NCD991278540_19960614_Weyerhaeuser Company_FRBCERCLA PA SI_Site Inspection Prioritization - Revised-OCR

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State of North Carolina
Department of Environment, Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary.
William L. Meyer, Director
Ms. Cynthia Gurley
NC CERCLA Project Officer
June 14, 1996
US EPA Region IV Waste Division, 6th Floor
345 Courtland Street, NE
Atlanta, GA 30365
.AVA
DEHNR
Subject: Site Inspection Prioritization -Revised
Weyerhauser Co./Plymouth (NCD 991 278 540)
Plymouth, Martin County, NC
Dear Ms. Gurley:
This revised report contains the findings of the Site Inspection Prioritization (SIP) of the
Weyerhauser Co. /Plymouth site (NCD 991 278 540), locaied on State Road 1565, Plymouth, Martin
County, North Carolina. Please refer to the original June 30, 1995 SIP report for all references,
tables, and figures.
The Weyerhauser Co. site is an active wood and paper products manufacturing facility
located on State Road 1565 in Plymouth, Martin County, NC. Weyerhauser has been in operation
at this site since 1957 when the company merged .with the Kieckhefer-Eddy Co. who began
operations at the site in 1937. The paper bleaching operation began at the site in the mid-1940's. The
Wood Products Division of Weyerhauser produces finished lumber and plywood from raw pine and
hardwoods. Since 1979, Weyerhauser has been treating lumber with a chromated ·copper arsenate
process that produces approximately 1500 pounds of treatment sludge per quarter. A collection
system is used to capture excess treatment solution and sludge which is then shipped off-site to a
RCRA disposal facility.
A mercury cell chlorine plant was operational at the site from approximately 1952 to 1965.
Spent graphite electrodes and marble cells, having absorbed mercury during the chlorine production
process, were disposed ofin an on-site landfill with other mill wastes. The exact quantity of mercury
disposed of during this period is unknown. However, Weyerhauser Co. estimates range from 60
pounds to 11,000 pounds of mercury. A series ofU-drains in the floor of the building collected spilled
process fluid and directed it toward a collection sump which in tum discharged to a drainage trench
that emptied into the Roanoke River. The chlorine production building was demolished in 1987;
approximately 1,300 tons of mercury contaminated soil and
P.O. Box 27687, .
Raleigh, North Carolina 27611-7687
Voice 919-733-4996 f#M£JIPJ&MD
FAX [phone]
An Equal Opportunity Affirmative Action Employer
50% recycled/lO"k post-consumer paper
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Ms. Gurley
June 14, 1996
Page 2
debris was removed to the GSX hazardous waste landfill in Pinewood, South Carolina. The area of
the former building was then backfilled with clean fill and capped with asphalt pavement.
Mercury contaminated soils remain in place at a depth of approximately 4. 5 feet below land
surface due to a high water table. Three shallow (12 ft) monitoring wells were constructed in a
triangular pattern around the area of the former chlorine building. Groundwater from the monitoring
well between the former building and the river consistently reveals elevated levels of mercury. A
background monitoring well is free of mercury contamination.
From the time operations began at the facility, untreated process wastewater from the paper
products division was originally discharged to the Roanoke River. During the period between the
early 1960's and 1968, all untreated process wastewater was discharged to Welch Creek instead of
the Roanoke River. Since 1968, all process wastewater except cooling water has been treated at an
on-site secondary treatment facility prior to discharge. Wastewaier is directed to two settling ponds
where solids are allowed to settle out and removed for burning in the plants' steam boiler.
Wastewater is then sent to an aeration basin and finally to a serpentine retention pond approximately
750 acres in size. During the period between 1968 to 1988, wastewater from the retention pond was
discharged to Welch Creek. Since 1988, Weyerhauser has been discharging treated process
wastewater to the Roanoke River at a point approximately 1/2-mile downstream of the facility. The
Weyerhauser Paper Company currently holds an NPDES Permit (# 0000680) to discharge treated
wastewater, non-contact cooling water, and storm water runoff to the Roanoke River . Under the
permit, Weyerhauser has a discharge limit of 1.3 pg/I of dioxin and is required to sample its effluent
quarterly. Weyerhauser's original NPDES Permit was issued in 1975.
In 1985, a Site Inspection was conducted by the North Carolina Solid and Hazardous Waste
Management Branch/CERCLA Unit. No sarnpling was conducted during the Site Inspection. A fish
consumption advisory has been issued by the NC Division of Environmental Management for the
Roanoke River and Welch Creek based on fish tissue samples collected in 1988 exhibiting high dioxin
concentrations.
Sampling for the Weyerhauser Co. SIP (June 19-20, 1995) focused on sediment and surface
water samples collected from the Roanoke River which is a closed fishery and has significant wetland
surface water pathway frontage. Sediment and surface water samples were also collected from
Welch Creek. An off-site drinking water sample was collected from the nearest residential well
located at the James Johnson residence; an on-site .drinking water sample was collected from
Weyerhauser well #13. All samples were analyzed under the U.S. Environmental Protection Agency
(EPA) Contract Laboratory Program (CLP). No further waste/source sampling was performed at
the facility during the SIP.
Prior sampling data indicates that the shallow groundwater aquifer and subsurface soils under
the former chlorine production building have been impacted by a release of mercury. Elevated levels
of dioxin/furan have also been found in fish tissue samples collected from the Roanoke River and
Welch Creek below Weyerhauser discharge points. The laboratory analytical data for sediment
samples collected from the surface water pathway during the SIP indicate that an observed release
of mercury has occurred, as well as the same isomers of dioxin/furan detected in fish tissue.
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Ms. Gurley
June 14, 1996
Page 3
The drinking water samples were found to be free of chemical contaminants. Based on the above
factors, it is apparent that the site poses a threat to human health and the environment and is in need
of additional action under CERCLA/SARA. The \yeyerhauser Co./Plymouth site is therefore
recommended to receive a low priority status for an Expanded Site Inspection assignment.
If you have any questions, please feel free to contact me at [phone].
Sincerely,
G. Doug Rumford
Hydro geologist
NC Superfund Section
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STATE OF
NORTH CAROLINA
Department of Environment, Health,
and Natural Resources
Division of Solid Waste Management
Superfund Section
REVISED SITE INSPECTION PRIORITIZATION
Weyerhauser Co./Plymouth Wood Treating
NCD 991 278 540
Plymouth, Martin County, North Carolina
Reference No. 03156
June 1996
George D. Rumford
Hydrogeologist
Division of Solid Waste Management
Superfund Section
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Prepared by:
REVISED SITE INSPECTION PRTORITIZA TTON
Weyerhauser Co./Plymouth Wood Treating
NCD 991 278 540
Plymouth, Martin County, North Carolina
Reference No. 03156
June 1996
Superfund Section
Division of Solid Waste Management
North Carolina Department of Environment, Health
and Natural Resources
&----y-Q VJ
George D. Rumford
Hydrogeologist
fuiieRosa
CERCLA BranchHead
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TABLE OF CONTENTS
EXECUTIVE SUMMARY
1.0 INTRODUCTION ............................................... 1
2.0 SITE DESCRIPTION, Operational History, and Waste Characteristics ...... 1
2.1 Site Location ................................................ 1
2.2 Site Description ................... · ........................... 1
2.3 Operational History and Waste Characteristics ...................... 2
3.0 WASTE/SOURCE SAMPLING .................................... 4
4.0 GROUNDWATERPATHWAY .................................... 4
4.1 Hydrogeologic Setting ........................................ 4
4.2 Ground Water Targets ........................................ 5
4 .3 Sample Locations ............................. ·. . . . . . . . . . . . . . . 6
4 .4 Analytical Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
4. 5 Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
5.0 SURFACE WATER PATHWAY ................................... 7
5.1 Hydrologic Setting ........................................... 7
5.2 Surface Water Targets .............. : .......................... 8
5.3 Sample Locations ............................................ 8
5 .4 Analytical Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
5. 5 Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
6.0 SOILEXPOSUREANDAIRPATHWAYS .......................... 10
6.1 Physical Conditions ................. ·. . . . . . . . . . . . . . . . . . . . . . . . . 10
6.2 Soil and Air Targets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
6.3 Sampling Locations ......................................... 11
6.4 Analytical Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
6.5 Conclusions ................................................ 11
7.0 SUMMARY AND CONCLUSIONS ................................ 12
PHOTOGRAPHS
APPENDIX A
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EXECUTIVE SUMMARY
The Weyerhauser Co. site is an active wood and paper products manufacturing facility
located on State Road 1565 in Plymouth, Martin County, NC. The site consists of the Weyerhauser
Paper Co. (WPC) and the Weyerhauser Forest Products Division (WFPD). The WPC has been in
operation at this site since 1957 when the company merged with the Kieckhefer-Eddy Co. who began
operations at the site in 1937. The paper bleaching operation began at the site in the mid-1940's. The
WFPD produces finished lumber and plywood from raw pine and hardwoods. Since 1979, WFPD
has been treating lumber with a chromated copper arsenate process that produces approximately 1500
pounds of treatment sludge per quater. Excess treatment solution and sludge is shipped off-site to
a RCRA disposal facility.
A mercury cell chlorine plant was operational at the WPC facility from approximately I 952
to 1965. Spent graphite electrodes and marble cells, having absorbed mercury during the chlorine
production process, were disposed of in an on-site landfill with other mill wastes. The estimated
quantity of mercury disposed of by WPC during this period ranges from 60 pounds to 11,000
pounds. Spilled process fluid was collected in a series of U-drains in the floor of the building and
discharged into the Roanoke River. The chlorine production building was demolished in I 987 and
mercury contaminated soil was excavated to a depth of. 4. 5 feet. The area was then backfilled with
clean fill and capped with asphalt pavement. Groundwater samples from two of the three shallow
(12 ft) monitoring wells in the area of the former chlorine building revealed elevated levels of
mercury. The background monitoring well is free of mercury contamination. The WPC currently
holds an NPDES Permit(# 0000680), originally issued in 1975, to discharge treated wastewater, non-
contact cooling water, and storm water runoff to the Roanoke River. Under the permit, Weyerhauser
has a discharge limit of 1.3 pg/I of dioxin and is required to sample its effluent quarterly.
In 1985, a Site Inspection was conducted by the North Carolina Solid and Hazardous Waste
Management Branch/CERCLA Unit. No sampling was conducted during the Site Inspection. A fish
consumption advisory has been issued by the NC Division of Environmental Management for the
Roanoke River and Welch Creek based on fish tissue samples collected in 1988 exhibiting high
dioxin/furan concentrations.
Sampling for the Weyerhauser Co. SIP (June 19-20, 1995) focused on sediment and surface
water samples collected from the Roanoke River and Welch Creek, both having received untreated
wastewater from WPC. An off-site drinking water sample was collected from the nearest residential
well located at the James Johnson residence; an on-site drinking water sample was collected from
Weyerhauser well #13. All samples were analyzed under the U.S. Environmental Protection Agency
(EPA) Contract Laboratory Program (CLP). No further waste/source sampling was performed at
the facility during the SIP.
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Prior sampling data indicates that the shallow groundwater aquifer and subsurface soils under the
former chlorine production building have been impacted by a release of mercury. Elevated levels of
dioxin/furan have also been found in fish tissue samples collected below Weyerhauser discharge
points. The laboratory analytical data for sediment samples collected from the surface water pathway
during the SIP indicate that an observed release of chromium, mercury, nickel, vanadium, and
dioxin/furan to sediments of the Roanoke River and Welch Creek has occurred. The isomers of
dioxin/furan found in sediments of the surface water pathway are the same as those that have been
detected in fish tissue samples. The drinking water samples were found to be free of chemical
contaminants. Based on the above factors, it is apparent that the site poses a threat to human health
and the environment and is in need of additional action under CERCLNSARA. The Weyerhauser
Co./Plymouth site is therefore recommended to receive a low priority status for an Expanded Site
Inspection assignment.
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1.0 INTRODUCTION
Under the authority of the Comprehensive Environmental Response, Compensation, and
Liability Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization Act of 1986
(SARA), the North Carolina Superfund Section conducted a Site Inspection Prioritization (SIP) of
the Weyerhauser Co./Plymouth (NCD 991 278 540) (WCP) facility in Plymouth, Martin County,
North Carolina. The purpose of this investigation was to update information on conditions at the
Weyerhauser site. Information regarding potentially impacted populations and sensitive environments
not documented in the original Site Inspection report, March 21, 1986, was also updated. This data
was used to assess the threat posed to human health and the environment and to determine the need
for additional CERCLNSARA or other appropriate action. The scope of the Site Inspection
Prioritization included review of available file information, a revised target survey, on-site
reconnaissance (August 22, 1994), on and off-site sampling (June 19&20, 1995), and a more
thorough evaluation of the surface water pathway.
2.0 SITE DESCRIPTION, OPERATIONAL HISTORY, AND WASTE
CHARACTERISTICS
2.1 Location
The Weyerhauser Co. facility is located in a suburban area.of Plymouth, NC on State Road
1565, approximately 1.5 miles west of the downtown district. The site is-located at 35° 51' 47" North
Latitude and 76° 46' 46.5" West Longitude (Refs. l; 2). The 2-year, 24°hour rainfall is approximately
4 inches (Ref 3). Normal annual total precipitation in this area is 50 inches. Mean annual lake
evaporation in this area is 41 inches, yielding a net annual rainfall of9 inches (Ref 4).
The area is characterized by a flat, low lying topography with elevation increasing south of
the facility. The elevation of the facility is 5 feet above mean sea level (MSL). The surrounding areas
range in elevation from 5 feet above MSL to 15 feet above MSL within a I mile radius of the site
(Fig. 1).
2.2 Site Description
The Weyerhauser Co. site is an active manufact~ring facility located on State Road 1565 in
Plymouth, Martin County, NC. There are two operational divisions at the facility, the pulp and paper
products division and the forest products division. The facility consists of several buildings,
warehouses, kilns, boilers, storage areas, and milling equipment utilized in the production of paper
and finished lumber products. The total combined area of the site is approximately 2400 acres (Figs.
1; 2). Access to the facility from State Road 1565 is restricted by two guarded gatehouses; a fence
surrounds the perimeter of the pulp and paper mill. Access to the site from the south is only
restricted by woodlands and from the east by Welch Creek (Refs. 6, p.1; 43). The mill is bounded to
the north by the Roanoke River, to the east by Welch Creek and suburban areas of Plymouth, to the
west by wetlands, and to the south by rural and undeveloped woodland (Fig. I).
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The site is primarily covered with asphalt although some sections are hard packed dirt and
gravel or grass covered (Ref 6, pp.1,3,4; Photos). The site borders the city limits of the City of
Plymouth. The nearest school, Plymouth High School, is located approximately 2.5 mile east of the
site (Fig. I). The nearest off-site residence is located approximately I mile southeast of the paper
products facility (Fig. 1). There are approximately 6616 residents within a 4-mile radius of the site
(Refs. 37; 39).
2.3 Operational History and Waste Characteristics
. Weyerhauser has been in operation at this site since 1957 when the company merged with
the Kieckhefer-Eddy Co. (Ref 5). The Kieckhefer-Eddy Co., which began operations at the site in
1937, also manufactured wood pulp. The paper bleaching operation began at the site in the mid-
1940's (Ref 43). Current operations at the facility include those of the Weyerhauser Paper Company
and the Weyerhauser Forest Products Division. The Weyerhauser Paper Co. produces wood pulp,
finished paper, and paperboard (Ref. 8; Fig. 2). The Forest Products Division of Weyerhauser
produces finished lumber and plywood from raw pine and hardwoods (Ref 9; Fig. 3).
Since 1979, the forest products division has been treating lumber with a chromated copper
arsenate (CCA) process that produces approximately I 500 pounds of treatment sludge per quarter
(Refs. 6, p.5; 9). No wood treating took place prior to 1979 and no creosote or pentachlorophenol
has been used in the wood treating process. Wood treaiment sludges have not been disposed of on-
site. A sealed drip pad with collection system is used to capture excess treatment solution and sludge
which is then shipped off-site to a RCRA disposal facility (Refs. 6, p.4; 9). The entire treatment area
is covered with a roof structure to reduce surface water runoff(Ref 6, p.4; Photos). In January of
1995, the RCRA classification for the Weyerhauser Forest Products Division was changed from
small quantity generator to large quantity generator (Refs. 7; I 0).
A mercury cell chlorine production plant was operational at the paper company facility from
approximately 1952 to 1965 (Ref 6, p.1; Fig. 4). Spent graphite electrodes and marble cells, having
absorbed mercury during the chlorine production process, were routinely disposed of in an on-site
landfill with other mill wastes (Ref. 14). The tanks and process vessels were removed from the
building in 1979 and disposed ofin the on-site landfill (Refs. 12; 14). The exact quantity of mercury
disposed of during this period is unknown. However, Weyerhauser Co. estimates range from 60
pounds to 11,000 pounds of mercury (Refs. 11, p.5; 12; 13). A series ofU-drains in the floor of the
building collected spilled process fluid and directed it toward a collection sump which in turn
discharged to a drainage trench that emptied into the Roanoke River (Refs 6, p.1; 15, p.2-1).
The chlorine production building was demolished in 1987; approximately 1300 tons of
mercury contaminated soil and debris was removed to the GSX hazardous waste landfill in Pinewood,
South Carolina (Refs. 6, p. l; 15, pp.3-2, 4-1). The concrete building slab was demolished and
removed in 1992; the collection sump and section ofU-drain from the building to the river bank was
also removed (Ref 15, pp.4-2, 4-4). Approximately 90 feet of U-drain located west of the chlorine
building was not removed (Ref 15, fig. 8). Mercury contaminated soil beneath the slab and U-drain
was excavated to a depth ranging from 4 feet to 5 feet below grade (Ref 15, p.4-3). All excavated
areas of the former building were then backfilled with clean sand fill, graded to match existing surface
elevation, and a surface runoff collection system was installed. The area was then capped with
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asphalt pavement (Ref 15, pp.4-3,4-7).
A total of 3,130 tons of debris was transported to the GSX landfill for disposal (Ref 15, p.4-
6). The area of excavation and subsurface soil sampling points/mercury concentrations are illustrated
in Figure 8 of Reference 15.
In 1987, three shallow (12 ft) monitoring wells, located in a triangular pattern around the area
of the former chlorine building, were constructed at· the site. Groundwater from the two wells
between the former building and the river consistently reveal elevated levels of mercury; mercury has
not been detected in the background well (#3). Monitoring well #3 was abandoned when the railroad
tracks surrounding it were removed (Refs. 6, p.2; 15, pp.2-2, 6-4, fig. 3; 16).
From the time operations began at the facility, untreated process wastewater from the paper
products division was originally discharged to the Roanoke River. During the period between the
early 1960's and 1968, all untreated process wastewater was discharged to Welch Creek instead of
the Roanoke River. Since 1968, all process wastewater except cooling water has been treated at an
on-site secondary treatment facility prior to discharge. Wastewater is directed to two settling ponds
where solids are allowed to settle out and removed for burning in the plants' steam boiler.
Wastewater is then sent to an aeration basin and finally to a serpentine retention pond approximately
750 acres in size. During the period between 1968 to 1988, wastewater from the retention pond was
discharged to Welch Creek (Refs. 6, p.3; 20, p.97; Fig. 4). Since 1988, Weyerhauser has been
discharging treated process wastewater to the Roanoke River at a point approximately 1/2-mile
downstream of the facility (Ref 6, p.1). The Weyerhauser Paper Company currently holds an
NPDES Permit(# 0000680) to discharge treated wastewater, non-contact cooling water, and storm
water runoff to the Roanoke River. Under the permit, Weyerhauser has a discharge limit of 1.3 pg/I
of dioxin and is required to sample its effiuent quarterly (Ref 28). Weyerhauser's original NPDES
Permit was issued in 1975 (Ref 43). ·
In 1985, a Site Inspection was conducted by the North Carolina Solid and Hazardous Waste
Management Branch/ CERCLA Unit. No sampling was conducted during the Site Inspection (Ref
17). A fish consumption advisory has been issued by the NC Division of Environmental Management
for the Roanoke River and Welch Creek based on high dioxin concentrations in fish tissue samples
(Ref 18, p.14; 19).
Sampling for the Weyerhauser Co. SIP (June 19-20, 1995) focused on sediment and surface
water samples collected from the Roanoke River which is a closed fishery and has significant wetland
surface water pathway frontage. Sediment and surface water samples were also collected from
Welch Creek. An off-site drinking water sample was collected from the nearest residential well
located at the James Johnson residence; an on-site drinking water sample was collected from
Weyerhauser well #13 (Ref 33). All samples were analyzed under the U.S. Environmental Protection
Agency (EPA) Contract Laboratory Program (CLP).
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3.0 WASTE I SOURCE SAMPLING
Potential source areas at the WCP site include the mercury contaminated soil around and
under the former chlorine production building, the inactive on-site landfill, the aeration basin/settling
ponds, and the drip pad area at the wood products division facility. Source samples were not
collected from the site during the Site Inspection ofFebruary 1985. A Final Closure Report of the
former chlorine production building was submitted to the Waste Management Branch of the NC
Hazardous Waste Section by Weyerhauser Paper Company in October 1992. The report describes
a source area approximately 3130 cubic yards in volume, and includes analytical data for mercury
contaminated soil (Ref 15}. No further waste/source sampling was performed at the facility during
the SIP.
The inactive on-site landfill was operational from approximately 1952 until 1978 and is nearly
60 acres in size. This area is currently gravel covered and used as an equipment storage yard; rio
signs of current or past industrial waste dumping were obvious during the site-recon (Ref 6, pp.2,3).
At the wood products division, lumber is treated with CCA in a pressurized vessel and allowed to
drip onto a sealed pad. Excess treatment solution is collected for off-site disposal at a RCRA
approved facility (Ref 6, pp.3,4).
4.0 GROUNDWATER PATHWAY
4.1 Hydrogeologic Setting
The Weyerhauser Co.-Plymouth facility is located within the Coastal Plain Physiographic
Province which is characterized by a flat landscape of coastal swamps and marshes grading to rolling
uplands along the inner margin of the region. The area is underlain by unconsolidated sediments that
consist principally of sand, silt, and clay. These sediments, originally deposited by streams from the
adjoining uplands, have a relatively uniform layering and dip orientation towards the coast. The
greatest thickness of these formations is along the seaward edge of the region (Refs. 21, p.52; 22,
p.23). The predominant formation type of this belt is the sandy, fossiliferous clay of the Yorktown
Formation (Ref 23). The Coastal Plain is covered with a layer of post-Yorktown age surficial
deposits that ranges in thickness from a few feet to ab~ut 3 0 feet.
Soils in the area of the site are primarily of the Craven fine sandy loam, Dorovan muck, and.
Urban land soil series. The Craven soil series is moderately weil drained and nearly level. Typically,
this soil has a dark grayish brown fine sandy loam surface layer 9 inches thick grading to a subsoil of
gray clay loam with red, yellow, and brown mottles to a depth of 67 inches. The Dorovan muck is
nearly level and very poorly drained; it is found in swampy areas near the Roanoke River. This soil
consists of brown to black muck to a depth of 65 inches grading to a gray sand. The areas mapped
as Urban land are areas where natural soils, landscapes, topography, and drainage have been greatly
altered (Ref 29, pp.13,15,24, sheet 9). ·
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In the area of the Coastal Plain region where"the site is located, the surficial deposits are
underlain by the confined Yorktown, Pungo, and Castle Hayne Aquifers (Refs. 24, p. 70; 27, pp.24,
25). The extent of water withdrawal from the aquifers overlying the Castle Hayne in the vicinity of
the site is unknown; no groundwater targets were identified for aquifers other than the Castle Hayne.
The principal source of groundwater in the vicinity of the site is the confined Castle Hayne Aquifer
of the limestone, sandy limestone, and sand Castle Hayne Formation (Refs. 25, p.53; 26, p-330).
Recharge to the surficial aquifer is directly from precipitation. Recharge to the underlying
groundwater system occurs in the upland interstream areas where sand layers crop out (Refs. 22,
p-24; 27, p-14). Discharge from the system occurs by seepage to streams, estuaries, and the ocean.
Movement of water from recharge areas to discharge is controlled primarily by the hydraulic gradients
of the dipping beds (Refs. 21, p.52; 22, p-24).
Site-specific geologic data is not available, however, the Castle Hayne Aquifer is found in
Washington County at a depth ranging from about 120 feet in the western part of the county to about
400 feet in the eastern part (Ref 25, p.53)_ Based on production well depths at and near the site, the
Castle Hayne Aquifer is found at approximately 150 feet below land surface (Refs. 6; 33). Water level
readings collected from three shallow on-site groundwater monitoring wells revealed that
groundwater occurs at the site at a depth between 4.5 to 6.0 feet below ground surface (Ref 15, p.
2-2). The average hydraulic conductivity value for the Castle Hayne Aquifer was estimated to range
between approximately 15 ft/day to 200 ft/day (5.3xJ6·3 cm/sec to 7. lxJ0·2 crn/sec)(Ref 27, p.25).
The average thicknesses for the confining units of the Yorktown, Pungo, and Castle Hayne Aquifers
are 25, 55, and 10 ft. respectively (Ref 27, pp.20,22,25). Vertical hydraulic conductivity values of
the typical clay bed confining unit material range from 6x10·9 cm/sec to 2.35x10·11 cm/sec (Ref 27,
p.60).
4.2 Groundwater Targets
Most residents in the vicinity of the Weyerhauser facility are serviced by the municipal water
system of the City of Plymouth. The city system is supplied by four drilled wells ranging in depth
from approximately 115 to 185 feet and installed in 1964 (Ref 30). The Plymouth system supplies
approximately 4119 residents within the city limits plus another 1850 customers outside the city limits
who are serviced by the Washington County Water Department (Ref 30). All four of the city wells
are located roughly 2.25 miles east of the site (Fig. 1). Based on the depth of these wells, they are
likely screened in the Castle Hayne Aquifer (Ref 25, p.53). The nearest residential well is located
at the James Johnson residence. This well is approximately I. I mile south of the site, is about 160
feet deep, and serves 4 residents (Ref 6, p.6). The Johnson well is also likely screened in the Castle
Hayne Aquifer due to its depth (Ref 25, p.53).
There are nine production wells in use over the entire Weyerhauser facility. Drinking water
at both the paper mill and the wood products facility is supplied by these on-site wells (Refs. 6, p.4;
34). The three wells(#! I, #12, #13) that supply drinking water to the paper mill range in depth from
153 to 183 ft bis and have pumping rates ranging from 590 to 726 gallons per minute (gpm) (Refs.
33, pp.4, 5; 34).
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Two wells are located at the wood yard and not used for drinking. The 4 wells that supply drinking
water to the wood products division are located southwest of the former chlorine production building
at distances ranging from 0.5-mile to I-mile (Ref. 34; Fig. I). There are no designated well head
protection areas located within the 4-mile site radius (Ref. 32). The wells of the Plymouth water
system were the only community wells identified within the 4-mile site radius. There are
approximately 8733 groundwater users within the 4-mile radius of the site (Ref. 35). A breakdown
of the groundwater users per distance ring follows:
4.3 Sample Locations
Distance Ring
0 -1/4 mi.
>1/4-1/2
> 1/2 -I
>1-2
>2 - 3
>3 -4
Total
Groundwater Pop.
178
356
1067
55
6394
683
8733
Two shallow groundwater monitoring wells are located between the former chlorine
production building and the Roanoke River. A third monitoring well, used for background
comparison, was abandoned when the railroad tracks surrounding it were removed. These wells were
last sampled in 1992 and were not resampled during the SIP (Ref. 15, pp. 6-4, 6-5, fig.3). Four
drinking water samples were collected from the paper mill water system by WCP in 1985. These
samples were collected from various faucets and water fountains throughout the mill and submitted
to WaterTest Corp. for analysis. However these samples were only analyzed for select volatile
organic compounds (VOC's) and inorganics (Ref. 3 !).
During the SIP, the Weyerhauser production well# 13, located approximately 1800 feet east
of the former chlorine production building was sampled directly at the well head and a split sample
was provided to Richard Gay of Weyerhauser Co. (Table I; Figs. I; 2). This sample (WC-002-DW)
was submitted for VOC, ~emi-volatile organic compounds (SVOC, dioxin, .and inorganic analysis
(Refs. 33, pp. 4, 5; 34). One off-site drinking water sample (WC-001-DW) was collected for analysis
during the SIP and analyz,:d for VOC's, SVOC's, dioxin, and inorganics (Ref. 33; Fig. !). This
sample was collected from the James Johnson residential well located approximately 1.1 mile south,
and slightly upgradient of the former chlorine production building. All SIP sampling locations are
illustrated in Figure 6. No private drinking water wells were identified downgradient of the site
(Ref. 33; Fig. !). The City of Plymouth is required to perform yearly sampling of its water system
for VOC's, SVOC's, and inorganics. The results of the latest sampling analysis were provided by the
city, consequently, these wells were not resampled during the SIP.
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4.4 Analytical Results
At the time of the SIP sampling event, organic compound analytical results for post-treatment
samples collected from the City of Plymouth system in October I 993 and June 1994 were available.
No chemical contaminants were detected above maximum contaminant levels allowable in NC public
drinking water supplies (Ref. 36). Inorganic chemical analyses for the city system was available from
1995. Detected inorganics included fluoride, nitrate, iron, sulfate, and sodium; none of which were
above allowable limits (Ref. 36).
Mercury was detected in monitoring wells MW-IB & MW-2, in 1992, at concentrations of
0.0142 mg/Land 0.0005 mg/L respectively. These wells are located between the river and the
former chlorine building. Mercury was not detected in the background (MW-3) monitoring well (Ref.
15, pp. 6-4, 6-5, table 4). Therefore an observed release· of mercury to the shallow aquifer of the site
has been previously documented. Iron and sodium were the only inorganics detected in the 1986
paper mill drinking water samples; mercury was not detected nor were any VOC's (Ref. 31 ).
Laboratory analytical data for the groundwater pathway samples collected during the SIP
indicate that drinking water supplies have not been impacted by conditions at the site. The Johnson
residential well and the Weyerhauser well #13 were both free of chemical contaminants (App. A).
4.5 Conclusions
Most of the residents in the vicinity of the site receive their potable water from the City of
Plymouth water system which is supplied by four wells located approximately 2.25 miles east of the
site. Those residents within the 4-mile site radius that do not receive city-supplied drinking water
utilize private wells for drinking water. The nearest off-site drinking water well, relative to the former
Weyerhauser chlorine production building, is located approximately 1.1 mile south at the Johnson
residence. There are several on-site production wells that are blended into a combined water system
for drinking water at the facility. The Johnson well and the downgradient Weyerhauser well closest
to the former chlorine production building were sampled during the SIP. An observed release of
rnercury to the surficial groundwater aquifer has been previously documented in two monitoring
wells at the pulp and paper mill portion of the site. f!:owever, the surficial aquifer is not used for
drinking water. The primary drinking water aquifer in the area, the Castle Hayne Aquifer, has not
been impacted by conditions at the site.
5.0 SURFACEWATERPATHWAY
5.1 Hydrologic Setting
The Weyerhauser Co./Plymouth site is located in the watershed of Welch Creek near its
mouth at the Roanoke River. All surface run-off from the site is directed to the waste water
treatment facility (Ref. 6, p. l ). Treated wastewater, non-contact cooling water, and storm water
runoff are currently discharged to the Roanoke River at a point approximately 0.6 mile downstream
of the mill (Refs. 16; 28; Fig. !).
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During the period of operation of the chlorine production plant ( 19 52-1965), process waste
water was discharged directly to the Roanoke River. From this probable point of entry (PPE #I), the
Roanoke River continues for 8 miles to the Albemarle Sound (Fig. 5). The area of the former
chlorine production building was paved over following its demolition and removal. All storm water
run-off from this area is now directed to the waste water treatment facility (Ref. 6, p. I).
Prior to 1988, wastewater from the treatment system was discharged to Welch Creek (Refs.
6, p.3; 20, p.97; Fig. 4). From this former discharge point (PPE #2), Welch Creek flows
approximately 2.5 miles northeast to its confluence with the Roanoke River. The surface water
pathway continues 7 more miles along the Roanoke River to the Albemarle Sound where the 15-mile
target distance limit ends (Fig. 5).
A floodplain map was unavailable for the section of Martin County where the site is located.
However, based upon the topography of the area, the Weyerhauser facility is most likely located
within the JOO-year floodplain of the Roanoke River and Welch Creek. Mean annual flow rates along
the surface water pathway were calculated for the Roanoke River and Welch Creek. The average
annual outflow of the Roanoke River at the mouth is about 8900 cubic feet per second (cfs). The
flow rate of Welch Creek at the mouth is approximately I 1.5 cfs (Ref. 40).
5.2 Surface Water Targets
There are no surface water intakes located along the IS-mile surface water pathway (Ref. 38).
The entire course of the Roanoke River, including the Albemarle Sound, is not suitable as a water
supply source. These waters are classified as being suitable for aquatic life propagation and survival,
primary and secondary recreation and agricultural use (Ref. 41 ). Recreational fishing is documented
along the Roanoke River, however, the segment of river below the city of Williamston to the
Albemarle Sound and the section of the sound to Bull Bay has been issued a fish consumption
advisory. The fish consumption advisory includes all of the 15-mile surface water pathway. The
entire channel of Welch Creek has also been closed to fishing (Ref. 19). A state wide dioxin study
was undertaken by the NCDEM in 1988 to evaluate the impact of pulp and paper mill discharge on
the aquatic environment. Elevated levels of dioxin found in fish tissue prompted the State Health
Director to issue the fish consumption advisory (Ref. 18, p.1,2,39). During the sampling activities
of the SIP, fishing was observed along the banks of the Roanoke River (Ref. 33, p.5). Approximately
13.5 miles of wetland frontage is located along the Roanoke River below PPE #1 (Fig. !). The
habitat of one State classified species of special concern, the Tidewater Mucket, was identified along
the 15-mile site surface water pathway. The habitat of this freshwater mollusk is located
approximately 6.5 miles downstream of PPE #2 (Ref. _39).
5.3 Sample Locations
Surface water and sediment samples were collected from Welch Creek and the Roanoke River
during the June 1995 SIP (Ref. 33). These samples were collected to determine a release of site
specific contaminants to the surface water pathway. Locations and descriptions of all samples
collected from the surface water pathway are outlined in Table I and shown in Figure 6. The
Weyerhauser Co. collects fish from the Roanoke River and Welch Creek for tissue analysis of
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2,3,7,8-TCDD and 2,3,7,8-TCDF. Weyerhauser then submits the data to the Water Quality Section
ofNCDEM on a quarterly basis (Ref. 42).
5.4 Analytical Results
Laboratory analytical data for the surface water· pathway sediment samples collected during
the SIP indicate that an observed release of 2,3,7,8-TCDD, 2,3,7,8-TCDF, mercury, chromium,
nickel, and vanadium has occurred in Welch Creek and the Roanoke River. In the Roanoke River,
mercury was detected in sediments below PPE #1 (sample WC-107-SD) at a concentration of2. l
mg/kg (ppm) while not being detected in the upstream background sample (WC-008-SD). Mercury
was also detected in sediments ofWelch Creek below PPE #2, in samples WC-005-SD and WC-004-
SD, at concentrations of 1.0 ppm and 0.28 ppm respectively. Chromium was detected in Welch
Creek sediment samples WC-004-SD and WC-005-SD at concentrations of 46 ppm and 98 ppm
respectively. Vanadium was detected in sample WC-004-SD at a concentration of 68 ppm; nickel
was detected in sample WC-005-SD at a concentration of 21 ppm. The concentrations of mercury,
vanadium, and nickel in the upstream Welch Creek background sediment sample (WC-006-SD)
were below the laboratory minimum quantitation limit while chromium was detected at 8. 7 ppm (App.
A).
At the PPE#l sediment sample location (WC-107-SD), 1,2,3,6,7,8-HCDD was detected at
6.5 ng/kg (ppt). Downstream ofPPE #2, estimated concentrations of 2,3,7,8-TCDD in sediment
samples WC-005-SD, WC-004-SD, and WC-003-SD were detected at 23J ppt , 17J ppt, and 2. IJ
ppt respectively; 2,3, 7,8-TCDF was also detected in these samples at concentrations of 160 ppt, 89
ppt, and 10 ppt respectively. Background concentrat"ions of2,3,7,8-TCDD and 2,3,7,8-TCDF in
sediment sample WC-008-SD, upstream in the Roanoke River, were below the laboratory minimum
quantitation limit. Background concentrations of 2,3, 7,8-TCDD and 2,3,7,8-TCDF in sediment
sample WC-006-SD, upstream in Welch Creek, were 4.9J ppt and 39 ppt respectively (App. A).
Dioxin analysis offish tissue samples collected in I 993 indicate levels of 2,3, 7,8-TCDD in channel
catfish as high as 18.5 ppt and 2,3,7,8-TCDF levels in white perch as high as 18 ppt (Ref. 42).
5.5 Conclusions
The Roanoke River and Welch Creek have been closed to fish consumption due to elevated
levels of dioxin/ furan in the fish. An observed release of the same dioxin / furan isomers found in
fish tissue samples was documented in sediments of Welch Creek and the Roanoke River below PPE
# 2. An observed release of mercury has been documented in sediments of the Roanoke River
downstream of PPE # 1; mercury vanadium, nickel, and chromium have been detected in sediments
of Welch Creek downstream of PPE #2. The former probable point of entry of paper production
chemical contaminant migration to.Welch Creek is at PPE #2, approximately 2.5 miles upstream of
its mouth. Process waste water from the former chlorine production building was discharged io the
Roanoke River at PPE #1, located approximately I-mile upstream of the Welch Creek mouth.
Currently, treated waste water is discharged at a penpitted discharge point on the Roanoke River
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approximately 0.6 mile downstream of the paper mill.
The surface water pathway includes i 3 .5 miles of wetland frontage. The habitat of one State
classified species of special concern was identified along the 15-mile site surface water pathway.
There are no drinking water intakes located on the surface water pathway within the 15-mile site
target distance limit.
6.0 SOIL EXPOSURE AND AIR PATHWAY
6.1 Physical Conditions
Access to the facility from State Road 1565 is restricted by two guarded gatehouses; a fence
surrounds .the perimeter of the pulp and paper mill. Access to the site from the south is only
restricted by woodlands and from the east by Welch Creek (Refs. 6, p.l; 43). The former chlorine
production building, the wood treatment and storage area, and the inactive on-site landfill are located
within the perimeter fence; the aeration basin/settling ponds are accessible from the south (Figs. 1;3).
The site is primarily covered with asphalt although some sections are hard packed dirt and gravel or
grass covered (Ref. 6, pp.1,3,4; Photos). At the forest products division, the area in the vicinity
of the wood treating operation is gravel covered (Ref. 6, p.4; Photos).
Following destruction of the former chlorine building and the excavation of the underlying soils to
a depth of 4.5 feet bis, a surface runoff collection system was installed and the area was then capped
with asphalt pavement (Ref. 15, pp.4-4,4-7).
6.2 Soil and Air Targets
Activities at the Weyerhauser Co. facility require the efforts of approximately 1610 workers
on site per work day (Fig. 2). There are no households located within a I mile radius of the former
chlorine production building. The nearest school, Plymouth High School, is located approximately
2. 5 mile east of the site ( Fig. I). The nearest off-site residence is located approximately 1 mile
southeast of the paper products facility (Fig. 1). There are a total of 6616 residents living within 4
miles of the site (Ref. 37; 39). A breakdown of the residential population per distance ring follows:
Distance Ring
>O -1/4 mi.
>1/4-1/2
> 1/2 -.1
>1-2
>2 -3
>3 -4
Total
10
Residential Pop.
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2567
1244
6616
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There is one State classified significantly rare animal species habitat within the 4-mile site radius. A
total of8000 acres of wetlands have been identified within 4-miles of the site; the nearest wetland,
an island in the Roanoke River approximately 40 acres in size, is located 600 feet north of the former
chlorine building (Ref 39; Fig. I).
6.3 Sample Locations
No off-site soil sampling was conducted during the SIP, nor were any samples collected from
on-site at either the forest products division or at the paper mill. However, a total of 129 on-site
subsurface soil samples were collected by OHM Remediation Services (OHM) and/or Harding
Lawson Associates (HLA) following excavation of the chlorine building foundation in 1992. These
samples were analyzed for total mercury only. Collection locations for these samples included under
and around the-building foundation and along the U-drain to the river; collection depths ranged from
I foot bis to 5 feet bis (Ref 15, pp.6-2, 6-3, 6-4, fig. 7). No air sampling was conducted as no source
areas were disturbed by sampling during the SIP.
6.4 Analytical Results
Mercury concentrations in the 129 soil samples collected from the area of the chlorine
building ranged from below detection limit to 9520 mg/kg. Excavation operations were halted at
approximately 4.5 feet bis when groundwater was encountered.
Consequently, soils with niercury concentrations as high as 9520 mg/kg were left in place (Ref 15,
pp. 4-3, 6-3, table IA, table IB, fig. 8). Mercury was detected in soil samples S-59 and S-62 at
concentrations of 59.8 ppm and 23.4 ppm respectively. Both samples were collected at a depth of
I foot bis from a gravel and grass covered area near the fence along the river. The soils at these two
sample locations were not excavated (Ref 15, table IB, fig. 8; Photos).
6.5 Conclusions
Subsurface soils around and under the former chlorine production building have been
impacted with high concentrations of total mercury. Contaminated soil to a depth of approximately
4.5 feet bis was removed during excavation of the building's foundation. However, mercury
contaminated soil was left in place under the former chlorine building due to the high water table.
Following the excavation process, a surface runoff collection system was installed and the area was
then capped with asphalt pavement. Surficial soils with elevated levels of mercury also remain in
place along the river. The wood treatment area of th~ wood products division consists of a sealed
drip pad with collection system to capture excess treatment solution and sludge and a roof structure
to reduce runoff to surrounding wood storage areas underlain by gravel. Excess treatment solution
and sludge is collected for shipment off-site to a RCRA disposal facility.
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7.0 SUMMARY AND CONCLUSIONS
The Weyerhauser Co./ Plymouth site was assessed to identify conditions at the site, potentially
impacted populations and sensitive environments. Prior sampling and analytical data has shown that
as a result of practices associated with the chlorine production operation, groundwater in the shallow
aquifer and subsurface soils under the former chlorine production building have been impacted by a ,
release of mercury. Surficial soils with elevated concentrations of mercury are also present along the
river near the former chlorine production building. Elevated levels of dioxin/furan have also been
found in fish tissue samples collected below Weyerhauser process wastewater discharge points.
In 1985, a Site Inspection was conducted by the North Carolina Solid and Hazardous Waste
Management Branch/CERCLA Unit. No sampling was conducted during the Site Inspection. A fish
consumption advisory was issued in 1988 by the NC Division of Environmental Management for the
Roanoke River and Welch Creek. The advisory was based on fish tissue samples collected by
Weyerhauser Co. that exhibited high dioxin/furan concentrations.
On June 19-20, 1995, a SIP was conducted at the site by the NC Superfund Section. Off-site
samples from the surface water pathway and on/off-site drinking water samples were collected to
determine the extent of mercury and dioxin/furan contamination. All samples were submitted for
analysis under the CLP program. No samples were collected from the soil and air pathway, nor were
any waste/source samples collected.
The Roanoke River is a closed fishery and has significant wetland surface water pathway
frontage. Laboratory analytical data indicates that observed release of chromium, mercury, nickel,
vanadium, and dioxin/furan have been documented in sediments of the surface water pathway
downstream of Weyerhauser's former wastewater discharge points. Drinking water samples collected
from the primary drinking water aquifer were free of chemical contaminants. Based on the above
factors, it is apparent that the site poses a threat to human health and the environment and is in need
of additional action under CERCLA/SARA. The Weyerhauser Co./Plymouth site is therefore
recommended to receive a low priority status for an Expanded Site Inspection.
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Photo Number
13-14
15-17
18-19
PHOTO LOG
Weyerhauser Co. -Plymouth
Plymouth, Martin County, NC
NCD 991 278 540
SIP Sampling Event: June 19-20, 1995
Description
Sample collection at WC-007-SD location -photo
taken at discharge point from former chlorine
production building
Weyerhauser Paper Co. production wells I.D. tags
Sample WC-002-DW collection location at Weyerhauser
production well # 13
Photographs 13 -14: Sample collection at WC-007-SD location -photo taken at discharge point from former chlorine production building
Photographs 15, 16: Weyerhauser Paper Co. production wells I.D. tags
Photographs 17: Weyerhauser Paper Co. production wells I.D. tags
Photographs 18 -19: Sample WC-002-DW collection location at Weyerhauser production well # 13
liiiii liiiiii iiiii iiill liiii iiilii
DRINKING WATER
SAMPLE
WC-001-DW
Chloromethane 10U
Bromomethane 10U
V1nv1 Chloride 10U
Chloroethane 10U
Methvlene Chloride 10U
Acetone 10U
Carbon Disulfide 10U
1, 1-0ichloroethene (1, 1-0ichloroethvlene\ 10U
1, 1-0ichloroethane 10U
1,2-0ichloroethene (Total\ 10U
Chloroform 10U
1,2-0ichloroethane 10U
Methvl Ethv1 Ketone 10U
1, 1, 1-Trichlotoethane 10U
Carbon Tetrachloride 1ou
Bromodi Chloromethane 10U
1 ,2-0ichloronro""ne 10U
CIS-1,3--DichloroOl'ooene 10U
T richloroethene ITrichloroethvlene\ 10U
Dibromochloromethane 10U
1, 1,2-Trichloroethane 10U
Ben.:ene 10U
Trans-1 3--Dichloronro,....ne 10U
Bromoform 10U
Meth vi I sob• ... A Ketone 1ou
Methv1 B· ... ., Ketone 10U
T etrachloroethene IT etrachioroethv1ene' 10U
1, 1,2,2-Tetrachloroethane 10U
Toluene 10U
Chlorobenzene 10U
Ethvt Benzene 10U
Stvrene 10U
Total xv1en~ 10U
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ANALYTICAL DATA SUMMARY
WEYERHAUSER CO., Pl YMOUTH, NORTH CAROLINA, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A -TABLE 1. PURGEABLE ORGANIC □~TA
DRINKING WATER DRINKING WATER SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-101-DV.1 WC-002-DW WC-003-SW WC-003-SO
1DU 10U 10U 14U
1DU 10U 10U 14U
10U 1DU 10U 14U
1DU 10U 10U 14U
1DU 1DU 10U 14U
20U 10U 10U 60U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 12J
10U 10U 10U 14U
10U 10U 1ou 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
1DU 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10\J 14U
10U 10U 10U 14U
1DU 10U 10U 14U
. 1DU 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
10U 10U 10U 14U
U: Material analyzed for but not detected. Val~ given is the minimum quantitatlon llmit
J: Estimated Value
Water Sample Results: UG/L
SoiVSedlment Results: UG!KG Page 1 of2
------
SURFACE WATER SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-004-SW WC-004-SD wc-oos-sw WC-005-SD
10U 13U 10U 14U
10U 13U 1ou 14U
10U 13U 10U 14U
10U 13U 10U JOU
10U 13U 10U 14U
10U 50U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U · 10U 14U
10U 13U 10U 14U
10U 9J 10U 14U
10U 13U 10U 14U
1ou 13U 10U 14U
10U 13U 1ou 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 1ou 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 1ou 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13u· 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 10U 14U
10U 13U 1ou 14U
10U 13U 1ou 14U
10U 13U 10U 1ou
==
SU_RFACE WATER
SAMPLE
WC-006-SW
Chlofomethane iou
Bromomethane !OU
Vinvt Chloride IOU
Chloroothane IOU
Methvlene Chloride IOU
ACetone !OU
Carbon Disulfide IOU
1, 1-0k;hloroethene 11.1-Dichloroethvlene\ IOU
1, 1-Dichloroethane IOU
1.2-Dichloroethene rTotal'l IOU
Chloroform IOU
1.2-0ichloroethane IOU
Methvl Ethu! Ketone IOU
1, 1.1-Trichloroethane IOU
Carbon Tetrachloride IOU
Bromodi Chloromethane IOU
1 ;2-0ich1oroorooane IOU
CIS• 1 ,3-Dichloronro""ne !OU
Trichloroethene rfr\chlofoeth•~ene' IOU
Dibromochloromethane IOU
1.1.2· Trichloroethane IOU
Benzene IOU
Trans· 1 ,3·Dichloronro-ne IOU
Bromoform IOU
Methvt lsob· ... J Ketone IOU
Methv1 BuM Ketone IOU
T etrachloroethene IT etrachloroethvlene) IOU
1, 1,2,2•Tetrachloroelhane IOU
Toluene IOU
Chlorobenzene !OU
Ethvl Benzene IOU
s~-ene IOU
Total xu1enes IOU
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ANALYTICAL DATA SUMMARY
WEYERHAUSER CO., PLYMOUTH, NORTH CAROLINA, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A· TABLE 1. PURGEABLE ORGANIC DATA
SEDIMENT SURFACE WATER SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE
WC-OOS-SD WC-007·SW WC-007-SD ·WC-107-SW WC-107-SD
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU ,OU . 20U 60U
13U !OU 21U IOU 24U
13U IOU 21U !OU 24U
13U IOU 21U IOU 24U
13U IOU 21U !OU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU !OJ
13U IOU 21U IOU 24U
13U IOU 21U !OU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U !OU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U' IOU 21U IOU 2'U
13U IOU 21U IOU 24U
13U IOU 21U IOU 2'U
13U IOU 21U !OU 24U
13U !OU 21U IOU 24U
13U IOU 21U !OU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 24U
13U IOU 21U IOU 2'U
13U IOU 21U !OU 24U
13U IOU 21U IOU 2'U
13U IOU 21U !OU 2'U
13U IOU 21U IOU 2'U
U: Malerial analyzed !or but not detected. Value given Is the minimum quantitatlon limit
J: Estimated Value
Water Sample Rnults: UG/L
Soil/Sediment Results: UG!KG Page 2 of2
liiiil -liii --
SEDIMENT
SURFACE WATER SEDIMENT SAMPLE
SAMPLE SAMPLE WC-108-SO
WC-008--SW WC-008--SD MATRIX SPIKE
IOU 2OU 13U
IOU 20U 13U
!OU 2OU 13U
IOU 20U 13U
IOU ,OU 13U
IOU ,ou 13U
!OU 7J 13U
IOU 20U 13U
IOU 20U 13U
IOU 20U 13U
IOU ,ou 13U
IOU 2OU 13U
. IOU 20U 13U
!OU ,OU 13U
IOU ,ou 13U
IOU 20U 13U
IOU 2OU 13U
IOU ,ou 13U
IOU 20U 13U
1OU 2OU 13U
IOU 20U 13U
IOU 2OU 13U
IOU 20U 13U
IOU 2OU 13U
IOU 20U 13U
IOU 2OU 13U
IOU ,ou 13U
1OU 2OU 13U
IOU 2OU 13U
IOU 2OU 13U
IOU 20U 13U
!OU 2OU 13U
IOU 2OU 13U
== i;;a lililiil Iii& liliil iiii liiii iiill -
ANALYTICAL DATA SUMMARY
WEYERHAUSER CO., PLYMOUTH,., NORTH CAROLINA, NCO 991 278 540 SIP June l':1-20, 1995
APPENDIX A -TABLE 2. PESTICIDES/PCB'S DATA REPORT
DRINKING WATER DRINKING WATER DRINKING WATER
SAMPLE SAMPLE SAMPLE
WC-001-DW WC-101-DW WC-002-DW
Alnha-BHC 0.0SU o.osu 0.0SU
Beta-BHC o.osu O.OSU o.osu
Oelta-BHC 0.0SU o.osu 0.0SU
Gamma-BHC llindane\ 0.0SU o.osu 0.0SU
Heotachlor o.osu 0.0SU o.osu
Aldrin 0.0SU 0.0SU 0.0SU
Hentachlor Enoxide 0.0SU O.OSU 0.0SU
Endosulfan I /Alnha' o.osu 0.0SU O.OSU
Oieldrin 0.10U 0.10U 0.10U
4 4'-DDE IP P'-DDE\ 0.10UJ 0.10UJ 0.10UJ
Endrin 0.10U 0.10U o.,ou
Endosulfan II meta) 0.10U 0.10U 0.10U
4 4'-DDD IP,P'-DDD\ 0.10U 0.10U 0.10U
Endosulfan Sulfate 0.10U 0.10U 0.10U
4 4'-00T tP,P'-OOTI 0.10U 0.10U 0.10U
Methoxvchlor 0.50U 0.50U 0.S0U
Endrin Ketone 0.10U o.,ou 0.10U
Endrin Aldehvde 0.10U a.mu 0.10U
Chlordane ITech. Mixture' /1 ---
Gamma-Chlordane f2 0.05U 0.0SU 0.05U
Alnha-Chlordane /2 0.0SU 0.05U 0.05U
Toxaohene 5.0U 5.0U 5.0U
PCB-1016 tAroclor 1016) 1.0UR 1.0UR 1.0UR
PCB 1221 fAroclor 1221\ 2.0U 2.0U 2.0U
PCB 1232 (Aroclor 1232' 1.0U 1.0U 1.0U
PCB 1242 (Aroclor 1242\ 1.0U 1.0U 1.0U
PCB 1248 tAroclor 12481 1.0U 1.0U 1.0U
PCB 1254 (Aroclor 1254\ 1.0U 1.0U 1.0U
PCB 1260 f Aroclor 1260\ 1.0U 1.0U 1.0U
U: Material analyzed for but not detected. Value given is the minimum quantitation limit
J: Estimated Value
R: QC indicates that data unusable. Compound may or may not be present
Water Sample Results: UG/L
Soil/Sediment Results: UG/KG
SURFACE WATER SEDIMENT
SAMPLE SAMPLE
WC-003-SW WC-003-SD
o.osu 3.SU
0.0SU 3.SU
o.osu 3.SU
0.0SU 3.SU
0.0SU 3.SU
O.OSU 3.SU
0.0SU 3.SU
0.0SU 3.SU
0.10U 6.9U
0. 10UJ 6.9U
0.10U 6.9U
o.,ou 6.9U
0.10U 6.9U
0.10U 6.9U
0.10U 6.9U
0.S0U 35U
0.10U 6.9U
0.10U 6.9U
--
0.0SU 3.SU
O.OSU 3.5U
5.0U 350U
1.0UR 69U
2.0U 140U
1.0U 69U
1.0U 69U
1.0U 69U
1.0U 69U
1.0U 69U
Page 1 of2
SURFACE WATER
SAMPLE
WC-004-SW
0.0SU
0.0SU
0.0SU
0.0SU
0.0SU
0.0SU
o.osu
O.OSU
0.10U
0.10UJ
0.10U
0.10U
0.10U
0.10U
0.10U
0.50U
0.10U
0.10U
-
o.osu
0.0SU
5.0U
1.0UR
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
--- -
SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE
WC-004-SD WC-005-SW WC-005-SD
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5.0U 0.0SU 2.6U
5,0U O.OSU 2.6U
9.7U 0.10U 5.1U
9.7U 0.10UJ 5.1U
9.7U 0.10U 5.1U
9.7U 0.10IJ 5.1U
9.7U 0.10U 5.1U
9.7U 0.10U 5.1U
9.7U 0.10U 5.1U
sou 0.50U 21JN
9.7U 0.10U 5.1U
9.7U 0.10U 5.1U
---
5.0U 0.05U 2.6U
5.0U O.OSU 2.6U
soou 5.0U 260U
. 97 1.0UR 51U
200U 2.0U 100U
97U 1.0U 51U
97U 1.0U 51U
97U 1.0U 51U
97U 1.0U 51U
97U 1.0U 51U
== liiiiil liiiiil liiii liiiill
ANALYTICAL DATA SUMMARY
WEYERHAUSER CO .. PLYMOUTH, NORTH CAROLINA, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A-TABLE 2. PESTICIDES/PCB'S DATA REPORT
SURFACE WATER SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-006-SW WC-006-S0 WC-007-SW WC-007-S0
Alpha-BHC O.OSU 2.BU 0.0SU 4.0U
Bela-BHC O.OSU 2.BU 0.05U 4.0U
Della-BHC 0.05U 2.BU 0.05U 4.0U
Gamma-BHC (Undanel o.osu 2.BU o.osu 4.0U
Heotachlor o.osu 2.BU 0.05U 4.0U
Aldrin 0.05U 2.BU o.osu 4.0U
Heotachlor Eooxide O.OSU 2.BU 0.0SU 4.0U
Endosu!fan I {Aloha} 0.05U 2.BU 0.05U 4.0U
Oieldrin 0.10U · 5.4U 0.10U 7.7U
4,4'-DDE {P P'-ODE) 0.10UJ 5.4U 0.10UJ 7.7U
Endrin 0.10U 5.4U D.10U 7.7U
Endosu1fan II (Beta) 0.10U 5.4U D.10U 7.7U
4 4'-000 f P P'-000\ D.1DU 5.4U o.1ou 7.7U
Endosu!fan Sulfate 0.10U 5.4U 0.10U 7.7U
4,4'-00T (P P'-DDT\ 0.10U 5.4U 0.10U 7.7U
Methoxvchlor 0.50U 2BU 0.50U 40U
Endrin Ketone 0.10U 5.4U D.10U 7.7U
Endrin Aldehvde 0.10U 5.4U 0.10U 7.7U
Chlordane {Tech. Mixture} 11 ----
Gamma-Chlordane f2 0.05U 2.SU i 0.05U 4.0U
Aloha-Chlordane f2 0.05U 2.BU 0.05U 4.0U
Toxaphene 5.0U 280U 5.0U 400U
PCB-1016 (Aroclor 10161 1.0UR 54U 1.0UR 77U
PCB 1221 (Aroclor 1221) 2.0U 110U 2.0U 160U
PCB 1232 (Aroclor 12321· 1.0U 54U 1.0U 77U
PCB 1242 fAroclor 12421 1.0U 54U 1.0U 77U
PCB 1248 (Aroclor 12481 1.0U 54U 1.0U 77U
PCB 1254 fAroclor 12541 1.0U 54U 1.0U 77U
PCB 1260 fAroclor 1260) 1.0U 54U 1.0U 77U
U: Material analyzed for but not detected. Value given is the minimum quantitation limit
J: Estimated Value
R: QC indicates that data unusable. Compound may or may not be present
Water Sample Results: UG/L
Soil/Sediment Results: UG/KG
Page 2 of2
SURFACE WATER SEDIMENT
SAMPLE SAMPLE
WC-107-SW WC-107-SD
o.osu 3.9U
0.05U 3.9U
0.05U 3.9U
o.osu 3.9U
o.osu 3.9U
o.osu 3.9U
0.05U 3.9U
0.05U 3.9U
0.10U 7.5U
0.10UJ 7.5U
0.10U 7.5U
0.10U 7.5U
0.10U 7.5U
D.10U . 7.5U
0.10U 7.5U
0.50U 39U
D.10U 7.5U
0.10U 7.5U
--
0.05U 3.9U
0.05U 3.9U
5.0U 390U
1.0UR 75U
2.0U 150U
1.0U 75U
1.0U 75U
1.0U 75U
1.0U 75U
1.0U 75U
liiii --

-
-

-
SEDIMENT
SURFACE WATER SEDIMENT SAMPLE
SAMPLE SAMPLE WC-108-SO
WC-008-SW WC-008-SD MATRIX SPIKE
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
0.05U 3.1U 3,1U
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
0.10U 6.1U 6.0U
0.10UJ 6.1U 6.0U
0.10U 6.1U 6.0U
0.10U 6.1U 6.0U
0.10U 6.1U 6.0U
D.10U 6.1U 6.0U
0.10U 6.1U 6.0U
0.50U 31U 31U
0.10U 6.1U 6.0U
0.10U 6.1U 6.0U
---
0.05U 3.1U 3.1U
0.05U 3.1U 3.1U
5.0U 310U 310U
1.0UR 61U 60U
2.0U 120U 120U
1.0U 61U 60U
1.0U 61U 60U
1.0U 61U 60U
1.0U 61U 60U
1.0U 61U 60U
!!!I i= == liiiiil
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth North Carolina, NCO 991 278 540
APPENDIX A-TABLE 3. EXTRACTABLE ORGANICS DATA REPORT
SIP June 19 20 1995 -
DRINKING WATER DRINKING WATER DRINKING WATER SURFACE WATER SEDIMENT SURFACE WATER
SAMPLE SAMPLE
WC-001-DW WC-101-DW
Phenol 10U 10U
Bisf2-Chloroeth',11Ether 10U 10U
2-Chloroohenol 10U 10U
1 3-Dichlorobenzene 10U 10U
1 4-Dichlorobenzene 10U 10U
1 2-Dichlorobenzene 10U 10U
2-Me-,."henol 10U 10U
2 2'-Chloroisonro"',.ether 10U 10U
3-and/or 4-)Meth•,."henol 10U 10U
N-Nitrosodi-N-Pro"'Aamine 100 10U
Hexachloroethane 10U 10U
Nitrobenzene 10U 10U
lsoohorone 10U 10U
2-Nitroohenol 10U 10U
2 4-Dimeth'""'henol 10U 10U
Bisl2-Chloroetho"'''Methane 10U 10U
2 4-Dimeth•""'henol 10U 10U
1 2 4-Trichlorobenzene 10U 10U
Naohthalene 10U 10U
4-Chloroaniline 10U 10U
Hexachorobutadiene 10U 10U
4-Chloro-3-Meth-""henol 10U 10U
2-Methv!naohathalene 10U 10U
Hexachlor"'"'.,.,fooentadiene IHCCP\ 10U 10U
2 4 6-Trichloronhenol 10U 10U
2 4 5-Trichloronhenol 25U 25U
2-Chloronanthalene 10U 10U
2-Nitroaniline 25U 25U
Dimethvl Phthalate 10U 10U
Acenaohthvlene 10U 10U
2 6-Dinitrototuene 10U 10U
3-Nitroaniline 25U 25U
Acenaohthene fou 10U
2 4-0initronhenol 2su· 25U
U: Material analyzed for but not detected. Value given is the minimum quantitation limit
J: Estimated Value
Water Sample Results: UG/L
Soil/Sediment ReSults: UG/KG
SAMPLE SAMPLE SAMPLE SAMPLE
WC-002-DW WC-003-SW WC--003-SD WC-004-SW
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U -
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U . 10U
10U 10U 700U 10U
25U 25U 1800U 25U
10U 10U 700U 10U
25U 25U 1800U 25U
10U 10U 700U 10U
10U 10U 700U 10U
10U 10U 700U 10U
25U 25U . 1800U 25U
10U 10U 700U 10U -
2su· 25U ·,aoou 25U
Page 1 of 4
--
SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE
WC-004-SD WC-005-SW WC-005-SD
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
970U 10U 520U
2400U 25U 1300U
970U 10U 520U
2400U 25U 1300U
970U 10U 520U
970i.J 10U 520U
970U 10U 520U
2400U 25U 1300U
970U 10U 520U
2400U 25U 1300U
a!!9
I
I!!!!!!! == == == raa liiiil
SURFACE WATER
SAMPLE
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth North Carolina, NCD 991 278 540
APPENDIX A-TABLE 3. EXTRACTABLE ORGANICS DATA REPORT
C::.TP .l -lQ .?fl 1 QQ<;
SEDIMENT SURFACE WATER SEDIMENT SURFACE WATER
SAMPLE SAMPLE SAMPLE SAMPLE
SEDIMENT
SAMPLE
WC-006-SW WC-006-SD WC-007-SW WC-007-SO WC-107-SW WC-107-SO
Phenol ,ou 540U ·1ou
Bisf2-Chloroethv1'Ether 10U 540U
2-Chloronhenol 10U 540U
1 3-Dichlorobenzene 10U 540U
1 4-Dichlorobenzene 10U 540U
1 2-Dichlorobenzene ,ou 540U
2-Mettr~-henol ,ou 540U
2 2'-Chloroisooronvlether ,ou 540U
3-and/or 4-\Methvlnhenol ,ou 540U
N-Nitrosodi-N-Pronvtamine ,ou 540U
Hexachloroethane 10U 540U
Nitrobenzene ,ou 540U
tsonhorone 10U 540U
2-Nitronhenol 10U 540U
2 4-Dimeth·J-henol 10U S40U
Bisl2-Chloroetho~·'Methane ,ou 540U
2 4-Dimeth·J-henol ,ou 540U
1 2 4-Trichlorobenzene ,ou 540U
Nanhthalene 10U 540U
4-Ch!oroaniline 10U 540U
Hexachorobutadlene 10U 540U
4-Chloro-3-MettrJ-henol 10U 540U I
2-Methvlnanhathalene 10U 540U '
Hexachlor-~-lonentadiene IHCCP) 10U 540U
2 4 6-Trichloronhenol 10U 540U
2 4 5-Trichloronhenol 25U 1400U
2-Chloronantha1ene 10U 540U
2-Nitroaniline 25U 1400U
Dimethvl Phtha!ate ,ou 540U
Acenaohthv1ene 10U 540U
2 6-Dinitrotoluene 10U 540U
3-Nitroaniline 25U 1400U
Acenaohthene 10U 540U
2 4-Dinitroohenol 25U 1400U
U: Material analyzed for but not detected. Value given is the minimum quantitation Umit
J; Estimated Value
Water Sample Results: UG/L
Soil/Sediment Results: UG/KG
,ou
10U
10U
,ou
,ou
,ou
,ou
,ou
,ou
10U
10U
,ou
,ou
,ou
10U
10U
,ou
,ou
,ou
10U
10U
,ou
,ou
10U
25U
10U
25U
,ou
,ou
,ou
25U
,ou
25U
770U 10U 750U
770U 10U 7SOU
770U 10U 7SOU
770U 10U 7SOU
770U 10U· 750U
770U ,ou 750U
770U 10U 750U
770U ,ou 750U
770U 10U 750U
770U 10U 750U
770U 10U 750U
770U ,ou 750U
770U ,ou 750U
770U ,ou 750U
770U ,ou 7S0U
770U ,ou 750U
770U ,ou 750U
770U 10U 7S0U
770U 10U iS0U
770U 10U 7S0U
770U 10U 7S0U
770U 10U 7S0U
770U 10U 7S0U
770U 10U 750U
770U 10U 7S0U
1900U 25U 1900U
770U ,ou 750U
1900U 25U 1900U
770U 10U 7S0U
770U 10U 7S0U
770U 10U 7S0U
1900U 25U 1900U
770U 10U 7S0U
1900U 25U 1900U
Page2of4
iilil ----
SEDIMENT.
SURFACE WATER SEDIMENT SAMPLE
SAMPLE SAMPLE WC-108-SO
WC-008-SW WC-008-SO MATRIX SPIKE
,ou 610U 600U
,ou 610U BOOU
,ou 610U 600U
,ou 610U BOOU
,ou 610U BOOU
,ou 610U BOOU
,ou 610U B0OU
,ou 610U B00U
,ou 610U BO0U
,ou 610U B0OU
10U 610U 600U
,ou 610U 600U
,ou 610U 600U
10U 610U 600U
10U 610U 600U
10U 610U 600U
,ou 610U 600U
,ou 610U B0OU
,ou 610U 600U
,ou 610U B00U
,ou 610U BO0U
,ou 610U 600U
,ou 610U B00U
,ou 610U B00U
,ou 610U 600U
25U 1500U 1S00U
10U 610U 600U
25U 1500U 1500U
10U 610U 600U
,ou 610U 600U
,ou 610U 600U
25U 1500U 1500U
10U 610U 600U
25U 1500U 1500U
;
!!!!!!I
DRINKING WATER
SAMPLE
WC-001-0W
4-Nitroohenol 25U
Dit:ienzofuran 10U
2 4-Dinitrotoluene 10U
Diethvl Phthalate 10U
4-Chloroohenvt Phenvl Ether 10U
Fluorene 10U
4-Nitroaniline 25U
2-Methvl-4 6-0initroohenol 25U
N-Nitrosodinhenvtamine/Dinh"enylamine 10U
4-Bromoohen'-'1 Phen'-'1 Ether 10U ·
Hexachlorobenzene lHCB) 10U
Pentachloroohenol 25U
Phenanthrene 10U
Anthracene 10U
Carbazole 10U
Di-N-8• lfvlnhtha!ate 10U
Fluoranthene 10U
o.~ene 10U
Be""'" B• .+.A Phthalate 10U
3 3'-Dichlorobenzidine 10U
Benzo(A \l>.nthracene 10U
Chrvc:.ene 10U
Bisl2-Ethv!hevvl\ Phthalate 10U
Oi-N-1"\r+,A"hthalate 10U
BenzofB and/or K)Fluoranthene 10U
Benzo-A-P.wene 10U
lndeno (1 2 3-CO) Pvrene 10U
Dibenzo fl>. H.) Anthracene 10U
Benzo IGHI) Pervlene 10U
ma liiia -
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Carolina, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A-TABLE 3. EXTRACTABLE ORGANICS DATA REPORT
DRINKING WATER DRINKING WATER SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-101-DW WC--002-DW WC-003-SW WC-003-SD
25U 25U 25U 1800U
10U 10U 10U-700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
25U 25U 25U 1800U
25U 25U 25U 1800U
.10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
25U 25U 25U 1600U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
10U 10U 10U 700U
U: Material was analyzed for but not detected. Value given is the" minimum quantitation ~mit
J: Estimated Value
Water Sample Results: UGJL
SoiVSediment Sample Results: UGJKG Page3of4
---

-
SURFACE WATER SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-004-SW WC-004-SO WC-005-SW WC--005-SD
25U 2400U 25U 1300U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
25U 2400U 25U 1300U
25U 2400U 25U 1300U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
25U 2400U 25U 1300U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
-10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
10U 970U 10U 520U
!!!!I == ==
SURFACE WATER
SAMPLE
WC--006-SW
4-Nitrophenol 25U
Oibenzofuran 10U
2,4-Dinitrotoluene 10U
Oie!h\ I Phthalate 10U
4-Chlorophenvl Phen,.i Ether 10U
Fluorene 10U
4-Nitroaniline 25U
2-Meth~ 1--4, 6-Di nitrophenol · 25U
N-Nitrosodi phenvla mine/Di Ph en~ I amine 10U
4-Bromoohenvl Phem I Ether 1DU
Hexachlorobenzene (HCBl 10U
Pentachtorophenol 25U
Phenanthrene 10U
Anthracene 1DU
Carbazole 1DU
Di-N-Butylphthalate 10U
Fluoranthene 10U
Pvrene 10U
Benzvl Buhl Phthalate 10U
3 3'-Dichlorobenzidine 10U
Benzo(A\Anthracene 10U
Chrvsene 10U
Bis12-Ethylhexyl) Phthalate 10U
Di-N-Octvlohthalate 10U
Benzo(B and/or KlFJuoranthene 10U
Benzo--A-Pvrene 10U
lndeno (1 2.3-CO) Pvrene 10U
Dibenzo (A,H. l Anthracene 10U
Benzo rGHll Perv1ene 10U
raD ;;;a liiill liiiiii
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Carolina, NCO 991 278 540
SlP June 19-20, 1995
APPENDIX A -TABLE 3. EXTRACTABLE ORGANICS DATA REPORT
SEDIMENT SURFACE WATER SEDIMENT SURFACE WATER
SAMPLE SAMPLE SAMPLE SAMPLE
WC-006-SD WC-007-SW WC-007-SO WC-107-SW
1400U 25U 1900U 25U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U. 10U
540U 10U 770U 10U
540U 10U 770U 10U
1400J 25U 1900U 25U
1400J 25U 1900U 25U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
1400U 25U 1900U 25U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 96J 10U
540U 10U ' 770U 10U '
540U 10U ' 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
540U 10U 770U 10U
U: Material was analyzed for but not detected. Vatue given is the minimum quantitation limit
J: Estimated Value
Wale,-Sample Results: UG/L
Soil/Sediment Sample Results: UG/KG
Page4of4
--- - --
SEDIMENT
SEDIMENT SURFACE WATER SEDIMENT SAMPLE
SAMPLE SAMPLE SAMPLE WC-108-SO
WC-107-SD WC-008-SW WC--008-SD MATRIX SPIKE
1900U 25U 1500U 1500U
750U 10U 610U BOOU
750U 10U 610U 600U
750U 10U 610U 600U
750U 10U 610U 600U
750U 10U 610U 600U
1900U 25U 1500U 1500U
1900U 25U 1500U 1500U
750U 10U 610U 600U
750U 10U 610U 600U
750U 10U 610U 600U
1900U 25U 1500U 1500U
750U 10U 610U 83J
750U 10U 610U B00U
750U 10U 610U 600U
750U 10U 610U 600U
750U 10U 610U 130J
160J 10U 610U 380J
750U 10U 610U B00U
750U 10U 610U 600U
750U 10U 610U 80J
750U 10U 610U 130J
750U 10U 610U 600U
750U 10U 610U 600U
750U 10U 610U 140J
~
99J 10U 610U 90J
750U 10U 610U 600U
750U 10U 610U B00U
140J 10U 610U 600U
!!!!I 9!!I
/
I!!!! ==
DRINKING WATE DRINKING WATER
SAMPLE SAMPLE
WC-001-DW WC-101-DW
Aluminum 20UJ 20UJ
Antimonv 20UJ 20UJ
Arsenic 4UJ 4UJ
Barium 6UJ 5UJ
Beryllium 1UJ 1UJ
Cadmium 1UJ 1UJ
Calclum 45000J 44000J
Chromium 5UJ 5UJ
Cobalt 2UJ 2UJ
Conner 6UJ 4UJ
Iron 70UJ S0UJ
Lead 3UJ 3UJ
Maqnesium 25000J 25000J
Manoanese 1UJ 1UJ
Mercurv 0.38J 0.2UJ
Nickel 5UJ 5UJ
Potassium 16000J 16000J
Selenium 3UJ 3UJ
Silver 3UJ 3UJ
Sodium 57000J 57000J
Thallium 6UJ 6UJ
Tiri NA NA
Vanadium 3UJ 3UJ
Zinc 590J 630J
;;;a liiiiil
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Carolina, i'JCO 991 278 540
SIP June 19-20, 1995
APPENDIX A-TABLE 4. METALS DATA REPORT
DRINKING WATER SURFACE WATER SEDIMENT SURFACE WATER
SAMPLE SAMPLE SAMPLE SAMPLE
WC-002-DW WC-003-SW WC-003-SD WC-004-SW
20UJ 650J 2100 430
20UJ 20UJ 6UR 20U
4UJ 4UJ 3U 4U
2UJ 30UJ 190 30U
1UJ 1UJ 0.26U 1U
1UJ 1UJ 0.44U 1U
38000J 7000UJ 1900 7500U
5UJ 5UJ 41 SU
2UJ 2UJ 20U 2U
SUJ 3UJ 27 3U
10UJ 1200J 36000 1100
3UJ 3UJ 20 3U
23000J 2800J 3500 2700
1UJ 71J 990 72
0.10UJ 0.2UJ 0.2U 0.2U
5UJ 5UJ 15J SU
19000J 2200J 2100 2200J
3UJ 3UJ 1.1U 3U
3UJ 3UJ 1.2U 3U
120000J 9100J 150U 8900
6UJ 6UJ 2.3U 6U
NA NA NA NA
3UJ 3UJ 62 3U
7UJ 5UJ 110 4U
U: Material was analyzed for but not detected. Value is minimum quantitation limit
J: Estimated Value
Water Sample Results: UG/L
Soil/Sediment Results: MG/KG
Concentrations in Bold Exceed 3X Background
Page 1 of2
liiiii lliil .. -liil
SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE
WC-004-SO WC-005-SW WC-005-SO
21000 200UJ 1900
7.6UR 20UJ 4UR
3U 4UJ 0.96U
200 46J 85
2U 1UJ 0.17U
0.56U 1UJ 1U
3600 110000UJ 150000
46 5UJ 98
20U 2UJ 3U
30 3UJ 8.4
35000 2000J 4300
26 3UJ · 11
3300 2100J 2200
790 77J 71
0.28 0.2UJ 1
16J 5UJ 21
1900 2200J 230
1.4U 3UJ 0.73U
1.5U 3UJ 1J
210U 8800J . 610
2.9U · 6UJ 1.5U
NA NA NA
68 4UJ 20U
120 4UJ sou
!!!!!I l!!!!I ell
SURFACE WATER SEDIMENT
SAMPLE SAMPLE
WC-006-SW WC-006-SO
Aluminum 180UJ 7100
Antimonv 20UJ 4.5UR
Arsenic 4UJ 2U
Barium 46J 41
Ben.Ilium 1UJ 0.20U
Cadmium 2UJ 0.33U
Calcium 10000J 1300
Chromium 5UJ 8.7
Cobalt 2UJ 3U
Co--er 3UJ 7.7J
Iron 1400J 6800
Lead 3UJ 31
Mannesium 1900J 450
Mannanese 53J 55
Mercurv · 0.21J · 0.09U
Nickel 5UJ 3U
Potassium 1900J 390
Selenium 3UJ 0.82U
Silver 3UJ 0.89U
Sodium 5500J 70U
Thallium 6UJ 1.7U
Tin NA NA
Vanadium 3UJ 20U
Zinc 9UJ 40U
== ==
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Carolina, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A-TABLE 4. METALS DATA REPORT
SURFACE WATER SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE SAMPLE
WC-007-SW WC-007-SD WC-107-SW WC-107-SD
470J 18000 304J 21000
20UJ 6.2UR 20UJ 6.5UR
4UJ 4U 4UJ 4U
30UJ 200 30UJ 220
1UJ 1U 1UJ 0.29U
2UJ 0.46U 2UJ 0.48U
6600UJ 1500 6700J 1700
5UJ 37 5UJ 41
2UJ 20U 2UJ 18
9UJ 29 6UJ 30
1000J 37000 930J 42000
3UJ 21 3UJ 22
2700J 3400 2700J 3700
65J 1200 66J 1300
0.10UJ 1.7 0.10UJ 2.1
5UJ 15J 5UJ 16J
2100J 2000 2100J 2200
3UJ 1.1U 3UJ 1.2U
3UJ 1.2U 3UJ 1.3U
8900J 160U 8700J 170U
6UJ 2.4U 6UJ 2.5U
NA NA NA NA
3UJ 62 3UJ 71
4UJ 100 2UJ 110
U: Material was analyzed for but not detected. Value is minimum quantitation limit
J: Estimated Value
Water Sample Results: UG/L
Soll/Sediment R~sults: MG/KG ·
Concentrations in Bold Exceed 3X Background
Page2of2
iiiii liiiii &ii --liiil
St:.DIMENT
SU~FACE WATER SEDIMENT SAMPLE
SAMPLE SAMPLE WC-108-SD
WC-008-SW WC-008-SO MATRIX SPIKE
720J 18000 16000
20UJ SAUR 5.1UR
4UJ 2.9J 2U
34J 160 160
2UJ 1U 1U
2UJ 0.40U 0.38U
6800UJ 1500 1500
5UJ 32 32
2UJ 20U 20U
10UJ 22 21
1500J 29000 29000
3UJ 16 16
2800J 3200 3100
110J 770 790
0.10UJ 0.09U 0.09U
5UJ 13J 13J
2100J 1900 1900
3UJ 0.99U 0.94U
3UJ 1.1U 1U
9600J 130U 130U
6UJ 2.1U 2U
NA NA NA
4UJ 52 51
5UJ 89 85
l!l!!!!I l!!!!!!!!I
;
I!!!!! I!!!! 1111111 aa
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Caroiina, NCO 991 278 540
SIP June 19-20, 1995
APPENDIX A -TABLE 5. DIOXIN/FURAN DATA REPORT
DRINKING WATER DRINKING WATE DRINKING WATER
SAMPLE SAMPLE SAMPLE
WC-001-DW WC-101-DW WC.002-DW
2,3,7,8 Tetrachlorodibenzodioxin 0.012U 0.012U 0.012U
Tetrachlorodibenzodioxin tTotal\ 0.012UJ 0.012UJ 0.012UJ
12,378 Pentachlorodibenzodioxin 0.06U 0.06U 0.06U
Pentachlorodibenzodioxin 1Total' 0.06UJ 0.06UJ 0.06UJ
1,2,3,4, 7,8 Hexachlorodibenzodioxin 0.06U 0.06U 0.06U
1 2,3,6. 7 B Hexachlorodibenzodioxin 0.06U 0.06U 0.06U
1 2,3,7.8 9 Hexachlorodibenzodioxin 0.06U 0.06U 0.06U
Hexachlorodibenzodioxin (Total) 0.06UJ 0.06UJ 0.06UJ
1,2, 3,4,6, 7 ,8 Heotachlorodibenzodioxin 0.06U 0.06U 0.06U
Heotachlorodibenzodioxin <Totatl 0.06UJ 0.06UJ 0.06UJ
Octachlorodibenzodioxin (Total\ 0.12U 0.12U 0.12U
2,3, 7,8 Tetrachlorodibenzofuran 0.012U 0.012U 0.012U
Tetrachlorodibe~zofuran /Total\ 0.012UJ 0.012UJ 0.012UJ
1 2 3,7 8 Pentachlorodibenzofuran 0.06U 0.06U 0.06U
2 3,4,7 8 Pentachlorodibenzofuran 0.06U 0.06U 0.06U
Pentachlorodibenzofuran /Total\ 0.06UJ 0.06UJ 0.06UJ
1,2,3,4,7,8 Hexachlorodibenzofuran 0.06U 0.06U 0.06U
1,2,3,6,7 ,8 Hexachlorodibenzofuran 0.06U 0.06U 0.06U
1 2,3, 7 8 9 Hexachlorodibenzofuran 0.06U 0.06U 0.06U
2,3,4,6,7,8 Hexachlorodibenzofuran 0.06U · 0.06U 0.06U
Hexachlorodibenzofuran tTotall 0.06UJ 0.06UJ 0.06UJ
1,2,3,4,6, 7 ,8 Heotachlorodibenzofuran 0.06U 0.06U 0.06U
1 2 3,4. 7,8,9 Heotachlorodibenzofuran 0.06U 0.06U 0.06U
Heotachlorodibenzofuran <Totall 0.06UJ 0.06UJ 0.06UJ
Octachlorodibenzofuran fTotan 0.12U 0.12U 0.12U
TEO fToxic. Eauiv. Value, From t-TEF/89 0 0 0
Concentrations in Bold Exceed 3X Background
U: Material analyzed for but not detected. Value given is the minimum quantitation limit
J: Estimated Value
Water Sample Results: NG/L
S?il/Seciiment Sample Results: NG/KG
Paga 1 of2
SEDIMENT
SAMPLE
WC-003-SD
2.1J
7.3J
10U
10UJ
1.1J
1.7J
2.0J
30J
57
160J
2500J
10
18J
10U
10U
1.6J
10U
10U
10U
10U
5.7J
7.2J
10U
17J
8.BJ
6,7
iill ---- -
SURFACE WATER SEDIMENT SURFACE WATER
SAMPLE SAMPLE SAMPLE
WC-004-SW WC-004-SD WC-OQS-SW
0.014U 17J 0.012U
0.014UJ 24J 0.012UJ
0.07U 5.0U o.06U
0.07UJ 5.0UJ 0.0BUJ
0.07U 1.9J 0.06U
0.07U 3.9J 0.06U
0.07U 3.6J 0.06U
0.07U 59J · 0.06UJ
O.OOBJ 97 0.06U
0.017J 310J 0.06UJ
0.12J 3100 0.12U
0.014U 89 0.012U
0.014UJ 190J 0.012UJ
0.07U 5.0U 0.06U
0.07U 5.0U 0.06U
0.07UJ 5.0UJ 0.06UJ
0.07U 2.5J o.osu'
0.07U 0.74J o.osu·
0.07U 5.0U 0.06U
D.07U 1.4J 0.06U
0.07U 20J 0.06UJ
0.07U 20 0.06U
0.07U 5.0U 0.06U
0.07U 50J 0.06UJ
D.14U 29 0.12U
0.0002J 32J 0
- -
l!!!!!!!!I -l!!!!!I liiiiil lllil
ANALYTICAL DATA SUMMARY
Weyerhauser Co., Plymouth, North Carolina, NCO 991 278 540
SIP June 19~20, 1995
APPENDIX A -TABLE 5. DIOXIN/FURAN DATA REPORT
SEDIMENT SURFACE WATER SEDIMENT
SAMPLE SAMPLE SAMPLE
WC-005--SD WC-006-SW WC-006-SD
2,3, 7,8 Tetrachlorodibenzodioxin 23J 0.012U 4.9J
Tetrachlorodibenzodioxin (Total\ 23J 0.012UJ 5.SJ
1,2 3 7,8 Pentachlorodibenzodioxin 5.0U 0.06U 5.0U
Pentachforodibenzodioxin !Total\ 5.0UJ O.OBUJ 5.0UJ
1 2 3 4 7,8 Hexachlorodibenzodioxin 5.0U 0.06U 5.0U
1,2,3,6, 7,8 Hexachlorodibenzodioxin 3.8J 0.06U 1.5J
1,2,3, 7,8,9 Hexachlorodibenzodioxin 2.9J 0.06U 2.2J
Hexachlorodibenzodioxin fTota11 25J 0.06UJ 12J
1,2,3,4,6, 7,8 Heotachlorodibenzodioxin 31 0.06U 39J
Heptachlorodibenzodioxin fTotall 39J 0.06UJ 52J
Octachlorodibenzodioxin rTotall 920 0.12U 1900
2,3,7,8 Tetrachlorodibenzofuran 160 0.012U 39
Tetrachlorodibenzofuran /Total\ 330J 0.03UJ 79J
1,2,3. 7 8 Pentachlorodibenzofuran 5.0U 0.06U 5.0U
2,3,4.7,8 Pentachlorodibenzofuran 5.0U 0.06U 5.0U
Pentachlorodibenzofuran lTotall 5.0UJ 0.06UJ 5.0UJ
1,2 3.4 7,8 Hexachlorodibenzofuran 5.0U 0.06U 5.0U
1,2,3,6,7,8 Hexachlorodibenzofuran 5.0U 0.06U s.ou
1 2,3 7 8 9 Hexachlorodibenzofuran 5.0U 0.06U 5.0U
2,346 7 8 Hexachlorodibenzofuran 5.0U 0.06U 5.0U
Hexachlorodibenzofuran fTotan 5.0UJ 0.06UJ 5.0UJ
1 2 3 4 6 7 8 Heotachlorodibenzofuran 2.8J 0.06U 2.7J
1 2 3 4 7 8 9 Hentachlorodibenzofuran 5.0U 0.06U 5.0U
Heptachlorodibenzofuran /Total\ 8.3J 0.06UJ 2.7J
Octachlorodibenzofuran tTotal\ 10U 0.12U 8.2J
TEQ (Toxic. EQuiv. Value, From I-TEF/891 41 0 12J
Concentrations in Bold Exceed 3X Background
U: Material analyzed for but not detected. Value given is the minimum quantitation limit
J: Estimated Value
Water Sample Results: NG/l.
Soil/Sediment Sample Results: NG/KG Pege2of2
SEDIMENT SEDIMENT
SAMPLE SAMPLE
WC-007-SO ·wc-101-so
1.0U 1.0U
12J 9.7J
5.0U 5.0U
5.3J 5.0UJ
2.7J 5.0U
6 6.5
6.8 5.0U
130J 110J
190 200
320J 520J
7300J BOOOJ
5.0U 6.0U
16J 15J
5.0U 5.0U
1.7J 5.0U
12J 16J
5.0U 5.0U
1.0J 5.0U
5.0U 5.0U
1.7J 5.0U
23J 13J
23 18
s.ou 5.0U
52J 38J
26 22
12J 11J
SURFACE WATER
SAMPLE
WC--008-SW
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0.009J
0.017J
0.18
0.012U
0.012UJ
0.06U
0.06U
0.06UJ
0.06U
0.06U
0.06U
· 0.06U
0.06UJ
0.06U
0.06U
0.06UJ
0.12
0.00027
- ----
SEDIMENT
SEDIMENT SAMPLE
SAMPLE WC-108-SO
WC-008-SD MATRIX SPIKE
1.0U 1.0U
8.9J 6.8J
5.0U 5.0U
3.2J 3.5J
1.5J 2.5J
3.7J 3.3J
4.3J 4.SJ
75J 71J
110 120
140J 160J
4300J 5000J
1.0U 2.0U
10J 7.0UJ
5.0U 5.0U
5.0U 5.0i.J
9.0J 4.4J
5.0U 5.0U
5.0U 5.0U
5.0U 5.0U
1.3J 1.1J
8.9J 6.3J
9.2 11
5.0U 5.0U
26J 26J
22 16
6.6J 7.5J
I
I
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
.***MEMORANDUM******
I DATE: 08/12/95
1TBJECT: Results
95-0295
of Extractable Organic Analysis;
WEYERHAEUSER CO.
PLYMOUTH NC
I
I TO: PAT DEROSA
Attached are the results of analysis of samples collected as part of 11e subject project.
As a result of the Quality Assurance Review, certain data qualifiers '.1ftY have been placed on the data. Attached is a DATA QUALIFIER
'UPORT which explains the reasons that these qualifiers were required.
If
B
D
u
D
you have any questions please contact me.
ATTACHMENT
METALS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ••
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95539
SOURCE, WEYERHAEUSER CO.
STATION ID, SPIKE TT1297 CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE·, SEDIMSPK PROG ELEM, NSF
CITY, PLYMOUTH
COLLECTION START,
MD NUMBER, KA51
COLLECTED BY, D RUMFORD ST, NC
06/20/95 STOP, 00/00/00
**
**
** •• ** *** * * * * * * * * * * * * * * * * * * * * * * *· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG
1200
22
480
1400
0 .12U
580
72000
16
16
620
19000
39000
37000
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
250
9.3
140
310
21
33
94
1.6
NA
29
150000
ANALYTICAL RESULTS
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
---- - - -
l!!!l!!!l!I I!!!!!! l!!!!I == liiiiiii iiiiii liil -
- ----METALS DATA REPORT --sAMl!ll!IIAND 111!1,YsI~AGB sE EPA-REGION IV ESD, ATHENS, GA.
11111!1 l!!!!!!!I l!!!!!l!!I --08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** ••
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95538 SOURCE, WEYERHAEUSER CO . STATION ID, SPIKE 0025296 CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, WATSPK PROG ELEM, NSF
CITY, PLYMOUTH
COLLECTION START, MD NUMBER, KA50
COLLECTED BY, D RUMFORD
ST, NC
06/20/95 STOP, 00/00/00
**
**
**
**
** *** * * * * * * * * * * * * -. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
410
62
4
3
1
12
5100
11
63
8
6400
3U
40U
UG/L
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
37
O.lOU
7
7000
24
3U
1600
6U
NA
240
10
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN .TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
METALS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
**
**
** •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 002-DW CASE NUMBER, 23680
SAMPLE NO. 95534 co.
SAS NUMBER,
SAMPLE TYPE, DRKWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA71
BY, D RUMFORD
ST, NC
1515 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L
20UJ
20UJ
4UJ
2UJ
lUJ
lUJ
38000J
5UJ
2UJ
5UJ
lOUJ
3UJ
23000J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM BERYLLIUM
CADMIUM CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
lUJ
O.lOUJ
5UJ 19000J
3UJ
3UJ
120000J
6UJ
NA
3UJ
?UJ
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
------1!!1111!1 -l!!!!!!!!!!I 1!!11 1!!1111 l!!!!I l!!!!!!!!!!I l!l!!!I ==
- -- - ------SAMi?'LEAND ANALYSIS MANAGEMENT -SYSTEM -liiiiliiil ;;;;;ii
METALS DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95533
SOURCE, WEYERHAEUSER-CO.
STATION ID, 107-SD
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 MD NUMBER, KA70
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
**
**
**
**
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG
21000
6.5UR
4U 220
0.29U
0.48U
1700
41
18
30
42000
22
3700
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
ANALYTICAL RESULTS MG/KG
1300
2.1
16J
2200
1.2U
1.3U
170U
2.5U
NA
71
110
60
MANGANESE
MERCURY
NICKEL POTASSIUM
SELENIUM SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
PERCENT MOISTURE
***FOOTNOTES***
. *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANASEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/03/95
METALS DATA REPORT *** * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** **
**
PROJECT NO. 95-0295 SAMPLE NO. 95532
SOURCE, WEYERHAEUSER CO.
STATION ID, 107-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 MD NUMBER, KA69
BY, D RUMFORD
ST, NC 1415 STOP, 00/00/00
** •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
340J
20UJ
4UJ
30UJ 1UJ
2UJ
6700J
5UJ
2UJ
6UJ
930J
3UJ
2700J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS UG/L 66J
0.l0UJ
5UJ
2100J
3UJ
3UJ
8700J
6UJ
NA
3UJ
2UJ
MANGANESE
MERCURY NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.-
---- ---!!!!!!I !!l!!!!I I!!!!! 1!!!11 !!!!!I == == liiiiiill
- -- -- --== == --11!!!!!1 METALS DATA REPORT 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95531 SOURCE, WEYERHAEUSER CO. SAMPLE TYPE, SOIL
STATION ID, 007-SD
CASE NUMBER, 23680 SAS NUMBER,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA68
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
•• • • •• •• • •
MG/KG
18000 6.2UR
4U
200
1U
0.46U
1500
37
20U
29
37000
21
3400
ALUMINUM
ANTIMONY
ARSENIC BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
1200
1. 7
15J
2000
l.lU
l.2U
160U
2 .4U
NA
62
100
59
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
METALS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA~REGION IV ESD, ATHENS, GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95530
SOURCE, WEYERHAEUSER CO.
STATION ID, 007-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA67
BY, D RUMFORD ST, NC
1415 STOP, 00/00/00
**
** **
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
470J
20UJ
4UJ
30UJ
lUJ
2UJ
6600UJ
5UJ
2UJ
9UJ lOOOJ
3UJ
2700J
ALUMINUM
ANTIMONY
ARSENIC BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
65J
O.lOUJ
5UJ 2100J
3UJ
3UJ
8900J
6UJ
NA
3UJ
4UJ
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL.
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN.VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-- ------1!!!!!!!1!11 1!!!!!11 I!!!!!!!! li!!!!l!!I l!!!!!I == liliiiiiiil &iiiiil
- --- ---SYSTEM -== l!I!! !II!!!
METALS DATA REPORT GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 108-SD
CASE NUMBER, 23680
SAMPLE NO. 95529 co .
SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 MD NUMBER, KA66
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
•• •• **
**
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG
16000 5.lUR
2U
160
lU
0.38U
1500
32
20U
21
29000
16
3100
ALUMINUM
ANTIMONY
ARSENIC BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
790 0.09U
13J
1900
0.94U
lU
130U
2U
NA
51
85
49
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
METALS DATA REPORT ••• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * * * * * * * * * * * * * * * * * * * * * * * *
•• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95528 SAMPLE TYpE, SOIL
SOURCE, WEYERHAEUSER CO.
STATION ID, 008-SD CASE NUMBER, 23680 SAS NUMBER,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA65
BY, D RUMFORD
ST, NC 1330 STOP, 00/00/00
08/03/95
• • * ••• •• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
MG/KG
18000 5.4UR
2.9J
160
1U
0.40U
1500
32
20U
22
29000
16
3200
ALUMINUM
ANTIMONY
ARSENIC
BARIUM BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
770
0.09U
13J
1900
0.99U
l.lU
130U
2 .lU
NA
52
89
51
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
---- ----I!!!!!!! l!l!!!!I l!!!!!!I 111!!1 ll!'l!II == ==
-- --METALS DATA REPORT ---AMI-ND -YSI-lAGE-' SY-~REG!u'fl""IV ~ATH1'l'l'!s, GA. --*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO, 95527
SOURCE, WEYERHAEUSER CO.
STATION ID, 008-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA6 4
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •.• * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
720J
20UJ
4UJ
34J
2UJ
2UJ
6800UJ
5UJ
2UJ
lOUJ
1500J
3UJ
2800J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
llOJ
O.lOUJ
5UJ
2100J
3UJ
3UJ
9000J
6UJ
NA
4UJ
5UJ
MANGANESE
MERCURY
NICKEL POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
METALS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
** ..
**
** ..
PROJECT NO. 95-0295 SAMPLE NO. 95526
SOURCE, WEYERHAEUSER CO .
STATION ID, 004-SD
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA63
BY, D RUMFORD
ST, NC
1200 STOP, 00/00/00
** •• •• ••
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
MG/KG
21000
7.6UR
3U
200
2U
0.56U
3600
46
20U
30
35000
26
3300
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
790
0.28
16J
1900
l.4U
l.5U
210U
2.9U
NA
68
120
65
ANALYTICAL RESULTS
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
·--

-

-
--

-
-1!!!111!1 l!!!!I l!!!!!I 11111 ==
~-s D~EP-- - - -liliii"""llliil'v 'lill'""lii ""-* -••• 1111 -* * * * ~ *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ••
** ** •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 004-SW
CASE NUMBER, 23680
SAMPLE NO. 95525 co.
SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA62
BY, D RUMFORD
ST, NC
1150 STOP, 00/00/00
** ** ** •• **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
430
20U
4U
30U
lU
UG/L
lU
7500U
SU
2U
3U
llOO
3U
2700
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
72
0.2U
SU
2200J
3U 3U
8900
6U
NA
3U
4U
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAT-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT.-RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/03/95
METALS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
**
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95524
SOURCE, WEYERHAEUSER CO. STATION ID, 003-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
MD NUMBER, KA61
BY, D RUMFORD
ST, NC 1110 STOP, 00/00/00
**
** ** ** **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * ***
UG/L
650J 20UJ
4UJ 30UJ
lUJ
lUJ
7000UJ
SUJ
2UJ
3UJ
1200J
3UJ
2800J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
71J
0.2UJ
SUJ 2200J
3UJ
3UJ
9100J
6UJ
NA
3UJ
SUJ
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN· *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-- -- ---l!!!!!!I I!!!!!!! l!!!!!!!I 1!!!!!!11 11!!!!1 l!!!!I Siiiiiil
-- -----AM -,;D iiii,i, Y S I 'iioili,l,i<AG Eillliiiif SY liiiiioli,W
-"""""REG""'9IV 1"""" AT~ GA .... &Iii METALS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95523
SOURCE, WEYERHAEUSER CO.
STATION ID, 003-SD
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SOIL FROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 MD NUMBER, KA60
BY, D RUMFORD
ST, NC
1115 STOP, 00/00/00
** •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** MG/KG
21000
6UR
3U
190
0.26U
0.44U
1900 41
20U
27
36000
20
3500
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
990
0.2U
15J
2100
1.lU
1.2U 150U
2 .3U
NA
62
110
55
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ANALYTICAL RESULTS
ZINC
PERCENT-MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
METALS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *' * * *
•• PROJECT NO. 95-0295 SAMPLE NO. 95517 SAMPLE TYPE, GROUNDWA
** SOURCE: WEYERHAEUSER CO.
** STATION ID: 001-DW
** CASE NUMBER: 23680 SAS NUMBER:
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
MD NUMBER, KASS
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
08/03/95
* * * ***
**
**
**
**
** ** *** * * * * * * * * * "* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L
lUJ 0.38J
SUJ
16000J
3UJ
3UJ
57000J
6UJ
NA
ANALYTICAL RESULTS UG/L
20UJ
20UJ
4UJ
6UJ
lUJ
lUJ
4SOOOJ
SUJ
2UJ
6UJ
70UJ
3UJ
2SOOOJ
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REM.ARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
3UJ
590J
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------.. 1!!!111 I!!!!!!! 1!1111111 == lliiiiil iiiiii iiiii
-- --METALS DATA REPORT - -
_,AM~D -YSI-.AO_, S'll!!BI
~REG'!"ljff""IV ~ AT~, G~ 11!!!!1 0-95 -
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
** **
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 005-SW
CASE NUMBER, 23680
SAMPLE NO. 95516 co.
SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
MD NUMBER, KA54
BY, D RUMFORD
ST, NC
1455 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
200UJ
20UJ
4UJ
46J
lUJ
lUJ
llOOOUJ
5UJ
2UJ
3UJ
2000J
3UJ
2100J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
77J
0.2UJ
5UJ
2200J
3UJ
3UJ
8800J
6UJ
NA
4UJ
4UJ
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.• 08/03/95
METALS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ••
**
** •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95519
SOURCE, WEYERHAEUSER CO.
STATION ID, 006-SW CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
MD NUMBER, KA57
BY, D RUMFORD ST, NC
1640 STOP, 00/00/00
** ** **
** **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L
lBOUJ
20UJ 4UJ
46J
1UJ
2UJ
10000J
5UJ
2UJ
3UJ
1400J
3UJ
1900J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
. ***FOOTNOTES***
UG/L
53J 0.21J
5UJ
1900J
3UJ
3UJ
5SOOJ
6UJ
NA
3UJ
9UJ
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--- ---111!!!11 !!!!!I !!!!I == liiiiia iiii liiii
----METALS DATA REPORT -_AM,...,,D a.t,,sI..-iAGia.l SY-
EPA-REGION IV ESD, ATHENS, GA. 11111111 ==
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 101-DW
CASE NUMBER, 23680
SAMPLE NO. 95518 co.
SAS NUMBER,
SAMPLE TYPE, GROUNDWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
MD NUMBER, KA56
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
20UJ . 20UJ
4UJ
5UJ
1UJ
1UJ
44000J .5UJ
2UJ
4UJ
50UJ
3UJ
25000J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
UG/L
1UJ
0.2UJ
5UJ
16000J
3UJ
3UJ
57000J
6UJ
NA
3UJ
630J
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT-SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/03/95
METALS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
•• ..
•• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95520
SOURCE, WEYERHAEUSER CO.
STATION ID, 006-SD
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
MD NUMBER, KASS
BY, D RUMFORD
ST, NC
1650 STOP, 00/00/00
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
MG/KG
7100
4.5UR
2U 41
0.20U 0.33U
1300
8.7
3U
7.7J
6800
31 450
ALUMINUM ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***FOOTNOTES***
ANALYTICAL RESULTS MG/KG
55
0.09U
3U
390
0.82U
0.89U
70U
1. 7U
NA
20U
40U
41
ANALYTICAL RESULTS
MANGANESE MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE-IS KNOWN TO BE LESS THAN VALUE GIVEN *L·ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--- ----l!l!!!!I l!!!!I == liliiiiil liiiiil iiiii -
--- --METALS DATA REPORT -----SAMPLE·AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
111111 l!!!!!E!!
08/03/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROJECT NO. 95-0295 SOURCE,
STATION ID, 012-PB CASE NUMBER, 23680
SAMPLE NO. 95522
SAS NUMBER,
•• •• •• •• •• ••• ••• * * * * * * * * * * * * * * * * * UG/L 20UJ
20UJ
4UJ
2UJ
lUJ lUJ
30UJ
5UJ
2UJ
3UJ
lOUJ
3UJ
40UJ
ALUMINUM
ANTIMONY
ARSENIC BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
***REMARKS***
ANALYTICAL RESULTS
SAMPLE RECEIVED WITH A PH GREATER THAN 2
***FOOTNOTES***
SAMPLE TYPE, WATER PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/20/95 MD NUMBER , KA5 9
BY, D RUMFORD ST, NC
1800 STOP, 00/00/00
* * * * * * * * * * .~ * * • • • • • • • • • * * * * * * * * * * * * * * * * * * * * UG/L
lUJ
O.lOUJ
5UJ
90UJ
3UJ
3UJ
44J
6UJ
NA
3UJ
3UJ
MANGANESE
MERCURY NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
***REMARKS***
ANALYTICAL RESULTS
•• •• •• •• •• •••
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
I
INORGANIC DATA QUALIFIERS REPORT I
Case Number:_.2~3~6=8~0,__ ______________ _
Project Number:~9~5~--0=2~9~5~------------
Site: Weyerhaeuser Co. 1 Plymouth, NC
Element
A, Waters
Be,
Al,
Fe,
Cd,
Ba,
Na,
Se
K
Pb
Co,
Ca,
Zn
All Metals
!! -Soils
Be, Cd, Co,
Al, Ba, Ca,
Mg, Na, Zn
Se
Sb
Cr
As
Ni
As
Ag
v,
Cu,
V,
Fe,
Flag
u
u
J
J
u
J
u
u
J
J
R
J
u
u
J
J
Samples "Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
All with Al or Fe
Concentrations in solution
> 140,000 ug/L
All positives
MDKA64
MDKA54, 55, 56, 57, 59, 61,
64, 67, 69, & 71
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
All with Al or Fe
Concentrations in solution
> 140,000 ug/L
All positives
All negatives
All positives
MDKA58, 60, 63, 66, & 68
MDKA58
MDKA65
MDKA53
Reason
Baseline instability
Positives in blanks
Suspected over correction as
noted in the contractor ICS
I
I
I
I
Blind spike recovery> action limit I
%RSD > 20% for ICP multiple exposures
and results> IDL, but< CRDL
Sample pH> 2.0 when received by I
by the laboratory for metals analysis
Baseline instability
Positives in blanks
Suspected over correction as
noted in the contractor res
I
I
I
Matrix spike recovery 27. 7% I
Blind spike recovery> action limitJ
% RSD > 20% for ICP multipl
exposures and results > IDL, but<
CRDL J
% RSD > 20% for ICP multipl
exposures and results > IDL, but <
CRDL
Only analysis
required by
analysis
Only analysis
required by
analysis
of 2X
contract
of 2X
contract
CRDL
sow
CRDL
sow
standarJ
for ICP
standarJ
for ICP
I
I
I
.:.: .._
I
I
I
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
l***MEMORANDUM******
I DATE: 08/04/95
rBJECT: Results
95-0295
of Metals Analysis;
WEYERHAEUSER CO.
PLYMOUTH NC
CASE NO: 23680
I FROM: Charles H. Hooper
Chief, Laboratory Evaluation/Quality Assurance Section
I
••
TO: PAT DEROSA
Attached are the results of analysis of samples collected as part of re subject project.
As a result of the Quality Assurance Review, certain data qualifiers 11::Y have been placed on the data. Attached is a DATA QUALIFIER
FPORT which explains the reasons that these qualifiers were required.
I
I
I
••
I
I
you have any questions please contact me.
ATTACHMENT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/24/95
DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
**
** ** ** **
PROJECT NO. 95-0296 SAMPLE NO. 95498 SAMPLE TYPE, GROUNDWA
SOURCE, WEYERHAEUSER CO
STATION ID, 101-DW
CASE NUMBER, 0 SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D NUMBER, 101DW
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
**
** **
** ..
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/L
0.0120
0.012UJ
0.060
0.06UJ
0.060
0.060
0.060
0.06UJ
0.060
0.06UJ
0.120
0.0120
0.012UJ
0.060
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.060
0.06UJ
0.060
0.060
0.060
0.060
0.06UJ
0.06U
0.06U
0.06UJ
0.120
0
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACl!LORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA.UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--11!!!!1 l!!l!!!!I !!!!I l!!!!I liiiiiil iiiil iiiii -
--- -
DIOXIN/FURAN DATA REPORT --AM~D -YSI'!!!l!!!llAG~ SYll!li!!I ~REGiml""'IV e'S'rr," AT~ GA. li!!I!!!!! 11!1!!1 0 B ~ 5 -
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0296 SAMPLE NO. 95497 SAMPLE TYPE, SURFACEWA
SOURCE, WEYERHAEUSER CO
STATION ID, 006-SW
CASE NUMBER, 0 SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D NUMBER, 006SW
BY, D RUMFORD
ST, NC
1640 STOP, 00/00/00
** ••
** •• ..
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/L
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0. 06UJ
0.06U
0.06UJ
0 .12U
0.012U
0.03UJ
0.06U
ANALYTICAL RESULTS
2,3,7,B TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.06U
0.06UJ
0 .06U
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06U
0.06UJ
0.12U
0
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT.ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT .
. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY. OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
DIOXIN/FURAN DATA REPORT
*** * * * * * * * * * * * ** PROJECT NO. 95-0296 ** SOURCE: WEYERHAEUSER ** STATION ID: 006-SD
** CASE NUMBER: 0 ••
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * SAMPLE NO. 95496 SAMPLE TYPE, SOIL co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D NUMBER, 006SD
BY, D RUMFORD
ST, NC
1650 STOP, 00/00/00
08/24/95
•• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * *** NG/KG
4.9J
5.5J
5.0U
5.0UJ
5.0U
1.5J
2.2J
12J
39J
52J
1900
39
79J
5.0U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTA1)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTA1)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTA1)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTA1)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTA1)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
NG/KG
5.0U
5.0UJ
5.0U
5.0U
5.0U
5.0U
5.0UJ
2.7J
5.0U
2.7J
8.2J
12J
43
ANA1YTICA1 RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTA1)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTA1) 1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTA1)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VA1UE, FROM I-TEF/89)
% MOISTURE
***FOOTNOTES*** *A-AVERAGE VA1UE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VA1UE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIA1
•K-ACTUA1 VA1UE IS KNOWN TO BE LESS THAN VA1UE GIVEN *L-ACTUA1 VALUE IS KNOWN TO BE GREATER THAN VA1UE GIVEN
*U-MATERIA1 WAS ANA1YZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT QATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT, RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-----l!!!I!! l!!!!!!I l!!!!I == &iii liiiii iiiil
----DIOXIN/FURAN DATA REPORT - -
-AM~D ~SI~AGE-SY-~REGfflrIV 8;;n-:""ATHll'f'l'S7 GA. 11!111 !111!!!!1 0 8 ~ 5 11!!!!1
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** **
**
PROJECT NO. 95-0296 SAMPLE NO. 95495 SAMPLE TYPE, SURFACEWA
SOURCE, WEYERHAEUSER CO
STATION ID, 005-SW
CASE NUMBER, 0 SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D NUMBER, 005SW
BY, D RUMFORD
ST, NC
1455 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/L
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0.06U
0. 06UJ
0.12U
0.012U
0.012UJ
0.06U
ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06U
0.06UJ
0.12U
0
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND .MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *
•• PROJECT NO. 95-0296 SAMPLE NO. 95494 SAMPLE TYPE, SOIL
** SOURCE: WEYERHAEUSER CO
** STATION ID: 005-SD ** CASE NUMBER: 0 SAS NUMBER: SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D NUMBER, OOSSD
BY, D RUMFORD
ST, NC 1445 STOP, 00/00/00
08/24/95
* * * *** ••
** ** **
** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/KG
23J
23J s.ou
5.0UJ s.ou
3.8J
2.9J
26J
31
39J
920
160
330J
5.0U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL) .
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
NG/KG
5.0U 5.0UJ s.ou s.ou s.ou
5.0U
5.0UJ
2.8J
5.0U
8.3J
lOU
41
36
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
---- -
I!!!!!!! l!!l!!I 1!!!11 I!!!! l!!!!!!!!I l!!!!I ==
--- -DIOXIN/FURAN DATA REPORT ---AM~lrn _.SI~AGE-SY-EPA-REGION IV ESD, ATHENS, GA. -liliiil
*** * * * * * * * * * * * * * * * * * * * * * ·* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** **
**
PROJECT NO. 95-0296
SOURCE, WEYERHAEUSER
STATION ID, 001-DW
CASE NUMBER, 0
SAMPLE NO. 95493 SAMPLE TYPE, GROUNDWA co
SAS NUMBER, · SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95 D NUMBER, OOlDW
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
**
**
** **
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/L
0.012U
0.012UJ 0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06UJ
0.12U
0.012U
0.012UJ
0.06U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06U 0.06UJ
0.06U
0.06U
. 0.06UJ
0.12U
0
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFUR.AN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/24/95
DIOXIN/FURAN DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0296 SAMPLE NO. 95492 SAMPLE TYPE, SOIL
SOURCE, WEYERHAEUSER CO
STATION ID, 108-SD CASE NUMBER, 0 SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D NUMBER, 108SD
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG
l.OU
6.8J s.ou
3.SJ
2.5J
3.3J
4.5J
71J
120
160J
SOOOJ
2.0U
7.0UJ s.ou
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7;8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/KG s.ou
4 .4J s.ou s.ou s.ou
l.lJ
6.3J
11 s.ou
26J
16
7 .SJ
so
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
------l!l!!!!!I l!!l!I l!!!!I I!!!!! == == liiiiil
-- --DIOXIN/FURAN DATA REPORT - -
-AM~D _,.SI~AG~ SY-~REGfflrIV ~AT~ GA. --08.,5 1!11!!
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0296
SOURCE, WEYERHAEUSER
STATION ID, 17-SW
CASE NUMBER, 0
SAMPLE NO. 95491 SAMPLE TYPE, SURFACEWA co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D NUMBER, 107SW
BY, D RUMFORD.
ST, NC
1415 STOP, 00/00/00
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •· * * * * * * * * * * *. * * * * * * * * * *** NG/L
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06UJ
0. llJ
0.012U
0.012UJ
0.06U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
l,2,3,7,8·PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.06U
0.06UJ
0.06U
0.06U 0.06U
0.06U
0.06UJ
0.06U
0.06U
0.06UJ
0.12U
0. 000llJ
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS.NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/24/95
DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
** ** •• •• ••
PROJECT NO. 95-0296
SOURCE, WEYERHAEUSER
STATION ID, 107-SD
CASE NUMBER, 0
SAMPLE NO. 95490 SAMPLE TYPE, SOIL co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D NUMBER, 107SD
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
** ••
** ••
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/KG
l.OU
9.7J
5.0U
5.0UJ
5.0U
6.5
5.0U
llOJ
200
520J
8000J
6.0U
15J
5.0U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
NG/KG
5.0U
16J
5.0U
5.0U
5.0U
5.0U
.13J
18
5.0U
38J
22
llJ
58
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
---- -
-.11!!!1!1 l!!l!!I l!!!!!!I !!!:!I l!l!!!!!I == ==
------_,ru•,'lilf~~c.iliiliili~-'-jlliiiiif~~;-G~ -lallll == m:I lllll\iiil 081!!!!1!195 I!!!!! .DIOXIN/FURAN DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. *** **
**
**
**
**
PROJECT NO. 95-0296 SAMPLE NO. 95489 SAMPLE TYPE, SURFACEWA
SOURCE, WEYERHAEUSER CO
STATION ID, 008-SW
CASE NUMBER, 0 SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D NUMBER, 008SW
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/L
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0,009J
0.017J
0.18
0.012U
0.012UJ
0.06U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1, 2, 3, 6, 7, 8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0 .06U
0.06UJ
0.06U
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06U
0.06UJ
0.12
0.00027
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
J.l.U.l\..LP/ • ~•~-• __
*** * * * * * * * * * ~ R
**
**
**
**
**
PROJECT NO. 95-0296 SAMPLE NO. 95488 ::>1-U'lt'uc.
SOURCE, WEYERHAEUSER CO
STATION ID, 008-SD
CASE NUMBER, 0 SAS NUMBER, SPR
L.l. l. 1; .i: ........ ·---
COLLECTION START: 06/2U/~~ ~~JV
D NUMBER, 008SD **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/KG
l.OU
8.9J
5.0U
3.2J
1. 5J
3. 7J
4.3J
75J
l.10
140J
4300J
1.0U
lOJ
5.0U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN

TETRACHLORODIBENZODIOXIN
(
T
O
T
A
L
)

1,2,3,7,8 PENTACHLORODIBENZODIOXIN

PENTACHLORODIBENZODIOXIN
(
T
O
T
A
L
)

1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN
(
T
O
T
A
L
J

1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN
(
T
O
T
A
L
)

OCTACHLORODIBENZODIOXIN(T
O
T
A
L
}

2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN
(
T
O
T
A
L
)

1,2,3,7,8 PENTACHLORODIBENZOFURAN

NG/KG
5.0U
9.0J
5.0U
5.0U
5.0U
1. 3J
8.9J
9.2
5.0U
26J
22
6.6J
48
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(T
O
T
A
L
)

1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(T
O
T
A
L
)

1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN

1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TO
T
A
L
)

OCTACHLORODIBENZOFURAN(TOTA
L
)

TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION .
------. ·_ ,·.·
>~---== == -. liiiill
-h~l~-~*-~E--** PROJECT NO. 95-0296 ** SOURCE: WEYERHAEUSER ** STATION ID: 007-SD ** CASE NUMBER: 0 **
1111 == --...... * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *
SAMPLE NO. 95487 SAMPLE TYPE, SOIL co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED CITY, PLYMOUTH COLLECTION START, 06/20/95 D NUMBER, 007SD
BY, D RUMFORD ST, NC 1430 STOP, 00/00/00
-· !l!l!!I 1i'1i72 4 / 9 S
* * * * *** **
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/KG
1.0U
12J s.ou
S.3J
2.7J
6.0
6.8
130J
190
320J
7300J s.ou
16J s.ou
ANALYTICAL RESULTS 2,3,7,B TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,B PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/KG
1. 7J
12J s.ou
l.OJ s.ou
1.7J 23J.
23 s.ou
S2J
26
12J
SB
ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN 1,2,3,6,7,8 HEXACHLORODIBENZOFURAN 1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESl\MPLING.AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
DIOXIN/FURAN DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *
** PROJECT NO. 95-0296 SAMPLE NO. 95486 SAMPLE TYPE, SURFACEWA
** SOURCE: WEYERHAEUSER CO ** STATION ID: 004-SW ** CASE NUMBER: 0 SAS NUMBER: SPR
**
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D NUMBER, 004SW
BY, D RUMFORD
ST, NC
1150 STOP, 00/00/00
08/24/95
* * * ***
**
**
**
** **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * *. ***
NG/L
0. 014U
0.014UJ
0.07U
0.07UJ
0.07U
0.07U
0.07U
0.07UJ
0.008J
0.017J
0.12J
0. 014U
0. 014UJ
0.07U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,"8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL) 1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
NG/L
0.07U
0.07UJ
0.07U
0.07U
0.07U
0.07U
0.07UJ
0.07U
0.07U
0.07UJ
0 .14U
0.0002J
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED · *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-- ----11111! I!!!!! l!!!!!!!!I l!!l!!!!I l!!!!!I == iiii
--- -DIOXIN/FURAN DATA REPORT ---AM~D _,,SI-!AGialli SY-· -EPA-REGION IV ESD, ATHENS, GA. == 11119 0 8 "'9 5 I!!!!!!!!
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0296
SOURCE, WEYERHAEUSER
STATION ID, 004-SD
CASE NUMBER, 0
SAMPLE NO. 95485 SAMPLE TYPE, SOIL co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED BY, D RUMFORD
CITY, PLYMOUTH ST, NC
COLLECTION START, 06/20/95 1200 STOP, 00/00/00
D NUMBER, 004SD
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** NG/KG
17J
24J
5.0U
5.0UJ
1.9J
3.9J
3.6J
59J
97
310J
3100
89
190J
5.0U
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/KG
5,0U
5.0UJ
2.SJ
0.74J
5.0U
1.4J
20J
20
5.0U
50J
29
32J
67
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN
2,3,4,6,7,8 HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE rs KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION,
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
DIOXIN/FURAN DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *
•• PROJECT NO. 95-0296 SAMPLE NO. 95484 SAMPLE TYPE, SOIL
** SOURCE: WEYERHAEUSER CO
** STATION ID: 003-SD
** CASE NUMBER, 0 SAS NUMBER, SPR
**
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
0 NUMBER, 003SO
BY, 0 RUMFORD
ST, NC
1115 STOP, 00/00/00
08/24/95
* * * ***
**
** •• •• ..
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
NG/KG
2.lJ
7. 3J
lOU
lOUJ
l.lJ
1. 7J
2.0J
30J
57
160J
2500J
10
18J
lOU
ANALYTICAL RESULTS
2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZOOIOXIN(TOTAL)
1,2,3,7,8 PENTACHLOROOIBENZOOIOXIN
PENTACHLOROOIBENZOOIOXIN{TOTAL)
1,2,3,4,7,8 HEXACHLOROOIBENZOOIOXIN
1,2,3,6,7,8 HEXACHLOROOIBENZOOIOXIN
1,2,3,7,8,9 HEXACHLOROOIBENZOOIOXIN
HEXACHLOROOIBENZOOIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLOROOIBENZOOIOXIN
HEPTACHLOROOIBENZOOIOXIN(TOTAL)
OCTACHLOROOIBENZOOIOXIN(TOTAL)
2,3,7,8 TETRACHLOROOIBENZOFURAN
TETRACHLOROOIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLOROOIBENZOFURAN
NG/KG
lOU
1. 6J
lOU
lOU
lOU
lOU
5. 7J
7.2J
lOU
17J
8.8J
6.7
55
ANALYTICAL RESULTS
2,3,4,7,8 PENTACHLOROOIBENZOFURAN
PENTACHLOROOIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLOROOIBENZOFURAN
1,2,3,6,7,8 HEXACHLOROOIBENZOFURAN
1,2,3,7,8,9 HEXACHLOROOIBENZOFURAN
2,3,4,6,7,8 HEXACHLOROOIBENZOFURAN
HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLOROOIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLOROOIBENZOFURAN
HEPTACHLOROOIBENZOFURAN(TOTAL)
OCTACHLOROOIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV. VALUE, FROM I-TEF/89)
% MOISTURE
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATEO VALUE. *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. .
*R-QC_INOICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING ANO REANALYSIS IS NECESSARY FOR VERIFICATION.
-----1111!!!1 !!!!!I 11!!!1 == ;;a iiiiii --
- - -- ---1!!!11! l!!!!I -08/24/95 DIOXIN/FURAN DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0296 SOURCE, WEYERHAEUSER STATION ID, 002-DW CASE NUMBER, 0
SAMPLE NO. 95483 SAMPLE TYPE, GROUNDWA co
SAS NUMBER, SPR
PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/20/95 D NUMBER, 002DW
BY, D RUMFORD ST, NC
1515 STOP, 00/00/00
**
**
**
** •• ***·* * * * * * * * * * * * * * * * * * * * * •· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. *** NG/L
0.012U
0.012UJ
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06UJ
0.06U
0.06UJ
0.12U
0.012U
0.012UJ
0.06U
ANALYTICAL RESULTS 2,3,7,8 TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZODIOXIN 1,2,3,6,7,8 HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9 HEXACHLORODIBENZODIOXIN HEXACHLORODIBENZODIOXIN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN(TOTAL)
OCTACHLORODIBENZODIOXIN(TOTAL)
·2,3,7,8 TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN(TOTAL)
1,2,3,7,8 PENTACHLORODIBENZOFURAN
***FOOTNOTES***
NG/L
0.06U
0.06UJ
0.06U
0.06U
0.06U
0.06U 0.06UJ
0.06U
0.06U
0.06UJ
0.12U
0
ANALYTICAL RESULTS 2,3,4,7,8 PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,7,8 HEXACHLORODIBENZOFURAN
1,2,3,6,7,8 HEXACHLORODIBENZOFURAN
1,2,3,7,8,9 HEXACHLORODIBENZOFURAN 2,3,4,6,7,8 HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN(TOTAL)
1,2,3,4,6,7,8 HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9 HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN(TOTAL)
OCTACHLORODIBENZOFURAN(TOTAL)
TEQ(TOXIC. EQUIV_. VALUE, FROM I-TEF/89)
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPµING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
95492 123478-HxCDD J 1
123678-HxCDD J 1
123789-HxCDD J 1
OCDD J 2
234678-HxCDF J 1
95494 2378-TCDD J high spike recovery
123678-HxCDD J 1
123789-HxCDD J 1
1234678-HpCDF J 1
95496 2378-TCDD J high spike recovery
123678-HxCDD J 1
123789-HxCDD J 1
1234678-HpCDD J high MS/MSD RPD
1234678-HpCDF J 1
OCDF J 1
TEQ's : The Toxic Equivalent (TEQ) represents a summation of
values from the individual equivalents that are calculated for
each of the 2,3,7,8 containing isomers. If 101 or greater of the
total value was from data considered to be estimated, then the
TEQ is reported as estimated (J flag).
Abbreviation Key:
TCDD = Tetrachlorodibenzodioxin TCDF = Tetrachlorodibenzofuran
PeCDD Penta " " " PeCDF Penta 11 11 11 11
HxCDD = Hexa 11 11 11 HxCDF = Hexa " 11 11 11
HpCDD = Hepta " " " HpCDF = Hepta " " " "
OCDD Octa " " " OCDF Octa " 1, ,1 r,
Reason Codes
1. Results lower than the minimum quantitation limit
2. Results higher than the maximum calibration limit
3. Poor precision on the 2,3,7,8-TCDF confirmation column
I
I
n
0
n
n
I
D
D
I
I
•
I
I
I
I
I
I
I DATA QUALIFIER REPORT
I Project No. : 95-0296
SPR No.: 44855
I Site Name: Weyerhaeuser Co., Plymouth, NC
Affected Flag
I Samples Analyte Used Reason
All total congeners J Assumed Resp. Factors/
D Cal. Stds not available
for all congeners
I 95484 2378-TCDD J high spike recovery
123478-HxCDD J 1
123678-HxCDD J 1
123789-HxCDD J 1
I OCDD J 2
1234678-HpCDF J 1
OCDF J 1
I 95485 2378-TCDD J high spike recovery
123478-HxCDD J 1
I 123678-HxCDD J 1
123789-HxCDD J 1
1234 78 -HxCDF J 1
123678-HxCDF J 1
I 234678-HxCDF J 1
95486 1234678-HpCDD J 1
I OCDD J 1
95487 123478-HxCDD J 1
OCDD J 2
I 23478-PeCDF J 1
123678-HxCDF J 1
234678-HxCDF J 1
I 95488 123478-HxCDD J 1
123678-HxCDD J 1
I 123789-HxCDD J 1
OCDD J 2
234678-HxCDF J 1
I 95489 1234678-HpCDD J 1
95490 OCDD J 2
I 95491 OCDD J 1
I
I
I
I
I
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
'ATE: 08/25/95
Results
95-0296
of Dioxin/Furan Analysis;
WEYERHAEUSER CO
PLYMOUTH NC
SAS NO: SPR
I r .
ROM: ~ Charles H. Hooper ~p LLL-c..5
Chief, Laboratory Evaluation/Quality Assurance Section
I
I TO: PAT DEROSA
Attached are the results of analysis of samples collected as part of
tf subject project.
As a result of the Quality Assurance Review, certain data qualifiers ml have been placed on the data. Attached is a DATA QUALIFIER
R ORT which explains the reasons that these qualifiers were required.
I
D
I
D
I
m
have any.questions please contact me.
ATTACHMENT
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 008-SD
CASE.NO., 23680
SAMPLE NO. 95528 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA65
BY, D RUMFORD ST, NC
1330 STOP, 00/00/00
MD NO, KA65
**
**
** **
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
20JN
***FOOTNOTES•••
ANALYTICAL RESULTS UG/KG
DIMETHYSULFIDE
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES ·•J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--1!!11 l!l!!!!!I 111191 == ; llilil liiii iiiiii ---- - - -- -
- - ---Illa .111;1,PLJ!!!III ANfllllis IIIIEMillllllYsT .. --- -- -
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
** ••
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 003-SD
CASE .NO., 23680
SAMPLE NO. 95523 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA60
BY, D RUMFORD
ST, NC
1115 STOP, 00/00/00
MD NO, KA60
** ••
**
** ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
20JN
***FOOTNOTES***
ANALYTICAL RESULTS UG/KG
DIMETHYLSULFIDE
*A-AVERAGE VALUE *NA-NOT.ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SOURCE, WEYERHAEUSER
STATION ID, 006-SD
CASE.NO., 23680
SAMPLE NO. 95520 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KAASB
BY, D RUMFORD
ST, NC
1650 STOP, 00/00/00
MD NO, KASS
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
***FOOTNOTES***
ANALYTICAL RESULTS UG/KG
20J 1 UNIDENTIFIED COMPOUND
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--!!!II == lliiiiil - -- -- - - --- -
-- --raa IJ!!BMPLll!IIJ ~IS _,EMalilYs .... - -- - - -PURGEABLE ORGANICS DATA REPORT EPA-REGION IV ESD, ATHENS, GA. OB/ll/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95534
SOURCE, WEYERHAEUSER CO.
STATION ID, 002-DW
CASE NO., 23680
SAMPLE TYPE, DRKWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
BY, D RUMFORD
ST, NC
1515 STOP, 00/00/00
**
**
**
**
** D. NO., KA71 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
** ** ** **
PROJECT NO. 95-0295 SAMPLE NO. 95533
SOURCE, WEYERHAEUSER CO.
STATION ID, 107-SD
CASE NO., 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA70
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
** **
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
24U
24U
24U
24U 24U
60U
24U
24U
24U
24U
24U
24U
lOJ
24U
24U
24U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U
24U 24U
24U
59
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS--1, 3 -DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE STYRENE.
TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO Bil LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
---== iiii -- -- - -- -- -
- -PURGEABLE ORGANICS DATA REPORT
.PL"'° Jl!!ffl:rn -GEMl!llllsYs ..
. EPA-REGION IV ESD, ATHENS, GA. -- - -- -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 107-SW
CASE NO., 23680
SAMPLE NO. 95532 co. SAMPLE TYPE, SURFACEWA
SAS NO.:
FROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
BY: D RUMFORD
ST: NC
1415 STOP: 00/00/00
•• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
D. NO.: KA69
UG/L
lOU lOU
lOU
lOU
lOU
20U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1, 1-DICHLOROET!IANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
**
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95531
SOURCE, WEYERHAEUSER CO.
STATION ID, 007-SD
CASE NO., 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA68
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
**
** •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
21U
21U
21U
21U
21U 30U
21U
21U
21U
21U
21U
21U
21U
21U
21U
21U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE.CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG
21U
21U
21U 21U 21U
21U
21U
21U
21U
21U
21U
21U
21U
21U
21U
21U
21U
52
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE rs KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE rs KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT.
·*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION.
--1!!!!!!1!11 I!!!!! == ;;;;a iiiiii iiil -- - - --- -
- --PURGEABLE ORGANICS DATA REPORT --lilllMPLllll, AJlllll Is llllllGEMl!ll!IJlsys-
EPA-REG I ON IV ESD, ATHENS, GA. --- -- - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * *** •• ••
** •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 007-SW
CASE NO., 23680
SAMPLE NO. 95530 co . SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA67
BY, D RUMFORD
ST, NC
1415 STOP, 00/00/00
•• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
"*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
BAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * *** **
**
**
** **
PROJECT NO. 95-0295 SAMPLE NO. 95529 SOURCE, WEYERHAEUSER CO.
STATION ID, 108,SD
CASE NO., 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA66
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
**
**
**
**
**
*** * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANA1YTICAL RESULTS
13U CHLOROMETHANE
13U BROMOMETHANE
13U VINYL CHLORIDE 13U CHLOROETHANE 13U METHYLENE CHLORIDE
13U ACETONE
13U CARBON DISULFIDE
13U 1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
13U 1,1-DICHLOROETHANE
13U 1,2-DICHLOROETHENE (TOTA1)
13 U CHLOROFORM 13U 1,2-DICHLOROETHANE
13U METHYL ETHYL KETONE
13U 1,1,1-TRICHLOROETHANE
13U CARBON TETRACHLORIDE
13U BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG ANA1YTICA1 RESULTS
13U 1,2-DICHLOROPROPANE
13U CIS-1,3-DICHLOROPROPENE
13U TRICHLOROETHENE(TRICHLOROETHYLENE)
13U DIBROMOCHLOROMETHANE
13U 1,1,2-TRICHLOROETHANE
13U BENZENE
13U TRANS-1,3-DICHLOROPROPENE
13U BROMOFORM 13U METHYL ISOBUTYL KETONE
13U METHYL BUTY"L KETONE
13U TETRACHLOROETHENE(TETRACHLOROETHYLENE)
13U 1,1,2,2-TETRACHLOROETHANE
13U TOLUENE
13U CHLOROBENZENE
13U ETHYL BENZENE
13U STYRENE
13U TOTAL XYLENES
24 PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VA1UE *NA-NOT ANA1YZED *NAI-INTERFERENCES *J-ESTIMATED VA1UE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIA1
*K-ACTUA1 VA1UE IS KNOWN TO BE LESS THAN VA1UE GIVEN *L-ACTUA1 VA1UE IS KNOWN TO BE GREATER THAN VA1UE GIVEN
*U-MATERIA1 WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANA1YSIS IS NECESSARY FOR VERIFICATION. .. I!!!!! l!!!!!I == iiiii liiiiil --·----- - --
--·--.iPL~ AN-IS ~-EM~YST .. -- --·--EPA-REGION IV ESD, ATHENS, GA. 08/ll/95 PURGEABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95528 SOURCE, WEYERHAEUSER CO .
STATION ID, 008-SD
CASE NO., 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA65
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
•• •• •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
20U
20U
20U
20U
20U
40U
7J
20U
20U
20U
20U
20U
20U
20U
20U
20U
ANALYTICAL RESULTS
Cl!LOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
Cl!LOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U
20U so
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 008-SW
CASE NO. , 23680
SAMPLE NO. 95527 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D.NO.,KA64
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
•• • • •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
10U
10U
lOU
10U
lOU
10U
lOU
10U lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICIILOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACIILOROETIIYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED .*NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER rs THE MINIMUM QUANTITATION LIMIT.
·•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
liiia iiiil --- -- -
-- -- --
-l!!!l!I .. ------SAMPLE AND ANALYSIS MANAGEMENT SYSTEM -- --- -PURGEABLE ORGANICS DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 004-SD
CASE NO., 23680
SAMPLE NO. 95526 co . SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA63
BY, D RUMFORD
ST, NC
1200 STOP, 00/00/00
•• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS
13U CHLOROMETHANE
13U BROMOMETHANE
13U VINYL CHLORIDE
13U CHLOROETHANE
13U METHYLENE CHLORIDE
SOU ACETONE
13U CARBON DISULFIDE
13U 1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
13U 1,1-DICHLOROETHANE
13U 1,2-DICHLOROETHENE (TOTAL)
13U CHLOROFORM
13U 1·, 2-DICHLOROETHANE
9J METHYL ETHYL KETONE
13U 1,1,1-TRICHLOROETHANE
13U CARBON TETRACHLORIDE
13U BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
24
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
"*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95525
SOURCE, WEYERHAEUSER CO.
STATION ID, 004-SW
SAMPLE TYPE, SURFACEWA_
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA62
BY, D RUMFORD
ST, NC
1150 STOP, 00/00/00
•• •• •• • • •• CASE NO., 23680
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
.*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ·•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--l!!!l!!I l!!!!!I == la'iiil iiiii -liiil --- - - -
--PURGEABLE ORGANICS DATA REPORT
-· IIIJ!!!!1PL~ ANll.!lrs rlllilEME.MYsT-EPA-REGION IV ESD, ATHENS, GA. -- --- -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 003-SW
CASE NO., 23680
SAMPLE NO. 95524 co . SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA61
BY, D RUMFORD
ST, NC
1110 STOP, 00/00/00
•• •• •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAl RESULTS
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
10U
ANALYTICAl RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
'*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT •••• * •••• * * * * •• * * * * * * * * * *. *. * .-•• *. * * * * * * * * * * * *. * * •• * * * *. * * * * * * * ••••• •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 003-SD
SAMPLE NO. 95523 co.
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D.NO.,KA60
BY, D RUMFORD
ST, NC
1115 STOP, 00/00/00
•• •• • • •• •• CASE NO., 23680 ***. *. * * *. * * * * * * * * * * * *. * * * * * * * *. * * * * *. * * * * * * * * * * •• * * * * * * * * * * * * * * * ***
UG/KG
14U
14U
14U
14U
14U
60U
14U
14U
14U
14U
14U
14U
12J
14U
14U
14U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
ACETONE CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
UG/KG
14U
14U 14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
26
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
***FOOTNOTES*** •A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. •R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
l!l!!!S == iiiiii iiii ---- - -----
11!!1!1 -lil!ltPLiJIIII ANlll!l!IIs ral!lt;EMEMYsT .. -- --- -
PURGEABLE ORGANICS DATA REPORT EPA-REGION IV ESD, ATHENS, GA. 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 011-TP
CASE NO. , 23680
SAMPLE NO. 95521 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
BY, D RUMFORD
ST, NC
1300 STOP, 00/00/00
**
**
** **
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
D. NO., KA59
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
CHLOROMETHANE
BROMOMETHANE
ANALYTICAL RESULTS
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE) 1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE) DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·•R-QC INDICATES THAT-DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
I
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. REPRINTED ON 08/21/95
PURGEABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• ..
•• ••
PROJECT NO. 95-0295 SAMPLE NO. 95520
SOURCE, WEYERHAEUSER CO.
STATION ID, 006-SD
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KAA58
BY, D RUMFORD ST, NC
1650 STOP, 00/00/00
•• •• • • •• CASE NO., 23680 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/KG
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
UG/KG
13U
13U
13U
13U
13U
13U 13U
13U
13U
13U
13U
13U
13U 13U
13U
13U
13U
39
ANALYTICAL RESULTS
i,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL.KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
PERCENT MOISTURE
***REM.ARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-I!!!! l!!!!!I l!!!!!I lliiiia liiiiii liiiil iiiil ---- -
1111 liliiiil 1111,;1
PURGEABLE ORGANICS DATA REPORT
ll91PL1-AN-IS 1-EM~YST-E~GIOl'l""T'l' ESrr,-J\'l:'HE~A. l!!!!!!!!!I ---*** * •••• * •• *. * ••• * * * * *. * * * * ·*. * * * *. * ••• * *. * * * * * •• * • *. * •••• * * * * * * •• *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 006-SW
CASE NO. , 23680
SAMPLE NO. 95519 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA57
BY, D RUMFORD
ST, NC
1640 STOP, 00/00/00
•• •• •• • • ••
*** * * *. * *. * * *. * * * ••• * * •• * * * * * * *. *. * •• * * •.• * *. *. * * * * *. * * * * * * * * * * * * * *** UG/L
IOU
IOU IOU
IOU
IOU
IOU
IOU
IOU
IOU
IOU
IOU
IOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLO ROM ETHANE
BROMOMETHANE VINYL CHLORIDE
CHLO RO ETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,1-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
IOU
lOU
IOU
IOU
IOU
IOU
IOU
IOU
lOU
IOU
lOU
IOU
lOU
lOU
IOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE. *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
.•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** ** •• •• ** ••
PROJECT NO. 95-0295 SAMPLE NO. 95518
SOURCE, WEYERHAEUSER CO.
STATION ID, 101-DW
CASE NO., 23680
SAMPLE TYPE, GROUNDWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA56
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
** **
**
** ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
20U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLO ROM ETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE ETHYL BENZENE
STYRENE
TOTAL XYLENES
•
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
.*.U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
I!!!!!!! l!!l!I 11111111 lilliiil liiiil - - --- -----
lililiil 11!!1!
PURGEABLE ORGANICS DATA REPORT
1!1111!!11 l!lll!IILPL,.J ~IS ..,EMP.iYs1'11111
EPA-REGION IV ESD, ATHENS, GA. --- -- -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95517
SOURCE, WEYERHAEUSER CO . STATION ID, 001-DW
CASE NO., 23680
SAMPLE TYPE, GROUNDWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA55
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
•• •• •• • • •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTN'OTES***
UG/L
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U 10U
10U
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
-•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES.THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PURGEABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95516
SOURCE, WEYERHAEUSER CO.
STATION ID, 005-SW
SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA54
BY, D RUMFORD
ST, NC
1455 STOP, 00/00/00
**
** •• ** •• CASE NO., 23680
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE ,
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
-*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
l!!!!9 l!!l!I 1111111 == == liiiiiil liiiil iiil - - --- -- - -
1111
PURGEABLE ORGANICS DATA REPORT
lllliPLIIIWi MRis ~EM ... YS~
EPA-REGION IV ESD, ATHENS, GA. --- - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
** **
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95515
SOURCE, WEYERHAEUSER CO. STATION ID, 005-SD
CASE NO. , 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA53
BY, D RUMFORD
ST, NC
1445 STOP, 00/00/00
**
**
**
** **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
14U
14U
14U 14U
14U
30U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
ANALYTICAL RESULTS
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE(l,l-DICHLOROETHYLENE)
1,1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
***REMARKS***
***FOOTNOTES***
UG/KG
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U
14U 14U
30
ANALYTICAL RESULTS
1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE(TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE TOTAL XYLENES
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE. *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
ORGANIC DATA QUALIFIER REPORT
Case Number 23680 Project Number 95-0295 SAS Number
Site ID. Weyerhaeuser Co., Plymouth, NC
Affected Samples
Volatiles
95523,95526,
95533
95528
Extractables
95526
95529
95531
95533
Pesticides
all waters
95515
Compound or Fraction
2-butanone
J
carbon disulfide J
4-methylphenol J
phenanthrene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
pyrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
4,4'-DDE
aroclor-1016
methoxychlor
J
J
J
J
J
R
J
N
Flag
Used Reason
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantita!::ion limit
< quantitation limit
low blind spike recovery
unacceptable blind spike recovery
< quantitation limit
difference in column
quantitations
I
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
*l**MEMORANDUM******
.DATE: 08/12/95
I
I
Results
95-0295
TO: PAT DEROSA
of Purgeable Organic Analysis;
WEYERHAEUSER CO.
PLYMOUTH NC
RECEIVED
AUG 2 8 1995
SUPERFUNO SECTION
Attached are the results of analysis of samples collected as part of T subject project. ·
As a result of the Quality Assurance Review, certain data qualifiers
~ have been placed on the data. Attached is a DATA QUALIFIER
yoRT which explains the reasons that these qualifiers were required.
If
I
I
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I
you have any questions please contact me.
ATTACHMENT
SAMPLE·AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 95534 SAMPLE TYPE: DRKWA
** SOURCE: WEYERHAEUSER CO. ** STATION ID: 002-DW
•• CASE NUMBER, 23680 SAS NUMBER, ••
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA71
BY, D RUMFORD
ST: NC
1515 STOP: 00/00/00
08/11/95
• • • ••• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * *·* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
0.05U ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC O.lOU ENDRIN KETONE
0.05U DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016)
O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
O.lOUJ 4,4'-DDE (P,P'-DDE) l.OU PCB-1232 (AROCLOR 1232)
O.lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242)
O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248)
O.lOU 4, 4' -ODD (P,P'-DDD) 1.0U PCB-1254 (AROCLOR 1254)
O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260)
O.lOU 4,4'-DDT (P,P'-DDT)
***REMARKS*** **.*REMARKS***
**"!'FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•c-CONFIRMED BY GCMS 1. WHEN NO VALUE rs REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-liiiiiiil iiii - -- - - -- - --
-1111!11 -PESTICIDES/PCB'S DATA REPORT
-sAMilaAND-YS~AG~ s~ -EPA-REGION IV ESD, ATHENS, GA. - --- -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE: WEYERHAEUSER
STATION ID: 107-SD
CASE NUMBER: 23680
SAMPLE NO. 95533 co.
SAS NUMBER:
SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
D. NUMBER: KA70
BY: D RUMFORD
ST: NC
1430 STOP: 00/00/00
•• ** •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
3.9U ALPHA-BHC 39U METHOXYCHLOR 3.9U BETA-BHC 7 .SU ENDRIN KETONE 3.9U DELTA-BHC 7.SU ENDRIN ALDEHYDE 3.9U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 3.9U HEPTACHLOR 3.9U GAMMA-CHLORDANE /2 3.9U ALDRIN 3.9U ALPHA-CHLORDANE /2 3.9U HEPTACHLOR EPOXIDE 390U TOXAPHENE 3.9U ENDOSULFAN I (ALPHA) 75U PCB-1016 (AROCLOR 1016) 7.SU DIELDRIN 150U PCB-1221 (AROCLOR 1221) 7.SU 4,4' -DOE (P,P'-DDE) 75U PCB-1232 (AROCLOR 1232) 7.SU ENDRIN 75U PCB-1242 (AROCLOR 1242) 7.SU ENDOSULFAN II (BETA) 75U PCB-1248 (AROCLOR 1248) 7.SU 4,4'-DDD (P, P' -DDD) 75U PCB-1254 (AROCLOR 1254) 7.SU ENDOSULFAN SULFATE 75U PCB-1260 (AROCLOR 1260) 7.SU 4,4'-DDT (P,P' -DDT) 56 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CO~STITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
*** * * ~ * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 95532 SAMPLE TYPE, SURFACEWA ** SOURCE: WEYERHAEUSER CO. ** STATION ID: 107-SW ** CASE NUMBER: 23680 SAS NUMBER:
**
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA69
BY, D RUMFORD
ST, NC
1415 STOP, 00/00/00
08/11/95
* * * ***
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * ·• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016)
O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
0,10UJ 4, 4' -DOE (P, P' -ODE) l.OU PCB-1232 (AROCLOR 1232) 0.10U ENDRIN l.OU PCB-1242 (AROCLOR 1242)
0.10U ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248)
0.10U 4,4' -DDD (P, P' -DOD) l.OU PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260)
O.lOU 4,4'-DDT (P,P' -DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAT-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE-GIVEN
*U-MATERIAL WAS ANALYZED FOR.BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-== i:;;;;a liiiiil iiiiil - - -- - ------
PESTICIDES/PCB'S DATA REPORT
-AM~D-_,.SI-iAG_, SY-
~REGffl'r-r'"IV ~AT~ GA. - - ---00""95 -
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95531 'SAMPLE TYPE: SOIL SOURCE: WEYERHAEUSER CO .
STATION ID: 007-SD
CASE NUMBER: 23680 SAS NUMBER:
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
D. NUMBER: KA68
BY: D RUMFORD
ST: NC
1430 STOP: 00/00/00
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAI RESULTS
4.0U AIPHA-BHC 400 METHOXYCHLOR 4 .OU BETA-BHC 7.7U ENDR IN KETONE 4.0U DELTA-BHC 7.7U ENDRIN AIDEHYDE 4 .OU GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 4.0U HEPTACHLOR 4.0U GAMMA-CHLORDANE /2 4.0U AIDRIN 4.0U AIPHA-CHLORDANE /2 4 .OU HEPTACHLOR EPOXIDE 4000 TOXAPHENE 4.0U ENDOSULFAN I (AIPHA) 770 PCB-1016 (AROCLOR 1016) 7.7U DIELDRIN 160U PCB-1221 (AROCLOR 1221) 7.7U 4,4'-DDE (P,P' -DDE) 77U PCB-1232 (AROCLOR 1232) 7.7U ENDRIN 77U PCB-1242 (AROCLOR 1242) 7.7U ENDOSULFAN II (BETA) 77U PCB-1248 (AROCLOR 1248) 7.7U 4,4' -DDD (P, P' -DDD) 77U PCB-1254 (AROCLOR 1254) 7.7U ENDOSULFAN SULFATE 77U PCB-1260 (AROCLOR 1260) 7.7U 4, 4' -DDT (P, P' -DDT) 57 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VAIUE *NA-NOT ANAIYZED *NAI-INTERFERENCES *J-ESTIMATED VAIUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAI *K-ACTUAI VAIUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAI VAIUE IS KNOWN TO BE GREATER THAN VAIUE GIVEN
*U-MATERIAI WAS ANAIYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANAIYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VAIUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CON,STITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * *
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 007-SW
CASE NUMBER, 23680
SAMPLE NO. 95530 co. SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
BY, D RUMFORD
ST, NC
SAS NUMBER,
COLLECTION START, 06/20/95
D. NUMBER, KA67
1415 STOP, 00/00/00
08/11/95
* * * *** •• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR
o.osu BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE s.ou TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016)
O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
O.lOUJ 4, 4' -ODE (P, P' -ODE) l.OU PCB-1232 (AROCLOR 1232)
O.lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242)
O.lOU ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248)
O.lOU 4, 4' -DOD (P, P' -DDD) l.OU PCB-1254 (AROCLOR 1254)
O.lOU ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260)
O.lOU 4,4'-DDT (P,P' -DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CO~STITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
== == liiiiiil liiiiil liiii liii liiiii -liiil liiiil -- - - -
-PESTICIDES/PCB'S DATA REPORT
1!!!11!!11,AMi81!1BND l!!!!l!!IYSI-IAGJ-SY-EPA-REGION IV ESD, ATHENS, GA. 11!!!1!!!1 ---- --08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO .. 95-0295
SOURCE: WEYERHAEUSER
STATION ID: 108-SD CASE NUMBER, 23680
SAMPLE NO. 95529 co.
SAS NUMBER,
SAMPLE TYPE: SOIL PROG ELEM, NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
D. NUMBER: KA66
BY: D RUMFORD
ST, NC
1330 STOP: 00/00/00
**
**
**
** ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
3.1U ALPHA-BHC 31U METHOXYCHLOR 3.1U BETA-BHC 6.0U ENDRIN KETONE 3.lU DELTA-BHC 6.0U ENDRIN ALDEHYDE 3.lU GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 3.lU HEPTACHLOR 3.lU GAMMA-CHLORDANE /2 3.lU ALDRIN 3.1U ALPHA-CHLORDANE /2 3.1U HEPTACHLOR EPOXIDE 310U TOXAPHENE 3.1U ENDOSULFAN I (ALPHA) 60U PCB-1016 (AROCLOR 1016) 6.0U DIELDRIN 120U PCB-1221 (AROCLOR 1221) 6.0U 4,4'-DDE (P, P' -DOE) 60U PCB-1232 (AROCLOR 1232) 6.0U ENDRIN 60U PCB-1242 (AROCLOR 1242) 6.0U ENDOSULFAN II (BETA) 60U PCB-1248 (AROCLOR 1248) 6.0U 4, 4' -ODD (P, P' -ODD) 60U PCB-1254 (AROCLOR 1254) 6.0U ENDOSULFAN SULFATE 60U PCB-1260 (AROCLOR 1260) 6 .OU 4,4'-DDT (P,P'-DDT) 45 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • • • * * * * * * * * * * * * * * * * * * * * * * * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 95528 SAMPLE TYPE, SOIL
** SOURCE, WEYERHAEUSER CO. ** STATION ID: 008-SD ** CASE NUMBER: 23680 SAS NUMBER: ••
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA65
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
08/11/95
• • • • •• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
3.lU ALPHA-BHC 31U METHOXYCHLOR
3.lU BETA-BHC 6 .lU ENDRIN KETONE
3 .lU DELTA-BHC 6 .lU ENDRIN ALDEHYDE
3 .lU GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1
3.lU HEPTACHLOR 3.lU GAMMA-CHLORDANE /2
3.lU ALDRIN 3.lU ALPHA-CHLORDANE /2
3.lU HEPTACHLOR EPOXIDE 310U TOXAPHENE
3.lU ENDOSULFAN I (ALPHA) 61U PCB-1016 (AROCLOR 1016)
6.lU DIELDRIN 120U PCB-1221 (AROCLOR 1221)
6.lU 4,4'-DDE (P,P'-DDE) 61U PCB-1232 (AROCLOR 1232)
6.lU ENDRIN 61U PCB-1242 (AROCLOR 1242)
6.lU ENDOSULFAN II (BETA) 61U PCB-1248 (AROCLOR 1248)
6.lU 4,4'-DDD (P,P'-DDD) 61U PCB-1254 (AROCLOR 1254)
6.lU ENDOSULFAN SULFATE 61U PCB-1260 (AROCLOR 1260)
6.lU 4,4'-DDT (P, P' -DDT) 46 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
1111 == iiiil liiil - - ------- -
... -
1111!1 ·!11!!1 111111,AM....,.D -YSillll9lAG--S,,.. EPA-REGION IV ESD, ATHENS, GA. ----PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• ** •• ••
**
PROJECT NO. 95-0295 SAMPLE NO. 95527
SOURCE, WEYERHAEUSER CO. STATION ID, 008-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA64
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
** •• •• **
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * •.• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR 0. osu BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN 2 .OU PCB-1221 (AROCLOR 1221) O.lOUJ 4,4' -DOE (P,P'-DDE) l.OU PCB-1232 (AROCLOR 1232) 0. lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248) O.lOU 4,4' -DDD (P,P'-DDD) l.OU PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260) o:1ou 4,4'-DDT (P,P' -DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION. *C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PESTICIDES/PCB'S DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * •• * *** •• •• •• •• ••
PROJECT NO. 95-0295 SOURCE, WEYERHAEUSER STATION ID, 004-SD CASE NUMBER, 23680
SAMPLE NO. 95526 co.
SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF
CITY, PLYMOUTH
COLLECTION START,
D. NUMBER, KA63
COLLECTED BY, D RUMFORD
ST, NC
06/20/95 1200 STOP, 00/00/00
•• • • •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
5.0U ALPHA-BHC sou METHOXYCHLOR s.ou BETA-BHC 9.7U ENDRIN KETONE s.ou DELTA-BHC 9.7U ENDRIN ALDEHYDE
5.0U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 s.ou HEPTACHLOR 5.0U GAMMA-CHLORDANE /2
5.0U ALDRIN s.ou ALPHA-CHLORDANE /2 s.ou HEPTACHLOR EPOXIDE soou TOXAPHENE s.ou ENDOSULFAN I (ALPHA) 97U PCB-1016 (AROCLOR 1016)
9.7U DIELDRIN 200U PCB-1221 (AROCLOR 1221)
9.7U 4,4'-DDE (P, P' -DDE) 97U PCB-1232 (AROCLOR 1232)
9.7U ENDRIN 97U PCB-1242 (AROCLOR 1242)
9.7U ENDOSULFAN II (BETA) 97U PCB-1248 (AROCLOR 1248)
9.7U 4 ,4' -DOD (P,P' -DDD) 97U PCB-1254 (AROCLOR 1254)
9.7U ENDOSULFAN SULFATE 97U PCB-1260 (AROCLOR 1260)
9.7U 4,4'-DDT (P,P'-DDT) 66 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
.*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
;,;;a iiiil liiii ----- - -----
1111!1
PESTICIDES/PCB'S DATA REPORT
!!!!!I -AMP__,D ,-sI~AGE-SY-
~EG:rnr"IV ~ATH~ GA. -----08.5 -
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 004-SW
CASE NUMBER, 23680
SAMPLE NO. 95525 co.
SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA62
BY, D RUMFORD
ST, NC
1150 STOP, 00/00/00
**
**
** **
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR 0.05U BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR 0.05U GAMMA-CHLORDANE /2 0 :osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016) O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) O.lOUJ 4,4'-DDE (P, P' -DOE) 1.0U PCB-1232 (AROCLOR 1232) O.lOU ENDRIN 1.0U PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248) O.lOU 4,4'-DDD (P, P' -DOD) l.OU PCB-1254 (AROCLOR 1254) O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260) O.lOU 4,4'-DDT (P, P' -DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
PESTICIDES/PCB'S DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95524
SOURCE, WEYERHAEUSER CO.
STATION ID, 003-SW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NUMBER, KA61
BY, D RUMFORD
ST, NC 1110 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR
o.osu BETA-BHC 0.100 ENDRIN KETONE
o.osu DELTA-BHC 0.100 ENDRIN ALDEHYDE
o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1
o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2
o.osu ALDRIN o.osu ALPHA-CHLORDANE /2
o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE
o.osu ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016)
0.100 DIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
0.10UJ 4, 4' -ODE (P,P' -DOE) 1.0U PCB-1232 (AROCLOR 1232)
0.100 ENDRIN 1.0U PCB-1242 (AROCLOR 1242)
0.100 ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248)
0.100 4,4' -ODD (P,P'-DDD) 1.0U PCB-1254 (AROCLOR 1254)
0.100 ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260)
0.100 4,4'-DDT (P, P' -DDT)
***REMARKS*** ***REMARKS***.
***FOOTNOTES*"!'* *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES. *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. _CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
--l!l!!!I !!Ill l!!!!!!J ;;;a liiiiil iiiiii liliil liiiil .. - - --
-liiil -PESTICIDES/PCB'S DATA REPORT .. --SAMallooJ l!ll!,YSIBBr,AG9llr S,_ 1!11!!!!1 EPA-REGION IV ESD, ATHENS, GA. --*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
** ..
PROJECT NO. 95-0295
SOURCE: WEYERHAEUSER
STATION ID: 003-SD
CASE NUMBER: 23680
SAMPLE NO. 95523 co.
SAS NUMBER:
SAMPLE TYPE: SOIL PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
D. NUMBER: KA60
BY: D RUMFORD
ST: NC
1115 STOP: 00/00/00
**
**
**
**
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * *. * *** UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
3.5U ALPHA-BHC 35U METHOXYCHLOR 3.5U BETA-BHC 6.9U ENDRIN KETONE 3.5U DELTA-BHC 6.9U ENDRIN ALDEHYDE 3.5U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 3.SU HEPTACHLOR 3.SU GAMMA-CHLORDANE /2 3.SU ALDRIN 3.SU ALPHA-CHLORDANE /2 3.SU HEPTACHLOR EPOXIDE 3500 TOXAPHENE 3.SU ENDOSULFAN I (ALPHA) 69U PCB-1016 (AROCLOR 1016) 6.9U DIELDRIN 1400 PCB-1221 (AROCLOR 1221) 6.9U 4,4'-DDE (P,P' -DDE) 69U PCB-1232 (AROCLOR 1232) 6.9U ENDRIN 69U PCB-1242 (AROCLOR 1242) 6.9U ENDOSULFAN II (BETA) 69U PCB-1248 (AROCLOR 1248) 6.9U 4,4' -DDD (P,P' -DDD) 69U PCB-1254 (AROCLOR 1254) 6.9U ENDOSULFAN SULFATE 69U PCB-1260 (AROCLOR 1260) 6.9U 4,4' -DDT (P,P'-DDT) 52 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • • * * * * * * * * * * * * * * * * * * * * * * * • * *
•• PROJECT NO. 95-0295 SAMPLE NO. 95520 SAMPLE TYPE: SOIL
** SOURCE: WEYERHAEUSER CO. ** STATION ID: 006-SD ** CASE NUMBER: 23680 SAS NUMBER: ••
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/19/95
D. NUMBER: KAA58
BY: D RUMFORD
ST: NC
1650 STOP: 00/00/00
08/11/95
••• ••• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
2.BU ALPHA-BHC 28U METHOXYCHLOR
2.BU BETA-BHC 5.4U ENDRIN KETONE
2.BU DELTA-BHC 5.4U ENDRIN ALDEHYDE
2.BU GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1
2.BU HEPTACHLOR 2 .BU GAMMA-CHLORDANE /2
2.BU ALDRIN 2 .BU ALPHA-CHLORDANE /2
2.BU HEPTACHLOR EPOXIDE 280U TOXAPHENE
2.BU ENDOSULFAN I (ALPHA) 54U PCB-1016 (AROCLOR 1016)
5.4U DIELDRIN llOU PCB-1221 (AROCLOR 1221)
5.4U 4, 4' -ODE (P, P' -DDE) 54U PCB-1232 (AROCLOR 1232)
5.4U ENDRIN 54U PCB-1242 (AROCLOR 1242)
5.4U ENDOSULFAN II (BETA) 54U PCB-1248 (AROCLOR 1248)
5.4U 4, 4' -DDD (P, P' -DDD) 54U PCB-1254 (AROCLOR 1254)
5.4U ENDOSULFAN SULFATE 54U PCB-1260 (AROCLOR 1260)
5.4U 4,4'-DDT (P, P' -DDT) 39 PERCENT MOISTURE
. ***REMARKS*** ***REMARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
liiiil iiii - - -- ---------
l!!l!l!!!!J --PESTICIDES/PCB'S DATA REPORT
-AMi:aliaND ~SI~AGEIIII SY-~REGION IV ESD, ATHENS, GA. - - --*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 006-SW
CASE NUMBER, 23680
SAMPLE NO. 95519 co .
SAS NUMBER,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NUMBER, KA57
BY, D RUMFORD
ST, NC
1640 STOP, 00/00/00
•• •• •• •• • • *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC 0.10U ENDRIN KETONE o.osu DELTA-BHC 0.10U ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN a .osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE s.ou TOXAPHENE o.osu ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016) 0.10U DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) 0.10UJ 4,4' -ODE (P,P'-DDE) 1.0U PCB-1232 (AROCLOR 1232) 0.10U ENDRIN 1.0U PCB-1242 (AROCLOR 1242) 0.10U ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248) 0.10U 4 ,4' -DDD (P, P' -DDD) 1.0U PCB-1254 (AROCLOR 1254) 0.10U ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR ).260) 0.10U 4, 4' -DDT (P, P' -DDT)
***REM.ARKS***. ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * •• PROJECT NO. 95-0295 SAMPLE NO. 95518 SAMPLE TYPE, GROUNDWA·
** SOURCE: WEYERHAEUSER CO. ** STATION ID: 101-DW ** CASE NUMBER: 23680 SAS NUMBER: ••
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NUMBER, KA56
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
08/11/95
• • • ••• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE s.ou TOXAPHENE o.osu ENDOSULFAN I (ALPHA) 1.0UR PCB-1016 (AROCLOR 1016)
O.lOU OIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
O.lOUJ 4, 4' -DOE (P, P' -DOE) 1.0U PCB-1232 (AROCLOR 1232)
O.lOU ENDRIN 1.0U PCB-1242 (AROCLOR 1242)
O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248)
O.lOU 4,4' -DDD (P,P'-000) l.OU PCB-1254 (AROCLOR 1254)
O.lOU ENDOSULFAN SULFATE 1.0U PCB-1260 (AROCLOR 1260)
O.lOU 4,4' -DDT (P, P' -DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J~ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
.*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
liiiiiiii liiiii liiil. -- -- - --------
-PESTICIDES/PCB'S DATA REPORT
-· --AMPIIILD ..,SI~AGE-SY-EPA-REGION IV ESD, ATHENS, GA. - - -- - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95517
SOURCE, WEYERHAEUSER CO.
STATION ID, 001-DW
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, GROUNDWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NUMBER, KASS
BY, D RUMFORD
ST, NC
1605 STOP, 00/00/00
**
** •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *· * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC 0. lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE s.ou TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016)
O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221) O.lOUJ 4, 4' -DDE (P, P' -DDE) 1.0U PCB-1232 (AROCLOR 1232)
O.lOU ENDRIN 1.0U PCB-1242 (AROCLOR 1242) O.lOU ENDOSULFAN II (BETA) 1.0U PCB-1248 (AROCLOR 1248)
0.10U 4,4' -DDD (P, P' -DDD) 1.0U PCB-1254 (AROCLOR 1254) 0.10U ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260) 0.10U 4,4'-DDT (P,P'-DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE: COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •. * * * * * * * * * * * * * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 95516 SAMPLE TYPE, SURFACEWA
** SOURCE, WEYERHAEUSER CO.
** STATION ID: 005-SW ** CASE NUMBER: ··23680 SAS NUMBER:
**
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NUMBER, KA54
BY, D RUMFORD
ST, NC
1455 STOP, 00/00/00
08/11/95
***
**
**
**
** ••
*** * * * * * * * * * * * * * * * * * * * * * * * .• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
o.osu ALPHA-BHC a.sou METHOXYCHLOR o.osu BETA-BHC O.lOU ENDRIN KETONE o.osu DELTA-BHC O.lOU ENDRIN ALDEHYDE o.osu GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 .o.osu HEPTACHLOR o.osu GAMMA-CHLORDANE /2 o.osu ALDRIN o.osu ALPHA-CHLORDANE /2 o.osu HEPTACHLOR EPOXIDE 5.0U TOXAPHENE o.osu ENDOSULFAN I (ALPHA) l.OUR PCB-1016 (AROCLOR 1016)
O.lOU DIELDRIN 2.0U PCB-1221 (AROCLOR 1221)
O.lOUJ 4,4' -ODE (P,P'-DDE) l.OU PCB-1232 (AROCLOR 1232)
O.lOU ENDRIN l.OU PCB-1242 (AROCLOR 1242)
O.lOU ENDOSULFAN II (BETA) l.OU PCB-1248 (AROCLOR 1248)
O.lOU 4, 4' -ODD (P,P' -DOD) l.OU PCB-1254 (AROCLOR 1254)
O.lOU ENDOSULFAN SULFATE l.OU PCB-1260 (AROCLOR 1260)
O.lOU 4,4'-DDT (P,P'-DDT)
***REMARKS*** ***REMARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS.THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
--l!!!!I!!! !!!!II !!!II == aa liiiiiii iiiii liiii --- -- - - --
-liiii lilllll
PESTICIDES/PCB'S DATA REPORT
11111,AMil!BllND -YSI-.AG ..... s,11111
EPA-REGION IV ESD, ATHENS, GA. - - -- - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * •.• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95515 SOURCE, WEYERHAEUSER CO.
STATION ID, 005-SD
CASE NUMBER, 23680 SAS NUMBER,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NUMBER, KA53
BY, D RUMFORD
ST, NC
1445 STOP, 00/00/00
**
** •• •• ** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ••• UG/KG ANALYTICAL RESULTS UG/KG ANALYTICAL RESULTS
2.6U ALPHA-BHC 21JN METHOXYCHLOR 2 .6U BETA-BHC 5.1U ENDRIN KETONE 2.6U DELTA-BHC 5.1U ENDRIN ALDEHYDE 2.6U GAMMA-BHC (LINDANE) CHLORDANE (TECH. MIXTURE) /1 2.6U HEPTACHLOR 2.6U GAMMA-CHLORDANE /2 2 .6U ALDRIN 2.6U ALPHA-CHLORDANE /2 2.6U HEPTACHLOR EPOXIDE 260U TOXAPHENE 2.6U ENDOSULFAN I (ALPHA) 51U PCB-1016 (AROCLOR 1016) 5 .1U DIELDRIN 100U PCB-1221 (AROCLOR 1221) 5.1U 4,4' -DOE (P, P' -ODE) 51U PCB-1232 (AROCLOR 1232) 5.1U ENDRIN 51U PCB-1242 (AROCLOR 1242) 5.1U ENDOSULFAN II (BETA) 51U PCB-1248 (AROCLOR 1248) 5.1U 4,4' -DOD (P,P'-DDD) 51U PCB-1254 (AROCLOR 1254) 5.1U ENDOSULFAN SULFATE 51U PCB-1260 (AROCLOR 1260) 5.1U 4,4'-DDT (P, P' -DDT) 35 PERCENT MOISTURE
***REMARKS*** ***REMARKS***
***FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ,a
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
*C-CONFIRMED BY GCMS 1. WHEN NO VALUE IS REPORTED, SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
C •
ORGANIC DATA QUALIFIER REPORT
Gase Number 23680 Project Number 95-0295 SAS Number
Site ID. Weyerhaeuser Go., Plymouth, NG
Affected Samples
Volatiles
95523,95526,
95533
95528
Extractables
95526
95529
95531
95533
Pesticides
all waters
95515
Compound or Fraction
2-butanone
carbon disulfide
4-methylphenol
phenanthrene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b/k)fluoranthene
benzo (a)pyrene
pyrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
4,4' -DOE
aroclor-1016
methoxychlor
J
J
J
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J
J
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J
R
J
N
Flag
Used Reason
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitat:ion limit
< quantitation limit
low blind spike recovery
unacceptable blind spike recovery
< quantitation limit
difference in column
quantitations
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
*.**MEMORANDUM******
.DATE: 08/12/95
I
Results of Pesticide/PCB Analysis;
95-0295 WEYERHAEUSER CO.
PLYMOUTH NC
CASE NO: 23680
arles~~r .
ief, Laboratory Evaluation/Quality Assurance Section
I TO: PAT DEROSA
Attached are the results of analysis of samples collected as part of
ti subject project.
As a result of the Quality Assurance Review, certain data qualifiers ml have been placed on the data. Attached is a DATA QUALIFIER
R ORT which explains the reasons that these qualifiers were required.
I
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have any questions please contact me.
ATTACHMENT
SAMPLF-.AHO ANALYSIS MANAGEMENT SYSTEM
EPJ:.,-REGION IV ESD, ATHENS, GA. 08/ll/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 007-SW
CASE.NO., 23680
SAMPLE NO. 95530 co.
SAS NO.,
SAMPLE TYPE, SURFACEWA **
**
**
** **
*** * * * * * * * * * * * * * * * * * * * * * * *
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
4JN PHENOXYETHANOL
2JN BUTOXYETHANOL
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH COLLECTION START, 06/20/95
D. NO., KA67
* * * * * * * * * * * * *
BY, D RUMFORD
ST, NC
1415 STOP, 00/00/00
MD NO, KA67
* * * * * * * * * * * * * * * *
**
**
**
**
**
***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-l!!!!!I liii liiiil - - -------
--l!!!!i!!!I 1!!111,AM~D -YsI..aiAG~ SY-
EPA-REGION IV ESD, ATHENS, GA. - --- - - -
08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95531 SOURCE, WEYERHAEUSER CO.
STATION ID, 007-SD
CASE.NO., 23680 SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 D. NO., KA68
BY, D RUMFORD ST, NC
1430 STOP, 00/00/00
MD NO, KA68
•• •• •• •• •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * ***
lOOOJ
***FOOTNOTES***
ANALYTICAL RESULTS UG/KG
1 UNIDENTIFIED COMPOUND
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA. 08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
**
**
**
**
**
PROJECT NO. 95-0295 SOURCE, WEYERHAEUSER
STATION ID, 008-SD
CASE.NO., 23680
SAMPLE NO. 95528 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA65
BY, D RUMFORD ST, NC 1330 STOP, 00/00/00
MD NO, KA65
**
**
** **
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
***FOOTNOTES***
300JN
200JN
3000J
ANALYTICAL RESULTS UG/KG
DODECANOIC ACID
HEXADECANOIC ACID
2 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J.-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN .
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-l!!!!!!!I liiii iiii - - -- - --.. -
-iiiiil == !!l!!!!!IAMPl!lil!l,D ~SIS-AGE-SY~ EPA-REGION IV ESD, ATHENS, GA.
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT -·--- - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 108-SD
CASE.NO., 23680
SAMPLE NO. 95529 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA66
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00. MD NO, KA66
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * ***
***FOOTNOTES***
200JN
3000J
ANALYTICAL RESULTS UG/KG
HEXADECANOIC ACID
2 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*IT-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT ••• •• •• •• •• ••
• • • • • • • • • • • PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 004-SD
CASE.NO., 23680
• • • • • •
SAMPLE NO. co.
SAS NO.,
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• * * * * *** 95526 SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA63
BY, D RUMFORD
ST, NC
1200 STOP, 00/00/00
MD NO, KA63
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •• ***
***FOOTNOTES***
l000JN
800JN
500JN
500JN 20000J
ANALYTICAL RESULTS UG/KG
BENZENEACETIC ACID
HYDROXYBENZENEACETIC ACID
HEXADECANOIC ACID
HEXAHYDROXYTRIMETHYL(METHYLETHYL)PHENANTHRENONE
7 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES .*J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
1!111 1111111 == ;a; iiiii ----- - ---
&iiil 11!!11!!1 · -AM~D alilYsIJlillliAGia!il' s~ -- -----EPA-REGION IV ESD, ATHENS, GA. 08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION to, 008-SW
CASE.NO., 23680
SAMPLE NO. 95527 co.
SAS NO.,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95 D. NO., KA64
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00 MD NO, KA64
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * ***
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
3JN PHENOXYETHANOL
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL.
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT:: RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA ••• • • • • • • • • • • • • • • • • • • • • •• PROJECT NO . 95-0295 SAMPLE NO. 95523 •• SOURCE, WEYERHAEUSER co. •• STATION ID, 003-SD •• CASE.NO., 23680 SAS NO.,
**
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM tPA-REGION IV ESD, ATHENS, GA.
REPORT • • • • • • • • • • • • • • • • • • • • •
SAMPLE TYPE, SOIL PROG ELEM, NSF
CITY, PLYMOUTH
•
COLLECTION START,
D. NO., KA60
• • • • • • • • • • •
COLLECTED BY, D RUMFORD ST, NC
06/20/95 1115 STOP,
MD NO, KA60
• • • • •
00/00/00
• •
08/11/95
• • • •• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * ***
***FOOTNOTES***
300JN
10000J
ANALYTICAL RESULTS UG/KG
HEXADECANOIC ACID
5 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-liiiiil iiil -- - - ----- -
-.. 1!!11!!!1 -..,AM~D -YSI.-sAG~' SY-
EPA-REGION IV ESD, ATHENS, GA. -----08/11/95 -
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** **
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 003-SW CASE.NO., 23680
SAMPLE NO. 95524 co.
SAS NO.,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA61
BY, D RUMFORD ST, NC
1110 STOP, 00/00/00 MD NO, KA61 .
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * .• * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
3JN PHENOXYETHANOL
2JN HEXADECANOIC ACID
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA . •
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *
•• PROJECT NO. 95-0295 SAMPLE NO. 95519 SAMPLE TYPE: SURFACEWA
** SOURCE: WEYERHAEUSER CO. ** STATION ID: 006-SW ** CASE.NO.:_ 23680 SAS NO.: ••
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH COLLECTION START: 06/19/95
D. NO.: KA57
BY: D RUMFORD
ST: NC
1640 STOP: 00/00/00 MD NO: KA57 .
08/11/95
••• ••• •• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
ANALYTICAL RESULTS UG/L
3JN HEXADECANOIC ACID
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. . *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
l!!!!!I lillii liii ---- - -------
lilllil --aAM~D -YSI"-!liAG~ SY--EPA-REGION IV ESD, ATHENS, GA. --- - - -
08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * *** **
**
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER STATION ID, 006-SD
CASE.NO., 23680
SAMPLE NO. 95520 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KAASB
BY, D RUMFORD
ST, NC
1650 STOP, 00/00/00
MD NO, KASS
**
**
** **
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •••
***FOOTNOTES***
700JN
200JN
20000J
ANALYTICAL RESULTS UG/KG
HEXAHYDROHYDROXYTRIMETHYL(METHYLETHYL)
PHENANTHRENONE
OCTAHYDROTRIMETHYL(METHYLETHYL)PHENANTHRENE 11 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAT-INTERFERENCES *J-ESTIMATED VALUE .*N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL *K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * - * * * * * * * * * * * * * * * * * *** **
**
** **
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 005-SW
CASE .NO. , 23680
SAMPLE NO. 95516 co.
SAS NO.,
SAMPLE TYPE, SURFACEWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH COLLECTION START, 06/19/95
D. NO., KA54
BY, D RUMFORD
ST, NC
1455 STOP, DD/DD/DD MD NO, KA54 .
**
** **
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * ***
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
4JN HEXADECANOIC ACID
2JN DIHYDROXYDIMETHYLBENZOIC ACID
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-== liiiiJ - -- - --- ---.. --
lliiil == ..asAM-.Um -YSI_,AG_, S,... EPA-REGION IV ESD, ATHENS, GA. - -- -
-08""95 --
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** •• **
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 001-DW
CASE.NO., 23680
SAMPLE NO. 95517 co.
SAS NO.,
SAMPLE TYPE, GROUNDWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KASS
BY, D RUMFORD ST, NC
1605 STOP, 00/00/00
MD NO, KASS
••
** •• **
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
***FOOTNOTES***
ANALYTICAL RESULTS UG/L
2JN PHENOXYETHANOL
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE. PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM·
EPA-REGION IV ESD, ATHENS, GA. 08/ll/95
EXTRACTABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * •. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95534
SOURCE, WEYERHAEUSER CO.
STATION ID, 002-DW
SAMPLE TYPE, DRKWA PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
BY, D RUMFORD
ST, NC
1515 STOP, 00/00/00
•• •• • • ••
** CASE NO.: 23680 SAS NO.: D. NO.: KA71 **
*** * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
25U
lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3,DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE 2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U
25U lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT .
. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
11!!!!!1 !!!!I == lliiil iiii liii liiil liii liiiliil -- -- -
lliil llil!l!IAMPl!lil!LD l!BtsH-AG~ SY-
EPA-REGION IV ESD, ·ATHENS, GA. -- -----08/11/95
MISCELLANEOUS EXTRACTABLE COMPOUNDS -DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * *** •• •• •• •• ••
PROJECT NO. 95-0295 SOURCE, WEYERHAEUSER STATION ID, 005-SD
CASE.NO., 23680
SAMPLE NO. 95515 co.
SAS NO.,
SAMPLE TYPE, SOIL PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH COLLECTION START, 06/19/95
D. NO., KA53
BY, D RUMFORD
ST, NC 1445 STOP, 00/00/00
MD NO, KA53
•• •• •• •• • •
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * ***
60000J
***FOOTNOTES***
ANALYTICAL.RESULTS UG/KG
20 UNIDENTIFIED COMPOUNDS
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT.BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH **
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95532
SOURCE, WEYERHAEUSER CO.
STATION ID, 107-SW
** CASE NO.: 23680
SAMPLE TYPE, SURFACEWA
SAS NO.,
COLLECTION START, 06/20/95
D. NO., KA69
BY, D RUMFORD
ST, NC
1415 STO~, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
25U
lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE 2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U 25U
lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-*R"QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
liiii.iil liiiiiii liiiiiii iiiiiii -iiiii .. -- ---
i;;;;i ll!l!!tAM~D IJltsIJ!:11,AGiR SY------- --EPA-REGION IV ESD, ATHENS, GA. 08/11/95
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95533
SOURCE, WEYERHAEUSER CO .
STATION ID, 107-SD
** CASE NO.: 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA70
BY, D RUMFORD
ST, NC
1430 STOP, 00/00/00
•• •• •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
750U
750U
750U
750U
750U
750U 750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U
750U 750U
750U
750U
1900U
750U
1900U
750U
750U
750U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE 2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4 -CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE 2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
1900U
750U
1900U
1900U
750U
750U
750U
750U
7500
19000
1900U
750U
750U
750U
1900U
750U
750U
750U
750U
750U
160J
750U ·
750U
750U
750U
750U
750U
750U
99J
750U
750U
140J
56
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE 2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R"QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * •• PROJECT NO. 95-0295 SAMPLE NO. 95530
•• SOURCE, WEYERHAEUSER CO.
** STATION ID: 007-SW ••
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. REPRINTED ON 08/21/95
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ••• •• •• •• •• ••
SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA67
BY, D RUMFORD
ST, NC
1415 STOP, 00/00/00
** CASE NO.: 23680 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/L
100
100
100 100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
250
100
250 100
100
100
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4°DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISO PHO RONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE 2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
250
100
250
250
100
100
100
100
100
250
250
100
100
100
250
100
100
100
100
100
100
100
100·
100
100
100
100
100
100 100
100 100
ANALYTICAL RESULTS
3-NITROANILINE ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE CHRYSENE .
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•o-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
l!!!I !!!!I 1!111 == == 1111111.1 -iiiil iiiil iiiil liiiil -- -
liiiill 111111\AM~D ~sIM!l,AGE-SY-----EPA-REGION IV ESD, ATHENS, GA. 08/11/95
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** **
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95531
SOURCE, WEYERHAEUSER CO.
STATION ID, 007-SD
** CASE NO.: 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM: NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO.: KA68
BY, D RUMFORD
ST, NC
1430 STOP: 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * *** UG/KG
770U
770U
770U
770U
770U
770U 770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U
770U 770U
19000
770U
19000
770U
770U
770U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
1900U 770U
1900U 19000
770U
770U
770U
770U
770U
19000
1900U
770U
770U
770U
19000
770U
770U
770U 770U
770U
96J 770U ·
770U
770U 770U
770U
770U
770U
770U
770U
770U
770U
57
ANALYTICAL RESULTS
3-NITROANILINE ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. ~RCQC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
EXTRACTABLE ORGANICS DATA
*** * * * * * * * * * * * ** PROJECT NO. 95-0295 ** SOURCE: WEYERHAEUSER ** STATION ID: 008-SD
REPORT * * * * * * * * * SAMPLE NO. 95528 co.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
* * * * * * * * * * • • • SAMPLE TYPE: SOIL
* * * * * * * * * * * * * PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
* * * * * * * * * * * * * BY: D RUMFORD
ST: NC
1330 STOP: 00/00/00
08/11/95
• • • ••• •• •• •• •• •• ** CASE NO.: 23680 SAS NO.: D. NO.: KA65 **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * ***
UG/KG
610U 610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
1500U
610U
1500U
610U
610U
610U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL l,3cDICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL 2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
UG/KG
1500U
610U
1500U
1500U
610U
610U
610U
610U
610U
1500U
1500U
610U
610U
610U
1500U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
610U
46
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE .
***REMARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT. *R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
!1!!11 1!1111 cm liiiiii liiiii Iii& iiiil ilii iiiil ----- -
liliil lll!lsAM~D -Ysil!!!!IINAGall:-s,,... ------EPA-REGION IV ESD, ATHENS, GA. 08/11/95 EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * ·* * * ·* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95529
SOURCE, WEYERHAEUSER CO.
STATION ID, 108-SD
** CASE NO.: 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA66
BY, D RUMFORD
ST, NC
1330 STOP, 00/00/00
•• • • •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
600U
15000
600U 15000
600U 600U
600U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL 1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE 2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
15000
600U
15000
15000
600U
600U
600U
600U
600U
15000
15000
600U
600U
600U
15000
83J
600U
600U
600U
130J
380J
600U ·
600U
BOJ
130J
600U 600U
140J
90J
600U
600U
600U
45
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO "(1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
**.*REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
· *U~MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 95526
** SOURCE: WEYERHAEUSER CO.
** STATION ID: 004-SD
** ** CASE NO.: 23680
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * SAMPLE TYPE: SOIL
SAS NO.:
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/20/95
D. NO.: KA63
BY: D RUMFORD
ST: NC
1200 STOP: 00/00/00
08/11/95
• * * *** **
** **
** ** *** * *· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
970U
970U
970U
970U
970U
970U
970U
970U
340J
970U
970U
970U
970U
970U 970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
2400U
970U
2400U
970U
970U
970U
ANALYTICAL RESULTS
PHENOL BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
l,3cDICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISO PHO RONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REM.ARKS***
***FOOTNOTES***
UG/KG
2400U
970U
2400U
2400U
970U
970U
970U
970U
970U
2400U
2400U
970U
970U
970U
2400U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
970U
66
ANALYTICAL RESULTS
3-NITROANILINE ACENAPHTHENE
2,4-DINITROPHENOL 4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE BENZO ( GHI) PERYLENE .
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
· *U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
,•RCQC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
iiiii iiil - - -
---- -
-------- --
----SAM~D -YSI!Jlllli!laiAGllfr s.,. -- - - - - -
EPA-REGION IV ESD, ATHENS, GA. EXTRACTABLE ORGANICS DATA REPORT 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• ** ••
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 008-SW
** CASE NO.: 23680
SAMPLE NO. 95527 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA64
BY, D RUMFORD
ST, NC
1330 STOP, , 00/00/00
•• •• •• •• ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * *. * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
100
100
100
100
100
lOU
lOU
100
100 lOU
100
100
lOU
100 lOU lOU
100
100
25U
100
250
lOU
100
100
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4 -CHLOROANILINE
HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
OG/L
250
100
250 250
lOU
lOU
100
100
100
250
250
100
lOU
lOU
250
100
lOU
100
lOU 100 . 100
lOU ·
100
100
100
lOU
lOU
100
100
100
100
100
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL 4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLOENE
DIETHYL PHTHALATE
4-CHl,OROPHENYL PHENYL ETHER
FLOORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE FLUORANTHENE
PYRENE BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE.VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES. *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTOAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTOAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
· *0-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QOANTITATION LIMIT.
*R"QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95524
SOURCE, WEYERHAEUSER CO.
STATION ID, 003-SW
** CASE NO.: 23680
SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMO!ITH
COLLECTION START, 06/20/95
D.NO.,KA61
BY, D RUMFORD
ST, NC
1110 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *·* * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
25U
lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4'DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROB!ITADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U
25U
lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU
lOU
lOU.
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
ANALYTICAL RESULTS
3-NITROANILINE ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BlITYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BlITYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES .*J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
·•U-MATERIAL WAS ANALYZED FOR BlIT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-*R"QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--- --- - - ------ - - --
---- --EXTRACTABLE ORGANICS DATA REPORT
-SAM-,,.,,D -ysilllllr,AGallr s~ -EPA-REGION IV ESD, ATHENS, GA. - - - - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * *** ••
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 004-SW
** CASE NO.: 23680
SAMPLE NO. 95525 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA62
BY, D RUMFORD
ST, NC
1150 STOP, 00/00/00
**
**
**
**
** *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
lOU
lOU
25U
lOU
25U lOU lOU
lOU
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U
25U
lOU
lOU
lOU
lOU
lOU
2SU
2SU
lOU
lOU
lOU
25U
lOU lOU
lOU
lOU
lOU
lOU
lOU ·
lOU
lOU
lOU
lOU lOU
lOU lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
Dl-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE rs KNOWN TO BE GREATER THAN VALUE GIVEN
· *UcMATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • • • * * * * * * * * * * * * * * * * * * * * * * * * * * •• PROJECT NO. 95-0295 SAMPLE NO. 95520 SAMPLE TYPE, SOIL
** SOURCE, WEYERHAEUSER CO.
** STATION ID: 006-SD ..
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
BY, D RUMFORD
ST, NC
1650 STOP, 00/00/00
06/11/95
••• ••• •• •• •• .. •• •• CASE NO.: 23680 SAS NO.: D. NO.: KAASB
-·· * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *'* * * * * * * * •••
UG/KG
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
1400U
540U
1400U
540U
540U
540U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
1400U
540U 1400U
1400U
540U
540U
540U
540U
540U
1400U
1400U
540U
540U
540U
1400U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
540U
39
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE rs KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ·•u-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R~QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION.
---- - -- - --- - -- - - - ---
--- ---- - - - -EXTRACTABLE ORGANICS DATA REPORT 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95523
SOURCE, WEYERHAEUSER CO .
STATION ID, 003-SD
** CASE NO.: 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/20/95
D. NO., KA60
BY, D RUMFORD
ST, NC
1115 STOP, 00/00/00
•• •• •• • • ••
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
?DOU
700U
700U
700U
?DOU
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
700U
1800U
700U
1800U
700U
700U
700U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3°DICHLOROBENZENE 1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
1800U
700U
1800U
1800U
700U
700U
700U
700U
700U
lB00U
lB00U
700U
700U
700U
lB00U
700U
700U
700U
700U 700U
700U
700U
700U
700U
700U 700U
700U
700U
700U
700U
700U
700U
53
ANALYTICAL RESULTS
"3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
· *UcMATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA.
EXTRACTABLE ORGANICS DATA REPORT
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * ** PROJECT NO. 95-0295 SAMPLE NO. 9551B SAMPLE TYPE: GROUNDWA
** SOURCE: WEYERHAEUSER CO. ** STATION ID: 101-DW ••
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH COLLECTION START: 06/19/95
BY: D RUMFORD
ST: NC 1605 STOP: 00/00/00
08/11/95
• • • ••• •• •• **
**
** CASE NO.: 23680 SAS NO.: D. NO.: K.AS6 **
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * •. * * ***
UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
25U lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U
25U
lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU lOU lOU.
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE PYRENE
BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ·•u7MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
--- --- ------- --- ---
-- - - --- - - - -EXTRACTABLE ORGANICS DATA REPORT 08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * *** •• •• •• ••
PROJECT NO. 95-0295 SAMPLE NO. 95519
SOURCE, WEYERHAEUSER CO .
STATION ID, 006-SW
** CASE NO.: 23680
SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA57
BY, D RUMFORD
ST, NC
1640 STOP, 00/00/00
•• •• •• • • ••
**.* * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * .• * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU ·25u
lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL
l,3°DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISO PH ORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
25U
lOU
25U
25U
lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
·•u-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD, ATHENS, GA. 08/11/95
EXTRACTABLE ORGANICS DATA REPORT *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
PROJECT NO. 95-0295
SOURCE, WEYERHAEUSER
STATION ID, 005-SW
SAMPLE NO. 95516 co. SAMPLE TYPE, SURFACEWA
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA54
BY, D RUMFORD
ST, NC
1455 STOP, 00/00/00
**
**
** **
** ** CASE NO.: 23680 *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * ***
UG/L
lOU
lOU lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
25U
lOU
25U
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4:DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
UG/L
25U
lOU
25U
25U lOU
lOU
lOU
lOU
lOU
25U
25U
lOU
lOU
lOU
25U
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE 4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
***FOOTNOTES*** *A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
·•u-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•*R:Qc INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS rs NECESSARY FOR VERIFICATION.
---- --- -- ------ - - - -
--- --EXTRACTABLE ORGANICS DATA REPORT --SAM~D-,YsrlllLAG-r s~ -EPA-REGION IV ESD, ATHENS, GA. - -- - - -
08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
** ••
PROJECT NO. 95-0295
SOURCE: WEYERHAEUSER
STATION ID: 001-DW
** CASE NO.: 23680
SAMPLE NO. 95517 co. SAMPLE TYPE: GROUNDWA
SAS NO.:
PROG ELEM: NSF COLLECTED
CITY: PLYMOUTH
COLLECTION START: 06/19/95
D. NO.: KASS
BY: D RUMFORD
ST: NC
1605 STOP: 00/00/00
•• •• ••
** •• *** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/L
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
25U
lOU
2SU
lOU
lOU
lOU
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
l,3,DICHLOROBENZENE
1,4-DICHLOROBENZENE
l,2-DICHLOROBENZENE
2-METHYLPHENOL
2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
l,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/L
2SU
lOU
2SU
2SU
lOU
lOU
lOU
lOU
lOU
2SU
2SU
lOU
lOU
lOU
2SU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
lOU
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
·•ucMATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
·•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
ORGANIC DATA QUALIFIER REPORT
Case Number 23680 Project Number 95-0295 SAS Number
Site ID. Weyerhaeuser Co., Plymouth, NC
Affected Samples
Volatiles
95523,95526,
95533
95528
Extractables
95526
95529
95531
95533
Pesticides
all waters
95515
Compound or Fraction
2-butanone
carbon disulfide
4-methylphenol
phenanthrene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b/k)fluotanthene
benzo(a)pyrene
pyrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
4,4'-DDE
aroclor-1016
methoxychlor
Flag
· Used
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
R
J
N
Reason
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitat:ion limit
< quantitation limit
low blind spike recovery
unacceptable blind spike recovery
< quantitation limit
difference in column
quantitations
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
------EXTRACTABLE ORGANICS DATA REPORT
-SAl'-AND-.YS:ila.NA.Gll-fr S-·1 E~A-REGION IV ESD, ATHENS, GA. -----08/11/95
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** **
**
**
**
PROJECT NO. 95-0295 SAMPLE NO. 95515
SOURCE, WEYERHAEUSER CO.
STATION ID, 005-SD
** CASE NO.: 23680
SAMPLE TYPE, SOIL
SAS NO.,
PROG ELEM, NSF COLLECTED
CITY, PLYMOUTH
COLLECTION START, 06/19/95
D. NO., KA53
BY, D RUMFORD
ST, NC
1445 STOP, 00/00/00
**
**
**
**
**
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * *** UG/KG
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
· 520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
520U
1300U
520U
1300U
520U
520U
520U
ANALYTICAL RESULTS
PHENOL
BIS(2-CHLOROETHYL) ETHER
.2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL 2,2'-CHLOROISOPROPYLETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
***REMARKS***
***FOOTNOTES***
UG/KG
1300U
520U
1300U
1300U
520U
520U
520U
520U
520U
1300U
1300U
520U
520U 520U
1300U
520U
520U
520U
520U
520U
520U
520U 520U
520U
520U
520U
520U
520U
520U
520U 520U
520U
36
ANALYTICAL RESULTS
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHI)PERYLENE
PERCENT MOISTURE
***REMARKS***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.