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HomeMy WebLinkAboutNCD986187094_20030212_Reasor Chemical Company_FRBCERCLA SAP QAPP_Field Sampling and Analysis Plan - Revision 0-OCRI I I I I I I I I I I I I I I I I I I Prepared By: Prepared and Approved By: Approved By: Approved By: REASOR CHEMICAL COMPANY/ , CASTLE HAYNE, NORTH CAROLINA REMEDIAL DESIGN FIELD SAMPLING AND ANALYSIS PLAN REVISION O -12 FEBRUARY 2003 WORK ASSIGNMENT NO. 147-RDRD-A424 Prepared for U.S. EPA Contract No. 68-W?-0026 U.S. Environmental Protection Agency 77 West Jackson Boulevard Chicago, Illinois 60604 p.,l"'Ralph P. rAKeen,i>.E. Project Engineer FEB 1 8 2003 Date: j.. -I :z.-o ::J Teresa Offne ~ Site Manager James M. Burton, P.E. Program Manager Geoffrey B. Noakes Administrative Support Manager Date: ------ Date: ------ ' .. NOR/K:\WP\20064\147'FSP-Rev0-Feb03.doc RFW-147-28-AMPB This documenl was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I Section 1 2 3 TABLE OF CONTENTS Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Page INTRODUCTION .............................................................................................. 1-1 I. I 1.2 Site/Facility Description .......................................................................... 1-1 Project Objectives .................................................................................... 1-3 SITE MANAGEMENT PLAN ......................................................................... 2-1 2.1 Site Control. ......... : ................................................................................... 2-1 2.1.1 Site Access ......................................................................................... 2-1 2.1.2 Site Security ....................................................................................... 2-1 2.2 Project Organization And Personnel Responsibilities ............................. 2-1 2.3 Project Schedule ...................................................................................... 2-3 FIELD SAMPLING AND ANALYSIS PLAN ................................................ 3-1 3.1 3.2 3.3 Scope Of Work ........................................................................................ 3-1 Sampling Protocols .................................................................................. 3-2 3.2.1 General .............................................................................................. 3:2 3.2.2 Surface Water and Sediment Sampling ............................................. 3-2 3.2.2.1 3.2.2.2 Surface Water Sampling ........................................................ 3-2 Sediment Sampling ................................................................ 3-4 3.2.3 Surface Soil Sampling ....................................................................... 3-4 3.2.4 Groundwater-Level Measurements ................................................... 3-5 3.2.5 Monitor Well Installation .................................................................. 3-6 3.2.6 Monitor Well Development.. ............................................................. 3-9 3.2.7 Monitor Well and Production Well Sampling ................................... 3-9 3.2.7.1 3.2.7.2 3.2.7.3 Calculating Purge Volumes and Well Purging Procedures. 3-10 Temperature, pH, and Conductivity Readings .................... 3-12 Groundwater Sampling ........................................................ 3-13 Field QC Samples .................................................................................. 3-13 3.3)1 3.3.2 Equipment Rinsates ......................................................................... 3-14 Field Duplicates ....................................... : ....................................... 3-14 I I I I I I I I I I I I I I I , I I I I Section 4 3.4 3.5 3.6 3.7 3.3.3 3.3.4 3.3.5 TABLE OF CONTENTS (Continued) Title Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Material Blanks ............................................................................... 3-14 Matrix Spike/Matrix Spike Duplicate ............................................. 3-14 Inorganic Blanks .............................................................................. 3-15 Residuals Management.. ........................................................................ 3-15 Sample Packaging ................................................................................. 3-15 3.5.1 3.5.2 3.5.3 Completing Sample Collection Field Records ................................ 3-16 Completing Sample Labels and Tags .............................................. 3-16 Sample Packaging and Shipment .................................................... 3-18 Equipment Decontamination Procedures .............................................. 3-18 3.6.1 3.6.2 3.6.3 Monitor Well Instruments ............................................................... 3-19 Submersible Pumps and Hoses ........................................................ 3-19 Augers and Tools ............................................................................. 3-20 Documentation And Chain-Of-Custody Procedures ............................. 3-20 3.7.1 3.7.2 3.7.3 Field Logbook .............................. ~·················································· 3-21 Chain-of-Custody Procedures .......................................................... 3-22 Custody Transfer and Shipment ...................................................... 3-22 QUALITY ASSURANCE OBJECTIVES ....................................................... 4-1 4.1 Data Quality Objectives ........................................................................... 4-1 4.2 Intended Use Of The Data ....................................................................... 4-1 NOR/K:\W P\20064\ 14 7\FSP•RevO-F eb03.doc II RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. )I shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I Figure No. 3-1 3-2 3-3 TABLE OF CONTENTS (Continued) LIST OF FIGURES Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Sample Location Map .......................................................................................... 3-3 Shallow Well Construction Diagram ................................................................... 3-7 Deep Well Construction Diagram ........................................................................ 3-8 NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I II I I I SECTION I INTRODUCTION I.I SITE/FACILITY DESCRIPTION Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147•RDRD-A424 Revision: 0 Date: 12 February 2003 Weston Solutions, Inc. (WESTON®) has prepared this Field Sampling and Analysis Plan (FSP) for the U.S. Environmental Protection Agency (U.S. EPA) Regions 4 and 5 describing procedures for field activities required to complete the Remedial Design (RD) for the Reasor Chemical Company (RCC) site located in Castle Hayne, North Carolina. WESTON has prepared this report under Work Assignment No. 147-RDRD-A424 of Contract No. 68-W7-0026 with U.S. EPA and in accordance with the 23 September 2002 U.S. EPA Statement of Work (SOW) and the RD Work Plan prepared by WESTON dated 18 December 2002. The Reasor Chemical Company Site is located in the southeastern part of North Carolina approximately IO miles north of Wilmington, North Carolina. The specific site location is 5100 North College Road, 0.5 miles southeast of the intersection of NC Route 132 and US Route 117 in Castle Hayne, New Hanover County, North Carolina. The site is approximately 25 acres in size. The RCC site is the location of a former stump rendering facility, which operated from 1959 to 1972. RCC produced turpentine, pine, resin, pitch, tall oil, pine oil, camphor, pine tar, and charcoal from pine tree stumps. The facility is believed to have used various solvents to extract raw product from chipped stumps, distilling the extract into separate product fractions. The solvents used in the extraction process were likely stored on site in 55-gallon drums, the remains of which are still visible in a surface drum disposal area near the center of the property. NOR/K:\WP\20064\ 147\FSP-RevO--F eb03.doc 1-1 RFW-147-28-AMPB This documeol was prepared by Weston Solulions, Inc:., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 RCC operated the facility until I 972 when the property was sold to Martin Marietta Corporation (MMC). Residual buildings, machinery, and equipment were to be cleared from the site before 1 December 1971, prior to the sale of the property to MMC. RCC intended to remove the boiler room building and rosin warehouse 90 days from the date of closing. A fire, and possible explosion, occurring on the property on 7 April 1972, damaged or destroyed the remaining buildings and materials on the site property. At the time of MMC's purchase of the site, the property consisted of ruins of some of the buildings, scrap metal, debris, and cardboard barrels containing hardened resin. MMC, a producer of aggregates for the construction industry, never conducted operations at the RCC property, and in I 986, MMC sold the property to Hilda C. Cameron and Nathan S. Sanders and wife, Judia S. Sanders. The property is currently vacant. Unpaved roads run along the inner periphery of the property and throughout the site. The site is currently overgrown with brush and second growth forest. Site features which are still distinguishable include three tank cradle areas (north tank cradle, south tank cradle, and work tank areas), a boiler house, and the concrete slabs from the former rosin warehouse, laboratory, garage, truck scale, still, process line, transformer area, train scale, pipe shop, and several other unidentified former buildings across the site. Five surface impoundments or ponds, which were likely used in the manufacturing process, a scrap copper area, two railroad sidings, a surface drum disposal area, a sluice area, and several drainage ditches are also still present at the site. In August 1996, U.S. EPA issued a work assignment to WESTON to perform a Remedial Investigation. The RI was completed in December 1999. The Remedial Investigation led to a Focused Feasibility Study (FFS) to determine the most cost-effective remedial action for the RCC site. The FFS was completed in July 2002. NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 1-2 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disc:losed in whole or in part without the express written permission or U.S. EPA. I I I I I I I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 U.S. EPA issued the Record of Decision (ROD) for the site in September 2002. The ROD called for removal of approximately 500,000 gallons of contaminated surface water, excavation and removal of 1,600 cubic yards of soil and sediment, and annual groundwater monitoring. This Field Sampling and Analysis Plan (FSP) for the Reasor Chemical Company site presents the procedures to be used in support of the Remedial Design (RD) for the site. Additional information concerning project operations is contained in the Quality Assurance Project Plan (QAPP) and the Health and Safety Plan (HASP) submitted under separate cover. The objective of the RD at the Reasor site is to perform the necessary activities required to develop the final plans and specifications, general provisions, and special requirements necessary to translate the selected remedies as defined in the ROD into the remedy to be constructed under the Remedial Action (RA) phase. 1-2 PROJECT OBJECTIVES Meeting the goal described previously will require fulfilling the objectives and data requirements itemized below: • Surface Water: Surface water impounded by four of the five on-site ponds_will_be pumped out and removed as part of the remedial action. A composite water sample from all four ponds will be collected and analyzed for waste profiling using the TCLP procedure. • Surface Soil: Surface soil in three areas will be removed and disposed off-site. One composite soil sample from these three areas will be collected and analyzed for waste profiling using the TCLP procedure. • Sediment: Sediment in the four on-site ponds will be excavated and removed after the surface water has been pumped out. A composite sample will be collected from all four ponds and analyzed using the TCLP procedure. NOR/K:\WP\20064\ 141\FSP-RevO-f eb03.doc 1-3 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission or U.S. EPA. I I I I I I I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 • Groundwater: There are eight monitor wells and three production wells currently on site. As part of the RD activities, two additional monitor wells ( one shallow and one deep) will be installed to augment the existing groundwater monitoring network. All existing monitor wells will then be sampled and analyzed for total metals. Two rounds of sampling of the groundwater monitor wells are anticipated as part of this ID/ -~ '---0 .,_ / 'a-, I'--( . ..+..,(~'? NOR/K:\WP\20064\ 147\FSP-RevQ.f eb03.doc RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the npress written permission or U.S. EPA. I I I I I I I I I I I I I I I I I I I SECTION2 SITE MANAGEMENT PLAN Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 This section provides general operating guidelines for access, security, and the field team organization that will be implemented during investigation activities, as referenced in the RD Work Plan. 2.1 SITE CONTROL 2.1.1 Site Access Access to the site is adequate to most of the study area; some roads may need to be cleared of minor debris (man-made or natural). Locations for the additional monitor wells may need minimal adjustment for trees, fences, and other obstructions. 2.1.2 Site Security Since the site is only accessible by one road, a security gate with padlocked chain is in place to limit access. The security gate and chain will be locked at the completion of each workday. Monitor wells will be secured with a locking protective cover prior to the completion of a workday. 2.2 PROJECT ORGANIZATION AND PERSONNEL RESPONSIBILITIES The project team for WESTON at the RCC site will work under the direction of the EPA Work Assignment Manager (W AM), the WESTON Program Manager (PM) and the Site Manager NOR/K:\WP\20064\ 147\FSP-Rev0-Feb03.doc 2-1 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 (SM). The field team will also work under the direction of the PM and SM. Project personnel responsibilities are listed below. Program Manager (PM). Mr. James Burton, will serve as project director. Mr. Burton will be responsible for assessing and monitoring corporate resources, approving project plans, conclusions/recommendations, leading major briefings/meeting negotiations, and technical oversight. Site Manager (SM). Ms. Teresa Offner, P.G., will serve as the Site Manager. Ms. Offner's duties and responsibilities will include project team management, project scheduling, budget monitoring, technical task integration, and communication and coordination of team members and field efforts. In addition, Ms. Offner will serve as the Project Geologist/Hydrogeologist for determining monitor well locations. She will also coordinate the collection of water level data and the collection of soil and groundwater «-i,J I '._.(_ ~ samples. " Field Geologist/Hydrogeologist. The Field Geologist/Hydrogeologist will be responsible for implementing all activities related to the geology/hydrogeology including overseeing monitor well installations, Iithologic logging, and collection of soil and groundwater· 5w, 5eJ? samples. Another Geologist or Scientist will assist the Field Geologist during the sample collection activities. One of the field team members will be designated as the Sample Custody Officer. This person will be responsible for ensuring proper completion of sample custody forms as well as proper packaging and shipment of samples. Project Quality Assurance Officer. The Project Quality Assurance Officer (PQAO) will be responsible for the direct oversight and overall implementation of the Quality Assurance project Plan (QAPP). The PQAO will monitor and audit implementation of NOR/K:\WP\200641147\FSP-Rev0-Feb03.doc @ RFW-147-2S-AMPB This document was prepar-ed by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 the approved document, including field activities, using the procedures as defined in the QAPP. 2.3 PROJECT SCHEDULE Section 3 of the RD Work Plan presents the estimated project schedule. The schedule begins with the submittal of the RD Work Plan. Several assumptions are built into this schedule such as EPA review of deliverables and CLP laboratory analysis turnaround. These activities will directly impact the schedule accordingly. NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 2-3 RFW-147-28-AMPB This document WH prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the npress written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I SECTION 3 FIELD SAMPLING AND ANALYSIS PLAN Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 This section describes the sampling and analysis procedures for conducting the actions recommended in Section I. The sampling protocols comply with the U.S. EPA's (EPA) Environmental Investigation Standard Operating Procedures and Quality Assurance Manual (EISOPQAM), Region 4, revised November 2001. If any deviations in sampling procedures from the approved Work Plan occur, these deviations will be recorded in the field logbooks as described in this section under "Documentation and Chain-of-Custody Procedures." 3.1 SCOPE OF WORK Based on the discussion in Section I of this plan, further investigation is recommended in the following areas to obtain data needed to accomplish the RD objectives: • Surface Water • Sediment Sampling • Surface Soil Sampling • Groundwater-Level Measurement • Monitor Well Installation • Monitor Well Development • Existing Monitor Well and Production Well Sampling Investigative methods, operating procedures for samples, equipment decontamination, and documentation follow. NOR/K:\WP\20064\147\F$P-Rev0-Feb03.doc 3-1 RFW-147-28-AMPB This documenl was prepared by Weston Solutions, Inc., expressly for U.S. EPA, It shall not be released or disclosed in whole or in part wilhout the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I 3.2 SAMPLING PROTOCOLS 3.2.1 General The following activities will be conducted prior to all sampling events: Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147~RDRl)..A424 Revision: 0 Date: 12 February 2003 • All sampling equipment will be decontaminated prior to and immediately after use • All field data will be logged in a bound field book Details regarding these activities are contained in this section. Figure 3-1 shows the locations of the existing and proposed monitor wells, and the four (4) ponds and three (3) soil areas that will be sampled. 3.2.2 Surface Water and Sediment Sampling 3.2.2.1 Surface Water Sampling The surface water samples will be collected directly into a sample container for compositing. For pond locations at the RCC site, surface water samples may be collected using an extension sampling device. The sampler will lower the sample container into the water at a low angle relative to the water surface. The surface water sample will be collected prior to a sediment sample at the same location. A composite sample from all four ponds will be collected. A minimum of I quart of liquid will be collected from each pond and combined in a pre-cleaned stainless steel bucket. The composite sample will be placed into the following containers for analysis: • I -One gallon glass amber • 3 -40 ml glass septum • I - I liter polyethylene NOR/K:\W P\20064\ 147\FSP-Rev0-Feb03.doc TCLP Extractable Organics TCLP Volatile Organics TCLP Metals 3-2 RFW-147-28-AMPB This document was prepared by Weston Solulions., Inc., expressly for U.S. EPA. It shall not be releued or disclosed in whole or in part wilhout the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I s-~ -0 :;o 0 -0 ~ ---1 --< C z Pl TRAIN CAR-....J.fJ SCALES MW-2 $ CONC. FlLLED TRANSFORMER BANK FORMER LABORATORY-- STEEL COLUMNS )~ONC. PLATFORM N PILINGS ,..---SCRAP COPPER $ MW-4S MW-4D \ , . EXTRACTOR -/ I ----- SOU TANK CRADLE AREA -5 $ -· MW-1 $ REMAINS OF BOILER HOUSE REFlNERY FORMER ROSIN WAREHOUSE LEGEND I I if_f_J -$- SOIL LOCA 110NS EXCEEDING Q..EANUP GOAL SEDIMENT LOCATIONS EXCEEDING 0.£ANUP GOAL PROPOSED NEW MONITOR WELL LOCATION I I I '---NORTH TANK CRADLE JAREA DRUM DISPOSAL AREA WORK TANKS I I I I I L---- - -----X / . I I I - I I I I I I I I I I ,-----_I SETTLING POND \ - i=-A C'T A ,...,....r-..... - <( z ....J wo t: Cl:'. V) <( >-u Q. Z:J: <( <( I-:::;; Q. Cl:'. :::;;o z WOODED AREA oz 0 I u I-I") ....J >-" <( <(I-u w Uz 0 Cl:'. -:::> ....J :::> :::;;o <.!) WU w LL I ....J UC!:'. Q. Cl:'.~ :::;; <( oo V) V)Z <( <( WI Cl:'. ;;: w z z 0 z vi < 5 _J w 0. a:: VJ C> LL VJ LL z I-_J :::; LL 0. < < :le 0:: z < 0 Li: VJ APPROX. 0 MOUND AREA ~ _J "' "' l!I 0 0 "' < --------------- 0 <D r---"' -. ----:le :le :le 0. 0. 0. a:: a:: 0:: I I I D I m I I I I I I I I I I I Reasor Chemical Company . Field Sampling and Analysis Plan WA No: l47-RDRD-A424 Revision: 0 Date: 12 February 2003 The composite surface water sample will be submitted to a fixed laboratory for the required analyses. 3.2.2.2 Sediment Sampling If the surface water body is wadeable, the sediment samples will be collected by using a stainless steel scoop or spoon. The sampling method will be accomplished by wading into the surface water body and scooping the sample along the bottom of the surface water body. Excess water may be removed from the scoop or spoon. However, this may result in the loss of some fine particle size material associated with the bottom of the pond. In ponds that are too deep to wade, but less than eight feet deep, a stainless steel scoop or spoon attached to a piece of conduit can be used from the banks of the pond. If the above-mentioned sampling methods are not practical, the Eckman dredge will be used to collect the sediment samples. A sample from each pond will be placed into a stainless steel bowl, stirred, and mixed thoroughly. The composite sample will be placed in the following containers for analysis: • 1 -8 ounce glass • 1 -2 ounce glass • 1 -8 ounce glass TCLP Extractable Organics TCLP Volatile Organics TCLP Metals All sediment samples will be submitted to a fixed laboratory for the required analyses. 3.2.3 Surface Soil Sampling Composite surface soil samples will be collected from three areas using a stainless scoop from the O to 6-inch depth below ground surface horizon. The scoop will be advanced through the selected sampling depth, and the contents will be emptied directly into a stainless steel bowl. NOR/K:\W P\20064\ 14 7\FSP-Rev0-Feb03.doc 3-4 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission or U.S. EPA. I I I I n I I I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 For VOC compound samples, the soil will be selected from the scoop and placed directly into the -2 sample jars. The sample will be packed tightly into the jar to remove all open head space. Before collecting samples of the soil for other analytical compounds, the soil will be thoroughly stirred and mixed within the bowl. The composite sample will be placed in the following containers for analysis: • I - 8 ounce glass • I - 2 ounce glass • 1 - 8 ounce glass TCLP Extractable Organics TCLP Volatile Organics TCLP Metals Soil samples will be submitted to a fixed laboratory for the required analyses. 3.2.4 Groundwater-Level Measurements Groundwater-level measurements are to be collected from the eight existing permanent monitor wells, two proposed monitor wells, and three existing production wells. This will be done to evaluate the hydraulic gradient at the site. Groundwater-level measurement procedures will be performed in accordance with the EISOP QAM (Region 4 EPA-SESD, November 2001, Section 15.8). An electronic water-level indicator will be used for the field work. This instrument consists of a coil of connector wire, a probe, and an indicator assembly. When the probe comes into contact with the water, the circuit through the connector wire is closed and a light or buzzer is emitted. Recordings will be made to the nearest 0.01 foot. The assembly will be decontaminated in accordance with the decontamination procedures outlined in the EISOPQAM. . ·~ (p l ,,._{ Sev+-· · Calibration and maintenance information will be documented in the field log book. Water level measurement data will be recorded in the logbook or on field data sheets, which will include at a NOR/K:\ W P\20064\ 14 7\FSP•Re\lO-F eb03.doc RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., eipnssly for U.S. EPA. II shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I D D I I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 minimum the well number, date, time of day, and a description of the reference point on the well casing from which the measurements were taken. The reference point will be tied into the National Geodetic Vertical Datum (NGVD). 3.2.5 Monitor Well Installation The newly proposed monitor wells will be installed using the hollow-stem auger drilling method. The drill rig and all drilling materials will be decontaminated prior to beginning field work and between installation of each well. Refer to Subsection 3.6 for decontamination procedures. Figures 3-2 and 3-3 depict typical well construction details for shallow and deep wells, respectively. The materials and methods used m the construction of the monitor wells will include the following: • Well depth will be approximately 10 feet below the top of the water table for shallow wells and approximately _25 feet below the water table for deep wells, which at the Reasor site is expected to occur at approximately 5 feet below ground surface (bgs). The well screen will be 2-inch, stainless steel, IO feet long for shallow wells and 5 feet long for deep wells, and will have 0.0 I 0-inch slot widths. • The bottom of the well screen will be fitted with a stainless steel end cap, which will be threaded onto the screen. This cap will be placed within 0.5 feet of the open portion of the well screen. • The screen filter pack will be a silica sand, extending from approximately 0.5 feet below the well screen to 2 feet above the screen. • A 2-foot-thick bentonite pellet seal will be placed above the top of the filter pack and allowed to hydrate for approximately 8 hours. • The annular space will consist of a grout seal of 20: I cement and bentonite slurry. Cement will be commercial Portland cement. The grout will be placed using standard tremie techniques. NOR/K:\W P\20064\ 147\FSP-RevO-F eb03.doc 3-6 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express wr-itten permission or U.S. EPA. I I I I I I I I u D D u I m <D 0:: I 0 0 • ~ 0 / .... .... 0 / I 0 0 -.j--.j- 0 / I ~ 0 ~ z ,;_; I ..J ;;: I CLIENT: U.S. EPA, REGION IV WELL NO.: EXAMPl£ -SHAU.OW WELL LONGITUDE _____ _ LATTT\JDE _____ _ PROJECT· REASOR CHEMICAL CITY/TOWN· CASllE HAYNE STATE· NORTH CAROLINA ELEV. TOP or CASING: 0RIWNG DATES: DRIIJJNG METHOD~•---"'HOll=O~W~S~lEM=--A~U~GER""-------'----- DRIIJJNG CONTRACTOR•;....---------'------ STARlED, _____ _ FINISHED, _____ _ DRILLER NAME:_• ____ _ ABOVE GROIJNJ) COIIPLBTION PROTECTM SJm.. POST EACH CORNER or CONCRETE PAD 4• X 4"' STm. PROlECl'N'E C<MJt wmt LOCKING CN> WELL PURPOSE: GROUND WA lER MONITORING REMARKS: NONE NOTES: All DEPTHS ARE MEASURED FROM GROUND SURF ACE UNLESS OlHERl'IISE NOlED NOT TO SCAI.£ PLUSH IIOONT COIIPIBTION BOTTOM OF BOR[H()l.£ .•.•. 15.5 FT. 11/A>--GROUT 5£,11. APPROX. 0.25 10 ...L9__rr. '..1---~ ... llWIE1IR BOREi0LE ....., __ SNl>PMX 2.ll....10~. ,_. __ _z_..,DWIEIDt 2J!lJ!. SlDl10> ,,_,.. SIED. sam, ....§&_ 10 ~ "· SHALLOW-WELL CONSTRUCT/ON DIAGRAM REASOR CHEMICAL SITE CASTLE HAYNE, NORTH CAROLINA FICURE 3-2 I I I I I I I I D I I '" 0 I 0 ll / " Ii 0 st st CLIENT: U.S. EPA. REGION IV WELi. NO.: EXAMPLE -DEEP YID.I. LONGITUDE _____ _ LATITUDE _____ _ PROJECT: REASOR CHEMICAL CITY/TOWN•~C_AS_TI..E~H_A_YN~E~-----STATE· NORTH CAROLINA ELEV. TOP or CASING: DRIWNG DATES: DRILLING METHOD~· ~HOLL=0~W~S~TEM~~AU~GER~--------- DRILLING CONTRACTOR·------------- STARTED, _____ _ FlNISHED,------ DRILLER NAME-· ____ _ ABOVB GROUND COMPIJ!TJOK CONCREI[ p (J'x 3'ic G"') PROTEC1lYE srm POST EACH CORNER Of CONCRETE PAD 4• X 4• STm. PROTECT1YE CCMR WITI1 lOCKIHG CN' WELL PURPOSE: GROUNDWATER MONITORING REMARKS: NONE NOTES: ALL DEPTHS ARE MEASURED FROM GROUND SURFACE UNLESS OTHERWISE NOTED NOT TO SCAI.£ YWSII IIOUNT COMPIJ!TJOK eomJM OF BOREHOl..E .• • .. 30.5 FT. i+---GROOT 5£Al. APPROX. 0.25 TO 21.0 FT. A---~ K OWIETER BORD«ll£ ----SAND PACK 23.0ro~. 1=-..+--.---2......JN. llWEER Q.QlJl. SLOTTED STMO.£SS srm. SCRmt 25.Q lO 30.0 FT. Ii 01------------------------------------·• / 11 I ...J ;;: DEEP WELL CONSTRUCTION DIAGRAM REASOR CHEMICAL SITE CASTLE HAYNE, NORTH CAROLINA FIGURE 3-3 I I I I I I I I I I I g g u D D Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 • The top of the monitor well casing will be completed with a lockable cap. • A protective, lockable, steel outer casing will be installed around the monitor well. • A brass key lock will be placed on the outer casing to maintain well integrity. • The monitor wells will be identified on the outer casing with a permanent marking, indicating the monitor well designation and total depth. • 3.2.6 Drill cuttings and development · liquids from well installation act1v11Ies will be /containerized, sampled, and profiled. for d_isposal in . accordance with all applicable (regulations.) "-.~.HJ ,.). fe-,<-r,l..,.t . ~ -Sech-3.+ Monitor Well Development The newly completed monitor wells will be developed,,~ ¥(hen the grout has been allowed to -----~------cure no less than 24 hours fnstallation. This will allow sufficient time for the well materials to --cure before the development procedures are initiated. A submersible pump will be used to remove the residual materials remaining in the wells and to try to re-establish the natural hydraulic flow conditions of the formation, which may have been disturbed by well construction around the immediate vicinity of each well. The new monitor wells will be developed until the column of water in the well is free of visible sediment,' and the pH, temperature, turbidity, and specific conductivity have stabilized. Well development water will be handled and disposed of as described in Section 3.4. 3.2.7 Monitor Well and Production Well Sampling Monitor wells and on-site production wells will be sampled to establish the aquifer conditions and to evaluate the groundwater quality. Two such groundwater sampling events are scheduled. The first event will be conducted at the same time surface water, sediment, and soil sampling is -7 . vl conducted for disposal profiling. The second event is planned to occur approximately 6 months ~,}'· ,_:... ~11,~;J1.,,.,., NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc RFW-147-2B--AMPB , .. " '7 This document was prepared by Weston Solutions, Inc., expre y . EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I g D I D D Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 after the first (Note: This sampling plan will be modified as necessary for the second sampling event when the status of the dedicated pneumatic pumps are verified.) Well purging and sampling procedures will be performed in accordance with the EISOPQAM (Region 4 EPA- SESD, November 2001, Section 7). Groundwater samples will be analyzed for total metals using CLP methods. 3.2.7.1 Calculating Purge Volumes and Well Purging Procedures Purge volumes during the well sampling phase will be computed in conjunction with the known diameter of the well casing and the standing casing water volume. To calculate the purge volumes: I. 2. Multiply the standing casing water volume by a factor of three to establish the minimum purge volume. Record the measurements and the purge volume calculation in the field logbook or on a monitor well sampling sheet. Following the determination of the well purge volume, the well will be purged prior to collecting groundwater samples. All of the existing monitor wells have dedicated, submersible, pneumatic pumps that were installed during the remedial investigation activities. WESTON plans to utilize these dedicated pumps for purging and sampling. The existing production wells will not have dedicated pumps and the following procedures will be used for purging. In addition, these procedures may also be used in the existing monitor wells if any of the dedicated pumps fail to operate: By submersible pumps NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 3-10 RFW-147-28-AMPB This document was prepared by Weston Solulioos, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I a H n R I. 2. 3. 4. 5. 6. 7. 8. By bailer: Lower a submersible pump into the well. Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 Set the pump intake as high in the water column as practical so that the entire water column will be affected during the purge. Adjust the pump height or the flow rate, as necessary. Record the adjusted pump flow rate, the time of adjustment, and the new flow rate in the field logbook. Start the pump. Using the start time, initial flow rate and, if applicable, the adjusted flow rate(s), and time of adjustment(s), calculate the volume removed during pumping and compare the actual pumping rates to the calculated minimum and maximum purge volumes. Record the actual flow rates and any adjustments into the field logbook. Record observations regarding water clarity, color, and odor; field weather conditions; and any unusual conditions. 1. Lower bailer into the well. 2. Calculate the volume of standing water in the well. 3. Calculate the purge volume. NOR/K:\WP\20064\ 14 7\FSP-RevO-F eb03.doc 3-11 RFW-147-28-AMPB This document was prepar-ed by Weston Solutions, Inc., expressly for U.S. EPA. Jt shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I n D I I I I 4. 5. 6. Calculate the volume of water the bailer will remove. Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Lower the bailer into the well, fill the bailer, and deposit the water into an appropriate container until the required volume of water has been purged from the well. Record observations regarding water clarity, color, and odor; field weather conditions; and any unusual conditions. Purge water will be collected and/or containerized, and emptied into one of the four on-site ponds for disposal with surface water during the remedial action activities. Pumps or hailers will be decontaminated after use in each well. 3.2.7.2 . Temperature, pH, and Conductivity Readings ---(.~J:1a During the well purge, the temperature, pH, and conductivity of the effluent will be periodically checked. Procedures for measuring temperature, pH, and conductivity are as follows: I. 2. 3. 4. Collect approximately 3 ounces of purge water in a clean, wide-mouth glass jar. Measure pH, conductivity, turbidity, and temperature of the water using field instruments. Collect a minimum of three separate readings of each parameter during the well purge. Rinse the collection jar with distilled water between each reading. NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc ~ RFW,147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I D 0 I I I I I I I I I 5. 6. Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Record all measurements in the field logbook or on a field water sampling sheet. Purging activities will be considered complete when 3 readings for each parameter agree to within 0. I standard pH units, 0.5 degree centigrade, and to within 5 percent microhms, or when 5 volumes have been purged from the well. . , '7 L+vrb,L7 1 3.2.7.3 Groundwater Sampling Procedures for collecting each groundwater sample are as follows: I. 2. 3. 4. 5. 6. Put on a clean pair of surgical gloves. Lower the pump into the well (if dedicated pump not in place). Completely submerge the pump into the water column and start pumping slowly (if dedicated pump not in place). Fill the appropriate sample bottle. Preserve the sample as soon as possible ( unless the bottle is already preserved or is to be unpreserved). Decontaminate all sampling equipment as per following equipment decontamination procedures. 3.3 FIELD QC SAMPLES The collection of quality control (QC) samples and sampling frequencies are described in this section. ~ NOR/K.IWP\200641147\FSP-Rev0-Feb03 doc (3]~ RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I g D I I I I I I I I I I 3.3.1 Equipment Rinsates Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Equipment rinsate are samples of the final analyte-free water rinse from equipment cleaning. One equipment blank will be collected and analyzed for Target Analyte List (TAL) metals during each groundwater sampling event. 3.3.2 Field Duplicates One field duplicate sample will be collected during each groundwater sampling event. The duplicate sample will be collected immediately following collection of an actual groundwater sample. 3.3.3 Material Blanks Material blanks consist of samples collected from the materials used to construct monitor well filter packs, seals, and grout. One sample will be collected during the monitor well installation phase from the sand used to create the filter. pack, the bentonite pellets used to create the seal, the grout used in the outer annulus of the well, and tap water (if used to prevent bridging). The samples will be analyzed for T AL metals. 3.3.4 Matrix Spike/Matrix Spike Duplicate Additional sample volume for the matrix spike/duplicate (MS/MSD) will be obtained at one sample location and collected into the appropriate sample containers as the field duplicate. NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 3-14 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. H shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I D n I I I I I I I I I 3.3.5 Inorganic Blanks Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 An inorganic sample preservative blank will be preserved in the field at the end of field operations. An inorganic sample container will be filled with analyte-free water and transported to the field and preserved and submitted for T AL metals analysis. 3.4 RESIDUALS MANAGEMENT I ~-~ L' ...,ti.,__ All excess soil cuttings generated during the installation of the new moni'F wells will be placed in the drum disposal area, which will be sampled for waste profiling. · This soil will remam staged on site until it is sent off-site for disposal with the pond sediments and soil during the remedial actions. I'/ c, All water generated from investigation activities will be containerized on-site in 55-gallon drums or placed into a mobile polyethylene tank. The water will eventually be transferred into one of the four ponds on site for disposal during the remedial action. 3.5 SAMPLE PACKAGING WESTON will follow EP NSESD Region 4 protocols concerning sample container requirements, preservation, and holding times during project sampling activities. Details regarding EPA protocols are contained in Appendix A of the EISOPQAM. The laboratory will provide sample bottles. For samples requiring preservation, the preservative will be added to the sample container prior to sample collection. NOR/K:\WP\200f?4\147\FSP-Rev0-Feb03.doc RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., eipressly for U.S. EPA. JI shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I I 0 E I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 3.5.1 Completing Sample Collection Field Records Field records, including field logbooks and/or field forms will be completed at the time the sample is collected. Once the sample has been collected, the sample collector(s) will complete the field records as follows: I. 2. 3. 4. Complete the field record with the following information: • Unique sampling or log number • Date and time • Source of sample (including name, location, and sample type) • Other pertinent field data Sign and initial the field record, including the date and time. Record the time, date, site location, and a brief description of the subject in the field logbook. Turn over the samples to the appointed field custodian. The site manager will document each transaction and the sample will remain in his/her custody until it is shipped to the laboratory. 3.5.2 Completing Sample Labels and Tags Each sample must be sealed immediately after a sample is collected. A label will be affixed to the sample with pertinent information recorded using waterproof ink. Label tags may be filled out prior to collection to limit handling of the sample containers. NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 3-16 RFW-147-2B-AMPB This document was pr-epared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I u u I I I I I I I I Reasor Chemkal Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 The site manager will be responsible for overseeing the labeling of each sample. The site manager will ensure that labels are completed as follows: I. 2. 3. 4. 5. Using waterproof ink, complete the label with the following information: • A sample identification number • The date and time of collection • The preservative used • The analysis required • The collector's initials If a label is not available, legibly inscribe the above information onto the container with waterproof ink. Wipe sample container dry. Affix a standardized tag/label on the sample container. Place the labeled sample container, chain-of-custody record, field records, and analysis request form in a transportation case. Seal and Jock the transportation case. 6. Note lost, voided, or damaged sample tags in logbook. When a lockable transportation case is not convenient or available, seal the cap of the individual sample container in a way that any tampering would be easily detected. All samples will be identified with sample numbers usmg abbreviations for sample type, including: NORJK:\W P\20064\ 14 7\FSP•RevO-F eb03.doc 3-17 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed In whole or in part without the express written permission of U.S. EPA. I I I I I n I I I I I I I I I I I • SS -surface soil • SW -surface water • SE -sediment • MW -monitor well • MBL -material blank • RBL -rinse blank • MS/MSD -matrix spike/matrix spike duplicate • TBL -trip blank • IBL -inorganic blank Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 All samples collected during the field investigation will be identified according to the following procedure: (!) site name abbreviation, i.e., RC; (2) sample type abbreviation; (3) sample location. For example, a groundwater sample collected from the new monitor well location 15 will be identified as RC-MW-15. A composite surface soil sample will be identified as RC-SS- COMPI. 3.5.3 Sample Packaging and Shipment Samples _will be packaged and shipped in accordance with U.S. Department of Transportation and International Air Transport Association (IA TA) requirements. One of the field team members will be designated as the Sample Custody Officer. In addition to being responsible for maintaining proper Chain-of-Custody procedures, the Sample Custody Officer will also be responsible for coordinating the packaging and shipment of samples. The Sample Custody Officer will contact the analytical laboratory on the day of each shipment of samples and provide the laboratory with the type and number of samples to be shipped. 3.6 EQUIPMENT DECO NT AMINA TION PROCEDURES Decontamination procedures to be used in the field investigations at the project site will be designed with respect to the intended use of the equipment. Decontamination procedures will be NOR/K:\WP\20064\147\FSP-Re\JO..Feb03.doc 3-18 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., eipressly for U.S. EPA. It shall not be released or disclosed In whole or in part without lhe express written permission or U.S. EPA. I I I I I I I 0 u I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 conducted prior to and post sampling activities, and in accordance with EP NSESD Region 4 EJSOPQAM. 3.6.1 Monitor Well Instruments 3.6.2 1. Rinse equipment with potable water. 2. 3. 4. 5. Wash equipment in solution of phosphate-free laboratory detergent and potable water. Rinse equipment with potable water. Rinse equipment with analyte-free water. Place equipment completely inside plastic bag. Submersible Pumps and Hoses I. Wash and scrub the equipment in a solution of potable water and phosphate-free laboratory detergent. 2. 3. 4. Thoroughly rinse the equipment with potable water. Submerge the equipment in a clean drum filled with potable water and activating the pump. Rinse the equipment thoroughly with analyte-free water. 5. Place the equipment inside a plastic bag so that no portion of the equipment is NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 3-19 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., eipressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA. I I I I I I I I D 0 I I I I I I I 6. exposed. Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Wrap the bag around the instrument and secure opened end. 3.6.3 Augers and Tools I. 2. 3. 4. 5. 6. Remove excess soil and mud from the equipment at the sampling location. Steam clean the equipment thoroughly with hot potable water and soap. Rinse the equipment thoroughly with tap water. Allow the equipment to air dry as long as possible. Wrap the equipment with aluminum foil (if appropriate) to prevent contamination if equipment is going to be stored or transported. Use clean plastic to wrap augers. 3_7 DOCUMENTATION AND CHAIN-OF-CUSTODY PROCEDURES All information pertinent to field activities, including sampling, must be recorded in various ' forms. This section describes each documentation form and the information to be recorded for each form. Each sampling team must keep detailed records of inspections and investigations, and review notes before leaving the site. The purpose of document control is to assure that all documents for a specific project are accounted for when the project is completed. Accountable documents include items such as logbooks, field data records, correspondence, sample tags, graphs, chain-of-custody records, and NOR/K:\WP\20064\147\FSP-Rev0-Feb03.doc 3-20 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the e:1press written permission of U.S. EPA. I I I I I I n D I I I I I I I I I I Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 analytical records. Each document should bear a serial number and should be listed with an assigned number in a project document inventory assembled at the project's completion. Waterproof ink must be used in recording all data in document bearing serial numbers. 3.7.1 Field Logbook All information pertinent to a field activity must be entered in a bound book with consecutively numbered pages. Entries in the logbook must include, at a minimum, the following: • Date and time oflogbook entry • Weather conditions • Field observations • Log and summary of daily activities and significant events • Description of sample and sampling location • Date and time of samIJle collection • Number and size of sample taken • Collector's sample identification number(s) and/or name • References such as maps or photographs of the sampling site • Any field measurements made such as pH, flammability, or explosivity • Results of calibrations and field measurements • Name and affiliation of personnel or visitors on-site • Notes of conversations with coordinating officials • Decontamination activities NOR/K:\WP\20064\ 14 7\FSP•RevO-F eb03.doc 3-21 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., e1pressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission or U.S. EPA. I I I I I I n u Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDR~A424 Revision: 0 Date: 12 February 2003 • Reference to other field logbooks or forms that contain specific information pertinent to field activities • Discussion of problems encountered and their resolution • Discussion of deviations from the Work Plan, EPA SOP, or other governing documents Because sampling situations vary widely, notes should be as descriptive and as inclusive as possible. Someone reading the entries should be able to reconstruct the sampling situation from the recorded information. If anyone other than the person to whom the logbook was assigned makes an entry, he/she must date and sign the entry. 3.7.2 Chain-of-Custody Procedures I Written procedures must be available and followed whenever samples are collected, transferred, stored, analyzed, or destroyed. The primary objective of these procedures is to create an accurate I I I I I I I written record that can be used to trace the possession and handling of the sample from the moment of its collection through analysis. A sample is in someone's "custody" if it is: • in one's actual possession • in one's view, after being in one's physical possession • in ones' physical possession and then locked up so that no one can tamper with it • kept in a secured area, restricted to authorized personnel only 3.7.3 Custody Transfer and Shipment When transferring samples, the transferee must sign and record the date and time of transfer on the Chain-of-Custody record. Custody transfers made to a sample custodian in the field should account for each sample, although samples may be transferred as a group. Each person who I NOR/K:IWP\20064\147\FSP-Rev0-Feb03.doc 3-22 RFW-147-28-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part I without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I g n D Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Dale: 12 February 2003 takes custody must fill in the appropriate section of the Chain-of-Custody record. To limit the number of custody records, the number of custodians in the Chain-of-Possession should be kept to as few as feasible. When shipping or transporting samples to the laboratory, the following procedures will be followed: I. 2. 3. 4. 5. Complete Chain-of-Custody information as described in this section. Include Chain-of-Custody and other pertinent forms and records with package to be sent to the laboratory. Retain a copy of the forms. Mail packages by registered mail with return receipt requested or by common carrier. When packages are shipped by common carrier, retain the receipts as part of the permanent Chain-of-Custody documentation. The laboratory will return a copy of the completed Chain-of-Custody with the analytical results. Samples to be shipped must be packed so as not to break the package seal or locked so that any tampering can be readily detected. NOR/K:\WP\20064\ 147\FSP-RevO-F eb03.doc 3-23 RFW-147-211-AMPB This document was prepared by Weston Solutions, Inc., expressly for U.S. EPA. II shall not be released or disclosed In whole or in part without the express written permission of U.S. EPA. I I I I I I I I I I I I I I I I I I I SECTION 4 QUALITY ASSURANCE OBJECTIVES 4.1 DATA QUALITY OBJECTIVES Reasor Chemical Company Field Sampling and Analysis Plan WA No: 147-RDRD-A424 Revision: 0 Date: 12 February 2003 Data Quality Objectives (DQOs) are qualitative and quantitative references as to the quality of data obtained from field-related sampling activities that allow or support administrative decisions and/or regulatory action. Data generated will be used in the decision-making process leading to the remedial action. The investigative methods and associated DQOs are detailed in the project Quality Assurance Project Plan (QAPP). 4.2 INTENDED USE OF THE DATA The intended use of the data generated as a result of the RD is to monitor groundwater quality for metals concentrations and to profile surface water, sediment, soil and surface soil to finalize disposal options. This data will be made available to potential bidders for remedial action activities. NOR/K:\WP\20064\ 147\FSP•RevO-F eb03.doc 4-1 RFW-147-28-AMPB This document wu prepared by Weston Solutions, Inc., expressly for U.S. EPA. It shall not be released or disclosed in whole or in part without the express written permission of U.S. EPA.