NCD991278953_19970401_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Fourth Quarter 1996 OU-1 and OU-2-OCR

I
I
I
I
I
D
D
D
m
m
•
I
I
I
I
I
I
ii
I
Quarterly Report
Fourth Quarter 1996
Operable Units No. 1 and 2 .
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
April 1997
L
JkY ~ 1097
I
I
I
I
I
I
I
I
m
I
I
I
I
m
I
I
I
I
I
Quarterly Report
Fourth Quarter 1996
Operable Units No. 1 and 2
RECEIVED
MAY 15 1997
SUPERFUND SECTION
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
April 1997
I
I
I
I
I
I
m
I
I
I
I
I
I
I
I
I
I
I
Table of Contents
1.0 Groundwater Monitoring Activities for the Fourth Quarter 1996 ..
2.0 Planned Groundwater Monitoring Activities ..
3. 0 References .
Appendix -Certificates of Analysis
Appendix A -Report of Laboratory Analysis
Plume Periphery Wells &
Trench Area Wells
Appendix B -Volatile Organics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix C -Semivolatile Organics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix D -Inorganics Analysis Data Sheets
Plume Periphery Wells &
Trench Area Wells
Appendix E -Chain-of-Custody Records
Plume Periphery Wells &
Trench Area Wells
Appendix F -Out of Service Well Pumping Records
Plume Periphery Wells and Trench Area Wells
Environmental Data Management, Inc.
P.O. Box 16326
Chapel Hill, NC 27516
IED1t't♦
5
6
I Environmental Data Management, Inc.
I List of Tables
I
I
I
I
I
D
I
I
I
I
I
I
I
I
I
I
I
Table Title
List of Sample Analysis and Water Level Monitoring Performed
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Fourth Quarter I 996, Plume Periphery Wells
3 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Fourth Quarter I 996, Trench Area Monitoring Wells
4 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Fourth Quarter 1996, Trench Area Extraction Wells
5 Groundwater Cleanup Criteria, Operable Unit No. I
6 Water Level Measurements, Fourth Quarter 1996, Plume Periphery Wells
7 Water Level Measurements, Fourth Quarter 1996, Trench Area Wells
List of Figures
Site Map
2 Quarterly Summary of Acetone -Plume Periphery
3 Quarterly Summary of 1,2-Dichloroethane -Plume Periphery
4 Quarterly Summary of 1,2-Dichloropropane -Plume Periphery
5 Quarterly Summary ofBis(2-chloroethyl)ether -Plume Periphery
6 Quarterly Summary of Acetone -Trench Area
7 Quarterly Summary of 1,2-Dichloroethane -Trench Area
8 Quarterly Summary of 1,2-Dichloropropane -Trench Area
9 Quarterly Summary ofBis(2-chloroethyl)ether -Trench Area
IO Groundwater Contour Map for October 14, I 996
11 Individual Periphery Wells Pumping Rate (Quarter 3-1996)
12 Combined Periphery Wells Pumping Rate (Quarter 3-1996)
13 Combined Trench Area Wells Pumping Rate (Quarter 3-1996)
I Environmental Data Management, lnc.
I
I
I
I
I
I
g
I
n
I
I
I
I
I
I
I
I
1.0 Groundwater Monitoring Activities for Fourth Quarter 1996
This fourth quarter I 996 report presents the findings from the groundwater monitoring
conducted at Operable Units No. I and 2 at the National Starch and Chemical Company
site on Cedar Springs Road, Salisbury, North Carolina. This report is prepared in
accordance with Record of Decisions (ROD) issued by the U.S. EPA on September 30,
1988 for Operable Unit No. I (OU!) and on September 30, 1990 for Operable Unit No. 2
(OU2). Operable Unit No. I consists of contaminated groundwater area located in the
west-southwest portion of the facility. Operable Unit No. 2 consists of contaminated soils
and surface water/sediments in tributaries surrounding a trench area west of the plant
operation area.
Operable Unit No. 1 (Plume Periphery Wells)
Groundwater samples from the four downgradient groundwater monitoring wells (NS29,
NS30, NS3 I, and NS32) and four bedrock extraction wells (EX0I, EX02, EX03, and
EX04) were collected on October 14, 1996. All samples were analyzed for Target
Compound List (TCL) volatile and semivolatile organic compounds (VOC and SVOC),
Target Analyte List (T AL) metals, and general chemistry. In addition, samples from the
monitoring wells and extraction wells were analyzed for selected water quality parameters
to monitor influent loadings for the Combined Pretreatment System (CPS). A sample
analysis summary is provided in Table I. The samples were collected in accordance with
U.S. EPA (Region IV) protocols. The TCL and TAL compounds were analyzed
supporting U.S. EPA Level IV Contract Laboratory Program (CLP) protocol.
The four plume periphery extraction wells (EX0I, EX02, EX03, and EX04) continued to
operate during the third quarter of I 996, except for a brief shut down due to a hurricane
'Fran'. In addition to the plume periphery wells, six extraction wells (EX0S, EX06,
EX07, EX08, EX09, and EXI0), located in the trench area, began a startup pumping
operation on February 26, 1996 (see page 3).
Results from the chemical analysis for Operable Unit No. I plume periphery wells are
presented in Table 2. The chemical analysis results for the Trench Area monitoring and
extraction wells are presented in Table 3 and Table 4, respectively. The list of compounds
presented in these tables represents the contaminants specified in Operable Unit No. I
Record of Decision (ROD). The list of designated compounds from the ROD (OU!) and
associated cleanup levels are provided in Table 5. Figure I is a site map showing the well
locations. The certificates of analysis are provided in the Appendix.
The results of this quarters sampling indicated that five organic compounds, acetone, 1,2-
dichloroethane (1,2-DCA), 1-2-dichloropropane (1,2-DCP), methylene chloride and bis(2-
chloroethyl)ether exhibited levels that exceeded cleanup levels (shaded bold faced values
in Table 2).
I
I
I
I
I
I
I
n
I
I
I
I
I
I
I
I
Environmental Data Management, Inc.
The acetone level remained above the cleanup standard in extraction well EX02 and
EX03. Acetone levels in extraction wells EX0 I and EX04 remained relatively unchanged,
below the cleanup standard. Since the previous quarter, acetone levels in monitoring wells
NS29 and NS30 remained above the cleanup standard. However, the level of the acetone
in the monitoring well NS29 decreased by nearly one-half, while the acetone level
increased in well NS3 l (see Figure 2). Monitoring wells NS30 and NS32 continue to
show no significant contaminant concentrations are present (see Table 2).
Also, Bis(2-chloroethyl)ether levels remained above the cleanup standard in most of the
OU! wells (see Figure 5) With the exception of Bis(2-chloroethyl)ether, extraction well
EX0 I did not exceed the cleanup standards for any of the other VOC compounds.
The general trends for the four organic compounds that have exceeded the cleanup criteria
over the past four quarterly sampling events are presented in graphical form on Figures 2
through 5. These four organic compounds are acetone, 1,2-dichloroethane, 1,2-dichloro-
propane, and bis(2-chloroethyl)ether. Manganese exceeded cleanup standards in two
wells (EX02 and NS29). Barium exceeded cleanup standards in three wells EX02, NS29
and NS31. Chromium exceeded cleanup standards in extraction well EX03 (see Table 2).
Water level measurements were taken on October 14, 1996, from seventeen selected
monitoring wells and ten extraction wells. The static water level for NS32 was not
measured, due to artesian conditions. Well NS32 has been under artesian conditions
during all previous sampling events. The results of the water level measurements are
presented in Table 6. A groundwater contour map of the subject area showing the
effectiveness of the extraction wells is shown in Figure I 0. The groundwater contour was
computer generated using a krig algorithm set to a linear type semi-variogram with a 50
foot x-y grid spacing.
During the past quarter, the extraction well system experienced some downtime which
kept the actual pumping rates below design rates. The well pumping data presented in this
report represents data recorded during the previous quarter (Quarter 3). A plot of the
individual pumping rates for each periphery well for the previous quarter in presented in
Figure I I. Note that the periphery well system was briefly shut down because of
excessive rainfall events caused by hurricane 'Fran'. The combined average quarterly
pumping rate for the four extraction wells (EX0I, EX02, EX03 and EX04) is about 60
gpm (see Figure 12). The efficiency of the plume control and hydraulic control will be
evaluated in more detail after all trench area extraction wells are fully operating.
2
I
I
I
I
I
I
I
•
I
I
I
b
I
I
. 1
I
I
Environmental Doto Management, Inc.
Operable Unit No. 2 Groundwater Monitoring
The Remedial Design/Performance Monitoring Work Plan for Operable Unit 2 states that
National Starch and Chemical may use the groundwater data collected for the OU!
monitoring program to satisfy the OU2 monitoring requirements. The monitoring plan for
OU2 requires the periodic sampling of groundwater from eight wells NS09, NSI0, NS! 1,
NS 15, EX06, EX07, EX08, and EX09. Additional groundwater data from extraction
wells EX05 and EX! 0 are also included in this report.
Trench Area Monitoring Wells
Groundwater samples were collected from monitoring wells NS09, NSI0, NS! 1, and
NS 15 on October 14, 1996. All samples were analyzed for selected TCL VOCs and
SVOCs, T AL metals, total dissolved solids (TDS), and chloride. A sample analysis
summary is provided in Table 1. The samples were collected in accordance with U.S.
EPA (Region IV) protocol. The TCL and T AL compounds were analyzed under U.S.
EPA Level IV CLP protocol.
Results from the chemical analysis for these wells are presented in Table 3. The list of
compounds presented in Table 3 represents the contaminants specified in Operable Unit
No. 1 ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 5. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
All four of the monitoring wells (NS09, NSI0, NS! I and NS15) in the trench area had
levels of 1,2-DCA that exceeded the cleanup standards. Monitoring well NS09 also
exceeded cleanup standards for I, I DCE, methylene chloride, and vinyl chloride.
Manganese exceeded clean up levels in monitoring wells NS09 and NS I 5. Monitoring
wells NS IO and NS I I continue to have manganese concentrations below the cleanup.
NS0? also exceeded the cleanup standard for chromium (see Table 3).
Water level measurements were taken on October 14, 1996 from each of the four
monitoring wells. The results are provided in Table 7. A groundwater contour map of the
subject area is provided in Figure 10 .
Trench Area Extraction Wells
Six extraction wells (EX05, EX06, EX07, EX08, EX09, and EXI0) began pumping in the
trench area west of the main plant on February 26, 1996. With some minor adjustments in
the pumping rates for the individual wells, the wells have been pumping at a combined rate
of about I 6 gpm. A chart showing the combined pumping rate for the six extraction wells
3
I
I
I
I
I
I
I
I
I
I
D
I
I
I
Environmental Dato Management, Inc.
during the previous (Quarter 3) is presented in Figure 13. Note that the trench well
system experienced a reduced combined pumping rate for approximately a two week
period in early August because of pump motor problems in well EX08. The pump motor
in well EX08 was subsequently replaced. Well EX08 pumping problems were noted in the
monthly progress reports for Quarter 3.
With the start up of the trench area extraction wells, the trench area pretreatment area was
also utilized for the first time. Problems with this start up have been noted in the monthly
progress reports.
Groundwater samples were collected from the six new extraction wells on October 14,
I 996. This report presents the laboratory analysis results for the second time since the
wells went into operation during the first quarter of this year. All future quarterly
reporting for OU! and OU2 will include the sampling and analysis of groundwater from
these wells.
All samples were analyzed for selected TCL VOCs and SVOCs, T AL metals, total
dissolved solids (TDS), and chloride. A sample analysis summary is provided in Table 1.
The samples were collected in accordance with U.S. EPA (Region IV) protocol. The
TCL and T AL compounds were analyzed under U.S. EPA Level IV CLP protocol.
Results from the chemical analysis for Trench Area are presented in Table 4. The list of
compounds presented in Table 4 represents the contaminants specified in Operable Unit
No. l ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 5. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
The results of this quarter's sampling indicated that nine organic compounds, acetone, 1,2-
DCA, 1,2-DCP, methylene chloride, toluene, 1,1,2-TCA, vinyl chloride, xylene, and bis(2-
chloroethyl)ether were found in one or more of the trench area extraction wells and
exhibited levels that exceeded cleanup levels (shaded bold faced values in Table 4). Note
that not all of the above mentioned compounds were found in any single extraction well,
however, acetone, 1,2-DCP, methylene chloride, and toluene appeared to be present in all
of the trench area extraction wells.
Three other VOC compounds, not part of the ROD (OU!) listed contaminants, were
found in the trench area wells. These VOC compounds are I, I Dichloroethane, 4-Methyl-
2-Pentanone, and Acrylonitrile. These compounds were found in relatively high
concentrations in EX0S, EX07, EX08, EX09, and EXI0 (see Table 4).
Also, five inorganic (metals) compounds including, Beryllium, Cadmium, Chromium,
Manganese, and Nickel were found in concentrations exceeding the cleanup standard in
wells EX0S, EX07, EX08, EX09, and EXI0 (see Table 4).
4
I
I
I
I
I
I
I
I
I
m
I
0
Environmental Data Management, Inc.
For comparative purposes, the four organic compounds that have exceeded the cleanup
criteria for the plume periphery wells are presented in graphical form on Figures 6 through
9 for the trench area wells. These four organic compounds are acetone, 1,2-
dichloroethane, 1,2-dichloropropane, and bis(2-chloroethyl)ether. Note that several of the
compound concentrations shown on the figures have an asterisk. The asterisk indicates
that the detection limit for that compound exceeded the groundwater clean up standard.
2.0 Planned Groundwater Monitoring Activities
Plume Periphery Wells
The implementation of the extraction well system will continue as planned with the 24-
hour operation of the plume periphery extraction wells EX0I, EX02, EX03, and EX04.
Groundwater monitoring will continue. Care will be taken to closely monitor the daily
pumping rates of the extraction well system. Particular attention will be made io assure
that all plume periphery extraction wells continue to pump at optimum efficiency and that
downtime for pump maintenance is minimized.
National Starch and Chemical Company will continue to alert laboratory personnel of
samples from wells with known high VOC concentrations.
Trench Area Wells
The six extraction wells will continue to operate 24-hours a day. During this startup
phase the extraction wells will be monitored closely and their pumping rates may be
modified in order to optimize their performance. The efficiency of the plume control and
hydraulic control for both Operable Units I & 2 will be evaluated in more detail after all
trench area extraction wells are fully operating.
Groundwater monitoring will continue. Very high concentrations of VOC compounds
found in the trench area wells will require that laboratory personnel be alerted prior to
testing groundwater samples so that proper procedures can be taken to minimize
laboratory contamination and improve compound detection limits.
Groundwater level measurements will be taken prior to the sampling of the extraction
wells so that the effectiveness of the pumping program in the trench area can be evaluated.
5
I
I
I
I
I
I
I
I-
I
I
I
I
I
I
Environmental Data Management, Inc.
3. References
EDM, Inc., February 1997, "Quarterly Report -Third Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., August 1996, "Quarterly Report -Second Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., May 1996, "Quarterly Report -First Quarter 1996 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., February 1996, "Quarterly Report -Fourth Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., October 1995, "Quarterly Report -Third Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., August 1995, "Quarterly Report -Second Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, May 1995 , "Quarterly Report -First Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, February I 995 , "Quarterly Report -Fourth Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, October 1994 , "Quarterly Report -Third Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
North Carolina Environmental Management Commission, North Carolina Administrative
Code: !SA NCAC Subchapter 2L (August 1993).
U.S. EPA, September 30, 1990, Record of Decision (ROD) for Operable Unit No 2,
National Starch and Chemical Company, Salisbury, NC.
U.S. EPA, September 30, 1988, Record of Decision (ROD) for Operable Unit No I,
National Starch and Chemical Company, Salisbury, NC.
6
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Environmental Data Management, Inc.
Table 1
List of Sample Analysis and Water Level Monitoring Performed
Fourth Quarter 1996
Operable Units No. 1 and 2
National Starch and Chemical Company
Salisbury, North Carolina
Well Number Well TCL TCL TAL Water
Tu=' VOCs' SVOCs' Metals' TOS'
0nerabIe1unitNo!t1,,eIiime''PenotiervWeII~
Ch~ride . COD' TKN' Level ;n ... ~ ........ ,.,: ..
EX01 BE X X X ' X ..... ''EX62 BE X X X ! X .............. ·······-· ..... i. i -..... -l---
EX03 BE X X ) .... X ! X
EX04 BE X X X X
~~~~ I i~ i 1
NS22 BM
NS23 SM ············-···· NS26 i BM ....... ····-··· .... :· . ···········-·· .: ... NS27 1 BM i
NS28 BM
NS29 BM . -·····-NS30 i BM . . . . ' ! . .
NS31 BM
NS32 BM
P01 BM
Stream i NAg ·
(3-auge_No, 11!.
Stream
Gaune No. 2 i
NA
X
X
X
X
:.. ......•............ j ..
............. : _______ :
X
X
X
X
i
. . . . . . . . . . . : . . . i
X ! X
X X
X X
X X
X X X X
X X X X .. ···! X X X X .... , ............................... -..... ···-... .
X X X X
X
X
X
X
X
X
X
X
i ~ ... i .
----······· )( X
X
X
X ---············•·--x
X
X
X
.... ' . . •, : ·.:-:-.
NS09 SM X X x_~~x---'---~x_ X
X
X
X
NS1_Q .. l . ~M ..... .l.<:.. . . ,, .. , .X.. X i . X X
NS11 SM X X X i X X
NS15 BM X .... X r X X X
f;l<_Q~ -'--=B::=E:........-'--...:.:...-X X ! X X .. . ..................
EX06 BE X X X X .. --··-··· ········-···· .. --. , ..... EX07 BE X X .. X X ' EX08 BE X X X X
EX09 BE X X X X
EX10 BE X X X X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
aBE -= Bedrock extraction well, BM = Bedrock monitonng well, SM = Saprollte (shallow) monitoring well
bProject TCL consisting of 13 VOCs, 2 SVOCs, and 9 metals, and meets Operable Unit No. 1 cleanup criteria (Table 5).
cTDS -Total dissolved solids
dCOD -Chemical oxygen demand
'TKN • Total Kjeldahl nrtrogen
'Iron pins in southwest tributary for monitoring stream elevations.
gNA -Not Applicable
X
X
X
X
X
X
I Environmental Data Management, lnc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Table 2
ROD (OU1 I Contaminants and Selected
Water Quality Parameters in Groundwater
Fourth Quarter 1996
Plume Periphery Wells
National Starch and Chemical Company
Salisbury, North Carolina
Extraction Wells Monitorina Wells
Well Number: EX01 EX02 I EX03 EX04 NS29 I NS30 I NS31 I NS32
Sample Date: 10/14/96 10/14/96 I 10/14/96 10/14/96 10/14/96 I 10/14/96 I 10/14/96 10/14/96
Volatile Organics (ug/1)
Acetone 10Ui 32000E\ 10000Ei 380E i 48000E i
Benzene 1 OU! 250U ! 250U i 0.6J: SOOU !
Bromodichloromethane 10U! 250U( 250U :~.~~-i ... SOOUi ..
Chloroform --------,-ou]" 250U 250U 1 OU' SOOU i 11--------------+----~--------+----+---1,2-Dichloroethane, ____ 5~_! ........ 140J; __ 60J_,_ 3J: 1200i
. _1,1_:~ichloroethylene 10U 250Ui 250U 10U --soo(/
_____ 1,2:Dichlo_r_o_propane __ 1J _____ 100,Ji 71J 1/ ----1800! ... ; .. Ethyl benzene 1 OU 32J, 250U 2J, SOOU;
,au 5411ooe1 10u
10U --iiioout· 10U
,au. ,oooul ,ou
10U 1000U! 10U
,au -c,11""0J=; --,-o"'u
10U -iiiiiou I
,au -----· 1siif
10U ,ooou
_____ Methylene_Chloride 0.6Ji 18J 16J[ 1J' 37J-i ---
-_ _ __________ Tol~e_n_e 1J 250' 120J 26' 44ilj(
0.6J-'''''' ,ci(j 110J
,ou
,au
10U
0,7J
,au
,au
10U
1,1,2-Trichloroethane ,au 250U' 2sou 10U' sooui
Trichloroelhene 1 OU 250U' 250U 1 OU i SOOl.i!-11---------cc~-:c---~I -ccct-~=~~=+--=~ Vinyl Chloride__ ,au 2sou; 250U ,au soou 1
-----~-x-y1-e-ne1---,7ou-,1-: -26Ji 2sou1 SJ-----56J\
Semivolatile Oraanic Cua/ll
Bis (2:<::~loroethyl) Ether
4-Nitrophenol
lnoraanics Cua/ll
171
25Ui
3_00Ef.
25U
1301 ,oou! 49j
25Ui
Arsenic 1.1ur 1.1u; 1.1U! 1.1u:
,, ___________ B_a_n_·u_m_,_ __ -_12_e_"t~ __ 1_·3_7_Q~(_· __ :i_·49·1 ... EffSBT
Beryllium a.JU i 0.3U i O.J_U_j 0.3U i
Cadmium .... ~ ... ~~.J.. ..... 4'.~U.'. 4.BU i 4.BU:
Chromium 4.9U! 17.1: ------iiist'" 4.9U•
.. -;;..;a·nganese 2os1 18800! ····· .. 3920·1 · 3340;
740!
isoui
,_,u,
. 11&0[
a.JUI
4.su:
4.9Ul 6840! ...
15.JU' 11--------:::::::::::::::~~=N:::ic:::ke:::1::::::::::,~s:::.J;u;,:::::::::,:s~_~J:::u;,::::::::::::,a~,_:~~.:; -::_-::_1~s~.J~u~'-
se1enium _ O.BU_\____ O.BU: O.BU ! O.BU · ---,--_suj"'
Zinc 33.9 i 28.2: 34.0 i ----1 mi" 19.0B i
Water Quality (m11/ll
COD 26 840"
Chloride 93 1 1 oo( .
N~rogen (TKN) <0.1 6.2 !
ll---------"-~~T=D~S+---~,~SOO=c'i-~3800'
Note Data Qualifier Definitions:
270!
' ... ' 210;
1,2!
2500!
130'
140
1,2,
3200'
B (Organics) = Compound was detected in the 11ssociat11d blank.
NA'
BHJi
NA• ''' -1-5100;
,au
10U_
10U'
,au·
4Ji
25U 1
uu
32.1B'
O.JU-
4.BU
4.9U-
1400
37QJ!
,oooui
,oooui
,ooou
1000U'
220Ei
soui
,au
,au
,au
25U
uu, ,.,u
6280: 91.SB ...... ·•···········-· ...... a.Ju, a.Ju
4.BU : 4.BU
4.9U! 4.9U
s,oi 109
15.JU-
O.BU--~=
15.JUi
O.BUi
15.3U
O.BU
23.51 15.38[ 19.9B
NA NA\ NA
60 530i ,,
-----NA( NA NA
1500' "'4iioo'i --1700
B Unorganicll) = Compound concentration is below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace value, or it is II nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
mass spectrometry inatrum11nt.
NO = Not detected at or above the detection limit of analysis method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates a detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30·88).
I Environmental Dato Management, Inc.
I
I
I
I
I
I
u
I
I
I
I
I
I
I
I
I
I
Table 3
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Fourth Quarter 1996
Trench Area Monitoring Wells
National Starch and Chemical Company
Salisbury, North Carolina
Monitorina Wells
Well Number: NS09 I NS10 I NS11 I NS15
Sample Date: 10/14/96 I 10/14/96 I 10/14196 I 10/14/96
' -
Volatile Organics (ug/1)
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-0ichloroethane
200'
100U!
10ou:
----ioou
5800Ei , __ _ ·-----•······'"·· .. •···.
1&JI ... ,.: ~ -~ichloroethyl~ne
. 1_ ,~.-Di~hl~~op~~p~~~ .
Ethy1benzene
100U'
BJ'
............. 7Jj 200:
1oou' .........
1oou'
100U! 10U 10U
1oou: 1ou-10U
1oou: 10U' 10U
100U 10U 10U
__ 4800E\_ ___ 34: 150
1oou-10U 10U
100U: 10U: 10U
1·001/ 92' 10U
______ 7Ji __ 10U 1J
9Ji 19 6J
100U: 10u' 10U
ioouT 10U' 10U
.. Methylene Chloride
Toluene
_1, 1,2-T_richloroethane
Trichloroethene
Vinyl Chloride --------·•·-----··'"
Xy1ene
Semivolatile Organic (ug/1)
-------_ ---_6,i~(2_:~~l?rc,ethyl)_E'.her
4-Nitrophenot
lnoraanics !ua/ll
Arsenic
Barium
Beryllium
Cadmium
1101
21Ji
uu: . ·········755t
0.48i
4_au,
Nickel 40.9:
-~s~.,~.n~iu-m
Zinc
Water Qualitv Ima/II
0_8U'
84_2!
100Ui ---••···········••----·•·-·· 100U
UU!
293:
0_3Ui
4_su-
4_9u
-4850
35.48'
0_8U'
41.1
COD NA 210
" Chloride 1100; 490 !
10U
140
10U
25Ui
uu
301
0_68
4_8U
34_2,
841'
40_7
o_su-
65_0
210
4_2-
n--------N-lt-,og-en-(TKN)t----c,NccAcc:-----ccN-coA--c: ----,c--c---NA
TDS 4900' 3600: 24001
Note Data Qualifier Definitions:
B (Organics) = Compound was detected in the auociatad blank..
B (lnorganica) = Compound concentration is below the contract•required detection limit.
10U
1J
10U
25U
uu
405
0_3U
4_8U
4_9u
13800
15_3U
0_8U
30_6
NA
1000
NA
4400
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace vatue, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
men spectrometry instrument.
ND = Not detected at or above the detection limit of analysis method.
NA = Not analyzed.
Also Note: Shaded bold face d11t11 indicates II detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30-88).
I
I
I
I
I
I
I
I
u
I
I
I
I
I
I
I
I
I
I
Environmental Data Management, Inc.
Table 5
Groundwater Cleanup Criteria
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Compound Cleanup Concentration (ug/1)
, ... , , ,.•;; _.::';:'.,c. J1 .... ,•,;\:1•,i•)•••P:I/
.,J",,,,:,;.:;',('',•:;(];,;;::,,:,),k;l•il;:. Volatlle'10rganics' ,,,,,,,,, ; ,,,,
· ... •1.. , , .. ,_i', .. -... , ,,.:,.,,•1,;·t.1.,:, .. .-.... '•.:=.·. ,,,,. 1\?u:J:r 01;
Acetone: 3500 ·····················-Be~n--'z~e~n--'e~! _______ 5 ll-------8-ro_m_o_d_ic_h_lo_r_,omethanei 5
.,., , Chloroform[ 5
___ 1'-'-,2~---=D"-'ichloroethane(DCA) 5
1, 1-Dichloroethylene:_________ 7
1,2-IJichloropropane! ... 6
Ethylbenzenei 3500
... Methylene ctiicinciei 5
,~------------'T--=oc::lu~e~nc=e~l _____ __,2000
... 1, 1,2:Trichloroethane (TCA)[ . 5
, .. i:.nc:hlorciethei,nl:l (}:C:Ef 5
·-----'V'-'-inyl Chloride' 2
X lenei 350
Arsenic, 10 ---------'-==--•····-····
ll--------------=B~a~ri~um::.:.c., _______ 1000
''' ,,,,, BeryUiurn 17.5
Cadmium 10
Chromium 50 ---------~~ ······--·•----·-.. ··· ,. ___________ c:Mc::a:.:..:ng,;:a::;nc=e-=s.=:e;..., ______ .-:7.-:7..:0:.:::0
Nickeli 350 ···· ·· ·· ·· •···· ·· · ·· ····· ·· ··· · ·· ·· se1eniur11l 1 o
.,., ••••••••• j.
Zinc! 7350
Reference: U.S. EPA , September 30, 1988, Record of Decision (ROD) , Operable Unit No. 1,
National Starch and Chemical Company, Salisbury, North Carolina.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Environmental Data Management, Inc.
Table 6
Water Level Measurements
Fourth Quarter 1996
Plume Periphery Wells
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to Water Level
Measurement Point of Elevation Water Elevation
Well Name Date Reference (Ft. MSLI IFt.) IFt. MSL)
l----'E=-X-'--=0-'-1----'---i --'1CCOC.C/1--'4/cc9~6-'-, __ Tc_:Oc_:C=--------'----'-'73c_:1C-"_8,_,,5'------'---' _ ~o~,QQ ----------625,85
EX02 , 10/14/96 TOC 718.24 61.96 656.28 ····----···•--------··············-··•·--• ········-........ ·····--·•·--·• ..................... ·······--·--.......................................................... . EX03 , 10/14/96 TOC 740.46 94.00 646.46
EX04 10/14/96 TOC 754.12 74.00 680.12 . .. .. ..... ..
NS05 10/14/96 TOC_~ __ __..c.7::.67:..:..9::.:6:__ ____ 2_1_.6!........... 746.29
NS06 10/14/96 TOC 738.87 8.00 730.87 ........................... ····•·--·• ---•• ········-········-••·-·•·---NS21 10/14/96 TOC 739.13 6.00 733.13 .......... ····--
NS22 10/14/96 TOC 715.94 18.00 697.94 ---····················--··-··· ...... . NS23 10/14/96 TOC 752.36 22.25 730.11 ....................... ______________ ............ ·····•·--•
NS26 10/14/96 1 T<:lC: ___ .... 720.77 __ . _________ 8.42 _ 712.35 _____ _
NS27 10/14/96 -TOC 749.47 20.42 729.05 ···-~-..
NS28 10/14/96 TOC 767.82 22.50 745.32 ...... .....•... . .. ••······
NS29 10/14/96 TOC 715.50 47.42 668.08 1--~~................................ ...................... . ..... ··-••---••····················••---·•···············
NS30 10/14/96 TOC 718.54 27.54 691.00 .......................... --•· ·····-............. ···•--.-• ···················-···•···•·-························--••···· NS31 10/14/96 TOC 711.15 45.33 665.82 .... ,.... . ....
NS32 10/14/96 TOC 699.48 NA" NA"
P01 ; 10/14/96 --' TOC 708.09 _--_--_-_ NAb ---NAb
SG1 10/14/96 TOC 712.26 NAb NAb l---=-SG2 -·········· .... fo/14i96 . 'foe· . 693.:.::_9=-0 -.......... NA' .... ---··----· NAb
NA• • Not Applicable, well is artesian.
NAb • Not Applicable, well is dry, or stream level not measured.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
D
D
I
Environmental Data Management, Inc.
Well Name
EX05
EX06 ...............
EX07 ..
EX08
EX09
EX10 --·-·········· NS09 . """ NS10
NS11
NS15
Table 7
Water Level Measurements
Fourth Quarter 1996
Trench Area Wells
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (Ft. MSL) (Ft.)
10/14/96 TOC 781.26 33.50 ---------· 10/14/96 TOC 788.28 40.50 .. ··············-------··········· ........ . ................. ........ ·-····················----·•····· -------······ 10/14/96 TOC 789.23 27.08 ........
10/14/96 TOC 789.19 47.75
10/14/96 TOC 782.29 34.50
10/14/96 TOC 775.92 32.58
. ....
........ ......... ......... ------.. -• .......
10/14/96 TOC 778.45 29.67
10/14/96 TOC 786.72 34.00 .............. ···················· ................... ···········••· ----· 10/14/96 TOC 775.65 21.17 ,.,. ..... _______ ,., ........
10/14/96 TOC 792.60 43.67
Water Level
Elevation
(Ft. MSL)
747.76 ·······-···-···············-········ 747.78 ......................
762.15
741.44
747.79 ······--·--·······--··········· 743.34
748.78
752.72
754.48 ---······-···········-·····-·· 748.93
11111 == == 111111 lliil liiiii iii iiiii -----------
I·
~~+ 3
,/~•-· ~-I \ ~·
!Environmental Data Management, Inc.
National Starch & Chemical Company
Cedar Springs !Road
Salisbury, North Carolina
/ I
+-Monitoring Well
--Roads, Buildings. etc.
--~ Fence Line
t-t+H+t-Railroad
-----Property Line
-Tributary Stream
-n~ ----Topographic Contour Line
(Ft.. ~SL) Contour ln!.-,voi ~ 5ft.
0 400 800 1200
~-I I Scale In Feet
Scale 1 Inch = 800 Feet
Site Map
4th Quarter Report 1996
For
Operable Units I & 2
!!Ill 111111 -== --iiiii iiii iiiil ------ -- --Figure 2 m :, < a· :,
3 m :, fl:
Quarterly Summary of Acetone Concentration C, ~ s: 100,000 a :, a "' """' ~ 3
90,000 m ~
c," r
80,000
70,000 m Qtr1 • '96
Oil Qtr2-'96
::: Ell Qtr3-'96 "' 60,000 · ::,
.5 S.000 ■Qtr4-'96
C
0 :;::; 50,000 · ~ -C .. " C 40,000 0 (.)
30,000
20,000
10,000 · 3,500 ug/1
---------------• ~r~u_n~_t1:r f:~8!-~up ___
0 .
EX01 EX02 EX03 EX04 NS29 NS30 NS31
Monitoring and Extraction Wells • Plume Periphery
EDN Quarterly Report For
National Starch and Chemical Company Operable Units No. 1 & 2
Environmenlal Oala Management, Inc. Salisbury, North Carolina 4th Quarter 1996 April 1997
-liiii iiliii iiii - - - -
Figure 3
Quarterly Summary of 1,2 Dichloroethane
10,000
1,000
=:::
"' :::,
C
C 0 :;::: 100 ~ -C .. u
C 0 u
10 -
1
EX01 EX02 EX03 EX04 NS29
Monitoring and Extraction Wells . Plume Periphery
Note: Concentrations depicted with iln asterisk or at or below 5 ug/1 1epresenl the detection limit of laboratory analysis method
EDN
Environmental Data Management, Inc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
--
NS30
-
NS31
- -
t!il Qtr1-'96
fill Qtr2-'96
1111 Qtr3-'96
■Qtr4-'96
····-5 ug/1 -Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
a,
:,
C
C
0 ~ -C .,
u C
0 0
==
10,000
1,000 ·
100
10 ·
1
EX01 EX02
-liiii iiil ilii - -Figure 4
Quarterly Summary of 1,2 Dichloropropane
EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
Note: Concentrations depicted with an asterisk or at or below 6 ug/1 rep1esent the detection hm1t of laboratory analr-,is method
EDN
Environmental Data Management. Inc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -
NS30
-
NS31
- -
!!ii Qtr1-'96
IIIl Qtr2-'96
11!1 Qtr3-'96
■Qtr4-'96
6 ug/1-Cleanup
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
l!!!!!!!I I!!!!!! --=
10,000
1,000
ci :,
C:
C: 0 :;:: 100 .. --C: .. u C: 0 u
EX01
EDN
Environmenlal Data Management, Inc.
April 1997
== 1111111 llii liiii iiii ---- -
EX02
Figure 5
Quarterly Summary of Bis(2-chloroethyl)ether
EX03 EX04 NS29
Monitoring and Extraction Wells -Plume Periphery
National Starch and Chemical Company
Salisbury, North Carolina
NS30
- - ---
l!l Qtr1 -'96
llD Qtr2-'96
1111Qtr3-'96
■Qtr4-'96
5 ,gll
~ Cleanup Concentration
NS31
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
1!11!1 I!!!!!!
e:: "' ::,
.5
C 0 :;: I! -C .,
u
C
0 CJ
EDN
==i 1111 a; liiii &ii liiii ---------
Figure 6
Quarterly Summary of Acetone Concentration
80,000 ---------------------------------------~
70,000 +-----------------------
60,000 -·/------------------------
50,000 -
40,000 -
30,000 -
20,000 +-----
10,000 __ , ___ _
3,500 ug/1 Groundwater Cleanup Cone.
EX05 EX06 EX07 EX08 EX09 EX10
Monitoring and Extraction Wells -Trench Area
!ill Qtr3-'96
■0tr4-'96
Environmental Data Managemenl, Inc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
I!!!!! == liiiiiil iiil iiiil --Figure 7
Quarterly Summary of 1,2 Dichloroethane
1,000,000
100,000
10,000
=::: CII :,
·= C 0 :;::: 1,000 t!! ... C .,
u C 0 0
100
10
EX05 EX06 EX07 EXOB
Monitoring and Extraction Wells -Trench Area
Note. Concentrations depicted with an asterisk 01 al or below 5 ug/l represent the detection hmit of laboratory analr-,is method
EDN
Environmental Dala Management, Inc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -
EX09
- - -
!iii Qtr3-'96
■Qtr4-'96
Concentration
EX10
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
-l!!!!I liiii iiii liiii - - --Figure 8
Quarterly Summary of 1,2 Dichloropropane
100,000
10,000
a,
:,
C
C 0 .:: ., --C .,
L> 100 C
0 0
10
EX0S EX06 EX07 EX08 EX09
Monitoring and Extraction Wells -Trench Area
Note. Concentrations depicted with an astem;k 01 at or below 6 ug/1 represent the detection hm1t o1 laboratory anal~is method
EDN
Environmental Dala Management, Inc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -- -
lli1Qtr3-'96
■Qtr4-'96
Concentration
EX10
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
l!!!!!I == liiill iiiii --- -Figure 9
Quarterly Summary of Bis(2-chloroethyl)ether
100,000
10,000 ·
=:: Cl 1,000 · :,
C
C 0 .:: I! -C ., • • u C 100 -0 u
1
EXOS EX06 EX07 EX08 EX09
Monitoring and Extraction Wells -Trench Area
Note: Concentrations depicted With an asterisk or at or below 5 ug/1 represent the detection limit of laboratory analysis method
EDN
Environmental Oala Management, Jnc.
April 1997
National Starch and Chemical Company
Salisbury, North Carolina
- -
EX10
- -
!li!Qtr3-'96
■Qtr4-'96
5 ug/1
Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
--l!!!!!I 1!11!1 == --&iiiiii iiiii -- - - -
, Sre111
·. Ga1 ge #' ,,
7
NS30
Stream
/ ✓ NS28 "
k¼=\===4=~~~
I
SQ5_
--.:..,::::::::--__
AG0011 ~ -
0--."-; ~ "O
.. 4 \\\
' I . '
NSJ5
/ I
PLAHT AREA
D .. :: ,•
0 200 400 600
1"'1"'.'-""'•1.-~'-E=I /, Gauge # l I
Scale in Feet
Scale 1 Inch = 400 Feel
Roads, Buildings, etc.
Fence Line
Property Line
Tributary Stream
-725-Groundwater Contour Line (Ft. !vi.SU -+i~ Monttormg Well
$
7
I·lew Startup Extraction Wells
Stream Gauge
\ I
Mational Starch & Chemical Company
Cedar Springs Road
Salisbury, Horth Carolina
Environmental Data Management. llnc.
figure 10
Groundwater Contour Map
for October 14. I 996
4th Quarter Report 1996
For
Operable Units I & 2
- -m :, < er :,
3 "' :,
[
" ~ ;:
0 :,
0 "' "' 3 "' _a
5' 0
11111111 == == == -11111111 liliiiiiil iiiii liiii iiiiii - ---- - - -Figure 11 Individual Periphery Wells Pumping Rate 35 T Heavy rain event on 912/96 and from ~, / Hurricane 'Fran' on 9/6/96 caused pumping · · :_........ / system to be shut down because of too much water for lagoon. 30-I ·························~···· 25 ~.... . .. l/1. ~'XX :e 11. C) :=-i ... ~._ X X ?00<-• ~ 20f ~~·· · .• .. i ·········••··.. . ............ . ~ I ' . ~ .........• 8. • 11 I! i I :~~ . ········ X .. ·····~ ~·········· .. ~ I ............'. : .................................. . ii II I i a: 15 i I Cl 1111 ,5 j , EX01 pump down for repair. A a. I/ ,._ E I ::, , , t,,.t,,' MA 'I ' . 0... 1 Q _ ____ ' ------· ,PAAAAAAAAAAAAAA_ .... ········· AAAAAAA ·· ··········.WM·····-·A----· --··\·1·1/t,.:··.* .. Al I · M :' 66666666 : ·:A! AAAAAA AAAAAA ·.MA/ \_ ,i ' " ll: .Ii □ AAAAAAAAA ! . . .. .. ... ... . t,,.t,, . . ... " t,,.t,,t,,.t,,6 ! --,.,,,,,,,.,,,,. '1 0 DQ p CDXIJ□[l□□□□□a:ICIJ□CIJ□[X] ;·. 111: \I!' 5 I?· j D HI•• j · .. rm tx:u:xx:ncx:n··· ······ I I I I I• U II HI H H II I d I•• Id• I I·;····', ', o,□c;I,. i;o::iq CD□CDQ [][J[JQ················ P t::n:D tJ a::D, !, ,; i, a a i I I A ii ii I j ; 0 -1-t-t-l-t-t-t#f-H-t-H-H-t-t-H-t-H-t-t-H-t-l-t-t-t-t-t-H-t-t-t-t-t-H-t-H-t-f-H-t-H-t-t-t-t-t-t-HH ~•·t-t-H-t-t-t-t-f-t-t-t-t-H-t-t-H-l-t-t-t-t co co co co co co co co co co co co co co co co co co co co co co co co co co co co ID ID ID "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' "' <J) ~ "' -;;, - -;;, (0 -"' '° co -;;, - -"' '° - - -;;: -£:! '° co -;;, -a -;,; ~ r---0 "' ~ ~ "' CX) ~ ... 0 ~ r---(<) ID -;;: -~ ~ ~ ~ !:::I !:::I N (<) --~ ~ ~ N !:::I N (<) ;,; ;,; ~ ~ ~ N N N N r---r---;;: - - - --CX) CX) CX) - -co co -co "' - -;,; -;,; - -r---r---r---r---r---r---r---CX) CX) CX) CX) "' "' "' "' "' Quarter 3 -1996 (July, August, September) ♦ EX01 · · o · ·EX02 · -6 -EX03 -----M-EX04 EDN Environmental Data Managemenl, Inc. April, 1997 National Starch and Chemical Company Salisbury, North Carolina Quarterly Report For Operable Units No. 1 & 2 4th Quarter 1996 -m ~ < g· 3 .. ~ [ ~ Q s: Q ~ Q "' .. 3 .. ~ 5" 0
-I!!!!!!!! -1111111 liiiiii liiii iiii -- - - -
Figure 12
Combined Periphery Wells Pumping Rate
80 ------------------------------------
EX01 pump down for repair.
30 · · ~
II::
"' .!: 20 a. E ::,
11.
EDN
10 ·
0
<D ~
~ ;:::
''
<D <D <D <D ~ ~ m m 0 ;;; ~ t: ~ ~ ,-.. ,-.. -;::: ,-..
Environmental Data Managemenl, Inc.
April, 1997
<D <D <D <D m m m m ----<D m "' "' ~ ~ ~ ~ ;::: ;::: ,-.. ,-..
•
••••••••••••• •••• •••••. 1. ..
............... ( ...
. . . '
'' '.'' '
<D <D <D <D <D <D <D <D <D <D <D <D <D m ~ m m ~ m m m m m m m m
ii, ;;; ---ii, ---0 -~ ~ m "' "' ~ ... ,-.. ~ ~ "' ii, -~ ~ ~ ~ ~ ~ "' -co co ii, --ii, ,-.. ,-.. co co co co co
<D m '° -m
Quarter 3 -1996 (July, August, September)
National Starch and Chemical Company
Salisbury, North Carolina
Heavy rain evenl on 9/2/96 and from
Hurricane 'Fran' on 9/6196 caused
pumping system lo be shul down
because of loo much water for lagoon .
''' ' , , I 1 I,
<D <D <D <D <D <D <D <D m ~ m m m m m m -~ --;;; --co ,-.. 0 <D m a; ~ ~ ~ ~ "' ~ "' --a; -a; m m m m m
- - -
1-o-Combined Rate I
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-
-11!!1!1 !!!!!I liliiil iiii ---- - -
Figure 13
Combined Trench Wells Pumping Rate
16.4 ~------------.r.llA-·----------------------------------7
:;;; l); 16 .2 +,1·o6.il ·o6,!"6,! ··"6,!"6,!16,!16,!!,lMM!,,116
C
0 ~ 16 >< w
"0 ~ 15.8 .,;
0 >< w 0015.6
0 >< w
::; 15.4 >< w .,;
~ 15.2 w .,;
0 ~ 15
~
it: 14.8 · ..
Cl
C ·5.
§ 14.6 · ·
D.
Pump motor in EXOB down for repair.
14.4 f-++t+H-t+-t+t-t-t-l-t-t-l-l+-t-l-l-t-+-t-l-l+-t-l-H-H+-t-H-+-t+-t-H-+-t+H+-t-l-H+-t+-t-t-t+t-1-H-t-H--t-l·I-I-I-I-I-I-I-H+-t-t-+l-t+t-l-H-
<D <D <D CJ> CJ> CJ> -.;, -~ CJ> ;::: ;::: ;:::
EDN
Environmenlal Data Managemenl, Inc.
April, 1997
<D <D <D <D CJ> CJ> ~ CJ> -;::: .;, (") ~
~ ~ N ~ ;::: --r--r--r--
<D <D <D <D <D <D <D <D <D <D <D
CJ> CJ> CJ> CJ> CJ> CJ> CJ> CJ> CJ> CJ> CJ> ---0 ~ -N <O ---CJ> ~ <D CX) 0 (") r--
~ -~ ~ ~ N N (") --CX) CX) o3 o3 o3 --o3 CJ> CJ> r--CX) CX)
Quarter 3 -1996 (July, August, September)
National Starch and Chemical Company
Salisbury, North Carolina
<D <D <D <D <D ~ CJ> CJ> CJ> CJ> .;, ol -;::: ~ (")
~ ~ ~ N ~ ol -ol ol CJ> CJ>
-- -
j-A-Combined Rate I
Quarterly Report For
Operable Units No. 1 & 2
4th Quarter 1996
-m :, < er :,
3
<!) :,
[
0 ~
;::
0 :, ,g
<!)
3
<!) _a.
:,
0
I
I
I
I
I Appendix A
I Report of Laboratory Analysis
Plume Periphery Wells
I
I
I
I
I
I
I
I
D
u
I
•
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
m
I
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
December 05, 1996
Mr. Ken Kluttz
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 2B144
RE: PACE Project No. 661015.501
Client Reference: CLP Quarterly Monitoring
Dear Mr. Kluttz:
Enclosed is the report of laboratory analyses for samples received
October 15, 1996.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
J~J1
Felicia C Grogan ~
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.
Tel: [phone]
Fax: [phone]
-Pace Analytical
December 5, 1996
Mr. Ken Kluttz
National Starch and Chemical Co.
485 Cedar Springs Road
Salisbury, NC 28144
PACE Project No.: 661015.501
CASE NARRATIVE
Client Reference: Quarterly Monitoring
Sample receipt:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Su rte 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
•· .... --------A total of fourteen water samples were received at Pace Analytical Laboratory in
Huntersville, NC on I 0/ 15/96. The samples were logged into the Laboratory Data
Management System and PACE laboratory sample numbers were assigned to the samples.
Samples requiring CLP Volatiles, CLP Semi-Volatiles, CLP Metals, and TKN were then
shipped via Federal Express on I 0/15/96 to Pace Laboratories in Houston for analysis.
Sample ID PACE -Charlotte ID
NS-09 92 069822.3
NS-IO 92 069823.1
NS-I I 92 069824.0
NS-29 92 069825.8
NS-30 92 069826.6
NS-15 92 069827.4
NS-31 92 069828.2
NS-32 92 069829.0
EX-02 92 069830.4
EX-02 Matrix 92 069831.2
EX-02 Duplicate 92 069832.0 -·-·~ ----EX-04 .. 92 069833.9
EX-03 92 069834.7
EX-01 92 069835.5
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
National Starch & Chemical I P.O. Box 399
Salisbury, NC 28144
Company December 05, 1996
PACE Project Number: 661015501
Attn: Mr. Ken Kluttz I Client Reference: CLP Quarterly Monitoring
I PACE Sample Number:
Date Collected:
Date Received:
I Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride I Solids, Total Dissolved
I
I
I
•
I
D
D
I
I
I
I
92 0698223
10/14/96
10/15/96
NS-09
Units PRL ____ METHOD DATE ANALYZED
mg/L
mg/L
1
I
1100
4900
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
325.3
2540 C
10/21/96
10/17/96
Pace Analytical
Pace Analytical Services, !nc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 2 December 05, 1996
PACE Project Number: 661015501 I
Client Referenc~: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected: 92 0698231
10/14/96 I
Date Received:
Client Sample ID:
Parameter Units PRL
10115/96 I NS-10
____ METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
mg/L
mg/L
mg/L
25
1
1
210
490
3600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
5220 B 10/16/96 I 325.3 10/21/96
2540 C 10/17/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
I Mr. Ken Kluttz
Page 3
Pace Analytical Services, !nc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP Quarterly Monitoring
I PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
m
n
n
I
I
I
I
I
I
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
92 0698240
10jl4/96
10/15/96
NS-11
Units PRL ____ METHOD DATE ANALYZED
mg/L
mg/L
mg/L
25
1
1
210
4.2
2400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc.
5220 8
325.3
2540 C
10/16/96
10/21/96
10/17/96
Pace Analytical
Mr. Ken Kluttz
Page 4
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
1
1
PRL
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
December 05, 1996
PACE Project Number: 661015501 I
92 0698258 I
10/14/96
10/15/96
NS-29 I METHOD DATE ANALYZED ----
810
5100
325.3
2540 C
I
10/21/96 I 10/17/96
I
I
I
I
I
I
I
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. I
I
I Pace Analytical
I Mr. Ken Kluttz
Page 5
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
· Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP Quarterly Monitoring
I PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
I
I
I
n
D
D
I
m
I
I
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
92 0698266
10/14/96
10/15/96
NS-30
Units PRL ____ METHOD DATE ANALYZED
mg/L
mg/L
1
1
60
1500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
325.3
2540 C
10/23/96
10/17/96
Pace Analytical
Pace Analytical Services. Inc.
9800 Kincey Avenue, Surte 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 6 December 05, 1996
PACE Project Number: 6610155011
Client Reference: CLP Quarterly Monitoring
PACE Sample Number: 92 0698274
10/14/96
10/15/96
NS-15
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Sol ids, Total Dissolved
Units
mg/L
mg/L
I
I
PRL ----
1000
4400
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD
325.3
2540 C
I
DATE ANALYZED I
I
10/23/96 I 10/17/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
I Mr. Ken Kluttz
Page 7
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP Quarterly Monitoring
I PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
I
I
I
D
I
I
m
I
I
I
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
1
1
PRL
92 0698282
10/14/96
10/15/96
NS-31
----
530
4000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD DATE ANALYZED
325.3
2540 C
10/23/96
10/17/96
Pace Analytical
Mr. Ken Kluttz
Page 8
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
1
1
PRL
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
December 05, 1996
PACE Project Number: 661015501 I
92 0698290 I
10/14/96
10/15/96
NS-32 I
METHOD DATE ANALYZED ----
11
1700
325.3
2540 C
I
10/23/96 I 10/17/96
I
I
I
I
I
I
I
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc. ·1
I
I Pace Analytical
I Mr. Ken Kluttz
Page 9
Pace Analytical Services, Inc.
9800 Kincey Av~nue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
I
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
I
m
I
D
D
I
m
I
I
I
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
50
1
1
92 0698304
10/14/96
10/15/96
EX-02
----
840
1100
3800
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD DATE ANALYZED
5220 B
325.3
2540 C
10/16/96
10/23/96
10/17/96
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Surte 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr, Ken Kluttz
Page 10
December 05, 1996
PACE Project Number: 6610155011
Client Reference: CLP Quarterly Monitoring
PACE Sample Number: 92 0698312
10/14/96
10/15/96
EX-02
Matrix
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
50
1
1
840
1000
4300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, 1nc.
I
METHOD DATE ANALYZED I
5220 B
325.3
2540 C
10/16/96
10/23/96
10/17/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
Mr. Ken Kluttz I Page 11
Pace Analytical Services, Inc.
9800 Kincey Avenue, Surre 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP Quarterly Monitoring
I PACE Sample Number: 92 0698320
10/14/96
10/15/96
EX-02
Date Collected:
Date Received: I Client Sample ID:
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
I
I
I
I
! m
I
D
D
I
I
I
I
Units PRL Duplicate METHOD DATE ANALYZED
mg/L
mg/L
mg/L
25
1
1
800
1000
3600
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
5220 B
325.3
2540 C
10/16/96
10/23/96
10/17/96
Pace Analytical
Pace Analytlca1 Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 12 December 05, 1996 I
PACE Project Number: 661015501. _
Client Reference: CLP Quarterly Monitoring
PACE Sample Number: 92 0698339
10/14/96
10/15/96
EX-04
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
50
1
1
----
130
140
3200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD DATE ANALYZED
5220 B 10/16/96
325.3 10/23/96
2540 C 10/17/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
Mr. Ken Kluttz I Page 13
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP
I PACE Samp 1 e Number:
Quarterly Monitoring
Date Co 11 ected:
Date Received: I Client Sample ID:
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
I
I
I
I
I
I
I
I
I
I
Units
mg/L
mg/L
mg/L
PRL
50
1
1
92 0698347
10/14/96
10/15/96
EX-03
----
270
210
2500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD DATE ANALYZED
5220 B
325.3
2540 C
10/16/96
10/23/96
10/17/96
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 14
December 05, 1996
PACE Project Number: 661015501 I
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
25
I
I
These data have been reviewed and are approved for release.
Margaret S. Harding
Manager, Laboratory Operations
92 0698355
10/14/96
10/15/96
EX-01
----
26
93
1500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Ser.iices, Inc.
METHOD
5220 B
325.3
2540 C
DATE ANALYZED
10/16/96
10/23/96
10/17/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
I Mr. Ken Kluttz
Page 15
FOOTNOTES
for pages 1 through 14
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Huntersville. NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996
PACE Project Number: 661015501
Client Reference: CLP Quarterly Monitoring
I
I
I
I
I
, I
I
I
•
I
g
u
n
I
D
I
PRL PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 16
QUALITY CONTROL DATA December 05, 1996
PACE Project Number: 661015501 I
Client Reference: CLP Quarterly Monitoring
Chemical Oxygen Demand
Batch: 92 51515
Samples: 92 0698231, 92 0698240, 92 0698304, 92 0698312, 92 0698320
92 0698339, 92 0698347, 92 0698355
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
Units
mg/L
PRL
25
Method
Blank
ND
920698320
EX-02
Duplicate
800
Duplicate
of
92 0698320
800
920698312
EX-02 Spike
Units
mg/L
mg/L
PRL
50
100
Matrix Spike Recv
Units
mg/L
PRL
25
840
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
2000 108%
Reference
Value Recv
500 107%
I
I
I
RPO I 0%
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996 I Mr. Ken Kluttz
Page 17 PACE Project Number: 661015501
I
Client Reference: CLP Quarterly Monitoring
Chloride
Batch: 92 51603 I Samples: 92 0698223, 92 0698231, 92 0698240, 92 0698258
I METHOD BLANK AND SAMPLE DUPLICATE:
I
Parameter
Chloride
I SPIKE:
Parameter
Chloride
I
LABORATORY CONTROL SAMPLE:
I Parameter
Chloride
Units
mg/L
Units
mg/L
Units
mg/L
PRL -1-
PRL -1-
PRL -1-
Method
Blank
ND
Duplicate
of
920694058 92 0694058
2. 2 2. 2
Spike
920694058 Spike Recv
2. 2 5. 0 98%
Reference
Value Recv
20 100%
I
I
D
D
I
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPD
0%
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 18
QUALITY CONTROL DATA December 05, 1996
PACE Project Number: 661015501 I
Client Reference: CLP Quarterly Monitoring
Chloride
Batch: 92 51728
Samples: 92 0698266, 92 0698274, 92 0698282, 92 0698290, 92 0698304
92 0698312, 92 0698320, 92 0698339, 92 0698347, 92 0698355
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
Chloride
Units
mg/L
PRL -1-
Method
Blank
ND
Duplicate
920698266 of
NS-30 92 0698266 ~6~0---63
920698282 Spike
Recv
94%
Units
mg/L
PRL -]-NS-31 Spike
530 500
Units
mg/L
PRL -1-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Reference
Value Recv
20.0 100%
I
I
I
RPO I
5%'
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 05, 1996 I Mr. Ken Kluttz
Page 19 PACE Project Number: 661015501
I
Client Reference: CLP Quarterly Monitoring
Solids, Total Dissolved
Batch: 92 51639
I Samples: .92 0698223,
92 0698274,
92 0698320,
92 0698231,
92 0698282,
92 0698339,
92 0698240,
92 0698290,
92 0698347,
92 0698258,
92 0698304,
92 0698355
I METHOD BLANK AND SAMPLE DUPLICATE:
I Parameter
Solids, Total Dissolved
I LABORATORY CONTROL SAMPLE:
I Parameter
Solids, Total Dissolved
I
•
I
Units
mg/L
Units
mg/L
PRL -1-
PRL -I-
92 0698266
92 0698312
Method
Blank
1
Duplicate
920698339 of
EX-04 92 0698339
""3 2=o~oc----3 400
Reference
Value Recv
100 107%
D
D
D
u
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPD
6%
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 20
FOOTNOTES
for pages 16 through 19
December 05, 1996
PACE Project Number: 661015501 I
Client Reference: CLP Quarterly Monitoring
ND
PRL
RPO
Not detected at or above the PRL.
PACE Reporting Limit
Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
g
I
I
D
I
I
I
Appendix A
Report of Laboratory Analysis
Trench Area Wells
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
December 04, 1996
Mr. Ken Kluttz
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 28144
RE: PACE Project No. 661008.504
Client Reference: Trench Wells
Dear Mr. Kluttz:
Enclosed is the report of laboratory analyses for samples received
October 08, 1996.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
3 .L-l--c..~ CCJ )--j(CX~e(,•"'
Felicia C Grogan
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Tel: [phone]
Fax: [phone]
I
I
I
I
.--. ----· NATIONAL STARCH I
AND CHEMICAL CO.
DAT A PACKAGE I
I
December 3, 1996
I
I
I
I
-. ----------· ... I
I
SUBMITTED BY I
PACE ANALYTICAL SERVICES INC
9800 KINCEY A VE I SUITE 100
HUNTERSVILLE, NORTH CAROLINA 28078 I [phone]
I
I -·--·-------· ..
I
I
I
I
I
I
I
I
I
I
I
•
I
I
I
I
u
I
I
I
-----·----·
December 3, I 996
Mr. Ken Kluttz
National Starch and Chemical Co.
485 Cedar Springs Road
Salisbury, NC 28144
CASE NARRATIVE
PACE Project No.: 661008.504
Client Reference: Trench Wells
Sample receipt:
A total of six water samples were received at Pace Analytical Laboratory in Huntersville, NC
on I 0/8/96. The samples were logged into the Laboratory Data Management System and
PACE laboratory sample numbers were assigned to the samples. Samples requiring CLP
Volatiles, CLP Semi-Volatiles, CLP Metals, and TKN were then shipped via Federal Express
on l 0/8/96 to Pace Laboratories in Houston for analysis.
Sample ID
EX-05
EX-06
EX-07
EX-08
EX-09
EX-10
PACE -Charlotte ID
92 069360.4
92 069361.2
92 069362.0
92 069363.9
92 069364.7
92 069365.5
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
National Starch & Chemical Company
P.O. Box 399
December 04, 1996
PACE Project Number: 661008504 I Salisbury, NC 28144
Attn: Mr. Ken Kluttz
Client Reference: Trench Wells
PACE Sample Number:
Oate Co 11 ected:
Date Received:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day
Chemical Oxygen Demand
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
2
2000
1
92 0693604
10/07/96
10/08/96
EX-05
----
>6000
24000
33000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc.
I
I
METHOD DATE ANALYZED I
1
5210B 10/09/96 I 5220 B 10/09/96
2540 C 10/14/96
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
I Mr. Ken Kluttz
Page 2
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
PACE Project Number: 661008504
I Client Reference: Trench Wells
PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
•
I
I
0
I
I
I
m
I
I
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand,
Chemical Oxygen Demand
Solids, Total Dissolved
92 0693612
10/07/96
10/08/96
EX-06
Units PRL ____ METHOD DATE ANALYZED
05 Day mg/L
mg/L
mg/L
2
25
1
320
130
210
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
5210B
5220 B
2540 C
10/09/96
10/09/96
10/10/96
Pace Analytical
Mr. Ken Kluttz
Page 3
Client Reference: Trench Wells
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day
Chemical Oxygen Demand
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
2
250
1
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
December 04, 1996 I PACE Project Number: 661008504
92 0693620 I
10/07/96
10/08/96 I EX-07
____ METHOD DATE ANALYZED
1100
2600
8000
52108
5220 B
2540 C
10/09/96
10/09/96
10/10/96
I
I
I
I
I
I
I
I
I
I
I
I
I
REPORT OF LABORATORY ANALYSIS I This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I Pace Analytical.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I Mr. Ken Kluttz
Page 4
December 04, 1996
PACE Project Number: 661008504
Client Reference: Trench Wells
I PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
I
g
I
D
I
I
I
I
I
I
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand,
Chemical Oxygen Demand
Sol ids, Total Dissolved
92 0693639
10/07/96
10/08/96
EX-08
Units PRL ____ METHOD DATE ANALYZED
05 Day mg/L
mg/L
mg/L
2
2000
1
>6500
24000
29000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
5210B
5220 B
2540 C
10/09/96
10/09/96
10/14/96
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. 'Ken Kluttz
Page 5 December 04, 1996 I PACE Project Number: 66100850
Client Reference: Trench Wells
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand, 05 Day Chemical Oxygen Demand
Solids, Total Dissolved
Units
mg/L
mg/L
mg/L
PRL
2
1000
I
92 0693647
10/07/96
10/08/96
EX-09
----
>5800
19000
20000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
METHOD
52108
5220 B
2540 C
I
I DATE ANALYZED
I
10/09/96 I 10/09/96
10/10/96
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I Mr. Ken Kluttz
Page 6
December 04, 1996
PACE Project Number: 661008504
I Client Reference: Trench Wells
PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
INDIVIDUAL PARAMETERS
Biochemical Oxygen Demand,
Chemical Oxygen Demand
Solids, Total Dissolved
05 Day
Units
mg/L
mg/L
mg/L
PRL
2
1000
1
I These data have been reviewed and are approved for release.
1-------.11 c~f::_L . I _\ ,", J'.-0
Margaret S. Harding I Manager, Laboratory Operations
I
I
I
D
I
92 0693655
10/07/96
10/08/96
EX-10
----
2900
11000
15000
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, 1nc.
METHOD DATE ANALYZED
5210B
5220 B
2540 C
10/09/96
10/09/96
10/10/96
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 7 FOOTNOTES
for pages I through 6
December 04, 1996
PACE Project Number: 6610085041
Client Reference: Trench Wells
>
PRL
Greater than reported value.
PACE Reporting Limit
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
QUALITY CONTROL DATA
Pace Analytical Services, Inc
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
I
I
I
Mr. Ken Kluttz
Page 8 PACE Project Number: 661008504
Client Reference: Trench Wells
Biochemical Oxygen Demand, 05 Day
Batch: 92 51365
I Samples: 92 0693604, 92 0693612, 92 0693620, 92 0693639, 92 0693647
92 0693655
I METHOD BLANK AND SAMPLE DUPLICATE:
I Parameter
Biochemical Oxygen Demand, 05 Day
I LABORATORY CONTROL SAMPLE:
Parameter
0 Biochemical Oxygen Demand, 05 Day
Units
mg/L
Units
mg/L
PRL -2-
PRL -2-
Method
Blank
ND
Duplicate
of
920693884 92 0693884
7 7
Reference
Value Recv
200 113%
I
I
I
I
I
I
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPO
0%
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 9
QUALITY CONTROL DATA December 04, 1996
PACE Project Number: 661008504 I
Client Reference: Trench Wells
Chemical Oxygen Demand
Batch: 92 51272
Samples: 92 0693604
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
SPIKE:
Units
mg/L
PRL
25
Method
Blank
ND
Duplicate
of
920689526 92 0689526
57 62
Parameter
Chemical Oxygen Demand
Units
mg/L
PRL
25
920689526 Spike
Spike
Recv
87%
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
57 500
Units
mg/L
PRL
25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Reference
Value Recv
500 98%
RPD
I
I
I
8% I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
QUALITY CONTROL DATA
Pace Analytical Services, \nc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996 I Mr. Ken Kluttz
Page 10 PACE Project Number: 661008504
I Client Reference: Trench Wells
Chemical Oxygen Demand
Batch: 92 51273 I Samples: 92 0693612, 92 0693620, 92 0693639, 92 0693647, 92 0693655
I METHOD BLANK AND SAMPLE DUPLICATE:
Method
Blank
ND
Duplicate
of
920693698 92 0693698
I
I
!I
Parameter
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
I Parameter
I
I
•
I
H
D
I
.1
I
Chemical Oxygen Demand
Units
mg/L
Units
mg/L
Units
mg/L
PRL
25
PRL
25
PRL
25
ND ND
920693612
EX-06 Spike ~13~0~--500
Spike
Recv
79%
Reference
Value Recv
500 99%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPO
NC
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Surre 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr, Ken Kluttz
Page II QUALITY CONTROL DATA December 04, 1996
PACE Project Number: 6610085041
Client Reference: Trench Wells
Solids, Total Dissolved
Batch: 92 51361
Samples: 92 0693612, 92 0693620, 92 0693647, 92 0693655
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Solids, Total Dissolved
LABORATORY CONTROL SAMPLE:
Parameter
Solids, Total Dissolved
Units
mg/L
Units
mg/L
PRL -1-
PRL -1-
Method
Blank
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seivices, Inc.
920693655
EX-10
15000
Reference
Duplicate
of
92 0693655
16000
Value Recv
100 109%
RPO
I
I
I
6%1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996 I Mr. Ken Kluttz
Page 12
QUALITY CONTROL DATA
PACE Project Number: 661008504
Client Reference: Trench Wells
I Solids, Total Dissolved
Batch: 92 51377 I Samples: 92 0693604, 92 0693639
I METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
I Solids, Total Dissolved
LABORATORY CONTROL SAMPLE:
Parameter
Solids, Total Dissolved
Units
mg/L
Units
mg/L
PRL -1-
PRL -1-
Method
Blank
1
Duplicate
of
920694015 92 0694015
160 180
Reference
Value Recv
100 109%
I
I
I
I
m
I
D
D
I
I
I
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RPO
12%
Pace Analytical
Pace Analytical Serv·1ces, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
Mr. Ken Kluttz
Page 13
FOOTNOTES
for pages 8 through 12
December 04, 1996 I PACE Project Number: 661008504
Client Reference: Trench Wells
NC
ND
PRL
RPO
No calculation due to value below detection limit. Not detected at or above the PRL. PACE Reporting Limit
Relative Percent Difference
REPORT OF LABORATORY ANALYSIS
This report sh811 not be reproduced, except in full,
w·11haut the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
n
D
I
•
I
Appendix 8
Volatile Organics Analysis Data Sheets
Plume Periphery Wells
00015
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-01
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
I % Moisture: not dee.
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437852
Lab File ID: YV102413
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0 I GC Column:
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
1
I
I
I
I
I
I
n
D
R
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane ..
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
10 u
10 u
0.6 J
10 u
10 u
10 u
10 u
5 J
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
10 u
3/90
U 1) iJ l J
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-01
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
i Moisture: not dee.
5.000 (g/mL) ML
LOW
GC Column: ID: 0.53 (mm)
Soil Extract Volume: _____ (uL)
CAS NO. COMPOUND
74-87-3---------Chloromethane
Lab Sample ID: H437852
Lab File ID: YV102413
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------107 - l 3 - l - - - - - - - -Ac r y lo nit rile~-------
----------------Xylene (total) ______ _
10 U
50 U
10 U
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
OLJIJ5Q
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-02
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: ( soil/water) WATER
I Sample wt/vol:
I
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
ID: O. 53 (mm)
Lab Sample ID: H437847
Lab File ID: YV102422
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 25.0 I GC Column:
Soil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL
1
I
I
I
I
I
I
D
I
I
I
I
I
----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---·-----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79--34-5-0 - - - - - --1, 1, 2, 2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
250 u
250 u
250 u
18 J
32000 E
250 u
250 u
250 u
140 J
250 u
250 u
250 u
250 u
250 u
100 J
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250
250 u
32 J
250 u
3/90
:') : l i.' 'i l. ---' u \.).
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
Lab Sample ID: H437847
Lab File ID: YV102422
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 25.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------
Q
107 -l 3 -l --------Ac r y lo nit rile _______ _
----------------Xylene (total) ______ _
250 U
1200 U
26 J
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
0002G
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-02DL
I Lab Code: 001
Matrix:
Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
(soil/water) WATER Lab Sample ID: H437847
I Sample wt/vol: 5.000 (g/mL) ML Lab File ID: YV102415
Level: (low/med) LOW
I % Moisture: not dee.
I GC Column:
Soil Extract Volume: (uL)
ID: 0.53 (mm)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 200.0
Soil Aliquot Volume: _____ (uL
1
I
I
I
I
I
I
I
I
I
I
I
I
-----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 2000 u
75-01-4---------Vinyl Chloride 2000 u
75-00-3---------Chloroethane 2000 u
75-09-2---------Methylene Chloride 110 DJ
67-64-1---------Acetone 25000 D
75-15-0---------Carbon Disulfide 2000 u
75-35-4---------1,1-Dichloroethene 2000 u
75-34-3---"-----l,l-Dichloroethane 2000 u
107-06-2--------1,2-Dichloroethane 2000 u
67-66-3---------Chloroform 2000 u
78-93-3---------2-Butanone 2000 u
71-55-6---------1,1,1-Trichloroethane 2000 u
56-23-5---------Carbon Tetrachloride 2000 u
75-27-4---------Bromodichloromethane 2000 u
78-87-5---------1,2-Dichloropropane 2000 u
10061-01-5------cis-l,3-Dichloropropene 2000 u
79-01-6---------Trichloroethene 2000 u
71-43-2---------Benzene 2000 u
10061-02-6------trans-l,3-Dichloropropene 2000 u
79-00-5---------1,1,2-Trichloroethane --2000 u
124-48-1--------Chlorodibromomethane 2000 u
75-25-2---------Bromoform 2000 u
108-10-1--------4-Methyl-2-pentanone 2000 u
79-34-5---------1,1,2,2-Tetrachloroethane --2000 u
127-18-4--------Tetrachloroethene 2000 u
591-78-6--------2-Hexanone 2000 u
108-88-3--------Toluene 550 DJ
108-90-7--------Chlorobenzene 2000 u
100-41-4--------Ethylbenzene 2000 u
100-42-5------~-Styrene 2000 u
FORM I VOA 3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: O. 53 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437847
Lab File ID: YV102415
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 200.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
2000
10000
2000
-----
Q
u
u
u
FORM I VOA 3/90
I
I
I
I
I
(uLI
1
I
I
I
I
I
I
I
I
I
I
I
I
00038
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-02DUP
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437849
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: YV102416
(low/med) Level: I % Moisture: not dee.
I GC Column: ID: 0. 53 (mm)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 200.0
Soil Aliquot Volume:
I
I
D
I
I
I
I
I
I
I
I
I
m
Soil Extract Volume: (uL) --------
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 2000 u
75-01-4---------Vinyl Chloride 2000 u
75-00-3---------Chloroethane 2000 u
75-09-2---------Methylene Chloride 130 J
67-64-1---------Acetone 25000
75-15-0---------Carbon Disulfide 2000 u
75-35-4---------1,1-Dichloroethene 2000 u
75-34-3---"-----l,l-Dichloroethane 2000 u
107-06-2--------1,2-Dichloroethane 2000 u
67-66-3---------Chloroform 2000 u
78-93-3---------2-Butanone 2000 u
71-55-6---------1,1,1-Trichloroethane 2000 u
56-23-5---------Carbon Tetrachloride 2000 u
75-27-4---------Bromodichloromethane 2000 u
78-87-5---------1,2-Dichloropropane 2000 u
10061-01-5------cis-1,3-Dichloropropene 2000 u
79-01-6---------Trichloroethene 2000 u
71-43-2---------Benzene 2000 u
10061-02-6------trans-1·, 3-Dichloropropene 2000 u
79-0~-5---------1,1,2-Trichloroethane --2000 u
124-48-1--------Chlorodibromomethane 2000 u
75-25-2---------Bromoform 2000 u
108-10-1--------4-Methyl-2-pentanone 2000 u
79-34-5---------1,1,2,2-Tetrachloroethane 2000 u --127-18-4--------Tetrachloroethene 2000 u
591-78-6--------2-Hexanone 2000 u
108-88-3--------Toluene 310 J
108-90-7--------Chlorobenzene 2000 u
100-41-4--------Ethylbenzene 2000 u
100-42-5--------Styrene 2000 u
FORM I VOA 3/90
(uL
l}l) 0 3 '..!
lA EPA SAMPLE NO.
VOLAT~LE ORGANICS ANALYSIS DATA SHEET
EX-02DUP
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene ( total)
Lab Sample ID: H437849
Lab File ID: YV102416
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 200.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
2000
10000
2000
Q
u
u
u
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
r,_ ,.._ .....
I OOOG8
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-03
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
I
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm) I GC Column:
Soil Extract Volume: (uL)
Lab Sample ID: H437851
Lab File ID: YV102412
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 25.0
Soil Aliquot Volume: ---------
1
I
D
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 250 u
75-01-4---------Vinyl Chloride 250 u
75-00-3---------Chloroethane 250 u
75-09-2---------Methylene Chloride 16 J
67-64-1---------Acetone 10000 E
75-15-0---------Carbon Disulfide 250 u
75-35-4---------1,1-Dichloroethene 250 u
75-34-3---------1,1-Dichloroethane 250 u
107-06-2-- - - - - --1, 2-Dich:j.or.oethane 60 J
67-66-3---------Chloroform 250 u
78-93-3---------2-Butanone 250 u
71-55-6---------1,1,1-Trichloroethane 250 u
56-23-5---------Carbon Tetrachloride 250 u
75-27-4---------Bromodichloromethane 250 u
78-87-5---------1,2-Dichloropropane 71 J
10061-01-5------cis-l,3-Dichloropropene 250 u
79-01-6---------Trichloroethene 250 u
71-43-2---------Benzene 250 u
10061-02-6------trans-l,3-Dichloropropene 250 u
79-00-5---------1,1,2-Trichloroethane --250 u
124-48-1--------Chlorodibromomethane 250 u
75-25-2---------Bromoform 250 u
108-10-1--------4-Methyl-2-pentanone 250 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 250 u
127-18-4--------Tetrachloroethene 250 u
591-78-6--------2-Hexanone 250 u
108-88-3--------Toluene 120 J
108-90-7--------Chlorobenzene 250 u
100-41-4--------Ethylbenzene 250 u
100-42-5--------Styrene 250 u
FORM I VOA 3/90
(uL
0 '1 C -·· • ' . '' l1 V ,_,
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Lab Sample ID: H437851
Lab File ID: YV102412
Date Received: 10/16/96
Date Analyzed: 10/24/96
I
I
I
I
I
GC Column: ID: 0.53 (mm)
Soil Extract Volume: (uL) Soil Aliquot Volume:
Dilution Factor: 25.0 __ (ul -----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 250 u
107-13-1--------Acrylonitrile 1200 u
----------------Xylene ( total) 250 u
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-03DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437851
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: YV102417
(low/med) Level: I % Moisture: not dee.
I GC Column: ID: O. 53 (mm)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 100.0
____ (uL
I
I
I
R
I
I
I
I
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: -----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 1000 u
75-01-4---------Vinyl Chloride 1000 u
75-00-3---------Chloroethane 1000 u
75-09-2---------Methylene Chloride 69 DJ
67-64-1---------Acetone 7200 D
75-15-0---------Carbon Disulfide 1000 u
75-35-4---------1,1-Dichloroethene 1000 u
75-34-3---•-----l,l-Dichloroethane 1000 u
107-06-2--------1,2-Dichloroethane .1000 u
67-66-3---------Chloroform 1000 u
78-93-3---------2-Butanone 1000 u
71-55-6---------1,1,1-Trichloroethane 1000 u
56-23-5---------Carbon Tetrachloride 1000 u
75-27-4---------Bromodichloromethane 1000 u
78-87-5---------1,2-Dichloropropane 1000 u
10061-01-5------cis-l,3-Dichloropropene 1000 u
79-01-6---------Trichloroethene 1000 u
71-43-2---------Benzene 1000 u
10061-02-6------trans-l,3-Dichloropropene 1000 u
79-00-5---------1,1,2-Trichloroethane --1000 u
124-48-1--------Chlorodibromomethane 1000 u
75-25-2---------Bromoform 1000 u
108-10-1--------4-Methyl-2-pentanone 1000 u
79-34-5---------1,1,2,2-Tetrachloroethane 1000 u --127-18-4--------Tetrachloroethene 1000 u
591-78-6--------2-Hexanone 1000 u
108-88-3--------Toluene 150 DJ
108-90-7--------Chlorobenzene 1000 u
100-41-4--------Ethylbenzene 1000 u
100-42-5--------Styrene 1000 u
FORM I VOA 3/90
OOOS4
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 . Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Lab Sample ID: H437851
Lab File ID: YV102417
Date Received: 10/16/96
Date Analyzed: 10/24/96
I
I
I
I
I
GC Column: ID: 0.53 (mm)
Soil Extract Volume: ____ (uL) Soil Aliquot Volume:
Dilution Factor: 100.0 __ (uJ
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane --------107 -13 - l - - - - - - - -Ac r y lo nit rile~-------
----------------Xylene (total) ______ _
FORM I VOA
1000 U
5000 U
1000 U
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
0 0':1° J 1 I, ,J
EPA SAMPLE .NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-04
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
(low/med) Level:
I % Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437850
Lab File ID: YV102504
Date Received: 10/16/96
Date Analyzed: 10/25/96
Dilution Factor: 1.0 I
I
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
I
I
D
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---·-----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
10 u
10 u
1 J
380 E
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
0.6 J
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
26
2 J
2 J
10 u
3/90
001 0 '.3
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437850
Lab File ID: YV102504
Date Received: 10/16/96
Date Analyzed: 10/25/96
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
10
50
5
Q
u
u
J
I
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90 I
I
I
I
I
I
I
I
I
I
n
I
I
I
I
I
I
I
I
I
I
OCG'.)2
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Lab Sample ID: H437850
Lab File ID: YV102418
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 5.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---~-----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1;3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
50 u
50 u
50 u
4 DJ
460 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
31 DJ
3 DJ
50 u
50 u
3/90
(UL
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: _____ (uL)
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437850
Lab File ID: YV102418
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 5.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
50 u
250 u
3 DJ
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-09
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437839
I Sample wt/vol: Lab File ID: YV101728
1 Level:
% Moisture: not dee.
(low/med)
5.000 (g/mL) ML
LOW Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 10.0 I
I
I
I
I
I
I
I
I
I
I
I
n
GC Column: ID: 0. 53 (mm)
Soil Extract Volume: _____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3----~----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
100
110
55
7
200
100
15
100
5800
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
200
100
8
100
____ (uL
Q
u
J
J
u
J
u
E
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
J
u
3/90
UClJi
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-09
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Lab Sample ID: H437839
Lab File ID: YV101728
Date Received: 10/16/96
Date Analyzed: 10/18/96
I
I
I
I
I
GC Column: ID: 0.53 (mm)
Soil Extract Volume: (uL)
Dilution Factor: 10.0 _(uJ Soil Aliquot Volume: -----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane --------107 -l 3 -l --------Ac r y lo nit rile~-------
----------------Xylene (total) _______ _
FORM I VOA
100 U
500 U
21 J
Q
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-09DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
(low/med) Level:
I % Moisture: not dee.
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437839
Lab File ID: YV102407
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 50.0 I GC Column:
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (UL
m
I
R
I
I
I
I
I
I
I
I
I
g
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 500 u
75-01-4---------Vinyl Chloride 500 u
75-00-3---------Chloroethane 500 u
75-09-2---------Methylene Chloride 500 u
67-64-1---------Acetone 500 u
75-15-0---------Carbon Disulfide 500 u
75-35-4---------1,1-Dichloroethene 500 u
75-34-3---0 -----l,l-Dichloroethane 500 u
107 0 06-2--------1,2-Dichloroethane 7100 D
67-66-3---------Chloroform 500 u
78-93-3---------2-Butanone 500 u
71-55-6---------1,1,1-Trichloroethane 500 u
56-23-5---------Carbon Tetrachloride 500 u
75-27-4---------Bromodichloromethane 500 u
78-87-5---------1,2-Dichloropropane 500 u
10061-01-5------cis-1,3-Dichloropropene 500 u
79-01-6---------Trichloroethene 500 u
71-43-2---------Benzene 500 u
10061-02-6------trans-1,3-Dichloropropene 500 u --79-00-5---------1,1,2-Trichloroethane 500 u
124-48-1--------Chlorodibromomethane 500 u
75-25-2---------Bromoform 500 u
108-10-1--------4-Methyl-2-pentanone 500 u
79-34-5---------1,1,2,2-Tetrachloroethane 500 u --127-18-4--------Tetrachloroethene 500 u
591-78-6--------2-Hexanone 500 u
108-88-3--------Toluene 240 DJ
108-90-7--------Chlorobenzene 500 u
100-41-4--------Ethylbenzene 500 u
100-42-5--------Styrene 500 u
FORM I VOA 3/90
lA
C :: I .:i G
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-09DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: _____ (uL)
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437839
Lab File ID: YV102407
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 50.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
500
2500
500
Q
u
u
u
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
0"1•~f' \) \,' U ,_j
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
NS-l0DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
I
I
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5. 000 (g/mL) ML
LOW
I GC Column:
Soil Extract Volume: (uL)
ID: 0. 53 (mm)
Lab Sample ID: H437840
Lab File ID: YV102405
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 25.0
Soil Aliquot Volume: ----
1
I
I
D
I
I
I
I
I
I
I
I
I
-----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 250 u
75-01-4---------Vinyl Chloride 250 u
75-00-3---------Chloroethane 250 u
75-09-2---~-----Methylene Chloride 15 DJ
67-64-1---------Acetone 250 u
75-15-0---------Carbon Disulfide 250 u
75-35-4---------1,1-Dichloroethene 250 u
75-34-3---0 -----1,l-Dichloroethane 250 u
107-06-2--------1,2-Dichloroethane 4500 D
67-66-3---------Chloroform 250 u
78-93-3---------2-Butanone 250 u
71-55-6---------1,1,1-Trichloroethane 250 u
56-23-5---------Carbon Tetrachloride 250 u
75-27-4---------Bromodichloromethane 250 u
78-87-5---------1,2-Dichloropropane 250 u
10061-01-5------cis-1,3-Dichloropropene 250 u
79-01-6---------Trichloroethene 250 u
71-43-2---------Benzene 250 u
10061-02-6------trans-1,3-Dichloropropene 250 u
79-00-5---------1,1,2-Trichloroethane --250 u
124-48-1--------Chlorodibromomethane 250 u
75-25-2---------Bromoform 250 u
108-10-1--------4-Methyl-2-pentanone 250 u
79-34-5---------1,1,2,2-Tetrachloroethane --250 u
127-18-4--------Tetrachloroethene 250 u
591-78-6--------2-Hexanone 250 u
108-88-3--------Toluene 19 DJ
108-90-7--------Chlorobenzene 250 u
100-41-4--------Ethylbenzene 250 u
100-42-5--------Styrene 250 u
FORM I VOA 3/90
(uL
n .~. l .-··
-..: " i. .J !
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-l0DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Lab Sample ID: H437840
Lab File ID: YV102405
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 25.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane _______ _ 250 U
1200 U
250 U
107-13-1--------Acrylonitrile~-------
----------------Xylene (total) _______ _
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
(' , ... 1 -~-·
-.. '} :. ' 'J
EPA SAMPLE NO.
I Lab Name: PAST, HOUSTON Contract: 001
NS-10
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
I Level: (low/med)
% Moisture: not dee.
I GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437840
Lab File ID: YV102419
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 10.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: -----
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 100 u
75-01-4---------Vinyl Chloride 100 u
75-00-3---------Chloroethane 100 u
75-09-2---------Methylene Chloride 7 J
67-64-1---------Acetone 100 u
75~15-0-------~-Carbon Disulfide 100 u
75-35-4---------1,1-Dichloroethene 100 u
75-34-3---~-----l,l-Dichloroethane 100 u
107-06-2--------1,2-Dichloroethane 4800 E
67-66-3---------Chloroform 100 u
78-93-3---------2-Butanone 100 u
71-55-6---------1,1,1-Trichloroethane 100 u
56-23-5---------Carbon Tetrachloride 100 u
75-27-4---------Bromodichloromethane 100 u
78-87-5---------1,2-Dichloropropane 100 u
10061-01-5------cis-l,3-Dichloropropene 100 u
79-01-6---------Trichloroethene 100 u
71-43-2---------Benzene 100 u
10061-02-6------trans-l,3-Dichloropropene 100 u
79-00-5---------1,1,2-Trichloroethane --100 u
124-48-1--------Chlorodibromomethane 100 u
75-25-2---------Bromoform 100 u
108-10-1--------4-Methyl-2-pentanone 100 u
79-34-5---------1,1,2,2-Tetrachloroethane --100 u
127-18-4--------Tetrachloroethene 100 u
591-78-6--------2-Hexanone 100 u
108-88-3--------Toluene 9 J
108-90-7--------Chlorobenzene 100 u
100-41-4--------Ethylbenzene 100 u
100-42-5--------Styrene 100 u
FORM I VOA 3/90
(uL
(• :: J ; (" ., ·' • ' lJ
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-10
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
~ Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: O. 53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
Lab Sample ID: H437840
Lab File ID: YV102419
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 10.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane _______ _ 100 U
500 U
100 U
107-13-1--------Acrylonitrile-,-______ _
----------------Xylene (total) _______ _
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-11
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med) I% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437841
Lab File ID: YV101730
Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 1.0 I Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
I
.I
I
a
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4-----~---l,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5-----"cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
34
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
19
10 u
92
1 J
3/90
lA
,.... rl ! t' .-\.J' ', __ ,1. ,) ,)
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-11
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437841
Lab File ID: YV101730
Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
10
50
140
u
u
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
NS-15
I Lab Code: 001
Matrix: (soil/water) WATER
-Case No. : CHARLOTTE SAS No. : 004 SDG No. : PKG12
Lab Sample ID: H437844
I Sample wt/vol: 5.000 (g/mL) ML Lab File ID: YV102406
Level: (low/med) LOW
I % Moi•sture: not dee.
I GC Column:
Soil Extract Volume: _____ (uL)
ID: 0. 53 (mm)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0
Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
·I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
----
Q
10 u
10 u
10 u
1 J
10 u
10 u
. 10 u
10 u
150
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
5 J
6 J
10 u
10 u
10 u
3/90
(uL
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-15
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL) ----
c;AS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437844
Lab File ID: YV102406
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
10
50
1
Q
u
u
J
I
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90 1
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
NS-29
I Lab Code: 001
Matrix:
Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
(soil/water) WATER
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab Sample ID: H437842
Lab File ID: YV101731
Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 50.0
Level: ( low/med)
I % Moisture: not dee.
1 GC Column:
Soil Extract Volume: ____ (uL)
ID: 0.53 (mm)
Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS: I CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---"-----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
500 u
500 u
500 u
37 J
48000 E
500 u
500 u
500 u
1200
500 u
500 u
500 u
500 u
500 u
1800
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
440 J
500 u
500 u
500 u
3/90
;,r,,,01 ~----t
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: ( soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
74c87-3---------Chloromethane
107 - l 3 - l - - - - - - - -Ac r y lo nit rile
Lab Sample ID: H437842
Lab File ID: YV101731
Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 50.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------
Q
--------- - - - - - - - - - - - - - - -Xylene (total) _______ _
500 U
2500 U
56 J
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS
TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
I Lab Name: PASI, HOUSTON Contract: 001
NS-29
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
I Level: (low/med)
% Moisture: not dee.
5. 000 (g/mL) ML
LOW
ID: O. 53 (mm)
Lab Sample ID: H437842
Lab File ID: YVlOl 731
Date Received: 10/16/96
Date Analyzed: 10/18/96
Dilution Factor: 50.0 I GC Column:
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
I
I
a
I
I
I
I
I
I
I
I
I
D
Number TICs found: 4
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
CAS NUMBER COMPOUND NAME RT EST. CONC.
================ ============================ =====;:;::::.:::= =======:::::=====
1. 115-11-7 1-PROPENE, 2-METHYL-7.33 4400
2. UNKNOWN 9.69 1400
3 . 75-18-3 DIMETHYL SULFIDE 10.57 3100
4. 557-40-4 1-PROPENE, 3, 3' -OXYBIS-16.17 690
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
FORM-I VOA-TIC
Q
=====
NJ
J
NJ
NJ
3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water} WATER
Sample wt/vol:
Level: (low/med}
% Moisture: not dee.
GC Column:
5.000 (g/mL} ML
LOW
ID: 0. 53 (mm}
Lab Sample ID: H437842
Lab File ID: YV102408
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 500.0
Soil Extract Volume: _____ (uL} Soil Aliquot Volume: -----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
5000 u
5000 u
5000 u
320 DJ
50000 D
5000 u
5000 u
5000 u
1200 DJ
5000 u
5000 u
5000 u
5000 u
5000 u
1700 DJ
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
5000 u
690 DJ
5000 u
5000 u
5000 u
3/90
I
I
I
I
I
(u'
1
I
I
I
I
I
I
I
I
I
I
I
I
lA
CC'.~ :1 J
EPA SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-29DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No.: PKG12
Matrix: (soil/water) WATER
I Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
I % Moisture: not dee.
I GC Column:
Soil Extract Volume: (uL)
ID: O. 53 (mm)
-----
1 CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437842
Lab File ID: YV102408
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 500.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
5000 u
25000 u
5000 u
I
I
I
I
I
I
I
I
I
I
B
I
FORM I VOA 3/90
(uL
lA
0 1:.:<:.: J l
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-30
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437843
Lab File ID: YV101727
Date Received: 10/16/96
Date Analyzed: 10/17/96
Soil Extract Volume: _____ (uL)
Dilution Factor: 1.0
Soil Aliquot Volume: ----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
79-00-5---------1,1,2-Trichloroethane
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane __
127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
10 u
10 u
0.6 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
(uJ
1
I
I
I
I
I
I
I
I
I
I
I
I
. " · .. -· -
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
NS-30
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437843
I Sample wt/vol: 5.000 (g/mL) ML
LOW
Lab File ID: YV101727
I
I
I
I
I
I
I
I
I
I
I
I
d
I
I
Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0_53· (mm)
Date Received: 10/16/96
Date Analyzed: 10/17/96
Dilution Factor: 1.0
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane --------107 -l 3 -l --------Ac r y lo nit rile~-------
----------------Xylene (total) _______ _
FORM I VOA
10 U
50 U
10 U
Q
3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437845
Sample wt/vol: Lab File ID: YV102409
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Soil Extract Volume: (uL)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 100.0
Soil Aliquot Volume: ----
CAS NO. COMPOUND
74-83-9---------Bromomethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
---------75 -01 -4 ---------Vinyl Chloride _______ _
75-00-3---------Chloroethane ~~~------75 -0 _ 9 -2 ---------Methylene Chloride _____ _
67-64-1---------Acetone ___________ _
75-15-0---------Carbon Disulfide ______ _
75-35-4---------1,1-Dichloroethene _____ _
75-34-3---0 -----l,l-Dichloroethane _____ _
107-06-2--------1,2-Dichloroethane _____ _
67-66-3---------Chloroform ----------78 -93 -3 ---------2 -But anon e ___ ~------
71-55-6---------1,1,1-Trichloroethane ___ _
56-23-5---------Carbon Tetrachloride -----75-27-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane ____ _
10061-01-5------cis-l,3-Dichloropropene __ _
79-01-6---------Trichloroethene ______ _
71-43-2---------Benzene--~~,c--------
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane ___ -~_-_
124-48-1--------Chlorodibromomethane ____ _
75-25-2---------Bromoform -----------108 -10 -l --------4 -Methyl -2 -pent anon e ~----
79-34-5---------1,1,2,2-Tetrachloroethane
127-18-4--------Tetrachloroethene _____ -_-~_
591-78-6--------2-Hexanone _________ _
108-88-3--------Toluene ___________ _
108-90-7--------Chlorobenzene ________ _
100-41-4--------Ethylbenzene ________ _
100-42-5--------Styrene ___________ _
FORM I VOA
Q
1000 u
1000 u
1000 u
110 J
54000 E
1000 u
1000 u
1000 u
170 J
1000 u
1000 u
1000 u
1000 u
1000 u
160 J
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
370 J
1000 u
1000 u
1000 u
3/90
I
I
I
I
I
(uJ
I
I
I
I
I
I
I
I
I
I
I
I
I
lA EPA SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON
NS-31
Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol: 5.000 (g/mL) ML
LOW (low/med) Level: I % Moisture: not dee. o GC Column: ID: 0. 53 (mm)
Soil Extract Volume: (uL) -----
I CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437845
Lab File ID: YV102409
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 100.0
Soil.Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
1000 u
5000 u
1000 u
I
I
I
I
I
I
I
I
I
I
I
I
FORM IVOA 3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437845
Lab File ID: YV102414
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 250.0
Soil Aliquot Volume: ----------
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---•-----l,l-Dichloroethane
107-06-2-7 ------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane __
127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
2500 u
2500 u
2500 u
150 DJ
41000 D
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
530 DJ
2500 u
2500 u
2500 u
3/90
I
I
I
I
I
(uJ
1
I
I
I
I
I
I
I
I
I
I
I
I
lA
'-1 •. ) ::: • j
EPA SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-31DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol: 5.000 (g/mL) ML
LOW I
I
I
Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0. 53 (mm)
Soil Extract Volume: (uL) -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437845
Lab File ID: YV102414
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 250.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
2500
12000
2500
____ (UL
Q
u
u
u
I
I
I
I
I
I
I
I
I
I
B
I
FORM I VOA 3/90
II 'l ·) :~ .._
,) ' • ·-·-· . j
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-32
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437846
Sample wt/vol: Lab File ID: YV102404
Level: (low/med)
% Moisture: not dee.
GC Column:
5. 000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Soil Extract Volume: (uL)
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0
Soil Aliquot Volume: -----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4-------~-l,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane __
127-18-4--------Tetrachloroethene
591-78-6-~------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
10 u
10 u
0.7 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
0.8 J
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-32
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER
I Sample wt/vol:
(low/med) I Level:
% Moisture: not dee.
I GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437846
Lab File ID: YV102404
Date Received: 10/16/96
Date Analyzed: 10/24/96
Dilution Factor: 1.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
•
I
-----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane --------107 -13 -l - - - - - - - -Ac r y lo nit rile.---______ _
----------------Xylene (total) ______ _
FORM I VOA
10 U
50 U
10 U
Q
3/90
(uL
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Appendix B
Volatile Organics Analysis Data Sheets
Trench Area Wells
I lA
ttnonn·-: J
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-05
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
I Sample wt/vol:
Level: (low/med)
I % Moisture: not dee.
5. 000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437572
Lab File ID: YV101719
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 200.0 I GC Column:
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
1
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 2000 u
75-01-4---------Vinyl Chloride 2000 u
75-00-3---------Chloroethane 2000 u
75-09-2---------Methylene Chloride 130 J
67-64-1---------Acetone 28000
75-15-0---------Carbon Disulfide 2000 u
75-35-4---------1,1-Dichloroethene 2000 u
75-34-3---0 -----1,1-Dichloroethane 2000 u
107-06-2--------1,2-Dichloroethane 300000 E
67-66-3---------Chloroform 2000 u
78-93-3---------2-Butanone 2000 u
71-55-6---------1,1,1-Trichloroethane 2000 u
56-23-5---------Carbon Tetrachloride 2000 u
75-27-4---------Bromodichloromethane 20.00 u
78-87-5---------1,2-Dichloropropane 250 J
10061-01-5------cis-1,3-Dichloropropene 2000 u
79-01-6---------Trichloroethene 2000 u
71-43-2---------Benzene 2000 u
10061-02-6------trans-1,3-Dichloropropene 390 J
79-00-5---------1,1,2-Trichloroethane --2000 u
124-48-1--------Chlorodibromomethane 2000 u
75-25-2---------Bromoform 2000 u
108-10-1--------4-Methyl-2-pentanone 3200
79-34-5---------1,1,2,2-Tetrachloroethane 2000 u --127-18-4--------Tetrachloroethene 2000 u
591-78-6--------2-Hexanone 2000 u
108-88-3--------Toluene 20000
108-90-7--------Chlorobenzene 2000 u
100-41-4--------Ethylbenzene 120 J
100-42-5--------Styrene 2000 u
FORM I VOA 3/90
lA
(l(lf\(11-lC,
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-05
Lab Name: PASI, HOUSTON Contract: O O 1
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437572
Lab File ID: YV101719
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 200.0
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: I ____ (uL ----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane --------107 -13 -l --------Ac r y lo nit rile-,--______ _
----------------Xylene (total) _______ _
FORM I VOA
2000 U
7100 J
250 J
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-05DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
I Sample wt/vol:
(low/med) I Level:
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437572
Lab File ID: YV101713
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 5000.0 I
I
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
50000
50000
50000
50000
50000
50000
50000
50000
107-06-2--------1,2-Dichloroethane 430000
67-66-3---------Chloroform 50000
78-93-3---------2-Butanone 50000
71-55-6---------1,1,1-Trichloroethane 50000
56-23-5---------Carbon Tetrachloride 50000
75-27-4---------Bromodichloromethane 50000
78-87-5---------1,2-Dichloropropane 50000
10061-01-5------cis-l,3-Dichloropropene 50000
79-01-6---------Trichloroethene 50000
71-43-2---------Benzene 50000
10061-02-6------trans-l,3-Dichloropropene 50000
79-00-5---------1,1,2-Trichloroethane --50000
124-48-1--------Chlorodibromomethane 50000
75-25-2---------Bromoform 50000
108-10-1--------4-Methyl-2-pentanone 50000
79-34-5---------1,1,2,2-Tetrachloroethane --50000
127-18-4--------Tetrachloroethene 50000
591-78-6--------2-Hexanone 50000
108-88-3--------Toluene 21000
108-90-7--------Chlorobenzene 50000
100-41-4--------Ethylbenzene 50000
100-42-5--------Styrene 50000
FORM I VOA
Q
u
u
u
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
DJ
u
u
u
3/90
lA
( '{:fl( i( :t ·8
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-05DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: ( low/med)
% Moisture: not dee.
5. 000 (g/mL) ML
LOW
Lab Sample ID: H437572
Lab File ID: YV101713
Date Received: 10/09/96
Date Analyzed: 10/17/96
I
I
I
I
I
GC Column: ID: O. 53 (mm) Dilution Factor: 5000.0 I
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Soil Aliquot Volume: ____ (u~
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
50000
250000
50000
Q I
u
u
u
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
{'llfl(lll.1'7
EPA SAMPLE NO.
I Lab Name: PASI, HOUSTON Contract: 001
EX-06
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
I Sample wt/vol:
I Level: (low/med)
% Moisture: not dee.
I GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437573
Lab File ID: YV101720
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1.0
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ____ (uL
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10 u
4 J
10 u
2 J
390 E
10 u
10 u
10 u
220 E
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
10 u
87
10 u
10 u
10 u
65
10 u
10 u
10 u
3/90
lA
l'(llllif'.1/S
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
%-Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437573
Lab File ID:. YV101720
Date Received: 10/09/96
Date Analyzed: 10/17/96
I
I
I
I
I
I Soil Extract Volume: (uL)
Dilution Factor: 1.0
Soil Aliquot Volume: ____ (UL -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
FORM I VOA
10 u
50 u
0.6 J
Q
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-06DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
I Sample wt/vol:
I Level: (low/med)
% Moisture: not dee.
I GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437573
Lab File ID: YV101714
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 10.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
-----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 100 u
75-01-4---------Vinyl Chloride 100 u
75-00-3---------Chloroethane 100 u
75-09-2---------Methylene Chloride 6 DJ
67-64-1---------Acetone 300 D
75-15-0---------Carbon Disulfide 100 u
75-35-4---------1,1-Dichloroethene 100 u
75-34-3---0 -----1,l-Dichloroethane 100 u
107-06-2--------1,2-Dichloroethane 240 D
67-66-3---------Chloroform 100 u
78-93-3---------2-Butanone 100 u
71-55-6---------1,1,1-Trichloroethane 100 u
56-23-5---------Carbon Tetrachloride 100 u
75-27-4---------Bromodichloromethane 100 u
78-87-5---------1,2-Dichloropropane 100 u
10061-01-5------cis-l,3-Dichloropropene 100 u
79-01-6---------Trichloroethene 100 u
71-43-2---------Benzene 100 u
10061-02-6------trans-l,3-Dichloropropene 100 u
79-00-5---------1,1,2-Trichloroethane --100 u
124-48-1--------Chlorodibromomethane 100 u
75-25-2---------Bromoform 100 u
108-10-1--------4-Methyl-2-pentanone 79 DJ
79-34-5---------1,1,2,2-Tetrachloroethane 100 u --127-18-4--------Tetrachloroethene 100 u
591-78-6--------2-Hexanone 100 u
108-88-3--------Toluene 71 DJ
108-90-7--------Chlorobenzene 100 u
100-41-4--------Ethylbenzene 100 u
100-42-5--------Styrene 100 u
FORM I VOA 3/90
(uL
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437573
Lab File ID: YV101714
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 10.0
I
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
FORM I VOA
100 u
500 u
100 u
Q
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07
Lab Name: PASI, HOUSTON .Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437574
Lab File ID: YV101721
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 25.0
Soil Aliquot Volume: ---------
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chlor.ide
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
250 u
250 u
250 u
16 J
5200 E
250 u
250 u
250 u
34000 E
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
250 u
32 J
14 J
250 u
250 u
2400
250 u
250 u
250 u
1700
250 u
250 u
250 u
3/90
(uL
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wi:/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: O. 53 (mm)
Lab Sample ID: H437574
Lab File ID: YV101721
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 25.0
I
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: ____ (UL -----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 250 u
107-13-1--------Acrylonitrile 2800
----------------Xylene (total) 18 J
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I
Lab Name: PASI, HOUSTON Contract: 001
EX-07DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437574
I Sample wt/vol: 5. 000 (g/mL) ML
·LOW
Lab File ID: YV101715
I Level:
% Moisture: not dee.
( low/med)
I GC Column: ID: O. 53 (mm)
Soil Extract Volume: (uL)
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
Soil Aliquot Volume: ----
I
I
I
I
I
I
I
I
I
I
I
I
I
-----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---~-----2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane __
127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7-a------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10000 u
10000 u
10000 u
550 DJ
10000 u
10000 u
10000 u
10000 u
50000 D
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
1700 DJ
10000 u
10000 u
10000 u
3/90
(uL
lA
flflllllll',0
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07DL -Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437574
Lab File ID: YV101715
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
Soil Aliquot Volume: ---------
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane --------107 -13 - l - - - - - - - -Ac r y lo nit rile c-------------------------Xylene (total) _______ _
FORM I VOA
10000 U
50000 U
10000 U
Q
3/90
I
I
I
I
I
I (uL
1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
(I flf )/11 "8
EPA SAMPLE NO.
EX-08
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I Matrix: (soil/water) WATER
Sample wt/vol:
Lab Sample ID: H437575
Lab File ID: YV101724
I Level: (low/med)
5.000 (g/mL) ML
LOW Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 500.0 I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: (uL) Soil Aliquot Volume: -----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2--------"Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
5000
5000
5000
300
72000
5000
5000
5000
107-06-2--------1,2-Dichloroethane 280000
67-66-3---------Chloroform 5000
78-93-3---------2-Butanone 5000
71-55-6---------1,1,1-Trichloroethane 5000
56-23-5---------Carbon Tetrachloride 5000
75-27-4---------Bromodichloromethane 5000
78-87-5---------1,2-Dichloropropane 5000
10061-01-5------cis-l,3-Dichloropropene 5000
79-01-6---------Trichloroethene 5000
71-43-2---------Benzene 5000
10061-02-6------trans-l,3-Dichloropropene 5000
79-00-5---------1,1,2-Trichloroethane --5000
124-48-1--------Chlorodibromomethane 5000
75-25-2---------Bromoform 5000
108-10-1--------4-Methyl-2-pentanone 33000
79-34-5---------1,1,2,2-Tetrachloroethane 5000 --127-18-4--------Tetrachloroethene 5000
591-78-6--------2-Hexanone 5000
108-88-3--------Toluene 25000
108-90-7--------Chlorobenzene 5000
100-41-4--------Ethylbenzene 5000
100-42-5--------Styrene 5000
FORM I VOA
____ (UL
Q
u
u
u
J
u
u
u
E
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-08
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water} WATER
Sample wt/vol:
Level: (low/med}
% Moisture: not dee.
GC Column:
5.000 (g/mL} ML
LOW
ID: 0.53 (mm}
Soil Extract Volume: (uL} -----
CAS NO. COMPOUND
74-87-3---------Chloromethane
107-13-1--------Acrylonitrile
----------------Xylene (total}
Lab Sample ID: H437575
Lab File ID: YV101724
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 500.0
Soil Aliquot Volume:
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
5000
15000
5000
-----
Q
u
J
u
FORM I VOA 3/90
I
I
I
I
I
I
(uL
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-0SDL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: I (soil/water) WATER
Sample wt/vol:
Lab Sample ID: H437575
Lab File ID: YV101716
I Level: (low/med)
5.000 (g/mL) ML
LOW Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 2500.0 I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: not dee.
GC Column: ID: 0. 53 (mm)
Soil Extract Volume: (uL) Soil Aliquot Volume: ----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
25000
25000
25000
1400
58000
25000
25000
25000
107-06-2--------1,2-Dichloroethane 350000
67-66-3---------Chloroform 25000
78-93-3---------2-Butanone 25000
71-55-6---------1,1,1-Trichloroethane 25000
56-23-5---------Carbon Tetrachloride 25000
75-27-4---------Bromodichloromethane 25000
78-87-5---------1,2-Dichloropropane 25000
10061-01-5------cis-l,3-Dichloropropene 25000
79-01-6---------Trichloroethene -25000
71-43-2---------Benzene 25000
10061-02-6------trans-l,3-Dichloropropene 25000
79-00-5---------1,1,2-Trichloroethane --25000
124-48-1--------Chlorodibromomethane 25000
75-25-2---------Bromoform 25000
108-10-1--------4-Methyl-2-pentanone 37000
79-34-5---------1,1,2,2-Tetrachloroethane 25000 --127-18-4--------Tetrachloroethene 25000
591-78-6--------2-Hexanone 25000
108-88-3--------Toluene 27000
108-90-7--------Chlorobenzene 25000
100-41-4--------Ethylbenzene 25000
100-42-5--------Styrene 25000
FORM I VOA
-----
Q
u
u
u
DJ
D
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
u
D
u
u
u
D
u
u
u
3/90
(uL
lA
(11Hl(.,)~4S
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-0BDL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Soil Extract Volume: (uL)
Lab Sample ID: H437575
Lab File ID: YV101716
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor:. 2500.0
Soil Aliquot Volume: ---------
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane _______ _
107-13-1--------Acrylonitrile~-------
----------------Xylene (total) _______ _
FORM I VOA
25000 U
120000 U
25000 U
3/90
I
·• I
I
I
I
(UL
1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
c1iln111:,c
EPA SAMPLE NO.
EX-09
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
Matrix: (soil/water) WATER
Sample wt/vol:
Lab Sample ID: H437576
Lab File ID: YV101725
I Level: (low/med)
5.000 (g/mL) ML
LOW Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 250.0 I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: (uL) Soil Aliquot Volume: -----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
2500
2500
2500
170
37000
2500
2500
2500
107-06-2--------1,2-Dichloroethane 160000
67-66-3---------Chloroform 2500
78-93-3---------2-Butanone 2500
71-55-6---------1,1,1-Trichloroethane 620
56-23-5---------Carbon Tetrachloride 2500
75-27-4---------Bromodichloromethane 2500
78-87-5---------1,2-Dichloropropane 11000
10061-01-5------cis-l,3-Dichloropropene 2500
79-01-6---------Trichloroethene 2500
71-43-2---------Benzene 2500
10061-02-6------trans-l,3-Dichloropropene 560
79-00-5---------1 1 2-Trichloroethane --2500
. ' ' 124-48-1--------Chlorodibromomethane 2500
75-25-2---------Bromoform 2500
108-10-1--------4-Methyl-2-pentanone 3300
79-34-5---------1,1,2,2-Tetrachloroethane --2500
127-18-4--------Tetrachloroethene 2500
591-78-6--------2-Hexanone 510
108-88-3--------Toluene 28000
108-90-7--------Chlorobenzene 2500
100-41-4--------Ethylbenzene 480
100-42-5--------Styrene 2500
FORM I VOA
____ (uL
Q
u
u
u
J
u
u
u
E
u
u
J
u
u
u
u
u
J
u
u
u
u
u
J
u
J
u
3/90
('1 lfl/, 1 _'(','
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437576
Lab File ID: YV101725
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 250.0
I
I
I
I
I
I
Soil Extract Volume: (uL) -----Soil Aliquot Volume: _____ (uL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane _______ _
107-13-1--------Acrylonitrile _______ _
----------------Xylene (total) ______ _
FORM I VOA
2500 U
25000
1800 J
Q
3/90
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-09DL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No.: PKGll
I
I
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Lab Sample ID: H437576
Lab File ID: YV101717
I GC Column: ID: 0.53 (mm)
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: ----
CAS NO. COMPOUND
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---0 -----1,l-Dichloroethane
10000
10000
10000
550
46000
10000
10000
10000
107-06-2--------1,2-Dichloroethane 190000
67-66-3---------Chloroform 10000
78-93-3---------2-Butanone 10000
71-55-6---------1,1,1-Trichloroethane 10000
56-23-5---------Carbon Tetrachloride 10000
75-27-4---------Bromodichloromethane 10000
78-87-5---------1,2-Dichloropropane 10000
10061-01-5------cis-l,3-Dichloropropene 10000
79-01-6---------Trichloroethene 10000
71-43-2---------Benzene 10000
10061-02-6------trans-l,3-Dichloropropene 10000
79-00-5---------1,1,2-Trichloroethane --10000
124-48-1--------Chlorodibromomethane 10000
75-25-2---------Bromoform 10000
108-10-1--------4-Methyl-2-pentanone 2700
79-34-5---------1,1,2,2-Tetrachloroethane --10000
127-18-4--------Tetrachloroethene 10000
591-78-6--------2-Hexanone 10000
108-88-3--------Toluene 28000
108-90-7--~-----Chlorobenzene 10000
100-41-4--------Ethylbenzene 10000
100-42-5--------Styrene 10000
FORM I VOA
____ (uL
Q
u u
u
DJ
D u
u u
D
u u u
u u
D
u u
u
u
u
u
u
DJ
u
u
u
D
u
u
u
3/90
lA
(1(1(101 '.'2
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No.: PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0. 53 (mm)
Lab Sample ID: H437576
Lab File ID: YV101717
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
I
I
I
I
I
I
Soil Extract Volume: (uL) ----Soil Aliquot Volume: _____ (UL
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane --------107 -l 3 -l --------Ac r y lo nit rile~-------
----------------Xylene (total) _______ _
FORM I VOA
10000 U
19000 DJ
1200 DJ
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-10
Lab Name: PASI, HOUSTON Contract: 001 I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
I
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
5.000 (g/mL) ML
LOW
Lab Sample ID: H437577
Lab File ID: YV101718
I GC Column: ID: 0. 53 (mm)
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 500.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Extract Volume: (uL) -----Soil Aliquot Volume: ----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-83-9---------Bromomethane 5000 u
75-01-4---------Vinyl Chloride 5000 u
75-00-3---------Chloroethane 5000 u
75-09-2---------Methylene Chloride 370 J
67-64-1---------Acetone 75000
75-15-0---------Carbon Disulfide 5000 u
75-35-4---------1,1-Dichloroethene 5000 u
75-34-3---0 -----1,l-Dichloroethane 5000 u
107-06-2--------1,2-Dichloroethane 35000
67-66-3---------Chloroform 5000 u
78-93-3---------2-Butanone 5000 u
71-55-6---------1,1,1-Trichloroethane 5000 u
56-23-5---------Carbon Tetrachloride 5000 u
75-27-4---------Bromodichloromethane 5000 u
78-87-5---------1,2-Dichloropropane 78000
10061-01-5------cis-l,3-Dichloropropene 5000 u
79-01-6---------Trichloroethene 5000 u
71-43-2---------Benzene 5000 u
10061-02-6------trans-l,3-Dichloropropene 5000 u
79-00-5---------1,1,2-Trichloroethane --5000 u
124-48-1--------Chlorodibromomethane 5000 u
75-25-2---------Bromoform 5000 u
108-10-1--------4-Methyl-2-pentanone 5000 u
79-34-5---------1,1,2,2-Tetrachloroethane 5000 u --127-18-4--------Tetrachloroethene 5000 u
591-78-6--------2-Hexanone 5000 u
108-88-3--------Toluene 15000
108-90-7--------Chlorobenzene 5000 u
100-41-4--------Ethylbenzene 2400 J
100-42-5--------Styrene 5000 u
FORM I VOA 3/90
(uL
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-10
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol: 5.000 (g/mL) ML
LOW Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0.53 (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
74-87-3---------Chlorornethane
107-13-1--------Acrylonitrile
----------------Xylene (total)
Lab Sample ID: H437577
Lab File ID: YV101718
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 500.0
Soil Aliquot Volume: ----
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
5000 u
13000 J
7300
FORM I VOA 3/90
I
I
I
I
I
I
(uL
1
I
I
I
I
I
I
I
I
I
I
I
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-l0DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437577
I Sample wt/vol: 5. 000 (g/mL) ML
LOW
Lab File ID: YV101723
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Level: (low/med)
% Moisture: not dee.
GC Column: ID: 0. 53, (mm)
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---•-----l,l-Dichloroethane
107-06-2--------1,2-Dichloroethane
67-66-3---------Chloroform
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
124-48-1--------Chlorodibromomethane
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-pentanone
79-34-5---------1,1,2,2-Tetrachloroethane --127-18-4--------Tetrachloroethene
591-78-6--------2-Hexanone
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
FORM I VOA
Q
10000 u
10000 u
10000 u
740 DJ
52000 D
10000 u
10000 u
10000 u
30000 D
10000 u
10000 u
10000 u
10000 u
10000 u
64000 D
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
10000 u
12000 D
10000 u
1600 DJ
10000 u
3/90
lA
(HI001'.{3 EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX-l0DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
GC Column:
5.000 (g/mL) ML
LOW
ID: 0.53 (mm)
Lab Sample ID: H437577
Lab File ID: YV101723
Date Received: 10/09/96
Date Analyzed: 10/17/96
Dilution Factor: 1000.0
I
I
I
I
I
I
Soil Extract Volume: (uL) Soil Aliquot Volume: ____ (uL ----
CAS NO. COMPOUND
74-87-3---------Chloromethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------107 -l 3 - l - - ----- -Ac r y lo nit rile~--------
----------------Xylene (total) _______ _
Q
10000 U
50000 U
5400 DJ
-----------------------------, _______ ---
FORM I VOA 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
m
I
D
D
m
E
I
I
I
I
I
I
I
I
I
I
I
Appendix C
Semivolatile Organics Analysis Data Sheets
Plume Periphery Wells
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
._:! ·.: .') •·~ :i
EPA SAMPLE NO.
EX-01
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
m
D
Matrix: (soil/water} WATER
Sample wt/vol:
Level: (low/med}
% Moisture:
1000
LOW
(g/mL} ML
decanted:
Lab Sample ID: H437852
Lab File ID: ZV110422
D Concentrated Extract Volume:
(Y/N}
1000 (uL}
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 1.0
m
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL}
GPC Cleanup: (Y/N} N pH: 7 .1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl}ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane}
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy}methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
10 u
17
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
lC EPA SAMPLE NO.
SEMIVOLA,TILE ORGANICS ANALYSIS DATA SHEET
EX-01
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437852
Sample wt/vol: Lab File ID: ZV110422
Level: (low/med)
% Moisture:
100 0 ( g /mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--"-----4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
3 J
10 u
10 u
28
10 u
10 u
10 u
140 E
7 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
EPA SAMPLE NO.
EX-02
m Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water)
m Sample wt/vol:
D Level: (low/med)
% Moisture:
D Concentrated Extract
Injection Volume:
WATER
1000 (g/mL) ML
LOW
decanted: (Y/N)
Volume: l000(uL)
2.0(uL)
Lab Sample ID: H437847
Lab File ID: ZV110419
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
D GPC Cleanup: (Y/N) N pH: 7.2
m
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9-- - - - --·-2, 4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Diriitrotoluene
FORM I SV-1
Q
180 E
300 E
10 u
10 u
10 u
10 u
10 u
1.0 u
10 u
21
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
:·1 f 1 .. ~ n ri
. -, t ·~ ,)
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437847
Sample wt/vol: Lab File ID: ZV110419
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--"-----4,6-Dinitro-2-methylphenol
86-30-6-- - - --. - --N-Nitrosodiphenylamine_ ( 1) =
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I
Lab Name: PASI, HOUSTON Contract: 001
EX-02DUP
• Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix:
m Sample wt/vol:
(soil/water) WATER
(g/mL) ML
Lab Sample ID: H437849
Lab File ID: ZV110421 o Level: (low/med)
1000
LOW
decanted: (Y/N)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
% Moisture:
0 Concentrated Extract Volume: 1000 (uL)
n
m
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
240 E
380 E
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004
·": f: ~, .~.! -i
EPA SAMPLE.NO.
EX-02DUP
SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437849
Sample wt/vol: Lab File ID: ZV110421
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)---101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8 ---------Phenanthr.ene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02DL
Lab Name: PASI, HOUSTON Contract: 001
m Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
g Matrix:
Sample wt/vol:
(soil/water) WATER
(g/mL) ML Lab File ID:
Lab Sample ID: H437847
ZS111709 o Level: (low/med)
1000
LOW
decanted: (Y/N)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 5.0
% Moisture:
D Concentrated Extract Volume: l000(uL)
m
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
111-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-5O-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2, 2 '.-Oxybis ( 1-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloioethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-S7-6---------2-Methylnaphthalene
77-4 7-·4------ ---Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
9S-9S-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
Sl-28-S---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
200 D
320 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
22 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
so u
so u so u
120 u
120 u so u
120 u
50 u
120 u
120 u
50 u
3/90
lC
:·.·_, :: ) ,1 ·:: I
EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-02DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437847
Sample wt/vol: Lab File ID: ZS111709
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)---101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9-- - - - - --Chrysene · ·
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo{b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-03DL
Lab Name: PASI, HOUSTON Contract: 001 • Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix:
m
(soil/water) WATER
Sample wt/vol: (g/mL) ML
Lab Sample ID: H437851
Lab File ID: ZV110427 o Level: (low/med)
1000
LOW
decanted: (Y /N)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 5.0
% Moisture:
D Concentrated Extract Volume: l000(uL)
D
m
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
39 DJ
140 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
6 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
120 u
50 u
120 u
50 u
120 u
120 u
50 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437851
Sample wt/vol: Lab File ID: ZV110427
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--"-----4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b}fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
50 u
50 u
4 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
EX-03
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437851
m Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: ZS111713
n Level: (low/med)
% Moisture: decanted: (Y /N)
D Concentrated Extract Volume: 1000 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/18/96
Dilution Factor: 4.0
ti
m
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
37 J
130
40 u
40 u
40 u
40 u
40 u
40 u
40 u
6 J
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
100 u
100 u
40 u
100 u
40 u
100 u
100 u
40 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-03
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437851
Sample wt/vol: Lab File ID: ZS111713
Level: (low/med)
% Moisture:
10 0 0 ( g /mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/18/96
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-ll-3--------Dimethylp---,-h~t~h-a~l~a-t~e-------
84-66-2---------Diethylphthalate~-~-~--
7005-72-3-------4-Chlorophenyl phenyl ether
100-01-6--------4-Nitroaniline -~-~~-~-534 -52 -l - - - - - - - -4, 6 -Dini tr o - 2 -methyl phenol
86-30-6---------N-Nitrosodiphenylamine (l)-
101-55-3--------4-Bromophenyl phenyl ether-
118-74-1--------Hexachlorobenzene ------87-86-5---------Pentachlorophenol _____ _
85-01-8---------Phenanthrene ---------120 - l 2 - 7 - - - - - - - -Ant hr ace n e ~~~~------84 -74 - 2 - - - - - - - - -Di -N -butyl p ht ha late ____ _
206-44-0--------Fluoranthene ________ _
129-00-0--------Pyrene __ ~~~~~-----
85-68-7---------Butylbenzylphthalate ___ _
56-55-3---------Benzo(a)anthracene_..,-----
91-94-1---------3,3'-Dichlorobenzidine ---218-01-9--------Chrysene,_.,,..,..-----,-.,-.,....,--,-~-,---
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate ____ -_-
205-99-2--------Benzo(b)fluoranthene ____ _
207-08-9--------Benzo(k)fluoranthene ____ _
50-32-8---------Benzo(a)pyrene...,.,.. ______ _
193-39-5--------Indeno(l,2,3-cd)pyrene __ _
53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ____ _
132-64-9--------Dibenzofuran~--------
606-20-2--------2,6-Dinitrotoluene _____ _
86-74-8---------Carbazole __________ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
40 u
40 u
40 u
40 u
100 u
100 u
40 u
40 u
40 u
100 u
40 u
40 u
40 u
40 u
40 u
4 J
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
, I
I
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04DL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
m
Matrix: (soil/water) WATER
Sample wt/vol: (g/mL) ML
Lab Sample ID: H437850
Lab File ID: ZV110426
g Level: (low/med)
1000
LOW
decanted: (Y/N)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 5.0
% Moisture:
U Concentrated Extract Volume: 1000 (uL)
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1------~-2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
8 DJ
52 D
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
120 u
50 u
120 u
50 u
120 u
120 u
50 u
3/90
.,
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437850
Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZV110426
Level: (low/med)
% Moisture:
Concentrated Extract
Injection Volume:
LOW
decanted:
Volume:
2. 0 (uL)
(Y/N)
1000 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
• 56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
50 u
50 u
3 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 1B
'·,. ; ' I ' • -: •_:f.)..:_ _I
EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-04
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437850
m Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZS111712
I Level.:· (low/med)
% Moisture:
LOW
decanted:
I Concentrated Extract Volume:
(Y/N)
1000 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/18/96
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2. 0 (uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
2
49
4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
25
25
10
25
10
25
25
10
Q
J
J
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3/90
•I ,, G .-1· ,_ .. -
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-04
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437850
Sample wt/vol: Lab File ID: ZS111712
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/18/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
m
I
H
I
I
I
n
R
I
I
I
I
I
1B
r1 fl r:;, ~
EPA SAAPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-09
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437839
Sample wt/vol: Lab File ID: ZV110424
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 2.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
8 J
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
50 u
50 u
20 u
50 u
20 u
50 u
3 J
20 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-09
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437839
Sample wt/vol: Lab File ID: ZV110424
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Injection Volume: 2.0(uL) Dilution Factor: 2.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--r-----4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl phenyl ether--118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1--~------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
20
20
20
20
50
50
20
20
20
50
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Q
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
18
,·; (; (; :.
EPA SAMPLE NO:
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-10
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
I
I
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture:
1000
LOW
(g/mL) ML
decanted:
Lab Sample ID: H437840
Lab File ID: ZV110428
I Concentrated Extract Volume:
(Y/N)
l00O(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 10.0 Injection Volume: 2.0(uL)
I GPC Cleanup: (Y/N) N pH: 7.0
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4------0 -Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---"-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
250 u
100 u
250 u
250 u
100 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-10
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437840
Sample wt/vol: Lab File ID: ZV110428
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y/N)
l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)---101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3 ---------Benzo (a).anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
,-, (, . ., .
' I : . .J EPA SAMPLE NO.
NS-11
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437841
I Sample wt/vol: 1000
LOW
(g/mL) ML Lab File ID: ZV110423
I
I
I
I
I
I
I
I
I
I
I
I
I
B
I
Level: (low/med)
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 1.0
GPC Cleanup: (Y /N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene --88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
4 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-11
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437841
Sample wt/vol: Lab File ID: ZV110423
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
86-73-7---------Fluorene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
-----------13 l -l l - 3 - - - - - - - -Dimethyl p ht ha late _____ _
84-66-2---------Diethylphthalate~-~-~--
7005-72-3-------4-Chlorophenyl phenyl ether
100-01-6--------4-Nitroaniline ----,---,----,----,--534 -52 - l - -, - - - - -4, 6 -Dini tr o - 2 -methyl phenol
86-30-6---------N-Nitrosodiphenylamine (l)-
10·1-55-3--------4-Bromophenyl phenyl ether=
118-74-1--------Hexachlorobenzene ------87-86-5---------Pentachlorophenol _____ _
85-01-8---------Phenanthrene ________ _
120-12-7--------Anthracene ~~~-------84 -74 - 2 - - - - - - - - -Di -N -butyl p ht ha late ____ _
206-44-0--------Fluoranthene ________ _
129-00-0--------Pyrene __ ~~-~------
85-68-7---------Butylbenzylphthalate ____ _
56-55-3---------Benzo(a)anthracene..,,.., ____ _
91-94-1---------3,3'-Dichlorobenzidine ---218-01-9--------Chrysene ____ ~~~~---
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate ____ -_-
205-99-2--------Benzo(b)fluoranthene ___ _
207-08-9--------Benzo(k)fluoranthene ___ _
50-32-8---------Benzo(a)pyrene=-------
193-39-5--------Indeno(l,2,3-cd)pyrene __ _
53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ___ _
132-64-9--------Dibenzofuran~--------
606-20-2--------2,6-Dinitrotoluene _____ _
86074-8---------Carbazole __________ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
4 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
n r, 'l . -
EPA SAMPLE r:fo·l
NS-15
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Matrix: (soil/water) WATER Lab Sample ID: H437844
Sample wt/vol: (g/mL) ML Lab File ID: ZV110417
Level: (low/med)
% Moisture:
1000
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
1 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-15
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437844
Sample wt/vol: (g/mL) ML Lab File ID: ZV110417
Level: (low/med)
% Moisture:
1000
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Injection Volume: 2.0(uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
10
10
10
10
25
25
10
10
10
25
10
10
10
10
10
10
10
10
10
2
10
10
10
10
10
10
10
10
10
10
Q
u
u
u
u u u
u
u
u
u
u
u
u
u u
u
u
u u
J u
u
u
u
u
u
u u
u u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-29
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437842
I Sample wt/vol: 1000
LOW
(g/mL) ML Lab File ID: ZV110429
I -% Moisture:
Level: (low/med)
decanted: (Y/N)
I Concentrated Extract Volume: l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 10.0
I
I
I
I
I
I
I
I
D
I
I
I
I
Injection Volume: 2 . 0 (UL)
GPC Cleanup: (Y/N) N pH: 7 .1
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50.-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1---.-----2, 2' -Oxybis (1-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
270
740
100 u
100 u
100 u
100 u
100 u
100 u
100 u
25 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
250 u
100 u
250 u
250 u
100 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437842
Sample wt/vol: Lab File ID: ZV110429
Level: (low/med)
% Moisture:
10 0 0 ( g /mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 10.0
GPC Cleanup: (Y/N) N pH: 7 .1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29DL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
I
Matrix:
Sample wt/vol: (g/mL) ML Lab File ID:
(soil/water) WATER Lab Sample ID: H437842
ZS111707
I Level: (low/med)
1000
LOW
decanted: ( Y /N)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 20.0
% Moisture:
I Concentrated Extract Volume: 1000 (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
320 D
740 D
200 u
200 u
200 u
200 u
200 u
200 u
200 u
26 DJ
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
500 u
500 u
200 u
500 u
200 u
500 u
500 u
200 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-29DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437842
Sample wt/vol: Lab File ID: ZS111707
Level: (low/med)
% Moisture:
10 0 0 ( g /mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 20.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1-----~--4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylarnine_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
200 u
200 u
200 u
200 u
500 u
500 u
200 u
200 u
200 u
500 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
200 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
EPA SAMPLE NO.
NS-30
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Matrix: (soil/water) WATER Lab Sample ID: H437843
Sample wt/vol: (g/mL) ML Lab File ID: ZV110416
Level: (low/med)
% Moisture:
1000
LOW
decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7 .1
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---~-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1--------~Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50°7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7------~-4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
10 u
4 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-30
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437843
Sample wt/vol: Lab File ID: ZV110416
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Difution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene.....,..~--,~-------
131-ll-3--------Dimethylphthalate ______ 1
84-66-2---------Diethylphthalate. ______ _
7005-72-3-------4-Chlorophenyl phenyl ether
100-01-6--------4-Nitroaniline -~-,--,-----;--534 -52 - l - --- - - - -4, 6 -Dini tr o - 2 -methyl phenol
86-30-6---------N-Nitrosodiphenylamine (l)-
101-55-3--------4-Bromophenyl phenyl ether-
118-74-1--------Hexachlorobenzene ------87-86-5---------Pentachlorophenol _____ _
85-01-8---------Phenanthrene ________ _
120-12-7--------Anthracene ---,-~--,~------84 -74 - 2 - - - - - - - - -Di -N -butyl p ht ha late ____ _
206-44-0--------Fluoranthene ________ _
129-00-0--------Pyrene _____ ~------
85-68-7---------Butylbenzylphthalate ___ _
56-55-3---------Benzo(a)anthracene~-----
91-94-1---------3,3'-Dichlorobenzidine ----
218-01-9--------Chrysene,--~---,,...,.--,--,--;---=----
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate ____ _
205-99-2--------Benzo(b)fluoranthene ___ _
207-08-9--------Benzo(k)fluoranthene ____ _
50-32-8---------Benzo(a)pyrene _______ _
193-39-5--------Indeno(l,2,3-cd)pyrene __ _
53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ___ _
132-64-9--------Dibenzofuran~--------
606-20-2--------2,6-Dinitrotoluene _____ _
86-74-8---------Carbazole __________ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
•., -' I 18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PASI, HOUSTON Contract: 001
NS-31
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437845
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: ZV110425
I Level: (low/med)
% Moisture: decanted: (Y /N)
I Concentrated Extract Volume: l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 2.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---·-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
120
220 E
20 u
20 u
20 u
20 u
20 u
20 u
20 u
15 J
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
50 u
50 u
20 u
50 u
20 u
50 u
50 u
20 u
3/90
''.
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437845
Sample wt/vol: Lab File ID: ZV110425
Level: ( low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/05/96
Dilution Factor: 2.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
20 u
20 u
20 u
20 u
50 u
50 u
20 u.
20 u
20 u
50 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
20 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
.. , ( \ .---EPA SAMPLE·'.'Nb-! 1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31DL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001
Matrix:
Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
(soil/water) WATER Lab Sample ID: H437845
I Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZS111708
I Level: (low/med)
%-Moisture:
LOW
decanted:
I Concentrated Extract Volume:
(Y/N)
l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 4.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene --88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
100 D
200 D
40 u
40 u
40 u
40 u
40 u
40 u
40 u
13 DJ
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
100 u
100 u
40 u
100 u
40 u
100 u
100 u
40 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-31DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437845
Sample wt/vol: Lab File ID: ZS111708
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/17/96
Dilution Factor: 4.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
86-73-7---------Fluorene
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
---,--~~----,--------13 l -11 -3 --------Dimethyl p ht ha late _____ _
84-66-2---------Diethylphthalate,.......-~----,----
7005-72-3-------4-Chlorophenyl phenyl ether
100-01-6--------4-Nitroaniline -~~~,--~-534 -52 -1 --------4, 6 -Dini tr o -2 -methyl phenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl phenyl ether-
118-74-1--------Hexachlorobenzene _____ _
87-86-5---------Pentachlorophenol _____ _
85-01-8---------Phenanthrene ________ _
120-12-7--------Anthracene~~~,-,--------
84-74-2---------Di-N-butylphthalate ____ _
206-44-0--------Fluoranthene ________ _
129-00-0--------Pyrene __ ~---,----,-------,,----,------
85-68-7---------Butylbenzylphthalate ___ _
56-55-3---------Benzo(a)anthracene~-----
91-94-1---------3,3'-Dichlorobenzidine ----218-01-9--------Chrysene,.......=--~~~~,---
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate ____ -_-
205-99-2--------Benzo(b)fluoranthene ____ _
207-08-9-·-------Benzo (kl fluoranthene ___ _
50-32-8---------Benzo(a)pyrene=-------
193-39-5--------Indeno(l,2,3-cd)pyrene ---53-70-3---------Dibenz(a,h)anthracene ___ _
191-24-2--------Benzo(g,h,i)perylene ____ _
132-64-9--------Dibenzofuran ________ _
606-20-2--------2,6-Dinitrotoluene _____ _
86-74-8---------Carbazole __________ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
40 u
40 u
40 u
40 u
100 u
100 u
40 u
40 u
40 u
100 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
40 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-32
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001
Matrix:
Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
(soil/water) WATER Lab Sample ID: H437846
I Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZV110418
I Level: (low/med)
% Moisture:
LOW
decanted:
I Concentrated Extract Volume:
(Y/N)
1000 (uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6------~-4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamin~_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
I (1) -Cannot be separated from Diphenylamine
FORM I SV-2
I
Q
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3/90
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS-32
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKG12
Matrix: (soil/water) WATER Lab Sample ID: H437846
Sample wt/vol: Lab File ID: ZV110418
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Date Received: 10/16/96
Date Extracted:10/20/96
Date Analyzed: 11/04/96
Injection Volume: 2.0(uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1-------~-1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
25
25
10
25
10
25
25
10
Q
u
u
u
u
u
u
u u
u
u u
u u
u u u
u
u
u u u u
u
u
u u
u
u
u
u
u
u
u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Q
II
11 II
Appendix C
Semivolatile Organics Analysis Data Sheets
Trench Area Wells
I
I
18
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
ill H If,' ,.·t'~1
EPA SAMPLE NO.
EX~05
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Matrix: (soil/water) WATER Lab Sample ID: H437572
Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZV110413
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 50.0
Concentrated Extract Volume: 5000(uL)
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9--------~Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
3800
170 J
2500 u
2500 u
2500 u
2500 u
760 J
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
6200 u
6200 u
2500 u
6200 u
2500 u
6200 u
6200 u
2500 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-05
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437572
Sample wt/vol: Lab File ID: ZV110413
Level: (low/med)
% Moisture:
100 0 ( g /mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 5000 (uL)
Injection Volume: 2.0(uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 50.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86_-30-6 - - - - - - - --N-Nitrosodiphenylamine __ ( 1) =
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
2500 u
2500 u
2500 u
2500 u
6200 u
6200 u
2500 u
2500 u
2500 u
6200 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
fJD2G'J
18 EPA SAMPLE NO ..
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
Matrix: (soil/water) WATER
Sample wt/vol: (g/mL) ML
Lab Sample ID: H437573
Lab File ID: ZV110216
I Level: (low/med)
1000
LOW
decanted: (Y /N)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/02/96
Dilution Factor: 1.0
% Moisture:
I Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
I GPC Cleanup: (Y/N) N pH: 7.2
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
290 E
16
10 u
10 u
10 u
10 u
10 u
10 u
10 u
12
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
25 u
10 u
25 u
25 u
10 u
3/90
00270
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437573
Sample wt/vol: Lab File ID: ZV110216
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: ( Y /N)
Concentrated Extract Volume: l000(uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/02/96
Injection Volume: 2. 0 (uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO . COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--•-----4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2--~------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
10
10
10
10
25
25
10
10
10
25
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Q
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
OUJOO
EPA SAMPLE NO.
EX-06DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437573
I Sample wt/vol: (g/mL) ML Lab File ID: ZV110404
I Level:
% Moisture:
(low/med)
1000
LOW
decanted: (Y/N)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 5.0
I Concentrated Extract Volume: l000(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5-~-------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
310 D
15 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
13 DJ
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
120 u
120 u
50 u
120 u
50 u
120 u
120 u
50 u
3/90
lC
OUJ01
EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-06DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437573
Sample wt/vol: Lab File ID: ZV110404
Level: ( low/med)
% Moisture:
10 0 0 ( g /mL) ML
LOW
decanted:
Concentrated Extract Volume:
(Y /N)
l0O0(uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 5.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--,-----4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene '
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--0 -----Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
50 u
50 u
50 u
120 u
120 u
50 u
50 u
50 u
120 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
50 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
0 r,'"'"' ""l LI J Jr..
EPA SAMPLE NO.
EX-07
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
I
I
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
% Moisture:
Concentrated Extract
Injection Volume:
WATER
1000 (g/mL) ML
LOW
decanted: (Y /N)
Volume: l000(uL)
2:0(uL)
Lab Sample ID: H437574
Lab File ID: ZV110217
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/03/96
Dilution Factor: 10.0
I GPC Cleanup: (Y/N) N pH: 7 .2
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
111-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---·-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine --106-44-5--------4-~ethylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
111-91-1--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
1700 E
100 u
7 J
100 u
100 u
100 u
100 u
100 u
100 u
32 J
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
250 u
250 u
100 u
250 u
100 u
250 u
250 u
100 u
3/90
O(J"'l' ,J J J
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437574
Sample wt/vol: Lab File ID: ZV110217
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Date Received: 10/09/96
Date Extracted:i0/11/96
Date Analyzed: 11/03/96
Injection Volume: 2.0(uL) Dilution Factor: 10.0
GPC Cleanup: (Y /N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl phenyl ether=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
.206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9---~----Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
100 u
100 u
100 u
100 u
250 u
250 u
100 u
100 u
100 u
250 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
100 u
Q
.
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
EPA SAMPLE NO.
EX-07DL
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I Matrix:
Sample wt/vol: (g/mL) ML Lab File ID:
(soil/water) WATER Lab Sample ID: H437574
ZV110409
I Level: (low/med)
1000
LOW Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 50.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N
(Y/N)
1000 (uL)
pH: 7.0
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---•-----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
2200 D
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
31 DJ
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
1200 u
1200 u
500 u
1200 u
500 u
1200 u
1200 u
500 u
3/90
(\'''),-,·
· 1.... J '...J J
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-07DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437574
Sample wt/vol: Lab File ID: ZV110409
Level: (low/med)
% Moisture:
10 0 0 ( g /mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 50.0
GPC Cleanup: (Y/N) N pH: 7.0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6------~--N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74~2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
500 u
500 u
500 u
500 u
1200 u
1200 u
500 u
500 u
500 u
1200 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
500 u
3/90
I
I
I
I
I
I
I
I
I
I C
I
I
I
I
I
I
I
I
I
I
I
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PASI, HOUSTON Contract: 001
00383
EPA SAMPLE NO.
EX-08
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Matrix: (soil/water) WATER Lab Sample ID: H437575
Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZV110412
Level: (low/med) LOW Date Received: 10/09/96
% Moisture: decanted: (Y/N) Date Extracted:10/11/96
Concentrated Extract Volume: 5000(uL) Date Analyzed: 11/04/96
Injection Volume: 2.0(uL) Dilution Factor: 50.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene --88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
7300
2500 u
2500 u
2500 u
2500 u
2500 u
410 J
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
6200 u
6200 u
2500 u
6200 u
2500 u
6200 u
6200 u
2500 u
3/90
,_) ,_; '-'
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-08
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437575
Sample wt/vol: Lab File ID: ZV110412
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y /N)
Concentrated Extract Volume: 5000 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 50.0
GPC Cleanup: (Y/N) N pH: 7.1
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--•-----4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine (1) - -101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
2500 u
2500 u
2500 u
2500 u
6200 u
6200 u
2500 u
2500 u
2500 u
6200 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
2500 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
'', · l 1 · ,
·~, 'J : .t ' -1 I
I
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: • 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I
I
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture:
1000
LOW
(g/mL) ML
decanted: ( Y /N)
Lab Sample ID: H437576
Lab File ID: ZV110410
I Concentrated Extract Volume: 5000 (uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 20.0 Injection Volume:
I GPC Cleanup:
2 .0 (uL)
(Y/N) N pH: 7. 2
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
BB-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
1800
6600
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
2500 u
2500 u
1000 u
2500 u
1000 u
2500 u
2500 u
1000 u
3/90
. '
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-09
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437576
Sample wt/vol: Lab File ID: ZV110410
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 5000(uL)
Injection Volume: 2.0(uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 20.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--•-----4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
11 7-81-7-- --.-- --bis (2 -Ethylhexyl) phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
1000 u
1000 u
1000 u
1000 u
2500 u
2500 u
1000 u
1000 u
1000 u
2500 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
1000 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I lB EPA sAMEliE 4io0
I
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-10
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
I Matrix: ( soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Lab Sample ID: H437577
Lab File ID: ZV110218
I Level: (low/med) LOW
% Moisture: decanted: (Y/N)
I Concentrated Extract Volume: 1500 (uL)
1 Injection Volume:
GPC Cleanup: (Y/N) N
2.0(uL)
pH: 7.2
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/03/96
Dilution Factor: 200.0
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1--------2,2'-Oxybis(l-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
1200 J
27000 E
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
7500 u
7500 u
3000 u
7500 u
3000 u
7500 u
7500 u
3000 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-10
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437577
Sample wt/vol: Lab File ID: ZV110218
Level: (low/med)
% Moisture:
1000 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1500 (uL)
Injection Volume: 2. 0 (uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/03/96
Dilution Factor: 200.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--0 -----4,6-Dinitro-2-methylphenol_
86-30-6---------N-Nitrosodiphenylamine_(l)_
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo{b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9--------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
3000 u
3000 u
3000 u
3000 u
7500 u
7500 u
3000 u
3000 u
3000 u
7500 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3000 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I EX-l0DL
Lab Name: PASI, HOUSTON Contract: 001
I Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: I (soil/water) WATER
Sample wt/vol: (g/mL) ML
Lab Sample ID: H437577
Lab File ID: ZV110405
I Level: (low/med)
1000
LOW Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 400.0
% Moisture: decanted: (Y /N)
I Concentrated Extract Volume: 1500(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
111-44-4--------Bis(2-chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---0 -----2-Methylphenol
108-60-1.-- - - - - --2, 2' -Oxybis ( 1-chloropropane)
621-64-7--------N-Nitrosodi-N-propylamine __
106-44-5--------4-Methylphenol
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1--------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------Bis(2-chloroethoxy)methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
88-74-4---------2-Nitroaniline
208-96-8--------Acenaphthylene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
121-14-2--------2,4-Dinitrotoluene
FORM I SV-1
Q
1200 DJ
29000 D
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
15000 u
15000 u
6000 u
15000 u
6000 u
15000 u
15000 u
6000 u
3/90
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX-l0DL
Lab Name: PASI, HOUSTON Contract: 001
Lab Code: 001 Case No.: CHARLOTTE SAS No.: 004 SDG No. : PKGll
Matrix: (soil/water) WATER Lab Sample ID: H437577
Sample wt/vol: 1000 (g/mL) ML Lab File ID: ZV110405
Level: (low/med) LOW
% Moisture: decanted: (Y /N)
Concentrated Extract Volume: 1500 (uL)
Injection Volume: 2.0(uL)
Date Received: 10/09/96
Date Extracted:10/11/96
Date Analyzed: 11/04/96
Dilution Factor: 400.0
GPC Cleanup: (Y/N) N pH: 7.2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
86-73-7---------Fluorene
131-11-3--------Dimethylphthalate
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl phenyl ether -100-01-6--------4-Nitroaniline
534-52-1--0 -----4,6-Dinitro-2-methylphenol
86-30-6---------N-Nitrosodiphenylamine_(l)=
101-55-3--------4-Bromophenyl phenyl ether -118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-N-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
56-55-3---------Benzo(a)anthracene
91-94-1---------3,3'-Dichlorobenzidine
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate_
117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenz(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
132-64-9-~------Dibenzofuran
606-20-2--------2,6-Dinitrotoluene
86-74-8---------Carbazole
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
6000 u
6000 u
6000 u
6000 u
15000 u
15000 u
6000 u
6000 u
6000 u
15000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
6000 u
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Appendix D
I lnorganics Analysis Data Sheets
Plume Periphery Wells
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALi SBURY, NC 28145-03_99
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069822.3/ NS-09
SAMPLE NO: H437839
SAMPLE MATRIX: \JATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
2B
30
TEST
CODE
OVTUC
OSTWC
ABEWC
ACDWC
ACRWC
AMNUC
ANIWC
AZNWC
AASWC
ASEIJC
AALWC
ASBIJC
ACAWC
ACOWC
ACUWC
AFEWC
APBWC
AMGWC
AHGWC
AKWC
AAGWC
ANAWC
ATLWC
AWC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package \Jater
Data Package -VOA
TCL -BNA + CLP Data Package Water
Data Package -BNA
CLP Beryl l illll, Total (Be)
CLP Beryl l iun, Total
CLP Caciniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nick.et
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Al uni nun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (CU)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP SodillTI (Na)
CLP Thelliun (Tl)
CLP Vanadiun (V)
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Anal)'1ical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: 71J.l88-4661
Decerrber 04, 1996
Report No.: 00056911
Section A Page 1
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
0719 0641
661015501
000592
VERBAL
DATE SAMPLED: 14-0CT-96 0935
DATE RECEIVED: 16-0CT-96
PROJECT MANAGER: Katren Jenkins
DILUTION
FACTOR RESULT UNITS
off line
off line
0.4 B ug/L
4.8 u ug/L
97.2 ug/L
18,200 ug/l
40.9 ug/L
84.2 ug/l
,. 1 u ug/L
0.8 U ug/L
28,600 ug/L
4.3 u ug/l
250,000 ug/l
49. 7 B ug/L
131 ug/L
37,800 ug/L
2.5 B ug/L
96,000 ug/L
0.2 U ug/L
2,510 B ug/L
8.4 U ug/L
65,600 ug/L
1.6 U ug/L
26.4 B ug/L
Done
785 ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 26145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069823.1/ NS-10
SAMPLE NO: H437840
SAMPLE MATRIX: WATER
LN
2
6
7
6
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
26
30
TEST
CODE
OVTWC
OSTWC
ABEWC
ACOWC
ACRWC
AMNWC
ANIWC
AZNWC
AASWC
ASEWC
AALWC
ASBWC
ACAWC
ACO\JC
ACUWC
AFEWC
APBWC
AMGWC
AHGWC
AKIIC
AAGWC
ANAWC
ATLWC
AWC
OPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package \Jater
Data Package -VOA
TCL -BNA + CLP Data Package \.later
Data Package -BNA
CLP Berylliun, Total (Be)
CLP Berylliun, Total
CLP Caciniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Aluninun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thal liun (Tl)
CLP Vanadh.rn (V)
CLP Data Package Deliverable
CLP· Bariun, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: 71~-1610
Fax: [phone]
0ecelTber 04, 1996
Report No.: 00056911
Section A Page 2
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECE I VEO:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1000
16-0CT-96
Katren Jenkins
RESULT UN I TS
off line
offl ine
0.3 U ug/L
4.8 U ug/L
4.9 u ug/L.
4,850 ug/L
35.4 B ug/L
41. 1 ug/L
,. 1 u ug/L
0.8 u ug/L
478 ug/L
4.3 U ug/L
92,600 ug/l
44.8 B ug/L
6.4 U ug/l
3,730 ug/L
0.6 U ug/L
51,200 ug/L
0.2 U ug/l
1,470 B ug/l
8.4 U ug/l
115,000 ug/L
1.6 U ug/L
3.9 U ug/l
Done
293 ug/l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069824.0/ NS·11
SAMPLE NO: H437841
SAMPLE MATRIX: WATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
COOE
OVTWC
OSTWC
ABEWC
ACOWC
ACRWC
AMNWC
ANIWC
AZNUC
AASWC
ASEWC
AALWC
ASBWC
ACA\.IC
ACOWC
ACU\IC
AFEWC
APBWC
AMGWC
AHGWC
AKWC
AAGWC
ANAWC
ATLWC
AVWC
DPACK
ABAWC
DETERMINATION
TCL ·VOA+ CLP Data Package \.later
Data Package -VOA
TCL -BNA + CLP Data Package \.later
Data Package -BNA
CLP Beryl l iUTI, Total (Be)
CLP Beryl l iun, Total
CLP Cadmiun, Total (Cd)
CLP Chromiun, Total ( Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Aluninun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (CU)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thelliun (Tl)
CLP Venediun (V)
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Analytical Services, lnc.
900 Gemini Avenue
Houston, TX 77058
Tel: 71J.188-1810
Fax: 71~88-1661
Oecerrt>er 04, 1996
Report No.: 00056911
Section A Page 3
LI MS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1025
16·0CT·96
Katren Jenkins
RESULT UNITS
off line
offl ine
0.6 B ug/l
4.8 U ug/l
34.2 ug/L
841 ug/L
40.7 ug/l
65.0 ug/L
,. 1 u ug/L
D.8 U ug/L
11,500 ug/L
4.3 U ug/L
8,160 ug/L
44.5 B ug/L
39.5 ug/L
38,900 ug/L
2.8 B ug/L
5,390 ug/L
0.2 U ug/L
1,290 B ug/L
8.4 U ug/L
89,100 ug/L
1.6 U ug/L
63.4 ug/L
Done
301 ug/L
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX TT058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056911
Section A Page 4
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069825.8/ NS-29
SAMPLE NO: H437842
SAMPLE MATRIX: WATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
COOE
OVTWC
OSTWC
ABEWC
ACDWC
ACRWC
AMNWC
ANIWC
AZNWC
MSWC
ASEWC
MLWC
ASBWC
ACAWC
ACOIIC
ACUIIC
AFEWC
APBWC
AMGWC
AHGWC
AKIIC
MGWC
ANAWC
ATLWC
AVWC
DPACK
ABAWC
COMMENTS:
DETERMINATION
TCL -VOA+ CLP Data Package Water
Data Package -VOA
TCL -BNA + CLP Data Package Water
Data Package -BNA
CLP Beryl l iun, Total (Be)
CLP Beryl l iun, Total
CLP Cadmiun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Aluninun, Total (Al)
CLP Antimony
CLP-Calcillll, Total (Ca)
CLP Cabal t, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassl\.rn
CLP Silver, Total (Ag)
CLP Sodlln (Na)
CLP Thalliun (Tl)
CLP Vanadiun CV)
CLP Data Package Deliverable
CLP -Berilln, Total
* The salll)le required dilution due to matrix
a higher detection limit for Seleniun.
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
interferences which resulted in
DILUTION
FACTOR
2
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
0719 0641
661015501
000592
VERBAL
14-0CT-96 1125
16-0CT-96
Katren Jenkins
RESULT UN 1 TS
off line
offl ine
0.3 u ug/L
4.8 u ug/L
4.9 U ug/L
5,840 ug/l
15.3 U ug/L
19.0 B ug/L
1. 1 u ug/L
1.6 U * ug/L
114 B ug/L
4.3 u ug/L
443,000 ug/L
4.6 U ug/L
6.4 U ug/L
894 ug/l
0.8 U ug/L
47,300 ug/l
0.2 U ug/L
2,900 B ug/L
8.4 U ug/L
80,900 ug/L
1.6 U ug/L
8.4 B ug/L
Done
1,150 ug/l
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID, 92 069826,6/ NS-30
SAMPLE NO: H437843
SAMPLE MATRIX: WATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
COOE
OVTYC
OST\.JC
ABEYC
ACDYC
ACRYC
AMNYC
ANI\JC
AZNWC
AAS\JC
ASEWC
AALWC
ASB'JC
ACAYC
ACO'JC
ACWC
AFEYC
APB\JC
AMGWC
AHGWC
AKIIC
AAGYC
ANAWC
ATLYC
AWC
DPACK
ABA'JC
DETERMINATION
TCL ·VOA+ CLP Data Package Yater
Data Package -VOA
TCL -BNA + CLP Data Package 'water
Data Package -BNA
CLP Beryl l iun, Total (Be)
CLP Beryl l iun, Total
CLP Caciniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (A_s)
CLP Seleniun
CLP Al uni nun, Total (Al)
CLP Antimony
CLP-Catciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP Sodiiin (Na)
CLP Thall iun (Tl l
CLP Vanadiiin (V)
CLP Data Package Deliverable
CLP -BarillTI, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX TT058
Tel: [phone]
Fax: [phone]
Decenber 04, 1996
Report No.: 00056911
Section A Page 5
LIMS CLIENT,
PACE PROJECT:
PACE CLIENT:
P.O. NO,
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1140
16-0CT-96
Katren Jenkins
RESULT UNITS
off line
off line
0.3 U ug/L
4,8 U ug/L
4.9 U ug/L
1,400 ug/L
15.3 U ug/L
23.5 ug/L
1.1 U ug/L
0.8 U ug/L
104 B ug/L
4_3 U ug/l
93,400 ug/L
4.6 U ug/L
6.4 U ug/L
917 ug/L
0.8 U ug/L
17,800 ug/L
0.2 U ug/L
1,200 B ug/L
8.4 U ug/L
13,000 ug/L
1.6 U ug/L
3.9 U ug/L
Done
32.1 B ug/l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
·SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE 10: 92 069827.4/ NS-15
SAMPLE NO: H437844
SAMPLE MATRIX: WATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
COOE
OVTWC
OSTWC
ABEWC
ACDWC
ACRWC
AMNWC
ANIWC
AZNWC
AASWC
ASEWC
AAUJC
ASS\JC
ACAWC
ACOWC
ACUWC
AFEWC
APBWC
AMGWC
AHGWC
AKWC
AAGWC
ANA\JC
ATLWC
AVWC
DPACK
ABAWC
DETERMINATION
TCL -VOA + CLP Data Package Water
Data Package -VOA
TCL -BNA + CLP Data Package Water
Data Package -BNA
CLP Beryllillll, Total (Be)
CLP Beryl l illll, Total
CLP Cactniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenillll
CLP Alllllinllll, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP SocHun (Na)
CLP Thalth.m (Tll
CLP Vanadh.m .<VJ
CLP Data Package Deliv~rable
CLP· Baril.In, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX TT058
Tel: [phone]
Fax: 713-48~661
December 04, 1996
Report No. : 00056911
Section A Page 6
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1330
16-0CT-96
Katren Jenkins
RESULT UNITS
off line
offline
0.3 U ug/L
4.8 U ug/l
4.9 U ug/l
13,800 ug/L
15.3 U ug/L
30.6 ug/L
,. 1 u ug/L
0.8 U ug/L
94.4 B ug/l
4.3 u ug/L
321,000 ug/L
38.6 B ug/L
6.4 U ug/L
7,920 ug/L
0.8 U ug/L
153,000 ug/L
0.2 U ug/L
2,160 8 ug/L
8.4 U ug/L
57,400 ug/L
1.6 U ug/L
3.9 U ug/L
Done
405 ug/L
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: HR. KEN KLUTTZ
SAMPLE ID: 92 069828.2/ NS-31
SAMPLE NO: H437845
SAMPLE MATRIX: IJATER
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
CODE
OVTIJC
OSTYC
ABEi.JC
ACDYC
ACRYC
AMNWC
ANIYC
AZNYC
AAS\JC
ASEYC
AALYC
ASBYC
ACAYC
ACOIJC
ACUWC
AFEWC
APBWC
AMGYC
AHGWC
AKYC
AAGYC
ANAWC
ATLWC
AVYC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package 'water
Data Package -VOA
TCL -BNA + CLP Data Package \.later
Data Package -BNA
CLP Beryl l iun, Total (Be)
CLP Beryl l iun, Total
CLP caaniun, Total (Cd)
CLP ChromiLITl, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Al uni nun, Total (Al)
CLP Antimony
CLP-Cal c i Lill, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassii.in
CLP Silver, Total (Ag)
C_LP Sodiun (Na)
CLP Thalliun (Tl)
CLP Vanadiun CV)
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056911
Section A Page 7
LI MS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1355
16-0CT-96
Katren Jenkins
RESULT UN I TS
off line
offl ine
0.3 U ug/l
4.8 U ug/l
4.9 U ug/L
510 ug/L
15.3 u ug/L
15.3 B ug/L
1. 1 U ug/L
0.8 U ug/L
141 B ug/L
4.3 U ug/L
358,000 ug/L
4.6 U ug/L
6.4 U Ug/L
310 ug/L
0.8 U ug/L
17,700 ug/L
0.2 U ug/L
3,740 B ug/L
8.4 U ug/L
46,600 ug/L
1 .6 U ug/L
3.9 U ug/L
Done
6,280 ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069829.0/ NS-32
SAMPLE NO: H437846
SAMPLE MATRIX: WATER
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056911
Section A Page 8
LI MS Cll ENT: 0719 0641
PACE PROJECT: 661015501
PACE CLIENT: 000592
P.O. NO: VERBAL
DATE SAMPLED: 14-0CT-96 1415
DATE RECEIVED: 16-0CT-96
PROJECT MANAGER: Katren Jenkins
---------------------------------------------------. ------------------------------------------------. ---. -. -------------. ---- - -
LN
2
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
COOE
OVTWC
OSTWC
ABEWC
ACDWC
ACRWC
AMNWC
ANIWC
AZNWC
AASWC
ASEWC
AALWC
ASBWC
ACAWC
ACOWC
ACUWC
AFEWC
AP8WC
AMGWC
AHGWC
AKIIC
AAGWC
ANAWC
ATLWC
AVWC
DPACK
ABAWC
DETERMINATION
TCL ·VOA+ CLP Data Package Water
Data Package -VOA
TCL -BNA + CLP Data Package Water
Data Package -SNA
CLP Beryl l iun, Total (Be)
CLP Beryll iun, Total
CLP Caafliun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP AluninLrTI, Total (Al)
CLP Antimony
CLP-CalciLrTI, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (CU)
CLP Iron
CLP Lead
CLP Magnesill1l
CLP Mercury
CLP Potassill1l
CLP Silver, Total (Ag)
CLP Sodh.111 (Na)
CLP Thall iun (Tl)
CLP Vanadill1l (V)
CLP Data Package Deliverable
CLP -Sariun, Total
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
DILUTION
FACTOR RESULT UNITS
off line
off line
0.3 U ug/l
4.8 U ug/l
4.9 U ug/l
109 ug/L
15.3 u ug/l
19.9 B ug/l
1. 1 u ug/l
0.8 U ug/l
106 B ug/l
4.3 u ug/l
49,200 ug/l
4.6 U ug/l
6.4 u ug/l
198 ug/l
1. 9 B ug/l
8,370 ug/l
0.2 U ug/l
2,580 8 ug/L
8.4 U ug/l
8,890 B ug/L
1.6 u ug/L
3.9 U ug/L
Done
91.5 B ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069830,4/ EX·02
SAMPLE NO: H437847
SAMPLE MATRIX: UATER
LN
2
3
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
CODE
OVTWC
OSTWC
1435
ABEWC
ACDWC
ACR\JC
AMNWC
ANIWC
AZNWC
AASWC
ASEWC
AALWC
ASBWC
ACA\JC
ACO\IC
AC\JIIC
AFEWC
APBWC
AMGWC
AHGWC
AKIIC
AAGWC
ANAWC
ATLWC
AVIIC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package \Jater
Data Package -VOA
TCL -BNA + CLP Data Package w'ater
Data Package -BNA
Nitrogen, Kjeldahl (N)
CLP Beryl l iun, Total (Be)
CLP Beryl l iun, Total
CLP Cactniun, Total (Cd)
CLP Chromil,n, Total (Cr)
CLP Manganese
CLP. Nick.el
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Aluninun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thalliun (Tl)
CLP Vanadiun CV>
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report ~o.: 00056911
Section A Page 9
LIMS CLIENT:
PACE PROJECT:
PACE Cl I ENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14·0CT·96 1445
16-0CT-96
Katren Jenkins
RESULT UNITS
off line
offl ine
6.2 mg/L
0.3 u ug/L
4,8 u ug/L
17, 1 ug/L,
16,800 ug/l
15.3 U ug/L
28,2 ug/L
1.1 u ug/L
0.8 u ug/L
106 B ug/L
4,3 U ug/L
340,000 ug/L
4,6 U ug/L
6.4 U ug/L
13,000 ug/l
0,8 U ug/L
100,000 ug/L
0.2 U ug/L
3,170 B ug/L
8.4 u ug/l
108,000 ug/L
1.6 U ug/L
6. 1 B ug/L
Done
1,370 ug/l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME:
ADDRESS:
NATIONAL STARCH & CHEMICAL COMPANY
P.O. BOX 399
ATTENTION:
SALISBURY, NC 28145·0399
MR. KEN KLUTTZ
SAMPLE ID: 92 069831.2/ EX-02 MATRIX
SAMPLE NO: H437848
SAMPLE MATRIX: WATER
LN
TEST
CODE DETERMINATION
OVTWC TCL -VOA+ CLP Data Package Water
Data Package -VOA
2 OST\JC TCL -BNA + CLP Data Package Water
Data Package -BNA
3 1435 Nitrogen, Kjetdahl (N)
6 ABE\JC CLP Beryl l iLITI, Total (Be)
CLP Beryll iun, Total
7 ACDWC CLP Caciniun, Total (Cd)
8 ACRWC CLP ChromillTl, Total (Cr)
9 AMNWC CLP ManganeSe
10 ANIWC CLP Nickel
11 AZNWC CLP Zinc
12 AASWC CLP Arsenic, Total (As)
13 ASEWC CLP Seleniun
14 AALWC CLP Al uni nun, Total (Al)
15 ASBWC CLP Antimony
16 ACAWC CLP-Calciun, Total (Ca)
17 ACOWC CLP Cobalt, Total (Co)
18 ACUWC CLP Copper, Total (Cu)
19 AFE\JC CLP Iron
20 APBWC CLP Lead
21 AMGWC CLP Magnesiun
22 AHGWC CLP Mercury
23 AKIIC CLP Potassiun
24 AAGWC CLP Silver, Total (Ag)
25 ANAWC CLP Sodh.111 (Na)
26 ATLWC CLP Thallilrn (Tl)
27 AVWC CLP Vanadiun CV)
28 DPACK CLP Data Package Deliverable
30 ABAWC CLP -Bariun, Total
COMMENTS: Continued on next page.
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
Decerrber 04, 1996
Report No.: 00056911
Section A Page 10
Lt MS Cll ENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
1.
0719 0641
661015501
000592
VERBAL
14-0CT-96 1455
16-0CT ·96
Katren Jenkins
RESULT UNITS
offl ine
offl ine
6.2 mg/L
48.7 * ug/l
45.0 * Ug/l
185 * ug/L
17,000 • ug/l
449 * ug/L
468 • ug/L
33.8 * ug/L
6.1 * ug/l
2,03_0 • ug/L
95.7 * ug/L
355,000 • ug/L
438 * ug/L
234 * ug/L
13,800 * ug/L
17.9 * ug/L
117,000 • ug/L
2.0 * ug/L
22,500 • ug/L
40.6 • ug/L
123,000 • ug/L
34.2 * ug/L
490 * ug/L
Done
3,450 • ug/l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Anatytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
LN
Pace Analytical
CLIENT NAME:
SAMPLE ID:
SAMPLE NO:
TEST
CODE
LABORATORY ANALYSIS REPORT
NATIONAL STARCH & CHEMICAL COMPANY
92 069831.2/ EX·02 MATRIX
H437848
DETERMINATION
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, Tl( 77058
Tel: [phone]
Fax: [phone]
Decerrber 04, 1996
Report No.: 00056911
DILUTION
FACTOR
Section A Page 11
RESULT UNITS
COMMENTS: • The matrix spike recoveries are as follows:
AlllTlinun = 96.2 %
Antimony= 95.7 %
Arsenic = 84.5 %
BarillTl = 104.0 %
Berylliun = 97.4 %
CaCITliun = 90.0 %
Calciun = 75.0 %
Chromiun = 84.0 %
Cobalt= 87.6 %
Copper= 93.6 %
Iron= 80.0 %
Lead= 89.5 %
Magnesiun = 85~0 %
Manganese= ---••
Mercury= 100.0 %
Nickel = 89.8 %
Potassiun = 96.6 %
Seleniun = 61.0 % ***
Silver= 81.2 %
Sodiun = 75.0 %
Thalliun = 68.4 % ***
Vanadiun = 96.8 %
Zinc = 88.0 %
**The concentration of ~he analyte prevented accurate determination of the
matrix spike recovery.
***Recovery of the matrix spike indicates the presence of a matrix interference.
This should be considered in evaluating the data.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
I
I
Deceni:ier 04, 1996 I
Report No.: 00056911
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P_Q. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069832.0/ EX-02 OUP.
SAMPLE NO: H437849
SAMPLE MATRIX: WATER
Section A Page 12
I LIHS CLIENT: 0719 0641
PACE PROJECT: 661015501
PACE CLIENT: 000592
P.O. NO: VERBAL I
DATE SAMPLED: 14-0CT-96 1505
DATE RECEIVED: 16-0CT-96
PROJECT MANAGER: Katren Jenkins I
·----------------------------------------------------------·-------------------------------------------------------------------1
TEST D 1 LUTlON
LN COOE OETERM I NAT I ON FACTOR RESULT UN ITS
OVTWC
2 OSTWC
3 1435
6 ABEWC
7 ACDWC
8 ACRWC
9 AMNWC
10 ANIWC
11 AZNWC
12 AASWC
13 ASEWC
14 AALWC
15 ASBWC
16 ACAWC
17 ACO\IC
18 ACUWC
19 AfEWC
20 APBWC
21 AMGWC
22 AHGWC
23 AKWC
24 AAGWC
25 ANAWC
26 ATLWC
27 AVWC
28 DPACK
30 ABAWC
COMMENTS:
TCL -VOA+ CLP Data Package Water
Data Package -VOA
TCL -BNA + CLP Data Package Water
Date Package -BNA
Nitrogen, Kjeldahl (N)
CLP Beryl l iLITI, Total (Be)
CLP Beryl l iun, Total
CLP caaniun, Total (Cd)
CLP Chromi un, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenillll
CLP Alllllinun, Total (Al)
CLP Antimony
CLP-CalCillTI, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (CU)
CLP Iron
CLP Lead
CLP Magnesii.in
CLP Mercury
CLP PotassillTI
CLP Silver, Total (Ag)
CLP SodhJ'll (Na)
CLP Thalliun (Tl)
CLP Vanadilltl (V)
CLP Data Package Deliverable
CLP· Barilln, Total
Continued on next page.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
without the written consent of Pace Analytical Services, Inc.
off line
offl ine'
6.0 mg/L
0.3 u * ug/L
4.8 U * ug/L
16.6 * ugtl
17,000 * ug/l
15.3 U ug/l
28.7 * ug/L
1.1 u * ug/l
0.8 U * ug/L
93.2 B * ug/L
4.3 u * ug/L
345,000 * ug/L
4.6 U * ug/l
6.4 U * ug/L
13,000 * ug/L
0.8 U * ug/L
101,000 * ug/L
0.2 u * ug/L
3,270 B * ug/L
8.4 U * ug/L
108,000 * ug/L
1.6 U * ug/L
5.4 B ug/L
Done
1,390 * ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
LN
pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
SAMPLE ID: 92 069832.0/ EX-02 DUP.
SAMPLE NO: H437849
TEST
COOE DETERMINATION
COMMENTS: * The relative percent differences are as follows:
Alllllim.m = 12.9
Antimony= ---
Arsenic = ---
Bariun = 1 .4
Beryl l iun = ---
CaCITliun = ---
Catciun = 1.5
Chromiun = 3.0
Cobalt= ---
Copper= ---
Iron= 0.0
Lead= ---
Magnesiun = 1.0
Manganese= 1.2
Mercury = ---
Nickel = ---
Potassillll = 3.1
Seleniun = ---
Silver = ---
Sodiun = 0.0
Thalliun =
Vanadiun = 12.2
Zinc= 1.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056911
DILUTION
FACTOR
Section A Page 13
RESULT UNITS
Pace Analytical
/·
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069834.7/ EX-03
SAMPLE NO: H437851
SAMPLE MATRIX: WATER
LN
2
3
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
CODE
OVTWC
OSTWC
1435
ABEWC
ACDWC
ACRWC
AMNWC
ANIWC
AZNWC
AASWC
ASEWC
AALWC
ASBWC
ACAWC
ACOWC
ACUWC
AFEWC
APBWC
AMGWC
AHGWC
AKWC
AAGWC
ANAWC
ATLWC
AVWC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package Water
Data Package -VOA
TCL -BNA + CLP Data Package Water
Data Package -BNA
Nitrogen, Kjeldahl (N)
CLP Berylliun, Total (Be)
CLP Berylliun, Total
CLP caaniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP ManganeSe
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Aluninun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP -Magnesiun
CLP -Mercury
CLP -Potassiun
CLP -Silver, Total (Ag)
CLP Sodiun (Na>
CLP -Thalliun (Tl)
CLP -Vanedilin (V)
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056911
Section A Page 15
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1720
16-0CT-96
Katren Jenkins
RESULT UN I TS
off line
offline
1 . 2 mg/L
0.3 u ug/L
4.8 U ug/L
62.6 ug/L
3,920 ug/L
81.6 ug/l
34.0 ug/L
1.1 U ug/l
0.8 U ug/l
78.4 B ug/L
4.3 U ug/L
168,000 ug/L
4.6 U ug/l
6.4 U ug/L
4,300 ug/L
0.8 U ug/L
29,400 ug/L
0.2 U ug/L
2,280 B ug/L
8.4 u ug/L
28,400 ug/L
1.6 U ug/L
3.9 U ug/L
Done
349 ug/L
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069833.9/ EX-04
SAMPLE NO: H437850
SAMPLE MATRIX: \./ATER
LN
2
3
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
CODE
ovn,c
OST\.IC
1435
ABE\.IC
ACD\.IC
ACRWC
AHNIJC
ANIWC
AZNWC
AASIJC
ASEWC
AALWC
ASBWC
ACAWC
ACOWC
ACUWC
AFE\JC
APBWC
AHGWC
AHGWC
AKWC
AAGWC
ANAWC
ATLWC
AVIIC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package \.later
Data Package -VOA
TCL · BNA + CLP Data Package \.later
Data Package -BNA
Nitrogen, Kjeldahl (N)
CLP Beryl l iun, Total (Be)
CLP Beryl l i Lill, Total
CLP CaCl'lliun, Total (Cd)
CLP Chromllin, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Al uni nun, Total (Al)
CLP Antimony
CLP-Calcillll, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Pot ass i lll1
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thalliun (Tl)
CLP Vanadiun CV>
CLP Data Package Deliverable
CLP -Baril.lTI, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: [phone]
Decent>er 04, 1996
Report No.: 00056911
section A Page 14
LIHS CLIENT: 0719 0641
PACE PROJECT: 661015501
PACE CLIENT: 000592
P.O. NO: VERBAL
OATE SAMPLED: 14·0CT·96
DATE RECEIVED: 16·0CT·96
PROJECT MANAGER: Katren Jenkins
DILUTION
FACTOR RESULT UNITS
off line
offl ine
1.2 mg/L
0.3 u ug/L
4.8 U Ug/L
4.9 U ug/l
3,340 ug/l
15.3 U ug/L
109 ug/L
,_ 1 u ug/l
0.8 U ug/l
84. 1 B ug/l
4.3 u ug/l
124,DOO ug/L
18.4 B ug/l
6.4 U ug/l
2,180 ug/l
D.8 U ug/L
29,600 ug/L
0.2 U ug/L
2,470 B ug/L
8.4 U ug/L
14,200 ug/L
1.6 u ug/L
3.9 U ug/L
Done
61.5 B ug/l
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID: 92 069835.5/ EX-01
SAMPLE NO: H437852
SAMPLE MATRIX: UATER
LN
2
3
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
30
TEST
CODE
OVTWC
OSTWC
1435
ABEWC
ACDWC
ACRWC
AMN\.IC
ANIWC
AZNWC
AASWC
ASEWC
AAUJC
ASBWC
ACAWC
ACOWC
ACU\IC
AFEWC
APBWC
AMGWC
AHG\JC
AK\IC
AAGWC
ANA\JC
ATLWC
AVWC
DPACK
ABAWC
DETERMINATION
TCL -VOA+ CLP Data Package 'water
Data Package -VOA
TCL -BNA + CLP Data Pack.age \.later
Data Package -BNA
Nitrogen, Kjeldahl (N)
CLP Beryll iun, Total (Be)
CLP Berylliun, Total
CLP Cactniun, Total (Cd)
CLP Chromiun, Total (Cr)
CLP ManganeSe
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Seleniun
CLP Al uni nun, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesiun
CLP Mercury
CLP Potassiun
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thalli"'1 (Tl)
CLP Vanadiun CV)
CLP Data Package Deliverable
CLP -Bariun, Total
Pace Analytical Services, Inc.
900 Gemini Avenue
Houston, TX 77058
Tel: [phone]
Fax: 71:J.188.4661
December 04, 1996
Report No.: 00056911
Section A Page 16
LIMS CLIENT:
PACE PROJECT:
PACE CL I ENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661015501
000592
VERBAL
14-0CT-96 1700
16-0CT-96
Katren Jenkins
RESULT UNITS
off line
off line
< 0.1 mg/L
0.3 U ug/L
4.8 U ug/L
4.9 U ug/L
205 ug/L
15.3 U ug/L
33.9 ug/L
,. 1 u ug/L
0.8 U ug/L
119 B ug/L
4.3 U ug/L
89,700 ug/L
4.6 u ug/L
6.4 U ug/L
61.3 B ug/L
0.8 U ug/L
9,310 ug/L
0.2 U ug/L
1,630 8 ug/L
8.4 U ug/L
10,900 ug/L
1.6 U ug/L
3.9 U ug/L
Done
126 8 ug/L
REPORT OF LABORATORY ANALYSIS
Thia report shall not be reproduced, except in full,
without the written consent of Pace Anatytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
,I
I
I
I
Appendix D
lnorganics Analysis Data Sheets
Trench Area Wells
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
CLIENT NAME:
ADDRESS,
ATTENTION:
SAMPLE JO:
SAMPLE NO:
SAMPLE MATRIX:
LN
TEST
CODE
LA80BAT08Y ANAi YSIS REPORT
NA T,I ONAL ST ARCH & CHEM I CAL COMPANY
p_Q_ BOX 399
SALISBURY, NC 28145-0399
MR. KEN KLUTTZ
92 069360.4/ EX-05
H437572
~ATER
DETERMINATION
Pace Analytical Services. Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
section A Page 1
LIMS CLIENT:
PACE PROJECT:
PACE CL I ENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
0 I LUT !ON
FACTOR
0719 0641
661008504
000592
VERBAL
07-0CT·96
09-0CT-96
Katren Jenkins
RESUL i UN I TS -------------------------------------------------------------------------------------------------------------------------------
OVTWC TCL -VOA+ CLP Data Package· Water Data Package VOA
Data Package -VOA
Data Package· VOA 2 OST\JC TCL · BNA + CLP Data Package· Yater
3 !435
6 ABEUC
7 ACDUC
8 ACRI.JC
9 AMN\JC
10 ANl~C
11 AZN~C
12 AAS\JC
13 ASEUC
14 AAL~C
15 ASB\JC
16 ACA~C
17 ACOUC
18 ACUUC
19 AFEUC
20 APBUC
21 AMG\JC
22 AHG\JC
23 AK~C
24 AAGUC
25 ANAUC
26 ATL~C
27AVIIC
26 DPACK
28 OPACK
30 ASAI.JC
COMMENTS:
Data Package· BNA
Nitrogen, Kjeldahl (N)
CLP Beryllium, Total (Be)
CLP Beryllium, Total
CLP Cadmium, Total (Cd)
CLP Chromium, Total (Cr) CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenium
CLP Aluminum, Total (Al) CLP Antimoriy
CLP-CalciLITl, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu}
CLP Iron
CLP Lead
CLP Magnesium
CLP Mercury
CLP PotassillTI
CLP Silver, Total (Ag) CLP Sodiun (Na)
CLP Thallium (Tl)
CLP Vanadilml (V)
CLP Data Package Deliverable
CLP Data Package Deliverable
CLP -Barillll, Total
Continued on next page.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
60
1
1
1
20
1
1
4
4
1
1
20'
1
1
1
2
1
1
1
1
20
4
off line
off line
420
0.3 u
6.8
26.2
144,000
654
220
4.4 U "
5. 2 u ,.
78.2 U
4.3 U
1,270,000
1,240
651
1,210
1 .6 U ,.
484,000
0.2 u
20,000
16.5
6,470,000
6.4 U,.
3.9 U
Done
157 B
mg/L
ug/L
ug/l
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Pace Analytical
LABORATORY ANALYSIS REPORT
~-ctiENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
LN
SAMPLE JO: 92 069360.4/ EX·OS
SAMPLE NO: H437572
TEST
COOE DETERMINATION
COMMENTS: • The sample required dilution due to matrix interferences ~hich resulted in
a higher detection limit for Thallium, Lead, Arsenic and Selenium.
Analysis performed by Pace Analytical Services, Inc., Houston, Texas.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 2
O[LUTION
FACTOR RESULT UNITS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1----
I
I
I
I
I
Pace Analytica·1
lABOBATOBY ANAtYSJS REPORT
CLIENT NAME:
ADDRESS:
NATIONAL STARCH & CHEMICAL COMPANY
P.O. BOX 399
ATTENTION:
SAMPLE ID:
SAMPLE NO:
SAMPLE MATRIX:
SALISBURY, NC 28145-0399
MR. KEN KLUTTZ
92 069361.2/ EX-06
H437573
UATER
LN
TEST
CODE DETERMINATION
OVT\.IC TCL -VOA+ CLP Data Package I.Jater
Data Package -VOA
_<.....J)1TUC . TCL · BNA + CLP Data Package \,later
Data Package· BNA
3 1435 Nitrogen, Kjeldahl C N l
6 ABEUC CLP Beryl l iun, Total (Be)
CLP Beryl L ium, Total
'7 ACOUC CLP Cadmium, Total (Cd)
8 ACRWC CLP Chromium, Total (Cr)
9 AMNWC CLP Manganese
10 ANIUC CLP Nickel
11 AZNWC CLP Zinc
12 AASWC CLP Arsenic, Total (As)
13 ASEWC CLP Selenium
14 AALWC CLP Aluminum, Total (Al)
15 ASBWC CLP Antimony
16 ACAUC CLP·Calciun, Total (Ca)
17 ACOWC CLP Cabal t, Total (Co)
18 ACUUC CLP Copper, Total (Cu)
19 AFEUC CLP Iron
20 APBWC CLP Lead
21 AMGWC CLP Magnesium
22 AHGUC CLP Mercury
23 AKUC CLP Potassium
24 AAGUC CLP Silver, Total (Ag)
25 ANA\.IC CLP Sodium (Na)
26 ATLWC CLP Thallium (Tl)
27 AVUC CLP Vanadium (V)
28 □PACK CLP Data Package Deliverable
30 ABAWC CLP· Barium, Total
COMMENTS: Analysis performed by Pace Analytical Services, lnc., Houston, Texas.
Pace Analytical Services, lnc.
9800 Kincey Avenue, Suite 100
· Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 3
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
DATE SAMPLED:
DATE RECEIVED:
PROJECT MANAGER:
DILUTION
FACTOR
0719 0641
661008504
000592
VERBAL
07-0CT-96
09-0CT-96
Katren Jenkins
RESULT UN I TS
off line
offl ine
1. 2 mg/L
0.3 U ug/L
4.8 U ug/l
4.9 U ug/L
3,620 ug/L
15.3 U ug/L
2.4 u ug/L
1. 1 u ug/l
1.3 u ug/L
129 B ug/L
4.3 U ug/L
36,400 ug/L
4.6 U ug/L
6.4 U ug/L
3,310 ug/L
1.0 B ug/L
17,800 ug/L
0.2 U Ug/l
1, 190 B ug/l
8.4 U ug/L
130,000 ug/l
1.6 U ug/L
3.9 U ug/l
Done
107 B ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANA!YSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
___ AJ.TENUON: MR. KEN KLUTTZ
SAMPLE IO: 92 069362.0/ EX-07
SAMPLE NO: H437574
SAMPLE MATRIX: WATER
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 4
LIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
0719 0641
661008504
000592
VERBAL
DATE SAMPLED: 07·0CT·96
DATE RECEIVED: 09·0CT·96
PROJECT MANAGER: Katren Jenkins
I
I
I
I
I
. :~ _ .. _ ~~~~ _ ... ____ . ______ . ___ . __ .. _. D:TERM 1 •~TI~~. ____ ._ ............... _ .... ___ ...... _. __ D '.~~;bt __ .. ___ •:~~: T .. UN 1 '.s __ .. __ ... I
OVTUC
2 OSTUC
3 1435
6 ABEUC
7 ACOWC
8 ACRUC
9 AMNUC
10 ANIUC
11 AZNUC
12 AAS\JC
13 ASEUC
14 AALUC
15 ASBUC
16 ACA\JC
17 ACO\JC
18 ACUUC
197\FEUC-
20 APB\JC
21 AMGUC
22 AHGUC
23 AKUC
24 AAGUC
25 ANAUC
26 ATLUC
27 AVIIC
28 DPACK
30 ABAUC
COMMENTS:
TCL -VOA+ CLP Data Pnckage Water
Data Package -VOA
TCL -BNA ♦ CLP Data Package Uater
Data Package -BNA
Nitrogen, Kjeldahl (N)
CLP Beryllium, Total (Be)
CLP Beryllium, Total
CLP Cadmium, Total (Cd)
CLP Chromium, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenium
CLP Aluminum, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesium
CLP Mercury
CLP Potassium
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thalliun (Tl)
CLP Vanadiun CV)
CLP Data Package Deliverable
CLP -Bariun, Total.
Continued on next page.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, lnc.
off line I
off line
16 mg/l
1 0.3 U ug/L
1 4.8 u ug/L I
1 16.9 ug/L
5 60,400 ug/l
1 91. 1 ug/L
1 20.1 ug/L I
1 1. 1 u ug/L
1 1.3 u ug/L
1 113 8 ug/L
1 4.3 U ug/L
5 673,000 ug/L I
1 397 ug/L
1 35.9 ug/L
1 10,600 ug/l
1 5.3 ug/l I
1 285, DOO ug/l
1 0.2 U ug/L
1 5,670 ug/L
1 8.4 U ug/L
5 665,000 ug/L I
2 3.2 U * ug/L
7.6 8 ug/L
Done
319 ug/L I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANA\YSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
SAMPLE ID, 92 D69362.0/ EX-07
SAMPLE NO, H437S74
Pace Analytical Seivices, lnc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 5
······---····-··---------------------------------------------------------------------------------------------------------------
I
I
I
I
I
I
I
I
I
1--
I
I
I
I
D
LN
TEST
CODE DETERMINATION
COMMENTS: • The sample required dilution due to matrix interferences which resulted in
a higher detection limit for Thallium.
Analysis performed by Pace Analytical Services, Inc., Houston, Texas.
DILUTION.
FACTOR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
RESULT UNITS
CLIENT NAME:
ADDRESS:
---Ar.TE NT.l ON:
SAMPLE ID:
SAMPLE NO:
NATIONAL STARCH & CHEMICAL P .0. BOX 399
SALISBURY, NC 28145-0399 MR. KEN KLUTTZ
92 069363.9/ EX-08
H437575
LABOBATORY ANA!XSIS REPORT
COMPANY
I Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 1 DO
Huntersville, NC 280781
Tel: [phone]
Fax: [phone]
December 04, 1996 Report No.; 00056890
Section A Page 6
lIMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P.O. NO:
0719 0641
661008504
000592
VERBAL
I
I
'.~'.C, • ,., " ~ "" '"'."C, ""'."'" "'"'. '.-•• I TEST
DILUTION LN COOE DETERMINATION
FACTOR RESULT UNITS
DA TE SAMPLED:
DATE RECE I VEO:
07-0CT ·96
09·0CT·96 I
.............................................................................
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
.
•

1 OVTUC TCL ·VOA+ CLP Data Package -Water Data Package -VOA 2 OSTUC TCL -BNA • CLP Data Package -Water Data Package -BNA 3 1435
6 ABEWC
7 ACOWC
8 ACRWC
9 AMNWC
10 ANIWC
11 AZNWC
12 AASWC
13 ASEWC
14 AALWC
15 ASBWC
16 ACAWC
17 ACOIIC
18 ACUWC
T9"°AFEWC
20 APBWC
21 AMGWC
22 AHGWC
23 AK\IC
24 AAGWC
25 ANAWC
26 ATLWC
27 AV\IC
28 OPACK
30 ABAWC
Nitrogen, Kjeldahl (N) CLP Beryllit.m, Total (Be) CLP Beryllium, Total CLP Cadmium, Total {Cd) CLP Chromium, Total (Cr) CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As} CLP Selenium
CLP Aluminum, Total (Al) CLP Antimony
CLP-CalcilJll,' Total (Ca) CLP Cobalt, Total (Co) CLP Copper, Total (Cu) CLP I ran
CLP Lead
CLP Magnesium
CLP Mercury
CLP Potassium
CLP Silver, Total (Ag) CLP Sodium (Na)
CLP Thallium (Tl)
CLP Vanadium (V)
CLP Data Package Deliverable CLP -Bariun, Total·
COMMENTS: Continued on next page.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services. Inc
50
1
1
1
20
1
1
2
4
1
1
20
1
1
1
2
1
1
1
1
20
2
1
off line
offl ine
230 mg/L
20,6
15.5
79.8
332,000
1,350
1,690
2.2 U *
5 .2 U *
74,200
4.3 U
576,000
6,080
1,060
30,400
1.6 U *
369,000
0.2 u
20,800
42.2
5,640,000
3.2 U *
10.4 B
Done
29.1 B
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
UQ/L
ug/L
ug/L
ug/L
ug/L
ug/L
Ug/L
ug/L
ug/L
Ug/L
ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I-
I
I
I
I
I
LN
Pace Analytical
LABORATORY ANAi YS!S REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
SAMPLE ro: 92 069363.9/ EX-08
SAMPLE NO: H437575
TEST
CODE DETERMINATION
COMMENTS: * The sample required dilution due to matrix lnterferences which resulted in
a higher detection limit for Thallium, Lead, Arsenic and Selenium.
Analysis performed by Pace Analytical Services, Inc., Houston, Texas.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 7
OllUTION
FACTOR RESULT UNITS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145-0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE IO: 92 069364.7/ EX-09
SAMPLE NO: H437576
SAMPLE MATRIX: WATER
LN
2
3
6
7
8
9
10 ,,
12
13
14
15
16
17
18
TEST
CODE
OVTw'C
OST'i./C
1435
ABEWC
ACOWC
ACRWC
AMNWC
ANIWC
AZNWC
AASWC
ASE\JC
AALIJC
ASBWC
ACAWC
ACOWC
ACU\JC
W---MEWC·-
20 AP8WC
21 AMGWC
22 AHGWC
23 AKWC
24 AAGWC
25 ANAWC
26 ATLWC.
27 AVWC
28 OPACK
30 ABAWC
COMMENTS:
DETERMINATION
TCL -VOA+ CLP Data Package 'water
Data Package -VOA
TCL -BNA + CLP Data Package 'water
Data Package -BNA
~itrogen, Kjeldahl (N)
CLP Beryl l iun, Total (Be)
CLP Beryllillll, Total
CLP Cadmium, Total (Cd)
CLP Chromium, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenium
CLP Aluminum, Total (Al)
CLP Antimony
CLP-CalcillTI, Tdtal (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP · Iron
CLP Lead
CLP Magnesium
CLP Mercury
CLP Potassium
CLP Silver, Total (Ag)
CLP SodiLrn (Na}
CLP Thallium (Tl)
CLP VanadillTI (V)
CLP Data Package Deliverable
CLP -BariLrn, Total-
Continued on next page.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 8
LIMS CLIENT:
PACE PROJECT:
PACE Cl! ENT:
P.O. NO:
0719 0641
661008504
000592
VERBAL
DATE SAMPLED: 07-0CT-96
DATE RECEIVED: 09-0CT-96
PROJECT MANAGER: Katren Jenkins
DILUTION
FACTOR
50
1
1
20
1
' 4
1
1
2
1
1
1
1
20
2
RESULT UNITS
off line
offl ine
380 mg/L
25 .6 ug/L
8,4 ug/L
63.5 ug/L
170,000 ug/L
906 ug/L
2,850 ug/L
4.4 U * ug/L
5 .2 u * ug/l
114,000 ug/L
4.3 U ug/L
321,000 ug/L
4,540 ug/L
1,030 ug/L
18,800 ug/L
1.6 u * ug/L
109,000 ug/L
0.2 u ug/l
15,100 ug/L
20.2 ug/L
,, 760,000 ug/L
3.2 U * ug/L
15.6 B ug/l
Done
17. 1 B ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
--Pace Analytical
LN
LABORATORY ANA!YSJS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
SAMPLE ID: 92 069364_7/ EX-09
SAMPLE NO: H437S76
TEST
CODE DETERMINATlON
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 9
DlLUTION
FACTOR RESULT UNITS --------··············---------------------------------------------------------------------------------------------------------
COMMENTS: * The sample required dilution due to matrix interferences which resulted in
a higher detection limit for Thallium, Lead, Arsenic and Selenium.
Analysis performed by Pace Analytical Services, Inc., Houston, Texas.
·--., ----
,--
I
I
I
I REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
LABORATORY ANAIYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
ADDRESS: P.O. BOX 399
SALISBURY, NC 28145·0399
ATTENTION: MR. KEN KLUTTZ
SAMPLE ID:
SAMPLE NO:
92 069365.5/ EX-10
H437577
SAM?L-E MATRIX: YATER
LN
2
3
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
TEST
CODE
OVTYC
OSTYC
1435
ABEUC
ACOYC
ACRYC
AMNUC
ANIUC
AZNUC
AASUC
ASEUC
AALUC
ASBUC
ACAUC
ACOUC
ACUUC
AFE~C
APB~C
AMGYC
?2.....,l_l[GYC
23 AK\.IC
24 AAGUC
25 ANAUC
26 ATLUC
27 AWC
28 DPACK
30 ABAUC
COMMENTS:
DETERMINATION
TCL -VOA+ CLP Data Package \Jater
Data Package -VOA
TCL -BNA + CLP Data Pack.age \Jater
Data Package -SNA
Nitrogen, Kjeldahl (N1
CLP Beryllium, Total (Be)
CLP Beryllium, Total
CLP Cadmium, Total (Cd)
CLP Chromium, Total (Cr)
CLP Manganese
CLP Nickel
CLP Zinc
CLP Arsenic, Total (As)
CLP Selenium
CLP Aluminum, Total (Al)
CLP Antimony
CLP-Calciun, Total (Ca)
CLP Cobalt, Total (Co)
CLP Copper, Total (Cu)
CLP Iron
CLP Lead
CLP Magnesium
CLP .Mercury
CLP Potassium
CLP Silver, Total (Ag)
CLP Sodiun (Na)
CLP Thalliun (Tl)
CLP Vanadium (V)
CLP Data Package Deliverable
CLP -Barii.in, Total.
Continued on next page.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel· 704-875-9092
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 10
LJMS CLIENT:
PACE PROJECT:
PACE CLIENT:
P .0. NO:
DATE SAMPLED:
DATE RECE 1 VED:
PROJECT MANAGER:
DILUTION
FACTOR
25
1
1
1
20
1
1
2
2
1
1
1
1
1
1
1
1
1
1
20
1
1
0719 0641
661008504
000592
VERBAL
07-0CT-96
09-0CT-96
Katren Jenkins
RESULT UNITS
off line
offline
160 mg/l
18.8 ug/l
4.8 U ug/l
46.5 ug/l
138,000 ug/l
505 ug/l
2, 120 ug/l
2.2 u • ug/l
2.6 U * ug/l
74,400 ug/L
4.3 U ug/L
378,000 ug/L
3,420 ug/l
799 ug/L
22,600 ug/L
0.8 U ug/l
176,000 ug/l
0.2 u ug/L
16,800 ug/l
17.7 ug/l
3,620,000 ug/L
1.6 U ug/l
15 .8 B ug/l
Done
21 .4 B ug/l
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Pace Analytical
LABORATORY ANALYSIS REPORT
CLIENT NAME: NATIONAL STARCH & CHEMICAL COMPANY
SAMPLE IO: 92 069365.5/ EX-10
SAMPLE NO: H4375TT
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section A Page 11
-------------------------------------------------------------------------------------------------------------------------------
LN
TEST
CODE DETERMINATION
DILUTION
FACTOR RESULT UN I TS -------------------------------------------------------------------------------------------------------------------------------
COMMENTS: • The sample required dilution due to matrix interferences ~hich resulted in
a higher detection limit for Arsenic and Selenium.
Analysis performed by Pace Analytical Services, Inc., Houston, Texas.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
SUPPLEMENTAL INFORMATION
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 000S6890
Section B Page 1
-------------------------------------------------------------------------------------------------------------------------------
SAMPLE ID: 92 069360.4/ EX-05
1 OVTUC
22--A~GWC -
28 DPACK
2 OSTUC
3 1435
6 ABEWC
7 ACOIJC
8 ACRWC
9 AMN\JC
10 ANIWC
11 AZNWC
14 AALWC
t5 ASBWC
16 ACAWC
17 ACOWC
18 ACUWC
19 AFEWC
21 AMGWC
23 AKWC
24 AAGWC
25 ANAWC
27 AVWC
30 ABAI.JC
12 AASUC
13 ASEWC
20 APBUC
26 ATLWC
0
67977
0
67966
67884
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67905
67906
67906
67906
67906
0 NA
67977 NA
0 NA
67966 96
67884 02-351.2
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CL'
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 '47-CLP
67906 A6·CLP
67906 A6·CLP
67906 A6·CLP
67906 A6·CLP
SAMPLE ID: 92 069361.2/ EX-06
_1_0,Y.TUC
22 AHGWC
28 0PACK
2 OSTWC
3 1435
6 ABEWC
7 ACDWC
8 ACRWC
9 AMNWC
10 ANIWC
11 AZNWC
0
67977
0
67966
67884
67905
67905
67905
67905
67905
67905
0 NA
67977 NA
0 NA
67966 96
67884 02-351.2
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
67905 47-CLP
11·0CT·96 0900 RDQ
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16·0CT·96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16·0CT·96 1015 SAO
16-0CT-96 1020 SAO
16-0CT-96 1020 SAO
16-0CT-96 1020 SAO
16-0CT-96 1020 SAO
11-0CT-96 0900 RDQ
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
16-0CT-96 1015 SAO
20-CLP
47-245.1
NA
20-CLPSW
02-351.2
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-204.2
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
A6-206.2
A6·270.2
47-239.2
47-279.2
20-CLP
47-245.1
NA
20-CLPSW
02-351.2
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
47-200.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
SAMPLE NO: H437572
17-0CT-96 0000 JC
17-0CT-96 1836 CCJ
03-0EC-93 0800 RM
04-NOV-96 1805 ASP
11-0CT-96 0900 AMC
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16·0CT·96 1922 CCJ
17-0CT-96 1849 CCJ
16·0CT·96 1922 CCJ
16-0CT-96 1922 CCJ
16·0CT·96 1922 CCJ
22-0CT-96 0843 GAB
17-0CT-96 1849 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
17-0CT-96 1849 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
21-0CT-96 05~8 GAB
21·0CT·96 1053 GAB
22-0CT-96 0420 GAB
24-0CT-96 0327 GAB
SAMPLE NO:
17-0CT-96 0000 JC
17-0CT-96 1836 CCJ
03-DEC-93 0800 RM
04-NOV-96 1137 ASP
11-0CT-96 0900 AMC
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
16-0CT-96 1922 CCJ
GC:-!SY
1 OOMET
GCMSZ
303UAT
?COMET
700MET
700MET
700MET
?COMET
700MET
700MET
405MET
700MET
700MET
700MET
700MET
700MET
700MET
700MET
700MET
700MET
700MET
405MET
405MET
405MET
405MET
H437573
GCMSY
100MET
GCMSZ
303\JAT
700MET
700MET
700MET
700MET
700MET
700MET
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078 •-Pace Analytical
Tel: [phone]
Fax: [phone]
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SUPPIEMENTAL !NFOBMATION
December 04, 1996
Report No.: 00056890
Section B Page 2
---------------------------------------------------------·········-------------------------------------------------------------
LN
TEST
COOE
LCSR
BLNK
BATCH
DUP/MS
MS/MSD
BATCH LR-METHOD
SAMPLE PREPARATION ······-······
DATE/Tl ME ANALYST LR-METHOD DATE/T !ME ANALYST ! NSTRUMEMT ----------------------------------------------------------------------------------------------------········-------------------
SAMPLE ID: 92 069361.2/ EX-06 SAMPLE NO: H437573
14 AAU./C 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET 15 ASB\./C 67905 67905 4 7-CLP 16-0CT-96 1015 SAO 47-204.2 22-0CT-96 0843 GAB 405MET 16 ACA'wC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET 17 ACOI.JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET 18 ACUUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET 19 AFE\JC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200. 7 16-0CT-96 1922 CCJ 700MET 21 AMG\JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200. 7 16-0CT-96 1922 CCJ 700MET
23 AKUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
24 AAGIJC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
25 ANAUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
27 AVIIC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
30 ABAIJC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
12 AASIJC 67906 67906 A6-CLP 16-0CT-96 1020 SAO A6·206.2 21-0CT-96 0548 GAB 405MET
13 ASEUC 67906 67906 A6-CLP 16-0CT-96 1020 SAO A6·270.2 21 ·0CT-96 1053 GAB 405MET
20 APBIJC 67906 67906 A6·CLP 16-0CT-96 1020 SAO 47-239.2 22 ·0CT · 96 0420 GAB 405MET
26-AfLUC -67906 67906 A6-CLP 16·0CT·96 1020 SAO 47-279.2 24-0CT-96 0327 GAB 405MET
SAMPLE ID: 92 069362.0/ EX-07 SAMPLE NO: H437574
1 OVT\JC 0 0 NA 20-CLP 17·0CT·96 0000 JC GCMSY
22 AHGUC 67977 67977 NA 47-245.1 17-0CT-96 1836 CCJ 100MET
28 OPACK 0 0 NA NA 03-0EC-93 0800 R M
2 OST\JC 67966 67966 ' 96 11-0CT-96 0900 ROO 20-CLPSU 04-NOV-96 1512 ASP GCMSZ 3 1435 67884 67884 02-351.2 02-351.2 11-0CT-96 0900 AMC 303UAT 6 ABE\JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
7 ACDUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
8 ACRUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200. 7 16·0CT·96 1922 CCJ 700MET
9 AMNUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 17-0CT-96 1849 CCJ 700MET
10 ANIUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
11 AZNUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET 14 AAL\JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET 15 ASBUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-204.2 22 ·OCT· 96 0843 GAB 405MET
16 ACAUC. 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 17-0CT-96 1849 CCJ 700MET
17 ACO\IC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
18 ACUUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
19 AFEUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
21 AMG\JC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET 23 AICUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET 24 AAGUC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16·0CT·96 1922 CCJ 700MET
25 ANAUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7 17-0CT-96 1849 CCJ 700MET 27 AVIIC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7 16-0CT-96 1922 CCJ 700MET
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Analytical 9800 Kincey Avenue, Sutte 100
eace Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
Oecenber 04, 1996
Report No.: 00056890
Section B Page 3
SUPPLEMENTAL I NFOBMAT! ON
... -.. -. --. ---------.. -------. -.. -. -------------. -------------------------------------... ------------------·. - - -----... -
LCSR OUP/MS -----------. -SAMPLE PREPARATION ····------··· ·············· SAMPLE ANALYSfS ··············-
TEST BLNK MS/MSO
LN CODE BATCH BATCH LR·METHOO DATE/If ME ANALYST LR-METHOD DATE/TIME ANALYST INSTRUMENT
... --. --. -... -. -... -----. --------------. -.. ----... ----. ------. -----. ------. -----. -------. ----------.... --....... ---. -. -. -. -. --.
SAMPLE ID: 92 069362.0/ EX-07
30 ABAWC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
12 AASWC 67906 67906 A6·CLP 16-0CT-96 1020 SAO A6·206.2
n-Jt~Euc·· 67906 67906 A6·CLP 16-0CT-96 1020 SAO A6·270.2
20 APBWC 67906 67906 A6·CLP 16-0CT-96 1020 SAO 47-239.2
26 ATLWC 67906 67906 A6·CLP 16-0CT-96 1020 SAO 47-279.2
SAMPLE ID: 92 069363.9/ EX-OB
1 OVTUC 0 0 NA 20-CLP
22 AHGWC 67977 67977 NA 47-245.1
28 □PACK 0 0 NA NA
2 OSTWC 67966 67966 96 11·0CT·96 0900 ROO 20-CLPSW
3 f435 67884 67884 02-351.2 02-351.2
6 ABEUC 67905 67905 4 7-CL,· 16·0CT·96 1015 SAO 47-200.7
7 ACOWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
8 ACR\,/C 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
9 AMN\,/C 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
10 ANIWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200. 7
11 AZNWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
14 AALUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
15 ASBWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-204.2
16 ACAWC 67905 67905 4 7 · CLP 16·0CT·96 1015 SAO 47-200.7
17 ACO'wC 67905 67905 · 47-CLP 16·0CT·96 1015 SAO 47-200.7
18 ACUWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
19 AFEWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
21 AMGWC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200. 7
23 AK'wC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
24 AAG'wC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
25 ANA\,IC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
27 AWC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
30 ABA\olC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
.12....MSWC .. 67906 67906 A6·CLP 16·0CT·96 1020 SAO A6·206.2
13 ASEWC 67906 67906 A6·CLP 16-0CT-96 1020 SAO A6·270.2
20 APBWC 67906 67906 A6·CLP 16·0CT·96 1020 SAO 47-239.2
26 ATLWC 67906 67906 A6·CLP 16-0CT ·96 1020 SAO 47-279.2
SAMPLE ID: 92'069364.7/ EX-09
1 OVTWC 0 0 NA 20-CLP
22 AHG\olC 67977 67977 NA 47-245.1
28 DPACK 0 0 NA NA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
SAMPLE NO: H437574
16-0CT-96 1922 CCJ ?COMET
21·0CT·96 0548 GAB 405MET
21-0CT-96 1053 GAB 405MET
22-0CT-96 0420 GAB 405MET
24·0CT·96 0327 GAB 405MET
SAMPLE NO: H437575
17-0CT-96 0000 JC GCMSY
17-0CT-96 1836 CCJ 100MET
03-0EC-93 0800 R M
04·NOV·96 1721 ASP GCMSZ
11·0CT·96 0900 AMC 303UAT
16·0CT·96 1922 CCJ ?COMET
16-0CT-96 1922 CCJ ?COMET
16·0CT·96 1922 CCJ ?COMET
17-0CT-96 1849 CCJ ?COMET
16-0CT-96 1922 CCJ ?COMET
16-0CT-96 1922 CCJ ?COMET
16·0CT·96 1922 CCJ 700MET
22-0CT-96 0843 GAB 405MET
17-0CT-96 1849 CCJ ?COMET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ ?COMET
16·0CT·96 1922 CCJ ?COMET
16·0CT·96 1922 CCJ 700MET
17-0CT-96 1849 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
21-0CT-96 0548 GAB 405MET
21-0CT-96 1053 GAB 405MET
22-0CT-96 0420 GAB 405MET
24·0CT·96 0327 GAB 405MET
SAMPLE NO: H437576
17·0CT·96 ODDO JC GCMSY
17-0CT-96 1836 CCJ 100MET
03-0EC-93 0800 R M
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
-1----
I
I
I
I
I
I
LN
TEST
COOE
SAMPLE ID:
2 OSTUC
3 1435
6 ABEUC
7 ACDUC
B ACRUC
9 AMN\.IC
10 ANIUC
11 AZNUC
14 AALUC
15 ASBUC
16 ACA\.IC
17 ACOUC
18 ACUUC
19 AFEI.IC
21 AMGWC
23 AKUC
24 AAGUC
25 ANA\JC
LCSR
BLNK
BATCH
OUP/MS
MS/MSO
BATCH
92 069364.7/ EX-09
67966 67966
67884 67884
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
67905 67905
96
02-351.2
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47-CLP
47·CLP
47-CLP
47-CLP
27_}//',,/C ·-67905 67905 47-CLP
I 30 ABAUC 67905 67905 47-CLP
12 AAS\JC 67906 67906 A6-CLP
13 ASEUC 67906 67906 A6·CLP
20 APBUC 67906 67906 ·A6-CLP
26 ATLUC 67906 67906 A6-CLP
I SAMPLE to: 92 069365.5/ EX·10
1 OVHIC 0 0 NA
I 22 AHG\.IC 67977 67977 NA
28 DPACK 0 0 NA
2 OSTUC 67966 67966 96
3 1435 67884 67884 02-351.2
6 ABEUC 67905 67905 47-CLP
I 7 ACDUC 67905 67905 47-CLP
8 ACRUC 67905 67905 47-CLP
9 AMNUC 67905 67905 47-CLP
10 ANIUC 67905 67905 47-CLP
I 11 AZNUC 67905 67905 47-CLP
14 AALUC 67905 67905 47-CLP
15 ASBUC 67905 67905 47-CLP
16 ACAUC 67905 67905 47-CLP
I
1-
I
I
SUPPLEMENTAL INFORMATION
DATE/TIME ANALYST LR-METHOD
11-0CT-96 0900 ROO 20-CLPSU
02-351.2
16-0CT-96 1015 SAO 47-200. 7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200. 7
16-0CT-96 1015 SAO 47-204.2
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200. 7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47·200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47·200.7
16-0CT-96 1020 SAO A6-206.2
16-0CT-96 1020 SAO A6·270.2
16·0CT ·96 1020 SAO 47-239.2
16-0CT-96 1020 SAO 47-279.2
20·CLP
47-245.1
HA
11-0CT-96 0900 ROO 20-CLPSU
02·351.2
16-0CT-96 1015 SAO 47-200,7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200. 7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200.7
16-0CT-96 1015 SAO 47-200. 7
16-0CT-96 1015 SAO 47-204.2
16-0CT-96 1015 SAO 47-200.7
Pace Analytical Services, lnc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section B Page 4
DATE/TIME ANALYST INSTRUMENT
SAMPLE NO: H437576
04-NOV-96 1555 ASP GCMSZ
11-0CT-96 0900 AMC 303UAT
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
17-0CT-96 1849 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
22 -OCT -96 0843 GAB 405MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
17-0CT-96 1849 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
21 ·0CT·96 0548 GAB 405MET
21-0CT-96 1053 GAB 405MET
22·0CT ·96 0420 GAB 405MET
24-0CT-96 0327 GAB 405MET
SAMPLE NO: H437577
17-0CT-96 0000 JC GCMSY
17-0CT·96 1836 CCJ 100MET
03-0EC-93 0800 R M
04-NOV-96 1220 ASP GCMSZ
11 ·0CT ·96 0900 AMC 303UAT
16-0CT·96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
17-0CT-96 1849 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
22-0CT-96 0843 GAB 405MET
16-0CT-96 1922 CCJ 700MET
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Pace Analytical
SUPPIEMENTAL INFORMAT!ON
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section B Page 5
-------------------------------------------------------------------------------------------------------------------------------
LCSR DUP/MS -------------SAMPLE PREPARATION ------------· --··········-· SAMPLE ANALYSIS ---------------
TEST BLNK MS/MSO
LN CODE BATCH BATCH LR-METHOD OATE/T !ME ANALYST LR-METHOD DATE/TIME ANALYST INSTRUMENT -------.. --------. ------------------- -------. -------. --.. ---- - -----------------------------------------------------------------
SAMPLE 10: 92 069365.5/ EX-10
17 ACO\JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
18 ACU\JC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
19 AFEWC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
21 AMG\JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
23 AKUC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47·200. 7
24--AAGWC·· 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
25 ANAi.JC 67905 67905 47-CLP 16·0CT·96 1015 SAO 47-200.7
27 AVWC 67905 67905 47·CLP 16·0CT·96 1015 SAO 47-200.7
30 ASAI.JC 67905 67905 47-CLP 16-0CT-96 1015 SAO 47-200.7
12 AASWC 67906 67906 A6-CLP 16-0CT-96 1020 SAO A6·206.2
13 ASEWC 67906 67906 A6·CLP 16-0CT·96 1020 SAO A6·270.2
20 APB\JC 67906 67906 A6·CLP 16-0CT-96 1020 SAO 47-239.2
26 ATLWC 67906 67906 A6-CLP 16-0CT-96 1020 SAO 47-279.2
LR Method Literature Reference
02 EPA-Methods for Chemical Analysis of Uater & \Jastes, 1984.
20 USEPA CLP SOU for Organic Analysis, Multi-Cone., Rev. 2/88
47 USEPA CLP SOU of [norg. Analysis Multi-Cane., SOU #788, revised 2/89.
96 USEPA CLP SO\J for Organic Analysis, Doc No. OLM01.0 incl OLM01. 1 thru OLM 01.8 R
A6 USEPA CLP SQ\J of lnorg. Analysis Multi-Cane., ILM03.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
SAMPLE NO: H437577
16-0CT-96 1922 CCJ ?COMET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16·0CT·96 1922 CCJ 700MET
17-0CT-96 1849 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
16-0CT-96 1922 CCJ 700MET
21 ·0CT-96 0548 GAB 405MET
21-0CT-96 1053 GAB 405MET
22·0CT·96 0420 GAB 405MET
24-0CT-96 0327 GAB 405MET
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
LABORATORY CONTROL SAMPLE RECOVERY
Pace Analytical SeNices, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section D Page 1
I --. --.. ----------------------------------------------------------------------------. -. -- --. -- - - -.. ---.... ------------. ---
TEST
CODE DETERMINATION
LCS o/.
RECOVERY
ACCEPTANCE
LIM! TS .. ------------------------------.... ----------------------------. --- ------. -. - - ------------ -... - -.. -.. ----. - -------------------
I
I
I
I
I
I
I
I
I
I
I
I_
I
I
I
BATCH NO: 67884
1435 Nitrogen, Kjeldahl (N)
BATCH NO: 67905
A.AGIJC CLP Silver, Total (Ag)
AAL\JC CLP Aluninun, Total (Al)
ABA\JC CLP Bariun, Total
ABEi.JC CLP Beryl l iun, Total (Be)
CLP Beryllium, Total
ACAWC CLP-Calciun, Total (Ca)
ACDWC CLP Cadmiun, Total (Cd)
ACOWC CLP Cobalt, Total (Col
ACRWC CLP Chromium, Total (Cr)
ACUWC CLP Copper, Total (Cu)
AFEWC CLP Iron
AKWC CLP Potassium
AMGWC CLP Magnesium
AMN\.IC CLP Manganese
ANAWC CLP Sodiun (Na)
--ANIWC ~ CLP •Niclcel
ASBWC CLP Antimony
AVWC CLP Vanadium (V)
AZNWC CLP Zinc
BATCH NO: 67906
AASWC CLP Arsenic, Total (As)
AP8WC CLP Lead
ASEWC CLP Seleniun
ATLWC CLP Thallium (Tl)
BATCH NO: 67966
OSTWC TCL -BNA + CLP Data Package -Water
Data PaClcage -BNA
95
81.8
105.6
92.7
98.8
98.0
96.8
93.5
95.2
92.2
103.9
99.9
97.3
94.6
100.0
94.9
105.8
99.4
93.9
93.0
102.5
94.0
92.0
offl i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
SAMPLE NO: H376496
SAMPLE NO: H376532
SAMPLE NO: H376534
SAMPLE NO: H376624
Pace Analytical
METHOD BIANK DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section E Page 1
. -. ------. ------ ----------------------. -------.. --- -. ----.. ------------------- -. ------------.. --------------. -------. --. ----
TEST
CODE DETERMINATION RESULT UNIT ·----------------------------········------------------------------------------------------------------------------------------
BATCH NO: 67884
1435 Nitrogen, Kjeldahl (N) < 0. 1
BATCH NO: 67905
AAGUC CLP Silver, Total (Ag) 8.4 U
AALUC CLP Aluminum, Total (Al) 88.7 B
--"·--A8AUC--CLP ·Barium, Total 0.6 U
ABEWC CLP Beryllium, Total (Be)
CLP Beryllium, Total 0.3 U ACAWC CLP-Calciun, Total (Ca) 47.8 U ACDWC CLP Cadmium, Total (Cd) 4,8 U
ACOWC CLP Cobalt, Total (Co) 4.6 U
ACRWC CLP Chromium, Total (Cr) 4.9 U
ACUWC CLP Copper, Total (Cu) 6,4 U
AFE\.IC CLP I ran 79.0 B
AKWC CLP Potassium 912 U
AMGWC CLP Magnesium 37.2 U
AMNWC CLP Manganese 3.5 B
ANAWC CLP Sodium (Na) 1,120 B
ANIWC CLP Nickel 15.3 U
ASBWC CLP Antimony 4,3 U
AV\.IC CLP Vanadium CV) 3.9 U
AZNWC CLP Zinc 2.4 U
BATCH NO: 67906
AAS\.IC CLP Arsenic, T eta l (As) 1. 1 U
APB\.IC CLP Lead 0.8 U
ASE\.IC CLP Seleniun 1.3 U
ATLWC CLP Thallium CT l l 1.6 U
BATCH NO: 67966
OSTWC TCL -BNA + CLP Data Package -Water
Data Package -BNA off line
BATCH NO: ·-679n
AHGWC CLP -Mercury 0.2 U
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
SAMPLE NO: H376497
mg/L
SAMPLE NO: H376533
ug/L
ug/L
ug/L
ug/L
ug/L
ug/l
ug/L
ug/l
ug/L
ug/l
ug/l
ug/L
ug/l
ug/l
ug/l
ug/L
ug/L
ug/L
SAMPLE NO: H376535
ug/l
ug/L
ug/l
ug/L
SAMPLE NO: H376625
SAMPLE NO: H376640
ug/l
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
Pace Ana!ytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
1-----· December 04, 1996
Report No.: 00056890
' Section F Page 1
I
I
I
I
I
I
I
I
I
I
I
I
I.
I
I
I
OUP\ !CATE AND MATRIX SPIKE DATA
-------------------------------------------------------------------------------------------------------------------------------
TEST
CODE DETERMINATION
ORIGINAL
RESULT
DUPLICATE
RESULT UNITS
RANGE /
RPO
BATCH NO: 67884
1435 Nitrogen, Kjeldahl (N)
BATCH NO: 67884
[435 Nitrogen, Kjeldahl ( N)
BATCH NO: 67905
ABE~C CLP Beryllium, Total (Be)
CLP Beryl l iun, Total
ACO~C CLP Cadmium, Total (Cd)
ACR~C CLP Chromiun, Total (Cr)
AMN\.IC CLP Manganese
• The concentration of the analyte
matrix spike recovery.
ANIWC CLP -Nickel
AZNWC CLP -Zinc
* The concentration of the anal yte
matrix spike recovery.
0.5 0.5
0.6 0.7
18.8 18.4
4.8 U 5 .0
46.5 45.6
138,000 134,000
prevented accurate determination
505 500
2,120 2, 100
prevented accurate determination
mg/L
mg/l
ug/L
ug/l
ug/L
ug/l
of the
ug/L
ug/L
of the
0.0
15.4
2.2
2.0
2.9
1.0
0.9
--AALI.JC--CLP · .AluminllTl, Total (Al) 74,400 73,300 ug/l 1.5
* The concentration of the analyte prevented accurate determination of the
matrix spike recovery.
ASBI.JC CLP · Antimony, 4.3 U 4.3 U ug/l
* Recovery of the matrix spike indicates the presence of a matrix interference.
This should be considered in evaluating the data.
ACAi.JC CLP-CalciLITI, Total (Ca) 378,000 376,000 ug/L 0.5
* The concentration of the analyte prevented accurate determination of the
matrix spike recovery.
ACO\JC CLP -Cobalt, Total (Co) 3,420 3,400 ug/l 0.6
* The concentration of the analyte prevented accurate determination of the
matrix spike recovery.
ACUWC CLP · Copper, Total (Cu) 799 783 ug/L 2.0
.* Recovery of the matrix spike indicates the presence of a matrix interference.
ThiS should be considered in evaluating the data.
AFEWC CLP -Iron 22,600 22,400 ug/L 0.9
AMGWC
·----
* The concentration of the analyte prevented accurate determination of the
matrix spike recovery.
CLP -Magnes i LITI
* The concentration of
matrix spike recovery.
176,000 175,000 ug/L
the analyte prevented accurate determination of the
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futl,
without the written consent of Pace Analytical Services, Inc.
0.6
SAMPLE
SAMPLE
SAMPLE
MS
RESULT
NO: H437309
2.6
NO: H437607
2.5
NO: H437577
62.7
48.6
210
131,000
891
2,410
73,500 ..
54.2 ..
382,000 •
3,710 ..
980 *
22,700 *
187,000 •
MS ¼
RCVRY
105
94.5
87.8
97.2
81.8
77.2
54.2
72.4
Pace Analytical
Pace Ana!ytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
I
I
December 04, 1996
Report No. : 00056890 I Section F Page 2 DUPLICATE AND MATRIX SPIKE DATA ------------------------------------------------------------------------------------------------------------------------------1 TEST ORIGINAL DUPLICATE RANGE / MS MS i. CODE DETERMINATION RESULT RESULT UNITS RPO RESULT RCVRY
AK\.JC CLP -Potasslum 16,800 16,800 ug/L AAG\JC CLP -Si l ver, Total (Ag) 17.7 17. 1 ug/L * Recovery of the matrix spike indicates the presence of a matrix interference. This should be considered in evaluating the data.
-· --ANAi.iC--CLP -Sodium (Na) 3,620,000 3,540,000 ug/L
AV\.IC
ABAUC
BATCH NO:
AAS\.JC
ASEWC
APBWC
ATL~C
BATCH NO:
AHG\.JC
• The concentration of the analyte prevented accurate determination of the matrix spike recovery.
CLP Vanadiun (V) 1s_8 0 14.5 B ug/L CLP Barium, Total 21 .4 B 20_9 B ug/L
67906
CLP Arsenic, Total (As) 1-1 u 1-1 U ug/l CLP Selenium 1.3 U 1.3 U ug/L CLP Lead 1-0 B 0.9 B ug/L CLP Thallium ( TL l 1.6 u 1-6 U ug/l * Recovery of the matriA spike indicates the presence of a matrix interference. This
67977
CLP
should be considered in evaluating the data.
-Mercury 0.2 u 0.2 U ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
o_o 36,300 97,5 I 3.4 53.6 * 71-8
2.2 3,540,000 • I
8_6 476 92.0
2.4 1,750 86.4 I SAMPLE NO: H437573
39_0 97_5
10.5
9.3 93.0 I 23.9 114. 5
35.3 * 70_6
SAMPLE NO: H437574 I
3-7 92.5 I
I
I
I
I
I
I
I
I
I
I
I Pace Analytical
1-----
MATRIX SPIKE AND MATRIX SPIKE PUP! !CATE DATA
Pace Analytical Services, lnc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Tel: [phone]
Fax: [phone]
December 04, 1996
Report No.: 00056890
Section H Page 1
I
I
I
I
I
I
I
I
I
I
I
I
·····--···--------------------------------------------------------·····--·--·--------------------------·-----------------------
,_
I
I
I
TEST
CODE
BATCH NO: 67966
DETERMINATION
MS
RESULT
MSD
RESULT UNITS
OSTUC TCL -BNA + CLP Data Package · Uater
Data Package -BNA off line offline
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seivices, Inc.
RPD
MS PCT
RC1JRY
SAMPLE NO: H376625
MSO PCT
RCVRY
I
I
I
I
I Appendix E
I Chain-of-Custody Records
Plume Periphery Wells
I
I
I
I
I
I
I
I
I
I
I
I
I
-----.. r Pace Analyt1ca -
;1 Lo
i<J
~ (' I . b I/ .) .· ') Q I I I I/ .Ji.; , 1 5 w-; /v. ,. . ,r o 7
'
Phone '/o 7 -G 3 3-J 7 JI
Sampled By (PRINT): (f) a:
,J:. '/ !lrAA .-.r, y
w z
"' Samplef Signature ' Date Sampled_ .·. ··1 ,h--
)~.l--" /7!"/],.,-1<--'(_./..__..,.7
>-z 0
(,)
u_
0
ITEM SAMPLE DESCRIPTION TIME MATRIX PACE NO. NO.
ci z
~JS-09
,(JI,/•,.,,, . ''\ . 'f•_ '•
, ID· II/· 1i ,, ·q:35 ,.
Am
,
,:,-:.
2
3 I r );.
4 NS-oq /0-J'j -9(, \,,/
5
6
7
8
Additional Comments ; -~---.. -:1--------:----·--· •'.•' j, .,· ,-· .I •"""t_..-. I ••~--, -ii_. : • i
3
---

-
-I • ,. ✓ I : ,' ~
-I
'/ J/J 17'·
Report To: A e 11 I) 1) I z
D (i Bill To: I · ._, ·
.--j
l_~J ,, ,., ' ·1 ' , I
..._; f
P.O.#/ Billing Reference
Project Name/ No.
PRESERVATIVES ANALYSES
f--,---,---,--,---,--,REOUEST
0 w > a: w ( __ ) C.
(f) -w a: a, z ::::,
' .• ' / ... ':::._--'
0 0 "' -✓-:
(f) z 0 £ I >
X X
X X
_X X
X
-/,--..,, . ,_.,
CHAIN-OF-CUSTODY RECORD
Analytical Request .. , , , .-
f.1.'.'( ~::t .. ):! ~
Pace Ghent No. 'f7.~-> ,..,.. ...._)
Pace Project Manag,er
' ,
Pace Project No. ( /
"Requested Due Date:
t · / (
REMARKS
..
. v ,--·-,,. ' I ::-_ I ' ' I ' )_~
SEE REVERSE SIDE FOR INSTRUCTIONS
Pace Analytical
',. i ;·-'-1.,,.,.,I + '-(11 ,·_·,,1,c..•,·I Client /i: I/ I tj(1 -', -, .c r, 11
I ~
S;//sbur/ /.I> ,-19!,JLj
Phone /(JI/ b 33 1 'J.J I Ex. ?o 3
Sampled By (PRINT):
]~, ,, , Ii" tAofl
Date Sampled
0
Cf) a: w z
<( >-z 0 u
u_
0
ci z
~
Jf
I
L, j -' 17-
Report To: '"'Cf) \ / {) : 1 .Z..
Bill To:
P .0. # / Billing Reference •J ·/-/ C ~; ,I.;: '/
Project Name I No.
PRESERVATIVES ANALYSES 1
f-~~-~~-~--JREQUEST ,.,,,-,
0 w > a: w ~~ J
Cf) w a: a_ z ::,
0 0
Cf) z I I
-"-~ -
"' -c
0 <~ >
X X
y._ X
X
CHAIN-OF-CUSTODY RECORD
Analytical Request
I' ••.
Pace Client No. (; I{_.'. ..,
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
2
3
4
5
6
7
8
,,_-~ .. ::''·'' ('i .·-:.1 ._. X.
I ·x
Additional Comments
3
X
SEE REVERSE SIDE FOR INSTRUCTIONS -------
-

-

-
-1y_,.. r Pace Ana t1ca
() .
-:.O
'
Phone '/(Y-1 -/233-/'!JI E" . .;2o3
----

-
< -/JJ J
Report To: kc /1
Bill To: po. /) J(' -, 15 ox I'!
-
ri, 7 -/ 11.'-· -') / -7 P .0. #/Billing Reference _ / c?
Project Name I No.
---3 biiiliilt+ t.•
CHAIN-OF-CUSTODY RECORD
Analytical Request
(I / /\ ,'
Pace Client No. _:: 1 ..,J __ , ::-
Pace Pro;ect Manager
Pace Proiecl No.
"Requested Due Date:
Sampled By (PRINT):
,Jeyy, /in fh ol\
Cf) a: w
PRESERVATIVES ANALYSES
1------~-------iREQUEST
Sampler Signature Date Sampled
_))_✓-7 7~7J:':7 Jo -Ji/-.:,1 In
ITEOM. SAMPLE DESCRIPTION TIME MATRIX PACC NO. N .
•·· -. ,---.
NS-II
"(}:';·,-,1,•;i:fH)~_•'.,-·:f-:i;?it-H,;.;,11-'/6:~,5: 'tr-,.-:,.h •. fo'.1 "/---.•!:.; ·. 10-111-96 . ,:i,;, . ·\. ")j\
-~ --J. . ...-. :·--::·.·
z
<(
f-z 0 0
u._
0
ci z
1
2 t I ' /j-
3 1 i.-.. /
0 w > a: w-
Cf) w a: n. z ::,
4
5 /JS -I I 10:)S
11,.,
I Y--
1
6
7
8
Additional Comments
3
c_, ·-·:r:
0 0 -,_·
Cf) "' N z 0 0 I I > ' REMARKS
'I.
X
X X
X
X
RELINQUISHED BY/ AFFILIATION ACCEPTED BY/ AFFILIATION 1111 '"/,--· --' . ' : !' )/ I
SEE REVERSE SIDE FOR INSTRUCTIONS
Pace Analytical
' } s.-, I I 5 bvr '/ tU C. ;;; '8 If 11
1
Phone 701/ & 33 · I tJ /
2
3
4
5
6
7
8
Additional Comments
ID-11/'Y& ,:-; .. '.f :; 1'::.t:-~
~-··.:: -.
. . . , •-.~.-. ;:
l/
Report To: Kc,., I J; H·:-:. /, u .:... .. ,
Bill To: J-1. 0.
P.O.# I Billing Reference
Project Name I No.
<...J
::r:: ,. ', -c « -,....
0 >
~
X
X
ANALYSES
REQUEST.
X
X
X
j
X
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No .
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
-3---------SEE REVERSE SIDE FOR INSTRUCTIONS ---------
-I
Phone /Oy (,?3-l'/3/ Ex :J03
4
5
6
7
8
Additional Comments
3
----,·
,)·~ u
Bill To: p 0.
-I!,/
/ ' -
P.O.#/ Billing Relerence q 7 · / (,7 (, '/
• 0 CJ)
N
I
Proiect Name I No.
~-) ,,
-::r:-!;
M -<:.: 0 <l'. -z 0 C I >
'I-
X
·x X
X
CHAIN-OF-CUSTODY RECORD
Analytical Request
I ! I\ ;• -, ,,,,::._"
Pace Client No. D / (_1 --' .---·
Pace Proiect Manager
Pace Project No.
'Requested Due Date:
REMARKS
Ill
j (•,; I
SEE REVERSE SIDE FOR INSTRUCTIONS
Pace Analytical
51., re). 1
! ,I
;) ,~; J Y'.)/
I
Phone /() i./ 6 3 3 · J 'J 3 /
Sampled By (PRINT):
Sampler Signature Date Sampled
_.)//~ d.b7 I.
ITEM SAMPLE D~SCRIPTION TIME MATRIX PACE NO. NO.
5
6
7
--· · ,-~,;:,'. ·,;,·;~/: '.""}'\.~\~:}?<;~"~, :·: _f:"',:;_i_· ~-':'.:°%•~/';'Y)?t
8
-3-- - - - - -
c_;: :'"=_,~
,/
Report To:
Bill To:
7 ,-/.
P.O.# I Billing Reference , ,
Project Name / No.
PRESERVATIVES K? ANALYSES l ·) w f--~-~~~~-~-REQUEST . z ;, >-
0 w > ,.r a: ·..:...1 ~ w 5 l
u Cf) .. __
w .. £: a: 0 0 -t--· n. .,: z Cf) z 0 C ::, :i' I >
0 ... -.,_,
{\..J d ., z •. . •· . . 'I,.
X X :x
I 'f
X
X
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
--SEE REVERSE SIDE FOR INSTRUCTIONS ---------
---------Pace Analytical -

-

-

-

-
Client A/cti·o,icc J 5fa,cJ..
Address J.; g ) CC cf C. {
I
Phone 7o t; · /2 .?.J -/7 3/ Ex ..?a 3
Sampled By (PRINT):
.Tc( /l '
Sampler Date Sampled ..--, .
-~-;;,, /0-11!-;G
/,. •• • _.tj I • ,' I r;I 1tf
[I
Report To: )<·;~ ,n
I J ! i/ KlvlT.z..
Bill To: P()
P .0. # / Billing Reference r, 7 I I -; G -, 'l -l,.-I
Project Name/ No.
CfJ E ATIVES ANALYSES ffi f--.P_R_ErS_RrV-,---,-i REQUEST
z
<( 5:l
f-> z a: 0 UJ
() Cf)
u.. UJ
-<:.J
:::i::::.
. '·I
\.
'-'
0 ~ ,tJ
0 z ,-..... 0 0 .,: +-Cf) z 0 z :::, :i' I >
... '# .;
1
2
3
4
5
6
7
8
· · ... . I 0· I I/' 1 .. . j X X
':' r 1,c,·,;•.:.cj{';~,·_;,>!p':c;,c.--,-"''2°>it""':;'. :t ~;._. . '[;;}{ ; ; ..
. , ·-.--· .. ,,.._ ,. :· "':·. ---~";:~~,.:· .. :: ~ :::::· ·--~.--,:~·j-~ I
~--,,•···•'>:, ,·· ·:"''/: •
NS-Ji ' I X
•
X
X
X
X
X
-

-
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
Ill
-'·~-*bi
-· . . .
Additional Comments
\ ((\}·>:C\r:,,:...:J(}:-,., 1'1/1-~ (;()
SEE REVERSE SIDE FOR INSTRUCTIONS
3
Pace Analytical
CHAIN-OF-CUSTODY RECORD
Analytical Request
;,; r ., ' t. I Client /(..·,··, I { fr~
-r
Address ::z' )5.,)
/ ·J '/ Phone ,, ( \"
Sampled By (PRINT):
.,__! e ~· < -A ,-...1 h o l' ,
Sampler Signature
,·.. /-. .Y -·---//.,..
i
2
3
4
5
6
7
8
Date Sampled
-3----
/l
0
IO !'I·.
0 w > a: w
Cf) w a: C. z :,
X
kF··_' Report To: _ /,
Bill To: Po
t(lvttz..
!) -:>GO UOY--JI/
P .0. # / Billing Reference q 17 ~ / {:, :_) (; ·7
Project Name I No.
PRESERVATIVES
,::....J ~
::i:: .~_J
0 0 --c:
Cf) < . ..,_
N z 0 I I >
X X
X
X X
X
,,.,. I-'\ ·'?
Pace Client No. (-;. I { ..' ,_.~
Pace Project Manager
Pace Proiect No.
REMARKS
RELINQUISHED BY I AFFILIATION ACCEPTED SY/ AFFILIATION
---·--'""I~--.,.· ... ,-~ •-4 ' : -,. ~ '
SEE REVERSE SIDE FOR INSTRUCTIONS --------------
-------Pace Analytical
I
Phone )QI/ -{,s3 -/'731 Ex ..:>o3
2
3
4
6
·,1_ r;,.·,
7
·.·':"•./·;~-:::.-:,..-.~~).:)>''.:-, -· "',"'"• ,•,. . -,
~---;! d ::.··; ··T r,;•:-.;.r~ -,:.:1-:·,.
Additional Comments
3
- -- -- -
Report To: KE' n
Bill To: Po
p .0. # I Billing Reference 9 ~7 ~ I (s ,2 C '7
Project Name/ No.
. •·· !, ' --. .. ' . ' . . !~; : -••. . l7 7
- -
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. r; j O _?" ;) .J.
Pace Project Manager
Pace Pr<?ject No.
·Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
Sampled By (PRINT):
. ' /;.' ,,.;,, -!!,.,,,'
Sampler Signature D te Sampled
fi<, ~~:f. .-.
Cf) a: w ,:: 0 <( w I-> z a: 0 w 0 Cf)
u. w
0 a: a. ci z z ::,
Additional Comments
3-- - - - - -
'/~'-// P .0. #/Billing Reference / ,,-. --
P-r'oject Name I No.
PRESERVATIVES ANALYSES
REQUEST
'.,\ ., ·,· '·
'-,"
0 0 '·.f' Cf)
:E z I
/7
325955
CHAIN-OF-CUSTODY RECORD
Analytical Request
/ ;' Pace Client No. ( ,··
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
-SEE REVERSE SIDE FOR INSTRUCTIONS ---------
-.. -----r Pace Analytica -
Sampled By (PRINT):
_,1;1L 4,,,_ / ··1 ..
en a: w z 0 ;, w >-> z a: 0 w 0 en u. w
0 a: Q_
ci z z :::,
4
5
6
' '. __ ,._.•; ,,-~,-••;•-·~:'',_'',·;··-_l.;"·f-~'t" ,~:':~-.r::;..;,,, .• -: ,~"':\
,., 't _,
Additional Comments
3
' /
Report To: t'/ .. :: /t,/
Bill To: /-__,. /'.
---
,·• 7 // I
P .0. # / Billing Reference '/ ,, --' •-,,,, _.✓••• (
Project Name I No.
PRESERVATIVES
'•J \
::;:·
----' .-,
0 't-0 en
IN z I
·• I·
--CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. //
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
c,. ! ""'\ ,,-·;
( \.~
SEE REVERSE SIDE FOR INSTRUCTIONS
-
Pace Analytical
Client
Address -
Phone
Sampled By (PRINT):
Sampler Signature
2
3
4
5
6
7
-3-
: }
. i·
Date Sampled
- - -- -
. ,. . ·f
v·
-
Repor1 To:,\
Bill To:
P .0. # / Billing Reference
Project Name I No.
~ PRESERVATIVES w f---,--.--,----,--.-----, z ~ z 0 0
'-L o
ci z
l I
0 w > a: w <fJ w a: 0. z ::,
0 0,.,
<fJ z I I
\
<t 0 >
I
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
-SEE REVERSE SIDE FOR INSTRUCTIONS ---------
-------Pace Analytical
Phone
Sampled By (PRINT):
1
2
3
4
5
6
7
,---.::.~;r.'"(,_.~~~--. ·::.;, ---~ --~
'
-
, j l
----
Report To: -) ,:.-· ,//
Bill To Pa ,=$c,t 3 Cfo/
q-7 '/I-< P .0. # f Billing Reference ,. ~ /r/ d l,,. /
Project Name I No.
(/) ER T VES ANALYSES ffi ,.---,-P_R7E,s_rv_A--,l ___ __,REOUEST
z ~ z 0 (.)
0 w > a: w (/) w a: "-z :::,
0 0 ~ z I I
X
<(
0 >
--CHAIN-OF-CUSTODY RECORD
Analytical Request
/ / ..
Pace Client No. (,? / .:..-'
Pace Pro/ect Manager
Pace Project No.
·Requested Due Date:
REMARKS
-,. ··., v, ,. ·,, · ·· k1·/~o~_;Jf'.t?-:,e-
L_ ____ ~----~-----, ;' -·"' 7 ,It/''~"''.'""? .
Additional Comments • / .
,.-:~ .. "-'1':' •·:.·: ---
SEE REVERSE SIDE FOR INSTRUCTIONS
3
ii.:
Pace Analytical I I
Client 1/k-1-/oAIAI-91"/iK-A. .... cA~.c!'1-L ReportTo LeA!'. /,'ltLY2-
Address '/f5 L e/Af.-5,Pt-i ~ .(o&4= Bill To lb, 6~ X 37?
'>A[<;bµ.t'/;, ,f/,k, ,,;t.'8'fl/1/ P.O.#/BillingReference '17-//.GZ~ 7
Phone 7o Y-{3, -17 "3 I a Z.:> 3 Project Name I No.
Sampled By (P
2
3
4
5
·, ,._.-1 '.,·
...... ,··
••
·x
I y
'/
X
X X X
X x
X f x.
.• .:: '
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. /4 /C' ,.5 i>2 ::;-
Pace Project Manager
Pace Project No.
'Requested Due Date:
REMARKS
ACCEPTED BY/ AFFILIATION
Additional Comments
3
SEE REVERSE SIDE FOR INSTRUCTIONS ------
I
I
I
I
I
Appendix E
I Chain-of-Custody Records
Trench Area Wells
I
I
I
I
I
I
I
I
I
I
I I
m
0
-l!!!!!!!!I >1!11111· -iiiii -

-
-P~_ce 1Aoalytical
i-. i
Client \\-. .. , t:... 1;
Address
\
Phone (r-.:o-~
Sampled By (PRINT):
;:_::·~!-·(~ ~.v· Jl~
Sampler Signatur Date Sampled
2
3
4
5
6
7
1
D w > a: w (f) w a: a_ z ::,
0 (f)
:i'
0 z
I
------
CHAIN-OF-CUSTODY RECORD
Analytical Request LP\ ;;i l\~
Pace Client No.(, \ 0 D K2
Pace Pro~t Manager
"Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR iNSTRUCTIONS
Pa~ce 'Analytical
Sampled By (PRINT):
,:-\,.f..t/ I iJ
Sampler Signature
(J) a: w z 0 < w >--> z a: 0 w 0 (J)
/0-
Date Sampled
u.. w
0 a:
ci a. z z ::,
2
3
4
5
•;, ,'r'--'£
6 ::,,..1:·,
7
8
P.O.#, Billi::§ Eloferoeso C\1 - \ 62\ '3,3
G)e\\s Project Name/ No. ---1.-,nC'h
PRESERVATIVES ANALYSES
REQUEST
• 0 ~
(J) 0
N z I I
35223 7
CHAIN-OF-CUSTODY RECORD
Analytlcal Request
P~ce Client Na. l, \ ·\!)~
Pace. Project *ager fro;'O.H, f .,,.. ;,,,-
Pace Pro)ect No. i'b O 'f/~ ,/,t,. Y
*Requested Due Date:
--
-l!!!!!!!I r!!!!!!I =:;; iiiii -

-
PaJ:e,.'Analytical
Sampled By (PRINT):
/·\ . -_, .:<·: .,,.>-' /<In/,-~ /o-l
Sampler Signature Date Sampled
2
i.l-•
3
4
5
6
7
8
-
U)
0: w z ~ z 0 ()_
LL 0
ci z
----,,,--,
0
P.O.# i Billing Reference C\f] -\ (:::,:i. '"33
PRESERVATIVES ANALYSES
f-~-~-~-~-~---jAE0UEST
0 w > 0: w
U) w 0: a. z ::,
0 U)
N I
0 z I
--
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No. l__.., \ D ::> ;s,
Pace Pr:Jct Manager .
•Requested Due Date:-------~-
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
P ':'.Ca·' An a lyti ca I
_i;cc'1;~e_r:,n!_t !_/'Lr A,c!f/J~1~:c-Lt..e.~~~(_~~!.l'.!C6a,_._;;2'1'.~(_LLJ~~'..,''.:C.,;;.~a_/ CO·
Address c:;CJ....,/
'j/~.!,/
Sampled By (PRINT):
/o-·
sampler Signature Date Sampled
EX
2
3
4
5
6
7
8
if) a: w z ~ z 0 0
u. 0
ci z
0 w > a: w
if) w a: a.. z :::,
-
'
s;11Ta/?O &~ 3 9'9 . -..
Pro·ect Name I No.
PRESERVATIVES
0 if)
£
0 z I
352239
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace c1;ent No. ~IO 3 ;zr
--
-liiiii iiiii -

-

-
-Pa~e~ i Analytical -
Phone ID:'/
Sampled By (PRINT): ff) a:
h/~;,~
S3mpler Signature Date Sampled
w z 0 < w f-> z a: 0 w 0 ff)
LL w
0 a: 0.
0 z z ::,
., '
2
'.:·
3
4
5
6
7
8
--
,'Re~a'rnolj.A/ f1u//z.-
Bi11To ?o. ;Jox.319
P .0. # / Billing Reference 9 7 -/ (p 2
Pro·ect Name/ No. 7.:-.e:.d
0 r:5' ff) N z
I I
---CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Proiect Manager .
11/o,"of''-! /Y.,#1),/ ···
Pace Project No. C. ~ 0 '1/ .:!. , /&-,;/ ·>,--.
ARKS
SEE REV~RSE SIDE FOR INSTRUCTIONS
Analyt·ical
l I
Phone 7o c1 -l,, J3 -17 J 1 1:::xr .:zt.) '?
Sampled By (PRINT):
;i-:C:ic/ /J~ /o-
Sampler Signature. Date Sampled
<J) a: w z 0 < w .... > z a: 0 w (_) <J) w a:
(1-z ::,
2
3
4
5
6
7
'
. \
i '· Repollt To: Ke:,-c,1 lrk-ltk
BillTo Po. /5<)X 399
P.O.# J BiiiirlQ R01ePence 9 1-/(o 2J J
Pro·ect Name I No. ~t!.
PRESERVATIVES
'1
0 0 <J) N z I I
-
352241
CHAIN-OF-CUSTODY RECORD i
,,( / --~
Pace Client No. & / () J 2. 5 \ .'
Analytical Request
REMARKS
--
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Appendix F
Out of Service Well Pumping Records
Periphery and Trench Area Wells
I·
I
I
I
I
I
I
I
I
Well# EX-01
Checklist Tag# P-1031A
Set Flowrate for the Pumas :)/ C p;1·1
Actual Flowrate for the Pu mos P"''
Any Adjustment to Flowrate t~bo1
Made?
-
Date: q !'3 Ii(,
Well# EX-01
Checklist Tag# P-1031A
Set Flowrate for the Pumas ) I C-I/YI
Actual Flowrate for the Pu mos Jo (;f fY1
Any Adjustment to Flowrate
Made? )/or,"
Date: l'//7{,
Well# EX-01
Checklist Ta # P-1031A
Set Flowrate for the Pum s / / G f fh
I Actual Flowrate for the Pum s
I
I
I
I
I
I
I
I
I
Any Adjustment to Flowrate
Made?
Date: 'i /5/ 76
Checklist
Set Flowrate for the Pumas
Actual Flowrate for the Pumas
Any Adjustment to Flowrate
Made?
t Date: 'i t6t'i
• Checklist
Set Flowrate for the Pumas
Actual Flowrate for the Pumas
Any Adjustment to Flowrate
Made?
Well# EX-01
Tag# P-1031A
2, GP1•1
:Jo GP((\
fJoAJe,,
Well# EX-01
Taa # P-1031A
'}. I CP1"'
P""'P~
Daily Checklist for Plume Periphery Wells
Well# EX-02
Taa # P-1031B
1 GffYJ
,p, O i--:P
cl«y
Well# EX-02
Taa # P-1031B
1 C-Pfh
5 Gfr·
; I . 'I,,.. ... ~-,' ·1,.)I ·C:
Well# EX-02
Ta # P-1031B
Well# EX-02
Taa # P-1031B
9 c ~11 ,
5 C-P (Y"\
/,Jo,Je.....
Well #EX-02
Taa # P-1031B
,7 C'/;;,,,,,
aft
Well# EX-03
Taa # P-1031C
3:J (;..Pr>1
p~ ,,..ps
J,..,:; b.1
Well# EX-03
Taa # P-1031C
3) Gfrr>
(0 r;pr,,
/Jr,,,<
Well# EX-03
Ta # P-1031C
C\
Well# EX-03
Taa # P-1031C
j 2 C-f'-',-,,
ID (_f tr1
A)orJL
Well# EX-03
Taa # P-1031C
'3;2 Gf>,,,
f r,,.1>1p
Well# EX-04
Taa # P-1031D
19 C-P/>1
'-I'-{' " .
c:Jc,y
Well# EX-04
Taa # P-1031D
;q C.f/17
3:) C-Pfh
f/<f,, e
Well# EX-04
Ta # P-1031D
Well# EX-04
Taa # P-1031D
;t:j Gp✓,,
31 !':Pm
l\)O/,J?-
. Well # EX-04
Taa # P-1031D
; 0 _C,D/Y I
a~
' .... -.. ..,,
PATc: t.Je.L-L .S-r,t:;l'l.-r
:IP 77 "1.€
7/41 7(, Gt-oS
(;Y---0 6
II l-'-F,---f=-------71-:::c..._-;-~~1---=3=---+-----W.--
! · \I r-t-t---r----==~--;;-;---:-:4--~2:::.-o -1-----1-.)_ _ _:J:,
1:,1· t--,r-f----;:;::~---::;;~3~. a---f-.--~h::t__J
I
. /(,_ L/
:!'•· r----t-t-----t,:::::_ __ "71~~:'.:+..3!:..~~_:_::::_~-i '~,. '.:..~ /!.,~ ;2:::J~.\..4-/!._f_..,{_ _ _J
I
,) . 0 V~'j ,n_:7
:1111f_Y_---0_1f--*==---:;-::r--:::::~1--f.:...:. O::.__+---+-__J_ _ _j
S 0
FY-o5 2.3
1 . . 1 i -Y--06 2 cJ i 1--r-i---~-;;:;--:::~=-----;:7-:-:-----:7~:::.:-~-+--~-j_ _ _J
_,.,., ;I 1-t----r-_:::__7c::::,___~.fL--~~~3:::'..:.·..::::.0 ---i--~~1to_j-2L-.J
('.lc:r·~ c.o-z_ ,. o fh-,,-f ~ i---i--Ftt....;<-:.::--""-O_g__f~--jr;,-:;-:-:;;,f~~iv-:::--:;;:,t-,--~~{}r_,d~,,~//
1
~
,
,
J
~
-W,--~-_J
I X-~ ~.V
1.-.. -r-r~~---rr::---::?tL--~~~-i----1-L-__j
,· ,-; :;-y-/o ,-v !;;h 1----
i
I
'
??Arc
t5C-0 7
G-:X--/0
--··· --··· ---· -··-··-.
2,0
J.0
4,0
··----··· -·-· .. ·-----------·---------·----·
·,
\
\ ' I
i -
I (
~. --T,e,,5vc,h' ,6t-1>G-: S-p;ar-u/? ht1,s;,&i"'1H-1 ,_·-~...----,----,--~
Acru19t.
J.o :J
fy-b7
;S.; .
Ey-1D S.o
()
3,o )5. I
0
-; ,~_,,
I
I I l:
I,
I
r---..----.------r----------r-----r---.....-----
t.Je.L-L 5 r,q IZ.. r PA1c
8-1q&
~v . .
:IP
[f-o~
f, ,()(p
f /-t71
:X-~'t
7 z !, -09
' t.,
S~L --n,
C. /) U' L,
~
I
•
I
,.
IC ,··
'
' I
I
r I
PATc
i(;;2/9b
I
I
1/t6h6
·-·-··· -
t../l;l.(_ 5r412.-r S-r.,:, '° Ser C"~l>f ~"'71-~ -;;,.,._'= 9f"M
2-3
2,0
,D
-m ,,,,._
S-'->-.. ~f ,.,,--.\..0 ............. •~~. '.
£1-DC
'£ '/-o7
E. i-ot
f-Y-0?
EV-ID
.. ·-·• "' . ,. -. --·· ·-·-··•··