c::.__"'""""-'--'---ftf-"--'-'---L-+-------------Gener2.t-:ng v Cnc.i-::: c: ?oss·ession: 1. signature 2. signature 3. sign2.-cure .()Cl~CS I " (I I '\ ,cl. v / c::----. title inclusive dates inclusiv e dates lns::-u ctio;-i s: Complete 2.11 2.pplica·ole i.ifcr.::ctio .. inclucin6 s igna tures , 2:-1d submit '\.:ith ·.2.nciysis reaues: fo:::-I::s. STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O . BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C . 27611. ORGANIC CHEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD# COMPOOND TYPE UNITS N-nitrosodimethvlamine tnl :?3o bis(2-chloroethyl)ether 2-chloroohenol phenol 1 3-dichlorobenzene 1 4-dichlorobenzene 1 2-dichlorobenzene bis (2-ch loroi sooroovl )ether hexachloroethane - N-ni troso-di --n--0roovl amine nitrobenzene isoohorone 2-ni troohenol 2 4-dimethylphenol bis(2-chloroethoxy)methane 2 4-dichloroohenol 1 2 4-trichlorobenzene naphthalene hexachlorobutadiene 4-chloro-m--cresol hexachlorocvclOOf>ntadiene 2 4 6-trichloroohenol 2-chloronaphthalene acenaohthylene dimethyl phthalate 2 6-dinitrotoluene acenaohthene 'V 2 4-dinitroohenol S0/ihSO 2 4-dinitrotoluene I0/330 4-ni troohenol 'S'O/;t.,50 fluorene /0/.330 4-chloroohenvlohenvlether I diethyl ohthalate ,v 4 6-dinitro-o-cresol So/J~.r;o di phenyl amine I azobenzene ~ 4--brcrroohenylphenylether /()/.330 hexachlorobenzene 10/_?.10 pentachloroohenol S0//05"0 ohenanthrene JIJ/330 anthracene dibutyl ohthalate fl uoranthene \" J -Estimated value. ml)L flz..O/SO/l- 90Soo9 CJos-o Io l~OCPL/ /_:l, Ou:;S ( "}) ( 3 ) ~(uq/kq ~(µq/kqJ Ii _ I,/ \/ \/ K -Actua l value is known to be less than value given. L -Actual value is known to be greater than value given. 90SOI I /-l,o~f.o ( "5""'") ~µq/ko' t,/ \V q oS o I .;J. I,;), O(o 7 ( :;, ) ~ u q / k q) . /.,( I ,; 90501 ~ l~o(p 9 (S) ~q/kq I A' \I/ U -Katerial was analyzed for but not detected. The nurber NA -Not analyzed. is the Hi nirrun Detect ion Limit. rn Ti L -- -1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. N.C. V-<-v,U -<-On. 06 He.al.;th Sviv-<-C.U VHS 3063 -0 (4/86 LaboJta.:to~y) - CD ( ) µq/1 uo/kq STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUKAN RESCXJRCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 ORGANIC Q-lEMICAL ANALYSIS BASE/NEUTRAL NID ACID LAB NO qosooq CJoSo/D 9'oSo! I qoso1.;i_ 9oSoJ? EXTRACT ABLES FIELD II 1.:i.otot./ /~()ijJ I .:?fJ(p 0 l.:J.C>fo7 OJMP()JND TYPE ( S) (3) ( S) (3) UNITS ~q/kq u.or-1 (i;q/kQ I ~oiq/kq ~l(1Jq/kqJ pyrene I0/330 IA LL-IA iL benz idine ."l"IJ /11,.~o butyl benzyl phthal ate /0/330 benz(a)anthracene chrysene J, 3 3--di ch lorobenzidi ne sol!h50 bis(2--ethvlhexyl)phthalate 10/330 di -n--OCt vl ohtha 1 ate IO/.l~o benzo(b)fluoranthene so/11:Do benzo(k)fluoranthene benzo(a)ovrene i ndeno ( l 2 3-cd) pyrene dibenzo(a h)anthracene benzo(q h i )oervlene \/ \/ \/ ,i; ,y aniline so /11-, "o L,{_ I.,(__ [;{ -I,,{_.. benzoic acid benzyl alcohol 4-ch 1 oroan i 1 i ne ' / dibenzofuran 10/3=?0 2-methyl naphthalene 2-methyl pheno 1 j ~thvl oheoo l -.ll' 2-nitroaniline S"o/;~',o 3-ni troani line 4--n i troan i 1 i ne 2 4 5-trichlorophenol -..,J/ \I \/ \! ,I f111)L- J -,Estimated value. H2.0I SOIL.. to be less than value given. K -Actual value is k~n L -Actll<ll value is k~n U -Katerial was analyzed NA -Not analyzed . to be greater than value given . for but not detected. The nuroer is the Min irrun Det ection Limit. 1/ -Tentative iden tification. ~/ -On NROC Li s t of Pr iority Pollutants . N.C. D,zv,z_.!J -tO>t 06 He.a.Uh SVtv-tc.e/2 DHS 3068 -0 {4/86 LaboJt.a.):o ~y ) l~olPR (-5) ~1cuq/ka l,L \/ U- ,V 0 ( ) \JQ/ 1 uo/kq STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOORCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 BASE/NEUTRAL AND ACID LAB NO EXTRACT ABLES FIELD # CCl"IPOOND TYPE UNITS N-nitrosodimethvlamine fr,/ ~=30 bis(2-chloroethvl)ether 2-ch l orooheno l phenol 1 3-dichlorobenzene 1 4-dichlorobenzene 1 2-dichlorobenzene bis (2-ch loroi sooroovl )ether hexachloroethane - N-nitroso-di-n-oroovlamine nitrobenzene i =horone 2-n i t rooheno 1 2 4-dirrethvlphenol bis(2-chloroethoxv)rrethane 2 4-dichloroohenol 1.2 4-trichlorobenzene n;inhthalene hexachlorobutadiene 4-chloro--m-cresol hexachlorocvclooentadiene 2 4.6-trichloroohenol 2-chloronaohthalene acenaohthvlene dirrethvl ohthalate 2 6-dinitrotoluene acen;inhthene 'V 2 4-dinitrnrihenol S0/JhSO 2 4-dinitrotoluene 101::r~o 4-n i t rooheno 1 '.So/J1,.~o fluorene /0/~30 4-chloroohenvlphenvlether I diethvl ohthalate -L, 4 6-dinitro--o-cresol so/Jrnso diohenvlamine I azobenzene 'V 4-braroohenvlohenvlether !rJ/..330 hexachlorobenzene I0/330 :>entachlornrihenol so/11oso )henanthrene /t)/330 anthracene dibutvl phthalate fluoranthene ',v J -Estimated value. m""D L fl2..0/SO/l- ORGANIC CHEMICAL ANALYSIS qoso1 '-I qo_"J 0/S q oso; ta /~00 CJ /,:,{0 70 /-?o7 / ( . =3) ( -')) ( .::,, ) ~uq/kq ~uq/kq) mf1-Yu-q/kQ) IA LL IA \I \I/ \v < -Actual value is known to be less than value given. CJl).'10/ 7 /~07c:J.. L3") -w:i."(\JQ/kQJ II \V CJoc;-01?? /~073 ( .If) ~ Cuq/kq ..... LL ✓ \v L -Actual value is known to be greater than value given. J -~~terial was analyzed for but not detected. The nu:rber is the Min i1TU11 Detection Limit. rnJJL ~ -Not anal yzed . -. --- 1/ -Tentative ident i fication . ~/ -On NRDC List of Priority Pollutants. ! • C. Viv,Ui,Z_o n. 06 HeaLth SVtv-<-c.e/2 ·Hs 30 68 -0 (4/86 Labo~a.to~y) ( ) 1 uq/1 ua/kq r . STATE LABORATOOY OF PUBLIC HEALlH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOORCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611 OOGANIC OiEMICAL ANALYSIS BASE/NEUTRAL AND ACID LAB NO 9fJ5'0/L/ 9050/S C/OSOI& 9t1 \0/7 EXTRACT ABLES FIELD fl /.;?o/2 9 /<>{070 /-7.07/ /oln 7C:Z COMPOOND TYPE (-3) ( ~) ( ..3) (3) UNITS ~(µq/lcq ~~('µq/kq ~(Gq/kq~ ~q/kqJ pyrene /0/~30 I I u_, . i.,c:: IA._ benzidine S-tJ/J/60 butyl benzyl phthal ate J0/330 benz(a)anthracene , chrvsene J, 3 3-dichlorobenzidine so/11,..,0 bis(2--ethylhexyl)phthalate lo/330 di-n-octvl phtha 1 ate /0/.1~0 benzo (b) fl uoranthene SO/JfnO benzo(k)fluoranthene benzo(a)ovrene i ndeno ( 1 2 3-cd l ovrene dibenzo(a h)anthracene benzo(q h i )Derylene \/ \V \/ \V \/ aniline :Sa/11,,,,:-0 \A_. [IL-LL IA- benzoic acid benzvl alcohol 4--ch 1 oroan i 1 i ne '-,./ dibenzofuran 10/..=Ro 2--methylnaphthalene 2--irethylphenol ~ 4-{rethvloheool 'V 2-nitroaniline S-o/; t,,.r,o 3-nitroaniline 4-nitroani 1 ine 2 4 5-trichlorophenol ',j/ \1/ \/ \V \/ m1H- J -Esti~te<.1 value. Hz.O/ Soli- to be less than value given. K -Actual value is known L -Actual value is known U -Katerial was analyzed NA -Not analyzed. to be greater than value given . for but not detecte<.1. The nuroer is the Hinirru:n Detection Limit. 1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants. N. C. D-<..v.u.i-<..011 06 He,a.Lth SVtv-<..ce~ OHS 306 8-0 {4/86 Labotta.-to~y) C/().\()/ J? /~o7-3 ( '7) ( ) ...mi:t:1 <uq/ka ua/1 uq/kq u.. \/ u_ \/ m::zn ... -