NCD991278953_19971001_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Second Quarter 1997 OU-1 and OU-2-OCR

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Quarterly Report
Second Quarter 1997
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
October 1997
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Quarterly Report
RECEIVED
NOV 181997
SUPERFUND SECTION
Second Quarter 1997
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
October 1997
~ wvttl
NOV I 2 !097
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Table of Contents
1.0 Groundwater Monitoring Activities for the Second Quarter 1997 .
2.0 Planned Groundwater Monitoring Activities ..
3. 0 References .
Appendix -Certificates of Analysis
Appendix A -Report of Laboratory Analysis
Plume Periphery Wells &
Trench Area Wells
Appendix B -Volatile Organics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix C -Semivolatile Organics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix D -Inorganics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix E -Chain-of-Custody Records
Plume Periphery Wells &
Trench Area Wells
Appendix F -Out of Service Well Pumping Records·
Plume Periphery Wells and Trench Area Wells
Environmental Data Management, Inc,
· P.O. Box 16326
Chapel Hill. NC 275 I 6
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List of Tables
Table Title
I List of Sample Analysis and Water Level Monitoring Performed
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Second Quarter 1997, Plume Periphery Wells
3 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Second Quarter 1997, Trench Area Monitoring Wells
4 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Second Quarter 1997, Trench Area Extraction Wells
5 Groundwater Cleanup Criteria, Operable Unit No. I
6 Water Level Measurements, Second Quarter 1997, Plume Periphery Wells
7 Water Level Measurements, Second Quarter 1997, Trench Area Wells
List of Figures
Figure Title
Site Map
2 Quarterly Summary of Acetone -Plume Periphery
3 Quarterly Summary of 1,2-Dichloroethane -Plume Periphery
4 Quarterly Summary of 1,2-Dichloropropane -Plume Periphery
5 Quarterly Summary of Bis(2-chloroethyl)ether -Plume Periphery
6 Quarterly Summary of Acetone -Trench Area
7 Quarterly Summary of 1,2-Dichloroethane -Trench Area
8 Quarterly Summary of 1,2-Dichloropropane -Trench Area
9 Quarterly Summary of Bis(2-chloroethyl)ether -Trench Area
IO Groundwater Contour Map for April 7, I 997
11 Individual Periphery Wells Pumping Rate (Quarter 1-1997)
12 Combined Periphery Wells Pumping Rate (Quarter 1-1997)
13 Combined Trench Area Wells Pumping Rate (Quarter 1-1997)
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Environmental Data Management, Inc.
1.0 Groundwater Monitoring Activities for Second Quarter 1997
This second quarter 1997 report presents the findings from the groundwater monitoring
conducted at Operable Units No. I and 2 at the National Starch and Chemical Company
site on Cedar Springs Road, Salisbury, North Carolina. This report is prepared in
accordance with Record of Decisions (ROD) issued by the U.S. EPA on Sep.tember 30,
1988 for Operable Unit No. I (OU!) and on September 30, 1990 for Operable Unit No. 2
(OU2). Operable Unit No. I consists of contaminated groundwater area located in the
west-southwest portion of the facility. Operable Unit No. 2 consists of contaminated soils
and surface water/sediments in tributaries surrounding a trench area west of the plant
operation area.
Operable Unit No. l {Plume Periphery Wells)
Groundwater samples from the four downgradient groundwater monitoring wells (NS29,
NS30, NS31, and NS32) and four bedrock extraction wells (EX0I, EX02, EX03, and
EX04) were collected on April 7, I 997. All samples were analyzed for Target Compound
List (TCL) volatile and semivolatile organic compounds (VOC and SVOC), Target
Analyte List (T AL) metals, and general chemistry. In addition, samples from the
monitoring wells and extraction wells were analyzed for selected water quality parameters
to monitor influent loadings for the Combined Pretreatment System (CPS). A sample
analysis summary is provided in Table I. The samples were collected in accordance with
U.S. EPA (Region IV) protocols. The TCL and TAL compounds were analyzed
supporting U.S. EPA Level IV Contract Laboratory Program (CLP) protocol.
The four plume periphery extraction wells (EX0I, EX02, EX03, and EX04) continued to
operate during the first quarter of I 997, except for a scheduled shutdown in mid March
for well and pump maintenance (see Figures 11 and 12). In addition to the plume
periphery wells, six extraction wells (EX0S, EX06, EX07, EX08, EX09, and EXI0),
located in the trench area pumped continuously during the first quarter (see Figure 13).
Results from the chemical analysis for Operable Unit No. I plume periphery wells are
presented in Table 2. The chemical analysis results for the Trench Area monitoring and
extraction wells are presented in Table 3 and Table 4, respectively. The list of compounds
presented in these tables represents the contaminants specified in Operable Unit No. I
Record of Decision (ROD). The list of designated compounds from the ROD (OU!) and
associated cleanup levels are provided in Table S. Figure I is a site map showing the well
locations. The certificates of analysis are provided in the Appendix. ·
The results ohhis quarters sampling indicated that four organic compounds, acetone, 1,2-
dichloroethane (1,2-DCA), 1-2-dichloropropane (1,2-DCP) and bis(2-chloroethyl)ether
exhibited levels that exceeded cleanup levels (shaded bold faced values in Table 2).
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The acetone level remained above the cleanup standard .in extraction well EX02 and
EX03 _ However, the acetone levels in these extraction wells decreased significantly since
the previous quarter (see Figure 2). Acetone levels in extraction wells EX0I and EX04
remained relatively unchanged, below the cleanup standard. Since the previous quarter,
acetone levels in monitoring wells NS29 and NS3 l remained above the cleanup standard.
However, the acetone level in NS29 decreased and the acetone level in NS3 l increased
since the previous quarter (see Figure 2). Monitoring wells NS30 and NS32 continue to
show no significant contaminant concentrations are present (see Table 2).
Also, Bis(2-chloroethyl)ether levels remained above the cleanup standard in most of the
OU! wells (see Figure 5). Except for Bis(2-chloroethyl)ether, extraction well EX0I did
not exceed the cleanup standard for the other target compounds.
The general trends for the four organic compounds that have exceeded the cleanup criteria
over the past four quarterly sampling events are presented in graphical form on Figures 2
through 5. These four organic compounds are acetone, 1,2-dichloroethane, 1,2-dichloro-
propane, and bis(2-chloroethyl)ether. Manganese exceeded cleanup standards in only well
EX02. Barium exceeded cleanup standards in only well NS3 l (see Table 2)
Water level measurements were taken on April 7, 1997, from seventeen selected
monitoring wells and ten extraction wells. The static water level for NS32 was not
measured, due to artesian conditions. Well NS32 has been under artesian conditions
during all previous sampling events. The results of the water level measurements are
presented in Table 6. A groundwater contour map of the subject area showing the
effectiveness of the extraction wells is shown in Figure IO. The groundwater contour was
computer generated using a krig algorithm set to a linear type semi-variogram with a SO-
foot x-y grid spacing.
During the past quarter, the extraction well system experienced some downtime. The well
pumping data presented in this report represents data recorded during the previous quarter
(Quarter I 1997). A plot of the individual pumping rates for each periphery well for the
previous quarter in presented in Figure 11. Note the individual periphery wells were
alternately shutdown for scheduled maintenance for a brief period in mid March. The
combined average quarterly pumping rate for the four extraction wells (EX0 I, EX02,
EX03 and EX04) is about 80 gpm (see Figure 12). The efficiency of the plume control
and hydraulic control will be evaluated in more detail after all trench area extraction wells
are fully operating. ·
Operable Unit No. 2 Groundwater Monitoring
The Remedial Design/Performance Monitoring Work Plan for Operable Unit 2 states that
National Starch and Chemical may use the groundwater data collected for the OU I
monitoring program to satisfy the OU2 monitoring requirements. The monitoring plan for
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OU2 requires the periodic sampling of groundwater from eight wells: NS09, NSI0, NS! I,
NS15, EX06, EX07, EX08, and EX09. Additional groundwater data from extraction
wells EX05 and EX IO are also included in this report
Trench Area Monitoring Wells
Groundwater samples were collected from monitoring wells NS09, NSI0, NS! I, and
NS15 on April 8, 1997. All samples were analyzed for selected TCL VOCs and SVOCs,
and T AL metals. A sample analysis summary is provided in Table I. The samples were
collected in accordance with U.S. EPA (Region IV) protocol. The TCL and TAL
compounds were analyzed under U.S. EPA Level IV CLP protocol.
Results from the chemical analysis for these wells are presented in Table 3. The list of
compounds presented in Table 3 represents the contaminants specified in Operable Unit
No. 1 ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 5. Figure 1 is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
Three of the monitoring wells (NS09, NSl0, and NS15) in the trench area had levels of
1,2-DCA that exceeded the cleanup standards. Monitoring wells NS09 and NS 15
exceeded cleanup standards for vinyl chloride. Monitoring well NS 11 did not exceed the
cleanup standard for any of the target compounds.
Manganese exceeded clean up levels in monitoring wells NS09 and NS 15. Monitoring
wells NS 10 and; NS i 1 continue to have manganese concentrations below the cleanup
standard (see Table 3).
Water level measurements were taken on April 7, 1997 from each of the four monitoring
wells. The results are provided in Table 7. A groundwater contour map of the subject
area is provided in Figure I 0.
Trench Area Extraction Wells
Six extraction wells (EX05, EX06, EX07, EX08, EX09, and EXl0) began pumping in the
trench area west of the main plant on February 26, 1996. With some minor adjustments in
the pumping rates for the individual wells, the wells have been pumping at a combined rate
of averaging about 18 gpm. A chart showing the combined pumping rate for the six
extraction wells during the previous (Quarter 4) is presented in Figure 13.
With the start up of the trench area extraction wells, the trench area pretreatment area was
also utilized for the first time. Problems with this start up have been noted in the monthly
progress reports.
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Groundwater samples were collected from the six new extraction wells on April 8, 1997.
All future quarterly reporting for OU I and OU2 will include the sampling and analysis of
groundwater from these wells.
All samples were analyzed for selected TCL VOCs and SVOCs, and T AL metals. A
sample analysis summary is provided in Table I. The samples were collected in
accordance with U.S. EPA (Region IV) protocol. The TCL and TAL compounds were
analyzed under U.S. EPA Level IV CLP protocol.
Results from the chemical analysis for Trench Area are presented in Table 4. The list of
compounds presented in Table 4 represents the contaminants specified in Operable Unit
No. I ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 5. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
The results of this quarter's sampling indicated that seven organic compounds, acetone,
1,2-DCA, 1,2-DCP, toluene, vinyl. chloride, xylene, and bis(2-chloroethyl)ether were
found in one or more of the trench area extraction wells and exhibited levels that exceeded
cleanup levels (shaded bold faced values in Table 4). Note that not all of the above
mentioned compounds were found in any single extraction well, however, 1,2-DCA, was
present in all of the trench area extraction wells.
One other. VOC compound, 4-Methyl-2-Pentanone, not part of the ROD (OU!) listed
contaminants, was found in the trench area wells. This compound was found in relatively
high concentrations in EX0S, EX06, EX07, EX08, and EX09 (see Table 4).
Four inorganic compounds including, Cadmium, Manganese, Nickel and Selenium were
found in concentrations exceeding the cleanup standard in wells EX0S, EX07, EX08,
EX09, and EX IO. Also, the presence of Arsenic, slightly exceeding the cleanup standard,
was found in EX0S (see Table 4).
For comparative purposes, the four organic compounds that have exceeded the cleanup
criteria for the plume periphery wells are presented in graphical form on Figures 6 through
9 for the trench area wells. These four organic compounds are acetone, 1,2-
dichloroethane, 1,2-dichloropropane, and bis(2-chloroethyl)ether.
Note that several of the compound concentrations shown on the figures have an asterisk.
The asterisk indicates that the detection limit for that compound exceeded the
groundwater cleanup standard. The higher detection limit for certain target compounds
results because the sample must be diluted to prevent contamination of the GC/MS from
the very high concentrations of 1,2-Dichloroethane, Toluene, or Acetone that are typically
found in the site area wells.
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2.0 Planned Groundwater Monitoring Activities
Plume Periphery Wells
The implementation of the extraction well system will continue as planned with the 24-
hour operation of the plume periphery extraction wells EX0I, EX02, EX03, and EX04.
Groundwater monitoring will continue. Care will be taken to closely monitor the daily
pumping rates of the extraction well system. Particular attention will be made to assure
that all plume periphery extraction wells continue to pump at optimum efficiency and that
downtime for pump maintenance is minimized.
National Starch and Chemical Company will continue to alert laboratory personnel of
samples from wells with known high VOC concentrations.
Trench Area Wells
The six extraction wells will continue to operate. During this initial operating phase the
extraction wells will be monitored closely and their pumping rates may be modified in
order to optimize their performance. The efficiency of the plume control and hydraulic
control for both Operable Units 1 & 2 will be evaluated in more detail using information
gathered from this initial operating phase.
Groundwater monitoring will continue. Very high concentrations of VOC compounds
found in the trench area wells will require that laboratory personnel be alerted prior to
testing groundwater samples so that proper procedures can be taken to minimize
laboratory contamination and improve compound detection limits.
Groundwater level measurements will be taken prior to the sampling of the extraction
wells so that the effectiveness of the pumping program in the trench area can be evaluated.
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3. References
EDM, Inc., July 1997, "Quarterly Report -First Quarter 1997 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., April I 997, "Quarterly Report -Fourth Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., February 1997, "Quarterly Report -Third Quarter 1996 Operable Units
No. 1 & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., August 1996, "Quarterly Report -Second Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., May 1996, "Quarterly Report -First Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., February 1996, "Quarterly Report -Fourth Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., October 1995, "Quarterly Report -Third Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., August 1995, "Quarterly Report -Second Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, May 1995 , "Quarterly Report -First Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, February 1995 , "Quarterly Report -Fourth Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, October 1994 , "Quarterly Report -Third Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
North Carolina Environmental Management Commission, North Carolina Administrative
Code: !SA NCAC Subchapter 2L (August 1993).
U.S. EPA, September 30, 1990, Record ofDecision (ROD) for Operable Unit No 2,
National Starch and Chemical Company, Salisbury, NC.
U.S. EPA, September 30, 1988, Record of Decision (ROD) for Operable Unit No I,
National Starch and Chemical Company, Salisbury, NC.
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Table 1
List of Sample Analysis and Water Level Monitoring Performed
Second Quarter 1997
Operable Units No. 1 and 2
National Starch and Chemical Company
Salisbury, North Carolina
Well Number Well TCL TCL TAL Water
Tvoe' VOCs' SVOCs' Metals' Level
ooerat>1e·••.uriit·••No>1if Pti.iffie••Penotierv.we11sg ····•·•········••· <.·•.•.<.·••·•x<••>·····••••n·•·•··,··••··············•··•·••:•.iv·.·•····
EX01 • BE . X X , X • X .............. "·
EX02 BE ............ --
EX03 BE
EX04 BE ······-···-····•·-NS05 ! SM . ············. NS06 SM .................. ······. --···· ···-·····-·-··· ..
NS21 BM ···········-······-"
t-1§:!2. ····'····-· BM NS23 SM
NS26 BM NS2i . --BM........ •
NS28 BM
X
X
X
X
X
X
X
X
X
11---···········-··········•······-=-"c..._ __ . __ ~ ____ ._~ ____ _
NS29 BM X X X
NS30 BM X X X
NS31 BM X X : X
NS32 -...cBcc.Mcc.-_~_~x::----x-X
PO1 BM
Stream • ···NAa
Gauge No,.1°: ....
Stream
Gauae No. 2 ,
NA
NS09 SM X
NS10 SM X
NS11 SM X --·.··-··-NS15 BM X
X
X
X
X
X
X
X
X
EX05 BE X X X ---EX06 BE X X X , .. y ............ ,, ............. ·+·-
EX07 BE ·-X X • X
lf----'EX=0c.=8 ___ -=Bo.cE'----~-~x'-------=x-'----~·--'x
EX09 BE X X X .......................
EX10 BE X X X
---c--
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
x
X
'BE = Bedrock extraction well, BM = Bedrock monitonng well, SM = Saprolite (shallow) monitonng well
bProject TCL consisting of 13 VOCs, 2 SVOCs, and 9 metals, and meets Operable Unit No. 1 cleanup criteria (Table 5).
clron pins in southwest tributary for monitoring stream elevations.
dNA -Not Applicable
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Table 2
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1997
Plume Periphery Wells
National Starch and Chemical Company
Salisbury, North Carolina
Extraction Wells Monitorino Wells
Well Number: EX01 EX02 I EX03 EX04 NS29 I NS30 I NS31 NS32
Sample Date: 4n /97 417197 I 417/97 4/7/97 417197 I 417197 I 417 /97 I 417197
Volatile Organics (ug/1)
sromodichloro~:~:~: .. ... . ~~ [)sr~'!0.~!~1 2
~~~ l~.oo~~'. 4J8 :43000EB 3J8 .......... J.,,s,,-,,_._ ...•. ,, " .•
10U: 1000U 10U
10U' 1000U 10U
Chloroform 10U 250Ui 250Ui 10Ui SOOU
If---.-... -.-... -. -... --~-.:~-/-.1-cc;g-c~.~"c~-c?"l_r_I_;~-;-;-~~-•. 1--:·.-· ... -.~ ___ ~::"'~ci·· i·:;;::!r':;:)'.i[:;;,:;,!:~;::::·~·r-'•'£··~~~.+-i--,-o-u-,--1000~-u--,l-... --1 o=u
1ou; 1000U 10U
10U' 1000U 10U
10U' 1000Ul 10U ... \ . 1ou• . iooau; 10U
. . .. ...... Methylene.Chloride 1ou; .. 2/xJU.L. 250U 1ou; ....... ~.l/I .1ou: .... 1J!f!QJ,/······-i@
Toluene 10U: 110J: 160J 33 260J; 10U' 370Ji 10U
... 1:1.~~'rri~iiioroethane(TCA) iiiiJ! 2soi/ 250LJ ioUl soou' ioU 1000U. 10U
Trichloroethene (TCE) · ·10Uj · ~; 2sou ·· · ·1or/ · soou ...... W!. ....... 1.ooou 1ou
lf---------,-Vc-in-yl'""C=chloride 1f!j/_ ~i ~ W!.[ ··5oiiiJ .. . .. 10!/_ .... 1900!/_. 10U
. Xylene. 1 OU 1000U 1 OU 10U 250UI 250U 10• soou · iouT ... .... . ........... ~ _,_\g~~hl~~-~thane·
4-Methyl-2-Pentanone*
Acrylonitrtle*
Semivolatile Oraanic {ua/ll
lnor11anics (u!l/ll
Arsenic
Barium
Beryllium
Cadmium
-----C~hromium
.. ~~~~.a-~~~.
Nickel
Selenium
Zinc
Note Data Qualifier Definitions:
10U 250U: 250U
10U, isou• 250U1
NA! NA' NA\
500U
isJi 500U __ ,_,.,,· ..........
13NJI NA!
10U,
10U
1000U
1000U
10U
10U
NA
ru ru ru ru• Wi 7U. ru1 ru
1530 9li2 · · 647 4ii iiif 120' 2a0 i'i!friiiifoi 930 . I · ... ,"/··,· ·~,, 2U . 2u;·· 2U ..... ·2u!·······2u:. 2U• 2U 2U
3Ui 3Ui 3U 3U' 3U.i 3U' ~3~U+---3U
······1· 5U 5.68; 5U 5U• .. su1.. 5Ui 5U 5U
451 i'ili::J1eool··-· 3960 · 4530! 31101 is1·or 993 114
20U 20U i 20U 20U ,· .... 20U :· 20U' 20U 20U ······•·r'------7U 9.8i 5U 5U; 7.21 5U• 5U\ 5U
5U! 10.98' 5Ui 5Ui 5Ui 5U• ....... 5U!° 5U
B (Organics) = Compound was detected in the associated blank.
B (Inorganic,) = Compound concentration is_ below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace value, or it is a nontargat for which no calibration waa performed.
U = Compound waa analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gaa chromatography/
maas spectrometry instrument.
ND= Not detected at or above the detection limit of analyais method.
NA= Not analyzed.
Note: Shaded bold face data indicates a detected concentration that exceeds the groundwater cleanup standard (US EPA 9-30-88).
Italic and underlined data indicates the laboratory detection limit exceeded the groundwater cleanup standard.
Also Note: The three chemicals with an asterisk are not ROD (OU1) contaminants but are analyzed for since they have been detected
in the trench area.
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Table 3
ROD (OU1 I Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1997
Trench Area Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
Monitorinn Wells
Well Nuniber: NS09 I NS10 I NS11 I
Sample Date: 418/97 I 4/8/97 I 4/8/97 I
Volatile Oraanics lua/11
Acetone
Benzene
94JB'
1oou,
... 78JB:
100U;
BroniodiCh1orometha·ne ·········100ur·· 100U!
22B;
10U;
ioi/
NS16
417/97
10U
10U
10U
Chloroform ............. ···iooi.F 1oou, ioiJ: 10U 11---------------l
______ ----~..'.~~~i_?_~~~roethane i~:::!~•'>{:i';/:4!00E !·H!t'!:=:+::":"Hi~(;::t!.70! ___ _ .. _______ 3J _ ~=:::::b-'::'iJi+t:: t< :J 120
1.,1'.~ichl~re>et~~~n~ . 100U 1oou, 1ou, 1ou
1,~:~ichloroproP.ane 1oou: 1Cl0ll[
Ethylbenzene 1 OOU ' 1 OOU :
''----------"M-'e'--th'-'yl-'e'--n'--e_C:._h.:..lo'-r-'idc.e, ---~1oo=u"';'----~1=0=0U=i _
Toluene 80J \ 1 OOU :
...... 1,1,~:Trichlorci,,ttian~ (fCA) JgQQ; . iooi/.
Trichlciroethene (TCE) 1001/ .. ·1001)( --=="-----~=~-Vinyl Chloride_ t:::./•!•· 1 ~ ; 1 48Ji 100U!
''------·--~ Xylene... 1oou\····· 100U'
•..• ~ .. _1_ ~~~~!?~-~~~~-':'-~-~ ___ .... "fOOUT" ...... 1.00ijf
4-Methyl-2-Pentanone• 1 DOU: 100U j
Semivalatile Oraanic lua/ll
Bis (2-Chloroethyl) Ether! 1oou:
4-Nitrophenol I SOU' 250U'
lnornanics tun/II
ll------------'-Ar.~~~~ ••-•······---7-U~l _____ 7_U \
Barium 329: 205;
. Berylliu111 .. jiJ\ 2U'
Cadmium 3U f · .... iJT
Chromium 21.7f · SU!
1ou:
20:.
1ou,
SJ;
1ou,
10i/
10U:
2su:
1u:
199B;
2U
3U'
8.2B;
10U
10U
10U
4J
10U
10U
10U
10U
10U
2SU
7U
342
2U
3U
SU
................. -~~~-~-~~~ ~~itlif1::lfi:0i~!~l 2150'
ii.:iiiT sur
. ~~~ :Nnt;:~-~';:i!;\i11~
Nickel 20Ui 21.9B; 20U
Selenium •·e:tt SU SU
Zinc 10.9B; 37.2! 22.4! SU
Note Data Qualifier Definitions:
B (Organics) = Compound was detected in the auociatad blank.
B Onorganics) = Compound concentration is below the contract-required detection limit.
J = Compound concentration ia an estimate. Either the compound was positively
identified at a trace value, or it is a nontargat for which no calibration'was performed.
U = Compound was analyzed for but not detected at the listed concentration. ·
E = Compound concentration Oxcaeda calibration range of the gas chromatography/
maH spectrometry instrument.
ND= Not detected at or above the detection limit of analyai• method.
NA = Not analyzed.
Note: Shaded bold face data indicates a detected concentration that exceeds tho groundwater cleanup standard fUS EPA 9-30-881.
Italic and under1ined data indicates the laboratory detection limit exceeded the groundwater cleanup standard.
Also Note: The two chemicals with an asterisk are not ROD (OU 11 contaminants but are analyzed tor since they have been detected
in the trench area.
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Environmental Data Management, lnc.
Table 4
ROD (OU1 I Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1997
Trench Area Extraction Wells
National Starch and Chemical Company
Salisbury, North Carolina
Extraction Wells
Well Number: EX05 I EX0& I EX07 J EX08 J EX09 J EX10
Sample Date: 4/8/97 I 418/97 I 4/8/97 I 418/97 I 418/97 I 416/97
Volatile Ornanics lua/11
__ _cA.;.:cetone ,,r,; 3~00B! 380EB ;%:;,:· .. -;40~BJf.!~OO~EB\!'··:,:~ooe(:_l.,L~~2B
Benzene 2ooou: 1ou: 25ou; sooou: 2soou: sooou
.... Ei,omodichloromethane .... 2ooiJjj; . ·;oi/' ........ 250Uj"'. sooou, 2.5Cou'. sooou
Chloroform 2000U' 1ou; ~' sooou, 2soou, sooou
''--------, ,-2--D-ic~h-lo-,-oe-th_a_n___,e ;:':, 390000E t;;;•:rn!)T:'48iie[N,:: 31000E)[i<29C>OOOE] •·• 1 ;1.30!JG~fiJ'.i~
1,1-Dichloroethylene 2ooou 1.Q![ 250U' sooou; 2500U' sooou
i ,:i:oic~ioropropane •.. 2ooou: 1ou ....... 2iioi/ ... ~ i ,,; ' fi100!!\1/TsliiJoo
Ethylbenzene 2000U ... i OU r .... 250\J : siioou: "" ' 2soou\' "''i'aooJ
''------'-'MC:etC:h!..:yl:::en.:_:e__:C:.,_h,:,:lo::.,rt::.:de,, 2ooou: 1ou: 2sou, sooou: 2500U! sooou
Toluene ~:rf ·z3000j 37: ·········•·•~-~}~!~'.ri:'!~'ff:~~;J;lf~~J.~!i? \12000 ······· ,:; ::2:r~ciiioroeiiiiiiie ifcA) ....... 2000(): ········· iou1 2sou sooou 2soou .. sooou
.. Trichlo;oeihene(TCE) 20oou: •·•······ 1iiiJ; ·25iJu'· 5iJiiiJu! . ~: sooou
11 _________ V_in~yl_C_h_lo_n_·d_e1 !i~! :\1,200J}1'•:tc:1:•::~ ,H 3J I 2!i!lQ' SOOOU ! 2;jQQjj;
Xylene 2000U 1 OU , 250U 5()00UfI:Cli Jl\!!1':,rn:;:; ;,f~!)II
· i','i' oichta,oeiiian•' · 2ooou · ·· · 'i'au , · 2sou, sooou , 2soou • sooou
· ';j:.'i.i.1t111:2 .. i>eniaiian•' 3000 as; 2sixi: 33000: s100: sooou _..::.c::.::.;,_.;.:;,:=
Acrylonitrile* NA' NA i 470NJ i 6600NJ : 6000NJ : 4000NJ
Semivolatile Oraanic lua/li
,,__ ___ ...cB:ci•'--"(2:...·C_h_lo_roet_h~yl-'-) _E_th_er_ 0 --'=11=o=uc.; --=1o=u=.:;_.....c1=oo=U-"i<'•,;:C•r, k.390 \:'·'!?:' •~ !q: :}G 14!JOO
4-Nitrophenol 260U ! 25U ! 250U ! 250U : 1 DOU i 5300U
lnoraanics lua/ll
Note Data Qualifier Definitions:
B (Organics) = Compound was detected in the auociated blank.
B !Inorganic•) = Compound concentration is below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively
identifiad at II trace value, or it is II nontarget for which no calibration WIIS performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
man spectrometry instrument.
ND= Not detected at or above tho detection limit of analysis method.
NA= Not analyzed.
Note: Shaded bold face data indicates a detected concentration that exceeds the groundwater cleanup standard (US EPA 9-30-88).
Italic and under1ined data indicate• the laboratory detection limit _exceeded the groundwater cleanup standard.
Also Note: The three chemicals with an asterisk are not ROD IOU1) contaminants but are analyzed for since they have been
detected in the trench area.
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Environmental Data Management, Inc.
Table 5
Groundwater Cleanup Criteria
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Compound Cleanup Concentration (ug/1)
Acetone! 3500
If----------_ -_-_-_-___ -Be_n~z~e_n_e_i -------~5 ________ _
Brornodichlgr()rn~thane[ 5
Chloroform 5 .....................
······· 1,2-Dichl()r()~than~(P9!9+--------5
______ 1-'-''"-1--'-D=-'i-"chloroethy-'-'lec.c.n.c.ce+--_______ 7
1,?:Pichloropropan~ 6
...... ... . .. E:thylb..enz.eril:l .. 3500
Methylene Chl()ride 5
Toluene 2000 ______ _,,
... . .. 1,1,2:Trichl()rC)Elth<1ne (TGA)i 5
Trichl()roethen~JrgE)[ ... 5
_______ Vinyl Chloride\ ..... _ 2
X lenei
Arsenic': 10 ········r--·-------Bariumi 1000
.8-~rxniurn 17.5
Cadmium 10
Chromium 50
Manganese: 7700 11--------------'=~ Nickell 350
Seleniumr . 10 . zind . 7350
Reference: U.S. EPA, September 30, 1988, Record of Decision (ROD), Operable Unit No. 1,
National Starch and Chemical Company, Salisbury, North Caroline.
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Environmental Data Management, Inc.
Well Name
EX01
EX02
EX03 ········"•" EX04 ..•.....
NS05
Table 6
Water Level Measurements
Second Quarter 1997
Plume Periphery Wells
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (Ft. MSLJ (Ft.)
4/7/97 ' TOC 731.85 ' 143.4 .
---·--·-'.---4/7/97 TOC 718.24 83.1 ------•·••---
4/7/97 TOC 740.46 96.7 ' ... ... . . .. ·•· ..
4/7/97 TOC 754.12 181.77 ................. -. ................... .........
4/7/97 TOC 767.96 18.69 .........................
Water Level
Elevation
(Ft. MSLJ
588.45 ···-··-··-·-----···-·······-·-·
635.14 .. ------···········--··-···· 643.76
572.35
749.27
NS06 4/7/97 ----------'····· TOC 738.87 4.78 .............. 734.09. ···---...........................• ............. ----........... . ... . ...
NS21 4/7/97 TOC 739.13 4.45 734.68 •········· .. ···-··-········· ·······-...
NS22 ....... _). 4/7/97 TOC 715.94 21.9 694.04 ............. .,_, ___ ...........•.... ............ ·············-······ ..
NS23 ' 4/7/97 ' TOC 752.36 20.15 732.21
NS26 4/7/97 TOC 720.77 7.38 713.39 ....... ..• ................. ...... ., . ... .. .................
NS27 ····••.-!---4/7/97 TOC 749.47 16.74 732.73 ··········•···. .............................. , .... .. .......... ·····•·-:·· NS28 4/7/97 TOC 767.82 19.63 748.19 .. .. .. .. . .-.... .. ..,.
NS29 4/7/97 TOC 715.50 61.42 654.08 ··---•·· NS30 4/7/97 TOC 718.54 65.42 653.12 ····--·-·--···
NS31 4/7/97 TOC 711.15 58.8 652.35
"'"''"/""" .. . ............ , ... , ..... ... ' .......... , .... NA" -NA" NS32 4/7/97 TOC 699.48 ··--·····--······. •••••-••'·•••n ··-·-········-. -N.A.b .. NAb P01 4/7/97 TOC 708.09
SG1 4/7/97 TOC 712.26 1.63 710.63 ............... ·····•••· ·······••;••· ······· ··········· . ...... ..... ...................
SG2 4/7/97 TOC 693.90 1.77 692.13
NA• • Not Applicable, well is artesian.
NAb -Not Applicable, well is dry, or stream level not measured.
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Environmental Data Management, Inc.
Table 7
Water Level Measurements
Second Quarter 1997
Trench Area Wells
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to Water Level
Measurement Point of Elevation Water Elevation
Well Name Date Reference (Ft. MSL) (Ft.) (Ft. MSL)
EX05 4/7/97 TOC 781.26 32.53 748.73 ............... --------EX06 4/7/97 TOC 788.28 66.30 721.98 ········--···················-··-------.... ------···········-······· --···-··· ------------·-···· EX07 4/7/97 TOC 789.23 42.95 746.28 ······· .... ' .......... ............ .......
EX08 4/7/97 TOC 789.19 53.88 735.31 --··-··-··-............... ....... ····-................. ,.,_, __ .... , .
EX09 4/7/97 TOC 782.29 56.00 726.29 ----EX10 4/7/97 TOC 775.92 60.04 715.88 --········· ....... . ......... ......................... ..... ......... -----------.--------..... ..... •--m••····••••••• . ................
NS09 4/7/97 TOC 778.45 28.47 749.98 ·•··· .......... ,. ... ........ ... .. ·····-· . NS10 4/7/97 TOC 786.72 34.08 752.64 .................... ...... ···-· ········-···········•········ . ··•·· ···•···· .........•. ·······················-····-·· .. ·•······ NS11 4/7/97 TOC 775.65 19.66 755.99 ······· ········-······· ··••·••··· NS15 4/7/97 TOC 792.60 44.68 747.92
-------------------
GROI.JtJDWAl[R MOtllTQt<ltlG AR[A ($[[ fl(;UR[ I Oj
ror OPER"'8LE unns 1 6c 2
Environmental Data Management, Inc.
National Starch & Chemical Company
Cedar Springs Road
Salisbury, North Carolina
/ I
+ Monitoring Well
-Roads, Buildings, etc.
---Fence Line
rtttttt Railroad
-----Property Line
-Tributary Stream --n~-Topographic Contour Line
(F1., I.ASL) Contour ln\Nvol = 5F1.
0 400 800 1200
'""-,M..,l I I
Scale in Feet
Scale 1 Inch = 800 Feel
Site Map
2nd Quarter Report I 997
For
Operable Units I & 2
- -- - - - -- - - - --- -- -
Figure 2
Quarterly Summary of Acetone Concentration
100,000 ~-------------------------------------
92000
90,000 -l-------------------------1:' ~--------------
80,000 -!----------------------
70,000 -1----------------------~:si---------------!;:!Qtr3-'96
[] Qtr4-'96
E!I Qtr1-'97
■Qtr2-'97
'a, ::, 60,000 -1-----------------------➔~----------~----
.5
C 0
~ 50,000
c
8 § 40,000 -1-------
(J
30,000 -/------
20,000 -!------~
10,000 -1-------f::
12
0-1------~
EX01
EDN
Environmental Data Managemenl. Inc.
October 1997
EX02
660
EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
National Starch and Chemical Company
Salisbury, North Carolina
NS30
54000
•JOOO
NS31
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-m " < a·
" 3 <T> " 1i:
CJ ~
;::
0 " 0 '° <T>
3 <T> _a
',
0
- -
:::: "' ::,
.5
C
0 ~ -C .,
" C 0 0
-
10,000
1,000
100
10
1
- --
EX01 EX02
------ -
Figure 3
Quarterly Summary of 1,2 Dichloroethane
EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
Note: Concentrations depicted with an uterisk or al or below 5 ug/1 represent the detection limit of labor.ltory analysis method
EDN
Environmental Data Management, Inc.
October 1997
National Starch and Chemical Company
Salisbury, North Carolina
--
*
NS30
-
*
NS31
- -
. l:l Qtr3-'96
CII Qtr4-'96
E9 Qtr1-'97
Ii Qtr2-'97
5 ug/1 -Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-m ~ < er ~ 3 ~ ~
§:
Cl
9. 0 s: 0 ~ 0 <O ~ 3 ~ ."-
:, ,,
-------- -- - - - - -
Figure 4
Quarterly Summary of 1,2 Dichloropropane
10,000
1,000
,:: 01 :::,
.5
C 0 ., . 100 I! -C ., ... C 0
0
10
1
EX01 EX02 EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
Note· Concentrations depicted with an astensk or at or below 6 ug/1 represent the detection limit of laboratory anillys.is method
EDN
Environmental Data Management, Inc.
October 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -
NS30
-
NS31
- -
Ill Qtr3-'96
[]Qtr4-'96
Ell Qtr1-'97
Iii Qtr2-'97
Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-m ~ < er ~ 3
<!) ~ §:
a g_
0
,::
0 ~ 0 <O <!)
3
<!) _a
5' 0
- -
:::
"' :,
.!:
C
0 ! C: .,
u C 0 (J
EDN
- -
10,000
1,000
100
10
1
EX01
Environmental Data Management, Inc.
October 1997
- -
EX02
- -- - --.. Figure 5
Quarterly Summary of Bis(2-chloroethyl)ether
EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
National Starch and Chemical Company
Salisbury, North Carolina
--
NS30
-
NS31
--
Ill Qtr3-'96
[] Qtr4-'96
E!I Qtr1-'97
■Qtr2-'97
5,g/1
_Cleanup Concentrabon
Quarterly Reporl For
Operable Units No. 1 & 2
2nd Quarter 1997
-
- -- - - - -- - ----- - -- -
Figure 6
Quarterly Summary of Acetone Concentration
120,000 ~-------------------------------------
100,000 +----------------------
80,000
::: "' :,
.5
C 0 ., 60,000 f! -C .,
u C 0 u
40,000
20,000 -1-------1
EX05
EDN
Environmental Data Management, Inc.
Octobe, 1997
3,500 ug/l Groundwater Cleanup Cone.
EX06 EX07 EX0B
Monitoring and Extraction Wells -Trench Area
National Starch and Chemical Company
Salisbury, North Carolina
EX09 EX10
Isl Qtr3-'96
[]Qlr4-'96
E!I Qtr1-'97
■Qtr2-'97
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-m :, < a· :,
3
II) :, [
0 ~ ,:
a :, a <□ II)
3
II) _a
- --------1!!11!1!!!1 !!!1!!!11
Figure 7
Quarterly Summary of 1,2 Dichloroethane
1,000,000
100,000
10,000
.:,:
CIJ :,
·= C 0 :;::: 1,000 I!! -C .. u C 0 u
100
10
1
EX05 EX06 EX07 EX0B
Monitoring and Extraction Wells -Trench Area
Note: Concentrations depicted with an asterisk or at or below 5 ug/1 represent the detecilon timrt of ~boratory analysis method
EDN
Environmental Data Managemenl. Inc.
October 1997
National Starch and Chemical Company
Salisbury, North Carolina
EX09
liili
EX10
liiii liiiiil
Ill Qtr3-'96
I] Qtr4-'96
Ea Qtr1-'97
■Qtr2-'97
5 ug/1 . Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-
--·--- - --1!!!11
Figure 8
Quarterly Summary of 1,2 Dichloropropane
100,000
10,000
=:: Cl 1,000 :::,
.5
C
0 .,
I! .. C .. u C 100 0 (J
10
1
EX0S EX06 EX07 EX0B
Monitoring and Extraction Wells -Trench Area
Note: Concentrations depicted with an asterisk or at or below 6 ug/1 rep,esent the detection limit of laboratory analY5is method.
EDR
Environmental Data Management, Inc.
October 1997
National Starch and Chemical Company
Salisbury, North Carolina
lilliil
EX09
liii
EX10
liili liiliiil
!:'I Qtr3-'96
CD Qtr4-'96
Im Qtr1-'97
■Qtr2-'97
6 ug/1 -Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-
- ---- - -- - --Figure 9
Quarterly Summary of Bis(2-chloroethyl)ether
100,000
10,000
"" 01 1,000 :,
.5
C 0 .: I!! ... C .,
u C 100 0 u
10
1
EX05 EX06 EX07 EX0B EX09
Monitoring and Extraction Wells • Trench Area
Note. Concentr.itions depicted with an asterisk 01 at or belO'w 5 ug/1 represent the detection limit of labon1tory an.itys.is method
EDN
Environmental Data Management, Inc.
October 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -
EX10
--
lil!Qtr3-'96
IDQtr4-'96
EIIQtr1-'97
■Qtr2-'97
5 ,g/1
Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-
- - - --
. '
0 200 400 "'-•.l
' Scale in Feet
Scale l Inch ~ 400
Roads, Buildings, etc.
Fence Line
Property Line
Tributary Stream
600
' Feel
-
(
-7 2 s -Groundwater Contour Lme (Ft MSU + ♦ 'v
Monitoring Well
New Startup Extraction Wells
Stream Gauge
\
-
Stream
Gauge
- - - - -
I
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National Starch & Chemical Company
Cedar Springs !Road
Salisbury, North Carolina
Environmental Data Management, Inc.
-
. '
-
.......
- --·-
NS!5
+
/ I
PLMJ1 AREA
□
Figure 10
Groundwater Contour Map
for April 7, 1997
2nd Quarter Report 1997
For
Operable Units I & 2
-
- -
i ... "' a.
* It:
- -
40
25
20
- - --- -- - - --Figure 11
Individual Periphery Wells Pumping Rate
. ~.~ -
....................... ·••····· ··•···········•·--··•--)GGSSSaa aaaO(
•
Individual periphery wells
·· shutdown for scheduled
maintenance.
~ ···•···• •••• •---1---·j-;······•• ................. .
_, • ' ' '·ooooooc• )000 e EMh )8(
-
•
)(
--
• EX01
--o--EX02
-A-· EX03
-l(---EX04
"' C: ·s. 15 . □·
E ::,
11.
EDN
' ..
II p •
11 □ .
□ p
1 0 +□:a:nrnoa:ia:mrncnn:mcri11JC•JC■ x, x1■a, ··················'·;'· b·· . ·····p□□··· . ····~ ........ •p□□□□m ·ClCD□□ .. c;i tua:xrn IPiiliidlHIIPH ■iO liiiliidi
..
•'
5 -J ................................ ······· .......................... ······· ............................ ·················· ························ ............ ·················· □·············· ....... .. ········ ....... .
0 -H-H--HH-H-t·-t-H-H-t-t-t-t-++++-tt+t+-t-H--HH-H-t-t-++++-H+t+t-H-H--HH-H-t-t-+-t-++++-tt-t-t-H-H--HH-H-t-t-t-•t-t-t-t-H--t-t-H
~#~~##~###~#ft~#~$~#~g##~#~~~~~ ~~~~~~~~##$~~~~~~~~#4V~~~~~#~~#
Quarter 1 -1997 (January, February, March)
Environmental Data Management, Inc.
October, 1997
National Starch and Chemical Company
Salisbury, North Carolina
Quarterly Repor1 For
Operable Units No. 1 & 2
2nd Quar1er 1997
-m :, <
Cf :,
3
<l) :, ii
0 0 0
;::
0 :,
0 co <l)
3
<l)
-" :,
!°'
- -- - - ------· -- --
90
80
::i: IL C, 70
C:
~ 0 >< 60 w
..;
0 >< w 50 N 0 >< LL! -40 0 >< !!:!.
i 30 a:
"' C: 'ii 20 E :,
IL
10
0
EDN
Figure 12
Combined Periphery Wells Pumping Rate
Periphery well system
~---------------------------------!shutdown for scheduled maintenance.
~i\~~o,,ae uo,i\p~•~,
··························--·-···················-·-·•····························-•····----·················-·-·····························-··· .. ····-··················----••·--·---············
,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._ ,.._
"' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' -~ - - -co -;;i -- -
;;, - -
;;i - -- - -
;;i -ci5 - - --t: a <') "' .,, co -<D "' .,, co -... ,.._ .,, -... ,.._ - -----N N !::! <') ;;i ;;i ;;i ---;;j N ;;j -;;, ;;, ------- - - - - --;;i ;;i ;;i ;;i <') -----------<') <') <')
Quarter 1 -1997 (January, February, March)
Environmental Data Management. Inc.
October, 1997
National Starch and Chemical Company
Salisbury, North Carolina
,.._
"' -a N -<')
-
,.._ ,.._ ,.._
"' "' "' -co a; <')
!::! N N - -
<') <') <')
---
I~-Combined Rate I
Quarterly Report For
Operable Units No. 1 & 2
2nd Quarter 1997
-m
" < a·
" 3 ffl " [
0 ~ s: 0 " 0 co ffl 3 ffl _a
" !'
z !!l. 5· ::,
"' (/) -"' (/) ~6>"
C" cl C: ::r -< "' z a
0 (") ;:,. ::r
::r "' (") 3 "'-· a£
5()
"'0
3
"O "' ::,
'<
Pumping Rate (EX05,EX06,EX07,EX08,EX09,andEX10) in GPM 0 ... O> 00 1/1/97 +--_,_----"---'----J_-___J_ __ ,.__--'----'--------l 1/4/97 1/7/97 1/10/97 --1/13/97 _,
1/16/97
1/19/97
1/22/97
1/25/97
0 1/28/97
C
1/31/97 Ill ~
:_ 2/3/97
-2/6/97 ... !!: 2/9/97
-
.:: Ill 2/12/97 t ::, . & 2/15/97
~ 2/18/97 .,,
& 2/21/97 ... ! 2/24/97:
-, 2/27/97 ., a,, .,
!:n 3/2/97 : ., .:: 3/5/97
3/8/97
3/11/97
3/14/97
3/17/97
3/20/97 L
L 3/23/97 ,t
L 3/26/97 t
3/29/97 L L
+ (")
0
3
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ct> C.
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•
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i
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Appendix A
Report of Laboratory Analysis
Plume Periphery Wells and Trench Area Wells
·1
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Pace Analytical
Pace Analytical Services, Inc.
1700 Elm Street • Suite 200
Minneapolis, MN 55414
June 9, 1997
Mr. Ken Kluttz
National Starch & Chemical
Sample Delivery Group 4635 Narrative
Tel: [phone]
Fax: [phone]
Enclosed are the analytical results representing the analysis of 6 water samples
received at Pace Analytical Services April 8, 1997. All samples were analyzed
following the 8/94 revision of the CLP Statement of Work (SOW) for Organics,
document OLM03.0 and ILM03.0 for lnorganics. The M flag was used on the
raw data to indicate where manual integrations have occurred. Please note the
following comments concerning the sample analysis.
CLP Volatile Analyses
Holding Times. All samples were analyzed within CLP holding times.
GC/MS Tunjng. All BFB tuning criteria were met prior to the
analysis.of calibration standards and samples.
Instrumental Calibrations. All instrument.al calibrations met CLP criteria
and all continuing calibrations met CLP criteria with the following
exceptions:
The continuing calibration analyzed 04/17/97 at 1819 reported two
outliers, which is allowed under CLP guidance. Vinyl Chloride, however,
was reported at 40.4% Difference, which exceeds the 40% criteria. The
data were accepted based on the holding time constraints of all the
samples remaining to be analyzed.
Method Blanks. The method blank analyzed with the samples met
OLM3.0CLP criteria.
Surrogate Recoveries. All calculated surrogate recoveries met
OLM3.0CLP criteria, with the following exceptions:
Sample
NS-05
NS-05DL
1,2-Dichloroethane-d4
115%
115%
QC limit
76-114%
76-114%
· Since the recoveries were elevated with a positive bias and the results
. were replicated, the data were accepted.
Pace Analytical
Pace Analytical Services, Inc.
1700 Elm Street -Suite 200
Minneapolis, MN 55414
Internal Standard Response. All internal standard responses were
within the QC limits established by the daily calibration standard.
MS/MSP An MS/MSD was not required for this SDG.
Tel: [phone]
Fax: [phone]
Laboratory Control Sample. An LCS was analyzed for this SDG on
each day of analysis and met all OLM3.0CLP criteria. The LCS was also
evaluated for every compound and acceptable recoveries were reported
except for Bromomethane in VBLK107MS {130%) and VBLK108MSD
{128%). Since the results were elevated creating a positive bias, the data
were accepted.
Analysis comments. The samples were analyzed on a J&W Scientific
60M 0.32ID OB624 capillary column with a 1.8uM film thickness. The
trap used was a Supelco Purge Trap "K" with Carbopack/Carboxen
1000/1001. The samples were analyzed two times per the request of the
client and dilutions were performed from historical data.
CLP Semivolatile Analyses
Holding Tjmes. All samples were extracted and analyzed within CLP
holding times.
GC/MS Tuning. All DFTPP tuning criteria were within limits prior to the
analysis of calibration standards and extracts.
Instrumental Calibrations. All instrumental calibrations were within CLP
criteria, with the following exceptions:
Toe continuing calibration analyzed on 05/19/97 at 1639 reported
numerous outliers, but the samples were analyzed as they were going
outside of holding times the following day. Toe original, most concentrated
analysis was reported under CLP compliance.
Method Blanks. Toe method blank was within CLP criteria.
Surrogate Recoveries. All calculated surrogate recoveries were within
CLP quality control limits.
Internal Standard Response. Samples EX-10, EX-07, EX-06 reported elevated
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internal standard responses, which may have biased the results low. The solutions I
utilized to spike the extracts had concentrated and were not noticed until after sample
analysis. Pace-Minnesota has implemented a shorter expiration time and shelf life on
the vials of the internal standard solution to avoid this situation in the future. I
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Pace Analytical Services, Inc.
1700 Elm Street -Suite 200
Pace Analytical Minneapolis. MN 55414
Tel: [phone]
Fax: [phone]
Matrix Spikef Pupncate There was insufficient sample volume to perform an MS/MSD
on a sample from this SDG. These samples were extracted with the samples from
SDG 4649. Please refer to the LCS/LCSD portion of this narrative for comments.
LCS/LCSP Recoveries All recoveries were within the CLP MS/MSD QC
limits with the following exception:
SBLK100MSD OC-L!MII
2,4-Dinitrotoluene 118% 22-105%
The RPO between the LCS and LCSD were outside of QC limits.
Analysis Comments. An E-flag was utilized to denote analytes that
exceeded the calibration range of the analytical system. A B-flag was
utilized to denote analytes that were detected in the method blank as well
as the associated samples. A O-flag was utilized to denote analytes that
were diluted. The U-flag denotes an unidentified analyte and its
corresponding reporting limit.
There were significant amounts of tentatively identified compounds. Please
refer to the Form 1 E in the raw data package.
CLP Metals
Holding Times. All samples were prepared and analyzed within CLP
holding times.
Instrument CaHbratjons. All instrument calibrations met CLP criteria
prior to the analysis of samples.
initial and Continuing Calibration Verificatjons. All initial and
continuing calibration verification standards are within specified control
limits with the following exceptions:
Sodium CCV was outside of control limits and affected samples were
reanalyzed with proper dilutions. Antimony ICV was outside of control
limits and affected samples were analyzed on trace ICP.
Initial and Continuing Calibration Blanks. All initial and continuing
calibration blanks are within specified control limits.
Method Blanks. The method blank results are within specified control
limits.
pace Analytical
Pace Analytical Services, 1nc.
1700 Elm Street -Suite 200
Minneapolis, MN 55414
. Tel: [phone]
Laboratory Control Samples, All laboratory control sample results ate: s12-s11-6444
within specified control limits.
Matrjx Duplicate Results, All matrix duplicate results are within specified
control limits.
Matrix Spike Results. All matrix spike results are within specified control
limits.
Serial DHutjon. Serial dilution results are within specified control limits.
Analysis Comments. In order to accommodate the six character
limitation for the EPA sample 1.0., the client sample 1.0.s were modified
as necessary. Full sample 1.0.s are listed on form 1's.
"I certify that this data package is in compliance with the terms and conditions of
the contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package
and in the computer readable data submitted on diskette has been authorized by
the laboratory manager designee, as verified by the following signature."
Sincerely,
~V.OJL-
Jo<>dgo&i ·
Account Executive
Date
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-

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--·--

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--

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Sheetl
rtJ
Client: National Starch & Chemical (Pace Charlotte)
Project: Trench Wells
Program: EPACLP-3.0
SDG: 4635
Due: Full PackaQe due S.'!illlf s 12117 -
EDD: EPA CLP Fonnat A plus excel file of results -
Hard Copv: Level IV Include all raw data ~
Case: NA •. •
Contract: NA
PM: LAA -
e[!1111,1 ea"1 t111. ~ll!!al l,D, Qc. Mi!ldl! Sam11l11. Oalfl. BtHt Qatt• ~Le-llQA eJ:I !;;Le-SllQQ r1 P Uafolc (TAl I 1ST
10562 4635.8 EX-05 X(METALS) water 4/8/97 4/8/97 X X X X
10562 4636.6 EX-06 water 4/8/97 4/8/97 X X X X
10562 4637.4 EX-07 water 4/8/97 4/8/97 X X X X
10562 4641.6 EX-08 water 4/8/97 4/8/97 X X X X
10562 4642.4 EX-09 waler 4/8/97 4/8/97 X X X X
10562 4643.2 EX-10 water 4/8/97 4/8/97 X X X X
• Received at Charlotte
lnoraanic QC -Metals oerfonn LCS, MS, and DUP / Choose a different sample for the HG MS and DUP .
Oraanic QC -Perfonn LCS / LCSD
I .
NOTE: MULTIPLE DILUTIONS ARE REQUIRED FOR VOLATILE AND SEMIVOLA TILE ANALYSES
REFER TO HISTORICAL DATA FOR APPROXIMATE DILUTIONS
I I I
VOLATILES: ALL SAMPLES IN THIS SDG REQUIRE lWO REPORTED DILUTIONS
I
SEMIVOA: SAMPLES EX-06, EX-07, AND EX-10 REQUIRE lWO REPORTED DILUTIONS
,:: 5·
~
~~ I,':
"' 0 ~~ -~ NN ,:: (Jl u,
NA z
tr~ ~ w~ '.t! w~ -,A N "" w N
Page 1
Pace Analytical
Pace Analytical Services, Inc.
1700 Elm Street -Suite 200
Minneapolis, MN 55414
June 9, 1997
Mr. Ken Kluttz
National Starch & Chemical
Sample Delivery Group 4649 Narrative
Tel: [phone]
Fax: [phone]
Enclosed are the analytical results representing the analysis of 13 water samples
received at Pace Analytical Services April 8, 1997. All samples were analyzed
following the 8/94 revision of the CLP Statement of Work (SOW) for Organics,
document OLM03.0 and ILM03.0 for lnorganics. The M flag was used on the
raw data to indicate where manual integrations have occurred. Please note the
following comments concerning the sample analysis.
CLP Volatile Analyses
Holding Times. All samples were analyzed within CLP holding times.
GC/MS Tunjng. All BFB tuning criteria were met prior to the
analysis of calibration standards and samples.
Instrumental Calibrations. All instrumental calibrations met CLP criteria
and all continuing calibrations met CLP criteria with the following
exceptions:
The continuing calibration analyzed 04/15/97 at 0908 reported two
outliers, which is allowed under CLP guidance. Vinyl Chloride, however,
was reported at 40.4% Difference, which exceeds the 40% criteria. The
data were accepted based on the holding time constraints of all the
samples remaining to be analyzed.
Method Blanks. The method blank analyzed with the samples met
OLM3.0CLP criteria.
Surrogate Recoveries. All calculated surrogate recoveries met
OLM3.0CLP criteria, with the following exceptions:
Sample 1,2-Dichloroethane-d4
VBLK105MS 118%
EX-04 115%
NS-10 117%
NS-10DL 121%
QC limit
76-114%
76-114%
76-114%
76-114%
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Pace Analytical Services, Inc.
1700 Elm Street -Suite 200 Pace Analytjcal , . ,., '• Minneapolis, MN 55414
Tel: [phone]
Since the recoveries were elevated, thus creating a positive bias, the dat1112-617-6444
were accepted. ·
· Internal Standard Response. All internal standard responses were
within the QC limits established by the daily calibration standard.
MS/MSD Sample EX-01 was injected with matrix spike. All recoveries
were within OLM3.0 CLP criteria.
Laboratory Control Sample. An LCS was analyzed for this SDG on
each day of analysis and met all OLM3.0CLP criteria. The LCS was also
evaluated for every compound and acceptable recoveries were reported.
Analysis comments. The samples were analyzed on a J&W Scientific
60M 0.32ID D8624 capillary column with a 1.BuM film thickness. The
trap used was a Supelco Purge Trap "K" with Carbopack/Carboxen
1000/1001. The samples were analyzed two times per the request of the
client and dilutions were performed from historical data.
CLP Semivolatile Analyses
Holding Times. All samples were extracted and analyzed within CLP
holding times.
GC/MS Tuning. All DFTPP tuning criteria were within limits prior to the ·
analysis of calibration standards and extracts.
Instrumental Calibrations. All instrumental calibrations were within CLP
criteria
Method Blanks. The method blank was within CLP criteria.
Surrogate Recoveries. All calculated surrogate recoveries were within
CLP quality control limits.
Internal Standard Response. All internal standard responses were within QC limits,
with the following exceptions:
SBLK101
NS-15
NS-09
NS-31
Perylene-d 12
Napthalene-dB
Perylene-d 12
Acenapthene-d10, Chrysene-d12, Perylene-d12
Pace Analytical Services, lnc. I
• 1700 Elm Street -Suite 200 pace Analyt1cal Minneapolis, MN 55414
Tel: [phone] I
All the samples reported a diminished response due to matrix interfereooeSJ2·TI1t!4Method
blank reported a diminished response due to probable glassware contamination. The
associated LCS/LCSD and sample reported acceptable responses. I
I Matrix Spjke/Dup(jcate Sample EX-01 was utilized as the MS/MSD sample and
reported the following outliers:
4-Nitrophenol
2,4-Dinitrotoluene
EX-01MS
88%
104% ,
EX-01MSD
84%
100%
OC-UMII
10-80%
24-96%
I
Since the results were reported with a positive bias, the data were accepted. I
LCS/LCSD Recoveries All recoveries were within the CLP MS/MSD QC I
limits with the following exceptions:
SBLK100MSD OC-UMII
2,4-Dinitrotoluene 118% 22-105%
Analysis Comments. An E-flag was utilized to denote analytes that
exceeded the calibration range of the analytical system. A B-flag was
utilized to denote analytes that were detected in the method blank as well
as the associated samples. A D-flag was utilized to denote analytes that
were diluted. The U-flag denotes an unidentified analyte and its
corresponding reporting limit.
There were significant amounts of tentatively identified compounds. Please
refer to the Form 1 E in the raw data package
CLP Metals
Holding Times. All samples were prepared and analyzed within CLP
holding times.
Instrument Ca(jbratjons. All instrument calibrations met CLP criteria
prior to the analysis of samples.
Initial and Continuing Calibration Verifications, All initial and
continuing calibration verification standards are within specified control
limits.
Initial and Continuing Calibration Blanks, All initial and continuing
calibration blanks are within specified control limits.
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Pace Analytical Services, Inc.
1700 Elm S1reet -Suite 200 pace Anaiytjcal Minneapolis. MN 55414
Tel: [phone]
Method Blanks. The method blank results are within specified contralax: 612·617-6444
limits.
Laboratory Control Samples, All laboratory control sample results are
within specified control limits.
Matrix Duplicate Results. All matrix duplicate results are within specified
control limits.
Matrix Spike Results. All matrix spike results are within specified control
limits with the following exception: The spike recovery for Manganese
was 68.2% (75-125) the post spike recovery was 158 %.
Serial Dilution. Serial dilution results are within specified control limits
with the following exception:
The serial dilution % difference result for Iron on sample E32697
exceeded 10%. indicating matrix and/or spectral interference. Forms 1
and 9 are flagged with an "E".
Analysis Comments. In order to accommodate the six character
limitation for the EPA sample I.D., the client sample I.D.s were modified
as necessary. Full sample I.D.s are listed on form 1 's.
"I certify that this data package is in compliance with the terms and conditions of
the contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package
and in the computer readable data submitted on diskette has been authorized by
the laboratory manager designee, as verified by the following signature."
Sincerely,
J~:6fr·
Account Executive
•
Pace Analytical
June 10, 1997
Mr. Ken Kluttz
National Starch & Chemical
Sample Delivery Group 1273 Narrative
Pace Analytical Services, Inc.
1700 Elm Street • Suite 200
Minneapolis, MN 55414
Tel: 612·617-6400
Fax: [phone]
Enclosed are the analytical results representing the analysis of 22 water
samples received at Pace Analytical Services May 22, 1997. All samples
were analyzed following the 8/94 revision of the CLP Statement of Work
(SOW) ILM03.0 for lnorganics. Please note the following comments
concerning the sample analysis.
CLP Metals
Holding Times, All samples were prepared and analyzed within CLP
holding times.
Instrument Calibrations, All instrument calibrations met CLP criteria
prior to the analysis of samples.
Initial and Continuing Calibration Verifications, All initial and
continuing calibration verification standards are within specified control
limits. '
Initial and Continuing Calibration Blanks, All initial and continuing
calibration blanks are within specified control limits.
Method Blanks. The method blank results are within specified control
limits.
Laboratory Control Samples, All laboratory control sample results are
within specified control limits.
Matrix Duplicate Results, All matrix duplicate results are within specified
control limits.
Analysis Comments, In order to accommodate the six character
limitation for the EPA sample 1.0., the client sample 1.O.s were modified
as necessary. Full sample 1.O.s are listed on form 1's.
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"I certify that this data package is in compliance with the terms and conditions of
the contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package
and in the computer readable data submitted on diskette has been authorized by
the laboratory manager designee, as verified by the following signature."
Sincerely,
~Q~ JohPodgki
Account Executive
C -/o. <J 1-
Date
Sheet1
Client: National Starch & Chemical (Pace Charlotte)
Project: Quarterly Monitoring Wells
Program: EPACLP-3.0
SDG: 4649
Due: Full Packane due~ < /2./q7
EDD: EPA CLP Format A plus excel file of results
Hard Conv: Level IV Include all raw data
Case: NA
Contract: NA
PM: LAA
~ ea,e: ~Q. Cli1tnl I.I:!, ~ Mmill Samgle: Date Be:~ Datft* CLe-1/QA fl:! CLe-Sl/QC !:;Le M1tlill1i {IAL LISI)
10563 4649.9 EX-01 X water 4f7/97 4/8/97 X X X X
10563 4650.7 EX-01DUP water 4f7/97 4/8/97 X X X x.
10563 4651.5 EX-02 water 4f7/97 4/8/97 X X X X
10563 4652.3 EX-03 water 4f7/97 4/8/97 X X X X
10563 4653.1 EX-04 water 4f7/97 4/8/97 X X X X
10563 4654.9 NS-09 water 4/8/97 4/8/97 X X X X
10563 4655.6 NS-10 water 4/8/97 4/8/97 X X.' X X
10563 4656.4 NS-11 water 4/8/97 4/8/97 X X X X
10563 4657.2 NS-15 water 4f7/97 4/8/97 X X X X
10563 4658.0 NS-29 water 4f7/97 4/8/97 X X X X
10563 4659.8 NS-30 water 4f7/97 4/8/97 X X X . X
10563 4660.6 NS-31 water 4f7/97 4/8/97 X X X X
10563 4661.4 NS-32 water 4f7/97 4/8/97 X X X X
• Received at Charlotte .
lnorQanic QC -Metals perform LCS, MS, and DUP / Choose a different samole for the HG MS and DUP
Oraanic QC -Perform LCS and MS/MSD
I
NOTE: MULTIPLE DILUTIONS ARE REQUIRED FOR VOLATILE AND SEMIVOLATILE ANALYSES
REFER TO HISTORICAL DATA FOR APPROXIMATE DILUTIONS
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VOLATILES: SAMPLES EX--02, EX--03, EX--04, NS--09, NS-10, NS-29, and NS-31REQUIRE TWO REPORTED DILUTIONS
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SEMIVOA: SAMPLES EX--02, EX--03, EX--04, NS-29, and NS-31 REQUIRE TWO REPORTED DILUTIONS I
Page 1 - -- - ------------ - - -
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Appendix B
Volatile Organics Analysis Data Sheets
Plume Periphery Wells
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.: I Matrix: (soil/water) WATER I Sample wt/vol:
Level: (low/med) I% Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0. 32 (mm)
Contract:
SAS No.:
EX-01
SDG No.: 4649
Lab Sample ID: 4649.9
Lab File ID: 10-10508
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (UL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chlorornethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3-c-------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55c6---------l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichlorornethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibrornochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoforrn --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
4 JB
10 u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture,· noi:. dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0.32 (mm)
E:X-01 Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4649.9
Lab File ID: 10-10508
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
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Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (ut
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l _______ 1_ol_u __
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FORM I VOA
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OLM03. 0 I
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VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.: I Matrix: (soil/water) WATER I Sample wt/vol:
Level: (low/med) I %-Moisture: not dee.
5.000 (g/mL) ML
LOW
Contract:
SAS No.:
Lab
Lab
Date
Date
EPA SAMPLE NO.
EX-0lDUP
SDG No.: 4649
Sample ID: 4650.7
File ID: 10-10604
Received: 04/08/97
Analyzed: 04/16/97
GC Column: DB624 ID : 0 . 3 2 (mm) Dilution Factor: 1.0 I Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene
67-64-1---------Acetone
Chloriae
75-15-0---------Carbon bisulb.cle
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroetnane
78-93-3---------2-Butanone
71-55~6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75°27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dicfiloropropene
75-25-2---------Bromoform --
108-10-1-------~4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroetnene
79-34-5--------cl,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
10
10
10
10
10
5
10
10
10
10
10
3
10
10
10
10
3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Q
u u u u u
JB u u u u u
J u u u u
J u u u u u u u u u u u u u u u u
(uL
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I
I
FORM I VOA OLM03.0
lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.:
EX-0lDUP
SDG No.: 4649
Lab Sample ID: 4650.7
Lab File ID: 10-10604
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ f _______ 1_of_u __
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FORM I VOA OLM03. ol
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I
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I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.:
Matrix: (soil/water) WATER
EPA SAMPLE NO.
EX-02
I Sample wt/vol:
Level: (low/med)
5.000 (g/mL) ML
LOW
SDG No.: 4649
Lab Sample ID: 4651.5
Lab File ID: 10-10611
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0
I % Moisture: not dee.
GC Column: DB624 ID: 0. 3 2 (mm)
I Soil Extract Volume: (uL) ----Soil Aliquot Volume:
I
I
I
I
I
I ,1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene
67-64-1---------Acetone
Chlon.de
75-15-0---------Carbon Disulb.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--~-----l,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6------~--l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
250
250
250
250
250
7500
250
250
250
250
250
290
250
250
250
250
190
250
250
250
250
250
250
250
250
250
250
250
110
250
250
250
250
----
Q
u u u u u
EB u u u u u
u u u u
J u u u
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u u u u
u
u u
J u u
u u
(uL
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FORM I VOA OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water)' WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: O. 32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.:
EX-02
SDG No . : 4 6 4 9
Lab Sample ID: A651.5
Lab File ID: 10-10611
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ J
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FORM I VOA OLM03, 01
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02DL
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
Level: (low/med) LOW
%-Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4651.SDL
Lab File ID: 10-10610
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 200.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 2000 u 74-83-9---------Bromomethane 2000 u
75-01-4---------Vinyl Chloride 2000 u
75-00-3---------Chloroethane 2000 u 75-09-2---------Methylene Chloride 2000 u 67-64-1---------Acetone 7800 DB
75-15-0---------Carbon Disulfide 2000 u
75-35-4---------1,1-Dichloroethene 2000 u 75-34-3---------1,1-Dichloroethane 2000 u 540-59-0--------1,2-Dichloroethene ( total) 2000 u -67-66-3---------Chloroform 2000 u 107-06-2--------1,2-Dichloroethane 2000 u
78-93c3---------2-Butanone 2000 u
71-55-6---------1,1,1-Trichloroethane 2000 u
56-23-5---------Carbon Tetrachloride 2000 u
75-27-4---------Bromodichloromethane 2000 u 78-87-5---------1,2-Dichloropropane 2000 u
10061-01-5------cis-l,3-Dichloropropene 2000 u
79-01-6---------Trichloroethene 2000 u
124-48-1--------Dibromochloromethane 2000 u
79-00-5---------1,1,2-Trichloroethane 2000 u 71-43-2---------Benzene 2000 u 10061-02-6------trans-1,3-Dichloropropene 2000 u 75-25-2---~-----Bromoform --2000 u 108-10-1--------4-Methyl-2-Pentanone 2000 u 591-78-6--------2-Hexanone 2000 u 127-18-4--------Tetrachloroethene 2000 u
79-34-5---------1,1,2,2-Tetrachloroethane 2000 u --108-88-3--------Toluene 2000 u 108-90-7--------Chlorobenzene 2000 u 100-41-4--------Ethylbenzene 2000 u 100-42-5--------Styrene 2000 u 1330-20-7-------Xylene (total) 2000 u
FORM I VOA OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
~ Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID:. 0. 32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
EX-02DL
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4651.SDL
Lab File ID: 10-10610
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 200.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 2000 U
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FORM I VOA OLM03.0I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES
Case No.: I Lab Code: PACE
Matrix: (s·oil/water) WATER
I
I
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
EX-03
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3
Lab File ID: 10-10609
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0 I Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
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I '
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I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
-
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75~01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55~6-----~---1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform ·
108-10-1------~-4-Methyl-2-Pentanone
591-78-6----~---2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
250 u
250 u
250 u
250 u
250 u
10000 EB
250 u
250 u
250 u
250 u
250 u
240 J
250 u
250 u
250 u
250 u
240 J
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
160 J
250 u
250 u
250 u
250 u
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID : 0 . 3 2 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
EX-03
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3
Lab File ID: 10-10609
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l 250 ju __ _
FORM I VOA OLM03.0
I
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' I
I
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I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
:I Lab Name: PACE ANALYTICAL SERVICES
EX-03DL
Contract:
I
••
.I
I
I ,.
I
I
I
I
I
I
I
I
I
I
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Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3DL
Lab File ID: 10-10608
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 100.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (uL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3-------c-Chloromethane
74-83-9---------Bromomethane
75-01-4~--------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulride
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55"6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1---c----4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroechene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
1000 u
1000 u
1000 u
1000 u
1000 u
12000 DB
1000 u
1000 u
1000 u
1000 u
1000 u
310 DJ
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
EX-03DL
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3DL
Lab File ID: 10-10608
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 100.0
I
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I
I
I
Soil Extract Volume: (uL) -----Soil Aliquot Volume: __ (ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene
FORM I VOA
1000 U
Q I
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OLM03.0I
I
I
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I
I
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4653.1 I Sample wt/vol:
( low/med)
5.000 (g/mL) ML
LOW
Lab File ID: 10-10513
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
Level: I% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
I Soil Extract Volume: (uL) Soil Aliquot Volume:
I
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I
-----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3-------~-Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55C6------~--l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene '
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene ..
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
10
3
10
8
10
2500
24
10
10
10
10
6
14
10
10
10
17
10
10
10
10
2
10
10
4
10
10
10
33
4
4
10
10
-----
Q
u
J u
J u
EB
u
u u u
J
u
u u
u
u u u
J u
u
J u
u u
J
J u
(uL
I
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I
FORM I VOA OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
EX-04
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4653.1
Lab File ID: 10-10513
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l _______ 1_ol_u __
FORM I VOA OLM03.0
I
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I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES EX-04DL
Contract:
I Lab Code: PACE
Matrix:
Case No.:
(soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4653.lDL I Sample wt/vol:
Level: (low/med)
5.000 (g/mL) ML
LOW
Lab File ID: 10-10605
I
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Date Received: 04/08/97·
% Moisture: not dee. Date Analyzed: 04/16/97
GC Column: DB624 ID: 0.32 (mm) Dilution Factor: 20.0
Soil Extract Volume: (uL) -----Soil Aliquot Volume: _____ (uL
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 200 u 74-83-9---------Bromomethane 200 u 75-01-4---------Vinyl Chloride 200 u 75-00-3---------Chloroethane 200 u 75-09-2---------Methylene Chloride 200 u 67-64-1---------Acetone 2200 DB 75-15-0---------Carbon Disulfide 200 u 75-35-4---------1,1-Dichloroethene 200 u 75-34-3---------1,1-Dichloroethane 200 u 540-59-0--------1,2-Dichloroethene (total) ,200 u 67-66-3---------Chloroform -200 u 107-06-2--------1,2-Dichloroethane 200 u 78-93-3------c--2-Butanone · 200 u 71-55~6---------1,1,1-Trichloroethane 200 u 56-23-5---------Carbon Tetrachloride 200 u 75-27-4---------Bromodichloromethane 200 u 78-87-5---------l,2-Dichloro1ropane 200 u 10061-01-5------cis-l,3-Dich oropropene 200 u 79-01-6---------Trichloroethene 20,0 u 124-48-1--------Dibromochloromethane 200 u 79-00-5---------1,1,2-Trichloroethane 200 u 71-43-2---------Benzene 200 u 10061-02-6------trans-l,3-Dichloropropene 200 u 75-25-2---------Bromoform --200 u 108-10-1--------4-Methyl-2-Pentanone 200 u 591-78-6--------2-Hexanone 200 u 127-18-4--------Tetrachloroethene 200 u 79-34-5---------1,1,2,2-Tetrachloroethane --200 u 108-88-3--------Toluene 200 u 108-90-7--------Chlorobenzene 200 u 100-41-4--------Ethylbenzene 200 u 100-42-5--------Styrene 200 u 1330-20-7-------Xylene ( total) 200 u
FORM I VOA OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
-----
ID: 0.32 (mm)
Soil Extract Volume: (uL) --.---
CAS NO. COMPOUND
EX-04DL
Contract:
SAS No. SDG No.: 4649
Lab Sample ID: 4653.lDL
Lab File ID: 10-10605
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 20.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l
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FORM I VOA OLM03.0I
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I
lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4658.0 I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10615
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I
I
Level: (low/med)
% Moisture: not dee.
GC Column: DB624 ID : 0 . 3 2 (mm)
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 50.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (UL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.cte
67-64-1---------Acetone
75-15-0---------Carbon Disulride
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
15-27-4---------Brcimodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
500 u
500 u
500 u
500 u
500 u
33000 EB
500 u
500 u
500 u
500 u
500 u
680
500 u
500 u
500 u
500 u
980
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
260 J
500 u
500 u
500 u
500 u
OLM03.0
--------------------------------------------
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-29
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: ( low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4658.0
Lab File ID: 10-10615
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 50.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ 500 U
FORM I VOA OLM03.0
I
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I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-29DL
Lab Code: PACE Case No.: ' Matrix: ·(soil/water) WATER I Sample wt/vol:
Level: (low/med) I% Moisture: not dee.
_GC Column: DB624
5.000 (g/mL) ML
LOW
ID: O. 32 (mm)
SAS No.: SDG No.: 4649
Lab Sample ID: 4658.0DL
Lab File ID: 10-10614
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 500.0
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Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3-------~-2-Butanone
71-55~6------~--l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform ·
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
5000 u
5000 u
5000 u
5000 u
5000 u
37000 DB
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
1100 DJ
5000 u
500.0 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
·sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.:
NS-29DL
SDG No.: 4649
Lab Sample ID: 4658.0DL
Lab File ID: 10-10614
Date Received:. 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ 5000 U
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I FORM I VOA OLM03.0
I
I
1. lA 2PA SAMPL2 NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
.Lab Name: PACE ANALYTICAL SERVICES
NS-30
Contract:
,, Lab Code: PACE
Matrix: (soil/water)
Case No.: SAS No.: SDG No.: 4649
I Sample
Level:
wt/vol:
(low/med)
WATER
5. 000 (g/mL) ML
LOW
Lab Sample ID: 4659.8
Lab File ID:
Date Received:
10-10506
04/08/97
,:I%-Moisture: not dee. Date Analyzed: 04/15/97
Dilution Factor: 1.0 GC Column: DB624 ID: 0.32 (mm) I Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
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C.l>.S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2----~---l,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10~1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5~-------Styrene
1330-20-7-------Xylene (total)
10
10
10
10
10
4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
----
Q
u u u u u
JB u u u u u u u u u
u
u u u u u u u u u u u u u u u u u
(uL
I
I
I
FORM I VOA OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0.32 (mm)
Contract:
SAS No.:
NS-30
SDG No.: 4649
Lab Sample ID: 4659.8
Lab File ID: 10-10506
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
I
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Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l ______ 1_ol_u __
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FORM I VOA OLM03. 01
I
I
lA EPA SAMPLE :'JO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-31
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4660.6 I Sample wt/vol:
Level: (low/med)
5. 000 (g/mL) ML
LOW
Lab File ID: 10-10613
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 100.0
1· % Moisture: not dee.
GC Column: DB624 ID: 0. 32 (mm)
I Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75°27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,l,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
1000
1000
1000
1000
1000
43000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
370
1000
1000
1000
1000
----
Q
u u u u u
EB u u u u u u u u u u u u u u u u u u u u u u
J u u u u
(uL
,,
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I
FORM I VOA OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/wat:er) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 3 2 (mm)
NS-31
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4660.6
Lab File ID: 10-10613
I
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I
Soil Extract Volume: ____ (uL)
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 100.0
Soil Aliquot Volume: ____ (ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene __
FORM I VOA
Q
1000 U
I
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I
I
OLM03. 01
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-31DL
I
I
I
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5 :000 (g/mL) ML
LOW
ID: 0.32 (mm)
SAS No.: SDG No.: 4649
Lab Sample ID: 4660.6DL
Lab File ID: 10-10612
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 250.0 I Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane .
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene ( total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform · --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
2500 u
2500 u
2500 u
2500 u
2500 u
30000 DB
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
OLM03.0
-lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
· Soil Extract Volume : ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.:
NS-31DL
SDG No.: 4649
Lab Sample ID: 4660.6DL
Lab File ID: 10-10612
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 250.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 2500 U
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FORM I VOA OLM03.0I
I
I
I lA EPA SAMPLS NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
Case No.: I Lab Code: PACE
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
I % Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0.32 ( mm)
Contract:
SAS No.:
NS-32
SDG No.: 4649
Lab Sample ID: 4661.4
Lab File ID: 10-10507
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0 I Soil Extract Volume : _____ (uL) Soil Aliquot Volume: ____ (uL
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D
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 10 u
67-64-1---------Acetone 3 JB
75-15-0---------Carbon Disulfide 10 u
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
540-59-0--------1,2-Dichloroethene (total) 10 u
67-66-3---------Chloroform -10 u
107-06-2--------1,2-Dichloroethane 10 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
56-23-5---------Carbon Tetrachloride 10 u
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-l,3-Dichloropropene 10 u
79-01-6---------Trichloroethene 10 u
124-48-1--------Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
10061-02-6------trans-l,3-Dichloropropene __ 10 u 75-25-2---------Bromoform 10 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 10 u
79-34-5---------1,1,2,2-Tetrachloroethane 10 u --108-88-3--------Toluene 10 u 108-90-7--------Chlorobenzene 10 u 100-41-4--------Ethylbenzene 10 u 100-42-5--------Styrene 10 u
1330-20-7-------Xylene (total) 10 u
FORM I VOA OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
NS-32 Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4661.4
Lab File ID: 10-10507
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ J _______ 1_oi_u __
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FORM I VOA OLM03.0I
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••
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Appendix B
Volatile Organics Analysis Data Sheets
Trench Area Wells
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-05
Contract:
I Lab Code: PACE
Matrix: (s•oil/water) WATER
Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4635.8
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10723
Level: (low/med)
I % Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 200.0 I Soil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (UL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
2000
2000
1200
660
2000
33000
2000
2000
2000
2000
2000
107-06-2--------1,2-Dichloroethane 390000
78-93~3---------2-Butanone 2000
71-55-6---------1,1,1-Trichloroethane 2000
56-23-5---------Carbon Tetrachloride 2000
75-27-4---------Bromodichloromethane 2000
78-87-5---------1,2-Dichloropropane 2000
10061-01-5------cis-l,3-Dichloropropene 2000
79-01-6---------Trichloroethene 2000
124-48-1--------Dibromochloromethane 2000
79-00-5---------1,1,2-Trichloroethane 2000
71-43-2---------Benzene 2000
10061-02-6------trans-l,3-Dichloropropene 2000
75-25-2---------Bromoform --2000
108-10-1--------4-Methyl-2-Pentanone 3800
591-78-6--------2-Hexanone 2000
127-18-4--------Tetrachloroethene 2000
79-34-5---------1,1,2,2-Tetrachloroethane 2000 --108-88-3--------Toluene 23000
108-90-7--------Chlorobenzene 2000
100-41-4--------Ethylbenzene 2000
100-42-5--------Styrene 2000
1330-20-7-------Xylene (tocal) 2000
FORM I VOA
Q
u
u
J
J
u
B
u u u u u
E u u u
u u u u
u
u u u u
u u u
u u u u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0 . 3 2 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.:
EX-05
SDGNo.: 4635
Lab Sample ID: 4635.8
Lab File ID: 10-10723
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 200.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 2000 U
FORM I VOA OLM03.0
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g /mL)
Level: (low/med) LOW
Contract:
SAS No.:
ML
EX-05DL
SDG No.: 4635
Lab Sample ID: 4635.BDL
Lab File ID: 10-10722
: I % Moisture: not dee.
Date Received: 04/0B/97
Date Analyzed: 04/18/97
Dilution Factor: 5000.0
Soil Aliquot Volume:
GC Column: DB624 ID: 0.32 (mm) I Soil Extract Volume: ____ (uL)
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I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-B7-3---------Chloromethane
74-B3-9---------Bromomethane --------
75-01-4---------Vinyl Chlori e
75-00-3---------Chloroethane --------
75-09-2---------Methylene Chloride
67-64-1---------Acetone -----
75-15-0---------Carbon Disulfide 75-35-4---------1,1-Dichloroethe_n_e _____ _
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene~(~t-o~t-a~l-)-
67-66-3---------Chloroform 107-06-2--------1,2-Dichlo~r-o-e~t'h_a_n_e _____ _
7B-93-3---------2-Butanone ----------71 -55 - 6 - - - - - - - - -l, l, l -Tri ch Io roe thane
56-23-5---------Carbon Tetrachloride----
75-27-4---------Bromodichloromethane ----7B-87-5---------1,2-Dichloropropane 10061-01-5------cis-l,3-Dichloropro_p_e_n_e __ _
79-01-6---------Trichloroethene
124-48-l--------Dibromochlorome~t~h~a-n~e-----
79-00-5---------1,l,2-Trichloroethane ___ _
71-43-2---------Benzene 10061-02-6------trans-1-,=3--~D~i-c~h-l_o_r_o_p_r_o_p_e_n_e __
75-25-2---------Bromoform~~~---------_-
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone ----
127-18-4--------Tetrachloroethene 79-34-5---------1,1,2,2-Tetrachlo_r_o_e~t-h_a_n_e __
108-88-3--------Toluene 108-90-7--------Chlorobe_n_z_e_n_e _______ _
100-41-4--------Ethylbenzene ---------100-42-5--------Styrene 1330-20-7-------Xylene '(~t~o~t~a~I~)~-------
FORM I VOA
50000
50000
50000
50000
50000
160000
50000
50000
50000
50000
50000
470000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
50000
21000
50000
50000
50000
50000
____ (UL
Q
u u u u u
DB u u u u u
D u u u u u u u u u u u u u u u u
DJ u u u u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-05DL
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: DB624 ID: 0.32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4635.8DL
Lab File ID: 10-10722
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 5000.0
Soil Aliquot Volume:
.CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 50000 U
FORM I VOA OLM03.0
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
EPA SAMPLE NO.
EX-06
I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4636.6
I
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I
I
I,
I
I
I
I
Matrix: (soil/water)
Sample wt/vol:
Level: "(low/med)
,_
0 Moisture: not dee.
GC Column: DB624
WATER
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Lab File ID: 10-10617
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 1.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (uL
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloricte 3 J
75-00-3~--------Chloroethane 10 u
75-09-2---------Methylene Chlon.de 10 u
67-64-1---------Acetone 380 EB
75-15-0---------Carbon Disulfide 10 u
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
540-59-0--------1,2-Dichloroethene (total) 10 u
67-66-3---------Chloroform -10 u
107-06-2--------1,2-Dichloroethane 490 E
78-93-3---------2-Butanone 8 J
71-55-6---------1,1,1-Trichloroethane 10 u
56-23-5---------Carbon Tetrachloride 10 u
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-1,3-Dichloropropene 10 u
79-01-6---------Trichloroethene 10 u
124-48-1--------Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
10061-02-6------trans-1,3-Dichloropropene 10 u
75-25-2---------Bromoform --10 u
108-10-1--------4-Methyl-2-Pentanone 89
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 10 u
79-34-5---------1,1,2,2-Tetrachloroethane 10 u
108-88-3--------Toluene --37
108-90-7--------Chlorobenzene 10 u
100-41-4--------Ethylbenzene 10 u
100-42-5--------Styrene 10 u
1330-20-7-------Xylene (total) 10 u
FORM I VOA OLM03.0
'
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (s6il/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.:
EX-06
SDG No . : 4 6 3 5
Lab Sample ID: 4636.6
Lab File ID: 10-10617
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l _______ 1_ol_u __
FORM I VOA OLM03.0
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4636.6DL
Sample wt/vol: 5.000 (g/mL) ML Lab File ID: 10-10616
Level: (low/med) LOW
% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Soil Extract Volume: (uL)
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 10.0
Soil Aliquot Volume: ____ (UL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloria:e
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon D1.sulf1.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93~3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5------c--Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-D1.chloropropene
75-25-2---------Bromoform · --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
100 u
100 u
100 u
100 u
100 u
470 DB
100 u
100 u
100 u
100 u
100 u
530 D
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
90 DJ
22 DJ
100 u
100 u
38 DJ
100 u
100 u
100 u
100 u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
EX-06DL
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4636.6DL
Lab File ID: 10-10616
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 10.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l
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I
. I OLM03.0 FORM I VOA
I
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I
I
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:.
Matrix: (soil/water) WATER
Contract:
SAS No.:
EX-07
SDG No.: 4635
Lab Sample ID: 4637.4
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10619
Level: (low/med) I% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm) I Soil Extract Volume: ____ (uL)
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (UL
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I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloricte
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------Carbon Disulb.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93°3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5----~----l,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
250 u
250 u
250 u
250 u
250 u
4000 B
250 u
250 u
250 u
250 u
250 u
35000 E
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
2500
250 u
250 u
250 u
1200
250 u
250 u
250 u
250 u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Contract:
SAS No.:
EX-07
SDG No.: 4635
Lab Sample ID: 4637.4
Lab File ID: 10-10619
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 25.0
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I
Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (url
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene __ l
FORM I VOA
Q
250 \u_. __
OLM03.0
I
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I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-07DL
Lab Name: PACE ANALYTICAL SERVICES I Lab Code: PACE Case No.:
Matrix: (s'oil/water) WATER
I Sample wt/vol:
Level: (low/med) I% Moisture: not dee.
5. 000 (g/mL) ML
LOW
GC Column: DB624 ID: 0.32 (mm)
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4637.4DL
Lab File ID: 10-10618
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 1000.0 I Soil Extract Volume : ____ (uL) Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND. CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------l,2-Dichloro1ropane
10061-01-5------cis-l,3-Dich oropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------strrene
1330-2007-------Xy ene (total)
FORM I VOA
Q
10000 u
10000 u
10000 u
10000 u
10000 u
10000 DB
10000 u
10000 u
10000 u
10000 u
10000 u
35000 D
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
2100 DJ
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07DL
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: noc dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 32 (mm)
Soil Excract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4637.4DL
Lab File ID: 10-10618
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 1000.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 10000 U
FORM I VOA OLM03.0
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I lA EPA SAMPLE NO ..
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-08
Lab Name: PACE ANALYTICAL SERVICES Contract: I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4641.6 I Sample wt/vol: 5.000 (g/mL) ML Lab File ID: 10-10721
Level: (.low/med) LOW Date Received: 04/08/97
I % Moisture: not dee. Date Analyzed: 04/18/97
GC Column: DB624 ID: 0.32 (mm) Dilution Factor: 500.0 I Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane 5000
74-83-9---------Bromomethane 5000
75-01-4---------Vinyl Chloriae 5000
75-00-3---------Chloroethane 5000
75-09-2---------Methylene Chloride 5000
67-64-1---------Acetone 100000
75-15-0---------Carbon Disulfide 5000
75-35-4---------1,1-Dichloroethene 5000
75-34-3---------1,1-Dichloroethane 5000
540-59-0--------1,2-Dichloroethene (total) 5000
67-66-3---------Chloroform -5000
107-06-2--------1,2-Dichloroethane 29000.0
78-93-3---------2-Butanone 5000
71-55-6---------1,1,1-Trichloroethane 5000
56-23-5---------Carbon Tetrachloride 5000
75-27-4---------Bromodichloromethane 5000
78-87-5---------1,2-Dichloropropane 5000
10061-01-5------cis-l,3-Dichloropropene 5000
79-01-6---------Trichloroethene 5000
124-48-1--------Dibromochloromethane 5000
79-00-5---------1,1,2-Trichloroethane 5000
71-43-2---------Benzene 5000
10061-02-6------trans-l,3-Dichloropropene 5000 75-25-2---------Bromoform --5000
108-10-1--------4-Methyl-2-Pentanone 33000
591-78-6--------2-Hexanone 5000
127-18-4--------Tetrachloroethene 5000
79-34-5---------1,1,2,2-Tetrachloroethane 5000 --108-88-3--------Toluene 24000
108-90-7--------Chlorobenzene 5000
100-41-4--------Ethylbenzene 5000
100-42-5--------Styrene 5000
1330-20-7-------Xylene ( total) 5000
FORM I VOA
Q
u u
u
u u
EB u u u
u
u
E u u
u
u u u u
u
u u u u
u u
u
u
u u u
OLM03.0
lA EPA SAMPLE NO. I
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol: 5. 000 (g/m.L) ML
Level: (low/med). LOW
% Moisture: not dee.
GC Column: DB624 ID : 0 . 3 2 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.:
EX-08
SDG No.: 4635
Lab Sample ID: 4641.6
Lab File ID: 10-10721
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ 5000 U
FORM I VOA
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OLM03.0
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-08DL
Lab Name: PACE ANALYTICAL SERVICES I Lab Code: PACE Case No.:
Matrix: (soil/water) WATER I Sample wt/vol: 5. 000 (g/m_L) ML
Level: (low/med) LOW I% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Contract:
SAS No.: SDG No . : 4 6 3 5
Lab Sample ID: 4641.6DL
Lab File ID: 10-10720
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 2500.0 I Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane 25000
74-83-9---------Bromomethane 25000
75-01-4---------Vinyl Chloricte 25000
75-00-3---------Chloroethane 25000
75-09-2---------Methylene Chloride 25000
67-64-1---------Acetone 130000
75-15-0---------Carbon Disulfide 25000
75-35-4---------1,1-Dichloroethene 25000
75-34-3---------1,1-Dichloroethane 25000
540-59-0-------~l,2-Dichloroethene (total) 25000
67-66-3---------Chloroform -25000
107-06-2--------1,2-Dichloroethane 290000
78-93-3------~--2-Butanone 25000
71-55-6---------1,l,l-Tricfiloroethane 25000
56-23-5----~----Carbon Tetrachloride 25000
75-27-4---------Bromodichloromethane 25000
78-87-5---------1,2-Dichloropropane 25000
10061-01-5------cis-l,3-Dichloropropene 25000
79-01-6---------Trichloroethene 25000
124-48-1--------Dibromochloromethane 25000
79-00-5---------1,1,2-Trichloroethane 25000
71-43-2---------Benzene 25000
10061-02c6------trans-l,3-Dichloropropene 25000
75-25-2---------Bromoform --25000
108-10-1--------4-Methyl-2-Pentanone 30000
591-78-6--------2-Hexanone 25000
127-18-4--------Tetrachloroethene 25000
79-34-5---------1,1,2,2-Tetrachloroethane 25000
108-88-3--------Toluene --22000
108-90-7--------Chlorobenzene 25000
100-41-4--------Ethylbenzene 25000
100-42-5--------Styrene 25000
1330-20-7-------Xylene (total) 25000
FORM I VOA
Q
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OLM03.0
lA
VOLATILE ORG.l'..NICS .l'..NALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE .l'..NALYTICAL SERVICES EX-08DL
Lab Code: PACE Case No.:
Matrix: (s·oil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: DB624 ID: 0. 32 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
Contract:
SAS No.: SDG No.: 4635
·Lab Sample ID: 4641.6DL
Lab File ID: 10-10720
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 2500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ 25000 U
FORM I VOA OLM03.0
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I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET I Lab Name: PACE ANALYTICAL SERVICES I Lab Code: PACE Case No.:
Matrix: (soil/water) WATER I Sample wt/vol: 5.000 (g/mL) ML
Level: (low/med) LOW I% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
EX-09
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4642.4
Lab File ID: 10-10804
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 250.0 I Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (UL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74~83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
2500
2500
2500
2500
2500
40000
2500
2500
2500
2500
2500
107-06-2--------1,2-Dichloroethane 130000
78-93-3---------2-Butanone 2500
71-55-6---------1,1,1-Trichloroethane 2500
56-23-5---------Carbon Tetrachloride 2500
75-27-4---------Bromodichloromethane 2500
78-87-5---------1,2-Dichloropropane 9100
10061-01-5------cis-l,3-Dichloropropene 2500
79-01-6---------Trichloroethene 2500
124-48-1--------Dibromochloromethane 2500
79-00-5---------1,1,2-Trichloroethane 2500
71-43-2---------Benzene 2500
10061-02-6-----ctrans-l,3-Dichloropropene 2500
75-25-2---------Bromoform --2500
108-10-1--------4-Methyl-2-Pentanone 5700
591-78-6--------2-Hexanone 2500
127-18-4--------Tetrachloroethene 2500
79-34-5---------1,1,2,2-Tetrachloroethane 2500 --108-88-3--------Toluene 20000
108-90-7--------Chlorobenzene 2500
100-41-4--------Ethylbenzene 2500
100-42-5--------Styrene 2500
1330-20-7-------Xylene (total) 1000
FORM I VOA
Q
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u u
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OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
EX-09
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4642.4
Lab File ID: 10-10804
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 250.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene 2500 U
FORM I VOA OLM03.0
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I Lab
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09DL
Name: PACE ANALYTICAL SERVICES Contract: I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4642.4DL Matrix: (soil/water) WATER I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10803
Level: (low/med) ·I% Moisture: not dee.
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 1000.0 GC Column: DB624 ID: 0. 32 (mm) I Soil Extract Volume: ____ (uL) Soil Aliquot Volume:
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1·
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon D1.sult1.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
10000
10000
10000
10000
10000
42000
10000
10000
10000
10000
10000
107-06-2--------1,2-Dichloroethane 130000
78-93c3---------2-Butanone 10000
71-55-6---------1,1,1-Trichloroethane 10000
56-23-5---------Carbon Tetrachloride 10000
75-27-4---------Bromodichloromethane 10000
78-87-5---------1,2-Dichloropropane 9300
10061-01-5------cis-l,3-Dichloropropene 10000
79-01-6---------Trichloroethene 10000
124-48-1--------Dibromochloromethane 10000
79-00-5---------1,1,2-Trichloroethane 10000
71-43-2---------Benzene 10000
10061-02-6------trans-l,3-Dichloropropene 10000
75-25-2---------Bromoform --10000
108-10-1--------4-Methyl-2-Pentanone 4900
591-78-6--------2-Hexanone 10000
127-18-4--------Tetrachloroethene 10000
79-34-5---------1,1,2,2-Tetrachloroethane 10000 --108-88-3--------Toluene 20000 108-90-7--------Chlorobenzene 10000
100-41-4--------Ethylbenzene 10000
100-42-5--------Styrene 10000
1330-20-7-------Xylene (total) 10000
----
Q
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FORM I VOA OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5. 000 (g/mL) ML
LOW
GC Column: DB624 ID: 0.32 (mm)
Contract:
SAS No.:
EX-09DL
SDG No.: 4635
Lab Sample ID: 4642.4DL
Lab File ID: 10-10803
Date Received: 04/08/97
Date Analyzed: 04/18/97
Dilution Factor: 1000.0
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Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ (uJ
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene
FORM I VOA
10000 U
Q
OLM03.0
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I lA EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-10
Lab Name: PACE ANALYTICAL SERVICES Contract:
I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4643.2 I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10715
Level: (low/med) Date Received: 04/08/97 I% Moisture: not dee. Date Analyzed: 04/17/97
I GC Column: DB624 ID: 0.32 (mm) Dilution Factor: 500.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volu~e:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2--------~Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------strrene
1330-20-7-------Xy ene (total)
5000
5000
5000
5000
5000
92000
5000
5000
5000
5000
5000
30000
5000
5000
5000
5000
56000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
12000
5000
1800
5000
5800
----
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FORM I VOA OLM03.0
lA EPA SAMPLE NO. I
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VOLATILE ORG~.NICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: DB624 ID: 0.32 (mm)
EX-10
Contract:
SAS No.: SDG No.: 4635
.Lab Sample ID: 4643.2
Lab File ID: 10-10715
Date Received: 04/08/97
Date Analyzed: 04/17/97
Dilution Factor: 500.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: __ ,ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-1,2-Dichloroethene
FORM I VOA
5000 U
Q I
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OLM03.0
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.:
EX-l0DL
SDG No. : 4 6 3 5
Lab Sample ID: 4643.2DL I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: 10-10714
Level: (low/med)
I % Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Date Received: 04/08/97
Date Analyzed: 04/17/97
Dilution Factor: 1000.0 I Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) ·uG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chlorioe
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon D1.sulf1.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-9303---------2-Butanone
71-55C6---------l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-D1.chloropropene ·
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7----·----Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10000 u
10000 u
10000 u
10000 u
10000 u
99000 DB
10000 u
10000 u
10000 u
10000 u
10000 u
30000 D
10000 u
10000 u
10000 u
10000 u
56000 D
10000 u
1000.0 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
13000 D
10000 u
1900 DJ
10000 u
4700 DJ
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
.5.000 (g/mL) ML
LOW
Contract:
SAS No.:
EX-l0DL
SDG No.: 4635
Lab Sample ID: 4643.2DL
Lab File ID: 10-10714
Date Received: 04/08/97
Date Analyzed: 04/17/97
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ID: 0. 32 (mm)
Soil Extract Volume: ____ (uL)
Dilution Factor: 1000.0 __ (ul Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene
FORM I VOA
10000 U
Q
OLM03.0
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lA
VO_LATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.:
NS-09
SDG No . : 4 6 4 9
Lab Sample ID: 4654.9 I Sample
Level:
wt/vol:
(low/med)
5.000 (g/mL) ML
LOW
Lab File ID: 10-10607
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 10.0
I% Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm) I Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4----0 ----Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene
67-64-1---------Acetone
Chloride
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
100
100
49
24
100
94
100
100
100
100
100
4100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
80
100
100
100
100
____ (UL
Q
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JB
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E u
u u u u
u
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u u u u u u u
u u
J u
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u
u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Contract:
SAS No.:
NS-09
SDG·No.: 4649
Lab Sample ID: 4654.9
Lab File ID: 10-10607
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 10.0
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Soil Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (uJ
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene_· __ I
FORM I VOA
Q
OLM03.0
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I lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-09DL
I Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4654.9DL Matrix: (soil/water) WATER I Sample wt/vol:
Level: (low/med) I % Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 3 2 (mm)
Lab File ID: 10-10606
Date Received: 04/08/97
Date Analyzed: 04/16/97
Dilution Factor: 50.0 I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---0 -----Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulride 75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total) 67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-9303---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride 75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dicfiloropropene
75-25-2---------Bromoform --108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene . · .
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
500 u
500 u
500 u
500 u
500 u
360 DJB
500 u
500 u
500 u
500 u
500 u
4400 D
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
88 DJ
500 u
500 u
500 u
500 u
OLM03.0
lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Contract:
SAS No.:
NS-09DL
SDG No.: 4649
Lab Sample ID: 4654.9DL
Lab File ID: 10-10606
Date Received: 04/08/97
Date Analyzed: 04/16/97
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GC Column: DB624 ID: 0.32 (mm)
Soil Extract Volume: (uL) -----Soil Aliquot Volume:
Dilution Factor: 50.0 __ (uJ
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene __ l
FORM I VOA
Q
5ooj_u __
OLM03.0
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.000 (g/mL) ML
LOW
Contract:
SAS No.:
NS-10
SDG No.: 4649
Lab Sample ID: 4655.6
Lab File ID: 10-10515
I % Moisture: not dee.
Date Receiv~d: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 10.0 GC Column: DB624 ID: 0.32 (mm) I Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloricte
75-00-3----~----Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-~---------l,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
100
100
100
100
100
78
100
100
100
100
100
870
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
____ (uL
Q
u
u u u u
JB
u u u
u u
u u u u u u
u u
u u u u u
u u
u u u
u u u
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL. SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
Contract:
SAS No.:
NS-10
SDG No.: 4649
Lab Sample ID: 4655.6
Lab File ID: 10-10515
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 10.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
156-60-5--------trans-l,2-Dichloroethene __ l
FORM I VOA OLM03.0
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I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I NS-l0DL
Lab Name: PACE ANALYTICAL SERVICES Contract: I Lab Code : PACE Case No.: SAS No.: SDG No . : 4 6 4 9
Lab Sample ID: 4655.6DL
I
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
Lab File ID: 10-10516
I % Moisture: not dee.
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 25.0
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GC Column: DB624 ID: 0.32 (mm)
Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene ( total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55~6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5-----~---l,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-96-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene ( tot:al)
FORM I VOA
250
250
250
250
250
84
250
250
250
250
250
940
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
250
____ (UL
Q
u u u u u
DJB u u u u u
D u u u u u u u u u u u u u u u u u u u u u
OLM03.0
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. I
I
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Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0.32 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Contract:
SAS No.:
NS-l0DL
SDG No.: 4649
Lab Sample ID: 4655.6DL
Lab File ID: 10-10516
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 25.0
Soil Aliquot Volume: ____ (ul
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q I
156-60-5·~-------trans-l, 2-Dichloroethene __ J 250 J_u__ I
FORM I VOA OLM03.0
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES
I Lab Code: PACE Case No.:
Matrix: (soil/water) WATER I Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med) I % Moisture: not dee.
GC Column: DB624 ID: 0.32 (mm)
Contract:
SAS No.:
NS-11
SDG No.: 4649
Lab Sample ID: 4656.4
Lab File ID: 10-10504
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0 I Soil-Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (uL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene ( total) 67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55~6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
22 B
10 u
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
5 J
10 u
20
10 u
35
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0.32 (mm)
Contract:
SAS No.:
NS-11
SDG No.: 4649
Lab Sample ID: 4656.4
Lab File ID: 10-10504
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
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Soil Extract Volume: ____ (uL) Soil Aliquot Volume: _____ (ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene __ l
FORM I VOA
Q
OLM03.0
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I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.: I Matrix: (soil/water) WATER I Sample wt/vol:
Level: (low/med) I % Moisture: not dee.
GC Column: DB624
5. 000 (g/mL) ML
LOW
ID: 0.32 (mm)
NS-15
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4657.2
Lab File ID: 10-10505
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (UL
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)
67-66-3---------Chloroform -
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55c6---------l,l,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061~01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3-~------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
2 J
10 u
10 u
10 u
18
10 u
10 u
10 u
10 u
120
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
10 u
OLM03.0
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column: DB624
5.000 (g/mL) ML
LOW
ID: 0. 3 2 (mm)
NS-15
Contract:
SAS No.: SDG No.: 4649
Lab Sample ID: 4657.2
Lab File ID: 10-10505
Date Received: 04/08/97
Date Analyzed: 04/15/97
Dilution Factor: 1.0
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Soil· Extract Volume: (uL) -----Soil Aliquot Volume: __ (ul
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
156-60-5--------trans-l,2-Dichloroethene __ l
FORM I VOA
Q
OLM03.0
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Appendix C
Semivolatile Organics Analysis Data Sheets
Plume Periphery Wells
I '1'1B , ..... EPA SAMPLE NO.
I
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (~oil/water) WATER
Contract:
SAS No.:
EX-01
SDG No.: 4649
Lab Sample ID: 4649.9 I Sample wt/vol: 1000 (g/mL) ML Lab File ID: 11502
Level: (low/med) LOW
I % Moisture: decanted: _(Y /N)
Concentrated Extract Volume: lOOO(uL) I Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
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GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro~henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7------~-N-Nitroso-di-n-propylamine
67-72~1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitropheno~
105-67-9--------2,4-Dimethylphenol
111-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
~20-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methllnaphthalene
77-47-4---------Hexach oroc1clopentadiene
ss~oG-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethhlphthalate
208-96-8--------Acena~ thylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
21
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 .u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-01
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4649.9
Sample wt/vol: Lab File ID: 11502
Level: (low/med)
% Moisture:
10 0 0 ( g /TI)L) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N. pH: 7.0
CAS NO . COMPOUND ·
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01~6--------4-Nitroaniline
534-52./1--------4,6-Dinitro-2-methylphenoi
86-30-~---------N-Nitrosodiphenhlamine (l)=
101-55-3-----~--4-Bromophenyl-p enylether I -118-74-1--------Hexachlorobenzene , . I 87-86-5~,-------Pentachlorophenol
85-01-8~1-------Phenanthrene
120-12L7--------Anthracene ' I 86-74-B-~-------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00°-0'--------Pyrene
85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene ..
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
.
( J -Cannot be separated trom Dipnenylamine
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
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I lB EPA SAMPLE NO.
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I
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (s'oil/water) WATER
Contract:
SAS No.:
EX-02
SDG No.: 4649
Lab Sample ID: 4651.5
I Sample wt/vol: 950. 0 (g/1;1L) ML
LOW
Lab File ID: 11918
Level: (low/med) I % Moisture: decanted: (Y/N)
l000(uL)
Date Received: 04/08/97
.Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0 I
I
I
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I
R
I
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I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine ..
67-72,-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methllnaphthalene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
230 E
340 E
10 u
10 u
10 u
10 u
10 u
10 u
34
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-02
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (sbil/water) WATER
SAS No .. : SDG No.: 4649
Lab Sample ID: 4651.5
Sample wt/vol: Lab File ID: 11918
Level: (low/med)
% Moisture:
950.0 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
( )
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2 4-Dinitrophenol I ' I I 100-02-7--------4-Nitrophenol
132-64-9-~------Dibenzofuran
121-14-2-------~2,4-Dinitrotoluene
84-66-2·--, ------Diethylphthalate
7005-72~3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1-~------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenhlamine (l)=
101-55-3-----0 --4-Bromophenyl-p enylether
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8--~------Phenanthrene
120-12-7--------Anthracene
86-74-81_._,_ ------Carbazole
84-74-2'-'-I-------Di-n-butylphthalate
206-44i0-I-------Fluoranthene
129-00-0--------Pyrene
85-68-7~~-------Butylbenzrlphthalate
91-94-i-~-------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9-. -------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-cannot be sep arated from D h ip enylami ne
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
I
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (doil/water) WATER
Contract:
SAS No.:
EX-02
SDG No.: 4649
Lab Sample ID: 4651.5 I Sample wt/vol: 950.0 (g/mL) ML Lab File ID: 11918
I
I
I
I
I
I
I
I
I
I
D
m
Level: (low/med)
% Moisture:
LOW
decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
(Y /N)
1000 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane .
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
i20-82-l--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethylhhthalate
208-96-8--------Acena~ht ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
230 E
340 E
10 u
10 u
10 u
10 u
10 u
10 u
34
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
26 u
10 u
26 u
10 u
10 u
10 u
26 u
10 u
OLM03.0
lC EPA SAMPLE NO. I
I
I
I
I
I
I
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (~oil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4651.5
Sample wt/vol: Lab File ID: 11918
Level: (low/med)
% Moisture:
950.0 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84 -66-2--·-- - - - --Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-71-_:_ - - - - --Fluorene -, I 100-01-,6-•-- - - - --4-Nitroaniline
534-52-l~-------4,6-Dinitro-2-methylphenol
86-3 0-6--'-- - - - --N-Nitrosodiphenylamine ( 1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2-~-------Di-n-buthlphthalate
206-44-0------~-Fluorant ene
129-00-0a-------Pyrene
85-68-7---------Butylbenzllphthalate
91-94-l-~-------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2~-------Benzo(g,h,i)perylene
(1) -Cannot be separated tram Diphenylamine
FORM I SV-2
Q
26 u
26 u
10 u
10 u
10 u
10 u
10 u
26 u
26 u
10 u
10 u
10 u
26 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
I
I
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OLM03.0
I
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lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
EPA SAMPLE NO.
EX-02DL
I Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4651.5DL
I
Matrix: (sbil/water) WATER
Sample wt/vol:
Level: (low/med)
950. 0 (g/f;1L} ML
LOW
Lab File ID: 11916
I % Moisture: decanted: (Y/N)
l000(uL}
~ate Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0 I
:I
I
I
I
fl
m
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
111-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-o0 bis(l-Chloropropane)
106044-5--------4-Methy phenol ·
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane .-
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenoi
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4--------~Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7--------~2-C~loron~l~tha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
190 D
250 D
53 u
53 u
53 u
53 u
53 u
53 u
17 DJ
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
130 u
53 u
130 u
53 u
53 u
53 u
130 u
53 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-02DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4651.5DL
Sample wt/vol: Lab File ID: 11916
Level: (low/med)
% Moisture:
950.0 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
lOOO(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.0
( )
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2 107------Diethylphthalate ·
7005-72 13 1 ------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
'' 1 4 N" 100-01-60--------itroaniline
534-52-ill------4,6-Dinitro-2-methylphenol 86-30-6!_l ______ N-Nitrosodiphenhlamine (1)-•·-11 -101-55-3-1------4-Bromophenyl-p enylether __
118-74-1--------Hexachlorobenzene
I ' 87-86-5--0 ------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00-0--------Pyrene
85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
.218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24--2-- - - - - --Benzo (g, h, i) perylene
-Cannot be se p arated from Di hen p y lamine
FORM I SV-2
Q
130 u·
130 u
53 u
53 u
53 u
53 u
53 u
130 u
130 u
53 u
53 u
53 u
130 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
53 u
OLM03.0
I
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03
Lab Name: PACE ANALYTICAL SERVICES Contract: f Lab Code: PACE
Matrix: ( sbil/water) I' Sample wt/vol:
Case No.:
WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3
Lab File ID: 11921
Level: (low/med)
,, % Moisture:
· Concentrated Extract I Injection Volume:
1000 (g/mL) ML
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 4.0
I GPC
I/
I ,.
·1
'I
•
m
,I
••
I
I
1,
Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95~50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxibis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1------0 --Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7------~--4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine ,
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
160
180
40 u
40 u
40 u
40 u
40 u
40 u
12 J.
.40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
100 u
40 u
100 u
40 u
40 u
40 u
100 u
40 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-03 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (E!Oil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3
Sample wt/vol: Lab File ID: 11921
Level: (low/med)
%-Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7.0
( )
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5--a------2,4-Dinitrophenol
100-02-7-~------4-Nitrophenol
132-64-9-1------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2--~------Diethylphthalate
7005-72-3~------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6~~-------N-Nitrosodiphenhlamine (1)=
101-55·-3 - - - - -c --4-Bromophenyl-p enylether
118-74~1--------Hexachlorobenzene --
87-86-5°-0 ------Pentachlorophenol
85-01-sl-~------Phenanthrene , ' I 120-12-7,1------Anthracene
86-74-Sl--------carbazole
84-74-2~,t------Di-n-buthlphthalate
206-44-0~,------Fluorant ene
129-00-o-~------Pyrene
85-68-7--~------Butylbenzllphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3--,------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethllhexyl)phthalate
117-84-0-~------Di-n-octy phthalate -
205-99-2-----,--Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Can not be se p arated from Di p hen y !amine
FORM I SV-2
Q
100 u
100 u
40 u
40 u
40 u
40 u
40 u
100 u
100 u
40 u
40 u
40 u
100 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
OLM03.0
I
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I EX-03DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
,. Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3DL Matrix: (sbil/water) WATER I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11920
Level: (low/med) 1· % Moisture: decanted: (Y/N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0 I
I
I
I
I
I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxibis(l-Chloropropane)
106-44-5--------4-Methy phenol ·-.. -621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-NitrophenoL
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach orocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethhlphthalate
208-96-8--------Acena~ thylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
160 D
190 D
50 u
50 u
50 u
50 u
50 u
50 u
12 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
50 u
120 u
50 u
50 u
50 u
120 u
50 u
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-03DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case .No.:
Matrix: (sbil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4652.3DL
Sample wt/vol: Lab File ID: 11920
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)_. _
1000 (uL')
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.0
)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene 84-66-2c_c ______ Diethylphthalate I · I 7005-72-3-------4-Chlorophenyl-phenylether I I l -86-73-7---------F uorene . I I I 100-01-6~"------4-Nitroaniline
534-52-i~~------4,6-Dinitro-2-methylphenol
'. 1 • d' h 1 . ( )-86-30-Gt-,------N-Nitroso ip enh amine 1 _
101-55-3-------~4-Bromophenyl-p enylether
118-74-1--------Hexachlorobenzene --
87-86-5-----"---Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene • I 129-00-0-s------Pyrene
85-68-7~--------Butylbenzilphthalate
91-94-l~-L------3,3'-Dich orobenzidine
56-55-3~-~------Benzo(a)anthracene
218-01-9--------Chrysene
117-Bl-7-~------bis(2-Ethilhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2-~------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8-- - - - - - --Benzo (a) pyrene .•
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di p hen y lamine
FORM I SV-2
Q
120 u
120 u
50 u
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
OLM03.0
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04
Lab Name: PACE ANALYTICAL SERVICES Contract:
,, Lab Code : PACE Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4653.1 Matrix: (sbil/water) WATER , 1· Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11919
Level:. (low/med)
,, % Moisture: decanted: (Y/N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0
.,. ,,
I ,,
I
I
I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72cl------c--Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3 - - - - - - --.-Hexachlorobutadiene
59-50-7---------4-Chloro-3-methrlphenol .
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine ,
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
5 J
100 E
10 u
2 J
10 u
10 u
10 u
10 u
9 J
10 U'
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
lC EPA SAMPLE NO. I
I
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (sbil/water) WATER Lab Sample ID: 4653.1
Sample wt/vol: Lab File ID: 11919
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 1.0
GPC Cleanup: (Y /N) N pH: 7.0
.)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-7--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-0l-6-~------4-Nitroan1l1ne
534 -52-1/-:-1------4, 6 ~Dinitr<?-2-methy~phenol_
86-30-61~-------N-N1trosod1phenylam1ne (1)
101-55-3 -!-
1
---a --4 -Bromophenyl-phenylether -
118-74-~--------Hexachlorobenzene --
87-86-5~-~------Pentachlorophenol
85-01-8~-•------Phenanthrene 2 7 I h . 120-1 ---------Ant racene
86-74-8-'--'------Carbazole I , 84-74-2-,--, ------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00-0-~------Pyrene
85-68-7~--------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated from D1phenylam1ne
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
1.0 u
10 u
10 u
10 u
10 u
10 u
10 u
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04DL
Lab Name: PACE ANALYTICAL SERVICES Contract: , I Lab Code: PACE Case No. :
Matrix: (s'bil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4653.lDL
1· Sample wt/vol: 1000 (g/mL) ML Lab File ID: 11917
Level: (low/med) I· % Moisture:
, Concentrated Extract
·'· Injection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 04/08/97
.Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0 .,1. GPC Cleanup: (Y/N) N pH: 7.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
l
' ••
I
••
CAS NO. COMPOUND
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroetho~)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20~3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2 4 5-Trichloro1henol . ' ' 91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
50 u
74 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
50 u
120 u
50 u
50 u
50 u
120 u
50 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-04DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4653.lDL
Sample wt/vol: Lab File ID: 11917
Level: (low/med)
% MoiSture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.0
( )
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14 -2,-- - - - - --2, 4-Dinitrotoluene
84-66-2-~-~-----Diethylphthalate
7005-72-3 -·-- - - --4-Chlorophenyl-phenylether
86-73-7-l-~-----Fluorene . -
100-01-61~.:. _ - - - --4-Nitroan1.l1.ne
534-52-1.-- - - - - --4, 6-Dinitro-2-methylphenol
86-30-6-,-- - - - - --N-Nitrosodiphenhlamine ( 1) =
101-55-3.-- - - - - --4-Bromophenyl-p enylether
118-74 -1'--·-- - - --Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00-0--------Pyrene
85-68-7---------Butylbenzilphthalate
91-94-1---------3,3'-Dich orobenzidine
56~55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethilhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene ..
193-39-5--------Indeno(l,2,.3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-e Cannot bes p arated from D1. p hen y lam1.ne
FORM I SV-2
Q
120 u
120 u
50 u
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
5.0 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water} WATER
SActNo.: SDG No.: 4649
Lab Sample ID: 4658.0
Sample wt/vol: Lab File ID: 11923
Level: (low/med}
% Moisture:
1000 (g/mL} ML
LOW
decanted: (Y/N}
Concentrated Extract Volume: 1000 (uI,) · ·
Injection Volume: 2. 0 (uL}
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N} N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chloronaphtha ene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--0 -----Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
100
410
100 u . 100 u
100 u
100 u
100 u
100 u
22 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
100 u
250 u
100 u
100 u
100 u
250 u
100 u
OLM03.0
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-29 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4658.0
Sample wt/vol: Lab File ID: 11923
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uLl
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72"3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-e--------4-Nitroan1l1ne
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
I 1 -101-55-3.-~------4-Bromopheny •phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
250 u
250 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
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Lab Name: PACE ANALYTICAL SERVICES Contract: t Lab Code: PACE Case No. : SAS No.: SDG No.: 4649
· Matrix: (sbil/water) WATER Lab Sample ID: 4658.0DL
I' Sample wt/vol: Lab File ID: 11922
Level: (low/med)
I'%-Moisture:
Concentrated Extract I Injection Volume:
1000 (g/mL) ML
LOW
decanted: (Y /NI
Volume:
2. 0 (uL)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 20.0
·1·
·I·
I V
I
I·
I
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-7201---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach orocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chlorona1hthalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
69 DJ
530 D
200 u
200 u
200 u
200 u
200 u
200 u
21 DJ
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
500 u
200 u
500 u
200 u
200 u
200 u
500 u
200 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-29DL Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (sbil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
SAS No.:
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
SDG No.: 4649
Lab Sample ID: 4658.0DL
Lab File ID: 11922
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 20.0
GPC Cleanup: (Y/N) N pH: 7.0
,.)
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5~-c------2,4-Dinitrophenol
100-02-7-0 ------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72~3:..------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenhlamine (1)-
101-55-3--------4-Bromophenyl-p enylether -
118-74-[-'...------Hexachlorobenzene --
87-86-5L_l ______ Pentachlorophenol
85-01-8~-~-•----Phenanthrene
120-12 -,7-- - - - - --Anthracene
86-74-8~1-------Carbazole
84 -74 -21--,-- - ----Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-oo-lo-!---- - --Pyrene
85-68-~--;-------Butylbenzrlphthalate
91-94-~--:-------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di p hen y lamine
FORM I SV-2
Q
500 u
500 u
200 u
200 u
200 u
200 u
200 u
500 u
500 u
200 u
200 u
200 u
500 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
OLM03.0
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
EPA SAMPLE NO.
NS-30
f Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4659.8
I ,,
t .,,
,,
Matrix: (soil/water) WATER
Sample wt/vol: Lab File ID: 10757
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/11/97
Date Analyzed: 04/17/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---~-----2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
--
91-58-7---------2-Chlorona1hthalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethhlphthalate
208-96-8--------Acenap thylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
7 J
19
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
-----------------------------------------------
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
NS-30
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4659.8
Sample wt/vol: Lab File ID: 10757
Level: (low/med)
% Moisture:
1000 (g/rnL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/11/97
Date Analyzed: 04/17/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5C--------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9----0 ---Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3"------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100"01-6-C------4-Nitroaniline
534-52-i-.~------4,6-Dinitro-2-methylphenol
86-30-6~-~------N-Nitrosodiphenylamine (1)-
I I -101-55-6-r------4-Bromophenyl-phenylether
118-74-i-r------Hexachlorobenzene --
87-86-5L--------Pentachlorophenol
85-01-8~~~------Phenanthrene
120-12-7--------Anthracene
86-74-8~-~------Carbazole
84-74-2--(------Di-n-buthlphthalate
206-44-0--------Fluorant ene
129-00-~-:-------Pyrene
85-68-7---------Butylbenzrlphthalat~
91-94-1-~-------3,3 -Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene _
193-39-5--------Inderio(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
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OLM03.0
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q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.:
NS-31
SDG No.: 4649
Lab Sample ID: 4660.6 I Sample wt/vol: 1000 (g/mL) ML Lab File ID: 11925
Level: (low/med) LOW ,, % Moisture: decanted: (Y /N)
Concentrated Extract Volume: 100 O (uL)
·I, Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 2.0
I
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro~henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-C~loron~~~thalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimechylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
20 u
400 E
20 u
20 u
20 u
20 u
20 u
20 u
22
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
50 u
20 u
50 u
20 u
5 J
20 u
50 u
20 u
OLM03.0
lC EPA SAMPLE NO. I
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4660.6
Sample wt/vol: Lab File ID: 11925
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (ul'.,)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 2.0
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol _____ _
100-02-7--------4-Nitrophenol 132-64-9--------Dibenzofuran --------
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate -----
7005-72;-~~------4-Chlorophenyl-phenylether
86-73-71--'-------Fluorene .-100-01-6~-------4-Nitroa_n_i_l_i_n_e _______ _
534-52~1--------4,6-Dinitro-2-methylphenol
86-30-~~~-------N-Nitrosodiphenylamine (1)-
101-55J3J-------4-Bromophenyl-phenylether -
118-74Jl~-------Hexa~hlorobenzene --
' I 87-86-5-,-------Pentachlorophenol _____ _
85-01-8---------Phenanthrene _______ _
120-12J7~-------Anthracene
86-74-8-~-------Carbazole ---------
84-74-2---------Di-n-butylphthalate ____ _
206-44-0--------Fluoranthene ---------129-00-0--------Pyrene 85-68-7-~-------Butylb_e_n_z-1-r-p-h~t-h_a_l~a-t_e ____ _
91-94-1---------3,3'-Dich orobenzidine __ _
56-55-3---------Benzo(a)anthracene -----218-01-9--------Chrysene 117-81-7--------bis(2-Et~h-y-l~h-e_x_y_l_)_p_h_t_h_a_l~a-t_e __
117-84-0--------Di-n-octylphthalate ____ -_-_
205-99-2--------Benzo(b)fluoranthene ----207-08-9--------Benzo(k)fluoranthene ___ _
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-c-a~)p-y~re-n-e~---
53-70-3---------Dibenz(a,h)anthracene ----191-24-2--------Benzo(g,h,i)perylene ___ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
50 U
50 U
20 ,u
20 U
20 U
20 U
20 U
50 U
50 U
20 U
20 U
20 U
50 U
20 U
20 U
20 U
20 U
20 U
20 U
20 U
20 U
20 U
20 U
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20 U
20 U
20 U
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20 U
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Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.:
NS-31DL
SDG No.: 4649
Lab Sample ID: 4660.GDL
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11924
Level: (low/med)
I· % Moisture: decanted: (Y/N)
toncentrated Extract Volume: l000(uL)
I-Injection Volume:
' 2. 0 (uL)
Date Received: 04/08/97
.Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 4.0
I
I
I··
I
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GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108°95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95~3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95~95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chlorona1hthalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
38 DJ
390 DE
40 u
'40 u
40 u
40 u
40 u
40 u
20 DJ
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
100 u
40 u
100 u
40 u
40 u
40 u
100 u
40 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-31DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4660.6DL
Sample wt/vol: Lab File ID: 11924
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: lOOO(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/30/97
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5-~-------2,4-Dinitrophenol
100-02-7~-------4-Nitrophenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I I "b f 132-64-9~-------Di enzo uran
121-14~2J-------2,4-Dinitrotoluene
84-66-~0 ~-------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
' 1 1 -.86-73-7-1 -------F uorene
100-0116,-------4-Nitroaniline
534-52~1--------4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine (1)
101-55-3·0 - - - - - --4 -Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8-c-------Carbazole
84-74-2-~-------Di-n-butylphthalate
206-44r0"-------Fluoranthene
129-00,0c-------Pyrene
85-68-?-~-------Butylbenzylphthalate
91-94-l~L-------3,3'-Dichlorobenzidine
56-55-3-~-------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------b~s(2-Ethllhexyl)phthalate_
117-84-0--------Di-n-octy phthalate ·
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
100 u
100 u
40 u
40 u
40 u
40 u
40 u
100 u
100 u
40 u
40 u
40 u
100 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
4 DJB
40 u
40 u
40 u
40 u
40 u
40 u
40 u
,
OLM03.0
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I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-32
I Lab Code: PACE
Matrix: (soil/water) I Sample wt/vol:
Case No.:
WATER
1000 (g/mL) ML
LOW
SAS No.: SDG No.: 4649
Lab Sample ID: 4661.4
Lab File ID: 11505
Level: (low/med)
11 % Moisture: ___ decanted: (Y/N)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
Concentrated Extract Volume: lOOO(uL) I Injection Volume: 2.0(uL)
I
I
I
I
I
I
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GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72sl---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chlorona1hthalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
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10 u
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25 u
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OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-32
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4661.4
Sample wt/vol: Lab File ID: 11505
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
( J
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-~---------2,4-Dinitrophenol
100-02~7~-------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101·-55-3 - - - - - - --4 -Bromophenyl-phenylether -
118-74"1--------Hexachlorobenzene --
87-86-5-;-------Pentachlorophenol
85-01-8---------Phenanthrene
120-12l7l-------Anthracene ' ' 86-74-8-0 -------Carbazole . ' 84-74-2-0 -------Di-n-but&lphthalate
205-44LoL-------Fluorant ene
129-ooLoL-------Pyrene ' ' 85-68-7-c-------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di hen p y lamine
FORM I SV-2
Q
25 u
25 u
10 u
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25 u
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10 u
10 u
10 u
25 u
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OLM03.0
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Appendix C
Semivolatile Organics Analysis Data Sheets
Trench Area Wells
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Sample wt/vol: 940.0 (g/mL)
Level: (low/med) LOW
ML
Contract:
SAS No.:
EX-05
SDG No.: 4635
Lab Sample ID: 4635.B
· Lab File ID: 11103
I %-Moisture: decanted: (Y /N)
S000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0 I
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Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
.
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-B---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72cl---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene ' 106-47-8--------4-Chloroaniline
8?-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocrclopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylhhthalate
208-96-8--------Acena~ht ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
4500 E
110 u
110 u
110 u
110 u
110 u
1300
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
11.0 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
260 u
110 u
260 u
110 u
110 u
110 u
260 u
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OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-05 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4635.8
Sample wt/vol: Lab File ID: 11103
Level: (low/med)
% Moisture:
940.0 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 5000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date E~tracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7.0
( J
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-r---------Fluorene -
100-0lL6--------4-Nitroan1l1ne
534-52L1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-I . -101-55-3----~---4-Bromophenyl-phenylether
118-74~1--------Hexachlorobenzene --
87-86-~---------Pentachlorophenol
85-01~8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68"7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethllhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di hen p y lamine
FORM I SV-2
Q
260 u
260 u
110 u
110 u
110 u
110 u
110 u
260 u
260 u
110 u
110 u
110 u
260 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
110 u
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110 u
110 u
110 u
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I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-05DL
Contract: I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4635.8DL
I Sample wt/vol:
Level: (low/med)
940.0 (g/mL) ML
LOW
Lab File ID: 13907
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 20.0
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% Moisture: decanted: (Y /N)
Concentrated Extract Volume: 5000 (uL").
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol .
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxibis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophen6I
105-67-9--------2,4-Dfmethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachloroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83 -3 2-9-- - - - - - --Acenaphth_ene
FORM I SV-1
Q
1200 D
210 u
210 u
210 u
210 u
210 u
820 D
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
210 u
530 u
210 u
530 u
210 u
210 u
210 u
530 u
210 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-05DL
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4635
Lab Sample ID: 4635.8DL
Sample wt/vol: Lab File ID: 13907
Level: (low/med)
% Moisture:
940.0 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 5000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 20.0
GPC Cleanup: (Y/N) N
CAS NO.
pH: 7.0
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol _____ _
100-02~7--------4-Nitrophenol _______ _
132-64!9~-------Dibenzofuran 121-14i2~-------2,4-Dinitrot_o_l_u_e_n_e _____ _
84-66-2°--------Diethylphthalate _____ _
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene 100-01~6--------4-Nitroa_n_i_l_i_n_e _______ _
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)-
101-55-30-------4-Bromophenyl~phenylether -
118-74-1--------Hexachlorobenzene. ____ ~~~
87-86-5---------Pentachlorophenol. _____ _
85-01-8---------Phenanthrene ________ _
120-12'-7-- - - - - --Anthracene
86 -74-:8-- - - - - - --Carbazole ·----------
84-74-12-- - - - - - --Di-n-butylphthalate. ____ _
206-4~~0--------Fluoranthene ________ _
129-oo~o--------Pyrene 85-68J7~--------Butylb_e_n_z_y_l_p_h_t_h_a_l_a_t_e ____ _
91-94Jl---------3,3'-Dichlorobenzidine 56-55~3---------Benzo(a)anthracene · __ _
218-01-9--------Chrysene 117-81-7--------bis(2-Et-~h_y_l_h_e_x_y_l~)~p-h~t-h_a_l_a_t_e_
117-84-0--------Di-n-octylphthalate ____ -_-
205-99-2--------Benzo(b)fluoranthene ----207-08-9--------Benzo(k)fluoranthene ___ _
50-32-8---------Benzo(a)pyrene ___ ~-----
193-39-5--------Indeno(l,2,3-cd)pyrene __ _
53-70-3---------Dibenz(a,h)anthracene ----191-24-2--------Benzo(g,h,i)perylene ___ _
) -Cannot be separated from Diphenylamine
FORM I SV-2
530 U
530 U
210 U
210 U
210 U
210 U
210 U
530 U
530 U
210 U
210 U
210 U
530 U
210 U
210 U
210 U
210 U
210 U
210 U
210 U
210 U
210 U
210 U
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210 U
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Q
OLM03.0
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I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-06
Contract: I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No . : SDG No. : 4 6 3 5
Lab Sample ID: 4636.6 I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11111
Level: (low/med)
I % Moisture: decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL) I Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 1.0
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GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxibis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72cl------c--Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol.
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylhhthalate
208-96-8--------Acena~ht ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
160 E
10 u
10 u
10 u
10 u
10 u
10 u
10 u
19
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
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25 u
10 u
10 u
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25 u
10 u
OLM03.0
lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4635
Lab Sample ID: 4636.6
Sample wt/vol: Lab File ID: 11111
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y /N)
l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2-----c--2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-,6--

-

-

-

-

-

-
-N-Nitrosodiphenhlamine ( 1) = 101"55-3--------4-Bromophenyl-p enylether 118-74ll--------Hexachlorobenzene --' 87-86-5---------Pentachlorophenol
85-01-~---------Phenanthrene
120-121-·7--------Anthracene · 86-74"81--------Carbazole
84-74]2"--------Di-n-buthlphthalate
206-44.-0--------Fluorant ene 129-0d-o--------Pyrene
85-68~7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate 117-84-0--------Di-n-octy phthalate -205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di hen p y lamine
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
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10 u
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.:
EX-06DL
SDG No.: 4635
Lab Sample ID: 4636.6DL
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11110
Level: (low/med)
I % Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL) I Injection Volume: 2.0(uL)
Date Received: 04/08/97 -
.Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 5.0
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GPC Cleanup: (Y/N) N pH: 7.0
CAS NO . COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
111-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
9S-48-7---------2-Methylphenol
108-60-1--------2,2'-oxrbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocrclopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
160 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
15 DJ
50 u
50 u
50 u
50 u so u
50 u so u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
50 u
120 u
50 u
50 u
50 u
120 u
50 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-06DL Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4636.6DL
Sample wt/vol: Lab File ID: 11110
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 100.0 (uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51~28-5---------2,4-Dinitrophenol _____ _
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran --------
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate -----
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene_~-----------100-01c6--------4-Nitroaniline
534-52L1--------4,6-Dinitro-2--m-e-t~h-y~l-p~h-e_n_o~l-
86-30-~-i--------N-Nitrosodiphenylamine (l)=
101-55r~--------4-Bromophenyl-phenylether __
118-74rl--------Hexachlorobenzene ------87-86-5"--------Pentachlorophenol _____ _
85-01-8~--------Phenanthrene 120-121-7--------Anthracene ---------
86-74-81-- - - - - --carbazole 84-74-2---------Di-n-buty~r-p~h~t~h~a~l~a~t~e~----
206-44-0--------Fluoranthene
129-00-0--------Pyrene --------
85-68-7-"-------Butylbenzylpnthalate 91-94-1---------3,3'-Dichlorobenzidi_n_e __ _
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene -----
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate ___ ~~-
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene ___ _
50-32-8---------Benzo(a)pyrene 193-39-5--------Indeno(l,2,3-c~a~)-p_y_r_e_n_e __ _
53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ----
) -Cannot be separated from Diphenylamine
120 U
120 U
50 U
50 U
50 U
50 U
50 U
120 U
120 U
50 U
50 U
50 U
120 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
50 U
·so JJ
50 U
50 U
50 U
50 U
50 U
Q
I
I
I
I
I
I
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I
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I
FORM I SV-2 OLM03 .01
I
I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-07
Contract: I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4637.4
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11109
Level: (low/med)
I % Moisture: decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL) I Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0
I
I
I
I
I
I
I
I.
I
I
I
I
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-7201---------Hexachloroethane -·
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9-------~2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane .
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methrlnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7--------0 2-Chlorona1hthalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2000 E
100 u
100 u
100 u
100 u
100 u
100 u
100 u
67 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
100 u
250 U.
100 u
100 u
100 u
250 u
100 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES EX-07
Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4635
Lab Sample ID: 4637.4
Sample wt/vol: Lab File ID: 11109
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:· (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
132-64-9--------Dibenzofuran
121-14!2~-------2,4-Dinitrotoluene ·
84 -66-2-·-- - - - - --Diethylphthalate
7005-7~-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01~6--------4-Nitroaniline
534-52cl--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12.-7------ --Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butblphthalate
206-44~0--------Fluorant ene
129-ooLb--------Pyrene
85-68-17-- - - - - - --Butylbenzylphthalate
91-94-!l-- - - - ----3, 3' -Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
ll7-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
250 u
250 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
OLM03.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I EX-07DL Lab Name: PACE ANALYTICAL SERVICES Contract:
I Lab Code: PACE Case No.": SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4637.4DL I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11108
Level: (low/med) I % Moisture: decanted: (Y/N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 50.0 I
I
I
I
I
I'
I
I
I
I
I
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol 541-73-1--------1,3-Dich orobenzene 106-46-7--------1,4-Dichlorobenzene
95-50-1-------~-l,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1------~--Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachloroc1clopentadiene 88-06-2---------2,4,6-Trich orophenol --95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chlorona1hthalene 88-74-4---------2-Nitroani ine 131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2500 D
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
· 500 u
500 u
500 u
1200 u
500 u
1200 u
500 u
500 u
500 u
1200 u
500 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-07DL Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE c.ase No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4637.4DL
Sample wt/vol: Lab File ID: 11108
·Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: · (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 50.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5~--------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-~--------2,4-Dinitrotoluene
84-66-2'---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52~1--------4,6-D{nitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55.!3--------4-Bromophenyl-phenylether -
118-74.Jl--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-1217--------Anthracene ' " 86-74-8°--------Carbazole
84-74-2°--------Di-n-buthlphthalate
206-4410~-------Fluorant ene
129-oo+o---~----Pyrene
85-68-?'1--------Butylbenzylphthalate
91-94-1---------3,3'-Dithlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24.-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
Q
1200 u
1200 u
500 u
500 u
500 u
500 u
500 u
1200 u
1200 u
500 u
500 u
500 u
1200 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
I
I
I
n
D
D
I
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I
FORM I SV-2 OLM03. 0 I
I
I
I 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: PACE ANALYTICAL SERVICES EX-08 Contract:
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4641.6 I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11104
Level: (low/med) I% Moisture: decanted: (Y /N)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0
Concentrated Extract Volume: 5000 (uL) I Injection Volume: 2.0(uL)
I
I
I
I
I
I
I
I
I
I
I
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol .
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1------~--Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitropheno~
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methllphenol
91-57-6---------2-Methllnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chloronaphtha ene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylhhthalate
208-96-8--------Acena~ht ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
7700 E
390
100 u
100 u
100 u
100 u
300
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
100 u
250 u
100 u
100 u
100 u
250 u
100 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-08 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4641.6
Sample wt/vol: Lab File ID: 11104
Levef: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:· (Y /N)
Concentrated Extract Volume: 5000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01L6--------4-Nitroan1l1ne
534-52L1--------4,6-Dinitro-2-methylphenol .
86-30-GC--------N-Nitrosodiphenhlamine (1)-
101-5_5'~3--- - - - - --4-Bromophenyl-p enylether-=
118-74-1--------Hexachlorobenzene ,, ' 87-86-5---------Pentachlorophenol
85-01-:8 ~ - - - - - - --Phenanthrene
120-12:-7-- - - - - --Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzilphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117~81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom D1phenylam1ne
Q
250 u
250 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
I
I
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D
I
m
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I
I
FORM I SV-2 OLM03. 01
I
I
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-08DL
Contract:
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4635
Lab Sample ID: 4641.6DL
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 13909
Level: (low/med) I %-Moisture: decanted: (Y/N)
5000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 40.0 I
I
I
I
I
·I
I
I
I
I
I
I
I
I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro~henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxlbis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64 -7-- - - - - --N-Nitroso-di-n-pr_opylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophen6I
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8~-------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methllnaphthalene
77-47-4---------Hexach orocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-D1.nitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
4800 D
400 u
400 u
400 u
400 u
400 u
230 DJ
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
1000 u
400 u
1000 u
400 u
400 u
400 u
1000 u
400 u
OLM03.0
'
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES Contract: EX-08DL
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4635
Lab Sample ID: 4641.6DL
Sample wt/vol: Lab File ID: 13909
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
5000 (uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 40.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02,7--~-----4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-~~--------Diethylphthalate
7005-72°3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene h 6 . 100-01---------4-N1troan1l1ne
534 -52'~ 1-- - - - - --4, 6 -Dini tro-2 -methylphenol
86-30~f~-.-------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl~phenylether -I 1 --118-74,1--------Hexach orobenzene
8 7 - 8 6 -5-.-- - - - - - -Pentachlorophenol
85-01-8---------Phenanthrene
12 0-12'1-7-- - - - - --Anthracene
86-74•8~--------Carbazole
84 -74 ~,2:---------Di-n-buthlphthalate
206-44L0--------Fluorant ene I 129-00~o--------Pyrene
85-6 8 -:17,-- - - - - - --Butylb~nz11phthal<;1 t~
91-9411---------3,3'-Dich orobenz1d1ne
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------b~s(2-Eth11hexyl)phthalate_
117-84-0--------Di-n-octy phthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom D1phenylam1ne
Q
1000 u
1000 u
400 u
400 u
400 u
400 u
400 u
1000 u
1000 u
400 u
400 u
400 u
1000 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
400 u
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FORM I SV-2 OLM03.0I
I
I
I 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name:,PACE ANALYTICAL SERVICES Contract:
EX-09
I Lab Code: PACE Case No.: SAS No.: SDG No.: 4635
Matrix: (soil/water) WATER Lab Sample ID: 4642.4 I Sample wt/vol: Lab File ID: 11105
Level: (low/med)
10 0 0 ( g /mL) ML
LOW I %-Moisture: ___ decanted: (Y /N)
Concentrated Extract Volume: 5000(uL) I Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7. 0
I
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I
! I'
I
1.
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4------~-bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1-----~---l,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1------~--Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol . -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocrclopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chloronaphtha ene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylhhthalate
208-96-8--------Acena~ht ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
40 u
6500 E
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
100 u
40 u
100 u
40 u
40 u
40 u
100 u
40 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-09 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No. : 4 6 3 5
Lab Sample ID: 4642.4
Sample wt/vol: Lab File ID: 11105
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted·,
Concentrated Extract Volume:
(Y/N)
5000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7.0
)
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-0207--------4-Nitrophenol
132-64°9--------Dibenzofuran ,, ' ' ' 121-14-2--------2 4-Dinitrotoluene ,II J t 84-66~2---------Diethylphthalate
7005-~2~3-------4-Chlorophenyl-phenylether_
86-73-7c~-------Fluorene
100-01t6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenhlamine (l)=
101-55-3-----~--4-Bromophenyl-p enylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene I 129-00-0--------Pyrene
85-68~7---------Butylbenzrlphthalate
91-94~1---------3,3'-Dich orobenzidine
56-55-i---------Benzo(a)anthracene
218-01-9----~---Chrysene
117-81-7--------bis(2-Ethllhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di hen p y lamine
FORM I SV-2
Q
100 u
100 u
40 u
40 u
40 u
40 u
40 u
100 u
100 u
40 u
40 u
40 u
100 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
.40 u
40 u
40 u
40 u
40 u
40 u
OLM03.0
I
I
I
I
u
D
g
I
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I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-09DL
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.:
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4642.4DL
I Sample wt/vol:
(low/med)
1000 (g /mL) ML
LOW
Lab File ID: 13908
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 20.0
Level: I % Moisture: decanted: (Y/N)
5_000 (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2~Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-C~lorona1~thalene
88-74-4---------2-Nitroani ine
131-11-3--------Dimethylphthalate
208-96-8--~-----Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
200 u
3800 D
200 u
200 u
200 u
200 u
100 DJ
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
500 u
200 u
500 u
200 u
200 u
200 u
500 u
200 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
EX-09DL Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No.: 4635
Lab Sample ID: 4642.4DL
Sample wt/vol: Lab File ID: 13908
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
5000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 05/19/97
Dilution Factor: 20.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02°7--------4-Nitrophenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
132-64"9--------Dibenzofuran
121-14~2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6-------C4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene .
8 7 - 8 6 -.. 5 - - - - - - - - -Pentachlorophenol
85-01-8---------Phenanthrene
120-12'-7--------Anthracene
86-74-:8-- - - - - - --Carbazole
84-74~2---------Di-n-butKlphthalate
206-44-0--------Fluorant ene
129-06-o--------Pyrene
85-68;7---------Butylbenzylphthalate
91-94;1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------b~s(2-Ethilhexyl)phthalate_
117-84-0------·--Di-n-octy phthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
Q
500 u
500 u
200 u
200 u
200 u
200 u
200 u
500 u
500 u
200 u
200 u
200 u
500 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
I
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FORM I SV-2 OLM03. 01
I
I
I 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
EX-10
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.:
I Sample wt/vol:
Level: (low/med)
950.0 (g/mL) ML
LOW
SAS No.: SDG No.: 4635
Lab Sample ID: 4643.2
Lab File ID: 11107
I % Moisture: decanted: (Y/N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 200.0 I
I
I
I
I
I.
I
I
I
I
••
I
I
I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
.
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95~3------~--Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitropheno~
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachloroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2100 u
14000
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
5300 u
2100 u
5300 u
2100 u
2100 u
2100 u
5300 u
2100 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
EX-10 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No. : 4 6 3 5
Lab Sample ID: 4643.2
Sample wt/vol: Lab File ID: 11107
Level: (low/med)
% Moisture:
950.0 (g/mL) ML
LOW
decanted:. (Y/N)
Concentrated Extract Volume: lOOO(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 200.0
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO: COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64~9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-5211--------4,6-Dinitro-2-methylphenol
86-30-k~--------N-Nitrosodiphenilamine (1)-
101"55}3-----a--4-Bromophenyl-p enylether -
118-741-1--------Hexachlorobenzene --;I 87-86-15-- - - - - - --Pentachlorophenol
85-01~~~--------Phenanthrene
120-12"-7--------Anthracene
8 6 - 7 4 -110•~ - - - - - - --Carbazole
84-74~~---------Di-n-butilphthalate
206-44,-0-- - - - - --Fluorant ene
129-0~-o--------Pyrene
85-68-7---------Butylbenzrlphthalate
91-94-1---------3,3'-Dich orobenzidine
56-55~3---------Benzo(a)anthracene
218-01:-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70°3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
Q
5300 u
5300 u
2100 u
2100 u
2100 u
2100 u
2100 u
5300 u
5300 u
2100 u
2100 u
2100 u
5300 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
2100 u
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FORM I SV-2 OLM03. 0 I
I
I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
EX-l0DL
I Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
Contract:
SAS No.: SDG No.: 4635
Lab Sample ID: 4643.2DL I Sample wt/vol:
Level: (low/med)
950.0 (g/mL) ML
LOW
Lab File ID: 11106
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 400.0
I %-Moisture: decanted: (Y/N)
1000 (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND CONCENTRATION UNITS:
. (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95~3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methylnaphtha ene
77-47-4---------Hexachlorocyclopentadiene
BB-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chloronaphtha ene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
4200 u
17000 D
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
10000 u
4200 u
10000 u
4200 u
4200 u
4200 u
10000 u
4200 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES EX-l0DL Contract:
Lab Code: PACE Case No.:
Matrix: (soil/water) WATER
SAS No.: SDG No . : 4 6 3 5
Lab Sample ID: 4643.2DL
Sample wt/vol: Lab File ID: 11106
Level: (low/med)
% Moisture:
950.0 (g/mL) ML
LOW
decanted,·. (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/21/97
Dilution Factor: 400.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7----~---4-Nitrophenol
132-6409--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14c2--------2,4-Dinitrotoluene
84 -66-.2-- - - - - - --Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-p---------Fluorene
100-0~-6--------4-Nitroaniline
534-s2l1--------4,6-Dinitro-2-methylphenol
86-30~k---------N-Nitrosodiphenylamine (1)-ii . -101-55-3--------4-Bromophenyl-phenylether
118-7~~1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-~---------Phenanthrene
120-12'-7--------Anthracene
86-74-~---------Carbazole
84-74-2---------Di-n-butKlphthalate
206-44-0--------Fluorant ene
129-0d-0--------Pyrene
85-68J7~--------Butylbenzylphthalate
91-94~1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-0]-9--------Chrysene ·
117-8l-7--------bis(2-Ethylhexyl)phthalate .
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32°8-----~---Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70~3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
I
(1) -Cannot be separated trom D1phenylam1ne
FORM I SV-2
Q
10000 u
10000 u
4200 u
4200 u
4200 u
4200 u
4200 u
10000 u
10000 u
4200 u
4200 u
4200 u
10000 u
4200 u
4200 u
4200 u
420.0 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
4200 u
OLM03.0
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I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES
NS-09
Contract:
I Lab Code: PACE
Matrix: (soil/water) WATER
Case, No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4654.9
I Sample wt/vol: 1000 (g/mL) ML Lab File ID: 11506
Level: (low/med) LOW Date Received: 04/08/97
I'% Moisture: decanted: (Y/N) Date Extracted:04/10/97
I
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Concentrated Extract Volume: lOOO(uL) Date Analyzed: 04/25/97
Injection Volume: 2.0(uL) Dilution Factor: 2.0
GPC Cleanup: (Y /N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1-------~1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72cl------~--Hexachloroethane -
98-95-3---------Nitrobenzene
78-S9-1---------Isophorone
88-7S-S---------2-NitrophenoL
l0S-67-9--------2,4-Dimethylphenol
111-91-1--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
S9-S0-7---------4-Chloro-3-methllphenol
91-S7-6---------2-Meth1lnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
9S-9S-4---------2,4,S-Trichloro1henol
91-SB-7---------2-Chloronaphtha ene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethhlhhthalate
208-96-8--------Acena~ t ylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u so u
20 u so u
20 u
20 u
20 u so u
20 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. m
I
0
I
·1
NS-09
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4654.9
Sample wt/vol: Lab File ID: 11506
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: lOOO(uL)
Injection Volµme: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor:. 2.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
51-28-15-- - - - - - --2, 4 -Dinitrophenol
100-02-7--------4-Nitrophenol
132-6~-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66~2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1~~------4,6-Dinitro-2-methylphenol
86-30 76---------N-Nitrosodiphenylamine (l)=
101-55-3--------4-Bromophenyl-phenylether __ ·
118-74-1--------Hexachlorobenzene
87-86l5---------Pentachlorophenol
85-01l0---------Phenanthrene ·' 120-12-7--------Anthracene
86-74~8---------Carbazole I 84-74,;-2---------Di-n-buthlphthalate
206-44-0--------Fluorant ene ,. . 129-00-0--------Pyrene
85-681!..7_ - - - - - - --Butylbenzllphthalate I , · h b ·ct· 91-94~1---------3,3 -Die oro enzi ine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Eth11hexyl)phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(ll -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
50 u
50 u
20 u
20 u
20 u
20 u
20 u
50 u
50 u . 20 u
20 u
20 u
50 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
2 JB
20 u
20 u
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20 u
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I OLM03.0
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-10
Lab Name: PACE ANALYTICAL SERVICES Contract: I Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER Lab Sample ID: 4655.6
I Sample wt/vol: 1000 (g/mL) ML Lab File ID: 11912
Level: (low/med) LOW Date Received: 04/08/97 I %-Moisture: decanted: (Y/N) Date Extracted:04/10/97
Volume: 1000 (uL) Date Analyzed: 04/29/97 Concentrated Extract I Injection Volume: 2.0(uL) Dilution Factor: 10.0
I
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I.
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GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541-73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------2,2'-ox1bis(l-Chloropropane)
106-44-5--------4-Methy phenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72~1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83~2--------2,4-Dichloropheno -
1·20-82-1-- - - - - --1, 2, 4-Trichlorobenzene
91-20~3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach oroc1clopentadiene
88-06-2---------2,4,6-Trich orophenol --
95-95-4---------2,4,5-Trichloro1henol
91-58-7---------2-Chlorona1htha ene
88-74-4---------2-Nitroani ine .
131-11-3--------Dimethylphthalate
208-96-8--------Acena~hthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
100 u
250 u
100 u
100 u
100 u
250 u
100 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES NS-10 Contract:
Lab Code: PACE Case No.:
Matrix: (sbil/water) WATER
SAS No.: SDG No.: 4649
Lab Sample ID: 4655.6
Sample wt/vol: Lab File ID: 11912
I Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:" (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/29/97
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7.0
( J
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14~2--------2,4-Dinitrotoluene
84-66-2----;-----Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01~6--------4-Nitroaniline
534-52~1--------4,6-Dinitro-2-methylphenol
86-30~6---------N-Nitrosodiphenhlamine (1)-
I h -101-55-3--------4-Bromop enyl-p enylether ii 1 b --118-74-1--------Hexach oro enzene ,, h 87-86 ~;,5------ - --Pen tac lorophenol
85-01~8~--------Phenanthrene
120-12)-7--------Anthracene
86-74-8---------Carbazole
84-74 -!2-- - - - - ---Di-n-butylphthalate
206-4~-0--------Fluoranthene
129-0~-o--------Pyrene
85-68-7---------Butylbenzllphthalate
91-94J1---------3,3'-Dich orobenzidine
56-55-13------- --Benzo (a) anthracene
218-01-9--------Chrysene ·
11 7-81-7-.-- - ----bis (2-Ethllhexyl) phthalate
117-84-0--------Di-n-octy phthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32 7 8---------Benzo(a)pyrene .
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70~3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be se p arated from Di p hen y !amine
FORM I SV-2
Q
25.0 u
250 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
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100 u
100 u
100 u
100 u
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OLM03.0
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS .l\NALYSIS DATA SHEET
NS-11
Lab Name: PACE ANALYTICAL SERVICES Contract: o Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4656.4 D Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: 11503
Level: (low/med)
I %-Moisture: decanted: (Y/N)
Concentrated Extract Volume: l000(ul,)
• Injection Volume: 2. 0 (uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
I
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1·
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I.
I
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chloro1henol
541~73-1--------1,3-Dich orobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenoi
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethox1)methane
120-83-2--------2,4-Dichloropheno -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methilphenol
91-57-6---------2-Methilnaphtha ene
77-47-4---------Hexach orocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
_131-11-3 - - - - - - --Dimethhlphthalate
208-96-8--------Acenap thylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9--------~Acenaphthene
FORM I SV-1
Q
2 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
NS-11 Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: SDG No.: 4649
Matrix: (soil/water) WATER
'
Lab Sample ID: 4656.4
Sample wt/vol: Lab File ID: 11503
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N) __
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N
CAS NO.
pH: 7.0
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol ------
132-64~9--------Dibenzofuran 121-14-2--------2,4-Dinitrot~o-r_u_e_n_e _____ _
84-66-?----------Diethylphthalate~-----
7005-7?--3-------4-Chlorophenyl-phenylether_
86-73~p-'--------Fluorene 100-0]-6--------4-Nitroa~n-i_l_i_n_e _______ _
534 -52/-1--'-- - - --4, 6-Dinitro-2-methylphenol
86-3016---------N-Nitrosodiphenylamine (l)-
101-5:i-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
8 7 -86 ~ 5 - - - - - - - - -Pentachlorophenol·------
8 5-0l ,18 - - - - - - - --Phenanthrene ________ _
120-12-7--------Anthracene 86-74 ~;8-- - - - - - --Carbazole ·---------~
84-74 ~:2 - -~ - - - - --Di-n-butylphthalate ____ _
206-4'1-0--------Fluoranthene ________ _
129-00-0--------Pyrene 85-6817--~------Butylb_e_n_z_y_l_p_h_t_h_a_l~a-t_e ___ _
91-9411---------3,3'-Dichlorobenzidine __ _
56-55~3---------Benzo(a)anthracene ____ _
218-01-9--------Chrysene 117-8i-7--------bis(2-Et-~h-1-1-h_e_xy_l~)-p_h_t_h_a_l_a_t_e-:_-=:
117-84-0--------Di-n-octy phthalate ____ _
205-99-2--------Benzo(b)fluoranthene ___ _
207-08-9--------Benzo(k)fluoranthene ----5 0 - 3 2" 8 - - - - - - - -
0 Benzo (a) pyrene __ 193-39-5--------Indeno(l,2,3-c-a~J-p_y_r_e~n_e ___ _
53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ___ _
(1) -Cannot be separated from D1phenylam1ne
FORM I SV-2
25 U
25 U
10 U
10 U
10 U
10 U
10 U
25 U
25 U
10 U
10 U
10 U
25 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
10 U
4 JB
10 U
10 U
10 U
10 U
10 U
10 U
10 U
Q
OLM03.0
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I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
NS-15
I Lab Code: PACE
Matrix: (soil/water) WATER
Case No.: SAS No.: SDG No.: 4649
Lab Sample ID: 4657.2 I Sample wt/vol: 1000
LOW
(g/mL) ML Lab File ID: 11504
I
I
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I
I
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I
I
I
••
I
I
I
Level: (low/med)
%-Moisture: decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
(Y /N)
l000(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Iso~horone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene --88c06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--0 -----Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
9 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: PACE ANALYTICAL SERVICES NS-15 Contract:
Lab Code: PACE Case No.:
Matrix: (soil{water) WATER
SAS No.: . SDG No.: 464.9
Lab Sample ID: 4657.2
Sample wt/vol: Lab.File ID: 11504
Level: (low/med)
%-Moisture: . / ~--
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 04/08/97
Date Extracted:04/10/97
Date Analyzed: 04/25/97
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO;. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64 -9--c-----Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14 -2--------2,4-Dinitrotoluene
84-66i2"--------Diethylphthalate .
7005-i2"3-------4-Chlorophenyl-phenylether
86-73~7---------Fluorene -
100-0~-6--------4-Nitroaniline
534-5~-1--------4,6-Dinitro-2-methylphenol
86-30~6---------N-Nitrosodiphenilamine (1)-
101-55-3--------4-Bromophenyl-p enylether-=
118-74-1--------Hexachlorobenzene
87-86 15---------Pentachlorophenol
85-01,8---------Phenanthrene
120-12-7--------Anthracene
86-7418---------Carbazole 1 . 84-74~2c--------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68~7"--------Butylbenzrlphthalate
91-94il---------3,3'-Dich orobenzidine
56-55,3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethrlhexyl)phthalate_
117-84-0--------Di-n-octy phthalate ·
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32~8---------Benzo(a)pyrene ·
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70c3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom D1phenylam1ne
FORM I SV-2
Q
' 25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
6 JB
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
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Appendix D
Inorganics Analysis Data Sheets
Plume Periphery Wells
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ENVIROFORMS/INORGANIC CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
Lab Name:.PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE
SOW No.: 3/90
Case No.: SAS No.: N/A SDG No. : . XX4649
Sample No.
XEX-01
XEX-0lD
XEX-0lS
XEX-02
XEX-03
XEX-04
XNS-09
XNS-10
XNS-11
XNS-15
XNS-29
XNS-30
XNS-31
XNS-32
Were ICP interelement corrections applied?
Were ICP background corrections applied?
If yes, were raw data generated before
application of background corrections?
Comments:
Lab Sample ID.
46499
46499D
46499S
46515
46523
46531
46549
46556
46564
46572
46580
46598
46606
46614
Yes/No
Yes/No
Yes/No
YES
YES
NO
I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted
on floppy diskette has been authorized by the Laboratory Manager or the
Manager's des~ as verified by the following signature.
Signature: ~ f~-Name: Tok~ "?ot>,or<.si<i
Date: "t;-10·"1'?-Title: ~k.,, =~,w-=-
COVER PAGE -IN 800001
I
ENVIROFORMS/INORGANIC CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
Lab Name: ,PACE ANALYTICAL SERVICES Contract: I
Lab Code: PACE
SOW No.: 3/90
Case No.: SAS No:: N/A SDG No.: XX4635 n
i 11.
Sample No.
XEX-05
XEX-0SD
XEX-0SS
XEX-06
XEX-07
XEX-08
XEX-09
XEX-10
Were ICP interelement corrections applied?
:I
Were ICP background corrections applied?
If yes, ,,were raw data generated before
application of background corrections?
Comments:
Lab Sample
1046358
1046358D
1046358S
1046366
1046374
1046416
1046424
1046432
ID.
Yes/No YES
Yes/No YES
Yes/No NO
I certify t.hat · this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted
on floppy di.skette has been authorized by the Laboratory Manager or the
:::::::~: 'd'.esSnH' er;;~ i fied by che ::::owins;;:na ;::•,, •~ '
Date: · , '7 -,=i Title: 4-<-u,c,,_,,y 0«'uA-r,~r
COVER PAGE -IN
E'C-0001
D
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ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract: ..
Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-01
SDG No.: XX4649 I Matrix (soil/water): WATER
I Level (low/med): LOW
Lab Sample ID: 46499
Date Received: 04/08/97
% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
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I
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I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After:
romments:
COLORLESS
Analyte Concentration C
-Aluminum 51. 3 B
Antimony 55.0 u
Arsenic 7.0 u
Barium 163 B
Beryllium 2.0 u
Cadmium 3.0 u -Calcium -98600 -Chromium 5.0 u
Cobalt 10.0 u
COJ2J2er 4.0 u
Iron 53.8 B
Lead 2.0 u -Magnesium 10900 -Manganese 461 -Mercury -Nickel 20.0 u
Potassium 2720 B
Selenium 5.0 u
Silver 6.0 u -Sodium 14800
Thallium 6.0 u -Vanadium 5.0 u
Zinc 5.0 u -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p -p
p
p
p
p
p
* p
p
N p
p
p
p
p
p
p
p
* p
Texture:
Artifacts:
' I
ENVIROFORMS/INORGANIC CLP
SAMPLE NO. I 1
INORGANIC ANALYSIS DATA SHEET
XEX-02 D Lab Name: PACE ANALYTICAL SERVICES Contract:
• Lab Code: PACE Case No.: SAS No.: N/A SDG No,: XX4649 a
Matrix ( soil/water) : WATER I Lab Sample ID: 46515
I
Level (low/med) : LOW Date Received: 04/08/97 I
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) : UG/L • !
CAS No. Analyte Concentration C Q M I --7429-90-5 Aluminum 33.6 B p
7440-36-0 Antimony 55.0 u p I 7440-38-2 Arsenic 7.0 u p -7440-39-3 Barium 982 p -7440-41-7 Be!:}'.llium ,, 2.0 u p I II 7440-43-9 Cadmium 3.0 u p ., Calcium -
:1
7440-70-2 274000 p
Chromium -7440-47-3 5.6 B p
,, 7440-48-4 Cobalt 10.6 B p I 7440-50-8 Copper 4.0 u p -7439-89-6 Iron 20200 p
I' Lead -7439-92-1 2.0 B * p I Magnesium -7439-95-4 76300 p -7439-96-5 Manganese 11600 N p - -7439-97-6 Mercury I --
' 7440-02-0 Nickel 20.0 u p
ii
7440-09-7 Potassium 3350 B p
Selenium -7782-49-2 9.8 p
Silver -I !j 7440-22-4 6.0 u p
Sodium -7440-23-5 85700 p
'! Thallium -7440-28-0 6. 0 u p -Vanadium I 7440-62-2 22.5 B p
7440-66-6 Zinc 10.9 B * p --Cyanide - -
' I
,, I
Color Before:' COLORLESS Clarity Before: CLEAR Texture:
Color After: 1 COLORLESS Clarity After: CLEAR Artifacts: I
Comments: 11 I ,,
FORM I -IN scoooJ I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
• Case No.: SAS No.: N/A
SAMPLE NO.
XEX-03
SDG No.: XX4649 I Lab Code: PACE
Matrix (soil/water): WATER
I Level (low/med): LOW
0.0
Lab Sample ID: 46523
Date Received: 04/08/97
% Solids:
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After: COLORLESS
(omments:
I
Analyte Concentration C
-Aluminum 78.5 B
Antimony 55.0 u
Arsenic 7.0 u -Barium 647
Beryllium 2.0 u
Cadmium 3.0 u -Calcium 209000 -Chromium 5.0 u
Cobalt 10.0 u
Copper 4.0 u -Iron 3370 -Lead 2.0 u -Magnesium 30100 -Manganese 3960 -Mercury -Nickel 20.0 u
Potassium 3970 B
Selenium 5.0 u
Silver 6.0 u -Sodium 48800 -Thallium 6.0 u
Vanadium 5.0 u
Zinc 5.0 u -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p -p
p
p
p
* p
p
N p -
p
p
p
p
p
p
p
* p --
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
' Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-04
SDG No.: XX4649
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 46531
Date Received: 04/08/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
,7440-70-2
, 7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
.I 7782-49-2
I
' 7440-22-4
'I 7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
Analyte Concentration C
-Aluminum 25.0 u
Antimony 55.0 u
Arsenic 7.0 u
Barium 45.1 B
Beryllium 2.0 u
Cadmium 3.0 u -Calcium 129000 -Chromium 5.0 u
Cobalt 10.0 u
Copper 4.0 u -Iron 2830 -Lead 2.0 u -Magnesium 36500 -Manganese 4530 -Mercury -Nickel 20.0 u
Potassium 3790 B
Selenium 5.0 u
Silver 6.0 u -Sodium 15300 -Thallium 6.0 u
Vanadium 5.0 u
Zinc 5.0 u -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p -p
p
p
p
p -p
p
p
p
* p -p
N p -
-p
p -p
p
p -p
p
* p -
-
Texture:
Artifacts:
I
I
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n
I
m
I
I
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I Lab Name:
Lab Code:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
PACE ANALYTICAL SERVICES Contract:
l>ACE Case No.: SAS No.: N/A
SAMPLE NO.
XNS-29
SDG No.: XX4649
I Matrix (soil/water,): WATER
I
I
Level (low/med): LOW
0.0
Lab Sample ID: 46580
Date Received: 04/08/97
% .Solids:
I
I
I
I
I
I
I
I
I
I Color
lolor
Before:
After:
Comments:
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum 43.5 B p
7440-36-0' Antimony 55.0 u p
7440-38-2 Arsenic 7.0 u p -7440-39-3 Barium 720 p
7440-41-7 Beryllium 2.0 u p
7440-43-9 Cadmium 3.0 u p -7440-70-2 Calcium 285000 p -7440-47-3 Chromium 5.0 u p
7440-48-4 Cobalt 10.0 u p
7440-50-8 Copper 4.0 u p -7439-89-6 Iron 707 p -7439--92-1 Lead 2.0 u * p -Magnesium 7439-95-4 35200 p -7439-96-5 Manganese 3710 N p - -7439-97-6 Mercury: - -7440-02-0 Nickel 20.0 u P.
7440-09-7 Potassium 2900 B p -7782-49-2 Selenium 7.2 p -7440-22-4 Silver 6.0 u p -7440-23-5 Sodium 50500 p --7440-28-0 Thallium 6.0 u p
7440-62-2 Vanadium ·5.0 u p
7440-66-6 Zinc 5.0 u * p
Cyanide --
--
COLORLESS Clarity Before: CLEAR Texture:
COLORLESS Clari_ty After: CLEAR Artifacts:
FORM I -IN
f,C0010
ENVIROFORMS/INORGANIC CLP
1
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
XNS-30
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: 'PACE Case No.: SAS No.: N/A SDG No.: XX4649
Matrix (soil/water): WATER
Level (low/med) :
% Solids:
LOW
0.0
Lab Sample ID: 46598
Date Received: 04/08/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
•I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
'I
I
7440-70-2
7440-47-3
!
I
7440-48-4
7440-50-8
7439-89-6
7439-92-1
l ,q
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
I
Color After: lcoLORLESS
Comments:
' : 'I
Analyte Concentration C
-Aluminum 25.0 u
Antimony 55.0 u
Arsenic 7.0 u
Barium 28.0 B
Beryllium 2.0 u
Cadmium 3.0 u -Calcium 75600 -Chromium 5.0 u
Cobalt 10.0 u
Copper 4.0 u -Iron 746 -Lead 2.0 u -Magnesium 18900 -Manganese 1510 -MerCU!}'. -Nickel 20.0 u
Potassium 2000 B -Selenium 5.0 u
Silver 6.0 u -Sodium 12300 -Thallium 6.0 u -Vanadium 5.0 u
Zinc 5.0 u -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p -p
p
p -p
p
* p
p
N p -
-p
p
p -p
p
p
p -* p --
Texture:
Artifacts:
800011
I
I
I
n
I
u
I
I
I
I
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I
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I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
• Lab Code: PACE Case· No.: SAS No.: N/A
SAMPLE NO.
XNS-31
SDG No.: XX4649
I Matrix (soil/water): WATER
I Level (low/med) :
% Solids:
LOW
0.0
Lab Sample ID: 46606
Date Received: 04/08/97
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6'
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After: COLORLESS
iomments:
Analyte Concentration C
Aluminum 93.7 B -Antimony 55.0 u
Arsenic 7.0 u
Barium 6870 -
Be!:}'.llium 2.0 -u
Cadmium 3.0 u
Calcium 418000 -
Chromium 5.0 -u
Cobalt 10.0 u
Copper 4.0 u -Iron 161
Lead 2.0 -u -Magnesium 24400 -Manganese 993 -Mercury -Nickel 20.0 u
Potassium 5290 -
Selenium 5.0 -u
Silver 6.0 u
Sodium 59100 --Thallium 6.0 u
Vanadium 5.0 u
Zinc 5.0 u
Cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p
-p
* p
p
N p -
-p
p
p
p
p
p
p
* p --
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
XNS-32
Lab Code: 'PACE Case No.: SAS No.: N/A SDG No.: XX4649
Matrix (soil/~ater): WATER
' Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 46614
Date Received: 04/08/97
co'ncentration Units (ug/L or mg/kg dry weight): UG/L
,, CAS No.
', 7429-90-5
7440-36-0
7440-38-2
r'
7440-39-3.
7440-41-7
· 7440-43-9
'7440-70-2 ,r ' '. 7440-47-3 '' 7440-48-4
7440-50-.8
,I 7439-89-6
7439-92-1
' I 7439-95-4
7439-96-5
' 7439-97-6 'I 7440-02-0
I 7440-09-7
'i '7782-49-2
I 7440-22-4
I 7440-23-5
i '7440-28-0
I 7440-62-2
' 7440-66-6
I
Color Before: COLORLESS
Color After: ,COLORLESS
Comments:
Analyte Concentration C
Aluminum 25.0 u
Antimony 55.0 u
Arsenic 7.0 u
Barium 93.0 B
Beryllium . 2.0 u
Cadmium 3.0 u
Calcium -47400
Chromium 5.0 u
Cobalt 10.0 u
Copper 4.0 u -Iron 160
Lead 2.0 -u
Magnesium 8480 -
-Manganese 114 -Mercury -Nickel 20.0 u
Potassium 4270 B
Selenium -5.0 u
Silver 6.0 u -Sodium 8860
Thallium -6.0 u
Vanadium 5.0 u
Zinc 5.0 u
Cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p
p
* p
p
N p -
-p
p -p
p
p
p
p -* p -
-
Texture:
Artifact;.s:
I
I
u
D
I
I
I
I
I
I
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I
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I
I
I
I
I ENVIROFORMS/INORGANIC CLP
SAMPLE NO.
I 1
INORGANIC ANALYSIS DATA SHEET
XEX-01 I Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No. : X01273
I Matrix (soil/water)
Level (low/med) :
WATER
LOW
0.0
Lab Sample ID: 109478
Date Received: 05/22/97
I
I
I
I
I
I
I
I
I
I
I
%-Solids:
tolor Before:
Color After:
lomments:
I
I
Concentration Units (ug/L or mg/kg dry weight)
CAS No. Analyte Concentration C Q
-7429-90-5 Aluminum -7440-36-0 Antimony -7440-38-2 Arsenic -7440-39-3 Barium -Beryllium 7440-41-7 -7440-43-9 Cadmium -7440-70-2 Calcium -7440-47-3 Chromium -7440-48-4 Cobalt -7440-50-8 Copper -7439-89-6 Iron -7439-92-1 Lead -Magnesium 7439-95-4 -7439-96-5 Manganese -7439-97-6 Mercury 0.20 u -7440-02-0 Nickel -7440-09-7 Potassium -7782-49-2 Selenium -7440-22-4 Silver -7440-23-5 Sodium -7440-28-0 Thallium -7440-62-2 Vanadium -7440-66-6 Zinc -Cyanide -
Clarity Before:
Clarity After:
FORM I -IN
UG/L
M
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-AV -
-
-
--
-
-
--
-
Texture:
Artifacts:
8('0OOJ
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS.DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
SAMPLE NO.
XEX-02
I
I
Lab Code: PACE Case No.: SAS No.: N/A SDG No. : X01273 I
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 109460
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
Color Before:
Color After:
Comments:
I
I
' 'r
:: .
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
,7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
, 7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration C Q M
--Aluminum --Antimony --Arsenic --Barium --Beryllium --Cadmium --Calcium --Chromium --Cobalt --Copper --Iron --Lead --Magnesium --Manganese --Mercury 0.20 u AV --Nickel --Potassium --Selenium --Silver --Sodium --Thallium --Vanadium --Zinc --cyanide --
Clarity Before: Texture:
'
Clarity After: Artifacts:
FORM I -IN
I
D
D
m
I
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I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
'
Case No.: SAS No.: N/A
SAMPLE NO.
XEX-03
SDG No.: X01273
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lab Code: PACE
Matrix (soil/water)
Level (low/med):
WATER
LOW
0.0
Lab Sample ID: 109452
Date Received: 05/22/97
% Solids:
f:olor Before:
Color After:
lcomments:
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
7429-90-5 Aluminum~ --
--7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --7440-41-7 Beryllium --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead --7439-95-4 Magnesium --7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
8COOO:i
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I
SAMPLE NO.
XEX-04 I
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 m
Matrix (soil/water) WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109445
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
'I • 1\ 'I
,1 i ' I
·I i
':/
Color Before: ,
Color After:
Comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration C Q M
--Aluminum --Antimony --Arsenic --Barium --Beryllium --Cadmium --Calcium --Chromium --Cobalt --Copper --Iron --Lead --Magnesium --Manganese --Mercury 0.20 u AV --Nickel --Potassium --Selenium --Silver --Sodium --Thallium --Vanadium --Zinc --Cyanide --
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
seoooo I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XNS-29
SDG No.: X01273
I Matrix (soil/water) WATER
Level (low/med): LOW
Lab Sample ID: 109544
Date Received: 05/22/97
I % Solids:
I
I
I
I
I
I
I
I
I
Jolor Before:
Color After:
lomments:
I
I
0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper . --7439-89-6 Iron --7439-92-1 Lead --Magnesium 7439-95-4 --7439-96-5 Manganese -7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc . --Cyanide --
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN eelj018
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XNS-30
SDG No.: X01273
Matrix (soil/water): WATER
Level (low/med) LOW
Lab Sample ID: 109551
Date Received: 05/22/97
. .
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L
CAS No. Analyte Concentration C Q M
--
'I 7429-90-5 Aluminum --7440-36-0 Antimony
' --7440-38-2 Arsenic --
' 7440-39-3 Barium --
Beryllium ,I 7440-41-7 --' 7440-43-9 Cadmium
I --7440-70-2 Calcium --! I 7440-47-3 Chromium --
'l 7440-48-4 Cobalt --
I 7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead --,, 7439-95-4 Magnesium --:; 7439-96-5 Manganese --
' 7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --
7782-49-2 Selenium --
'I I
I
7440-22-4 Silver --, 7440-23-5 Sodium --
ii '
,1 7440-28-0 Thallium --
I 7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN
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I
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••
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I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Case No.: SAS No.: N/A
SAMPLE NO.
XNS-31
SDG No. : X01273
I
Lab Code: PACE
Matrix (soil/water)
Level (low/med):
WATER
LOW
0.0
Lab Sample ID: 109577
Date Received: 05/22/97
I % Solids:
I
I
I
I
I
I
I
I
I
I
.Color
Color
Before:
After:
lcomments:
I .
1•
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead --7439-95-4 Magnesium - -7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel - -7440-09-7 Potassium - -7782-49-2 Selenium --7440-22-4 Silver - -7440-23-5 Sodium - -7440-28-0 Thallium --7440-62-2 Vanadium - -7440-66-6 Zinc - -Cyanide - -
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
ENVIROFORMS/INORGANIC CLP
SAMPLE NO.
1
INORGANIC ANALYSIS DATA SHEET
XNS-32
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: N/A SDG No. : X01273
Matrix (soil/water): WATER
Level (low/me,cl.) : LOW
Lab Sample ID: 109569
Date Received: 05/22/97
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
:;
' i
I . ,r
I' I' ,! ' .,
' f 11,
I•
I;
Color Before: ·:
Color After:
Comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration C Q M
--Aluminum --Antimony --Arsenic --Barium --Beryllium --Cadmium --Calcium --Chromium --Cobalt --Copper --Iron --Lead --Magnesium --Manganese --Mercury 0.20 u AV --Nickel --Potassium --Selenium --Silver --Sodium --Thallium --Vanadium --Zinc --cyanide --
Clarity Before: Texture: '
Clarity After: Artifact,s:
FORM I -IN
I
I
n
D
D
I
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I
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I
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Appendix D
lnorganics Analysis Data Sheets
Trench Area Wells
I
I
ENVIROFORMS/INORGANIC CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
I Lab Name: PACE ANALYTICAL SERVICES Contract:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lab Code: PACE Case No.: SAS No.: N/A SDG No.: X01273
SOW No.: 3/90
Sample No.
XEX-01
XEX-02
XEX-03
XEX-04
XEX-05
XEX-06
XEX-07
XEX-08
XEX-09
XEX-10
XNS-09
XNS-10
XNS-l0D
XNS-l0S
XNS-11
XNS-14
XNS-14D
XNS-14S
XNS-15 ·
XNS-29
Were ICP interelement corrections applied?
Were ICP background corrections applied?
If yes, were raw data generated before
application of background corrections?
Comments:
Lab Sample ID.
109478
109460
109452
109445
109502
109510
109528
109536
109494
109486
109619
109601
109601D
109601S
109593
109403
109403D
109403S
109585
109544
Yes/No YES
Yes/No
Yes/No
YES
NO
I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted
on floppy diskette has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature.
Signature: li04l.J..·
Date: ~-'i'r --------------
Name:
Title: th=-cchN--r
COVER PAGE -IN
800001
ENVIROFORMS/INORGANIC CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE
SOW No. : 3/90
Case No.:
Sample No.
XNS-30
XNS-31
XNS-32
XNS-39
XNS-40
XNS-42
Were ICP interelement corrections applied?
Were ICP background corrections applied?
If yes, were raw data generated before
application of background corrections?
Comments:
Contract:
SAS No.: N/A SDG No.,: X01273
Lab Sample ID.
109551
109577
109569
109411
109437
109429
Yes/No YES
Yes/No YES
Yes/No NO
I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted
on floppy diskette has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature.
Signature: Name:
Date: Title:
COVER PAGE -IN
I
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I
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seoooz I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: 'PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-05
SDGNo.: XX4635
I Matrix (soil/water): WATER
1 Level (low/med) :
%-Solids:
LOW
0.0
Lab Sample ID: 1046358
Date Received: 04/08/97
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
lolor After: COLORLESS
Comments:
I
I
Analyte Concentration C
-· Aluminum 61.8 B
Antimony 55.0 u -Arsenic 10.6 -Barium 138 B
Beryllium 2.0 u -Cadmium 12.8 -Calcium 1420000 -Chromium 5.0 u -Cobalt 1220 -Copper 647 -Iron 287 -Lead 15.8 -Magnesium 616000 -Manganese 125000 -Mercury -Nickel 587 -Potassium 16000 -Selenium 77.3 -Silver 29.4 -Sodium 5880000 -Thallium 38.4 -Vanadium 5.0 u -Zinc 219 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E
E
E
M
-p -p
p
p
p
p
p -p -p
p -p
p
p
p -
-p
p
p
p
p
p
p
p -
-
Texture:
Artifacts:
onr no-, (,_-:.._. ~lJ A..
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I
SAMPLE NO.
XEX-05 m
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 I
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109502
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum - -7440-36-0 Antimony --.7440-38-2 Arsenic --7440-39-3 Barium - -Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper --7439-89-6 Iron - -7439-92-1 Lead - -7439-95-4 Magnesium --7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium - -7782-49-2 Selenium --7440-22-4 Silver - -7440-23-5 Sodium --7440-28-0 Thallium - -7440-62-2 Vanadium - -7440-66-6 Zinc - -Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN 800007
I
•
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
' Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-06
SDGNo.: XX4635
I Matrix (soil/water): WATER
I Level (low/med) : LOW
0.0
Lab Sample ID: 1046366
Date Received: 04/08/97
% Solids:
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After: COLORLESS
(omments:
I
Analyte Concentration C
-Aluminum 44.5 B
Antimony 55.0 u
Arsenic 7.0 u
Barium 87.6 B
Beryllium 2.0 u
Cadmium 3.0 u -Calcium 29300 -Chromium 5.0 u
Cobalt 10.0 u -Copper 250 -Iron 3350 -Lead 12.5 -Magnesium 15700 -Manganese 2850 -Mercury: -Nickel 20.0 u
Potassium 3060 B
Selenium 5.0 u
Silver 6.0 u -Sodium 3510000 -Thallium 6.0 u
Vanadium 6.9 B -Zinc 25.4 -Cyanide -
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p
p
P·
p
p -
p
p
p
p
p
p
p
p
Texture:
Artifacts:
SCGOOJ
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
SAMPLE NO.
XEX-06
I
I
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 m
Matrix (soil/water): WATER Lab Sample ID: 109510
Level (low/med): LOW Date Received: 05/22/97
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --Antimony 7440-36-0 --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead --Magnesium 7439-95-4 --7439-96-5 Manganese -7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN BP0008
I
n
g
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
• Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-07
SDG No.: XX4635
I Matrix (soil/water): WATER
I Level (low/med): LOW
Lab Sample ID: 1046374
Date Received: 04/08/97
% Solids: 0.0 I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4,
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After:
fomments:
I
COLORLESS
Analyte Concentration C
-Aluminum 64.7 B
Antimony 55.0 u
Arsenic 7.0 u -Barium 315 -Beryllium 2.0 u
Cadmium 4.2 B -Calcium 526000
Chromium 5.0 u -Cobalt 286 -Copper 37.8 -Iron 16800 -Lead 8.6 -Magnesium 255000 -Manganese 43600 -Mercury -Nickel 61. 3 -Potassium 5160 -Selenium 24.7 -Silver 6.0 u -Sodium 407000 -Thallium 13.5 -Vanadium 5.0 u -Zinc 113 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p -p
p
p
p
p
p
p
p
E p
p
p
p --p
p
p -p
E p
p -p
E p -
-
Texture:
Artifacts:
600OO-t
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract:
SAMPLE NO.
XEX-07
I
I
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.: SAS No.: N/A SDG No. : X01273 n
Matrix (soil/water) WATER Lab Sample ID: 109528
Level (low/med): LOW Date Received: 05/22/97
%-Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --Antimony 7440-36-0 - -7440-38-2 Arsenic --7440-39-3 Barium - -Beryllium 7440-41-7 --7440-43-9 Cadmium - -7440-70-2 Calcium --7440-47-3 Chromium - -7440-48-4 Cobalt - -7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead - -Magnesium 7439-95-4 --7439-96-5 Manganese -7439-97-6 Mercury 0.20 u AV - -7440-02-0 Nickel --7440-09-7 Potassium - -7782-49-2 Selenium - -7440-22-4 Silver --7440-23-5 Sodium - -7440-28-0 Thallium - -7440-62-2 Vanadium - -7440-66-6 Zinc --Cyanide - -
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN 8{'(1009
B
I
I
I
I
I
I
I
I
I
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I
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I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
' Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-08
SDG No. : XX4635
I
I
Matrix (soil/water): WATER
Level (low/med): LOW
Lab Sample ID: 1046416
Date Received: 04/08/97
% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: YELLOW
lcolor After: COLORLESS
IComments:
I
Analyte Concentration C
-Aluminum 55400 -Antimony 55.0 u
Arsenic 7.0 u
Barium 22.9 B -Beryllium 15.4 -Cadmium 3.0 u -Calcium 473000 -Chromium 12.6 -Cobalt 5350 -Copper 853 -Iron 22800 -Lead 11. 6 -Magnesium 363000 -Manganese 232000 -Mercury -Nickel 1140 -Potassium 15000 -Selenium 59.9 -Silver 47.4 -Sodium 4590000 -Thallium 45.8
Vanadium 5.0 u -Zinc 1510 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E
E
E
M
-p
p
p
p
p
p
p
p
p
p
p
p
p -p -
-p
p
p
p
p
p
p -p -
-
Texture:
Artifacts:
or,r oo-· LC -'J J
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
SAMPLE NO.
XEX-08
I
I
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 n
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109536
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --Antimony 7440-36-0 --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --
,I 7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 COEEer --7439-89-6 Iron --7439-92-1 Lead --7439-95-4 Magnesium --7439-96-5 Manganese -7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifact·s:
Comments:
FORM I -IN
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XEX-09
SDG No.: XX4635
I
I
I
I
I
I
I
I
I
I
I
Matrix (soil/water): WATER Lab Sample ID: 1046424
Level (low/med):
% Solids:
LOW
0.0
Date Received: 04/08/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: YELLOW
lolor After: COLORLESS
tomments:
I
Analyte Concentration C
-Aluminum 70100 -Antimony 55.0 u
Arsenic 7.0 u -Barium 11.8 B -Beryllium 17.1 -Cadmium 3.0 u -Calcium 266000 -Chromium 19.5 -Cobalt 3490 -Copper 730 -Iron 14900 -Lead 3.8 -Magnesium 85200 -Manganese 114000 -Mercury -Nickel 653 -Potassium 11400 -Selenium 19.7 -Silver 19.2 -Sodium 3670000 -Thallium 22.6 -Vanadium 5.0 u -Zinc 2060 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p
p -p
p -p
p
p
p
p
E p
p -p
p -
-p
p
p
p
E p
p
p
E p
-
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
XEX-09
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: PACE Case No.: SAS No.: N/A SDG No.: X01273
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109494
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum --7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --7440-41-7 Beryllium --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48°4 Cobalt --7440-50-8 co1212er --7439-89-6 Iron --7439-92-1 Lead --7439-95-4 Magnesium - -7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide - -
Color Before: Clarity· Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN
8{'0011
I
I
m
I
D
D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Lab
Lab
Name: PACE
Code: 'PACE
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
ANALYTICAL SERVICES Contract:
Case No.: SAS No.: N/A
SAMPLE NO.
XEX-10
SDGNo.: XX4635
I Matrix (soil/water) :
Level (low/med):
WATER
LOW
0.0
Lab Sample ID: 1046432
Date Received: 04/08/97
I % Solids:
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22·-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
'olor Before: COLORLESS
,_olor After:
Comments:
I
I
COLORLESS
Analyte Concentration C
-Aluminum 44800 -Antimon:i::: 55.0 u
Arsenic 7.0 u
Barium 18.0 B -Ber:i:::llium 12.1 -Cadmium 3.0 u -Calcium 319000 -Chromium 10.3 -Cobalt 2680 -Copper 572 -Iron 17500 -Lead 4.9 -Magnesium 153000 -Manganese 91900 -Mercur:i::: -Nickel 365 -Potassium 13000 -Selenium 25.8 -Silver 16.9 -Sodium 2490000 -Thallium 27.7 -Vanadium 5.0 u -Zinc 1360 -c:i:::anide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p -E p
p
p -p -
-p
p
p -p
E p
p -p
E p -
-
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
SAMPLE NO.
XEX-10
I
I
Lab Code: PACE Case No.: SAS No.: N/A SDG No.: X01273 E
Matrix (soil/water) WATER
Level (low/med) LOW
% Solids: 0.0
· Lab Sample ID: 109486
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Co:e:eer --7439-89-6 Iron --7439-92-1 Lead --Magnesium 7439-95-4 --7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN
se0O12
I
I
H
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
I SAMPLE NO.
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
XNS-09
• Lab Code: PACE SAS No.: N/A SDG No.: XX4649 Case No.: n Matrix (soil/water): WATER
I Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 46549
Date Received: 04/08/97
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I
Color Before: COLORLESS
J.olor After: COLORLESS
.Comments:
I
Analyte Concentration C
-Aluminum 5600 -Antimony 55.0 u -Arsenic 7.0 u -Barium 329 -Beryllium 2.0 u -Cadmium 3.0 u -Calcium 133000 -Chromium 21. 7 -Cobalt 18.7 B
Copper 19.4 B -Iron 20600 -Lead 2.6 B -Magnesium 55300 -Manganese 10300 -Mercury -Nickel 20.0 u
Potassium 2510 B -Selenium. 6.8 -Silver 6.0 u -Sodium 35500 -Thallium 6.0 u
Vanadium 6.4 B
Zinc 10.9 B -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p -p
p
p
p -p
p
p
p
p -P·
* p
p
N p
p
p
p
p
p
p
p
* p
Texture:
Artifacts:
8C-000h
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
I
SAMPLE NO.
XNS-09 I
Lab Code: PACE Case No.: SAS No.: N/A SDG No. : X01273 m
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109619
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum --7440-36-0 Antimony --7440-38-2 Arsenic --7440-39-3 Barium --Beryllium 7440-41-7 --7440-43-9 Cadmium --7440-70-2 Calcium --7440-47-3 Chromium --7440-48-4 Cobalt --7440-50-8 Copper --7439-89-6 Iron --7439-92-1 Lead --Magnesium 7439-95-4 --7439-96-5 Manganese --7439-97-6 Mercury 0.20 u AV --7440-02-0 Nickel --7440-09-7 Potassium --7782-49-2 Selenium --7440-22-4 Silver --7440-23-5 Sodium --7440-28-0 Thallium --7440-62-2 Vanadium --7440-66-6 Zinc --Cyanide --
Color Before: Clarity Before: Texture:
Color After: Clarity After: Artifacts:
Comments:
FORM I -IN
8P001J
I
D
u
g
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE ANALYTICAL SERVICES Contract:
• Lab Code: PACE Case No.: SAS No.: N/A
SAMPLE NO.
XNS-10
SDG No.: XX4649 I
I
I
I
I
I
I
I
I
Matrix (soil/water): WATER
Level (low/med) :
'i; Solids:
LOW
0.0
Lab Sample ID: 46556
Date Received: 04/08/97
Concentration Units (ug/L or mg/kg dry weight): UG/L
1.
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
l:olor After: COLORLESS
.Comments:
I
Analyte Concentration C
-Aluminum 494 -Antimony 55.0 u
Arsenic 7.0 u -Barium 205 -Be:!,Yllium 2.0 u
Cadmium 3.0 u -Calcium 52200 -Chromium 5.0 u
Cobalt 21. 7 B
Copper 4.0 u -Iron 1200 -Lead 2.0 u -Magnesium 31900 -Manganese 2150 -Mercury -Nickel 23.2 B
Potassium 2120 B
Selenium 5.0 u
Silver 6.0 u -Sodium 45800 -Thallium 6.0 u
Vanadium 5.0 u -Zinc 37.2 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p -p
p
p
p
p
p
p
* p
p
N p
p
p
p
p
p
p
p
* p
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
SAMPLE NO.
XNS-10
I
I
Lab Name: PACE ANALYTICAL SERVICES
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 I
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 109601
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
I,
, I
Color Before:
Color After:
. Comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
COEEer
Iron
Lead
Magnesium
Manganese
Mercury 0.20
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Clarity Before:
Clarity After:
FORM I -IN
C Q M
--
- -
- -
- -
--
--
----
--
--
--
--
--
--
-u AV --
--
--
--
--
- -
- -
- -
--
- -
Texture:
Artifacts:
D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
I SAMPLE NO.
1
INORGANIC ANALYSIS DATA SHEET a Lab Name: PACE ANALYTICAL SERVICES Contract:
XNS-11
• Lab Code: PACE Case No.: SAS No.: N/A SDG No.: XX4649
I Matrix (soil/water): WATER
I Level (low/med) :
% Solids:
LOW
0.0
Lab Sample ID: 46564
Date Received: 04/08/97
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
folor After: COLORLESS
Comments:
I
I
Analyte Concentration C
-Aluminum 641 -Antimony 55.0 u
Arsenic 7.0 u
Barium 199 B
Beryllium 2.0 u
Cadmium 3.0 u -Calcium 6850 -Chromium 8.2 B
Cobalt 31.6 B
Copper 15.2 B -Iron 20100 -Lead 2.2 B -Magnesium 5710 -Manganese 889 -Mercury -Nickel 21.9 B
Potassium 3370 B
Selenium 5.0 u
Silver 6.0 u -Sodium 75500 -Thallium 6.0 u
Vanadium 5.0 u -Zinc 22.4 -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p
p
* p
p -N p -
-p
p
p
p
p -p
p -* p -
-
Texture:
Artifacts:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES
SAMPLE NO.
XNS-11
I
I
Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 I
Matrix (soil/water) WATER Lab Sample ID: 109593
Level (low/med): LOW Date Received: 05/22/97
% Solids: 0.0
Concentration.Units (ug/L or mg/kg dry weight) UG/L
Color Before:
Color After:
Comments:
I,
11
11
lj
Ii i1
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Co1212er
Iron
Lead
Magnesium
Manganese
Mercury 0.20
Nickel
Potassium
Selenium
Silver
Sodium
Thallium
Vanadium
Zinc
Cyanide
Clarity Before:
Clarity After:
FORM I -IN
C Q M
--
--
--
--
--
--
--
--
----
--
--
--
--
u AV ----
--
--
--
--
--
--
--
--
Texture:
Artifacts:
fl
D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE ANALYTICAL SERVICES Contract:
Lab Code: 'PACE Case No.: SAS No.: N/A
SAMPLE NO.
XNS-15
SDG No.: XX4649
I
I
I
I Matrix (soil/water): WATER
I Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 46572
Date Received: 04/08/97
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
Jolor After: COLORLESS
Comments:
I
I
Analyte Concentration C
-Aluminum 46.7 B
Antimony 55.0 u
Arsenic 7.0 u -Barium 342 -Beryllium 2.0 u
Cadmium 3.0 u -Calcium 296000 -Chromium 5.0 u
Cobalt 29.6 B
Copper 4.0 u -Iron 7540 -Lead 2.0 u -Magnesium 154000 -Manganese 11800 -Mercury -Nickel 20.0 u
Potassium 4230 B
Selenium 5.0 u
Silver 6.0 u -Sodium 46300 -Thallium 6.0 u
Vanadium 5.0 u
Zinc 5.0 u -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p
p
p
p
p
p
p
p
p
p
p
* p
p
N p -
-p
p
p -p
p
p
p
* p --
Texture:
Artifacts:
800009
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
I
SAMPLE NO.
I XNS-15
Lab Name: PACE ANALYTICAL SERVICES
' Lab Code: PACE Case No.:
Contract:
SAS No.: N/A SDG No.: X01273 I
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 109585
Date Received: 05/22/97
Concentration Units (ug/L or mg/kg dry weight) UG/L
Color Before:
Color After:
Comments:
I
1,
I:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
I, 7440-41-7
I, 7440-43-9
"7440-70-2
II 7440-47-3 Ii
I[ 7440-48-4
1, 7440-50-8
'i 7439-89-6
. 7439-92-1
i 7439-95-4
7439-96-5
7439-97-6
' 7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Analyte Concentration C Q M
--Aluminum --Antimony --Arsenic --Barium --Beryllium --Cadmium --Calcium --Chromium --Cobalt --Copper --Iron --Lead --Magnesium --Manganese --Mercury 0.20 u AV --Nickel --Potassium --Selenium --Silver --Sodium --Thallium --Vanadium --Zinc --Cyanide --
Clarity Before: Texture:
Clarity After: Artifacts:
FORM I -IN
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Appendix E
Chain-of-Custody Records
Plume Periphery Wells and Trench Area Wells
P-ace Analytical
I I
Phone 70'1 -& 33 · I 731 Ex. ;ia 3
EX-01
2 E'I. ·OI
3 EX-DI
4 EX-D1 JriatY ix
5 EX-01 , matrix
6 Ex-DJ . m"tr;x
7
8
Additional Comments
N~ed two Ois!< '" /;PA rov'mQt C.11cl '(e.-.sv!fs
on Spreac/ Sh,,.A.s
h'ock;Aj No, ,7o3)5. Ibo -3 -- - ---
Report To k',:11 k/u 1t:z.
Bill To: 1/8.5 c~Ja.-Sori'tro ~ R,.1 r ?
. P .0. # I Billing Reference 9 7-/ 7~ 5;;;..
Project Name/ No.
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. 0 / Q 3,;? 5 ·
Pacram
it f5=2C/
"Requested Due Date:
-SEE REVERSE SIDE FOR INSTRUCTIONS ---------
: -P cft: rA'1l an,t i c ffl
Client <l/rrbona / Sfa rch ancl C.hero ,'c,, /
Address 1/85 CeJo,, 5/>tt'tJ) f Rood
70',' I I 1
Phone· Id 5 3 -/ 7 3 /
.Ex-01
2 £)1.-0J
3 !:.)(-o/
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7
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smro J./85 Ccchc S;2ti'11js
P.O.# I Billing Reterence 97-/ 'J,1. S).
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Proiect Name I No.
-_,oaau-
CHAIN-OF-CUSTODY RECORD
Analytlcal Request
Pace Client No. 0/Q 3.2 5
Pace Project Manager
Pace Project No.
•Requested Due Date:
Ill
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J . SEE REVERSE SIDE FOR INSTRUCTIONS
" . ....
P-ace Analytical .)10.J0.1.
CHAIN-OF-CUSTODY RECORD
Analytical Request
Client Nc,1,oy,/ c..~t;,r,!, c,a,I [/4,,,,-,,'cc,I Co.
Address 495 Ccc(,,e .Sp,-,'c,) S f<o~d
Report To: ke11 KLw 1Tz..
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P.O.# I Billing Reference 7 / -/ 2J 5 d
Pace Client No. (;, / () ? ;J. 5
Pace Project Manager
T'
PhoneQo•/) b 3 3 -I 7 ?/
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Pace Project No.
Project Name I No.
REMA KS
SEE REVERSE SIDE FOR INSTRUCTIONS ---:-- - - - - -
'Pa'ce~ ii aTytTc aT iiii
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Address :(J'$ C<>c/c.t: i<o, J
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Project Name I No.
PRESERVATIVES ANALYSES
REQUEST_
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-CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. & /0 ]:25
·Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
P-ace Analytical 5
Report To Keo K/i, ttz c1ien1Alat:ar,c} ,}farc/2 a,,J Cbeo,,-c4/ Co.
Address 1/55 CeclCiY'. 5Ptc'",#S R()acl Bill To /./8S D~dc r'. ,5/1'.1~5 £.;
P.O.# I Billing Reference q 7-/ 7 2 5 2
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Phone 701/· (:,33. /73/ £1-. dD3 Project Name/ No.
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Analytical Request
Pace Client No. &/0 3 :2 5
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
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Pace:'AiialyticaT
Address l/.'( 5
Phone( '/c:,•( J ? 3 3 -I 7 ])
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g! PRESERVATIVES ANALYSES ~ 1--,~--,---,----.-.----1REOUEST
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Pace Client No. (,/o 3;2S
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"Requested Due Date:
REMARKS
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3 SEE REVERSE SIDE FOR INSTRUCTIONS . '
P-ace Analytical
Client NS c.
Address C If I
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Phone
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A_dditional Comments
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Pro;ect Name I No.
PRESERVATIVES ANALYSES
f--',---,---,---,---,----,REOUEST
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CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. 0/ Q' 32 S
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS . . ,
__ llll■-_ 111!11! __ ;,---

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PRESERVATIVES ANALYSES f--,--,--,--,--,---, REQUEST
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Analytical Request
I \r--.-• ,.•·,,-Pace Client No. ~.c_ 1......._; ::_v-:::-:.:~
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Pace Project No.
"Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
•
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Client (\\ t
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Pace Client No. r~~ \(.:1 3-~ .. :
Pace Project Manager
Pace Project No.
~Requested Due Date:
REMARKS .,_,G.9Lf/. ;)_
-4,' c·· -~•:·· 'j 'f_ Io tf{,tff ~
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SEE REVERSE SIDE FOR INSTRUCTIONS - -----... -
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Appendix F
Out of Service Well Pumping Records
Periphery and Trench Area Wells
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a11v ec 1st for D -1 Ch kl"
....... M< , ,1 EX-01
,H ,_•~-1•j/'•·•
Tag'JJ j:5:f031A
Date :~, I 11'1 I '°17 ··;,., __ ... i ~ _cr-1
Time \~\:=-~
Set flow rate for pumo •,,_-).) •~ '\)\,,I
Actual flow rate for pump ,......__ r::~/' . 0 ', (. <? \ ,•.
Adjustment to flowrate made l,.J~-. ...,, . _.,
Flow meter reading 'VJ \ (,, ,_:, ' ~ ~ '.:-,.
Date ~III / C\, '._.,_,_ \ \-c.\7
Time 1.\..11 .... -~
Set flow rate for oumo ..L ,r""t·, -.. _,
Actual flow rate for pump A. ,l,\ \-\-i O' ~
Adiustment to flowrate made (~ G> \\•1cc.,.1
Flow meter readinA
Date -:i.. I ,.,! "\"") --=-...,_ \"d-°l'l
Time • .} \\ '::) <'> "'
Set flow rate for pump ,.., \ ~ ~"
Actual flow rate for oumo rl-\ C:r.-i/,A
Adjustment to flowrate made 1-.. '"'('\,:;
Flow meter reading ~ °" ·;::r;Yl, 1 oo
Date '3!1;1197
Time .-ti') 2¥,. ./i'f ,.,_
Set flow rate for oumo 2. ! {~:~: • ~\.
Actual flow rate for pump ? I f;i',,'-'··
Adjustment to flowrate made '. ( ·. t;··r-~--t...-~
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Date ?/ I"\ / 0., 7 6-1.1.--q-,
Time It, \Vo..
Set flow rate for oump ")\ "'~
Actual flow rate for pump r--.\~,,..fl,.. ....
' ' Adjustment to flowrate made l-'. ,., ;r,• . .-
Flow meter readina '.J_~':J,~ \~ C(.)
Date I I
Time
Set flow rate for pump
Actual flow rate for oumo
Adjustment to flowrate made
Flow meter readini:i
Date I I
Time
Set flow rate for pump
Actual flow rate for pumo
Adiustment to flowrate made
Flow meter reading
p ume p -h er10 ery W II e s
EX-02 "' -.,.,. ~:9:3-.· , 1.'1 ,..,~,04 : 106C tti·I? i ,-. l! (_.).:::,
Tag ltP-1 Tag#P-1031c· Tag P-10310
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