NCD991278953_19950801_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Second Quarter 1995 OU-1 & OU-2-OCR

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Quarterly Report
Second Quarter 1995
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
August 1995
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RECEIVED
SEP 071995
SUPERFUND SECTION
Quarterly Report
Second Quarter 1995
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
August 1995
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Environmental Data Management, Inc.
Table of Contents
I. 0 Groundwater Monitoring Activities for the Second Quarter 1995 .
2. 0 Planned Groundwater Monitoring Activities .
3. 0 References .
Appendix -Certificates of Analysis
Appendix A -Report of Laboratory Analysis
Appendix B -Sample Delivery Group Narrative
Appendix C -Volatile Organics Analysis Data Sheets
Appendix D -Sernivolatile Organics Analysis Data Sheets
Appendix E -Inorganics Analysis Data Sheets
Appendix F -Chain-of-Custody Records
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List oITables
Title
List of Sample Analysis and Water Level Monitoring Performed
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Second Quarter 1995, Operable Unit No. I
3 ROD (OU2) Contaminants and Selected Water Quality Parameters in
Groundwater, Second Quarter 1995, Operable Unit No. 2
4 Groundwater Cleanup Criteria, Operable Unit No. I
5 Water Level Measurements, Second Quarter I 995, Operable Unit No. I
6 Water Level Measurements, Second Quarter 1995, Operable Unit No. 2
List of Figures
Site Map
2 Quarterly Summary of Acetone
3 Quarterly Summary of 1,2-Dichloroethane
4 Quarterly Summary of 1,2-Dichloropropane
5 Quarterly Summary ofBis(2-chloroethyl)ether
6 • Groundwater Contour Map for April 3, 1995
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1.0 Groundwater Monitoring Activities for Second Quarter 1995
This report for the second quarter of 1995 presents the findings from the groundwater
monitoring conducted at Operable Units No. I and 2 at the National Starch and Chemical
Company site on Cedar Springs Road, Salisbury, North Carolina. This report is prepared
in accordance with Record of Decisions (ROD) issued by the U.S. EPA on September 30,
I 988 for Operable Unit No. I (OU!) and on September 30, I 990 for Operable Unit No. 2
(OU2). Operable Unit No. I consists of contaminated groundwater area located in the
east-southeast portion of the facility. Operable Unit No. 2 consists of contaminated soils
and surface water/sediments in tributaries surrounding a trench area east of the plant
operation area.
Operable Unit No. 1
Groundwater samples from the four downgradient groundwater monitoring wells (NS29,
NS30, NS31, and NS32) and four bedrock extraction wells (EX0I, EX02, EX03, and
EX04) were collected on April 3-4, 1995. All samples were analyzed for Target
Compound List (TCL) volatile and semivolatile organic compounds (VOC and SVOC),
Target Analyte List (T AL) metals, and general chemistry. In addition, from the
monitoring wells and extraction wells were analyzed for selected water quality parameters
to monitor influent loadings for the Combined Pretreatment System (CPS). A sample
analysis summary is provided in Table I. The samples were collected in accordance with
U.S. EPA (Region IV) protocols. The TCL and T AL compounds were analyzed
supporting U.S. EPA Level IV Contract Laboratory Program (CPL) protocol.
No significant problems impacting the remediation system have occurred during this
quarter. All four extraction wells were operational.
Results from the chemical analysis for Operable Unit No. I and Operable Unit No. 2 are
presented in Tables 2 and 3, respectively. The list of compounds presented in these tables
represents the contaminants specified in Operable Unit No. I Record of Decision (ROD).
The list of designated compounds from the ROD (OU!) and associated cleanup levels are
provided in Table 4. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
The results of this quarters sampling indicated that four organic compounds, acetone, 1,2-
dichloroethane ( 1,2-DCA), 1-2-dichloropropane, and bis(2-chloroethyl)ether exhibited
levels that exceeded cleanup levels (shaded bold faced values in Table 2). As expected the
acetone levels continue to rise in all four of the extraction wells as these pumping wells
capture the contaminant plume. There appears to have been a significant increase in the
acetone concentration since the last quarterly sampling event possibly due to increased
pumping capacity or because of increased seasonal rainfall during the first and second
quarter of 1995. In addition to acetone, extraction well EX03 exhibited significant
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increases in 1,2-dicholoroethane, 1,2-dichloropropane, and bis(2-chloroethyl)ether since
the first quarter of 1995. Extraction wells EX0l and EX04 did not exceed the cleanup
standards for any of the VOC compounds. However, EX04 did show a significant
increase in bis(2-chloroethyl)ether since the first quarter 1995 sampling event.
Similar to the extraction wells, some of the downgradient wells have two VOC
compounds (1,2-dicholoroethane and 1,2-dichloropropane), and one SVOC compound
bis(2-chloroethyl)ether that exceed cleanup standards. None of the monitoring wells
exceeded the cleanup standard for acetone. Chemical data from samples collected to date
indicate that the contaminant concentrations in wells NS29, NS30, and NS3 l have
generally decreased over time and that no contaminants are present in NS32. However,
since the last quarterly sampling event there has been a significant increase in the
concentration of acetone, 1,2-dicholoroethane, 1,2-dichloropropane, and bis(2-
chloroethyl)ether in monitoring well NS29. Also, there has been a significant decline of
the same three VOC compounds in well NS3 l since the last quarterly sampling event.
The general trends for the four organic compounds that have exceeded the cleanup criteria
over the past four quarterly sampling events are presented in graphical form on Figures 2
through 5. These four organic compounds are acetone, 1,2-DCA, 1,2-dichoropropane,
and bis(2-chloroethyl)ether.
Methylene chloride was detected in some samples above cleanup standards (see Table 2),
but is disregarded as a valid groundwater contaminant since the compound was also
detected at similar concentrations in the associated blank water samples.
Water level measurements were taken on April 3-4, 1995, from 12 selected monitoring
wells and 2 stream gauges located in Operable Units No. 1 and 2. It is no longer possible
to take static water level measurements from extraction wells EX0 1, EX02, EX03, and
EX04, since these wells are continuously pumping. Also, dedicated bailers located in
monitoring wells NS29 and NS30 prohibits access for future water level measurement.
The static water level for NS32 was also not measured, due to artesian conditions. Well
NS32 has been under artesian conditions during all previous sampling events. The results
of the water level measurements are presented in Table 5. A groundwater elevations
contour map, is provided in Figure 6.
The hydraulic control of the contaminant plume is presently difficult to ascertain since the
extraction well program is not in full operation and the currently operating extraction
wells are not yet operating at full capacity. The efficiency of the plume control and
hydraulic control can be evaluated in more detail after all extraction wells are operating
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Operable Unit No. 2
Groundwater samples were collected from monitoring wells NS09, NSI0, NSI I, and
NS 15 on April 3-4, I 995. All samples were analyzed for selected TCL VOCs and
SVOCs, T AL metals, total dissolved solids (TDS), and chloride. In addition, the samples
were analyzed for selected water quality parameters to provide design information and
project start-up flow rates for the CPS. A sample analysis summary is provided in Table
I. The samples were collected in accordance with U.S. EPA (Region IV) protocol. The
TCL and T AL compounds were analyzed under U.S. EPA Level IV CLP protocol.
Results from the chemical analysis for Operable Unit No. 2 are presented in Table 3. The
list of compounds presented in Table 3 represents the contaminants specified in Operable
Unit No. I ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 4. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
Three of the four monitoring wells in Operable Unit No. 2 had compounds that exceeded
the cleanup standards. Monitoring well NS 11 had no compounds to exceed the standard.
Even though monitoring well NS 15 continues show concentrations of manganese and
vinyl chloride in excess of the cleanup standard, there appears to have been a significant
decline in the concentrations of several of the T AL compounds in this well. Monitoring
well NS09 exhibits some of the most diverse contaminants with four compounds acetone,
barium, chromium, and manganese exceeding the cleanup standard. Monitoring well
NS IO was the only OU2 well to exceed the cleanup standard for 1,2-DCA.
As with the first quarter 1995 sampling, manganese exceeded clean up levels in three
monitoring wells (NS09, NSI0, and NS15). Monitoring well NS! I continues to have
manganese concentrations below the cleanup standard.
Water level measurements were taken on April 3, 1995 from each of the four monitoring
wells. The results are provided in Table 6. A groundwater elevations contour map, is
provided in Figure 6.
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2.0 Planned Groundwater Monitoring Activities
Operable Unit No. 1
Groundwater monitoring will continue. Due to the very high concentrations of acetone in
the sample from extraction well EX02, care will be taken during the next sampling event
to alert the laboratory of the potential high concentration of acetone in this sample so that
they can properly calibrate their instruments prior the running their analysis. Other
samples will continue to be analyzed following routine procedures. The implementation of
the extraction well system will continue as planned with the continued operation of the
extraction wells EX0I, EX02, EX03, and EX04.
Operable Unit No. 2
Groundwater monitoring will continue. Like the sample from extraction well EX02, the
groundwater sample from monitoring well NS09 contains very high concentrations of
acetone. Therefore, the analytical procedure for voe analysis will be modified when
analyzing the sample from well NS09. Also, since a high concentration if 1,2-DeA was
detected in monitoring well NS I 0, similar caution will be taken in the laboratory to assure
that proper procedures are followed prior to performing the groundwater analysis. The
procedure modification will ensure greater accuracy in the voe analytical results.
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3. References
IT Corporation, May 1995 , "Quarterly Report -First Quarter I 995 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, February 1995,"Quarterly Report -Fourth Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, October I 994,"Quarterly Report -Third Quarter 1994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, July I 994 , "Quarterly Report -Second Quarter I 994 Operable Units
No. I & 2", National Starch and Chemical Company, Salisbury, NC.
North Carolina Environmental Management Commission, North Carolina Administrative
Code: ISA NCAC Subchapter 2L (August 1993).
U.S. EPA, September 30, 1990, Record of Decision (ROD) for Operable Unit No 2,
National Starch and Chemical Company, Salisbury, NC.
U.S. EPA, September 30, 1988, Record of Decision (ROD) for Operable Unit No I,
National Starch and Chemical Company, Salisbury, NC.
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- - - ---·--------------·-Table 1
List of Sample Analysis and Water Level Monitoring Performed
Second Quarter 1995
Operable Units No. 1 and 2
National Starch and Chemical Company
Salisbury, North Carolina
Well Number TCL
Well Tvr,e• VOCs0
Operable Unit No, 1 ... > >
TCL
svocs0
TAL
Metals0
EX01 BE X X X
EX02 BE X X X
EX03 BE X X X - --·--·-···-··· ··········--····>··· ........................ -----·
TDS'
·.
X
X
X
Chloride
X
X
X ... ····-···-···
coo'
X
X
X
TKN•
Water
Level
.............. l=.J:<Q:4. .. --~_ BE,_-+--'-x'----'--x:.:....._+-_-'-x'---1----=.o.....-, __ ....:..:_-+--'-"----~ X X X
X
X
X
X
X
X
X
X
X
X
X
X
X
NS0S SM ··--------------------------
. f'-!S.06. ............... _ ?IVI •I•••••••••••••••••••••••••+•••••••••••••••-•••••••• •••••••rn•-•--•••"~-"•I••••••••••••••••••••••••••• '•••••••••••••••••••••••••••• • •
NS21 BM
NS22 BM ........ ,. ·························~---···i NS23 SM -·-----------····· NS26 BM
NS27 BM
NS28 ·--~ ....... 13IVI .......... .
NS29 BM X ··----------------...................... . NS30 BM X
X
X
X X X
X X X ........ -.... ----...... , ... ___ -.... ................ ···········•·-•··--·-···· ' ......... ·····
NS31 BM X ............... ······---··
NS32 -~_BM X
PO1 BM sfream.Gai:19Ei°No,·1r . NA0
Stream Gauae No. 2 · NA
Operable Unit No. 2
NS09 SM ........................ . .......... .
t,IStQ •· ... . ... §M._ i..·-·······
NS11 SM
NS15 BE
X
X
X X •......... J:<.
X X X
X X. _ _,___
X ._.). X
X ' X
X X
X
X
X
X
·········-·-····
X
X
X
X
11BE = Bedrock extraction welt, BM = Bedrock monitonng well, SM = Saprollte (shallow) monitoring well
bProject TCL consisting of 13 voes, 2 SVOCs, and 9 metals, and meets Operable Unit No. 1 cleanup criteria (Table 4).
cTDS -Total dissolved solids
dcoo -Chemical oxygen demand
eTKN -Total Kjeldaht nitrogen
elron pins in southwest tributary for monitoring stream elevations.
gNA -Not Applicable
X
...•.... ··--···-x
x
X
······················•············x
• . X
X
X
X ············'········ .. ·--···-··-·· X
X
X
X
X
X
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Table 2
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1995
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina •
Extraction Wells Monitorina Wells
Well Number:
Sample Date:
EX01 I EX02 I EX03 I EX04
4/4/95 4/4/95 I 4/4/95 I 4/4/95
NS29 I NS30 I NS31 I NS32
4/3/95 I 4/3/95 I 4/4/95 I 4/3/95
Volatile OrQanics (U!l/1)
::~:~: 21~~/ 36~~~>98:~: 38~~ ~~! t~~ 25~~' t~~
Bromodichloromethane 5Ui 42Ui "'""45"LJ\''' s·ut 12U 'i:fUT"'""''1oUj SU
ll------~='Cc-C~h~l~or~o~ro~rm~~--=sc:u~i-·_=42==-c:U~:_·_··_··=45~·~u+i_·_~s~u.::.,-•--t~2~u=+i _ _c:s~u~·--~1~0c:u~i __ su
t,t-Dichloroethylenel---cc7c:Uc;i. 59U: 63U'. 7u: t8Ui 7U'. tSU! 7U
1,2-Dichloroethane 5 U i · i>760' : .. • .. : ...... ·.•.• .. :, •. •.ia·.& .• 90· .. ·.·.l,' ... · 5 ' . 37' "" 's'u'•" 41 '. 5 U ...... , t.2:Dichloropropane ii'uL (1300' ,. ' . sii ,, iii'' 6 Li"f' '{soj 6 u
Ethylbenzene tau[' 85U'. 89u• 10u• ··2ii'u'l 10u· 21 u, tOU
MethyleneChloride 3BJ'. 44B! 41 BJ' 7B' 13B'. 10B. 16B'. 11 B
1,1,2-Trichloroethane SU'. 42U 45U SU! 12U'. su; tOUi SU
Toluene tOU'. 280 80Ji 26: ·2sui••··1ofr'." .iiJ! 10 U
Trichloroethene . ·s·u j . 4iU'/"" 1:i'U i"" 5 U ! 10··l/ 5 U
--i----45 Ui SU!
11 ---------V_i n~y l_C h Io ride l---=2c:u..,i __ t, 7~u.c· _ __:,c.,:c+--~=+--5 U '. 2 U 4 U '. ........ JU
Xylene 10U! 24J is·u;--,o-u-,--2-,-U~! 10U
18 U i 2U'
89 Ui 10 U •
Semivolatile Or!lanic lu1111)
.......... Bis (2:Chloroeth~) Ether .
4-Nitrophenol
3Jj,. i\)!60 220Ei;·· ,,,,.,·,55
26Uj "z7o'Li'' ''s2'Li! 140U'.
32!
21 ui
18):
28 u,
78! 5 U .-.·,.l_,.
51 U i 26 U
lnor11anics /u1111)
Arsenic 2.7U 3.8B 2.7U'. 2.7Ui 2.7U( 2.7U' 29B'
Barium 26.SB 1880' 475! 72.7Bi 84.7Bi 27.SB! i;{tis! ·----------==CCJ-,,::.;CC..=.J,-· ·~'··~···-·,•-'~--'~'-~:c;_.=c,_,:_ ·---~--
Beryili~rr,f---Q._20_UL__.:Q,::,2:c:3~Bcc-0.20 U i 0.28 B: 0.20 U '. 0.20 U' 0.20 U i
II-----------C-a~dmium 1.4U' 1.4U t.4U! tAU· 1.4U'. tAU' 1.4U'.
20Ui ·:fou''
2.8 B
93.3 B
0.28 B
1.4 U
2.0 U Chromium . 2DlJi 2.0U . z.Qu'i 20Ui .2.ou!
Manganese 53.4 18800··· 4810! .. 4170; 268,
Nickel 5.5 u 5.5 U 5.5 Llj 5.5 U: s.s u'
2.7 u,
2290 zs.s: 111
5 su:--s-'.sC..u-'' s.s u·
2.7 u: Selenium 2.7 B 3.0 B 2.7 U '. 2.7 U:
Zinc 9.4 B, 5.8 U 16.0 Bi ..... S:iiu'i 58 u't
2.7 U, 3.2 B
6.0 B
Water Qualitv (mall)
TDS 200 3200 1200 750· 430'. 480' 6so: •I--•• " .. . it: . 91' Chloride 20 1100 240 tso, 90'.
COD 25 1300' 300 100: NA! NA! NA!
Nrtrogen (TKN) ND! 3.7' tAi 1.4' ..... NAi NA' NA!
Note Data Qualifier Definitions:
B (Organics) = Compound was detected in the associated blank.
B (Inorganic&) = Compound concentration is below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively
identified et a trace value, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected et the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
mass spectrometry instrument.
ND= Not detected at or above the detection limit of analysis method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates a detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30-88).
220
9.8
NA
NA
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Table 3
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1995
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Monitorinn Wells
Well Number: NS09 I NS10 I NS11 I
Sample Date: 414195 I 413195 I 414195 I
Volatile Oraanics {ua/ll
___________ A_c_e_to_n_e 1 ::<'L::::V<i;~4~_004El _____ ················~~-qi
Benzene 500 u ' 89 U •
10 u.
5 u. ...... . ........................................... , .. .
Br~~~-i-~!1:~~~~~-7.thane 500 U I -~~--~-! Chloroform .... ·············soo U : 89 U [
SU
SU
1, 1-Dichloroethylen!_ _ 700 U:
..... ~.'.~~-~-i~_~loroethane 500 U .-,,.. ::i:·![!j,j~,~~~;;~L
130 u· 7U
SU
.... _1,2'.Dichloropropane 600 u 110 U'
Ethyl benzene 1000 U • ·iaii u'.
6 u.
76•
78
SU
Methylene Chlorid~'l----'-1:CC300~B=-;-: __ __:2°c30~8:..;' ___ _
1,1,2-Trichloroethane 500 u: 89 u: .......................................................
NS15
413195
10 U
SU
SU .......... ···-···
SU
7U
290 E
6U
10 U ________ .,. _____________
58
· SU
Toluene 340J• 180U 11 BJ
Trichloroethene ... 500 U: ....... ·agfr· 5 U • 5 U
ll--------"v;",n.cyl.cC.:.:chl.con.c.d;.:e+---~200~U--'-• ---~36=u"':--·--2'-'-u ff::.:!::: "}': .; '4
Xylene 1000U' 1BOU' 44: 10U
Semivolatile Oraanic lua/ll
Bi~ (2-Chloroethyl) Ether
4-Nitrophenol
lnoraanics {ua/ll
27U 250U SU 6U ..... i4iiu' 12oou• --··27u/· 28U
Arsenic 2.7 U • 2.7 U, 2.7 U • 2.7 U
" ____________ B_an_·u_m_+"·=··•:1@:jUUii::im'!i!120~:..:. :cl_·_··_···_·--_--_ ... _ .. 1:.:··g:.:j:.:. a=-···'-j· ___ .:.1.:.40::..:a,,. ____ .:.4::2B:11 ,.__ ____________ Be~lium __ __:o.;::.2=2.;::Bc.' ----=o=.2c:.0..:Uc.' ___ ..:0:,:.2.:.4..:Bc.' ~ 0.20 U
Cadmium 1.4Ui 1.4Uj 1.4Ui 1.4U
···M~r:a:~s: i~~~~~,~~~~1~jrnlf:'.!iF:l[;[:;1i:~;;i~!I·-················~~i·.~·!1: ]}f'.i;j\11:,1:~ 11--------;.:_:.;===1
____________ l'li~~c( 43.6: 20 1 B: 5.5 U 5.5 U
----Selenium 2.7 u: 2.7 u: 2.7 u· 2.7 U ...................... Zinc 141 i 13.28 5.BU
Water Qualitv lma/ll
TDS 2900: .................................. --··············· ........... ,._..
Chloride 2100'
COD NA• 11-------~--= Nnrogen (TKN) ND
Note Data Qualifier Definitions:
1000' ...................... ; .....
410:
250
NA:
B !Organics) = Compound was detected in the essocieted blank.
320
5.4
245
NA:
B (lnorganics) = Compound concentration is below the contract-required detection limit.
2400
1100
NA
NA
J = Compound concentration is an estimate. Either the compound was positively
identified at II trace value, or it is II nontarget tor which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
mass spectrometry instrument.
NO= Not detected et or above the detection limit of enetysis method.
NA= Not analyzed.
Also Note: Shaded bold f11ce dote indicates II detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9·30-88).
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Table 4
Groundwater Cleanup Criteria
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Compound Cleanup Concentration (ug/1)
Volatile Organics
Acetonel
Benzene
Bromodichloromethane ............ ··-•--• .. ···•·--........... .
Chloroform
··1.2~bic:tl1oroettianeibc11i;.-i ____ _
1, 1-Dichloroethy,.cle::.:nc.:e:.;.i ___ ~--
-~ ,?~Pi<,:h.lorop~cipaf}~
............ ... E:thyll:>en;~f}~
·----'-'-Mc=e=thyleneC.=-h~lo~riccd.c..e'----
Toluene
.................... 1, 1,:1:Trichlorci~than~(TCII)
..... Trichloroethene (TCE)
_______ __:.V=iny.I Chloride,
Xylene!
Semivolatiles
........... E3is .. (2:C:::hlciro~th.yl) Eth.~rL ....
4-Nitroohenol,
·: ·.-:· ' .. : ·•
· · lnorganics
Arsenid
Barium
...... Beryllium
Cadmium
Chromium
n-----------'-'-M~ac:.:nganese
Nickel
Selenium
Zinc
3500
5
5
5
5
7 ___ ·----<
6
3500
5
2000
5
5
2
350
5
350
10
1000
17.5
10
50
7700
350
10
7350
Reference: U.S. EPA, September 30, 1988, Record of Dec1s1on (ROD), Operable Unit No. 1,
National Starch and Chemical Company, Salisbury, North Carolina.
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Table 5
Water Level Measurements
Second Quarter 1995
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to Water Level
Measurement Water Elevation Point of Elevation
Well Name Date (Ft.I (Ft. MSL) Reference (Ft. MSLI
' TOC ' 731.85
TOC 718.24
TOC ' 740.46
NS06 4/4/95 TOC 738.87 5.9 732:.::.9c_7 __ 1
........ NS21........... 4/~l~!i ....... TClC..................... 739.13 ........ 5.8 ...... .. 733.33 .. .
NS22 . 4/~/95. TClC: 715.94 15.5 700.44 .•...... l
1 _ ___,N_c;S:::2::.:3=---~--"4/...:4c.-:/9:.::5 _ _:,.__--'-TO=C-~ __ 7c...:5:.=2:.:;.3,_,6:___:,._" _ _:_1.:::8·=5-~ __ 7=3~,8§.
NS26 4/4/95 TOC 720.77 8.8 711.97
NS2?... ....... ~/~/95. .. .. . .. Toc ................... 749.47 16.8 732.67
NS28 4/4/95 TOC 767.82 . 21.1 746.72 ····· l\iszg···· · 4t3iils ;········toc , 115.s ············Niib NAb
..... l'!§}_Q 4/3/95 ! TOC 71.8.54.. . ..... ~A0 NAb ...
NS31 4/4/95 TOC 711.15 . 31.6 679.55
....... NS32 :: . 4/3/95 ............... TO..C. ........ 699~48 ... NAC NAC
P01 • 4/4/95 TOC 708.09 NA'.. NA' .. 1----'-"'...'.---'---'-'-==---'--..:..:::=--'----'-'='-"---'---' --~--'-=--•
_ . §~1_ -'------'4::.../4.:c./.:::95=----•-----'T'-'O:..:C=--...... ._, _...:7...:12:::-:::2.::.6_~~ 0.2 -~--712.06
SG2 : 4/4/95 TOC 693.9 i 0.4 693.5
NA• -Not Applicable, well is an extraction well and is pumping.
NAb -Not Applicable, well has a dedicated bailer with no access for taking water level measurments.
NA c -Not Applicable, well is artesian.
NAd -Not Applicable, well is dry, or stream level not measured.
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Environmental Data Management, Inc.
Table 6
Water Level Measurements
Second Quarter 1995
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Well Name Date Reference (Ft. MSL) IFt.l
NS09 i 4/3/95 ! TOC ; 778.45 ' 28.5 ' NS10 4/3/95 TOC 786.72 32.4
NS11 4/4/95 TOC -'.---····· 775.65 .-...•... 17 •·-•··· .. ••-•-.............. ........ -·····•·· ········· .......
NS15 4/3/95 TOC 792.6 44.8
NA1 -Not Applicable, well is an extraction well and is pumping.
NAb -Not Applicable, well has a dedicated bailer with no access for taking water level measurments.
NAe -Not Applicable, well is artesian.
NAd -Not Applicable, well is dry, or stream level not measured.
Water Level
Elevation
(Ft. MSL)
749.95
754.32
758.65
747.8
---·---~
~
I}
-+
CROUNDWAT[R tJ0N110R!NC A.REA (SH FIGURE 6) -
Fo• ()P[J>A8L[ UNITS 1 & 2
Environmental Data Management, Inc.
- - ----
National Starch & Chemncal Company
Cedar Springs Road
Salisbury, north Caroluna
-----·
/ I
-+ Monltoring Well
-Roads, Building~ etc.
-~ Fence Line
-H-+ Railroad
............. Property Line
-Tributary Stream
-
----n~-Topographic Contour Line
(FL I.ISL) Contc,u, lnle•vol • 5Fl.
0 400 800 1200
L..s.l I I
Scale in Feel
Scale 1 lnch = 800 Feet
Site Map
2nd Quarter Report 1995
For
◊~rat.le Units I & 2
-
-------------------Figure 2
Quarterly Summary of Acetone Concentration
45,000 ~----------------------------------------
40,000 +--------
35,000
30,000
:::: "' ::,
,5 25,000 C 0 ! -C 20,000 .. u C 0 u
15,000
10,000
5,000 --1---------
EX01
EDN
Environmental Dala Management, Inc.
Augusl 1995
EX02
'""'
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Unit No.1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
matr3-'94
llil Qtr4-'94
1111 Qtr1-'95
■Otr2-'95
""'
NS31
Quartery Report For
Operable Units No. 1 & 2
2nd Quarter 1995
-------------------
'§,
:::,
.5
C: 0
! -C: .. u C: 0 (,)
EX01 EX02
Figure 3
Quarterly Summary of 1,2 Dichloroethane
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
NoCe: Concertratiotrs depicted at or beklw 5 uo,1 represent deled/on lirl'II of tab<>nltory analysis metl'IOd
EDII
Environmental Data Management, Inc.
August 1995
National Starch and Chemical Company
Salisbury, North Carolina
NS30 NS31
E!l Qtr3-'94
ml Qtr4-'94
1111 Qtr1-'95
■Qtr2-'95
Quarterly Report For
Operable Units No. 1 &2
2nd Quarter 1995
-- - -
a, :,
C:
C: 0 ., 100 I!! -C: ., u C: 0 u
EX01
---------------Figure 4
Quarterly Summary of 1,2 Dichloropropane
EX02 EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
l!lQtr3-'94
IIII Qtr4-'94
El Qtr1-'95
■Qtr2-'95
NS30 NS31
m
j < (f
j
3 ro
j
£
CJ
Q a
;::
Q j
Q <O ro
3 ro -" j r
Note: Concert111tiom depicied 111 or below 6 UG/1 represent de!ection Ii/Tit of laborll!ory 11n11~s method
EDN
Environmental Data Management. Inc.
August 1995
National Starch and Chemical Company
Salisbury, North Carolina
Quarterly Report For
Operable Units No. 1 &2
2nd Quarter 1995
- - - -
100
=:: Cl :,
.5
C 0 '! -C .. u
C 0 0
10
EX01
EDN
Environmental Data Management, Inc.
August 1995
---------------
EX02
Figure 5
Quarterly Summary of Bis(2-chloroethyl)ether
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
Ell Qtr3-'94
IIll Qtr4-'94
m Qtr1-'95
■ Qtr2-'95
5 ,g/1
-:--cleanup Concentration
NS31
Quarterly Report For
Operable Units No. 1 &2
2nd Quarter 1995
-------------------
&
I I +
I
0 200 400
~....l t
Scale in Feet
I
800
t
Scale 1 Inch = 400 Feel
Legend
-Roads, Buildings. etc.
-·--Fence Line
-Property Line
-Tributary Stream
\
\
-12 5 -Groundwater Contour Line (Ft MSL) -+ Monitoring Well
'v Stream Gauge
) I I'-.
NS30
Stream
'V Gauge # 1 I
I ' ' '
\
I
/
J\lational Starch & Chemical Company
Cedar Springs Road
Salisbury, North Carolina
!Environmental Data Management, Inc.
' '
NSIO -+
•----.,.
' .....
NS15
-t-
/ I
PLAt'JT AREA
□
Elf lfo. 4
' '
Figure 6
Groundlwater Contour Map
for April 3, 1995
2nd Quarter Report 1995
For
Operable Units I & 2
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r,:1-#E:J
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
May 05, 1995
Mr. Ken Kluttz
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 2B144
RE: PACE Project No. 650405.503
•
Client Reference: Quarterly Monitoring -CLP
Dear Mr. Kluttz:
Enclosed is the report of laboratory analyses for samples received
April 05, 1995.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Kris H. Kommalan
Project Manager
Enclosures
9800 Kincev Avenue. Suire 100
Huntersville. NC 28078
TEL: [phone]
FAX· 70,1-875-909i
An Equal Opportunity Employer
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(tI£:l
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 28144
I Attn: Mr. Ken Kluttz
I
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Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
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Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kince1• Avenue. Suite 1 DO
Huntersville. NC 28078
TEL: 704•875-9092
fAX· l0J-875-9091
Units
mg/L
mg/L
•
MDL
1.0
I
May 05, 1995
PACE Project Number: 650405503
92 0369203
04/03/95
04/05/95
NS-32
____ METHOD DATE ANALYZED
9.8
220
DONE
DONE
DONE
407B
160.l
CLP, EPA
CLP, EPA
CLP, EPA
04/08/95
04/08/95
04/13/95
04/12/95
04/12/95
An Equal Opportunity Employer
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(cX£:l
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 2
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles Target Compounds List -Volatiles
9800 Kincev Avenue, Suite 100
Humcrsville. NC 28078
TEL: [phone]
FAX: "/011-875-9091
Units
mg/L
mg/L
• MDL
1.0
1
May 05, 1995
PACE Project Number: 650405503
92 0369211
04/03/95
04/05/95
NS-09
----
2100
2900
DONE
DONE
DONE
METHOD DATE ANALYZED
4078
160.]
CLP, EPA
· CLP, EPA
CLP, EPA
04/08/95
04/08/95
04/13/95
04/12/95
04/12/95
An Eoual Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 3
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincev Avenue. Suite 100
lfon101sville. NC 28078
TEL: [phone]
FAX· 704-875-9091
Units
mg/L
mg/L
mg/L
• MDL
10
I. 0
I
May 05, 1995
PACE Project Number: 650405503
92 0369220
04/03/95
04/05/95
NS-10
----
250
410
1000
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
4078
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/08/95
04/13/95
04/13/95
04/12/95
An Equal Opportunity Employer
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(cl.)li;l
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 4
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue. Suite 100
Huntersville. MC 28078
TEL: [phone]
fAX: [phone]
Units
mg/L
mg/L
• MDL
1.0
1
May 05, 1995
PACE Project Number: 650405503
92 0369238
04/03/95
04/05/95
NS-30
____ METHOD DATE ANALYZED
91
480
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
04/08/95
04/08/95
04/13/95
04/12/95
04/12/95
An Equal Opportunity Employer
I
I r,l.ili:l
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
Page 5
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Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Ki11cev Ave1111e. Suite l DO
1-lu1llersville. NC 28078
TEL: [phone]
rAX: 704-875-9091,
Units
mg/L
mg/L
• MDL
1.0
1
May 05, 1995
PACE Project Number: 650405503
92 0369246
04/03/95
04/05/95
NS-15
----
1100
2400
DONE
DONE
DONE
METHOD DATE ANALYZED
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
04/0B/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
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(;l.).li:J
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 6
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
,,
9800 Kincev Ave11ue, Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
• MDL
1.0
1
May 05, 1995
PACE Project Number: 650405503
92 0369254
04/03/95
04/05/95
NS-29
____ METHOD DATE ANALYZED
71
430
DONE
DONE
DONE
407B
160 .1
CLP, EPA
CLP, EPA
CLP, EPA
04/08/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
I
I
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ENVIRONMENTAL LABORATORIES
Mr. Ken Kluttz
Page 7
REPORT OF LABORATORY ANALYSIS
May 05, 1995
PACE Project Number: 650405503 I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number: 92 0369262
04/04/95
04/05/95
NS-31
Date Co 11 ected:
Date Received:
Client Sample ID: I
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride I
I
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I
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincev Aven11e. Suite 100
Huntersville_ NC 28078
TEL: [phone]
rAx· 704-875-9091
Units
mg/L
mg/L
• MDL
1.0
1
____ METHOD DATE ANALYZED
90
650
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
04/08/95
04/08/95
04/13/95
04 /12/95
04/13/95
An Equal Opportunity Employer
I
I (;:X.lli:l
ENVIRONMENTAL LABORATORIES
I Mr. Ken Kluttz
Page 8
REPORT OF LABORATORY ANALYSIS
May 05, 1995
PACE Project Number: 650405503
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected: I Date Received:
Client Sample JD:
Parameter
I INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
i
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
•• INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles 1·
I
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I
I
I
9800 Kincev Avenue. Suite 100
I Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
• MDL
10
1.0
I
92 0369270
04/04/95
04/05/95
NS-II
----
245
5.4
320
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/08/95
04/13/95
04/12/95
04/14/95
A~ Equal Opportunity Employer
I (cl~E-l
ENVIRONMENTAL LABORATORIES I REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
Page 9
1 Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
I Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS I Chemical Oxygen Demand
-, Chloride
Nitrogen, Kjeldahl
I-Solids, Total Dissolved
. · Target Analyte List -Inorganics
I, ORGANIC ANALYSIS
I
I
I
I
I (\
I
I
I
I
I
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
9800 Kincey Avenue, Suiw 100
Huntersville. NC 2B078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units
mg/L
mg/L
mg/L
mg/L
• MDL
10
1.0
0.5
1
May 05, 1995
PACE Project Number: 650405503
92 0369289
04/04/95
04/05/95
EX-04
____ METHOD DATE ANALYZED
100
150
1.4
750
DONE
DONE
DONE
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/24/95
04/08/95
04/13/95
04/12/95
04/14/95
An.Equal Opportunity Employer
c~iili:l
ENVIRONMENTAL LABORATORIES
Mr. Ken Kluttz
Page 10
REPORT OF LABORATORY ANALYSIS
May 05, 1995
PACE Project Number: 650405503
I
m
D
u Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID: I Parameter ·-I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS ·1 Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
I-Solids, Total Dissolved
_ Target Analyte List -Inorganics
I
I
I
I
I
I
I
I
I
I
I
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey .'wenue, Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
• MDL
10
1.0
0.5
1
92 0369297
04/04/95
04/05/95
EX-04 MS
____ METHOD DATE ANALYZED
100
150
1.6
740
DONE
DONE
DONE
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/24/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
I
I INCORPORATED
ENVIRONMENTAL LABORATORIES
0 Mr. Ken Kluttz D Page 11
REPORT OF LABORATORY ANALYSIS
May 05, 1995
PACE Project Number: 650405503
u
I
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter I INORGANIC ANALYSIS
I
I
I
I
I
I
I
I
I
I
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue. Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
• MDL
10
1. 0
0.5
1
92 0369300
04/04/95
04/05/95
EX-04 MSD
----
100
150
1.1
740
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/24/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
I r,iili:l
ENVIRONMENTAL LABORATORIES I
I .. · Mr. Ken Kluttz
Page 12
REPORT OF LABORATORY ANALYSIS
May 05, 1995
PACE Project Number: 650405503
I ::~:n:a::~:r:::::/uarterly Monitoring -CLP
92 0369319
04/04/95
04/05/95
EX-03
Date Collected:
I-Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
0-.
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
D Solids, Total Dissolved
· .. Target Analyte List -Inorganics
I
I
I
I
I
I
I
I
I
I
I
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
9800 Kinccv Avenue. Suite 100
Huntersville. NC 28078
TEL: [phone]
rAX: 704-875-9091
Semivolatiles
Volatiles
Units
mg/L
mg/L
mg/L
mg/L
• MDL
10
1.0
0.5
I
----
300
240
1.4
1200
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
4078
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/24/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
Page l 3
Client Reference: Quarterly Monitoring -CLP I PACE Sample Number:
Date Co 11 ected:
I .. Date Received:
Client Sample ID:
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Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue. Suite 100
H11n1ersville, NC 28078
TEL: [phone]
FAX: 70~•875•9□ 91
Units
mg/L
mg/L
mg/L
mg/L
•
MDL
10
1.0
0.5
I
May 05, 1995
PACE Project Number: 650405503
92 0369327
04/04/95
04/05/95
EX-02
____ METHOD DATE ANALYZED
1300
1100
3.7
3200
DONE
DONE
DONE
8000
4078
351.3
160.I
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
04/24/95
04/08/95
04/13/95
04/13/95
04/13/95
An Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
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Mr. Ken Kluttz
Page 14
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
Units
mg/L
mg/L
mg/L
mg/L
• MDL
10
1.0
0.5
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These data have been reviewed and are approved for release.
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Charles M. Cabaniss
Manager, Inorganic Chemistry . .
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Margaret S. Harding
Manager, Organic Chemistry
9800 Kincev A\·en11e. Suite 100
1-iuniersville. NC 28078
TEL: [phone]
FAX: [phone]
May 05, 1995
PACE Project Number: 650405503
92 0369335
04/04/95
04/05/95
EX-01
----
25
20
ND
200
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351.3
160 .1
CLP, EPA
CLP, EPA
CLP, EPA
05/01/95
04/08/95
05/01/95
04/08/95
04/13/95
04/12/95
04/13/95
An Equal Opportunity Employer
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I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
FOOTNOTES I .Mr. Ken Kluttz
Page 15 for pages 1 through 14
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Client Reference: Quarterly Monitoring -CLP
MDL Method Detection Limit
ND Not detected at or above the MDL.
9800 Kince.,. Avenue, Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
•
May 05, 1995
PACE Project Number: 650405503
An Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA May 05, 1995 Mr. Ken Kluttz
Page 16 PACE Project Number: 650405503
Client Reference: Quarterly Monitoring -CLP
Chemical Oxygen Demand
Batch: 92 35823
Samples: 92 0369220, 92 0369270, 92 0369289, 92 0369297, 92 0369300
92 0369319, 92 0369327, 92 0369335
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
9800 K111r,cy Avr.nue. Suite 100
Huntersville. NC 28078
TEL: [phone]
Ft1X: 704-875-9091 _
Units
mg/L
Units
mg/L
Units
mg/L
•
MDL
To
MDL
To
MDL
To
Method
Blank
ND
Duplicate
920369220 of
;;.,NS~--=-10=----92 0369220
250 250
920369270 Spike
Recv
100%
NS-11 Spike
245 250
Reference
Value
50
Recv
96%
An Equal Opportunity Employer
RPO
0%
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I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
Page 17
QUALITY CONTROL DATA
1 Client Reference: Quarterly Monitoring -CLP
Chloride
Batch: I Samples:
92 35244
92 0369203,
92 0369254,
92 0369300,
92 0369211,
92 0369262,
92 0369319,
92 0369220,
92 0369270,
92 0369327,
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METHOD BLANK AND SAMPLE DUPLICATE:
1'
Parameter
Chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
Chloride
9800 Kincey Avenue. Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX· 704-875-9091
Units
mg/L
Units
mg/L
Units
mg/L
92 0369238,
92 0369289,
92 0369335 •
MDL
1.0
MDL
1.0
MDL
1.0
May 05, 1995
PACE Project Number: 650405503
92 0369246
92 0369297
Method
Blank
ND
Duplicate
920369203 of
NS-32 92 0369203 ~_.c...c.--9. 8 9.8
Spike
920369475 Spike Recv
15 10 100%
Reference
Value Recv
100 100%
An Equal Opportunity Employer
RPO
0%
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 18
QUALITY CONTROL DATA
Client Reference: Quarterly Monitoring -CLP
Nitrogen, Kjeldahl
Batch: 92 35929
Samples: 92 0369335
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Nitrogen, Kjeldahl
9800 Ki11ccv Avenue. Suite 100
H11111ersville. NC 28078
TEL: [phone]
FAX 70•1-875-9091
Units
iiig7L
•
MDL
0.5
May 05, 1995
PACE Project Number: 650405503
Method
Blank 920380363
ND O. 97
Duplicate
of
92 0380363
1. 2
An Equal Opportunity Employer
RPO
21%
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 19
QUALITY CONTROL DATA May 05, 1995
PACE Project Number: 650405503
Client Reference: Quarterly Monitoring -CLP
Solids, Total Dissolved
Batch: 92 35249
Samples: 92 0369203, 92 0369211, 92 0369220, 92 0369238, 92 0369246
92 0369254, 92 0369262, 92 0369270, 92 0369289, 92 0369297
92 0369300, 92 0369319, 92 0369327, 92 0369335
METHOD BLANK:
Parameter
Sol ids, Total Dissolved
LABORATORY CONTROL SAMPLE:
Parameter
Sol ids, Total Dissolved
9800 Kincey Avem1e, Suiw 1 DO
Huntersville. NC 28078
TEL: 704•875-9092
FAX. [phone] •
Units
mg/L
Units
mg/L
•
MDL -1-
MDL -1-
Method
Blank
ND
Reference
Value Recv
100 98%
An Equal Opportunity Employei
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
FOOTNOTES Mr. Ken Kluttz
Page 20 for pages 16 through 19
Client Reference: Quarterly Monitoring -CLP
MDL Method Detection Limit
ND Not detected at or above the MDL.
RPO Relative Percent Difference
9800 Kincev Avr.rwe, Suite 100
Huntersville. NC 28078
TEL: [phone]
fAX: [phone]
•
May 05, 1995
PACE Project Number: 650405503
An Equal Opponunity Employer
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I Appendix B
I Sample Delivery Group Narrative
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THE ASSURA'iCE OF QUALITY
May 3, 1995
Mr. Ken Kluttz
National Starch & Chemical Company
485 Cedar Spring Road
Salisbury, NC 28144
Case: PCHAR
SDG: NASO?
SAMPLE DELIVERY GROUP NARRATIVE
Laboratory: PACE New England -New Hampshire Laboratory, Hampton, NH
Lab Numbers: 43530
Analytical Protocol: OLM0l.8/ILM0l.2 with modified target lists. Format A disk--
Form I sample data.
Sample Receipt: Samples for this SDG were received at PACE'S Charlotte Laboratory
on April 5, 1995. They were forwarded by Federal Express carrier to PACE New
Hampshire for analysis. PACE New Hampshire laboratory sample numbers were assigned
as listed on the Sample Table which follows this narrative. Field sample identifiers
were abbreviated to accommodate CLP software requirements. Although temperature
blanks were not included with the shipments, samples were received cool. Bottles and
labels matched the Chains-of-Custody (COC) provided. Details of sample delivery are
noted as follows:
The samples received at PACE New Hampshire on 4/06/95 were assigned PACE lab# 43530.
Samples were accompanied by COC documents. No problems were encountered with the
shipment of these samples. The sample designated on the COC for QC for this SDG was
11EX04 4-4-95."
Volatiles Analysis: Samples were analyzed within holding time under the CLP OLM0l.8
water method. In accordance with project requirements, the protocol was modified to
a target list of fourteen compounds with special detection limits. Nontarget
searches were not required. In addition, the client requested that samples needing
dilution be run a second time at lesser dilution to achieve lower detection limits.
Ten samples therefore have two sets of data reported. All samples except NS31XX and
NSllXX were determined to have pH< 2 at time of analysis.
Samples were run within compliant twelve-hour tune windows. Standards met CLP
calibration criteria for the compounds of interest. Method blanks contained low
levels of methylene chloride. This common lab contaminant was reported.with a 11B 11
qualifier when detected in associated samples. Results for this analyte should be
used with due consideration.
Matrix spike analyses were conducted on sample EX04XX, which exhibited acceptable
accuracy and precision. Because they were run at the same dilution as EX04XXDL, the
spikes were named EX04XXDLMS and EX04XXDLMSD. Values reported on the Form III spike
recovery sheet should be considered accurate to two significant figures.
Internal standard areas were compliant for all analyses. Surrogate recoveries were
also compliant with the exception of high DCE recoveries in samples NSl0XX and
NS15XX. These samples had high 1,2-dichloroethane content which caused an
interference with the surrogate. Surrogate recoveries were acceptable in the diluted
analyses of these two samples.
P.O. Box 2130
One Lafayette Road
Hampton, NH 03842
TEL: GID-926-7777
r.Av. cn'l n'lC ,n')()
o·l
An Equal Opportunity Employer
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THE ASSURANCE OF DUALITY
SDG Narrative
Case: PCHAR, SDG: NASO?
Samples EXOlXX, EX02XX, EX03XX, EX04XX, NS09XX, NS29XX, and NS31XX required dilutions
due to high acetone levels. Samples NSlOXX and NSlSXX required dilutions due to high
1,2-dichloroethane levels. Concentrations for these analytes exceeded the
calibration range (11 E11 qualifier) in the lesser dilutions; results should be taken
from the secondary dilutions as necessary. Sample NSllXX was run at a 1.67-fold
dilution in order to quantitate acetone. When subsequently run undiluted, the
acetone was not detected. A similar event occurred for sample NSlSXX. Significant
differences in acetone values were also observed for several other samples. It was
believed that the acetone levels varied between vials of the same sample.
The reporting software caused the Form I sample data sheets to contain an extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
tenth of a milliliter.
Semivolatiles Analysis: Samples were extracted and analyzed within holding time
under the CLP OLMOl.B water method. In accordance with project requirements, the
protocol was modified to a target list of bis(2-chloroethyl)ether and 4-nitrophenol
with special detection limits. Nontarget searches were not required.
Samples were analyzed within compliant DFTPP tuning windows.
calibration criteria for the compounds of interest. The method
target compound contamination.
Standards met CLP
blanks were free of
Matrix spike analyses were conducted on sample EX04XX, which showed high recoveries
for 4-nitrophenol (112, 103% > 80%). This may have resulted from the use of
continuous liquid/liquid extractors which have higher statistical recovery windows
than those set for separatory fwmels. In addition, the spikes were run at a
fivefold dilution due to high nontarget compound concentrations. No corrective
action was required for the high recoveries. Values reported on the Form III spike
recovery sheet should be considered accurate to two significant figures.
Internal standard areas and surrogate recoveries were compliant for all analyses.
Sample NSlSXX had a high surrogate NBZ recovery, but the data remained compliant
since no other base/neutral surrogates were out of range. Samples NS09XX and EX03XX
had high NBZ recoveries and EX03XX had a low FBP recovery but the data remained
compliant since these were diluted analyses. The secondary dilution EX03XXDL had all
recoveries within limits. Matrix spike EX04XX received double surrogate during
extraction; recoveries were calculated accordingly and found acceptable.
Samples NS09XX, NSlOXX, EX04XX and EX04XXMS/MSD required dilutions due to high
nontarget compound concentrations. These dilutions were required in order to
maintain instrument performance. Samples NS31XX, EX03XX, EX03XXDL, and EX02XX
required dilutions in order to quantitate high target compound concentrations. The
level of bis(2-chloroethyl)ether exceeded the calibration range in EX03XX; results
for this analyte should be taken from EX03XXDL.
The reporting software caused the Form I sample data sheets to contain an .extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
milliliter.
Metals Analysis: The analytical protocol for metals analytes established for this
project is compliant with the EPA CLP SOW (Document Number ILM03.0) except as noted
below. Samples were analyzed and data reported for the client-designated modified
target list. Matrix QC was performed on the sample designated "EX04XX". Field ID' s
P.O. Box 2130
One Lafayette Road
Hampton, NH 03842
TEL: [phone]
1:/1.V· l::O?.O'Jl::."1Q'Xl
B-2
An Equal Opportunity Employer
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THE ASSURANCE Of OUAL!Tl
SDG Narrative
Case: PCHAR, SDG: NASO?
are modified in order to satisfy a six-character software requirement.
ICP Analysis: Samples were prepared in one water batch on 04/14/95. Samples were
analyzed in one analytical sequence on the TJAOl on 04/17/95. Samples were analyzed
for arsenic and selenium in one analytical sequence on the TJA02 on 04/20/95. The
spike recovery and duplicate precision for sample "EX04XX" met CLP QC limits. All
other QC samples also met CLP QC limits.
Statement of Compliancy and Data Authorization
I certify that this data package is in compliance with the terms and conditions of
the contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package and in
the computer-readable data submitted on floppy diskette has been authorized by the
Laboratory Manager or his designee, as verified by the following signature.
Authorized Signature
PACE Incorporated, New England-New Hampshire
P.O. Box 2130
One Lafayette Road
Hampton, NH 03842
TEL: [phone]
Ci\V· hn-,_O?h.lO'Xl
B ·3
May 3, 1995
An Equal Opportunity Employer
\
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SAMPLE TABLE
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CLIENT ID.
I REPORTED AS MATRIX PACE# PARAMETERS
---------------------------------------------
NS-32 4-3-95
NS32XX WATER 43530-001 ACID EXTRACTABLE$
I BASE/NEUTRAL EXTRACTABLES
43530-013 GC/MS VOA
43530-025 Ba, Be, Cd, Cr, Mn, Ni, Zn,
I As, Se
NS-09 4-3-95
I NS09XX WATER 43530-002 ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLE$
NS09XXDL (VOA) 43530-014 GC/MS VOA
43530-026 Ba, Be, Cd, Cr, Mn, Ni, Zn,
I As, Se
NS-10 4-3-95
I NSlOXX WATER 43530-003 ACID EXTRACTABLE$
BASE/NEUTRAL EXTRACTABLES
NSlOXXDL (VOA) 43530-015 GC/MS VOA
43530-027 Ba, Be, Cd, Cr, Mn, Ni, Zn, I As, Se
NS-30 4-3-95
I NS30XX WATER 43530-004 ACID EXTRACTABLE$
BASE/NEUTRAL EXTRACTABLE$
43530-016 GC/MS VOA
I 43530-028 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
NS-15 4-3-95 I NS15XX WATER 43530-005 ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLE$
NS15XXDL (VOA) 43530-017 GC/MS VOA
I 43530-029 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
I NS-29 4-3-95
NS29XX WATER 43530-006 ACID EXTRACTABLE$
BASE/NEUTRAL EXTRACTABLES
NS29XXDL (VOA) 43530-018 GC/MS VOA I 43530-030 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
I NS-31 4-4-95
NS31XX WATER 43530-007 ACID EXTRACTABLE$
BASE/NEUTRAL EXTRACTABLE$
I NS31XXDL (VOA) 43530-019 GC/MS VOA
43530-031 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
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1•1 >llu"HI 0> Oulll!!
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SAMPLE TABLE
(CONTINUED)
CLIENT ID.
REPORTED AS MATRIX PACE#
-----------------------------------
NS-11 4-4-95
NSllXX WATER 43530-008
NSllXXDL (VOA) 43530-020
43530-032
EX-04 4-4-95
EX04XX WATER 43530-009
*SQC*
EX04XXDL (VOA) 43530-021
43530-033
EX-03 4-4-95
EX03XX WATER 43530-010
EX03XXDL (VOA) 43530-022
43530-034
EX-02 4-4-95
EX02XX WATER 43530-011
EX02XXDL (VOA) 43530-023
43530-035
EX-01 4-4-95
EXOlXX WATER 43530-012
EXOlXXDL (VOA) 43530-024
43530-036
PARAMETERS
----------
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, ·er, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
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Appendix C
Volatile Organics Analysis Data Sheets
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX01XX lab Name: PACE NEW ENGLA Contract:
Lab Code: Case No. PC HAR SAS No. SDG No. NAS07
latrix: (soil/water) WATER Lab Sample ID: 43530-24
.ample wt /vol:
level: ( low/med)
5.00 (g/mL) ML
LOW
Lab Fi1e ID: C8127
Date Received: 04/05/95
I Moisture: not dee. Date Analyzed: 04/13/95
GC Column: SP1000
loil Extract Volume:
ID: 2. 00 (mm) Dilution Factor: 1 . 0
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(uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone ______________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ------------107 -06 - 2 - - - - - - - -1, 2 -Di ch lo roe thane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane ______ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene ______________ _
108-88-3--------Toluene ______________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
I
2 JU
3 JBJ
210 IE
7 JU
5 JU
5 JU
5 JU
6 JU
.5 JU
5 JU
5 JU
10 JU
10 JU
1 0 JU
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FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EXD1XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code: Case No.: PCHAR SAS No. SDG No.: NAS07
latrix: (soil/water) WATER
Sample wt/vol: level: (low/med)
I Moisture: not dee.
5.00 (g/mL) ML
LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
43530-24DL
C8143
04/05/95
04/ 14/95
GC Column: SP1000 ID: 2.00 (mm) Dilution Factor: 1 . 5
loil Extract Volume: (UL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ------------107 -06 - 2 - - - - - - - -1, 2 -Di ch lo roe thane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
3
14
33
1 0
7
7
7
9
7
7
7
15
15
15
Q
u
BO
D
u
u
u
u
u
u
u
u
u
u
u
(uL)
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FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX02XX
tab Name: PACE NEW ENGLA Contract:
Lab Code: Case No. PC HAR SAS No. : SDG No. : NAS07
Jatrix: (soiJ./water) WATER
SampJ.e wt/vol.:
level.: (J.ow/med)
r Moisture: not dee.
5.00 (g/mL) ML
LOW
Lab SampJ.e ID: 43530-23
Lab FiJ.e ID: C8126
Date Received:
Date Analyzed:
GC CoJ.umn: SP1000 ID: 2.00 (mm) Dilution Factor:
04/05/95
04/13/95
8.5
Extract Volume: (UL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------VinyJ. ChJ.oride ________ _ 1 7
75-09-2---------MethyJ.ene ChJ.oride ______ _ 44
67-64-1---------Acetone _____________ _ 36000
75-35-4---------1 ,1-DichJ.oroethene ______ _ 59
67-66-3---------ChJ.oroform ___________ _ 42
107-06-2--------1 ,2-Dichloroethane ______ _ 750
75-27-4---------Bromodichloromethane _____ _ 42
78-87-5---------1 ,2-Dichloropropane _____ _ 1300
79-01-6---------Trichloroethene ________ _ 42
79-00-5---------1,1 ,2-Trichloroethane ____ _ 42
71-43-2---------Benzene _____________ _ 42
108-88-3--------ToJ.uene _____________ _ 280
100-41-4--------EthyJ.benzene __________ _ 85
1330-20-7-------XyJ.ene (total.) _________ _ 24
I 1u
IB
IE
1u
IU
I
IU
I 1u
IU
1u
I
1u
IJ
I
Q
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX02XXDL
" l al1 Name: l
PACE NEW ENGLA Contract:
Lab Code: Case No. PC HAR SAS No. : SDG No.: NAS07
latrix: (soil/water) WATER Lab Sample ID: 43530-23DL
Sample wt/vol:
level: ( low/med)
5.00 (g/mL) ML Lab File ID: C8142
LOW
I; Moisture: not dee.
Date Received:
Date Anal.yzed:
04/05/95
04/ 14/95
GC Column: SP1000 ID: 2.00 (mm) Dilution Factor: 250.0
I
I
I
I
I
I
I
I
Extract Vol.ume: (UL) Soil Al.iquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _ 500
75-09-2---------Methylene Chloride ______ _ 2600
67-64-1---------Acetone _____________ _ 24000
75-35-4---------1,1-Dichloroethene ______ _ 1800
67-66-3---------Chloroform ___________ _ 1200
107-06-2--------1 ,2-0ichl.oroethane ______ _ 1 200
75-27-4---------Bromodichl.oromethane _____ _ 1200
78-87-5---------1 ,2-Dichloropropane _____ _ 1000
7~-01-6---------Trichl.oroethene ________ _ 1 200
79-00-5---------1 ,1,2-Trichloroethane ____ _ 1200
71-43-2---------Benzene _____________ _ 1200
108-88-3--------Toluene _____________ _ 2500
100-41-4--------Ethylbenzene __________ _ 2500
1330-20-7-------Xylene (total) _________ _ 2500
I
IU
IBD
'ID
1u
IU
1u
IU
IDJ
IU
1u
IU
IU
1u
IU
I
Q
(uL)
I
I
.I
FORM I VOA 3/90
\'
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
latrix: (soil./water) WATER
Sampl.e wt/vol.:
level.: (l.ow/med)
5.00 (g/mL) ML
LOW
Moisture: not dee.
Contract:
SAS No.
Lab
Lab
Date
Date
EX03XX
SDG No. : NAS07
Sample ID: 43530-22
File ID: C8125
Received: 04/05/95
Anal.yzed: 04 I 13 / 95 I GC Col.umn: SP1000 ID: 2.00 (mm)
(uL)
Dilution Factor: 8.9
I
I
I
I
I
I
I
I
I
I
I
I
I
Extract Volume: Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride _________ _
75-09-2---------Methyl.ene Chl.oride ______ _
18
41
67-64-1---------Acetone _____________ _ 9800
75-35-4---------1 ,1-Dichloroethene ______ _ 63
67-66-3---------Chl.oroform ___________ _ 45
107-06-2--------1,2-Dichloroethane ______ _ 59
75-27-4---------Bromodichloromethane _____ _ 45
78-87-5---------1 ,2-Dichloropropane _____ _ 160
79-01-6---------Trichloroethene ________ _ 45
79-00-5---------1,1,2-Trichloroethane ____ _ 45
71-43-2---------Benzene _____________ _ 45
108-88-3--------Tol.uene _____________ _ 80
100-41-4--------Ethyl.benzene __________ _ 89
1330-20-7-------Xyl.ene (total.) _________ _ 89
FORM-I VOA
(uL)
a
u
BJ
E
u
u
u
u
u
u
J
u
u
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX03XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code: Case No. PCHAR SAS No. : SDG No.: NAS07
latrix: (soil./water) WATER
.ample wt/vol:
'eve 1: ( low/med)
5.00 (g/mL) ML
LOW
Lab Sampl.e ID: 43530-22DL
Lab Fil.e ID: C8141
Date Received: 04/05/95
Date Analyzed: I Moisture: not dee.
GC Col.umn: SP1000
loil. Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor:
04/14/95
69.4
Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride ________ _
75-09-2---------Methyl.ene Chl.oride ______ _
140
600
67-64-1---------Acetone _____________ _ 9200
75-35-4---------1 ,1-Dichloroethene ______ _ 490
67-66-3---------Chl.oroform ___________ _ 350
107-06-2--------1 ,2-0ichloroethane ______ _ 350
75-27-4---------Bromodichloromethane _____ _ 350
78-87-5---------1 ,2-Dichloropropane _____ _ 420
79-01-6---------Trichloroethene ________ _ 350
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 350
71-43-2---------Benzene _____________ _ 350
108-88-3--------Tol.uene _____________ _ 690
100-41-4--------Ethyl.benzene __________ _ 690
1330-20-7-------Xyl.ene (total.) _________ _ 690
I
IU
IBD
ID
1u
1u
IU
1u
1u
1u
1u
1u
1u
1u
IU
I
Q
(UL)
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
1A EPA SAMPLE NO. I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX04XX
lab Name: PACE NEW ENGLA Contract:
Lab Code: Case No. PCHAR SAS No. SDG No. NAS07
l1atrix: (soil/water) WATER Lab Sample ID: 43530-21
lfample wt/vol:
level: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID: cs1·49
Date Received: 04/05/95
I Moisture: not dee. Date Analyzed: 04/14/95
GC Column: SP1000 ID: 2.00 (mm) Dilution Factor: .1 . 0
I
I
I
I
I
I
I
I
I
I
I
Extract Volume: (UL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone ______________ _
75-35-4---------1,1-Dichloroethene ______ _
67-66-3---------Chloroform ____________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-57 --------1 ,2-Dichloropropane ______ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1,2-Trichloroethane ____ _
71-43-2---------Benzene ______________ _
108-88-3--------Toluene ______________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
2
7
380
7
5
5
5
6
5
5
5
26
10
1 0
a
u
8
E
u
u
u
u
u
u
u
u
(uL)
I
I
FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
EX04XXDL tab Name: PACE NEW ENGLA Contract:
Lab Code: Case No. PCHAR SAS No. SDG No.: NAS07
l,atrix: (soil./water) WATER Lab SampJ.e ID: 43530-21DL
Jampl.e wt /vol.:
l.eveJ.: (J.ow/med)
5.00 (g/mL) ML
LOW
Lab Fil.e ID: C8137
Date Received: 04/05/95
r Moisture: not dee. Date Anal.yzed: 04/ 14/95
GC CoJ.umn: SP1000 ID: 2.00 (mm) Dil.ution Factor: 31. 2
Extract Yol.ume: (uL) Soil. Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. ChJ.oride ________ _
75-09-2---------MethyJ.ene ChJ.oride ______ _
62
180
67-64-1---------Acetone _____________ _ 11 00
75-35-4---------1 ,1-Dichl.oroethene ______ _ 220
67-66-3---------ChJ.oroform ___________ _ 160
107-06-2--------1,2-DichJ.oroethane ______ _ 160
75-27-4---------Bromodichloromethane _____ _ 160
78-87-5---------1 ,2-0ichl.oropropane _____ _ 190
79-01-6---------Trichl.oroethene ________ _ 160
79-00-5---------1,1 ,2-Trichl.oroethane ____ _ 160
71-43-2---------Benzene _____________ _ 160
108-88-3--------ToJ.uene _____________ _ 310
100-41-4--------EthyJ.benzene __________ _ 310
1330-20-7-------XyJ.ene (total.) _________ _ 310
I
IU
IBD
ID
1u
IU
1u
IU
1u
1u
1u
IU
IU
IU
1u
I
Q
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS09XX lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PCHAR SAS No. : SDG No.: NAS07
(soiJ./water) WATER Lab SampJ.e ID: 43530-14
lilampJ.e wt/vol.: 5.00 (g/mL) ML Lab FiJ.e ID: C8106
.eveJ.: (J.ow/med) LOW Date Received: 04/05/95
I Moisture: not dee. Date Anal.yzed: 04/12/95
GC CoJ.umn: SP1000 ID: 2.00 (mm) Dilution Factor: , I oil.
I
i
I
I
,1
Extract Volume: ( u L) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------VinyJ. ChJ.oride ________ _ 200
75-09-2---------MethyJ.ene ChJ.oride ______ _ 1300
67-64-1---------Acetone _____________ _ 74000
75-35-4---------1,1-Dichloroethene ______ _ 700
67-66-3---------ChJ.oroform ___________ _ 500
107-06-2--------1 ,2-0ichloroethane ______ _ 500
75-27-4---------Bromodichloromethane _____ _ 500
78-87-5----~----1 ,2-Dichloropropane _____ _ 600
79-01-6---------TrichJ.oroethene ________ _ 500
79-00-5---------1 ,1,2-Trichloroethane ____ _ 500
71-43-2---------Benzene _____________ _ 500
108-88-3--------ToJ.uene _____________ _ 340
100-41-4--------EthyJ.benzene __________ _ 1 000
1330-20-7-------XyJ.ene (total.) ________ _ 1000
100.0
Q
u
B
E
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u
u
u
u
u
u
u
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u
u
( u L)
I
I
I
I
I
I
I
I
FORM I VOA 3/90
"
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS09XXDL lab Name: PACE NEW ENGLA Contract:
Case NO.: PC HAR SAS No. : SDG No. : NAS07 Lab Code:
latrix: (soil/water) WATER Lab Sample ID: 43530-14DL
ramp le wt /vol.:
~evel: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
Date Received:
C8117
04/05/95
t Moisture: not dee. Date Analyzed: 04/13/95
GC Column: SP1000 loil Extract Volume:
ID: 2.00 (mm) Dil.ution Factor: soc.a
I
I
I
I
I
I
I
I
I
I
I
i
I
(UL) Soil Aliquot Volume: (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _ 1000
75-09-2---------Methylene Chloride ______ _ 3700
67-64-1---------Acetone _____________ _ 87000
75-35-4---------1 ,1-Dichloroethene ______ _ 3500
67-66-3---------Chloroform ___________ _ 2500
107-06-2--------1,2-Dichl.oroethane ______ _ 2500
75-27-4---------Bromodichl.oromethane _____ _ 2500
78-87-5---------1 ,2-0ichloropropane _____ _ 3000
79-01-6---------Trichloroethene ________ _ 2500
79-00-5---------1,1,2-Trichloroethane ____ _ 2500
71-43-2---------Benzene _____________ _ 2500
108-88-3--------Toluene _____________ _ 5000
100-41-4--------Ethylbenzene __________ _ 5000
1330-20-7-------Xylene (total) ________ _ 5000
FORM I VOA
Q
I
\U
\BO
\D
1u
\U
\U
\U
\U
\U
\U
\U
1u
\U
\U
I
3/90
"
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
Jab Name: PACE NEW ENGLA
Case No.: PC HAR Lab Code:
~atrix: (soi1/water) WATER
Samp1e wt/voi:
leve1: (1ow/med)
5.00 (g/mL) ML
LOW
t Moisture: not dee.
Contract:
SAS No.
Lab
Lab
Date
Date
NS10XX
SDG No.: NAS07
Samp1e ID: 43530-15
File ID: C8107
Received: 04/05/95
Ana1yzed: 04/12/95
, GC coiumn: SP1000 ID: 2.00 (mm) Dilution Factor: 17.9
I
I
I
I
I
I
I
I
I
I
I
I
I
Extract Volume: (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyi Ch1oride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Ch1oroform ___________ _
36
230
800
130
89
107-06-2--------1 ,2-Dichloroethane ______ _ 12000
75-27-4---------Bromodichloromethane _____ _ 89
78-87-5---------1 ,2-Dichloropropane _____ _ , , 0
79-01-6---------Trichloroethene ________ _ 89
79-00-5---------1,1,2-Trichloroethane ____ _ 89
71-43-2---------Benzene _____________ _ 89
108-88-3--------Toiuene _____________ _ 180
100-41-4--------Ethy1benzene __________ _ 180
1330-20-7-------xyiene (tota1) ________ _ 180
FORM I VOA
I
IU
IB
I
IU
1u
IE
IU
1u
IU
1u
IU
1u
IU
1u
I
(UL)
Q
3/90
"
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS10XXDL tab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No. PCHAR SAS No. SDG No.: NAS07
(soil/water) WATER Lab Sampl.e ID: 43530-15DL
lllfample wt/vol:
'tevel: (low/med)
5.0D (g/mL) ML
LOW
Lab File ID: C8118
Date Received: 04/05/95
I Moisture: not dee. Date Anal.yzed: 04/13/95
GC Column: SP1000
loil Extract Volume:
ID: 2.00 (mm) Dil.ution Factor: 83.3
I
,, . I
I I
I
I
I I
I
1.
I I
I
I
I
I I
I
I
I I
I
-1
I
' I
I
I
(UL) Soil Al.iquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _ 170
75-09-2---------Methylene Chloride ______ _ 580
67-64-1---------Acetone _____________ _ 1800
75-35-4---------1 ,1-Dichloroethene ______ _ 580
67-66-3---------Chloroform ___________ _ 420
107-06-2--------1 ,2-Dichloroethane ______ _ 9800
75-27-4---------Bromodichl.oromethane _____ _ 420
78-87-5----~----1 ,2-Dichloropropane _____ _ 500
79-01-6---------Trichl.oroethene ________ _ 420
79-00-5---------1,1,2-Trichl.oroethane ____ _ 420
71-43-2---------Benzene _____________ _ 420
108-88-3--------Toluene _____________ _ 830
100-41-4--------Ethylbenzene __________ _ 830
1330-20-7-------Xylene (total) ________ _ 830
u
BO
D
u
u
D
u
u
u
u
u
IU
1u
1u
I
Q
(UL)
I FORM I VOA 3/90
I
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS11XX lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PCHAR SAS No. : SDG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-20
.ample wt/vol:
11.evel: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
Date Received:
C8136
04/05/95
I Moisture: not dee. Date Analyzed: 04/ 14/95
GC Column: SP1000 loil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 1.0
(uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
I
2 1u
7 IB
10 1u
7 u
5 u
5 u
5 u
6 u
5 u
5 u
5 u
1 1
76
44
Q
(uL)
I
I
I
I
I
I
I
I
I
I
i
I
FORM I VOA 3/90
"
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS11XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No. PCHAR SAS No. : SOG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-20DL
1 ampl.e wt/vol.:
~evel.: (l.ow/med) LOW
5.00 (g/mL) ML Lab Fil.e IO:
Date Received:
C8122
04/05/95 I Moisture: not dee. Date Anal.yzed: 04/13/95
GC Col.umn: SP1000 loil. Extract Vol.ume:
IO: 2.00 (mm)
(uL)
Dilution Factor: 1.7
Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
75-01-4---------Vinyl Chl.oride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethyl.benzene __________ _
1330-20-7-------Xylene (total.) _________ _
I
3 IU
10 IBD
130 ID
1 2 1u
8 IU
8 1u
8 1u
10 1u
8 1u
8 1u
8 1u
12 IDJ
78 ID
45 10
I
Q
(uL)
I
I
I
I
I
I
I
FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
latrix: (soil/water) WATER
11ampl.e wt/vol:
llevel: (low/med)
5.00 (g/mL) ML
LOW
I Moisture: not dee.
Contract:
SAS No. :
NS15XX
SDG No.: NAS07
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
43530-17
C8120
04/05/95
04 I 13 /95
GC Column: SP1000 ID: 2.00 (mm) Dil.ution Factor: 1 . 0
I oil
I
I
I
I
I
I
I
I
I
I
I
I
I
Extract Vol.ume: (uL) Soil Al.iquot Vol.ume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methyl.ene Chl.oride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-0ichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
FORM I VOA
I
4 I
5 IB
10 jU
7 u
5 u
290 E
s u
6 u
5 u
5 u
5 u
8 J
1 0 u
10 u
(uL)
Q
3/90
\
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
NS15XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code: Case No.: PC HAR SAS No. SDG No.: NAS07
latrix: (soil/water) WATER Lab Sample ID: 43530-17DL
Sample wt/vol:
level: ( low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
Date Received:
C8123
04/05/95
I Moisture: not dee. Date Anal.yzed: 04/13/95
GC Column: SP1000 ID: 2.00 (mm) Dilution Factor: 2.0
loil Extract Volume: (UL) Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
I 67-64-1---------Acetone _____________ _
I
I
I
I
I
I
I
I
I
I
I
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
I ____________________ _
I
4 ID
10 IBD
55 ID
14 IU
10 1u
330 ID
10 1u
12 1u
10 IU
10 1u
1 0 IU
10 IDJ
20 IU
20 1u
I
Q
( u L)
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS29XX lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No. PCHAR SAS No. SDG No. NAS07
(soi1/water) WATER Lab Samp1e ID: 43530-18
jamp1e wt/voi:
eve1: ( iow/med)
5.00 (g/mL) ML
LOW
Lab Fi1e ID:
Date Received:
C8124
04/05/95
I Moisture: not dee.
GC Co1umn: SP1000
Date Anaiyzed: 04/13/95
I
I
I
I
I
I
I
I
I
I
I
ID: 2.00 (mm) Dilution Factor: 2.5
Extract Volume: (UL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
75-01-4---------Vinyi Ch1oride _________ _ I
75-09-2---------Methyiene Ch1oride ______ _ I
67-64-1---------Acetone ______________ _ I
75-35-4---------1,1-Dichloroethene ______ _ I
67-66-3---------Ch1oroform ____________ _ I
107-06-2--------1 ,2-Dichloroethane ______ _ I
75-27-4---------Bromodichloromethane _____ _ I
78-87-5---------1,2-Dichloropropane ______ _ I
79-01-6---------Trichloroethene ________ _ I
79-00-5---------1 ,1 ,2-Trich1oroethane ____ _ I
71-43-2---------Benzene ______________ _ I
108-88-3--------Toiuene ______________ _ I
100-41-4--------Ethy1benzene __________ _ I
1330-20-7-------Xyiene (tota1) _________ _ I
I
5 u
1 3 B
540 E
18 u
12 u
37
1 2 u
12 J
12 u
1 2 u
1 2 u
25 u
25 u
25 1u
I
Q
(UL)
I
I
FORM I VOA 3/90
1A EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
NS29XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PC HAR SAS No. SDG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-18DL
jample wt/vol:
.evel: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
Date Received:
C8119
04/05/95
Date Analyzed: 04/13/95 I Moisture: not dee.
GC Column: SP1000
loil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 12.5
(UL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
25
81 I
I
I
I
I
I
I
67-64-1---------Acetone _____________ _ 11 00
75-35-4---------1,1-Dichloroethene ______ _ 88
67-66-3---------Chloroform ___________ _ 62
107-06-2--------1,2-Dichloroethane ______ _ 42
75-27-4---------Bromodichloromethane ------62
78-87-5---------1 ,2-Dichloropropane _____ _ 75
79-01-6---------Trichloroethene ________ _ 62
79-00-5---------1,1,2-Trichloroethane ____ _ 62
71-43-2---------Benzene _____________ _ 62
108-88-3--------Toluene _____________ _ 120
100-41-4--------Ethylbenzene _________ _ 120
1330-20-7-------Xylene (total) ________ _ 120
'I
I
IU
IBD
ID
1u
1u
IDJ
1u
1u
1u
IU
IU
IU
1u
1u
I
Q
(uL)
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS30XX lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PC HAR SAS No. : SDG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-16
11 ample wt/vol:
level: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
_Date Received:
C8102
04/05/95
I Moisture: not dee. Date Anal.yzed: 04/12/95
GC Column: SP1000 loil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 1 . 0
(uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4-----~--Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
I
2· IU
10 IB
10 1u
7 1u
5 1u
5 IU
5 1u
6 IU
5 1u
5 1u
5 1u
10 IU
1 0 IU
10 1u
I
Q
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
\
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS31XX lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PCHAR SAS No. : SDG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-19
jample wt/vol:
'evel: ( low/med) LOW
5.00 (g/mL) ML Lab File ID:
Da"te Received:
C8121
04/05/95
Date Analyzed: 04/13/95 I Moisture: not dee.
GC Column: SP1000
loil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 2. 1
(uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
4
16
67-64-1---------Acetone _____________ _ 2500
75-35-4---------1 ,1-Dichloroethene ______ _ 1 5
67-66-3---------Chloroform ___________ _ ·1 0
107-06-2--------1 ,2-Dichloroethane ______ _ 41
75-27-4---------Bromodichloromethane _____ _ 10
78-87-5---------1 ,2-Dichloropropane _____ _ 50
79-01-6---------Trichloroethene ________ _ 10
79-00-5---------1,1,2-Trichloroethane ____ _ 10
71-43-2---------Benzene _____________ _ 10
108-88-3--------Toluene _____________ _ 1 2
100-41-4--------Ethylbenzene __________ _ 21
1330-20-7-------Xylene (total) _________ _ 21
I
IU
IB
IE
IU
1u
I
IU
I
IU
1u
IU
IJ
1u
1u
I
a
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
\
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS31XXDL lab Name: PACE NEW ENGLA Contract:
Lab Code:
latrix:
Case No.: PCHAR SAS No. : SDG No.: NAS07
(soil/water) WATER Lab Sample ID: 43530-19DL
iample wt/vol: 5.00 (g/mL) ML Lab File ID: C8128
evel: (low/med) I Moisture: not dee.
GC Column: SP1000
,~il Extract Volume:
LOW Date Received:
Date Anal.yzed:
04/05/95
04/13/95
ID: 2.00 (mm) Dilution Factor: 167.0
(uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _ 330
75-09-2---------Methylene Chloride ______ _ 760
67-64-1---------Acetone _____________ _ 15000
75-35-4---------1,1-Dichloroethene ______ _ 1200
67-66-3---------Chloroform ___________ _ 830
107-06-2--------1 ,2-Dichloroethane ______ _ 830
75-27-4---------Bromodichloromethane _____ _ 830
78-87-5---------1 ,2-Dichloropropane _____ _ 1000
79-01-6---------Trichloroethene ________ _ 830
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 830
71-43-2---------Benzene _____________ _ 830
108-88-3--------Toluene _____________ _ 1700
100-41-4--------Ethylbenzene __________ _ 1 700
1330-20-7-------Xylene (total) ________ _ 1700
a
I
JU
JBDJ
ID
JU
JU
JU
JU
JU
JU
JU
JU
JU
JU
JU
I
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
"
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Case No.: PCHAR Lab Code:
latrix: (soil/water) WATER
11ample wt/vol:
'evel: (low/med)
5.00 (g/mL) ML
LOW
Contract:
SAS No.
Lab
Lab
Date
Date
NS32XX
SDG No.: NAS07
Sample ID: 43530-13
File ID: C8101
Received: 04/05/95
Analyzed: 04/12/95 I Moisture: not dee.
GC Column: SP1000
loil Extract Vol.ume:
ID: 2.00 (mm) Dilution Factor: 1 . 0
(uL) Soil Aliquot Volume:
I CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
I
I
I
I
I
I
I
I
I
I
I
I
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1,2-Trichloroethane ____ _
71-43-2---------Benzene ____________ _
108-88-3--------Toluene ____________ _
100-41-4--------Ethylbenzene _________ _
1330-20-7-------Xylene (total) ________ _
FORM I VOA
2·
1 1
1 0
7
5
5
5
6
5
5
5
10
1 0
10
(UL)
Q
u
8
u
u
u
u
u
u
u
u
u
u
u
1u
I
3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Appendix D
Semivolatile Organics Analysis Data Sheets
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PC HAR latrix: (soiJ./water) WATER
lfamp1e wt/vo1:
.eveJ.: (J.ow/med)
970.0 (g/mL) ML
LOW
r Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection VoJ.ume: 2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX01XX
Contract:
SAS No. SDG No.: NAS07
(uL)
Lab SampJ.e ID:
Lab Fil.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-12
H8214
04/05/95
04/08/95
04/12/95
1 . 0
Q
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-ChJ.oroethyJ.)ether ___ _ 3
26
I
IJ
1u 100-02-7--------4-NitrophenoJ. _________ _
________ 1 __ _
FORM I SV-1 3/90
1 8 EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PC HAR
l,atrix: (soil/water) WATER
Sample wt/vo1:
level: (low/med)
940.0 (g/mL) ML
LOW
r Moisture: decanted: (YIN)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC
I
Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
EX02XX
Contract:
SAS No. SDG No.: NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-1 1
H8234
04/05/95
04/08/95
04/13/95
10.0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 650
270
I
IU 100-02-7--------4-Nitrophenol _________ _
-----'------1 __ _
FORM I SV-2 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name;
Lab Code:
PACE NEW ENGLA
Case No. PC HAR latrix: (soil/water) WATER
Sample wt/vol:
level: (low/med) LOW
960.0 (g/mL) ML
I Moisture: decanted: (Y /N)
Concentrated Extract Volume: 1000
Injection Volume: 2.D(uL)
GPC
I
Cleanup:
CAS NO.
(Y/N) N pH;
COMPOUND
EX03XX
Contract:
SAS No. ; SDG No.: NAS07
(UL)
Lab Sample ID:
Lab Fi::Le ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS;
(ug/L or ug/Kg) UG/L
43530-10
H8217
04/05/95
04/08/95
04/12/95
2.0
Q
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 220
52
I
IE
1u 100-02-7--------4-Nitrophenol _________ _
________ 1 __ _
FORM I SV-3 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR latrix: (soil/water) WATER
Sample wt/vol:
level: (low/med)
I Moisture:
960.0 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC
I
Cleanup:
CAS NO.
(Y/N) N pH:
COMPOUND
EX03XXDL
Contract:
SAS No. SDG No. : NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-10DL
H8233
04/05/95
04/08/95
04/1.3/95
4.0
Q
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 180
100
I
ID
IU 100-02-7--------4-Nitrophenol. _________ _
________ I __ _
FORM I SV-4 3/90
1 B EPA SAMPLE NO. I SEMIYOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Case No.: PCHAR Lab Code:
latrix: (soi1/water) WATER
.;ampl.e wt/vol.:
.. evei: (1ow/med)
910.0 (g/mL) ML
LOW
I Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Vol.ume: 2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX04XX
Contract:
SAS No. : SDG No.: NAS07
(UL)
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Extracted:
Date Anaiyzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-9
H8219
04/05/95
04/08/95
04/12/95
5.0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Ch1oroethy1)ether ___ _ 55
140
I
IU 100-02-7--------4-Nitrophenoi _________ _
_______ 1 __ _
FORM I sy.:.5 3/90
1 8 EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
latrix: (soil/water) WATER
aampl.e wt/vol.:
'evel: (low/med)
920.0 (g/mL) ML
LOW
I Moisture: decanted: (Y/N)
Concentrated Extract Vol.ume: 1000
Injection Vol.ume: 2.0(uL)
Cl.eanup: (Y/N) N pH:
CAS NO. COMPOUND
NS09XX
Contract:
SAS No. SDG No.: NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Di l.ut ion Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-2
H8218
04/05/95
04/08/95
04 / 1 2 / 95
5.0
Q
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _
I
27 I u
, 40 . I u 100-02-7--------4-Nitrophenol _________ _
________ 1 __ _
'I FORM I SV-6 3/90
I
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
l,atrix: (soil/water) WATER
(
ample wt/vol:
evel: (low/med)
1 000
LOW
(g/mL) ML
I Moisture: decanted: (YIN)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC
I
Cleanup:
CAS NO.
(Y/N) N pH:
COMPOUND
NS10XX
Contract:
SAS No. : SDG No. : NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-3
H8235
04/05/95
04/08/95
04/13/95
50.0
Q
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 250
1200
I
1u
1u 100-02-7--------4-Nitrophenol _________ _ _______ I __ _
FORM I SV-7 3/90
!1
I
I
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
tab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
l,atrix: (soil/water) WATER
Sample wt/vol:
level: (low/med)
940.0 (g/mL) ML
LOW
I Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC
I
Cleanup:
CAS NO.
(Y /N) N
COMPOUND
pH:
NS11XX
Contract:
SAS No. : SDG No.: NAS07
(UL)
Lab Sample ID:
Lab Fil.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-8
H8213
04/05/95
04/08/95
04/12/95
, . 0
Q
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 5
27
I
1u
1u 100-02-7--------4-Nitrophenol. _________ _
________ I __ _
FORM I SV-8 3/90
1 8 EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
l,atrix: (soil/water) WATER
r/amp1e wt/vol:
level: (low/med)
I Moisture:
890.0 (g/mL) ML
LOW
decanted: ( y / N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS15XX
Contract:
SAS No. SDG No.: NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-5
H8215
04/05/95
04/08/95
04/12/95
1 . 0
a
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 6
28
I
IU
1u 100-02-7--------4-Nitrophenol. _________ _
________ I __ _
FORM I SV-9 3/90
1 B EPA SAMPLE NO.
I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
11atrix: (soil/water) WATER
Sample wt/vol: 940.0 (g/mL) ML
level.: (low/med) LOW
a, Moisture:
~oncentrated
decanted: (Y/N)
Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
NS29XX
Contract:
SAS No. SDG No.: NAS07
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-6
H8212
04/05/95
04/08/95
04/12/95
, . 0
Q
I
I
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 32
27
I
1u 100-02-7--------4-Nitrophenol _________ _
________ 1 __ _
FORM I SV-1 3/90
1 B EPA SAMPLE NO.
I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
latrix: (soil/water) WATER
Sampl.e wt/vol.:
level: (low/med) LOW
900.0 (g/mL) ML
I Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
I CAS NO. COMPOUND
NS30XX
Contract:
SAS No. SDG No.: NAS07
(uL)
Lab Sampl.e ID:
Lab F il.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Di l.ut ion Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-4
H8211
04/05/95
04/08/95
04/12/95
1 . 0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 16
28
I
1u 100-02-7--------4-Nitrophenol. _________ _
________ 1 __ _
FORM I SV-2 3/90
1 8 EPA SAMPLE NO.
I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
latrix: (soil/water) WATER
Sample wt /vol: 980.0 (g/mL) ML
level: (low/med) LOW
I Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
GPC Cleanup: (YIN) N pH:
I CAS NO. COMPOUND
NS31XX
Contract:
SAS No. : SDG No.: NAS07
(uL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-7
H8216
04/05/95
04/08/95
04/12/95
2.0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 78
51
I
1u 100-02-7--------4-Nitrophenol. _________ _
________ 1 __ _
FORM I SV-3 3/90
1 B EPA SAMPLE NO.
D SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Dab Name: PACE NEW ENGLA
Lab Code:
ltatrix: (soil/water)
Sample wt/vol:
level: (low/med)
I Moisture:
,oncentrated Extract
Injection Volume:
Case No. PCHAR
WATER
970.0 (g/mL) ML
LOW
decanted: (Y /N)
Volume: 1 000
2.0(uL)
GPC Cl.eanllp: (Y/N) N pH:
I CAS NO. COMPOUND
NS32XX
Contract:
SAS No. SDG No.: NAS07
( u L)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
43530-1
H8210
04/05/95
04/08/95
04/12/95
1 . 0
Q
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 5
26
I
1u
IU 100-02-7--------4-Nitrophenol _________ _
________ 1 __ _
FORM I SV-4 3/90
I
I
I
I
I
I ,,
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Contract:
SAS No. :
EXOlXX
SDG No. : MNAS07
Lab Sample ID: 43530-036
Date Received: 04/06/95
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.7 u p
7440-39-3 Barium 26.5 B p
7440-41-7 Beryllium 0.20 u p
7440-43-9 Cadmium 1. 4 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.0 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 53.4 p
7439-97-6 Mercury NR
7440-02-0 Nickel 5.5 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.7 B p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 9.4 B p
cyanide NR
- -
I color Before: COLORLESS Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
I Color After:
Comments:
I
I
I
COLORLESS Artifacts:
FORM I -IN 3/90
I
••
I
I
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO .
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Contract:
SAS No. :
EX02XX
SDG No. : MNAS07
Lab Sample ID: 43530-035
Date Received: 04/06/95
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 3.8 B p
7440-39-3 Barium 1860 p
7440-41-7 Beryllium 0.23 B p
7440-43-9 Cadmium 1.4 u p
-= 7440-70-2 Calcium NR
7440-47-3 Chromium 2.0 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 18800 p
7439-97-6 Mercury NR
7440-02-0 Nickel 5.5 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 3.0 B p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 5.8 u p
cyanide NR
--
,I color Before: COLORLESS Clarity Before: CLEAR
Clarity After: CLEAR
Texture: I Color After:
Comments:
I
I
I
YELLOW Artifacts:
FORM I -IN 3/90
I
I
I
I
I
I
I
I
1.
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Contract:
SAS No. :
EX03XX
SDG No.: MNAS07
Lab Sample ID: 43530-034
Date Received: 04/06/95
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.7 u p
7440-39-3 Barium 475 p
7440-41-7 Beryllium 0.20 u p
7440-43-9 Cadmium 1. 4 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.0 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 4810 p
7439-97-6 Mercury NR
7440-02-0 Nickel 5.5 u p
7440-09-7 Potassium NR
.7782-49-2 Selenium 2.7 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 16.0 B p
cyanide NR
--
·'color Before: COLORLESS Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
I Color After:
I
I
Comments:
COLORLESS Artifacts:
FORM I -IN 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Contract:
SAS No.:
EX04XX
SDG No. : MNAS07
Lab Sample ID: 43530-033
Date Received: 04/06/95
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.7 u p
7440-39-3 Barium 72.7 B p
7440-41-7 Beryllium 0.28 B p
7440-43-9 Cadmium 1. 4 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.0 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 4170 p
7439-97-6 Mercury NR
7440-02-0 Nickel 5.5 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.7 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 5.8 u p
cyanide NR
- -
I Color Before: COLORLESS Clarity Before: CLEAR Texture:
I Color After:
I
I
I
Comments:
COLORLESS Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No. : PCHAR SAS No. :
EPA SAMPLE NO.
NS09XX
I Matrix (soil/water): WATER
SDG No. : MNAS07
Lab Sample ID: 43530-026
Date Received: 04/06/95 Level (low/med):
% Solids:
LOW
0.0 I
I
I
1,
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I color Before: WHITE
I Color After:
I
I
I
Comments:
YELLOW
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.7 u
Barium 2030
Beryllium 0.22 B
Cadmium 1. 4 u
Calcium
Chromium 127
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 51800
Mercury
Nickel 43.6
Potassium
Selenium 2.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 141
cyanide
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH Contract:
EPA SAMPLE NO.
NSl0XX
u
m
I
I
Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER Lab Sample ID: 43530-027
Date Received: 04/06/95 Level (low/med) : I % Solids:
LOW
0.0
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0·
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
.Color After:
· Comments:
I
COLORLESS
Analyte Concentration C Q M
Aluminum -NR
Antimony NR
Arsenic 2.7 u p
Barium 193 B p
Beryllium 0.20 u p
Cadmium 1.4 u p
Calcium NR
Chromium 4.0 B p
Cobalt NR
coeeer NR
Iron NR
Lead NR
Magnesium NR
Manganese 8960 p
Mercury NR
Nickel 20.1 B p
Potassium NR
Selenium 2.7 u p
Silver NR
Sodium NR
Thallium NR
Vanadium NR
Zinc 24.8 p
cyanide NR
--
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
0
0
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No. : PCHAR SAS No. :
EPA SAMPLE NO.
NSllXX
I Matrix (soil/water): WATER
SDG No. : MNAS07
Lab Sample ID: 43530-032
Date Received: 04/06/95 Level (low/med):
% Solids:
LOW
0.0 I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
I
I
I
Comments:
COLORLESS
Analyte Concentration C
Aluminum -
Antimony
Arsenic 2.7 u
Barium 140 B
Beryllium 0.24 B
Cadmium 1. 4 u
Calcium
Chromium 2.0 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 62.6
Mercury
Nickel 5.5 u
Potassium
Selenium 2.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 13.2 B
cyanide
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
U.S. EPA -CLP
1
EPA SAMPLE NO.
0
u
m
I
INORGANIC ANALYSIS DATA SHEET
NS15XX
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER
Level (low/med): I % Solids:
LOW
0.0
Lab Sample ID: 43530-029
Date Received: 04/06/95
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
lcolor Before: COLORLESS
.Color After:
Comments:
I
I
I
COLORLESS
Analyte Concentration C Q M
-Aluminum NR
Antimony NR
Arsenic 2.7 u p
Barium 428 p
Beryllium 0. 20 u p
Cadmium 1. 4 u p
Calcium NR
Chromium 2.0 u p
Cobalt NR
coeeer NR
Iron NR
Lead NR
Magnesium NR
Manganese 16800 p
Mercury NR
Nickel 5.5 u p
Potassium NR
Selenium 2.7 u p
Silver NR
Sodium NR
Thallium NR
Vanadium NR
Zinc 5.8 u p
cyanide NR
--
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
m
0
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
NS29XX
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 43530-030
Date Received: 04/06/95
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.7 u p
7440-39-3 Barium 84.7 B p
7440-41-7 Beryllium 0. 20 u p
7440-43-9 Cadmium 1.4 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.0 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 268 p
7439-97-6 Mercury NR
7440-02-0 Nickel 5.5 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.7 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 5.8 u p
cyanide NR
--
I Color Before: COLORLESS Clarity Before: CLEAR
Clarity After: CLEAR
Texture: I Color After:
I
I
I
Comments:
COLORLESS Artifacts:
FORM I -IN 3/90
U.S. EPA -CLP
1
EPA SAMPLE NO.
I
0
D
I
INORGANIC ANALYSIS DATA SHEET
NS30XX
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER
Level (low/med):
I % Solids:
LOW
0.0
Lab Sample ID: 43530-028
Date Received: 04/06/95
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
I
I
I
Comments:
COLORLESS
Analyte Concentration C
Aluminum -
Antimony
Arsenic 2.7 u
Barium 27.5 B
Beryllium 0. 20 u
Cadmium 1.4 u
Calcium
Chromium 2.0 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 2290
Mercury
Nickel 5.5 u
Potassium
Selenium 2.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 5.8 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
U.S. EPA -CLP
1
EPA SAMPLE NO.
a
D
E
I
INORGANIC ANALYSIS DATA SHEET
NS31XX
Lab Name: PACE Inc., NE-NH Contract:
Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER
Level (low/med): I % Solids:
LOW
0.0
Lab Sample ID: 43530-031
Date Received: 04/06/95
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
.7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
'lcolor Before: COLORLESS
.Color After:
Comments:
I
I
I
COLORLESS
Analyte Concentration C
Aluminum -
Antimony
Arsenic 2.9 B
Barium 12.6 B
Beryllium 0.20 u
Cadmium 1. 4 u
Calcium
Chromium 2.0 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 25.8
Mercury
Nickel 5.5 u
Potassium
Selenium 2.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 5.8 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
u
u
Lab
Lab
Name: PACE Inc. ,
Code:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
NE-NH Contract:
EPA SAMPLE NO.
NS32XX
Case No. : PCHAR SAS No.: SDG No.: MNAS07
Matrix (soil/water): WATER Lab Sample ID: 43530-025
Date Received: 04/06/95 Level (low/med): LOW
% Solids: o.o I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
, Comments:
I
I
I
COLORLESS
Analyte Concentration C
Aluminum -
Antimony
Arsenic 2.8 B
Barium 93.3 B
Beryllium 0.28 B
Cadmium 1. 4 u
Calcium
Chromium 2.0 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 117
Mercury
Nickel 5.5 u
Potassium
Selenium 3.2 B
Silver
Sodium
Thallium
Vanadium
Zinc 6.0 B
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
0
fl
I
I
I
I
I
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I
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I
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Appendix F
Chain-of-Custody Records
--

-
Additional Comments
2
---

-
CHAIN-OF-CUSTODY RECORD
Analytical Request '
Report To /(c, 11 Kfu f/ Pace Client No.
BillTo Po. Box 3?f Pace Project Manager
P.O. # I Billing Relerence 9 7-/ [2 &£
'
Pace Project No.
Project Name I No. •Requested Due Date:
a: PRESERVATIVES
w z D ii' w
z >
0 a: w 0 Cf) u.. w
0 a:
0 a. z z ::::,
J~
If
/ X
0 O <
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I X
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X
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X
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't.
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-,;)(,,,
X
X
f : • • I
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REMARKS
.. r:
ACCEPTED BY / AFflllATION . . '
--. . , ... -~:'.W~---1~;· /-~
.... ,.,,.,.,!.
SEE REVERSE SIDE FOR INSTRUCTIONS
-·f C;i.ili:l -

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-

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ENVIRONMENTAL LABORATORIES
Report To ,k,,/ k/4; -//7---
BillTo Po.Baz 32'9
P.O. # , 'Billing Reference 97-/ 1/ (jJ £
Project Name / No.
a: PRESERVATIVES w 1---~-~--~---< z
-------------------------< ~
S pier Si z 0 0
Additional Comments
c5 0 <(
UJ z O I I >
X X
X
X
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CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
2 SEE REVERSE SIDE FOR INSTRUCTIONS
-C~;XiU;l -

-

-
ENVIRONMENTAL LABORATORIES
Client
11'1 ,;,,,•q -~1· 0 '
. ,, ,/'1 . ·. '. ' .
:"••; ,-,.,~ ,_,~•;r!
'
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ii
c5 Cl/. I
Report To: Kc::11
BillTo; R o.
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Box 399
-
P.O.# I Billing Reference 9 7-/ -/2 (j) £:
Project Name/ No.
r:S ., z 0 I >
X --
X
)(
X
X
X
X
X
X,,
)(
X ·x
RELINQUISHED BY/ AFFILIATION
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
•Requested Due Dale:
REMARKS
,,·
' : . .
'---~-~~---1 ''~-~~
Additional Comments
2 SEE REVERSE SIDE FOR INSTRUCTIONS
·fC1.iti:l
ENVIRONMENTAL LABORATORIES
.
1
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s·· r -ll .. f:i--:Jl: ,9" ._
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Additional Comments
2
(/) a: w z 0 ~ w
z 6: 8 ~ w a:
0. z :::,
Report To kc.&, KltA ffz
Bill To f!o 8o'X. £92
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
PO #/Billing Reference 97 -/].J /a£ Pace Project No.
Proje"ct Name/ No.
PRESERVATIVES
0 O c:: C1,. Z 0
I I >
><
ANALY
REOUE
X ·•·,.. r.
•Requested Due Date:
REMARKS
., .
v•~--_v,0-,,,,,.Wc~ 1/ -:5. l ;S.
SEE REVERSE SIDE FOR INSTRUCTIONS
-uLal -

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ENVIRONMENTAL LABORATORIES
. .. ll ·t!t:/l. , .. ··.
2 /(.,. ··.• .. 'f.~'f :.95'"
3 '.i,.. 1/-:'I-: 96
4
s·
Additional Comments
2
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: "•'"'!
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IX
I
I ,
ReporlTo J(eN klu + l:z
BillTo t?o. Bax 399
P.O.# I Billing Relerence CJ7-/ ? 2 0 Lj"'
Project Name/ No.
x
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
--
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3
Additional Comments
2
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---0 of JO --

-
Report To Kefl/ !<lu t-tz_ '
Bill ro .Po Bax. 199
PO #/Billing Reference 97-/J2&,£
Project Name/ No.
6 0
(j) z C5 I I >
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CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
"Requested Due Date:
REMARKS
.-•···· ........ -~·-·· ... -..
SEE REVERSE SIDE FOR INSTRUCTIONS
-ttllli:l - --
ENVIRONMENTAL LABORATORIES
Client,[2 • C.6em/. toffJ~
Addres ·
Phone
Sampled By (P : err
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Additional Comments
2
-- -
Report To NIIL /(/off 2-
Bill lo Po l10 >C ?2'1 •
l!!!!!!!!J !!!!!S
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
PO.# I Billing Reference 9 7-/ 3 2, C:, 5"" Pace Project No.
0 w > a: w
(f) w
Project Name I No.
PRESERVATIVES
a: d ,., ~ (/} ~ c3
:::J I I >
' ..,0
• Requested Due Date:
REMARKS
. . ACCEPTED BY/ AFFILIATION .
. -., .
,·,_ ...... --.. --.' .
SEE REVERSE SIDE FOR INSTRUCTIONS
f~i•-~:J ----- -
ENVIRONMENTAL LABORATORIES
Report To /CeN' )(Jl M--
Bill To /!IJ. Box ?99 ,
ClientMfl~a/0 /5-fa/'1;£ t1:Cben11cal &~~7
Address '/8 rCeda.r ),Pt?tad7s ,f4a.d
Sa/4 '<:buL'>4 &C .:2vw P.O.# I Billing Reference 9 7-/3.20 £
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Phone 71?1/·dJ 1 ?-/ ZJJ £x-,2Q3
Sampled By (PRINT): -:}err ,-, 11.lc//
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Date Sampled tj. I/-9 .5"'
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4
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6
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7
Additional Comments
Project Name I No.
a: PRESERVATIVES w 1---~~~~-~-, z ~ z 0 0
Cl w > a: w
Cf) w a: a_ z ::,
0 Cf) i::
0 "' z 0 I >
X
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CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
·Requested Due Date:
REMARKS
2 SEE REVERSE SIDE FOR INSTRUCTIONS
· l.lli:l -
ENVIRONMENTAL LABORATORIES
ITEM
NO.,
-,·-:• -·~-:;y:-:·-" .. 4'. . ..
Additional Comments
2
Date Sampled
SAMPLE DESCRIPTION
")" ...... _ · .
. ... '1f.:::L:i~' ., '
--~~--'-107 /0 --
Report 1o Ke111 ;(k !/2
Bill To Pa Bo :t '399
-
PO.# I Billing Reference 97" /32(a£
en a:
Project Name I No.
PRESERVATIVES w >--~~~-~~-< z ~ ~ z > 0 a:
0 l½ u. w
0 a:
• TIME " MATRIX PACE NO. ci ~ z :::,
0 0 « <f/.. Z 0
I I >
l!!!!!!!I
CHAIN-OF-CUSTODY RECORD
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No.
•Requested Due Date:
REMARKS
Ill .. -:~• .... , . ,,, ;
. .... .1fc---Zr y. );
SEE REVERSE SIDE FOR INSTRUCTIONS
ta.ili;j -
ENVIRONMENTAL LABORATORIES
Sampled By (PRINT): Jerry ,t;J__, oN Y
L • .,.,.v, ~A'~d..'-'1 s
Date Sampled
Additional Comments
2
-------/0 of/0
._ l!!!!!!I!! l!!!!!I !!!!I ~ 1 ~6 P
CHAIN-OF-CUSTODY RECORD
Analytical Request
Report To N'.Al dJu.H2
BillTa /20. Box. '392
Pace Client No.
Pace Project Manager
PO #/Billing Referenc~ 97-/.LJ ,t:J £ Pace Project No.
V) a:
Project Name I No.
PRESERVATIVES
w t--r---0--,--,-,-7 z ~ ~ z > . 0 a:
0 lli w 8:0oc2: z CJ) z O
:J I I >
•Requested Due Date:
REMARKS
• ACCEPTED BY I AFFILIATION
·. . , . -.¥ •,-
SEE REVERSE SIDE FOR INSTRUCTIONS