NCD981927502_20020205_Geigy Chemical Corporation_FRBCERCLA RA_October 2001 Sampling Event Downgradient Area Monitoring Report-OCR

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
r',
\; 0,1\(ll~
. --:\
l J)1u~ ,,, '. ::! '1\
: . I ' i I ! , FEB -7 2002 ' ;:J
l I l
OCTOBER 2001 SAMPLING EVE~T . ,JN
DOWNGRADIENT AREA MONITORING REPORT
Geigy Chemical Corporation
CERCLA Site
Aberdeen, North Carolina
FEBRUARY 2002
• THE PINNACLE CONSULTING GROUP • ~!!!!. . .__ _________________________ _ • • • t ..
Providing Decision Support Through Knowledge and Technology
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Geigy Chemical Corporation Site
Aberdeen, North Carolina
Committee Correspondence
February 5, 2002
Ms. Giezelle Bennett
Remedial Project Manager
USEPA Region IV, North Superfund Remedial Branch
I Ith Floor
61 Forsyth Street, SW
Atlanta, GA 30303-3104
RE: October 200 I Sampling Event
Downgradient Area Monitoring Report
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Giezelle:
YJA QYEBNJGHI DEJ.IYEBY
In accordance with the Downgradient Groundwater Remedial Action Work Plan (RA WP), please
find attached one copy of the analytical results for the October 200 I sampling of the Geigy
Downgradient Area. To facilitate your review, analytical data summary tables and figures showing
. detected concentrations at sample locations are attached .
Samples for the monitoring event were collected October 9, 2001 through October 12, 2001.
However, analytical results for one sample, MW-38L, indicated detections of compounds never
previously detected in that well as well as the absence of the one pesticide typically detected in that
well. This well was resampled on January 10, 2002. Those results were consistent with historical
concentrations in that well and results from the resampling event are presented in this report .
Monitoring well MW-I ID was not sampled during this event because the well was dry. Findings
of the monitoring results (Tables I and 2) include:
Upper Black Creek Aquifer
• Pesticide concentrations in monitoring wells located west of the groundwater extraction
system (i.e., in the downgradient area) remain comparable to levels found during previous
monitoring events and the initial downgradient area groundwater-sampling event (August
1995) .
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • C
extraction system are below the maximum BHC isomer concentrations forecasted for the Upper
Black Creek aquifer by the transport model (see Table 3) .
I rnver Black Creek Aqwfer
• The extent of pesticides in the Lower Black Creek aquifer is similar to conditions reflected by
previous quarterly monitoring events and the baseline sampling event (June 1996 for wells
PZ-5, MW-31L and MW-32L; August 1995 for all other wells) .
• Pesticides were not detected in sentinel wells MW-32L and MW-39L, which adjoin
Aberdeen and Ray's Mill Creeks, respectively. Dieldrin was the only constituent detected in
sentinel well MW-38L, located adjacent to Aberdeen Creek, at an estimated concentration of
0.033 ug/L. The detection of dieldrin in MW-38L is not considered Site-related .
• Pesticides were not detected in well MW-36L, which serves as a sentinel monitoring point
for Town Well No. 2 .
• Routine monitoring conducted by the Town of Aberdeen continues to demonstrate that Town
Well No. 2 meets Federal and State drinking water standards .
• BHC levels in the Lower Black Creek aquifer are near or below the maximum concentrations
forecasted by the transport model (see Table 4 ) .
\tream Surface Water
• Analytical results for sentinel wells MW-32L, MW-38L and MW-39L, which monitor the
Lower Black Creek aquifer prior to its discharge to surface water, demonstrate that pesticides
in downgradient area groundwater do not extend to Aberdeen and Ray's Mill Creeks .
• Alpha, beta-, delta-and gamma-BHC were detected at McFarland's Branch surface water
locations SW-02 and SW-03. Concentrations of BHC isomers detected at SW-02 and SW-03
are less than previous monitoring levels. Results of all isomers are within the range of
surface water concentrations estimated for these locations by the transport model (Table 3-10
of the RA WP) and are at levels that are protective of potential human and ecological
receptors .
• Estimated concentrations of alpha-, beta-and delta-BHC were detected in surface water
samples SW-04, SW-05, SW-06, SW-07, SW-08 and SW-11-2 from Aberdeen Creek .
Gamma-BHC, heptachlor and heptachlor epoxide were not detected in the surface water
samples collected from Aberdeen Creek. The concentrations are comparable to historical
monitoring results and are at levels that are protective of potential human and ecological
receptors .
• The highest concentrations of pesticides in Aberdeen Creek were detected in an area that lies
outside of the downgradient extent of Site-related pesticides (i.e., surface water sample SW-
08. located upstream of the confluence with Ray's Mill Creek). This finding indicates the
source of pesticides detected in Aberdeen Creek is not Site-related .
• Pesticide concentrations are similar among surface water samples collected from Aberdeen
Creek at locations downstream and upstream of the confluence with McFarland's Branch,
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • C
thereby indicating that the estimated levels of pesticides in Aberdeen Creek are not
attributable to Site conditions .
• Surface water and groundwater analytical results collectively reveal that the pesticides
detected in Aberdeen Creek are not Site-related .
• Pesticides were not detected in surface water samples collected from Ray's Mill Creek .
Pn"vore Well S111Yey
• A survey to identify newly installed residential water supply wells was performed as part of the
quarterly monitoring event by driving each road in the downgradient area and conducting a
visual inspection of the properties to locate pump houses and/or well heads. No newly installed
private wells were identified .
In accordance with the sampling frequency described in the approved RA WP, monitoring of the
downgradient area will be conducted every six months during years four and five of the remedy .
The next monitoring event will be conducted during April 2002 .
Olin Corporation has recently appointed a new Project Coordinator, Ray Hom, for the Geigy
Chemical Corporation CERCLA Site. Mr. Hom can be reached at [phone]. Further
correspondence should be directed to Mr. Hom at the following address:
Olin Corporation
1186 Lower River Road, NW
Charleston, TN 37310
Regards,
~c//41/ /JJMS
Ray Hom
Project Coordinator
/Enclosure
c: R. McElveen (NCDENR)
T. Eggert (CDM)
H. Moats (Syngenta)
H. Grubbs, Esq. (WCS&R)
B. Vinzant (Kaiser)
M. Sheehan (Pinnacle)
a
t
t • • t • t , , • • • • 8 • • • • I • • • • • • • I)
0 • • • •• • ()
0
() • • • • • • • • • • • e • • • • ,f
II)
SUMMARY TABLES AND FIGURES
OCTOBER 2001
DOWNGRADIENT AREA
•••••••••••••••••••••••••••••••••••••••••••••••••••••••
UPPER BLACK CREEK AQUIFER
Sample ID: MW-18D
Date Collected: 10110/2001
Performance
Pesticides (ug/L) Standard tu-"
Aldrin 0.05 < 0.05 //
alpha-BHC ' 0.05 f :\0,~4~) // .:.;t,.y•.;,"; ,·, .. beta-BHC 0.05 ,,.,,~0.71// (itio:1.1 II delta-BHC 0.05 ·~-_, . , ... ~
gamma-BHC (Lindane) 0.2 .. ,. -,:0•4111 r·~ -,, .
alpha-Chlordane --< 0.05 //
gamma-Chlordane --< 0.05 II
4,4'-DDD --< 0.1 II
4,4'-DDE --< 0.1 II
4,4'-DDT --< 0.1 II
Dieldrin 0.1 0.058 JI/
Endosulfan I --< 0.05 II
Endosulfan II --< 0.1 II
Endosulfan sulfate --< · .0.1 II
Endrin --< 0.1 II
Endrin aldehyde --< 0.1 II
Endrin ketone 0.1 0.072 JI!
Heptachlor --< 0.05 II
Heptachlor epoxide --< 0.05 II
Methoxychlor --< 0.5 II
Toxaohene I < 2 II
Notes:
Detects shown in bold type.
TABLE 1
OCTOBER2001
GROUNDWATER MONITORING
DOWNGRADIENT AREA
,MW-20D MW-22D MW-23D
101912001 10110/2001 1011112001
< 0.05 II < 0.05 II < 0.05 II
~II l•~'~j" ll¥;it,~,~~~"
,J:~o:ill II fli!eo:13)// r.Jo'.4~11 'I"' -~J,;,• ·.lo+ i"cr ~ ·.•
~19,}311 ,,;'.05811/ 0.037 JI/
~0;45 II '.j,,, .•. ··1
i:,;J_Q.;37, II 0.14 //
< 0.05 II < 0.05 II < 0.05 II
< 0.05 II < 0.05 II < 0.05 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.05 II < 0.05 II < 0.05 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.1 II < 0.1 II < 0.1 II
< 0.05 II < 0.05 II < 0.05 II
< 0.05 II < 0.05 II < 0.05 II
< 0.5 II < 0.5 II < 0.5 II
< 2 II < 211 < 2 II
Values exceeding downgradient groundwater performance standards indicated by shading.
I -Separates qualifiers added by the laboratory and qualifiers added as a result of validation.
J-Estimated value.
MW-26D MW-30D MW-35D
1011moo1 10112/2001 101912001
< 0.05 II < 0.25 II < 0.05 II
J.9.,1!,~~1" fF:;"0;41l11 f;;;:'t, oh2111
'-"~"'' ~ 1~~:n,-,, ... ,· .. :
~:,,0,082 II r'i\'), ; •/;~ I I /~(00l9.~j II 1£:--·~w ~,,,o:u 11 ;-·j\·-:o:36 II 0.022 JI/ ~· •• "J'
0.085 // .'··-~:o:2§ II 0.077 //
< 0.05 II < 0.25 II < 0.05 II
< 0.05 II < 0.25 II < 0.05 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II [ii:O~J/1 < 0.1 II
< 0.05 II < 0.25 II < 0.05 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II < 0.5 II < 0.1 II
< 0.1 II lf~0.4~ JI/ < 0. I II
< 0.05 II < 0.25 II < 0.05 II
< 0.05 II < 0.25 II < 0.05 II
< 0.5 II < 2.5 II < 0.5 II
< 211 < 10 // < 2 II
•••••••••••••••••••••••••••••••••••••••••••••••••••••••
LOWER BLACK CREEK AQUIFER
Sample ID:
Date Collected:
Performance
Pesticides (ug/L) Standard lu-"
Aldrin 0.05
alpha-BHC 0.05
beta-BHC 0.05
delta-BHC 0.05
gamma-BHC (Lindane; 0.2
alpha-Chlordane ..
gamma-Chlordane ..
4,4'-DDD ..
4.4'-DDE ..
4,4'-DDT ..
Dieldrin 0.1
Endosulfan I --
Endosulfan II --
Endosulfan sulfate --
Endrin --
Endrin aldehyde --
Endrin ketone 0.1
Heptachlor --
Heptachlor epoxide --
Methoxychlor --
Toxaohene 1
Notes:
Detects shown in bold type.
TABLE 1
OCTOBER 2001
GROUNDWATER MONITORING
DOWNGRADIENT AREA
MW-22L MW-2SL MW-27L
1011012001 1011112001 1011012001
< 0.5 II < 0.25 II < i 0.5 II
ti~" ~.:e:~~"171// k,'}",,,3·7 II ., r~:~4:-t ~--,,; ¥\:;!;,8 II t;'J0:351// $!ilc5 II r'.lffe'-···1 W"''r
fiH>2:~~ II ~.68// lf· 2A II
.:f~~::1~! 11 )1,11 ?',fy ,.-r...,~~ 2;3 II ,,....,, ____ J
< 0.5 II < 0.25 II < 0.5 II
< 0.5 II < 0.25 II < 0.5 II
< 1 // < 0.5 II < I II
< I II < 0.5'/I < I II
< I II < 0.5 II < 1 //
< 10 II < 0.5 II < I //
< 0.5 II < 0.25 II < 0.5 II
< I II < 0.5 II < I //
< 1 II < 0.5 II < 2.5 GIi
< I II < 0.5 II < I II
< 1 II < 0.5 II < 1 II
< 10 // < 0.5 II < 1 //
< 0.5 II < 0.25 II < 0.5 II
< 0.5 II < 0.25 II < 0.5 II
< 5 II < 2.5 II < 5 II
< 20 II < 10 // < 20 II
Values exceeding downgradient groundwater perfonnance standards indicated by shading.
I -Separates qualifiers added by the laboratory and qualifiers added as a result of validation.
J-Estimated value.
G-Surrogate recovery less than 10%
MW-31L MW-32L MW-36L
10112/2001 10112/2001 1011112001
I
< 0.25 II < 0.05 II < 0.05 II
,.;2·1r < 0.05 II <-0.05 II
:,/R·~~ II < 0.05 II < 0.05 II ~,?-~,,w1 < 0.05 II < 0.05 II
;,;.i,,1.2,// < 0.05 II < 0.05 II
< 0.25 II < 0.05 II < 0.05 II
< 0.25 II < 0.05 II < 0.05 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.25 II < 0.05 II < 0.05 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.25 II < 0.05 II < 0.05 II
< 0.25 II < 0.05 II < 0.05 II
< 2.5 II < 0.5 II < 0.5 II
< 10 // < 2 // < 2 II
•••••••••••••••••••••••••••••••••••••••••••••••••••••••
LOWER BLACK CREEK AQUIFER
TABLE 1
OCTOBER 2001
GROUNDWATER MONITORING
DOWNGRADIENT AREA
Sample ID: MW-37L MW-38L MW-39L MW-40L
Date Collected: 10/11/2001 111012002
Performance
Pesticides (ug/L) Standard (ui:l!,l
Aldrin 0.05 < 0.25 II < 0.05
alpha-BHC 0.05 ~5'/1 < 0.05 •.I
beta-BHC 0.05 ~,,~~J,111 0.05 <
delta-BHC 0.05 t ,;,,t~,9.~\ II < 0.05
gamma-BHC (Lindane) ffi' -0.2 .:il; II < 0.05
alpha-Chlordane --< 0.25 II < 0.05
gamma-Chlordane· --< 0.25 II < 0.05
4,4'-DDD --< 0.5 II < 0.1
4.4'-DDE --< 0.5 II < 0.1
4,4'-DDT --< 0.5 II < 0.1
Dieldrin 0.1 < 0.5 II 0.021 JI/
Endosulfan I --< 0.25 II < 0.05
Endosulfan II --< 0.5 II < 0.1
Endosulfan sulfate --< 0.5 II < 0.1
Endrin --< 0.5 II < 0.1
Endrin aldehyde --< 0.5 II < 0.1
Endrin ketone 0.1 < 0.5 II < 0.1
Heptachlor --< 0.25 II < 0.05
Heptachlor epoxide --< 0.25 II < 0.05
Methoxychlor --< 2.5 II < 0.5
Toxaohene I < lO // < 2.
Notes:
Detects shown in bold type.
Values exceeding downgradient groundwater perfonnance standards indicated by shading.
/ -Separates qualifiers added by the laboratory and qualifiers added as a result of validation.
J-Estimated value.
1011012001 10111/2001
< 0.05 II < 0.25 II
< 0.05 II _';•J?i f<_ 1~2 II It" ... 0.05 II _iff~~1_s II <
< 0.05 II .' •}ii0.76 II
< 0.05 II 0.18 JI/
< 0.05 II < 0.25 II
< 0.05 II < 0.25 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.05 II < 0.25 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.1 II < 0.5 II
< 0.05 II < 0.25 II
< 0.05 II < 0.25 II
< 0.5 II < 2.5 II
<. 2 II < 10 II
PZ-2 PZ-3 PZ-5
1019/2001 101912001 1011onoo1
< 0.25 II < 0.05 II < 0.05 II
,:\"0:62111 r'.1.o,49J!! r,·-:0'o~isl11
~\~o;i~J// L~f@J11 ',.ti, j ,;, ,:li~i~l.! II t-1't ·0~25 II ft,,Lo,11111 0.021 JII
•'%'!•' " -~ ts-~•lo/ ·;•, 1 1·.-,:-rv-.,,.-: L~;51; 11 ;:;,>!.9A1/I L, .. 0.26J//
< 0.25 II < 0.05 II < 0.05 II
< 0.25 II < 0.05 II < 0.05 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.25 II < 0.05 II < 0.05 .I/
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.5 II < 0.1 II < 0.1 II
< 0.25 II < 0.05 II < 0.05 II
< 0.25 II < 0.05 II < 0.05 II
< 2.5 II < 0.5 II < 0.5 II
< 10 II < 2 II < 2 II
•••••••••••••••••••••••••••••••••••••••••••••••••••••••
SURFACE WATER McFarland's Branch
Sampling Event 4Q0I 4Q0I 4Q0I
Sample ID SW-I SW-2 SW-3
Date Collected 10/9/2001 10/9/2001 10/9/2001
Pesticides (ug/L)
alpha-BHC ug/L < 0.05 II 0.02 JI/ 0.02 JI/
beta-BHC ug/L < 0.05 // 0.054 Ji/ 0.044 JI/
delta-BHC ug/L < 0.05 II 0.049 JI/ 0.041 JI/
gamma-BHC (Lindane) ug/L < 0.05 II 0.017 JI/ 0.011 JI/
Heptachlor ug/L < 0.05 II < 0.05 II < 0.05 II
Heptachlor epoxide ug/L < 0.05 II < 0.05 II < 0.05 II
Notes:
Detects shown in bold type.
I -Separates qualifiers added by the laboratory and qualifiers added as a result of validation.
J-Estimated value.
TABLE2
r, OCTOBER 2001
SURFACE WATER
DOWNGRADIENT AREA
4Q0I 4Q0I
SW-4 SW-5
10/9/2001 10/9/2001
0.017 JI/ 0.017 JI/
0.016 JI/ 0.016 JI/
0.018 JI/ 0.02 JI/
< 0.05 II < 0.05 II <
< 0.05 II < 0.05 II <
< 0.05 II < 0.05 II <
Aberdeen Creek Ray's Mill Creek
4Q0I 4Q0I 4Q0I 4Q0I. 4Q0I
SW-6 SW-7 SW-8 SW 11-2 SW-9
10/9/2001 10/9/2001 10/9/2001 10/9/2001 10/9/2001
0.014 JI/ 0.015 JI/ 0.021 JI/ 0.014 Ji/ < 0.05 If
0.022 JI/ 0.625 JI/ 0.039 JI/ 0.026 JI/ < 0.05 II
0.024 JI/ 0.027 JI/ 0.041 JI/ 0.029 J/1 < 0.05 II
0.05 II < 0.05 II < 0.05 II < 0.05 II < 0.05 II
0.05 II < 0.05 II < 0.05 II < 0.05 II < 0.05 II
0.05 II < 0.05 II < 0.05 II < 0.05 II < 0.05 II
• • • • • • • e
e>
9 • e • • • • • 9 • • 4i
e • • • • • 4i
.i
0 • 4' • • • • ~
0 e
e • • • • • • • • e • e • • • •
s Monitonng Wells
Stream
Road
Railroad
C) Pond
Swamp
This map is a product of the Pima::!• Consultng Group Reasonable o.:on. ~-~"
made 10 ensl.1'11 the accuracy of !his map Tho P1nnec1e Consulting P ex,,.-,
dladelms any raponsibility a llablity with regard to the uae of this map. Thl!I Pinnade
Consuttng Group promote$ and 16COl11ffl1Nds the 1o..iepfdldeld veriftc:atkln cl any data
contained on this map by the user of this map product.
Date: Januaiy 08, 2002
Creator: mrd g:lgls~\novartis\geigy\av ___projects\quarter1yWq01\upperaeek.apc-~ 0.1 0 0.1 0.2 0.3 0.4 Miles
THE PINNACLE CONSULTING GROUP
• 0
0 • • • • • Q
0 • • • • • • • a • • • • • e • • • • • • • • • • • • • _,
0 = • • • • • • • • • • 0 • • • •
0.1 0 0.1 0.2 0.3 0.4 Miles • THI PINNACU CONSULTING GROUP
s Monitonng Well
Streams
Road
Railroad
Pond
Swamp
This map IS a product of the Pinnacle Conaulting Group Reesonabhl efforts have been
made to ensure the accuracy of this map Tho PIMecle Consutlng Group expreuly
dtsdalms any responslbilty or-llabllty vritth regard to the use of this map. The Plmacle
~ Group promotes and recommenda the hdepe,..Jern verfflcatlon of any data
contained on tt'Q map by the user of this map prodoct
Data: January oe, 2002.
Creator. mrd g:\gil\pfojoct:s\novartis'Gfligy\av__proj«:.u\quarter1y\4q()11JO\WJrt:reelc.apr
• • • • • • • • • 9
8 • • 9 • (I • • • • • ~
.i)
@ • • • • • .i)
g
0 • • • • • • 0
0 e • • • • • • • • • • • • • •
0.1 0 0.1 0.2 0.3 0.4 Miles ~
THI PINNACU CONSULTING GROUP
Geigy Chemical Corporation Site
Aberdeen, North Carolina
Surface Water Sampling Locations
Streams C) Pond
Road Swamp
Railroad
This map la a product of the Pinnado Conutng Gfcup Rsaonable afforts have bcNn
made to erlSU'9 the accurw:y of thil map The Pimacie Consuts,g Group expressly
dbdl:bns any reaponslbllty or llablllty with regard to the uao or lhla map. Tho PiMacle
Consultlng Group promotm and recommenda the lndepe, .de, ,t vertflcatkln of any data
contained on !his map bo/ lhe u:sor of this map product.
Date: Jmtuary 08, 2002
Creator. mrd g:\gis\projects\ncwartislgeigy',av_projectsq.Jarterlyl,4q01\sur1acewater.apr
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
UPPER BLACK CREEK AQUIFER
GROUNDWATER MONITORING RES UL TS
OCTOBER 2001
DOWNGRADIENT AREA
0
0
0
0
0 • • • • • I) • • • • • • • t)
t)
t) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ..•• : GlJ130168-010
Date Sampled ... : 10/10/01
Prep Date ...... : 10/16/01
Prep Batch# ... : 1290292
Dilution F"actor: 1
PARAMETER
Aldrin
alpha-BBC
beta-BBC
delta-BBC
gamma-BBC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4 1 -DDD
4, 4' -ODE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone ·
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S):
! Eszima1ed result. Result is less than RL
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID: MW lBD
GC Semivolatile~
Work Order# ... : ELSFAlAA
Date Received .. : 10/13/01
Analysis Date .. : 10/27/01
Matrix ......... : WATER
Method ......... ·: sws46 aos:A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L '0.0060
0.43 0.050 ug/L ·0.0080
0.70 0.050 ug/L 0.0040
0.17 0.050 ug/L 0.0060
0 .40 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0,0080
0.058 J 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0 .10 ug/L 0.020
ND 0.10 ug/L 0.029
0.072 J 0.10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.033
ND 0,050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0, 040
ND 2,0 ug/L 1. 4
PERCENT RECOVERY
RECOVERY LIMITS
71 (10 162)
59 (39 -130)
STL -Sacramento [phone] 37 ol 78 .
0
0
0
e e
e
e e
t)
t)
t) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ••• : G1J120284-0l2
Date Sampled ... : 10/09/01
Prep Date ...... : 10/16/01
Prep Batch# ... : 1289343
Dilution Factor: l
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BBC
delta-BBC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE·
Dieldrin
Endrin
4,4'wDDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
. Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
. Decachlorobiphenyl
Tetrachloro-m-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: MW-20D
GC Semivolatiles
Work Order# ... : EL3RN1AA Matrix ......... : WATER
Date Received .. : 10/12/01
.Analysis Date .. : 10/27/01
Method. -

-
...... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.45 0.050 ug/L 0.0080
0.45 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.41 0.050 ug/L 0.0040
0.63 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0. 015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.50 ug/L 0. 040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
105 (10 -162)
80 (39 -130)
(916) 373 • 5600 20 of 60
Cit • 0
0
0
0
0 e • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Let-Sample # ... : GlJ120284-015
Date Sampled •.. : 10/10/01
Prep Date ...... : 10/16/01
Prep Batch # ••• : 1290292
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4,4 1 -DDE
4,4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: MW-22D
GC Semivolatiles
Work Order# ... : EL3RR1M Matrix ......... : WATER
Date Received. _: 10/12/01
Analysis Date .. : 10/26/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
0.44 0.050 ug/L 0.0080
0.61 0.050 ug/L 0.0040
0.78 0.050 ug/L 0.0060
0.37 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.10 ug/L 0. 024
ND 0.050 ug/L 0.010
ND 0 .10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0. 040
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
80 (10 -162)
63 (39 -130)
(916) 373 -5600 23 ol 60
(t • • • 0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... ' GlJ120284-020
Date Sampled ... , 10/11/01
Prep Date ...... , 10/17/01
Prep Batch JI ••. , 1290304
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4, 4' -DDD
4, 4' -DDE
4,4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S) ,
J Estimated result. Result is less than RL .
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID, MW-23D
GC Semivolatiles
Work Order# ... , EL3R21AA Matrix ......... , WATER
Date Received .. : 10/12/01
Analysis Date .. , 10/29/01
Method ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
0.23 0.050 ug/L 0.0080
0.13 0.050 ug/L 0. 0040
0.037 J 0.050 ug/L 0.0060
0 .14 0.050 ug/L 0.010
ND 0,050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0,10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0.040
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
101 (10 -162)
73 (39 -130)
(916) 373 • 5600 28 of 60
• • 0
0
0
0 .,
• • I) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... , GlJ130168-012
Date Sampled ... , 10/11/01
Prep Date ...... , 10/17/01
Prep Batch# ... , 1290304
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
ganuna-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4, 4' -DDE
4,4' -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID, MW 26D
GC Semivolatiles
Work Order# ... , ELSFDlAA
Date Received .. : 10/13/01
Analysis Date .. , 10/29/01
Matrix ......... : WATER
Method ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
0.056 0.050 ug/L 0.0080
0.082 0.050 ug/L 0.0040
0.11 0.050 ug/L 0.0060
0.085 0.050 ug/L 0. 010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0. 10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.10 ug/L 0. 024
ND 0.050 ug/L 0. 010
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0.040
ND 2.0 ug/L l. 4
PERCENT RECOVERY
RECOVERY LIMITS
108 (10 162)
74 (39 -130)
STL -Sacramento (916) 373 -5600 39 of 78
• G
G
G
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : G1Jl30168-015
Date Sampled ... : 10/12/01
Prep Date ...... : 10/18/01
Prep Batch# ... : 1291251
Dilution Factor: S
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BBC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4, 4 1 -DDD
4,4'-DDE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S):
l Estirnatcd resull. Result is less than RL.
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID: MW 30D
GC Semivolatiles
Work Order# ... : EL5FG1AA
Date Received .. : 10/13/01
Analysis Date .. : 11/08/01
Matrix ......... : WATER
Method ..•...... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.25 ug/L 0. 030
0.47 0.25 ug/L 0.040
4.0 0.25 ug/L 0.020
0.36 0.25 ug/L 0.030
0.26 0.25 ug/L 0.050
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0.040
0.38 J 0.50 ug/L 0.J.0
ND 0.50 ug/L 0.025
ND 0.50 ug/L 0.075
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0 .10
ND 0.50 ug/L 0. 14
0.45 J 0.50 ug/L 0. J.2
ND 0.25 ug/L 0.050
ND a.so ug/L 0.10
ND 0.50 ug/L 0.16
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0. 040
ND 2.5 ug/L 0.20
ND 10 ug/L 7.0
PERCENT RECOVERY
RECOVERY LIMITS
60 (10 -162)
44 (39 -130)·
STL -Sacramento (916) 373 -5600 42 of 78
• Cl
C,
D
0
0
0 • e • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample II ••• : GlJ120284-010
Date Sampled ... : 10/09/01
Prep Date •...•. : 10/16/01
Prep Batch # ••• : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
garmia-BHC (Linda.De)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE
Dieldrin
Endrin
4, 4' -DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S),
J Estimated result. Re.mil is Jcs.s than RL .
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: MW-35D
GC Semivolatiles
Work Order# ... : EL3RL1AA Matrix ......... : WATER
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Met.hod ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.12 0.050 ug/L 0.0080
0.077 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.088 0.050 ug/L 0.0040
0.022 J 0 .050. ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.50 ug/L 0.040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
103 (10 -162)
71 (39 -130)
(916) 373 · 5600 18 of 60
• 0
0
0
0
0 • • • • I) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
LOWER BLACK CREEK AQUIFER
GROUNDWATER MONITORING RESULTS
OCTOBER 2001
DOWNGRADIENT AREA
• • • 8
0
0
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
PINNACLE CONSULTING GROUP
Client sample ID: MW-22L
GC Sem.ivolatiles
Lot-Sample II ••• : G1J120284-014 Work Order # ••• : EL3RQ1AA Matrix ......... : WATER
Date Sampled ... : 10/10/01 Date Received .. : 10/12/01
Prep Date .•...• : 10/16/01 Analysis Date .. : 10/29/01
Prep Batch.ft ... : 1289343
Dilution Factor: 10 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT UNITS MDL
alpha-BHC 2 .1. 0.50 ug/L 0.080
gamma-BBC (Lindane) 1.. 8 0.50 ug/L 0.1.0
Heptachlor ND 0.50 ug/L 0.070
Aldrin ND 0.50 ug/L 0.060
beta-BHC l..8 0.50 ug/L 0.040
delta-BHC 2.1. 0.50 ug/L 0.060
Heptachlor epoxide ND 0.50 ug/L 0.080
Endosulfan I ND 0.50 ug/L 0.10
gamma-Chlordane ND 0.50 ug/L 0.080
alpha-Chlordane ND 0.50 ug/L 0.070
4,4'-DDE ND l..O ug/L 0.15
Dieldrin ND 10 ug/L 0.20
Endrin ND 1.0 ug/L 0.20
4,4'-DDD ND 1.0 ug/L 0.050
Endosulfan II ND 1.0 ug/L 0.20
4,4'-DDT ND 1.0 ug/L 0.20
Endrin aldehyde ND 1.0 ug/L 0.29
Me thoxychlor ND 5.0 ug/L 0.40
Endosulfan sulfate ND 1.0 ug/L 0.33
Endrin ketone ND 10 ug/L 0.24
Toxaphene ND 20 ug/L 14
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Decachlorobiphenyl 0.0 SRD (10 -162)
Tetrachloro-m-xylene 0.0 SRD (39 -130)
IIOTB(S}:
SRD TIie surrogate rca;r;,uy wa.s 001 calcul2tcd because the extract was dilWed be)'OBi the abilicy 10 quantitate a recovery .
STL Sacramento (916) 373 • 5600 22 of 60
(t • • • • 0 • • • ., • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... , GlJ120284-019
Date Sampled ... , 10/11/01
Prep Date ...... , 10/17/01
Prep Batch # ... , 1290304
Dilution Factor: 5
PARAMETER
Aldrin
alpba-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4, 4 '-DDE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
E:idosulfan II
Endosulfan sul::"ate
Heptachlor
Heptachlor epcxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
Sil Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID, MW-25L
GC Semivolatiles
Work Order# ... , EL3R01AA
Date Received .. , 10/12/01
Analysis Date .. , 11/07/01
Matrix.········= WATER
Method ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.25 ug/L 0.030
1. 7 0.25 ug/L 0. 040
0.35 0.25 ug/L 0.020
0.68 0.25 ug/L 0.030
1.2 0.25 ug/L 0.050
ND 0.25 ug/L 0. 035
ND 0.25 ug/L 0. 040
ND 0.50 ug/L 0 .10
ND 0.50 ug/L 0.025
ND 0.50 ug/L 0.075
ND 0.50 ug/L 0. 10
ND 0.50 ug/L 0 .10
ND 0.50 ug/L 0.14
ND 0.50 ug/L 0. 12
ND 0.25 ug/L 0.050
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.16
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0. 04 0
ND 2.5 ug/L 0.20
ND 10 ug/L 7.0
PERCENT RECOVERY
RECOVERY LIMITS
77 (10 -162)
51 (39 -130)
(916) 373 • 5600 27 of 60
• • • 0 e
0
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... , GlJ120284-016
Date Sampltod ... , 10/10/01
Prep Date ...... , 10/16/01
Prep Batch # ... ' 1290292
PINNACLE CONSULTING GROUP
Client Sample ID, MW-27L
GC Semivolatiles
Work order # ... , EL3RTL!\A
Date Received .. , 10/12/01
Analysis Date .. , 10/29/01
Matrix ......... , WATER
Dilution Factor: lO Method ......... , SW846 8081A
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND 0.50
alpha-BHC 3.7 0.50
beta-BHC 1.5 0.50
delta-BHC 2.4 0.50
gamma-BHC (Lindane) 2.3 0.50
alpha-Chlordane ND 0.50
gamma-Chlordane ND 0.50
Dieldrin ND 1.0
4, 4' -DDD ND 1.0
4, 4' -DDE ND 1.0
4,4'-DDT ND 1.0
Endrin ND 1.0
Endrin aldehyde ND 1.0
Endrin ketone ND 1.0
Endosulfan I ND 0.50
Endosulfan II ND 1.0
Endosulfan sulfate ND G 2.5
Heptachlor ND 0.50
Heptachlor epoxide ND a.so
Met:loxychlor ND 5.0
Toxaphene ND 20
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Decachlorobiphenyl a.a SRO ( 10 -162)
Tetrachloro-m-xylene a.a SRD (39 -130)
NOTE(S),
SRD 111<: Airrogsie recovery wu 11.ot calculated because tl1e cx.rract was dil11cd beyond the ability c-o qua111i1Atc a reco1,·CI)' .
G Elt:'Jetcd rcponini; limit. TI1c rL1)0~ limi1 b c:kvucd due 10 1u111P. imerlcn:-ucc.
STL Sacramento (916) 373 • 5600 .
UNITS MDL
ug/L 0.060
ug/L 0.080
ug/L 0. 040
ug/L 0.060
ug/L 0.10
ug/L 0.070
ug/L 0. 080
ug/L 0.20
ug/L 0.050
ug/L 0.15
ug/L 0.20
ug/L 0.20
ug/L 0.29
ug/L 0.24
ug/L 0.10
ug/L 0.20
ug/L 0.33
ug/L 0.070
ug/L 0.080
ug/L 0 .40
ug/L 14
24 of 60
ct • • G
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... , G1J130168-0ll.
Date Sampled .... , 10/12/01
Prep Date ...... : 10/18/01
Prep Batch# ... , 1291251
Dilution Factor: 5
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4 1 -DDD
4,4'-DDE
4,4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone·
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID: MW 31L
GC Semivolatiles
Work Order# ... : EL5FC1AA
Date Received .. , 10/13/01
Analysis Date .. , 11/07/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.25 ug/L 0.030
2.2 0.25 ug/L 0.040
0.62 0.25 ug/L 0.020
1.1 0.25 ug/L 0.030
1.2 0.25 ug/L 0.050
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0.040
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.025
ND 0.50 ug/L 0.075
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.14
ND 0.50 ug/L 0.12
ND 0.25 ug/L 0.050
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.16
ND 0.25 ug/L 0. 035
ND 0.25 ug/L 0. 040
ND 2.5 ug/L 0.20
ND 10 ug/L 7,0
PERCENT RECOVERY
RECOVERY LIMITS
77 (10 -162)
58 (39 -130)
STL -Sacramento (916) 373 -5600 38 of 76
• • 0
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... : GlJ130168-016
Date Sampled ... : 10/12/01
Prep Date ...... : 10/18/01
Prep Batch # ... : 1291251
Dilution Factor: l
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindanel
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4 1 -DDD
4,4' -DDE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID: MW 32L
GC Semivolatiles
Work Order # ... : EL5FH1AA Matrix ......... : WATER
Date Received .. : 10/13/01
Analysis Date .. : 10/28/01
Method ........ -: SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0040
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0 .10 ug/L 0.029
ND 0 .10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0 .10 ug/L 0.020
ND 0.10 ug/L 0. 033
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0.040
ND 2.0 ug/L 1. 4
PERCENT RECOVERY
RECOVERY LIMITS
30 (10 162)
62 (39 -130)
STL • Sacramento (916) 373 -5600 43 of 78
• • • • • e • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • e • • •
Lot-Sample # ... ' GlJ130168-013
Date Sampled ... : 10/11/01
Prep Date ...... , 10/17/01
Prep Batch # ••• : 1290304
Dilutiori Factor: l
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4, 4' -ODE
4, 4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
':'oxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
G1K130168
PINNACLE CONSULTING GROUP
Client Sample ID, MW 36L
GC Semivolatiles
Work Order # ... : EL5FE1AA Matrix ......... : WATER
Date Received .. : 10/13/01
Analysis Date .. : 10/29/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MOL
NO 0.050 ug/L 0.0060
NO 0.050 ug/L 0.0080
NO 0.050 ug/L 0.0040
NO 0.050 ug/L 0.0060
NO 0.050 ug/L 0.010
NO 0.050 ug/L 0.0070
NO · 0. 050 ug/L 0.0080
NO 0.10 ug/L o·. 020
NO 0 .10 ug/L 0.0050
NO 0.10 ug/L 0.015
NO 0 .10 ug/L 0.020
NO 0 .10-ug/L 0.020
NO 0.10 ug/L 0. 029
NO 0.10 ug/L 0.024
NO 0.050 ug/L 0.010
NO 0.10 ug/L 0.020
NO 0.10 ug/L 0.033
NO 0.050 ug/L 0.0070
NO 0.050 ug/L 0.0080
NO 0.50 ug/L 0.040
NO 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
104 (10 -162)
73 (39 -130)
$TL -Sacramento (916) 373 · 5600 40 of 78
• • • G
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : G1Jl20284··021
Date Sampled ... : 10/11/01
Prep Date ...... : 10/17/01
Prep Batch# ... : 1290304
Dilution Factor: 5
?ARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindanel
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4,4'-DDE
4,4'-DDT
Endrin
Endrin aldehyde
Endri:i. ketone
Endosulfan I
Endosulfan I-I
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-rn-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: MW-37L
GC Semivolatiles
Work Order ff ... : ELJR41AA
Date Received .. : 10/12/01
Analysis Date .. : 11/07/01
Matrix ... ······= WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.25 ug/!., 0. 030
2.5 0.25 ug/L 0.040
0.37 0.25 ug/L 0.020
0.91 0.25 ug/L 0.030
2.0 0.25 ug/L 0.050
ND 0.25 ug/L 0. 035
ND 0.25 ug/L 0. 040
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0. 025
ND 0.50 ug/L 0.075
ND 0.50 ug/L 0.10
NO 0.50 ug/L 0.10
ND 0.50 ug/L 0.14
NO 0.50 ug/L 0 .12
NO 0.25 ug/L 0.050
NO 0.50 ug/L 0 .10
NO 0.50 ug/L 0.16
ND 0.25 ug/L 0.035
NO 0.25 ug/L 0. 040
NO 2.5 ug/L 0.20
ND 10 ug/L 7.0
PERCENT RECOVERY
RECOVERY LIMITS
96 (10 -162)
75 (39 -130)
(916) 373 · 5600 29 of 60
• • • G
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ••. , G2Al10239-001
Date Sampled ... , 01/10/02
Prep Date ...... , 01/14/02
Prep Batch # ... , 2014331
Dilution Factor: 1
PARAMETER
Aldri11
alpha·BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4, 4 '-DDD
4, 4 '·DOE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTEW),
J Estimated rcsu1L ~ll is lr:ss tbJD RL
G2A 110239
PINNACLE CONSULTING GROUP
Client Sample m, MW-38L
GC Semivolatiles
Work Order # ... , ERJRAlAA
Date Recei vcd .. : 01/11/02
Analysis Date •• , 01/23/02
Matrix ......... , WATER
Method ......... ' SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0040
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
0.021 J O.J.O ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.029
ND 0.10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0. 040
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
76 (10 -162)
81 (39 -130)
STL Sacramento (916) 373 -5600 8 of 12
• • ct • • 0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ••• : GlJ120284-01B
Date Sampled •.. : 10/10/01
Prep Date ...... : 10/16/01
Prep Batch# .•• : 1290292
Dilution Factor: 1
PARAMETER
Aldrin
alpha·BHC
beta·BHC
delta·BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4 ,4 1 -DDD
4,4'-DDE
4,4'-DDT
Endrin
Endrin aldehyde
Endrin ketone.
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
STL Sacramento
PINNACLE CONSOLTING GRO!JP
Client Sample ID: MW-39L
GC Semivolatiles
Work Order# ... : EL3RX1AA Matrix ......... : WATER
Date Received .. : 10/12/01
Analysis Date .. : 10/26/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0040
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0. 020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0 .10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0.050 ug/L . 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0. 040
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
67 (10 -162)
59 (39 -130)
(916) 373 · 5600 26 ol 60
r
(t • • 0
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lat-sample# ... : GlJ130168-020
Date Sampled ... : 10/11/01
Prep Date ...... : 10/18/01
Prep Batch # ... : 1291251
Dilution Factor: 5
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
galllllla-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4 1 -DDD
4,4'-DDE
4, 4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S) :
J Estimated result. Result is less l.haa RL
•. G1K130168 •
PINNACLE CONSULTING GROUP
Client Sample ID: MW 40L
GC Semivolatiles
Work Order # ... : ELSFMlAA Matrix ......... : WATER
Date Received .. : 10/13/01
Analysis Date .. : 11/08/01
Method ...•...•• : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.25 ug/L 0.030
1.2 0.25 ug/L 0.040
0.45 0.25 ug/L 0.020
0.76 0.25 ug/L 0.030
0.18 J 0.25 ug/L 0.050
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0.040
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.025
ND a.so ug/L 0.075
ND 0.50 ug/L 0 .10
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.14
ND 0.50 ug/L 0.12
ND 0.25 ug/L 0.050
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.16
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0.040
ND 2.5 ug/L 0.20
ND 10 ug/L 7.0
PERCENT RECOVERY
RECOVERY LIMITS
38 . (10 -162)
42 (39 -130)
STL -Sacramento [phone] 47 of 78
• • • 0 • C) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : GlJ120284-013
Date Sampled ... : 10/09/01
Prep Date ...... : ·10/16/01
Prep Batch# ... : 1289343
Dilution Factor: 5
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4 1 -DDE
Dieldrin
Endrin
4,4'-DDD
Endosulfan II
4,4 1 -DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J Estimated result. Result is less than RL .
STL Sacramento
PINNACLE CONSULTlNG GROUP
Client Sample ID: PZ-2
GC Semivolatiles
Work Order II ••. : EL3RP1AA
Date Received .. : 10/12/01
Analysis Date .. : 10/29/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.62 0.25 ug/L 0.040
0.56 0.25 ug/L 0.050
ND 0.25 ug/L 0.035
ND 0.25 ug/L 0.030
0. l. 7 J 0.25 ug/L 0.020
0 .25 0.25 ug/L 0.030
ND 0.25 ug/L 0.040
ND 0.25 ug/L 0.050
ND 0.25 ug/L 0.040
ND 0.25 ug/L 0.035
ND 0.50 ug/L 0.075
ND 0.50 ug/L 0.10
ND a.so ug/L 0.10
ND 0.50 ug/L 0.025
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.10
ND 0.50 ug/L 0.14
ND 2 .5 · ug/L 0.20
ND 0.50 ug/L 0.16
ND 0.50 ug/L 0. 12
ND 10 ug/L 7.0
PERCENT RECOVERY
RECOVERY LIMITS
59 (10 -162)
72 (39 -130)
(916) 373 • 5600 21 of 60
D • G
0 • • I) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •• • • • • • • • • • 1• • • • • • •
Lot-Sample ll .•. : GlJl.20284-011
Date Sampled ... : 10/09/01
!?rep Date ...... : 10/16/01
Prep Batch# ... : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gannna-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE
Dieldrin
Endrin
4,4' -DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachlord-m-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: PZ-3
GC Semivolatiles
Work Order# ... : EL3RMlAA
Date Received .. : 10/12/01
J\Dalysis Date .. : 10/27/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0 .49 0.050 ug/L 0.0080
0.42 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0 .11 0.050 ug/L 0.0040
0.17 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.50 ug/L 0.040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1. 4
PERCENT RECOVERY
RECOVERY LIMITS
100 (10 -162)
73 (39 -130)
(916) 373 • 5600 19 of 60
Cl
G
G
0 e
t) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... : G1Jl20284-017
Date Sampled ... : 10/10/01
Prep Date ...... : 10/16/01
Prep Batch # ••• : 1290292
Dilution Factor: l
PARAMETER
Aldrin
alpha-BHC
beta-BBC
delta-BBC
gamma-BBC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4, 4' -DDE
4,4 1 -DDT
Endrin
Endrin aldehyde
Endrin ketone
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J Estimated result. Resull is less than RI..
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: PZ-5
GC Semivolatiles
Work Order# ... : EL3RW1AA Matrix ......... : WATER
Date Received .. : 10/12/01
Analysis Date .. : 10/26/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0060
0.18 0.050 ug/L 0.0080
0.069 0.050 ug/L 0.0040
0.021 J 0.050 ug/L 0.0060
0.26 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 0.10 ug/L 0.024
ND 0.050 ug/L 0.010
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.033
ND 0. 050 ug/L 0.0070
ND 0.050 ug/L 0.0080
ND 0.50 ug/L 0. 040
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
73 ( 10 -162)
61 (39 -130)
(916) 373 · 5600 25 of 60
8 • • • .,
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
STREAM SURFACE WATER MONITORING RESULTS
OCTOBER 2001
DOWNGRADIENT AREA
0
0
C)
C)
C) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : GlJ120284-008
Date Sampled ... : 10/09/01
Prep Date ...... : 10/16/01
Prep Batch# ... : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE
Dieldrin
Endrin
4, 4 1 -DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client sample ID: SW-1
GC Semivolatiles
Work Order# ... : EL3RJ1AC
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0040
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 2.0 ug/L 0. 040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
97 (10 -162)
85 (39 -130)
(916) 373 · 5600 16 of 60
• • • • • • • • • • • • • • • • • • • • • • • • • • •• • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ... ' G1Jl20284-007
Date Sampled .. _ , 10/09/01
Prep Date ...... : 10/16/01
Prep Batch #. --: 1289343
Dilution Factor: 1
PARAMETER
alpha-BBC
gamma-BHC {I,iudaoe)
Heptachlor
Aldrin
beta-BBC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4, 4' -DOE.
Dieldrin
Endrin
4,4' -DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
~ndrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J ~ed result. Rcsull is less than RL .
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID, SW-2
GC Semivolatiles
Work Order # ..• ' EL3RH1AC Matrix .. -...... :. WATER
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.020 J 0.050 ug/L 0.0080
0.017 J 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.054 J 0.050 ug/L 0. 0040
0.049 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 2.0 ug/L 0.040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
BO (10 162)
61 (39 -130)
(916) 373 -5600 15 of 60
0
0 • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-sample# ... : GlJ120284-006
Date Sampled ... : 10/09/0l
Prep Date ...... : 10/16/01
Prep Batch# ... : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC {Lindane)
Heptachlor
Aldrin
beta-BBC
delta-BBC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDS
Dieldrin
Endrin
4,4'-DDD
Endosulfan II
4,4 1 -DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J Estimated result. Result is less than RL .
STL Sacramento
PINNACLE CONSULTING GROUP
Client sample ID: SW-3
GC Semivolatiles
Work Order# ... : EL3RF1AC
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.020 J 0.050 ug/L 0.0080
0.011. J 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.044 J 0.050 ug/L 0.0040
0.041 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/i:, 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 2.0 ug/L 0.040
ND 0 .10 ug/L 0.033
ND 0;10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
83 (10 -162)
72 (39 -130)
(916) 373 • 5600 14 of 60
0
0
G
G • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample ii •.. : G1Jl20284-001
Date Sampled ... : 10/09/01
Prep Date ...... : 10/16/01
Prep Batch ll •.• : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4' -DDE
Dieldrin
Endrin
4,4'-DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J Estimated rc:su.11. Result is less than RL
STL Sacramento
PINNACLE CONSULTmG GROUP
Client Sample ID: SW-4
GC Semivolatiles
Work Order# ... : EL3Q91AC
Date Received .. : 10/12/01
Analysis Date.~: 10/27/01
Matrix ......... : WATER
Method .•.•..... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
O.Ol.7 J 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.016 J 0.050 ug/L 0.0040
0.018 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 2.0 ug/L 0.040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1. 4
PE:RCENT RECOVERY
RECOVERY LIMITS
66 (10 -162)
78 (39 -130)
(916) 373 · 5600 9 of60
0
0 • I)
e
e • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : GlJ120284-002
Date Sampled.:.: 10/09/01
Prep Date ...... : 10/16/01
Prep Batch# ... : 1289343
Dilution Factor: 1
PARAMETER
alpha-BBC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Bndosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE
Dieldrin
Endrin
4,4'-DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S) :
J EstimalCd r~I. Result is less than RL.
STL Sacramento
PlNNACLE CONSULTING GROUP
Client Sample ID: SW-5
GC Semivolat~les
Work Order# ... : EL3RA1AC
Date Received .. : 10/12/01
Analysis Date •• : 10/27/01
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.017 J 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.016 J 0.050 ug/L 0. 0040
0.020 J 0.050 ug/L 0.0060
ND 0.050 ug/L .o. 0080
ND 0.050 ug/L 0. 010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.029
ND 2.0 ug/L 0. 040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1. 4
PERCENT RECOVERY
RECOVERY LIMITS
63 (10 -162)
81 (39 -130)
(916) 373 • 5600 . 10 of 60
• • t)
t) • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # ..• : GlJl30l68-022
Date Sampled ... : 10/09/0l
Prep Date ...... : 10/16/0l
Prep Batch# ... : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
beta-BHC
delta-BHC
Heptachlor epoxide
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOT!l (S):
J Estimated result. Result is less UWl RL .
• G1K130168 •
PINNACLE CONSULTING GROUP
CJ.ient Sample ID: SW 6
GC Semivolatiles
Work Order# ... : ELSFPlAC Matrix ......... : WATER
Date Received_ . : 10/13/0l
Aoa.J.ysis Date .. : 10/28/01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0. 01.4 J 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
0.022 J 0.050 ug/L 0.0040
0.024 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
PERCENT RECOVERY
RECOVERY LIMITS
45 (10 -162)
71 (39 . 130)
STL • Sacramento {916) 373-5600 49 of 78
e • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample II •.. : G1J120284-003
Date Sampled ... : 10/09/01
Prep Date ...... : 10/16/01
Prep Batch # ••. : 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4'-DDE
Oieldrin
Endrin
4,4' -DOD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Metho,cychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE(S):
J Estimated result. Resull is less lhan RL
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: SW-7
GC Semivolatiles
Work Order# ... : EL3RC1AC Matrix ......... : WATER
Date Received .. : 10/12/01
Analysis Date .. : 10 /27 /01
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.015 J 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.025 J 0.050 ug/L 0.0040
0.027 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0. 029
ND 2.0 ug/L 0.040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2. 0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
62 (10 -162)
68 (39 -130)
(916) 373 · 5600 11 of 60
., • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-sample II ... : GlJl20284-004
Date sampled ... : 10/09/01
Prep Date ...... : 10/16/01
Prep Batch II ... : 1289343
Dilution Factor: l
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordane
4,4 1 -DDE
Dieldrin
Endrin
4,4'-DDD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin.ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTK(SJ:
J Estimated r~. R.csult is less than RL
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: SW-8
GC Semivolatiles
Work order II ... : EL3RDlAC
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Matrix ......... : WATER
Method •••••..•. : SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0.021 J o.oso ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
0.039 J 0.050 ug/L 0.0040
0.041 J 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.015
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0.020
ND 0.10 ug/L 0. 029
ND 2.0 ug/L 0. 040
ND 0.10 ug/L 0.033
ND 0.10 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
73 (10 -162)
83 (39 -130)
(916) 373 • 5600 12 ol 60
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample# ... : GlJ120284-005
Date Sampled ... : 10/09/01
Prep Date ...... : 10/16/01·
Prep Batch # ... : 1289343
Dilution Factor: 1.
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
Aldrin
beta-BHC
delta-BHC
Heptachlor epoxide
Endosulfan I
gamma-Chlordane
alpha-Chlordan_e
4,4'-DDE
Dieldrin
Endrin
4, 4' -ODD
Endosulfan II
4,4'-DDT
Endrin aldehyde
Methoxychlor
Endosulfan sulfate
Endrin ketone
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
STL Sacramento
PINNACLE CONSULTING GROUP
Client Sample ID: SW-9
GC Semivolatiles
Work Order# ... : EL3RE1AC Matrix ...•..... : WATER
Date Received .. : 10/12/01
Analysis Date .. : 10/27/01
Method ......... : SW846 8081.A
REPORTING
RESULT LIMIT UNITS MDL
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.010
ND 0.050 ug/L 0.0070
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0040
ND 0.050 ug/L 0.0060
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.01.0
ND 0.050 ug/L 0.0080
ND 0.050 ug/L 0.0070
ND 0.10 ug/L 0.01.5
ND 0 .1.0 ug/L 0.020
ND 0. 1.0 ug/L 0.020
ND 0.10 ug/L 0.0050
ND 0.10 ug/L 0.020
ND 0 .1.0 ug/L 0.020
ND 0.1.0 ug/L 0.029
ND 2.0 ug/L 0.040
ND 0.1.0 ug/L 0.033
ND 0. 1.0 ug/L 0.024
ND 2.0 ug/L 1.4
PERCENT RECOVERY
RECOVERY LIMITS
75 (10 -1.62)
76 (39 -1.30)
(916) 373 -5600 13of 60
• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •
Lot-Sample # •.• ' G1Jl30168-023
Date Sampled ... , 10/09/01
Prep Date ...... : 10/16/01
Prep Batch # •.. , 1289343
Dilution Factor: 1
PARAMETER
alpha-BHC
gamma-BHC (Lindane)
Heptachlor
beta-BHC
delta-BHC
Heptachlor epoxide
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
NOTE (S),
J ES1ima1ed result. Resull is less than RL .
• G1K130168 •
PINNACLE CONSULTING GROUP
Client Sample ID, SW 11-2
GC Semivolatiles
Work Order# ... : EL5FQ1AC Matrix ......... : WATER
Date Received .. : 10/13/01
Analysis Date .. : 10/28/01
Method .•••..... ' SW846 8081A
REPORTING
RESULT LIMIT UNITS MDL
0. 0l.4 J 0.050 ug/L 0.0080
ND 0 :050 ug/L 0.010
ND 0.050 ug/L 0.0070
0.026 J 0.050 ug/L 0. 0040
0.029 J 0.050 ug/L 0.0060
ND 0. 050 ug/L 0.0080
PERCENT RECOVERY
RECOVERY LIMITS
46 (10 -162)
71 (39 -130)
STL • Sacramento (916) 373 • 5600 50 of 78