NCD991278953_19980924_National Starch & Chemical Corp._FRBCERCLA LTRA_Second Quarter 1998 OU-1 and OU-2 Monitoring Report-OCR

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· REPORT ,
Second Quarter 1998 OUJ
and OU2 Monitoring
Report
National Starch and Chemical Company
Salisbury, North Carolina
September 1998
BBL
BLASLAND, BOUCK & LEE, INC ..
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BtASlAND, BOUCK & LEE. INC.
engineers & scientists
8 South River Road
Cranbury, New Jersey 08512-9502
[phone]
TECHNICAL REPORT
RE --,,tED
OCT 06 1998
SUPERFUND SECTION
Second Quarter 1998 OUJ
and OU2 Monitoring
Report
National Starch and Chemical Company
Salisbury, North Carolina
September 1998
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Table of Contents
Section 1.
Section 2.
Section 3.
Section 4.
Section 5.
Tables.
72680562.wPD ·· 9fl◄fi8
Introduction .......................................... 1-1
1.1 · Purpose and Objectives ........................... 1-1
1.2 Monitoring Program Overview ...................... 1-1
1.3 Report Organization .............................. 1-2
Field Procedures ...................................... 2-1
2.1
2.2
Water Level Measurement ......................... 2-1
Sample Collection ................................ 2-1
Results .............................................. 3-1
3.1
3.2
3.2.1
3.2.2
3.3
3.3.1
Ground-Water Elevations .......................... 3-1
Analytical Res·ults ................................ 3-1
Plume Periphery Wells ............................ 3-1
Trench Area Wells ................. -.............. 3-2
Pumping Data ................................... 3-3
Second Quarter 1998 ............................. 3-3
Data Validation ....................................... 4-1
4.1 Laboratory Conformance .......................... 4-1
4.2 Method Detection Limits and Dilution Factors ........... 4-1
4.2.1 Plume Periphery Wells ............................ 4-1
4.2.2 Trench Area Wells ............................... 4-2
4.3 QA/QC Samples ................................. 4-3
4.3.1 Blind Duplicate Sample ........................... 4-3
4.3.2 MS/MSD Samples and Laboratory Method
Blanks ........................... _-_ ............ 4-3
Future Actions ........................................ 5-1
2-1
3-1
3-2
3-3
3-4
3-5
3-6
3-7
3-8
3-9
Sample Summary
Depth to Water and Ground-Water Elevation Measurements
Comparison of Second Quarter 1998 Analytical Results for
Plume Periphery Wells to Performance Standards
Analytical Results -VOCs -Plume Periphery
Analytical Results -SVOCs -Plume Periphery
Analytical Results -Metals -Plume Periphery
Comparison of Second Quarter 1998 Analytical Results for
Trench Area Wells to Performance Standards
Analytical Results -VOCs -Trench Area
Analytical Results -SVOCs -Trench Area
Analytical Results -Metals -Trench Area ·
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Figures.
Attachment.
72680562.WPO .• 9n4fi8
3-10 Pumping Rates -Second Quarter 1998 -Plume Periphery
Extraction Wells
3-11 Pumping Rates -Second Quarter 1998 -Trench Area Extraction
Wells
1-1 Site Location Map
1-2 Well Location Map
3-1 Ground-Water Elevations -Second Quarter 1998
3-2 Individual Pumping Rates -Second Quarter 1998 -Plume
Periphery Extraction Wells
3-3 Daily Total Pumping Rates -Second Quarter 1998 -Plume
Periphery Extraction Wells
3-4 Individual Pumping Rates -Second Quarter 1998 -Trench Area
Extraction Wells
3-5 Daily Total Pumping Rates -Second Quarter 1998-Trench Area
Extraction Wells
A Laboratory Analysis Data Sheets
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1. Introduction
This quarterly monitoring report presents the results of the second quarter 1998 ground-water monitoring and pumping data for Operable Units (OU) Nos, I and 2 at the National Starch and Chemical Company (NSCC)'facility" -located on Cedar Springs Road in Salisbury, North Carolina (Figure 1-1 ). OU I consists of ground water located in the west-southwest portion of the facility, and OU2 consists of soil in the Trench Area, located west of the Production Area. Ground-water monitoring is conducted in accordance with the Records of Decision (RODs) issued for OU I and OU2 by the United States Environmental Protection Agency (USEPA) in September 1988 and September 1990, respectively.
1.1 Purpose and Objectives
The purpose of the OU I and OU2 ground-water monitoring program is to provide analytical data to evaluate the effectiveness and protectiveness of the OU! and OU2 remedial actions. The objectives of the ground-water
monitoring program are as follows:
• monitor ground water for selected constituents of concern (COCs) identified in the OU! ROD;
• evaluate ground-water quality relative to the Performance Standards identified in the OU I ROD;
• evaluate ground-water quality relative to historic data to identify concentration trends; and
• provide recommendations based on analytical results and historic COC concentration trends to improve the
effectiveness of the monitoring program.
1.2 Monitoring l"rogram Overview
Extraction and monitoring wells sampled as part of the OU! and OU2 monitoring program are shown in Figure 1-2
and include the following:
• OU I (Plume Periphery Wells)
Extraction Wells: EX-01, EX-02, EX-03, and EX-04
Monitoring Wells: NS-29, NS-30, NS-31, and NS-32
• OU2 (Trench Area Wells)
Extraction Wells: EX-OS, EX-06, EX-07, EX-08, EX-09, and EX-I 0
Monitoring Wells: NS-09, NS-10, NS-I 1, and NS-IS
Plume Periphery extraction and monitoring wells have been sampled for 22 quarters from first quarter 1993 through second quarter 1998 with the exception of extraction well EX-02, which was not sampled during first quarter 1993. Trench Area extraction wells have been sampled for 9 quarters from second quarter 1996 through second quarter I 998 and Trench Area monitoring wells have been sampled for 21 quarters from second quarter I 993 through
second quarter 1998.
Ground-water samples collected from the Plume Periphery and Trench Area extraction and monitoring wells have been analyzed for Volatile Organic Compounds (VOCs), Semivolatile Organic Compounds (SVOCs) and metals. Ground-water COCs include the following 14 VOCs, two SVOCs, and nine metals:
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Acetone 4-Nitrophenol Arsenic
Benzene Bis(2-chloroethyl)cther Barium
Bromodichloromethane Beryllium
Chloroform Cadmium
I, 1-Dichloroethene Chromium
1,2-Dichloroethane Manganese
1,2-Dichloropropane Nickel
Ethylbenzene Selenium
Methylene Chloride Zinc
Toluene
I, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylene
1.3 Report Organization
The report is organized into the following sections:
• Section 2 -Field Procedures: discussion of methods for field sampling and laboratory analysis of samples
• Section 3 -Results:
• Section 4 -Data Validation:
• Section 5 -Summary:
B.\72680562.WPO .. 9n4f)8
presentation of the analytical results and evaluation relative to regulatory
criteria and historical.data
review of general laboratory conformance and evaluation of method detection
limits, dilution factors, and QA/QC sample results
highlights current ground-water quality and changes in ground-water results
relative to historic results; provides recommendations for changes to the
ground-water monitoring program
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2. Field Procedures
The second quarter 1998 monitoring event was conducted in June 1998. Field sampling procedures used during
the sampling event are discussed below and summarized in-Table 2-1.
2.1 Water Level Measurement
Water level measurements were taken on June 16, 1998 from two stream gauges (SG-1 and SG-2) in the southwest
tributary and the following extraction and monitoring wells:
• Plume Periphery
Extraction wells (4):
Monitoring wells (12):
• Trench Area
-Extraction wells ( 6):
-Monitoring wells (4):
EX-OJ, EX-02, EX-03, EX-04
NS-05, NS-06, NS-21, NS-22, NS-23, NS-26, NS-27, NS-28, NS-29, NS-30, and
NS-31
EX-05, EX-06, EX-07, EX-08, EX-09, and EX-10
NS-09, NS-I 0, NS-I 1, and NS-15
The static water level was not measured in monitoring well NS-32 due to artesian conditions, which have been
present during all of the previous sampling events since first quarter 1993. No measurements were collected from
monitoring well P-0 I because an obstruction exists inside this well.
2.2 Sample CoUection
As indicated in Section 1.2, ground-water samples were collected from the following wells:
• Plume Periphery
Extraction wells (4):
Monitoring wells (4):
• Trench Area
Extraction wells ( 6):
Monitoring wells ( 4 ):
EX-0 I, EX-02, EX-03, EX-04
NS-29, NS-30, NS-31, and NS-32
EX-05, EX-06, EX-07, EX-08, EX-09, and EX-10
NS-09, NS-I 0, NS-11, and NS-15
Ground-water samples were collected by filling sample jars directly from the dedicated pumps located in each well,
with the exception of NS-09, NS-I 0, NS-I ! , and NS-31. Samples from these wells were collected using a portable
submersible pump in accordance with the Performance Standard Verification Plan (PSVP).
Quality Assurance/Quality Control (QNQC) samples included collection of one "blind duplicate" sample at well
EX-03 and one matrix spike (MS) sample and one matrix spike duplicate (MSD) sample at well EX-01.
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3. Results
This section outlines the results of the ground-water elevation measurements, laboratory analyses of ground-water
samples, and pumping data for second quarter 1998.
3.1 Ground-Water Elevations
Depth to water {DTW) and ground-water elevations are shown in Table 3-1 and on Figure 3-1 for the second quarter
1998 sampling event.
3.2 Analytical Results
This section summarizes the current analytical results for ground-water samples relative to the Performance
Standards and historical data. NSCC recognizes detection limits for some constituents are greater than the
performance standard due to the inherent limitations of CLP methods.
3.2.1 Plume Periphery Wells
Ground-water samples collected from the Plume Periphery wells were analyzed for Target Compound List (TCL)
VOCs and SVOCs and Target Analyte List (TAL) metals using the USEPA Level IV Contract Laboratory Program
(CLP) protocol.
Analytical results are compared to the Performance Standards as shown in Table 3-2. This comparison indicates
the following:
• Detected concentrations ofVOCs are less than the Performance Standards with the exception of the following:
Well
Acetone 3,500
1,2-Dichlorocthane 5
1.2-Dichloropropanc 6
"-" concentration less than Perfonnance Standard
D -concentration from diluted run sample
EX-02 EX-03**
3,800 6,900D
410 190
170 235
1l -analyte also detected in associated method blank (method blank concentration -3) ug/1)
• Performance Standards from OUI ROD.
** Average concentration ofEX-03 and duplicate sample
NS-29 NS-31
100,000DE"* 47,000DB
4,200
3,700
*** Acetone concentration in NS-29DL was 0.15 ug/1 over the calibration range; the analytical laboratory did not rerun the sample.
• Detected concentrations of SVOCs are less than the Performance Standards with the exception of bis(2-
chloroethyl)ether in EX-0 I ( 14 ug/1), EX-02 ( 140D ug/1), EX-03 ( 195D ug/1), EX-04 (28 ug/1), NS-29 (3, I 00D
ug/1), and NS-31 (2,700D ug/1). The Performance Standard for bis(2-chloroethyl)ether is 5 ug/1.
• Detected concentrations of metals are less than the Performance Standards with the exception of the following:
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Well EX-02 NS-29 NS-31
Barium 1,000 1,130 1,370 9,330
Manganese 7,700 12,100 32,100
Selenium 10 15.6
Detection limits and dilution factors for the second quarter 1998 sampling event are discussed in Section 4.2.
Analytical results for the 22 monitoring events are shown in Tables 3-3, 3-4, and 3-5 for VOCs, SVOCs, and
metals, respectively. As shown in these tables, analytical results for the second quarter 1998 monitoring event are
similar to or less than the historical results.
3.2,2 Trench Area Wells
Ground-water samples collected from the Trench Area wells were analyzed for TCL VOCs and SVOCs and TAL
metals using the USEPA Level IV CLP protocol.
Analytical results are compared to the Performance Standards as shown in Table 3-6. This comparison indicates
the following:
• Detected concentrations ofVOCs are less than the Performance Standards with the exception of the following:
.. , ,:rs:? . ,· ,,. ... TI , . :"'r·C,:-: •. ,._,_.-,•C:-.•· ,i • •--~ •····•.·•··> yoc. . , .·.,, . ...... •• .. ,, "'
Well EX-05 EX-06 EX-08 EX-09 EX-10 NS-09 NS-10 NS-/5
Acetone 3,500 170008 -72000D 14000 93000B ---
1,2-Dichloroethane 5 340000D 270D 2200000 85000D 29000D 25000 1900D 130
1,2-Dichloropropanc 6 --2800 13000 44000D ---
Methylene chloride 5 --420) "'"""' l30J ---,.,,.v~
Toluene 2,000 14000 -20000 15000 7600 ---
Vinyl chloride 2 ----210) 17) --
Xylene 350 --1100) 2300 6200 ---
Units in. ug/1
PS -Pcrfonnancc Standard from OUI ROD (These values are not reflective of the changes recommended in the OU2 Five-Year Review.)
"-" concentration less than Performance Standard
J -estimated concentration less than the detection limit
D -concentration from diluted run sample
B -analyte also detected in associated method blank (laboratory method blank concentrations= 3J ug/1 and 61 ug/1)
• Detected concentrations of SVOCs are less than the Performance Standards with the exception of bis(2-
chloroethyl)ether is EX-08 ( I ,900 ug/1), EX-09 (7, I 000 ug/1), and EX-IO (23,0000 ug/1). The Performance
Standard for bis(2-chloroethyl)ether is 5 ug/1.
• Detected concentrations of metals are less than the Performance Standards with the exception of the following:
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Well EX-05 EX-07 EX-08 EX-09 EX-JO NS-09 NS-15
Beryllium 17.5 46.8)
Manganese 7,700 255000 26200 311000 178000 184000 12400 15600
Nickel 350 9601 1330) 940)
Selenium 10 66.9 78.7 43 46
Detection limits and dilution factors for the second quarter 1998 sampling event are discussed in Section 4.2.
Analytical results for the 22 monitoring events are shown in Tables 3-7, 3-8, and 3-9 for VOCs, _SVOCs, and
metals, respectively. As shown in these tables, analytical results for the second quarter 1998 monitoring event are
similar to or less than the historical results.
3.3 Pumping Data
This section presents the pumping data for second quarter 1998.
3.3.1 Second Quarter 1998
Pumping rates for second quarter 1998 are shown in Tables 3-10 and 3-11 for the plume periphery extraction wells
(EX-01, EX-02, EX-03, and EX-04) and the trench area extraction wells (EX-05, EX-06, EX-07, EX-08, EX-09,
and EX-I 0), respeciively. On March 29, 1998 the trench area extraction wells began a 24-hour per day, 7 day per
week operation schedule. Throughout second quarter 1998, the plume periphery and trench area extraction wells
operated on a 24-hour per day, 7 day per week operation schedule, with the exception of the following
interruptions:
• Monday 5/4/98 to Wednesday 5/6/98 -OU2 wells shut down for maintenance and to fix broken valve on
hydrolysis tank.
• Thursday 5/28/98 to Friday 5/29/98 -OU2 wells shut down for hydrolysis tank maintenance and cleaning.
• Friday 6/12/98 -OU2 wells shut down for air column maintenance and cleaning.
Individual and daily average pumping rates for the periphery wells are shown in Figures 3-2 and 3-3, respectively,
and are summarized below:
EX-02 5 -15 11
EX-03 14 -35 28
EX-04 5 -20 14
Total 68
gpm -gallons per mmutc
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Individual and daily average pumping rates for the trench area wells are shown in Figures 3-4 and 3-5, respectively,
and are summarized below:
EX-05 0.5 • 2.3 1.8
EX-06 0.5 -1.8 I.I
EX-07 0.8 -1.5 1.0
EX-08 1.2 -2.1 1.8
EX-09 2.0 -4.0 3.2
EX-10 0.5 -1.0 1.0
Total 9.9
gpm -gallons per mmute
• Not including maintenance shut-downs
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4. Data Validation
Data validation for the second quarter 1998 ground-water monitoring samples included a review of general
laboratory conformance and an evaluation of method detection limits, dilution factors, and QA/QC sample results.
4.1 Laboratory Conformance
The laboratory conformance summary was reviewed to identify possible analytical difficulties and their potential
effects on the analytical results. Holding times, instrument calibrations, surrogate recoveries, and internal standard
responses met CLP criteria with the exception of the following:
• VOCs: (I) dilutions for samples EX-06, EX-09, EX-I 0, NS-09, and NS-31 were slightly out of hold time;
(2) sample EX-03 was originally over diluted based on historical data, then analyzed more
concentration, with the final concentrated analysis out of hold time; (3) surrogate recoveries of 1,2-
Dichloroethane d4 were outside method criteria; (4) Sample EX-06DLB reported low internal
standard recoveries for all three internal standards.
• SVOCs: (I) Sample NS-30 had a low recovery due to extraction problems; (2) LCS recoveries for 4-
nitrophenol were greater than CLP limits, indicating a positive bias.
• Metals: selenium matrix spike and matrix spike duplicates were outside specific control limits for sample
NS-31.
4.2 Method Detection Limits and Dilution Factors
Method detection limits and dilution factors were reviewed for the Plume Periphery and Trench Area wells.
4.2.1 Plume Periphery Wells
Detection limits for VOCs, SVOCs, and metals are less than the Performance Standards in undiluted samples for
the Plume Periphery wells with the exception of the following:
• benzene, bromodichloromethane, chloroform, I, 1-dichloroethene, methylene chloride, .I, 1,2:tric_hloroethane,
trichloroethene, and vinyl chloride in the eight samples and the EX-03 duplicate;
• 1,2-dichloroethane and 1,2-dichloropropane in EX-01, EX-04, NS-31, and NS-32; and
• bis(2-chloroethyl)ether in NS-32.
Dilution factors for VOCs and SVOCs in undiluted samples in the Plume Periphery wells are as follows:
Dillitioit· FactO·r's:·:-· <', .,-.-~·-' .. ....... ,. . ·-·~:~,.~:~i§{fJC(~fl):,:··-:.//{/ Well :
voes SVOes voes SVOes
EX-01 1.0 1.0 NS-29 50.0 10.0
EX-02 25.0 1.0 NS-30 1.0 1.0
EX-03 10.0 1.0 NS-31 250.0 10.0
EX-04 1.0 1.0 NS-32 1.0 1.0
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The analytical method for voes and SVOes will be changed so that detection limits for undiluted ground-water
samples (indicated by dilution factor equal to one) will be equal to or less than the Performance Standard. The
analytical laboratory will also be instructed to reduce the dilution factors as much as possible for samples requiring
additional dilution.
4.2.2 Trench Area Wells
Detection limits for voes, SVOes, and metals are less than the Performance Standards in undiluted samples for
the Trench Area wells with the exception of the following:
• benzene, bromodichloromethane, chloroform, I, 1-dichloroethene, I, I ,2-trichloroethane, and trichloroethene
in the ten samples;
• 1,2-dichloroethane in EX-07;
• i,2-dichloropropane and methylene chloride in EX-05, EX-06, EX-07, NS-09, NS-IO, NS-I I, and NS-15;
• ethylbenzene in EX-05;
• vinyl chloride in EX-05, EX-07, EX-08, EX-09, NS-IO, NS-I I, and NS-15;
• xylene in EX-05;
• bis(2-chloroethyl)ether in EX-05, EX-06, EX-07, NS-10, NS-I I, and NS-15;
• beryllium in EX-05, EX-08, and EX-IO;
• chromium in EX-05, EX-08, EX-09, and EX-10; and
• nickel in EX-I 0.
Dilution factors for VOCs and SVOCs in umiiluied samples in the Trench Area wells are as follows:
I./ ~<-1•<··•·•)<1 ~;,, w; (,•·•······~ ... ··~ '"' ........
VOCs SVOCs VOCs SVOCs
EX-05 500.0 10.0 EX-10 50.0 10.0
EX-06 1.0 1.0 NS-09 10.0 1.0
EX-07 10.0 1.0 J:-!S-10 2.0 1.0
EX-08 250.0 10.0 NS-I I LO 1.0
EX-09 100.0 l0.0 NS-15 1.0 1.0
The analytical method for voes and SVOes will be changed so that detection limits for undiluted ground-water
samples (indicated by dilution factor equal to one) will be equal to or less than the Performance Standard. The
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analytical laboratory will also be instructed to reduce the dilution factors as much as possible for samples requiring
additional dilution.
4.3 QA/QC Samples
QA/QC samples for the second quarter 1998 monitoring event included one blind duplicate and MS/MSD samples.
Constituent concentrations detected in these samples, as well as the laboratory method blanks, were evaluated to
identify possible contamination of environmental samples from other sources, such as sampling equipment, or
sampling or laboratory practices.
4.3.1 Blind Duplicate Sample
The blind duplicate ground-water sample was obtained from well EX-03, and the analytical results are consistent
with the results for the EX-03 sample.
4.3.2 MS/MSD Samples and Laboratory Method Blanks
The MS and MSD samples were obtained from well EX-01. According to the laboratory conformance summary,
matrix spikes for VOCs were within CLP limits, matrix spikes for SVOCs were outside CLP limits due to matrix
interference, and matrix spikes for four metals were outside control limits for two samples.
VOCs and SVOCs were not detected in the laboratory method blanks with the exception of acetone, which was
detected in all four method blanks at concentrations ranging from 2J ug/1 to 6J ug/1.
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5. Future Actions
The next ground-water sampling event for the Trench Area and Plume Periphery wells is scheduled to occur in
September 1998_ Recommendations made in the Data Evaluation, submitted· as an attachment to the OU2 Five
Year Review, include changes in the monitoring frequency. Approval has been requested to change the frequency
of ground-water sampling for the Plume Periphery wells from quarterly sampling to semi-annual sampling, and
change the frequency of ground-water sampling for the Trench Area wells from quarterly sampling to annual
sampling_ Sampling will be conducted in accordance with the current Performance Standard Verification Plan
(PSVP).
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Tables
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Table 2-1
Sample Summary
National Starch and Chemical Company
Salisbury, North Carolina
Measurement Measurement
Point Type
Plume Periphery Wells
EX-01 BE
EX-02 BE
EX-03 BE
EX-04 BE
NS-05 SM
NS-06 SM
NS-21 BM
NS-22 BM
NS-23 SM
NS-26 BM
NS-27 BM
NS-28 BM
NS-29 BM
NS-30 BM
NS-31 BM
NS-32 BM
P01 BM
SG-1 SG
SG-2 SG
Trench Area Wells
EX-05 BE
EX-06 BE
EX-07 BE
EX-08 BE
EX-09 BE
EX-10 BE
NS-09 SM
NS-10 SM I NS-11 SM
NS-15 BM
voes -Volatile Organic Compounds
SVOCs -Semivolatile Organic Compound
Water Level I
Measurement voes
X X
X X
X X
X X
X
X
X
X
X
X
X
X
X X
X X
X X
X X
X
X
X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
Laboratory Analysis•
SVOCs Metals
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X X
X ;(
•Laboratory analysis includes 13 VOCs, 2 SVOCs, and 9 metals identified in the OU1 Record of Decision
Measurement Types:
-SE -Bedrock Extraction Well
BM -Bedrock Monitoring Well
SM -Saprolite (shallow) Monitoring Well
SG -Stream Gauge (iron pins located in the southwest tributary)
':l,OJECTSINSCCIMONITOR\2Q9812Q98.WB2
Page 1 of 1
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Measurement
Table 3-1
Water Level Measurements
National Starch and Chemical Company
Salisbury, North Carolina
Measurement TOC Elevation Depth to Water Level I Point Type Date (ft. MSL) Water (ft) Elevation (ft. MSL)
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Plume Periphery Wells
EX-01 BE 06/16/98 731.85
EX-02 BE 06/16/98 718.24
EX-03 BE 06/16/98 740.46
EX-04 BE 06/16/98 754.12
NS-05 SM 06/16/98 767.96
NS-06 SM 06/16/98 738.87
NS-21 BM 06/16/98 739.13
NS-22 BM 06/16/98 715.94
NS-23 SM 06/16/98 752.36
NS-26 BM 06/16/98 720.77
NS-27 BM 06/16/98 749.47
NS-28 BM 06/16/98 767.82
NS-29 BM 06/16/98 715.5
NS-30 BM 06/16/98 718.54
NS-31 BM 06/16/98 711.15
NS-32 BM 06/16/98 699.48
P01 BM 06/16/98 708.09
SG-1 SG 06/16/98 712.26
SG-2 SG 06/16/98 693.9
Trench Area Wells
EX-05 BE 06/16/98 781.26
EX-06 BE 06/16/98 788.28
EX-07 BE 06/16/98 789.23
EX-08 BE 06/16/98 789.19
EX-09 BE 06/16/98 782.29
EX-10 BE 06/16/98 775.92
NS-09 SM 06/16/98 778.45
NS-10 SM 06/16/98 786.72
NS-11 SM 06/16/98 775.65
NS-15 BM 06/16/98 792.6
Water level measurements collected from Top of Casing (TOG)
• Well is artesian
.,. Obstruction is present in well
Measurement Types:
BE -Bedrock Extraction Well
BM -Bedrock Monitoring Well
SM -Saprolite (shallow) Monitoring Well
SG -Stream Gauge (iron pins located in the southwest tributary)
IPROJECTS\NSCCIMONITORl209812098.WB2
45.80 . 686.05
55.98 662.26
55.50 684.96
65.65 688.47
21.04 746.92
7.15 731.72
6.50 732.63
17.62 698.32
22.80 729.56
7.64 713.13
20.95 728.52
20.85 746.97
24.00 691.50
25.73 692.81
20.50 690.65
Not Measured*
13.50 694.59
0.25 712.01
0.50 693.40
26.8 754.46
43.72 744.56
37.67 751.56
62.5 726.69
74.02 708.27
66.65 709.27
28.78 749.67
34.14 752.58
18.79 756.86
44.21 748.39
Page 1 of 1
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Well ID EX-01 EX-02 EX-02DL
Sample No. 10696441 10696458 106964580L
Sample Date 06/17/98 06/17/98 06/17/98
Dilution Factor Performance 1.0 25.0 -
Associated Method Blank S1andard VBLK178 VBLK183 -voes -
Acetone 3,500 3 J 3,800 -
Benzene 5 10 u 250 u -
Bromodicllloromethane 5 10 u 250 u -
Chloroform 5 10 u .• 250 u -
1. 1-0icllloioethene 7 10 u , 250 u -
1,2-DicllloroeUlane 5 10 u 410 -
1.2-Dicllloropropane 6 10 u 170 J -
Ethyibenzene 3,500 10 u 250 u -
Methylene chloride 5 10 u 250 u -
Toluene 2,000 10 u 130 J -
1.1.2-Trichloroethane 5 10 u 250 u -
Trichloroethene 5 10 u 250 u -
'.'inyl chloride 2 10 u 250 u -
Xylene 350 10 u 250 J -
Dilution Factor 1.0 1.0 5.0
Associated Me1hod Blank SBLK13739 SBLK13739 SBLK13739
SVOCs
Bis(2-ch/oroethyt}ether 5 14 220 E 140 D
4-Nitrophenol 350 26 u 26 u 130 u
Metals
Arsenic 10 1.3 u 1.3 u -
Barium 1.000 137 J 1130 -
Beryllium 17.5 1 u .1 u -
Cadmium 10 0.26 u 0.26 u -..j ••• Chromium 50 4.8 J 4.2 J -
Manganese 7.700 237 12100 -
Nickel 350 14 u 14 u -
Selenium 10 4.3 u 4.4 J -
Zinc 7.350 5 u 5 u -
Units in ug/1
U -Not Detected
8 (organics) -analyte also detected in associated method blank
Tablo 3-2
Comparison or Second Quarter 1998 Analytical Results for Pfume Periphery Wells to Performance Standards
National Starch and Chemical Company
Salisbury, North Carolina
EX-03 EX-oJDL DUPLICATE OUPLICATE-DL EX--04 NS-29
10696466 10696466OL 10696474 106964740L 10696482 1696318
06/17/98 06/17/98 06/17/98 06/17/98 06/17/98 06/16/98
10.0 100.0 10.0 100.0 1.0 50.0
VBLK183B VBLK183 VBLK183 VBLK183 VBLK178B VBLK178
4,700 EB 7200 D 6000 E 6600 D 7 J 76000 E
100 u 1000 u 100 u 1000 u 10 u 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
190 180 OJ 190 180 OJ 10 u 4200
230 240 OJ 240 230 OJ 10 u 3700
100 J 1000 u 100 u 1000 u 2 J 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
180 240 OJ 190 210 OJ 11 1400
100 u 1000 u 100 u 1000 u 10 u 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
100 u 1000 u 100 u 1000 u 10 u 500 u
22 J 1000 u 45 J 1000 u 6 J 220 J
1.0 5.0 1.0 5.0 1.0 10.0
SBLK13739 SBLK13739 SBLK13739 SBLK13739 SBLK13739 SBLK13739
280 E 200 D 240 E 190 D 28 1700 E
26 u 130 u 26 u 130 u 26 u 260 u
1.3 u -1.3 u -1.3 u 1.3 u
677 -675 36 J 1370
1 u -1 u -1 u 1.2 J
0.26 u -0.26 u 0.26 u 0.26 u
8.2 J -8.3 J -4.1 J 12.3
4850 -4500 4130 32100
14 u -14 u -14 u 14 u
4.3 u -4.3 lJ -4.3 u 15.6
5 u -5 u -5 u 5 u
8 (inorganics) • concentration greater than Instrument Detection Limit (IDL) but less than Contract Required Detection limit (CRDL)
J • estimated concentration less than the detection limit
D -concentration in diluted run sample
Bold rant indicates detected concentration greater than Performance Standard
Italic rant indicates detection limit in an undiuted sample greater than the Performance Standard
NS-290L NS-30 NS-31
16963180L 10696326 10696300
06/16/98 06/16/98 06/16/98
500.0 1.0 250.0
VBLK178 VBcK78 VBLK183
100000 DE 91 53000 E
5000 u 10 u 2500 u
5000 u 10 u 2500 u
5000 u 10 u 2500 u
5000 u 10 u 2500 V
4400 OJ 5 J 2500 u
3700 OJ 5 J 2500 u
5000 u 10 u 2500 u
5000 •U 10 u 2500 u
1400 DJ 10 u 980 J
5000 u 10 u 2500 u
5000 u 10 u 2500 u
5000 u 10 u 2500 u
5000 u 10 u 2500 u
100.0 1.0 10.0
SBLK13739 SBLK13739 SBLK13739
3100 D 2 J 1200 E
2600 u 26 u 260 u
-1.3 u 1.3 u
-36 J 9330
-1 u 1 u
-0.26 'J 0.28 u
-4.1 J 12.9
-1250 4150
-14 u 23.2 J
-4.3 u 4.3 u
-5 u 5 u
NOTE: According to Pace Laboratory. the acetone concentration in sample NS-290L was only over the calibration range by 0.15 ppb so the sample was not rerun at a higher dilution. The aceione concentration was still ~E" qualified. but the sample.was not diluted a third time.
IF:IPROJECTS\NSCC\MONITOR\2Q9812Q98.WB2
I
Page 1 of 1
NS-310L NS-32
106963000L 10696375
06/16198 06/16/98
500.0 1.0
VBLK183B VBLK178
47000 DB 4 J
5000 u 10 u
5000 u 10 u
5000 u 10 u
5vw u 10 u
5000 u 10 u
5000 u 10 u
5000 u 10 u
5000 u 10 u
930 OJ 10 u
5000 u 10 u
5000 u 10 u
5000 u 10 u
5000 u 10 u
100.0 1.0
SBLK13739 SBLK13739
2700 D 10 u
2600 u 26 u
-1.3 u
-105 J
-1 u
-0.26 u
-4 u
-139
-14 u
-4.3 u
-5 lJ
-- - --- -- -- - -
Quarter EX01 EX02 EX03
1093 75 NS 1300
2093 10 u 29000 D 2200
3093 6 J 34000 DB 6100
4093 10 u 27000 1200
1094 10 u 26000 220·)
2094 10 u 31000 B 3700
3094 10 u 41000 140,J
4094 10 u 28000 §;:~\St: 3700
1095 10 u 21000; 1001)
2095 33 D 24000; D 9200
3095 70 29000 D 2500
4095 39 50000 1900
1096 10 u 10000 5800
D
D
DB
B
D
D
Table 3-3A
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Che;nical Company
Salisbury, North Carolina
ACETONE
EX04 N529
1200 D 12000
10 u 10
29 B 10
27 10
21 10
30 B 10
20 10
15 10
10 u 39
1100 D 1100
2000 D 42000
820 80000
9 J 12000
D
u
u
u
u
u
u
D
D
2096 14 12000 E. ·,\ .'.~~f~!~9, : E · · -,_:-_1 ~oo;:1,1ifili-!~'.~5 E::j.·-1:~· &:ff64DQ~}:r};1,~p{Elim§
3096 12 33000 D 8800 D
4096 10 u 25000 D 7200 D
1097 8 BJ 30000 DB 14000 DB
2097 4.5 JB 7800 DB 12000 DB
3Q97 10 J 12000 D 15000 D
4097 10 u 7900 D 8000 D
1098 4 JB 3200 DB 10400 DB
2098 3 J 3800 6900 D
Units in ugn
U -Not Detected
J -Estimated concentration le~s than the detection limit
B -Constituent also detected in associated method blank (concentration in meth,xl blank unknown)
E -Exceeded calibration range
D -Concentration from diluted run sample
ROD Performance Standard: 3,500 ug/L
Bold font indicates detected concentration greater than ROD Perfonnance ~tanc ard
Italic font indicates detection limit greater than ROD Performance Standard
Shading indicates "E" qualified concentration for which a diluted run concentration is unavailable.
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.W82
675 D 100000 D
460 D 50000 D
810 DB 39000 DB
2200 DB 37000 DB
2400 100000 DB
460 D 59000 D
850 DB 93000 DB
7 J 100000 DE
I ~::fl.I• ,.,I 1•1 - --- -- -
N530 N531 N532
2900 4700 D 10 u
10 u 10 u 10 u
11 18 10 u
10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u
13 11 10 u
10 u 130 B 10 u
10 u 9200 10 u
10 u 15000 D 10 u
32 4800 D 10 u
10 u 16000 10 u
10 u 3500 10 u
13 ;,1/,H§j)Ot,(f~' !.!;~ -~ -.:....:___ -10 u
8 J 33000 D 10 u
10 u 41000 D 10 u
6 BJ 43000 DB 10 BJ
4 JB 30000 DB 3 JB
6 BJ 19000 B 4 BJ
10 u 31000 D 10 u
8 JB 45000 DB 13 B
91 47000 DB 4 J
-- - --
Quarter EX01 EX02
1093 5 u NS
2093 5 u 5
3093 10 u ,
4093 10 u 3300
1094 10 u 2500
2094 5 u 1700
3094 5 u 1200
4094 5 u 660
1095 5 u 1000
2095 5 u 42
3095 5 u 250
4095 5 u 2500
1096 5 u 500
2096 5 u 50
3096 10 u 1000
4096 10 u 250
1097 10 u 250
2097 10 u 250
3097 10 u 250
4097 10 u 250
1098 10 u 50
2098 10 u 250
Units in ug/1
U -Not Detected
J -Estimated c.oncentration less than the detection limit
ROD Pelformance Standard: 5 ug/L
- -
E:(03
5
u 5
J 10
u 170
u 250
u 120
u 50
u 93
u 33
u 45
u 17
u 50
u 500
u 25
u 25(>
u 250
u 25(•
u 250
u 250
u 250
u 100
u 100
Bold font indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Standard
NS · Nol Sampled
F:\PROJECTS\NSCC\MONITOR\HJSTRC_2.W82
- -- --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-3B
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BENZENE
EX04 NS29
2 J 5
5 u 5 , J 10
10 u 10
10 u 10
5 u 5
5 u 5
5 u 5
5 u 5
5 u 12
17 u 250
62 u 3100
5 u 500
25 u 50
2 J 97
0.6 J 500
10 u 500
2 J 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J
u
u
u
u
u
u
u
t'd!,ld 4 UI 14 - --- -- -
NS30 NS31 NS32
120 u 5 u 5 u
5 u 5 u 5 u
10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 250 u 5 u
5 u 10 u 5 u
5 u 32 u 5 u
5 u 500 u 5 u
5 u 250 u 5 u
5 u 100 u 5 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 250 u 10 u
10 u 2500 u 10 u
- -- - -- -
Quarter EX01 EX02
1093 5 u NS s
2093 5 u 5 u 5
3093 10 u 10 u 10
4093 10 u 3300 u 170
1094 10 u 2500 u 250
2094 5 u 1700 u 120
3094 5 u 1200 u 50
4094 5 u 660 u 93
1095 5 u 1000 u 33
2095 5 u 42 u 45
3095 5 u 250 u 17
4095 5 u 2500 u 50
1096 5 u 500 u 500
2096 5 u 50 u 25
3096 10 u 1000 u 250
4096 10 u 250 u 250
1097 10 u 250 u 250
2097 10 u 250 u 250
3097 10 u 250 u 250
4097 10 u 250 u 250
1098 10 u 50 u 100
2098 10 u 250 u 100
Units in ug/1
U -Not Detected
ROD Performance Standard: 5 ug/L
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
EXOJ
- -- --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-3C
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BROMODICHLOROMETHANE
EX04 NS29
5 u 5
5 u 5
10 u 10
10 u 10
10 u 10
5 u 5
5 u 5
5 u 5
5 u 5
5 u 12
17 u 250
62 u 3100
5 u 500
. 25 u 50
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
- --- -
Page 3 ot 14 - -
NS30 NS31 NS32
120 u 5 u 5 u
5 u 5 u 5 u
10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 250 u 5 u
5 u 10 u 5 u
5 u 32 u 5 u
5 u 500 u 5 u
5 u 250 u 5 u
5 u 100 u 5 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 250 u 10 u
10 U· 2500 u 10 u
- -- -- --
Quarter EX01 EX02
1093 5 u NS
2093 5 u 5
3093 10 u 10
4093 10 u 3300
1094 10 u 2500
2094 5 u 1700
3Q94 5 u 1200
4094 5 u 660
1095 5 u 1000
2095 5 u 42
3095 5 u 250
4095 5 u 2500
1096 5 u 500
2096 5 u 50
3096, 10 u 1000
4096 10 u 250
1097 10 u 250
2097 10 u 250
3097 10 u 250
4097 10 u 250
1098 10 u 50
2098 10 u 250
Units in ug/1
U • Not Detected
J -Estimated concentration less than the detection limit
ROD Performance Standard: 5 ug/L
5
u 5
u "' u 170
u 250
u 120
u 50
u 93
u 33
u 45
u 17
u 50
u 500
u 2S
u 250
u 250
u 250
u 25?
u 250
u 250
u 100
u 1oa
Italic font indicates detection limit greater than ROD F-erformance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
EX03
- -- --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-30
Analytical Results -VOCs
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
CHLOROFORM
EX04 NS29
5 u 5
5 u 5
10 u 10
10 u 10
10 u 10
5 u 5
5 u 5
5 u 5
5 u 5
5 u 12
17 u 250
62 u 3100
5 u 500
25 u 50
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-
120
5
10
10
10
5
5
5
5
5
5
5
5
5
10
10
10
10
10
10
10
10
--- -
11!!!!!!1 I!!!!
NS30 NS31 NS32
u 2 J 5 u
u 5 u 5 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 5 u 5 u
u 5 u 5 u
u 5 u 5 u
u 250 u 5 u
u 10 u 5 u
u 32 u 5 u
u 500 u 5 u
u 250 u 5 u
u 100 u 5 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 250 u 10 u
u 2500 u 10 u
-- - - -
Quarter EX01 EX02
1093 20 NS
2093 5 u 460
3093 10 u 510
4093 10 u 3300
1094 10 u 2500
2094 5 u 1700
3094 5 u 1200
4094 5 . u 550
1095 5 u 1000
2095 5 u 750
3095 3 J 570
4095 5 2500
1096 5 u 1200
2096 4 J 590
3096 10 u 610
4096 5 J 140
1097 7 J 520
2097 3.S J 290
3097 10 u 690
4097 10 u 920
1098 10 u 230
2098 10 u 410
Units in ug/1
U -Not Detected
J -Estimated concentratlon Jess than the detection limit
D -concentration from diluted run sample
ROD Performance Standard: 5 ug/L
- -
EX03
23
DJ 65
DJ 60
u 5S
u 250
u 120
u 50
J 9.J
u 33
59
10
u 61
150
42
J 250
J 6(1
220
240
200
230
200
190
Bold font indicates detected concentration greater than ROD Perfonnance Standard
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
f:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
-- - --
J
u
u
u
u
u
J
J
u
J
J
J
J
J
Table 3-3E
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch end Chemical Company
Salisbury, North Carolina
1,2-DICHLOROETHANE
EX04 NS29
4 J 110
3 J 22
5 J 3
10 u 3
10 u 10
5 u 17
5 3
3 J 43
7 8
5 37 ·
17 u 690
62 u 3100
4 J 860
25 u 300
10 u 500
3 J 1200
5 J 760
6 J 680
5 J 1900
10 u 1700
10 u 2300
10 u 4200
J
J
u
J
u
u
---- -- -
NS30 NS31 NS32
79 J 100 5 u
8 71 5 u
S6 49 10 u
10 u 20 10 u
10 u 9 J 10 u
4 J 5 5 u
5 u 4 J s u
5 u 4 J 5 u
5 u 250 u 5 u
5 u 41 5 u
s u 120 5 u
5 u 500 u 5 u
5 u 250 u 5 u
5 u 100 u 5 u
10 u 1000 u 10 u
10 u 170 J 10 u
3 J 1S0 J 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 260 10 u
5 J 2500 u 10 u
- ----- -
Quarter EX01 EX02
1093 5 u NS 5
2093 5 u 5 u 5
3093 10 u 10 u 10
4093 10 u 3300 u 170
1094 10 u 2500 u 250
2094 7 u 2300 u 180
3094 7 u 1800 u 70
4094 7 u 920 u 130
1095 7 u 1400 u 47
2095 7 u 59 u 63
3095 7 u 350 u 23
4095 7 u 3500 u 70
1096 5 u 500 u 500
2096 5 u 50 u 25
3096 10 u 1000 u 250
4096 10 u 250 u 250
1097 10 u 250 u 250
2097 10 u 250 u 250
3097 10 u 250 u 250
4097 10 u 250 u 250
1098 10 u 50 u 100
2096 10 u 250 u 100
Units in ug/t
U -Not Detected
ROD Performance Standard: 7 ug/L
Italic font indicates detection limit greater than ROD Performance Standard
NS · Nol Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.W82
EX03
-- - --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3<:iF
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
1, 1-DICHLOROETHENE
EX04 NS29
5 u 5
5 u 5
10 u 10
10 u 10
10 u 10
7 u 7
7 u 7
7 u 7
7 u 7
7 u 18
23 u 350
88 u 4400
5 u 500
25 u 50
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
- --- -
NS30 NS31 NS32
120 u 5 u 5 u
5 u 5 u 5 u
10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u
7 u 7 u 7 u
7 u 7 u 7 u
7 u 7 u 7 u
7 u 350 u 7 u
7 u 15 u 7 u
7 u 45 u 7 u
7 u 700 u 7 u
5 u 250 u 5 u
5 u 100 u 5 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 250 u 10 u
10 u 2500 u 10 u
-----
Quarter EX01 EX02
1Q93 35 NS
2093 4 J 820
JQ93 10 u 1000
4093 10 u 3300
1Q94 10 u 2500
2Q94 6 u 1600
3Q94 6 u 1200
4Q94 6 u 1200
1Q95 6 u 670
2Q95 6 u 1300
3095 6 u 890
4095 6 u 3000
1Q96 5 u 830
2Q96 5 u 650
3096 10 u 640
4Q96 1 J 100
1097 7 J 400
2097 3 J 190
3097 2 J 460
4097 10 u 730
1098 10 u 130
2098 10 u 170
Units in ug/1
U • Not Detected
J -Estimated concentration less than the detection limit
D -concentration from diluted run sample
ROD Performance Standard: 6 ug/L
--
EXOJ
120
DJ 180
DJ 150
u 170
u 250
J 70
J 44
53
J 40
160
24
u 130
140
33
J 87
J 71
150
J 240
230
310
200
J 235
Bold font indicates detected concentration greater than ROD Performance Stand:1rci
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
-----
u
u
J
J
J
u
J
J
J
J
J
J
Table 3-3G
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
1,2-DICHLOROPROPANE
EX04 NS29
5 u 350
5 u 46.5
10 u 5
10 u 10
10 u 10
6 u 6
6 u 6
6 u 6
6 u 6
6 12
26 1000
75 u 2200
5 u 1600
25 u 710
2 J 1900
1 J 1800
7 J 1200
17 980
7 J 2500
2 J 2700
3 J 2700
10 u 3700
D
J
u
u
u
u
u
u
J
J
-------
NSJO NS31 NS32
190 170 5 u
23 200 5 u
97 83 1 J
10 u 31 10 u
10 u 10 u 10 u
6 u 3 J 6 u
6 u 6 u 6 u
6 u 6 u 6 u
6 u 300 u 6 u
6 u 50 6 u
6 u 260 6 u
6 u 340 J 6 u
5 u 250 u 5 u
5 u 94 J 5 u
10 u 1000 u 10 u
10 u 160 J 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 170 J 10 u
5 J 2500 u 10 u
- -- -- --
Quarter EX01 EX02
1093 5 u NS
2093 5 u 9
3093 10 u 13
4093 10 u 3300
1094 10 u 2500
2094 10 u 3300
3094 10 u 2500
4094 10 u 1300
1095 10 u 2000
2095 10 u 85
3095 10 u 500
4095 10 u 500{)
1096 5 u 500
2096 5 u 12
3096 10 u 1000
4096 10 u 32
1097 10 u 250
2097 10 u 250
3097 10 u 250
4097 10 u 250
1098 10 u 50
2098 10 u 250
Units in ug/1
U -Not Detected
J -Estimated concentration less than the detection limit
ROD Performance Standard: 3,500 ug/L
5
2
3
u 170
u 250
u 250
u 100
u 190
u 67
u 89
u 33
u 100
u 500
J 25
u 250
J 250
u 25•)
u 25·)
u 250
u 250
u 100
u 100
Italic font indicates detection limit greater than ROD Perlormance Standard
NS· Nol Sampled
F:\PROJECTS\NSCC\MONITOR\H1STRC_2.WB2
EX03
- -- --
u
J
J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-3H
Anal}1ical Results • voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
ETHYLBENZENE
EX04 NS29
2 J 5
5 u 5
10 u 10
10 u 10
10 u 10
3 J 10
10 u 10
10 u 10
10 u 10
10 u 25
33 u 500
120 u 6200
5 u 500
25 u 50
2 J 500
2 J 500
3 J 500
4 J 500
10 u 500
2 J 500
2 J 500
2 J 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-
120
5
1
10
10
10
10
10
10
10
10
10
5
5
10
10
10
10
10
10
10
10
-- --- -
NS30 NS31 NS32
u 2 J 5 u
u 2 J 5 u
J 1 J 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 500 u 10 u
u 21 u 10 u
u 65 u 10 u
u 1000 u 10 u
u 250 u 5 u
u 100 u 5 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 250 u 10 u
u 2500 u 10 u
------- -----
Quarter EX01 EX02
1093 2 BJ NS
2093 1 J 4 J
3093 2 . BJ 10 u
4093 NR NR
1094 NR NR
2094 5 u 1700 u
3094 9 B 2900 B
4094 5 u 1200 B
1095 5 u 1300 B
2095 3 BJ 44 B
3095 5 u 250 u
4095 5 u 2500 I u / 1096 2 BJ 150 BJ
2096 1 BJ 13 J
3096 10 u 620 -'J
4096 0.6 J 74 J
1097 10 u 250 u
2097 10 u 250 u
3097 10 u 250 u
4097 10 u 40 J
1098 10 u 50 u
2098 10 u 250 u
Units in ug/1
U • Not Detected
J -Estimated concentration less than the detection limit
EX03
2 BJ
2 J
10 u
NR
NR
120 u
110 B
150 B
37 B
41 BJ
17 u
72 B
160 BJ
25 u
14(1 J
16 J
25(1 u
250 u
250 u
40 J
100 u
100 u
Table 3-31
Analytical Results -voes
Plume Periphery Extraction &nd Monitoring Wells
National Starch end Chamical Company
Salisbury, North Carolina
METHYLENE CHLORIDE
EX04 NS29
5 u 3
2 J 2
5 BJ 2
NR NR
NR NR
5 u 5
7 B 8
6 B 7
3 BJ 3
7 B 13
17 u 250
62 u 3100
2 BJ 150
5 BJ 50
4 J 2200
1 J 37
10 u 500
10 u 500
10 u 500
10 u 89
10 u 500
10 u 500
8 • Constituent also detected in associated method blank (concentffition in method blank unknown) ROD Performance Standard: 5 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Standard
NR · Not Reported
NS · Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
BJ
J
BJ
u
B
B
BJ
B
u
u
BJ
u
J
u.
u
u
J
u
u
-----
NS30 NS31 NS32
48 BJ 3 BJ 2 BJ
5 u 5 u 1 J
2 BJ 2 BJ 1 J
NR NR NR
NR NR NR
5 u 5 u 5 u
8 B 9 B 9 B
5 u 6 B 9 B
5 u 200 BJ 4 BJ
10 B 16 B 11 B
5 u 32 u 5 u
5 u 480 BJ 5 u
2 BJ 71 BJ 2 BJ
5 u 21 J 5 u
10 u 310 J 10 u
0.6 J 110 J 0.7 J
10 u 1600 B 3 J
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 160 J 10 u
10 u 250 u 10 u
10 u 2500 u 10 u
-- -- -- -
Quarter EX01 EX02
1093 13 NS
2093 5 u 110
3093 10 u 2500
4093 10 u 3300
1094 10 u 2500
2094 10 u 3300
3094 10 u 2500
4094 10 u 420
1095 10 u 2000
2095 10 u 280
3095 10 u 280
4095 10 u 5000
1096 5 u 290
2096 5 u 260
3096 10 u 340
4096 1 J 280
1097 10 u 300
2097 10 u 110
3097 10 u 210
4097 10 u 290
1098 10 u 62
2098 10 u 130
Units in ugfl
U • Not Detected
J -Estimated concentration less than the detection limit
ROD Performance Standard: 2,000 ug/L
58
46
u 55
u 66
u 250
u 91
u 60
J 87
u 69
80
J 32
u 60
J 130
55
J 99
120
190
J 160
J 180
200
165
J 185
Italic font indicates detection limit greater than ROD Performance Btandard
NS -Not Sampled
f:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
EX03
-- -- -
J
u
J
J
J
J
J
J
J
J
J
J
J
J
J
Table 3-3J
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
TOLUENE
EX04 NS29
5 60
2 J 6.5
3 J 3
3 J 10
10 u 10
7 J 10
4 J 10
7 J 10
10 u 10
26 25
31 J 200
120 u 6200
2 J 370
46 150
31 J 850
26 440
41 400
33 260
23 910
17 1100
22 950
11 1400
J
u
u
u
u
u
u
u
J
u
J
J
J
J
-
34
2
23
10
10
10
10
10
10
10
10
10
5
5
10
10
10
10
10
10
10
10
---- --
NS30 NS31 NS32
J 34 5 u
J 34 5 u
15 10 u
u 6 J 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 500 u 10 u
u 12 J 10 u
u 45 J 10 u
u 1000 u 10 u
u 64 J 5 u
u 150 5 u
u 310 J 10 u
u 370 J 0.8 J
u 315 J 10 u
u 370 J 10 u
u 390 J 10 u
u 610 J 10 u
u 620 10 u
u 980 J 10 u
- - -- -- -
Quarter EX01 EX02 ·
1093 5 u NS 5
2093 5 u 5 u 5
3093 10 u 10 u 10
4093 10 u 3300 u 170
1094 10 u 2500 u 250
2094 5 u 1700 u 120
3094 5 u 1200 u 50
4094 5 u 660 u 93
1095 5 u 1000 u 33
2095 5 u 42 u 45
3095 5 u 250 u 17
4095 5 u 2500 u 50
1096 5 u 500 u 500
2096 5 u 50 u 25
3096 10 u 1000 u 250
4096 10 u 250 u 250
1097 10 u 250 u 250
2097 10 u 250 u 250
3097 10 u 250 u 250
4097 10 u 250 u 250
1098 10 u 50 u 100
2098 10 u 250 u 100
Units in ug/1
U -Nol Detected
ROD Performance Standard: 5 ug/L
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.wa2
EX03
-- - --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-'.:lK
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
1,1,2-TRICHLOROETHANE
EX04 NS29
5 u 5
5 u 5
10 u 10
10 u 10
10 u 10
5 u 5
5 u 5
5 u 5
5 u 5
5 u 12
17 u 250
62 u 3100
5 u 500
25 u 50
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-
120
5
10
10
10
5
5
5
5
5
5
5
5
5
10
10
10
10
10
10
10
10
--- -- -
NS30 NS31 NS32
u 5 u 5 u
u 5 u 5 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 5 u 5 u
u 5 u 5 u
u 5 u 5 u
u 250 u 5 u
u 10 u 5 u
u 32 u 5 u
u 500 u 5 u
u 250 u 5 u
u 100 u 5 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 250 u 10 u
u 2500 u 10 u
- -- - -- -
Quarter EX01 EX02
1093 5 u NS 5
2093 5 u 5 u 5
3093 10 u 10 u 10
4093 10 u 3300 u 170
1094 10 u 2500 u 250
2094 5 u 1700 u 120
3094 5 u 1200 u S,)
4094 5 u 660 u 93
1095 5 u 1000 u 33
2095 5 u 42 u 45
3095 5 u 250 u 17
4095 5 u 2500 u 50
1096 5 u 500 u 500
2096 5 u 50 u 25
3096 10 u 1000 u 250
4096 10 u 250 u 250
1097 10 u 250 u 250
2097 10 u 250 u 250
3097 10 u 250 u 250
4097 10 u 250 u 250
1098 10 u 50 u 100
2098 10 u 250 u 100
Units in ug/1
u -Not Detected
ROD Pertormance Standard: 5 ug/L
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.wa2
EX03
- -- - -
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-Jl
Analytical Results -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
TRICHLOROETHENE
EX04 NS29
5 u 5
5 u 5
10 u 10
10 u 10
10 u 10
5 u 5
5 u 5
5 u 5
5 u 5
5 u 12
17 u 250
62 u 3100
5 u 500
25 u 50
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
- -- -- --
NS30 NS31 NS32
120 u 5 u 5 u
5 u 5 u 5 u
10 u 10 u 10 u
10 u 10 u 10 u
10 u 10 u 10 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 250 u 5 u
5 u 10 u 5 u
5 u 32 u 5 u
5 u 500 u 5 u
5 u 250 u 5 u
5 u 100 u 5 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 250 u 10 u
10 u 2500 u 10 u
- - -- -- -
Quarter EX01 EX02 EX03
1093 10 u NS 10
2093 10 u 10 u 10
3093 10 u 19 10
4093 10 u 3300 u 170
1094 10 u 2500 u 250
2094 2 u 670 u 50
3094 2 u 500 u 20
4094 2 u 260 u 3;'
1095 2 u 400 u 13
2095 2 u 17 u 18
3095 2 u 100 u 7
4095 2 u 1000 u 20
1096 10 u 1000 u 1000
2096 10 u 100 u 50
3096 10 u 1000 u 250
4096 10 u 250 u 250
1097 10 u 250 u 250
2097 10 u 250 u 250
3097 10 u 250 u 250
4097 10 u 250 u 250
1098 10 u 50 u 100
2098 10 u 250 u 100
Units in ug/1
U • Not Detected
ROD Performance Standard: 2 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
-- -- -
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-3M
Analytical Resu!ts • voes
Plume Periphery Extraction and Monitoring Welts
Natlonal Starch and Chemical Company
Salisbury, North Carolina
VINYL CHLORIDE
EX04 NS29
28 10
10 u 10
10 u 10
10 u 10
10 u 10
2 u 2
2 u 2
2 u 2
2 u 2
2 u 5
7 u 100
25 u 1200
10 u 1000
50 u 100
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
10 u 500
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
- --- -- -
NS30 NS31 NS32
250 u 10 u 10 u
10 u 10 u 10 u
10 u 2 J 10 u
10 u 10 u 10 u
10 u 10 u 10 u
2 u 2 u 2 u
2 u 2 u 2 u
2 u 2 u 2 u
2 u 100 u 2 u
2 u 4 u 2 u
2 u 13 u 2 u
2 u 200 u 2 u
10 u 500 u 10 u
10 u 200 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 1000 u 10 u
10 u 250 u 10 u
10 u 2500 u 10 u
--- - -
Quarter EX01 EX02
1093 2 J NS
2093 5 u 38
3093 10 u 52
4093 10 u 3300
1094 10 u 2500
2094 10 u 3300
3094 10 u 2500
4094 10 u 1300
1095 10 2000
2095 10 u 24
3095 10 u 500
4095 10 u 5000
1096 5 u 500
2096 5 u 34
3096 10 u 1000
4096 10 u 26
1097 10 u 250
2097 10 u 250
3097 10 u 250
4097 10 u 250
1098 10 u 50
2098 10 u 250
Units in ug/1
U • Not Detected
J • Estimated concentration less than the detection limit
ROD Performance Standard: 350 ug/L
- -
10
7
10
u 170
u 250
u 250
u 100
u 190
u 6"/
J 8!1
u 33
u 100
u 500
J 6
u 250
J 250
u 250
u 250
u 250
u 250
u 17
J 33.5
Italic font indicates detection limit greater than ROD Performance Standard
NS · Not Sampled
F:\PROJECTS\NSCC\MONJTOR\HISTRC_2.WB2
-
E:X03
u
u
u
u
u
u
u
u
u
u
J
u
u
u
u
u
u
J
J
- ---Table 3-3N
Analytical Resuas -voes
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
XYLENE
EX04 NS29
2 J 12
1 J 2
2 J 2
10 u 10
10 u 10
10 u 10
10 u 10
10 u 10
10 u 10
10 u 25
33 u 500
120 u 6200
5 u 500
25 u 20
6 J 110
5 J 56
6 J 500
10 500
2 J 110
4 J 160
5 J 130
6 J 220
J
J
u
u
u
u
u
u
u
u
u
u
J
J
J
u
u
J
J
J
J
-
120
5
4
10
10
10
10
10
10
10
10
10
5
5
10
10
10
10
10
10
10
10
t'i:IIJtt 14 01 14 -- --- -
NSJ0 NS31 NS32
u 6 5 u
u 7 5 u
J 4 J 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 10 u 10 u
u 500 u 10 u
u 21 u 10 u
u 65 u 10 u
u 1000 u 10 u
u 250 u 5 u
u 100 u 5 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 1000 u 10 u
u 89 J 10 u
u 2500 u 10 u
-- - --- -- -- --
Quarter EX01 EX02
1093 38 NS
2093 4 J 380
3093 11 u 540
4093 11 u 440
1094 10 u 510
2094 11 u 770
3094 6 u 680
4094 5 u 570
1095 5 u 540
2095 3 J 650
3095 14 570
4095 11 570
1096 9 J 400
2096 7 J 500
3096 10 u 430
4096 17 320
1097 31 490
2097 21 250
3097 24 310
4097 17 43
1098 46 180
2098 14 140
Units in ug/1
U • Not Detected
J -Estimaled concentration Jess than the detection limit
D • concentration in diluted run sample
E -Exceeded calibration range
ROD Performance Standard: 5 ug/L
EX03
82
D 100
D 10
74
150
120
56
110
130
180
120
140
130
E_~fr~l 93
170
D 130
D 180
D 180
D 210
260
D 350
D 195
Bold font indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Standard
u
D
D
D
D
D
D
Table 3-4A
Analytical Results · SVOCs
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury. North Carolina
B15(2-CHLOROETHYL)ETHER
EX04 NS29
12 190
5 J 52
11 25
53 u 18
22 J 8
17 J 12
13 J 12
21 J 17
14 J 13
55 32
64 450
41 1100
10 590
71 250
48 1400
49 740
68 D 810
74 D 410
68 D 1400
47 D 1400
94 D 2400
28 3100
Shading indicates ME" qualified concentration for which a diluted run concentratic,n is unavailable.
NS · Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
J
D
D
D
D
D
D
t'aytl I ut "l. --- ----
NS30 NS31 NS32
44 71 10 u
32 95 10 u
10 u 38 10 u
10 J 25 11 u
41 24 11 u
29 20 10 u
17 21 5 u
21 14 5 u
17.5 11 5 u
16 78 5 u
12 130 6 u
10 320 370
5 J 72 10 u
7 J 160 10 u
7 J 380 10 u
4 J 200 D 10 u
10 J 540 D 10 u
7 J 390 D 10 u
8 J 21 u 650 D
10 u 19 560 D
9 J 1500 D 10 u
2 J 2700 D 10 u
-- - -- --
Quarter EX01 EX02
1093 50 u NS 52
2093 50 u 52 u 56
3093 26 u 26 u 25
4093 27 u 260 u 52
1094 26 u 250 u 26
2094 27 u 1100 u 54
3094 29 u 530 u 27
4094 27 u 1400 u 53
1095 27 u 540 u 53
2095 26 u 270 u 52
3095 28 u 670 u 110
4095 25 u 500 u 53
1096 25 u 500 u 50
2096 25 u 120 u so
3096 25 u 250 u 250
4096 25 u 25 u 100
1097 26 u 25 u 100
2097 25 u 26 u 100
3097 25 u 26 u 26
4097 26 u 26 u 26
1098 26 u 26 u 26
2098 26 u 26 u 26
Units in ug/1
U • Not Detected
ROD Performance Standard: 350 ugll
Italic font indicates detection limit greater than ROD Performance Standard
NS -Nol Sampled
F:\PROJECTS\NSCC\MONITOR\H1STRC_2.WB2
EX03
--- --
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Table 3-4B
Analytical Results -SVOCs
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
4-NITROPHENOL
EX04 NS29
50 u 52
54 u 54
25 u 26
130 u 26
100 u 25
100 u 26
110 u 27
260 u 26
260 u 29
140 u 27
140 u 690
54 u 1300
25 u 25
120 u 120
50 u 250
25 u 250
25 u 260
25 u 250
26 u 250
28 u 260
27 u 130
26 u 260
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
-------
NS30 NS31 NS32
so u 50 u 50 u
50 u 52 u 50 u
26 u 25 u 25 u
27 u 26 u 26 u
26 u 27 u 27 u
27 u 26 u 26 u
26 u 27 u 26 u
26 u 26 u 27 u
26 u 26 u 25 u
28 u 51 u 26 u
27 u 130 u 28 u
26 u 260 u 520 u
25 u 25 u 25 u
25 u 120 u 25 u
25 u 120 u 25 u
25 u 50 u 25 u
26 u 50 u 26 u
25 u 50 u 25 u
26 u 52 u 26 u
26 u 26 u 26 u
26 u 26 u 26 u
26 u 260 u 26 u
------ --- ---
Quarter EX01 EX02
1093 2 u NS
2093 2 u 2 u
3093 2 u 2 u
4093 2.4 u 4.8 u
1094 2.9 u 5.8 u
2094 2.6 u 7.8 u
3094 2.1 u 2.1 u
4094 3.3 B 2.1 u
1095 0.8 u 1.1 B
2095 2.7 u 3.8 8
3095 1.9 u 2.8 B
4095 1.5 u 1.5 u
1096 1.1 u 1.1 u
2096 1.1 u 1.1 u
3096 1.1 u 1.1 u
4096 1.1 u 1.1 u
1097 7 u 7 u
2097 7 u 7 u
3097 7 u 7 u
4097 6 u 6 u
1098 6 u 6 u
2098 1.3 u 1.3 u
Units in ug/1
U -Not Detected
EX03
2 u
2 u
2 u
4.8 u
5.8 u
2.6 u
2.1 u
2.1 u
0.8 u
2.1 u
1.9 u
1.5 u
1.1 u
1.1 u
1. 1 u
1.1 u
7 u
7 u
7 u
6 u
6 u
1.3 u
Table 3-SA
Analytical Results . Metals
Plume Periphery Extraction and Monitoring Wells
National Starch and CMmical Company
Salisbury. North Carolina
ARSENIC
EX04 NS29
2 u 2
2 u 2
2 u 2
2.4 u 2.4
2.9 u 2.9
2.6 u 2.6
2.1 u 2.1
2.8 B 2.1
0.8 u 1.5
2.7 u 2.7
1.9 u 2.2
1.5 u 1.5
1.1 u 1.1
1.1 u 1.1
1.1 u 1.5
1.1 u 1.1
7 u 7
7 u 7
7 u 7
6 u 6
6 u 6
1.3 u 1.3
B · Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 10 ug/L
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
u
u
u
u
u
u
u
u
8
u
8
u
u
u
8
u
u
li
u
u
u
u
-----
NS30 NS31 NS32
2 u 2 u 2 u
2 u 2 u 2 u
2 u 2 u 2 u
2.4 u 2.9 B 2.4 B
2.9 u 2.9 u 2.9 u
2.9 B 3.7 B 2.6 u
2.1 u 2.1 u 2.1 u
2.1 B 2.1 u 3.1 B
0.8 u 1.3 8 0.8 u
2.7 u 2.9 8 2.8 B
1.9 u 1.9 u 2.3 B
1.5 u 1.5 u 1.5 u
1.1 u 1.1 u 1.1 u
1.1 u 1. 1 u 1.1 u
1.1 u 1.1 u 1. 1 u
1.1 u 1.1 u 1. 1 u
7 u 7 u 7 u
7 u 7 u 7 u
7 u 7 u 7 u
7 8 6 u 6 u
6 u 6 u 6 u
1.3 u 1.3 u 1.3 u
------- -----
Quarter EX01 EX02
1093 68.2 B NS 166
2093 25.3 8 1250 140
3093 27.2 8 1780 235
4093 22.8 8 1490 278
1094 17.1 8 1680 405
2094 23 8 1830 5113
3094 18.3 8 1540 608
4094 25.3 8 1070 498
1095 17.7 8 1080 625
2095 26.5 8 1860 475
3095 61.4 8 1820 265
4095 54.5 8 1930 387
1096 104 B 1970 553
2096 93.6 B 1780 415
3096 37.9 8 1560 440
4096 126 8 1370 349
1097 154 B 1170 SHI
2097 163 8 982 647
3097 173 8 1110 722
4097 181 8 1210 703
1098 213 713 71i
2098 137 J 1130 676
Units in ug/1
U -Not Detected
EX03
8
8
Table 3-5B
Analytical Results -Metals
Plume Periphery Extraction and Monitoring Wells
National Starch and ChBmical Company
Salisbury, North Carolina
BARIUM
EX04 NS29
37.3 8 1B2
26.9 8 87.4
29.4 8 80.9
36.3 8 61.7
29.3 8 45.3
56.4 8 64.1
27 8 52.2
45.9 8 57.6
34.4 8 64
72.7 8 84.7
52.6 8 190
42.8 8 1420
35.4 8 867
114 8 324
71.6 8 2490
61.5 8 1150
40.8 8 1360
45.1 8 720
44.7 8 1800
42 8 2110
46 8 1600
36 J 1370
8 -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting limit
ROD Performance Standard: 1,000 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Nol Sampled
F:\PROJECTS\NSCC\MONITOR\H!STRC_2.WB2
8
8
8
8
8
8
8
8
8
B
B
-----
NS30 NS31 NS32
23.4 8 193 8 65.B 8
31.8 8 36.3 8 69 8
33 8 19.5 8 86 8
29.8 8 15.6 8 85.6 8
49.4 8 2.4 u 85.5 8
35.6 8 17.4 8 82.6 8
31.6 8 8.2 8 85.2 8
26.9 8 1.7 8 85.5 B
27.3 8 19.6 8 85 8
27.5 8 12.6 B 93.3 8
19.7 B 207 89.7
18.1 8 1680 66.6 8
28 8 1630 87.8 B
31.1 8 3350 96.5 8
32.5 8 5180 95.8 8
32.1 B 6280 91.5 8
27.4 8 6780 97.3 8
28 8 6870 93 B
29.1 8 9280 96.3 B
25.8 8 4680 98.2 8
28.7 8 9850 99.1 8
36 J 9330 105 J
------
Quarter EX01 EX02
1093 1 u NS
2093 1 u 1 u
3093 1 5 B 1.7 B
4093 0.4 u 0.4 u
1Q94 0.4 u 0.4 u
2Q94 02 u 0.32 B
3Q94 0.3 u 0.3 U.
4Q94 0.3 u 0.3 u
1095 0.3 u 0.3 u
2Q95 02 u 0.23 B
3095 0.32 B 0.3 u
4095 0.3 u 0.3 u
1Q96 0.3 u 0.3 u
2096 0.3 u 0.3 u
3Q96 0.3 u 0.3 u
4096 0.3 u 0.3 u
1097 2 u 2 u
2097 2 u 2 u
3097 2 u 2 u
4097 1 u 1 u
1098 1 u 1 u
2098 1 u 1 u
Units in ug/1
U • Not Detected
- -
EX03
1 u
1 u
1.8 B
0.4 u
0.4 u
o.;:4 B
0.3 u
0.3 u
0.3 u
0.2 u
0.3 u
0.3 u
0.3 u
0.3 u
0.3 u
a.a u
2 u
2 u
2 u
1 u
1 u
1 u
---Table 3-SC
Analytical Results -Metals -
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BERYLLIUM
EX04 NS29
1 u 1
1 u 1
1.5 B 1.4
0.4 u 0.4
0.4 u 0.4
0.23 B 0.23
0.3 u 0.3
0.3 u 0.3
0.3 u 0.3
0.28 B 0.2
0.3 u 0.3
0.3 u 0.3
0.45 B 0.3
0.3 u 0.3
0.3 u 0.3
0.3 u 0.3
2 u 2
2 u 2
2 u 2
1 u 1
1 u 1
1 u 1.2
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit ROD Performance Standard: 17.5 ug/L
NS -Not Sampled
F:\PROJECTS\NSCC\MQNITOR\HISTRC_2.WB2
-----
N530 NS31 N532 u 1 u 1 u 1 u u 1 u 1 u 1 u
B 1.4 B 1.8 B 1.6 B
u 0.4 u 0.4 u 0.4 u
u 0.4 u 0.4 u 0.4 u
B 0.2 u 0.2 u 0.2 u u 0.3 u 0.3 u 0.3 u u 0.3 u 0.3 u 0.3 u
u 0.3 u 0.3 u 0.3 u
u 0.2 u 0.2 u 0.28 B
u 0.3 u 0.3 u 0.3 u
u 0.3 u 0.3 u 0.3 u
u 0.3 B 0.3 u 0.3 u
u 0.3 u 0.3 u 0.3 u
u 0.3 u 0.3 u 0.3 u
u 0.3 u 0.3 u 0.3 u y 2 u 2 u 2 u u 2 u 2 u 2 u u 2 u 2 u 2 u u 1 u 1 u 1 u
u 1 u 1 u 1 u
J 1 u 1 u 1 u
------- -----
Quarter EX01 EX02
1093 5 u NS
2093 5 u 5 u
3093 5 u 5 u
4093 2.3 u 2.3 u
1094 2.1 u 2.1 u
2094 1.3 u 1.7 8
3094 1.6 u 1.6 u
4094 1.6 u 1.6 u
1095 2 1 u 2.1 u
2095 1.4 u 1.4 u
3095 1.2 u 1.2 u
4095 1.9 u 1.9 u
1096 4.8 u 4.8 u
2096 5 u 5 u
3096 5 u 5 u
4096 4.8 u 4.8 u
1097 0.5 u 0.74 8
2097 3 u 3 u
3097 3 u 3 u
4097 4 u 4.5 8
109B 4 u 4 u
2098 0 26 u 0.26 u
Units in ug/1
U -Not Detected
EX03
5 u
5 u
5 u
2.3 u
2.1 u
1.3 u
1.6 u
1.6 u
2.1 u
1.4 u
1.2 u
Ul u
4.11 u
5 u
5 u
4.6 u
0.5 u
3 u
10.4
4 u
4 u
0.26 u
Table 3-5D
Analytical Results -Metals
Plume Periphery Extraction and Mon·I1oring Wells
National Starch and Chemical Company
Salisbury, North Carolina
CADMIUM
EX04 NS29
5 u 5
5 u 5
5 u 5
2.3 u 2.3
2.1 u 2.1
1.3 u 1.3
1.7 8 1.6
1.7 8 1.6
2.1 u 2.1
1.4 u 1.4
1.2 u 1.2
1.9 u 1.9
4.8 u 4.8
5 u 5
5 u 5
4.8 u 4.8
0.5 u 0.5
3 u 3
3 u 3
17.8 4.5
4 u 4
0.26 u 0.26
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 10 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Li
u
8
u
u
-----
NS30 NS31 NS32
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
2.3 u 2.3 u 2.3 u
2.1 u 2.1 u 2.1 u
1.3 u 1.3 u 1.3 u
1.6 u 1.6 u 1.6 u
1.6 u 1.6 u 1.6 u
2.1 u 2.1 u 2.1 u
1.4 u 1.4 u 1.4 u
1.2 u 1.2 u 1.2 u
1.9 u 1.9 u 1.9 u
4.8 u 4.8 u 4.8 u
5 u 5 u 5 u
5 u 5 u 5 u
4.8 u 4.8 u 4.8 u
0.5 u 0.5 u 0.5 u
3 u 3 u 3 u
3 u 26.9 3 u
4 u 4 u 4 u
4 u 4 u 4 u
0.26 u 0.26 u 0.26 u
--- -- ---- ---
Quarter EX01 EX02
1093 12 NS
2093 10 u 12.8
3093 10 u 13.7
4093 2.7 u 2.7 u
1094 2 3 u 3.1 8
2094 2.9 u 2.9 u
3094 24 u 2.4 u
4094 3 B 3 8
1095 4.3 u 4.3 u
2095 2 u 2 u
3095 3.1 u 5.1 B
4095 2.4 u 2.9 B
1096 7.7 8 4.9 u
2096 5 u 5 u
3096 5 u 31.1
4096 49 u 17.1
1097 5 u 5 u
2097 5 u 5.6 B
3097 5 u 5 u
4097 4 u 4 u
1098 4 u 4 u
2096 4.8 J 4.2 J
Units in ug/1
U -Not Detected
EX03
10 u
10 u
10 u
2.8 8
2.4 8
2.9 u
2.4 u
2.4 u
4.3 u
2 u
3.4 B
2.4 u
7.8 8
5 u
5 u
62,6
5 u
5 u
5 u
4 u
4 u
8.25 J
Table 3-SE
Analytical Results -Metals
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury. North Carolina
CHROMIUM
EX04 NS29
10 u 11.1
10 u 14.5
10 u 10
2.7 u 2.7
4,3 8 3
2.9 u 2.9
2.4 u 2.4
3.9 8 2.4
4.3 u 4.3
2 u 2
3.1 u 3.1
2.4 u 2.4
7.4 8 6.9
5 u 5
5 u 5
4.9 u 4.9
11.6 5.8
5 u 5
5 u 5
4 u 4.3
4 u 4
4.1 J 12.3
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 50 ug/L
Bold font indicates detected concentration greater than ROD Perlormance Standard
NS· Nol Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
u
u
B
u
u
u
u
u
u
u
B
u
u
u
B
u
u
B
u
- ------
NS30 NS31 N532
10 u 77.5 10 u
10 u 74 10 u
10 u 22.2 10
2.7 u 2.7 u 2.7 u
2.7 B 2.3 u 2.3 u
2.9 u 13.3 2.9 u
2.6 8 2.4 u 3.1 B
2.4 u 2.4 u 2.4 B
4.3 u 4.3 u 4.3 u
2 u 2 u 2 u
3.1 u 3.1 u 3.1 u
2.4 u 2.4 u 2.4 u
9.8 B 4.9 u 8.8 B
5 u 5 u 5 u
5 u 5 u 5 u
4.9 u 4.9 u 4.9 u
5 u 7.2 B 5 u
5 u 5 u 5 u
5 u 5 u 5 u
4 u 4 u 4 u
4 u 101 4 u
4.1 J 12.9 4 u
- - -- --
Quarter EX01 EX02
1093 222 NS
2093 206 7180
3093 112 10800
4093 24.3 10800
1094 25.1 14300
2094 78.8 17100
3094 50.3 15100
4094, 42 14000
1095 9.9 B 11900
2095 53.4 18800
3095 117 18300
4095 98.6 19000
1096 142 17900
2096 132 16100
3096 53.1 16300
4098 205 16800
1097 345 18000
2097 461 11600
3097 316 13900
4097 332 16900
1098 345 11000
2098 237 12100
Units in ug/1
-
EX03
39~,0
2760
3360
11200
11000
3980
1430
3640
2010
4810
3970
3380
2130
2855
4270
3920
2610
3960
3840
4510
4695
4675
- -- -Table 3-SF
Analytical Results -Metals -
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
MANGANESE
EX04 NS29
4290 475
3270 192.5
4810 201
5090 177
5610 153
5280 265
5430 287
4970 259
4730 239
4170 268
3210 611
4750 3810
3580 4030
3860 1780
3185 8560
3340 5640
5140 4820
4530 3710
4330 12000
3880 18400
4520 22200
4130 32100
B -Estimated concentration greater than the Instrument Detection limit but less than the Reporting limit
ROD Performance Standard: 7,700 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
t'i:lijtj ti UI !;I --- - ---
NS30 NS31 NS32
839 17.9 80,6
1620 47.1 78.2
1435 28.9 108
2110 21.4 99.8
2170 22.1 107
2270 52 106
1930 26.1 106
2480 20.4 108
2360 372 107
2290 25.8 117
1800 35.7 107
1990 63.9 112
1540 60.3 92.6
1720 141 105
1570 123 109
1400 510 109
1660 1110 114
1510 993 114
1530 1100 115
1520 1870 118
147 2670 118
1250 4150 139
----

-
-

-
---

-
-
Quarter EX01 EX02
1093 20 u NS
2093 20 u 75.5
3093 20 u 20 u
4093 11.8 B 13.8 B
1094 10.4 u 10.4 u
2094 6.2 u 6.2 u
3094 6.9 u 6.9 u
4094 6.9 u 6.9 u
1095 10.3 u 10.3 u
2095 5.5 u 5.5 u
3095 7.2 u 7.2 u
4095 8.8 u 8.8 u
1096 15.3 u 15.3 u
2096 15 u 15 u
3096 15 u 43.8
4096 15.3 u 15.3 u
1097 20 u 20 u
2097 20 u 20 u
3097 20 u 20 u
4097 16 u 16 u
1098 16 u 16 u
2098 14 u 14 u
Units in ug/1
U • Not petected
EX03
20 u
20 u
20 u
8.4 u
10.4 u
6.2 u
6.9 u
6.9 u
10.3 u
5.5 u
7.2 u
8.8 u
15.3 u
15 u
15 u
81.6
20 u
20 u
20 u
16 u
16 u
14 u
Table 3-SG
Analytical Results -Metals
Plume Periphery Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
NICKEL
EX04 NS29
20 u 20
20 u 20
20 u 20
8.4 u 8.4
10.4 u 10.4 ·
6.2 u 6.2
6.9 u 6.9
6.9 u 6.9
10.3 u 10.3
5.5 u 5.5
7.2 u 7.2
8.8 u 8.8
15.3 u 15.3
15 u 15
15 u 15
15.3 u 15.3
20 u 20
20 u 20
20 u 20
16 u 16
16 u 16
14 u 14
B -Estimated concentration greater than the Instrument Detection limit but les~-than the Reporting limit
ROD Performance Standard: 350 ug/L
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
---

-
---
NS30 NS31 NS32
20 u 39.3 B 20 u
20 u 47.5 20 u
20 u 20 u 20 u
8.4 u 8.4 u 8.4 u
10.4 u 10.4 u 10.4 u
6.2 u 9.6 B 6.2 u
6.9 u 6.9 u 6.9 u
6.9 u 6.9 u 6.9 u
10.3 u 10.3 u 10.3 u
5.5 u 5.5 u 5.5 u
7.2 u 7.2 u 7.2 u
8.8 u 8.8 u 8.8 u
15.3 u 15.3 u 15.3 u
15 u 15 u 15 u
15 u 15 u 15 u
15.3 u 15.3 u 15.3 u
20 u 20 u 20 u
20 u 20 u 20 u
20 u 20 u 20 u
16 u 16 u 16 u
16 u 51.6 16 u
14 u 23.2 J 14 u
------------
Quarter EX01 EX02
1093 2 u NS
2093 2 u 2 u
3093 2 u 2 u
4093 2.3 u 4.6 u
1094 1.7 u 3.4 u
2094 2.6 u 1 6 B
3094 3.1 u 3 1 u
4094 3.1 u 3.1 u
1095 0.9 u 0.9 u
2095 2.7 B 3 B
3095 1 7 u 1.8 B
4095 1 u 1 u
1096 1.6 u 32 u
2096 0.8 u 1.6 u
3096 0.8 u 1.6 u
4096 0.8 u 08 u
1097 6.9 12.4
2097 5 u 9.8
3097 5 u 5 u
4097 5 u 10.5
1098 5 u 55
2098 4.3 u 4.4 J
Units in ug/1
U • Not Detected
E<03
4 u
2 u
2 u
4.6 u
3.4 u
2.6 u
3.1 u
3.1 u
0.9 u
2.7 u
1. 7 u
1 u
1.6 u
0.8 u
1.6 u
0.8 u
5
5 u
6.3
5 u
5 u
4.3 u
Table 3•5H
Analytical Results -Metals
Plume Periphery Extraction ;md Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
SELENIUM
EX04 NS29
4 u 2
2 u 2
2 u 2
2.3 u 2.3
1.7 u 1.7
2.6 u 2.6
3.1 u 3. 1
3.1 u 3.1
0.9 u 0.9
2.7 u 2.7
1. 7 u 3
1 u 1
1.6 u 3.2
0.8 u 0.8
0.8 u 1.6
0.8 u 1.6
5 u 5
5 u 7.2
5 u 5
5 u 5
5 u 12.8
4.3 u 15.6
B -Estimated concentration greater than the Instrument Detection limit but less than the Reporting Limit ROD Performance Standard: 10 ug/L
Bold font indicates detected concentration greater than ROD Pertormance Standard
NS -Not Sampled
F:\PROJECTS\NSCC\MONITOR\HISTRC_2.WB2
u
u
u
u
u
u
u
u
u
u
8
u
u
u
u
u
u
u
u
-------
NS30 NS31 NS32
2 u 2 u 2 u
2 u 2 u 2 u
2 u 2 u 2 u
2.3 u 2.3 u 2.3 u
1.7 u 1.7 u 1.7 u
2.6 u 2.6 u 2.6 u
3.1 u 3.1 u 3.1 u
3. 1 u 3.1 u 3.1 u
0.9 u 0.9 u 0.9 u
2.7 u 2.7 u 3.2 B
2 B 2.7 B 2 8
1 u 1 u 1 u
1.6 u 1.6 u 1.6 u
0.8 u 0.8 u 0.8 u
1.6 u 0.8 u 0.8 u
0.8 u 0.8 u 0.8 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
5 u 5 u 5 u
4.3 u 4.3 u 4.3 u
I
I
I
I
I
I
I
I
I
I
I
I
I
WeUID EX--05 EX-OSOL EX-,)6 EX--060LB EX--07
Sample No. 10696383 10B963830L 10696391 10696391DLB 10696409
Sample Date 06/16198 06/16198 06/16198 06/16198 06/16198
Dilution Factor Perlonnanca 500,0 5000,0 1.0 20.0 10.0
Associated Method Blank Standard VBLK1838 VBLK183 VBLK178B VBLK1788 VBLK183B voes
Acetone 3,500 17000 B 43000 DJ 240 E 430 B 59 JB Be<,zone 5 5000 u 50000 u 10 u 200 u 100 u Brornodichloromethane 5 5000 u 50000 u 10 u 200 u 100 u CNon,rom, 5 5000 u 50000 u 10 u 200 u 100 u 1, 1-DichJoroethene 7 5000 u 50000 u 10 u 200 u 100 u
1,2-0ichloroethane 5 220000 E 340000 D 390 E 550 100 u 1,2~ 6 5000 u 50000 u 10 u 200 u 100 u Ethy!l>ef,zene 3,500 5000 u 50000 u 10 J 200 u 100 u
Methytene chk:ride 5 5000 u 50000 u 10 u 200 u 100 u Toluene 2,000 14000 15000 DJ 75 73 J 56 J
1, 1,2-Trictuoroethane 5 5000 u 50000 u 10 . u 200 u ioo u T richJoroethene 5 5000 u 50000 u 10 u 200 u 100 u
Vinyl ctuoride 2 5000 u 50000 u 2 J 200 u 100 u
Xylene 350 5000 u 50000 u 10 u 200 u 100 u
D,Jution Factor 10.0 . 1.0 1.0
Associated Method Blank SBLK13739 SBLK13739 SBLK13739
SVOCs
Bis(2-chloroethyl)ether 5 110 u 11 u 11 u
4-Nitrophenol 350 260 u 2B u 2B u
Metals .
Arsenic 10 1,3 u . 1.3 u 1.3 u
Barium 1,000 540 J 90.3 J 246
Beryllium 17.5 40 u 1 u 1 u Cadmium 10 6.9 0.26 u 0.26 u
Chromium so 160 u . 4 u 15.4
Manganese 7,700 255000 3170 26200
Nickel 350 960 J 14 u 14 u
Selenium 10 66.9 4.3 u 8.2 Zinc 7,350 200 u 5 u 6.7 J
Units 1n ug/1
U -Not Detected
a 1orgamcs) • anatyte also detected in associated method blank
B (inorganics) -concentration greater lhan Instrument Detection limit (IDL) but less than Conttact Requited Detection lim1l (CRDL)
J -estimated concentration less than the dotection limit
O • concentration in diluted run sample
Bold font indicates detected concentration greater than Performance Standard
Italic Joni indicates detection limit in an undiuted sample greater than the Performance Standard
Table :>6
Comparison of Second Quarter 1998 Analytical Results tot Trench Area Wells to Pertonnance Standad:s
National Stan::h and Chemical Company
. __ Salisbury, North Carolina
EX--08 EX--08Dl EX--09 EX.OSOL EX-10 EX-100L EX-100LB
10896417 106964170L 10696425 10696425DL 10696433 10696433Dl 10696433DL8
06/16198 06/16198 06/16198 06/16198 06/19/98 06/19/98 06/19/98
250.0 2500.0 100.0 500.0 50.0 500.0 1000.0
VBLK183 VBLK183 VBLK183 VBLK183B V8LK183 VBLK183 V8LK1838
56000 E 72000 D 14000 14000 DB 74000 E 100000 DE 03000 B
2500 u 25000 u 1000 u 5000 u 500 u 5000 u 10000 u 2500 u 25000 u 1000 u 5000 u 500 u 5000 u 10000 u 2500 u 25000 u 1000 u 5000 u 500 u 5000 u 10000 u 2500 u 25000 u 1000 u 5(00 u 500 u 5000 u 10000 u 140000 E 220000 D 54000 E asooo D 21000 E 29000 D 29000
2800 25000 u 13000 15000 D 20000 E 44000 D 48000 2500 u 25000 u 660 J 570 DJ 2000 1900 DJ 1900 J 420 J 25000 u 220 J 5(()() u 130 J 5000 u 10000 u 20000 ;?~ DJ 15000 16000 D 7600 8900 D 9100 J 2500 u 25000 u 1000 u 5000 u 500 u 5000 u 10000 u 2500 u 25000 u 1000 u 5000 u 500 u 5000 u 10000 u 2500 u 25000 u 1000 u 5000 u 210 J 5000 u 10000 u 1100 J 25000 u 2300 1500 DJ 6200 6300 D ◄700 J 10.0 10.0 100.0 10.0
SBLK13739 SBLK13739 SBL.K13739 SBLK13739 SBL.K13739 .
1900 noo E 7100 D 30000 E 23000 D .
260 u 270 u 2?00 u 260 u
1.3 u 1.3 u 1.3 u .
60 u 60 u 60 u .
40 u 46,B J 40 u .
7.5 1.9 2.3 .
160 u 160 u 160 u
311000 178000 18◄000
1330 J 940 J . 560 u
78,7 43 ..
1540 2450 1950
I NOTE: According to Pace laboratory. the anJaytical results for sample EX-OODL did not qualify and analytical results from sample EX-OOOLB should be used.
I
I
I
I F:\PROJECTS\NSCC\MONITOR\2Q9B\2Q98.'t-182
I
Page 1 of 1
NS-09 NS-09DL NS--09DLB NS-10 NS-100l NS-11 NS-15
10fl9633.4 10696334DL 10696334DLB 10696342 106963420L 10096359 10696367 06/16198 06/16198 06/16198 06/16198 06/16198 06(16198 06/16198
10.0 100.0 200.0 2.0 25.0 1.0 1.0 VBLK178 VBLK178 VBU<183B VBLK1788 VBLK178B VBI...K1788 VBLK178
53 J 380 DJ 550 JB 6 J 110 DJ 2 J 6 J 100 u 1000 u 2000 u 20 u 250 u 10 u 10 u 100 u 1000 u 2000 u 20 u 250 u 10 u 10 u
100 u 1000 u 2000 u 20 u 250 u 10 u 10 u
100 u 1000 u 2000 u 20 u 250 u 10 u 10 u 6200 E 20000 DE 25000 970 E 1900 D • J 130
100 u 1000 u 2000 u 20 u 250 u 10 u 10 u 100 u 1000 u 2000 u 20 u 250 u 15 10 u
100 u 1000 u 2000 u 20 u 250 u 10 u 10 u
76 J 1000 u 2000 u 5 J 250 u 6 J 7 J 100 u 1000 u 2000 u 20 u 250 u 10 u 10 u 100 u 1000 u 2000 u 20 u 250 u 10 u 10 u 17 J 1000 u 2000 u 20 u 250 u 10 u 10 0 22 J 1000 u 2000 u 4 J 250 u 64 10 u
1.0 1.0 1.0 1.0 S8U<13739 S8LK13739 . SBLK13739 S8LK13739
3 J . . 10 u . 11 u 10 u
26 u 2B u 27 u 26 u
1.3 u . 1.3 u . 1.3 u 1.3 u
270 259 . 190 J 4$9
1 u . 1 u 1 u 1 u
0.26 u 0.26 u . 0.26 u 0.26 u
B.4 J . 5.5 J 4 u 5.2 J
12400 2670 . 133 15600
23.3 J 14 u 14 u 14 u
4.3 u 4.3 u . 4.3 u 4.6 J
47.1 . 32.2 11.3 J 5 u
- ---- ---
Quu1er EXOS EX06 EX07
1093 NS NS NS NS
2Q93 NS NS NS NS
3093 NS NS NS NS
4093 NS NS NS NS
1Q94 NS NS NS NS
2094 NS NS NS NS
3094 NS NS NS NS
4Q94 NS NS NS NS
1095 NS NS NS NS
2095 NS NS NS NS
309S NS NS NS NS
4095 NS NS NS NS
1Q96 NS NS NS NS
2Q96 24000 D 420 7100 DJ 230000
3096 3200 J 36 920 J 11000
4Q96 28000 300 D 550 DJ 72000
1097 27000 B 170 B 4900 B ',20000
2097 33000 B 470 OB 4000 B 130000
3097 34000 500 D 2000 B 67000
4097 36000 '" D 3600 :(20000
1098 29000 B 120 B 3300 B 83000
2098 17000 B 430 B 59 JB 72000
Untts in ug,1
U · Not Detected
J · Estimated concentration less ttian the detectrnn lmut
B -Constituent a!so detected In associated method blank (concenlra\JOt\ in method blank unknow,1)
E -Exceeds calIbrallon range
D -Concentration from dduted Nn sampje
ROD Performance Standard: 3,500 ug/L
Bold font indicates detected coocentration greater than ROD Performance Stanaatd
llalic lont llld1cates detection hrmt greater lllan ROD Performance Standard
Shading mchcates ·e· qualified concentration !or whid'l a diluted run concentration Is unavai'able
NR • Not Repo(ted
NS -Not Sampled
f_\PROJECTSINSCC\MONLTOR\HISTRC_2.'N82
EX08
D
DB
OB
B
0
OB
D
- - -
Table 3-7A
Analytical Results -voes
Trench Area Extraction aM Monitoring WeUs
Na\Jonal Starch and Chemical Company
Salisbury. North Caroltna
ACETONE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
23000 D '3000
'100 8200
37000 75000
nooo DB 96000
40000 B 82000
23000 B 49000
-
D
B
B
B
19000 g~~~~~m
24000 OB 12000 DB
14000 '3000 B
---- ---
NSOI NS10 NS11 NS11
NS NS NS NS
10 u 10 u 10 u NR
3000 D 100 15 10 u
720 330 u 130 67 u
130 500 u 4100 50 u ..... B 2100 B .. B 25 u
330000 670 u 29 530
390000 270 "' 18 B
"400 D 620 u 21 25 u
'7000 D 600 10 u 10 u
450 D 170 u 10 u 120
1600 670 u 17 21
7 J 500 u 10 u 20 u
110 100 u 10 u ' J
22 J a J 7 J 8:, J ' 200 100 u 10 u 10) u
110 B .. BJ 6 BJ 15 B .. JB 78 JB 22 B 10 u
830 B 300 OB J2 OBJ 40 B
180 100 u ,. 7 J
" JB 10 u 10 u ' JB
53 J 6 J 2 J • J
-----
Quarter EXOS EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
4094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
.C095 NS NS
1096 NS NS
2096 .. J 25
3096 5000 u 10
4096 2000 u 10
1097 2000 u 10
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
Urwtsin uo,1
U -Not Delecte<l
J • Esllfnated coocentratroo less than the detectton brrut
ROD Performance Standard: 5 ug/l
u
u
u
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
" 3300
250
250
250
250
250
1000
100
Bold font mdlc.ares detected concentration greater than ROD Pertonnance Standard
11.811c font inaic.ates detection limt greater than ROD Perfom,ance Standard
NR -Not Repo,ted
NS · Not Sampled
F.IPROJECTS\NSCC\MONITOR\HlSTRC_2.'NB2
- -
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
J ,. J u 5000 u
u 5000 u
u 5000 u
u 5000 u u 5000 u u 5000 u u 2500 u u 2500 u
---Table 3-7B
Analytical RescltJ. voes
Trench Area Extrac!ion and Mootonng Welts
National Stardl and Chl'lll'lical Company
Salisbury, Nolth Carolina
BENZENE
-
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
84 J 40 J
3300 u 1700 u
2500 u 5000 u
2500 u 5000 u
2500 u 5000 u
2500 u 5000 u
2500 u 5000 u
1000 u 500 u
1000 u 500 u
-------
NS09 NS10 NS11 NS15 NS NS NS NS
5 u 5 u 5 u NR
10 u 10 u 10 u 10 u
250 u 330 u 25 u " u
10 u 500 u 500 u 50 u
3100 u 310 u 5 u 12 u
8300 u 330 u 5 u 25 u 10000 u 17 u 5 u 5 u , J 310 u 5 u 12 u
500 u " u 5 u 5 u
5 u 83 u 5 u 5 u
" u 330 u 5 u 8 u
10 u 250 u 5 u 10 u
50 u 50 u 5 u ' u 50 • u 10 u 10 u \~ it>,1 u 100 u 100 u 10 u 10/ u 100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 10 u 10 u 10 u
100 u 20 u 10 u 10 u
--- -- -
Quuter EXOS EX06
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
<094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
◄095 NS NS NS
1096 NS NS NS
2096 120 u 25 u 120
3096 5000 u IO u 3300
◄096 2000 u IO u 250
1097 2000 u IO u 250
2097 2000 u IO u 250
3097 2000 u IO u 250
4097 2000 u IO u 250
1098 5000 u IO u 1000
2098 5000 u IO u 100
Units in ug,1
U • Not Detected
ROD Performance Standard: 5 ug/L
Italic font indicates detec11on 11rrut greater ttlan ROD Perf0011ance Standard
NR • Not Reponea
NS -Not Sample(J
F.\PROJECTSV-.,SCC\MONITORIHISTRC_2.'NB2
EX07
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120 u
u 5000 u
u 5000 u u 5000 u
u 5000 u
u 5000 u
u 5000 u
u 2500 u u 2500 u
-- -
Table 3-7C
Analytical Rasu!ls -VOCs
Trench Area Extraction erv.1 Monitonng Wells
Nabonal Stardl and Chemical Company
Sal!sbury, North Carolina
BROMODICHLOROMETHANE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
120 u 120
JJOO u 1700
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 500
1000 u 500
- -------
NSOI NS10 NS11 NS11
NS NS NS NS
5 u 5 u ' u NR
10 u IO u 10 u IO u
250 u JJO u 25 u " u
10 u 500 u 500 u so u
JIOO u 310 u 5 u 12 u
8300 u 330 u 5 u 25 u
10000 u 17 u 5 u 5 u
5 u 310 u 5 u 12 u
500 u ., u 5 u 5 u s u B3 u 5 u 5 u
57 u 330 u 5 u ' u
IO u 250 u 5 u IO u u so u so u 5 u 5 u u so u IO u 10 u \··:) u • u 100 u 100 u 10 u u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u IO u u 100 u 100 u IO u IO u u 100 u 100 u 10 u IO u u 100 u IO u IO u IO u u 100 u 20 u IO u IO u
--- --
Qu.u1er EX05 EX06
1Q93 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
309' NS NS
<094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 .. J 25
3096 5000 u ,o
<096 2000 u 10
1097 2000 u ,o
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
Units in uW,
U · Not Deteaed
J • Esbmated concentration less IJ'lan the detection hmit
ROD Performance Standard: 5 ug/l
u
u
u
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120
3300
250
250
250
250
250
1000
100
Bold font IndIcates aeteca,d concentrabon greater than ROD Performance Standard
Jtahc font indJcales de!ectlon limit greater than ROD Performance Standard
NR • Not Reponeo
NS . Not Sampled
F.IPROJECTSWSCC\MONITOR\HISTRC_2.W82
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120 u u 5000 u u 5000 u u 5000 u u 5000 u u 5000 u u 5000 u u 2500 u u 2500 u
-- -
Table 3-70
Analytical Results • voes
Trench Area Extraction end Monitoring Wall1
Nabonal Starch and Chemical Company
Sa5sbu'y. NoM Carolina
CHLOROFORM
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
120 u 120
3300 u 1100
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 500
1000 u 500
--------
NSOO NS10 NS11 NS1fi
NS NS NS NS
5 u 5 u 5 u NR
10 u , J 10 u 10 u
250 u 330 u 25 u 61 u
10 u 500 u 500 u 50 u
3100 u 310 u 5 u 12 u
8300 u 330 u 5 u 25 u
10000 u 11 u 5 u 5 u
5 u 310 u 5 u 12 u
500 u " u 5 u 5 u
5 u 83 u 5 u 5 u
57 u 330 u 5 u 8 u
10 u 250 u 5 u 10 u u 50 u 50 u 5 u 5 u u 50 u 10 u 10 u " 10 u • u 100 u 100 u 10 u ' 10: u u 100 u 100 u 10 u 1rl u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u 10 u
u 100 u 100 u 2 J 10 u
u 100 u 10 u 10 u 10 u
u 100 u 20 u 10 u 10 u
--- -
Quarter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS ,a .. NS NS ,a .. NS NS
309' NS NS ,a .. NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS ,a,. NS NS
2Q96 350000 D 920
3096 5000 u 10
<Q96 430-000 D 240
1097 510000 D " 2097 470000 D 530
3097 J.«1OOO D 550
4097 380000 D 140
,098 340000 D 80
2Q98 340000 D 550
Units in ug11
U -Not Detected
J • Esbmate<I concentration less than Iha detectJon lmut
E • E.,:;ceeds catibfaoon range
D -Concentration from diluted run sample
ROD Pertormance Standard: 5 ug/l
- -
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
83000
u 3300
D 50000
34000
D 35000
D 36000
27000
1,000
100
Bold loot inwcates detected concentrabon greater than ROD Performance Standard
Italic font indlcates aeiecoon lmut greater than ROD Per1cxmance Standard
-
D
u
D
D
D
D
D
u
Shalllng inc!lcates ·e· qua!1fiea concentration for which a d1!uted run c.oncentraoon is unavad.lble
NR -Not Rej'.)Ofled
NS -Not Sampled
F.\PROJECTS\NSCCIMONITOR\HISlRC_2.'11182
-
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
:130000 D
5000 u
350000 D
J,0000 D
;:90000 D
:110000 D
270000 D
noooo D
::20000 D
-- -
Table 3-71:
Ar.alytical Results -voes
Trench Area &traction 8lld Monitonng Wells
National Starch and Chemical Company
Salisbury, Nor111 Carobna
1,2-DICHLOROETHANE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
71000 D 210-00
3300 u 1700
190000 D 35000
110000 D 310-00
130000 D 30000
180000 D 53000
130000 D 69000
110000 D 44000
18000 D 29000
---- ----
NS09 NS10 NS11 NS15
NS NS NS NS
10000 D 11000 D ' u NR
14000 D aooo D 100 440 D
4700 2100 " u ,,.
170 aa00 500 u ...
3100 u '700 • ...
8300 u 7100 5 u , ..
10000 u 420 5 u f'J!!iilfKlllt1i,ll!fii ,. 9100 5 u '70
500 u 9100 D 5 u ,,. D
11 7600 D • 280 D
1700 1100 5 280 • J 6100 • 280
D ... t{~~5c\!ti'1!.§E;~ 5 u t~W-~1~~\ u 2100 D 2200 D 11 _-rr.' f 7100 D 4600 D 34 · uo;
10000 D 2000 D 400 D 190
4400 D 170 3 J 120
490-0 D 1100 170 D 180 D
5900 D 1600 210 D 150
D 10000 D 120 D 24 100
D 28000 1900 D • J 130
-----
Ouuter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
<094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 '20 u 25
3096 5000 u 10
<096 2000 u 10
1097 2000 u ,0
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
UJ'lltsm ugl1
U • Not Detected
J -Es\Jmated coocantra\Jon less lha/:1 the detection lirmt
ROD Performance Standard: 7 ug/l
u
u
u
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120
3300
250
250
250
250
250
1000
100
Bold font indicates detected concantra!Jon greater Ulan ROD Performance Standard
Italic font indicates detectron lm11t greater than ROD Performance Standard
NR . Nol Reported
NS -Nol Sampled
F.\PROJECTSINSCC\MONITOR\HJSTRC_2.'NE2
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120 u u 5000 u u 5000 u u 5000 u u 5000 u
u 5000 u
u 5000 u u 2500 u u 2500 u
---Tabla 3-7F
Analytical Results. voes
Trench Area Extraction and Morutoring WuUs
National Starch and Chemical Company
Salisbury, North Carolina
1, 1-DICHLDROETHENE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
no u 120
3300 u 1700
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 500
1000 u 500
Page 6 ol 14 ------- -
NS09 NS10 NS11 NS11 NS NS NS NS
10 5 u 5 u NR
11 2 J 10 u 10 u
250 u 330 u 25 u ., u
10 u 500 u 500 u 50 u -u 440 u 7 u 18 u 1'000 u 470 u 7 u 35 u
14000 u 23 u 7 u 7 u • J 440 u 7 u 18 u
700 u 130 u 7 u 7 u • 120 u 7 u 7 u
BO u <70 u 7 u " u • J 250 u 5 u 10 u u 50 u 50 u 5 u s u u 50 u 10 u 10 u ' _. f(l, u ' u 15 J 100 u 10 u 10j u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u 10 u u " J 100 u 10 u 10 u u 100 u 100 u 10 u 10 u u 100 u 10 u 10 u 10 u u 100 u 20 u 10 u 10 u
- -- --
Quarter EXDS EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
4094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2oo; 350 25
30o; 5000 u 10
,oo; 250 J 10
1097 2000 u 10
2097 2000 u 10
3097 2000 u ,o
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
Units mug,\
U · Not ~IIM:tttd
J -Esllmat&d concentra11on !ass tnan lhe detection limit
ROD Performance Standard: 6 ug/L
u
u
u
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120
3300
250
250
250
250
250
1000
100
Bold l001 IOd,c.ates detected concenl1a\Jon greater than ROD PerfOfTTlance Standard
Italic lent mdIca1es aetectJon t1m11 greater lllan ROD Performanca Standard
NR . Not Repofte<l
NS . Not Sample<!
F.\PROJECTS\NSCC\ti.,ONllOR\HISTRC_ "2 V'-IB2
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u '" u 5000 u
u 5000 u
u 5000 u
u 5000 u
u 5000 u
u 1000 J
u 1200 J
u 2800
-- -
Table 3-7G
Analytical Results -voes
Trench Acea ExtractJon and Monctonng WeUs
Natiooal Starch and Chemical Company
Salisbwy. North Carolina
1,2-DICHLOROPROPANE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
9400 D 12000
12000 '1000
11000 71000
12000 6'000
9100 56000
11000 60000
12000 75000
12000 41000
13000 44000
-- ------
NSOII NS10 NS11 NS11
NS NS NS NS
' u 2 J ' u NR
10 u 1 J 10 u 2 J
250 u 330 u 25 u 61 u
10 u 500 u 500 u so u
3800 u 380 u 8 u " u
10000 u 400 u ' u 30 u
12000 u 20 u 8 u 8 u
' u 380 u ' u 15 u
""' u 110 u 8 u ' u • u 100 u ' u ' u
" u 400 u ' u 10 u
10 u 250 u ' u 10 u
D so u so u ' u ' u
D so u 10 u 10 u \ . 10' u ii ' 1oj 100 u 100 u 10 u u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
D 100 u 10 u 10 u 10 u
D 100 u 20 u 10 u 10 u
-----
Cuuter EXOS EX06
,093 NS NS
2093 NS NS
3093 NS NS
4Qg3 NS NS
10 .. NS NS
209' NS NS
30 .. NS NS
400◄ NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 190 25
3096 5000 u 10
4096 120 J 10
1097 2000 u 10
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
Units 1n ug,'J
U -Not Detec1ed
J -Estimated c.oncentrabon len man the detection limit
ROD Performance Standard: 3,500 ug/L
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120
u 3300
u 250
u 250
u 250
u 250
u 250
u 1000
J 100
lla!tc lont Iodlcat11s detection br1111 greater than ROD Performance Standarc:I
NR -Not Reported
NS . Not Sampled
F .\PROJECTS\NSCC\MON!TOR\HIS T RC _2.INB2
EX07
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 140
u 5000 u
u 5000 u
u 5000 u u 5000 u u 5000 u
u 5000 u
u 2500 u
u 2500 u
---Tabla 3-7H
Ar.alytical Results -voes
Trench Area Extraction and MOllltoling W9Jls
National St.asch and Chemical Company
Sallsbury, North Ca101ina
ETHYLBENZENE
-
exo, EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
1300 2400
590 J 2400
460 J 2400 J
410 J 2200 J
2500 u 1600 J
2500 u 1900 J
500 J 2500 J
490 J 1900
660 J 2000
-----P1g1 8 of 14 - -
NSOt NS10 NS11 NS15
NS NS NS NS
32 ' J " NR .. 4 J 140 10 u
250 u 330 u 300 67 u
6 J 500 u 500 u 50 u
6200 u 620 u 10 u 25 u 17000 u 670 u 91 50 u
20000 u 33 u 40 10 u
4 J 620 u 120 25 u
1000 u 180 u 76 10 u
5 J 170 u .. 10 u
110 u 670 u 57 17 u
10 250 u 62 10 u
50 u 50 u 61 5 u
50 u 10 u 100 ·._-• 1Q._ I u ,
6 J 100 u " 10j u
100 u 100 u 140 10 u
100 u 100 u 20 10 u
100 u 100 u 5 J 10 u
100 u 100 u 22 10 u
100 u 10 u " 10 u
100 u 20 u " 10 u
- - -- - - -
Qu.uter EX0S EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
209' NS NS NS
309' NS NS NS
409' NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 " J 25 u 120 u
3096 1900 BJ 4 BJ 1200 BJ
4096 130 J 2 J 16 J
1097 2000 u IO u 250 u
2097 2000 u 10 u 250 u
3097 2000 u IO u 250 u
4097 "' J 10 u .. J
1098 5000 u IO u 1000 u
2098 5000 u 10 u 100 u
Units in~
U -Not Detected
J -Estimated concentration less lhan the detection lim1t
B -Constituent also detected m associated method l:>lank (concentration in method blank unknown,
ROD Performance Standard: 5 ug/l
Bold foot Indicates detected concentration greater than ROD Performance Standard
Jtalic 1001 ma,cates detection hm1t greater than ROD Performance Standard
NR -Not Reponed
NS -Not Sampled
F.\PROJECTS\NSCC\MONITOR\HIS'iRC_2.'NB2
-
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
" J
5000 u
300 J
5000 u
5000 u
5000 u
5000 u
2500 u
"' J
---Table 3-71
Analytical Resvlts -voes
Trenth Area Extraction and Monitonng Wells
NaliotlaJ Sia/Ch end ChE.micel Company
SaJisbWy. North Caroline
METHYLENE CHLORIDE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS .. J .. ... BJ .. ,
170 J 370
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 200
220 J 130
t'dlj,_ \;I U! 14 - - -- - - --
.... NS10 NS11 NS1li
NS NS NS NS
·' u 3 J 1 J NR • BJ • BJ • BJ 3 BJ
NR NR NR NR
NR NR NR NR
JIOO u 170 BJ 5 u 12 u
14000 B "' B • B " BJ
13000 B 17 u 5 u " B • BJ '" B 2 BJ 12 u
1300 B "' B 1 B 5 B
5 u 83 u 5 u 5 u
51 u 330 u 5 u 1 BJ
10 u 73 BJ 2 BJ 3 BJ
J 50 ·u 10 BJ 5 u 2 J
BJ 50 u 2 J 10 u •, , '·' J t ' J 1 J 1 J 10 u 1. J u 100 u 100 u 10 u 1/ u u 100 u 100 u 10 u 10 u
u 100 u 100 u 10 u 10 u
u 100 u 100 u 10 u 10 u
J 100 u 10 u 10 u 10 u
J 100 u 20 u 10 u 10 u
--- -
Ou•rter EXOS EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1a!l4 NS NS
2Q\l4 NS NS
309' NS NS
,a.,. NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1Q96 NS NS
2Q96 16000 D " 3096 19000 67
◄Q96 20000 65
1097 2,000 " 2097 23006 37
3097 22000 62
4097 21000 " 1Q98 21000 40
2Q98 1◄000 75
Un1\s in ugA
U -Not Detected
J -Estimate<! concentration less than tne detection limit
D -Concentration tram diluted run sample
ROD Performance Standard: 2,000 ug/l
- -
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
3200
2200
1700
1600
1200
1100
1100
620
56
Bold font indicates detected coocentfabon greater than ROD Perfocmanco Standan:I
Italic font indicates de1ectton hmn greater than ROD Pertonnance Standard
NR • Not Reponed
NS -Not Sampled
F \PROJECTSV>ISCC\MONITOR\HISTRC_2.'vV82
--
EXO!
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
68000 D
J Z8000
25000
)0000
?-4000
15000
28000
J 14000
J 20000
- - -
Tabla 3-7J
Analytical Results . voes
Trench Area Extraction and Monitonng Wells
National Starch end Chemic.al Company
Salisbury, North Carollna
TOLUENE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
38000 D 14000
2-15000
215000 15000
28006 16006
20000 12000
23006 12000
22000 14000
21000 D 9000
15000 7&00
- - - --- - -
NS09 NS10 NS11 NS15
NS NS NS NS
""' D 2 J " NR
1100 D 17 " 23
330 330 u ,,. 18 J
100 500 u 500 u 50 u
0200 u 620 u 7 J 13 J
17000 u 670 u 13 17 J
20000 u 33 u • J 10
47 620 u 23 10 J
340 J 180 u 11 6 J
130 170 u 15 5 J
410 670 u • J ' J
180 250 u 6 11
D 170 50 u 11 15
69 ' J ,, 2:' J • 200 9 J ,, 6 / J
100 u 100 u 26 5 J
80 J 100 u 5 J ' J
150 100 u 7 J 10
110 100 u " 8 J
30 J 10 u ' J 3 J
76 J 5 J 6 J 7 J
--- -
a~rter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
309' NS NS
409' NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
""" NS NS
2096 .. J 25
3096 5000 u 10
1097 2000 u fO
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
Units in ug,1
U · Not Detecte(;J
J • Esbmated concentration less lhan the detection ltmil
ROD Performance Standard: 5 ug/L
--
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 1'0
u 3300
u 250
u 250
u 250
u 250
u 1000 u 100
Bold loot indicates detected concentr3tion greater than ROD Performance Standard
lta11c font inchcates detection l1m1I granter than ROD Perfomiance Standard
NR -Not Reponea
NS. Not Sampled
F.\PROJECTS\NSCC\MONlTQR\HISTRC_2.WB2
--
exoe
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u !20 J
u 5000 u u 5000 u u 5000 u
u 5000 u
u 5000 u
u 2500 u
u 2500 u
-- -
Tabla 3-iK
Analytical Results -voes
Trench Area Extraction and Morutoong Wells
National Starch and Chemical Company
Sat:sbuty, North Carolina
1, 1,2-TRICHLOROETHANE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
120 u 120
3300 u 1700
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 500
1000 u 500
-
u
u
u
u
u
u u
u
---- ---
NSot NS10 NS11 NS11
NS NS NS NS
3 J 10 5 u NR • J 12 10 u 10 u
250 u 330 u 25 u " u
fO u 500 u 500 u 50 u
J!OO u J!0 u 5 u 12 u
8300 u 330 u 5 u 25 u
10000 u " u 5 u 5 u
5 u 310 u 5 u 12 u
500 u 89 u 5 u 5 u
5 u 83 u 5 u 5 u
57 u 330 u 5 u • u
10 u 250 u 5 u 10 u
50 u 50 u 5 u 5 u
50 u • J 10 u : 10-, u ,
100 u 20 J 10 u 10 j u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 100 u 10 u 10 u
100 u 2 J 10 u 10 u
100 u 20 u 10 u 10 u
--- -- ---
... ·:il1 EXOS
' NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120 u ., 5000 u ., 5000 u
·' 5000 u
5000 u
5000 u
5000 u
2500 u
2500 u ·-
. ·' , ..... , ;, ,.,,,,,_.:,. .... -
-- -
Table 3-7L
Analytical Results -voes
Trench Area ExtraCl.ioo and Monitoring Welts
National Starch ana Chftmical Company
Salisbury, NoM Carolina
TRICHLOROETHENE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS .NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
120 u IW
3300 u 1700
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
1000 u 500
1000 u 500
--
NSOt
NS
' 3
250
10
3100
8300
10000
5
500
5
57
10
u 50
u 50
u 100
u 100
u 100
u 100
u 100
u 100
u 100
------
NS10 NS11 NS11
NS NS NS
u 1 J ' u NR
J 10 u 10 u 10 u
u 330 u 25 u 61 u
u 500 u 500 u 50 u
u 310 u 5 u " u
u 330 u 5 u ,s u
u 17 u ' u ' u
u 310 u ' u " u
u " u ' u ' u
u 83 u ' u ' u
u 330 u 5 u • u
u 250 u ' u 10 u
u 50 u 5 u 5 u
u 10 u 10 u \.·· 10,, u ' u 100 u 10 u .• 10) u
u 100 u 10 u 10 u
u 100 u 10 u 10 u
u 100 u 10 u 10 u
u 100 u 10 u 10 u
u 10 u 10 u 10 u
u 20 u 10 u 10 u
-----
Qu1rter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
/094 NS NS
2094 NS NS
3094 NS NS
◄094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 .. J 25
3096 5QOO u ,o
1097 200-0 u ,o
2097 2000 u 10
3097 2000 u ,o
4097 2000 u /0
1098 5QOO u 10
2098 5QOO u 10
Units m ug.,1
U -Not Detected
J -Estimated concen11a11on less tnan Ille da1ec11on brrut
ROD Performance Standard: 5 ug/L
u
u
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120
3300
250
250
250
25Q
/000
100
Bold font indicates detected concentration greater than ROD Per10m1ance Standard
Italic font me11cates detection hrrut greater than ROD Performance Standard
NR -Not Reponad
NS -NOC SampllKI
F:\PROJ ECT S\NSCC\MON/TOR\HIS T .:i.c _ 2 .v...B2
-
u
u
u
u
u
u
u
u
-
EXO!
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
120 J
5QOO u .... u .... u
5QOO u
5QOO u
2500 u
2500 u
---Table 3-7K
Analytical Results -VOCI
Trench Afea Extraction an-J Monitoring wens
Nabonal Starch and Chemical Company
Sallsbury, North Carolina
1, 1,2-TRJCHLOROETHANE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
,20 u 120
3300 u 1700
2500 u 5QOO
2500 u ....
2500 u ....
2500 u 5QOO
1000 u 500
1000 u 500
--
NS0t
NS
3 • 250
,o
3/00
8300
/0000
5
500
5
57
10 u ..
u ..
u 100
u 10-0
u 100
u 100
u 100
u 100
--
NS10
NS
J 10
J 12 u 330 u u ... u u 3,0 u u 330 u
u 17 u u 3/0 u u " u u 83 u u 330 u u 250 u
u .. u
u • J
u 20 J u 100 u
u 100 u
u 100 u u 2 J u 20 u
---P■ge1.
u
u
u
u
u
u
u
" u
-·-,, 'l115Hltl ~a
NS -i~:· IS NS " • •·1e:·3 u1 C NR • IQ '4$G.~3 "JJ:· hs· /0 u II' 2s.: 'lla..ieJ u ~, " "·· l<S 500. ~$09<1 u: ,s .. u !<I ,· l~SQ94 u NS 12 u. ~-· ; ;] NS094 uJ. l,s 25 U, ,s
' N0094 u s • u-.-. s 1! NSQ95 u NS 12 U, Ls
5 N$095 u NS 5 u1 s
5 NSQ95 u NS 5 u, s
' NIQ95 u NS 8 u HS
5 NSQ96 u NS 10 ul ~s • 1211J96 u 20 5 u uj :. 11, JJillll96 u . ~·10,, , ~, 11, 25<096 u ..:.000 1oi J .~
11, 2!m97 u l,oo 10 ~ bo
11, 2$.Ci97 u ul>oo 10 u u; •o
11 25097 u ul,oo 10 u I 0
II 2sa:::197 u ul>oo 10 V u 0
1 1ooa,,a u ··'-10 .LJ I 0
""'" U5QOO u 10
Units In ug/1
u • Nol Oetectoa
J • EsumetDd concontre.Uon leu U'iarl 1h11 attec:Clon Umlt
ROD Performance Standard: 5 ug/L
::1 rr-artce s~ lont llldicatos c1e1oct1on l!mit greater 11\an ROD Perl
'l!R. Noe Reoonea
"lS • ND/_ S8ffl01oo
------
Ouuter EXOS EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
209,,t, NS NS
3094 NS NS ,o .. NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 120 u 25
3096 5000 u 10
4096 2000 u 10
1097 2000 u 10
2097 2000 u 10
3097 2000 u 10
4097 2000 u 10
1098 5000 u 10
2098 5000 u 10
UN" m"' U -Not Detected
J • Estimated concentration lass than the detection limit
ROD Performance Standard: 5 ug/L
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS u 120 u 3300 u 250 u 250
u 250
u 250
u 250
u 1000
u 100
lta11c loot Indicates detection limlt greater than ROD Performance Standan:l
NR -Not Reported
NS -Nol Sampled
F.\PROJECTSINSCC\MONITOR\HISTRC_2.'N82
EX07
- -
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
u 120 u u 5000 u u 5000 u u 5000 u u 5000 u u 5000 u u 5000 u u 2500 u
u 2500 u
---Table 3-7L
AnatyticaJ RHl.l!ts -voes
Trench Area Extraction and MorutOfir,g Wells
National Starch and Chemical Company
Salisbury, NoM<..:arolina
TRICHLOROETHENE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
120 u 120
3300 u 1700
2500 u 5000
2500 u 5000
2500 u 5000
2500 u 5000
2500 u ' 5000
1000 u 500
1000 u 500
t'a1,10 1:.1 or 14 ------- -
NSOt NS10 NS11 NS11 NS NS NS NS
5 u 1 J 5 u NR
3 J 10 u 10 u 10 u
250 u 330 u ,, u " u
10 u 500 u 500 u so u
3100 u 310 u 5 u 12 u
8300 u 330 u 5 u 25 u 10000 u 17 u 5 u 5 u 5 u 310 u 5 u 12 u
500 u 89 u 5 u 5 u
5 u 83 u 5 u 5 u
57 u 330 u 5 u ' u
10 u 250 u 5 u 10 u u so u 50 u 5 u ' u u so • u 10 u 10 u \" ti>: u u 100 u 100 u 10 u 10/ u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u 10 u u 100 u 100 u 10 u 10 u u 100 u 10 u 10 u 10 u u 100 u 20 u 10 u 10 u
- -- --
Quuter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
<094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 ... 50
3096 ,000 u 10
<096 2000 u ' 1097 970 J 4
2097 1200 J 3
3097, ... J 3
4097 020 J 10
1098 5000 u 10
2098 5000 u 2
UOIIS inug.-1
U -Not Detected
J • Estimated concentra!Jon less than the detection limit
0 -Concentration from diluted run sample
ROD Performance Standard: 2 ug/l
u
u
J
J
J
J
u
u
J
-
EJ<07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
250
3300
250
53
250
250
250
1000
100
Bold fool mchcates de!ede(I concentra!Jon greater than ROD Perfocmance Standard
Italic lont indicates deleCllori llmit greater than ROD Performance Standard
NR -Not Reported
NS -Not Sampled
F.\PROJECTS\NSCC\MONITORIHISTRC_2.'N82
--
EX08
NS
NS
NS
NS
' NS
NS
NS
NS
NS
NS
NS
NS
NS
u 250 u
u ,000 u
u ,000 u
J 5000 u
u ,000 u
u 5000 u
u 5000 u
u 2500 u
u 2500 u
- --Table 3-7M
Analytical Results. voes
Trench Area E.:traction and MOl'lltonng Wens
National Starch and Ch6mical Company
Salisbury, North Carolina
VINYL CHLORIDE
EJ(O, mo
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
250 u 220
3300 u 1700
2,00 u 5000
2500 u 5000
2,00 u 5000
2,00 u 5000
2,00 u 5000
1000 u 250
1000 u 210
--------
.... NS1O NS11 NS15
NS NS NS NS
10 u • J 10 u NR ... OJ 10 u 10 u ,.
71 J 330 u 25 u ., u .. 500 u ""' u "' u
1200 u 120 u 2 u ' u
3300 u 130 u 2 u 10 u
4000 u 7 u 2 u 2 u .. 120 u 2 u • 200 u 36 u 2 u • 11 33 u 2 u • , .. 130 u 2 u ' 12 ,00 u 10 u 20 u
J .. J 100 u 10 u 10 u
u 50 u 10 u 10 u \ * '°". u • u 110 100 u 10 u _,. 1oj u u 20 J 100 u 10 u ' J
u .. J 100 u 10 u 2 J u .. J 100 u 10 u 2 J u 100 u 100 u 10 u 10 u
J " J 10 u 10 u 10 u
J 17 J 20 u 10 u 10 u
.. - --
Q1u1ner EXO5 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
109' NS NS
2094 NS NS
3094 NS NS
409' NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 470 25
3096 5000 u 10
<096 25-0 J 06
1097 2000 u 10
2097 2000 u 10
3097 390 J 10
4097 '40 J 10
1098 5000 u 10
2098 5000 u 10
Unats llluo,,'1
U -Not Det&etfld
J -Esumated concentrauon less than the detection limit
D • Coocentra11on from diluted run sample
ROD Performance Standard: 350 ug/L
u
u
J
u
u
u
u
u
u
-
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
29
3300
18
25-0
25-0
250
250
1000
100
Bold font Indicates detected concentration greater than ROD PertormallC8 Standard
llal1c tont 11"1C11cetes deteCllon limit greater than ROD Pertormance Standard
NR • Not Reponed
NS -Nol Sampled
F .\PROJECTS\NSCC\MONI T QRIHIS TRC _ 2 Vv'82
--
EX08
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
J "' u 5000 u
J 5-000 u
u 5000 u
u 5000 u
u 5000 u
u 5-000 u
u 680 J
u · 1100 J
- --Table 3-7N
Analytical Results -voes
Trench Area Extraction and Monitoring WeUs
National Starch and Chemical Company
Salisbury, North Carolina
XYLENE
EX09 EX10
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
NS NS
3000 7700
2300 J 7800
1'00 J 7300
1300 J 6800
1000 J 6800
1100 J 6300
1800 J '300
1800 6200
2300 6200
------
NS09 NS10 NS11 NS11
NS NS NS NS
69 10 150 NR
120 DJ 10 220 1 J
250 u lJO u ... ., u
13 ,co u ,co u 50 u
6200 u '" u 100 25 u
17000 u 670 u 110 50 u
20000 u l3 u 50 10 u • J 620 u 120 ,. u
1000 u 180 u " 10 u
15 170 u 66 10 u
110 u 610 u 22 17 u
23 25-0 u 21 10 u
D 12 J 5-0 u .. • u • J 10 u 50 • ',.' 10., u
21 J 100 u 1<0 ' 1 j J
100 u 100 u 180 10 u
100 u 100 u 35 10 u
100 u 100 u • J 10 u
100 u 100 u 42 10 u
100 u 2 J 110 10 u
22 J • J .. 10 u
------------
Quarter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
4094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 2500 u 100 u
3096 5000 u 4 J
4096 170 J 16
1097 530 u 10 u
2097 110 u 10 u
3097 500 u 10 u
4097 55 J 10 u
1098 53 u 10 u
2098 110 u 11 u
Units in ug/1
U -Not Detected
J -Estimated concentration less than the detection limit
ROD Performance Standard: 5 ug/L
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
200
100
100
100
100
110
18
14
11
u
u
u
u
u
u
J
J
u
Table 3-8A
Analytical Results -SVOCs
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BIS(2-CHLOROETHYL)ETHER
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
320 J 10000 35000
5000 u NR 47000
2500 u 6600 29000
210 7200 29000
390 3800 D 14000
620 7500 30000
810 7400 D 16000
1100 10000 D 68000
1900 7100 D 23000
Bold fonl indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Stanclard
NR -Not Reported
NS -Not Sampled
1':IPROJcCTSINSCC\MONITORIHISTRC_2.WB2
D
D
D
D
D
D
D
-----Page 1 of 2 - -
NS09 NS10 NS11 NS15
NS NS NS NS
10 u 11 u 11 u 11 u
56 u 10 u 10 u 10 u
530 u 50 u 10 u 42 u
8 J 220 u 10 u 10 u
20 u 1100 u 11 u 22 u
6 u 110 u 5 u 21 u
11 u 22 u 5 u , .
10 u ' \;
' 53 u 520 u 5 u 11 u
27 u 250 u 5 u 6 u
28 u 310 u 6 u 5 u
50 u 260 u 5 u 5 u
10 u 500 u 10 u 10 u
50 u 200 u 50 u 50 u
50 u 200 u 10 u 20 u
20 u 100 u 10 u 10 u
10 u 10 u 10 u 10 u
20 u 100 u 10 u 10 u
20 u 10 u 10 u 10 u
2 J 11 u 11 u 10 u
11 u 10 u 10 u 11 u
3 J 10 u 11 u 10 u
-------;-----
Quarter EXOS EX06 EX07
1Q93 NS NS NS
2Q93 NS NS NS
3Q93 NS NS NS
4Q93 NS NS NS
1Q94 NS NS NS
2Q94 NS NS NS
3Q94 NS NS NS
4Q94 NS NS NS
1Q95 NS NS NS
2Q95 NS NS NS
3Q95 NS NS NS
4Q95 NS NS NS
1Q96 NS NS NS
2Q96 6200 u 250 u 500 u
Table 3-88
Analytical Results -SVOCs
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
4-NITROPHENOL
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
6200 u 6200 u 2500
3Q96 12000 u 25 u 250 u 12000 u 12000 u 25000 4Q96 6200 u 25 u
1Q97 1300 u 25 u
2Q97 260 u 25 u
3Q97 1200 u 26 u
4Q97 260 u 26 u
1Q98 130 u 26 u
2Q98 280 u 28 u
Units in ug/1
U -Not Detected
J • Estimated concentration less than the detection limit
ROD Performance Standard: 350 ug/L
250 u
260 u
250 u
280 u
260 IJ
260 u
26 u
Italic font indicates detection limit greater than ROD Performance Stand_ard
NS -Not Sampled
F:IPROJECTSINSCC\MONITOR\HISTRC_2.WB2
6200 u 2500 u 7500
25 u 520 u 260
250 u 100 u 5300
1400 u 530 u 1000
260 u 260 u 260
260 u 260 IJ 270
260 u 270 u 260
u
u·
u
u
u
u
u
u
u
-----
NS09 NS10 NS11 NS15
NS NS NS NS
50 u 53 u 56 u 54 u
140 u 25 u 26 u 25 u
1300 u 120 u 26 u 110 u
25 u 540 u 26 u 26 u
50 u 2600 u 27 u 54 u
28 u 530 u 27 u 110 u
56 u 110 u 26 u ·, .. "61 u J ,,
260 u 2600 u 26 u 84 u
140 u 1200 u 27 u 28 u
140 u 1600 u 28 u 27 u
250 u 1300 u 25 u 26 u
25 u 1200 u 25 u 25 u
120 u 500 u 120 u 120 u
120 u 500 u 25 u 50 u
3 J 250 u 25 u 25 u
25 u 26 u 26 u 26 u
50 u 250 u 25 u 25 u
50 u 26 u 26 u 26 u
26 u 27 u 26 u 26 u
27 u 26 u 26 u 26 u
26 u 26 u 27 u 26 u
-- --- ---- -- -
Quarter EX0S EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS .. NS
2094 NS NS \ NS
3094 NS NS \ NS
\ ' 4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 11 1.1 u 1.1 u
3096 2.2 u 1.1 u 1.1 u
4096 4.4 u 1.1 u 1.1 u
1097 7 u 7 u 7 u
2097 10.6 7 u 7 u
3097 7 u 7 u 7 u
4097 6 u 6 u 6 u
1098 6 u 6 u 6 u ' 2098 1.3 u 1.3 u 1.3 u
Units in ug/1
U -Not Detected I
Table 3-9A
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, Nortt, Carolina
ARSENIC
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
22 u 11 u 11
2.2 u 2.2 u 2.2
2.2 u 4.4 u 2.2
7 u 9.8 B 7
7 u 7 u 7
7 u 7 u 7
9 B 8.5 B 9.5
6 u 6 u 6
1.3 u 1.3 u 1.3
B -Estimated concentration greater than the Instrument Detection Limjt but less than the Reporting Limit
ROD Performance Standard: 10 ug/L I i Bold font indicates detected concentration greater than ROD Performance Standard
Italic font indicates detection limit greater than ROD Performance Stan~ard
NS -Not Sampled
F:IPROJECTSINSCCIMONITORIHISTRC_2.WB2
u
u.
u
u
u
u
B
u
u
-------
NS09 NS10 NS11 NS15
NS NS NS NS
2 u 2 u 2 u 2 u
2.2 B 2 u 2 u 2 u
8.2 B 2.4 u 2.4 u 4.8 u
2.9 u 2.9 u 2.9 u 5.8 u
2.6 u 2.6 u 2.6 u 5.2 u
2.1 u 2.1 u 2.1 u 2.1 u
2.1 u 2.9 B 2.1 u 3-:7 B I
1.5 B 1.7 B 2 B 0~8 u
2.7 u 2.7 u 2.7 u 2.7 u
3.2 B 2.2 B 2.4 B 1.9 u
1.5 u 1.5 u 1.5 u 1.5 u
1.1 u 1.1 u 1.1 u 1.1 u
1.1 u 1.1 u 1.1 u 1.1 u
1.1 u 1.1 u 1.1 u 1.1 u
1.1 u 1.1 u 1.1 u 1.1 u
7 u 7 u 7 u 7 u
7 u 7 u 7 u 7 u
7.4 B 7 u 7 u 7 u
6 u 6 u 6 u 6 u
6 u 6 u 6 u 6 u
1.3 u 1.3 u 1.3 u 1.3 u
- ----- -
Quarter EX0S EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 124 B 313 425
3096 159 B 106 B 305
4096 157 B 107 B 319
1097 158 B 80.9 B 335
2097 138 B 87.6 B 315
3097 179 B 98.2 B 280
4097 217 70.8 B 260
1098 244 81.6 B 290
2098 540 J 90.3 J 248
Units in ug/1
- - - --Table 3-9B
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BARIUM
EX0B EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
25.6 B 12.9 B 19.3 B
28.6 B 17.9 B 18.6 B·
29.1 B 17.1 B 21.4 B
21 B 10.9 B 29.2 B
22.9 B 11.8 B 18 B
26 B 15.7 B 19.1 B
25.5 B 15.5 B 17.8 B
21.3 B 11 B 15.7 B
80 u 80 u 80 u
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 1,000 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Not Sampled
F:IPROJECTS\NSCC\MONITORIHISTRC_2.WB2
--- - -
NS09 NS10 NS11 NS15
NS NS NS NS
1480 297 115 B 448
3160 155 B 190 B 445
1020 155 B 85.9 B 444
412 276 143 B 416
264 144 B 134 B 418
227 131 B 127 B 461
428 96.3 B 151 B \; 3'/0 ~ ' 364 573 124 B 169 B
2030 193 B 140 B 428
1200 176 B 237 387
1340 164 B 98.8 B 452
993 156 B 156 B 432
752 277 136 B 533
504 181 B 144 B 296
785 293 301 405
1270 305 124 B 398
329 205 199 B 342
523 236 576 508
507 280 178 B 467
605 234 178 B 365
270 259 180 J 469
-- -- --
Quarter EX05 EX06 EX07
1093 NS ·NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 0.3 u 0.3 u 0.3
3096 0.3 u 0.3 u 0.3
4096 0.3 u 0.3 u 0.3
1097 2 u 2 u 2
2097 2 u 2 u 2
3097 2 u 2 u 2
4097 1 u 1 u 1
1098 1 u 1 u 1
2098 40 u 1 u 1
Units in ug/1
U -Not Detected
- -- ---
u
u
u
u
u
u
u
u
u
Table 3-9C
Analytical Results -Metals ·
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
BERYLLIUM
EX0B EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
34 26.1 25.1
22.7 27.5 21.3
20.6 25.6 18.8
18.5 22 14.9
15.4 17.1 12.1
14 19.8 14.3
13.4 18.4 13.8
14.1 18.9 14.9
40 u 46.8 J 40 u
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 17.5 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Nol Sampled
F:IPROJECTSINSCCIMONITORIHISTRC_2.WB2
---- -
NS09 NS10 NS11 NS15
NS NS NS NS
1 u 1 u 1 u 1 u
3.4 B 1.8 B 1.9 B 1.2 B
0.75 B 0.4 u 0.4 u 0.4 u
0.4 u 0.4 u 0.4 u 0.4 u
0.21 B 0.2 u 0.2 u 0.32 B
0.3 u 0.3 u 0.3 u 0.3 u
0.3 u 0.3 u 0.3 u ·e,3 u • 0.3 u 0.3 u 0.3 u ri.3 u
0.22 B 0.2 u 0.24 B 0.2 u
0.3 u 0.3 u 0.55 B 0.3 u
0.3 u 0.3 u 0.3 u 0.3 u
0.3 u 0.4 B 0.3 u 0.3 u
0.3 u 0.3 u 0.3 u 0.3 u
0.3 u 0.3 u 0.3 u 0.3 u
0.4 B 0.3 u 0.6 B 0.3 u
2 u 2 u 2 u 2 u
2 u 2 u 2 u 2 u
2 u 2 u 2 u 2 u
1 u 1 u 1 u 1 u
1 u 1 u 1 u 1 u
1 u 1 u 1 u 1 u
------------
Quarter EX05 EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 17.5 5 u 5
3096 10.6 4.8 u 4.8
4096 6.8 4.8 u 4.8
1097 6.9 0.5 u 0.74
2097 12.8 3 u 4.2
3097 15.4 18 4.7
4097 21 4 u 4
1098 10.1 4 u 4
2098 8.9 0.26 u 0.26
Units in ug/1
U -Not Detected
u
u
u
B
B
B
u
u
u
Table 3-9D
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
CADMIUM
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS Ns· NS
44 12.7 12.6
18.7 7.7 6.6
15.5 8.4 4.8
13.4 6.1 4.3
3 u 3 u 3
7.4 4.6 3
4.1 B 4 u 4.3
12.7 5.4 6.3
7.5 1.9 2.3
B -Estimated concentration greater than the Instrument Detection l.imif but less than the Reporting Limit.
ROD Performance Standard: 10 ug/L
Bold font indicates detected concentration greater than ROD Performar,c:.e Standard
NS -Not Sampled
F:IPROJECTSINSCCIMONITORIHISTRC_2.WB2
u
B
u
u
B
-----
NS09 NS10 NS11 NS15
NS NS NS NS
5 u 5 u 5 u 5 u
5 u 5 u 5 u 5 u
2.3 u 2.3 u 2.3 u 2.3 u
2.1 u 2.1 u 2.1 u 2.1 u
1.3 u 1.3 u 1.3 u 1.3 u
4.9 B 1.6 ·U 1.6 u 1.6 u
1.6 u 1.6 u 1.6 u . 1 :6 u • 2.1 u 2.1 u 2.1 u i1 u
1.4 u 1.4 u 1.4 u 1.4 u
1.8 B 1.2 u 1.2 u 1.2 u
1.9 u 1.9 u 1.9 u 1.9 u
4.8 u 4.8 u 4.8 u 4.8 u
5 u 5 u 5 u 5 u
5 u 5 u 5 u 5 u
4.8 u 4.8 u 4.8 u 4.8 u
1.5 B 0.5 u 0.5 u 0.5 u
3 u 3 u 3 u 3 u
3 u 3 u 3 u 3 u
4 u 18 4 u 4 u
4 u 4 u 4 u 4 u
0.26 u 0.26 u 0.26 u 0.26 u
- -- - ---- - -- -
Quarter EX0S EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 18.1 5 u 7.5
3096 25.1 4.9 u 14.8
4096 26.2 4.9 u 16.9
1097 5 u 5 u 5
2097 5 u 5 u 5
3097 5 u 5 u 5.8
4097 11 4 u 4
1098 4 u 4 u 4
2098 160 u 4 u 15.4
Units in ugtl
U -Not Detected
B
u
u
B
u
u
Table 3-9E
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
CHROMIUM
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
80.2 48 44.4
84.7 63.9 56.1
79.8 63.5 46.5
19.8 27.4 16.3
12.6 19.5 10.3
9.6 B 19.2 11.8
9.9 B 17.6 11.2
4 u 14.4 4
160 u 160 :J 160
B -Estimated concentration greater than the Instrument Detection Limil but less than the Reporting Limit
ROD Performance Standard: 50 ug/L
Bold font indicates detected concentration greater than ROD Performa;ice Standard
NS -Not Sampled
F:IPROJECTS\NSCCl."'1ONITORIHISTRC_2.WB2
u
u
-- -- ---
NS09 NS10 NS11 NS15
NS NS NS NS
50.1 14.2 10 u 11. 7
304 11.7 35.6 10.6
127 16.3 17.4 3.6 B
20.6 36.9 4.2 B 3.6 B
11.9 6.1 B 2.9 u 2.9 u
24.3 3.1 B 2.4 u 4.3 B
7.1 B 8.8 B 4.1 B ' ·. ·4,3 B ,
8.8 B 9.1 B 4,3 u 4'.3 u
127 4 B 2 u 2 u
42 6.7 B 5.2 B 3.1 u
31.1 2.4 u 2.4 u 2.4 u
4,9 u 4.9 u 7 B 9.4 B
5 u 5 u 5 u 5 u
20.3 5 u 5 u 5 u
97.2 4,9 u 34.2 4.9 u
375 5 u 5 u 5 u
21.7 5 u 8.2 B 5 u
62.7 5 u 57.2 5 u
69.6 4 u 4 u 4 u
175 5.1 B 4 u 4 u
8.4 J 5.5 J 4 u 5.2 J
------
Quarter EX05 EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 200000 7680 73700
3096 170000 3250 64200
4096 144000 3620 60400
1097 138000 2520 68000
2097 125000 2850 43600
3097 118000 3300 41300
4097 98900 2180 40200
1098 161000 2810 43400
2098 255000 3170 26200
Units in ug/1
ROD Performance Standard: 7,700 ug/L
-----Table 3-9F
Analytical Results -Metals -
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
MANGANESE
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
516000 98800 198000
393000 160000 159000
332000 170000 138000
352000 192000 126000
232000 114000 91900
231000 143000 132000
203000 113000 103000
271000 138000 143000
311000 178000 184000
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Nol Sampled
F:IPROJECTSINSCCIMONITORIHISTRC_2.WB2
-----Page ti of 9 --
NS09 NS10 NS11 NS15
NS NS NS NS
51300 14300 63.1 15200
60500 7760 118 15000
28100 3540 55.6 15100
15300 7930 71.5 17600
11000 9650 47 17800
6760 9200 67 18600
14300 2760 83.2 \: 14$00 ' 18800 14400 124 1.r.100
51800 8960 62.6 16800
33600 9320 248 13400
34600 8880 37.8 16200
25700 5860 32 14200
20500 10050 48.2 16400
13800 2290 44 8670
18200 4850 841 13800
31600 4260 67.2 14300
10300 2150 889 11800
22400 2730 366 16700
19600 2760 136 15500
8280 1830 132 13000
12400 2670 133 15600
--- --- ---- --
Quarter EX05 EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 678 19.7 8 117
3096 601 15.3 u 110
4096 654 15.3 u 91.1
1097 732 20 u 69.7
2097 587 20 u 61.3
3097 622 20 u 35.8
4097 566 16 u 22.9
1098 591 16 u 16
2098 960 J 14 u 14
Units in ug/1
U -Not Detected
B
8
u
u
Table 3-9G
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
NICKEL
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
1990 645 698
1440 798 549
1350 906 505
1270 843 444
1140 653 365
1120 706 451
989 657 410"
1020 680 484
1330 J 940 J 560
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 350 ug/L
Bold font indicates detected concentration greater than ROD Performance Standard
NS -Not Sampled
F:IPROJECTS\NSCCIMONITORIHISTRC_2.WB2
u
----- --
NS09 NS10 NS11 NS15
NS NS NS NS
23.9 8 45.2 20 u 20 u
102 25.1 8 28.2 8 20 u
54 33.9 8 35.1 8 10.3 B
10.4 u 57.5 10.4 u 10.4 u
13.8 8 30.2 8 6.4 8 6.2 u
19.2 8 27.5 B 6.9 u 6.9 u
10.5 8 25.6 8 10.3 8 .. ·.7 8 J · ..
1.0.3 10.3 u 33.7 8 16.2 8 u
43.6 20.1 B 5.5 u 5.5 u
9.4 8 20.6 B 12 8 7.2 u
20.1 8 26.9 8 8.8 u 8.8 u
15.3 u 15.3 u 15.3 u 15.3 u
15 u 27.6 B 15 u 15 u
15 u 22.9 8 15 u 15 u
40.9 35.4 8 40.7 15.3 u
223 35.6 B 20 u 20 u
20 u 23.2 B 21.9 8 20 u
34.8 8 21 8 64.3 20 u
63.2 30.5 B 16.5 8 16 u
81.9 23.6 8 16 u 16 u
23.3 J 14 u 14 u 14 u
- ---- ---- - --
Quarter EX0S EX06 EX07
1093 NS NS NS
2093 NS NS NS
3093 NS NS NS
4093 NS NS NS
1094 NS NS NS
2094 NS NS NS
3094 NS NS NS
4094 NS NS NS
1095 NS NS NS
2095 NS NS NS
3095 NS NS NS
4095 NS NS NS
1096 NS NS NS
2096 8 u 0.8 u 1.6
3096 16 u 0.8 u 1.6
4096 5.2 u 1.3 u 1.3
1097 86.1 5 u 31.7
2097 77.3 5 u 24.7
3097 68.1 5 u 24.7
4097 66.1 5 u 19.5
1098 64.6 5 u 20.6
2098 66.9 4.3 u 8.2
Units in ug/1
U • Not Detected
u
u
u
Table 3-9H
Analytical Results • Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
SELENIUM
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
8 u 8 u 8
1.6 u 1.6 u 4
5.2 u 5.2 u 2.6
171 88.3 67.9
59.9 19.7 25.8
58.9 23.5 32.8
118 61.1 63.7
104 61.6 58.l
78.7 43 46
B • Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 10 ug/L
Bold font indicates detected concentration greater than ROD Performar,ce Standard
Italic font indicates detection limit greater than ROD Performance StanC'ard
NS -Not Sampled .
F:IPROJECTS\NSCCIMONITORIHISTRC_2.WB2
u
u
u
' .. ~ ... .., .... ;J ----- -
11!!!!!!!1
NS09 NS10 NS11 NS15
NS NS NS NS
10 u 2 u 2 u 2 u
4 u 2 u 2 u 2 u
6.9 u 2.3 u 2.3 u 4.6 u
1.7 u 1.7 u 1.7 u 3.4 u
2.6 u 2.6 u 2.6 u 5.2 u
3.1 u 3.1 u 3.1 u 3.1 u
3.1 u· 3.1 u 3.1 u \ .· 311 u I>
0.9 u 0.9 u 0.9 u 0.9 u
2.7 u 2.7 u 2.7 u 2.7 u
2 B 1.7 u 3.6 B 1.7 u
1 u 1 u 1 u 1 u
1.6 u 1.6 u 1.6 u 1.6 u
0.8 u 0.8 u 0.8 u 0.8 u
0.8 u 0.8 u 0.8 u 0.8 u
0.8 u 0.8 u 0.8 u 0.8 u
21.9 5 u 5.2 6.6
6.8 5 u 5 u 5 u
18.8 6.8 5 u 9.1
12.6 5 u 5 u 11.4
5 u 5 u 5 u 9
4.3 u 4.3 u 4.3 u 4.8 J
- - ---
Quarter EX05 EX06
1093 NS NS
2093 NS NS
3093 NS NS
4093 NS NS
1094 NS NS
2094 NS NS
3094 NS NS
4094 NS NS
1095 NS NS
2095 NS NS
3095 NS NS
4095 NS NS
1096 NS NS
2096 363 10.2 B
3096 234 3.7 B
4096 220 2.4 u
1097 221 25.1
2097 219 25.4
3097 188 24.7
4097 135 15 u
1098 126 15 u
2098 200 u 5 u
Units in ug/1
U -Not Detected
--
EX07
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
43.2
34.3
20.1
35.3
113
119
15 u
15 u
6.7 J
-

-

-

-
-Table 3-91
Analytical Results -Metals
Trench Area Extraction and Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
ZINC
EX08 EX09 EX10
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
NS NS NS
3200 2880 3280
1820 2750 2320
1690 2850 2120
1860 2900 2010
1510 2060 1360
1400 2230 1370
1250 1940 1230
1320 1960 1540
1540 2450 1950
B -Estimated concentration greater than the Instrument Detection Limit but less than the Reporting Limit
ROD Performance Standard: 7,350 ug/L
NS -Not Sampled
F:IPROJECTSINSCC\MONITORIHtSTRC_2.WB2
-

-
-----
NS09 NS10 NS11 NS15
NS NS NS NS
49.2 47.4 32.5 14.5 B
156 54 37.4 12.6 B
75.6 43.2 15 B 1.8 u
11.4 B 85.2 7.2 B 1.7 u
8.7 B 20.1 3.1 B 0.9 u
217 54.1 12.8 B 3.8 u
35.6 33.1 27.8 \ •' ·3,5 u ' ., ' 31 44.9 38.7 :t.5 u
141 24.8 13.2 B 5.8 u
46.6 16.6 B 41.3 2.6 u
13.8 B 24.5 5.2 u 5.2 u
10.8 B 28.6 8.2 B 3.6 B
37.8 24 9.6 B 6.4 B
16.3 B 25.4 3.9 B 2.5 B
84.2 41.1 65 30.6
111 50.6 11.9 B 11.7 B
10.9 B 37.2 22.4 5 u
47.9 54 127 15.1 B
107 49 31.2 15 u
153 91.1 29.8 15 u
47.1 32.2 11.3 J 5 u
I
I
I
I Well
Date Day
04/01/98 Wednesday
I 04/02/98 Thursday
04/03/98 Friday
04/04/98 Saturday
I 04/05/98 Sunday
04/06/98 Monday
04/07/98 Tuesday
04/08/98 Wednesday
I 04/09/98 Thursday
04/10/98 Friday
04/11/98 Saturday
I 04/12/98 Sunday
04/13/98 Monday
04/14/98 Tuesday
04/15/98 Wednesday
I 04/16/98 Thursday
04/17/98 Friday
04/18/98 Saturday
I 04/19/98 Sunday
04/20/98 Monday
04/21/98 Tuesday
04/22/98 Wednesday
I 04/23/98 Thursday
04/24/98 Friday
04/25/98 Saturday
04/26/98 Sunday I 04/27/98 Monday
04/28/98 Tuesday
04/29/98 Wednesday
I 04/30/98 Thursday
05/01/98 Friday
05/02/98 Saturday
05/03/98 Sunday
I 05/04/98 Monday
05105/96 Tuesday
05/06/98 Wednesday
I 05/07/98 Thursday
05/08/98 Friday
05/09/98 Saturday
05/10/98 Sunday
I 05/11/98 Monday
05/12/98 Tuesday
05/13/98 Wednesday
I 05/14/98 Thursday
05/15/98 Friday
05/16/98 Saturday
I
rlsERSIKRWI050551PUMP2098.WB2
Table 3-10
Pumping Rates -Second Quarter 1998
Plume Periphery Extraction Wells
National Starch and Chemical Company
Salisbury, North Carolina
Actual Pumping Rate (gpm)
EX-01 EX-02 EX-03 EX-04
19 13 32 18
19 13 32 19
18 13 32 19
.19 13 31 19
19 12 30 19
20 12 32 18
19 12 32 18
19 13 32 20
19 12 32 18
19 13 32 19
1S 13 32 19
19 13 32 19
19 13 32 17
19 13 32 18
19 13 32 18
19 13 32 18
20 13 32 20
18 13 35 15
18 13 33 15
18 13 32 17
18 12 28 17
18 13 30 18
19 13 31 16
19 13 31 16
19 13 30 18
19 13 30 19
18 12 32 13
17 12 32 15
16 12 31 15
15 12 31 15
17 12 31 15
19 13 31 18
18 13 32 17
20 13 32 18
17 14 34 16
22 15 32 16
20 13 32 16
18 13 33 17
19 13 32 17
18 13 30 17
17 13 32 17
17 13 32 17
17 13 32 18
18 13 32 17
18 13 32 18
18 13 30 19
Page 1 of2
Total Daily Ave.
82 20.5
83 20.75
82 20.5
82 20.5
80 20
82 20.5
81 20.25
84 21
81 20.25
83 20.75
83 20.75
83 20.75
81 20.25
82 20.5
82 20.5
82 20.5
85 21.25
81 20.25
79 19.75
80 20
75 18.75
79 19.75
79 19.75
79 19.75
80 20
81 20.25
75 18.75
76 19
74 18.~
73 18.25
75 18.75
81 20.25
80 20
83 20.75
81 20.25
85 21.25
81 20.25
81 20.25
81 20.25
78 19.5
79 19.75
79 19.75
80 20
80 20
81 20.25
80 20
I
I
I Well
Date Day
I
05/17/98 Sunday
05/18/98 Monday
05/19/98 Tuesday
05/20/98 Wednesday
I 05/21/98 Thursday
05/22/98 Friday
05/23/98 Saturday
05/24/98 Sunday
I 05/25/98 Monday
05/26/98 Tuesday
05/27/98 V.'e~ncsday
I 05/28/98 Thursday
05/29/98 Friday
05/30/98 Saturday
05/31/98 Sunday
I 06/01/98 Monday
06/02/98 Tuesday
06/03/98 Wednesday
I 06/04/98 Thursday
06/05/98 Friday
06/06/98 Saturday
06/07/98 Sunday
I 06/08/98 Monday
06/09/98 Tuesday
06/10/98 Wednesday
I 06/11/98 Thursday
06/12/98 Friday
06/13/98 Saturday
06/14/98 Sunday
I 06/15/98 Monday
06/16/98 Tuesday
06/17/98 Wednesday
I
06/18/98 Thursday
06/19/98 Friday
06/20/98 Saturday
06/21/98 Sunday
I 06/22/98 Monday
06/23/98 Tuesday
06/24/98 Wednesday
I 06/25/98 Thursday
06/26/98 Friday
06/27/98 Saturday
06/28/98 Sunday
I 06/29/98 Monday
06/30/98 Tuesday
Average
I
lusERS1KRW105o551PUMP2098.ws2
Table 3-10
Pumping Rates -Second Quarter 1998
Plume Periphery Extraction Wells
National Starch and Chemical Company
Salisbury, North Carolina
Actual Pumping Rate (gpm)
EX-01 EX-02 EX-03 EX-04
19 13 30 18
19 13 30 18
18 13 30 19
18 13 32 20
18 13 32 18
19 13 32 17
17 13 32 15
19 12 32 13
19 14 32 18
18 14 32 16
19 14 32 18
19 14 32 15
18 14 32 16
13 12 32 18
15 13 32 18
16 13 32 16
15 13 34 14
14 13 32 12
15 13 32 15
14 13 32 11
12 12 32 12
12 11 32 12
7 7 20 8
5 5 16 6
5 5 16 7
5 5 17 5
8 6 18 6
7 6 18 6
8 6 18 6
5 6 16 6
,; 6 16 6
5 6 16 6
5 6 16 6
6 5 17 6
6 5 17 6
6 5 17 6
5 5 17 5
6 6 17 5
6 5 17 6
6 5 17 6
6 5 16 6
5 5 16 6
5 5 16 5
5 6 14 6
5 5 15 5
15 11 28 14
Page 2 of2
Combined Daily Ave.
80 20
80 20
80 20
83 20.75
81 20.25
81 20.25
77 19.25
76 19
83 20.75
80 20
83 20.75
80 20
80 20
75 18.75
78 19.5
77 19.25
76 19
71 17.75
75 18.75
70 17.5
68 17
67 16.75
42 10.5
32 8
33 8.25
32 8
38 9.5
37 9.25
38 9.5
33 8.25
33 8.25
33 8.25
33 8.25
34 8.5
34 8.5
34 8.5
32 8
34 8.5
34 8.5
34 8.5
33 8.25
32 8
31 7.75
31 7.75
30 7.5
68 17
I
I
I
I Well EX-05
Date Day
04101196 Wednesday 2.1
I 04102196 Thursday 2.1
04103196 Friday 2.2
04104196 Saturday 2.3
I 04/05196 Sunday 2.2
04106196 Monday 2.3
04107196 Tuesday 2.1
04106196 Wednesday 2.3
I 04109/96 Thursday 1.0
04110196 Friday 1.0
04111196 Saturday 1.0
I 04112196 Sunday 1.0
04113196 Monday 2.0
04114196 Tuesday 1.6
04115196 Wednesday 1.6
I 04116196 Thursday 1.6
04117196 Friday 1.5
04116196 Saturday 1.3
I 04119196 Sunday 1.2
04120196 Monday 1.5
04121196 Tuesday 1.5
04122/96 Wednesday 1.7
I 04123196 Thursday 1.5
04124/96 Friday 1.0
04125196 Saturday 2.0
I
04126196 Sunday 2.0
04127196 Monday 1.0
04126196 Tuesday 2.0
04129196 Wednesday 2.0
I 04130196 Thursday 2.0
05101196 Friday 2.0
05102196 Saturday 2.0
I
05103196 Sunday 2.0
05104196 Monday
05105196 Tuesday
05106196 Wednesday
I 05107/96 Thursday 2.0
05106196 Friday 2.0
05/09/98 Saturday 2.0
I
05110196 Sunday 2.0
05111196 Monday 2.0
05112/96 Tuesday 2.0
05113196 Wednesday 2.0
I 05/14/98 Thursday 2.0
05115196 Friday 2.0
05116196 Saturday 2.0
I
lusERS1KRW105o551PUMP2D96.WB2
Table 3-11
Pumping Rates -Second Quarter 1998
Trench Area Extraction Wells
National Starch and Chemical Company
Salisbury, North Carolina
Actual Pumping Rate (gpm)
EX-06 EX-07 EX-06 EX-09
1.6 1.0 2.0 3.6
1.6 1.0 2.1 3.9
1.2 1.0 1.9 3.1
1.6 1.0 1.9 3.0
1.6 1.0 2.0 3.0
1.3 1.0 2.1 3.2
1.6 1.0 2.1 3.5
1.5 1.0 2.0 3.2
1.5 1.0 2.0 3.5
1.5 1.0 2.0 3.5
1.5 1.0 2.0 2.0
1.7 1.0 2.0 2.0
1.0 1.0 2.0 3.1
1.0 1.0 2.0 3.0
1.0 1.0 2.0 3.0
1.0 1.0 2.0 3.0
1.0 1.0 2.1 3.5
1.5 1.0 1.9 3.0
0.5 1.0 1.9 3.2
1.0 0.5 1.6 3.6
1.0 1.5 1.6 3.6
0.5 1.4 1.9 3.7
0.5 0.5 1.9 3.5
0.5 0.5 1.9 3.7
1.0 1.0 1.9 3.5
1.0 1.0 1.9 3.5
1.0 1.0 1.2 3.0
1.9 1.0 2.0 3.0
1.9 1.0 2.0 3.0
1.9 1.0 2.0 3.0
1.9 1.0 2.0 3.0
1.2 1.0 2.0 3.2
1.0 1.0 2.0 3.0
MAINTENANCE
1.0 1.0 2.0 3.1
1.0 1.0 2.0 3.7
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.7
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
EX-10 Total Daily Ave.
1.0 11.7 2.0
1.0 11.9 2.0
1.0 10.4 1.7
1.0 11.0 1.6
1.0 11.0 1.6
1.0 10.9 1.6
1.0 11.5 1.9
1.0 11.0 1.6
1.0 10.0 1.7
1.0 10.0 1.7
1.0 6.5 1.4
1.0 6.7 1.5
1.0 10.1 1.7
1.0 9.6 1.6
1.0 9.6· 1.6
1.0 9.6 1.6
1.0 10.1 1.7
1.0 9.7 1.6
1.0 6.6 1.5
0.5 9.1 1.5
1.0 10.6 1.6
1.0 10.2 1.7
0.5 6.4 1.4
1.0 6.6 1.4
1.0 10.4 1.7
1.0 10.4 1.7
1.0 6.2 1.4
1.0 10.9 1.6
1.0 10.9 1.6
1.0 10.9 1.6
1.0 10.9 1.6
1.0 10.4 1.7
1.0 10.0 1.7
1.0 10.1 1.7
1.0 10.7 1.6
1.0 10.5 1.6
1.0 10.7 1.6
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.5 1.6
I
I
I
I Well
Date Day
I
05/17/96 Sunday
05/16/96 Monday
05/19/96 Tuesday
05/20/96 Wednesday
I 05/21/96 Thursday
05/22/96 Friday
05/23/96 Saturday
05/24/96 Sunday
I 05/25/96 Monday
05/26/96 Tuesday
05/27/96 Wednesday
I 05/26/96 Thursday
05/29/96 Friday
05/30/96 Saturday
05/31/96 Sunday
I 06/01/96 Monday
06/02/96 Tuesday
06/03/96 Wednesday
I 06/04/96 Thursday
06/05/96 Friday
06/06/96 Saturday
06/07/96 Sunday
I 06/06/96 Monday
06/09/96 Tuesday
06/10/96 Wednesday
I
06/11/96 Thursday
06/12/96 Friday
06/13/96 Saturday
06/14/98 Sunday
I 06/15/96 Monday
06/16/96 Tuesday
06/17/96 Wednesday
I
06/16/96 Thursday
06/19/96 Friday
06/20/96 Saturday
06/21/96 Sunday
I 06/22/98 Monday
06/23/96 Tuesday
06/24/96 Wednesday
I
06/25/96 Thursday
06/26/96 Friday
06/27/96 Saturday
06/26/96 Sunday
I 06/29/96 Monday
06/30/96 Tuesday
Average•
EX-05
1.6
2.0
2.0
2.0
2.0
2.0
2.0
2.0
1.9
2.0
0.5
1.5
2.0
1.0
0.9
1.0
1.0
1.0
2.0
2.0
2.0
1.5
1.2
1.5
1.5
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
1.9
1.5
1.7
1.6
Table 3-11
Pumping Rates -Second Quarter 1996
Trench Area Extraction Wells
National Starch and Chemical Company
Salisbury, North Carolina
Actual Pumping Rate (gpm)
EX-06 EX-07 EX-06 EX-09
1.0 1.0 2.0 3.4
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.4
1.0 1.0 2.1 4.0
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.0 2.0 3.5
1.0 1.5 2.0 3.0
1.0 1.5 2.0 2.6
0.4 hi 1.2 3.0
MAINTENANCE
1.5 0.6 1.5 2.7
1.5 1.0 1.6 3.5
1.0 1.0 1.6 3.0
1.0 1.0 1.3 3.0
1.0 1.0 1.5 3.0
0.4 1.0 1.5 3.0
0.4 1.0 1.0 3.0
1.0 1.0 1.2 2.6
1.0 1.0 1.6 3.0
1.0 1.0 1.5 3.0
1.0 1.0 1.2 2.6
1.0 1.0 1.2 2.6
1.0 1.0 1.5 3.0
MAINTENANCE
1.0 1.0 1.5 3.0
1.0 1.0 1.8 3.0
1.0 1.0 2.0 3.2
1.0 1.0 2.0 3.0
1.0 1.0 1.6 3.0
1.0 1.0 1.6 3.0
1.0 1.0 2.0 4.0
1.0 1.0 2.0 3.0
1.0 1.0 2.0 3.5
1.0 1.0 1.8 3.0
1.0 1.0 1.6 3.0
1.0 1.0 1.6 3.0
1.0 1.0 1.6 3.0
1.0 1.0 1.6 3.0
1.0 1.0 1.7 3.0
1.0 1.0 1.5 3.0
1.0 1.0 1.5 3.0
1.0 1.0 1.5 3.0
1.1 1.0 1.6 3.2
I • Averages calculated not including time down for maintenance
lsERs1KRw.050551PuMP2096.ws2
Page 2 of 2
EX-10 Combined Daily Ave.
1.0 10.2 1.7
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.4 1.7
1.0 11.1 1.9
1.0 10.5 1.6
1.0 10.5 1.6
1.0 10.5 1.6·
1.0 10.4 1.7
1.0 10.3 1.7
1.0 7.1 1.2
0.6 6.6 1.5
1.0 10.6 1.6
1.0 6.6 1.5
1.0 6.2 1.4
1.0 6.5 1.4
1.0 7.9 1.3
1.0 7.4 1.2
1.0 9.0 1.5
1.0 9.6 1.6
1.0 9.5 1.6
1.0 6.5 1.4
1.0 6.2 1.4
1.0 9.0 1.5
0.0 0.0
1.0 9.0 1.5
1.0 9.6 1.6
1.0 10.2 1.7
1.0 10.0 1.7
1.0 9.6 1.6
1.0 9.6 1.6
1.0 11.0 1.6
1.0 10.0 1.7
1.0 10.5 1.6
1.0 9.6 1.6
1.0 9.6 1.6
1.0 9.6 1.6
1.0 9.6 1.6
1.0 9.6 1.6
1.0 9.7 1.6.
1.0 9.4 1.6
1.0 9.0 1.5
1.0 9.2 1.5
1.0 9.9 1.7
E
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Figures
BLASLAND, BOUCK & LEE, INC.
engineers & scientists
I ..
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Figures
BLASLAND. BOUCK & LEE. INC.
engineers & sc/enflsts
, .
REFERENCE: Base Map Source. USGS 7.5 Min. Topo. Quad., China Grove, N.C. 1969 and Rowan Mills, N.C.,1970.
200a o 200a
Approximate Scale: 1" = 2000'
■
AREA LOCATION
NATIONAL STARCH ANO CHEMICAL COMPANY
CEDAR SPRINGS ROAD PLANT
SALISBURY, NORTH CAROLINA
SITE LOCATION MAP
BBL BlASLN-JO. BOUCK & LEE, INC. e--;,g-,.,eorJ ,t sc/o·n.,.-,-j·;;--,
FIGURE
1-1
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\
\
\
\
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/
\
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/
LEGEND
e MONITORING Vv£LL LOCATION
♦ EXTRACTION WELL LOCATION
SOURCES: FOR NATIONAL STARCH
_ MAP ENTln.ED ·s11E MAf' /vRf~tflr?A rlONAL TECHNOLOGY AND CHEMICAL COMPALNLE TENN DATED 5/18/93. CORPORATION, KNOXVl • .,
SCHULENBERGER SURVE~NG MONITORING WEUSLLBUSRUYRVENI 8bATED 1/21/97 COMPANY, SA • · .,
-MONITORING ~}rf8R¥_7Jg8Y TAYLOR 'MJSMAN & TAYLOR, RALEIGH N.C.,
SCALE IN FEET
S ND CHEMICAL COMPANY
/// /iL--N-A-TIO_N_AJL~S~TA~R~CQl!HA~S~A~Ll~SB~U~R~YN_O_R-TH-CA_R_O_LI-NAl / CEDAR SPRINGS ROAD PLANT, B OU 1 AND OU2
SECOND iut:l~~~1~J 9 REPORT
WELL LOCATION MAP
BBL BLASLAND, BOUCK & LEE, _INC. I
engineers & sc,ent1sts
FIGURE
1-2
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LEGEND
e MONITORING WELL LOCATION
♦ EXTRACTION WELL LOCA TlON
(651.40) GROUND-WATER ELEVATION
SOURCES:
-~~b §~rJr-JfL .. eb1xp~~r tlfi1t11fJ'A~g~A~Att°cii~cJt~CH
CORPORATION, KNOXVILLE, TENN., DATED 5/18/93.
\ \ \ I
I
MONITORING WELL SURVEY BY SCHULENBERGER SURVEYING COMPANY, SALISBURY. N.C., DATED 1/21/97
I I
\ \
\
\
-MONITORING WELL SURVEY BY TAYLOR WEISMAN & TAYLOR, RALEIGH N.C .. DATED J/98
,oo' <00'
SCALE IN FEET
NATIONAL STARCH AND CHEMICAL COMPANY
CEDAR SPRINGS ROAD PLANT, SALISBURY, NORTH CAROLINA
SECOND QUARTER 1998 OU1 AND OU2
MONITORING REPORT
GROUND-WATER ELEVATION MAP
SECOND QUARTER 1998
) BBL BlASLAND, BOUCK & LEE, INC, I
engineers & scientists
FIGURE
3-1
----~~~~~~~~~------Figure 3-2
Individual Pumping Rates -2Q98
Plume Periphery Extraction Wells
I -•-EX-01 -v------EX-02 -•-EX-03 -.t.-· EX-04
!!!!!I l!!!!!!I l!!!!I !!!!!I !!I!!! i== == i::;:;a liiiiiiil liiiiilil iiii liiiiii liiili iiii iiii iiiil iiil iiiii iliil
70 -----1--1-----f--E 0.
9
2
Figure 3-3
Daily Total Pumping Rates -2Q98
Plume Periphery Extraction Wells
-

-

-
--l+l-l-l-1-l--1--l--

-
,I,
-1+--l-l->--t-l+-H-1-.Hil+-l-l+-l--l---
~ --l-l-++-1--1--1+-l-l+I--
----1-1----I----
_LJ..l._J_LI_
ro Cl'. 60 -

-
----------------
Ol
C ·o.
E :::,
-1--+-l-l-+-l-++-l-l-l---1+-W--++W_jl-l-J-l+LU.H-I-H+f-H-++++l+-1-l-l-1-\.-I---I--W-1..U-1--1--1--1-UI t--rf-H-Ht~+t+l-t-1-1-1--H-++H~'-H-\-\.-l..jj
a. 50 -tt-i+f-H+t+i+t-H-'l+l++-t+++-H-IH--l+~-l--l-+--l--l-l--1-l--l--l--l--1-1-W-W-l-l--l-UJJ.W-IJJJJJ -H-f+l--l+-+-H-1-1-1+++++~-I--+---

-

-
I 40 -tr+-H--t++rH4,-l-l+H··t-tHiit·H--Hiit-H--l-t-t7t-H--H--t+l-t+-l+l-l++l--l+l---l+-l+l+l---l+-1+1---lrl--t--l---l--l---W--1---t--l---l--l---1--l--l--1../..WJ_L
•
30 -I ■ ■■■ 1'.( •
I 04/01 98 04/07 98 04/13/98 04/19/98 04/25/98 05 01 98 05 07 98 05 13 98 05/19 98 05/25 98 05/31 98 06/06/98 06/12 98 06/18 98 06 24 98 06 30/98 Date
-------------------Figure 3-4
Individual Pumping Rates -2Q98
Trench Area Extraction Wells
:_ -. ------I-re ·•-/
1--

-
--1F-i••+-1-t-+-l+l--H-++·l+l--H-+++-J-..l-+-l-l+W-W ♦+-1-H-t-'I--H-++l-i+++-l-l..\+.\-.\--(-j,+..\..W..l--W-I--JJ I .. ;
i
O I -' I 04/01/98 04/07 98 04/13 98 04/19 98 04/25 98 05/01 98, I 5/07 98 05/13 98 5/19 98 05/25 98 05/31 98 06/06 98 06/12 9o 6/18 9$, I 6/24 98 Date
[-•-EX-05 -•-EX-06 --•-EX-07 -•--EX-08 --e--EX-09 ~v·--EX-10 I _______ , __________________ __._
l!!!!!!!!I - - - - - - - - - - - - - - - - - -
12
11
E
(l_ 10 .3
Q)
'" a:::
Ol C ·o. E 9
:::,
0..
8
7
04
Iii I : ■
!
l
Figure 3-5
Daily Total Pumping Rates -2Q98
Trench Area Extraction Wells
I _J_ I_,_ I I II ;. -++-L
1T f ... ---------.. -----
' ·, I -:11 • 1:~ •Ell
I 'i I 1 I •ii\ 1y,\ I II 1, \
I ,o
,JI
\ n I ■ I \/ ~,.
D \ I ■ ~ I,,■
I " ---7' ~l I I ■■-,~ I i "_\ ---------' .. ---
\------- ------~ ---'
i I I I ! -I i,
'
'■ 1, I I ,i, I I.
/ ■ . ---------■----+--+--f --- - - --~ I
I,/ ,.
--~--------- --.
I
C
1) Ii
''\ 1,, Iii,
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Date
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06/18 98 06/24/ 98
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BLASLAND, BOUCK & LEE. INC.
engineers & scientists
lA
VOLATILE ORGA.J.~!CS A.J.~ALYSIS DATA SHEET
EPA SA.J."!PLE NO.
DUPLIC."'-TE
PACE ANALYTIC.ll.L SERVICES Contract:
fide: P.Z\.CE Case No.: SAS No.: SDG No.: 108085
r~: (soil/water)
wt/vol:
(low/med)
otture: not dee.
WATER
5.000 (g/mL) ML
LOW
Column: DB-624 ID: 0.32 (mm)
Lab Sample ID: 10696474
Lab File ID: 1831701017
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 10.0
Soil Aliquot Volume: 111=:xtract Volume: ____ (uL) ----
D
D
I
I
CAS NO. COMPOu-m)
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-35-4---------1,l-Dichloroechene
75-09-2---------Methvlene Chloride
75-34-3---------1,1-bichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Tricnloroechane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2-----~--l,2-Dichloroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100~4·1-4--

-
~ -

-

-
-Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l 3-Dichloroorooene --, --
1330-20~7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disu1.riae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(TotaI) --
Q
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100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
190
100 u
240
100 u
190
100 u
100 u
100 u
-·· 10 o· ·u
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100 u
100 u
100 u
100 u
45 J
6000 E
44 J
100 u
32 J
100 u
100 u
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FOR."! I VOA OLM03.0
100018
I lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
DUPLICATE
PACE ANALYTICAL SERVICES Contract: ,1Code: PACE Case No.: SAS No.: SDG No.: 108086
, __ ix: (soil/wate:::)
,rrlle wt/vol:
,vel: (low/med)
1Jisture: not dee.
WATER
5.000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm)
,i(I Sxtract Volume: ____ (uL)
ifer TICs roun d : 6
CAS NUMBER COMPOUND N_ll_ME
Lab Sample ID: 10696474
Lab File ID: 1831701017
Date Received: 05/22/98
Date .Z\nalyzed: 07/02/98
Dilution Facto:::: 10.0
Soil Aliquot Volume: ----
CONCSNTRATION UNITS:
ug L or ug·L ug ( I I l / L
RT EST. CONC. n ~
,=u============= ----------------------------======== -------------===== . 115-07-1 PROPENE 4.71 690 NJB
2. 105-98-9 1-BUTENE 5.39 110 NJ
0: 75-18-3 DIMETHYL SULFIDE 7.80 500 NJ
75-65-0 2 -PROPP,NOL, 2-METHYL-8.38 76 NJ
75-33-2 2-PROPANETHIOL 8.61 390 NJ
6. 557-40-4 1-PROPSNE, 3,3'-OXYBIS-12.10 280 NJ
': 10.
lm-1 .
13.
tl
17. 1,. l . -
2 .
21. ~· 24. ~-2' .
28. ~,
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FORM I VOA-TIC OLM03.0
I lA EP.l\. SJ:. ... "!PLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
PACE ANALYTICAL SERVICES
:Jfode: PACE
:::cix: (soil/water)
7\fe wt/vol:
·,el: (low/med) :1f sture: not dee.
Column: DB-624
Case No.:
WATER
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
EX·0l
Contract:
SAS No.: SDG No.: 108086
Lab Sample ID: 10696441
Lab File ID: 1780701007
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
ii Extract Volume : ____ (uL) Soil Aliquot Volume: ----
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
n
I
0
D
n
u
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,l-Trichloroechane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2-----~--l,2-Dichloroechane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroecnane
127-18-4--------Tetrachloroethene
124-48-~--------Dibrornochloromethane
10 8 -90~.7➔~-- --:-•• =--. -.. -Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-2a:7-------Xylene (Total)
67-64~1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
Q
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10 u
10 u
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10 u
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10 u
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10 u
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FORM I VOA OLM03.0 .
lE I VOLATILE ORG.O,.NICS ?~~ALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
olName: PACE ANALYTICAL SERVICES
0111 Coc.e: Pi\CE
Jlix: (soil/wate:::-)
wt/vol:
(low/mec.)
11isture: not c.ec.
Case No.:
WATSR
5.000 (g/mL) ML
LOW
: ~olumn: DB-624 ID: 0.32 (mm)
Extract Volume: ____ (uL)
EX-01 Contract:
SAS No.: SDG No.: 108086
Lab Sample ID: 10696441
Lab File ID:
Date Receivec.:
1780701007
06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----
er TICs found: 2
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CU.NC. =1t============ :::::::::::;:::===== ============== ¥. 115-07-1
UNKNOWN
PROPENE 4.42
4.75
3. _______ ---------------------fl----------------------------
6. _______ ---------------------
~----------------------------~o. ______ _ ~,, __
:I'----------------------------. 7. _______ ----------------
92
13
Q
====:::
JB
NJB
-'--------------------------------------
l. _______ ----------------------------~· 4. ______ _
~I :.._ _____ _
3. ______ _
s1
FORM I VOA-TIC OLM03.0
I
(uL
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I ao Name: PACE ANALYTIC.ll.L SERVICES Contract:
EX-02
al Code: PACE
atrix: ( soil/water)
Case No. : SAS No.: SDG No.: 108086
WATER Lab Sample ID: 10696458
alle wt/vol: 5.000 (g/mL) ML Lab File ID: 1831601016
evel: (low/med) LOW Date Received: 06/22/98
listure: not dee. Date Analyzed: 07/02/98
::mfolumn: DB-624 ID: 0.32 (mm) Dilution Factor: 25.0
:ii Sxtract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
m
u
a
g
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2-----~--l,2-Dicnloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5--------cl,l,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124-48~1~-~~~~--Dibromochloromethane
108-90-7-------·-Chlorobenzens
100-41-4--------Ethvlbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-Ql-5------cis-1,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64°1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disul:r:ia:e
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
250
250
250
250
250
250
250
250
250
250
250
410
250
170
250
130
250
250
250
~-~ ~::::•..J
250
250
250
250
250
250
0
3800
62
250
250
250
250
----
Q
u u u u u u u u u u u
u
J u
J
u u u u u u
u u u u
J
J u u
u u
(uL
FORM I VOA OLM03·. 0
D 100061
I lE
VOLATILE ORGANICS P.NP.LYSIS DATA SHEET
COMPOUNDS
EPA S;'-.l~PLE NO.
EX-02 J TENTATIVELY IDENTIFIED
: Name: PACE AJ.'JALYTICAL SERVICES Core.tract:
1code: ?.~CE
•t:::-:!.x: (so:!.l/water) -tle wt/vol:
vol· (low/med)
tistu::-e: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm)
s;..s No.: SDG No.: 108085
Lab Sample ID: 10696458
Lab File ID: 1831601016
Date Received: 06/22/98
Date ;._~alyzed: 07/02/98
Dilution Factor: 25.0 -I Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
··er TI Cs found: 3
COMPOl,'ND NA.Mt
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST.
'
CONC. Q fS NUMBER ============ ======--======------======== ======== -------------=====
2.
I:
i:
9.
tt: 1 .
13.
t': l . 1: .
20.
2,. 2 .
2 .
24.
2 •. 2 .
27.
2,. 2 .
3 .
I·
I
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115-07-1 PROPENE
75-08-1 ETH.llliETHIOL
557-40-4 1-PROPENE,
4.72 600 NJB
7.80 700 NJ
3,3'-OXYBIS-12.11 250 NJ
... . . I
FORM I VOA-TIC OLM03.0
100()62
I L\
VOLATILE ORGANICS ll~~ALYSIS DATA SHEET
EPA Sll .. M?LE NO.
EX-02DL
?ACE ANALYTICAL SERVICES Cont:!:"act:
")Code: ?ACE
l~_ix: (scil/wate:::)
Case No.: Sll.S No.: SDG No.: 108086
-,_°Ille
::Jl1:
wt/vol:
(low/med)
WATE:R
5.000
LOW
(g/mL) ML
Lab Sample ID: 10696458DL
Lab File ID:
Date Received:
1830801008
06/22/98
1istu:::e: not dee. Date A.,alyzed: 07/02/98
Dilution Factor: 200.0 : Column: DB-624 ID: 0.32 (mm)
iij) Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
D
u
D
I
.1
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug./Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroethene
75-09~2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Tricnloroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------l,2-Dicn1oroetnane
79-01-6---------Trichloroethene
78-87-5---------1 2-Dichloroorooane ' .. . 75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chloi=otenzene -
100-41-4--------Ethylbenzene -··---I 100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64~1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Ca:::bon Disulricte
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Total) --
FORM I VOA
Q
2000 1J
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
380 DJ
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
4800 D
2000 u
2000 u
2000 u
2000 u
2000 u
OLM03.0
I lE
VOLATILE ORGANICS ANALYSIS
TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
EPA SP.~'IP!.E NO.
EX-02D!. ,J Name: PACE ANALYTICAL SERVICES Contract:
·1· Code: ?_".CE Case No. :
'-lX: (soil/water) WATER
111e wt/-.,ol:
,vel: (low/med)
1Jisture: not dee.
5.000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm)
SAS No.: SDG No.: 108085
Lab Sample ID: 10696458DL
Lab File ID: 1830801008
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 200.0 ti Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
er TICs found: 1 (ug/L or ug/L) ug/L
1AS NUMBER COMPOUND NAME RT EST. CONC. Q ;;;;:;;;:=========:;;;= ==:;;;:================:;;;:======== ======== -------------===== . 115-07-1 PROPENE 4.73 2900 NJBD
2.
I:
6 .
I:
ti:
13.
tl
17. -·----··· ..... ,,. . .. ,' •· ··--~ ~, I
11
24.
i-.
rn. !I
FORM I VOA-TIC OLM03.0
I
I lA EPA SAMPLc NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03
PACE ANALYTICAL SERVICES Contract:
:Jn=oC.e: Pll.CE Case No.: SAS No.: SDG No.: 108086
::cix: ( soil/wate:c)
:nf_e wt/vol:
vel: (low/med)
~1-stu:ce: not dee.
WAT:SR
5.000 (g/mL) ML
LOW
Lab
Lab
Date
Date
Sample ID: 10696466
File ID: 1833501035
Received: 06/22/98
Analyzed: 07/03/98
Column: DB-624 ID: 0.32 (mm) Dilution Factor: 10.0
ii Ext:cact Volume : ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I ,,
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chlo~omethaue
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3··--------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2-----C--l,2-Dichioroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnioroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane .. •-He• .-... . ····-
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-20~7-------Xylene (Total)
67-64~1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disul:ciae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Total) --
FORM I VOA
100
100
100
100
100
100
100
100
100
100
100
190
100
230
100
180
100
100
100
.100 . 0
100
100
100
100
100
22
4700
36
100
28
100
100
____ (uL
Q
u u u u u u u u u u u
u
u
u u
u u
J u u u u
u
J
EB
J u
J u
u
OLM03.0
1.0.CCSS
l:S I VOLATILE ORGANICS .:i.NALYSIS DATA SHEET
TENTATIV2LY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
PACE Ai.\JALYTICAL SERVICES Contract: EX-03
'). Coc.e: P.~.CE Case No.: SAS No.: SDG No.: 108086
ix• (soi 1 /w-"'":::,...-} ' -• --C. ~ --
'.]le
' l:
we/vol:
(low/mec.}
1isture: not dee .
WATER
5.000
LOW
(g/mL} ML
. Column: DB-624 ID: 0.32 (mm}
im Extract Volume: ____ (uL}
Lab Sample ID: 10696465
Lab File ID:
Date Receivec.:
1833501035
05/22/98
Date ~~,alyzed: 07/03/98
Dilution Factor: 10.0
Soil Aliquot Volume: ----
TICs found: CONCENTRATION UNITS: u er 7 (ug/L or ug/L} ug/L
c.r..s NTJMBER COMPOUND NAME RT EST. CONC. Q =,-=========== ========-====-============== :;:;;;::;:;:;:;:::;::;:;;;:::::: ====:;;====-=== ===== 115-07-1 PROPENE 4.75 700 NJB . 115-11-7 1-PROPENE, 2-METHYL-5.43 98 NJ I 57-54-1 ACETONE 7.54 780 NJ 75-18-3 DIMETHYL SULFIDE 7.83 470 NJ 75-55-0 2 -PROP Ai.\JOL, 2-METHYL-8.40 60 NJ 6. 75-33-2 2-PROPANETHIOL 8.64 270 NJ -557-40-4 i-PROPENE, 3,3'-OXYBIS~ 12.13 250 NJ
cO. cl c3.
<1 -:I
'7. ----·4·•···· ,.
: ~--I . -.. -
I 11. :1
4.
~ • . 7.
8. ~.
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I FORM I VOA-TIC OLM03.0
I 10CC-ki
(UL
I Ll\. VOLATILE ORGAnrcs ~.N"~.LYSIS DATA SHEET
EPA SAMPLE NO.
Jlame: PACS AnALYTICAL SERVICES Contract:
EX-03DL
"l·e
I , •
wt/vol:
(low/med)
Case No.:
WATER
5 . 0 0 0 ( g / :nL) ML
LOW
SAS No.: SDG No.: 108086
Lab Sample ID: 10696466DL
Lab File ID:
Date Received:
1830901009
06/22/98
11sture: not dee.
Column: DB-624 ID: 0.32 (mm)
Date Analyzed: 07/02/98
Dilution Factor: 100.0
~,Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
,
1
_c_A_s_N_o_. _____ c_oM_Po_UN_m ______ (u_g_l_L_o_r_u_g~/-K_g_l_u_G_I_L __ _,. __ a_·_
74-87-3---------Chloromethane 1ooolu
I 75-01-4---------Vinyl Chlorid-e~~~~~~~~~~~~~~= 1000 U
I
I
I
I
I
I
I
I
I·
I
I
74-83-9---------Bromomethane 1000 U 75-00-3---------Chloroethane_________ 1000 U
75-35-4---------1,i-Dichloroetnene 1000 U 75-09-2---------Methylene Chloride______ 1000 U
75-34-3---------1,l-Dichloroethane______ 1000 U
67-66-3---------Chloroform 1000 U 71-55-6---------i,l,l-Tric-h~l-o_r_o_e_t_n_a_n_e_____ 1000 U
56-23-5---------Carbon Tetrachloride 1000 U ----71-43-2---------Benzene___________ 1000 U
107-06-2--------l,2-Dicn1oroetnane 180 DJ
79-01-6---------Trichloroethene -----1000 U
78-87-5---------1,2-Dichloropropane 240 DJ 75-27-4---------Bromodichloromethan_e____ 1000 U
108-88-3--------Toluene 240 DJ 79-00-5---------1,1,2-T_r_i_c~n~l-o_r_o_e_t ___ n_a_n_e____ 1000 U
127-18-4--------Tetrachloroethene 1000 U 124-48-1--------Dibromochlorometh_a_n_e_____ 1000 U
108-90-7--------Chlorobenzene ·-1000 U --------100 -4 l -4 - - - - - - -0 Ethyl benzene_________ 1000 U
1 "'0 42 5 Styrene ., "''"'"' U ~u - ---------
75-25-2---------Bromoform
79-34"5---------1,1,2,2-Tetracnloroetnane
10061-02-6------trans-l 3-Dichloroorooene--' . . 10061-01-5------cis-l 3-Dichloroorooene --' . . 1330-20~7-------Xylene (Total)
67-64.1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulr:iae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Total) --
FORM I VOA
.J..VVV
1000
1000
1000
1000
1000
7200
1000
740
1000
1000
1000
u u u u
u
D u
DJ u u u
OLM03. 0 .
lE I
,I Name:
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAl'1?LE NO.
?ACE .il.i~.il.LYTICAL SERVICES Contract: EX-03DL ,1Code: PACE Case No.: SAS No.: SDG No.: 108086
, __ ix: (soil/water) WATER
wt/vol:
(low/med)
1isture: not dee.
5.000 (c/mL) ML
LOW
. Column: DB-624 ID: 0.32 (mm) t Extract Volume: ____ (uL)
Lab Sample ID: 10696466DL
Lab File ID: 1830901009
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 100.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS:
" er TICs found: 2 (ug I L
C.l\S NUMBER
=t============
. 115-07-1
2.
I:
6.
' ~o. ~D
'.3 .
" ~I
~ 7. ~-:1. '.I
.4.
I
. 8.
I
I
I
75-18-3
----~·--
..
COMPOUND N.il.i"!E
============================ PROPENE
DIMETHYL SULFIDE
-..
FORM I VOA-TIC
or ug/L) ua/L
~T EST. CONC. Q ==:;;::===== -==--======== ===== 4.72 2000 NJBD 7.82 530 NJD
I I
OLM03.0
:tGO-J 07
(uL
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SP..,'1PLE NO.
EX-04
?ACE P...c\/ALYTIC.".L SC:RVICES Contract:
']'Code: ?."-.CE Case No.: SAS No,: SDG No.: 108086
:.t_ ix: ( soil/wate~) WATER Lab Sample ID: 10696482
Lab File ID: 1782701027 '1le wt/vol:
,vel: (low/med)
1isture: not dee.
5. 000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 06/28/98
Dilution Factor: 1.0 ,ii ·-
I
I
I
Extract Volume: (uL) Soil Aliquot Volume: ----
CP..S NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chlorumethan~
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Tricnloroethane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicnloroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroecnane
127-18-4--------Tetrachloroethene
... 124c48:l-~---.---Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4-------~Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l 3-Dichloroorooene --' . . 1330-20-7-------Xylene (Total)
67-64•1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(TotaI) --
10
10
10
2
10
10
10
10
10
10
10
10
10
10
10
11
10
10
10
4
2
10
10
10
10
10
6
7
3
10
2
3
10
----
Q
u u u
J u u u u u u u u u u u
u
u
u
J
J u u
u u u
J
J
J u
J
J
u
(uL
D
E
I
I
I
I
I·
I
I
FORM I VOA OLM03.0
lE I VOLATILE ORGANICS A.J.~ALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
PACE A.J.~ALYTICAL SERVICES
"•e •.-,;:/vol:
1i: (low/med)
1fsture: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
Column: DB-624 ID: 0.32 (mm)
EX-04
Contract:
SAS No.: SDG No.: 108086
Lab Sample ID: 10696482
Lab File ID: 1782701027
Date Received: 06/22/98
Date Analyzed: 06/28/98
Dilution Factor: 1.0
~,Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTR.~TION UNITS:
.l er TICs found: 5 (ug/L or ug/L) ug/L
I
I ,....AS NUMBER COMPOUND NAME RT EST. CONC. Q
=I============ ===-----====--------======== ;;:;:======= -------=====:;;:::: ====:::= UNKNOWN 4.41 130 JB
2. 115-07-1 PROPENE 4.75 140 NJB
I 115-11-7 1-PROPENE, 2-MET!ITL-5.44 40 NJ
75-65-0 2-PROPANOL, 2-METHYL-8.40 40 NJ
107-13-1 2-PROPENENITRILE 8.68 6 NJ
r 0 • ,.
-0 . :I ·_3 . ~-. 7. :I I -I
! 0.
]1
~4 .
jQ ..
!8. ·1
FORM I VOA-TIC OLM03. 0
g
1001:0
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
3.1 Nanie: PACE ANALYTICAL SERVICES Contract: EX-OS
c11· Code: P.Z\.CE
=---ix: ( soil/water)
we/vol:
(low/med)
Case No.:
WAT:C::R
5.000 (g/mL) ML
LOW
SAS No.: SDG No.: 108086
Lab Sample ID: 10696383
Lab File ID: 1832501025
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 500.0
fisture: not dee.
~ Column: DB-624 ID: 0.32 (mm)
Ext:ract Volume: ____ (uL)
C.?i.S NO. COMPOUND
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
----
Q I
I
I
I
I
I
I
I
I
74-87-3---------Chloromethane sooo 1u 75-01-4---------Vinyl Chloride 5000 u 74-83-9---------Bromomethane 5000 u
75-00-3---------Chloroethane 5000 u
75-35-4---------1,1-Dichloroet:hene 5000 u 75-09-2---------Methylene Chloride 5000 u
75-34-3---------1,1-Dichloroethane 5000 u
67-66-3---------Chloroform 5000 u
71-55-6---------1,1,1-Tricnloroecnane 5000 u
56-23-5---------Carbon Tetrachloride 5000 u
71-43-2---------Benzene 5000 u
107-06-2----~---l,2-Dichloroecnane 220000 E
79-01-6---------Trichloroethene 5000 u
78-87-5---------1,2-Dichloropropane 5000 u
75-27-4---------Bromodichloromethane 5000 u
108-88-3--------Toluene 14000
79-00-5---------1,1,2-Tricnloroecnane 5000 u
127-18-4--------Tetrachloroethene 5000 u
124-48-1--------Dibromochloromethane 5000 u 10 8 - 9 0 - 7 - - -_· _:-::·-:. -thlorobenzeii.e 5000 u ' ... ,...,.. ~~ 4 . ....,I-, l' --·---5000 u I ~uu-~~---------t~ny oenzene
100-42-5--------Styrene 5000 u
75-25-2---------Bromoform 5000 u
79-34-5---------1,1,2,2-Tetracnloroetnane 5000 u
10061-02-6------trans-l,3-Dichloropropene--5000 u
10061-01-5------cis-l 3-Dichloroorooene --5000 u ' -. 1330-20.-7-------Xylene (Total) 5000 u
67-64-1---------Acetone 17000 B
78-93-3---------2-Butanone 5000 u
75-15-0---------Carbon Disulriae 5000 u
108-10-1--------4-Methyl-2-Pentanone 2900 J
591-78-6--------2-Hexanone 5000 u
540-59-0--------1,2-Dichloroethene(Total) 5000 u --
(uL
u
D
FORM I VOA OLM03.0
100153
I lE VOLATILE ORGANICS ANF..LYSIS
TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
EPA SA.i"!PLE NO.
,JName: PACE F~~ALYTICAL SERVICES Contract:
EX-05
·r:acode: P.<l.CE
,~ix: (soil/water)
Case No.: SAS No.: SDG No.: 108086
11e
:vel:
wt/vol:
(low/med)
1isture: not dee.
WF.TER
5.000 (g/mL) ML
LOW
'Column: DB-624 ID: 0.32 (mm) ii Extract Volume: ____ (uL)
Lab Sample ID: 10696383
Lab File ID: 1832501025
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
er TICS found: 4 (ug/L or ug/L)
tl'.\S NUMBER
= ============ 115-07-1
2.
': 6. ,.
tl
13.
ti
7..7.
ti 20.
ii
.24.
lJ
28. ~u
0·
D
67-63-0
107-18-6
557-40-4
.
-----
COMPomm NA.NE RT
---------------------======= ======::=
PROPENE 4.76
ISOPROPYL ALCOEOL 7.78
2-PROPEN-1-OL 9.22
1-PROPENE, 3,3'-OXY3IS-12.12
__ ,,_ --·-..
FORM I VOA-TIC
ug/L
EST. CONC. Q _____ ;;;;:======= ===== 16000 NJB
8700 NJ
3300 NJ
11000 NJ
..
OLM03.0
:1DD1.54
lA _ VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAi"!PLE NO.
EX-05DL Name: PACE ANALYTICAL SERVICES Contract:
Code: ?ACE Case No.:
:a::rix: (soil/wa::e::-) WATSR
SAS No.: SDG No.: 108086
Lab Sample ID: 10696383DL alle wt/0,ol: 5. 000 (g/mL) ML Lab File ID: 1831201012 e~l: (low/med)
liisture: not dee.
LOW
ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 5000.0
:folumn: DB-624
J __ Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL I
I
I
I
I
I
I
I
I
[
11 ,.
D
D
CAS NO. COMPOUND CONCSNTRATION UNITS: (ug/L or ug(Kg) UG/L
74-87-3---------Chloromethane
50000 75-01-4---------Vinvl Chloride--50000 74-83-9---------Bro~omethane
50000 75-00-3---------Chloroethane
50000 75-35-4---------1,1-Dichloroecnene
50000 75-09-2---------Methylene Chloride 50000 75-34-3---------1,l-Dichloroethane
50000 67-66-3---------Chloroform
50000 71-55-6---------1,1,l-Tricnloroecnane
50000 56-23-5---------Carbon Tetrachloride 50000 71-43-2---------Benzene
50000 107-06-2--------1,2-Dichloroecnane
340000 79-01-6------~--Trichloroethene
50000 78-87-5---------1,2-Dichloropropane
50000 75-27-4---------Bromodichloromethane
50000 108-88-3--------Toluene
15000 79-00-5---------1,1,2-Tricnloroecnane
50000 127-18-4--------Tetrachloroethene
50000 124-48-1--------Dibromochloromethane
50000 108-90-7--------Chlorobenzene
50000 100-41-4--------Ethylbenzene_
50000 .... -100-42-5--------Stvrene
---50000 75-25-2---------Bromoform
50000 79-34-5---------1,1,2,2-Tecracnloroethane
50000 10061-02-6------trans-1,3-Dichloropropene--
50000 10061-01-5------cis-1 3-Dichloroorooene --50000 ' --1330-20-7-------Xylene (Total) 50000 67-64-1---------Acetone
43000 78-93-3---------2-Butanone
50000 75-15-o~:---~---Carbon Disulriae 50000 108-10-1--------4-Methyl-2-Pentanone
50000 591-78-6--------2-Hexanone
50000 540-59-0--------1,2-Dichloroethene(TotaIJ
50000 --
FOR.IV) I VOA
Q
u
u u u u u
u u u u u
D u u u
DJ
u
u
u u --u u
u u u u
u
DJ u u
u
u u
OLM03.0
l.E I VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
3.b Na!c'.e :
3.1 Code:
PACE ANALYTICA.L SERVICES
PACE
-•'x· (soil/water)
:.~e-wt/vol:
~'11: (low/med)
l'listure: not dee.
Case No.:
WATSR
5. 000 (g/mL) ML
LOW
~ rlumn: DB-624 ID: 0.32 (mm)
.i Extract Volume: (uL) ----
s;,..s No.:
EX-05DL
SDG No.: 108086
Lab Sample ID: 10696383DL
Lab File ID: 1831201012
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 5000.0
Soil Aliquot Volume: ____ (uL
uler TICs found: 1 CONCENTRATION UNITS: (ug/L or ug/L) ug/L ts NUMBER ::: :;;:::::::::===:;;:===:::-
1. 115-07-1
J.
5 . I 8.
9 ~,
2. ~· ::, .
5 ~· 3
J ;I
l.
::I
:I
I
' I
I
I
.--·
COMPOUND NAME RT EST. .CONC. Q ===:;;:===~--~======-=========== ======== ============= ===== PROPENE 4.72 74000 NJBD
-·
I
FORM I VOA-TIC OLM03.0
10015'.J
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPJ\. Sl> .. MPLE NO.
'llName: P.l\.CE ANALYTICAL SERVICES. Cor,tc-1ct:
EX-06
1b Code: PACE case No. : Sl>.S No. : SDG No.: 108086
,lix: (soil/water) WATER Lab Sample ID: 10695391
wt/vol: 5.000 (g/mL) ML Lab File ID: 1783001030
(low/med) LOW Date Received: 06/22/98
Date Ar1alyzed: 06/28/98 'listure: not dee.
· olumn: DB-624 ID: 0.32 (mm)
Extract Volume: ____ (uL)
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug(Kg) UG/L
74-87-3---------Chloromethane ···-.
75-0l-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------l,l-Dichloroetnene
75-09-2---------Methylene Chloride 75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------l,l,l-Trichloroetnane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2--------1,2-Dicnloroetnane
79-01-6------~--Trichloroethene
78-87-5~--------l,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-lS-4--------Tetrachloroethene
124-48-l--------Dibromochloromethane
108-90-7--------Chlo~obenzene . . . .. ....
100-4l-4--------Ethylbenzene I 100-42-5--------Stvrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
l006l-0l-5------cis-l 3-Dichloroorooene --' .. .. 1330-20-7-------Xylene (Total) 67-64-l•--------Acetone
78-93-3---------2-Butanone
75-l5-0---------Carbon Disulriae 108-l0-l--------4-Methyl-2-Pentanone
591-78-6-.-------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
Q
10 u
2 J
10 u
l2
10 u
l0 u
10 u
l0 u
10 u
l0 u
10 u
390 E
l0 u
l0 u
10 u
75
10 u
10 u
10 u
10 u
0 .J -· .
10 u
10 u
l0 u
l0 u
l0 u
10 u
240 E
5 J
l0 u
9l
l0 u
10 u
(uL
FORM I VOA OLM03.0
n 100178
:LE I VOLATILE ORGANICS ~~~ALYSIS DATA SHEET
TENTATIVELY IDENTI?IED COMPOUNDS
b[Name:
.b ~ode:
PACE ANALYTICAL SERVICES
PACE
~lfx· (soil/wate:::-)
:n~e wt/vol:
.,, : (low/me~)
~oistu:::-e: not cec.
Case No.:
WATER
5. 000 (a/mL) ML
LOW
tlumn: DB-624 ID: 0.32 (mm)
il Ext!"act Volume: (uL) ----
-Contract:
SAS No.:
EX-06
SDG No.: 108086
Lab Sample ID: 10696391
Lab File ID: 17830010.J0
Date Received: 06/22/98
Date Analyzed: 06/28/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL
lie:::-TICS found: 6
CONCENTRATION UNITS:
(ug/L or ug/.L) ug/L
Is NUMBER COMPOUND NAME RT EST. CONC. Q ============---=======================~==== --------====;;;;:;======== :=:==== 1. UNKNOWN 4.42 110 JB I 115-07-1 PROPENE 4.73 560 NJB 115-11-7 1-PROPENE, 2-METHYL-5.45 150 NJ 4. 2313-65-7 2-HEXANOL, 3-METHYL-7.82 8 NJ
I 75-65-0 2-PROPANOL, 2-METh-YL-8.40 33 NJ
557-40-4 1-PROPENE, 3,3'-OXY3IS-12.15 10 NJ
8 .. -.
1·' i .1.
.2. ~· 5 . -~. 8 .
9. ' . •-..• --' --. I
~I I
2.
3. ~· 5.
~g
9.
0. -0
'
'O FORM I VOA-TIC OLM03.0
u :10G1.·..rl
m
1::::
I VOLATILE ORGANICS ,'I_NALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
~ab Name: PACE ANALYTICAL SERVICES ,al Code: P.2\.CS Case No.:
!atrix: (soil/wa~e::?:') WATER alle wt/vol: 5.000 (g/~L) ML .ell: (low/med)
istu~e: not dee.
::ltolumn: DB-624
LOW
ID: 0.32 (mm) J. Extract Volume: {uL) ----
Contract:
S.:'.\.S No.:
EX-06DL
SDG No. : 108086
Lab Sample ID: 1069639lDL
Lab File ID: 1782901029
Date Received: 06/22/98
Date Analyzed: 06/28/95
Dilution Factor: 10.0
Soil Aliquot Volume: ----
i~er TI Cs found: 3 CONCSNTRATION UNITS: {ug/L or ug/L) ug/L ts NUMBER COMPOUND NAME 0"' EST. __ CONC. Q ·-· .::= =====---=---=======-==-==-=-=--========= ======== -==-========= ====== 1. UNKNOWN 4.43 210 JBD l. 115-07-1 PROPENE 4.78 890 NJBD 115-11-7 1-PROPSNE, 2-METHYL-5.46 100 NJD 5. ,.
9. -
ti
~2.
~~ • . 5 .
. 6. ~· I .. .... .. --
'::!.
·-" I ~I
3. ~.
J •
7. ~:I
l .
I
'
I
I :ORM I VOA-TIC OLM03.0
I
I
10.0702
(UL
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE ANALYTICAL SERVICES
Code: PACE
11trix: (soil/water)
simple wt/vol:
I.Jlvel: (low/med)
¾"Moisture: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
C:I Column: DB-624 ID: 0.32 (mm)
Soil Extract Volume: ____ (uL)
Contract:
SAS No.:
EX-06DLB
SDG No.: 108086
Lab Sample ID: 10696391DLB
Lab File ID: 1833601036
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 20.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
____ (uL
Q
-I
I
I
I
··I
I
I
'
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2-------~-Methylene Chloride
75-34-3---~-----l,l-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-TrichLoroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicnloroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-TricnLoroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Ethvlbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l 3-Dichloroprooene--' . 10061-01-5------cis-l 3-Dichloroorooene --, -. 1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene{TotaI) --
FORM I VOA
200 u·
.. -. 200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
550
200 u
200 u
200 u
73 J
200 u
200 u
200 u
200 u
200 u . --.... -200 u ..
200 u -
200 u
200 u
200 u
200 u
430 B
200 u
200 u
95 J
200 u
200 u
OLM03.0
lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Name: PACE ANll.LYTICAL SERVICES
Code : P .l\.CE Case No.:
'l~:::-ix: (soil/wate:::-) WATSR
a. _le wt/vol: 5.000 (g/mL) ML
e[l: (low/med)
1DLStu:::-e: not dee.
LOW
Corrt:::-a-ct: ·
s;..s No.:
Lab
Lab
Date
Date
EX-06DLi3
SDG No.: 108086
Sample ID: 1069539lDLi3
File ID·: 183360:.036
Received: 06/22/98
Analyzed: 07/03/93
:folumn: DB-624 ID: 0.32 (mm) Dilution Factor: 20.0
:,il Extract Volume: (uL) ----Soil Aliquot Volume: ----~Ler TICs found: 1 CONCENTRATION UNITS: (ug/L or ug/L) ug/L
~S NUMBER COMPOu'"ND NAME RT EST. CONC. Q :=============== ·================~=========== ======== ============::: ===== 1. 115-07-1 PROPENE 4.77 1100 NJB I:
4.
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8.
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FORM I VOA-TIC OLM03.0
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(UL
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SA..'1PLE NO.
EX-07 PACE ANALYTICAL SERVICES ,,Name:
~b Code: Case No.:
ifix: (soil/water} WATER
Contract·:
s.:i.s No. : SDG No.: 108086
Lab Sample ID: 10696409
,mple wt/vol: 5.000 (g/mL} ML Lab File ID: 1832401024
.■; . -~-· (low/med}
Moisture: not dee.
LOW
: lolumn: DB-624 ID: 0.32 (mm}
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 10.0 ii Extract Volume: (uL} ----Soil Aliquot Volume: ____ (uL
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg} UG/L Q
74-87-3---------Chloromethane , ,., ,., n J..UU u 75-01-4---------Vinyl Chloride 100 u 74-83-9---------Bromomethane 100 u 75-00-3---------Chloroethane 100 u 75-35-4---------1,1-Dichloroetnene 100 u 75-09-2---------Methylene Chloride 100 u 75-34-3---------1,1-Dichloroethane 100 u 67-66-3---------Chloroform 100 u 71-55-6---------1,1,1-Trichloroetnane 100 u 56-23-5---------Carbon Tetrachloride 100 u 71-43-2---------Benzene 100 u 107-06-2--------1,2-Dichloroethane 100 u 79-01-6---------Trichloroethene 100 u 78-87-5---------1,2-Dichloropropane 100 u 75-27-4---------Bromodichloromethane 100 u 108-88-3--------Toluene 56 J 79-00-5---------1,1,2-Tricnloroetnane 100 u 127-18-4--------Tetrachloroethene 100 u 124-48-1--------Dibromochloromethane 100 u 108-90-7--------Chlorobenzene 100 u ·100-41·-'4 ~" -

-

-

-

-
-Ethylbenzene 100 u 100-42-5---------styrene 100 u 75-25-2---------Bromoform 100 u 79-34-5---------1,1,2,2-Tetrachloroethane 100 u 10061-02-6------trans-1,3-Dichloropropene--100 u 10061-01-5------cis-1 3-Dichloroprooene --100 u , -1330-20-7-------Xylene (Total) 100 u 67-64-1---------Acetone 59 JB 78-93-j~--------2-Butanone 100 u 75-15-0---------Carbon Disulria:e 100 u 108-10-1--------4-Methyl-2-Pentanone 19 J 591-78-6--------2-Hexanone 100 u 540-59-0--------1,2-Dichloroethene(Total) 100 u --
FOR.I<! I VOA OLM03.0
100.??6
lE EPA S~~PL2 NO. I VOLATILE ORGANICS AI,ALYSIS .DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EX-07 e.l Name: P .l\.CE ANALYTICAL SERVICES Contract:
3. Code: PACE Case No.: ,1i·c (soil/water) WATER
;,,_ le wt/vol: 5. 000 (g/mL) ML 'Jl: (low/med)
,oisture: not dee.
LOW
~1olumn: DB-624 ID: 0.32 (mm)
.il Extract Volume: ____ (uL)
SAS No.: SDG No.: 108086
Lab Sample ID: 10696409
Lab File ID: 1832401024
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 10.0
Soil Aliquot Volume: ____ (uL •:1ler TI Cs found: 2 CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
Js NUMBER COMPOUND NAME RT EST. CONC. Q ======-======== =======--===-==-=-========== ======== -=-========== ==:== 1. 115-07-1 PROPENE 4.73 1500 NJB I 115-11-7 1-PROPSNE, 2-METHYL-5.40 52 NJ
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I 100?:Z?
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lA VOLATILE ORGANICS ~.NALYSIS DATA SHEET E?A SAMPLE NO.
EX-07DL Name: PACE ANALYTICAL SERVICES Contract:
I
:I Code: PACE Case No.: SAS No.: SDG No.: 108086
·1rix: (soil/water)
am9le wt/vol:
WATSR Lab Sample ID:
Lab File ID:
10696409DL
1832301023
(low/med)
Moisture: not dee.
25. 00 (g/rrG) ML
LOW
:Jolumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 100.0
Jil
I
I-
I
I
I
I
0
n
Extract Volume: (uL) ----Soil Aliquot Volume: ____ (UL
CAS NO. COMPOUND CONCSNTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4-------.:.:vrnyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride 75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Tricnloroetnane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2-----~--l,2-Dich1oroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------l,l,2-Tr1.cn1oroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromociloromethane
108-90-7--------Chlorobenzene
10 o -41-4 -

-
-----·~-~~-Ethylbenzen-e
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloro9ropene--
10061-01-5------cis-l 3-Dichloroorooene --' --1330-20-7-------Xylene (Total) 67-64-1---------Acetone
78-93~3-:--------2-Butanone
75-15-0---------Carbon Disu1r1.ae 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Total)
--
FORM I VOA
Q
, """ _._,._, UV u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
910 DJB
1000 u
1000 u
1000 u
1000 u
1000 u
OLM03.0 .
1002.':;7
lE I VOLATILE ORGANICS ~~~ALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
"'JName:
a Code:
?ACE ANALYTIC.l;L SERVICES
?ACE Case No.:
Ccint:::act:
SAS No.:
EX-07DL
SDG No.: 108086
Lab Sample ID: 10696409DL
~,ix: (soil/wate:::) WATE~
~mple wt/·,ol: 25. 00 (g/mL) ML Lab File ID: 1832301023
(low/med) LOW
Moisture: not dee.
: .lumn: DB-624 ID: 0.32
il Extract
·.iler TICs
Volume: (uL) ----
found: 1
(mm)
s NUMBER COMPO1:JND NAME
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 100.0
Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS: (ug/L or ug/L) ug/L
·-----, RT EST. ! CONC. Q ====::::=;:;.:=====:;:-= ---------------------------. ========== ============= ===== I 115-07-1 PROPENE 4. 73 2600 NJBD
4. ~,
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FORM I VOA-TIC OLM03.0 I
I 1002~8
I
lA VOLATILE ORGA.11/ICS .Z,..NALYSIS DATA SHEET EPA SAf.!PLE-No.
EX-07DLB ~ab Name: PACE A.J.~ALYTICAL SERVICES Contract: :,f Code: PACE Case No.: SAS No.: SDG No. : 108086
Lab Sample ID: 10696409DLB
•!atrix: (soil/water) WATER
,Jple wt/vol: 5.000 (c/:nL) ML· Lab File ID: 1831101011
~~el: (low/med) LOW Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 1000.0
-loisture: not dee.
;CW.column: DB-624 ID: O .32 (mm)
J1 Extract Volume: (uL) ----Soil Aliquot Volume: ----I
I
I
I
I
I
I
I
H
'
CAS NO. COMPO!.Thu CONCENTRATION UNITS: (ug/L or ug-/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chlorid~e--------74-83-9---------Bromomethan~ · 75-00-3---------Chloroethane ________ _
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride--~--75-34-3---------1,l-Dichloroethane
67-66-3---------Chloroform -----71-55-6---------1,l,l-Tricnloroetnane
56-23-5---------Carbon Tetrachloride----71-43-2---------Benzene 107-06-2--------1,2-Dic_n_i_o_r_o_e_t_h_a_n_e _____ _
79-01-6---------Trichloroethene
78-87-5---------l,2-Dichloropro-p7a~n~e-----75-27-4---------Bromodichloromethane
108-88-3--------Toluene ----79-00-5---------1,l,2-Tricnloroetnane
127-18-4--------Tetrachloroethene ----124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene ----100-41-4-~------Ethylbenzene
~00-42-5--------Styrene . . ... --... -
75-25-2---------Bromoform --· -79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --1330-20-7-------Xylene (Total) 67-64 0 1---------Acetone
78-93-3---------2-Butanone
75-15-O°--------Carbon Disulriae 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total)
--
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
10000 U
8100 J
10000 U
10000 U
10000 U
10000 U
10000 U
Q
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D
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FORM I VOA OLM03.0
100:?45
lE I ·VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SJ'..MPLE NO.
.ab Name: PACE ANALYTICAL SERVICES J Code: PACE
Tix: (soil/water)
;;lile wt/vol: ~11: (low/med)
1.sture: not dee.
:a:olumn: DB-624
Case No.:
WATER
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
J~ Extract Volume: (uL) ----
Contract:
SAS No.:
EX-07DLB
SDG No.: 108086
Lab Sample ID:
Lab File ID:
10696409DLB
1831101011
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 1000.0
Soil Aliquot Volume:. ____ (uL
rLer TI Cs found: 1 CONCENTRATION UNITS:
JAs NUMBER
~---===--=--==--
l.
I:
i:
8 . . ii:
12.
ti l:, .
L6. ti
c9.
lJ.
13. :p
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115-07-1
(ug/L or ug/L) ug/L
COMPOGND NAME RT EST. CONC. Q =======--==-================ ========· =-=========== ===== PROPENE 4. 73 14000 NJB
.,. ' ,, . '
.,,
FORM I VOA-TIC OLM03.0
I . lA . _ ... VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SA.'11PLE NO.
ai Name: PACE ANALYTICAL SERVICES Contract:
EX-08
al Code: PACE Case No.:
·a[ix: ( soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696417
a,_le wt/vol: 5.000 (g/mL) ML Lab File ID: 1831401014 ell: (low/med)
,oisture: not dee.
LOW
::folumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 250.0
· ~il Extract Volume: (uL) Soil Aliquot Volume:
I
I
I
I
I
I
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n
H
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane _______ _
75-01-4---------Vinvl Chloride
74-83-9---------Bromomethane ------'---'-'--
75-00-3---------Chloroethane 75-35-4---------1,l-Dichloro.~e~c-n-e-n_e _____ _
75-09-2---------Methylene Chloride
75-34-3---------1,l-Dichloroethane ____ _
67-66-3---------Chloroform 71-55-6---------l,l,l-Tric~h-l_o_r_o_e_t_h_a_n_e ___ _
56-23-5------~--Carbon Tetrachloride
71-43-2---------Benzene -----
107-06-2----~---l,2-Dichloroethane ____ _
79-01-6---------Trichloroethene ______ _
78-87-5---------1,2-Dichloropropane ____ _
75-27-4---------Bromodichloromethane
108-88-3--------Toluene ----
79-00-5---------1,l,2-Tricnloroethane
127-18-4--------Tetrachloroethene ----
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene ----
100-41-4--------Ethylbenzene ____ _,_ __ ~~
100-42-5--------Styrene
7 5 -2 5-2 - - - - - - - --Eromof o:-:r=m----------
79-34 -5 ---------l, l, 2, 2 -Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-0l-5------cis-l,3-Dichloropropene_===
1330-20-7-------Xylene (Total) ______ _
67-64-1---------Acetone 78-93-3c--------2-Butan_o_n_e _________ _
75-15-0---------Carbon Disulride ______ _
108-10-1--------4-Methyl-2-Pentanone. ____ _
591-78-6--------2-Hexanone 540-59-0--------1,2-Dichlo_r_o_e_t_h_e_n_e_(T_o_t_a_l_) __
2500 U
2500 U
2500 U
2500 U
2500 U
4.20 J
2500 U
2500 U
2500 U
2500 U
2500 U
140000 E
2500 U
2800
2500 U
20000
2500 U
2500 U
2500 U
2500 U
2500IU
2500 U
2500 U
2500 U
2500 U
2500 U
1100 J
56000 E
2500 U
2500 U
13 000
2500 U
2500 U
----
Q
(uL
FORM I VOA OLM03.0
E 100753
I .. lE VOLATILE ORGANICS ANALYSIS TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
EPA Sll .. MPLE N '0.
EX-08 Name: PACE ANALYTICAL SERVICES Contract:
Code: PACE
•!°lirix: (soil/water)
·clple wt/vol: .ell: (low/med)
. 1.sture: not dee.
Case No.:
WATSR
5.000 (g/mL) ML
LOW
SAS No.: SDG No.: 108086
Lab Sample ID: 10696417
Lab File ID: 1831401014
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 250.0
Clolumn: DB-624 ID: 0.32 (mm)
~1.-Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
'11.ibe:c TI Cs found: 6 CONCSNTRATION UNITS: (ug/L or ug/L) ug/L
I I J.l\.S N1JMBER COMPOUND NAME RT EST .. CONC. Q ~ ============-========---=--=-============ ======== -==-========= =====: 1. 115-07-1 PROPENE 4.72 6600 NJB I:
67-63-0 ISOPROPYL ALCOHOL 7.77 4300 NJ 79-20-9 ACETIC ACID, METHYL ESTER 8.12 1800 NJ 107-13-1 2-PROPENENITRILE 8.63 3 700 NJ 5 . 513-37-1 1-PROPENE, l-CHLORO-2-METHYL 10.17 2000 NJ I 557-40-4 1-PROPENE, 3,3'-OXYBIS-12.12 6200 NJ 8. -ti
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I
'.1D0254 I
lA VOLATILE -ORGi'l_l\IICS AI/ALYS IS DATA -SHE-E°T .EPA SAI1PLE NO.
Name: PACE ANALYTICAL SERVlCES
Code: !?ACE Case No.:
:atrix: (soil/water) WATER
ali1e wt/vol: 5.000 (g/mL) ML
evel: (low/med) LOW
Jisture: not dee.
:-=olumn: DB-624 ID: o. 32 (mm) J. Extract Volume: (uL)
Contract:
SAS No.:
EX-08DL
SDG No.: 108086
Lab Sample ID: 10696417DL
Lab File ID: 183060:!.006
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 2500.0
----Soil Aliquot Volume: ----
I
I
I
I
I
I
I
0
0
D
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
25000 75-01-4---------Vinyl Chloride . -----25000 74-83-9---------B:comomethane 25000 75-00-3---------Chloroethane
25000 75-35-4---------1,1-Dichloroetnene 25000 75-09-2---------Methylene Chloride 25000 75-34-3---------1,1-Dichloroethane 25000 67-66-3---------Chloroform 25000 71-55-6---------1,1,1-Trichloroet .. nane 25000 56-23-5---------Carbon Tetrachloride 25000 71-43-2---------Benzene -25000 107-06-2--------1,2-Dicnioroethane 220000 79-01-6---------Trichloroethene 25000 78-87-5---------1,2-Dichloropropane 25000 75-27-4---------Bromodichloromethane 25000
Q
u u u u u u u u u u
u
D u
u
u 108-88-3--------Toluene 23000 DJ 79-00-5---------1,1,2-Tricnloroetnane 25000 u 127-18-4--------Tetrachloroethene 25000 u 124-48-1--------Dibromochloromethane 25000 u 108-90-7--------Chlorobenzene 25000 TJ 100-41-4---~----Ethylbenzene .. _25000 lu. ,,· ·-100-42-5--------St.yrene . ,. ·-. 25000 u 75-25-2---------Bromoform 25000 u 79-34-5---------1,1,2,2-Tetracnloroethane 25000 u 10061-02-6------trans-l,3-Dichloropropene--25000 u 10061-01-5------cis-l,3-Dichloropropene --25000 u 1330-20-7-------Xylene (Total) 25000 u 67-64-1---------Acetone 72000 D 78-93-j---------2-Butanone 25000 u 75-15-0•--------Carbon Disulricte 25000 u 108-10-1--------4-Methyl-2-Pentanone 13000 DJ 591-78-6--------2-Hexanone 25000 u 540-59-0--------1,2-Dichloroethene(Total) 25000 u --
I
----
(uL
FORM I VOA OLM03. 0
100?.7S
I
lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
--EPA-Sfl ... "!?LE NO · .
EX-08DL Lab Name: PACE ANALYTICAL SERVICES Contract: ::,I Code: PACE Case No.: SAS No.:
1atrix: (soil/water) WATER
,lple wt/vol: 5.000 (g/mL) ML
SDG No.: 108086
Lab Sample ID: 10595417DL
Lab File ID: 1830601005
Date Received: 05/22/98
Date Analyzed: 07/02/98
Dilution Factor: 2500.0
~evel: (low/med) LOW
-loisture: not dee.
:cacolumn: DB-624 ID: 0 .32 (mm)
·0'1 Extract Volume: ____ (uL)
~~er TICs found: 1
COMPOUND NAME
Soil Aliquot Volume:
CONCENTRATION UNITS: (ug/L or ug/L) ug/L
RT EST.
----
CONC. _g ___ -
1:s NUMBER
= ===========---=-=---------------=-====== ======== -------------===== -· ·1:-. 115-07-1 PROPENE 4.72 30000 NJBD I:
5 .
I:
9.
1 •. l .
12. ii l .
16. ~B .c::,. -.. -···-·-· ... 20. --. ...
211 -· 2.
23.
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m
1no-:>?h
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lA ___ EPA SAi'1PLE NO. -. VOLATILE ORGANICS-ANALYSIS DATA SHEET
EX-09 ab Name: PACE ANALYTICAL SERVICES Contract:
t Code: PACE Case No.: SAS No.: SDG No.: 108086
atrix: (soil/water) WATER Lab Sample ID: 10696425
2.lle wt/vol: 5.000 (g/mL) ML Lab File ID: 1831001010
evel: (low/med) LOW Date Received: 06/22/98
listure: not dee. Date Analyzed: 07/02/98
:iifolumn: DB-624 ID: 0.32 (mm)
JI_ Extract Volume: (uL)
Dilution Factor: 100.0
----Soil Aliquot Volume: ----I
a
0
E
I
·-•
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane 1000 75-01-4---------Vinyl Chloride 1000 74-83-9---------Bromomethane
1000 75-00-3---------Chloroethane
1000 75-35-4---------1,1-Dichloroethene
1000 75-09-2---------Methylene Chloride 220 75-34-3---------1,1-Dichloroethane 1000 67-66-3---------Chloroform 1000 71-55-6---------1,1,1-Trichloroetnane 1000 56-23-5---------Carbon Tetrachloride 1000 71-43-2---------Benzene 1000 107-06-2-----~--1,2-Dichloroethane 54000 79-01°6---------Trichloroethene 1000 78-87-5---------1,2-Dichloropropane 13000 75-27-4---------Bromodichloromethane 1000 108-88-3--------Toluene 15000 79-00-5---------1,1,2-Tricnloroechane 1000 127-18-4--------Tetrachloroethene 1000 124-48-1--------Dibromochloromethane 1000 108-90-7--------Chlorobenzene 1000 -
Q
u
U-••m-
u u
U.
J u u
u u u
E u
u
u
u u
u 100-41-4--

-

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-

-

-
-Ethylbenzen·e 660_jJ_ ..... 100-42-5--------Sty~ene 1000 U 75-25-2---------Bromoform 1000 u-79c34-5--~------l,1,2,2-Tecrachloroechane 1000 u 10061-02-6------trans-1,3-Dichloropropene--1000 u 10061-01-5------cis-1 3-Dichloroprooene --1000 u , . 1330-20-7-------Xylene (Total) 2300 67-64-1---------Acetone 14000 78-93-3---------2-Butanone 1000 u 75-15-o~--------Carbon Disuiriae 1000 u 108-10-1--------4-Methyl-2-Pentanone 5800 591-78-6--------2-Hexanone 1000 u 540-59-0--------1,2-Dichloroethene(Total) 1000 u --
I
(uL
FORM I VOA OLM03. 0
I
lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE---No _--·· · ···1·•··
:,ab Name: PACE ANALYTICAL SERVICES ~t Code : PACE Case No.:
•!atrix: (soil/water) WATER ,alle w::/vol: 5. 000 (g/mL) ML
,evel: (low/med) LOW
Listure: not dee.
C.folumn: DB-624 ID: 0.32 (mm)
Contract,·
SAS No.:
Lab
Lab
Date
Date
EX-09
SDG No.: 108086
Sample ID: 10696425
File ID: 1831001010
Received: 06/22/98
Analyzed: 07/02/98
Dilution Factor: 100.0 :ii. Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
~•er TICs found: 7 CONCENT!<.ATION UNITS: (ug/L or ug/L) ug/L
IAS NUMBER COMPOUND NAME RT I EST. CONC ... Q I I = =======-==-=-=======----=-=-=-=-========= ======== ===--=-~====== ===== :i.. 115-0'7-l· PROPENE -4.72 2700 NJB
I:
67-63-0 ISOPROPYL ALCOHOL 7.77 2900 NJ 107-13-1 2-PROPENENITRILE 8.63 2100 NJ 563-47-3 1-PROPENE, 3-CHLORO-2-METHYL 10.17 1500 NJ 5. 96-33-3 2-PROPENOIC ACID, METHYL EST 10.25 640 NJ I: 78-83-1 1-PROPANOL, 2-METHYL-11.08 1200 NJ 557-40-4 1-PROPENE, 3,3'-OXYBIS-12.11 10000 NJ
9.
tJ
ti
16.
tfl ! --------'0. ·-··-·--.... -..... ·-· ----no ..
: 3 .
'" :~u
. 7. ~o 0.
m .
m FORM I VOA-TIC OLM03.0
m :1ro::·s7
•
lA
I VOLATILE ORGP.NICS P~~ALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Case No.:
~atrix: (soil/water) WATER
,lple wt/vol: 5.000 (g/mL) ML
.:.,evel: (low/med) LOW
'c loisture: not dee.
,cacolumn: DB-624 ID: O . 3 2 ( mm) ·Ji Extract Volume: ____ (uL)
Contract:
SAS No.:
EX-09DL
SDG No.: 108086
Lab Sample ID: 10696425DL
Lab File ID: 1833301033
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 500.0
Soil Aliquot Volume: ----I
I
I
I
CA.S NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug-/Kg) UG/L Q
0
u
I
I
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride 7<±-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride 75--34 -3 -

-

-

-

-

-

-

-
-1, 1-Dichloroethane 67-66-3---------Chloroform
71~55-6---------1,1,1-Trichloroecnane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2--------l,2-Dicn1oroecnane
79-01-6--~------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroecnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
-100-42-5--~-~---Styrene
75-25-2----~----Bromoform
79-34-5---------1,1,2,2-Tecrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene
--1330-20-7-------Xylene (Total) 67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0~~-------Carbon Disu1riae 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Tocal)
--
5000 u 5000 u 5000 u
5000 u
5000 u 5000 u 5000 u 5000 u
5000 u
5000 u
5000 u
85000 D
5000 u
15000 D
5000 u
18000 D
5000 u 5000 u
5000 u 5000 u
570 DJ
5000 u
5000 u
5000 u 5000 u
5000 u
1500 DJ
14000 DB
5000 u
5000 u
5700 D
5000 u 5000 u
(UL
FORM I VOA OLM03.0
I
lE
I --VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA S~2-!PLE NO.
Name: PA.CE ANALYTICAL SERVICES sJ Code: PA.CE
1atrix: ( soil/water)
,,9le wt/vol:
"'a°el: (low/med)
-lo~sture: not dee.
;cwcolumn: DB-624
Case No.:
WATER
5.000 (g/mL) ML
LOW
ID: 0 .32 (mm)
Contract:
SAS No.:
EX-09DL
SDG No.: 102086
Lab Sample ID: 10696425DL
Lab File ID: 1833301033
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 500.0 ·cl1 Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
~er TICs found: 3 CONCENTRATION UNITS: (ug/L or ug-/L) ug/L
lAS NUMBER COMPOUND NA.ME RT EST. CONC. Q = ========-::::==-======-=-=================== :::======= -===::;:======== ===== 1 . 115-07-1 PROPENE. 4.75 6800 NJBD I: 57-55-6 PROPYLENE GLYCOL 7.79 2800 NJD 557-40-4 1-PROPENE, 3,3'-OXYBIS-12.13 11000 NJD 5. ': 9. I:
12. j:
.
16.
tJ. .
I '
1 (\ ..... ··-. ·-... ll . ..
!3 .
'J
.7.
I 0 . -. .
I .. ·• FORM I VOA-TIC OLM03.0
',·.;.:, . ,._, .... \ ' -~, .. I
100310
I -
lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SP. . .MPLE NO. I
PACE ANALYTICAL SERVICES E:<-10 Contract: =.b Name: ,I code: PACE
1trix: ( soil/water) . Ile wt/vol:
Case No.: SAS No. : SDG No.: 108086
Lab Sample ID: 10696433 .
5.000 (g/mL) ML
LOW
Lab File ID: 1831501015 ,ll: (low/med)
,. isture: not dee.
ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/02/98
·Dilution Factor: 50.0 ·.rlumn: DB-624
i Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4-----.----Vinyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride 75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroetnane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2-----~--1,2-Dich~oroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7-------~Chlorobenzene
100-41-4--------Eth lbenzene 1, y .
I l O O -4 2 -5 ::·:: ..:·::·:.c·:··_:: Styrene
g
D
D
75-25-2---------Bromofo_rm __________ _
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-1,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene_::=
1330-20-7-------Xylene (Total) ______ _ 67-64-1---------Acetone 78-93-3---------2-Butan_o_n_e _________ _
75-15-o-·~-------Carbon Disul:ciae 108-10-1--------4-Methyl-2-Penta_n_o_n_e ____ _ 591-78-6--------2-Hexanone
540-59-0--------1,2-Dichlo_r_o_e_t_h_e_n_e~(T~o-t~a-r-)--
FORM I VOA
500 u
210 J
500 u
500 u
500 u
13 0 J
200 J
500 u
500 u
500 u
500 u
21000 E
500 u
20000 $ 500 u
.7600
500 u
500 u
500 u
500 u
2000
5001u
500 U
500 .u
500 U
500 U
6200
74000 E
500
500 U
110 J
1900
500 U
Q
OLM03.0
l.S
I VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDSNTIFIED COMPOUNDS
EPA SAMPLE NO.
.ab Name: PACE ANALYTICAL SERVICES
al Code: PACE Case No.:
atrix: ( soil/water) WATSR
alle wt/vol: 5.000 (s/m.::.r ML
9vel: (low/med) LOW
listure: not dee.
: !Solumn: DB-624 ID: 0.32 (mm)
Contract:
SAS No.:
EX-10
SDG No.: 108086
Lab Sample ID: 10696433
Lab File ID: 1831501015
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 50.0 ,JI Extract Volume: (uL) ----Soil Aliquot Volume: ____ (UL
ulJoer TICs found: 9 CONCENTRATION UNITS: (ug/L or ug/L) ug/L IS NUMBER COMPOUND NAME RT EST. CONC. I q = =====::====== ---------------------~ --------======== --==-======== ===== 1 115-07-1 PROPENE 4.72 9300 NJB I 67-63-0 ISOPROPYL ALCOHOL 7.76 9200 NJ 79-20-9 ACETIC ACID, METHYL ESTER 8.12 700 NJ 107-13-1 2-PROPENENITRILE 8.62 2000 NJ 5. 107-18-6 2-PROPEN-1-OL 9.21 490 NJ , 96-33-3 2-PROPENOIC ACID, METHYL EST 10.26 260 NJ 78-83-1 1-PROPA.i.'l"OL, 2-METHYL--11.09 640 NJ 557-40-4 1-PROPENE, 3,3'-OXYBIS-12.10 14000 NJ 9. 111-44-4 S-DICHLOROETHYL ETHER 20.37 1100 NJ I 2.
~I
5 . . 7 ~-I .. ·---1. ·-!.
; .
. ,
:1
,1 .
I FORM I VOA-TIC OLM03.0
I
:t 00.:27 I
I
lA EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
,b Name: PACE ANALYTICAL SERVICES
,_4code: P.l\CE Case No.:
,trix: ( soil/water) WATER
,nllewt/vol: 5.000 (g/mL) ML
,vel: (low/med) LOW
~sture: not dee.
rlumn: DB-624 ID: 0.32 (mm)
i Extract Volume: (uL) ----
Contract:
SAS No.:
EX-l0DL
SDG No.: 108086
Lab Sample ID: 10696433DL
Lab File ID: i830701O07
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 500.0
Soil Aliquot Volume: ----I CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
D
D
I
m
I
I
I
I -•
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride 75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroecnane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2--------1,2-Dicn~oroecnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroecnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Echylbenzene
1.00-42-5--------Sty:::-ene----···-· -..
75-25-2---------Bromoform _ . -. 79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l 3-Dichloroprooene --, -1330-20-7-------Xylene (Total) 67-64-1---------Acetone
78-93-j---------2-Butanone
75-15-o~•-------Carbon Disulricte 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total)
--
5000 u
5000 u
5000 u
5000 u 5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
29000 D
5000 u
44000 D
5000 u
8900 D
5000 u
5000 u
5000 u
5000 u -·· 1900 DJ
SOOD u
Cf'\nl"\ u ..JVVV
5000 u
5000 u
5000 u
6300 D
100000 DE
5000 u
5000 u
5000 u
5000 u
5000 u
(UL
I
I
I
FORM I VOA OLI'103. 0
I
.al Name:
lE VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTI?IED COMPOUNDS
PACE ANALYTICAL SERVICES Contract·:
EPA SA..VfPLE NO.
EX-l0DL
.alCode: PACE Case No. : SAS No.: SDG No.: 108086
a ix: (soil/wat:er) WATER ·a1le wt/vol:
e l: (low/med)
· [llisture: not dee.
5. 000 (g/mL) ML
LOW
C~olumn: DB-624 ID: 0.32 (mm)
Extract Volume: ____ (uL)
Lab Sample ID: 10696433DL
Lab File ID: 1830701007
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 500.0
Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
N er TICs found: 3 (ug/L or ug/L) ug/L
I
CAS NUMBER COMPOUND NAME .. . RT EST. CONC. Q
=~============= ========================= ·== ======== ------======= ===== . 115-07-1 PROPENE 4.73 18000 NJBD
. 67-63-0 ISOPROPYL ALCOHOL 7.77 14000 NJTI
d: 557-40-4 1-PROPENE, 3,3'-OXY3IS-12.11 26000 NJTI
6.
I:
10.
~:
14. I:
17.
I: . -·· """"""' .... ~ , ...... ~ . .... , ..... ·~·~ .. -I -
21.
I:
i:
28. f:
' •··
I FORM I VOA-TIC OLM03.0
I 100.358
I
I 1.",.
VOLATILE ORGANICS AN~.LYSIS DATA SHEET
EPA SAM?LE NO.
EX-l0DLB
PACE ANALYTICAL SERVICES Contract:
::i._coc:e: ?ACE Case No.: SAS No.: SDG No.: 108086
::l.x: (soil/water)
we/vol:
WATER Lab Sample ID: l0696433DLB
5.000 (g/mL) ML
LOW
Lab File ID: 1833201032
(low/med)
~1-sture: not dee.
~olumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 1000.0
ii Extract Volume : ____ (uL) Soil Aliquot Volume: ---:--(UL
D
D
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane -•-~·
75-01-4---------Vinyl Chloric:e
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform •'
71-55-6---------1,1,1-Tricnloroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dichloroetnane
79-01-6---------Trichloroethene
78-87-5---------1 2-Dichloroorooane ' --75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroecnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
29000
10000
48000
10000
9100
10000
10000
10000
108-30-7--------Chlorobenzene . ... .... ··-------··-· -· -··-.... ., .. ·--1·0 0 0 O
100-41-4-~-0 ----Ethylbenzene ... 1900
100-42-5--------Styrene 10000
75-25-2---------Bromoform 10000
79-34-5---------1,1,2,2-Tetracnloroethane 10000
10061-02-6------trans-l,3-Dichloropropene--10000
10061-01-5------cis-l 3-Dichloroorooene --10000 ' --1330-2O:7-------Xylene (Total) 4700
67-64-1~--------Acetone 93000
78-93-3---------2-Butanone 10000
75-15-0---------Carbon Disulriae 10000
108-10-1--------4-Methyl-2-Pentanone 10000
591-78-6--------2-Hexanone 10000
540-59-0--------1,2-Dichloroetnene(Total) --10000
rORM I VOA
Q
u u u u u u u u u u u
u
u
J u u u u
J
u u u u
u
J
B u u
u
u u
OLM03.0
lE I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTI?IED COMPOu"'NDS
EPA S)I.NPLE NO_
:n •. e
-.,~:
PACE ANALYTICAL SERVICES
wt/vol:
(low/med)
.Case No.:
WATER
5. 000 (g/mL) Ml..
LOW
~,sture: not dee.
Column: DB-624 ID: 0.32 (mm) :.I Extract Volume : ____ (uL)
Contract:
SAS No.:
EX-lCDLB
SDG No.: 108086
Lab Sample ID: 10696433DLB
Lab File ID:
Date Received:
1833201032
06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 1000.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS:
.l er ~ s oun d 3 : ( /L /L) /L ug or ug ug
.... ..
C.Z\S NUMBER COMPOUND NA.."lE RT EST. CONC. Q
=1============ ====================-------= :=:======= -----=-:;:===== ===== . 115-07-1 PROPENE 4.75 22000 NJB
2. UNKNOWN 7.79 14000 J
fl 557-40-4 t-PROPENE, 3,3'-OXY3IS-12.12 25000 NJ
6.
~
-0 . ~,
_3 .
ll :1
.7. .. . . :J I . '
'.l. :I
4 .
I ..
. 8.
~I
(uL
I
I
FORM I VOA-TIC OLM03.0
1 i
I lA VOLATILE ORGANICS A.i~A.LYSIS DA.TA SHEET
P.Z\.CE ANALYTICAL SERVICES
'1Code: PACE
,trix: (soil/water) ,f le wt/vol:
,vel: (low/med)
fisture: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
Contract:
SAS No.:
Lab
Lab
Date
Date
EPA SAMPLE
NS-09
SDG No. : 108086
Sample ID: 10696334
File ID: 1781501015
Received: 06/22/98
Analyzed: 06/27/98
: Column: DB-624 ID: 0.32 (mm) Dilution Factor: 10.0
NO.
,I Extract Volume : ____ (uL) Soil Aliquot Volume: ----
g
0
0
0
I
CA.S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,l-Trichloroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2----~---l,2-Dich~oroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlcrobe~zenc ..
100-41~4 --~-- - - --Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64~1---------Acetone -78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
Q
···-··
100 u
17 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
8200 E
100 u
100 u
100 u
76 J
100 u
100 u
100. _u __ ---· -100 u
100 u
100 u
100 u
100 u
100 u
100 u
22 J
53 J
100 u
100 u
100 u
100 u
100 u
(uL
FORM I VOA OLM03.0
I 100.188
1£ I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SA.."IPLE NO.
J Name: PACE ANALYTICAL SERVICES
, lode: P!\CE
:rix: ( soil/water) nle wt/vol:
''ir: (low/med)
~•.sture: not dee.
Case No.:
WATER
5. 000 (g/mL) ML
LOW
l'lumn: DB-624 ID: 0.32 (mm)
Contract:
SAS No.:
_NS-09
SDG No.: 108086
Lab Sample ID: 10696334
Lab File ID: 1781501015
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 10.0
i.l'Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
iler TICs found: 3
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
... . .. .. . ..
I:: NUMBER COMPOUND NAME RT EST. CONC. Q
= =-==-==--=-=======-==-================= ======== -=;;;; __ ;::;::;::::;;:==== =====
1. UNKNOWN 4.40 400 JB
I 115-07-1 PROPENE 4.74 370 NJB
557-40-4 1-PROPENE, 3,3'-OXYBIS-12.15 94 NJ
5 .
' ti
12.
ti
16.
ti I I I
.1.;:, •
~~
23. ~-27. ~• 30.
FORM I VOA-TIC OLM03.0
I 100,189
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
_b Name: PACE ~~~~.LYTIC.ll.L SERVICES Contract:
EPA SAMPLE NO.
NS-09DL
:::il=oce.: P.Z\.CE
_c:;rix: (soil/water)
mle wt:/vol:
Case No.:
WATER
SAS No.: -SDGNo.: 1080_86
Lab Sample ID: 10696334DL
Lab File ID: 1781401014
.v1, (low/med)
M sture: not dee.
5.000 (g/mL) ML
LOW
'
lumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 100.0
i Extract Volume: ____ (uL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
g
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroet:nene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2------~--Benzene
107-06-2--------1,2-DichLoroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroethane
127-" 18--4 -, __ ------aTetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7------~~Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-0l-S------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulride
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Tot:al) --
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
20000
1000
1000
1000
1000
1000
1000
l('\"" V VV
1000
1000
1000
1000
1000
1000
1000
1000
360
1000
1000
1000
1000
1000
----
Q
u u u u u u u u u u u
DE u u u
u u u u u u
u
u u u u
u
DJ u
u
u u u
(uL
0
H
D
D
FORM I VOA OLM03.0 •
100404
12 I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SA..'1PLE NO.
al Name: PACE ANALYTICAL SERVICES
ab Code: PACE Case No.:
al-ix: (soil/water) WATER alle wt/vol:
= 1: (low/med)
5.000 (g/mL) ML
LOW
l isture: not dee.
: olumn: DB-624 ID: 0.32 (mm)
Extract Volume: (uL) ----
~umber TICs found: 2
NS-09DL
Contract:
SAS No.: SDG No.: 108085
Lab Sample ID: 10696334bL
Lab File ID: 1781401014
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 100.0
Soil AliQ.J.ot Volume:
CONCENTR.~TION UNITS:
(ug/L or ug'/L) ug/L
____ (uL
CAS NUMBER COMPOUND NAME . RT EST. CONC. I
Q
·1-============
_. 115-07-1
3. ': 7.
I: 10_.
1,. 1 .
1 .
14.
1,. 1 .
l, .
.1.8. ~m: --------
21.
!I
25.
~P. jb
0
D
==========================c= =;;;::====== -------====== ===== UNKNOWN 4.39 3400 JBD PROPENE 4.74 1400 NJBD
. .
••es••-••~·----·-..... ·-·-· . .
---·
FORM I VOA-TIC OLM03.0
•
100'105
I
I
Ll\.
VOLATILE ORGANICS ANALYSIS DATA SHEET
PACE ANALYTICAL SERVICES Car.tract:
EPA SAMPLE NO.
NS-09DLB ''a Name:
1.Code: PACE ,lix: (soil/water)
1 _ le wt/vol:
Case No.:
WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696334DLB
5.000
LOW
(g/mL) ML Lab File ID: 1833701037
=•l: (low/med)
loisture: not dee.
:folumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 200.0
Jil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
I
I
I
I
I
I
m
g
n
0
D
' ·o
'
I
CAS NO. CO_MJ'OUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,l-Trichloroetnane -
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicnloroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
12 7 -18 -4 - - - --·0·=-·=Teit"ia·cnloroethene
124-48-1--------DibromochloJ?ometh-ane
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroetnane
10061-0~-6------trans-l,3-Dichlorooropene--
10061-01-5------cis-l 3-Dichloroorooene --' --1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disuli:iae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
FORM I VOA
Q
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
25000
2000 0
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
2000 u
550 JB
2000 u
4500 B
2000 u
2000 u
2000 u
OLM03.0 .
1004 '1
lE
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
?ACE ANALYTICAL SERVICES
Case No.:
~]ix: (soil/water) WATER
, _le wt/vol: 5.000 (g/mL) ML 'Jl: (low/med)
L oisture: not dee.
LOW
~ tlumn: DB-624 ID: 0.32 (mm)
Contract:
SAS No.:
NS-09DLB
SDGNo.: 108086
Lab Sample ID: 10696334DLB
Lab File ID: 1833701037
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 200.0
,il Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
iuloer TI Cs found: 1
ls NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST.
-
CONC. Q
~======--=------===========-===--=========== ======== ============= =====
I:
115-07-1 ?ROPENE 4.75 2300 NJB
4.
I:
8.
1,: 1 .
12. 11-1 .
15.
i· .. , ··-··--·••--·•·· ........ ··•·· .. •...
~ :
I --
19. j:
2 .
21. 2 .
2 .
25.
20. 2 .
2 .
30.
-0
,·
·n FORM I VOA-TIC OLM03.0
100415
I
I
:LA VOLATILE ORGANICS A.~ALYSIS DATA SHEET
EPA SAMPLE NO.
NS-10
j Name: PACE A.~ALYTICAL SERVICES Contract:
jlode: P.",.CE Case No. : SAS No. :
--ix• (soil/water) WATER
SDG No.: 108086
:,e.wt/vol: 5.000 (g/mL) ML
vw: (low/med)
~J_sture: not dee.
LOW
Lab
Lab
Date
Date
Sample ID: 10696342
File ID: 1783301033
Received: 06/22/98
Analyzed: 06/28/98
,
lumn: DB-624 ID: 0.32 (mm) Dilution Factor: 2.0
i_ Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
I
n
D
D
I • '
CAS NO. COMPOUND
74~87-3---------Chloromethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chlorid_e _______ _
74-83-9---------Bromomethane 75-00-3---------Chloroethane~--------
75-35-4·---------l,l-Dichloroecnene
75-09-2---------Methylene Chloride _____ _
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform ------
71-55-6---------1,l,l-Tricnloroecnane
56-23-5---------Carbon Tetrachloride----
71-43-2------~--Benzene 107-06-2--------l,2-Dic_n_1_o_r_o_e_c_n_a_n_e _____ _
79-01-6---------Trichloroethene 78-87-5---------1,2-Dichloropro_p_a_n_e ____ _
75-27-4---------Bromodichloromethane
108-88-3--------Toluene -----
79-00-5---------l,l,2-Tricn1oroecnane
127-18-4--------Tetrachloroethene. -----
124-48-l--------DibromocblnrnmQrn~~0
108-90-7--------Chlorobenzene -----
100-41-4--------Ethylbenzene ---------100 -42 - 5 - - - - - - - -Styrene
75-25-2---------Bromofo-rm-,-----------
79-34-5---------l,l,2,2-Tetracnloroecnane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloroorooene_===
1330-20-7-------Xylene (Total) --
67-64-1---------Acetone --------
78-93-3---------2-Butanone ----------75 - l 5 - 0 - - - - - - - - -Carbon Disul~lOe -------108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone --_---
540-59-0--------1,2-Dichloroetnene(Total)
20
20
20
20
20
20
20
20
20
20
20
970
20
20
20
5
20
20
20
20
20
20
20
20
20
20
4
6
20
20
20
20
20
----
Q
u u u u u u u u u u u
E u u
u
J u u u
u u u u
u
u u
J
J u u u u
u
( 1.!L
m ?OR."1. I VOA OLM03.0 .
100414
I LS
VOLJ>.TILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SA."!? LE NO .
=-I Name:
3.::, Code :
PACE P~~P.LYTICAL SERVICES
P .Z\.CE Case No.:
=-I ix, (soil/water) WATER
3.mple wt/vol: 5.000 (g/mL)
=11: (low/med) LOW
Contract:
SAS No.:
MT,
NS-10
SDG No.: 108086
Lab Sample ID: 10696342
Lab File ID: 1783301033
Moisture: not dee.
= lolumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 06/28/98
Dilution Factor: 2.0 J] Extract
iumber TICS
s NUMBER
Volume: ____ (uL)
found: 2
COMPOUND NP.I'1E
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
···RT EST.
----
CONC. Q !=============== --------------------------.-======::::= =============;;;:; ====== ': UNKNOWN 4.42 150 JB 115-07-1 PROPENE 4.76 34 NJB
" I ---
7.
1,
11.
ti
14.
ti
I 18. ... _ ······"' ... --· -. .
!P.
··-I
22.
ru
25.
Jil
29.
~11
I
FORM I VOA-TIC OLM03. 0
I
I 1004.?S
(uL
I lA VOLATILE ORGP..NICS ANALYSIS DATA SEEET EPA SP...,"!PLE NO.
,, Na~e:
,a.o Coae:
PACE ANALYTICAL SERVICES
P.l\CE Case No.:
Cont:::-act:
SP..S No. : SDG No.: 108086
Lab Sample ID: 10696342DL
Lab File ID: 1783201032
Date Received: 06/22/98
Date P.~,alyzed: 06/28/98
Dilution Factor: 25.0
•trix: (soil/water) WATER
·ample wt/vol: 5.000 (g/mL) ML
(low/med) LOW
Moisture: not dee.
cJolumn: DB-624 ID: 0.32 (mm)
Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
I
I
H
D
I i
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane --·· -· 75-01-4---------Vinyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4-----~---l,l-Dichloroecnene
75-09-2---------Methylene Chloride 75-34-3---------1,l-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,l-Trichloroechane .. 56-23-5-~-------Carbon Tetrachloride 71-43-2------"--Benzene
107-06-2--------1,2-Dicnloroecnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroechane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochlorometh~ne
108-90-7--------Chlorobenzene -· ·--,._ 100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tecracnloroechane
10061-02-6------trans-1,3-Dichloropropene--
10061-01-5------cis-l 3-Dichloroorooene --' --1330-20-7-------Xylene (Total) 67-64-1~--------Acecone
78-93-3---------2-Butanone
75-15-0---------Carbon DisuJ.riae 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Totaij --
250
250
250
250
250
250
250
250
250
250
250
1900
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
110
250
250
250
250
250
----
Q.
u u
u u u u u u u
u u
D u u
u u u u u
T_J
U.
u u
u u u
u
DJ u
u
u u
u
(uL
FORM I VOA OLM0J.0
I
I 1004J6
lE
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTI?IED COMPOUNDS
EPA s;. ... MPLE NO.
,ab Name: .al Code:
?ACE ANALYTI°CAL SERVICSS
,atrix: ( soil/wate:::-) alle wt/vol: .ell: (low/med)
. isture: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
Cfolumn: DB--624 ID: 0.32 (mm)
:n_ Extract Volume: (uL) ----
N~er TICs found: 2
Cont:::-act:
SAS No.:
NS--l0DL
SDG No.: 103086
Lab Sample ID: :!.0696342DL
Lab ?ile ID: 1783201032
Date Received: 06/22/38
Date .Z\.nalyzed: 06/28/98
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (UL
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
... J!s NUMBER COMPOu""ND NAME RT EST. CONC. Q = ========--== ============================ ===::;;;:===== ==:;;;:========== ===== 1. UNKNOWN 4.42 940 JBD
I:
115-07-1 PROPENE 4.75 300 NJBD
5 .
I:
8.
ii:
12. 11. 1 .
1 :J •
16. -·· .. -~ --__ _,, ,. . --. iR I
19.
!ft
23. ~-2b.
27.
~II
30.
-m_ . ' ' I . FORM I VOA-TIC . OLM03_ 0
I 10043'7
I
I L!\. VOLATILE ORGANICS A,_~p~YSIS DATA SHEET
PACE P~~ALYTICAL SERVICES Contract:
EPA SAL"IPLE NO.
NS-11
,yame:
c~Code: P .!\.CE Case No.: SAS No.: SDG No.: 108086
.,ix: (soil/water) WATER
,mple wt/vol: 5.000 (g/r.S) ML
Lab Sample ID: 10696359
Lab File ID: 1782401024
,11: (low/med) LOW Date Received: 06/22/98
Date Analyzed: 06/28/98 Moisture: not dee.
: .lumn: DB-624 ID: 0 .32 (mm)
Extract Volume: ____ (uL)
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL
I
I
n
I 0
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01.-4-- - - - - - --Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2-------~-Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Tricnloroetnane
56-23-5------c--Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicn~oroecnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene . , ..... ·······~ ··--· ...
124 -48 -1-- - - - - --Dil.J:cumoc~1.loromethane
... 108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-1 3-Dichloroorooene--' --10061-01-5------cis-l 3-Dichloroorooene --' --1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
6 J
10 u -· 10· u···
10 U· ..
10 u
15
10 u
10 u
10 u
10 u
10 u
64
2 J
10 u
10 u
10 u
10 u
10 u
OLM0.3. 0 .
I l.E VOLATILE ORGANICS ANALYSIS
TENTATIVELY IDENT!?IED
DATA SHEET
COMPOUNDS
EPA S.z>..l'1PLE NO.
NS-11 al Name: PACE ANALYTICAL SERVICES Contract:
alCode: PACE
3. ix: (soil/water) alle
= 1:
wt/vol:
(low/med)
.isture: not dee.
Case No.:
WATER
5. 000 (g/mL)
LOW
ML
:~olumn: DB-624 ID: 0.32 (mm)
SAS No.: SDG No.: 108086
Lab Sample ID: 10696359
Lab File ID: 1782401024
Date ~eceived: 06/22/98
Date .z>.~~alyzed: 06/28/98
Dilution Factor: 1.0 )I Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (UL
CONCENTRATION UNITS: r er TICs found: 3 (ug/L or ug/L) ug/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
'1_============ =====-=----------=========== ==:::===== ---========== ===== UNKNOWN 4.43 140 JB . 115-07-1 PROPENE 4.77 29 NJB 3. I: 590-50-1 2-PENTANONE, 4,4-DIMETHYL-15.07 4 NJ
6 .
I:
10.
~:
14.
~:
17.
... -···-'··· I
oo·:
-... I
..... ,.
·-· ---..
21. 1: 2 ..
ir 2 .
28.
21. 3 .
'
...
I FORM I VOA-TIC OLM03;0
I 100447
I
I
.b Name:
lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SA..'1PLE NO.
NS-15
PACE AN".ZU.YTICAL SERVICES
J:ode: PACE Case No.:
.t.ix: ( soil/water) WATER
Contract:
-SAS No.: SDG No.:· 108086
Lab Sample ID: 10696367
"'le wt/vol: 5.000 (g/mL) ML Lab File ID: 1780801008 vr.: (low/med)
'1 _sture: not dee.
LOW Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
'
lumn: DB-624 ID: 0.32 (mm)
i Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
I
I
I
g
u
I
I
I
I
I
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2------~--Benzene
107-06-2--------1,2-Dichloroechane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroethane
127-18-4--------Tetrachloroethene
12~~48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulride
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
13 0
10 u
10 u
10 u
7 J
10 u
10 U·. ···-···
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
6 J
2 J
10 u
2 J
10 u
10 u
OLM03.0
lS
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SA.'1PLE NO.
0yame:
.::lcoc.e :
PACE ANALYTICAL SERVICES
PACS Case No.: ·1ix· (soil/wate::-)
: ,_ ~~.wt/vol:
•f: (low/med)
~isture: not dee.
WATER
5.000 (g/mL) ML
LOW
tlumn: DB-624 ID: 0.32 (mm)
il Extract Volume: ____ (uL)
Cont::-act:
SAS No.:
NS-15
SDG No.: 108086
Lab Sample ID: 10696367
Lab File ID: 1780801008
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL
uler TICs found: 15
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
s NUMBER
==========-----I
4.
D.
8.
tP
ti
15.
tl
L9.
lJ.
11
~ 6.
:I
,0.
I
•
I
115-07-1
115-11-7
75-65-0
75-33-2
71-36-3
557-40-4
513-86-0
627-59-8
50996-72-0
50996-72-0
595-41-5
5700-04-9
2568-90-3
54518-04-6 ---... «-•·-~-
COMPOUND NAME
----------------------------UNKNOWN
PROPENE
1-PROPENE, 2-METHYL-
2-PROPANOL, 2-METHYL-
2-PROPANETHIOL
1-BUTANOL
1-PROPENE, 3,3'-OXYBis~
2-BUTANONE, 3-h'YDROXY-
2-HEXANOL, 5-METHYL-
1-PROPENE, 3-[(1-METHYLETHYL
1-PROPENE, 3 - [ ( 1-METHYLETHYL .
3-PENTANOL, 2,3-DIMETHYL-
l,3-DIAZACYCLOHEPTAi'TE-2-THIO
BUTANE, 1,1'-[METHYLENEBIS(O
METHAN'OL, DIBUTOXY--..
. •.
FOfu'1 I VOA-TIC
RT EST. CONC. Q ======== ============= =====
4.41 160 JB
4.71 490 NJB
5.43 110 NJ
8.39 29 NJ
8.65 8 NJ
12.08 11 NJ
12.14 79 NJ
13.72 17 NJ
14.80 80 NJ
15.94 9 NJ
17.11 6 NJ
17.82 16 NJ
18.96 6 NJ
20.01 12 NJ
20.97 47 NJ
OLM03 :'O
100465
I
I
:.ab :,I
l.A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES NS-29 Contract:
Code : P _1\CE Case No.: SAS No.:
1atrix: (soil/water) WATER
SDG No.: 108086
Lab Sample ID: 10696318
Lab File ID: 1781201012
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 50.0
,lple wt/vol: 5.000 (g/mL) ML
aevel: (low/med) LOW
, loisture: not dee.
,~Column: DB-624 ID: 0.32 (mm)
,cll1 Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
g
D
D
E
E
I
CAS NO. COMPOUND
.
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug./Kg) UG/L
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-TricnLoroechane
56-23-5---------Carbon Tetrachloride
71-43-2-----,---Benzene
107-06-2--------1,2-DicnLoroecnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-TricnLoroetnane
127-18-4--.------Tetrachloroethene
12·4:: 48~ l. ~ - -·_ - -~ -Dibromochloromethane
108-50-7--------Chlorbbenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroechane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l 3-Dichloroorooene --' --1330-2O-7-------Xylene (Total)
500
500
500
500
500
500
500
500
500
500
500
4200
500
3700
500
1400
500
500
500
500
500
0
500
500
500
500
220 67-64-1---------Acetone 76000 78-93-3---------2-Butanone 310 75-15-0---------Carbon Disulriae 500 108-10-1--------4-Methyl-2-Pentanone 89 591-78-6--------2-Hexanone 500 540-59-0--------1,2-Dichloroechene(Total) 500 --
FORM I VOA
u u u u u
u u u u u u
u
u
u
TJ
u u u
J u u
u u
J
E
J
u
J u u
____ (UL
Q
!
OLM03.0
lE I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA Sl> .. MPLE NO.
,IName: PACE ANALYTICAL SERVICES
,b Code: PACE Case No. :
,fix: (soil/wat:er) WATER
,mole wt/vol: 5.000 (g/rnL) ML Ji, (low/med) LOW
l isture: not dee.
'. olumn: DB-524 ID: 0. 32 (mm)
Extract Volume: (uL) ----
Contract:
SAS No.:
NS-29
SDG No.: 108086
Lab Sample ID: 10695318
Lab File ID: 1781201012
Date Received: 05/22/98
Date Analyzed: 05/27/98
Dilution Factor: 50.0
Soil Aliquot Volume: ____ (uL
"umber TI Cs found: 8
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
c.~s ~TT.'MBER
71.============
. 115-07-1
3.
m:
0 •
7 .
R:
10.
tu: 1 .
14.
t9: 1 .
18.
lm-2 .
21.
2 •. 2 .
2 - .
25. ~,:
2 .
29. 31
I
I
115-11-7
75-08-1
79-20-9
75-65-0
557-40-4.
10152-76-8
..
COMPOUND NAME
--------------------------.-UNKNOWN
PROPENE
1-PROPENE, 2-METHYL-
ETHANETHIOL
ACETIC ACID, METHYL ESTER
2-PROPANOL, 2-METHYL-
1-PROPENE, 3, 3' -OXYBIS-
SULFIDE, ALLYL METHYL
··-~··--·--·····--·-.... . .. . ..
FORM I VOA-TIC
RT EST. CONC. ,....
"' =======;;;:: ;;;:;:::::;;_:;:_:::;;:;::;;;;;:;:;;::;:: =====
4.40 1900 JB
4.74 3400 NJB
5.44 1900 NJ
7.83 4700 NJ
8.15 250 NJ
8.41 290 NJ
12.15 1900 NJ
12.45 620 NJ'
OLM03.0 ....
I
I
l."'.
VOLATILE ORGANICS ANJ\.LYSIS DATA SHEET EPA SAMPLE NO.
,b Name: PACE ANALYTICAL SERVICES ,I Code: P!\.CE Case No. :
.1•ix: (soil/water) WATER
ulle wt/vol:
-''11: (low/med)
t-listure: not dee.
5.000
LOW
(g/mL) ML
ID: 0.32 (mm)
Contract:
SJ\.S No. :
NS-29DL
SDG No.: 108086
Lab Sample ID: 10696318DL
Lab File ID: 1781101011
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 500.0 : lolumn: DB-624
i.1. Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
I
g
D
D
m
I
I
I
I
I
... -..
••
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-35-4---------1,1-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-DicnLoroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroechane
127~18-4-------~Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoforrn
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l 3-Dichloroprooene--' -10061-01-5------cis-l,3-Dichloropropene --
1330-2.0-7-- - - - --Xvlene (Total)
Q
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
770 DJ
5000 u
5000 u
4400 DJ
5000 u
3700 DJ
5000 u
1400 DJ
5000 u
5000 u
5000 u ' 5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
67-64-1---------Acetone 100000 DE
78-93-3---------2-Butanone 840 DJ
75-15-0---------Carbon Disul:cicte 5000 u
108-10-1--------4-Methyl-2-Pentanone 5000 u
591-78-6--------2-Hexanone 940 .DJ
540-59-0--------1,2-Dichloroethene(Total) 5000 u --
FORM I VOA OLM03.0.
100518
lE
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA S;IJ<!PLE NO.
ib Name:
,Icade:
PACE ANALYTICAL SERVICES
P.l\.CE Case No.:
,.:rix: (soil/water) WATER
;rile wt/vol: 5.000 (g/mL) ML
,v"l: (low/med) LOW
listure: not dee.
: rlumn: DB-624 ID: 0.32 (mm)
i_ Extract Volume: (uL) ----
Contract:
SAS No.:
_NS-29DL
SDG No.: 108086
Lab Sample ID: 10696318DL
Lab File ID: 1781101011
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 500.0
Soil Aliquot Volume: ____ (uL
:uler TI Cs found: 4 CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
ts NUMBER
= ============
1.
I.
5. p
9. tfl
12. ~-~'
16.
t'-11
; 3 .
ll
!7. :I
'0.
I .
I
I
115-07-1
75-08-1
557-40-4
COMPOUND NAME
============================
UNKNOWN
PROPENE
ETF.ANETHIOL
1-PROPENE, 3,3'-OXY3IS-
. ·---· '. ··-
FORM I VOA-TIC
RT EST. CONC. Q
==:====== -------;:;:;===== ;;:;;::;;::;;::;;:
4.42 21000 JBD 4.76 · 9600 NJBD 7.84 5600 NJD 12.16 3300 NJD
.. ···-. .. ' . ....
OLM03.0
100S19
I
I
lA VOLATILE ORGANICS ANALYSIS DATA SHEET
1b Name: PACE A.'IALYTICAL SERVICES Contract:
EPA SAMPLE NO.
NS-30
11 Code: P.ll.CE
;.trix: (soil/water) ,Ile wt/vol:
Case No.: SAS No.: SDG No.: 108086
Lab Sample ID: 10696326
5.000 (g/mL) ML Lab File ID: 1780501005
,vel: (low/med) LOW
listure: not dee.
~ 11olumn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0 J, Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
I
a
D
D
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroetnane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicnloroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Trichloroethane
127-18-4--------Tetrachloroethene. .. . . ~ -···~. -... _,,. ..
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene -
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-0~-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulricte
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
5 J
10 u
5 J
10 u
10 u
10 u
10 u
10 u -10 u I
10 u
10 u
10 u
10 u
10 u
10 u
10 u
91
10 u
10 u
10 u
10 u I 10 u
I
OLM03.0
I 1E EPA S,111PLE
3.1 Name:
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
PACE ANALYTICAL SERVICES
3.1 Code : P .l\.CE
3.trix: (soil/water)
3.lle wt/vol:
~vel: (low/med)
listure: not dee.
: Column: DB-624
Case No.:
WATER
5.000 (g/mL) ML
LOW
ID: 0.32 (mm) JI Extract Volume: (uL)
NS-_:30
Contract:
SAS No.: SDG No.: 108086
Lab Sample ID: 10696325
Lab File ID: 1780501005
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
Soil Aliquot Volume:
NO.
--------
~twer TICs found: 3
COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. fS NUMBER
= ==::::========= ----------------------------======== =:;::;::::=:=========
UNKNOWN 4.42 94
2. 115-07-1 PROPENE 4.78 38
0: 75-18-3 DIMETHYL SlJLFIDE 7.85 9
5 .
d:
9.
I:
13. I:
16.
I: ... ·----. --~ ,. ---·-..
-
20.
I:
24. I:
27. j:
3 .
Q
::;;::::===
JB
NJB
NJ
--
.
(uL
I
I
I
FORM I VOA-TIC OLM03.0
I
I
L!\
VOLATILE ORGANICS ANALYSIS DATA SHEET
,b Name: PACE ANALYTICAL SERVICES Contract:
EPA SAMPLE NO.
NS-31
,.jccde: P.ll.CE Case No.: SAS No.: SDG No.: 108086
,trix: ( soil/wate:::-} WATER Lab Sample ID: 10696300
rrl1e wt/vol: 5. 000 (g/mL} ML Lab File ID: 1831301013
.vel: (low/med} LOW
Jist~:::-e: not dee.
.rlumn: DB-624 ID: 0.32 (mm}
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 250.0
l-Extracc Volume: (uL} Soil Aliquot Volume:
a
0
I
I
I
-I
I
I
I
I
'
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,l-Dichloroecnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2--------1,2-Dicnioroetnane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------l,l,2-T:::-icn1oroecnane
127-18-4--------Tetrachloroethene . . -.. . . -124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetracnloroechane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-2O-7-------Xylene (Total}
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
980
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
67-64-1---------Acetone 53000
78-93-3---------2-Butanone 840
75-15-0---------Carbon Disulr:ia:e 2500
108-10-1--------4-Methyl-2-Pentanone 2500
591-78-6--------2-Hexanone 2500
540-59-0--------1,2-Dichloroetnene(Total) 2500 --
----
Q
u u u u u u u u u u u u u u u
J u u .... u u u u u u u u u
E
J u u u u
(uL
I FORM I VOA OLM03.0
I
I lE
VOLATILE ORGANICS ANP.LYSIS DATA SHEET
EPA SP.1'1PLE NO.
J TENTATIVELY IDENTIFIED COMPOUNDS
,. Name: PAC2 ANALYTICAL SERVICE:S Contract: NS-31 1 --'I Code: P.ZI.CE
~trix: (soil/water)
Case No.: SAS No.: SDG No.: 108086
,,le wt/vol:
cvel: (low/med)
tisture: not dee.
WATER
5.000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm)
JI Extract Volume: ____ (uL)
Lab Sample ID: 10696300
Lab File ID: 1831301013
Date Received: 06/22/98
Date Analyzed: 07/02/98
Dilution Factor: 250.0
Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
,fber TICs found: 3 (ug/L or ug/L) ug/L
------------fS NUMBER COMPOUND NAME RT EST. CONC. Q
~ ============ ==========--====-====-====== =======::::: :;::::;::::===::;;====::;;= =====
115-07-1 PROPENE 4.73 6000 NJB
2. 513-85-9 2,3-BUTANEDIOL 7.77 2600 NJ
~: 557-40-4 1-PROPENE, 3,3'-OXYBIS-12.11 1600 NJ
6.
I:
9.
i:
13.
I:
_ 17 .... I: ----.....• ..
--
20.
I:
24.
~:
28. I:
I .. •
I FORM I VOA-TIC OLM03.0
I 100.549
I
I
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31DL
;.b Name : PACE ANALYTICAL SERVICES Cont::::act:
SAS No.: SDGNo.: 108086 ~,Code: PACE Case No. :
11::rix: (soil/water) WATSR Lab Sample ID: 10696300DL
ifle wt/vol: 5.000 (g/rnL) ML Lab File ID: 1833401034
,vel: (low/med) LOW
listure: not dee.
:~olurnn: DB-624 ID: 0.32 (mm)
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 500.0
,jl Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
D
D
m
I
I
I
I
I
I
•
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
-
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09~2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---~-----l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2---------Benzene
107-06-2-----~--l,2-Dichloroechane
79-01-6---------Trichloroethene
78-87-5---------1 2-Dichloroorooane ' . -75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroetnane
127-18-4--------Tetrachloroethene
124 -4 8 -1--------Dil:irrnnochloro,nethane
108-90-7---------Chlorobenzene
100-41-4--------Ethvlbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-O1-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disul:tioe
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroetnene(Totall --
FORM I VOA
Q
I
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
930 DJ
5000 u
5000 u
SOOD· u -·---
5000 u
5000 n u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
47000 DB
5000 u
5000 u
5000 u
5000 u
5000 u
OLM03.0
I
I lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
.al Name: PACE ANALYTICAL SERVICES al Code: PACE
at:::-:'..x: (soil/wate:::-)
a.Ile wt/vol:
evel: (low/med)
listu:::-e: not dee.
Case No.:
WATER
5.000 (g/mL) ML
LOW
: Column: DB-624 ID: 0.32 (mm) ~I Extract Volume: ____ (uL)
11Jrier TICs found: 1
...
NS-31DL
SAS No.: SDG No.: 108086
Lab Sample ID: 10696300DL
Lab File ID: 1833401034
Date Received: 06/22/98
Date Analyzed: 07/03/98
Dilution Factor: 500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
I
____ (UL
F NUMBER COMPOUND NAME RT EST. CONC. Q : =========== ============================ ======== -------------===== 115-07-1 PROPENE
2. 4.75 7300 NJBD
': I:
9.
I:
13.
1,. 1 .
1 . 1-, . -•·• -· . -_. ____ .. I
fl: --· I
20.
2,. 2 .
2 .
24.
2 •. 2 .
27. ~k 3 .
1 . .. •
I FORM I VOA-TIC OLM03.0
I l00.~61
1.l\. I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
ab Name: PACE AJ.'llAL YT I CAL SERVI CSS Contract: al Code: P.l\.CE Case No. : Si'>.S No. :
atrix: (soil/water) WATER Lab alle wt/vol: 5.000 (g/mL) ML Lab
evel: (low/med) LOW Date
listure: not dee. Date
EPA SAMPLE NO.
NS-32
SDG No.: 108086
Sample ID: 10696375
File ID: 1780601006
Received: 06/22/98
Analyzed: 06/27/98
:iolumn: DB-624 ID: 0.32 (mm)
:ill Extract Volume: (uL) ----
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (uL
0
D
I
I
I
I
I
I
C.l\.S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75-09-2---------Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
71-43-2-----~---Benzene
107-06-2--------1,2-Dicnloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Tricnloroethane
127-18-4--------Tetrachloroethene
124 -4·8 -1--: : --·--Dibromochloromethane
108-90-7--------Chloroben~ene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-1,3-Dichloropropene--
10061-O1-5------cis-1,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64~1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulricte
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total) --
F'ORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
1.0 u
]. 0 u
10 u
10 u
10 u
10 u
]. 0 u
10 u
10 u
10 u
10 u
10 u
]. 0 u
10 u
10 u
10 u
10 u
1.0 u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
10 u
10 u
OLM03.0
... c,,....,,...,.,
.,&. .v ... J ·•
lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPL2
Name: PACE ANALYTICAL SERVICES
.,. Coc.e: PACE Case No. :
,a,rix: (soil/water) WATSR
·Tie wt/vol:
.evel: (low/mec.)
tisture: not dee.
5.000 (g/mL) ML
LOW
·C Column: DB-624 ID: 0.32 (mm)
NS-32 Contract:
S!l.SNo.: SDGNo.: 108086
Lab Sample ID: 10696375
Lab File ID: 1780601006
Date Received: 06/22/98
Date Analyzed: 06/27/98
Dilution Factor: 1.0
NO.
~I Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS: N er TICs found: 2 (ug/L or ug-/L) ug/L
=t~S =~/T-'MBER==== COMPOUND NAME RT EST. CONC. Q =======------==---=----=-=== ====::::==== -=--==-:;:;====:::; :;::;==== UNKNOWN 4.42 84 JB 2. 115-07-1 PROPENE 4.75 13 NJB
I:
6.
q:
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13.
oo: 1 .
17. .. . -. ..
I ~: I
21. 2 .
2 .
24.
iS.
28. ~•
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I FORM I VOA-TIC OLM03.0
I 100572
I
I
I
I Method Blank
I
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I
I
I .·
n
u
H
I
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
,al Name: PACE ANALYTICAL SERVICES VBLKl 78 Contract:
aab Code: PACE Case No.: SAS No.: SDG No.: 108086
·alix: (soil/water)
a[le wt/vol:
e 1: (low/med)
WATER
5.000 (g/mL) ML
LOW
Lab Sample ID: VBLK178
Lab File ID: 1780401004
Date Received:
l'isture: not dee.
:~olumn: DB-624 ID: 0. 32 (mm)
Date Analyzed: 06/27/98
Dilution Factor: 1.0
Extract Volume: (uL) -----____ (uL Soil Aliquot Volume:
I
I
I
I
D
D
0
D
.u
u
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane· -10 u 75-01-4---------Vinyl Chloride 10 u 74-83-9---------Bromomethane 10 u 75-00-3---------Chloroethane 10 u 75-35-4---------1,1-Dichloroethene 10 u 75-09-2---------Methylene Chloride 10 u 75-34-3---------1,1-Dichloroethane 10 u 67-66-3---------Chloroform 10 u 71-55-6---------1,1,1-Trichloroethane 10 u 56-23-5---------Carbon Tetrachloride 10 u 71-43-2---------Benzene 10 u 107-06-2----~---l,2-Dichloroethane 10 u 79-01-6---------Trichloroethene 10 u 78-87-5---------1,2-Dichloropropane 10 u 75-27-4---------Bromodichloromethane 10 u 108-88-3--------Toluene 10 u 79-00-5---------1,1,2-Trichloroethane 10 u 127-18-4--------Tetrachloroethene 10 u 124-48-1--------Dibromochloromethane 10 u 108 -90-7--

-

-

-

-

-
-Chlorobenze!c.e .... ,,-.. _ .. ....... _. ___ ., ··--· 10 u 100-41-4--------Ethylbenzene ~----10 u 100-42-5--------Styrene 10 u 75-25-2---------Bromoform 10 u 79-34-5---------1,1,2,2-Tetrachloroethane 10 u 10061-02-6------trans-1,3-Dichloropropene--10 u 10061-01-5------cis-l,3-Dichloropropene --10 u 1330-20-7-------Xylene (Total) 10 u 67-64~1---------Acetone 5 J 78-93-3---------2-Butanone 10 u 75-15-0---------Carbon Disulfide 10 u 108-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 540-59-0--------1,2-Dichloroethene(Total) 10 u --
FORM I VOA OLM03.0
lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
VBLK178B Name: PACE ANALYTICAL SERVICES Contract:
Code: PACE Case No.:
]trix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: VBLK178B
Sample wt/vol: 5.000 (g/mL) ML Lab File ID: 1782201022
( low/med) LOW Date Received: :.,tel:
~ Moisture: not dee.
}.Column: DB-624 ID: 0.32 (mm)
Date Analyzed: 06/27/98
Dilution Factor: 1.0 ;oil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL I
I
I
I
I
D
D
D
E
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
-.. 75-01-4---------Vinyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride 75-34-3---------1,l-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2----C---l,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,1,2-Trichloroethane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene
···--····· 100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --1330-20-7-------Xylene (Total) 67-547_1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulria:e 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Total)
--
FORM I VOA
Q
-·-10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
~-.. 10 u. , .....
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2 J 10 u
10 u
10 u
10 u
10 u
OLM03.0
1006:.'.i8
lE I VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
:,t Name:
:,ab Code:
PACE ANALYTICAL SERVICES
?ACE Case No.:
1trix: (soil/water) WATER
Contract:
SAS No.:
VBLKl 78B
SDG No. : 108086
Lab Sample ID: VBLK178B ,ample wt/vol: 5.000 (g/mL) ML Lab File ID: 1782201022 (low/med) LOW
· Moisture: not dee.
,cf:olumn: DB-624 ID: 0.32 (mm)
oil Extract Volume: (uL) I -
~umber TICs found: 2
AS NUMBER COMPOUND NAME
Date Received:
Date Analyzed: 06/27/98
Dilution Factor: 1.0
Soil Aliquot Volume: ----CONCENTRATION UNITS: (ug/L or ug/L) ug/L
RT EST. CONC. Q ========-=-==-=--------=--=-=----=--=-====== ======== --=========== ===== I: UNKNOWN 4.42 38 J 115-07-1 PROPENE 4.77 11 NJ 4. ~:
8.
11:
11. ii 1 -.
15.
~--.... --. ·_9 . ·-· -···· --· -· ..
;fl -----• ---
:2.
~
6. ~D 9.
0.
I -1)
(uL
.. ,
FORM I VOA-TIC OLM03.0
m
100f>-~9
E
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
PACE ANALYTICAL SERVICES VBLK183 Contract: ,al Name:
,ab Code: PACE Case No.:
·aJix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: VBLK183
amole wt/vol: 5.000 (g/mL) ML ell, (low/med) LOW
Lab File ID:
Date Received:
1830301003
Moisture: not dee.
clolumn: DB-624 ID: 0.32 (mm)
Date Analyzed: 07/02/98
Dilution Factor: 1.0
I
I
I
•
g
0
D
D
I
Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroetnene
75·-09-2-- - - - - - --Methylene Chloride
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
· 71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2----~---l,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5---------1,l,2-Trichloroethane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
108-90-7--------Chlorobenzene --.. 1 o·o -4·1 -·4 - --- - - --Ethylbenzene
100-42-5~•==•---Styrene --
75-25-2---------Bromoform
79-34-5---------l,l,2,2-Tetrachloroethane
10061-02-6------trans-l,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --
1330-20-7-------Xylene (Total)
67-64-1---------Acetone
78-93-3---------2-Butanone
75-15-0---------Carbon Disulriae
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene{Total) --
FORM I VOA
Q
10 TJ
10 u
10 u
10 u
10 u
10 u
10 u 10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
·10 u
10-n V
10 u
10 u
10 u
10 u
10 u
6 J
10 u
10 u
10 u
10 u
10 u
OLM03.0
1006.57
lE I VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
+ Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.:
*rix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
Llel: (low/med) LOW
~.roisture: not dee.
:;I Column: DB-624 ID: 0. 32 (mm)
VBLK183
SDG No.: 108086
Lab Sample ID: VBLK183
Lab File ID: 1830301003
Date Received:
Date Analyzed: 07/02/98
Dilution Factor: 1.0
Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
Number TICs found: 1 CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
c_~s NUMBER----============-=== 11. 2 .
3 .
• 4. 5.
6.
7.
,8. 9.
0 .
11 .
• 2. 3 .
14.
ms. 6 .
7.
18. u~-V •
1.
22.
,3. 4.
5.
fa: .
29.
~ j
I
I
115-07-1
COMPOUND NAME RT EST. CONC. Q ======-=====-=============== ========= ::;;::;::;::;:::;::;;::;::;::;::::;:;:;;:::;: ===== PROPENE 4.73 22 NJ
' ------!
FORM I VOA-TIC OLM03.0
100658
I lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
lb Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
ltrix: (soil/water) WATER
s11mple wt/vol:
r.lvel: (low/med)
~~oisture: not dee.
5.000 (g/mL) ML
LOW
cl Column: DB-624 ID: 0.32 (mm)
VBLK183B Contract:
SAS No.: SDG No.: 108086
Lab Sample ID: VBLK183B
Lab File ID: 1832101021
Date Received:
Extract Volume: (uL) ----
Date Analyzed: 07/02/98
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (UL
I
I
I
I
I
I
I
CAS NO. COMPOUND. CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride 74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride 75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride 71-43-2---------Benzene
107-06-2--------1,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
75-27-4---------Bromodichloromethane
108-88-3--------Toluene
79-00-5-------~-1,l,2-Trichloroethane
127-18-4--------Tetrachloroethene
124-48-1--------Dibromochloromethane
_10.8 -.9..0 c .. 7-. ~ --. -.c.-.c.Chlorobenzene 100-41-4-----~-:Ethylbenzene I 100-42-5--------Styrene
75-25-2---------Bromoform
79-34-5---------1,1,2,2-Tetrachloroethane
10061-02-6------trans-1,3-Dichloropropene--
10061-01-5------cis-l,3-Dichloropropene --1330-20-7-------Xylene (Total) 67-64-1---------Acetone
78-9j-3~--------2-Butanone
75-15-0---------Carbon Disull:iae 108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
540-59-0--------1,2-Dichloroethene(Totall --
FORM I VOA
Q·
I
10 u I
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u I
10 TT . I
V I 10 u
10 u
10 u
10 u
10 u
10 u
3 J
10 u
4 J
10 u
10 u
10 u
OLM03.0
100665
I lE
.al Name:
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
PACE ANALYTICAL SERVICES
a. Code: PACE Case No.:
.a~ix: (soil/water) WATER arle wt/vol:
.evel: (low/med)
tisture: not dee.
5.000 (g/mL) ML
LOW
C Column: DB-624 ID: 0.32 (mm)
VBLK183B Contract:
SAS No. : SDG No. : 108086
Lab Sample ID: VBLK183B
Lab File ID: 1832101021
Date Received:
Date Analyzed: 07/02/98
Dilution Factor: 1.0 ~1 Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
N er TICs found: 1 (ug/L or ug/L) ug/L
···-CAS NUMBER COMPOUND NAME RT EST. CONC. Q
=1============= =======-==================== ======== -------------===== . 115-07-1 PROPENE 4.73 10 NJ
2.
d:
6 .
d:
10.
ft:
14.
II:
17.
M:
... ····------.. ..
I -.. --·----
21.
I:
25. I:
28. 1:
' •· FORM I VOA-TIC OLM03.0
I
I 10066ii
I lB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
tb Name: PACE ANALYTICAL SERVICES EX-01 Contract:
Lab Code: PACE Case No.:
rJtrix: ·(soil/water) WATER
SAS No.: SDG No. : 108086
Lab Sample ID: 10696441 Sample wt/vol: 970.0 (g/mL) ML Lab File ID: 18024 LJel: (low/med) LOW
~ Moisture: ___ decanted: (Y/N)
:Jcentrated Extract Volume: l000(uL)
=1·ection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0 , Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRAT1ON UNITS: (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-l~---~---l,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----7---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylpnenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2 4-Dichloroohenol -, . 120-82-1--------1,2,4-Trichlorobenzene.
91-20-3-------~~N~Phtfi~l~~e .. 106-47-8--------4-ChloroaniLine
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methrlnaphthalene
77-47-4---------Hexach orocyclopentadiene 88-06-2---------2,4,6-Trichlorophenol
--95-95-4---------2,4,5-Trichlorophenol
91-58~7~--------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylohthalate · 208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
l0
14
10
l 0
10
10
10
10
10
10
10
10
10
10
l0
10
10
10
10
l0
10
10
10
10
l0
26
10
26
10
10
10
26
10
u
u u u u u u u u u u
u
u
u u u u u u
u u
u
u
u u u u
u u u
u
u
("\ ><
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES Contract: EX-01
:.,I Code: PACE Case No.: SAS No.: SDG No.: 108086
.1 rix: (soil/water) WATER Lab Sample ID: 10696441
wt/vol: Lab File ID: 18024
(low/med)
970.0 (g/mL) ML
LOW
'< toisture: ___ decanted: (Y /N)
:oncentrated Extract Volume: l000(uL)
:lection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
;pc Cleanup: (Y/N) N pH: 7.0
E
I
I
I
I
I
I
I
I
I
l (1)
CAS NO. COM.!'OUND CONCENTRATION UNITS:
(-ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86 -3 0-6 - - - - -·_ - --N-Nitrosodiphenylamine ( 1) -
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate 206-44-0-- - - - - --Fluo:?:"anthene· ···· ......
129-OO-O--------Pyrene .. ...
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84~0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-co)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
2 J
10 u
10 '' V
10 u
10 u
10 u
10 u
6 JB
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0 I
I .:[)(VSJ
I
,J
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES
.• Code: PACE Case No. :
!a,rix: (soil/water) WATER atle wt/vol:
-evel: (low/med)
970.0 (g/mL) ML
LOW
tisture: ___ decanted: (Y/N)
Contract:: EX-01
SAS No.: SDG No.: 108086
Lab Sample· ID: 10696441
Lab File ID: 18024
·oncentrated Extract Volume: l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0 nl=ction Volume: 2.0(uL)
PC Cleanup: (Y/N) N pH: 7.0 D .
N1_1!!'.be:?:" TI Cs found: 10
AS NUMBER COMPOUND NAME
================
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q =======-==================== =:::===::;;;== ===::========;::== =====
I: UNKNOWN 3.48 30 J UNKNOWN 4.11 2 J UNKNOWN 4.28 7 J 4. UNKNOWN 4.37 2 J -: UNKNOWN 4.44 4 J UNKNOWN 4.48 4 J UNKNOWN 5.86 4 J 8. UNKNOWN 6.45 18 J B: UNKNOWN 6.86 34 J UNKNOWN 7.05 5 J 11.
I:
15.
I: I ·-
19. I:
22.
I: ..
26.
I:
30.
I '
I
I FORM I SV-TIC OLM03.0
I
1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ri Name: PACE ANALYTICAL SERVICES EX-02. Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 108086 Ml.rix: (soil/water) WATER Lab Sample ID: 10696458
Lab File ID: 18023
Siple wt/vol:
L el: (low/med)
l; foisture:
:cllcentrated Extract
I11ection Volume:
970.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0 ;~ Cleanup: (Y /N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I·
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (-.ig/L or ug/Kg)·· UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroetnyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol . 108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -. ·---~-·•-·-~-··"-120-82-1---------1,2,4-Trichlcrobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
140 E
220 E
10 u
10 u
10 u
10 u
10 u
10 u
11
10 u
10 u
10 u
10 u
10 u
10 u
10 u . . 10 u
10 u·,
10 u . ....
10 u
10 u
10 u
10 u
10 u
10 u
.26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
..
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
,al Name: EX-02 PACE ANALYTICAL SERVICES Contract:
·atll ~ode: P~CE Case No. : SAS No.: SDG No.: 108086
'afrix: (soil/water) WATER Lab Sample ID: 10696458
atle wt/vol: Lab File ID: 18023
evel : (low/med)
970.0 (g/mL) ML
LOW
tisture: ___ decanted: (Y/N)
~ncentrated Extract Volume: l000(uL)
nJction Volume: 2. 0 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
PC Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg)··uG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1----~---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate ~---.. -.-•-----------206-44-0--------Fluoranthene ..
129-00-0--------Pvrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84~0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
.. 10. u
10 u
10 u
10 u
10 u
10 u
10 u
10 JB
10 u
.10 u
10 u
10 u
10 u
10 u
10 u
400507
OLM03.0
I lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I TENTATIVELY IDENTIFIED COMPOUNDS
,a Name: PACE ANALYTICAL SERVICES Contract: EX-02
Case No.: ·"I Code: PACE
'at:rix: (soil/water) WATER tple wt/vol:
evel: (low/med)
970.0 (g/mL) ML
LOW
tisture: ___ decanted: (Y /N)
SAS No.:
oncentrated Extract Volume: l000(uL)
nllction Volume: 2.0(uL)
?C Cleanup: . (Y/N) N pH: 7.0
SDG No.: 108086
Lab Sample ID: 10696458
Lab File ID: 18023
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
~ler TICs found: 28 CONCENTRATION UNITS:
(ug/L or ug/Li ug/L
AS NUMBER
~========---==--, I:
4 .
Q:
8.
JD:
11.
1· 1 .
15. . -I:
19. 211. 211.
22.
2 •. 2 .
2 .
26.
2 .
79-31-2
78-40-0
...
4769-73-7
10544-50-0
COMPOUND NAME ==----=----=--============== PROPANOIC ACID, 2-METHYL-UNKNOWN ORGANIC ACID UNKNOWN
UNKNOWN ORGANIC ACID TRIETHYL PHOSPHATE
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
I TJN!<".NOWN .
UNKNOWN
UNKNOWN
HYDROCARBON
HYDROCARBON
ORGANIC ACID
2-PROPANOL, l-CHLORO-3-PHENO
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
SULFUR, MOL. (S8)
I
RT ======== 4.06
4.29
4.41
4.68
5.62
5.74
5.76
5.95
6.13
6.46
6.51
6.60
6.68
6.73
6.84
7.67
7.761
7.83
8.04
8.15
8.33
8.38
8.44
8.56
8.74
8.94
9.80
12.04
2,.
2 ·--------------------------30 ·--------------------------, I
EST. CONC. Q -:::======::::==== ===== 12 NJ
19 J
5 J
12 J
11 NJ
6 J
3 J
14 J
30 J
2 J
3 J
3 J
5 J
13 J
.. 2. _J __ , ...
1201J
6 1J
8 J
16 NJ
18 J
10 J
8 J
9 J
8 J
6 J
9 J
11 J
700 NJ
...
I
I
I
FORM I SV-TIC OLM03.0
400508
lB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-02DL
Name: PACE ANALYTICAL SERVICES Contract:
-J~ Code: PACE Case No. : SAS No.: SDG No.: 108086
,1J!lrix: (soil/water) WATER Lab Sample ID: 10696458DL
Lab File ID: 18117 'Jole wt/vol:
" el: (low/med)
'; moisture:
~oncentrated Extract
970.0 (g/mL) ML
LOW
decanted:
Volume:
(Y/N)
l000(uL)
:1ection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
;pc Cleanup: (Y/N) N pH: 7. 0
I
I
I
I
, I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
111-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol .
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isoohorone
88-75-5---------2-Nltroohenol
105-67-9--------2,4-Dimethylpnenol
111-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
Q
120 D
140 D
52 u
52 u
52 u
52 u
52 u
52 u
15 DJ
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
120-82-1--------1,2,4-Trichlorobenzene 52-u ........... , ..
I
I
I
I
1.
I
I
91-20-3---------Naohthalene
106-47-8-~-~-----4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichloroohenol --
95-95~·4---------2, 4, 5-Trichloroohenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
52 u
52 u
52 u
52 u
52 u
52 u
52 u
130 u
52 u
130 u
52 u
52 u
52 u
130 u
52 u
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
.al Name: PACE ANALYTICAL SERVICES
EX-02DL
Contract:
alCode: PACE Case No.: SAS No.: SDG No.: 108086
.a ix: (soil/water) WATER Lab Sample ID: 10696458DL
alllfle wt/vol: Lab File ID: 18117
e~l: (low/med)
risture:
~ncentrated Extract
:1tction Volume:
970.0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
PC Cleanup: (Y/N) N pH: 7.0
I
I
I
I
R
I
I
I
I
I
1(1)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kq) UG/L -.
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenhlamine (l)=
101-55-3--------4-Bromophenyl-p enylether
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
2 0 6 -4 4---0 -.-.-.---·--·Fl uoran thene
129-00-0--------Pyrene . .
85-68-7---------Butylbenzyipntnaiate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99w2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
Q
130 u
130 u
52 u
52 u
52 u
52 u
52 u
130 u
130 u
52 u
52 u
52 u
130 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
10 DJB
52 u
52 u
52 u
52 u
52 u
52 u
52 u
OLM03.0
I
I 400S58
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I TENTATIVELY IDENTIFIED COMPOUNDS
,1'Name: PACE ANALYTICAL SERVICES Contract: EX-02DL
11 Code: PACE Case No. : SAS No.:. SDG No.: 108086
,rrix: (soil/water) WATER Lab Sample ID: 10696458DL '1tle wt/vol:
,vel: (low/med)
970.0 (g/mL) ML
LOW f isture: ___ decanted: (Y /N)
1ncentrated Extract Volume: l000(uL)
,:lction Volume: 2.0(uL)
'C Cleanup: (Y/N) N pH: 7.0
Tuler TICs found: 13
s NUMBER COMPOUND NAME
Lab File ID: 18117
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. ====;;;::========== ---=-===----================ ======;;= =============
I:
107-92-6 BUTANOIC ACID 3.99 74 109-52~4 PENTANOIC ACID 4.43 37 UNKNOWN 4.93 11 4. 78-40-0 TRIETHYL PHOSPHATE 5.56 26 ': 109-59-1 ETHANOL, 2-(1-METHYLETHOXY)-5.86 16
UNKNOWN 6.69 24 UNKNOWN 6.85 33 8. UNKNOWN 7.06 130
11: UNKNOWN 7.27 2000 UNKNOWN 7.57 150 11. UNKNOWN 7.97 18
ti UNKNOWN 8.05 15 10544-50-0 SULFUR, MOL. (S8) 12.00 510
15. if 1 .
19. ~,
!t
26.
ii
3 0.
Q
===== NJD
NJD
JD
NJD
NJD
JD
JD
JD
JD
JD
JD
JD
NJD
i
,1
I
I
FORM I SV-TIC OLM03.0
lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
3.1 Name: PACE ANALYTICAL SERVICES Contract:
EX-03
3.iJ Code: PACE
3.Dll-ix: (soil/water)
Case No.: SAS No.: SDG No.: 108086
,.l\'le
e~l:
wt/vol:
(low/med)
WATER
960.0 (g/mL) ML
LOW
Lab Sample ID: 10696466
Lab File ID: 18025
lflfisture: decanted: (Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
JM!:entrated Extract Volume:
111tction Volume:
?C Cleanup: (Y/N) N
2. 0 (uL)
D
D
D
u
pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether -
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7---------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
12 0 -8 2 -1-- - - - -.-.. --1,.2., 4.-Trichlorobenzerre
51-20-3----~----Naphthalene
106-47-8--------4-Chloroaniline ---!
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
Q
130 E
280 E
10 u
10 u
10 u
10 u
10 u
10 u
8 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
lO u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
I
m
I
I
I
I
I.
I
I
FORM I SV-1 OLM03.0
400587
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
3.1 Name: PACE ANALYTICAL SERVICES Contract: EX-03
3.iuCode: PACE Case No.: SAS No.: SDG No.: 108086
3.111:-ix: (soil/water) WATER Lab Sample ID: 10696466
3.1lfle wt/vol: Lab File ID: 18025
~Jl!,1, (low/med)
1isture:
Jncentrated Extract
1tction Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
8~-74-8------•--Carbazole
84-74-2---------Di-n-butylphthalate
2 0 6 -4 4 - 0 - - - - ----·--Fl uoran thene· ·--·-·
129-00-0--------Pyrene _ -· 85-68-7---------Butylbenzylphcnaiate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine ..
FORM I SV-2
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
69 B
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
400SS8
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
EX-03 ,i Name: PACE ANALYTICAL SERVICES Contract:
,ab Code: PACE Case No.: SAS No.: SDG No.: 108086
·.Jlrix: (soil/water) WATER
,a.,le wt/vol:
elllkl: (low/med)
l isture:
~ entrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
nrction Vol,ume:
?~ Cleanup: (Y/N) N pH: 7.0
~Ler TICs found: 27
COMPOUND NAME
Lab Sample ID: 10696466
Lab File ID: 18025
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q
IAS NUMBER
= ============= ====-======================= ==;;;:===== -============= ===== 1. UNKNOWN 4.08 8 J
G: 1746-77-6 CARBAMIC ACID, 1-METHYLETHYL 4.24 2 NJ 2114-11-6 CARBAMIC ACID, 2-PROPENYL ES 5.32 2 NJ UNKNOWN 5.56 3 J 5 . 78-40-0 TRIETHYL PHOSPHATE 5.63 9 NJ
I: UNKNOWN 5.72 4 J UNKNOWN 5.97 13 J UNKNOWN 6.45 2 J 9 . UNKNOWN 6.49 3 J 11. UNKNOWN 6.74 5 J 1 . UNKNOWN 6.89 10 J 12. UNKNOWN 7.70 290 J
1,. UNKNOWN 8.00 4 J 1 . UNKNOWN 8.07 17 J 1 . UNKNOWN 8.17 36 J 16. UNKNOWN HYnRnr'M~BON-··· ···-· · ··· ··· . ~--• ··-···-··8-; 4 5· 35 J ~,-UNKNOWN 8. 58. 7 T u ~ . GNKNOWN 8.75 27 J. 1 . UNKNOWN 8.88 3 J 20. UNKNOWN 8.96 5 J
I ~I UNKNOWN 9.31 3 J UNKNOWN 9.57 2 J 23. UNKNOWN 9.61 4 J ii UNKNOWN 9.80 3 J UNKNOWN 10.16 2 J UNKNOWN 10.66 3 J 27. UNKNOWN 10.76 4 J ~-l . . ..
I I
. 1
OLM03.0 FORM I SV-TIC
I
I 40058:J
m 1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
.al Name: PACE ANALYTICAL SERVICES
EX-03DL
Contract:
alcode: PACE Case No.: SAS No.: SDG No.: 108086
.a ix: (soil/water) WATER Lab Sample ID: 10696466DL
Lab File ID: 18118 alfle
e'Jlle1:
wt/vol:
(low/med)
risture:
oncentrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
(Y/N)
l000(uL)
ntction Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
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I
1.
I
I
-
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1-- - - ----1, 2, 4 -Trich~lorobenzene•~-··-·
91-20-3---------Naohthalene ·
106-47-8--------4-Chloroaniline ----
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95~4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
140 D
200 D
52 u
52 u
52 u
52 u
52 u
52 u
7 DJ
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 u
52 1J
52 u
52 u
52 u
52 u
52 u
52 u
52 u
130 u
52 u
130 u
52 u
52 u
52 u
130 u
52 u
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
,al Name: PACE ANALYTICAL SERVICES Contract:
EX-03DL
all Code: PACE Case No.: SAS No.: SDG No.: 108086
.a~ix: (soil/water) WATER Lab Sample ID: 10696466DL
Lab File ID: 18118 arle wt/vol:
evel: (low/med)
960.0 (g/mL) ML
LOW
decanted: tisture:
oncentrated Extract Volume:
(Y/N)
1000 (uL)
ntction Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
PC Cleanup: (Y/N) N pH: 7.0
I
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, I
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol_
86-30-6-----~---N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
130
130
52
52
52
52
52
130
130
52
52
52
130
52
52
52
52
206.-41-0--------Fluoranthene ., ...... -•·· ----·····-·••-"••••-· · ·., 52
129-00-0--------Pyrene 52
85-68-7---------Butylbenzylphthalate 52
91-94-1---------3,3'-Dichlorobenzidine 52
56-55-3---------Benzo(a)anthracene 52
218-01-9--------Chrysene 52
117-Bl-7--------bis(2-Ethylhexyl)phthalate 61
117-84-0--------Di-n-octylphthalate -52
205-99~2--------Benzo(b)fluoranthene 52
207-08-9--------Benzo(k)fluoranthene 52
50-32-8---------Benzo(a)pyrene 52
193-39-5--------Indeno(l,2,3-cd)pyrene 52
53-70-3---------Dibenz(a,h)anthracene 52
191-24-2--------Benzo(g,h,i)perylene 52
-Cannot be separated rrom Diphenylamine
Q
u u u u u u u u u
u u u
u u u u u u
U. u
u u u
DB u u
u u u u u
I
FORM I SV-2 OLM03.0
I
I 400638
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES EX-03DL Contract:
LI Code: PACE Case No.: SAS No.: SDG No.: 108086
~ rix: (soil/water) WATER
S1f1ple wt/vol:
Lllrel: (low/med)
960.0 (g/mL) ML
LOW
%-lroisture:
::oncentrated
decanted:
Extract Volume:
Ilection Volume: 2.0(uL)
(Y/N)
1000 (uL)
3PC Cleanup: (Y/N) N pH: 7.0
Lab Sample ID: 10696466DL
Lab File ID: 18118
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
Imber TICs found: 21 CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
lcAs NUMBER
===========-=--= 1.
.2. 3.
4. .5. 6.
7.
8.
,9. 0.
l.
12.
,3. 4 .
5 .
,6. 7.
8.
19.
,0. l.
2.
23. 1: .
ti:
30 .
••
I
I
79·-o 9-4
107-49-3
10544-50-0
106-51-4
10544-50-0
COMPOUND NAME
-------------=============== PROPANOIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID UNKNOWN
UNKNOWN
UNKNOWN ORGANIC ACID
UNKNOWN
UNKNOWN
UNKNOWN
DI PHOSPHORIC ACID, TETRAETHY
SULFUR, MOL. ( S8)
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN ··-·······
UNKNOWN
UNKNOWN
P-BENZOQUINONE
UNKNOWN
SULFUR, MOL. (SB)
FORM I SV-TIC
RT EST. CONC. Q
========= ===:::::;;::;;::;;:;:;;;:;;;:;;;:;;;;;;:;; ===== 2.88 38 NJD 3.52 430 JD
3.72 150 JD
4.04 170 JD
4.09 94 JD
4.24 16 JD
4.36 110 JD
5. 21 180 JD
5.29 13 JD
5.55 32 NJD
5.69 13 NJD
5.86 46 JD
6.67 22 JD
6.85 53 JD
7.05 48 JD --·--···-?·:"59 ., --" .. -. ., 230 JD ...
7.76 --11 JD
7.98 19 JD
8.05 17 NJD
8.33 14 JD
12.00 590 NJD
OLM03.0
4006 ~
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
DUPLICATE
Name: PACE ANALYTICAL SERVICES Contract:
~tp Code: PACE Case No.: SAS No.: SDG No.: 108086
1.l:rix: (soil/water) WATER Lab Sample ID: 10696474
:;lfole wt/vol: Lab File ID: 18027
~~el: (low/med)
%-lroisture:
:oncentrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
(Y/N)
l000(uL)
:1ection Volume: 2. 0 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
3PC Cleanup: (Y/N) N pH: 7.0
I
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I
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CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol _
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---.-- - - --2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
Q
120 E
240 E
10 u
10 u
10 u
10 u
10 u
10 u
7 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
---
120-83-2--------2,4-Dich~oropheno -
120-82-1--------1,2,4-Trichlorobenzene ,_ '•• -----·····'l:0--u•-· ... -. -
1
I
I
I
I
I
.91.-20-3---------Naohthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachloroclclopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95~4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
10 u
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
DUPLICATE
Name: PACE ANALYTICAL SERVICES Contract:
,. Code: PACE
'.a,rix: ( soil/water)
;fple wt/vol:
Case No .. : SAS No.: SDG No.: 108086
WATER Lab Sample ID: 10696474
Lab File ID: 18027
,evel: (low/med)
· loisture:
960.0 (g/mL) ML
LOW
decanted: (Y /N)
:oncentrated Extract Volume: l000(uL)
:rlection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
:pc Cleanup: (Y/N) N pH: 7.0
I
I
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I
I
I
I
I
I
I
1. '
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-3 o -6-- - --·-- --N-Nitrosodiphenylamine ( 1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
26
26
10
10
10
10
10
26
26
10
10
10
26
10
10
10
10 84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene ... ---····-.. ........ . ----~-10
129-00-0----~---Pyrene 10
85-68-7---------Butylbenzrlphthalate 10
91-94-1---------3,3'-Dich orobenzidine 10
56-55-3---------Benzo(a)anthracene 10
218-01-9--------Chrysene 10
117-81-7--------bis(2-Ethylhexyl)phthalate 28
117-8J-0--------Di-n-octylphthalate -10
205-99-2--------Benzo(b)fluoranthene 10
207-08-9--------Benzo(k)fluoranthene 10
50-32-8---------Benzo(a)pyrene 10
193-39-5--------Indeno(l,2,3-cd)pyrene 10
53-70-3---------Dibenz(a,h)anthracene 10
191-24-2--------Benzo(g,h,i)perylene 10
(1) -Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
u u u u u u u u u u u u u u u u u u ·-·
u u u u u
B
u u u u u u
u
I
OLM03.0
lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY tDENTIFIED COMPOUNDS
.al Name: PACE ANALYTICAL SERVICES
DUPLICATE
Contract:
·1· Code: PACE Case No. : SAS No.: SDG No.: 108086
:a rix: (soil/water) WATER
-Tie we/vol:
,evel: (low/med)
960.0 (g/mL) ML
LOW
· loisture:
'.oncentrated
decanted:
Extract Volume:
·rJect:ion Volume: 2.0(uL)
(Y/N)
l000(uL)
,PC Cleanup: (Y/N) N pH: 7.0
Lab Sample ID: 10696474
Lab File ID: 18027
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
Jmber TICs found: 30
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
----------------============================ ======== -============ =====
11.
2 .
3.
4. 2114-11-6
15.
6. 78-40-0
7 .
8 .
~
9.
0.
1.
12.
13' 4.
15.
16 ,·• 10-7--58--4
7. . . --
8 .
19.
l o.
1.
L2.
23.
14.
5 .
26.
17.
8. 126-73-8
9.
30. 10544-50-0
I
I
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN
CARBAMIC ACID, 2-PROPENYL ES
UNKNOWN
TRIETHYL PHOSPHATE
UNKNOWN
UNKNOWN HYDROCARBON
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
UNKNOWN
2-!:'ROPENAMIDE, N-(1,1-DIMETH
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
UNKNOWN ALCOHOL
UNKNOWN
UNKNOWN
UNK..7'JOWN
PHOSPHORIC ACID TRIBUTYL EST
UNKNOWN
SULFUR, MOL. (SB)
FORM I SV-TIC
3.97
4.08
4.25
4.48
5.56
5.63
5.72
5.81
5.97
6.14
6.29
6.35
6.45
6.49
6.60
6.74
6.87
7.70
7.87
8.06
8.19
8.42
8.46
8.58
8.78
8.90
8.96
9.29
9.63
12.07
5 J
3 J
4 J
4 NJ
20 J
·79 NJ
40 J
3 J
120 J
140 J
4 J
25 J
25 J
14 J
10 J -.4.8. NJ _____ ._, ____ ..
3 J
250 J
15 J
5 J
47 J
4 J
14 J
7 J
72 J
2 J
21 J
3 NJ
5 J
2200 J
OLM03.0
400023
u lB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
lb Name: · DUPLICATEDL PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
ttrix: (soil/water) WATER
SAS No.: SDG No. : 108086
Lab Sample ID: 10696474DL
Sample wt/vol: 960.0 (g/mL) ML Lab File ID: 18120 rlvel: (low/med) LOW
% .Moisture:
~centrated Extract
Ijaiection Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
G~ Cleanuo: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis{2-rC~h,l~o~r~o-e-,,.t~h-y~l~)~e~t,h~e-r __ _ 95-57-8---------2-Chlorophenol 541-73-1--------1,3-Dichlorobe_n_z_e~n_e ____ _ 106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene ____ _ 95-48-7---------2-Methylphenol 108-60-1--------2,2'-oxybis{l-rC~h~I-o_r_o_p_r_o_p_a_n_e~}
106-44-5--------4-Methylphenol 621-64-7--------N-Nitroso-di-n ___ p_r_o_p_y_l~a_m_i_n_e_ 67-72-1--

-

-

-

-

-

-
-Hexachloroethane ______ -_-98-95-3--

-

-

-

-

-

-
-Nitrobenzene 78-59-1---------Isophorone ---------88-75-5---------2-Nitropheno 105-67-9--------2,4-Dimethylp~h-e_n_o_l _____ _ lll-91-l--------bis{2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol ____ ~.=
130 D
190 D
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
52 U
Q I
I
I
I
I
I
I
I
I
I
I
I
I
120-82-1--------1,2,4-Trichlorobenzene s2. _u~···--·.. __ ._,,. ....... __ _ -91-20-3---------Naphthalene ---106 -4 7-_8_--

-

-

-

-

-
-4-Chloroani~ine 87-68-3---------Hexachlorobutad~i-e_n_e ____ _ 59-50-7---------4-Chloro-3-methylphenol ---91-57-6---------2-Methrlnaphthalene 77-47-4---------Hexach orocrclopent_a_d~i-e_n_e __ 88-06-2---------2,4,6-Trich orophenol __ === 95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene ----88-74-4---------2-Nitroaniline
131-ll-3--------Dimethylphthal~a~t~e------
208-96-8--------Acena~hthylene 606-20-2--------2,6-Dinitrotol~u-e_n_e _____ _ 99-09-2---------3-Nitroaniline --------83 -32 -

9

-

-

-

-

-

-

-

-

-
Ace nap ht hen e ________ _
FORM I SV-1
52 U
52 U
52 U
52 U
52 U
52 U
52 U
130 U
52 U
130 U
52 U
52 U
52 U
130 U
52 U
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES Contract: DUPLICATEDL
cab Code: PACE Case No. :
,lrix: · (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696474DL
Lab File ID: 18120 ;lple wt/vol:
, el: (low/med)
: Moisture:
.Jcentrated Extract
rjection Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
~ Cleanup: (Y/N) N pH: 7.0
I
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I
I
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I
I
I
I
I
(
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----:----N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206 :.14.~.0.: -:..-:..c.:-.. 7 .c. cl'luoranthene
129-00-0--------?yrene ·
85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99=2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p aratect rrom Di hen p y lamine
FORM I SV-2
Q
130 u
130 u
52 u
52 u
52 u
52 u
52 u
130 u
130 u
52 u
52 u
52 u
130 u
52 u
52 u
52 u
52 u
5 ?. u
52 u
52 u
52 u
52 u
52 u
26 DJB
52 u
52 u
52 u
52 u
52 u
52 u
52 u
I
OLM03.0
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
-all Name: PACE ANALYTICAL SERVICES Contract: DUPLICATEDL
.ab Code: PACE Case No. : SAS No.: SDG No.: 108086 ·.all=ix: (soil/water) WATER
.amole wt/vol: ell: (low/med)
[
isture:
o entrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
nrction Volume:
?c Cleanup: (Y/N) N pH: 7.0
Lab Sample ID: 10696474DL
Lab File ID: 18120
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
~,lwer TICs found: 20
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
.AS NUMBER COMPOUND NAME RT EST. CONC. Q =· ;;;:======----;::;--==-=====-=;;;::=--===-=========;;;:= =======::;; =========::;;==== ===== 1. UNKNOWN 3.52 420 JD
I: UNKNOWN ORGAJ.'-IIC ACID 3.70 160 JD 503-74-2 BUTANOIC ACID, 3-METHYL-3.93 30 NJD UNKNOWN 4.03 70 JD 5 . UNKNOWN ALCOHOL 4.09 36 JD
I: UNKNOWN ORGANIC ACID 4.23 19 JD UNKNOWN ORGANIC ACID 4.35 110 JD UNKNOWN 5.20 240 JD 9. 78-40-0 TRIETHYL PHOSPHATE 5.53 28 NJD I: UNKNOWN 5.69 12 JD l.JNKNOWN 5.85 46 JD 12. UNKNOWN 6.67 25 JD j: UNKNOWN 6.87 71 JD UNKNOWN 7.05 44 JD . UNKNOWN HYDROCARBON 7.59 210 JD 16. UNKNOWN 7.98 19 JD J: -· •·•·· .... ·-·· -..• UN Ki'l"O WN 8.05 16JJD UNKNOWN -8.14 ---1--...... .l.O uLJ 1 . UNKNOWN 8.33 14 JD
i 20. 10544-50-0 SULFUR, MOL. (SB) 11.81 2100 NJD
2 •. 2 .
23.
2 •. 2 .
2 .
27.
2,. 2 .
3 .
,1
FORM I SV-TIC OLM03.0
I
I -~HJ D 0':"" 4
lB SEMIVOLATILE ORG~.NICS ANALYSIS DATA SHEET EPA SAMPLE NO.
cil Name: PACE ANALYTICAL SERVICES Contract:
EX-04
ci~Code: PACE Case No.: SAS No.: SDG No.: 108086
cil:ix: (soil/water) WATER Lab Sample ID: 10696482
Lab File ID: 18026 '"Ile wt/vol:
! 1: (low/med)
listure:
~ncentrated Extract
~,ction Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
?C Cleanuo: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl}ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methyl.[Jhenol
108-60-1--------2,2'-o~bis(l-Chloropropane}
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenoi
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
12 0-82 -1-- ----.-_,.,..,-.1.,-2 ,-4 -T-rich1orobenzene I 91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2 J
28
10 u
1 J
10 u
1 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
:!..O U.
10 u
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
I
.J
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-04 Name: PACE ANALYTICAL SERVICES Contract:
c!j Code: PACE Case No.: SAS No.: SDG No.: 108086
.air ix: ( soil/wat·er) WATER Lab Sample ID: 10696482
Lab File ID: 18026 ·11e wt/vol:
e 1: (low/med)
l='isture:
~9'centrated Extract
ntction Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
.I (1)
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
205-44-0--------Fluoranthene
129-00-0--------Pyrene __
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99•2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated tram Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 n V
10 TJ
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J TENTATIVELY IDENTIFIED COMPOUNDS
3. Na~e: PACE ANALYTICAL SERVICES Contract:
EX-04
"-I Code: PACE Case No. : SAS No.: SDG No.: 108086
3.trix: (soil/water) WATER
,,le wt/vol:
3.vel: (low/med)
960.0 (g/mL) ML
LOW f isture: ___ decanted: (Y /N)
~ncentrated Extract Volume: l000(uL)
1fction Volume: 2.0(uL)
~c Cleanun: (Y/N) N pH: 7.0 I -
!umber TICs found: 25
'AS NUMBER COMPOUND NAME
Lab Sample ID: 10696482
Lab File ID: 18026
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q
========--------==-===-===================== --------============= ===== , 78-40-0 TRIETHYL PHOSPHATE 5.70 9 NJ I: UNKNOWN 7.52 4 J
101-84-8 DIPHENYL ETHER 7.57 22 NJ
4. UNKNOWN 7.76 3 J
-:
UNKNOWN 7.98 5 J
UNKNOWN 8.03 9 J
UNKNOWN 8.09 3 J
8. UNKNOWN 8.29 2 J I: UNKNOWN HYDROCARBON 8.49 89 J
UNKNOWN 8.63 3 J
11. UNKNOWN 8.91 8 J
I: UNKNOWN 9.17 5 J
UNKNOWN 9.25 26 J
UNKNOWN 9.50 5 J
15. UNKNOWN HYDROCARBON 9.58 6 J
I: m, l\.l,vm, -.. ,. ----~--------• •►-' ..... --9.79 10 T
TThTV_}T('\fAThT -10.10 5 J
UNKNOWN 10.58 7 J
19. UNKNOWN 10.67 6 J
I: UNKNOWN 11.12 18 J
UNKNOWN 11.75 7 J
UNKNOWN 12.07 99 J
i: UNKNOWN 12.26 2 J
UNKNOWN 13.98 10 J
UNKNOWN 16.17 3 J
25.
I:
30 .
i
. 1
I
I
FORM I SV-TIC OLM03.0
I J.S SEMIVOLATILE ORGANICS AN~.LYSIS DATA SHEET EPA SAMPLE NO.
EX-05 PACE ANALYTICAL SERVICES Contract:
,i:.icode: PACE Case No. : SAS No.: SDG No.: J.08086
,tlix: (soil/water) WATER Lab Sample ID: 10696383
Lab File ID: 18124 ']le wt/vol:
, 1: (low/med)
l isture:
entrated Extract
·.j.ction Volume:
880.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
C Cleanup: (Y/N) N pH: 7.0
I
I
••
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
J.08-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
9S-so-J.---------l,2-Dichlorobenzene
95-48-7---------2-Methylphenol .
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1------~-l,2,4-Trichlorobenzene .. •• #""•·-
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline ·-. -· -
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95~4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
Q
2200
110 u
110 u
110 u
110 u
110 u
110 u
110 u
720
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
280 u
110 u
280 u
110 u
110 u
110 u
280 u
110 u
I
FORM I SV-1 OLM03.0
I
I 4CG'719
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
PACE ANALYTICAL SERVICES Contract: EX-OS
Jab Code: PACE
1lrix: ( soil/water)
Case No.:
WP..TER ·
SAS No.: SDG No.: 108086
Lab Sample·ID: 10696383
iamole wt/vol: 880.0 (g/mL) ML ,1:1, (low/med) LOW
Lab File ID: 18124
Joisture:
· centrated Extract
decanted:
Volume:
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/3_0/98
Dilution Factor: 10.0 J. ction Volume:
_ Cleanup: (Y /N) N
2.0(uL)
pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------i,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
280
280
110
110
110
110
110
280
280
110
110
110
280
110
110
110
110 206-44-0--------F'lnoranthene . --·----· ··---·•· _ .11 o _ 129-00-0--------Pyrene 110
Q
u u u u u u u u u u u u u
u
u u
u _ u_ , ...
u
I
I
I
I
I
I
·I-85-68-7---------Butylbenzr~pfithalate 110 u ------
I
• n
I
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo{a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separatect trom Diphenylamine
FORM I SV-2
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
OLM03.0 .
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EX-OS Name: PACE ANALYTICAL SERVICES Contract:
~ab Code: PACE Case No.: SAS No.: SDG No.: 108086
-!lrix: -(soil/water) WATER
;lple wt/vol:
, el: (low/med)
·Joisture:
'. centrated Extract
rwection Volume:
880. 0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
SOOO(uL)
-~ Cleanup: (Y/N) N pH: 7.0
~er TICs found: 26
COMPOUND NAME
Lab'Sample ID: 10696383
Lab File ID: 18124
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q lAS NUMBER
= ===========----=-===-==================== ======== -============ ===== 1. UNKNOWN ORGANIC ACID 3.90 160 J l: 1746-77-6 CARBAMIC ACID, 1-METHYLETHYL 4.17 130 NJ UNKNOWN 4.73 2800 J UNKNOWN 5.40 110 J 5 . UNKNOWN 5.66 23000 J -~ UNKNOWN 5.80 3200 J UNKNOWN 6.02 1300 J UNKNOWN 6.23 23000 J 9. UNKNOWN 6. 37 12000 J I: UNKNOWN 6.55 1500 J UNKNOWN 6.69 10000 J 12. UNKNOWN 6.76 1000 J I: UNKNOWN 7.71 290000 J UNKNOWN 7.71 290000 J UNKNOWN 7.71 . 290000 J 16. UNKNOWN --7. 7J. 290000 J I:
"' --... ,,_,,_, ....... -~ ·• · .. UNKNOWN 7.71 290000 ,T UNKNOWN 7.71 290000 J UNKNOWN 7.71 290000 J 20. UNKNOWN 8.03 6900 J I: UNKNOWN 8.18 4000 J UNKNOWN 8.91 2200 J 23. UNKNOWN 9.02 4000 J
2--UNKNOWN 9.21 2300 J 2 . UNKNOWN 9.30 1800 J 2 . UNKNOWN 9.57 2300 J 27.
2,. 2 .
3 .
·-·•-
FORM I SV-TIC OLM03.0
I 4CC721
I 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
'!I Name:
3.b Code:
EX-0SRE PACE ANALYTICAL SERVICES Contract:
PACE Case No.: '!fix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696383RE
Lab File ID: 19107 3.ile wt/vol:
! 1: (low/med)
l isture:
J entrated Extract
11· ct ion Volume:
880.0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 10.0
; Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
0
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1-----~--l,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
31-20-3--------"·Naphthalene ····· ···
106-47~8--------4-Chloroaniline ·-· -· 87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2400
110 u
110 u
110 u
110 u
110 u
110 u
110 u
590
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
1 1 f' TJ -'--'-'-'
110 u
110 u
110 u
110 u
110 u
280 u
110 u
280 u
110 u
110 u
110 u
280 u
110 u
OLM03.0
I
I 400774
I l.C SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
:.I Name: EX-0SRE PACE ANALYTICAL SERVICES Contract:
:Oab Code: PACE Case No. :
·!lrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696383RE
,ample wt/vol: 880.0 (g/mL) ML Lab File ID: 19107 ,Jel: (low/med) LOW
:Joisture:
: centrated Extract
decanted:
Volume:
rjection Volume: 2.0(uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 10.0 =' Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
D
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
121-14-2---~----2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-metnylphenol
86-30-6---------N-Nitrosodiphenhlamine (l)= 101-55-3--------4-Bromophenyl-p enylether __ 118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlpfithalate
206-44-0--------Fluorant ene 129-00-0~ -~-:::-~·=·=::i=>yrene · BS-68-7---------Butylbenzylpntnalace
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Dipnenylamine
•• FORM I SV-2
Q
280 u
280 u
110 u 110 u
110 u
110 u 110 u
280 u
280 u
110 u
110 u 110 u
280 u
110 u
110 u
110 u
110 u , , " u --v 110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u 110 u
110 u
110 u
OLM03.0
I
I 400'775
g lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
EX-05RE JI Name: PACE ANALYTICAL SERVICES Contract:
.ab Code: PACE Case No. : alix: (soil/water) WATER
SAS No.: SDG No.: 108086
alle wt/vol:
'" 1: (low/med)
l isture:
~ entrated Extract
880.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
5000(uL)
~,ction Volume:
? Cleanup: (Y/N) N pH: 7.0
~Ler TICs found: 30
COMPOUND NAME
Lab Sample ID: 10696383RE
Lab File ID: 19107
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 10.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q IAS NUMBER
= ============= ==--======================== ======::::= ====;;======== ===== 1. UNKNOWN 5.67 730 J
-:
6728-26-3 2-HEXENAL, (E) -6.44 440 NJ UNKNOWN 6 .46 580 J UNKNOWN 6.60 13000 J 5. UNKNOWN 6.74 1000 J I: UNKNOWN 6.83 32000 J UNKNOWN 7.63 470000 J 8. UNKNOWN 7.84 1300 J
I: UNKNOWN 7.93 14000 J UNKNOWN 8.09 5500 J UNKNOWN 8.55 80000 J 12. UNKNOWN 8.84 7500 J j: UNKNOWN 8.95 5600 J UNKNOWN 9.14 4200 J J!~. UNKNOWN 9.21 2400 J 16. UNKNOWN .-.-·-·--···--·.' ___ ;. ·-.. -· . -··· 9.41 1600 J
J: L.i"NKNOV\/1..J' 9.50 1800 J UNKl'i' OWN --9·~5 2· -380 J UNKNOWN 9.69 440 J
I: UNKNOWN 9.80 2500 J UNKNOWN 10.05 460 J UNKNOWN 10.15 400 J 23. UNKNOWN 10.22 400 J
I: UNKNOWN 10.73 1200 J UNKNOWN 11.01 420 J UNKNOWN 11.26 370 J 27. UNKNOWN 11.89 680 J
2,. UNKNOWN 12.08 390 J 2 . UNKNOWN 12.33 620 J 3 . UNKNOWN 12.66 390 J .
I
1
I
I
FORM I SV-TIC OLM03.0
400776
I 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
,ilJ Name: PACE ANALYTICAL SERVICES Contract:
EX-06
,ab Code: PACE Case No. :
!al)r-ix: . (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696391
;ample wt/vol: 890.0 (g/mL) ML Lab File ID: 18022 ,eJl: (low/med) LOW
Moisture:
:olentrated Extract
.n,· ction Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
1000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
,p Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
D·
n
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73 -1--------1·, 3 -Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-l--------bis{2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20 -3 ---------Naphthalene· ----·-· · ---~· . ·-
106-47-8--------4-Chloroaniline -
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methrlphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene . ,.
FORM I SV-1
Q
120 E
11 u
11 u
11 u
11 u
11 u
11 u
11 u
3 J
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
111u
i ~ TT ~~ V
11 u
11 u
11 u
11 u
11 u
28 u
11 u
28 u
11 u
11 u
11 u
28 u
11 u
400822
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
alName: PACE ANALYTICAL SERVICES Contract:
EX-06
alCode: PACE Case No. : SAS No.: SDG No.: 108086
a _ix: (soil/water) WATER Lab Sample ID: 10696391
alfle wt/vol: Lab File ID: 18022
a8tl: (low/med)
risture:
Jncentrated Extract
890.0 (g/mL) ML
LOW
decanted:
Volume:
(Y/N)
l000(uL)
~tction Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene - . -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol .
86-30-6-----~---N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene .. --· .. ····-·-··· -----..............
129-00-0--------Pyrene
85-68-7---------ButylbenzyLpncnaLace -·-··
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
) -Cannot be separated trom Diphenylamine
Q
28 u
28 u
11 u
11 u
11 u
11 u
11 u
28 u
28 u
11 u
11 u
11 u
28 u
11 u
11 u
11 u
11 u
11 u
ii 18
11 u
11 u
11 u
44 B
11 u
11 u
11 u
11 u
11 u
11 u
11 u
I
FORM I SV-2 OLM03.0
n
D 4008.23
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
,, Name: PACE ANALYTICAL SERVICES Contract: EX-06.
,ab Code: PACE Case No. : SAS No.: SDG No.: 108086 rf rix: ( soil/water) WATER
,ample wt/vol: 890.0 (g/mL) ML
,I-el: (low/med) LOW
Moisture:
:lcentrated Extract
·Djiection Volume:
decanted:
Volume:
2.0(uL)
0EI Cleanup: (Y /N) N
4mber TICs found: 28
(Y/N)
lOOO(uL)
pH: 7. 0
COMPOUND NAME ===-----=-----
-Lab Sample ID: 10696391
Lab File ID: 18022
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q =ICAS NUMBER =-=====--=================== ======== ============== ===== 1. UNKNOWN 4.04 54 J 2. UNKNOWN ALCOHOL 4.11 10 J I: UNKNOWN 4.86 440 J UNKNOWN 5.28 34 J 5 . 78-40-0 TRIETHYL PHOSPHATE 5.57 25 NJ
IL UNKNOWN 5.70 42 J UNKNOWN 5.94 16 J UNKNOWN 6.09 91 J 9. UNKNOWN HYDROCARBON 6.29 14 J I: UNKNOWN 6.58 460 J UNKNOWN 6.76 35 J UNKNOWN 6.93 560 J 13. UNKNOWN 6.99 27 J I: UNKNOWN 7.11 62 J UNKNOWN HYDROCARBON 7.57 16 J 16. 104-68-7 ETHANOL, 2-(2-PHENOXYETHOXY) 7.75 28 NJ lINKNOw1i , .. -"•"•"···--~ ---···· . 7:'8 T 11· J I: L'NK.llj"OWN HYD?..OC.".?..BON 7.96 --33 ~ u UNKNOWN 8.04 14 J 20. UNKNOWN 8.10 25 J I: UNKNOWN HYDROCARBON 8.32 22 J UNKNOWN 8.39 20 J UNKNOWN 8.51 16 J 24. UNKNOWN 8.69 19 J ,. UNKNOWN 8.94 20 J . UNKNOWN 9.61 16 J 27. UNKNOWN 9.79 14 J I: UNKNOWN 11. 34 10 J
I
I
FORM I SV-TIC OLM03.0
I
I 13
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
ag Name: PACE ANALYTICAL SERVICES Contract:
EX-06DL
ab Code: PACE Case No.:
al\Jr-ix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696391DL
amole wt/vol: 890.0 (g/mL) ML Lab File ID: 18116 eJl, (low/med)
Moisture:
~lentrated Extract
nr· ct ion Volume:
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
? Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1-----~---Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylpnenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
, .. -... _, '• ' .
Q
140 D
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
56 u
··--· 91-20-3---------Naphthalene .. ·56 u .
106-47-8--------4-Chloroaniline 56 u_~_J
I
D
I
I
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
56 u
56 u
56 u
56 u
56 u
140 u
56 u
140 u
56 u
56 u
56 u
140 u
-5.6 u
OLM03.0
4CC871
lC EPA SA."!PLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PACE ANALYTICAL SERVICES Contract: EX-06DJ:.
Lab Code: PACE Case No. :
~lrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696391DL
3amole wt/vol: 890.0 (g/mL) ML Lab File ID: 18116 -,1:1, ( low/med)
, .ioisture:
:cllcentrated Extract
:]·ection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
' Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitroohenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine {l)= 101-55-3--------4-Bromophenyl-phenylether
118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene ..... -........ -... , -. 129-00-0--------Pyrene
85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine 56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99:2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
Q
140 u
140 u
56 u
56 u
56 u
56 u
56 u
140 u
140 u
56 u
56 u
56 u
140 u
56 u
56 u
56 u
56 u
-56 u 56_ u
56 u
56 u
56 u
56 u
45 DJB
56 u
56 u
56 u
56 u
56 u
56 u
56 u
' I
FORM I SV-2 OLM03.0 g
u 40GEJ72
lF EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EX-0_6DL I ,11 Name: PACE ANALYTICAL SERVICES·--Contract:
,1b Code: PACE Case No.: SAS No.:
~I-ix: (soil/water) WATER
~ile wt/vol: 890.0 (g/mL) ML
~ l: -(low/med) LOW
l isture: decanted:
J entrated Extract Volume:
1ifction Volume:
"~Cleanup: (Y/N) N
2.0(uL)
(Y/N)
l000(uL)
pH: 7.0
__ -
SDG No.: 108086
Lab Sample ID: 10696391DL
Lab File ID: 18116
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 5.0
r~er TICs found: 16
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
JIAS NUMBER : =========---= l .
I:
5 .
I:
9.
ill:
12. l_. 1 .
1 .
16. ,,. -.
' ~ .
1 .
20. i,:
Ji
'. 7.
1a
I
I
1707-71-7
89-98-5
--
--
COMPOUND NAME --------========-===========
ETHYL PYROPHOSPHATE
BENZALDEHYDE, 2-CHLORO-
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
---'
FORM I SV-TIC
RT EST. CONC. Q =====:;:== -==--======:;;= ===== 5.53 12 NJD 5.62 15 NJD
5.69 23 JD
5.85 12 JD 6.47 310 JD
6.67 15 JD
6.87 470 JD
6.96 15 JD
7.05 46 JD 7.24 52 JD 7.55 12 JD 7.73 24 JD
7.95 24 JD
8.07 26 JD
8. 30 32 JD
8.91 20. . . JD. ___
OLM03.0
40G87J
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
,rlName: PACE ANALYTICAL SERVICES
EX-07
Contract:
1b Code: PACE Case No.: SAS No.: SDG No.: 108086
,IJix: (soil/water) WATER Lab Sample ID: 10696409
Lab File ID: 18127 i]le wt/vol:
~ 1: (low/med)
1Jisture:
)rl!entrated Extract
1ilction Volume:
940.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 1.0
'~Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
••
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorofhenol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7-----~--N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
··91-20-3 - - - - - - - --Naphthalene
106-47-8--------4-Chloroaniline
-.
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methllnaphthalene -
77-47-4---------Hexach orocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
13
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 ·u --.
11 u
11 u
11 u
11 u
11 u
11 u
26 u
11 u
26 u
11 u
11 u
11 u
26 u
11 u
OLM03.0
I 400903
I lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lt Name: EX-07. PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
1frix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample"ID: 10696409
3ample wt/vol: 940.0 (g/mL) ML Lab File ID: 18127
~lei: (low/med) LOW
, Moisture: ___ decanted: (Y/N)
:lcentrated Extract Volume: l000(uL)
=1·ection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 1.0
; Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
( 1)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenhlamine (l)= 101-55-3--------4-Bromophenyl-p enylether __ 118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
12 9 -0 0-0 ~-~-~-·~ --·~ ·c Pyrene
85-58-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99-2--------Benzo(b)fluoranthene
207-0S0 9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-ca)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-cannot be separated trom Diphenylamine
FORM I SV-2
Q
26 u
26 u
11 u
11 u
11 u
11 u
11 u
.26 u
26 u
11 u
11 u
11 u
26 u
11 u
11 u
11 u
6 J
11.U
11 u
11 u
11 u
11 u
11 u
18 B
11 u
11 u
11 u
11 u
11 u
11 u
11 u
OLM03.0
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
sf Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.:
'1,rix: (soil/water) WATER
3ample wt/vol: 940.0 (g/mL) ML ~lel: (low/med) LOW
, lifoisture:
~cllcentrated Extract
:ljection Volume:
decanted:
Volume:
2.0(uL)
; .. Cleanup: (Y /NJ N
(Y/N)
l000(uL)
pH: 7.0
EX-07
SDG No.: 108086
Lab Sample ID: 10696409
Lab File ID: 18127
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 1.0
-
~mber TICs found: 30 CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
=lAS NUMBER COMPOUND NAME RT EST. CONC. Q ::::======::::===== -::::::::--==-=::::-======::::=====::::==== ::::::::::::::::::::=== :::::;:::;:::::::::::;::;:::::::::::;;:::::::::;:;::::::::: ===== 1. UNKNOWN 3.84 4 J I: UNKNOWN .4.08 4 J UNKNOWN 4.14 2 J UNKNOWN 4.23 6 J 5 . UNKNOWN 4.30 13 J i: UNKNOWN ORGANIC ACID 4.44 6 J 2114-11-6 CARBAMIC ACID, 2-PROPENYL ES 5.26 9 NJ 78-40-0 TRIETHYL PHOSPHATE 5.57 14 NJ 9. UNKNOWN 5.74 59 J I: UNKNOWN 6.10 300 J UNKNOWN 6.27 16 J UNKNOWN 6.35 13 J 13. UNKNOWN 6.39 3 J I: UNKNOWN 6.42 12 J UNKNOWN 6.47 11 J 16. UNKNOWN 6.76 32 ·I I: . " --··-·· ... ~-.. UNKNOWN 6.85 4 J UNKNOWN ·--· 7.11 34 J UNKNOWN 7.67 7 J 20. UNKNOWN 7.75 9 J I: UNKNOWN 8.45 5 J UNKNOWN 8.57 8 J 121-66-4 2-THIAZOLAMINE, 5-NITRO-8.87 2 NJ 24. UNKNOWN 9.47 13 J I: 578-67"6 5-QUINOLINOL 9.57 13 NJ 17071-52-2 ETHER, BUTYL ISOPENTYL 9.98 210 NJ 27. 6765-39-5 1-HEPTADECENE 10.23 33 NJ I: 2033-89-8 PHENOL, 3,4-DIMETHOXY-10.74 8 NJ 10544-50-0 SULFUR, MOL. (SB) 12.06 1100 NJ 29833-69-0 1-PENTADECENE, 2-METHYL-12.79 7 NJ
I
I·
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I
FORM I SV-TIC OLM03.0
4CC905
I lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-08 PACE ANALYTICAL SERVICES Contract: "'I Name:
,ab Code: PACE Case No.:
itrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696417
·ample wt/vol: 960.0 (g/mL) ML Lab File ID: 18112
(low/med)
Moisture:
LOW
decanted: (Y /N)
=IJcentrated Extract Volume: S000(uL)
:1~ection Volume: 2. 0 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0 ?I Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
. 108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol 541-73-1--------1,3-Dich orobenzene 106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7-----~--N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthaiene -. -
106-47-8--------4-Chloroaniline -----87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95-4---------2,4,5-Trichlorophenol
91-58~7~--------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9-~-------Acenaphthene
Q
6300 E
1900
100 u
100 u
100 u
100 u
100 u
100 u
270
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
260 u
100 u
260 u
100 u
100 u
100 u
260 u
100 u
I
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I
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I
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FORM I SV-1 OLM03.0
400950 I
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
all Name: PACE ANALYTICAL SERVICES
EX-08
Contract:
.ab Code: PACE Case No. : SAS No.: SDG No.: 108086
·allrix: (soil/water) WATER Lab Sample ID.: 10696417
ailW'le wt/vol: Lab File ID: 18112
Jlel: (low/med)
111oisture:
:lbentrated Extract
nr· ction Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
? Cleanup: (Y/N) N pH: 7.0
I
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I
I
I
I
I
I
I
I
I·
I
( 1)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyren~ -..
a C: -68-7-- ---- ---0 "'"Y1 be-~"' ~h,-h~.1 ate '-'...J ........... ,._ .l. ..... ""'i.._.t" .. .._,,_._.c,...,_
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
:c -Cannot be separated Lrom Diphenylamine
FORM I SV-2
Q
260 u
260 u
100 u
100 u
100 u
100 u
100 u
260 u
260 u
100 u
100 u
100 u
260 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
OLM03.0
I 400951
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
~• Name: PACE ANALYTICAL SERVICES Contract:
~ab Code: PACE Case No.:
-1Jlrix: (soil/water) WATER
SAS No.: SDG No.: 108086
31ole wt/vol:
~ el: (low/med)
, IM"oisture:
:clcentrated Extract
:iJection Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
S000(uL)
;p~ Cleanup: (Y/N) N pH: 7.0
Ler TICs found: 16
COMPOUND NAME
Lab Sample ID: 10696417
Lab File ID: 18112
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
..
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q lAS NUMBER
= ======--===---=---------=----=--===-===== ======== =====::::=====::::= ====:== 1.
-: 5 . ~:
I:
12.
I:
16.
I:
20. I:
23. 1:
27.
I:
.I
I
I
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
ORGANIC ACID
HYDROCARBON
HYDROCARBON
HYDROCARBON
.. ....
FORM I SV-TIC
4.06 320 J 4.33 120 J 5.45 340 J 6.20 7900 J 6.58 3800 J
6.84 4000 J 6.98 94000 J 7.14 7800 J
9.84 440 J
9.93 650 J
10.20 430 J
10.35 260 J
11.40 330 J
12.02 1600 J
12.34 400 J
----. -12.62 , .. --· 1200 J
OLM03.0
400952
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
~1 Name: PACE ANALYTICAL SERVICES Contract:
.:.ab Code: PACE Case No.:
1lrix: (soil/water) WATER
SAS No.: SDG No. : 108086
Lab Sample ID: 10696417DL
.3ample wt/vol: Lab File ID: 18122
~•el: (low/med)
'Joisture:
: centrated Extract
:fjection Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 100.0
~" Cleanup: (Y/N) Y pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphchalene -------· . -~ .
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95~4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene .
FORM I SV-1
Q
7900 D
1800 D
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
2600 u
1000 u
2600 u
1000 u
1000 u
1000 u
2600 u
1000 u
OLM03.0
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
.£ame: PACE ANALYTICAL SE~VICES Contract:·
EX-08IlL
a.b Code: PACE Case No. :
,Jlix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696417DL
Lab File ID: 18122 "]le wt/vol:
, 1: (low/med)
l isture:
J entrated Extract
,j.ction Volume:
960. 0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
5000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 100.0
.'~Cleanup: (Y/N) Y pH: 7.0
I
I
I
I
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
Q
2600 u
2600 u
1000 u
1000 u
1000 u
1000 u
1000 u
2600 u
2600 u
1000 u
1000 u
1000 u
2600 u
1000 u
1000 u
1000 u
1000 u
1000 u
129-00-0--------Pyrene
... --···-···~-·· ·ro o o· u. -..
I
I
I
I
85-68-7---------Bucylbenz{ipnthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
ll7-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-9~-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo{a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
OLM03.0
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
,JName: PACE ANALYTICAL SERVICES Contract:
EX-08DL
,1-,code: PACE Case No. : SAS No.: SDG No.: 108086
,tlix: (soir/water) WATER
']le wt/vol:
! 1: (low/med)
960.0 (g/mL) ML
LOW
listure:
~ncentrated Extract
decanted:
Volume:
:ifction Volume: 2.0(uL)
?C Cleanup: (Y/N) Y
NLer TICs found: 26
(Y/N)
5000 (uL)
pH: 7.0
COMPOUND NAME
Lab Sample ID: 10696417DL
Lab File ID: 18122
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 100.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q
IAs NUMBER
=--========-==== =====-=================-==== ======== =====;;;======= =====
1. UNKNOWN 4.02 2700 JD
I: UNKNOWN 4.09 10000 JD
UNKNOWN 4.34 6700 JD
4. 104-76-7 1-HEXANOL, 2-ETHYL-4.97 2600 NJD
t: UNKNOWN 5.20 14000 JD
78-40-0 TRIETHYL PHOSPHATE 5.54 6000 NJD
UNKNOWN 5.67 4800 JD
8. UNKNOWN 5.86 2500 JD
I: UNKNOWN HYDROCARBON 6.43 1200 JD
UNKNOWN HYDROCARBON 6.47 3700 JD
UNKNOWN 6.69 1900 JD
12. UNKNOWN 6.88 66000 JD
,3. UNKNOWN 7.05 4600 JD
4. UNKNOWN 7.54 1800 JD
5. UNKNOWN HYDROCARBON 7.62 150000 JD
16. UNKNOWN 7.78 10000 JD
.7. UNKNOWN .. · ····· -7 ·; 8-7· -· -----· --~. · ---2000 ,JD
8 . UNKNOWN 7.99 27000 JD
UNKNOWN 2100·0 JD
19. 8.10
lo. 122-99-6 ETHANOL, 2-PHENOXY-8.31 72000 NJD
1. UNKNOWN HYDROCARBON 8.42 18000 JD
2. UNKNOWN 8.52 1800 JD
23. UNKNOWN 8.90 5100 JD
_4_ UNKNOWN 9.32 1400 JD
5. UNKNOWN 9.65 3000 JD
6 . UNKNOWN 11. 98 1500 JD
27 .
• 8. 9.
30.
I '
I-
I
I
FORM I SV-TIC OLM03.0
400988
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
31Name: PACE ANALYTICAL SERVICES Contract:
EX-09
3lCode: PACE Case No.: SAS No.: SDG No.: 108086
3 ix: (soil/water)
wt/vol:
WATER Lab Sample ID: 10696425
Lab File ID: 18113
(low/med)
l)isture:
~'=entrated Extract
~,ction Volume:
910.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
5000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
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I
I
I
I
I
I
I
I.
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7------------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1, 2, 4-Trichlorobenzene ________ .. ----~. ·-91-20-3--~-=----Naphthalene
105-47-8--------4-Chloroaniline --
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
-95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
1000
7700 E
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
1101u
110 U
110 u
110 u
110 u
110 u
110 u
270 u
110 u
270 u
110 u
110 u
110 u
270 u
110 u
OLM03.0
I
I 401078
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
1IName:
EX-09
PACE ANALYTICAL SERVICES Contract:
'-ii Code: PACE
a.I-ix: ( soil/water)
Case No.: SAS No.: SDG No. : 108086
,Ile
= el:
wt/vol:
(low/med)
WATER
910.0 (g/mL) ML
LOW
-Lab Sample ID: 10696425
Lab File ID: 18113
risture:
~ncentrated Extract
decanted:
Volume:
(Y/N)
5000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0 ~tction Volume: 2.0(uL)
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I. (1)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitroohenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534~52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphtnalate
206-44-0--------Fluoranthene ···•·-· ......
129-00-0--------Pyrene
85-68-7---------ButylbenzyLpntnaLate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Etfiylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
270 u
270 u
110 u
110 u
110 u
110 u
110 u
270 u
270 u
110 u
110 u
110 u
270 u
110 u
110 u
110 u
110 u
110 u
74 J
110· u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
OLM03.0
I
I 4010'2:9
lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
JName: PACE ANALYTICAL SERVICES
EX.-09
Contract:
·1code: PACE Case No.: SAS No.: SDG No.: 108086
~ ix: (soil/water) WATER
"Ile wt/vol:
J!h, (low/med)
1isture:
.ncentrated Extract
910.0 (g/mL) ML
LOW
decanted:
Volume:
(Y/N)
5000(uL)
·I ct ion Volume: 2. 0 (uL)
·C Cleanup: (Y/N) N pH: 7.0
Lab Sample ID: 10696425
Lab File ID: 18113
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/3_0/98
Dilution Factor: 10.0
,Ler TICs found: 30
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
IAs NUMBER COMPOUND NAME RT EST. CONC.
:========:=:=::;:==== ============================ :;;::;;:::;:::;:::;:::;:::;:::;: =======:;::;=====
1. UNKNOWN SUBSTITUTED BENZENE 3.96 240
I: 108-93-0 CYCLOHEXANOL 4.15 1100
UNKNOWN 4.50 400
4. UNKNOWN 4.93 4400
I: UNKNOWN 5.01 600
UNKNOWN 5.37 1800
UNKNOWN 5.57 1400
8 . UNKNOWN 5.71 10000
I: UNKNOWN 5.80 1100
UNKNOWN 5.97 1500
UNKNOWN 6.13 4200
12. UNKNOWN 6.45 1000
l: UNKNOWN HYDROCARBON 6.50 7400
UNKNOWN 7.12 20000
UNKNOWN 7. 35 19000
j UNY-1-JOWN 7.82 530000
UNKNOWN 8.01 --···--. •-·-5300
-·: ··-UNKNOWN HYDROCARBON · 8.06 420
19. UNKNOWN 8.19 9300
I: UNKNOWN ORGANIC ACID 8.24 5000
UNKNOWN 8.58 30000
UNKNOWN 9.02 2900
23. UNKNOWN 9.60 800
I: UNKNOWN 9.71 3400
UNKNOWN 10.16 490
UNKNOWN 10.22 280
I: UNKNOWN 10.94 360
UNKNOWN 11.38 770
UNKNOWN 12.01 1700
30. UNKNOWN 12.34 450
FORM I SV-TIC
Q
::;::::;:::::;;;:::;:
J
NJ
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J -·-
J
J
J
J
J
J
J
J
J
J
J
J
J
OLM03.0
I
I
401020
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09DL
PACE ANALYTICAL SERVICES Contract: ,. Name:
,~ Code: PACE
. -. ,.ix• ( soil/water)
Case No.:
WATER
SAS No.: SDG No. : 108086
Lab Sample ID: 10696425DL
1mple wt/vol: 910.0 (g/mL) ML Lab File ID: 18123
,11, (low/m~d) LOW
Moisture: ___ decanted: (Y/N)
,Jentrated Extract Volume: S000(uL)
1~ction Volume: 2. 0 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 100.0
0 lc1eanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2°Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
Q
1600 D
7100 D
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
I
I
I
I
I
I
I
I
1.
I
I
I
91-20-3---------Naphthalene . ·····--.......... 1100 u, -~----.
; I
I
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol -
91-SS-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
2700 u
1100 u
2700 u
1100 u
1100 u
1100 u
2700 u
1100 u
OLM03.0
401CBO
I lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
,I Name: PACE ANALYTICAL SERVICES
EX-09DL
Contract:
'ii Code: PACE Case No. : SAS No. : SDG No. : 108086
,.ix: (soil/water) WATER Lab Sample ID: 10696425DL
Lab File ID: 18123 ,Ile wt/vol:
, 1: (low/med)
l isture:
) entrated Extract
1,ction Volume:
910.0 (g/mL) ML
LOW
decant:ed:
Volume:
2.0(uL)
(Y/N)
S000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 100.0
'C Cleanup: (Y /N) N pH: 7.0
I
I
I
I
I
I ---. -· I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
' 51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1-----~--4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylpfit:halat:e
206-44-0--------Fluoranthene
129-00-0--------Pyrene I 85-68-7-~~------But:ylbenzyipnt:naiate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
11 7-81-7--

-

-

-

-

-
-bis {2-Ethylhexyl) phtfialate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cct)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
/ -Cannot be separat:ed trom Diphenylamine
FORM I SV-2
Q
2700 u
2700 u
1100 u
1100 u
1100 u
1100 u
1100 u
2700 u
2700 u
1100 u
1100 u
1100 u
2700 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u·
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
1100 u
·-·-1
OLM03.0
I
I 401081
lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS EX-09DL
Name: PACE ANALYTICAL SERVICES Contract: 'I Code: PACE Case No. : SAS No.: SDG No.: 108086
! rix: (soil/water) WATER
·1ple wt/vol:
,evel: (low/med)
910.0 (g/mL) ML
LOW
loisture:
:oncentrated
decanted:
Extract Volume:
tection Volume: 2.0(uL)
(Y/N)
5000(uL)
,PC Cleanup: (Y/N) N pH: 7.0
lmber TICs found: 22
lcAs NUMBER COMPOUND NAME
Lab Sample ID: 10696425DL
Lab File ID: 18123
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/3_0/98
Dilution Factor: 100.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q
==========-===== ============================ :;;::;:::;;::;;::;;::;;::;;:=: -----===;::;;:::;::;;:== =====
1.
.2. 3.
4. .5. 6.
7.
8. 107-58-4 1: 1.
12. I: 15. 15 ... . -., 17: 8.
19.
I:
23. I:
26.
I:
.30.
•·
I
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
2-PROPENAMIDE, N-(1,1-DIMETH
UNKNOWN HYDROCARBON
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
FORM I SV-TIC
4.42 1500 JD
4.97 5700 JD
5.20 12000 JD
5.51 1600 JD
5.66 6300 JD
5.87 2300 JD
6.47 4600 JD
6.68 10000 NJD
6.86 37000 JD
7.05 14000 JD
7.65 320000 JD
7.78 6300 JD
7.98 13000 JD
8.05 3700 JD
8.08 2100 JD
0 ..," V • "'>J · -2-7000 JD. ..
8.40 19000 JD
8.89 2600 JD
9.32 1700 JD
9.65 3300 JD
11.99 1200 JD
12.57 2300 JD
OLM03.0
401C82
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
.,Name: PACE ANALYTICAL SERVICES
EX-10
Contract:
,b Code: PACE Case No. : SAS No.: SDG No.: 108086 fix: (soil/wa·ter) WATER Lab Sample·ID: 10696433
Lab File ID: 18110 wt/vol:
(low/med)
1fisture:
rlentrated Extract
·:Wction Volume:
940.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
5000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
~Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene 9 i-2 o·--3 ...:·.: ~-.: _·...:·_ -.:·Na°i:ihthalene . .. .
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7~--------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95~4~--------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniiine
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
400
30000 E
380
110 u
110 u
110 u
110 u
110 u
110
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
~~~ltJ
.L.L u u
110 u
110 u
110 u
110 u
110 u
260 u
110 u
260 u
110 u
110 u
110 u
260 u
110 u
I
OLM03.0
D ~01118
\
I lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Name: PACE ANALYTICAL SERVICES EX-10 Contract:
.ab Code : PACE Case No. : SAS No.: SDG No.: 108086
Jrix: (soil/water) WATER Lab Sample ID: 10696433
Lab File ID: 18110 I le wt/vol:
_l: (low/med)
t='isture:
Jl:entrated Extract
:1,ction Volume:
940.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
5000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
° Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitroohenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --100-01-6--------4-Nitroaniline
534 -52 -1--

-

-
-.---4, 6 -Dinitro-2 -methylphenol_ 86-30-6---------N-Nitrosodiphenylamine (1) 101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
2 0.6.~.~-4 -0.-,a --. "·'·='"-Fl uoranthene 129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
260
260
110
110
110
110
110
260
260
110
110
110
260
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
110
I
I
~01119
Q
u u u u u u u u u u u
u u
u u u u u u
u u u u
u
u u u u u u
u
OLM03.0
I
I
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
EX-10 Name: PACE ANALYTICAL SERVICES Contract:
,2j Code: PACE Case No. : SAS No.: SDG No.: 108086
.Jlrix: (soil/water) WATER
Jple wt/vol:
el: (low/med)
risture:
oncentrated Extract
.ction Volume:
940.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
5000(uL)
?C Cleanup: (Y/N) N pH: 7.0
NLer TICs found: 27
COMPOUND NAME
Lab Sample ID: 10696433
Lab File ID: 18110
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/3_0/98
Dilution Factor: 10.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. lAs NUMBER =--============= -=========================== ==;;;;==::;:;== ::;.;::;;;;;;;;;;;;;;;;;;;;=====::: 1 . 100-41-4 ETHYLBENZENE 3.85 120 I: UNKNOWN SUBSTITUTED BENZENE 3.93 120 UNKNOWN 5.44 910 4. 78-40-0 TRIETHYL PHOSPHATE 5.68 250
I: UNKNOWN 6.16 2200 UNKNOWN 6.57 360 UNKNOWN 6.85 13000 8. UNKNOWN 7.16 9800
f: UNKNOWN 7.25 350 UNKNOWN 7.36 9000 UNKNOWN 7.78 66000 12. UNKNOWN 7.89 140
I: UNKNOWN HYDROCARBON 7.98 220 UNKNOWN 8.17 210 UNKNOWN 8.20 180
I: · u"NKNOWN AMINE .. -. -8.42 190
UNKNOWN ----3.47 130 UNKNOWN 8.96 2300 19. UNKNOWN 9.08 130
I: UNKNOWN 9.42 250 UNKNOWN 9.54 170 UNKNOWN 9.68 150 23. UNKNOWN 9.83 160
I: UNKNOWN 10.15 630 UNKNOWN 11.39 410 UNKNOWN 12.04 490 27. UNKNOWN 12.85 150
2 •. 2 .
30 .
Q
=====
NJ
J
J
NJ
J
J
J
J
J
J
J
J
J
J
J
J --
,]'
J
J
J
J
J
J
J
J
J
J
. I
I
FORM I SV-TIC OLM03.0
I 13 EPA SAL'V!PLE NO . SEMIVOLATILE ORGANICS AN~.LYSIS DATA SHEET
·-• Name: PACE ANALYTICAL SERVICES Contract: NS-09
:.,ab Code: PACE Case No. :
1Jrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696334
,ample wt/vol: 965.0 (g/mL) ML Lab File ID: 18017 ,lel: (low/med) LOW
; .roisture:
'.&centrated Extract
·1·ection Volume:
decanted:
Volume:
2.0(uL)
(Y /N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
·. Cleanup: (Y/N) N pH: 7.0
..
CAS NO. COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol . 541-73-1--------1,3-Dich orobenzene 106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2 4-Dichloroohenol -' -120-82-1--------1,2,4-Trichlorobenzene
91-2 o -3 -

-

-

-
-·-.;:::Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
Q
8 J
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 T_T
10 u
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
I
I
I
I
I
I
I
I
I
I
I
·I
I
FORM I SV-1 OLM03.0
40010G I
I
•
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-09 Name: PACE ANALYTICAL SERVICES Contract:
~ab Code: PACE Case No.: SAS No.: SDG No.: 108086
1lrix: ( soil/water) WATER Lab Sample ID: 10696334
3j11ple wt/vol: Lab File ID: 18017
,l,el: (low/med)
; .roisture:
·Acentrated Extract
1iection Volume:
965.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0 ~ Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
( 1) ,I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9-~------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1----~---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphtnalate
206-44-0--------Fluoranthene --· ······ ··--~~~ . 129-00-0--------Pyrene .. ., 85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine 56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 u -~ TT ~u u
10 u
10 u
10 u
10 u
4 JB
10 u
10 u
10 u
10 u
10 u
10 u
10 u
400107
I
OLM03.0
' -i
' I !
I
'1
l
I i l
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
NS-09 Name: PACE ANALYTICAL SERVICES Contract:
,1Code: PACE case No. : SAS No.: SDG No.: 108086
!a ix: (soil/wat:er) WATER
,a[le wt/vol:
,e 1: (low/med)
· 1fisture:
ol:entrated Extract
965.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
ntction Volume:
PC Cleanup: (Y/N) N pH: 7.0
Nlber TICs found: 25
COMPOUND NAME
Lab Sample ID: 10696334
Lab File ID: 18017
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q l:AS NUMBER =~~=========---= =======--==--==-===-======== =====::;:::=: ==-:;;::==-======= ====::; 1 . ': 5 . I:
8.
q t:
12. J: 1 .
.!.O .
ii:
19. 21. 2 .
2 .
23.
2,. 2 .
2 .
27. ~• 30.
I
I
108-88-3
. . .
TOLUENE
UNKNOWN
UNKNOWN ALCOHOL
UNKNOWN SUBSTITUTED BENZENE UNKNOWN SUBSTITUTED BENZENE
UNKNOWN HYDROCARBON
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN HYDROCARBON
UNY.NOW!-! .. ~··· .... .. ...
UNKNOWN . UNKNOWN
UNKNOWN ALCOHOL
UNKNOWN
UNKNOWN HYDROCARBON
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
FORM I SV-TIC
3.09 21 NJ 3.16 5 J 3.89 7 J
3.97 5 J 4.13 3 J 4.28 2 J 4.48 3 J 4.81 200 J 5.70 3 J
6.25 1 J 6.44 4 J
6.71 20 J
6.93 43 J
7.08 4 J
7.57 22 J .. r-; ~~. I • I .t. 2 u
8.04 ,., j" ~
8.32 4 J 8.51 9 J 8.64 4 J 8.72 3 J 8.96 3 J 9.59 10 J 9.80 14 J 12.01 8 J
OLM03.0
I lB EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
,t Name: PACE ANALYTICAL SERVICES NS-10 Contract:
,ab Code: PACE Case No. : SAS No.: SDG No.: 108086
+ix: (soil/water) WATER Lab Sample ID: 10696342
Lab File ID: 18018
ample wt/vol: ;:ll: (low/med)
Moisture:
Jlentrated Extract
.11· ct ion Volume:
950.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
~ Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2aChloro1henol 541-73-1--------1,3-Dich orobenzene 106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitropheno~
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -120-82-1--------1,2,4-Trichlorobenzene ... -·-···· ,, ,._ .. 91-20-3---------Naphthalene
106-47-8--------4-Chloroanii111e
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95~4---------2,4,5-Trichlorophenol
91-58-7~--------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FOR."! I SV -1
Q
7 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
~ --~ l 0 u
10 u -----10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u . ..
10 u
400152
OLM03.0
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-10 lb Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
ftrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696342 Sample wt/vol: 950.0 (g/mL) ML Lab File ID: 18018 rlvel: (low/med) LOW
% Moisture: ___ decanted: (Y/N)
~centrated Extract Volume: l000(uL)
I~ection Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0 31: Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----0 ---N-Nitrosodiphenylamine (1)-101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene
--87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
. -· ---.,., .... ----... 129-00-0--------Pyrene
----85-68-7---------Butylbenzyipncnalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99-2--------Benzo(b)fluoranthene
207-08~9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated tram Diphenylamine
FORM I SV-2
I
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
lO u
10 TT ~
10 u
10 u
10 u
10 u
28 B
10 u
10 u
10 u
10 u
10 u
10 u
10 u
400153
OLM03.0
I lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
NS-10 lb Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 108086 ltrix: (soil/water) WATER
1iimple wt/vol:
rlvel : (low/med)
%-(Moisture:
C .centrated Extract
950.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Il'ection Volume:
3 Cleanup: (Y/N) N pH: 7.0
Imber TICs found: 28
COMPOUND NAME
Lab Sample ID: 10696342
Lab File ID: 18018
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
CONCENTRATION UNITS: (ug/L or ug/L) ug/L ·
RT EST. CONC. Q
JcAS NUMBER ==========-==---=--======================= ;;::======= ==-===:;;::====== ===== 1. 108-88-3 TOLUENE 3.89 21 NJ I: UNKNOWN 4.36 33 J 78-40-0 TRIETHYL PHOSPHATE 5.61 190 NJ UNKNOWN 5.70 44 J 5 . UNKNOWN 6.13 25 J ~: UNKNOWN 6.28 610 J UNKNOWN 6.44 61 J UNKNOWN HYDROCARBON 6.51 31 J i: UNKNOWN 6.90 1200 J UNKNOWN 7.12 49 J 104-68-7 ETHANOL, 2-(2-PHENOXYETHOXY) 7.92 95 NJ 12. 4769-73-7 2-PROPANOL, 1-CHLORO-3-PHENO 8.17 520 NJ I: UNKNOWN 8.23 150 J UNKNOWN HYDROCARBON 8.76 1500 J UNKNOWN 9.03 ··-.. -· . . -.. 22. J . --... ,. 6. -UNF.}TOWN 9.091 ~~,~ ·-1: UNKNOWN HYDROCA . ..'R.BON 9.47 .Lb u -· UNKNOWN 9.60 100 J . UNKNOWN 9.71 42 J 20. UNKNOWN 9.89 24 J 2 •. UNKNOWN HYDROCARBON 10.36 90 J 2 . UNKNOWN 10.55 61 J 23. UNKNOWN 10.66 33 J ~-UNKNOWN 11.81 71 J UNKNOWN HYDROCARBON 11.97 45 J UNKNOWN 12.10 420 J 27. UNKNOWN 15.35 22 J 2,. UNKNOWN 15.67 50 J 2
3 .
I
,,
I
I
FORM I SV-TIC OLM03.0
400154
I lB SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE.NO.
lb Name: PACE ANALYTICAL SERVICES NS-11 Contract:
Lab Code: PACE Case No.:
ttrix: (soil/water) WATER
SAS No.: SDG No. : 108086
Lab Sample ID: 10696359 Sample wt/vol: 930.0 (g/mL) ML Lab File ID: 18019 rlel: (low/med) LOW
?,; Moisture:
clcentrated Extract
Il'ection Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0 3 Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
'--....
I
0
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-9l-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol
-
11
11
11
11
11
· 11
11
11
11
11
11
11
11
11
11
11
11 120-82-1--------1,2,4-Trichlorobenzene ·· ··-····· r1 91-20-3---------Naphthalene
11 106-47-8--------4-ChloroaniTine
11 87-68-3---------Hexachlorobutadiene
11 59-50-7---------4-Chloro-3-methylphenol
11 91-57-6---------2-Methylnaphthalene
11 77-47-4---------Hexachlorocyclopentadiene
11 88-06-2---------2,4,6-Trichlorophenol
--11 95-95~4---------2,4,5-Trichlorophenol
27 91-58-7---------2-Chloronaphthalene
11 88-74-4---------2-Nitroaniline
27 131-11-3----~---Dimethylphthalate
11 208-96-8--------Acena~hthylene
11 606-20-2--------2,6-Dinitrotoluene
11 99-09-2---------3-Nitroaniline
27 83-32-9---------Acenaphthene
11
FORM I SV-1
Q
u u u u u u u u u u u u u u u u u u ., ... ,
u u u u u u u u u u u u u u u
OLM03.0
lC EPA SAMPLE; NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE ANALYTICAL SERVICES Contract:
~ab Code: PACE Case No.:
,J,rix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696359
Lab File ID: 18019 31ple wt/vol: 930.0 (g/mL) ML
, el: (low/med) LOW
;Joisture:
: centrated Extract
:rwection Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
1000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
:~ Cleanup: (Y /N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1----~---4,6-Dinitro-2-methylphenol
86-30-5---------N-Nitrosodiphenhlamine (l)= 101-55-3--------4-Bromophenyl-p enylether 118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
_ .. 7. 0.§..-4.4:::.0 -

-
a-.::-.::---Fl uoraY'.thene ..
129-00-0--------Pyrene
85-68-7-----~---Butylbenzllphthalate
91-94-1---------3,3'-Dich orobenzidine 56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
( 1) -cannot be separated rrom D1phenylam1ne
Q
27 u
27 u
11 u
11 u
11 u
·11 u
11 u
27 u
27 u
11 u
11 u
11 u
27 u
11 u
11 u
11 u
11 u
ll u
11 u
11 u
11 u
11 u
11 u
26 B
11 u
11 u
11 u
11 u
11 u
11 u
11 u
I .. --··------
,g
FORM I SV-2 OLM03.0
D
lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
~ti Name: PACE ANALYTICAL SERVICES Contract: NS-11
~ab Code: PACE Case No.:
,J.rix: (soil/water) WATER
SAS No. : SDG No. : 108086
;lole wt/vol: 930.0 (g/mL) ML
, el: (low/med)
, foisture:
:clcentrated Extract
:raection Volume:
LOW
decanted:
Volume:
2.0(uL)
,~ Cleanup: (Y /N) N
(Y/N)
l000(uL)
pH: 7.0
Lab Sample ID: 10696359
Lab File ID: 18019
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
~er TICs found: 22 CONCENTRATION UNITS: (ug/L or ug/L) ug/L
lAS NUMBER = =====--=--=--
1. -: 5. ~:
I:
12.
I:
16 ..
ft:
I:
23.
I:
27.
2,. 2 .
3 .
I
I
3581-91-7
120-93-4
101-84-8
126-73-8
·-·-. ,_ .. ,_ ..... ······ .
3389-71-7
COMPOUND NAME ---=--=--=--=-============== UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
THIAZOLE, 4,5-DIMETHYL-
2-IMIDAZOLIDINONE
UNKNOWN
DIPHENYL ETHER
UNKNOWN
UNKNOWN
UNKNOWN
PHOSPHORIC ACID TRIBUTYL EST G~.JKNOWN-..
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN SUBSTITUTED BENZENE BICYCLO[2.2.l)HEPTA-2,5-DIEN
FORM I SV-TIC
RT EST. CONC. Q ======== :::;:;:;;:;;:;;:;;::;;:;;;:::::;:;;:;:::::;:::;:::; ===== 3.59 5 J 4.28 8 J 4.43 18 J 4.49 8 J 5.19 58 J 5.86 23 J 5.93 15 J 6.30 4 NJ 6.79 56 NJ 6.98 4 J 7.55 22 NJ 8.37 3 J 8.69 23 J 9.12 4 J 9.21 5 NJ 9.76 4 J 9.89 4 J,
10.19 4 J 10.79 2 J 10.90 2 J 11.37 22 J 11.77 6 NJ
OLM03.0
4co:-:01
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
tJ Name: PACE ANALYTICAL SERVICES NS-15 Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 108086
~rix: (soil/water) WATER Lab Sample ID: 10696367
Simple wt/vol: Lab File ID: 18020
Lll,-e1: (low/med)
'-'1oisture:
:li.centrated Extract
Il'ection Volume:
970.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
; Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
g
n
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol _ 108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120 -82 -1--

-

-

-
----~ 1,.2., .. 4 -Trichlorcbenzene 91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2 4 6-Trichloroohenol --, , -95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniiine
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u v
10 TJ
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
I
I
I ~002.JS
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Name: PACE ANALYTICAL SERVICES NS-15 Contract:
~\l' Code: PACE . Case No. : SAS No.: SDG No.: 108086
11.rix: ( soil/water) WATER Lab Sample ID: 10696367
Lab File ID: 18020 :;lple wt/vol:
, el : (low/med)
'Joisture:
: centrated Extract
·raection Volume:
970.0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
1000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
P' Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
g
R
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene . -
100-01-6--------4-Nitroaniline
534-52-1----c---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene · --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
2 O 6 -44 - O - - -..,.-·""'---~ ... --F,luoranthene
129-00-0--------Pvrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u ., n u .J.U
10 TJ
10 u
10 u
10 u
10 u
10 JB
10 u
10 u
10 u
10 u
10 u
10 u
10 u
I
OLM03.0
I
I i:ioo2.J6
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Name: PACE ANALYTICAL SERVICES Contract: NS-15
·Jab Code: PACE Case No. : SAS No.: SDG No.: 108086 ,Jrix: ( soil/water) WATER
;lole wt/vol:
, el: (low/med)
970.0 (g/mL) ML
LOW
·Joisture:
centrated Extract
decanted: (Y/N)
Volume: l000(uL)
2.0(uL) raection Volume:
P~ Cleanup: (Y/N) N pH: 7.0
Ler TICs found: 30
COMPOUND NAME
Lab Sample ID: 10696367
Lab File ID: 18020
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/L) ug/L
RT EST.
1.0
CONC. ~S NUMBER
= ==-=:;:;::---==--==-=-======================= =;:;:====== ============= 1. UNKNOWN 3. 63 12 I: UNKNOWN 4.12 10 UNKNOWN 4.29 47 UNKNOWN ORGANIC ACID 4.49 9 5 . UNKNOWN HYDROCARBON 4.62 5 I: UNKNOWN HYDROCARBON 4.89 88 UNKNOWN HYDROCARBON 5.14 100 8. UNKNOWN 5.27 5 I: UNKNOWN 5.32 5 UNKNOWN 6.61 4 UNKNOWN 7.31 220 12. UNKNOWN 7.63 190 I: UNKNOWN 7.78 10 UNKNOWN ALCOHOL 7.81 3 UNKNOWN 7.94 3 Hi. tJNKNOWN . _ .. ---· . -. ...... 7.98 7 I: UNKNOWN -8.07 3 UNKNOWN 8.16 5 UNKNOWN 8.36 63 20. UNKNOWN 8.44 38 I: UNKNOWN 8.55 73 UNKNOWN 8.65 15 23. UNKNOWN 8.93 5 2 __ UNKNOWN HYDROCARBON 9.44 27 2 . UNKNOWN 9.53 4 2 . UNKNOWN HYDROCARBON 9.93 200 27. UNKNOWN HYDROCARBON 10.10 47
2, UNKNOWN HYDROCARBON 10.17 20 2 UNKNOWN PHTHALATE 10.62 60 3 . UNKNOWN 10.69 16
Q
=====
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
T u
J
J
J
J
J
J
J
J
J
J
J
J
J.
I
FORM I SV-TIC OLM03.0 I
I 4002.:7
1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
rJ Name: NS-29 PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Mtrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696318
Sample wt/vol: 960.0 (g/mL) ML Lab File ID: 18125
Llel: (low/med) LOW
~ Moisture: ___ decanted: (Y/N)
:lcentrated Extract Volume: l000(uL)
I1jection Volume: 2. 0 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0 ;ii Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -120-82-1--------1 2 4-Trichlorobenzene ,. f I • ·-____ --•• 91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline -
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene 77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
..
FORM I SV-1
Q
1100 E
1700 E
100 u
100 u
100 u
100 u
100 u
100 u
64 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u 1/1(\ TT
166lu
100 u
100 u
100 u
100 u
100 u
100 u
260 u
100 u
260 u
100 u
100 u
100 u
260 u
100 u
OLM03.0
n
I 400780
I lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
rJ Name: NS-29 PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
~Jrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696318
3amole wt/vol: 960.0 (g/mL) ML Lab File ID: 18125 :,1:1, (low/med)
.-Moisture:
:lcentrated Extract
:1·ection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 10.0
1 Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenylamine (1)-101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene . . ,, -.•.. . --. .. ... . .-, .--129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
Q
260 u
260 u 10·0 u
100 u
100 u
100 u
100 u
260 u
260 u
100 u
100 u
100 u
260 u
100 u
100 u
100 u
100 u
J..VV n u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
OLM03.0
I
I 400~81
n 1.F EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
NS-29 ·,I Name: PACE ANALYTICAL SERVICES Contract:
cab Code: PACE Case No. : SAS No.: SDG No.: 1.08086
1-llrix: (soil/water) WATER
,ample wt/vol: 960.0 (g/mL) ML ,Jel: (low/med) LOW
: 11oisture:
:cl::entrated Extract
decanted:
Volume:
2.0(uL) J. ction Volume:
Cleanup: (Y/N) N
N~er TICs found: 29
(Y/N)
1.000 (uL)
pH: 7.0
COMPOUND NAME
Lab Sample ID: 1.069631.8
Lab File ID: 1.81.25
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q IAS NUMBER = ==========--= --=---====================== ======== =-==-::::===::;::;::;;;::; =-=== 1.
I:
5 .
I:
9.
I:
I:
1.6.
I:
20. 1: . 2i. 2 .
2 .
27.
!l
I
I
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID UNKNOWN ORGANIC ACID UNKNOWN ORGANIC ACID UNKNOWN ORGANIC ACID
TJ.N:KNOWN
UNKNOWN
UNKNOWN
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
l..TNKNOWN -·---· .. UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
FORM I SV-TIC
3.63 6000 J 4 . 21. 1.6000 J 4. 41. 1.3000 J 4.49 1.400 J 4.62 2300 J 4.72 92 J 5.01. 5400 J 5.05 62 J
5. 1.4 35 J 5.32 1.1.00 J 5.68 1.1.00 J
5.96 470 J 6.00 28 J 6. 1.2 1.400 J
6 . 31. 1.70 J
----· -6-: 44· • ... 110 I J 6.48 --230 J
6.59 75 J 6.73 630 J 6.90 4400 J 7.66 1.200 J 7. 81. 47 J 8.1.3 180 J 8. 38 22 J 8.56 75 J 8.83 42 J 8.93 78 J 10.74 30 J 11. 38 40 J
OLM03.0
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
·t Name:
.ab Code:
PACE ANALYTICAL SERVICES Contract: NS-29DL
P.11.CE Case No.:
·aljrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696318DL
ample wt/vol: 960.0 (g/mL) ML Lab File ID: 19104
(low/med) LOW
Moisture: ___ decanted: (Y/N)
olentrated Extract Volume: l000(uL)
:1,· ct ion Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
?• Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methvlohenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7-----·---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1----~---bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
Q
1200 D
3100 D
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
I
I
I
I
I
I
I
I
I
I
I
I
I
I 91-20-3---------Naphthalene .. -1000 u --106-47-8--------4-Chlo~oaniline 1000 u 87-68-3---------Hexachlorobutadiene 1000 u 59-50-7---------4-Chloro-3-methylphenol 1000 u 91-57-6---------2-Methylnaphthalene 1000 u 77-47-4---------Hexachlorocyclopentadiene 1000 u 88-06-2---------2,4,6-Trichlorophenol --1000 u 95-95~4---------2,4,5-Trichlorophenol 2600 u 91-58-7---------2-Chloronaphthalene 1000 u 88-74-4---------2-Nitroaniline 2600 u 131-11-3--------Dimethylphthalate
. 1000 u 208-96-8--------Acenaphthylene 1000 u 606-20-2--------2,5-Dinitrotoluene 1000 u 99-09-2---------3-Nitroaniline 2600 u 83-32-9---------Acenaphthene 1000 u
FORM I SV-1
40()332
I
OLM03.0
I lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
~1 Name: PACE ANALYTICAL SERVICES NS-29DL Contract:
~ab Code: PACE Case No.:
·1lrix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ·tD: 10696318DL
3amole wt/vol: 960.0 (g/mL) ML Lab File ID: 19104 ~1:1, (low/med)
'Joisture:
~ centrated Extract
:111ection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
,i,I Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
D
m
( 1)
·I
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate _ 7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6-----~---N-Nitrosodiphenylamine (1)-101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene .. -.... 129-00~0--------Pyrene
.. 85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo{a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo{a)pyrene
193-39-5--------Indeno{l,2,3-cd)pyrene
53-70-3---------Dibenz(~,h)anthracene
191-24-2--------Benzo{g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
2600 u
2600 u 1000 u
1000 u
1000 u 1000 u 1000 u
2600 u
2600 u
1000 u 1000 u
1000 u
2600 u
1000 u 1000 u
1000 u 1000 u ., ",.." u ••·;J..VVV"
1000 T_T
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u ..
OLM03.0
I
I 400333
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
NS-29DL Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 108086
·1lrix: (soil/water) WATER
3i\11ple wt/vol:
:.ll,el: (low/med)
¾ .roisture:
:&centrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
'J. ·ection Volume:
; Cleanup: (Y /N) N pH: 7.0
Lab Sample ID: 10696318DL
Lab File ID: 19104
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
Imber TICs found: 11
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
JcAS NUMBER ==-::===--===--
-·
1.
f:
5 . I: 8.
9. I:
12.
I:
16 ..
I:
20. I· .
23.
I:
27.
I:
I
I
I
3274-29-1
-.
COMPOUND NAME ==-====--=================== UNKNOWN ORGANIC ACID
UNKNOWN
UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN
HEPTANOIC ACID, 2-ETHYL-
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
FORM I SV-TIC
RT EST. CONC. Q ======:;;;:= _:;::::=-====;:;;:==== ===== 4.10 1100 JD 4 .14 320 JD 4.27 4300 JD 4.74 8600 JD 5.10 1400 JD 5.46 360 NJD
5.75 230 JD
6.57 360 JD 6.76 3700 JD
6.94 500 JD 7.46 1700 JD
-, ---. --·-
OLM03.0
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
c.J Name:
c.ab Code:
NS-30 PACE ANALYTICAL SERVICES Contract:
PACE case No.:
~frix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696326
3ample wt/vol: 960.0 (g/mL) ML Lab File ID: 18016 ~lel: (low/med) LOW
; Moisture:
:Jcentrated Extract
:lljection Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
1000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
~• Cleanup: (Y/N) N pH: 7. O
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylpnenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
Q
10 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u u
I
I
I
I
I
I
I
I
120-82-1--------1,2,4-Trichlorobenzene 10 -· -··· ..
I
I
91-20-3---------Naphthalene ----106~47-8----------4-Chloroaniiine
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --95-95~4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
10 u
10 u ..
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
I lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
rt Name: PACE ANALYTICAL SERVICES NS-30 Contract:
Lab Code: PACE
♦rix: (soil/water)
Case No.:
WATER
SAS No.: SDG No.: 108086
Lab Sample "ID: 10696326
Samole wt/vol: 960.0 (g/mL) ML Lab File ID: 18016 LJ:1: (low/med)
t_,ioisture:
:&centrated Extract
r1·ection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
-; Cleanuo: (Y/N) N pH: 7. 0
( 1)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitroohenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylpfithalate
206-44-0--------Fluoranthene
129-00°0---::~--~Pyrene
85-68-7---------Butylbenzrlpntna~ate
91-94-1---------3,3'-Dich orobenzidine 56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phtfialate
117-84-0--------Di-n-octylphthalate -205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 TT u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
i
I
I
I
I
I
I
I
I
I
I
I FORM I SV-2 OLM03.0
I
I 400:-,sg
I lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
NS-30 al Name: PACE ANALYTICAL SERVICES Contract:
alilCode: PACE Case No.: SAS No.: SDG No.: 108086
al-ix: (soil/water) WATER
alle wt/vol:
= 1: (low/med)
l isture:
~ entrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y /N)
l000(uL)
~,ction Volume:
?C Cleanup: (Y/N) N pH: 7.0
~Ler TICs found: 4
JAs NUMBER COMPOUND NAME
= =============
Lab Sample ID: 10696326
Lab File ID: 18016
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q -======-=-=====--=========== ===;;;;==== ==-=========== :;;::==== 1.
I:
5 . I:
8 .
11: 1 .
12.
1,. 1 .
1 .
16.
1,. 1 .
1 .
21. 2 .
2 .
23. ~,
2 .
27. i,
I
I
1707-71-7
--·· .. ··--
ETHYL PYROPHOSPHATE 5.52 3 NJ UNKNOWN 5.82 4 J UNKNOWN 6.35 3 J UNKNOWN HYDROCARBON 8.33 6 J
.
FORM I SV-TIC OLM03.0
I 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
+ame: PACE ANALYTICAL SERVICES Contract: NS-30RE
.b Code: PACE Case No.:
clix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696326RE
.mole wt/vol: 960.0 (g/mL) ML Lab File ID: 18106 Ji, (low/med) LOW
M[' sture:
n ntrated Extract
decanted:
Volume:
:t==tion Volume:
_'l:leanup: (Y/N) Y
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/96
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
pH: 7.0
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlo~ophenol
541-73-1--------1,3-Dichlorobenzene
~06-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7-----"--N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3------00 cNaphthalene ·
106-47-8--------4-Chloroaniiine
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95a4~--------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
• n u .I.V
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0 I
I
I 40037'1
I
rJ
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-30RE Name: PACE ANALYTICAL SERVICES Contract:·
Lab Code: PACE Case No.: SAS No.: SDG No.: 108086
~lrix: (soil/water) WATER Lab Sample ID: 10696326RE
Lab File ID: 18106 3ample wt/vol: ~lel: (low/med)
~.roisture:
:licentrated Extract
Il'ection Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/96
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
; Cleanup: (Y /N) Y pH: 7.0
I
I
I
I
I
I
I
I
I
I
••
I
( 1)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
8 6 -3 0-6 -

-

-

-
-·--

-
-N-Nitrosodiphenylamine ( 1) -101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5-------~-Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0: ~ ~·:·: -~-Py.rene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99~2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM0J.0
I 400375
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
NS-30RE.
Name: PACE ANALYTICAL SERVICES Contract:
~'iii' Code: PACE Case No.: SAS No.: SDG No.: 108086
·1.rix: (soil/water) WATER
:;lple wt/vol:
J el: (low/med)
'Joisture:
: centrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
:1ection Volume:
;pc Cleanup: (Y /N) Y pH: 7.0
Jmber TICs found: S
COMPOUND NAME
Lab Sample ID: 10696326RE
Lab File ID: 18106
Date Received: 06/22/96
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q JCAs NUMBER --=========-----============================ =======:;::: ============= ::;::;::;::;::;
1. I: 4.
5. I:
8 .
I:
12.
I:
16. I: 19.
I:
23.
I:
27.
I:
I
I
I
78-40-0 TRIETHYL
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
PHOSPHATE 5.53 3 NJ
5.83 4 J
6.35 3 J
7.11 3 J
HYDROCARBON 8.33 7 J
' -~-. -· -··· . ·-----. -,,
FORM I SV-TIC OLM03.0
400:176
I 13
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
al Name: PACE ANALYTICAL SERVICES NS-31
Contract:
ai Code: PACE Case No.: SAS No.: SDG No.: 108086
al-ix: (soil/water) WATER Lab Sample ID: 10696300
Lab File ID: 18126 alle wt/vol:
e 1: (low/med)
l isture:
J entrated Extract
:1.lction Volume: ·
970.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 10.0
?C Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Mechylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5----~---4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitroohenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
!20-82-1--------1,2,4-Trichlcrobenzene---·-· ...
91-20-3---------Naohthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-95-8--------Acenaphthylene
605-20-2--------2,5-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
?ORM I SV-1
Q
980 E
1200 E
100 u
100 u
100 u
100 u
100 u
100 u
100 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 U·
100 u
100 u
100 u
100 u
100 u
100 u
100 u
260 u
100 u
260 u
100 u
100 u
100 u
250 u
100 u
OLM03.0
I lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
,J Name: PACE ANALYTICAL SERVICES NS-31 Contract:
,aj Code: PACE Case No.: SAS No.: SDG No.: 108086 ,air ix: ( soil/water) WATER Lab Sample ID: 10696300
'Tle
,ei:l:
wt/vol:
(low/med)
970.0 (g/mL) ML
LOW
Lab File ID: 18126
fJisture:
o~entrated
decanted:
Extract Volume:
(Y/N)
1000 (uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 10.0 ntction Volume:
PC Cleanup: (Y/N) N
2.0(uL)
pH: 7. 0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenyletfier
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1----~---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine {1)-101-55-3--------4-Bromophenyl-phenylether -118-74-1--------Hexachlorobenzene --87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
260
260
100
100
100
100
100
260
260
100
100
100
260
100
100
100
100
I
I
I
I
I
I
I
I
I
206-44-0--------Flucranthene .. ·---···----"·•--1ou·
I
I
129-00-0--------Pvrene
85-68-7---------Butylbenzylpfitfialate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene . 117-81-7--------bis(2-Etfiylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
100
100
100
100
100
38
100
100
100
100
100
100
100
Q
u u u u u u u u u u u
u u
u u u
u u-
TT u·
u
u u
u
JB u
u u u u u
u
OLM03.0
I lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I TENTATIVELY IDENTIFIED COMPOUNDS
a Name: PACE ANALYTICAL SERVICES Contract:
NS-31
al' Code: PACE Case No.: SAS No.: SDG No.: 108086
a ix: (soil/water) WATER ctrle wt/vol:
=vel: (low/med)
970.0 (g/rnL) ML
LOW
fisture:
:Jncentrated
decanted:
Extract Volume:
~fction Volume: 2.0(uL)
(Y/N)
l000(uL)
?C Cleanup: (Y/N) N pH: 7.0
~l\ber TICs found: 24
s NUMBER COMPOUND NAME
Lab Sample ID: 10696300
Lab File ID: 18126
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/01/98
Dilution Factor: 10.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q ----------------========-------------======= =====::::;;:;:;; ========:;;:::::;;:::;::;;: :::::::::::;;:;:;
I: UNKNOWN ORGANIC ACID 3.92 390 J
UNKNOWN ORGANIC ACID 4.21 46 J
UNKNOWN ORGANIC ACID 4.24 40 J
4. UNKNOWN ORGANIC ACID '1.35 54 J
I: UNKNOWN ORGANIC ACID 4.48 44 J
UNKNOWN ORGANIC ACID 4.61 34 J
UNKNOWN 4.92 700 J
8. UNKNOWN ORGANIC ACID 5.28 130 J
I: UNKNOWN ORGANIC ACID 5.65 24 J
UNKNOWN 5.90 48 J
UNKNOWN 6.08 180 J
12. UNKNOWN 6.47 76 J I: UNKNOWN 6.57 56 J
UNKNOWN 6.71 400 J
15. UNKNOWN 7.08 2100 J
i: UNKNOWN HYDROCARBON 7.S9 .. ~---... . .. ·-340 J
UNKNOWN 7.99 52 ~ U·
UNKNOWN 8.06 56 J
19. UNKNOWN 8.10 22 J
I: UNKNOWN ALCOHOL 8.14 50 J
UNKNOWN 8.32 48 J UNKNOWN 8.81 26 J
23. 17233-.71-5 HEXATHIEPANE 10.13 23 NJ I: UNKNOWN 10.73 24 J
26.
i:
30.
I
FORM I SV-TIC OLM03.0
I
I
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
-al Name: PACE ANALYTICAL SERVICES NS-31DL Contract:
,ab Code: P.l\.CE Case No. : SAS No.: SDG No.: 108086 ·aJ-ix: (soil/water) WATER Lab Sample ID: 10696300DL
a/ilfle wt/vol: Lab File ID: 19103
e.l: (low/med)
970. 0 (g/mL) ML
LOW
decanted:
[
isture:
o entrated Extract Volume:
(Y /N)
l000(uL)
n,· ct ion Volume: 2.0(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
? Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -120-82-1~-------l,2,4-Trichlorobenzene
·91-20~3--:------Naphthalene
106-47-8--------4-Chloroaniiine
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
·88-06-2---------2,4,6-Trichlorophenol --95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphchene
FORM I SV-1
Q
1300 D
2700 D
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
120 DJ
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 TT c.·
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
2600 u
1000 u
2600 u
1000 u
1000 u
1000 u
2600 u
1000 u
·•
OLM03.0
I lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-31DL Name: PACE ANALYTICAL SERVICES Contract:
·1Code: PACE Case No. : SAS No.: SDG No.: 108086
ix: (soil/water) WATER Lab Sample ID: 10696300DL
Lab File ID: 19103 alle wt/vol:
e 1: (low/med)
tl'isture:
~'=entrated Extract
n,ction Volume:
970. 0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
? Cleanup: (Y/N) N pH: 7. 0
I
I
I
I
I
I
I
I
I
I I (1)
I
I
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1----c---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0-~ ---- ---Fluvranthene
129-00-0--------Pvrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated rrom D1phenylam1ne
E'ORM I SV-2
Q
2600 u
2600 u
1000 u
1000 u
1000 u
1000 u
1000 u
2600 u
2600 u
1000 u
1000 u
1000 u
2600 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
4004.:6
OLM03.0
I
.J
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
NS-31DL Name: PACE ANALYTICAL SERVICES Contract:
'2j Code: PACE Case No. : SAS No.: SDG No.: 108086
,alrix: (soil/water) WATER 'Ile wt/vol:
,eel: (low/med)
. risture:
.oncentrated Extract
ntction Volume:
970.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
PC Cleanup: (Y/N) N pH: 7.0
NLer TICs found: 11
IAS NUMBER COMPOUND NAME
Lab Sample ID: 10696300DL
Lab File ID: 19103
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 07/10/98
Dilution Factor: 100.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q =--======-====--=======-==================== ======== ============= ===== 1. ~:
I:
8.
i:
12.
I:
16. I:
19.
I:
23.
2,. 2 .
2 .
27.
2 •. 2 .
30.
·•
I
I
UNKNOWN ORGANIC ACID UNKNOWN ORGANIC ACID UNKNOWN ORGANIC ACID
UNKNOWN ORGANIC ACID
UNKNOWN
UNKNOWN ORGANIC ACID
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
... -· •... .. -~ -· .. , . ----
.
FORM I SV-TIC
3.55 3800 JD 3.72 3300 JD 4.05 2500 JD
4.28 780 JD 5.08 1100 JD 5.45 350 JD 6. 35 340 JD 6.57 420 JD 6.76 710 JD
6.95 400 JD 7.47 460 JD
i
OLM03.0
4004:::,7
I 13 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
al Name:
.ab Code:
NS-32 PACE ANALYTICAL SERVICES Contract:
PACE
·al-ix: (soil/water)
Case No.:
WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696375
ample wt/vol: 960.0 (g /mL) ML Lab File ID: 18021 ell: (low/med)
l isture:
~ entrated Extract
:1wction Volume:
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
?~Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
••
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloroohenol
541-73-1--------1,3-Dichiorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitroohen6I
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3-=-=~-:=-Na~hth~lene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10,U
1olu
lU 0
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
I
OLM03.0
I lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
.1 Name: PACE ANALYTICAL SERVICES NS-32
Contract:
,ab Code: PACE Case No. :
!Jrix: ( soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: 10696375
Lab File ID: 18021 ;Jole wt/vol:
, el: (low/med)
'Joisture:
: centrated Extract
·1ction Volume:
960.0 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
·P Cleanup, (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
..
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1----~---4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene ..
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl}phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo{b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd}pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
7 JB
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
I
I 4004£4
I lF SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
NS-32 Name: PACE ANALYTICAL SERVICES Contract:
Lif Code: PACE Case No. : SAS No. : SDG No. : 108086
11:rix: (soil/water) WATER 31ole wt/vol:
~ el: (low/med)
~,oisture:
: centrated Extract
960.0 (g/mL) ML
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
l000(uL)
election Volume:
; Cleanup: (Y/N) N pH: 7.0
Imber TICs found: 6
JcAs NUMBER COMPOUND NAME ===::;;:=====-----
Lab Sample ID: 10696375
Lab File ID: 18021
Date Received: 06/22/98
Date Extracted:06/23/98
Date Analyzed: 06/29/98
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q -============-====::;;::========= ======== ----==-====== ===== 1. UNKNOWN
.2. 3 .
4.
5.
.6. 7.
8 .
• 9. 0.
1.
12.
I:
1.6.
I:
at
23.
I:
27.
I:
I
I
I
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
UNKNOWN
3.39 4 J 3. 46 3 J 3.59 4 J 4.28 8 J HYDROCARBON 4. 36 2 J HYDROCARBON 4.48 5 J
. ....
-
-
FORM I SV-TIC OLM03.0
40046S
I
I
I
I
I Method Blank
I
I
I
I
I
I
I
·I-. . .. -__ ., _____ , --··
I
I
I
...
I
I 401?.96
I 13 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
al Name: PACE ANALYTICAL SERVICES Contract:
.. !,BLK13739
,ab Code: PACE Case No. :
alix: (soil/water) WATER
SAS No.: SDG No.: 108086
alle wt/vol: 1000 (g/mL) ML
LOW
Lab Sample ID: SBLK13739
Lab File ID: 18103
e l: (low/med) Date Received:
l isture:
~ entrated Extract
n,ction Volume:
decanted:
Volume:
2.0(uL)
(Y/N)
1000 (uL)
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
? Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95~57-8---------2-Chlorochenol
541-73-1--------1,3-Dichiorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---~-----2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7----~---N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-NitrochenoL
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-T:cichlorober..zer..e,
91-20-3---------Naphthalene
106-47~8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocyclopentadiene
88-06~2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
I
I·
I
I 40179?
I lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
al Name: . PACE ANALYTICAL SERVICES
SBLK13739
Contract:
ab Code: PACE Case No.:
aJix: (soil/water) WATER
SAS No.: SDG No.: 108086
Lab Sample ID: SBLK13739
ample wt/vol: 1000 (g/mL) ML Lab File ID: 18103 ell: (low/med) LOW Date Received:
Moisture: ___ decanted: (Y/N)
?lentrated Extract Volume: l000(uL)
:11· ct ion Volume: 2.0(uL)
Date Extracted:06/23/98
Date Analyzed: 06/30/98
Dilution Factor: 1.0
? Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-oB~9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
I·
I
I
FORM I SV-2
·-•· .... .. , ' -
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
.... ·:1. o· u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u •
OLM03.0
I
lF I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
.i Name: PACE ANALYTICAL SERVICES Contract: SBLK13739
Jab Code: PACE Case No. :
:Jrix: (soil/water) WATER
SAS No.: SDG No.: 108086
;Ile wt/vol:
l: (low/med)
jtiisture:
ol::entrated Extract
1000 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Lab Sample ID: SBLK13739
Lab File ID: 18103
Date Received:
Date Extracted:06/23/98
Date Analyzed: 06/3_0/98
Dilution Factor: 1.0 n,ction Volume:
P Cleanup: (Y/N) N pH: 7.0
NLer TICs found: 0
COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/L) ug/L
RT EST. CONC. Q IAS NUMBER
= ============= ============================ ======::= --====::;::====== ===== 1.
I:
5 .
~:
9. I:
12.
I:
16. -.. --· .... ;_,.. ----.. -.... ..
I I:
20. I:
23.
I:
27.
2,. 2 .
3 .
•· FORM I SV-TIC OLM03.0
I
I 40113'.J
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting F onn
Jab Sample ID: ____ 10_6_9_6_44_1 __ _ · Client ID: EX-01
f/j'1atrix:
llveight:
I
I
I
I
I
I
I
I
I
:orents:
Water
50 ----
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units:
Volume:
I WU
Mass
' 308.2
206.8
189.0
493.4
313.0
226.5
370.6
267.7
228.6
324.8
271.4
220.4
279.1
257.6
253.7
231.6
766.5
196.0
328.1
589
190.9
292.4
213.9
zel,n Generator Version 1.00
ppb
50
I IDL I
' ' 86
4.232
1.3
2
1
0.263
84
4
7
4
36
2.518
48
6
0.0613
14
766
4.316
2
124
3.311
5
5
Prep Date: 6/23/98
Percent Moisture:
Report
I I I Limit Cone Q DF
' ' ' 300 86 u 1
5 4.2 u I
5 IJ u ·>
200 137 J 1
5 I u 1
0.5 0.26' u I
250 67500 1
10 4.8 J 1
so 11.3 J 1
20 6.8 J 1
100 36 u I
3 2.5 u 1
200 9340 1
15 237 1
0.2 0.095 J 1
40 14 u I
2500 1740 J 1
5 4.3 u I
10 2 u !
500 9420 1
10 3.3 u 1
15 5 u 1
20 5 u 1
Prep Batch: 13749 ICP
I Instr I
Anal Anal I
Date . Time
' ' ' ' ICP 7/15/98 8:38
ICPST 7/15/98 9:39
ICPST 7/15/98 9:39
ICP 7/15/98 8:38,
ICP 7/15/98 8:38
ICPST 7/15/98 9:39
ICP 7/15/98 8:38
ICP 7/15/98 8:38
ICP 7/15/98 8:38
ICP 7/15/98 8:38
ICP 7/15/98 8:38
ICPST 7/15/98 9:39
ICP 7/15/98 8:38
ICP 7/15/98 8:38
CVAA 7/15/98 16:43
ICP 7/15/98 8:38
ICP 7/15/98 8:38
ICPST 7/15/98 9:39
ICP 7/15/98 ... 8:38
Tr-D 7/15/98 8:38 ·~·
ICPST 7/15/98 9:39
ICP 7/15/98 8:38
ICP 7/15/98 8:38
800G17
Form ! Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Fonn
lab Sample ID: ____ 10_6_9_6_45_8 __ _ Client ID: EX-02
Matrix: Water leig~t= __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
I·'
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Units: ppb
Volume: 50
WU I Mass IDL
308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 ' '
226.5, 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 J6
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.l 2
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I
Report
I Limit Cone 0 DF
' ' ' 300 86 u I
5 4.2 u I
5 1.3 u . I
200 1130 1
5 1 u I
0.5 0.26" u 1
250 324000 1
10 4.2 J 1
50 7 u I
20 4 u 1
100 13800 1
3 2.5 u 1
200 89800 1
15 12100 1
0.2 0.14 J 1
40 14 u 1
2500 3120 1
5 4.4 J 1
10 2 u l
500 79900 l
10 3.3 u I
15 7.6 J 1
20 5 u 1
Prep Batch: 13749 ICP
Anal Anal
Instr Date Time
' ' ' ICP 7/15/98 8:42
ICPST 7/15/98 9:43
ICPST 7/15/98 9:43
ICP 7/15/98 8:42
ICP 7/15/98 8:42
ICPST 7/15/98 9:43
ICP 7/15/98 8:42
ICP 7/15/98 8:42
ICP 7/15/98 8:42
ICP 7/15/98 8:42
ICP. 7/15/98 8:42
ICPST 7/15/98 9:43
ICP 7/15/98 8:42
ICP 7/15/98 8:42
CVAA 7/15/98 16:48
ICP 7/15/98 8:42
ICP 7/15/98 8:42
ICPST 7/15/98 9:43
ICP ....... . .7/15/98. . 8:42
ICP 7/15/98 8:42
ICPST 7/15/98 9:43
ICP 7/15/98 8:42
ICP 7/15/98 8:42
800018
:omments: ___________________________________ _
.e, Generator Version 1.00 Form I Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
J-ab Sample ID: ____ 10_6_9_6_46_6 __ _ Client ID: EX-03
Matrix: Water
Leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
I.··
I
Element
Alwninwn
Antimony
Ars~nic
Barium
Berylliwn
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver.
Sodium
Thallium
Vanadium
Zinc
Units: ppb
Volume: 50
I
WU
Mass IDL
' ' 308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 1
226.5 0.263
370.6 84
267.7 4·
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.3678
231.6 14
766.5 766
196.0 4.316
328.1 2
589 124
190.9 3 .3 1 1
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report I I Limit Cone Q DF
' ' ' ' 300 86 u I
5 4.2 u I
5 1.3 u -,
200 677 1
5 I u 1
0.5 0.26 u 1
250 217000 1
10 8.2 J 1
50 7 u I
20 4 u I
100 .1100 1
3 2.5 u I
200 33200 1
15 4850 1
1.2 0.49 J 1
40 14 u I
2500 3890 1
5 4.3 u 1
10 2 u 1
500 58000 ' •
10 3.3 u 1
15 5 u I
20 5 u 1
Prep Batch: 13749 ICP
I Instr I Anal
I
Anal
Date Time
' ' ' ICP 7/15/98 8:46
ICPST 7/15/98 9:48
ICPST 7/15/98 9:48
ICP 7/15/98 8:46.
ICP 7/15/98 8:46
ICPST 7/15/98 9:48
ICP 7/15/98 8:46
ICP 7/15/98 8:46
ICP 7/15/98 8:46
ICP 7/15/98 8:46
ICP 7/15/98 8:46
!CPST 7/15/98 9:48
ICP 7/15/98 8:46
ICP 7/15/98 8:46
CVAA 7/15/98 16:50
!CP 7/15/98 8:46
ICP 7/15/98 8:46
ICPST 7/15/98 9:48
rrp "1/1t:/no 8:46 1·~ II i..J/70
,rn "'f/1/!.'lfl~ 8:46 ·~· II .J..:J/ ::,o
ICPST 7/15/98 9:48
!CP 7/15/98 8:46
ICP 7/15/98 8:46
800G19
:ornments: ------------------------'--------------:elrt Generator Version 1.00 Farm J Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
Jab Sample ID: ____ I 0_6_9_6_47_4 __ _ Client ID: DUPLICATE
l',,Iatrix:
8,veight:
I
I
I
I
I
I
I
I
I
I
I
I
I,.'
I
Water Units:
50 Volume: ----
I
WL/
Element Mass
' Alwninum 308.2
Antimony 206.8
Arsenic 189.0
Barium 493.4
Beryllium 313.0
Cadmium 226.5
Calcium 370.6
Chromium 267.7
Cobalt . 228.6
Copper 324.8
Iron 271.4
Lead 220.4
Magnesium 279.1
Manganese 257.6
Mercury 253.7
Nickel 231.6
Potassium 766.5
Selenium 196.0
Sil"er. 328.l
Sodium 589
Thallium 190.9
Vanadium 292.4
Zinc 213.9
:lments:
z rt Generator Version 1.00
ppb
50
IDL I
' ' 86
4.232
1.3
2
I
0.263
84
4
7
4
36
2.518
48
6
0.0613
14
766
4.316
2
124
3.311
5
5
Prep Date: 6/23/98 Prep Batch: 13749 ICP
Percent Moisture:
Report
I I I I Instr I Anal
I
Anal
Limit Cone Q DF Date Time
' ' ' ' ' ' ' 300 86 u I ICP 7/15/98 8:50
5 4.2 u I ICPST 7/15/98 9:52
5 1.3 u . I· ICPST 7/15/98 9:52
200 675 1 ICP 7/15/98 8:50
5 I u I ICP 7/15/98 8:50
0.5 0.26 u I ICPST 7/15/98 9:52
250 211000 1 ICP 7/15/98 8:50
10 8.3 J 1 ICP 7/15/98 8:50
50 7 u I ICP 7/15/98 8:50
20 4 u I ICP 7/15/98 8:50
100 . 592 1 ICP 7/15/98 8:50
3 2.5 u I ICPST 7/15/98 9:52
200 30600 1 ICP 7/15/98 8:50
15 4500 1 ICP 7/15/98 8:50
0.2 0.1 J 1 CVAA 7/15/98 16:52
40 14 u l ICP 7/15/98 8:50
2500 3430 1 ICP 7/15/98 8:50
5 4.3 u l ICPST 7/15/98 9:52
!O 2 u l ICP 7/15/93 8:50
500 57100 ' ICP 7/15/98 8:50 ' 10 3.3 u I ICPST 7/15/98 9:52
15 5 u I ICP 7/15/98 8:50
20 5 u I ICP 7/15/98 8:50
800020
Farm 1 Eq~ivalent
I
'ample Results
Pace Analytical Services
Metals Data Reporting Form
Jab Sample ID: ____ I 0_6_9_6_4_82 __ _ Client ID: EX-04
Matrix: Water Units:
Leight: __ 5_0 __
Volume:
I I
WL/
Element Mass ,
I Aluminum 308.2
Antimony 206.8
Arsenic 189.0 I Barium 493.-l
Beryllium 313.0
I Cadmium 226.5
Calcium 370.6
Chromium 267.7
I Cobalt 228.6
Copper 324.8
Iron 271.-l
Lead 220.4
Magnesium 279.1
Manganese 257.6
Mercury 253.7
Nickel 231.6
Potassium 766.5
Selenium 196.0
Silver 328.l
I
I
I
I
I
I
I , ..
....... ·-.
Sodium 589
Thallium 190.9
Vanadium 292.4
Zinc 213.9
I
ppb
50
I IDL ,
86
4.232
1.3
2
I
0.263
84
4
7
4
36
2.518
48
6
0.0613
14
766
4.316
2
124
3.311
5
5
Prep Date: 6/23/98
Percent Moisture:
I Report
I I I Limit Cone Q DF , , , ,
300 86 u I
5 4.2 u I
5 1.3 u . L
200 36 J 1
5 I u I
0.5 0.26 u I
250 112000 1
10 4.1 J 1
so 10.6 J 1
20 4 u I
100 12000 1
3 2.5 u I
200 32700 1
15 4130 1
0.2 0.11 J 1
40 14 u I
2500 2480 J 1
5 4.3 u I
10 2 u I
500 12000 1
10 3.3 u I
15 5 u I
20 5 u l
Prep Batch: 13749 ICP
I Instr I
Anal I Anal
Date Time
' ' ,
ICP 7/15/98 8:54
ICPST 7/15/98 9:57
ICPST 7/15/98 9:57
ICP 7/15/98 8:54.
ICF 7/15/98 8:54
ICPST 7/15/98 9:57
ICP 7/15/98 8:54
ICP 7/15/98 8:54
ICP 7/15/98 8:54
ICP 7/15/98 8:54
ICP 7/15/98 8:54
ICPST 7/15/98 9:57
ICP 7/15/98 8:54
ICP 7/15/98 8:54
CVAA 7/15/98 16:35
ICP 7/15/98 8:54
ICP 7/15/98 8:54
ICPST 7/15/98 9:57
ICP 7/15/98 8:54
l1cP 111519s I I 8:54
ICPST 7/15/98 9:57
ICP 7/15/98 8:54
ICP 7/15/98 8:54
800021
:amments: ------------------------------------
'.e. Generator Version 1.00 Form I Equivalent
I
I
Sample Results
Pace Analytical Services
:t-.1etals Data Reµorting Form .
I Lab Sample ID: 10735199 Client ID: EX-04 DUPLICATE ---------I Matrix: __ W_a_te_r_
Weight: 50
I
I
I
I
I
·•
I
I
I
I
I
I
I\.-•
I
----
Element
' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Cents:
, ort Generator Version 1.00
Units: ppb
Volume: 50
WU
I Mass IDL
' 308,2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 I
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.l 48
257.6 6
231.6 14
766.5 766
196.0 4.316
328.l 2
589 i24
190.9 3.311
292.4 5
213.9 5
I
'
Prep Date: 7/13/98 Prep Batch: 13749 ICP
Percent Moisture:
Report
I I I Instr I
Anal i Anal Limit Cone Q DF Date Time
' ' ' ' ' ' 300 86 u I ICP 7/14/98 16:25
5 4.2 u I ICPST 7/14/98 12:12
5 1.3 u . I ICPST 7/14/98 12:12
200 · 36.4 J 1 ICP 7/14/98 16:25
5 I u I ICP 7/14/98 16:25
0.5 0.26 u I ICPST 7/14/98 12:12
250 115000 1 ICP 7/14/98 16:25
10 4.1 J 1 ICP 7/14/98 16:25
so 10.3 J l ICP 7/14/98 16:25
20 4 u I ICP 7/14/98 16:25
100 12900 1 ICP 7/14/98 16:25
3 2.5 u I ICPST 7/14/98 12:12
200 33300 1 ICP 7/14/98 16:25
15 4270 1 ICP 7/14/98 16:25
40 17.6 J 1 ICP 7/14/98 16:25
2500 3230 1 ICP 7/14/98 16:25
5 4.3 u I ICPST 7/14/98 12:12
10 2 u 1 ICP 7/14/98 16:25
500 12600 1 jlCP 7/14/98 · 16,25 · ·
10 3.9 J 1 ICPST 7/14/98 12:12
15 14.1 J 1 ICP 7/14/98 16:25
20 5 u I ICP 7/14/98 16:25
E000~2
Form j Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
ILab Sample ID: ____ 10_6_9_6_38_3 __ _ Client ID: EX-05
Matrix: Water
Leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
•· ,'
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver . -.. ··--·
Sodium
Thallium
Vanadium
Zinc
Units:
Volume:
I
WL/
Mass
' 308.2
206.3
189.0
493.4
313.0
226.5
370.6
267.7
228.6
324.8
271.4
220.4
279.1
257.6
253.7
231.6
766.5
196.0
328.l ..
589
190.9
292.4
213.9
1
::1omments: _
I cl. rt Generator Version l.00
ppb
50
I IDL
'
3440
4.232
1.3
80
40
0.263
3360
160.
280
160
1440
2.518
1920
240
0.0613
560
30640
4.316
80
4960
3.311
200
200
Prep Date: 6/23/98
Percent Moisture:
I
Report I I I Limit Cone 0 DF
' ' 12000 3440 u 40
5 4.2 u I
5 1.3 u . I
8000 540 J 40
200 40 u 40
0.5 8.9 1
10000 2430000 40
400 160 u 40
2000 3030 40
800 632 J 40
4000 .Z680 J 40
3 7.7 1
8000 1230000 40
600 255000 40
0.2 0.061 u I
1600 960 J 40
100000 30600 u 40
5 66.9 1
400 80 TJ 40
20000 9360000 40
10 15.1 1
600 200 u 40
800 200 u 40
Prep Batch: 13749 ICP
I Instr I Anal
I Anal I
Date Time
' ' ' ' ICP 7/15/98 8:23
ICPST 7/14/98 l l :21
ICPST 7/14/98 11 :2 I
ICP 7/15/98 8:23
ICP 7115198 8:23
ICPST 7/14/98 11:21
ICP 7/15/98 8:23
ICP 7/15/98 8:23
ICP 7/15/98 8:23
ICP 7/15/98 8:23
ICP 7/15/98 8:23
ICPST 7/14/98 11:21
ICP 7/15/98 8:23
ICP 7/15/98 8:23
CVAA 6/23/98 13:51
ICP 7/15/98 8:23
ICP 7/15/98 8:23
ICPST 7/14/98 11:21
Tr? 7/15/98 8:23 Ii~~ I 7/15/98 8:23.
ICPST 7/14/98 11:21
ICP 7/15/98 8:23
ICP 7/15/98 8:23
EOOC11
Form I Equivalent
I
I
Sample Results lab Sample ID: 10696391
Pace Analytical Services
Metals Data Reporting Form
Client ID: EX-06 ---------
lffatrix:
~eight:
I
I
I
I
I
I
I
I
-···.
I
I
Water
50 ----
Element
' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver .....
Sodium
Thallium
Vanadium
Zinc
=cents:
R art Generator Version 1.00
Units: ppb
Volume: 50
WL/
I I Mass IDL
308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 I
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 -36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.l 2
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
Report
I I I Limit Cone 0 DF
' ' 300 86 u I
5 4.2 u I
5 1.3 u . I·
200 90.3 J 1
5 I u I
0.5 0.26 u I
250 40500 1
10 4 u I
50 7 u I
20 4 u I
100 .3910 1
3 2.5 u I
200 19100 I
15 3170 1
0.2 0.061 u l
40 14 u l
2500 1820 J I
5 4.3 u l
10 2 u !
500 127000 1
10 3.3 u I
15 9.7 J I
20 5 u l
Prep Batch: 13749 ICP
I I
Anal l Anal
Instr Date Time
' ' ICP 7/14/98 15:45
ICPST 7/14/98 11:26
ICPST 7/14/98 11 :26
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICPST 7/14/98 I 1:26
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICPST 7/14/98 11 :26
ICP 7/14/98 15:45
ICP 7/14/98 15:45
CVAA 6/23/98 18:53
ICP 7/14/98 15:45
ICP 7/14/98 15:45
ICPST 7/14/98 11 :26
!CP 7/14/98 15:45
!CP 7/14/98 15:45
ICPST 7/14/98 11:26
ICP 7/14/98 15:45
ICP 7/14/98 15:45
800012
F onn I Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
lab Sample ID: ____ 10_6_9_6_40_9 __ _ Client ID: EX-07
Matrix: Water
leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
R
I
I
I·'
I
I Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt .
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Units: ppb
Volume: 50
WU
I Mass IDL
' 308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 1
226.5 0.263
370.6 84
267.7 4
223.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.1 2 -·. .
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report
I I I Limit Cone Q DF
' ' ' 300 86 u 1
5 4.2 u 1
5 1.3 u • ].
200 248 1
5 1 u 1
0.5 0.26. u 1
250 562000 1
10 15.4 1
50 7 u 1
20 4 u 1
100 . _9400 1
3 2.5 u 1
200 228000 1
15 26200 1
0.2 0.061 u 1
40 14 u 1
2500 3180 1
5 8.2 I
10 2 u 1 ..
500 126000 l
10 4.7 J 1
15 8.6 J 1
20 6.7 J 1
Prep Batch: 13749 ICP
I Instr
Anal
I Anal I
Date Time
' ' '
ICP 7/14/98 15:49
ICPST 7/14/98 11:30
ICPST 7/14/98 11:30
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICPST 7/14/98 11:30
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICPST 7/14/98 11:30
ICP 7/14/98 15:49
ICP 7/14/98 15:49
CVAA 6/23/98 18:55
ICP 7/14/98 15:49
ICP 7/14/98 15:49
ICPST 7/14/98 11:30
1CP 7/14/9R 15:49
ICP 7/14/9~ 15:49
ICPST 7/14/98 11:30
ICP 7/14/98 15:49
ICP 7/14/98 15:49
800013
omments: ___________________________________ _ .el Generator Version 1.00 Farm I Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
lab Sample ID: ____ l 0_6_9_6_4_1 -_, __ _ Client ID: EX-08
lfatrix:
~eight:
I
I
I
I
I
I
I
I
I
I
I
I
Water
50 ----
Element
' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt.
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver:_ .. ___
Sodium
Thallium
Vanadium
Zinc
Units:
Volume:
I
WL/
Mass
' 308.2
206.8
189.0
493.4
313.0
226.5
370.6
267.7
228.6
324.8
271.-1
220.4
279.1
257.6
253.7
231.6
766.5
196.0
328.l ... -
589
190.9
292.4
213.9
:Ients:
cl rt Generator Version 1.00
ppb
50
I IDL
'
34-10
4.232
l.3
80
40
0.263
3360
160
280
160
1440
2.518
1920
240
0.3678
560
30640
4.316
. ·-80
4960
3.311
200
200
Prep Date: 6/23/98
Percent Moisture:
I
Report
I I Limit Cone 0 DF
' ' ' 12000 83300 40
5 4.2 u l
5 l.3 u .,
8000 80 u 40
200 40 u 40
0.5 7.5 I
10000 748000 40
400 160 u 40
2000 7730 40
800 1090 40
4000 25600 40
3 11.8 1
8000 58-1000 40
600 311000 40
1.2 0.92 J I
1600 1330 J 40
100000 30600 u 40
5 78.7 I
400 80 u 40
20000 6510000 40
10 38 I
600 200 u 40
800 1540 40
Prep Batch: 13749 ICP
I
Anal l Anal
Instr Date Time
' ' ' ICP 7/15/98 8:27
ICPST 7/14/98 11 :35
ICPST 7/14/98 11 :35
ICP 7/15/98 8:27.
iCP 7/15/98 8:27
ICPST 7/14/98 11:35
ICP 7/15/98 8:27
ICP 7/15/98 8:27
ICP 7/15/98 8:27
ICP 7/15/98 8:27
ICP 7/15/98 8:27
ICPST 7/14/98 11:35
ICP 7/15/98 8:27
ICP 7/15/98 8:27
CVAA 7/15/98 16:37
ICP 7/15/98 8:27
!CP 7/15/98 8:27
ICPST 7/14/98 11:35
TCP 7/15/98 8:27
lrcP 7/15/98 8:27
ICPST 7/14/98 11:35
!CP 7/15/98 8:27
ICP 7/15/98 8:27
SOOG1'1
Form I Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
ILab Sample ID: ____ 10_6_9_6_4_2)_-__ _ Client ID: EX-09
Matrix: Water
Leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
Element
Aluminum
Antimony
Arsenic
Barium
Jleryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Pocassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Units: ppb
Volume: 50
WU
I Mass IDL
' 308.2 3440
206.8 4.232
189.0 1.3
493.4 80
313.0 40
226.5 0.263
370.6 3360
267.7 160
228.6 280
324.8 160
271.4 1440
220.4 2.518
279.1 1920
257.6 240
253.7 0.0613
231.6 560
766.5 30640
196.0 4.316
328.1 80
589 4960
190.9 3.311
292.4 200
213.9 200
Prep Date: 6/23/98
Percent Moisture:
I
Report
I I I Limit Cone 0 DF
' ' ' ' 12000 110000 40
5 4.2 u 1
5 1.3 u . 1
8000 80 u 40
200 46.8 J 40
0.5 1.9 1
10000 510000 40
400 160 . u 40
2000 6590 40
800 1110 40
4000 _26100 40
3 5.8 1
8000 152000 40
600 178000 40
0.2 0.22 1
1600 940 J 40
100000 30600 u 40
5 43 1
400 80 •-·--u 40.
20000 6790000 40
10 17.7 1
600 200 u 40
800 2450 40
Prep Batch: 13749 ICP
I I
Anal I Anal
Instr Date Time
' ' ' ICP 7/15/98 8:31
ICPST 7/14/98 11:40
ICPST 7/14/98 11 :40
ICP 7/15/98 8:31.
ICP 7/15/98 8:31
ICPST 7/14/98 11:40
ICP 7/15/98 8:31
ICP 7/15/98 8:31
ICP 7/15/98 8:31
ICP 7/15/98 8:31
ICP 7/15/98 8:31
ICPST 7/14/98 11:40
ICP 7/15/98 8:31
ICP 7/15/98 8:31
CVAA 7/15/98 16:39
ICP 7/15/98 8:31
ICP 7/15/98 8:31
ICPST 7/14/98 11:40
ICP 7115198 8:31
ICP 7/15/98 R·~l -, ... -
ICPST 7/14/98 11:40
ICP 7/15/98 8:31
ICP 7/15/98 8:31
fGGG1S :omments: ___________________________________ _ 3.lrt Generator Version 1.00 Form I Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
J.ab Sam pie ID: ____ I _06_9_6_4_33 __ _ Client ID: EX-10
Matrix: Water
Leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
I,.,
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt.
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units: ppb
Volume: 50
WU
I Mass IDL
' ' 308.2 3440
206.3 4.232
189.0 1.3
493.4 80
313.0 40
226.5 0.263
370.6 3360
267.7 160
228.6 280
324.8 160
271.4 1440
220.4 2.518
279.1 1920
257.6 240
253.7 0.3678
231.6 560
766.5 30640
196.0 4.316
328.1 80 . ..
589 4960
190.9 3.311
292.4 200
213.9 200
Prep Date: 6/23/98
Percent Moisture:
I
Report
I I I Limit Cone 0 DF
' ' ' 12000 67400 40
5 4.2 u I
5 1.3 u . I-
8000 80 u 40
200 40 u 40
0.5 2.3' 1
10000 600000 40
400 160 u 40
2000 5840 40
800 5540 40
4000 3_9800 40
3 22.9 1
8000 377000 40
600 184000 40
1.2 I J 1
1600 560 u 40
100000 45800 J 40
5 46 1
400 80 u 40 , .
20000 5790000 40
10 28.3 1
600 200 u 40
800 1950 40
Prep Batch: 13749 ICP
I Instr
Anal
I Anal I
Date Time
' ' ' ICP 7/15/98 8:35
ICPST 7/14/98 11:44
ICPST 7/14/98 11 :44
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICPST 7/14/98 11:44
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICPST 7/14/98 11:44
ICP 7/15/98 8:35
ICP 7/15/98 8:35
CVAA 7/15/98 16:41
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICPST 7/14/98 11:44
ICP 7/15/98 8:35
ICP 7/15/98 8:35
ICPST 7/14/98 11:44
ICP 7/15/98 8:35
ICP 7/15/98 8:35
800016
:omments: ___________________________________ _ :lr1 Generator Version 1.00 Form I Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
IL b S I ID 10696<<4 a amp e : ______ "_" __ _ Client ID: NS-09
Matrix: Water
lweight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
I, .-
1
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units:
Volume:
I
WU
I Mass
' ' 308.2
206.3
189.0
493.4
313.0
226.5
370.6
267.7
228.6
324.8
271.4
220.4
279.1
257.6
253.7
231.6
766.5
196.0
328.I
589
190.9
292.4
213.9
ppb Prep Date: 6/23/98
50 Percent Moisture:
I
Report
I I I IDL Limit Cone 0 DF
' ' 86 300 520 I
4.232 5 4.2 u 1
1.3 5 1.3 u . 1
2 200 270 I
! 5 ! u 1
0.263 0.5 0.26 u 1
84 250 153000 I
4 IO 8.4 J 1
7 50 24 J 1
4 20 13.2 J I
36 100 16300 I
2.518 3 4.8 1
48 200 57200 I
6 15 12400 1
0.0613 0.2 0.061 u I
14 40 23.3 J 1
766 2500 2060 J I
4.316 5 4.3 u 1
2 10 2 u 1
124 500 37400 l
3.311 10 3.3 u 1
5 15 8.7 J l
5 20 47.1 I
Prep Batch: 13749 ICP
I Instr I Anal I Anal
Date Time
' ' ' IICp 7/14/98 15:34
ICPST 7/14/98 11: 12
ICPST 7/14/98 11: 12
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICPST 7/14/98 11 :12
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICPST 7/14/98 11:12
ICP 7/14/98 15:34
ICP 7/14/98 15:34
CVAA 6/23/98 2I:01
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICPST 7/14/98 11: 12
ICP 7/14/98 15:34
ICP 7/14/98 15:34
ICPST 7/14/98 11: 12
ICP 7/14/98 15:34
ICP 7/14/98 15:34
8oacoG
:::omments: ___________________________________ _
:l.lort Generator Version 1.00 Farm I Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
ILab Sample ID: ____ 10_6_9_6_34_2 __ _ Client ID: NS-10
Matrix: Water
lweight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I
I
I
crents:
Element
Aluminum
Antimony
Arsenic
Barium
Be:-yllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units:
Volume:
I WU
I Mass
' 308.2
206.8
189.0
493.4
313.0
226.5
370.6
267.7
228.6
324.8
271.4
220.4
279.1
257.6
253.7
231.6
766.5
196.0
328.1
589
190.9
292.4
213.9
Rlort Generator Version 1.00
ppb
50
I IDL
' 86
4.232
1.3
2
1
0.263
84
4
7
4
36
2.518
48
6
0.0613
14
766
4.316
2
124
3.311
5
5
Prep Date: 6/23/98
Percent Moisture:
I
Report
I I I Limit Cone 0 DF
' ' ' I
300 86 u I
5 4.2 u I
5 1.3 u . l
200 259 1
5 I u I
0.5 0.26 u I
250 62500 1
IO 5.5 J 1
50 29.8 J 1
20 4 u I
JOO 1920 1
3 2.5 u I
200 35600 1
15 2670 1
0.2 0.061 u I
40 14 u I
2500 1840 J 1
5 4.3 u I
_ . 10 ... 2 u l
500 75700 1
10 3.3 u 1
15 5 u 1
20 32.2 1
Prep Batch: 13749 ICP
I Instr
Anal
I Anal
Date Time
' ' ICP 7/14/98 15:30
ICPST 7/14/98 I 1:07
ICPST 7/14/98 11:07
ICP 7/14/98 15:30
ICP 7/14/98 15:30
ICPST 7/14/98 11:07
ICP 7/14/98 15:30
ICP 7/14/98 15:30
ICP 7/14/98 15:30
ICP 7/14/98 15:30
ICP 7/14/98 15:"30
ICPST 7/14/98 I 1:07
ICP 7/14/98 15:30
ICP 7/14/98 15:30
CVAA 6/23/98 21:06
ICP 7/14/98 15:30
ICP 7/14/98 15:30
ICPST 7/14/98 11:07
!CP 7/14/98 15:30
ICP 7/14/r,Jg 15:30
ICPST 7/14/98 11:07
ICP 7/14/98 15:30
ICP 7/14/98 15:30
800007
Form I Equivalent
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
lab Sample ID: ____ 10_6_9_6_35_9 __ _ Client ID: NS-I I
Matrix: Water
Leight: __ 5_0 __
I
I
I
I
I
I
I
I
I
I
I-'
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Units: ppb
Volume: 50
WU I Mass IDL
' 308.2 86
206.3 4.232
l 89.0 1.3
493.4 2
313.0 l
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
23 l.6 14
766.5 766
196.0 4.316
328.l 2
589 124
190.9 3.3 l l
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report I I Limit Cone 0 OF ' ' ' ' 300 400 1
5 4.2 u l
5 1.3 u · l.
200 180 J 1
5 I u I
0.5 0.26 u l
250 7820 1
10 4 u l
50 18.3 J 1
20 4 u I
100 . 7090 1
3 2.5 u l
200 6250 1
15 133 1
0.2 0.061 u I
40 14 u l
2500 2320 J 1
5 4.3 u I
10 2 u ' ' 500 89200 ,
' 10 3.3 u I
15 10.7 J 1
20 11.3 J 1
Prep Batch: 13749 ICP
I Anal I Anal
Instr Date · Time
' ' ICP i/14/98 15:18
!CPST 7/14/98 10:53
ICPST 7/14/98 10:53
ICP 7/14/98 15:18
!CP 7/14/98 15: 18
!CPST 7/14/98 10:53
ICP 7/14/98 15:18
·rep 7/14/98 15: 18
ICP 7/14/98 15:18
ICP 7/14/98 15:18
ICP 7/14/98 15:18
!CPST 7/14/98 10:53
ICP 7/14/98 15:18
ICP 7/14/98 15:18
CVAA 6/23/98 21:08
!CP 7/14/98 15: 13
ICP 7/14/98 15:18
ICPST 7/14/98 10:53
IICP 7/14/98 15: 18
7/14/98 15:18 ICP
ICPST 7/14/98 10:53
ICP 7/14/98 15:18
ICP 7/14/98 15:18
800008
,mments: -------------------------'-------------:1 Generator Version l.00 Farm I Equtvaler.:
I
I Sample Results
Pace Analytical Services
Metals Data Reporting Form
.Lab Sample ID: ____ I0_6_9_6J_'6_7 __ _ Client ID: NS-15
Matrix: Water
lweight: --50--
I
I
I
I
I
m
n
D
I
I
I
I
1--'
I
Element
Aluminum
Antimony
Menic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units: ppb
Volume: 50
I WU I Mass IDL
' '
308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 I
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.l 2
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report
I I Limit Cone 0 DF
' ' ' 300 86 u I
5 4.2 u I
5 1.3 u -l
200 469 1
5 I u I
0.5 0.26 u I
250 349000 1
10 5.2 J 1
50 28.8 J 1
20 4 u I
100 9720 1
3 2.5 u I
200 171000 1
15 15600 1
0.2 0.061 u I
40 14 u I
2500 2510 1
5 4.8 J 1
10 2 u I
500 73400 1
10 3.3 u I
15 8.6 J 1
20 5 u I
Prep Batch: 13749 ICP
I
Anal I Anal I Instr Date Time
' ' ' ICP 7/14/98 15: 15
ICPST 7/14/98 10:49
ICPST 7/14/98 10:49
ICP 7/14/98 15:15
ICP 7/14/98 15:15
ICPST 7/14/98 10:49
ICP 7/14/98 15:15
ICP 7/14/98 15:15
ICP 7/14/98 15:15
ICP 7/14/98 15:15
ICP 7/14/98 15:15
ICPST 7/14/98 10:49
ICP 7/14/98 15:15
ICP 7/14/98 15:15
CVAA 6/23/98 21 :10
ICP 7/14/98 15: 15
ICP 7/14/98 15:15
ICPST 7/14/98 10:49
ICP 7/14198 , r.,,.
lJ.lJ
ICP 7/14/98 15:15
ICPST 7/14/98 10:49
ICP 7/14/98 15:15
ICP 7/14/98 15:15
800009
:o=ents: ___________________________________
_ '.lrt Generator Version 1.00 Form ! Equivalent
I
I .
Sample Results
Pace Analytical Services
Metals Data Reporting Form
Jab Sample ID: ____ 10_6_9_6_3_18 __ _ Client ID: NS-29
Matrix: Water
Leight: --50--
I
I
I
I
I
I
I
I
I
I
I
I
I-'
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
Units: ppb
Volume: 50
WU I Mass IDL
' 308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 1
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.1 2
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report
I I Limit Cone 0 DF
' ' ' 300 86 u I
5 4.2 u I
5 1.3 u . J.
200 1370 1
5 1.2 J 1
0.5 0.26 u I
250 892000 1
10 12.3 I
50 7 u I
20 4 u I
100 .3040 I
3 2.5 u I
200 140000 1
15 32100 I
0.2 0.061 u I
40 14 u I
2500 5240 I
5 15.6 I
10 2 u ! I 500 280000 1.
10 4.4 J 1
15 25.9 I
20 5 u I
Prep Batch: 13749 ICP
I Instr I Anal
I
Anal
Date Time
' ' ' ICP 7/14/98 15:07
ICPST 7/14/98 10:40
ICPST 7/14/98 10:40
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICPST 7/14/98 10:40
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICPST 7/14/98 10:40
ICP 7/14/98 15:07
ICP 7/14/98 15:07
CVAA 6/23/98 20:57
ICP 7/14/98 15:07
ICP 7/14/98 15:07
ICPST 7/14/98 10:40
!CP -,11 A 190 15:07 I II ... ..,, u
ICP ""f 1"1 ~ lf\O 15:0i II J. .. l;,Q
ICPST 7/14/98 10:40
ICP 7/14/98 15:07
ICP 7/14/98 15:07
800004
omments: ------------------------'--------------el Generator Version 1.00 Form I Equtva!ent
I
I Sample Results
Pace Analytical Services
M~tals Data Reporting Form
.ab Sample ID: ____ 10_6_9_6_32_6 __ _ Client ID: NS-30
Matrix: Water
Leight: --50--
I
I
I
I
I
I
I
I
I
I
I
1··
I
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
. Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
I
'
Units: ppb
Volume: 50
WU I Mass IDL
' 308.2 86
206.8 4.232
189.0 l.3
493.4 2
313.0 I
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.1 2
589 124
190.9 3.3 I I
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report I I I I Limit Cone 0 DF
' ' 300 86 u I
5 4.2 u I
5 1.3 u -I
200 36 J I
5 I u I
0.5 0.26 u I
250 82700 1
10 4.1 J I
50 7 u I
20 4 u I
100 799 I
3 2.5 u I
200 16600 1
15 1250 1
0.2 0.096 J 1
40 14 u I
2500 1930 J 1
5 4.3 u I
IO 2 TT I I u
500 !!900 1
IO 3.3 u I
15 5 u I
20 5 u I
Prep Batch: I 3749 ICP
I Anal l A_nal I Instr Date Time
' ' !CP 7/14/98 15:38
!CPST 7/14/98 11: 17
ICPST 7/14/98 l l: 17
ICP 7/14/98 15:38
!CP 7/14/98 15:38
!CPST 7/14/98 11: 17
ICP 7/14/98 15:38
ICP 7/14/98 15:38
!CP 7/14/98 15:38
ICP 7/14/98 15:38
ICP 7/14/98 15:38
ICPST 7/14/98 11: 17
ICP 7/14/98 15:38
ICP 7/14/98 15:38
CVAA 6/23/98 20:59
ICP 7/14/98 15:38
ICP 7/14/98 15:38
ICPST 7/14/98 l l: 17
ICP 7/14/98 15:38
ICP 7/14/98 15:38
ICPST 7/14/98 11 :17
ICP 7/14/98 15:38
ICP 7/14/98 15:38
800005
omments: -----------------------~------------
\ _e, Generator Version 1.00 Farm I Equfv.::le:-zt I
I
.Sample Results
Pace Analytical Services
Metals Data Reporting Form
.Lab Sample ID: ____ 10_6_9_6_30_0 __ _ Client ID: NS-31
Matrix:
lweight:
I
I
I
I
I
I
I
I
I
I
I
I ...
I
,=ents:
Water ----
50 ----
Element
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units: ppb
Volume: 50
I WU I Mass IDL
' ' 308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 I
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.I 48
257.6 6
253.7 0.0613
231.6 14
766.5 766
196.0 4.316
328.1 2
589 124
190.9 3.311
292.4 5
213.9 5
Prep Date: 6/23/98
Percent Moisture:
I Report I I I Limit Cone 0 DF
' ' ' ' 300 86 u I
5 4.2 u I
5 l.3 u -L
200 9330 1
5 I u i
0.5 0.26 u I
250 956000 1
10 12.9 1
50 7 u I
20 4 u I
100 376 I
3 2.5 u I
200 64300 I
15 4150 I
0.2 0.079 J 1
40 23-.2 J I
2500 6650 I
5 4.3 u 1
10 2 u 1
500 160000 I
10 3.3 u I
15 14.1 J 1
20 5 u 1
Prep Batch: 13749 ICP
I I Anal I A_nai j Instr Date Time.
' ' ' ICP 7/14/98 14:52
ICPST 7/14/98 10:21
!CPST 7/14/98 10:21.
ICP 7/14/98 14:52
ICF 7/14/98 14:52
ICPST 7/14/98 10:21
ICP 7/14/98 14:52
ICP 7/14/98 14:52
ICP 7/14/98 14:52
ICP 7/14/98 14:52
ICP 7/14/98 14:52
ICPST 7/14/98 10:21
ICP 7/14/98 14:52
ICP 7/14/98 14:52
CVAA 6/23/98 20:55
ICP 7/14/98 14:52
ICP 7/14/98 14:52
!CPST 7/14/98 10:21
TCP 7/14/98 14:52
ICP 7/14/98 1-1:52
ICPST 7/14/98 10:21
ICP 7/14/98 14:52
ICP 7/14/98 14:52
800003
------------------------------------: f Generator Version 1.00 Form I Equivalent
I
I
Sample Results
Pace Analytical Services
Metals Data Reporting Form
I Lab Sample ID: ____ 10_6_9_6_37_5 __ _ Client ID: NS-32
Matrix:
I weight:
I
I
I
I
I
I
I
I
I
I
I
1.-'
I
Water
50 ----
Element I
' Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Mercury
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Units: ppb
Volume: 50
WU
I Mass IDL
' 308.2 86
206.8 4.232
189.0 1.3
493.4 2
313.0 1
226.5 0.263
370.6 84
267.7 4
228.6 7
324.8 4
271.4 36
220.4 2.518
279.1 48
257.6 6
253.7 0.0613
23 l.6 14
766.5 766
196.0 4.316
328.l 2
589 124
190.9 3.311
292.4 5
213.9 5.
Prep Date: 6/23/98
Percent Moisture:
I Report I I I Limit Cone 0 DF
' ' ' 300 86 u I
5 4.2 u I
5 1.3 u . ·I
200 105 J 1
5 l u I
0.5 0.26 u I
250 53600 1
10 4 u I
50 7 u I
20 4 u I
JOO 170 1
3 2.5 u l
200 9210 I
15 139 1
0.2 0.061 u I
40 14 u l
2500 3560 1
5 4.3 u I
10 2 u ' ' 500 9660 1
10 3.3 u I
15 5 u I
20 5 u I
Prep Batch: 13749 ICP
I Instr
Anal I Anal
Date Time
' ' ' ICP 7/14/98 15: 11
ICPST 7/14/98 10:44
ICPST 7/14/98 10:44
ICP 7/14/98 15:11
ICP 7/14/98 15: 11
ICPST 7/14/98 10:44
ICP 7/14/98 15:11
ICP 7/14/98 15: 11
ICP 7/14/98 15: 11
ICP 7/14/98 15: l l
ICP 7/14/98 15:11
ICPST 7/14/98 10:44
ICP 7/14/98 15:11
ICP 7/14/98 15:11
CVAA 6/23/98 18:50
!CP 7/14/98 l 5: l l
ICP 7/14/98 15:11
ICPST 7/14/98 10:44
ICF 7/14/90 i 5: ii
ICP i/i4/98 iS:11
ICPST 7/14/98 10:44
ICP 7/14/98 15: 11
ICP 7/14/98 15:11
800010
:om meats:------------------------------------,111 Generator Version l.00 Form I Equivalent