NCD981927502_19991014_Geigy Chemical Corporation_FRBCERCLA RA_Fifth Event Second Quarter 1999 Downgradient Area Monitoring Report-OCR

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FIFTH EVENT, SECOND QUARTER 1999
DOWNGRADIENT AREA MONITORING REPORT
Geigy Chemical Corporation '
...,,. CERCLA Site
Aberdeen, North Carolina
OCTOBER 1999
RECE\\/EO
OCi 1s 1999
r:\.)i,\O sE.C1\0l'-I
s\.l?~R,
THE PINNACLE CONSULTING GROUP
"Providing Decision Support Through Knowledge and Technology"
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October 14, 1999
Ms. Giezelle Bennett
Remedial Project Manager
Geigy Chemical Corporation Site
Aberdeen, North Carolina
Committee Correspondence
USEPA Region IV, North Superfund Remedial Branch
11th Floor
61 Forsyth Street, SW
Atlanta, GA 30303-3104 VIA QYEBNTGHT DEJ.TYEBY
RE: Fifth Event, Second Quarter 1999 Downgradient Area Monitoring Report
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Giezelle:
In accordance with the Downgradient Groundwater Remedial Action Work Plan (RA WP), please
find attached one copy of the analytical results for the second quarter 1999 downgradient area
monitoring event (the fifth in a series of twelve quarterly monitoring events scheduled for the initial
three years of the remedy). To facilitate your review, analytical data summary tables and figures
showing detected concentrations at sample locations are attached.
Samples for the second quarter monitoring event were collected April 12, 1999 through April 15,
1999. Monitoring results (Table I) indicate that the remedy continu~s to be protective of potential
human and ecological receptors, as well as area streams. Findings that support this conclusion
include:
I Tpper Black Creek Aquifer
• Pesticide concentrations in monitoring wells located west of the groundwater extraction
system (i.e., in the downgradient area) are comparable to levels found during previous
monitoring events. The lateral extent of pesticides exceeding groundwater performance
standards in the Upper Black Creek aquifer continues to be less than that observed during the
initial downgradient area groundwater-sampling event (June 1996 for wells PZ-5, MW-31L
and MW-32L; August 1995 for all other wells).
• Beta-BHC was detected at a concentration of 0.1 ug/1 in the groundwater sample collected on
April 14, 1999 from monitoring well MW-34D, and at a concentration of 0.13 ug/l in a
confirmatory sample collected from MW-34D on June 15, 1999. No otherTCL pesticides were
detected in the April 14, 1999 or June 15, 1999 samples collected from this well.
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• BHC isomer concentrations in monitoring wells located downgradient of the groundwater
extraction system are below the maximum BHC isomer concentrations forecasted for the Upper
Black Creek aquifer by the transport model (see Table 3).
Tower Black Creek Aquifer
• The extent of pesticides in the Lower Black Creek aquifer is similar to conditions reflected by
previous quarterly monitoring events and the baseline sampling event (June 1996 for wells
PZ-5, MW-31L and MW-32L; August 1995 for all other wells).
• Pesticides were not detected in well MW-36L as part of this or previous quarterly sampling
events for this well. Well MW-36L was installed to serve as a sentinel monitoring point for
Town Well No. 2.
• With the exception of BHC isomer concentrations reported for MW-27L and an estimated
beta-BHC concentration reported for MW-22L, BHC levels in the Lower Black Creek aquifer
are below the maximum concentrations forecasted by the transport model (see Table 4).
Analytical results for monitoring wells surrounding MW-27L (i.e., MW-22L, MW-25L,
MW-28L, MW-36L, MW-37L and PZ-3) indicate that the BHC levels observed at MW-27L
are limited in extent and therefore· are not anticipated to affect the remedy duration or level of
protection.
• As predicted by Site groundwater flow and transport model simulations conducted for the
Downgradient Groundwater Remedial Action Work Plan, BHC isomer concentrations in well
MW-31L have experienced a slight increase due to the migration of peak BHC
concentrations towards Aberdeen Creek. The BHC isomer concentrations at MW-3!L
continue to be protective of groundwater concentrations at wells immediately downgradient
of this general area (MW-32L and MW-38L).
• Pesticides were not detected in wells MW-32L and MW-39L, which adjoin Aberdeen and
Ray's Mill Creeks, respectively. Dieldrin was the only constituent detected in well MW-38L,
located adjacent to Aberdeen Creek, at an estimated concentration of 0.054 ug/L. Dieldrin
was not detected at any other monitoring well in the Lower Black Creek aquifer.
Stream Surface Water
• Analytical results for sentinel wells MW-32L, MW-38L and MW-39L, which monitor the
Lower Black Creek aquifer prior to its discharge to surface water, were non-detect for the
constituents found in Aberdeen Creek surface water samples and demonstrate that pesticides
in downgradient area groundwater do not extend to Aberdeen and Ray's Mill Creeks.
• Pesticides were not detected above the reported sample quantitation limits in the surface
water sample collected from the headwaters of McFarland's Branch (SW-01).
• Alpha-, beta-, delta-and gamma-BHC were detected at surface water locations SW-02 and
SW-03 in McFarland's Branch. Concentrations detected at each location are nearly identical
to previous quarterly monitoring levels, and slightly less than the concentrations reported for
these locations during the June 1996 monitoring event. The results are within the range of
surface water concentrations estimated for these locations by the transport model (Table 3-10
of the RA WP) and are at levels that are protective of potential human and ecological
receptors.
• Estimated concentrations of alpha-, beta-and delta-BHC were detected in surface water
samples SW-04, SW-05, SW-07 and SW-08 collected on April 12, 1999 from Aberdeen
Creek. Laboratory quality control problems were associated with the analysis of Aberdeen
Creek surface water SW-06, collected on April 12, 1999. SW-06 was therefore re-sampled
on June 15, 1999. Estimated concentrations of beta-and delta-BHC were detected in this
surface water .sample at levels comparable to those reported for surface water samples
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collected from SW-04, SW-05, SW-07 and SW-08 on April 12, 1999.
• Surface water and groundwater analytical results collectively reveal that the pesticides
detected in Aberdeen Creek are not Site-related. Aberdeen Creek surface water results reveal
that surface water concentrations arc at levels that are protective of potential human and
ecological receptors.
• Pesticides were detected in Aberdeen Creek in an area that lies outside of the downgradient
extent of Site-related pesticides (i.e., surface water sample SW-08, located upstream of the
confluence with Ray's Mill Creek). This finding indicates the source of pesticides detected
in Aberdeen Creek lies upstream of SW-08 and is not Site-related.
• Pesticide concentrations are nearly identical among surface water samples collected from
Aberdeen Creek at locations downstream and upstream of the confluence with McFarland's
Branch, thereby further indicating that the estimated levels of pesticides in Aberdeen Creek
are not attributable to Site conditions.
Private Well Survey
• A survey to identify newly installed residential water supply wells was performed as part of the
quarterly monitoring event by driving each road in the downgradient area and conducting a
visual inspection of the properties to locate pump houses and/or well heads. No newly installed
private wells were identified.
The Companies are reviewing preliminary results for the third quarter 1999 monitoring event and
anticipate that the data will be reported to the Agencies next month. If you require additional
copies of the enclosed materials, or have any questions about the monitoring results, please contact
me at [phone].
Regards,
Garland Hilliard
Project Coordinator
/Enclosure
c: R. McElveen (NCDENR)7
T. Eggert (CDM)
H. Moats (Novartis)
H. Grubbs, Esq. (WCS&R)
B. Vinzant (Kaiser)
M. Sheehan (Pinnacle)
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I SUMMARY TABLES AND FIGURES
SECOND QUARTER 1999
DOWNGRADIENT AREA
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Table 1
Second Quarter 1999
Downgradient Area Monitoring Results
Geigy Chemical Corporation Site
Aberdeen, North Carolina
UPPER BLACK CREEK A UIFER
Sampling Event 2Q99 2Q99 2Q99 2Q99
Sample ID MW-11D MW-18D MW-19D MW-20D
Date Collected 04/13/1999 04/15/1999 04/13/1999 04/13/1999
Pesticides (ug/L) Performance Standard
Aldrin 0.05
alpha-BHC 0.05
beta-BHC 0.05
delta-BHC 0.05
gamma-BHC (Lindane) 0.20
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin 0.1
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone 0.1
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxa hene 1.0
Notes:
Previous sampling results shown for comparison.
Detects shown in bold type.
< ,,
' I .,; '
<
<
<
<
0.5 < 0.5 <
1.8 1
6.9 4.9
1.3 0.78
0.33 J 0.7
0.5 0.5 <
0.5 0.5 <
<
<
1 <
0.28 J 0.29 J <
0.5 0.5 <
1 1 <
<
<
I 1 <
0.43 J 0.57 J <
0.5 < 0.5 <
0.5 < 0.5 <
5 < 5 <
20 < 20 <
Values exceeding downgradient groundwater performance standards indicated by shading.
0.05 <
0.037 J I 0.016 J
0.022 J
0.038 J '
0.05 <
0.05 <
0.1 <
0.1 <
0.1 <
0.1 <
0.05 <
0.1 <
0.1 <
0.1 <
0.1 <
0.1 <
0.05 <
0.05 <
0.5 <
2 <
I -Separates the qualifiers added by the laboratory from the qualifiers added as a result of the validalion process.
J -Estimated value.
NA -Not analyzed.
"' Co'nfirmatory sample
Page I of 5
0.2
0.61
0.41
0.82
0.63
0.2
0.2
0:4
0.4
0.4
0.4
0.2
0.4
0.4
0.4
0.4
0.4
0.2
0.2
2
8
-----I --
2Q99 2Q99
MW-22D MW-23D
04/13/1999 04/13/1999
< 0.2 < 0.05
0.59 0.33
0.45 0.17
0.75 0.073
0.55 0.21
< 0.2 < 0.05
< 0.2 < 0.05
< 0.4 < 0.1
< 0.4 < 0.1
< 0.4 < 0.1
< 0.4 < 0.1
< 0.2 < 0.05
< 0.4 < 0.1
< 0.4 < 0.1
< 0.4 < 0.1
< 0.4 < 0.1
< 0.4 < 0.1
< 0.2 < 0.05
< 0.2 < 0.05
< 2 < 0.5
< 8 < 2
---- - -
UPPER BLACK CREEK AQUIFER
Sampling Event
----
2Q99
Table 1
Second Quarter 1999
Downgradient Area Monitoring Results
Geigy Chemical Corporation Site
Aberdeen, North Carolina
2Q99 2Q99 2Q99
Sample ID MW-24D MW-25D MW-26D MW-30D
Date Collected 04/13/1999 04114/1999 04/13/1999 04/15/1999
Pesticides (ug/L) Performance Standard
Aldrin 0.05
alpha-BHC 0.05
beta-BHC 0.05
delta-BHC 0.05
gamma-BHC (Lindane) 0.20
alpha-Chlordane --
gamma-Chlordane --
4,4'-DDD --
4,4'-DDE --
4,4'-DDT --
Dieldrin 0.1
Endosulfan I --
Endosulfan II --
Endosulfan sulfate --
Endrin --
Endrin aldehyde --
Endrin ketone 0.1
Heptachlor --
Heptachlor epoxide --
Methoxychlor --
Toxaohcne 1.0
Notes:
Previous sampling results shown for comparison.
Detects shown in bold type.
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
0.05 < 0.05 II <
0-05 < 0.05 II
0.037 J < 0.05 II
0.01 J < 0.05 II
0.041 J < 0.05 II
0.05 < 0.05 /J <
0.05 < 0.05 II <
0.1 < 0.1 /J <
0.1 < 0.1 /J <
0.1 < 0.1 /J <
0.1 < 0.1 /J <
0.05 < 0.05 II <
0.1 < 0.1 II <
0.1 < 0.1 II <
0.1 < 0.1 II <
0.1 < 0.1 II <
0.1 < 0.1 II <
0.05 < 0.05 /J <
0.05 < 0.05 II ·<
0.5 < 0.5 /J <
2 < 2 II <
Values exceeding downgradient groundwater performance standards indicated by shading.
0.05 <
0.021 J I 0.021 J ~1;~-0.012 J ,.,
0.047 J
0.05 <
0.05 <
0.1 <
0.1 <
0.1 <
0.1
0.05 <
0.1 <
0.1 <
0.1 <
0.1 <
0.1
0.05 <
0.05 <
0.5 <
2 <
I -Separates the qualifiers added by the laboratory from the qualifiers added as a result of the validation process.
J • Estimated value.
NA -Not analyzed.
"' Confirmatory sample
Page 2 of 5
0.25
0.78
2.5
0.52
0.42
0.25
0.25
0.5
0.5
0.5
0.15
0.25
0.5
0.5
0.5
0.5
0,28
0.25
0.25
2.5
IO
-- --
2Q99 2Q99 2Q99
MW-34D MW-34D MW-35D
0411411999 0611511999' 0411211999
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 I 0.2 • 0.1 a 0.13 . 0.12
< 0.05 < 0.05 0.033 J
< 0.05 < 0.05 0,13
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
J < 0.1 < 0.1 < 0.1
< 0.05 < 0.05 < 0.05
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
J < 0.1 < 0.1 < 0.1
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.5 < 0.5 < 0.5
< 2 < 2 < 2
---- ---_, ,_ -------
Table 1
Second Quarter 1999
Geigy Chemical Corporation Site
Aberdeen, North Carolina
LOWER BLACK CREEK A UIFER
Sampling Event 2Q99 2Q99 2Q99 2Q99 2Q99 2Q99
Sample ID MW-22L MW-25L MW-27L MW-28L MW-31L MW-32L
Date Collected 04/13/1999 04/14/1999 04/15/1999 04/14/1999 04/13/1999 04/13/1999
Pesticides (ug/L) Performance Standard
Aldrin 0.05 < < 0.5 < < 0.05 < 0.5 < 0.05
alpha-BHC 0.05 4 3.7 12 0.057 3.5 < 0.05
beta-BHC 0.05 2.2 0.63 3 0.025 J 0.9 < 0.05
delta-BHC 0.05 3.5 1.2 5.7 0.D28 J 1.4 < 0.05
gamma-BHC 0.20 3.6 3.1 9.9 0.057 2.8 < 0.05
alpha-Chlordane < < 0.5 < < 0.05 < 0.5 < 0.05
gamma-Chlordane < < 0.5 < < 0.05 < 0.5 < 0.05
4,4'-DDD < 2 < < 2 < 0.1 < < 0.1
4,4"-DDE 0.1 < 2 < < 2 < 0.1 < < 0.1
4,4"-DDT < 2 < < 2 < 0.1 < < 0.1
Dieldrin < 2 < < 2 < 0.1 < < 0.1
Endosulfan I < < 0.5 < 1 < 0.05 < 0.5 < 0.05
Endosulfan 11 < 2 < 1 < 2 < 0.1 < 1 < 0.1
Endosulfan sulfate < 2 < < 2 < 0.1 < < 0.1
Endrin < 2 < < 2 < 0.1 < < 0.1
Endrin aldehyde < 2 < < 2 < 0.1 < < 0.1
Endrin ketone 0.1 < 2 < 1 < 2 < 0.1 < 1 < 0.1
Heptachlor < 1 < 0.5 < < 0.05 < 0.5 < 0.05
Heptachlor epoxide < < 0.5 < < 0.05 < 0.5 < 0.05
Methoxychlor < 10 < 5 < 10 < 0.5 < 5 < 0.5
Toxa hene 1.0 < 40 < 20 < 40 < 2 < 20 < 2
Notes:
Detects shown in bold type.
Values exceeding downgradient groundwater performance standards indicated by shading.
J -Estimated value.
NA -Not analyzed.
Page 3 of 5
----- --- --_, - - ---liiil liiil -
Table 1
Second Quarter 1999
Geigy Chemical Corporation Site
Aberdeen, North Carnlina
LOWER BLACK CREEK A UIFER
Sampling Event 2Q99 2Q99 2Q99 2Q99 2Q99 2Q99
Sample ID MW-36L MW-37L MW-38L MW-39L MW-40L PZ-2
Date Collected 04/14/1999 04/14/1999 04/13/1999 04/13/1999 04/14/1999 04/15/1999
Pesticides (ug/L) Performance Standard
Aldrin 0.05 < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
alpha-BHC 0.05 < 0.05 1.7 < 0.05 < 0.05 2 0.91
beta-BHC 0.05 < 0.05 0.24 J < 0.05 < 0.05 0.26 J 0.25
delta-BHC 0.05 < 0.05 0.55 < 0.05 < 0.05 0.52 0.38
gamma-BHC 0.20 < 0.05 1.3 < 0.05 < 0.05 1.6 0.8
alpha-Chlordane < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
gamma-Chlordane < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
4,4'-DDD < 0.1 < l < 0.1 < 0.1 < l < 0.4
4,4'-DDE 0.1 < 0.1 < < 0.1 < 0.1 < < 0.4
4,4'-DDT < 0.1 < < 0.1 < 0.1 < < 0.4
Dieldrin < 0.1 < 0.054 J < 0.1 < < 0.4
Endosulfan I < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
Endosulfan ll < 0.1 < I < 0.1 < 0.1 < I < 0.4
Endosulfan sulfate < 0.1 < < 0.1 < 0.1 < < 0.4
Endrin < 0.1 < < 0.1 < 0.1 < < 0.4
Endrin aldehyde < 0.1 < < 0.1 < 0.1 < I < 0.4
Endrin ketone 0.1 < 0.1 < I < 0.1 < 0.1 < I < 0.4
1-Ieptachlor < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
Heptachlor epoxide < 0.05 < 0.5 < 0.05 < 0.05 < 0.5 < 0.2
Meth9xychlor < 0.5 < 5 < 0.5 < 0.5 < 5 < 2
Toxa hene 1.0 < 2 < 20 < 2 < 2 < 20 < 8
Notes:
Detects shown in bold type.
Values exceeding downgradient groundwater perfonnance standards indicated by shading.
J -Estimated value.
NA -Not analyzed.
Page4of5
. , ·. -------_..:... ----- -----·
Table I
Second Quarler 1999
Geigy Chemical Corporation Sile
Aberdeen, North Carolina
LOWER BLACK CREEK AOUIFER
Sampling Event 2Q99
Sample ID PZ-3
Date Collected 04/15/1999
Pesticides (ug/L) Performance Standard
Aldrin 0.05 < 0.05
alpha-BHC 0.05 II' 0.43
beta-BHC 0.05 0.091
delta-BBC 0.05 ~-~ 0.15
gamma-BBC 0.20 . 0.38
alpha-Chlordane --< 0.05
gamma-Chlordane --< 0.05
4,4'-DDD --< 0.1
4,4'-DDE 0.1 < 0.1
4.4'-DDT --< 0.1
Dieldrin --< 0.1
Endosulfan I --< 0.05
Endosulfan II --< 0.1
Endosulfan sulfate --< 0.1
Endrin --< 0.1
Endrin aldehyde --< 0.1
Endrin ketone 0.1 < 0.1
Heptachlor --< 0.05
Hcptachlor epoxidc --< 0.05
Methoxychlor --< 0.5
Toxanhene 1.0 < 2
Notes:
Detects shown in bold type.
-
2Q99
PZ-5
04/15/1999
< 0.05
0.048
0.046
< 0.05
0.12
< 0.05
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.05
< 0.5
< 2
Values exceeding downgradient groundwater performance standards indicated by shading.
J -Estimated value.
NA -Not analyzed.
Page 5 of5
------
J
J
----- -
SURFACE WATER
Sampling Event 2Q99
Sample ID SW--01
-- ---
Table 2
Second Quarter 1999
Downgradient Area Monitoring Results
Geigy Chemical Corporation Site
Aberdeen, i''orth Carolina
MacFarland's Branch
2Q99 2Q99 2Q99
SW--02 SW-03 SW-04
-
Date Collected 04/12/1999 0411211999 04/12/1999 04/12/1999
Pesticides (ug/L)
alpha-BHC < 0.05
beta-BHC < 0.05
delta-BHC < 0.05
gamma-BHC (Lindane) < 0.05
alpha.Chlordane NA
gamma-Chlordane NA
4,4'-DDD NA
4,4'-DDE NA
4,4'-DDT NA
Dieldrin NA
Endosulfan I NA
Endosulfan II NA
Endosulfan sulfate NA
Endrin NA
Endrin aldehyde NA
Endrin ketone NA
Heptachlor < 0.05
Heptachlor epoxide < 0.05
Methoxychlor NA
Toxanhene NA
Noles:
Previous sampling results shown for comparison.
Detects shown in bold type.
0.032 J 0.032 J <
0.067 0.050
0.075 0.051
0.031 J 0.021 J <
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
< 0.05 < 0.05 <
< 0.05 < 0.05 <
NA NA
NA NA
/. Separates the qualifiers added by 1he laboratory from the qualifiers added as a result of the validation process.
J • Estimated value.
NA · Not analyzed.
*•Confirmatory Sample
Page 1 of2
0.05
0.021 J
0.019 J
0.05
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
0.05
0.05
NA
NA
------
Abei-deen Creek
2Q99 2Q99 2Q99
SW--05 SW--06 SW--06
04/12/1999 04/12/1999 06/15/1999•
< 0.05 < 0.05 IR < 0.056
0.02 J < 0.05 IR 0.013 J
0.02 J < 0.05 IR 0.012 J
< 0.05 < . 0.05 IR < 0.056
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
NA NA NA
< 0.05 < 0.05 IR < 0.056
< 0.05 < 0.05 IR < 0.056
NA NA NA
NA NA NA
-- -- - ---
SURFACE WATER
Sampling Ennt
Sample ID
Date Collected
Pesticides (ug/L)
alpha-BHC <
beta-BHC
delta-BHC
gamma-BHC (Lindane) <
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
lleptachlor <
lteptachlor epoxide <
Methoxych\or
Toxanhene
Notes:
---
Table 2
Second Quarter 1999
Downgradient Area Monitodng Resulls
Geigy Chemical Corporation Site
Aberdeen, North Carolina
Aberdeen Creek
2Q999 2Q99
SW--07 SW--08
04/12/1999 04/12/1999
0.05 < 0.05
0.019 J 0.021 J
0.02 J 0.021 J
0.05 < 0.05
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
0.05 < 0.05
0.05 < 0.05
NA NA
NA NA
Previous sampling results shm\'Tl for comparison.
Detects shown in bold type.
- - -
Rav's Mill Creek
2Q99 2Q99
SW--09 SW-10
04/12/1999 04/12/1999
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
NA NA
< 0.05 < 0.05
< 0.05 < 0.05
NA NA
NA NA
/ -Separates the qualifiers added by the laboratory from the qualifiers added as a result of the \·alidation process.
J -Estimated value.
NA -N"ot analyzed.
Page 2 of2
--· --
- - --
L-lworlclconcept/202127ffable 3&A.xl.r
-- -- -- -- -TABLE3
F.STThlATED MAXIMUM CONCENTRATION TRENDS IN GROUNDWATER OVER TL\1E
UPPER BLACK CREEK AQUIFER
GEIGY CHEMICAL CORPORATION SITE
ABERDEEN, NORTH CAROLINA
- -
O Years1 4 Years 10 Years 20 Years 30 Ym,J
Alpha BBC
l.5 year Half-Life & Retardation Factor = 8 ' 2.8 0.31 <O.0l <0.05 <0.05
No Degradation & No Retardation 3 2.8 l.39 0.67 0.07 <.0.05
l year Half-Life & Retardation Factor = 8 4 2.8 1.13 0.46 0.10 <ll.05
10 year Half-Life & Retardation Factor= 12 5 2.8 1.52 0.96 0.44 0.21
Beta BHC
1.5 year Half-Life & Retardation Factor = 8 2 l.0 0.l6 <0.05 <0,05 <0.05
No Degradation & No Retardation 3 l.0 2.13 0.92 0.11 <O.0l
l year Half-Life & Retardation Factor = 8 4 l.0 2.01 0.80 0.17 <0.05
10 year Half-Life & Retardation Factor= 12 5 l.0 2.86 1.66 0.77 0.35
Delta BBC
1.5 year Half-Life & Retardation Factor = 12 2 4.2 0.47 <0.05 <O.0l <0.05
No Degradation & No Retardation 3 4.2 1.99 0.93 0.12 <0.05
l year llalf-Life & Retardation Factor = 12 ' 4.2 1.72 0.72 0.17 <0.05
10 year Half-Life & Retardation Factor = 20 5 4.2. 2.30 l.47 0.70 0.33
Gamma BBC
1.5 year Half-Life & Retardation Factor = 5.3 2 2.8 0.30 <ll.20 <0.20 <0.20
No Degradation & No Retardation 3 2.8 1.44 . 0.71 <0.20 <ll.20
l year Half-Life & Retardation Factor = 5.3 4 2.8 l.ll 0.44 <:0.20 <:0.20
10 year Half-Life & Retardation Factor = 8.4 5 2.8 1.50 0.93 0.42 <0.20
Notes:
I. Based an August 1995 sampling event. ~-la1dmum concentration measured in MW-11D (alpha, delta, and gamma-BHC) and MW-181
2. Simulation results rcpreselll average adsorption properties and calculated half lives.
3. Simulation results represent bascline conditions requested by EPA during 5/14/96 meeting.
4. Simulation results-represent average adsorptiou properties and sensitivity analysis of half lives ( +200 percent).
5. Simulation results rcpresent slowest anticipated concentration decrease with time (sensitivity analysis of adsorption ( +50-60 percent) a
Retardation factors vary due to chemical-specific partition coefficients and range in fa;: values.
Pagel ofl
----
January 1999
... ·---- --- --- ----
TABLE4
ESTIMATED MAXIMUM CON CENT RATION TRENDS IN GROUNDWATER OVER TIME
LOWER BLACK CREEK AQUIFER
GEIGY CHEMICAL CORPORATION SITE
ABERDEEN, NORTH CAROLINA
O Years ' 4 Years IO Years 20 Years
Alpha BHC
1.5 year-Half-Life & Retardation Factor = 5.:f 6.0 0.79 <0.05 <0.05
No Degradation & No Retardation 3 6.0 3.33 1.70 0.43
5 year Half-Life & Retardation Factor = 5.T 6.0 2.89 1.062 0.21
10 year Half-Life & Retardation Factor = 6.Y 6.0 3.88 2.21 0.89
Beta BHC
1.5 year Half-Life & Retardation Factor = 5.i 2.10 0.25 <0.05 <0.05
No Degradation & No Retardation 3 2.10 0.99 0.58 0.25
5 year Half-Life & Retardation Factor = 5.3' 2.10 0.94 0.35 0.06
10 year Half-Life & Retardation Factor = 6.f 2.10 1.26 0.73 0.27
DeltaBHC
1.5 year Half-Life & Retardation Factor = 'i-4.90 0.59 <0.05 <0.05
No Degradation & No Retardation 3 4.90 2.44 1.37 0.43
5 year Half-Life & Retardation Factor = 8 4 4.90 2.18 0.85 0.18
10 year Half-Life & Retardation Factor = IO~ 4.90 2.91 1.75 0.75
GammaBHC
1.5 year Half-Life & Retardation Factor = 3.s2 5.0 0.57 <0.20 <0.20
No Degradation & No Retardation 3 5.0 2.88 1.61 0.41
5 year Half-Life & Retardation Factor ::;:; 3.£' 5.0 2.088 0.81 0.16
10 year Half-Life & Retardation Factor = 4.55 5.0 2.83 1.66 0.68
Notes:
1. Based on August 1995 and June 1996 sampling events. Maximum concentration measured in MW-27L.
2. Simulation results represent average adsorption properties and calculated half lives.
3. Simulation results represent bas_eline conditions requested by EPA during 5/14/96 meeting.
4. Simulation results represent average adsorption properties and sensitivity analysis of half lives (+200 percent).
--
30 Years
<0.05
<0.05
<0.05
0.37
<0.05
·0.06
<0.05
0.11
<0.05
0.080
<0.05
0.33
<0.20
<0.20
<0.20
0.28
5. Simulation results represent slowest anticipated concentration decrease with time (sensitivity analysis of adsorption (+50-60 percent) and half liv-
Retardation factors vary due to chemical-specific partition coefficients and range in l;,c; values.
L-lworklconcepr/202127/fable 3&4.xls Page I of/
-- -
January /999
~
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i I
j I
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I ,-
~
rm~
/V
' .,
.rv
/V
0
Legend
Pond
Swamp
Paved Roads
lhlpaved Ro.ta
Reilroada
Stromn
Monitoring Well
)ii~(li:tt:kil \;;]~;ti~ ·:~t~~B~~~
• <" • A '
'0.2 ..
·0.12 ·"MW=.-.;;· 2;..4..;;D_--'--'-Conc. ug/L': ,
alpha-,' 0.05
alpha-BHC 1.8
, beta-BHC 8.9
delta-BHC 1.3 '•
,gamma-:BHC (Lindane) · 0.33 '.' J = ·
·,Dieldrin ·,0.2&:· ·:J:
Endrin ketone • . 0.43' .J =
alpha-BHC '
beta-BHC
,:,:
. • .... ,~· ••• ,_ .. ~'\• ,<_'_ ~ -1.,,• .. ,,;.,,,,, ·.':~ ,J.'-·~-~-~--'l;\''{•f<,;<~t•\0 .,:'.· i:-:·';'1~-~/.1)._;l;'.·.•;v, :,; ;t·,\:~i\·: \,•:.. ~~··,:.,,· '-.\11 ',,''-• gamma-BHC(Lindane) 0.041 J. -;:·" ,J..(tr :.-:, gamma-BHC(Lindane) 021 .. ,;_\', ~-":',..,T; 1J
J ,);,t~)i~i{;:titt'.~:i·i}:it)ij&{,f '\~ti"lJEitt~~j{f)}}f:i::;., {::,.,,::;,:'.·{.s:;)~~{~~:{:iii/l·)l:~}r~:y:·;~'..::;.::\{(i;'.,~f~~,~~}j·~'~:'~?'.\{~}1~:Z-~::~~;:Ctl:;::~r:[,~)~;~~Jl
•• ..,,,,_,. ... < "'•••~--'• "'"' .-1~_.,. •-•-••A•...,__....,...,•'•""" ~·-•,:-.-A-,-•.-'i.~~-' .,__ ,__ ~•---.:t.!.\:=,__:_..,_ .. ,:.,_...., -..... ~ -~-w .. ,_.i,. .... ~•;:;. ~s..1:i..'.'.--~'oii:!rr, .;,;lU,').1><>.¢• O ..-,\,,.a:J..:,_ ... -1..,"-i..:..., ..... ~-....lt--•,_h,."),.,C".,,.:J,-""-4-........ ~~-... ,........,,~-----""' -•-~~-k.,_..v_ --"
Analytical Flags
"J" -Estimated Value
• Sample was collected twice. Sample collected on
4114199 contained 0.1 ug/L beta -BHC only.
Confirmation sample collected on 6/16199 contained 0.13 ug/L beta -BHC only.
0
THE PINNACLE CONSULTING GROUP
14
0 800
SCALE IN FEET
1 2
SCALE IN MILES
1600
34
13-0CT-1999
FIGURE 1
DOWNGRADIENT REMEDIAL ACTION
FIFTH EVENT, SECOND QUARTER 1999
UPPER BLACK CREEK AQUIFER MONITORING RESULTS
GEIGY CHEMICAL CORPORATION SITE
ABERDEEN NORTH CAROLINA
D
8
I
I
I . Noli-Detect ·
I .MW-38L'
. OiE!ldrin
I
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I N
I
I Legend
I 1)'£)¼!ll Pond
r:1ri1i Swamp
I /V Paved Roads
, ,, Unpaved Roads
JV Railroads
I /V Stream
@ US EPA
Monitoring Well/Piezometer
I m Monitoring Well
~~
MW-39i.-
alpha0BHC
beta'BHC .
. gam~~BH~· ·
Analytical Flags
"J" -Estimated Value
.0.048. i
0.048 ,J
0.12.'
~~nii-.u~L
'•'2 · . o.is J
'.0,62 J,8,
0
• THE PINNACLE CONSULTING GROUP
800
1 4
0 800
SCA LE IN FEET
1 2
SCALE IN MILES
1800
34
13-0CT-1999
FIGURE2
DOWNGRADIENT REMEDIAL ACTION
FIFTH EVENT, SECOND QUARTER 1999
LOWER BLACK CREEK AQUIFER MONITORING RESULTS
GEIGY CHEMICAL CORPORATION SITE
ABEROEEN NORTH CAROLINA
B
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A I
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!Er:li:ll
l,..~]::;Jl
/V
7Y'
/V
0
Pond
Swamp
·SW-08
:beta-BHC
delta-BHC'
,beto·BHC.
: delta-BHC.
·sw-oe·~
beto·BHC delta-BHC
.·.sw,os
beio-BHC
. d.eltit-BHC .
Legend
Paved Roads
Unpaved Roads
Railroads
Stream
0.013 ·j. 0.012 ;J. ·
~~O~c.'ug,L:
' \ 0.02 ~ ·
0.02· J •
Surface Water Sampling Location
Unite are ug/kg for soil and mg/L for water
Analytical Flags
"J" -Estimated Value
olpho'BHC ·
beto-BHC
delta-BHi::
. ga~riaa-:BHC ·, '
; 0:032 :J.· :·-.. o.os·,_ ·
'0.061'
0:021. J' .
• Sample was recollected on 6/15/99. First ..
sample data was unusable due to the 1_na~1hty
to analyze the sample and meet QC cntena.
0
~
Cone, ug/L
OJ)32 J
THE PINNACLE CONSULTING GROUP
800
1 4
0 800
SCALE IN FEET
1 2
SCALE IN MILES
FIGURE3
1800
34
13-OCT-1999
DOWNGRADIENT REMEDIAL ACTION
FIFTH EVENT, SECOND QUARTER 1999
SURFACE WATER/ SEDIMENT MONITORING RESULTS
GEIGY CHEMICAL CORPORATION SITE
ABERDEEN NORTH CAROLINA
I
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•
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g
a
UPPER BLACK CREEK AQUIFER
GROUNDWATER MONITORING RESULTS
SECOND QUARTER 1999
DOWNGRADIENT AREA
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Lot-Sample# ... : G9Dl40220-010
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch, ... : 9106302
RUST E & I
Client Sample ID: MW-110
GC Semivolatiles
Work Order # ..• : CTLE2101
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
{!Puanterra
Matrix ......... : WATER
Dilution Factor: 10 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND 0.50
alpba-BHC 1.8 Q 0.50
beta-BHC 6.9 0.50
delta-BHC 1.3 0.50
gamma-BHC (Lindane) 0.33 J 0.50
alpha-Chlordane ND 0.50
gamma-Chlordane ND 0.50
4,4'-DDD ND 1. 0
4,4'-DDE ND 1.0
4,4'-DDT ND 1.0
Dieldrin 0.28 J 1.0
Endosulfan I ND 0.50
Endosulfan II ND 1.0
Endosulfan sulfate ND 1.0
Endrin ND 1. 0
Endrin aldehyde ND l: 0
Endrin ketone 0.43 J 1.0
Heptachlor ND 0.50
Heptachlor epoxide ND 0.50
Methoxychlor ND 5.0
Toxaphene ND 20
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 0.0 SRD (47 -119)
Decachlorobiphenyl 0.0 SRD (10 -146)
NOTE(S):
SRO The nrrog.111e recovery was not calcuJ.accd because the CMraCt was diluted beyond the ability to quantitate a recovery.
Q Elevated reporting limit The repo~ limit i:1 elevated due to high analytc levels.
J Estimated remit. Result is less than RL
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
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Lot-Sampl.e # •.• : G9D170137-005
Date Sampled ... : 04/15/99
Prep Date ...... : 04/20/99
Prep Batch # ..• : 9110328
ROST B & I
Cl.ient Sample ID: MW-l.8D
GC Semivolatiles
Work Order# ... : CTQ2Rl01
Date Received .. : 04/16/99
Analysis Date .. : 04 ;2a/99
~)' ~uanterra
Matrix ......... : WATER
Dilution Factor: 10 Method ......... : SW846 8081A
PARAMETER
Aldrin
al.pha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -DDD
4, 4' -DDE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE (S) :
RESULT
ND Q
1.0
4.9
0.78
0.70
ND
ND
ND
ND
ND
0.29 J
ND
ND
ND
ND
ND
0.57 J
ND
ND
ND
ND
PERCENT
RECOVERY
64
101
Q Elcvntcd reporting limiL The rcponing limit is ~lcvatcd due to high analyte levels.
J futimatcd rculL Result is kss than RL
REPORTING
LIMIT UNITS
0.50 ug/L
0.50 ug/L
0.50 ug/L
0.50 ug/L
0.50 ug/L
0.50 ug/L
0.50 ug/L
1.0 ug/L
1.0 ug/L
1.0 ug/L
1.0 ug/L
0.50 ug/L
1.0 ug/L
1.,0 ug/L
1.0 ug/L
1.0 ug/L
1.0 ug/L
0.50 ug/L
0.50 ug/L
5.0 ug/L
20 ug/L
RECOVERY
LIMITS
(47 -119)
(10 -146)
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Lot-Sample# ... : G9Dl40220-012
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106302
Dilution Factor: 1
PARAMETER
Aldrin
alpba-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha -Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTK(S) ·:
J &timated rcsulL Result i.s less than RL
RUSTK&I
Client Sample ID: MW-19D
GC Semivolatiles
Work Order # ... : CTLE5 l O 1
Date Received .. : 04/14/99
Analysis Date .. : 04/30./99
(/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.037 J 0.050 ug/L
0.016 J 0.050 ug/L
0.022 J 0.050 ug/i..
0. 038 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0. 10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0:10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
78 (47 -119)
88 (10 -146)
u
u
0
0
D
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Lot-Sample II ... : G9Dl40220-005
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch # .•. : 9106302
Diluticm Factor: 4
PARAMETER
Aldrin
alpba-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4 1 -D_DE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUST E I. I
Client Sample ID: Mli'-20D
GC Semivolatiles
Work Order II ... : CTLDPl0l
Date Received .. : 04/14/99 .
Analysis Date .. : 04/30/99
(}Puanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
0.61 Q 0.20 ug/L
0.41 0.20 ug/L
0.82 0.20 ug/L
0.63 0.20 ug/L.
ND 0.20 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0. 40 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0. 40 ug/L
ND 0.40 ug/L
ND 0.20 ug/L
ND 0. 20 ug/L
ND 2.0 ug/L
ND 8.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
77 (47 -119)
95 I 10 -146)
I NOTE(S):
Q Elevated reporting limit. The r;q,onini: limh is clcvatcd due to high analytc levels.
I
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u
0
0
H
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Lot-Sample# ... : G9Dl40220-013
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch # ... : 9106302
Dilution Factor: 4
PARAMETER
Aldrin
alpba-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4 '-DDD
4,4'-DPE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
RUSTE&I
Client Sample ID: MW-22D
GC Semivolatiles
Work Order # ... : CTLE7101
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
~uanterra
Matrix ......... : WATER
Method ......... : .SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
0.59 Q 0.20 ug/L
0.45 0.20 ug/L
0.75 0.20 ug/L
0.55 0.20 ug/L
ND 0.20 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0. 40 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.20 ug/L
ND 0.20 ug/L
ND 2.0 ug/L
ND 8.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
92 (4 7 -119)
87 (10 -146)
Q Blevatcd reponine: limit. The rq,orting limit is clcvatcd due to hi~ analytc levels.
I
I
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D
u
D
H
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Lot-Sample# ... : G9Dl40220-002
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106302
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (T.indane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosul fan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUST E & I
Client Sample ID: MW-23D
GC Semivolatiles
Work Order # ... : CTLDEl0l
Date Received .. : 04/14/99
Analysis Date .. : 04/29/99
'Jeuanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.33 0.050 ug/L
0.17 0.050 ug/L
0.073 0.050 ug/L
0.21 0.050 ug/L
ND 0.050 ug/L
ND 0. 050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0. 050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND o·: 10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
69 (47 -119)
101 ( 10 -146)
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D
D
u
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wt-Sample# ... : G9D140220-004
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106302
Dilution Factor: 1
PARAMETER
Aldrin
alpba-BHC
beta-BHC
delta-BHC
ganma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4' -DOD
4,4 '-DDE
4,4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
I Eso:awat result. Rcsn1t is less than RL
RUST E & I
Client Sample ID: MW-24D
GC Semivolatiles
Work Order # ... : CTLDKl O 1
Date Received .. : 04/14/99
Analysis Date .. : 04/29/99
(/euanferra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.050 0.050 ug/L
0. 037 J 0.050 ug/L
0. 010 J 0.050 ug/L
0.041 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0:10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
66 (47 -119)
101 (10 -146)
D
0
D
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl50233-004
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch, ... : 9109476
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4' -DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
I Tetrachloro-m-xylene
Decachlorobiphenyl
I NOTE(S):
• Surropte recovery is ouuide stated control limits.
I
I
I
I
I
RUST E &. I
Client Sample ID: MW-25D
GC Semivolatiles
Wo:dc Order It ... : CTN76101
Date Received .. : 04/15/99
Analysis Date .. : 04/27/99
~)\ -,euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
43 * (47 -119)
11 (10 -146)
I
I
I
I
I
I
I
I
H
I
Lot-Sample# ... : G9Dl40220-008
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106302
Dilution Factor: l
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4 '-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone n Heptachlor
Heptachlor epoxide
Methoxychlor
d Toxaphene
SURROGATE n Tetrachloro-m-xylene
Decachlorobiphenyl
n
H
g
I
I
I
NOTE(S):
J Estinwod rcsuh. Rcsnlt is less than RL
RUSTE&I
Client Sample ID: MW-26D
GC Semivolatiles
Work Order # ..• : CTLDW101
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
lj)\ ~uanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.021 J 0.050 ug/L
0.021 J 0.050 ug/L
0.012 J 0.050 ug/L
0.047 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0:10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
80 (47 -119)
86 (10 -146)
I
I
I
I
,I
I
I
I'
I
I
I
I
I
I
I
i
~uanterra
RUST ll & I
Client Sample ID: Mli-30D
GC Semivolatiles
Lot-Sample it ..• : G9Dl70137-003 Work Order it ... : CTQ2Pl01 Matrix ......... : WATER Date Sampled ... : 04/15/99 Date Received. _ : 04/16/99
Prep Date ...... : 04/20/99 Analysis Date .. : 04/29/99
Prep Batch it ... : 9110328
Dilution Factor: 5 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT UNITS
Aldrin ND 0.25 ug/L
alpha-BHC 0.78 0.25 ug/L
beta-BHC 2.5 Q 0.25 ug/L
delta-BHC 0.52 0.25 ug/L
gamma-BHC (Lindane) 0.42 0.25 ug/L
alpha•Chlordane ND 0.25 ug/L
gamma-Chlordane ND .0.25 ug/L
4,4'-DDD ND 0.50 ug/L
4, 4' ·DDE ND 0.50 ug/L
4,4 1 -DOT ND 0.50 ug/L
Dieldrin 0.15 J 0.50 ug/L
Endosulfan I ND 0.25 ug/L
Endosulfan II ND 0.50 ug/L
Endosulfan sulfate ND 0.50 ug/L
Bndrin ND 0.50 ug/L
Endrin aldehyde ND 0~50 ug/L
Endrin ketone 0.28 J 0.50 ug/L
Heptachlor ND 0.25 ug/L
Heptachlor epoxide ND 0.25 ug/L
Methoxychlor ND 2.5 ug/L
Toxaphene ND 10 ug/L
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 51 (47 -119)
Decachlorobiphenyl 71 (10 -146)
NOTE (S) :
Q Elevated reporting limit. The reporting limit is elevated due to high anaJyte levels.
J Estimat.cd mult. Result is less than RL
I
I
I
I
I
I
I
,I
I
,I
I
I
I
i
I
I
I
I
I
Lot-Sample# ... : G9Dl50233-007
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch# ... : 9109476
Dilution Factor: l
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUSTE&I
Client Sample ID: MW-34D
GC Semivolatiles
Work Order # ... : CTN? Al O 1
Date Received .. : 04/15/99
Analysis Date .. : 04/21/99
(/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
0.10 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND o·: 10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
80 (47 -119)
59 (10 -146)
I
I
I
I
.I
I
1l
I
I
1·
I
Amended
Lot-Sample# ... : G9F160238-001
Date Sampled ... : 06/15/99
Prep Date ...... : 06/21/99
Prep Batch # ••• : 9172421
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -DOD
4, 4' -DOE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Decachlorobiphenyl
Tetrachloro-m-xylene
Quanterra
EARTH TRCII B&I
Client Sample ID: MW-34D
GC Semivolatiles
Work Order# ... : CX0LA101 Matrix ......... : WATER
Date Received .. : 06/16/99
Analysis Date .. : 07 /13/99
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
0.13 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0:10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
106 (10 -146)
88 (47 . 119)
I
I
I
I'
·I
I
I
,g,
ii
·b
I
I
I
I
Lot-Sample# ... , G9Dl30221-012
Date Sampled ... , 04/12/99
Prep Date ...... , 04/16/99
Prep Batch # ... ' 9106241
Dilution Factor, l
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (r.;naawe)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4, 4' -DDE
4,4 1-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NO'l'E(S),
J Eltimated resa.k. Result is less tho RL
RUSTE&I
Client Sample ID, MW-35D
GC Semivolatiles
work Order# ... , CTKAEl0l
Date Received .. , 04/13/99
Analysis Date .. , 04/27 /99
Quanterra
Matrix ......... , WATER
Method ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.20 0.050 ug/L
0.12 0.050 ug/L
0.033 J 0.050 ug/L
0.13 0.050 ug/L
ND 0.050 ug/L
ND 0,050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0,10 ug/L
ND 0.050 ug/L
ND 0,10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND o·.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
88 (47 -119)
71 (10 -146)
I
I
I
I
I
I
I
I
I'
., 1.
I
i ,,
I
I
!I
I
I
d (J
LOWER BLACK CREEK AQUIFER
GROUNDWATER MONITORING RES UL TS
SECOND QUARTER 1999
DOWNGRADIENT AREA
I
I
I
I
I
I
I
I
I
I
Lot-Sample fl ... : G9Dl40220-0ll
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch # ... : 9106302
RUST E & I
Client Sample ID: MW-22L
GC Semivolatiles
Work Order fl ... : CTLE4101
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
(}Puanterra
Matrix ......... : WATER
Dilution Factor: 20 Method ......... : SW846 8081A ·
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND 1.0
alpha-BHC 4.0 Q 1.0
beta-BHC 2.2 1.0
delta-BHC 3.5 1.0
gamma-BHC (Lindane) 3.6 1.0
alpha-Chlordane ND 1.0
gamma-Chlordane ND 1.0
4,4'-DDD ND 2.0
4,4'-[?DE ND 2.0
4,4'-DDT ND 2.0
Dieldrin ND 2.0
Endosulfan I ND 1.0
Endosulfan II ND 2.0
Endosulfan sulfate ND 2.0
Endrin ND 2.0
Endr.in aldehyde ND 2 .. 0
Endrin ketone ND 2.0
Heptachlor ND 1.0
Heptachlor epoxide ND 1.0
Methoxychlor ND 10
Toxaphene ND 40
PERCENT RECOVERY SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 0.0 SRO (4 7 -119)
Decachlorobiphenyl 0.0 SRD (10 -146)
NOTE(S):
SRO The surroptc recovery was not ca1culatcd because the extract was diluted beyond the ability to qu.antitatc • rccovay.
Q Elevated reporting: lhnit. The reporting lim.Jt is elevated due to high analytc levels.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
I
I
I
I
I
I
·W·
·I
I
I
I
I
I
I
Lot-Sample I ... : G9D150233-003
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch# ... : 9109476
RUSTE&I
Client Sample ID: MW-25L
GC Semivolatiles
Work Order I ... : CTN74101
Date Received .. : 04/15/99
Analysis Date .. : 04/29/99
IJ!uanterra
Matrix ......... : WATER
Dilution Factor: 10 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND Q 0.50
alpha-BHC 3.7 0.50
beta-BHC 0.63 0.50
delta-BHC 1.2 0.50
gamma-BHC (Lindane) 3.1 0.50
alpha-Chlordane ND 0,50
gamma-Chlordane ND 0.50
4,4'-DDD ND 1. 0
4,4'-DDE ND 1.0
4,4'-DDT ND 1.0
Dieldrin ND 1.0
Endosulfan I ND 0.50
Endosulfan II ND 1.0
Endosulfan sulfate ND 1.0
Endrin ND 1.0
Endrin aldehyde ND i.·o
Endrin ketone ND 1.0
Heptachlor ND a.so
Heptachlor epoxide ND 0.50
Methoxychlor ND 5.0
Toxaphene ND 20
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 0.0 SRD (47 -119)
Decachlorobiphenyl 0.0 SRD (10 -146)
NOTE(S):
SRD ne surroeate recovery was not caJculatcd becanse the ~tract was diluted beyond the ability to quantitatc a R:COVcry.
Q Elevated reporting lhnit. The rcportin& lhnit is devated due to hi2h analyte levels.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample ft ... : G9Dl 70137-006
Date Sampled ... : 04/15/99
Prep Date ...... : 04/20/99
Prep Batch ft ... : 9110328
Dilution Factor: 20
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gallllllil-BHC {Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -DDD
4, 4' -DDE
4, 4 '-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NCYrH (SJ :
(}l)uanterra
RUSTB&I
Client Sample ID: MW-27L
GC Semivolatiles
Work Order ft ... : CTQ2Tl01 Matrix ......... : WATER
Date Received .. : 04/16/99
Analysis Date .. : 04/29/99
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 1.0 ug/L
12 Q 1.0 ug/L
3.0 1.0 ug/L
5.7 1.0 ug/L
9.9 1.0 ug/L
ND 1. 0 ug/L
ND 1.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 1.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 2.0 ug/L
ND 1. 0 ug/L
ND 1. 0 ug/L
ND 10 ug/L
ND 40 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
63 (47 -119)
84 (10 -146)
Q Elevated reporting limit. The reporting limit i, elevated due to high analytc levels.
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl50233-002
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch, ... : 9109476
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
heta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
·Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
J &timatcd rem1t. Result is less than RL
RUST E & I
Client Sample ID: MW-2BL
GC Semivolatiles
Work Order IJ. .. : CTN72101
Date Received .. : 04/15/99
Analysis Date .. : 04/27/99
Quanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.057 0.050 ug/L
0.025 J 0.050 ug/L
0.028 J 0.050 ug/L
0.057 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0 .. 10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND o:so ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
75 (47 -119)
39 (10 -146)
I
I
I
I
I
I
I
I
I
.I
I
I
I
0
u
I
I
I
I
Lot-Sample II ... , G9Dl40220-006
Date Sampled ... , 04/13/99
Prep Date ...... , 04/16/99
Prep Batch II ... : 9106302
RUSTE&I
Client Sample ID, MW-31L
GC Semivolatiles
Work Order II ... , CTLDQl0l
Date Received .. , 04/14/99
Analysis Date .. , 04/30/99
{!puanterra
Matrix ......... : WATER
Dilution Factor: 10 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND 0.50
alpha-BHC 3.5 Q 0.50
beta-BHC 0.90 0.50
delta-BHC 1.4 0.50
garmna-BHC (Lindane) 2.8 0.50
alpha-Chlordane ND 0.50
gamma-Chlordane ND a.so
4,4'-DDD ND 1. 0
4, 4 1 -DDE ND 1.0
4,4'-DDT ND 1.0
Dieldrin ND 1.0
Endosulfan I ND a.so
Endosulfan II ND 1.0
Endosulfan sulfate ND 1.0
Endrin ND 1.0
Endrin aldehyde ND 1.0
Endrin ketone ND 1. 0
Heptachlor ND a.so
Heptachlor epoxide ND a.so
Methoxychlor ND 5.0
Toxaphene ND 20
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 0.0 SRD (47 -119)
Decachlorobiphenyl 0.0 SRD (10 -146)
NOTE(S):
SRD n1c surro&;atc recovery was no1 c:alcalated because the CAtnlCI: wa.s diluted beyond the ability to quantir.atc • recovery.
Q Elevated n:portm&: Limit. The reporting limit ls elevated due to hi~ analyte levels.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample # ... : G9Dl40220-007
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch ' ... : 9106302
RUSTE&I
Client Sample ID: MW-31L-A
GC Semivolatiles
Werle Order # ... : CTLDT101
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
{lpuanterra
Matrix ......... : WATER
Dilution Factor: 10 Method ......... : SW846 8081A
REPORTING
PARAMETER RESULT LIMIT
Aldrin ND 0.50
alpha-BHC 3.3 Q 0.50
beta-BHC 0.84 0.50
delta-BHC 1.3 0.50
gamma-BHC (Lindane) 2.7 0.50
alpha-Chlordane ND 0.50
gamma-Chlordane ND 0.50
4,4'-DDD ND 1.0
4,4'-DDE ND 1. 0
4,4'-DDT ND 1. 0
Dieldrin ND 1.0
Endosulfan I ND 0.50
Endosulfan II ND 1.0
Endosulfan sulfate ND 1.0
Endrin ND 1.0
Endrin aldehyde ND 1.0
Endrin ketone ND 1.0
Heptachlor ND 0.50
Heptachlor epoxide ND 0.50
Methoxychlor ND 5.0
Toxaphene ND 20
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Tetrachloro-m-xylene 0.0 SRD (47 -119)
Decachlorobiphenyl 0.0 SRD (10 -146)
NOTE(S):
SRO The "1mJCate recovery was not calculated because the ~ was dilated beyond the ability to quantitate a n:covcry.
Q Elevated rqxutini: limit. The rcpartini: limil: is elevated due to hidt analytc levda.
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample If. .. : G9Dl.40220-003
Date Sampled ... : 04/13/99
Prep Date ...... : 04/16/99
Prep Batch # .•. : 9106302
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUST E & I
Client Sample ID: MW-32L
GC Semivolatiles
Work Order It ... : CI'LDHlOl
Date Received .. : 04/14/99
Analysis Date .. : 04/29/99
(/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
79 (47 -119)
69 (10 -146)
I
I
B
B
B
u
B
I
I
I
•
I
I
I
I
I
I
I
I
Lot-Sample# ... , G9D150233-005
Date Sampled ... , 04/14/99
Prep Date ...... , 04/19/99
Prep Batch •... , 9109476
Dilution !'actor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -ODD
4,4'-DPE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUSTE&I
Client Sample ID, MW-36L
GC Semivolatiles
Work Order # ... , CTN77101
Date Received .. : 04/15/99
Analysis Date .. , 04/28/99
'Jeuanterra
Matrix ......... , WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/i:..
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
82 (47 -119)
50 (10 -146)
0
I
D
8
u
D
B
I
11
I
I
B
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl50233-006
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch# ... : 9109476
RUSTE&I
Client Sample ID: Mii'-37L
GC Semivolatiles
Work Order# ... : CI'N79101
Date Received .. : 04/15/99
Analysis Date .. : 04/28/99
Quanterra
Matrix ......... : WATER
Dilution Factor, 10 . Method ......... , SW846 8081A
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BBC (T.indanP.)
alpha -Chlordane
gamma-Chlordane
4,4'-DDD
4,4°-DDE
4,4 1 -DbT
Dieldrin
Endosulfan I
Endosul fan I I
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
RESULT
ND Q
1. 7
0.24 J
0.55
1.3
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
0.0 SRD
0.0 SRD
REPORTING
LIMIT
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.0
1. 0
1.0
1.0
0.50
1. 0
1.0
1.0
1.0
1.0
0.50
0.50
5.0
20
RECOVERY
LIMITS
(47 -119)
(10 -146)
SRD The stuTOgate recovery was not cak:alatcd because the extaict was diluted beyond thi: ability to quantitate a recovery.
Q Elevated reporting limit. The rcportin&: limit is elevated due to hieh analytc lcvcls.
I BSWWlted result. Result U1 less than RL
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
I
B
I
I
B
B
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... , G9Dl40220-001
Date Sampled ... , 04/13/99
· Prep Date ...... , 04/16/99
Prep Batch# ... , 9106302
Dilution Factor, 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
lilOTE (S) ,
I &tim.ated rcsall. lu:sult is 1c:ss dum RL
RUSTE&I
Client Sample ID, MW-38L
GC Semivolatiles
Work Order # ... , CTLDOlOl
Date Received .. , 04/14/99
Analysis Date .. ,. 04/30/99
(/euanterra
Matrix ......... , WATER
Method ......... , SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
0.054 J 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
69 (47 -119)
85 (10 -146)
I
I
I
I
B
I
u
I
I
I
B
g
B
8
I
I
I
I
I
Lot-Sample # ... : G9Dl40220-009
Date Sampled .. ,: 04/13/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106302
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUSTE&I
Client Sample ID: MW-39L
GC Semivolatiles
Work Order # ... : CTLE0l0l
Date Received .. : 04/14/99
Analysis Date .. : 04/30/99
{!euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
80 (47 -119)
73 (10 -146)
Lot-Sample# ... : G9D150233-001
Date Sampled ... : 04/14/99
Prep Date ...... : 04/19/99
Prep Batch # ... : 91094 76
RUSTE&I
Client Sample ID: Mii'-40L
GC Semivolatiles
Work Order# ... : CI'N70101
Date Received .. : 04/15/99
Analysis Date .. : 04/21/99
ieuanterra
Matrix ......... : WATER
I
I
I
I
B
I
I
I
I
I
I
I
Dilution Factor: 10 Method ......... : SW846 8081A
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindam•)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4,4'-Df?E
4, 4 '-DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RESULT
ND Q
2.0
0.26 J
0.52
1.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
0.0 SRO
0.0 SRO
REPORTING
LIMIT
0.50
0.50
0.50
0.50
0.50
0.50
0.50
1.0
1.0
1.0
1.0
0.50
1.0
1. 0
1.0
1.0
1.0
0.50
0.50
5.0
20
RECOVERY
LIMITS
( 4 7 -119)
(10 -146)
I NOTE(SJ:
SRD The surroi:atc recovery was not calculated becaasc the ~ w.u dihned beyond lhe ability to quntitatc a recovery.
Q Elevated reporting limit. The reporting limit is elevated due 10 hidt analyte levels.
• I Estimat<d =uh. R=lt ;, I= 1han RL
I
I
I
I
UNITS
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
I
I
I
D
D
I
I
I
I
I
I
I
I
Lot-Sample # •.• : G9Dl 70137-004
Date Sampled ... : 04/15/99
Prep Date ...... : 04/20/99
Prep Batch # .•. : 9110328
Dilution Factor: 4
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -DDD
4,4' -DDE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
(/euanterra
RUSTB&I
Client Sample ID: PZ-2
GC Semivolatiles
Work Order# ... : CTQ2Ql01 Matrix ......... : WATER
Date Received_.: 04/16/99
Analysis Date .. : 04/29/99
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
0.91 Q 0.20 ug/L
0.25 0.20 ug/L
0.38 0.20 ug/L
0.80 0.20 ug/L
ND 0.20 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.20 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.40 ug/L
ND 0.20 ug/L
ND 0.20 ug/L
ND 2.0 ug/L
ND 8.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
59 (47 -119)
91 (10 -146)
I NOTE(S):
Q Elevated reporting limiL The reporting limit is elevated due to high analytc levels,
I
I
I
I
I
I
D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl70137-001
Date Sampled ... : 04/15/99
Prep Date ...... : 04/20/99
Prep Batch# ... : 9110328
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4, 4' -DDD
4, 4' -DDE
4,4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
ROSTE&I
Client Sample ID: PZ-3
GC Semivolatiles
Work Order# ... : CTQ2Ml01
Date Received .. : 04/16/99
Analysis Date .. : 04/28/99
'Jeuanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0,050 ug/L
0.43 0.050 ug/L
0.091 0.050 ug/L
0.15 0.050 ug/L
0.38 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 6.·10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0. 050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
47 (47 -119)
92 ( 10 -146)
I
I
I
I
D
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl 70137-002
Date Sampled ... : 04/15/99
Prep Date ...... : 04/20/99
Prep Batch # ... : 9110328
Dilution Factor: 1
PARAMETER
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
4,4'-DDD
4, 4' -ODE
4, 4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
J Estimated m:ull Rcsuh is less lhan RL
(/euanterra
RUST E & I
Client Sample ID: PZ-5
GC Semivolatiles
Work Order # ... : CTQ2Nl01 Matrix ......... : WATER
Date Received .. : 04/16/99
Analysis Date .. : 04/28/99
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.048 J 0.050 ug/L
0.046 J 0.050 ug/L
ND 0.050 ug/L
0.12 0.050 ug/L
· ND 0. 050 ug/L
ND 0.050 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0 .10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.10 ug/L
ND 0.050 ug/L
ND 0. 050 ug/L
ND 0.50 ug/L
ND 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
49 (47 -119)
69 (10 -146)
D
I
I
I
I
I
D
I
I
I
I
I
I
I
I
I
I
I
I
STREAM SURFACE WATER MONITORING RESULTS
SECOND QUARTER 1999
DOWNGRADIENT AREA
I
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•
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I
n
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I
I
I
I
Lot-Sample# ... : G9D130221-006
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUSTE&I
Client Sample ID: SW-01
GC Semivolatiles
Werle Order # ... : CTKA21 o 1
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
(/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
83 (4 7 -119)
46 (10 -146)
I
I
I
I
0
0
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9Dl30221-006
Date Sampled ... : 04/12/99
ROST E & I
Client Sample ID: SW-01
General Chemistry
Work Order # .•. : CTKA2
Date Received .. : 04/13/99
{PJuanterra
Matrix ......... , WATER
··PREPARATION-PREP ~P~ARAM==E=T=E~R _______ R_E~S_UL_T __ RL _____ UN_I_T_S ___ M_E_TH_O_D ______ ANALYSIS DATE BATCH # Non-Filterable Solid ND 5.0 mg/L MCAWW 160.2 04/14/99 9104269 (Residue)
Dilution Factor: 1
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample # ... : G9D13022l-005
Date Sampled ... : 04/12/99
Prep.Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BBC
gamma-BHC (L:i:ndane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
J Estimated resnlt. Result ii Jc.ss than RL
RUST E & I
Client Sample ID: SW-02
GC Semivolatiles
Work Order # ... : CTKAl 101
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
Quanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
0.032 J 0.050 og/L
0.067 0. 050 ug/L
0.075 0.050 ug/L
0. 031 J 0.050 og/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
79 (47 -119)
55 (10 -146)
I
I
0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9D130221-005
Date Sampled ... : 04/12/99
RUST E & I
Client Sample ID: SW-02
General Chemistry
Work Order # .•. : CTKAl
Date Received .. : 04/13/99
Quanterra
Matrix ......... : WATER
PREPARATION-PREP ~PARAM==E~T~E=R"------~R~E~S~UL=T __ ~R=L ___ =UN=I=T=S ___ ~M=E=T~H=O=□------ANALYSIS DATE BATCH# Non-Filterable Solid ND 5.0 mg/L MCAWW 160.2 04/14/99 9104269 (Residue)
Dilution Factor: 1
I
I
0
I
I
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I
I
I
I
I
I
I
I
I
I
I
I
I
Lot-Sample# ... : G9D130221-003
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
bet:a-BHC
delt:a-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
I Estimated t"C$dlL Remit is less than RL.
RUST E & I
Client Sample ID: SW-03
GC Semivolatiles
Werle Order# ... : CTK9Xl01
Date Received .. : 04/13/99
lllJalysis Date .. : 04/27/99
lj'!\ ,euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
0.032 J 0.050 ug/L
0.050 0.050 ug/L
0.051 0.050 ug/L
0.021 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
83 (47 -119)
54 ( 10 -146)
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I I
Lot-Sample# ... : G9D130221·003
Date Sampled ... : 04/12/99
ROST ll & I
Client Sample ID: SW-03
General Chemistry
Work Order t ... : CTK9X
Date Received .. : 04/13/99
IJ)uanterra
Matrix ......... : WATER
PREPARATION· PREP _PARAM~~~E_T_E_R ______ "R"'E"'S'-"UL=T __ R'-'L=-----=lJN=I=T=S ___ M~E~TH=O~D~-----ANALYSIS DATE BATCH # Non-Filterable Solid ND 5.0 mg/L MCAWW 160.2 04/14/99 9104269 (Residue)
Dilution Factor: l
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D
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I
Lot-Sample# ... : G9D130221-004
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpba-BHC
beta-BBC
delta-BBC
gamma-BBC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
1 Eaimatcd n::sult. Result is less than RL
RUSTE&I
Client Sample ID: SW-03-a
GC Semivolatiles
Work Order # ... : CTKA0l0l
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
\
~uanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
0.032 J 0.050 ug/L
0.051 0.050 ug/L
0.055 0.050 ug/L
0.022 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
85 (47 -119)
54 (10 -146)
I
I
I Lot-Sample# ... : G9Dl30221-004
1 Date Sampled ... : 04/12/99
RUSTE&I
Client Sample ID: SW-03-a
General Chemistry
Work Order # ... : CTKA0
Date Received .. : 04/13/99
~~ ~uanterra
Matrix ......... : WATER
PREPARATION-PREP
~P"-'ARAM==E~T=EccR ______ ~R~E~S~UL=T~_ ~RL==----~UN=I'-'T,.,S,..__ __ M=ETH=O::cD::._ ____ _ ANALYSIS DATE
04/14/99
BATCH#
9104269 I
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Non-Filterable Solid ND 5.0 mg/L MCAWW 160.2
(Residue)
Dilution Factor: 1
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Lot-Sample# ... : G9Dl30221-001
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
I Estimated rt:mh. Result is less than RL
RUST E &. I
Client Sample ID: SW-04
GC Semivolatiles
Work Order # ..• : CTK9Vl01
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
(/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.021 J 0.050 ug/L
0.019 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
86 (4 7 -119)
63 (10 -146)
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Lot-Sample# ... : G9Dl30221-001
Date Sampled ... : 04/12/99
RDSTE&I
Client Sample ID: SW-04
General Chemistry
Work Order # .•• : CTK9V
Date Received .. : 04/13/99
~~ ~uanterra
Matrix ......... : WATER
PREPARATION-PREP
PARAMETER RESULT ===~-~RL==---0UN=I~T~S'---~M=E=TH=O=D ______ ANALYSIS DATE BATCH#
Non·Filterable Solid ND 5.0 mg/L MCAWW 160.2 04/14/99 9104269
(Residue)
Dilution Factor: 1
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Lot-Sample# ... : G9Dl30221-002
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BBC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
HOTE(S):
1 Estimated result. Rc:salt is. less than RL
RUSTE&I
Client Sample ID: SW-05
GC Semivolatiles
Work Order# ... : CTK9Wl0l
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
fPuanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.020 J 0.050 ug/L
0. 020 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
84 (47 -119)
62 (10 -146)
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Lot-Sample# ... : G9D130221-002
Date Sampled ... : 04/12/99
~P~ARAM==E~TE=R'------RESULT
Non-Filterable Solid ND
(Residue)
RUSTB&I
Client Sample ID: SW-05
General Chemistry
Work Order # .•. : CTK9W
Date Received .. : 04/13/99
RL UNITS METHOD
5.0 mg/L MCAWW 160.2
Dilution Factor: 1
(/euanterra
Matrix ......... : WATER
PREPARATION-PREP
ANALYSIS DATE BATCH#
04/14/99 9104269
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Lot-Sample# ... : G9Dl30221·007
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch, ... : 9106241
Dilution Factor:. 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
• SUrro.-:ate rcaivezy is outside staled control limits,
RUSTE&I
Client Sample ID: SW-06
GC Semivolatiles
Work Order ff ... : CTKAB l 0 1
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
,;/euanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
RESULT
ND
ND
ND
ND
ND
ND
PERCENT
RECOVERY
2.8 •
1. 3 •
REPORTING
LIMIT UNITS
0. 050 · ug/L
0.050 ug/L
0.050 ug/L
0.050 ug/L
0.050 ug/L
0.050 ug/L
RECOVERY
LIMITS
(47 · 119)
(10 · 146)
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Lot-Sample# ... : G9Dl30221-007
1 Date Sampled ... : 04/12/99
PARAMETER RESULT n Non-Filterable Solid 5.0 II (Residue)
RUST K & I
Client Sample ID: SW-06
General Chemistry
work Order # .•• : CTKAB
Date Received .. : 04/13/99
R'-'L"'---UNITS METHOD
5.0 mg/L MCAWW 160.2
Dilu~ion Factor: 1
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Quanterra
Matrix ......... : WATER
PREPARATION-PREP
ANALYSIS DATE BATCH#
04/14/99 9104269
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Quanterra
BARTH TBCII E&I ,
Client: Sample ID: SW-06
GC Semivolatiles
Lot:-Sample # ..• : G9F160238·002 Work Order # ••• : CXOLClOl ·Matrix ......... : WATER Dat:e Sampled ... : 06/15/99 Dat:e Received .. : 06/16/99
Prep Dat:e ...... : 06/21/99 Analysis Dat:e .. : 07 /13/99
Prep Bat:ch # ... : 9172421
Dilution Factor: l Method ......... : SW846 8081A
PARAMETER RESULT
alpha-BHC ND V
beta-BHC 0.013 J
delt:a-BHC 0.012 J
gamrna-BHC (Lindane) ND
Heptachlor ND
Heptachlor epoxide ND
PERCENT
SURROGATE RECOVERY
Decachlorobiphenyl 82
Tetrachloro-m-xylene 90
1110TB ( S ) :
V Elevated reporting limit. The rq,orting limit is clcv11Cd due to limited sample volnmc.
I ~ n:suJt. Result is lea 1ban RL
REPORTING
LIMIT UNITS
0.056 ug/L
0.056 ug/L
0.056 ug/L
0.056 ug/L
0.056 ug/L
0.056 ug/L
RECOVERY
LIMITS
(10 -146)
(47 . 119)
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Lot-Sample# ... : G9Fl60238-002
Date Sampled ..• : 06/15/99
BARTH TECH B&I
Client Sample ID: Slf-06
General Chemistry
Work Order # ••. : CXOLC
Date Received .. : 06/16/99
Quanterra
Matrix ......... : WATER
PREPARATION-PREP '-'PARAM==E'-'T~E~R~----~R=E=S=UL=T~_RL ~~--~UN~IT~S~ __ M __ ETH_O~D~-----ANALYSIS DATE BATCH # Non•Filterable Solid ND 5. 0 mg/L MCAWW 160 .2 06/18/99 9173410 (Residue)
Dilution Factor: 1
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Lot-Sample# ... : G9D130221-008
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch, ... : 9106241
Dilution Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BBC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
1 &timatcd n:sa.tt. Rcsnlt is less than RL
RUSf E & I
Client Sample ID: SW-07
GC Semivolatiles
Work Order IL .. : CTKA9101
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
{!Puanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0.019 J 0.050 ug/L
0.020 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
91 (47 -119)
36 (10 -146)
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Lot-Sample# ... : G9D130221·008
Date Sampled ... : 04/12/99
PARAMETER RESULT
I Non-Filterable Solid ND
(Residue)
ROSTB&I
Client Sample ID: SW-07
General Chemistry
Work order# ... : CTKA9
Date Received .. : 04/13/99
t}puanterra
Matrix ......... : WATER
:..,RL:,_ __ _,,UN=Ic.:T.:,Sc..... __ M'-'-E"-T=-'H:.cOe,Dc:._ ____ _
PREPARATION· PREP
ANALYSIS DATE BATCH #
04/14/99 9104269 5.0 mg/L MCAWW 160.2
Dilution Factor: l
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Lot-Sample# ... : G9D130221-009
Date Sampled ... : 04/12/99
Prep Date ...... : 04/16/99
Prep Batch# ... : 9106241
Diluticm Factor: 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
NOTE(S):
J Estimated result. Result i.s less than RL
RUST E &,I
Client Sample ID: Sli'-08
GC Semivolatiles
Work Order # ... : CTKAAl O 1
Date Received .. : 04/13/99
Analysis Date .. : 04/27/99
(/puanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
0. 021 J 0.050 ug/L
0.021 J 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
81 (47 -119)
37 (10 -146)
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Lot-Sample# ... : G9Dl30221-009
Date Sampled ... : 04/12/99
ROSTB&I
Client Sample ID: SW-08
General Chemistry
Work Order # ... : CTKAA
Date Received .• : 04/13/99
'JPuanterra
Matrix ......... , WATER
PREPARATION-PREP PARAMETER
Non-Filterable
RESULT =='--,,RL=.. ___ ON_I_T~S ___ M,_,E,,_TH=Oe:D=...... _____ ANALYSIS DATE BATCH#
9104269 Solid 6.0 5.0 mg/L MCAiiii' 160.2 04/14/99
(Residue)
Dilution Factor: 1
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Lot-Sample# ... , G9D130221-010
Date Sampled ... , 04/12/99
Prep Date ...... , 04/16/99
Prep Batch# ... , 9106241
Dilution Factor, 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC {Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUST E & I
Client Sample ID, Sii'-09
GC Semivolatiles
Work Order # ..• , CTKACl O 1
Date Received .. , 04/13/99
Analysis Date .. , 04/27/99
~uanterra
Matrix ......... , WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
88 (47 -119)
33 (10 ·-146)
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Lot-Sample# ... : G9D130221-010
Date Sampled ... : 04/12/99
RUSTK&I
Client Sample ID: SW-09
General Chemistry
Work Order # ••. : CTKAC
Date Received .. : 04/13/99
~uanterra
Matrix ......... : WATER
PREPARATION-PREP
PARAMETER RESULT ==---:..:R::L ___ ~UN=I'-'T'-"S'----,.,M::E.:.TH,.,_O""D=------ANALYSIS DATE BATCH#
04/14/99 9104269 Non-Filterable Solid ND 5. 0 mg/L MCAWW 160 . .2
(Residue)
Dilution Factor: 1
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Lot-Sample# ... , G9Dl30221-0ll
Date Sampled ... , 04/12/99
Prep Date ...... , 04/16/99
Prep Batch# ... , 9106241
Dilution Factor, 1
PARAMETER
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
SURROGATE
Tetrachloro-m-xylene
Decachlorobiphenyl
RUSTE&I
Client Sample ID, Slf-10
GC Semivolatiles
Work Order ft ... ' CTKADlOl
Date Received .. , 04/13/99
Analysis Date .. : 04/2J/99
Quanterra
Matrix ......... : WATER
Method ......... : SW846 8081A
REPORTING
RESULT LIMIT UNITS
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
ND 0.050 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
81 (47 -119)
38 (10 -146)
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Lot-Sample# ... : G9Dl30221-011
Date Sampled ... : 04/12/99
PARAMETER RESULT
Non-Filterable Solid ND
(Residue)
RUSTB&I
Client Sample ID: SW-10
General Chemistry
Work Order i ... : CTKAD
Date Received .. : 04/13/99
RL UNITS METHOD
5.0 mg/L MCAWW 160.2
Dilution F•ctor: l
Quanterra
Matrix ......... : WATER
PREPARATION-
ANALYSIS DATE
04/14/99
PREP
a·ATCH #
9104269