NCD986232379_19961010_Greshams Lake Industrial Park_SERB PA SI_Combined Preliminary Assessment Site Inspection Volume I - Text Photos Appendix-OCR

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STATE OF
NORTH CAROLINA
Department of Environment, Health,
and Natural Resources
Division of Waste Management
Superfund Section
COMBINED PREUMINARY ASSESSMENT/SITE INSPECTION
Greshams Lake Industrial Park
NCD 986 323 '379
Raleigh, Wake County, NC.
Reference No. 06117
October 1996
Irene Williams
Environmental Chemist
Division of Waste Management
Superfund Section
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t:
State of North Carolina j •
Department of Environment, I,
Health and Natural Resources 1
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Ms. Cynthia Gurley
EPA NC CERCLA Project Officer
U.S. EPARegion IV
Atlanta Federal Building
100 Alabama St., SW
Atlanta, Georgia 30303-3140
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October 10, 1996 I'
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DEHNR
Subject: Combined Prelimin~ry Assessment/Site Inspection ' ' . Greshams Lake Industnal Park
NCD 986 232 379 i:
Raleigh, Wake Courity, N.C. ' i :
j Dear Ms. Gurley:
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The enclosed report contains thei findings of the Combined Preliminary Assessment/Site
Inspection conducted June 11, 1996, by the\NC Superfund Section at the Greshams Lake Industrial 1,
Park Site (NCD 986 232 379) located in Raleigh, Wake County, North Carolina.
The Greshams Lake Industrial PJ~ consists of a small industrial park on the outskirts of " northeastern Raleigh in Wake County, North Carolina. Contamination of ground water with
chlorinated hydrocarbons has been documedted in the Greshams Lake Industrial Park area since 1989.
Workers at industries with contaminated w61Is have used bottled water for drinking since the ground
water contamination was reported in 1989) I Although it cannot be established as the only source of
ground water contamination, the property dfthe ABLE Manufacturing Company at 3220 Northside
Drive has been the central focus of numeroJs investigations of this industrial park. In this report, the
term "site" refers to the ABLE Manufacturiig Company property and industries near ABLE that have
' drinking water wells contaminated with chlorinated solvents. j I
ABLE operated a metal fabricatink facility from I 989 until the company closed the facility
in 1993. Prior to ABLE's purchase of the property, the site was occupied by South State
Engineering, a tool and die manufacture1 that operated at the site from the late l 970's until 1989.
When ABLE purchased the property, the .former owner removed a large pile of metal turnings that
had accumulated behind the plant building.j I In the former location of disposed turnings is an area of
oil stained soil and stressed vegetation. Chlorinated solvents were used at the facility in the past and
have been found in the facility's septic tank. j (A degreasing unit was located near the center of the shop
floor for several years. While ABLE appears to be one of the sources that has contributed to the
chlorinated solvent plume(s), it may not Sb the only source. Other industries in the area may have ' contributed to the chlorinated solvent plume(s).
P.O. Box 27687,
1: !Tk. •r~ ~1'1 FAX [phone]
Raleigh, North Carolina 27611-7687
Voice 919-733-4996
l J •~'-1 An Equal Opportunity Affirmative Action Employer
f#rrftldJI/., J;sm 50% recycled/ l 0% post-consumer paper
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• Ms. Gurley
10-10-96 !; Page2
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On June 11, 1996, the NC SuperfuJd Section conducted a Site Inspection in the Greshams
Lake Industrial Park area to supplement the analytical data from previous investigations, and to
determine if contaminants had migrated to do~rearn targets from the site via the ground waier and
surface water pathways. Downgradient wel/s were sampled as w_ell as surface water and sediments
in the surface water pathway. SarnplesJ were analyzed for selected metals, volatile organic
compounds, and semi-volatile organic compounds.
A number of chlorinated solvents J~re found in water samp.les from private wells near the
site. Trichloroethylene exceeding health-bascil'benchrnarks was found at the Charlie Brown's Catering
Service 0.25 mile from ABLE. The well ~t Billings and Garrett, next door to ABLE, contained
methyl-t-butyl ether below health-based benchmarks. Surface water pathway sampling points
' included Gresharns Lake downgradient of ABLE and a point approximately 300 feet into the wetlands
surrounding Perry Creek, which drains the' lake.
Analytical data indicate that no col~tituents attributable to the site or to the contaminated
ground water plume(s) were found at levbls above detection limits in surface water or sediment
samples collected during the SI. However, the potential for deleterious effects on the surface water
pathway from future ground water to surflce water discharge should be investigated.
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The June 1996 SI revealed that the~e is continued evidence of ground water contamination
with chlorinated hydrocarbons in drinkingjwater wells in the vicinity of the site. However, there
continues to be difficulty in attributing the fontamination to a single source.-Further investigation
is needed to delineate sources, extent of contaminated ground water plumes( s ), migration of the
plume( s ), and potential effects on surface tater. ! ' .
I Ii. · · · ii 1· ! 1 rfi d . d fi " n ear er mvesttgatlons so sarnp mg was pe orme m an attempt to e me source areas ,or
the site. Potential sources include the septic tank, soil in the former location of the metal turnings
pile, drums, and degreaser at ABLE Manufacturing Company; contaminated subsurface soils at the
former Halliburton Industries facility and thb'lot adjacent to ABLE; the asphalt laboratory at,nearby
REA Construction; and other industries in it~e area.
There is potential for direct exposure to areas of surface soil contaminated with bis(2-
i ethylhexyl)phthalate on the ABLE propefty; however, the levels found are below health-based
benchmarks. The location of the site in an industrial area with no nearby residences, schools, or day
care centers minimizes risk of direct expo Jure of the general public to contaminated soil. Because
of the nature of the soil contamination on the site, there is little likelihood of a significant release to
air. r .
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, Ms. Gurley
10-10-96
Page3
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Concerning site prioritization, because1 of the number of affected drinking water wells and
the employees they served, and because the plud.e(s) may continue to migrate, it is recommended that
the Greshams Lake Industrial Park be the sJbject of an Expanded Site Inspection (ESI). The .,
objectives of the ESI will be to delineate and track the movement.of the contaminated ground water
plume(s) and to determine, if possible, the sourccl(s) of the contaminants in the ground water. Septic
tanks at ABLE Manufacturing and other busine~ses in the site vicinity should be sampled during the
ESI to determine whether removal is needed in. brder to preclude future leaching into ground water.
Drinking water wells pertinent to this investig~tion and the status of water and sewer lines to serve
the area should continue to be monitored. · l ·
The NC Superfund Section recommJds that the Greshams Lake Industrial Park site be
assigned a status of low priority for an ExpandJd Site Inspection. If you have any questions please
contact me at 919/733-2801, extension 283. I
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Enclosure
Sincerely,
Irene Williams
Environmental Chemist
Superfund Section
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COMBINED PRELIMINARY ASSESSMENT/SITE INSPECTION : I
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. I Greshams Lake Industrial Park . ' NCD 986 232 379 • Raleigh,'Wake County, N.C.
Refe~ence No. 06117
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October 10, 1996
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Supel-rund Section ' Division of Waste Management t North Carolina Department of Environment, Health " and Nl)tural Resources
Prepared by:
L0~
Irene Willams
Environmental Chemist
C11t✓L
Bruce Nicholson
Special Remediation
Branch Head
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TABL¢1oF CONTENTS
EXECUTIVE SUMMARY
1.0
2.0
3.0
5.0
6.0
7.0
INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 I : I
SITE DESCRIPTION, OPERATIONAL HISTORY, AND WASTE ......... 1
2.1 Location ............... l ................................. 1
2.2 Description ............. 1 I ................................. 1
2.3 Operational History and Wast~ Characteristics ..................... 5
2.4 Previous Investigations/ Analytical Results . . . . . . . . . . . . . . . . . . . . . . 5-6 : I
::::::::RS:::: /1··::::::::::::::::::::::::::::::: .6-:
4.1 Hydrogeologic Setting ..... ' ................................ 7-8
4.2 Targets ................. ·1· . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-9
4.3 Sample Locations ........................................... 9
4.4 Analytical Results ......... '·I· . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 . . 4. 5 Conclus1ons .............. •. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
SURFACE WATER PATHWAY . .-l-............................... 12
5.1 Hydrologic Setting ........ :\· ............................... 12
5.2 Surface Water Targets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12-15
5.3 Sampl: Locations ........ -i· ........................•...... 15
5. 4 Analytical Results ........ : I· ............. : . . . . . . . . . . . . . . . . . 15
5. 5 Conclusion .............. 1 ,. • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • 16
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SOIL EXPOSURE AND AIR PATHWAYS 16 • 6.1 Physical Conditions ......... l . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
6.2 Soil and Air Targets ........ ! . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . I 6
6.3 Soil Sampling ............. l ..... : . . . . . . . . . . . . . . . . . . . . . . 16-17
6.4 Air Monitoring ........... : ! . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
6.5 Conclusions ............. _;) ............................... 17 ' I
SUMMARY AND CONCLUSIONS .-i-· .......................... 17-18
PHOTOGRAPHS : I
APPENDIX
REFERENCES
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LIS'f10F TABLES
Ground Water Population Estimate : I ....................................... 9
Summary of Significant Analytical Rlsults .. : . . . . . . . . . . . . . . . . . . . . . . . . . . . . I 0-11
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LIST OF FIGURES : i
Topographic map ............. ·l · ..................................... 2
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Site location map ............. · + ...................................... 3
Site layout map with SI sampling loc_ations ................................... 4
o,~milrndi•s map .......... · I · ........................... · ... · .. · · 13
Surface Water Pathway map ..... :
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:I EXECTIVE SUMMARY ' .
The Greshams Lake Industrial Parli: consists of a small industrial park on the outskirts of
northeastern Raleigh in Wake County, Ndrth Carolina. Contamination of ground water with
chlorinated hydrocarbons has been document&! in the Gresharns Lake Industrial Park area since 1989.
Workers at industries with contaminated well§ have used bottled water for drinking since the ground
water contamination was reported in 1989.: Wthough it cannot be established as the only source of
ground water contamination, the property of'.the ABLE Manufacturing Company at 3220 Northside ' .
Drive has been the central focus ofnumeroustinvestigations of this industrial park. In this report, the
term "site" refers to the ABLE Manufacturing Company property and industries near ABLE that have
drinking water wells contaminated with chlorinated solvents. ' . ' I ' ABLE operated a metal fabricating facility from 1989 until the company closed the facility
in 1993. Prior to ABLE's purchase or" the property, the site was occupied by South State
Engineering, a tool and die manufacturer t~at operated at the site from the late 1970's until 1989.
When ABLE purchased the property, the f6imer owner removed a large pile of metal turnings that
' had accumulated behind the plant building. In the former location of dispo_ sed turnings is an area of
'" oil stained soil and stressed vegetation. Chlorjnated solvents were used at the facility in the past and
have been found in the facility's septic tank. N degreasing unit was located near the center of the shop
floor for several years. While ABLE appd&s to be one of the sources that has contributed to the
chlorinated solvent plume( s ), it may not be, the only source. Other industries in the area may have
contributed to the chlorinated solvent plum;(s).
On June 11, 1996, the NC Su~lrfund Section conducted a Combined Preliminary
Assessment/Site Inspection (SI) in the Gi-~shams Lake Industrial Park area to supplement the
analytical data from previous investigatio~t and to determine if contaminants had migrated to
downstream targets from the site via the grciJnd water and surface water pathways. Downgradient
wells were sampled as well as surface water :and sediments in the surface water pathway. Samples
were analyzed for selected metals, volatile orglinic compounds, and semi-volatile organic compounds.
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A number of chlorinated solvents J~re found in water samples from private wells near the
site. Trichloroethylene exceeding health-based benchmarks was found at the Charlie Brown's Catering
Service 0.25 mile from ABLE. The well at Billings and Garrett, next door to ABLE, contained
methyl-t-butyl ether below health-based bdnchmarks. Surface water pathway sampling points
included Greshams Lake downgradient of AB't.E and a point approximately 300 feet into the wetlands
surrounding Perry Creek, which drains the ,11ke.
Analytical data indicate that no con'Jituents attributable to the site or to the contaminated
" ground water plume( s) were found at levels above detection limits in surface water or sediment
samples collected during the SI. However, the potential for deleterious effects on the surface water
pathway from future ground water to surfaciJ water discharge should be investigated.
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The June 1996 SI revealed that there' is continued evidence of ground water contamination
with chlorinated hydrocarbons in drinking J!ter wells in the vicinity of the site. However, there
continues to be difficulty in attributing the c6~tamination to a single source. Further investigation
is needed to delineate sources, extent of coJtaminated ground water plumes( s ), migration of the
plume( s ), and potential effects on surface wat~r. I
In earlier investigations soil sampling ~ls performed in an attempt to define source areas for
the site. Potential sources include the septic, tank, soil in the former location of the metal turnings
pile, drums, and degreaser at ABLE Manufactiring Company; contaminated subsurface soils at the
former Halliburton Industries facility and the ldt adjacent to ABLE; the asphalt laboratory at nearby
REA Construction; and other industries in thel area.
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There is potential for direct exposure to areas of surface soil contaminated with bis(2-
1 ' . ethylhexyl)phthalate on the ABLE property;j however, the levels found are below health-based
benchmarks. The location of the site in an indu~trial area with no nearby residences, schools, or day
care centers minimizes risk of direct exposure) of the general public to contaminated soil. Because
of the nature of the soil contamination on the site, there is little likelihood of a significant release to
air. 1 I
Concerning site prioritization, becausejof the number of affected drinking water wells and
the employees they served, and because the plume(s) may continue to migrate, it is recommended that
the Greshams Lake Industrial Park be the stibject of an Expanded Site Inspection (ESI). The
objectives of the ESI will be to delineate and traick the movement of the contaminated ground water
plume(s) and to determine, if possible, the sourcJ(s) of the contaminants in the ground water. Septic
tanks at ABLE Manufacturing and other businesses in the site vicinity should be sampled during the
ESI to determine whether removal is needed in, 6rder to preclude future leaching into ground water.
Drinking water wells pertinent to this investigation and the status of water and sewer lines to serve
the area should continue to be monitored. , j
The NC Superfund Section recomm~Jds that the Greshams Lake Industrial Park site be
assigned a status oflow priority for an Expandkd Site Inspection. · I ' , I ,I ,,
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1.0 INTRODUCTION
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Under authority of the Comprehensivf;Environrnental Response, Compensation, and Liability
Act of 1980 (CERCLA) and the Superfund Amendments and Reauthorization Act of 1986 (SARA),
the North Carolina Superfund Section conduct~ a Combined Preliminary Assessment/Site Inspection
(SI) of the Greshams Lake Industrial Park site (NCD 986 232 379). The purpose of this investigation
was to collect sufficient information concerning conditions at the site to assess the threat posed to ' human health and the environment, and to determine the need for additional CERCLNSARA or
other appropriate action. The scope of the invJstigation included review of available file information,
a comprehensive target survey, update of n~nsampling data, a site reconnaissance (October 31, ' . 1995), and the SI sampling trip (June 11, 1996). Samples were collected of ground water from an
upgradient background well and several thfeatened drinking water wells. In the surface water
pathway, background and downstream surfac~ water and sediments were collected.
2.0 SITE DESCRIPTION, OPEJTIONAL HISTORY, AND WASTE
CHARACTERISTICS
2.1 Location
The Greshains Lake Industrial Park ~~nsists of a small industrial park on the outskirts of
northeastern Raleigh in Wake County, North c'Jrolina (Ref3). Investigations of the Greshams Lake
Industrial Park have centered on the property of the ABLE Manufacturing Company at 3220
Northside Drive. In this report, the term "site" rtfers to the ABLE Manufacturing Company property
and industries near ABLE that have drinking ~ater wells contaminated with chlorinated solvents.
These industries include REA Construction Codipany, which has an asphalt laboratory on Greshams
Lake Road, the former Halliburton Industries bllilding located across Northside Drive from ABLE,
a.,d Billings and Garrett Utility Contractors, I~1corporated, on Northside Drive next door to ABLE
(Figs.1,2,3). While ABLE appears to be a soJrce, it may not be the only source. Other industries ' in the area may have contributed to the chlorinated solvent plume(s).
To reach the site from Raleigh, take u~!Highway 1 northeast to Greshams Lake Road, tum
west onto Greshams Lake Road, cross the railroad, and proceed to Northside Drive which exits to
the left. Prnceed on Northside Drive to the ~ABLE Manufacturing Company property at 3220
(Figs.1,2). The geographic coordinates ofthci site are 35° 53' O" N latitude and 78° 34' 54" W
longitude (Ref.3). • l · .
2.2 Description , I
Since several investigations of the Gresliams Lake Industrial Park have centered on ABLE,
there is a considerable amount of data available o~ the ABLE property. The ABLE property consists
of approximately 1.8 acres which slopes gently to the south toward Greshams Lake (Ref 5; Fig. I).
Bedrock crops out locally on site (Ref5). D&ring a site reconnaissance on October 3 I, I 995,
Superfund Section staff observed a large manufa~turing building with loading docks, several drums,
some of which appeared to have leaked, a dumpsttr, and two empty truck trailers. A drinking water '" well is located in front of the building near Northside Drive (Refs.6,7;Fig.3; Photographs).
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r MILLBR~Ll I.,, EXCHANGE ,
, PARK '. {t .. § -"".-,, -· I
I 1.sJm~rtin Ci
'l.Q-o,, Pollll C!
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Fig. No: 2
North Carolina Division
of Waste Management
Superfund Section
L ' cf: oa1' Fore \
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Title:· Site Location.Map
Date:
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October 1996
Site Name: Greshams Lake Industrial Park
Drawn By: I. Williams
NCD 986 232 379
Fig. No: 3
North Carolina Division
of Waste Management
..... ?u~rfund Section
Camp ="~ Durant I
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Greshat1"15
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Lal<e Rd.
Northside Dr.
Greshams Lake
Title: Site Layout with SI Sampling Locations
Scale: Not to Scale Date: October 1996
Site Name: Greshams Lake Industrial Park.
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Drawn By:Stephanie Kozel
NCD 986 232 379
Mettrey/Hallburton
OSupplyWell
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Drinking Water Well
Drums
Dumpster
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on Stained Soil
Northside Dr.
ABLE
Manufacturing
Former Turning Disposal Areai---7
(Stressed Vegetation) j j
Site Layout Map With Sampling Locations
1. ABLE Manufacturing Company 9. Perry Creek downstream of Rowland landfilVOuarry
GL-004-SW/SO
2. Billings and Garrett, Inc. 10. PPE at Gresham lake
GL-006-PW GL-005-S~/SO, GL-105-SW/SD
3. Charlie Brown's Catering Service 11. Perry Creek 300' into wetlands
Gl-004-PW GL-004-SW/SD
4. Century Precast Steps 12. Du+rant Lake
GL-005-PW · GL-001-SW/SD
5. Jones Well -Vineland Drive 13. Lincoln Park North
GL-002-PW GL-001-PW
6. Drake Well -Vineland Drive 14. Mettrey/Hal!iburton
GL-007-PW GL-003-PW
7. Lake Center -Clearfield Road 15. Overhead Door Company
GL-008-PW
8. Perry Creek upstream of Rowland LandfilVOuarry 16. Weeks Construction Company
GL-003-SW/SD
w Wetlands
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2.3 Operational/Regulatory History and Waste Characteristics
Ground water monitoring in the area has shown the presence of several chlorinated solvents
including vinyl chloride, cis-1,2-dichloroethene, and trichloroethene. A single source of this
contamination has not been identified. Multiple sources are a strong possibility. A possible second
plume containing methyl-t-butyl-ether (MTBE) is also indicated by the ground water data. As
mentioned above, the Greshams Lake Industrial Park includes a number oflight to medium industrial
facilities. These facilities include machine shops, auto repair shops, and other small facilities that
could use a variety of solvents, including chlorinated hydrocarbons (Ref.4).
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ABLE Manufacturing Company operated a metal fabricating facility from I 989 until the
company closed the facility in 1993 (Refs.2,5). Prior to ABLE's purchase of the property, the site
was occupied by South State Engineering, a tool and die manufacturer that operated at the site from
the late 1970's until 1989 (Ref.5) When ABLE purchased the property, the former owner removed
a large pile of metal turnings that had accumulated behind the plant building (Ref.5). Reportedly, this
pile of metal turnings was disposed in an approximately 20 foot by 45 foot area in the southwest ,
portion of the property. The turnings pile was described as being approximately 4 feet high.(Ref. 30).
In the former location of disposed turnings, stressed vegetation was observed during the June 11,
1991 SI by N.C. Superfimd Section staff (Ref.30). Chlorinated solvents were used at the facility in
the past. A former employee of both South State and ABLE reported that trichloroethylene was
used at the site, although it was his belief that its use was " limited." A small degreasing unit had been
located near the center of the shop floor for several years, but was replaced by a Safety-Kleen unit
that did not use chlorinated hydrocarbon solvents (Ref.5).
2.4 Previous Investigations/ Analytical Results
The area has had numerous investigations which have been unable to establish ABLE as the
sole source of chlorinated solvents. In I 989, the NC Department of Health and Human Resources
found evidence of chlorinated hydrocarbons in samples from the facility's drinking water well. Results
revealed the presence ofvinyl chloride at 5.4 micrograms/liter (ug/1 ), 1-2-dichloroethylene at 135.3
ug/1 and trichloroethylene at 98.5 ug/1 (Refs.5,8). Investigations at the site by the NC Superfund
Section and the Division of Environmental Management in 1990 and 1991 also revealed chlorinated
hydrocarbons in the ground water, including 39 ug/1 vinyl chloride in the ABLE drinking water well
(Ref.9). Drinking water wells upgradient, downgradient, and cross-gradient of the site contained
trichloroethylene levels as high as 26. 7 ug/1 in the well at Charlie Brown's Restaurant approximately
0.25 mile south of the site and cis-1,2-dichloroethylene at 28.6 ug/1 in the Halliburton Industries well
just north of ABLE Manufacturing on Northside Drive. These wells range from 0.1 mile to 0.25 mile
from the site. Soils collected on the ABLE property were found to contain bis(2-ethylhexyl)
phthalate at 18 milligrams/kilogram (mg/kg) and 32 mg/kg. No chlorinated hydrocarbons were
detected in soils on the ABLE property (Refs.8,9).
Trigon Engineering conducted a site investigation for ABLE Manufacturing in 1991. Trigon
reported that ground water samples taken in July and September of 1991 from 5 monitoring wells and
one domestic well contained levels of chlorinated hydrocarbons above "the state standard
concentrations." Highest levels of the following chemicals were reported in Appendix C of the
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Trigon report: 75 ugll trichloroethene, 10 ug/l vinyl chloride, 2 ug/l trans-1,2-dichloroethene, and I:
ug/l tetrachloroethene in the ABLE drinking water well (DW-1 ); 41 ug/l total 1,2-dichloroethene in:
monitoring well MW-3; 34 ug/l l, I, I-trichloroethane and 8 ug/l l, 1-dichloroethene in monitoring welL
MW-4. Soil samples were collected from areas near the loading dock, in the former disposal area for·
metal turnings, and from soil borings under the building. Results indicated that soils sampled,
contained no petroleum hydrocarbons, volatile halocarbons, or volatile aromatics above the,
quantitation limits of the analytical methods used (Ref5). ·
In 1992 the NC Division of Environmental Management (DEM) conducted an extensive,
investigation of ground water contamination at the site. In monitoring wells and domestic wells at '
ABLE Manufacturing and Halliburton Corporation (across Northside Drive to the north of ABLE),
the following compounds were found. Maximum levels in ug/l are given in parentheses:
trichloroethylene ( 62), cis-1,2-dichloroethylene(l 46), trans-1,2-dichloroethylene (2),
tetrachloroethene (3), trichloroethane (24), 1,1-dichloroethylene (11), 1,1-dichloroethane (3.9)
chlorobenzene (1.6), 1,4-dichlorobenzene (3. 7), chloroform (1.2), and MTBE (9.8) (Ref I!).
At the request of DEM, the Wake County Health Department sampled septage from the septic'
tank at the ABLE property. Analytical results revealed the following: 11. 7 ug/l trichloroethene, 5.4.
ug/l benzene, 104 ug/l cis-1,2-dichloroethene, 3.3 ug/l chloroform, 37.9 ug/l toluene, and 57.3 ug/1:
xylenes (Ref39). These results establish ABLE as at least a partial contributor to the chlorinated
w~mp~=-·
As mentioned above, on October 3 I, 1995, the NC Superfund Section conducted a site
reconnaissance at and near the ABLE Manufacturing property. Superfund staff observed and
photographed drums, empty truck trailers, and stained soil on the site. At that time the building '
appeared to have been abandoned (Refs.6, 7;Fig.3; Photographs).
On June 11, 1996, the NC Superfund Section conducted a Site Inspection in the Greshams ·
Lake Industrial Park area to supplement the analytical data from previous investigations, and to
determine if contaminants had migrated to downstream targets from the site via the ground water and ·
surface water pathways. Downgradient wells were sampled as well as surface water and sediments ,
in the surface water pathway. Samples were analyzed for selected metals, volatile organic
compounds, and semi-volatile organic compounds. Analyses were performed by the NC Laboratory
of Public Health in Raleigh, NC. Results of the laboratory analyses are detailed in pertinent pathway
sections of this report (Ref 12, 13).
The Division of Environmental Health monitors several wells within two miles of the site.
Data from the final quarter of 1995 and the first quarter of 1996 reveal low levels of chlorinated
solvents in wells at REA Construction Company, approximately 0.17 mile from ABLE, and
Homestead Village Mobile Home Park located within 0.9 mile of ABLE (Ref 17).
3.0 WASTE/SOURCE SAMPLING
As described in Section 2.4 of this report, extensive soil sampling has been performed in an
attempt to define source areas for the site. Ground water contamination with chlorinated :
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hydrocarbons has been documented, but no clearly defined source of the contaminants found in the
ground water have been identified as attributable to soils on the site. Because potential sources had
been thoroughly studied in earlier investigations, no waste or source sampling was performed during
the June 11, I 996 Site Inspection.
Potential sources of the contaminated ground water plume( s) in the Greshams Lake
Industrial Park include the septic tank, turnings pile, drums, and degreaser at ABLE Manufacturing
Company; contaminated soils at the former Halliburton Industries facility and the lot adjacent to
ABLE; as well as the asphalt laboratory at nearby REA Construction and other industries in the area.
Wells serving five businesses with approximately 76 employees.at the time were closed for drinking
because of one or more contaminated ground water plumes (Ref40).
4.0 GROUND WATER PATHWAY
4.1 Hydrogeologic Setting
There is one aquifer of concern in the site area; this starts in the saprolite, the weathered rock
that forms the land surface, and extends down into the bedrock. Ground water is contained in the
pore spaces of the weathered bedrock (i.e. saprolite) and the bedrock fractures. The ground water
in the pore spaces generally acts as a reservoir that recharges the fracture system. Because it is
hydraulically well-connected, the bedrock/saprolite system acts as one aquifer (Ref32).
The site is located in central Wake County on the northeastern outskirts of Raleigh, NC. All
of Wake County, with the exception ofa small area in the southern edge of the county, lies in the
Piedmont physiographic province. This province is characterized by rolling hills and V-shaped valleys
(Ref 14).
There are outcrops ofbedrock, consisting mainly of mica gneiss, on the site (Ref5). The site
is in an area of mica gneiss and hornblende gneiss. The predominant rock types included in the mica
gneiss unit are biotite-feldspar gneiss, quartz gneiss, garnet-mica gneiss, biotite gneiss; and
interbedded mica schist and gneiss. These are all metamorphic rocks which show banding, foliation,
or gneissic texture. The hornblende gneiss bodies are medium to coarse grained and vary in color
from green to dark-gray. Where the hornblende content is especially high, the gneissic texture is less
apparent and the rock has a schistose foliation of well-developed and well-aligned hornblende crystals
(Ref 14).
The amount of water that can be stored in the rocks and soil is controlled by the size, shape,
and number of pore spaces they contain. The rocks of the earth's crust, including soils and weathered
saprolite materials, contain pore space or interstices that are filled with water in the zone of
saturation. In crystalline rocks such as granite, schist, and gneiss, the volume of primary pore space
between individual components is very small. In the igneous and metamorphic rocks that underlie
most of the Raleigh area, many of the interstices are formed or enlarged by normal weathering
processes at or near the earth's surface. With depth, the size and abundance of interstices decreases,
consequently, in this area of the state, most ground water is stored in the upper JOO-to 200-foot-zone
of the earth's crust, notably in the saprolite (Ref 14).
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Water level elevations in monitoring wells on and near the site ranged from 62.8 feet to 61.3
feet during the Trigon investigation on September 25, 1991. Depth to water table on that date ranged
from 61.3 feet to 63. I feet. The Trigon study indicates that ground water flows from north to south
across the site (Refs.5, 8). This flow pattern was confirmed in the 1992 DEM investigation (Ref 11 ).
Soils in the vicinity of the site are described in the Soil Survey of Wake County, North
Carolina, as belonging to the Cecil-Appling association: gently sloping to steep, deep, well-drained
soils that have a subsoil of firm clay loam to clay; derived mostly from weathered granite, gneiss, and
schist (Ref 15). As part of the Trigon study for ABLE Manufacturing Company soil borings were
performed. In the Trigon report soils at the site were described as appearing to consist of saprolitic,
firm to very firm, slightly micaceous to micaceous, silty, coarse to fine sands to the termination depth
of the borings. Boring depths ranged from 35 feet to 43.5 feet below the ground surface. In this
study, measurable hydraulic conductivities of soils in the vicinity of the water table were determined
to be on the order of7.5 X 10-s centimeters/second (cm/sec) (Ref5). ·
4.2 Targets
The site is located northeast of Raleigh (Fig.!). The city of Raleigh and its extraterritorial
service areas obtain drinking water from the Raleigh municipal water system. The system uses an ·
intake at Falls Lake for its water source. This intake is located considerably upstream of, and
therefore not threatened by, the site (Fig. I). The Raleigh municipal water service area, as provided .
by the Raleigh Public Utilities Office, is marked on the topographic map (Ref.16; Fig. I). In August .
I 996, construction of a 16 inch water main on Greshams Lake Road from Litchford Road to US
Highway I was completed. Industries in the Greshams Lake Industrial Park should have ready access
to both water and sewer service by June 1997 (Ref 16).
There are a number of private and community wells within a 4-mile radius of the site
(Refs. I 7, 18; Fig. I). The drinking water well located at ABLE is considered the nearest well (Fig ..
I). Businesses on the site and within a 0.25-mile radius of the site, include ABLE, Billings and
Garrett, Mettrey Properties rental property (former location of Halliburton Industries), REA
Construction, and the Charlie Brown's Catering Service. These businesses, which employed about
76 employees at the time the ground water contamination was discovered, have reportedly used
bottled water for drinking since ground water contamination was reported (Refs.2, 12,34,35,40).
There are no wellhead protection areas within a 4-mile radius of the site (Ref 19).
The population using ground water for drinking within a four-mile radius of the site was
estimated by counting the houses on the topographic map (Fig. I) in those areas not served by the
Raleigh municipal water system. Appropriate 1990 census data ratio (2.46 persons per household)
was applied to the number of households counted to calculate the population using private wells
(Ref 18). Pertinent community wells were identified from Public Water Supply records (Ref36).
These community wells are marked on the topographic map (Fig. I). Population figures for the
community wells are included in the population using ground water shown in Table I, below. The
7 6 workers employed at the five businesses mentioned above, as well as employees at other
businesses where the wells were sampled in earlier investigations, are also included in the ground
water population calculation for Table I. Table I describes the population estimated to use ground
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water for drinking within a 4-mile radius of the site, an estimated total of9,442 ground water users (Ref. l 8;Table I).
TABLE 1. GROUND WATER POPULATION ESTIMATE
(Reference 18)
MILE PRIVATE COMMUNITY TOTALGW RADIUS WELLS PERSONS WELLS USERS POPULATION
>0-0.25 7 145 0 145 >0.25 -0.5 29 71 25 96 >0.5 -1.0 93 229 I, 148 1,377 >1.0 -2.0 227 558 325 883 >2.0 -3.0 530 1,304 894 2,198 >3.0 -4.0 918 2,258 2,485 4 743 TOTALS: 1,804 4,665 4,877 9,442
4.3 Sample Locations
Eight drinking water wells located upgradient, cross-gradient, and downgradient of the ABLE property were sampled during the June 11, 1996 Site inspection (Ref 12,13, Table 2; Fig.3). These samples (GL-001-PW through GL-008-PW) are described in Table 2 and shown in Figure 3 (Table 2; Fig.3;Photographs).
4.4 Analytical Results
Ground water samples were analyzed for selected metals, volatile organic compounds, and semi-volatile organics (Refs. 12, 13;). Analytical results are summarized in Table 2. Laboratory reports are provided in the Appendix to this report (Table 2; Appendix).
A number of chlorinated solvents were found in water samples from private wells near the site. The levels found in most cases were trace levels or estimated concentrations below detection limits, with the following exceptions. The well at the former Halliburton property, across Northside Drive from ABLE Manufacturing, was found to contain IO ug/1 cis-1,2-dichloroethene and 7 ug/1 lead. The well at Charlie Brown's Catering Service near Greshams Lake on Overlook Road contained 30 ug/1 trichloroethylene, 60 ug/1 copper, 6 ug/1 lead, and 140 ug/1 zinc. The well at Century Precast Steps contained 70 ug/1 zinc. The well at Billings and Garrett, next door to ABLE Manufacturing, contained 7 ug/1 MTBE. One well on Vineland Drive on the far side of Greshams Lake from the site contained 140 ug/1 zinc (Table 2, Appendix). The only level exceeding health-based benchmarks was the 30 trichloroethylene level found _at the Charlie Brown's Catering Service well (Refs.31,38). Metals detected in the ground water cannot be attributed to the site.
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GRESHAMS LAKE INDUSTRIAL PARK
NCD 986 232 379
SITE INSPECTION
JUNE 11, 1996
TABLE 2. SUMMARY OF SIGNIFICANT ANALYTICAL RESULTS
SAMPLE ID LOCATION ORGANICS (ppb) TOTAL METALS (ppm)
GL-001-PW Lincoln Park Acetone 6J Barium0.06
North (Upgradient Methylene Chloride Trace Chromium0.01
well) 1,1-Dichloroethane Trace
2-Butanone 2J
Chloroform Trace
1, I, 1-Trichloroethane Trace
GL-002-PW Jones well on 2-Butanone lJ Barium 0.05
Vineland Chloroform Trace
GL-003-PW Mettrey well ( old Acetone 3J Barium 0.08 Halliburton well Trans-1,2-Dichloroethene Tr. Lead 0.007 on Northsidc Cis-1,2-Dichloroethene 10
Drive) Chloroform Trace
Trichloroethylene 4J
1,4-Dichlorobenzene Trace
GL-004-PW Charlie Brown's Acetone SJ Barium 0.04
Catering Service Methylene Chloride lJ Copper0.06
well Trans-1,2-Dichoroethene Tr. Lead 0.006
2-Butanone lJ Zinc 0.14
Cis-1,2-Dichloroethene 2J
Chloroform Trace
Trichloroethylene 30
GL-005-PW Century Precast Acetone 4J Barium 0.05
Steps well Zinc 0,07
GL-006-PW · Billings and Acetone 4J Barium 0.06
Garrett well Chloroform Trace
Methyl-t-Butyl Ether 7
GL-007-PW Drake well on Acetone 4J Barium 0.08
Vineland Chloroform Trace Zinc 0.14
GL-008-PW Lake Center well 2-Butanone Trace Barium 0.08
on Clearfield Road Chloroform Trace
1,1 ,!-Trichloroethane Trace
GL-001-SW Durant Lake Acetone 6J Barium 0.03
(Background) 2-B utanone lJ
ppb = parts per billion (water: ug/1; soil/sediment: ugtkg)
ppm = parts per million (water:mg/1; soil/sediment: mgtkg)
C = Possible laboratory contamination or background
PW= Potable Well
SL= Soil
SW= Surface Water
SD = Sediment
J = Estimated Tr. = Trace U = <Minimwn Detection Limit Highlighted levels are significantly above background
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GRESHAMS LAKE INDUSTRIAL PARK
NCD 986 232 379 SITE INSPECTION
JUNE 11, 1996
TABLE 2. SUMMARY OF SIGNIFICANT ANALYTICAL RESULTS
SAMPLE ID LOCATION ORGANICS (ppb) TOTAL METALS (ppm)
GL-002-SW Peny Creek Acetone 9J Barium 0.16 upstream of Methylene Chloride lJ Chromium 0.02 landfill Toluene Trace Lead 0.11
GL-003-SW PenyCreek Acetone 9J ·• Barium 0.16 Zinc 0.06 downstream of 2-Butanone lJ Chromium 0.02 Lead 0.011 landfill Toluene Trace
GL-004-SW Wetlands Benzene Trace Barium 0.08
GL-005-SW GresharnsLake Acetone 6J Barium 0.07
Methylene Chloride 3J
2-Butanone Trace
Benzene Trace
GL-105-SW Grcshams Lake Acetone 6J Barium 0.06
' (Duplicate) Methylene Chloride lJ
2-Butanone lJ
' GL-001-SD Durant Lake u Barium 16 (Background) Zinc 14
GL-002-SD Peny Creek Acetone 7 J,C Barium IO upstream of Methylene Chloride l.5J,C Zinc 0.12 landfill Carbon Disulfide Trace
GL-003-SD Pcny Creek u Barium 24 downstream of Zinc 14 landfill
GL-004-SD Wetlands u Barium 33 Zinc 14
GL-005-SD Greshams Lake u Barium 57 Chromium27
Copper 12 Zinc 27
GL-105-SD Lake Duplicate u Barium 55 Chromium27
Copper 12 Zinc 27
GL-001-TB Trip blank Acetone 4J 2-Butanone lJ
GL-001-PB Preservative blank u
ppb = parts per billion (water: ug/1; soil/sediment: ug/l<g) ppm= parts per million (water:mg/1; soil/sediment: mg/l<g) C = Possible laboratory contamination or background
PW= Potable Well
SL= Soil
SW= Surface Water
SD = Sediment
I= Estimated Tr. = Trace U = <Minimum Detection Limit Highlighted levels are significantly above background
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4.5 Conclusions
There is continued evidence of ground water contamination with chlorinated hydrocarbons in wells in the vicinity of the site. At least five businesses within 0.25 mile are supplying bottled water for their employees. However, there continues to be difficulty in attributing the contamination to a single source. Further investigation is required to delineate sources, extent of contaminated ground water plumes(s), migration of the plume(s), and future effects on ground water quality.
5.0 SURFACEWATERPATHWAY
5.1 Hydrologic Setting
The site lies within the Neuse River drainage basin. It is located in an area of minimal flooding, outside the 500 year floodplain (Ref20). The two-year, 24-hour rainfall is approximately 3.5 inches (Ref21).
The topography of the site and surrounding area directs surface water runoff to the south , toward Greshams Lake, the probable point of entry to surface water (PPE). Surface water runoff flows overland approximately 0.3 mile to the lake (Fig.4). About 0.4 mile farther downstream water flows from the lake into Perry Creek which is surrounded by wetlands (Ref22). Perry Creek flows about 2.2 miles to the Neuse River. The Neuse River flows approximately 12.4 miles to the end of the 15-mile target distance limit for the surface water pathway at a point about 0. 75 mile upstream of State Road 2555 (Figs.1,5). The southern spillway from Greshams Lake to part of Perry Creek shown on the topographic map has been blocked by highway construction debris that has been deposited in the lake (Ref 13;Figs. l,5; Photographs).
The flow rate of Perry Creek is estimated to be approximately 2 cubic feet per second (cfs) (Ref23). The flow rate ofGreshams Lake is assumed to be the same as that of Perry Creek (2 cfs). The Neuse River flow rate in the site area is estimated at 429 cfs (Ref26).
5.2 Surface Water Targets
There are no surface water intakes located within 15 miles downstream of the PPE. The intake for the city of Raleigh is located considerably upstream of the site at Falls Lake (Ref24;Fig. I).
Perry Creek is part of the Neuse River basin and is classified as "B" and "NSW" waters from its source to Greshams Lake and as "C" and "NSW" waters from the dam at Greshams Lake to the Neuse River. Class "B" denotes waters protected for primary recreation and any other usage specified by the "C" classification. The "C" classification calls for protection of the water body for aquatic life propagation and survival, fishing, wildlife, secondary recreation, and agriculture. The "NSW" designation requires limitations on nutrient inputs. The Neuse River from the dam at Falls Lake to the mouth of Beddingfield Creek, considerably downstream of the IS-mile target distance limit from the site, is classified as "C" and "NSW" (Ref25).
12
>ig. No: 4
orth Carolina
ivision of
Title: One-Mile Radius Map
Waste Management Scale: 1:24,000 Date: October 1996 Draw~ By:Williams
uperfund Section Site Name:Greshams Lake Industrial Park NCD 986 232 379
2.2 Ml
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-----®---
w
w
w
(
PERRY CRIEEK
2 CFS
FISHERY
I Vl j 1,i,i
DAMI<
PPE I .. ' GRESKA/,\S UJ<E '1/ . ',\ ·,
SITE.---, ' 2CFS
' ;___ .. i FISHERY
ovc,;:u\/'-10 FLO\'/
0 31.11
NEUSE RIVER
429 CFS
FISHERY
;;-_:_g. !Sc: 5 Ti=!e: s~rface ~a=e:-Path~ay -------------1
No::::-t.!1 :::.:-oli::.a. :::-ivision
o: ~~s=e ~a~a~ement
Site Name: Greshams Lake Indus:rial Park
w
_15 Ml
12.4 Ml---------------------------------;i>) TDL
SE1
9.9 Ml. W
1t 4 ML
/
SE3
11.4 Ml.
13. 2 l ~I. /~__)
SE~ \'/
~-
/ W 13.25 Ml.
OVERLAND FLOW · -· · --
PPE PROBABLE POl,NT OF ENTRY TO SURFACE WATER
W WETLANDS
TDL 15-MILE TARGET DISTANCE LIMIT
SENSITIVE ENVIRONr~1ENTS
SE1 NOTURUS FURIOSUS (FISH)
SE2 ELLIPTIO ROANOKENSIS (MOLLUSK)
SE3 VILLOSA CONSTRICTA (MOLLUSK\
SE4 ALASMIDONTA HETERODON (MOLLUSK)'
SES NECTLJRUS LEWISI (AMPHIBIAN)
'ENDANGERED SPECIES
Drawn By. Stephanie r:ozel
UCO 986 232 379
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Greshams Lake is fished for recreation and as a food source (Photographs). Crappie and bass
are caught there (Refs.6,7,13). This lake is located downgradient of contaminated wells and is the
logical ground water to surface water discharge point (Fig. I). Downstream of Gresharns Lake, Perry
Creek and the Neuse River are also fisheries. Perry Creek from Gresharns Lake to the Neuse River
is fished mainly for red breast and blue gill, but probably bass and crappie as well. The Neuse River
is a major fishery for numerous species of freshwater fish. No harvest data are available for these
three fisheries (Ref.27; Fig.5).
Wetlands occur on both sides of Perry Creek from the Greshams Lake dam to more than 300
feet downstream (Figs.3,5). According to National Wetlands Maps, the wetlands continue on both
sides of the creek to the Neuse River (Ref.22). Total wetland frontage along Perry Creek is
approximately 4.4 miles. Wetlands with a total frontage of 11.4 miles occur along the Neuse River.
The total wetlands frontage in the surface water pathway is approximately 15.8 miles (Ref.22; Fig.5).
In the 15-mile surface water pathway downstream of the PPE there is one known habitat of
an animal officially classified "Endangered" at both the state and federal levels. The species is the
Alasmidonta heterodon, a mollusk with the common name ofDwarfWedgemussel. There are four
other species of animals of concern to the North Carolina Natural Heritage Program. These species
are Noturus furiosus (fish), Elliptic roanokensis (mollusk), Villosa constricta (mollusk), and Necturus
lewisi (amphibian) (Ref.28). Habitats of the five species of concern are indicated on the topographic
map and the surface water pathway map (Figs.1,5).
5.3 Sample Locations
During the June 11, 1996 SI, the NC Superfund Section collected surface water and sediment
samples to determine whether site contaminants had migrated to surface water. Sampling points are
illustrated in Figure 3 and described below. These samples included three background surface water
and sediment samples. The first of these was collected from Durant Lake as a control sample from
a similar lake in a different local watershed. The other background samples were from Perry Creek
upstream of Greshams Lake at points upstream and downstream of the Rowland Landfill ( samples
GL-003-SW/SD and GL-002-SD/SW, respectively). Surface water target samples included:
duplicate samples at the PPE at Greshams Lake (GL-005-SW/SD and GL-105-SW/SD) and one
sample of surface water and sediment at a point approximately 300 feet into the wetlands
surrounding Perry Creek (GL-004-SW/SD). Samples of surface water and sediments taken during
the June 11, 1996 SI are described in Table 2, the SI trip report and in the SI field notes, and are
shown in Figure 3 (Refs.12, 13; Fig.3; Table 2; Photographs).
5.4 Analytical Results
Surface water and sediment samples were analyzed for selected metals, volatile organics, and
semi-volatiles. Table 2 summarizes analytical results for surface water and sediments. The Appendix
to this report contains laboratory reports of analytical data. No surface water samples contained
levels of constituents significantly above background. The two sediment samples from Greshams
Lake at the PPE (GL-005-SD and GL-105-SD) each contained 27 mg/kg total chromium (Table 2;
Appendix).
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5.5 Conclusions
Analytical data indicate that no constituents attributable to the site were found at levels above
detection limits in surface water or sediment samples collected during the SI. Elevated levels of
chromium in sediment from Greshams Lake cannot be attributed to the site. For site prioritization
purposes, the most important sample in the surface water pathway is that taken in the Perry Creek
wetland. The sampling results indicate that this wetland contains no site-related contaminants.
6.0 SOIL EXPOSURE AND AIR PATHWAYS
6.1 Physical Conditions
The site is located in an industrial area with no residences located within 200 feet of the site
(Figs.1,3} . As mentioned above in Section 2.2, the ABLE Manufacturing Company property consists
of approximately 1.8 acres. The property slopes gently to the south toward Greshams Lake.
Bedrock crops out locally on the property (Ref5).
During a site reconnaissance on October 31, 1995 and the Site Inspection on June 11, 1996,
Superfund Section staff observed a large, abandoned manufacturing building with loading docks,
several drums that appeared to have leaked near the main loading dock, a dumpster, and two empty
truck trailers. Stained soil was observed near the loading dock and stressed vegetation was noted in
the former location of the metals turnings pile. A drinking water well was observed in front of the
building near Northside Drive (Refs.6, 7, 12, 13;Fig.3;Photographs)
6.2 Soil and Air Targets
Since the facility is inactive, there ·are no workers employed at the site. There are no
residences, schools or day care centers within 200 feet of the site (Ref 6, 7;Figs. l,3}. The total
populations residing within 1 mile and within 4 miles of the site are 1,795 and 25,229, respectively
(Ref29}. Air targets have not been evaluated because it is unlikely that there are any significant air
releases from the site.
6.3 Soil Sampling
As described above, in Section 2.4 of this report, extensive soil sampling has been performed
in an attempt to define source areas for the site. Areas of soil contaminated with bis(2-
ethylhexyl)phthalate have been identified on the ABLE property by the NC Superfund Section
(Ref9). However, its concentration (32 mg/kg} is below health-based benchmarks (Refs.9,31).
In the 1992 DEM investigation, subsurface soil samples from three points near the ABLE
property were found to contain chlorinated organic compounds. The levels found on property
adjacent to ABLE were 1.8 micrograms/kilogram (ug/kg) cis-1,2-dichloroethene and 1.8 ug/kg
trichloroethene at a depth of 23 feet. Levels found in soils located on the former Halliburton property
upgradient of ABLE were 8.3 ug/kg 1,4-dichlorobenzene, 7.4 ug/kg chlorobenzene, 4 ug/kg 1,3-
dichlornbenzene, and trace levels of 1,2,4-trichlorobenzene at a depth of3-8 feet (Ref. I I}.
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Purchase of the ABLE Manufacturing Company property was under consideration in August
1996. The potential buyer has reportedly proposed an independent cleanup of the property that
would include removal of drums and contaminated soil from the property (Ref33).
6.4 Air Monitoring
Because of the nature of the soil contamination and the depths at which it has occurred at the
site, there is little likelihood of a release to air, nor is it deemed to pose a threat. No air monitoring
was performed during the June 11, 1996 SI.
6.5 Conclusions
Since the facility is not fenced, there is some potential for direct exposure of the general public
to surface soil contaminated with bis(2-ethylhexyl)phthalate; however, levels of this contaminant are
below health-based benchmarks. Because of the nature of the soil contamination on the site, there
is little likelihood of a release to air.
7.0 SUMMARY AND CONCLUSIONS
Contamination of ground water with chlorinated hydrocarbons has been documented in the
Greshams Lake Industrial Park area since 1989. The Site Inspection performed June 11, 1996 by
the NC Superfund Section has confirmed that there is continued evidence of ground water
contamination with chlorinated hydrocarbons in drinking water wells in the vicinity of the site.
However, there continues to be difficulty in attributing the contamination to a single source. Further
investigation is needed to delineate sources, extent of contaminated ground water plumes(s), and
migration of the plume(s).
A number of chlorinated solvents were found in water samples from private wells near the
site. Trichloroethylene exceeding health-based benchmarks was found at the Charlie Brown's Catering
Service 0.25 mile from ABLE. The well at Billings and Garrett, next door to ABLE, contained
MTBE below health-based benchmarks. Surface water pathway sampling points included Greshams
Lake downgradient of ABLE and a point approximately 300 feet into the wetlands surrounding Perry
Creek, the stream that drains the lake.
Analytical data indicate that no constituents attributable to the site or to the contaminated
ground water plume( s) were found at levels above detection limits in surface water or sediment
samples collected during the SI. However, the potential for deleterious effects on the surface water
pathway from future ground water to surface water discharge should be investigated.
In earlier investigations soil sampling was performed in an attempt to define source areas for
the site. Potential sources include the septic tank, soil in the former location of the metal turnings
pile, drums, and degreaser at ABLE Manufacturing Company; contaminated subsurface soils at the
former Halliburton Industries facility and the lot adjacent to ABLE; the asphalt laboratory at nearby
REA Construction; and other industries in the area.
17
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There is potential for direct exposure to areas of surface soil contaminated with bis(2-
ethylhexyl)phthalate on the ABLE property; however, the levels found are below health-based
benchmarks. The location of the site in an industrial area with no nearby residences, schools, or day
care centers minimizes risk of direct exposure of the general public to contaminated soil. Because
of the nature of the soil contamination on the site, there is little likelihood of a significant release to
air.
Concerning site prioritization, because of the number of affected drinking water wells and
the employees they served, and because the plume(s) may continue _to migrate, it is recommended that
the Greshams Lake Industrial Park be the subject of an Expa~ded Site Inspection (ESI). The
objectives of the ESI will be to delineate and track the movement of the contaminated ground water
plume(s) and to determine, if possible, the source(s) of the contaminants in the ground water. Septic
tanks at ABLE Manufacturing and other businesses in the site vicinity should be sampled during the
ESI to determine whether removal is needed in order to preclude future leaching into ground water.
Drinking water wells pertinent to this investigation and the status of water and sewer lines to serve
the area should continue to be monitored.
The NC Superfund Section recommends that the Greshams Lake Industrial Park site be
assigned a status oflow priority for an Expanded Site Inspection.
18
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1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
12.
13.
List of References
Greshams Lake Industrial Park
NCD 986 232 379
Combined Preliminary Assessment/Site Inspection
U.S. Department of the Interior, Geological Survey, Quadrangles: Wake Forest, N.C., 1967,
Photorevised 1987; Bayleaf, N.C., 1967, Photorevised 1987; Raleigh East, N.C., 1968,
Photorevised 1987; Raleigh West, N.C., 1968, Photorevised 1987, Photoinspected 1988;
Garner, N.C., 1964, Photorevised 1987. ·
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Teleconference
with Mr. Wallace Green, ABLE Manufacturing, August 27, 1996.
Williams, Irene, N.C. Superfund Section, Longitude and latitude calculation work sheet,
October 12, 1995.
DeRosa, Pat, Head CERCLA Branch, N.C. Superfund Section, CERCLIS Site Addition
letter, April 19, 1993.
Trigon Engineering Consultants, Incorporated, Phase II Groundwater and Soils Investigation,
ABLE manufacturing, Trigon Project Nos. 035-91-027 and 035-91-033, October 11, 1991.
Williams, Irene, NC. Superfund Section, Memorandum to File Reference: October 31, 1995
Site Reconnaissance Trip Report.
Williams, Irene, N. C. Superfund Section, Site Reconnaissance Field Log Book, October 3 I,
1995.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Review of early
DNR and DEM analytical results, September 26, 1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Review of early
Superfund Section analytical results, September 26, 1996.
United States Environmental Protection Agency, 40 CFR 300, Hazard Ranking System, Final
Rule, Table 3-6, p. 57, December 14, 1990.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Review of 1992
DEM results, September 26, 1996.
Williams, Irene, NC. Superfund Section, Memorandum to File Reference: June 11, 1996 Site
Inspection Trip Report.
Williams, Irene and Rumford, Doug, N.C. Superfund Section, Field Log Books, Site
Inspection Sampling Trip, June 11, 1996.
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References (Greshams Lake Industrial Park)
Page2
14. May, V. Jeff and Thomas, J. D., North Carolina Department of Water Resources, Geology
and Ground-Water Resources in the Raleigh Area, North Carolina. Ground-Water Bulletin
Number 15, Raleigh, November, 1968.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
United States Department of Agriculture Soil Conservation Service, Soil Survey of Wake
County, North Carolina, I 970, General Soil Map.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Raleigh, NC water
lines information, September 27, 1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Public Water
Supplies community well data, August 13, 1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Ground water
using population, February 21, I 996.
Stanley, J., N.C. Superfund Section, Memorandum to StaffReference: Update on status of
well head protection programs in N.C., August 15, 1996.
Federal Emergency Management Agency, Flood Insurance Rate Map, Wake County, North
Carolina and Incorporated Areas, Panel 165 of 810, Map Number 37183C0165 E, March 3,
1992.
United States Department of Commerce, Technical Paper No. 40, Rainfall Frequency Atlas
of the United States, 1961.
Williams, Irene, N.C. Superfund Section Memorandum to File Reference: Wetlands
identification, September 26, 1996.
Ragland, B.C., et al, Water Resources Data North Carolina Water Year 1988, Volume 1.
Surface-Water Records, U.S. Geological Survey Water-Data Report NC-88-1. ,
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Teleconferences:
Surface water intakes, August 22, 1996.
North Carolina Department of Environment, Health, and Natural Resources, Classifications
and Water Quality Standards Assigned to The Waters of the Neuse River Basin, February 1,
1993.
Ragland, B.C., et al, Water Resources Data North Carolina Water Year 1994, Volume I.
Surface-Water Records, U.S. Geological Survey Water-Data Report NC-94-1.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Fishing conditions
in surface water pathway, September 5; 1996.
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References (Greshams Industrial Park)
Page 3
28.
29.
30.
31.
32.
33.
34.
35.
36.
37.
38.
39.
40.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Investigation of
sensitive environments, September 26, 1996.
N. C. State Center for Geographic Information and Analysis, Report on populations and
households within specified distance rings, Site Name., Greshams Lake Industrial Park,
October I 7, 1995.
Butler, Jack, N.C. Superfund Section, Memorandum to File Reference: Sampling visit trip
report, June 11, 1991.
United States Environmental Protection Agency, Superfund Chemical Data Matrix, Appendix
B Tables, June 24, 1994.
Heath, Ralph, Basic Elements of Ground-Water Hydrology with Reference to Conditions in
North Carolina. U.S. Geological Survey Water-Resources Investigations, Open-File Report
80-44, 1980.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Teleconference
with Mr. Stanley Green, August 22, 1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Teleconference
with REA Construction Company office, March 7, 1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Teleconference
with Mr. John Mettrey, September 26, 1996.
North Carolina Department of Human Resources, Public Water Supply System Active
Systems Data Base, August 17, 1995.
United States Department of Commerce, I 990 Census of Population and Housing
Characteristics, 1990.
North Carolina Administrative Code, Title I SA, Department of Environment, Health, and
Natural Resources, Division of Environmental Management, Subchapter 2L, Groundwater
Classification and Standards, November 8, 1993 and subsequent revisions. ·
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: ABLE
Manufacturing Company septic tank information and results of septage analysis, October 3,
1996.
Williams, Irene, N.C. Superfund Section, Memorandum to File Reference: Well depths and
number of employees in vicinity of site, October 3, I 996.
Greshams Lake lnaus rial I?
NCD 986 232 379 -:-'
2.' ABLEManu~ltturing Co.
----------, ·:···~, ':: /;
----._Greshanis-Lake Industrial Park Neb 986·232 37'.9 ----------
ABLE Manufacturing Co. 6/11/96 ----------------
Greshams Lake Industrial Park
NCO 986 232 379
4. ABLE Manufacturing Co.
6/11/96
,.1 I
Greshams Lake I
NCD 986 232 379'
5. ABLE Manufa '
6
. ._
~~i~{;:;,,~ , __ ~-'
Greshams Lake Industrial Park
NCD 986 232 379 ~
/
8. Construction debris at Greshams
Lake r'
6/11/96
f
I
Greshams Lake Industrial Park
NCD 986 232 379
9. Fisherman at Greshams Lake
10/31/95
-•~' ,il_r;~~-r~~';~-,,;'~-:::,%,,:.
~
Greshams Lake Industrial Park
NCD 986 232 379
11. Durant Lake, samples GL-001-
SW/SD
6/11/96
Greshams Lake Industrial Park
NCD 986 232 379
12. East along Perry Creek
downstream of Greshams Lake
6/11/96
Greshams Lake Industrial Park
NCO 986 232 379
13. Upstream Perry Creek, same
location as Photo# 12,
6/11/96
Greshams Lake Industrial Park
NCD 986 232 379
14. Perry Creek, location of samples
GL-002-SW/SD, 6/11/96
. ·1C. Depan:ment of Human Resources
l ision of Health Services SAMPLE ANALYSES REQUEST
Scace Laboratory of Public He:ilth
P. 0. Box 28047
306 N. Wilmingcon Screec
Raleigh, 27611
I Number _,(,"'-· -=\...=---_o=-,.o-"S"'----0-=--='Q"-------Field Sample Number -------------'-----
h,r-me of Sice ('-, ..,a,;......g.&,,g,...,.,.,,s, 4-,.,,___r=., Site Location __________________ _
( \leered By ____________ !Di/ ______ Date Collected _...:l.,,,,,.,..=__,l~),_-~9'-'l.J=-----
T ype of Sample:
Jnvironmental
___ Groundwater (I) 1--Surface Water (2)
__ Soil (3) I--Other ( 4)
' Extractables
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
D
INORGANIC CHEMISTRY
Comments
Total -I Parameter Results mg/ 1 Parameter Results mg/K_5 Parameter
I ~rsenic
L... C -.:::, ·;;_ ~rsenic L.. :"; .'.] V Silver
anum Q, '1 ':.J --rium ~C.: 7--··.• __ Sulfates
--~admium ..,___o.o~ __ Cadmium < lei ~inc
1 ~hromium ....4Q .:o-:5 -~loride _Ph
;)-ead .-!.C -1c --~romium '7)._~ __ Conductivity
--~ercury ...(_ c• _ c-_ i __ Copper I 1.. _TDS
.--r5elenium ..L.. C:-C'c:"2 __ fluoride _TOC
'=Silver -<.O~ ,;;;..5 __ Iron --
('. • ., Op,"--,--s::. ,1, C, ( --~ead .L._ cbL' --. , C!. ,• C: ?-__ 'L..,·\'""'\~ -~anese --
I= __ Mercury ~ci .. ~Cj --
--~race --
--__ elenium -'-."', -~l --
I ORGANIE: CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ I Parameter
I= P& T:GC/MS _£DB __ Methoxychlor
Acid:B/N Exe. __ PCB's __ T oxaphene
_TOX __ Petroleum -2.4-D
I= __ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
.
MICROBIOLOGY RADIOCHEMISTRY
Time / / '. '.'J(J
Results mg/1<3
,:· . /,1
'?-+-
--
Results mg/ I
Parameter Par~meter Results PCi/ I
__ (MF) Coliform Colonies/!00mls I= (MPN) Coliform Colonies/lO0mls
_e Received
__ Gross Alpha
__ Gross Beta
Date Reported __________________ _
Ill:e Extracted -------------------Date Analy:ed O~'JP,St JON 1?96
f orted By ____________________ Lab Number ___________________ _
Jaji 3l91 (Revised 7/85)
~~ :md H:i:ardous Wasre (Review 7/87)
. •N.t. Dcpnnment or Environment, • ·1 llc::ilth, & Natural Re.sources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P .0. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
I Site Nun
Name of
GL-105-5D 06/11/96 1150
Greshans Lake, NC I. WILLIAMS
GRAB nple Number _______________ _
SEDIMENT
ESD LAB
ation __________________ _
Sediment I Collectec G L -
METALS
36 ,Uected. __________ Time _____ _
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I ----
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments v Arsenic .L.. C,,,-).8-.
I . i/Barium D--SA
__ Groundwater (1) _Solid (5) ----V Cadmium <.'.._ C' .. C-~
vChromium --'-e, .o.'.:I 1--Surface water (2) · Liquid (6) _.,cLead -<... C -~Q
_2'Mercury .L.....c .. _,-_,l
_Soil (3) Sludge (7) v Selenium ·.L_c~-(~:s
I i/ Other ( 4) .Jl Other (8)
7 Silver L... o -Q5
Se. d; ra 1:,, tJ. -r 5(ff;~;: <O,().S-
(,. C q
I --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) P~eter Results~(mg/kg) Organic Compounds Results(mg/1)
I P&T:GC/MS ~senic L.. -~-~] benzene --_ Acid:B/N Ext. Barium ,t,-S-carbon tetrachloride --MTBE _IL'.'.Cadmium <' i ,, chlordane ----
I= Chloride chlorobenzene
✓Chromium --chloroform ·7·::,... "' . --~ ✓ Copper I J... o-cresol --Fluoride m-cresol ----Iron p-cresol
✓Lead --
I I
--.L.., ~() cresol --
--Manganese --1,4-dichlorobenzene
--?Mercury <'... 0. \ 1,2-dichloroethane
--Nitrate __ 1,1-dichloroethylene v Selenium L'._ ,, -'J --2,4-dinitrotoluene
I V Silver < /c heptachlor ----Radiochemistry Sulfates hexachlorobenzene
✓Zinc "J.}----hexachlorobutadiene --11 Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene ----
I J
TOC __ pentachlorophenol --
--__ pyridine
Microbiology --__ tetrachloroethylene
I Parameter
__ trichloroethylene
Results (Coi/IO0ml) --__ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ' ----
~-vinyl chloride ----endrin --lindane --Dale Received Reported by __ methoxychlor
I Dale Exlraclc<l
__ toxaphene
Dale ReQorted clU~l 1~-9 G 2,4-D 0'19>',S~ _ 2,4,5-TP (Silvex)
Dale Analy,cd Lab Number
DI !S JJIJI (llcvi$Cd 2/91) --I
REGION: IV P~OJ. LEAOER: I. WILLIAHS COHPANY: SUPERFUND
. ACTIVITY: li_ SPILL IO: PROJECT ID: __________ _
SITE NAHE: Greshams Lake
C[TY, STATE: Raleigh/Wake, NC
I
-----------------ti~-------------------------1 DATE SH[PPED: 06/)t'Ji96 CARRIER: Hand Delivered
I
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. AIRBILL: _____ _
SHIPPED TO: NC Public Health Laboratory
Bath Building
Wilmington Street
Raleigh I NC
ATTN: __________ _
PHONE: [phone]
LAB
DESCRIPTION
REGION: IV SUPERFUND
CHAIN-OF-CUSTODY RECORD
RE'' C /',;r-· , ....
1 VLj \ '-:::.J.)
AUG O 21996
HATRIX DATE/TIME SAMPLER I SAHPLE IO STATION
------------------------------=----------=-===========-==== =============== ========== ===============
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GL-005-SD Sediment
(2) GL·
HETALS(2J
30, 30
GL-005-
HETALS(2J Potable well -6583 Vineland GL·OO/-P
HETALS( 2) (2) GL-58, 58
GL-008-PW Potable Well -Lake Center
HETALS(2d
( 2) GL -61, 61
Sediment GL-105-s
HETALS(2J (2) GL-36, 36
(urtace Water GL-105-S 2) GL -33, 33 HETALS 2
Sediment 06-11/1150 H. ZINN
Surface Water 06-1171140 H. ZINN
Ground water 06-[[7[605 I. WILLIAMS
Ground Water 06-11/1700 [. W[LLIAHS
Sediment 06·1171150 H. ZINN
Surface Water 06-1171140 A. ZINN
I White -LAB Copy for Return to Samplers Yellow -LAB Copy Pink· Sampler's Copy Gold -Extra Copy
REGION: IV REGION: IV SUPE.t-<t-Ul'IU
P~OJ. LEADER: I. WILLIAMS COMPANY: SUPERFUND
ACTIVITY: ll__ SPILL ID: I PROJECT ID: __________ _
CHAIN-OF-CUSTODY RECORD
SITE NAME: Greshams Lake
CITY, STATE: Raleigh/Wake, NC
I
I
-----------------n , '/-----------------.-------ri.-ll"""' .DATE SHIPPED: 061-11/96 CARRIER: Hand Delivered
AIRBILL: _____ _ I SHIPPED TO: NC Public Health Laboratory
Bath Building
I
I LAB
SAMPLE ID I====,,===
Wilmington Street
Raleigh, NC
STATION DESCRIPTION
Preserv. Blank (2) GL-63, 63
Da.:fe. ,;.,..,
MATRIX OATE/TIHE SAMPLER
Other 06-11/1800 I. WILLIAMS GL-001-PB
METALS(2J
I GL-001-P
----l!HµET~AL'/J..S(¼,/2)___,~~--------....,.,-,=~--=-TT'T.'<,crr-.,,.-,n-mr-------GL-001-SD
Potable Well Ground water 06-ll/!loo I. WILLIAHS
(2) GL-39, 39
re1iment Sediment 06-ll/0815 R. ZINN
6 1----l!MµETA~L'/J..S( M2)___,~~=----------=~-=rc-c---=-.,.,..,.a-nr.,,.-,n-mr-------GL -001-Sil
2 GL -6,
Surface Water Surface water o6-ll/08l0 R. ZINN
(2) GL-3, 3
METALS( 2J
I Gl-002-P
----4~.sc.!.l:~::.;a~;l.l;;,gJ1-=~,r------------,.-~=--....,,.,~...,,.,,.,.,,...,,---,.,.,,,,----------
Potable Well Ground Water 06-11/0915 t. WILLIAMS
(2) GL-42, 42
(e1mnt Sediment 06-ll/!020 H. ZINN
l---...;~,;,c-'.;'.~;;,5~'"l.;.,gJ1--~-~~----------,.-=-~-~~~~~~---------
METALS( 2) I GL-003-PW
----+~"'t~,;;~~ijji"lg~J-""""=,,-------------,.-~=---,,,.,~'"",..,.....,..---rnrr __________ _
1---,~~c:"~~a5~lgcna-==:.r::=-----------,,=,.,.,,..,,.,..,.=---.,~.,,..,,.'"",......,,nm-----------
2 GL-12, 12
surface water Su rt ace water 06-lt/!0!5 H. ZINN
(2) GL-9' 9
Potable well Ground water 06-11/1000 !. wtll!ARS
(2) GL-45, 45
~e1uent Sediment 06-ll/!!05 H. ZINN 2 GL-18, 18
Surface water Surface water 06-11/[055 H. ZINN
(2) GL-15, 15
HETALs( 2) Potable Well -Charlie Brown's Ground Water 06-11/1140 I. WILLIAMS
( 2) GL -48, 48
Wetlands Sediment 06-ll/0915 H. ZINN
I METALS( 2) ----"G!),..L-L\\00"4"-'-sa.!Q----,----~-----~--~-~~~~~~-----------
MET ALS( 2)
(2) GL-24, 24
Surface water in wetlands Surf ace water 06-11/0910 H. ZINN
( 2) GL -2_1, 21
Potable Well-Century Precast Steps Ground Water 06-li/1400 I. wtlltARS
(2) GL-52, 52 I GL -005-PW
___ ...,H""E.,_,_TAecLS'-'-"-"2 '------------------------------------
1 White -LAB Copy for Return to Samplers Yellow -LAB Copy Pink -Sampler's Copy Gold -Extra Copy
r.· I
N.c. Oc:par.:mcnt o( Environment,
I lc::1lth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST St.ate Laboratory of Public HCalth
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, Nonh. c.a_rolina 27611
I Site N GL-001-SD 06/11/96 0815
Greshams Lake, NC I. WILLIAMS
SEDIHENT
GRAB ,ample Number _______________ _
Name .ocation ESD LAB METALS
6
Sediment -------------------I Callee GL-Co U e ct e d Time ----------------
I
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I ----
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate Comments ✓ Arsenic ~O.o I
I vBarium u,,o
__ Groundwater (1) Solid (5) ✓Cadmium <:Q.·QI-
I ~Surface water (2)
✓Chromium < C, 0 I-
_Liquid (6) vLead <'. 0, _/ (l
___::::::'Mercury ..t:....o_ c.. l
_Soil (3) _ Sludge (7) ✓ Selenium -< \
I ,/ Other ( 4)
./ Silver z (], {)_.( .
J!!!. Other (8) 54'; ,,, .,, n r V Cu t..,c.e.r <:' !) .. C, ~-V 7 t, Ii --:Z:.•nc
I --Organic Chemistry Inorganic Chemistry .. --
Parameter Results(mg/1) Parameter Resr"••wo 61''.mg/kg) Organic Compounds Resuits (mg/I)
I P&T:GC/MS V Arsenic .,< ":, -c., benzene
_ Acid:B/N Ext. ~Barium I /2 --carbon tetrachloride --MTBE ✓Cadmium < /0 chlordane ----
I --Chloride chlorobenzene
VChromium ----< /0 chloroform
7copper --
--< 1,, o-cresol --
I --Fluoride m-cresol ----
--~ron p-cresol --. Lead .-,:...-?,C• cresol ------
I --~anganese --1,4-dichlorobenzene
--__ Mercury ..L.._ 0-e:'7 1,2-dichloroethane
--v{'.itrate __ 1,1-dichloroethylene
Pselenium L_ -~ -<.7 2,4-dinitrotoluene
I : Silver ( /t __ heptachlor
Radiochemistry Sulfates hexachlorobenzene
VZinc I lf
--hexachlorobutadiene --
1 I Parameter Results (PCi/1) _pH hexachloroethane --I_ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ----
~ TOC __ pentachlorophenol --
--__ pyridine
Microbiology tetrachloroethylene ----I Parameter --__ trichloroethylene
Results (Col/lOOml) __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol ----vinyl chloride J-----endi-in --lindane --Date Received Reported by __ methoxychlor
loalc Extracted
__ toxaphene
· Dale Reported 2,4-D
0'1'1~8':' clO.½ I? 96 _ 2,4,5-TP (Silvex)
IDalc AnalyLcd Lab Number
Ill IS Jl'JI {Revised 2/91_) --
l
I .. Ocpnrtmcnt of Environment,
c:illh, &. Nalurai Resources
d Was1c Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P .0. Box 28047, 306 N. Wilmington Street
Raleigh, North. Carolina 27611
le Number_
GL-002-SD 06/11/96 1020 GRAB
Gresha•s Lake, NC !. WILLIAMS
Number _______________ _
SEDIMENT
Name of Site ESD LAB METALS Sediment
fnected By _____ G_L_-____ 12 .ad Time ----------------.
rency. Hazardous Waste Solid Waste __ Superfund TCLP Compounds
-----
Sample Type
Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments ✓Arsenic L.. c .. c.:...\
t Ground water (1)
·. VBarium . -, li,if::
_Solid (5) vcadmium < c,, r, \~
~urface water (2)
t,/'Chromium < {2, r, r
Liquid (6) VLead < C!,Lc,
vMercury ..,__ D.DI
_ Soil (3) _Sludge (7) . v'Selenium L. Q -\
~ Other (4) &other (8) S.r-d! : ~,, ~ rv •r vsilver < Q,~-s-
v c.~'ffLjr < Q .. 0-'.l
~ ?-t2 (__,., Q, i '.';1_
I --
Organic Chemistry Inorganic Chemistry
..
--
t=meter Results(mg/1) Parameter Results~ (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS V Arsenic .L., 'l -f, benzene
_ Acid:B/N Ext, '7Barium
--carbon tetrachloride /O --
MTBE 7cadmium < (6 chlordane
F
--
Chloride chlorobenzene
VChromium <Io --chloroform
?copper < /c
--o-cresol --
I= Fluoride m~cresol
--p-cresol --v{ron
--·-
Lead 4. ;)....(.) cresol --
I= ~anganese --1, 4-dichlorobenzene
__ Mercury .L-. c• -._-c-"1 __ 1,2-dichloroethane
--~itrate __ 1,1-dichloroethylene
I
9selenium .,,__ "':> .• <CJ 2,4-dinitrotoluene
Silver < i C __ heptachlor
Radiochemistry Sulfates hexachlorobenzene
VZinc
--
··--I if hexachlorobutadiene --
'Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene
~-
--TOC __ pentachlorophenol
--__ pyridine
--
Microbiology --__ tetrachloroethylene
I Parameter
--__ trichloroethylene
Results (Col/lO0ml) --__ 2,4,5-trichlorophenol
--
__ 2,4;6-trichlorophenol
--__ vinyl chloride
----endrin --lindane
Date Received Reported by = methoxychlor
I Date Extracted
__ toxaphene
Dale R(1~o~~f;f.1 JIJ~I 1: 9 G _2,4-0
I
2,4,5-TP (Silvex)
Date Analyzed Lab Number
Ill IS Jl'Jl (l(cv;scd 2/91)
--
I
I.C. Oepartmc:nl of Environment,
I k:ilth, &. Natural Resources
J!id Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P .0. Box 28047, 306 N. Wilmington Street
Raleigh, Nonh Carolina 27611
lile NUI
Name o
GL-003-5D 06/11/96 1105
Greshams Lake, NC I. WILLIAMS
GRAB rnple Number ________________ _
SEDIMENT
E5D LAB METALS
18
Sediment
:ation --------------------
I ollecte G L -ollected Time ----------------
rgency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
---
Sample Type lnori;anic Compounds Results(mg/1)
Environmental Concentrate Comments ✓ Arsenic -<-o.o'-1
I __ Ground water (1)
-./Barium {!_, ':/..S-
Solid (5) ✓Cadmium <O·Q-'
~urface water (2)
VChromium < ' --0,( .. :,.
Liquid (6) ✓Lead <0, IQ
i/ Mercury L.D.c.1
_ Soil (3) Sludge (7) =?selenium --<.O.j
I ✓ Other (4) £. Other (8) Se.cf..1/r>V>"r
ilver < o .. 1)-4 ,
-v§tfY' < Q, c r-
--"-'= i b. (,c 0, !1
I --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results~ (mg/kg) Organic Compounds Results(mg/1)
I-P&T:GC/MS V Arsenic L. 3.9 benzene --
Acid:B/N Ext. L Barium J. lf carbon tetrachloride --
MTBE ✓Cadmium < /c, chlordane
I
--
Chloride chlorobenzene
VChromium < /o --chloroform
✓Copper I fl
--o-cresol
----
I=
Fluoride m-cresol
~ran = p-cresol
--Lead .L.~0 cresol --
I=
~ anganese --1,4-dichlorobenzene
__ Mercury L_ C, -<'~, 1,2-dichloroethane
~itrate --1,1-dichloroethylene
--9se1enium L.. -,, .c-1 2,4-dinitrotoluene
• Silver < ic --heptachlor --
Radiochemistry Sulfates hexachlorobenzene
VZinc
--
.. -.--iii hexachlorobutadiene --
11 Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobenzene
----= pentachlorophenol
I TOC
I --
I --__ pyridine
Microbiology --__ tetrachloroethylene
I --__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol
--
----__ 2,4,6-trichlorophenol
I ----vinyl chloride
endrin --lindane --
I
Date Received
methoxychlor
I
Reported by --
--toxaphene
Date Extracted Dale Reiorted 2,4-0
00 -p,~,•_l JUN 13 9ti -2,4,5-TP (Silvex)
Date Analy,cd Lab Number
DI IS )!!JI (Revised 2/91)
--
i'<.C. Department of Environment,
I lc:illh, &. Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
Site Numb, GL-004-SD 06/11/96 0915 GRAB le Number Greshams Lake, NC l. W[LL!AHS
Name of Si WETLANDS on I
I
ESD LAB METALS Sediment
Collected E,, GL-24 ,cted
I Agency: Hazardous Waste Solid Waste __ Superfund --
Sample Type
Environmental Concentrate Comments
I __ Ground water (1) _ Solid (5)
I gSurface water (2) _ Liquid (6)
_ Soil (3) _ Sludge (7)
I ✓ Other (4) 1other (8) 5~/11:Je,h r
I Organic Chemistry Inorganic Chemistry
I
Parameter Results(mg/1) Parameter Results..,.i) (mg/kg)
_ P&T:GC/MS V Arsenic L. ''L'J
t(Barium _ Acid:B/N Ext. 3:J
MTBE ✓Cadmium <. /t' --I --Chloride
VChromium --<1c:.,
7copper --< /o
I --Fluoride ----~ron
---Lead ..:::::::J.c --
I --~anganese
' __ Mercury L.. c,_ c,':) . . I v{'.itrate --
I ~e[enium L.. ~. r-,
Silver < /1) --Radiochemistry Sulfates
VZinc ····--Lif_ I Parameter Results (PCi/1) pH --__ Gross Alpha Conductivity ----Gross Beta TDS --
I TOC --
--Microbiology
IParameter Results (Col/lOOml)
--
I= --
Date Received Reported by
Lale Extracted Dale Riorted ,IUN 13 96 O~ P,91\ Jalc Analy,cd Lab Number
11.S 31 1)\ (Revised 2/91)
State Laboratory of Public Hcal!h
P.O. Box: 28047, 306 N. Wilmington Slre::1
Ra.lei~. North Carolina 27611
Time
TCLP Compounds
Inorganic Com pounds Results(mg/1)
V Arsenic .f-.c,_-, c, 2, ·✓Barium 0.'-45
?cadmium ~O.Q.5'
I/Chromium ..:. .:, -c_::l:·
¾ad ,sQ-\0,
__ Mercury .L..C"-C:i
/Selenium .L. C,.! -r, ~
7si[ver ~ o . .s5
=z ~1:_'~ s: 0, Q {
_L "'-C', O"=l-
--,.
--
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --ch[orobenzene --chloroform --o-cresol --m-cresol --__ p-cresol
cresol --1,4-dich[orobenzec.c --1,2-dichloroethane --__ 1,1-dichloroethylene
2,4-dinitrotoluene --__ heptachlor
hexachlorobenzene --hexachlorobutadiene --hexachloroethane
__ methyl ethyl ketone
nitrobenzene
__ pentachlorophenol
__ pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin --lindane --
--methoxychlor
__ toxaphene
2,4-D --_ 2,4,5-TP (Silvex)
--
. ,' ,.,,.· .
,:·1.,.N.C.' Department or Environment,
/ I k:illh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
GL-001-SW 06/11/96 0810 GRAB
State Ulborntory oC PUblic Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, N~;:c.tiJJ!.. 2_7611
Ht: GI::: ' c---• I ~.; :. ·.. .· I Site Numi
Name of:
Gres hams Lake, NC I. WILLIAHS
SURFACE WATER
,pie Number ___________ -rr;--;--.s-::----
J UL O 3 1996
ESD LAB METALS Surface Water ,tioo __________________ _
GL-3 I Collected 1:>y _________ _
1 Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental · Concentrate . Comments Arsenic
I --Barium ---Cadmium __ Groundwater (1) _Solid (5) --
I V Surface water (2)
Chromium --Lead _ Liquid (6) --
-. --Mercury
_ Soil (3) _ Sludge (7) Selenium --
•-Other (4)
Silver --
_ Other (8) ----
I --
Organic Chemistry Inorganic Chemistry --'
Parameter Results(mg/1) Parameter Results(mg/1) I ,, g) Organic Compounds Results (mg/I)
I V Arsenic
bi
_ P&T:GC/MS <: D, o':i_ benzene
_ Acid:B/N Ext. 2Barium D, o:1 --carbon tetrachloride
MTBE 7cadmium <o.Qg-;l. --chlordane
--I Chloride --chlorobenzene --VChromium < 6, C, (
--chloroform --VCopper <o, o,< --o-cresol ----
I --Fluoride m-cresol
--~ron = p-cresol
Lead < o. ooc; cresol ------
I --~anganese --1,4-dichlorobenzene
--__ Mercury L.C-0005 1,2-dichloroethane
--~itrate = 1, 1-dichloroethylene
I
9se1enium < 6. 0 (" 2,4-dinitrotoluene
Silver 4-U _ C·5 = heptachlor
Radiochemistry Sulfates hexachlorobenzene
VZinc <o.o.C --hexachlorobutadiene
I
--
Paramekr Results (PCi/1) pH hexachloroethane ----
__ Gross Alpha Conductivity methyl ethyl ketone
Gross Beta ----nitrobenzene TDS ------penlachlorophenol I TOC --__ pyridine --Microbiology --__ tetrachloroethylene
I --__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --' 2,4,6-trichlorophenol ----= vinyl chloride
I ----endrin --lindane --
Date Received Reported by __ methoxychlor
I Date Extracted (Tu lvC!,,e __ toxaphene
Date Reported 2,4-0 --OGS[7~ c1U11l39 6 2,4,5-TP (Silvex)
I Dale Analy,cd Lab Number
DI IS 3191 (Revised 2/91)
--
·, .. j' ;.>~ /_ .
~, N.C. Ocp.artmc:nt of Environment,
I Ic:ilth, & Nalural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hc:i.lth
P.O. Box 28047, 306 N. Wilmington Strecl
Raleigh, Nonh Carolina 27611
GL-002-SW 06/11/96 1015 GRAB
.• Site Numbt Gres hams Lake, NC I. WILLIAMS le Number --------------
SURFACE WATER
Name of Si ESD LAB METALS Surface Water on __________________ _
I GL-9
Collected B, _________ _ acted __________ Time _____ _
1 Agency: Hazardous Waste Solid W a.ste __ Superfund TCLP Compounds
-----
Sample Type Inorganic Compounds Results (mg/I)
I Environmental Concentrate -Comments Arsenic --Barium ·,·, --
__ Ground water (1) _ Solid (5) Cadmium --
I V Surface water (2)
Chromium --
Liquid (6) Lead
.. Mercury
_ Soil (3) Sludge (7) --Selenium --
._ Other (4)
Silver --
_ Other (8) --
. --
I --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) fa11/i;g) Organic Compounds Results (~g/1)
I _P&T:GC/MS V Arsenic ~12.aY benzene --
_ Acid:B/N Ext. £Barium f),16. carbon tetrachloride --
MTBE ✓Cadmium <o .. co d chlordane
I --< --
--Chloride chlorobenzene
VChromium
--
--D D), chloroform
7copper
--
--<O,D C o--cresol --
I --Fluoride m-cresol --
--~ran p-cresol
--Lead 6,01( cresol ----
I --~anganese 1,4-dichlorobenzene --
--__ Mercury L C . OQC .5 __ 1,2-dichloroethane
--~itrate __ 1,1-dichloroethylene
I
9selenium < Q, IQ 2,4-dinitrotoluene
Silver 4..., CJ. c,.5 heptachlor
Radiochemistry Sulfates hexachlorobenzene
VZinc
--
I
L o,o.~ hexachlorobutadiene --
ParJmeter Results (PCi/1) pH hexachloroethane
__ Gross Alpha Conductivity methyl ethyl ketone
Gross Beta ----nitrobenzene
--TDS
I
--= pentachlorophenol TOC --__ pyridine --
Microbiology --__ letrachloroethylene
I --__ trichloroethylene
Parameter Results (Col/lOOml) __ 2,4,5-trichlorophenol --
--2,4,6-trichlorophenol
--= vinyl chloride
I ----endrin --lindane
I
Date Received Reported by = methoxychlor
I __ toxaphene
Date Extracted Date Rf!'~r;.,e.,') J!.!N 17 Q 6 2,4-D
!1 .. • ... , " 2,4,5-TP (Silvex)
Date Analyzed Lab Number
DIIS 3191 (Revised 2/91)
--
I N.t. Department or Environment,
lkallh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P .0. Box ~7, 306 N. Wilmington Stn:et
Raleigh, North Carolina 27611
I Site N GL-003-SW 06/11/96 1055 GRAB ,ample Number _______________ _
Gresha1s Lake, NC I. WILLIAMS
Name SURFACE WATER .ocation -------------------I Callee. E_5D' _L_A_s ____ M_E_T_~=-L=Lsc... __
Surf ace Water
15 Collected, ______ ___; ___ Time. ______ _
I Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic '
I Barium --Cadmium __ Groundwater (1) _Solid (5) --
I ( Surface water (2)
Chromium --Lead Liquid (6) --,. Mercury --
_Soil (3) _Sludge (7) Selenium --
I ~ther (8)
Silver
_ Other (4) <Sea~:, ,t ------
I --
Organic Chemistry Inorganic Chemistry .. --
I Parameter Results (mg/I) P/meter, Results(mg/1} ( (Jg) Organic Compounds Results(mg/1) Si
_ P&T:GC/MS · Arseruc ~-0-Q!:! benzene
Acid:B/N Ext, VBarium Q. l f:, --carbon tetrachloride
✓ Cadmium
--
I --MTBE < o. QQ ::;l chlordane
--V Chloride
--
--chlorobenzene --
Chromium 0, 0 J. chloroform
--7 Copper --
---< t,), i2.,C::-o-cresol
I Fluoride
--m-cresol
--
--7 rron = p-cresol
--Lead 0, o II cresol --
I --VManganese 1,4-dichlorobenzene --
--__ Mercury "':::ao ... acx~5 1,2-dichloroethane
--T Nitrate = 1,1-dichloroethylene
I Selenium ( 0, ID 2,4-dinitrotoluene
VSilver = heptachlor L:... o.o.5
Radiochemistry =:iZ: Sulfates hexachlorobenzene o. o c; --
I
Zinc hexachlorobutadiene --
Par.imeter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity = methyl ethyl ketone
Gross Beta TDS nitrobenzene --I --TOC __ penlachlorophenol --__ pyridine --Microbiology --__ tetrachloroethylene
I __ trichloroethylene
Parameter Results (Col/l00ml) --__ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol
----
I __ vinyl chloride
----endrin --lindane --
I
Date Received I
Reported by __ methoxychlor
__ toxaphene
Dale Exlraclc<l Dale Re~orted 2,4-0
O'l_r.74 JON 13 9b --_ 2,4,5-TP (Silvex)
Date Analy,cd Lab Number
DJ IS 3J!JI (Revised 2/91)
--
. /
',./... N.C'. Department o( Environment, -1 I Ic:illh, &. Natural Resources
· Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory o( Public Health
P.O. Box 28047, 306 N. Wilmington Strt:ct
Raleigh, North Carolina 27611
_,Site Numb
Name of S
GL-004-SW 06/11/96 0910 GRAB
Greshams Lake, NC I. WILLIAHS ,le Number ________ ~-------
SURFACE WATER IN WETLANDS
ESD LAB METALS Surface Water
100 __________________ _
I Collected l GL-21 ected Time ,__________ -------
.Agency: __ Hazardous Waste Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compounds R-esults(mg/1)
Environmental Concentrate , Comments Arsenic --I .. Barium --Cadmium __ Ground water (1) Solid (5) --I V Surface water (2)
Chromium --_ Liquid (6) Lead --
-· Mercury
_Soil (3) _ Sludge (7) --Selenium --1-Other (4)
Silver --Other (8) --
--
l --
Organic Chemistry Inorganic Chemistry -----
Parameter Results(mg/1) Parameter Results (mg/I)( g;ll,gj Organic Compounds Results(mg/1) I_ P&T:GC/MS V Arsenic ( O,CV benzene
°2Barium --Acid:B/N Ext. t>, D 8 carbon tetrachloride --MTBE 7cadmium < 0,() O), chlordane ----
I= Chloride chlorobenzene
VChromium < o. ot --chloroform
?copper --
--(/J. 0 '> o--cresol --
I Fluoride m-cresol ----
~ran p-cresol <o.oc,< --Lead cresol ------
I
~anganese --1,4-dichlorobenzene
__ Mercury J...C-C>or-..5 __ 1,2-dichloroethane
~itrate __ 1,1-dichloroethylene
9selenium <O,D S:: 2,4-dinitrotoluene
I Silver L...C, .c-5 __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
VZinc <i).oc: --
. -· hexachlorobutadiene --IParnmeter Results (PCi/1) _pH hexachloroethane --__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ----
I TOC __ penlachlorophenol --__ pyridine --Microbiology --__ tetrachloroethylene
farameler
__ trichloroethylene
Results (Col/lOOml) --__ 2,4,5-trichlorophenol --' __ 2,4,6-trichlorophenol ----
J=
__ vinyl chloride --endrin --lindane
Date Received Reported by __ methoxychlor
late Extracted
__ toxaphene
Dale Reported JU~! 1~ 9 b 2,4-D
00(lf'-75 --_ 2,4,5-TP (Silvex) Jate AnalyLcd Lab Number
I IS JJIJI (Revised 2/91) --
N.C. Department of Environment,
I lc:::ilth, & Natural Resources
Solid Wasle Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Site Num GL-005-SW 06/11/96 1140
Greshaes Lake, NC I. WILLIAMS
Name of SURFACE WATER
ESD LAB
GRAB ,pie Number _______________ _
1lion ----------------I Collected GL-
METALS
27
Surface Water
Uected Time
I Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic
I '. --Barium --__ Groundwater (1) Solid (5) Cadmium --Chromium
I V Surface water (2)
--
Liquid (6) Lead --,. __ Mercury
_Soil (3) Sludge (7) Selenium --
I Silver --
_ Other (4) _ Other (8) ----
I --
Organic Chemistry Inorganic Chemistry --
I Parameter Results (mg/I) Parameter Results (mg/I) ~gfllgj Organic Compounds Results (mg/I)
_P&T:GC/MS V Arsenic < o.oy benzene
_ Acid:B/N Ext. "'2_Barium --ti., t) "7-carbon tetrachloride
MTBE ✓Cadmium --< o.oa 1 chlordane
I ----
--Chloride chlorobenzene
VChromium --
--< o.o ( chloroform
7copper --
--<o, o s-: o-cresol --
I --Fluoride m-cresol --
--~ran p-cresol < 0,06,( --
--Lead cresol ----
I --~anganese 1,4-dichlorobenzene
--__ Mercury ..i..c_ce,o 5 __ 1,2-dichloroethane
~itrate __ 1,1-dichloroethylene --{Q,C)\ I 9se1enium 2,4-dinitrotoluene
Silver L.. C. 0.5 heptachlor --Radiochemistry Sulfates hexachlorobenzene
VZinc --< 0.9,:, hexachlorobutadiene --I ParJmth:r Results (PCi/1) pH hexachloroethane
__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Bela TDS --nitrobenzene ----I TOC __ pentachlorophenol ----__ pyridine
Microbiology __ tetrachloroethylene
I --__ trichloroethylene
Parameter Results (Col/lO0ml) __ 2,4,5-trichlorophenol --' __ 2,4,6-trichlorophenol ----
I
. __ vinyl chloride ------endrin
lindane --Date Received Reported by __ melhoxychlor
I " __ toxaphene
Dole ExlroclcJ Dale R~orled 2,4-0 JU~l 13 ~ 6 --()'1 ! r;7r:; _ 2,4,5-TP (Silvex)
I Dole Analy,cd Lab Number
IJI IS 3191 (Revised 2/91) --
. -,_ C. Department of Human Resources
Division of Health Services
I
SAMPLE ANALYSES REQUEST
State Laboratory of Public He::ilth
P. 0. Box 28047
306 N. Wilrningcon Street
Raleigh, 2761 I
Site Number .;,C,,:·•_,l=---___,_),.Q.,__,,,5"----=S.,_'::½,J=-\'-----------Field Sample Number-----------------
Site Location __________________ _ lme of Site _;G,..,-'-"',Cf-Sl-=,....Sh=o"'rm,;;,:=,,._,_, ____,_d,=.o,9,,;..&,;;=,.,__ ____ _
Collected By _::r:_.__ __ ,.,,,._,,~,_,o.,q,._,L9:!"'-<S8° ==--ID#------Date Collected __ <,,_,9_-__._,~1_-_9_,_t,=-----Time I ·, ·, 'i p
lpe of Sample:
Environmental
1---Groundwater (I)
-6urface Water (2)
1--Soil (3)
__ Other (4)
I Extractable,
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Parameter Results mg/ l Parameter Results mg/ l
~Arsenic
Comments
Total
Parameter Results mg/1
.,,/ Silver ....!._O -.... -:' c:;_·
l=Arsenic <'.'.D,Q~
1--Barium ---=::Barium ~,~t-i-__ Sulfaces
.-Cadmium . ~admium -=:'.1inc <D,D~
_Chromium __ Chloride _Ph
__ Lead ~hromium < Q, b I __ Conducrivicy
1--Mercury < o.o,C _TDS _·_copper
l=Selenium __ Fluoride _TOC
Silver __ Iron --
I-__ '.'.'fead ~ Q.Oo,\ --
I= __ Manganese --
_ ""'Mercury .L...D.,!:2Qt:'~ 5 --
1-
__ Nirrate --
--~leniu~ ~ b-0 ~ --
. ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/ l Parameter Results mg/ 1
1-P& T:GC/MS _EDB __ Methoxychlor
__ Acid:B/N Ext. __ PCB's __ Toxaphene
i: TOX
__ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (siivex)
__ Lindane ----
I MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/ 1
.-(MF) Coliform Colonies/!00mls __ Gross Alpha
-(MPN) Coliform Colonies/!00mls __ Gross Beta
--, __
I --
Dare Received -------------------Dare Reported __________________ _
.• te Extracted __________________ _ Date Analyzed __________________ _
Reported By --------------------Lab Number
IS 319! (Revised 7/85)
: 1J anJ Hn::irdous Wa.sre (Review 7/87)
N.C.' Oep::irtmcn( of Environment,
I I lc::ihh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Stn:ct
Raleigh, North Carolina 27611
Site N GL-001-PW 06/11/96 1100
I Gres hams Lake, NC I. WILLIAMS
GRAB Sample Number _______________ _
POTABLE WELL ..ocation Name· ESD LAB METALS
39
Ground Water -------------------I Callee. GL-Co II e ct e d Time ·-----------------
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I -----
Sample Type Inorganic Compounds Results (mg/I)
Environmental Concentrate -Comments Arsenic --I V Ground water (1)
Barium
'Dr;ry 1::-•n; lJvt'!,r --Cadmium _Solid (5) --Chromium --Lead 1--Surface water (2) _ Liquid (6) --.. --Mercury
_Soil (3) _ Sludge.(?) Selenium --I-Other (4)
Silver --_ Other (8) --
--
--I Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) ( g;'llg} Organic Compounds Results(mg/1)
I P&T:GC/MS ✓ Arsenic <'.c, O\{ benzene
_ Acid:B/N Ext. ✓Barium --/), 0 (, carbon tetrachloride --MTBE __iL Cadmium <6.oc,), chlordane ----
I --Chloride chlorobenzene
✓Chromium --
--a" bl chloroform
✓copper <o. os---o-cresol ----
I, --Fluoride m-cresol ----Iron __ p-cresol
--v Lead < Q. 00,(° cresol ; --
1'1= Manganese --1,4-dichloroben::ene
✓Mercury .,L O • C, D Q =:;i 1,2-dichloroethane
Nitrate = 1,1-dichloroethylene
V"Selenium <o, os: 2,4-dinitrotoluene ✓Silver --r ,L__o-r,S heptachlor
Radiochemistry ----
Sulfates hexachlorobenzene
~Zinc <o. o,( --hexachlorobutadiene --I Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity --. methyl ethyl ketone
__ Gross Beta TDS --nitrobenzene --
t TOC __ pentachlorophenol --__ pyridine ' --Microbiology ----tetrachloroethylene
I Parameter
__ trichloroethylene
Results (Col/lO0ml) --__ 2,4,5-trichlorophenol --2,4,6-trichlorophenol ------vinyl chloride .-----endrin --lindane --Date Received methoxychlor Reported by --
loatc Extracted
toxaphene --
Date Re~~~ _ I' '1/ ! ,.. q b 2,4-0 n~ .... ,ei Lc1, _l. = 2,4,5-TP (Silvex)
.Dale Analyzed Lab Number
DI IS 3191 (Revised 2/91) --
N.C. • Department of Environment, 1 1 fcallh, & Natural Re.sources
Sulid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box ·28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
•
Site J GL-002-PW 06/11/96 0915 GRAB
Greshams Lake, NC I. WILLIAMS
Sample Number ________________ _
Nam-POTABLE WELL
ESD LAB METALS Ground Water
Location. __________________ _
I Colle GL-42 -• Collected Time
I Agency: --Hazardous Waste Solid Waste __ Superfund TCLP Compounds
Sample Type Inorganic Com pounds Results (mg/I)
Environmental Concentrate , Comments Arsenic --I Barium .,
V Ground water (1) 'Dr:~ ~•n 1 l.Ja..,,f"e.,r --Cadmium _ Solid (5)
u --Chromium --Lead 1--Surface water (2) _Liquid (6) --.. --Mercury
_Soil (3) _ Sludge (7) Selenium --1-Other (4)
Silver --_ Other (8) ----
II --
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/JHmg(lml Organic Compounds Results (mg/I)
I_ P&T:GC/MS ✓ Arsenic {O,DLj benzene
I _ Acid:B/N Ext. V"'Barium --6,D' carbon tetrachloride --MTBE _iL Cadmium (0,00 ".'1, chlordane
I
--Chloride chlorobenzene
✓Chromium < o.o; --chloroform
✓copper --
--<o,o, o-cresol --
I=
Fluoride m-cresol --Iron __ p-cresol
v Lead < O.or,;,S:'" cresol ----
1= Manganese 1,4-dichlorobenzene
i?'Mercury --
.L...,Q .. DOD :'5 1,2-dichloroethane
Nitrate = 1,1-dichloroethylene
,.,/Selenium <o.o C 2,4-dinitrotoluene
t ✓Silver --heptachlor .L..0 .. 1-5 --Radiochemistry Sulfates hexachlorobenzene
V°'Zinc < o, o.< --hexachlorobutadiene ----
IParnmeter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobenzene ----
I TOC __ pentachlorophenol --
--__ pyridine
Microbiology __ tetraehloroethylene ' --
IParameter
__ trichloroethylene
Results (Col/lO0ml) --__ 2,4,5-trichlorophenol --
' 2,4,6-trichloropbenol ----= vinyl chloride
I= --endrin --lindane --Date Received Reported by methoxychlor --
IDate Extracted
toxaphene --Date Reported 2,4-0
(1','}P.7'.:I JON l'J Y 6 -2,4,5-TP (Silvex)
.Date Analyzed Lab Number
JI IS 3191 (Rcv;scd 2/91) --
N.C:Oepartmcnt of Environment, I I lc::ihh, &. Nalural Rcsourcc..s
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Stri:.et
Raleigh, North Carolina 27611
.Site Nt
Name -
GL-003-PW 06/11/96 1000
Greshams Lake, NC I. WILLIAMS
POTABLE WELL
GRAB :ample Number _______________ _
ESD LAB Ground Water
Jcatioo __________________ _
I Collect GL-
METALS
45 Collected __________ Time _____ _
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate . Comments Arsenic --I Barium V Ground water (1) 'Dr:~ t,n '!: u.}a.,t'e.,r --Cadmium _ Solid (5)
<) --Chromium --Lead I-Surface water (2) _Liquid (6) --
--Mercury
_Soil (3) Sludge (7)
·• Selenium --Silver 1--Other (4)
--_ Other (8) --
--
l --Organic Chemistry Inorganic Chemistry ---·
Parameter Results(mg/I) Parameter Results(mg/1)~ g;'llg) Organic Compounds Results (mg/I) 1:-P&T:GC/MS ✓ Arsenic {o,oY benzene
v Barium --_ Acid:B/N Ext. D,Q 8 carbon tetrachloride I --MTBE ---1..L. Cadmium < o. ,)c, ·J; chlordane ----I= Chloride chlorobeozene
✓Chromium ,;::_ a, O I --chloroform
✓Copper <o. o s~ --o-cresol ----
I= Fluoride m-cresol --Iron __ p-cresol
v Lead Q .-C, 0 '::1-cresol ----
F Manganese 1,4-dichlorobenzene
v'Mercury --1,2-dichloroethane 2.... C -..:::, c,. c-,:o,5
Nitrate = 1,1-dichloroethylene
9se1enium { Q,lO --2,4-dinitrotoluene
I Silver L ,,-~ -CL5 heptachlor ----Radiochemistry Sulfates hexachlorobenzene
v"Zinc --<O-O!;. hexachlorobutadiene --
[:meter Results (PCi/1) _pH hexachloroethane
Gross Alpha __ Conductivity --methyl ethyl ketone --__ Gross Beta --TDS nitrobenzene
TOC __ pentachlorophenol ----__ pyridine
Microbiology tetrachloroethylene ----
l.1rameter
trichloroethylene
Results (Col/l00ml) ----2,4,5-trichlorophenol ----2,4,6-trichloropheool --' ----vinyl chloride
F ----endrin --lindane --Date Received Reported by --methoxychlor
late Extracted --toxaphene
Date Reported 2,4-D
oagP.t:LJ JUN l'J 9b = 2,4,5-TP (Silvex)
'ale Analyzed Lab Number
I IS 3191 (Revised 2/91) --
N.C.' Dep::i.nmcnt of Environment,
11 lcallh, & Nalural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. BoJt 28047, 306 N. Wilmington Street
lulcigh, North Carolina 27611
ISite Nu,
Name o
GL-004-PW 06/11/96 1140
Greshams Lake, NC I. WILLIAMS
GRAB tIDple Number _______________ _
POTABLE WELL -CHARLIE BROWN'S
ESD LAB METALS Ground Water
48
cation. __________________ _
ICollecte GL-:ollected __________ Time _____ _
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I -----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate . Comments Arsenic --I V Ground water (1)
.,-. Barium
1)r;~ /::..,11-r: lJa..,,-r6r --Cadmium _. Solid (5)
u --Chromium --Lead 1--Surface water (2) Liquid (6) --
.. --Mercury
_Soil (3) Sludge (7) Selenium --Silver 1--Other (4) --Other (8) --
----l Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/I) ( HJ' gl Organic Com pounds Results(mg/1) I: P&T:GC/MS ✓ Arsenic <o, ◊4 benzene
v'Barium --_ Ac,d:B/N Ext. o, ol/ carbon tetrachloride --MTBE _LL. Cadmium <o.oo;;i chlordane ----
I= Chloride chlorobenzene
✓Chromium ✓;,,DI --chloroform
✓copper --
--Q, Q" o-cresol --Fluoride m-cresol I= --= p-cresol Iron
✓ Lead O,OD(p cresol ----Manganese 1,4-dichlorobenzene
F 7Mercury --1,2-dichloroethane L... b • .::::::,c:,n ,5
Nitrate 1,1-dichloroethylene
1,/"'Selenium <o,OS:-2,4-dinitrotoluene
I ✓silver < c,.n.5 = heptachlor --Radiochemistry Sulfates hexachlorobenzene
--V-zinc --0, i'-l hexachlorobutadiene
Results (PCi/1) ----
r::me!er _pH hexachloroethane
Gross Alpha __ Conductivity --methyl ethyl ketone --Gross Beta TDS nitrobenzene --TOC __ pentachlorophenol ------pyridine
Microbiology --__ tetrachloroethylene
larameter
trichloroethylene
Results (Col/lO0ml) --2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol I ----vinyl chloride
I ----endrin ' --lindane --Date Received Reported by __ methoxychlor
late Extracted
__ toxaphene
Date Reported 2,4-0
n0ci P[11. JUN 1'39 b = 2,4,5-TP (Silvex) f atc Analyzed Lab Number
I IS Jl1JI (Revised 2/91) --
)
N.<;.'Dcpanmcnt o( Environment,
l lk:ilth, & Natural Resources
· olid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
GL-005-PW 06/11/96 1400
Greshams Lake, NC I. WILLIAMS
POTABLE WELL-CENTURY PRECAST STEPS
GRAB Sample Number _______________ _
ESD LAB METALS
Location --------------------
GL-
Ground Water
52 : Collected. __________ Time _____ _
Agency: --Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I Sample Type Inorganic Com pounds Results(mg/1)
Environmental Concentrate . Comments Arsenic --I V Ground water (1) .
·:, Barium '
Solid (5) 1)r;~ /::.!n,r t.,Ja.,,-t!;r Cadmium
u --Chromium --Lead t-Surface water (2) _Liquid (6) --Mercury
_Soil (3) Sludge (7)
. --Selenium --
1--Other (4)
Silver --
Other (8) --
-----l Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1)(~ Organic Compounds Results(mg/1) I P&T:GC/MS ✓ Arsenic h~b:!i benzene
_ Acid:B/N Ext. v'Barium
--carbon tetrachloride --
MTBE _JL.Cadmium <o,oo?. chlordane ----
I:
Chloride chlorobenzene
✓Chromium <0.01 --chloroform
✓Copper --
--< o. Q,C:-o-cresol --
I= Fluoride m-cresol --= p-cresol Iron
✓ Lead <0.COi cresol ----
F
Manganese --1,4-dichlorobenzene
✓Mercury .t_ C--c-c.o,5 1,2-dichloroethane
Nitrate --1, 1-dichloroethylene
✓selenium < O, l C 2,4-dinitrotoluene
I VSilver L..c~.(._--:-i J __ heptachlor
Radiochemistry Sulfates hexachlorobenzene
--i:;::,-Zin c o,or --hexachlorobutadiene
[:meter
--
Results (PCi/1) _pH hexachloroethane
Gross Alpha __ Conductivity = methyl ethyl ketone
Gross Beta TDS nitrobenzene --
I TOC __ pentachlorophenol --
--pyridine
Microbiology __ tetrach!oroethylene --
IParameter
__ trichloroethylene
Results (Col/l00ml) --__ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol --' --__ vinyl chloride
F --endrin --lindane --
Date Received Reported by --methoxychlor
loatc Extractcu
toxaphene. --
0
011~f'l?~d c1u11 1 s 9 b 2,4-D = 2,4,5-TP (Silvex)
Dale Analyzed Lab Number
DI IS 3191 (Revised 2/91)
--I
I
I
N.c.· Department o( Environment,
llcalth,·& Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Labor.uory of Public Health
P.O. Box 28047, 306 N. Wilmi~gton Street
Raleigh, North Carolina 27611
I SiteN1 GL-006-PW 06/11/96 1445
Greshams Lake, NC !. WILLIAHS
Name POTABLE WELL -BILLINGS & GARRETT
GRAB ample Number _______________ _
Jcation
ESD LAB METALS
GL-
Ground Water
55
-------------------I Collect Co II e ct e d Time ·-----------------
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds
I ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate -Comments Arsenic --I Barium V Ground water (1)
,_
1)r;~ 1::-, n 'f. /.JJa.,,,t"(.,r --Cadmium _ Solid (5)
<.J --Chromium --Lead 1--Surface water (2) _ Liquid (6) --
--Mercury
_ Soil (3) Sludge (7) .. Selenium --
•-· Other (4)
Silver --_ Other (8) --
--
--I Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results (mg/Ii 'JIIR {kg} Organic Compounds Results (mg/I)
I _P&T:GC/MS ✓ Arsenic < Q, 0~ benzene
_ Acid:B/N Ext. v'Barium Q, Q.< --carbon tetrachloride
MTBE _iL_ Cadmium / Q. O=◊ 1. --chlordane ----
I.= Chloride chlorobenzene
✓Chromium --chloroform ~ Q. QI ✓copper -< (!, Q < --o-cresol ----11-. Fluoride m-cresol --
1-Iron __ p-cresol v Lead < O, DOS" cresol ----
I
Manganese --1,4-dichlorobenzene
✓Mercury L..C 1 i:::::C!O 5 1,2-dichloroethane
Nitrate = 1,1-dichloroethylene
9se1enium < D., 0,£◊ --2,4-dinitrotoluene
r Silver ..::::..o.,c.;,_5 heptachlor ----Radiochemistry Sulfates hexachlorobenzene
V'Zinc < o. o< -----hexachlorobutadiene --I Parameter Results (PCi/1) _pH hexachloroethane
__ Gross Alpha __ Conductivity methyl ethyl ketone
Gross Beta TDS --nitrobenzene ----
~ TOC __ pentachlorophenol --
--__ pyridine
Microbiology tetrachloroethylene ----I Parameter --__ trichloroethylene
Results (Col/lO0ml) __ 2,4,5-trichlorophenol --__ 2,4,6-trichlorophenol --' --__ vinyl chloride ,---endrin --Iindane --Date Received Reported by methoxychlor --
loate ExtraclcJ
toxaphene --Dale Reported 2,4-0 --~ O'J-lP.83 cllJN 1J96 2,4,5-TP (Silvex)
'Dale Am1lyLcd --Lab Number
ll IS 319l (ttcv;scd 2/91) --
N.I. ~epartment of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
Scace Laboratory of Public He:ilrh
P. 0. Box 28047
306 N. W Limington Street
Raleigh, 27611.
I Site Number (', L -O o7 -P'-'.l Field Sample Number-----------------
Nie of Site
C ecced By
Site Location __________________ _
:I. '-"--' , a Q ,;..,,..,,, ID# ______ Dace Collected --~l~,,__~·~l ~l _-_'9~_G,'----Time ....!...h o..5
Tl of Sample:
vi/ental
---Groundwater (1) I-Surface Water (2)
__ Soil (3) I-Other (4)
Concentrate
__ Solid (5) .
__ Liquid (6)
__ Sludge (7)
__ Other (8)
GL-.SB
INORGANIC CHEMISTRY
Comments
I ' Extractables
Total
Parameter Results mg/1
'=Arsenic
Barium
__ Cadmium ·I= Chromium
Lead
__ Mercury
l=Selenium
Silver
--
.I=
--
Parameter Results mg/ 1
EP&T:GC/MS
__ Acid:B/N Exe.
_TOX
I=
MICROBIOLOGY
Parameter
--(MF) Coliform Colonies/l00mls I= (MPN) Coliform Colonies/!00mls
Parameter Results mg/ 1
~rsenic < O. Oi./
__ Barium O..· ~B
--.k'Cadmium C..rJ, D 2
__ Chloride
~hromium ~.-Q,QI
~opper !(12., Q (~
__ fluoride
__ Iron
_v(.;ad ~ Q,. Q o.s-
__ Manganese
-~ercury .L.o ~ oao. 5
-~trace
__ Selenium < 0, f()
ORGANIE: CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/ 1
Parameter
__ Gross Alpha
_· _ Gross Beta
Parameter Results mg/1
-':'.'.'.Silver ""-C•. c,..5
~!fates
__ Zinc (), t4'
_Ph
__ Conducciviry
_TDS
:
_TOC
----
----
----
Parameter Results mg/ 1
__ Mechoxychlor
__ T oxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ 1
are Received ___________________ Dace Reported __________________ _
Ire Exrracted -------------------Date Analyzed
!porred By -----------------Lab Number __ (1_'1~.Cl~f'_.,r--:~~~4~,I_/J_N~l~1~9~6'--------
IS 3191 {Revised 7/85)
J anJ H:i.:ardous Waste (Review i /Si)
N.c.·oepartmcnt C!f Environment,
I I Icalth, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST State Laboratory of Public Hc:ilth
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
. GL-008-PW 06/11/96 1700 GRAB
I Site 1' Greshams Lake, NC I. WILL!AHS
Sample Number _______________ _
POTABLE WELL· LAKE CENTER
Name ESD LAB METALS Ground Water :...Ocation -------------------
I GL-61 Callee .. _ -,___________ _ __ _ ; Collected Time ----------------
Agencv: Hazardous Waste Solid Waste __ Superfund TCLP Compounds I ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental. Concentrate , Comments Arsenic --I Barium
V Ground water (1) 1),.-~ i:.•v lJvf'e.,r --
Solid (5) Cadmium --Chromium --Lead 1--Surface water (2) _Liquid (6) ----Mercury
_ Soil (3) Sludge (7) . -Selenium --. Silver 1-· Other (4)
--· Other (8) --
----l Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results(mg/')Gs,i,l Organic Compounds Results(mg/1)
I_ P&T:GC/MS ✓ Arsenic <0,.04 benzene
v'Barium --_ Acid:B/N Ext. /;.%~ "J_
carbon tetrachloride --
--MTBE ~ Cadmium chlordane --1_ Chloride chlorobenzene
✓Chromium < Q, r;; I --chloroform
✓Copper (), /} --o-cresol ----
I= Fluoride m-cresol --Iron __ p-cresol
v Lead < Q, DCC cresol ----Manganese 1,4-dichlorobcnzene
1= ✓Mercury --
.l....c .,DC,D...5 1,2-dichloroethane
Nitrate --1,1-dichloroethylene
9se1enium < e. o..ro 2,4-dinitrotoluene . r Silver '-C) -ci_=i __ heptachlor --Radiochemistry Sulfates hexachlorobenzene
--i::;;,--Zin c ? I).()~< --hexachlorobutadiene ----
.Parameter Results (PCi/1) pH hexachloroethane ----__ Gross Alpha --Conductivity methyl ethyl ketone --Gross Beta TDS nitrobenzene ----
I TOC __ pentachlorophenol ------pyridine
Microbiology --__ tetrachloroethylene
tarameter --trichloroethylene
Results (Coi/lO0ml) --2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol ----' vinyl chloride
F ----endrin --lindane --Date Received Reported by methoxychlor --
ialc ExlrJclc<l
toxaphene --Dale Reported 2,4-0
n0~r.0.5 ,JUN l'J 9 6 --2,4,5-TP (Silvex) --Fate Analyzed Lab Number
I IS 31'!1 (Rcv;scu 2/91) --
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i':'.C. Dep.ir1ment of Environment,
I Ic.illh, & Natural Resources
Solid Waste Management Division
SAMPLE ANALYSIS REQUEST
Site GL-001-PB 06/11/96 1800 GRAB · i Sample Number
Greshams Lake, NC I. WILLIAMS
Nan PRESERV. BLANK Location
ESD LAB METALS Other
Coll GL-63 te Collected
Agency: Hazardous Waste Solid Waste __ Superfund ----
Sample Type
Environmental Concentrate Comments
__ Groundwater (1) Solid (5)
__ Surface water (2) _Liquid (6)
..
_Soil (3) Sludge (7)
i/ Other (4) Other (8) J.hJv ' 3 f;.--,,.<;erl'"'-b v'L OitL.J
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) P✓meter Results(mg/1)(; mil g)
_ P&T:GC/MS · Arsenic f%o1! ,7 Barium _ Acid:B/N Ext.
/Cadmium < ,ol
MTBE cJ.oo-:i._ ----Chloride --✓Chromium < o. ◊ I --
--✓Copper <o,o.r::
Fluoride ----Iron --✓Lead ( Q, oc,C --Manganese --
--✓Mercury ..t..._ O_c:,c,C...:,.$
Nitrate --V Selenium < Q. o,r-c
?silver L. c~ ~c•.::5
Radiochemistry Sulfates
//Zinc ,:(o.o,S: ····---
Parameter Results (PCi/1) _pH
__ Gross Alpha --Conductivity
Gross Beta TDS ----TOC ----Microbiology --
--Parameter Results (Col/lO0ml) --
----
----
Date Received Reported by
Date Extracted Date Reported
0'1'1.P.IJ6 JJl-11'!96
Date Analyzed Lab Number
DI JS 31')1 (Revised 2/91)
State Laboratory of Public Health
P.O. Box 28047, 306 N. Wilmington Street
Raleigh, North Carolina 27611
Time
TCLP Compounds
Inorganic Compounds Results(mg/1)
Arsenic .--Barium --Cadmium --Chromium --Lead
__ Mercury
Selenium --Silver ----
--
--
--
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o--cresol I --m-cresol
__ p-cresol
cresol --1,4-dichlorobenzcne I ----1,2-dichloroethane
__ 1, 1-dichloroethylene
__ ., 2,4-dinitrotoluene
--heptachlor
hexachlorobenzene --hexachlorobutadiene --hexachloroethane
methyl ethyl ketone
--nitrobenzene
__ pentachlorophenol
--pyridine
__ tetrachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
__ vinyl chloride
endrin --lindane
__ methoxychlor
--toxaphene
2,4-D --2,4,5-TP (Silvex) --
--I
NC .D~•nmcnI ,of Environment,
. H,C;-llU!., & N1.tural Rc.wurcc,
Solid Wui.c Mana~cmi::ru Divi,ion
SAMPLE A.~ALYSIS REQUEST SL.ate Labor.a1.0ry of Public He-111.h
P.O. Box :?RO-;?, 306 N. Wilmin,:t.on St.
R1.lciJ,;h, Nonh Carolin.a 27611-8047
I Sit.e Number--------------Su.mp le ID Number/Name _J.0)_,_,_· ..:(_,.==------=o=-..:o:......:./_---'s__I)='===':__--I-/_---
Name of Sit.e ~fJ ?0-ztA.. d{"a,/-1 ... Co!kctod By __________ ~_ !D# ___ I_.,__ __
I Sit.el.owion tf2,:;h,11~b124& /i•Oatc Co~td__,/,'"",;_-_/'-'/-;:-:=7:::::::(p======T,.:.:_tm=e=========-
I
Agency: Hazardous Wa.st.e Solid Wa.st.e _V_ S 'uperfund TCLP Compounds
Sample Type
Environment.ii
I Ground Water (I)
I Surface Water (2)
Soil (3)
I ✓Other (4)
All.~
Concentrate Comments
Solid (5) 1/o ~~
Llquid (6) £U/~ ~
Sludge (7) _,,tl~,!z . ~
Other (8)
Organic Chemistry Inorganic Chemistry
Parameter
I 1,/""' P&T:GC/MS
Acid:B/N Ext.
2,4-D
I
2,4,5-TP(Silvex)
chlordane
beptuchlor
hc:xachloro ben.2ene
Results (mg/I)
-------
hc:xachlorobuLadic:nc ~------
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endrin
lindane
mcthoxych!or
toxaphc:nc
FOR LAB USE ONLY
I Date Receivod
Date Extractod
I
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----------
1 Lab Number
Di!SJl91 (Rcvi~cd l~/9J)
Parameter Results(mg/l)(mg/kg)
anLimony
ursc:ruc
barium
beryllium
cadmium
chloride
chromium
cob.It
copper
fluoride
iron
kad
nu.ngani:!S:: -------
mc:rcury
nickd
nilralc
selenium
silver
.sulfutc:s
thallium
vanadium
2.inc
pH
conductiviry ______ _
TDS
1l1c.:h point
lnor;:anic CompoW1d,; Result.s(mg/1)
arsenic
barium
cadmium
chromiR,E('•-n 1,::--
l""d
mercury
se!c,uumJ UN ~ ::i i!:J!:Jb ----'-'..C...C'------
.silver
SUPEF?ft'Ji\l(i ,i..';.:,-:i-:r,,r,;
Organic CompOW1ill
bcll2t:ne
carbon tetrachloride
chlordane
chlorobcnz.enc:
chloroform
a-ere.sol
m-crc:sol
p-<:resol
crc:so!
Result.s(mg/1)
1,4-dichlorobenune ______ _
1,2-dichloroc:thanc
l, 1-dichloroethylcne ______ _
'.!,4-dichloroetbylene ______ _
hept.<chlor
hex.ach..lorobcnzcne
hc:xachlorobutadiene
hexachloroetbane
methyl e;hyl ketone
nitrobc:ru.cne
penLUchlorophenol
pyridine
tetrachloroethy lene
trichloroc:Lhylcne
---'------
2,4,5-trichlorophenol ______ _
2,4,6-trichlorophc:nol ______ _
vinyl chloridc:
cndrin
!indane
methoxychlor
toxaphenc
'.'.,4-D
2,4,5-TP (Silvex)
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NC .D~anmcnt _of En\lironrncnt,
H,e;a,lrJl, &. Natuul R~urcr.,
Solid Wulc Mana.-cmr;;ru Divi,ioo
SAMPLE ANALYSIS REQUEST SLa~ Uboratory of Public Hc:.a.lth
P.O. Box 28047, 306 N. Wilmini;t.on Sc.
R.alr.i;;h, North Carolin,, 27~11-8047
Si1.eNumbcr ______________ SampldD Number/Name _ _,,Vl=<..:....::L:::_-_,O::....,O"--..J,.,__=---5L.J2..J-/.._ ___ _
NameofSi1.e ~/2 C0:::?:L::?-o{'a,l;J __. Oilloctc<lBy _________ ~_ID# / 0
SiLcLoc:.>tion 6< cJ!.v... -~/;,U/1 h foQa1.eCollocl.Cd '--->-I ✓Superfund Agency: H=dous WasLc Solid Waste TCLP Compounds ----
Time
Sample Type lnor,:anic Compow1ds Resu.lt.s(mg/1)
Environment.'11 Concentrate Comments -arsewc
barium -
Ground Water (I) Solid (5) -cadmium --chromium -
Surface Water (2) Liquid (6) -lead ---mercury
Soil (3) Sludge (7) -se:len.ium --
/ Other (4)
-:;ilvcr
Other (8) --
/41.e. ,;;Lu-~ --
Organic Chemistry Inorganic Chemistry -..
P~eter Results (mg/I) Parameter Resu.!ts(mg/l)(mg/kg) Organic Compounds Rcsult.s(mg/1)
_ P&T:GC/MS antimony -bt:nunc: -
Acid:B/N Ext. 11.rsenic -carbon tetrachloride ---2,4-D barium -chlordane -
-2,4,5-TP(Silvex) -beryllium -ch.lorobcn.uni;:
chlordn.nc cadmium ch.loroform ---
-beplJlchlor chloride -o-crc::;ol -hc:xach.loroben.z.ene chromium -m-crc.:ml --
-hex.ach.l oro bu tadi enc cobalt p-cresol --
-endrin copper Cfc!:iO! --
lindane fluoride 1,4-dichlorobenz.::ne ---
-meLhoxychlor iron -l ,2-dichlorocthane --tox.aphene lead -1, 1-dichJoroethylenc ---manganese -2, 4-di chloroc:th y lcne
-macury hep~chlor --
-nickel hcx.achlorobcn.z.c::nc --
-nitraLG hexachlorobuta<liene --selenium hexach.loroelhune --silver --methyl e;hyl ketone
FOR LAB USE ONLY -.sulfates nil robenune -
& -p-'7[p &LO
thallium penl.!l.chlorophenol --
Date Received vanadium pyridine --
z.inc tetrachloroethylcne --Date Extracted pH trichloroethylenc ---conductivity -2,4,5-Lrichloropheool
Dale Analyw:l (o-/ 9-91.JJ 714[ TDS 2,4,6-trichlorophenol ---1111.:ih point -vinyl chloride
Reported By . cnJrin --lindane --
Date Reponed -methoxychlor -':c.: ·,, ~ 13 -Loxaphcoe -Lab Number ...J '._,}.J,... 2,4-D --
--2,4,S·TP (Silvex)
D11S 319l (Rc:viicd l'1/9J)
NC ,O~artmc,n.1 .of En~ironmcnt,
H~e;a-ltn, &. Natural Rc..ourcc,
Solid Wilk M•n.atcmcru Divi,ion
SAMPLE ANALYSIS REQUEST S1.&lc Ubor&Lory of Public Hc.1.\1.h
P.O. Box 28047, 306 N. Wilmini:ton St.
Ralci.h, Nonh Cuolina 27611-80•'7
I Sit.eNwnbcr
Name of Site
------------S=plc!DNuwber/Name C, L--00'3 -s;f)
~ I, Af:rt-4 ~a/41 ~ Collc.ct<rlBy ______ ~_ ID tt---'-/ (c+----
I Sil.eLcC3t.ioo ~-~/;,u,Jz,, /UOat.eCollc.ctd '--"' J ✓Superfund A£ency: Hazardous W ast.e --Solid Waste TCLP Compounds
I --
Sample Type Inorganic Compowuis Result.s(mg/1)
Time
EnvironmenL'lJ Concentrate Comments arsc:ruc -I_ · barium -
Ground Water (1) Solid (5) -cadmium --chromium -
1-Surface Water (2) Liquid (6) Jc,id ---mercury
Soil (3) Sludge (7) !:ielcn.ium ---
/other (4)
!:iilver
I -
-Other (8) -
Ll.Jd..u~.:;t---
•1
Organic Chemistry Inorganic Chemistry -.
·-
Parameter Results (mg/I) Parameter ResulLS(mg/1) (mg/kg) Organic Compounds Rc:sult.s(mg/1)
P&T:GC/MS antimony benzene
~ ---
-Acid:BIN Ext. .11rsen.ic carbon tetrachlorid::: --
-2,4-D barium chlonhne --
-2,4,5-TP(Silvex) -beryllium -chlorobcn.unc
~ -chlordane cu<lmium chloroform --
-bcpuicWor -chloride -o-cre!iol
-hexachloro benu:ne chromium m-cresol --
-hex a.ch.I orobut.adi enc cobalt p~resol --
-endrin copper Cfe!)Ol --
-Jindane fluoride 1,4-dicWoroben.z.ene --
I -methoxychlor -iron l ,2-dichloroc:thanc: -
-toxaphene -lead 1, 1-dichJoroc:thylcne -
--rrunganese -2, 4-dichloroelhylcne
I ---mercury -hept,icWor
-nickc:l hex.acWorobenz.c:o~ ' --
-nitrate bexacWorobutsdic:ne --sc:lenium hexachlorocthane ---
I -silver methyl e\hyl ketone -
FOR LAll USE ONLY -:.ulfutes n.itroben:unc -
& -1,2--9~ 6,1) -thallium pent.ucWoropbcnol -
I Date Reaived vanadium pyridine ----zinc tetruch!oroethylene -
Date Extracted pH lrich.10 roc:th y 1 enc ----conductivity -2,4,5-tricWorophenol
I Date Analyzul {p-;J_ 0 -C/ (.p '17 w--TDS 2,4,6-trichlorophenol ---flu.:.:h point -vinyl chloride
Rcport<rl By . c:nUrin ---
I ---lindnne
Date Reported -methoxycWor -
, ',·. ·, .·1 'I 4 --Loxaphcne
Lab Number
.. ;,,:-(),._j..1...;...
I --2,4-D
---2,4,5-TP (Silvcx)
D11S 3191 (Rcvi~ci.! 1"1/?J)
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NC .D~aruncru. of En'Viroruncnl,
Ht;,111.!l, &. Natural R.c.wurcc,
Solid Wui..:. Man,.~cmc.ru. Oi\'i,ion
SAMPLE ANALYSIS REQUEST S1.&1c Laboratory of Public Hc:.alth
P .0. Box 2.11047, 306 N. Wihnin1:ton Sr.
R.alc.i.;h, Nonh Carolin& 2761 l-!047
I SiteNwnber ____________ Su.mplc!D Numbcr/N=e _..::UJc...:....L ___ o_o--1-Lf_-_;5=.;.])=. ___ _
Name of Site ~Ii (0-:,14 o('aAJ,.. Coll.:.::tod By _________ ~_ ID #_-"'-2:~r __
I? a£v.. ~/;~ ~ faQaieCollo.:t«J I Si 1eLic.1tio n ,...,;: ,_._._
I ✓Supcrfund Agency: Hazardous W asie --Solid Waste TCLP Compounds
D ---
Sample Type Inorganic Compow1d.s Results(mg/1)
Environment:1J Concentrate Comments -arsenic
Time
D -barium
-Ground Water (I) Solid (5) -cadmium --chtoro.ium -u-Surface Water (2) Liquid (6) --kud --mercury
Soil (3) Sludge (7) selenium ---::;ilvcr
Votbcr (4l
-g -Other (8) -
--
~ Organic Chemistry Inorganic Chemistry -
P~eter Re:;ullS (mg/I) Parameter Re:;ullS(mg/J)(mg/kg) Organic Compounds Results(mg/1)
I _ P&T:GCIMS --antimony -bcnunc
-Acid:B/N Ext. 11.rscnic carbon tetrachloride --2,4-D barium chlord.anc ---
I -2,4,5-TP(Silvex) --beryllium -chJorobcnu:nc
-chlordane cudm.ium chloroform --
-hcpLUcWor chloride o-cre:.ol ---
-h cxachloro ben.z.ene chromium rn-crc!iOI --
I -hcxachloro but.a.¢ i enc -cobalt p-cresol -
-e:Jd ri.n copper cre!iol --
-!ind.inc fluoride 1,4-dichlorobenuoc --
I -mclhoxychlor --iron 1,2-dichloroclhane -
-loxaphene --lead 1, 1-dichJoroethylcne -
--rrunganese -1, 4•dichlorocthylene
I ---mercury -hcptachlor
-nickel hexachlorobcnzcne ---nitrale bcxachlorobut.atliene ----selenium hcxachlo roetba.ne ---
~-
--silver methyl eµiyl ketone -FOR LAll USE ONLY -sulfates n.itrobenune -
u -o-9re ,e;[) --thallium penLUchlorophenol
Date Rcccivc,J -
I vanadium pyridine --
--zinc letruchloroeth y I ene
Date Extractod ---pH -trichloroethylene
-conductivity -2,4 ,5-tddUorophenol
I Date Analyzed (,, -;JQ-9(p 71 w: -TDS 2,4 ,6-trichlorophenol ---1111..:::;h point vinyl chloride -Reported By > cndri.n ---
I ---lindane
Date Reponcd mcthoxychlor ---·: .: ·., 15 --toxaphcae
Lab Number .. ~ ...... ....:. ..... -
I ---2,4-D
DIIS JJ91 (Rcvi1cJ 11/93) ---2,4,5-TP (Silvcx)
I
I NC _D~1.runc.n1 _of Environment,
Hc.;ah.n, &:. N1.wr1.l R.c..ourcc,
SoJia Wu1.1: Man.ai:i:mcnt Divi,ion
SAMPLE A.~ALYSIS REQUEST SLatr:. Laborat.ory of Public Hulth
P.O. Bax 280-.7, 306 N. WilminblOn St.
R,lci;;h, North Carolin& 2761 l~R047
I Site Number ______________ Sample!D Number/Name __ Ci---'_L __ -_o_o __ S"' __ .=_s=---.j)=----
Namc of Site ~h u./v1'\A--'?f°ifJ _. Colle.:t,:,I By __________ ~_ ID # __ 2-_ __.Jc._ __
t}afv_' ~/;,ud}?,,: faDaieColle.:led I SiieLoc.,.tion '-"' I ✓Superfund Agency: Ha.z.a.rdoll5 W asie Solid Waste TCLP Compounds
I ----
Sample Type Inorganic Compowuls ResuJt.s(mg/1)
EnvironmenL'll Concrntr;,te Commenlc; arsenic -
Time
I_ -barium
Ground Water (I) Solid (5) cadmium ---chroOlium -1-Surface Water (:?) Liquid (6) l""d ---mercury
Soil (3) Sludge (7) selenium ---I Vothcr (4),
!:iilver -
-Other (8) -
-4--(. o,/ ,vi,. ~ . --
I Organic Chemistry Inorganic Chemistry -'
~elu Results (mg/I) Parameter ResuJLS(mg/l)(mg/kg) Organic Compounds ResulLS(mg/1)
I _ P&T:GC/MS -anlimony -bcnunc
-Acid:B/N Ext. arsc:ruc carbon lelrachloridc: ---
-:?,4-D --barium chlor&nc -
I -:?,4 ,5-TP(Sil vex) --beryllium -ch.Jorobcn.u:nc
-chlordn.ne cudm.ium chloroform --
-heplllchJor ch.lori<l.: o-crcsol ---
-hcxachlo ro benzene chromium rn-crc:sol --I -hcxachloro bu Lad icne cobalt p-<:resol --
-cndrin copper crcsol --lindane fluoride: 1,4-dichlorobcnzcnc ---
I -mc:lhoxychlor -iron 1,2-dichlorocthane -
-toxaphcne -lead I, 1-dichlorocthylcnc ---nun g an es c -2, 4-dichloroetb y Jen c
I ---mercury -hcpt.ach.lor
-nickel hcxach.lorobcnzcne --nitrale hexachlorobutadicn~ ----selenium hc:xach.loroelhane ---I silver methyl c;hyl ketone . ---FOR LAil USE ONLY --sulfates nitroben21:ne -
& -1:i--u 13£J -thallium pcn!Jlchl oropbcnol
Date Receivw -vanadium pyridine I Date ·E,tractw
---zinc let rach.l o roeth y l enc ---pH -trichloroethylcnc
-conductiviry -2 ,4,5-trichJorophenol I Date Analyz=d (p-,;JQ-g{.p n11r -TDS :?,4 ,6-trich!orophenol ---flush point -vinyl chloride
Report,:,! By . cn<lrin ---
I --linwmc
Date Report,:,! -
--methoxychlor
~~0~]116 --toxaphene
Lab Number -
I ---2,4-D
DH5 3191 (R.::viw.l l~/9J) ---2,4,5-TP (Silvcx)
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NC. D~anin.cn.t. of Environment,
H~il..'l, &. NaOJral Re.ourci::,
Solid Waw. Manai;cmeru Divi,ion
SAMPLE ANALYSIS REQUEST Si...le Labor&I.Ory of Public:· Hc.alr.h
P.O. Box 280-;7, 306 N. Wilm.in1:ton St.
Raleii;h, Non.h C,rolin.. 2761 !•80,n
I SiteNumbcr ____________ Su.mple!DNumber/Name UJ L -J cJ S--_5-2)
Na.meofSite ~h(,vvr1.,Q.~a/!-J, Collecta!By _________ ~_ID# 3 f
6< d.v._' ~/;_uliA /UbateColle.:tcd I SiteL:,wioo '-"' ; ✓Superfund Agency: Hazardous Waste Solid Waste TCLP Compounds'
I ----
Sample Type lnori;anic Compound, ResullS(mg/1)
Environment'll Concentrate Comments arsenic -
Time
I barium -
Ground Water(]) Solid (5) -cadmium ---chromium -1-Surface Water (2) Liquid (6) -le,id --mercury
Soil (3) Sludge (7) selenium ---I L/2tber,(4)
::.:ilver -
Other (8) --~ --I Organic Chemistry Inorganic Chemistry -
~ter Results (mg/l) Parameter Results (mg/l )(mg/kg) Organic Compound, Rc,;ullS(mg/l)
I _ P&T:GC/MS anlirnony -bc:UU:ne --Acid:B/N Ext. '• carbon tetrachloride -arseruc ---
-2,4-D barium chlordane --
I -2,4,5-TP(Silvcx) -beryllium -cWorobcnu:nc:
-chlordane: cadmium . cWoroform --heptachlor chloride o-crcsol ----
-hcxachloroben.z.cne chrom.ium m·cre!iOl --I -hcxach.loro but.ad i enc cob.tlt p-<:rcsol --
-cndrin copper crc!iol --
-lindane fluoride 1,4-dichlorobrnz.onc ---
I mcthoxychlor iron . 1,2-dicWorocthane ----
-toxaphenc lc.a.d J, 1-dichlorocthylene --
--nunganc:sc: -'2, 4•di chi orocthy l enc
I ---mercury -hcptach.lor
---nicki!l hexachlorobcnz.onc -nitralc hc:xachlorobutllc.lic:nc: ----sc:k:nium hc:xachloroclhanc: ---I --silver -methyl e;hyl ketone
FOR LAil USE ONLY --.sul fu.Lcs n.iLrobcnz..cnc -
t,-;:i.-?6 61,0 --thallium pc:nw.chJorophcnol -I Date _Received --vanadium pyridine -
--zinc lelrachloroc:thylcne -Date Extracted pH trichlorocthylcnc ---I Date AnalywJ (p-J,0--9(p --conductiviry -2,4 ,5-trichlorophcnol
1711£ -TDS 2,4 ,6-trichloroplic:no\ -
--flush point -vinyl chloride
Reporta! By . cndrin ---
I ---lindane
Date Rcporiw mc:thoxychlor ----
. "'11 toxaphcnc '~ -,. . ....., ---
1 Lab Number ..._ Ov I 2,4-D ------2,4,5-TP (Silvex)
OHS 3191 (Rc:viicd l~/9))
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NC Dc:panmcrJ of Environment,
. tluilh, &. Natural R~urcc,
Solid WuLc Mana~cmcru Divi,ion
SAMPLE ANALYSIS REQUEST S1.1tc Laboratory of Public Hc,,lth
P.O. Box 280-17, 306 N. Wilmin.i:ton St .
Ralcii;h, North Carolina 27611-8047
SiteNumbcr ______________ SIIJllplclDNumber/Name (al.. -O O / -5:J)
Name of Site -'-4«i~~2Q.5"a,i.-..a~~L.!;;(,~,J,~~&( __ CollectroBy ____________ lD#_~S:::~---
I SiteLi"-'tion /{~ / tu~ /4J (1
--I ✓Superfund
Date Collected Time
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Agency: --Haurdous Waste --
Sample Type
EnvirorunenL'lt Concentrate
-Ground Water (I) -Solid (5)
-Surfac:: Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
v' Other (4) -Other (8)
~
Organic Chemistry
Parameter Results (mg/I)
~T:GC/MS
_ Ac1d:B/N Ext.
-2,4-D
-2,4,5-TP(Silvex)
chlordane -
-beplJlchJor
hcx.achloroben.z.ene -hcxachlorobutadicne -cndrin -lindane --mcthoxychJor
-1oxaphene
--
--
FOR LAB USE ONLY
Date Recciv.:,l b -/ ,,2--9(,, 61{)
Date Extracted G,-}'-f_q~ -SA
Date Analyzed
Reported By
Date Repor1ed
ub Number .:.:,JJ11s
OHS 3191 (R,vhcJ l~/93)
Solid Waste TCLP Compounds
Inorganic Compow1ds Rc,;~ts(mg/1)
Comments arsenic -barium -cadmium -chromium -leod --mercury
selcn.ium -~ilvcr ---
-Inorganic Chemistry -
Parameter Results(mg/l)(mg/kg) Organic CompoWlds Rc,;ults(mg/1)
antimony bcD.2Cnc: --
11.rscnic carbon tetrachloride --
barium chlordane --
-beryllium -chJorobcnzenc
cadmium chloroform --chloride o-crc;;;ol --chromium m-crc;;;ol --cobalt p-cresol --copper cre~ol --fluoride 1,4-dichJorobenune --iron 1,2-dichloroetha.Ile ---lead J, 1-dichJorocthykne --m.J.n g an es e -2, 4-di chlorocthy knc
-mercury -heptachJor
nickel bcxachlorobenune --nitrale bexachlorobutadieoe --selc::njum hcxachloroelhane --
-silver methyl ethyl ketone -sulfutes nitroben.u:ne ---thallium pent.achlorophcnol -vanadium pyridine --
-zinc tetrachJoroeth y !enc --pH -trichJoroethylcoe
-conductiviry -2 ,4,5-trich.lorophenol
-TDS 2,4,6-trichlorophenol --flu:;h point -vinyl chloride
cmlrin --lindane --
--methoxychlor
--toxaphcnc
--2,4-D
--2,4,5-TP (Silvex)
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NC Dqiartmcnl or Environment,
, Hullh, &. Naruul R.~urce,
Solid Wur.c Mana.cmcnl Divi,ion
SAMPLE ANALYSIS REQUEST S1.at~ Laboratory or Public He1.lth
P.O. Box 28047, 306 N. Wilmini:t.on St.
RaleiJ:h, Nonh Cuolina 2761 l-R047
SiteNumbcr ______________ SumpklDNumbcr/NIUilc G L -(2 () '2. -5 D
Name of Site~ c:1"J 1 . C<illcctcdBy ___________ ID # _ __,_J_,_/ __ _
SiteLoc..tiontf?a¥,lw~ µ (_ DateCollccLM 01 -//-7 e:,
/ TCLP Compounds Agency: HJ12Mdous Waste Solid Waste __ Supcrfund ----
Time
Sample Type Inorganic Compowids Rcsuh.s(mg/1)
Environment:\} Concent[:i!te Comments -a.rs.ewe
·, barium -
Ground Water (I) Solid (5) -cadmium --chromium -
Surface Water (2) Liquid (6) -l""d ---mercury
-Soil (3) Sludge (7) -stlcn..ium -
_:('Other (4)
-~ilvcr
-Other (8) -
A I ,.,/1/l .. ,_ ~ -j--. -Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compowids Rcsult.s(mg/1)
~T:GC/MS antimony -bcnune -_ Ac1d:B/N Ext. urscnic -carbon tetrachloride -
-2,4-D barium -chlordane -
-2,4,5-TP(Silvex) -beryllium -chlorobenzcnc
chlordane cuc.lmium -chloroform ---hepuichlor -chloric.lc -o-cresol
-hcxachlorobenz.cne chromium -m•cre!:iol --hcxach.lorobutadicne cobalt p-cresol --
-cndrin copper ere.sol --
-!ind.:ine fluoride 1,4-dichlorobcnzcoc --
-methoxychlor iron -l ,2-dich.lorocthane --toxaphcne lead I, 1-dichloroethy!ene ----nu.nganese -2,4-dichloroethylene
--mercury -heptachlor
nickel hexachlorobenzene ---nitrate hexachlorobutndicoo ---selenium hc:xachloroclhanc --silver -methyl ethyl ketone -FOR LAil USE ONLY .:.ulfutes nitrobcn2.ene --
le -1,,1-91, &12 thallium pcnlllchlorophenol --Date Receivc<l vanadium pyridine --
-zinc tetrachlorocthylcne
Cc-14-SG SA -Date Extractc<l pH trichloroc:th y lcnc --
-conductiviry -2,4,5-tric!ilorophenol
Date Analyzed TDS -2,416-trichloropl1cnol --flush point -vinyl chloride
Reportc<l By cndrin --lindane --
Date Reportc<l --methoxychJor
~oJ119 -Loxaphene
Lab Number ---2,4-D
--2,4,5-TP (Silvcx)
DIIS 3191 (Rc..-i~cd l~/9J)
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N.c Ccpanrmnl of Environment,
Hcahh, &. N.tural R~ourcc,
Solid \lr'utc Mana1:cmcn1 Divi,ion
SAMPLE ANALYSIS REQUEST S1.atc Laboratory of Public Hulth
P.O. Box 28047, 306 N. WilminJ:i.on St.
RalciJ:h, Nonh Carolin.a; 2761 J-8047
SiLeNumher ______________ S=ple!D Number/N,une __ c;;_c..~_----'o=-0=-_3,__-__.s~-"-D""-; ---
Nameo(SiLe hzu/.rvk, <'· ~ CollectodBy ___________ lD# __ /'--7.,_ __
SiLel.oc:tion.f'a_/ + / t<J~ µ [P__ I -
Agency: Hazardous WasLe Solid WasLe l---'(uperfund TCLP Compounds ----
Date Collecled Time
Sample Type Ino~anic Compawids Results(mg/1)
Environment.'11 Concentrate Comments -arseruc
barium -Ground Water (J) Solid (5) -cadmium --chromium --Surface Water (2) -Liquid (6) -J.,,,d
-mercury
-Soil (3) Sludge (7) selenium --
v'other ( 4) -silver
-Other (8) -
/'I -_,/I•-~ . -' -Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mgll)(mglkg) Organic Compowids ResulLS(mg/1)
~&T:GCIMS antimony bcnu:m: --_ Ac,d:B/N Ext. arsc:ruc cn.rbon tetrachloride ---2,4-D -barium chlordane --2,4,5-TP(Silvex) -beryllium -chlorobcnzenc
chlordane cadmium chloroform ---
-heptachJor -chloride o-crc::;ol -hexachloroben.z.ene chromium m-crc:wl ----hcxachlorobuL.iidicnc cobalt p-<:resol ---cndrin copper cresol --lindane fluoride r J ,4-dichlorobenunc ----methoxychlor -iron 1,2-dichloroethanc ---toxaphenc -lead 1, 1-dichJorocthylcnc ---manganese -2, 4-d ichl oroeth y I ene
--mercury -heptachlor
-nickel bex.achlorobcnzene ----nitrate hexachlorobutadiene -selenium hc:xachloroethane ---silver methyl ethyl kelOne -FOR LAB USE ONLY ~ulfotes Wtroben2t:ne --
/; -J;l -J?, ,,g "° -thallium pc:nl.Jlchlorophenol -Date Received vanadium pyridine --
1,~1L/-1fc -z.inc letrachloroethylene 5A -Date Extracted pH trichloroethylcnc ---conductiviry -2,4,5-trichlorophenol
Date Analyzed -TDS 2,4 ,6·trichlorophenol --Hu.!ih point -vinyl chloride
Reportod By -cndrin -lindruie --Date Reponod --methoxychlor
~SJ1ZO --toxaphenc
Lab Number 2,4-D ----2,4,5-TP (Silvex)
DIIS 3191 {Rr.vi~c:d 11/93)
1--
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NC Dcpanmcru o( Environment,
Hc.alLh, & Nawral Rc.0ur1;c,
Solid Wutc Man.ai;cmcru Divi,ion
SAMPLE ANALYSIS REQUEST Sc..1.c. l..aborai.ory of Public Hc.a.hh
P.O. Box 28047, 306 N. Wilmington St.
Ralcii,:h, Nonh Carolin. 27611-80◄7
Sii,, Number Sample ID Number/Name __ Uj=-.t._,l-=-_-_,0=..:::0::.._C/L__-__..S!..L.7),!_ ___ _
NamcofSii,, ~ ~ C,,JkctedBy ____________ ID # _ __::::.,,,2_..;.· _3""'---
1 Sitr.Loc;;tio£~ !tu~ /U ~Date.Collected l
~crfund
Time
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Agency: Hazardous Wa.str. ----
Sample Type
Environment..'11 Concentrate
-Ground Watr.r (I) -Solid (5)
-Surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
/Other (4) -Other (8)
/I • .... II._ --
Organic Chemistry
Parameter Results (mg/I)
~T:GC/MS
_ Ac,d:B/N Ext.
-2,4-D
-2,4,5-TP(Silvcx)
chlordane -
-beptachlor
hcxnch!oroben.z.ene -hcxAch!oro bu Lad i enc -cndrin -lindanc --methoxychlor
-loxaphcnc
--
--
FOR LAB USE ONLY
Date Rcccive,l u-J.)-CJt,,/.3£J
Date Extracted fr-11-9tv SA
Date Analyzed
Rcporte,l By
Date Rcponed
Lab Number
{ _ .. , ... ! ...--;.
._:; G , ... ):.._ ,_;, 1
DUS 3191 (R,vimi l'.:':/9J)
Solid Wa.stc. TCLP Compounds
Inorganic Compow>ds Results(mg/1)
Comments arsewc -barium -cadmium -chromium -lCJtd --mercury
selcn..ium -~ilvcr ----Inorgaruc Chemistry -.
Parameter Results(mg/l)(mg/kg) Organic Compow1ds Result.,;(mg/1)
antimony benzene --
11rscn.ic carbon tetrachloride --ba.rium chlordane ---beryllium -chlorobcnzenc
cadmium chloroform --chloride O•CfC!iOI --chromium m-crcsol --co bu.It p-cresol --copper crc:sol --fluoride 1,4-dichlorobenuoe --
-iron -1,2-dichlorocthanc
-le.1<l J, 1-dichloroethylenc --nunganese -2,4-dichloroethylene
-mc:rcury -beptachlor
nickel hexachlorobenzcoc --nitrate: hexachlorobuLadic:ne --selenium hexachloroethanc ---silver methyl ethyl ketone -:.ulfotes nilrobc:rucnc --
-thallium pentachlorophenol -vanadium pyridine ---z.inc letrachloroethy !enc -
-pH -lrichloroethylcnc
-conductivity -2,4 ,5-lrichlorophcool
-TDS 2,4,6-trichlorophenol -
-Ha.sh point -vinyl chloride
cndrin --lindane ----methoxychlor
--toxapheoe
--2,4-D
--2,4,5-TP (Silvex)
.
I NC Dcpartmc.n!. of Environmcnl,
Jiull.h, & Nat11ral Rc:.wurcc,
Solid WHLc Muu~cmcnl Divi,ion
SAMPLE ANALYSIS REQUEST SL.a~ Labora10ry of Public Hc.alth
P.O. Bax 28047, 306 N. Wilmin.:wn St.
R...lcii;h, Nonh Carolina 27611·8047
I SitcNumbcr _____________ Su.mplelDNumber/Nu.me __ VJ_G-__ -_0_0_~ __ -_ __s_J) ____ _
Name of Site~~ ~ CollectodBy _____________ lD# __ d __ 7.__· __
Time
I Agcocy: Hlll.lltdous Waste Solid Wast.: ~erfund TCLP Compounds ----
Sample Type lnori:aiuc Compowuls Results(mg/1)
Environment..'ll Cnncentr;ite Comments -arsenic
I -barium
Ground Water (I) Solid (5) cadmium ---chromium -1-Surface Water ('.2) Liquid (6) -kad --mercury
-Soil (3) Sludge (7) selenium --I ~lher (4)
-~ilvcr
-Other (8) -
,4-J!_ cli.,vv<-&...:r --I Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organ.ic Compounds Rcsults(mg/1)
I ~T:GC/MS antimony bcn:z.enc --_ Ac,d:B/N Ext. uscn.ic carbon telrachloride --
-2,4-D -barium -chlordane
I -'.2,4,5-TP(Silvex) -beryllium -chlorobcn.z.cnc
-chlordane cudmium chloroform --beplJlcWor chJoridc o-crcsol ----hexacWorobeI1ZCne chromium m-crcsol --I -hcx.a.chJorobu Lad icne cob.Jt p-<:resol --
-cndrin copper crcsol --
-lindane fluoride 1,4-dichloroben.z.ene --
I -methoxychJor -iron l ,2-dichlorodhane -
-toxaphc:ne -le.1d I, l ·dicWorocthylene ---rrunganese -2, 4-dichl oroctby I c:ne
I -mercury hcptachlor ----nickel hcxach.Jorobenzene -nitrate bexachlorobutadiene ----selc:nium hc:xachloroethanc --I -silver methyl ethyl ketone --FOR LAB USE ONLY -!.Ulfutes nitrobenune -
u -1 ;i -rt/; ,eef) -thallium pcntachlorophenol -
I Dale Received vanadium pyridine --
-zinc tetnichlorocthylene
Date Extracted (,-llf-9{,, SA -
-pH -trichloroc:thylene
-conductivity 2,4 ,5-tricWorophenol
I -Date Analyzed -TDS -2,4 ,6-trichloroplicnol
-Hash point -vinyl chloride
Reported Dy --cndrin
I -Jindnne
Date Reported ---methoxychlor
1..·•· ·-:1~') . ..., -toxaphcnc
Lab Number ...JG J ,;.,,_,, -
I --'.2,4-D
DUS 3191 {Revised 11/93) --2,4,5-TP (Silvex)
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NC D<J)•nmcru of Environm,ru, SMfPLE ANALYSIS REQUEST SLo1< l..obomory of Public Health
, Hullh, &. Nawral Ruourcc, P.O. Box 28047, 306 N. Wilminiton St.
Solid Wutc Man.a~cmcn1 Divi,ion R..alcii,:h, Nan.h Carolin.a 27611-!047
Site Number ______________ Sumple!D Number/Name __ (/) __ {. __ /_D--=S=---~•-5"-:.])==--------
Name of Sile~ ~x ~ Coll«:tedBy ___________ lD#_· _3::;.._=_s--'--_
Sittl.outio~/u)~ ,t(_/f' DateCol!.:,:lc<l
Agency: Hazardous Wasu: Solid Waste ~rfuod TCLP Compounds ----
Time
Sample Type lnor,:anic Compow,ds Results(mg/1)
Environment'\! Concentrate Comments arsewc -' barium -Ground Water (J) Solid (5) -cadmium --chromium -Surface Water (2) Liquid (6) -load ---mercury
Soil (3) Sludge (7) seleJUum ---
~!her (4)
:;ilver -Other (8) -
,cu__~ ---Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compow,ds Rcsults(mg/1)
P&T:GC/MS antimony -bc:nzenc
~cid:B/N ExL -arsc:ruc cn..rboo tetrachloride: ---2,4-D barium chlordane --
-2,4,5-TP(Silvex) beryllium -chlorobcnzene -chlorWlne cudm.ium chloroform ----hepwchlor chloric.lc -o-crc:.:ml -hcxachlorobenz.ene chtoITUum m-crc:;ol ----hcxachlorobuLadiene cobalt p-cresol ---cndrin copper crc:sol --
-!ind.l!le fluoride 1,4-dichlorobenune ---mc:thoxychlor -iron -l ,2-dichlorocthanc -·
-toxaphc:ne -lead -I, 1-dich!oroelhylene
--m:1I1ganese -2,4-dichlorocthylene
--mercury -beptachlor
nickel hexachlorobenune ---nitratc: bexachlorobuta<liene ·---selenium hc:.xachloroc:tbanc ---silver methyl ethy I ketone -FOR LAil USE ONLY sulfates nitrobc:ru.enc: --
& -/;)-CJ(,,~£)
thallium pcnlJlch!orophenol --Date Received vanadium pyridine ---z.inc tetrnchlorOethylc:nc (-,-/4-90 SA--Date Extracted pH trichloroc:thy lc:ne ---conductivity -2,4,5-trichlorophenol
Date Analyzed -TDS -2,4,6-trichloroplu:nol
-lla.h point -vinyl chloride:
Reported Ily --cndrin
lindllne --Date Reponcd --methoxychlor ,,,,1~3 toxaphcne .. ,j G, ...J ,:.. --Lab Number 2,4-D ----2,4,5-TP (Silvex)
D11S 319! (Re.viml 11/93)
t,t.G1Uls, l V h!l:::::.G..LUN = ..L V SUPERFUND PROJ . .LEADER: I. WILLIANS CONPAHY: SUPERFUHD
SPILL IO: I. ACIIVHY: 11._·
PROJECT -IO: __________ _
SITE HANE: Sresha1s Lake
I
CITY, STATE: Raleigh/Wake, NC
I
.ATE SHIPPED: 06/13/96 CARRIER: Hand Delivered
AIRBILL: ____ _ I SHIPPED TO: NC Public Health Laboratory
Bath Building
I Wil1in9ton Street
Raleigh, NC
I , I , 1, 1
n 61, 61
10, 10, 10, 11, 11
a er
7, 7, 7, 8, 8
1 e We 11
L-43, 43, 0, 44, 44
en
L-16, 16, 16, 17, 17 1) ace Water SL-13, 13, 13, 14, 14
( 1 I e Well -charl1e Brown's 46, 46, 46, 47, 47
CHArN-oF-CUS,ODY RECORb
er
Ground Water 06-11/0915 I. WILLIAHS
e uen
ur ace
Ground Water 06-11/looo I. WllllAHS
e 11en
surface Water 06-11/1055 R. ZIHH
Ground Water 06-1171140 I. WILLIARS
e uen
I ( 5 SL -
,.__ __ .,_,VO""A(_,,_3ul....,,E.o.,XT__,0""R"'-(-'..J1 )'-----------------------------~---
lhite -LAB Copy for Return to Samplers Yellow -LAB Copy Pink -Saipler's Copy Sold -Extra Copy
1 ,L.U.l.LIH -1" II .._ .._ ...__. ....I... ._,I. PROJ. LEADER: I. WILLIAHS
I. ACTlVJTr: li._.
PROJECT .JO:
COHPANY: SUPERFUHD
SPILL ID: CHAIN-0~-CUSTODY R~CORD
~ . SITE HAHE: -Gr-es~h-am_s_L-ak~e-------=="'--'=-------
I
CITY, STATE: Raleigh/Wake, NC
I
IAIE SHIPPED: 06/13/96 CARRIER: Hand Delivered
AIRBILL: ____ _ I SHIPPED TO: NC Public Health Laboratory
Bath Building
I Wil1ington Street
Raleigh, HC
STATION DESCRIPTION
GL-005-SD edi1ent 5) GL-28, 28, 28, 29, 29
er 25, 25, 25, 26, 26 VOA 3 EX
34, 34, 34, 35, 35
a er 31, 31, 31, 32, 32
KA TRIX DATE/TIHE SAHPLER
5edi1ent 06-11/1150 H. ZIHH
Ground !later 06-ll/1605 I. IIILLIAHS
•~-----------
I
• hite -LAB Copy for Return to Sa1plers Yellow -LAB Copy Pink -Saipler's Copy Gold· Extra Copy
I
I
STATE UBORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
I PURGEABU: COMPOUNDS LAB NO 'llJ, 31 l;t 9£D31l3 C,u,311't qu,3/)~ 91P3// lo
FIELD NO GL-VOl-51) Gi..·oOJ..-5D G-1,-003.51) G-t-·oo<t-5D I &l·Db5 -sD
I COMPOUND TYPE ( 1./ ) ( t ) ( 't ) ( 4-) ( 1-f )
~~i,)!-~pb')pprn 1¥,b'.)ppm tppb ppm tppl,)pp,,-; (ppt,)ppm
~RO?aTRANE. JO LL. I I 1 i { I
CHLORIDE 10
I BROMOM.E'THA?R; ;J..0
ICHLOROETRANE iO
TRICBLOROFLUOROMrl'RANE JO '
[ACETONE ,;;i_ 0 '7 -:r, C,
I l.1-DICM.ORO!:TBE?t'E 5 LL
Jl0001""TlW!l: J;
I 0 5 :r.c. ME'THYIZNE Clll.ORIDE
I CARBON DISIJU'IDE +r-o.ce..
TRA."fS-l.2·DICfil.OROETHErn: J, I 1
t ACRYLO?<ITRllZ ~
1, l·DlCHLOROE"TB..i\1ra 5
2-BUT AN ONE .;:1.D
I CLS-1,2-DICHLOROJITHEN!: 5
CHLOROF'ORM I
I 11,1,1-TRlCHl.OROJITHANE I
CARBON TZ'TRA.CHLORIDE
lBENZ,:NE
1,l·DICID.OROIITHANE
l TRICHLOROETH.BfE
I I l,2-DICHLOROPROPANE
I f ROMOO!CHLOROHETHANE ,11 ' I ' I ,v \I 'I
-.. -. ·-C Po.,..,,':)I....E: 1-MB c...:..N1ANi1NA1 iO~ oR BALK.6-R.c;...l'JD .
J -EstUll4ted value
L -Actual value is known to be greater than value given. I IC -Actual value is known to be less than value given.
U -Material was analyzed for but not detected. The number
:&A -Not a.naly:c:ed.
is the Minim.um Detection Limit.
1/ -Tentative identification.
I]/· C.C/'A,Pou.l'io RE!..lf\6L'f OST,:C,(-;\;':1..£ C,l,)L'/ IN H 16"H
✓-SAMPU! HIG·Hl...'I 011-_L,TEW. ~1DL'"".:• De Nol APPL"/.
DEBNR 3065-0 (10/93)
I
C!)
qG au 7
GL·J05-:5D
( 4 )
rppi,} A=Jm
u.....-
.
·, I
PURGCOM.ORG
ST.ATE LABORATORY OF PUBLIC HEALTH I
I
PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
I PrrnGEABLE COlllPOONDS LAB NO Cfu o 11.). C/(.p3/J3 9£t~ll4 9C.03l15 q1.i;3JJ(i;
FIELD NO bl· co 1-s1> ::i-L-OQ;I -9.) Gl·DD3-5D 6-L·OO't-SD GI.· COS· SI)
I I
COMPOUND TYPE ( i./ ) <if ) ( 4-) ( 4 ) ( 4-)
n~rt PP~ ppm rPpb f Pfl1 vpp/j PFfY'l (pp§ FPrn 'fPb, ppm
1 DIBROMOMrrHA.NE 5 l).. LL-iL.· L,L. I J
I ,o 4-METHTL-2•n~A."f0NE
CIS-l,3•DICHLOROPROPENE 5
TOLtn;NE
TRA.'fS--1,3-DICHLOROPROPENE
l, 1,2,2· TrrRACHLOROUHA..?U;
1.1,:2-TRlcm.oROETBA?fE ' /
2-~0NE JO
I
TrrRACHLOROETH!:l'fE 5
I DIBROMOCHLOROlaTHAN'E
!:THn.!::'fl: DIBROMIDE
II
Cffi.OROBE~
1.1.l.l·nrRACHLORO!:'THANE
rrHYL BOZZNE
==
STTR!:Nz: ' I
tBROMOP'ORM ;o .
TRAI'f5-,l,4--DICHLOR0•2--BUTZN'E io
I 1,2,3-TRicm.oROPROPANE .5
1.4-DICHLOROBENZJ;N?: I
I 1.2-DICHLOROBENZENE -v I
1,2-DIBROM0-3--CHLOROPROPANE ~CJ I
~ VINYL ACtfATE ~o ' / ' I ., I -,j/ ' /
•
. -. C -j>~.:»oLe LAe. Cc:,ril=\hl.1,Jj~TlUN OP, BACt;.C--t<C.l..'JQ.
I J -Estimated value
~ -Actual value ia known to be leas than value given.
L -Actual value is known to be greater than value given.
0 -Material was a.naly:z:ed for but not detected. The number i■ the Minimum Detection Lim.it.
NA -Not a.naly:z:ed.
I 1/ -Tentative identification.
I.1 -coMPo1.l!JD R:a1..1f"cLY oisTEcTf\BU= c,\JLY iN HIG·H
✓ .. :S,1t'1Pi..t:: Hl{i·HLY Di LUTED. t~i)L•~ no J,,y_,7"" (".PPL-/.
DEHNR 3068-0 (10/93)
I
qG?J/17
(;;-1, • I 05-51)
( if-)
/ ppb ppm
I I
.. /
PURGCOM.ORG
STATE LABORATORY OF PUBLIC HEALTH I
I P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC OlEHICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO C/IP" I Y <7IA-< I I '-1' <-I ,A :i. 1 ,:;,o t,1/.,, 11.:i..1
-EXTRACT ABLES FIELD # r-L-00/-<;n r..1-00 "L-m ':JJL -oo3--5]) r,;; -00</-SJ)
COMPOUND TYPE ( LL l ( lt-) ( IJ-) ( 'f )
UNITS =irua/kn =nev .. n/kq --v"' .. n/k□ ,-,-Y un/kQ
-itrosodimethvlamine IOI .,.,,0 I -I.,<..-A IA. -
-(2-ehloroethvllether
2-<:hlornnhenol
lnol -dichlorobenzene
·,
-dichlorobenzene
l 2-dichlorobenzene 11 (2-eh loroi <nnrnnvJ) ether
! ach 1 oroethane
N-nitroso-di-n-nrnnvlamine
lobenzene
horone
trnnhenol
4-dimethvloheno 1
· 1(2-eh loroethoxv)methane
. -dichloroohenol
1.2.4-trichlorobenzene
:lhthalene
achlorobutadiene
4-ehloro-m--cresol
:lxachlorocvclnn<>ntadiene
1 6-trichloroohenol
<-<:hloronaohthalene
acenaohthvlene
fthvl ohthalate
-dinitrotoluene
acen°0 hthene '
14-dinitrnnhenol SOI roso
4-dinitrotoluene 10 "l,/Q
4-nitrnnhenol ,01i1 • .:;o
1 uorene . /0/330
chlornnhenvlohenvlether
ethvl ohthalate J,
4 6-dinitro-o-cresol SOI 11,,,0
henvlamine /0/330
obenzene
4-bramohenvlohenvlether
lxach 1 orobenzene 'j
ntachlornnhenol s-0111.:fo
ohenanthrene //1/ "'13D
thracene
butvl ohthalate I I I I
uoranthene ,, ' ' ' 'I /
rn"D L
I-Estin"'ted value. H,..o/SO/J ...
-Actual value is known to be less than value given.
L_ -Actual value is known to be greater than value given.
c.1t,, :< I 1 _i
'n(..-Oo5-.s])
( 1./ )
~ .. n/ka
!A.-
/
'
t-Material was analyzed for but not detected. The nUTber
-Not analyzed.
is the Hini1TU11 Detection !:_imit. m'JJL --Tentative identification. ff -On NROC List of Priority Pollutants.
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I~//~,~ '?
u,L-n,-.:,J)
(U )
~ua/kq'\
L,<__
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BASE/NEUTRAL AND ACID
EXTRACT ABLES
aJIIPOOND
nvrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3.3-dichlorobenzidine
bis(2...,,thvlhexvllohthalate
di-n--octvl ohthalate
benzo(b}fluoranthene
benzo(klfluoranthene
benzo(a'nvrene
indeno( 1.2 3-cd\nvrene
dibenzo(a.h)anthracene
benzo(a h. il=rvlene
aniline
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2-<rethvl n.>nhtha 1 ene
2-<rethvlohenol
4-<rethvlohenol
2-nitroani line
3-nltroani line
4--nitroaniline
2 4.5-trichloroohenol
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON. ST., RALEIGH, N.C. 21611
ORGANIC OlEMICAL ANALYSIS
LAB NO qt,_ -or; J y il//"' '?II '-:I ~{/ :?/,,.1._0 Cj(,_, ~ I J_ /
FIELD# 'nl·I)() 1-s]) {;,l-r:J02·57' 'hl-003-:51) l'"nl-00'/--,7
TYPE ( "1 ) ( .,. } ( 'f ) ( 'I" )
UNITS ~ ,n/ka ------"'.":,./k:a ........,.-;,nfka ✓ /ka
/0/~ 30 ,~ l 1....---I• -[.,t_...-
_<;11 I •l,50
JOI '30
. ,
'/t..'i() SOI
l()/330
Jo/_g_::;o
soht.<o
I I / /
\ ., ' ' '
.'f"O /11,,~o /,\_.-1,,, -IA -' -
' ,,.
101=0
~,.
s-ot,1,,50
I / I F
'IJ,. ' ' '\
fl'l:DL.
J -Estirruted value. H.a.0/ Se;//..
K -Actual value is known to be less than value given.
C-/r,.,'J,,-,
tr✓ -oor-.51)
( 'f )
.-u.i: <. ,u /k:a
IA......
.
/
' "
. I A
/
'
l -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nuroer is the Minirrun Detection Limit. ~
NA -Not analyzed.
1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
'-/t,3n ~
r'n(:-/0:,-~ 7
( ye-)
~, ""'/ko
IA--
,r
(A__
/
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-.... N{: Dc;otruN:n! n( Environmcnl,
Hc.allh, &. NaDJral Rc:40urcc,
Solid Wul.c Mana~cmcnt Divi,ion
SAMPLE ANALYSIS REQUEST SLalc Labomory of Public He.a.Ith
P.O. Box 28047, 306 N. Wilminbwn St.
R.alc:i,;h, Nonh C.rolina 2'7611-R047
Siu:Numbcr ______________ Su.mple!D Number/Nu.me _,Ui=.;:;L-:,__-..:,0,:._::0:.....,_/_:=S:.....:cw _______ _
Name of Sil<: ~ f0:?1--4-o(°a/4-I _. Collcct.:<lBy
.: c: ("' :::-·. -I I ;,, __ .. _ , __ ID#_·-'-----
Si1<:l.Dcati ,,{) ~/;,u ~ /U6al<: Collected OD -:, ! •
Agency: Hazardous Waste Solid Wa.su: ✓Superfund SUPe:FM'-J;~P.~\/!lds ----
II I hi 2i}m1fl96
Sample Type Inorganic Compow1d,; Resull.s(mg/1)
EnvirorunenL'll Concen!!J!!e Comments -arsewc
. II o /2,;..µJ1,r -barium
Ground Water (I) Solid (5) -cadmium -M' / Surface Water (2) a! A. 1-;y ~~,t_b -chromium
Liquid (6) -!Clld --•.
I, '-'-('rl--mercury
./i'J,_,__IC·._t.j -
Soil (3) Sludge (7) -selenium --
-'.2 ,,;;..-i ;.,-otc;;;-~ ~i}vcr -
Other (4) Other (8) ---I '-----'' --
Organic Chemistry Inorganic Chemistry -
~eler Results (mg/I) Parameter ResullS(mg/!)(mg/kg) Orgaruc Compound,; Rcsults(mg/1)
P&T:GC/MS antimony -benzene --Acid:B/N Ext. 11.rscn..ic -carbon tetrachloride --2,4-D -barium -chlordane
-2,4,5-TP(Silvex) -beryllium -chlorobcnzcnl!
-chlordane cudmium -ch.lorofann --hepUichlor -chloride -o-crcsol
hcxnchloroben.z.ene chromium -m-crc!iOl ---hcxach.lorobutadicnc co bu.It p-cresol --
-cndrin copper crcsol --
lindane fluoride 1,4-dichlorobcnune ---
-methoxychlor -iron -l ,2-dichloroc:thanc
-toxaphcnc lead -J, 1-dicl~oroethylene -
--nunganese -'.!,4-dichlorocthylcnc
--mercury -heplJlchJor
-nickd hcxach..lorobcn.zene --nitrate hcxachlorobutadiene ---
sclcnium hcxa.chloroctbanc --silver --methyl ethyl ketone
FOR LAB USE ONLY -sulfates -nitrobcnzenc
I,-/)--'7c,~ 4 ,<f}
thallium pcnlfichlorophcnol --Date Received vanadium pyridine ---2.inc letruch.lorocthylcnc -Date Extracted pH trich..lorocthy l enc --
&-ti-f-9& -conductivity -2,4 ,5-trichlorophenol
Date Analyz.ed -nur TDS 2,4 ,6-trich!orophenol --
di11 t? /l II~, / -fla!ih point -vinyl chloride
Report By c:ndrin , ..,~ -
Date Repor(I_ J; ~2--0 -9(::, -lindane ---methoxychlor
loxaphcne
,; -:-: !) 9 ~ --
Lab Number ~J \.),., ! •i a 2,4-D --
-2,4,5-TP (Silvex) -OHS jJ9J (Revised 11/93)
'N~pqi~rtmr;n! o,f Environment,
Hc.ahn, & N.awul R.cwurcc,
Solid Wu~ M.an.a~cmcru Divi,ion
SAJ'v!PLE ANALYSIS REQUEST SL.ale Ltbout.ory of Public He.1.llh
P.O. Box 2&0-11, 306 N. Wilmini:U>n St.
R.ah::ii;h, North C.arolin.a 2761 l •&047
I Si1eNumbcr _____________ Su.mplelD Number/Nu.me __ 6,_(._,_-_0_0_2_-_-~S_w _____ _
Name of Sit<: ~-/2 wn1,,4 ,::;(a/:-J,... Collo::tc:,l By __________ ~_ ID # __ 7_,__ __ _
I Sit<:Loc,.tion /? ,d!,v._' -~h_ua._h faDat<:Co!lo::t<:d 1'1 -11-9 0 Time
'---" I ✓Superfund
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Agency: --H=dous W JI.Ste --
Sample Type
Environment."'1.1 Concentrpte
-Ground Water (I) -Solid (5)
✓surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
Pt/o'eler Results (mg/I)
_ P&T:GC/MS
Acid:B/N Ext. --2,4-D
-2,4,5-TP(Silvex)
chlordJUlc --bepWlchlor
hexachloro ben.z.ene -hcxachloro bu tad i enc -cndrin -linWlile --methoxychlor
-toxaphc:ne
----
.
FOR LAB USE ONLY
Date Received &-f.).-7(., BtO
Date Extracted
Date Analyz.:d (p -I if-9 ~ -nu..r-
Reportw By
Date Reported
Lab Number
·, ... -' ·", ,.... ·~ .....,; ·c, .J 1J<Sll
DH.S j19] (Rt.Yi~cd l~/93)
Solid Wll.Sle TCLP Compounds
Inorganic Compounds Results(mg/1)
Comments arsenic -· .. ba.rium -cadmium -chromium -lead --mercury
selenium -::.:ilver ----
Inorganic Chemistry -
Par:imeler Results(mg/l)(mg/kg) Organic Compounds Rcsull!i(mg/1)
--anlirnony bcnune -
11.rsenic c:i..rbon tetrachloride ---
barium chlordfil1e ---
-beryllium -chlorobcnzenc
cadmium chloroform --
ch.lori<le o·cre:.ol ---
chromium rn-cn::.ol --
cobult p-cresol --
copper crcsol --
fluoride I ,4-dichlorobe01.ene --
--iron 1,2-dichl~roelhane -
--lead l, 1-dichJoroethylcne -
-nungancse -2, 4-d ichl a roe thy Jene
--mercury -hept..chlor
nickel bcx.achlorobcnz.enc ---nitrale bcxachlorobutaJicnt ---
selenium hcxachloroetbanc ---
--silver methyl e[hyl ketone -sulfates niLrobcnunc: ---. -thallium pcnLUchlorophcnol -vanadium pyridine ---
--z.inc tetrachlorocthylcne ---pH -trichlorocthylene
--conductivity -2,4 ,5-trichlorophenol
-TDS 2,4 ,6-trichlorophenol ---11,csh point -vinyl chloride . cndri.n ---
---lindllne
---mcthoxychlor
---toxaphene
---2,4-D
---2,4,5-TP (Silvex)
... -.... , .... -.....
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--NC· Dcp&rtmcru of Environment,
Huhn, & Na~nl Rc.50urc:c,
Solid Wu1.c Man.a.(;mcru. Divi,ion
SAMPLE ANALYSIS REQUEST S1.&1.e Labont.ory of Public He&lth
P.O. Bax 28047, 306 N. WilmintLOn St.
R•lcii,:h, North Carolina 2761 l-SO•t7
SiLCNumbcr ______________ Su.mplc!DNumbcr/N=c U) l, -C)Q 3'-5G.J
NameofSite ~?0::n-4~aA/--CollcctcdBy _________ ~_ID# /.3
Si le I.Dc.ttion ,,{) a1v..· ~/; ,J 61. /?,J, /UC..Uate Collected '-"' 7 ✓Supcrfund Asency: Hauu-dous W ..,LC --Solid Wa.sLC TCLP Compounds --
Time
Sample Type lno~anic Compowul.s Results(mg/1)
Environment'\! Concentrate Comments -arsen.ic
barium -
Ground Water (I) Solid (5) -cadrcium
JSurfacc Water (2)
-chromiuin -
Liquid (6) -lead --mercury
Soil (3) Sludge (7) -selenium --:i:ilvcr -
-Other (4) Other (8) ----Organic Chemistry Inorganic Chemistry --·
~eler Results (mg/!) Parameter Resul15(mg/l)(mg/kg) Organic CompoW1ds R6ullS(mgll)
_ P&T:GC/MS -antimony -bc:nunc
Acid:B/N Ext. .u.rscruc -CUibon tetrachloride --
-2,4-D barium chlordane --
-2,4,5-TP(Silvex) -beryllium -chlorobcnz.cnc:
-chlordane cadmium chloroform --
-bcpl'1chlor -ch.lo ride -o-crcsol
-hcxachlorobenz.ene chromium m-crcsol --
-hcx.achlorobut.adicnc cob.Jt p-crcsol --.
-endrin copper crcsol --
-lindane fluoride:: 1,4-dichJorobenune --
-methoxychlor -iron l ,2-dichlorocthanc -
-toxaphcne -lead -l, l-dichJorocthylcne
--nungancse 2, 4•dichl orocth y lcnc -
--mercury -hcptachJor
nickel hcxachlorobenune ---nitrate: bcxachlorobuta<liene ---sdcnium hcxachloroc:thane --
-silver -methyl c;hyl ketone
FOR LAil USE ONLY -sulfates nitrobcnunc: -
{p-;;L-9t, 19& -thallium pcnLllchlorophcnol -
Date Received vanadium pyridine ---zinc -tetruchloroc:thy lcne
Date Extracted pH trichloroc:lh y lcoc --
ui-lL/-91,, -nw--conductivity -2,4 ,5-trichlorophenol
Date Analyz=d -TDS 2,4 ,6-trichloroplu::nol --Hush point -vinyl chloride
Reported By . endrin --lindJUie ---Date Reponcd --rnethoxychlor
-_-:-. .-__ ~ -.~ ,'). ,. r---Loxaphcnc
Lab Number • .•. '\_jl_.;,I_,(~.) 2,4-D ----2,4,5-TP (Silvex)
OHS 319! (Ri:vi1cd l~/93)
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SAMPLE ANALYSIS REQUEST Si.de Labom.ory of Public He.11th
P.O. Bax 28047, 306 N. Wilrnini:ton St.
. Ralc.ii;h, North Carolina 1761 l·B047
NC·Dcpanmcnt of Environment,
i-i'c.a!Ln, & Naw"cal R.c.wurce,
Solid W1'1.1: Man.ai:cmc.ru Divi,ion
Site Number ______________ Sample ID Number/Name ....=(n...,__l_,_r_O_O_l/,__-_.5~W _______ _
Name of Site ~ 0'1::11-4-q{'a/;I _. ColloctroBy ________ ~_ lD #_,__f---,o/,____
SiteLoc,tion o< a1v.· -~/;,J &.h foc?..nate Colkctcd Time u.-I ✓Superfund Agency: Hazardous W a.ste Solid Waste TCLP Compounds ----
Sample Type lnori:anic Com pow,d.s Result.s(mg/1)
Environment:11 Concentrate Comment5 -arsenic
barium -
Ground Water (1) Solid (5) -cadmium --
~Surface Water (2)
-chromium
Liquid (6) -lead --mc:rcury
Soil (3) Sludge (7) -sekn.ium --silvc:r -
-Other (4) Other (8) ----
Organic Chemistry Inorganic Chemistry -
P~eter Results (mg/!) Parameter ResullS(mg/1) (mg/kg) Organic Compow,d.s Rc,;ult.s(mg/1)
_ P&T:GC/MS antimony -bcn.unc --Acid:B/N Ext. arsenic carbon tetrachlorid.c ----
-2,4-D barium chlordane --
-2,4,5-TP(Silvex) beryllium -chJorobcnzcnl! --
-chlordane cadmium -chloroform -
-heptnchlor --ch.loridc: -o·crc:;ol
h c:: xach.l o ro ben.z.en e chromium m-crc::.:ml ----hc::xach..lorobuL.ad i c:nc: cobalt p-cresol ---
-c:ndri.n copper crc::sol --
-lindane fiuoride 1,4-dichloroben:z.ene ---
-methoxychlor --iron -1,2-dichloroethanc:
-toxaphc::nc lead l, 1-dich.loroethylenc ------nunganc.sc:: -2, 4~d ichl oroeth y lt::nc
---mercury -hc:pt.achlor
nickel hi:x.achlorobenzenc ----nitrate bexachlorobuu,diene ----selenium hc:xachloroethanc ---
--silvc:r methyl c\hyl ketone -FOR LAil USE ONLY --~ulfutes nitrobc::n.une -
b -1 ;i-?t,,, t3~0 thallium penu.chloropbenol ---Date Received vanadium pyridine --z.inc 1etruch1oroethylcnc ---Date Extracted pH ---trich.lorocthy li:oc:
--conductivity -2,4,5-trichlorophenol
Date Analyzed Ca-llf-Cfle -fJW-TDS 2,4 ,6-trichlorophcnol --
--flu::.:h point -vinyl chloride
Reportro By . cndrin ---I linWllle ---Date Reported ---mcthoxychlor , .... , ·" ···s toxaphcne
Lab Number :._y '\:;, U lj l~ • ---
---2,4-D
---2,4,5-TP (Silvex)
DHS 3191 (Rcvi~cd l:!/IJJ)
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-NC-Dqi•~ni of Environment,
.H.ullll, &. N,rural RUDurcc,
Solid Wu~ M,nai;cmcru Divi,ion
SAMPLE ANALYSIS REQUEST S1.1.1c Laboui.ory of Public H,;.a.llh
P.O. Box 28047, 306 N. Wilmini;wn St.
Ralcii;h, North Carolin.27611-&047
Sit<:Numbcr ______________ Slllllple!D Numbor/Nlllllo ......,.G=-=l,'-_c)___.c()...;S;;__-..:5=--_w ______ _
~ uM1.A-q'9a/:--) _. C,,llc:.::tc:,:!By ________ ~_ ID#_,-;)_"--'~"'-·-·_ Name of Sit<:
Sit,: Loc.,.tion £J d.v._' -~/;.J,1h fae?.nateCollc:.::td Time '-"' I ✓Supafund Agency: Hazardous W a.st<: Solid W a.ste TCLP Compounds ----
Sample Type lno11:.ulic Compowuls Results(mg/1)
Environmental Concentrate Comments arsenic -barium -
_ Ground Water (!) Solid (5) -cadmium.
/Surfae<: Wa<er (2)
---ch.rom.iurn
Llquid (6) l""d ----mercury
-Soil (3) Sludge (7) -selenium -!iilvcr -
-Other (4) -Other (8) --
-
Organic Chemistry Inorganic Chemistry -
~eler Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compounds RcsulLS(~g/1)
_ P&T:GC/MS --antimony -benune
-Acid:B/N Ext. .t:1.rsi::nic Cll.Ibon tetrachloride ---
-2,4-D barium chlordane --
-2,4 ,5-TP(Silvex) --boryllium -chloroben.une
-chlordane cadmium chloroform --
-bopucWor -chJori<le o-cn:.sol --hexach.lorobco.z.ene chromium m-cn::sol ---hexach.lorobutad ienc cobalt p-cre::iOI --
-c:ndrin coppa crcsol --
-lindane fluoride 1,4-dichJorobc:n:z.coe --
mothoxychlor iron 1,2-dichloroctha.r.•.: ----
-toxaphc:nc --I .:ad J, J -dicWoroethylcne -
--nunganese -2, 4-d ichl a roc:thy !enc
---mercury -hcptacWor
nickel bcxachJorobcnzene ----nilralc bcxachlorobutadienc ----selenium hc:xachlor·oelha.nc -----silver methyl o\hyl kotone -FOR LAB USE ONLY --::.ulfotcs n.itroben.z.ene -
b-/J--9(P f3£) --thallium ponlJlcWorophonol
Date Receive:,:! -vanadium pyridino ---
--2.inc letruch!oroeth y l enc -Date Extractc:,:I --pH -lrich.Joroc:th y lcne
--conductiviry -2, 4 ,5-tricWoro phenol
Date Analyw:I &-16 -9& --out: -TDS 2,4,6-trichlorophcnol ---flu.sh point -vinyl chloride
Rcportc:,:I By . cndrin ---lindane ---Date Reponc:,:! ---melhoxychlor
1.:: -~ ~ .-., •'"\ s . --loxaphene
. Lab Number ~-11.~•.J 1.)i 7 -
---2,4-D
---2,4,5-TP (Silvex)
OHS 3191 (Ri:visciJ 11/93)
NC-D~1.rtm£nt of Environment,
"t¾°c.a.lth, &. Na.Weal R~urci:,
Solid Wa.w;. Mua~cmc:nl Divi,ion
SAMPLE ANALYSIS REQUEST S1.&le l...a.bora.i.ory of Public He.a.Ith
P.O. Box 28047, 306 N. Wilmini;ton S1.
Ra.lc:ii:h, Nonh Ca.roli.n.a ::?.7611-&047
,cl--/oS-5 lJ I Site Number . S=plc!D Number/N,me _..:V:::....7..:c._.L __ __::_.....::::.__ _______ _
NmeofSite ~ ?0:z14 ~a,1:.1 ... Oillccte,!By _________ ~_IDU_=:3__,/'----
I SitcLo~tioo £!.dv_. -~/,u~ feDatcCollccttil u-I ✓Superfund
1 Agency: Hazardou.s Waste ----
Sample Type
I Environment..'l1 Concentrate
Ground Water (1) Solid (5)
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--
✓ Surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
P~eler Results (mg/I)
_ P&T:GC/MS
Acid:B/N Ext. --2,4-D
-2,4,5-TP(Silvex)
chlord=e --beptachlor
hc:x.achlorobcn:z.ene -hcx.achlorobutad i enc -cndrin -lindane --··· --mcthoxychlor
-tox.aphcnc
----
FOR LAB USE ONLY
Date Received & -µ -9t, I/cl
Date Extracted
Date Analyzed {o-{_~-9& -tlW-
Reported By
Date Reported
Lab Number
. '.·· ., , .. 8 0 ~:_;J·i.};:j
DHSJ191 (Ri:'Ji.1cJ 11/?J)
Solid Waste
Comments
Inorganic Chemistry
Parameter Results(mg/1) (mg/kg)
--antimony
arsenic --barium ---beryllium
cu<lmium -ch.lo ride -chromium -cobult --copper
fluoride --iron --lead ---nunganesc
-mercury
nickel --nitrate --selenium --silver --sulfutcs --thallium --vanadium -i.inc --
--pH
--conductivity
TDS ---fl,.,h point .
----------
--
Time
TCLP Compounds
Inorganic CompowH!s Result.s(mg/1)
arsenic -barium
cadmium -chromium -l""d --mercury
sc:lc:n.ium -~ilvcr ----
-...
Organic CompoW1ds Rcsult,;(mg/1)
bcn.u:nc: -carbon letrachloridc -chlordane -chlorobcnzenc -chloroform -o-crcsol -m-crc!i'ol --p-crcsol
cn:sol --1,4-dichlorobcnune
-l ,2-dichJorocthane
-I, 1-dichlorocthyknc
-2, 4-dichlorocthylcnc
-hcpt..achJor
hcxachlorobcnzcnc -hcx.acWorobutac.liene . -hcxachloroelhane --methyl eµ>yl ketone
nitrobcn.2Cnc --pentach!orophcnol
-pyridine
-Letruchlorocth y lcne
-trichloroc:.thylcoc
-2,4 ,5-lrichloraphenol
-2,4 ,6-trichlorophenol
-vinyl chloride
cndrin -!indane --methoxychlor
-loxaphcne
-2,4-D
-2,4,5-TP (Silvex)
SAMPLE A.1'/ALYSIS REQUEST SL&Lc l..aboui.ory of Public H,;.dlh
P.O. Box 28047, 306 N. Wilmington St.
Ral~ii,:h, Nonh Caro\U\.l 21611-8047
NC Dcparun.cn.t of Environment,
.H.c.&l~, &. Naalul R~urci;,
Solid WuLc Man.ai:cm,;nt Divi,ion I Sii.eNumber _____________ Su.mple!D Number/Name U, {._. -0 0 J -'PW
NuneofSit.e ~?0:n,,Q.~oA-1---Co!lc.ct"'1By _________ ~_ID# i 7
I Sit.eLDc,.tion ,{) a1v..· -~/;,Jt'J..fe fa6atcColkcwl /,7 -I /-9 (p Time CJ,, j ✓Superfund
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Agency: H a.z.a.rd o us Was t.e ----
Sample Type
Environment1l Concentrate
V Ground Water (1) -Solid (5)
Surf= Water (2) Llquid (6) --
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
P~eter Results (mg/I)
_ P&T:GC/MS
Acid:B/N Ext. -2,4-D -
-2,4 ,5-TP(Silvex)
ehlordAne --bepuichlor
hc:xachlarobco.z.cne -hexa.chlorabut.adienc: -cndrio -!ind.we --methoxychlor
-tax.aphc:ne
--
. --
FOR LAil USE ONLY
Date Received & -1~ -9v 13.0
Date Extracted
Date Analyud &-18 9&-nur::
Reporl"'1 By
Dale Rcponed
Lab Number ; ... , r-q9 ~J ~; \J,(),__. ...
DHS 3191 (Ri:vi1cd 11/9J)
Solid Wa.,tc TCLP Compounds
Inorganic Compowul.s RcswLS(mg/1)
Comments -arsenic
barium -cadmium -chromium -lc.td --mercury
selenium -!:iilvcr ----Inorgaruc Chemistry -
Parameter Results(mg/l)(mg/kg) Organic Compounds Rcsu!LS(mg/1)
-antimony -bcn:z..ene
.11rs!!nic carbon letrachloride --barium -chlordAne I -
-beryllium -chJorobcnzcnc
cudm.iurn ch.Joroform --chloride -o-crcsol -chromium m-cresol --cobalt p-crcsol --copper crc!:iOI --
fluoride 1,4-dichlorobcnune --
iron -1,2-dichJorocthanc -lead --l, 1-dichloroethyknc
-nun g an CS(! -2, 4-dichl o roc:tby h:ne
-mc:rcury -hcpwchlor
nickel -hcx.achlarobcnz.cnc -nitralt: bcxachlorobut.adiene --
selenium hcxachlorocthanc --silver --methyl e\hyl ketone
sulfutes -n.itrabc:n.unc --thallium pcnt.achlorophc:nol -vanadium pyridine --zinc --tetrachloroeth y !enc
-pH -tricWoroethylcnc
-conductivity -2,4 ,5-lrichlorophenol
TDS 2,4 ,6-trich!oroplicnol ---flush point -vinyl chloride
. . cmlrin --lindllne ----methoxychlor
--toxaphcnc
--2,4-D
-2,4,5-TP (Silvex) -
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, NC Dq,•rtmcnt of Environment,
HulLtl, &. N,.C!Jul Rc:.wurcc,
Solid WuLc Man.ai:cmcru Divi,ion
SAMPLE ANALYSIS REQUEST S1.&Li; Laboruory of Public Health
P.O. Box :?80-i?, 306 N. Wilrnin,.;ton SL
R.alc::ii;h., Nonh Carolina 27611-RO~?
Sii,:Numbcr Swnple!DNumbcr/N=c {p(__,. ~<JO 2 -/Jt,,._} ------------
Na.me ofSii,: ~ ½'.'.f:'.?'yQ-ot'oAI--Collected By _______ ~_ IDU L/ D
Site Location ;{J cJl,v..' /4..-5hAJ. ~ ,.i(? . .Da1<:Collo::td Time ,__,:: ,_._._
I ✓Superfund Agency: Hazardous W asl<: --Solid Wast,: TCLP Compounds --
Sample Type lnori:aruc Com powul.s Results(mg/1)
Envirorunent.'11 Concentrate Comments arsenic -
/ -barium
_ Ground Water (l) Solid (5) cadmium ---chromium -
Surf=: Water (2) Liquid (6) l""d -----mercury
Soil (3) Sludge (7) selenium ----~ilvcr -
-Other (4) -Other (8) ---
Organic Chemistry Inorganic Chemistry -
P✓u:eler Results (mg/!) Parameter Results (mg/I) (mg/kg) Organ.ic CompoWlds Rc:iults(mg/1)
_ P&T:GC/MS --antimony -bcn.unc
Acid:B/N Ext. 11.rscnic c:irbon tetrachloride ----
-2,4-D barium chlorWllle ---
-2,4,5-TP(Silvex) --beryllium -chJorobenune
chlordane ca<l!1l.lum chloroform ---
-heptachlor --chloride o-crc:;;ol -
h c x.ac h1 a ro bco.z.cn e chromium m-crc::iDI ---
-hcxach.lorobut..adicnc cobalt p-<:resol ---
-endrin copper crc~ol --
-linWl!le fluoride 1,4-dichlorobcnune ----
-methoxychlor --iron 1,2-dichlorocthanc -
-toxaphcnc --l~d 1, 1-dichloroethylcnc -
--nun ganesc -2,4-dichloroctllykne
---mcrcury -hcptachlor
---nickel bcxachJorobcn.z.enc -
---nitrate bexachlorobulA<liene -selenium hcxachlorocthanc ---
--silver methyl e;hyl ketone -
FOR LAB USE ONLY :i:ulfates nitrobcn.z.cne ---
{p -/;I -9t, t3£) --thallium pentachlorophenol
Date Receive<!
-vanadium pyridine ----z.inc tetrachlorocthy lcnc -
Date Extracted pH trich.loroethylcnc ---
--conductivity -2,4 ,5-trich.Jorophenol
Date Analyzul G,-1 B-9u 7'/v.r TDS 2,4 ,6-trichlorophtnol ---
--111.,;h point -vinyl chloride
Reported By . cndrin ---linclane ---
Date Reported ---methoxychlor
'.' ·~-: 0 90 ---Loxaphcoe
Lab Number ..__r ·U 0 \.; -2,4-D ------2,4,5-TP (Silvex)
D11S 3191 (Re~i1i:d l~/93)
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· NC D91runcn1 _of Environmcn.1,
Huhn,&:. N10Jr1l Rc.ourcc,
Solid Wa.Lc M1ru.cmcru Di..,i,ion
SAMPLE ANALYSIS REQUEST SLatc Labou1.0ry of Public Hc.&lth
P.O. Box 28047, 306 N. WilmingLOn St.
Ralcibh, North Carolin. 2761 l-R0~7
/'coo3-?'·' Sii.::Number _______________ Sample ID Number/Name -~W~ ______ ,._l....'__f.;V__.::c ______ _
NameofSit<: ~A LvnY+-oea/41--Collo.:tedBy ______ ~_ lD#--1-st'---L3 __
Si 1<:Loc,tion I? obA. -~/;,ua_At ;1;c?__natcCollo.:ted Time u-I ✓Superfwid Agency: H=dous Wasi.e --Solid Waste TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/l)
Environmental Concentr;ite Comments arseruc -·. barium
V Ground Water (I)
-
Solid (5) -cadmium --chromium -
-Surf au Water (2) Llquid (6) -lead ---mercury
-Soil (3) Sludge (7) -!ielcn.jum --~ilvcr -
-Other (4) --Other (8) ---
Organic Chemistry Inorganic Chemistry -
P~eter Results (mg/I) Parameter Results(mg/l) (mg/kg) Organ.ic Compounds Rcsults(mg/1)
_ P&T:GCIMS anlimony -bc::nu:nc --Acid:B/N Ext. 11.rsc::ruc carbon tetrachloride --
-2,4-D barium -chlonLu,c ---2,4,5-TP(Silvex) --beryllium -chJorobcn.zcnc
-chlordn.nc cadmium chloroform --
-heplJlcWor chloride 0-CfC!iOl ----hcx!l.ch.lorobcn:z.ene chromium m-crc!iol --
hcxachlorobuLadicnc --cobalt p-cresol -
-cndrin copper cresol --
lindane fluoride 1,4-dichlorobenune -----mdhoxychlor --iron -1,2-dichloroethanc
-toxaphenc --lead 1, l-dichJoroethyknc ---rru.ngancse -2,4-dichloroethylene
mercury hcpt.:J.chlor ' ----nickd hcxachlorobcnzenc ----nitr.lle hexachlorobutadiene ----seknium hcxachlorocthane ---silver methyl c\hyl ketone --FOR LAU USE ONLY --:i.ulfotes nitrobcru.cnc -
4' -1,:,2. -'1 t .6'~ -thallium pcnLuchlorophcnol
Date Received -vanadium pyridine ---z.inc letrachloroc:thylc:nc -Date Extracted --pH -trichloroc:thylcnc
--conductivity -2,4,5-trichlorophenol
Dale Analyzed &-19 9& --rzw: TDS 2, 4, 6-trichl ore pheno I ----11,..,h point -vinyl chloride
Reported By . cn<lrin ---lindane ' ---Date Reported ---methoxychlor
; . ~:_~ ·-~ r. , . ---toxaphene
Lab Number . __; ,_, '-; u ~ 1 2,4·D ---
---2,4,5-TP (Silvcx)
DHS Jl9l (Rcvi~cd l'1/9J)
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•N.c, D~an..rmru of Environment,
Hullh, 6:. Nawul R.c:40urci:;,
Solid Wut.c M.aru~cmcn1 Divi,ion
SAMPLE ANALYSIS REQUF.ST SLlle Laboutory of Public Heail.h
P.O. Box 211047, 306 N. WilminJ:ton Sl.
R.alcii;h, North Caroli..ru 27611-11047
Sit.eNumbcr --------------S=plc!D Number/NiUilc _U""'-n,__L._-0---'----'-o--'V_-_,_g___:;w_.::,_ ____ _
Na.me of Sit<: ~;,tvnlA-~41---Coll~t«!By ______ ~_ID#_~L-..-..:!.v __
6< dv_' ~/;,u ~ /DC!_nat.e Coll~tcd I Sit.el.oc.,.tion c,:; I ✓Superfund
Time
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Agency: --Ha:z.ardous Wa.st.e --
Sample Type
Environment..'ll · Conc:f'nt[i!te
/ Ground Water (I) -Solid (5)
-Surface Waler (2) -Liquid (6)
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
P✓Peter Results (mg/I)
_ P&T:GC/MS
Acid:B/N Ext. -2,4•D --2,4,5-TP(Silvcx)
chlordane --heplJlchlor
h ex.achlo re be112ene -hex.ach.1orobut.a.diene -cndrin -lindanc --mcthoxychlor
-toxaphcne
-
--
-
FOR LAU USE ONLY
Dale Received (p -1 .J--9y 6&
Date Extracted
Date Analyzul {.,2_-/8-Ci& 7/eu-
Reported By
Date Reported
ub Number .. ,-'(1-':)0 .. :_; 1.) '-j ,;: .. ' ,:r..
OHS 3191 {Revised 11/93)
Solid Wa.st.e TCLP Compounds
lnor,:anic Compow1ds Results(mg/1)
Comments -arsenic
barium -cadmium -chromium -lead --mercury
selenium -~ilvcr -
---Inorganic Chemistry -
Parameter Results(mg/1) (mg/kg) Organic Compowids Rl::iults(mg/1)
-antimony -bc=n.unc
llfSC:IUC carbon te.trachlorid::. --barium -chlordane --beryllium -chJorobcn.zc:nl!
cadmium -chloroform -chJoridc o-crc~ol --chromium m-cn::wl --
cobaJt p--cresol --
copper crc::;ol --fluoride: --1,4-dichlorobcn:z.ene
iron l ,2-dichloroc:.thanc --
-lc:ad 1, l -dichlorocthylcnc -
-nun ganesc -2, 4-d ichlorocthy l enc
-mcrcury ~ hcpt.:.1chlor
nickc:I he x.ac hl o rob cn.zcne --nitrate bexachl orobu ta<lienc: --
selenium hcxachlorocthane ---silver methyl e,hyl ketone -:.ulfou:s nitrobcn.unc ---thallium pcnLachlorophcnol -vanadium pyridine ---zinc letrach!oroethykne --pH -trich!orocthylcDe
-conductivity -2,4,5-trichJorophenol
-TDS -2, 4, 6-lrichl ore phenol
-flu,h point -vinyl chloride . cndrin --lindane ----methoxychlor
--toxaphcne
2,4·D --
--2,4,S·TP (Silvex)
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• N_C_ O~•rtmc.nt of Environment,
Hc.a.11.n, &: Narur.al R.c.ourc:c:,
Solid Wutc Mana~cmcru Oivi,ion
SAMJ>LE ANALYSIS REQUEST Su.!.(. Labora.LOry of Public: Hc.alth
P.O. Box 28.().;7, 306 N. Wilminr:tcn St.
R&lc:i1,;h., Nonh Carolin.a 27611-8047
/;._ l,.-00 ,_ /J,. 1 Sit<: Nwnbcr _______________ Su.mp le ID Number/N=e _ _,U"--' J ______ ...l_-'0_'-::.C/V_:_ _____ _
Name of Sit<: ~ ?0::zt-4, of'a/;.J _. C,,Jlected By ________ ~_ID #____,,~"---'o:::::...___
S j t<: l.Dc, ti OD ,,{) a1v._· -~ /; ,U a_h ;(;C..Uat<: Collected Time '--"' I ✓Superfund Agency: Hazardous Wast<: --Solid Wast<: TCLP Compounds --
Sample Type Inorganic Com powids Rcsult.s(mg/1)
Environment.-il Concentrate Comments -arsenic
barium ✓ Ground Water(])
-
Solid (5) -cadmium --chromium -
Surface Water (2) Llquid (6) -lead ----mercury
-Soil (3) Sludge (7) -selcn.ium -!iilvcr -
-Other (4) Other (8) ----Organic Chemistry Inorganic Chemistry -
P~eler Result.s (mg/1) Parameter Result.s(mg/l)(mg/kg) Organic Compowids Rt.:Sult.s(mg/1)
_ P&T:GCIMS antimony . bcnu:nc --
Acid:B/N Ext. .ll.rsen.ic -curbon tetrachloride --2,4-D barium chlorWUle --
-2,4,5-TP(Silvex) -beryllium -chJorobc::n.z.::nc
-chlordane cadmium chJoroform --
-hcpt.achlor -chloride:: -o-crc!iol
-hcx.achloroben.une chroITUum rn-crcsol ---hcxachlorobutadicnc cobalt p-<:rcsol ---
-cndrio copper crcso! --
-lindane fluoride 1,4-dichlorobcnz::ne --
-mcthoxychlor -iron -l ,2-dichJorocthanc
-tox.iphene -IC'1d I, 1-dichlorocthylene -
--nunganl!Se -2, 4-d ichl a roe th ylenc
--mercury -hcpt.ach.Jor
nickel bcxachlorobenzcnc ---nitrate bcxachlorobutadiene ----selcnjum hcxachloroelbane ----silver methyl e;hyl ketone -FOR LAB USE ONLY -sulfotcs nilroben.zene -
&-/,,L-1(,tj;Q -thallium penLachJorophcnol
Date Received -vanadium pyridine --
-z.inc letrachloroelhylene -Date Extracted -pH -trichloroethylenc
(;-;tf-91; -conductiviry -2,4 ,5-trich!orophenol
Date Analyzed 7/W--TDS 2, 4, 6-trichl orophcno I -
--flush point -vinyl chloride
Reported By . cndrin ---linWU1e --Date Reponed --mcthoxychlor
, .. _· 1'~33 ---loxaphcnc
Lab Number •.J vu,_,, '.!,4-D -----2,4,5-TP (Silvcx)
O!IS 3191 (Rcvi:.cd l'l/93)
,, -·-·-··'·•'·•· ... -
. NC: Deyartmeru of E.n"Yironrncnt,
Huhn, &. N.Wrai R~urcc:,
Solid Wut.c t.-bna•cmcru Divi,ion
SAMPLE A.1\'ALYSIS REQUEST S1.&1i: l..&borai.ory of Publii: Hc.tllh
P.O. Box 280-t?, 306 N. Wilmini:i.on Si.
R.alci1:h, North C.rotin.a 27611-8047
Si1':Numbcr ______________ Samplc!DNumbcr/Namc Vl {_ -0 0 & -f b<.}
I Name of Si1': ~/, 0'n'!-4-o('a/?-J ~ Collcctctl By _________ ~_ ID II 5 3
,(> a1v._· ~/;,u,~ fo0a1':Collcctd I Si td.Dt:.1UOD w:: 7 ✓Supcrfund Agency: H=d o us Was"' Solid Wa.s1': TCLP Compounds
I ----
Sample Type lnorganic Compounds Resull!i(mg/1)
Environmental Concentrate Comments -arsenic
Time
I ✓ Ground Water (I)
barium -
Solid (5) -cadmium -chromium -
I Surface Water (2) Llquid (6) !cod ----mercury
Soil (3) Sludge (7) sdenium ---.tiilver -I -Other (4) -Other (8) ---
•1
Organic Chemistry Inorganic Chemistry -
Pv':,'eler Results (mg/I) Parameter Results (mg/I )(mg/kg) Organic Compounds Resull!i(mg/1)
~ _ l'&T:GC/MS -antimony -bcn.z.cnc
-Acid:B/N Ext. Hrscruc carbon tetrachloride ---
-2,4-D --barium -chlordane
-2,4,5-TP(Silvex) . --bcryllillm -chlorobcnunc
-chlordane cadmium chloroform --
-hcplnchlar --chloride -o-crc::;ol
-hcxachlorobenz.cne --chromium m-cre:wl -
I -hex.ach.lorobuLadicnc cobalt p-crcsol --
-endrin copper crcsol --
-limLlJle fluoride 1,4-dichlorobcnune ---
I= mclhoxychlor -iron l ,2-dich.loroethanc -
toxaphene -lco<l l, 1-dichJorocthylcne -
I --nunganesi: -2, 4-d ichl oroetby I enc
I ---mercury -hept.ach.lor
---nickel hexach.lorobenz.enc -nitrate hc:xachlorobuta<lienc ----selenium hexachloroclba.nc ---I --silver methyl ethyl ketone -
FOR LAB USE ONLY --:.ulfutes nitrobcnz.cnc -
(p -J;l. --9 (,, 13 j{) --thallillm pent.achJorophcnol -Date Received vanadium pyridine I Date .Extracted
---
--z.inc tetrach.loroeth y l enc ---pH -lrich.lo roe thy lcne
--conductivity -2,4 ,5-trichJorophenol I Date Analyzed 6-l l-/-C/fe -riur -TDS 2,4 ,6-trichlorophcnol -
--fl1LSh point vinyl chloride -Reporlctl By . cndrin ---I Date Rcpanctl --lindane ----methoxychlor
Lab Number _'_; ,;-;.]{)94 --toxapheoc -
I OHS Jt9t (Ro,i"J l:!/9))
---2,4-D
---2,4,5-TP (Silvcx)
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-N_C. D~aruncru, of Environment,
Huhn, & Nao..iul R.e.ourcc,
Solid Wu~ Man.a~i::mcru Oivi,ion
SAMPLE ANALYSIS REQUEST S1.&lc Laboratory of Public Hc.ah.h
P.O. Box 28047, 306 N. Wilmini;ton Sc.
Ralcii;h, Nonh Carollll.127611-8047
I Sit.eNumbcr -------------S=plc!D Numbcr/N..me _ _,V7"--'--_L_-----"0'-0_7_,__-_,/l'--w"-"''--------
Nameof Site ~ ½'.'.Y'.?1A, if'o.AJ,.. Collcctc:,l By _________ ~_ ID #_~5'"--'(o=---
,(} d,v_' ~/;_u a__h ;t(:J)atc Collected I Sitcl.oc.,.tion c.,:; I ✓Superfund Agency: H=dous Waste --Solid Waste TCLP Compounds
I --
Sample Type lnor,:aruc Compow1d.s Result.s(mg/1)
Time
Environment.'11 Concentrate Comments -arsc:ruc
I J:('Ground Waler (I)
-ba.rium
Solid (5) -cadmium --chromium -
I Surface Water (2) Liquid (6) -ICJ<d ----mercury
Soil (J) Sludge (7) selenium ----.::;iJver -I -Oilier (4) Other (8) -----
I Organic Chemistry Inorganic Chemistry -..
~eler Results (mg/I) Parameter Resull.s(mg/l)(mg/kg) Organic Compowid.s ResulLS(mg/1)
I _ P&T:GC/MS antimony -bc:11.Ztnc --
-Acid:B/N Ext. -.t1rsi:nic -carbon tetrachloride
-2,4-D barium ··-chlorruine -
I -2,4,5-TP(Silvex) -beryllium -chJoroben.z.cnc
-chlordane cudm.ium chloroform --
hcptachlor chloride o-cre!>ol ---
-hcx.achJoro ben2.ene chroITUum m-cre!iol --
I -hexachlorobuLadicnc cobalt p-cresol --
-cndrin copper cre!iol --
-lindane fluoride 1,4-dichJorobeo.uoe --
I -mcthoxychlor -iron l ,'2•dichJorocthanc: --1ox.aphenc -lead I, 1-dichJoroclhylcne ---m,;i.nganesc -2, 4~d i chi o roethy I enc
I ---mercury -hcpuchJor
---nickel hexach.Iorobcm.coc -nitrate bcxachlorobutadienc ----sc:leniurn hexachloroethanc ---I -silver -methyl e!hyl ketone
FOR LAB USE ONLY --~ulfutes nitroberu.c:ne -
if -µ-9? ,6{) -thallium pcnt.u.chlorophcnoJ -
I Date Received vanadium pyridine --
-zinc Letruchloroethylcne -Date Extracted pH lrich1orocthylcoc ---conductiviry -2,4,5-trichJoropheool
I Dale Analy:z.ed &-1cr-q& ..,,,w--TDS 2,4,6-trichloroph~nol -
--Hash point -vinyl chloride
Rcportc:,l By . cndri.n ---
I ---lindane
Date Reportc:,l -methoxychlor -
~~~ -~: _J ,;:) 3 S --loxaphcoe
I ub Number 2,4-D --
DHS 3191 {Revised l~/93) ---2,4,5-TP (Silvcx)
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SAMPLE ANALYSIS REQUEST S1.1.1c Labor&Lory of Public He.11th
P.O. Box 28047, 306 N. Wilm.ini;ton St.
Ralc:i1:h, North Carolin.a 21611-BO•t?
.~c. Dcpa~ni. of Environment,
Hc.allh, & NaDJ.ral Rc..ourcc,
Solid Wau.c M.uui;cmcru Divi,ion
Si«:Numbcr ______________ SlWlplclDNumbcr/Name U) {__-Q O y-f)u.J
Name of Si«: ~h Wl:1'l-:Q-ef'a/'d .-Collcct«!By ______ ~_ID# 5' CJ
I Sile!..o~t.ioo £!._dv._' ~/,ua__h ;iiDai,:Co!lccted u:: J ✓Superfund
Time
Agency: Ha.z.a.rd o us Was«: Solid Wast,: TCLP Compounds
I ----
Sample Type Inorganic Com powHis Resu!ts(mg/1)
EnvironmenL1l Concentrate Comments -arseruc
I ✓ Grouod Water (!)
barium -
Solid (5) -cadmium -chromium -
I Surface Water (2) · Liquid (6) load ----mercury
Soil (3) Sludge (7) selc:aium ---silver -I -Other (4) -Other (8) --
-
I Organic Chemistry Inorganic Chemistry -
PVi,'eler Results (mg/I) Parameter Results(mg/l}(mg/kg) Organic Compounds Rcsults(mg/1)
I _ P&T:GC/MS --anlimony -benunc
-Acid:B/N Ext. ursen.ic carbon letrachloride ---2,4-D barium chlordane --
I -2,4,5-TP(Silvex) --beryllium -chlorobenzcnl!
-chlordane cadm,jum chloroform --beptochJor chloride o-crcsol ----
-hexachlo ro ben..z.ene chromium m-crc:~ol --
I -hcxachlorobu tad i c:ne cobalt p-cresol ---cndrin copper crc:!iol --
-liniline fluoride 1,4-dichlorobenunc ---
I -methoxychlor --iron 1,2-dichloroethanc -
-toxaphenc --lead I, !-dichJoroethylcne ---rrungancse -2, 4-dichloroeth y l enc:
I ---mercury -hcpt.achlor
--nickd hcx.acltlorobcn.unc -nitrate bcxachlorobuta<liene ----selenium hcxachlorocthane ---I -silver methyl e\hyl ketone -FOR LAB USE ONLY --.sulfu.tes nitroben.:z..:nc -
(p -µ -9~t3& --thallium penlllchlorophenol
Date Received -
I vanadium pyridine ----zinc tetrachloroethylc=nc
Date Extracted ---pH -trichlorocthylcnc
--conductivity -2 ,4 ,5-trichJorophenol
I Date Analywl (0-1 <l-C/fo 721J.t--TDS 2,4,6-trichloropheno\ ---flush point vinyl chloride -Report«! By -cndrin ---
I --. !inWllle
Date Repor1ed -methoxychlor ---\ ~ ...... , ..... _1"\3 ...... toxaphcne . .. . '-t
Lab Number
.. ..., vvv .) ---
I DIISjJ91 (R"'"' 1::!/9))
---2,4-D
---2,4,5-TP (Silvc<)
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}:'~ Dcpanmcru, of Environment,
Huhn,&. Nawul Ruource,
Solid ViuLc Man.a~cmcru Divi,ion
SAMPLE ANALYSIS REQUEST Su.tc Uboul.Ory of PubiiC Hc.1.lth
P.O. Bo:1 28047, 306 N. Wilm.ini;I.On St.
Ralcii;h, Nonh Carolina 1761 l·BO,t?
Site Number ______________ SIUllplc!D Number/N.me __ U)=~_-(__ __ -_Q_....cQ'-'/'---__,~c......1;/)c..""'------
Na.me of Site ~fl w:n1A-o{'ajv,.. Collectc:,JBy ______ ~_ ID#___,V""--"'.).-=-----
Siteloc,ition ,{J o.1.v._· ~/;,u,~ faC:.nate Collectci Time '-"' I ✓Superfund Agency: Hazardous Wa.ste Solid Wast<: TCLP Compounds ----
Sample Type lnorxaruc CompoW1d,; Resu!ts(mg/1)
Environment.11 Concentrate Comments arse:Wc -barium -
-Ground Water (!) Solid (5) -cadmium -chromium --Surface Water (2) Liquid (6) -l""d --mercury
--Soil (3) Sludge (7) -selenium --
✓Othfr (4)
-silver
Other (8) -7: , -A.Jn . 15--, -
Organic Chemistry Inorganic Chemistry -
~eler Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic CompoW1ds Rcsults(mg/1)
_ P&T:GC/MS --antimony -bcnunc
Acid:B/N Ext. 11.rscnic ca.rboo tetrachloride ---
-2,4-D barium chlordane --
-2,4,5-TP(Silvex) -beryllium -chlorobenzcnc:
-chlordane cudmium chloroform ---hept.achlor chloride -O·Cre!>ol --hexachlorobe:n.z.ene: chromium m-crcsol --
-hexachlorobut.adiene cobult p-cresol --
-e:::idrin copper cresol --
-lindane fluoride I ,4-dichloroben.z.ene ---
-methoxychlor iron 1,2-dichloroethane --
-tox.aphene lead l, 1-dichlorocthylcne: ----rrunganese -2, 4-d ichl o rocth y l enc
---mercury -hept,ichJor
nickel hexachlorobcnunc . ---nitrate: bc::xachlorobutac.lienG ----sc:lcnium hc:xa.chloroc:thanc ---
--silver methyl e\hyl ketone -FOR LAB USE ONLY --sulfutcs ni tro bcn.z.cne -
& -i,J--9 {:, diO --thallium pcn1..t1ch.lorophenol
Date Received -vanadium pyridine --
--Unc tetrachloroethylene -Date Extractc:,l --pH -trichloroc:lhylcne
-conductiviry -2,4,5-trichlorophenol
Date Analyw:l &-1 ?-9{p 77ut: -TDS 2,4 ,6-trichlorophenol -
--flu.sh point -vinyl chloride
Rcportc:,l By . cndri.n ---lindane ---Date Reponc:,l ---methoxychlor
' .. · '''37 ---toxaphene
Lib Number .. _.;,c,,,u.(_., . ' 2,4-D ------2,4,5-TP (Silvex)
DHS Jl9l {Ri:vhed 11/93)
a
STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH. NC 27611
I ORGANIC CHEMICAL ANALYSIS
rr========;====r=====;=====r======r===~=;=:====r=====;i
PURGEABLECOMPOUNDS LABNO 'iG,3053 C/u,'3Cfa'f C/u:3065 q~306{J; q(o"3QQ;7 C/u,~086
li:=========~FIE=LD=N=o=;=t=/..=-=o=o=/-=S:.u~=G-=l-=oo=;i=-s=w~&=l=-o=o=:,=-S=w~' =G=L.-=OO='-l=-=5w='*Gt..=-=o=o=5=-S=u:=;';,=6-=L=-='o5===-=5~w~1
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COMPOUND
CHLOROMETHANE
VINTI. CHUlRIDE
BROMOMETB.A.NE
CHLOROETRANE
TRICHLOROFLUOROHrrH.A1fl!:
ACETONE
I IODOM:l;'T'li,\N'E
METHYLENE CHLORID!:
TYPE
J.O ,o
10
JO
5
I CARBON DISULYIDp; I
( ;i__ J
'ppbJpprn I r-rb)pprri
I I I
I I -
( .;2. )
(pp~pprr: rfpi;Jppm
/ J fl I I I 1
• I
In -:r Io :r
I 1 11 I 1 LL
J_,,
I . J
11 ~
TRANS-1.2-DICHLOROETHENE JI' j
lt---------f----"---f--+--+--+---+--+---l----l---+--+----+---+---11
I == ~ I
l,1-DICHLOROl!:THANE: 5 ' / ' / ' /' ' / ,LI ' I
2--BUTANONE I C!S-l,2·DICHLOR0"1'HEN],: 5 I \ t I I i J I '
:J..O I -;r I 3 I J' I :r +,111~.a
I J
CHLOROFORM I I -'·-'·_'•_TRJ_cm.o __ RO_..,._=----+-+--+--'l---+---l---+---l~--+---l-,----+--Jh"--+--l----11
CARBON TrrRACHI.ORIDE ' / '\ /
I I ---~ fflfr-
1.2-mCHLOROE'THANE I , I I
I ,.,__TRJ_C_HLO_R_O_= ______ t--L---+--+,---J--+----ll--+---l--h---l---+---1---+-' .,--~I
11
1,2-DICHLOROPROPAXE I BROMOD!CHLOROMETHANE ,J; ' / ' / \ / '\ / . / ' /
I
c-.?o-:.~ ... e4,:: i-Af3 <.:..:,:,rTAi''HNATio1J CR. BAc.,::.G-R.c;..jND.
J -!atim.ated value
I K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value givec.
0 -Material was analy:ed for but cot detected. The cumber is the Minimum. Detec~ion Limit.
NA -Not 1UU1.ly-zod.
1/ -Tentative ideotificatioc.
I It -C:..Ct-A,Pcu.1!10 REL\ABL.'f 0£T~LlMSLE U"-lL'/ 1N H l(rt-1 C.cNct:.NTRATicN,.),
✓-SAMPd:. i-llfYHl...'/ CiLhTE:W. ,-.10L•~ De ·Nol RPf'LV·.
DEHNR 3065-0 (10/93)
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Pl!RGCOM.ORG
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P!/RGEABLE COMPOUNDS
COMPOUND
l DIBROMOMETRANE
4-ME'THTL-2-PENTANON'E
CIS-1.~·DICBLOROPROPENE
TOLUENE
TRANS-1,3-D[CID.OROPROPENE
l,l,2,2-TrrRACHLOROETHA10!:
l, l ,l-TRICHLO ROETHhl'l'E
2-BZ.XMONE
TrrRACHLOROr:THE?l'E:
DIBROMOCHLOROM?:l"HANE
rrHYIJ!:NE DIBROMIDE
CHLOROBE!'<ZENE
1,1,1,2-TETRACHLOROnHANE
!:THYL B!::'l'Zl!:NE
rru:,ras
,, .
1··::::0R><
:!.:J TRANS-1,4-DICHLORO-l-Btn"ZNE
I 1,2,3-TRICfil.OROPROPANE
l, 4-DlCRLOROBE.'"ttE."fE
I 1,2-DICm..oROBENZENE
1,2-DIBROM 0-3-Cm.0 RO PROP Al"l'E
7 ~ A.CEfATZ
)-1-,41,, -J_ t -1-.u.+,, I e.+lu r
' ' I
STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO
5 fl II l1 /1 /l
,o
5 '/ ' I
LL.-I
JO
5
' I
;o
'g°O
5
I
-!I
,;a::i
;;J-C)O '-I 'I ' I
5 LL (A_ U-
C. -·pM-::aOLc. l-FH3 CcNIH.~tlJAn<.:iN. oR BRc.hC....f<cu,-JI),
I J -Zstim.ated value
~ -Actual value is known to be leas than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The number ia the Mini.mum Detection Lim.it.
ID.. -Not analyzed.
I 1/ -Teotative identification.
'IJ -COI-\PoU.1.iD R:il..\M:;!..y Dt:TE'c1F,6U:: t,\JcY IN HIG-H CCt·.!C[NTRATic~l.'.j,
✓ ·· 5,~MPLf Hl(i·HLY DiLL:.T£D. f~t..,,;_f·:'J th) J\1/...7(' t~.PPL."/.
. DEHNR 3068-0 (10/93)
.I
(iipb') ppm
u__
LL
PURGCOM.ORG
STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047 ~ 306 N. WILMINGTON ST .• RALEIGH, NC 27611
I ORGANIC CHEMICAL ANALYSIS
I PURGEABI.E COMPOUNDS
FIELD NO &l-DO/-Pl)) G-1--ood-~ U-co3-fu! GL-CJ0'-1-P11.. u-i-Do5-P.,J 6-t-cz:,t,,-/-iu
I COMPOUND TYPE c / l c I l C I l ( ( J ( 1 ) ( I l
"ppb) ppm "(-pb) ppm 'ppb )ppm (ppb pp,r..
rHLOROMETHANE JO ( 1 I 1 I I I
CHLORIDE 10
BROMOMETHAN'E
ICHLORO<TRANE
d.0
iO
TRICHLOROFLUOROMZTHAliE iO , I 'I ,/
3 ::r
l,l•DICHLOROJITHENE 5 I l I J I 1
f IODOKE"T1<Alfz:
J,,
METHYLE~ CHLORIDE
I CARBON DISUl.l"IDE J I J
I I TRA.,s-t,l•DICHLOROETH!:NX
I ACRYWNrl'RILE
1.1 • DICHLOROE"TJ:L,\NE
j --I r
I
J,
~ , I
5 l..rflr" ' I
2.-BUTAHONE :20 .;;l ::r I -;r '
Cl.S-L.2·DICHLOROETHZN?: 5 LL / ' /0 ' I
:__ _____ ....\..._.L __ L:itr::sl!~~LlU:.Q.!~"-L:+t.rr'<~Q!JC~e...~_J_.:.;.brC'C"l!·:t::...P~L-J.._ __ Ll+r':r.:.run,r:e_,o.....JI I I +rl"lc_e.... ' '
I l, l.1-TRICHLORO!:THANE +rr1_;P. I , I I I I •
CARBON -nnv..cHLORIDE I ,i.. -
I BENZ!:NX ' J
I l,2·DtCHLOROr::TBANE · /
I TRlCHLOROETREfE 4 ::r :3() I
lf-1_.2_-□_,c_m.o_R_o_,_Ro_,_= ____ -i---_!..---l---4---l---l----4-.JLL,"l=~--1-___,Jl.,::'h,.. _ _j __ !._j __ -!-_-1----1!
1 f-•R_o_"_o_□,_cHLO--Ro_MET __ = ___ f--_\!/1----+--'-/ __ +---\------!---J,;---l---·-L---1--'-I_/· --+--'-/---<I
I
c-.?0 ~~,eLG. L..AB c.:..:..N·cr1Ni1t.JPi1 iO~ oR BAc.K.CtR.c;..ir-JD.
J -Estimated value
I ~ -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was a.n.aly::ed for but not detected. Tho number is the Mini.mum. Detection Limit.
RA -Not a.n.aly:ed.
1/ -Tentative identification.
I ~/ -C:.CM.Pou.l'IP RE!..!f\E,L.'f O!e.T,:cTl"\ELE c,sl'-'/ IN H1i-,-1 C.c;,ccNTRATlc/J';.
✓-SAMPi_~ HIG·Hl...'( CiLhTf::i:::-. t--1D1}-:;, De No! APPLY.
DEHNR 3065-0 (10/93)
I
PURGCOM.ORG
STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMJNGTON ST .• RALEIGH. NC 27611
I ORGANIC CHEMICAL ANALYSIS
1 PUR.GEABLE COMPOUNDS LAB NO qCo3Di?9 9&'3CAO 9w::rA I q(f 3::A.J 9Co3o'73
<:,1,-col-P w 6-L-·OD:J.-Piv Gl-ro3-PciJ 6-1.,-co 1/-PILl uL--Cd5-I'"-' FIELD NO
I COMPOOJVD TYPE < I ) (_ I ) ( -( ) ( I ) ( I )
!J,Wft (ppb ppm (ppb )ppm (ppb)ppfn (pp8) Ff'rn ,,-~b)ppm
IDlllROMOMETRAN?: 5 I 1 I , LL --I I I I
,o 4-ME'THYL-2-P?:NTAMONE
r!S-1.3-DICHLOROPROPENE 5
TOLU!:NE
t TI<ANS-1.3-DICHLOROPROPENE
1.1,2.2-Ttl'RACHLORO P:'t1iAlfE
1.1.2--TRICHLOROl:THANE ,"
2-Hl':.L\ltONE 10
TrTRA.CHLORO~l'fE 5
I DIBROMOCHLOROMETHANE I
~:a; DIBROMID!:
I CHLOROBENZEn
l.l,1,2·-n:TRACHLOROETHANE
I :tTHTLB?:NZENE:
==
I STTR.Em: ' I
BROMOP'OR.M iO
:!d TRANS-1.4-DICHLOR0-2-BUTENE $IO
I 1,2,3--TRICHLOROPROPANE ..5 I
1,4-D[CHLOROBEN'Z?:N?; I -i--r fl ,. "'
I 1.2-DICHLOROBE~ -J; l I
~8 l,2·DIBROM0·3-CHLOROPROPA."<E
1 V!NYL A.CtrATE ;;J_cJQ -, / \I/ ,I/ \ / 'I
M ~-lh'-' 1--f-h ,.j..,_ / eth Fr 5 [,A....,..-Ll-L,L... I 1 I.A-
. I
I , ---..
~ -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
O -Material was analy-::ed for but not detected. The number i• tho Minimum Detection Limit.
NA -Not analyzed.
1 1/ -Tentative identification.
I 1 -cOMP<lu.1JD ~[;I..\Ac'>-Y DE:1f'cTF;5l..e OJLY IN HIG·t-1 cc1·.ICCNTR!Hi6N:i.
✓ ·· :S:•HvlPi...t Hl~·HLY DiLUT£D. fJ.C'L'-:'J DD )v'_,--(" P.f'f~L-/.
DEHNR 3068-0 (10/93)
I
C((_I) ?JcR If-
&l·DOl,,-/1,)
( I ) I
✓,,pl::) ppm
LL-
'
..
,/
'7
PURGCOM.ORG
___.
I
I
rGEABU: COMPOUNDS
CO/dPOUM>
STATE IABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO CjC,3)95 qCo3cR&i qc.,,3Jq7
FIELD NO &L."CD7-Pw &l -DO'i;-fr,J Gt.,·00/-713
TYPE ( I ) c I ) 14 ) ( ) ( )
I M ~i,')s (ppb /ppbJ ppm ,rrb;pprn ,, ppb ppm ppl' pp,-r: ppl' ppm_
_
1
'1.0ROM:ET!W<E J..O , J u_ I l
NY!.-CHI..ORIDE 10
BROMOM..ETRA."fE ,;;J,0
ERO=<ME iO
TRICHLOROFLO'ORO!O!;'T'RA."fE iO ,/ ' I
1~~0N1': ;;i.o 4:5 Lt :r
-DICBLOROZTHENE 5 I ' I I
1~== HYlZN?; CHLORIDE EON O!SUI.FIDE
S-1.2-D ICHLORO l!:THE:"f'E J,,
<Cim.olilTRIU ;;!Li
1.l-OICHLORO=<ME 5 ' I 'I
:1-BUTANONZ .;:2.0 +r-11 Cf'..., 1-:r
(!S-1,2-DICHLORO?;Titt,<,: 5 '/ I 1 LL-
l Cffi,QROF'ORM I +vnce_ -l--rt1rt°
,1,1.1-TRICHLORO~IW<E I I ) • +,Cl.ce..,..
I CARBON TrrRACHI.ORIDE I
l·BENZ!:Nl': I
1,2-DICHLOROJITHANE. I
t TRICBLORO= I
1,2-DICHLOROPROP.t\l'l'E I
BROMODICHLOROMETRAN!: ,J; \/ \/ \ I
. . c-.Po-:;!,,el....l::. 1..A8 G.:-N1Ai'ft1NP..Tiot-J oR. BAc.,::-.,6-R.c~ND .
J -Estimated value
L -Actual value is known to be greater than value given. I ~ -Actual value is known to be less than value given.
0 -Material was a.naly:::ed for but not detected. The number
&A -Not a.naly:::ed.
is the Mini.Jnum Detection Lim.it.
1/ -Tentative identification.
I J_/ -C.Ci'!,_P~u.!'10 RE~lf\E,. L'f D£Teci'(-l\:;t..£ G"lL'/ IN H l(nl
✓-SAMPu~. t-\lG·i-11...'/ Oil-l.Tf'u. f-.1\D1.1~ Uc NoT RPP;_y·.
DEHNR 3065-0 (10/93)
I
c.c,-..JC( NT l<ATic>J').
( )
pp/;; 1-"PiT1
FURGCOM.ORG
I
I
I
I PUR.GEA.&E COMPOUNDS
I COMPOIJJVD
t. rBROM0""'2"HANE
4-METHYL-2-nxr Al(ONE
ES-1.>•0ICHLOROPROPENE
OLUENE t TRA.SS-1,3-DlCHLOR0PROPENE
1.1.2.l·T?TRACHLORO!:TB.-VfZ
l, l,2-TRICfil.OROE'TBANE
2-ll:EL\lfON!:
STATE IABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611
ORGANIC CHEMICAL ANALYSIS
LJIB NO q (o3()q.'5 qc.., 3oC/ <.o qec3oq7
FIELD NO c-,,-co7-Pw Gl·CD'i-·fu.J 6-l--001 -T.8
TYl'E c I ) ( l ) ( 'f ) ( ) ( )
!J,~f.,:, ✓,,pbJ f'pm !pp~~ f'P/tl 'ppb) pprn ppb f{J,n (Pb ppm
5 I I I I l,L · ..
,o
5
,/
JO
j Trnu.cHLOROETHE?t'E 5
I
I
II
l
;y
I
I
4
I
I I
I
l 0IBR0MOCHLOR0ia:raANE I
rnnu::n DIBROMIDE
CHl-OROBENZl.:NZ:
1.l.l,2·T?:!llACHLORO?;THA.."fE
rrnn, BE:."fZZNE
==
STTJU:ITT: '\
BROMOP'OR!il iO
TRAJfS-.l.4-DICHLORO-Z..BUTENE 'lo
1,2,3-TRlCIIl.OROPROPANE 5
1,4-DICBLOROBEN'ZZN?; I
1.2-DICHLOR0BENZENE .Ji
l.2·DIBRO!d0-3-CHLOROPROPANE ,-,5
0-I
VINYL ACETATE ;;l{JQ \ I v ,(
·-
~ -Actual value is known to be lees than value given.
L -Actual value is known to be greater than value given.
U -Material was analy:zed for but not detected. The number is the Minimum ~tection Limit.
NA -Not analyzed.
1/ -Tentative identification.
'i.1 -coM110u.1JP f?.~/..IPicLY o.eTecrr:'6U= c,v.LY ;N HIG-H ccr.JCCNTRATi,oi1:.;.
✓ .. :Si1t-iPLt Hl~·HLY DiL~T(D. t~i)L'"J no hl'--71 1.J..PtL'o./.
DEENR 3068-0 (10/93)
( )
ppb ppm
.
I
PIJRGCOM.ORG
·· 1 NC·P~•ttmcnt of En"Yironment.,
-Hullh, & N&tura\
0Ruource,
Solid Wul.c M.1n.ai;cmcru Dl'Ji,ion
SAMPLE ANALYSIS REQUEST SL.Ate UbonLOry of r'Ublii: tti:.ann
P.O. Box 28.0--17, 306 N. Wilming1.0n St.
R.1.lci1:h, North Carolina :2761 l-S047
.N~------------~k!DN~=~G~·~L~-~-~O~
/
-
-
-
·
~
S
~
0
~
-
-
-
-
-
,a.meofSitc ~Ii P:1m-4, ef'o./:--1,.. Collected By __________ ~_ ID#_.,,_?-----___ _
Jt.oc..tion c{1a£v1~bAJa.& foQatcCo~wJ__._/,,,_,7 _-:_:_I /-;::-:::::7::::(p=====Ti:_:1m:::::e ======::::==-
rency: H=dous Waste Solid Waste _V_ 'Supcrfund TCLP Compounds
Sample Type
Inorganic Compounds Resu!LS(m~/1)
Environment..'11 Concrntrate Comments arsenic
I
b~um
Ground Waier (I) Solid (5) 7/o ~ AAub _ cadmRif:C""''--'-\_f"-C:-~. ·_-,~-----
(
chromium -·· ·
Surfau Water('.!) Llquid (6) -A-,y/~ ~ l"'1d --------
mcrcu,,y UN 2:_:J~i~9=9b~· ____ _
_ Soil (3) Sludge (7) c?~ . @ selenium
I-Other (4) Other (8)
Organic Chemistry
ameter Resul15 (mg/I)
.!' T:GC/MS
Acid:B/N Ext.
2,4-D
2,4,5-TP(Silvex)
chlordane
heptachlor
hcx..ach.lo ro benzene ------
hcxachloro bu t..adi enc
endflil
lindane
rnethoxychlor
to:x.aphcnc
------
FOR LAB USE ONLY
Inorganic Chemistry
Parameter Resul15(rng/l)(mg/kg)
antimony
:1.rsen.ic
barium
beryllium
cu<llTuum
chloride
chromium
cob.lt
copper
fluoride
iron
lead
manganese
mercury
nickel
nilralc:
selenium
silvc:r
!iulfutes
thallium
!iiBUPEMrut~·•...:;_,~--·--;c··,_".c• -'-'"-'------
Organlc Compounds
bca..zcne
c.ubon telrachloride
chlordane
ch1orobcnune
chloroform
o-cre:;;ol
m-cre~ol
p-cresol
cre!iol
R,:,;ult.s(mg/1).
1,4-dichlorobeo.une ______ _
1,2-dich.lorocthanc
J, 1-dichloroethylene ______ _
2,4-dichloroelbylcnc ______ _
heptachlor
bexachlorobenzcne
bexach.lorobutadiene ______ _
hexachlorocthanc
methyl e\hyl ketone
nitrobcn.zcne
pentachloropbenol
& -/.,2 -9~ /3~ I Date Received
Date Extracted le-1.3-9{, SA A6
vanadium
zinc
pH
pyridine
letruchloroc:thy kne
trich.loroclhylcne
I
I
I
,
;f)
D e Reported _ __,h~-_-Z,...:.../_-...,_t/_,6"'----
•. ,_: ·: r,>Lh.)
...._,; ;_; ._;:·L_,·JcJ
Lab Number
D11S3191 (RcviicJ l~/9J)
conductivity ______ _ 2,4,5-trichlorophenol ______ _
TDS
2,4,6-trichlaroplu::nol ______ _
t1a:sh point vinyl chloride
cnJrin
lindane
methoxychlor
toxaphene
2,4-D
2,4,5-TP (Silva)
I. NC· Dr;PatUnenl of Environment,
· -Hc.&h.n, & Nawral 'Rc.ourc:e,
Solid Wui.c Marui:cmcnl Di,.,i,ion
SAMPLE ANALYSIS REQUEST S1.a1e L,.baruory of Public: Hc:.a.lU'l
P.O. Box 280-t?, 306 N. Wilrninbwn St.
RalciJ.h, North CarolUU 11611-P.04'7
re L-U 0.2. -S · . 1 I Si1.eNumbcr _______________ Su.mplelD Number/Name --=lf) __________ v<J-='-------
NameofSiLC ~ ?0-?l--4, clC'a.&f ..-CollcctcrlBy __________ ~_ ID # _ __,g"+----
1 Sitd..nc.,.tion £!_du_' -~/2,u,~ foQat.cCollc::td
'-"' I
~uperfund
!11 -; /-9 (p Time
1 Agency: Hazardous Waste ----
Sample Type
I
I
I
I
EnvironmenL"'l.1 Concentrate
-Ground Water (1) -Solid (5)
✓ Surfac,: Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
Parameter Results (mg/I)
P&T:GC/MS
v'Acid:B/N Ext.
-2,4-D
-2,4,5-TP(Silvex)
chlordane --hcplllch.lor
hcx.achloroben.zene -hcxachlorobutadic::nc:: -endrin -!indane --methoxych.lor
-toxaphcne
----
FOR LAil USE ONLY
Date Received &1-V-'1k ,8.1/J
Date Extractcrl &-13'-Q(, SA N3
Date Analyz:d (o-/7-'1/e 13[)
Reportcrl By
Date Reported
I
I
I
I
I
I
I
I
I
I
I
Lab Number ·, .l. ~ , ; r'i C"
...... '1....>~.....:•.,.1..._,9
DHS 3191 (Rcvi~cJ l~/93)
Solid W a.st.c TCLP Compounds
lno~anic Compow,ds Results(mg/1)
Comments arsenic -barium -cadmium -chromium -!C>1d --mercury
sdcn.ium -!iilvcr ----
Inorganic Chemistry -
Parameter Results (m g/1 )(mg/kg) Organic Com pow,d.s Results(mg/1)
antimony bcnunc
--
arsenic carbon tetrachloride --
barium chlordJ.ne --
-beryllium -chlorobcnzen:!
cadmium chloroform --
chloride o-cn:sol --
chromium m-crcsol --
cobalt p-crc::sol --
copper crcsol --
fluorido 1,4-dich.lorobclll.One
--
iron 1,2-dichloroc:thane --
-lead l, 1-dichloroethylcne -
nun g an c!Se 2, 4-dichl oroc::thy !enc '
--
-mercury -hcptachJor
nickel hexachlorobenune ' --
nitrate boxachlorobutadicno --
sc::lc:nium hc::xachlorocthane --
-silvcr methyl e\hyl ke10ne -
:.ulf,ues ni1robcnunc --
thallium penlllch.lorophenol --
vanadium pyridine --
-zrnc tel rac h.i ore ct h y lcnc -
-pH -lrichloroc::lhylcnc
-conductivicy -2 ,4 ,5-trichlorophenol
-TDS 2,4 ,6-trichlorophonol -
-fla,h point -vinyl chloride . cmlrin --lindano --
--mcthoxychlor
--toxaphcnc
--2,4-D
--2,4,5-TP (Silvex)
I
I
I
I
I
I
I
I· NC·DC9artmcnt of Environment,
Huhn, & Naruul ·Rc.ourcc,
Solid Wut.c. Man.a~cmcru Divi,ion
SAMPLE A.NALYSIS REQUEST S~lc. Laboruory of Public Hu.Ith
P.O. Box 28047, 306 N. Wilmini:t.on St.
R.alcii;h, North Carolina 27611-&047
1Si1.cNumbcr _____________ Su.mple!DNumber/Nu.me U) (_ -QO 3 -$W
Name of Site ~ ?0::zt,4.. ~a/-! --Collected By __________ -'-_ ID#_,_)__,_<-/ ___ _
titel.ocstion £!._dv__. ~/;,u.~ ,/4,QateCol!ecte-d :.9 <:............: I ✓Supcrfund
'geney: Ha.u.rdous Waste Solid Waste TCLP Compounds
----
Sample Type Inorganic CompoWlds Results(mg/1)
Time
EnvironmenL1l Concentrate Comments -arseruc
I_ Ground Water(!)
-barium
Solid (5) -cadmium
--•✓ Surface Water (2)
-chromium
Liquid (6) -l""d --mercury
-Soil (3) -Sludge(:)) -::;clcn.ium
I-
!iilva -
Other (4) -Other (8) ---
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Res u!LS (mg/I )(mg /kg) Organic CompoWld.s Rt.::iullS(mg/1)
P&T:GC/MS anlimony bc:n.z.enc
v'Acid:B/N Ext. ---
urs~n.ic carbon tetrachloride --
-2,4-D barium chlord.one ---
-2, 4, 5-TP(Sil vex) --beryllium -ch.lorobcnzcnc
chlordnnc: cudm.ium chloroform
---
-beptachJor --chloride -o•crc:.-ol
hc:x.ach1orobell.Une chromium m-crc!iol
---
-hcxachloro but.ad iene cobalt p-cresol ---
-cndrin , copper cre!iol --
-lintlane fluoride 1,4-dichJoroben.zene ---
-mc:lhoxychlor --iron l ,2•dich1oroethane -
-tox.aphc:nc --lead I, 1-dichJoroethylene -
---rrunganesc -2, 4-d ichloroeth y lene
---mercury -heptachJor
-nickel hexachJoroben.zene ---
nitrate hexachJorobu1adiene
----
selenium hcxachloroethanc ---
--silver methyl e!hyl ketone -
FOR LAil USE ONLY sulfutes · nitrobcn.z.ene ---
--thallium penl.llchlorophcnol -
&-tJ:-it .tJiO Date Received I vanadium pyridine· ---
--z.inc 1e1ruchJoroe1hy!cne
Date Extracted
-
/p-ls-g,, SA
I
I
I
I
' NS
Date Analyz.erl &-17-9&, 6fJ
Reported By
Date Roported
Lab Number
'. ,, '• 00 -.J (.i0..i., '
DIis 3191 (Rc:vi.wl I:!/93)
-----------------
--
pH -trichloroethylc::oe
conductivity -2 ,4 ,5-trichJorophenol
TDS 2,4 ,6-trichlorojJl1c::nol -
l11ish point -vinyl chloride . cndrin -!indune --methoxychlor
-toxaphene
-2,4-D
-2,4,5-TP (Silvex)
NC D~1.nmcnt of Environment,
Huhn, &. N1.ruul R.~urcc,
Solid Wu1.c M1.na~cmcn1 Divi,ion
SAMPLE ANALYSIS REQUEST SL&Lc Liborawry of Public Hc.&lth
P.O. Box 28047, 306 N. Wilmin~ton :s1.
R1.lci1;h, Nonh C1.rolina :?.7611-S047
I Site Number _____________ Samplc!D Number/Name U, L -001/--S lJ
Nawcof Site ~h D-1a'1A-or'o,,/-1,.. Collected By __________ ~_ ID #-,,,.c,2=->-O"'---
I SitcLoc.1tion 6< c,£v._, -~/;,u ~ ;l{! . .Date Collected Time
CJ., I ✓Superfund
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Agency: Hazardous W a.ste ----
Sample Type
Environment..'\! Concentryte
-Grouod Water (1) --Solid (5)
JL Surface Water (2) --Liquid (6)
-Soil (3) --Sludge (7)
-Other (4) --Other (8)
Organic Chemistry
Parameter Results (mg/!}
~&T:GC/MS
_ Ac,d:B/N Ext.
-2,4-D
-2, 4, 5-TP(Silvcx)
chlordane --hcpU1ch1or
hc:xachlarobenz.ene -hexachlorobutadiene -endrin -lindanc -
-methaxychlor
-taxa.phcnc
----
FOR LAB USE ONL V
Date Received b -1 ,,2-cz~ 4J.!J
Date Extracted l2-1.s-q1, 48 SA ,
Date Analyzed &-J7-9&/3iJ
Reported By
Date Reported
Lab Number Ji)J101
OHS j 191 (Rcviicd l~/93)
Solid Waste TCLP Compounds I
Inorganic Compow,d.s Result.s(~g/1)
Comments arsenic -barium -cadmium -chromium -lo:1d --mercury :
selenium -~il ver -
-
--
Inorganic Chemistry -
'
Parameter Result.s(mg/l)(mg/kg) Organic Compow,d.s Rcsult.s(mg/1)
antimony bcn:unc ---
Hrseruc cll.Ibon tetraChloride
---
barium chlordAne ---
--beryllium -ch.Jorobcnz.cne
cu<lmium ch.Joroform :
--
ch.loric..lc o-cresol ---
chromium m-cre.sol ---
cobalt p-creso! --
copper ere.sol --
fluoride I ,4-dichlorobcnunc ---
iron 1,2-dich.lorocthane
---
lead 1, 1-dichlorocthylcnc ---
-m:..i.nganl!Se -2, 4-dichloracthylcnc
--mercury -hept.achlor
nickel hcx.achlorobcn.zene '
---
nitralc bc:xachlorobuta<lienc ---
selenium hc:x.achloroc::thane ---
--silver methyl c!hyl ketone -
.sulfates JU t ro bc:nune --
--thallium pcnt.achlarophcnal --
vanadium pyridine --
--:z.inc tetrachloroethylene -
--pH -trichloroethylc::nc
--conductivity -2 ,4 ,5-trichlorophenol
--TOS 2,4,6-trichlorophenol -
--11,..,h point -vinyl chloride . cnc..lrin '
---lindllne ---
---mcthoxychlor
---toxaphcne
----2,4-D
---2,4 ,5-TP (Sil vex)
.
I NC D~art1n£n.1 of Environment,
Hc.ahn, &. Naruul R~urcc,
Solid Wu1.c M•n.a•cmcru Divi,ion
SMil'LE ANALYSIS REQUEST SL.ate Labou.LO,:y of Public Hc:.a.llh
P.O. Box 280-n, 306 N. Wilmiri;;ton St.
Ra.lci;;h, North Carolina 27~11-8047
I Site Number SampldD Number/Name VJ L. -0 0 S" -S u...J
Name of Siu: ~ ('.u:1,:714 ci(°oAJ ... C,,lle::tw By _________ ~_ ID# ;;L. (.c
rf! ~--,I.__ 1/; _.J a.,h ;{.(~.Date Co lle::Le<l I Sit.eLocsrjon '--" I ✓Superfund
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ll
Agency: Hazardous Was Le ----
Sample Type
Envirorunent..11 Concentrate
_ Ground Water (I) Solid (5) -J Surf= Water (2) Liquid (6) -
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
Parameter Results (mg/I)
P&T:GC/MS
VAcid:BIN Ext.
-2,4-D
-2,4 ,5-TP(Silvex)
chlordane --heptuchlor
hcxachloroben.z.ene -hcxachJorobut.adicnc -cndri.c -lindane --methaxychlor
-toxaphcnc
----
FOR LAB USE ONLY
Date Re<:eived IP -/,). -'lt,, t6 LO
Date Extracted lii-13-Q(, SI-\ /\6 '
Date Analyzed {p -J / -f {,, 13;{)
Reportw Ily
Da[e Reponed
L,,.b Number ' ·:·1 ")? ·,• ;-:, , ~ ·1 ~
D11S 3191 (Rcvisr;:J l~/93)
Solid Waste
Comments
Inorgaruc Chemistry
Parameter Results (mg/I) (mg/kg)
-antimony
urscnic -barium --beryllium
cu<lm.ium -chloritlc -chromium -i:obalt -
-copper
fluoride -iron -kad -
-nun gancsc
-mercury
nickel -niLratc -selenium -silver -.sulfulcs -thallium · -vanadium -:zjnc --pH
-conductivity
TDS --flu.sh point . ------
Time
TCLP Compounds
lno~anic Compow1ds Resulls(mg/1)
arsenic -barium -cadmium -chromium -lood --mercury
sclcn.ium -!iilvcr -
-' ---
Organic Compounds Rcsulls(mg/1)
bcnunc -carbon tetrachloridc -chlordane -chJorobcnzcnc -chloroform -o-crc.::;ol -m-crc:.::;ol --p.-crcsol
Cn:sol -1,4-dichlorobc=ne -l ,2-dichloroc:.th.a.nc --1, 1-dichloroethylcne
-2, 4-d ichl a roelh y !enc
-hcpt.ach.lor
hexachlorobcn.zcnc -hex,chlorobutudiene -hcxachloroclha.nc -
-methyl ethyl ketone
nitrobcruenc --pcnt..achloropbcnol
-pyridine
-tetruch!orocthylcne
-trichlorocthylenc
-2,4,5-trichJorophcnol
-2,4,6-trichlorophcnol
-vinyl chloride
cndrin -lindiine --me[hoxychlor
-loxaphcne
-2,4-D
-2,4,5-TP (Silvcx)
I NC' DC3>•~nt of E:1vironmeru,
Hu.Ith, & Natural Re.aurce1
Solid Wul.c: Man.a~cmcru Oivi,ion
SAMPLE ANALYSIS REQUEST SL&~ LaboraLOry of Public He.11th
P.O. Box 28041, 306 N. Wilmini:ton St.
R..s.lciJ;h, Nonh Carolin.a. 17611-8047
I Siu:Numbcr ______________ S=plc!D Number/Name _.,,C,<....L_,,L,::__,l:_::v:...,,~)::...-___,5::::...clJ=:::...... ____ _
NameofSiu: ~/i~o{'a/41,.. Collcctc<lBy _________ ~_ID# , :Z,J---
1 Siu:Loc,itioo £) a1.v..· ~/;,,urih foQau:Collcctd '--"' I ✓Suporfund
I
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Agency: --HaZArdous Wasu: --
Sample Type
EnvironmenL'll Concentrate
-Ground Water (1) -Solid (5)
✓ Surfw: Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
-Other (4) -Other (8)
Organic Chemistry
Parameter Results (mg/I)
~&T:GCIMS
_ Ac,d:B/N Ext.
-2,4-D
-2,4,5-TP(Silvex)
chlordane -
-bepwch!or
hexach1orobenunc -hexachlorobuLadiene -c:ndri.n -!indane -
-methoxych!or
-toxaphcnc
----
FOR LAB USE ONLY
Date Received &? -/4). -9 t,,64)
Date Extractc<l u-i'-/-9,i.., f5.te,,{Jt'>
Date Analywl &-11-90 sfJ
Reportc<l By
Date Reported
ub Number ','"·'"3 ::;0 0.JLV
DHS 3191 (Rcvi~cJ l~/9J)
Solid Wasu:
Comments
lnorgan.ic Chemistry
Parameter Results(mg/l)(mg/kg)
-anlimony
arsenic -barium --beryllium
cadmium -ch..loride -chromium -cobalt --copper
fluoride -iron -lead --man g an cse
-mercury
nickel -nitrate -sdc:nium -· silver -sulfutcs -thallium -vanadium , -z.inc --pH
-conductivicy
TDS --1111,h point . ------
Time
TCLP Compounds
lno~aruc Compowuls Results(mg/1)
arsenic -
·. -barium
cadmium -chroilllum -lead --mercury
sc:len.ium -:i:ilvcr -
-' --
-
Organic Compounds Resulls(mg/1)
bc:nunc -ca.rbon tetrachloridt! -chlordane -chJorobcn.z.cn<! -chloroform -o-cresol -m-cn:sol -
-p-<:resol
crc:;;ol -
-1,4-dich!orobenune
-l ,2-dichloroethane
-l, I-dichloroethylene
-2, 4-d i ch! oroetb y !enc
-heptachlor
hcx.achlorobcnzcne -hexachlorobutadiene -hcxachloroclb.lile -
-methyl e!hyl ketone
n.itroberuene -
-penl.!l.chlorophenol
-pyridine
-tetrachloroethylene
-trichloroethy lcne
-2,4 ,5-trichlorophenol
-2,4 ,6-trichloroplu:nol
-vinyl chloride
enc.Jrin -lindane --mcthoxychlor
-toxaphene
-'.2,4-D
-2,4,5-TP (Silvex)
I NC Dep•~nt of ~vironmcnt,
H""llll, &:. Nacuul Ruoun:c,
Solid Wut.c: Man.ai;c:mcru. Di'ili,ion
SAMPLE ANALYSIS REQUEST S1.1.1e l.aboraLOry of Public Hc.1.lr.h
P.O. Bax 28047, 306 N. Wilmin1:t.0n St.
Ralc:ibl'l, North Carolin.. 27611·8047
I Site Number _____________ Su.mpldD Numbcr/N=c _G~'--'L=-_-_o_o__,,_;_-__,_P__,u.J"-'=''-----
NameofSite ~A~of'a./;J .... Col!octedBy _________ ~_JD# ___] 'g
I Sitel.oc,tion £!..aiv._' -~/;,U~ /UQateCo!le.:tcd /,1 -1 I -9 l.,o Time
I
w-I ✓Superfund Agency: H=dous WASte Solid Waste TCLP Compounds ----
Sample Type lnori:w.ic Compow,d.s Results(mg/1)
I Environment:11 Concentrate Comments arsenic -
I -barium
~ Ground Water (1) Solid (5) cadmium ---chromium -
I Surface Water (2) Liquid (6) -lCJ1d ---mercury
-Soil (3) Sludge (7) -selenium --
I
~ilvc:r -
-Other (4) -Other (8) --
I -
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Compow,d.s Results(mg/1)
I ~&T:GC/MS antimony bc:!n.une ---
_ Ac,d:B/N Ext. 11.rsc:n.ic -carbon tetrachloride --
-2,4-D barium chlordane ---
I -2,4,5-TP(Silvex) --beryllium -chlorobcn.z.cnc:
-chlordo.nc cu<lmium chloroform --
-bcpuchlor ch.lori<lc: o•crc:~ol --
I -hc:xachloroberu.ene chromium m-cn:.sol --
-hexachlorobutadienc cobalt p-cresol --
-cndrin copper cresol --
lindane fluoride 1,4-dichlorobenune ----
I -methoxychJor --iron 1,2-dichJ,\roethanc -
--toxaphenc lead l, 1-dichlorocthylcne ---
--rrunganese -:2, 4-di chl oroethy !enc
I ---mercury -hcpt.ichJor
-nickel hcx.ach.lorobcnzcnc --nitrale hexachlorobutadiene ----
I
selenium hexachloroctha.nc ---
silver methyl e;hyl ketone ---
FOR LAB USE ONLY sulfutc::.s nitrobc:nz.t:ne ---
I (p -/;L-~& 6<0 -thallium pent..achlorophenol
Date Received -vanadium pyridine --:z.inc tetruch.loroethy l enc
Date Extracted &,-H-9(, SA ---
' M --pH -trichlorocthylenc
I u -;fJj[; 13,,[) --conductiviry -2,4,5-trichlorophenol
Date Analyzed -TDS 2,4,6-trichloroplienol -
--1111.!>h point -vinyl chloride
I
Reported By . cndri.n ---lindane
Date Reported ---methoxychJor ---
I ',· ;104 --Loxaphcne
Lab Number ....].j...._J' -
---2,4-D
---2,4,5-TP (Silvcx)
DHS 3191 (Reviled l~/93)
I NC Ocyuu~1ent of E:ivironmcnt,
Huhn, &. NaOJral Rc.wurcc:,
Solid Wutc Mana1:c:mcru. Divi,ion
SAMPLE A.NALYSIS REQUEST St.ale Uborat.ary of Public Health
P.O. Box 28047, 306 N. Wilm.ini;LOn St.
R,licibh, North Carolina 27611-8047
I SiteNwnber --------------Sample ID Number/Name --~=-L=_-_____coc......:o::_.2 __ ---'-f.....::w-=-----
Nameof Site ~ ~ ~aA-1--Co!l.:.ct<!dBy __________ ~_lD# __ 3/_,_'--/ __ _
I Siteloc,tioa ,{) a1v..· -~/;,Ur~ foQateColl.:.ctGd '--'"' 7 ✓Superfund
I Agency: Hazardous Waste ----
Sample Type
Environment'\} Concentrate
I / Ground Water (I) Solid (5) -
1-Surface Water (2) -Liquid (6)
-Soil (3) -Sludge (7)
1-Other (4) -Other (8)
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Organic Chemistry
Parameter Results (mg/I)
~&T:GC/MS
_ Ac,d:B/N Ext.
-2,4-D
-2,4,5-TP(Silvex)
chlordane --hcplJlch]or
hcx.ach] ore ben.z.ene -hcxach.1oro bu ta.di enc -c:ndrin -lindane
-mcthoxycWor
-toxaphcne
-
-
--
FOR LAil USE ONLY
Date Received te -o-94442
Date Extracted lr:H:91, 3A 46
Date Analyz:<l (p-;i'-9& f3))
Report<!d By
Date Repon<!d
Lab Number .S-SJ10S
OHS J19J (Rcvi~cJ l~/9J)
Solid Waste
Comments
Inorganic Chemistry
Parameter Results(mg/1) (mg/kg)
-antimony
llrsenic -barium --beryllium
cadmium -chloride -chromium -cobalt --copper
fluoride -iron -lead --nunganc:.se
-mercury
nickel -nitrate: -selenium -silver -sulfates -thallium -vanadium -z.inc --pH
-conductiviry
TDS --flu.sh point . ------
Time
TCLP Compounds
lnori!aniC Compowuls Results(mg/1)
arsenic -barium -cadmium -chromium -lead --mercury
selenium -silver -----
Organic Compow,ds Rcsults(mg/1)
bc=nunc -carbon tetrachloride: -chlordane -chlorobcn.z.ene -chloroform -o-crc:ml -m-cn:sol --p+eresol
crc:~ol -1,4-dichlorobenune -l ,2•dicWorocthan~ --1, 1-dichlorocthylcne
-2, 4·d i chi o roe thy lc:nc:
-heptacWor
hcxachlorobenu:ne -bexachlorobut.adient -hc:xachloroc:thJ.I1c -
-methyl eµiyl ketone
nitrobenune --pent.uchlorophc:nol
-pyridine:
-tetrach.loroethy Jene
-trichloroc:thy lc:ne
-2 ,4 ,5-trichlorophenol
-2,4 ,6·trichlorophenol
-vinyl chloride
endrin -linr.Iane --methoxychlor
-loxaphcnc
-2,4-D
-2,4,5-TP (Silvcx)
·· 1· NC Dc:p.a.rtn:J.£nl of E-:vironmcru,
Hc.alUl., &:. Nawul Rc.ourcc:,
Solid WuLc Matui;c:mc:01 Oivi,ion
SAMPLE ANALYSIS REQUEST Sl&le Ubora1.0ry of Public Hc.atUl ~
P.O. Box 28047, 306 N. Wilmin1,1.0n St.
R.1.h::i~h, North Carolina '.!7611-8047
lite Number _____________ Su.mp!e!D Numbcr/Niilllc __;U)~· .::;L::.__-----:0:::;_;0:::...,3,:e_-~j>'--:::.W.= ____ _
Na.me of Site ~ ~ ef'O-;l!J,.. Calloctod By __________ ~_ JD # __ 3/:.;-'f-1---
litel..oc.,uon tf< ~· ~/;.J~ faQateColloclod
'-"' I ✓Supcrfund
fgency: Haz.ardous Waste Solid Waste TCLP Compounds
----
Sample Type
Inorganic Compow1d.s Re,;ult,(mg/1)
Time
Environment.,! Concentrate Comments -arseruc
V Ground Water (1)
-barium
Solid (5) -cadmium
-chromium -
I--Surface Water (2) Liquid (6) -lead
--roc::rcury
-Soil (3) -Sludge (7) -:,elc:n.iuro
I-
~il \/Cf -
Oilier (4) -Other (8) --
I
-
Organic Chemistry Inorganic Chemistry -..
Parameter Results (mg/I) Parameter Results(mg/l)(mg/kg) Organic Com pounds R<!:iult.,(mg/1)"
,~T:GC/MS
antimony bco.z.enc
--
_ Ac,d:B/N Ext. llrsenic -carbon tetrachloride
-
-2,4-D -barium -chlordane
IJ= 2,4,5-TP(Silvex) -beryllium -ch.lorobcnzcne
chlordane cudm.ium chloroform
--
hepWlcWor chloride o-cn::i:ol
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-hcxachloroberu.ene -hcxach.lorobutadienc -c:ldrin -lint.lane --mcthoxychlor
-toxaphenc
----
FOR LAB USE ONLY
Date Received fe -/cJ--9k cl&
Date Extracted /a-l':J-9(p SA,/¥)·
Date Analyzed t~ -1 f-CJt afJ
Rcportod By
Date Reported
Lab Number '·:: : .. 06 -~ t..,.._,..i,.
DHS J19l (Reviled 11/?J)
-
-----·-
---------------------
-
chromium m-crcsol -
cobalt p-cresol -
copper CfCtiOl -
fluoridc -1,4-dichlorobenune
iron -1,2•-dich.lorodhane
lead I, 1-dicWoroethy!ene -
nunganese -2, 4-dichloroethylene
mercury -heptachlor
nickel hcx..ac hloro bcn.:z..ene -
nitrnlc hexachlorobuta<liene ' -
selenium hexachlorocthanc -
silver methyl e,hyl ketone -
sulfates nitroberucne -
thallium penlJlchlorophenol -
vanadium pyridine -
:z.inc tctruchloroethylcne -
pH -trich.loroethy 1cnc
conductiviry -2, 4, 5-trichlorophenol
TDS 2,4, 6-trichlorophcnol -
lltLSh point -vinyl chloride . cndrin -liniline --methoxychlor
-toxaphene
-2,4-D
-2,4,5-TP (Silvex)
I NC Oqt,nn;cn.t of ~vironmcnt,
Hc.ah.n, &. Natural Rc.wurcc,
Solid Wuic },-hru.i;cmcru. Dl\li,ion
SAMJ'LE ANALYSIS REQUEST Su.le Labor1.L0ry of Public Hc:.1.lth
P.O. Box 2!0-r7, 306 N. Wilmini;ton St.
R..lcii;h, North Carolin.a 17611-!0'17
I SiLeNumbcr ____________ Sample ID Number/Name CJ L -0 D </ -I'° t,{J
Name of Site ~Ii~ o{'a/;I e Collect<rl By ________ ~_ ID# 1/: 7
lsitel.nc:.,.tion ~-~/;,u,~ ;{,•QaieCollecLed Time
~ I ~upafund
.Agency: Hazardous W a.sLe Solid Wa.sLe TCLP Compounds
----
Sample Type lnorgaruc Compowids ResullS(mg/1)
Environment.'ll Concentrate Comments -arsenlc
I / Ground Water (1)
barium ·-
Solid (5) cadmium
---chromium -
1-Surface Water (2) Liquid (6) -le,,d
--mercury
Soil (3) Sludge (7) -:::clc1Uum
---
1-
!iilvcr -
Other (4) Other (8) ---
I
-
Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Para.meter Result.s(mg/l)(mg/kg) Organic Compowids Rc,;ullS(mg/1)
I ~&T:GC/MS antimony bcn.unc ---
_ Ac,d:B/N Ext. 11.rse:ruc carbon tetrachloridG
---
-2,4-D barium chlordJl.ne ---
I -2,4,5-TP(Silvex) --beryllium -chlorobcn.z.::nc
-chlordane cadmium chloroform --
beptachlor ch.loricJc o-crc!iol
----
hcxach1oro bcn.z.c:ne chromium m-crc:ml
-I ---
-hcxachlorobut..adicne cobalt p-crcsol ---
cndri.n copper crc!:iOl
---
-!ind.we fluoride 1,4-dichlorobcnune ---
I -methoxychlor --iron 1,2-dichloroc:thane -
-toxaphcnc lc:id I, 1-dichlorocthylene ---
---nu.nganc.sc -2, 4-d ichl oroc:lh ylenc
I ---mercury -hcp~chlor
-nickel bexachloroben:z.cne ---
---nitrate bexachlorobut.a<liene -
I
selenium hcxachloroethanc ---
--silver methyl e~yl ketone -
FOR LAil USE ONLY sulfates n.itrobcn.zcnc ---
I & lc,l-'J tt44J thallium pcntachlorophcnol ---
Date Received vanadium pyridine ---
--zinc tetracitlorocthylcne
12·/<-J-91, SA iY;,
-
Date Extracted pH trich1orocthylcne ---
I & -/ f-9.? 13d) --conductivity -2,4 ,5-trichlorophenol
Date Analyzed -TDS 2,4 ,6-trichlorophcnol -
--1111.:.h point -vinyl chloride
Report<rl By
. cmlrin ---
I --lind=e
Date Reponc:d
-
--methoxychlor -
I
• . .' ·:: ~ -1 -J'-, --toxaphcne
Lab Number
-
...._; UV ..i,.. • ( 2,4-D ---
---2,4,5-TP (Silvex)
OHS '..1191 (Ri:viu:d l~/9:J)
I }-/C 0"9&rt.r~n.1 of ~vironmcru,
Hc.allil, & Narural Ruourcc,
Solid Wut.c Maiu~cmc:ru Di'i'i,ion
SAMPLE ANALYSIS REQUEST SL.ale Labor.uory of Public Hc.&lth
P.O. Box 28047, 306 N. Wilmington St.
R.alc:ii;h, North C1.rolina 276,l l -8047
I SiteNumber _~ ___________ Sumplc!D Number/Na.me _..::UJ'-'-_L __ o_·_o=---=~'----f>:..._vO=--==-----
Nameof Site ~~~a.Al--Collected By __________ ~_ID # __ 5-<--1/'----
1 Sitd.oc.1tion If! cd,v_. -~/;,ua__h /UQat<:Collc::tcd '--'-I ✓Superfund
I Agency: Hazardous W a.ste --Solid Waste TCLP Compounds· --
Sample Type Inorganic Compow1ds Results(mg/l)
Envirorunent.'ll Concrntr.ite Comments arsenic -
Time
I ./ Ground Waler (!)
barium -
Solid (5) cadmium ---chromium -
I Surface Water (2) Liquid (6) l""d -----mercury
Soil (3) Sludge (7) sdca.ium I ----~ilvcr
I -
-Other (4) -Other (8) -
--I OrgJnic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Results(mg/!)(mg/kg) Organic Compolillds Results(mg/1)
I ~&T:GC/MS anlimony · bc:n.u:nc --
_ Acid:B/N Ext. arsc:n.ic carbon tetrachloride! --
-2,4-D -barium -chlordAne
I -2,4 ,5· TP(Sil vex) --beryllium -chlorobc:cu.cnc
-chlordn.ne cadmium chloroform --
-heplllchJor --chloride -o•crc~ol
hcxacWo ro beD.1.ene chromium m-crc.sol -I --
-hcxachJorobuta:dicnc cobwl p-cresol --
-cndrin copper crc.sol --
!ind;uie fluoride 1,4-dichlorobenuoc ---
I -methoxychlor --iron 1,2-dichloroethanc --tox.:iphcnc -lead 1, 1-dicWorocthylcnc -
--nungancsc -2, 4-di chl a rocth y !enc
I --mercury -hcptachlor
-nickel hcx.ac hl o rob cn.z.cne --nitrate h cxachl o rob u tad i enc ----
selcnium hcxachloroethane
I -----silver methyl e;hyl ketone -
FOR LAil USE ONLY sulfates n.itrnbcnu:ne ---
u -/ ,,2 -2f .6'dJ -thallium penr..achlorophcnol
Dale Received -
I vanadium pyridine --
lo-19-9t:? tJLJ -zjnc tctrachlorocthylcne
Date Extracted -
-pH -trichlorocthylcnc
I --conductivity -2 ,4 ,5-lrichJorophenol
Date Analywl -TDS 2,4 ,6-trichlorophcno\ ---flu,h point -vinyl chloride
Reported By . cn<lri.n ---
I ---lindanc
Dale Reported --melhoxychlor -
\. ·:··. > .1 ...... 3 toxaphene
Lab Number
,...;G,.J,-11.,J{ ---
I ---2,4-D
---2,4,5-TP (Silvex)
DHS 3191 (Ri:viicJ l"l/?3)
I
I ?ic Oq:!ann;cru of Environment,
Hu!Ul., &. Nawul Rc.ourccs
Solid Wa1.1c. Manai;cmcru Oi'v'i,ion
SAMPLE ANALYSIS REQUEST St.&le Labora1.0ry of Public Hcallh
P.O. Box 28047, 306 N. Wilm.inl,!toO. St.
R1.lcii:h, North Caroli.n.a 27611-R047
ool:,-A-1 I Sil<:Numbcr _______________ Su.mplclDNumber/N.me (,,,{./
NameofSil<: ~fi~ef'a/-1.-Coll~tcrlBy __________ ~_lD# 5</
I Siu::Locatioa £> d,v_' ~/;,J a._h /L(:__nateColl~wl
CJ-I ✓Superfuod
Agency: Hauu-dous Wa.sl<:
I ----
Sample Type
Environment:\! Concentr.>te
I /Ground Water (I) --Solid (5)
1-Surface Water (:?) Llquid (6) -
Soil (3) Sludge (7) --
I-Other (4) -Other (8)
I
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Organic Chemistry
Parameter Results (mg/I)
~T:GC/MS
_ Acid:B/N Ext.
-2,4-D
-2,4,5-TP(Silvex)
chlordane -
-bepuichJor
hexachlorobenune -hex.achlorobutad i enc: -endri.n -lin<lane --mdhoxych.lor
-loxaphene
--
-
-
FOR LAB USE ONLY
Date Received {p -;,;J..-9&/Ji{)
Date Extracted le-/9-9~ 6,0
Date Analyzed
Reportcrl By
Date Reported
Lab Number '. -'1 D9 ~J· (,.....:, ,A,. -
DHS 319] (Rcvi~cJ l~/9J)
Solid Waste
Comments
Inorgan.ic Chemistry
Parameter Results(mg/l)(mg/kg)
--antimony
11.rscn.ic -barium --beryllium
cuc.lmium -chloriUc -chromium -cobalt --copper
fluoride -iron -lea<l --nunganl!Sc::
--mercury
nickel -nitrate -sdcnjurn --silver -sulfates -thallium -vanadium -:z.inc ---pH
-conductivity
TDS --flu~h point . --------
Time
TCLP Compounds
'
Inorganic Compow,d,; Results(mg/1)
arsenic -barium ··-cadmium -chromium -lcod --mercury
selenium -!:iilver -----.·•
Organic Compow,ds Results(mg/1)
bcnune -carbon lelrachloridc -chlordane
.
-ch.lorobcnu:ne -chloroform -o-crc::;ol -m-crc!iol --p-crcsol
crc:::i-ol --1,4-dich.loroben.u:::ie
-1,2-dich.loroetham:.
-I, 1-dichloroethylcne
-2, 4-d ichl a roe thy lc:ne
-hcptachlor
hexachlorobcn:z.:nc -hcxachlorobut.ndienc: --hc:x·achloroetqanc:
-methyl e\hyl ketone
nitrobcnz.cnc: --pc:nt.uchlorophenol
-pyridine
-letrnchloroc:thylenc
-lrichloroc:thylc:nc:
-2, 4, 5-trichlorophenol
-2, 4, 6-trichl o rophcno I
-vinyl chloride:
c:ndrin -lin<lane -
-methoxychlor
-toxaphcne
-2,4-D
-2,4,5-TP (Silvcx)
SAJv!PLE A.1'/ALYSIS REQUEST 51.&le Laboruory of Public Hc.allh
P.O. Box 28047, 306 N. Wilmi~,:1.0n St.
R1.lcii;h, Nonh Carolina 27611-8047
I SiieNumber ______________ Sumplc!D Numbcr/Numc --'a~·-L __ -_o_..;;0'-'7_-_,_/?___,w==--------
Nameof Site ~ 0'.'.f::rt-:4 q°aAJ,.. Olllcctod By _________ ----'-_ ID #_,-~<C..---1.7:....___
I SitcLoc,tion ti? a1v._· ~/vr:th faDa1eCollcctcd Time
'-"' I
~upcrfund Aiency: H a.z.ard o us W a.s ie Solid Waste TCLP Compounds '
I ----
Sample Type lno~anic Compowids Result.;(mg/1)
EnvironmenL1J Concentr:i te Comments arseruc -
I ✓ Ground Water (1)
·-barium
Solid (5) cadmium ---chromium -
1-Surface Water (2) Liquid (6) l""d ---mercury
Soil (3) Sludge (7) selenium
----sil vcr
I--
Other (4) Other (8) ----
I I Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Parameter Re:sults(mg/l)(mg/kg) Organic Compowids Rcsult.;(mg/1)
I ~T:GC/MS anlimony bcnunc --
_ Ac,d:B/N Ext. 11.rsenic carbon tetrachloride: --
-2,4-D -barium chlord=e -
11= 2,4 ,5-TP(Silvex) -beryllium chlorobcnz.:::nc -
chlordane cud mi um chloroform --
bcpt..achlor cWori<lc o-crc:iol --
h c x.achJ o ro ben:z.en e chromium m-crc::!iol ---
I -hcxa.ch.!orobuLadienc cobalt p-crcso\ --
-endrin copper crcsol --
-lind.1.ne fluoride 1,4-dichlorobenz.::ne --
I -mcthoxychlor --iron 1,2-dicWoroethanc: -
-toxaphc:ne lead 1, 1-dichlorocthylcne --
--rIUn g ant!Se -2, 4-d ichloroeth y Jene
I ---mercury -hcptachlor
--nickd hexachlorobcnunc: -
nitrate hexach.loro buta<liene ---sdc:nium hcxacb.loroethane
1 ·
--
-silver methyl e;hyl ketone -
FOR LAB USE ONLY --:.:ulfulcs nitrobcn.z.enc -
(p -o-rt-&0 -thallium pcnt..ach1orophcnol -
1 Date Rccei ved -vanadium pyridine -
&-Jf-7(,, &.Q -z..inc tetrachloroethylene -
Date Extracted pH trichloroct~ylenc ---
I Date Analywl
-conductiviry -2,4 ,5-trichlorophenol
-TDS 2,4 ,6-trichlorophenol -
--fla!ih point -vinyl chloride
Reported By . c:ndrin ---I Date Reported
---lind.1.nc
---mcthoxychlor
I
';,.: '1 10 ---toxaphcnc
Lab Number ,,...;0 ........... 2,4-D --
---2,4,5-TP (Si!vcx)
DHS 3191 (Revi:.cJ l'.:1./93)
I
i Nl.:' D~aruncnt of Environment,
Hultn, &. N•Wral R~urcc,
Solid W•1k M.an.ai;cmcru Divi,ion
SAMPLE ANALYSIS REQUEST SL&Lc Laborai.ory of Public Hulth
P.O. Box 28047, 306 N. Wilmin;:1.0n St.
R1.lci.1,:h, Nonh Carolina 276J J .a047
I Site Number ______________ Su.mple!D Number/Name __ G_c...c_~cc..__-_o __ o--=~"----P __ v..J _____ _
Name of Site ~ ?0::zt,.,:?-ef'ci.A-1---Oill.:cte<l By _________ ~_ ID #_-'luca<......,;O~· -
I Sitel.oc,.tion ,{) afv__' -~/;,u,u0 ;t(!_naizColl.:ctcd CJ-I ✓Supcrfund
I Agency; Hazardous W a.ste --Solid Wa.siz TCLP Compounds --
Sample Type Inorganic CompowHI, Results(mg/1)
Time
EnvironmenL11 Conc:rntrate Comments -arsenic
I J Ground Water(!)
·-barium
Solid (5) -cadmium -chromium -I-Surface Water (2) Liquid (6) -le.ad --mercury
Soil (3) Sludge (7) -::;elca.ium
--
1--~ilvcr
Other (4) Other (8) ---
I -
Organic Chemistry lnorgan.ic Chemistry -..
Parameter Results (mg/I) Parameter Results(mg/1) (mg/kg) Organ.ic Compolillds Results(mg/1)
I l'&T:GC/MS antimony -bcn.u:nc
~Acid:B/N Ext.
--
J:ifSCIUC -carbon tetrachloride --
-1,4-D barium -chlorwme --
I -2,4,5-TP(Silvex) beryllium -chJorobcn.u:nc: --
-chlordane cuc.lmium chloroform ---
bcpUlcWor ch.JoricJc o-cn:::;ol ----
hcxachloroben.z.ene chromium m-crc:ml
I ----
-hcxach.loro bu Lad icnc cobaJt p-<:rcsol . ---
-endrin copper crc:sol ---
lindane fluoride 1,4-dichlorobenune ----
I -melhoxychlor iron 1,2-dichloroc:thanc ---
-toxaphcne l""d I, 1-dicWorocthylcne ---
--nun g an es e -2, 4-di chi oroc:th y I enc
I ---mercury -hepUJ.chlor
-nickel hc:xachlorobenzcm: ---
nitrate: bcxachlorobuUldiene ----
I
selenium hcxachloroethanc ---
--silver -methyl c\hyl ketone
FOR LAB USE ONLY sulfates n.itrobc:rucne ---.
{p -/,;) -9(;;, tJ;fj thallium pcnLUchloropbenol ---
I Date Received vanadium pyridine ---
zinc tetrachloroethy lenc
{P -/tJ-ft,, Bt[) ---
Date Extracted pH trichlorocthy lcnc: ---I Date AnalywJ --conductivity -2 ,4,5-trichlorophenol
TDS 2,4 ,6-trichlorophenol -----fla!ih point -vinyl chloride
Reporte<l By . cnJri.n ---I Date Reponed ---lindane
---mcthoxychlor
• ,. ,·, .. q ... Loxaphcne
.. ..;v,~j..&..-1.1 ---
Lab Number 2,4-D ---
---2,4,5-TP (Silvcx)
OHS 3191 (Ri::vili::d 11/9J) I
I
._ .. , •·--·--··.·
STATE LABORATORY OF PUBLIC HEALTH I
I P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO 10/-~,"LJO </IA :::;l -~ '7'(,7 "?/00 U/,,,_.':J/0 I
EXTRACT ABLES -FIELD # V.:. I -CXJ J -<;' t<., -:.1 ~ 1 -<:,. 1 v..:,, -Oo3~" , lnt..-001/ .,;;,
C01POOND TYPE ( _; ') (o<l ( .;l.) ( ...:2 l
UNITS V .. n/1 uo/1 \,nl~n uo/1 un/1 "lrn,,t,,,
itrosodirnethvlamine I0/_,,,10 VI_, I IL-I i.A--
(2-chloroethvl)ether
hlornnhenol
I henol
1--<iichlorobenzene
. -dichlorobenzene
1.2--<iichlorobenzene
_ ,(2-chloroi•~r~ul)ether
t ach l oroethane
-n i troso--<ii -n-<>roovl amine
r · trobenzene
liohorone
1i trnnhenol
2 4--<iirnethvlohenol
(2-chloroethoxvlrnethane
--<lichlo~henol
l 2,4-trichlorobenzene
ththalene
achlorobutadiene
-ch l oro--m-creso l
lach lorocvc lnnPntadi ene
,.6-trichlornnhenol
hloronaphthalene
acenaohthvlene
l;thvl ohthalate
--<iinitrotoluene
acenaohthene
0 4--<iinitrnnhenol SO/ 'hSO
4--<iinitrotoluene i/OI '330
,-nitroohenol ,;"QI 1150
fl uorene /0/330
chlornnhenvlohenvlether
ethvl ohthalate ..v
4,6-dinitro-o--cresol so, ,.,,._i:-o
rhenvlamine /01330
obenzene
· 4--br,...,.,.,,,henvl ohenvl ether
lxachlorobenzene ~
ntachlor~henol SO,lt,,5"0
1enanthrene l/'I F ~30
anthracene
butvl ohthalate I , -
uoranthene ,, I • I 'I
,n']) L
I-Estimated value. /-1,,_o/SO/t-
-Actual value is known to be less than value given.
w1,,~1o;i_
6jl. -oos-,w
( .,;i. )
uo/1 l.nn'm
I A
I
'
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nuroer
I -Not analyzed.
is the Hinirrun Detection Limit. m'I)L -----Tentative identification.
_ -On NROC List of Priority Pollutants.
I
4'/, -{/0, -f
,-.:.c-10)"-<;,, 1
( cl\
l'un/l ~
I
/
"' /
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
BASE/NEUTRAL ANO ACIO
EXTRACT ABLES
OltlPOONO
ovrene
benz i dine
butyl benzvl ohthalate
benz(a)anthracene
chrvsene
3. 3-dich lorobenzidi ne
bis(Z-<athvlhexvllnhthalate
di-n--0etvl ohthalate
benzo/blfluoranthene
benzo(klfluoranthene
benzo(a'\n..,rene
indeno(l 2.3-cd)nvrene
dibenzo(a h)anthracene
benzo(o.h il=rvlene
aniline
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2-<rethvlnaohthalene
2-<rethvl oheno l
4-rrethvlphenol
2-nitroaniline
3--n i troan i 1 i ne
4-nitroani 1 ine
2 4.5-trichloroohenol
,,,·,~:-.'
STATE LASORATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
LAB HO 4'/4.~QVY 1C//o.Ju I-, 1qw~100 14'w.=?JOI
FIELD# -::, -001-s,; ;"7/-oo.i--o "'l -0<861.,J lt'.:.L-00'-/-51,
TYPE r,;:,, J r.2. l I 7) ( .2. l
UNITS ..,,...,n/1 ~n .. n/) ~ .. n/) ~ uotl" ..
/()/:;30 I.I(__ I -ilL-j
l_.i;-n /1h50
101.:,30
. ,
so/1"-""0
10/330
10/.i.◄O
.so/1Afo
I I I /
,✓ ' ' \
L~O /J,_,.O I -IA -lA-IA
'-'· ia t.=o
,..,
s-o ,, f,,So
/ I I I ,, ' ' I ' ' ,
t'rl1)L-
J -Estimated value. H:zO/ So/i...
K -Actual value is known to be less than value given.
iC/l, ~I!).).._
1/41,-0oS J;.
I~ l
""/ l ""\. ..
,1
/
µ_
/
\
l -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurt,er is the Mininun Detection Limit. ~
NA -Not analyzed.
1/ -Tentative identification. fl -On NROC List of Priority Pollutants.
C,/_ =?/(1 :i
'-L-m -<i.J... (-: '
,,qi)-L....,,. -
-I
I
'
I A. -
,
\
I
I
BASE/NEUTRAL AND ACID
EXTRACT ABLES
COIIPOUND
litrosodirrethvlamine
(2-ch loroethvllether
-ch 1 ornnheno 1
lnol -dichlorobenzene
-dichlorobenzene
1.2-dichlorobenzene
1(2-chloroi llether
ach 1 oroethane
N-ni troso-di -n ~roovlamine
~obenzene
horone
-nitr,..,.,henol
14-dirrethvlohenol
s(2-chloroethoxv)rrethane
4-dichlo~henol
1 2 4-trichlorobenzene
rhthalene
xachlorobutadiene
4-chloro-m-cresol I rachlorocvcl=ntadiene
4 6-trichlor=henol
-chloronaohthalene
acenaohthvlene
rrethvl ohtha late
6-dinitrotoluene
acen>nhthene
4-dinitrnnhenol
4-dinitrotoluene
4-nitronhenol
I 1 uorene
-chlornnhenvlohenvlether
iethvl ohthalate
4 6-dinitro-o-cresol
lohenvlamlne
zobenzene
4-br~henvlnhenvlether I exachlorobenzene
"'ntach 1 ornnheno 1
henanthrene
-nthracene
ibutvl ohthalate
luoranthene
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. _WILHINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEHICAL ANALYSIS
LAB NO '-ft,,_ 1/ a 1..1-C/1._;.uo \ qf,,-<J OIA 'fl,,,.~/()/
FIELD # (',; l-OO/ ft,J Ull -OO). -ft,,J :lnL-00::i.-ll,1 u,l ·OO</ -ll,
TYPE < I l r / l r J l ( / )
UNITS ,.... ua/1 ' ·-ua/1 \,-~ ua/1 )mttm u a/ 1 ). """'7n
IO/ -<~t:J •A-'" v<-IA
SOI '&.50
'/()/ .-~o ,o/ '650
·/0/330
J,
50' i,-_i:o
/0/330
,,
.so/11.:ro
J/1 r :1~0
I I I I ,, '
m"DL
I -Estimated value. fl,.O/S0/1 ...
-Actual value is known to be less than value given.
f./1, -"// O,Y
l'nl -oor-1,,,
( / )
IJQ/1) ~-
0<.-
/
L -Actual value is known to be greater than value given.
~ -Haterial was analyzed for but not detected. The nurber
A -Not analyzed.
is the HinilTUll Detection Limit. m']JL ----
I -Tentative identification.
_I -On NROC List of Priority Pollutants.
I
'I(;,. :? I 0'-t
{nl~-l1L}
( J )
ua/1~
LA._
'
..
I
\
STATE LABORATORY OF PUBLIC HEALTH I
I
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I
P.O. BOX 28047 -306 N. WILMINGTON, S1., RALEIGH, N.C. 27611
ORGNl!C CHEMICAL MALYSIS
,. BASE/NEUTRAL MD AC ID LAB NO '-/&3/0<f '/I; "fl/l, '-f (., :.: I 11t,, 9&3Jo7
EXTRACTABLES FIELD# In l-001-/l,J ,,._ l -o o::i. ·f/.,) Ciil-003--/7.1.. U//rOO</-fl, /
00'1POOND TYPE < I ) . ( / ) C./) { / )
UNITS /1,n/l J,-ru a/ 1 l , "°""" 11n/l" un/1 J~.4
ovrene /01 '130 I I , I , 1/L-
benzidine .,/J ln,,;o
butvl benzvl ohthalate J0/'130
benz(a)anthracene
chrvsene .
3.3--<lichlorobenzidine lt,.'iO SO/
bis (2-ethvl hexvl lnhtha late l()/330
di-n-octvl ohtha 1 ate J0/.1.~o
benzo(b) fluoranthene SO/t~'i'O
benzo(k)fluoranthene
benzo (a) nvrene
indeno(l .2 3-<:dlovrene
dibenzo(a h)anthracene J I I I
benzo(a h. il=rvlene ,v ' ' I
aniline .<a/JhS'O ,,_ IA-1/-L,-L ...
benzoic acid
benzvl alcohol
4-<:h loroani 1 i ne ' ,
dibenzofuran 1oz=a
2-m,thvlnanhthalene
2-m,thvlohenol
4-rrethvlohenol ~--
2-nl troani 1 ine S"o/Jl.So
3--{l i troan i l i ne
4--{li troani 1 ine I / / I
2.4 5-trichlo=henol '/ "\ ' ' J '
I
I
I
m1H ..
J -Estimated value. H2-0/ Solt..
K -Actual value is known to be less than value given.
l -Actual value is known to be greater than value given.
<-It, ::/1 ox
(w-oa:;i-f-},el
r I )
HO/]
t,(._-
I
'I.
IA-
I
"\
I
I
I
U -Material was analyzed for but not detected. The nurber is the Minirrun Detection Limit. ~
NA -Not analyzed.
1/ -Tentative identification.
~I -On NRDC List of Priority Pollutants.
';/t,31 O<t'
r n/ -()(X,-/1, )
(/ )
,on/1 J....A....
1,'l_....
I
' I
'-~
.
I
'
···-· : .. -,,_,
I
I
BASE/NEUTRAL ANO ACID
EXTRACTABLES
IXJMPCXJNO
STATE LABORATORY OF PUBLIC HEALTH
P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO 'f{o -<// 0 ','/n ~I/ I
FIELD # nl-007 •J"'Jt.., u,t..-om-n.,
TYPE t I l r I l ( ) ( l ( )
UNITS .. n/1 .tn-,,p,, un/1 ~ un/1 .. n/ko .. n/1 ua/ko ua/ 1 .. n/ka I ~nitrosodimethvlamine 10/::no I• I•
is(2-chloroethvl)ether
-chlor~henol
henol I 3-<iichlorobenzene
4-<lichlorobenzene
1 2-<lichlorobenzene
l:s(Z-chloroi Jlether
xachloroethane
N-nitroso-di-n---'"'rr'V'l"lamine
1
i trobenzene
kr'V'lhorone
-nitr....,..henol
2.4-<limethvlnhenol
lis(2-chloroethoxvlmethane
, . 4-<lich lo=heno 1
1 -2 4-trichlorobenzene
aohthalene
exachlorobutadiene
4-chloro-m-cresol
I exachlorocvcll"V"\.Ontadiene
4.6-trichlor~henol
-chloronanhthalene
acenaohthvlene
imethvl nhthalate
6-<linitrotoluene
acen:inhthene
4-<linitr~henol Sllhr,,so
4-<linitrotoluene !Ol~"IO
4-nitr~~henol <"Obf#SO
1 luorene to/E3o
~chlor~henvlohenvlether
1ethvl nhthalate j,
4 6-<linitro-o-cresol ~1'-<:"0 50 1
iohenvlamine /01330
zobenzene
4-br~henvlnhenvlether
I exachlorobenzene ' =ntach 1 or-heno 1 S0l/6'5'0
henanthrene ,,, /·:r::,o
I
nthracene
ibutvl ohthalate / /
luoranthene ',, ' rn'"DL
I -EstirMted value. 1-l,.o/sott-
-Actual value is known to be less than value given.
L_ -Actual value is known to be greater than value given.
-Material was analyzed for but not detected. The nurber
-Not analyzed.
-Tentative identification.
is the Mini1TU11 Detection Limit. mTJL ----
_ -On NROC List of Priority Pollutants.
I
( l
un/ 1 .. n/ka
I
I
I
I
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I
I
I
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BASE/NEUTRAL AND AC ID
EXTRACTABLES
aJMPCXJND
nvrene
benzidine
butyl benzvl ohthalate
benzfa)anthracene
chrvsene
3 3--<lichlorobenzidine
bis (2--ethv I hexv I\ nhtha 1 ate
di-n--octvl ohthalate
benzo(blfluoranthene
benzo(k)fluoranthene
benzo(a)nvrene
indeno(l.2 3-cd)nvrene
dibenzo(a h)anthracene
benzo(o h. il=rvlene
aniline
benzoTC acid
benzvl alcohol
4-chloroanil ine
dibenzofuran
2-rrethvln,nhthalene
2-rrethvl oheno 1
4-rrethvlohenol
2-n i troan i 1 i ne
3-ni troani line
4-n i troan i line
2.4 5-trichlo~henol
J -Estimated value.
K -Actual value is known
I L -Actual value is known
U -Material was analyzed NA -Not analyzed.
STATE LABORATORY Of PUBLlC HEAUH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO <'./(n -<!ID 'f{,,-{/1 I I
FIELD# 'oi-007-/JV nl-001'-fh
TYPE LJ ) r ) ( . ) ( )
UNITS un/] J....&o .. n/1 1.--. uo/ I uo/kq uo/ I un/kq
/0/ '30 ,, -I -'5'1'.l 11,50
10, 'l.JO
.
so/1t..'i'o
I0/330
I0/.1.:.o
so/J,;,,;-o
I I ,,. ' "I
5"0/lh.•O 1/4-(..,{__
~ ,
10Z=o
~:,
S-oht,,So
I / ' ., '
mnL
H2.0I Sall...
to be less than value given.
to be greater than value given. for but not detected. The nurber is the Minirrun Detection Limit.
l/ -Tentative identification.
I
~/ -On NROC List of Priority Pollutants.
r ) ( )
uo/ 1 uo/kq . uo/ l un/ko
()'J::Z)l ..
; \• .. , 'I N. C. Departmenc ofH~man Resources SAMPLE ANALYSES REQUEST
Seate Labor:;,;vry of Public Hca
~ Divl~ion of J:-iea!ch S:cryi~.C;S ... P. 0. Box 28C
306 :-i. Wilmington Srr
Raleigh, 27t ii Site Number '7 .2 d) -; g d-. Field Sample Number _/_..S_-_c?_7~~----------
~ NameofSite &c:p.s,{a-,,.,, Lc,,)e, SiteLocation ~0'/4,,<y,h, /1,/,C,
. ' ' .,.,,-7 'I .. Colie~ted By ¾ c:ft' dJ u f/e:v-' ''i Tb){'' .•,-fl Z::. -, .... Date Collected J Oc /; / 9': '10 .·
: Type of Sample:
I
I
ii
I
I
I
I
I
Environmental Concentrate Comments
✓ .
__ Groundwater (I) __ Solid (5)
___ Liquid (6)
__ Sludge (7)
__ Other (8)
~c?, He, /u-krTon W,q,.d
__ Surface Water (2)
--Soil (3)
__ Other (4)
Extractables
Parameter .Results mg/1
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
__ Mercury -
__ Scl.cnium
__ Silver
--..
--
--
-----
Parameter Results mg/ 1
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX .. -
--
--
INORGANIC CHEMISTRY. .,,,~-R-u Toi:'al t ND Sf.GTWM
Parameter Results mg/1 Parameter
,.,..,-A . __ rsemc .L,::, ol /Silver
...,....-Barium Q IB __ Sulfates
.,,/'Cadmium .L...o ao!c> __ Zinc
__ Chloride _Ph
./ Chromium Lo ;:;;l __ Conductivity
___ Copper _TDS
_Fluoride _TOC
__ Iron --
J Lead Lo~co;;! --
/Manganese --{), OooJ __ Mercury --
__ Nitrate. --
· / Selen·i~m LQ ,:-C,;;. --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Par;;i.meter
..
_EDB .. .. _· _.,. Methoxychlor
__ PCB'.s . _._. _. Toxaphene
__ Petroleum _· 2,4-D
__ Encirin _._. 2,4,5-TP (silvex)
· __ Lindane --
MICROBIOLOGY ·. RADIOCHEMISTRY
Timc . .2.,'.2(,7
Results mg/ 1
-'--o.oS
..
Results mg/;
.
I P~r~metC:r .. ,.. . : Parameter·. RC:sults PCi/1
\---'-''-----"-"-'-----'-----------·-~,+-'.'-'----.. -. -.----------------
--(MF) Coliform Colonics/lOOmls __ Gross Alpha I __ (MPN) Coliform Colonies/lOOmls _._·_Gross Beta
I Date Received ----------~-------
• Date Extracted
Reported By __________________ _
I DHS 3191 (Revised 7165)
, .. 1;,l .,..,,1 H::1:,rrln,1~ \Varn:: (Review 7/87)
Date Reported -----~-----------
Date Analyzed ---c-i--c-'-c-'cr-----,--------
J /\_' ·1,
Lab Number
. . .
SAMPLE ANALYSES REQUEST
. Scat~ Labor~~-o~Y-~r P-~-blic H~a:
P. 0. Box 280
·· 306 ~-Wilmington Seri
I . Raleigh, 276
'!!!ice Number 7 2 · dJ -T ,g A-Field Sample Number ~/~~~-"?~7~,r_· ---------
aiame of Site Gres/[aw, L Cl' ).e,,. Site Loca,ion 'd'?0'/4,9Yb/ A/, C,
, "llt,1ie~ted By ;:;z;;.c,k dfuf/er-·•:, TD#~, '':Z::: z=· -, ... Date Collected J Oc/;. /9'.'1.0
II ypc of Sample:
I Environmental Concentrate Comments
-✓ .
___ Groundwater (I)
1---Surface Water (2)
__ Soil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
___ Other (8)
-'#1, A6/e, . dfc;,,, Wei/
1--Ocher (4)
Extractables
I
I
Parameter
__ Mercury
__ Scl.cnium ·
__ Silver
Parameter
_P&T:GC/MS
__ Acid:B/N Ext.
_Tox-
--
--
-Results mg/1
Results mg/1
-
INORGANIC CHEMISTRY.
Parameter
,_,,,..A . __ rsemc
..,,,-Barium
,.,,,----Cadmium ·
__ Chloride
/chromium
___ Copper
~Fluorid~
__ Iron
J Lead
JManganese
__ Mercury
__ Nitrate.
·v Selen"i;,m
Results mg/1
L.o-q\.'
0.18
L.o. oo'q
Lo.o\
La.ool;;:,
o, aoo..7
Le -006
ORGANIC CHEMISTRY
Parameter Results mg/1
. .
_EDB
., .. ·.'.:
__ PCBls . --.: ... .. . •·
__ Petroleum
__ Endrin
__ Lindane
I I. '
Total
' .•.
Parameter
,._,/ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_T(JC
Parameter ..
_· _.,. Methoxychlor
_ ... _· _. Toxaphene
_. 2,4-D
_._. '2,4,5-TP (silvex)
--
I MICROBIOLOGY •. RADIOCHEMISTRY
Time..2,'L/0
Results mg/1
Results mg/,
•. . ... .
.
P~r~met~r : Parameter. .-RC:sults PCi/1
I --(MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/100mls
_· _ Gross Alpha
_. _· _ Gross Beta
I Date Received Dace Reported
Date Extracted---------------~--Date Analy,ed ________________ _
I Reported By ---.----------------Lab Number
:'UC: <101 rn.-vic;rt{ 7/85)
...
. ' . '.
SAMPLE ANALYSES REQUEST. Sratc Laborarory of Public Hcah
P. 0. Box 280,
306 ~-\Vilmingt:on Sm:
I
Raleigh, 2761
te Nµmber '7 ,2 · ,£) -T /3 A-Field Sample Number _/'---'=S<'-=-;f-'-7,--=6"'---·---------
t me of Site Gc:es-6'.a<'.'1 Lcr)-e--.. · SiteLoca,ion d'(0',0,/(:y_h, A,/,C,
,,_ liCcted By . ~c/t' dfvt f.!'t;:JY ·•;; ib1l'' ·":Z:: z::· -"·-· Date Collected '3 Oc M9'. 9:"0 .•
jj.YPC of Sample:
I Environmental ,/ ..
___ Groundwater ( 1)
1---Surface Water (2)
__ Soil (3)
1--Other (4)
I Extractab les
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
'•
Comments
. "lit" /0, ,ij,✓/1,-,.,Qs <r 6:oere""lt · we//
C:Ac,,,/,-he.J u,,,r-fJ,. ])'YI/ H #0?)
I
INORGANIC CHEMISTRY.
Total '
Parameter Results mg/1 Parameter Results rng/ 1 Parameter Results mg/1
I FArs_enic
,,,,-A . .L.0.01.1 -· ._/Silver -· Lo -1.J 5
__ rsenic
...,,.,..-Barium L..o.o::\ __ Sulfates "
__ Banum
__ Cadmium ._,.,/ Cadmium · LO,OQf111 __ Zinc
I ,__ Chrorr.ium __ Chloride _Ph
__ Lead ./ Chromium Le 01 __ Conductivity
__ Mercury -___ Copper _TOS
1-Scl.cnium
. -Fluoride _TOC
-..
__ Silver __ Iron --
--. <./ Lead LO-Qclf• --
.. .. ✓Manganese
I --< b, Qoo-::i_ --
--__ Mercury --
--. __ Nirrate.
1-V Selen·i~m 0 OQ~ --
. . " .. ORGANIC CHEMISTRY
I Parameter Results mg/1 Parameter Results mg/1 Parameter Results mg/1
.. ... . . _· _·•· Mechoxychlor
'·
_P&T:GC/MS _EOB
"
__ Acid:B/N Ext. __ PCB's . -~ -· .. " . '• _._. _. Toxaphene
I _Tox-. . __ Perroleum
.•, _. 2,4-0 ,• .
__ Endrin
. __ .·. 2,4,5-TP (silvex)
----· __ Lindane --
I MICROBIOLOGY · RADIOCHEMISTRY
Par~me·t~i: . :i·~ : • : Parameter· . . ~, . Re'sults PCi-/1
I __ (MF) Coliform Colonies/lOOmls _·_Gross Alpha
--{MPN) Coliform Colonies/lOOmls _. _· _ Gross Beta
----..
1---
Dace Received ----------~-------Date Reported -----~-----------
.Date.Extracted
Dace Analyzed ---~--:-er-~~--------
' i ,/ -__.·
Lab Number
I Reported By
1'\UC <101 (Q,.:,;c,-rl 7/R'i)
I ~-C. Dcparcm~nc of H~man Resources
: Division of f::-iea!th_,$.cry~~~ .. ,
Scace Labora:vrY Of Pubfrc H
. P. 0. Box 2:
306 !'-i. \Vilmington ~ _SAMPLE ANALYSES REQUEST .
'I Raleigh, 2·
/ Sicc Number '1 ,2 · d.) -I ,6 A-Field Sample Number _/_~_-_,2"_'7_7_· _______ _
i Name ofSice Gre:.:r/4,.,, L c,, )e.-Site Loca,ion ?'f'o-/4,/tyh, MC,
;·l·collCcced By . ~c,,k dJ.,{f/r::r ·,:• TIJ#''' ·":Z: r -~---oate Collected ·Joe 61i'lo
i Type of Sample:
Concentrate Comments ··-:I Environmental
: --✓
: ___ Groundwater (1) __ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
#//✓/<ea Con£7rucf,·on /A/e/1
i I ___ Surface Water (2)
ii
. '
I
I
I
I
I
I
I
I
I
__ Soil (3)
__ O,her (4)
Extractable,
Parameter .Results mg/1
_· _Arsenic
__ · Barillm
__ Cadmium
__ Chromium
__ Lead
__ Mercury -
__ Sel_cnium
__ Silver
--.. .. -------i-
Parameter· Results mg/1
_P&T:GC/MS
__ Acid:B/N Ext.
_Tax--
----
MICROBIOLOGY
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Colifor,n Colonies/100mls
..
INORGANIC CHEMISTRY.
Parameter Results mg/1
,✓,-A . Lo_c·\ , __ rsemc -
,__,.,---Barium Q.0\.9
..,,,-Cadmium· L D::,,O:C;?:c:.,l
__ Chloride
/chromium ""'-o. a\
___ Copper
~Fluoride
__ Iron
'-✓' Lead '-O_ QO'g
Total
I I. ,
Parameter
./ Silver
_·_Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC .. --
----
.
--;::?Manganese
(0; 000 __ Mercury d,, --
__ Nirrate. --
v Seleni~m o.oo§ --
ORGANIC CHEMISTRY
Parameter Result, mg/1 Parameter
. . ., .. ·.'.: .. _· _,•. Methoxychlor _EDB
__ PCB's -·.:. :•--~-· ·, _ .. _. _. T oxaphene
__ Petroleum
. _. 2,4-D . ·.
__ Endrin __ .. 2,4,5-TP (silvcx)
· __ Lindane --
·. RADIOCHEMISTRY
.
Results mg/
--LO -OS
.
.
Results mg
-'
-
:_Parameter· .. . Results PCi/1
_·_Gross Alpha .
_. _· _ Gross Beta
I
I
I
Date Received -----------'--------Date Reported -----~----------
Date Excracted ---------------~--Date Analyzed ----,--:-:-----------
Lab Number ___ · __ .·_i_,_-_··_<_J_, ____ ::_J~_· ____ _
Reported By
llHS 3191 (Revised 7/85)
DIVISIO/, OF s.E.J.J.,T~ S:C:?.\'IC:C:S
SOLID n,7:l E.< .. U.PJ)OUS \,'ASTE ~c<J;;.Gc:>-8: 3:::._syCH
Cnci~ of Cus:::g_ci•,· Record
I E2z2rdous ~2ste ~Eteri2ls
Geuer2to-r
I
Tele_:,:~o::ie( 9 / ,9' ) 73 5-Z rf'O / ---
D2r S2-:nple6 . <? Oc T',,-/9''70 Tille Sc.3vied ----------
T Y,:·e c·:: Pr DC" s s Gener 2. t; ~ g 'n' 2. s te~t:::cc0'.'.'.~n"'-',,(~·~H~O~U=Y~M=--------------------
I
2 -1;----=--~--"--'f'/'____,_P_-_a....:::.;,;...z.,,,/~-~"-""-"-=---==-
signature
3•--------:-----------sign~tur.e
_?-9--Qi:;;p; 70
inclusive d2. t:es
inclusive dates
inclusive 0.2.ces
d2.r:e
Complete c..11 2pplicc.·01e inforcc:io-;-, inciuC:inb sifF12cures> and
· submic. \.cich ·..2.nc:lysis reques.: fo:-:::s.
I
' I C. Oc~arcIT'.:!"lt of H~man Resources
vision of Mt.::.!:h S_cryic_cs _ .. SAMPLE ANALYSES REQUEST
$(ate Labor,:.._"lry of Public Hc::i·
P. 0. Box 280
306 ~. \Vilmington Ser
Raleigh, 276
Nome of Sire
lolie~ced By
Type of Sarc~!e:
Concentrate
Comments I Environr..ental
/ C.-,:-,~1ndw:ncr (1)
1---Sc:iace Water (2)
C: ., (')
__ Solid (5)
___ Liquid (6)
__ Sludge (7)
___ Other (8)
,;l:cf7, dq //'½u,,-70-n We-//
---.... c:: J 1--C:her ( 4)
Extractables
-
I
I
I
I
I Pararr:eter
__ Arser-:1.:
--Bariu::;.
__ C2drr,::.1rn
__ Chro:-::ium
___ Lead
.. .-k{erc..:ry ;, . ··.· s ., .... :.,
1··-··· S~~;~~m
I_
--
----. .. --
Parameter
_,_ P&T:GC/MS
__ Acid:5/N Exe.
_TOX ·-
----
Results mg/1
..
..
Results mg/ 1
-
,, 11'
0
-'!'-ll'f.~11 .. •·• ·•
INORGANIC CHEMISTRY. ,. '. -.
Tot':l\it'ttihmD SECTION
Parameter Results mg/ 1 Parameter
__ Arsenic __ Silver
__ Barium _·_ Sulfates
__ Cadmium
. __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
___ Copper _TDS
,__ Fluorid;: -_TOC
__ lron --
__Lead --
__ Mc.nganese --
__ Mercury --
__ Nirrace _ --
_.-_,_Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter
.,
_EDB
.. • _· _.,. Methoxychlor
__ PCB'.s -_ ... _. _. Toxaphene
__ Petroleum ·. _. 2,4-D
__ Encirin _._. 2,4,5-TP (silvcxj
__ Lindane --
Results mg/]
Results mg,
-
I r--------M_I.,..C_R_O_B_I_O_L_O_G_Y-------,-----i----
-
·
-
·

_R_A_D_I_O_C_B_E_-M_IS_T_R_1~------
P3:r~rne·c~r
I __ (MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/l00mls
I
I
. '-·
Date Received ~'~o~--L/~-r~·v __ A_4 _________ _
, Parameter·. Results PCi-/1
_·_Gross Alpha
_._._Gross llcra
Z--
SAMPLE ANALYSES REQUEST
State Lnbora~ory of Public Hc:i!
P, 0. Box 230
306 ~-\v'i!mingwn Ser
IL:~•jumbcr J' .2 · t?} -1 .({ /-Field Sample Number _/_2_..2~6''--5'-______ R_a_lc_ig_h_,
2
_
7
_(
l am< of Site S";-:m,Jaw, / er .ke. Site Loca;ion. ,.;f'D'.41,y;;'/ A/, C,
• ~o\i;,"cted By :::i;;,.,:: {-d? k(-,/'. ,.~,r ·•? ib){'' _.,,41. /,_£ .. -•... Date Collected J .oc I";./()' P'o
l~ypc of Samp!e:
Environmental Conccn trate Comments
I
V G,o,indwatcr (I)
Surface \Varer (2)
___ Solid (5)
___ Liquid (6)
__ Sludge (7)
___ Ocher (8)
*cf: dor //,-).,uY-7:o,a U/e,//
I ___ Or her ( 4)
I Extractables
I Parameter
__ Arsenic
, __ Barium I
•
I
__ Co.dmlt!m
__ Crlrorr:ium
.1.t~}; = ~:1curv
1·· . ; . . • . ..-· S ·1cn;nm 1--I..:•. L-l
'=Silver
I
I
I
I
I
--
--------
Parameter
_P&T:GC/MS
1..,,-""' Acid: B/N Exe.
_·_TOX .. ..
----
Resu Its mg/ 1
..
.. .. -
Results mg/1
-
MICROBIOLOGY
,
I
INORGANIC CHEMISTRY
Total
Parameter Results mg·/1 Parameter
__ Arsenic __ Silver
__ B;:;.rium _·_ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _TDS
. __ Fluoride _TOG
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nirra~~---
• C: l . _·_. _ .... e.er\!um --·
ORGANIC CHEMISTRY
Parameter Results mg/1 Paranteter
_EDB
.. • __ ·•· Methoxychlor
__ PCB'.s .•.,. . ...... _. _. Toxaphene
__ Petroleum __ · 2,4-D
__ Encirin -·-· 2.4,5-TP (si\vex)
· __ Lindane --
·. RADIOCHEMISTRY
--7 ';, 1 ii\1C -(o, 0
Resu Its mg/ j
-
Results mg,
'
-
P3:r~me·t~-r : Parameter·. . Results PCi-11
I --(MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
I
I Date Received ~(~o_-~././_-~C/~0~~14_fl~---------
Datc Extracted IO -S-'lo ,1t'1 4 A
I Reported By
_·_Gross Alpha
_. _· _ Gross Beta
Date Reported-----~----------
Date Analyzed ~/_0_-_,,1._J._-"~7o_g=£;~· ________ _
Lab Number ___ 9_0_6_-7_S~6~------
. ··. ~· .
SAMPLE ANALYSES REQUEST
·.· State Labor::.:.:i,y of ~~~l;c ~~31
P. 0. Bo, 280·
306 ~-\Vilming,:on Sen
rpc of Sarr-,;,!e:
Environr.:ental
I / G:o,indwacer (1)
___ Sc:focc Water (2)
Concentrate
___ Solid (5)
___ Liquid (6)
__ Sludge (7)
__ Ocher (8)
l f
INOB,_GANIC CHEMISTRY-
Extractable,
I Parameter
__ Arse1:l.:
, _._ Bariu::.
~--Cadm•~m
__ Chro=:-.ium
.·•:'"-;--Lead
j~-~2: ,;:_ }A.erc~ry I
I
I
I
I
I
__ Si.!l.c;:iwm , ·. __ ..... llve~
-------
-· ------
Paramet~r ·
,/ P&T:GC/MS
__ Acici:B/N Exe.
_TOX---
--
--
Results mg/ 1
..
..
-
.
Results mg/ 1
.
MICROBIOLOGY
Parameter Results mg/ 1
__ Arsenic
__ Barium
i
__ Cadmium
__ Chloride
__ Chromium
___ Copper
,__Fh.10.idf! -
__ lron
__ Lead
__ Manganese
__ Mercury
__ Nirrate
_-· _ _._Selenium
ORGANIC CHEMISTRY
Parameter Results mg/ 1
_EDB
... . --
__ PCB'.s .. .: . ·-.. ~-·.
__ Petroleum
__ Endrin
.-
__ Lindane
Comments
' ' •
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC
------
--
----
Parameter
.. _-_.,. Mechoxychloc
_. ----_. T oxaphene
-. __ -2,4-D . ·-
____ '2.,4,5-TP (silvex)
--
·-RADIOCHEMISTRY
. Raleigh, 276
.,
Results mg/:
-.
..
Results mg
. •
.
ll-----'-'--P_a __ r_~_m_e_·c_~-~{~--~---------------~+--'-'-
P
_
a
_
r
_
a
_
m
_
e
_
t
_
e
_
r
_
·

_______ R_~_u_l_cs_P_C_i/_1 __
__ (MF) Coliform Colonies/l00mls _-__ Gross Alpha -
I
__ (MPN) Coliform Colonies/l00mls _-_-_Gross Beta
I D ~ · cl /Q·l/-'/V 11/l D R cl
_ ate "ece1ve ~~~~-~~---~--------_
ate eporce ------,,--~----------
f>-((6<.(/VI?
Dace bcracced ___________________
Date Analyzed ---'-l'--!D::,-,.,1.,_::i,:-c:;"1c,D~2uU.,JJ,cr-___ .:._ __ _
I
906757
Reported By
Lab Number _______________ _
SAMPLE ANALYSES REQUEST
Smee Labo;~:vry of Public Hc:t·
P. 0. Bo:< 28C
306 >:. \'1/ilmington Ser
Raleigh, 27(
·IC itc...-_,X:\;rnber :.._7_2_dJc;_·. ----'J_____,,,!'<~{L/_._-________ Field Sample Number _1_2_;z._c_,,"-)_· ________ _
Name of Site .-Srm,Jat"'.1 / cr.-f-e. SiteJ...ocation ,;;:?o-,0,cth, A/, C'
"loli~~ted By ,J; C r d?u -::1:a,'.i<:fY' ., i 'i"b'.a''' .-,4"-1 /, -•.. Date Colle~ied . J i:::JC /; -/? er 0
Type of Sample:
I Environmental
,_/ Groundw:itcr ( 1)
___ Surface Water (2) I
I
__ Soil (3)
___ Ocher (4)
Concentrate
___ Solid (5)
___ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY.
,
Extractables
I Parameter
, __ Arsenic
• __ .Barium
, __ Cadm;um 1--Chrorr.ium
I
I
I
I
I
I
I
I
___ Lead
1>_:_' .-_ Mercury
-1~-St:l.cnium
__ Silver
--
----------
Parameter·
__ P&T:GG/MS
c..-----'""' Acid:B/N Ext.
_Tox·, __
--
--
Results mg/1
..
Results mg/ 1
. .
MICROBIOLOGY
Parameter Results mg/ 1
__ Arsenic ,
n . __ oanum
,
__ Cadmium
__ Chloride
__ Chromium
__ Copper
_fluoride
__ lron
__ Lead
__ Manganese
__ Mercury
__ Nirra~~.
_.·_._Selenium
ORGANIC CHEMISTRY
· Parameter Results mg/ 1
.... '. . .• '
_EDB
__ PCB'.s .• -· . ' ;• .....
__ Perroleum
__ Endrin
__ Lindane
Comments
' ' '
/,,// e;//
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_·_Ph
__ Conductivity
_TDS
_TOG
----
--
------
Parameter
__ ·•· Methoxychlor
_._. _. Toxaphene
. ·. __ · 2,4-D
..
-·-· 2,4,5-TP (si\v~x)
--
·· RADIOCHEMISTRY
Ti,nc 2, '9-0
Results mg/
Results mg
. .
.
I --{~F) C~liform ~~lonies/lOOmls
__ (MPN) Coliform Colonies/100mls
: Parameter·. .·. Results PGi/1
I
I
I
Date Received
Date ExcractCd
__ Gross Alpha
_._·_Gross occa
lo-t!·9o ,41/ ~~~~----------Dace Reported-----~----------
N,-s-'lo J"1~.IJA
Reported By -------------------Lab Number
' -,,...,.,
SAMPLE ANALYSES REQUEST ·-: s~-~tc Labor~:.:-ry or Public HC3l
. P: 0, Box 280
.306 >:. \Vilmingcon Ser,
Raleigh, 276
.:..'7_7_ . ...:,I)_-_~:...; __,,t?~.'~_,4'--------------Field Sample Number _/_,_2~~6_6 _________ _
9i1nm<! of Site :;.,.,. ,er,!a,.,, / C¥ ./:e,, Site Loca;ion. -<"Y'o-;,g,fr'..h/ /(/, C,
"Roliecred Br :Tqc f d!u -:f.'./t';'f"' -,; 'ib'.ii'_,_.,,_ . .v~,--,-'-+,-_./_,-__ . Date Collected "S.CJc /;. -19'.C?'.O
Jvpc of Sarr.;:-\e:
I Environmental / .
• ___ C:2c1r.dwoccr (I)
Concentrate
Com.men ts
o/ Co, v ,,-e if
/
I ___ Sc,facc Water (2)
___ So;! (3)
__ So\id (SJ
___ Liquid (6) ·
__ Sludge (7)
__ Other (8)
· LA c, c,/, -✓-:> er/ IA/ , / -I /4
I __ Other (4)
,
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Extractables
Total
INORGANIC CHEMTSTRY.
Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter
__ Arsei'!:c
__ Arsenic
__ Silver
__ ·Bariu::-,
__ Barium
,' __ Sulfates
__ Cadmi..1m __ Cadmium __ Zinc
__ Chro:-:;ium __ Chloride _Ph
__ Lead __ Chromium __ Conductivity
-_ Merc~ry --.-Copper
_TDS
_:__ Se..\c1;ium .__ Fl1.1orid~ -_TOC
. <; .• __ Iron
__ ..... 11ve:~
--
--__ Lead --
--__ Manganese --
--__ Mercury --
---. _ Nirra~~. --
-1--_.·_,_Selenium --
ORGANIC CHEMISTRY
Paramet~r · Results mg/ 1 Parameter Results mg/1 Parameter
__ P&T:GC/MS _EDB
'. _· _.,. Methoxychlor
__ Acid:B/N Ext. __ PCB'.s .· ~ . . . " .. •, _. ··--_. T oxaphene
_TOX ... . -__ Petroleum
. •, _. 2,4-D
.
--__ Endrin __ . 2,4,5,TP (silvcx)
--
__ Lindane --
MICROBIOLOGY
· RADIOCHEMISTRY
Results mg/
.
Results m,
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··. : Parart\.eter·. . Results PCi/1
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__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
Reported By
__ Gross Alpha .
_.·_Gross l:lcta
SAMPLE ANALYSES REQUEST
Smee Labor;;.:vry of Public Hc:1 ·
P. 0. Box 28C
306 '.':. \X/ilmingcon Ser
Raleigh, 27C
-'-'7-_7 _·_/]_-_1_/<"-',.~< ,,,d"-_-_________ Field Sample Number _/_-,_-_7 _r{~7~---------
'
om< of Sicc .·:;:;--f!J,/o.wz / cr.<te, Sice)..oca;ion.40',/e,L,-;;'/ ffe C'
.... oli~~tcd B\' ::Tc,,,; ( d!u-1.:,:~;Y· ··:, Yb'..f".,,.e ,;,/ ... -, .. Dace Collected ::oc ;\.;qe>-o
'
ypc of Sam;:,!e:
Environment:i.l
I r/ Croundwoter (I)
___ Su~facc \Va~er (2)
__ Soil (3)
___ Ocher ( 4)
Concentrate
__ So!id (5)
___ Liquid (6)
___ Sludge (7)
__ Other (8)
/
Comments
c:r kcrf",,,e,.j-i Ive/I
' ' '
I '
L , l INORGANIC CHEMISTRY
Extractables
Parameter Results mg/1
I __ Arsenk
__ Badurr,
__ Cadmium 1-.-Chr~;,,ium
__ Leaa
,~;-;<._:_ Mercurv .. 1~--Scleni•o;,,
__ Silvec
I ---
-----. --
Parameter· Results mg/1
_P&T:CC/MS
1..---""'Acid:B/N he.
_TOX .. -
--
--l
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I MICROBIOLOGY
I
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\ .....
__ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
; __
Parameter Results mg/1
__ Arsenic
__ Brtrium
__ Cadmium
__ Chloride
__ Chromium
-.-Copper
. __ Fluocide -
__ \ran
__ Lead
__ Manganese
--. Mercury
__ Nirra~~.
. <: l . _·_. _ ...... e.emum
ORGANIC CHEMISTRY
Parameter
_EOB
__ PCB'.s
_·_ Petro!eum
__ Endrin
__ Lind::i.ne
Result, mg/ 1
...
.• C
· 1 ··. : Par;1.rneter·.
__ Gross Alpha
_._Gross Beta
Total
Parameter Results mg/
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
[_TOG ,--
----
--
----
Parameter Results m,
__ .,. Methoxychlor
_. _. T oxaphene
__ . 2,4-0
_._. 2,4,5-TP (silvex) -
--
RADIOCHEMISTRY
. Results PCi/1
I D. ce Received _,._,/ .,__-_,_tf_-_'i',ccO,___li_l_c_f __ _c_ ______ _ Date Reported -----~----------
Date Analyzed JO-,:l,J -9o 8,1}
Date Extracted 10-1/-CJ O /Jt.:) :f/11
I Kcporced By
Lab Number 906760
SAMPLE ANALYSES REQUEST
·.' Stat~ Labor:.:..,,y of.P~b!i~ Hc:1'.
P. OiBox 280
306 >. \v'i\mingto~ Ser
Raleigh, 276
l ypc of Sam,le:
En vlronr.i.ental Concentrate
Con,ments
/ 1---G, ;:,uc.dw,rcr ( 1)
___ Sucfacc Water (2)
___ So:! (3)
I C:her (4)
I Extractables
__ Solid (5)
___ Liquid (6)
__ Sludge (7)
___ Other {8)
,~//, ,?f?e,c, -~o'"' r -fvoc;T,'o;,,
INORGANIC CHEMISTRY.
Total
,
' •
,
1Yel I
I Parameter Results mg/1 Parameter Results mg/1 Parameter Results mg/
.
__ Arse~\c __ Arsenic
__ Silver
__ Barium
. ,' __ Sulfates
__ . Bariu:-:-,
-
I __ Cadrr,ium __ Cadmium __ Zinc '
__ Chro:-:':ium __ Chloride _Ph
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"'°c--Lead
__ Chromium __ Conductivily
:i;•:,:_'·.:_ Merc.:rv .. ___ Copper _TDS
._,, -'
__ Se.!.cnium ,._ Fluoride -_TQC
__ Silve: __ lron --
--__ Lead --
.. .. __ Manganese
-----
--__ Mercury --
--__ Nitrate --
. ,
-1--_·_,_Selenium --
ORGANIC CHEMISTRY
Parameter· Results mg/1 Parameter Results mg/ 1 Parameter Results mi
,/ P&T:GC/MS
__ Acid:B/N Exe.
_Tox··.
.
--
--
MICROBIOLOGY
__ (MF) Coliform Colonies/ lOOmls
__ (MPN) Coliform Colonies/lO0mls
_EDB
__ PCB'.s
__ Petroleum
__ Encirin
__ Lindane
., .. . ,•
.·.:' ' :---....
,·
: Parameter·.
_·_Gross Alpha
_. _· _ Gross Beta
., _· _.,. Methoxychlor ' ,,
_ .. ·_-_. Toxaphene
, •, __ · 2,4-D
_·_._. 2,4,5-TP (silvcx) .
--
·. RADIOCHEMISTRY
.·_ Results PCi/1
Dace: Received -.L/ul!_· ·_(/'--· 0.c.r -"0---',4-'-'-'A'----'-------Dace Reported --=,......--~---------
fl'I] &c/-"" _-5
Date Excr2c<ed ___________________
Date Analyzed -~rC~i~-: ... ,2~,;J,---5..µD~::zi...,..1_1~/_.,_· __ ~---
Reported By --------------Lab Number 306761
•,
. ' . .
. ,. ~. Clcp•:·,m~~t of H~man Resources
iv!slon of }:-ic;;,!;:h S.cryiccs SAMPLE ANALYSES REQUEST
Stace L:1bor,~0ry' of Public Hi.::-
P. 0. Do:-: 28(
306 :--: . \Y/ilmington Ser
R,l,igh, 271
f ypc of Ssm;,!e:
Environmental
I
I
{ / .
__ ../_ Ground,,·ater
___ Surface Water (2)
___ Soi! (3)
___ Ocher (4)
Concentrate
___ Sludge (7)
__ Other (8) ' ' '
I
INORGANIC CHEMISTRY l L
Extractables
I Parameter
' j--Ars_enic i __ Banu~,
1
__ C2dm!':m
1--Chrc~ium
1-. _ Lead
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.' _ 'Mercury \
I~--S~!.cnium
__ Silver
------------
Parameter·
_P&T:GC/MS
.........--, Acid:B/N Ext.
__ TOX ..
I-, __
i
Results mg/1
..
..
Results mg/1
MICROBIOLOGY
I
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__ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
Total
Parameter Results mg/1 Parameter Resu Its mg/
__ . ..\rsenic __ Silver
__ 32.num __ Sulfates
__ Cadmium __ Zinc
__ Chloride
__ Ph
__ Chromium __ . Conductivicy
__ Copper _TDS
. __ Pluorid~ _·_TOG
__ lron --
' __ Leao --
__ ~-{anganese --
__ \-\ercury --
__ Nirra~e. --
...::..,_ Se!e:1ium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results m1
_EDB
... __ .... Mechoxychlor ..
_PCB.'s . __ . Toxaphenc
__ Perroleum .. _· 2,4-D
__ Endrin __ 2,4,5-TP (silvex) '
__ Lindane --
RADIOCHEMISTRY
-' Parameter·. Results PCi/ 1
__ Gross Alpha
_._._Gross Seta
I
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Date Received -~/ 0~·-· ti_· _C/~0_ . ..c.L//1'"'· ---~------Date Reporced -----~----------
~cportcd By
Lab Number
DIVISION OF ~i.T.:: s:::?.VIC:::s
SO!... ID J. ... '>\""D H_: . .2f._R.DOU'S \-,1.ASTE ;1,._:.]~;..G~3"T 3?..._:.J~CB
Sco:-2ge ?cciliLy
I -----------------
1"''"': 's ~,2..::2 (::;::-r .er h ~ _ /::_o-::_. __.i..:./-'---"e-,= ________ T e.l·:':_;-.:•cc,e ( ____ ) __________ _
.b.,foiess & O"/e/-o,/4 A/, ,C ✓
'cl.lee:::,,:' S :,2.2-c: -WL~~~ ./ v
Die
:1=~ c:
.: ::..:::1.c 7 ':""'l~o-:--:-.:: ;--: ~';"'\
J ____________________ _
•<
.l2.1.c. c: Possession:
J
I
3.
I
signaLui-.e
. / I
C..,.fti,,.1
.?-Y~;z'.:t
-i":'"'c:.lusive dc.-ce.s
-i-..:lusive d2.ces
-::~elusive. 02.ce~
~:..:_:_: s __ __ll4-'-#,"f+-,~-;::_.7,!_'Zf,;{:?'~<0'.:J-s~::::::::_ ___ _
I
I
Complete ·~11 2pplic2.·01e in~o1.~~:i.o~, inciuCin6-sig:12cures, and
subroic \..'ic.h ·...:::nzlysis re.aves;: fo:-:::s.
oASE/NEUTRAL NID ACID
EXTRACT ABLES
a::.IPOUNO·
N-ni trosodirrethvlamine.
is(Z-chloroethvl)ether
chlorrvihenol
phenol I J. 3-di ch lorobenzene
4-dichlorobenzene
.2---dichlorobenzene
bis(2-chloroi llether
,exach 1 oroethane
-ni troso-di--n....:Ornnvlamine
nitrobenzene
soohorcine
-n i trooheno l
2.4-<lirrethvlohenol
is(2-chloroethoxv)rrethane
.. 4-d i ch l orooheno l
l 2 4-trichlorobenzene
nanhthalene
exachlorobutadiene
-chloro-m-cresol
.· ·-.xach lorocvcl~ntadi ene
' · ; 4 6-tri ch lormheno l
-chloronaohthalene
acenaohthvlene
dirrethvl ohthalate
.6---dinitrotoluene
acenaohthene
· ?~_4---dinitrlYlhenol E 4-dinitrotoluene
-n i trooheno 1
fluorene
4-ch lornohenvlohenv lether
diethvl ohthalate
4 6-dinitro-o-cresol
diohenvlamine
azobenzene
4-braroohenv l ohenv le ther
hexachlorobenzene
~n tach l ornoheno l
enanthrene
anthracene
dibutvl phthalate
fl uoranthene
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEAL TH SERVICES, N. C. DEPARTMENT Of HUKAN RESCXJRCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL NIALYSIS
LAB NO IO/JIA7SI~ l.4t}/475f 'ofD!.,7 bO a ,,t,, 71,,,;;;i_
FIELD # 1.-.:11. 3 /.~.~ t~ ._.-/?,)/.7 1~ ~1 .. q
TYPE (/ ) (/ ) < I ) ( ; )
UNITS v ua/1-__ ua/lhm7'li'll 1 ua/J),.~ /~q/1}~
to/ -<-<o -Ii -/J..-u__ IL -
101:·
·. /01:"'
ION:
;,<....,
' !Ok
·1
so, 1.,,50
/01 ~'10
,01 ,,. ,_o
/0 '.;3o
J.,
so, )l.,11
,J,
1~/330
I o/:;>,r,
S0lllnS0
//1/330
,
V • '
m"DL
IJ -Estimated value. H,.o/.SO/L-
·. · K -Actual value is known to be less than ·value give~.
( )
ua/1 ua/kq
,, L -Actual· value 1s known to be greater than value given.
--· U -l\aterial was analyzed for but not detected. The nurber
INA -Not analyzed. ·
is the Mininun Detection Limit. ml)L ---
1/ -Tentative identification. fl -On NROC List of Priority Pollutants.
II'.:'. C. V.{.v.U.,.{.OYL o 6
lf'HS 3068-0 ( 4 I 86
He.a.Uh SVtV.{.C.e/2
Lab0Jta.;to1t.y)
-
( l
~q/ l .. n/kq
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STATE LI\BOOATOOY Of PUBLIC HEALTH
orvisroo OF HEALTH SERVICES, N.C. DEPARTMENT Of HUIWl RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 2761 I
ORGANIC 01EMICAL ANALYSIS
BASE/NEUTRAL ANO ACID LAB NO f./171~75& C/o&-1~)( ,'f'Ol~//nn Oi,1_,/ ~
EXTRACTABLE$ FIELD# '/.;? _l /_ '<' ;.;i-;_,;: / 1-, /_ 7 /.,J_ ,£q
COMPOUND TYPE ( ) ( ) ( / ) ' , I 1 •
UNITS ,.,.,; l ,~-.. n/ I ~ "n / \'-..-.Lw, .. n/l\,n-8-,,
ovrene /0/.'?30 , , l.l -K.--
benzidine ,n /,,_c-o
butvl benzvl ohtha late /0 ::;30
beni(a)anthracene
chrvsene . ,
· 3 3-<Jichlorobenzidine so/1k,;-o
bis (2-€thvl hex vi l ohtha late lo/330
di-n-oetvl ohthalate 1/0/3~0
benrn(b) fluoranthene so/11,,,;o
benio(k)fluoranthene
benw(alovrene
i ndeno( l 2. 3-cdlnvrene
dibenzo(a.h)anthracene
benzo(a h. i)D<ervlene ' , ' ' / ' I ' I
aniline <o 1,,__,,,,o i,,L. ll~ /,I -; ,I ~
benzoic acid
ben,vl alcohol
4-chloroaniline ,,,,
dibenzofuran /0 =o
2-n-ethvlnaphthalene
2-n-ethvlohenol
4-n-ethvloheool '\l'
2-ni troani 1 ine S-ol,l-.~o
3-nitroani line
4---nitroani 1 ine -.
2 4 5-trichlo~henol ,J/ '\ \' \ '
IK'IRI./ 1-VL. r'/IIJS, +I-( J (..+ ) (-) ( )
m]) ,.._
J -Estimated value. H:z.OI Soli-
to be less than value given. K -Actual value is known
L -Actual value is known
U -Katerial was analyzed
NA -Nol analyzed.
to be greater than value given.
for but not detected. The nurrber is the Hinirru:n Detection Limit.
1/ -Tentative identification.
~/ -On HROC List of Priority Pollutants.
N. C. D-i.v,u.,-i.011 o 6 He.a.Uh SeAv-i.cv.,
VHS 3068-0 (4/86 LaboJLJUo~y)
( ) ( )
ua/ 1 .. n/ka .. ,.,; I ""/kc
~
I STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOORCES
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611
I(> Laboratory No. tJor;,755 PURGEABLE COMPOONDS Date of Analysis
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COMPOOND µg/l COMPOOND
Dichlorodifluoranethane IA Chlorobenzene
Ch l oranethane Ethvlbenzene
v'Vinvl Chloride 1 l l.2-Tetrachloroethane
Brcm::methane n-Xvlene
Chloroethane m-Xvlene
Trichlorofluoranethane o-Xvlene
✓l 1-Dichloroethvlene Stvrene
Methvlene Chloride Broonfonn
tert-Butvl Methvl Ether I !benzene
fl rans) 1.2-Dich loroethvlene 1. l 2 2-Tetrachloroethane
Is 1 ether Broonbenzene
1. 1-Dichloroethane n-Prnnvlbenzene
2 2-Dichlo~~ane I 1.2 3-Trichlo~rnnane
fCisl l .2-Dichloroethvlene ? )(, /_ 2-Chlorotoluene
Chloroform u 1. 3 5-Triirethvlbenzene
fBCM) Branochloranethane I
✓l. 1 1-Trichloroethane I
4-Ch l oroto 1 uene
/Tert) Butvl Benzene
l. l Dichlornn.-nn,,ne ! Pentachloroethane
✓carbon Tetrachloride I 1 2 4-Triirethvlbenzene
✓Benzene I. rsecl Butvl Benzene
✓l 2-Dichloroethane vi ri-I lto 1 uene.
✓Trichloroethvlene 1(),7 l 3-0ichlorobenzene
l 2-Dichlornnrnnane " ✓l 4-Dichlorobenzene
Brarodichloranethane n-Butvlbenzene
Di b rcm::me thane l 2 Dichlorobenzene
Toluene I fBisl 2 Chloroisnnrnnvl Ether
l. l 2 Trichloroethane J/ l 2-Dibroon 3 Chloroornnane
Tetrachloroethene 1-nu,e.. 1 2 4-Trichlorobenzene
1.3-Dichloroornnane I). Hexachlorobutadiene
Dibroonchloranethane Nanhthalene
1.2-Dibraroethane IEOBl , l.2 3-Trichlorobenzene
1-Ch l orohexane
COlt!ENTS:
MDL -Hininun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification.
✓ -Re~ulated voe
T -Tr1halanethane
N.C. Division of Health Services
OHS 3068-0 (1/89 Laboratory)
µg/l
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STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HU!IAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611
Laboratory No. 9a 0 7'f9 PURGEABLE COHPOONDS Date of Analysis
COHPOOND µg/1 COMPOUND
Dichlorodifluoranethane u Ch 1 orobenzene
Chloranethane I Ethvlbenzene
v'Vinvl Chloride 1.1, 1.2-Tetrachloroethane
Braocmethane o-Xvlene
Chloroethane m-Xvlene
Trichlorofluoranethane o-Xvlene
✓1. 1-Dichloroethvlene Stvrene
Methvlene Chloride ' Braoofonn
tert-Butvl Methvl Ether /9,, '1 Is lbenzene
(Transl 1.2-Dichloroethvlene /) 1 1 2 2-Tetrachloroethane
Is 1 ether I Braoobenzene
l 1-Dichloroethane n-Prnnv]benzene
2 2-Dichlornnrnnane \Y 1.2 3-Trichlornnrnnane
(Cisl 1.2-Dichloroethvlene , 1-< 2-Chlorotol uene
Chlorofonn u 1.3.5-Tri,nathvlbenzene
fBCH) Braooch 1 oranethane i 4-Ch 1 oroto 1 uene
✓1 1 1-Trichloroethane I CTertl Butvl Benzene
1 1-DichlornnrnnPne I Pentachloroethane
✓Garbon Tetrachloride I 1 2 4-Tri,nathvlbenzene
✓Benzene I (Sec) Butvl Benzene
✓1 2-Dichloroethane ·J/ o-Isnnrnnvltoluene
✓Trichloroethvlene ii< 1,3-Dichlorobenzene
1 2-Dichlornnrnnane (.,\ ✓1 4-Dichlorobenzene
Brcrrodichloranethane I n-Butvlbenzene
Dibraocmethane I 1 2-Dichlorobenzene
Toluene I (Bis) 2 Chloroisonrnnvl Ether
1 1 2-Trichloroethane y 1 2-Dibraoo-3 Chloroornnane
Tetrachloroethene Ii< 1 2 4-Trichlorobenzene
l 3-Dichlornnrnnane /1 Hexachlorobutadiene
Dibraoochloranethane Naohthalene
1 2 Dibraooethane (EDBl 1 2.3-Trichlorobenzene
1-Ch 1 orohexane I
aJltENTS:
MDL -MininuTI Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification.
✓ -Re~ulated voe
T -Tr1halanethane
N.C. Division of Health Services
OHS 3068-0 (l/89 Laboratory)
µg/1
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STATE LAflOMTORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPART/1£Nl OF HUKAN RESOURCES
P.O. BOX 28047 -306 N. ~!LM!NGTON. ST., RALEIGH, N.C. 21611 .
ORGNH C CHEM I CAL ANAL YS IS
PURGEABLE CXJMPQJNDS LAB 00 O()fo I!,-/ qr,r,71,J
FIELD I I ;;;J.;J.(p L/-I ;}.;l v, 0-.
COMPOOND TYPE ( I ) l ) . ( l. ( l
UNITS uo/ll uo/kq f'"iJ<Vl)uo/ko uo/1 •·-/ko ··-/1 uo/ko
ch lororethane 10 A-k ' IA
bf"O'lOl'ethane ,,...,, '
dichlorodifluorarethane ., /
vinvl chloride ,o :-;:\c.J ·,
ch l oroethane ,n '' irethvlene chloride ,:; 1....-.-.rP
trichlorofluoronethane ''
ethene l. 1-<lichloro J-'1/
ethane 1. 1-<lichloro--1...U"" ... r' 0 ,..,
1.2-•. ;-<Ji ch 1 oroethene .:210 +,e1c.e..
chloroform (,,L, '~
ethane_ 1 2-<lichloro-I
ethane 1 1.1-trichloro-I
carbontetrachloride
brarodichloronethane
nrQJane. 1.2-<lichloro-
1.3--trans-<lichlo 'V ' I/
trichloroethvlene s,,9 -i-.r-n r o
ch 1 orod i b f"O'lOl'ethane LL-; I
benzene I -l-,n' e
ethane 1. 1 2-trichloro-; '
1 3-cis-<lichlo ne \ I
2-<:hloroethvl vinvl ether 10 I
brorofonn ,n I
ethane. I I 2 2-tetrachloro-"i ~ -.//
ethene tetrachloro-+,--~~ 0 +r.-1 r n '
toluene l,\__' I, .. t
chlorobenzene R
ethvlbenz,ene ' / .v ''
acetooe lo I, I
2-butanone ,n
ca rbood i SU 1 fide ,;
2-hexanone //)
~thvl -2~ntanone I f'1
stvrene "i
vinvl acetate ID '/
xvleneS /-Mal'> C: ,1 +-rne..L
E.;-h" I e+her I" Ll-""J,
-!'r-A I'll ,r
J -Estimated value.
K -Actual value is known to be less than valu,e given.
L -Actual value· is lnown to be greater than value given.
U -Material was analyzed for but not detected. The nuro,er is the 11ininun Detection Limit.
NA -Not analyzed.
1/ -Tentative identification.
fl -On NRDC List of Priority Pollutants.
N.C. Division of Health Services
· DHS 3068-0 (4/86 Laboratory)
I
( l ' ( l
..o/1 ""/ko 110/l uo/kq
;
I
I
I
I
S2mpling: Gener2 coi:"
!.2odf:i.J.l
ol•..c;·,y' s k,:,;eG___e._..f_Aa nA."'--'----",,!'-'--'Q=/_s;;e,,"""-____ Te.'L,::.;•c·,nc( ___ ._ .. __ ) _____ _
::if"-ess c?f?'a/4;o,,6 1 /1/C ~ ·
/ /.
oJ.}.ec::o::' s 1~2...m2_ ·c2A,..._...,.A /4 ~ .. . .. I ~~.,__ s i 671?. c c, :-e
"""' S=:c,iec ·y-ocT, /9'?0
}I= c.:f ? re: e S 5 Gener 2. ti,:, g ;,• 2 S .:e._~M=.ch:z·J;(:'-."::.L.h-"-'co"-<k-Va<:.--'n:.,__ _________________ _
ii:,_ c l :::: □=a c ion
A /I sqny/D s a c / di "b "-eol
I
I
::-oz.i,:; of Posses sioo:
2.
I·
l
C 6~9J
inclusive date!
s:i.gno.c.ur.e inclusive date
Comple::e c..ll 2pplic2.·01e inforc:c:iot, i11ciuC::i..n~ sig7l2cures, and
· subroir. \.:ic·n ·2.nc.lysis re~ues.: ro~s.
I ({s'.;,
N. C. Dcpartmcm of }-luman Resources
State Laboratory o( Public Healr
·1ivision of Health Services SAMPLE ANALYSES REQUEST P. 0. Box 2804
306 N. Wilmington Scrci
Raleigh, 276 I
.ite Number 9 .2 m -7tf3 A -Field Sample Number =/_,-r:;7?..,,-"-z;_,_r{-'.,___· _________ _
lame of Site GeJ /jq,-u La-I,:!;?/ Site l-oca;ion ,efcr / e, 9'. ,(,, AC,./
Collected By · -:-lc,c & ofdi/e?'i lbif'' ·"'2':;Z::: -,, ·oate Collected 5£ Oc,f;-/9 '10 Time // OS"
I ypc of Sample:
Environmental Concentrate
Comments
I v"" Groundwater (1) __ Solid (5)
___ Surface Water (2) __ Liquid (6)
~ / .2, C 6a ,,. I'. -e-ffe o u» U/ ,,0 //
I __ Soil (3) __ Sludge (7)
Other (4) ___ Other (8) r
INORGANIC CHEMISTR\'JllP
Extractable,
Total
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Res.ult, rog/1
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
....IL.. Arsenic
_L Barium
..Lcadmium
__ Chloride
./ Chromium
.L..o.ol
L'..Q,o:\:
.L..O.i::igS
Lo .Q\
-·-.. Silver ·"-0, . .:,5
__ Sulfates
__ Zinc
_Ph
__ Conductivity
I __ Mercury
__ Si.:1.cnium
__ Silver
__ Copper
__ fluorid,
__ Iron
_TOS
_Toe
v Lead .L..c ,QQSl
. __ Manganese
./ Mercury <a,i:1aa:J I
7 Nirra\e.
__ Sdemum L-o.oQ~ l.___ ___ _._____ ___ -1--__ _
I
I
Parameter
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX
----
Results mg/1
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results n:,g/
_EOB
... __ · Methoxychlor
_PCBls __ Toxaphene
__ Perroleum _2,4-D
__ Endrin __ 2,4,5-TP (sHvex)
__ Lindane --
'-
I MICROBIOLOGY
RADIOCHEMISTRY
,-------,-------------------,---~-i-------------~-----
P-!, ram Cc er
Parameter· Re.sults PCi/1
I --(MF) Coliform Colonies/lOOmls
--(MPN) Coliform Colonies/l00mls
I
__ Gross Alpha
__ Gross Beta
I Date Received ------------'---------Date Reporred
Date Extracted __________________ Date Analyzed -...,.-.,-,.,c-rr"crr-,-----;:'-',-----
I Reported By ___________________ Lab Number
nuc: 1.101 tQ,..,;* .. .-17/R'i)
~ ,_: I 9 I 72. , · ··1 ~
.,. C. Department of Human Resources
Division of Health Services
,✓::~,
i ;·.-•.\,
SAMPLE ANALYSES REQlJ cST
State Laboratory of Public Heal
P. 0. Box 280·
.1
306 N. Wilmington Str(
Raleigh, 276
Site Number 9 .2 {7J -7tfJ A -Field Sample Number _/_~~;p~·~7~9'~---------
l.ame of Site ... G-'-'r:..,e:;::.,,..,5..,.,,6, .... 0'.ukf="""'--'L=-=o"--'-l~e,,=--------Site l-oca1ion <%'£er/ e I 9'. /4 I # C /
Collected By Jqc ,K cf?u·f /er· '16'!{_' _·5':.._.f:~_· _ Date Collected 9 Oc f_ /9' o/,0 Time/, -JO
I ypc of Sample:
Environmental Concentrate
__ Solid (5) .
___ Liquid (6)
__ Sludge (7)
__ Ocher (8)
Comments
I V Groundwater ( 1)
___ Surface Water (2)
I
I
__ Soil (3)
__ Ocher (4)
Extraccables
.
I Parameter Results mg/1
__ Arsenic
__ Barium
I __ Cadmium
__ Chronoium
__ Lead
__ Mercury
__ Selenium
__ Silver
--
--
--
-----
Parameter Results mg/1
_P&T:GC/MS
__ Acid:B/N Exe.
_TOX
----
-
I
I
I
I
I
I
I
I
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
#/J, &mmexc,'a/ Ef«'if>&~d-f W,.,,,//
INORGANIC CHEMISTRY
Parameter Results mg/1
Y Arsenic .L..o,Qj
~ Barium L.o_a'-\
_L.cadmium L D-.s;:H:2 ~
__ Chloride
.,/ Chromium ..t_ 0 -ol
__ Copper
__ Flllorid,
__ lron
-./ Lead L.. o. 00'.;;:J
__ Manganese
./ Mercury <o,aaa~
7 Nitrace.
__ Selenium □~QQ '1
,
ORGANIC CHEMISTRY
Parameter
_EDB
_PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/ I
'
Parameter
__ Gross Alpha
__ Gross llcca
' :
Total
Parameter Results mg/1
/ Silver ..,t'...,__O:iQ~1
__ Sulfates
__ Zinc
_Ph
__ Conductivity ·
_TDS
_TOC
----
--------
Parameter Results mg;
_._ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Date Reported _______________ _
I Dace Received
Date Extracted _________________ _
I Reported By ___________________ Lab Number
OHS 3191 (Rc~·iscd 7185)
-. (""'.
.-i. C. Department of Human Resources _,·:
Division of Health Services
C0
SAMPLE ANALYSES REQ8°2ST
Seate Uborarnry of Public He:
P. 0. Box 281
306 N. Wilmington Sc
Raleigh, 27·
_9~2~r12"'-'-_-...,_7_t{J~A~----,------Field Sample Number ~l~,">"-&_e~o----~---
C,-e,[./icYi-f-! Lo /e,, Site }..oca,ion e'(q/e,9: ~ , MC,./
~ameofSite
· -=ollected By Jqc tf d?,«-j /e?"· ·10#" ·:9-,f:: .. Date Collected.?: Oc f_. /9' '/() TimeJ,'oo
l;r ypc of Sample:
Environmental Concentrate
Comments
I
V Groundwater (I)
___ Surface Water (2)
__ . Soil (3)
__ Solid (5) fl:/ & Ovedea.ol LJoor kt/r',,(/
I __ Other (4)
Extractables
· __ Liquid (6)
__ Sludge (7)
___ Other (8)
INORGANIC CHEMISTRY
Parameter Resu Its mg/ I Parameter Resu Its mg/ l
__ Arsenic .JL.Arsenic .L.O.o\
__ Barium ~Barium Lo.c.1-+
__ Cadmium ....LCadmium L O.QO~
__ Chromium __ Chloride
__ Lead ../ Chromium ,L. D -ol
__ Mercury
__ Copper
__ Selenium __ fluoride -
__ Silver __ Iron
--../ Lead L. □.005':
,
I
Total
Parameter Results mg/
__ Silver ..t...o .. a'7i
_·_ Sul faces
__ Zinc
_Ph
__ . Conductivity
_TDS
_TOC
--
--
I
I
I
I
I
I
I
I
I
I
I
----
. __ Manganese --
/ Mercury ~0. ~OQ ";} --
--.
··-
P.irameter Results mg/ I
_P&T:GC/MS
__ Acid:B/N Ext.
_TOX
----
MICROBIOLOGY
Parame.ter
__ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/lOOmls
--·
✓Nitrate.
__ Selenium 0 001
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB'.s
__ Petroleum
__ Endrin
__ Lindane
Results mg/ I
Parameter
__ Gross Alpha
__ Gross Beta
----
Parameter Results m1
__ Methoxychlor
__ T oxaphene
_2,4-D
--2,4,5-TP (silvcx)
--
RADIOCHEMISTRY
Re.suits PCi/1
Date Received -,----------~-------
Date Reported _______________ _
Reported By
Date Extracted __________________
Date Analyzed _______________ _
l.'19174_:;~-
-------------------
Lab Number
'~l--. . '
DHS }191 (R,vi"d 7/85) .
-•·· ''' > •.• ,v1 ••.• fD ... :,.,,.7/~/,
, <,:cc' /,:\~; I ~ -
•[.:~~->
N. C. Dcpanmcnt of Human Resources
Seate. Laborat0ry of Public Heal
,Division of Health Services SAMPLE ANALYSES REQUEST P, 0, Box 280·
I
306 N. Wi~mington Ser(
Raleigh, 276
Sice Number 9 2 rJJ -7tfJ A -Field Sample Number -:-'-/_S-:-'tf'"'--cf"'-"-j ________ _
lomeofSic• GeJtfQ'.ld& Lo-/e,, . Sice)_,ocarion e'(q/e,9:/2 , AC./
Collecced By 7crc& d?dr/e?.' 1b){_'·_·7:.,_,,,r~-· -Dace Collected '9 Oc-f../9' o/0 , Time.:Z,J:7
lypc of Sample:
Environmental Concentrate
Comments
I · V Groundwacer ( 1.)
___ Surface Water (2)
__ Solid (5) · · #/,j"': %7ne.-c_ kuc. I S/2<>.,-,o
1--Soil (3)
__ Ocher (4)
I l Extractables
___ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
.
I Parameter Resulcs mg/ 1 Parameter Results mg/ 1
__ Arsenic -k'.'.'.:.Arsenic Lo-cl
__ Barium ~Barium LO,Q~
Total
' ' '
Parameter
/ Silver
__ Sulfaces
I __ Cadmium _Lcad.nium Lo , ... ,o~ __ Z.inc
__ Chromium
__ Lead
I __ Mercury
__ Selenium
__ Silver
I ---
----.---
Parameter Results mg/ 1
_P&T:GC/MS
__ Acid:B/N Exe.
_TOX
----
I
I
I
I MICROBIOLOGY
Parame.tcr
I __ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
I
__ Chloride
/ Chromium Lo .o \
__ Copper
__ fluoride
__ Iron
.,,/ Lead LQ Q Q '::J
__ Manganese
./ Mercury 6-Oo o G
✓Nitrate.
__ Selenium ,,__ 0 ooe.i
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Pecroleum
_· _Endrin
__ Lindane
Re,ulc, mg/1
' '
Parameter
__ Gross Alpha
--Gross Bera
__ Ph
__ Conductivity
_T0S
_·_TOC
----
----
----
Parameter
__ Mechoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (si\vcx)
--
RADIOCHEMISTR y
Results mg/1
..t._o_o~
Results mg/
I Dare Received __________ ...c., _______ Dace Reported _______________ _
Dace Excracced
Date Analyzed ___ 77.TA-n--r,--a-,-,----,,-,-.,-----
:. 171 75 ~ 'h·
I Reporced By
Lab Number
, .., ,nr:,
·"'/ . ·.:_; _t;.t•,.··, /11/' .· .
. ' /
N. C. Department of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
Seate Laboratory of Public Hcah:
P .. 0. Box 2804
306 N. Wilmington StrCl
Raleigh, 2761 I
Site Number _C/'--"',2,_rJJ~_-_7~t?i~A~---,--------Field Sample Number ~/~,2.~;z.~7,~i<~~--------
. t•me o·f Site We-l/ictwt-Lo/ e-, Site location t?fq/ e,9: /2 , £,, C ./
Collected By Jqc & d'?et-f /t;,Y' Tb)!' '.z'::f:: · Date Collected?: Oc f /9' ?'o' Time
t ypc of Sample:
E7mental
I ___ Groundwater ( 1)
__ Surface Water (2)
I _._ Soil (3)
__ Other (4)
I Extractables
Concentrate
__ Solid (5)
___ Uquid (6)
-~ Sludge (7)
___ Other (8)
INORGANIC CHEMISTRY
I Parameter Resu I ts mg/ 1 Parameter Results mg/ 1
I
I
I
I
I
I
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
__ Lead
__ Mercury
____ Si.:lcnium
__ Silver
--
--
----
--
Parameter Results mg/1
v' p& T:GC/MS
__ Acid:B/N Ext.
_TOX
----
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter Results mg/ 1
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Comments
~11crnc11a1n. l"lf'"f\~1na.1
..,,.. • ,_,, "-..1'!1,.,1 UL\Jl 1Ul,,,
Total
Parameter Results mg/ 1
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC
--
------------
-
Parameter Results rng/ I
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
I MICROBIOLOGY
Pararne'ter Parameter
RADIOCHEMISTRY
Results PCi/1
I __ (MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
__ Gross Alpha
__ Qross Beta
. •~-----~~,-'-------
Date Received IO -'S' -<; 0 .f3 /) Date Reported . /o ·-:l. Ci -f o
I */)
Date Extracted __________________ Date Analyzed ID 15 '!O ·
f7e L__ /),, /J L--. 1 r 906776
Reported By T'f//1 ~/L-tt'v Lab Number ---------''-==---------
[\\I ~H.s 3191 (R,vis,o 7185) JF-906 77 C -9 0 ~ 7
I ""1.,J -,n,l H:11:irdous Waste (Review 7/87) S-.3
I. '• t: C. Depmment of Human Resources
Division of Health Services
State Laboratory of Public Hcalt
SAMPLE ANALYSES REQUEST P. 0. Box 2804
I
306 N. Wilmington Stre·
Raleigh, 2761
Site Number _9.~2~t22~--~Z~d]~~A~----:,-------Field Sample Number _/_,2._;L __ 7_7 ________ _
.. t.•me of Site .._C,.,_,--~e~...[~6,=<Y~kl:~-t-~~L=o~/_<~e,,~-------Site J.,ocation vk"q / e 12'. h 1 £ C, /
Collected By Jere,& d'i'.«7/&~'Ib)i ·5':5--::·· Date Collected 5:"0cf. /f<z'.0 Timc/,'05':
rypc of Sample:
Environmental Concentrate Cmnments
I V Groundwater (l)
__ Surface Water (2)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
~/ 2_ Char/,·e, Arou,u 11/~I/
I
__ Soil (3)
__ Other (4)
I Extractables
I
I
I
I
I
I
I
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chrow.ium
___ Lead
__ Mercury
__ S!.!lenium
__ Silver
--
. ----
--. --
Parameter
~&T:GC/MS
__ Ac1d:B/N Ext.
_TOX
----
Results mg/ 1
Results mg/ 1
INORGANIC CHEMISTRY
Total
Parameter Results mg/ 1 Parameter Results mg/1
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity ' __ Copper _TDS
__ Fluoride _TOC
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate --
__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ I Parameter Results mg/ I
_EDB __ Methoxychlor
__ PCBls __ Toxaphene
__ Petroleum _2,4-D
__ Endrin . __ 2,4,5-TP (silvex)
__ Lindane --
I r-_______ M_I_C_R_O_B_I_O_L_O_G_Y _______ _,_ __ -;-____ R_A_D_I_O_C_H_E_M_IS_T_R~Y~-----
Pararne"ter Parameter Results PCi/1
I __ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
__ Gross Alpha
__ Gross Beta
l~-----~~--.--
Datc Received _l_D_-_. -~-_-_q_o~B_J9.. __ -'--------Date Reported --------------''---
• Date Extracted ~;_o_--,~l--_,_~_o_8.cc...uJ~l-:r._wi ________ Date Analyzed _,_J~o'--;1.'-'-=3'---'9-'o'-"/3~,J=----------
Reported By _________________ Lab Number ____ 9_0_6_7_7_· _? _______ _
~, DHS 3191 (Revised 7185) I~· .SoliJ and H:nardous Waste (Review 7187)
I; C. Department of Human Resources
Division o( Heahh Sc:rviccs SAMPLE ANALYSES REQUEST
State Labor awry of Public Hcalt
P. 0. Box 280·1
I
306 N. Wilmington Sere
Raleigh, Z76i
Site Number _9~2~rJ2~-~Z~t!J~A~_-________ Field Sample Number _/_.2-_;z._7,~cf'~---------
-_ tame of Site ._r,,,--~r:~c'-'-,°"'~-.5=6,=-0'.~n="4=·~~L=Q~/_,~e.,~-------Site Location c:?fq / e 7, /2j fa C /
Collected Bv -:l;c .K cifcd7 /e?". \Ci# -•~'.z::_.,,_f: __ Dace Collected 'r Oc T,, /9' ')'tJ Time
Ir ypc of Samr!c::
Concentrate Cornmcnts
E7mental
I __ G~.Jundw~ncr ( 1)
__ Surface Water ( 2)
__ Solid (5)
___ Liquid (6)
___ Sludge (7)
___ Ocher (8)
#" / l, Co;n me-e'C-I q I .£~~---t We:,,//
I __ Soil (3)
__ Ocher (4)
I Extractables
I
I
I
I
I
I
I
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chromium
___ Lead
__ Mercury
____ Sl'.!cnium
__ Silver
--
----
----
Parameter
V"p&T:GC/MS
__ Acid:B/N Exe.
_TOX
--
--
Results mg/1
· Results mg/1
-
I MICROBIOLOGY
INORGANIC CHEMISTRY
Total
Parameter Results mg/1 Parameter Results mg/1
__ Arsenic __ Silver
__ Bnrium __ Sulfates '
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _TOS
__ Fllloridl! _TOC
__ Iron --
__ Lead --
__ }..,fonganese --
__ Mercury --
__ Nitrate --
___ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/]
_EOB __ Methoxychlor
__ PCB'.s __ Toxaphene
__ Petroleum _2,4-0
__ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
Parameter Parameter
RADIOCHEMISTRY
Re.suits PCi/1
I __ (MF) Coliform Colonies/!OOmls
__ (MPN) Coliform Colonies/lOOmls
Dace Received /0 -f"-9 0 13 ,&
__ Gross Alpha
__ Gross Bcca
Dace Reported ________________ _
Date Excracced __________________ Date Analyzed"17b/149tj/?1'i ·
______________ Lab Number · · 906??8
Reported By
OHS 31 91 ( Revised 7185)
• • • •• ' • \VI ••• ~ 10 ... :.,,. 7/A;,
1: C. Dcpanrnent of Human Resources
Division o( Health Services SAMPLE ANALYSES REQUEST
State L:'lbor:uory of Public Hc:llt
P. 0. Box 2804
306 N. Wilmington Strc•
Raleigh, 2761
I
Site Number 9 2 cJ2 -/ cfJ A -Field Sample Number _,_/_,,2=7-,'-'--'--7_,__f _______ _
0,c,,JkO'.kfd.-LO} e,, Site Location cfq/ e,9: /2 , /0 C /
~nmt! of Site
'l:ollected By
' . /2 ~
~c /4: dfw?' /e,.:,-[[li/ _··.L.9:~f:'---_· _ Date Collected 9 Oc T~ /9' o/0 Time /, '.JO
f ypc of Sample:
Environmental
~ Ground"·atcr (I)
I __ Surface Water (2)
__ Soil (3) I __ Othet (4)
Concentrate
___ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Othet (8)
Co1nments
I
INORGANIC CHEMISTRY
Extractables
Parameter I 1--Arsenic
I
I
I
I
I
I
__ Barium
__ Cadmium
__ Chrordum
___ Lead
__ Mercury
____ Selenium
--Silver
--
--
--
--,
--
Parameter
~&TGC/MS
__ Ac1d:B/N Ext.
_TOX
----
Results mg/ 1
Results mg/ l
'
-
Total
Paran1etcr Results mg/ 1 Parameter Results mg/ l
__ Arsenic __ Silver
__ Barium __ Sulfates
..
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _TDS
__ Fluoridf! _TOC
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate ' --
__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ I
_EDB __ Methoxychlor
__ PCB:s __ Toxaphene
__ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
I ~-------M_IC_R_O_B_I.c_O_L_:O_G_Y ____________ .:._ __ R_A_;D_I_O_C_H_E_M_IS_T_R_Y~-----
Parametcr
I __ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
Parameter Results PCi/1
__ Gross Alpha
__ Gross Bera
•--------'---~-----
Dace Received /O-S--70 f3JSJ .
I Date Extracted /0-lt.-'i O 11M_i -ve "'vJ
Reported By I DHS 319\ (R,vised 7/65)
Date Reported ________________ _
Date Analyzed _,/c.:ac..,_,-.)."'-"3'---=9o-'--_,8"-£1-=----------
Lab Number ____ 9_0_G_?_?_9 _____ _
,::, .. 1;,I .. ~.l u., . .,,,-1,.,.,~ \V:istc (R~Yicw 7/87)
:</ .1··.·.
/( ... ~-Deparrm,n: or Hu,nan Rosoucces
State Laboratorv of Public Hca\r:
Division of Heal,:, 5miccs SAMPLE AN AL YSES REQUEST P. 0. Box 2804
I
306 N. \Vilrnington Scree
Raleigh, 2761
Site Number _0-'--i--"_"-7 --"rJ)""-_-~T'----'<f1<-L--"A---"----~------Field Sample Number _/_2_;:?.... __ @._V _________ _
tame of Site -C:::;-.o,J.{CY,-frt LO I e,_,, Site Loca;ion t1/t'q j e j?:.b_;) fa c/
Collected By ;J';c & df'er://,e,;,-' ![>;';' _··~2:_.,_T __ Date Collected :f': Oc 7,_ -/9' 'z(] Time .2/?0
lypc of Samr•!c:
Concentrate Con1ments
Envir,9,nmencal
---,, ... , ..... , ___ I VG··.•· -'·-·at"r ( 1) ___ Solid (5)
___ Liquid (6)
___ Sludge (7)
___ Other (8)
~/½ Oved.e.,:;v;L_,£1oac M=~~~r1/-'----
___ Suri,ce Water (2)
1 --Soil (3)
__ Other (➔)
I Excractables
I Parameter
__ Arseni..:
__ Barium
I __ Cadmiucc,
__ Chrorr-.ium
__ Lead
__ MerCl.!r·:·
I ____ Si:li:niur:i
__ Silver
--
----
I------11--
I
I
I
I
Parameter
.......-P&T:GC/MS
__ Acid:B/N Ext.
_TOX
--
--
Results mg/ 1
Results mg/1
-
INORGANIC CHE 1ISTRY 1,
Total
Parameter Results mg/ 1 Paran1eter Results mg/1
__ Arsenic __ Silver ..
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _TDS
__ fluoride _TOC
__ iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate --
__ Selenium --., ___
·-·-·
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1
_EOB __ Methoxychlor
__ PCBls __ Toxaphene
__ Petroleum _2,4-D
__ Endrin __ -2,4,5-TP (silvex)
__ Lindane --
1.--______ M_IC_R_O_B_I_O_L_O_G_Y _______ -.---_______ R_A_D_I_O_C_H_E_M_IS_T_R_Y~-----
Parameter
I .. __ (MF) Coliform Colonies/ lOOmls
__ (MPN) Coliform Colonies/lOOmls
Parameter
__ Gross Alpha
__ Gross &ta
Re.sults PCi/1
•'----------------'------c----c-----
I Date Received / 0 ~ ~-9 c) B ;,9. Date Reported
Date Extracted------------------Date Analyzed l}o~l1shocJ111 -

·

. I I ~0678' I Reported By Lab Number • · . -0
OHS 3191 (RC'vi5~d 7185)
, .C Depar:m,nt of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
Stace Laborat1..>ry of Public Hc:ih
P. 0. Box 2801:
I
306 N. \'(./i\mingrnn Sere
Raleigh, 2761
Site Number _9~~~7~(/J~--~Z~tf1~-"A~-----,-------Field Sample Number _ _,./_2_:J._P'.__,/ _________ _
t ame of Site .,_C,..,__<-,--"'""'-",--f,._,{=D'.=n.,,t._..cL=o-c....c/_,-'e,;=-------Site location t1/?q / e '9-h , # C, / . :;r~
Collected By ~c /( dfe17 /er ·1c1ii _·_,.7_.,_f: __ Dace Collected 'r Oc /,, /9' o/0 Time .Z,'oo
Ir ypc of Sample:
Environmental Concentrate Coin men ts
I ~ Ground'-llcr ( 1)
__ Surface \Vacer (2)
__ Solid (5)
__ liquid ( 6)
__ Sludge (7)
__ Other (8)
'i¢/½ Ov~Y4~Llah.~~-~k6=~,µ_ ___ _
I __ Soil (3)
__ Other (4)
Extractables
I
I Ii Parameter
: __ Arsenic
I •
I
I
I
I
I
I
, __ Barium
/ __ Cadmium
i __ Chromium
j ___ Lead
' __ Mercury
______ St.:lcnium
__ Silver
--
----
--,
--
Parameter
~&TGC/MS
__ Ac1d:B/N Ext.
_TOX
----
Results mg/ I
Results mg/ 1
a
-
lNORGANJC CHEMlSTRY
Total
Parameter Results mg/ 1 Paran1etcr Re~ults mg/1
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zir1c
__ Chloride _Ph
__ Chromium --Conductivity
__ Copper _TOS
__ F\uoridr: -_TOC
__ Iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate --
__ Selenium --
ORGANIC CHEMJSTRY
Parameter Results mg/ 1 Parameter Results mg/:
..
_EDB __ Methoxychlor
__ PCB's __ Toxaphene
__ Petroleum _2,4-0
__ Endrin __ 2,4,5-TP (si\vex)
__ Lindane --
I MlCROBIOLOGY RADIOCHEMJSTRY
~-----------__.:._:..._c ______________ _.:_ ___ --'-'------~-----
Parameter I --(MF) Coliform Colonies/ lO0mls
__ (MPN) Coliform Colonies/ l00mls
I
Parameter
__ Gross Alpha
__ Gross Beta
Results PCi/ 1
I Date Received -L~V_-_-s_·~y_O_=B=JJ.--~-------Date Repotted _______________ _
Dace Extracted /0-/6-90. v,,t-1/p Nw ~ ..J I Reported By
!?HS 3191 (Re-vised 7/85)
Date Analyzed -"-/~o'----.l-=-3_--"-9_0___,_,l3"'-'--'&'---------
Lab Number ___ 9_0_6_7_8_1 ______ _
•v• .. rn. ,;_,., 7 /07\
I .·.
1~. C. Department of Human Resources
Division o( Hea!ch Si!rdces SAMPLE ANALYSES REQUEST
Srntc Laboracory o( Public Hcali
P. O .. Box 280~
306 N. Wilmington Strc
,Raleigh, 276i I
Site Number 9 2 rJ2 -TtfJ A -Field Sample Number __,_/_2-'-2__,c?_=-,,J'"""', _________ _
lame of Site ,_C,_,_,-L...;,""'-'-,-Jc..6'aw-O'.un~""a-~-=L=o-~/_<_e,,=-------Site Loca;ion ~q / e !J>' h_j ft C, /
Collected By J;c ,K dfet-/ /e,r• lOil _··..L7---..L.5l-__ Date Collected 5:': Oc 7,. /9' <j'{] Time l ✓'J {)
Concentrate Comn1ents
__ Solid (S)
__ Liquid (6)
___ Sludge (7)
__ Other (8)
"#/_r;: iv,,,,Y,..!!f kuc& SA.otf' ~
1 --Soil (3)
__ Other (4)
I Extractables
I Parameter
• __ Arsenic
I
I
I
I
I
I
__ Barium
__ Cadmium
__ Chron:ium
__ Lead
__ Mercury
____ Sl'.lcnium
__ Silver
--
--
--
--
Parameter
v'p&T:GC/MS
__ Acid:B/N Ext.
_TOX
----
Results mg/1
Results mg/ 1
.
-
s INORGANIC CHEMI TRY
Total
Parameter Results mg/1 Parameter Results mg/1
.
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conduccivicy
__ Copper _TDS
__ Fluo:-id~ _TOC
.
__ lron --
__ Lead --
__ i1anganese --
__ Mercury --
__ Nirrace --
__ Selenium --
ORGANIC CHEMISTRY
Parameter Results.mg/! Parameter Results mg/ 1
_EDB __ Methoxychlor
__ PCB's __ Toxaphene
__ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
I ~------M_IC_R_O_B_I_O_L_O_G_Y _______ ~ _______ R_A_D_I_O_C_H_E_-M_IS_T_R_Y~-----
Parameter I --(MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/ IOOmls
Parameter
__ Gross Alpha
__ Gross Octa
Results PCi/ 1
•~--------'--------,---,-----
I Da tc Received
Date Extracted __________________ _
I Reported By
DHS 3191 {Rev;sed 7185)
Date Reported _________________ _
Date Analyzed v0fol 1s l20'.':t'flri1 .
Lab Number I
1
' ~06782
--, 10-,,
IL C Dcpanmen( of Human o.,:sources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Heal:
P. 0. Box 280,
306 N. Wilmingron Srrc
Raleigh, 276 i I
Site Number _C/'--=.2'--'C}><L--_-_,_7_...t!J.L..C.A__,,c...· _______ Field Sample Number _/_Z_,2....,J"'---"3"----------
~.1me of Sire
'tollected By
0,o,J tfr/k(d Lo/e-, Sire)...ocation ,:?'i?q/e.,9-j, , AC./
. . ,%7
:Tc:-,ctf dfet-f/er· 0lC>ii ·7:f-:. Date Collected 5L0c T,. /9'jt(J Timc2/.]0
f ypc of Sample:
Environmental Concentrate Comn1ents
I _ V Groundw3.c~r ( l)
__ Surface Water (2)
·--Solid (5)
__ Liquid (6)
__ Sludge (7)
___ Other (8)
H:/S: k/47 _kl.e,_!______L,-uc.l: (/4117 W&,,,,,J/---
I
__ Soil (3)
__ Other (4)
I Extractables
I
I
I
I
I
I
I
Parameter Resu Its mg/ 1
__ Arsenic
__ Barium
__ Cadmium
__ Chrorr.ium
___ Lead
__ Mercury
____ Selenium
__ Silver
--
--
--
--,
--
Parameter Results mg/1.
::),'.& T GC/MS
__ Ac1d:B/N Exe.
_TOX '
--
--
-
I MICROBIOLOGY
INORGANIC CHEMISTRY
Total
Parameter Results mg/ 1 Parameter Res;,lts mg/!
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _TDS
__ F\uoridi! _TOC
__ iron --
__ Lead --
__ Manganese --
__ Mercury --
__ Nitrate. --
__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/1
_EDB __ Methoxychlor
__ PCB'.s __ Toxaphene
__ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
RADIOCHEMISTRY
Parameter Parameter Results PCi/1
I __ (MF) Coliform Colonies/ IO0mls
__ (MPN) Coliform Colonies/ l00mls
__ Gross Alpha
__ Gross Beta
•~---------'--~,-------
Date Received / 0 -J • 9 CJ M.
Date Extracted fO-/,fz-9,Q. ll");~ NW
Reported By
OHS 319 I ( Revised 7185)
c .. 1:.I ~--l U~~~-.-1,..,.,~ \YJ,.~rr (Rt".vicw 7/87)
Date Reporred ________________ _
Date Analyzed ~f_0_-_2~3=-c-cc-9=o..c13=--,d:!'-·-----'----
9Q6783 Lab Number ________________ _
DIVISION OF E.S-.LT:: S:C:?,\'IC:C:S
I
I
SOLID Ll.,c) ll..'-..U..PJ)OUS i-:ASTE uJ-J;;_G::>-8': 3,.iYC2
I
__ Storage Facility
✓ Ocher: #n i:nou,,n
~I~ .o: Process Gener~t:0:ig
:: _!,_-.le ID.io:.wc.r.ion
I
I
I
S=ple No. /--2,? 7 6"
c1.iri. of Possession:
/.22:77
l~~
• ~ signar:ure
signature
signature
I
Dis;)osc:.l ?2cility __ l.2ndfill
Telephone( ___ ) ________ _
Time S=pled /, '00 -.2 ,-JO cf',, ./'1,,
lie
/ ..2.,,2.J) .2..
tit.le inclusive dates
r.i:.~e inclusive dates
dc.ce
Is;:: :-uc .:ions: Complete 2..ll 2ppliccble infon::::c:io-;-, incluCin,; sig:12tures> ,and
-suDmit \.:id1 ·2n2.lysis reques.:: fo:-=:s.
I
I BASE/NEUTRAL ANO ACIO
EXTRACT ABLES
OJMPOUNO
nitrosodimethvlamine
bis(2-chloroethvllether I '-"hloroohenol
henol
.3-dichlorobenzene
1
4--<Jichlorobenzene
2--<Jichlorobenzene
is(2-chloroi llether
hexachloroethane l"i troso...<Ji -n~r,.,,vlami ne
trobenzene
i c.rnhorone
I nitroohenol
4--<Jimethvlohenol
s(2-chloroethoxv1methane
2 4--<Jichlo~henol
E-4-trichlorobenzene
hthalene
hexachlorobutadiene
t;hloro-m-cresol
achlorocvcl~ntadiene
2.4.6-trichloroohenol
1
-chloron•nhthalene
en>nhthvlene
imethvl ohthalate
2.6...<Jinitrotoluene
en>nhthene
4--dinitr,.,,henol
2 4--<Jinitrotoluene It" i trooheno 1 uorene
4-chlornnhenvlohenvlether
1
iethvl ohthalate
6...<Jinitro--0-<:resol
iohenvlamine
azobenzene
-b~henvlohenvlether
xachlorobenzene
=ntachlor,.,,henol
enanthrene
thracene
ibutvl ohthalate
1 uoranthene
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTl1ENT Of HUIIAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC OlEMICAL ANALYSIS
LAB NO -qnt,,7--,-, , , q ~06,7Y/ ~ob7fl3
FIELD# /.:l.J.77 I :i..:J 7'1 /.J.:J...QJ I .:Z. .:J. 5i' 3
TYPE r i I I l < I l ( I l
UNITS ,.n/) .......... uo/1 1--'-'---r,,,,,1......_ ·,,n/1 n:n:7W'n
/,ii ,:>A I I,( ,-,c -I.,(__
,
$f1h,_,,.O
/t,l?':IO
""a~ro
roh1:to
.I.
'l"O ,,, ,.
J·
I I"' ""'O
J•h•"•
S-OIP-~
IA F '"'"
' /
m1)L I
J -Estimated value. /1,.0/SOII-
( l
..n/) ,.n/ka
t-Actual value is known to be less than value given. -Actual value is known to be greater than value given.
-Material was analyzed for but not detected. The nlll"ber is the Mininun Detection Limit. m'])L ----Not analyzed.
1/ -Tentative identification.
'
/ -On NROC List of Priority Pollutants .
. C. V-<.v-W-<.on 06 He.al.th SVtv-<.c.u Is 3068-0 (4/86 Laboll.a..t.o~y)
-
( l
.. n/ 1 .. n/ka
-·
.
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I
STATE LABORATORY Of PUBLIC HEALTH
OIVISIOH Of HEALTH SERVICES, N.C. OEPARTMENT Of HUIIAH RESOURCES
P.O. BOX 28041 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC OlEMICAL ANALYSIS
BASE/NEUTRAL ANO ACIO lA8 NO q/)/,,777 '-fOu,77'1 '16&7~1 "'0 /,,7 fl "'
EXTRACT ABLES FIELO # /;J.;). 77 1-,;;_7q /.1.:l.X I I,..?.;;. x "1
aJl1POONO TYPE < I l r / l r / l C I l
UNITS un/1 •--"n/1' 11n/l' .,. uQ/1),,,.,,,,,.,
nvrene 10/:Hn (;<_. I.A.-i.,<.... u.__
benzidine <"",, /JI. c; 0 i,C
butvl benzvl ohthalate JO/ :,:io I ;;i._
benzCalanthracene ,_,,__
chrvsene . ·.
3. 3-di ch lorobenzi dine SO' u .. ,;;o,
bis(2-ethvlhexvllnhthalate ,,,,I i.3n
di-n-octvl ohthalate 10/.s~O
benzoCblfluoranthene so /11!.-rt.
benzo(klfluoranthene .
benzo(a)nvrene
indeno( 1 2.3-cdlnvrene
dibenzo(a hlanthracene , ,. , ,
benzo(n h. il=rvlene \ , ' I
ani 11 ne ... ,, ,., (.,(_ ~ (;<.._ U--
benzoic acid
benzvl alcohol
4-chloroaniline ... ,
dibenzofuran '"/=,11
2-<rethvln•nhthalene
2-<rethvlohenol
4-<rethvlohenol '" 2-nitroani 1 ine S'oht,,,;o
3-nitroani 1 ine
4-nitroaniline
2 4.5-trichlo~henol "' ' ' \
m1H ...
J -Estimated value. Ha.0/ St'JIL:
K -Actual value is known to be less than value given.
L -Actu.,1 value is known to be greater than value given.
U -"-'terial was analyzed for but not detected. The nunber is the Hininun Detection Limit.
NA -Not analyzed.
1/ -Tenl.dtive identification. £1 -On NROC List of Priority Pollutants.
N. C. D.{.V.(.6.(.0>! 0 6 He.aLth SVtV.{.Ce/2
OHS 3068-0 (4/86 Labowo~yl
( ) ( l
.. n/1 ·ua/kq ua/ 1 un/k<
.
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I,
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I
STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611 tJt; &, 77t.? PURGEABLE COMPOUNDS Date of Analysis Laboratory No,
COMPOUND µg/1 COMPOUND
Dichlorodifluoromethane IA Chlorobenzene
Ch loromethane Ethvlbenzene
"1/invl Chloride l l l 2-Tetrachloroethane
Braranethane o-Xvlene
Ch l oroethane m-Xvlene
Trichlorofluoromethane o-Xvlene
✓1 l Dichloroethvlene Stvrene
Plethvlene Chloride Brorofonn
tert-Butvl Plethvl Ether I !benzene
(Transl 1.2-Dichloroethvlene l. 1.2.2-Tetrachloroethane
Is=~ul ether Brorobenzene
l. 1-Dichloroethane n-P~"lbenzene
2 2-Dichlo~~ane ·,
(Cisl 1.2-Dichloroethvlene II<
1.2. 3-Trich loroorooane
2-Chlorotoluene
Chlorofonn ' ' 1.3.5 Trimethvlbenzene
(BCMl Branochloromethane 4-Ch l oroto l uene
✓1. l. I-Trichloroethane CTertl Butvl Benzene
l 1-Dichlo ne Pentachloroethane
✓Carbon Tetrachloride 1.2 .4-Trimethvlbenzene
✓Benzene rsecl Butvl Benzene
✓l.2-Dichloroethane D-I !toluene
✓Trichloroethvlene _17. '/ l 3-0ichlorobenzene
l 2-Dichlor~r=ane ,, ✓l.4-Dichlorobenzene
Branodichloranethane n-Butvlbenzene
Di braranethane 1.2-Dichlorobenzene
Toluene ' (Bis) 2 Chloroi l Ether
l l 2-Trichloroethane "("~J/1 ~ 1.2-Dibroro-3 Chloroorooane
Tetrachloroethene l 2 4-Trichlorobenzene
1.3-DichloP"rV"'lrl'V'loane Hexachlorobutadiene
Dibranochloromethane N•nhthalene
1.2-Dibranoethane fEDBl l 2.3-Trichlorobenzene
1-Chlorohexane
COIIMENTS:
MDL -MinillUTI Detection Limit for water (EPA Plethod 502.2), is 1.0 µg/1.
J -Estimated value. K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed,
1/ -Tentative identification.
✓ -Re~ulated voe
T -Tr1halanethane
N.C. Division of Health Services
OHS 3068--0 (l/89 laboratory)
µg/1
IJ '
I
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I, ,v
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STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611
Laboratory No. z?o c:;:;, 77g PURGEABLE COMPOUNDS Date of Analysis /~~,be
COMPOUND µg/1 COMPOUND
Dichlorodifluoranethane . Ch l orobenzene
Ch 1 oranethane Ethvlbenzene
v'Vinv] Chloride l l l 2-Tetrachloroethane
Bl"Clllmethane n-Xvlene
Chloroethane m-Xvlene
Trichlorofluoranethane o-Xvlene
✓l 1-Dichloroethvlene Stvrene
Hethvlene Chloride Branofonn
tert-Butvl Hethvl Ether I lbenzene
'Trans' 1 2-Dichloroethv]ene 1-1.2.2-Tetrachloroethane
I 1 ether Branobenzene
l 1-Dichloroethane n-Proovlbenzene
2 2-Dichlo--ane 1 2 3-Trichlo--ane
'Cis' l 2-Dichloroethvlene 2-Chlorotoluene
Chlorofonn l 3 5-Trimethvlbenzene
IBCH' Brarochloranethane 4-Chlorotoluene
✓l -1-1-Trichloroethane ITertl Butvl Benzene
1 1-Dichlo ne Pentachloroethane
✓carbon Tetrachloride 1 2 4-Trimethvlbenzene
✓Benzene ISec' Butvl Benzene
✓l 2-Dichloroethane D-I ltoluene
✓Trichloroethvlene 1 3-0ichlorobenzene
l 2 Dichlor=-ane ✓l 4-0ichlorobenzene
Branodichloranethane n-Butvlbenzene
Dibl"Clllmethane I 1 2-Dichlorobenzene
Toluene !Bis\ 2 Chlorois l Ether
l l 2-Trichloroethane I l 2-Dibrano-3 Chlo--ane
Tetrachloroethene I 1.2.4-Trichlorobenzene
1 3-Dichlo-r-ane Hexachlorobutadiene
Dibranochloranethane N•nhthalene
1 2-Dibranoethane IEDB' -1 2 3-Trichlorobenzene
1-Chlorohexane -
MDL -Mininun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification,
✓ -Re9ulated voe T -Tr1halanethane
N.C. Division of Health Services
OHS 3068-0 ( l/89 Laboratory)
µg/1
ll
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STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTPIENT OF HUIIAN RESOURCES
Laboratory No.
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611 /,,, /i <i.J/
7 tJtJ6 7JD PURGEABLE COMPOUNDS Date of Analysis~
COMPOUND µg/1 COMPOUND
Dichlorodifluoranethane I, Chlorobenzene
Ch l oranethane Ethvlbenzene
v'Vinvl Chloride 1 1 1 2-Tetrachloroethane
Brononethane o-Xvlene
Chloroethane m-Xvlene
Trichlorofluoranethane o-Xvlene
v'L 1-Dichloroethvlene Stvrene
Hethvlene Chloride Branofonn
tert-Butvl Hethvl Ether I ]benzene
'Transl l 2-0ichloroethvlene l.1.2.2-Tetrachloroethane
Is~~uJ ether Branobenzene
11-0ichloroethane n-P~0 lbenzene
2 2-0ichlo--ane 1 2.3-Trichlo--ane
ICisl l 2-Dichloroethvlene . 2-Chlorotoluene
Chlorofonn IK 1 l. 3. 5 Trimethvlbenzene
IBCHl Branochloranethane I l 4-Chlorotoluene
✓1 1 1 Trichloroethane (Tertl Butvl Benzene
l. 1-Dichlo ne Pentachloroethane
✓carbon Tetrachloride 1.2.4-Trimethvlbenzene
✓Benzene (Sec) Butvl Benzene
✓1.2-Dichloroethane o-I !toluene
✓Trichloroethvlene l 3-0ichlorobenzene
1 2-Dichlo -ne vl.4-0ichlorobenzene
Brcrrodichloranethane n-Butvlbenzene
Dibrononethane 1.2-Dichlorobenzene
Toluene (Bis) 2 Chloroi 1 Ether
1 1 2-Trichloroethane 1.2-Dibrano 3 Chlo--ane
Tetrachloroethene 1 2 4-Trichlorobenzene
1.3-Dichloroorooane Hexachlorobutadiene
Dibranochloranethane N•nhthalene
l.2-Dibraooethane IEDB) I. l 2.3-Trichlorobenzene
1-Chlorohexane -II
COl'l!ENTS:
MDL -Hininun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given. L -Actual value is known to be greater than value given. U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification.
✓ -Re~ulated VOC T ~ Tr1halomethane
N.C. Division of Health Services DHS ·3068-0 (1/89 Laboratory)
µg/1
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STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF .HEALTH SERVICES, N.C. DEPARTPIENT OF HUMN RESOURCES
Laboratory No.
P.O. BOX 28047 -306 N. WILMINGTON ST, RALEIGH, N.C. 27611 , .~ /; ,:/ j On
fc,7 4z Z'J,:;J..._ PURGEABLE COl1POUNDS Date of Analysis ~
COl1POUND µg/1 COl1POUND
Dichlorodifluoromethane J Chlorobenzene
Chloromethane Ethvlbenzene
v'Vinvl Chloride 1. 1. 1.2-Tetrachloroethane
Brananethane n-Xvlene
Chloroethane m-Xvlene
Trichlorofluoromethane o-Xvlene
v'l. 1--0ichloroethvlene Stvrene
Methvlene Chloride Braoofonn
tert-Butvl Methvl Ether I ]benzene
ITransll.2--0ichloroethvlene 1. 1.2.2-Tetrachloroethane
I 1 ether Braoobenzene
1 1--0ichloroethane n-P....-.nv 1 benzene
2.2--0ichlornnrnnane 1 2 3-Trichlo ane
!Cisl 1 2-Dichloroethvlene 2--Chlorotoluene
Chlorofonn 1 3 5-Trimethvlbenzene
IBClll Braooch loromethane . 4--Chlorotoluene
v'l 1.1-Trichloroethane ITertl Butvl Benzene
1. 1--0ichlo.-nnrnn<>ne Pentachloroethane
v'Garbon Tetrachloride 1 2.4-Trimethvlbenzene
v'Benzene (Sec) Butvl Benzene
v'l 2-Dichloroethane D-I ]toluene
v'Tri ch loroethvl ene 1 3--0ichlorobenzene
1.2-Dichloroornnane v'l.4--0ichlorobenzene
Brooooichlorarethane n-Butvlbenzene
Di braranethane 1 2-Dichlorobenzene
Toluene (Bisi 2 Chloroi ·•1 Ether
1. 1 2-Trichloroethane I 1 2-Dibraoo-3 Chlo~~ane
Tetrachloroethene I 1 2.4-Trichlorobenzene
1.3-Dichlornnrnnane I Hexachlorobutadiene
Dibraoochloromethane N•nhthalene
1.2-Dibraooethane (EDB) 1 2 3-Trichlorobenzene
1--Chlorohexane I
CXlllEHTS:
MDL -Hininun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected.
NA -Not analyzed.
1/ -Tentative identification.
v' -Resulated VOC T -Tr1halarethane
N.C. Division of Health Services
OHS 3068--0 (1/89 Laboratory)
µg/1
,l,L.
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SOLID
DIVISION OF
L',!) l'_',.L.,_RDOU S
( . -.
Cne iD 0£
!:...S'..LT:: S:C:?.\'IC::S
\.,'AST£ :-'.;.J~;._c::::-;~T. 3?._.'..J~C:: ,-·---. ;'--.
I
SM/er~nt/
B2z2rdous ~asce ~aceri21!s ___ ~~~------
Sampling: te.I:et~Loi·
·---··
I
S2!1ple No. /,52,_s-7-
:li_n. of Possession:
·L,0ie, cL ~// ,/'
c■---_ · . sign2 Lure
Ell J/ / £ ,M 9' . /,:;? J u-n-...e--/ f' cf I
--~~~-t-.;--<'.~-~-.-e----_ c_ inc~usi,;re Gc.te.s
-I v~~~ inclusive datii
.I---'---------signc.r.ure inclusive d2.ce£
· Complete c.ll 2pplic2Dle infon=c:io;-; inciuCini; sig7"'12c.ures, end
· submit '-'it.ii ·..=.nc.lysis req·...ies-;:: fo::-:::s.
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N.C. {?cpartment of Environment,
I Icahh, & Natural Resources
Solid Waste Management Division
S;V'.'PLE ANALYSIS REQUEST --:. Stale Laboratory of Public Hca1thC/=
( ·P.O. Box 28047, 306 N. Wilmington Slrcet •._ .. _
Raleigh, North Carolina 27611
Sile Number f 2. £J -/AA· Field Sample Numbcr--'/~C_..Z..-,-0_Z ________ _
NamcofSil"67~sit½f /«,,(~ 1/d, l'~#){~C'a~ t?(Cf/~,y:4_,. fl C ./ ..
Collcclcd By ~e,/t dJ#-f'/e-v ID# 'T,Y.-Dale Collcctcd/C/Ju>-1~ /9'fft,6&\V~O:
Agency: Hazardous Waste ----Solid Waste ,_/ Supcrfund . TCLl>f€omiod~~1 ·
Sample Type Inorganic Com~Y~ffls v'Jt"e's'~ff (mg/1)
Environmental Concentrate Comments ,./ Arsenic L..o.o\
. ✓ Barium Q.SR
__ Groundwater (1) _Solid (5) /-,tf/q,r So,/ v Cadmium L.. Q-oB
7 ....,, Chromium L..Q.)Q
__ Surface water (2) Liquid (6) ..,.L. Lead LQ•!:i □
<./"soil (3)
../ Mercury L. o.c:i...
_ Sludge (7) ..L.. Sclcoium .L. o. oo=i
.../Silver Lo;. ~Q
Other ( 4) Other (8) ------
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter R·esults~(mg/kg) Organic Compounds Results(mg/1)
_P&T:GC/MS / Arsenic L. ;;)__ benzene
""7 Barium
--
_ Acid:B/N Ext. '-i \ carbon tetrachloride
"7 Cadmium --
MTBE .,,_ \ I,,, chlordane
------.. Chloride chlorobcnzcnc
----
/ Chromium -'-.;.o chloroform
----
--__ Copper o-crcsol --
Fluoride m-crcso!
------
--Iron p-cresol
--/Lead 31 cresol --
--__ Manganese --1,4-dichlorobcnzenc
--./ Mercury L.O.o9 --1,2-dichloroclhanc
--Nitrate __ 1,1-dichlorocthylenc
/ Selenium ..L.. \ 2,4-dinitroto luene
✓ S ii vcr
--.,_ .-.o __ heptachlor
Radiochemistry Sulfates hexochlnrobcnzcnc ----
·-···········-·-··-· Zinc hexachlorobutadicne ----
P~1rametcr Results (l'Ci/1) pH hcxochloroethane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nilrobcnzcne
----TOC __ pentachlorophenol ----__ pyridine
Microbiology --__ telrachlarocthylene
--_· _ Lrichloroethylene
Parameter Resulls (Col/lOOml) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichlorophenol
----__ vinyl chloride
cmlrin --lindanc --
0;1tc Rcci..:ivt.:<l Reporleu by --rnclhoxych!or
__ toxophcnc
Datc Ext r:.idc<l Dale Reported 2,4-D --2,4,5-TP (Silvcx)
Dale Analy1.cd Lah Number --
C:l'IJR'JE p ·;· ' r, 0119~0 Jli,i.,.91
I. :-:.C. Department of Environment,
l lcal1h, & N.ilural Resources
Solid Waste Management Division
SA •-·~LE ANALYSIS REQUEST ., ,_ .. State Laboratory o( Public Hcahh.
:.;~.;Ir.o. Box ~7. 306 N. Wilmingt~n Street·,.
··· · · Raleigh, Nonh Carolina 27611
I Site Number '1 2 ti} -7 d?A Field Sample Number_/_b--'---2----''""-f:~2=·"'--. _______ _
Name of Sit0:t-c<..rlam /cr;fr:!-1,.,c/, I'};,/!){~ {t/4fa~ tff Cf/c,y4_,, fl C /
I Collcctcd By ~c/t dl,,rf-lev 10# 'T,T Date Collcctcd/VJU>-1~ /9'9'/ Time /o,-,r-o
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Agency; --Hazardous Waste Solid Waste --/ Superfund
Sample Type
Environmt::nfal Concentrate Comments
__ Groundwater (1) _ Solid (5) 2,, Loa,e/, · h4' dloek
/
__ Surface water (2) _ Liquid (6)
/ Soil (3) _Sludge (7)
Other ( 4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results~)(mg/kg)
_P&T:GC/MS / Arsenic "';)._
_ Acid:8/N Ext, -:7' Barium .;), "-\
-:7" Cadmium MTSE .L_ I '::, ----Chloride --/ Chromium --\G>O --
----Copper
Fluoride ----Iron --/ Lead "1L, --
---Manganese ---
--.__,/ Mercury Lo.o-=.
Nitrate --/ Selenium L._\
,/Silver -'-do.
Radiochemistry Sulfates --·············-·····-···-··---·---··--------------Zinc --Parun11.:lcr Results (l'Ci/1) _pH
_ Gross Alpha __ Conductivity
Gross Beta TDS ----T0C ----
Microbiology --
--
Pur~mcter Results (Col/lOOml) --
----
----
O;t!c Rl.:cl.:ivcd Reported by
Dale Ext racled 0;.i!<.; Rcporlctl
Date Analy-1.cd I.ah Number
C:t'IJR'JI: 01 IO·. I
I /U JU' r, 9 . it : . '-~
TCLP Compounds
Inorganic Compounds Results(mg/1)
/ Arsenic ""'-o .ci l
✓ Barium 0. d!:!
v Cadmium --,;_ 0,08
v Chromium 'Lo~ iQ
-..L-Lead .L..o -SQ
/ Mercury ..L_O -C:;}...
_L Selenium LC .. oo';j
..,/Silver Kt.~Vf:1:1 ----SEP !! 1991' --
--SUPERFtlND SEeTION
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --
-chloroben7.enc --
--chlo,oform
o-crcsol --m-crcsol --
--p-crcsol
crcsol --1,4-dichlorobenzcne --1,2-dichloroethane --__ 1, 1-dichloroethylcne
2,4-din ilrotolucne --
--heptachlor
hexochloroben7.ene --hcxac h lorobu ta die ne --hexochlorocthane --
--methyl ethyl ketone
nilrobcnzcne --
--penlachlorophenol
--pyridine
--tetrachloioethylene
__ trichloroelhylene
__ 2,4,5-trichlorophenol
2,4,6-trichlorophenol
--vinyl chloride --cn<lrin --lindane ----melhoxychlm
--tox;,iphcne
2,4-D ----2,4,5-TP (Silvex)
--
N.c Ocpal1mcnt of Environment,
•··• I lca!th, & Natural Resources
Solid Waste Managcmcnl Division
SAMPLE ANALYSIS REQUEST
(~~
State Laboratory of Public Health.
,,~·-~.O. Box 2W7, 306 N. Wilmington Street .. ·
Raleigh, Nanh Carolina 2761 l
Site Number '? 2. £) -7 6A Field Sample Number--'/'----,?-'-z--'--'s"-'z:"-. -----'-----
I Nameo[SitC('.b-c,:sJo'?t lcrl:r::-1~ ,;P~,µ)~~«aa~ vf!ct/cj?:4.,, A/ C /
I Collected By ::;-;,e,;t d},,11/-e,,,,-10# 'r,T Date Co\leclcd/i'.'./Junc-/9'1/ Time ///'00
/ Supcrfund
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Agency: Hazardous Waste Solid Waste ----
Sample Type
Environmental Concentrate Comments
__ Groundwater (1) _ Solid (5) :Ji d},?fZ= s I-( r l'c,,c e,,
--Surface waler (2) _ Liquid (6)
L,/"' Soil (3) _Sludge (7)
_ Other (4) Other (8) --, ..
Organic Chemistry Inorganic Chemistry
Paramder Results(mg/1) Parameter Resull,.i Ji', (mg/kg)
P&T:GC/MS / Arsenic ,'.,.::l._ --Acid:B/N Ext. -::;,'Barium 37 ---:7" Cadmium MTBE -'-1 L, ----.. Chloride --./ Chromium --..L. J..Q
--__ Copper
Fluoride ----Iron --/ Lead --94
--__ Manganese
--J Mercury L.0-)
Nitrate --/ Selenium L,\
LSilvcr ,;.., ;,.o
Radiochemistry Sulfales --
··•-···-············-···-------···--··-· Zinc --
P.inimclcr Results (!'Ci/I) _pH
__ Gros.s_ Alpha __ Conductivity
Gross Bela TDS ----TOC --
--
Microbiology --
--
P:..iramcter Results (Col/lOOml) --
----
----
O;llc R1..:ccivt:d Reporled l,y
D<ll!..! Ext r:H.:k<l Dale Reported
Date Analy1.cd Lah Number
C::l'IJR'JI: 01 19,0 : \' I J')
. ' _,2 JU11. _ 91
TCLP Compounds
Inorganic Compounds Results(mg/1)
../ Arsenic ('.'.o. a r
../ Barium 0.,3:l.
·✓Cadmium L, o.os --J Chromium . .L...o ... \O
...,L. Lead .<.o 50
,./ Mercury 4 ~0 ~ . .
_,L_ Selenium O. O 05°
,./ Silver t(f {;f;tyt,1)
----~ f f2 q ~ 1991
--
--SIIPEREUND SECTION
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobcnzcnc --chloroform --o-crcsol --m-cresol --__ p-crcsol
crcsol --1,4-dichlorobcnzcnc -·--1,2-dichlorocLhanc
__ 1, 1-dichlorocthylcnc
2, 4-dinitrololuene --__ hcplach\or
hcxcich\orobcnzcnc --hex a ch I oro bu tad icne --hexachlorocthane
__ methyl eLhyl ketone
nilrobcnzcne
__ pcntachlorophenol
__ pyridine
--letrachloroethylene
__ Lrichloroethylene·
_. _2,4,5-trichlorophenol
__ 2,4,6-trichlorophenol
_·-_ vinyl chloride
cndrin --lind:mc
__ methoxychlor
--lox;,,ipht:nc
2,4-D ' --_ 2,4,5-TP (Si\vcx)
--
SAMPLE ANALYSIS REQUEST
(]\
. ·''·
Stale Laboratory of-Public Health
.,,...-._P.O. Box 280-17, 306 N. Wilmington Street .'
!,". :.::_ ,:· Raleigh, North Caroli~a 27611 l lcalth, & Natural Resources I Solid Waste Management Division
Site Number '? .Z t!} -7 d?A Field Sample Number_,_/=?~2~S:~~=·~,_·_ ---'---'-----
I Name of Si10-!-~si011 lcr/-r:!-1,d, 11~,#)~fte «aa~ {f c;/cj74.,< fl C /
I Collected By ~e,/t dJ/,(f'/ev lD# 'r,T: Date Collcctcd/OJu,1.:::._ /9'1/ Time // 1/...:;-
..
._/ Superfund TCLP Compounds
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Agency: Hazardous Waste Solid Waste ----
Sample Type
Environmental Concentrate Comments
Grouod water (1) _Solid (5) ·:z; .&,~/ Z-r/. t.De~
__ Surface water (2) Liquid (6)
<../"soil (3) Sludge (7)
_ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
Paramett:!r Results(mg/1) Parameter Results~ (mg/kg)
_P&T:GC/MS / Arsenic "'-2,,
---::7 Barium _ Acid:B/N Ext, 50
-::;r Cadmium MTBE -<._ \ 5 ----Chloride --/ Chromium --~.:,,o
--__ Copper
Fluoride ----Iron --/ Lead d] -
--__ Mang,rncsc
--/ Mercury L..D.09
Nitrate --✓ Selenium L.. \
1/ Silver ~..,Q
Radiochemistry Sulfates --
·············-·····-···------·-----Zinc --
Parameler Results (l'Ci/1) _. pH
__ Gross Alpha __ Conductivity
Gross Beta TDS ----TOC --
--
Microbiology --
--Parameter Results (Col/lllOml) --
----
----
O;ilc Received ReporteJ l,y
Dall.: Ex\rJc.:lccJ Dale ReporteJ
Date Analy-1.cd Lah Number
C:l'DR'JI~ Q0') !\''I"'\ 0 l I , U._; JU,, .. · .. 91
·--
Inorganic Compounds Results(mg/1)
./ Arsenic {o.a '(
✓ Barium 0~~5
✓ Cadmium Lo,08 --v Chromium L..c,. ,o
__,,c_Lead Lo.~D
./ Mercury L.. .
_.L.. Selenium f i:,.~ s
...,/Silver ,Lo. \0
----HfUEIVt:tJ
--SEP lJ 1991 --
Organic Com~Pu~~fUNDSfGTJUMs(mg/1)
benzene --carbon lelrachloride --chlordane --chloroben7.ene --chloroform --o-crcsol --m-crcsol --__ p-eresol
cresol --1,4-dichloroben?.ene --1,2-dichloroethane
__ 1, 1-dichloroethylene
2,4-din itrotol uene --
--heptachlor
hexachlorobenzene · --hexachlorohutadiene --hexochloroethane
__ methyl ethyl ketone
nitrobcnzcne
__ penlachlorophenol
__ pyridine
__ tetrachlor~elhylene
__ Lrichloroelhylene
__ 2,4,5-Lrichlorophenol
__ 2,4,6-triehlorophenol
--vinyl chloride
cndrin --lindane --
--methoxychlor
--loxaphcnc
2,4-D = 2,4,5-TP (Silvex)
--'
r-:.c. Dcpanmcnt 01 Cn\1IVl\lll<:.an,
J_kalth, &. Natural Resources P.O. Bex 2.SO-li, 306 N. Wi1.~·.:npor. Street
••·1·,,1 w_.:sic·Managcmcnl Division G l [ / +t~;_:· R..a!cig.h, North Carolina 27611
~ / o• M,. / , ' , n lf ·
•
.• 1 l,.. J ~-in ,, y-,.,-:, , '-f "/'') ;t-
Site Number f 2.. r:[} -7 A/J :__:_ Field sa:iiple Nu~ber _):,:., -;T:.5 2:.:-:.__ ·
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' I ' /d)/e.. //ry, ,£) I / C
Name of Sit& c:, .r Jam L. er /4-r::. 1,nd, /Y/:,//7 · Sile Loe:!lion_...,~c:__;_.::..,Cf_:_/..= t::C::::._.,., 9''-'-"1,_,,_·,-'--#"'-✓--/-----
-. ,/ ~ _;;;-
Collcelc<l By :_;-;,,c./t d5#-f'/-e.v ID# 'T T Date Colicetcd /0 Jun C-/9';?/ Time/ 0, ,✓ ,rO ,
Agency: H azar<lous Waste Solid Waste / Supcrrun<l TCLP Compounds -----
Sample Type Inorganic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --
,6/,qy So,/ Barium
/, --
Ground waler (1) _ Solid (5) Cadmium ----/ Chromium --
Surrace waler (2) Liquid (6) L d ,.,, t·r··' ' ca l·,,;'c> r,~ L t"::: . 0
\ ... : ;:, f ' --= McrcJ·ry L,.\. ... /: ~i·.:·': ' .::::·.,.-.·
/ Soil ('.1) _ Sludge (7) Selenium · . r •. •,;:_.,:-.··
--Silver 1 ·-' ' -..
--
_ Other (4) _ Other (8) --(''. t\/'.I~'.:nr.:\ I 1..>cr\·un;,.> ... _,' _,-., , .. ,, ...... _, ... -' -
--
--
Organic Chemistry Inorganic Chemistry --
Paramctu Rcsulls(mg/1) Pararnctt'.f Results(rng/1) (mg/kg) Organic Compounds Rcsults(mg/1)
✓ P&T:GC/MS Arsenic benzene ------
,./ Aeid:B/N Ext. Barium carbon lctraehloride
JMTBE
----
Cadmium chlordane ----
ChloriJe chlorobcnzcnc
------Chromium chlorororm
------
Copper o-crcsol
------
Fluoride m-crcsol
------
Iron p-crcsol ------
Lead crcsol
------
----J\bngan(:5C --1,4-dich lorobenzcnc
----tdcrcury --1,2-dichiorocl hane
Nitrate 1, 1-dichloroelhylcnc
------
Selenium 2, 4-d in it rotolucnc ----
Silver heplachlor ----
Radiochemistry Sulfates hexachiorobcnzcne ----.... ·······--·-··-···----··--···-------·--· Zinc hcxachlorohutad icne ----
P:irnmetcr Results (l'Ci/1) pH hcxachlorocthanc ----
__ Gross Alpha --Con<lucli,ity __ methyl ethyl ketone
Gross Bela TDS nilrobcnzcnc ------
TOC pcntachlorophcnol ----
----pyridine
Microbiology ----lelrach!oroethylcne
--__ trichlorocthylcnc
. Parameter Results (Col/lO0ml) __ 2,4,5-trichloropheool --
' __ 2,4,6-triehlorophcnol
----
----_·_vinyl chloride
cn<lrin --
RcporlcJ 1,/1
~!10Lfl 9/7)1 / / 77_,# d /
lin<l:rnc
0;1lc r-'.cn:ivcd
--
// mcthoxychlur
r1
Dale Rc~c<l
--__ tox;_iphcnt..:
Dale Ext r:ictc<l 7 · / 6 · q / /Ill /i._~/if-f/ --2,4-0
15Nf/ f',' __ 2,4,:i-TP (Silvcx)
D:ilc Anali-1.c<l f-1-'1 i P-13-91 L1h Number o -1 ? ~ ,., '"'I Y,.<·,~~·..;.,,' I --
C:i'IJS'JE 8,9 7,A.,C"'
I,., .
lfcal1h, & Nalura! Resources • •'--'· JJV'-~•, --~-•· ........ b~-.. -··--·
·Soli.d, Wast,; Management Division k.ti-b,;_/ t I"\ he.ff)(:,, •, /~ f.. 7' j 3 R..llci , North Carolina 27611.
1 · Sile Number '12 t!} -7 t/sA (J> Field Sa~plc Number L. ~---5=~"-11----------
. . / ,:!/1J/& //,1-, A7 / / C
Name ofSilcGc_r)om L.cr;t'e-.1;,d, tf/:, /T' Sile Location ncf/C:1C?'/-7 , # /
I CollccleJ By ~e,/t tfl#-//ev ID# ~L,T Dale CollcclcJ/v'J'u,..,:: ;'79'/ Time /0,~ S-0
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Agency: Huzudous Waste Solid Wasle / Superfund -----
Sample Type
Enviro11ment,1I Conct:ntrate Commen t:::i
Ground waler (1) --_ Solid (5) -2~ £..o c:=/,r n, Q &oc/4
/
Surface water (2) Liquid (6) --
/soil (1) _ Sludge (7)
Other ( 4) Other (8) --
Organic Chemistry Inorganic Chemistry
Paramder l(esults(mg/1) Paramelcr Kesults(mg/1) (mg/kg)
✓ P&T:GC/MS Arsenic --
../ Acid:B/N Ext. Barium
JMTBE
--Cadmium ----Chloride ----Chromium ----
----Copper
Fluoride ----I ran ----Lead ----
----Mang:.incsc
--__ Mercury
Nilrale ----Selenium --Silver --
Radiochemistry Sulfates --
···········-----···-------·----··-----··-·· Zinc --
Parameter Results (PCi/1) _pH
__ Gross Alpha --Conduclivity
Gross Bela TDS ----TOC --
--
Microbiology --
--
Parameter Resulls (Col/lOOml) --
----
----
&!10/11 «yrn 0;1(c;. Rcccivcd Rcporled 1,y
T J
Date Ext racled 7-Lt-q_i ,4,4 Dale Reported
f]µ(l ·,Pr Oi: 91...,4
Dale Anal·p.cd 8'-d-'i / f.-1~-'j_/ Lah Number •-' _.,,~ft..' (
C:l'l)R'JI\ 6/J =-
TCLP Compounds
·--
Inorganic Compounds Rcsults(mg/1)
Arsenic --Barium --Cadmium
. Chromium· .... _[-'" -.r r-: ,: ,.,. ,. = Lead l: \:: tL.:..1.:. .. -.r .. :-.::.!: \·1 !:~~~)-.· ;
•'
__ Mercury /::, ,··
Selenium .u · .. i ' ; : ~-,. --__ Silver S'.,J.if:f;;:•tr,~-. n.--,.-
... '"-l'I\ l )~;) 0.t:;,.,i°!-;__)/\'
--
--
--
Organic Compounds Rcsulls(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobcnzcnc --chloroform --o-crcsol --m-crcsol --
--p-crcsol
cresol --1,4-dichloroben7.cne --1,2-dichluroelhane
1, 1-dichlorocthylcne
--2,4-dinilrotoluene --__ heptachlor
hexach lorobenzene --hcxachlorobu tadiene --hcxachloroclhane --
--mclhyl clhy\ ketone
nitrobcnzcnc --__ pentachlorophcnol
__ pyridine
__ tctrachlorocthylenc
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophcnol
__ · vinyl chloride
cndrin --linU:rnc --
--mcthnxychlor
lox:1phcnt.:. --2,4-0
__ 2,4,.5-TP (Silvex)
--
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1 leallh, &. Natural Resources
'M)!(d Was!e Management Division
Agency: . Hazardous Waslc ---
Sample Type
Solid Waslc ---/ Supcrrund
Environmental Concentrrite Comments
Ground waler (1) --_ Solid (5) .)', r:;?, f ,17' z, Su-,,.. r'°=c e,
Surracc waler (2) --_ Liquicl(G)
/ Soil (3) _ Sludge (7)
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Resulls(nig/1) Parameler Results(mg/1) (mg/kg)
✓ P&T:GC/MS Arsenic --
,./ Acid:B/N Ext. Barium
JMTBE
--Cadmium --Chloride
----Chromium ----
--__ Copper
Fluoride ----I ran ----Lead ----
----i'.-fangancsc
----,\1crcury
NiLralc ----Selenium --Silver --
Radiochemistry Sulfates --
·············----·-···-·-----·--------·-Zinc --P.1raniekr Results (l'Ci/1) --pH
__ Gross Alpha --ConducliviLy
Gross Bela TDS ----TOC --
--
Microbiology --
--
Parameter Results (Col/lOOml) --
----
----
fr_ /;o/9._t qrm 0;1tc Rctcivi;d Reported by
I I
Dall: Ext r:ll.:lttl 7-16·1'/l AA Dale Reporled
(3µf!· fl, Q ',( ") -~ 7 .,..
Date Analy1.cd F?-.2-9 ( 8:-1,1-'i I Lah Number •-' .1 .. ~ L ;)
C:l'l)R'Jt: 8~ -nw---
TCLP Compounds
Inorganic Compounds Rcsults(mg/1)
Arsenic --Barium --Cadmium = Chromi.u.rp,1( '{'~r1Ji~i, Y Lead \·, \. c.\,f .. ,-, .. ,. ,, .......
--__ Mercury /',: :~. ' '\ (_:: :.; '!
Selenium --Silver ~:r:r1r:np1r,:ri ~f~~T!f~\·.} --,. , ~-' ', c...~ I,' ! .
--
--
--
--
Organic Compounds Results(mg/1)
benzene --carbon Lclrachloride --chlordane --chlorobcn7.G,ne --chloroform --o-crcsol --m-crcso! --
--p·crcsol
cresol --1,4-dichlorobenzcne --1, 2-<lich loroclh,rnc --
--1, 1-dichloroclhylcnc
2.1 4-d in iLrotol ucnc --
--hcplachlor
hcxochlorobcnzcnc --hexachlorobuLad ic ne --hcxachloroclhane --
--mcLhyl ethyl kclone
nitrobcnzcne --
--pcntachlorophenol
--pyridine
--Let rachloroethylene
__ trichloroethylene
__ 2,4,5-trichlorophenol
__ 2,4,6-trichlorophcnol
__ vinyl chloride
cntlrin --lin<l:rnc
__ mcthoxych!or I
--lux:.qihl'nt.:
2,4•0 --
--2,4,5-TP (Silvcx)
--
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Agency: H;wu<lou~ Waste Solid Waslc / Supcrfun<l -----
Sample Type
Enviro11menf;1l Concentr"te Commtnl.s
.5; £},-:,,,,..,, z-;"/, d)ee,a_ Ground waler (1) _ Solid (5) --z;, z;,
Surface waler (2) Liquid (6) --
/soil (3) Sludge (7)
Other (4) --_ Olher (8)
Organic Chemistry Inorganic Chemistry
Parameter Resulls(mg/1) Parameter Results(mg/1) (mg/kg)
./ P&T:GC/MS --Arsenic
/ Aci<l:B/N Ext. Barium
JMTBE
--Cadmium ----Chloride ----Chromium ----
----Copper
Fluoride ----Iron ----Lead ----
----M angancsc
----Mercury
Nitrate ----Selenium --Silver ·--
Radiochemistry Sulfates --
········-·-··-···--·-···--·------·--· Zinc --
P:1ramekr Results (l'Ci/1) pH --
__ · Gross Alpha --Conductivity
Gross Bela TDS ----TOC --
--Microbiology --
--
Paramder Results (Col/l00ml) --
----
----
.
0!1c I 11cy1
'J)~ 0;1le Received RcportcJ by
( I '
Dale Extraclcd 7-/( ·9/ I/A DJtc Rcpor1cJ
,clt,>,4 f}T O<i .0-~ ,.., -~.
Date Analy-1.cd fJ·.2-'l I 6-i3-4t Lah Number ._, ..;:.. ffo•..:... ~ t,
C:l'DE'J!: f:]i[) ~
TCLP ·compounds
·--
Inorganic Compounds Results(mg/1)
Arsenic --Barium --Cadmium --Chromium -, ·r. "
Lead ," \ , ' \ ,,; .. i ' ~ ---.. --· ---~-~.-1 __ Mercury
Sc!cniufr(:. :~-~ " t:::.::i .: •._/ --Silver --_.., ' ''"' :-r-1 :-, it·. i,: ' • . ' l . ; ' ,"' ; ·: ''\~;_,-:-.ii,!1c-1 .\'.•·i ;·:1·v;~~!;·~ .. ' --... ', ... ---
--
--
--
Or-ganic Compounds Results(mg/1)
benzene --carbon tclrachloride --chlordane --chlorobcnzcnc --chloroform --o-crcsol --m-crc.sol --p-crcsol --cresol --1,4-c\ichlorobcnzcnc --1 )-<lic\1 lorocl hanc --
--1, 1-dichloroclhylenc
2, 4-di nil rolol ucne --
--hcplachlor
hexaehlorobenzcnc --hcxachlorohu La<licne --hexachloroethanc --
--methyl ethyl ketone
nitrobcnzcne
__ pcntachlorophenol
pyridine --__ letrachlorocthylene
__ lrichloroelhylenc
__ 2,4,5-lrichlorophcnol
__ 2,4,6-trichlorophcnol
vinyl chloride --cmlrin --lin1.Lrnc --
--mclhoxychlor
--lux;iphcne
2,4-D
_ 2,4,5-TP (Silvcx)
--
/7:'-.
<<"/.'."c.i!:! 0£ Cus-::9_C...-?,ecord
I
of S2..Illpling:
I
S=ple No.
I
,.n. of Poss.ession:
-~cL~/1_______, r . . . sign2;:ure inclusive 02.t:es
. f
I 7/ 0-?1 c;; luaA __ d
" signet:ure -c.it.le inclusive dates
1-------signc.cure inclusive. d2.r.es
~
CoO?plece 2.ll 2.pplic2.·c1e inforcc.:io:-, incluC::.n; s}..g:-12cures, and
su'oIT!iC \..0:i.c·:1 ·2nc.lysis re(!ues~ fo:-=s.
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f;:'7;:STATE LABORATOOY OF PUBLIC HEALTH /:;· ·_.
'DIVISION OF:c:\:·_TH SERVICES, N.C. DEPARTMENT OF .HUIIAI :·.;\;OJRCES
. P.O. BOX 2&~~1 -306 N. _WILHINGTON, ST., RALEIGH, N,_;;· 27611
ORGANIC 0-0:HICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO 0/ ,,-7-., 4'/ .. ?J 7d '-1 I J17.:, '-I I -, 1 7&,
EXTRACT ABLES FIELD# I IJ.9 ~ .J.. /LJ.Cj <-~ lll-"i3'-I-j/JQC?,
CXJMPOOND TYPE ( ;;, l • ( .:;> l ( 3) ( ;;, l
UNITS ua/ l ,,,n/kri' """'1 r.,n/ka .. un/kn lroArua/ka
,-nitrosodimethvlamine f/'\/;;/"V, ,,-' , t,\_. IA
is(2-<:hloroethvllether
2-<:h 1 ornnheno 1
lhenol
, . 3-<li ch lorobenzene 1·-~.'-'
1 4-<lichlorobenzene l, \.:
1 2-<lichlorobenzene
is(2-<:hloroi l)ether
• exach 1 oNJethane [1ft
N-ni troso--di -n .nrf'V'lvl amine
-.._,,.,
~obenzene
horone
2-n i trooheno 1
14-<limethvlohenol
is(Z-<:hloroethoxvlmethane
2 4-<lichlo~henol
-~( trichlorobenzene hthalene
achlorobutadiene
4-<:h l oro--m-creso 1
exachlorocvclnnPntadiene
4 6-trichlo~henol
· 2-<:hloronanhthalene I cen•nhthvl ene
imethvl ohthalate
6-<linitrotoluene
lcenaohthene I
4-<linitrnnhenol sn/n,.,;o
_,4-dinitrotoluene IOI ?.'10
4-n i trooheno l ,;o/t '-~o
lluorene • 10/ ~30
-chlornnhenvlohenvlether
diethyl ohthalate . , l. 6-<linitro--0--<:resol ,;a ~/-',(j .
iohenvlamine
azobenzene ,,
f.rcm10henv l ohenvl ether Ir> ·:i30
xach l orobenzene /,A/j</i
ntachlornnhenol so/11,,57J
ohenanthrene ,,,, /:nr.
nthracene
ibutvl ohthalate I I , /
fl uoranthene ~ \
I ml)L
-Estimated value. l-{,.o/S0/1,...
K -Actual value is known to be less than value given.
/
~
r )
un/ 1 un/ka
.::-. r " [i-:-r '.' r i:_.~
=· '~! ~; :,;'. i. \: : . .::
. : : r• -: •.( , ....
·.,n;·rp•y_~, ,,~n·
;_:~1 ~JH,.' ._;;_\;
L -Actual value is known to be greater than value given. ■ -tlaterial was analyzed for but not detected. The nurt>er is the Hinirrun Detection Limit. m1JL ---W, -Mot analyzed. .
,I -Tentative identification. fl -On NROC List of Priority Pollutants.
'
. C. V-<.v-<-6-<.0n 06 He.a.Uh ·se1tvic.v.,
HS 3068-0 (4/86 Laboll.a.-to~y)
I
-
( )
un/ 1 ua/ka
:" ',',
~:.:.{.-·
., . .
·,~·-·
,, • .:!'.:
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BASE/NEUTRAL ANO ACID
EXTRACT ABLES
ClJMPOONO
nvrene
benzidine
butvl benzvl ohthalate
benz(a)anthracene
chrvsene
3 3-dichlorobenzidine
bis(2-ethvlhexvl)ohthalate
di-n-octvl ohthalate
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)nvrene
i ndeno( 1 2 3-<:dl ovrene
dibenzo(a h)anthracene
benzo(o h. il~rvlene
aniline
benzoic acid
benzvl alcohol
4-<:hloroani line
dibenzofuran
2-<rethvl nanhtha lene
2-<rethvlohenol
4-<rethvloheool
2-nitroani 1 ine
3-nitroaniline
4-nitroaniline
2 4 5-trichlorooheool
/-I 'I;]) I? 0 <!A /?_13 0 ,._; -.:s
J -Estimated value·.
(·_\\ STATE LABORATORY Of PUBLIC HEALi•
DIVIS!ON.-c.f HEALTH SERVICES, N.C .. DEPARTMENT Of k:AH RESCXJRCES
P.O. BOX 28047 -306 N. WILMINGTON, ST .• RALEIGH, N.C. 27611
ORGANIC QjEMICAL ANALYSIS
LAB NO Cf/.,) I 7 ~ '1/,-:J. J7i../ Cj 1.217.5 4 J.:::J.17&>
FIELD# I t.J.9 '?-2-/IM'<.~ Ill C, ,=?U ;<I, 'i.3.\
TYPE ( -=?) ( -) (_:;,) ( ::, )
UNITS crm'-ll; , n /kn" _,...,_, I ,n/ko an=r 11r/kn ,.m'-1 <,, o / k o
IO/~",,, u\.__,. /.A_, ve: (A
,'){) /1150
10I.:1::io
I .. , , 1'. \
so/lh,;,,, \ / .. ,v
llo/330 I '>< &, t., 7 'Z.:; :::i 5< '-I
10/.J.~o ; ,, -·u
So/1~',t'; ~,•;,
J / ,
'., ' / .\ ' /
_,("t, /,~ ·vL, l,L..-vL., (A__·
.. .
"' "· /()/'<J'1
~:,
S'o/,t.,;o
J I ,, '.1 '\ \ \
___,_ -~-+1-(-) ( +1 (+} (. "'; , -
m'X>1-
H2.0I $OIi..
to be less thdn value given.
rv'
l/J
( )
uo/1 uo/ko
I• \o.-, ~ " _•· :'
-'-=: ~.-.. tL.J· t· L
; '· .. -. ' ..
---·· .. . .
·1J~l"!_i!'f:.i 0-tL
I
K -Actual value is known
L -Actual value is known
U -Katerial was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nuroer is the Hinirrun Detection Limit.
1/ -Tentative identification. £1 -On NROC List of Priority Pollutants.
N. C. D-i.v.u-i.on o 6 Hea.Uh SVtv-i.ev.,
VHS 3068-0 14/86 LaboJuLt.o~y)
( )
11n/ 1 .. n/J
r ' :.L-:-J.
;;:)t\.
PURGEABLE CO'iPOUN0S
lXll' .POUN 0
STATE LABORATORY Of f'UBLIC HEAL!H
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 2800 -3(),; N. 1.'ILMINGIOII. ST., RALEIGH, N.C. 21611
ORGANIC D-<EMICAL NIALYS!S
LAB NO Y I ;LI r, ,l q1217+ '-; t:2176 C.1-;:l,/f(n
FIELD# /11.C? 3-;/, !IJ533 DJ.G3'-f-11/C _,,;
TYPE ( 3) ( ,! ) ( ' "! ) c'~?)
A/
i l/
' ( ) ( )
i)
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UNITS uo/ T 'u<i/kQJ ua/ 1, uo/kn uo/ I ruo/kq uo/ J,u'o/k ) uo/ T un/ko ua/ I "0 /kq
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chlorcrrethane 10 ........ b " ' u.... , '
broronethane ,I, I
dichlorodifluorcmethane 5Mh I 1, ~ .. ;:-;'""" i. ,. r.:.•-;:
vinyl .. I .. ---. ~ .. ·--chloride
chloroethane ,I ' ( -v -.I/ .
methvlene chloride / 1.-. '7. I r_,; /0
trichlorofluorcmethane I I I , '. I,_ ' i '. Df.{:;:;1; .: :·;
ethene. l l-<lichloro I I
ethane 1 1-<lichloro-I I
1,2-trans-dichloroethene I I
chloroform , I ,
ethane 1,2--dichlorr..-I ! I
ethane. 1. 1 1-trichloro-I I I
carbontetrachloride I. I I i
brorodichloronethane I i I I
prN1ane. 1.2-<lichloro-I I I I
1 3-trans--dichlo ne ! ! i
trich loroethvl ene I ; i
chlorodibrcn-o-nethane I ' ' benzene I I ! ' ' eth..ane. l 1.2-trichloro-,, i I
1 3-cis-<lichloroo=ne 1O-.,-,h !
2-chloroethvl vinvl ether .,J; I \
braroform 5 --"' ;
ethane 1. 1.2 2-tetrachloro-.. '
ethene tetrachloro-
toluene
chlorobenzene I '
ethvlbenzene / "' -~/ °I' V
acetone to __ J.. ,,. ;,i (-t-) I ' I'
2-butanone ;o· u_ i I
carbondisulfide 5 j I I
2-hexanone 10 I I
4-<rethvl-2..n,,ntanone 10 i !
styrene ", i I
vinvl acet.a te ,a I '
xvlenes /+«tall 5 I i
... ,P./3. ,=; ' ,, ,/ ' / _i/ J./
·11 v1DI 1'
J -Estimated value.
K -Actual value is knc,..,n to be less than value given.
to be greater than value given.
for but not detected. The n~r is the Minirrun Dete-<:tion Limit.
1 j.~:-.
i::-· ,-r-.·r: ... t[:: . .. . -..
I l -Actual value· is known
U -Xdterial was analyzed
NA -Not analyzed.
1/ -Tentative identification.
I ~/ -0~ NRDC List of Priority Pollutants.
-'>f--;) .. 1) -· -. I ' .I '
105:)1 D e ,e+r15·ercdor CQ7'\'l'Q rv\, f1.ccr·10-,'1. ·
I
C -~i.J.75PEC:, LR8 C..ONTAMrNAT>ON.
N.C. Division of l{ealth Services
DHS 3068--0 (~/86 Laboratory)
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References 2 through 40 appear in Volume II
l MILE
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'' '
' ' I: ' .
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''
WAKE: FORE:ST, N. C.
NE!', RALEIGH 15 Glll~CllAN'll F
35078 H5 TF 024
1967
DMA 5255 I Ntl -SCC,IES VB4?
· I .11
770000
CCIT
•n
""
....___