NCD991278953_19940201_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Fourth Quarter 1993 OU-1 & OU-2-OCR

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Quarterly Report
Fourth Quarter 1993
Operable Units One and Two
i~.P 'r\l!"E .
: J,, FE3 2 8 1994 r:,. c::nil,l!J·.-.......,..,--1 J Li~~-'--..
1::0 .". -· HEGION n'
RECE1v · ,,
MAR O 3 19S4
SUPERFUND SECflCi,,
National Starch and Chemical Company Site
Ce.par Springs Road
Salisbury, North Carolina
Prepared by:
IT Corporation
312 Directors Drive
Knoxville, Tennessee
February 1994
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Quarterly Report
Fourth Quarter 1993
Operable Unit:s One and Two
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, N1:>rth Carolina
Prepared by:
IT Corporation
312 Directors Drive
Knoxville, Tennessee
February 1994
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Table of Contents'-----------------
Groundwater Monitoring Activities for the Fourth Quarter 1993 . . . . . . . . . . . . . . . . . . . I
Activities Planned for the First Quarter 1994 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Appendix A -Certificates of Analysis
KNn 339.M'Pl 339.TXT/02-17-94/DO 8:58am
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List of Tables, _________________ _
Table Title
I Sample Analysis and Water Level Monitoring Summary, Fourth Quarter 1993,
Operable Units One and Two
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in Groundwater,
Fourth Quarter 1993, Operable Unit One
3 ROD (OU!) Contaminants and Selected Water Quality Parameters in Groundwater,
Fourth Quarter 1993, Operable Unit Two
4 Groundwater Cleanup Criteria, Operable Unit One
5 Water Level Measurements, Fourth Quarter I 993, Operable Unit One
6 Water Level Measurements, Fourth Quarter 1993, Operable Unit Two
List of Figures. _________________ _
Figure Title
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2
Site Map
Summary of Acetone Data from OU I Monitoring and Extraction Wells
3 Summary of 1,2-Dichloroethane Data from OU! Monitoring and Extraction Wells
4
5
Summary of 1,2-Dichloropropane Data from OU! Monitoring and Extr.iction Wells
Summary of Methylene Chloride Data from OU! Monitoring and Extraction Wells
6 Summary of Bis(2-chloroethyl)ether Data from OU I Monitoring and Extraction Wells
7 Water Level Contour Map for Bedrock Water Levels, October 11, 1993
KN/1339/WPl 339.TXTft:>2-17-94/DO 8:5&..m II
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Groundwater Monitoring Activities for the Fourth Quarter
1993, ____________________ _
This report for the fourth quarter 1993 presents findings from groundwater monitoring
conducted at Operable Units One and Two at the National Starch and Chemical Company site
on Cedar Springs Road, Salisbury, North Carolina.
Operable Unit One. Groundwater samples from four downgradient groundwater
monitoring wells (NS29, NS30, NS31, and NS32) and four bedrock extraction wells (EX0l,
EX02, EX03, and EX04) were collected on October 11, 1993. All samples were analyzed for
selected Target Compound List (TCL), volatile and semivolatile organic compounds (VOC
and SVOC), and Target Analyte List (T AL) metals. In addition, samples from the monitoring
wells and extraction wells were analyzed for selected water quality parameters to monitor
influent loadings for the Combined Pretreatment System (CPS). A sample analysis summary
is provided in Table 1. The samples were collected in accordance with U.S. Environmental
Protection Agency (EPA) (Region IV) protocols. The TCL and TAL compounds were
analyzed under EPA Level IV Contract Laboratory Program (CLP) protocol.
All plume periphery extraction wells were in operation during sampling. All extraction wells
were shut down in late November through late December due to construction of the CPS and
removal of sludge from the pretreatment lagoons. Wells EX02 and EX03 were started the
last week in December. Trench area extraction wells EX05 through EXl0 went through
startup and shakedown operations.
Results from the chemical analysis for Operable Unit One and Operable Unit Two are
presented in Tables 2 and 3, respectively. The list of compounds presented in these tables
represents the contaminants specified in the Operable Unit One Record of Decision (ROD).
The list of compounds from the ROD and associated cleanup levels are provided in Table 4
for reference. Figure 1 is a site map showing the well locations. The certificates of analysis
are provided in Appendix A.
For the downgradient monitoring wells, two VOCs and one SVOC exhibited levels that
exceed cleanup levels (shaded values in Table 2). Chemical data from samples collected
during the 1992 event and the first, second, third, and fourth quarters 1993 indicate that the
contaminant concentrations in wells NS29, NS30, and NS31 have generally decreased over
time and that no contaminants are present in well NS32. Figures 2 through 6 present
KN/l 339/WP1339.TXT/02-17-94/DO 8:49am 1
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summaries of data (in bar-chart form) from all four quarters of 1993 (and the 1992 event) for
the five organic compounds that have exceeded cleanup criteria. These five organic
compounds are acetone, 1,2-dichloroethane, 1,2-dichloropropane, methylene chloride, and
bis(2-chloroethyl)ether. Methylene chloride was not reponed from the laboratory. Data from
monitoring well NS32 is not presented graphically (in bar-chart form) since contamination has
not been found in any samples. Acetone, which usually leads the contaminant front, was
present at significant levels during the second and third quarters 1993 in operating extraction
wells EX02 and EX03. High levels of acetone were also present during the 1992 and fust
quarter 1993 events in three of the four downgradient monitoring wells; however, acetone
levels dropped significant! y during the second and third quarters and was not detected during
the founh quarter. This drop in acetone levels in the monitoring wells indicates that pumping
is controlling the spread of acetone. 1,2-Dichloroethane and 1,2-dichloropropane were present
in well NS31 at 20 parts per billion (ppb) and 31 ppb, respectively. Bis(2-chloroethyl)ether
was present at wells NS29, NS30, and NS31 with the highest level at 25 ppb. The levels of
these three contaminants have generally decreased over time. Levels of 1,2-dichloroethane
have consistently been elevated at extraction well EX02, ranging from 27,000 ppb to 34,000
ppb during the past three quarters.
Water level measurements were taken (October 11, 1993) from the four downgradient
monitoring wells, several other selected monitoring wells, and the four extraction wells.
NS32 water level was not measured due to artesian conditions. Results of the water level
measurements are provided in Table 5. Groundwater elevations and a bedrock groundwater
contour map are provided in Figure 7.
Hydraulic control of the contaminant plume is difficult to ascenain at this time due to the
extraction wells not being in full operation. The efficiency of plume control and hydraulic
control can be evaluated in more detail after all extraction wells are operating. Well NS32
has been artesian during all monitoring events.
Operable Unit Two. Groundwater samples were collected from monitoring wells NS09,
NSIO, NS!!, and NS15 on October II, 1993. All samples were analyzed for selected TCL
VOCs and SVOCs, and TAL metals. In addition, the samples were analyzed for selected
water quality parameters to provide design information and project start-up flow rates for the
CPS. A sample analysis summary is provided in Table 1. The samples were collected in
accordance with EPA (Region IV) protocol. The TCL and TAL compounds were analyzed
under EPA Level IV CLP protocol.
KN/1339/WP1339.TXT/02-17-94/00 8:49am 2
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Results from the chemical analysis for Operable Unit Two are presented in Table 3. The list
of compounds presented in Table 3 represent the contaminants specified in the Operable Unit
One ROD. The list of compounds from the ROD and associated cleanup levels are provided
in Table 4 for reference. Figure 1 is a site map showing the well locations. The certificates
of analysis are provided in Appendix A.
Three VOCs and three metals exhibited levels that exceed cleanup levels (shaded values in
Table 3). Elevated levels of 1,2-dichloroethane were detected in three of the four wells
ranging from 530 ppb to 4,700 ppb. These results are very similar to results from the
previous quarter except that 1,2-dichloroethane was not detected in well NS 11. Vinyl
chloride was detected at 75 ppb (estimated) and xylenes at 560 ppb in wells NS09 and NS 11,
respectively. Levels of barium, chromium, and manganese exceeded cleanup levels for the
third consecutive quarter but were within one order of magnitude.
Water level measurements were taken (October 11, 1993) from each of the four monitoring
wells. Results are provided in Table 6. Groundwater elevations and a bedrock groundwater
contour map, constructed primarily from Operable Unit One wells, are provided in Figure 7.
KN/1339/WP 1339.TXT/02-17-94/DO 1 :39pm 3
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Activities Planned for the First Quarter 1994 _____ _
Operable Unit One. Groundwater monitoring will continue. Operation of extraction wells
EX-02 and EX-03 will continue. When the CPS construction is complete all extraction wells
will become operational.
Operable Unit Two. Groundwater monitoring will continue.
KN/1339/WP 1339.TXT/02-17-94/DO 8:51am 4
-------------------
Well
Well Number Type8
Operable Unit One
EX01 BE
EX02 BE
EX03 BE
EX04 BE
NS05 SM
NS06 SM
NS21 BM
NS22 BM
NS23 SM
NS26 BM
NS27 BM
NS28 BM
NS29 BM
NS30 BM
KN/1339/WP1 339.T 1 /02-17-94/F 1
Table 1
Sample Analysis and Water Level Monitoring Summary
Fourth Quarter 1993
TCL
Operable Units One and Two
National Starch and Chemical Company
Salisbury, North Carolina
(Page 1 of 2)
TCL TAL
vocsb svocsb Metals TDSC Chloride cood
X X X X X X
X X X X X X
X X X X X X
X X X X X X
X X X X X
X X X X X
Water
TKN8 Level
X X
X X
X X
X X
X
X
X
X
X
X
X
X
X
X
-------------------
Well
Well Number Type•
Operable Unit One (Continued)
NS31 BM
NS32 BM
P01 BM
Stream Gage No.1 1 NA9
Stream Gage No. 2 NA
Operable Unit Two
NS09 SM
NS10 SM
NS11 SM
NS15 BM
"BE -Bedrock extraction well
BM -Bedrock monitoring well
TCL TCL
vocsb svocsb
X X
X X
NA NA
NA NA
X X
X X
X X
X X
Table 1
(Page 2 of 2)
TAL
Metals TDS0
X X
X X
NA NA
NA NA
X X
X X
X X
X X
Water
Chloride cood TKN8 Level
X X
X X
X
NA NA NA X
NA NA NA X
X
X X
X X
X X
X X
SM -Saprolite (shallow) monitoring well
bProject TCL list consisting of 13 VOCs and 2 SVOCs, which matches the Operable Unit One cleanup criteria (Table 4).
Methylene
chloride was not reported.
0TDS -Total dissolved solids
dcoo -Chemical oxygen demand
8TKN -Total Kjeldahl nitrogen 1Iron pins in southwest tributary for monitoring stream elevations 9NA -not applicable
KN/1339/WP1 339.T 1 /02-17 ·94/F 1
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Well Number
Sample Date
Volatile Organics (ppb)8
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-Dichloroethane
1, 1-Dichloroethylene
1,2-Dichloropropane
Ethyl benzene
Toluene
1, 1,2-Trichloroethane
Trichloroethylene
Vinyl chloride
Xylenes (total)
Semlvolatlle Organics (ppb)
bis(2-Chloroethyl)ether
4-Nrtrophenol
KN/1339/WP1339.T2/02-16·94/00 3:32pm
Table 2
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Fourth Quarter 1993
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
(Page 1 of 4)
EX01 EX02 EX03
October 1993 October 1993 October 1993
10 Ub 27,000 1200
10 U 3300 U 170U
10 U 3300 U 170U
10 U 3300 U 170 U
10 U 3300 U 55 J
10 U 3300 U 170 U
10 U 3300 U 170 U
10 U 3300 U 170U
10 U 3300 U 66 J
10 U 3300 U 170U
10 U 3300 U 170U
10 U 3300 U 170 U
10 U 3300 U 170 U
11 U 440 74
27 U 260 U 52 U
EX04
October 1993
27
10 U
~o u
10 U
10 U
10 U
10 U
10 U
3J
10 U
10 U
10 U
10 U
53 U
130 U
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1•
Well Number
Sample Date
lnorganlcs (ppb)
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
Water Quality (ppm)0
TDS
Chloride
COD
TKN
KN/1339/WP 1339.T2/02-16-94/DO 3:32pm
Table 2
(Page 2 of 4)
EX01 EX02
October 1993 October 1993
2.4 U 4.8 U
22.8 B 1490
0.40 U 0.40 U
2.3 U 2.3 U
2.7 U 2.7 U
24.3 10800
11.8 B 13.8 B
2.3 U 4.6 U
9.7 B 56.5
170 3000
5.4 730
10 1000
NDd 4.0
EX03 EX04
October 1993 October 1993
4.8 U 2.4 U
278 36.3 B
0.40 U 0.40 U
2.3 U 2.3 U
2.8 B 2.7 U
11,200 5090
8.4 U 8.4U
4.6 U 2.3 U
2.5 B 1.8 U
1700 680
420 140
190 90
1.6 1.8
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Well Number
Sample Date
Volatile Organics (ppb)
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-Dichloroethane
1, 1-Dichloroethylene
1,2-Dichloropropane
Ethyl benzene
Toluene
1, 1,2-Trichloroethane
Trichloroethylene
Vinyl chloride
Xylenes (total)
Semlvolatlle Organics (ppb)
bis(2-Chloroethyl)ether
4-Nitrophenol
lnorganlcs (ppb)
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
KN/1339/WP1339.T2/02-16·94/00 3:32pm
Table 2
(Page 3 of 4)
NS29 NS30
October 1993 October 1993
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
3J 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
••I·••·•••••r••••····••·••••i•s····· ...................... •.····
.· .. •
·.•·· IU.v,c
26 U 27 U
2.4 U 2.4 U
61.7 B 29.8 B
0.40 U 0.40 U
2.3 U 2.3 U
2.7 U 2.7 U
177 2110
8.4 U 8.4 U
2.3 U 2.3 U
2.6 B 2.2 B
NS31 NS32
October 1993 October 1993
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
~ ••• 10 U
10 U 10 U -10 U
10 U 10 U
6J 10 U
10 U 10 U
10 U 10 U
10 U 10 U
10 U 10 U
)~ 11 U
26 U 26 U
2.9 B 2.4 B
15.6 B 85.6 B
0.40 U 0.40 U
2.3 U 2.3 U
2.7 U 2.7 U
21.4 99.8
8.4 U 8.4 U
2.3 U 2.3 U
2.6 B 1.8 U
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Well Number
Sample Date
Water Quality (ppm)
TDS
Chloride
NS29
Table 2
(Page 4 of 4)
NS30
October 1993 October 1993
410 510
59 78
8 ppb -parts per billion.
boualifiers: B (organics) • Compound was detected in the associated blank.
NS31 NS32
October 1 993 October 1993
51 220
610 9.6
B (inorganics) • Compound concentration is between the instrument detection limit and the contract-
required detection limit.
J • Compound concentration is an estimate. Either the compound was positively identified at a trace
value, or it is a nontarget for which no calibration was pertormed.
U • Compound was analyzed for but not detected at the listed concentration.
}.'Pm -parts per million.
ND -Not detected at or above the method detection limit.
KN/13391WP1339.T2/02-16-94/00 9:38am
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Well Number
Sample Date
Table 3
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Fourth Quarter 1993
Operable Unit Two
National Starch and Chemical Company,
Salisbury, North Carolina
(Page 1 of 2)
NS09 NS10 NS11
October 1993 October 1993 October 1993
Volatile Organics (ppb)"
Acetone 720 330 Ub 130
Benzene 250 U 330 U 25 U
Bromodichloromethane 250 U 330 U 25 U
Chloroform 250 U 330 U 25 U
1,2-Dichloroethane I ?J,, .•• 25 U
1, 1-Dichloroethylene 250 U 330 U 25 U
1,2-Dichloropropane 250 U 330 U 25 U
Ethyl benzene 250 U 330 U 300
Toluene 330 330 U 120
1, 1,2-Trichloroethane 250 U 330 U 25 U
Trichloroethylene 250 U 330 U 25 U
:-:."-_":::-:-:.-:·,·:·
Vinyl chloride 75·1,<i• 330 U 25 U
Xylenes (total) 250 U 330 U = • Semlvolatlle Organics (ppb)
bis(2-Chloroethyl)ether 530 U 50 U 10 U
4-Nitrophenol 1300 U 120 U 26 U
lnorganlcs (ppb)
Arsenic 8.2 B 2.4 U 2.4 U
Barium 1):(\:/; n?li :I·:.:.' ,: : :: 155 B 85.9 B •.• ··.•.•.·
Beryllium 0.75 B 0.40 U 0.40 U
Cadmium 2.3 U 2.3 U 2.3 U
Chromium .... _,_21.-•••tx•·••·•·•· 16.3 17.4
Manganese ii ?a!io&•••·••··••·• .. 3540 55.6
KN/1339/WP1339.T3/02·16·94!00 3:40pm
NS15
October 1993
67 U
67 U
67 U
67 U
II!
67 U
67 U
67 U
18 J
67 U
67 U
67 U
67 U
42 U
110 U
4.8 U
444
0.40 U
2.3 U
3.6 B
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Well Number NS09
Table 3
(Page 2 of 2)
NS10 NS11 NS15
Sample Date October 1993 October 1993 October 1993 October 1993
Nickel 54.0 33.9 B 35.1 10.3 B
Selenium 6.9 U 2.3 U 2.3 U 4.6 U
Zinc 75.6 43.2 15.0 B 1.8 U
Water Quality (ppm)°
TDS 5100 820 400 3200
Chloride 1600 300 9.2 910
COD NAd NA NA NA
TKN NA NA NA NA
8ppb • parts per billion
boualifiers: B (organics) = Compound was detected in the associated blank.
B (inorganics) = Compound concentration is between the instrument detection limit and the
contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively identrtied
at a trace value, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
l'pm • parts per million
NA • not analyzed
KN/1339JWP 1339.T~02-16-94/00 9:39am
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Table 4
Groundwater Cleanup Criteria
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
I Compound I Cleanup Concentration (ppb)"
Volatile Organics
Acetone 3,500
Benzene 5
Bromodichloromethane 5
Chloroform 5
1,2-dichloroethane 5
1, 1-dichloroethylene 7
1,2-dichloropropane 6
Ethyl benzene 3,500
Methylene chloride 5
Toluene 2,000
1, 1 ,2-trichloroethane 5
Trichloroethylene 5
Vinyl chloride 2
Xylenes 350
Semlvolatlle Organics
Bis(2-chloroethyl)ether 5
4-Nitrophenol 350
lnorganlcs
Arsenic 10
Barium 1,000
Beryllium 17.5
Cadmium 10
Chromium 50
Manganese 7,700
Nickel 350
Selenium 10
Zinc 7,350
"ppb = parts per billion.
I
Reference source: U.S. Environmental Protection Agency, Enforcement Record of Decision, Remedial
Alternative Selection for Operable Untt One, National Starch and Chemical Corporation Stte, prepared
for U.S. EPA Region IV, Atlanta, Georgia (9-30-88), p. 19.
KN/1339/WP1339.T 4102-17-94l00
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Well
EX01
EX02
EX03
EX04
NS05
NS06
NS21
NS22
NS23
NS26
NS27
NS28
NS29
NS30
NS31
NS32
P01
Stream Gage 1
Stream Gage 2
Table 5
Water Level Measurements
Fourth Quarter 1993
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (ft msl)3 (ft msl)
10/11/93 TOCb 731.85 42.0
10/11/93 TOC 718.24 3.0
10/11/93 TOC 740.46 27.7
10/11/93 TOC 754.12 40.4
10/11/93 TOC 767.96 23.5
10/11/93 TOC 738.87 13.75
10/11/93 TOC 739.13 8.17
10/11/93 TOC 715.94 NAC
10/11/93 TOC 752.36 23.58
10/11/93 TOC 720.77 18.0
10/11/93 TOC 749.47 28.58
10/11/93 TOC 767.82 22.17
10/11/93 TOC 715.50 46.7
10/11/93 TOC 718.54 54.3
10/11/93 TOC 711.15 9.54
10/11/93 TOC 699.48 NAd
10/11/93 TOC 708.09 8.25
10/11/93 Iron pin" 712.26 NA1
10/11/93 Iron pin 693.90 2.02
Water Level
Elevation
(ft msl)
689.85
715.24
712.76
713.72
744.46
725.12
730.96
NAC
728.78
702.77
720.89
745.65
668.80
664.24
701.61
NAd
699.84
NA1
691.88
a ft msl -Feet, mean sea level, National Starch and Chemical Company plant vertical datum elevation
777. 79 feet msl.
b TOC -Measurement taken from top of inner well casing.
C NA -Not applicable' well is dry.
d NA -Not applicable, well is artesian.
0 NA -Measurement taken from top of iron pin next to stream.
NA -Not applicable, no water present.
KN/1339/WP1339.T5102-17-94/01
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Well
NS09
NS10
NS11
NS15
Table 6
Water Level Measurements
Fourth Quarter 1993
Operable Unit Two
National Starch and Chemical Company,
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (ft MSL)8 (ft)
10/11/93 TOCb 778.45 29.29
10/11/93 TOG 786.72 32.71
10/11/93 TOG 775.65 20.5
10/11/93 TOG 792.60 43.81
Water Level
Elevation
(ft MSL)
749.16
754.01
755.15
748.79
a MSL -Mean sea level, National Starch and Chemical Company plant vertical datum
elevation 777. 79 feet msl.
b TOG -Measurement taken from top of inner well casing.
KN/13391WP1339.T6/02•17•94/01
Q)
C
0 -Q)
(.)
<( -0
C
0
~ ~ -C
Q)
(.)
C 0 (.)
12,000 -
8,000 1-· · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · · • • · · · · · ·······I: 1: ,,I . ,, r ;
6,000 -·· ................................................... '
.
I:
4,000 -··· · ....................... .
3,500 t---.. f--------
(See note 1)
··· ··· ··· ·· .... ·· ....... ·, 11
2,000 t--. < i .•.••......
, X
0 1 2 3 4 1 2 3 -'
,I
1 2 J 4 1 2 3 4 1 ' ' NS29 NS30 NS31 EX01 EX02
Well Number
(See note 4)
. ..... ' ................. .
'
1234 1234
EX03 EX04
§I 1992
II 1st Quarter 1993
~ 2nd Quarter 1993
!f'.! 3rd Quarter 1 993
~ 4th Quarter 1993
NOTES:
1. Clean up level.
2. EX01, EX02, EX03, and EX04 samples were not
analyzed for acetone during the 1992 event.
3. EX02 was not sampled during the first quarter 1993.
4. Second, third, and fourth quaner levels are 29,000 ppb
34,000 ppb, and 27,000 ppb, respectively, for EX02.
[i] INTERNATIONAL
TECHNOLOGY
CORPORATION'
Figure 2. Summary of Acetone Data from OU1 Monitoring and Extraction Wells
National Starch and Chemical Company, Salisbury, North Carolina
-----·--------------
600
500
W 1992
■• 1st Quarter 1993
~ 2nd Quarter 1993
3rd Quarter 1993
~ 4th Quarter 1993
~ ~ ···························································· ································
ct! .r:: .... Q) e
0
.r:: u 300 .................................................. · ·······························
0
' (\J
,-..... 0
C
0 ~ .... .... C
Q) u
C
0 (.)
200
100
1 2 3 4
NS29 NS30 NS31 EX01
Well Number
1 2 3 4 1 2 3 4
EX02 EX03
1 2 3 4
EX04
NOTES:
1. Clean up level.
2. EX02 was not sampled during the first quarter 1993.
[D INTERNATIONAL
TECHNOLOGY CORPORATION ~-------------------------------------------------'
Figure 3. Summary of 1,2-Dichloroethane Data from OU1 Monitoring and Extraction Wells
National Starch and Chemical Company, Salisbury, North Carolina
f I
- - ---· - --- -l8 ----· ----
QJ
C
Cll
0.. 0 .....
0.. e 0
.c -~ 0
' C\J .... ..... 0
C 0
~ ...... C
QJ
()
C
0
(.)
1,000
800 ~ ------------------------------------------------------------l
'
600 -···························································· \: ·····························•···
400 -···························································: ·································
-11
~ :~ ;
' c ' .......................... ~ .................... :· . '
' ~ ~ ~ :: .~ ·, '
200 >--···
~ ~ . -~ I ;
(See ~o~l:=1:-:::lf;!l l:jJ~~=::eii;II:" ·!J;:j~=til::l::~il!;lli••:f;:· ,:l::::Blffll!:11,: ":k::;:::=±11:;:!;!l!;::J=::lr::i-. !;iliil;!J!~=±""':i;:::;!:;;::';:::=:::l 0 1234 1234 1234 1234 1234 1234 1234
NS29 NS30 NS31 EX01 EX02 EX03 EX04
Well Number
m 1992
ii 1st Quarter 1993
~ 2nd Quarter 1993
3rd Quarter 1993
~ 4th Quarter 1993
NOTES,
1. Clean up level.
2. EX02 was not sampled during the first quarter 1993.
[i] INTERNATIONAL
TECHNOLOGY
CORPORATION
Figure 4. Summary of 1,2-Dichloropropane Data from OU1 Monitoring and Extraction Wells
National Starch and Chemical Company, Salisbury, North Carolina
----~--------------
:c D..
D.. ~
Q)
-0 ·c
0
.c
0
Q)
C
Q)
>, .c -Q)
::i: -0
C
0 ~ ~ -C Q) u C 0
0
100
80
60
40 .................. ·······································•·············· ..................... .
20
Well Number
~c 1992
■ 1st Quarter 1993
~ 2nd Quarter 1993
3rd Quarter 1993
NOTES:
1. Clean up level.
2. EX02 was not sampled during the first quarter 1993.
3. Methylene chloride not analyzed for fourth quarter 1993.
ID INTERNATIONAL
TECHNOLOGY
CORPORATION
Figure 5. Summary of Methylene Chloride Data from OU1 Monitoring and Extraction Wells
National Starch and Chemical Company, Salisbury, North Carolina
-------------------
~ .c
0.. 0..
~ ....
(I) .c .....
(I)
~
>, .c ..... (I)
0 ....
0
.c
(.)
' C\J ~ en
co .....
0
C 0 :;::,
Cl! .... ..... C
(I)
(.)
C
0
(.)
600 ,--------------------------,
500
400
300
200
100
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
························································ ..
,
,
/ / / : ...................•.....•..•• / /
/
/ / ;
/ '. j :,· / . / .;, j
·: /
\ j ·················•··•········· :, /
ff :
( j
.-;
/
/
/ ~
1 2 3 4
NS29 NS30 NS31 EX01 EX02 EX03 EX04
Well Number
m 1992
■ 1st Quarter 1993
~ 2nd Quarter 1993
3rd Quarter 1993
~ 4th Quarter 1993
NOTES:
1. Clean up level.
2. EX02 was not sampled during the first quarter 1993.
rn INTERNATIONAL
TECHNOLOGY
CORPORATION f .__ ______________________________________________ ___.]
Figure 6. Summary of Bis(2-chloroethyl)ether Data from OU1 Monitoring and Extraction Wells
National Starch and Chemical Company, Salisbury, North Carolina
--- ------
300 0 300
"f!!!...ll.i.'Thvl.:.i.ii!_ I
150
GRAPH
---
600
450
-
,0
' ' rlsoJ
r21 l 0· ' ' ' '¾-
-
,
' ' ' ' ' '
, , ,
, , ,
o
-- ---
LEGEND
® EX!STING PIEZOMETER
~ EXISTING BEDROCK MONITORING V,'ELL
[ill] EXISTING BEDROCK EXTRACTlmJ WELL
~ EXISTING SAPROLITE CSHAL.LOW)
MONITORING WELL
~ PROPOSED EXTRACTION WELLS
-750-GROUNDWATER SURFACE ELEVATION
(MSU ANO CONTOUR (DASHED WHERE INFERRED)
NOTES:
WATER LEVEL FOR NSJ2 WAS NOT MEASURED DUE
TO ARTESIAN CO/~DITIONS.
2. WATER LEVEL FOR /JS22
WAS NOT MEASURED DUE
TO THE WELL BEING DRY.
3.WATER LEVEL FOR STREAM
GAGE •1 WAS i~OT MEASURED
DUE TO STREAM BEli'JG DRY.
4.GROUNDWATER COMTOURS ARE NOT
PRESD!TED DOWNGRADIE/H OF
ELEVATION 710; ONLY WATER LEVELS
AT THE WELLS ARE SHOWN.
OPERABLE UNITS ONE AND TWO FIGURE 7
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I Appendix A
I Certificates of Analysis
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I KNfl 339/WP1339.TXT/02-l7-94/DO 8:58am
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300 600
/
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m INTERNATIONAL
TECHNOLOGY
CORPORATION
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\~_... -.. ..
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[]
LEGEND
ifo\\p '8 EXISTING PIEZOMETER
EXISTING BEDROCI< MO,,JITORING WELL
EXISTING BEDROCK EXTR.l\CTION WELL
l@I EXISTING SAPROLITE (SHALLOW)
MONITORING WELL
C§J PROPOSED EXTRACTION WELLS
-750-GROUNDWATER SURFACE ELEVATION
(MSU AND CONTOUR <DASHED
WHERE INFERRED)
t::JOTES:
1. WAH:R LEVEL FOR NS32
~AS NOT MEASURED DUE
TO A.RTESIAN COIJDITIO"IS.
2.WATER LEVEL FOR NS22
WAS NOT MEASURED DUE
TO THE WELL BEl"IG DRY.
3. WATER LEVEL FOR STREJ,M
GAGE •1 W.l\S "JOT MEASURED
DUE TO STREAI-~ BEll•JG DRY.
4.GROUf,JDW.l\TER COeJTOURS 1\RE l~OT
PRESENTED DOWl,JGRADlan OF
ELEVATION 710; ONLY WATER LEVELS
AT THE WELLS ARE SHOWN .
NATIONAL ST ARCH 8c CHEM
SALISBURY, NC
co ST ART DATE• 09/22/93
DRAWN:
P.O. TERRY
K/IOX'.'ILI.E. TErl/!ESSEE FIGURE 7
ll!!S ORA'IIICIG SJ,0 '-CL INFORMATIO/i WATER LEVEL CONTOUR M At>
CHECKED:
Tll!::fffOrJ IS CO,'lFIOGllV'1_ t..i'JD l,1UST ,.....
.. 10r BE i,1.t..DE Puauc OR coP1rn UNLESS FOR BEDROCK WATER LEVELS APPROVED=
DULY ,,U1'iORIZf:D, SHfJ.l. NOT BE USED
150 450 D'.CEPT FOR THE PURPOSE FOR WHICH '-.,,====="O"'C"--'T..;O;.;B:;.::;E"-R"'-__ 19 ___ 9_3 ______ DRAWl'JG NO· IT VIAS SUPPLIED, A/JO IS SUBJECT TO ~ ' . R!::TURrJ UPOi·l DEl,tA'lD. ALL RIGHTS OF REVISION DESCRIPTION F
~:i... ___________________________ ... G:.1.R,...A..:./...P.l.H .. I_.C"--"'s~c ... A.ll.L ... E..,:___.l_"_= ... 3 ... 0 .. 0 ... ' __ ...... ,;;."';.;;-'E;;.rlT;;.IO;;.N_o;;.R..;D;;.E_s,o;;.N_AR..;.;.E;;.R.;;.;ES;,;;E;;.RV;,;;E;;.D._,.___.....,.;;.o;..PaaEa.aR""'AB"'L"'E....;U;;;.N""IT"-S"'-O_N_E_AN __ D __ T;..W;..,;;.O_ ..... ____ ,_G_U_R_E __ 7 __ __
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CLIENT
CASE
SDG
LAB NO.
ISSUED
SUMMARY SAMPLE DATA PACKAGE
NATIONAL STARCH & CHEMICAL CO.
PCHAR
NASOl
37965 37995 38016
NOVEMBER 20 1993
PACE New England, Inc.
Hampton, New Hampshire
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!Hf ASSUfiA'iCf OF OUALIII
November 20, 1993
National Starch & Chemical Company
c/o PACE Charlotte
485 Cedar Spring Road
Salisbury, NC 28144
Case: PCHAR
SDG: NASOl
SAMPLE DELIVERY GROUP NARRATIVE
Laboratory: PACE New England, Inc. of Hampton, NH
Lab Numbers: 37965/37995/38016
Analytical Protocol: OLMOl.8/ILMOl.2 with modified target lists. Format A disk.
Sample Receipt: Samples for this SDG were received at PACE Charlotte Laboratory
from October 13-15, 1993. They were forwarded by overnight carrier to PACE New
England for analysis. Laboratory sample numbers were assigned ae listed on the
sample table which follows this narrative. Field sample identifiers were abbreviated
to accommodate CLP software requirements. Although temperature blanks were not
included with the shipments, samples were received cool and in good condition.
Bottles and labels matched the Chains-of-Custody (COC) provided, with exceptions
noted as follows:
The samples received at PACE New England on 10/14/93 were assigned PACE lab# 37965.
The coc listed four samples for metals analysis (EXOl, EX02, EX03, and EX04) which
were missing from this shipment. The project manager at PACE Charlotte was notified
of this omission and the samples were included in the shipment received on 10/16/93.
The second group of samples was received at PACE New England on 10/15/93 and was
assigned PACE lab# 37995. This shipment had no discrepenciee.
The final group of samples was received at PACE New England on 10/16/93 and was
assigned PACE lab# 38016. This shipment included the four samples for metals
analysis which were not included in the 10/14/93 shipment. These samples were not
listed on the chain of custody for this shipment. In addition, the samples listed
on the ·chain of custody as NS-31B for metals, volatile organics, and semivolatile
organics were a duplicate of sample NS-31 and were meant to provide adequate volume
for quality control analyses for this SDG. Thie change was made at the request of
the project manager at PACE Charlotte after consultation with her client. Any
references on raw data to samples 38016-2, -10, or -16 refer to the extra sample
provided for NS-31.
Volatile Analysis I Samples were analyzed within holding time by the CLP water
method. The project target compound list consisted of thirteen CLP compounds with
no nontarget search requirement. Standards and tunes met all calibration criteria.
Blanke were free of target compound contamination. Matrix spikes performed on sample
NS31 exhibited acceptable spike recoveries and analytical precision. Internal
standard areas and surrogate recoveries were acceptable for all analyses.
Samples EX02, EX03, NSlO, NSll, NS15, and NS9 required dilutions in order to
quantitate high levels of target compounds.
The reporting software caused the Form 1 sample data sheets to contain an extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
tenth of a milliliter.
P.O. Box 2130
1 Lalayette Road
Hampton. flH 03842
TEL: [phone]
800-992-0714
FAX: [phone]
1
An Equal Qpportuni!y Em°ii;llyer
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TH! ASSUAANCE Of OUAlllY
SDG Narrative
Case PCHAR SDG NASOl
Semivolatile Analysis: The majority of samples were extracted within CLP holding
time (5days from receipt) by the water method. Samples of lab number 37965 (EXOl,
EX02, EX03, EX04) were extracted on the sixth day from receipt. Since this was on
the seventh day from sampling (SW846 holding time), the data quality remained
acceptable. This was discussed between the PACE New England and PACE Charlotte
Organics Managers. Analyses proceeded within holding time.
Standards and DFTPP tunes met calibration requirements. The target compound list for
this project consisted of bis(2-Chloroethyl)ether and 4-Nitrophenol. These compounds
were not detected in the method blanks. Matrix spikes conducted on sample NS31 had
acceptable 4-Nitrophenol recoveries. Internal standard areas were acceptable for all
analyses. Surrogate recoveries were compliant although there were some outliers
(NSll had 2FP at 10%, and EX04 had TBP at 2% which was acceptable for the diluted
extract). Sample NS9 required dilution which caused the surrogates to go below
detectable limits.
Samples NS9, NS15, NSlO, and EX04 required dilutions for high levels of nontarget
compounds. Nontarget searches were not requested for this project.
The reporting software caused the Form 1 sample data sheets to contain an extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
milliliter.
Metals Analysis and Cyanide: The analytical protocol for metals analytes established
for this project is compliant with the ILMOl.2 except as noted below. Holding times
follow CLP rules and were calculated from verified time of sample receipt (VTSR).
In several cases, the shortened field IDs were prefixed with an "M." to accommodate
a six-character software requirement. Matrix quality control was performed on sample
MMNS31 for metals analyses.
ICP Analysis: Samples were prepared in one water batch on 10/20/93. Samples were
analyzed in two analytical sequences on the TJAOl. One sequence was performed on
11/08/93, the second on 11/09/93 for a manganese dilution only. samples were
analyzed for arsenic, and selenium in one sequence on 11/08/93 on the TJA02. Several
samples were diluted due to high levels of interferents, with no effect on the CRDL.
Spike recovery for sample MMNS31 met CLP QC limits. Cadmium is flagged as out of
control limits on Form 5, however, according to the CLP SOW 125.4% rounds to 125% and
therefore the recovery for cadmium is acceptable. Sample results are not flagged
with the "N" qualifier accordingly. A post digestion spike was not performed. The
percent recovery for the LCS for cadmium was 120.6%, this is with in the laboratory's
upper control limit established by in house control charts. No cadmium was observed
in any of the samples. Serial dilution analyses were performed on sample MMNS31 with
acceptable results.
Steven Rhode, Organics Manager
PACE, Incorporated
P 0. Bo~ 2\30
I Lafayette Road
Hamo1on. f.JH 03842
TEl [phone]
B00-992-0724
FAX: [phone]
2
Nn.H.-n,{-£,L .:c-11 '1 :;,
November 20, 1993
An Equal Opportunity Emp;~yer
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CLIENT ID.
REPORTED AS -------------------
EXOl-10/93
EXOl
EX02-10/93
EX02
EX03-10/93
EX03
EX04-10/93
EX04
92 010927.9
92 010927.9
92 010928.7
92 010928. 7
92 010929.5
92 010929.5
SAMPLE TABLE
MATRIX PACE# ----------------
WATER 37965-001
37965-005
WATER 37965-002
37965-006
WATER 37965-003
37965-007
WATER 37965-004
37965-008
WATER 37965-009
WATER 37965-010
WATER 37965-011
PARAMETERS ----------
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
As, Se
As, Se
As, Se
~,q~~-
'"' IIUIUCI II lu111t,
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SAMPLE TABLE
CLIENT ID.
REPORTED AS MATRIX PACE# -----------------------------------
NS-15
NS-30
NS-29
NS15 WATER 37995-001
NS30 WATER
NS29 WATER
37995-004
37995-007
37995-002
37995-005
37995-008
37995-003
37995-006
37995-009
(:-.i,
PARAMETERS
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
GC/MS VOA
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
~,q~~-
, •• UIIIUII If, .. ,.,,
I SAMPLE TABLE
I CLIENT ID,
REPORTED AS MATRIX PACE# PARAMETERS
I ---------------------------------------------
NS-31
NS31 WATER 38016-001 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
I *SQC* 38016-009 ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
38016-015 GC/MS VOA
I NS-10
NSlO WATER 38016-003 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
I 38016-011 ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
38016-017 GC/MS VOA
I NS-11
NSll WATER 38016-004 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
38016-012 ACID EXTRACTABLES
I BASE/NEUTRAL EXTRACTABLES
38016-018 GC/MS VOA
I NS-32
NS32 WATER 38016-005 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
38016-013 ACID EXTRACTABLES
I BASE/NEUTRAL EXTRACTABLES
38016-019 GC/MS VOA
NS-9
I NS9 WATER 38016-006 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
38016-014 ACID EXTRACTABLES
I
BASE/NEUTRAL EXTRACTABLES
38016-020 GC/MS VOA
EX-02
I EX02 WATER 38016-007 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
EX-03
I EX03 WATER 38016-008 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
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"l •11••••<1 II IO&tlll
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CLIENT ID,
REPORTED AS -------------------
TRIP BLANK
TRIP BLANK
EX-01
EXOl
EX-04
EX04
SAMPLE TABLE
(CONTINUED)
MATRIX PACE # ----------------
WATER 38016-021
WATER 38016-022
WATER 38016-023
C.-4
PARAMETERS
----------
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
Ba, Be, Cd, Cr, Mn, Ni, Zn,
AB, Se
~,q~,.
'"' &I ..... , ... """"
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: PACE NEW ENG LA
EXOl
Contract:
.Lab code: case No.: PCHAR
Matrix: (soil/water) WATER
SAS No.: SDG No.: NASOl
Lab Sample ID: 37965-5
1sample wt/vol: 5.00 (g/mL) ML Lab File ID: C9179
Level: (low/med) LOW Date Received: 10/13/93
1% Moisture: not dee. Date Analyzed: 10/21/93
IGC Column: SPlOOO
Soil Extract Volume:
ID: 2.00 (mm)
(UL)
Dilution Factor: 1.0
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Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride --------67 -64 - 1 - - - - - - - - -Acetone c---,-----,--,---------75-35-4---------l, 1-Dichloroethene ------67-66-3---------Chloroform ----,--,--------107 -06 - 2 - - - - - - - -1, 2 -Di ch lo roe thane ------75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane -----
79-01-6---------Trichloroethene ~------79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene ----
108-88-3--------Toluene ------------100-41-4--------Ethylbenzene~--------
1330-20-7-------Xylene (total) _______ _
FORM I VOA
modified
10 u
10 u
10 u
10 u
10 u
10 u
10 ,u
10 u
10 u
10 u
10 u
10 u
10 u
(UL)
Q
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: PACE NEW ENGLA
EX02
Contract:
.Lab Code: Case No. : PCHAR
WATER
SAS No.: SDG No.: NASOl
Matrix: {soil/water) Lab Sample ID: 37965-6
.Sample wt/vol: 5.00 {g/mL) ML Lab File ID: C9180 -
Level: {low/med) LOW Date Received: 10/13/93
1% Moisture: not dee. Date Analyzed: 10/21/93
ID: Dilution Factor: 333.0 IGC Column: SPlOOO
Soil Extract Volume:
2.00 (mm)
{uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _ 3300
67-64-1---------Acetone 27000 ------------75 -35 - 4 - - - - - - - - -1, 1 -Di ch lo roe then e _____ _ 3300
67-66-3---------Chloroform 3300 -----------107-06-2--------1, 2-Dichloroethane 3300
75-27-4---------Bromodichlorometha_n_e ____ _ 3300
78-87-5---------1,2-Dichloropropane _____ _ 3300
79-01-6---------Trichloroethene 3300 --------79 -00 - 5 - - - - - - - - -1, 1, 2 -Tri ch lo roe thane 3300 -----71-43-2---------Benzene 3300 108-88-3--------Toluene ___________ _ 3300
100-41-4--------Ethylbenzene ~-------_;_ 1330-20-7-------Xylene (total) --------
3300
3300
Q
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'U u u u u u u
{uL)
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FORM I VOA
modified
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: PACE NEW ENGLA
EX03
Contract:
.Lab Code:
Matrix: (soil/water)
Case No. : PCHAR
WATER
SAS No.: SDG No.: NASOl
Lab Sample ID: 37965-7
lsample wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
I % Moisture: not dee.
Lab File ID: C9181
Date Received: 10/13/93
Date Analyzed: 10/21/93
I.Ge Column: SPlOOO
Soil Extract Volume:
ID: 2.00 (mm)
{UL)
Dilution Factor: 16.7
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Aliquot Volume: (uL)
CAS NO. COMPOUND
75-01-4---------Vinyl Chloride
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------170
67 -64 - l - - - - - - - - -Acetone 1200 ~--~~-------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e ------67-66-3---------Chloroform -----------107-06-2--------l, 2-Dichloroethane _____ _
75-27-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ~-------79 -00 - 5 - - - - - - - - -l, l, 2 -Tri ch lo roe thane -----71-43-2---------Benzene 108-88-3--------Toluene ___________ _
100-41-4--------Ethylbenzene ---------1330 -20 - 7 - - - - - - -Xylene (total) --------
FORM I VOA
modified
170
170
55
170
170
170
170
170
66
170
170
Q
u
u u
J
u
u
,u
u
u
J
u
u
3/90
lA I VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA
.Lab Code:
Matrix: (soil/water)
Case No. : PCHAR
WATER
lsample wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
1% Moisture: not dee.
Contract:
SAS No. :
Lab
Lab
Date
Date
EPA SAMPLE NO.
EX04
SDG No.: NASOl
Sample ID: 37965-8
File ID: C9182
Received: 10/13/93
Analyzed: 10/21/93
IGC Column: SPlOOO ID: 2. oo (mm)
(uL)
Dilution Factor: LO
· Soil Extract Volume: Soil Aliquot Volume:
I
I
I
I
I
I
I
I
I
i
I
I
I
CAS NO. COMPOUND
75-01-4---------Vinyl Chloride
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
67-64-1---------Acetone --------
75-35-4---------1,l-Dichloroethene
67-66-3---------Chloroform ------
107-06-2--------l,2-Dichloroethane ------75-~7-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane
79-01-6---------Trichloroethene ------
79-00-5---------1,l,2-Trichloroethane
71-43-2---------Benzene -----
108-88-3--------Toluene ------------100 - 4 l - 4 - - - - - - - -Ethyl benzene~----------'--
1330-20-7-------Xylene (total) --------
FORM I VOA
modified
10
27
10
10
10
10
10
10
10
10
3
10
10
I I :u
I
I :u :u :u :u :u u
u
u
J u
u
(uL)
Q
3/90
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NSlO
Name: PACE NEW ENGLA Contract: rab Code: Case No.: PCHAR SAS No.: SDG No.: NASOl
Matrix: (soil/water) WATER
l,sample wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
1% Moisture: not dee.
Lab Sample ID: 38016-17
Lab File ID: C9185
Date Received: 10/15/93
Date Analyzed: 10/21/93 re Column: SPlOOO
Soil Extract Volume:
ID: 2. 00 (mm)
(uL)
Dilution Factor: 33.3
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Aliquot Volume: (uL)
CAS NO. COMPOUND
75-01-4---------Vinyl Chloride
67 -64 - l - - - - - - - - -Acetone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------~--~~-------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e ------67-66-3---------Chloroform -~~--------
330
330
330
330
107-06-2--------l, 2-Dichloroethane 2800 ------75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane -----
79-01-6---------Trichloroethene -~------79 -00 - 5 - - - - - - - - -l, l, 2 -Tri ch lo roe thane
71-43-2---------Benzene ----
108-88-3--------Toluene ------------100 - 4 l - 4 - - - - - - - -Ethyl benzene~-------~
1330-20-7-------Xylene (total) --------
FORM I VOA
modified
330
330
330
330
330
330
330
330
Q
I
I :u :u :u :u
I
I :u :u :u :u :u :u :u :u
I
I
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NSll
Name: PACE NEW ENGLA Contract: rab Code: Case No.: PCHAR
WATER
SAS No.: SDG No.: NASOl
·Matrix: (soil/water) Lab Sample ID: 38016-18
lsample wt/vol: 5.00 (g/mL) ML Lab File ID: C9187
Level: (low/med) LOW
,I% Moisture: not dee.
Date Received: 10/15/93
Date Analyzed: 10/21/93
ID: Dilution Factor: re Column: SPlOOO
Soil Extract Volume:
2.00 (mm)
(uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _
67-64-1---------Acetone ------------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e _____ _
67-66-3---------Chloroform -----------107-06-2--------l, 2-Dichloroethane ------75-27-4---------Bromodichlorornethane -----78-87-5---------1,2-Dichloropropane _____ _
79-01-6---------Trichloroethene --------79 -00 - 5 - - - - - - - - -l, l, 2 -Tri ch lo roe thane -----71-43-2---------Benzene ------------108 -88 - 3 - - - - - - - -Toluene ------------100 - 4 l - 4 - - - - - - - -Ethyl benzene ~-------~ 1330-20-7-------Xylene (total) --------
25
130
25
25
25
25
25
25
25
25
120
300
560
I
I :u
I
I :u :u :u
'U
u u
u
u
2.5
Q
(UL)
I
I
I
I
i
I
I
I
I
I
I
I
I
FORM I VOA
modified
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS15
Name: PACE NEW ENGLA Contract:
:ILab Code: Case No. : PCHAR SAS No. : SDG No.: NASOl
· Matrix: (soil/water) WATER Lab Sample ID: 37995-1
lsample wt/vol: 5.00 (g/mL) ML Lab File ID: C9204
.Level: (low/med) LOW
:I% Moisture: not dee.
Date Received: 10/14/93
Date Analyzed: 10/22/93
IGC Column: SPlOOO
Soil Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 6.7
Soil Aliquot Volume:
CAS NO. COMPOUND
75-01-4---------Vinyl Chloride
67 -64 -1 ---------Acetone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
--------
c-:--~--------75 -35 -4 ---------1, 1 -Di ch lo roe then e ------67-66-3---------Chloroform 107-06-2--------1,2-Dichlo_r_o_e7t7h_a_n_e ______ _
75-27-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane
79-01-6---------Trichloroethene ------
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene -----
108-88-3--------Toluene ------------100 -41 -4 --------Ethyl benzene~--------
1330-20-7-------Xylene (total) --------
I
I
67 :u
67 :u
67 :u
67 :u
530 I
I 67 :u
67 u
67 u
67 u
67 u
18 J
67 u
67 ,u
I
I
Q
(uL)
I
I
I
I
I
I
I
I
i
D
FORM I VOA
modified
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS29
Name: PACE NEW ENGLA Contract:
'Lab Code: Case No. : PCHAR
WATER
SAS No.: SDG No.: NASOl
Matrix: (soil/water) Lab Sample ID: 37995-3
lsample wt/vol: 5.00 (g/mL) ML Lab File ID: C9206
.Level: (low/med) LOW
1% Moisture: not dee.
Date Received: 10/14/93
Date Analyzed: 10/22/93
ID: Dilution Factor: IGC Column: SPlOOO
Soil Extract Volume:
2.00 (mm)
(uL) Soil Aliquot Volume:
I .,
I
I
I
I
I
I
I
I
I I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _
67-64-l---------Acetone ___ ~--------
75-35-4---------1,l-Dichloroethene ------67-66-3---------Chloroform -~~--------107-06-2--------l, 2-Dichloroethane _____ _
75-27-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane _____ _
79-01-6---------Trichloroethene
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene ------------108 -88 - 3 - - - - - - - -Toluene ------------100 - 4 l - 4 - - - - - - - -Ethyl benzene ---------1330-20-7-------Xylene (total) --------
I
I
10 :u
10 'U
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 ,u
10 :u
10 :u
I
I
1.0
Q
(uL)
I
I
FORM I VOA
modified
3/90
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA
,,ab Code:
Matrix: (soil/water)
lsample wt/vol:
case No.: PCHAR
WATER
5.00 (g/mL) ML
Level: (low/med) LOW
1% Moisture: not dee.
Contract:
SAS No.:
Lab
Lab
Date
Date
NS30
SDG No. : NASOl
Sample ID: 37995-2
File ID: C9205
Received: 10/14/93
Analyzed: 10/22/93
lr-,c column: SPlOOO
Soil Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 1.0
I
I
I
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _
67-64-1---------Acetone ------------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e _____ _
67-66-3---------Chloroform -----------107-06-2--------l, 2-Dichloroethane _____ _
75-27-4---------Bromodichloromethane -----78-87-5---------1,2-Dichloropropane ------79-01-6---------Trichloroethene
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene ------------108 -88 - 3 - - - - - - - -Toluene ------------100 - 4 l - 4 - - - - - - - -Ethyl benzene ---------1330-20-7-------Xylene (total) _______ _
10 U
10 U
10 U
10 U
10 U
10 I U
10 :u
10 :u
10 :u
10 :u
10 : U
10 :u
10 :u
I
Q
-------'---
(uL)
I
I
f
I
I
I
I
I
I! FORM I VOA
modified
3/90
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
-
ILab Name: PACE NEW ENGLA
NS31
Contract:
,,Lab Code: Case No. : PCHAR
WATER
SAS No.: SDG No.: NASOl
Matrix: (soil/water) I Sample wt/vol:
Lab Sample ID: 38016-15
5.00 (g/mL) ML Lab File ID: C9191
Level: (low/med) LOW
-11% Moisture: not dee.
Date Received: 10/15/93
Date Analyzed: 10/21/93
ID: Dilution Factor: IGC Column: SPlOOO
Soil Extract Volume:
2.00 (mm)
{uL) Soil Aliquot Volume:
I
I.
I
I
I
I
I
~ I
I
I
I
,.
CAS NO. COMPOUND
75-01-4---------Vinyl Chloride
CONCENTRATION UNITS:
(ug/L or ug{Kg) UG/L
--------67 -64 - 1 - - - - - - - - -Acetone ~--~--------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e
67-66-3---------Chloroform ------
107-06-2--------1,2-Dichloroethane
75-27-4---------Bromodichlorometha_n_e ____ _
78-87-5---------1,2-Dichloropropane
79-01-6---------Trichloroethene ------
79-00-5---------1,1,2-Trichloroethane -----71-43-2---------Benzene 108-88-3--------Toluene ___________ _
100-41-4--------Ethylbenzene ---------1330-20-7-------Xylene (total) _______ _
I
I 10 :u
10 :u
10 :u
10 :u
20
10 u
31
10 u
10 u
10 u
6 J
10 u
10 :u
I I
1.0
Q
(uL)
I FORM I VOA
modified
3/90
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
NS32
Name: PACE NEW ENGLA Contract: rab Code:
'•Matrix: ( soil/water)
Case No.: PCHAR
WATER
SAS No.: SDG No. : NASOl
Lab Sample ID: 38016-19
'Sample wt/vol: 5.00 (g/mL) ML Lab File ID: C9188
Level: (low/med) LOW Date Received: 10/15/93
L Moisture: not dee. Date Analyzed: 10/21/93
IGC Column: SPlOOO
Soil Extract Volume:
ID: 2.00 (mm)
(UL)
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
l
I
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride --------67-64-1---------Acetone ~--~--------75-35-4---------1, 1-Dichloroethene _____ _
67-66-3---------Chloroform ----------107 -06 - 2 - - - - - - - -1, 2 -Di ch lo roe thane
75-27-4---------Bromodichlorometha_n_e ____ _
78-87-5---------1,2-Dichloropropane ____ _
79-01-6---------Trichloroethene -------79-00-5---------1,1,2-Trichloroethane ----71-43-2---------Benzene ------------108-88-3--------Toluene ------------100-41-4--------Ethylbenzene ---------1330-20-7-------Xylene (total) --------
FORM I VOA
modified
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 :u
10 :u
10 :u
10 :u
10 :u
10 :u
I
I
(uL)
Q
3/90
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
lab Name: PACE NEW ENGLA
NS9
contract:
tab Code: Case No. : PCHAR SAS No.: SDG No.: NASOl
Matrix: (soil/water) WATER
lample wt/vol:
t(evel: (low/med)
5.00 (g/mL) ML
LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
38016-20
C9203
10/15/93
10/22/93 R Moisture: not dee. IC Column: SPlOOO ID: 2.00 (mm)
(uL)
Dilution Factor: 25.0
Soil Extract Volume: Soil Aliquot Volume: (uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _
67-64-l---------Acetone;-.----,--,,--------
75-35-4---------1,1-Dichloroethene
67-66-3---------Chloroform ------
75
720
250
250
107-06-2--------l,2-Dichloroethane 4700
75-27-4---------Bromodichlorometha_n_e ____ _
78-87-5---------1,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ~~------79 -00 - 5 - - - - - - - - -l, l, 2 -Tri ch lo roe thane ____ _
71-43-2---------Benzene 108-88-3--------Toluene ___________ _
100-41-4--------Ethylbenzene-,--c---------'-
1330-20-7---~---Xylene (total) --------
FORM I VOA
modified
250
250
250
250
250
330
250
250
Q
I I lJ
I I u
u
u
u
u
u u
u
:u
I I
3/90
lA I
lab
VOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA Contract:
tab Code:
'Matrix: (soil/water)
Case No. : PCHAR
WATER
SAS No.:
Lab
lsample wt/vol: 5.00 (g/mL) ML Lab
_Level: (low/med) LOW
L Moisture: not dee.
Date
Date
EPA SAMPLE NO.
TB
SDG No. : NASOl
Sample ID: 38016-21
File ID: C9190
Received: 10/15/93
Analyzed: 10/21/93
IGC Column: SPlOOO
Soil Extract Volume:
ID: 2. 00 (mm)
(uL)
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _______ _
67-64-1---------Acetone ~--~~-------75 -35 - 4 - - - - - - - - -l, l -Di ch lo roe then e _____ _
67-66-3---------Chloroform --~--------107-06-2--------l, 2-Dichloroethane
75-27-4---------Bromodichlorometha_n_e ____ _
78-87-5---------1,2-Dichloropropane _____ _
79-01-6---------Trichloroethene
79-00-5---------1,1,2-Trichloro-e~t~h-a_n_e ____ _
71-43-2---------Benzene 108-88-3--------Toluene ___________ _
100-41-4--------Ethylbenzene .,....,.--------1330 -20 - 7 - - - - - - -Xylene (total) --------
FORM I VOA
modified
I I
10 :u
10 :u
10 :u
10 :u
10 :u
10 'U
10 u
10 u
10 u
10 u
10 u
10 u
10 u
(UL)
Q
3/90
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
lfab Code:
~atrix: (soil/water)
1sample wt/vol:
Level: (low/med)
1% Moisture:
case No. : PCHAR
WATER
910.0 (g/mL) ML
LOW
decanted: (Y/N)
'Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
IGPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EXOl
Contract:
SAS No. : SDG No.: NASOl
Lab Sample ID: 37965-1
Lab File ID: F5451
Date Received: 10/13/93
Date Extracted: 10/19/93
(uL) Date Analyzed: 11/01/93
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether __ _ 11 :u
27 :u 100-02-7--------4-Nitrophenol ________ _
FORM I SV-2
modified
I -------'---
3/90
I
lab
lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA
w,ab ~ode:
~atrix: (soil/water)
.Sample wt/vol:
Level: (low/med)
1% Moisture:
Case No. : PCHAR
WATER
955.0 (g/mL) ML
LOW
decanted: (Y/N)
'Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
IGPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX02
Contract:
SAS No. : SDG No. : NASOl
Lab Sample ID: 37965-2
Lab File ID: F5459
Date Received: 10/13/93
Date Extracted: 10/19/93
(uL) Date Analyzed: 11/01/93
Dilution Factor: 10.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
lll-44-4--------bis(2-Chloroethyl)ether __ _ 440
260
I
I :u
I
100-02-7--------4-Nitrophenol --------
I
I
I
I
I
I
I
I
I
-------------------------------'---
1' I
I FORM I SV-2
modified
3/90
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA rb Code:
Matrix: (soil/water)
lample wt/vol:
Level: (low/med)
I Moisture:
Case No. : PCHAR
WATER
960.0 (g/mL) ML
LOW
decanted: (Y/N)
loncentrated Extract Volume: 1000
'!njection Volume: 2.0(uL)
.PC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX03
Contract:
SAS No.: SDG No.: NASOl
Lab Sample ID: 37965-3
Lab File ID: F5460
Date Received: 10/13/93
Date Extracted: 10/19/93
(UL) Date Analyzed: 11/01/93
Dilution Factor: 2.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I I
I
I
I
I
I
I
I
I
I
I
I
lll-44-4--------bis(2-Chloroethyl)ether __ _ 74
52
I
I
100-02-7--------4-Nitrophenol _______ _
FORM I SV-2
modified
:u
I -------'---
3/90
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA
ILab Code:
Matrix: (soil/water)
lsample wt/vol:
ILevel: (low/med)
% Moisture:
case No. : PCHAR
WATER
940.0 (g/mL) ML
LOW
decanted: (Y/N)
.Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
IGPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX04
Contract:
SAS No.: SDG No.: NASOl
Lab Sample ID: 37965-4
Lab File ID: F5461
Date Received: 10/13/93
Date Extracted: 10/19/93
(UL) Date Analyzed: 11/01/93
Dilution Factor: 5.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I I
lll-44-4--------bis(2-Chloroethyl)ether __ _ 53
130
:u :u 100-02-7--------4-Nitrophenol ________ _
I
I
I
I
I
I
I
I
I
I
I
I
-------------------------------'---
i I FORM I SV-2
modified
3/90
I 1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE NEW ENGLA
ILab Code:
Matrix: (soil/water)
lsample wt/vol:
Level: (low/med)
I% Moisture:
Case No. : PCHAR
WATER
1000 (g/mL) ML
LOW
decanted: (Y /N)
I Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
I GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NSlO
Contract:
SAS No.: SDG No.: NASOl
Lab Sample ID: 38016-11
Lab File ID: F5463
Date Received: 10/15/93
Date Extracted: 10/20/93
(uL) Date Analyzed: 11/02/93
Dilution Factor: 5.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether __ _ 50
120
:u :u 100-02-7--------4-Nitrophenol _______ _
FORM I SV-2
modified
I -------'---
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: PACE NEW ENGLA
1Lab ~ode:
Matrix: (soil/water)
,.sample wt/vol:
Level: (low/med)
I% Moisture:
Case No. : PCHAR
WATER
980.0 (g/mL) ML
LOW
decanted: (Y/N)
.Concentrated Extract Volume: 1000
Injection Volume: 2.0(uL)
IGPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NSll
Contract:
SAS No.: SDG No.: NASOl
Lab sample ID: 38016-12
Lab File ID: F5457
Date Received: 10/15/93
Date Extracted: 10/20/93
(UL) Date Analyzed: 11/01/93
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
lll-44-4--------bis(2-Chloroethyl)ether ---10 : U
26 :u 100-02-7--------4-Nitrophenol _______ _
I
I
I
I
I
I
I
I
I
I
I
I
I
-------------------------------'---
FORM I SV-2
modified
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS15 I Lab Name: PACE NEW ENGLA Contract:
Lab Code: case No.: PCHAR SAS No.: SDG No.: NASOl
I Matrix: (soil/water) WATER Lab Sample ID: 37995-4
I Sample wt/vol:
Level: (low/med)
950.0 (g/mL) ML
LOW
Lab
Date
File ID: F5462
Received: 10/14/93
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: decanted: (Y/N) Date Extracted: 10/19/93
concentrated Extract Volume: 1000 (UL) Date Analyzed: 11/02/93
Injection Volume: 2. 0 (UL) Dilution Factor:
GPC Cleanup: (Y/N) N pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (~g/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether __ _
100-02-7--------4-Nitrophenol _______ _
42
110
I
I :u :u
I
4.0
Q
-------------------------------'---
FORM I SV-2
modified
3/90
1B I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
ltab Code:
latrix: (soil/water)
rample
Level:
wt/vol:
(low/med)
I Moisture:
Case No. : PCHAR
WATER
975.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1000
Contract:
SAS No.:
Lab
Lab
Date
Date
(uL) Date
EPA SAMPLE NO.
NS29
SDG No.: NASOl
Sample ID: 37995-6
File ID: F5453
Received: 10/14/93
Extracted: 10/19/93
Analyzed: 11/01/93 Concentrated Extract
Injection Volume: 2.0(uL) Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
Cleanup: (Y/N) N
CAS NO.
pH:
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
111-44-4--------bis(2-Chloroethyl)ether __ _
100-02-7--------4-Nitrophenol _______ _
18
26
I I I
I :u
I
Q
-------------------------------'---
FORM I SV-2
modified
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
ILab Name: PACE NEW ENGLA
NS30
Contract:
1Lab ~ode:
Matrix: (soil/water)
Case No. : PCHAR
WATER
SAS No.: SDG No.: NASOl
Lab Sample ID: 37995-5
I Sample wt/vol: 920.0 (g/mL) ML Lab File ID: F5452
Level: (low/med) LOW Date Received: 10/14/93
Date Extracted: 10/19/93
(uL) Date Analyzed: 11/01/93
I % Moisture:
concentrated Extract
I Injection Volume:
decanted: (Y/N)
Volume: 1000
2.0(uL) Dilution Factor: 1.0
I GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)ether __ _
100-02-7--------4-Nitrophenol ________ _
I
I
10 :J
27 :u
I
Q
I
I
I
I
I
I
I
I
I
I
I
I
-------------------------------'---
FORM I SV-2
modified
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
I Matrix: (soil/water) WATER
I sample wt/vol:
Level: (low/med)
960.0 (g/mL) ML
LOW
I % Moisture: decanted: (Y/N)
concentrated Extract Volume: 1000
I Injection Volume: 2.0(uL)
GPC Cleanup:
I CAS NO.
(Y/N) N pH:
COMPOUND
NS31
Contract:
SAS No.: SDG No.: NASOl
Lab Sample ID: 38016-9
Lab File ID: F5454
Date Received: 10/15/93
Date Extracted: 10/20/93
(UL) Date Analyzed: 11/01/93
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I I lll-44-4--------bis(2-Chloroethyl)ether ---25
26
I
I I 100-02-7--------4-Nitrophenol --------:u
I I
I
I
I
I
I
I
I
I
I
I
-------------------------------'---
FORM I SV-2
modified
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: PACE NEW ENGLA
lb Code:
iatrix: (soil/water)
lmple wt/vol:
~evel: (low/med)
I Moisture:
Case No.: PCHAR
WATER
950.0 (g/mL) ML
LOW
decanted: (Y/N)
loncentrated Extract Volume: 1000
'lfnjection Volume: 2.0(uL)
IPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS32
Contract:
SAS No.: SDG No.: NAS0l
Lab Sample ID: 38016-13
Lab File ID: F5458
Date Received: 10/15/93
Date Extracted: 10/20/93
(uL) Date Analyzed: 11/ 01/93
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
lll-44-4--------bis(2-Chloroethyl)ether __ _ 11 :u
26 :u
100-02-7--------4-Nitrophenol --------I
I
I
I
I
I
I
I
I
I
I
I
I
-------'---
FORM I SV-2
modified
3/90
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lab Name: PACE NEW ENGLA
.-,ab code:
'tatrix: (soil/water)
tample wt/vol:
case No.: PCHAR
WATER
950.0 (g/mL) ML
Level: (low/med) LOW
'Moisture: decanted: (Y/N)
aconcentrated Extract Volume: 1000
!lrnjection Volume: 2.0(uL) tpc Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS9
Contract:
SAS No.: SDG No.: NASOl
Lab Sample ID: 38016-14
Lab File ID: F5464
Date Received: 10/15/93
Date Extracted: 10/20/93
(uL) Date Analyzed: 11/02/93
Dilution Factor: 50.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I I
I
I
I
I
I
I
I
I
I
I
I
lll-44-4--------bis(2-Chloroethyl)ether __ _ 530 :u
1300 : U 100-02-7--------4-Nitrophenol ________ _
FORM I SV-2
modified
I -------'---
3/90
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc. contract:
Lab Code: Case No. : PCHAR SAS No. :
EPA SAMPLE NO.
MMEXOl
I Matrix (soil/water): WATER
SDG No.: MNASOl
Lab Sample ID: 38016-022
Date Received: 10/15/93 Level (low/med):
% Solids:
LOW
a.a I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
I
I
I
Comments:
COLORLESS
Analyte Concentration C Q M
-Aluminum NR
Antimony NR
Arsenic 2.4 u p
Barium 22.8 B p
Beryllium 0.40 u p
Cadmium 2.3 u p
Calcium NR
Chromium 2.7 u p
Cobalt NR
coeeer NR
Iron NR
Lead NR
Magnesium NR
Manganese 24.3 p
Mercury NR
Nickel 11. 8 B p
Potassium NR
Selenium 2. 3 u p
Silver NR
Sodium NR
Thallium NR
Vanadium NR
Zinc 9.7 B p
cyanide NR
--
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
I
I
I
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I
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I
I
I
I
I
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I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc.
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med) :
% Solids:
LOW
0.0
Contract:
SAS No.:
MMEX02
SDG No.: MNASOl
Lab Sample ID: 38016-007
Date Received: 10/15/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 4.8 u p
7440-39-3 Barium 1490 p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2. 3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.7 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 10800 p
7439-97-6 Mercury NR
7440-02-0 Nickel 13.8 B p
7440-09-7 Potassium NR
7782-49-2 Selenium 4. 6 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 56.5 p
cyanide NR
--
I Color Before: COLORLESS
YELLOW
Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
I Color After:
I
I
I
Comments:
Artifacts:
FORM I -IN 3/90
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc. Contract:
Lab Code: Case No.: PCHAR SAS No.:
EPA SAMPLE NO.
MMEX03
I Matrix (soil/water): WATER
SDG No.: MNAS0l
Lab Sample ID: 38016-008
Date Received: 10/15/93 Level (low/med):
% Solids:
LOW
0.0 I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
I
I
I
Comments:
YELLOW
Analyte Concentration C Q M
- -Aluminum NR
Antimony NR
Arsenic 4.8 u p
Barium 278 p
Beryllium 0.40 u p
Cadmium 2.3 u p
Calcium NR
Chromium 2.8 B p
Cobalt NR
coeeer NR
Iron NR
Lead NR
Magnesium NR
Manganese 11200 p
Mercury NR
Nickel 8.4 u p
Potassium NR
Selenium 4.6 u p
Silver NR
Sodium NR
Thallium NR
Vanadium NR
Zinc 2.5 B p
cyanide NR
- -
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc. Contract:
Lab Code: Case No. : PCHAR SAS No.:
EPA SAMPLE NO.
MMEX04
I Matrix (soil/water): WATER
SDG No.: MNAS0l
Lab Sample ID: 38016-023
Date Received: 10/15/93 Level (low/med):
% Solids:
LOW
o.o I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS
I Color After:
I
I
I
Comments:
COLORLESS
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.4 u
Barium 36.3 B
Beryllium 0.40 u
Cadmium 2. 3 u
Calcium
Chromium 2.7 u
Cobalt
Coeeer
Iron
Lead
Magnesium
Manganese 5090
Mercury
Nickel 8.4 u
Potassium
Selenium 2 . 3 u
Silver
Sodium
Thallium
Vanadium
Zinc 1.8 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
U.S. EPA -CLP
1
EPA SAMPLE NO.
I
I
I
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc.
Lab Code: Case No. : PCHAR
I Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Contract:
SAS No.:
MMMNS9
SDG No.: MNAS0l
Lab Sample ID: 38016-006
Date Received: 10/15/93
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: TAN
I Color After:
I
I
I
Comments:
YELLOW
Analyte Concentration C Q M
-Aluminum NR
Antimony NR
Arsenic 8.2 B p
Barium 1020 p
Beryllium 0.75 B p
Cadmium 2.3 u p
Calcium NR
Chromium 127 p
Cobalt NR
coeeer NR
Iron NR
Lead NR
Magnesium NR
Manganese 28100 p
Mercury NR
Nickel 54. 0 p
Potassium NR
Selenium 6.9 u p
Silver NR
Sodium NR
Thallium NR
Vanadium NR
Zinc 75.6 p
cyanide NR
--
Clarity Before: OPAQUE Texture:
Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England,
Lab Code: Case
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Inc.
No.: PCHAR
Contract:
SAS No.:
MMNSlO
SDG No.: MNASOl
Lab Sample ID: 38016-003
Date Received: 10/15/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.4 u p
7440-39-3 Barium 155 B p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2. 3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 16.3 p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 3540 p
7439-97-6 Mercury NR
7440-02-0 Nickel 33.9 B p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.3 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 43.2 p
cyanide NR
- -
Color Before: Texture:
I Color After:
TAN
COLORLESS
Clarity Before: CLOUDY
Clarity After: CLEAR Artifacts:
Comments:
I
I
I
FORM I -IN 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc.
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med) :
% Solids:
LOW
o.o
MMNSll
Contract:
SAS No.: SDG No.: MNAS0l
Lab Sample ID: 38016-004
Date Received: 10/15/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
- -7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.4 u p
7440-39-3 Barium 85.9 B p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2. 3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 17.4 p
7440-48-4 Cobalt NR
7440-50-8 COEEer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 55.6 p
7439-97-6 Mercury NR
7440-02-0 Nickel 35.1 B p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.3 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 15.0 B p
cyanide NR
--
I Color Before: TAN Clarity Before: CLOUDY
Clarity After: CLEAR
Texture:
I Color After: COLORLESS Artifacts:
Comments:
I
FORM I -IN 3/90
I
I
I
I
I
I
I
I
I
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc.
Lab Code: Case No. : PCHAR
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Contract:
SAS No. :
MMNS15
SDG No.: MNASOl
Lab Sample ID: 37995-007
Date Received: 10/14/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
-7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 4.8 u p
7440-39-3 Barium 444 p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2. 3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 3. 6 B p
7440-48-4 Cobalt NR
7440-50-8 Coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 15100 p
7439-97-6 Mercury NR
7440-02-0 Nickel 10.3 B p
7440-09-7 Potassium NR
7782-49-2 Selenium 4.6 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 1.8 u p
cyanide NR
--
I Color Before: COLORLESS Clarity Before: CLEAR Texture:
I Color After:
I
I
I
Comments:
COLORLESS Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
I
I
I
-I
I
I
I
I
a
I
I
I
I
I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England,
Lab Code: Case
Matrix (soil/water): WATER
Level (low/med) :
% Solids:
LOW
0.0
Inc.
No. : PCHAR
Contract:
SAS No. :
MMNS29
SDG No. : MNASOl
Lab Sample ID: 37995-009
Date Received: 10/14/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.4 u p
7440-39-3 Barium 61. 7 B p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2. 3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.7 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 177 p
7439-97-6 Mercury NR
7440-02-0 Nickel 8.4 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 2. 3 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 2.6 B p
cyanide NR
--
Before: COLORLESS
IColor After: COLORLESS
Comments:
Clarity Before: CLEAR
Clarity After: CLEAR
Texture:
Artifacts:
I
I
I
FORM I -IN 3/90
I
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I
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I
U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc.
Lab Code: Case No.: PCHAR
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
contract:
SAS No.:
MMNS30
SDG No.: MNASOl
Lab Sample ID: 37995-008
Date Received: 10/14/93
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No. Analyte Concentration C Q M
--7429-90-5 Aluminum NR
7440-36-0 Antimony NR
7440-38-2 Arsenic 2.4 u p
7440-39-3 Barium 29.8 B p
7440-41-7 Beryllium 0.40 u p
7440-43-9 Cadmium 2.3 u p
7440-70-2 Calcium NR
7440-47-3 Chromium 2.7 u p
7440-48-4 Cobalt NR
7440-50-8 coeeer NR
7439-89-6 Iron NR
7439-92-1 Lead NR
7439-95-4 Magnesium NR
7439-96-5 Manganese 2110 p
7439-97-6 Mercury NR
7440-02-0 Nickel 8.4 u p
7440-09-7 Potassium NR
7782-49-2 Selenium 2.3 u p
7440-22-4 Silver NR
7440-23-5 Sodium NR
7440-28-0 Thallium NR
7440-62-2 Vanadium NR
7440-66-6 Zinc 2. 2 B p
cyanide NR
--
I Color Before: COLORLESS Clarity Before: CLEAR Texture:
I Color After:
/
I
I
I
Comments:
COLORLESS Clarity After: CLEAR Artifacts:
FORM I -IN 3/90
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc. Contract:
Lab Code: Case No. : PCHAR SAS No.:
EPA SAMPLE NO.
MMNS31
I Matrix (soil/water): WATER
SDG No. : MNASOl
Lab Sample ID: 38016-001
Date Received: 10/15/93 Level (low/med):
% Solids:
LOW
0.0 I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Before: COLORLESS I Color After: COLORLESS
I
I
I
Comments:
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.9 B
Barium 15.6 B
Beryllium 0.40 u
Cadmium 2.3 u
Calcium
Chromium 2.7 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 21. 4
Mercury
Nickel 8.4 u
Potassium
Selenium 2. 3 u
Silver
Sodium
Thallium
Vanadium
Zinc 2. 6 B
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: PACE New England, Inc. Contract:
Lab Code: Case No.: PCHAR SAS No.:
EPA SAMPLE NO.
MMNS32
I Matrix (soil/water): WATER
SDG No. : MNASOl
Lab Sample ID: 38016-005
Level (low/med):
% Solids:
LOW
0.0
Date Received: 10/15/93
I
I
I
I
I
I
I
:I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: COLORLESS I Color After: COLORLESS
I
I
I
Comments:
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.4 B
Barium 85.6 B
Beryllium 0.40 u
Cadmium 2.3 u
Calcium
Chromium 2.7 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 99.8
Mercury
Nickel 8.4 u
Potassium
Selenium 2. 3 u
Silver
Sodium
Thallium
Vanadium
Zinc 1.8 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
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11
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SEE REVERSE SIDE FOR INSTRUCTIONS
I
I THE ASSURANCE Of QUALITY
I National Starch & Chemical
P.O. Box 399
Cedar Springs Road I Salisbury, NC 28145-0399
Attn: Mr. Jerry Smith
Company
I. Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
I Date Collected:
Date Received:
I Parameter
INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
I Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I Target Compounds List -Volatiles
Target Compounds List -Volatiles
I
I
I
I
I
I
I
9800 Kincey Avenue, Suite 100
I Hunte,sville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
10
1.0
0.5
1
December 28, 1993
PACE Project Number: 631013509
92 0109406
10/12/93
10/13/93
EXOl-10/93
----
10
5.4
ND
170
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351. 3
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
10/15/93
10/14/93
10/19/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
I THE ASSURANCE Cf QUALITY
I Mr. Jerry Smith
Page 2
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected: I Da1te Recseive1d: ID C ient amp e :
Parameter
I INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl I Sol ids, Total Dissolved
Target Analyte List -Jnorganics
I
I
I
I
I
I
I
I
I
I
I
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9 800 Kincey Avenue, Suite 100
Huntersvil!e, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
10
1.0
0.5
I
December 28, 1993
PACE Project Number: 631013509
92 0109414
10/12/93
10/13/93
EX02-I0/93
____ METHOD DATE ANALYZED
1000
730
4.0
3000
DONE
DONE
DONE
8000
4078
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/15/93
10/14/93
10/19/93
10/19/93
11/22/93
11 /22/93
11/22/93
An Equal Opportunity Employer
I
I lH[ ASSURANCE Of QUALITY
I Mr. Jerry Smith
Page 3
I
I
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
I INORGANIC ANALYSIS
I
I
I
I
I
I
I
I
I
I I
g
I
I
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincey Avenue. Suite 100
Huntersville, NC 28078
TEL: 704-B75-9092
FAX: 704-B75-9091
Units
mg/L
mg/L
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
JO
1.0
0.5
I
December 28, 1993
PACE Project Number: 631013509
92 0109422
10/12/93
10/13/93
EX3-J0/93
----
190
420
1.6
1700
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/15/93
10/14/93
10/26/93
10/19/93
11/22/93
11/22/93
11 /22/93
An Equal Opportunity Employer
I
I THE ASSURANCE OF OUlLIIY
I Mr. Jerry Smith
Page 4
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected: I Date Received:
Client Sample ID:
Parameter I INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS I Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
I Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I Target Compounds List -Volatiles
Target Compounds List -Volatiles
I
I
I
I
I
I
I
I
I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28G78
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
10
1.0
0.5
1
December 28, 1993
PACE Project Number: 631013509
92 0109430
10/12/93
10/13/93
EX4-10/93
----
90
140
1.8
680
DONE
DONE
DONE
METHOD DATE ANALYZED
8000
407B
351. 3
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
10/15/93
10/14/93
11/09/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
I TH!: ASSURANCE Of OUHITl
I Mr. Jerry Smith
Page 5
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kinny Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
I
December 28, 1993
PACE Project Number: 631013509
92 0110625
10/13/93
10/14/93
NS-15
10/93 METHOD DATE ANALYZED
910
3200
DONE
DONE
DONE
4078
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11 /22/93
11 /22/93
An Equal Opportunity Employer
I
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THE ASSURANCf Of QUALITY
Mr. Jerry Smith
Page 6
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0110633
10/13/93
10/14/93
NS-30
10/93 METHOD DATE ANALYZED
78
510
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/14/93
10/19/93
11 /22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
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TH£ ASSURANCE Of OUAlllY
Mr. Jerry Smith
Page 7
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/l
mg/l
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0110641
10/13/93
10/14/93
NS-29
10/93 METHOD DATE ANALYZED
59
410
DONE
DONE
DONE
4078
160 .1
CLP, EPA
CLP, EPA
CLP, EPA
10/14/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
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THE ASSURANCE Of QUALITY
Mr. Jerry Smith
Page 8
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kint1ty Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0111346
10/14/93
10/15/93
NS-31
10/93 METHOD DATE ANALYZED
51
610
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opponunitv Employer
I
I THE ASSURANCE OF QUALITY
I Mr. Jerry Smith
Page 9
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected: I Date Received:
Client Sample ID:
I
I
I
I
I
I
I
I
'I
I
I
I
I
I
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincev Avenue, Suite 100
Hun1emille, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0111400
10/14/93
10/15/93
NS-31B MS
10/93 METHOD DATE ANALYZED
50
620
DONE
DONE
DONE
407B
160 .1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11 /22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
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THE ASSURA~CE Of QUALITY
Mr. Jerry Smith
Page I 0
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample JD:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suitt 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0111435
10/14/93
10/15/93
NS-10
10/93 METHOD DATE ANALYZED
300
820
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11 /22/93
11/22/93
An Equal Opportunity Employer
I
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THE ASSURA~CE Of QUALITY
Mr. Jerry Smith
Page 11
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample ID:
.Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Units
Chloride mg/L
Solids, Total Dissolved mg/L
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincev Avenue, Suit, 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
REPORT OF LABORATORY ANALYSIS
MDL
1.0
I
December 28, 1993
PACE Project Number: 631013509
92 0111451
10/14/93
10/15/93
NS-11
""'10'-'--/.c....93'---METHOD DATE ANALYZED
9.2
400
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11/22/93
11 /22/93
An EQua! Opportunity Employer
I
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T~E ASSURA'-CE OF QUALITY
Mr. Jerry Smith
Page 12
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL, 704-875-9092
FAX, 704-875-9091
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
I
December 28, 1993
PACE Project Number: 631013509
92 0111478
10/14/93
10/15/93
NS-32
10/93 METHOD DATE ANALYZED
9.6
220
DONE
DONE
DONE
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
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Mr. Jerry Smith
Page 13
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
9800 Kincev Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0111486
10/14/93
10/15/93
NS-09
10/93 METHOD DATE ANALYZED
1600
5100
DONE
DONE
DONE
407B
160. 1
CLP, EPA
CLP, EPA
CLP, EPA
10/22/93
10/19/93
11/22/93
11/22/93
11/22/93
An Equal Opportunity Employer
I
I
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THE ASSURANCE Of QUALITY
Mr. Jerry Smith
Page 14
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Date Received:
Client Sample IO:
Parameter
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
9800 Kincev Avenue, Suite 100
Huntersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
REPORT OF LABORATORY ANALYSIS
MDL
December 28, 1993
PACE Project Number: 631013509
92 0111850
10/14/93
10/15/93
Trip Blank
____ METHOD DATE ANALYZED
DONE CLP, EPA 11/22/93
An Equal Opportunity Employer
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THE ASSURANCE Of OUAllTY
Mr. Jerry Smith
Page 15
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Sol ids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
Target Compounds List -Volatiles
Units
mg/L
mg/L
REPORT OF LABORATORY ANALYSIS
MDL
1.0
1
December 28, 1993
PACE Project Number: 631013509
92 0115953
10/14/93
10/15/93
NS318 MSD
10/93 METHOD DATE ANALYZED
52
610
DONE
DONE
DONE
4078
160.1
CLP, EPA
CLP, EPA
CLP, EPA
10/28/93
10/26/93
11/22/93
11/22/93
11/22/93
These data have been reviewed and are approved for release.
Charles M. Cabaniss
Manager, Inorganic Chemistry
, ) !';/ -~ , ,,
: /-I/ti, -~'1 ',!/ I , V J C
fargaret S. Harding ~--
Manager, Organic Chemistry
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: 704,875-9091
An EQual Opportunity Employer
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REPORT OF LABORATORY ANALYSIS
T~t ASSURANCl: OF QUALITY
Mr. Jerry Smith
Page 16
FOOTNOTES
for pages 1 through
Client Reference: Quarterly Monitoring -CLP
MDL
ND
Method Detection Limit
Not detected at or above the MDL.
9800 Kincey Avenue, Sui1e 100
Hun1emille, NC 28078
TEL: [phone]
FAX: [phone]
December 28, 1993
15 PACE Project Number: 631013509
An Equal Opportunity Employer
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REPORT OF LABORATORY ANALYSIS
THE ASSURANCE Of QUALITY
Mr. Jerry Smith
Page 17
QUALITY CONTROL DATA December 28, 1993
Client Reference: Quarterly Monitoring -CLP
Chemical Oxygen Demand
Batch: 92 23281
Samples: 92 0109406, 92 0109414, 92 0109430
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
SPIKE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
9800 Kincey Avenue, Suite 1 OD
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
Units
mg/L
Units
mg/L
MDL
To
MDL
To
MDL
To
PACE Project Number: 631013509
Method
Blank
ND
Duplicate
of
920106008 92 0106008
1000 1000
Spike
920106008 Spike Recv
1000 ~ 100%
Reference
Value Recv
1000 100%
An Equal Opportunity Employer
RPO
0%
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REPORT OF LABORATORY ANALYSIS
TH[ ASSURANCE Of OUALITY
QUALITY CONTROL DATA December 28, 1993 Mr. Jerry Smith
Page 18 PACE Project Number: 631013509
Client Reference: Quarterly Monitoring -CLP
Chloride
Batch: 92 23268
Samples: 92 0109406, 92 0109414, 92 0109422, 92 0109430, 92 0110633
92 0110641
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
chloride
9800 Kincev Avenue. Suite 100
Huniersville. NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/ L
Units
mg/L
Units
mg/L
MDL
1.0
MDL r:o
MDL r:o
Method
Blank
ND
Duplicate
of
920105214 92 0105214
2.0 2.9
Spike
920105222 Spike Recv
12 W-100%
Reference
Value Recv
1000 100%
An Equal Opportunitv Employer
RPD
37%
I
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REPORT OF LABORATORY ANALYSIS
THE ASSURA'-CE OF □UAllTY
QUALITY CONTROL DATA December 28, 1993 Mr. Jerry Smith
Page 19 PACE Project Number: 631013509
Client Reference: Quarterly Monitoring -CLP
Chloride
Batch: 92 23490
Samples: 92 0]10625, 92 Olll346, 92 Olll400, 92 0111435, 92 Olll451
92 0111478, 92 0111486
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
Chloride
9800 Kincey Avenue. Suite 100
HuntersviJ!e, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
Units
mg/L
Units
mg/L
MDL
1.0
MDL
1.0
MDL
1.0
Method
Duplicate
of
Blank 920112580 92 0112580
3.9 ND 4.3
Spike
920113772 Spike Recv
5.3 10 101%
Reference
Value Recv
1000 100%
An Eciual Opportunity Employer
RPD
10%
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REPORT OF LABORATORY ANALYSIS
THE ASSURANCE OF OUALITY
Mr. Jerry Smith
Page 20
QUALITY CONTROL DATA December 28, 1993
Client Reference: Quarterly Monitoring -CLP
Chloride
Batch: 92 23629
Samples: 92 0115953
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
Chloride
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
Units
mg/L
Units
mg/L
MDL
1.0
MDL r:o
MDL
1.0
PACE Project Number: 631013509
Method
Blank 920115155
ND 4.3
920115953
NS31B MSD
10/93 Spike
52 10
Reference
Value
1000
Duplicate
of
92 0115155
4.8
Spike
Recv
100%
Recv
100%
An Equal Opportunity Employer
RPO
11%
I
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REPORT OF LABORATORY ANALYSIS
THE ASSURANCE Of QUALITY
Mr. Jerry Smith
Page 21
QUALITY CONTROL DATA December 28, 1993
Client Reference: Quarterly Monitoring -CLP
Nitrogen, Kjeldahl
Batch: 92 23426
Samples: 92 0109406, 92 0109414
METHOD BLANK:
Parameter
Nitrogen, Kjeldahl
LABORATORY CONTROL SAMPLE:
Parameter
Nitrogen, Kjeldahl
9800 Kincev Avenu11, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
Units
mg/L
MDL o:s
MDL
0.5
PACE Project Number: 631013509
Method
Blank
ND
Reference
Value Recv
20 90%
An Equal Opportunity Employer
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REPORT OF LABORATORY ANALYSIS
THE ASSURANCE Of OUAtlTY
Mr. Jerry Smith
Page 22
QUALITY CONTROL DATA December 28, 1993
Client Reference: Quarterly Monitoring -CLP
Nitrogen, Kjeldahl
Batch: 92 23649
Samples: 92 0109422
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Nitrogen, Kjeldahl
LABORATORY CONTROL SAMPLE:
Parameter
Nitrogen, Kjeldahl
9800 Kincey Avenue, Suite 100
Huntersvil!e, NC 28078
TEL: 704-B75-9092
FAX: 704-B75-9091
Units
mg/L
Units
mg/L
MDL
0.5
MDL
0.5
PACE Project Number: 631013509
Method
Blank
ND
Duplicate
of
920112750 92 0112750
1.4 I. I
Reference
Value Recv
20 90%
An Equal Opportunity Employer
RPD
24%
I
REPORT OF LABORATORY ANALYSIS I THE ASSURA~CE Of OUALIH
I Mr. Jerry Smith
Page 23
QUALITY CONTROL DATA December 28, 1993
I Client Reference: Quarterly Monitoring -CLP
Nitrogen, Kjeldahl
I
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Batch: 92 23960
Samples: 92 0109430
METHOD BLANK AND SAMPLE DUPLICATE:
Parameter
Nitrogen, Kjeldahl
SPIKE:
Parameter
Nitrogen, Kjeldahl
LABORATORY CONTROL SAMPLE:
Parameter
Nitrogen, Kjeldahl
9800 Kincey Avenue, Suite 100
Huntersvitle, NC 28078
TEL: 704-B75-9092
FAX: [phone]
Units
mg/L
Units
mg/L
Units
mg/L
MDL
0.5
MDL
0.5
MDL
0.5
PACE Project Number: 631013509
Method
Blank
ND
920109430
EX4-10/93
1.8
Duplicate
of
92 0109430
1.6
92011715B Spike
Spike
Recv
120% 35 10
Reference
Value Recv
20 80%
An Equal Opportunity Employer
RPD
12%
I
I REPORT OF LABORATORY ANALYSIS
THE ASSURANCE Of OUALlTY
I Mr. Jerry Smith .
Page 24
QUALITY CONTROL DATA December 28, 1993
I Client Reference: Quarterly Monitoring -CLP
Solids, Total Dissolved
Batch: 92 23407 I Samples: 92 0109406,
92 0110633,
92 0111451,
I
92 0109414,
92 0110641,
92 0111478,
92 0109422,
92 0111346,
92 0111486
METHOD BLANK AND SAMPLE DUPLICATE:
I Parameter
I
I
I
I
I
I
I
I
I
I
I
I
Solids, Total Dissolved
LABORATORY CONTROL SAMPLE:
Parameter
Sol ids, Total Dissolved
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
Units
mg/L
PACE Project Number: 631013509
92 0109430, 92 0110625
92 0111400, 92 0111435
MDL -]-
MDL -1-
Method
Blank
ND
Duplicate
of
920108981 92 0108981
2200 2200
Reference
Value Recv
100 100%
An Equal Opportunity Employer
RPD
0%
I
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THt ASSUAUCE Of QUAllTY
Mr. Jerry Smith
Page 25
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA December 28, 1993
PACE Project Number: 631013509
Client Reference: Quarterly Monitoring -CLP
Solids, Total Dissolved
Batch: 92 23606
Samples: 92 0115953
METHOD BLANK:
Parameter
Solids, Total Dissolved
SPIKE:
Parameter
Solids, Total Dissolved
LABORATORY CONTROL SAMPLE:
Parameter
Sol ids, Total Dissolved
9800 Kincey Avenue, Suite 100
Huntersville. NC 28078
TEL, 704-875-9092
FAX, 704-875-9091
Units
mg/L
Units
mg/L
Units
mg/L
MDL -1-
MDL -1-
MDL -1-
Method
Blank
ND
920115953
NS31B MSD
10/93 Spike
610 100
Reference
Value
100
Spike
Recv
100%
Recv
98%
An Equal Opportufllly Employer
I
REPORT OF LABORATORY ANALYSIS I THE ASSURA~CE OF QUALITY
I Mr. Jerry Smith
Page 26
FOOTNOTES
for pages 17 through 25
I Client Reference: Quarterly Monitoring -CLP
I MDL
ND
RPO
I
I
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I
Method Detection Limit
Not detected at or above the MDL.
Relative Percent Difference
9800 Kincey Avenue, Suite 100
HuntersviUe, NC 28078
TEL: [phone]
FAX: [phone]
December 28, 1993
PACE Project Number: 631013509
An Equal Opportunity Employer