NCD991278953_19960501_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - First Quarter 1996 OU-1 and OU-2-OCR

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Quarterly Report
First Quarter 1996
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
May 1996
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Quarterly Report
First Quarter 1996
Operable Units No. 1 and 2
........._...:JI?...,, :'"\
n 7 1996
[Su u
IPA-RIGIOMIV
ATLAMTA,GA
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
May 1996
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Table of Contents
1.0 Groundwater Monitoring Activities for the First Quarter 1996 .
2. 0 Planned Groundwater Monitoring Activities .
3. 0 References ..
Appendix -Certificates of Analysis
Appendix A -Report of Laboratory Analysis
Appendix B -Sample Delivery Group Narrative
Appendix C -Volatile Organics Analysis Data Sheets
Appendix D -Semivolatile Organics Analysis Data Sheets
Appendix E -Inorganics Analysis Data Sheets
Appendix F -Chain-of-Custody Records
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List off ables
Table Title
List of Sample Analysis and Water Level Monitoring Performed
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, First Quarter 1996, Operable Unit No. I
3 ROD (OU2) Contaminants and Selected Water Quality Parameters in
Groundwater, First Quarter I 996, Operable Unit No. 2
4 Groundwater Cleanup Criteria, Operable Unit No. I
5 Water Level Measurements, First Quarter 1996, Operable Unit No.
6 Water Level Measurements, First Quarter 1996, Operable Unit No. 2
List of Figures
Figure Title
Site Map
2 Quarterly Summary of Acetone
3 Quarterly Summary of 1,2-Dichloroethane
4 Quarterly Summary of 1,2-Dichloropropane
5 Quarterly Summary of Bis(2-chloroethyl)ether
6 Groundwater Contour Map for January 15, 1996
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1.0 Groundwater Monitoring Activities for First Quarter 1996
This first quarter 1996 report presents the findings from the groundwater monitoring
conducted at Operable Units No. l and 2 at the National Starch and Chemical Company
site on Cedar Springs Road, Salisbury, North Carolina. This report is prepared in
accordance with Record of Decisions (ROD) issued by the U.S. EPA on September 30,
I 988 for Operable Unit No. I (OU!) and on September 30, I 990 for Operable Unit No. 2
(OU2). Operable Unit No. l consists of contaminated groundwater area located in the
east-southeast portion of the facility. Operable Unit No. 2 consists of contaminated soils
and surface water/sediments in tributaries surrounding a trench area east of the plant
operation area.
Operable Unit No. 1
Groundwater samples from the four downgradient groundwater monitoring wells (NS29,
NS30, NS3 l, and NS32) and four bedrock extraction wells (EX0l, EX02, EX03, and
EX04) were collected on January 15, 1996. All samples were analyzed for Target
Compound List (TCL) volatile and semivolatile organic compounds (VOC and SVOC),
Target Analyte List (T AL) metals, and general chemistry. In addition, samples from the
monitoring wells and extraction wells were analyzed for selected water quality parameters
to monitor influent loadings for the Combined Pretreatment System (CPS). A sample
analysis summary is provided in Table l. The samples were collected in accordance with
U.S. EPA (Region IV) protocols. The TCL and T AL compounds were analyzed
supporting U .S EPA Level IV Contract Laboratory Program (CPL) protocol.
All four plume periphery extraction wells are currently operational. The trench area
extraction wells are not operational at this time because of the RCRA closure of Lagoon
No.2.
Results from the chemical analysis for Operable Unit No. I and Operable Unit No. 2 are
presented in Tables 2 and 3, respectively. The list of compounds presented in these tables
represents the contaminants specified in Operable Unit No.· l Record of Decision (ROD).
The list of designated compounds from the ROD (OU!) and associated cleanup levels are
provided in Table 4. Figure l is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
The results of this quarters sampling indicated that four organic compounds, acetone, 1,2-
dichloroethane ( 1,2-DCA), 1-2-dichloropropane ( 1,2-DCP), and bis(2-chloroethyl)ether
exhibited levels that exceeded cleanup levels (shaded bold faced values in Table 2). The
acetone levels decreased from the previous quarter in three of the four extraction wells
(EX0I, EX02, and EX04) and increased in well EX03. A significant decline in acetone
levels was recorded in EX02 over the previous sampling period. The decline in acetone
and other compounds is most likely attributed to the fact that EX02 (that had pump
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problems during the third quarter of last year) is now working properly and pumping
continuously.
Also, acetone levels has declined significantly in monitoring wells NS29 and NS3 l over
the previous sampling period. The decline in these wells is attributed to the fact that
EX02 is now pumping continuously and capturing some of the compounds before they
reach the down gradient monitoring wells.
Also, levels of 1,2-DCA and 1,2-DCP have decreased in wells NS29 and NS3 I over the
previous quarter sampling. Monitoring well NS32 continues to show that no
contaminants are present.
Extraction well EX0 I did not exceed the cleanup standards for any of the VOC
compounds. However since the third quarter 1995 sampling event, EX0 I did exceed the
cleanup standard for bis(2-chloroethyl)ether a semi-volatile compound. Concentrations of
_Bis(2-chloroethyl)ether exceeded cleanup standards in all sampled wells (see Table 2). All
of the sampled wells showed a decrease in Bis(2-chloroethyl)ether concentration since the
previous fourth quarter report (see Figure 5).
The general trends for· the four organic compounds that have exceeded the cleanup criteria
over the past four quarterly sampling events are presented in graphical form on Figures 2
through 5. These four organic compounds are acetone, I ,2-dichloroethane, 1,2-
dichloropropane, and bis(2-chloroethyl)ether. Manganese exceeded cleanup standards in
only one well, EX02. Barium exceeded cleanup standards in extraction well EX02 and
monitoring well NS3 l (see Table 2).
Water level measurements were taken on January I 5, 1996, from seventeen selected
monitoring wells and four extraction wells located in Operable Units No. I and 2. The
static water level for NS32 was not measured, due to artesian conditions. Well NS32 has
been under artesian conditions during all previous sampling events. The results of the
water level measurements are presented in Table 5. Note that for this quarterly report,
water level measurements were taken after the extraction well system was temporarily
shutdown. Therefore, the groundwater contour map presented in Figure 6, represents the
natural groundwater gradient across the subject area.
During the past quarter, all of the plume periphery extraction wells maintained their
pumping capacity over the previous fourth quarter 1995. The combined average quarterly
pumping rate for the four extraction wells (EX0I, EX02, EX03 and EX04) is about 86
gpm. The efficiency of the plume control and hydraulic control will be evaluated in more
detail after all trench area extraction wells are fully operating.
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Operable Unit No. 2
Groundwater samples were collected from monitoring wells NS09, NSl0, NSl 1, and
NS 15 on January 15, 1996. All samples were analyzed for selected TCL VOCs and
SVOCs, T AL metals, total dissolved solids (TDS), and chloride. A sample analysis
summary is provided in Table I. The samples were collected in accordance with U.S.
EPA (Region IV) protocol. The TCL and TAL compounds were analyzed under U.S.
EPA Level IV CLP protocol.
Results from the chemical analysis for Operable Unit No. 2 are presented in Table 3. The
list of compounds presented in Table 3 represents the contaminants specified in Operable
Unit No. 1 ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 4. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
All four monitoring wells (NS09, NSl0, NS! 1 and NS15) in Operable Unit No. 2 had
levels of 1,2-DCA that exceeded the cleanup standards (See Table 3). Except for the
chemical 1,2-DCA, monitoring well NS 11 has no organic or inorganic compound to
exceed the cleanup standard. Acetone may be present in the sampled Operable Unit No. 2
wells, but the concentration is below the detection limit and cleanup standard. Vinyl
chloride exceeded the cleanup standard in wells NS09.
Manganese exceeded clean up levels in monitoring wells NS09 and NS 15. Manganese
concentrations in monitoring well NS 10 declined for the first time below cleanup standard.
Monitoring well NS 11 continues to have manganese concentrations below the cleanup
standard.
Water level measurements were taken on January 15, 1996 from each of the four
monitoring wells. The results are provided in Table 6. A groundwater contour map of the
subject area is provided in Figure 6.
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2.0 Planned Groundwater Monitoring Activities
Operable Unit No. 1
Groundwater monitoring will continue. Care will be taken to closely monitor the daily
pumping rates of the extraction well system. Particular attention will be made to assure
that all plume periphery extraction wells continue to pump at optimum efficiency and that
downtime for pump maintenance is minimized. The implementation of the extraction well
system will continue as planned with the continued operation of the plume periphery
extraction wells EX0 l, EX02, EX03, and EX04.
National Starch and Chemical Company will continue to alert laboratory personnel of
samples from wells with known high VOC concentrations.
Operable Unit No. 2
On February 26, 1996, a new startup pumping operation began in Operable Unit No. 2
(trench area). Six extraction wells (EX05, EX06, EX07, EX08, EX09, and EX! 0) began
pumping at a combined pumping rate of about 17 GPM. During this startup phase these
extraction wells will be monitored closely and their pumping rates may be modified in
order to optimize their performance. The efficiency of the plume control and hydraulic
control for both Operable Units I & 2 will be evaluated in more detail after all trench area
extraction wells are fully operating.
Groundwater monitoring will continue. Like the groundwater samples from the wells in
Operable Unit One, the samples from monitoring well NS IO contains high concentrations
of l ,2-DCA. Therefore, care will be taken to alert laboratory personnel of samples from
wells with known high VOC concentrations .
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3. References
EDM, Inc., February I 996, "Quarterly Report -Fourth Quarter I 995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., October 1995, "Quarterly Report -Third Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
EDM, Inc., August 1995, "Quarterly Report -Second Quarter 1995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, May I 995 , "Quarterly Report -First Quarter l 995 Operable Units
No. l & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, February I 995,"Quarterly Report -Fourth Quarter I 994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, October 1994,"Quarterly Report -Third Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
North Carolina Environmental Management Commission, North Carolina Administrative
Code !SA NCAC Subchapter 2L (August 1993).
U.S. EPA, September 30, 1990, Record of Decision (ROD) for Operable Unit No 2,
National Starch and Chemical Company, Salisbury, NC.
U.S. EPA, September 30, 1988, Record of Decision (ROD) for Operable Unit No I,
National Starch and Chemical Company', Salisbury, NC.
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------·-- --· - ---- ---· -;-Table 1
List of Sample Analysis and Water Level Monitoring Performed
First Quarter 1996
Operable Units No. 1 and 2
National Starch and Chemical Company
Salisbury, North Carolina
Well Number
EX01 · · Exo2"·
EX03
EX04
BE ............... ·---..
BE
---'-'--····-. .' .......•. X -X ·········• ... , . X
X
NS05
NS06
NS21
BE
SM -----·--· !-----· ------·------·. --SM
NS22
NS23
NS26
NS27
NS28 ·······-··· .. ·······-· NS29
NS30
NS31
NS32
BM
BM
SM
BM
BM
BM
, BM ....... BM··--·
BM
BM
X
X
X
X
X --------------· ... ---···-·-x
X
X
·--·············---·-----·-·····----------·········--·------·-··-··-····
P01 . BM stream Gaugi;No. 11 .. NA"
Stream Gau e No. 2 NA
NS09 SM
NS10 SM -------------..... . ...... -····· ·--·
NS11 SM
NS15 BE
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
BE = Bedrock extraction well, BM = Bedrock monitoring well, SM = Saprolite (shallow) monitoring well
bProject TCL consisting of 13 voes, 2 SVOCs, and 9 metals, and meets Operable Unit No. 1 cleanup criteria (Table 4).
cTDS -Total dissolved solids
dCOD -Chemical oxygen demand
eTKN -Total Kjeldahl nitrogen
'tron pins in southwest tributary for monitoring stream elevations.
gNA • Not Applicable
X
X
Water
X
X
X
X
X ............ ---------x
X
X
X
X
X
X ------------x
X
X
X
X
X
m :, < a· :,
3 "' :,
ii:
0 0 0 s: 0 :,
0
<O "' 3 "' _el
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Table 2
ROD (OU1 l Contaminants and Selected
Water Quality Parameters in Groundwater
First Quarter 1996
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Extraction Wells Monitorinn Wells
Well Number: EX01 EX02 l EX03 I EX04 NS29 I NS30 I NS31 I NS32
Sample Date: 1115196 1115196 I 1115195 1115195 1115196 I 1115196 I 1115196 I 111519&
Volatile Oraanics /ua/ll
Acetone
Benzene
10U :·;;•:;10000;; ,,,.o,,IIII!~
sui,, ·--soou
9J :t:: 12000! 10U, 3500[ 10U
su,··· ·soou! . ··s·u·:··. 250ui·· SU .... . ... ··-········· ... Bromodichloromethane su; soou:
500U
500U ····su soou[ su, 2soul su ..................................................•..
Chloroform
1,2-0ich1oroethane
SU 500U!
SU ->'·il,P,ii';:1·12001: ....... :.:c:v;1, ... _ .. _ t,
5.:.00:_:U'-'---__ 5:..Uec: '"500;.:.;:U,:_f_· __ 5:_:U:..'_ 250U i SU s1:~ ~ ;}'iii'!i~~jl :~ i ~=:a-=-o~"-.'--, ---=-:~ ·····················-1, 1-Dichloroethy1ene SU soou:
. ...... su. i!·:,,··a30i[}1; '14liJ SU· :iifool su: . :isoui SU
SU 500U ! 500U SU;• 500U j ·su' 250L( SU
-·-, ,2-0iChlorOPl"oParie . ·· ···· · · ·Eiiiyilieniene
Methylene.Chloride ,,,, ..•. 2BJ 150BJ' 160BJ 2BJ; 150BJ' 2BJ· 71BJ! ·2BJ
Toluene SU 290J 130J 2J 370J ! SU: 64J i SU
i ,1 ,2ii,ich.ioroethane SU sciou 500U SU' 500U: SU . 250Uj SU
Trichloroethene 1 __ __:5:.:U:c. _ _;5::00=Uc.! _ _:5::00=U-'-i _· ·_··_··_···-=-su=-···~; _,,::5,:,00::U:c,,,i _ __:5::Ucc; __ 2:::5:,:0::Uc:.! SU
VinylChloride ,au; 1ooou: 1ooou: ,au: 1000Uj ,au: soou: 10u
Xylene su, ···sooui soou; su soou: su: ···2soul su
Semivalatile Oraanic Cua/I\
Bis (2-Chloroethyl) Ether I' !':\'"' i · ,.9J !I ':"t'.'(14lfr2 · :, , 1.30 I,.· i', , , > 10j': 47~!= j: ····•-············4-Nitrc;phenot ... ,.,,,.,,,,250"( soou: --soul' . '2su': 25U\
lnornanics lua/11
1,1 u;
&J:\' ,,::••:41! 2su:· "'2sui
uu, Arsenic UU' 1.1U' uu;
Barium \04'i::1'!:1:W!1if~.7CCio·L( _ __:=:,___:ccc,e:___: _ _:·s--=e-'-i~j'_· -===
"----------=B=eryllium .,,._o:c·.:.30:ci'-----'o"-.3"0"U""'-= 0.30U !
uu; ,1 .. ,
35.4B' 553i
030U!
UU'
28.osi'ii i::1930!
•,.,_.......:;._ ----· 0.30B' 0.30U!
Cadmium ...... 4.BU-1.____ 4.BU I
Chromium 7.7B ! ···4_9-(j"[
ll----'---------'M=anecge:a::.n:::e,:,se=-l---·.:.1 _::42=-·· l}f)Jr:fiii800l ..
Nickel 15.3U i 15.3U
Selenium ....... 1.6U! ......... 3.2Ui _____ _
Zinc 7.68! 14.3B!
Water Qualitv /ma/ll
coo
Chloride
Nrtrogen (TKN)
TDS
Note Data Qualifier Definitions:
19 1370:
59 ·· iriso
0.6 7.3!
3621 2978'
0.456'
45(j'1 4.8U' ' 7.8B' 7.4B: .....
3580: 2130
15.3U 15.3U'
1.6U 1.6U'
9.0B 15.6B'
440i 79! .. ,_.,,.,:,,,
262! 117!
1.51 1.5;
12esT 392'.
48U' ·
69B f
:io:ioi
15.3U' . :i2U]
2.4Ui
NIA•
745!
NIAi
B !Organics) = Compound was detected in the associated blank.
4.8U·
9.8B•
. 15401.
15.3U'
1.6U,
2.46:
N/A·
72
N/A·
375;
B (lnorganics) = Compound concentration is below the contract-required detection limit.
4.8U!
49Ui
sci:i!
1 s:i(i:
1.6Ui
3.2B i
NIA
181 i
NIAi
9541
....
10U
25U
uu
87.8B .......
0.30U
4.8U
8.8B
92.6
15.3U
1.6U
9,46
NIA
9
NIA
98
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace value, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed tor but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
mau spectrometry instrument.
ND= Not detected at or above the detection limit of analysis method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates a detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30·88).
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Table 3
ROD (OU 1) Contaminants and Selected
Water Quality Parameters in Groundwater
First Quarter 1996
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Monitorinn Wells
Well Number: NS09 I NS10 I NS11 I
Sample Date: 1115196 I 1115196 I 1115196 I
NS15
1115196
Volatile Oraanics lua/1\
,L __________ Acetone ____ 7J: ___ soo_u---': ____ 1ou~ '----=2:...0-=u,11 Benzene 1 riiT 250U ' SU . 1 OU
Bromodichiciromethi:i"iie 1 OU; 250U \ SU: 1 OU
,,_ _____ ·_··_···_··_··_·-_·-=c.chc.:10'-ro:...fo:...r.cmc, 1 OU: 250U: sUT" 1 OU
1 ,2-D ich1oroethane i'.'.:1tUi1i?J'):!:::1:. ~ ;:: ··. ,,.:,.""'·,' : ·,:,_..,,. :: 6100 l :,,-;,,-•.,,,. __ :,; · .,}-;s: ·:<:::::} ':_~~ff )i'.:!:i;i:;:::::1.·:1:[:;:;/:;' :•::250 ..... 5/.:o;~~!~~:~~~hYt~~~ --9J: ··:;,;-,,,:•;•,_'c:,(,'·2so"Utr:::.•.. --~=ff.J: - " -10U
... !!~-~~_i_?_~~~r_?P~~p-~-~~ 1 OU: 250(i ! SU: 1 OU
Ethyl benzene 10 I 250U, ··s2r·· 1 OU 11--------====c.=1 Methylene Chloridel-___ 1:.:0c:U:...' ____ ,7_:3c.::B.cJ.;..( __ 2BJ; 3BJ
Toluene 180' 250U ' 6 11 ............ •····-··
1, 1,2-Trichloroethane 10U · 250U' SU; 10U
Trichloroethene 1 OU; ··25QLJf . slJf 1 OU
Vinyl Chloride 500U [ 1 OU' 20U _________ .._C ___ _,
Xylene 23, 250U I 21 ' 1 OU
Semivolatile Oraanic (ua/ll
Bis.(2:~hl~roe!~YI) Ether .
4-Nitrophenot
lnoraanics lua/ll
Arsenic
Barium
Beryllium
· 10U
25U
soou, · ·· i2oou
1.1U 1.1u: 993 ............ 1566 i
0 30U 0.40B,
10u,
2su:
1.1 U,
is5s(
o.3ou,
4.8u:
1DU
25U
1.1 U
432
0.30U
4.8U Cadmium ...... ················ciiromium 4.8U'
4.9U'
4.8U,
4.9U
5860
15.3U:
7.08' 9.48
Manganese .. ::iilf25700j ..... ,.· _· 32 :r::11:!!':fr::i::r?t .}-1200
Nickel 15.3U' 15.3U' 15.3U ·············--·· Selenium
Zinc
1.6U,
· 1o.aiii
Water Qualitv fmo/ll
COD NIA:
Chloride ·1··1·70·,··
N~rogen (TKN) . ---NIA
TDS 2604:
Note Data Qualifier Definitions:
1.6U'
28.6!
297,
4191
NIA;
1018:
B !Organics) = Compound was detected ln the associated blank.
1.6U\
8.2B1
192'
4
NIA
265
B !Inorganic&) = Compound concentration is below the contract-required detection limit.
1.6U
3.6B
NIA
1070
NIA
2652
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace value, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
ma11 spectrometry instrument.
ND = Not detected at or above the detection limit of analysis method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates a detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30-88).
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Table 4
Groundwater Cleanup Criteria
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Compound Cleanup Concentration (ug/1)
Acetone! 3500
---Benzenel 5
Bromodichloromethane 5
Chloroform 5
............. 1.~~[)ichloroethane([)t::t\)+----5
1, 1-Dichloroethy_le~n_e+--------~7 ________ 11
1,2-DichlC>ropropane 6
Eth.yl~enzene 3500
.... Methylene _Chloride ................................................ 5 ..... .
Toluene 2000
1, 1,2-TrichloroElth.ane (T9"l .. 5
Trichloroe.thene. (TC:E:) 5
Vinyl Chloride
· X lenei
Arsenic! ----
Barium!
.. E3Elrylliuni!.
<::adniillmL
Chromium I
,1-__________ M_a_nganese:
. SEll~~4;n;\
...................
1000
17.5
10
50
7700
350
10
7350
Reference: U.S. EPA , September 30, 1988, Record of Decision (ROD) , Operable Unit No. 1,
National Starch and Chemical Company, Salisbury, North Carolina.
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Table 5
Water Level Measurerrients"
First Quarter 1996
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to Water Level
Measurement Point of Elevation Water Elevation
Well Name Date Reference (Ft. MSL) (Ft.) (Ft. MSL)
EX01
'
1/15/96 TOC 731.85 30.03 i 701.82 ·---·······-· ----------·-·-----------.. --·-·· EX02 ' 1/15/96 TOC 718.24 25.41 692.83 .................... ............... . .... ·····-------·-··· ...............
EX03 1/15/96 TOC 740.46 18.48 721.98
EX04 1/15/96 TOC 754.12 13.86 740.26 ... .,
NS05 1 /15/96 TOC 767.96 18.67 749.29
NS06 1 /15/96 TOC 738.87 5.58 733.29 _____________ ,. _______ ··-·-------------········· ---------------.... .................... .... ........ ·····-----·-•········· ·-·----············· NS21 1/15/96 TOC 739.13 5.5 733.63
NS22 1/15/96 TOC 715.94 16.33 699.61 ......... .-..
NS23 1/15/96 TOC 752.36 19.17 733.19
NS26 1/15/96 TOC 720.77 7.75 713.02 ·------.............. .............. ·······----------.-----............ .................. ........................ . ...
NS27 1/15/96 TOC 749.47 16.58 732.89 ... ..
NS28 1 /15/96 TOC 767.82 19.67 748.15 . ........ .. ....
NS29 1 /15/96 TOC 715.50 25.41 690.09 .........
NS30 1/15/96 TOC 718.54 27.72 690.82 ---·-·· ................. ........ ....•... .............. -----------·-········--·-········ NS31 1/15/96 TOC 711.15 24.58 686.57 .. .. ... ... ....
NA' NA' NS32 1/15/96 TOC 699.48
P01 1 /15/96 TOC 708.09 NAb NAb
SG1 1 /15/96 TOC 712.26 NA b NA b--•·······.
TOC NAb ·········---NAb SG2 1/15/96 693.90
-Water level measurements were taken while the extraction well system was temporarily shutdown.
NA• -Not Applicable, well is artesian.
NAb -Not Applicable, well is dry, or stream level not measured.
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Environmental Data Management, Inc.
Well Name
NS09
NS10 ··········· .. NS11
NS15
Table 6
Water Level Measurements•
First Quarter 1996
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference {Ft. MSLl {Ft.l
1/15/96 ' TOG 778.45 ' 27.83 ' ' 1 /15/96 .· ...... !QC: 786.72 31.42 ........... , ........ .......................... . .. ... .......
1/15/96 TOG 775.65 17.08
1/15/96 TOG 792.60 44.17
* -Water level measurements were taken while the extraction well system .was temporarily shutdown.
NA1 -Not Applicable, well is artesian.
NAb -Not Applicable, well is dry, or stream·level not measured.
Water Level
Elevation
{Ft. MSLl
750.62 ····-·············-··· 755.30 . ......
758.57
748.43
------·-------------.· / ' / )\':~( .·. 1' ,, ~r?i~1i\t · ,..-,~ -""'CC.Y'-• 'c;? ~;~1\( tfl) ,,~))
--j-
/
CFIOU~IDWAl~:. uo:~~~:~ ;:~: 1 1:££2 ncu~·[ 6) ~ ) (
I '
--
,_,, -) --~ ~ \
138GiJ
\ '1S28 ~+ ,,,
;,-_--"it' 6
♦
i; '
t·IS06 ~-1-i~i._ ,---
152
E.·03 ~t·J
Environmental [•ata Management, Inc.
National Starch & Chemical Company
Cedar Springs !Road
Salisbury, North Carolina
/ I
♦ Monitoring Well
-Roads, Buildings, etc.
--Fence Line
ttH+-++ Ratlroad
-Property Line
-Tributary Stream
-n~ -Topographic Contour Line
(fl., I.ISL) Contour lnt~rval = 5ft.
0 400 800 1200
~i;.J I I
Scale in Feel
Scale 1 Inch = 800 Feet
Site IVfa1p
1st Quarter Report 1996
For
Operable Units I & 2
-------------------Figure 2
Quarterly Summary of Acetone Concentration
80,000 ~------------------------
70,000 -/-------------------------
01 ::,
·= C 0 :;::;
~ -C ., u C 0 u
EDN
60,000
50,000
40,000
30,000
20,000 +-------
10,000 +-------
0-1------~
EX01
Environmental Data Management, Inc.
May 1996
EX02 EX03
3,500 ug/1
Groundwater Cleanup
EX04 NS29
Monitoring and Extraction Wells -Operable Unit No.1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
Ill! Qtr2-'95
!Ill Qtr3-'95
11111 Qtr4-'95
■ Qtr1-'96
'6000
-,
NS31
Quarterly Report For
Operable Units No. 1 & 2
1st Quarter 1996
----- - -- -- - - - ---Figure 3
Quarterly Summary of 1,2 Dichloroethane
10,000 ~-------------------------------------
1,000
= ::,
,!:
C
0 ., 100 ca ~ -C ., u C 0 u
EX01 EX02 EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
Note· Concentrations depicted at or below 5 ugll represent detection limit of laboratory
EDN
Environmenlal Data Management, Inc.
May 1996
National Starch and Chemical Company
Salisbury, North Carolina
NS30 NS31
m Qtr2-'95
IIIl Qtr3-'95
1111 Qtr4-'95
■ Qtr1-'96
5 ugfl -Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
1st Quarter 1996
-
----- - - - --- - -- -
Figure 4
Quarterly Summary of 1,2 Dichloropropane
1,000 -1-------
::: Cl ::,
·= C: 0 :;::; 100 l!! -C:
CIJ " C: 0 u
6 ug/1 -Cleanup Concentration
1
EX01 EX02 EX03 EX04 NS29 NS30
Monitoring and Extraction Wells -Operable Units No. 1
Note. Concentrations depicted at or below 6 ug/I1epresent detection hm1l of laboratory
EDN
Environmental Data Management, Inc.
May 1996
National Starch and Chemical Company
Salisbury, North Carolina
-- -
lill Qtr2-'95
IIIIQtr3-'95
1111 Qtr4-'95
■ Qtr1-'96
NS31
Quarterly Report For
Operable Units No. 1 & 2
1st Quarter 1996
-
- - - - - - --

-

-

-

-
-

-
10,000
1,000 ·
.;,
:,
·= C
0 .: 100 ca ~ -C .,
u
C 0 u
EX01
EDN
Environmental Data Management, Inc.
May 1996
EX02
Figure 5
Quarterly Summary of Bis(2-chloroethyl)ether
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
-

-

-

-

-
li!JQtr2-'95
IIIIQtr3-'95
11!1Qtr4-'95
■ Qtr1-'96
5ug/l
_ Cleanup Concentration
NS31
Quarterly Report For
Operable Units No. 1 & 2
1st Quarter 1996
- - - - -
........_ Stream
·. Gauge #2
'
+
-
·.
\
' '
\
I
--------- - ---
." EXOl
t-NS I 0
~ / I
' \
PLAHT AREA
NS30
I
v I 0 200 -100 600 ~-I
Scale in 1·eet
Scale 1 Inch = 400 Feet
Legend
Roads, Buildings, etc.
Fence Line
Property Line
~ Tributary Stream
-125-Groundwater Contour Line (Ft. MSLl
·$-Monitoring Well
\1 Stream Gauge
\
Slream
Gauge #1
I
I
National Starch & Chemical Company
Cedar Springs Road
Salisbury, Horth Carolina
Environmental Data Management, Inc.
Figure 6
Groundwater Contour Map
for January 15, 1996
Isl Quarter Report 1996
For
Operable Units I & 2
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Appendix A
I Report of Laboratory Analysis
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REPORT OF LABORATORY ANALYSIS
February 14, 1996
Mr. Ken Kluttz
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 28144
RE: PACE Project No. 660116.507
Client Reference: CLP Quarterly Monitoring
Dear Mr. Kluttz:
Enclosed is the report of laboratory analyses for samples received
January 16, 1996.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us ..
Sincerely,
~~o~J:lorr
Project Manager
Enclosures
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
An Equal Opportunity Employer
0
0
0 National Starch & Chemical
P.O. Box 399
Salisbury, NC 28144
REPORT OF LABORATORY ANALYSIS
Company February 14, 1996
PACE Project Number: 660116507
fl Attn: Mr. Ken Kluttz
Client Reference: CLP Quarterly Monitoring
I PACE Sample Number:
Date Co 11 ected: m Date Received:
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride I
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Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 7()4.a75-9092
FAX: 704.a75.9091
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
3.0
0. 1
5
92 0535499
01/15/96
01/16/96
EX-01
----
19
59
0.6
382
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
4078
351. 3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01 /18/96
01/29/96.
01/26/96
01/25/96
01/22/96
An Equal Opportunity Em~oyer
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Mr. Ken Kluttz
Page 2
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
I
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
3
0 .1
5
92 0535502
01/15/96
01/16/96
EX-01
Dup METHOD DATE ANALYZED
BDR
60
0.4
356
DONE
DONE
DONE
8000
407B
351. 3
160.I
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01/25/96
01/18/96
01/26/96
01/25/96
01/22/96
An Equal Opportuni1y Employer
0
D
0 Mr. Ken Kluttz
Page 3
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507
u Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
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INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS·
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 704-87s-9092
FAX: 704-675·9091
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
3
0 .1
5
92 0535510
01/15/96
01/16/96
EX-01
Matrix METHOD DATE ANALYZED
BDR
59
0.2
293
DONE
DONE
DONE
8000
407B
351. 3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01/25/.96
01/18/96
01/26/96
01/25/96
01/22/96
An Equal Opportunity Em~oyer
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RPQRATED
ENVIRONIIEHTAL LABORATOR1ES
Mr. Ken Kluttz
Page 4
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Su~e 100
Huntersville, NC 28078
TEL: 7044!75'9092
FAX: [phone]
Units
mg/L
mg/L
3
5
MDL
92 0535529
01/15/96
01/16/96
NS-29
____ METHOD DATE ANALYZED
745
2678
DONE
DONE
DONE
4078
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/29/96
01/29/96
01/29/96
An Equal Opportunrty Employer
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REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 5
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Sutte 100
Huntersville, NC 28078
TEL: TI>W7;.9092
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
3
0 .1
5
February 14, 1996
PACE Project Number: 660116507
92 0535537
01/15/96
01/16/96
EX-03
____ METHOD DATE ANALYZED
440
262
1.5
1265
DONE
DONE
DONE
8000
407B
351.3
160 .1
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
0.1/25/96
01 /18/96
01/26/96
01/25/96
01/22/96
An Equal Opportu,ity Employer
0
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 6
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter Units
I INORGANIC ANALYSIS
I
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0
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INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 704-ll75-9092
FAX: 704-875·9091
mg/L
mg/L
3
1
MDL
February 14, 1996
·PACE Project Number: 660116507
92 0535545
01/15/96
01/16/96
NS-32
____ METHOD DATE ANALYZED
9
98
DONE
DONE
DONE
4078
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/29/96
01/29/96
01/29/96
An Equal Opportunity Employer
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REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 7
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Units
Chemical Oxygen Demand mg/L
Chloride mg/L
Nitrogen, Kjeldahl mg/L
Solids, Total Dissolved mg/L
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 704-<!75-9092
FAX: 704-675·9091
MDL
10
3
0 .1
5
February 14, 1996
PACE Project Number: 660116507
92 0535553
01/15/96
01/16/96
EX-04
----
79
117
I. 5
392
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351. 3
160. I
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01/25/96
01/18/96
01/26/96
01/23/96
01/26/96
An Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 8
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
MDL
20
3
0. 1
5
February 14, 1996
PACE Project Number: 660116507
92 0535561
01/15/96
01/16/96
EX-02
----
1370
1080
7.3
2978
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
4078
351.3
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/24/96
01/25/96
01/18/96
01/26/96
01 /23/96
01/26/96
AA Equal Opportunity ~oyer
El
ENVIRONMENTAL LABORATORIES
0 Mr. Ken Kluttz
Page 9
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507 o Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
0 Date Collected:
Date Received:
Client Sample ID:
I
m
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved I Target Analyte List -lnorganics
ORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles I Target Compounds List -Volatiles
I
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9800 Kincey Avenue Suite 100
Huntersvil!e, NC 2B078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
MDL
10
3
5
92 0535570
01/15/96
01/16/96
NS-11
----
192
4
265
DONE
DONE
DONE
METHOD DATE-ANALYZED
8000
407B
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01/ 18/9.6
01/26/96
01/23/96
01 /25/96
An Equal Opportunity Employer
cw
ENVIRONMENTAL LABORATORIES
0 Mr. Ken Kluttz
Page 10
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507
I Client Reference: CLP Quarterly Monitoring
92 0535588
01/15/96
01 /16/96
NS-09 I
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PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
HuntelSVille, NC 28078
TEL: [phone]
FAX: 704-a75-9091
Units
mg/L
mg/L
MDL
3
5
____ METHOD DATE ANALYZED
1170
2604
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/29/96
01/24/96
01/26/96
"'1 Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 11
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 7DW75-9092
FAX: [phone]
Units
mg/L
mg/L
mg/L
MDL
10
3
5
February 14, 1996
PACE Project Number: 660116507
92 0535596
01/15/96
01/16/96
NS-10
----
297
419
1018
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/17/96
01/24/96
01/18/96
01 /26/96
01/24/96
01 /26/96
AA Equal Opportunity Em~oyer
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ENVIRONMENTAi.. LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 12
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: 704-875•9091
Units
mg/L
mg/L
3
5
MDL
February 14, 1996
PACE Project Number: 660116507
92 0535600
01/15/96
01/16/96
NS-15
____ METHOD DATE ANALYZED
1070
2652
DONE
DONE
DONE
407B
160.l
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/26/96
01/24/96
01/26/96
AIi Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES
n Mr. Ken Kluttz
Page 13
REPORT OF LABORATORY ANALYSIS
February 14, 1996
PACE Project Number: 660116507
u Client Reference: CLP Quarterly Monitoring
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PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
3
5
MDL
92 0535618
01/15/96
01/16/96
NS-31
____ METHOD DATE ANALYZED
181
954
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/26/96
01/29/96
01/26/96
An Equal Opportunity Employer
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ENVIAONMEHTAL LABORATOfflES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 14
Client Reference: CLP Quarterly Monitoring
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
Units
mg/L
mg/L
3
5
MDL
These data have been reviewed and are approved for release.
£21/ Dan H. Jones
Inorganic Department
Margaret S. Harding
Manager, Organic Chemistry
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
February 14, 1996
PACE Project Number: 660116507
92 0535626
01/15/96
01/16/96
NS-30
____ METHOD DATE ANALYZED
72
375
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
01/24/96
01/18/96
01/26/96
01/29/96
01/25/96
/VI Equal 0pportun;ty Employer
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Page I 5
REPORT OF LABORATORY ANALYSIS
FOOTNOTES February 14, 1996
for pages I through 14 PACE Project Number: 660116507
I Client Reference: CLP Quarterly Monitoring
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MDL Method Detection Limit
9800 KillCey Avenue Suite 100
Huntersville, NC 28078
TEL: 70W75-9092
FAX: [phone]
AA Equal Oppoounity Employer
D REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA February 14, 1996 ,n· Mr. Ken Kluttz
Page 16 PACE Project Number: 660116507
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Client Reference: CLP
Chemical
Batch:
Oxygen Demand
92 42949
Quarterly Monitoring
Samples: 92 0535499, 92 0535502,
92 0535570, 92 0535596
92 0535510, 92 0535537, 92 0535553
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 70W75-9092
FAX: [phone]
Units
mg/L
Units
mg/L
Units
mg/L
MDL
To
MDL
To
MDL
To
Method
Blank
ND
Duplicate
920535499 of
~EX;;.--...:0-=-l __ 92 0535499
19 24
920535499 Spike
Recv
101%
EX-01 Spike
19 500
Reference
Value
500
Recv
101%
An Equ~ Oppor\\Jni\y Em~oyer
RPO
23%
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REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 17
QUALITY CONTROL DATA
Client Reference: CLP Quarterly Monitoring
Chemical Oxygen Demand
Batch: 92 43115
Samples: 92 0535561
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 704,U5-9092
FAX: [phone]
Units
mg/L
mg/L
Units
mg/L
Units
mg/L
MDL'
To
40
MDL
40
MDL
To
February 14, 1996
PACE Project Number: 660116507
Method
Blank 92053B560
ND
3320
920538560
3320
s p _i_l<_e_
2oOO
Reference
Value
500
Duplicate
of
92 0538560
3280
Spike
Recv
101%
Recv
102%
AA Equal Opportunny Employer
RPD
1%
D
I REPORT OF LABORATORY ANALYSIS
'I, Mr. Ken Kluttz
Page 18
FOOTNOTES
for pages 16 through 17
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Client Reference: CLP Quarterly Monitoring
MDL Method Detection Limit
ND Not detected at or above the MDL.
RPD Relative Percent Difference
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
TEL: 704-87S-9092
FAX: 704-875·9091
February 14, 1996
PACE Project Number: 660116507
AA Equal Opportunity Employer
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Appendix B
Sample Delivery Group Narrative
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February 14, 1996
Mr. Ken Kluttz
National Starch and Chemical Co.
485 Ceder Springs Road
Salisbury, NC 28144
PACE Project No. 660116.507
Sample receipt:
CASE NARRATIVE
A total of fourteen water samples were received at the Pace laboratory in Huntersville, NC on
1/16/96 .. The samples were logged into the Laboratory Data Management System and PACE
laboratory sample numbers were assigned to the samples. Samples were then shipped via
Federal Express on 1/16/96 to the PACE-Houston, Texas facility for analysis.
Sample ID PACE -Charlotte ID PACE -Houston ID
EX-01 92 053549.9 H420740
EX-01 DUP 92 053550.2 H420741
EX-0 I Matrix 92053551.0 H420742
NS-29 92 053552.9 H420743
EX-03 92 053553.7 H420744
NS-32 92 053554.5 H420745
EX-04 92 053555.3 H420746
EX-02 92 053556.1 H420747
NS-I I 92 053557.0 H420748
NS-09 92 053558.8 H420749
NS-10 92 053559.6 H420750
NS-15 92 053560.0 H420751
NS-31 92 053561.8 H420752
NS-30 92 053562.6 H420753
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Sample Receipt:
CASE NARRATIVE
FOR
PACE ANALYTICAL SERVICES, INC. CHARLOTTE
ORGANICS/ INORGANICS
MATRIX: WATER
The PACE Charlotte project was submitted for arsenic and selenium to be analyzed by CLP
SOW ILM03.0 on Graphite Furnace Atomic Absorption (GFAA). Barium, beryllium, cadmium,
chromium, manganese, nickel and zinc were submitted to be analyzed by CLP SOW ILM03.0 on
ICP. Volatile and semivolatile analysis were submitted to be analyzed by CLP SOW OLM0!.9.
Samples were received by PACE Analytical Services, Inc. on O 1/17 /96. The Inorganic data
• package has a Case Number identified as "PCHAR" and the SDG is identified on the CLP forms
as "PACI".
lnorganics:
Samples were digested for CLP SOW ILM03.0 methodology for water. Samples were digested
on 01/25/96 for analysis by ICP. Samples were digested on 01/26/96 for analysis by GFAA.
Data calculations of Form I through 14 were performed using Telecation Associates software
(Enviroforms and Version 3.13 Smartlog) for the ILM03.0 protocols. Occasional differences in
rounding are encountered due to initial rounding of the numerical data by this software. The
effects of this rounding are considered minor and no serious errors in the final data are expected.
The EPA views the use of this software as satisfactory for CLP-type data package generation.
The sources for LCS, ICY, CCV, and calibration standards are High Purity, Inorganic Ventures,
Environmental Resource Associates and Spex. The abbreviations for these sources appear on
the appropriate CLP-type forms in the data package. The abbreviations listed are HP (High
Purity), IV (Inorganic Ventures), ERA (Environmental Resource Associates) and SPEX (Spex).
See enclosed list for definitions of flags.
The samples, matrix spike and duplicate were prepared and analyzed within the hold time period
for this package.
Volatile & Semivolatile Organics:
Although temperature blanks were not received, the samples were shipped with ice and ice packs
and the temperature of the cooler measured at 4.8 degrees C. The sample received met the EPA
requirements for containers and sample integrity.
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The calibration check compounds (CCCs), the system performance check compounds (SPCCs),
and the internal standard1areas all met method criteria. A method blank and a laboratoiy control
sample were analyzed wi~h each analytical sample batch set of20 or fewer samples. A matrix
spike and a matrix spike duplicate were analyzed with this sample.
Sample with ID 92-053~61-8 was extracted and analyzed, in hold, on 1/24/96. However, four
surrogate recoveries we~e outside of the contract recovery limits. The sample was re-extracted
outside of hold time and reanalyzed; both sets of data are presented.
I
Sample with ID 92-053~58-8 was originally analyzed on 1/23/96. Due to matrix interference,
internal standard recoveries were outside of the SOW required recoveries. The sample was
diluted and reanalyzed th.e reanalysis met all internal standard recoveiy requirements.
All raw data have been included in the data•·package.
, David Rose-Metals Gro~p Leader
&;cwee~ ..
lissell Morgan-Operions Manager
~"----G.~0~~ ...... --"
Emmanuel Young-Organiics Manager
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Appendix C
Volatile Organics Analysis Data Sheets
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
cX-Oi
92 053549 9
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No.: PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab Sample ID: 8420740
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVP01259601
Level: (low/med) LOW Date Received: 01/17/96
% Moisture: not dee. Date Analyzed: 01/25/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON Contract:
Lab Code: PACE Case No.: PACE SAS No.:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (uL)
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Ex-01 Dli(
92_053550_2
No.: PKG5
H420741
UVP01259602
01/17/96
01/25/96
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroforrn 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5-----~---1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO .
t:>< -QI i1,trP.1 I(
92 053551 0
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No. : PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab Sample ID: H420742
Sample wt/vol: 5. 0 (g/mL) ML Lab File ID: UVP01259603
Level: (low/med) LOW Date Received: 01/17/96
% Moisture: not dee. Date Analyzed: 01/25/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4------~--Vinyl Chloride 10 u
75-09-2-~-------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 0.9 J
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (UL)
Contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
6<.-0L
92 053556 1
No.: PKG5
H420747
UVP01269605
01/17/96
01/26/96
Dilution Factor: 100.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 1000 u
75-09-2---------Methylene Chloride 150 BJ
67-64-1---------Acetone 10000
75-35-4---------1,1-Dichloroethene 500 u
67-66-3---------chloroform 500 u
107-06-2--------1,2-Dichloroethane 1200
75-27-4---------Bromodichloromethane 500 u
78-87-5---------1,2-Dichloropropane 830
79-01-6---------Trichloroethene 500 u
79-00-5---------1,1,2-Trichloroethane 500 u
71-43-2---------Benzene 500 u
108-88-3--------Toluene 290 J
100-41-4--------Ethylbenzene 500 u
1330-20-7-------xylene (total) 500 u
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: s.o (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (uL)
contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
6(-03
92 053553 7
No.: PKGS
H420744
UVP01269603
01/17/96
01/26/96
Dilution Factor: 100.0
Soil Aliquot Volume: {UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 1000 u
75-09-2---------Methylene Chloride 160 BJ
67-64-1---------Acetone 5800
75-35-4---------1,1-Dichloroethene 500 u
67-66-3---------Chloroforrn 500 u
107-06-2--------1,2-Dichloroethane 150 J
75-27-4---------Bromodichloromethane 500 u
78-87-5---------1,2-Dichloropropane 140 J
79-01-6---------Trichloroethene soc u
79-00-5---------1,1,2-Trichloroethane 500 u
71-43-2---------Benzene 500 u
108-88-3--------Toluene 130 J
100-41-4--------Ethylbenzene 500 u
1330-20-7-------Xylene (total) 500 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (uL)
Contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
5(-04
92 053555 3
No.: PKG5
H420746
UVP01269601
01/17/96
01/26/96
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 9 J
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 4 J
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 2 J
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (uL)
Contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
NS-o'!
92_053558 8
No.: PKG5
H420749
UVP01269607
01/17/96
01/26/96
Dilution Factor: 2.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 62
75-09-2---------Methylene Chloride 10 u
67-64-1---------Acetone 7 J
75-35-4---------1,1-Dichloroethene 9 J
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 9 J
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
79-01-6---------Trichloroethene 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
108-88-3--------Toluene 180
100-41-4--------Ethylbenzene 10
1330-20-7-------Xylene (total) 23
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Ns-10
92 053559 6
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No.: PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab Sample ID: H420750
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVP0l269606
Level: (low/med) LOW Date Received: 01/17/96
% Moisture: not dee. Date Analyzed: 01/26/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 50.0
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 500 u
75-09-2---------Methylene Chloride 73 BJ
67-64-1---------Acetone 500 u
75-35-4---------l,l-Dichloroethene 250 u
67-66-3---------Chloroform 250 u
107-06-2--------l,2-Dichloroethane 6100
75-27-4---------Bromodichloromethane 250 u
78-87-5---------l,2-Dichloropropane 250 u
79-01-6---------Trichloroethene 250 u
79-00-5---------l,l,2-Trichloroethane 250 u
71-43-2---------Benzene 250 u
108-88-3--------Toluene 250 u
100-41-4--------Ethylbenzene 250 u
1330-20-7-------Xylene (total) 250 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET ~s -II
92 053557 0
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No. : PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab sample ID: H420748
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVP01259604
Level: (low/med) LOW Date Received: 01/17/96
% Moisture: not dee. Date Analyzed: 01/25/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 9
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 6
100-41-4--------Ethylbenzene 62
1330-20-7-------Xylene (total) 21
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS-15'
92 053560 0
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No. : PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab Sample ID: H420751
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVP01269602
Level: (low/med) LOW Date Received: 01/17/96
% Moisture: not dee. Date Analyzed: 01/26/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 2.0
Soil Extract Volume: (UL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 20 u
75-09-2---------Methylene Chloride 3 BJ
67-64-1---------Acetone 20 u
75-35-4---------1,1-Dichloroethene 10 u
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 250
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
79-01-6---------Trichloroethene 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
108-88-3--------Toluene 11
100-41-4--------Ethylbenzene 10 u
1330-20-7-------Xylene (total) 10 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP
Soil Extract Volume:
ID: 0.530 (mm)
(uL)
Contract:
SAS No.:
NS-.29
92 053552 9
CHARLOTTE
SDG No.: PKG5
Lab Sample ID: H420743
Lab File ID: UVP01269604
Date Received: 01/17/96
Date Analyzed: 01/26/96
Dilution Factor: 100.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 1000 u
75-09-2---------Methylene Chloride 150 BJ
67-64-1---------Acetone 12000
75-35-4---------1,1-Dichloroethene 500 u
67-66-3---------Chloroform 500 u
107-06-2--------1,2-Dichloroethane 860
75-27-4---------Bromodichloromethane 500 u
78-87-5---------1,2-Dichloropropane 1600
79-01-6---------Trichloroethene 500 u
79-00-5---------1,1,2-Trichloroethane 500 u
71-43-2---------Benzene 500 u
108-88-3--------Toluene 370 J
100-41-4--------Ethylbenzene 500 u
1330-20-7-------Xylene (total) 500 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP
Soil Extract Volume:
ID: 0.530 (mm)
(UL)
Contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
/VS •2Q
92 053562 6
No.: PKGS
H420753
UVP01259606
01/17/96
01/25/96
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,l-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP
Soil Extract Volume:
ID: 0.530 (mm)
(uL)
contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
NS-3i
92_053561 8
No.: PKG5
H420752
UVP01269608
01/17/96
01/26/96
Dilution Factor: 50.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 500 u
75-09-2---------Methylene Chloride 71 BJ
67-64-1---------Acetone 3500
75-35-4---------1,1-Dichloroethene 250 u
67-66-3---------Chloroform 250 u
107-06-2--------1,2-Dichloroethane 250 u
75-27-4---------Bromodichloromethane 250 u
78-87-5---------1,2-Dichloropropane 250 u
79-01-6---------Trichloroethene 250 u
79-00-5---------1,1,2-Trichloroethane 250 u
71-43-2---------Benzene 250 u
108-88-3--------Toluene 64 J
100-41-4--------Ethylbenzene 250 u
1330-20-7-------Xylene (total) 250 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
\ Moisture: not dee.
GC Column: CAP ID: 0.530 (mm)
Soil Extract Volume: (uL)
Contract:
SAS No.:
CHARLOTTE
SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
NS-3.2
92 053554 5
No.: PKG5
H420745
UVP01259605
01/17/96
01/25/96
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 B~
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP
Soil Extract Volume:
ID: 0.530 (mm)
(uL)
Contract:
SAS No.:
VBLKUA
CHARLOTTE
SDG No.: PKG5
Lab Sample ID: H363163
Lab File ID: UVB01259601
Date Received:
Date Analyzed: 01/25/96
Dilution Factor: 1.0
Soil Aliquot Volume: (UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 J
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-B8-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLKUB
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No.: PACE SAS No.: SDG No.: PKG5
Matrix: (soil/water) WATER Lab Sample ID: H363165
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVB01269601
Level: (low/med) LOW Date Received:
% Moisture: not dee. Date Analyzed: 01/26/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 2 J
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
108-88-3--------Toluene 5 u
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dee.
GC Column: CAP
Soil Extract Volume:
ID: 0.530 (mm)
(uL)
Contract:
SAS No.:
920535499MS
CHARLOTTE
SDG No.: PKG5
Lab Sample ID: H420740MS
Lab File ID: UVP01259615
Date Received: 01/17/96
Date Analyzed: 01/26/96
Dilution Factor: 1.0
Soil Aliquot Volume: {UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 4 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,l-Dichloroethene 35
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 39
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 48
108-88-3--------Toluene 45
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
920535499MSD
Lab Name: PACE HOUSTON Contract: CHARLOTTE
Lab Code: PACE Case No.: PACE SAS No.: SDG No.: PKGS
Matrix: (soil/water) WATER Lab Sample ID: H420740MSD
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: UVP01259616
Level: (low/med) LOW Date Received: 01/17/96
't Moisture: not dee. Date Analyzed: 01/26/96
GC Column: CAP ID: 0.530 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: {UL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-01-4---------Vinyl Chloride 10 u
75-09-2---------Methylene Chloride 4 BJ
67-64-1---------Acetone 10 u
75-35-4---------1,1-Dichloroethene 34
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
79-01-6---------Trichloroethene 41
79-00-S---------l,l,2-Trichloroethane 5 u
71-43-2---------Benzene so
108-88-3--------Toluene 47
100-41-4--------Ethylbenzene 5 u
1330-20-7-------Xylene (total) 5 u
---
FORM I VOA 3/90
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Appendix D
Semivolatile Organics Analysis Data Sheets
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
/;:x-01
92 053549 9
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
{uL)
Lab Sample ID: H420740
Lab File ID: SBP01229602
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/22/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7. 0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether 9
100-02-7--------4-Nitrophenol 25
FORM I SV-1
Q
J
u
---
3/90
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18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET a
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: .(Y/N) N pH:
CAS NO. COMPOUND
&-oi Dul>
92 53550 2 --Contract: CHARLOTTE
SAS No.: SDG No. : PKG5
(uL)
7.0
Lab Sample ID:
Lab File ID:
H420741
SBP01229603
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/22/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 10
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
\ Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
t:K-01 fJl,Hf!/X,
92 053551 0
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.1
Lab Sample ID: H420742
Lab File ID: SBP01229604
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/22/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
111-44-4--------bis(2-Chloroethyl)Ether 9 J
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: ( Y /N) N pH:
CAS NO. COMPOUND
fx-OZ.
92 53556 1
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.2
Lab Sample ID:
Lab File ID:
H420747
SBP01239605
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/23/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
20.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 400
100-02-7--------4-Nitrophenol 500 u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume:
Ex-03
92 053553 7
Contract: CHARLOTTE
SAS No.: SDG No.: PKGS
(uL)
Lab_ Sample ID: H420744
Lab File ID: SBP01239607
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/23/96
Dilution Factor: 2.0
GPC Cleanup: (Y/N) N
CAS NO.
pH: 7.1
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
111-44-4--------bis(2-Chloroethyl)Ether 130
100-02-7--------4-Nitrophenol so u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Ex-o+
92 53555 3
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: ( Y /N) N pH:
CAS NO. COMPOUND
Contract: CHARLOTTE
SAS No.: SDG No. : PKG5
(uL)
7.2
Lab Sample.ID:
Lab File ID:
H420746
SBP01239604
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/23/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 10
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
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18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
N5>-u9
92 053558 8
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.2
Lab Sample ID: H420749
Lab File ID: SBP01239608
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/23/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
111-44-4--------bis(2-Chloroethyl)Ether 10 u
100-02-7--------4-Nitrophenol ', 25 u
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
I Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS-O'/ DL
92 053558 8DL - -Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.2
Lab Sample ID: H420749DL
Lab File ID: SBP01249601
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/24/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
3.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 30 u
100-02-7--------4-Nitrophenol 75 u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Ns-10
92_053559 6
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Contract: CHARLOTTE
SAS No.: SDG No. : PKGS
Lab Sample ID: H420750
Sample wt/vol: 1000 (g/mL) ML Lab File ID: SBP01249602
Level: (low/med) LOW
i Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: 7. 3
CAS NO. COMPOUND
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/24/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
so.a
Q
lll-44-4--------bis(2-Chloroethyl)Ether 500 u
100-02-7--------4-Nitrophenol 1200 u
---
FORM I SV-1 3/90
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
/'15-11
92 53557 0
Contract: CHARLOTTE
SAS No.: SDG No. : PKG5
Lab Sample ID: H420748
(UL)
7.1
Lab File ID: SBP01239606
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/23/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
111-44-4--------bis(2-Chloroethyl)Ether 10 u
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
1:
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I:
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS -15
92 053560 0
Contract: CHARLOTTE
SAS No.: SDG No. : PKG5
Lab Sample ID: H420751
(uL)
7.2
Lab File ID: SBP01249603
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/24/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 10 u
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
I.
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: ( Y /N) N pH:
CAS NO. COMPOUND
t/S--.J'I
92 053552 9
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.2
Lab Sample ID:
Lab File ID:
Date Received:
H420743
SBP01229607
01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/22/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
lll-44-4--------bis(2-Chloroethyl)Ether 470 E
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
I
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I
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
,\&.Jt OL
92_053552_9DL
Contract: CHARLOTTE
SAS No.: SDG No. : PKGS
Lab Sample ID: H420743DL
Lab File ID: SBP01239603
Date Received: 01/17/96
Date Extracted: 01/19/96
(uL) Date Analyzed: 01/23/96
7.2
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
so.a
Q
lll-44-4--------bis(2-Chloroethyl)Ether 590 D
100-02-7--------4-Nitrophenol 1200 u
FORM I SV-1 3/90
I
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS 0 3U
92 053562 6
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(UL)
7.2
Lab Sample ID: H420753
Lab File ID: SBP01299603
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/29/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
lll-44-4--------bia(2-Chloroethyl)Ether 5 J
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
I
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I
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I
I,
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1,
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
NS-3i
92 053561 8
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
Lab Sample ID: H420752
(uL)
7.2
Lab File ID: SBP01249604
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/24/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
111-44-4--------bis(2-Chloroethyl)Ether 41
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
I
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
/JS-31 £e_
Lab Name: PACE HOUSTON
Lab Code: PACE Case No.: PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
\ Moisture: decanted: ( Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
92 053561 BRE
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
Lab Sample ID:
Lab File ID:
Date Received:
H420752RE
SBP01299602
01/17/96
Date Extracted: 1/25/96
Date Analyzed: 01/29/96
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH: 7. 2
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
111-44-4--------bis(2-Chloroethyl)Ether 72
100-02-7--------4-Nitrophenol 25
FORM I SV-1
Q
u
---
3/90
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3
B
0
1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: PACE HOUSTON
Lab Code: PACE Case No. : PACE
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: decanted: (Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
NS-32.
92 053554 5
Contract: CHARLOTTE
SAS No.: SDG No.: PKG5
(uL)
7.3
Lab Sample ID:
Lab File ID:
H420745
SBP01229609
Date Received: 01/17/96
Date Extracted: 01/19/96
Date Analyzed: 01/22/96
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1.0
Q
111-44-4--------bis(2-Chloroethyl)Ether 10 u
100-02-7--------4-Nitrophenol 25 u
---
FORM I SV-1 3/90
I
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0
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Appendix E
Inorganics Analysis Data Sheets
I
I ENVIROFORMS/INORGANIC CLP
1
,111110001
SAMPLE NO.
I Lab Name: PACE INC.
INORGANIC ANALYSIS DATA SHEET
PCEXOl
Contract: PACE CHAR.
I
I
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
100.0
SAS No. : SDG No. : PACl
Lab Sample ID: H420740
Date Received: 01/17/96
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
R
u
n
B
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lcolor After: COLORLESS
. Comments: I CLIENT ID: EXOl
I
Analyte Concentration C
-Aluminum -Antimony -Arsenic 1.1 u -Barium 104 B
Beryllium 0.30 u
Cadmium 4.8 u -Calcium -Chromium -7.7 B -Cobalt -Copper -Iron -Lead -Magnesium -Manganese 142 -Mercury
Nickel . 15.3 u -Potassium
Selenium 1.6 u -Silver -Sodium -Thallium -Vanadium -Zinc 7.6 B -Cyanide -
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
F
p
p
p
NR
p
NR
NR
NR
NR -NR
E p
NR
p
NR
w F
NR
NR
NR
NR
p
NR -
Texture:
Artifacts:
I
I
I
I
I
I
I
ti
m
0
0
u
D
I)
I
ENVIROFORMS/INORGANIC CLP
1
(10fl(l0()2
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE INC.
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
100.0
PCEX02
Contract: PACE CHAR.
SAS No.: SDG No.: PACl
Lab Sample ID: H420747
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C
-7429-90-5 Aluminum -7440-36-0 Antimony
7440-38-2 Arsenic 1.1 u
7440-39-3 Barium -1970
7440-41-7 Beryllium 0.30 u
7440-43-9 Cadmium 4.8 u
7440-70-2 Calcium -
-7440-47-3 Chromium 4.9 u -7440-48-4 Cobalt -7440-50-8 Copper -7439-89-6 Iron -7439-92-1 Lead -Magnesium 7439-95-4 -7439-96-5 Manganese 17900 -7439-97-6 Mercury -7440-02-0 Nickel 15.3 u
7440-09-7 Potassium -
-7782-49-2 Selenium 3.2 u
7440-22-4 Silver -
7440-23-5 Sodium -
-7440-28-0 Thallium
7440-62-2 Vanadium -
7440-66-6 zlnc 14.3 B
cyanide -
-
Color Before: COLORLESS Clarity Before: CLEAR
Q
E
M
NR -NR
F
p
p
p
N
p
N
N
N
N
N
p
N
p
N
F
N
N
N
N
R
R
R
R
R
R
R
R
R
R
R
R
p
N R
Texture:
m Color After: COLORLESS Clarity After: CLEAR Artifacts:
I Comments:
CLIENT ID: EX02
I FORM I -IN
I
I
I
I
I
I
D
D
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
(1()11(1()()3
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE INC.
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
100.0
PCEX03
Contract: PACE CHAR.
SAS No.: SDG No.: PACl
Lab Sample ID: 8420744
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
-7429-90-5 Aluminum NR
7440-36-0 Antimony -NR
7440-38-2 Arsenic 1.1 u F
7440-39-3 Barium 553 -p
7440-41-7 Beryllium 0.30 -u p
7440-43-9 Cadmium 4.8 u p
7440-70-2 Calcium -NR
7440-47-3 Chromium -7. 8 --B p
7440-48-4 Cobalt - -NR - -7440-50-8 Copper NR - -7439-89-6 Iron NR - -7439-92-1 Lead NR
Magnesium -7439-95-4 NR --7439-96-5 Manganese 2130 E p -7439-97-6 Mercury NR
7440-02-0 Nickel 15.3 u p
7440-09-7 Potassium -NR
7782-49-2 Selenium 1.6 u F
7440-22-4 Silver -NR
Sodium -7440-23-5 NR
7440-28-0 Thallium -NR
7440-62-2 Vanadium -NR
7440-66-6 Zinc 9.0 B p
cyanide -NR --
Color Before: COLORLESS Texture: I Color After: COLORLESS
Comments:
Clarity Before: CLEAR
Clarity After: CLEAR Artifacts:
I CLIENT ID: EX03
I FORM I -IN
I
I
I
I
I
I
R
n
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
PCEX04 Lab Name: PACE INC.
Lab Code:
Contract: PACE CHAR.
Case No.: PCHAR SAS No.: SDG No.: PACl
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW·
100.0
Lab Sample ID: H420746
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
CLIENT ID: EX04
Analyte Concentration C
Aluminum -
Antimony -
Arsenic 1.1 u
Barium 35.4 B
Beryllium 0.45 B
Cadmium 4.8 u
Calcium -
Chromium -7.4 B
Cobalt -
Copper -
Iron -
Lead -
Magnesium -
-Manganese
Mercury
3580 -
Nickel 15.3 u
Potassium -
Selenium -1. 6 u
Silver -
Sodium -
Thallium -
Vanadium -
Zinc -15.6 B
cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR -NR
F
p
p -p -NR
p
NR
NR
NR
NR -NR
E p
NR
p -NR
w F
NR
NR
NR
NR
p
NR -
Texture:
Artifacts:
I
I
I
I
I
I
B
D
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract: PACE CHAR.
SAMPLE NO.
PCNS09
Lab Name: PACE INC.
Lab Code: Case No. : PCHAR SAS No.: SDG No.: PACl
Matrix (soil/water): WATER
Level (low/med): LOW
I Solids: 100.0
Lab Sample ID: H420749
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic 1.1
7440-39-3 Barium 993
7440-41-7 Beryllium 0.30
7440-43-9 Cadmium 4.8
7440-70-2 Calcium
7440-47-3 Chromium 4.9
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese 25700
7439-97-6 Mercury
7440-02-0 Nickel 15.3
7440-09-7 Potassium
7782-49-2 Selenium 1.6
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc 10.8
cyanide
C Q
-
-
u -
u -u -
u -
-
-
-
-
-E -
-u -
-u w -
-
-
-
B -
-
M
N
N
R
R
F
p
p
p
N
p
N
N
N
N
N
R
R
R
R
R
R
p
N
p
N
F
N
N
N
N
p
N
R
R
R
R
R
R
R
Color I Color
Before: COLORLESS
After: COLORLESS
Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
Artifacts:
I Comments:
CLIENT ID: NS09
I FORM I -IN
I
I
I
I
I
I
I
I
D
D
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
(!iHIO(H)6
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE INC.
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 100.0
PCNSlO
Contract: PACE CHAR.
SAS No.: SDG No.: PACl
Lab Sample ID: H420750
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
7429-90-5 Aluminum --NR
Antimony --7440-36-0 NR -7440-38-2 Arsenic 1.1 u F
7440-39-3 Barium 156 -B p
7440-41-7 Beryllium 0. 40 B p
7440-43-9 Cadmium 4.8 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 4.9 u p
7440-48-4 Cobalt -NR
7440-50-8 -Copper NR -7439-89-6 Iron NR
7439-92-1 Lead - -NR
Magnesium --7439-95-4 NR -7439-96-5 Manganese 5860 E p -7439-97-6 Mercury NR -7440-02-0 Nickel 15.3 u p
7440-09-7 Potassium --NR
7782-49-2 Selenium 1.6 --u F
7440-22-4 Silver -NR
7440-23-5 Sodium -NR
7440-28-0 Thallium -NR
7440-62-2 Vanadium -NR
7440-66-6 Zinc 28.6 -p
Cyanide -NR --
Color Texture: I color
Before: COLORLESS
After: COLORLESS
Clarity Before: CLEAR
Clarity After: CLEAR Artifacts:
I Comments:
CLIENT ID: NSlO
I FORM I -IN
Lab Name: PACE INC.
Lab Code:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract: PACE CHAR.
(!1):10007
SAMPLE NO.
PCNSll
Case No. : PCHAR SAS No.: SDG No.: PACl
I
I
I
I
I
I
I
I
g
Matrix (soil/water): WATER Lab Sample ID: H420748
Date Received: 01/17/96 Level (low/med): LOW
% Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
8
u
•
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lcolor After: COLORLESS
Comments: I CLIENT ID: NSll
I
Analyte Concentration C
Aluminum -
Antimony -
Arsenic 1.1 u
Barium 156 B
Beryllium -0.30 u
Cadmium 4.8 u
Calcium -
Chromium -7.0 B -Cobalt -Copper -Iron -Lead
Magnesium -
-Manganese 32.0 -Mercury -Nickel 15.3 u
Potassium -
Selenium -1.6 u
Silver -
Sodium -
Thallium -
Vanadium -
Zinc 8.2 B
cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E
w
M
NR
NR
F
p
p
p
NR
p
N
N
N
N
N
p
N
p
N
F
N
N
N
N
p
N
R
R
R
R
R
R
R
R
R
R
R
R
Texture:
Artifacts:
I
I
I
I
I
I
I
I
I
I
I
I
D
0
ENVIROFORMS/INORGANIC CLP
1
l't)l)(l()(l8
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE INC.
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 100.0
PCNS15
Contract: PACE CHAR.
SAS No.: SDG No.: PACl
Lab Sample ID: H420751
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
Antimony --7440-36-0 NR
7440-38-2 Arsenic 1.1 u F
7440-39-3 Barium 432 -p
7440-41-7 Beryllium 0.30 u p
7440-43-9 Cadmium 4.8 u p
7440-70-2 Calcium -NR
7440-47-3 Chromium -9. 4 B p
7440-48-4 Cobalt -NR -7440-50-8 Copper NR -7439-89-6 Iron NR
7439-92-1 Lead -NR
Magnesium -7439-95-4 NR -7439-96-5 Manganese 14200 E p --7439-97-6 Mercury NR
7440-02-0 Nickel 15.3 u p
7440-09-7 Potassium -NR
7782-49-2 Selenium 1.6 u F
7440-22-4 Silver -NR
7440-23-5 Sodium -NR
7440-28-0 Thallium -NR
Vanadium -7440-62-2 NR
Zinc -7440-66-6 3. 6 B p
cyanide -NR --
Color Before: COLORLESS Texture: D Color After: COLORLESS
Clarity Before: CLEAR
Clarity After: CLEAR Artifacts:
Ucomments:
CLIENT ID: NS15
u FORM I -IN
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ENVIROFORMS/INORGANIC CLP
1
l!il!l{)()f)9
SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
PCNS29
Contract: PACE CHAR. Lab Name: PACE INC.
Lab Code: Case No. : PCHAR SAS No.: SDG No.: PACl
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 100.0
Lab Sample ID: H420743
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte
7429-90-5 Aluminum
7440-36-0 Antimony
7440-38-2 Arsenic
7440-39-3 Barium
7440-41-7 Beryllium
7440-43-9 Cadmium
7440-70-2 Calcium
7440-47-3 Chromium
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese
7439-97-6 Mercury
7440-02-0 Nickel
7440-09-7 Potassium
7782-49-2 Selenium
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc
Cyanide
Color Before: COLORLESS
Concentration C
-
-
-1.1 u -867
0.30 u
4.8 u -
--6.9 B -
-
-
-
-
-4030 E -
-15.3 u -
3.2 u -
-
-
-
2.4 u -
-
Q M
-NR
NR
F -p
p
p
NR
p
NR
NR
NR
N
N
p
N
p
N
F
N
N
N
N
p
N
R
R
R
R
R
R
R
R
R
Texture: I Color After: COLORLESS
Comments:
Clarity Before: CLEAR
Clarity After: CLEAR Artifacts:
I CLIENT ID: NS29
I FORM I -IN
Lab Name: PACE INC.
Lab Code:
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract: PACE CHAR.
SAMPLE NO.
PCNS30
Case No. : PCHAR SAS No.: SDG No.: PACl
I
I
I
I
I
I
I
I
I
I
I
g
Matrix (soil/water): WATER Lab Sample ID: H420753
Date Received: 01/17/96 Level (low/med): LOW
% Solids: 100.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
D
0
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
74.40-62-2
7440-66-6
Color
B Color
Before: COLORLESS
After: COLORLESS
· Comments: I CLIENT ID: NS30
I
Analyte Concentration C
Aluminum -
Antimony -
Arsenic 1. 1 u
Barium 28.0 -B
Beryllium 0.30 B -Cadmium 4.8 u
Calcium -
Chromium -9.8 B -Cobalt -Copper -Iron -Lead
Magnesium -
-Manganese 1540 -Mercury
Nickel 15.3 u
Potassium -
Selenium -1. 6 u
Silver -
Sodium -
Thallium -
Vanadium -
Zinc -2.4 B
cyanide -
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q
E
w
M
NR
N R
F
p
p
p
N
p
N
N
N
N
N
p
N
p
N
F
N
N
N
N
p
N
R
R
R
R
R
R
R
R
R
R
R
R
R
Texture:
Artifacts:
I
I
I
I
I
I
I
I
I
I
•
I
n
D
u
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract: PACE CHAR.
I' 1111( Hill
SAMPLE NO.
PCNS31
Lab Name: PACE INC.
Lab Code: Case No. : PCHAR SAS No.: SDG No.: PACl
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 100.0
Lab Sample ID: H420752
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR -7440-36-0 Antimony NR
7440-38-2 Arsenic 1.1 u F --7440-39-3 Barium 1630 p -7440-41-7 Beryllium 0.30 u p
7440-43-9 Cadmium 4.8 u p -7440-70-2 Calcium NR
7440-47-3 Chromium 4.9 u p --7440-48-4 Cobalt NR -7440-50-8 Copper NR - -7439-89-6 Iron NR - -7439-92-1 Lead NR - -Magnesium 7439-95-4 NR -7439-96-5 Manganese 60.3 E p - -7439-97-6 Mercury NR -7440-02-0 Nickel 15.3 u p -7440-09-7 Potassium NR - -7782-49-2 Selenium 1. 6 u F -7440-22-4 Silver NR -7440-23-5 Sodium NR -7440-28-0 Thallium NR - -7440-62-2 Vanadium NR -7440-66-6 Zinc 3. 2 B p -cyanide NR --
Color
m Color
Before: COLORLESS
After: COLORLESS
Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
Artifacts:
I Comments:
CLIENT ID: NS31
I FORM I -IN
I
I
I
I
I
I
I
I
I
a
0
D
m
E
I
I
ENVIROFORMS/INORGANIC CLP
1
INORGANIC ANALYSIS DATA SHEET
Contract: PACE CHAR.
i It lil0012
SAMPLE NO.
PCNS32 Lab Name: PACE INC.
Lab Code: Case No.: PCHAR SAS No.: SDG No.: PACl
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 100.0
Lab Sample ID: H420745
Date Received: 01/17/96
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration
7429-90-5 Aluminum
7440-36-0 Antimony
Arsenic 7440-38-2 1.1
7440-39-3 Barium 87.8
7440-41-7 Beryllium 0.30
7440-43-9 Cadmium 4.8
7440-70-2 Calcium
7440-47-3 Chromium -8. 8
7440-48-4 Cobalt
7440-50-8 Copper
7439-89-6 Iron
7439-92-1 Lead
7439-95-4 Magnesium
7439-96-5 Manganese 92.6
7439-97-6 Mercury
7440-02-0 Nickel 15.3
7440-09-7 Potassium
7782-49-2 Selenium 1. 6
7440-22-4 Silver
7440-23-5 Sodium
7440-28-0 Thallium
7440-62-2 Vanadium
7440-66-6 Zinc 9.4
cyanide
C Q
-
-
u
B
u
u -
-B -
-
-
-
-
-E -
-u -
u w --
-
-
B -
-
M
-NR
NR -F -p
p
p
NR
p -NR
N
N
N
N
p
N
p
N
F
R
R
R
R
N
R
R
R
R
R
R
N
N
N
p
N R
Color
I Color
Before: COLORLESS
After: COLORLESS
Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
Artifacts:
I Comments:
CLIENT ID: NS32
I FORM I -IN
I
I
I
I
I
Appendix F
I Chain-of-Custody Records
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ENVIRONMENTAL LABORATORIES
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REMARKS
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ENVIRONMENTAL LABORATORIES
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*Requested Due Date:
REMARKS
RELINQUISHED BY/ AFFILIATION ACCEPTED BY/ AFFILIATION . ,
SEE REVERSE SIDE FOR INSTRUCTIONS
-
-- - --- - - - -5
ENVIRONMENTAL LABORATORIES
CHAIN-OF-CUSTODY RECORD
Analytical Request
ClientAJa ;D/\<i /
Address )/ 8.5
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PRESERVATIVES ANALYSES
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Additional Comments
SEE REVERSE SIDE FOR INSTRUCTIONS
-
- -
ENVIRONMENTAL LABORATORIES
Client/J.,/,'~",j Sbrc c ,,j C~f,,11c4
Ce<'/" r 5 J) {,' r1 y s Address f ,S')
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Phone ,/Of · C.33 · I/ 3 / £1 •
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Report To: Kr I\ k'luffz
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Project Name I No.
5i N I
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- -
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
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