NCD991278953_19930716_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Second Quarter 1993 OU-1 OU-2-OCR

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Quarterly Report
Second Quarter 1993
Operable Units One and Two
National Starch and Chemical Company Site
Cedar Springs Road
KN/1162/WP 1162.TXT/07-12-93/04
Salisbury, North Carolina
Prepared by:
IT Corporation
312 Directors Drive
Knoxville, Tennessee
July 16, 1993
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INTERNATIONAL TECHNOLOGY
CORPORATION
July 16, 1993
Kt.G!tlVtU
JUL 2 3 l~~j
SUPERFUND SfCJJON
IT Project No. 408668. I 9. JO
408668. 70.91
Mr. Jon Bornholm
Remedial Project Manager
Environmental Protection Agency
345 Courtland Street, N.E.
Atlanta, Georgia 30365
Quarterly Report. Second Quarter 1993,
Operable Units One and Two
National Starch and Chemical Company Site
Salisbury, North Carolina
Dear Jon:
Enclosed are five bound and one unbound copies of the quarterly report. If you have any
questions, please call me at 615/690-3211.
Sincerely,
IT CORPORATION
Michael N. Sturdevant, P.E.
Project Manager
Enclosures
cc: Hank Graulich, NSCC
Alex Samson, NSCC
Ray Parodowski, NSCC
Regional O!tice
312 Directors Dnve •Knoxville.Tennessee 37923 • 615-690-3211
KN/KP.J 1/07-16-93
lT Corporation is a who/ly owned subsidiary of Internat10nal Technology Corporation
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Quarterly Report
Second Quarter 1993
Operable Units One and Two
National Starch and Chemical Company Site
Cedar Springs Road
KN/l 162/WP1162.TXT~7-12-93/D4
Salisbury, North Carolina
Prepared by:
IT Corporation
312 Directors Drive
Knoxville, Tennessee
July 16, 1993
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List of Tables'--------------------
Table Title
1 Sample Analysis and Water Level Monitoring Summary
2 ROD (QUI) Contaminants and Selected Water Quality Parameters in Groundwater
(QUI)
3 ROD (QUI) Contaminants and Selected Water Quality Parameters in Groundwater
(OU2)
4 Groundwater Cleanup Criteria, Operable Unit One
5 Water Level Measurements, Second Quarter 1993, Operable Unit One
6 Water Level Measurements, Second Quarter 1993, Operable Unit Two
List of Figures. _________________ _
Figure Title
1 Site Map
2 Water Level Contour Map for Bedrock Water Levels, May 3, 1993
·,
KNnt62JWPl162.TXT,o?-12·93/D4 11
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Table of Contents'-------------------
Groundwater Monitoring Activities for the Second Quarter 1993 . . . . . . . . . . . . . . . . . . . 1
Activities Planned for the Third Quarter 1993 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Appendix A -Certificates of Analysis
KN/1162./WPI 162.1XfJ07-12-93/D4 1
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Groundwater Monitoring Activities for the Second Quarter
1993, ___________________ _
Operable Unit One. Groundwater samples from four downgradient groundwater
monitoring wells (NS29, NS30, NS31, and NS32) and four bedrock extraction wells (EX0l,
EX02, EX03, and EX04) were collected on May 4, 1993. Extraction wells EX02 and EX03
were in operation. All samples were analyzed for Target Compound List (TCL), volatile and
semivolatile organic compounds (VOCs and SVoes), and Target Analyte List (TAL) metals.
In addition, samples from the four downgradient monitoring wells were analyzed for selected
water quality parameters to monitor influent loadings to the Plume Periphery Pretreatment
System (PPPS) and to project start-up flow rates for the Combined Pretreatment System
(CPS). A sample analysis summary is provided in Table 1. The TCL and TAL compounds
were analyzed under U.S. Environmental Protection Agency (EPA) Level IV Contract
Laboratory Program (CLP) protocol.
Results from the chemical analysis for Operable Unit One and Operable Unit Two are
presented in Tables 2 and 3, respectively. The list of compounds presented in these tables
represents the contaminants specified in the Operable Unit One Record of Decision (ROD).
The list of compounds from the ROD and associated cleanup levels are provided in Table 4
for reference. Figure 1 is a site map showing the well locations. The Certificates of Analysis
are provided in Appendix A.
The most predominant contaminants are voes. For the extraction wells, four VOCs, one
svoe, and one metal were detected at levels that exceed cleanup levels (shaded values in
Table 2). Samples from extraction wells EX02 and EX03 contained elevated levels of
acetone, 1,2-dichloroethane, 1,2-dichloropropane, and bis(2-chloroethyl)ether. For the
downgradient wells, two Voes, one SVOC, and one metal exhibited levels that exceed
cleanup levels (shaded values in Table 2).
Compared to the first quarter data from the downgradient monitoring wells, there has been a
considerable decrease in levels of acetone and 1,2-dichloroethane in wells NS29, NS30, and
NS31. During the first quarter, acetone was detected in these wells ranging from 2,900 parts
per billion (ppb) (NS30) to 12,000 ppb (NS29). Acetone was not detected in any of the
downgradient wells during the second quarter. Levels of 1,2-dichloroethane have decreased
by one order of magnitude in each of these wells.
KN/1162/WPI 162.TXTAJ7-12-93/04 I
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Water level measurements were taken (May 3, 1993) from all four downgradient and several
other selected monitoring wells and all four extraction wells. Results are provided in Table 5.
Groundwater elevations and a bedrock groundwater contour map is provided as Figure 2.
The extraction wells have been fouled by a black substance that is probably a result of iron
and manganese precipitation. This precipitation was the apparent cause of the pump failure in
well EX02 during the first quarter (February 1993). The motor in EX02 was replaced and
has been functioning properly.
Operable Unit Two. Groundwater samples were collected from monitoring wells NS09,
NSlO, NSll, and NS15 on May 4, 1993. All samples were analyzed for TCL VOCs and
SVOCs, and T AL metals. In addition, the samples were analyzed for selected water quality
parameters to provide design information and project start-up flow rates for the CPS. A
sample analysis summary is provided in Table 1. The TCL and TAL compounds were
analyzed under EPA Level IV CLP protocol.
Results from the chemical analysis are presented in Table 3. The list of compounds presented
in Table 3 represent the contaminants specified in the Operable Unit One ROD. The list of
compounds from the ROD and associated cleanup levels are provided in Table 4 for
reference. Figure I is a site map showing the well locations. The Certificates of Analysis are
provided in Appendix A.
The most predominant contaminants are VOCs. Four VOCs and three metals exhibited levels
that exceed cleanup levels (shaded values in Table 3). Elevated levels of 1,2-dichloroethane
were detected in NS09, NSlO, and NS15 ranging from 500 ppb to 16,000 ppb.
Water level measurements were taken (May 3, 1993) from each of the four monitoring wells.
Results are provided in Table 6. Groundwater elevations and a bedrock contour map,
constructed primarily from Operable Unit One wells, is provided as Figure 2.
KNn 162/WPI I62.TXT,m-t 2-93/D4 2
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Activities Planned for the Third Quarter 1993. _____ _
Operable Unit One. Groundwater monitoring will continue. Operation of extraction wells
EX02 and EX03 will continue. Start-up of the Combined Pretreatment System is scheduled
for September 1993. Upon completion of the pretreatment system start-up, extraction wells
EX0 1 and EX04 will be returned to service so that all extraction wells are operating.
However, the data indicate that the plume is not present at these wells.
Operable Unit Two. Groundwater monitoring will continue. Presently, bids are being
solicited from subcontractors to install the six new extraction wells (EX05, EX06, EX07,
EX08, EX09, and EXlO) in the trench area. Construction is scheduled for September 1993
with completion by November 1993 and start-up in February 1994. The extraction well
locations are shown in Figure 1.
KN/ll62/WPl162TXT,o7-12•93/D4 3
Well
Well Number Type'
Operable Unit One
EXOl BE
EXO2 BE
EXO3 BE
EXO4 BE
NSO5 SM
NSO6 SM
NS21 BM
NS22 BM
NS23 SM
NS26 BM
NS27 BM
NS28 BM
NS29 BM
NS3O BM
KN/1162/WP1162. T1 /06-30-93/02
Table 1
Sample Analysis and Water Level Monitoring Summary
Second Quarter 1993
TCL
Operable Units One and Two
National Starch and Chemical Company
Salisbury, North Carolina
(Page 1 of 2)
TCL TAL
voes SVOCs Metals TDSb Chloride COD'
X X X X X X
X X X X X X
X X X X X X
X X X X X X
X X X X X
X X X X X
Water
TKNd Level
X X
X X
X X
X X
X
X
X
X
X
X
X
X
X
X
Well TCL TCL
Table 1
(Page 2 of 2)
TAL
Well Number Type' voes SVOCs Metals TDSb
Operable Unit One (Continued)
NS31 BM X
NS32 BM X
Stream Gage No. 1 • NA' NA
Stream Gage No. 2 NA NA
Operable Unit Two
NS09 SM X
NS10 SM X
NS11 SM X
NS15 BM X
'BE -Bedrock extraction well
SM -Saprolite (shallow) monitoring well
BM -Bedrock monitoring well
bTDS -Total dissolved solids
'COD -Chemical oxygen demand
dTKN -Total Kjeldahl nitrogen
X X
X X
NA NA
NA NA
X X
X X
X X
X X
'Iron pins in southwest tributary for monitoring stream elevations
'NA -not applicable
KN/1162/WP1162. T1 /06-30-93/02
X
X
NA
NA
X
X
X
X
Water
Chloride COD' TKNd Level
X X
X X
NA NA NA X
NA NA NA X
X
X X
X X X
X X X
X X
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Well Number
Sample Date
Volatile Organics (ppb)'
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-Dichloroethane
1, 1-Dichloroethylene
1,2-Dichloropropane
Ethyl benzene
Methylene chloride
Toluene
1, 1,2-Trichloroethane
Trichloroethylene
Vinyl chloride
Xylenes (total)
Semivolatile Organics (ppb)
bis(2-Chloroethyl)ether
4-Nitrophenol
KN/1162/WP1162.T2/0&28·93/D2
Table 2
ROD (OU1) Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1993
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
(Page 1 of 4)
EX01 EX02 EX03
May 1993 May 1993 May 1993
10 U' · .. : .. · .
29;000 D ··••· .22000 ... ·· •.•
SU SU 5 U
SU SU SU
SU 5 U SU
·.···· • i\ I < es•·. ·••· t i SU :·.•· ·.: i4'700
SU SU SU .. . ·::;::::,:-·_;· 4J 820 DJ 180 . · : •• . .
SU 9 2J
1 J 4J 2J
SU 1 10 46
SU SU SU
SU SU 5 U
10 U 10 U 10 U
SU 38 7
4J 3800 100
50 U 52 U 56 U
EX04
May 1993
10 U
SU
5 U
SU
3J
SU
SU
SU
2J
2J
SU
5 U
10 U
1 J
SJ
54 U
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Well Number
Sample Date
lnorganlcs (ppb)
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
Water Quality (ppm)d
TDS
Chloride
COD
TKN
KN/11621WP1162. T2/06-28·93/02
Table 2
(Page 2 of 4)
EX01 EX02
May 1993 May 1993
2.0U 2.0 U
25.3 B
1.0U 1.0 U
5.0 U 5.0 U
10.0 U 12.8
206 7180
20.0 U 75.5
2.0 U 2.0 U
32.7 15.4 B
204 2540
6.5 460
50 902
0.7 2.8
EX02° EX03 EX04
May 1993 May 1993 May 1993
2.0 U 2.0 U 2.0 U
~ 140 B 26.9 B
1.0U 1.0 U 1.0 U
5.0 U 5.0 U 5.0 U
12.89 10.0 U 10.0 U
7165.41 2760 3270
69.99 20.0 U 20.0 U
2.0 U 2.0 U 2.0 U
16.37 B 16.9 B 172 B
NA 968 488
NA 29 23
NA 348 85
NA 0.7 0.4
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Well Number
Sample Date
Volatile Organics (ppb)
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-Dichloroethane
1, 1-Dichloroethylene
1,2-Dichloropropane
Ethyl benzene
Methylene chloride
Toluene
1, 1,2-Trichloroethane
Trichloroethylene
Vinyl chloride
Xylenes (total)
Semivolatile Organics (ppb)
bis(2-Chloroethyl)ether
4-Nitrophenol
lnorganics (ppb)
Arsenic
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Selenium
Zinc
KN/11621WP1162.T2/06-28-93/D2
NS29
May 1993
10 U
5 U
5 U
5U
.··
21
5U
.• < 43)}!
5 U
2J
6
5U
5 U
10 U
2 J
. .-:·,.:..··: ·-•:,;::•.-,_
.. .. -. ·•
56 U
2.0 U
97.0 B
1.0 U
5.0 U
16.6
218
20.0 U
2.0 U
15.8 8
. '
Table 2
(Page 3 of 41
NS29'
May 1993
10 U
5U
5U
5U ... .
23. I
5 U
>• ....
I . '/
5U
5U
7
5 U
5U
10 U
2J
........
'f.50
52 U
2.0 U
77.8 8
1.0 U
5.0 U
12.4
167
20.0 U
2.0 U
18.2 8
NS30 NS31 NS32
May 1993 May 1993 May 1993
10 U 10 U 10 U
5U 5U 5U
5 U 5 U 5U
5 U 5 U 5U
•8 .. Ii 71 · . . ... 5U
5U 5U 5 U
.\ .. ·· .... ,.; \, )t ·., ... > 5U
5 U 2J 5U
5 U 5U 1 J
2J 34 5U
5U 5U 5 U
5U 5 U 5U
10 U 10 U 10 U
5 U 7 5U
32 ' } ·,. · .. ·· "" ? 10 U
50 U 52 U 50 U
2.0 U 2.0 U 2.0 U
31.8 8 36.3 8 69.0 8
1.0 U 1.0 U 1.0 U
5.0 U 5.0 U 5.0 U
'., .,:-:•:'•' ·:,,•,•,:,. '·.-:: .. , __ ._,_
10.0 U .. /74:0. 10.0 U
1,620 47 .1 78.2
20.0 U 47.5 20.0 U
2.0 U 2.0 U 2.0 U
12.1 8 1,640 57.0
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Table 2
(Page 4 of 41
Well Number NS29 NS29' NS30 NS31 NS32
Sample Date May 1993 May 1993 May 1993 May 1993 May 1993
Water Quality (ppm)
TDS 582 454 606 744 250
Chloride 34 11 22 140 4.5
'ppb -parts per billion.
bQualifiers: U -compound was analyzed for, but not detected. The number is the detection limit for the sample.
J -indicates an estimated value less than the detection limit.
0Duplicate.
B (organics) -analyte was found in the blank as well as the sample.
B (inorganics) -Value greater than instrument detection limit, but less than contract required
quantitation limit.
D -compound analyzed at a secondary dilution factor.
dppm -parts per million.
KN/1162/WP1162. T2/06-28-93/D2
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Table 3
ROD (OU1 l Contaminants and Selected
Water Quality Parameters in Groundwater
Second Quarter 1993
Well Number
Sample Date
Volatile Organics (ppb)'
Acetone
Benzene
Bromodichloromethane
Chloroform
1,2-Dichloroethane
1, 1-Dichloroethylene
1,2-Dichloropropane
Ethyl benzene
Methylene chloride
Toluene
1, 1,2-Trichloroethane
Trichloroethylene
Vinyl chloride
Xylenes (total)
Operable Unit Two
National Starch and Chemical Company,
Salisbury, North Carolina
(Page 1 of 2)
NS09 NSlO NS11
May 1993 May 1993 May 1993
10 U' 10 U 10 U
5U 5U 5U
5U 5 U SU
5 U SU 5 U
ir1q,ObOh••••• .... 16,000 Ci. . .. 5U .•.... • \fo /
· ..... ·. 5 U 5U
5U 2 J 5U
32 4J 95
SU 3 J 1 J
••·•• .. )466•6·.•.·············· 2J 61
3 J r· ·•• ......... < •• 1 Qi•,•.· .. · ... SU
5 U 1 J 5 U
S .. ··.•·. .. >\ 10 U ,8.J. 10 U
69 10 150
Semivolatile Organics (ppbJ
bisl2-ChloroethyIJether 10 U 11 U 1 1 U
4-Nitrophenol 50 U 53 U 56 U
lnorganics (ppbJ
Arsenic 2.0 U 2.0 U 2.0 U
', :'''
Barium 1480 297 115 B
Beryllium 1.0 U 1.0 U 1.0 U
Cadmium 5.0 U 5.0 U 5.0 U
Chromium ·.·... sdH" ···• 1-,., .. :--/ _ .. :·.: 14.2 10.0 U
KN/1162/WP1162. T3/06-30-93/D3
NS15
May 1993
10 U
SU
SU
SU
• .. ,., .,,;,•';'. . .. .•
.500D
SU
2J
SU
2J
22
SU
SU
10 U
SU
11 U
54 U
2.0 U
448
1.0 U
5.0 U
11. 7
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Well Number
Sample Date
Manganese
Nickel
Selenium
Zinc
Water Quality (ppm)0
TDS
Chloride
COD
TKN
NS09
Table 3
(Page 2 of 2)
NS10
May 1993
23.9 B 45.2
10.0 U 2.0 U
492 47.4
4130 478
2300 1000
616
NA 2.0
NS11
May 1993
63.1
20.0 U
2.0 U
32.5
2390
1.0
473
180
NS15
20.0 U
2.0 U
14.5 B
2630
950
NA
NA
8 ppb -parts per billion
baualifiers: U -compound was analyzed for but not detected. The number is the detection limit for
the sample.
J -indicates an estimated value less than the detection limit.
B (organics) -analyte was found in the blank as well as the sample.
B (inorganics) -Value greater than instrument detection limit, but
less than contract required quantitation limit.
D -compound analyzed at a secondary dilution factor.
0ppm -parts per million
dNA -not analyzed
KN/1162/WPl 162.T3/06-30-93/D3
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Table 4
Groundwater Cleanup Criteria
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
Compound Cleanup Concentration (ppb)3
Volatlle Organics
Acetone 3,500
Benzene 5
Bromodichloromethane 5
Chloroform 5
1 ,2-dichloroethane 5
1 , 1-dichloroethylene 7
1,2-dichloropropane 6
Ethyl benzene 3,500
Methylene chloride 5
Toluene 2,000
1, 1 ,2-trichloroethane 5
Trichloroethylene 5
Vinyl chloride 2
Xylenes 350
Semlvolatlle Organics
Bis(2-chloroethyl)ether 5
4-Nitrophenol 350
lnorganlcs
Arsenic 10
Barium 1,000
Beryllium 17.5
Cadmium 10
Chromium 50
Manganese. 7,700
Nickel 350
Selenium 10
Zinc 7,350
"ppb = parts per billion.
Reference source: U.S. Environmental Protection Agency, Enforcement Record of Decision, Remedial
Alternative Selection for Operable Unit One, National Starch and Chemical Corporation Site, prepared
for U.S. EPA Region IV, Atlanta, Georgia (9-30-88), p. 19.
KNl1161!WP1161.T410&25-93/01
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Well
EX01
EX02
EX03
EX04
NS05
NS06
NS21
NS22
NS23
NS26
NS27
NS28
NS29
NS30
NS31
NS32
P01
Stream Gage 1
Stream Gage 2
Table 5
Water Level Measurements
Second Quarter 1993
Operable Unit One
National Starch and Chemical Company,
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (ft msll' (ft msll
5/3/93 TOC' 731.85 28.86
5/3/93 TOC 718.24 9.87
5/3/93 TOC 740.46 26.03
5/3/93 TOC 754.12 40.11
5/3/93 TOC 767.96 14.34
5/3/93 TOC 738.87 4.58
5/3/93 TOC 739.13 4.99
5/3/93 TOC 715.94 14.47
5/3/93 TOC 752.36 15.00
5/3/93 TOC 720.77 8.76
5/3/93 TOC 749.47 13.69
5/3/93 TOC 767.82 17.55
5/3/93 TOC 715.50 9.94
5/3/93 TOC 718.54 5.79
5/3/93 TOC 711.15 4.18
5/3/93 TOC 699.48 NA'
5/4/93 TOC 708.09 4.15
5/3/93 Iron pin' 712.26 1 .77
5/3/93 Iron pin 693.90 1.88
Water Level
Elevation
1ft msll
702.99
708.37
714.43
714.01
753.62
734.29
734.14
701.4 7
737.36
712.01
735.78
750.27
705.56
712.75
706.97
NA
703.94
710.49
692.02
"ft msl -Feet, mean sea level, National Starch and Chemical Company plant vertical datum elevation 777. 79 feet msl.
• TOC -Measurement taken from top of inner well casing.
' NA -Not applicable, well is artesian.
' Measurement taken from top of iron pin next to stream.
KN/1162/WP1162. TS/06-30-93/03
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Well
NS09
NS10
NS11
NS15
Table 6
Water Level Measurements
Second Quarter 1993
Operable Unit Two
National Starch and Chemical Company,
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (ft MSL)' (ft)
5/3/93 TOCb 778.45 26.21
5/3/93 TOC 786. 72 30.60
5/3/93 TOC 775.65 15.49
5/3/93 TOC 792.60 44.36
Water Level
Elevation
(ft MSL)
752.24
756.12
760.16
748.24
• MSL -Mean sea level, National Starch and Chemical Company plant vertical datum
elevation 777. 79 feet msl.
b TOC -Measurement taken from top of inner well casing.
KN/1162/WP1162. TG/06-30-93/02
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300 0 300 600
F' Im •◄IYIQl.,c1■010»'' He■,., IN" IIIMI►' iiiiii I 14 e,l@ii IINIII mo+ iiiiiiii Oil.,
GRAPHIC
150
SCALE:
450
1 '=300'
KNOXVILLE, TENNESSEE
THIS DRAWING AND ALL INF0Rt.-1A TION
THEREON IS CONFIDENTIAL AND MUST
NOT BE MADE PUBLIC OR COPIED UNLESS
DULY AUTHORIZED, SHALL NOT BE USED
EXCEPT FOR THE PURPOSE FOR WHICH
IT W/JS SUPPLIED, HID IS SUBJECT TO
RETURN UPON DEMAND. ALL RIGHTS OF
INVENTION OR DESIGN ARE RESERVED.
I
'
[]
REVISION DESCRIP.TION
LEGEND
@ EXISTING PIEZOMETER
~ EXISTING BEDROCK MONITORING WELL
l@I EXISTING BEDROCK EXTRACTION WELL
l@I EXISTING SAPROLITE (SHALLOW)
MONITORING WELL
[Eil PROPOSED EXTRACTION WELLS
FIGURE 1
SITE MAP
CHECKED=
APPROVED1
DRAWING NO:
FIGURE 1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
PO 4
®
300 0 300 600
l'"w111n•1 ■• fFIBOfiii PE EFPi@iililfRIMl,;a Ci I Fi¥ ,
150 450
GRAPHIC SCALE: 1 '=300'
I
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I I I
I ... =•:/
/ / I
I / \\
. I I
I I I
I I I I I I ,--) 1 f
.0 I I I / ,~ / : l ' I I I I I I ' I J I l ' \l NS15/ / \ \ ~/ l \ 1 74Bf24 / l
I I I I I I
I I I
I I I I I
I // I
I I I I I I I I I
I I I I I I
I I I I
I ~: I
,✓-
I
\
__ ,... t\ ,,~
' \\\ r5
KNOXVILLE, TENNESSEE
. II
Ill
LEGEND
® EXISTING PIEZOMETER
EXISTING BEDROCK MONITORING WELL
EXISTING BEDROCK EXTRACTION WELL
l@I EXISTING SAPROLITE (SHALLOW)
MONITORING WELL
Cf§] PROPOSED EXTRACTION WELLS
·-749.15-WATER SURFACE ELEVATION
(MSU AND CONTOUR <DASHED
WHERE INFERRED)
NOTES
1. WATER LEVEL FOR NS32
WAS NOT MEASURED DUE
TO ARTESIAN CONDITIONS.
FIGURE 2 CHECKED:
04/06/93
THIS DRAWING AND ALL INFORMATION
THEREON JS CONFIDENTIAL Nm MUST
NOT BE MADE PUBLIC OR COPIED UNLESS
DULY AUTHORIZED, SHALL NOT BE USED
EXCEPT FOR THE PURPOSE FOR WHICH
WATER LEVEL CONTOUR MAP
FOR BEDROCK WATER LEVELS APPROVED:
IT WJ,,S SUPPLIED, AND IS SUBJECT TO
RETURN UPON DEM.AND. ALL RIGHTS OF
INVENTION OR DESIGN ME RESERVED.
..... """' ..... "'"""""""""'M""""A_Y'--3=--19=9_3 ________ DRAWING NO•
R VISION ESCRlPTION
OPERABLE UNITS ONE AND TWO FIGURE 2
I
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I
I Appendix A
I
I
Certificates of Analysis
I
I
I
I
I
I
I
I KN/I 162M'Pl 162.TXT,07-12-93/04
0
0
D
[D INTERNATIONAL
TECHNOLOGY
CORPORATION
ANALYTICAL
SERVICES
CERTIFICATE OF ANALYSIS
E IT Corporation July I, 1993
3 I 2 Directors Drive
II Knoxville, TN 37923
II.I Attn: Mike Sturdevant
I Job Number: ITEK 54029 P.O. Number: 408668.009.60
I
This is the Certificate of Analysis for the following samples:
Client Project ID:
I
Date Received by Lab:
Number of Samples:
Sample Type:
I I. Introduction
National Starch
05/06/93
Nine (9)
Water -seven (7), Trip Blanks -two (2)
I On 05/06/93, seven (7) water samples and two (2) trip blanks arrived at the ITAS-Knoxville, Tennessee,
laboratory from IT Corporation, Knoxville, Tennessee, in support of the National Starch project. The list
of analytical tests performed, as well as date of receipt and analysis, can be found in the attached report.
I II. Analytical Results/Methodology
I The analytical results for this report are presented by analytical test. Each set of data will include sample
identification information and the analytical results. Please note that the data are not blank corrected.
I The samples were analyzed for Target Compound List (TCL) volatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
I
I
I
I
I
I
The samples were analyzed for Target Compound List (TCL) semivolatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
Reviewed and Approved:
Alyce l Moore
Laboratory Manager
American Council ot Independent Laboratories
International Assoc,ation ol Environmental Testing Laboratories
American Assoc1ation tor Laboratory Accred1tallon
IT Analytical Services, 5815 Middlebrook Pike, Knoxville. TN 37921 681-1-89
E IT Corporation
July I, 1993
I
I
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE. TN
Client Project ID: National Starch Job Number: ITEK 54029
II. Analytical Results/Methodology (continued)
I The samples were analyzed for Target Analyte List (TAL) metals by cold vapor atomic absorption
spectroscopy (CV AA), graphite furnace atomic absorption spectroscopy (GFAA), and inductively coupled I plasma spectroscopy (ICP) in accordance with the EPA CLP II.MO! Statement of Work.
The samples were analyzed for chloride based on EPA method 325.3.
I The total dissolved solids (TDS) content of the samples was determined using EPA method 160.1.
I Chemical oxygen demand (COD) was measured using the EPA approved HACH procedure, HACH Water
Analysis Handbook, HACH Chemical Company, 1980.
I The samples were analyzed for total Kjeldahl nitrogen (TKN) based on EPA method 351.3.
1 m. Quality Control
The volatiles analyses were performed by purge and trap with a J&W DB-624 megabore column on a
I Finnigan INCOS GC/MS/DS unit. The sample analyses went well. The twenty-fold dilution of EX-03-
5/93 was eight days past sample holding time. The data compared well, and the analyses were considered
reliable. Matrix interferences were observed using the method primary and secondary mass ions in the
I calculation of the surrogate 1,2-dichloroethane-d4 for samples NS-15-5/93, NS-09-5/93 and NS-10-5/93.
Another ion, mass 67, was used successfully in quantifying recoveries of this surrogate. There were no
problems seen in final data review.
I The semivolatiles analyses were performed by direct injection of sample extract on a Restek XTI-5
capillary column on a Finnigan 4500 GC/MS/DS unit. The sample analyses met with some difficulties.
I The surrogate recoveries for samples NS-09-5/93, NS-10-5/93, NS-15-5/93 and EX-04-5/93 were very
poor. This appears to be sample matrix related as there were heavy emulsions noted during separatory
funnel extractions. There was insufficient sample for reanalysis and confirmation for these samples. The
I organic background in these samples appears to be long chain alkanes and long chain organic acids. There
were no other problems seen in final data review.
I
I
I
I
I
2
68:.'·1·89
I IT Corporation
July 1, 1993
I
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE. TN
Client Project ID: National Starch Job Number: ITEK 54029
I
III. Quality Control (continued)
I Data were reported with qualifiers as follows:
Compound was analyzed for but not detected; value given is quantification limit.
Compound exceeded calibration range.
Compound analyzed at secondary dilution.
Compound detected but below quantification limit; value estimated.
Compound found in method blank.
Spiked compound.
Suspected aldol condensation product.
Indistinguishable isomer in tentatively identified compounds.
The samples were digested on 05/19/93 for ICP and 05/19/93 for GFAA. The samples for mercury
analysis were prepared just prior to analysis. The CV AA analysis for mercury was performed on
I 05/25/93; the GFAA analyses for arsenic, lead, selenium and thallium were performed on 06/11 -
06/17 /93; the remaining metals were analyzed by ICP on 06/02/93. All run QC was acceptable. No
problems were encountered.
I Data were reported with qualifiers as follows:
I "C" Qualifiers
U Compound was analyzed for but not detected. The number is the detection limit for the sample. I B Value greater than instrument detection limit, but less than contract required quantitation limit.
"O" Qualifiers
Duplicate analysis outside control limits.
Spiked sample recovery outside control limits.
Post-digestion spike for GFAA was out of control limits (85-115 %), while sample absorbance was
less than 50 % of spike absorbance.
I
I
I
I
I
s The reported value was determined by method of standard additions.
3
682·1·89
I IT Corporation
July 1, 1993
I
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE. TN
I
Client Project ID: National Starch Job Number: ITEK 54029
ill. Quality Control (continued)
I
"M" Qualifiers
I p
V I F
C
Analysis performed by ICP.
Analysis performed by CV AA.
Analysis performed by GFAA.
Cyanide analysis by manual distillation/colorimetric determination.
I Miscellaneous
I ~
NR-
1 G -
X -
Duplicate.
Spike.
Not required.
Native analyte > 4 times spike added, therefore, acceptance criteria do not apply.
Detection limits higher than normal due to sample matrix interferences.
I The samples were analyzed for chloride using the mercuric nitrate titrimetric procedure with HACH
reagents. No problems were encountered.
I The TDS content of the samples was determined gravimetrically by filtration and evaporation of the filtrate
to a constant weight at 180°C. No problems were encountered.
I The COD of the samples was measured using the reactor digestion method followed by titration with
ferrous ammonium sulfate. No problems were encountered.
I
I
The samples were prepared for TKN analysis by acid digestion/distillation using a micro-Kjeldahl system.
The distillate was analyzed by Nesslerization using HACH reagents. No problems were encountered.
I
I
I
I
I
4
682-1-89
I m INTERNATIONAL II TECHNOLOGY I] CORPORATION
I
ANALYTICAL
SERVICES
CERTIFICATE OF ANALYSIS
I IT Corporation July I, 1993
312 Directors Drive
I Knoxville, TN 37923
Attn: Mike Sturdevant
I Job Number: ITEK 54011 P.O. Number: 408668
This is the Certificate of Analysis for the following samples:
I Client Project ID: National Starch
Date Received by Lab: 05/05/93 I Number of Samples: Eight (8)
Sample Type: Water -six (6), Trip Blank -two (2)
I I. Introduction
I On 05/05/93, six (6) water samples and two (2) trip blanks arrived at the ITAS-Knoxville, Tennessee,
laboratory from IT Corporation, Knoxville, Tennessee, in support of the National Starch project. The list
of analytical tests performed, as well as date of receipt and analysis, can be found in the attached report.
I II. Analytical Results/Methodology
I The analytical results for this report are presented by analytical test. Each set of data will include sample
identification information and the analytical results. Please note that the data are not blank corrected.
I The samples were analyzed for Target Compound List (TCL) volatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
I The samples were analyzed for Target Compound List (TCL) semivolatiles by gas chromatography/mass
spectroscopy (GC/MS) in accordance with the EPA CLP 2/88 Statement of Work.
I ReviYJ~ and Approved:
I w~ C//~,,
Alyce ~oore
1 Laboratory Manager
I
I
American Council ol Independent Laboratories
!nlerna!ional Associalion ot Environmental Testing Laboratories
P•,.rnencan Assoc1otion tor Laboratory Accreditat1on
IT Analytical Services. 5815 Middleb1ook Pike, Knoxville, TN 37921 681·1·89
m
IT Corporation E July 1, 1993
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE. TN
Client Project ID: National Starch Job Number: ITEK 5401 I
I
II. Analytical Results/Methodology (continued)
I The samples were analyzed for Target Analyte List (T AL) metals by cold vapor atomic absorption
spectroscopy (CV AA), graphite furnace atomic absorption spectroscopy (GFAA), and inductively coupled I plasma spectroscopy (ICP) in accordance with the EPA CLP ILMOI Statement of Work.
The samples were analyzed for chloride based on EPA method 325.3.
I The total dissolved solids (TDS) content of the samples was determined using EPA method 160. J.
I Chemical oxygen demand (COD) was measured using the EPA approved HACH procedure. HACH Water
Analysis Handbook, HACH Chemical Company, 1980.
I The samples were analyzed for total Kjeldahl nitrogen (TKN) based on EPA method 351.3.
I III. Quality Control
I The volatiles analyses were performed by purge and trap with a J&W DB-624 megabore column on
. Finnigan IN COS and OW A GC/MS/DS units. The sample analyses generally went well. Both of the trip
blanks were received with headspace, and acetone was seen at levels greater than typical background. EX-
1,. 02-5/93 required dilutions for acetone, 1,2-dichloroethane, and 1,2-dichloropropane. l ,2-Dichloroethane-
d4 was successfully integrated with a compliant recovery in the undiluted analysis of EX-02-5/93 using
mass 104. Manual integration with this mass was necessary due to sample matrix interferences with the
I primary and secondary mass ions. The final dilution concentration of 1,2-dichloropropane was below the
practical quantification limit, but considering its close agreement with the mid-level dilution, the value was
considered reliable. There were no other problems seen in final data review.
I The semivolatiles analyses were performed by direct injection of sample extract on a Restek XTI-5
capillary column on a Finnigan 4500 GC/MS/DS unit. The sample analyses went well. Two analyses had
I one low surrogate recovery each, but the recoveries were greater than ten percent, and overall all analyses
met CLP QC criteria. The MS/MSD had one low spike recovery and two RPDs outside advised limits.
These appear to be a function of matrix. EX-02-5/93 required dilution for bis (2-chloroethyl) ether. There I were no problems seen in final data review.
I
I
I 2
I IT Corporation I July I, 1993
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVIU.E. TN
I
i
Client Project ID: National Starch Job Number: ITEK 54011
m. Quality Control (continued)
Data were reported with qualifiers as follows:
A
Compound analyzed for but not detected; value given is quantification limit.
Compound exceeded calibration range.
Compound analyzed at secondary dilution.
Compound detected but below quantification limit; value estimated.
Compound found in method blank.
Suspected aldol condensation product.
Indistinguishable isomer in tentatively identified compounds.
The samples were digested on 05/18/93 for ICP and for GFAA. The samples for mercury analysis were
prepared just prior to analysis. The CV AA analysis for mercury was performed on 05/25/93; the GFAA
analyses for arsenic, lead, selenium, and thallium were performed on·06/11 -06/16/93; the remaining
metals were analyzed by ICP on 06/01/93. All run QC was acceptable. A duplicate/spike pair was
prepared using sample number EX-02-5/93. Spike recovery (accuracy) results were within acceptance
limits for all parameters by ICP, GFAA, and CV AA analyses except for cadmium by ICP analysis and
arsenic by GFAA analysis. Both analytes were slightly outside acceptance limits (73.1 % and 72.4%, I respectively). Duplicate RFD (precision) results were within acceptance limits for all parameters by ICP,
GFAA and CV AA analyses except for thallium by ICP analysis. As thallium is reported by GFAA
I. analysis, this does not adversely affect the data. Selenium was spiked at 10 x CLP required spiking level
during sample digestion. No other problems were encountered .
. , Data were reported with qualifiers as follows:
"C" Qualifiers
"Q" Qualifiers
*
Compound was analyzed for but not detected. The number is the detection limit for the
sample.
Value greater than instrument detection limit, but less than contract required quantitation
limit.
Duplicate analysis outside control limits.
Spiked sample recovery outside control limits.
Post-digestion spike for GFAA was out of control limits (85-115 % ), while sample
absorbance was less than 50 % of spike absorbance.
The reported value was determined by method of standard additions.
3
I IT Corporation
• July I, 1993
IT ANALYTICAL SERVICES
5815 MIDDLEBROOK PIKE
KNOXVILLE, TN
I
Client Project ID: National Starch
ill. Quality Control (continued)
"M" Qualifiers
Analysis performed by ICP.
Analysis performed by CV AA.
Analysis performed by GFAA.
Cyanide analysis by manual distillation/colorimetric determination.
Job Number: ITEK 54011
I Miscellaneous
Duplicate.
Spike.
Not required.
Native analyte > 4 times spike added, therefore, acceptance criteria do not apply.
Detection limits higher than normal due to sample matrix interferences.
The samples were analyzed for chloride using the mercuric nitrate titrimetric procedure with HACH I, reagents. No problems were encountered.
I
I
I,
I
·1
I
I
' I
The ms content of the samples was determined gravimetrically by filtration and evaporation of the filtrate
to a constant weight at 180°C. No problems were encountered.
The COD of the samples was measured using the reactor digestion method followed by titration with
ferrous ammonium sulfate. No problems were encountered.
The samples were prepared for TKN analysis by acid digestion/distillation using a micro-Kjeldahl system.
The distillate was analyzed by Nesslerization using HACH reagents. No problems were encountered.
4
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. 2 j
,. Lab Name: ITAS-KNOXVILLE Contract: EX01593
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No.: EX0159
.Matrix: (soil/water) WATER Lab Sample ID: ~X~X=3=3~4~7 ___ _
Sample
I Level:
wt/vol:
(low/med)
5.0
LOW
(g/mL) !11.__ Lab File ID: XX3347
Date Received: 05/06/93 1% Moisture: not dee. Date Analyzed: 05/14/93
I
I
I
I
I
I
I
I
I
I
I
Column: (pack/cap) ~C=A=P __ Dilution Factor: 1.0 ~~--
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5------~--l,l,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
1 J
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
10 u
5 u
4 J
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
438
lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX01593
Name: ITAS-KNOXVILLE Contract: .Lab
Lab Code: ITSTU Case No.: 54029
WATER
SAS No.: NA SDG No.: EX0lS
'Matrix: (soil/water)
Sample wt/vol: 1000
(low/med) LOW ='--'-----
(g/mL) ML
% Moisture:
,.Extraction:
not dee. dee.
SEPF
=-----
Lab Sample ID: XX3356
Lab File ID: XX3356
Date Received: 05/06/93
Date Extracted: 05/11/93
Date Analyzed: 05/25/93
IGPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) N pH: Dilution Factor: 1.0
I
I
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I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
111-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-6.0-1-- - - - - --bis (2-Chloroisopropyl) Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
111-91-1--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
10 u
4 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u so u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u so u
10 u so u
10 u
10 u
10 u
1/87 Rev.
439
lC EPA SAMPLE NO.
It SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX01593
Name: ITAS-KNOXVILLE Contract: Lab
I Lab Code: ITSTU Case No.: 54029
WATER
SAS No. : :..:N=-=A'----SDG No. : EX015
'
Matrix: (soil/water)
Sample wt/vol: I Level: (low/med)
% Moisture: not dee.
1000 (g/mL) ML
LOW
dee. I Extraction: (SepF/Cont/Sonc) SEPF
Lab Sample ID: XX3356
Lab File ID: XX3356
Date Received: 05/06/93
Date Extracted: 05/11/93
Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
I
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I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)--
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' ' (l) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
l/87 Rev.
If
I
Lab
m Lab
Name: ITAS KNOXVILLE
U.S. EPA -CLP
1 INORGANIC ANALYSES DATA SHEET
------
Code: ITSTU Case No.: 54029
Contract: NAT. STARC
SAS No.:
EPA SAMPLE NO.
EX-01-5/93
SDG No.: EX-02
Matrix (soil/water): WATER m Level (low/med): LOW
Lab Sample ID: XX3375
Date Received: 05/06/93
% Solids: o.o I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
' I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2 7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
'lcolor Before: COLORLESS
Color After: COLORLESS
lcomments:
I
I
I.
I
I
Analyte Concentration c Q
Aluminum 40.0 U
Antimony-30.0 U Arsenic ------2.0 U
Barium -5. 3 B
Beryllium 1.0 U
Cadmium 5.0 U
Calcium-44200
Chromium 10.0 U __ _
Cobalt -20.0 U Copper--31.1 ---
Iron:_::~ 281 Lead 2. 0 U 1 ___ _
Magnesium 200
Manganese 206
Mercury .20 U __ _
Nickel -20.0 U
Potassium 1000 u
Selenium 2.0 U
Silver -5.0 U Sodium--610
Thallium 2. 0 U Vanadium-0.0 U ---
Zinc 32. 7 Cyanide _______ _
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Texture:
Artifacts:
3/90
62:
Ii 1 lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: ITAS-KNOXVILLE EX02593
Contract:
ILab Code: ITSTU
!Matrix: (soil/water)
Sample wt/vol:
Case No.: 54011 SAS No.: SDG No.: EX0259
WATER Lab Sample ID: XX3173
5.0 (g/mL) fil,_ Lab File ID: XX3173
.Level: (low/med) LOW Date Received: 05/05/93
% Moisture: not dee.
l:olumn: (pack/cap) CAP
Date Analyzed: 05/13/93
Dilution Factor: ~1~-~o'---
I
I
I
I
I
I
I
·a
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane 10 74-83-9---------Bromomethane 10 75-01-4---------Vinyl Chloride 10 75-00-3---------Chloroethane 10 75-09-2---------Methylene Chloride 4 67-64-1---------Acetone 36000 75-15-0---------carbon Disulfide gq " 75-35-4---------1,1-Dichloroethene 5 75-34-3---------1,1-Dichloroethane 5 540-59-0--------1,2-Dichloroethene(Total) __ 5 67-66-3---------Chloroform 5 107-06-2--------1,2-Dichloroethane 460 78-93-3---------2-Butanone 2" ;i,e 71-55-6---------1,1,1-Trichloroethane 5 56-23-5---------carbon Tetrachloride 5 108-05-4--------Vinyl Acetate 10 75-27-4-------~-Bromodichloromethane 5 78-87-5---------1,2-Dichloropropane 920 10061-01-5------cis-l,3-Dichloropropene 5 79-01-6---------Trichloroethene 5 124-48-1--------Dibromochloromethane 5 79-00-5---------1,1,2-Trichloroethane 5 71-43-2---------Benzene 5 10061-02-6------trans-1,3-Dichloropropene __ 5 75-25-2---------Bromoform 5 108-10-1--------4-Methyl-2-Pentanone 10 591-78-6--------2-Hexanone 10 127-18-4--------Tetrachloroethene 5 79-34-5---------1 1 2 2-Tetrachloroethane 5 , , , --108-88-3--------Toluene 110 108-90-7--------Chlorobenzene 5 100-41-4--------Ethylbenzene 9 100-42-5--------styrene 5 1330-20-7-------Xylene (total) 38
FORM I VOA
Q
u
u
u
u
J
E
J,!
u
u
u
u
E
-<:I-
u
u
u
u
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u
u
u
u
u
u
u
u
u
u
u
u
u
~1,1
1/87 Revc;;
48
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX02593DL2 Lab Name: ITAS-KNOXVILLE Contract: I Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX0259
m Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) !11_
Lab Sample ID: ~X~X=3~1~7~3 ___ _
Lab File ID: XX3173D2 I Level: ( low/med) LOW Date Received: 05/05/93
% Moisture: not dee. Date Analyzed: 05/14/93
m Column:
m
I
I
I
I
I
I
I
I
I
I
(pack/cap) CAP Dilution Factor: 4.0 ~~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chlorornethane 40
74-83-9---------Bromomethane 40 75-01-4---------Vinyl Chloride 40
75-00-3---------Chloroethane 19
75-09-2---------Methylene Chloride 24 67-64-1---------Acetone 26000 75-15-0---------Carbon Disulfide 48
75-35-4---------1,1-Dichloroethene 20 75-34-3---------1,1-Dichloroethane 20
540-59-0--------1,2-Dichloroethene(Total) __ 20 67-66-3---------Chloroforrn 20
107-06-2--------1,2-Dichloroethane 470
78-93-3---------2-Butanone 40
71-55-6---------1,1,1-Trichloroethane 20
56-23-5---------carbon Tetrachloride 20
108-05-4--------Vinyl Acetate 40
75-27-4---------Brornodichlorornethane 20
78-87-5---------1,2-Dichloropropane 820
10061-01-5------cis-l,3-Dichloropropene 20
79-01-6---------Trichloroethene 20
124-48-1--------Dibromochloromethane 20
79-00-5---------1,1,2-Trichloroethane 20
71-43-2---------Benzene 20
10061-02-6------trans-l,3-Dichloropropene __ 20
75-25-2---------Brornoforrn 20
108-10-1--------4-Methyl-2-Pentanone 40
591-78-6--------2-Hexanone 40
127-18-4--------Tetrachloroethene 20
79-34-5---------1,1,2,2-Tetrachloroethane __ 20
108-88-3--------Toluene 160
108-90-7--------Chlorobenzene 20
100-41-4--------Ethylbenzene 7
100-42-5--------styrene 20
1330-20-7-------Xylene (total) 30
FORM I VOA
Q
u
u
u
DJ
D
DE
D
u
u
u
u
D
D
u
u
u
u
DE
u
u
u
u
u
u
u
u
u
u
u
D
u
DJ
u
D
1/87 Rev ..
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA
7b
SAMPLE NO. 7
Name: ITAS-KNOXVILLE Contract: Lab
m Lab Code: ITSTU Case No.: 54011 SAS No.:
.Matrix: (soil/water)
· Sample wt/vol:
WATER
5.0
m Level: (low/med) LOW
% Moisture: not dee .
• Column: (pack/cap) CAP
(g/mL) M1_
EX02593DL
SDG No.: EX0259
Lab Sample ID: XX3173
Lab File ID: XX3173DL
Date Received: 05/05/93
Date Analyzed: 05/14/93
Dilution Factor: =2=5=0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
11
I
I
I
'I
I
I
I
I
I
I
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
2500 u
2500 u
2500 u
2500 u
820 DJ
29000 D
1200 u
1200 u
1200 u
1200 u
1200 u
460 DJ
2500 u
1200 u
1200 u
2500 u
1200 u
820 DJ
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
2500 u
2500 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1200 u
1/87 Rev.
I
I
lB 329 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX02593
Lab Name: ITAS-KNOXVILLE Contract: I Lab Code: IT STU
Matrix: (soil/water) I Sample wt/vol:
Case No.: 54011
WATER
SAS No . : :.:N::..:Ac..._ __ SDG No.: EX025
Lab Sample ID: XX3183
960 (g/mL) ML Lab File ID: XX3183
Level: (low/med) LOW Date Received: 05/05/93
11% Moisture: not dee. dee. Date Extracted: 05/10/93 I Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
E
E
I
• I
'I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
111-91-1--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
70
340 E
10 u
10 u
10 u
10 u
10 u
10 u
10 u
14
10 u
10 u
10 u
10 u
10 u
10 u
18 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
52 u
10 u
52 u
10 u
10 u
10 u
1/87 Rev.
33C lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE Contract:
EX02593
I Lab Code: ITSTU Case No.: 54011 SAS No.: NA SDG No.: EX025 ----
Matrix: (soil/water) WATER Lab Sample ID: XX3183
lsample wt/vol: 960 (g/mL) ML Lab File ID: XX3183
-Level: (low/med) LOW Date Received: 05/05/93 .% Moisture: not dee. dee. Date Extracted: 05/10/93
.Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
•
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' ' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
52 u
10 u
52 u
52 u
10 u
10 u
10 u
10 u
10 u
52 u
52 u
10 u
10 u
10 u
52 u
10 u
10 u
10 u
10 u
10 u
10 u
21 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1/87 Rev.
lB
~sl/ 3
EPA SAMPLE NO. 5
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX02593DL
Name: ITAS-KNOXVILLE Contract:
Code: ITSTU Case No.: 54011
WATER
SAS No . : :.:N:.:Ac...._ __ SDG No.: EX025
(atrix: (soil/water)
Sample wt/vol:
.Level: (low/med)
960
LOW
Lab
(g/mL) ML Lab
Date
Sample ID: XX3183D
File ID: XX3183D
Received: 05/05/93
% Moisture: not dee. dee. Date Extracted: 05/10/93
f:xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/26/93
GPC Cleanup: (Y/N) N pH:
I
Dilution Factor:
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol 64
111-44-4--------bis(2-Chloroethyl)Ether 380
95-57-8---------2-Chlorophenol 21
541-73-1--------1,3-Dichlorobenzene 21
106-46-7--------1,4-Dichlorobenzene 21
100-51-6--------Benzyl Alcohol 21
95-50-1---------1,2-Dichlorobenzene 21
95-48-7---------2-Methylphenol 21
108-60-1--------bis(2-Chloroisopropyl)Ether 21
106-44-5--------4-Methylphenol -12
621-64-7--------N-Nitroso-Di-n-Propylamine 21
67-72-1---------Hexachloroethane --21
98-95-3---------Nitrobenzene 21
78-59-1---------Isophorone 21
88-75-5---------2-Nitrophenol 21
105-67-9--------2,4-Dimethylphenol 21
65-85-0---------Benzoic Acid 8
111-91-1--------bis(2-Chloroethoxy)Methane 21
120-83-2--------2,4-Dichlorophenol --21
120-82-1--------1,2,4-Trichlorobenzene 21
91-20-3---------Naphthalene 21
106-47-8--------4-Chloroaniline 21
87-68-3---------Hexachlorobutadiene 21
59-50-7---------4-Chloro-3-Methylphenol 21
91-57-6---------2-Methylnaphthalene 21
77-47-4---------Hexachlorocyclopentadiene __ 21
88-06-2---------2,4,6-Trichlorophenol 21
95-95-4---------2,4,5-Trichlorophenol 100
91-58-7---------2-Chloronaphthalene 21
88-74-4---------2-Nitroaniline 100
131-11-3--------Dimethyl Phthalate 21
208-96-8--------Acenaphthylene 21
606-20-2--------2,6-Dinitrotoluene 21
FORM I SV-1
2.0
Q
D
D
u
u
u
u
u u
u
DJ
u
u u
u u
u
DJ
u u
u
u
u
u
u
u u
u
u u u u
u
u
1/87 Rev.
I lC EPA
;;3SS'
SAMPLE N0~5
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX02593DL Name: ITAS-KNOXVILLE Contract: Lab
m Lab Code: ITSTU Case No.: 54011
WATER
SAS No.: NA ='----SDG No. : EX025
It Matrix: (soil/water)
II Sample wt/vol:
• Level: (low/med)
960
LOW
Lab
(g/mL) ML Lab
Date
Sample ID: XX3183D
File ID:. XX3183D
Received: 05/05/93
% Moisture: not dee. dee. Date Extracted: 05/10/93 I Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/26/93
I
I
I
I
I
I
I
I
I
I
I
I
I
GPC Cleanup: (Y/N) N pH: Dilution Factor:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
99-09-2---------3-Nitroaniline --------83-32-9---------Acenaphthene. ________ _
51-28-5---------2,4-Dinitrophenol _____ _
100-02-7--------4-Nitrophenol. _______ _
132-64-9--------Dibenzofuran. ________ _
121-14-2--------2,4-Dinitrotoluene ------84-66-2---------Diethylphthalate ______ _
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene.~~-------~~~
100-01-6--------4-Nitroaniline ·--------534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)--
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene ------87-86-5---------Pentachlorophenol _____ _
85-01-8---------Phenanthrene
120-12-7--------Anthracene ---------
84-74-2---------Di-n-Butylphthalate ____ _
206-44-0--------Fluoranthene
129-00-0--------Pyrene ---------
85-68-7---------Butylb_e_n_z_y~l-p~h-t~h-a~l-a_t_e ____ _
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene ----------218-01-9--------Chrysene __________ _
117-81-7--------bis(2-Ethylhexyl)Phthaiate
117-84-0--------Di-n-Octyl Phthalate ___ ===
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene -----
-----50-32-8---------Benzo(a)Pyrene _______ _
193-39-5--------Indeno(l,2,3-cd)Pyrene ----53-70-3-------~-Dibenz(a,h)Anthracene ___ _
191-24-2--------Benzo(g,h,i)Perylene ____ _
(1) -Cannot be separated from Diphenylamine
FORM I SV-2
UG/L
100
21
100
100
21
21
21
21
21
100
100
21
21
21
100
21
21
21
21
21
21
42
21
21
21
21
21
21
21
21
21
21
2.0
u u
u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
Q
1/87 Rev.
U.S. EPA -CLP
1 EPA SAMPLE NO.
D
I INORGANIC ANALYSES DATA SHEET
.Lab Name: ITAS_KNOXVILLE______ Contract: NAT._STARC EX-02-5/93
Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX-02-
.Matrix (soil/water): ·WATER Lab Sample ID: XX3198
Level (low/med): LOW Date Received: 05/05/93 .% Solids: o.o
Concentration Units (ug/L or mg/kg dry weight): UG/L I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
color Before: BLACK __
lolor After: COLORLESS
'Comments:
I
I
I
I
Analyte Concentration C Q
Aluminum 40.0 u Antimony-30.0 u Arsenic -2.0 u _N_ Barium -1250 Berylliuiii 1.0 u Cadmium 5.0 u _N __ Calcium-:!27000 Chromium-12.8 -
Cobalt -20.0 u Copper--56.9 Iron --2570 -
Lead 2.0 u w Magnesium 5:!100 ---
Manganese 7180 -
Mercury 0.20 u Nickel -75.5 Potassiuiii 2330 n Selenium_ 2.0 u w Silver 5.0 u ---
Sodium--55100 Thalliuin 2.0 u w Vanadium: 10.0 u ---
Zinc 15.4 B Cyanide_ --
Clarity Before: CLOUDY
Clarity After: CLOUDY
FORM I -IN
M
i:r p-
F p-
p p-
p-
p-
p-
p-
p-
F-p-
p-
c'J p
p-
F-p-
p-
F-
p-
p-
N~
-
Texture:
Artifacts:
3/90
D SENT BY:
I
lf'ab Name: ITAS_KNOXVILLE
6-21-93 ; I :45PM ; ITAS-KNOXVILI..E/ MBRK-<
U.S. EPA -CLP
6
DUPLICATES
ilr,ab Code: ITSTU_ Case No.: 54011
Contract: NAT._STARC
SAS No.:
EPA SAMPLE NO.
EX-02-5/930
SDG No.: EX-02-
lf'□trix {soil/water):
~ Solids for Sample:
WATER
0.0
Level {low/med): _LOW_
\ Solids for Duplicate: _o.o
I
I
I
I
I
I
I
I
I
I
I
Concentration units (ug/L or mg/kg dry weight): UG/L_
Control )l.i(.~~q-'D
Analyte Limit Sample ( S) C Duplicate ( D) C RPD
Aluminum 40.0uuu u 40.0uuu(U Antimony-30.0000 u 30-0000 u Arsenic -10.0 40 ,,0000 u 40.0000 u Barium ----1254. 6400 1261. 7800 0.6 Berylliurii 1.0000 u 1.0000 u --
Cadmium 5.0 5.0000 u 5.0000 u Calcium -326587.8900 324996.1200 0.5 Chromium 10.0 --12,7500 ---12,8900 --l. l -
Cobalt ---20.0000 u 20.0000 u ---
Copper--25.0 56.8800 57.5300 1.1 Iron ----2570. 0700 -2570.5500 --0.0 -
Lead 40.0000 tJ' 40.0000 tJ' ---
Magnesium 53107.5200 53354.5900 0.5 Manganese --7177.7700 ---7165.4100 --o. 2: Mercury 0.2 0.2000 0 0.2000 u --
Nickel -40.0-15.5300 69.9900 I • 6 Potassium --2330.8500 !J 2390.1400 B =2.s: Selenium 60.0000 u 60.0000 u Silver -5.0000 u 5,0000 u Sodium -55093.9100 55572,4400 0.9 Thallium_ 10.0 --40.0000 tJ' --57.0000 -~o.o: Vanadium ---10.0000 u 10.0000 u Zinc -15,4400 B 16.3700 B 5.8 Cyanide_ -------
FORM VI -IN
Q M
-I' -p -p -p -p -p -p -p -p -p -p -p -p -p -C v -p -p -p -p -p -. p
p -p -N --
J/90
D SENT BY:
E
IILab Name: ITAS_KNOXVILLE
6-21-33 ; l :46PM ; ITAS-KNOXVIU£/ MBRK~
U.S. EPA -CLP
6 DUPLICATES
If Lab Code: ITSTU Case No.: 54011
Contract: NAT._STARC
SAS No.:
615-531-7335:.12
EPA SAMPLF. NO.
EX-02-5/93D
SDG No.; EX-02-
IIMatrix (soil/water):
Iii Solids for Sample:
WATER
_o.o
Level (low/med):
% Solids for Duplicate:
LOW --
o.o
I
I
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
Control ali 31"1'1-D
Analyte Limit Sample (S) C Duplicate ( D) C RPO
Aluminum -·
Antimony---
Arsenic -2.0000 u 2.0000 0 Barium -
BeryllTiiiii -

-
Cadmium --
Calcium-----Chromium --
Cobalt --

-
Copper-·---
Iron ---
Lead 2.0000 U· 2.0000 u Magnesium
Hangane:,e --Mercury --
Nickel ---
Potassiuiii -

-
Selenium 2.0000 u 2.0000 u Silver ----
Sodium ---
Thallium 2.0000 u 2.0000 0 Vanadium
Zinc ---
Cyam.ae_ ------
FORM VI -IN
Q M
-NR -NR -F -NR -NR -NR -NR -NR -NR -NR -NR -F -NR -NR -NR -NR -NR -F -NR -NR -F -NR -NR -NR ---
3/90
D
E
E
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~-;,,
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
EX03593
Lab Name: ITAS-KNOXVILLE Contract:
Lab Code: IT STU case No.: 54029 SAS No.: SDG No.: EX0159
Matrix: (soil/water) WATER Lab Sample ID: ~X~X~3~3~4~9 ___ _
Sample wt/vol: 5.0 ( g/mL) !11_ Lab File ID: XX3349
Level: (low/med) LOW Date Received: 05/06/93
% Moisture: not dee. Date Analyzed: 05/14/93
Column: (pack/cap) CAP Dilution Factor: 1.0 ~-"---
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
10
10
10
10
2
67-64-1---------Acetone 1900
75-15-0---------carbon Disulfide 16
75-35-4---------1,1-Dichloroethene 5
75-34-3---------1,1-Dichloroethane 5
540-59-0--------1,2-Dichloroethene {Total) 5
67-66-3---------Chloroform 5
107-06-2--------1,2-Dichloroethane 65
78-93-3---------2-Butanone ~i!I(
71-55-6---------1,1,1-Trichloroethane 5
56-23-5---------carbon Tetrachloride 5
108-05-4--------Vinyl Acetate 10
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 180
10061-01-5------cis-1,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43-2---------Benzene 5
10061-02-6------trans-1,3-Dichloropropene __ 5
75-25-2---------Bromoform 5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10
127-18-4--------Tetrachloroethene 5
79-34-5-----7---1,l,2,2-Tetrachloroethane __ 5
108-88-3--------Toluene 46
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 2
100-42-5--------Styrene 5
1330-20-7-------Xylene (total) 7
FORM I VOA
Q
u u
u
u
J
E
u u u
u
u u
u
u
u u u
u
u u u u u
u
u
u
J
u
lit
1/87 R;D.
D
u lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
61
EPA SAMPLE NO.
m Lab Name: ITAS-KNOXVILLE Contract:
EX03593DL
m
I
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I
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I
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I
Lab Code: ITSTU Case No.: 54029 SAS No. : SDG No. : EX0159
Matrix: (soil/water) WATER Lab Sample ID: XX3349
Sample wt/vol: 5.0 ( g/mL) Mk__ Lab File ID: XX3349D
Level: ( low/med) LOW Date Received: 05/06/93
% Moisture: not dee. Date Analyzed: 05/24/93
Column: (pack/cap) CAP Dilution Factor: ~2~0c_ __
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
200
200
200
200
50
67-64-1---------Acetone 2200
75-15-0---------carbon Disulfide 100
75-35-4---------1,1-Dichloroethene 100
75-34-3---------1,1-Dichloroethane 100
540-59-0--------1,2-Dichloroethene (Total) 100
67-66-3---------Chloroform 100
107-06-2--------1,2-Dichloroethane 61
78-93-3---------2-Butanone 200
71-55-6---------1,1,1-Trichloroethane 100
56-23-5---------Carbon Tetrachloride 100
108-05-4--------Vinyl Acetate 200
75-27-4---------Bromodichloromethane 100
78-87-5---------1,2-Dichloropropane 150
10061-01-5------cis-l,J-Dichloropropene 100
79-01-6---------Trichloroethene 100
124-48-1--------Dibromochloromethane 100
79-00-5---------1,1,2-Trichloroethane 100
71-43-2---------Benzene 100
10061-02-6------trans-l,J-Dichloropropene __ 100
75-25-2---------Bromoform 100
108-10-1--------4-Methyl-2-Pentanone 200
591-78-6--------2-Hexanone 200
127-18-4--------Tetrachloroethene 100
79-34-5---------1 1 2 2-Tetrachloroethane , , , --100
108-88-3--------Toluene 38
108-90-7--------Chlorobenzene 100
100-41-4--------Ethylbenzene 100
100-42-5--------styrene 100
1330-20-7-------Xylene (total) 100
FORM I VOA
Q
u
u
u
u
BDJ
D
u
u
u
u
u
DJ
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
DJ
u
u
u
u
1/87 Rev.
45: 0
u lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EX03593
Name: ITAS-KNOXVILLE Contract:
Code: ITSTU Case No.: 54029 SAS No.: NA SDG No. : EX015 ----I Matrix: (soil/water) WATER Lab Sample ID: XX3358
Sample wt/vol: 900 (g/mL) ML Lab File ID: XX3358
m Level: (low/med) LOW Date Received: 05/06/93
% Moisture: not dee. dee. Date Extracted: 05/11/93
• Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
IGPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine
67-72-1---------Hexachloroethane --
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
12
100
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
56 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
56 u
11 u
56 u
11 u
11 u
11 u
1/87 Rev.
0
0 lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
451'.
EPA SAMPLE NO.
EX03593 oLab
Lab Code: ITSTU Case No.: 54029 SAS No.: NA SDG No.: EX015
uMatrix: (soil/water) WATER
Sample wt/vol: 900 (g/mL) ML
ILevel: ( low/med) c:cL.::.OW'-'---
% Moisture:
.Extraction:
not dee. dee.
(SepF/Cont/Sonc) SEPF
----
Lab Sample ID: XX3358
Lab File ID: XX3358
Date Received: 05/06/93
Date Extracted: 05/11/93
Date Analyzed: 05/25/93
.GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
I
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I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate -.-
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' ' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
56 u
11 u
56 u
56 u
11 u
11 u
11 u
11 u
11 u
56 u
56 u
11 u
11 u
11 u
56 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
m
D
Lab 0 Lab
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
Name: ITAS KNOXVILLE _____ _ Contract: NAT. STARC
SAS No.: Code: ITSTU
EPA SAMPLE NO.
EX-03-5/93
SDG No. : EX-02
Matrix (soil/water): 0 Level ( low/med) :
Case No.: 54029
WATER
LOW
Lab Sample ID: XX3377
Date Received: 05/06/93
% Solids: 0.0
m Concentration Units (ug/L or mg/kg dry weight): UG/L_
m
E
I
I
I
I
I
lcolor Before:
•
Color After:
Comments:
I
I
I
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I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
Aluminum 4 o. 1l u Antimony-30.0 u Arsenic -2.0 u
Barium -140 B
Berylliuiii 1.0 u
Cadmium 5.0 u Calcium-H,9000 Chromium-10.0 u Cobalt 21. 3 B Copper--10.0 u Iron --7380
Lead 2.0 u
Magnesium 26600 -Manganese 2760
Mercury 0.20 u Nickel -20.0 u
Potassiuiii 1720 B
Selenium 2.0 u Silver 5.0 u Sodium--l:4400
Thallium_ 2.0 u Vanadium 10.0 u
Zinc -16.9 B
Cyanicle_ --
Clarity Before: CLOUDY
Clarity After: CLOUDY
FORM I -IN
Q M
~ p
w F ----p-
p -p -p -p p-
p-
p
F-p-
p-
c'J p p-
w F ----p -p
F-p-
p
N~
-
Texture:
Artifacts:
3/90
62i
n
0 lA EPA SAMPLE NZ.8
VOLATILE ORGANICS ANALYSIS DATA SHEET
0 Lab Name: ITAS-KNOXVILLE Contract:
EX04593
u Lab Code: ITS TU
Matrix: (soil/water) WATER
Case No.: 54029 SAS No.: SDG No.: EX0159
Lab Sample ID: ~X~X~3~3~4~8 ___ _
I Sample wt/vol: 5.0 (g/mL) !11.._ Lab File ID: XX3348
Level: ( low/med) LOW Date Received: 05/06/93 I% Moisture: not dee. Date Analyzed: 05/14/93
1 Column:
I
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I
(pack/cap) CAP Dilution Factor: =l~-~□---
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-1,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
12 7-18-4-----.---Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
Q
10 u
10 u
10 u
5 J
2 J
10 u
5 u
5 u
5 u
5 u
5 u
3 J
10 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
2 J
2 J
5 u
5 u
l J
1IR7 Rev.
0 lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO. 4 7
EX04593
ITAS-KNOXVILLE Contract: rab Name:
Lab Code: ITSTU Case No.: 54029
WATER
SAS No.: NA SDG No. : EX015
ltatrix: (soil/water)
Sample wt/vol: 930 (g/mL) ML
l}:.evel: (low/med) LOW
% Moisture:
lkxtraction:
---
not dee. dee.
(SepF/Cont/Sonc) SEPF
----
Lab Sample ID: XX3357
Lab File ID: XX3357
Date Received: 05/06/93
Date Extracted: 05/11/93
Date Analyzed: 05/25/93
Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
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I
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I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether
106-44-5--------4-Methylphenol -
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
111-9l-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
11 u
5 J
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
54 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
54 u
11 u
54 u
11 u
11 u
11 u
1/87 Rev.
n lC 4 7= EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
0 EX04593
Lab Name: ITAS-KNOXVILLE Contract:
D Lab Code: ITSTU Case No.: 54029 SAS No.: NA SDG No. : EX015 ----
Matrix: (soil/water) WATER Lab Sample ID: XX3357 I Sample wt/vol: 930 (g/mL) ML Lab File ID: XX3357
Level: (low/med) =L~OW.:..;__
I% Moisture: not dee. dee.
Date Received: 05/06/93
Date Extracted: 05/11/93
(SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93 I Extraction:
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-0l-6--------4-Nitroanil1ne
534-52-1--------4,6-Dinitro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (1)
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' (ll -Cannot be separated from Diphenylamine
FORM I SV-2
Q
54 u
11 u
54 u
54 u
11 u
11 u
11 u
11 u
11 u
54 u
54 u
11 u
11 u
11 u
54 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
0
0
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: ITAS_KNOXVILLE _____ _ Contract: NAT._STARC
SAS No.: D Lab Code: ITSTU_ Case No.: 54029
EPA SAMPLE NO.
EX-04-5/93
SDG No.: EX-02
Matrix (soil/water): WATER I Level ( low/med) :
·% Solids:
LOW
Lab Sample ID: XX3376
Date Received: 05/06/93
0.0
m Concentration Units (ug/L or mg/kg dry weight): UG/L_
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I color Before: COLORLESS
Color After: I Comments:
I
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COLORLESS
Analyte Concentration C
Aluminum 40.0 u Antimony-30.0 u Arsenic -2.0 u Barium -:;>6.9 B Berylliuiii 1.0 u
Cadmium 5.0 u Calcium-82600
Chromium 10.0 u Cobalt -20.0 u Copper= 10.0 u
Iron 1300 Lead 2.0 u Magnesium 25400 Manganese 3270 -
Mercury 0.20 u Nickel -20.0 u Potassiuiii 1630 B Selenium_ 2.0 u Silver 5.0 u Sodium--8530
Thallium 2.0 u Vanadium-10.0 u Zinc 17.2 B
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p
p
F-p-
p-
p-
p--p p-
p-
p
F-
p--p
cv p p-
F-p-
p-
F-
p-
p-
Nii:
-
Texture:
Artifacts:
3/90
62
1 1 2 D
D
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
NS29593
Lab Name: ITAS-KNOXVILLE Contract:
m Lab Code: ITSTU
.Matrix: (soil/water)
Sample wt/vol:
Case No.: 54011 SAS No.: SDG No.: EX0259
WATER Lab Sample ID: XX3169
5.0 (g/mL) !1.1_ Lab File ID: XX3169
I Level: ( low/med) LOW Date Received: 05/05/93
% Moisture: not dee.
lcolumn: (pack/cap) CAP
Date Analyzed: 05/13/93
Dilution Factor: =1~-~o'---
I
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CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1 1 2 2-Tetrachloroethane ' ' ' --108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
2 J
10 u
5 u
5 u
5 u
5 u
5 u
21
10 u
5 u
5 u
10 u
5 u
43
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
6
5 u
5 u
5 u
2 J
1/87 Rev.
D lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
37r;
EPA SAMPLE NOJ 7
NS29593 Name: ITAS-KNOXVILLE Contract:
Code: ITSTU Case No.: 54011
WATER
SAS No.: _N_A __ _ SDG No.: EX025
I Matrix: (soil/water)
Sample wt/vol:
I Level: (low/med)
900
LOW
Lab
(g/mL) ML Lab
Date
Sample ID: XX3179
File ID: XX3179
Received: 05/05/93
% Moisture: not dee. dee. Date Extracted: 05/10/93 I Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/20/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
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CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine
67-72-1---------Hexachloroethane --
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
111-91-1--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
11 u
54
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
56 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
56 u
11 u
56 u
11 u
11 u
11 u
1/87 Rev.
n
D
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE Contract:
.37%
EPA SAMPLE NO.j 7,
NS29593
I Lab Code: IT STU
Matrix: (soil/water) I sample wt/vol:
Case No.: 54011
WATER
SAS No. : ""'N-'-'A'----SDG No.: EX025
Lab Sample ID: XX3179
900 (g/mL) ML Lab File ID: XX3179
.Level: (low/med)
~ % Moisture: not dee.
LOW
dee.
Date Received: 05/05/93
Date Extracted: 05/10/93
'Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/20/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
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=
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2----~----3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether __
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)=
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate __
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Pluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
I (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
56 u
11 u
56 u
56 u
11 u
11 u
11 u
11 u
11 u
56 u
56 u
11 u
11 u
11 u
56 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET EPA SAMPLE NO.
.,Lab Name: ITAS_KNOXVILLE______ Contract: NAT._STARC NS-29-5/93
Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX-02-
tatrix (soil/water): ·WATER Lab Sample ID: XX3194
Level ( low/med) : LOW_ Date Received: 05/05/93
1% Solids: 0.0
I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
I
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l1
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I
CAS No.
7429-90 5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
lolor After: COLORLESS
Comments:
I
I
I
I
I
Analyte Concentration C
Aluminum i55. :! Ii Antimony-30.0 u Arsenic -2.0 u Barium -97.0 B Berylliiiiii 1.0 u Cadmium 5.0 u Calcium-~i5400 Chromium_ 16.6 -
Cobalt 20.0 u Copper= 10.0 u Iron 493 Lead 6.0 -
Magnesium ~480 -
Manganese 218 -
Mercury u.20 u Nickel -20.0 u Potassiuiii 1000 u Selenium 2.0 u Silver -5.0 u Sodium--9650 Thallium 2.0 u Vanadium-J.0.0 u Zinc -15.8 B Cyanide_ --
Clarity Before: CLEAR
Clarity After: CLEAR_
FORM I -IN
Q M
p p-
N F ---p-
p-
N p----p p-
p-
p-
p-
F-p-
p-
CV p p-
w F----p-
p-
F-p-
p
NR:
-
Texture:
Artifacts:
3/90
D lA 91 EPA SAMPLE NO.
I VOLATILE ORGANICS ANALYSIS DATA SHEET
NS29B593
Lab Name: ITAS-KNOXVILLE Contract:
• Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX0259
I Matrix: (soil/water) WATER Lab Sample ID: XX3170
Sample wt/vol: 5.0 (g/mL) Mk_ Lab File ID: XX3170
Level: (low/med) LOW Date Received: 05/05/93
"' 0 Moisture: not dee. Date Analyzed: 05/13/93
I ,,
Column: (pack/cap) CAP Dilution Factor: 1.0
I
:I
I ,,
.I
I [)
1.
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9---------Brornornethane .
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Brornodichlorornethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibrornochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Brornoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
23
10 u
5 u
5 u
10 u
5 u
50
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
7
5 u
5 u
5 u
2 J
1/87 Rev.
391/
lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.J9
NS29B593
Name: ITAS-KNOXVILLE Contract: Lab
ILab Code: ITSTU Case No.: 54011
WATER
SAS No.: c.cNc..cA __ _ SDG No.: EX025
'Matrix: (soil/water)
Sample wt/vol:
.Level: (low/med)
% Moisture: not dee.
950 (g/mL) ML
LOW
dee.
(SepF/Cont/Sonc) SEPF
Lab Sample ID: XX3180
Lab File ID: XX3180
Date Received: 05/05/93
Date Extracted: 05/10/93
Date Analyzed: 05/25/93 ·IExtraction:
.GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
I
I ,,
fl,
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
10 u
50
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
52 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
52 u
10 u
52 u
10 u
10 u
10 u
1/87 Rev.
lC I
I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE Contract:
;JCJS
EPA SAMPLE No.39
NS29B593
'Jab Code: IT STU
_Matrix: (soil/water)
lample wt/vol:
Case No.: 54011
WATER
SAS No. : ::.cN=-=A'----SDG No.: EX025
Lab Sample ID: XX3180
950 (g/mL) ML Lab File ID: XX3180
lr"'evel: (low/med)
II. Moisture: not dee.
LOW
dee.
Date Received: 05/05/93
Date Extracted: 05/10/93
~
\rxtrac tion: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 52 u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 52 u
100-02-7----~---4-Nitrophenol 52 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether __ 10 u
86-73-7---------Fluorene 10 u 100-01-6--------4-Nitroanilin~ 52 u
534-52-1--------4,6-Dinitro-2 .. Methylphenol 52 u
86-30-6-- - - - - - --N-Nitrosodiph13nylamine (1)--10 u
101-55-3--------4-Bromophenyl-phenylether --10 u
118-74-1--------Hexachlorobenzene --10 u
87-86-5---------Pentachlorophenol 52 u
85-01-8---------Phenanthrene 10 u
120-12-7--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u 206-44-0--------Fluoranthene 10 u
129-00-0--------Pyrene 10 u
I 85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 21 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate 10 u
117-84-0--------Di-n-OctyllPhthalate --10 u
205-99-2-- - - - - --Benzo·(b) Fluoranthene 10 u
207-08-9--------Benzo(k)Fluor.mthene 10 u 50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u 53-70-3---------Dibenz(a,h)Anthracene 10 u 191-24-2--------Benzo(g,h,i)Perylene 10 u
' (1) -Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
I
I
ff
-Lab
ULab
U.S. EPA -CLP
1 INORGANIC ANALYSES DATA SHEET
Name: ITAS KNOXVILLE _____ _ Contract: NAT,_STARC
SAS No.: Code: ITSTU_ Case No.: 54011
EPA SAMPLE NO.
NS-29B-5/93
SDG No.: EX-02-
n. Matrix (soil/water): 'WATER
Level (low/med): LOW_
Lab Sample ID: XXJ195
Date Received: 05/05/93
Solids: o.o I%
Concentration Units (ug/L or mg/kg dry weight): UG/L_
,m
I
I
I
I
I
I
Before:
lolor After:
comments:
I
••
I
1.
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C Q
Aluminum Ioo B Antimony-30. 0 u Arsenic -2.0 u N Barium -77.8 B ---
Beryll'Iwii 1.0 u Cadmium 5.0 u _N_ Calcium-7740,0 Chromium_ 12.4 -
Cobalt 20.0 u Copper= 10.0 u Iron 520 Lead 2.0 u Magnesium 8900
Manganese 167 -
Mercury 0.20 u Nickel -20.0 u Potass'Iwii 1000 u Selenium_ 2.0 u w Silver 5.0 u ---
Sodium--8520
Thallium 2.0 u Vanadium: 10.0 u Zinc 18.2 B Cyaniae_ --
Clarity Before: CLEAR_
Clarity After: CLEAR_
FORM I -IN
M
I> p-
F-
p-
p p-
p-
p-
p-
p-
p-
F-p-
p-
CV p p-
F-
p-
p-
F-
p p-
N ~
Texture:
Artifacts:
3/90
lA
13S-13
EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE NS30593
m, Lab Code: ITS TU
Contract:
Case No.: 54011 SAS No.: SDG No.: EX0259
'E
m ,,
I
I
It
Matrix: (soil/water) WATER Lab Sample ID: XX3171
Sample wt/vol: 5.0 (g/mL) !:1k._ Lab File ID: XX3171
Level: (low/med) LOW Date Received: 05/05/93
% Moisture: not dee. Date Analyzed: 05/13/93
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UGLL Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 5 u 67-64-1---------Acetone 10 u 75-15-o---------carbon Disulfide 3 J 75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene(Total) __ 5 u 67-66-3---------Chloroform 5 u 107-06-2--------1,2-Dichloroethane 8 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 5 u 56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane 5 u 78-87-5---------1,2-Dichloropropane 23 10061-01-5------cis-l,3-Dichloropropene 5 u 79-01-6---------Trichloroethene 5 u 124-48-1--------Dibromochloromethane 5 u 79-00-5---------1,1,2-Trichloroethane 5 u 71-43-2---------Benzene 5 u 10061-02-6------trans-1,3-Dichloropropene __ 5 u 75-25-2---------Bromoform 5 u 108-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 5 u 79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u 108-88-3--------Toluene 2 J 108-90-7--------Chlorobenzene 5 u 100-41-4--------Ethylbenzene 5 u 100-42-5--------styrene 5 U.
1330-20-7-------Xylene (total) 5 u
FORM I VOA 1/87 Rev ..
D lB
l/01
EPA SAMPLE NO .4 Q
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
OLab Name: ITAS-KNOXVILLE Contract:
NS30593
DLab Code: ITSTU Case No.: 54011 SAS No. : N::.cA=---SDG No.: EX025
Matrix: (soil/water) WATER Lab Sample ID: XX3181
'fl sample wt/vol: 1000 (g/mL) ML Lab File ID: XX3181
Level: (low/med) LOW
·m% Moisture: not dee. dee.
Date Received: 05/05/93
Date Extracted: 05/10/93
(SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93 _,Extraction:
· GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
ll
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
108-95-2--------Phenol lll-44-4--------bis(2-·~c=h~l~o-r_o_e_t~h~y~l~)=E-t~h-e_r __ _
95-57-8---------2-Chlorophenol 541-73-1--------1,3-Dichlorobe_n_z_e_n_e _____ _
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol -----
95-50-1---------1,2-Dichlorobenzene ____ _
95-48-7---------2-Methylphenol
108-60-1--------bis(2-Chlorois_o_p_r_o_p_y~ln)~E~t~h"e~r,,--
106-44-5--------4-Methylphenol-=,---.-~-----
621-64-7--------N-Nitroso-Di-n-Propylamine
67-72-1---------Hexachloroethane ______ -_-_-_
98-95-3---------Nitrobenzene ________ _
78-59-1---------Isophorone
88-75-5---------2-Nitrophe_n_o·i---------
105-67-9--------2,4-Dimethylphenol _____ _
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloro~e7t'h_o_xy-..)~M~e-t·h-an_e __
120-83-2--------2,4-Dichlorophenol _____ -_-_-_
120-82-1--------1,2,4-Trichlorobenzene. ___ _
91-20-3---------Naphthalene....,. ________ _
106-47-8--------4-Chloroaniline 87-68-3---------Hexachlorobutad7i_e_n_e ____ _
59-50-7---------4-Chloro-3-Methylphenol. __ _
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopent-a~d~i-e_n_e __
88-06-2---------2,4,6-Trichlorophenol __ ~~~~
95-95-4---------2,4,5-Trichlorophenol ___ _
91-58-7---------2-Chloronaphthalene ____ _
88-74-4---------2-Nitroaniline 131-11-3--------Dimethyl Phtha.~l-a7t_e _____ _
208-96-8--------Acenaphthylene 606-20-2--------2,6-Dinitrotol._u_e_n_e _____ _
FORM I SV-1
UG/L Q
10 u
32
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
1/87 Rev.
D
u lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA
-'-//{)
SAMPLE NO .4 l
NS30593
1 Lab
Lab Code: ITSTU Case No.: 54011
WATER
SAS No.: NA SDG No.: EX025
,_Matrix: (soil/water)
Sample wt/vol: 1000 (g/mL) ML I Level: (low/med) LOW
% Moisture: not dee. dee.
IExtraction: (SepF/Cont/Sonc) SEPF
----
Lab Sample ID: XX3181
Lab File ID: XX3181
Date Received: 05/05/93
Date Extracted: 05/10/93
Date Analyzed: 05/25/93
IGPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
I,
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether __
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' ' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
so u
10 u so u so u
10 u
10 u
10 u
10 u
10 u
so u so u
10 u
10 u
10 u so u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1/87 Rev.
U.S. EPA -CLP
1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET
I Lab Name: ITAS_KNOXVILLE _____ _ Contract: NAT._STARC NS-30-5/93
Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX-02-
IMatrix (soil/water): ·wATER Lab Sample ID: XX3196
Level (low/med): LOW Date Received: 05/05/93 1% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L_ I
I
I
I
I
I
I,
I
Color
lolor
Before:
After:
(omments:
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C Q
Aluminum 4 0. o u Antimony-30.0 u Arsenic -2.0 u _N __ Barium -:ll.8 B Berylliwii 1.0 u cadmium 5.0 u _N __ Calcium-!07000 Chromium 10.0 u Cobalt 20.0 u copper= 10.0 u Iron 1150 Lead 2.0 u Magnesium 2!900 Manganese 1620 -
Mercury 0.20 u Nickel -20.0 u Potassiuiii 1030 B Selenium 2.0 u w Silver 5.0 u ---
Sodium--!2100
Thallium 2.0 u vanadium-.LO.O u Zinc 12.1 B cyanide_ --
Clarity Before: CLEAR
Clarity After: CLEAR_
FORM I -IN
M
p--
p-
F-p-
p-
p p-
p-
p-
p-
p-
F-p-
p-
CV p p-
F-p-
p-
F-
p-
p-
Nl<
Texture:
Artifacts:
3/90
154 E lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I NS31593 Lab Name: ITAS-KNOXVILLE Contract:
I Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX0259
Matrix: ( soil/water)
I Sample wt/vol:
I Level: ( low/med)
% Moisture: not dee.
WATER
5.0 (g/mL) ill,_
LOW
Lab Sample ID: XX3168
Lab File ID: XX3168
Date Received: 05/05/93
Date Analyzed: 05/13/93 I column: (pack/cap) CAP Dilution Factor: 1.0 ~~--
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
10
10
10
10
5
10
5
5
5
5
5
71
10
5
5
10
5
78-87-5---------1,2-Dichloropropane 200
10061-01-5------cis-l,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43-2---------Benzene 5 10061-02-6------trans-l,3-Dichloropropene __ 5
75-25-2---------Bromoform 5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10 127-18-4--------Tetrachloroethene 5
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 108-88-3--------Toluene 34 108-90-7-----~--Chlorobenzene 5
100-41-4--------Ethylbenzene 2 100-42-5--------styrene 5 1.3 3 0-2 0-7-------Xylene (total) 7
FORM I VOA
Q
u
u
u
u
u
u
u
u
u u
u
u u
u
u u
u
u
u
u
u
u
u
u
u u
u
u
J u
1/87 Rev.
D
C lB
i.fcJc/
EPA SAMPLE No.42 '
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS31593 fab Name: ITAS-KNOXVILLE Contract:
Lab Code: ITSTU Case No.: 54011 SAS No . : :.:N::.:A:.___ __ SDG No.: EX025
,tatrix: (soil/water) WATER Lab Sample ID: XX3178
Sample wt/vol: 970 (g/mL) ML Lab File ID: XX3178
'evel: (low/med) LOW Date Received: 05/05/93
'I; Moisture: not dee. dee.
lxtraction: (SepF/Cont/Sonc)
Date Extracted: 05/10/93
I
I
I
I
I
I
,I
I
I
I
I
I
SEPF Date Analyzed: 05/20/93
Cleanup: (Y /N) N pH: Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u lll-44-4--------bis(2-Chloroethyl)Ether 95
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
108-60-l--------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 6 J
621-64-7--------N-Nitroso-Di-n-Propylamine 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-0---------Benzoic Acid 52 u
lll-91-l--------bis(2-Chloroethoxy)Methane 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-82-1--------1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u 77-47-4---------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 52 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 52 u
131-11-3--------Dimethyl Phthalate .10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I SV-1 1/87 Rev.
E lC
;I½
EPA SAMPLE N0.42 SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE Contract:
NS31593
.Lab Code: ITSTU Case No.: 54011 SAS No.: c.cNc..cA __ _ SDG No.: EX025
Matrix: (soil/water) WATER Lab Sample ID: XX3178
lsample wt/vol: 970 (g/mL) ML Lab File ID: XX3178
Level: (low/med) LOW l Moisture: not dee. dee.
Date Received: 05/05/93
Date Extracted: 05/10/93
(SepF/Cont/Sonc) SEPF Date Analyzed: 05/20/93 rxtraction:
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.00
I
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (l)= 101-55-3--------4-Bromophenyl-phenylether __ 118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' (1) -cannot be separated from Diphenylamine
FORM I SV-2
Q
52 u
10 u
52 u
52 u
10 u
10 u
10 u
10 u
10 u
52 u
52 u
10 u
10 u
10 u
52 u
10 u
10 u
10 u
10 u
10 u
10 u
21 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1/87 Rev.
I Lab
Lab
Name: ITAS KNOXVILLE
U.S. EPA -CLP
1 INORGANIC ANALYSES DATA SHEET
------
Code: ITSTU Case No.: 54011
Contract: NAT. STARC
SAS No.:
5 i.3sa
EPA SAMPLE NO.
NS-31-5/93
SDG No.: EX-02-
.Matrix (soil/water):·WATER
Level (low/med): LOW_
Lab Sample ID: XX3193
Date Received: 05/05/93
Solids: _o.o
concentration Units (ug/L or mg/kg dry weight): UG/L_
I
I
I
I
I
I
I
I Color Before:
folor After:
Comments:
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte concentration C Q
Aluminum 67.j B Antimony-30.0 u Arsenic -2.0 u N Barium -.J 6. 3 ---B Berylliuiii 1.0 u Cadmium 5.0 u N Calcium-IHlooo ---
Chromium 74.0 -
Cobalt -20.0 u Copper--10.0 u Iron --3260 Lead 4.0 Magnesium !:>090 Manganese 47.1 -
Mercury 0.20 u Nickel -47.5 Potassiuiii 3180 11 Selenium_ 2.0 u Silver 5.0 u Sodium --14700
Thalliuin 2.0 u Vanadium: 10.0 u Zinc 1640 Cyanide_ ---
Clarity Before: CLEAR_
Clarity After: CLEAR_
FORM I -IN
M
p
p-
F p-
p-
p-
p-
p
p-
p-
p-
F-p-
p
c'J p -p -F p-
p-
F p-
p-
NR
-
Texture:
Artifacts:
3/90
I lA 170
EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: ITAS-KNOXVILLE Contract:
NS32593
I Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX0259
Matrix: (soil/water) I Sample wt/vol:
I Level: ( low/med)
% Moisture: not dee.
WATER
5.0
LOW
Lab Sample ID: XX3172
(g/mL) !1k.._ Lab File ID: XX3172
Date Received: 05/05/93
Date Analyzed: 05/13/93 I Column: (pack/cap) CAP Dilution Factor: 1.0 ~-"---
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-1,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1 1 2 2-Tetrachloroethane I I I __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
1 J
10 u
3 J
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
I
I
lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE Contract:
EPA
L/'13 4 L
SAMPLE NO.
NS32593
I Lab Code: ITSTU
Matrix: (soil/water) I Sample wt/vol:
Case No.: 54011
WATER
SAS No . : :.:N:.:A'----SDG No. : EX025
Lab Sample ID: XX3182
1000 (g/mL) ML Lab File ID: XX3182 I Level: (low/med)
% Moisture: not dee.
LOW
dee.
Date Received: 05/05/93
Date Extracted: 05/10/93
.Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether
106-44-5--------4-Methylphenol -
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane __
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
1/87 Rev.
,;.;1~4,
I
rab
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS32593 Name: ITAS-KNOXVILLE Contract:
Lab Code: ITSTU Case No.: 54011 SAS No. : ::.cN=..:A;__ __ SDG No.: EX025
tatrix: (soil/water) WATER Lab Sample ID: XX3182
Sample wt/vol: 1000 (g/mL) ML Lab File ID: XX3182
l,evel: (low/med) LOW Date Received: 05/05/93
% Moisture:
lxtraction:
not dee. dee. Date Extracted: 05/10/93
I
I
I
I
I
I
I
I
I
I
I
I
SEPF Date Analyzed: 05/25/93
Cleanup:
(SepF/Cont/Sonc)
(Y /N) N pH: Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u 83-32-9---------Acenaphthene 10 u 51-28-5---------2,4-Dinitrophenol 50 u 100-02-7--------4-Nitrophenol 50 u 132-64-9--------Dibenzofuran 10 u 121-14-2--------2,4-Dinitrotoluene 10 u 84-66-2---------Diethylphthalate 10 u 7005-72-3-------4-Chlorophenyl-phenylether 10 u 86-73-7---------Fluorene --10 u 100-01-6--------4-Nitroaniline 50 u 534-52-1--------4,6-Dinitro-2-Methylphenol 50 u
86-30-6---------N-Nitrosodiphenylamine (1)= 10 u 101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u 87-86-5---------Pentachlorophenol 50 u 85-01-8---------Phenanthrene 10 u 120-12-7--------Anthracene 10 u 84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u 129-00-0--------Pyrene 1.0 u
85-68-7---------Butylbenzylphthalate 10 u 91-94-1---------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u 218-01-9--------Chrysene 10 u 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 10 u
117~84-0--------Di-n-Octyl Phthalate 10 u 205-99-2--------Benzo(b)Fluoranthene 10 u 207-08-9--------Benzo(k)Fluoranthene 10 u 50-32-8---------Benzo(a)Pyrene 10 u 193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u 53-70-3---------Dibenz(a,h)Anthracene 10 u 191-24-2--------Benzo(g,h,i)Perylene 10 u
• • (1) -Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
I
I
U.S. EPA -CLP
l INORGANIC ANALYSES DATA SHEET
Name: ITAS_KNOXVILLE _____ _ Contract: NAT._STARC
58; 58
EPA SAMPLE NO.
NS-32-5/93 Lab I Lab Code: ITSTU Case No.: 54011
Matrix (soil/water):·WATER I Level (low/med): LOW_
SAS No.: SDG No.: EX-02-
Lab Sample ID: XX3197
Date Received: 05/05/93
Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
I
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I
I
I
I
lolor Before:
.olor After:
~omments:
I
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I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte concentration C Q
Aluminum 11;0 B Antimony-..10. 0 u Arsenic -2.0 u WN Barium -69.0 B -

-
Berylliuiii 1.0 u Cadmium 5.0 u N Calcium-37300 ---
Chromium_ 10.0 u Cobalt 20.0 u Copper--13.5 B Iron --361 Lead 2.7 B Magnesium 6650 Manganese 78.2 -
Mercury 0.20 u Nickel -20.0 u Potassiuiii 1790 B Selenium_ 2.0 u Silver 5.0 u Sodium--6290
Thalliiiin 2.0 u Vanadium-.1.0. 0 u Zinc 57.0 Cyanide_ ---
Clarity Before: CLEAR_
Clarity After: CLEAR_
FORM I -IN
M
I> p--F p-
p
p-
p p-
p-
p-
p-
F-
p-
p
c'J p p-
F -p -p
F-p-
p-
Nfi:
-
Texture:
Artifacts:
3/90
D 100
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I Lab Name: ITAS-KNOXVILLE Contract:
NS09593
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No.: EX0159 I Matrix: ( soil/water) WATER Lab Sample ID: ~X~X~3~3~5~1~---
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Sample wt/vol: 5.0 ( g/mL) lli,_ Lab File ID: XX3351
Level: (low/med) LOW Date Received: 05/06/93
% Moisture: not dee. Date Analyzed: 05/14/93
Column: (pack/cap) CAP Dilution Factor: ~l~-~o'---
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)_
10
10
10
10
5
10
5
10
5
5
5
107-06-2--------1,2-Dichloroethane 4400
78-93-3---------2-Butanone ~ ~
71-55-6---------1,1,1-Trichloroethane 5
56-23-5---------carbon Tetrachloride 5
108-05-4--------Vinyl Acetate 10
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 5
10061-01-5------cis-l,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 3
71-43-2---------Benzene 5
10061-02-6------trans-l,3-Dichloropropene __ 5
75-25-2---------Bromoform 5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10
127-18-4--------Tetrachloroethene 5
79-34-5---------1,1,2,2-Tetrachloroethane __ 5
108-88-3--------Toluene 460
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 32
100-42-5--------styrene 5
1330-20-7-------Xylene (total) 69
FORM I VOA
Q
u
u
u
u
u
u
u
u
u
u
E
u
u
u
u
u
u
u
u
J
u
u
u
u
u
u u
E
u
u
1/87 Rev.
lA
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE Contract:
Case No. : 54 029 Lab Code: ITSTU I
SAS No.:
Matrix: (soil/water) WATER Lab
I Sample wt/vol: 5.0 (g/rnL) ML_ Lab
Level: (low/med) LOW Date
I % Moisture: not dee. Date
124
EPA SAMPLE NO.
NS09593DL
SDG No.: EX0159
Sample ID: XX3351
File ID: XX3351D3
Received: 05/06/93
Analyzed: 05/15/93
Column: (pack/cap) CAP Dilution Factor: 67 ~---I
I
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I
I
I
I
I
I
I
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromornethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)_
670
670
670
670
250
670
330
330
330
330
330
107-06-2--------1,2-Dichloroethane 10000
78-93-3---------2-Butanone 670
71-55-6---------1,1,1-Trichloroethane 330
56-23-5---------carbon Tetrachloride 330
108-05-4--------Vinyl Acetate 670
75-27-4---------Bromodichloromethane 330
78-87-5---------1,2-Dichloropropane 330
10061-01-5------cis-l,3-Dichloropropene 330
79-01-6---------Trichloroethene 330
124-48-1--------Dibromochloromethane 330
79-00-5---------1,l,2-Trichloroethane 330
71-43-2---------Benzene 330
10061-02-6------trans-l,3-Dichloropropene __ 330
75-25-2---------Bromoform 330
108-10-1--------4-Methyl-2-Pentanone 670
591-78-6--------2-Hexanone 670
127-18-4--------Tetrachloroethene 330
79-34-5---------1,1,2,2-Tetrachloroethane __ 330
108-88-3--------Toluene 400
108-90-7--------Chlorobenzene 330
100-41-4--------Ethylbenzene 67
lD0-42-5--------Styrene 330
1330-20-7-------Xylene (total) 330
FORM I VOA
Q
u
u
u
u
DJ
u
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
D
u
DJ
u
u
1/87 Rev.
lA EPA SAMPLE NO.
I
I VOLATILE ORGANICS ANALYSIS DATA SHEET
tab Name: ITAS-KNOXVILLE
NS09593DL2
Contract:
Lab Code: ITSTU Case No.: 54029 SAS No.: ----SDG. No.: EX0159
liatrix: (soil/water) WATER Lab Sample ID: ~X~X~3~5~5~1 ___ _
[ample wt/vol:
Level: ( low/med)
5.0 (g/mL) !:11.._ Lab File ID: XX3551DL
LOW Date Received: 05/06/93
1: Moisture: not dee. Date Analyzed: 05/15/93
Column: (pack/cap) CAP Dilution Factor: ~3~-~3 __ _
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L Q
I
I
I
I
I
I
I
I
I
I
I
I
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (Total)
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
33 u
33 u
33 u
33 u
12 DJ
33 u
17 u
9 DJ
17 u
17 u
17 u
8500 DE
33 u
17 u
17 u
33 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
33 u
33 u
17 u
17 u
450 D
17 u
29 D
17 u
64 D
J 4 I
FORM I VOA 1/87 Rev.
I
I lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO~ 8 ~
NS09593
.Lab
Lab Code: ITSTU Case No.: 54029
WATER
SAS No.: NA SDG No. : EX015
ratrix: (soil/water)
Sample wt/vol: 1000
tevel: (low/med) LOW
(g/mL) ML
----
Lab Sample ID: XX3360
Lab File ID: XX3360
Date Received: 05/06/93
% Moisture: not dee. dee. Date Extracted: 05/11/93
l:xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
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I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
19
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
1/87 Rev.
I
I
lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO .4 9
NS09593 Lab I Lab Code: ITSTU Case No.: 54029
WATER
SAS No.: NA SDG No.: EX015
.Matrix: (soil/water)
Sample wt/vol:
.Level: (low/med)
% Moisture: not dee.
1000 (g/mL) ML
LOW
dee. I Extraction: (SepF/Cont/Sonc) SEPF
----
Lab Sample ID: XX3360
Lab File ID: XX3360
Date Received: 05/06/93
Date Extracted: 05/11/93
D·ate Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0 cc...;;_.c___ __ I
I
I
I
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I
I
I
I
I
I
I
I
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-Bl-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd}Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2------~-Benzo(g,h,i)Perylene
' (11 -cannot be separated from Diphenylamine
FORM I SV-2
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1/87 Rev.
I
I
Lab Name: ITAS KNOXVILLE
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
------I Lab Code: ITSTU Case No.: 54029
Contract: NAT. STARC
SAS No.:
EPA SAMPLE NO.
NS-09-5/93
SDG No.: EX-02
Matrix (soil/water): WATER Lab Sample ID: XX3379 I Level (low/med): LOW Date Received: 05/06/93
% Solids: 0.0 I Concentration Units (ug/L or mg/kg dry weight): UG/L_
I
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I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
I Color Before: YELLOW __
Color After: I comments:
I
I
I
I
I
YELLOW __
Analyte Concentration C
Aluminum II1oo -
Antimony-30.0 u Arsenic -2.0 u Barium -.L480
BeryllTiiiii 1.0 u Cadmium 5.0 u Calcium-1i51!000 Chromium 50.1 -
Cobalt 119 -
Copper--o8.9 -
Iron --45300 -
Lead 2.0 u
Magnesium 2SI000 Manganese 51300 -
Mercury 0.20 u Nickel -23.9 B
PotassTiiiii 3240 B Selenium_ 10.0 u
Silver 5.0 u Sodium--I:!9000
Thallium 2.0 u
Vanadium: .LO. 0 u
Zinc 49.2
Cyaniae_ ---
Clarity Before: CLOUDY
Clarity After: CLOUDY
FORM I -IN
Q M
V p w F----p-
p-
p p-
p-
p p-
p
w F----p-
p-
c'J p -p -F -p p-
w F----p-
p-
NR
-
Texture:
Artifacts:
3/90
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
1 6;
EPA SAMPLE NO.
NS10593 I Lab Name: ITAS-KNOXVILLE Contract:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No.: EX0159
Matrix: (soil/water) WATER Lab Sample ID: XX3353
Sample wt/vol: 5.0 (g/mL) Mk__ Lab File ID: XX3353
Level: ( low/med) LOW Date Received: 05/06/93
95 Moisture: not dee. Date Analyzed: 05/15/93
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 8 J
75-00-3---------Chloroethane 5 J
75-09-2---------Methylene Chloride 3 J
67-64-1---------Acetone 10 u
75-15-0---------carbon Disulfide 8
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (Total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5400 E
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 2 J
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 1 J
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 10
71-43-2---------Benzene 5 u
10061-02-6------trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 65
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 2 J
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 4 J
100-42-5--------Styrene 5 u
1330-20-7-------Xylene (total) 10
FORM I VOA 1/87 Rev.
1 8 E
I
I lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE Contract:
NS10593DL
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No. : EX0159
I Matrix: (soil/water) WATER Lab Sample ID: XX3353
1 Sample wt/vol:
Level: (low/med)
5.0 (g/mL) ML_
LOW
Lab File ID: XX3353D
Date Received: 05/06/93 I% Moisture: not dee. Date Analyzed: 05/15/93
I
I
I
I
I
I
I
I
I
I
I
I
I
Column: (pack/cap) CAP Dilution Factor: 80 ~---
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane 800 74-83-9---------Bromomethane 800 75-01-4---------Vinyl Chloride 800
75-00-3---------Chloroethane 800
75-09-2---------Methylene Chloride . 130 67-64-1---------Acetone 800 75-15-0---------Carbon Disulfide 400
75-35-4---------1,1-Dichloroethene 400
75-34-3---------1,1-Dichloroethane 400 540-59-0--------1,2-Dichloroethene (Total) 400
67-66-3---------Chloroform 400
107-06-2--------1,2-Dichloroethane 16000
78-93-3---------2-Butanone 800
71-55-6---------1,1,1-Trichloroethane 400
56-23-5---------carbon Tetrachloride 400
108-05-4--------Vinyl Acetate 800
75-27-4---------Bromodichloromethane 400
78-87-5---------1,2-Dichloropropane 400
10061-01-5------cis-1,3-Dichloropropene 400
79-01-6---------Trichloroethene 400
124-48-1--------Dibromochloromethane 400
79-00-5---------1,1,2-Trichloroethane 400 71-43-2---------Benzene 400
10061-02-6------trans-l,3-Dichloropropene __ 400
75-25-2---------Bromoform 400
108-10-1--------4-Methyl-2-Pentanone 800 591-78-6--------2-Hexanone 800
127-18-4--------Tetrachloroethene 400
79-34-5---------1,1,2,2-Tetrachloroethane __ 400
108-88-3--------Toluene 400
108-90-7--------Chlorobenzene 400
100-41-4--------Ethylbenzene 400 100-42-5--------styrene 400
1330-20-7-------Xylene (total) 400
FORM I VOA
Q
u
u
u
u
DJ
u
u
u
u
u
u
D
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1/87 Rev.
I
I
lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO. 5 j
NS10593
I Lab
Lab Code: ITSTU Case No.: 54029
WATER
SAS No . : :cN::cA:......_ __ SDG No.: EX015 I Matrix: (soil/water)
Sample wt/vol:
I Level: (low/med)
940
LOW
Lab
(g/mL) ML Lab
Date
Sample ID: XX3362
File ID: XX3362
Received: 05/06/93
% Moisture: not dee. dee. Date Extracted: 05/11/93 I Extraction: SEPF Date Analyzed: 05/26/93
I
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) N pH: Dilution Factor: 1.00
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0--------.-Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
53 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
53 u
11 u
53 u
11 u
11 u
11 u
1/87 Rev.
I
I lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO. 5 )
NS10593 I Lab
Lab Code: ITSTU Case No.: 54029 SAS No.: NA ='----SDG No. : EX015
.Matrix: (soil/water) WATER Lab Sample ID: XX3362
Sample wt/vol: 940 (g/mL) ML Lab File ID: XX3362 I Level: (low/med) LOW Date Received: 05/06/93
% Moisture: I Extraction:
not dee. dee.
SEPF
Date Extracted: 05/11/93
Date Analyzed: 05/26/93
I GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) N pH: Dilution Factor: 1.00
I
I
I
I
I
I
I
I
I
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phtba1ate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Pluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' ' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
53 u
11 u
53 u
53 u
11 u
11 u
11 u
ll u
11 u
53 u
53 u
11 u
11 u
11 u
53 u
11 u
11 u
11 u
11 u
11 u
11 u
21 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
I
I
Lab Name:
I Lab Code:
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
ITAS_KNOXVILLE _____ _ Contract: NAT. STARC
SAS No.: ITSTU_ Case No.: 54029
EPA SAMPLE NO .6 3 1
NS-10-5/93
SDG No.: EX-02
Matrix (soil/water): WATER I Level ( low/med) :
% Solids:
LOW
0.0
Lab Sample ID: XX3381
Date Received: 05/06/93
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
•
lcolor Before: COLORLES_
Color After: I comments:
I
I
I
I
I
COLORLESS
Analyte Concentration C Q
Aluminum 566 -
Antimony-30.0 u
Arsenic -2.0 u Barium -297
BeryllTiiiii 1.0 u Cadmium 5.0 u Calcium-222000 Chromium 14.2 -
Cobalt 45.4 ti Copper= 10.0 u Iron 2260 Lead 3.5 -w
Magnesium !!6000 -
Manganese 14300 -
Mercury 0.20 u Nickel -45.2
PotassTiiiii 1620 ti Selenium_ 2.0 u w
Silver 5.0 u ---
Sodium --!5~000
Thallium 2.0 u w Vanadium-10.0 u ---
Zinc 47.4 Cyanide -
-
Clarity Before: CLEAR_
Clarity After: CLEAR_
FORM I -IN
M
r p-
F-
p-
p-
p-
p-
p-
p-
p-
p-
F-p-
p-
cV p p-
F-p-
p-
F-p-
p-
N'R
-
Texture:
Artifacts:
3/90
I
I lA EPA SAMPLE NO~ Q
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE Contract:
NS11593
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No.: EX0159
Matrix: (soil/water) WATER Lab Sample ID: XX3352
Sample wt/vol: 5.0 (g/mL) !:l1,_ Lab File ID: XX3352R
Level: (low/med) LOW Date Received: 05,:06,:93
% Moisture: not dee. Date Analyzed: 05,:15,:93
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG,:L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 1 J
67-64-1---------Acetone 10 u
75-15-0---------Carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (Total) 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------trans-1,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 4 J
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1 1 2 2-Tetrachloroethane , , , --5 u
108-88-3--------Toluene 61
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 95
100-42-5--------Styrene 5 u
1330-20-7-------Xylene (total) 150
FORM I VOA 1/87 Rev.
525 I
I lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
NS11593 Name: ITAS-KNOXVILLE Contract: .Lab
Lab Code: ITSTU Case No.: 54029
WATER
SAS No. : ::..:N::..:A;__ __ SDG No. : EX015
tatrix: (soil/water)
Sample wt/vol: 900
J,evel: (low/med) LOW
Lab
(g/mL) ML Lab
Date
Sample ID: XX3361
File ID: XX3361
Received: 05/06/93
% Moisture:
lxtraction:
not dee. dee. Date Extracted: 05/11/93
I
I
I
I
I
I
I
I
I
I
I
I
(SepF/Cont/Sonc) SEPF Date Analyzed: 05/26/93
Cleanup: (Y/N) N pH: Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 11 u lll-44-4--------bis(2-Chloroethyl)Ether 11 u
95-57-8---------2-Chlorophenol 11 u
541-73-1--------1,3-Dichlorobenzene 11 u 106-46-7--------l,4-Dichlorobenzene 11 u
100-51-6--------Benzyl Alcohol 11 u 95-50-1---------1,2-Dichlorobenzene 11 u
95-48-7---------2-Methylphenol 11 u 108-60-l--------bis(2-Chloroisopropyl)Ether_ 11 u
106-44-5--------4-Methylphenol 11 u 621-64-7--------N-Nitroso-Di-n-Propylamine __ 11 u
67-72-1---------Hexachloroethane 11 u 98-95-3---------Nitrobenzene 11 u
78-59-1---------Isophorone 11 u 88-75-5---------2-Nitrophenol 11 u
105-67-9--------2,4-Dimethylphenol 11 u 65-85-0---------Benzoic Acid 56 u
lll-91-l--------bis(2-Chloroethoxy)Methane 11 u
120-83-2--------2,4-Dichlorophenol --11 u 120-82-1--------1,2,4-Trichlorobenzene 11 u 91-20-3---------Naphthalene 11 u
106-47-8--------4-Chloroaniline 11 u
87-68-3---------Hexachlorobutadiene 11 u
59-50-7---------4-Chloro-3-Methylphenol 11 u 91-57-6---------2-Methylnaphthalene 11 u 77-47-4---------Hexachlorocyclopentadiene __ 11 u
88-06-2---------2,4,6-Trichlorophenol 11 u
95-95-4---------2,4,5-Trichlorophenol 56 u
91-58-7---------2-Chloronaphthalene 11 u
88-74-4---------2-Nitroaniline 56 u 131-11-3--------Dimethyl Phthalate 11 u 208-96-8--------Acenaphthylene 11 u 606-20-2--------2,6-Dinitrotoluene 11 u
FORM I SV-1 1/87 Rev.
I
I lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO.5~
NS11593
.Lab
Lab Code: ITSTU Case No.: 54029
WATER
SAS No. : '"'N"'A'---SDG No.: EX015
'Matrix: (soil/water)
Sample wt/vol: 900 (g/mL) ML
ILevel: (low/med) LOW
% Moisture: not dee. dee.
11Extraction: (SepF/Cont/Sonc) SEPF
Lab
Lab
Date
Date
Date
Sample ID: XX3361
File ID: XX3361
Received: 05/06/93
Extracted: 05/11/93
Analyzed: 05/26/93
Cleanup: (Y /N) N pH: Dilution Factor: 1.00
I
I
I
·I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene --
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (1)
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenz(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
56 u
11 u
56 u
56 u
11 u
11 u
11 u
11 u
11 u
56 u
56 u
11 u
11 u
11 u
56 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
I
I
Lab Name: ITAS KNOXVILLE ,1 Lab Code: ITSTU
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
------Contract: NAT. STARC
SAS No.:
EPA SAMPLE NO.
NS-11-5/93
SDG No. : EX-02
, Matrix (soil/water): I Level (low/med):
% Solids:
Case No.: 54029
WATER
LOW
Lab Sample ID: XX3380
Date Received: 05/06/93
0.0
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L_
a
I
I
I
I
I
f Color Before:
Color After:
11 Comments:
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLES_
COLORLESS
Analyte Concentration C
Aluminum 'l:1:lo -
Antimony-30.0 u Arsenic -2.0 u Barium -115 B
Berylliuni 1.0 u
Cadmium 5.0 u Calcium-4910 B
Chromium_ 10.0 u Cobalt 20.0 u Copper--10.0 u Iron --6330
Lead 2.0 u
Magnesium 4150 B
Manganese 63.1
Mercury 0.20 u Nickel -20.0 u Potassiuni 1280 B
Selenium_ 2.0 u Silver 5.0 u Sodium--II!!ooo Thallium 2.0 u
Vanadium: .LO.O u
Zinc 32.5
cyaniae ---
Clarity Before: CLOUDY
Clarity After: CLOUDY
FORM I -IN
Q M
p -p w F ----p-
p-
p-
p p-
p p-
p-
F-p-
p-
c'J p p-
F p-
p-
F-p-
p
N
Texture:
Artifacts:
3/90
63;
220 I
D lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
fl Lab Name: ITAS-KNOXVILLE
NS15593
Contract:
" Lab Code: ITS TU Case No. :
ff Matrix: (soil/water)
54029 SAS No.: ____ SDG No.: EX0159
n Sample
Level:
wt/vol:
( low/med)
WATER
5.0
LOW
Lab Sample ID: ~x~x~3~3~5~0c_ __ _
(g/mL) Mk_ Lab File ID: XX3350
Date Received: 05/06/93
D % Moisture: not dee. Date Analyzed: 05/14/93
'Column:
·I
I
g
0
a
D
(pack/cap) CAP Dilution Factor: ~1~-~0c_ __
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)_
10
10
10
10
2
10
5
5
5
5
5
107-06-2--------1,2-Dichloroethane 480
78-93-3---------2-Butanone 10
71-55-6---------1,1,1-Trichloroethane 5
56-23-5---------carbon Tetrachloride 5
108-05-4--------Vinyl Acetate 10
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 2
10061-01-5------cis-1,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43-2---------Benzene 5
10061-02-6------trans-l,3-Dichloropropene __ 5
75-25-2---------Bromoform 5
100-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2-Hexanone 10
127-18-4--------Tetrachloroethene 5
79-34-5---------1,1,2,2-Tetrachloroethane __ 5
108-88-3--------Toluene 22
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 5
100-42-5--------styrene 5
1330-20-7-------Xylene (total) 5
FORM I VOA
Q
u u
u
u
J
u
u
u
u
u u
E
u u
u u
u
J u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
1/87 Rev.
235 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE Contract:
Lab Code: ITSTU case No.: 54029 SAS No.: U Matrix: (soil/water) WATER
Sample.wt/vol: 5.0 (g/mL) M1.._ m Level: (low/med) ~L~O~W __
1 % Moisture: not dee.
Column: (pack/cap) ~C~A~P __
NS15593DL
SDG No.: EX0159
Lab Sample ID: XX3550 =~~----
Lab File ID: XX3550D
Date Received: 05/06/93
Date Analyzed: 05/15/93
Dilution Factor: 3.3 ~~--It
I
I
I
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I
I
I
I.
CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q
I
I
I
I
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Acetone
75-15-0---------carbon Disulfide 75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (Total) __ 67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride 108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __ 75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
__ 108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
33 u
33 u
33 u
33 u
12 DJ
33 u
17 u
17 u
17 u
17 u
17 u
500 D
33 u
17 u
17 u
33 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
17 u
33 u
33 u
17 u
17 u
25 D
17 u
17 u
17 u
17 u
1/87 Rev.
D
0 lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE No .531
NS15593
Code: ITSTU Case No.: 54029
WATER
SAS No . : :.:N:.:Ac...._ __ SDG No. : EX015
tatrix: (soil/water)
Sample wt/vol: 930 (g/mL) ML
(low/med) LOW
% Moisture: not dee. dee.
·Lxtraction: (SepF/Cont/Sonc) SEPF
Lab
Lab
Date
Date
Date
Sample ID: XX3359
File ID: XX3359
Received: 05/06/93
Extracted: 05/11/93
Analyzed: 05/25/93
Cleanup: (Y /N) N pH: Dilution Factor: 1.0
I
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I
I,
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-l--------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane
120-83-2--------2,4-Dichlorophenol --
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I SV-1
Q
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
54 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
54 u
11 u
54 u
11 u
11 u
11 u
1/87 Rev.
I
I
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Name: ITAS-KNOXVILLE Contract:
EPA SAMPLE NO .5 3 '.
NS15593
(
Lab
ab Code: ITSTU Case No.: 54029 SAS No.: NA SDG No.: EX015 ----
(atrix: (soil/water) WATER Lab Sample ID: XX3359
ample wt/vol: 930 (g/mL) ML Lab File ID: XX3359
tevel: (low/med) LOW Date Received: 05/06/93
% Moisture: not dee. dee. Date Extracted: 05/11/93
•Jxtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 05/25/93
GPC Cleanup: (Y/N) N pH: Dilution Factor: 1.0
I
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I
I
I
I
••
I
I
I
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether __
86-73-7---------Fluorene
100-0l-6--------4-Nitroan1l1ne
534-52-1--------4,6-Dinitro-2-Methylphenol
86-30-6---------N-Nitrosodiphenylamine (1)--
101-55-3--------4-Bromophenyl-phenylether --
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate
117-84-0--------Di-n-Octyl Phthalate --
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3-- - - - -----Dibenz (a, h) Anthracene
191-24-2--------Benzo(g,h,i)Perylene
' (1) -Cannot be separated from Diphenylamine
FORM I SV-2
Q
54 u
11 u
54 u
54 u
11 u
11 u
11 u
11 u
11 u
54 u
54 u
11 u
11 u
11 u
54 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
I
I
Lab I Lab
Name: ITAS KNOXVILLE
U.S. EPA -CLP
1 INORGANIC ANALYSES DATA SHEET
------
Code: ITSTU Case No.: 54029
Contract: NAT. STARC
SAS No.:
EPA SAMPLE NO.
NS-15-5/93
SDG No.: EX-02
__ Matrix (soil/water): WATER Lab Sample ID: XX3378 I Level (low/med): LOW Date Received: 05/06/93
% Solids: 0.0 I Concentration Units (ug/L or mg/kg dry weight): UG/L_
I
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I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
lcolor Before: COLORLESS
Color After:
lcomments:
I
I
I
I
I
COLORLESS
Analyte Concentration C Q
Aluminum 40.0 u Antimony-30.0 u Arsenic -2.0 u Barium -448 Berylliuiii 1.0 u Cadmium 5.0 u Calcium-323000 Chromium 11.7 -
Cobalt -82.6 -
Copper--10.0 u Iron --3040 Lead 8.7 -
Magnesium !55000
Manganese 15200 -
Mercury 0.20 u Nickel -20.0 u Potassiuiii 2020 B
Selenium_ 2.0 u w Silver 5.0 u ---
Sodium --57300
Thalliuin 2.0 u w Vanadium-.1.0. 0 u ---
Zinc -14. 5 B
Cyaniae_ --
Clarity Before: CLEAR_
Clarity After: CLEAR_
FORM I -IN
M
p
p -F p-
p-
p-
p p-
p p-
p-
F-
p-
p-
CV p p-
F= p
p-
F-p-
p-
NR:
-
Texture:
Artifacts:
3/90
63
I
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA
JZ'/
SAMPLE No! E
I Lab Name: ITAS-KNOXVILLE Contract:
TRIPBLANK
Lab Code: ITSTU Case No.: 54011 SAS No.: SDG No.: EX0259 I Matrix: (soil/water) WATER Lab Sample ID: ~X~X~3~1~7~6e...._ __ _
I
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I
I
I
I
I
I
I
I
Sample wt/vol: 5.0 (g/mL) !1k.._ Lab File ID: XX3176R
Level: ( low/med) LOW Date Received: 05/05/93
% Moisture: not dee. Date Analyzed: 05/14/93
Column: (pack/cap) CAP Dilution Factor: 1.0 ~~--
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1 1 2 2-Tetrachloroethane . t I I --108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
3 J
91
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
2 J
5 u
5 u
5 u
5 u
1/87 Rev.
m
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: ITAS-KNOXVILLE Contract:
EPA
I Cf g' 1 c
SAMPLE NO, ✓
TRIPBLANK2
I Lab Code: IT STU Case No.: 54011 SAS No.: SDG No.: EX0259
I Matrix: (soil/water) WATER
Sample wt/vol: 5.0 ( g/mL) !11,_
Lab Sample ID: =X=X=3~1~7~7 ___ _
Lab File ID: XX3177 I Level: (low/med) ±L~O~W __ Date Received: 05/05/93
% Moisture: not dee. Date Analyzed: 05/13/93 I Column:
I
I
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I
I
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I
I
I
I
I
I
(pack/cap) CAP Dilution Factor: 1.0 =~--
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
540-59-0--------1,2-Dichloroethene(Total) __
67-66-3---------Chloroforrn
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Brornodichlorornethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibrornochlorornethane
79-00-5---------1,1,2-Trichloroethane
71-43~2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Brornoforrn
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
3 J
40
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
lA
0
m VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: ITAS-KNOXVILLE contract:
EPA SAMPLE NO~ 5
TRIPBLANK
Lab Code: ITSTU case No.: 54029 SAS No.: ____ SDG No.: EX0159 I Matrix: (soil/water) WATER Lab Sample ID: =X=X=3=3=5~4 ___ _ Sample I Level:
wt/vol:
(low/med)
5.0
LOW
( g/mL) M1_ Lab File ID: XX3354R
Date Received: 05/06/93 I% Moisture: not dee. Date Analyzed: 05/15/93
Column: (pack/cap) CAP Dilution Factor: ~l~-~o __ _ I
I
I
I
I
I
I
I
I
I
I
I
I
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Acetone
75-15-0---------carbon Disulfide 75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroforn
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
•
(Total)
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride 108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __ 75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
__ 108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
3 J
10 u
5 u
5 u
5 u
5 u
21
5 u
10 u
5 u
5 u
10 u
1 J
5
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
26, I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I Lab Name: ITAS-KNOXVILLE Contract:
TRIPBLANK2
Lab Code: ITSTU Case No.: 54029 SAS No.: SDG No.: EX0159 I Matrix: (soil/water)
Sample wt/vol: I Level: ( low/med)
WATER
5.0 (g/mL) fil,___
LOW
Lab Sample ID: XX3355
Lab File ID: XX3355
Date Received: 05/06/93
1 % Moisture: not dee. Date Analyzed: 05/15/93
I
I
I
I
I
I
I
I
I
I
I
I
I
Column: (pack/cap) CAP Dilution Factor: ~1~-~o __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(Total)_
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Xylene (total)
FORM I VOA
Q
10 u
10 u
10 u
10 u
4 J
77
5 u
5 u
5 u
5 u
5 u
2 J
10 u
5 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
1 J
5 u
5 u
5 u
5 u
1/87 Rev.
n
I
•
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
EX-01-5193
EX-04-5/93
EX-03-5/93
NS-15-5193
NS-09-5/93
NS-11-5/93
NS-10-5193
CHLORIDE ANALYSIS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter (ppm)
Lab Sample ID
P5048/P5049
XX3363
XX3364
XX3365
XX3366
XX3367
XX3368
XX3369
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Result
0.5
6.5
23
29
950
2,300
1.0
1,000
NA
ITEK 54029
NA
05112193
Qualifier
u
I u Compound was analyzed for but not detected. The number is the detection limit for the sample.
I
1236
I
m
u
0
n
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
NS-31-5/93
NS-29-5/93
NS-29B-5/93
NS-30-5/93
NS-32-5/93
EX-02-5/93
CHLORIDE ANALYSIS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Lab Sample ID
P5048
XX3186
XX3187
XX3188
XX3189
XX3190
XX3191
U -Compound was analyzed for but not detected. The number is the detection limit for the sample.
NA
ITEK 5401 I
NA
05/ I 2/93
Result
0.5 u
140
34
11
22
4.5
460
I Io~
I
D
D
D
D
0
D
D
m
m
m
•
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
EX-01-5/93
EX-04-5/93
EX-03-5/93
NS-15-5/93
NS-09-5/93
NS-I 1-5/93
NS-10-5/93
TOTAL DISSOLVED SOLIDS ANALYSIS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter (ppm)
Lab Sample ID
P5037
XX3363
XX3364
XX3365
XX3366
XX3367
XX3368
XX3369
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Result
204
488
968
2,630
4,130
2,390
478
NA
ITEK 54029
NA
05/07 /93
Qualifier
u
u Compound was analyzed for but not detected. The number is the detection limit for the sample.
1237
I
I
I
I
I
I
I
m
u
E
I
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
NS-31-5/93
NS-29-5/93
NS-29B-5/93
NS-30-5/93
NS-32-5/93
EX-02-5/93
TOTAL DISSOLVED SOLIDS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Lab Sample ID
P5034/P5035
XX3186
XX3187
XX3188
XX3189
XX3190
XX3191
u -Compound was aoalyzed for but not detected. The number is the detection limit for the sample.
NA
ITEK 5401 I
NA
05/06/93
Result
u
744
582
454
606
250
2540
l l O 5
I
I
I
I
I
I
I
n
u
I
I
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
Method Blank
EX-01-5/93
EX-04-5/93
EX-03-5/93
NS-11-5/93
NS-10-5/93
CHEMICAL OXYGEN DEMAND ANALYSIS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter (ppm)
Lab Sample ID
P505l
P5050
XX3370
XX337l
XX3372
XX3373
XX3374
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Result
5.525
5.625
50
85
348
473
616
NA
ITEK 54029
NA
05/10/93
Qualifier
U Compound was analyzed for but not detected. The number is the detection limit for the sample.
1238
I
I
I
I
I
I
I
I
I
I
I
I
I
D
D
u
m
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
EX-02-5/93
CHEMICAL OXYGEN DEMAND
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Lab Sample ID
P5052
XX3192
NA
ITEK 54011
NA
05/10/93
Result
5.6
902
1 1 06
I
I
I
I
I
g
0
m
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
EX-01-5/93
EX-04-5/93
EX-03-5/93
NS-I 1-5/93
NS-l0-5/93
TOTAL K,JELDAHL NITROGEN ANALYSIS
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter (ppm)
Lab Sample ID
P5046/P5047
XX3370
XX3371
XX3372
XX3373
XX3374
SDG Number:
Job Number:
Collection Date:
Analysis Date:
.
Result
0. I
0.7
0.4
0.7
180
2.0
NA
ITEK 54029
NA
05/10/93
1239
Qualifier
u
I u Compound was analyzed for but not detected. The number is the detection limit for the sample.
I
I
I
I
I
I
I
I
g
0
E
I
I
I
I
I
I
I
I
I
I
Laboratory Name:
Contract Name:
Sample Matrix:
Concentration Units:
Client Sample ID
Method Blank
EX-02-5/93
TOTAL KJELDAHL NITROGEN
IT AS-KNOXVILLE
NATIONAL STARCH
WATER
mg/liter
SDG Number:
Job Number:
Collection Date:
Analysis Date:
Lab Sample ID
P5046
XX3192
U -Compound was analyzed for but not detected. The number is the detection limit for the sample.
NA
ITEK 54011
NA
051 l0193
Result
JO u
2.8
1 1 0 7
____ om.. a!II
TECHNOLOGY
'---~CORPORATION
!!!!!I a!!!IA .. YSIS REiii:SfitiN[ji&I
CHAIN OF CUSTODY RECORD*
iiii Merr:M LJJSBl11e"'-'o.-. • -
Page 1 of~
Samples Shipment Date !_,_z;i/~/l3,~---'-_
Lab Destination ~T--<I ..... -, . ,(j '''-1 ,.8 ~-/,--· --·-~ ---4 D
. Lab Contact ';s,,,,,.,i---\'L'-'-'-'-;_·"'· ___ -· · -· §
4 · / 12L:c·./•~ f.),. • /{ · 3 Project Manager_,,L.(-L .... J-'-''••L:L .. _L..__ Project Contact/Phone -'-~CLLL'J~_:_·,:,/___ 10 · ,1, u
/ . . 13 fF,,_,Qe r"'-/ Ev,a•·<..LI Report to: _,;c.~_V..:...LJ .......... )•-),'--cc.:<,,.-·-~
Purchase Order No._~.......6!-;-f·-~'-· ·_____ · Carr1er/Wayb1II No. ___ ~_:,i:_9_0.J:/L+...3.---,--r ,_C"'-r,rL,-. . gj
Required Report Date _1_1-_5= /
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Sample 14 Sample 15 Date/Time 16 Cantainer1 Sample 1 Pre-19 Requested Testing 20
Number Descriptian/Tvae Collected Tune Volume sen,ative Praaram
Condition on 21
Receiat
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Record Na.
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Possible Hazard Identification: 24 -' Sample Disposal: 25 ,· . ·· • -·· ~
N_on-hazard U Flammable l_j' Skin Irritant !_j Poison B l_j · Unknown _;Vj Return to Client l_j Disposal by Lab \J.. Archive __ . ____ (mos.) ~
Turnar.o,..u_nd Time Required: 26 QC Level: 21 · , ~
Norma11,,J Rushl..J 1.1..J 11.1..J 111.l_j Proiect S□ecific (s□ecifv): /' -"''ll..._c_' · • ,· -·-'"·' . ·1-· __ .. . ~
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/ Date: __________ ~_ 2. Received by Date:__ "'
Time: [Signature/Affiliation) Time: 2. Relinquished by
[Signature/ Affiliation]
3. Relinquished by
[Signature/ Affiliation I
Date: _____________ 3. Received by Date:_
Time: (Signature/Affiliation) Time:
Comments: 29
ur•-
TE-ION.
ECHNOLOGY
CORPORATION -- - - --I!!!! e= i::;; ANALYSIS REQUEST AND liiiiii -- - - -Reference Document No.30 ,:::? S-'> J.?:.("'
CHAIN OF CUSTODY RECORD (cont.)* Page__z_of _z_
""-IJ'1\J w1J11fl .. •ll)IU-.• ·-
Project No. ~:¼o:½.c.'l • , 1 , .,{ Samples Shipment Date
Sample 14 Sample 15 _ Date/Time 16 Container 1 i Sample18 Pre--19 Requested Testing 20 Condition on 21 Disposal 22 Number Description/Tune Collected Type Volume servative Program Receiot Record No. " n,
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-l!!!!!!!I a= =a iiiii --------- --Reference Document No. 3 2 2 9 / j rn INTERNATl~NAL
TECHNOLOGY
CORPORATION
ANALYSIS REQUEST AND
CHAIN OF CUSTODY RECORD* Page 1 of --3
~
· Project Name/No.1,A/.J.,..,,Jsf,,._, J.. ~(.~ Samples Shipment Date _7--..,s; {....sj'l..3. .... __ 0-/lni/o,J<// '(-.,/,C... 7i ~al,-,, f_...,
Sample Team Members l ___ -::L . .4.-,:,~·b_____ 1 Lab Destination 8.II.11,!._--:_.t!'/.,_W~'-_______________ .,
Bill to:5 _____ ~j.1J _________ ~-
Pr~fit Center No. 3 Lab Contact 9_::r.,.,.,,,>'__:y_..._.._.__c._____ _ ______________ §
Project Manager~Jtl;J, ,Sf_,.,,.1_._,,,.~1.-f~ Project Contact/Phone ~~~~~h~p~-~/to: 1~_ ~~ ,.,__,,_B.._..,,};,_ ___ ---~
Purctiyse Order No. 6 /',/../_11: Carrier /Waybill No. _1_:¥> 5"' ~ ~ 0 S"'"// ,..7 • ?.;:: _::r_r C...O r~f.._-t_,_"'-:1 .. ---~
11 /. / IC' ,3/ 2.. ,D,_-.,.• ~..-.:,..s ..b_r_ . ' { 3 Required Report Date ___ .,s:: z. c. -~J -----··· .-.... 111 ■ •11111 ■=--~ -··-----. --·· ---------
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Special Instructions: 23 3 a
Possible Hazard Identification: 24 Sample Disposal: 25
Disposal by Lab '}{_
7
Unknown~ "' Non-hazard _J Flammable .J Skin Irritant .J Poison B .J Return to Client .J Archive [mos.] c 0
j QC Level: 27 I r
Turnaround Time Required: 26 L, I(/ !
Normal ~ Rush:.J 111. .J Project Specific (specifv]: 1.:-:PA CLF .2lL C I. .J 11.' .J ii
1 . Relinquished by 28 -O• .. ._fN_ 4/_ 11! --Date: >/._'7'JJ ' ~ Date _ 5/r..,;-/,'N 1 . Received by 28 r"-~ p;:,,,~..;..J C ,. -Time: ~,
[Signature/ Atf1hacionJ ., r-, . -,, ' -Time: ., • r-[S19nature/Aff1haLion) /] .l ·// .11.' / __ r---v> ,-,,, 7 /;, ~ -✓-' , ,, ' Date: " 2. Relinquished by Date: 2. Received by ·-. ... Time: (Signature/ Affiliation) Time: (Signature/ Affiliation)
3. Relinquished by Date: 3. Received by Date:
(Signature/Aff1hatlon) ' Time: (Signature/ Attihationl Time:
' Comments: 29
1 MCA 3115191
rn INTERNATIONAL
TECHNOLOGY
CORPORATION
Project Name d,.,.-1 ;,,_!.,._/ J-1.,.,,.<:c_ ',
ANALYSIS REQUEST AND
CHAIN OF CUSTODY RECORD (cont.)*
Project No. ">-' "a· CC ~
Reference Document No.30 -", 2 2? 7_?
Page Z of l
. /,.
Samples Shipment Date _sj .r; '1_ ._J ____ ...
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Sampla14 Sample 15 Date/Time 16 Conteiner1 Sample18 Pre-19 Requested Testing 20 Condition on 21 Disposal 22 ~
Number Description/TvDB Collected TvPB Volume servative Prnnram Receipt Rscord No. ~·
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-- - - - - - - - --!!l!!I c:::la liiiiiiii iliiiill - - - -rn INTERNATIONAL
TECHNOLOGY
CORPORATION
Project NameA .... --/. o, A/ _ .S--f. v_ ~ \
Sample14 Sample 15
Number Descriptian/Tvae
,1,;__.;, -/ a-c:,-/4 3 c/e_•-r ~ -----,..... ~·
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-
"7'y,n PJ..,L c.lt '"'/4.-( -
• c/-e-~-,, 17:. , {!)., '/L .
ANALYSIS REQUEST AND
CHAIN OF CUSTODY RECORD (cont.)*
Reference Document No.30 .3,:;'? z;
Page~of .3
Project No. ~ cf (, r <I Samples Shipment Date ~0/9,:,
■u.1 ■•.l
~ Date/Time 16 Container 1 1 Sample18 Pre-19 Requested Testing 20 Condition on 21 Disposal 22 :r
Collected Tvae Volume servative Proaram Receipt Record No. £
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