NCN000410161_20110610_GMH Electronics_FRBCERCLA C_General Correspondence 2008 - 2011-OCR

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EPA Home> Superfund >Sites> Superfund Information Systems> Search Superfund Site Information
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Superfund Site Progress
Profile
GMH ELECTRONICS (EPAID
More Details ...
NCN000410161)
This profile provides you with information on EPA's cleanup
progress at this Superfund site. This information includes: Site
Location, Cleanup Progress Summary, Cleanup Impact
Summary. Contamination, and Cleanup Progress. Please use the
links and the "More Details ... " box to find more details on this
site.
$ Site Contacts (EPA Cleanup
Managers, etc.)
Other Names for this Site (Aliases)
View GPRA Measures at this Site
/see glossary\
The data and content on this page were last updated on
Friday, June 10, 2011.
Site Location
Get an interactive
!lli!ll
EPA Region 4 >
Serving Alabama,
Florida, Georgia,
Kentucky,
Mississippi, North
Carolina, South
Carolina and
Tennessee
Site 1600
Address: VIRGILINA
ROAD
ROXBORO,
North
Carolina
27574
County: PERSON
U.S. Congressional
District: 13
Population within one
mile: 0-100
Cleanup Progress Summary
Early Action Construction
Initiated/Completed Underway
Physical cleanup activities have started.
view detailed list of cleanup activities at this
site>>
The National Priorities List (NPL) is the list of
the most hazardous sites across the U.S. and
its territories.
This site is on the NPL and is known as a
Final NPL site (see glossary).
Superfund law requires that EPA give
communities information about site progress
and plans so that they can be actively
involved in site cleanup decisions. Learn ·
more about community involvement at this
site>>
Cleanup Impact
Summary
At each site, EPA assesses
the risk to humans and the
environment and determines
the best approach to
address the risk. During
initial site studies and
cleanup, EPA determines if
current human exposures to
contaminants are under
control and takes actions to
control any possible human
exposures until cleanup has
been completed. Once
complete, cleanup provides
long-term human health and
environmental protection at
the site.
~
·~EPA is
. ;;. workin~ to
,_ · determ me
whether
there are
human
exposures to
contaminants
see glossary definition for
~Human Exposure
Environmental Indicator
Measure.">>
learn more about human
exposure conditions at this
site>>
At each site with known
ground water contamination,
EPA documents whether
ground water contamination
is below protective risk-
based levels or, if not,
whether the migration of
contaminated ground water
is stabilized.
http:/ /cfpub.cpa.gov/supercpad/cursites/csitinfo.cfm?id=0410161 6/10/2011
Superfund Information Systems: Site Progress Profile
Contamination
Page 2 of 4
There is
insufficient
data to
determine
migration
control
status"
see glossary definition for
"Contaminated Ground
Water Migration
Environmental Indicator
Measure.">>
Contaminants (i.e., hazardous substances, pollutants or contaminants) can be found in several
different types of materials on the site including soil and other solid-based media and water or
another liquid-based medium (see glossary).
The contaminants listed via the links below are considered the contaminants of concern {.§_@_
glossary) to be addressed by cleanup actions at the site.
Contaminated Media: Groundwater
EPA classifies contaminants found into groups or types (listed below). To view all contaminants of
concern at the site click on the "view contaminants of concern at this site" link.
Types of Contaminants: voe
see glossary definition for "types of contaminants" >>
view contaminants of concern at this site >>
ATSDR ToxFacts information on contaminants (t:x1 rdi..:,·l•inn·r►I
,..,, back to top I view glossary >>
Cleanup Progress
Major Site Cleanup Milestones
see glossary definitions for major site cleanup milestones >>
1st
Cleanup Listed as
Action Proposed Final on the
Initiated to the NPL NPL
Final
Remedy
Selected
0 o. ~
00. & -r~ <,t w .. • -~·. $ ~,r ~· ,,
12/05/2007 04/09/2009 09/23/2009
http://cfpub.epa.gov/supercpad/cursites/csitinfo.cfm?id=04 l 0 161
Deleted
from the
Construction NPL
Complete ~-;_C,';).:
@ \:t,"' ~t t> G[
6/10/2011
Superfund Information Systems: Site Progress Profile Page 3 of 4
Cleanup Activities At This Site
see glossary definitions for cleanup activities >>
There are many stages of cleanup, inCluding site study, remedy selection, remedy design, remedy
construction, and post-construction. Activities undertaken early in the cleanup process focus on
understanding problems at the site while those taken later in the cleanup process focus on
physically addressing those problems identified.
Many NPL sites are large and complicated. These sites are often broken up into smaller areas to
make cleanup easier and more manageable. These areas are called "Operable Units" or OUs (~
~).
The chart below shows the different types of activities that are underway or complete at each of the
cleanup areas (operable units) at the site. Some activities apply to the entire site; EPA assigns
these activities to the site-wide operable unit (designated as OU 0).
Cleanup Areas
(Operable Units)
OU1
Removal•
Study and
Remedy
Selection
QUO 12/2212007
Complete Underway
Remedy Remedy Post-
Design Construction Construction
09128/2008
view activities details>> view OU details>>
more in-depth site details (EPA Regional
Content)
* At many sites an action, called a "Removal Action~ (see glossary), must be taken to eliminate
immediate and near-term threats to human health and the environment. Removal actions do not
occur at all sites.
Community Involvement
The goals of the Superfund community involvement (Cl) program are to: 1) keep communities
affected by sites informed throughout the cleanup process, 2) provide opportunities for
communities to comment and offer their input about site cleanup plans, and 3) facilitate the
resolution of community issues tied to a site. EPA accomplishes these goals by providing
communities different tools and resources to support their site involvement. These resources
include independent technical assistance so community members can understand the technical
aspects of a site, a public forum for community members to present and discuss their needs and
concerns related to the Superfund decision making process, and a job training program to
encourage employment of local workers. These are just some of the Cl program's resources; to
learn more, go to htt9:llw-Nw.epa.gov/superfund/community/.
To find out more about community involvement activities at this Superfund site and how you can
become involved in site cleanup/reuse decisions, view a list of contacts for this site >>.
Land Reuse
EPA places a high priority on land
revitalization as an integral part of its
Superfund response program mission, so EPA
tries to select cleanup options that encourage
and support future use of a site. Sites made
ready for use are deemed "Site-wide Ready
for Anticipated Use" (see glossary), which
means, in part, that all cleanup goals have
been achieved for both current and reasonably
anticipated future land use.
This site currently does not meet the criteria
http://cfpub.epa.gov/supercpad/cursites/csitinfo.cfm?id~0410161
Post-Co.nstruction
Post-Construction (see glossary) is the stage
following completion of the remedy
construction. It includes, among other things,
activities such as operating the remedy to
address the contamination (e.g., ground water
pump and treat); implementing, monitoring,
and enforcing institutional controls; and a
review of the implemented remedies at least
every five years to ensure they continue to
protect human health and the environment.
Institutional controls (see glossary) such as
6/10/20 I I
Superfund Information Systems:_ Site Progress Profile
for Site-wide Ready for Anticipated Use,
however parts of the site may be suitable for
reuse.
Page 4 of4
administrative or legal restrictions may also be
components of remedies at a site that remain
in place post-construction completion.
Sites or portions of sites may be deleted ~
glossary) from the National Priorities List when
all cleanup goals have been achieved.
This site has not been deleted from the
National Priorities List
111, back to top I view glossary >>
DISCLAIMER: Be advised that the data contained in these profiles are intended solely for informational
purposes use by employees of the U.S. Environmental Protection Agency for management of the
Superfund program. They are not intended for use in calculating Cost Recovery Statutes of Limitations
and cannot be relied upon to create any rights, substantive or procedural, enforceable by any party in
litigation with the United States. EPA reserves the right to change these data at any time without public
notice.
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URL: http://cfpub.epa.gov/supercpad/cursites/csitinfo.cfm?id=0410161
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http:/ /cfpub.epa.gov/supercpad/cursites/csitinfo.cfm?id=04 IO 161 6/10/2011
U.S. Em·ironmemal Protection Agency
Region 4: AL, FL, Gi\, KY, MS, NC, SC, TN
Office of External Affairs
Sam Nunn Atbnta Feder.ii Center
61 Forsyth St. SW
Aclama, GA 30303-3104
ENVIRONMENTAL NEWS
PHONE: [phone] Fi\X: (4114)5!,2-8.135
EPA announces Waterline Completion at GMH Electronics Site in Person County, NC
Contact Information: James Pinkney, (404) [e-mail]
(Atlanta-Dec. 1, 2010) Today, the U.S. Environmental Protection Agency (EPA) announced the completion
of a waterline construction project at the GMH Electronics site in Roxboro, NC.
The project will serve over 40 houses and provide clean drinking water to more than 60 people. To
recognize this milestone, EPA officials will be in attendance at the Person County Commissioners Meeting
at 304 South Morgan Street, Roxboro, NC on December 6, 2010 at 7:00 p.m.
The work was performed by Person County under a Superfund Political Subdivision Lead Remedial
Cooperative Agreement and funded by the American Recovery and Reinvestment Act (ARRA) of 2009. In
December, 2007 EPA's Emergency Response Program installed whole house carbon filtration systems
and began providing bottled water to households impacted by the site contaminants that exceeded EPA's
acceptable risk limits for human health. As a result of completing the connections, EPA filter systems have
been removed and bottled water service will be terminated this week. Minor construction activities, such as
grading, seeding, and repair of asphalt drives, will continue in December. Additionally, the Person County
Health Department will oversee the abandonment of private wells of the homes now connected to public
water.
GMH Electronics operated at the site from 1972 to 2004 producing electronics components. As part of its
parts washing operations, GMH Electronics used chlorinated solvents that were discharged into an on-site
septic system without proper treatment. Sample results show waste solvents from GMH Electronics'
operations have discharged into the groundwater and have become co-mingled with petroleum
hydrocarbons from two previously removed underground storage tanks located on the site property and
across the intersection. '
This project is one of more than 50 across the country to receive money under ARRA. EPA is using the
$600 million appropriated to the Superfund program to start long-term cleanup projects and to accelerate
ongoing construction projects at sites listed on the National Priorities List. Work performed with ARRA
funding helps clean up contaminated land and creates jobs.
For more information on:
• GMH Electronics Superfi.md site, go to:
http://www.epa.gov/region4/waste/npl/nplnc/gmhe1ectnc.htm
• Superfund and the American Recovery and Reinvestment Act, go to:
http://www.epa.gov/superfund/eparecovery/index.html;
• EPA and ARRA, go to: http://www.epa.gov/rccovcry; and
• ARRA across the United States, go to: http://www.recovery.gov.
##11-
Beverly Eaves Perdue
Governor
RA
l'!ICDENR
North Carolina Department of Environment and Natural Resources
Division of Waste Management
TO:
FROM:
Dexter R. Matthews
Director
August 4, 20 I 0
Nile Testerman
David Lilley 'l)~L
RE: Review of the Draft Health Consultation, GMH
Electronics NPL Site, Roxboro, Person County, NC
July 14, 2010
1. No comments.
Dee Freeman
Secretary
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] I FAX: [phone] I Internet: www.wastenotnc.org
OnehC 1· Nort aroma
An Equal Opportunity I Affirmative Action Employer /Vatura//!f
RA
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Beverly Eaves Perdue
Governor
Dexter R. Matthews
Director
30 March 2009
Ms. Corey Diehl-Miller
Superfund Branch, Waste Management Division
US EPA Region IV
61 Forsyth Street. SW
Atlanta, Georgia 30303
SUBJECT: Concurrence with Record of Decision
GMH Electronics
Roxboro, Person County
Dear Ms. Diehl-Miller:
Dee Freeman
Secretary
The State of North Carolina by and through its Department of Environment and Natural Resources,
Division of Waste Management (herein after referred to as "the state"), reviewed the Record of Decision (ROD)
received by the Division on 26 March 2009 for the GMHElectronics Site and concurs with the selected remedy,
subject to the following conditions:
1. State concurrence on the ROD for this site is based solely on _the information contained in the
ROD received by the State on 26 March 2009. Should the State receive new or additional
information which significantly affects the conclusions or amended remedy contained iii the
ROD, it may modify or withdraw this concurrence with written notice to EPA Region IV.
2. State concurrence on this ROD in no way binds the State to concur in future decisions or
commits the State to participate, financially or otherwise, in the clean up of the site. The State
reserves the right to review, overview comment, and make independent assessment of all future
work relating to this site:
3.. If, after remediation is complete, the total residual risk level exceeds 10·6, the State may require
deed recordation/restriction to document the presence of residual contamination and possibly
limit future use of the property as specified in NCGS 130A-3 l 0.8
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ FAX: [phone] \ Internet: www.wastenotnc.org
An Equal Opportunity I Affirmative Action Employer
Oneh 1. Nort Caro ma Naturally
The State of North Carolina appreciates the opportunity to co!Ilment on the ROD and looks forward to
working with EPA on the remedy for the subject site. If you have any questions or comments, please call Mr.
Nile Testerman at 919 508-8482.
cc: Jack-Butler, Chief NC Superfund Section
David Lown, NC Superfund
Nile Testerman, NC Superfund
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Dexter R. Matthews, Director
Division of Waste Management
Phone: [phone] I FAX: [phone] I Internet: www.wastenotnc.org
An Equal Opportunity\ Affinnativa Action Employer
One . NorthCarohna
/'vnturn//y
TO:
FROM:
March 4, 2009
Nile Testerman
David Lilley
RE: Comments on Appendix B, Focused Human Health
Risk Assessment contained in the Focused Remedial
Investigation Report, Drinking Water Contamination,
GMH Electronics Site, Roxboro, NC
1. Section 2.0, second paragraph: Correct second sentence.
2. Page 3, Selection of Contaminants of Potential Concern, third paragraph: In other
human health risk assessments, the RSL (1/10 RSL for noncarcinogens) is used as
the screening level in RAGS Part D tables 2.x. Since the goal of this report
appears to be to calculate risk to people using the water, it is recommended the
initial screen be the RSLs and not the MCLs.
3. Tables 2.1 and 2.2: Footnote 4 claims the RSL appears in the "Screeni_ng Toxicity
Value" column. This is not true for chemicals with a MCL. Only RLSs should
appear in this column.
4. Table 2.1: The MCL for methylene chloride (dichloromethane) is 5 ug/1. Please add
to the table.
5. Table 2.1: The MCL for chloroform (as total trihalomethanes) is 80 ug/1. Please add
to the table.
6. Table 2.1: The MCL for o-xylene (as total xylenes) is 10,000 ug/1. Please add to the
table.
7. Table 2.2: Isopropylbenzene (cumene) has an adjusted RSL of6.8 ug/1. Please add to
the table.
8. Table 2.2: Methylcyclohexane has an adjusted RSL of 63 ug/1. Please add lo the table.
9. Table 5.1: According to the latest RSL table, 1,2-dichloroethane does not have a
current oral RID. Please correct.
I 0. Table 6.1: According to the latest RSL table, chloroform has an oral SF of 3. I E-02
(mg/kg-d)"1• Please correct.
11. Table 5.1: Non-cancer toxicity data should be included for I, 1-dichloroethane. The
RSL table provides a value of2.0E-01 mg/kg-d.
12. Section 3 should be rewritten to fully describe the models and procedures used to
calculate dermal exposure so the process is transparent and reproducible.
13. Given the above issues, I cannot agree or disagree with the risk summary as
presented in Table 1, page 12 of 29.
&,f'A --.. ,;~~ NCDE_M_R
North Carolina Department of Environment and Natural Resources
Dexter Matthews, Director
Ms. Jennifer Wendel, RPM
US EPA Region IV Waste Division
Atlanta Federal Building
61 Forsyth St., I Ith Floor
Atlanta, GA 30303-3104
Division of Waste Management
January 27, 2009
Subject: HRS Documentation Package --Revised
GMH Electronics
EPAID#NCN000410161
Roxboro, Person County, NC
Dear Ms. Wendel:
Beverly Eaves Perdue, Governor
Dee Freeman, Secretary
This letter confirms the transmittal of the attached revised HRS Documentation Package
for the GMH Electronics site (NCN 000 410 161 ), Roxboro, Person County, NC. This transmittal
includes:
. Documentation Record -two copies
NPL Characteristics Data Collection Form --two copies
Reference Corrections and Additions -two copies
In response to the Quality Assurance (QA) letter from Leslie Meador, Computer Sciences
Corporation, dated December 8, 2009, to Angelo Carasea, US EPA, the following responses are
offered:
2.4.2.5 Chain-of-Custody Forms and Sample Collection Notes -No chain-of-custody
forms are available for sampling conducted by the Person County Health
Department.
3.1.3 Well Depths and Well Screened Intervals -Information concerning well depths
and well screening intervals is not available. An wells included in the HRS
Documentation Package are used for potable water supply. Wells are constructed
in the sapprolite/bedrock aquifer, an interconnected hydrogeologic unit.
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] I FAX: [phone] I Internet: www.wastenotnc.org
An Equal Opportunity I Affirmative Action Employer• 50 % Recycled\ 10 % Post Consumer Paper·
Nirth Carolina
)Vaturall!I
4.5 Reference List -Some references and reference pages have been updated/made
more legible. Three additional references have been added to supplement the HRS
Documentation Package. A list of changes and additions to the references are as
follows:
• Reference 1 has been updated as to more accurately reflect the source.
• Reference 5, pp. 81 & 82, to.delete blank pages in original reference.copy.
• References 13 and 16, pp. 1 & 2 of each, to make the entire title of references
visible.
• Reference 15, pp. 84/85, 94/95, 124/125, 128/129, 140-145, to make more
legible copies.
• References 23 and 32, to make more legible copies and correctly number all
pages.
• References 50, 51, and 52 w/cover pages are additions to the HRS
Documentation Package.
• Reference labels have been updated to reflect correct name of site. Please
place attached adhesive labels over current reference labels in your copies.
All other issues _discussed in the QA letter have been addressed in the revised HRS
Documentation Package. If you have any questions, please contact me at
[e-mail] or [phone].
~~tt
Melanie Bartlett
Environmental Engineer
Site Evaluation and Removal Branch
NC Superfund Section
Enclosures
cc: File
St~
Branch Head
Site Evaluation and Removal Branch
NC Superfund Section
&~-':~A -,~~ ---NCDENR
North Carolina Department of Environment and Natural Resources
Dexter R. Matthews, Director Division of Waste Management Michael F. Easley, Governor
William G. Ross Jr., Secretary
04 December 2008
Ms. Corey Diehl-Miller
Superfund Branch, Waste Management Division
US EPA Region IV
61 Forsyth Street. SW
Atlanta, Georgia 30303
SUBJECT: North Carolina Applicable or Relevant and Appropriate Requirements (ARARs)
GMH Electronics
Roxboro, Person County
Dear Ms. Diehl-Miller:
The State of North Carolina has reviewed the request from EPA to list the state Applicable
or Relevant and Appropriate Requirements (ARARs) specific to the GMH Electronics site located
in Roxboro, Person County. The following North Carolina ARARs are to be met at this site:
State Action-Specific ARARs:
Solid Waste (lSA NCAC Subchapter 138)
NC Solid Waste Management Act (NCGS 130A, Article 9)
Public Water Supply (lSA NCAC Subchapter 18C)
North Carolina Drinking Water Act (NCGS Chapter 130A, Article 10)
Groundwater (I SA NCAC Subchapter 2L)
Water Quality (15A NCAC Subchapter 28)
Hazardous Waste Management (I5A NCAC Subchapterl3A)
Erosion and Sedimentation (I SA NCAC Subchapter 4B)
Oil Pollution and Hazardous Substances Control Act (NCGS Chapter 143, Article 21A)
Sedimentation Pollution Control Act (NCGS Chapter I I 3A, Article 4)
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone [phone] \ FAX [phone] \ Internet http//wastenotnc.org
An Equal Opportunity/ Affirmative Action Employer-Printed on Dual Purpose Recycled Paper
cc:
State Location-Specific ARARs:
NC Hazardous Waste Management Rules (15A NCAC Subchapters 13A .0009 & .0012)
State Chemical-Specific ARARs:
Groundwater (15A Subchapter 21)
Water Quality (15A NCAC Subchapter 2B)
NC Drinking Water Act (NCGS 130A, Article 10)
If you have any questions or comments, please call me at 919 508-8482.
File/
Jack Butler
Sincerely,
'ft/4~
Nile Testerman, PE
Superfund Section
C:\Documents and Settings\ntesterman\My Documents\WP\MSWORD\GMH\ARARS 2008.doc
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 4
December I, 2008
Mr. Jack Butler
NCDENR Superfund Section
40 I Oberlin Rd, Suite 150
Raleigh, NC 27605
ATLANTA FEDERAL CENTER fmi-
61 FORSYTH sTREET D ;c~-
ATLANTA GEORGIA 30303-8960 ,c ' :;-;-;,-a, ' J-J
. EC 2 zo u
TIO.f\J _,_
SUBJECT: Request for Identification of the State of North Carolina Applicable or Relevant and
Appropriate Requirements that Pertain to the GMH Electronics Superfund Site, located
in Roxboro, Person County, North Carolina.
Dear Mr. Butler:
Under Section 121 (d)(2)(A)(ii) of the Comprehensive Environmental Response, Compensation,
and Liability Act (CERCLA), on-site remedial actions must meet (or waive) Applicable or Relevant
and Appropriate Requirements (ARARs). In particular, potential CERCLA State ARARs include any
standard, requirement, criteria, or limitation under a State environmental or facility siting law that is
properly promulgated, identified in a timely manner, and more stringent than a federal requirement.
You may wish to refer to the National Oil and Hazardous Substances Pollution Contingency Plan, 40
C.F.R. § 300.5, which contains more detailed definitions of "applicable" 'and "relevant and appropriate"
requirements.
This correspondence requests that the State of North Carolina identify all more stringent State
ARARs that may pertain to the GMH Electronics Superfund Site, located in Roxboro, Person County,
North Carolina. As discussed in 40 C.F.R. §§ 300.400(g), 300.430(e)(9), and 300.5 I 5(d) and (h),
ARARs should be identified by the lead and support agencies carrying out CERCLA deanups. In your
response, please include a specific citation for each provision identified as a potential ARAR so that
this information can be considered in the CERCLA remedy selection process and where appropriate,
incorporated into the forthcoming Record of Decision. Also, please provide a brief explanation of why
the cited requirement is considered by the State to be a potential ARAR; a more detailed explanation of
this process is contained in 55 Fed. Reg. 8746 ( 1990).
To· ensure that the response action selectio!1 process stays on schedule, please provide this ·
infonnation within three weeks of the date of this letter. Also, please update your. response as new or
additional State ARA Rs are identified during the CERCLA response action for this Site. If you have
any questions or need additional information about the scope of this request or the Site, please feel free
to contact me at 404-562-8738.
cc: Nile Testerman....--------
Sincerely,
~hJl-l11JJL
Corey Diehl-Uiler
Remedial Project Manager
Internet Address (URL) • http://WWW.epa.gov
Recycled/Recyclable• Printed with Vegetable 011 Based Inks on Recycled Paper (Minimum 30% Postconsumer}
Site Name GMH Electronics
SITE HEALTH AND SAFETY PLAN
A. General Information
Location 1800 Virgilina Road, Roxboro, NC
Proposed Date ·of Investigation 11/19/08 to 12/19/08
Date of Briefing 11/17/08
Date of Debriefing 1/5/09
Nature of Visit (cheCk one): On-Site Reconnaissance
·Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
ID# NCN 000 410 161
X
Health Department Official Contacted Harold Kelly via voice mail
Date of Contact 11/17/08
Site Investigation Team: All site personnel have read the Site Health and
Safety Plari and are familiar with its provisions.
Personnel
Team 1 Nile Testerman
Team 1 Melanie Bartlett
Plan Preparation:
Responsibilities
team leader, sampling
sampling
Prepared By: David Lilley, Industrial Hygiene Consultant
Signature
Reviewed By: Jack Butler, Superfund · Section Chief ·
B. ·sITE/WASTE CHARACTERISTICS
Waste Type(s) __ X_Liquid Solid Sludge Gas __ X_Vapor
Characteristics Corrosive __ X_Igz:iitable RadiOactive
X Volatile X Toxic Reactive Other
List Known or Suspected Hazards (physical, chemical biological or radioactive)
on Site and their toxicological effects. Also, if-known, list chemical amounts
EXPOSURE
HAZARD WARNING PROPERTIES
1,1-dichloroethzlene Odor Threshold (OT) -190
1,2-dichloroethane OT -6 -10 EEm
1,1,1-trichloroethane OT 44 m
trichloroethzlene OT -28 m
UNDERGROUND UTILITIES CHECKLIST
Utility
Power
Telephone
Gas
Water
Sewer
Call made bz:
Locator/Contact Person Phone#
2
EEm
LIMIT
1 EEm
1 EEm
350 EEm
10 EEm
Date of Location
',,,
ID# NCN 000 410 161
Facility Description·: Size unknown Buildings yes
Disposal Methods Being Investigated unknown
·Unusual Features on ~ite (dike integrity, power lines, terrain, etc.):
None known
History of the Site, The site is a groundwater plume.
C. HAZARD EVALUATION
The site can be toured and sampled in level D protection. PVC gloves
will be worn while collecting water samples. Chemically resistant knee length
boots will be worn on site.
Map or Sketch Attached? ~
Perimeter Identified? no
Command Post Identified? no
Zones of Contamination Identified? no
D. WORK PLAN INSTRUCTION
Personal Protective ·Equipment/Level of Protection: C ---X D
Modifications
3
Surveillance Equipment:
HNU
OVA
Explosimeter
Decontamination Procedures
ID# NCN 000 410 161
Detector Tubes and Pumps
02 Meter
Radiation Monitor
____ Level C Respi"rator wash, respirator removal, suit wash {if needed),
suit removal, boot wash, boot removal and glove removal.
-~X~_Level D Boot wash and rinse and bOot removal, sl.lit removal., glove
and goggle removal.
Modifications Dispose of trash properly, on-site if possible.
Work Schedule/Visit Objectives The purpose of this visit is to determine
if the site poses a threat to the public health or envirohment because of
releases of contaminants to soil, surface water, groundwater, or air.
Sampling may consist of groundwater sampling.
EMERGENCY PRECAUTIONS
Route of Exposure
E es
Skin
Inhalation
Ingestion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
X
X
ID# NCN 000 410 161
Location of Nearest Phone: nearby residences
Hospital (Address and Phone Number)
Person Memorial Hospital. 615 Ridge Rd, Roxboro, NC Tel: [phone]
Emergency Transportation Systems (Phone Numbers)
Fire 911
Ambulance 911
Rescue Squad 911
Emergency Route to Hospital see next page
PREVAILING WEATHER CONDITIONS AND FORECAST
EQUIPMENT CHECKLIST
Air purifying respirator
Cartridg~s for respirator
Eye Wash Unit
X
X
X
First Aid Kit
3 gal. Deionized H20
Rain suit
HNU
OVA
Explosimeter
Radiation Monitor
Decontamination
Materials
X
X
Gloves (PE/PVC/nitrile/cloth)
Boots/Boot Covers
__ x_ Coveralls (tyvek/saranex)
-~X-Eye Protection (goggles/shield)
X Hard Hat ---
STATE POISON CONTROL CENTER
1-800-848-6946
North Carolina OSHA
1-800-LABOR-NC
safeform.doc 5
Driving Directions from 1800 Virgilina Rd, Roxboro, NC to 615 Rid... http://www.mapquest.com/maps? I c=Roxboro& I s=NC& I a= 1800+ V ...
I of 2
MAPClUIEST.
Total Time: 4 minutes Total Distance: 2.59 miles
A: 1800 Virgilina Rd, Roxboro, NC 27574-8188
l~l
---------
1. Start out going WEST on NC-49NIRGILINA RD toward
. GRAVITTE RD. Continue to follow NC-49.
~ 2: Turn RIGHT onto CARVER DR.
---------~ 3: Turn LEFT onto RIDGE RD.
ffl 4: End at 615 Ridge Rd Roxboro, NC 27573-4629
B: 615 Ridge Rd, Roxboro, NC 27573-4629
Total Time: 4 minutes Total Distance: 2.59 miles
2-_\!( Call 1--800-FREE411 (1·800-373-3411) and get MapQuest Directions_ via text rrlessage. ~--·:-m--~ ,•l'.at)~f'lli:f1 1/fft}o/f,' ' '
All rights reserved. Use subject to License/Copyright Map Legend
Directions and maps are informational only. We make no warranties on the accuracy of their content, road conditions or .
2.0 mi
0.4 mi
0.1 mi
I 1/17/2008 10:36 AM
Chemical Name: 1,1-dichloroethylene
III. HAZARDOUS CHARACTERISTICS
A.
B.
Combustibility Yes X
Toxic by-products
Flammability LEL
C. Reactivity Hazard
No
D. Corrosivity Hazard
Neutralizing agent:
yes/no
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCE
UEL
pH:
Exposure Rate
1. The Merck Index, 11th Edition, 1989
Reference
1
2. Threshold Limit Values and Biological Exposure Indicies, ACGIH,
2007
3. 29 CFR 1910.1000
HAZARDOUS _SUBSTANCE INFORMATION .FORM
Chemical Name: 1,2-dichloroethane
I.· PHYSICAL/CHEMICAL PROPERTIES
Chemical Formula --.fi H4 Cl2 __________ ~
Natural· Physical State at 25°C -'l"'i"q"u=-i=-· d=-------
Vapor Pressure 62 mm Hg at 20°c
Melting Point -32 °F/°C Boiling Point --~l=-8=-3=---__ 0 =.F/°C
Flash Point (open or closed cup) ----=-5=-5 __ °C/°F
0.8% Solubility -H,O
Other alcohol, chlorform, ether
Reference
1
2
2
2
2
2
1
Physical Features: (odor, color, etc.) ·clear liquid with a sweet
odor like chlorofrom(2) lP-11.12 ev, HNU sensitivity-12.9 with 11.7 eV
robe.
II. TOXICOLOGICAL DATA REL
Standards: 10 ppm(3) TLV
1 ppm for 10 hour TWA (2)
suspect
1 ppm(4) PEL carcinogen IDLH -~2'-----
Routes of Exposure: Inhalation, Ingestio'n, Skin absorption, eye contact
Acute/Chronic Symptoms: Central nervous system depression, nausea, vomiting,
dermititis, eye irritation, corneal opacity, suspect carcinogen(2).
First Aid: Inhalat.ion: artificial respiration; Ingestion: get medical
attention immediately;· Eye contact: irrigate immediately; Skin contact:
soap and water wash immediately
Chemical Name: 1,2-dichloroethane
III. HAZARDOUS CHARACTERISTICS
A. Combustibility Yes X No
Toxic by-products
B. Flammability LEL 6.2%
Reference
1
UEL -~lc..6c..%c_ __ 2
C. Reactivity Hazard
chemically active
strong oxidizers and caustics, ~2~---
metals such as aluminum or magnesium powder,
sodium, potassium.
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
yes/no
pH:
1. The Merck Index, 11th Edition, 1989.
Exposure Rate
2. NIOSH Pocket Guide to Chemical Hazards, 1987.
3. Threshold Limit Values and Biological Exposure
Indices for,2007
4. 29 CFR 1910.1000.
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: 1,1,1 Trichloroethane (Methyl Chloroform)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C2 H3 C13
Natural Physical State at 25EC liquid
Vapor Pressure 100 mm Hg at 20EC
Melting Point -23EF/EC Boiling Point 165 EF/EC
.1
_l
2
2
Flash Point (open or closed cup) autoignitionEC/EF 3
Solubility - H2O 0.4% temperature= 500EC
Other Soluble in acetone, benzene, carbon
tetrachloride methanol ether
2
1
Physical Features: (odor, color, etc.) Colorless liquid
with a mild chloroform-like odor (2) IP= 11.5 eV
II. TOXICOLOGICAL DATA
Standards: 350 ppm (4) TLV 350 ppm (5) PEL 1000 ppm (2) IDLH
Routes of Exposure:
contact.
Inhalation, Ingestion, and skin and/or eye
Acute/Chronic Symptoms: Headaches, lassitude, central nervous
system depression, poor equilibrium, eye irritation, dermatitis,
cardiac arrhythmias (irregular heart beat) (2) ·
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irriqate
immediately; Skin contact: soap and water wash immediately.
Chemical Name:. 1,1,1 Trichlorethane
III. HAZARDOUS CHARACTERISTICS Reference
B.
A. Combustibility Yes _L No
Toxic by-products
Flammability LEL 8%
2
UEL 10.5% 3
C. Reactivity Hazard Incompatible with strong caustics, __ 2
strong oxidizers, chemically active metals, such as aluminum,
magnesium, powders, sodium, potassium.
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive· Hazard
Background
Alpha particles
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
yes/no
yes/no
yes/no
pH:
Exposure Rate
1. The Merck Index, 11th Edition, 1989
2. Pocket Guide to Chemical Hazards, NIOSH, 1990
3. Chemical and Engineering News, December 12, 1988.
4. Threshold Limit Values and Biological Exposure Indice~
for 2003 ACGIH
5. CFR 1910.1000
HAZARDOUS SUB.STANCE INFORMATION FORM
Chemical Name: Trichloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C2 HC13 ~~~=--------------
Natural Physical State at 25EC liquid
Vapor Pressure 58 mm Hg at 20EC
Melting Point --~9~9 __ .~E~F/EC Boiling Point
Flash Point (open
Solubility - H
2 0
or closed cup) 32EC/EF
0.1% at 77EF
__ 1_8~9-~E_F /EC
Other Ether, alcohoi, chloroform
1
1
2
_l
2
Physical Features: (odor, color, etc.) Colorless liquid
(unless dyed) with a sweet odor like chloroform lP = 9.45 eV (2)
· OVA Relative Response= 70%
II. TOXICOLOGICAL DATA
Standards: 10 ppm (4) TLV
potential
human
50 ppm (5) PEL carcinogen(2) IDLH
Routes of Exposure:
contact (2)
Inhalation, ingestion, skin and/or eye
Acute/Chronic Symptoms: Acute: Headache, vertigo, visual.
disturbance, tremors,drowsiness, nausea, vomiting, eye
irritation, dermititis, irregular heartbeat,skin irritation;
chronic: carcinogenic (2)
First Aid.: Inhalation: artificial respiration; Ingestion: get
medical attention immediatelv: Eve contact: irrigate
immediately; Skin coritact: soap and water wash immediately
Chemical Name: Trichloreothylene
III. HAZARDOUS CHARACTERISTICS
A. Combustibility Yes X No
Toxic by-products
B. Flammability LEL 12.5%
Reference
UEL 90%
C. Reactivity Hazard Incompatible with strong caustics:
when acidic reacts with aluminum, chemically active metals,
barium, lithium, sodium, magnesium, titanium.
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES .
yes/no pH:
Exposure Rate
(1) The Merck Index, lith Edition, 1989
(2) Pocket Guide to Chemical Hazards, NIOSH, 1990
(3) Chemical and Engineering News, December 12, 1988.
(4) Threshold Limit Values and Biological Exposure
Indices for 2007 ACGIH
(5) 29 CFR 1910 .1000
_2
__ 3
2
Exhibit 4
'·
Section No, 4.0
Revision No. 7
Date: 8-11-00
·Page 2 of 2
.·. . . KEY RJSK M.A.NAGEM:ENT SERVJCES, !NC. comucare · ATT:--i: STAIT UNTT
P0.30X49l29 ·
GREENSBORO, NC 274 l 9 NETWORK,INC.
\VORKERS' COMPENSATION T\-1EDICA.L A UTHORlZATION
:--;-arne of Employee/Patient: Last First
Dare oflniur,: I Social Securirv Number:
Name ofEmployer/Company: STATE OF NORTH CAROLINA
Employer Authorization: Doctor To Be Seen:
'TJDlover:
::1nlovt.::
~,-s I c I an:
____________ .. --Com pk re-this form,-and-give -h-ro-the-injured-employee·before·a·doc10r·is-seenc-· ·-·---
Sho\v this for:n to tht doctor.
When a reie:.al is necessary• use-CompCare Physicians and call I_ 0 800-366-15 I I, to !er the state 2.g~ncy claims repres:ntarive k.no\v rhat the patient is being ref::red.
-,ENTI BILL DIRECTLY TO KEY RISK MANAGEMINT SERVICES, INC.
I I
&~-.*?'A -;~~ ---NCDENR
North Carolina Department of Environment and Natural Resources
Michael F. Easley, Governor
Mr. J. I. Palmer
Regional Administrator
U.S. Environmental Protection Agency
61 Forsyth Street, SW
Atlanta, GA 30303-3104
November 5, 2008
SUBJECT: NPL Listing; GMH Electronics
Roxboro, Person County, NC
NCN 000 410 161
Dear Mr. Palmer,
William G. Ross Jr., Secretary
I am writing in response to.your request for the state of North Carolina's position
• regarding the proposed listing of the GMH Electronics site (NCN 000 410 161) on the National
Priorities List (NPL).
The state of North Carolina agrees that the site poses a significant threat to the public
health. Therefore, we support the Environmental Protection Agency's efforts to propose this site
for inclusion on the NPL:
North Carolina appreciates the EPA's continued assistance to protect the state's public .
health and the environment.
· · cc: . Dexter Matthews, NC DWM
Jack Butler, NC DWM
James Bateson, NC DWM
Franklin Hill, US EPA Region 4
Jennifer Wendel, US EPA Region 4
1601 Mail Service Center, Raleigh, North Carolina 27699-1601
Phone: [phone] I FAX: [phone] I Internet: www.enr.state.nc.us/ENR/
An Equal.Opportunity I Affirmative Action Emp!?yer-50 % Recycled I 10 % Post Consumer Paper
f
WILLIAMS MULLEN
Direct Dial: 919.981.4312
[e-mail]
Admitted in Florida, Virginia and Washington, DC
BY FIRST CLASS MAIL
Mark Powers
Regional Supervisor
Underground Storage Tank Section
August 27, 2008
North Carolina Department of Environment and Natural Resources
1628 Mail Service Center
Raleigh, NC-27699
Re: Notice of Violation -Incident No. 3684
Dear Mr. Powers:
-----· Not adinim:d in North Carolina
Supervised by Members of the NC Bar
\DJ.~cc~~~~~
I~ OCT 172008 ~
SUPERFUND SECTION
Please find enclosed a report prepared by Mid-Atlantic Associates, Inc.· ("Mid-Atlantic")
regarding the GMH Electronics Site located at the corner of State Road 1521 and Highway 49 in
Roxboro, North Carolina (the "Site"). As you know, this firm continues to represent Mr. Marvin
J. Eanes ("Mr. Eanes"), as executor to the estate of Mr. Marvin Eanes, regarding environmental
issues.
You will see in the report that Mid-Atlantic was able to sample four of the thirteen
groundwater wells in the vicinity. The remaining wells could not be sampled due to the presence
of free-product, because there was insufficient water in the wells, or because the wells could not
be located.
I would like to schedule a time to discuss the status of this matter with you. Please
contact me at your convenience at [phone].
Sincerely,
/Oll!d~
Sean M. Sullivan
A Professional Corporation
NORTH CAROLINA • VIRGINIA • WASHINGTON, D.C. • LONDON
3200 BeechleafCourt, Suite 500 (27604) P.O. Box 19764 Raleigh, NC 27619-9764 Tel: [phone] Fax: [phone]
www.williamsmullen.com
August 27, 2008
Page 2
cc: Marvin J. Eanes
Amos C. Dawson, III, Esq.
George Jackson, Esq.
i
M!1?;tl¼{\liT!~ ·, ' AUG 2 8 ?nmi -'-• ·t
August 19, 2008
Enxineering & En\'ir,n1111,~11tal Solution.\
409 Rogers new Court I Raleigh I North Carolina 117610
80().486-7568 /9/9-15().99/819/9-15().9950 Facsimile
www.MAAonline.com
Mr. Marvin J. Eanes, Executor
The Estate of Marvin Eanes
435 Old Durham Road
Roxboro, North Carolina 27573
Reference: LETTER REPORT OF ENVIRONMENTAL SERVICES
FORMER GMH ELECTRONICS SITE
ROXBORO, NORTH CAROLINA
INCIDENT NO. 3684
MID-ATLANTIC JOB NO. 000R2001.00
Dear Mr. Eanes:
·-· . n: r,·r,· .· ._ .. t.:
In accordance with Mid-Atlantic Proposal No. P07R-4542R, dated June 10, 2008 and authorized by you on July 11, 2008, Mid-Atlantic Associates, Inc. (Mid-Atlantic) hereby submits this Letter Report of Environmental Services associated with the above referenced property ' (Drawing 1 ). The proposed work entailed the following four discrete tasks:
North Carolina Department of Environment and Natural Resources File Review
Mid-Atlantic conducted the file review on July 22 and 23, 2008 at the Raleigh Regional Office of North Carolina Department of Environment and Natural Resources (NCDENR). The key technical elements gleaned from the file review are summarized below. This summary does not include a discussion of regulatory correspondence.
► The earliest documentation of a release is a completed Pollution Incident Reporting
Form, dated December 3, 1987. This document cites a complaint by Mrs. Archie Wrenn of gasoline contamination in her well.
► Assessment activities were conducted by Richard Catlin and Associates, Inc, (Catlin) starting in approximately 1988. By 1990, the results of the assessment work suggested
that the underground storage tanks formerly located at the Archie Wrenn store may have contributed to the contamination discovered in the vicinity of the former GMH
Electronics site.
f
Letter Report of Environmental Services
GMH Electronics
Roxboro, North Carolina
August 19, 2008
Page 2
► Catlin issued a Groundwater Assessment Report dated April 19, 1991 followed by a
-E:orrective Action Plan dated October 25;-1991-:--A-Corrective-Action-Plan Addendum
was developed for the site by Clark Environmental Services, Inc. and dated July 7,
1995. These appear to be the only substantial reports in the file. Based on current site
conditions, it does not appear that additional assessment activities have occurred since
those reported in the documents above. The corrective action measures described in
the above documents do not appear to have been implemented.
► Starting in September 2007, several water supply wells in the vicinity of the GMH
Electronics site were sampled by both NCDENR and the Person County Health
Department. These tests indicate that several water-supply wells are impacted by
compounds typically associated with petroleum.
► In December 2007, TN & Associates, Inc, working for EPA under the Superfund
Technical Assessment and Response Team program, sampled approximately 37
water-supply wells in the vicinity of the GHM Electronics facility. Petroleum compounds
and chlorinated solvents were detected in several of the samples collected from these
wells.
Groundwater Sample Collection and Testing
On July 24, 2008 Mid-Atlantic visited the subject site to sample the 13 monitoring wells
associated with the subject site identified in the July 7, 1995 Clark Environmental Services
report. Mid-Atlantic was successful in sampling only four of the targeted wells. The following
conditions prohibited sampling of the other nine wells:
Monitoring Well Identification
B-1, B-5, B-8
B-2, B-7
B-9, B-11
B-10, B-12
Condition
Wells contained free product
Wells could not be located
Wells used for air monitoring, dry
Wells contained insufficient water to sample
The free product thicknesses recorded in B-1, B-5 and B-8 were 0.28 feet, 0.11 feet and 0.02
feet, respectively.
Groundwater samples were collected from monitoring wells B-3, B-4, B-6 and B-13. The.
samples were tested by SGS Laboratories of Wilmington, North Carolina. A tabular summary
of the detected compounds is provided as attached Table 1. These data are also shown on the
attached Drawing 2.
MP?;~J:¼\~T!~
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,·
Letter Report of Environmental Services
GMH Electronics
Roxboro, North Carolina
August 19, 2008
Page 3
Relative Wellhead Elevation and Groundwater Flow Direction Estimation
During the July 24, 2008 site visit, Mid-Atlantic also recorded the elevations of the top of well
casings with respect to an assumed benchmark (base of power pole in northeast corner of
subject site) of 100 feet. The elevations of the well casings are summarized and provided as
attached Table 2.
These data and the depth to water data were used to estimate the water table elevation at the
subject site. An interpretation of water table elevation is provided in attached Drawing 3. The
water table depicted in Drawing 3 suggests a significant northerly component to groundwater
flow due to the relatively low groundwater elevation at monitoring well B-13: Groundwater
contour maps previously developed by Catlin depict primarily eastern groundwater flow. These
earlier maps did not include data from monitoring well B-13.
Sensitive Receptor Survey Update
During site visits on July 21 and 24, Mid-Atlantic conducted an update of potential sensitive
receptors in the vicinity of the· subject site. The essential receptors for this incident are
domestic water-supply wells. Several nearby domestic water-supply wells are known to be
contaminated based on work previously conducted at the subject site. Our review of current
conditions confirms that domestic water-supply wells are still the exclusive source of drinking
water for the area. Municipal water supply is present approximately 1.5 miles west from the
subject site along North Carolina Highway 49.
Mr. Eanes we appreciate the opportunity to submit this Letter Report to you. If you have any
questions, please feel free to contact us at 919-250-9918.
Sincerely,
MID-ATLANTIC ASSOCIATES, INC.
Daniel H. Nielsen, PE
Principal Engineer
Attachments:
Drawings
Tables
Laboratory Report
cc: Mr. Sean Sullivan, Williams Mullen
7t--A U-------
Thomas A. Proctor, LG
Principal Environmental Geologist
000R2001.00 Revised Former GMH Electronics Letter Report of Sampling/DHN/jnc
M!9s-tc11t\~T!~
f.'111i11rrrin, ,l f111•;,.,,,,.,,,,1J/ So/111i!>nl
r
DRAWINGS
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:\===========================================--=;i
i
1. ,,
lj
ii I :i
I
j
N
REFERENCES:
1. ROXBORO, NC DIGITAL RASTER GRAPHIC, USGS. SCANNED FROM 1:2-4,000-SCALE ROXBORO, NC TOPOGRAPHIC UAP, PUBLISHED 1082, uses. 2. INSET MAP DIGITAL DATA FROM BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, O.C .. 0
M~9:~ ~,~T~TJ~ £,,,:,,,.,,.,,,,f c. 1,..,.,,~.,~,,n1nl :;,,J,,!""'"
TOPOGRAPHIC SITE MAP
GMH ELECTRONICS
N.C. HIGHWAY 49 AT
HALIFAX ROAD
ROXBORO, NORTH CAROLINA
SCALE: 1:24,000
1,000 2,000
DRAWN L,,,4-
BY: r:.,J7
DRAFT -"7, (' CHECK: /-'1
ENG. .-<..A.. CHECK: qv•
Feet
4,000
DATE:
JULY 2008
JOB NO:
OOOR2001.00
GI N :
01G-R2001.~1
APPROVAL: ~ DWG NO: 1
M~~;!li¼~~~.Tl~f
Enginecni1g & EnvironmcnflJ/ Solutions
8TEX, MTBE AND LEAD
IN GROUNDWATER
FORMER GMH ELECTRONICS
HIGHWA.Y 49 AND
HALIFAX ROAD
ROXBORO, NORTH CAROLINA
DRAWN BY,
IL -
C . "
DATE: AUGUST 2008
~~rTING CHECK ·7111 JOB NO: 000R2001.00
ENGINEER CHEC~1 CAD # 01-200-103 BY: ,/4 r
owe ND: 2
REFERENCE, ClARK ENVIRONMENTAL ScRVICES, INC. DRAWING NOT DATED; MID-ATlANTIC FIELD NOTES.
T
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i
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g
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8. r i i ~ iH !~ fH~~ij ~ur ~i•!i~ ~ ~ i 1 i1i
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i t t s
Ii
I 0 •
0
MID-ATLANTIC
ASSOC I ATES, INC.
Engineering & Env_ironmenta/ Solutions
0
~:
WATER TABLE CONTOUR MAP
FORMER GMH ELECTRONICS
HIGHWAY 49 AND
HALIFAX ROAD
ROXBORO, NORTH CAROLINA
DRAWN
BY:
DRAFTING CHECK BY:
ENGINEER CH BY,
APPROVED BY, I REFERENCE: CLARK ENVIRONMENTAL SERVICES, INC. DRAWING NOT DATED; MIO-ATLANTIC FIELD NOTES.
~-
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~
DATE: AUGUST 2008
JOB NO: OOOR2001.00
CAO# 01-200102
DWG NO: .3
' I
I
TABLES
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,• .•.. •. .., ., ~ ,~ii.'""";,/;l;l,J;;''./f"l, ~~ii( '.: 1.,:;, •. ;~--~~\: ... ~ ,::.U..:!"f,--..., ,...j-,,;:._:~ ., ·,, -'• 1i·~,t~;..r.:,:·? ·-:•'<11.t;.:coMPOUNDS' "'1 :~•l·V,l -~ ,~ ..... ,., '.C:· .;·1.•'-•,/4-.;.;,'_1-:'_ ---., --·• .. ,,. ;-~· -~"-ttt 1.. _"-:,i;5, .. ~;•l&t{iS,~1i1.!@~:1tr;~:Y.f~~J;~~-~~ t~
Volatile Organic Compounds
Benzene ·-
Toluene
Ethylbenzene
n otal Xylenes
natal BTEX
lsopropylbenzene
Naphthalene
n-Propylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Diisopropyl ether (DIPE)
MTBE
n-Butylbenzene
1, 1-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloroethane
1, 1, 1-Trichloroethane
MADEPVPH
CS-CB Aliphatics
C9-C12 Allphatlcs
C9-C 10 Aromatics
Metals
Lead
NOTES:
ug/L -micrograms per liter
BQL -Below Quanitification Limits
Bold Values exceed NCGQS
Shaded values exceed GCL
• -Method Detection Level'above NCGQS
NA -Not Applicable
GW Monitoring Report Tables.xis Table 1
.1A','i;:,.'l.'1l.,~'./i';t.;'~~l!~t·CONCENTRATIONT/uii/L:)~:;'if,:~/ij/~",~.1.lr,ii~i.$1/.~~
y,r;1r::( . ..,7.~., ,.,....~ "':• ,-,;-:-; -·~-~~~ ... _,,; .. ~ ~ r:•:'-,, ... ;,.~ i _;~!i'~---~--~•t;. ~"' •• , ~~ ..... , ..... -: "'_: •• w,l_,, .. ~,½i:1-iulj
~Bij~~ ~B':4t~i;:i; ~~;;6il,i,.;\ ~J!3~~ \~CGC;l~l\; ~GCl{1jf , ~,~ 1~ --" ~.._ .;;-t~_. ....... ~J ·f. _,J.~ ~ .. ..,S •. •.,'--... . .f.£ . .,_. \,,;i:.,.,~,.-40,:,,_';w, .. t"..--::1'1:-_,._.,:.
15.2 6,490 0.100 315 1 5,000
29.6 15,700 1.37 1.10 1,000 257,500
92.8 2,040 0.630 BOL 550 84,500
359 13,110 3.42 14.4 530 87,500
496.6 37,340 5.50 330.5 NA NA
14.8 128 BQL 4.00 70 7,000
133 1,020 BOL 13.0 21 15,500
40.4 368 0.240 BQL 70 30,000
604 3,300 1.66 11.3 350 28,500
276 888 0.470 BQL 350 25,000
BQL 120 0.410 48.3 70 70,000
BQL 904 4.69 BQL 200 20,000
BQL BQL 0.290 BQL 70 6,900
BOL BOL 37.7 BOL 70 70,000
BOL BQL 8.51 BQL 7 7,000
BQL BQL 0.540 56.3 0.38 380
BQL BQL 0.350 BQL 200 200,000
325 43,300 BQL 804 420 NL
894 28,300 BQL BQL 4,200 NL
3370 13,400 BQL BQL 4,200 NL
14.7 83.1 12.2 I 35.3 15 15,000
Page 1 of 1
B-1 07/24/08 99.32 24.78 0.28
B-3 07/24/08 99.13 0.00
B-4 07/24/08 98.85. 0.00
B-5 07/24/08 99.29 24.70 0.11
B-6 07/24/08 101.81 0.00
B-8 07/24/08 95.1 20.32 0.02
B-10 07/24/08 98.7.7----0.00
B-12 07/24/08 100.18 0.00
B-13 07/24/08 99.12 0.00
'Static water level corrected using free product density of 5.6 lb/gal.
TOC = Top of Casing
DTP = Depth to Product
FP = Free Product
DTW = Depth to Water
SWLE = Static Water Level Elevation
ft= Feet
GW Monitoring Report Tables.xis/Table 2
25.06
23.94 75.19
24.80 74.05
24.81 74.55'
26.59 75.22
20.34 74.77'
Mud
24.66 75.52
22.61 72.51
Page 1 of 1
LABORATORY REPORT
MP?.;ti\1M\MT!~
f11,1i111:rrin~ ,I £11,iro11,.nuc1/ Su/111;,,,,,
SGS fdJ(i r) 4 2008
Chuck Hoffman
Mid-Atlantic Associates
409 Rogers View Court
Raleigh, NC 27610 .
Rerort Number: G 122-32 I 3
Client Project: EMI-I Electronics
Dear Chuck Hoffman,
Enclosed arc the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our tiles for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there arc any questions about the report or the services performed during this project,
please call SGS Environmental Services at [phone]. We will be happy to answer
any questions or concerns which you may have.
Thank you for using SGS Environmental Services for your analytical services, We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
SGS Environnlcntal Services, Inc.
5500 Business Or., Wilmington, NC 28405 t [phone] I !910) 350-1557 www.us sg~f°ef--34.--
Member ll! the SGS Group
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Ouantitation Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
POL= Practical Quantitation Limit
RL/CL = Reporting Limit/ Control Limit
RPO = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm; parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30_ percent.
Mt34.021208.4
2 of 34
Results for Volatiles
by GCMS 6210D
Client Sample ID: B-3 Analyzed By: RSB
Client Project ID: EMH Electronics Date Collected: 7/2412008 13:00
Lab Sample ID: G122-3213-1A Date Received: 712612008
Lab Project ID: 8122-3213 Matrix: Water
Sample Amount: 5 ml
Result. Quantitation MDL Dilution Date
Compound UG/L Limit UG/L UG/L Factor Analyzed Flag
Benzene 15.2 20.0 2.60 40 7/30/2008 j
Bromobenzene BOL 20.0 2.24 40 7/30/2008
Bromochloromethane BOL 20.0 4.04 40 7/30/2008
Bromodichloromethane BOL 20.0 3.04 40 7/30/2008
Bromoform SOL 20.0 4.80 40 7/3012008
Bromomethane SOL 20.0 5.32 40 7/30/2008
n-Butylbenzene SOL 20.0 4.36 40 7130/2008
sec-Butyl benzene SOL 20.0 3.36 40 7130/2008
tert-Butylbenzene SOL 20.0 2.00 40 7130/2008
Carbon tetrachloride BOL 20.0 3.48 40 7/30/2008
Chlorobenzene BOL 20.0 3.28 40 7/30/2008
Chloroethane SOL 20.0 4.24 40 7/30/2008
Chloroform BOL 20.0 3.16' 40 7/30/2008
C hloromethane BOL 20.0 5.84 40 7/30/2008
2-Chlorotoluene BOL 20.0 3.96 40 7/30/2008
4-Chlorotoluene BOL 20.0 3.20 40 7130/2008,
Dibromochloromethane BOL 20.0 3.60 40 7130/2008
1,2-Dibromo-3-chloropropane SOL 200 48.4 40 7/30/2008
Dibromomethane SOL 20.0 4.52 40 713012008
1,2-Dibromoethane (EDB) SOL 20.0 4.96 40 7130/2008
1,2-Dichlorobenzene BOL 20.0 5.08 40 7/30/2008
1,3-Dichlorobenzene SOL 20.0 3.24 40 7/30/2008
1,4-Dichlorobenzene BOL 20.0 3.16 40 7130/2008
1, 1-Dichloroethane BOL 20.0 2.96 40 7130/2008
1, 1-Dichloroethene BOL 20.0 3.56 40 7/30/2008
1,2-Dichloroethane BOL 20.0 3.16 40 7/30/2008
cis-1,2-Dichloroethene BOL 20.0 2.60 40 7130/2008
trans-1,2-dichloroethene BOL 20.0 3.56 40 7/30/2008
1,2-Dichloropropane SOL 20.0 3.76 40 7/30/2008
1,3-Dichloropropane BOL 20.0 5.08 40 7130/2008
2,2-Dichloropropane BOL 20.0 2.36 40 7/30/2008
1, 1-Dichloropropene BOL 20.0 2.88 40 7130/2008
Dichlorodifluoromethane BOL 200 3.76 40 7130/2008
Diisopropyl ether (DIPE) BOL 20.0 2.92 40 7130/2008
Ethyl benzene 92.8 20.0 3 08 40 7130/2008
Hexachlorobutadiene BOL 20.0 9.12 40 7130/2008
lsopropylbenzene 14.8 20.0 2.84 40 7/30/2008 j
4-lsopropyltoluene SOL 20.0 1.92 40 7/30/2008
Methylene chloride BOL 200 3.92 40 7/30/2008
Methyl-tert-butyl ether (MTBE) BOL 20.0 2.68 40 7/30/2008
Naphthalene 133 20.0 5.32 40 7130/2008
n-Propyl benzene 40.4 20.0 3.20 40 7130/2008
Styrene BOL 20.0 3.40 40 7/30/2008
1, 1, 1,2-Tetrachloroethane BOL 20.0 3.60 40 7/30/2008
1, 1,2,2-Tetrachloroethane BOL 20.0 4.60 40 7/30/2008
Page 1 of 2 GCMS.xl&
6'10D 3 Qf 34
c,,eoSGSr
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-1A
Lab Project ID: G122-3213
Compound
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1.1,2-Trichloroethane
Trichlorofluoromelhane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
1,2-Dichloroelhane-d4
Toluene-dB
4-Bromofluorobenzene
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Analyst: ~'b
Results for Volatiles
by GCMS 62100
·-------
Result Quantitation MDL
UG/L Limit UG/L UG/L
BQL 20.0 2.76
29.6 20.0 3.04
BQL 20.0 7.60
BQL 20.0 4.76
BQL 20.0 2.16
BQL 20.0 2.16
BQL 20.0 7.28
BQL 20.0 4.44
BQL 20.0 4.80
604 20.0 2.60
276 20.0 2.96
BQL 20.0 5.96
220 40.0 3.92
139 20.0 2.60
Spike Spike
Added Result
10 10.8
10 10.1
10 9.94
Page 2 of 2
Analyzed By: RSB
Date Collected: 7/24/2008 13:00
Date Received: 7/26/2008
. Matrix: Water.
Sample Amount: 5 ml
Dilution· Date
Factor Analyzed Flag
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
40 7/30/2008
Percent
Recovered
108
101
99
Reviewed By:~
GCMS.~/1
62100 4 of 34
c,.,S,e. Results for Volatiles
by GCMS 6210D
Analyzed By: RSB
Client Project ID: EMH Electronics Date Collected: 7 /2412008 13:50
Lab Sample ID: G122-3213-3A Date Received: 7/2612008
Lab Project ID: G122-3213 --. Matrix: Water·-
Sample Amount: 5 ml
Result Quantitation MDL Dilution Date
Compound UG/L Limit UG/L UG/L Factor Analyzed Flag
Benzene · 6490 400 52.0 800 7/30/2008
Bromobenzene BQL 400 44.8 800 7130/2008
Bromochloromethane BQL 400 80.8 800 7/30/2008
Bromodichloromethane BQL 400 60.8 800 7130/2008 .... -·•·· Bromororm BQL 400 96.0 800 7130/2008
Bromomethane BQL 400 106 800 7130/2008
n-Butylbenzene BQL 400 87.2 800 7130/2008
sec-Butylbenzene BQL 400 67.2 800 7130/2008
tert-Butylbenzene BQL 400 40.0 800 7/30/2008
Carbon tetrachloride BQL 400 69.6 800 7130/2008
Chlorobenzene BQL 400 65.6 800 7130/2008
Chloroethane BQL 400 84.8 800 7/3012008
Chloroform BQL 400 63.2 800 7130/2008
Chloromethane BQL 400 117 800 7130/2008
2-Chlorotoluene BQL 400 79.2 800 7130/2008
4-Chlorotoluene BQL 400 64.0 800 7130/2008
Dibromochloromethane BQL 400 72.0 800 7130/2008
1,2-Dibromo-3-chloropropane BQL 4000 968 800 7/30/2008
Dibromomethane BQL 400 90.4 800 7/30/2008
1,2-Dibromoethane (EDB) BQL 400 99.2 800 7/30/2008
1 ,2-Dichlorobenzene BQL 400 102 800 7/30/2008
1 ,3-Dichlorobenzene BQL 400 64.8 800 7130/2008
1 ,4-Dichlorobenzene BQL 400 63.2 800 7130/2008
1, 1-Dichloroethane BQL 400 59.2 800 7/3012008
1 .1-Dichloroethene BQL 400 71.2 800 7/30/2008
1 ,2-Dichloroethane BQL 400 63.2 800 7/30/2008
cis-1,2-Dichloroethene BQL 400 52.0 800 7/30/2008
trans-1,2-dichloroethene BQL 400 71.2 800 7/30/2008
1 ,2-Dichloropropane BQL 400 75.2 800 7130/2008
1 ,3-Dichloropropane BQL 400 102 800 7/30/2008
2 ,2-Dichloropropane BQL 400 47.2 800 7/30/2008
1 , 1-Dichloropropene BQL 400 57.6 800 7/30/2008
Dichlorodifluoromethane BQL 4000 75.2 800 7/30/2008
Diisopropyl ether (DIPE) 120 400 58.4 800 7/30/2008 J
Ethylbenzene 2040 400 61.6 800 7/30/2008
Hexachlorobutadiene BQL 400 182 800 7/30/2008
lsopropylbenzene 128 400 56.8 800 7130/2008 J
4-lsopropyltoluene BQL 400 38.4 800 7130/2008
Methylene chloride BQL 4000 78.4 800 7/3012008
Methyl-tert-butyl ether (MTBE) 904 400 53.6 800 7130/2008
Naphthalene 1020 400 106 800 7/30/2008
n-Propyl benzene 368 400 64.0 800 7/3012008 J
Styrene BQL 400 68.0 800 7130/2008
1, 1, 1,2-Tetrachloroethane BQL 400 72.0 800 7/30/2008
1, 1,2,2-Tetrachloroethane BQL 400 92.0 800 713012008
Page 1 of 2 GCMS.•ls
62100 f 3 7o 4
Client Sample ID: B-4
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-3A
Lab Project ID: G 122-3213
Compound
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1 ,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
1,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Analyst: ____ _
Results for Volatiles
by GCMS 621 OD
Result Quantitation MDL
UG/L Limit UG/L UG/L
BQL 400 55.2
15700 400 60.8
BQL 400 152
BQL 400 95.2
BQL 400 43.2
BQL 400 · 43.2
BQL 400 146
BQL 400 88.8
BOL 400 96,0
3300 400 52.0
888 400 59.2
BQL 400 119
8840 800 78.4
4270 400 52.0
Spike Spike
Added Result
10 10.7
10 10.1
10 10.1
Page 2 of 2
Analyzed By: RSB
Date Collected: 7/24/2008 13:50
Date Received: 7/26/2008
Matrix: Water
Sample Amount: 5 ml
Dilution Date
Factor Analyzed Flag
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
800 7/30/2008
Percent
Recovered
107
101
101 --·------
Reviewed By:~
GCM5.Xl5
"
100 8 of 34
c,,,oSfiS Results for Volatiles
by GCMS 6210D
Analyzed By: RSB
Client Project ID: EMH Electronics Date Collected: 7/24/2008 13:20
Lab Sample ID: G122-3213-2A Date Received: 7/26/2008
Lab Project-ID' G122-3213 · Matrix: -Water
Sample Amount: 5 ml
Result Quantitation MDL Dilution Date
Compound UG/L Limit UG/L UG/L Factor Analyzed Flag
Benzene 0.100 0.500 0.0650 1 7/30/2008 J
Bromobenzene BQL 0.500 0.0560 7/30/2008
Bromochloromethane BOL 0.500 0.101 7/30/2008
Bromodichloromethane BQL 0.500 0.0760 7/30/2008
Bromoform BQL 0.500 0.120 7/30/2008
Bromomethane BOL 0.500 0.133 7/30/2008
n-Butylbenzene 0.290 0.500 0.109 7/30/2008 J
sec-Butylbenzene BQL 0.500 0.0840 1 7/30/2008
tert-Butylbenzene BQL 0.500 0.0500 1 7/30/2008
Carbon tetrachloride BOL 0.500 0.0870 1 7/30/2008
Chlorobenzene BOL 0.500 0.0820 1 7/30/2008
Chloroethane BOL 0.500 0.106 7/30/2008
Chloroform BQL 0.500 0.0790 1 7/30/2008
Chloromethane BQL 0.500 0.146 7/30/2008
2-Chlorotoluene BOL 0.500 0.0990 7/30/2008
4-Chlorotoluene BOL 0.500 0.0800 7/30/2008
Dibromochloromethane BOL 0.500 0.0900 7/30/2008
1,2-Dibromo-3-chloropropane BOL 5.00 1.21 1 7/30/2008
Dibromomethane · BOL 0.500 0.113 1 7/30/2008
1 ,2-Dibromoethane (EDB) BOL 0.500 0.124 1 7/30/2008
1 ,2-Dichlorobenzene SOL 0.500 0.127 7/30/2008
1,3-Dichlorobenzene BOL 0.500 0.0810 1 7/30/2008
1,4-Dichlorobenzene BOL 0.500 0.0790 1 7/30/2008
1, 1-Dichloroethane 37.7 0.500 0.0740 1 7/30/2008
1 , 1-Dichloroethene 8.51 .0.500 0.0890 1 7/30/2008
1 ,2-Dichloroethane 0.540 0.500 0.0790 1 7/30/2008
cis-1.2-Dichloroethene BQL 0.500 0.0650 1 7/30/2008
trans-1.2-dichloroethene BOL 0.500 0.0890 7/30/2008
1 ,2-Dichloropropane BOL 0.500 0.0940 7/30/2008
1,3-Dichloropropane BOL 0.500 0.127 1 7/30/2008
2 ,2-Dichloropropane BOL 0.500 0.0590 1 7/30/2008
1 , 1-Dichloropropene BOL 0.500 0.0720 1 7/30/2008
Dichlorodifluoromethane BOL 5.00 0.0940 1 7/30/2008
· Diisopropyl ether (DIPE) 0.410 0.500 0.0730 1 7/30/2008 J
Ethyl benzene 0.630 0.500 0.0770 1 7/30/2008
Hexachlorobutadiene BQL 0.500 0.228 1 7/30/2008
lsopropylbenzene BOL 0.500 0.0710 1 7/30/2008
4-lsopropyltoluene BQL 0.500 0.0480 7/30/2008
Methylene chloride BOL 5.00 0.0980 7/30/2008
Methyl-tert-butyl ether (MTBE) 4.69 0.500 0.0670 7/30/2008
Naphthalene BOL 0.500 0.133 7/30/2008
n-Propyl benzene 0.240 0.500 0.0800 7/30/2008 J
Styrene BOL 0.500 0.0850 7/30/2008
1, 1, 1,2-Tetrachloroethane BOL 0.500 0.0900 1 7/30/2008
1, 1,2,2-Tetrachloroethane SOL 0.500 0.115 1 7/30/2008
Page 1 of 2 GCMS ils
6110D 5 of 34
c,.,S.6SL
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-2A
Lab Project ID: 8122-3213
Compound
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1 ,2 ,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
1,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
"·
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Delected below the quantitation limit.
Analyst: ~
Results for Volatiles
by GCMS 621 OD
Result Quantitation MDL
UG/L Limit UG/L UG/L
BQL 0.500 0.0690
1.37 0.500 0.0760
BQL 0.500 0.190
BQL 0.500 0.119
BQL 0.500 0.0540
0.350 0.500 0.0540
BQL 0.500 0.182
BOL 0.500 0.111
BQL 0.500 0.120
1.66 0.500 0.0650
0.470 0.500 0.0740
BQL 0.500 0.14,9
2.28 1.00 0.0980
1.14 0.500 0.0650
Spike Spike
Added Result
10 10.6
10 10.1
10 9.93
Page 2 of 2
Analyzed By: RSB
Date Collected: 7/24/2008 13:20
Date Received: 7/26/2008
-·Matrix: Water
Sample Amount: 5 ml
Dilution Date
Factor Analyzed
1 7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7130/2008
1 7/30/200&
1 7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
Percent
Recovered
105
101
99
Flag
J
J
Reviewed By:+
GCMS.~I•
52100 6 of 34
c,.,S6~ Results for Volatiles
by GCMS 6210D
Analyzed By:. RSB
Client Project ID: EMH Electronics Date Collected: 7/24/2008 14:30
Lab Sample ID: G122-3213-4A Date Received: 7/26/2008
Lab Project ID: G122-3213 Matrix: Water
Sample Amount: 5 ml
Result Quantitation MDL Dilution Date
Compound UG/L Limit UG/L UG/L Factor Analyzed Flag
Benzene 315 5.00 0.650 10 7/30/2008
Bromobenzene BQL 5.00 0.560 10 7/30/2008
Bromochioromethane BQL 5.00 1.01 10 7/30/2008
Bromodichloromethane BQL 5.00 0.760 10 7/30/2008
Bromoform BQL 5.00 1.20 10 7/30/2008
Bromomethane BQL 5.00 1;33 10 7/30/2008
n-Butylbenzene BQL 5.00 1.09 10 7/30/2008
sec-Butylbenzene BQL 5.00 0.840 10 7/30/2008
tert-Butylbenzene BQL 5.00 0.500 10 7/30/2008
Carbon tetrachloride BQL 5.00 0.870 10 7/30/2008
Chlorobenzene BQL 5.00 0.820 10 7/30/2008
Chloroethane BQL 5.00 1.06 10 7/30/2008
Chloroform BQL 5.00 0.790 10 7/30/2008
Chloromethane BQL 5.00 1.46 10 7/30/2008
2-Chlorotoluene BQL 5.00 0.990 10 7/30/2008
4-Chlorotoluene BQL 5.00 0.800 10 7/30/2008
Dibromochloromethane BQL 5.00 0.900 10 7/30/2008
1,2-0ibromo-3-chloropropane BQL 50.0 12.1 10 7/30/2008
Oibromomethane BQL 5.00 1.13 10 7/30/2008
1,2-Dibromoethane (EDB) BQL 5.00 1.24 10 7/30/2008
1,2-Dichlorobenzene BQL 5.00 1.27 10 7/30/2008
1,3-Dichlorobenzene BQL 5.00 0.810 10 7/30/2008
1,4-Dichlorobenzene BQL 5.00 0.790 10 7/30/2008
1 , 1-Dichtoroethane BQL 5.00 0.740 10 7/30/2008
1, 1-Dichloroethene BQL 5.00 0.890 10 7/30/2008
1 ,2-Dichloroethane 56.3 5.00 0.790 10 7/30/2008
cis-1,2-Dichloroethene BQL 5.00 0.650 10 7/30/2008
trans-1,2-dichloroethene BQL 5.00 0.890 10 7/30/2008
1,2-Dichloropropane BQL 5.00 0.940 10 7/30/2008
1,3-Dichloropropane BQL 5.00 1.27 10 7/30/2008
2,2-Dichloropropane BQL -5.00 0.590 10 7/30/2008
1, 1-Dichloropropene BQL 5.00 0.720 10 7/30/2008
Dichlorodifiuoromethane BQL 50.0 0.940 10 7/30/2008
Diisopropyl ether (DIPE) 48.3 5.00 0.730 10 7/30/2008
Ethylbenzene BQL 5.00 0.770 10 7/30/2008
Hexachlorobutadiene BQL 5.00 2.28 10 7/30/2008
lsopropylbenzene 4.00 5.00 0.710 10 7/30/2008 j
4-lsopropyltoluene BQL 5.00 0.480 10 7/30/2008
Methylene chloride BQL 50.0 0.980 10 7/30/2008
Methyl-tert-butyl ether (MTBE) BQL 5.00 0.670 10 7/30/2008
Naphthalene 13.0 5.00 1.33 10 7/30/2008
n-Propyl benzene BQL 5.00 0.800 10 7/30/2008
Styrene BQL 5.00 0.850 10 7/30/2008
1, 1, 1,2-Tetrachloroethane BQL 5.00 0.900 10 7/30/2008
1, 1,2,2-Tetrachloroethane BQL 5.00 1.15 10 7/30/2008
Page 1 of 2 GCMS
6210D 9 of 34
c,,,SGS
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-4A
Lab Project-ID: 8122-3213
Compound
Tetrachloroethene
Toluene
1 ,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1 , 1, 1-T richloroethane
1, 1,2-Trichloroethane
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
1,2-Dichloroethane-d4
Toluene-dB
4-B ro m ofluorobenzen e
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit.
Analyst:#-
Results for Volatiles
by GCMS 6210D
Result Quantitatlon MDL
UG/L Limit UG/L UG/L
BQL 5.00 0.690
1.10 5.00 0.760
BQL 5.00 1.90
BQL 5.00 1.19
BQ.L 5.00 0.540
BQL 5.00 0.540
BOL 5.00 1.82
BQL 5.00 1 .11
BQL 5.00 1.20
11.3 5.00 0.650
BQL 5.00 0.740
BQL 5.00 1.49
BQL 10.0 0.980
14.4 5.00 0.650
Spike Spike
Added Result
10 11.2
10 10.3
10 9.89
Page 2 of 2
Analyzed By: RSB
Date Collected: 7/24/2008 14:30
Date Received: 7/26/2008
Matrix: Water
Sample Amount: 5 ml
Dilution Date
Factor Analyzed
10 7130/2008
10 7/30/2008
10 7/30/2008
10 7/30/2008
10 . 7/30/2008
10 7/30/2008
10 7/30/2008
10 7/30/2008
10 7130/2008
10 7/30/2008
10 7/30/2008
10 7130/2008
10 7/30/2008
10 7/30/2008
Percent
Recovered
112
103
99
Reviewed By:+
Flag
J
GCMS
62100
10 of 34
s Results for Volatiles
by GCMS 6210D
Client Samp e et ad Blank Analyzed By: RSB
Client Project ID: Dale Collected:
Lab Sample ID: VBLK30730088 Date Received:
Lab Project ID: ............... Matrix:-Water
Sample Amount: 5 ml
Result Quantitation MDL Dilution Dato
Compound UG/L Limit UG/L UG/L Factor Analyzed Flag
Benzene SOL 0.500 0.0650 1 7/30/2008
Sromobenzene SOL 0.500 0.0560 · 1 7/30/2008
Sromochloromethane SOL 0.500 0.101 1 7/30/2008
Sromodichloromethane SOL 0.500 0.0760 1 7/30/2008
Sromoform SOL 0.500 0.120 1 7/30/2008
Sromomethane SOL 0.500 0.133 7/30/2008
n-Sutylbenzene SOL 0.500 0.109 7/30/2008
sec-Sutylbenzene SOL 0.500 0.0840 7/30/2008
tert-Butylbenzene SOL 0.500 0.0500 7/30/2008
Carbon tetrachloride SOL 0.500 0.0870 7/30/2008
Chlorobenzene SOL 0.500 0.0820 7/30/2008
Chloroethane SOL 0.500 0.106 7/30/2008
Chloroform SOL 0.500 0.0790 7/30/2008
Chiaro methane SOL 0.500 0.146 7/30/2008
2-Chlorotoluene · SOL 0.500 0.0990 7/30/2008
4-Chlorotoluene BOL 0.500 0.0800 7/30/2008
Dibromochloromethane SOL 0.500 0.0900 7/30/2008
1 ,2-Dibromo-3-chloropropane SOL 5.00 1.21 1 7/30/2008
Dibromomethane SOL 0.500 0.113 1 7/30/2008
1,2-Dibromoelhane (EDS) SOL 0.500 0.124 1 7/30/2008
1,2-Dichloroberizene SOL 0.500. 0.127 1 7/30/2008
1,3-Dichlorobenzene SOL 0.500. 0.0810 1 7/30/2008
1,4-Dichlorobenzene SOL 0.500 0.0790 1 7/30/2008
1, 1-Dichloroethane SOL 0.500 0.0740 1 7/30/2008
1, 1-Dichloroethene SOL 0.500 0.0890 1 . 7/30/2008
1,2-Dichloroethane SOL 0.500 0.0790 7/30/2008
cis-1,2-Dichloroethene SOL 0.500 0.0650 7/30/2008
trans-1,2-dichloroethene SOL 0.500 0.0890 7/30/2008
1 ,2-Dichloropropane SOL 0.500 0.0940 7/30/2008
1,3-Dichloropropane SOL 0.500 0.127 7/30/2008
2 ,2-Dichloropropane SOL 0.500 0.0590 7/30/2008
1, 1-Dichloropropene BOL 0.500 0.0720 7/30/2008
Dichlorodifiuoromethane SOL 5.00 0.0940 7/30/2008
Diisopropyl ether (DIPE) SOL 0.500 0.0730 7/30/2008
Ethylbenzene SOL 0.500 0.0770 7/30/2008
Hexachlorobutadiene SOL 0.500 0.228 1 7/30/2008
lsopropylbenzene SOL 0.500 0.0710 1 7/30/2008
4-lsopropyltoluene SOL 0.500 0.0480 1 7/30/2008
Methylene chloride SOL 5.00 0.0980 1 7/30/2008
Methyl-tert-butyl ether (MTBE) SOL 0.500 0.0670 ,1 7/30/2008
Naphthalene SOL 0.500 0.133 1 7/30/2008
n-Propyl benzene SOL 0.500 0.0800 1 7/30/2008
Styrene SOL 0.500 0.0850 7/30/2008 1, 1, 1,2-Tetrachloroethane SOL 0.500 0.0900 7/30/2008
1, 1,2,2-Tetrachloroethane SOL 0.500 0.115 7/30/2008
Page 1 of 2 GCMS.xl,
""
0 11 of 34
Client Project ID:
Lab Sample ID: VBLK3073008B
Lab Project ID:
Compound
Tetrachloroethene
Toluene
1 ,2 ,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Trichloroethene
1 , 1 , 1-T richloroethane
1, 1 ,2-Trichloroethane
T richlo rofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m-,p-Xylene
a-Xylene
1,2-Dichloroethane-d4
Toluene-dB
4-Bromonuorobenzene
Comments:
Flags:
BQL = Below Quantitation Limits.
J = Detected below the quantitation limit
Analyst: -I'~-'\,''----
Result
UG/L
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
Results for Volatiles
by GCMS 621 OD
Quantitation MDL
Limit UG/L, UG/L
0.500 0.0690
0.500 0.0760
0.500 0.190
0.500 0.119
0.500 0.0540
0.500 0.0540
0.500 0.182
0.500 0.111
0.500 0.120
0.500 0.0650
0.500 0.0740
0.500 0.149
1.00 · 0.0980
0.500 0.0650
Spike Spike
Added Result
10 10,3
10 10, 1
10 10.1
Page 2 of 2
Analyzed By: RSB
Date Collected:
Date Received:
Matrix: Water
Sample Amount: 5 ml
Dilution Date
Factor Analyzed
1 7/30/2008
1 7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
7/30/2008
Percent
Recovered
103
101
101
Flag
GCMS.ds
62100 12 of 34
SGS Environmental Sevices
CONTROL SAMPLE/LABORATORY CONTROL SAMPLE DUPLICAT~ RECOVERY
Dilution:
Lab Code: NC00919
LCS: LCSJ073008A
LCSD: LCS30730088
YJ<1trix: Water
ilename: 0730305.D
1Jerwme: 0730306.D
Date Analyzed: 07/:!t1/1)8 10:53
Dale Analyzed: 07/"J0/1;8 11:28
LC1? LCS LCS LCSO
SPIKE CONC • SPIKE
COMPOUND (µg/L) (µg/L) REC I (µg/L)
acetone 25.0 25.6 102 25.0
acrolein 125 101 80.B 12 5
acrylonitrile 125 101 85.3 125
benzene 5.00 4.80 96.0 5.00
bromobenzene 5.00 4.69 93.B 5.00
bromochloromethane 5.00 '1. 7 6 95.2 5.00
bromodichloromethane 5.00 4.83 96. 6 5.00
bromoform 5.00 4.28 85.6 5.00
bromomethane 5.00 3.96 79.2 5.00
2-butanone 25.0 26.0 1 o, 25.0
n-butylbenzene 5.00 4.61 92.2 5.00
sec-butylbenzene 5.00 '1. '11 88 . 2 5.00
tert-butylbenzene 5.00 4.69 9J. 8 5.00
Carbon disulfide 5.00 4. 8 4 96 .8 5.00
carbon tetrachloride 5.00 '1. 92 98. ' 5.00
chlorobenzene 5.00 4.52 90.4 5.00
chloroethane 5.00 4. 19 83.8 5.00
2-chloroethyl vinyl ether 125 99.3 79.4 125
chloroform 5.00 4 . 8 5 91 .0 5.00
chloromethane 5.00 3.84 16 . 8 5.00
2-chlorotoluene 5.00 4.85 91 .0 5.00
4-chlorotoluene 5.00 '1. 35 81 • D 5.00
· dibromochloromethane 5.00 IJ. 54 90.8 5.00
1,2-dibromo-3-chloropropane 25.0 25.2 101 ·25. 0
1, 2 dibromomethane 5.00 4.16 B3.2 5.00
dibromomethane 5.00 '1. 40 !18. 0 5.00
1,2-dichlorobenzene 5.00 4.79 95.8 5.00
1,3-dichlorobenzcne 5.00 4.75 95.0 . 5.00
1,4-dichlorobenzene 5.00 4.84 ·96. 8 5.00
trans-1,4-Dichloro-2-butene 25.0 21. 6 8 6. 4 25.0
dichlorodifluoromethane 5.00 4.25 8 5. 0 5.00
1,1-dichloroethane 5.00 4.93 96.6 5.00
1,2-dichloroethane 5.00 5.04 l 01 5.00
1,1-dichloroethene 5.00 4.78 95.6 5.00
cls-1,2-dichloroethene 5.00 4 . 91 98.2 5.00
trans-1,2-dichloroethene 5.00 4 . 81 96.2 5.00
],2-dichior.opropane 5.00 4.70 94 .0 5.00
1,3-dichlorupropane 5.00 · 4. 67 93. ' 5.00
2,2-dichloropropanc 5.00 4. 87 91. ' 5.00
1, 1-dichloropropene 5.00 ' .9J 98.6 5.00
cis-1,3-dichloropropene 5.00 4.1;13 96.6 5.00
Column to b?. used to flag recovery dOd RPO values with an asteri8k
Values outside of QC limits
RPO: l out of 72 outside of limits
Spike Recovery: 0 out of 144 outside of limits
COMMENTS:
pilge 1 of 2 LCS/LCSD VOA-1
LCSD LCSD
CONC • (µg/L) REC I
2 8. I: 114
i;:·, 102
1:16 109
5. '.l ~ 111
5,Hl 10 9
5. '.}I 111
5. J!! 112
5. 1 ·1 lOJ
5. 11 108
29. P. 119
5. 11 102
5.0~ 101
·5 . .16 101
5. i,o 110
5. ()'I llJ
5. J1 106
5. I 0 104
l ;:q, I 103
5. !,l 110
5.0J 101
5. '.i"J 111
'1.'.i!; 99.0
5. 1 •.i 104
2H.G 112
5. Ill 100
5. 1;: 102
5. :i:~ 110
5. J~• 108
5. '10 108
24.6 9B.5
5. '1fi 109
5. :,u 112
5. '/IJ 115
5.61 112
5. '.)2 110
5. 4fi 109
5. 51 110
5. '10 108
5. ·15 115
5. ·10 11'
5. '.iU 110
' QC LIMITS
RPO RPO REC
10.9 JO 23.5-141
2J .0 JO 31.4-182
2 4 • 0 JO 64.2-140
14. 5 JO 76.6-120
15.2 JO 75.0-122
15.7 JO 74 . 8 121
14. 4 30 76,4-117
18,8 JO 62.4-127
30.9· JO 34.2-166
13. 6 30 '14.9-126
10.3 30 72.0-122
13. 5 30 78.)-116
13. 3 JO 53.1-148
12.8 JO 69.0-118
13. 6 JO 71. 7-12'1
15.9 JO 75.5-116
21. l JO 7B.2-138
2 6. l 30 5.57-235
12.7 30 80.6-117
26.B 30 72.6-127
13.B 30 91. 4-117
12.9 30 82.1-116
1 J . 4 30 73.1-117
10.7 JO 58.0-133
1 B. 5 JO 75.5-118
15. 1 30 77. 3-12'1
14. 2 30 76.3-115
12.6 30 79.1-114
10.5 JO 76.8-115
13.2 JO 52.3 llO
24. 9 30 69.8-13'1
14. 4 30 78.0-120
13.0 30 72.8-126
15.B 30 74.6-121
11. 7 30 78.0-121
12.6 30 60.7-14'1
15. 9 30 75.8-119
14. 5 30 78. 5-113
16.6 JO '/5. 6-130
14 . 5 JO 79.7-117
13. 0 30 79.8-113
0LM04. 2
13 of 34
SGS Environmental Sevices
CONTROL SAMPLE/LABORATORY CONTROL SAMPLE DUPLICATE RECOVERY
Dilution:
LC$: LCS3073008A
LCSD: LCS3073008B
COMPOUND
t rans-1, 3-dichl oropropene
Diisopropyl ether
cthylbenzene
hexachlorobutadiene
?.-hexanone
Iodomethane
isopropylbenzene
4-isopropyltolucne
Methyl-tert-butyl ether
methylene chloride
4-methyl-2-pentanone
n<1phthalene
n-propyl benzene
styrene
1, 1, I, 2-tetrachlorocthane
1,1,2,2-tetrachloroethane
tetrachloroethene
toluene
1,2,)-trichlorobenzene
l, 2, 4.-trichlorobenzene
1,1,1-crichloroethane
1,1,2-trichloroethane
trichloroethene
trichlorofluoromethane
1,2,3-trichloropropane
1,2,4-trimethylbenzene
1,3,S-trimethylbenzene
Vinyl acetate
vinyl chloride
m/p-xylenc
o-><ylene
System Monitoring Compound Results
460-00-4 4-Bromofluorobenzene
17060-07-0 l,2-Dichloroethane-d4.
2037-26-5 Toluene-dB
ilenarae: 0730)05.D
ilename: 0730306.D
LCS
SPIKE
(µg/L)
5.00
5.00
5.00
5.00
25.0
5.00
5.00
5.00
5.00
5.00
25.0
5.00
5.00
5,00
~.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5 . 00
5.00
5.00
5.00
12.5
5.00
10.0
5.00
LCS
SPIKE
{µg/L)
10
10
10
LCS
CONC
(µg/L)
4.83
4. 9 3
4.74
5. 19
25.0
4.n
4. 7 B
4. 82
<1 • 10
4. 82
2 4 . 6
5. 51
4.81
'1. 71
'1. 68
4.90
4. 65
4.88
5.31
5.02
4.82
4. 64.
4 . 82
4 . 36
4 . 2 3
4 . 81
4 . 81
12.3
4.23
9.53
'1.67
LCS
CONC
(µg/L)
9.9
10.5
10.22
Date Analyzed: 07/:tO/liS 10: 53
Date Ar,alyzed: 07/:l0/1l8 11:28
LCS LCSD LCSll I LCSD • SPIKE co:K • REC I {µg/L) (µg/1.) REC D
96.6 5.00 5. ~l• 110
98.6 5.00 5. '1li 110
94 . 8 5.00 5. Jl 106
104 5.00 5. 1 f. 103
100 25.0 2 ~. {) 116
ea .2 5.00 4 .:!'/ 85.4
95. 6 5.00 5. " 101
96. 4 ·s.oo 5. " 101
95. 6 5.00 5. ',. 109
96. 4 5.00 5. D 101
98 .5 25.0 29. I 116
110 5.00 5. fi() 112
96.2 5.00 5. ] ~) 101
94.2 5.00 5. ] J 107
93.6 5.00 5. UI 104
98.0 5.00 5. 69 114
93.0 5.00 5.Hl 110
97.6 5.00 5.60 112
106 5.00 5. ] ~· 108
100 5.00 5. ];' 106
96.'1 5.00 5. '.1'.) 111
92 . 0 5.00 5. '11 108
96. 4 5.00 S. 6 4 113
8'"/. 2 5.00 5. r.o 112
84.6 5.00 '1. 'J'.! 98.6
96.2 5.00 5.]8 108
96.2 5.00 5. J!> 108
98.6 12.5 14 . 0 112
84.6 5.00 5.4) 108
95.3 10.0 IO .. _, 101
93.4 5.00 5. Jh 107
LCS LCSO LC~;p LCSO
I SPIKE CCNC I
REC tt (µg/L) (µg/1.) REC tt
99.0 10 9. U~; 98.5
105 10 10. 7] 107
102 10 10.29 103
Matrix: Water
• QC LIMITS
RPO RPO REC
13 . 0 JO 79.0-113
10.6 JO 71-.8-115
11. 3 JO 80.5-115
0. 580 JO 63.3-139
14 .8 JO 46. 8-123
3.22 JO 29.3-156
11. l JO Bl. 6-114
10.2 JO 78.4-119
1) .1 30 76.0-114
10.0 30 72.9-120
16,'"/ 30 56.2-124
1. 62 JO 24.0-182
10.6 30 79.0-116
12.4 JO 6'1.8-1)2
10,1 30 78.8-118
l '1. 9 30 69.7-119
16. ~ 30 55.)-144
13. 7 30 78.6-117
1.50 30 20 ,8-193
5.80 30 "· 9-150
14 . I 30 18 .8-120
15.3 JO 73. 6-117
15. 8 30 80.1-116
2 4 . 9 30 80.5-130
15.3 JO 35.6-152
11 . 2 30 77.0-116
11. 4. 30 79.'1-114
12.7 30 60. 7-127
24.8 30 77.5-126
11. 8 JO 82.9-112
13.0 JO 81,)-113
QC LIMITS
REC
84.7-115
63.5-140
81.8-117
If Column to be used to flag recovery and RPO values with an asterisk
Values outside of QC limit5
RPO: l out of 72 outside of limits
Spike Recovery: 0 out of 144 outside of limits
COMMENTS:
An.:1lyst:
. page 2 of 2
Reviewed by,¥-
LCS/LCSD VOA-2 0LM0'1. 2
14 of 34
SGS EnvironmCntal Services
3A
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Code: NC00919
EPA Sample No.: gl22-3213-3a, gl22-3213-3a, gl22-3213-3a
filenames; 0730313.D, 073031'1.0, 0730315.D
SAHPLE MS MS MS MSD
CONC SPIKE CONC ' SPIKE
COMPOUND {µg/L) (ug/L) (µg/L) REC ' {µg/L)
acetone BQL 20000 22700 114 • 20000
acrolein DQL 100000 97200 97.2 100000
acrylonitrile DQL 100000 102000 102 100000
benzene 64 90 4000 10900 111 4000
bromobenzenc BQL 4000 4'120 l l 0 4000
bromochloromethane BQL 4000 4 4 l 0 11 0 4000
bromodichloromethane BQL 4000 4430 111 4000
bromoform BQL 4000 3930 98.2 4000
bromomethane DQL 4000 3540 9 9. 6 4000
2-butanone BQL 20000 24600 12 3 • · 20000
n-butylbenzene BQL 4000 3990 99.8 ,woo
sec-butylbcnzene BQL 4000 3840 96.0 4000
tert-butylbcnzene OQL 4000 4340 10B 4000
Carbon disulfide BQL 4000 4230 106 4000
carbon tetrachloride BQL 4000 4290 107 4000
chlorobenzene DQL 4000 3940 99.6 4000
chloroethane BQL 4000 3540 89.4 4000
2-chloroethyl vinyl ether BQL 10000 99500 895· 10000
chlorofocm BQL 4000 4280 107 4000
chlocomethane BQL · 4000 3460 8 6. 4 4000
2-chlorotoluene BQL 4000 4180 1 o, 4000
'1-chlorotolucne BQL 4000 3730 93.2 4000
dibromochloromethane OQL 4000 4140 103 4000
1,2-dibromo-3-chloropropane BQL 20000 24300 121 20000
1,2-dibromomethane BQL 4000 4160 1 o, 4000
dibromomethane BQL ,moo 4110 103 4000
1,2-dichlorobenzene BQL 4000 4.420 110 4000
1,3-dichlorobenzene OQL 4000 4180 105 4000
1,4-dichlorobenzene BQL 4000 4160 104 4000
trans-1,4-Dichloro-2-butenc BQL 20000 20400 102 20000
dichJorodifluoromethane BQI, 4000 3880 97.0 4000
1,1-dichlorocthane BQL 4000 4280 107 4000
1,2-dichlorocthane BQL 4000 5200 130· 4000
1,1-dichloroethene BQL 4000 4060 10 1 ,ooo
cis-1,2-dichloroethene BQL 1000 4250 106 4000
trans-1,2-dichloroethene BQL 4000 414 0 103 4000
1,2-dichloropropane BQL 4000 4220 10 6 4000
1,3-dichloropropane BQL 4000 4360 109 4000
?.,2-dichloropropane BQL q 000 4390 110 4000
1,1-dichloropropene BQL 4000 4370 109 4000
ci3-l,3-dichloropropcne BQI, 4000 4390 110 4000
~ Column to be used to [lag recovery and RPO values with an asterisk
Values outside of QC limits
COMMENTS:
pagelof2 FORM III V0A-1
MSll
C-:)tJC
(µ:J/1.)
2 I '.!CH;
101.0()')
lOf:iUOO
1 lOOO
~ l ·10
4 ·i •I 0
4 1')0
3q·10
J'/1i(l
21100
4 0]0
3!190
'1.1.90
4?.llO
I\ 340
4 0 50
:!FIO
9 lfi()(;
,n,i(J ---:if} 1.0
'1 Of,()
]llJO
4100
2100(;
4 1.;!o
40?0
4/.90'
41 !JO
41.'Hl
21)200
Ji.no
41:'.0
~ l Hl
4 1.40
'1:LJO
4?.]0
4 JOO
4?.90
l\]'10
4 3·10
4:no
Inst: HS03
Batch: 307 3008
Dilution: 800
Matrix: Water
MSD
' I QC LIMITS
REC ' RPD RPO REC
108 * 5.50 30 17.7-85. 2
101 3.91 30 0.00-424
106 3.68 30 85.0-175
113 1. 60 30 61.6-135
10, 5.78 30 65.1-125
108 1. 65 30 75.5-126
110 0.907 30 14. 3-123
99.2 1.01 30 57.. 3-122
94. 0 5. 91 30 10.0-284
120* 2.20 30 36.1-107
101 0.997 30 70.2-124
97.2 1. 24 30 62.0-133
105 3.38 30 73.5-121
107 1. 13 30 68.8-129
109 1. 11 30 71.8-122
101 2. 60 30 77. 2-118
94.2 6. 35 30 10.0-233
936* 4,54 30 16.7-283
109 1. 30 30 74.0-128
90.2 4,30 30 72.0-139
101 2.92 30 79.3-118
95.8 2,75 30 76.8-120
103 0.777 30 69. 0-117
120 1. 13 30 20.2-171
103 0.966 30 78.5-123
100 . 2.36 30 71.3-137
107 2.94 30 75.1-120
1 o, 0. 191 30 73.1-121
107 3.03 30 74.8 118
101 1. 10 30 25.7-149
98.2 1 , 2 3 30 41. 7-166
110 3. 13 30 75,6-128
128* 1. 71 30 n. 1-121
10, 2. 15 30 64.4-130
109 1. 86 30 72.7-134
106 2.29 30 74. 6-124
107 1. 69 30 76. 5-129
107 L 66 30 79.1-121
109 1.10 30 31.5-157
109 0.00 30 72.5-120
109 0.548 30 66,6-132
0LM04.2
15 of 34
SGS Environmental services
3A SG$
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATI·: Rl~COVERY
Lab Name: SGS Environmental
Lab Code: NC00919
EPA Sample No.: gl22-3213-33, gl22-3213-3a·, gl22-3213-3a
Filenames: 0730313.D, 0730314.D, 0730315.D
SAMPLE MS MS MS MS □
CONC SPIKE CONC I SPIKE
COMPOUND (µg/L) (µg/L) {µg/L) REC " (µg/L)
trans-1,3-dichloropropene BQL 4000 4390 110 4000
Di1sopropyl ether BQL 4000 4500 110 4000
!!thylbenzene 2040 4000 6120 102 4000
hexachlorobutadiene BQL 4000 3820 95.6 4000
2-hexanone BQL 20000 24900 124* 20000
Iodomethanc BQL 4 000 24 50 61. 2 4000
isapropylbenzene BQL 4000 4180 101 4000
4-isopropyltoluene BQL 4000 41'10 104 11000
Methyl-tert-butyl ether 904 4000 5520 l 15 4000
methylene chloride BQL q 000 4250 106 4000
4-methyl-2-pentanone BQL 20000 2000 122 20000
naphthalene 1020 4000 5470 111 ,1000
n-propyl benzene BQL 4000 2380 50. 4 .. 4000
::;tyrene BQL 4000 4400 110 4000
1,1,1,2-tetrachloroethane BQL 4000 4120 103 4000
1,1,2,2-tetrachloroethane BQL 4000 <1770 119 4000
cetrachloroethenc BQL 4000 4060 102 4000
toluene 15600 4000 20400 118 4000
1,2,3-trichlorobenzene BQL 4000 3980 99.4 4000
l,2,4-trichlorobenzene BQL qOOO 4140 103 4000
1, 1,1-trichloroethane BQL 4000 4360 109 4000
• 1,1,2-trichloroethane DQL 4000 4280 107 4000
trichloroethene BQL 4000 4340 108 4000
trichlorofluoromethane BQL 4000 3950 98.8 4000
1,2,3-trichloropropane BQL 4000 4050 101 4000
1,2,4-trimethylbenzene 3300 4000 7500 105 4000
1,3,5-trimethylbenzene 888 4000 5100 105 4000
Vinyl acetate BQL 10000 11400 114 10000
vinyl chloride BQL 4000 3750 93.8 4000
m/p-xylene 88'10 8000 17300 105 8000
o-xylene 4270 4000 8390 103 4000
System Monitoring Compound Results MS MS MS MSD
SPIKE CONC I SPIKE
(µg/L) (µg/L) REC " (µg/L)
460-00-4 4-Bromofluorobenzene l 0 9.95 99.5 10
17060-07-0 l,2-Dichloroethane-d1 10 11. 21 112 10
2037-26-5 Toluene-dB 10 10. 17 102 10
Column to be used to flag recovery and RPO value8 with an asterisk
Values outside of QC limits
MSI)
CONC
{µrill,)
4'.!'!0
'1 '.iEiO
(, 100
4 o:~ n
2,1.1 nc
t."/•10
t, ;~-I 0
401!0
!i•l'.-:O
'1 l '10
21?.0C
~) /. '.i ()
4 4 "l()
4 ]llO
'10'10
46!J0
4 1'10
20400
4 7.'.iO
4 l!lO
4 400
I) \"}()
•HOO
I\ 0-J()
I\ OiHl
·1 1:,0
'.;()(i()
11 ~oi;
lj{l()(l
1 h9(){;
ti:rno
MSU
COtJC
(1-.tq/l,l
9. H'.i
l l . ;'. ;·
}1).1]
Inst: MSD3
Batch: 3073008
Dilution: 800
Matrix: Water
MS□
' I QC l.JMITS
REC " RPD RPD REC
109 0.548 30 44.7-1'14
111 1. 27 30 79.4-122
101 0.590 30 73.8-126
100 4. 90 30 51. 8-134
120• 3.26 30 41.6-111
68,6 11. 4 30 40.6-126
103 1. 37 30 74.3-123
102 1. 56 30 74.6-122
113 2.10 30 66. 5-136
105 l. 33 JO qa.6-155
121 0.594 30 6.88-166
106 5. 17 30 55.1-140
102 67. 4 .. 30 71. 6-128
109 0. 547 30 73.2-123
101 l. 96 30 69. 4-120
117 1. 86 30 75. 7-136
104 1.95 30 45.8-153
118 0.508 30 66.4-128
106 6.61 JO 61. 0-126
105 1. 15 30 60.6-125
110 0. 913 30 78.4-121
104 2. 65 30 64. 8-128
110 1. 46 30 84.9-136
102 2.99 30 76.8-132
102 0.787 30 10,0-218
101 3. 68 30 31.0-172
104 1. 14 30 67,7-132
115 0.349 30 0.00-355
100 6. 40 30 68.1-137
101 4.07 30 "/9.. 8-118
100 2.76 30 80.0-121
MSD
' QC LIMITS
REC # REC
98.5 84. "/-115
112 63.5-1.40
10 1 81.8-117
MS Spike Recovery: 6 failure(s) out of 72. MSD Spike Recovery: 5 failure(sl 011t of 72.
RPO: l out of 72 outside of limits
COMMENTS:
Analyst,~ Reviewed by, f
page2of2 FORM III VOA-2 0LM01.2
16 of 34
VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name: Mid-Atlantic Associates
Project Name: EMH Electronics
Sample Identification
Sample Matrix
Sample Information
Collection Option (for Soil}"
Date Collected
Date Received
B-3
Water
NA
07/24/08
07/26/08
Date Extracted 07/31/08 10:52 -07/31/08 10:52
. Date Analyzed 07/31/08 10:52 -07/31/08 10:52
Ory Weight NA
Dilution Factor 2-2
Analytical Results
Report
Analyte Result Limit
µg/L µg/L Flags
C5-C8 Aliphatics .. 325 100
C9-C 12 Aliphatics" 894 100
C9-C10 Aromatics'' 3370 100
Percent Limits
Recovery Flags Lower I Upper
Surrogate % Recovery -PIO 105 70 130
Surrogate % Recovery -FID 110 70 130
* = Option 1 = Established fill line. on vial, Option 2 = Sampling Device/Brand, or Option 3 = Field weight of soil.
.. = Excludes any surrogates or internal standards and are unadjusted for individual analytes.
Lab Info: G122-3213-1e Lab Info: G122-3213-1e
FID Info: VP073108/008F0101.D PIO Info: VP073108/008R0101.D
Reviewed By: '¾}ct
17 of 34
_S
VPH (Aliphatics/Aromatics) Laboratory Reporting Form . --
Client Name: Mid-Atlantic Associates
Project Name: EMH Electronics
Sample Information
Sample Identification B-4
Sample Matrix Water
Collection Option (for Soil)' NA
Date Collected 07/24/08
Date Received 07/26/08
Date Extracted 07/31/08 11:19-07/31/0811:19
Date Analyzed 07/31/0811:19-07/31/0811:19
Dry Weight NA
Dilution Factor 125 -125
Analytical Results
Report
Analyte Result Limit
µg/L µg/L Flags --C5-C8 Aliphatics .. 43300 631
C9-C 12 Aliphatics" 28300 472
C9-C 10 Aromatics** 13400 282
Percent Limits
Recovery Flags Lower I Upper
Surrogate % Recovery -PIO 95.9 70 130
Surrogate% Recovery -FID 98.5 70 130
• = Option 1 = EstabUshed fill line on vial, Option 2 = Sampling Device/Brand, or Option 3 = Field weight of soil.
0 = Excludes any surrogates or internal standards and are unadjusted for individual analytes.
Lab Info: G122-3213-3e Lab Info: G122-3213-3e
FID Info: VP073108/009F0101.D PIO Info: VP073108/009R0101.D
Reviewed By: ~Ciq.,.,,../ __
19 of 34
SGS
VPH (Aliph~tics/Aromatics) Laborat?ry Reporting Form
Client Name: Mid-Atlantic Associates
Project Name: EMH Electronics
Sample Identification
Sample Matrix
Sample Information
Collection Option (for Soil)*
Date Collected
Date Received
B-6
Water
.NA
07/24/08
07/26/08
Date Extracted 07/31/08 03:08 -07/31/08 03:08
Date Analyzed 07/31/08 03:08 -07/31/08 03:08
Dry Weight NA
Dilution Factor 1 • 1
Analytical Results
Report
Analyte Result Limit
µg/L µg/L Flags
C5-C8 Aliphatics•• BOL 100 .
c,-C12 Aliphatics•• BOL 100
C9-C 10 Aromatics•• BOL 100
Percent Limits
Recovery Flags Lower I Upper
Surrogate % Recovery -PIO 94.7 70 130
Surrogate % Recovery -FID 98.9 70 130
* = Option 1 = Established fill line on vial, Option 2 = Sampling Device!Brand, or Option 3 = Field weight of soil.
..., = Excludes any surroga.tes or internal standards and are unadjusted for indiVidual analytes.
Lab Info: G122-3213-2d Lab Info: G 122-3213-2d
FID Info: VP073008/044F0101.D PIO Info: VP073008/044R0101.D
Reviewed By: .,.(¼,.,J.__· _
18 of 34
VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name: Mid-Atlantic Associates
Project Name: EMH Electronics
Sample Identification
Sample Matrix
Sample Information
Collection Option (for Soil}"
Date Collected
Date Received
B-13
Water
NA
07/24/08
07/26/08
Date Extracted 07/31/08 10:25 -07/31/08 10:25
Date Analyzed 07/31/08 10:25, 07/31/08 10:25
Dry Weight NA
Dilution Factor 1 - 1
Analytical Results
Report
Analyte Result Limit
µg/L µg/L Flags
C5-C, Aliphatics" 804 100
C9-C12 Aliphatics" BQL 100
C9-C10 Aromatics"'" BQL 100
Percent Limits
Recovery Flags Lower I Upper
Surrogate % Recovery -PIO 101 70 130
Surrogate % Recovery -FID 104 70 130
* = Option 1 = Established fill line on vial, Option 2 = Sampling Device/Brand, or Option 3 = Field weight of soil.
... = Excludes any surrogates or internal standards and are unadjusted for individual analytes.
Lab Info: G122-3213-4c Lab Info: G122-3213-4c
FID Info: VP073108/007F0101.D PIO Info: VP073108/007R0101.D
Reviewed By: i,1,=~..,,~1 __
20 of 34
VPH (Aliphatics/Aromatics) Laboratory_Reporting_Form
Client Name: _________________________ _
Project Name: _________________________ _
Sample Information
Sample Identification VBLK4073008a
Sample Matrix Water
Collection Option (for Soil;< NA
Date Collected
Date Received
Date Extracted
Date Analyzed 07/30/08 10:01 -07/30/08 10:01
Dry Weight 100
Dilution Factor 1 - 1
Analytical Results
Report
Analyle Result Limit
µg/L µg/L Flags
C5-C8 Aliphatics .. BOL 100
C9-C 12 Aliphatics•· BOL 100
C9-C10 Aromatics0 BOL 100
Percent Limits
Recovery Flags Lower I Upper
Surrogate % Recovery -PID 93.1 70 130
Surrogate % Recovery -FID 97.9 70 130
• = Option 1 = Established fill line on vlat, Option 2 = Sampling Device/Brand, or Option 3 .= Field weight of soil.
** = Excludes any surrogates or internal standards and are unadjusted for individual analytes.
Lab Info: VBLK4073008a Lab Info: VBLK4073008a
FID Info: VP073008/006F0101.D PID Info: VP073008/006R0101.D
Reviewed By:~
21 of 34
SGS
Lab Sample ID:
Lab Project ID:
Report Basis:
Analyte
C5-C8 Aliphatics
C9-C 12 Aliphatics
C9-C10 Aromatics
Total VPH
Surrogate
Standards
Surrogate -PIO
Surrogate -FID
LABORATORY CONTROL SPIKE RESULTS
by Method VPH
SGS Environmental Services, Inc.
LCS4073008A
Batch QC
Wet
Analyzed By:
Matrix:
Percent Solids:
Analvtical QC Results Summarv
Expected Measured Percent Lower . Upper
Amount Amount Recovery Limit Limit
uo/L ua/L {%) (%) 1%)
79.5
42.8
24.0
200 146 73.0 70.0 130
Expected Measured Percent Lower Upper
Amount Amount Recovery Limit Limit
11n/L ua/L (%) (%) (%)
1250 886 70.9 70.0 130
1250 1128 90.2 70.0 130
Water
NA %
Qualifier
Qualifier
Reviewed By: -~""Y'd._-____ _
22 of 34
SGS MATRIX SPIKE I MATRIX SPIKE DUPLICATE RESULTS
by Melhod VPH
SGS Environmental Services, Inc.
Lab Sample ID: G563-226-3a Analyzed By: MJC
MS Sample.ID: G563-226-3a Matrix: Soil
MSD Sample ID: G563-226-3a Percenl Solids: 92.6 .%
Lab Project ID: Batch QC for VP073008
Report Basis: Dry
Matrix S ike Results Summa
Analyte Sample Spiked Measured Percent Lower Upper Qualifier
Amount Amount Recovery Limit Limit
m IK m IK % % %
C5-C8 Aliphatics 3.860
C9-C 12 Aliphatics 6.810 11.40
C9-C10 Aromatics 8.610 11.20
TolalVPH 19.300 17.8 37.1 101.0 70 130
Matrix S llcate Results Summa
Analyte Spiked Measured Percent Lower Upper Qualifier
Amount Recovery Limit Limit
m % % %
C5-C8 Aliphatics
C9-C12 Aliphalics 12.10
C9-C 1 O Aromatics 11.50
Total VPH 17.8 38.5 108.0 70 130
Analyte MS MSD RPO RPO Qualifier
Amount Amount Value Limit
mg/Kg mg/Kg (%) (%)
CS-CB Aliphalics
C9-C 12 Aliphatics
C9-C 10 Aromatics
Total VPH 37.1 38.5 4 20
Reviewed By: -=4,...,el~----
23 of 34
VPH (Alipliatics/Aromatics) Laoorafory Reporting Form
Client Name: _________________________ _
Project Name: _________________________ _
Sample lnfonnation
Sample Identification VBLK4073108a
Sample Matrix Water
Collection Option (for Soilt NA
Date Collected
Date Received
Date Extracted
Date Analyzed 07131/08 09:58 -07131/08 09:58
Dry Weight 100
Dilution Factor 1-1
Analytical Results
Report
Analyte Result Limit
.. ..
µg/L µg/L
... ....
Fiags
C5-C 8 Aliphatics .. BQL 100.
C9-C12 Aliphatics .. BQL 100
C9-C,0 Aromatics0 BQL 100
Percent Limits
Recovery Flags Lower f Upper
Surrogate% Recovery-PID 101 70 130
Surrogate% Recovery -FID 104 70 130
* = Option 1 = Established fill line on vial, Option 2 = Sampling Device/Brand, or OJ)tion 3 = Ffefd weight of soil.
.. = Excludes any surrogates or internal standards and are unadjusted for individual analytes.
Lab Info: VBLK4073108a Lab Info: VBLK4073108a
FID Info: VP073108/006F0101.D PIO Info: VP073108/006R0101.D
Reviewed By: ~
24 of 34
SG$
Lab Sample ID:
Lab Project ID:
-· Report Basis:
Analyte
C5-C8 Aliphatics
C9-C 12 Aliphatics
C9-C 10 Aromatics
Total VPH
Surrogate
Standards
Surrogate -Pl D
Surroaate -FID
LABORATORY CONTROL SPIKE RESULTS
by Method VPH
SGS Environmental Services, Inc.
LCS40731 OBA
Batch QC
Analyzed By:
Matrix:
Wet Percent Solids:
Analytical QC Results Summary
Expected Measured Percent Lower Upper
Amount Amount Recovery Limit Limit
un/L 11n/L (%\ (%\ (%)
121
58.3
45.4
200 224 112 70.0 130
Expected Measured Percent Lower Upper
Amount Amount Recovery Limit Limit
11n/L 11n/L {%\ {%) {%\
1250 1227 98.1 70.0 130
1250 1275 102 70.0 130
Water
NA %
Qualifier
Qualifier
Reviewed By:-¥,=,,-------
25 of 34
Lab Sanip]? lQ;
MS Sample ID:
MSD Sample ID:
Lab Project ID:
Report Basis:
Analyte
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C 10 Aromatics
Total VPH
Analyte
C5-C8 Aliphatic.s
C9-C12 Aliphatics
C9-C10 Aromatics
Total VPH
Analyte
C5-C8 Aliphatics
C9-C12 Aliphatics
C9-C10 Aromatics
TolalVPH
MATRIX SPIKE/ MATRIX SPIKE DUPLICATE RESULTS
by Method VPH
SGS Environmental Services, Inc.
G 161-2781-Se
G161-2781-5e
G161-2781-5e
Batch QC for VP073108
Dry
Analyzed By_:
Matrix:.
Percent Solids:
Matrix S ike Results Summa
Sample Spiked Measured Percent Lower
Amount Recovery Limit
m IK % %
7.000
9.750 14.30
9.260 11.40
26.000 16.6 43.4 105.0 70
Matrix S licate Results Summa
Spiked Measured Percent Lower
Amount Recovery Limit
m % %
14.30
11.90
16.6 44.9 114.0 70
MS MSD RPD
Amount Amount Value
m11/K11 m11/K11 (%1
43.4 44.9 3
MJC
Soil
77.4
Upper
Limit
%
130
Upper
Limit
%
130
RPD
Limit
(%)
20
%
Qualifier
Qualifier
Qualifier
Reviewed By: -=-?A➔~"------
26 of 34
SGS
Client Sample ID: B-3
Client Project ID:
Lab Sample ID:
EMH Electronics
G122-3213-1
Lab Project ID:
Batch ID:
Metals
Lead
Comments
G 122-3213
11977
Result
14.7
BOL = Below Quantitation Limits
OF = Dilution Factor
J = Between MDL and RL
B= Amount in Prep Blank> MDL
Samples Prepared by 3030C
RL
5.00
Results for Metals
MDL OF Units
0.617 25 UG/L
Analyzed By: PSW
Date Collected: 7/24/2008 13:00
Date Received: 7/26/2008
Matrix: WATER
Method
6020
Date Flags
Analyzed
7/29/2008
Reviewed By: ,1,.,,/
M~
27 of 34
Cli.ent Sample ID: 8-4
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-3
Lab Project ID: G122-3213
Batch ID: 11977
Metals Result
Lead 83.1
Comments
BQL = Below Quantitation Limits
OF = Dilution Factor
J = Between MOL and RL
B= Amount in Prep Blank > MDL
Samples Prepared by 3030C
RL
5.00
Results for Metals
MDL OF
0.617 25
Units
UG/L
Analyzed By: PSW
Date Collected: 7/24/2008 13:50
Date Received: 7/26/2008 ·
Matrix: WATER
Method Date Flags
Analyzed
6020 7/29/2008
Reviewed By: ueu/
M~
29 of 34
Client S.ampJe ID: Bc6. __ .
Client Project ID: EMH Electronics
Lab Sample ID: G122-3213-2
Lab Project ID: G122-3213
Batch ID: 11977
Metals Result
Lead 12.2
Comments
BOL = Below Ouantitation Limits
DF = Dilution Factor
J = Between MDL and RL
B= Amount in Prep Blank > MDL
Samples Prepared by 3030C
RL
5.00
Results for Metals
MDL DF
0.617 ·25
Units
UG/L
Analyzed.By:--·-·--RSW.-
Date Collected: 7/24/2008 13:20
Date Received: · 7/26/2008
Matrix: WATER
Method Date Flags
Analyzed
6020 7/29/2008
Reviewed By: Qa,/
M~
28 of 34
SG$
Client SampleJD: .B::-13
Client Project ID:
Lab Sample ID:
Lab Project ID:
Batch ID:
EMH Electronics
G122-3213-4
G122-3213
11977
Metals Result
Lead 35.3
Comments
BOL = Below Quantitation Limits
OF = Dilution Factor
J = Between MDL and RL
B= Amount in Prep Blank > MDL
Samples Prepared by 3030C
RL
5.00
Results for Metals
MDL DF Units
0.617 25 UG/L
Analyzed By: PSW
Date Collected: 7/24/2008 14:30
Date Received: 7/26/2008
Matrix: WATER
Method
6020
Date
Analyzed
7/29/2008
Flags
Reviewed By: r.,w)
M~
30 of 34
Client Sample ID: Lab Blank
Client Project ID:
Lab Sample ID:
Lab Project ID:
Batch ID:
Metals
Lead
Comments
pb11977
11977
Result
BOL
BOL = Below Ouantitation Limits
OF = Dilution Factor
J = Between MDL and RL
B= Amount in Prep Blank > MDL
Samples Prepared by 3030C
Results for Metals
RL MDL OF
5.00 0.617 25
Units
UG/L
Analyzed By:
Date Collected:
Date Received:
Matrix:
Method
6020
PSW
WATER
Date
Analyzod
7/29/2008
Flags
Reviewed By: ((~rl
MElALS XLS
31 of 34
SGSl
ICP Batch: 11977
HG Batch:
Other:
TRUE
Analyte Value
Lead 0.400
Comments
LCS
0.418
'=Out of Limits
METALS Results for LCS/LCD
LCS LCD LCD
%REC %REC
105 0.410 103
Matrix: WATER
Units: MG/L
Limit
Lower Upper
80 120
RPO RPO
Llmlr
1.93 20
NA = Not applicable, due to sample concentrat_ion greater than three times spike concentration
Reviewed By: C>;:f d
32 of 34
SC$
Lab ID: G122-3213-3
MS Lab ID: G122-3213-3
MSD Lab ID: G122-3213-3
ICP Batch: 11977
HG Batch:
Other:
Sample
Analyte Result
SA
MS
Lead 0.0831 0.400
Comments
·=out of Limits
MS
Result
0.509
MS/MSD Results for METALS
MS SA MSD
¾REC MSD Result
106 0.400 0.514 .
Analyzed By: PSW
Matrix: Water
Units: MG/L
Limit
MSD Lower Upper
¾REC
__ ,108. -_75_ --125
RPO
0.978
NA= Not applicable, due to sample concentration greater than three times spike concentration
Reviewed By: ¥-
RPO
Limit
20 ,
33 of 34
w .t,.
0 -,,
w .t,.
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• New Jersey ·'North Carolina < l • West Virginia 07 " ' www.us.sgs.com,
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Collected/Relinquished By:(1) Date Time If ecei v;Y Date Time Shipping Carrier: Samples Received Cold? (Cirde~NO ' tJ/4/) Temperature !C: 4 ,# (R i y ' ,loft Shipping licket No:
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CONFIDENTIAL: l.lie information C-Ontainc:d in this facalmile mesaag,: is confidential and-in!ended only for the use of the named recipient. ff the reader Is not the intended recipient,
please know tt:liat any dissemination, dlstribution or copy of this communication is strictly prohibited. If you have oocelved mis communication in error, please notify us immediately by
telephone and r"turn the original me!!eage ro w,, Thank you.
10 38v'd o;, !AN3 MNnm N0S<i3d 808LL559Ec 50'G0 L00c/EU/cl
Person Countv Petroleum Pro~t; .. 'Revised: I 11/19/2007 l \RESULTS
i~·li··· .. · i·Record#-Address I · · ··· I~ Map· Owne-,.-•. -.. -t-1----;..-·-·-····•·:~atas ··· --·-1---···
1 13207 1534 VirgiHna Rd. ?3-:£8 Perkins ...•.. I ! I ---··------
2 .. ,.13218 1555jViLl!Hina Rd. 73.~8 ·-----Peed ' ·,f . . . ----~---1
3 91931 157.0._Vlrgilina Rd. 73·27 ... , .. Martin ! ... -------t----,'
1
,
4 13213, 1579.~irsili.na Rd. 173-9 'oanlel ..... .. .... _-+ ____ ,._,._. ---+---......
5 · ... -9192 160§\Virgilina Rd. 73-26 Villine• i
6 15061 1605 Virollina Rd. 73-10· . . ehanev .. ·-t1-(1r-en-t-~----. ----+--........ .
,--•··· i. 10229 162~tirgihna Rd. !73-20--Solomon ! .. , ·· ··-1----+----I
···· 8L. 9088 1639 Virollina f.<~"· ,.73-11 · Watson 1 ··-····. ---'----·-
9· 6621 ... IVirgil!!Ja Rd. 73-53 Melton _ (vacantlo~ ---+------'-
10 2269.2. Vin:iilina Rd. 73-70 Holt ...• )vacant lot}. · ---t-i---1
··-··-··
1
1
2
11····· .. 3196 ,Vl,~ilinaR,f. 73~51 · Melton ,(vacantlot) ...... ···-·, 1.
. 11518 16991.Vi·rgl!inaRd. ;73•12 ,Holt .PS 10123/07 ........ ,Safe··-·
---"13'-+.--1,-1~1··04.. ., .. .1-7:14 Virgilina Rd. ·1!_3:~5 ·Meiton irrental) ""lvoc-:1-,-11"'1-=-9----,-I ....
14
1
... 9857 1719JVi!£lillna Rd. !3.:13 Wolfe IUNSAF~ (8{?9107) IVOeJ111_5,_ __ -+"1Uc..N'=S'-'Ac:,,.FE::::-J
... 1
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6
... 10942 176611/in;iilina R.d, .73-24 IMelton (("~tal) IVOC 1111~
1
, ____ . ___ ~U~NS~A~F~E'--l
14685 Viroilina Rd. 173-14 !Wolfe tvacant lot) . ,
17 .... i.5178 1771 iY.i.rgilina Rd .. :-7.3.:24:f · iWrenn 'Runts Pl~c_elold stationJ ·-··.-..
1a1· .. ·1s179 Virailina Rd, '74-12 Wrenn (va'carit lot) ' I -.. ·-·--------··
···--1~9,,--105 .. 53 1800,Virgl\lna Rd. 73•23-1 ·Eanes (Business/old station) ,voe 11115 .... UNSAFE
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_, 151771 ... !.~2_~,Yirgilina R,( .. 74•13 Wrenn P~. 1013 J ... --;'--···_··_· -+-j ----+IU':'N-'-So'A.,CFccEc--1.
,-___ , __ 1_0~939 18!_~_'Jirgilina Rd. 73-15 ..... AD. Prop. VOe 11115 . ... IUNS/\FE
22 12924 !Virgilina Rd . .!_4:22 · Garrett 1vacant lot)
f----:2~3'" · ·· · · 14769 1850 Virgilina Rd. ,73.37 Bowes .. l,~ntal) I ·c--c·-· ...,· ~·-·---+---· _·-=_-=,-·----·
.. -•~'37,~5,...' _710"'8""3-=0-···· 189\iVirg_ili~a Rd, 174-9 A. Garrett (empltv lot and well lot ----··-
___ 2_4,-..I __ 10828 1?_~9_ Vifgilina Rd. 74-14 W. Gorrett EPccS;...1-"0"'/2:c3c../0:..:7 ___ -'-__ ...... ·-· ......... UNSAFE
-_____ .251 131i~ci: 1915,Virailina R~ ·174.15 Barker .... PS 11114 ---·· I ,!UNSAFE
26 13891 1~39 Vlrgi.li~a Rd. 74-16 !Maxson PS 1.1J-'-14-'------'----+---. UNSAFE
271 .. 14_1831 1969 Viroillna Rd. ·74-17Sto~ef·.
>---2~8''-··· 19636, Virgilina Rd 7.f:.·27 ,Hend~e-rs_o_n-+,(-v-ac_a_n_t_lc-t) ____ _, __ ,..... · ·· --e---.. -·-· ...
-·-29 113571 2021 Virgiiliia.~d 74~18-Henderson , .. . .. ····-·-f----+-----1
··-·· I -+----+-----f-··. ;
--· 30. 112s;l· "T27THa;;ax-Rd ,,74~3-: .• ~• 'w_-_11,liams ··-.-.-.... -+----"-I·.·--· ..
· -·-----3; 103871-2276 Halifax:~d .. 74•8 Jones l ---,1-,,-------.---I--·, ...
31,5 ..... 9289i 2250 Halifax Rd. 74-24 • Moore L
32 9774r-1· · Halifax Rd. 174•10 Gravltte . j(ental)_l____ I --'-•. -, .. ----'-,-... -.. -... -_ ...
... _·-_--3~3~j· .. -· ·i:is'!Z., · ... 2185 l:i~lifax R.d. 74-4 16.uchanan ... voe11119 ---,.---_~.----,===-l
34 139~9' 2176 Halifa:i_Rd, 174-11 Buchanan voe 11/15 '_ !UNSAFE
---351 10~ 2165 Halifax Rd. :74.5 _J Bowes··--,VOC 11119... ----.;.. ,. -~--
.. ____ 36' 9406 .... 21271Halifax Rd_.-74-6 , .. ,Lo .... n .. n ... ·lifoe 11/15.__ .. 1 ·-· ;·--.. -+S~a-,-fe---1
.. , 37 103881 . 215o1Hailfax Rd. 74-9-1 .. !Reian PS l1./14 I I : ... I i.J1,i"sAFE·::;
38 9405. 2099,Halifax Rd. 74-7 !_Melton ioe 11115 . UNSAFE
39 14771 1, .. 1955IHalifax Rd, 73.23:3 1wtiiit"-voe 11/15 . . --,-, ---+;Uc;.NSAFE
40 ·20111 I .Halifax Rd, 73-57 °Eane,s -: .. (well location i~i 1800Vlrgillna_Rd,.).·_· --~---· ..
-......,-4"1+ · 112671 .. 1929IHalifax Rd~· 73-42 Harris ,voe 11/19 ___ _, .. · ,
-~42: 10941: 1912 Halifax Rd. ,73-23-2 ·1HaCris -· I .. · -1 ! .. ·i· £' ·
----43. 12166·1 1885,Holifax Rd, 173-22 Bass ·-· -·-·
~-·· ~-~~~~~· ·--;~~~1~:::::~ ~~: i;~!~ --1r~:: --~--~-l. -1 .....:. .;. __ ... _._··-, .-~:
.. ~:---· 17~-;HalifaxRd. 173-45· Lee =lcvacantlot) ---t---
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00 39~d 0all\N3 AlNnOJ N0Si:13d 808ll559EE
Pi.WE~~ lflSTRUCTION SHEET voe
·wA VlALS CONTAIN 1:1 HCL
OONOTRINSE
N.C. Dcpartmenl ot Heallh and Human Sen,ices
Di,·i:ilon or l'ubllc Health
SI.ale Laboratory of Public Health P.O. Bo" 2!1047, 306 N. Wilmlnelon St., Raleigt,, NC 27611-8047
· Environmental Sciences Analysis Report
Narne or O\fner, Pat~nt
Or Supply: \y,,e\ \or-, T<ltphone f (__) __________ _
Addrcs!l __ ..1.r:Xffl;Jl..:~ll,-, L..J:\.\:!JQ=l.\~i..(::::,;.s::/J...a;t.)9"-'-.!.:&ILJ... __ Counry:'.:Je..r&:::,
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Laboratory ,1\'umb~r Samo/e # Samn/e Dercrintion or Remark, R,sullS /11 071758 2-4nt?vtl 1/,'""'-l-..... ,. SEE ATTACHED S HEET(S) {,.<; v( ' ,/
D•<•Receiled: NOV 1 6 2007 Dalt Rtpor1,d: __________ _ NOV 2 8 2007
Date Extracted: __________ _ Dai. Analyud: (/~/'J--~
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~ru.AO INSTRUCTION SHE!ff,C, Department or He.Ith and Human Services Dh'islon or Public Health
SI.ale Laboratory of Public Health P.O. Box 28047,306 N. Wilmington St., RBleigh, NC 27611-8047
Environmental Sciences Analysis Report
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Name or Own.r, Pationt 1,. 1D\/\ Or Supply; ____ __,JD!,__,_,=:tt"-------Telephone IL.....) __________ _
Addr•ss: IJ l5 \1:cg;1 \,1.1)4, Rs:\
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Parson C<iunly Eovironmsn1al Health l'tl<phun, # fc._.,_1 --"92!i19'i-~S;c-!ltl!illot""'IIGl..,,...i S~l!eet...,.,,.---
Address: _____ 'aiiiiilwi~Sl~ullei'i;;C~~l-Riitiio. NC 27573
Coll•ct,d By, ____________ _
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Nov 1· t> t.UU i Ir IM All D:.ite Re<:ehcd: __________ ~1._ ~ I Uau ~pon,d:_N_O_l/_2_8_20_0_7 __ _ Date Extracied: __________ _
DH!IS Form 2l~
Ubor.uory (Rcv.06-'99) r-_;mlrpr
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DIVISION OP liEAL TB AND HUMAN SEllVIC£S
ffATEJ.AIIORATOAYOJPIJBLICHEALTll
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Environmental Sciences Analysis Report
Tel,phone # {___) ___________ _
County: Pey6<;;D
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Date Ecttr.icled:, ___________ _ DateAnalyn·d: ///'/-~
DHHS Form IJ64
Labor.atory (Kt\1.06/99)
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Environmental Sciences Analysis Report
Name of O'Wntr, P~tient
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DIVISION OF HltALTH AND HUMAN SEllVIC!:S
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Environmental Sciences Analysis Report
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VOA VIALS CONTAIN 1:1 HCL DO NOT Ri,,iSE
N.C. Department or Hullh and Human Sen-ices Dh·lsion or Public Health
SI.ale L.iboralory or Public Health P.O. Box 28047, 306 N. Wilmington St~ Raleigh, NC :27611-8047
· Environmental Sciences Analysis Report
Name of Owntr, Patient " . Or Supply: . °"'ch>~c,;N"\cc.10:L.----Telephone I(_) __________ _
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Roilioio, NC 27573
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Analysis Desired:_~',,,__ _______ _
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PO BOX 28041 ,306 N. WlLMIIIGTON' ST, llALIUGB, NC l7611
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Report to:. ____________ _ Collecttd 871 ___________ _
P.G18011 Counly Environmental Healtl Ttltphont I(_) 32S S; t,bjjiii Sbwt
Add, .. ., 8ldlD C
lbbuiD. NC 27673
T .J,poone t 13:!m .. 5'.l.c,,,,,7..i.:.· _,_17--L:'zwC.;.> _____ _
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D•t• EX1rarttd: __________ _
DHHS Form 2364
Laboratory (Rev,06/99)
p _>n!rpt
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DIVISION OJI HEALTH .lND RUMAN SltllVlCES
STATI LABORATORY OF PIJBLICHltALTH
PO BOX 28041 • 306 N. WILMINGTON ST, RA.LEICH, NC 27611
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P.O. Box 28047, 306 N. Wilmington SL, Raleigh, NC 27611-r~·t,:,.::. •.
Environment.al Sciences Analysis Report k&:a.i.. : <: [:;:;,_J l!zt. -~,~-. ",... . "°"> l
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DI\IISION OP HEALTH AND Ill/MAN SERVICES
STATl. LABORATORY OP PUBLIC HEALTH
l'Q JIOX 2~7 • 306 N, WILMINIITON ST• RALEIGH, NC 27611
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Pl.EASE READ INSTRUCTION SHE.ET Divlslo11 of Public Health
SUIIC Laboralory of f'ublit Healllt
P.O. Box 28047, 306 N. Wilmington St., Raleigh, NC 27611-8047
EnviroM1ental Sciences Analysis Report
Td•phone # (_),_~---------
County: P-iU.Ool/J
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Division or Pubhc He:altb
SI.ale Laboratory of P\lblic Health
l'EIROU.UM PliOOOCIS.
P.O. Boll 28047, 306 N. Wllmincton St~ Raleigh, NC l7611,8047
EnYironmentll Sciences Analysis Report
Telephone 112?/o l 5ot./--7v,D6
County: PJ/\,DOV\
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