NCD991278953_19990316_National Starch & Chemical Corp._FRBCERCLA SAP QAPP_SamplingAnalytical Data 1992 - 1999-OCR

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Mr. Jon K. Bornholm
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
6 I Forsyth Street, 11 'h Floor
Atlanta, Georgia 30303
• NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
March I 0, 1999
RE: Reduction in Sampling Frequency
National Starch and Chemical Company NPL Site
Salisbury, Rowan County, NC
Dear Mr. Bornholm:
The Superfund Section and the Hazardous Waste Section of the North Carolina
Department of Environment and Natural Resources (NC DENR) have reviewed
the request to reduce the groundwater sampling frequency for Operable Unit# I
(OU I) and Operable Unit #2 (OU2). The State of North Carolina concurs with
the request to change the groundwater sampling frequency for OU I and OU2 to an
annual basis, subject to the following conditions.
I. Although groundwater sampling frequency for OU I and OU2 shall
be reduced to an annual basis, groundwater level measurements for
OU I and OU2 shall continue to be conducted quarterly. These
quarterly groundwater level measurements for OU I and OU2 shall
be used to demonstrate the effectiveness of the groundwater
extraction system in maintaining hydraulic containment of the
contaminant plume. Should the quarterly groundwater level
measurements for OUI and OU2 demonstrate the lack of hydraulic
containment or off site migration of the contaminant plume,
National Starch and Chemical Corporation (NSCC) shall be
required to conduct groundwater sampling activities on a quarterly
basis as well as conduct a thorough reevaluation of the
groundwater extraction system .
401 OEIERL.IN ROAD, SUITE 150, RAL.EIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL. OPPORTUNITY/ AFFIRMATIVE ACTION EM PL.OYER -50% RECYCL.E0/1 Oo/o POST-CONSUMER PAPER
Mr. Jon Bornholm
March I 0, I 999
Page 2
•
2. Annual groundwater sampling shall continue to be conducted until such time as
all groundwater monitoring wells achieve all of the specified cleanup goals for all
constituents of concern (COC). NSCC must then conduct groundwater sampling
activities on a quarterly basis. Quarterly sampling of all groundwater monitoring
wells for all COCs shall continue until four consecutive quarterly groundwater
sampling events indicate that each COC concentration meets the specified cleanup
levels. Upon achieving the specified cleanup goals at all groundwater monitoring
wells for all COCs for four consecutive quarterly groundwater sampling events,
NSCC shall seek written approval from the NC DENR and the United States
Environmental Protection Agency (US EPA) to discontinue the groundwater
extraction system. Once written approval has been received from the NC DENR
and the US EPA, NSCC may discontinue the groundwater extraction system. At
this point, quarterly groundwater sampling shall resume at all groundwater
monitoring wells until NSCC can demonstrate that the specified cleanup goals
have been maintained for four consecutive quarterly groundwater sampling events
for all COCs. If NSCC cannot make this demonstration to the satisfaction of the
NC DENR or the US EPA, NSCC shall evaluate additional groundwater treatment
options in order to meet the specified cleanup goals for all COCs.
3. State concurrence on the change in groundwater sampling frequency for OU! and
OU2 is based solely on the information contained in attached letter. Should the
State receive new or additional information that significantly affects the
conclusions contained in the attached letter, it may modify or withdraw this
concurrence with written notice to the US EPA Region IV.
4. State concurrence on the change in groundwater sampling frequency for OU I and
OU2 in no way binds the State to concur in future decisions or commits the State
to participate, financially or otherwise, in the clean up of the site. The State
reserves the right to review, overview, comment, and make independent
assessment of all future work relating to this site.
Mr. Jon Bornholm
March I 0, 1999
Page 3
• •
The State of North Carolina appreciates the opportunity to comment on this document. If you
have any questions or comments, please feel free to call me at [phone] extension 349.
Attachment
Sincerely,
7'>J~!~-:«5 Uij~r(
fuv;d B. Mattison, CHMM /
Environmental Engineer
Superfund Section
cc: Mr. Patrick Watters, NC DENR Hazardous Waste Section
Mr. Brent Birch, NC DENR Hazardous Waste Section, Mooresville Regional Office
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Mr. Jon K. Bomholm
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
61 Forsyth Street, 11th Floor
Atlanta, Georgia 30303
• NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
March I 0, 1999
RE: Reduction in Sampling Frequency
National Starch and Chemical Company NPL Site
Salisbury, Rowan County, NC
Dear Mr. Bomholm:
The Superfund Section and the Hazardous Waste Section of the North Carolina
Department of Environment and Natural Resources (NC DENR) have reviewed
the request to reduce the groundwater sampling frequency for Operable Unit #I
(OUl) and Operable Unit #2 (OU2). The State of North Carolina concurs with
the request to change the groundwater sampling frequency for OU 1 and OU2 to an
annual basis, subject to the following conditions.
I. Although groundwater sampling frequency for OUl and OU2 shall
be reduced to an annual basis, groundwater level measurements for
OU I and OU2 shall continue to be conducted quarterly. These
quarterly groundwater level measurements for OU I and OU2 shall
be used to demonstrate the effectiveness of the groundwater
extraction system in maintaining hydraulic containment of the
contaminant plume. Should the quarterly groundwater level
measurements for OU I and OU2 demonstrate the lack of hydraulic
containment or offsite migration of the contaminant plume,
National Starch and Chemical Corporation (NSCC) shall be
required to conduct groundwater sampling activities on a quarterly
basis as well as conduct a thorough reevaluation of the
groundwater extraction system.
401 OBERLIN ROAD, SUITE ISO, RALEIGH, NC 27605
PHONE [phone] FAX 919-715•3605
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER· 50% RECYCLED/I 0% POST-CONSUMER PAPER
Mr. Jon Bornholm
March 10, 1999
Page 2
•
2. Annual groundwater sampling shall continue to be conducted until such time as
all groundwater monitoring wells achieve all of the specified cleanup goals for all
constituents of concern (COC). NSCC must then conduct groundwater sampling
activities on a quarterly basis. Quarterly sampling of all groundwater monitoring
wells for all COCs shall continue until four consecutive quarterly groundwater
sampling events indicate that each COC concentration meets the specified cleanup
levels. Upon achieving the specified cleanup goals at all groundwater monitoring
wells for all COCs for four consecutive quarterly groundwater sampling events,
NSCC shall seek written approval from the NC DENR and the United States
Environmental Protection Agency (US EPA) to discontinue the groundwater
extraction system. Once written approval has been received from the NC DENR
and the US EPA, NSCC may discontinue the groundwater extraction system. At
this point, quarterly groundwater sampling shall resume at all groundwater
monitoring wells until NSCC can demonstrate that the specified cleanup goals
have been maintained for four consecutive quarterly groundwater sampling events
for all COCs. If NSCC cannot make this demonstration to the satisfaction of the
NC DENR or the US EPA, NSCC shall evaluate additional groundwater treatment
options in order to meet the specified cleanup goals for all COCs.
3. State concurrence on the change in groundwater sampling frequency for OU I and
OU2 is based solely on the information contained in attached letter. Should the
State receive new or additional information that significantly affects the
conclusions contained in the attached letter, it may modify or withdraw this
concurrence with written notice to the US EPA Region IV.
4. State concurrence on the change in groundwater sampling frequency for OU I and
OU2 in no way binds the State to concur in future decisions or commits the State
to participate, financially or otherwise, in the clean up of the site. The State
reserves the right to review, overview, comment, and make independent
assessment of all future work relating to this site.
Mr. Jon Bornholm
March I 0, 1999
Page 3
•
The State of North Carolina appreciates the opportunity to comment on this document. If you
have any questions or comments, please feel free to call me at [phone] extension 349.
Attachment
Sincerely,
7'>J f3>/l?::tc5 I O 1✓~P(
fuv;d B. Mattison, CHMM
Environmental Engineer
Superfund Section
cc: Mr. Patrick Watters, NC DENR Hazardous Waste Section
Mr. Brent Birch, NC DENR Hazardous Waste Section, Mooresville Regional Office
• • UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 4
4WD-NSMB
Mr. Dave Mattison
ATLANTA FEDERAL CENTER
61 Forsyth Street, S.W.
Atlanta, Georgia 30303-3104
March 2, 1999
North Carolina Department of Environment and
Natural Resources/Superfund Section
Suite 150
401 Oberlin Road
Raleigh, NC 27605
RECEIVED
MAR O 8 1999
SUPERFUND SECTION
SUBJ: Review Letter Requesting Concurrence to Reduce Sampling Frequency for
Operable Units #1 and #2 at the National Starch & Chemical Company
Superfund Site
Dear Mr. Mattison:
~nclosedfcir the'North Carolina.Department of Environment.and Natural
Resources information, review, and Site file is a copy of the above referenced
correspondence, dated March 2, 1999. Please review this letter. The Agency would
appreciate receiving either the State's comments and/or concurrence by Monday,
March 8, 1999. If the State is unable to make this deadline, please inform me as to
when the Agency can expect to receive a response for the State.
If you have any questions, I can be reached at 404-562-8820.
Sincerely,
Jon K. Bornholm
Remedial Project Manager
Enclosure ( 1)
1. ; . • ' ' : • , • . • ~' I ; ' . -• '-.:, Copy of Letter Requesting Concurrence toR!3duce,Samplii1g Frequency for
Operable Units #1 and #2 at the National Starch & Chemical Company ·
Superfund Site
,, ~lAR-02-1999 13 : 54
BBL 8LAAAM:l, LIQJCK & L;f, lr,,c.
engineers & !cienfl!f!
BBL -NJ OFFICE
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Transmitted Vi" Certified J,,fail/Retunr _Rectipt Requested -c.: ... .:.. ::~·.::nn. ))~I:~-"~·: ~n·i.:; :,::.
Man:h 2, 1999 ,, . ' ........
~·. -. Mr. Jon K. Bornholm ' J:·· · r.::-;,\•; ,=;•.,'.\SJ
Remedial Project Manage(. i.,fF .. . .,;,:
United States Environmental Protection Agency ·
Atlanta Federal Center '
61.Forsyth Street, S.W.'1:: ,\\;':
Atlanta, GA30303 3104' "''
Re: R,duction in Sampling Frequency
Cedar Springs Road Plant Site
Salisbury, North Carolina
Project#: 050.55 #2
Dear Mr. Bornholm:
609 860 8007 P.02 •
On behalf of National Starch & Chemical Company (NSCC), Bl03lnnd, Bouck & Lee, Inc. (DDL) ha.:s
prepared this petition to reduce the ground-water sampling frequency for Operable Units One and Two
(OUJ '"1d OU2) ai:i.J,~ C<:tlalSp"riiigsRuiJ,rPlai'il'Sil~ located'in Satisbuiy}North Carolina.· This petition
is being prepared per the United Srates Environmental Protection Agency's (USEPA's) request in their
February 9, 19':19 comment letter on the Third Quarter 1998 OU! and OU2 Monitoring Report (BBL,
December 1998). A separate petition regarding a change in the cUITent laboratory anal}iical methods was
also requested by the USEPA and will be submitted to the USEPA shortly.
Ground-water sampling has been conducted on a quarterly basis for the 18 OU! and OU2 monitoring and
extraction wells sampled from first quarter 1993 through fourth qu:u-ter 1998. NSCC fa proposing to
change the sampling frequency from the current quarterly basis to an annual basis based on the technical
discussion prcx.nted in the following doL.umeu~.
• the Ground-Water Data Evaluation for Plume Periphery and Trench Area Extraction Wells
(BBL, August 1998) submitted as an attachment to the Operable Unit Two Five-Year Review
(BBL, August 1998); and
• the cover correspondence dated December 21, 1998 for the Third Quarter i998 OUl and OU2
Mnni1·0ring: Re.port.
The technical evaluation pre3entcd in these docum,nts indicates:
.:ulk:cliou uf2 I ruunds ofquanerly data ftom t1rs1 quaner 1993 through second quarter !998
have been sufficient to identify conc~ntration trends for ground-water constituents of concern
{LUCS)'.
8 South Riv.,,-Rood • Crorbury, NJ 0B512·9502
tc: (C>O') UO 06?0 • Voice Mail (60i) 860 8072 • Fox (Wt) BoO 041?1 • Office~ ~latlor.wido
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, . .;;_ MAR-02-1999 13: 55 BBL -NJ OFFICE 609 860 8007 P.03
•
•
•
•
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Mr. Joii K. Bumholm, ·
:·:March 2, 1999
!:'age 2·of2
, - . conc:l!Yl'tions !)f:}lle groun.d0w~ter COCs':ii~ve been s~;ady from quarter to quarter
with~iit:rapid chru,!ges'in concentrations thilt.v.·ould require quarterly. monitoring; and
no seasonal trends were identified for any of the ground~water COCs. ·
data ccllected:in sampling.events conducted subsequent to the data evaluation are consistent
with tha prio-6futn o.nd the -c·oc concentration trends;·
~-.~ ~~ '
Lite ubscrvec:mdy trend of the dataols likely due to the hydrogeologic setting at the site (low ,
conductivity:nfaterials).and the effectiveness•·of,the Trench. Area Ex.traction System· at
controlling' g"round-waier flow and COC migration off site;
_:~· monitoriiig.,progrrun,~as established for the OU2 monitoring and extraction wells (Trench
.. Area Wellsrin the 1991 RemP;lial D.-sigo/Performance Monitoring Work Plan for O'U2 (IT,
1993), which was approvcd·by the USEPA. This approved monitoring plan specified quarterly
sampling for the first two yC11n nftcr Work Plan approval and mo11ituri111, uu a five-year
frequency starting in the fifth year after Work Plan approval; and
there is no USEPA-approved document which specifies a long-tenn sampling frequency for the
OU I morutoring and extraction wells; As indicated in the December 21, 1998 correspondence,
BBL is preparing an Operable Unit One Plume Periphery Well Remedy Evaluation Plan for
submittal to the USEPA by April !, 1999. This.plan will include a sampling program for
monitoring and extraction wells in the vir.inity of the Plume Periphery Wells.
If you have ·any qu~stions or comments reg,,nling thiG petition, please do not he,itate to c.ontact me at (609)
860-0590,
Sincerely,
BLASLA1''D, BOUCK & LEE, INC. 0c_ ___ _
Michael P. Fleischner
Seninr Projec.t Engineer
MPF\cml
a:\0~4!111\17,WPO
cc: Mr. Douglas E. Cregar, National Starch & Chemical Company
Mr. Alex S:mrno11, Naticnal Starch & Chemical CQmpany
Ms. Angela Dohl, National Srarch & Chemical Company
Mr. Rici,~,<.! D. FnmkliJ~ NHtional Siarch & Chemical Company
Mr. Joseph J. Hochrciter, Blasland, Bouck & Lee, Inc.
BLASLAND, BOUCK & LEE. INC.
-e;:; i,); n e er s & sci en t I$ i$
TOTAL P.03
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£.'
• • UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
4WD-NSRB
Mr. Bruce Nicholson
Superfund Section
345 COURTLAND STREET. N.E.
ATLANTA, GEORGIA 30365
August 29, 1994
North Carolina Department of Environment,
Health & Natural Resources
Suite 150
401 Oberlin Road
Raleigh, North Carolina 27605
RECE!VED
SEP 2 1994
!'\UPERFUND SECTION I
SUBJ: Analytical Data for Private Wells Sampled in July-August
1992 Timeframe in Conjunction to the National Starch &
Chemical Company Superfund Site
Dear Mr. Nicholson:
I was informed by Barbara Benoy, . -the preceding RPM for the
National Starch & Chemical Company (NSCC) Superfund site, that
only the State and NSCC collected samples during the July-August
1992 drinking water sampling effort. Therefore, the Agency does
not have any data from this effort. I passed this information on
to Mr. Javis Arey in Salisbury. I also informed him that I would
request that the State send him the data on the samples you
collected. I would appreciate it if you would also send me a
copy of the data as well. Mr Arey address is as follows:
Mr. Javis M. Arey
625 Catawba Road
Salisbury, NC 28144
And if you need it, his telephone number is [phone].
If you have any questions, please contact me at (404) 347-
7791 x-4106.
Sincerely yours,
. lro, t. W,_ ~
~~'. K > Bornho{m · ·
Remedial Project Manager
• • UNITED STATES ENVIRONMENTAL PROT CTION AGENCY
REGION IV
34e COURTLAND STRE.'.E:'r, N.E:,
ATLANTA, Gl!.ORGI/\ 30366
April 2n. 1994
CJP'l'10N/d ,:'(ikr.~lg<:) 17.,:io:
FA X t R A N S M I TT A L • 01 r,,,,.,, • /
4WD-NCI\S
Mr. Hank Graul1oh
National starch & Chemical company 10 Finderne Avenue
Bridgewater, Naw'Jeraey 08807
SUBJ, Apr11 14;; 1994 Correspondence from IT Corpe ation on "Evaluation of tiAfili·Jfy.i:i.ila'llt;i,..l!ID!?,for Evidence of Natural Biodegradation of 1, 2-Pichloroethane"
Dear Mr. Graulioh1
In reviewing the above referenced correaponde ce, it became evident that IT Corporation only diecusaed the analytical data btainad from the analyse& of groundwater aamplea. Did IT Corporation review the analytical data for aoil samples for the presence of chloroethana? If ao, what was their conoluaion?
It ie more important that the soil data show vidence of biodegradation then the groundwater data as Operable Unit #4 addr aaea the soil contamination in and around Area 2 and the wastewater treatment agoon area, If there is a complete absence of ohloroethane in the soil aampl~s, what ia this an indication of? This quaetion needs to be addreeaa~ in order to support the statement oonveyed at the top of page 3-3 in the F<tbruary 7, 1994 Draft Feasibility Study Report for Operable Unit #4, This sentence states, "The 1, 2-DCA concentration in plant area soile a.re eati.tl,ated to degrade to lees than 7 ppm in 5 to 10 years and less than l ppb wil!h 35 years," If thiB statement can be substantiate, NSCC would have a vQry strong argument to support the seleotion of Alterative S2 -rnatitutidnal Controls,
If you have any questions, please call ma at (1404 )347-7791,
Sinoerely yours, I
cc; Bruce-Nioholaon, NCDEHNk Alex Samaon, NSCC
Ml.aha.al Sturdevant , IT
jnl ~
Jon K. Bornholm
Remedial l'i:ojeot anager
i
ll
4WD-NCRS
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
345 COURTLAND STREET. N.E.
ATLANTA. GEORGIA 30365
April 14, 1994
Mr. Hank Graulich
National Starch & Chemical Company
10 Finderne Avenue
Bridgewater, New Jersey 08807
APR 1 9 1994
SUPERFUNO St:CTION
SUBJ: Response to Facsimile on Soil Boring and Purged Water
Drums from Well Installation at the National Starch &
Chemical Company Superfund Site
Dear Mr. Graulich:
The Agency received your facsimile referenced above on April
11, 1994. After reviewing this facsimile, the original submittal
entitled "Management Plan for Investigation-Derived Wastes"
prepared by IT Corporation on February 19, 1993, and the Agency's
comments on the February 19, 1993 submittal, the following items
needed to be addressed.
1. Since the approaches vary considerably for dealing with the
drummed soils, which document, the April 11, 1994 or the
February 19, 1993, takes.precedence.
2. The April 11 submittal lacks the following specifics:
a) Item #2: How long will it take to empty all the drums?
b) Item #2, the last two sentences: These two sentences
deal with the disposal of the drummed soils after
testing, however, the frequency the soil samples will
be collected is not specified. Are soil samples to be
collected from each drum? Are the contents of two
drums to be composited and then tested? Are the
contents of three (etc.) drums to be composited and
then tested?
c) Item #2: How long after removing the soil from any
particular drum will the soil sample, to represent that
drum's content, be collected for analysis?
d) Item #2: The February 19 submittal discussed
segregating the drums according to area of the Site the
,
2
soils where generated (i.e., Trench Area and elsewhere). Is this approach still to be taken?
e) Item #2: The February 19 submittal discussed conducting TCLP VOA, TCLP BNA, and TCLP metals analyses. Is this still the case?
f) Will the concrete pad be decontaminated after this effort? If so, how and what will be done with the washwater?
g) Item #3: Will the drum's lid be removed to allow sampling the head space with the OVA? Or will the OVA probe enter the head space through the bunghole?
i) The language in this Item needs to be alter to state that OVA probe will be inserted into the head space upon opening the drum so that several minutes will not elapse after exposing the head space to the atmosphere before the OVA reading is taken.
The above items need to be addressed prior to the Agency's approval for dealing with the investigation-derived wastes.
If you have any questions, please call me at [phone].
cc: Bruce Nicholson, NCDEHNR
Alex Samson, NSCC
Sincerely yours, t f (Jp✓. (__---
Jon K. Bornholm
Remedial Project Manager
• •
rn INTERNATIONAL •. TECHNOLOGY CORPORATION
TO
312 DIRECTORS DRIVE
KNOXVILLE. TENNESSEE 37923
[phone]
8orbor:-a lien /4
WE ARE SENDING YOU
OF TRANSMITTAL
CATE
ATTENTION
SUBJECT
~ached □ Under separate cover via _________ the following items:
0 Flow sheets
□ Shop drawings
D Copy at letter
COPIES DATE
□ P & 10
□ Prints
□ Change order
NO
THESE ARE TRANSMITTED as checked below:
□ For approval
□ For your use
~equested
□ Approved as submitted
C Approved as noted
□ Returned for corrections
□ For review & comment □
□
□ Plans □ Samples 0 Specifications
□
0 Resubmit __ copies for approval
□ Submit __ copies for distribution
□ Return __ corrected prints
□ FOR BIOS DUE ---~----------19 ___ 0 PRINTS RETURNED AFTER LOAN TO US REMARKS ___________________________________________ _
COPIES TO: ___________________ _
m INTERNATIONAL
TECHNOLOGY
CORPORATION
IT Corporation
312 Directors Drive
Knoxville, TN 37923
Attn: Mike Sturdevant
• ANALYTICAL
SERVICES
,:·=::-\: :,\-< .. /}-:-~ .,_, . . ~
"""~.
•
. I • ·' January 6, 1993
Job Number: ITEK 52659 r~"-~' I(~""' \\\ ~-r0\\ ,,~~ P.p. Number: 408668.09.62
This is the Certificate of Analysis for the following samples:
Client Project ID:
Date Received by Lab:
Number of Samples:
Sample Type:
I. Introduction
National Starch
10/24/92
Six (6)
Water
On 10/24/92, six (6) water samples arrived at the ITAS-Knoxville, Tennessee, laboratory from IT
Corporation, Knoxville, Tennessee in support of the National Starch project. The list of analytical tests
performed, as well as date of receipt and analysis, can be found in the attached report.
II. Analytical Results/Methodology
The analytical results for this report are presented by analytical test. Each set of data will include sample
identification information and the analytical results. Please note that the data are not blank corrected.
The samples were analyzed for Target Compound List (TCL) semivolatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
The samples were analyzed for Target Analyte List (T AL) metals by cold vapor atomic absorption
spectroscopy (CV AA), graphite furnace atomic absorption spectroscopy (GFAA), and inductively coupled
plasma spectroscopy (ICP) in accordance with the EPA CLP ILM0I Statement of Work.
Revie ed and roved:
. (.,,
Alyc . Moore
Laboratory Manager
Arnenr:on Council ot Independent Laboratones
!nterr,:::tionol /"1..Ssoc,at1on ol En'11ronmental T-::sl1ng Icboratones
.:-..me neon 1\ssoc101ion for Laborator·/ Accr":::d!tat,on
IT Analytical Services, 5815 Middlebrook Pike, Knoxville, TN 37921 681·1-89
IT Corporation
January 6, 1993
Client Project ID: National Starch
ill. Quality Control
•
Routine laboratory level I QC was followed.
.IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
The semivolatiles analyses were performed by direct injection of sample extract on a Restek XTI-5
capillary column on a Fisons VG-TRIO-I GC/MS/DS. The sample analyses went well. There were no
problems seen in final data review.
The samples were digested on 11/03/92 for ICP and for GFAA. The samples for mercury analysis were
prepared just prior to analysis. The CV AA analysis for mercury was performed on 11/12/92; the GFAA
analyses for arsenic, lead, selenium, and thallium were performed from 11/12 through 11/16/92; the
remaining metals were analyzed by ICP on 11/16/92. All run QC was acceptable. Slightly elevated
detection limits for lead were reported for sample Well #1. Elevated detection limits for selenium were
reported for all samples except Well #1 due to matrix interferences. No other problems were encountered.
2
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
Client Sample ID: Well #1
Lab Sample ID: Wl739
ComQound
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
benzyl alcohol
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ether
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
benzoic acid
SEMIVOLATILE TARGET COMPOUND UST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
10 u bis(2-chloroethoxy)methane
10 u 2,4-dichlorophenol
10 u 1,2,4-trichlorobenzene
10 u naphthalene
10 u 4-chloroaniline
10 u hexachlorobutadiene
10 u 4-chloro-3-methylphenol
10 u 2-methylnaphthalene
10 u hexachlorocyclopentadiene
10 u 2,4,6-trichlorophenol
10 u 2,4,5-trichlorophenol
10 u 2-chloronaphthalene
10 u 2-nitroaniline
10 u dimethyl phthalate
10 u acenaphthylene
10 u 2,6-dinitrotoluene
50 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
3
Concentration
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
IT Corporation
January 6, I 993
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND UST (continued)
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #I
Lab Sample ID: Wl739
Com(!OUnd Concentration Compound
3-nitroaniline 50 u anthracene
acenaphthene IO u di-n-butylphthalate
2,4-dinitrophenol 50 u fluoranthene
4-nitrophenol 50 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2, 4-dini trotol uene IO u 3 ,3 '-dichlorobenzidine
diethylphthalate IO u benzo(a)anthracene
4-chlorophenyl-phenylether IO u chrysene
tluorene 10 u bis(2-ethylhexyl)phthalate
4-nitroaniline 50 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 50 u benzo(b )fluoranthene
n-nitrosodiphenylamine1 IO u benzo(k)fluoranthene
4-bromophenyl-phenylether 10 u benzo(a)pyrene
hexachlorobenzene 10 u indeno(l ,2,3-cd)pyrene
pentachlorophenol 50 u di benzo( a, h )anthracene
phenanthrene 10 u benzo(g, h, i)pery lene
U Compound was analyzed for but not detected. The number is the detecti~n limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
I0/28/92
11/04/92
1.0
4
Concentration
10 u
10 u
10 u
10 u
IO u
20 u
IO u
10 u
10 u
10 u
IO u
10 u
10 u
IO u
10 u
10 u
IT Corporation
January 6, 1993 • .T ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
Client Sample ID: Well #5
Lab Sample ID: Wi740
ComQound
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
benzyl alcohol
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ether
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
benzoic acid
SEMIVOLATILE TARGET COMPOUND LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
10 u bis(2-chloroethoxy)methane
10 u 2,4-dichlorophenol
10 u 1,2,4-trichlorobenzene
10 u naphthalene
10 u 4-chloroaniline
10 u hexachlorobutadiene
10 u 4-chioro-3-methylphenol
10 u 2-methylnaphthalene
10 u hexachlorocyclopentadiene
10 u 2,4,6-trichlorophenol
10 u 2,4,5-trichlorophenol
10 u 2-chloronaphthalene
10 u 2-nitroaniline
10 u dimethyl phthalate
10 u acenaphthylene
10 u 2,6-dinitrotoluene
50 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
I i/04/92
1.0
5
Concentration
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
IT Corporation
January 6, 1993
Client Project ID: National Starch
• • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in /Lg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #5
Lab Sample ID: Wl740
ComQound Concentration Compound
3-nitroaniline 50 u anthracene
acenaphthene 10 u di-n-butylphthalate
2,4-dinitrophenol 50 u fluoranthene
4-nitrophenol 50 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2,4-dinitrotoluene 10 u 3 ,3 '-dichlorobenzidine
diethylphthalate 10 u benzo(a)anthracene
4-chlorophenyl-phenylether 10 u chrysene
fluorene 10 u bis(2-ethylhexyl)phthalate
4-nitroaniline 50 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 50 u benzo(b)fluoranthene
n-nitrosodiphenylamine1 10 u benzo(k)fluoranthene
4-bromophenyl-phenylether 10 u benzo(a)pyrene
hexachlorobenzene 10 u indeno( 1,2,3-cd)pyrene
pentachlorophenol 50 u dibenzo(a,h)anthracene
phenanthrene 10 u benzo(g,h, i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
6
Concentration
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
Client Sample ID: Well #12
Lab Sample ID: Wl741
ComQound
phenol
bis(2-chloroethyl)ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
benzyl alcohol
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ether
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
benzoic acid
SEMIVOLATILE TARGET COMPOUND LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
IO u bis(2-chloroethoxy)methane
IO u 2,4-dichlorophenol
10 u 1,2,4-trichlorobenzene
IO u naphthalene
IO u 4-chloroaniline
10 u hexachlorobutadiene
IO u 4-chloro-3-methylphenol
IO u 2-methylnaphthalene
IO u hexachlorocyclopentadiene
10 u 2,4,6-trichlorophenol
10 u 2,4,5-trichlorophenol
10 u 2-chloronaphthalene
IO u 2-nitroaniline
IO u dimethyl phthalate
IO u acenaphthylene
10 u 2,6-dinitrotoluene
52 u
U Compound was analyzed for but not detected, The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
LO
7
Concentration
IO u
IO u
IO u
10 u
IO u
IO u
IO u
IO u
IO u
IO u
52 u
10 u
52 u
10 u
10 u
IO u
IT Corporation
January 6, 1993
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE. TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #12
Lab Sample ID: Wl741
Compound Concentration Compound
3-nitroaniline 52 u anthracene
acenaphthene 10 u di-n-butylphthalate
2,4-dinitrophenol 52 u fluoranthene
4-nitrophenol 52 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2,4-dinitrotoluene 10 u 3 ,3 '-dichlorobenzidine
diethylphthalate 10 u benzo(a)anthracene
4-chlorophenyl-phenylether 10 u chrysene
fluorene 10 u bis(2-ethylhexyl)phthalate
4-nitroaniline 52 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 52 u benzo(b)fluoranthene
n-nitrosodiphenylamine1 10 u benzo(k)fluoranthene
4-bromophenyl-phenylether 10 u benzo(a)pyrene
hexachlorobenzene 10 u indeno( 1,2,3-cd)pyrene
pentachlorophenol 52 u dibenzo(a,h)anthracene
phenanthrene 10 u benzo(g,h, i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
8
Concentration
10 u
10 u
10 u
10 u
10 u
21 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
Client Sample ID: Well #14
Lab Sample ID: Wl742
Com11ound
phenol
bis(2-chloroethy I )ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
benzyl alcohol
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ether
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
benzoic acid
SEMlVOLATILE TARGET COMPOUND LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
II u bis(2-chloroethoxy)methane
II u 2,4-dichlorophenol
II u 1,2,4-trichlorobenzene
II u naphthalene
11 u 4-chloroaniline
11 u hexachlorobutadiene
11 u 4-chloro-3-methylphenol
11 u 2-methylnaphthalene
I I u hexachlorocyclopentadiene
11 u 2,4,6-trichlorophenol
11 u 2,4,5-trichlorophenol
11 u 2-chloronaphthalene
11 u 2-nitroaniline
11 u dimethyl phthalate
11 u acenaphthylene
11 u 2,6-dinitrotoluene
56 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
1 ]/04/92
1.0
9
Concentration
II u
11 u
II u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
56 u
11 u
56 u
11 u
11 u
11 u
IT Corporation
January 6, 1993
Client Project ID: National Starch
• • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #14
Lab Sample ID: Wl742
Compound Concentration Compound
3-nitroaniline 56 u anthracene
acenaphthene 11 u di-n-butylphthalate
2,4-dinitrophenol 56 u fluoranthene
4-nitrophenol 56 u pyrene
dibenzofuran 11 u butylbenzylphthalate
2,4-dinitrotoluene II u 3 ,3 '-dichlorobenzidine
diethylphthalate 11 u benzo(a)anthracene
4-chlorophenyl-phenylether 11 u chrysene
tluorene 11 u bis(2-ethylhexyl)phthalate
4-nitroaniline 56 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 56 u benzo(b )fluoranthene
n-nitrosodiphenylamine1 11 u benzo(k)fluoranthene
4-bromophenyl-phenylether 11 u benzo(a)pyrene
hexachlorobenzene 11 u indeno( 1,2,3-cd)pyrene
pentachlorophenol 56 u dibenzo(a,h)anthracene
phenanthrene 11 u benzo(g,h, i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
IO
Concentration
11 u
11 u
11 u
11 u
I I u
22 u
11 u
11 u
II u
II u
I 1 u
11 u
11 u
11 u
11 u
I 1 u
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND UST
Results in l'g/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #16
Lab Sample ID: Wl743
Compound Concentration Compound
phenol 10 u bis(2-chloroethoxy)methane
bis(2-chloroethyl)ether 10 u 2,4-dichlorophenol
2-chlorophenol 10 u 1,2,4-trichlorobenzene
1,3-dichlorobenzene 10 u naphthalene
1,4-dichlorobenzene 10 u 4-chloroaniline
benzyl alcohol 10 u hexachlorobutadiene
1,2-dichlorobenzene 10 u 4-chloro-3-methylphenol
2-methylphenol 10 u 2-methylnaphthalene
bis(2-chloroisopropyl)ether 10 u hexachlorocyclopentadiene
4-methylphenol IO u 2,4,6-trichlorophenol
n-nitr?so-di-n-propylamine 10 u 2,4,5-trichlorophenol
hexachloroethane 10 u 2-chloronaphthalene
nitrobenzene 10 u 2-nitroaniline
isophorone 10 u dimethyl phthalate
2-nitrophenol 10 u acenaphthylene
2,4-dimethylphenol 10 u 2,6-dinitrotoluene
benzoic acid 50 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
l l/04/92
1.0
11
Concentration
IO u
IO u
IO u
IO u
IO u
10 u
IO u
IO u
10 u
IO u
50 u
10 u
50 u
10 u
10 u
10 u
IT Corporation
January 6, I 993
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #16
Lab Sample ID: W1743
Com12ound Concentration Compound
3-nitroaniline 50 u anthracene
acenaphthene 10 u di-n-butylphthalate
2,4-dinitrophenol 50 u fluoranthene
4-nitrophenol 50 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2,4-dinitrotoluene 10 u 3,3 '-dichlorobenzidine
diethylphthalate 10 u benzo(a)anthracene
4-chlorophenyl-phenylether 10 u chrysene
fluorene 10 u bis(2-ethylhexyl)phthalate
4-nitroaniline 50 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 50 u benzo(b )fluoranthene
n-nitrosodiphenylamine1 10 u benzo(k)fluoranthene
4-bromophenyl-phenylether 10 u benzo(a)pyrene
hexachlorobenzene 10 u indeno( 1,2,3-cd)pyrene
pentachlorophenol 50 u dibenzo(a,h)anthracene
phenanthrene 10 u benzo(g,h,i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
12
Concentration
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
Client Sample ID: Well #28
Lab Sample ID: Wl744
Com12ound
phenol
bis(2-chloroethy I )ether
2-chlorophenol
1,3-dichlorobenzene
1,4-dichlorobenzene
benzyl alcohol
1,2-dichlorobenzene
2-methylphenol
bis(2-chloroisopropyl)ether
4-methylphenol
n-nitroso-di-n-propylamine
hexachloroethane
nitrobenzene
isophorone
2-nitrophenol
2,4-dimethylphenol
benzoic acid
SEMIVOLATILE TARGET COMPOUND LIST
Results in l'g/liter (ppb)
Sample Matrix: Water
Concentration Compound
IO u bis(2-chloroethoxy)methane
IO u 2,4-dichlorophenol
IO u 1,2,4-trichlorobenzene
IO u naphthalene
IO u 4-chloroaniline
IO u hexachlorobutadiene
IO u 4-chloro-3-methylphenol
IO u 2-methylnaphthalene
IO u hexachlorocyclopentadiene
IO u 2,4,6-trichlorophenol
10 u 2,4,5-trichlorophenol
IO u 2-chloronaphthalene
IO u 2-nitroaniline
IO u dimethyl phthalate
IO u acenaphthylene
IO u 2,6-dinitrotoluene
50 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
13
Concentration
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
50 u
IO u
50 u
IO u
IO u
IO u
IT Corporation
January 6, 1993
Client Project ID: National Starch
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #28
Lab Sample ID: WI744
Compound Concentration Compound
3-nitroaniline 50 u anthracene
acenaphthene IO u di-n-butylphthalate
2,4-dinitrophenol 50 u fluoranthene
4-nitrophenol 50 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2,4-dinitrotoluene IO u 3 ,3 '-dichlorobenzidine
diethylphthalate IO u benzo(a)anthracene
4-chlorophenyl-phenylether 10 u chrysene
fluorene IO u bis(2-ethylhexyl)phthalate
4-nitroaniline 50 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 50 u benzo(b )fluoranthene
n-nitrosodiphenylamine1 IO u benzo(k)fluoranthene
4-bromophenyl-phenylether IO u benzo(a)pyrene
hexachlorobenzene IO u indeno( 1,2,3-cd)pyrene
pentachlorophenol 50 u dibenzo(a,h)anthracene
phenanthrene IO u benzo(g,h,i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
Dilution Factor:
10/28/92
11/04/92
1.0
14
Concentration
10 u
IO u
IO u
IO u
IO u
20 u
IO u
IO u
IO u
IO u
10 u
IO u
IO u
IO u
IO u
IO u
IT Corporation
January 6, 1993 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND UST
Results in l'g/liter (ppb)
Sample Matrix: Water
Client Sample ID: Method Blank
Lab Sample ID: H2173
Compound Concentration Compound
phenol IO u bis(2-chloroethoxy)methane
bis(2-chloroethyl)ether IO u 2,4-dichlorophenol
2-chlorophenol IO u 1 ,2,4-trichlorobenzene
1,3-dichlorobenzene IO u naphthalene
1,4-dichlorobenzene IO u 4-chloroaniline
benzyl alcohol IO u hexachlorobutadiene
1,2-dichlorobenzene IO u 4-chloro-3-methylphenol
2-methylphenol IO u 2-methylnaphthalene
bis(2-chloroisopropyl)ether IO u hexachlorocyclopentadiene
4-methylphenol IO u 2,4,6-trichlorophenol
n-nitroso-di-n-propylamine IO u 2,4,5-trichlorophenol
hexachloroethane IO u 2-chloronaphthalene
ni trobenzene IO u 2-nitroaniline
isophorone IO u dimethyl phthalate
2-nitrophenol IO u acenaphthylene
2,4-dimethylphenol IO u 2,6-dinitrotoluene
benzoic acid 50 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Extraction:
Date of Analysis:
10/28/92
11/04/92
15
Concentration
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
IO u
50 u
IO u
50 u
IO u
IO u
IO u
IT Corporation
January 6, I 993
Client Project ID: National Starch
• • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
SEMIVOLATILE TARGET COMPOUND LIST (continued)
Results in l'g/liter (ppb)
Sample Matrix: Water
Client Sample ID: Method Blank
Lab Sample ID: H2173
Com12ound Concentration Compound
3-nitroaniline 50 u anthracene
acenaphthene 10 u di-n-butylphthalate
2,4-dinitrophenol 50 u fluorantbene
4-nitrophenol 50 u pyrene
dibenzofuran 10 u butylbenzylphthalate
2,4-dinitrotoluene 10 u 3 ,3 '-dichlorobenzidine
diethylphthalate 10 u benzo( a )anthracene
4-chlorophenyl-phenylether 10 u chrysene
fluorene 10 u bis(2-ethylhexyl)phthalate
4-nitroaniline 50 u di-n-octylphthalate
4,6-dinitro-2-methylphenol 50 u benzo(b )fluoranthene
n-nitrosodiphenylamine1 10 u benzo(k)fluoranthene
4-bromophenyl-phenylether 10 u benzo(a)pyrene
hexachlorobenzene 10 u indeno( 1,2,3-cd)pyrene
pentachlorophenol 50 u dibenzo(a,h)anthracene
phenanthrene 10 u benzo(g,h,i)perylene
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Detected as diphenylamine.
Date of Extraction:
Date of Analysis:
10128192
11/04192
16
Concentration
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
IT Corporation
January 6, 1993 •
Client Project ID: National Starch
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
WATER SURROGATE PERCENT RECOVERY SUMMARY
SEMI-VOLATILE
2,4,6-
Nitro-2-Fluoro-Terphenyl-2-Fluoro-Tribromo-
Benzene-D5 Biphenyl D14 Phenol-D5 Phenol Phenol
Client Samgle ID (35-114%)* (43-116%)* (33-141 %)* (10-94%)* (21-100%)* (10-123%)*
Well #1 70 78 83 27 46 72
Well #12 67 78 80 32 54 74
Well #14 65 74 79 32 56 76
Well #16 69 76 78 30 51 73
Well #28 69 76 79 30 52 70
Well #5 64 74 77 31 52 79
Method Blank 75 76 89 34 60 72
*Values in parentheses represent required QC limits.
17 \REC\2C. FRM
IT Corporation
January 6, 1993 •
Client Project ID: National Starch
Client Sample ID: Method Blank
Lab Sample ID: PBWC5355/PBWII 126
Comgound
aluminum
antimony
arsenic
barium
beryllium
cadmium
calcium
chromium
cobalt
copper
iron
lead
Date of Digestion: 11/03/92
METALS TARGET ANALYTE LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
40.000 u magnesium
30.000 u manganese
2.000 u mercury
2.000 u nickel
1.000 u potassium
5.000 u selenium
-66.550 B silver
10.000 u sodium
20.000 u thallium
10.000 u vanadium
11.530 B zinc
2.000 u
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), 11/12/92 (CVAA)
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVIUE, TN
Job Number: ITEK 52659
Concentration
30.000 u
2.000 u
0.200 u
20.000 u
1,000.000 u
2.000 u
5.000 u
-209.410 B
2.000 u
10.000 u
5.550 B
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
18 \METALSITAL.FRM 4113192
IT Corporation
January 6, 1993 •
Client Project ID: National Starch
METALS TARGET ANALYTE UST
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well #1
Lab Sample ID: Wl745
Compound Concentration Compound
aluminum 40.0 u magnesium
antimony 30.0 u manganese
arsenic 2.0 u· mercury
barium 73.7 B nickel
beryllium 1.0 u potassium
cadmium 5.0 u selenium
calcium 21,200 silver
chromium 10.0 u sodium
cobalt 20.0 u thallium
copper 10.0 u vanadium
iron 51.9 B zinc
lead 4.0 u
Date of Digestion: 11/03/92
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GPAA), 11/12/92 (CVAA)
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
11,800
2.0 u
0.20 u
20.0 u
1,410 B
2.0 u
5.0 u
6,620
2.0 u
10.0 u
55.7
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
19 IMETALS\TAL.FRM 4113/9'.2
IT Corporation
January 6, 1993
Client Project ID: National Starch
Client Sample ID: Well #5
Lab Sample ID: WJ746
Compound
aluminum
antimony
arsenic
barium
beryllium
cadmium
•
METALS TARGET ANALYTE UST
Results in l'g/liter (ppb)
Sample Matrix: Water
Concentration Compound
40.0 u magnesium
30.0 u manganese
2.0 u mercury
91.4 B nickel
1.0 u potassium
5.0 u selenium
calcium 26,800 silver
chromium 10.0 u sodium
cobalt 20.0 u thallium
copper 10.0 u vanadium
iron 575 zinc
lead 2.0 u
Date of Digestion: I I /03/92
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), 11/12/92 (CVAA)
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
11,300
4.1 B
0.20 u
20.0 u
2,170 B
4.0 u
5.0 u
8,350
2.0 u
10.0 u
16.5 B
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
20 \MET ALS\T AL.FRM 4/13/92
IT Corporation
January 6, 1993 •
Client Project ID: National Starch
Client Sample ID: Well #12
Lab Sample ID: W1747
Compound
aluminum
antimony
arsenic
barium
beryllium
cadmium
calcium
chromium
cobalt
copper
iron
lead
Date of Digestion: I 1 /03/92
METALS TARGET ANALYTE LIST
Results in l'g/liter (ppb)
Sample Matrix: Water
Concentration Compound
40,0 u magnesium
30.0 u manganese
2.0 u mercury
19.6 8 nickel
1.0 u potassium
5.0 u selenium
21,400 silver
10.0 u sodium
20.0 u thallium
10.0 u vanadium
179 zinc
2.0 u
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), 11/12/92 (CVAA)
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
9,950
2.0 u
0.20 u
20.0 u
I, 150 8
4.0 u
5.0 u
5,350
2.0 u
10.0 u
28.1
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
21 \METALS\TAL.FRM 4/13/'n
IT Corporation
January 6, 1993 •
Client Project ID: National Starch
Client Sample ID: Well #14
Lab Sample ID: Wl748
Compound
aluminum
antimony
arsemc
barium
beryllium
cadmium
calcium
chromium
cobalt
copper
iron
lead
Date of Digestion: I 1/03/92
METALS TARGET ANALYrE LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
40.0 u magnesium
30.0 u manganese
2.0 u mercury
27.4 B nickel
1.0 u potassium
5.0 u selenium
22,000 silver
10.0 u sodium
20.0 u thallium
10.0 u vanadium
10.0 u zinc
2.0 u
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), 11/12/92 (CVAA)
• IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
9,410
2.0 u
0.20 u
20.0 u
1,150 B
10.0 u
5.0 u
6,010
2.0 u
10.0 u
22.3
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
22 \Ml:.'TALSITAL.FRM 4113192
IT COf1JOration
January 6, 1993
Client Project ID: National Starch
Client Sample ID: Well #16
Lab Sample ID: W\749
Compound
aluminum
antimony
arsenic
barium
beryllium
cadmium
calcium
chromium
cobalt
copper
iron
lead
Date of Digestion: 11/03/92
•
METALS TARGET ANALYTE LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
40.0 u magnesium
30.0 u manganese
2.0 u mercury
63.7 B nickel
1.0 u potassium
5.0 u selenium
14,400 silver
10.0 u sodium
20.0 u thallium
l0.0 u vanadium
15.9 B zinc
2.0 u
Date of Analysis: 11/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), 11/12/92 (CV AA)
.T ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
6,190
2.0 u
0.20 u
20.0 u
1,720 B
6.0 u
5.0 u
6,620
2.0 u
10.0 u
21.8
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
23 \METAL.S\TAL.FRM 4113/92
IT Corporation
January 6, 1993
Client Project ID: National Starch
Client Sample ID: Well #28
Lab Sample ID: W1750
Com12ound
aluminum
antimony
arsenic
barium
beryllium
cadmium
calcium
chromium
cobalt
copper
iron
lead
Date of Digestion: 11/03/92
•
METALS TARGET ANALYfE LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Compound
40.0 u magnesium
30.0 u manganese
2.0 u mercury
54.7 B nickel
1.0 u potassium
5.0 u selenium
18,700 silver
10.0 u sodium
20.0 u thallium
10.0 u vanadium
79.7 B zinc
2.0 u
Date of Analysis: I 1/16/92 (ICP), 11/12/92 and 11/16/92 (GFAA), I 1/12/92 (CV AA)
.IT ANALYTICAL SERVICES
. 5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52659
Concentration
9,070
4.1 B
0.20 u
20.0 u
1,480 B
6.0 u
5.0 u
7,130
2.0 u
10.0 u
97.1
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
B Value greater than instrument detection limit, but less than contract required quantitation limit.
24 IMETALS\TAL.FKM 4113192
.c·r-:.c.··r;~;;~rtn~ent o! Environment,
1 lvJllh·,, & Nut::ra\ Resources
Solid Wa~_1.c\.1t":lanagcmcnt Division
SA.,E ANALYSIS REQUEST State Laboratory of P\lblic Health
•
. 0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Nllmber NC)') ~1 I }Jeri C\S::3 Field Sample Number_l'-"5"---"3"--C\-'-'-YJ·~--------
Name of Site N A--TlQN A::L ':, T'A€(J-\ Site Location S,'tt.-I'.:. isVJ~..'-:f J eo W iW (00 (0"11/
Collected ByLi2.uct. N I( \tel,'.:l:::t/ ID# 5'1 Date Collected I O -2 2-9 2 Time _____ _
Agency: Har..ardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) Sovwipk 1 Barium --Solid (5) Cadmium --Chromium Li*le 4cres \Jdl No.\ --__ Surface water (2) _ Liquid (6) Lead --
--Mercury.
_Soil (3) _ Sludge (7) Selenium RB;~IV~9 --Silver --_ Other (4) _ Other (8) --DEC I II 1992
--
--sumrn NO S~CllON Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_L_ P&T:GC/MS SfEATTACH~n "' EtrfSC's~nic benzene --_ Acid:B/N Ext. Banum carbon tetrachloride --MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ----
--__ Copper o-cresol --Fluoride m-cresol ------
--Iron p-cresol ----Lead cresol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury --1,2-dichloroethane
--Nitrate 1, 1-dichloroethylene ----Selenium 2,4-dinitrotoluene ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----······-Zinc hexachlorobutadiene ----Paramett!r Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcnc ----TOC __ pentachlorophenol --
----pyridine
Microbiology ----tctrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --~ /.?ti4 / Reported b/1
lindane
Date Received )On)'.3-96) 'SA,AA --methoxychlor
Date Repor~ /~7/?2----toxaphene
Date Extracted 2,4-D
voe_ ~ cb -,._-al-__ 2,4,5-TP (Silvex)
.;jN6UU J Date Analy1.ed 1,2,-J.-9'.1 <j' Lab Number --l)IJS JJ!Ji (Revised 2/91)
N.C."D~Part:,\ent of Environment,
I kalth\ & Natural Resources
Solid Waste Management Division
SA.,,E ANALYSIS REQUEST State Laboratory or Public Health
•
).0. Box 28047, 306 N. Wilmington StrcCt
Raleigh, North Carolina 27611
Sile Number NCI') q9 \ }7''6 353
Name of Site N A--TlQN[tL S T\'t€{Jt
Field Sample Number_~\_S-~3~0~1_:J~---------
Silc Location Sitt, I'., f;Ufl, '-{ J eo W i\N ( 00 f'v'T"'/
Collected ByJSR.ucE. NI( \i-c\..-Sn/ ID# 5'1 Dale Collected IO -2 2-9 J. Time --'""----'---------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments Arsenic --
/Ground water (1) SG\,mple I(, Barium --_Solid (5) Cadmium --Chromium l, ;i\e Aue.c, \Jell No.I~ --__ Surface water (2) _ Liquid (6) Lead --
KO\'\ v,blk We.\l --Mercury
_· Soil (3) _ Sludge (7) Selenium RECEIVED --Silver --_ Other (4) _ Other (8) --DEC IO 1992 ----Organic Chemistry Inorganic Chemistry --SOPFRFHNO SECTION
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I)
_L_ P&T:GC/MS NO VOIATILE COMPOU DS IO(,NmtOO: benzene --_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ----
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1, 1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Paramett:r Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ------TOC __ pentachlorophenol ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane
Date Received in-&s-9a fl/1,SA Reported by --__ methoxychlor
__ toxaphene
Date Extracted Dale Reported 2,4-D --voe_
'P\LabNumbcr
,c '?-, l.-ar _ 2,4,5-TP (Silvcx)
Date Analy1.cd /~ -p, -9,2 .::11.uu ~:)
])/IS JJl)l (Revised 2/91) --
r.:.c. ·otPunrnent of Environment,
I !-calth, & r-.:atura\ Resources
Solid Waste t;-Janagement Division
STE ANALYSIS REQUEST State Laboratory of Public Health
•
. 0. BoA 28047, 306 N. Wilmington Street
Raleigh, Nonh Carolin& 27611
Sile Number NCI', vJS I, }]'Ii C\53
Name of Sile N A---llONA:L ':>T't\€/,\-t
Field Sample Number I S-<-foo -~~~~~----------
Sile Location S,'tt-1'.:. 't,L/]2,':f J eoww Co0r0,-y
Collected Byl5 '2-vct. N I( \tt\};(:W ID# 5'1 Dale Collected I O -2 7--9 L Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds -- --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) s<½Yf~ Z% .
Barium --Solid (5) Cadmium --
No. l?J Chromium Lill& Acre:s lb)eU --__ Surface water (2) _ Liquid (6) Lead --
Sl-ew S1w\M®s \,Je l I --Mercury
_Soil (3) Sludge (7) Selenium --Silver flEetiVEB --_ Other (4) _ Other (8) --
--ore ± ti ,~~z --Organic Chemistry Inorganic Chemistry --stlPEftffiNfl Srerf ON
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_L_ P&T:GC/MS SEE ATTACHED Sl EET(S\Arsenie benzene ----Acid:B/N Ext. Barium carbon tetrachloride --MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--Copper o-cresol ----Fluoride m-cresol ----
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobcnzcne
--__ Mercury 1,2-dichlorocthane
--Nitrate __ 1,1-dichlorocthylene --Selenium 2,4-dinilrotoluenc ----Silver . __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane --Date Received IQ-!;l3-9 Q M,;S.Ci Reported by __ melhoxychlor
__ toxaphcne
Dale Extraclc<l Dale Reported 2,4-D --
Date Analyzed vocl(l-j -9:J, o/711\:-ab Number C:'?"?l.~87 2,4,5-TP (Silvcx)
'-',..~vu --1)/ IS JJIJI (Revised 2/91)
.
r,;.c.-o~Pan·,ncnt of Environment,
I :Cal th, & Natural Resources
Solid Was1e Management Division
S.E ANALYSIS REQUEST State Laboratory of Public Heahh
•
. 0. Box 28047, 306 N. Wilmington Strcel
Raleigh, North Carolina 27611
Site Number NCb lJS \ }7'D' C\53
Name of Sile N A--T)ONA-L ST'M{_\-\
Field Sample Number __ l_S_L/~o~!~----------
Collected ByL'2-ULt N I( itel.-S;(:t/ ID# 5'1
Site Location Sr\i.,1:, fsVf2-:{ )
Date Collected I O -2 2-9 L Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Com pounds Results(rng/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) s~Mpk, s Barium --_ Solid (5) Cadmium --Chromium L·1 ~\e, Aue~ lJell Na. S --__ Surface water (2) _ Liquid (6) Lead --Mercury
_ Soil (3) _ Sludge (7) --Selenium --Silver
_ Other (4) _ Other (8) ----REGl::IYEB ----DEC I ti 199t Organic Chemistry Inorganic Chemistry --
Organic Compound~PERRlN/}e~m,~il) Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) _L__ P&T:GC/MS t;:,:,: , "' =~1Ars~nic benzene
Acid:B/N Ex( --
--Banum carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ----TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichlciroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane
Date Received /O-~-{B:'Jl,AA Reported by __ methoxychlor
__ toxaphene
D"te Extr"cte<l Date Reported 2,4-D
voe /J -_ 2,4,5-TP (Silvex) S23S8S Date Analyzed /62,-J.-9J.'9 ~ab Number --DIIS 3191 (Revised 2/91)
~,;_c. O~pan·ment of Environment,
Health, & Natural Resources
Solid Waste Management Division
SA.,E ANALYSIS REQUEST State Laboratory or Public Health
•
. 0. Box 28047, 306 N. Wilmington Street
Raleigh, North C.arolina 2761 J
Site Number Neb Cjg 111i C\S:3
Name of Site N A--T7QN {t--L S T'tt€{Jt
Field Sample Number _ _,_! y-..,_.,_,(0~2:.._ _______ _
Collected ByJSf:.uct. N 1(\ttl,S;c,J
Site Location SA-t.. I'., '12:,V(l>J )
JD# 5'1 Date Collected I O -2 2-9 L -'""---'--Time ------
Agency: Hazardous Waste --Solid Waste _Lsuperfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) 50J&?\e) N6. Barium \ l---Solid (5) Cadmium ----Chromium Li¼~ AL,?,<, \1,)dl No.I?.. --__ Surface water (2) _ Liquid (6) Lead --
€. m . G 15llc\ Ml\11 -wcll __ Mercury
_ Soil (3) _ Sludge (7) ,) (. Selenium
I --Silver --RECtlVED _ Other (4) _ Other (8) --
--DECIO 1992 --Organic Chemistry Inorganic Chemistry --SUPERfDNOSECIION
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results (mg/I) _L P&T:GC/MS fiEEATTACHED SI EET{S)Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobcnzene
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium --2,4-dinitrotoluene
Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----···•·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
--Gross Bela TDS nitrobenzene ----TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
Parameter Results (Col/lOOml)
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin --lindane
Dale Received l'.h~3-9Q ."¼ AA '
Reported by __ methoxychlor
__ toxaphene
Date Extracted Date Reported 2,4-D --
voe. ~ S23S8~) _ 2,4,5-TP (Silvex)
Date Analyzed /2 -:). -9'2/11 Lab Number --DI IS 3191 (Revised 2/91) '
N.C. Oi:pa1 lment or Environment,
: lcalth, & Natural Resources '
Solid Waste Management Division
STE ANALYSIS REQUEST State Laboratory or Public Health
•
. 0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number NCJ\ '391 ].]''D C\:S::3 Field Sample Number_"--'JS-"'-Y'-'O"'-:)~---------
Name of Site N A---l]ON {t:L S TM(J\ Site Location SA-t,, 1 S, 'bU/2.-4 ) 2o W A-rJ C00 rvf'/
Collected ByJ5'2.vcf. N l(\tt\_.,':(Y ID# 5'1 Date Collected IO -"2 '2--9 L Time _____ _
Agency: Hazardous Waste Solid Waste __Lsuperfund TCLP Compounds -- --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) ~o\p \1 Barium --_ Solid (5) Cadmium --Chromium Li ~!e llixr s I ili\l N,.14 --· Surface water (2) _ Liquid (6) Lead --
~c;. ~~~-\l 2 lier: lA )i[I Mercury
_Soil (3) _ Sludge (7) --Selenium
-Rs;tlvED --Silver
_·_ Other (4) --_ Other (8) --OFC lU 1992 --
--Organic Chemistry Inorganic Chemistry --sulfflMND SECTION
Parameter Resultsbffl1d o~i5t!W[o. Results(mg/l)(mg/kg) Organic Compounds Results(mg/1) ..L__ P&T:GC/MS NO VOIATILE C O II seruc benzene --_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol --Lead cresol --------__ Manganese --1,4-dichlorobenzcne
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----······-·· Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Dale Received IQ-c';)~qJ~ M,:5A Reported by __ methoxychlor
__ toxaphene
Date Extracted Date Reported 2,4-D
voe-S,;;,·,t.-90 _ 2,4,5-TP (Silvex)
Date Analyzed / :)__ -2-9JC) /JyA Lab Number l•JU,J ' --Ill IS 3l'JI (ltcviscd 2/91)
N:C. Dcpurt~ent or Environment,
I lcallh, & Natural Resources
Solid Waste Management Division
S~E ANALYSIS REQUEST
•
State Laboratory or Public Health
.0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number N('J\ fl~,1,JJ'o: f\$3 ., " :·,
Name of Site N @ONA-:l S T'Af[J\
Field Sample Number __ l;..'.\:Y.,__,_,O"--"Lj'-----------
Site Location S,'\-t,1 '.:> F:,V(L'-{ J eo WW (00 rsry
ID# 5C\ Date Collected I C -2 7.--9 L Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Ground water (1) 1R.1P 'bL~~ \l.. --Cadmium Solid (5) --Chromium --Lead __ Surface water (2) Liquid (6)
Mercury
_ Soil (3) _ Sludge (7) --Selenium ·Rffii::IVEO --Silver --_ Other (4) Other (8) --8E6¼11 ~992 ----SOPERfflNfl SEeflON Organic Chemistry Inorganic Chemistry --
Parameter Resultsbm~I) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_L_ P&T:GC/MS NO VOLAlllE C M OU lS IDE~illic benzene ----Acid:B/N Ext. Barium carbon tetrachloride -----MTBE Cadmium chlordane ------Chloride chlorobenzene -----Chromium chloroform -----
--__ Copper o-cresol --Fluoride m-cresol ---
-Iron p-cresol --Lead cresol ---
--__ Manganese --1,4-dichlorobenzene
-__ Mercury 1,2-dichloroethane
-Nitrate --1,1-dichloroethylene --Selenium 2,4-dinitrotoluene --= heptachlor Silver --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCl/1) _pH hexachloroethane
_ Gross Alpha _ Conductivity = methyl ethyl ketone
Gross Beta TDS nitrobenzene ----TOC __ pentachlorophenol ----__ pyridine
Microbiology --tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --2,4,6-trichlorophenol --------= vinyl chloride
endrin --lindane
Date Received )0-<:93-CJ6l M SA Reported by --__ methoxychlor
__ toxaphene
Date Extracted Date Reported 2,4-D
voe.. S0 ''.' 1.-3"' = 2,4,5-TP (Silvex)
Dale Analyzed /:).., -:). -9.:J. .J1lr,\ Lab Number ,~uu .L --llllS 3191 (Revised 2/91)
.... •,.
l'~rpose: Enforcement a.pliance with the N.c·: Solid a_nd Hazard&aste Management R~:s: ' .. ,,
,Preparation: A sample analyses request form must be completed for each type of evaluation requested (e.g., inorganic,
organic, microbio}pgy, radiochemistry). For s~pling conditions which require '!lore than one (1) rontainer
(i.e., ground or surface water) a sample label must be affixed to:on_e of t~e !"'!1\ai!'er,;.:.The collector must
then write the site and sample number on the duplicate container. · ··,
•/ • I
Do not submit an analysis req11est form without any parameters indicated.
Equivalent measurements:
' '
ppm = µg/ml = mg/I = µg/g = mg/kg
ppb = µg/) = µg/lOOOg = µg/kg
DEFINITIONS/INSTRUCTIONS
Site Num_ber -A unique twelve-digit site/location identifier (i.e., the EPA identification number).
Field Sample Number -A unique six-digit samp!e identifier which is p;e-printed on the sample label.
. Name of Site -Name of facility, landfill; etc.
' -r '"*-, II • ' • . ' ' .,4, ,, "' ~"--1 ,t. ,c \ SiJe'.,~l!lion:: City and county .
.. ::tr .... ; i ··i ·"1 .
. . . ·: .. · Collected_ By -Name and staff identification number of collector.
•·,u:i.i 1-'o~t~'iui'd'Time Collected -Self-explanatory. -'
· Environ.mental -A sample of a naturally occurring substance such as grou~d water, surface water, or soils which may
be contaminated.
Concentrate - A sample of a waste, including but not Hmited to, sludges, resins, treatment effluents, or drummed
wastes.
Comme"ts Lists details regarding sample or sample point (e.g., sample location, well number, phase separation,
and/or odors.
Inorganic Chemistry Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the
element/compound in the space proyided.
Organic Chemistry Check ( ( ) the desired parameters to be a"alyzed. If not listed, enter the
element/compound in the space provided.
TCLP Compoun_ds -Check ( ✓ ) the desired parameters to be analyzed. If not listed, enter the
. element/compound in the space provided. TC/.-P can only be performed on solid or semi-
solid samples. For totals of the inorganic parameters, check ( ✓ ) the corresponding
parameter under Inorganic Chemistry.
Microbiology and Radloche_mlstry -Contact the Raleigh office prior to sampling either of these.
Distrib_ution:
Disposition:
1. Send or deliver the original to the State Laboratory of Public Health.
2. The Lab then sends a copy (with results) to the Solid Waste Management Division.
3. The Solid Waste Management Division sends a copy to the field person or collector.
This form may be destroyed i~ accordance with the E_nvironmental Health, Sol.id and HazardO)IS Waste
Section of the Records Disposition Schedule as publ~hed by the North Carolina Division of Archives and
History
Additional forms may be ordered fr_o,m: Solid Waste Managei,nent Division
Hazardous Waste Section
P.O. Box 27687
Raleigh, NC_ 27611
. r-.:.c o.-,pnr:iment or Environment,
1 lca\th, & Nalural Resources
Solid Wasle Management DivU:ion
S~LE ANALYSIS REQUEST St,He l...tibon.tol)· of i'ublic Hc•lrn
•
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number NC!') CJ 9 I }t6 °)\3
Name of Site N A·T]QNAf-STT\€(.\-1
Field Sample Number_~\ ~S:~L\~e:,_<;;'_-__________ _
Site Location SAL-15\sv~'I' , /2oLvt't-/v C.ovr--..1-, i
'
Collected By:]s((.ucc. N I( ltC\..--S)} ID# 5'1 Date Collected IO -2 '2--9 L Time 11: 4o
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) 'Sfim PL--f-1 Barium --Cadmium _ Solid (5) --
~ 1 rr~e Ac.ff:~]
Chromium
\ --
__ Surface water (2) _ Liquid (6) W!::.L-L-No. Lead --Mercury
_Soil (3) Sludge (7) --Selenium --Silver -REei:IVE6 --
_ Other (4) Other (8) ----BES ct tt 1992 --
Organic Chemistry Inorganic Chemistry --SUPE!lflfNO SECTION
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
::Z Acid:B/N Ext. ~ EC· 1 c Bariu':'
--
SEE UI~GH!'J) c; carbon tetrachloride --
MTBE · Cadmmm chlordane
------
Chloride chlorobenzene
------
Chromium chloroform
----
--__ Copper o-cresol --
Fluoride m-cresol
------
--Iron __ p-cresol
--Lead cresol
------
--Manganese --1,4-dichlorobenzene --
----Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
--Selenium 2,4-dinitrotolucne
----
Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobenzene
----
" Zinc hexachlorobutadiene ----
Parameter Results (PCi/1) _pH hcxachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnzcne
----TOC __ pcnlachlorophenol
----__ pyridine
Microbiology --__ tetrachloroethylene
--__ lrichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
cndrin --lindanc --
Dale Received 10-@3-'.3<9 A/J.. ;5('!!. Reported by __ mcthoxychlor
__ toxaphenc
Date ExtractcJ IQ-@'.l·9o>5A &A,WC Date Reported --2,4-D
Ll-3D -9.L dtJ 523592
2,4,5-TP (Silvex)
Date Analyzed Lab Number --
DIIS 3\IJI (Revised 2/91)
N.C. D1~partmcnt or Environment,
1 lcalth, & Nalunil Rcsourcu
Solid Wa~te Management Divi:sion
S~LE ANALYSIS REQUEST St&tc L.aa't.>oratory of f'ublic Hcallh
•
P.O. Box 28047, 306 N. Wilmington St~et
Raleigh, North Carolina 27611
Site Number NCb ~g I J:]7: 353
Name of Site N A--T]QNA::L S TY\£{,\i
Field Sample Number_-"\S-~-~~Q,=-----------
Site Location SfrU5 l!,v (2, l/
Collected By]si2.uct. N l(\tCly;;Ct/ JD# 5q Dale Collected I O -'2 2-9 J. Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
----
Sample Type In01;;anic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Ground water (1) S &IY\ i"L£, \~Q --
_Solid (5) Cadmium --Chromium
L 'L IB--Jz ActfS weuNo,10 --
__ Surface water (2) Liquid (6) Lead --
\s,otJ
__ Mercury
Soil (3) Sludge (7) WoLfE J OWNst-Selenium --Silver REesvea --
Other ( 4) Other (8) ----DEC l U 1992 --
Organic Chemistry Inorganic Chemistry --StlPERfflND SEC1'19N
Parameter Results (mg/I) Parameter Results(mg/I)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
::Z Acid:B/N Ext :iEEATTACHED S
--
Ems¥arium carbon tetrachloride --
MTBE Cadmium chlordane
------
Chloride chlorobenzene
------
Chromium chloroform
----
--__ Copper o•cresol --
Fluoride m•cresol ----
--Iron __ p-cresol --Lead cresol
------
--_·_ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroclhane
--Nitrate --1,1-dichloroethylene
--Selenium 2,4-dinitrotoluene --= heplachlor Silver --
Radiochemistry Sulfates hexachlorobenzene ----
Zinc hexachlorobutadiene ----
Parameh:r Results (PCi/1) _._pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne
----TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylcne
--__ trichloroethylcne
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
cndrin --lindane --
Dale Received )0-cD:3-9.QAASA Reported by methoxychlor
0 --__ toxaphene
Date Extracted I0-2'1-92'$A i,;G, M Date Reported --2,4-D
Date Analy,cd //-Jo -9.L-13,J) S2JS33
2,4,5-TP (Silvex)
Lab Number --
l)IIS3J<Jl (llcviscd 2/91)
·· KC. D,\par:imcnt or Environment,
J lcnllh, &. Nalura\ Resources
,s.;lid Waste Management Di-.i.s;ion
S'LE A.."lALYSIS REQliEST St.ate La:>onlc.,ry of f'ubjj,: Ht.:;.l!h
P.O. Box 28047, 306 N'.Wilmington S1rect
• Raleigh, North Carolin, 27611
Sile Number NC,\') q:311-T~ 3S::3
Name of Site N A--1]0N frL S T'A-fO-\
Field Sample Number _ ___,l_.,S-'-Y--l.Ooc:...7_,_ ________ _
Site Location SAL\5 l?,v !'.'-t/
Collected By]5 '2-uct. N K \tC\..-';r'!/ JD# 5'1 Dale Collected IO -"2 2 9 2 Time ------
Agency: Hazardous Waste Solid Waste _LsuperfWld TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) SB:IYIPl-e
Barium
2-22 --
_ Solid (5) Cadmium --Chromium
L1TTJ.£ Ace@) \\/H-L No. Z.o --Lead
Surface water (2) _ Liquid (6) --
_ Sludge (T) s ~(!.,\le S1(tllW\'.'.)':, wdJ __ Mercury
_Soil (3) Selenium
fl~tlVED --Silver
_ Other (4)
--
_ Other (8) --DEC 10 1992 --
--
Organic Chemistry Inorganic Chemistry --SUPERRIND SFCTJON
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
:Z Acid:B/N Ext.SEEATTAr1-1a-r,
--
)Barium carbon tetrachloride --
MTBE --._.,.Cadmium chlordane
------
Chloride chlorobenzene
------
Chromium chloroform
------
--__ Copper o-cresol --
Fluoride m-cr-:sol
----
--Iron __ p-cresol --Lead cresol
------
--__ Manganese 1,4-dichlorobenzene --
--__ · Mercury 1,2-dichloroclhane
--Nitrate __ 1,1-dichloroethylene
--Selenium 2,4-dinilrotolucne --Silver __ heplachlor
--
Radiochemistry Sulfates hexachlorobenzene ----
··----Zinc hexachlorobutadiene --
Paramekr Results (PCi/1) pH hexachloroelhane --
__ Gruss Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela TDS nitrobenzcne
------
TOC __ penlachlorophenol ----__ pyridine
Microbiology --__ tetrachloroethylenc
--__ trichlorocthylcne
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-lrichlorophenol
----__ vinyl chloride
endrin --lindanc
Date Received \0-~-'.36) M;';A
--
Reported by --mclhoxychlor
__ loxaphcne
Date Extractc<l Jo-,;,'7-9;;):\A,WG, M Dale Reported 2,4-0
Date Analyzed / /-Jo -9:l (3,S}
__ 2,4,5-TP (Silvcx)
Lab Number S23::;3.1,
DIIS 31 1)] (llcviscd 2/91)
--
t,.'.C. ['.;:partment of Environment,
i lcalth, & Natun.l Resources
Solid Was.le M11.nagcment Division
SciLE ANALYSIS REQUEST Stnt::. L..it..oratory ot t·uotic Hc.anh
P.O. Box 28047, 306 N. Wilmington Street
• R.tleigh, North Carolina 27611
Site Number NCI:) CJ9 j JJi C\S:3
Name of Site N A-T]ONA-L ST'ftl'.{.\i
Field Sample Number_-'j'-"S"'-L\--'-='o_,_8'------------
Site Location SAU5£,ue.y ' Qocv14-N CDvt--J-, i
'
ID# 5'1 Date Collected IO -2 2-9 L Time ------
Agency: Hazardous Waste Solid Waste Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) Scwv,fk 8
Barium --
_ Solid (5) Cadmium --Chromium
Lifrle Aves Wdl ~0-5 --
__ Surface water (2) Liquid (6) Lead --__ Mercury
Soil (3) _Sludge (7) Selenium --Silver -RE6t1VEB --
_ Other (4) Other (8) ----SES l Y 1992
--
Organic Chemistry Inorganic Chemistry --stlfEftfBND SEtTION
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene ----
v Acid:B/N Ext.SUAl'.n~11 _ Barium carbon tetrachloride
£T(S)cadmium
--MTBE --, ta Efl SFI chlordane
------
Chloride chlorobenzene ------
Chromium chloroform --= Copper
--
--
o-cresol --
Fluoride m-cresol
------
--Iron p-cresol --Lead cresol
------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury __ 1,2-dichlorocthane
--Nitrate __ 1,1-dichlorocthylene --Selenium 2,4-dinitrololuene ----
Silver __ hcplachlor --Radiochemistry Sulfates hexachlorobenzene
----
··----Zinc hexach lorobutadiene ----
Parameter Results (PCi/1) _pH hcxachlorocthane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnzcne
------
TOC __ pentachlorophenol ----__ pyridine
Microbiology --__ tctrachloroethylene
--__ trichloroethylenc
Paramckr Results (Col/lOOml) __ 2,4,5-lrichlorophenol
--
--
__ 2,4,6-lrichlorophenol --
----__ vinyl chloride
cndrin --lindane --
Dale Received lo-c::l3-CJ<9 M, Sf), Reported by __ methoxychlor
Dale Extractc<l IQ/2'7/1'.Jz Sil. hr. M Date Reported
__ loxaphenc
2,4-D
Date Analyzed / /-30 -9.:Z-8;.!) 523595 _ 2,4,5-TP (Silvex)
Lab Number --
n!IS 3J'J1 (llcviscd 2/91)
N,C"_ D,:.rn.r:tment or Environment, I lcalth, & Natural Resources &>1id Waste Management Dj\.-ision S'LE ANALYSIS REQUEST State Labora.tory of t'ublic Health •P.O. Box 28047, 306 N. Wilmington Street Raleigh, North Carolin• 27611 Site Number NC)') ~j I 7-7i C\53 Name of Sile N A-'flON ft:L S TY'ti;[,\i Field Sample Numbcr_-_,_l-5'-Y-'-"-o_,,_'1 _________ _ Site Location Sf\L-15\?,v~Y . Qo-wtd,,N Ci?vt0-t i t i' , Collected By'];~uct. N I( ltCJ---Sn/ JD# 5q Date Collected IO -2 2--9 2 !, Time ------Solid Waste __Lsuperfund TCLP Compounds --lnori:anic Compounds Results(mg/1) C,IIVll l/111111...IHRI '-'VHI... ... HLI U~I., Comments Arsenic --/Ground water (1) Barium S A-m PL.p,:, \'l---Cadmium _ Solid (5) --Ac~r-~ W5U-No.lZ Chromium __ Surface waler (2) _ Liquid (6) Linµ Lead E,tJ\. G ool>M BNJ 1' 11,, We\,\. Mercury Soil (3) _ Sludge (7) --Selenium ·RECBVEO --Silver --Other ( 4) _ Other (8) --DEC l Y 1992 f --Inorganic Chemistry --Sll~ERfffNB SEC'fl8N Organic Chemistry --Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) O11:3nlc Compounds Results(mg/1) P&T:GC/MS Aisenic benzene L Acid:B /N ExtSEf A:l'°MSI I --Barium --carbon tetrachloride ET(S) Cadmium --MTBE . fflSHt chlordane --Chloride chlorobenzene ------Chromium chloroform ----__ Copper o-cresol ----Fluoride m-crcsol ------Iron p-cresol --Lead cresol ------__ Manganese 1,4-dichlorobenzcne --__ Mercury __ 1,2-dichlorocthane --Nitrate __ 1,1-dichloroethylene --Selenium· 2,4-dinit rotolucne --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexach lorobutadiene --Parameter Results (PCi/1) _pH hexachloroelhane __ Gross Alpha __ Conductivity __ methyl ethyl ketone Gross Bela TDS nitrobenzcnc ----TOC __ pentachlorophenol ----__ pyridine Microbiology --__ tetrachloroethylene --__ trichloroethylene Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol ----__ 2,4,6-trichlorophenol ----__ vinyl chloride endrin --lindane Date Received [O-c:J3-':/bl AA:5A Reported by __ mcthoxychlor __ Loxaphcne Dale Extraclc<l [0-2'7:925A, bG; AA Date Reported 2,4-D Dale Analyzed 1/-Jo-'l.2-fit!) SZJ53G __ 2,4,5-TP (Silvcx) Lab Number --DI IS 31')\ (l~cviscd 2/91) " ,. ,.
KC. r..ct~nment of Environment,
I !callh, & Natural Resources
Solid Waste Management Dfl.'Uion
S11LE ANALYSIS REQUEST
•
State Ubonitory of Pubiic ilc•llh
•
P.O. Box 28047, 306 N. Wilmington S1rcct
Raid~. North Carolina 27611
Stle Number NCb 9S I }7<6 353
Name of Site N A---T]QN t3:L S TT't!:(, \-\
Field Sample Number _ _,_\5~L_,_\ ""!()~----------
Site Location SA-U5 E,u C-7' f2.oLvf'I-N C1>v ~-, i
Collected By]sg,ucc N 1(\Wv;;(:t/ JD# 5,q Date Collected I O -'2 '2--'l 2 Time ------
Agency: Hazardous Waste Solid Waste Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compnunds Results(mg/1)
Environmental Concentrate Comments Arsenic --
· /Ground water (1) Scvmplg, \4 Barium --Cadmium Solid (5) --
We\\ No, 14
Chromium
Li~le l\c(e<, --
__ Surface water (2) Liquid (6) Lead --
~\rs, \<(Y\,Jh £\\eY wJ Mercury
Soil (3) Sludge (7) --Selenium
-~~tll,.'ED --Silver --
Other ( 4) _ Other (8) --\IE C IO 1992 ----
Organic Chemistry Inorganic Chemistry --SIIPFRFHND SECTION
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
:Z Acid:B/N E~4™"HED SI I --Barium --carbon tetrachloride
rtsr-cadmium
--
MTBE , • " E chlordane ----
Chloride chlorobenzene
------
Chromium chloroform ----
--__ Copper o-cresol --
Fluoride m-cresol
------
--Iron __ p-cresol --Lead crcsol ------
----Manganese 1,4-dichlorobenzene --
--__ Mercury __ 1,2-dichloroelhane
--Nitrate __ 1,1-dichloroethylene
--Selenium 2,4-dinitrololucne ----
Silver __ heptachlor
--
Radiochemistry Sulfates hexachlorobenzene ----
"••··--Zinc hexachlorobu tadiene ----
Parameter Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela TDS nitrobenzcne
----TOC __ pentachlorophenol
----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroelhylene
Parameter Results (Col/!OOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ ,foyl chloride
endrin --lindane
Dale Received \Q-.::>3-9ai &,A,5A Reported by __ mcthoxychlor
__ loxaphene
Dale Extracted / 0 ·.1 J"-CJ J-, Dale Reported 2,4-D
Dale Analy,cd [,.<-/ -9 .1-A£) S2JS97
__ 2,4,5-TP (Silvcx)
Lab Number --
Dl!S 31 1)1 (ltcviscd 2/91)
'
. "' • •
SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
0 K6 iltN IC.
Chain of Custody Record
Hazardous Waste Materials
REGt.lV.ED
DEC 10 1992
SU PERRINO SECTION
CERCLA
Location of Sampling: Generator Transporter
Treatment Facility -storage Facility
-Disposal Facility -Landfill
X Other: J?rlvoJ-e.. \0.1,lls: 75tf sck
Company• s Name Ng_·\-i"mM~ :Skvc.\, ~ C\s..ill-1(.i'~lephone: }o if (.:,33, /]'!,/
Address C.eJc,,v:: ~Y'.lhAS en,) . .RJ,sh>vc~ h,Jc 2 % I 44 'c::, , I
Collector's Name~ . J/2.i; J.&,~c, c:-Telephone: 5'19 1'.:>-S-2901
signature
Date Sampled lo -1'2...::'.31., Time Sampled I I·; 4o ·-2 ·. t./o
Type of Process Generating Waste _______________ _
Field Information: :Pl(,'vcJ-e.. \,\ )ej\
\(ts,'i\ o v: ·p(A..v:\c
Field Sample No. 1539?:i IS:3°14 r(L/oo
IS-yo:;: IS-Yo6 1S:Yo1
Chain of Possession:
4=-= %lAL signature
~if~ signature
signature
R~:;;~
~gnature
t:f::C?z~Yos-rz. 3S--r 7
title
title
1,;: Yoz.
1S-Y 01
;ohzAi -!o/z3/cfz_
inclusive dates
inclusive dates
inclusive dates
Instructions: Complete all applicable information including
signatures, and submit with analysis request forms.
N. c. DEPART! Of ENVIRONMENT. HEALTH. & NATURAL REl:Es -RECt.1· 1vED
DIVISION Of LABORATORY SERVICES, ENVIRONMENTAL SCIENCES SECTION O [ C ij 1992
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611
Laboratory No. f /!...2J~ PURGEABLE COIIPOUNDS Date of AnalySillPER~9$!iCr!ON
COIIPOUND µg/1 COIIPOUND
Dichlorodifluoranethane /J ✓Chlorobenzene
Chloranethane ✓Ethvlbenzene
vVinvl Chloride 1 1 1 2-Tetrachloroethane
Bronanethane ✓o-Xvlene
Chloroethane ✓m--Xvlene
Trichlorofluoranethane ✓o-Xvlene
✓1. 1-0ichloroethvlene ✓Stvrene
Hethvlene Chloride Branofonn
tert-Butvl Hethvl Ether I lbenzene
✓trans-1 2-0ichloroethvlene 1 1 2 2-Tetrachloroethane
Is 1 ether Branobenzene
1 1-Dichloroethane n-Pr=vlbenzene
2 2-Dichlo ne 1 2 3-Trichlo~r-•ne
✓cis 1.2-Dichloroethvlene --;, 2-Chlorotoluene
Chlorofonn l K 7 1 3.5-Trimethvlbenzene
IBCHl Branochloranethane IJ 4-Chlorotoluene
✓1. 1. 1-Trichloroethane I tert-Butvl Benzene
1. 1-0ichlo ne I Pentachloroethane
✓Carbon Tetrachloride 1 2 4-Trimethvlbenzene
✓Benzene sec-Butvl Benzene
✓1 2-Dichloroethane D-I ltoluene
✓Tri ch 1 oroethv 1 ene 1.3-Dichlorobenzene
✓l .2-0ichlo ne ✓1 4-0ichlorobenzene
Bromodichloranethane n-Butvlbenzene
Dibronanethane ✓1.2-0ichlorobenzene
✓Toluene I Bis 12-Chlorois=r=v]) Ether
1 1 2-Trichloroethane I 1 2-0ibrano-3-Chlor-~•ne
✓Tetrachloroethvlene 1.2 4-Trichlorobenzene
1 3-Dichlo~r~ne Hexachlorobutadiene
Dibranochloranethane N•nhthalene
1.2-Dibranoethane (EDBl I 1.2.3-Trichlorobenzene
1-Chlorohexane -JI
COIIIENTS:
MDL -MinilllJITI Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value js known to be less than value given. L -Actua] value 1s known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed. 1/ -Tentative identification.
✓ -Re~ulated voe T -Tr1halanethane
N.C. Dept. of Environment, Health, & Natural Resources
DEHNR 3068-0 (Rev. 10/92 Laboratory Services)
#1532E D-18
µg/1
II
I
I
I
I
ii
e e RECl:IVED
N. C. DEPARTMENT OF ENVIRONMENT. HEALTH, & NATURAL RESOURCES DEC 1 O 1992 DIVISION OF LABORATORY SERVICES, ENVIRONMENTAL SCIENCES SECTION
Laboratory No.
I,) P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 276111MID
fj 358'1 PURGEABLE COMPOUNDS Date of Ana<;IJP~Rf~~J_
COMPOUND µg/1 COMPOUND
Dichlorodifluoranethane J , ✓Chlorobenzene
Chloranethane vEthv 1 benzene
vVinvl Chloride l 1 1 2-Tetrachloroethane
Brorranethane vn-Xvlene
Chloroethane vm-Xvlene
Trichlorofluoranethane vo-Xvlene
vl 1-0ichloroethvlene vStvrene
llethvlene Chloride Branofonn
tert-8utv1 llethvl Ether I !benzene
vtrans-1 2-0ichloroethvlene 1. 1 .2 2-Tetrachloroethane
I 1 ether Branobenzene
1 1-0ichloroethane n-Prnnv]benzene
2.2-0ichlo ne 1 2 3-Trichlo~r""'ne
vcis-1 2-0ichloroethvlene ,J/ 2-Chlorotoluene
Chlorofonn I I<'. -r 1 3.5-Trimethvlbenzene
IBCMl Branochloranethane ' 4-Chlorotoluene
vl 1 1-Trichloroethane tert-8utv1 Benzene
1 1-0ichlo ne Pentachloroethane
✓carbon Tetrachloride 1 2 4-Trimethvlbenzene
✓Benzene sec-8utv1 Benzene
vl 2-Dichloroethane D-I ltoluene
vTrichloroethvlene 1 3-Dichlorobenzene
✓1 2-0ichlor ne vl.4-Di chlorobenzene
Branodichloromethane n-8utvlbenzene
Dibrorranethane vl 2-0ichlorobenzene
✓Toluene Bis 12-Chloroisnnrnnvl) Ether
f 1 2-Trichloroethane 1.2-0ibrano-3-Chlo~r=•ne
vTetrachloroethvlene 1 2 4-Trichlorobenzene
1 3-Dichlor-r---ne Hexachlorobutadiene
Dibranochloromethane N>nhthalene
1 2-Dibranoethane 'EDB' 1.2.3-Trichlorobenzene
1-Chlorohexane
COMMENTS:
MDL -Mininun Detection Limit for water (EPA llethod 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected. NA -Not analyzed.
1/ -Tentative identification. v -Re9ulated voe T -Tr1halomethane
N.C. Dept. of Envirorvnent, Health, & Natural Resources DEHNR 3068-0 (Rev. 10/92 Laboratory Services)
#l532E 0-18
µg/1
J ,
I
I
JI
• • N. C. DEPARTMENT Of ENVIRONMENT, HEALTH, & NATURAL RESOURCES
DIVISION Of LABORATORY SERVICES, ENVIRONMENTAL SCIENCES SECTION
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611
Laboratory No. 9:;_ .35~$ PURGEABLE COl1POUNDS Date of Analysis
COl1POUND µg/1 COl1POUND
Dichlorodifluorarethane (A ,'Chlorobenzene
Chloranethane ,'Ethvlbenzene
vVinvl Chloride 1 1 1 2-Tetrachloroethane
Brooonethane ,'n-Xvlene
Chloroethane ,'m-Xvlene
Trichlorofluorarethane ,'o-Xvlene
,'1. 1-0ichloroethvlene .rstvrene
Methvlene Chloride Braoofonn
tert-Butvl Methvl Ether Is-r-· lbenzene
.rtrans-1.2-0ichloroethvlene 1. 1.2.2-Tetrachloroethane
I 1 ether Braoobenzene
1. 1-0ichloroethane n-Pr=vlbenzene
2.2-0ichlo, ne 1 2 3-Trichlo ne
.rcis-1 2-0ichloroethvlene ' 2-Chlorotoluene
Chlorofonn ,_ r-T 1 3.5-Trimethvlbenzene
(SCIO Branochloranethane ' I 4-Chlorotoluene
,'1 l. 1-Tri ch 1 oroethane K tert-Butvl Benzene
1 1-0ichlo ne ! Pentachloroethane
,'Carbon Tetrachloride 1.2 4-Trimethvlbenzene
,'Benzene sec-Sutvl Benzene
,'1 2-Dichloroethane o-I ltoluene
.rlrichloroethvlene 1 3-0ichlorobenzene
,r1 2-0ichlor=r=ane ,'1 4-Dichlorobenzene
Bromodichlorarethane n-Sutvlbenzene
Di brooonethane ,'1 2-0ichlorobenzene
.rloluene Bis 12-Chlorois=r=vll Ether
1. 1.2-Trichloroethane 1 2-0ibraoo-3-Chlo, ne
.rletrachloroethvlene 1 2 4-Trichlorobenzene
1 3-Dichlo~r=•ne Hexachlorobutadiene
Dibromochloranethane N·fththalene
1.2-Dibroo,oethane IEDBl 1.2.3-Trichlorobenzene
1-Chlorohexane
<XlllENTS:
MDL -Minillllll1 Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification.
,r -Re9ulated voe T -Tr1halanethane
N.C. Dept. of Environment, Health, & Natural Resources DEHNR 3068-0 (Rev. 10/92 Laboratory Services)
#1532E 0-18
µg/1
u
I
I
I
I
I
I
REC,1:IVfr
DEC 1019'
SllPERRf NO SECTm"
• • N. C. DEPARTMENT OF ENVIRONMENT, HEALTH, & NATURAL RESOURCES
Laboratory No. '
DIVISION OF LABORATORY SERVICES, ENVIRONMENTAL SCIENCES SECTION P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611 92,. q59'J PIJRGEABLE COMPOUNDS Date of Analysis
COMPOUND µg/1 COMPOUND µg/1
Dichlorodifluoranethane u ✓Chlorobenzene ,,
Chloranethane ✓Ethvlbenzene
v'Vinvl Chloride 1 1. 1.2-Tetrachloroethane
Brananethane ✓o-Xvlene
Ch 1 oroethane ✓m-Xvlene
Trichlorofluoranethane ✓o-Xvlene
✓l. 1-Dichloroethvlene ✓Stvrene
Methvlene Chloride Braooform
tert-Butvl Methvl Ether I lbenzene
✓trans-1.2-Dichloroethvlene 1. 1.2.2-Tetrachloroethane
I ,, 1 ether Braoobenzene
1. 1-Dichloroethane n-Proovlbenzene
2.2-Dichlo ne 1.2 3-Trichlornnr~ne
✓cis-1 2-0ichloroethvlene ' 2-Chlorotoluene
Chloroform ·' A .T 1.3 5-Trirrethvlbenzene
(BCMl Braoochloranethane LI 4-Chlorotoluene
✓1 1 1-Trichloroethane -1-rA~ ~ tert-Butvl Benzene
1. 1-DichlornnrnN>ne u Pentachloroethane
✓carbon Tetrachloride 1.2 4-Trirrethvlbenzene
✓Benzene sec-Butvl Benzene
✓1.2-Dichloroethane D-I ]toluene
✓Tri ch 1 oroethv 1 ene 1 3-Dichlorobenzene
✓1.2-Dichlornnrnnane ✓1.4-0ichlorobenzene
Brarodichloranethane n-Butvlbenzene
Di brananethane ✓1 2-Dichlorobenzene
✓Toluene Bis (2-Chlorois 1l Ether
1. 1.2-Trichloroethane 1.2-Dibrorro-3-Chlo
✓Tetrach loroethvlene 1 2 4-Trichlorobenzene
1.3-Dichloroor""-'ne Hexachlorobutadiene
Dibrarochloranethane N•nhthalene
1 2-Dibranoethane (EDB) I 1.2.3-Trichlorobenzene
1-Chlorohexane
MDL -Minirrum Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected.
NA -Not analyzed. 1/ -Tentative identification.
✓ -Re9ulated voe T -Tr1halanethane
N.C. Dept. of Environrrent, Health, & Natural Resources DEHNR 3068-0 (Rev. 10/92 Laboratory Services)
#1532E D-18
ne
11
RE(;l:IVED
C 10 1992
~IIPERflfNO SECTION
BASE/NEUTRAL AND ACID
EXTRACTABLES
COIIPOUND
N-nitrosodimethvlamine
bi s(2-ch loroethvl lether
2-chlornnhenol
ohenol
1.3-dichlorobenzene
1.4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n-nrf'V"lvlamine
nitrobenzene
i <:IY'lhorone
2-nitrnnhenol
2.4-dimethvlohenol
bisf2-chloroethoxvlmethane
2.4-dichloroohenol
1.2.4 trichlorobenzene
naohthalene
hexachlorobutadiene
4-chloro-m-cresol
hexachlorocvcl~ntadiene
2 4.6-trichlornnhenol
2-chloronanhthalene
acenaohthvlene
dimethvl ohthalate
2.6-dinitrotoluene
acenaohthene
2.4-dinitrnnhenol
2.4-dinitrotoluene
4-nitrnnhenol
fluorene
4-chlornnhenvlohenvlether
diethvl ohthalate
4 6-dinitro-o cresol
diphenvlamine
azobenzene
4-bramohenvlnhenvlether
hexachlorobenzene
=ntachlornnhenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
J -Estimated value.
• • STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUHAN RESOURCES
P.O. BOX 28047 -306 N. ,IHLHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO CJ;:/-;) ~.2.
FIELD#
TYPE
UNITS
'"'
,
SQI "hSO
IOI c'c'O ~a, ,.co
IO' '30
so, ),_i:-o
/0/330
' so/11,,:ro
,,., I '"O
' ,
m1)L
f{,_O/.S o I I-
1,1/ D'
( I l
••n/J \ ..
I ' -
• I
'-'-2~ i.\"T ~ CJ;(O?S9 </ .
/_<j I-QI-1,<107
( l ( 1 ,
u a/ 1 1-,,,.,""' .. n/1} ,.,../i..,,
IA-J,I
. .
' '
<.f,).3 \ 9S
ISYO)(
( l
· .. n/1 Im-.
(
.
'
K -Actual value is known to be less than value given.
C/.J-3 ,;y(., 'f,}. < ,'f 7
I ,"lo'-f /~I /0
( I) ( l
7.,n/ 1 , .. n/ 1 \rrm(lln
·,-:,:: I A. -
. . ,,
L -Actual value is known to be greater than value given. u -Material was analyzed for but not detected. The nUTber is
NA -Not analyzed.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N. C. V-<.v,{,6.fon 06 He.aLth SVtv-<.c.U
VHS 3068-0 (4/86 LaboMA:o~y)
the _!1ininun _2etection !.;_imit. ~(,1:f V►O
DEC 1 II
stJPERFOO SECTION
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
COMPOUND
nvrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3 3-<lichlarobenzidine
bis(Z-ethvlhexvllohthalate
di-n-oetvl ohthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a\nvrene
indeno(l .2 3-<:dlovrene
dibenzo(a h)anthracene
benzo(Q.h il,,.,rvlene
anll ine
benzoic acid
benzvl alcohol
4-<:h 1 oroan il i ne
dibenzofuran
2-n-ethvlnaohthalene
2-<rethvlohenol
4-n-ethvl oheno 1
2-ni troani 1 i ne
3-nitroaniline
4-rll troani Hne
2 4 5-trichlo~henol
• • STATE LABORATORY OF PUBLIC HEALlH
OIVISIOH OF HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC 01EMICAL ANALYSIS
LAB NO (./ .,J =? <'7.2-<./ ,;1..a_s'i~-1 'I .:1.3.) 7' y 'I .2. < \ '7'.J
FIELD # I S"'/0) /_'(', 0~ /S'lo7 1:r< '{) '/{
TYPE c I l r ) r I l ( 1
UNITS ,,....-uo/1 ' -ua/1 •=tvn .. n/ J .),nf,l,m Hn/1
10/:''/l'J ~ -I ~ i,{_... L,(.-
,;-,, /, ,,.,;-0
/0/. 130
.
so, '"'-'i1J
IO/ i3o
110/.s.~o
S"O/JJ.','r.
' , ·.' I ' ' '
<o'· I -I.A--IA-J ,A
... ~ I().
,,
5"0 I, 1,,,0
\l:t '/ \, \
mJ)L.
J -Estimated value. H;o.O/ .$()//..
K -Actual value is known to be less than value given.
RECt\VEO
DEC .LU 1992
SUPER~ND SECTION
'-/--2 ~S"r& -LL.3JY7
1/J'/0'7' l'\Y/0
( / 1 c I l
.. n/1 )rimm ua/1 1-·"
-vL--v.,_
-\
LA-IA
-
\" ' ,
L -Actual value is known to be greater than value given.
U -l'\aterial was analyzed for but not detected. The nurber is the HiniITIJTI Detection Limit.
NA -Not analyzed.
111:Dt.. -
1/ -Tentative identification.
~/. -On NROC List of Priority Pollutants.
N. C. V,i_v,i,;.i.o tt o 6 H eaUh SVLv.i.c.v.,
VHS 3068-0 (4/86 Labon.a.to~y)
• •
SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
. T l\lo 12.icdrN IC...
Chain of Custody Record
Hazardous Wast~ Materials
CERCLA
Location of Sampling: Generator Transporter
Treatment Facility --Storage Facility
--Disposal Facility =Landfill \J ✓other: fv,Vc,k lA\el!s DH: :5d---c
Company's Name NccbMJ Shwrl, b (:h, t½icJ Telephone: ] D~ 4c ~ 3-173/
I
Address CeA°'-1/' Spt1½':i ~c,d 1 Sc.,,l;qbur1 NC )9:i\ 4y,
Collector's Name~ fy{A [,J, · Telephone: q 1'3 1?}")-7.2;0\
signature
Date Sampled lo-7.:1-"\l..--Time Sampled \\~4o -2-~qo
Type of Process Generating Waste _________________ _
Fie 1 d Information : __,V_,1c_:r1 .. • \/cs,cc}=1c· •.Lf'. ~-_\J,"'-"-L)_,,_r,<J._I \,___,,'.$::i""""'\i\,\,'-"""fi'-'l.,,,e;"-'5,'--_,_E_,'(_,_OW\='--'='L:J.., .,,.W"=c,...,AL'-c'-'Y'-'=e C,
Tt:cc.c \-ev Pes.y\l
---1> --e_ , · L s ·
?reSe,vve:-f\fk,.,-r,-1.-1°¥-\-i~ -\'..-r
Field sample No. i(o51'1 \ (o5'3:l lioS-3\
Chain of Possession: ~ Jk,~L
signature
,c..a, ;:::)~t:e:d"'::' 1 signature
signature
Res~t~
· signature
C9 .,,............:::s: e,e:; 5:Y::----))'S"
title
title
10/iz/crz_-lo/25j,fL
inclusive dates
'.sh:, a <.51 ""-.sl-,
inclusive dates
inclusive dates
Instructions: Complete all applicable information including
signatures, and submit with analysis request forms.
J",:.C :::>c'par1mcnt or Environment,
' I lcaHh, & Natural Resources
Solid Waste Management Divuion
S~E ANALYSIS REQUEST ----···--·-··· -·-··~·.,·. S111te Laboratory ol Publir: Health
~. Dox: 28047, 306 N. Wilmington Street
'9' ~Jeigh, North Carolina 27611
Site Number NGb cis 11r~ C\S:3
Name of Sile N A--TlON A:L S TY\£l_ \-t
Field Sample Number_....,l...,C .... c_,S"'--"~'---s...-_______ _
Sile Location :Row B:r--l C OJ iNT':(
Collected Byl;~vcc. NI( \W,..-S:::t,I Date Collected IO -2 2-9 L Time -------
Agency: ---Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) ~Yf~ l Barium --
_Solid (5) Cadmium --
_ Liquid (6) Li*le [k,(\c '> Lllo\ I ~lo. I Chromium
Surface water (2)
--Lead --Mercury
Soil (3) _ Sludge (7) --Selenium --Silver --
Other ( 4) _ Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Pnrnmeter Results(mi;/1) Pzeter Results(mg/1) Organic Compounds Results(mg/1)
P&T:GC/MS
-
---✓,ArserJc ...::_o_c\ benzene
Acid:B/N Ext.
--
--Barium o. o'2, carbon tetrachloride
✓Cadmium --
MTBE .L...o.o::l chlordane
----
iChloride --
chlorobenzene --
--Chromium .L. C, .C, 4 chloroform --
--Copper L..o .o5 o-cresol --
Fluoride m-crcsol
----Iron ~o .. o5 __ p-cresol
--Lead ""-o.o'::'J cresol --
--Manganese L.o.o~ 1.4-dichlorobenzene --
--Mercury L.o. aoa:;.._ --1.2-dichloroethane
--1Nitrate 3. :':.o 1.1-dichloroethylene --
Selenium ""-o-=~ 2,4-dinitrotoluene --
Silver · ...,_ a -c:, '::i __ heptachlor
Radiochemistry ~Sulfates hexachlorobenzene --
····---Zinc L. a.a<::;, hexachlorobutadiene --
Paramelt!r Results (PCi/1) pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne
----TOC __ pcntachlorophenol ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Paramclt!r Results (Col/lOOml) --__ 2,4.5-trichlorophenol
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane
Date Received Reported by __ methoxychlor
__ toxaphene
0Jte Extractctl Date Reported 2,4-D --
Date Analyzed Lab Number
--2,4,5-TP (Silvex)
DIIS Jl 1J\ (llcviscd 2/91)
--
r-: ·n, nt. 5.,1 OCT 26 92
N.C Department of Environment,
I lcallh, &. Natun.1 Resources
Solid Waste Management Divuion
SAIJ-E ANALYSIS REQUEST State Labontory oC Public Hulth
, •. 0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Number NC\'\ 99 \ ].]'6 3S:3
Name of Sile N A-TlONA-L S 'T'f\-€f.\i
Field Sample Number __ \.,,("'o'-"5-"--'-?,,Q=:.__----------
Sitc Location MW f\:r-J (01 l(vT':(
Collected By£'2.ULC. N K. ltt\...-S;:t,I Date Collected I O -'2 '2--9 L Time ------
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) S01'"r> k, \c,
Barium --Cadmium
_Solid (5) --
No.I~ Chromium
L,~k /1.l'es lwll --
__ Surface waler (2) Liquid (6) Lead
QM ~~Jolie W0\l __ Mercury
Soil (3) _Sludge (7) Selenium --Silver
· Other ( 4) _ Other (8)
--------
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter _-Results(mg/1) (~ Organic Compounds Results(mg/1)
--P&T:GC/MS 7, Arseruc L.,o ..o \ benzene --
--Acid:B/N Ext. Barium 0_07 carbon I ctrachloride
✓Cadmium --
MTBE ~c. ... c:\ chlordane
----
iCWoride --
chlorobenzenc --
--Chromium Lc-c.::\ chloroform --
--Copper .::.a.o5 o-cresol --
--~Fluoride
m-crcsol
--Iron L., □-c:.S. p•cresol ·
--Lead Lc.c'-1 cresol --
--=:2'. Manganese L.. C. ·"' ~ --1,4-dichlorobcnzene
--Mercury L..o ... ~ga":l-1,2-dichloroethane
--~Nitrate L.. \ .oo __ 1,1-dichloroethylene
Selenium .L.O-c.o5 2, 4-dinit rotoluene --
Silver -<'...c:. _c:,';> heptachlor --
Radiochemistry ~Sulfates hexachlorobenzene --
··-·· Zinc .L..o.u~ hexachlorobutadiene --
Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nilrobenz.cne
----= pentachlorophenol TOC ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane
Date Received Reported by __ methoxychlor
__ toxaphene
Dale Extracted Date Reported 2,4-D
__ 2,4,5-TP (Silvcx)
Dale Analylcd Lab Number --
DIIS 3191 (Revised 2/91) r-;c·n ~, ~
r..::c Department of Environment,
llcallh, &. Natural Resources
Solid Waste Management Divuion
S.E ANALYSIS REQUEST State Laboratory of Public He.1l1h
•
. 0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 21611
Site Number N(,b qg I J--7'6 C\S:3
Name of Site N A--T1QN ft:L ':, TA1(J\
Field Sample Number_..,_\ ..cc(oc..c~=c....c.3_/,_ ________ _
Site Location &w A· t-J (07 ,(0T':(
Collected By]$~ULC. N l(ltC\.-':o/ Date Collected I a -'2 2-9 J. Time ------
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) sfl,Y)J~\R 2-3
Barium --Cadmium _ Solid (5) --Chromium
__ Surface water (2) llMG lli (~S l1)1( I No.11} --
_ Liquid (6) Lead --
Sk0, s l\)rl M<fl:1) Well --Mercury
_Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) ------
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter. Results(mg/1) '.j_:g~ Organic Compounds Results(mg/1)
_P&T:GC/MS 7 Arseruc 4o_c \ benzene --
--Acid:B/N Ext. Barium o.oc.,, carbon tetrachloride
MTBE ✓Cadmium L.c.c"i --chlordane
----
3"Chloride --
chlorobenzene --
--Chromium L.o -o-'i chloroform --
--Copper Lc .. c5 o-cresol --
Fluoride
. m-cresol
----
Iron --D.07 __ p-cresol
--Lead ..t...e,.o'i cresol --
--Manganese L...-c, -C~ --1,4-dichlorobenzene
--Mercury L.D_c, co?.. __ 1,2-dichloroethane
--1Nitrate ;;J. • ;;,_ d--__ 1, 1-dichloroethylene
Selenium L.o-c.oS 2,4-dinitrotoluene --
Silver .L..o.c5 heptachlor --
Radiochemistry ~Sulfates hcxachlorobenzene --
Zinc o-·,o hexachlorobutadiene --
Paramet~r Results (PCi/1) _pH hexachloroethane
__ Gruss Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne
------
TOC __ pentachlorophenol ----__ pyridine
Microbiology ----tetrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ ,inyl chloride
endrin --lindane --
Date Received Reported by --methoxychlor
__ toxaphene
D:itc Extraclc<l Dale Reported 2,4-D
__ 2,4,5-TP (Silvex)
Date AnalyLcd Lab Number --
[)IIS 3l'Jl (Revised 2/91) ,..~
!',:.C. D'cpanment or Environment,
1 lcalth, &. Natural Resources
Solid Was:c Management Divuion
S~E ANALYSIS REQUEST
-

-
State Laboratory ol P1.1blic Hc.ahn
•
. 0. Box 28047, 306 N. Wilming,on Street
Raleigh, North Carolina 27611
Sile Number N(,!') CJ9 i J7<:: C\S:3
Name of Sile N A--T1QN A-L S T'Afe. \-t
Field Sample Number _ _,_) (o""'-'5"-"3"-2-=----------
Sile Location &w A:r-l Cm )t.JT'{
Collected ByJSQ.ucE. N K ltCL-:;;'1/ ID# 5'1 Dale Collected I O -?. '2..-9 J Time ------
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) So,wrk-5 Barium --
_ Solid (5) Cadmium --Chromium
L i±t\~ 4cv<::, vile\\ Nv.S---
Surface water (2) _ Liquid (6) Lead ----Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --
Other ( 4) , _ Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter Results(mg/1) ~lliio'l°d Organic Compounds Results(mg/1)
--P&T:GC/MS ✓,Arsenic L..o-o\ benzene
Acid:B/N Ext.
--
--Barium D. ICJ carbon tetrachloride
✓Cadmium --
MTBE LO.o'j chlordane
----
iChloride --
chlorobenzene --
--Chromium L.. o. a':± chloroform --
--Copper ..c_a.,.c,~ o-cresol --
Fluoride m-crcsol
----
--~ -f-Iron L.. a.a '::l __ p-cresol
--.::I. Lead L.o-oi crcsol --
--..0,, Manganese Lo ... c~ --1,4-dichlorobenzene
--Mercury L-o.oco::;)..... __ 1,2-dichloroethane
Nitrate --.:l. 7~ __ 1, 1-dichloroethylene
Selenium L.c:>-0 c:,;, --2,4-dinitrotoluene
Silver ~c.os __ heplachlor
Radiochemistry ~Sulfates hcxachlorobenzene --
Zinc L. 0 -cs hexachlorobutadienc --
Paramder Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene
----TOC __ pentachlorophenol ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane --
Dale Received Reported by --methoxychlor
toxaphene
Date Extractc<l Date Reported 2,4-0
2,4,5-TP (Silvex)
Date Analyzed Lab Number --
DIIS Jl'JI (llcviscd 2/91)
01.7504 OCT 26 92
N.C:. Depanmenl or Environment,
. l lc3llh, &. Nalural Resources
Solid Waste Management D~ion
S,E ANALYSIS REQUEST State Ubontory o( Public He&lth
•
0. Box 28047, 306 N. Wilmington Street
· Raleigh, Nonh C..rolina 27611
Site Number NC,,D vJCJ \ J-7'6 553
Name of Site N A---T10N A--l S T)Wl\-t
Field Sample Number _ _,_\-"'(c...c5 ........ 3i,:":>-=-----------
Site Location MW A-rv Cm ,NT':r'
Collected By"lsg.uu:. N l(\t-C\...-::,)/ ID# 5"1. Date Collected I O -2 -Z..-9 L Time ------
Agency: __ Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Ground waler (1) 'Szvv,,f \,e \ 1.---
_Solid (5) Cadmium --
Well ~o. \?,
Chromium
Surface water (2) _ Liquid (6) Li~\i f\Gre,s --Lead --
E, M, C1CC<\ I\\Q)'.\J~ G l1k.ll
__ Mercury
Soil (3) _ Sludge (7) Selenium --Silver --
Other ( 4) _ Other (8) --
----
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter Results(mg/'; ,lllll,11:w) Organic Compounds Results(mg/1)
_P&T:GC/MS --3/ Arsenic L...O .o I benzene --
_ Acid:B/N Ext. Barium L... o. o'.:J carbon tetrachloride
✓Cadmium --
MTBE <C'...o -c:H chlordane
----
--iChloride
chlorobenzene --
--Chromium L.o .a:'i chloroform --
--Copper .<:..o.c'a o-cresol --
Fluoride m-cresol
----Iron o-o'.J = p-cresol
--, Lead L. c::..c4 cresol --
--L C. • c '.:> 1,4-dichlorobcnzene --
--1 Mercury Lo .,c ao·J-. __ 1,2-dichloroethane
--, Nitrate -\. al __ 1,1-dichloroethylene
Selenium L.. 0 .c.c.!:, 2,4-dinitrotol uene --
Silver .L. 0. -c, '::, __ heplachlor
Radiochemistry ~Sulfates hexachlorobenzene --
Zinc L.o.aZ hexach lorobutadiene --
Parameter Results (PCi/1) _pH hexaehloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzenc
----TOC __ pentachlorophenol ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
endrin --lindane --
Date Received Reported by --methoxychlor
__ toxaphene
Dote Extracted Date Reported 2,4-D ---_ 2,4,5-TP (Silvcx)
Dale Analy"Lcd Lab Number --
DIIS 3\IJl (lleviscd 2/91)
nt'7St;S OCT 26 92
r-.::c. Department o( Environment,
:
0I lca\lh, & Nalur.t\ Resources
Solid Wasle Management DiVUion
S~E ANALYSIS REQUEST State Uboratory o( Public Health
•
. 0. Box 2804. 7, ~ N. Wilmington Stn:.et
,, Ralcig.h, North Carolina 27611
Site Number NCD :19 ! }7<C 353
Name of Sile N A--:T10Nl}-l S T'fr€{J\
Field Sample Number __ \.,(.,,p;o,:5"'-'-'3::..4--1----------
Sile Location MW fl:~ Cm iNT'::(
Collccted BylsR.vu:. N K \t:Cl-S:::J Dale Collected IO -"2 -Z..-9 2-Time ------
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
--
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) S~"'12\e \4
Barium --
_ Solid (5) Cadmium --
L1 ~le. f1r~" ~Jell NQ, 14 Chromium --
__ Surface water (2) _ Liquid (6) Lead
\\\(s-ke t:1'&-tt EU{,,, Well Mercury
_ Soil (3) _Sludge (7) --Selenium --Silver --
_ Other (4) _ Other (8) --
----
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) rzeter. Res u I ts (mg/ I) Yii,8 (J'lt) Organic Compounds Results(mg/1)
--P&T:GC/MS -YArseruc Lo,ol benzene
Acid:B/N Ext.
--
--Barium o.o5 carbon tetrachloride
✓Cadmium --
MTBE Lo _e,'-\ chlordane
----
iCbJoride --
chlorobenzene --
--Chromium Lo.a:! chloroform --
--Copper <.a _c,=:, o-cresol --
Fluoride m-cresol
----Iron L... C -D'.;l p-cresol ·
--Lead ..<.. D ,c, i crcsol --
--Manganese L.. a-~ S --1,4-dichlorobcnzene
--Mercury L._ a_oc a'l... 1,2-dichloroethane
--Nitrate s. :;i-:... = 1,1-dichloroethylene
Selenium .L.. 0-oo=o 2,4-dinilrololuene
Silver "'-a,s;i'=i __ heplachlor
Radiochemistry =tSulfates . hexachlorobenzene --
Zinc Lc..p~ hcxachlorobutadiene --
ParJmeter Results (PCi/1) _pH hexaehloroelhane
__ Gross Alpha __ Conductivity methyl ethyl ketone
Gross Beta TDS --nitrobenzcne
----TOC __ penlachlorophenol
----__ pyridine
Microbiology --__ letrachloroethyleoe
--__ trichloroethylene
Parameter Results (CoI/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-lrichloropheool
----__ vinyl chloride
endrin --lindane
Date Received Reported by __ methoxychlor
__ loxaphcne
Dote Extracted Dale Reported 2,4-D = 2,4,5-TP (Silvcx)
Dale Analyzed Lab Number
DI IS 31'JI (llevi~cd 2/91) r-;
--
n
[D INTERNATIONAL
TECHNOLOGY
CORPORATION
• ANALYTICAL
SERVICES
ERTIF1CATE OF ANALYSIS
•
IT Corporation November 3, 1992
312 Directors Drive
Knoxville, TN 37923
Attn: Mike Sturdevant
P.O. Number: 408668.09.62
Client Project ID:
Date Received by Lab:
Number of Samples:
Sample Type:
I. Introduction
National Starch
10/24/92
Six (6)
Water
On 10/24/92, six (6) water samples arrived at the ITAS-Knoxville, Tennessee, laboratory from IT
Corporation; Knoxville, Tennessee in support of the National Starch project. The list of analytical tests
performed, as well as date of receipt and analysis, can be found in the attached report.
II. Analytical Results/Methodology
The analytical results for this report are presented by analytical test. Each set of data will include sample
identification information and the analytical results. Please note that the data are not blank corrected.
The samples were analyzed for Target Compound List (TCL) volatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
Reviewed and Approved:
Alyce . Moore
Laboratory Manager
American Council ot Independent Laboratories
International Associatlon ot Envnonmental Testing Laboratories
Amencan Association tor Laboratory Accreditation
IT Analytical Services, 5815 Middlebrook Pike, Knoxville, TN 37921 681-1-89
IT Corporation
November 3, 1992
Client Project ID: National Starch
m. Quality Control
•
Routine laboratory level I QC was followed.
.IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
The volatiles analyses were performed by purge and trap with a J&W DB-624 megabore column on a
Finnigan OWA GC/MS/DS. The sample analyses went well. There were no problems seen in final review
of the data.
2
IT Corporation
November 3, 1992
Client Prqject ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
VOLATILE ORGANIC TARGET COMPOUND LIST
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Method Blank
Lab Sample ID: VB1029
Coml!Qund Concentration Coml!Qund Concentration
chloromethane 10 u I , 2-dichloropropane 5 u
bromomethane 10 u cis-1,3-dichloropropene 5 u
vinyl chloride 10 u trichloroethene 5 u
chloroethane 10 u dibromochloromethane 5 u
methylene chloride 2 1 I, 1,2-trichloroethane 5 u
acetone 10 u benzene 5 u
carbon disulfide 5 u lrans-1,3-dichloropropene 5 u
I, 1-dichloroethene 5 u bromoform 5 u
I, 1-dichloroethane 5 u 4-methyl-2-pentanone 10 u
1,2-dichloroethene (total) 5 u 2-hexanone 10 u
chloroform 5 u tetrachloroethene 5 u
1,2-dichloroethane 5 u I, 1,2,2-tetrachloroethane 5 u
2-butanone 10 u toluene 5 u
I, I, I -trichloroethane 5 u chlorobenzene 5 u
carbon tetrachloride 5 u ethyl benzene 5 u
vinyl acetate 10 u styrene 5 u
bromodichloromethane 5 u xylenes (total) 5 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
Date of Analysis: 10/29/92
3 \VOLATJLE\TCLFRM 4/13192
682·1·89
IT Corporation
November 3, 1992
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
VOLA'PLE ORGANIC TARGEf COMPOUND UST
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well•!
Lab Sample ID: Wl733
ComllQund Concentration Compound Concentration
chloromethane 10 u 1,2--dichloropropane 5 u
bro mo methane 10 u cis-1,3--dichloropropene 5 u
vinyl chloride 10 u trichloroethene 5 u
chloroethane 10 u dibromochloromethane 5 u
methylene chloride 3 BJ I, 1,2-trichloroethane 5 u
acetone 10 u benzene 5 u
carbon disulfide 5 u trans· l ,3--dichloropropene 5 u
I, 1--dichloroethene 5 u bromoform 5 u
I, 1--dichloroethane 5 u 4--methyl-2-pentanone 10 u
1,2--dichloroethene (total) 5 u 2-hexanone 10 u
chloroform 5 u tetrachloroethene 5 u
I , 2--dichloroethane 5 u I, l ,2,2•tetrachloroethane 5 u
2-butanone 10 u toluene 5 u
I, I, I ·trichloroethane 5 u chlorobenz.ene 5 u
carbon tetrachloride 5 u ethyl benzene 5 u
vinyl acetate 10 u styrene 5 u
bromodichloromethane 5 u xylenes (total) 5 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
B Analyte was found in the blank as well as the sample.
Date of Analysis: 10/29/92
Dilution Factor: 1.00
4 \VOU.Tll.E\TCL.FRM -4/13192
682·1-89
IT Corporation
November 3, 1992 • • IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Proje<;t ID: National Starch Job Number: ITEK 52658
Client Sample ID: Well-5
Lab Sample ID: Wl734
Coml!Qund
chloromethane
bromomethane
vinyl chloride
chloroethane
methylene chloride
acetone
carbon disulfide
l, 1-dichloroethene
I, 1-dichloroethane
1,2-dichloroethene (total)
chloroform
1,2-dichloroethane
2-butanone
I, I, I -trichloroethane
carbon tetrachloride
vinyl acetate
bromodichloromethane
VOLATILE ORGANIC TARGEf COMPOUND UST
Results in i,g/liter (ppb)
Sample Matrix: Water
Concentration Coml!Qund
10 u 1,2-dichloropropane
10 u cis-1,3-dichloropropene
10 u trichloroethene
10 u dibromochloromethane
5 u 1, 1,2-trichloroethane
10 u ben:r.ene
5 u trans-1,3-dichloropropene
5 u bromoform
5 u 4-methyl-2-pentanone
5 u 2-hexanone
5 u tetrachloroethene
5 u I, 1,2,2-tetrachloroethane
10 u toluene
5 u chloroben:r.ene
5 u ethylbenzene
10 u styrene
5 u xylenes (total)
u . Compound was analyzed for but not detected. The number is the detection limit for the sample.
Date of Anslysis: 10/29/92
Dilution Factor: 1.00
5
Concentration
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
\VOLATIL6\TCLFRM 41131'1.2
IT CoIJJOration
November 3, 1992
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
VOLATILE ORGANIC TARGET COMPOUND UST
Results in µg/liter (ppb)
Sample Matrix: Water
Client Sample ID: Well-12
Lab Sample ID: Wl735
Comi!Qund Concentration Coml!Qund Concentration
chloromethane 10 u 1,2-dichloropropane 5 u
bromomethane 10 u cis-1,3-dichloropropene 5 u
vinyl chloride 10 u trichloroethene 5 u
chloroethane 10 u dibromochloromethane 5 u
methylene chloride I BJ I, 1,2-trichloroethane 5 u
acetone 10 u benzene s u
carbon disulfide 5 u lrans-1,3-dichloropropene 5 u
1, 1-dichloroethene 5 u bromoform 5 u
1, 1-dichloroethane 5 u 4-methyl-2-pentanone 10 u
1,2-dichloroethene (total) 5 u 2-hexanone 10 u
chloroform 5 u tetrachloroethene 5 u
1,2-dichloroethane 5 u I, 1,2,2-tetrachloroethane 5 u
2-butanone 10 u toluene 5 u
1, I, I -trichloroethane 5 u chlorobenzene 5 u
carbon tetrachloride 5 u ethylbenzene 5 u
vinyl acetate 10 u styrene 5 u
bromodichloromethane 5 u xylenes (total) 5 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
B Analyte was found in the blank as well as the sample.
Date of Analysis: 10/29/92
Dilution Factor: 1.00
6 \VOLATILE\TCLFRM ,1/13/9'2
682-1-89
IT Corporation
November 3, 1992 • .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52658
Client Sample JD: Well-14
Lab Sample ID: Wl736
COffil!QUDd
chloromethane
bromomethane
vinyl chloride
chloroethane
methylene chloride
acetone
carbon disulfide
l, 1-dichloroethene
I , 1-dichloroethane
1,2-dichloroethene (total)
chloroform
1,2-dichloroethane
2-butanone
I, I, I -trichloroethane
carbon tetrachloride
vinyl acetate
bromodichloromethane
VOLATILE ORGANIC TARGET COMPOUND UST
Results in µg/liter (ppb)
Sample Matrix: Water
Concentration Coml!Qund
10 u 1,2-dichloropropane
10 u cis-1,3-d.ichloropropene
10 u trichloroethene
10 u dibromochloromethane
5 u l, 1,2-trichloroethane
10 u benz.ene
5 u trans-1,3-dichloropropene
5 u bromoform
5 u 4-methyl-2-pentanone
5 u 2-hexanone
5 u tetrachloroethene
5 u I, 1,2,2-letrachloroethane
10 u toluene
5 u chlorobenz.ene
5 u ethylbenz.ene
10 u styrene
5 u xylenes (total)
u -Compound was analyzed for but not detected. The number is the detection limit for the sample.
Date of Analysis: 10/29/92
Dilution Factor: 1.00
7
Concentration
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
\VOIATILE\TCLFRM 411319'2
682·1-89
IT Corporation
November 3, 1992
Client Project ID: National Starch
• .IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
VOLATILE ORGANIC TARGET COMPOUND UST
Resuits in µgiliter (ppb)
Sample Matrix: Water
Client Sample ID: Well-16
Lab Sample ID: W1737
Compound Concentration Compound Concentration
chloromethane 10 u 1,2-dichloropropane 5 u
bromomethane 10 u cis-1,3-dichloropropene 5 u
vinyl chloride 10 u lrichloroethene 5 u
chloroethane 10 u dibromochloromethane 5 u
methylene chloride 1 BJ I, 1,2-trichloroethane 5 u
acetone 10 u benzene 5 u
carbon disulfide 5 u lrans-1,3-dichloropropene 5 u
1, 1-dichloroethene 5 u bromoform 5 u
1, 1-dichloroethane 5 u 4-methyl-2-pentanone 10 u
1,2-dichloroethene (total) 5 u 2-hexanone 10 u
chloroform 5 u tetrachloroethene 5 u
1,2-dichloroethane 5 u l, 1,2,2-tetrachloroethane 5 u
2-butanone 10 u toluene 5 u
1, 1, l •trichloroethane 5 u chlorobe11I.ene 5 u
carbon tetrachloride 5 u ethylbell7.ene 5 u
vinyl acetate 10 u styrene 5 u
bromodichloromethane 5 u xylenes (total) 5 u
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
J Indicates an estimated value less than the detection limit.
B Analyte was found in the blank as well as the sample.
Date of Analysis: 10/29/92
Dilution Factor: 1.00
8 \VOLATILE\TCL.FRM .Vl.319'2
682·1·89
IT Corporation
November 3, 1992 • • IT ANALYTICAL SERVICES
5615 MIDDLEBROOK PIKE
KNOXVILLE, TN
Client Project ID: National Starch Job Number: ITEK 52658
Client Sample ID: Well-28
Lab Sample ID: W1738
Compound
chloromethane
bromomethane
vinyl chloride
chloroetbane
methylene chloride
acetone
carbon disulfide
I, 1-<lichloroetbene
I , 1-dichloroethane
1,2-<lichloroetbene (total)
chloroform
1,2-<lichloroethane
2-butanone
I, I, I -trichloroethane
carbon tetrachloride
vinyl acetate
bromodichloromethane
VOLATILE ORGANIC TARGET COMPOUND UST
Results in 1<g/liter (ppb}
Sample Matrix: Water
Concentration Compound
10 u 1,2-dichloropropane
10 u cis-1,3-dichloropropene
10 u lrichloroethene
10 u dibromochloromethane
5 u I, 1,2-trichloroethane
10 u benz.ene
s u lrans-1,3-dichloropropene
s u bromoform
5 u 4-metbyl-2-pentanone
s u 2-hexanone
s u tetrachloroethene
s u I, 1,2,2-tetrachloroethane
10 u toluene
s u chlorobenzene
s u ethylbenz.ene
10 u styrene
s u xylenes (total}
u -Compound was analyzed for but not detected. The number is tbe detection limit for the sample.
Date of Analysis: 10/29/92
Dilution Factor: 1.00
9
Concentration
s u
5 u
s u
s u
5 u
s u
s u
s u
10 u
10 u
5 u
s u
s u
5 u
5 u
5 u
s u
\VOLATILE\TCL.FllM 4113192
682-1-89
IT Corporation
November 3, 1992
Client Project ID: National Starch
• .T ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
Job Number: ITEK 52658
WATER SURROGATE PERCENT RECOVERY SUMMARY
VOLATILE
Toluene-OS Bromofluorobenz.enc 1,2 Dichloroctbane-04
Client Sample ID (88-110%)* (86-115%)* (76-114%)*
Method Blank 101 100 92
Well-I 90 99 89
Wcll-12 88 93 84
Well-14 90 98 85
Well-16 88 94 85
Wcll-28 89 99 83
Well-5 97 100 91
*Values in parenthesis represent required QC limits.
10 \llF.c\2A.FRM
682-1-89
• • SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
01<.6 i\N IC Chain of Custody Record
Hazardous Waste Materials
Location of sampling: Generator Transporter
Treatment Facility --Storage Facility
--Disposal Facility ---Landfill
X Other: }?r,vv-k \JsJb-75ff S,'k
Company• s Name Nc,,-1-icV)lj~ Sh,vcl, ~ C,,\s-lt~\C~~lephone: Zo l/ (c33~ 17.7>1
Address Ccc\c,,,v:: ~nks ~c.,) . $:J,·sk,,vc~ b,Jc 2 9;144 '0, , I
Collector's Nam~ . J1;,; 1,&-t, c--. Telephone: q 13 1~ 3-® I
signature
Date Sampled_~\~o_-_1~'2--~:4~~1--~ _____ Time Sampled I\·. 4o --2 ·. yo
Type of Process Generating Waste _________________ _
Field Information: -Pv,voJ-€_ l.\ )e,\\
J1r1~1\ov' Yc--J C I ~~-----------------
Field Sample No. i539i', /<;'3~5 [(L/9 0
15L/o:: IS-YoG l S'L/o1
Chain of Possession:
~ 16il,AL
signature
signature
signature
Results Reported:
signature
1S-Yo1
I \L/0£3
title
title
title
,,:;yoi
1<:;Lf 01
10/2.z/qi -/o/;,3/12.
inclusive dates
inclusive dates
inclusive dates
date
Instructions: Complete all applicable information including
signatures, and s0bmit with analysis request forms.
• • SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
. OK(:d1N IC. Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator Transporter Treatment Facility --Storage Facility Disposal Facility Landfill X Other: J?r;,.,_k \v,?)\s: -r5\+ S,k
Company•s Name Nc,.ti"oYlli2 Sh,vcl, ~ (,\s,\t\\c;;,~lephone: 7o l/ (,:,33~ /]3,/
Address C C-dc,, { ~r:ih¾s ~,,,, cl ,' M ,'stb \ vc~ I ~Jc 2 s I 44
Collector.• s Name~ _ J1¼ j&,~::, c:---Telephone: c;i3 l:,-S-@\ signature
Date Sampled _ __,l~o_-_?_=_--''2--~:5__,_~J<~-----Time Sampled I J '; Yo -2 ·. yo
Type of Process Generating Waste _________________ _
Field Information: !=>1r 1'vg)-e.
,-,-_
re
Field Sample No· i'539f/, /c:;-35~ l(,4oo
15t/oS:: IS-YoG I S'Wo7
Chain of Possession:
~ 1-!v:L~,L
signature
signature
signature
Results Reported:
signature
1S"Yo1
I C:L/6?>
title
title
title
1c:Yoi
1<;Y 01
;oh.2/q-z_ -Jo/;3/C,z_
inclusive dates
inclusive dates
inclusive dates
date
Instructions: Complete all applicable information including signatures, and submit with analysis request forms.
I
N.C. Department or Environment,
) lcallh, & l','a1ural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST • S1ate Labontory or Public Health
P.O. Box 28047, 306 N. Wilmington Strccl
• Raleigh, North Carolina 27611
Site Number· NCb ~j 1 }]'D C\53 Field Sample Number_'"'/ S-"'---'3~9~V~~---------
Name of Sile N A-17QNA::L STT't€{,I-\ Site Location SA-t,1s. isV!L':{ J eowA+J C00rsry
Collected By'JSQ.uct. i'\J 1(\W,,-S;)/ ID# 5'1 Dale Collected IO -2 2-9 2 Time _____ _
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----.
Sample Type Inorganic Cr,mpounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground waler (1) Sa..vi.1,pk 1 Barium --Cadmium _Solid (5) --
lJdl Chromium / dtle Acr~s Iva. I --
Surface water (2) _ Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
LP&T:GC/MS Arsenic benzene ----Acid:B/N Ext. Barium carbon tetrachloride ------MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
' Copper o-cresol ------Fluoride rn-crcsol ------
--Iron p-cresol ----Lead crcsol ------
--__ Manganese --1,4-dichlorobcnzene
----Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotolucne ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobcnzene ----······-·· Zinc hexachlorobutadicne ----Parametu Results (PCi/1) _pH hcxachlorocthane --__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzcnc ----TOC __ pentachlorophenol --
----pyridine
Microbiology ----tctrachloroethylene
--__ lrichlorocthylenc
Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophcnol
!---vinyl chloride --endrin --lindane --Date Received Reported by --methox-ychlor
--toxaphene
Date Extracted Date Reported 2,4-0
__ 2,4,5-TP (Silvcx)
Date Analyzed Lab Number --DI IS 31 1)] (Revised 2/91)
I
KC. Department of Environment,
llcalth, & Natural Resources
Solid Waste Management DiVUion
SAMPLE A.."IALYSIS REQUEST • State Laboratory of Public H-:alth ·
P.O. Box 28047, 306 N. Wilmington Street
• Raleigh, North Carolina 27611
Site Number NC,)') :jj 1 }7''0 C\S:3
Name of Site N A·TlQNA-l STTt€/'.\-t
Field Sample Number_...,\_<;"~3'""--o-'---1 °_.__ _________ _
Site Location SAi.. I~ F:,V(L'-{ J eo l,J MJ C.00 rsry
Collected By-:}sQ.uct. N 1(\-1:Cl,.--;,:::t/ JD#___,5'"'--'1,___ Date Collected IO -2 2-9 2 Time _____ _
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) S'o,,V\1r le I ~ Barii:m --_Solid (5) Cadmium --Chromium I,; i\e Aur..s 1,kll No.\G --Surface water (2) _ Liquid (6) Lead ----
Koo \;,)al k 10c \ l --Mercury
_Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) Other (8) --
----Organic Chemistry · Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_L_ P&T:GC/MS Arsenic benzene ----
--Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--Copper o-cresol ----Fluoride m-cresol ----
--Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroethane --
--Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotoluene --Silver __ heptachlor --
' ····-
Radiochemistry Sulfates hcxachlorobenzene ----Zinc hexachlorobutadicne ----Parameh!r Results (PCi/1) --pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitroben7..cne ----TOC __ pcntachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichlorocthylcne
Parameter Results (Col/lO0rnl) --__ 2,4,5-trichlorophcnol
' --__ 2,4,6-trichlorophenol --------vinyl chloride
endrin --lindanc --Date Received Reported by __ methoxychlor
__ toxaphenc
Date Extracted Dale Reported 2,4-D --_ 2,4,5-TP (Silvcx)
Date Analy1.cd Lab Number --
l)J IS JJIJI (Revised 2/91)
I
,
!
,
t-:.C. Department of Environment,
I lcahh, & Natural Resources
Solid Waste Management Division
SA.1\1PLE ANALYSIS REQUEST • State Laboratory of Public Health
P.O. Box 28047, 3()6 N, Wilmington Streel
• Raleigh, North Carolina 27611
Site Number~N~C=D~CJ.__9_._.1_1~7~'o'-'-----'j-"-5=3 __ _ Field Sample Number_...,\~S-"---LJ~O~Q~---------
Name of Sile-'-N-'-W'--'\]'--'--"-ONLI'-'-'A:L-=-...csc....T)'\~I '-'-fi"'-'-'-J-'-\ __ _ Site Location S,'\i..-1'.:, ?.:,V(!._'-{ J
ID# 5'1 Dale Collected I O -2 2-9 2 Collected ByJ$'2.uct. NI( rt-Cl-Set/ -'='----'---Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) SQM-y)k 2% Barium --Cadmium _ Solid (5) --
No. 272
Chromium L½:k fkres \~)ell --__ Surface water (2) _ L:quid (6) Lead --
S~ew Si,~\t\\ril\S ½)ell --Mercury
_Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_L P&T:GC/MS Arsenic benzene ------Acid:B/N Ext, Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol --------Iron __ p-cresol --Lead cresol ------
--__ Manganese --1,4-dichlorobenzene
--__ Mercury 1,2-dichloroelhane
Nitrate __ 1, 1-dich loroethylene ----Selenium 2,4-dinitrotoluene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----······-~ Zinc hexachlorobutadicne ----Parameter Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha --Conducti,ity --methyl ethyl ketone
Gross Beta TDS nitrobenzcne ----T0C __ penlachlorophcnol --
--__ pyridine
Microbiology ----tclrachloroelhylcnc
--__ trichloroethylcne
Parameter Results (Col/IOOml) __ 2,4,5-trichlorophenol --
--__ 2,4,6-trichlorophenol --
--__ wnyl chloride --endrin --
lindanc
Date Received Reported by __ methoxychlor
--toxaphene
D"le Extracted Dale Reported 2,4-D
_ 2,4,5-TP (Silvcx)
D"tc Analyzed Lab Number --DI IS 3191 (Revised 2/91)
~.C. Department of Environment,
I Jc:a1th, & Natural Rcsourec:s
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST • State Laboratory of Public Heallh
P.O. Box 280-i7, 306 N. Wilmington Str;et
• Raleigh, North C-arolina 27611
Sile Number NC)') C\9 I }]i C\S:3
Name of Site N A--TlON A-l S T'f\f[J-\
Field Sample Number_--'-l~Sc....L_/-"o_,_I __ ~-------
Site Location S,4-i.,1:c, t2c,Vf2_'-( J eowW C00r0'fY
Collected By]5'2.uu:. N I( \tc\.,.;:a) ID# 5'1 Dale Collected IO -2 2-'l J. Time ------
Agency: Ha7,ardous Waste Solid Waste __Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) S~11ypk 5 Bariur:1 --_Solid (5) C~dmiur:i
Chro:nium
L·1 &\e-Ac.re~ ~Jell No-s -· __ Surface water (2) _Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) Selenium --. Silver --Other ( 4) Other (8) --
----Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
...L._ P&T:GC/MS Arsenic benzene ----Acid:B/N Ext, Barium carbon tetrachloride ------MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol --------Iron p-cresol ----Lead cresol ------
--__ Manganese --1,4-dichlorobenzcne
--__ Mercury 1,2-dichloroethane --
--Nitrate 1,1-dichloroethylene ----Selenium 2,4-dinitrotolucne ----Silver heptachlor ----Radiochemistry Sulfates hexachlorobenzene ----······-Zinc hexachlorobutadiene ----Parameter Results (PCi/1) --pH hexachloroethane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne ------TOC pentachlorophcnol ----
--__ pyridine
Microbiology --__ tetrachloroethylene
----trichloroethylene
Parameter Results (Col/lO0ml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by __ methoxychlor
__ toxaphene
D"tc Extracted Date Reported 2,4-D --_ 2,4,5-TP (Silvcx)
Date Analyzed Lab Number --])JJS 3191 (llcvi!>cd 2/91)
i i
I
i
;
N.C. Department or Environment,
I lcalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST • State I....aboruory or Public Health
P.O. Box 28047, 306 N. Wilmington Street
• RAieigh, North Carolina 27611
Site Number NCD vJ9 \ 17''(; C\S:3
Name of Sile N A--TlONA-l S T)'t€{,li
Field Sample Number_~\_S:::~(=0_2 _________ _
Collected BylStucE. {'J I(. 11-ct-Sct/ ID# 5'1 Dale Collected I a -"2 2-9 L Time ------
Agency: --Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds --
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) So,,)lvf\e1 No. I l-Barium --Cadmium _Solid (5) --Chromium Li~~ Acre.':, \1,k\l No.11---Surface water (2) _ Liquid (6) Lead --
8. M' G 6o,\.1Wl-1i 1 (, ~u __ Mercury
·_ Soil (3) _ Sludge (7) Selenium --I Silver --Other ( 4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
_L_P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol --Lead cresol --------__ Manganese 1,4-dichlorobenzcne --
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinilrotoluene ----Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta --TDS nitrobenzcnc ----
. TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lOOml) __ 2,4,5-trjchlorophenol --__ 2,4,6-trichlorophenol ------__ vinyl chloride --cndrin --lindane
Date Received Reported by --__ methoxychlor
--toxaphene
Dote Extracted Date Reported 2,4-0 --
Date Analyzed Lab Number
__ 2,4,5-TP (Silvcx)
DIIS 3191.(llcviscd 2/91) --
N.C. Department of Environment,
I lcalth, &:. Natural Resources
Solid Waste M11nagement Di\-Uion
SAMPLE ANALYSIS REQUEST • State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Stn::ct
• Raleigh, North C.arolina 27611
Sile Numbcr_N'--"-""'C"--D'---'j.,_j.u..l _,}'-'-7...:._'t_C\'"'-S:=3 __ _ Field Sample Nurnber_~jc;-<-~~/ ()_") __________ _
Name of Silc~N_@_~ON~' A:L~_S_Tflff~='~I-\ ___ _ Sile Location Sfli... I'., lsVP-'J )
ID# 5'1 Dale Collected IO -2 2.-9 L Collcclcd By-:\s'2.uct. N I/ \ffi_..';;(:t/ ~~~-
Time ------
Agency: Hazardous Waste Solid Waste __Lsupcrfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Gr~und water (1) ~D\j) \4 Barium --_ Solid (5) Cadmium --Chromium
Li ~!e Acl'\'S 102\I N?.14 --· Surface water (2) Liquid (6) Lead --
Mrs x'.efl,vr\, 9 \ lee \2i}lll __ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver
_·_ Other ( 4) --_ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results (mg/I)
_L_P&T:GC/MS Arsenic benzene ----
--Acid:B/N Ext. ' Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride ·chlorobenzene ------Chromium chloroform ------
--__ Copper o-cresol --Fluoride m-cresol ------Iron __ p-cresol --Lead cresol --------__ Manganese 1,4-dichlorobenzene ----__ Mercury --1,2-dich loroclhane
--Nitrate __ 1,1-dichloroelhylene --Selenium 2,4-dinitrotoluene --Silver __ heplachlor --Radiochemistry Sulfates hcxach lorobenzene ----Zinc hexachlorobuladiene ----Parameter Results (PCi/1) _pH hexachloroelhane --__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela --TDS nitrobenzcne ----TOC __ penlachlorophenol ----__ pyridine
Microbiology --__ letrachloroelhylene
--__ lrichloroethylene
Parameter Results (Col/IOOml) __ 2,4,5-trichlorophenol ----__ 2,4,6-lrichlorophenol
--__ vinyl chloride --endrin --lindane --Dale Received Reported by melhoxychlor --
--loxaphcne
Dole Extracted Date Reported 2,4-D --__ 2,4,5-TP (Silvcx)
Dole Analyzed Lab Number
DI IS 3191 (Revised 2/91) --
N.C. Department of Environment,
llcallh, & Natural Resources
Solid Waste Management Division
s,wLE ANALYSIS REQUEST State Labon.tory of Public Health
•
P.O. Box 28047, 306 N. Wilmington Stree1
Raleigh, North Carolina 27611
Site Number NCI'\ qg \,}7'6 C\53
Name of Sile N A-llON (H_ S T'f\f()t
Field Sample Number __ l_s::l\~=()~L~/ ________ _
Collected By--:\s'2.uct. \1\J I( \te\_..;:Q/
Site Location SA-t-Is. rsvp .. :--{ )
ID# 5'1 Date Collected I O -'2 2-9 L -'""----'--Time ------
Agency: Hazardous Waste Solid Waste _L_superfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) ?-,Ll'\-W \(. Barium
iR..1? --_ Solid (5) Cadmium --Chromium --__ Surface water (2) _ Liquid (6) Lead --
--Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) _ Other (8) --
----Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
..L_P&T:GC/MS Arsenic benzene ----_ Acid:B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ------Chloride chlorobenzene ------Chromium chloroform --------__ Copper o-cresol --Fluoride m-cresol --------Iron p-cresol ----Lead cresol ----------Manganese 1,4-dichlorobenzene ----__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene --Selenium 2,4-dinitrotoluene ----Silver __ heplachlor --Radiochemistry Sulfates hexachlorobenzene ----Zinc hexachlorobutadiene ----Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Bela TDS nitrobenzene ----TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --Date Received Reported by --methoxychlor
--toxaphene
Date Exlraclc<l Dale Reported 2,4-D
_ 2,4,5-TP (Silvcx)
Dale Analy,cd Lab Number --DI IS 3191 (Revised 2/91)
r,,:.c Dc:partmc.111 of ,cn...,rorirnc.r.i., ..., --_. _ .. -.. -

.

_

.. -· .. ___ ... _
1 lcallh, &. Naiun.l Rc.wurca
P.O. Bo.t ~7. Mr-;_ ·,.;,:,imini,1.or, :-.1r-t.c\
R.alci.,h, North Carolina 27611
Solid Warn: Managcmcr\t Divuion •
Sile Number NCI') ~ 9 I }]"ti °'55 Field Sample Number_'-\ S~·~· c;~-________ _
Na me of Site N @ON (tL S T}\fL r\ Sile Location SAL-15R,vi2'.~' { Qgw1't-N Cov~-1 i
Collected By]sR.uct. N IC\t-c\--S:::t/ ID# 5'1 Dale Collected IO -2 2-9 2 Time \I: 40
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
------
Sample Type Inorganic Compounds Rcsulls(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground waler (1) 'S f't M p L--f-j_ Barium --
_Solid (5) Cadmium --
( 11llt Ac.f£~J
Chromium
I --
__ Surface water (2) _ Liquid (6) WSLL No. Lead --
--Mercury
_Soil (3) _ Sludge (T) Selenium --. Silver --
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/!) (mg/lq:) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
Z Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane
------
Chloride chlorobenzene
------
Chromium chloroform ------
--__ Copper o-crcsol --
Fluoride m-crcsol
------
--Iron p-crcsol ----
Lead ere.sol ------
--__ Manganese --1,4-dichlorobenzcne
--__ · Mercury __ 1,2-dichloroclhane
--Nitrate __ 1,1-dichloroethylcne --Selenium 2,4-dinitrotolucne --Silver __ hcptachlor --Radiochemistry Sulfates hexachlorobcnzene ----
··----Zinc hcxachlorobutadiene
----
Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Al~ha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnzcne ------
TOC __ pcntachlorophcnol ----__ P)Tidine
Microbiology --__ tctrachloroethylcne
--__ trichloroethylcne
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophcnol
------vinyl chloride
cndrin --lindanc --
Date Received Reported by --mctho,ychlor
--toxaphcne
Date Extracted Date Reported __ 2,4-D
__ 2,4,5-TP (Silvcx)
Date Analyzed Lab Number
l)J[S 31 1)\ (l~cviscd :?/91)
--
r,;.C l)cp.inmc.11~ v: bhlr.:...imcr,;, "•-··--.,. ..... , ... ,.
llcallh, &. Natural R.c.wurcu P.O. li-0.1 z~;.o.n, 30(. :-;. -V.'1imir,£lor. ::.:rec,
Solid Waste M•nagcmcnl DM<ion • lulciV,, North Carolina 27611
Site Number NC.b ljCJ i }7''6 C\~ Field Sample Number_-'-\A~-'-"--"""----------
Name of Site N @ONA-l S TT\1;[.\i Site Location SA-L\5 l'.,U e. 'I . f2ow14-N Co V (0-1 i
'
Collected By:];R.ucc. N )( rt-ct-So/ ID# _,">'1 Date Collected IO -'2 2-9 2 Time ------
Agency: --Hazardous Waste ·--Solid Waste _Lsuperfund TCLP Compounds
Sample Type Inorganic Compoun_ds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Gr~und water (1) SAmPU::. \(o
Barium --Cadmium Solid (5) --Chromium
Lt. TT\.J: ~CffS \>Jf:U No. 10 --
_ Surface water (2) Liquid (6) Lead --__ Mercury
_ Soil (3) _ Sludge (7) \'ZotJ WOLFE J C)WNfJ, Selenium --Silver --
_ Other (4) Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
L Acid:B/N Ext. ----
Barium carbon tetrachloride
----
MTBE Cadmium chlordane
------
Chloride chlorobenzene ------
Chromium chloroform ----
--__ Copper o-crcsol --
Fluoride m-crcsol ------
--Iron p-crcsol --Lead· crcsol ------
--__ Manganese 1,4-dichlorobenzene --
--__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1, 1-dichlorocthylenc --Selenium 2,4-dinit rotolucnc
----
Silver __ heptachlor
--
Radiochemistry Sulfates hcxachlorobenzene
----
.. Zinc hcxachlorobutadiene ----
Parameter Results (PCi/1) --pH hexachlorocthane
_._ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzcne
------
TOC __ pcntachlorophenol ----__ pyridine
Microbiology --__ tetrachlorocthylcne
--__ trichlorocthylcne
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol
--
--
__ 2,4,6-trichlorophenol
--
--__ ,inyl chloride
--cndrin --lindanc --
Date Received Reported by __ methoxychlor
__ toxaphenc
Date Extractcu Dale Reported 2,4-D --2,4,5-TP (Silvex)
Date Analyzed Lab Number --
DIIS 3191 (Revised 2/91)
N.C Ocp.inmc.111 01 L;.t1v11011mu .. , .J• ........ ___ • _ •• -·-.. __
1 lcalth, & Nalural Rcwurces
P .0. Box U,.::1-n, 306 1'. Wilrr.ini;tDn Su-c.c1
Ralcii}\, North Carolina 27611
Solid Was<c Management D~-is;on.
Site Number NCD CJ91 17'6 °'~ Field Sample Number _ ___,_\--"---'--o'=-J-7 ________ _
Name of Site N A--IJQN A-L S TMrJ\
Collected By]sQ.ucE.. N I/ li-0,,.S:::t,I ID# 5'1 Date Collected IO -"2 2-9 L Time ------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) S 6:tl'\ PU::
Barium
2C8 --
_Solid (5) Cadmium --Chromium
L1TTl£-oce0;, \\Jell No. Z.S --
__ Surface water (2) _ Liquid (6) Lead --
.S: ~etve S1' l'\1 M(t)S \\/e,tR
__ Mercury
_Soil (3) _ Sludge (T) Selenium --Silver --
_ Other (4) Other (8) --
----
Organic Chemistry Inorganic Chemistry --'
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
::Z Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------
Chloride chlorobenzene ------
Chromium chloroform
------
__ Copper o-cresol
----
Fluoride m-crcsol ----
--Iron __ p-cresol --Lead crcsol ------
--__ Manganese --1,4-dichlorobcnzcne
--__ ·Mercury 1, 2-dich lorocthane
--Nitrate __ 1,1-dichlorocthylcnc
--Selenium 2, 4-dinit rotolucnc --Silver __ hcptachlor --
Radiochemistry Sulfates hexachlorobenzene ----
··----Zinc hexachlorobutad icnc ----
Paramdcr Results (PCi/1) _pH hcxachloroethanc
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnzcnc
------
--TOC __ pentachlorophcnol
--__ pyridine
Microbiology ----tctr a ch lo roet hylcnc
--__ trichlorocthylcne
P<tramctcr Results (Col/JOOml) --__ 2,4,5-trichlorophcnol
----__ 2,4,6-trichlorophcnol
----__ ,inyl chloride
cndrin --lindanc --
Date Received Reported by --mcthoxychlor
__ toxaphenc
Date ExtractcJ Date Reported 2,4-D
__ 2,4,5-TP (Silvcx)
Date Analy,cd Lab Number
DI IS 31 1)1 (llcviscd 2/91)
--
N.C OcJ)<lnmenl 01 l.;,l\V\ronmcm,
J lcallh, & 1'-alunil ~urce£
P.O. u-Ox 2SO·l7, 306 N. Wilrninf!Or. 5tn;ct
Ra!ei.h, North Carolina 276ll
Solid Wa,te Management Division •
Si1e Number NCD 09 i J7'o' °iU.
Name of Site N A-nON A-L S Ttt€[J\
Field Sample Numbcr _ _,_j-~. Lt.:cc:":.i.f3L.. __________ _
Site Location SA-U1l?,ve.y ' Rrnvf'l-/v Cou f'--)-1 i
'
Collected By]sr.ucc. N K ttc\---ScJ/ ID# 5"1 Date Collected IO -2 7..-9 ] Time -------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds ----
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentn1te Comments Arsenic --
/Gro,und water (1) fu0i,f\.e t)
Barium --
_ Solid (5) Cadmium --Chromium
Ldl-le Auu, Cve\\ \~o, '.) --Lead Surface water (2) Liquid (6) ----__ Mercury
_· Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Po ram et er Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
·P&T:GC/MS Arsenic benzene
L Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane
------
Chloride chlorobenzene ------
Chromium chloroform ------
--__ Copper o-cresol --
Fluoride m-crcsol ----
--Iron __ p-cresol --Lead cresol
------
--__ Manganese --1, 4-dichlorobcnzcne
--__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylcne
--Selenium __ 2,4-dinitrotolucne --Silver __ heplaehlor --
Radiochemistry Sulfates hexachlorobenzene ----
··----Zinc hexachlorobutadiene
----
Parameter Results (PCi/1) _pH hexachloroelhane --
__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnz.cnc
----TOC __ pcnlachlorophenol
----__ pyridine
Microbiology ----tetrachloroet hylcne
--__ trichloroethylene
Paramcltr Results (Col/!OOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophcnol
--__ vinyl chloride --cndrin --lindanc --
Date Received Reported by --methoxychlor
__ toxaphene
Date Extracted Dale Reported 2,4-0
__ 2,4,5-TP (Silvcx)
Date Analr,cd Lab Number
/)/IS 3J!JJ (llcviscd 2/91)
--
u.-...... , ...... _...., .... ··-----P.O. Box 28,.).47, 306 K Wilmlnr,:i-n Street
R.aleiV,, North Carolina 27611
r-,:.C Dcp.inmcnt O[ t.l'IYln.mmc.n;,
llcallh, & l'<alural Resoun:u
Solid Waste Managcmenl D~'aion • Sile Number_,__N=C~b~~~9_._I ..... J-.,_.._]'6_'.),_,_5~3 __ _
Name o: Sile--'-N---'-~-'--'\J-"-. ""ON_._,_,_' {\-L-'-'---_S=.cT)W--'-'-'"-'"-r\ ___ _
Field Sample Number_-1-l~..,_-'--"-'------------
Sile Location SAL-15 y,\J ~L/ r QovJ11riv C(!u ~-, i
'
Collected By-:}sP..ucE. N l(\tCl,,-S:::t/ JD# 5'1 Date Collected I O -?. 2-9 J. Time ------
Agency: Hazardous Waste Solid Waste __L'superfund TCLP Compounds --
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments · Arsenic --Barium
/Grdund waler (1)
r \'L --
Solid (5) 01\-m PLf✓:-Cadmium --
Ac~\S~
Chromium
L1n\ft \vi:;u. rJc. 12 --
__ Surface waler (2) _ Liquid (6) Lead --
E.M. Goot>MBNj 1 f-, wi:.u.
Mercury
_Soil (3) Sludge (7) --Selenium --Silver --
_ Other (4) Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS AisCnic benzene
::Z Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane
------
Chloride chlorobenzene ------
Chromium chloroform ------
--Copper o-cresol ----
Fluoride m-crcsol
------
--Iron p-crcsol ----Lead crcsol
------
--__ Manganese --1, 4-dichlorobenzcne
--__ Mercury __ 1,2-dichloroethane
--Nitrate __ 1, 1-dichloroethylene --Selenium 2,4-dinitrotoluene --Silver __ heptaehlor
Radiochemistry --Sulfates hexaehlorobenzcne ----
··----Zinc hexach lorobutadiene ----
Paramekr Results (PCi/1) _pH hexaehloroethane --
__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobc:nzcnc ------
TOC pentachlorophenol ----
----pyridine
Microbiology --__ tetrachloroethylenc
--__ trichloroethylcnc
Parameter Results (Col/!OOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-triehlorophenol
--vinyl chloride ----cndrin --lindane --
Date Received Reported by --methoxychlor
--toxaphcne
Dote Extracted Date Reported 2,4-D
__ 2,4,5-TP (Silvex)
Dale Analyzed Lab Number --
DIIS 3\CJJ Olcviscd 2/91)
r-:.c Uc:pannit.rn \JI L,nvuvuu, ... , ...
J Ic.allh, & Natunl Rc.wurcu
Solid Waste Management Divis.ion
P.O. Uox 2.&:)47, Y..16 :,.. W11m1npon .:>trcct
Ralcii,h, Nor\h Carolin• 27611 • Site Number-'--'N'-"C.ccD'-'-q-'---9-'-'/_J'---7-'--''6"--'C\""-5-"'-3 __ _
Name of Site N A--J]ON M-S T'A-l:{, \-\
Field Sample Number _ __L)A"'--'="--,"-------------
Sitc Location Sf\-L-111:,vl'-/ 1 Qp1-vf'I-N C&vt0-, J
Collected ByJS~uct. N IC.\Wv'-:cJ ID# 5'1 Date Collected I O -'2 2-9 J. Time -------
Agency: ___ Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
---
Sample Type Inorganic Compounds Results(mg/1)
En"ironmcntal Concentrnte Comments Arsenic --Barium
· /Gr~und water (1) \m,1rl;, \4 --
Solid (5) Cadmium --
No 14
Chromium
li:lt\e Aue, l~el\ --
__ Surface water (2) _Liquid (6) Lead --
1"1 rs_ 1<€1,,Jk r,l\eY wJ __ Mercury
_Soil (3) _ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
L Acid:B/N Ext ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane ------
Chloride chlorobenzene ------
Chromium chloroform ------
--__ Copper o-cresol --
Fluoride m-cresol ------
--Iron p-cresol --Lead crcsol
------
--__ Manganese --1,4-dichlorobenzcne
--__ Mercury 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
--Selenium 2, 4-dinit rotoluene --Silver __ heptachlor --Radiochemistry Sulfates hexachlorobenzene ----
··---Zinc hexach lorobutadiene ----
Pam meter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcn7..cnc
----TOC __ pcntachlorophenol
--
--__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophcnol
------vinyl chloride
endrin --lindanc --
Dale Received Reported by --methoxychlor
__ toxaphene
Date Extracted Date Reported 2,4-D --__ 2,4,5-TP (Silvcx)
Dale AnalyLcd Lab Number --
DIIS 3191 (ltcvi!-cd '2/91)
• • SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
. T \\)o12.1drN IC..
Chain of Custody Record
Hazardous Waste Materials
CERCLA
Location of Sampling: Generator Transporter
Treatment Facility ---Stbrage Facility
--Disposal Facility =Landfill
./ Other: f1',Vc,k \,1\elh ()\± Sd-<-
Company• s Name /\,)cc.hoxw~ Shwd, & C\--.,.,1iul~ Telephone: ] O~ (j, ~ 3 -I 7:i/
I
Address CeAecv· s,~y 1\v.s ~,,d / Sd1s\)U('{ NC )£,\ t.fy,
I '~ I
collector's Name~ ·Jib 11,J\= · Telephone: 3 IS
signature
Date Sampled i ()-L'l-'11---Time Sampled \\;!.\o -2.~yo
Type of Process Generating waste _________________ _
Field Information: V1rLvc..}e, ~,)I?\\ ;3,G\.'.I,\ fk-S Fv-oi'.':\
Tn,._,:_, ev
---f> ·Z..
?rec.,,e.vVc'.,,
. Field sa,mple No. 1(051·1
Chain of Possession: ~~ •ffi-;,k,L
signature
signature
signature
Results Reported:
signature
'
I C,5'?o IG S-31
fee.Sex ued . 1\~c_,.,__
11oc;33 \(,S-yt
10/22h2---10/2,Jr,_
inclusive dates
title inclusive dates
title inclusive dates
title date
Instructions: Complete all applicable information including
signatures, and submit with analysis request forms.
• • SOLID WASTE MANAGEMENT DIVISION
SUPERFUND SECTION
. T l\)oQ.6\1\-N IC Chain of Custody Record
Hazardous Waste Materials
Location of sampling: Generator Transporter Treatment Facility --Storage Facility --Disposal Facility =Landfill 7 Other: ?1',Vc,k L1\e_\ls ()w SCI-<-
\ 1 .• i 1 · h I Company Is Name Nc,_,ncfY)a~ S\-:cwrl, [. Ck, 1\\lCClf Telephone: 1 ()~ (,(' ~ 3-I T.'i( I
Address CeAo..,· Sp11\,,~<, ~c-~ J ScJ1s\;wr' NC ).?,l Lil}
Collector's Name~ Jt l,J= Telephone: 9 15 l?J;i-7.52,0 I signature
Date s amp 1 e d_~I ~0'---_7"'✓"''2_-_°\~1---~----,----T i me s amp 1 e d \\ ~ 4 O -2. :; L[ o
Type of Process Generating Waste _________________ _
Field Information: Vn\1,.,k. \),\q\\ 5Gwfk-S Fv-o:iYI
e.v
Field Sample No. i(r;S'l.·1
Chain of Possession: ~ :1k.iu.L signature 10/22h2--/o/;~/r2-
inc1usive dates
signature title inclusive dates
signature title inclusive dates
Results Reported:
signature title date
Instructions: Complete all applicable information including signatures, and submit with analysis request forms.
N.C Department o( Environment,
J lcallh, & Nah.1ral Rcwurcc.1.
Solid Waste Management Division
P.O. i.>O~ ~7, ,:,-,SN. Wilm1npor, !)tree\
R.alci£h, North Carolina 27611 • Site Num bcr--'--N"-"C""--b'-'--~-'-1~\_J-L...L.]'t_:_____;C\'-'-S:-'='3 __ _
Name of Site N A--T7QNl)-L STT\f[J\
Field Sample Number_->...:\ ~"-'-:=:._=-1->----------
Sitc Location 1?.,r,W A-r-J Ca, lN<'::(
Collected By1s'2.ucc. N I( ltwS:::t/ ID# 5'1 Date Collected I a -'2 7 __ 9 2 Time -------
AgenC)C ---Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Ground water (1) ~v19lt l --
_ Solid (5) Cadmium --Chromium
_ Liquid (6) Li*/e Wll/ '> L\lQ\ I ~lo. \ --
__ Surface water (2) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium --Silver --
Other ( 4) _ Other (8) ------
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter Results(mg/l)(mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS -3/ Arsenic benzene --
_ Acid:B/N Ext. Barium carbon tetrachloride
✓ Cadmium
--
MTBE chlordane
----
--iChloride
chloroben2ene --
Chromium chloroform --
--Copper o-cresol --
--7 Fluoridc m-crcsol --
--~ ::::,
p-cresol · --
--
creso\ --
--Manganese 1,4-dich\orobcnzene --
--Mercury 1, 2-dich loroethane
--1Nitrate __ 1,1-dichloroethylene
Selenium 2, 4-dinit rotoluene
Silver __ heptachlor
Radiochemistry -:;!'__Sulfates hexachloroben2ene --
····---Zinc hexachlorobutadiene --
Parameter Results (PCi/1) _pH hexachlorocthane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcn1.cnc
----TOC __ pcnlaehlorophcnol --
--__ pyridine
Microbiology --__ lelrachloroethylene
--__ lrichloroethylene
P<irametcr Results (Col/!OOml) --__ 2,4,5-lrichlorophcnol
----__ 2,4,6-trichlorophenol
------,;nyl chloride
cndrin --lindanc --
Date Received Reported by --methoxyehlor
--toxaphcnc
D,te ExtrJcicd Dale Reported 2,4-D --__ 2,4,5-TP (Silvcx)
Dale Analy1.cd Lab Number --
l)J\S 3\!Jl (llcviscd 2/91)
r,.:.C Ocpanmcnt of Environment,
t lcallh, & 1'alvral Re.sources
Solid Waste Management Di-vu.ion
P.O. Box 2&,47, Jv6 N. Wilmin~or. Sll--c.tl
~lcith, Nonh Carolina 21611 • Site Number_._NO-"C"'-'b'--'-CJ-'-Cj-'-'\_J-.~7-'-'b-'---'3-"--5=3 __ _
Name of Sile N A-T\QN A-L S Tt\t'.(. r\
Field Sample Number __ \!'-(.i.aQ~c,-=•='------------
Sile Location :J?,,-,w Pr tJ Ca, )(\..lT'--r'
Collected ByJS~uu:. N 11.\i·C\.,S:)/ Dale Collected IO -L 2-9 J Time -------
Agency: ---Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
---
Sample Type Inorganic Compo~nds Results(mg/1)
Environmental Concentrate Comments Arsenic --
/Ground water (1) ?iM")° le, \ (a
Barium --
_Solid (5) Cadmium --
l0Jll t)0 .IG Chromium
L,~k Aves --
Surface water (2) Liquid (6) Lead
----
~cm \i\lQ\~L \\10 \ I Mercury
_ Soil (3) _ Sludge (7) --Selenium --Silver --
Other ( 4) _ Other (8) ----
. --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) P✓,,;:eter. Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS --YAisewc benzene
----
Acid:B/N Ext. Barium carbon t otrachloride
--✓Cadmium --
MTBE chlordane
----
iChloride chlorobenzene
----
--Chromium chloroform --
Copper o-cresol
----
--2 Fluoride m-crcsol --
--Iron __ p-creso\ ·
;Lead crcsol
----
--jz'. Manganese --1,4-dichlorobcnzcne
--Mercury --1,2-dich \orocthane
--~Nitrate 1, 1-dichloroethylene --
Selenium 2,4-dinit rotol ucne
Silver __ heptach\or
Radiochemistry ~Sulfates hcxach lorobcn,.ene --
··-·· Zinc hexaehlorobutadiene --
Paramettr Results (PCi/1) --pH hexachlorocthane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcn1..cne
----TOC __ pentach\orophcnol --
--__ pyridine
Microbiology --__ lctrachloroethylene
--__ trichloroethylenc
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol
--
--
__ 2,4,6-trichlorophcnol
--
----__ vinyl chloride
endrin --lindanc
Date Received Reported by __ methoxychlor
__ toxaphene
Dote ExtroctcJ Date Reported 2,4-0
__ 2,4,5-TP (Silvcx)
· Dote Analy,cd Lah Number --
l)IIS 3\'Jl (llcvi:.cd 2/91)
f'\.C Department of Environmcnl,
llcalth, & Natunl R.esourcc.1
Solid Waste Managcmcnl D~ion
.;,ro-,.1..1. ~-.-,...,, ........ ___ _ P.O. Box 2&0,0, 3u6 K Wilminpor, 5Lr,;ct
R.alcii)\, North Carolina 27611 • Sile Number_,_N_,_,C'""-b'---1 '-01--'-\ j-'-'-\ ~1---']--''t_9'_,_\"-'3"-----Field Sample Numbcr_...:l...cGJc..·=----il _________ _
Name of Sile___,_N~f>t':..c'fl'--'-0!=>--:Jf!:L"""'""_S=..cT'f&-'--='-'-J'-'---\ __ _ Sile Location :Row B·rJ
Colleeled By]sr..ucE. NI( li:d--S:::J ID# 5'1 Dale Collected IO -2 2-9 2 Time -------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
------
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Ground water (1) S0Wf v. 7 3 --
_ Solid (5) Cadmium --Chromium
l1··\tL Acas IA)1II do.12> --
__ Surface water (2) _ Liquid (6) Lead --ii" Mercury
_ Sludge (7) Sk.-Vt' s 1)11 f'.Y!J:i),1 > We l/ --
_Soil (3) Selenium --Silver --
_ Other (4) _ Other (8) ----. --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter_ Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arseruc benzene
--Acid:B/N Ext. ✓,Barium --carbon tetrachloride
--MTBE ✓Cadmium --chlordane
----
5Chloride --
chlorobcnzene --
--Chromium chloroform --
--Copper o--cresol --
Fluoride
. m-crcsol
----
--Iron p-cresol --
Lead crcsol
----
--Manganese 1,4-dichlorobenzene --
--Mercury 1,2-dich lorocthane --
--iNitrate 1, 1-dichloroethylene --
Selenium 2,4-dinit rotoluene --
Silver __ heplachlor
Radiochemistl)' ~Sulfates hexachlorobenzene --
····---Zinc hexachlorobut adiene --
·Pan1metcr Results (PCi/1) _pH hcxachloroelhane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcn7..cne
------
TOC __ pentachlorophenol
--
--__ pyridine
Microbiology ----letrachloroethylcne
--__ trichloroethylenc
Parameter Results (Col/!OOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophenol
------,inyl chloride
cndrin --lindanc --
Date Received Reported by --methoxychlor
__ toxaphene
DJle ExtrJctc<l Date Reported 2,4-D --2,4,5-TP (Silvex)
Date Analyzed Lab Number --
DI IS 3191 (Hcvi:-cd ~/91)
t-,:.C Dep.artmcnl ol .E.rwironment,
1 lcallh, & Natural Re.sou~
Solid Waste Management Divis.ion
P.O. Uox :z.&:,47, 3r06 K Wilmington Strc<::
Ju.lei~. North Carolina 27611 • Site Number--'--'N~G"'-'b'--'--1'.J-'-9-'-'\_},_]_,_'t___,9'_,_S:-=3 __ _
Name of Site N A--TlONt½, Sl}-tfL,\-t
Field Sample Number _ _,_),,.-""'-=3"-2-=----------
Site Location MW R-tJ C OJ lNT'·:r'
Date Collected t O -'2 2-9 J. Time -------
Agency: Hazardous Waste Solid Waste _Lsuperfund TCLP Compounds
------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Gro,und water (1) ~f\e,5 --
_ Solid (5) Cadmium --Chromium
_Liquid (6) LiM\e Acv('.i lAkll N8.S' --
__ Surface water (2) Lead --
--Mercury
Soil (3) _ Sludge (7) Selenium --Silver --
Other ( 4) _ Other (8) ----
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Pzeter_ Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arseruc benzene
--✓,Barium --
--Acid:B/N Ext, carbon tetrachloride
MTBE ✓Cadmium --chlordane
----
iChloride --
chlorobenzene --
--Chromium chloroform --
--Copper o-cresol --
--=z: Fluoride m-cresol --
--Iron p-cresol --
Lead crcsol
·----
--Manganese --1, 4-dichlorobenzene
--Mercury __ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene
Selenium 2,4-di nitrotol uene
Silver __ heptachlor
Radiochemistry ~Sulfates hexachlorobenzcne --
··--··-Zinc hcxach lorobutadicnc --
Paramt:tt!r Results (PCi/1) _pH hexachloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnz.cnc
------
TOC __ pcntachlorophcnol ----__ pyridine
Microbiology --__ tetrachloroethylene
--__ trichloroethylcne
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophcnol
----__ 2,4,6-trichlorophenol
------vinyl chloride
endrin --lindane --
Date Received Reported by __ methoxychlor
--toxaphene
OJte Extracted Date Reported 2,4-D --. __ 2,4,5-TP (Silvcx)
Date AnalyLcd Lab Number --
[)!IS 3191 (llcviscd 2/91)
1'.C Depanmcn1 of l::..nvironmenl,
I leahh, & Natural Resourcc.s
Solid Waste Management OMS.ion
P.O. Box 2.BD•n, 3()6 K .:.'ilminpon S1r:c:
R.alcii}\, North Carolina 2?611 • Site Number~N=C~D~9~9 .... 1_1'--'-r_,c3~S:~3 __ _ Field Sample Nurnber _ __.\..,_(~C'-2--'--'·;,~----------
Name of Sile N A--T10l\l A-L S Tf\f{.\i Sile Location R~w 6: f'1 (01 1(0<':(
Collected By-:JsCucE. N K \-ltJ, .. f:(Y JD# 5'1 Dale Collected I O -2 2-9 J Time ------
Agency: --Hazardous Waste Solid Waste __Lsupcrfund TCLP Compounds
--
Sample Type Inorganic Compounds Resu Its (mg/I)
Environmental Concentrate Comments Arsenic --
/Ground waler (1) _ Solid (5) ~'f l.e, \ C-
Barium --Cadmium --
Na. \i
Chromium
Surface water (2) Liquid (6) LiM\i i\cre-s \veil --Lead
----
2. r{\ I C200A l'VIQVIJ:r C, ½)e)J
Mercury
_Soil (3) _ Sludge (7) --Selenium --Silver --
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) P/Aeter Results(mg/1) (i:ng/kg) Organic Compounds Results(mg/1)
P&T:GC/MS 7,Arsenic benzene
--Acid:B/N Ext.
--
--Barium carbon tetrachloride
/Cadmium
--
MTBE chlordane
----
--iChloride
chlorobenzene --
--Chromium chloroform --
--Copper o-cresol --
Fluoride m•crcsol
----
--Iron __ p-crcsol
--, Lead cresol --1,4-dichlorobenzene
----
--Mercury 1,2-dichlorocthanc
--, Nitrate __ 1,1-dichloroethylene
Selenium 2, 4.dinit rota\ ucne --
Silver --heptachlor
Radiochemistry ~Sulfates hexachlorobcnzene --
··••---Zinc hcxach lorobutad iene --
Parame:lt!r Results (PCi/1) --pH hcxachloroethane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnz.cnc
----TOC __ pcntachlorophenol
--
--__ pyridine
Microbiology --__ tetrachloroethylenc
--__ trichloroelhylenc
Parameter Results (Col/l00m\) --__ 2,4,5-trichlorophcnol
----__ 2,4,6-trichlorophenol
--
__ ,onyl chloride
--cndrin --lindanc --
Dale Received Reported by __ methoxychlor
__ toxaphcne
Date Extracted Dale Reported 2,4-D --2,4,5-TP (Silvcx)
Dale Analyzed Lab Number
Dl IS 3PJ1 (llcviscd 2/91)
--
t-,:.C. Department of i~.1win: ... nr:1ct1i,
licallh, & r--:alunl Resources
Solid Wane Management Oi\-Uion
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R.a.lcigh, North Carolina 27611 • Sile Number......,__N"-"C""-D'--'-9-'-S-'--'\-*,_,_]'6..:..._,'.}..,_')-"'3 __ _ Field Sample Number_..Jl'-'(.,.c·-'·=:;,"-4-1-. _________ _
Name of Si1e__,_N-'-'-'r1/-"-'17--'-'0N:..L.:C1ftl--'-=--'':,::::.Tt\,..:_i "-=f.1...:-Ii_:._ __ _ Sile Location :Row A:rJ Cm iNT'::(
Dale Collected IO -"2 2-9 L Time . ______ _
Agency: ---Hazardous Waste Solid Waste Lsuperfund TCLP Compounds
---
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium
/Grnund water (1) Sv,AvYf\e \4 --
Solid (5) Cadmium --
L1 ~le fkre?:< \\)ell No, 14 Chromium --
Surface water (2) _ Liquid (6) Lead
----
N(s. kc \'\N.tl'.\ E.\l{,v Well __ Mercury
_ Soil (3) _ Sludge (7) Selenium --Silver --
--Other (4) _ Other (8) --
----
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) P/Aeter_ Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS -3/ Arsewc bCnzene --
_ Acid:B/N Ext. Barium carbon tetrachloride
✓Cadmium --
MTBE chlordane
----
2Chloride chlorobenzene
----
--Chromium chloroform --
--Copper o-cresol --
--:Z: Fluoride m-cresol --
--Iron p-cresol --
Lead crcsol
----
--Manganese --1,4-dichlorobenzene
--Mercury 1,2-dich lorocthane
--Nitrate __ 1,1-dichloroethylcne
Selenium 2, 4-dinit rotolucne
Silver __ heplachlor
Radiochemistry :=i" Sulfates hcxachlorobenzene --
····---Zinc hcxachlorobuladiene --
Paramete'r Results (PCi/1) _pH hcxachlorocthane
__ Gross Alpha --Conductivity __ methyl ethyl ketone
Gross Beta TDS nilrobcnz.c.nc
----TOC __ pcntachlorophenol ----__ pyridine
Microbiology --__ Letrachloroethylcne
----trichloroethylene
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-trichlorophcnol
------vinyl chloride
endrin --lindanc --
Date Received Reported by --mcthoxychlor
--Loxaphene
Dale Extraclcd Dale Reported 2,4-D --__ 2,4,5-TP (Silvcx)
Dale Analy,cd Lob Number --
D!IS 31 1)1 (!{cviscd 2/91)