NCD981475932_19870520_FCX Inc. (Washington Plant)_FRBCERCLIS RI_Site Investigation Report-OCR

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SITE INVESTIGATICN REPORI'
FCX-Washington
NC D981475932
Washington, NC. 27889 ' J
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North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary
Ronald H. Levine, M.D., M.P.H.
Ms. Denise Smith
EPA NC CERCLA Project Officer
EPA Region IV waste Division
345 Courtland street, N.E,
Atlanta, GA 30365
Dear Ms, Smith:
20 May 1987
SUBJECT: Site Investigation Report
FCX -Washington NC D981475932
Washington, NC 27889
State Health Director
Enclosed please find the Site Investigation Report for the subject
site. conclusions and recommendations are based on a review of the available
data, conversations with FCX officials, an on-site inspection, and laboratory
analyses of samples collected during the on-site inspection,
High concentrations of pesticides and organics were found in samples
·of soil taken from an on-site area of past waste chemical burial, The waste
is deposited within five feet of the water table aquifer which recharges a
deeper aquifer used as a water supply by 2850 people within three miles of the
site. Four water supply wells around the site were sampled and found to be
uncontaminated. There is, however, concern that the pesticides and organics
might eventually migrate into the groundwater supply for the area.
If you have any questions, please contact me at [phone],
GN/tb/0175b
sincerely,
1::::: ~=:c ceoso,;s,
CERCLA Unit
solid and Hazardous waste Management Branch
Environmental Health Section
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SITE INSPECTION REPORT
FCX -Washington
NC D981475932
Grimes Road
Washington, Beaufort County, NC 27889
20 May 1987
By
Grover c. Nicholson, Geologist
Solid and Hazardous waste Management Branch
CERCLA Unit
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EXECUTIVE SUMMARY
FCX -Washington is located at the intersection of Grimes Road
(SR 1402) and Whispering Pine Road (SR 1404) in Washington, Beaufort County,
North Carolina 27889. The latitude is 35° 32' 36" and the longitude is
077° 04' 27'. The site, approximately eight acres in size, lies just to the
west-northwest of Washington city limits. The Tar River is less than one mile
to the south. About 11350 people live within three miles of the site, 2850 of
whom obtain their water supply from private or community wells. In the early
1970s, a trench approximately 12 feet by 250 feet by 10 to 12 feet deep was ___ _
dug and filled with waste pesticides, herbicides, and other agricultural:;~
chemicals. Samples of the surface soil from the trench area showed
concentrations of various hazardous constituents, including Chlordane, Aldrin,
DDT, DDE, Dieldrin, carbondisulfide, hexachlorobenzene, naphthalene,
phenanthrene, acenaphthylene, fluorene, dibenzofuran, 2-methylnaphthalene, and
mercury. These chemicals may move into the groundwater of the Post-Miocene
surficial aquifer which, together with the Miocene Yorktown aquifer, locally
recharges the underlying castle Hayne aquifer. The castle Hayne aquifer,
which top surface is about 30 feet below land surface at the site, is the
major water supply aquifer for wells in the vicinity.
The site, owned by FCX, Inc., 609 st. Marys Street, Raleigh, NC 27602
from 1945 until 1986, was used for repackaging and sales of herbicides,
pesticides, and other farm chemicals. In the summer of 1986, the facility was
sold to Fred Webb, Inc., P.O. Box 158, Greenville, NC 27834. The warehouse
on-site is to be used for grain storage. There have been no known remedial
actions to date; however, FCX, Inc. has employed Rose and Purcell, Inc. and
GSX to study on-site contamination and to recommend clean-up procedures for
the burial area and the warehouse.
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BACKGROUND
Location
The FCX -Washington site is located in the west quadrant of the
intersection of Grimes Road and Whispering Pine Road (SR 1404) in Washington,
Beaufort County, North Carolina 27889, The latitude is 35° 32' 36' and the
longitude is 077° 04' 27" (Reference 12).
Site Layout
The FCX Distribution Center property is approximately eight acres in
size and is bordered on the northeast by a railroad, on the southwest by a
wetland leading to the Tar River, on the northwest and southeast by
agricultural land, Land and buildings belonging to National Spinning Company,
a large textile manufacturer, lie to the south and southeast. On the FCX site
is a large warehouse with an adjoining tank farm (Reference 20 & 21). The
site of the chemical burial lies about 200 feet southwest of the warehouse. A
private well belonging to Cleon Latham is about 585 feet east of the trench
site and three wells owned by National Spinning are north, east, and west of
the site approximately 450 to 1100 feet away from the burial area. surface
drainage from the site is southwest toward the wetland and southeast toward a
drainage ditch (Reference 17), Primary population areas in the vicinity of
the site are northwest and southwest along Grimes Road (Reference 12).
Ownership and Site Use History
The site was owned by FCX, Inc., 609 st. Marys Street, Raleigh, NC
27602 from 1945 until 1986, The facility was used for the repackaging and
sale of herbicides, pesticides, and tobacco treating chemicals. wastes from
the operations were handled from late 1945 until 1985. About 1970, some
wastes were buried in a trench on-site. In the summer of 1986, the facility
was sold to Fred Webb, Inc., P.O. Box 158, Greenville, NC 27834. Apparently,
the warehouse is to be used as a grain storage building.
Permit and Regulatory History
There are no environmental permits known to have been issued nor has
there been any environmental regulation of the site.
Remedial Actions to Date
FCX Inc. has employed the engineering firm of Rose and Purcell, Inc, to
help study on-site contamination. Also, FCX Inc. has employed GSX to clear
the chemical warehouse and to recommend remedial action concerning the buried
wastes.
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summary Trip Report
The FCX property in Washington, which includes the area of the reported
pesticide burial in a trench, was in the process of being sold to Fred Webb,
Inc., just prior to the site investigation. Letters confirming approval to
conduct the site investigation were received from William H. McCullough, legal
counsel for FCX, on behalf of both FCX and Fred Webb. Additional consent
letters for inspecting, sampling, and photographing the site were signed by
Fred Webb, President of Fred Webb, Inc., and by J. Stewart Hodges, Vice
President of FCX. This was to insure full approval for the site investigation
during the ownership transition.
on 26 August 1986 Harry Holladay and Grover Nicholson met with the
following at the site:
c.A. Purcell, Jr.
J. Stewart Hodges
Cleon Latham
Steve Hall
Steve Jackson
-Rose and Purcell, Inc.
Consultant for FCX
-Vice President FCX
-Owner of associated residential property
-us EPA. surveillance and Analysis Division
-Fred Webb, Inc. representative
The purpose of the investigation and the preliminary sampling plan were
explained to all present. Holladay and Nicholson conducted a brief walk-over
of the site to re-appraise the sampling plan. It was found that GSX had used
a back-hoe to explore segments of the burial trench and an additional
previously unidentified burial area. The sampling plan was modified utilizing
the new findings to include sampling of the contaminated soils raised by the
back-hoe from the burial spots, as well as sampling from the warehouse
transfer areas, Mr. Latham's well, the adjacent drainage ditch, and the
background soil and groundwater areas.
Background soil samples and drainage ditch samples were taken in the
area of Mr. Latham's home adjacent to the FCX property. Holladay and
Nicholson donned protective equipment and entered the trench area where some
substances suspected to be pesticides and other agricultural waste were
exposed. A HNu meter was used to scan the site for volatile organics. None
were detected at concentrations above background levels. The odor on site was
like that at a garden supply store. A light wind swept the area to minimize
the exposure. Thus, tyvek suits and boots with no respiratory protection was
deemed safe as specified by the safety guide. sampling was done from 11:59 to
16:40 hours on 26 August 1986. Seven soils samples, four groundwater samples,
and one sediment sample were taken. Background soil and ground water sample
were included in this number. three groundwater samples were taken from the
deep wells adjacent to the FCX site which are operated by National Spinning.
All sampling was done following a standard sampling protocol and a chain of
custody for each sample was established on-site. Sketches and photographs
were made before and during the sampling activities.
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ENVIRONMENTAL SETTING
Topography
Reference 12, the USGS 7.5' Topographic maps, form the basis for this
section. The Site Sketch (Reference 21) shows a larger scale view of the
layout of the site. The Map Showing surface Water Flow Path (Reference 17)
shows the slope of the site as less than 3% and the slope of the intervening
terrain between the trench area and a small area of Kennedy creek to be less
than 1%.
surface waters
The closest downslope water body is Kennedy Creek which flows
southeastward into the Tar River. At the US 17/264 bridge across the river,
the Tar River becomes the Pamlico River. The river flows southeastward into
the Pamlico Sound. Kennedy creek and the Tar River are classified as Class c
waters which best usage are "fish and wildlife propagation, secondary
recreation, agriculture and other uses requiring waters of lower quality•.
The Pamlico River is denoted as Tidal Salt water and classified as Class SC
waters which best usage are "fish and wildlife propagation, secondary
recreation, and other uses requiring waters of lower quality" (Reference 22).
Geology, soils, and Groundwater
The site lies in the NC coastal Plain and is underlain by sedimentary
formations consisting of sand, silt, clay, shells, limestone, and combinations
of these lithologies. These sediments may be divided into three main
hydrogeologic units, or aquifers, based primarily on hydraulic conductivity
and other hydrogeologic characteristics. The aquifers, from the surface
downward, are: the Post-Miocene surficial aquifer or water-table aquifer
comprised of sand, silt, shells, and some clay; the Miocene age Yorktown
aquifer composed of interbedded sands and clays with some shells, and the
Eocene age castle Hayne aquifer composed mainly of shell limestone
(Reference 1).
In the area within three miles of the site, there are no extensive
confining units separating the three aquifers. Instead, the relative
hydraulic conductivities of the three units are the controlling factors in
groundwater movement. The hydraulic conductivity of the castle Hayne aquifer,
roughly 10-1 cm/sec, is 6 to 10 times greater than those of the Post-Miocene
surficial and Miocene Yorktown aquifers, which are about 1.7 x 10-2 cm/sec.
Therefore, the castle Hayne aquifer operates under semi-confined conditions
and is locally recharged from the two overlying aquifers (References 1,4,8).
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The aquifer of concern (the principal aquifer used for water supply) in
the area of the site is the castle Hayne aquifer which top lies about 30 feet
below land surface (Reference 4). The potentiometric surface for the castle
Hayne is typically 5 to 10 feet below land surface, which is only slightly
lower than the surficial aquifer's water table of 5 feet below land surface
(References 3 and 4). Water and contaminants move from the land surface
downward, slowly through the Post-Miocene surficial aquifer and the Miocene
Yorktown aquifer into the castle Hayne aquifer.
Climate and Meteorology
Land use
Average January temperature
Average July temperature
44 -46°F
78 -80°F
Prevailing Wind Velocity 9 mph SW
Emissions of pollutants 40 tons/square mile
includes particulate, sulfur dioxide, carbon monoxide,
hydrocarbons, and nitrogen dioxide.
Mean annual precipitation
Mean annual evaporation
Net annual precipitation
One year 24-hour rainfall
(Reference 7)
53.5'
41.5"
12·
3.48'
The site lies in a commercial-residential corridor about 1800 feet west
of Washington, a city of about 8500 people. Agricultural fields border the
site on the northwest and southeast and a wetland, approximately 180 acres in
size, lies between the site and the Tar River. Washington Park, a town of
about 500 people lies 3 miles southeast of the site. The Tar and Pamlico
Rivers, bordered by extensive wetlands, lie south and southeast. Within three
miles of the site to the west, north, and northwest are rural areas with most
land in agricultural use. Tranters creek flows from the northwest and enters
the Tar River about 1/2 mile upstream of the site. Both surface water intakes
for the city of Washington are on Tranters Creek (References 12 and 13).
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-I I I I ,1 I I i i ! I [ I I I I l r ' I I I Population Distribution and Water Supply These data are based on a house count from the USGS topographic map, on information about public and private water systems, and on an estimation of the percent of the city of Washington within each radius of the site. Within one mile of the site there are 994 residents, 850 using surface water from the Washington distribution system and 144 using private wells. Three industrial wells, belonging to National Spinning Company, and one surface water intake for the city of Washington are within one mile also. Between one and two miles of the site are about 6016 residents, 5100 of whom use city water, while the rest use private wells. Between two and three miles of the site are 4340 residents, 2550 of whom use groundwater while the rest use private wells. Three private groundwater supplies, Flanders Filters, Shad Bend Subdivision, and Trails End Mobile Home Park, are between two and three miles from the site also. The population served by these supplies is included in the 4340 residents. In total, within three miles of the site are 11350 residents, 8500 of whom are supplied by the city of Washington water system and 2850 of whom use groundwater. WATER SUPPLY AND POPULATION DISTRIBUTION No. houses served by private wells (from house count) No. people served by private wells (houses x 3.8 persons/home) No. people served by Washington water supply (est.) Other water supplies and no. people served by each Total No. of Residents Critical Environments Within l mile of site Between land 2 miles of site 38 144 850 Washington surface water intake Nat'l Spinning Co. wells-Industrial water supply wells 994 241 916 5100 6016 Between 2 and 3 miles of site 402 and 69 south of river 1528 262 2550 Flanders Filters Shad Bend S/D Trails End MHP (included in house count above) 4340 There are no federally designated critical environments within five miles of the site. However, a freshwater wetland approximately 275 acres in size lies adjacent to the Tar River and Kennedy Creek. It begins about 300 feet from the trench area (Reference 12 and 19). -6-Totals 750 2850 8500 11350
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WASTE TYPES AND QUANTITIES
In a telephone conversation (Reference 5) with Harry Holladay of the
NC Solid and Hazardous waste Management Branch CERCLA Unit, FCX Vice President
J. Stewart Hodges explained that, in about 1970, a burial of pesticides,
herbicides, and tobacco sucker control agent (MH30) occurred on the site. A
trench about 12 feet by 250 feet was dug 10 to 12 feet deep and intercepted
the water table. Two to three feet of soil were put back into the trench and,
then paper and plastic bags and jugs of wastes were put into the trench.
Based on observations during the site inspection it appears that the trench
was then covered with about two feet of soil. The quantity of wastes is not
known but can be estimated as 555 cubic yards based on trench dimensions of 12
feet by 250 feet by 7 feet deep.
waste types identified by sampling include Chlordane, Aldrin, DDT,
DDE, Dieldrin, carbondisulfide, hexachlorobenzene, naphthalene, phenanthrene,
acenaphthylene, fluorene, dibenzofuran, and 2-methylnaphthalene.
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sample
Location
1
2
3
4
5
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LABORATORY DATA SUMMARY
sample
Type
Sample Numbers
Inorg. Field/Lab
Org. Field/Lab
Background soil
0-2• deep
Ditch sediment
near Latham
house
Composite soil
Southeast trench
area
Composite soil
Southeast trench
area
composite soil
West end of trench
Composite soil
west end of trench
2991/17170
3201/602406
2992/17171
3202/602407
2993/17172
3203/602408
2994/17173
3204/602409
2995/17174
3205/602410
2996/17175
3206/602411
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Date
Sampled
26 Aug. 86
26 Aug. 86
26 Aug. 86
26 Aug. 86
26 Aug. 86
26 Aug. 86
Analyses Results
Code: Pest. = Pesticides
IT= Inorganic Totals,
IE= Inorganic Extractable
OP= Organic Purgeable,
OE= Organic Acid: Base/Neutral
Extractable
Pest: 0.035 ppm Aldrin
No IT, IE, OP, or OE.
Pest: 1.7 ppm Chlordane,
0.15 ppm Aldrin, 0.14 ppm DDT
0.46 ppm DDD. No IT, IE,
OP, or OE.
Pest: 35.4 ppm Chlordane,
46.3 ppm Aldrin,
OP: 6.5 ug/kg carbondisulfide
( ten ta ti ve, est. ID) •
No IT, IE, OE.
Pest: 33.4 ppm Aldrin,
0.70 ppm Chlordane,
0.62 ppm DDT, 0.26 ppm DDD,
0.22 ppm DDE & Dieldrin.
OP: 6270 ug/kg carbondisulfide
(tentative, est. ID).
No IT, IT, OE.
Pest: 159.5 ppm DDT,
37.7 ppm DDE & Dieldrin,
1585 ppm Aldrin.
28 mg/kg Hg which is 280
times background.
OE: 9333 ug/kg
hexachlorobenzene.
No IE, OP.
Pest: 12.0 ppm DDT, 27.2 ppm
Aldrin, 50.9 ppm Chlordane.
OE: 2833 ug/kg naphthalene,
7333 ug/kg phenanthrene,
7500 ug/kg acenaphthylene,
4500 ug/kg fluorene,
1167 ug/kg dibenzofuran (est.)
1333 ug/kg 2-methylnaphthalene
(est.). NO IT or IE.
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sample
Location
7
8
9
10
11
12
13
LABORATORY DATA SUMMARY (continued)
sample
Type
Composite soil
Northeast
loading dock
Composite soil
Northwest
loading dock
Sample Numbers
Inorg. Field/Lab
Org. Field/Lab
2997/17176
3207/602412
2998/17177
3208/602413
2999/17244 Groundwater
Latham well 3209/602414/602415
Groundwater
National Spinning
Co. Well 117
Groundwater
National Spinning
co. well 118
Groundwater
National Spinning
co. well 119
Groundwater
Background well
J.F. Rehm house
3001/17243
3211/602416
3216/602417
3507/603144
3508/603144
3964/17246
3217/602418
3218/602419
3503/603142
3504/603142
3750/17245
3219/602420
3220/602421
3505/603143
3506/603143
3509/603145
3510/603146
-9-
Date
Sampled
26 Aug. 86
26 Aug. 86
26 Aug. 86
26 Aug. 86
20 Nov. 86
26 Aug. 86
20 Nov. 86
26 Aug. 86
20 Nov. 86
20 Nov. 86
Analyses Results
Code: Pest.= Pesticides
IT Inorganic Totals,
IE Inorganic Extractable
OP Organic Purgeable,
OE= Organic Acid: Base/Neutral
Extractable
Pest: 0.61 ppm DDE & Dieldrin,
1.8 ppm DDT, 0.28 ppm Malathion.
No IT, IE, OP, OE.
Pest: 0.25 ppm Malathion,
0.23 ppm DDT, 0.15 ppm DDD,
0.15 ppm DDE and Dieldrin.
No IT, IE, OP, OE.
No IT, OP, or OE.
NO IT, OP, or OE.
Pest: None.
No IT, OP, or OE.
Pest: None.
NO IT, OP, or OE.
Pest: None.
No pest, OP, or OE.
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1 I MAP SHOWING SAMPL
LOCATIONS
-~-~••+
t~:-:·~-~.f'
I I I 1 , i / I , I ! . !·· I" ii 7 I I 1--'-LLL.LLL I ...
··'IFCX Warehouse :·1,-.
~. r I -1-1-.1. I I
.
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.,,,_.;i,{l -II'.-•
l!t'~ .';l\t~ . 'i!
-k -·· .. "'---~-·-. . . -. .
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TOXICOLOGICAL/CHEMICAL CHARACTERISTICS
Pathway Matrix Values
substance Groundwater surface Water Air
Aldrin 18 18 9
Chlordane 18 18 9
DDD 18 (?) 18 (?) 9 (?)
DDE 18 18 9
DDT 18 18 9
Dieldrin 18 18 9
Malathion ? ? ?
carbondisulfide 18 (?) 18 (?) 9 (?)
Mercury 18 18 9
Hexachlorobenzene 15 15 6
Naphthalene 9 9 6
Phenanthrene 15 15 9
Acenaphthylene 9 9 3
Fluorene
Dibenzofuran 18 (?) 18 ( ? ) 9 (?)
2-methylnaphthalene 6 (?) 6 (?) 6 (?)
From: Sax, N.I. Dan~erous Pro2erties of Industrial Materials,
6th Edition, Van Nostrand Reinhold company, New York, 1984,
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Appendix A
Maps and Photographs
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FCX Washington '
NCD 981 475 932
J(
,,, I I =-tot>
-LL ·o
Fe )( W i1112. E tu,us e ◊
------- -- -- ---- - -
l!!!!!!!I 1!11!
114 /15 1/6
West
Panoramic View of Site
---

-

-
liiiil iiiil liill .., --== == 111!!1 l!!!I!! l!!!l!I l!!!l!!I --
----------
117
North
---Panoramic View of Site
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Cleon Latham Well House -Inside
Cleon Latham Well House
L___ __ --------
...,
Loading Dock -Northeast side of Bldg.;
f'
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I Trench Area Trench Area
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Trench Area
---
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T • _._,,, •.
rench Area Trench Area
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Appendix B
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Laboratory Data
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<-:-,;.-, ... II C. Department of Human Rc&ourccs
111,,.ision of Health Services SAMPLE ANALYSES REQUEST
Stace Labomorv of Public Hcalch
P. 0. Box 28047
306 N. Wilminaton Srrcct
Raleigh, 27611 /.! f<J14?S-'l.12-. t-,~ ~umber O 7 L) !J::.tV!11ft2
eofSite FC.x-t,V,+o~,..,&,,r'oN
rw
Field Sample Number ---=J-f~9._../~-----------
Site Location. w,.~H,,v(,"r&A.)
elected By A(' 'J./4.-eeifiyA &-ID# _ _,£~£~--Date Collected __,2....,'-._"'19"-'v=,s,.~_..,r'-'t,.,_ __ Time
. of Sample:
I Environmental
__ Groundwater (I)
1--Surface Water (2)
__x_ Soil ( 3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid ( 6)
__ Sludge (7)
__ Other (8)
Comments
I -s 0-2 ., dt,,
I INORGANIC CHEMISTRY
Extractables Total
[ Parameter Results mg/1 Parameter Reaults mg/~ Parameter Results m11/~
!..¾..Arsenic <11-1'\I :!:Arsenic n,'-f __ silver
ltBarium < /l ., Barium <¥.'± __ Sulfates
Cadmium · < a.as-1eadmium __ Zinc /
IL Chromium S: a_. as ::!!!_chloride _Ph
ol Lead < Q, I _j(_ Chromium x". I __ Conductivity
~Mercury <o.a-:2 __ Copper _TDS • .1---._~Jtf!i4-m ____ __ Fluoride _TOC
__ Silver __ Iron --
I= ~Lead .].3 --
__ Manganese --
1----2(.Mercury < cJ-l --
~-
__ Nitrate --
__ Selenium --
I Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter Results mg/1
ORGANIC CHEMISTRY
_P&T:GC/MS _EDB __ Methoxychlor I ,__ Acid:B/N Ext. __ PCB's __ Toxaphene
_TOX __ Petroleum _2,4-D
--__ Endrin __ 2,4,5-TP (silvex)
1-__ Lindane --
MICROBIOLOGY RADIOCHEMISTRY
I Parameter Parameter Results PCi/ 1
__ (MF) Coliform Colonies/!OOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lO0mls __ Gross Beta
I= --
--
T
)ah~ Receiv<:d I Date Reported I Ve/db
Date Extracced -------------~---Date Analyzed ________________ _
leportcd By Lab Number --l1-7Hl'-17'-'-0'-,,..,.f,.l~lc ..... ;z--:1-7-tJS,.4--,----
[)HS 3101 !R~viscd 7/BS)
/2/i<'.--
I (2.~ n : : 'j·•~~·•:•('l"'~':'-''...','!;':!!.i~-~..v.,,.~,1., -
'---· ' . I · _· . . · /' ,...,._ /) C L IL .. ·_.-·· ·
N. C. Department of Human Resources . . · 1 . ffl_ o ,~Q-Laboratory of Public Health
Di,is,or.·of He~lth Services .· . . _ . SAMPLE ANAL Y_SES RE~Ur3~~J 396 N. w1'.i~!ixn 25B~~~
1)1_. 'nl_ -11!> ~--. . .. ' ,· .. · '· , .. . ·. l · . Raleigh, 27611
Site Number O? D td:l¾c:090 Field Sampl~ Nu~!i~:•p2r~z::•-""' . '
;_.-;-'
JlmeofSi~e FC.X-U,l*~H,~11,-T"o,,.; ·SiteJ..oca;ion ··w,,,$1-•n,vr,roAJ -NC.
~llected By '7./. ~-10# . 7'.8. Date Collected 2'-/9thS,• Z:6 Time ,//,'S)'
} ' (\ ··pe of Sample:
Env'ironmental Concentrate "t-Groundwater (1) ___ Solid (5)
__ Surface Water (2) ___ Liquid (6) '.· ·t-t-Soil (3) __ Sludge (7) '
__ Other (4) __ Other (8) .. ,
INORGANIC CHEMISTRY'
Extractable&
Parameter
__ Arsenic
__ · Barium
II--Cadmium ·
LChromium ---~i:~~~--
Results mg/1
~S-ilver ---
Parameter Resulu mg/ 1
Parameter
__ Arsenic
__ .. Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ fluoride
__ Iron
__ Lead-..
__ Manganese ·
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ 1
ORGANIC CHEMISTRY
Parameter Results mg/ 1
Comments
Total
Parameter
__ Silver
__ Sulfates
__ Zinc -.
_Ph
., '
__ Conductivity.' .
_ms ··
_TOC ,. J·
,I•' • l Sl ' " ··. '.
Parametei-'\, ;
Results mg/1
Results mg/ 1
-"'-P&T:GC/MS
Acid: BIN Ext.
TOX
---4--EDB ·
4PCB's
-4,-Petroleum
LEndrin
-X-Lindane
/V tf X-Methoxychlor . ---,-,r'-----
--"-_,v,-'-, .c./)_, ____ .+ Toxaphene : : ·
.X..2,4-D .,_ . <CZ· I
1-..X 2,4,5-TP (sl\'cx)
. MICROBIOLOGY RADIOCHEMI! :TRY .
C · Parameter · · · Parameter " · .. ,' Results PCi/ 1 . ' . ' '
(MF) Coliform Colonies/lO0mls __ Gross Alpha
.,
__ (MPN) Coliform Colonies/l00mls __ Gross Beta ., .. ' ·' . '
'
t=
.. , --' .. ,., .
--'.
l ate Recciv~d 1~-~,"';,7;-;'.f~/p-~~trn--t-....-· 7..,,...._~-__ Date Reported /P-9-)j 7 ·
~~~:3 =tt~vl ji[)~. . ff:.. · · (jJ.)A-. . · /Jf\ 'Pc.ST.
Date Extracted --<.,C...O=-:c..Lc:J!..!,!'--"--'><,-'>~.e=;c,,,__ __ ...::.,..,'__._-ie.:~"'"'-'''->v'--'j_,,__.f_)r~--Date Analyrerl 'l-1.i·BCc · · tj,--z;,'-f,-fl/ w, /o-/7;f/.1{P
I ~/11-,t;JJ-M. /1.{l-/ sn.240G: f.le-../4_
11~'7-K-13"P
cisortcd Dy ----1-__f_✓...,:,-f..""L.m~✓-~"-..!:.!.-+~~_,_ ___ r--'~==~----Lab Number __________________ _
I.I/ . .
I
N. C. Department of Human Resources
,.ion of Hcolth Services . SAMPLE ANALYSES REQUEST
.Dl 9frt 47-~ "JJZ r-v
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
. Raleigh, 27611
!Number O 7 l)Ji,Lfl-1:"ldo
eofSi~e FC.X-t-U,uH1Nf,,-T"oAJ
Field Sample Number --"'.:Jc"-. ..,_9_9,._-...,L~----------
Site Location. l-Uns ,..,.,.,.,,r,,ro AJ
l lccted By 1J ~ ~ ID# __ -J......;B~~ Date Collected _..z...,,:...._.,./l:z...,:;U.,.&-=---.,.,r'-'b"'---Time __./"",:l'-',..._• I,_!_-'
of Sample:
Concentrate Commenu Jnrironmcntal
{II-Groundwater ( 1)
=---Surface Water (2)
.__ Soil (3)
__ Solid (5)
__ Liquid (6).
__ Sludge (7)
__ Other (8)
5"9-P(!.<:: .,M ;J._ s -A✓-Mt{ -4,fd
/lo(9 T
g ){ Other (4-,.,i.J.
INORGANIC CHEMISTRY
ill Extractablea Total
Parameter Reaulumg/1 Parameter Resulumg/~ Parameter Resulumg/1
...X..Arsenic -< t'l . <') 1../.. L..Arscnic· ~-0 __ Silver '
·&=Barium Q • 1 _J(_ Barium ,S:.5"""" __ Sulfates .. • ···•'
Cadmium La,()~ -LCadmium < ;;2.-~-__ Zinc ,,-
-LChromium <a,as:: __ Chloride _Ph
:r=Lcad ~ o' l ~Chromium ;)... :,,-__ Conductivity
!' Mercury s:a.a-:2. __ Copper _ms
.. )---.S~Jt.t1il:'.rn. __ __ Fluoride _Toe
'.u=Silver __ Iron -·-
~Lead L°'f"S --
__ Manganese ·----
;11=
...lL-Mercury <I), I --' __ Nitrate --.
__ Selenium . --
n ORGANIC CHEMISTRY ·:;.
Parameter Reaulumg/1 Parameter Results mg/1 Parameter: Results mg/1
' P&T:GC/MS __ Methoxychlor
•.
_EDB o= Acid:B/N Ext. __ PCB•s __ Toxaphene
_TOX __ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (slvex) i II-__ Lindane --·--. i
, MICROBIOLOG r
Parameter
; __ (MF) Coliform Colonies/lOOmls ·u:= (MPN) Coliform Colonies/lOOmls
'
Parameter
__ Gross Alpha,
__ Gross Beta
RADIOCHEMI!,TRY , -~------~
Rcsulu PCi/1
1---=-------------------'-----~-------------__J
D,te Received _________________ Date Reported[ &J ~
'U' ,re Extracted--------------'----Date Analyzed
·1•<1rtcd By Lab Number __ /_/_/__./ ... /--"'-~U,.,G..._:~-'7'-lt.,.," t,!'-. _____ _
1'.l: :Departmen;,c,f.Human Resources
Oivisior~ of Health Services SAMPLE.ANALYSES REQUEST.' .
. State Laborat~ry of Public Health
. ·" P. 0. Box 28047
306 N, Wilmington Street
1,;·· . Raleigh, 27611
flmeofSi;e FC.x-U-1,HHl,J(,,,,-ON SiteLoca.ion t,.u,.r;,-n,vr.,roA) -NC.
CollectedBy ,:v'/)44...1d" lJ?# __ -'-/-'--"&'--_DateCollecred 4'-,9VG-$'6 Time /2,')/
11pe of Sample:
l\n~~onmental Concentrate t-Groundwater ( 1)
___ Surface Water (2)
-,... Soil (3) . . Bx Other ( 4) .}!,_£,
__ Solid (5)
--Liquid (6j ,• ....
__ Sludge (7) ·
__ Other (8)
Comments --c?-b ~ . . . I
INORGANIC CHEMISTRY. '.,1, j, V • ... ~ •:'. \•
'
Extractables
· Parameter
Arsenic
__ Bat'ium
ill--Cadmium ·
Ill-Chromium
I_Lead
Mercury
... ·selenium ___ _
Results mg/1 Parameter
__ Arsenic·
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ .Copper
_·_·Fluoride
__ Iron
__ Lead-
--Manganese ·
__ Mercury
__ Nitrate . ' ·
__ Selenium
Results mg/1
Total , .. .-· '' ·
·'Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ CondUctivity' . __ ms . _; ,.
_TOC ,,
Rcoults mg/1
_· ._. ''-'--------------
ORGANIC CHEMISTRY "'.j, :. '-~.
·.,. ,c'/,1,,
Parameter
Acid:B/N Ext.
TOX
Results m /1
MICROBIOLOGY
· · Pararrieter · ' ' · I=" (;_,ff) Coliform Colonies/lOOmls
-(MPN) Coliform Colonies/lOOmls
T
Parameter
__A__EDB
___&_PCB's
-4-Petroleum
_/-_Endrin
..2-Lindane
,•
Results mg/ 1
Yi%•
'
Parameter
__ · Gr~ss Alpha
__ Gross Beta
Results ~g/1
...L.. Methoxychlor
_L Toxaphene" , ✓
._X 2,4-D . : , . f#.5
-L 2,4,S-TF°(slvex) ·--"f""'A.,_J_,5L---
RADIOCHEMl/,TRY -~--------Rt· s u l ts PCi/ 1
, Date Reported -------,,-=----------ff. . ]>€ST. I
Date Analyzed ~£8¼, t2W:, /o-17-J"'t:', t/,;P,
I :l B · Lab Number ___ __:6c..-
1c..' l_Z_4_._0_? ________ _
cportc, y -------------------~~~~~~~r ~ •
N. C. Department of Human Resources State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
tion of Health Scrvic.. '7-i i-4?S 'l.r~ S;:LE ANALYSES REQUEST
Slf Number O 7 [) t,r~o Field Sample Number ------"{)."-'-'J--'9:....,;:,.5----------
~e of Si ~e FC.x -U,J,+~ H I A.I(;,, 'T"c, N Site Location .,., ..:;w...:;...:..;".::;$..;.H.:....c..1ccAJ:..<,;::...;..,._0'--",v=---•=-N;;..c:C..=-------
~lected By . ,,/J, ?rt i,k ,&v.,,, ID# 3 Z Date Collected 2 4 19 u,s,. Z' 6 Time I 'I.' I~
Ifl,eofSample:
En..:,_ronmental Concentrate ,11----Groundwater (1) Solid (5)
__ Surface Water (2) Liquid (6) · 1---Soil (3) Sludge (7)
~"-")(_ Other (4) ~. __ Other (8)
INORGANIC CHEMISTRY
Extractables
Parameter Resultsmg/1 Parameter
Arsenic 9·9 I
!Barium
Cadmium
i Chromium
<o-t · <a.a<
<o,OS::
:s =i·S::::
3
Comments
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity t-rf-Lcad :ftL Mercury· t ___ s~J~,f!iU_!_ll __
; __ Silver
e:~2
~Arsenic·
_K..Barium
~Cadmium
__ Chloride
---2!:o... Chromium
__ Copper ______ · _TDS .
!I= ' ,.
lt I •
! P&T:GC/MS !I Acid:B/N Ext.
i __ TOX
'
__ Fluoride
__ Iron
__x__ Lead
__ Manganese
_K.. Mercury··
__ Nitrate
__ Selenium
.L,o.(
ORGANIC CHEMISTRY
Results mg/1 Parameter Results mg/1
_EDB
_TOC
Parameter
__ Methoxychlor
__ Toxaphene
_·_z,4-D
Results mg/1 .
Results mg/1
I.
I: ~-----
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
--2,4,5-TP (s \vex) -i i --------------I! ______________ .,_ ______________ _.__ _____ ----------' i
RADIOCHEMl: -YRY 1 I _ Parameter · Parameter Ruults PCi/1 i
I
l __ (MF) Coliform Colonies/lOOmls __ Gross Alpha I ;)= (MPN) Coliform Colonies/lOOmls __ Gross Beta . '
•
I . --,__ ' --
MICROBIOLOGY
l
le Receivc;d Date Reported I &d:r£
llire Extracted Date Analyzed
,,1,0,tcd Ely· Lab Number l'1172 AUG2781t
IL// c:::....-
Bc·Dcpart~c~; .of Human Resources
Di"isioA Of H~alth Services SAMPLE ANALYSES REQUEST.
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
· • Raleigh, 27611 l11 't'DI 4?S91Z ~-.
Site Number ...,0"'--'7'--l'-).,___,!JJ'-41--£/_9" .. •Hif<=<..£..,"-"'O'----'-----Field Sample Number __ ,:~·3,..,'-'· z_=-· ·.c..~...;:.3::;.·_· ---------'-
B. m_ e of Si;e ~F_C.~X_-_t-V_,.._~_H_,_,.,_G-_T'<_o_,.J________ Site Location _· W "~ H' ',..;<,To AJ
~llected By ~,,8~.-J.2t><~=· ""'-'"'--"""""-'~--ID#_· _3'-'-7 __ Date Collected 1 ?'-· AvtS-$' 6
1tpe of Sample:
~nvironmental
'(I--Groundwater (1)
___ Surface Water (2)
·q .. · If--Soil (3)
II ;I,, Other (4) ~J
Concentrate
__ Solid (5)
___ Liquid (6) '-· .
__ Sludge (7)
__ Other (8) ,.
INORGANIC CHEMISTRY'
Extractables
Parameter
Arsenic
__ Bal'ium
Cadmium
Chromium
i __ Lead
-1=-~-~;~~;;_ -
--:Silver
Parameter
Acid: BIN Ext.
TOX
Results mg/1
Results mg/ 1
M.lCROBIOLOGY
Parameter 1
(MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls
Parameter
__ Arsenic·
--Bariuffi i .-
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ 1
ORGANIC CHEMISTRY
Parameter
..JLEDB
-25....-PCB's
---2{_ Petroleum
_l...Endrin
_,}£_ Lindane
Results mg/1
N-/),
N.A
Parameter·
__ Gross Alpha
__ Gross Beta
NC.
· Time /1/, . / S'
Comments"
Total· ·· '
· Parameter
_·_Silver
__ Sulfates
__ Zinc ,
_Ph
__ Conductiv'ity ·· _ms ,,_.·
__ TOC ;:··
Parametei :. i.
_x Methoxychlor
----2(__ Toxaphene.s·:
---2!=.2.4-D .. ,_-,
.....2!'...2,4,5-TP (s·lvex)
Results mg/1
Results !Di'!/ 1
RADIOCHEMit-1.1lY. ---'-'-"----------
R c. s u Its PCi/ 1
l ate Received ",{·;J..7-{r/, 1/,P • Date Reported __________________ _
. PcST.~/'iL.:i) "i}-D. . Pr_. · "?CST.·
Date Extracted 9· ;;:zt, -%b VT-: Date Analyzed 'l-l'i?-6'11 n«r IO·'/ Z-d'.h z{P -.
lcportcd By"-------------------Lab Number Gn2llc')8
g
C. Department of Human Resources 1f'" of Health Service• _ . SAMPLE ANALYSES REQUEST
/j" ' 'r'I I -f? ~ 9sZ-r1
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
t1fumber O 7 ()!§,lf,,lb;/lZO
a.llofSi;e FC.X-t-V,HH,-.,r.,.-ro,,.J
Field Sample Number _ _,,2,._-_';[......,.'j:......,.Y---------
SiteLoca:ion _ W,t$H,,.Jl/,-roA.J NC..
oW.cted By ,4. )1, -~
yjl of Sample:
ID# _ _..5...,7..._ __ Date Collected _.z.._.,4.._.c;/9z..e:;U.,,.S-::.___.1$'=6,__ __ Time
Env'ironmental -I--Groundwater (1).
___ Surface Water (2) ·1--Soil (3)
I
K Other (4)~
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Commenu
Extractables Total
-
Parameter Result& mg/1
..X..Arsenic < O·I 0
!Barium :Sea-I
Cadmium · <c.i,a \
~:~~ Chromium
*Lead Mercury
-Selenium ---------.. I Silver
-·-=It
Parameter Reoulu mg/1
r P&T:GC/MS fl= Acid:B/N Ext. LTOX
q ------------,
·-4 •
MICROBIOLOGY
Parameter
~--_(MF) Coliform Colonieo/lOOmls
~-I=' (MPN) Coliform Colonies/lOOmls 1 .
:i
Parameter Resulu mg/~-
~ Arsenic· /-"
1Barium <C:-
...,ll-Cadmium /Q ' __ Chloride
.....::,L Chromium £Z
__ Copper
__ Fluoride
__ Iron
--X-Lead ~o
__ Manganese --,'L Mercury o-:-i3_
__ . Nitrate .
__ Selenium
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Result& mg/1
Parameter
__ Gross Alpha
__ Gross Beta
Parame.ter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_Toe
------------
Parameter
__ Methoxychlor
__ Toxaphene
_._2,4-D
__ 2,4,5-TP (, !vex)
Resulumg/1
-! ' : ,.-.. -.. , .. ,
Results mg/ 1
RADIOCHEMI: ·,_.·R~Y._. _____ _
R, sulu PCi/ 1
':,-,---------------------'-------,----------------..J
c Received -----------'---------Date Reported --'-/_,,<9c"-'-"''L:"--~-=-=----------
l"le Extracted-------------~---Date Analyzed
, ,nrtcd By Lab Number __ 1_-_l_i _7.:;.J_4U.;..u.=.~.e.C.L7..,_81-11it'--------
12./1 2:--
i-.t: De;,artm
0
en; of.Human Resources
Division· of Health Services SAMPLE ANALYSES REQUEST ...
State Laboratory of Publi~ Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611 l,1· "/f'I-Rs"J?Z ,,,,_.,.,
Site Number -'D"'---7'--l'--"),G...,!4'-!e!-"/_¼=-c..~~'-"--"'o'--_fl _____ Field Sample Number---~• -?..,__2.._o---'.<f ________ _
fne of Site _:.F_C.=X.:..----=U,J.~,._'-'--'s-'-H-'-'-,_A,_G,-=-..;~_o;c;..;.;.J.:.._ _______ · Site Loca::'ion · W "$ H ',v r,, To A..J ,NC.
Collected By ~J~-~4~'-'~-~~~~~·---ID# --3"--'7'--·--Date Collected ' 2 '-' /9U6-Z' 6 Time °J'/.'2-2.-·
1(1:,eofSample:
~n~ronmental It-Groundwater (1)
___ Surface Water (2)
·1--;-Soil ( 3) .
., K Other (4) ~
Extractable&
Concentrate
__ Solid (5)
__ Liquid (6)' · '
__ Sludge (7)
__ Other (8)
. '
INORGANIC CHEMISTRY
Comments
.,,, -' ;.,·, '"-.,
Total . ,· "' /., ,• ' •
.
-II: Parameter Results mg/ 1 Parameter Results mg/ 1 Parameter ,' · Results mg/1
__ · Arsenic
_._._Barium II= Cadmium ·
_Chromium·
__ Lead
.1:_~;;~~~;_ -
__ Silver
II= --
E
Parameter
P&T:GC/MS ·
Acid:B/N Ext.
TOX
Results mg/ 1
MlCROBIOLOGY
1 Parameter ·
_·_·(;,,ff) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
I=
__ Arsenic
_·_.Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate. .
__ Selenium
ORGANIC CHEMISTRY
Parameter
_K.EDB
_lS_PCB's
~ Petroleum
--2i. Endrin
..;X..,Lindane
.
Results mg/ 1
N-1/,
{'(,[)'
Parameter
__ Gross Alpha
__ Gross Beta
----
;
'
,.
__ Silver .
__ Sulfates
__ Zinc
_Ph
__ Conductivity .. __ ms f. ·~.r
__ Toe · t~•
----.. -----. ----. :
Parameter,·; Results mg/ 1
'· t/ ' ...2L_ Methoxychlor.
_2f...._ Toxaphe,ne .
_X_Z,4-D ·· .. ·· · ,<.0, /.
_x_ 2,4,5-TP0
(s'l\'CX) -'c=o_,_,_{ ___ _
RADIOCHEMl: TRY , .
:.,. ·•1 R"sults PCi/ 1 ' .. , .... ..
.,
'•"
' '' ,._ ' . ;\ : ,.,, "• , . ,,
' '' .,
'·'
I R d ?-,;i.7-5[/ D, '), D R d .. • ate eccive ~-~-~-"e?,-=<L-'~,,~-__________ ate eporre ~~--· _____ _:._ _____ ...:_ __ _
P£;,~,-/l..9 8, D, .. ft . 'k:sr.
Date Extracted 7 -.,M -_ 4/,B Date Analyzed 'l-@-$1 '74: I_, /0-·/'7-Y,l!;·r,P,
I Lab Number 6 '.>2•10'9' •• ',, ·
cportcd By
I
J. C. Department of Human Resources
>l'ion of Health Servicca . SAMPLE ANALYSES REQUEST·
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
-~ 91'I ~?S 972 ~
ig Number O L I) !!J~ . ---Field Sample Number _ __ad..._.9'-•"-9_,6.,_ _________ _
,11,eofSite FC.x-t-U,HHl~f,,-T'OAI . Site Location ....:::lV:.::...:..:".:.S.:.H.:...c.•.::.,..,:..<,=r...:o:...::.-,.J::__N==C.=--------
ii1ected By df. Jt, ~-ID# __ 3~7 ___ Date Collected __.z"'-"4._.l9a..,V<-'<>-"'--'$"-"6~--Time ;c,t.'3o
rile of Sample:
Env'ironmental
1 I---Groundwater (I)
___ Surface Water (2)
Concentrate
__ Solid (5)
__ Liquid (6) .
1-Soil (3) __ Sludge (7)
__ Other (4) . __ Other (8)
INORGANIC CHEMISTRY
Extractablea
Parameter
LArscnic
l
~t~:7um ·
Lead
Reaults mg/1
<o-o, -<a-I -<a -o< -<a .o< < o. l
Parameter
_ilArsenic·
....:;L.Barium
--tCadmium
__ Chloride
Comments
Total
Parameter
__ silver
__ sulfates
__ Zinc
_Ph
__ Conductivity t~ Chromium
Mercury
-Sek11i4._m __
__ Silver
<a,o?, LChromium
__ Copper
__ Fluoride
__ Iron
______ · __ ms
1=---
-·-
I=
I Parameter Results mg/ 1
_P&T:GC/MS I-Acid:B/N Ext.
_TOX
--
I=. -
M!CROBIOLOGY
-1Lead
__ Manganese ·
_LMercury
__ Nitrate.
__ Selenium
ORGANIC CHEMISTRY
Parameter Results mg/1
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
_TOC
Parameter
__ Methoxychlor
__ Toxaphene
_·_z,4-D
--2,4,5-TP Is lvex)
----
RADIOCHEMl: TRY
Reaultsmg/1
Resultsmg/1
-
-~-------
Parameter
__ (MF) Coliform Colonies/l00mls F (MPN) Coliform Colonies/lOOmls
Parameter
__ Gross Alpha
__ Gross Beta
R <Sul ts PCi/1
Ire Receiv~d -----------'-------Date Reported --'-->-'-.I-<::_ ___________ _
~te Extracted-------------~---Date Analy,ed
:l;,ort<:d fly Lab Number __ t _7_1..c..7_4-'-'-AU"--G~?._7 ..... ~ ..... , _____ _
/ 2,/,1 2..-
JC:Dcpanmsn;.of Human Resources State Laboratory of Public Health
Divuion of Health Services . SAMPLE ANALYSES REQUEST . , . ,
l1 · f~, -?-15'l;'Z '!r"-' · .
P. 0. Box 2804 7 .
306 N. Wilmington Street
. Raleigh,.27611
Sire Number ~0~2:__.( ... )~_b-'=':..P,._~(=~--~--t'>-______ Field Sample Number -~;_3'~· 2..,~· D_--_-_:;; ________ _
JL. e of Si~e ~F_C.=)(-'--~t.-U.-'----,,..'--~-H-'--1_,..,_G--'--'T"'._o_AJ ________ · Site Loca;:ion . I.A/"~ H 1 "-' <, -ro -.., -NC.
~ected By __..L!....__,_/Z,..1-"~='-="'~'----ID# --=3__,7~·--Date Collected _.2.,_..'-._.19~· -"V'-'6-'--__.· 1$'....,,6'----Time I 't,' 3 C)
·~£Sample:
Environmental 11--Groundwater (I)
___ Surface Water (2)
·,-·a--;-Soil (3)
/X Other ( 4) c.n,.,.~.
Concentrate
__ Solid (5)
__ Liquid (6) 1 • •
__ Sludge (7)
__ Other (8)
·, · Comments
' INORGANIC CHEMISTRY
Extractable&
Parameter
__ · Arsenic
_._BaI'ium
Lcadmium,
Lchromium
__ Lead
.. l=_~J;~~;~_ .. _
__ Silver
Results mg/ 1 Parameter
__ Arsenic'
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese •
__ Mercury
__ Nitrate . ·
__ Selenium
Results mg/ 1
Total
Parameter
__ Silver·
__ Sulfates
__ Zinc
_Ph
_______ . _._ Conductivity ·· .
__ ms .1 __TOC .·• ' ..
. ,' . .. ,,.
Results mg/1
ORGANIC CHEMISTRY
Parameter
.:i,._P&T:GC/MS
Acid:B/N Ext.
TOX
Results mg/1
MICROBIOLOGY · I==-Parameter ·
(MF) Coliform Colonies/lO0mls
_._ (MPN) Coliform Colonies/l00mls
I=
l ateReceiv~d ?("-,;27-·,T'!, "7!;:l>;
f' c S 7: 4-,,-; Z3J_q l>
Date Extracted Cf'-,;y,-7G' y: P.'
Parameter
1EDB
-1LPCB's
---d'... Petroleum
~Endrin
-1£.Lindane
•
'
lcportcd By· __________________ _
Results mg/ 1 Parametei-" .. · Results mg/ 1
11/,/J' ---X Methoxychlor
/1/, 0,
;V./1. v
-L Toxaphene
-1L2,4-D . ' ' '
_..l!.. _2,4,5-TP (s'lvex)
,._,.......
RADIOCHEMit;TRY -
Parameter
.,, . R<.sults PCi/1 .I ., .,
__ Gross Alpha
__ Gross Beta I
.. ~
•' .. i. --: .. ' ... --: ,,; ·t
l' ."
Date Reported=-----,=-==----------fr_ . p,E-.:,,; '
Date Analyzed r-,12·8'/a 71a.l·, /,:J "/7-U·f,?,
Lab Number 6'}2410'.:
I
..J. C. Department of Human Resources
)'ion of Health Services _ . SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
.Dl 9"14?5 9JZ :,--·
l.. Number O 7 l)J.tt~ Field Sample Number _ ___.·,:Z__.5? ... 7'._6....__· ----------
eofSi~c FC.x-t,C,l,~~Hl~(;T"ON
~lccted By .If. 0, 'Ji~ · 10# _ _,_?~7,__ __ Date Collected _.z.,_,."..__~19.w:cP.,,t!:-c...-JZ'"-"'6'----Tim~ /ffJ~
Il,.ofSample:
En-rironmental
/~ Groundwater (q
__ Surface Water (2) 1--Soil (3)
_.:j__ Other (4)~f"
Extractable&
· Concentrate
__ Solid (5)
__ Liquid (6) ..
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Commenu
Total
I Parameter Reaulu mg/1 Parameter Results mg/~ ·. Parameter Reaulumg/1
·Ql _:;{_Arsenic <a.1 Ii Barium Cadmium · < a ,as,-
Chromium <Q.O~
t:Lcad Q,3
Mercury < Q, Q ,::,_
~SeJ~'!il!...m __
__ ,Silver
11=·
-·-
II=
I Parameter Results mg/1
_P&T:GC/MS I-Acid:B/N Ext.
_TOX -·
--I=
MICROBIOLOGY
Parameter
__ (MF) Coliform Colonies/lO0mls F (MPN) Coliform Colonies/lOOmls
(,. 'I .
_.}L Arsenic ·
.X Barium ~o
___,lL Cadmium :s: ~. ::i-
__ Chloride
_J.Chrornium 70
__ Copper
__ Fluoride
__ Iron
~Lead S-D
__ Manganese
....J(...Mercury ('), z,
__ Nitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Petroleum
__ Eridrin
__ Lindane
Results mg/1
Parameter
__ Gross Alpha
__ Gross Beta
__ Silver . ,·· .
__ Sulfates -__ Zinc . ,
_Ph
__ Conductivity
_ms
_· _TOC
----------. --
.
Parameter Rcaulumg/1
__ Methoxychlor ..
__ Toxaphene
_·_z,4-D
__ 2,4,5-TP (s !vex)
. --··-
RADIOCHEMt TRY -----------
Resulu PCi/1
lie Recciv~d ----------'--------Date Reported _ _,_/_&,......__~.,.·,../--'--_f(; __________ _
i''e Extracted ____________________ Date Analyzed
l:portcd By Lab Number ___ l.:...{.:...j .:...(:::,)_,Aco,U,._,Go.J("--'' (r.....,_t; '-' ____ _
/ 2,/J 2.--1·· ' ..
N. C. Dcpartrr.ent of HUman Resources
Di-is ion of Health Services SAMPLE AN AL YSES REQUEST
l 1 'l'i'I -1?-S' 9_ff'Z ~
. State Laboratory of Publi~ Health
P. 0. Box 2804 7
306 N. Wilmington Street
. Raleigh, 27611
Site Number _O~?c.-t ... ?"-'t,',,;d:'. .... =~~'--...... ~-------Field Sample Numbe~ _•·'_· __ 3~z._·o~b~-----------
lme of Si;e _,_F_C.=X-'---"t,.V---'-',.."--~-H-'-'-1-~_6-=--r._o"-AI--------NC.
Collected By -L' .. ·.,_.,__.,_}z,.,_1_._c .. ~====----ID# --3'--'--? __ Date Collected _.2='-"-/9=V=G--·__.z:,..6""--__ . Time
lpe .of Sample:
Enl-ironmental r Groundwater ( 1)
___ Surface Water (2) ·a-:-Soil (3) ' .
IX Other (4l~f-
Extractable&
Concentrate
__ Solid (5)
__ Liquid (6) ',•·
__ Sludge (7) ··
__ Other (8)
INORGANIC CHEMISTRY
Parameter Results mg/1 Parameter Results mg/ 1
Comments
Total·
· Parameter
__ Silver
__ Sulfates
__ Zinc , .
_Ph
_ ... _ Conductivity _ ....
Reaults mg/1
__ BaI'iurn
Cadmium
Chromium
I_Lead
Mercury
Se-leni~m_ .. _
__ Silver
__ Arsenic·
__ . Bariuffi
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ fluoride
__Iron
______ · _TDS j: '
_TOC ,,:
__ Lead
__ Manganese
__ Mercury
__ Nitrate. ·
__ Selenium
ORGANIC CHEMISTRY
Parameter
_LP&T:GC/MS
Acid:B/N Ext.
TOX
I-
Results,mg/1
. MICROBIOLOGY C Parameter ·
(MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lOOmls
Parameter
_z{_EDB
..X PCB's
1Petroleum
1Endrin
--2LLindane
l=-----
Results mg/ 1
111, II·
N, f),
Af,,1, .
i/ v
Parameter
__ Gross Alpha
__ Gross Beta
. ,· 1 <,,. I,
Parameter,·.
_l{_ Methoxychlor.
--X-Toxaphene
..jL-2 4-D ... · ·•
..L 2:4,s-ri (, 1:-c~i
RADIOCHEMt •TRY
Results mg/1
,-• R<·sults PCi/1
.. ,
I
~-C. Department of Human Resources
),. · ion of Health Services SAMPLE ANALYSES REQUEST
_ _,1 9S-l4?S</~Z ~
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
I.. Number O 7 L)fltW-gJzo Field Sample Number --·"'6"'-"9_9._,7 _________ _
e ofSi~e ,CC.x-U,)*~1-1,~r,,.-ro,.J Site l-oca:ion. w,,srl,AJ(,Yo A.) NC-
~lected By :Ii J, . 4 fr
iJ,e of Sample:;,;('~~
!DI/ --=•=----· Date Collected _,2...,.i:,._L/9=U~t:-~~2t~6~--Time
¥8
En~ronmental Concentrate 'I---Groundwater (1). __ Solid (5)
__ Surface Water (2) __ Liquid (6)
fL-Soil (3) __ Sludge (7)
--Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractablca
Parameter Rcaulumg/1
2 i::£m ·
~Chromium
<o-os:: <o,o,S::
< 0 ./
Parameter
Arsenic·
-A.Barium
--¥.-Cadmium
__ Chloride
Resulu mg/~
6·0
Commenu
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
Resu!Umg/1
,
,_6-Lcad If"-Mercury <o, o 2 <
_L Chromium
__ Copper
__ Fluoride
__ Iron
______ ._TDS .
. ·--Selenium __
__ ·Silver 1=.----
If= ___ _
I Parameter Results mg/ 1
_P&T:GC/MS I-Acid:B/N Ext.
_TOX
--I=
MICROBIOLOGY I Parameter
__ (MF) Coliform Colonics/lO0mls \ . F (MPN) Coliform Colonies_/lO0mls
----A-Lead
__ Manganese
~Mercury
__ Nirrate.
__ Selenium
..S-25
<o oa
ORGANIC CHEMISTRY
Parameter Results mg/1
_EDB
__ PCB's
__ Perroleum
__ Endrin
__ Lindane
Parameter
__ Gross Alpha
__ Gross Beta
----
_TOC
Parameter Rcaults mg/1
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (s \vex)
----·-
-
RADIOCHEMJ1 :::.1lY ..
R, sulu PCi/ 1
'
...
..
..
I« Received _________________ Date Reported -~/-=0.~b:~ __ Ph __________ _
It. e Extracted-------------~---Date Analyred I Ii 76 AUG2'78ii
1·ortcd By Lab Number __________ .::._ ______ _
/2/; 2--g '
N. C. Dcpartrn•:nt of HU.man Resources
o,rSIOn of Health Services SAMPLE. AN AL YSES REQUEST
·State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
.· Raleigh, 27611 .· 11 9tf'I ,t:;,~.9.;2---.
Site Number O 2: l) ,tgL.fl-i'"4ifC/ f/ · Field Sample Number ___ ·_,,3"-·-·2,_._o_7._.,--------'--
"e of Si~e ,CC.')(,-U,},f-~H,_,vi!,-T'O,v Site Loca.ion · W .,,~ H,;.., G-To AJ
Collected By '-~ ( a• ·
• of Sample: '~~
ID# __ 3'/Y.:zc,:_ __ Date Collected '2'-. 8t1~ 2!'6
½$
En~ronmental ioncentrate 11---Groundwater ( 1)
·--Surface Water (2) 1f--¼-Soil (3) .
__ Other (4)
__ Solid (5)
__ Liquid (6) ',. ·
__ Sludge (7) ·
__ Other (8)
Comments
NC.
Time _/-'-'f~, _.'c/-'-'1--'
INORGANIC.CHEMISTRY' ''
Extractable•
Parameter
__ Arsenic
Ba"rium · · ·
F Cadmium ·
! __ Chromium
I __ Lead .·
EMercury ____ '.tt:~:U!l'._ -
1-· ------
Results mg/1 Parameter
__ Arsenic·
__ . -Barium
__ . Cadmium
__ Chloride .
__ Chromium
__ Copper
__ Fluoride
__ Iron·
__ Lead
__ Manganese ·
__ Mercury.
__ Nitrate
__ Selenium
Results mg/ 1
Totat" · ··
Parameter
__ Silver
__ Sulfates
_·_Zinc ":. ;, .,
_Ph .
_,_ ConduCti~il)• i:
_______ · TDS ;, ;-; . /, ;
--··~:,:i.
_TOC · ·· .-. ·!
Results mg/ 1
ORGANIC CHEMISTRY -· ~ ·'.
Parameter Results mg/ 1
✓ EP&T:GC/MS
Acid:B/N Ext. i/
TOX -
---
. :MICROBIOLOGY 1 · · · Parameter · '
__ (MF) Coliform Colonies/l00mls
__ (MPN) Coliform Colonies/l00mls
Parameter
~EDB
LPCB's
_Lpetroleum
1Endrin
~Lindane
1=-----
Oate Received :z-,;;27-ff'h B, D.
. Pc,,r;(;5o;).>£.! E. J>,
Date Extracted q -,;:!./, -,'?ib ·11, 1',
lcportcd By· __________________ _
Results mg/1
,,,-. /I
JV, I),
N. !l. .
✓
V
. Parameter
__ Gross Alpha
__ Gross Beta
Parameter, ' ' Results mg/ 1
L Methoxychlor
., i,./
_L Toxaphene I/"'
___¼_ 2,4-D '. <O, l
~ 2,4,5-TP (,s \vex) · <O, I
, -----
RADIOCHEMJt,TRY
. ,', ,, Rt·sults PCi/ 1
Date Reported ==----=:--:---~---------
ff · ?~s·r.
Date Analyzecl 'Z-12fZ Po/-l(2•/7--J1i,--f(p
' / . '
Lab Number . 6P2412 · , :
D
-.J.C. Department of Human Resources
tion of Health Services SAMPLE ANALYSES REQUEST
.O 1 9ft 4?S 9.12 ~
Srate Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Sg Number O L l)_!.ilX.biz:l?;
~e ofSi;e FC.x-t,U~sH,N(;T'ON
Field Sample Number _.....J:.d=-9,__9'--'-8"-----------
Site Loca:ion. U/A$rl,~G,To A.) ,,vc.
~lected By ,4. '}z, ,/,./4,,,.,< ·
Tll,cofSample:
ID# __ j'.....,_7 ___ Date Collected _,2..,_,.'-._c;/9e.;V=6-:c......,'Z'<.6..,_ __ Time
Enrironmental ID--Groundwater ( l ).
__ Surface Water (2)
11../4--Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments
INORGANIC CHEMISTRY
Extractables
Parameter
Arsenic
Ba"rium
Cadmium
-,-Chromium
I,.,,__ Lead
It=~~;~~:_ -
__ Silver
Results mg/1
0 ·O I
(,1, 0 Q
1=·.---
-·-fl= ___ _
Parameter
....;i..-Arsenic·
±Barium
-2:::..._Cadmium
__ Chloride
--X.Chromium
__ Copper
_·_Fluoride
__ Iron
____K Lead
__ Manganese
_LMercury
__ Nitrate
__ Selenium
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductiviry
_ms
_TOC
Resultsmg/1
ORGANIC CHEMISTRY
Parameter
P&T:GC/MS
FAcid:B/N Ext.
_TOX
Results mg/1
MICROBIOLOGY I . Parameter ·
:--(MF) Coliform Colm,ies/l00mls '11= (MPN) Coliform Colonies/!O0mls
:--
Parameter
_EDB
_PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/1
Parameter
__ Gross Alpha
__ Gross Beta
Parameter
__ Methoxychlor
__ Toxaphene
-2,4-D
__ 2,4,5-TP (, !vex)
RADIOCHE:M fl TRY
Results mg/ 1
-~-------R <Sul ts PCi/1
lte Receiv~d ----------''--------Date Reported +/--'0c"'°-'----'J{.:..1 __ ~_-..:6:c.... _________ _
111':itc-Extracted
!'Ortc:d By· _________________ _
Date Analyzed _________________ _
Lab Number ___ /...;./....;/_./_,7'-"!:,...,ii.uf:+,.·+7--,.,:..,,b.-------
1:· DcpartmeM of Human Resources
Di,-uiM of Health Services . SAMPLE ANALYSES REQUEST
·11.· · · 91'14-?.59.ffZ ~-.•·
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
. Raleigh, 27611
Site Number _0~7'-l'-')"'--'fl"'-"/_~ftc.·,_E_":i,~'ZM"-"-~--.-·-· ___ Field Sample Number __ · ~3~2-·o~·~~·-··_•_· ________ _
.._e of Si~e -'-F_C.=x-'----"U,)-C.-'*"--~-H-'--,_,.,_G--=---7""-o-'--,.J--------Site Loca;:ion .. w ;t$ H, ,v G, To IV -NC.
~ccted By -"-,,f'/_.,· ~--'~"""'"', """--'-'-'""-"----ID#-~'$'-'?'----Date Collected _.z ...... "._· _,/9""--"P""G-'--_,Z'"'-"6'----Time /Y,' l/.r,~
'J,eofSample:
EnVironmental "t--Groundwater ( 1)
___ Surface Water (2) -~J-L Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
,·
__ Liquid (6) '.·
__ Sludge (7)
__ Other (8)°
Comments
INORGANIC CHEMISTRY '··' ,; '
Extractables Total
Parameter
__ Arsenic
_,._Bafium.
fl_Cadmium ·
Lchromium.
_. _Lead
.. t::_~f;~~'!';, __ -
__ ._Silver
Results mg/ l Parameter
__ Arsenic
__ . Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ l Parameter
__ Silver
__ Sulfates
__ Zinc :
_Ph
-------. __ Conductiv.it:y ··.
_TDS
__ TOC 1-' r:
Results mg/ l
ORGANIC CHEMISTRY
Parameter
I --Ir P& T:GC/MS
~ Acid:B/N Ext.
1-TOX
1-
Results mg/ l
M.I.CROBIOLOGY l= · Parameter ·
(MF) Coliform Colonies/lO0mls
__ (1:-'IPN) Coliform Colonies/l0Omls
I=
late Received 'i{-.J,7-J?b B, I>,
. :f> E-'n: {,<> ,L.:£} "E? .b,
Date Extracted 9--,p.,t,, · :[1, X ?,
Parameter
-X.EDB
__.&_ PCB's
.L Petroleum
~Endrin
__x,_Lindane_
'
lcportcd By --------,-------------
Results mg/ l
I]/
l',J, 0,
11(,4
Parameter ;
__ Gross Alpha
__ Gross Beta
' . ----
Parameter · Results mg/ l
_2L Methoxychlor.
L_ Toxaphene·
1,__2,4-D ~J:S
..L.. 2,4,S~TP (s'ivex) _ _
------·--------
RADIOCHEl'.rn:TRY.
.. Rt.suits PCi/ l · ..
'
.. ;.'' '_ .
. ·1 ' I
Date Reported;;:;::-----:=--:-:--,----------
ff · PeST-:.
Date Analyzed 't?-1:1$, m ~-' IO ·-I 7~Ylf1(,l:
Lab Number 6n2J1.1 :
I
N. C. DepattU:c. lg£ Human Resources rion of Hcal'.h Ser~ccs . . ·. SAMPLE ANALYSES REQUEST
.ol · · · ·. 'f~,, ?15-9J'2 ,_,,.
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
, Raleigh, 27611
l Number O 2: L).!JIV-dd'«?
c of Si~e FC.X-u.,J*''"flNti,-T'"o,.J
Field Sample Number ___ ,1,.,.,.__.·_,.9_9,_. -f-7-·--------'--
Site Location W-,~ ff ,,.,n;, ro AJ NC.
'iillcctcd By J1, fl 1 '44= ·
il,cofSamplc:
ID# _ _..?._2'---· Date Collected ·: 2 t:, l9Pt$-$' 6 · Time /6, 'to
Env'ironmental ~1--K-Ground,.;,.tcr (1)-.
___ Surface Water (2)
-~ Soil (3)
----'· Other ( 4)
Concentrate
__ Solid (5)
__ Liquid (6). ·
__ Sludge (7)
__ Other (8)
Comments
l.,,"TH,>N Cu,;,_,-
INORGANIC CHEMISTRY
Extractablca
Parameter
Arsenic
(1-Ba'rium
II-Cadmium ·
i---Chromium
[
I ·Lead
FMercury
,.____Selenium ·, ----··---.__-Silver
Resulta mg/1
l=---
1-----------
fl=----
I Parameter
I P&.T:GC/MS
FAcid:B/N Ext.
_TOX
l
Reaulta mg/1
E----
M !CROBIOLOGY I . Parameter ' . .
·-'_(MF) Coliform Colonies/lOOmls
! i= (MPN) Coliform Colonies/lOOmls
\
Parameter
_!(_Arsenic·
;_..1..Barium
...£.Cadmium
__ Chloride
___.{ Chromium
__ Copper
__ Fluoride ·
__ Iron
_,¥,_Lead
__ Manganese ·
.....1'...Mcrcury
__ Nitrate ·
__ Selenium
Results mg/1
·<o, I
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ ,S_,_-=<:J'-'''-"';:;..i[ ____ ._Conductivity ·
_TDS
_. _Toe
::S, 0. o3
Resul ta nig/ 1
ORGANIC CHEMISTRY ... ,·,. ·'· °i'i':.
. ,:. ,::,:-
Parametd
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Results mg/1
'
Parameter
Parameter :· ' :
__ Mcchoxychlo~
__ Toxaphcne
_._2,4-D
--2,4,ScTP (s lvex)
RADIOCHEMl'."TRY.
Resultsmg/1
--'------'---Ru u l ts PCi/ 1
_._Gross Alpha .,,/ __________ _;___;___
--GrOSS Beta .,,-:_:•: ,c,,..,h .. -------'--'---;_;_;__
I R · d D t R d q_l.'/-~!
te cce1v~ ----------'-------a e cporte ----'--'----'!:::_ ____________ _
I te Extracted Date Analy:ed
17244 AUG r.8 811
,,ortcd By· Lab Number --------~---------
f
I
Jl~ -D~partmem of Human Resources
Divuioo of Health Services SAMPLE. AN AL YSES REQUEST
• ,. t'
State Laboracory of Public Health
: , •" .. P. 0. Box 28047
306 N, Wilmington Street
. Raleigh, 27611 11 . "l'Dl4'r~'fj'Z, ~,.
Sice Number ~D"'-'7'--._l)""-JG-,E ... 1'""-~½ ... -l:_-..,4~i ... r~a ___ :_.·_• ___ Field Sampl~ Number __ ._··._:-J~-·2_'"_o_· ... ?~-----------
fne of Si~e __,_F_C.=x'--~t,,U..c...c,..~~-H'--, N----'6,-'--T'-_o'--AI________ Site Loca;ion . w "'!> H, A.Ir., To A,)
Collected By ~1t.~___.J7"-'-1 "'-cJc---'-'-~-=~--__ ID# --""-3_,_7 __ Date Collected '2'-"Av6-23'6
NC.
.of Sample:
Env'ironmental p Groundwater (1)
___ Surface Water (2)
~, .. ·t-Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6) ,-,
__ Sludge (7) ·
__ Other (8)' '
Comments
'· INORGANIC CHEMISTRY
Extractables
Parameter
__ Arsenic
_. _, _Ba"rium
Lcadmium.
Lchromium.
__ Lead
fl--, Mercury
.. ~~ek:'llU!_Il __ _
__ ._Silver
Results mg/1 Parameter
__ Arsenic·
__ ,·. -Barium
__ Cadmium
__ Chloride
__ Chromium
__ .Copper
__ Fluoride
__Iron
__ Lead
__ Manganese ·
__ Mercury
__ Nitrate
__ Selenium
Results mg/1
Total
Parameter
__ Silver
__ Sulfates
___ Zinc :
_Ph
_._ Conductivity . _______ · __ ms .. •;°,.:,• ...
_TOC. il
ORGANIC CHEMISTRY • r J ,, ' .
Parameter Results mg/ 1 Paramete~ '. ' I Parameter Resul~s mg/1
__K_ P& T:GC/MS 1 / __ EDB __ Methoxychlor
Time
Results mg/1
Results mg/1
l=Acid:B/NExt. __ PCB's __ Toxaphenc
TOX __ Petroleum __ 2,4-D -~-
1
--______ 1--Endrin __ 2,4,5-TP (slvex) ~-~--
•---------~:_-_-_-_-_-::_-_-:_= 1~:_-_L_in_d_a_n_e ___________ .,_ _______ :.:_-::_------r !1-1..!CROBIOLOGT RADIOCHEM.I: ,TRY
C Parameter Parameter Results PCi/ 1
(MF) Coliform Colonies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lO0mls __ Gross Beta ;
I= ----
I ate Received ?-...2 7-·,?°t:., B, D • Date Reported __________________ _
Date Extracted--------------~---Date Analyzed ....,</'---'-/(},,._-..,g=(e'--'7Jc;.,,,4.:.1 _____________ _
I 6'.)_!>41,4·
epc>rtcd Dy· ___________________ Lab Number -----~~=='-----------
I
N. C. 'Department of Human Resources
,,vision of Health S«viccs SAMPLE ANALYSES REQUEST
. '/<$1 ~~s-9,rz. ~
State Laboratory of Public Health
P. 0. Box 2804 7
306 N. Wilmington Street
Raleigh, 27611
!lite Number O 7 J>_j,i.4 r >'.7~
liame of Site F C )( -'('.1/4:44",71 f ,J..,,,., . 0
it°llected By $ )¼, e'¼ ID# Y ~
... ype of Sample:
Environmental Concentrate
I ~ Groundwater (I) __ Solid (5)
___ Surface Water (2) __ Liquid (6)
I __ Soil (3) __ Sludge (7)
Other ( 4) __ Othet (8)
Field Sample Number ----~3"'-'2..=/,__ ________ _
Site Location /u ,n.b 1 /-r,., ;;
Date Collected d t{. Cl,.,< t' t:: v
Comments
Al S'. -# 7 I
Ne..
Time _,_l.,.,b..__,' Lt+C---'
i INORGANIC CHEMISTRY
Extractable&
I Parameter Results mg/1
__ Arsenic
__ Barium
I __ Cadmium ·
__ Chromium
__ Lead
1--Mercury
__ Selenium
~ s;1 • .,
--
I . Parameter Results '}'Kl 1
...JL P& T:GC/MS V
I __ Acid:B/N Ext.
_TOX
--
--
MICROBIOLOGY
Parameter
I
I
__ (MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/l00mls
----
Total
Parameter Results mg/ 1 Parameter Results mg/ 1
__ Arsenic __ Silver .
__ · Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ Copper _ms
__ Fluoride _TOC
__ Iron --
__ Lead --
__ . Manganese --
__ Mercury --
__ Nitrate --
__ Selenium --
ORGANIC CHEMISTRY
Parameter Results mg/ 1 Parameter Results mg/ 1
_EDB __ Methoxychlor
__ PCB's __ Toxaphene
__ Petroleum _2,4-D
__ Endrin __ 2,4,5-TP (silvex)
__ Lindane --
RADIOCHEMISTRY
Parameter Results PCi/ 1
__ Gross Alpha
__ Gross Beta
--
--
~';?~-,.,-~"-7_-~,Y~?,~~E~· D=-~~-------Date Reported _________________ _ I Date Receiv~d
Date Extracted _________________ _ Date Analyzed _,tfc..·wl'J.~·/l.,..,~"-o..,7Z.,_.,./JL~------------
6 ').2416
Lab Number ------'--'--------------I Reported By
DHS 3191 ( Revised 7/85)
So\iJ anJ Ha~rdous Waste (Review 7/87)
Purpose:
Preparation
I
Enforcement and compliance with the N. C. Solid and ~rdous Waste Management Rules.
A sample analyses request form {OHS 3191) must be completed for each type of evaluation requested (e.g., I
inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one ( 1)
container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the containers. The
collector must then write the site and sample number on the duplicate. I
Do not submit an analysis request sheet with no parameters indicated.
Equivalent measurements:
ppm= µg/ml = mg/1 = µg/g = mg/kg
ppb = µg/1 = µg/lOOOg = µg/kg
DEFINITIONS/INSTRUCTIONS
Site Number -A rwelve-digit site/location identifier, assigned only by the district field representative.
Field Sample Number -A six-digit sample identifier which is pre-printed on the sample label.
Name of Site -Name of landfill, facility, etc.
Site Location -Address, street number, state road, etc.
Collected By -Name and ID of sample collector.
Date and Time Collected -Self-explanatory.
Environmental-A sample of a naturally occurring substance such as groundwater, surface water or soils which
I
I
I
I
I
may be contaminated. · · I
Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummed
wastes.
-·---______ .. ·-· ·-.. Comments -Lists details regarding sample or sample point, including but limited to, phase separation, and/or I
odors.
L
Inorganic Chemistry -Check ( ✓ ) the desired parameters to be analyzed. Extractables are only performed on a
solid or semi-solid. For routine landfill samples, check all parameters in the second and third columns. · I
Organic Chemistry-Check ( ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the space
provided. · ·
Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for either I
of these.
Distribution: 1. Original to State Labo~atory of Public Health
Environmenral Sciences Branch I
P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Management Branch. I
Disposition:
3. Solid and Hazardous Waste Management Branch sends copy to field person. · · I
This form may be destroyed in accordance with the Environmenral Health, Solid and Hazardous Waste Section of
the Reco,d., Disposition Schedule as published by the North Carolina Division of Archives and History.
Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch
Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
I
I
I
I
/ 2// ~
t-.l:·Departmr.M of Haman Resources
Di1,·i.sion of Health Services SAMPLE ANALYSES REQUEST ,
. State Laboratory of Public Health
P. 0. Box 2804 7
306 N. Wilmington Street
. Raleigh, 27611 ·ll · %1 4?S 9J'Z. f}c,J
Sice Number _0~7'--.,_l)""-fa--b'-'J'~L=J~(-~/--479Q~-'--'-~------Field Sample Nu~ber __ · _"'·'=3~2_.-_/ o_· _________ _
.e of Si~e __,_F_C.=:x'--.....;.~_c_c,.._~_H'-'--, ~--'&-'--r-_o'--AJ________ Site Loca:ion . W "I: H' ,v r, To AJ
Collected By _..1:J:....c·_;./1_.. . .:...; c .. k4,,_._===·---ID# __ 3"-'-} ___ Date Collected _.Z"-"'t:,._..19°"· -=v~&-"--_,Z'.....,,E>~--Time -'-'/lh"'.,_i_,_0..:o=--.....,
flpeofSample:
l\:n~ronmental
~ Groundwater (1)
___ Surface Water (2)
11--Soil (3) .
II~_ Other ( 4)
Concentrate
__ Solid (5)
__ Liquid (6) '' .
__ Sludge (7)
__ Other (8)
Comments
INORGANIC CHEMISTRY
Extractable&
Parameter
Arsenic
_·_· Barium
II= Cadmium ·
Chromium
I
_Lead
Mercury
S,;lenium ___ .. _
--:.Silver
Results mg/1 Parameter
__ Arsenic·
__ . BariuITl
__ Cadmium
__ Chloride
__ Chromium
___ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ 1
Total·
Parameter
· __ Silver
__ Sulfates
__ Zinc
_Ph
_._Conductivity
_ms
_TOC
'. I"' : Hi:
·. ,· i
• Results mg/ 1
ORGANIC CHEMISTRY
Parameter
Acid: BIN Ext.
TOX
Results mg/ 1
MICROBIOLOGY
Parameter I== (;.1F) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
I=
Parameter
_LEDB
-2L PCB's
_t_ Petroleum
1-Endrin
_){_ Lindane
Ila re Received J?-;27-:T? B, 2), u · &::' fl m p.u,::1 1-tJJ .
Date Extracted 'f-t9-Jfe&Q q -2.C; ,,r"(,, @
I
Results mg/1
N'.4
Parameter
__ Gross Alpha
__ Gross ·Beta
' ----
Parametei-' : '
_.!S,_ Methoxychlor'.
_:?5.._ Toxaphenc • ·
_L2,4-D •·'
~ 2,4,5-TP (s'ivex)
RADIOCHEMii-TRY
Results mg/ 1
'• t!Y
. Results PCi/ 1
..
. ,.
. . .,
-
Date Reported--------,------------
_. ' ,\'
Date Analyzed ..,_Jl.=~c.;.,-:...,7.c...·_,_/...:.P_•/:...-:..6_-S'J..,,"be:.. -r,.,_'u.f'..._•.:_: _. ______ _
Lab Number __ 6_: __ i,.__•-~_.4_1_5_-_' _____ -,-___ _
::lironmental
. Groundwater ( 1)
r. · Surface Water CZ)
Soil (3) ·.
Concentrate
__ Solid (5)
___ Liquid (6)
__ Sludge (7)
__ Other (8)
Time 11oS:-
Comments
1
Cleoa Lo../tqM We I/
r Other (4)
INORGAA'1C CHEMISTRY
Extra:ctables
aramcter
"ill Arsc nic
ilBarium ,-···
_Cadmium
llChromium
ii Lead
_Mercury
Selenium =rf sii~e~ --·-'
Results mg/1 _
-1-.. ---
-t
Pa.ramcter
= t P& T:GC/MS
_ Acid:B/N Ext.
tTOX.
Results mg/1
MICROBIOLOGY
Parameter ·
-I (MF) Coliform Colonies/l00mls
_ (MPN) Coliform Colonics/l00mls
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ fluoride
__ Iron
_Lead
__ Manganese
__ Mercury
_·_Nitrate ..
Selenium
Total
Results mg/1
.. -------
Parameter · ,
__ Silver •. ' ·
__ Sulfates
__ Zinc
_Ph
__ Conductivity ·: _ms .. ,
_TOC
Results mg/1
{ ORGANIC CHEMISTRY ~
Param .......... L
lEDB
--1LPCB's
...::£._ Petroleum
lEndrin
...LLindanc
Resu1ts mg/1 Parameter Results mg/
IV4 L Methoxychlor _::Q0,110~;~ < o. 0 00 I 1311("1. L Toxaphcne ---e fZ~!l.l'.}:!
N4-r ...x._2,4.0 ~ o,oo
<~. OOO{Jrtr\-_ $_ 2,4,5-TP (silvex) < o,oo/ -<e,oao4l~ .llL _. ________ _
Para.meter
__ Gross Alpha
__ Gross Beta
RADIOCHEMISTRY
Resulu PCi/1
Date Reported -,-,-,--· _/,~1/c)----'f;,'-"1/-;r;::;-,<f;;:;7~,.......,,.,.,.-,----)J,,J,_ · Pc.rr: ¥pc.e.l-
Date Analy-~d O -Io -,r(, 8,() 1,;z-1:>-rC. 7/. P
L:ib Number ____ 6_:_'.J,;;.', -=1=-=4==1=-------
State Laboratory or Pub!ic He.::.
. SAMPLE ANALYSES REQUEST . ·. P. 0. Box 2E<
306 N. Wil:ningr"n Sr:
_._ Raltibh, 2it
:lumber t!)j[) </?'.I 41-5 '132-
n, ~f s;;~: . f::C., >< -t,u~ C.. 7 <' 7 :/2-o .
X' ~d By ?J;.; t<..J-, C-0 c /4 ,~ · ID# _Q.a· :....?-.;.._ __ Date Collected ___,/c...:/_-_.Za..;Oa.--.... ~...,6"-----Time / Je> ~
. 7
f~m~~ · · · ·
·1-ironmental
__ Groundwater (1)
,...--Surface Water (2)
JI_ Soil (3) r Other (4) ·
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Comments
C'. kan Lo, /f..0= We. I/
Extractable, Total
Parameter Results mg/1 -Parameter Results mg/1 Parameter Results mg/1
1Arsenic __ Arsenic __ Silver '· ,·
Barium ,-· · __ Barium __ Sulfates
_Cadmium __ Cadmium __ Zinc ..
--·Chromium __ Chloride _Ph
_ Lead __ Chromium __ Conductivity ·
_Mercury ·· __ Copper _ms ...
Selenium __ Fluoride _TOC . ,. -----Silver __ Iron --. . _Lead .. . , ---·-
__ Manganese , . ~-~. ---
j __ Mercury . , •· --
'
. _· _Nitrate .. --
Selenium
-t ( ORGANIC CHEMISTRY ~
Parameter Results mg/ 1 ParamcLc< . Kesults mg/1 Parameter . Results mg/
P&T:GC/MS Nf\ -LEDB ..X.. Methoxychlor
_ Acid:B/N Ext. _LPCB's L Toxaphcne ·
tTOX ...:i...... Petroleum ~2,4-D . ~
..LEndrin L 2,4,5-TP (silv~x)
.::I,_ Lindane L· -
-.. MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/1 -I (MF) Coliform Colonics/l00mls __ Gross Alpha
__ (MPN) Coliform Colonies/l00rnls __ Gross Beta
------
)] Ri:ceivcd __________ _,;,. ________ Date Reported
)a Extracted ______________ ..,;,. ____ Date Anal)-..<:d ----:----::::---;--;---_;_ ______ _
Lab Number ___ &_o_:3_!_4-_I ______ _
l "l,rted By . _
1H:-)IQI (R,vir.cd 7185)
-:,l1J anJ H;,.:ardous Waste (Rcvit-w 7/87)
V6A -11.0-f a no.I~ zed
,1·. ~
N. C. Department of Human Resources
,i,-uion of Health Scn1ccs . SAMPLE ANALYSES REQUEST
ratory of Public Health
P. 0. Box 28047
Wilmington Street
R.alclgh, 27611 .Dl . 9~t4?S-9~Z ~ u:,
laitc: Number · 0 7 i) fJ'l/61-4@ Field Sample Number __ 3"'. _o-zrt ___ · •_. ________ _
l.ame of Si~e FC.X-U/,..~H ,,.,,r,,.T'oAI Site Location' ·w,,t: H ,,vr, To A.) -NC.
(
r llected By 7,/, ~,.__ ID# _...,L/_8 __ Date Collected 2'-19 v6-· Z' 6 Time /(;,, /I
' ~ ~
pc of Sample:
Environmental Comments I X.. Groundwater (1)
___ Surface Water (2)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
5...,,.....,e-c::: .:M NS it 7
t--Soil (3)
__ Other (4)
I
Extractablea
I Parameter Results mg/1
--Arsenic i--__ Ba'riu~
,-Cadmium·
__ Chromium
l_i:cad . . ,
___ Merc~ry
~~'"'""' ---·.Silver
' '
I= l
I Parameter Results mg/ 1
_P&T:GC/MS
,-Acid:B/N Ext.
_TOX
1-
INORGANIC CHEMISTRY
Parameter Result& mg/1
_1f_ Arsenic :s:::o,o I
__K.. Barium <o. I
_:i_Cadmium c: fl, ODS
~Chloride
· _}(_chromium ~&-~l
__ Copper
__ Fluoride
__ Iron
_f._ Lead <.o. "3
__ Manganese · <o,ooooJ ....::i-Mercury
__ Nitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter Results mg/1
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Total .. , • • < I ~•:• • ,,
Parameter
__ Silver
__ sulfates
__ Zinc
-Ph
_._Conductivity,· . · ms .;_ , .. --,,
_. TOC ' ----' ., .' --'' ----,, --.·,
·• ,"; r-•
Paramete~ ' .
__ Methoxychlor
__ Toxaphene ".•
. 2 4-D ,,: '' --' '~ __ 2,4,5-TP (slvex)
--.. -•
''
RADIOCHE:Ml1 TRY
Resulumg/1
Results mg/ 1
MICROBIOLOGY _.,_;_ _____ _ I · Parameter · ·
__ (MF) Coliform Colonics/lOOmls I' , . (MPN) Coliform Colonies/lOOmls
Parameter
--Gross Alpha
__ Gross Beta
Ruulu PCi/1
· late Recdv~d ----------'--------Date Reported ___ q-__ f~-~-~-'~· ----------.--
\
Date Extracted-------------~---Date Analyzed ------,-,.,..,.,-,,,-,.,..,.,,,----
1 . I 1243 AUG 2·3.,~ ·
·.,.vortcd lly· __________________ Lab Number ______ . ____ . __ ,.
. ,,.:•
r.
1-l: Depamn~m of Human Resources
Division of Health Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611 I ~l--lrS-'137! ~
__ (J~]~P-5~8..,.._~J~~~~~------Field Sample Number __ <5~d---_/_7 _________ _
lme of Site f:C k' -,u/o/1 43 /...... Site Location . tU a.,,£..., JP½,., Al c_
Site Number
Collected By ';1/ 'y.e/4/4. ID/I -~'t'.~A~'---Date Collected . -< U> t1u.J if C:
t of Sample: , ~
Time ltf,.'2-?
nvironmental Concentrate
~ Groundwater (1) . __ Solid (5)
c.._ __ Surface Water (2) __ Liquid (6)
a--Soil (3)
L_ Other ( 4)
__ Sludge (7)
__ Other (8)
I INORGANIC CHEMISTRY
Extractables .
l=Parameter Results mg/1 Parameter Results mg/1
Arsenic __ Arsenic
__ Barium __ Barium
l=Cadmium · __ Cadmium
Chromium __ Chloride
__ Lead __ Chromium
11=-~j';~~; _ -__ Copper
__ Fluoride
--•Silver __ Iron
_Lead
F __ Manganese
. __ Mercury
--__ Nitrate
I= __ Selenium
ORGANIC CHEMISTRY
I Parameter Results mg/1 Parameter Results mg/1 ,
~ P& T:GC/MS I/ _EDB
FAcid:B/N Ext. __ PCB's
TOX __ Petroleum
__ Endrin
--__ Lindane
I MICROBIOLOGY
ParamCter Parameter r=-(MF) Coliform Colonies/ lOOmls __ Gross Alpha
~ (MPN) Coliform Colonies/l00mls __ Gross Beta
----
0-,;;z 7-9--/.,? »·' late Received _,,r_"------=-"'~ '~=''-'0.-'-"~-'-'----"---------Date Reported
Comments
Total
Parameter Results mg/1
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_TDS
_TOC
------------
Parameter Results mg/1
__ Methoxychlor
__ Toxaphene
_2,4-D
__ 2,4,5-TP (silvex)
--
RADIOCHEMISTRY
Results PCi/ I
~ate Extracted Date Analr..ed ~J:-·~J:J--fi'~v,-Z.~74_r-____________ _
geported By _________________ Lab Number ___ 6_;~);_,,~:•~J=·c.1a.c8=-------,-----
DHS 3191 CR,vi><d 7185)
SoliJ anJ Ha:.:1rdous Waste {Review 7/87)
'
Purpose:
Preparation
Enforcement and compliance with the N. C. Solid and Hazardous. Waste Management Rules. I A sample analyses request form (DHS 3191) must be completed .for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than one~ container (i.e., ground or surface water from landfills) a sample label must be affixed to one of the ccntainers .. ,.. collector must then write the 1ite and 11ample number on the duplicate. ·. · Do not submit an analysis request sheet with no parameters indicated.
Equivalent measurements:
ppm= µg/ml = mg/1 = µg/g = mg/kg ppb = µg/1 = µg/lOOOg = µg/kg
DEFINITIONS/INSTRUCTIONS
Site Number -A twelve-digit site/location identifier, assigned only by the district field representative.
Field Sample Number -A six-digit sample identifier which is pre-printed on the sample label.
Name of Site -Name of landfill, facility, etc. . .. Site Location -Address, street number, state road, etc.
Collected By -Name and ID of sample collector.
Date and Time Collected -Self-explanatory.
I
I
I
I
I
Environmental-A sample of a naturally occurring substance such as groundwater, surface water or soils whicl may be contaminated. · . . Concentrate-A sample of a waste, including but not limited to, sludges, resi"5, treatment effluents or drumrn,1 wastes.
_, Comments -Lists details regarding sample or sample point, including but limited to, phase separation, and/o, odors.
1 Inorganic Chemistry-Checlc ( ✓ ) the desired parameters to be analyzed. Extractables are only performed ~n solid or semi-solid. For routine landfill samples, check all parameters in the second and third columns.
Organic Chemistry-Check ( ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the spacl provided. . ·
Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for eithel] of these.. II Diatribution: 1. Original to State Laboratory of Public Health ·
Dia position:
Environmental Sciences Branch P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Mar.agement Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person:
This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section 011 the Records Disposition Schedule as published by the North Carolina Division of Archives and History . . .;dci,io~.al forms may be ordered from:
Solid and Hazardous Waste Management Branch Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
D
D
D
/2/12.--
' l: .Departmr.~~ of Human Resources
Di"isioh of Health Services SAMPLE ANALYSES REQUEST ...
· State Laboratory of Public Health
P. 0. Box 28047
. 306 N. Wilmington Street
-Raleigh, 27611 11. ·. 9i°/4?5'1~Z _..
Site Number -'0"'--'7'--(<--)-<-..,_ij41,.,_/_¾-=-~='-L..,'--"''--u--____ Field Sample Number ___ ;?"'-=U~·..,,t~·----------
lme of Si~e _,_F_C.=X;:..-.....::;U-'..::..;,..c.;.c.~.;..l-f-'--'-,-~--'G,-"-~-o"--,.J--------Site Loca:ion . W "'fi -',v r,, -ro ,.; NC..
Collected By ~#~-~-__,.,'i¼-a~~=-~~=--~----ID# __ · ... ~_a::.__ Date Collected _.z.._'-,..__,/i=t1_,,6-'--_..$',._,6..,_ __ Time / t, .' I I
~of Sample:
· EnVironmental JL Groundwater ( 1 ). . .
___ Surface Water (2) ·1-Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
__ Liquid (6) ...
__ Sludge (7)
__ Other (8)
Comments
A)>
INORGANIC CHEMISTRY
Extractable•
Parameter
-'-Ba"rium
Cadmium
Chromium
· Lead .
Mercury
.. _s~_k.t!l.t!!fl. ___ _
·_Silver
Resu Its mg/ 1 Parameter
__ Arsenic·
__ . Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese ·
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ 1 _ ··Parameter
_·_Silver ·
__ Sulfates
__ Zinc
_Ph
__ Conductivity ·.
TDS ,· ,..,
--"I' _TOC '
... ,,,
Results mg/1
ORGANIC CHEMISTRY ' :.:.
Parameter
_p&T:GC/MS
Acid:B/N Ext.
TOX
Results mg/ 1
M \CROBIOLOGY
Parameter
....K_EDB
__K_PCB's
_¼_Petroleum
-A.. Endrin
-<l::..Lindane
Results mg/ 1
/;
qi o
't,14
Paramet~I" ",,
-21... Methoxychlor
--3._ Toxapherie
_,1{__2,4-D
..L_Z,4,5-TP (slvex)
RADIOCHEM11TRY
Results !Ilg/ 1
~------------------------,-----------------~---------C Parameter . .
(MF) Coliform Colonies/lO0mls
__ (MPN) Coliform Colonies/lO0mls
1=-----
gcportcd By" __________________ _
Parameter
__ Gross Alpha
__ Gross Beta
Rt suits PCi/ 1
Date Reported __________________ _
p,r,sz, · · · i ·
Date Analyzed l(1-:('7-Y61(,'1',
. •' I'
Lab Number __ ....,6.,.._, _ _,,;_.-'"",1,,_1.._7,.__· -·'-, ----,-----
. SAMPLE ANALYSES REQUEST
Jumbe~. 0 l-/7 CC'i[/ 4 f 5 o/ 3 2-. Field Sample Number 3SDl-
State: LaborJtory of Pu:lUc He ..
P. 0. Box 26:.:
306 N. Wih.i:,g,cn Sc:
R:i.lei~h. 2 it
of Sire €C-~x -tU~ c.. / r? 1' k Site Lo=ion i.U-'<-6 { 'r ~s 4--c
l ed By cf!;.;/0,c,_{:., /4,.,....., · ID# p?-Dare Collected //-zo-9;'6 Time / ---""'--'-----_...a,.,c_--""=-"""""'----
f Sample:
:'.lironmental
Groundwater ( 1)
r. Surface Water (2)
Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
___ Other (8)
Comments
# tuf' ~ i: }.I.)
T Other (4)
INORGANIC CHEMISTRY
Extra:ctables Total
arameter Results mg/1 Parameter Results mg/1 Parameter
1Arscnic · __ Arsenic __ Silver
Bariuin. _.:' .. __ Barium __ Sulfates
_Cadmium __ Cadmium __ Zinc
1Chromium __ Chloride _Ph
Lead __ Chromium __ Conductivity
_Mercury __ .Copper _TDS
Selenium __ Fluoride _TOC ' ,-.. --·-Silver __ Iron --__ Lead -···· --
-__ Manganese --
j __ Mercury --
__ Nitrate --.
Selenium
-t ( ORGANIC CHEMISTRY '°')
Parameter Results mg/1 Param~••• Kesults mg/ 1 Pa.ramete:-
-lEDB /V/.1-L M~r.l,,oxychlor ·-,P&T:GC/MS
-_ Acid:B/N Ext. N\'.;! -lLPCB's < o. 000 £:p,mvl_ l Toxaphene
tTOX ..:i_Perroleum ~&r .::i._2,4-D
lEndrin < Q. ooo l:p;n,-y\_. L 2,4,5-TP (silvex)
_.::l,._Lindane < 0, a. Q a. 'I-'trDrr,. -L -. ,
MICROBIOLOGY RADIOCHEMISTRY
Results m1:/ l
Results mg/:
<Q,OO!pp.m
< o, oo;i. f'fJil. -s:::.a.,oo l
<O,oo I
Parameter· Para.meter Results PCVl -I (MF) Coliform Colonies/l00mls __ Gross Alpha
_ (MPN) Coliform Colonies/l00mls __ G,-oss Beta
------
/
>,, R,:ceived Date Reported · re,+ ~~.FB:VP Pc:sr.cv-J>C.T?/""..,/
)a, Extracted _,_1?,.;•:,lll.-:..c~,sh'-------------'-----Date Anal,.ed J.,;J...-/h-·~1,::, y,'P . 6:·-311,1 Lab Numt>er ________________ _ :cff'rted [ly
,}l')IQI (R,viM:d 7185)
.,!1J anJ H;a::irdous Waste (Revit-w 7/87)
C. Department of Hull\an .Resour(.c:~ ·i,~ ofH~).th, Se_r~ccs · . SAMPLE ANALYSES REQUEST
State La6oratory of Pub:.ic t"':.c~
P. 0. Box 2S~
306 N. Wih.hg,on S:-:
, .' . . lWcihh, 2/t
Ju'."be_r CJ j D W/ 415 o/ 3 2-. Field Sample Number
of Site . EJ:.-,X -t,U~ C.. 7 a 7 6,-.--. Site Lo=ion L.O,:,_,; (.. 'i "'S ft...c tJC.....
'I' ed By ~;;:_)';ch~ /4 ,r,-'"l · ID# _'.3'"'. '-7--'----Date Collected ___:/;..;/_-_..zc..:o::;.._-... ';;,.,6,;__ ___ Time 11:3 ~ 7
of Sample:
Tironmental
JK__ Groundwater (1)
Concentrate
__ Solid (5)
___ Liquid (6) ·
__ Sludge (7)
__ Other (8)
Comments
tAJ ,P-r )JJ I
r. · Surface Water (2)
Soil (3) r Other (4) ·
INORGAA'IC CHEMISTRY
Extractables Total
Parameter Results mg/1 Parameter . Results mg/1 Parameter Results mg/1
1Arsenic · __ Arsenic __ Silver
Barium . _-:'.': __ Barium __ Sulfates
_Cadmium·· __ Cadmium __ Zinc
=-Chromium __ Chloride _Ph
Lead __ Chromium __ Conductivity
_Mercury __ .Copper _ms
~Sefrniurn ___ __Fluoride _TOC
Silver __ Iron --__ Lead .. ---
__ Manganese . ----
-I __ Mercury --
__ Nitrate --..
Selenium
-t (" ORGANIC CHEMISTRY "',
Parameter Results mg/1 Param,c,c,
P&T:GC/MS 1\JA lEDB -_ Acid:B/N Ext. ...JLPCB's :t. TOX _.:i_ Petroleum
lEndrin
...":l:.._Lindane -
MICROBIOLOGY
Parameter -1-(MF) Coliform Colonic:s/l00mls
__ (MPN) Coliform Colonies/I00mls
-
-)I R,:cdved
"Jo Extracted---------------'-----
,,.1rred [ly
>H:, JJOJ /R,vi0<d 7185)
",i1..! ;1r,J Ho1.:.Jrdous Wastc-(Rc:vie-w 7/87)
Kesults mg/ 1 Parameter Results mg/
L Metho,cychlor
LToxaphene
..)L2,4-D
..$_ 2,4,5-TP (silvcx) L
R.A.DIOCHEMISTRY
Parameter Results PCl/ l
__ Gross Alpha
__ G:-oss Beta
--.
--
Date Reported ________________ _
Date Anaiy:ed -----------,-------
Lob Number
,,
I
I. C. Department of Human Resources State Laboratory of Public Health
>,;~_"_ of Health Services · SAMPLE ANALYSES REQUEST P. o. Box 28047
. 306 N. Wilmington Street .
. ()1 '·,·. 9/1/??5'-fJ'Z-ff-: · · · Raleigh,27611· '.
ii.Number ~· 0~'2-..'(_.)._£,r.~'..f...,L""f,l=-?-.:;&,~'7r?._,'-""o'-------Field Sample Number __ ·, _-?.,_,_9...:~:::., .... f_, _______ _.:.t'.;_· .
~ll,e of Site ~~-c.=x __ ---"-t-U.---".+--" .. H='-""';..;c;..::..;.r,..;o=,J:;________ Site Locanon. {,,(.ht$ rl I A.I& ro A) ,NG
r cted By /¥ ~ · ID/I _ _,t/'--"''5"--_ Date Collected --'Z"""'c!,.._·_.19!:Z.-"v~&-~.s.$'w6.,_ __ Time /(, ,' 2. 7
fs 1 'd' o amp e: , •t
Environmental 'IL-Groundwater (1)
--Surface Water (2) 1--Soil (3)
Concentrate
_ Solid (5)
__ Liquid (6)'
__ Sludge (7)
-'--Other (8)
Commenta
..5",9,nPe,c:: ,H, Al s f
__ Other (4)
i Extractablca .,
\ Parameter ' "
I A . , __ rsemc
il=Barium
i Cadmium ·
1L-Chromium ~t=uad / Mercury
!l.!__Selenium 11 -Sil~.~ -

-
-E '
' ' i ' j .• ,, '
Parameter
']_ P& T:GC/MS
iL Acid:B/N Ext.
Rcaulta mg/1
-'
Reaulta mg/1
:LTOX -· ., -------,, ,--
MICROBIOLOGY 1 · . ., Parameter , .
__ (MF)'ci>liform Colonics/lOOmls
'.,t' .. .,,_. _(MPN) Coliform Colonies/lOOmls I-·. '
!i
INORGANIC CHEMISTRY
Parameter Rcaulta mg/1
..£Arsenic· ·-s:::.a. Q l
_Jl:_Barium <o,/
_,,__Cadmium <4&19:1:_
_Chloride
~Chromium -<.. a. o/
' ___ Copper
__ Fluoride
__ Iron
~uad < D, 03
__ Manganese <:"o I oc;2oq _j!.__ Mercury
__ '·:tNitrate
__ Selenium
ORGANIC CHEMISTRY
Parameter
_ EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Resulu mg/1
Parameter
__ Gross Alpha
__ Gross Beta
----
•
Total·
'
Parameter
__ Silver
__ sulfates
__ Zinc'.,
_Ph
__ Conductiviti ·'
·_ms ···· •,.,'
_. _TOC '.,
-----•,; --'i ... --. '•"·. --,' ·,. ., .. ; ., ,I•• '.•,' ..
Parameter : -'.,.
__ Methoxychlor _
__ Toxaphene ,
_·_2;4.0, ·••··.
"
__ 2,4,5sTP (s lvex)
;
RADIOCHEMI! -TRY
· Rcaulta mg/1
.
'
'•.
,, '. " . :-'•·:'
Reaulta mg/1
, . Rrsulta PCi/ 1 • . ,
.... ,. ' '• ·•.•,, :·,.·. •;,,,,. 1,1,:'1• •,:.~·.
'.
.r: '
I,. Receiv~d -----------'---'----•;:oate Reported __ 4.,__-""'//.'----·-~-~-------------
Date Extracted--------------'----Date Analyzed _________________ _
lportcd Ily · _______________ · ,Lab Number ........ , ➔)l1--7h2&4~b ....... Al ... lG""-.u.?..,3'..,,:c .. · ~::..._ _____ _
'{:.~:
·~:
i-l: Depamnent of Human Resources
Division of HC3.lth Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 2761 I g ~/,f-'1~9,n ~
_t!J=--...._7~Q"'""-:J....,.f?..W-.=-'--'-7_;z,'-L'z~9'-'Z>"------Field Sample Number--~· 1....,.2=-/','-{---------Site Number .e of Site F C X -uJ~Jfu Site Loca,.'ion o/ a,a,L J In,, 1 Ji· <..
Collected By _,,..,'Y-..:·_u=::,"""'~"' ... /."'1"'1-----ID# -~i~K~-Date Collected __,.:)=t,'-"'Ct ... 1 .. ~',l,.L· < ___.8""""''---Time --'-,/4,.,,G'-''~' '(<-.:Ct!---'
1J,eofSample:
l\nvironmental
g..__J;'._ Groundwater ( 1)
II~--Surface Water (2)
a---Soil (3)
II_ Other (4)
Concentrate
__ Solid (5)
__ Liqufd (6)
__ Sludge (7)
__ Other (8)
I INORGANIC CHEMISTRY
Extractables "
l='Paramcter Results mg/1 Parameter Results mg/ 1
Arsenic __ Arsenic
__ Barium __ Barium I== Cadmium · __ Cadmium
Chromium __ Chloride
__ Lead __ Chromium
Mercury __ Copper
-l=-s~Jf.n_i_u_!n _ ·-. __ Fluoride
__ $ilver __ Iron .
_Lead
I-__ Manganese
__ Mercury
--__ Nitrate
I= __ Selenium
ORGANIC CHEMISTRY
I Parameter Results 91g/l Parameter Results mg/1
~ P& T:GC/MS v _EDB
FAcid:B/N Ext. __ PCB's
TOX __ Petroleum
__ Endrin
--__ Lindane
I MICROBIOLOGY
Parameter Parameter
J=" (;.•ff) Coliform Colonies/lO0mls __ Gross Alpha
__ (MPN) Coliform Colonies/!00mls __ Gross Beta
E
----
Comments
Total
Parameter Results mg/1
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
_ms
_TOC
------------
Parameter Results mg/1
__ Methoxychlor
__ Toxaphcnc
_2,4-D
--2,4,5-TP (silvex)
--
RADIOCHEMISTR¥
Results PCi/ 1
late Received Y ,,;;2. ?-~ 811), Date Reported
ate Extracted --------------~---Date Anal}~..ed ~CZc.·_,J.,2 ... -c.£"-LIIQ....c.72uu...,__l----::-:----------
6 , ,.,~ ;izo
-------------------Lab Number ----~-·,_.' ..,_·_,,_,t_. _., _____ :---:-------
lcported By
HS3191 (Revi,cd7/85)
5oliiJ anJ Ha:ardous Waste (Review 7187)
Purpose:
Preparation
Distribution:
D
Enforcement and compliance with the N. C. Solid and ~rdous Waste Management Rules~ . o A sample analyses request form (OHS 3191) must be completed .for each type of evaluation requested (e.g., inorganic, organic, microbiology, radiochemistry). For sampling conditions which require more than onef'. container (i.e., ground or surface water from landfills) a sample label must be affixed i:o one of the containers. collector must then write the site and sample number on the duplicate. · · · Do not submit an analysis request sheet with no parameters indicated.
Equivalent measurements:
ppm= µg/ml = mg/1 = µg/g = mg/kg ppb = µg/1 = µg/lOOOg = µg/kg
DEFINITIONS/INSTRUCTIONS
Site Number -A twelve-digit site/location identifier, assigned only by the district field representative.
Field Sample Number -A six-digit sample identifier which is pre-printed on the sample label. Name of Site -Name of landfill, facility, etc.
Site Location -Address, street number, state road, etc.
Collected By -Name and ID of sample collecror.
Date and Time Collected -Self-explanatory.
u
Environmenta.l -A sample of a naturally occurring substance such as groundwater, surface water or soils whicll may be contaminated. · · · II Concentrate -A sample of a waste, including but not limited to, sludges, resins, treatment effluents or drummeii wastes. I eo·mments -Lists details regarding sample or sample point, including but limited to, phase separation, and/or odors.
Inorganic Chemistry-Checlc ( ✓ ) the desired parameters to be analyzed. Extraetables are only performed ~n I solid or semi-solid. For routine landfill samples, check all parameters in the second and third columns.
Organic Chemistry -Check ( ✓ ) the desired parameter to be analyzed. If not listed, enter the name in the spat provided. .
·
Microbiology and Radiochemistry -The Raleigh office should be consulted prior to sampling for eithlm of these. ·
1 . 1. Original to State Laboratory of Public Health · . . Environmental Sciences Branch
P. 0. Box 28047
Raleigh, NC 27611
2. Lab sends copy to Solid and Hazardous Waste Management Branch.
3. Solid and Hazardous Waste Management Branch sends copy to field person.
I
I Disposition: This form may be destroyed in accordance with the Environmental Health, Solid and Hazardous Waste Section 01 the Records Disposition Schedule as published by the North Carolina Division of Archives and History. Additional forms may be ordered from:
Solid and Hazardous Waste Management Branch Division of Health Services
P. 0. Box 2091
Raleigh, NC 27602-2091
I
I
I
JC .Deparnr.ent of Human Resources
Di vu ion of Health Services SAMPLE AN AL YSES REQUEST
l1 ~l-??5'9?Z ~--
. State Laboratory of Public Health .
P. 0. Box 28047
306.N. Wilmington Srreet
. _ Raleigh, 27611
Site Number ~0~7 ........ ( .... )-<---,0~,e/_.z:'.~?=··=¾~"'~VL~-. ______ Field Sample Number ____ 3_2.._/_8~·---------
lme of Si;e FC.x-t,,U,+-~••O,J(,,T'oAI Sitel...oca.ion_ t,.u,,,i:,-n,vr,,-roAJ ·-NC. ·
Collected By 1l ?~ ID# __ '-f.__· =8 __ Date Collected · 2?. ·· /9tl6-'Z' 6
c) lpe of Sample:
Environmental Concentrate Comments
~ Groundwater (1) . __ Solid (5) 5,;,,,. "''-C::::: .,e A; ,\ I{
___ Surface Water (2) __ .Liquid (6) ', . .-·t-Soil (3) . __ Sludge (7)
__ Other (4) __ Other (8)
INORGANIC CHEMISTRY
Extractables
Parameter
__ Bafium
Cadmium
Chromium
I_. _Lead
Mercury
_ Selenil!m ___ _
__ Silver
Parameter
_P&T:GC/MS
Acid:B/N Ext.
TOX
Results mg/1
Results mg/ 1
MICROBIOLOGY
Parameter
__ Arsenic·
__ . Barium
__ Cadmium
__ Chloride
__ Chromium
---Copper
__ Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate.
__ Selenium
Results mg/1
ORGANIC CHEMISTRY
Parameter
...K...EDB
LPCB's
_L.. Petroleum
iEndrin
iLindane
Results mg/ 1
,/
Total
Parameter
__ Silver·
__ Sulfates
_·_zinc
_Ph
__ Conductivity
_ms
_TOC
"
. f·
Parametei-..
..L.. Methoxychlor
~ Toxaphenc.
12,4-D
12,4,5-TP (s lvex)
RADIOCHE:Ml: TRY
Results mg/ 1
Results mg/ 1
q µ '5 qu s
-~-------~ C Parameter ·
(MF) Coliform Colonies/lO0mls .1 (MPN) Coliform Colonies/lO0mls
T
Parameter
__ Gross Alpha
__ Gross Beta
. Results PCi/.1
I 9 -;:z. 7 -,Jr;, e. b.
ate Receiv~d ....,...v-,.,. -~-----~-~-------Date Reported-::'.=---------,---'---------'
Poi{(~ (,gfp 11 J9. , f-if:t_;0 _ ,4 t{i£:f\ Pc:ry; . ,
Date Extracted :'.! fJ .L ,._1 tJCJ ~ Date Analyzer! /(2-./lf-.fli J! 1?
J
lcportcd By Lab Number 6' '.·2419
: .. Department of Human .Resource& iln of H~? ~cr":c~ .· · SAMPLE ANALYSES REQUEST< .. State Laboratory of Public He.::
P. 0. Box 28(
. 306 N. Wil:nington S:::
=1~~,~e.<· .07-lJ WI 415 932..
. >· :.:.~.::i:,-.. , R.nlcigh, 27t
Field S~~pie ~~mb~~ ''·' 3' 5' {) 3 .. . . '
Site Loca.-ion . /,b.eq; t. ~ ""S 4.-, /JC,_ rlofSite ,C:C.,X -t-O~ h"ln 7 6-r-, .
llfted By . ~; t<J-,. ch C 7/4 <?::!'.'.' . ID# _p>=..1-..;,_ __ Date Collected __,/-'/_-_..z"-'o'------~ ... 6,.__· ---Time 13 >'S-
iAr sample:''•.
yironmental
I_ Groundwater (1)
...--"-Surface Water (2)
.JI__ Soil (3) ·
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments # . . tuP-~ /JJ. S°n(n. I
r Other (4)
INORGANIC CHEMISTRY
Extractables Total . , ... " .
Parameter Results mg/1 _ Parameter Results mg/ 1 Parameter Result> mg/1
1~::un;_;''•··:· __ Arsenic __ Silver '· ,·.
__ Barium __ Sulfates
_Cadmium · __ Cadmium __ Zinc .. : .. "".:
1 Chromium . .. · __ Chloride -Ph
Lead . · __ · Chromium __ Conductivity "·
_Mercury ·· __ .Copper __ ms ... ,
,~ekniurn_ ·-_._Fluoride _TOC
Silver __ Iron --. . . _Lead ····· --.. __ Manganese -. --1· . __ Mercury ' --
·. , .. _.·:, -.. , .. •' .. _· _Nitrate . . . . . --. . '" ,,
" .. ... ~ ·-· . • .. ,, . Selenium
'., , ... :. __ . f r ORGANIC CHEMISTRY~
_ lParameter Results mg/ 1 ParameLcL Kesults mg/1 Parameter Result., mg/
. P&T:GC/MS lEDB IV'± _K_ Met.¾oxychlor ::~ _ L Acid:B/N Ext. Cf.I±. ...JLPCB's <Q. 000 /1f?ti1. LToxaphene
tTOX ~ Petroleum Af,4-I . _x_2,4-D·· . <0,00
.JLEndrin <o.ooo;~_ .$_ 2,4,5-TP c,il;ex) <o,oo/
.. ..::l,,._Lindane ./IL . . -<:o,a.12.
MICROBIOLOGY RADIOCHEMISTRY
Parameter· Parameter Results PCi/ 1 f (MF) Coliform Colonic:s/l00mls __ Gross Alpha
(MPN) Coliform Colonies/l00mls __ Gross Beta
----
'J Received J / -,::;I/ -fS(jJ
· .Pest-. 'At\
) Extracted , ; -;i-'-\e f6
Date Reporred ,==:,,-.,,,,=,-----------P£S7, 'I' -J>Z!e:r
Date Analy-..ed /.;1.-/S"·l"t.-V:'f,
:'f'rted By ---------------Lab Number _____ -6-=-.;'....:'J=-' =1:..:'1::::.2:_ ___ _
lf,)JQJ (Rrviocd 7185)
,r,J anJ H:i::irdou1 W2!oH' fRt'vi~w 7/87)
C. Department of Hu in.an .Resouccc:~ din ofHeal~h Scrvic~ _.·. . SAMPLE ANALYSES REQUEST . ·.
St.ate Laboratory of Public He
. P. 0. Box 2$:
. . . 306 N. Wilming,:on S,
... ':' .::.-.. •.•.. R.,..leigh, 27·
l uo.mf_ sb,.er.re: .. __.o ... · ~1...;tw:D;...·~-.... n-"'--'-1__,4_,_}-"5:;..._9.__;;:;3_2.. ___ Field Sam pie Nu;,;be~ _.c..3_-~_"9±.;c_...t_· -------"----
_ . .;J.F2_,.,_-'=-c.,""--"~x.__-_,· ?u.~~~~~c..,...'1we2c:..<..:;7'-'-6:c~_,__ ____ . s;re Loca."ion . /...Uk$ f.-; ~s 4-:c /Jc_.
,!lifted By 7Z; 1<:.,r; c..b ~ 7/4 ,,...,,,., · ID# _·_..3'"--:/--'----Dare Collected -..!/...:./_-_..2'-"0'---~_..-.,,.6..._ ___ Time /JS>
flllof Sample:
Eitvironmental
..L Groundwater (1)
,.--Surface Water (2)
_a_:_ Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments ..
tuf' ~.::g 1vJ. S..o,0 • ,
r Other (4~-
INORGANIC CHEMISTRY
Extractables
Parameter
11Arscnic
ii Barium :· ·
_Cadmium
__ Chromium
... Lead
_Mercury ·
Selenium ·
-1 -·--. ·--·-Silver _
. .
Parameter
P&T:GC/MS
_ Acid:B/N Ext.
Results mg/1
Results mg/1
N'.A
:J T_o_x _________ _
Total
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride ·
__ Chromium
__ .Copper
__ Fluoride
__lron
_Lead.-
__ Manganese ..
· __ Mercury
_· _._,Nitrate
__ Selenium
Results mg/ 1
ORGANIC CHEMISTRY
Param
-LEDB
_lLPCB's
iPerroleum
lEndrin
.:i,.._undane
esu ts mg/1
Parameter·
__ Silver ·
__ Sulfates
__ Zinc
_Ph
__ Conductivity .,_·.
__ TDS :-~:·.·
_TOC
Re.ults mg/l
Parameter Results mg/
L Methoxychlor
LToxaphene
___x,__2,4-D · ·. L 2,4,5-TP (silvcx) ____ _
L _. ---------
MICROBIOLO=-G=-Y=----------,----,-----'RA:..::;_-=.D_IO.:.....::C.:cHE=.cMI.=:=S_::TR.:..:..:Y ____ _
Parameter
J (MF) Coliform Colonies/l00mls
_._ (MPN) Coliform Colonies/lO0mls
Para.meter
__ Gross Alpha
__ Gross Beta
Results PCi./ l
)I Received -------------'---------Dare Rcporrcd
)· Extracted---------------'-----Dore Analy-.ed -----------------
Lab Number ______ ("--o ._,/';-"-,°'.3-'-'-( :t ......... ;j__=------
V OI/ -TL0-f c111-0. f y zed, •.
'-<f>rted By
>""'JJQJ (R,vi1<d 7185)
:\1ltJ :rnJ H,1,::Jrdou1 Wa,re (Revirw 7/87)
I
C. Department of Human Resources
vlon of Health Services . . SAMPLE ANALYSES REQUEST
. 9$/,fY~'f$Z f!O..V --.!.:.L.:::~[Q__j
atory of Public Health
P. 0. Box 28047
N. Wilmington Street
Raleigh, 27611
iwiumbcr l2_Z D __lJ?Lfl.-?--ft 96 Field Sample Numbc, _ __.3'."-'7~.s-Q-=---------
1& of Site «c-W~Jf.,._ SiteLocmon a/4a4o'aln-. -NC..
ojjctcd By ~ ~"j IDlf -~½: .... ~..._-Date Collected .Z le (1, :.I RC. Time ___./,.u:½u•-' </,._(..,.)'---'
rl of Sample:
Environmental .-t--Ground;,,,.ter (1)
__ Surface Water (2) I-Soil (3)
__ Other (4)
Concentrate
__ Solid (5)
--Liquia (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMISTRY
Extractablca
Parameter
_Arsenic
Barium
.Cad:-r•···-, · • .. -£l
_Chromlnm
:__Lead
~Mercury
, _Sckniu.rn_ ._
.:__Silver
t -l= ll
Parameter
'•! P& T:GC/MS -r-Acid:B/N Ext.
' TOX . . r------
Results mg/ 1
Results mg/1
MICROBIOLOGY
.!~ Parameter ·
! J-(;.,ff) Coliform Colonics/lOOmls
'L (MPN) Coliform Colonies/lOOmls
l "!:
Parameter Results mg/ 1
....&:.. Arsenic <O c,J
-&Barium <o, l
-6Cadmium <.£.<9&.S-
_Chloride
....X..Chromium .L_ l), 2>1
__ Copper
__ Fluoride
__ lron
_k_Lcad < Q,0:3
__ Manganese
-¥-Mercury · ~ ,Oot':3
__ Nitrate.
__ . Selenium ,,.,
' ORGANIC CHEMISTRY
Parameter
_EDB
__ PCB's
__ Perroleum
__ Endrin
__ Llndane
. Results mg/1
Parameter
__ Gross Alpha
__ Gross Beta
Comments
Total
Parameter
__ Silver
_Sulfaries
_Zinc
_Ph
--Conductivity
_TDS
_TOC
------------
Parameter
--Mdhoxvchlor
__ Toxaphene
-2,4-D
Results miv 1
Results mg/1
__ 2,4.S-TP(silvcx) ______ _
RADIOCHEMISTRY
Results PCi/1
,_a R d D R d 9-//-'06
"a" ccdve -----------------ate cportc ---:---------------
0,j,e Extracted------------------Date Analyu,d __ _..fl----;--:,;;::;-.-.~rn;r-:O"l'J""::--::------
1 17245 AUG (.8 c•
: ,01ted By Lab Number ----------~------
",i1S 3101 (Rev,.,d 7185)
1'l:·oepartme.~t of H·.iman Resources
Division Of He&lth Services SAMPLE ANALYSES REQUEST
State Laboratory of Public Health
P. 0. Box 28047
306 N. Wilmington Street
Raleigh, 27611 111. fft4?S "l~Z ~-
Sire Number _0~7'"-t._.)"'-[Jf.,_,_/_¼~1----IZ:l'"'-~--a~---·---Field Sample Number _3~2=•;.,.J,o=,c...· __________ _
fne of Si~e __,_F_C.=X.c.,---"~...c...,..'--~-H-'-'-,_...,_c;..."---r,-o.c....,,.;________ Site Loca.ion -'{..,V~--'-"-'$'-H'--'--,'-'""'=-<,"-'--r_o'--',.;"-------'-N_C.=-------
Collected By --~ff'-"--·-J/4-&.µ...::'---"''"~=ecll<_,,,d,.---ID# __ '-f~..ecp __ Date Collected __.2"'-"',:.,_.19a..:v"-'6-=-~Z'..._.6.__ __ Tim~ _J../J.:02'•'-'' Vic..:cl::_____,
1t,eofSample:
~nvironmental )1-L-Groundwater (I)
___ Surface Water (2)
·q JI--Soil ( 3)
II. __ Other ( 4)
Concentrate
__ Solid (5)
__ Liquid (6) ·_,
__ Sludge (7)
__ Other (8)
Comments
_5',s,-P,:.C: z,6 A_J_::, 7'
INORGANIC CHEMISTRY
Extractable•
Parameter
Arsenic
__ Bat'ium .
It= Cadmium ·
Chromium·
i_Lead
Mercury
Selenium ___ _
__ Silver
Results mg/1 Parameter
__ Arsenic·
__ . Barium ·
__ Cadmium
__ Chloride
__ Chromium
___ Copper
__ Fluoride
__ Iron
__ Lead
__ Mangane~e
__ Mercury
__ Nitrate.
__ Selenium
Results mg/ 1
Total·
·Parameter
__ Silver
__ Sulfates
_·_zinc .•
_Ph
__ Conductivity _______ · __ ms '·
1
• '
_TOC
ORGANIC CHEMISTRY
( Parameter
_ P& T:GC/MS , _J'.,.. EDB
~ Acid:B/N Ext. V ....M'... PCB's
11---TOX : -K. Petroleum
Results mg/ 1 Parameter Results mg/ 1
111. f.J-.
.II/. 0'
Parameter·
...-1".. Methoxychlor
~ Toxaphenc
.A...2,4,D
X 2,4,5-TP r, \vex)
Results mg/1
· Results mg/1
1,1/
_.!J4'µ"'-'-5 _____ . I ..,. qµs
F: ---------------
1
.X Endrin _______ '_K Lindane
----------------'-----------------·······-·)
MJCROBIOLOG7: RADIOCHEMI~ _T_R~Y_:.. _____ _
Parameter
(MF) Coliform Colonies/lO0mls 1--(MPN) Coliform Colonies/l00mls
Parameter
__ Gross Alpha
__ Gross Beta
R•,sults PCi/ 1
ate Received --'"'-,r'----'-'-''--='__,_c,_..,."''11+-~"-----=----Date Reported -,-------------------
• ~
-,:27-:?0 _".]) .
fJiJ a, v(-YV 2-0 , r!i?:_a ..,_ 5fPn. ;t:e-.•r. · ,,, .
Date Extracted ➔ {!])JI, 1 7. -.£'..!. -Vl/ til1K Date Analyzed /P·/J-Yo 1{?
II Lab Number 6 1 iZ421 llcportcd By' __________________ _
C. Department of Human .Resource!> ·i1n ofHcal_'h Ser~ces · . SAMPLE ANALYSES REQUEST
State La.:,Or::itory of Pu':>lic r.~..:
P. 0. Box ~0~
306 N. Wih.i"l:!on Sr:
lulci,;h, 2 ic
l umbe.r_ {J/i) 97!/ 415 -/32-. Field Sample Number
of Site . fl.'.-,X -tu~ C..:, e2 7 6,-.---Site l.o=ion lO&<.~ f-"r ,,.s 4-c /JC
l• tedBy c;?:;.tC,,7 e,.(:;, /4,.,..,..-, · ID#??-DateCollected //-zo-"?6 Time /410 I ~~-----~~~~-~~----
of Sample:
911vironmental
.Ii_, Groundwater ( 1)
-.---Surface Water
_.__ Soil (3)
(2)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments
# tu/'-9 ..v.J. 5,.,,..,
•
r Other (4)
INORGANIC CHEMlSTRY
Extra.ctables Total
Parameter Results mg/1 Parameter Results mg/ 1 Parameter Results m~/1
1~:;un!_ . __ Arsenic __ Silver
_·_Barium __ Sulfates
_Cadmium··. __ Cadmium __ Zinc
=-Chromium __ Chloride __ Ph
Lead __ Chromium __ Cor.ductivity
,_Mercury __ Copper _ms
,~eh,niul"_ .. __ Fluoride _TOC
Silver __ Iron --__ Lead ... --
-__ Manganese --
f . __ Mercury --
__ Nitrate .. --
Selenium
-1 ( ORGANIC CHEMISTRY"'-)
Parameter Results mg/1 Param~--· Ke&ults rog/1 Parameter Results mg/
~ t P& T:GC/MS ....LEDB t::/J-L Methoxychlor <o. OQl/¥J.12l
_ Acid:B/N Ext. N{-1-_lLPCB's < '2., Q(2_(2_[pprn. LToxaphene -c:::o, (2_0.:Z.i'fP-aJ
:tTOX ....::l..... Petroleum !VA-...)Lz,4-D /Q,0O/
..LEndrin ~::~ ,d.J 2,4,5-TP (silvex) -<'o.oo I
....1,_ Lindane --MICROBIOLOGY RADIOCHEMIST:R Y
Parameter · Pa.ra.meter Results PCi./ 1 =I (MF) Coliform Colonies/l00mls --Gross Alpha
(MPN) Coliform Colonies/l00mls __ Gross Beta
----
---
,.,.,rted By
,,!)JQJ (R,viocd 7185)
Lab Number 6::3143
•.i!iJ rnJ H;i.::irdous W:astc (Rc\liC"w 7/87)
State L.a:>Or;ac-ry of Pu':>Lic '.:'"!:-.
. SAMPLE ANALYSES REQUEST P. 0. Box 28~
306 N. ~'il:nhg:on S:::
JWeigO, 2it
e fj umber __,Owc.....1..l_...D~· . ...!.ecff~.!./---'4'--'-f--=5:::;__QL..( ..:::3:....2...=---Field Sample Number
rl of s;;; f:C., X -t6a ... < C.., a 7 6,-.--, Site Loc,.;ion lUeq; f.. 'i ~s fe...c tJC
'X' edBy ?2,~;/:._,,c,{.c /4,.,..,...-, . ID# "2;?-DateCo!l•cted //-zo-<?[6 T /1-10 7 -""'-:_____ --'--'--""-'"--""-=-----1:ne
-. f Sample:
Et,'ironmental
__L Groundwater (1)
,.-Surface Water (2)
JI._ Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6) ·
__ Sludge (7)
__ Other (8)
Comments
# tu?-9: JJJ-.
r Other. (4) ·
INORGM"'IC CHEVJSTRY
Extractables Total
arameter Results mg/1 Parameter Results rng/1 Pa.ameter
=I Arsenic __ Arsenic __ Silver
Barium · · __ Barium __ Sulfates
_Cadmium __ Cadmium __ Zinc
=-·Chromium __ Chloride __ Ph
Lead __ Chromium __ Conductivity
_Mercury __ Copper _ms
l_Sefrniurn_ ·-__ Fluoride _TOC
-Silver . __ Iron --
__ Lead --.. __ },fanganese ---
j __ Mercury --
__ Nitrate --..
Selenium
Results mg/!
i ( ORGANIC CHEMISTRY "',
Parameter Results mg/1 ParameLc1 Kesults mg/ 1 Parameter Results mg/
P&T:GC/MS NA ....LEDB L Methoxychlor
_ Acid:B/N Ext. -LPCB's ..J5_ Toxaphene
=ITOX i Petroleum ..X...2,4-D
lEndrin j 2,4,5-TP (silvex)
...::l:.___Lindane -
,. MICROBIOLOGY RADIOCHEMISTRY
Parameter Para.meter Results PCvl -I (MF) Coliform Colo:,ies/lOOmls __ Gross Alpha
__ (MPN) Coliform Colonies/lO0mls __ C-,-oss Beta
------
:,'II Received
·h~ Extracted---------------'-----
-----------'---------Date Reported ________________ _
Date Analy::ed ________________ _
Lab Numc-er ,/ r, l'lB /1.f. ~
Voll -Nof-a11_alyzed
~,.,rted [ly
,,,.)Io I ( R,vi,d 7185)
!-.,l1..! lnJ H.t::irdou, WaHe (Review 7187)
. SAMPLE ANALYSES REQUEST
State Laboratory of ?u:Jl.i, He.;
P. 0. Box 23:
306 N. ~'il:..i~on S:
•1um12,e_r 01[} W/ 4l-5 '/32-.
R.lcibh, 2 i1
Field Sample Number -~3_--'.'5t_:c....:0=-'1-'--------'---
Site Lo=ion t-0&<..s (.. ~..., S ft:c of Sire EC-,'( -t-O~ C.. "1 a 7 /2-r
lured By ?J;;. /4_,;-cG ~ 7/4 ,T>"'"> ' ID#_?~_?--___ Date Collected ~/~/_-~z_o_--~~6 ____ Time
JlofSample:
Etf'ironmental
_L_ Groundwater (1)
r. Surface Water (2)
~ Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Comments :r. F Re./2.m
-r Other (4)
INORGANIC CHEMISTRY
Extractable•
Parameter
ii Arsenic
-JIBariuin
__ Cadmium · ·
_11 Chromium
II Lead
_Mercury · .1Sekniurn __ _
. -Silver
Results mg/1
j----
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ Copper
__Fluoride
__ Iron
__ Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
Total
Results mg/ 1 Parameter
, __ Silver
__________ Sulfates
-~-----; __ Zinc _______ , __ Ph
_______ •---Conductivity ______ ·_ms
_TOC
Results mg/l
i---------------------
ORGANIC CHEMISTRY ,
Parameter
P&T:GC/MS
Acid:B/N Ext.
Results mg/1
=I T_o_x __________ _
MICROBIOLOGY
Parameter·
-I (MF) Coliform Colonic:s/l00mls
_ (MPN) Coliform Colonies/l00mls
Param
lEDB
..LPCB's
iPerroleum
_..2l_ Endrin
...:E,__ Lindane
I Received //-;J f -?5 ( 0 . ffe'/ft 1-f!A Ped M,vr, F6
) Extracted '@-Ol-.'fef? ,(JJJ 12-1 ~ ~4 .
'.,.,rtcd By
)~)IOI (R~vi1ed i/85}
diJ :.nJ H;,::irdou, \Vastc-(Rc-vii:w 7187)
CSU ts mg/1
Parameter
__ Gross Alpha
__ Gross Beta
Parameter Results mg/
Resu!"ts PCi./1
Date Reported ==::-::-;-,;,;:;:.;,,,-:-----------PE.IT o/ pc:a_ -;y
Date Anal,~d /;;J...-/6-cf'~-Y,7';
6!'3145
Lab N,;mber ------------'------
.-.,. ,·i :;..:irtri:i,cnt of Human_.Rcsou.rc.c:. State L..'oon.tory of Pu:J:.ic '.:-"::-
II·_·.' o_r_ .. ·H.·c·• . .1_,_h_·.•se'r··,ice,. . SAMPLE ANALYSES REQUEST P. o. Box 2cc; II 306 N. ~'il:r-i:,.g:on S::-.:-c•
. . R....lei~h. 216 l
l;,,.:,b;,. ,(}=· ~7-._·..,.l"--.) _. __.7?'-"'--'-/_4...,__·._f==c5__,_o/--=3=---2-c;___ Field Sample Number __ ..=3::c.=S-__e./_O ___ ____;____; __
.. n; s;;~· ..:...t:1~,:< -tUc£.<: {,_ ?o 7 ft-c Site Lo=ion t.(.)k6 (.~ "S ft..c /JC....
., •. ;:;,,,-JBy c:2-;/_.)'tc.-bc /4,,,.,...-, 7
. ,;f :]ample:
. . : i a·,:,ntnen t:~.I I\: ___ Grnundwater (1)
g. _ Surface Water (2)
···-Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
Date Collected _:_/:_/_-__..,2c..:0:;_-_~.,_,,,._6:__ ___ Time
Comments
-:f.F. Qt!t,,,,,
1._ .. Othec (4) ·
INORGA1'"1C CHEMISTRY .
Er.tractables
·'1.mn1ct:!r Results mg/1
.
I:
I
I
·-r\i·,:;enic
~c.riu!n ::·· ...
: ·:~d::ib.frn
; ::-1:-omium
1 ..... ::1d .. , .·,,,,-::ci.1r1
: ;~Jrr:it--!rn -·-
• 1~i'/C?'
.. ,,
..•
-
.. ·-
·-
-·
.':-•.:~1.1ne'!:ct· Re•ults mg/1
·c'-:cT:GC/MS
,\.dd:B/N Exe. ··:..~vx
..
.
-
Total
Parameter Results mg/1 Parameter Results m~/1
__ Arsenic __ Silver
__ Barium __ Sulfates
__ Cadmium __ Zinc
__ Chloride _Ph
__ Chromium __ Conductivity
__ .Copper _TDS
__ Fluoride _TOC
__ Iron --
_Lead , . --
__ Manganese '. --
__ Mercury --
__ Nitrate .. --
Selenium
( ORGANIC CHEMISTRY~
ParamcLc< Kesults mg/1 Parameter Results mg/1
-'LEDB ·,-.JI'.\ L Methoxychlor t,1 A
-lL.PCB's NA L Toxaphene 1,)A-
_:$._ Petroleum NA ...::lL2,4-D NA-
-2LEndrin NR-.£ 2,4,5-TP (silvex) NB
.LLindane 1'I CL L
• --MICROBIOLOGY
Pa!'c'..".metcr Parameter
RADIOCHEMlSTRY
Results PCi./1
i)/1") Coliform Colonics/lO0mls
r:., PN) Co!ifor,11 Colonies/l00mls
__ Gross Alpha
__ Gross Eeta I
I_ ·-----------------------'-----------,-----------
------------------Date Reported ________________ _
1·'
. !'',"
Dote Arul;-..ed --------~~-------
Lab Number ____ 6_._· .,_J_l_4_6 _____ _
··.-ir-~·d 7 /85)
:w.•.;~ ·.r1:.,,t~ (f\.e\·i~w 7/87)
STATE LABORATORY Of PUBLIC HEALTH I
I
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUNAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGAN C OlEIIICAL • LYSIS
BASE/NEUTRAL AND ACID LAB NO ,:,opL/o /_ ;;, /J..2 l/ () 7 I.A ?U,:J,[/ /. o;lu O<i
EXTRACTABLES FIELD ti 3;2.o/ ?.2 () 2--:,~oJ JJ,..4 y
COIIPWND TYPE ( 3) C 3' l I 31 I , l
UNITS .. n/1 t •"/kn .,n/\~ko\ .. n/1 /4/kn .. n/1 ,uo/ka)
-nitrosodilrethvlamine "~ I , ., t>r-1-
isl2-chloroethvllether I r i
-chlo~henol I I I
henol I I D 3-dichlorobenzene I I
,.4-dichlorobenzene I I
1.2-dichlorobenzene I I I
is(2-chloroi llether I I I
xach 1 oroethane I I I
N-ni troso-di -n...nrmvlamine I I
i trobenzene I I
•soohorone , I I
-nitrnnhenol I I I
2 4-dimethylphenol I I I
is(2-chloroethoxvlmethane I I
4-dichlornnhenol I I
1.2.4-trichlorobenzene I I
~hthalene I I I
achlorobutadiene I I I
4-ch 1 oro-m-creso 1 I I
I ~xach 1orocyc10DPntadi ene I I
4.6-trichlornnhenol I
-chloron•nhthalene I I
acenanhthvlene I I
imethvl ohthalate I I
6-dinitrotoluene , I I
acenanhthene ' I I
4-dinitrnohenol It, ,td I I
4-dinitrotoluene 3..3,:, I I
4-nitrnnhenol I t,tJ /J I I I 'luorene 330 I I,
-chlornnhenvlohenvlether :SJV I I V
iethvl Phthalate J31J I . 3 3DJ:
i.6-dinitro-o-cresol IL.10 I I I.,,
iPhenvlamine /6tl<J I I Ir.? iJtJ/<:..
zobenzene Jtty(.) I I I I •
4-branoohenvlphenvlether po I I I I
exachlorobenzene 330 I I I I
ntachlornohenol /600 I I I I
ohenanthrene '3J() I 11 I, I
nthracene 3Jo '-.Jj \/ VI w I ibutvl ohthalate 3JCI /? :S3or J -iD/( 5] ().<' -:,Joie
1 uoranthene -:JJo I,( 1/J 0 I~
f -/ . l fT}f))... ~ -/-o"."'-"' ,.,., ~/tl~k.._uJJ/iu. 15,,,·1) • -Estimated value. . G..! '.J. I
-Actual value is known to be less than value given. L -Actual value is known to be greater than value given.
-
-Material was analyzed for but not detected. The numer is the Mininun Detection Limit. A -Not analyzed. -
I -Tentative identification.
_I -On NROC List of Priority Pollutants.
■. C. V.i.v.u.,.i.on 06 He.a.lth SVtv.i.c.v.. a.is 3068-0 {4/86 Labo!Urto~y)
(j)
1 tJ:l'/ro loi::L '-I-I I
'l Z-41~ 3 ,_, (,
( J l C _J l
un/J •'"/kn/ un/ Vua/kn)
I /Jr
' '
I
I
I
I
I
I
I
I
I I .
'-!.{
-51Qk .., /<3' 3
I • VI
I I
'I/ I
' I .
-(50V \I/
l,,. 7, 5 oo
I 1.
I I,
I
I
I
\If
11 LI-JOO
V ,
IA
:?3ok_ I
(,._ I
vr I
IA I
V1 I
9.?35 I,
I Lot VJ
L1 l,3JJ
l,i 1,,.
330)(
l-1 IA
STATE LABORATORY OF PUBLIC HEALTH
I
I
I
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESWRCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
I
I
I
I
BASE/NEUTRAL AND ACID
EXTRACTABLES
COl1PWND
nvrene
benzidine
butvl benzvl ohthalate
benzlalanthracene
chrvsene
3 3-dichlorobenzidine
bis(2-ethvlhexvllohthalate
di n--octvl ohthalate
benzo(blfluoranthene
benzo(k)fluoranthene
benzo(alnvrene
i ndeno (1 2. 3-cdl nvrene
dibenzola.hlanthracene
benzorn h. i)n,,rvlene
aniline
benzoic acid
benzvl alcohol
4-ch loroani 1 i ne I
I
I
rf=
I
dibenzofuran
2---methvlnaohthalene
2---methvlohenol
4---methvlohenol
2-nitroani line
3-nitroaniline
4 ni troani 1 i ne
2.4.5-trichloroohenol
e.,,'rfl e"'t2.."""'/11,p,,
I
LAB NO
FIELD #
TYPE
UNITS
33 o
/l,()11
33V ~o
3Jo
j/,,(Jt)
3?1
::iJo
/too
' J
I I. 00
"1i.11t)
jLA,J
-<-:io
-:?3,0
"330
3"..tll
,Jo
;,, /J ti
l6nd
/£.po
I 11, a
3Jl
ORGANIC CHEMICAL ANALYSIS
r: r) 7 ///, /_ 1-01uo7 1-o1t(,;y
3,2.0I 3 1-v",,-'?l--a3
l _:3 l l 3 l ( '31
un/ 1 £a/kn un/1 /4/kn ••ft/1 r.,n/ko.
<>r IY l,i
I 1
I I
I I
I I I
I \I/ I
I ?YoK.. I
I ~Tok I
I I A I
I I I
I I I
I I I
I I I, I I
"!.I \I/ -w
Vi IA L-t
I I I
I I I
I I I
I I I
I I --I
I I I
I I I
I I I
I I I
I I I
---.. \I/ w \'/
Gt l1 V\.
IJ -Estirrated value. K -Actual value is known to be less than value given.
l~o2 \lo '1
32-.,r-
l .J l
un/1 ,in/ko
c:;-
i
I
I
I
I
I
I
I
I
I
I
I I
\J
L-t
I
I
I.
\Y
-:, "J tik
L-,i
I
I
I
I
\V
JJOe
L -Actual value is known to be greater than value given.
I U -Material was analyzed for but not detected. The nlllber is the Hininun Detection Limit.
NA -Not analyzed. _ 1/ -Tentative identification. . ff -On NRDC List of Priority Pollutants. IN. C. V.i.v.i..o.i.on 06 Hea.Uh SVtv.i.c.u,
VHS 3068-0 (4/86 Laboti.a;to~y)
l~O) Cf! o /A f) / y. //
}2-''.> ~2-<J?
l 3 l r J l
··-/1 f-n/kol un/)" ••n/ka)
,--;;---o,-
I I
I I
I I
I I,
I VI
I 3lok'
I -r;,
I I
I I
I I
I I
I , I
V , I/
~
I -l,1
1 •
I I
\J
I I t,7 J
,.333:F
~
I
I
I
I I
II/ . ·--·-
\/J ,~ V\
'
I
I
I
I
I
I
g
PURGEABLE COMPCXJNDS
COMPOUND
chloronethane
brararethane
dichlorodifluoronethane
vinvl chloride
ch l oroethane
irethvlene chloride
trichlorofluoronethane
ethene. 1. 1--dichloro
ethane 1 1--<lichloro--
1.2-trans--<lichloroethene
chlorofonn
ethane. 1.2--dichloro--
ethane. 1 1. 1 trichloro--
carbontetrachloride
branodichloronethane
H
I
I
lnrnnane. 1 2--<lichloro--
l 3-trans--<lichlo, ne
trichloroethvlene
chlorodibrararethane
benzene
ethane 1 1 2 trichloro--
1 3-<: i s--dich 1 o ne
2-<:hloroethvl vinvl ether
brorofonn
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPAATMENl Of HUAAN RESCXJRCES
P.O. BOX 28047 -306 N. WILMINGTON, Sl., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
/~, /I -. -. /., t'l.:; J./rJ 'I /./1(;2_4/))i?' /~ /1 74,y:/ LAB NO .,
FIELD I 3;:l..c I 3,1,c 'J.. TZ-d] JUI/
TYPE ( 3 \ ( 11-) C LL l ( 4-) -
UNITS un/l(ua/kQ' un/1 G/ka un/1 ,<n/kd .,n/Jrun/kii'
/() u:::::,, 1./4-· I, -;-, .
,'D
.20
}()
/<)
'i
;)_.c)
'J
,
I I)
5
ethane. I. 1 2 2 tetrachloro--
ethene, tetrachloro--
toluene
ch lorobenzene /
ethvlbenzene \I/ / / / ., /
acetone JO J .J I,.,<..--1./-,,
2-butanone ID 1/, I / . J'
/ .. " ; -' JJ.os-'
( tJ. ) ~
un/] l':,n/k-;.
t.0'
•/
u,....,'
/V
I
I
I
I
I
carbondi sulfide s--6',5 J 1'-!'1'70 J
2-hexanone /D I I I I
4--<rethvl-2-""ntanone lo
stvrene !,
vinyl acetate /0
o--xvlene !, I ' I ' I ,,
,,.u, .• r--· J~ +/ ( ) ,-) f.l? ,~.,
I
J -Estimated value.
K -Actual value is known to be less than value given.
IL -Actual value· is known to be greater than value given.
U -llaterial was analyzed for but not detected. The nurber is the Minil!U!l Detection Limit.
l/ -Tentative identification. · · r-r y Pollutants.
Division of Health Services
DHS 3068--0 (4/86 Laboratorvl
,/
r-J
CJJr,·,iT,j
32-d (,,
( "-\
un/] f.,•/ki(J
LL--
I
,~
.. /
(f-_)
-.._
STATE LABORATORY OF PUBLIC HEALTH I
I
m
I
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
g
D
n
D
u
I
I
I
I
I
I
BASE/NEUTRAL AND ACID
EXTRACTABLES
COKPOUND
N-nitrosodimethvlamine
bis(2-chloroethvllether
2-chlor~henol
ohenol
1.3-dichlorobenzene
1,4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n !amine
nitrobenzene
i~horone
2-n i trooheno 1
2.4-dimethvlohenol
bis(2-chloroethoxvlmethane
2.4-dichlornnhenol
1,2 4-trichlorobenzene
n;mhtha 1 ene
hexachlorobutadiene
4-ch 1 oro-m-creso 1
hexachlorocvcl~ntadiene
2.4.6-trichloroohenol
2-chloron,nhthalene
acen~nhthv 1 ene
dimethvl ohthalate
2.6-dinitrotoluene
acenaohthene
2 4-dinit~henol
2.4-dinitrotoluene
4-nit~henol
fluorene
4-chlornnhenvlohenvlether
diethvl Dhthalate
4.6-dinitro-o-cresol
diohenvlamine
azobenzene
4-b~henvlohenvlether
hexachlorobenzene
=ntachlo~henol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
LAB NO
FIELD#
TYPE
UNITS
I fl
.
' I
fo
Io
50
I iJ
//}
/0
,<) .,o
<,7)
lo
/0
!,"7>
iD
id
Id I?
/0
~.AM C CHEPUCAL A
I'. 0 ,,/1/ ('.L la tJ;il/l ;
3:lb7 · 32.ofr
( .) }_ ( -3 )
un/J/un/ka. ..n/1 ,Cn/ka
~
I I
I I
I
I
I
I
I
I
I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
.1 I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I, I,
~ '!J
.~?ok. ?70k
IA 1301<
q-F,,~ ,,.,d ,n' /JI«~/:... /n(}L
J -Estimated value. u.4// wtI.,l<r I IK -Actual value 1s known to be less than value given.
IALYSIS
I;__; t').2£//CL h c!.21..f I J
320'1 JU<>
( r l f /l
/.,n/1 J .. n/ka l,Cn/J) un/ka
-/V/1--~ ·1
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I I
I 11
I V
I , /OK
\I/ 0
L -Actual value is known to be greater than value given. -.U -Material was analyzed for but not detected. The nl>lber NA -Not analyzed.
is the Nininun Detection Limit.
1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants .
•
. C. V-i.v,U,-i.on 06 He.a.Uh Sv,.v-i.c.v.,
JHS 3068-0 {4/86 Labo/ta.to~y)
(j)
latJ2l//6 /~ tJ7-'f(7
311/ 3.21(,:,
r /1 . ( I l
un/1 un/ka ," ,-,;;7f": • n /kn
IV"'"' ~ t/J
I ,7
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I I
I
I
I
I
I
I
I
I
I
I
I
I
I
I.
V
, /,:;J:::.
\V I,'(_
,.
I
I
I
I
D
u
BASE/NEUTRAL AND ACID
I
I
I
I
I
EXTRACTABLES
COPIPOUND
pyrene
benzidine
butvl benzvl nhthalate
benz!alanthracene
chrvsene
3.3-dichlorobenzidine
bisl2-ethvlhexvl'"hthalate
di-n-octvl ohthalate
benzolblfluoranthene
benzo(k)fluoranthene
benzo(a)nvrene
indeno(l 2.3-cdlnvrene
dibenzo(a.hlanthracene
benzotn h il=rvlene
aniline
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran
2-methvlnaohthalene
2-methvlnhenol
4-methvlPhenol
2 nitroaniline
3-nitroaniline
4-ni troani line
2 4 5 trichlo~henol
/'. /1 -~· IA e,.l--/7 .
I
I
I
I
/
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUPIAN RESCXJRCES
P.O. BOX 28047 -306 N. WIL"INGTON, ST., RALEIGH, N.C. 27611
ORGANIC OlE"ICAL ANALYSIS
LAB NO !. ,,·i I/ 12 1.()2~/'3 I. 021/ I (( ;;, {))'f h
FIELD# , z..t7 "31-•Y J'].,r'f 32/{J
TYPE I 3 l I ;I l ( I ) ( I l
UNITS un/l/ua/ka, ··"/1 ,.-Cn/kn) ··"/1 •·"/ka ,,oofl, un/ka
10 IA '!-,-NA ~ -
57) I I
ID I I
/tJ I I
/u I, I ,
57) 'II I
/0 ::,J'ok I I, /4::
I o IA I <: 't)Y
6/) I I t.-i
7.u I I
So I I
52) I I
(d I I
!,?> '\I ,,; ' '
~ l-1 !. ,vrr I
~2' I t'
,71 I I ,~ I I
JO I I
/0 I I
I ti I I
/2 I I
~7) I I
0 I I
t,? I I
CJl ·w ,,; I -
s;'(I VJ VJ A//j-;;.,7, /',.
...,,.
I
I>'} fJL
"• I.JI ',~ -:,.~
IJ -Estimated value. K -Actual value is known to be less than value given.
!. ()2J// ~
31--11
( ( l
··"/1 ··"/kn
JA-
'
/1/ ,4
• I
A/Ll
L -Actual value is known to be greater than value given.
IU -Platerial was analyzed for but not detected. The nunoer
NA -Not analyzed.
is the "ininun Detection Limit.
1/ -Tentative identification. i1 -On NRDC List of Priority Pollutants. IN. C. V.i.v,u.,.i.on 06 He.a.Uh Svr.v.i.c.e/2
VHS 3068-0 (4/86 Labona.to~y)
/.()J.'f/7
'J :]./ (,
'/)
··"/1 -/ka
'1
Io/<
I/)
.
,
' I
IA
'
I
,_
'
I
I
BASE/NEUTRAL AND ACID
EXTRACTABLES
<X»IP()UND
N nitrosodimethvlamine
bis(2-chloroethvllether
2-chlo~henol
_ohenol
gl.3-dichlorobenzene
1. 4-di ch lorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-nitroso-di-n-0roovlamine
ni trobenzene
isoohorone
2-n i t mnheno 1
2 4-dimethvlohenol
bis(2-chloroethoxvlmethane
2 4-dichlo~henol
1.2.4-trichlorobenzene
l:;hthalene
achlorobutadiene
4-chloro-m-cresol
hexachlorocvcl~ntadiene
2.4.6-trichloroohenol
2-chloron>nhthalene
acen~nhthvlene
dimethvl ohthalate
2.6-dinitrotoluene
acen~nhthene
2.4-dinitrnnhenol
2 4-dinitrotoluene
4-nit~henol
fluorene
4-chlo~henvlohenvlether
diethyl ohthalate
4 6-dinitro-o-crosol
diohenvlarnine
azobenzene
4...1:Jraooohenvlohenvlether
hexachlorobenzene
ntachlor=henol
ohenanthrene
anthracene
ibutvl ohthalate
fl uoranthene
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
,,.,,..u C CHEMICAi • •LYSIS
LAB NO 1,, o,;u;-I :r /. ,,j ).LI-( 9 /,. A J t/;.L. i:.. /,. O;,L.u 'I I
FIELD I 32-17 -. "32/ f '31-N 3:J.J..o
TYPE I_/_ l I /l ( ( l ( I l
UNITS ,{n/J !.,n/ko ,<,,/ 1),n/ko .. n/J un/ko 1<n/JJ"n/ko
, V
. , ,,_,.. A • ,'I-'--" I
.
':'\
1,
',
" '-~
"
0.
~-i
I:'
\,'\
'V .
'
\ -
\
~'
'
I
' (Dk. , /Of<
' I 0 ' I t-i
IJ -Estimated value.
K -Actual value is known to be less than value given.
/
/
,t' / )
/.,n/J un/ko
l -Actual value is known to be greater than value given.
~
U -Material was analyzed for but not detected. The m1rber NA -Not analyzed.
is the Mininun Detection Limit.
I -Tentative identification.
_I -On NRDC List of Priority Pollutants.
Iii. C. V-i.v,<.1.,-i.on 06 He.a.Uh Svi.v-i.c.v., aHs 3068-0 (4/86 LQbo/f.a-to~y)
/
/
.,(' )
/.,n/J ,,n/kn
BASE/NEUTRAL ANO ACID
EXTRACTABLES
STATE LABORATORY Of PUBLIC HEALTH
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUIIAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO (/,O'J///Y ln/J"J.Jl./1!/ /, O 2lf2-0 ;,,, Cl 'J 1121
FIELD II 32.17 JU:f{ 3Z-l1 3 2-2-()
TYPE J-l1 c I i C I l _(. Ti
/
/
,I'' l
I
I
I
I
I
I
I
I
I
I
I
I
I
COIIPOUND UNITS ,(,n/1 ),n/kQ uo/1 .. n/ko ,ion/ J) .. n/ko .. n/1) .. n/ko ,{.n/J ,,n/kQ
nvrene '-c-/ 1/r l -._-,/A• -/ A
' benzidine
butvl benzvl ohthalate
benzlalanthracene I
chrvsene "'I
3 3-dichlorobenzidine ' I
bis(2-ethvlhexvJ'nhthalate !OK
di-n-octvl ohthalate ' /,,,
benzofblfluoranthene ... -
benzo(klfluoranthene " benzofa)nvrene "" i ndeno ( 1 • 2. 3-cdl nvrene "(l~
dibenzo(a.hlanthracene . I
benzo(Q.h.i).,..rvlene .l" ' I ' I '
\ ....1\1
aniline ~ ,-v,Lf IA N/J, t..,,
benzoic acid
benzvl alcohol
4-chloroaniline
dibenzofuran ' I\
2-methvln•nhthalene !l!
2-methvlohenol " 4-methvlohenol
2-nitroaniline '
3-nitroaniline ~
4-nitroaniline
2.4.5 trichloroohenol \ I ' " / ' I
I J -Estimated value. K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
I U -Material was analyzed for but not detected. The nurber is the Minin111 Detection Limit.
NA -Not analyzed. 1/ -Tentative identification. fl -On NROC List of Priority Pollutants. g N. C. v.;.v-i./2,fon 06 Hea.Uh SVtv,;_c.v.,
VHS 3068-0 (4/86 Laboll.ato~if)
/
/
,( l
{.o/1 un/kQ
I
I
I
I
I
I
g
g
D
D
H
I
I
I
PURGl:ABLE COIIPOUNDS
COIIPOUND
chlorcmethane
brcnorethane
dichlorodifluorarethane
vinvl chloride
chloroethane
inethvlene chloride
trichlorofluorcmethane
ethene. 1 1-dichloro
ethane. 1.1-dichloro-
1.2-trans-dichloroethene
chlorofonn
ethane. 1.2-dichloro-
ethane 1. I 1-trichloro-
carbontetrachloride
branodichlorarethane
orl'V'\ane 1 2-dichloro-
1.3--trans-dichlo ne
trichloroethvlene
chlorodibranarethane
benzene
ethane. 1.1.2 trichloro-
1.3-cis-dichlo ne
2-chloroethvl vinvl ether
bronofonn
--
STATE LABORATORY Of PUBLIC HEALTH DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUIIAN RESOURCl:S P.O. BOX 28041 -306 N. WILHINGTON, ST., RALEIGH, N.C. 21611
ORGAN IC 01EHICAL ANALYSIS H o . ;;)
LAB NO lnfi:Ji.J., Li /,.,/')_ "'II ,I// 11 IJJ. ',J /II? ,/ /l """I J '~"1/')
FIELD I J}_{)• 72.// ·~21-7 31-14
TYPE ..-1 I ) .• ( I ) k I l .. {. )
UNITS ua/1\' .. n/ka I ••n/ ff .. n/ka Fo,n/~ ·:m/ka .. n/J \ .,n/ka
/0 ,.__.. " -i .I ·u ---i·
/t)
2-()
lo
/0 ,,,
~ .
,
ID
~
ethane 1 1.2.2-tetrachloro-
ethene. tetrachloro-
toluene
chlorobenzene ,
ethvlbenzene • I ., I 'I ~ I ' I
acetooe /0 l i,,L i.A.. i ,
2-butanone Iv
carbondi sulfide '.)
2-hexanone ,0
~thv1-2~ntanone /J
stvrene ,;-
vinvl acetate Ji>
0-xvlene !, . I ' I I I
.,,...J..L -• ,,....._.~ .... /\.Aw, ... .-J 1 +-I (.. '\ (" ) r::.:,--.., (-)
I
J -Est1mated value. ~ -Actual value is known to be less than value given.
I
~r)_):.1./-::J
Jlo7
( :z )
.. n/1 ,:;;/kn
u.;.
/
'
I
(-)
Ill -Actual value· is known to be greater than value given.
IJU -Haterial was analyzed for but not detected. The m.nber
NA -Not analyzed.
is the Hininun Detection Limit.
1/ -Tentative identification. llf/ -On ~R~ ~ist of Priority Pollutants.
llN.C. D1v1s1on of Health Services
Dl!S 3068-0 (4/86 Laboratorv)
~
•
/.-r,7,1, "3
,uY
C :t l
··"/1 =tk~
[I:;;
' /
, .
\ /
C-I
STATE LABORATORY Of PUBLIC HEALTH
I
I DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT Of HUIIAN RESOURCES
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 21611
. ORGANiC OlEHICAL ANALYSIS
IBASE/NEUTRAL AND ACID LAB NO ln/J 3/ I/ "r / / /
EXTRACTABLES FIELD# .1'Fll'f ./ / /
COl1POUND TYPE ( i l I/ l ( /) I /l
UNITS /411 "":\n/ka .,,<; 1 .. n/ka ua'll uo/kn ,,J1 .. n/ka
l•itrosodimethvlamine ff) , ' ,
s (2-ch loroethvl l ether
2-chlo..,,.,henol
nol
3-dichlorobenzene
l 4-<lichlorobenzene
2-<lichlorobenzene
s(2-chloroi llether I
xachloroethane I troso-di -O-<lmnvl amine
robenzene
horone
2-nitroohenol
04-<limethvloheno l .
s(2-chloroethoxvlmethane
2 4-<lichlo,nnhenol
1.4-trichlorobenzene
hthalene
achlorobutadiene
4-chloro-<n-eresol .
ff•achlorocvcl~ntadiene
4.6-trichloroohenol
2-chloron>nhthalene
nenanhthvlene
methvl ohthalate
2.6-<linitrotoluene I
~hthene n i t rooheno l 5,J
4-<linitrotoluene /'-r!
4-ni t""'heno l ~ (/
uorene I iJ
hlo..,,.,henvlohenvlether /0
diethyl ohthalate /&
6-<linit~resol ">o
envlamine ',7/
azobenzene jV
"ranoohenvlohenvlether /0
chlorobenzene /?
ntachlomnhenol S"jj
,.nanthrene JO
thracene 1~
butvl ohthalate JO (;j /
fluoranthene JI)
I-Fe-..,~.I ,.,' 8/4,,t._
-Estimated value.
I -Actual value is known to be less than value given.
1
1 -Actual value is known to be greater than value given.
-Material was analyzed for but not detected. The nlllber is the 11ininun Detection Limit.
-Not analyzed. -Tentative identification. ·
lye~ :i::i~~to:f ::::Y ::~:::s.
S 3068-0 14/86 LabaM-ta1ty) .
, 7
/ /
'/i ( /)
,u<'/ 1 .. n/ka ,.,./1 un/kn
STATE LABORATORY Of PUBLIC HEALTH
I
I DIVISION Of HEALTH SERVICES, N.C. OEPARTIIENT Of HUIIAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
COIIPOUNO
rene
benzidine
'tvl benzvl ohthalate
nzCalanthracene
h~sene
3.3-<lichlarcbenzidine
isl2-ethvlhexvl'nhthalate
di-n-octvl ohthalate
benzolblfluoranthene
lt;nzo(klfluoranthene
nzo(a)nvrene
i ndeno ( 1 • 2. 3-cdl nvrene
~benzo(a.hlanthracene
nzoln h i'=~lene
aniline
benzoic acid
ben,vl• alcohol
4-chloroani line
dibenzofuran
2-methvln•nhthalene
2-methvlohenol
4-methvlohenol
2-nitroani 1 ine
3-nitroani line
4-ni troani line
2.4.5-trichloroohenol
D
11,6 -R,,-.,.,/ ,.,; /Jh11L IIJ -Estimated value.
LAB NO
FIELD 11
TYPE
UNITS ,~
So
/t!
/t!
It)
.S<l
It! a,
/0
'J7)
~
!,7
5P ID ;,
/D
/J
/o
l;"3
n
~
S7J
ORGANIC CHEIIICAL ANALYSIS
1-/) 1/ 'IS-/ /
357J't' / /
I_/ l 1/ ' ',71
l.n/1 J,n/ka ✓nn ••n/ka ··"11 .. n/ka
....__.,.IA / ,
,
' I
IA
\ I
K -Actual value is known to be less than value given.
/
/
1/)
uo/1 .. n/ka
L -Actual value is known to be greater than value given. IIU -llaterial was analyzed for but not detected. The m."t>er is the Ninil!Ull Detection Limit. II NA -Not ana 1 yzed. · 1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
~ . .
• C. V,i_v,<..o,i_o n a 6 H ea-Uh S Vtv,i_cu,
HS 3068-0 (4/86 LQboJta,tony)
/ /
/ /
C /l C/l
••"11 un/ka un-f] un/ka
.
STATE LABORATORY OF PUBLIC HEALTH
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
DIVISION Of HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
1.,0 ,?,iLi.f c, / / PURGEABLE CONPOUNDS LAB NO
FIELD# 'JS-) 0 -./ / /
COIIPOUNO TYPE I I l I /1 ,/ l 1/ l
UNITS uo/l}uq/ko .. ,r/ 1 .. n/ko £nil .. n/kq ..1,/] uo/kq
ch 1 oronethane • I I /
brooorethane
dichlorodifluorarethane
vinvl chloride
ch 1 oroethane
methvlene chloride
trichlorofluorarethane
ethene 1 1-dichloro
ethane. 1. 1-dichloro-
1 2-trans-dichloroethene
chloroform
ethane 1 2-dichloro-
ethane. 1 1. 1-trichloro-
carbontetrachloride
branodichloromethane
or~ane. 1.2-dichloro-
1 3-trans-dichlo ne
trichloroethvlene
chlorodibrooorethane
benzene
ethane. 1. 1.2-trichloro-
l 3-c is~ i ch 1 o ........... r,._,.,,ne
2---ehloroethvl vinvl ether
brcmoform
ethane. 1.1.2.2 tetrachloro-
ethene. tetrachloro-
toluene
ch 1 oroben zene
ethvlbenzene • I
acetone , -
2-butanone
carbondi SU 1 fide
2 hexanone
4-rrethvl-2-=ntanone
stvrene
vinvl acetate
--xvlene5 {. I l ' /
'
I J -Estunated value.
K -Actual value is known to be less than value given.
L -Actual value-is known to be greater than value given.
I U -Material was analyzed for but not detected. The nuroer is the Ninim.Jn Detection Limit. NA -Not analyzed.
1/ -Tentative identification.
~I -On NRDC List of Priority Pollutants. I N.C. Division of Health Services
DHS 3068--0 (4/86 Laboratory)
I, /
/ /
( /) I 1',,, )
ud'iJ un/ko n~/1 ""/ko
-iiii liiiil -.. .. liiii -.. -liiiill -liii1 iiiil -lliiil ---
-
SAMPLE II
?l',,,..__
Li / 7'; ,.? / ';,/
7/. .
/40,2__.</0 0 0,03S-ntYh1 ,
_,,
.,,, L ci,;:&o 7 0,/.S--·
"
?to ,;2,//0 8' aL"="
I I
,;.J
"i 6.c? ,,21< 0 ~ 33,~L
II
'Fl~ 0,:2.// IO I. S,?~ .. , -
I ,,
.,,
n-&o.:ZL/ // 2 '7. ,z,.,,,.,
' .
i'7 t;,o ,:2., 41.2-
~ e, ,,;ll/13
N.C. Division of Health Services
DHS 3068 (6/83 Laboratory)
'
DEPAR11'1ENT OF HUMAN RESOURCES -DIVISION OF HEALTH SERVICES
LABORATORY SECTION
.OCCUPATIONAL HEALTH
G C REPORT SHEET
DATE OF ANALYSIS: /(J-/(,•J76-tl,J?,/l1-/7-J'Z
rr""'--?f'"'"---:Pf>'"-J?w---pp,-,-.._
. /Ii /o;zd.,,!{1; IiDT I>D7'i J),:CWR1N'iDlJE -m.'!'-"' 771/o ,.,;
---✓.--: /, 7. r>f>n'I t), /,if Z,f),m__ 0, %1>7>n! , . ,, "
35:~lYPni
I '
0, 70cil7>1 t'J, £ ,_, __ O,,dZ~,,,,,,. 0' .2:2. nr,,, ,, I' ,, ' .
/Sf,S.--37,7,....,,,, . //
So, 97'iT»Y, I -2 . 0 7lIYrr, ,, I I
I,% 0,6/ 0. ,;:;_;;
,' I I I I .
--~~---:...-. 0, ;25:pp;,,,,. 0,/Sppm o, I $;;,,"1//1. tJ, .25 J:V1' , ' , r I "
- -. - -liiil liili -------liiiliil r,;;;;i == == == -liim DEPARTMENT OF HUMAN RESOURCES -DIVISION OF HEALTH SERVICES
LABORATORY SECTION
.OCCUPATIONAL HEALTH
G C REPORT SHEET . .
COMPANY:£(!_ )C -!J~/ 7l <!_ DATE OF ANALYSIS: //-/;J-J-'/,,,
/1~~ . C> /d7Z!~~a(!.id ,vi._.,
ft!!, vJ'7° ./3 (-' ~ ~ ) /o~//x--TOTAL Ill
.111<.d r:/; . :.. ~~ V -.:;,
SAMPLE II {U~ Q-2):J) .ZWT
/4ocJ.i/lS . -.. • I 7\ ' J /\ / ' . . -~
,VJ/ , I~ "'-V, j I •
& o;J_ </ I 7 -,--;--, /) ,r:;J,, /7, I"' -.u jJJ,) /J..L/ ,, V. '> . -,.,z.,.e -/ ... . ,
~ .. . " I,
/W h. I, , A -. . /~ . .
, j I ti • Tl , .
/40,;2_.</;CJ -V. I "U, I
/40;2'/:L/ / , .
' u I I u · I
N.C. Division of Health Services
DHS 3068 (6/83 Laboratory)
< u, I
{_), o<
,..., .--, , ._,.__ ;>
-,/ -u, / ,·J > [,.,
' ~ -~ -,,. ✓--I
/' -. -#-. --h--, -
!Vo r /'P "or/2 ~ "' ,tl,4.£ ~ d--' '
~✓-7 Z:..es-e. y:. i. o .,_ / ,Ls
/
"5 e '€. L.4 5_ ,,,v U' w; iJ,i,.--c::
6031¥,; -~ t1 31 ?£ (_
D
". ". ,ir;.r; ;uu.ru:.rn: Ulc' llUMAN RESOURCES DIVISION OF HEALTH SERVICES SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples
DThe samples described below were collected in c·onnection with the administration, enforcement, and documentation of the:
North Carolina Hazardous Waste Management Rules, 10 NCAC l0F
North Carolina Solid Waste Management Rules, 10 NCAC l0G
Comprehensive Environmental Response, Compensation and Liability Act (CERCLA)
Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, ~~-• specifically Section 11,of TSCA, 15 U.S.C. 6 2610.
Inspector's Address
1,7i • ,CJ I ✓~-7,/4-(../ ,k c:r~.c. .
Firm Address
11 /?n;,oPe:a-ry t) • .,veR-· ; irm Owner, . 0pi::ra -"'~o'-r"'-,"""'o;:::r'-'=;A"'g;::e~n7t--'---------;;:T7i':"tl:;-e-------------'--------
-
SAMPLE · COLLECTED SAMPLE TYPE ?-.1.P.'.EER DATE TIME WATER SOIL
/ s t'/2 (. /1.S'/ ;/
r--·~ P/4 e,. 12,j(
01,i;-t/i..6 ✓
,
Receipt for the sample(s) described love is hereby acknowledged:
✓~t6V/'JTI{/ .. rture-ofspector
'.c--wc ell.-,c ti
OTHER
S.-J.
DUPLICATE SAMPLES SAMPLE LOCATION OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE
✓ V" ,_,,..
v .......... V
v' ✓ V
. . Receipt/reJection of duplicate or split samples is hereby acknowledged: ~·~~ gnatureef Fi~~ Operator• or Agent
0AV/ll t4---:::: Title Title l~TS, _________________________________ _
~-~. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
u
D
Location of Sampling: Generator __ Transporter __ Treatment Facilitp
__ Storage Facility __ Disposal Facility _Landfill
~ Other: ______________________ _
Address ---------------------------------------
. --; / ,.-·/? ,/ /1,.... ' ,'7 .,,,,
CO 11 e Ct Or I s N ame _ _;c/_. --'-, ·:..''--. 01..r.-'-;,"',,,,-,:C-'':.<';.c., •:;;·'--'-/-'-,)-'-?..:,', ... c~:-'-'<'J"-:,~-!'-'';-",,____,=c..· ___ Tel e_ph one ( ;; / :; )_.:..7_",-'-'~--..:Z=,· 1..R-:..·•,_/ __
J signature
Date Sampled:___..::·'-'"'. :..l..::':7._,,_;,--:_./~5>_,,Y.'--___________ T.ilne Sampled. _________ _
Field Information
Field Sample No. 2,'f q J -
Chain of Possession:
1.
signature title inclusive dates
2.
signature title inclusive dates
3.
signature title inclusive dates
Results reported
signature title date
Instructions: Complete all applicable information including signatures, and
submit ~ith-.analysis request forms.
u
D
D
D
D
D
D
D
I
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH ·
Receipt for Samples
I The samples described below were collected in connection with the administration,
enforcement, and documentation of the:
I () North Carolina Hazardous Waste Management Rules, 10 NCAC l0F
1 () North Carolina Solid Waste Management Rules, 10 NCAC l0G
9<) Comprehensive Environmental Response, Compensation and Liability Act (CERCLA)
I () Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, ~~-• specifically
Section 11,of TSCA, 15 U.S.C. § 2610.
I /£//✓~ / ;J;, r:/1~
Inspector's Nam~· Inspector's· Address
I r ex -~_;MA;-3 ~ 2z. c.
Name of Firm / Firm Address
1 · 5'/e«ru/ · 1:/q-/lq..,-e;,,..,,_-,--· _· · ----'------1/.'-=.,:-P.'=+-. /_,_;::5-'-~=Aay.y=· "'"'~ J=---"'U="'< -~, M-1=· ::wft'-'-=c..Jz &~1..ca&-
Firm Owner, Op1e1-~7lr, . or Agent TitJ/e • .
-
SAMPLE . COLLECTED SAMPLE TYPE
I
I
I
I
NUMBER DATE ··'
3 efll/1,
4 r/u./1"
5 ~P6('11o
·{__ r/21,('Fb
-=, · i(u,/rc,
f5 r/u,(%
TIME WATER SOIL OTHER
/415 C.olW. P.
(4l.L ("""-P·
14Jo c ...... f'.
"';s-CoMT'-
1444 )(_
144,r X
.Receipt for the sample(s) described
1 above is hereby acknowledged:
~t:M""l! I (#:--Ai,/..__ Sigature of ~sp~r J ·~d,.....;.f, /
Title ?
DUPLICATE SAMPLES SAMPLE LOCATION
OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE ..
X. X X
)( ',( X
'f 'I K
r )( K ..
•.
)I' '(. X
X: ~ X
Receipt/rejection of duplicate_ or split
sis hereb owledged:
or Agent
I\...
lcoMMENTS, ____________________ ---,-_______________ _
I
·N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF.HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
D
D
Location of Sampling: Generator __ Transporter
-K_Disposal Facility
__ Treatment
__ Landfill
F ·1· D aci ity
__ Storage Facility
Other: _______________________ _
Company's Name /-C X (L/cvz-&-t<t-i q /4-,._.,, Telephone(, __ )
(/ --------
Address f'D 8,x Z...4-(q, h/r...~ 54. /4JC-.-Z.?a>L
Collector's Name Ji,.da/,,,,0 /}1,,~;./.,,,,,..._, Teleyhone( 16') 7~;? -2..,f'd/'
C1signature
Date Sampled . ? l2c/,,p b Time Sampled 1415"" ro 11-'l-'S
Type of Process Generating Waste /2 Cv/:(,,-,,t:lf«........ d-::':n::' I rq a,
V p
Field Information
Field Sample No. ?fl"/3 1/l9S Z'J}J{,
Chain
l.
3.
/<51--d-Y-6
date
Instructions: Complete all applicable information including signatures, and
submit ~ith·~nalysis request forms.
D
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I
I
I
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I
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I
n N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples n The samples described below were collected in c·onnection .. with the administration,
enforcement, and documentation of the:
North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
g· () North Carolina Solid Waste Management Rules, 10 NCAC lOG
U ~ Comprehensive Environmental Response, Compensation and Liability Act (CERCLA)
Toxic Substances Control Act (TSCA). 15· U.S.C.·§2601, et~-• specifically
Section 11,of TSCA, 15 U.S.C. § 2610.
I ~/41, /2/d~~
Inspector's ~Ame
I ('~/ /,:t£A~
Inspector's Address
Name of Firin /2~~ £,,gt
Firm Address I __
Firm _Owner, Opera,;:cr,,or Agent Title
I ..
SAMPLE · COLLECTED SAMPLE TYPE DUPLICATE SAMPLES SAMPLE LOCATION
I
I
I
I
I
NL~ER
JS
2,:;
C/'w
DATE
Rlz-t
J/;/h
f l1.
TIME WATER SOIL
)1,'-,-7 X
12:11
~
Receipt for the sample(s) described I above is hereby ackno ledged:
1 Sign ure of Ins
&.c.d-;it,I
OTrl.ER
$EI:>.
OFFERED ACCEPTED REJECTED ON-SITE OF!'-~ITE '
X )',,
X X
X 'le
Receipt/rejection
samples is hereby
~
Signature of Fi
04hr: Title
'><
X
'f
..
of duplicate or split .,. cknowledged:
Operator, or Agent
/ r"
I Title
COMMENTS, ___________________ ---c-----------'-----'-
I
·N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF.HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
D
D
Location of Sampling: Generator __ Transporter __ Treatment
__ Landfill
Facilitu
__ Storage Facility __ Disposal Facility
Other: ___________________ _;_ ____ _
Company's Name /'~0~, ;Lp,,__ &,&{'.,A ry · Telephone( ___ ~) _______ _
Address ---------..-----------------------------
Co 11 e ct or's Name /4(t{.,A/4,,, / JJ ,:e,t_,,.£./~ Tele_phone(9/ '3) 7~3--,7-,Y o 7
s'ignature
Date Sampled __ -"-~-'-½_2_6"'-'/;'---'-'}?_,?,'-'---__________ Time Sampled ________ _
Type of Process Generating·Waste._~u',,~_~,/.~a~,-,~-=A~--~~~-/'-'-,~'•~c~-~'--'c,~~~«-~'.4--'.~-~6~J~-~_.,,"------------
C/
Field Information
Field Sample No. 3 -Z(J I ,3 2 c:Q Z:. 3 Zl;J,9
title
(!,,Jvhc~--1--'
signature title 7 incl<isive dates
3.
signature title inclusive dates
Results reported
signature title date
Instructions: Complete all applicable information including signatures, and
submit_ with ·.analysis request' forms.
D
D
D
D
D
m
E
I
I
I
I
I
R
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples
D The samples described below were collected in connection with the administration,
enforcement, and documentation of the:
D () North Carolina Hazardous Waste Management Rules, 10 NCAC l0F
North Carolina Solid Waste Management· Rules, 10 NCAC l0G
Comprehensive Environmental Response,' Compensation and Liability Act (CERCLA)
Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, et~-• specifically
Section 11.of TSCA, 15 U.S.C. § 2610.
n 1/4.AAY lt:µAl>;;"/ /c.-va
Inspector's Name / n R.)( /,,UASM/-V6 ;-o,J
Name of Firm
/J, C,r(D~ s---
1 n sp e C tO r IS Address
Firm Address
n sre-~~-t: --~""'P."'1;; .... e?=---'---------=//:c:-'.'--:'P.--'-. ~&L.....<..-.::::...,c=~==·-'.J=---=/!/.c...u..~=~.:...:, ,,.:...,· ~---Firm Owner, Operator,, or Agent Title
D .
SAMPLE · COLLECTED SAMPLE TYPE
I
m
I
I
NUMBER DATE TIME WATER SOIL
) .Jul~ ,If/:,
-1-0u.r'tfl. /42Z..
. I .
5 k/2~/2, /4'!£>
I/ './2 l, .. 'Jz, i, ,.,, 7£°"
~/.
+ ··i,;z:J~ --.. K
~ ~~
I
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Receipt for the sample(s) described
OTHER
(',:,,;.. ,,
~-b. . ~--. ,.-, ..... ~n.
•
I above is hereby acknowledged:
. ~ 1.iJ.,,, <....
1 Sig ture of Ins ecto
La,.,,_,,,..._., w e/L,rt/
Title
DUPLICATE SAMPLES SAMPLE LOCATION
OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE
J( k' l(
x ',,( X'."
y X l(
V X )(
')( " )<
X -1. 'i
Receipt/rejection of duplicate or split
1 sis hereb owledged:
Owner, Operator, or Agent
vL e i fi," 4~,Wv\. Title · i I COMMENTS, ____________________ .....,.. _______________ _
' .
Location of Sampling:
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Generator __ Transporter __ Treatment
__ Storage Facility _LDisposal Facility __ Landfill
Other: -----------------------
Company's Name. _ _,_t:....:=Ca.,Xc:...._W=c.:ac,,se:...c..4.:..·;;.., "=")>-'k-,,.._'""'-.:....:·=------'Telephone (. ___ ) ________ _
Address . 1 ------r,1/.-;-~----;-. _/_7.,,_C,_,11._0 ____________ _
Collector's Name . ,41.,,(/cu{......., .o>-:J:~/s,r,,-,. Tele_phone(._ _ _,) _______ _
. -, /signature'
Date Sampled ~/4&/26 Time Sampled /"f/'S-/4,/ffS
I J
Type of Process Genera ting Waste. _ _,_;l....:...;f_~:.;r,:..:'~=-,_,=/_,_:,f-'-",0=.r..,l_ ... c_,::te,.,._· -=..!.;_,_e..c:2:.;GL...:::~.;..---------
V
Field Information
Field Sample No .3'U!f)3
ossession:
l. ~~;;Lid~, ~_J.....Y..::.=----ae~i,~-f 0 title signa
2.
title
3.
signature title inclusive dates
Results reported
signature · title date
Instructions: Complete all applicable information including signatures, and
. submit.with ·2nalysis request forms.
u
D
D
D
D
D
D
D
DIVISION OF HEALTH SERVICES
H SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples
ft1; samples described below were collected in connection with the administration, porcement, and documentation of the:
North Carolina Hazardous Waste Management Rules, 10 NCAC l0F
North Carolina Solid Waste Management Rules, 10 NCAC l0G
Comprehensive Environmental Response, Compensation and Liability Act (CERCLA)
Toxic Substances Control Act (TSCA).15 U.S.C. §2601, ~~-• specifica11y Section 11.of TSCA, 15 U.S.C. !I 2610.
Inspector's Address
lm!~ti~ ~a W~a &,.. 1 >t. c. Firm Address
• :c~ K.,....~ ....:...:KJ='§.~c ..... -·~"7'Q-.a...! ,'-----=--"--p_c._T.....;;E:..c....1-'-~-""~=~=---'-----: rm Owner, . 9p1:,ra tor, . or Agent c Title
-
AM!'LE · COLLECTED SAMPLE TYPE
~ "'UMBER DATE TIME WATER SOIL
S7 R/.z/f,n JC,:!( ✓ -
) 8' -/.I. I? 'z.7 t/
q cl,/~ V J,:;,' Yo
-
-1
-I
?.eceipt for the sample(s) described <1~ve is hereby acknowledged:
.::?/ r2 :4-((J~
::.,);!are of I.nspect):,r
--'~..,, ~ 4.e <!£._ ; s f ·
OTHER
DUPLICATE SAMPLES SAMPLE LOCATION OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE
V v .....-
~ V V'
~
~
..., .
..
Receipt/rejection of duplicate_ or split
samples is hereby acknowledged:
~ f::'. ~~ Pc 7 f{~q e .. Signature of Finn Owner, Operator, or Agent
Title 'l:le ·-:'.!-~TS-_______________________________________ _
Location of Sampling:
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGDIDIT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Generator
__ Storage Facility
_Transporter
Disposal Facility -.
_Trea0nent
__ Landfill Other: ________________________ _
Company's Name ?;,t,,/,i,,.,,4 £ ~01 ,..:;i Telephone(. ___ ) _______ _
~ddress, ____________________________________ _,, __
:ollector' s Name._,,_;S/4=-<«:'1:l:<ct.= .......... 7&=~==~-------Tele_phone(,.._ _ __,) _______ _ 0 signa;;tre
Date Sampled:..._._~p[...l./..it.2:..ll6U/,-<l,ru?,.__ _________ ..,.:Time Sampled ___________ _
,ield Information
'itld. Sai:iple No.
:b.ain of Possession:
signature title inclusive dates
signature title inclusive dates
D
D
D
D
0
D
D
D
m
signature title --:in;-=-:c::-:1;-u-s-:i:-v...,e--=d,..a_t_e_s__ I
~esul ts reported
signature title date
I.1~tructions: Complete all applicable information including signatures, and submit with-.analysis request forms.
I
I
I
I
I
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples
U The samples described below were collected in c·onnection with the administration,
enforcement, and documentation of the:
g ( ) North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
( ) North Carolina Solid Waste Management Rules, 10 NCAC lOG n (XJ Comprehensive Environmental Response, Compensation and Liability Act (CERCLA)
Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, ~~-• specifically
Section 11.of TSCA, 15 U.S.C. § 2610.
g Jt,;,t,i,, ,._()
Name of Firm
I -
SAMPLE . COLLECTED SAMPLE TYPE
I NUMBER DATE TIME WATER SOIL OTHER
AIS 7 Rl.ufn /t:, :,r ✓
IY(i g I pi,,;,,, /t;, Z-7 t/
I oL , ;.,,, l/ s q :/~,'Yo
..
I
I:
m Receipt for the sample(s) described
1above is ~ereby acknowledged: L
.,fiba,t>,M«,~, /'J-~
~./...e dl.......:sf·
Title
Inspector's Address
Firm Address
Title
DUPLICATE SAMPLES SAMPLE LOCATION
OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE
V v V
..... V ,_,.
..... -~
Receipt/rejection of duplicate or split
samples is hereby acknowledged:
~K--l~1> ft7 C1~qe
Signature of Firm Owner, Operator, or Agent
Title
lcoMMENTS, ____________________ ---,-_______________ _
N. C. DEPARTMENT OF HUMAN RESOURCES
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator __ Transporter __ Treatment
D
D
D Facility
__ Storage Facility
Other:
__ Disposal Facility __ Landfill
-------------------------
Telephone(. ___ ) _______ _ Company's Name };dr ,i,, 4 _f ~,,,.,.;., i
Address -------------------------------------
Collector's Name._.';(,./4,=~~~--~7/e-=~="==~-------Tele_phone(-_ _ _,) ________ _
0 sign~re
Date Sampled. __ ...,.£.....,/:....20."'6'---"-/,-",r_.6,._ __________ Time Sampled. _________ _
Type of Process Gene~ating Waste._....!8.:..cWe:s.::::.,;p-=~2::=cl<--4~'/a-lZ!::=wu..,1e.ao-<P..._.,~---------
Field Info:nnation
3 2. ,,
: ~2./f. Field Sample No. ,1f,$ 7
3.
signature
Results reported
signature
3'2-/~
3z..20
Ns9
title
title
inclusive dates
date
Instructions: Complete all applicable information including signatures, and
submit with·.analysis request forms.
D
D
D
D
D
D
D
D
D
D
D
D
D
D
DIVISION OF HEALTH SERVICES
I SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for SaJDples
I The samples described below were collected in connection with the administration.
enforcement, and documentation of the:
I () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
() North Carolina Solid Waste Management Rules, 10 NCAC lOG
I~ Comprehensive Environmental Response, Compensation and Liability Act (CER.C'.i...A)
I () Toxic Substances Control Act (TSCA). 15 U.S.C. §2601, et .!!:_g_,, specifically
Section 11,of TSCA, 15 U.S.C. ·Ii 2610.
I 62ove..-· .A/1cr10L.S-cJ/V
Inspector's ~imie
I W,Tr<•,<.,;fc :5,'o;,uA.r;N·.;.::,
Name of Firin
(') Ber.' 20 Cl'<./,;;;,., f M' 2. 76<
Inspector's Address
Po tscr;< 191 tui-,st.;,.,~ 1-o.~ N c 21-~1
Firm Address
I ~; .£ / p l>i~<;.:;..• -·----,--~-'------"'"a;;;-'0~17_,_)}--'½-"'~{~-•~.:::-f:.,______,Za::,C.,a:.
7
,{,"';c--,r, l:....:ri_"'~ .... <-;..::<2.....;< ____ _
Firm _0.."ller, _ 9pe:::atcr, _ or Agent T:!tle t
. -I
I
I
I
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SAMPLE · COLLECTED SAMPLE TYPE
l;to/.BEP. DATE TIME ,WATER SOIL OI'rlER
~~;..,,O
· WfJ··'?J
11kcfrf x 3£0"1 /5-SS
tuP-·'6 I I
1, /z,/sb /?.(5" -3.SO")· >< .
suP-i ,!z~ I 'iib ' :.(' 5°'0 ~--I 4 tu ✓
tvP_-1 ,; (zo {Sb ?< •",? ~:~c, (? 14 w
t,VP-1 . ti/ 2<>/f,b /4,s-->< '56"0-:+
lUP-:,. •/I'D/% )( 55',·,:;, /45:,'
Receipt for the saJDple(s) described
1 above · s, he-~eby acknowledged:
,. ·-=---
Si
I _ .. _-7'> a:y$ if. t
Title '
0E' /:;C.:, vi-N T ~-,,Jr-::-11:\l ~-\"; e.--
DUPLICATE SAMPLES SAMPLE LOCATION
OFFERED ACCEPTED REJECTED ON-SITE OU-SITE
")1j_· >f--·_",. ... >
:;-( I (-,' -.>r,
~ ><· .·!'
X )<
?<. ~
X ><
Receipt/rejection of duplicate or
saJDples is hereby ,.acknowledged:'
Cc-~---,_,;-:·\~~ . --o~"--< . •·:-. -. -=:.....:.-~--
Title ,.
~
)(_
~
)<
'f-'
y
split
or Agent
I ,~oMru::NTS, ___________________ .,... ________ __;_ ____ _
1-
---~------------------
DIVISION OF HEALTH SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH -
Chain of Custody Record
Hazardous Waste Materials
Location of Sampling: Generator Transporter __ Treatment Facility
_Storage Facility __ Disposal Facility __ Landfill
VOther: -----------------------
Address /PD Yc--c< )'ll t:Ch<o/i-<.~ L NC
Collector's Name U,,.,_____, (1 ,.t,;.~;(_ /.__ V signature/
Date ·sampled // /z,; Is,::
Telephone(t/;9 ) 946-'S I I(
·z 7 t..--t<o/
Tele_phone(9/ '7) 73,3 --2 ,"1 c / ·
0
Time Sampled __ /_£ _§"..a.5_·-_-"""f.,.1-:...;;.5...;':,;... __ _
'I )
Type of Process Gene~ating Waste_ .. /2'-'-,; ... -f""""''"":a"""-t""i-.8_·""~"",1.._.:..,u;.._•A"':C.'"'t"'"%{;"":1,'"'6"'"b:._,,..., ... _. _________ _
Field Information
p,.,,,C£dd a✓,;:t:1 ?4:-f'b <1¥'#{,1, <4J?t
--
title
2.~§(:ALU-
signature title inc1.usive dates
3.
signature title inclusive dates
Results reported
signature ...... ,. ... .. title . .... date·
Instructions: Complete all applicable information including signatures, and
submit ~ith-.analysis request forms.
i
I
I
I
I
I
I
I
I
I
I
I
DIVISION OF HEALTH SERVICES
I SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Receipt for Samples
I The samples described below were collected in connection with the administration.
enforcement, and documentation of the:
I () North Carolina Hazardous Waste Management Rules, 10 NCAC lOF
() North Carolina Solid Waste Management Rules, 10 NCAC lOG
I (,\j Comprehensive Environmental Response, Compensation and Liability Act (CERC"...A}
I ( ) Toxic Substances Control Act (TSCA).15 U.S.C. §2601, ~ ~·• specifically
Section 11.of TSCA, 15 U.S.C. 6 2610.
I Gro (/lf:_w ~-Pc{)/,fnn -'
Inspector's ~ame
lb dri ;/_oo/ I . Qc,_fc., 5 L £IC. 21-60?_
Inspector's Address
I .L t1vt"-1"---&, ,a, R.. e _sf.,· de 11 (t::_.
Name of Firm Firm Address
-I
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I
I
I-
I
SAMPLE COLLECTED SAMPLE TYPE DUPLICATE SAMPLES SAMPLE LOCATION.
m.o/.BER DATE TLl1E -~~ SOIL
, _/'
·jv"Vj rt 7½ Z,O /loo;:• 1.,/
~o_o,z_. 1 . I Jo ,:·· ;_,/ :ti/-· lo . : . .I
,'
Sig~ ure.of Ins ector
I . -,-G4/4f i$t·
Title
OT'.dER
.... ·-
OFFERED ACCEPTED REJECTED ON-SITE OFF-SITE .,
t/ .. ✓ J ..
,/ J ~.:::. :-/
-::'• -, ·-;~
Receipt/rejection of duplicate or split
samples is hereby ,.acknowledged:'
~(~'~'-
Title I ,:oMru:NTS, __________________ ...,..... ____________ _
I -
DIVISION OF HE.ALTB SERVICES
SOLID AND HAZARDOUS WASTE MANAGEMENT BRANCH
Chain of Custody Record
Hazardous Waste Materials
I ~
Lo~a:ion of Sampling: Ge:oerator __ Transporter
_Storage Facility __ Disposal Facility
__ Treatme:ot Facility~
__ La:odfill
L,/Other: a <Jlli'l .. ,luJ"p.,~ / ,f /-I! ( f -l
Company's Name ~t:?J -£:,e,df&ce-Telephone( 1/)y) . ; . . .
Address __ y......,,.-(}<-L-/-~W<::<....<.../"'-<au;'-"""'0aci_1->,J:}_.,,.cf}'-------------------
Collector Is Name &ro 11'-f., M; c/1--12--/,1,:P\
signature
Tele_phone(:9/ '7 )--"-7_:,"'3"--·-✓e..--,.,;.;.,_f-"c ... ,:,..1 _-_
Date -,Sampled;..._--"-/,,_/-f-/'----'·~::....s(!)"c;f-/--',f"--'-(,f-'."--------'----T.illle Sampled·----------
Type of Process Gene~a t i:og Was te;..._-"°&"'-'"''9·r,,,,"''"'t_..c:.,t._,.1'---fJ/4"',"'.,""_-.. -""-i"<1""{2"', .... · &.,.Jc,'l"'""'-k"'~""'u!;-._· ._,'. ....... -________ _
Field Infonnation
Field Sample No._ 3 bO J --
--
Chai:o of I
l. ' 1:itle
11 g6 I
signature s
2. l/,h1~<-I
signature title · inclusive dates
3.
signature title i:oclusive dates
Results reported
signature title __ da_te ·.
Instructions: Complete all appli~able information including signatures, and
submit ~ith-.analysis request forms.
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Appendix C
References
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1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
REFERENCES
•status Report on Groundwater conditions in Capacity Use Area No, 1
central Coastal Plain, North Carolina•, Groundwater Bulletin No. 21,
Groundwater Section, NC Department of Natural and Economic Resources,
Raleigh, NC, June 1974,
Well Construction Permits and Well records and logs associated with
the permits, NC Environmental Management Commission, NC Department
of Natural Resources and Community Development, Permit Nos.
06-0047-WC-0096, 06-0032-WC-0089, 06-0197-WC-0076, 06-0123-WS-0112,
and log of well N2ZG19.
Field notes from site inspections on 26 August 1986 and
20 November 1986.
Jeter, William; NC Groundwater Section, telephone conversation with
Grover Nicholson, NC Solid and Hazardous waste Management Branch CERCLA
Unit, 15 April 1987.
Hodges, J,S; V,P, FCX in Washington, NC, telephone conversation with
Harry Holladay, NC Solid and Hazardous waste Management Branch CERCLA
Unit, 18 July 1986.
Rainfall Frequency Atlas of the United States, Tech. Paper No. 40,
us Department of Commerce, US Government Printing Office, Washington,
DC, 1963,
Clay, Orr, and Stuart; North Carolina Atlas, University of North
Carolina Press, 1975, figures 5.15 and 5.20, pages 101 and 103.
Heath, R,C,; Basic Elements of Ground-Water Hydrology with Reference to
Conditions in North Carolina, U.S. Geological survey Water Resources
Investigations, Open-File Report 80-44, 1980.
wood, Fred; waste Management Specialist, NC Solid and Hazardous waste
Management Branch, telephone conversation with Harry Holladay, NC Solid
and Hazardous waste Management Branch CERCLA Unit, 18 August 1986,
Powers, Richard; NC Division of Environmental Management, telephone
conversation with Harry Holladay, NC Solid and Hazardous Waste
Management Branch CERCLA Unit, 23 July 1986,
Sax, N,I,; Dangerous Properties of Industrial Materials, 6th Edition,
New York, Van Nostrand Reinhold Company, 1984.
u.s. Geological survey 7.5° topographic quadrangles Washington and
Grimesland.
Alligood, cutler, and Whichard; water system owners and operators,
telephone conversations with Grover Nicholson, NC Solid and Hazardous
waste Management Branch CERCLA Unit, 22 April 1987.
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14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
Williamson, Dudley, Taylor, Dixon, Capehart, and Whitley; water systems
owners and operators, telephone conversations with Grover Nicholson, NC
Solid and Hazardous waste Management Branch CERCLA Unit, 23 April 1987.
Report WO415-Alpha, page 90, Water supply Branch, NC Department of Human
Resources, 19 September 1985.
Nicholson, Grover; NC Solid and Hazardous waste Management Branch CERCLA
Unit, memo to file, •water Supply and Population Distribution from House
Count around FCX -Washington NC D981475190", 23 April 1987.
Nicholson, Grover; NC Solid and Hazardous Waste Management Branch CERCLA
Unit, "Map Showing Surface Water Flow Path'.
Nicholson, Grover; NC Solid and Hazardous waste Management Branch CERCLA
Unit, 'Surface Water use around FCX -Washington•, 24 April 1987.
Parker, W.T.; U.S. Department of the Interior, Fish and Wildlife
Service, letter to Pat DeRosa, NC Solid and Hazardous waste Management
Branch CERCLA Unit, 21 June 1985.
Nicholson, Grover; NC Solid and Hazardous waste Management Branch CERCLA
Unit, telephone conversation with J. Stewart Hodges, v.P. FCX, Inc.,
8 May 1987.
Nicholson, Grover; NC Solid and Hazardous waste Management Branch CERCLA
Unit, Site Sketch FCX -Washington.
'Classifications and Water Quality Standards Assigned to the waters of
the Tar-Pamlico River Basin', NC Division of Environmental Management,
15 NCAC 2B .0316.
Preliminary Assessment, FCX -Washington NC D981474190, by Harry
Holladay, NC Solid and Hazardous waste Management Branch CERCLA Unit,
21 July 1986.
Purcell, C.A.; Rose and Purcell, Inc., letter to Harry Holladay, NC
Solid and Hazardous Waste Management Branch CERCLA Unit, 21 July 1986.
Purcell, C.A.; Rose and Purcell, Inc., telephone conversation with Harry
Holladay, NC Solid and Hazardous waste Management Branch CERCLA Unit,
21 July 1986.
Hodges, J.S.; V.P. FCX, letter to W.H. McCullough, 16 June 1986.
.. C.<==RC.LA
'REFERENCE /11_
STATUS REPORT ON
GROUiiDWATER CONDITIONS-IN CAPACITY USE AREA NO. 1
CENTRAL COASTAL PLAIN, NORTH CAROLINA
GROUNDYJATER BULLETIN NO. 21
GROUNDWATER SECTION
NORTH CAROLINA DEPARTMENT Of NATURAL AND ECONOMIC RESOURCES
RALEIGH, NORTH CAROLINA
JUNE 1974
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SI.Jl'il"ARY OF HYDROGEOLOGIC CONDITIONS
The hydrogeology of the Capacity Use Area has been discussed in
considerable detail in the reports mentioned previously, at least to the
extent information was available at the time the reports were prepared.
Therefore, only a brief summary is included here, based largely on these
reports.
Only a limited quantity of new hydrogeologic information has become
available since 1971, except at Ground Water Research Station No. 12
constructed near Arapahoe in Pamlico County. A diagram of this station
is shown in Figure 10.
HYDROGEOLOGIC FRAMEWORK
The Coastal Plain region is underlain by a "wedge" of sedimentary
formations ranging in age from Recent to a Cretaceous or older. These
sediments lie unconformably on a "basement" or crystalline rocks that are
similar or equivalent to the igneous and metamorphic rocks of the Piedmont
region along the western boundary of the Coastal Plain. The wedge of
sediments thickens seaward from a thin veeneer along the western boundary
to about 10,000 feet at Cape Hatteras, the easternmost land of the State.
In the Capacity Use Area, the sediments consist of sand, silt, clay,
shells, limestone and combinations of these lithologies. The thickness
ranges from about 1200 feet in the western part to more than 5,000feet in
the eastern part. The sediments may be divided into several hydrogeologic
units based primarily on differences in permeability and hydrologic
characteristics. Table 5 shows the hydrogeologic units along with the
established stratigraphic subdivisions that are based on geologic age.
The hydrogeologic units generally coincide with the stratigraphic units
35
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SYSTEM
QUATERNARY
TERTIARY
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CRETACEOUS
I I
TABLE 5. STRATIGRAPHIC AND HYDRCGEOL(X;IC I..NiTS
SERIES STRATIGRAPHIC HYDROGEOLOG IC CHARACTER
UNITS UNITS
RECENT UNDIFFERENTIATED POST-MIOCENE SAND, SLIT, SHELLS AND SOME CLAY. THIS UNIT
PLEISTOCENE UNNAMED UNIT COMPRISES THE UNCONFINED OR 11WATER-TABLE11 AQUIFER
UNIT (PM) AND INCLUDES SANDS OF THE YORKTOWN FORMATION IN
SCME LOCALITIES.
YORKT<:1t4N YORKTOWN 1'1TERBEDDED SAND ANO CLAY WITH SCME SHELL BEDS.
FORMATION UNIT CLAYS ARE GENERALLY SANDY AND CCMPRISE CONFINING
(MY) 5EDS OVER MOST OF THE AREA. THE BEDS OF SHELL AND
SA.'ID ARE CONFINED AQUIFERS EXCEPT IN Tt-E SOUTH-
MIOCENE WESTERN PART OF THE AREA.
?UI\GO RIVER PUr.GO RIVER 0 :":C:SPHATE AND QUARTZ SAND, SLIT, CLAY AND LIMESTO..Jf.
'." ORJ•'wO,T I ON UNIT PE~~EABILITY OF THE UNIT IS LOW BECAUSE OF SILT .AND
(MFR) cLAY CONTENT AND LAYERS OF OOLCMITIC LIMESTONE.
1.}t-iJT SERVES AS A CONFINING BED OVER /'-OST OF THE ARffi
t.;~y SERVE AS AN AQUIFER IN SClSE LOCALITIES.
UPPER PERMEABLE AND PORUS SHELL LIMESTONE. AN EXCELLENT
~ CASTLE ;quIFER AND THE MOST PRODUCTIVE UNIT OF THE CASTLE
HAYNE c!AYNE AQUIFER SYSTEM. t-CASTLE V, UNIT ,.. (U ECH) EUCENE 1-V-\YNE "' "' LIMESTO~ u,
'" LOWER SHELL LIMESTONE INTERBEDOED WITI-t CALCAREOUS SANDS.
" CASTLE A MODERATELY PRODUCTIVE AQUIFER, BUT LESS .j "' HAYNE PERMEABLE THAN THE UPPER CASTLE HAYNE UNIT.
~:J UNIT ,: (L ECH) 1:.
w .J FINE GLAUCONITIC SAND, SILTY /1.ND t-BEAUFORT CLAYEY IN PART. V,
PALEOCENE_ BEAUFORT 5 UNIT INCLUDES S/1.NDS OF THE UPPER PART OF THE PEEDEE
FORMATION (PB) FORMA Tl ON IN SCME LOCAL! TI ES . THE PERMEAB I LI TY
OF THE UNIT IS RELATIVELY LOW /1.NO THE UNIT IS
fl)T A HIGHLY PRODUCTIVE AQUIFER. .
PEEDEE
FORMATION
PEEDEE
BLACK CREEK UNIT
FORMATIOI< (KPD)
UPPER AND
CRETACEOUS UNDIFFERENTIATED INTERBED~ED CL/\Y, FINE S~D AND SILT lHAT FORM
CRETACEOUS A CONFIN!r.G BED BENEATH THE CASTLE HAYNE AQUIFER
TUSCALOOSA UNITS SYSTEM.
FORMATION
LOWER UNNAMED
CRETACEOUS FORMl\TION
~/1SEMENT
(FRCM 11Report on Hydrogeofogy and effects of pumping from Cai;lle !Jc.yn.e Aquifer System,
Beaufort County, North Carolina")
"
but may be a subdivision of a stratigraphic unit, or may overlap age
boundaries in some cases. Cross sections of the hydrogeolcgic system
are shown in Figures 23 and 24. This report is primarily concerned with
the Castle Hayne aquifer system and overlying hydrogeologic units.
The Castle Hayne aquifer system is the principal artesian system in
the area and the most productive in the State. It extends beneath the
Coastal area from Brunswick County to the Albemarle Sound area, and ranges
in width from 10 to 60 miles (Figure 25). Areally, the aquifer may be
divided into four groundwater basins. The natural movement of water in the
aquifer, regionally, is generally from west to east. Within the basins the
natural movement is from the upland recharge areas toward the streams,
estuaries.and sounds. Natural discharge areas include these waters and
adjacent land areas.
The Capacity Use Area includes most of the Pamlico River groundwater
basin and part of the Neuse River and Roanoke River groundwater basins.
Within this area the Castle Hayne aquifer system includes the Castle Hayne
limestone, the Beaufort formation and, in places, the upper part of the
Peedee formation as indicated in Figures 23 and 24 and Table 5 • The
Castle Hayne aquifer system has been divided into three hydrogeologic units
based on hydrologic character and permeability: The Beaufort unit, the
lower Castle Hayne unit and the upper Castle Hayne unit (Table 5).
The top of the aquifer, as shown in Figure 26, ranges from about sea
level in the western part of the area, to about 600 feet below sea level
in the eastern part. The thickness ranges from about 160 feet in the
western part of the area to more than 700 feet in the eastern part. The
transmissivity of the aquifer ranges from about 50,000 gallons per day per
37
A
50
YORKTOWN
MSL FORMATION
100 CASTLE HAYNE
LIME STONE
200 BEAUFORT
300 PEE OH.
FORMATION
400
BLACK CRf:EK
FORMATION
500
600
700
BOO
900
1000
P-22H
(',., ·--,..,..------...
\ BE~UFORT COUNTY ~
" WASHINGTOtl
0 IOrnilu '-,,,
SCALE ,.__ --
P-17 h-4
·-·:-·1~+;~,-~ :.~.-5~'~ ---.c
IIIQ:12,f,~~-~~:~-;,:~ ~: :_:,=,=:-j_~:
L
r
3 4
I
SCALE
FIGURE 23. -HYDROGEOLOGIC CROSS-SECTION A -A'
-·
Pci~NE
SURFICIAL
DEPOSITS
PUNGO RIVER
FORMATION
+50
MSL
100
200
300
400
500
600
700
BOO
900
1000
B
S-18
,-2
100 (AQUITARD)
200
CASTLE
,oo
400
,oo
600
700
800
900
1000
TO 1050
1100
1200
1300
1400
1500
1600
1700
1800
1900
2000
Q-17
h • >
YORKTOWN UNIT
PUNGO RIVER UNIT
HAYNE UPPER CASTLE
LOWER CASTLE
AQUIFER
BEAUFORT
TO BOO
P-17 0-17
h-4 i-3
P-'MLICO RIVER
HAYNE UNIT
HAYNE UNIT
UNIT
UNIT (AQUITARD)
TO
9'4
TO
700
SCALE
VERTICAL: IM. JOO'
HORJZONTIAL: IM• 2 mi
FIGURE 24.-HYDROGEOLOGIC CROSS SECTION B-B'
N-17
i-1
TO 2010
e'
M-17
•·2
TO
1966
•
100
200
,oo
400
,oo
600
700
BOO
900
1000
1100
1200
1300
1400
1500
1600
1700
1800
1900
2000
·r I I ~.
' r-----------------------..... ------,-.:...----'------------------...::"::'~:;'a..':aa'-,
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I 22 21 20 19
R
18 17 16 15 14 13
WATER USE MAP CASTL..,E HAYNE AQUIFER SYSTEM
• -•W. o-t:• TO tUI<! •>•'4 ..,..,..
$'<11[~
-..a.,ou •e< ••n• IU•~c• •HL, .-,t. "'•l •H• •ot•no
•~o .. ! "''°*" 10 .. ODVCE •oo,,, c,,n, """' •ow<• •••ft~.
NU~[-C>,JS OTH(, "'H'5 [,O$T ",~, .. ,.
12 II
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i:
.l. \' :i j
) ~:
·i
ii ! . !·;
i ;;
Ii:
'·?-¥i'i"'Efi1ff½Wiitli"'IP':fM:J't:"·i3:jt!'%ffir?Jf:txik:1i1lf'Re:"6¥~fS""Mt:!PE&l¥$1N1L~~vwR&a9:r'f.-T:P,l'i,.W¥%Z':7We:::;,,,~fyW§:{f't:c'iW@fs't~~-';l.~2w:GE?k:W~~,~
·~ . f •. fir"
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COLUMBUS
,,,, .... __ .,·
' BRUNS\
20
10 __:_: ~
• 7
N
l l
EXPLANATION
APPROXW,ATE EXTENT OF THE CASTLE HAYNE
r:::r:::::ciuMESTONE HYDROLOGIC AREA .
CONTOURS REPRESENT THE APPROXIMATE
!0"-HEIGHT IN FEET THAT WATER WILL RlS:: IN
WELLS WITH REFERENCE TO MEAN SEA LEVEL
----GROUND WATER BASIN BOUNDAR!ES
FIGURE 25,---EXTENT OF THE CJ\STl£ H.WNE AQUIFER SYSID1
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REFERENCE //2
E~~VIRO~~EKTAL M .. A ... '\AGEMENT COMXISSION
DEPAiUcfrSr OF NATURAL RESOURCES AJW COMMUNITY DEVELOPMENT
I PERMIT FOR THE C01iSTRUCT!ON OF A WElL OR WELL SYSTEM
In accordance with the provisions of Article 7, Chapter 87, North Carolina General I Statutes, and other applicable Laws, Rules and Regulations,
PE~~ISSION IS HEREBY GRANTED TO
National Spinning Company
FOR THE CONSTRUCTION OF A WELL/WELL SYSTEM located NW of the Washington Plant
I in~-~--Iieaufcrt County in accordance with the application dated 7 .January, 1982
with specfications and supporting data, all of which are filed with and' in conformity I the Department of Natural Resources and Community Development and are considered a
part of this Permit.
I This Permit is for well construction only, and does not waive any provisions or
requirements of the Water Use Act of 1967, or any other applicable laws or regulations.
Construction of a well under this Permit shall be in compliance with the North I Carolina Well Construction Regulations and Standards, and any other laws and regulations
i rtaining to well construction. I This Permit will be effective from the dace of its issuance until 12 Julv, 1982
a
n
D
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and shall be subject to other specified conditions, limitations, or exceptions as follows:
1. The 18 inches OD outer casing shall have a wall thickness of 0.375 inches and a
plain end weight of 70.59,pounds per foot; also the 8 inches ID inner casing shall
i1ave a wall thickness of 0.322 inches and a plain end weight of 28.55 pounds per
foot.
2. Notice of the name of the Drilling Contractor will be made to Bill Jeter, PO 1.507,
W.:ishington, ~C, 27889, telephone [phone] as soon as the bidS are let.
3. Notice of the pumping test will be given to Bill Jeter, PO Box 1507, Wasl1i11gton,
NC ~7889, telephone [phone], a minimum of 24 hours prior to the beginning
of the test.
l'ermit iss11ed ti1is the 12th day of January, 1982.
~ORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
I
Ji.m Mulligan, Regional Supervisor
Division of Environmental Management
By Authority of the
Env ironmcntal Management Commission
PE~'1lT NO. 06-004 7-WC-0096
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:w~·~), (;.KOL.I~,;. D[Pt,R1:~,::::1n or l<t.1UfU,L R[SOURCES f, COMMUNITY DE\'[LOf'MtN"i" \ 8cJ -3390
:JJ\'ISION or f:NV!RmJM[NTAL MA•Jt.G!.MEtH, GROUNDW/,TER SF.CTION-::ft:8
D.Q. BOX 27687 RALEIGH, N.C. 27611
DRILLH;G cor.-rnAcTOR Layne-Atlantic Co.k£G. ·No. 162 WELL coNSTRUCTlON PERMIT No.06-0047-\VC-009!
1. \<.'ELL LOCATION: (Show sketch of the location below)
Nearest Town: W:.ishin°ton N. C. county: _ _,,B'-'e~a"-'u'-'f"'o"rc.t,.-__.:O:._:...!~=='cc•~------
3rd St. Ext. (NW of Plant) /l/'Jv.,-, -/3 -=-c-c------cc--c--,-,-------,---,---,-,----,:c,---,-------Ouadrang 1 e No. __ ----1_;_..=._ __ r:._,__c...::._ __ _ (Road,Com:nunity or Subdivision and Lot No.)
National Soinning Co., Inc. 2, OWNER: ________ , ___ _:..._ __________ _ DRILLING LOG Well #8
3. ADDRESS: P. 0. Box 19], Washington, NC 27889 DEPT!l
FRO-M--TO
4. TOPOGRAPHY: draw, valley, slope, hil 1 top ~circle one)
5. USE OF WELL: Industrial OATE, 8/82 --------
6. DOES THIS WELL REPLACE AN EXISTING WELL?_~y_e_s __ _
7. TOTAL DEPT!l: -~2~4~9~'-RIG TYPE OR METHOD:_r~a~t~a~r~, .... ,_
8. FORMATION SAMPLES COLLECTED:
9. CASING: Depth Inside
Dia.
YES X NO -----
Wall thick.
or weight/ft.
type
From---±.f_to--2...Q_ft_~]~8~'-' _O~. 3~7~5~~s-~t=e=e~l __ _
10.
11.
+2 134' 8"
178' 188'
744' 24Q' GROU-tr': Dept/1
From_O_ t~ft
SCREEN: Depth
Froml34' tel64 ft ----
8"
R" Material
cement
Dia.
8"
0.322
" "
" " Method
pressure
Type & Opening
304 ss . 030
FORMATION DESCRIPTION
PleaS(;: see attached.
MINOR BASIN
BASIN CODES
HEADER ENT. G'il-1 ml.
If adoitional space is needeo, use back of form
LOCATION SKETCH
llB.'._ la1L 311 "
(Show distance to numbered roads, or other map reference points)
234' 244' 8" "
12. GRAVEL: Depth Size Material
siliceous From O t~ft No. 2
13. WATER ZONES (depth), 134 lo ] 64, l 78 lo 188,
234 to 244
14. STATIC WATER LEVEL: 28 ft.Xb!>oxl. ~op of casing --e ow
Casing is __ 3_ft. abc\·2 lar. .. ,_~!:ace ELEV:
15. YIELD {gpm): ]28 METHOD OF TESTING:_o.riiic.e
16. PUMPING WATER LEVEL: 129 ft.
after 24 hours at 128 gpr:1.
17. CHLORINATION: Type HTH Amount 50 ppm
18. WATER QUALITY: potable TEMPERATURE (0 F) __
19. PERMANENT PUMP: Date Installed. __ ~8~(~8~2~---
turbine 276 30 Type. ______ Capacity _____ (gpm)HP __ _
Make Layne & Bowler Intake Depth 135
Airline Depth_~l-9u2~--
Please see attached.
,~ -'?, '•/ . .,_
0, ,.
"/
"·'.·; ·_r '.
20. HAS THE OWl~ER BEE:~ PROVIDED A COPY OF TlllS RECORD AND INFORMED OF THE DEPARTMEt>TS Rf:OUIREMENTS AND
RECOMMENDATIONS?
21. REMARKS __________________________________________ _
I do hereby this
Regulations
was constructed in accordance with N.C. Well Construction
is well record is true and exact.
9/17/82
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O'
10'
20'
30'
60'
70'
90'
100'
110'
130'
1.40'
160'
180'
210'
240'
260'
-10'
-·20'
-30'
-60'
-70'
-90'
-100'
-110'
-130'
-140'
-160'
-180'
-210'
-240'
-260'
-280'
FOR!'\ATION LOG
National Spinning Company
Washington, Nortry_ Carolina
·well 081
May 5, 1982
Red clay and fine yellow sand
Fine yellow sand
Shell with fine sand
Shell
Soft limestone
Streak of hard limestone, soft in places
Hard limestone
Limestone and pepper sand
Limestone, shell, pepper sand
Pepper sand, little limestone
Mostly sand, some hard limestone
Sand, streaks of hard limestone
Little clay, sand, streak of limestone
Streaks of clay, sand, shell
Mostly clay, little sand and shell
Clay, little sand
0UNO W~'Tt.R SECJiOt\
GR (lA.tflGlla fl. C.
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1,..,'n•>~l<tl",..,~
fil\>"'t... ~,·
( Ytd --1---1
--+--,-+--+----4--l--,i----+-,L, 1-1-+--t-H-+-MW-i-__J
Q k,~-cJ O'i.7-W<-.-Oo 1'?
:if "B )
--1-1 I \ I I D ... . · · --1---1-J-.L K "-
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"CJ; ';T '}
"n'E t.L :::::c01::!
:~. C. 'J 7 t) l l
DRILLrnG co::,R1,CTOH L;:i,y:ic-At];.,;·:~ic Co. k1:G. :~o. l(i~ ¼T:,L co;~s-:::·n•cTrn:: Prn:•·.rT :m. Oli-00-17-WC-============-================= 0%
Nca rest To....,:: · _ _:I \.:.'o:ac:s.:.lc_l.:.i .:."cc'1' .:.l.:.Oc_ll.:..:_, _ci\_'_.:·_cc;..:.c_ ________ cou !1 t. y : _..._.:]~3~<:c:3.:.l~l~t"~o~'-" t~-~r.:.'~'--,-------3 r cl St. E:,;t. (NI\' of Plant) N ""' 0 ---,----,-------~----~,--------'c----Ouadrang Io i!o. ---~~~DS~V I t-{ Rond, Com:1:u:: i t.y o:· Suhc!ivision and Lot •;o ) 1 National Spinning Co., Jnc. 1{: \ DHl LLl :.;G LOG
3. ADDRESS: DEP'l'll
2. O...,..NER: _____________________ ~--
JJ, 0. Box 19]. 11':ishington, NC.27889
4. TOPOGR.t\PHY: C.ra1,,•,vallc:,-,slopc,hilltop(i1(circJe one)
5. USE OF V,,'ELL: Industrial DATE: __ 1_0_1_s_2 ___ _
FRO-M--TO FORMATION DESCRIPTION
Please see 3tt;ichccl.
6. DOES TlllS WELL REPI..ACE AN EXISTING WELL? No
7. TOTAL DEPTH: 245-3:' RIG TYPE OR METHOD: rotary
8. FOP-MATION SAMPLES COLLECTED: YES X NO ______ _
9. CASING: Depth Inside Wall thick. type
Di~. or weight/ft.
From + 2 to_j_Q_ft JS" 0. 375 steel
+2 l 30' 8" 0.322
.178; ~:fl;
10. DO' GROUT: ]30'-3" Depth
From 0 to 50ft 11 cement pressure --
rf aaa1t1onal space 1s needed, use oack al form 11. SCREEN: Dept.h Dia. Type & Opening
304 ss .030 LOCATION' SKETCH
From l 30'tal60'-bc'' 8','
176' JSb'-3'~,-s~,~,-.n (Shm.· distance to numbered roads, or other map rcfen~ncc points)
230, 240'-3" 8"
12. GRAVEL: Si 7.e Hnterial
,Fro:r._o_t.o 245h3 11 No.2 siliceous
13. WATER zo:eES(depcol ,_l_3_0_l_o_1_6_0_. _l_7_6_t_o_l_8_6,
230 to 240
Casing is 2 ft.. above lane su::.·face £LEV:
lS. YIELD(gpm) :~.1~2=5 ___ Ml:TH0D Of TES'!'I~lG: orifice
117. 5 lG. Pi..:!';t'ING WATER LE\'EL: _______ ~t.
1 7. CiiLORlNATIQ:;, Ty,,e HT H
1s. WATER OUALI'I",': potable
/..mo u n ·-______5il_µp_m_
'!':::!•lPERATliH.E (OF) __ _
19. l'ER:·tilNENT PLlMP: Da-::e lnstalJe,! 10/82 --~------
T Turbine YPl< ______ Capaci t:y ...2.QQ____ (gpml I\? ? ()
Mak,),a yne C~
Please see attached.
20. !it'\S -THE 0\•;1:ER BEE:.; ?ROV1DED
RECOt·4·\£!\DAT I rn:s? COi'Y 0:' THIS RECORD /'-ND lNFOR .. '-1!.::D OF 'l'rlE DEPART½l·::>TS REQUJRE:-',ENTS A!-.:D
2 l . RE;.:.,; (;,:;;s -:----:---:---:----:---.,-,-------,-----------------1. cio hcr .... by ,..,,as cons.:.ri.:cted in accorcianc;c with N.C. Well Construction Rcg1:lations th swell recorf is Lruc and exact.
I
I O' -10'
10' -20'
20' -30'
m 30' -SO'
SO' -80'
·so• -91'
I 91' -100'
100' -130'
130' -160'
I 160' -170'
170' -180'
180' -190'
I 190' -220'
220' -260'
260' -288'
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FORMATION LOG
National Spinning Company
Washington, North Carolina
Well 119'
September 10, 1982
Job //NK-OS31
Top soil, streaks of clay & fine sand
Soft white sand
Streaks of sand & shells
Shells & limestone
Soft limestone
Limestone, 87'-91' very hard
Soft pepper sand, little shell
Pepper sand, streaks of limestone & shells
Pepper sand, streaks of limestone
Streaks of hard shells, limestone with sand
Streaks of lumpy clay, fine sand, & streaks of limestone
Streaks of limestone, shells & sand
Little shells, limestone mixed with sand & clay
Streaks of sand & clay, little shells
Hostly clay, streaks of sand
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NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF NATURAL RESOURCES AND COMMUNITY DEVELOPMENT
PERMIT FOR THE CO~STRUCTION OF A WEIi OR WEIL SYSTEM
In accordance with the provisions of Article 7, Chapter 87, North Carolina General
Statutes, and other applicable Laws, Rules and Regulations,
PERMISSION IS HEREBY G)'ANTED TO
Flanders Filters, Inc;
FOR THE CONSTRUCTION OF A WELL/WELL SYSTEM located at the plant site on SR 1427
U in
and, in conformity with specfications and supporting data, all of which are filed with
Beaufort County in accordance with the application dated --------18 June 1981
the Department of Natural Resources and Community Development and are considered a 6 part of this Permit.
This Permit is for well construction only, and does not waive any provisions or R requirements of the Water Use Act of 1967, or any other applicable laws or regulations.
Construction of a well under this Permit shall be in compliance with the North D Carolina Well Construction Regulations and Standards, and any other laws and regulations.
pertaining to well construction.
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This Permit will be effective from the date of its issuance until 30 December 1981
shall be subject to other specified conditions, limitations, or exceptions as follows:
1. The eighteen (18) inches O.D. outer casing shall have a minimum plain-end
weight of 70.59 pounds/foot and wall thickness of 0.375 inches, also the
eight (8) inches I.D. inner casing shall have a minimum plain-end weight
of 28.55 pounds/foot and wall thickness of 0.322 inches.
2. Prior notice of the pumping test date must be given to Bill Jeter, P. 0.
Box 1507, Washington, NC 27889, telephone [phone], at least twenty-
four (24) hours prior to the. start of the test.
Permit issued this the 30th day of June, 1981.
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
ORIGINAL s,~;r;::o ,w
JIM MULL!Ci.:"
Jim Mulligan, Regional Supervisor
Division of Environmental Management
By Authority of the
Environmental Management Cormnission
NO. 06-0032-WC-0089
I
Straight-Screened
DlJ\GiU,E UF l·'illll'GStiJ
COKSTlluCT!ON SJ'ECIFIC.ATIONS
Ill or II Grnvcl-Puckcd Well XX
Open-End We 11
(Constructed in consolid-
ated forma~ions) .Con~tructed in unconsolida~ed formations)
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r--------------land surface ___________ _,
" A) Casing: ',:1/.··1 . -.' r,r,5:-:
t,,,.,
B)
1) Inner: X type 8" I. D 11 lbs./ft. -----'=--
(L(/~ .·
2) Outer:
200 ft. (depth) ft. (intp roe¼).·
7 r,, ~ 9 I iJt,11· <J.,:, ?>:J6-105 lbs. ft • ..-,',/-type 18" I. D .
:;20 -2B6 ft.
~
(depth)
Cement:
1) Innel" Casing: ft. to ____ .ft.
2) Outer Casing: 0 ft. to .ft .r; •.• ,mer-, .. -rr, ,,-n,.-m,7'(":r:1
-----Rock ,.
20 7 ,,,,., .. , ...
Rock c) Screen(s): type
ft.
ft.
to
to
__ I. D.
____ ft.
______ ft.
D) Gravel: ______ :t. to ______ f t. ____ --::i n.
(size)
(Fill in each blank that applies and use appropriate diagram
to show proposed construction including, but not limited to,
casing (outer and i,:,,~r), sealing .material (cement, clay,
etc.). packers, sci• "· gravel, chemical feed lines, etc.)
Location Diagram: (Previously jH'• ;•:ired maps may be submitted provided they con-
tain information r·equired in item (g} of the application}.
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il,:::i:.1c:,· \fell Cu. Rr.G. ,o.
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CIG-OCl:::2-Ii c-cJDS 7 !)RI LLIJJG CO/,"TRACTOR
l. ;.,·ELL LOCAT:o::: (Sho1,.· ske-..c:1 of the locat.ior. belo,,.-)
Slrnclbencl Subcli.vi.sion, SH J,J27 ____________________________ Quadranc;le :~a.~---'-----'---------( Road, Com.'l'lun i ty or Subdivision and Lot No. )
Fl:rnclers Fi 1 ters 2. OWNER:. _______________________ _ DRILLING WG
DEPTH J. ADDRESS c' ---'\'-V"'a"'s'-1"1-'i".1-'-1"•,_;1"-: '"~'""n'-'-__,N.,_C"''-----------
4. TOPOGRAPHY: draw,valley,slope,hilltop,__!.l~~{circle srne)
FROM ___ TO FORMATION DESCRIPTION
s. usE oF WELL: -~p_1_1b_l_1_·_c ____ oATE: _______ _
6. DOES THIS WELL REPI.ACE A~ EXISTING WELL? ______ _
7. TOTAL DEPTH: qo ,It RIG TYPE OR l-'.ETHOD: _____ _ See at 1:ached
8. FORMATION SAMPLES COLLECTED: YES NO -------'. CASING: Depth Inside Wall thick. type
Dia. or weight/ft.
to ft 6~ lit From --
LAT
JO, GROUT: Depth M.aterial Method
From to ft --
a 1 iona space is nee e use ac o 0 11. SCREEN: Depth Dia. Type & Opening
From to ft LOCATION SKETCH (Sho.,,· di6tance to numbered roada I or other map reference paint&)
12. GRAVEL: Depth Size Material
From ___ to ___ ft ___ _
13. WATER ZONES(depth) : _____________ _
14. STATIC WATER LEVEL: above . ft.belowtop of casing
Casing i6 ___ ft. above land surface ELEV:
15. YlELD(gpm) : _____ .METHOD OF TESTING: ___ _
16. PUMPING WATER LEVEL: _______ .ft.
after _____ hours at ______ gp::t.
17, CHLORl~ATION: Type ______ Amount _____ _
18. WATER OU ALI TY: ------~TE:M.PERATURE ( 0r ) __ _
19. PERMANENT PUMP: □ate Installed ________ _
Type ______ Capacity _____ (gpm)UP ___ _
Make ___________ Intake Depth~-----
Airline Depth _____ _
.-!
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\°1
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JUH '-.i 1982
D. f. !A.
20. HAS THE OWNER BEEN PROVIDED A COPY OF THIS RECORD AND INFORM.ED OF THE DEPARTMENTS REQUIREMENTS AND RECOMMENDATIONS? ves
21. REMARKS --------------------------------------1 do hereby certify that this well was consLructed in accordance with N.C. Well Construction Regulations and Standards and that this well record is true and exact.
,./·· I 7 r',..t_
OF AGENT ·-o;..Ti)
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I N. C. WELL DRILLER'S LICENSE .::1
llE,\Ti:
W[U_s --PU~PS or ALL TYPES -SERVICE
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HOME QVFICI:.
263 \.',' C.>-iATHAM S"TREET
r. 0. flOX 5'1 \•
CARY. ~•c;:n•-l CAROLINA Z.7:ll 1
PHO!'/E• ~19 -467-GIA\
CZi:;:'. 0 :-:1:d j -~'L~il(]C,.':,j
::{ ,';_Ocr':
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,~att n:/ ;11.,_.;::i'-~ .\ru:d 11.:Lt/1 .s::cf_f :-u1d ... \nr.C'
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BRANCH or,1cr:·
1532 [ISENHQW[r; on1vr:
COLUMBIA. S. C. ;;'!1203
PHONE: 803 -75A.:;:OG2
NATIONAL WATER WELL ,t,,GI.OC CERT1F'1CAT10N !ti
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1'1-'2./1 11-1 V
I
l\ORTH CAROLli\A
nJVIRONMENTAL ~\A.'iAGE~tENT CO:t}!ISSION •• I
DEPARHlE:JT OF NATURAL RESOURCES AND CO~t}!UNITY DEVELOP.'tENT
PERMIT FOR THE CO1~STRUCTION OF A WEIL OR WELL SYSTEM
In accordance with the provisions of Article 7, Chapter 87, North Carolina General
latutes, and other applicable Laws,· Rules and Regulations,
I PER.'lISSION IS HEREBY GRANffo TO
Robert L. Griffin, Sr. /1111/, P.-s~ IVNW.
FOR THE CONSTRUCTION OF A WELL/WEbb-SYSfEM located off us 264, 0.3 miles east of sR:1410 I Beaufort County•in accordance with the application dated 22 October 1979
and in conformity with specfications and supporting data, all of which are filed with
l e Department of Natural Resources and Community Development and are considered a
rt of this Permit.
I This Permit is for well construction only, and does not waive
quirements of the Water Use Act of 1967, or any other applicable
any provisions or
laws or regulations.
Construction of a well under this
lrolina Well Construction Regulations
Permit shall be in compliance with the North
and Standards, and any other laws and regulations
pertaining to well construction. 1 •his Permit will be effective from the date of its issuance until 7 May 1980
and shall be subject to other specified conditions, limitations, or exceptions as follows:
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l) Notice of the pumping test be given to Bill Jeter, P. 0. Box 1129,
Washington, NC, 27889, telephone [phone], a minimum of 24
hours prior to the beginning of the test.
Permit issued this the 7th day of November, 1979.
FOR THE NORTH CAROLI NA ENVIRONMENTAL MANAGEMENT COMM! SSI ON
ORIGINAL SIGNED BY
By JIM MULLIGAN _______ ,.,::.:.:.:;.,;;.:,:::..::.::;,,.~-~~=~=c------J IM MULLIGAN, REGIONAL SUPERVISOR
DIVISION OF ENVIRONMENTAL MANAGEMENT I Authority of the Secretary of the Department of Natural Resources and Community Development
n"RMIT NO. D6-0197-WC-0076 I
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THE CONSTRUCT!Oi'J OF A WELL OR WELL SYSTEM
U.> 7-r,{
/
P.-\HUCO I/ATER SYSTGIS, INC., (fiR. liATERCARE)
i:-OR Tiff CO~;STRUG-1-lO~l OF ,\ HELL loc~1ted at _1100 \\1est Fifth Street, h'ashington, North
Carolina, i11 13eaufort Cotinty in accorda11ce ~i.tl1 ct,e ap11licQtion dated April. 24,
1985, ~nc! i11 cor1::01:~ity witl1 specificiiti.ons and st1pporti!1g d~ta, all of wl1icl1 are
filed witl1 tl1e nep~rtnie11t of ~atural Resotirces anti Cor11n1unity D2vclopn1e11t and are
considered a pi1rc of tl1is Pe1:1nit.
This Pcnn.i.t Ls for well construction onl~·, ancl does not w.1ive any provisic-ns
or re:q_uirer:,ents or the 1..1::t:er Use ..-\ct of .L967, or any other .;:ppl . .i.c;1ble laws or-
regu.lations.
Construction of a well under this Permit shaL.L be i.n ,::onpl.L1.nce \•::ith the
\ortl1 Caroliiln Well Co11structi.on Regulations and Standards, Hnd ~ny otl1er la~s anc!
regtilations pertai11in~ to wel.1_ construction.
"'
This Permit will be effecti_ve from the date of its issuance. until Octobe.:-25,
1985, and shall be subject to other specified con<liti.ons, limitations, or exceptions
as follows:
l. h1.citer s2mples, from each production well, shall he:. collected and analyzed for chlor·i.cle content at the time of compl.etion of the new four inch ,,,,,ell. The older six inch well sl1all be sampled every six (6) months thereafter.
? If a11al,·ses of ti1e six i11cl1 well show an incrense of chlorides, or the wel.l becomes i.nsuf: ficient: for any reason, the we 1.1 shal L be abandoned as pc r ,JC:..\C 7.C . 0113.
Permit issued this the 25th clay of ,\pril, 1985.
PERHIT NO.
:/ORTH CAROLrnA ENVIRO>::'.E>lTAL :!ANAGE>!E:!T co:•!MISSTON
<.
Jim r
Div.· ·011 of Environme
By , thority of the
. upervisor
al Management
Environmental Management Commission
06-0123-\-!S-0112
I No,nH CAROLINA DEPARTMENT or NATURAL REsouRcEs & coMMui<1TY oevELoPMENT,6,o 3:, 7 G 3 WELL REf_OCD· , . : DIVISION Of ENVIRONMENTAL MANAGEMENT /V _ 0 j :lJ •W5aO/ j: .:,:.:,,:','·'· , . P,O,Bo,27687 -RALEIGH,N.C.27611 919-733·2020·· VU, ,: •.••. ~--.I -. / .· . 0"' LLING CON7R,\C1'0R; .<l.. I) /GI ~t G. NO. W£.LL CONSTRUCTION.PERMIT NO.
DRILLING L0C
' . FORMATION OESCRIPTIOfl
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.... - - --.. l!!!!!!!!I Ill!! I!!!!!! 1!!!11!!1 -lliilil 'lilli1, -~---,-// LOG ,\iELL fOR WASHINGTON ( CI'l'Y UF) HY LAYNE .LAN'!' IC
July 31, 1940, Located at Washington, N. C. Drilled
---') Formations and DeJ:!th of Well . DfJ'TII\ Ft.-7/ffCKNE!iS Dr J,..f/'/E:R. I<, t.
10 10 Surface sand and clay
20 10 Sand and shell
30 10 Soft limestone
40 10 H11 rd limes tone
42 2 Shell rock
81 41 Hard Shell rock
96 14 Hard limestone-Very hard
135 39 Black sand
163 28 Layers of Limestone & White sand
170 7 Shell rock and clay
180 10 Shell, rock & clay in layers
190 10 Shell, clay in layer
204 14 ;:;heJl rock and white sand
217 13 Shell rock and white sand
227 10 Clay and shell rock
249 22 Shell rock Sandy clay
294 45 Clay shells-Sandy
400 108 Blue clay
Reamed 18" hole to 1731
COMP,lNY, NORFOLK-';'., VIRIIIINIA ··
Dimensions of Casing & Screen
Ca.sings Ft. In.
Ft. In.
31 6
60 0
70
115
120
125
135
150
160
Screen or Casing
Ft'-·In· •.
· 31 6
60 0 Pipe
10 Screen
45 Pipe
5 Screen
5 iliei~i&l
10 Screen
15 Pipe
10 Screen
~
In.
18
10
10
10
10
10"
8"
8"
8"
Everdur
to 8"
Set new pump Sept. 21, 1940 with old motor Test 550 gpm(Ambrose) Oct. 11 -Al set new motor on pump. Oct. 25.
City started pump to service new motor. October 28-Test 500 gpm #19 pressure above ground.
Well Data:
Date Tested: 9/4/40 -Static level 9 1 Production: 350gpm PL:60 Permanent Test 500 Gals. 110' PS
Pump Data:
Shop No. 10303 'rype Lubr. Soelnoid 22U volt: Type Head TF618 Size Suction 6". Depth Setting: 100
Size column 6 x 1-3/16 x 2. Length Suction 10' with 6" Strainer. Type Bowel 8" KHC. No. Stages 11.
Capacity and Head: 500?. Pressure 19#.
!.!otor Data:
Horsepower 30: Voltage 22: RPIJ: 1750 Phase 3: Type CFU: Cycles: 60; Make: US; Frame No. 917.
Drilled second well in 1942 because first one did not produce 500gpm as was guaranteed. Yield dropped to 250.
2nd well abandoned; I too much iron.
~~~t:~;~~;,:~~t''~~h~:~-:Ji.r_,· --t~ ~~,~· .. . -...
-~~~-i:"~~zt;._ i~f{~:-·
·_;,::"--~~=~· ... -----------'-'~=;".,··-~•-c:;;-C:· .;-,;;.-2-·:.-~::.-~::a:s=====--..1-"'
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Pro~erty of /~t:. Dw 4:af'd . .L..r. .
~ ~cJ(Lid<~) ·
Address JJo &y :u>V ··
Telephone 733
' .
Fe;.. X -tAJ P..,O I,,_ I /t 'j br-· :: ..
't'o I 4~.S-, 9 $'.Z.
This Book is manufactured of a High Grade·.·
50% Rag Paper having a Water Resisting Surfr::e,
anj is sewed with Nylon Wata~;:iroof Trre1d.--.
·=. s"'"'-~h" '"'°' ,±'(;'•J:"~""Tf~ ., -"'"'-,.·, •a · ~1-,_;;;ri~;a:;r~
INDEX
·-•. -_,--.:.__:_:_ ___ 2-...:_ ______ _
.-
------·----------
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ct).,_(;(/~
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--,u,,;;-y, 7/--Jc-S p--d------------,------o---; -,. --
._,---,--;--,--------)J, ~:r'!I -
f;, · ;'1·/ 07/?° -
-u,.f. /,6/.
--:;:_,p G7--114vg--_::---;1----1A.:.'7JJ-----
..-z=,,t :2:1•/·.-'J-;>;);_ ;.,-:)-,~---I -J·J-y7q_ ----------·~;.f?·•••,7/t( _)"~
;
------------------------------------------------------.. ----------
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REFERENCE //4
April 15, 1987
To: file
From: Grover Nicholson f-----/J"J-/-
Re: FCX-Washington
A telecon with Bill Jeter (733-3221), former regional
hydrogeologist with the NC Division of Environmental Management and
currently hydrogeologist with the central office of the same division,
supplied the following information.
1. The Castle Hayne aquifer is the primary water supply
source for the area around the site. The aquifer is relatively
shallow, generally about 30 feet below land surface, and is overlain by
the i'1iocene Yorktown aquifer and the Post-Miocene surficial aquifer.
The Pungo River aquitard, which separates the Yorktown and Castle Hayne
aquifers further to the east, is missing in the area of the site.
Z. In the area of the site the water level in the Castle
Hayne aquifer if typically 5 to lU feet below the surface, or
approximately at the level of mean sea level.
3. The production wells used by National Spinning cause
localized cones of depression (lowering the water level) when pumping.
4. The Castle Hayne aquifer is "leaking" in the area of the
site. Groundwater in the aquifer moves to and from the overlying
formations.
GN/pw/0384b
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To:
From:
Re:
REFERENCE // 5
July 18, 1986
File
Grover Nicholson q. ,,..,_ µd. /-
FCX-Washington
In telecon J. Stewart Hodges, V,P. of FCX, explained the
following to Harry Holladay, NC SHWMB, CERCLA Unit.
1, A trench about 12' x 250' was dug on the FCX property and
paper and plastic bags and jugs of pesticides, herbicides, and tobacco
sucker control chemical (MIi 30) were buried there.
2. The trench was dug to the water table, about 10 to 12 feet
deep, and then backfilled with 2 to 3 feet of soil before the chemicals
were put in.
3. The disposal occurred about 15 years ago, in the early
1~71.)'s.
4. FCX owns about 8 acres of property at the site.
5, The buildings on-site are being cleaned in preparation for
the new owner. GSX is designing an investigation plan for the trench
disposal area.
6. The new owner is Fred Webb of Greenville, N.C.
7. National Spinning Company has four production wells around
the site. A domestic well about 60 feet deep is about 200 feet north
of the warehouse near the road.
8. Methoxychlor was used for seed treating until 1954. No
mercury compounds were used.
GN/pw/0384b
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NORTH CAROLINA V
tHF t/PtVEE'.:S✓-?">' OF NC ,l'l!E$$_,
(!HAPe-1. }fl✓,t.t.,, ,C,G > Fl&.lMl£
5,/5" pA~6 /()/ ,1,u-r, Ft~P.1!£
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Figure 5.2. Average January Temperatures in N.C.
Degrees Fahrenheit
48and above
46-48
44-46
): ::·~ 42-44
t(1\~ 40-42
~f 36-40
'Y below36
Source: U.S. Department of Commerce, Weather and Climate in North Carolina, t972.
Figure 5.9. Average July Temperature in N.C.
Degrees Fahrenheit
,:'-1'! 80 and above
Ji~!: 78-80
76-78.
72-76
68-72
belo~68
Source: U.S. Department of Commerce, Weather and Climate in Norr ti Carolina, 1972.
Page 94
Page 98
From: North Carolina Atlas, The University
of North Carolina Press, Chapel Hill, N.C.
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Figure 5.15. Avcrnge A~nual Precipitation in N.C.
Number of Inches
BO and above
,. 72-80
64-72
~'. ;:-;, 56-64
52-56---
48-52
44-48
below 44 Page 101
Source: U.S. Department of Commerce, Weather and Climate in North Carolina, 1972.
Figure 5.20. MoOn Annual Evaporotion in N.C .
Number of Inches
42and above
,, s'.,! 34-36
32-34
below32 Page 103
---~----_______ _J
Figure 5.21. Prevailing Winds and Mean Annual
Wind Speed in N,C.
NE
Source: U.S. Department of Commerce, Climatic Summary of the
U.S., 1972.
1 Source: U.S. Department of Commerce, Climatic Sum_mary of the
U.S., 1972.
Note: Wind speeds are noted in miles per hour.
Page 104
I L_ __ _
From: North Carolina Atlas, The Universit'y
of North Carolina Pres·s, Chapel Hill, N, C.
Figure 5.26. Emissions of Pollutants per Square Mile by N.C. Air Quality Control Regions, 1970
Tans per Mile Type of Pollutants
Page 108
Source: N.C, Department of Natural and Economic ResoUrces, The North Carolina Plan lot Implementing National Air
· Oua/iry Standards, 1970.
---------------
From: North Carolina Atlas, The University
of North Carolin& Press, Chapel Hill; -N. C.
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REFERENCE //8
0cal§rac [E~cemeu1rn of
4~ . R \'\ fJ.. f ~-P.~ TI , fl , ' '111D~(O)tUJ[:1(ru= w\1 crutICE:tr LI. dy'((]u~Odogy. .
iw~ri, ~lefren~en(Ce to ~lLon1cdmtaot11§
Nort!-n Carolina · · 0
BD1
~~Ll~.;~:~£:~~~l~C.:i:..'-:-~#.1.f ... 'l\='c~~~~ .. _:£·•·~_;;:;;~'f.r_~..;....iA-~;._~~ .. ~8:--&.\"..:,~.;J~~-:t"w~;":<Y,~~~~
lJ,§. GEOLOG!CAl SURVEY
V/ATER RESOURCES INVESTIGATIONS
O?l:N-fllE REPORT 80-44
Prepared in cooperation with the
North Carolina Department of Natural
Resources and Community Development
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UNITED STATES
DEPARTMENT OFTHE INTERIOR
GEOLOGICAL SURVEY
Basic Elements of Ground-Water Hydrology
With Reference to Conditions in North Carolina
By Ralph C. Heath
U.S. Geological Survey
Water-Resources Investigations
Open-File Report 80-44
Prepared in cooperation with the
North Carolina Department of Natural
Resources and Community Development
Raleigh, North Carolina
1980
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Rock Units and Aquifers
in the Coastal Plain
The Coastal Plain of North Carnlina is underlain by sedimentary · rocks that v,ere
deposited .in water in several different. layers
which geologists refer to as formations.
Formations are commonly given names for places near which they are exposed at the land
surface, for ease in re'.erring to _them in . ,· geologic literature. . ::. Rock layers are normally given names by
geologists if they have a distinct composition
or, if of variable composition, include materials
deposited during a particular segment of geologic time. Named rock units may or may
not coincide with hydrologic units so that in
ground-water reports some aquifers may be
referred to by the formal geologic names used by geologists, such as the Castle Hayne
Limestone and Yorktown Formation, and
others may be given more informal names,
such as the "Upper aquifer", "Surficial aquifer"· or "post-Miocene deposits." The name
"Surficial aquifer" indicates the aquifer in any
area that is closest to land surface and thus is clearly identifiable, regardless of any other
. names that may have been assigned to that
rock unit.
Non-geologists concerned both with ground-. water problems and with ground-water studies in the Coastal Plain are probably· con-
fused by the different named applied to t'he different hydrologic units. The following chart
was prepared in an effort to elimina_te some of
this confusion. We should note, however, that in
preparing the chart we have neither tried to include all formation names nor been overly
concerned with the relative geologic age of the formations. The names used in the last two
columns can be confusing to the extent that all
units are referred to as "aquifers." Confining
beds composed of clay occur in all of the formations and in the formations of Cretaceous
age clay comprises about half of the total thickness.
The two most important aquifers in the Coastal Plain are the upper aquifer and the
limestone aquifer. Recharge of the ground-
water system is from precipitation on the land surface. Therefore, the surficial aquifer has the largest yield in terms of rate per unit area (for
example, gallons per minute per square mile).
The upper aquifer is also most subject to pollution from land-su.rface waste dispo'sa/. The limestone aquifer is the most productive aquifer
in North Carolina in terms of yields of individual
wells. Wells capable of yielding more than 1000
gal/min can readily be developed in this aquifer.
. Geologic Formation 6r geologic Names used in some -Sirnpliest useful all:e · name. ground-water reoorts hvdrologic names
Pleistocene Pleistocene deposits Post-Miocene
Croatan Formation· deposits
Pliocene Yorktown Formation Upper_ aquifer
Miocene Pungo River Formation Yorktown
aquifer
Belgrade Formation
Oligocene River Bend. Formation Castle Hayne aquifer Limestone aquifer' Eocene Castle Hayne Limestone
Paleocene Beaufort Formation Beaufort aquifer
Peedee Formation Lo1-1er aquifer Cretaceous Black Creek Formation Cretaceous aquifer
. 11 Tuscaloosa ri Formation
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The complex interlaying of the ·sediments
underlying the Coastal Plain is shown in the
following cross section. It will also be observed
from the cross section.that the rock layers (and
L
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,ooo·
CJ So"d
formations) underlying the Coastal Plain dip
toward the coast at a rate of about 15 ft./mi. As a
· result, each formation occurs at a greater depth
below land suriace toward the coast. ·
(l;,LANATION
[E:'JSill
23
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0 10 20 lO KILOl.t(T(RS
v,nicol u0q~uo1io11 X 66
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1929 -= -
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6 = =
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of
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'-Ground-V✓ ate r Situation
ln the Coastal Plain
·. Stream
Recharge ore a
~ASTLE HAYNE AQUIFER
~ Sand Ld \~-j Cloy
Recharge of the ground-water system in the Coastal Plain occurs in the "upland" areas above the flood plains of perennial streams . Water reaching the saturated zone moves downward and laterally through the system to discharge areas.
Ground-water discharge occurs by seepage
through the bottoms and sides of streams and drainage ditches and also through evaporation froni the top of the capillary fringe in flood plains .and other areas in wt,ich the water table is within several feet of the land surface During the growing season, ground water is also us.ed by plants whose roots reach the capillary fringe or saturated zone. In the area adjacent to the coast, ground·water also discharges by seepage into the sides and bottoms of estuaries and the ocean. · The presence of clay layers in the Coastal Plain formations hampers recharge to the deeper aquifers, so that most of the recharge tends to move laterally to discharge areas through the shallowest aquifers. Recharge to
24
j~r;,""'~( Shells ~ Limestone
the deepest aquifers occurs only in the central part of the interstream recharge areas. This is an important point relative to waste disposal, in that if pollution of the deeper aquifers is to be avoided, waste disposal sites should be located as close as possible to perennial streams.
Prior to the construction of drainage ditches into the central part of the interstream areas, the water table reached the land surface in these areas during the fall, winter, and early spring recharge season. As a result, water was ponded on the surface· for periods of several months each year in high-level swamps referred to as pocosins. ·
Two region·a1 aspects of the Coastal Plain are of primary importance from the standpoint of ground-water occurrence and availability. The first is the nature of the surficial materials, which controls the recharge to the ground-water system. The second is the geologic con-ditions that control the occurrence of aquifers and confining beds.
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The materials forming the surface of the
Coastal Plain can usefully be divided into
sandy and clayey soil_s on the basis of their
effect on ground-water recharge. Recharge in
the areas underlain by _sandy soils is much
more effective than in the areas underlain by
clayey soils. One of the consequences of this is
a much larger sustained base flow of streams in
these areas.
The geologic conditions in the area of about
Hydrologlc Geohydrologic
area characlerisl!cs
Sand Hills Productive water-bearing sand
at the land surface and over-
lying, for the most part, much
less-productive material.
Outer Banks Productive water-bearing sand
at the land surface containing
fresh water in contact with
sea water.
Castle Hayne Productive limestone overlain
Umestone and underlain by less-productive
sanq interbedded with clay.
Central Numerous thin layers of water-
Coastal bearing sand complexly interbedded
Plain with clay.
SOILS
-
25,000 mi' occupied by the Coastal Plain
differ significantly from one part of the region
to another. These differences affect both the
occurrence and the availability of ground
water. As an aid to understanding the Coastal
Plain ground-water system, it is useful to divide
the region into four hydrologic areas.
Information on these is summarized in the
following table in which the areas are listed in
order from !he simpliest to the mos.t complex.
Yield of the most
productive WE'l1s Remarks
(gal/min)
50-250 Water obtained from both bored wells
and from screened drilled and driven
wells. Water only slightly mineralized. ~
25-100 Water obtained from both shallow,
vertical, screened wells, and !ram
horizontal collectors. Fresh-water
zone subject to salt-water encroach-
ment both from above and ·below.
more than Drilled open-hole wells. Water
1000 moderately hard. Aquifer is confined
and large wilhdrawals affect a large area.
250-1000 Sediments of Cretaceous age comprise
most productive zones and is
tapped by multiple-Screened drilled
wells. Waler of excellent quality
and, in places, naturally softened.
Surflcia1 sand aquifer also widely
used for domestic supplies.
.
HYDROLOG.IC AREAS
25
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HYDRAULIC CONDUCTIVITY AND TRANSMISSIVITY VALUES
FOR TYPICAL NORTH CAROLINA ROCKS AND AQUIFERS
Hydraulic Conductivity of Selected Rocks
Material
Cea rse sand ...................... .
Medium sand ..................... . Silt ............................... .
Clay .............................. .
Limestone (Castle Hayne) ......... . Saprolite ..........•...............•
Granite and gneiss .............•••.
Slate ............................. .
Hydraulic conductivity {rounded values)
(IVday) [(gal/day)/11'] (melon/day)
200
130
1
0.001
300
5
5
3
1500
1000
5
0.01
2000
50
50
25
60
40
0.2
0.0004
80
2
2
1
-z. +.OC, )( 10 -z.. 1-,G"I ;,< 10 -4
3.53 )( ,o_:+-
3,53 )( 10
I .O~ >( 10 -I
1,T~ >< 10-.3
l,':\T X IC-"3
\,Db I( 10~
Hydraulic conductivity replaces the term "field coefficient of permeability" and should be used when referring to the water-transmitting characteristic of material in quantitative terms. It is still permissible to refer in qualitative terms to "permeable" and "impermeable" material.
Average Values of Hydraulic Conductivity, Thickness, and Tranamlsalvlty
for Selected Aquifers In North Caroline
Hydreullc Conductivity Thlckneu Tren,ml11lvlty Aquifer C"' /,-, EC:., (11./day) (II.) (111./day)
' Post-Yorktown deposits -z. 50 20 1000 1 . .--;t -/ 10 -'t.
Yorktown Formation i,l '1 )( 10 50 40 2000 Castle Hayne Limestone · I ,Db )( ID-1 300 100 30000 Cretaceous deposits + .DI, X ll>-3 20 200 4000 -3 Saprolite / , '!-'I J< ID 5 50 250 Granite and gneiss -3 5 200 1000 /,7-'lxto
Transmissivity replaces the term "coefficient of transmissibility" because, by convention, an aquifer · is transmissive and the water in it is transmissible.
(from Heath, R. C., 1980, Basic elements of ground-water hydrology with reference to conditions in North Carolina; U.S. Geological Survey Water-Resources Investigations Report 80~44)
HYDR,:\l)t.-1 C.... Co"-J"DUC...7'1l/1,Y
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)( ?o.s CM /rr =-GM
DI\ ·1 864= e, E.,;. /D ft )' .:5 EC.
oR.
FT -4 N 3.53 K ro N C /'/l
DAY .:sec..
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TO:
FROM:
RE:
File
Harry P. Holladay
FCX -Washington
NCD981475932
REFERENCE //9
18 August 1986
Mr. Fred Wood, Greenville Waste Management Specialist, called to relay
the following information:
HH/w/pc
The contractor that made the burial for FCX is Bonnie Singleton
[(919) 946-32~7].
Singleton remembers lots of bags being buried, but thinks there
were no drums.
The earth work for the burial was 'done 10 -15 years ago. There
may be two burial trenches.
Singleton implies that he knows an ex-FCX employee that may have
information.
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FROM:
RE:
File
Harry P. Holladay
FCX Washington
NC D981475932
REFERENCE // 10
23 July 1986
Mr. Richard Powers, ·NRCD [phone], was called and trace solvents
indicated in the groundwater report from Rose and Purcell were discussed.
HH/tb/0193b
A shallow water sample can be taken with a well point in a hand
augered hole. NRCD has the equipment and wants to sample.
Area residential groundwater wells exist but they have largely
converted to city water.
The Washington Water System serves about 9350 people and has
intakes upstream from the FCX site. One intake is about 0.75 miles
west of FCX near SR 1567 and Tranters Creek. The other intake is
about five miles NW near us 264 and Tranters Creek.
National Spinning wells draw about 1.5 mgd for process use.
However, contamination of water would be of concern to them.
National Spinning is close to FCX.
Lithologic data for the area will be sent.
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To:
From:
Re:
REFERENCE // 13
April 22, 1987
File
Grover Nicholson 71',,.._... ,(/~./....__
Teleeons with water systems owners/operators near
FCX-Washington
I talked with Ms. Alligood, owner of Ash-Ma-Tau Mobile Home
Park. She gave me directions to the park and I plotted it on the topo
map. It is about 4 3/4 miles east of the site. The park has two wells
which serve 42 mobile homes.
I talked with Jerry Cutler, manager of the City of Washington's
water system. The city has two surface water intakes, one at Tranters
Creek and US 264 about 7 miles northwest of the site and one at
Tranters Creek and SR 1403 about 8 tenths of a mile west of the site.
Both intakes are plotted on the topographic map and are upstream of the
site. The water system also uses an existing well at the Slatestone
water plant on SR 1507 about 3 3/4 miles east of the site. The well is
10 inches in diameter and 184 feet deep. Water from this well is
mixed, after treatment, with the surface water in the distribution
system. A new well is being constructed on the water plant site. It
will be 20 inches in diameter and 185 feet deep. Sixteen inch diameter
easting will extend from the surface to 100 feet and the well will be
open-hole from 100 to 185 feet. After the new well is operational, the
old well will be abandoned. Mr. Cutler knows of no other surface water
intake in the area.
I talked with Billy Whichard, part owner of Whichard Beach
Water System. The other owner, Warren Whichard [phone], was not
contacted. The company operates two wells at Whichard Beach about
4 3/4 miles southeast of the site and three to four wells at Portside
Shores about 4 miles southeast of the site.
GN/ pw/U384b
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To:
From:
Re:
REFERENCE // 14
April 23, 1987
File
Grover Nicholson q.,,..._._ )..J~~/ r---
Telecons with water system owners/operators in the vicinity of
FCX-Washington.
I spoke with Charles Williamson, Mayor of Chocowinity, about
the water supply for Chocowinity. The town has two wells, one inside
and one just outside the town limits. Both wells are about 250 feet
deep and completed into the Castle Hayne aquifer. The wells are
plotted on the topo map and are 3.5 to 3.75 miles south of the site.
About 99% of the residents within the town limits use water from this
two-well system. The system has 350 meters and serves also Singer
Furniture Company (1 meter, 600 workers), the high school (1 meter, 800
students), and the elementary school (1 meter, 250-300 students).
People not using the town's water system use private wells. Older
wells are generally shallow and use a water softener. Newer wells are
usually deeper and completed into the Castle Hayne aquifer.
I spoke with Margaret Dudley, secretary to H. Williamson, Jr.,
owner of the Mimosa Mobile Manor. The park has two wells, only one of
which is used, which serve 88 mobile homes. The park is plotted on the
topographic map and lies 4.5 miles south-southeast of the site off NC
32.
I spoke with Keen Taylor, owner of Southern Pines Mobile Home
Park. The park is plotted on the topographic map and is about 3.75
miles northeast of the site. The park has three wells, all 180 to 200
feet deep, which serve 25 people.
I spoke with Ms. Dixon, owner of Trails End Mobile Home Park.
The park is plotted on the topographic map and lies three miles
northwest of the site, just off US 264. There are two wells at the
park which supply 49 mobile homes (about 150 people).
I spoke with Tony A. Copeland, V.P. of Operations for Flanders
Filters [phone]. Shad Bend Subdivision is owned(?) by Flanders
Filters and is supplied with water by them. Three wells, located on
the Flanders Filters property, supply 12 to 14 houses. Waters from all
three wells are mixed together before distribution. Shad Bend
Subdivision and Flanders Filters are about 2 1/2 miles northwest of the
site.
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I spoke with kobert Whitley, the owner of the kiver Road
Estates and Whitley Mobile Home Park. River Road Estates is located
about 5 1/2 miles southeast of the site along NC32. It has two wells,
both 57 feet deep, serving 115 people. Whitley Mobile Home Park is
located along NC 32 near Sevens Point about 7 miles from the site. It
has two wells, both 100 feet deep, serving 90 people.
I spoke with Robert McRay, a resident of Washington Park,
(919) ~46-1033 Ext. 221. He said that the residents of Washington Park
were supplied with water from individual private wells and not from
Washington's water system or another community system.
CN/pw/0384b
.. 1111 ---•
RE?ORT ~ATE 0~/1?/SS
?•,,JS N .AME PW ID
ASH-MA-TAU-1'.HP 0407101
AURORA TO:..IN Of C407~20
BATH TOW~ Of 0407030
3AYVIE'.J WAT ER WORKS 0407102
3ELHAVEN '..JAT ER DEPT 0407015
CHOCOWINITY TOWN OF 0407025
FLANDERS FILTERS 0407441
HILLS POINT SU3S IVISION 0407112
MIMOSA M03ILE MA NOR 0407401
OLD FORT M09iLE COURT 0407107
PAMLICO PLANTATION 0407117
PORTSIDE MH RETR:E.A.T 0407114
SOUTHERN PINES MHP 0407464
SPENCERS REST HOME 0407415
TRAILS END ;""H? 0407109
'ffASHir~GTON \ol ATER SYSTE,Y. 0407010
wH!CHAROS 3EACH I NC, 0407110
WHITLEY'S :O:HP 0407111
COUNTY =07 NU:'13ER OF RECOR OS
-- --- ----
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"REPORT ~0415-~LPH.A (WANG)
OHR -ENVI~JN~ENTAL HEALTri SECTION -WATE~ SUPPLY 3RANCH
ALPH~~ET:CAL ~!THIN COUNTY LISTING OF ACTIVE COMrUN!TY P~S
RES NAME ADDRESS CITY
,"IAYHUGH .ALLIGOOD OR RT 4 90X 92 WASHINGTON
rt E ~A _q E ESE °' ~GR OQ 30X 86 AURORA.
"' -CARSC!l OR ~GR PO BOX 6 BATH
DIC IE s RESP=ss OR M RT 2 3ELHAVEN
DANIEL G ADAMS OR :-':G PQ 60X 220 2ELHAVEN
J Ef F H.ADOCK OR ,%R PO 30X 145 C~OCOW_I_NIT_Y
MIC11.AEL EOY D Oil CURR_ p C BOX 1706 '.JASHINGTON
:,in, F HOLLIS ROUTE 2 sex 284 3LOUNTS CREE
HARVEY WILLIAMSON JR RT 5 30X 139 -.. i,.!ASHI~GTCN
ZENO M EVERETTE OR M RT 1 30X 34 8 VANC(sii"RO.
T03Y WOOLARD OR ~GR PO BOX 1167 JACKSONVILLE
WARREN WH!CHA_RD OR M PO __ BOX_ 7_46 CH OCO~!N II_Y
KEEN TAYL0, OR MGR SOUTHERN FINES Mi-IP ~ASHINGTON
ED',AsD SPENCER OR :-,:; PO SOX 62 PANHGO
HARVEY DIXON JR OR M 211 ~-MA IN ST. SASHINGTON
JE>RY ClJTLER OR MGR PO 30X 1988 wASH!NGfON
i,,1ARR EN WHICHASO OR M PO BOX 746 CHOCOWINITY
i-:03ERT ~HIT LEY OR MG RT 2 aox 74 WASH ING TON
1 8 TOTAL POPULATION = 15,937
ll P
27339
27306
27308
27510
27810
2?817
278e'I
2 7 :14
2 758 ;i
28596
28546
27817
279e9
27860
2786;1
27889
27 817
27389
- -- --
:..0415.AL.: PAGE 90
T A PCP.SRV s PHONE
------
C A 1 2 6 G 919-946-B570
C A 750 G 919-322-4011
C A 27 5 G ?19-_9_23~6471
C A 400 G 919-964-4911.
C A 2,475 G 919-943-2241
C A 1 ,_1_2_2 _ -G 919-946-65_68
C A 300 G 919-946-8081
C A 130 G 919-946-6236
C A 240 G 919-946-4115
C A 64 G 91 <i~zi.f-0991
C A 56 G 919-353-7000
C A 1 5 Q_ . G J.1""-:-9_4_6_:_42 75
C A 90 G 919-946-0014
C A 25 G 919-943-3533 :·.)
C A 147 G 919-946-5069
C A •19,35if ... s 91-9-946-f033 " C A 150 G ,19-946-4275
C A 210 G 919-946-5372
TO: File
FROM: Grover Nicholson
RE: Water Supply and
FCX -Washington
No. houses served by
private wells (from
house count)
No. people served
by private wells
REFERENCE // 16
23 April 1987
tj,-A-1rd/-
Population Distribution from House count Around
NC D981475932
Within 1 Between 1 and Between 2 and
mile of site 2 miles of site 3 miles of site
402 and 69
38 241 south of river
144 916 1528
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(houses x 3.8 persons/home) ;" ·,~ 262
No. people served
by Washington
water supply (est.)
Other water supplies
and no. people
served by each
Total No. of
Residents
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850
Washington surface
water intake
Nat'l Spinning co.
wells-Industrial
water supply wells
994
5100
6016
2550
Flanders Filters
Shad Bend S/D
Trails End MHP
(included in house
count above)
4340
Totals
750
2850
8500
11350
-···
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REFERENCE // 18
April Z4, 1;187
'ro: file
Frolll! Grover Nicholson C/1--IJ;-z/4-/....___
Re: Surface water use around FCX-Washington.
I talked by telephone with Henry Riddick, the Agricultural
Extension Agent for Beaufort County, [phone]. He furnished the
following information.
1. The Tar Kiver ends and the Pamlico Kiver begins along the
line of the liS 17 bridge across the river from Washington toward
Chocowinity.
2. The surface waters in the area of the site, including the
'rar and Pamlico Kivers ,af'e fresh.
3. There is no tidal influence on the river in the site area
except wind tide.
4. Kecreational boatini, and fishini,, and minor amounts of
swifilllling, occur on the river in the vicinity of the site. No use is
made of the river water as drinking water, except for the city of
wasninie,tou intake upstream of tne site on Trauters Creek.
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Ms. Pat Derosa
. ' REFERENCE II 19 .
United States Depart1nent of the Interior·
FISH AN.D .WILDLIFE SERVICE
ENDANGERED SPECIES FIELD STATION
100 OTIS STREET, ROOM 224
ASHEVILLE, NORTH CAROLINA 28801
June 21, 1985
Solid and Hazardous Waste Management Branch Environmental Health Section·
North Carolina Department of Human Resources P. 0. Box 2091 ·
Raleigh, North Carolina 27602
Dear Ms. Derosa,
In response to your telephone conversation with John Fridell on May 30, 1985, we are enclosing the following items of information:
A. North Carolina county distribution records of Federally listed, proposed and status review species,
8. map of the critical habitat of the threatened spotfin chub· (Hybopsis .monacha),
C. map of the critical habitat of mountain golden heather (Hudsonia montana), and
D. copy of the U.S. Fish and Wildlife Service interagency Section 7 consultation process .guidelines (included for your information)
Th2 abbreviations following the species names on the North Carolina species distribution records (A. above) indicate Federal status, i.e., E -endangered, T -threatened, PE -proposed endangered, PT -proposed threatened and SR -under status review. Status review species are not legally protected under the Endangered Species Act. However, they are subject to-being listed and agencies should be cognizant of their potential presence in a project area.
Since additions and deletions are made to the list of species on a regular basis, questions regarding updates of the list should be made to this office.
We hcipe this information will be of use to you. If we can be of any further assistance, please call John Fridell or Nora Murdock at [phone].
Sincerely yours,
' l . :'\r)
1\)[.i/,,cl_ \ -'<~
Warren T. Parker
Field Supervisor
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5/78
NORTH CAroLINA -Critical Habitat
Hylxlpsis nonacha, "spotfin chub"
Ma=n and Swain Counties. Little Tennessee River, ffi'l.in channel fran
the backwaters of Fontana Lake upstream to the North Carolina-Georgia
state line.
<> ~wain Co. __
----:\\ ;;:; c;.
Clar Co. (-.__ ~aron Co. . -----_____ ....___ _______ _
______ ; -\ Rabun Co.
To• n~ Co. 1
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:-.ORTII CAROl.l:s'A ---------GEORGIA
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NORTH CAROLINA -Critical Habitat
Hudsonia montana, "mountain golden· heather"
Burke County. The area bounded by the following: on the west by the
2200' contour; on the east by the Linville Gorge Wilderness Boundary
11/80
north from the intersection of the 2200' contour and the Shortoff Mountain
Trail to where it intersects the 3400' contour at "The Chimneys"--then
fol low the 3400' contour north until it reintersects the Wilderness
Boundary--then follow the Wilderness Boundary again northward until it
intersects the 3200' contour extending west from its intersection with
the Wilderness Boundary until it begins to turn south--.at this point the
Boundary extends due east until it intersects the 2200' contour.
4., Miles to
lonv1tlt r ,111
PISGAH
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Carey's saxifrag~ (Saxifraga careyana) -SR Gray's saxifrage (Saxifraga carolrniana) -SR Virginia spiraea (Spiraea virginiana -SR
Avery County
Virginia big-eared ·bat (Plecotus townsendii virginianus) -

E

Blue Ridge goldenrod (Solidago spithamaea) -

T

Hellbender (Cryptobranchus alleganiensis) -SR Bog turtle (Clemmys muhlenbergil -SR Biltmore sedge (Carex biltmoreanal -SR Bent avens (Geum geniculatum) -SR
Spreading avens (Geum radiatum) -SR Smoky Mountains manna grass (Glyceria·nubigena) -SR Mountain purple bluet (Hedyotis purpurea var. montanal ~ SR White.leaved sunflower (Helianthus glaucophyllusl -SR Heller's blazing star (L1atris helleri) -SR Gray's lily (Lilium grayil -SR
Roseroot (Sedum rosea var. roanensis) -SR Short-styled oconee-bells (Short1a galacifolia) -SR
Beaufort County
Bald eagle (Haliaeetus leucocephalus) -

E

Red-cockaded woodpecker (Picoides borealisl -

E

Carolina gopher frog (Rana areolata capitol -SR Pine barren gentian (GeritTana autumnal isl -SR_
0
Bertie County
Red-cockaded woodpecker (Picoides borealisl -

E

B 1 aden County
Red-cockaded woodpecker (Picoides borealisl -

E

American alligator (Alligator mississippiensis) -

E

Carolina gopher frog (Rana areolata capita) -SR Pine barrens treefrog (Hyla andersonii) -SR Cape Fear spike pearly mussel (Elliptic mar'supiobesa) -SR Wagner's spleenwort (Asplenium heteroresiliensl -SR Chapman's sedge (Carex chapmanii) -SR Resinous thoroughwort (Eupatorium resinosuml -SR Pine barren gentian (Gentiana autumnalis) -SR Lewis' heartleaf (Hexastylis lewis1i) -SR White-wicky (Kalmia cuneata) -SR Southern spicebush (Lindera melissifolia) -SR Carolina grass-of-parnassus (Parnass1a caroliniana) -SR Spring-flowering goldenrod (Solidago vernal -SR Wireleaf dropseed (Sporobolus teret1folius) -SR
'f, ..
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Spotfin Chub
---
Mountain Golden
Heather
1 inch~ approx. 53 miles
-llii -liiii
CRITICAL .TATS OF FEDERALLY.LISTED
ENDANGERED SPECIES IN NC
SURRY STOKES ROCKING-
HAM
YADKIN ORS_YtH GUll~Oll:O
UNION
iilil -•
rC.X-tvA~ H/A/Gr7cAJ
,,VC-I> 9-Gt '1-r+ 110
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From:
REFERENCE 1/20
i'iay 8, 1987
File
(;rover Nicholson 0-)J;.,,,/.~/.----
ft.:X-wasr,ington Kewedial Action
l spoke with J. Stewart Hodges, V.J!. fCX Inc. and asked for an
update on any rewedial action taken at the FCX site. Hr. Hodges said
that GSX had cleaned the warehouse on site and all chemicals had been
rewoved. 'ihere has been uo action taken regarding a cleanup of the
trench area.
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REFERENCE 1121
FCX Washington
NCD 981 475 932
J(
APPR.oJI. :SCALE
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SITE SJ<:ETCH
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Tizewc.1-1
Aee-A,_
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REFERENCE // 22
STATE OF NORTH CAROLINA
DEPARTMENT OF NATURAL RESOURCES AND COMXUNITY DEVELOP~NT
CLASSIFICATIONS AND WATER QUALITY STANDARDS
ASSIGNED TO
THE WATERS .OF THE TAR-PAMLICO RIVER BASIN
DIVISION OF ENVIRONMENTAL MANAGEMENT
RALEIGH, NORTH CAROLINA
Reprint from North Caroline Administrative Code: 15 NCAC 2B .0316
Current through September 1, 1981
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NRCD -ENVIRONMENTAL MANAGEMENT 2B .0300
.0301 CLASSIFICATIONS; GENERAL
(a) Schedule of Classifications. The classifications assigned
to the waters of the State of North Carolina are set forth in the
schedules of classifications and water quality standards assigned
to the waters of the river basins of North Carolina, 15 NCAC 2B
.0302 to .0317. These classifications are based upon the existing
or contemplated best usage of the various streams and segments of
streams in the basin, as determined through studies and
evaluations and the holding of public hearings for consideration
of the classifications proposed.
(b) Stream Names. The ·names of the streams listed in the
schedules of assigned classifications were taken 'as far as
possible from United States Geological Survey topographic maps.
Where topographic maps were unavailable, U.S. Corps of Engineers
maps, U.S. Department of Agriculture soil maps, and North Carolina
highway maps were used for the selection of stream names.
(c) Classifications. The classifications assigned to the
waters of North Carolina are denoted by the letters A-I, A-II, B,
C, SA, SB, and SC in the column headed "class." These class
designations refer to _ the classifications established by the
Rules, Regulations, Classifications and Water Quality Standards
Applicable to the Surface Waters of North Carolina, as adopted by
the North Carolina Board of Water and Air Resources on October 13,
1970, and approved by the Environmental Protection Agency on
January 20, 1971. A brief explanation of the "best usage" for
which the waters in each class must be protected is given as
follows:·
Fresh Waters
Class A-1: source of water supply for drinking, culinary,
or food processing purposes after treatment by
approved disinfection only, and any other usage
requiring waters of lower quality;
Class A-II: source of water supply for drinking, culinary, or
food processing purposes after approved
treatment equal to coagulation, sedimentation,
filtration, and disinfection, etc., and any other
usage specified by the "C" classification;
Class B: primary recreation and any other usage specified
by the "C" classification;
Class C: fish and wildlife propagation, secondary
recreation, agriculture and other
uses requiring waters of lower quality.
Tidal Salt Waters
Class SA: shellfishing for market purposes and any other
usage specified by the "SB" and "SC"
classification;
Class SB: primary recreation and any other usage specified
by the "SC" classification;
Class SC: fish and wildlife propagation, secondary
recreation, and other uses requiring waters of
lower quality.
-ii-
(d) Water Quality Standards. The water quality standards
applicable to each classification assigned are those established
in 15 NCAC 2B .0200, Classifications and Water Quality Standards
Applicable to the Surface Waters of North Carolina, as adopted by
the North Carolina Environmental Management Commission.
(e) Designation
(1) Trout Waters. Those streams suitable for the
propagation of natural trout and those suitable for
the maintenance of trout when stocked by the North
Carolina Wildlife Resources Commission are designated
in the appropriate columm· in the schedule of
classifications by the letters "Tr." ·
(2) Swamp Waters. Those waters which are topographically
located so as to generally have low velocities and
certain other characteristics which are different from
adjacent streams draining steeper topography are
designated by the letters "Sw" in the schedule.
(f) Index Number
(1) Reading the Index Number. The index number appearing
in the column so designated is an identification
number assigned to each stream or segment of a stream,
indicating the specific tributary progression between
the main stem stream and the tributary stream.
(2) Cross-Referencing the Index Number. The inclusion of
the index nmber in the Schedule is to provide an
adequate cross reference between the classification
schedules and an alphabetic list of streams.
(g) Classification Date. The classification date indicates the
date on which enforcement of the provisions of Section 143-215.1
of the General Statutes of North Carolina became effective with
reference to the classification assigned to the various streams
in North Carolina.
(h) Reference. Copies of the schedules of classifications
adopted and assigned to the waters of the various river basins
may be obtained at no charge by writing to:
Director
Division of Environmental Management
Department of Natural Resources
and Community Development
Post Office Box 27687
Raleigh, North Carolina 27611
History Note: Statutory Authority G.S. 143-214.1;
143-215.1; 143-215.3~a)(l);
Eff. February 1, 1976;
Amended Eff. September 9, 1979; November 1,
1978; March 1, 1977.
t
Note: Nutrient Sensitive Waters: Waters which are experiencing
or are subject to excessive growths of microscopic or
macroscopic vegetation or which are tributary to such
waters. (Nitrogen and phosphorus are the usually
controlled nutrients but other parameters may be
restricted.) They are designated in the schedule of
classifications by the letters "NSW". I
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I
Classification
N8t11e of Stream Description Class· Date Index No.
Breeches Swamp From source to Jacket SWamp C Sw 9/1/74 28-79-30-2-1-2
I Cow Hau1 Swamp From source to Beech Swatop C Sw 7/1/73 28-79-30-3
Maple Swamp From source to Fiehing Creek C 6/6/62 28<'.79-31'
Moore Svatnp From source to Maple Swamp C 6/6/62 28-79-31-1
Deep Creek From source to Fishing Creek C 7/1/73 28-79-32
I Canal Creek From source to Deep Creek C (2) 3/1/77 28-79-32-1
Marsh Swamp From source to Deep Creek C 7 /1/73 28-79-32-2
Indian Branch ~rem source to Deep Creek C 7/1/73 28-79-32-3 ·
TAR RIVER From Tarboro Raw Wat"er Supply Intake C 6/6/62 28-(80)
I to Suggs Creek
Hendricks Creek From source to Tar River C 9/1/74 28-81
Cromwell Canal and Connect-From source to Tar River C 9/1/74 28-82
ins Canals
Town Creek From source to Tar Rtver C 9/1/74. 28-83
I White S"".arnP Fro·m· source to Town Creek C 9/1/74 28-83-1
Cattail Swamp From source to White Swamp .c 9/1/74 28-83-1-1
· Williamson Branch From source to Town Creek C 9/1/74 28083-2
Cokey Swamp From source to Town Creek C 7/1/73 28-83-3
I Little Cokey Swamp From source to Cokey Swamp C 9/1/74 28-83-3-1
Deloach Branch · From source to Cokey Swamp C 7/1/73 28-83-3-2
Sasnett Mill Branch From source to Cokey Swamp. C 7/1/73 28-83-3-3
Bynuma Mi 11 Creek From source to ToWf\ Creek C 7/1/73 28-83-4
. Bynums· Mi 11 Run From source to Bynums MU l' Creek C (1) 3/1/77 28-83-4-1
I Briery Br ench From source to Bynums Mill Run C 3/1/77 28-83-4-1-1
TAR RIVER From Suggs Creek to Greenville Raw A-II 6/6/62 28-(84) .;
Water Supply Intake
Suggs Creek (Cheek Creek) From source to Tar River C 7/1/73 28-85
I· Otter Creek From source to Tar River C 6/6/62 28-86
Kitten Creek (Edson Mill From source to Otter Creek C 6/6/62 28-86-1.
Pond)
Conetoe Creek From source to Tar River C 6/6/62 28-87
Crif!P Creek From source to Conetoe Creek C 6/6/62 28-87-1
I Tyson Creek (King Creek) From source to t"ar Rt ver .c 6/6/62 28-88
(Harris Mill Pond)
Lawrence R\Jn From source to Ty eon Creek· C 6/6/62 28-88-1
Sama Branch From source to Tar River C 9/1/74 28-89
I Bryan Creek From source to Tar River C '9/1/74 28-90
Johnsons Mill Run From source to Tar River C 9 / l / 74 28-91
Har:ris Mill Run From source to Tar River C 9/1/74 28-92
SchoolhouSe Branch From source to Tar River C 9/1/74 28-93
I TAR RIVER From Greenville Raw Water Supply C 6/6/62 28-(94)
Intake to mouth at· U.S. Hwy. tl•
cr~ek
bridge at Washington
Parker From source to Tar River C 09/1/74. 28-95
Greens "Mlll Run From source to Tar River C 3/1/77 28-96
I Hardee Creek From SOiJt"CC to Tar River C 6/6/62 28-97
Barber Creek From source to Tar River C 6/6/62 28-98
Broad R~n From source tO Tar .River C 6/6/62 28-99
Moyes·· Ruri · From source to Broad Run c. 9/1/74 28-99-1
I Cannon S.iamp From source to Moyes Run C 9/1/74 28-99-1-1·
r,aldwin Swamp From source to Cannon Swamp C 9/1/74 28-99-1-1-1
Chicod CreeK From source to Tar River C 6/6/62 28-100
Juniper S·..-amp From source to Chicod Creek C 9/1/74' 28-100-1
Harding S"'·amp From source to Chicod Creek C 9 / l / 74 28-100-2
I Horseway Swlimp From source to Chicod Creek C 9 / l / 74 28-100-3
Island Swamp From source to Chicod Creek C 9/1/74 28-100-4
Co..... Swamp From source to Chicod Craek C 7/1/73 28-100-5
Cabin Branch From source to Cow Swamp C 9/1/74 28-100-5-1 f;J I Juniper Rranch From source to Chicod Creek C 7/1/73 · . 28-100-6
Grindle Creek From source to Tar River C 9 /I/ 74 28-101
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NRCD -· ENVIRONMENTAL MANAGEMENT
. Name of Strea!D
Hunting 'Run
Bear Creek
Chapel Branch
!ranters Creek
Flat Swamp
Trant_ers Creek
Collie Swamp
Turkey Swamp
· Beargrass Swamp (Harris.
Millpo~d)
Pinelog Branch
Meadow Branch
Great Branch
.Briery Swamp \Shepherd
Millpond)
Haw Branch
Horsepen .Swamp
Poley Branch
Pea Branch
Pocoaon Branch
Aggie Run
. Old Ford Swamp
Singleton Swamp
Latham Creek
Gum Swamp
Snoad Branch
Maple flranch
Mitchell Branch
Cherry Run
Trant.ere Creek
Shop Cove
Kennedy Creek
0PAHLIOO RIVER
. Jacka Creek
Runyori Creek
Runyon Creek
Herring Run and Connect-
·eanals
Pineygrove Brarich
Snode Creek
Rodman Creek
Rodman Creek
PAMLICO RIVER
Classification
Description Class -Date
From source to Grindle Creek C 9 /I/ 74
From source to Tar River C 7/1/73
_From source to Bear ~reek
From source to Collie Swamp
C 9/1/74
·c Sw 6/6/62
C SW (1.4)3/1/77 From source to Trant.era Creek
From Collie Sw&.mp to Washington
Auxiliary Raw Water Supply. Intake
From source to Tranters Creek
A-II Sw 6/6/62
C Sw
From source to Trant.ere Creek A-II Sw
From source to Turkey Swamp A-II Sw
FI"om source to Tranters Creek A-II Sw
From source to Trantera Creek A-II Sw
From source to Meadow Branch A-II sw
From source to Tranters Creek A-II Sw
From source to-Trariters Creek A-II Sw
Fr?m source to !ranters Creek A-II Sw
From source to Tranter& Creek A-II Sw
From source to Trant.era Creek A-II Sw
From source to Tranters Creek · A-II Sw
· From source to Tranter& _Creek A-II Sw
From source tO Aggie Run A-II Sw
From source to Old Ford Swamp A-II Sw
From source to Aggie Run A-II Sw
From source to Latham Creek A-II, Sw
From source to Aggie Run A-II Sw
From source to Trantera Creek A-II Sw
From source to Trant.era creek A-II Sw
From source to Tranters Creek A-II Sw
From'Washington Auxiliary Raw Water C Sw ·
Supply Intake to Tar Riv8r
From Source to r"rariters Creek
From source to Tar River
From U.S. Hwy. 17 bridge (mouth of
Ts~ River) at Washington to a line
.projected from the downstream
Co~porate Limit Line of the Town of
Washington Park in a.southwesterly
direction across PamliCo River to a
Point of Land 800 yards downstream
from Rodman Point ··
From source to Pamlico River
From source to U.S. Hwy. 264.
From U.S. Hwy. 264 to Pamlico River
From source to Runyon Creek
C
C
SC
C
C
SC
C
From source to Herring Run C
From source to Runyon CT.eek C
From source to a point one-h~lf mile C.Sw
above mouth
From.a pOint one-half mile-above SC
mouth to Pamlico River
From a line projected from the down-SB
stream Corporate Limit Line of the
Town of Washington Park in'a south-
westerly direction aoros~ Pamlico
River to a Point of L8nd 800 yards
downstream from Rodman Point to a
line across Pamlico River from Cousin
Point to Hickory Point
7/1/73
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/.6/62
6/6/62
6/6/62
6/6/62
·6/6/62
6/6/62
6/5/62.
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
6/6/62
7/1/73
7 /1/73
6/6/62
9/1/74
9/lf74
.9/1/74
9/1/74
6/6/62
6/6/62
2B .0300
TAR 7
Index No.·
28-101-1
28-102
28-102-1
28-103-(l)
28-103-2
28-103-0)
28-103-4
28-103-5
28-103-5-1
28-103-6
28-103-'/
28-103-7-1
28-103-8
:28-103-9
28-103-10
28~103-11
28-103-12
28-103-13
28-103-14
28-103-14-l
28-103-14-1-1
28-103-14-2
28-103-14-2-l
28-103-14-3
28-103-15
28-103-16
28-103-17
28-103-(18)
28-103-19
28-104
29-(1)
29-2
29-3-(1)
29-3-(2)
29-3-3
29-3-3-1
29-3-4
29-4-(l)
29-4-(2)
29-(5)'
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REFERENCE //23
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
Phillip J. Kirk, Jr., Secretary Ronald H. Levine, M.D., M.P.H.
21 July 1986
Ms. Denise Bland
EPA NC CERCLA Project Officer
Air and Hazardous Material Division
345 Courtland Street, N.E.
Atlanta, GA 30365
Dear..Ms. Bland:
SUBJECT: Preliminary Assessment Report
FCX -Washington NC D9814 75932
Grimes Road
Washington, Beaufort County, NC 27889
State Health Director
Enclosed please find the Preliminary Assessment report for the
subject site. This priority is based on review of available data.
FCX Inc. is roughly an 8 acre site located in Washington NC on
Grimes Road. The site was a farm distribution center for pesticides,
_herbicides, and tobacco treating products. ll'aste from these products were
handled from late 1945 to 1985. Apparently, about 1970, some of these toxic
wastes were buried on-site about 10 feet deep and 3 feet_above the water table
in a 12' x 250' trench.
FCX is now in bankruptcy. A sale of the property to Fred Webb of
Greensboro, NC apparently is likely. GSX has been employed to clear the
chemical 1,•arehouse and to recommend remedial action for: the buried 1-:astes.
FCX is not a RCRA facility.
Since substantial amounts·of a variety of toxic wastes are reported
buried on site and groundwater contamination is possible, it is recommended
that soil and possibly water sampling be conducted. Based on available
jnformation, a medium priority for inspection is recommended for this site.
If you have any questions, please contact me at [phone].
HH/tb/0193b
Sincerely,
A/4 p~~.
Ha~ Holladay, En,~nmental Chemist
Solid and Hazardous Waste ),\anagement Branch
Environmental Health Section
I
I POTENTIAL HAZARDOUS WASTE-SITE
PRELIMINARY ASSESSMENT
I I. IDENTIFICATION
PART I -

I

NF ORM, TI ON AND ASSESSf'ENT
SI TE t~AMC AND LOCA TI ON
: ,SITs NA~~E (Legal, common, or descriptive name of site) , _,. -Wash I ngton
1
02.STREET, .ROUTE NO., OR SPECIFIC LOCATION IDENTIFIER Gr 1mes Road
r"!• CITY
J\oiash ! ngton
vs COORDINATES: LATITUDE 35 32 36 I LONG! TUDE 77 04 27
DIRECTIONS TO SITE. (Starting from nearest pub I le road) Take US 264 West from Washington, NC. to Whispering ,e Road, turn south one block to Grimes Road -site NW of intersectlon.
RESPONSIBLE PARTIES
0 OWNER I If kno,nl r '-'X T nc. Debtor lt Debtor in Possess 1 on
07 OPERATOR (If known and d If ferent from owner) 08 STREET (Business, mal I ing, residential)
''ve /
0~ ~I TY I IO STATE 111 z IP CODE 112 TELEPHONE NUVBER I
:1r;:::P:::E-Of:::,--;O::-W::-N:::ER::-S::H::-l::Pc-:-(::-Ch:-e-c-:k-o_n_e:-) ---------------------~--------=------
111!1 A. PRIVATE I I B. FEDERAL: ____________ <A_,g""e-"n"-'-c) I JC. STATE l D. COUNTY ! l E: MUNICIPAL
I IF. ··oTHER: (Specify) JG. UNKNOWN
WNER/OPERATOR NOTIFICATION ON FILE (Check al I that apply) <CERCLA \03cl
J A •. RCRA 3001 DATE RECEIVED: IXJ B. UNCONTROLLED WASTE SITE DATE RECEIVED I I C, NONE
POTENTIAL HAZARD
BY (Check al I that apply) ,
I YES DATE I l A. EPA I l 8. EPA CONTRACTOR I l C. STATE I ) D. OTHER CONTRACTOR
I I NO CONTRACTOR NAME ( s) :
I l E. LOCAL HEALTH OFFICIAL I I F. OTHER:
J2 SITE STATUS (Check one)
A. ACTIVE IXJ.8. INACTIVE I IC. UNKNOWN
03 YEARS Of OPERATION
I 945 I 1985
BEGINNING YEAR . ENDING YEAR
l UNKNOWN
)4 DESCRIPTION OF SUBSTANCES POSSIBLY PRESENT. KNOWN, OR ALLEGED Wastes from iarm chem I ca Is -repackag Ing
,,,estlcldeo, :tobacco spray, herbicides, and the like.
)S DESCRIPTION OF POTENTIAL HAZARD TO ENVIRONMENT AND/OR POPULATION Toxic wastes reported buried on-site may ,,-r water systems -near Pam I I co River and CI ty of Wash I ngton. We I Is near s I te. Site Is about e I ght acres.
/ .li<IORITY ASSESS~ENT
JI PRIORITY FOR l,NSPECTIOI! (Check one. If h\ah.or medHium is checked,tcornplete P1artd2 -t Waste Information and . Part j -Descr1pt1on ot e:z.ar~ous l-Ond1 ions end nc1 en s)
.A. HIGH . \XI 8. MEDIUM I I C. LOW I l D. NONE
il:-is/pect/0(1 required .(lnspectlon required) (!nsp~ctbion on time (No further action 11i;eded prompr yJ ava1 le le basis> complete current disposition form)
II,FO?J'.'\TION AVAILABLE FROM
I 02 OF (Agency/Organ I zat ion l I 03 TELEPHONE NUMSER
te·.,·e:rt Hodges, V. P. IFCX Inc. I [phone]
·-ERSON RESPOl,S IBLE FOR ASSESSMEIH
r::: , y P. H.:il I aday/Grover Ni chc I son 1
05 AGENCY !ORGANIZATION 103 TELEPHONE 1w:,aER,08 DATE
NC DHR/DHSISHW Mgmt. Br. 1919) 733-280\ 07/14/66
I
I POTENTIAL·HAZARDOUS WASTE SITE
PRELIMINARY ASSESSMENT
PART 2 c WASTE I NFORl•'AT I ON
I I. IDENTIFICATION
IO I ~tA.TE I 02 SI TE. t!U:-GER D981475932
. ',ASTE STATES, Q8ANTITIES, At~D CHARACTERS
PHYSICAL FATES leheck al that apply) Ot WASTE QU.~flTY AT SITT; • Measuref g l:/as.7e quan+ j ti es 03 YASTE CHARACTERISTl?S Check al I that· app y) mus . e I noepen_den IXI A. ·TOXIC I 1 H.
I:
A SOLID I 1 E. SLURRY TONS ·
6. POWDER, FINES IXI F. LIQUID CU3 IC YARDS I I B. CORROSIVE l 1 I.
C. SLUDGE I 1 G. GAS . NO •. OF. DRUMS I I C. RADIOACTIVE I I J.
I I D. other I 1 D. PERSISTENT l 1 .K.
I I I E. SOLUBLE I 1 l.
I I F. INFECTIOUS I I M.
I I G. FLN-f-lABLE
,I. WASTE TYPES
ATEGORY SUBSTANCE NAME 0 I GROSS AMOUNT 02 UNIT OF MEASURE 03 COMMENTS SLU SLUDGE
.w Oil Y WASTE
SOL SOL VENTS
PSD PESTICIDES Not known
E OTHER ORGANIC CHEMICALS
INORGANIC CHEMICALS
ACD ADICS
e.AS BASES -fs HEAVY t-'ETALs;.
HAZARDOUS SUBSTNICES (See Append ix for most frequently cited CAS Numbers)
"EC-ORY SUBSTANCE NAME 03 GAS NUMBER 04 STORAGE/DISPOSAL METHOD 05 ·CONCENTRATION -Pest i cl des, herbicides buri a! as supp I led
and MH30 type materi a Is
lf
.
.
.
,· FECDSTOCKS <See Appendix for GAS numbers)
TE GORY 01 FEEDSTOCK NN•IE I 02 CAS NUMBER I CATEGORY 0 I FEEDSTOCK NAME
FDS I FDS
rns I FDS lFDS I FDS
rDs I FDS
't' l. souRc::-s Or l~ffQR;1..;TION (Cite specific references, e. g. state f°I les, sample analysis,
Notification 103(c) of 6/12/86 fro FCX lnc. Debtor and Debtor in Possessior ..
..... McCullou9h/J.S. Hodges telephone conversation with Harry Holladay 7/10/86.
cl FOilH 2070-12 17-Bt >
I
reports
IGNITABLE
HIGHLY VOLATILE
EXPLOSIVE
REACTIVE
I NCOt-'J' AT I BLE
NOT APPLICABLE
0&~t~~Y1lh?bN
I · 02 CAS NUMBER
I
I POTENTIAL HAZARDOUS WASTE SITE
PRELIMINARY ASSESSMENT
I I. IDENTIFICATION
Pf_qj 3 -DESCRIPTION OF HAZARDOUS 'crnm IT IONS AND I NC I OENTS 1
81: ST A TE IO? ~ 1 TE _ NIJMSER D981475932
HAZARDOUS CONDIT·IONS AND INCIDEIHS
IX'l A. GROUNDWATER COIHA~INATION
03 PO?ULATION POTENTIALLY AFFECTED ----lxic wastes burial just above.water
02 I I OBSERVED I DATE:
04 NARRATIVE DESCRIPTION
we1 Is in .area.
11_ l B. SURFACE WATER CONTAMINATION_ -02 I I OBSERVED <DATE:
POPULATION POTENTIALLY AFFECTED - · 04 NARRATIVE DESCRIPTION ----
I
01 I l C. COIHAMINATION OF AIR I POPULA T I ON POTENTIALLY AFFECTED
I I I D. FIRE/EXPLOSIVE CONDIT IONS
03 POPULATION POTENTIALLY AFFECTED
I
----
----
02 I l OBSERVED !DATE:
04 NARRATIVE DESCRIPTION
02 I I OBSERVED (DATE:
04 NARRATIVE DESCRIPTION
I l POTEIH I AL
I l POTENT I Al
Not I ikely •.
I l POTENT I AL
Not I ikely.
I l POTENT I AL
Not I ikely.
I l ALLEGED
I l ALLEGED
I I ALLEGED
I I ALLEGED
01 I l E. DIRECT CONTACT
IPOPULATION POTENTIALLY
02 I I OBSERVED COATE: I-NORTH-) J I l POTENTIAL I I. ALLEGED
AFFECTED ____ 04 IJARRATIVE DESCRIPTION Not likely._
l,)\l F. CONTAMINATION OF SOIL
03 AREA POTENTIALLY AFFECTED
ols and jugs.
(Acres)
I GI IXl G. DRINKING WATER CONTAMINATION
Ol(DPULA TI ON POTENTIALLY AFFECTED
=•le l ear in recent test.
I J H. WORKER EXPOSURE/INJURY
03 POPULAT I Oil POTENTIALLY AFFECTED
I ----
02 I I OBSERVED (DATE:
04 NARRATIVE DESCRIPTION
02 I I OBSERVED !DATE:
04 NARRATIVE DESCRIPTION
02 I I OBSERVED CDA TE:
04 NARRATIVE DESCRIPTION
0 I I.I. POPULATIW EXPOSURE/INJURY 02 I I OBSERVC:D !DATE:
03 POPULATION POTENTIALLY AFFECTED 04 NARRf.TIVE DESCRIPTION ----
I
c I FOK!-1 2070-12 I 7-8 I l
I l POTENTIAL I l ALLEGED
Toxic waste thought to be burled In
!. I POTENT I AL I J ALLEGED
One wel I 200' from FCX warehoUse said to
I J POTENT I AL
Not I ikely.
J POTENTIAL
Not I i ke I y at present.
I I ALLEGED
I I ALLEGED
I
I POTEIITI Al HAZARDOUS WASTE SI TE
PRELIMINARY ASSESSMENT
PART 3 -DESCRIPTlo:i OF HAZARDOUS CONDITIONS AIO INCIDENTS
. H.'.lA~DOUS CONDIJIONS AIJD INCIDENTS (Continued)
I l J. DP.~AGE TO FLORA 02 I J OBSERVED (DATE:
/ I. IDElmFICATION
IOINeTATE 102_ SITF. NUMBER.
· D9814 75Q32
I POTENTIAL _-,----,---03 POPULATION POTENTIALLY AFFECTED ____ 04 N_ARRATIVE DESCRIPTION Not kno,n. l l ALLEGED
I
I
I l K. DAMAGE TO FAUNA
IIARRATIVE DESCRIPTION Not known
01 l l l. COIHmlNATION OF FOOD CHAIN I NARRATIVE DESCRIPT.ION (include name(s)
02 I l OBSERVED (DATE: -----
02 I J OBSERVED (DATE: ~----of species) Not known
I / M, UNSTABLE CONTAINMENT OF WASTlc 02 I J OBSERVED COATE: Sp1 I ls/runoff/standing eaking drums) -----
I l POTENTIAL
I J POT EN Tl Al
I l POTENT! Al
03 POPULATIOll POTENTIALLY AFFECTED ____ 04 NARRATIVE DESCRIPTION Probably not.
I
l N. DAMAGE TO OFFSITE PROPERTY 02 I J OBSERVffi (DATE:
Not I ikely at present.
I
1--1 l o. &finio/g:NR~W~ oF
NARRATIVE DESCRIPTION
I
SEWERS, STORN
Not I ikely.
0 I I l P. I lLEGAl/UllAUTHOR I ZED DUMP I NG
No
02 I l OBSERVED (DATE:
02 I I OBSER YEO CDA TE:
OF ANY. OTHER KNOilN, POTENTIAL, OR ALLEGED HAZAROS
I
111. TOTAL POPULATION POTENTIALLY AFFECTED:
CC>t-1.·.,,::NTS
-----I . l POTENT !Al
I l · POTENT I Al -----
I· l POTENTIAL -----
None.
I l ALLEGED
I l ALLEGED
I l ALLEGED
I l ALLEGED
I l ALLEGED
I. l ALLEGED
is. rem:iving ·,,,,astes frorn the bui I dings and wi 11 consider burial problem. to recom'nend remedial action .
. SOURCES Or INFOR.~J..TlON (Site specific referenr:es, e .. , state files, sample analysis, reports)
Si:~ Part. l I VJ.
I
c?!-. FOilM 2070-1-2(7-81)
I
lO:.O 0 ]()')Q
CCliHOUR INTERl'i-L 5 FEET
N,t,0\0t>I/..L GEODETIC V(r.:TICI-.L DhlUM OF 1'329
600D
-. ··s ,,·o SO'"""lr.'GS a; rrc1.o.:.1ut-'. IS t•',£1,,t; LO'NW,1.l[R Q[r:ifJCU--\r. ,, ~ u,,.., -
/0:i.:J F[(j
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TO:
FROM:
RE:
Harry P. Holladay
FCX Washinrton
NC D981475932
18 July 1986
Mr. William McCullough (828-0564) legal counsel for FCX in Bankruptcy was contacted to arrange a site visit for 26 August 1986. Mr.· McCullough said he could see no problems and would issue· a letter to the concerned parties_ to inform them. He noted that sale of the property was imminent to Fred Webb of Greenville, NC, but that the new company owner was expected to be agreeable since they also wanted any problems present to be cleaned up.
Mr. McCullough was told that Grover Nicholson of .this office and Steve Hall of EPA would be part of the.visiting team. Of particular interest was the trench disposal area-where soil samples would be taken. Well water samples may also be taken. Mr. McCullough said that the well water had been tested and found clear: · A copy of the test results is to be sent here.
Mr. J. Steward Hodges, V.P. FXC (828-4411), was also contacted. The site is about 8 acres in size. Information has been collected from a number· of sources to. define the on-site disposal of the early 1970s. An aerial photograph shows-the· trench to be about 12' x 250'. It appears that the ·trench was dug to the water table and backfilled 2 -

3

feet to an estimated 10' -20' below ground level. Pesticides, herbicides, and tobacco sucker control (MH-30) materials are thought to be buried in bags and jugs. Residuals from the chemical build1ng are being cleaned up GSX. GSX has been told·about the trench material. They will develop a plan for the trench area.
FCX has a buyer for the warehouse which is considered by them to be a safe distance from the disposal area. The buyer, Fred Webb, knows of the · disposal, and will be in agreement with our visit. Mr. Hodges, or another representative, will be available to show us the disposal ·area; pwnp water for a well sample if possible, and answer questions during our August 26 visit.
The well is not on FCX property but used under a special agreement with the owner of that land. The well is about 200' from the warehouse toward the road. It is about 60' deep. National Spinning has four wells nearby.
No mercury or methoxychlor compounds for seed treating are thought to be on site.
. Willy Hardinson of NRCD [[phone]] indicated that National Spinning had wells designated numbers 8 and 9 under permit nwnber 06-0047-WC. · These 8" wells are about 100 yards from FCX and are about 244' deep. The well used by FCX was not shown in NRCD records.
HH/tb/0193b
I
I
I TO: Lee Crosby
Harry Holladay
20 June 1986
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I
FROM:
RE: Additional CERCLA Site
Please request that EPA add the. following site to the ERRIS list:
Site Name:
Address:
City:
. County:
State:
County· Code:
Congressional District:
Site Discovery Date:
FCX Washington Distribution Center
Grimes Road
Washington
Beaufort
North Carolina
07
01
11 June 1986
Contact Personnel: Harry Holladay /Grover Nicholson
I Narrative: The site is described as being similar to FCX Statesville
in the Section 103(c) notification form submitted by William H. McCullough on I ll Ju,,e 1986. The facility is in Chapter 11 bankruptcy proceedings.
,:iaterials which could include pesticides and heavy metals are allegedly buried
in.a 12' x 250' trench on-site. There is a well on-site which has been.
I reported to be clear of contamination by a consulting firm. Mr. Stewart·
HOGges, Vice-President of FCX, Inc. (not contacted) would appear to have the
best company information relating to the site.
I Soil contamination by pesticides and seed treating compounds (Hg) is
suspected. Potential for groundwater contamination exists. Residual I materials are located in the warehouse which are to be removed.
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HH/tb/0214b
I TCRAY SANf"ORD
J.A:,.LCN .,._DAMS .
WILLIA0M H. McCULLOUGH ·.
JO_,N O. 0E:ARD
E. 0. GASK:INS,JR.
ROBERT W. SPEARMAN.
HUGH STEVENS
CMARLES C. MEEKER
CATHARtr-.'E BIGGS ARAOWO~D
BA><6A"'1:A MILLS LARKIN
WILLIAM G. PAPPAS
SANFORD,ADAt,1S, McCULLOUGH & BEARD
ATTORNEYS AT LAW
P. 0, BOX 389
414 FAYETTEVILLE STREET MALL
RALEIGH, N~RTH· CAROLINA 27602 >
ALfRED P. CARLTON, JR. I CYNTHIA Lf;IGH w1rn ... cR·
··.:'LISA M. NIEMAN ..
STEVEN J. u:vnAS
'./{~:{~r--~--~:-~-_o-~:64: _-::
·· · ···CAsLE:._ADDREss SAML...A.w
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•. SLAIR LEVIN
JOHN J. 8Uilt:l'il
or (;OUNsl:.L::·
HE:MAt,r R.CI..ARK".
. .
·u r~Ited·._.·s·t&tes--
:::Proti;ctio:..1.· A rrc?1cy :-
·-... ,_:· ... P~egio:--.. _4:. ~, · .. ~ _ ._ .. -
· . .'. Sit€:S N otiflcatiOri·:··
. :._./.,, tl8nts., )~cor~-~->-· 30303 .. --:-'
cc: T.-120
·. r1--,e.~1----· !.··. :rUrc·..--.u ·:....,'• ... c.--, -· •·. ..... J
.Dr. C. r.e.•,:/e Fisher V.
WASl·HNGTON, o.c.orr1cc
2000 i,.,. STACE:T, N.W.
WASt-llNGTON.O.C.200.36.
{202) 223·0200
•. NCAL A.JAC",SON
MA.ATIN-C. F"IRCSTOSC.
DAVID P. iOWCY
F"QAO A6WAN
JO~N [;. LANIGAN
CART. OF"f"ICC ·
VILl.AGC SOUAAE. Of'F"1CC 9UILO\NG ·. ·
P.o.·aox s13 ·
CAAY; NOATt-1 CAF<OLLNA 27611
: 1919) 469·1069 ..
CHA AL.CS 1-1. MONTGOMCAY
ACt•i°l:E: J. MONTGOMCAY
NANCY. H. HEMPHILL:
.._,,,.,,v,11nt'n;a1 i-~-c-Agency •· --
1--= Thi,: i;iti~; notifi_cation ... information is ?leas-e type or print in ink.. If you need
required by Secuon 10..:,(c) of the Compre-additional space. use separate sheets of
Washington DC 2':L?'.
· hensive Environmental Response, Campen-paper. Indicate the lener. of the item
sation and Liability Act of 1980 and m~st Which applies.
be ma'iled by June 9, 1981. I
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Person Requir.ed to Notify:
Enter the name and addres..s of the person
or organization required to notify.
Site Location:
Enter the common name (if kr,own) and
actllBI location of the site.
Person to Contact:
Enter the name,'title (if applicable). and
business telephone number of the person
to contact regarding information
submitted on this form.
Dates of Waste Handling:
Enter the years that you estimate waste
treatment, storage, or disposal began and
ended at the site.
FCX. >nr Debtor and nPhtnr in Possession,
c/o J, Stewart Hodges, Vice President
_6C9 St. !~2.ly s SL..l.2c:.L.
Raleigh Zi;,Cod,e 27602
Grines Road (also known as Old Pactolus.Eigh"
c,ty Washington County Be.aufort5,.,. Zip Cooe
Nam,il,st.F.mondr-t .. 1 ·J. Stewart Hode:es ,· Vice President oi
r, 0 'il '1""> FCX Inc
Phon<t 3 3 2 -#ctrf: ' .
From('r'ur)
Late
1945 To (Yew) 198 5
I Was113 Type: Choose the option you prefer to complete
· :option :: Se:e~ gene.ral waste types and source cat~Ori~s."t(
YoL! do not know the general waste types or sources, you are · Option i:· This opti~n is ·available to persons familiar with r.i-~
ReS;Qurca Conservation and Recovery Act {RCRA) Section 3CC.
regulations (40 CFR Part 261 ). I enc:,uraged to describe the site in Item 1__:.oescription of. Sile.
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General Type of Waste: ,
Place an X in the appropriate
boxes. The categories listed
overlap. Check each applicable
category.
1. □ Organics
2: D lnorga'nics
3. D Solvents
4.xl. pesticides
5.,9: Heavy metals
6. D Acids
7. D Bases
8. D PCBs
9. D Mixed Municipal Waste
10. 0 Unknown
1 11. D Other (Specify)
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Form Ap;,roYed I O'.-n:I No. rnoo-01 Js
£C>.:., Form 8900·1
Source of Waste:
Place an X in the appropriate
boxes.
1. D Mining
2. D Construction
3. D Textiles·
4. D Fs;til:zer
5. D Paper /Printing
6. D Leather Tanning
7. D Iron/Steel Foundry
8. D Chemical, General
9. D Plating/Polishing
10. D Military/Ammunition
11. D Electrical Condoctors
12. D Transformers
13. D Utility Companies
14. D Sanitary/Refuse
15. D Photofinish
16. D Lab/Hospital
17. D Unl<nown
18. :Q Other (Specify)
A~ricultural
Suoolv Distributio
Center
Specific Type of Waste:
EPA has assigned a four-digit number to each hazardous W2::!i
listed in the regulations under Section 3001 of RCRA. Enter:
appr~riate four-digit number in the box.es provided. A copy c
the !1st of haz:ardous wastes and codes can be obtained by .
contacting the EPA Region serving the State in which the si-i.!
located.
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I WaS<a ·Quantity: ~ ' ..
Place en ... X in the appropriate boi;es to
inciicate the facility types found at the site.
ln the "total facility waste amount-space
I gi·...-e the estimated combined quantity
(volume) of hazardous wastes at the site
using cubic feet or gallons.
In the ··total facility area" space, give the
I estimated area siie which the facilities
occupy using square feet or acres.
Facility_ Type
1. □· Piles
2. D Land Treatment
3. Gl: Landfill
4. D Tanks
5. D lmpoundment
6. D Underground Injection
7. D Drums, A!)ove Ground
B. O Drums, Below Ground Ba gs
9. r.t Other (Specify) . ' ~ W~ tl U
Known, Suspected or Likely Rele,,se• to the Environment: opera tor)
Place an X in the appropriate bo.xes to indicate any lnO"NTl, suspected,
or likely releases of wastes to the environment.
T01al Facility Waste Amount
eob~ ,.., Unknown
Toual Facility Are«
/:, f; .. }U)
..,... 6'(aD-orox.)
bcttles, etc. located insic o oe re!nov a
D Likely O Sc,:-,, D Known O Suspect&d
~ \Jnlikel I Note: Items Hand I are optional Completing these items will assist EPA and State •nd local governments in locating and assess,:-,;
hazardous w~ste sites. Although completing the items is not required. you are encouraged to do so.
1 Sketch Map of Site location: (Optional)
Sketch a map showing streets. hHJhways,
routes or other prominent landmark..$ near
the site. Place an X on the map to indicate
I the si:e location. Draw an arro-,v shov,ing
the direction north. You may substitute a
publishing map showing the site location.
I On west side of Grimes Road (Old Pactolus Highway, also knc-wn as
SR 1402) several hundred feet north of the intersection of Grimes
Road and Whispering Pine RoaJ (SR 1404)
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'I o . · · t s· (O · 11 escript1on o 1te: pt1ona
Describe the history and present I conditions of the site. Give dire-...-tions to
the site and describe any nearby wells,
springs, lakes, or housing. Include such
~nformation as how waste was disposed I and where the waste came from. Provide
any other information or comments which
may help describe the site condit~ons.
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ignature and Title: t . .
The' person or authorized representmive
(sut:h as plant managers, superintend~nts,
ltrustees or anorneys) of persons requ_,red
:o notify must sign the form and provide a
~ailing address (if different lhan address
in item A). For other persons providing
notification, the signature is o-pttOnal. · l :heck the bo):;es which best describe ·the
ela:ionship to the site of the pers.on
required to notify. If you are not required
'.C notify check. "Other".
City
FCX, Inc. ,
J. Stet.1art
Debtor and Debtor in Possession
Eodges, Vice President f., Owner. Present
D Owner. Past
D Transporter
Rale. r-h s,.,, NC r.., eoa. 2 7 602 D Operator, Prese:-:1
D Operator, Past
0 Other
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REFERENCE /124
BOSE AID PURCELL, IIC.
SURVEYORS, ENGINEERS ·PLANNERS
July 21, 1986
Mr. Harry Holladay, Environmental Chemist
North Carolina Department of Human Resources
Solid and Hazardous Waste Management Branch
Post Office Box 2091
Raleigh, North Carolina 27602-2091
Subject: FCX Distribution Center Site
Washington, North Carolina
Dear Mr. Holladay:
104 GILLESPIE STREET
TELEPHONE [phone]
POST OFFICE BOX 103
FAYETTEVILLE, N.C. 28302
On May 13, 1986, I visited the FCX site in Washington, North Carolina and
took samples from the well serving Mr. Cleon Latham's house. This well is a
2" diameter well and is between 50 and 60 feet deep. The well was installed
around 1966, (see letter from Mr. Stewart Hodges attached). The well
location is shown on the attached photograph.
These samples were delivered to Carolina Chemist and Consultants, Inc.
for analysis. On June 2, 1986, I again visited the FCX site and took
another water sample in order to have the lab run TOX. Results of both
samples are attached.
Enclosed you will also find an 8 x 10 photograph showing a trench on the
rear of the property. The date of this photograph is unknown. This was
discussed with you by telephone this morning.
Please call me if you have any questions after reviewing this
information.
Enclosures
cc: Mr. W.H. McCullough
Mr. J. Stewart Hodges
CAP,jr./lk
Yours very truly,
EL1?/ IN.C. ~ -\._
arles_A • __ P.ur.cell ,_ Jr .• _____ .. _
BOSE AID PURCELL, IIC.
SURVEYORS· ENGINEERS ·PLANNERS
C.A. (ARCH) PURCELL, JR., P.E.
P.O. Box 103
Fayetteville, N.C. 28302
104 Gillespie Street
Telephone [phone]
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Inc.
5500 Commercial Avenue • Raleigh, N.C. 27612 • 19191 787-3061
June 9, 1986
CCC86278
Rose & Purcell
P. □. Box 103
Fayetteville, NC 28302
Attention: C. A. Purcell
Subject: Analysis of Sample for TOX Received 6-4-86
Sample Identification:
1. Water
RESULTS
Total Organic Halide, as Cl, ug/1
Robert W. Harris
Vice President of Scientific Affairs
RWH/km
27.4
AROLINA
HEMISTS &
I rn ONSUL TANTS, Inc.
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June 5, 1986
CCC86236
Rose & Purcell
104 Gillespie Street
Fayetteville, NC 28302
Attention: C. A. Purcell
5500 Commercial Avenue • Raleigh, N.C. 27612 • 19191 787-3061
I Subject: Analy_sis of Samples Received 5-14-86
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Sample Identification:
Thallium, total as Tl, mg/1
Arsenic, total as As, mg/1
Selenium, total as Se, mg/1
Chromium, total as Cr, mg/1
Cadmium, total as Cd, mg/1
Lead, total as Pb, mg/1
Copper, total as Cu, mg/1
Nickel, total as Ni, mg/1
Manganese, total as Mn, mg/1
Silver, total as Ag, mg/1
Mercury, total as Hg, mg/1
Magnesium, total as Mg, mg/1
Calcium, total as Ca, mg/1
Antimony, total as Sb, mg/1
Zinc, total as Zn, mg/1
Beryllium, total as Be, mg/1
Iron, total as Fe, mg/1
Cobalt, total as Co, mg/1
Vanadium, total as V, mg/1
Aluminum, total as Al, mg/1
Barium, total as Ba, mg/1
Well Water
RESULTS
<0.05
(0.05
<0.05
<0.01
<0.01
<0.02
<0.01
<0.02
0.06
<0.02
0.04 *
1 • 1
78
<0.02
0.09
<0.02
1 • 1
0.05
<0.01
0.79
<0.05
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CCC86236
6/05/86
Page 2
Total Organic
Total Organic
Chloride, as
Fluoride, as
Pesticides:
Carbon,
Carbon,
Cl, mg/1
F ' mg/1
as c, unpurged 37. 1
as c, N2' purged 34.3
10.6
0.10
None of the pesticides on the attached list were observed at or above
the reporting iimit. Some peaks were observed in the gas chromatogram
which were not identified. These unknown compounds are apparently
present at very low levels (fractional ppbl.
* Mercury data suspect due to unknown interference in
was insufficient sample to permit additional analysis.
that organomercurials have been used as pesticides.
Semi-Volatile Compounds
Phenol
bis (-2-Chloroethyl) Ether
2-Chlorophenol
1 3,Dichlorobenzene
1 4,Dichlorobenzene
Benzyl Alcohol
1 2-Dichlorobenzene
2 Methylphenol
N-Nitroso-Di-n-propylamine
Hexachloroethane
Nitrobenzene
lsophorone
2-Nitrophenol
2,4-0imethylphenol
Benzoic Acid
bis (2-chloroethoxy)Methane
2,4-0ichlorophenol
1,2,4-Trichlorobenzene
Naphthalene
RESULTS
ug/1
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
(50
<10
<10
<10
<10
sample. There
Please note
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CCC86236
6/05/86
Page 3
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-Methylphenol
2-Methylnaphthalene
Hexach lorocyc lo·pentad iene
2,.4 1 6-Trichlorophenol
2,4,5-Trichlorophenol
2-Chloronaphthalene
2-Nitroaniline
Dimethyl Phthalate
Acenaphthylene
3-Nitroaniline
Acenaphthene
2,4-Din~trophenol
4-Nitrophenol
0ibenzofuran
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Diethylphthalate
4-Chlorophenyl-phenylether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-Methylphenol
N-Nitrosodiphenylamine(l)
4-Bromophenyl-phenylether
Hexachlorobenzene
Pentachlorophenol
Phenanthrene
Anthracene
Di-n-Butylphthalate
Fluoranthene
Pyrene
Butylbenzylphthalate
3,3-Dichlorobenzidine
Benzo(a)Anthracene
bis(2-EthylhexyllPhthalate
Chrysene
Di-n-Dctyl Phthalate
Benzo(b)Fluoranthene
Benzo(k)Fluoranthene
Benzo(alPyrene
Indeno<l,2,3-cdlPyrene
Dibenz(a h) Anthracene
Benzo(g h llPerylene
<10
<10
<10
<10
<10
<10
<50
<10
<10
<10
<10
<50
<10
<50
<50
<10
<10
<10
<10
<10
<10
<50
<50
<10
<10
<10
<50
<10
<10
<10
<10
<10
<10
<20
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
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CCC86236 I • 6/05/86
Page 4
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Volatile Compounds
Chloromethane
Bromomethane
Vinyl Chloride
Chlorethane
Methylene Chloride
Acetone
Ca~bon Disulfide
1,1-0ichloroethene
1,1-0ichloroethane
Trans-1,2-Dichloroethene
Chloroform
1,2-Dichloroethane
2-Butanone
1,1,1-Trichloroethane
Carbon Tetrachloride
Vinyl Acetate
Bromodichloromethane
1,2-Dichloropropane
I. Trans 1, 3-Dichloropropene
Trichloroethene
Dibromochlorometharye
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1,1,2-Trichloroethane
Benzene
cis-1,3-Dichloropropene
2-Chloroethylvinylether
Bromoform
4-Methyl-2-Pentanone
2-Hexanone
Tetrachloroethene
1,1,2,2-Tetrachloroethane
Toluene
Chlorobenzene
Ethyl benzene
Styrene
Total Xylenes
Vice President of Scientific Affairs
I RWH/km ••
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ug/1
<10
<10
<10
<10
24
15
< 5
4.0
3. 1
< 5
< 5
< 5.
20
< 5
< 5
<10
< 5
< 5
< 5
< 5
< 5
< 5
< 5
< 5
<10
< 5
<10
<10
< 5
< 5
3.3
< 5
< 5
< 5
< 5
,,
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Mevinphos
I 2,4-D <ME)
Phorate
alpha-BHC
CDEC I 2,4-D<IPE>
Simazine
Atrazine
I Diazinon
Linda.ne
2,4,5-T<ME>
I beta-BHC
2,4-D(BE)l
gamma-BHC
I
Heptachlor
2,4,5-T(IPE)
2,4-D<BE>11
Dichlone
I Dimethoate
Aldrin (Reference)
Ronneil
1•1-Hydroxychlordene
M.Parathion
Heptachlor Epoxide
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Malathion
DCPA
Dyrene
a,p'-DDE
Chlorbenside
E. Parathion
Endosulfan I
p,p'-DDE
DDA<MEl
Captan
Folpet
Dieldrin
Parthane
o,p'-DDD
o,p'-DDT
Endrin
Chlordecone
p,p'-DDD
Endosulfan II
Ethion
p,p'-DDT
Carbophenothian
Dilan 1
•
Mirax
1 Methoxychlor
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PESTICIDES
Reporting Detection Limit
0.5 ug/1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5.
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
Dilan 11
Tetradifan
Azinphosmethyl
0.5
0.5
0.5·
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REFERENCE //25
21 July 1986
TO: File
Fil.OM: Grover Nicholson
RE: Ft;X -Washington
In a telephone conversation with Harry Holladay of the N(; Solid and
Hazardous Waste Management Branch CERCLA Unit, Arch Purcell of Rose and
Purcell, Inc. [phone] supplied the following information.
1. The nearest well, at Cleon Latham's house, is 250 feet from the
main warehouse. The well is 50 to 60 feet deep with 2 inch
diameter casing. It was installed in 1966.
2. He will send an 8 x 10 photo of the site showing the open trench
behind the warehouse. The trench was about 20 feet x 200 feet I x 6 feet deep.
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3. FCX now uses city water.
4. Arch l'urcell will be there during the site inspection if needed.
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REFERENCE // 26
P. 0. BOX 2419 • RALEIGH, NORTH CAROLINA 27602 • TELEPHONE [phone]
June 16, 1986
Mr. W. H. McCullough
Sanford, Adams, McCullough & Beard
Attorneys at Law
P. 0. Box 389
Raleigh, North Carolina 27602,
RE: WELL AT WASHINGTON DISTIUBUTION CENTER
Dear Bill:
I visited the Washington Distribution Center on Thursday,
June 12, 1986 and found that the well is a 2" well and that it is
no more than 60' deep. The well was drilled around 1966 .
The owner of the house (Cleon Latham) who used the well,
now connected with city water and lines from the well to
house have been cut. The well is also inoperative due to
and we no longer have service to the Distribution Center.
is
his
this
If there is any further information that you need on this,
please let me know.
~~:Ja:r. Charles i\, Purcell
Rose & Purcell
'P, O. Box 103
Fayetteville, NortbCarolina 28302
~•PO!itfi1 1MM!lfJHi➔JiMlli1·IHl 1 l!ifliliirl•FH--
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Appendix D
Site Inspection Form
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D
POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION
SITE INSPECTION REPORT NC D 981475932 oEPA
PART 1 • SITE LOCATION AND INSPECTION INFORMATION
01 STATE I 02 SITE NUMBER
II. SITE NAME AND LOCATION
01 SITE NAME (L-a•I. commo,,, ordncr/pli~ ,....,,, or 11re/ 02 STREET, ROUTE NO., OR SPECIFIC LOCATION IOENTIFlEA
FCX-Washington Grimes Road (SR 1402) OJ CITY 04 STATE I 05 ZIP CODE I 06COUNTY 1°7COUN1l 06 CONG COOE DIST Washington NC 27889 Beaufort . 07 01 09 COORDINATES 1 O TYPE OF OWNERSHIP (Cl>eck on•) LATIT.IJOE I t.OMGl~IDE je A. PRIVATE O B. FEDERAL 0 C.STATE 0 0. COUNTY O E. MUNICIPAL -35. 32... .3.6... . _Jf]']__ 0A 27 0 F.OTHER 0 G. UNKNOWN Ill. INSPECTION INFORMATION
01 DATE OF INSPE<;:TID_N 02 SITE STATUS 03 YEARS OF OPERATION
. M~N~Hi &,~ i,~
0 ACTIVE ]9~5 I ]986 _UNKNOWN -~ INACTIVE BEGINNING YEAR ENDING YEAR 04 AGENCY PERFORMING INSPECTION (Ch~-lllrh•t .,,,,irJ
0 A.EPA 0 B. EPA CONTRACTOR· 0 C. MUNICIPAL 0 D. MUNICIPAL CONTRACTOR
~E.STATE (N.,.,. ol //rm} f~Olllrm) 0 F. STATE CONTRACTOR □G.OTHER /N.,,..oflltm} {Specify} 05 CHIEF INSPECTOR 06 TITLE 07 ORGANIZATION 08 TELEPHONE NO.
Grover "' "h" 1 ---r-""' l ~, _,_ ··~ 1 q1 & rn .~qn 09 OTHER INSPECTORS 10 TITLE 11 ORGANIZA 110N 12 TELEPHONE NO.
Hart-v Holladav Chemist NC SFIWMB ( 919 733-280
( } ..
( }
.
( }
( }
13 SITE REPRESENTATIVES INTERVIEWED 14 TITLE ' 15AODRESS 16 TELEPHONE NC?£0"1'
J. Stewart Hodges V.P. FCX INC 609 St. Marys Sti:.2~£~ N , ! 91~ 832-,640"
( }
( }
( }
I }
( }
17 ACCESS GAINED BY 16 Tl~E OF INSPECTION 19 WEATHER CONDITIONS {Check one}
XJ PERMISSION □WARRANT 1000 Clear and warm
IV. INFORMATION AVAILABLE FROM
01 CONTACT 02 QF (Ao,in,;,~/Otpa,wi,eflotl,I 03 TELEPHONE NO. • ,
J. Stewart Hodges ( 919 {.o4 FCX, Inc. 832-~ 04 PERSON RESPONSIBLE FOR SITE INSPECTION FORM 05 AGENCY
'' 1
06 ORGANIZATION 2 07 TELEPHONE NO. 06DATE Grover Nicholson NC DHR SHWMB 919-733-2801 05 , n4, R7
MONTH DAY YEAR EPA FORM 2070-13 (7•6 I)
Notes: 1.
2.
North Carolina Department Of Human Resources Solid and Hazardous Waste Management ··Branch •
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION REPORT 01 STATE 102 SITE NUMBER NC D 981475932 PART 2 • WJ\STE INFORMATION
II. WASTE STATES, QUANTITIES, AND CHARACTERISTICS I
01 PHYSICAL ST ATES /Cl!t1c• aN mar •pply! 02 WASTE QUANTITY AT SITE 03 WASTE CHARACTERISTICS /Cl>•c• •• 111e1 "1'fl/y}
{Me,1su1os ot w.ure <1ua11/l/les
CJ A. SOLID lJ E. SLURRY 'Tl<JS! be mdel)ene1enr1 }i,! A. TOXIC 0 E. SOLUBLE 0 I.HIGHLY VOLATILE
C{ 8 POWDER. FINES XI F. UOU!D TONS IJ 8. CORROSIVE 0 F. INFECTIOUS 0 J. EXPLOSIVE
IJ C. SLUDGE lJ G.GAS 0 C. RADIOACTIVE □ G. FLAMMABLE 0 K. REACTIVE
CUBJCYARDS UNI< }l,l D. PERSISTENT 0 H. IGNITABLE 0 l. INCOMPATIBLE
U 0. OTHER 0 M. NOT APPLICABLE
I
(Spt1crly) NO.OF DRUMS
Ill. WASTE TYPE ..
CATEGORY SUBST ANGE NAME 01 GROSS AMOUNT 02 UNJT OF MEASURE OJ COMMENTS
SLU SLUDGE An . ~~~-J--i ..... TT r,_-f:
OLW OILY WASTE herbicides, nesticides, and
SOL SOLVENTS other fanu chemicals were buried
PSO PESTICIDES UNI< in ·an.' on-site trench in or
ace OTHER ORGANIC CHEMICALS Tll\TT< a=ut J.':J/U. D
roe INORGANIC CHEMICALS
ACO ACIDS
BAS BASES u
MES HEAVY METALS UNI<
IV. HAZARDOUS SUBSTANCES {See App,,ndJ~fo,most frequltntly c,redCAS N<1mbets/
01 CATEGORY 02 SUBSTANCE NAME 03 CAS NUMBER 04 STORAGE/DISPOSAL METHOD 05 CONCENTRATION 06 MEASURE OF
CONCENTRATION PSD Aldrin 31,ann2 Bu-'"i' Tll\TT< PSD Chlordane 57749 µ_,, ..... i::il ~ UNI< PSD DDE 72559 ,,,,~-( ;al : UNI< PSD DDT 50293 Burial' UNI< I
pc,r, n;o1..:i-;n Cf>C71 Burial. ---· ace Carbondisulfide 75150 Burial, fTI\Tl( ace Hexachlorobenzene 118741 Burial TThW I
occ Naphthalene 91203 ·Burial· UNI< occ Phenanthrene 85018 Burial· UNK occ Acenaphthylene 208968 ·.Burial T11\W I
C U...'C Fluorene 86737 n .•. ..:; C:::f UNI< U...'C Dibenzofuran " "-•""i "l ..• TThW occ . 2-Methylnaphthalene ·' . ... •f'o,~-i ;::il · TThW I
MES Mercury 7439976 Burial UNI< I
V. FEEOSTQCKS (SuAppendi. lorCAS N<Jmbers/
CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER CATEGORY 01 FEEDSTOCK NAME 02 CAS NUMBER
FOS FOS I
FOS FDS
FOS FOS
FOS FOS I
VI. SOURCES OF INFORMATION re,,., spec,11c,e1e,encu, "•<J• s(a/f f#n. ump/9 enelys1s, ,epo,rsJ
,.,
References 5.10 I
.
I EPA FORM 2070·13(7•81!
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION
SEPA 01 STATE! 02 SITE NUMBER SITE INSPECTION REPORT NC D 981 475 932 PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS
II. HAZARDOUS CONDITIONS AND INCIDENTS
01 Ill A. GROUNDWATER CONTAMINATION 02 0 OBSERVED(DATE: I ~POTENTIAL 0 ALLEGED
03 ,POPULATION POTENTIALLY AFFECTED: 2850 04 NARRATIVE DESCRIPTION
he' •wastes · may move into the groundwater, which is within 5 feet of the· deposition of
chemicals.
01 lil B. SURF ACE WATER CONTAMINATION 02 0 OBSERVEO(DATE: I ~ POTENTIAL D ALLEGED
03 POPULATION POTENTIALLY AFFECTED: {) 04 NARRATIVE DESCRIPTION
~ ·-Surface soils are contaminated and
into the adjacent wetland.
run off from the site may could carry contaminants
01 DC. CONTAMINATION OF AIR 02 0 OBSERVED(DATE: I 0 POTENTIAL 0 ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION
None noted
01 0 0. FIRE/EXPLOSIVE CONDITIONS 02 0 OBSERVED (DATE: I 0 POTENTIAL 0 ALLEGED
03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION
None noted
'
OlxJ E. DIRECT CONTACT 02 0 OBSERVED (DATE: I Ix POTENTIAL D ALLEGED
03 POPULATION POTENTIALLY AFFECTED: n 04 NARRATIVE DESCRIPTION .
Potential contact hazard to workers rerrovinq the contaminated soil or other per9ons who happen to be in the burifl area exists ..
01 (xF. CONTAMINATION OF SOIL 02 0 OBSERVED IOATE. 26 .Aug;. Jl6 0 POTENTIAL 0 ALLEGED
03 AREA PO"fENTIALLY AFFECTED: '< Q l 04 NARRATIVE DESCRIPTION (Acres/
Analyses of soil. sanples shows contamination with pesticides, organic chemicals, and mercury.
01fJ G. DRINKING WATER CONTAMINATION 02 □ OBSERVED (DATE: I ~POTENTIAL D ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 26SQ 04 NARRATIVE DESCRIPTION
The wastes may rrove into the groundwater which supplies 2850 6f the site. people within three miles
01 ~ H. WORKER EXPOSUREJINJUAY · 02 0 OBSERVED (DATE: I D POTENTIAL 0 ALLEGED 03 WORKERS POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION
Clean-up workers exposure is potentially hazardous.
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01 0 I. POPULATION EXPOSURE/INJURY 02 D OBSERVED (DATE: I D POTENTIAL. D ALLEGED 03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION
Not likely.
EPA FOAM 2070-13 (7•81 I
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION oEPA SITE INSPECTION REPORT 01 STATE,02 SITE NUMBER
PART 3 • DESCRIPTION OF HAZARDOUS CONDITIONS AND INCIDENTS "r fl 0A1 47S q,2
II. HAZARDOUS CONDITIONS AND INCIDENTS /C011/,nue<1/
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01 0 J. DAMAGE TO FLORA 02 0 OBSERVED (DATE· I 0 POTENTIAL D ALLEGED ! 04 NARRATIVE DESCRIPTION
None noted. I
01 0 K. DAMAGE TO FAUNA 02 0 OBSERVED (DATE: I 0 POTENTIAL 0 ALLEGED 04 NARA A TIVE DESCRIPTION u11c1ooe nJme/s! 01 spec~s, I
None noted. I 01 0 L. CONTAMINATION OF FOOD CHAIN 02 0 OBSERVED {DATE: I 0 POTENTIAL· 0 ALLEGED 04 NARRATIVE DESCRIPTION
Not likely.
01 0 M. UNSTABLE CONTAINMENT OF WASTES 02 □ OBSERVED (DATE: I 0 POTENTIAL 0 ALLEGED (S,:;><IIS!Runotf/St•lldm,;; /,Quids, Luk.i,,a dtumsl
03 POPULATION POTENTIALLY AFFECTED: 04 NARRATIVE DESCRIPTION
None noted.
01 0 N. DAM.AGE TO OFF SITE PROPERTY 02 0 OBSERVED (DATE: I □ POTENTIAL 0 ALLEGED 04 NARRATIVE DESCRIPTION
None noted.
01 0 0. CONTAMINATION OF SEWERS. STORM DRAINS, WWTPs 02 0 OBSERVED (DATE: I 0 POTENTIAL 0 ALLEGED 04 NARRATIVE DESCAlP_"flON
None noted.·
,.
01 0 P. ILLEGAUUNAUTHOAIZEO DUMPING 02 0 OBSERVED (DATE: I [] POTENTIAL D ALLEGED 04 NARRATIVE DESCRIPTION
None noted. D
05 DESCRIPTION OF ANY OTHER KNOWN. POTENTIAL. OR ALLEGED HAZARDS
0
Ill. TOTAL POPULATION POTENTIALLY AFFECTED:
IV. COMMENTS D
D
V. SOURCES OF INFORMATION 1c,1.,sp.,c11,c ,e,,,,.,ncH . ., 11 , S/dl.,f,16$. umo/.,,tndl~••s.1<>r,o,is1 D I References 1, 3, 4, 10, 12,13, 14, 15, 16, 18. . '-·------· --... .. . . .. u
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION ~e'' ATE I 'B S'MMiw, 5 932 PART 4 • PERMIT AND DESCRIPTIVE INFORMATION
II. PERMIT INFORMATION
01 TYPE OF PERMIT ISSUED 02 PERMIT NUMBER
/Cht1c;k di/lat •pl)ly/ 03 DATE ISSUED 04 EXPIRATION DATE OS COMMENTS
□A. NPDES
DB. UIC .
DC. AIR
DD. RCRA
OE. RCRA INTERIM STATUS
OF. SPCC PLAN
OG. STATE /Stit1c,ly!
OH. LOCAL tS()ec,M
[JI. OTHER f$pec1ty/
.
IXJ. NONE
Ill. SITE DESCRIPTION
0 I STORAGE/DISPOSAL /Ch•c• aR Iha/ .pply! 02 AMOUNT 03 UNIT OF MEASURE 04 TAEA HAEN! (Chee• .i111at ~ply/ OS OTHER
0 A. SURFACE IMPOUNOMENT 0 A. INCENEAA TION
0 B. PILES 0 8. UNDERGROUND INJECTION SI A. BUILDINGS ON SITE
0 C. DRUMS, ABOVE GROUND 0 C. CHEMICAUPHYSICAL
0 0. TANK, ABOVEGROUND 0 D. BIOLOGICAL
0 E. TANK, BELOW GROUND 0 E. WASTE OIL PROCESSING 06 AREA OF SITE .
D F. LANDFILL 0 F. SOLVENT RECOVERY
0 G. LANOFARM 0 G. OTHER RECYCUNG/RECOVEAY 8 {ACtH) . 0 H. OPEN DUMP 0 H.OTHER Trench burj,al lll:1.0THER_ ,Buria]_ ll!llK /Specify/
(:,Pcrc,ty} < 0:1 acre
07 COMMENTS
IV. CONTAINMENT
01 CONTAINMENT OF WASTES(Cfl-.::~ one/
0 A. ADEQUATE, SECURE 0 8. MODERATE ~C. INADEOUATE, POOR 0 D. INSECURE. UNSOUND, DANGEROUS
02 DESCRIPTION OF DRUMS. DIKING, LINERS. BARRIERS. ETC.
The wastes were buried in a trench about 12 feet by 250 feet by 10 to 12 feet deep.
V. ACCESSIBILITY
01 WASTE EASILY ACCESSIBLE: 0 YES 0 NO
-02COMMENTS
Moderately accessible. Some wastes are on surfa_ce mixed with soil. ',
VI. SOURCES OF INFORMATION /Cltesueei/,c1elere11ces. •·O i,.,ehles. 1.mp1e.,,,>1ysls. ret)Orf_SJ
References 3,5.
EPA FORM 2070-13 (7-81 J
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&EPA POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION
SITE INSPECTION REPORT 01 STATE,02SITENUMBER
PART 5 • WATER, DEMOG.RAPHIC, AND ENVIRONMENTAL DATA "'"' D qgl 475 932
II. DRINKING WATER SUPPLY
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01 TYPE OF DRINKING SUPPLY 02 STATUS 03 DISTANCE TOSITE (Cnect u ap,:,6cM1/eJ
SURFACE WELL ENDANGERED AFFECTED MONITORED 2 ),,-. ;, COMMUNITY A.cl{ s.1§ A.0 B.0 c.o A. 1900 (ml)
NON•COMMUNITY C.O D.lll D.0 E.0 F.0 B. (ml)
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Ill. GROUNDWA TEA
01 GROUNDWATER USE IN VICINITY (Check one) I
0 A. ONLY SOURCE FOR DRINKING [}{B. DRINKING 0 C. COMMERCIAL, INDUSTRIAL, IRAIGA TION 0 D.NOTUSED,UNUSEABLE (Other sources evaila~) (Llmll/Jd other 1oorc11$ av,Hable)
COMMERCIAL, INDUSTRIAL, IRRIGATION {No other water iourcu avahtJJ./ I
02 POPUL.A TION SERVED BY GROUND WATER 2850 03 DISTANCE TO NEAREST DRINKING WATER WELL 2QQQ ft, (mi)
04 DEPTH TQ GROUNDWATER 05 DIRECTION OF GROUNDWATER FLOW 06 DEPTH TO AQUIFER 07 POTENTIAL YIELD 08 SOLE SOURCE AQUIFER I south OF CONCERN OFAOUIFER 5 'ft) 5 -[XYES D NO (ft) •(gpd).
09 DESCRIPTION QF WELLS (lnclud!nQ use~•. depth, •nd/ocll/lon relative lo PQtWtatlon .n<1buld1ng,/
Most wells in the area are completed into.the Castle Hayne aquifer .which begin5about I
30 ft. below the surface and which is locally .recharged from the two overlying aquifers, the Post-Miocene surficial.aquifer:·and the Miocene Yorktown aquifer. I 10 RECHARGE AREA 11 DISCHARGE AREA
fj(YES COMMENTS 0 YES COMMENTS 0 NO ONO I IV.SURFACE WATER
01 SURFACE WATER USE/Chac~oneJ
~A. RESEAV01A, RECREATION 0 B. IRRIGATION, ECONOMICALLY 0 C. COMMERCIAL, INDUSTRIAL 0 0. NOT CURRENTLY USED DRINKING WATER SOURCE IMPORTANT RESOURCES I
02 AFFECTEDIPOTENTIALL Y AFFECTED BODIES OF WATER
NAME: AFFECTED DIST ANGE TO SITE I Tar River
D 3600 ft. {mi) Kennecty Creek D 800 fl:. (mi)
D {mi) I
V. DEMOGRAPHIC AND PROPERTY INFORMATION
01 TOTAL POPULATION WITHIN 02 DIST ANGE TO NEAREST POPULATION
ONE ( 1) MILE OF SITE TWO (2) MILES OF SITE THREE (3) MILES OF SITE City of Washington
A. 994 B. 7010 C. 11350 ...J8QQ~ ft. (rni)
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NO. OF flEASONS NO. OF P_ERSONS NO. QF PERSONS '
. -~
03 NUMBER OF BUILDINGS WITHIN TWO (2) MILES OF SITE 04 DISTANCE TO NEAAESTOFF•SITE BUILDING
UNI< 600 ft. (ml)
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05 POPULATION WITHIN VICINITY OF SITE /Pro'l'ide n•,,.llv• desc,t,tlon at n•wr• ot p0owa11on "''"'"' wcklitr ol Sir•. •.o n,rel, ><iflsO.,, d•nsely f)Op<Jlafed utben •r•aJ The city of Washington, population 8500, is about·, 1800 feet east of the site. Less I populated rural residential and commercial areas are adjacent to the site.
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EPA FORM 2070·13 /7•81) I
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I POTENTIAL HAZARDOUS WASTE SITE I. IOENTIFICA TION oEPA -SITE INSPECTION REPORT 1-\t•r•1°1f9'1lf3•ij75 932 PART 5 • WATER, DEMOGRAPHIC, AND ENVIRONMENTAL DATA
VI. ENVIRONMENTAL INFORMATION
01 PERMEABILITY OF UNSATURATED ZONE /Cll<IC:k o,,•J
D A. 1 o-6 -1 o-a cm/sec □ B. 1 Q--4 -1 o-6 cm/sec O c. 1 o-" -10-3 cm/sec f5 0. GREATER THAN 10-3 cm/sec I 02 PERMEABILITY OF BEDROCK /Ch•ck on•J
0 A. IMPERMEABLE □ B. REL.A TlVEL Y IMPERMEABLE 0 C. RELATIVELY PERMEABLE ~ 0. VERY PERMEABLE /Lesslhan ,o-6 cmlstK.} po-• -,o-11 "'"'HC} po-2 -,o-• cmlHC/ /Gr•.r•tnan ,o-2c,m1,..:1
03 DEPTH TO BEDROCK 04 DEPTH OF CONTAMINATED SOIL ZONE 05SOlLpH
To Cast130Ha~r L UNK UNK (ft)
D 06 NET PRECIPIT ATJON 07 ONE YEAR 24 HOUR RAINFALL 08SLOPE
SITE SLOPE I DIRECTION OF SITE SLOPE I TERRAIN AVERAGE SLOPE 12 {in) 3.48 (in) 3 ,. south 1 " 09 FLOOD POTENTIAL 10 D 0 SITE IS ON BARRIER ISLAND, COAST AL HIGH HAZARD AREA, RIVERINE FLOODWA Y SITE !SIN -YEAR FLOODPLAIN
11 DISTANCE TO WETLANDS rs • .,,.m,n.m""'/ 12 DISTANCE TO CRITICAL HABITAT /olend•"'J••ad 1<0«'-•I u ESTUARINE OTHER -(mi)
300 ft.lmil -A. (mi) B. ENDANGERED SPECIES: 1 3 LAND USE IN VICINITY
I DISTANCE TO:
RESIDENTIAL AREAS; NATlONAUST ATE PARKS, AGRICULTURAL LANDS COMMERCIALJINOUSTRIAL FORESTS, OR WILDLIFE RESERVES PRIME AG LANO AG LAND
A. 600 ft. (mil B. 600 ft. {ml) C. {ml) D. 120 ft.(ml)
14 DESCRIPTION OF SITE IN RELA!ION TO SURROUNDING TOPOGRAPHY
I The site lies in a low area adjacent to a wetland which leads to the Tar River. Agricultural land lies ·to the northwest ahd southeast. Slightly topographically higher residential and comuercial land lies to the east and northeast.
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I VII. SOURCES OF INFORMATION fC•r•si>•<:111<:,•l•,.""<n, •·O·· itat• t1••· umpM.,,-.,Ys,s, ••,x,,tiJ
I References 8,7,4, 1, 12, 17, 18
p I. E AFORM2070 13(7 81)
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION SEPA 01 STATE,02 SITE NUMBER SITE INSPECTION REPORT NC D 981 475 93. PART 6 -SAMPLE AND FIELD INFORMATION
II. SAMPLES TAKEN
01 NUMBER OF 02 SAMPLES SENT TO 03 ESTIMA TEO DATE SAMPLE TYPE SAMPLES TAKEN RESULTS AVAILABl.E
GROUNDWATER 5 NC State Laboratory of Public Health Feb_ 1982
SURFACE WATER
WASTE
AIR
RUNOFF
SPILL
SOIL 7 W' ~ . T ~· ,? r,.,= T').,hl .;r, u,....,1.J-'h ~-t-. l no·
VEGETATION -
_OTHER Sedirrent 1 NC State Laboratory of Public Health Feb. 198:
Ill. FIELD MEASUREMENTS TAKEN
01 TYPE 02 COMMENTS
IV. PHOTOGRAPHS AND MAPS Included
01 TYPE ~ GROUND O AERIAL I 02 IN CUSTODY OF i n _,
(Naffiff ol Of(Jltll/lllion or lndMdual}
03 MAPS 04 LOCATION OF MAPS
!XYES Included in rep:irt
0 NO
V. OTHER FIELD DATA COLLECTED (Prow:Jenerrat/,,edescrip/lOfl}
VI. SOURCES OF INFORMATION (Cltesru,c,f,cr.,rer9nces, "·11-, s11111 Ir/as. nmp/aaMlys,s. ,eponsJ
Reference 10 and site inspection of Aug. 26, 1986 and Nov. 20, 1986.
EPA FORM 2070-13 (7·81)
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POTENTIAL HAZARDOUS WASTE SITE I.IDENTIFICATION
&EPA SITE INSPECTION REPORT 0N'c''E 1°2 t1'·~~'f•i1s 93
PART 7 • OWNER INFORMATION
II. CURRENT OWNER($) PARENT COMPANY '"-,.;.at,i./
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jo1 NAME 02 O+B NUMBER 08 NAME 09 O+ B NUMBER
Fred Webb, Inc.
03 STREET AODRESS/P.0. 8o;r, RFOI, 11c.J 104 SIC CODE 10 STREET AOORESS(P.O. So,. RFD,, •le.I r 1 ~ICCO~ P.O. Box 158
OSCITY · r6~~TE 07 ZIP CODE 12 CITY 113STATE 14 ZIP CODE
·Greenville 27834
01NAME 02 D+B NUMBER 08 NAME 09D+BNUMBEA
I 03 STREET ADORESS/1'.0. Bo•. RFD11. ,1c.J l°'ISICCOOE 10 STREET AODRESS/P.O. Bo•. RFD•. a1c.J , , , SIC CODE, ·•-.-
I 05CITV ,□6 STATE 07 ZIP CODE 12 CITY 113STATE 14 ZIP CODE
01 NAME 02D+BNUMBEA 08NAME 09 0+8 NUMBER
I 03 STREET AOORESS(P.O. Bo,. RFD•. e/c,J 104 SICCOOE 1 0 STREET ADDRESS fl'.O. Bo•. RFD•. ,tc.J I\ tSICCOOE
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05 CITY 106 STATE 07 ZIP CODE 12 CITY r3STA~E 14 ZIP CODE
01NAME 02 D+B NUMBER OB NAME 09D+BNUMBER
I 03 STREET ADDRESSw.o Bo•. RFD,. •tc.J 104 SICCO~E 10 STREET ADDRESS (P.O. Bo•. RFD"· •tc.J r 1 SIC~ODE
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05 CITY 106 STAT 07 ZIP CODE 12CITY TJSTATE 14 ZIP CODE
Ill. PREVIOUS OWNER($) /List most ,CIC.,,, first) , IV. REAL TY OWNER($) (11 ipp,,,:at,i.: 11:st =t ,.cent fir$!/
01NAME 020+BNUMBER 01NAME 02 D+B NUMBER
FCX Inc.
03 STREET AODRESS/P.O, ao •. RFDI, •fc.! I 04 s'.c co_oE 03 STREET AODRESSrP.0, Bo,. RFD•. ate./ . I (?4 SIC CODE 609 St. Marys Street .
D
05CITY f°6STATE 07 ZIP CODE 0~ CITY I06STATE 07 ZIP CODE
Raleigh NC 27602
01 NAME 02 0+8 NUMBER 01NAME 02 D+B NUMBER
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03 STREET ADDRESS fP.0. Bo•. RFD•. •tc.J 104 SIC CODE 03 STREET ADDRESS (P.O. Bo•. RFD•. •tc.J I04SICCODE
05 CITY I06STAT.E 07 ZIP CODE 05CITY l06STATE 07 ZfPCODE
Ol·NAME 02 O+B NUMBER 01 NAME 02 D+BNUMBER·
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p3 STREET ADDAESSrP.O. Bo•. RFq,. •fc.} 104 SlCCOOE 03 STREET ADDRESS /P.O. Bo•. RFD•. ,1c} I 04 SICCOOE
05CITY I06STATE 07 ZJPCOOE 05 CITY 1°6STATE 07 ZIPCOOE
V. SOURCES OF INFORMATION /CII• w.cl/ic 1•t•ranc•s. •·O-, 111111~1. sarn/JM .,,~s;,;, '""°'U/
Preliminary Assesment.
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EPA FOAM 2070-13 (7•81)
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION REPORT o NC ATE I of) s,~~~MBJ~ 5 932 PART 8 · OPERATOR INFORMATION I II. CURRENT OPERA TOR (Pro>'kJ• ,r dlfl•~•nt from o•n•r/ OPERA TOR'S PARENT COMPANY /If app"Cllble} 01NAME 02 O+BNUMBER 10NAME I" O+BNUMOEA Same as owner. I 03 STREET ADDRESS (P.O. Bo•. RFD I, •tc.J 104 SIC CODE 12 STREET ADDRESS (P.0 Box. RFDI, etc.} r3SICCOOE
OS CITY 06STATE 07 ZIP CODE 14CITY 1'5STATTB ZIP CODE I
08 YEARS OF OPERATION I 09 NAME OF OWNER
I Ill. PREVIOUS OPERATOR(S) /L/$/mo,r ,.,m,r first; pro,,;,,• only lldlfl•r•nt from own•rJ PREVIOUS OPERATORS' PARENT COMPANIES flfaJ;lf>lkabioJ 01NAME 02 O+B NUMBER 10NAME r 1 D+B NUMBER FCX, Inc. I 03STREET ADDRESS fP.O. Box, RFDI. •lc.J r◄ SIC CODE 12 STREET ADDRESS /P.O. Box. FIFD1,etc.J 113 SJCCODE 609 St. Marys Street
05CITY 06STATE 07 ZIP CODE 14CITY I'S STATE I 16ZIPCO0E Raleigh NC 27602 I
08 '!'EARS OF OPERATION I 09 NAME OF OWNER DURING THIS PERIOD
1 o,c;_ 1 nee 1'Y'Y Tnr-
01 NAME 02 D+B NUMBER 10NAME I" O+BNUMBEA
03STREET ADDRESSrP.O Box. RFDI. •le.} l°'SICCOOE 12 STREET ADDRESS /P.O. Boi, RFDI. •tc.J 1'3 SIC CODE
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I 05 CITY 06STATE 07 ZIP CODE 14CITY 115 STATE I 16 ZIP CODE.
08 YEARS OF OPERATION I 09 NAME. OF OWNER DURING THIS PERIOD I
01NAME 02 D+B NUMBER 10NAME · ·,11D+BNUMBER I 03 STREET ADDRESS(P.O. Soi. RFDI. •tc./ IO◄SICCOOE 12 STREET ADDRESS (P.O. Bo•, RFDI • .ic,J I" SIC CO.OE
05CITY 06 STATE 07 ZIP CODE 14CITY r 5 STATE I 16 ZIP CODE I
08 YEARS OF OPERATION I 09 NAME OF O.WNER DURING THIS PERIOD I IV. SOURCES OF INFORMATION (C/lu :fpeclflc ,.,.,_.,•~. ·•·11'·, •t•t• f#H, •~ ,nalysJ•, r•pOl'lsJ
Preliminary Assesment. I
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EPA FORM 2070•13 (7-81)
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION REPORT °Ni:! ATEl 'B SllfB'J'.M'W) 5 932
PART 9 • GENERATOR/TRANSPORTER INFORMATION
II. ON-SITE GENERATOR
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01NAME 02 O+B NUMBER
FCX, Inc.
03 STREET ADDRESS /P.O. 8ox. RFDII, •tc./ I 04 SIC CODE
609 St. Ma.rvs Street
05CITY r• STATE OT ZIPCOOE
Raleigh NC 27602
I Ill. OFF-SITE GENERATOR(S)
01 NAME 02 D+B NUMBER 01NAME 02 D+B NUMBER
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03 STREET ADDRESS fP.O. Bo•. RFD II, •tc./ 104 SIC CODE 03 STREET ADDRESS /P.O. Box, RFD•. •IC./ 04SICCODE
OS CITY 106 STATE 07 ZIP CODE 05 CITY 1°6STATE 07 ZIP CODE
01NAME 02 O+B NUMBER 01NAME 02 O+B NUMBER
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03 STREET ADDRESS (P.O Box, RFDII, etc./ . I04SICCOOE 03 STREET ADDRESS /P.O. Bo•, RFD#, •tc./ 04 SIC CODE
OS CITY I06STATE 07 ZIP CODE 05 CITY 1°6STATE 07ZtPCODE
IV. TRANSPORTER(S)
01NAME . 02 D+B NUMBER 01NAME 02 D+B NUMBER
I 03 STREET ADDRESS /P.O. Bo•. RFD 11. etc./ IO.• SIC COOE 03 smeer ADDRESS (P.O. Bo•. RFDII, •tc.} 04SICCOOE
05 CITY I06STATE 07 ZIP CODE OS CITY 1°6 STATE 07 ZIP CODE
01NAME 02 D+B NUMBER 01NAME 02 D+B NUMBER
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03 STREET ADDRESS {P.O. SOI. RFD,. •rt:./ I0◄8_1CCODE 03 STREET ADDRESS /P.O. 8oI, RFOI • .rt:./ 04 SIC CODE
.. •· -.
05CITY r6STATE 07 ZIP CODE OS CITY l06STATE 07 ZIP CODE
V. SOURCES OF INFORMATION ,c11eat1e1:lflc,.r•""""· e.a .. 11111 ,,.,. •~•,,.'r$11. repa,tsJ
I Preliminary Assesment.
Reference 5
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EPA FORM 2070•13 (7:81)
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION oEPA SITE INSPECTION REPORT ouc'TEI Of> ~s"I'""4~ s 932 PART 10-PAST RESPONSE ACTIVITIES
II. PAST RESPONSE ACTIVITIES
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01 0 A. WATER SUPPLY CLOSED 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 8. TEMPORARY WATER SUPPLY PROVIDED 02 DATE 03AGENCY 04 DESCRIPTION
I 01 0 C. PERMANENT WATER SUPPLY PROVIDED 02 DATE 03AGENCY 04 DESCRIPTION
01 0 0. SPILLED MATERIAL REMOVED 02 DATE 03AGENCY I 04 DESCRIPTION
01 0 E. CONTAMINATED SOIL REMOVED 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 F. WASTE REPACKAGED 020ATE OJ AGENCY 04 DESCRIPTION I
01 0 G. WASTE DISPOSED ELSEWHERE 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 H. ON SITE BURIAL 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 I. IN SITU CHEMICAL TREATMENT 02DATE 03AGE~CY 04 DESCRIPTION
. I 01 0 J. IN SITU BIOLOGICAL TREATMENT 02 DATE 03AGENCY 04 DESCRIPTION
01 D K. IN SITU PHYSICAL TREATMENT 02 DATE 03AGENCY I 04 DESCRIPTION
01 0 L. ENCAPSULATION 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 M. EMERGENCY WAtiTE TREATMENT 02 DATE 03AGENCY 04 DESCRIPTION . I
01 0 N. CUTOFF WALLS 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 0. EMERGENCY DIKING/SURFACE WATER DIVERSION 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 P. CUTOFF TRENCHES/SUMP 02 DATE 03AGENCY 04 DESCRIPTION I
01 0 0. SUBSURFACE CUTOFF WALL 02 DATE 03AGENCY 04 DESCRIPTION
EPA FOAM 2070-13(7-81) I
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I POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION &EPA SITE INSPECTION REPORT 01 STATE! 02 SITE IT'".!" . NC D 98 75 932 PART 10-PAST RESPONSE ACTIVITIES
II PAST RESPONSE ACTIVITIESic.,,.,_,,
01 0 A. BARRIER WALLS CONSTRUCTED 02 DATE 03AGENCY 04 DESCRIPTION
I 01 0 S. CAPPING/COVERING 02 DATE 03AGENCY
04 DESCRIPTION
01 0 T. BULK TANKAGE REPAIRED 02 DATE 03AGENCY
I 04 DESCRIPTION
01 0 U.GROUTCURTAINCONSTRUCTED 02 DATE 03AGENCY 04 DESCRIPTION
I 01 0 V. BOTTOM SEALED 02 OATE 03AqENCY 04 DESCRIPTION
I 01 0 W. GAS CONTROL
04 DESCRIPTION 02 DATE 03 AGENCY
I O 1 D X. FJRE CONTROL 02 DATE 03AGENCY
04 DESCRIPTION
I 01 0 Y. LEACHATE TREATMENT 02 DATE 03AGENCY 04 DESCRIPTION
I 01 0 Z. AREA EVACUATED
04 DESCRIPTION 02 DATE 03 AGENCY
01 0 1 . ACCESS TO SITE RESTRICTED 02 DATE 03 AGENCY
04 DESCAJPTION
01 0 2. POPULATION RELOCATED 02 DATE 03AGENCY
04 DESCRIPTION
D .
01 0 3. OTHER REMEDIAL ACTIVITIES 02 DATE 03AGENCY 04 DESCRIPTION
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Ill. SOURCES OF INFORMATION IOI• w•cdlc ,ar•r•ncH. • g., tr•la 1'H, ump/• .,,., •• is. ••porU/
Reference 20
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EPA FORM 2070•13(7 61)
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POTENTIAL HAZARDOUS WASTE SITE I. IDENTIFICATION oEPA SITE INSPECTION REPORT 01 STATE! 02 SITE NUMBER NC D 981 475 PART 11 • ENFORCEMENT INFORMATION
II. ENFORCEMENT INFORMATION
01 PAST REGULATORY/ENFORCEMENT ACTION D YES GNO
02 DESCRIPTION OF FEDERAL. STATE, LOCAL REGULATORY/ENFORCEMENT ACTION
None Known.
Ill. SOURCES Of INFORMA TIQN (C11e specilic references, t1.Q, st•te l#~s. umphl .,,,1ys,s. rePOrlsJ
Preliminary Assesment.
EPA FORM 2070•13 {7•81)
932
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Appendix E
site Safety Plan
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TO: File
FROM:
RE:
Mary Giguere 'N\6
FCX Washington
NC D981475932
Addition to Site Safety Plan
Grover Nicholson and Pat DeRosa are returning to this site to collect
process water well and drinking water well samples. These are the only
samples that are being collected. The samples can be taken by personnel
wearing Level D protection. Goggles and gloves will be worn when preparing
sample containers and collecting preserved samples.
MG/tb/0354b
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Facility Description: Size 8 acres Buildings one
Disposal Methods Being Investigated burial of waste prod'_u_c7ts'-"'-a-n~dr--:-s-u~rf'a~c~e,--
contamination.
Unusual Features on Site (dike integrity, power lines, terrain etc.):
A 12' x 250' trench 3' above groundwater.
History of the Site: This site was a farm distribution center for pesticies,
herbicides and tobacco products. These products were handled from late 1945 to
1985. In 1970 some toxic wastes were buried in a trench 12' x 250' x 10'
on-site. Statesville FCX listed these pesticides as being packaged on site:
DDE, DDT, Chlordane, Malathion, Aldrin, Heptachlor and tobacco spray. A nearby
well has shown potential contamination with methylene chloride, carbon
disulfide, dichloroethane, dichloroethene, methyl ethyl ketone,
tetrachloroethane, acetone, and toluene in low ppb range.
C. HAZARD EVALUATION
The exact location of the trench is known, and there is no need to sample the
trench. Pesticides have low vapor pressure, but some of the pesticides that
could be present on site can be absorbed through the skin. The solvents found
in the nearby well are not common solvents to be used·for·farm chemical
fo11nulation; the probability that the source of the solvent contamination is
the FCX site is low. The location & tyPe of samples to be taken avoid the
areas of concentrated waste products: Most; if not all, of the sampling will
take place outdoors. Because of these reasons this site can be sampled in
Level D with special care paid to skin & eye protection. The HNu will be taken
i= readings of 5 to 20 ppm above background are measured respirators with
pesticide cartridges will be worn. If readings of greater than 20 ppm are
mea3ured the site will be vacated.
D. WORK PLAN INS'IRUCTION
Map or Sketch Attached? Yes
;•erimeter Identified? Yes
Command Post Identified? No
Zones of Contamination Identified? No
Personal Protective Equipment
Level of Protection ----=A ----'B ___ c X D
,~edifications Tyveks, rubber boots or boots with a tyvek cover, eye protection
and double PVC gloves will be used. If Level C is needed -respirators with
pesticide cartridges will be worn. Observers without respirators will stay at a
r.l.istance of at least 25 feet when respirators are in use. Observers who have
resp. with the correct cartridges may participate in all tyPes of sampling.
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TO:
FROM:
RE:
File
Mary Giguere ~
FCX Washington
NC D981475932
Sample Preservation
19 November 1986
Any well or ground water samples that are taken for volatile organic
analyses, that have no visible sediment, will be preserved with 4 drops of
hydrochloric (HCl) acid. Any well or ground water samples taken for metals,
that contain no visible sediment will be preserved with 3 ml of nitric acid.
If the pH of the metals sample is not less than 2, acid will be added until
the pH is less than 2 and greater than 1 (1 >pH< 2). Samples with 3 ml of
nitric acid will be marked with a check mark on the sample container cap. Any
sample with more than 3 ml of nitric acid will be labeled with the amount of
acid added.
Goggles and gloves will be worn while measuring acids and collecting
samples. Pasteur pipets will be used for measuring the hydrochloric acid.
These can been disposed of after rinsing. Graduated pipets will be used for
the nitric acid. These will be rinsed and returned to the equipment room.
Ma/tb/0354b
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TO: File
THROUGH: Lee Crosby
FROM:
RE:
Mary Giguere M0
FCX -Washington
Site Safety Plan
31 August 1986
NC D981475932
The site safety plan was modified on site by the sampling team. The
original safety plan did not include sampling of the material in the trench.
When the sampling team arrived the trench area had been uncovered exposing
some of the material that had been buried. This material was sampled. The
sampling was done by personnel wearing Tyvek suits, Tyvek booties or rubber
boots, and PVC gloves.
The material buried in the trench is thought to be pesticides,
herbicides, and/or outdated seed stock. For these substances, the protection
worn was adequate for the sampling that was done. The material had been
uncovered long enough for any substances that were to vaporize to have been
released; the HNu was used to survey the area. The HNu readings indicated
that there was not a respiratory hazard, therefore respirators were not used.
The gloves offered protection from the pesticides, herbicides, and seed stock
thought to be present.
This memo is being written to document the change made in the safety
plan. The changes made in the safety plan were reasonable and did not
endanger the health and safety of the sampling team.
LC/MG/tb/O21Ob
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SITE'. SAFETY PLAN
A: GENERAJ.: INFORMATION ' . ' .·• .· >· f ! .,i .
. Site; Name!~ FCX -Washington
.· . '·1; ,·• Location Grimes·Road
Site Number NC D981475932
Date 8/7/86
W;shington; Beaufort
• • ::;:;; d: "
C t Nc-oun y,
Purpose of°'Visit PA X SI ,\::~ ---Other ---
Proposed Dat'ei of Inspection __ 8"-'/-"2:..::6.:.../-"-86"--------·. , . . t ! ! :~~ .
Date of Bri
1
ering __ . ...::8,_/=.:15"-'/...::8:.:::6 ______ _
;• I t 1{; :/ 1
Priority Ranking .. • j' l . ---Low X Medium ___;:.;___; ___ High
Site Invesli~·ation Team
Personnel Responsibilities
Harry Holladay sampling
Grover Nicholson sampling
Steve Hall \, · observer
. ,'. ,~
· 1, r,: ,,f ~·
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PLAN PREPARATION:
Prepared By _:_·~M~a!L~.8.!:!!~:_~'.Y~'::!:/..__.l,.l_!!.ll;J,~~
.B. SITE/WASTE
Waste Type(s) X Liquid X Solid Gas __ Sludge ---
Characteristics Corrosive ___ _;Ignitable ·Radioactive ---Volatile ---X Toxic Reactive __ Other
List Known or Suspected Hazards (physical,chemical biological or radioactive)
on Site and their toxicological effects. Also, if known, list chemical amounts
HAZARD EFFECT(S)
Malathion TLV -10 mg/m (skin)
DDT, DDE, DDE TLV -1 m /m
Lindane & other isomers TLV • 5 mg/m (skin)
Chlordane TLV .5 mg/m (skin)
Aldrin, Dieldrin TLV -.25 mg/m (skin)
Heptachlor TLV -.5 mg/m (skin)
Endrin TLV .1 mg/m (skin)
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Surveillance; Equipment:
X · H Nu·. . Detector Tubes and Pumps
02 Meter I •' • ____ Explosimeter
· · · TLD >1 -.
••-~ I• (Radiation Monitor) ' . · :·t~ ~\· :·
Decontaminati'on·.Procedures . · . -Yf L1: !,. -
Level ._A\ lj•l. Segregated equipment drop, boot cover and glove wash, boot ---·_ ,j~)~ _: cover.and glove rinse, tape removal,. suit and hard hat, · · :;If.'.~.i; ' removal,· SCBA backpack removal, inner glove wash, inner ..
_ .. ~'\i:\;~ '. glove removal, inner clothing removal, field wash, redress . ••(•, ut ,{ , ' ,1,.,' i, ~ •
__ Level.'.Ji;1il . Segregated equipment drop, boot cover and glove wash, boot .:r,;,;1,'~ ' cover and glove rinse, tape removaL boot cover removal
j\(j[{ _-outer glo~e removal, suit/safety removal, SCBA backpack '.;.t·h · removal, inner glove wash, inner glove rinse, facepiece '.}l f~ -'. removal, inner glove removal, inner clothing removal; field ,Ji 1!i · wash, redress . . , .. ~ u I•~: ' •. , x · .· Level c'.: Segregated equipment drop, boot cover and glove wash, boot
' cover and glove rinse, tape removal; boot cover removal,
outer glove removal,suit/safety boot wash, suit/safety boot
rinse (Canister or Mask Change), safety boot removal, splash
·suit removal, inner glove wash, inner glove rinse; facepiece
. X
J{:,· · removal, inner glove removal; inner clothing removal. field
-•Uh· wash redress: ,, 1 rl::
"' ii Level;,_D}i .
:-!$-L;J, -
. " ·: 11,~
Segregated equipment drop. boot and glove wash, boot and
glove rinse .
Modifications ------------------------------
· _Work Schedule/ Limitations Sampling to be done: residential wells, surface . :,
soil and subsurface soil (not into trench), ditch sediment and background
soil.
I · l'MERGENCY PRECAUTIONS
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Exposure
e es
skin
inhalation
ingestion
First Aid
irrigate immediately
soap & water wash immediately
fresh air & artificial respiration
medical attention (see attached data
sheets)
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Hospital (Address and Phone Nwnber)
Beaufort County·Hospita1·
12 Street, Washington; NC
Bnergency Tr.ansportation Systems (Phone Numbers)
Fire use 911
Ambulance use 911· --==-=--=-=:.::__ ___________ _
t:.escue Squad -·-=u.::.se.::....:9:..:l::l=-------------
L111ergency l{oute to Hospital Get back on Hwy. 264 east, go through town;
11hen · 264 east bears to the right go to the left; the hosµi tal will be on your
left.
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PREVAILING WEATHER CONDITIONS ANlJ l:'ORECAST
, ..
X
1{,-1, . . . r , . . . . A1r pur1ty1ng respirator
----------------
X first Aid Kit
X Cartridges for respirator
3i,i 8710 Kespirator
(Pesticide) X 3 gal. Distilled H20
02 Indicator
Detector Tube ---& Ewnp
__;x:.:.· __ iye 1-iash Unit
X H Nu --'~----µH i,ieter
___ lixplosimeter
l{adioactive Monitor ---
A Personal Protective ---Clothing
X Boots or Boot Covers __;:.:.._ __ _x'-·--Coveralls (tyvek)
_A ___ Eye Protection
____ Hard Hat
X Decontamination _:..:..._ __
Materials.
Poison Control Center -State Coordinator
Duke University Medical Center
Telephone: [phone]
Box 3024
Durham, NC 27710
ASHEVILLE
704-1.55-4490
Western NC Poison
Control Center
Memorial Mission Hosp:
509 Biltmore Ave: 28801
CHAl{LOTIE Mercy Hospital
704-379-5827 2001 Vail Ave, 28207
DUllliAM Duke Univ iviedical Center
l-~00-672-1697 Box 3007, 27710
GiiliiNSBOKO Moses Cone Hospital
919-379-4105 · 12UO N. ilm St, 27420
l-!!OU-722-22.L.l.
HENDERSONVILLE
704-693-6522
&t:. 555; 556
HICKORY
704-322-6649
JACKSONVILLE
919-577-2555
WILMIHGTON
919-343-7046
Margaret R: Pardee
Memorial Hospital
Fleming st:, 28739
Catawba Mem: Hosp:
l:'airgrove Chur: l{d 28601
Onslow Mem: Hospital
Western Blvd. 28540
New Hanover Mem: Hospital
2131 S. 17th St, 28401 '
I
I HAZARDOUS SUBSTANCE INFORMATION FORM
0 I Common Name Aldrin Chemical Name __________ _
I I. PHYSICAL/CHEMICAL PROPERTIES
Reference
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Chemical l'onnula Cl2 H8 Cl6 --------------Nat_ u r al Pl1ys ical State at 25 °C crystals -'--'-'-_;_;__ ___ _
Vapor Pressure 7.5 x 10-4 mm Hg at 20°C
Melting Point 104 °F/@Boiling Point decomposes °F/°C
Flash Point (open or closed cup) N/A °C/°F
Solubility -H2o insoluble
Other very soluble in organic solvents·
1
1
1
2
2
1
1
I Physical Features:
. "ld chemical odor ( 2).
(odor, color, etc.) tan to dark brown solid with a
Formulations: emulsifiable concentrate, wettable I powder, granul,,s (l!'OG), dusts & dust concentrates, seed dressings, oil sol. (4)
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II. -TOXICOLOGtCAL DATA
3
Standards: 0.25 mg/m TLV 3 • 25 mg/m PEL 100 mg/m3 IDLH 4 ----
Routes of Exposure: Inhalation, skin absorption, ingestion
Acute/Chronic Symptoms: Acute: Renal damage, tremors, convulsions followed by
OIS depression, respiratory failure arid death.· Chronic: hepatic <lamage.
O1rst Aid: Eye: irrigate immediately, Skin: soap wash immediately ~---~------~----~-------~----~ I Inhalation: fresh air & artificial· resp. Ingestion: water and vomit (4).
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HAZARDOUS CHARACTERISTICS
.A. Combustibility Yes
Toxic by-products
Flammability
Explosivity
C. Reactivity Hazard
LFL
LEL
None
No
D. Corrosivity Hazard yes/~
Neutralizing agent:
E. ·Radioactive Hazard
Background yes~
Alpha particles yes,(§)
Beta particles yes@
Garmna radiation yes®
X
UFL
UEL
pi-I:----
Exposure Rate
IV. REFERENCES
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The Merck Index, 10th Edition,-1983,
Documentation of the TLV, 4th Edition, 1980.
Casarett and Doull's Toxicology, 2nd Edition, 1975.
NIOSH/OSHA Pocket Guide to Chemical Hazards, 1978,
Farm Chemicals Handbook 1982.
IG/3-86/Form 2
Reference
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b HAZARDOUS SUBSTANCE INFORMATION FORM
I Common Name Chiordane Chemical Name --'-'------'---------------------
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I. T'HYS ICAL/Cl-!f:MICAL PROPER TIPS
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I Chemical Formula _C_l_O_H_6_C_1_8_* ________ _
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Natural Physical State at 25°C _l_i~qu_i_d _____ _
Vapor Pressure 1 x 10-5 mm Hg at 20°C
Melting Point ____ °F/°C Boiling Point decomposes
.Flash Point (open or closed cup) N/A °C/°F · ----'-----
Solubility -Hz° insoluble
Other miscible with aliphatic & aromatic
solvents
Reference
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Of/OC 3
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. •· •· .· . Physical Features: (odor, color, etc.) viscous amber colored liquid ( 1).
_I.rt is odorless (2). Fonnulations: granules, dusts, wettable powder,
. emulsion concentrate and oil solutions. I
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11 Commercial product is a mixture containing 60 to 75% pure compound and
25 to 40% related compounds. Chlorine content 64 -67%.
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TOXICOLOGICAL DATA
3
.Standards: 0.5 mg/m TLV
. '3 .
0,5 mg/m PEL 500 mg/m 3 IDLH _3 __
'Routes of Exposure: inhalation, ingestion and skin absorption
1\.-,. ·,/Chronic Symptoms: Acute: irritating to skin, irritability, convulsions~
. ~ ,j :c:p depression. Chronic: li.ver damage possible (1),
I ,·u-st Aid: Eye: irrigate immediately. Skin: soap wash immediately.
I Inhalation: Fresh air and artificial resp,
I III. HAZARDOUS CHARACTERISTICS
Reference
I
A. Combustibility Yes
Toxic by-products
-~ .... B. :Flammability I··. Explosi.•.·ity
LFL
. LEL
No X
Ingestion: vomit (3).
UFL
UEL
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C. Reactivity Hazard stabile in alkaline conditions
I IV.
D. Corrosi.vity Hazard yes~
Neutralizing agent:
E. Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
REFERENCES
yesG)
yesei
yes~-
yes@
The Merck Index, 10th Edition, 1983.
pH:
Exposure Rate
Documentation of the TLV, 4th Edition, 1980.
NIOSH/OSHA Pocket Guide to Chemical Hazards, 1978. I Farm Chemicals Handbook 1982.
MG/3-86/Form 2
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~ HAZARDOUS SUBSTANCE INFORMATION FORM
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Common Name DDT & Derivatives Chemical Name -----------
:"JI\YSICAL/CHl:)IICAL PROPERTIES
Reference
Chemical Formula Cl4 H9 ClS 1 --------------
Natural Physical State at 25°C ~S_o_l~id _____ _ 1
Vapor Pressure 1,5 x 10-7 mm Hg at 20°C 1
Melting Point ...,..gg °F/Voiling Point decomposes °F/°C 1,2
Flash Point (open or closed cup) N/A °C/°F 3
Solubility -H2o insoluble 1
Other 78 g/100 ml benzene 1
I C,
I Physical F1.,atures: (odor, color, etc.) colorless to white to slightly
off-whit'e powder with a slightly aromatic odor. Formulations: aerosols,
I dusts, solution,;, wettable powders·, emulsifiable concentrates and granular,
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II. TOXICOLOGICAL DATA
3
Standards: 1 mg/m TLV
3
1 mg/m PEL N/A IDLH ---------
Routes ·of Exposure: inhalation, ingestion,.poor dermal absorption
I Acute/Chronic Symptoms: Acute:· tremors of head and neck, convulsions, cardiac
or respiratory failure. Chronic: hepatic damage, CNS degeneration, dermatitis
I C)'eakness, con vu ls ions.
I First Aid: Eyes: irrigate immediately. Skin: soap wash immediately,
• --__ .J ~-+-~t;,,..;,.,,, -r~c:n_ Tno~c;tion: water, vomit.
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I · III. HAZARDOUS CHARACTERISTICS
'O I . A. Combustibility Yes
Toxic _by-products
Flamrnabi.lity
Explosivity
LFL
LEL
No X --
UFL
UEL
C, Reactivity Hazard DDT is incompatible with alkaline
materials and strong oxidizers,
D. Corrosivity Hazard yes€) pH: ----
·1 -0
Neutralizing agent:
,,
E. ·Radioactive Hazard
Background
Alpha particles
Beta particles
Gamma radiation
Exposure Rate
IV. REFERENCES
The Merck Index, 105th Edition, 1983.
NIOSH/OSHA Pocket Guide to 01.emic.al Hazards, 1978,
Documentation of the TLV, 4th Edition, 1980.
Farm 01.emicals Handbook, 1982.
MG/3-86/Form 2
Reference
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lo HAZARDOUS SUBSTANCE INFORMATION FORM
I Common Name _D_i_el_d_r_i_n _________ Chemical Name __________ _
I I., PHYSICAL/Cl-~ICAL PROPERTIES
Reference
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Ch,,mical Furmula C12 H8 C16 0 --------------Natural Physical State at 25°C solid, crystals
Vapor Pressure 3.1 x 10-6 mm Hg at 20°C
Melting Point 176-177 °Ft{:s)Boiling Point decomposes
Flash Point (open or closed cup) N/A °C/°F ---'------
Solubility
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op;oc 1, 2
3
1 -H2o insoluble
Other moderate sol. in common organic solvents · _.::l ___ _
Physical Features: (odor, color, etc.) light brown, nonflammable solid. 1, ~ flakes at 25°C ( 2) mild chemical odor ( 3). Formulations: wettable
. ··· owder-emulsifiable concentrate, dusts, . ranules seed drsgs. solutions (4).
I II.
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TOX1COLOGICAL DATA
3
Standards: 0.25 mg/m TLV 3 0.25 mg/m PEL 450 mg/m3 IDLH _3 __ _
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1 Routes of Exposure: skin absorption, inhalation, and ingestion
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Acute/Chronic Symptoms: Acute: hYPerirritability, convulsions, and/or coma,
sometimes accompanied by nausea, vomiting and headache. Chronic: fainting,
muscle ·spasms, tremors and loss of weight (2).
F i rs t Aid : ;:E:.t..y.::e..:.: _:i:..:r:.:r..:i<z.g::.a t::.e::._:i:::m:.:m:.::e::.d::.i a::.t:..:e:.:l:LY..:.• _:S:.:k..:.i:.:.n:..::_· ::.s o:.:a:.tP:....::w.::a.::.s h:.:.....:i:.:.mm=e=d..:.i ::.a t::.e:..:l:,.Y..:.• ____ _
Inhalation: fresh air and artificial resp, Ingest ion: water, vomit ( 3).
19
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'III. HAZARDOUS CHARACTERISTICS
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A, Combustibility Yes
Toxic by-products
f'lammabi:'. lty
Explosivi.ty
LFL
LEL
No X
UFL
UEL
C, Reactivity Hazard concentrated mineral acids
catalysts, acid oxidizing agents, phenols & active metals.
D. Corrosivity Hazard yee) pH: ___ _
Neutralizing agent:
E, ' Radioactive Hazard
Background
Alpha particles
Beta particles
Gannna radiation
REFERENCES
yes/€)
yes~
yes~
ye~
The Merck Index, 10th Edition, 1983.
Exposure Rate
Documentation of the nv, 4th Edition, 1980.
NIOSH/OSfl~ Pocket Guide to Chemical Hazards, 1978.
Farm Chemicals Handbook, 1982,
flG/3-86/Form 2
Reference
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~ HAZARDOUS SUBSTANCE INFORMATION FORM
I Common Name Endrin Chemical Name
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i'l li'S TCAL/CHl:~fICAL PROPERTIES
Reference
Chemical Fonnula ClZ H8 Cl60 1 -----Natural Physical State at 25°C Solid 1 -----Vapor Pressure 2 x 10-7 mm Hg at_ 20°C __ l ___ _
Melting Point decomposes°F/°C Boiling Point _____ °F/°C -~l~----
Flash Point (open or closed cup) N/A °C/°F 1
Solubility -H20 ___ _
Other moderately soluble in benzene, xylene,
carbon tetrachloride and hexane.
-----
1
2
1 · · Physical Fc,:tures: (odor, color,
· a mild chemical odor. Fonnulat ions:
etc.) cream to light tan in color with
emulsifiable concentrate wettable I powde_r, dust & dust concentrate ( 3).
TOXICOLOGICAL DATA
I
3 Standards: .1 mg/m TLV 3 ,1 mg/m PEL ..3 200. mg /m IDLH 1 ----
I Routes of Exposure:
e osure. ·
Inhalation and skin absorption are major route of
I
Acute/Chronic s·ymptoms: Acute: renal damage, tremors, convulsions, followed by I CNS depress ion. Chronic: 1 i ver damage.
I)
First Aid: Eye: irrigate immediately:
Inhalation: fresh air & artificial res
soap wash immedi•ately.
I~ estion: immediate medical attent.
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~II. HAZARDOUS CHARACTERISTICS
.A. Combustibility Yes
. --I No
Toxic by-products
Flammability
Explosivity
LFL N/A
LEL N/A
X
UFL -----
UEL ------
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I C. Reactivity Hazard strong oxidizers and in presence of
1acids rearranges to less insecticidal derivative.
I D. Corrosivity Hazard yes9 pH: ----
-~. Neutralizing agent:· ________________ _
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E. · Radioactive Hazard Exposure Rate
BackgTound yes.@)
Alpha particles yes/@
Beta particles yes@
Gamma radiation yes€)
REFERENCES
NIOSH Pocket Guide to Chemical· Hazards, 1985.
Merck Index, 10th Edition; 1983.,
Farm Chemkals Handbook, 1982.
I MG/3-86/Form 2
Reference
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1,3
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0 HAZARDOUS SUBSTANCE INFORMATION FORM
Common Name _H_e._pa-'-t_cc..h_l_o_r ________ Chemical Name __________ _
I, PHYSICAL/CHFMICAL PROPERTIES
Chemical Formula ..:C:.::.1.::.0...:.H..::5:_::C.::.17'-----------
Natural Physical State at 25°C ~s~o-=-1-=-id"-------
Vapor Pressure 3 x 10-4 mm Hg at 20°C
Melting Point 95-96 °F/©oiling Point 135-145 °F/°C
Flash Point (open or closed cup) N/A °C/°F
Solubility -HO insoluble 2 .
Other slightly soluble in acetone, benzene,
hexane and xylene.
Reference
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3
2
2
1.o
I Physical Features: (odor, color, etc.) white or light tan,
non-combustible, waxy solid with a mild odor like camphor. Formulation:
I dust, dust concentrate, emulsifiable cone., wettable powder, oil solution (4)
II. TOXICOLOGICAL DATA
3 · Standards: O. 5 mg/m TLV .3 0. 5 mg/m PEL 100 mg/m:5' IDLH _3;___
Routes ·of Exposure: skin, inhalation and ingestion
Acute/Chronic Symptoms: Acute: stimulates CNS; <lepression and paralysis may
follow, Chronic: liver damage possible (1) •.
CD First Aid: E es: irri ate immediatel·. Skin: soa wash immediatel •
Inhalation: fresh air & artificial resp. Ingestion: water and vomit 3 .
•• l>II.
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HAZARDOUS CHARACTERISTICS
A. Combustibility Yes __ No X
Toxic by-products
FlammabU i ty
Explosivity
LFL
LEL
UFL
UEL
c. Reactivity Hazard melted heptachlor with iron
rust (3).
D. Corrosivity Hazard pH: ----
Neutralizing agent:
E. ·Radioactive Hazard Exposure Rate
Background yes@
Alpha particles yes@
Beta particles yes~
Garrnna radiation yes no
REFERENCES
I
The Merck Index, 10th Edition,. 1983.
Documentation of the TLV, 4th Edition, 1980.
NIOSH/OSHA Pocket Guide to Chemical Hazards, 1978.
Fann Chemicals Handbook 1982.
IIG/3-86/Form 2
Reference
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r:-. v HAZARDOUS SUBSTANCE INFORMATION FORM
Common Name _L~in~d_a~n~e __________ Chemical Name -◊'d--_B_H_C ______ _
L 1'!-!YS ICAL/CHB-HCAL PROPERTIES I Referenu,
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Chemical Formula C6 H6 Cl6 .=..:.___:_:c:__::.::...:. _________ _ 1
Natural Physical State at 25°C ~s~o~l~id'------1
Vapor Pressure 9. S x 10-6 mm Hg at 20°C 1 -----
Melting Point 112.S °F/°C Boiling Point. decomposes °F/°C __ 2 ___ _
Flash Point (open or closed cup) N/A °C/°F 2 -----
Solubility -H2o insoluble _l ____ _
Other soluble in acetone, benzene, ethanol, _l ___ _
ether
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Physical. Features: (odor, color, etc.) white crystalline substance with
a slightly musty odor (3). Formulation: emulsifiable concentrate, wettable
powde_r, oil-base sprays, granules, dusts, aerosols, smoke generator.
II. TOXICOLOGICAL DATA
2 Standards: 0.5 mg/m TLV 3 O.S mg/m PEL 3 1000 mg/m IDLH
Routes of Exposure: skin absorption, inhalation and ingestion (3).
3 ----
Acute/Chronic Symptoms: Acute: dizziness, headache, nausea, vomiting, diarrhea
tremors, convulsions, circulatory collapse. Chronic: local sensitivity, EEG
disturbances and possible liver damage. Suspect carcinogen.
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First Aid: Eyes: irrigate immediately. Skin: soap wash immediately
Inhalation: fresh ai.r & artificial resp. Ingestion: water and vomit (3).
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,II. HAZARDOUS CHARACTERISTICS
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.A. Combustibility Yes __ No x·
Toxic by-products
Flammability
Explosi vity
LFL
LEL
I C, Reactivity Hazard
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D. Corrosivity Hazard
Neutralizing agent:
E. 'Radioacti.ve Hazard
Background yes<[;;)
Alpha particles yes!o
Beta particles yes no
Gamma radiation yes no
REFERENCES
The Merck Index, 10th Edition, 1983.
pH:
UFL
UEL
Exposure Rate
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NIOSH/OSHA Pocket Guide to Chemical Hazards, 1978,
Documentation of the nv, 4th Edition, 1980.
Fann .Chemicals Handbook, 1982.
IMG/3-86/Fonn 2
Reference
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0 HAZARDOUS SUBSTANCE INFORMATION FOR.1.1
Common Name Malathion Chemical Name :.=.::..:::..::::..:c::..::..:c:__________ -----------
21-!YSICA.L/CHEMICA.L PROPERTIES
Reference
O1emical Formula Cl0 Hl9 06 PS2 1 -----
Natural Physical State at 2S°C liquid __ 1 ___ _
Vapor Pressure 4 x 10-S mm Hg at 20°C -~2 ___ _
Melting Point 2.9 °F/~Boiling Point 1S6 °F@_2 ___ _
Flash Point (open or closed cup) N/A °C/°F _l ___ _
Solubility -H20 14S ppm
Other miscible with many organic solvents
If o ... ' i . . .
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Physical. Features: (odor, color, etc.) clear to amber liquid with a
garlic oaor (3), skunk-like odor (1). Formulations: emulsifiable concentrate,
wettable powder, dust, ULV concentrate (3).
II. TOXICOLOGICAL DATA
3 Standards: 10 mg/m TLV .3 1S mg/m PEL
Routes of Exposure: inhalation and ingestion
S000 mg/m.3 IDLH 1 --'----
Acute/Chronic Symptoms: Acute: cholinesterase. inhibitor -nausea, vomiting,
diarrhea, excessive salivation, bronchoconstriction, muscle twitching,
convulsion, respiratory failure.
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i First Aid: Eye: irrigate immediately. Skin: soap and water wash,
1 Inhalation: fresh air & artificial resp. Ingestion: medical attention.
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dII. HAZARDOUS CHARACTERISTICS
A. Combustibility Yes __ No
Toxic by-products
n. Fla111,nabil i ty
Explosivity
LFL
LEL
X
C. Reactivity Hazard strong oxidizers
D. Corrosivity Hazard pH:
Neutralizing ageht:
E. ·Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV •. REFERENCES
UFL
UEL
Exposure Rate
NIOSH Pocket Guide to Chemical Hazards, 1985.
The Merck Index, 10th Edition, 1983,
Fann Chemicals Handbook; 1982.
MG/3-86/Fonn 2
Reference
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HAZARDOUS SUBSTANCE INFORMATION FORM
1 Common Name _T_o_xa~p_h_e_n_e _________ Chemical Name __________ _
PHYSICAL/GID1ICAL PROPERTIES
I :',d11ical Formula empirical formula: ClO HlO Cl8 *
·c<.tural Physi.cal State at 25°C solid
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--------
·._1:"por Pressure . 2 to • 4 mm Hg at 20°C
Melting Point 65 -90 °F/°C Boiling Point decomposes
Flash Point ( open or@gsed cupj) _2_7_5 ____ 0 c,@
Solubility -H20 insoluble
· Other freely sol. in aromatic solvents
Reference
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Of/OC 2
2
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Physical Features: (odor, color, etc.) amber, yellow waxy solid with a
ild odor of chlorine and cairrohor (pine odor) (1,2). Formulations:
emulsion concem:rates, wettao1e powders, d.usts (4'). 'LU% dust std. tonnulation I Emul. conc. 4 to 8 lbs/gal. · wettable powder 40%. Oil solutions -90% ( 4) •
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II. TOXICOLOGICAL DATA
. 3 Standards: 0.5 mg/m TLV 3 0. 5 mg/m PEL 200 mg/m3 IDLH 3 -=----
I Routes of Exposure: skin, inhalation, and ingestion.
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Tox!\rhene i.s ,7hlorinated C!\mphene. TI1ere are approximately 177 ClO
µolychloL·\nuL,,d dorlvc1tlvos la Tuxapht:nc. lt is 67-69i chlorine by weight.
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~lute/Chronic Symptoms: considered to have low toxicity in man (2), mild
..rrritation of skin, CNS stimulation with tremors, convulsions, and death. Has
used liver <lama · erimental animals. Listed as a carcinogen b EPA (1)
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1·11s1; Aid: Eyes: irrigate immediately. Skin: soap wash immediately, I' '.. 1 ,, · ic,r_. : __ f_re_·s_l_, __ a_i_r_&_a_r_t_i_f_ic_ia_l_r_e_s~p_. _I_n~g_e_st_1_· o_n_: __ wa_t_e_r_a_n_d_v_o_n_ii_t_( _3)_. __
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~::lillOUS CHJ\RACTERISTICS
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A. Combustibility Yes
Toxic by-products
B. Flammability
Explosivity
C. Reactivity Hazard
No X
LFL. ----LEL
corrosive to iron
UFL
UEL
D, · Corrosivity Hazard (Yey/no pH: ___ _
Neutralizing agent: ________________ _
E, Radioactive.Hazard
Background yes@
Alpha particles yes/e
Beta particles yes@
Gamma radiation yes®
REFERENCES
The Merck Index, 10th Edition, 1983.
Exposure Rate
Documentation of the TLV, 4th Edition, 1980.
NIOSH/OSHA Pocket Guide to· Chemical Hazards, 1978.
Farm Chemicals Handbook 1982.
1/3-86/Form 2
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,.. .(,, Ji ... 1 /)'rethroids.
. II . .
. Oq·. (Cll.1 J, .
CT CH,-0-C . , f ~ -CH
2 . . . 0 . 0 HC=C(C'/1 3),
Resmethrin
HI': Fairfield Amcricnn Corp. (Synthrin •) '.llilchel! Cot ts Chc111icnb Ltd, (Crear. Britnin)
/ltipkins Agricultural Chemical Co. (Resm cthrin 2.S%) l'enick Corpurnl lrrn (S/JP 1:J82 *, SDP 1382 *IBio-allethrin •)
.,.:tc,!or-see Gas rvlu:;k.
,,,,Q.
!.'HE~l/CAL COlvlPOSITION: A seed treatment consisting of a :1,1/Jlc dry-blend of moneb, hexcich/orobenzene, and captan with or ll"ithout inscct.icide.
ACTION: Seed protectant and disinfectant.
TOXICITY: Oral LDso (rat), 8000 mg/kg, Dermal LD,o > 1000 rng1kg.
SIGNAL WORD: CAUTION.
APPLICATIONS: Replacement of mercury seed dressings for control of seed-and soil-borne organisms attacking wheat, oats, burley, flax, rye, sorghum and milo.
F0HMULATIONS: Dust and slurry.
BP: PSI/Gordon Corp.
Restricted Use Pesticide
A pesticide which will be available fo_r purchase arid use only by certified pesticide appliculors. This group of pesticides will not be avniluble for use by the general public because of the very high toxicities ,md/or enVironmental hazards associated with these muteria!s.
Retard • -see Maleic Hy,(rnzide.
Retardants
A class of plant growth rt!gulmors useful especially in plant height control; especially in conimercinl greenhouse-grown floriculturnl crops.
Revenge• -see Dain pun~ .
RH-124 -sec Indar •.
RH-787 -see Vacor •.
RH-2161-see Sisthane •.
RH-2512 (Product discontinued by Rohm and Haas Co.)
ACTION: Preemergcnce herbicide.
:\P[JLICATION: For selective weed control in soybeans (ex-perimental registration).
flH-2915-see Oxyfluorfen.
f'!H-6201 -see Acit1uorfen.
Rhizoctol • (Product discontinued by Bayer AG, Federal Re-public of Germany)
CHEMICAL NAME: Methylarsinic sulfide.
I OTHER NAMES: Asozin •,MAS', Monk ii• WP, Urbasulf •.
ACTION: Fungicide, seed treatment.
TOXICITY: Acute oral LD5u (mt), 100 ing/kg; acute dermal LDso (rabbit), 1400 mg/kg.
I APPLICATlONS: Recommended chiefly for treating cotton seed; especially effective against Rhizoctonia solani.
FORMULATION: Dry seed dressing (6.2% elemental arsenic equivalent).
Active ingredient of Rhizoctol,.
Rhodanic Acid -see Rhodanine.
Rhodanine
CHEMICAL NAME: 2-Thioxo-4-thiazolidinonc.
OTHER NAME: Rhodanic acid.
ACTION: Fungicide.
Rhodax • -see Aliette •.
Rhodethanil
CHEMICAL NAME: 3-Chloro-4-(ethy!amino)phunyl thiocya~nte.
COrv1MON NAMES: rhodethonil (ISO); rodr.thw1i/ (Fr:m1:c).
ACTION: Herbicide.
Rhodia • -see 2,4-D:
Rhodiacide -sec Eth ion ♦•
NII-C,llo
Or
SCN
Rhodethanil.
Rhodiacuivre • -see Copper Oxychloride.
Rhodianebe -~ee Maneb ♦ •.
Rhodiatox • -sec Parathion ♦•
Rhodocide -see Eth ion+.
Rhomene • -see MCPA.
Rhonox • -see MCPA.
Rhothane •~see TDE + .
Ricetr·1ne • (California registrat\on only) ·
CHEMICAL COMPOSITION: Copper triethanolamine complex in liquid form. Chelated copper.
ACTION: Algicide, photosynthetic inhibitor.
CHEMICAL PROPERTIES: Dark blue-green liquid. Specific gravity 1.29 pH 7.7 ..
TOXICITY: Oral LD,o (rats), 0.50-2.00 ml/kg.
SIGNAL WORD: CAUTION.
ANTIDOTES: In c8se of.contact, flush contact with skin or eyes with plenty of water for at least 15 minutes. For eyes, get medical attention._May be harmful if swallowed, Do not induce vomiting. Give a glass of water and call a doctor immediately.
HANDLING AND STORAGE CAUTIONS: l(ecp out of reach of children, May cause skin damage. Do not ~cl on skin, eyes, or clothing. Conditions to avoid: Contamination wi~h acids.
APPLICATION: Prevents nnd controls u!gae growth in rice fields. Apply by aircraft or drip system. Trent at the first signs of algae growth. It is safe to enter the field immediately ufLcr treatment.
FORMULATION: 7.1% active, contains 0.76 l_bs. active/gal. as elemental copper from copP:er-triethnnolamine complex.
See Cutrine-Plus •.
BP: Applied Biochemists, Inc.
Ridomil •
CHEMICAL NAME: . N-(2,6-Dimethylpbcnyl)•N•(methoxy•
ucetyl)-alanine methyl ester. ·
COMMON NAME: '!'etaloxy/ ..
OTHER NAMES: Apron 2E, CGA 48988, Ridamil • 2E, Subdue 2E.
I Pesticide Dictionor" *-Indicates trade name. BP-Basic Producer. F-F'nrm1ilator. ,. -lnrlir11/"q """"''"'"" ,.,,•~•, ••• '' (• . .,.n:.,t r,.
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',., i·11·.,v11...:1\L !'\ t\!\·11•. · '..'.-H11:t llyl-~-\ m1:Ll1yltl1 iu) propi(Jnaldel1yd1: U-
{meLhylcarlrnmoyl) uxi!ll!:!.
COMMON NAME: uldicarb (ANSI, 13S1, ISO).
OTHER NAMES: O,HS 771 !WHO assigned no.), UC21149 (Union
Carbide).
ACTION: Systemic insecticide, S.caricide ond nemuticide for soi!
use.
Cl·IE~·iICAL PROPEHTIES: Technical aldicarb; white, crystalline
S(1lid; specific gravity. l.l~fi0 ut :25/2().lC; vapor_ pressure, l x 10-•
mm Hg at :25° C; solulJility in water 0.6% at ~50 C; non-corrosive to
common metals.and p!ustics.
TOXICITY:-Technical nldicarb; acute oral LDs11 (mt), 0.9 mg1 kg;
ur·Llte dermal LI)!,,,· frnlJIJit), > 5.0 mg/kg. Temik • lOG;
npprnximute oral L.!h, (ml), 7.0 mg/kg; acute dermal LD~o (rat),
dry: ~1UO-:J970 n1g1 kg.
:-:1c;:-::\L \\'OHO: D,\NGEIL
·'>n'IJ)O'l'E: A1ropir1c :,;u!fatc. Do not use opiates or cholinesterase
·'.l.ihi1 i11g ,lni::s.
. \JI.!~(;.,\;--_:!) s 1'!ll{.-\CE CAUTIONS: Do not. mix Ternih •
, sil,•s l'.'itli wat1ir ul' thl' re:;ultant :,;oluti1111 rnHy be :ll'riou:,;ly
·.',11,lw1s. Uo no! 1, .e :1pplic:nurs 1h11L will grind the grnnulcs.
,,:.:· l,Hig-sleeved ('l .. 1hi_1ii.: and protect,ive_glovcs when handling ..
\'::.~h h:inds and fnc1; i1elurc eating or smoking. Bnthc at the end o/
·:.ul'i; day, washing l'nlire Uody and hair with.soap and wut.er.
lhange contaminutt!I elothing dui!y and wash m strong washing
~odu solutmn and nnst: thoroughly before reusrng Store 111 a clean
dry and we\1-ventila!r:il i\ren.
APPLICATIONS: Ac·1:epted for use to control certairi insects, mites
and nematodes t!!l eottun, sugar beets, potatoes, peanuts,
ornamentals, .. sweet potatoes, oi'nnges, pecaris (S.E. only), dry
bcuns, soyl.wans, u11d sugarcune (Louisiana only). To l.Je used only
as n soil app!icution.
FOHMULATIONS: 10(;(, and 15% granules. Because of high
toxicitv of the part)nt compuund, only granules me offered, thus
signifiC!untly reducing handling hnwrds. · .
COM8!NATIONS: 'f'emik • cun be used Concurrently with many
pesticides. It is not affected b~ no,rma! fert!!izer upr!icat.ions;
however it should rll!l be applied 111 same !urrow with highly
alkaline/ forms. Do not use with lime or other highly alkaline
rnuterials, Temih • should not be mixed with other pesticides or
fenilizers prior to application.
CH 3
I ~ H
C! ,SCCH=NO<;N ( . . I CH,
Cl!,
A!dicar.b
BP: Union Curlii,i,, :\griculturu! Products Co., Inc.
Temporary Tolerance
A tolerance estnhli.,di,·d on an agriCultural commo.dity by EPA to
permit u pesticide m:111ufucturer or his agent time, usually one year,
to collect udditional residue dntu to suppurt u petition for a
permm1ent tolerance: in essence, an experimental tolerance.
Temus -see Hromadiolone •,
Tenoran • (Product discontinued in V.S.)
CHE!vl ICAL NAME: :l-jp-(p-chlorophenoxyl phenyl I -1, 1-
dimethylurea.
CO:vtMON NA!vlES: chluroxuron (ANSI, BS!, ISO, WSSA);
chluroxifenidim (USS/{).
OTHEH NA MRS: C-JfJR,'J (Ciba-Gei1,ty Ltd,), Norex • (dis-
co1itinued by NOH-Ai\·[ Agricultural huducts).
ACTION: Selective )wrhi('ic!e.
CHEfo..1ICAL PROPEH'l'IES: White crystals, melting point 149-
15(}.• C. Solubility :1 ppm in wutef; very soluble in acetone and
ch!oroform, only slightly in alcuhol and ei.her.
TOXICITY: For chluruxtiron technical: Acute oral LD~u (rut), 3700
mg/kg; acute dermal 1.1):,u (rabbit), greater than 10,000 mg/kg, Eye
irritution (rabbit). 11011-irrituting.
For Tenoran • SOW: A1:u1e oi'ul LD~l\ (rut), s:.no mg/kg.
SIGNAL WORD: CAUTION.
APPLICATIONS: Primarily for early postemergence control of
nnnual brondleaf weerl.s. !fogistered for postemergence use in
S(Jybcuns und celery; also for preemergence or pustemergence use on
~trawberries and curn,h.
Chloroxuron
BP: Ciba-Ge'igy Corp., Agriculturul Division
Ciba-Geigy Ltd. (Switzerland)
Tenox • tBP-2 Grain Preservative
CHEMICAL NAJ\-IE: lsobutvric acid, 59.ll-Gl.0% bv weight;
propionic acid, 39.0-.11.11,:;. \;y \Veii,;ln. ·
ACTION: Fungicide for pre.-.en•ing-high-moisturt'·l'lllltl'ttt g-r:1i1:
a storage period of on 1: _yl.:nr.
SIGNAL WORD: DA,\C:1-:II .
TOXICJTY CATEC:Ol{Y: Corrusive, cause:; V\'l· ;111d . :.111 d;u:
t'()mbustible Do not J'l.•use t•ll!pty rlru111: l{(:l11n, l!• d.
reconditioner or desaoy li.v pl'rfnr,ttini: ur cru~;hi11~ u11d buryini'. i11 .,
safe pluce nway from walr·r supplies. l{uliber gl1lves, rubber uprnn:;,
and rubber footweur, :md g-oggles ur t'atl! shil'ld should be worn.
Keep out of reach of childr1:n. Spillugl' should be nemi'alized with
sodium carbonate, sodiurn bicnrbonHte, chaH:, ur <.1gricultural lime
or washed awuy with plenty ufwuter. ·
ANTIDOTE: In case of contact, imrnedintely flush eyCs or skin with
plenty of water for at least 15 minutes while removing clothing and
shoes. Call physician. Wash clothing before reuse.
APPLICATION: T~nox • JHP-2 Grain Presf!ruatiue is suggested for
upplicalion (as directed on reJ,;istered lube!) immediately ufter
harvest to ·prevent fungnl growth in stored curn, milo, burle.v,
wheat, and oats.
BP: Eastman Chl!mical Products, Inc.
Tenox • P Grain Preservative
CHEMICAL NAME: Propionic acid.
COMtvlON NAME: propioni~ acid.
ACTION: Fungicide for preserving high-moisture-content grain.
SIGNAL WORD: DANGER.
TOXICITY: ~foderatelv 10xic for luborntory 11nimuls. Acute oral
LD1,11 is grCater thun 4(1\i rng/kg in ruts when udrninistered as a 1 s·;
s0lution in water. Intrnperitonca! LD,,11 for ruts is :Z00-,100 mg.'\q:.
Skin LO.~,. for rnbbits is U.fi ml/kg. .
ANTIDOTE: In case of contact, immediately flush eycis or skin with
plenty of water for at lenst 15 minutes while removing clothing and .
shoes. Cal! physician, Wash clothing before reuse.
HANDLING AND STOHAGE CAUTIONS: Must be stored or
disposed of in u munner th'nt will prevent contamination of water,
food, or feed. Spillage of Tenox I' should be neutralized ·with
sodium carbonate, sodium bicarbonate, chalk, or agricultural lime.
Unused product may be disposed of in R landfill approved fur
pesticides, incinernted, or buried in a safe pince nway from water
supplies.
APPLICATION:-A liquid chemical applied undiluted to freshly
harvested grain.by means of !ow-pressure sprny nozzles mounted to
cover the grain as it pus:jes through an auger-type applicator.
Grains treated with Tenox ]-'Dre corn, milo, barley, wheat, and oats.
Gruiri that has been treated with Tenox P is used exc!usi\·e!y for
livestock feeds.
BP: Eastman Chemical Products, Inc.
Tep a• .
CHEMICAL NAME: Trii,; ( 1-aziridinyl) phosi>hine oxide.
O'J'HE!l NAMES: Aphoxide, APO.
ACTION: In.Sect chemosteri!unt.
Tepllr0sia
, Genus of subtropical plunts from which rotenone is obtained,
largelY in. Old World nreas. Tephro.<;ia virginiana, native to the
southci.1stern U.S. from 'I'exus to Mnrylnnd nnd tu Mi,rnesotu in the
Mid west, contains small quantities of rotenone.
TEPP (Product discontinu·ed by Miller Chemicnl & Fertilizer
Corj1.)
CHEMICAL NAME: Tetruethyl diphosphate. (Also known as
tetruethyl pyrophosphate and ethyl pyrophosphute.)
COMMON NAME: 'l'El'l' WSI, ISOJ.
Pesticide Dictionarv *-1.ndicatcs trnde name. BP-Basic Producer. F-J<'ormu!atnr.
t -fnrlir-Alf•s r-nmmnn nHmP -"I N-~nPriAI I L,r11I N,,,,,l (' ?ll 1
i: r.,•· I". ·~ I· . , . .,:
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Fun go • 50 (Cont.)
COMBINATIONS: Available in combination with Truban • as the broad spectrum soil fungicide Banrot •; and with Zn, Mn, EBDC as the broad spectrum turf fungicide Duosan • .. ·
BP: Mallinckrodt, lnc.
Fungal• -see Wood.Pwservative,
Fungostop-see Zif am.·
Fun~us (plurnl: Fungi)
_.', :11•nd1lorophyll-bet1.ri1q.{ µlunt. Some fungi are able to infect and ~,:1.: ,. dist:Hs,is in plnnt:-l, nnimals, and mun. Oth1m-f can attnck nnd ' \',i•\' 1:,H1-l!vlng thing8 such us wood and fiber products. •il1::--{~r rli:;t'ase-l·a 1:;ing fungi: rusts, mildews, molds, smuts; •1.,".'<' rots :ind 511, lli11i-: blights. Fuugi cttusc many destructive ,I l:,L'dS,~3-
'. 1·'.'.·.1 !CAL NAME: '2,3-Dihydro-2,2-dimethyl-7-benzofuranyl · .;t:thyl1:i\fhamate.
,:U:.l"ION NAME: carbofuran (ANSI, BS!, ISO).
O'J'HEII NAMES: Bav 70/,/3, Curaterr •, D 1221, Ent 27164, FMC 10:2-12, NIA 10242, Yallox •.
ACTION: Broad spectrum carbamate insecticide, nematicide and miticide.
CHEMJCAL PROPEHT!ES: Technical carbofuran is an odorless, white, crystalline solid, melting at 150.1520 C. Specific gravity is 1.180 at 2()l/2Q:J C. VE1por rres::1Ure is 2 x lQ.6 mm Hg ot 330 C. Water solubility, 700 ppm ut 25(1 C. ·
TOXICITY: Oral LD,,(I (rat), 11 mi/kg; dermal LDbo (rabbit). lU,200 mg/kg.
SIGNAL WORD: IVAllNING, (Furodan Granules); DANGER, (Puradan 4 F!o'wable).
ANTIDOTE AND FJHST AID: If swallowed,· induce vomiting by l:iving·a tablespoonful of suit in a glass. of warm water. Repeat until vomitus is clear, Cull u physician immediately. (Some physicians may discourage use of snline emesis.)
1finha!ed, remove to fresh uir. Call a physician immediately.
To physician: Carbof1mm is a revei-sihle cholinestcnrne inhibitor. Du not use oximes :.,1ch ns 2·PAM. Give atropine 2 · mg intravenously or subc11· :rneously. lf in eye, instill one drop of _Homatropine.
HANDLING AND S'l'OHAGE CAUTIONS: When using Furodan .JF, go1rnles and a recom111e11ded mask or respirator should be worn to avoid exposure. N1it" r.he .,;pecific label warnings concerning hundling of granular.
APPLICATIONS: Mujor rei;istrations include field com to control corn rootworm and m(,:,t soil und foliar pests; alfalfa for alfalfa weevil, uphids ond lygu~ bugs; tobacco for nematodes and soil· and fuliuge feeding insects; rwunuts for nematodes and thrips; rice for rice water weevil; on sug-urcune for nematodes, wireworms and i;ugarcane borer; sorghum for greenbug; potatoes for Colorado pututo beetle, leafnopper.,;, and flea beetles, Future registrations are anticipated on soybeans, sweet com,· cotton, grapes, small grains, and a variety of other crops.
FOREIGN APPLICATIONS: Additional overseas uses include brurnnas, coffee, and sugar beets. Granules are used in lowland rice against leafiwppers, stem borers, and certain other insects.
FORMULATIONS: Granules (2, 3, 5, and 10%); flowable (4 pounds/gallon).•·
f :.-
1
--~cn,
Cli3 Ii \
I II\\
. 1!3C--N--C--O
0
Carbofuran
BP: FMC Cor·p., Agricultural Chemical ,Group (FMC 10242, Puradan •, NJA 10'242) F; Bayer AG (Federul Republic of 9-erm_any) (Curaterr • J
Mobuy Chemir.ul Corp., Agricultural Chemicals Division (.Furndan •)
Furalaxyl -see Fongarid •.
Furethrin . . . · . . •~\ CHEMICAL NAME: DL-3-(2-Furfuryl).4-hydroxy-2-methyl-2-\ '. c.yclopenten•~•On~ ester of DL•cis•troris.chrysanthemum \~ ,._ monocarboxyhc acid. . , \ COMMON NAME: furethrin. · · ~, ., ACTION: Insecticide. · ~" CHEMICAL PROPERTIES: A synthetic pyrethrin-like (pyrc-throid) (urfuryl derivative. First prepared in Japan.
APPLICATION: . Intended to be competitive ·with allethriri. Experiments showed a rapid knockdown of house flies. Furethrin did not go into commercial production.
See also Pyrethroids.
Furloe • -see C_hloro•IPC ".
Furmarin -see Fumnrin •.
Fusarex *
CHEMICAL NAME: l ,'2.,•I ,5-tetrachloro•3-nit rolnm:ene.
COMMON NAME: tecnas,,,, (BS!, ISO).
OTHERNAMES:Folosan ·, 'J'CNB (BnyerAG).
ACTION: F.ungicide and growth regi,.ilator.
CHEMICAL PROPERTIES: Colorless, odorless crystalline solid m.p,. 990 C, appreciably volutile at room temperature, insoluble in water, solubility in ethanol 40 g/1 at 250 C readily soluble in benzene, chloroform, carbon disulphide.
TOXICITY: Low mammalian toxicity. Acute oral LD~o (rat)::. 7500 mg/kg.
SIGNAL WORD: CAUTION.
APPLICATIONS: Control of dry rot in seed and ware potatoes; also prevents sprout development i~ storage.
FORMULATIONS: Dust containing 3% w/w tecnazene; Folosan • contains 5% W/w tecnazene.
COMBINATION: Y-BHC.
NO,.
Ci Cl
Cl Cl
Tecnazene
BP: JCI Plant Protection, Division (Great Britain) (Fusarex ~)
Fusilade •
CHEMICAL .NAME: butyl 2•14•(6-trifluoromethyl-2-pyridyl oxy). phenoxyj propionate.
COMMON NAME: fluazifop-butyl (proposed).
.ACTION: Herbicide. ·
CHEMICAL.PROPERTIES: Liquid, boiling point 17()l C (0.5mm Hg), soluble in most organic solvents.
TOXICITY: Acute oral LDoo (rat), 3000 mg/kg.
SIGNAL WORD: CAUTION.
APPLICATIONS: A new, highly active, selective herbicide for the postemergence control of both perennial and annual grass weeds in broadleaved crops."Fusilade • has been shown to be safe for use in over 60 annual and perennial broadleaved crops (agricultural, horticultur:Ul, orchard, and plantation crops) when used at over twice the rates reQuired for effective gra'ss control.
FORMULATIONS: Ou.tside U.S.A.: Fusilade *, 250 grams/liter; Fusi!ade • W, 250 grams/liter w!th added wetter. ·
BP: ICI Americas Inc., Agricultural Chemicals Div. ICI Plant Protection Division (Great Britain) Ishihara Sangyo Kaisha Ltd. (Japan)
Fussol • -see Fluoroacetamide.-
FW • 293 -see Dicofol t ; -
FW • 734 -see PrOpanil.
Fydulan G -see Cas~ron •. ·
Fydulex G _; see Casoron· •.
I
TOXICITY: Acute oral LD.~n {mt), 1000 mg/kg; acute dermal LD~o
(rabbit), 4100 mg:/kg. Malathion has been fed to rats for 104 weeks
I t level!> us high as 5000 ppm in the diet with no gross effects,
IGNAL \\'ORD: CAUTION.
ANTIDOTE: Atropine, PAivl, 2-PAr-.lCI, 2-PAr-.HvI, Toxogonin •
(ivlcrck).
I ANDLINC AND STOHAGE CAUTIONS: Harmful by
,·alloll'in1~. inhalation or skin contact. Avoid breathing: spray mist.
void contnct with skin. Wash thorouJ,:h!y after lrnndling. Change
eontuminated clothing. Do not contaminate food or fcctl products.
l·\PPLICATIONS: Malathion controls a wide variety of insects
ncluding: aphids, spider mites, scale insects, hoti"se fly, nnd
n,1sqt1i1rn'!-:is we!\ as o largc number of other sucking: and chewing
::1::t•.'1;; :.:1:1(:ki11g fruits, vegetables, ornamentals, nnd slorcd
pr<H!t:l'L· '.t:: w;,: i;; pmticu!nrly indicated where a high degree ·of
I.:·,• .. \ ,.. ,.:mm:ds is desin·d -•;1 tlllcrnncc of 1:l[l ppm for forngc,
, 1~ \iiiy allows mar'uthion to be applied (1n 1.he snme day
. • ,:"\"t'S!Cd.
v:,:1,hlishcd tolcn,:1ces ure for residiws of 8 ppm
Then~ are spcci:ilized uses with higher and lower I . ~·:!n/rahion is gener,dly compatible with n!! insecticides
· .11,:1, :dl•s in common usage. When mixed with alkaline
.. 1:11.--: ! l1i.! initial kills nm satisfactory but the residual toxicity
,,,,1_\' hl· reduct>d.
1"1Inlcithio11 UL V • ConcentrC/te contains !)l % 0, O-dimethyl S-(1,2
licarbethoxycthyl) phosphorodithionte and is registered for ultra-
ow volume ncrin! application lo ulfalfu, clover, pnsture nnd rnnge
grnsses, nonagricultural lnnd, cereal crops, cotton, snfflower,
soybeans, su!-{nr beets, corn, beuns, blueberries for the control of
l rnny insects nt rates of 4 Lo lG ounces per acre; olso npplied to beef
ut tie.
~_,·thion • or Fv/anon • or EmmatoR Extra• is a low-odor product
manufactured 1,y patented processes, and is availnhle for all uses of
malathion registered for all uses applicable to Malathion ULV • l,'onccntf"atc. In the United Stutes Lhis is the unly"i,.:rndc registered
ir use on stored grain, recommended for use inside homes, and
cccpted for use on humnns. . ·
FOHEIGN APPLICATIONS: Hilthion • is a broad spectrum
I. 1sc•cticide used for control of a variety of insect Pest::; of agriculture,
Hestrv, horticulture, nnd aninrnl and public health. It docs not
osc 1)roblems of residues wlicn used as recommended and is
relatively a less hazardous insecticide.
FOIU,1ULATIONS: Emulsifi:1ble concentrate, wettable powder,
lust., ULV concentrnte. Hiltf.i'ln • 25 WDP. Double-M • EC is a
1ixture with methoxychlor.
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(CH3 Ol,P--S-CH-C-OC2 H0
I rr
CH 2 -C-OC2 H0
Malathion •
BP: American Cyanamid Co .. (Cythion t, Malathion ULV *
Concentrate)
Cheminova (Denmnrk) (Fyfanon *)
C_vannmid India Ltd. (India) (Cythion •)
Cyanamid Quimica do Brasil Ltda. (Brazil) (Ma-
lathion•, Malatol +, Cythion ")
Cyanamid Taiwan Corp. (Taiwan) (Malathion*)
F::..t·,~l IndustriesLirni1ed (India) tCelthion +)
F:1r11wplnnt S.p.A. (~lontedison Group) (Maimed•)
Hindustan 1nsec1 icicles LL<l. (lndin) (Hilthion *,
Hilthiotl • 25 \VD/-')
i\-l/S Pesticides India (India) (Vc1:fru, Malatox)
Rhone-Poule\1C (France) (Calmathion, Malaph€/e, Sumi-
tox, Zithio/)
Sumitomo Chemical Co., Ltd. {Japnn) (MLT)
F: All India Medical Corp. (Ind in) (Mattox)
Devidnya! (Sales) Private Ltd. (India)
Hopkins Agricultural Chemical Co. (Double-M * EC,
Beef Cattle Oil) ·
Malathion• MLT-see Mo lath ion ♦,
lalathion ULV • Concentrate -see Malathion•.
Malatol • -sec Malathion• .
laldison • -see Malathion ♦,
Ct !bJ\llCAL NAMES. G-hydrux_,-0, .... ,
D1hydropyndaz1ne-3,G-dione. /. 1,). '"··· "?"' '/"' !,>·
COMMON NAME· MH (WSSA). .
TRIVIAL NAME: maleichydraz1de.
OTHER NAMES: Burtolm •, Chemform ,. , De-Cut •.~,)(,.sprout•,
Drexe/.Super P • (discontinued by Drexel), Fair 30, Fair /JS, KMH,
Maintain'" 3 · Maleic.Hydrazide 30% • (discontinued by Crystal
Chemical Co\ Malein §o •, MH-30 •, MH 36 Bayer (discontinued
by Bayer AG), ReKulox,. W, Regulox" 50W, Retard•, Ro_val MH-
30 .. , Royal Slo-Gro •, Slo-Gro •, Sprout-Stop •, Stu at-Man •,
Sucker-Stuff*, Super-De-Sprout ", Super Sprout Stop, Super
Sucker-Stuff•, Super Sucker-SW// HC, Vondalhyde ' (Pennwnlt
Holland), VondraX • (Pennwalt Hofland).
ACTION: Growth retardant.
CHEMICAL PROPERTIES: . Melting point 292" C. Solubility
(t.e<:h.) nt 25° C: water 0.6%, ethanol 0.1 %, DMF ~.4%.
TOXICITY: Both maleic hydrazide and its sodium s1dl hnvr. n low
order of toxicity. A<:utc orul LUr,u (rat). 6950 mg sodilllll !',a\ttkg; :-moo mJ.! dicthaliolum inc sul t/ki:.
SIGNAL WOHD: CAUTION .
ANTIDOTE: If swallowed, inducL• vomiting.
. APPLICATIONS: When sprayed on plants, it is ahsnrhl~d nnd
moves internally where it blod:s tell division. Ikspon.s~• to the
chemical often varies with the dos11ge and the st.ni;e · o( plant
development. . ·
Malcic hydrazide formulntions effectively control :stJch weeds in
turf and elsewhere as wild onion and wild garlic. Maldc hvdrozide
is recommended for the tempornry growth inhibi~inJi ol' various
trees, shrubs and grasses.and has also been· apptoved for use in
controlling the sprouting of edible· onions and pota1.rn!S in stornge.
Maleic hydrazide hus been effectively used to retard .sucker growth_
of tohncCo plunts and to protect citrus seedlings 11g11inst frost
damuge. ·
FORMULATIONS: Water-soluble liquids of the dieth:molamine
salt or lhe potassium salt; EC 300; EC 360 (Bayer AG). IHI* 43 (in
combination with 2,4~D) (Diamond Shamrock Agrochemicals
Ltd.). .
OH
I ,,,,.c' HC '-N I I . I
HC...._C,,,,-NH
II
0
Maleic Hydrazide
BP: Chemical Formulators. Inc. (Chemform ")
Diamond Shamrock Agrochemicals Lt.cl. (Great.
Britain) Wurtolin •, Regul_ox w•, Reguloxsow•) _
Drexel Ch.emical Co.' (Retard•, Sprout-Stop•,
Sucker-Stuff*, Super · Sprout Stop, Super
Sucker-Stuff•, Super Sucker:Stuff HC)
Fairmount Chemical Co., Inc. (De-Cut•, De-
Sprout •, Fair 30, Fair PS, Super De-Sprout •)
Nihon Nohynku Co., Ltd. (Japan) (Malein 30 •)
Uniroyal Chemical, Div. of Uniroyal, inc. (MH-
30 •, Royal MH-30', S/o-Gro ')
Maleic Hydrazide 30%-sec Maleic Hydruzi~e.
Malein 30 • -see Maleic Hydrazide.
Ma/ix·• -see Endosulfon.
Maimed -see Malathion ♦-
Malonoben * (Product discontinued by Gulf Oil Chemicn!s Co.)
OTHER NAME: GCP-5126.
ACTION: Acaricipe-insecticide.
Maloran • (Product has been discontinued in U.S.A.)
CHEMICAL NAME: 3-( 4-bromo-3-chlorophenyl). f-methoxy-1-
methy!urea.
COMMON NAMES: chlorbromuron (ANSJ, BS!, ISO, WSSA),
chlorobromuron (France).
OTHER NAMES: Bromex • (discontinued by NOR-AM
Agricultural Products), C6313 * (Cibn-Gei~y Ltd.).
ACTION: Selective herbicide.
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Neguvon • -see 'I'richlorfon + .
Nekal ~ Surfactants
CHEMICAL . NAME: BA, BX -Sodium alkylnap 1thal :ne
sulfonate. WT-Sulfonated aliphutic polyesters,
ACTJO~: Anionic wetting agents.
CHEMICAL PROPERTIES: BA, BX~ free flowing W'I'-aqueous solution,.
TOXICITY: JJJl.77: Acute oral LD5o, 1.35 g/kg; act.ite dermal LDbo,
•1,2 l{lkl{; ocular irritation, moderately irritating. BX.78: Acute oral
LD~o (rat), 1.5 g/kg; U~uinea pig), 1.5 g/kg.
APPLICATIONS: l\iekal • Bil-77 and !3X-78 are used as· wetting
111:ents fof insect.icida!" powders. Neka! • \VT-27 is used in wettable
puwders itnrl liquid fertilizers.
Set.! Dispersrmr.
!H': GAF C111·p., Chemirnl Products
Nekal • WT-27 -see Nckal •.
Nektaran
COM!\·ION NAt-.·11<:: nektaran.
OTHER NAM 1-:: /Jee Une.
ACTION: Nonpoisonous bee food attractant increases pollination,
crops of (ruit and seeds. ·
TOXICITY: None.
APPLICATIONS: NektarOn can be applied by airplane, con:
centrnted ground or full volume sprays. The dosar,:e rnte is 5 pounds
of Nehtaran per acre in any type of spray. For airplane~5-10gullons
of wnter per ucre. In r,:round sprays 100-150 g-11\lons of water per ucre, Muy also be applied with fungici~e spruy.· ·
Apply 2-3 applications per season, at early bloom, mid-bloom, and
late bloom, at 4-G day intervals, ·
HANDLING AND STORAGE CAUTJONS: Use only in cleun
spray equipuwnt. Do not apply with pesticides that are toxic to·
bees. Store in dry and cool place.
FORMULATION: Wettable powder.
F: Tamr,gan Ltd, {Israel) ·
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Nellite • (Product discontinued by The Dow Chemical Co.)
CHEMICAL NAME: PhenylN,N'-dimethyl phospho:odiamidate.
COMMON N1\\•lE: diamidfos.
ACTION: Ne111a1.icide.
CHEMICAL l'!WJ'ERTIES: White crystalline solid, very low
vapor pressur,·. ,\•ldt ing point, 105._5-lOGO C. Soluble in acetone,
chloroform, 1t:1:1.h,mol and mCthylene chloride; solubility in water is
40,000 ppm. · ·
TOXICITY: Atute om! LD~o (male rat),· 140 mg/kg. Acute dermal
LO5o {rabbit), 100-200 mg/kg. Sljght skin irritant. Toxicity to fish
and certain other aquatic animals is of a rel11tively low order. The
compound does not biouccumu!ate in aquatic food chain organisms.
SIGNAL WOJW: IVAllNJNG,.
APPLJCA1'IONS: Used ·on tobacco to control i-ootkl'lot nematodes.
Applied ii\ the transplunt wate~ at the time of planting.
FORMULATIONS: Ne/lite• 90; Ne/lite• WS.
Nemacur •
0 . 0 ,,.,,-NHCH,
II/ 0 p
-"-._NHCHi
Diamidfos
CHEMICAL NAME: Ethyl 3-methyl-4-(methylthio) phe•)YI (l-
H\l't hyh•t hyl \ ph,1::-phl,rnmi<lnte .
C,)_,l,\ON );A~\\•:: i,·11omiphos.
OTHER NAME: Boy 68138.
ACTION: Nenrnticide (systemic). .
CHEMICAL i'HOPEHTlES: Brown waxy solid; m.p. •19.2~C; v.p'.
ca lll-~ mb11r :ti ;i\P C; ~tnble under normal condition:; but subject rn
lwdn1l\'sis; ~.,\11\1\i• in 11h1::-t i..Hh:lllil· sul\'cnt:. und in wnll'r up to
nbout :100 1mm. ·
TOXlCl'I'Y: 'l'echnicnl: Acute oral LD~,11 (rm), 1-1.1-9.ll rng, lq;;
dermal LDsu (rut), 72-8·1 mg/kg.
ANTIDOTE: Administer atropine sulfate in large tlwrapeutic
doses. R.epeat ns necessary to the point of tolerance. 2-PA:\I nnd
Toxogonin ~ (Merck) nre also nntidotal and mny be administered in
conjynction with ntropine.
APPLICATIONS: A compound with high nematicidnl ncti\'iT.\'
which can·be applied broadcast, in-the-row, in band, b~· dr~11eh,
before or at pluming time, or to established plants. Cornp!ett• :;,ii!
\ncorporation is not essential.
Experimentnl results show it to he a liroud spe<:trn,n 1it•1n;1tic-i1\,:
with good plnnt tolerance to many field, vegetable, and fruiL l'WP"·
Presently reidstured for control of the mujor geucrn u!' 11L·1n:1t,.dc:;
attacking cotton, peanuts, soybeans, cabbage, Hrussc!s ,;p:·ti.:b,
bananas, turf ~rnsses, Emel non-benrinr-:-fruit trers in 111:!ic,\' i11:1;,1r
fruit producin~ slates. Currently under rcsearl·h in :m::1-. .,,·i•,·:",·
nematorles an: ;1 prnhlem.
For{MULATIUNS: Emulsifiahl,c C(JJ\<'.(:rltr:11,-I.Hi J'.f,
COMBINATJO0.'S: Nenwr.ur ~ + /J,,,.,.: ,u
cuncentrail' and gr;u1ul(:S.
Fenamiphos
BP: Bayer AG {Federal Republic of Germnny)
(Nemacur •)
Mobay Chemical Corp,, Ag-ricultural Chemicals
Division (Nemacur •)
Nemafene • -St!L' !).!) ~ Soi! Fumigunt.
Nemafos -see Zinophos •.
Nematume • -see Dibromochloropropone.
N~magon •-:--see Dibromochloroproprme. . .
Ne~an'ax ~ -see DiLromoch!oropropnnc.
Nemaphos • -see Zinophos *.
r,Jemaset •~sec Dibromochloropropune.
. Nern-A-Tak•.
CHEMICAL NAME: (Diethoxyphosph inylimino)-1,3-d ithie'tane.
COMMON NAME: fosthietnn (ANSI).
OTHER NAMES: ~\C 64,475, A econ em, CJ, 64,475, Gcofos.
ACTION: Soil nematicidc one! insecticide.
CHEMICAL PHOPERTlES: Technical Nem-A-Tak • is u slightly
turbid yel!ow liquid; solubi\ity in wntcr 5% w/w at 250 C; solubility > 90% in xylene, acetone, cyclohexononc, ~-propunol.
TOXICITY: Technicnl Nem-A-Tah •: ncute om! LD~·o (rut, mnlc),
4,7-7.7 mg/kg; (rat, female), 6.9 mg/kg. l3y sing!e 24-hour skin
contact, LD~o for technical mnterirt! in {rubhit, male), 27..t-GG.3
mg; kg; (rabbit, female). G5 mg/kg. Acute LD~u of Nem-A-'l'ak • 15-
G: (mt, mulc-ornl), 41.5-<\<1.l mg/kg; (rnhliit, malc-ncute dermal),
252-:l:H mg/k~. Aeutc LD~,u of Nem-A-Ta}~ • 2-/.,: (rut, mule-om!).
· 26-32.9 mg/kg; (acute dermal, rabbit fenwle). 371 mg/kr,:.
SIGNAL WORD: Nem-A-Tah • 15-G: DANG£R. Nem-A-Tak • 2-
L and 4-L: DANGER
ANTIDOTE: Atropine.
APPLICATION: An' experimcntnl rompound · for control·. of
nematodes nnd soi! insects in u vuriety of crops, including-: Tobacco,
petrnuts, soybeuns, n1id corn. ',
CAUTION: Nem-A-'J'ah • Tcchnicu!, 15-G, 2-L, and. 4-L nre
poison ow,; by ski1i cont net, eye wntnct, inhalation, or Hwul !owing.
FORMULATION: 1.r,.G is a 15% granul11r on 2,1/,50 mesh currier; 2-
l.. is 2-lb. active ingredient per ).!1dlon of wntcr miscible liquid, and
4-L is a 4-pound fictive ingredient per gallon of \'Ulter miscible
liquid.
Fosthietan
"A.P." AmPric-rrn Cvnnamid Co.
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CHEMICAL N~\ME: :,4,6-Trichloropheny!-4'-nitrophenyl ether.
COMMON NA~ 'E: C. vP.
ACTION: Select ve hr:bicide.
TOXICITY: AcUlti:..ofa! LD5o (mouse) (tech.), li,800 mg/ki{. Low
toxicity to fish.
APPLICATION: Fur con trot of weeds in rice paddies. -
FORMULATIONS: Emulsifiab!e concentrate (20%), granule (9%).
CNP
Hl': tvli1:, ti '!'ua1su Chemiculs Inc. (,Japan)
Shin.ing Corp. (Taiwan)
M40 • -see ~ICl'A.
Mobam, •
CHEMI_CAL NAME: 4-Benzothienyl N-methyl-carbamate.
OTHEI( NAME: MCA-600 •,
ACTION: Experime~tai contact insecticide, Not actively
developed by i\·lobi! Chemical Co.
APPLICAT!ONS: Effective against cockroaches, flieS, mosquitoes,
uphids, g:russhoppeni, und a variety of crop insects.
Mobilawn t {Product disContinued by Mobil Chemical Co.,
Phosphorus Div.)
CHEMICAL NAME: O-2,4-Dichlorophenyl 0, O-diethyl-
phosphoroth iunte.
COMMON NAMES: , dichlofenthion (ISO), , dichlorofenthion
(BSl).
OTHER NA~,tES: dichlof~ntion, Tri• VCJ3 ~ (Pennwalt· Holland),
VC-13 Nerrwcide •.
ACTION: Nt:1n:1ticide, insecticide.
CHEMICAL PHOPERTlES: A non-volatile, residual organic
phosphate, iHsoluble in water but readily soluble in 1~ost organic
solvents,
TOXICITY: :\cute ural LD~o, 270 Illg/kg.
S[GNAL wo:rn: IVARNlNG,'
A_PPLICA'l'JO.\!S: Controls. non-cyst forming nem8todes on
ornamentab ;uitl turf withotit damage to plants. Established
shrubs s\Jch ;1:,; boxwood, Japanese holly, etc., cun be treated to
control ne1w:1odc:. without phytotoxicity. Insecticide uses include
control of \;twn chinch bugs on St. Augustine grass. Used for
nelllutode Cllril rol on African violets.
FORMULATION: Emulsifiab!e cori'centrate 75% (7½
poundti/gullu1 t ~.
Cl .
0 .. ·~<OC,Hs.
Cl -0-P
· · · OC,Hs
0ichlofenthion
Mocap • .
CHEMICAL NAME: 0-Ethyl S,S-dipropyl phosphorodithioate.
COMMON NAME: ethoprop (U.S.A.).
OTHER NAJ'v!ES: Ethop'rophos· (Europe); Jolt (discontinued by
Ve!sicol Chemital Corp.), Prophos (discontinued).
ACTION: Nemuticide-soil insecticide.
CHEMICAL !J!{OPERTIES: Slightly soluble in water (750 pp.m);
readily solulile in most organic solvents.
TOXICITY: Acute orul LD~o (rat). 61.5 mg/kg:.
SIGNAL WOHDS: lUG., IVARNiNG; 6EC and 15 G, DANGER
ANTIDOTES: If .cyunosis is absent, give atropine 2-4 mg
intruvenously (0.US mg/kg for children). Hcpeat-ut.rupine ut 5-10
minute intervub until atropinization occurs (dry, flushed skin,
· tachycardiu, pupill1iry dilatation), and maintuin for •18 hours. If
cyanotil:, give initiu! atropine intrnmusculurly und !:>tart measures
to improve vcmi!ution.
l'rutopam Ull-,JU 11:;.:, ;:,..; Iv• d,1:«r~il) lll lUUcc .sati110.: uvocr J:\-~.il
minutes. If pulmonary edema is present, give intravenous!:-,' .s!uwly
as a 5% solution in winer over a period of not less than G minutes.
A second dose may be given after one hour if muscle weakness
persists. Additionn.l doses muy be g-iven cautiously for pcrsistc•nt
muscle weakness. Mny be given by intramuscular or subcutnne11us
routes if intrnvenous ndministrution is nut fensible.
In case of skin contnct wnsh patient with soap and wnter l'ollowed
by wash with 95% ethyl alcohol. Keep patient under cons1ant
observation for :!•1-:lG hours. Symptoms may per:;ist fur one nhinth.
The use of theophylline, morphine, burbiturntes, phcnothinzines,
reserpine, and sucl'inyl choline is contrnindicmed.
APPLICATIONS: For contrul of pl.111t pnrn:;itic nt:111:w,dL•s ;111d
soil-inhabiting insel'ts. Mocr1p • is not II fumig:rnt-type n~·m:ni,·il!,·.-
Action is bv Clint act. Chernicnl rnus1 be 111ixt~d with soil t,r ,·;1rrit·,!
bv water iii tu soil to lil' d'fective. [1 has n•sidual u1·1 ivil,\', ,!<>oi,:
nlovement in 1he soil, und ca11 be used at planting ti1HL' ... :it': 11,1
waiting periud.
Afocap" is re1·01n!llt!tlded for 1ie111_ur11dt· and ',\\rv:\·u:·,i'·
f1uc-cured tohu,:,:u; 1H:ma1ude, w1n·w,1ri11. ;11,,, !I•:,
control on sw,:1!l J)1J\Ul11; 111ir1i:1tod;1 1·111111·11' 1,n
plantains, c,1bh:1gl!, t:orn, pi11eapplt!, ~11;;:1r,·:1::c:. :;,,,•,
]lt\lHtO, penntllS, ('lJ(;U!lllic:r, snap :11H! li1n:l I:·,
recommended i'11r r1Jrn ro1>lWtirrn. L'Ul11·or111, n1·1r,;11• ,,!,.-. 1,·,:
wireworm contr,Jl llll corn; wire1\•,1r111 C(Ji\trul on whitl! p,Jt:1t<J: .:!:d
corn rootwonn (JJ1 peanuts nt )Hq.;ging. !1 is also n•corll!lll'llJL,d :lJf
nemntode control un Berrnudu, Zuy:;ia, St. Aug-ustine, centip,:dl',
and Bahia grasses in commen:ial turf.
FORMULATIONS: GEC, l0G, 15G, and Mocap • Plus 10-5G (10%
Mocap •, 5% Di-Sys ton ♦ granular). Mo cap• Plus ./-2 EC (-1 pounds
Mocap • + ~ pounds DiSyston ♦ /ga!!on). Mocap •-PCNR (3
pounds Mocap ~ + 10 pound!:> PCNB).
C~!-bO ~ C"H1S PAO
C,H,S
£tho prop
BP: Rhone-Poulenc Chemicnl Co., Agrochemical Div .
Mocap * PCNB -~ce t\i~ocap •.
Mocap • Plus -see Mocap ♦•
Modown *.
CHEMICAL., NAME; Methyl 5-(2,4-dichloropheiiu1yJ-2-ni-
trobenzoate. ·
COMMON NAME: bifenox (ANSI, IVSSA);
OTHER NAME: ;HC-4379.
ACTION: Herbicide.
CHEMICAL PHOPER'l'IES: Non-volatile crysrn!line so!id,
insoluble in water nnd modcrutely soluble in organic solvents. ll \:,
relutivcly stable in ultruviolct light.
TOXICITY: Acute oral LD!,u (rot), over tJ.\OQ mg/kg,
SIGNAL WOl!llS: 80\VP, CAUTlON: 2EC, DANGER: 4 Flowuble,
DANGER
ANTIDOTE: In cuse of contact with eyes, immediately flush eyes
with plenty of water for at least 15 minutes. Ca!\ physicinn. Wa!:ih
skin with plenty ofsonp and water.
APPLICATIONS: Particularly effective for brondleaf weed control.
Re!{istered for preplnnt incorporated and precmergence treatmems
for weed contni! n11 sovbeans, double trup soybeans, grain <;:;orghum,
preemergence nnd p0stemcrg-ence·t'reatmen.t for weed control on
direct-seeded rice and pine nun;ery seed beds.
FORMULATIONS: 80% wcttuhlc powder, 2 pounds per g;llon
emulsifiable concentrate, -I pounds per g-al\on f1owable.
COMBINATIONS: Afodown • tunk-mix with alachlor, propachlor,
or trifluralin; overlay with trifluralin, paraquat, or Roundup·.
COOCH, Cl No,-Q-o-Q-c1
BifenoK
HP: Rhone-Poulenc Chemicnl Co., Af{rochemicat Div.
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J.ACT!ON: Fungicide. . · · . .
· 1= CHEMICAL PROPERTIES: Solubility at 20°C in water 7100 ppm,
! 65% in methanol, 55% in benzene.
TOXlCITY: For technical metalaxyl: Acute oral LD5o (rat), 669 mg/kg; acute dermal LDso (rat), > :HOO mg/kg. Fish and wildlife relativdy nontoxic ..
SIGNAL WOHD: DANGER.
APPLJCA'l'!ON; For control of soil-borne diseases caused by Pythiwn nnd Phytophthora, and foliar diseases caused by the Phycomycett!S (downy mildews). Ridomil ~ 2E conditionally registcrl!d in the U.S. on tobacco.
FOREICN Al'PLICATIONS: Numerous foreign applications on vel'etuliles und fruits. Ciba-Geigy (Switzerland) offers for downy mildew contrn!: Ridomil"' com bi (metulax_vl + folpet) and Ridomil • plus (meta/axyl + copper) for g"rt1pes, Ridomil • ma11eb (metalux,,•/ + maneb) und Hido11Jil • M½ {met.a!axvl + mancozeb) 1·ur JHil:,ti'H:~, Vibacco, tomatues, liop, nnd v1:i.:elubleS.
l·'OHt\'l · !i ,:\'l'lUNS: EnwbifinUle rnncentrnle (~ puunds/gu!!on) 25 w1~, .:i(.
COl\-l!i:NXl'IONS: Sold by Ciba-Geigy (Switzerland): Ridomil • plus WI) 50, Uidomil • combi. WJ-' 60; CGA-48988/Cu, CGA-48988/Fulpet.
CH, 9H" Q ,,,-CH-COOCH,
. /
N '-.. CO-CH,OCH,
CH,
Metalaxyl
BP: Ciba-Geigy Corp., Agricultural Division Cilrn-Geigy Ltd. (Switzerland) ,.
Ridomil · 2E -see Ridomil •.
Ridomil ' Cambi -see Ridomil "'.
Ridomil • Maneb -see Ridomil "'.
Ridomil · MZ -see Fubol; Ridomil •.
Ridomil · MZ 5BWP ~ see Fubol.
Ridomil ' Plus -see Ridomil •.
Riflex • · :;ee Mctoxuron.
Rigo Oil Concentrate•
CHEM\1~AI .. l'ROPERTIES: A combination of superior parafinic buse uil 1111d :,;urt'uctant. ·
ACTION: Spray tank adjuvant.
SIGNAL WORD: CAUTION.
HANDLING AND STORAGE CAUTION: ·Keep container tightly closed and do not allow water to be introduced to contents of contuincr.
APJJL!CA'/'IO N: Spreuds pesticide8 evenly over leaf surface aiding· in penetration of herbicides into weed. Increuses efficiency oJ' defoliurlls.
FORMULATION: Liquid.
BP: Higo Company
Ripcord •
CHEMICAL NAME: a -cya.no-3-phenoxybenzyl 2,2-dimethyl-~-(2,:2-dichloroviny!) cyclopropane curboxylute.
COMMON NAME: cypermethrin (BSI, ISO).
O'l'J·!EH NAME: Barricade"'.
ACTION: Insecticide.
CHEMICAL PHOPEHTIES: More stable in acidic than in alkaline solution. Moderutely !iOluble in a runge of.organic solvents. High thernwl slubility, Ripcord Technical concentrute is a yellow-brown liqulJ contuining approximately 50% (w/w) cvpermethrin. Relatively non-voluti!e. · ¥
TOXICITY: Acute oral LD~o to rats is 251 mg/kg: acute dermal LD~o t(J rats i!:I > 1600 mg/kg (xylene solution). Highly toxic to fish.
:,. ' . ·---· .. curry out gastric luvage wit11 cun: to prevent asµirutiun. 'L~ symptomatically.
HANDLING AND STORAGE CAUTIONS: Avoid contact wi mouth, eyes, and skin. Store in original containers uwny from foo stuffs and anirnnl feed.·
APPLICATIONS: Used for conlrol of insecls in cotton nnd ii wi,
range of other crops.
FORMULATION: Emu!sifiable concentrntes, L1ltrn low vo!u11 concentrates, and wettable powder.
See also Barricade •.
H
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CH.,
C=C
Cl /
""Cl
CN
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C-0-CH 0 ~ 00
Cypermethrin
.BP: Shel! International Chemical Co. (Great Britain) F: Shell Cheniiculs U.K. Ltd. (Great Britain)
Ripenthol • -see Endothall ♦•
Risalin
CHEMICAL NAME: 3,5-Dinitro-N,N-di(n-propyl) sulfanilami_de
ACTION: Selective prcemergence herbicide.
CHEMICAL PROPERTIES: Orange crystuls melting at 13'.
138° C.
APPLICATION: 'l'o control grasses.
Risa!in
Riselect • -see Propanil.
Riverside Sodium Chlorate• -see Sodium Chlorate.
Roach -Chek • -see Hereon • Insectape with Propoxur.
Roach-Tape"' -sec Hereon "'lnsectope with Propoxur.
Roccal • -see Benzu\konium Chloride.
Rodent
• A member of the animal group (Order Rodentia) to Which rats mice, gophers, and porcupines belong.
Rodent Cake -see Diphacinone ♦ •
Rodenticide
A preparution intended for the control of rodents (rats, mice, etc.] and related animnls (such as rabbits).
A c!nssification of rodenticides is as follows:
_1. Coumurins.: dicumarol, warfari11, coumachlor, coumatetraly/.
2, Indandionc8: chlorophacinone, Piual •.
3. Organochlorines: DD'J', endrin.
4. Botanicals: red squiJJ, strychnine. s: Organophosphates: Gophacide •.
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CAS Registry Num!Jer: 56-38-2
Page 1 of 4
EPA CHEMICAL PROFILE
CHEMICAL IDENTITY --PARATHION
CAS Rcsgistry Number: 56-38-2
INTERIM
Date: October 31 1985
Rev is ion:
Synon,,:ns: Phosphorothioic Acid, 0,0-Dicthyl 0-(p-Nitrophenyl) Est.or
(Liquid Mixture); Parathion liquid; Alkron; Alleron; ,\mer.ican Cyana.tr!id :,.\.22;
Aphami te; Bayer E-605; B ladan; Diethyl 4-Nitrophenyl Phosphorothion:ne;
Diethyl p-Nitrophenyl Thionophosphate; Diethyl Parathion; Diethyl-p-Nitrophenyl
Monothiophosphate; DNTP; E 605; ENT 15,108; Ethyl Parathion; Etilon; Folidol;
Fosferno; Fostox; Genithion; NA 2783 (DOT); NCI-C00226; Niran; Nitrostigmina;
0,0-Diethyl 0-(p-Nitrophenyl) Phosphorothioate; 0,0 Diethyl 0-(p-nitrophenyl)
Thionophosphate 0,0-Diethyl 0-4-Nitrophenyl Thiophosphate; 0,0-Diethyl 0-p-
Nitrophenyl Phosphorothioate; 0leoparathion; Panthion; Paraflow; Paramar;
Paraphos; Parawet; Phenphos; Phoskil; Phosphenol; Phcsphorothioic Acid
0,0-Diethyl 0-(4-Nitrophenyl) Ester; Rhodi~tox; SNP; ~tatLion; Sulphos;
Thiophos; Vapophos
Chemical Formula: C10H14ND5PS
Molecul;;r Weight: 291.27
SECTIOI-./ I --HAZARDOUS INGREDIENTS/:DENTIT'( ll✓f-ORMATION
OSHA PEL: NA 0.1 rng/m' (skin) (NIOSH 1978, p. 148); ceiling 20
mg/;;1' (°''IARC 1972-1985)
AC(;IH TLV: TWA 0.1 mg/m' (skin); STEL 0.3 rng/rn' (skin) (ACGIH
1985, p. 26)
IDLH: 20 mg/m' (*Encyc of 0ccupat Health and Safety 1983)
Othe1-Limits Recommended: Occupational exposure recommended standard:
Air 0.05 mg/m' (NIOSH/0SHA 1978, p. 143)
SECTION II --PHYSICAL/CHEMICAL CHARACTERISTICS
Boiling Point: 707°F, 375°C (*Merck 1983)
Specific Gravity (H 20=l): 1.26 (*Merck 1983)
Vapor· Pressure (mmHg): 3. 78 x 10-S at 20°C (*Worthing 1979)
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PARATHION
CAS Registry Number: 56-38-2
P_age 2 of 4
SECTION 11 --PHYSICAL/CHEMICAL CHARACTERISTICS
11.elting Point: 4.3°F, 6°C (*Merck 1983)
Vapor Density (AIR=l): Not Found
1::vapo1·:.tion Rate (Butyl acctate=l): Not Found
Siolubilicy ir; Water: Practically insoluble; 12.4 mg/liter at 20°C (*Bo,·man 1979)
Appearance ·and Odor: Pale yellow liquid; technical grade is brm,n and has a garlic-like odor (*Worthing 1979).
SECTION Ill --FIRE AND EXPLOSIO~ HAZARD DATA
Flash Point (Method Used): 248-320°F, 120-160°C (Method not given) (*Clayton and Clayton 1981-82)
Flammable Limits: Not highly _flammable (*Encyc Occupat Health and Safety 1971)
LE L: Not Found
UEL: Not Found
Extinguis.hing Methods: Use water spray, dry chemical, foam, or carbon dioxide (*NFPA 1978).
Special Fire Fighting Procedures: Use water spray to keep fire-exposed con~ain~rs cool. If a leak or spill has not ignited, use water .spray to disperse vapors and to provide protection for firefighters. Water spray may be 1:sed to flush spills away from exposures. Fight adv81'.ced or massive fires from a safe distance·or from a protected .location. Special protective clothing should be worn; normal protective clothing may be . penefrated (*i'ffPA 1978).
Unusual Firo and Explosion Hazards: When heated to decomposition, it can e.rnit toxic fumes of oxides of nitrogen; phosphorus, and sulfur. High pressure hoses may scatter material from broken containers (*NFPA 1978). Containers may explode when heated (~CHRIS 1978).
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PARATHION
SECTION IV --REACTIVITY DATA
Stability: Unstable:
CAS Registry Number: 56-38-2 Page 3 of 4
St~ble: Yes, in distilled c,ater and in acid solution ('"Hac,ky 1981)
Conditions to Avoid: Store beloc, 25-30°C ('"Farm Chec,icals Handbook 19JJ). It slowly decomposes in e.ir and hydro1yz.-~s in cht= presence of
al!:aline material (*Hawley 1981). Containers may explode when heated
(i'CHRI S 19 7 8) .
I ncompz,tibility (Materials to Avoid): Not Found
Hazardous Decomposition or Byproducts: When heated to decomposition,
the material can emit toxic fumes of oxides of nitrogen, phosphorus, and
sulfur (*NFPA 1978).
Hazardous Polymerization: May Occur: Not Found May Not Occur: Not Found
Conditions to Avoid: Not Found 'I SECTION V --HEAL TH HAZARD DATA
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Routes of Entry: Inhalation:
Skin: Yes
Ingestion:
Yes (*Gosselin 1976) (*Gosselin 1976) Yes (*Gosseliri 1976)
Health H2zards (Acute, Delayed, and Chronic): This material is extremely toxic; the probable oral lethal dose is 5-50 mg/kg, or between 7
drops and 1 teaspoonful for a 150-lb. person. As little as 1 drop can
endanger life if splashed in the eye. Toxicity is highest by inhalation
(*Gosselin 1976).
Signs and Symptoins of Exposure: Symptoms may include nausea, vomiting,
abdominal cramps, diarrhea, excessive salivation, headache, giddiness,
·c,eakness, muscle twitching, difficult breathing, blurring or dimness of
vision, and loss of llluscle coordinat.ion. Death may occur from failure of
the respiratory center, paralysis of the respiratory muscles, intense bronchoconstriction, or all three (*Gosselin 1976).
Medical Conditions Generally Aggravated by Exposure: People at special
risk are those with a history of glaucorna 1 cardiovascular disease, hepatic
disease, renal disease, or central nervous sytem abnormalities (*Encyc
Occupat Health and Safety 1983).
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PARA TH ION
CAS Registry Number: 56-38-2 Page 4 of 4
SECTION V --HEAL TH HAZARD DATA (Continued)
Emergency end Firs{ A(d Prccedures: Move victim to fres:1 air; call emer~ency rne~ical care. I·f not breathing, give artificial respiration. If breathing is difficult, give oxygen. In case of contact with m2teri2l, ir11.me.diately flush skin or eyes i,.'ith running r..:ater for aL least 15 c:inutes. Speed in removing material from skin is of extreme i□porta~ce. Remove a:1d isolate contamineted clothing and shoes at the site. Ket::p victim qt1iet and maintain normal body temperature. Effects may be delsied; keep victim under observation (DOT 1984, Guide 55).
SECTION VI --USE INFORMATION
This material is used as an insecticide (*SRI) and is used almost exclusively in agriculture (Hayes 1982, p. 379).
SECTION V 11 --PRECAUTIONS FOR SAFE HANDLING AND USE (Steps to be Taken in Case Material is Released or Spilled)
In case of leaks or spills, special protective clothing should be worn. Use water spray to disperse vapors and flush spills e.way (*NFPA 1978). Ventilate area of spill or leak. Spills may be absorbed in vermiculite, ury sand; earth, or a similar material (*NIOSH/OSHA 1981).
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CAS Registry Number: 298-00-0
Page 1 of 4
EPA CHEMICAL PROFILE
CHEMICAL IDENTITY --PARATHION-METHYL
CAS P-,gistry Number: 298-00-0
INTERIM
Date: October 31, 1985
Revision:
Synonyms: Phosphorothioic Acid, 0,0-Dimethyl 0-(p-Nitrophenyl) Escer (Dry
Mixture); Methyl Parathion; Azofos; Azophos; BAY 11405; Bladan-M; Dalf;
Dimethylfenitrothion; Dimethyl 4-Nitrophenyl Phosphorothionate; Dimethyl
p-Nitrophenyl Phosphorothionate; Dimethyl p-Nitrophenyl Thiophosphate;
Dimethyl Parathion; E 601; ENT 17,292; Folidol M; Folidol M-40; Gearphos;
M-Parathion; Meptox; Metacid 50; Metacide; Metafos; Metafos (Pesticide);
Metaphos; Methyl-E 605; Methylthiophos; Metron; Metron (Pesticide);
NCI-C02971; Nitrox; Nitrox 80; 0,0-Dimethyl 0-(p-Nitrophenyl) ·
Phosphorothioate; 0,0-Dimethyl 0-(p-Nitrophenyl) Thionophosphate; 0,0-Dimethyl
0-(p-Nitrophenyl) Thiophosphate; 0leovofotox; Parathion Methyl Homolog; .
Partron M; Penncap M; Penncap MLS; Phenol, p-Nitro-, 0-Ester with 0,0-Dimethyl
Phosphorothioate;·Phosphorothioic Acid, 0,0-Dimethyl 0-(4-Nitrophenyl) Ester;
Quinophos; Sinafid M-48; Thiophenit; Vofatox; Wofatox; Wofotox; 8056 HC
Chemical Formula: C8H10N0 5PS
Molecu 11r Weight: 263.23
SECTION I --HAZARDOUS INGREDIENTS/IDENTITY INFORMATION
OSHA PEL: TWA 0.2 mg/m' ('"NIOSH/RTECS 1985)
ACGIH TLV: TWA 0.2 mg/m 3 ; STEL 0.6 mg/m' (skin) (,'<ACGIH 1983)
I DLH: Not Found
Other Limits Recommended: Toxicity information: 1c50 inhalation
(rat) 0:034 mg/liter/4 hours (*NIOSH/RTECS 1985)
SECTION II --PHYSICAL/CHEMICAL CHARACTERISTICS
Boiling Point: Not Found
Specific Gravity (H20=l):
Vapor Pressure (mmHg):
1.358 at 20°C (*Merck 1983)
. -6 . .
9. 7 x 10 at 20°C ('"Worthing 1979)
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CAS Registry Number: 298-00-0
Page 2 of 4
PARATH_ION-METHYL
I SECTION II --PHYSICAL/CHEMICAL CHARACTERISTICS (Continued)
I Melting Point: 99-100°F, 37-38°C (*Merck 1983)
Vapor Density (AIR=l): Not Found
I ·· vaporation RJte (Butyl acetate=l): Not Found
.::,lubility in Water: 50 mg/liter ('''Merck 1983) I
I
;\ppearance and Odor: White crystalline solid or powder (''NFPA 1978); odor like rotten eggs or garlic (*CHRIS 1978). Commercial product is a liquid consisting of 80 percent methyl parathion and 20 percent xylene (NFPA 1984, pp, 49-64); light to dark tan (*Worthing 1979).
I SECTION Ill --FIRE AND EXPLOSION HAZARD DATA
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Flash Point (Method Used)·: Not flammable at normal temperatures (*Clayton and Clayton 1982); commercial product, containing xylene, has flashpoint of 115°F (OC) (NFPA 1984, pp. 49-64),
Flammable Limits:
LEL: Not Found
UEL: Not Found
Extinguishins• Methods: -For small fires, use dry chemical, carbon dioxide, watnr spray, or foam. For large fires, use water spray, fog, or foam (,',DOT 1984).
Special Fire f:ighting Procedures: Fight fire from maximum distance. Dike fire co11trol water for later disposal; do not scatter the material ('''DOT 1984). Wear special protective clothing ('°'NFPA 1978).
Unusual Fire and Explosion Hazards: Poisonous gases are produced in .fire and when heated (''CHRIS 1978). Decomposition may lead to sufficient internal pressure to cause the container to rupture violently (NFPA 1984, pp. 49-64).
I SECTION IV --REACTIVITY DATA
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Stability: Unstable: Yes (''NFPA 1978)
Stable:
Conditions to Avoid: · High temperatures (120°F) cause decomposition. (NFPA 1984, pp. 49-64).
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Page 3 of 4
PARA TH ION-METHYL
SECTION IV --REACTIVITY DATA (Continued)
Incompatibility (Materials to Avoid): Oxidizing materials (NFPA 1984,
pp. 49-64).
Hazardous Decomposition or Byproducts: Decomposition may lead to
rupture of containers (NFPA 1984, pp. 49-64).
Hazardous Polymerization: May Occur: Not Found
May Not Occur: Not Found
Conditions to Avoid: Not Found
SECTION V --HEALTH HAZARD DATA • i1s ,
Routes of' Entry:. Inhalation:
Skin: Yes
Ingestion:
Yes ('~DOT 1984)
('''DOT 19 84)
Yes (*DOT 1984)
Health Hazards (Acute,. Delayed, and Chronic): This material is
extremely toxic; the probable,oral lethal dose is 5-50 mg/kg, or between 7
drops arid 1 teaspoonful for a 150-lb. person (*Gosselin 1984). Chronic
toxicity does no~ appear to be a major consideration (*NRC 1977).
Signs and Symptoms of Exposure: Symptoms may include nausea, vomiting,
abdominal cramps, diarrhea, excessive salivation, headache, giddiness,
dizziness, weakness, muscle twitching, difficult breathing, blurring or
dimness of vision, and loss of muscle coordination. Death may occur from
failure of the respiratory center, paralysis .of the respiratory muscles,
intense bronchoconstriction, or all three (*Gosselin·l984),
Medical Conditions Generally Aggravated by Exposure: Not Found
Emergency and First Aid Procedures: Move victim to fresh air; call
emergency medical care. If not breathing, give_artificial respiration.
• If breathing is difficult, give oxygen. In case of contact with material,
_immediately flush skin or eyes with running water for at least 15
minutes. Speed in removing material from skin is of extreme importance.
Remove and isolate contaminated clothing and shoes at the site. Keep
victim quiet and maintain normal body temperature. Effects ~ay be
delayed; keep victim under observation (*DOT 1984), ·
)
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CAS Registry Number: 298-00-0 Page 4 of 4
PARA TH ION-METHYL
1· SECTION VI --USE INFORMATION
I This material is used as an insecticide on over 50 crops, primarily cotton, · and on several ornamentals c,-,sRI).
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Sf:CTION VI i --PRECAUTIONS FOR SAFE HANDLING AND USE (Sc~ps to be Taken in Case Material is Released or Spilled)
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Do not touch spilled material; .stop leak if you can do it without risk. Use water spray to reduce vapors .. Small spills: take up with sand or other non-combustible absorbent material and place into containers for ·later disposal. Small dry spills: with clean shovel place material _into clean, dry containers and cover; move containers from spill area. Large .,,spills: dike far ahead· of spill for later disposal. Wear positive pressure breathing apparatus and special protective clothing (*DOT 1984).