NCD986187094_20010930_Reasor Chemical Company_FRBCERCLA SPD_HRS Documentation Package Volume III - Reference 4 (partial)-OCR

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Reasor Chemical
NCD 986 187 094
Castle Hayne, New Hanover Co., NC
HRS DOCUMENTATION PACKAGE
Volume III Reference 4 (partial)
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Ref. I
I • Reasor Chemical
NCD 986 187 094
'castle Hayne, New Hanover Co., NC +1-----!!!!!!! I Friday
December 14, 1990
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l?art II
Environmental
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Pirotection Agency
I 40 CFR Part 300
I Hazard' Ranking System; Final Rule
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Ref. 2
United States Office]ot Emergency and Reasor Chemical
Environmental Protection Remedial Response NCD 986 187 094
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Supertund I I
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&EPA
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Superfund ~hemical Data
Matrix
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NCO 986 I 87 094
Castle Hayne, New Hanover Co., NC
Ref 4
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I Document Control No. 4400-77-AHUA
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Revision 0 I
LABORATORY ANALYTICAL DATA
FOR I RE!\1EDIAL INVESTIGATION REPORT i
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REASOR CHEMICAL COMPANY SITE
CASTLE HAYNE, NEW HANO-yER COUNTY, NORTH CAROLINA
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I VOLUME! I I
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Work Assignment No. 77-4Rl24
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I OCTOBER 1998
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REGION IV
U.S. EPA CONTRACT NO. 68-W9-0057 I I
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I Roy F. WESTON, Inc.
SuitJ 200
5405 Me~ric Place
Norcross, GJorgia 30092
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WESTON W .O. No. ~OTT--0%-(KnS.00
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\ Document Control No. 4400-77-AHUA
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Retision 0 I
LABORATORY iALYTICAL DATA !
1l0R
RElvIBDIAL INVESTIGATION REPORT
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REASOR CHEMIC~ COMPANY SITE
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CASTLE HA Yl'.'E. l\'EW HANOVER COUNI'Y, NORTH CAROLINA . I
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I VOLUME II
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'\Vork Assignmelt No. 77-4RI24
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OCTOBER 1998
I I REGION IV
U.S. EPA CONTRAC;r NO. 68-W9-0057
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Roy F. WESl'ON, Inc.
I Suite 200
5405 MetriJ Place
Norcross, Geo~gia 30092
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I I -WESTON W.O. No. 04400-077-096-0015-00
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Reasor Chemical
NCD 986 187 094
Castle Hayne, New Hanover Co., NC
Ref 4
Reference 4 is subdivided as follows:
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Pages I -148
Al -A84
BI -B83
CI -C72
El -E45
FI -F43
GI-GII4
Data cover sheets
Surface water data
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Sediment Semivolatile data
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Sediment Volatile and metals data
Confirmatory Sampling -lugust 1998
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Duplicates, Rinsates, Trip blanks
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Analytical data sent under ~eparate cover -Followup samples collected
May 1999
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
MEMORANDUM
Date: 10/07 /97
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R~gion 4
' Science and Ecosystem Support Division
980 Colleg~ Station Road
Athens, Gecirgia 30605-2720
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Subject: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0352 REASOR CHEMICAL ! ·
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CASTLE HAYNE, NC I
From Ron Phelps#
To: RAY DOYLE
Thru· QA Office
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P ed are the results of analysis of samples collected as plrt of the subject project. I qc.auons, please contact me. -. !
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ATTACHMENT
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If you have any
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~,£.D .sr~,(.r . ft . i I i~J ~◄(,-g~~~ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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Region 4
I Science and Ecosystem Support Division
980 College Station Road ·
Athens, Georgia 30605-2720
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MEMORANDUM
Date: 10/07/97
Subject: Results of METALS INORGANIC Sample Analysis
97-0352 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Ron Phelps/II
To: RAY DOYLE
Thru· QA Office
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Attached are the results of analysis of samples collected as part lot the subject project.
ruestions, please contact me. -· I
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ATTACHMENT
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If you have any
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_.2~5=6~1~9c_ _____________ _
Project Number:~9~7,_-~0~3~5~2=---------------
Site: Reasor Chemical, Castle Hayne, NC
Element Flag
A. Waters
Be, Cd, Pb, Mn, u
Ag
Ba, Ca, Fe, Mg, u
K
Se R
Al J
?b J
Hg J
As u
Cr u
As J
Cr J
Cu J
Ni J
V J
B. Soils
Be, Cd, Pb, Mn, u
Ag
"la, Ca, Fe, Mg, u
Samoles Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12849, 12852, 12855, 12 8 5 9,
12862, 12 8 64
12849, 12852, 12855, 12859
12862, 12 8 64
12849, 12852, 12855, 12859,
12 8 62, 12864
12849, 12852, 12855, 12859,
12 8 62, 12864
12864
12 8 64
12859
12849, 12852
12 S 4 9, 12859, 12 8 64
12849, 12859
12859, 12864
All positives > IDL, but
< C?.DL
P..ll positives > IDL, but
< lOX contaminant level
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 36.6%
Blind spike recovery< action limit
Blind spike recovery> action limit
3lind spike recove=y > wa=ning limit
Blind spike recovery < warning limit
RSD >
exposures
CRDL
20% fo=
and results
IC? multiple
> IDL, but <
RSD >
exposi..:.::-es
CRDL
20% for
and results
ICP multiple
> IDL, but <
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X
=equired by contract
analysis
Only analysis of 2X
required by contract
analysis
CRDL
SOW
CRDL
sow
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analySis of 2X CRDL
required by contract sow
analysis
Baseline instability
Positives in blanks
standard
for ICP
standard
for ICP
standard
for ICP
standard
for ICP
standard
for ICP
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Nwnber: 25619
Project Number: 97-0352
Site: Reasor Chemical Castle Hayne, NC
Element Flaa Samoles Affected Reason
As J 12846, 12847, 12848, 12853, Matrix spike recovery = 51.9%
12854, 12857, 12858
Se J 12846, 12847, 12848, 12853, Matrix spike recovery 64. 1 %
12854, 12857, 12858
Ca J 12846, 12847, 12 8 4 8, 12853, Serial dilution pe=cent difference ---:: 12854, 12857, 12858 213.3%
Fe J 12846, 12847, 12848, 12853, Serial dilution percent difference
12854, 12857, 12858 213.3%
Blind spike recovery > warning limit
Al J 12846, 12847, 12 S 4 8, 12853, Blind spike recovery > action limit
12854, 12857, 12858
Ba J 12846, 12847, 12848, 12853, Blind spike recovery > warning action
12854, 12857, 12858 limit
Cc J 12846, 12847, 12348, 12853, Blind spike recove=y > warning action
1235~, 12857, 123SS limit
Cu J 12846, 12847, 12848, 12853, Blind spike recovery > warning act.::.
12854--; 12857, 12858 limit
Pb J 12846, 12847, 12 8 4 S, 12853, Blind spike recovery > warning action
12854, 12857, 12858 limit
Mg J 12846, 12847, 12848, 12353, Blind spike recovery > action limit
12854, 12357, 12353
Mn J 12846, 12847, 12848, 12853, Blind spike recovery > warning action
12354, 12857, 12858 limit
K J 12846, 12847, 12848, 12853, Blind spike recovery > warning action
128~4, 12857, 12858 limit
V J 12846, 12 8 4 7, 12848, 12853, Blind spike recovery > action limit
12854, 12857, 12858
Na J 12354, 12857 % RSD > 20% for ICP multiple
exposures
Zn J 12846, 12847, 12854 Only analysis of 2X CRDL standard
required by contract sow for IC?
analysis
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MEMORANDUM
Date: 10/22/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I SubJect: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0355 REASOR CHEMICAL
CASTLE HAYNE, NC
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From: Keith Bates 4 ~ /~
To: RAY DOYLE
Th ru: QA Office
~ttached are the results of analysis of samples collected as part of the subject project If you have any
iliuestions, please contact me. ~~?rs-;=::;-;;-;:;--:,__ __
I ffj{~([;EO'if~r,;
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ITTACHMENT
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!11 ,\i ;; I/ ._ 1/!}
: I ." -,, -3 1997 IY;·f
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(ril L66l t -,',C),'J ru
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D0CUM!:)lT CONTROL NUMBf..K lfi{l/1-t 9-B_0/ k
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INORGANIC DATA QUALIFIERS REPORT
Case Number:~2~5=6~4~5~--------------
Project Number:~9~7~--0=3=5~5~----------
Site: Reasor Chemical,
Element
Cu
Al, Ca, Mg, Na
Se
Na
Be
Co
V
Zn
Flaa
u
u
J
J
J
J
J
J
Castle Bayne, NC
samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12776
12774, 12775, 12776, 12777,
12778, 12779
12776, 12777, 12778
12775
12776, 12777, 12778
1277 4
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 143.8%
Serial dilution percent difference
13.6%
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
standard
for ICP
standard
for ICP
standard
for ICP
standa1.
for ICP
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MEMORANDUM
Date: 10/22/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of METALS INORGANIC Sample Analysis
97-0355 REASOR CHEMICAL
CASTLE HAYNE, NC
I From: Keith Bates ;:::_d /?~ / =
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To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
ruestions, please contact me.
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ITTACHMENT
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By-----:-==-=== -·
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INORGANIC DATA QUALIFIERS REPORT
Case Number:__.2~5~6~4~5"-----------------
Project Number:_e9~7~--0=3~5~5'-----------
Site: Reasor Chemical, Castle Bayne, NC
Element
Cu
Al, Ca, Mg, Na
Se
Na
Be
Co
V
Zn
Flag
u
u
J
J
J
J
J
J
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12776
12774, 12775, 12776, 12777,
12778, 12779
12776, 12777, 12778
12775
12776, 12777, 12778
12774
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 143.8%
Serial dilution percent difference
13.6%
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
standard
for ICP
standard
for ICP
standard
for ICP
standar1..-.
for ICP
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,:,.i\E.D ST,irE'.I'
. ft . I !~~ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Q y
I ' ~ , cl' '?"◄( PllO~e,'\
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I MEMORANDUM
I Date: 10/30/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: Keith Bates ~-r/4 6
To: RAY DOYLE
Thru: OA Office
lttached are the results oi analysis of samples collected as part of the subject project.
questions, please contact me.
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rACHMENT
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If you have any
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_.2~5=6=3~4c._ ______________ _
Project Number:~9~7~---"'0=3=5~3'--------------
Site: Reasor Chemical, Castle Bayne, SC
Element Flag
A. Waters
Sb, As, Be, Cd, U
Cr, Pb, Mn, Ag,
Tl
Ba, Ca, Fe, Mg,
K
Se
Cr
Al
Sa
Ca
Mg
Mn
K
Hg
Al
Co
Cu
Mg
Ni
u
R
J
J
J
J
J
J
J
J
J
J
J
J
J
•
samoles .n.ffected
.IUl positives> IDL, but
< CRDL
All positives> !DL, but
< lOX contaminant level
12726, 12728, 12730
12726, 12728, 12730
12738, 12740, 12742, 12743,
12746
12726, 12728, 12730
12726,
12726,
12726,
12726,
12726,
12740,
12743
12726,
1274 6
12730,
12742
12728, 12730
12 72 8, 12730
12728, 12730
12728, 12730
12728, 12730, 12738,
12742, 12743, 12746
12728, 12730, 12738,
12740, 12742, 12743
12726, 12730, 12738, 12740
Reason
Baseline instability
Positives in blanks
Matrix spike recovery 27. 1%
Matrix duplicate RPD 85. 6%
Serial dilution percent difference
20.2%
Serial dilutio~ percent difference
12.2%
Serial dilution percent difference
21.5%
Serial dilutio~ percent difference
32.4%
Serial dilution percent difference
36.6%
Serial dilution percent difference=
2 0. 4-%
Blind spike recovery< wa=ning limit
Only analysis of 2X CRDL
required by contract sow
analysis
standard
for ICP
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X
required by contract
analysis
CRDL
sow
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
requireC by contract SOW
analysis
standard
for ICP
standard
for ICP
standa.::-d
for re:
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INORGANIC DATA QUALIFIERS REPORT (continued)
I _ase Number:_,2~5~6~3~4 ______________ _
Project Number:_,9~7~-~0~3=5~3 ___________ _ I Site: Reasor Chemical, Castle
Element Flac Samoles Affected
Hayne, SC
V
I B. Soils
I s:i' ~.s, Be, Cd,
c:: f Pb, Mn, Ag,
Tl
I 3a, Ca, :e, Mg,
K
I As
Pb
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Se
I Se
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I Cr
Fe
I Fe
I 3a
I Ca
I Mg
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J 12726, 12728, 12730,
12740, 12746
1273S,
u
u
J
J
J
J
J
J
J
J
J
J
J
A.11 positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12711, 12 712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12735
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
Reason
Only analysis of 2X CRDL s~a~dard
required by contract SOW for
ICP analysis
Baseline instability
Positives in blanks
Matrix spike recovery
Mat::ix spike ::ecovery
Matrix duplicate RPD
Ma~rix spike recovery
Matri:-: spike recovery
Matrix duplicate RPO
Matrix duplicate RPO
Mat:-ix duplicate RPO
Matrix duplicate RPD
=
54. 1 %
180.8%
116.7%
65%
71. 6%
47.2%
54.3%
46.5%
141.9%
Serial dilution percent difference
47.19%
Se:-ial dilution percent difference~
113.7%
Blind spike recovery> warning limit
Serial dilutic~ pe:-cent diffe:-ence =
7 3. 8 %
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Nurnber:~2~5~6~3~4 ______________ _
Project Number:~9~7~--0~3=5=3 ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Element Flaa
K J
Ca J
Cu J
K J
•
Co u
Ni u
Se u
V u
Na J
Cr J
Co J
Ni J
Samoles Affected
12733, 12734, 12735, 12736
12 711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12 719, 12720, 12721, 12722,
12723, 12724, 12725, 127 32,
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12 715 / 12716, 12717, 12718,
12719, 12 72 0, 12721, 12722,
12 7 2 3 / 12724, 12725, 12732,
12733, 12734, 12735, 12736
12725
12723, 12724
12736
12711
12713, 12714, 12718
12718
12712, 12713, 12715, 1271~,
12720, 12723, 12724, 12735
J..2712, 12714, 12719, 12720,
12725, 12735, 12736
Reason
Serial dilution percent difference=
24.5%
Blind spike recovery> action limit
Blind spike recovery> warning limit
Blind spike recovery> action limit
Blind spike recovery> action limit
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
2 0% for
and r-esul ts
20% for
and results
20% for
and .:-esul ts
20% for
and =esul ts
20% for
ICP multip:
> IDL, but ,
IC? multiple
> IDL, but <
ICP multiple
> IDL, but <
ICP multiple
> IDL, but <
IC? multiple
Only analysis of 2X CRDL standard
requi=ed by co~t=act SOW fo= ICP
analysis
Only analysis
re qui red by
analysis
of 2X CRDL standa=d
contract sow for ICP
Only a~alysis of 2X CRDL standa=d
required by cont=act SOW for IC/
analysis
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INORGANIC DATA QUALIFIERS REPORT (continued)
...:ase Nurnber:__,,2~5~6~3~4,._ _____________ _
Project Nurnber:~9~7~-~0~3=5~3 ___________ _
Site: Reasor Chemical, Castle Hayne, SC
Element Flaa
V J
Zn J
•
Samoles Affected
12712, 12713, 12714,
12717, 12718, 12719,
12721, 12722, 12725,
12733, 12716
12721
12715,
12720,
12 7 32,
Reason
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standa=d
required by contract sow for ICP
analysis
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MEMORANDUM
Date: 10/30/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates ?://~
To: RAY DOYLE
Thru: QA Office
IJJ
I" ~ ~ cs: ~
1.1\ttached are the results of analysis of samples collected as e~-
questions, please contact me.
.he subject project. If you have any
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INORGANIC DATA QUALIFIERS REPORT
\)
~·ase Number: ~2~5=6=3~4~---------------
Pro j ect Nurnber:~9~7~--0=3~5~3~------------
Site; Reasor Chemical, Castle Bayne, SC
Element
A. Waters
Sb, As, Be, Cd,
Cr, Pb, Mn, Ag,
Tl
Ba, Ca, Fe, Mg,
K
Se
Cr
Ba
Ca
Mg
Mn
K
Hg
Co
Cu
Mg
Ni
Flao
u
u
J
J
J
J •
J
J
J
J
J
J
J
J
J
Sarnoles Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12726, 12728, 12730
12726, 12728, 12730
12738, 12740, 12742, 12743,
12746
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
12726,
12726,
12740,
12743
12728,
12728,
12742,
12730
12730,
1270,
12738,
127 4 6
12726, 12728, 12730, 12738,
1274 6
127 3 0, 12740, 12742, 12743
12742
12726, 12730, 12738, 12740
Reason
Baseline instability
Positives in blanks
Matrix spike recovery 27.1%
Mat=ix duplicate R?D 85.6%
serial dilution percent difference
20.2%
Serial dilution percent difference
12.2%
Serial dilution percent difference
21. 5-%
Serial dilution percent difference
32.4%
Serial dilution percent difference
3 6. 6%
Serial dilution percent difference
20. 4%
Blind spike recove:-y < warning limit
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CROL standard
required by contract SOW for ICP
analysis
Or.ly analysis of 2X
required by contract
analysis
CRDL
SOW
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
requi=ed by contract SOW
a:1alysis
standard
for ICP
standard
for IC?
standard
:for ICP
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:-"'2~5~6~3~4,_ _____________ _
Project Number:_,9~7=0~3=5=3 ___________ _
Site: Reasor Chemical
E:le!nent
V
B. Soils
Sb, P..s, 3e, Cd,
Cr, Pb, Mn, Ag,
Tl
Ba, Ca, :e, Mg,
K
As
Pb
Se
Se
P·..l
Cr
::e
Fe
Ba
Ca
Flaa
J
u
u
J
J
J
J
J
J
J
J
J
J
J
Castle Bayne, SC
Sam~les Affected
12726, 12728, 12730, 12738,
12740, 12746
A.11 positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12 7 2 0 1 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12 7 3 4 I 12735, 12736
127 33, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12 7 3 4, 12735, 12736
12733, 127 3 4, 12735, 12736
12733, 12734, 12735, 12736
Reason
Only analysis of 2X CRDL standard
required by contract SOW for
ICP analysis
Baseline instability
Positives in blanks
Matrix spike =ecovery
Matrix spike =ecovery
Matrix duplicate RPD
Matrix spike recovery
Mat::ix spiY.e recovery
Ma tri:-: du;ilicate RPD
Mat.ri:-: duplicate RPD
Matrix duplicate RPD
Matrix duplicate RPD
=
=
=
54. 1 %
180.8%
116.7%
65%
71.6%
½.7.2%
54.3%
45.5%
141.9%
Serial dilution percent difference
47.19%
Serial dilution percent diffe=e~ce =
113.7%
3lind spike recovery> warning limit
Se=ial dilution perce~~ dif:e=e~ce =
73. 8%
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:~2~5~6~3~4~--------------
Project Number:~9~7~--0~3=5~3 ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Element Flaa
K J
Ca J
Cu J
K J
•
Co u
Ni u
Se u
V u
Na J
Cr J
Co J
L'i J
Samoles Affected
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12 711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
1272 5
12723, 12724
12736
12711
12713, 12714, 12718
12718
12712, 12713, 12715, 12716,
12720, 12723, 12724, 12735
12712, 12714,
12725, 12735,
12719,
12736
12720,
Reason
Serial dilution percent difference=
24.5%
Blind spike recovery> action limit
Blind spike recovery> warnin9 li~~t
Blind spike recovery> action limit
Blind spike recovery> action limit
RSD > 20% for IC? multiple
e:-:posures and results > IDL, but <
CRDL
% RSD > 20% for ICP multiple
('-:•::;:iosu=es and results > IDL, but <
C:""'.DL
RSD > 2 0% for ICP multiple
ex?osu.:-es and results > IDL, but. <
CRDL
% RSD >
exposures
CRDL
20-% for
and results
IC? multiple
> IDL, but <
% RSD > 2 0% for ICP multiple
exposu::es
Only analysis
required by
analysis
Only analysis
required by
analysis
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
of 2X C~DL standard
contract SOW for IC!?
of 2X CRDL sta~da::d
contract sow for ICP
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INORGANIC DATA QUALIFIERS REPORT (continued}
Case Nwnber:_,2~5=6~3~4,_ ______________ _
Project Number:~9~7~-~0~3~5~3~------------
Site: Reasor Chemical,
E:lement Flao
V J
Zri J
Castle Bayne, SC
Samoles Affected
12712, 12713, 12714,
12717, 12718, 12719,
12721, 12722, 12725,
12733, 12716
12721
12715,
12720,
12732,
Reason
Only a~alysis of 2X CRDL standa=d
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for IC?
analysis
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MEMORANDUM
Date: 10/30/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates ~.h0~
To: ?JW DOYLE
.Thru: QA Office I .
Attached are the results of analysis of samples co))ected as part of the subject project. If you have any
questions, please contact me.
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ITTACHMENT
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INORGANIC DATA QUALIFIERS REPORT
Case Nwnber:_,2~5=6~3~4e_ ______________ _
Project Number:_,9~7~---"0~3~5~3,_ ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Element
A. Waters
Sb, P..s, Be, Cd 1
Cr, Pb, Mn, Ag,
Tl
Ba, Ca, Fe, Mg,
K
Se
Cr
3a
Ca
Mg
Mn
1-ig
Co
Cu
Mg
Ni
Flaa
u
u
R
J
J
J
J
J
J
J
J
J
J
J
J
J
'
Samcles Affected
All positives > IDL, but
< C?.DL
All positives> IDL, but
< l0X contaminant level
12726, 12728, 12730
12726, 12728, 12730
12738, 12740, 12742, 12743,
12746
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730, 12738,
12 7 Ll O, 12742, 12 7 4 3, 12746
1270
12726, 12728, 12730, 12 7 3 8,
12746
12730, 12740, 12742, 12743
12742
12726, 12730, 12738, 12740
Reason
Baseline instability
Positives in blanks
Matrix spike recovery
Matrix duplicate R?D
27.1%
85.6%
Serial dilution percent difference
20.2%
Serial Cilution pe=cent difference
12.2%
Serial dilution percent difference
21.5%
Serial dilution percent difference
32.4%
Serial dilution percent difference
36.6%
Serial dilution percent difference
20. 4%
Blind sµike recovery< ~ar~ing limit
Only analysis of 2X CRDL
required by contract SOW
analysis
standard
for ICP
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by cont.=act sow for ICP
analysis
Only analysis of 2X CRDL standard
.re qui red by contract sow for IC?
analysis
Only analysis of 2X CRDL standard
required by contract sow for IC?
analysis
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INORGANIC DATA QUALIFIERS REPORT (continued) I ·~ .. ;ase
Project Number:~9~7~--0~3=5~3 ___________ _
Number: ~2~5~6~3~4 ______________ _
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Site: Reasor Chemical, Castle Bayne, SC
Element Flaa
V J
B. Soils
Sb, As, Be, Cd, u
Cr, Pb, Mn, Ag,
Tl
3a, Ca, Fe, Mg, u
K
J'..s J
Pb J
Se J
Se J
P..l J
Cc J
Fe J
,e J
Ba J
Ce J
Mg J
Sam:::>les Affected
12726, 12728, 12730, 12738,
12740, 12746
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
127 l 5, 12716, 12717, 12713,
12 719, 12720, 12721, 12722,
12723, 1272 4, 12725, 12732,
12733, 12734, 12735, 12736
12733, 127 3.::J, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
1 ;. -,. 15, 12716, 12717, 12718,
1 :-::-i 19, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
Reason
Only analysis of 2X CRDL standard
required by contract sow for
ICP analysis
Baseline instability
Positives in blanks
Matrix spike recovery
Matrix spike recoverv
Matrix duplicate R?D
Matrix spike recovery
Matriz spike recovery
Matrix duplicate R?D
Matrix duplicate R?D
Matri:-: duplicate R?D
Matrix duplicate R?D
54.1%
180.8%
116.7%
65%
71. 6%
47.2%
54.3%
46.5%
141. 9%
Serial dilution percent difference=
0 .19%
Serial dilution percent difference=
113.7%
Blind spike recovery > warning limit
Se=ial dilution percent difference=
7 3. 8 %
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INORGANIC DATA QUALIFIERS REPORT {continued)
Case Number:_,2~5~6~3:..:,_4 ______________ _
Project Number:_,,9~7_-~0~3~5~3"--------------
Site: Reasor Chemical, Castle Bayne, SC
E:lement Flaa
K J
Ca J
Cu J
K J
•
Co u
Ni u
Se u
V u
Na J
Cr J
Co J
Ni J
Samoles Affected
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12 7 2 0, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12 7 3 4 I 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12725
12723, 12724
12736
12711
12713, 12714, 12718
12718
12712, 12713, 12715, 1271-6,
12720, 12723, 12724, 12735
12712, 12714, 12719, 12720,
12725, 12735, 12736
Reason
Serial dilution percent difference=
24.5%
Blind spike recovery> action limit
Blind spike recovery> warning limit
Blind spike recovery> action li:-:U.t
Blind spike recovery> action limit
RSD > 20% for IC? multi;,
exposures and results > IDL, but
CRDL
RSD > 20% for IC? mul ti;:,le
e:-:posures and results > IDL, but <
CRDL
% RSD >
exposures
CRDL
% RSD
exposures
CRDL
>
20% fo;c
and results
20% for
and results
IC? multiple
> IDL, but <
ICP multiple
> IDL, but <
RSD > 20% for ICP multiple
exposures
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by· contract sow for rcr
analysis
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INORGANIC DATA QUALIFIERS REPORT (continued)
:ase Number: ~2~5e.6e.3=4 ______________ _
Project Number:~9~7~-~0e.3,=5~3 ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Flaa
V J
J
Samoles Affected
12712, 12713, 12714,
12717, 12718, 12719,
12721, 12722, 12725,
12733, 12716
12721
12715,
12720,
12732,
Reason
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standa=d
required by contract SOW for ICP
analysis
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. ft .
i~} UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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"(½. ,,_{J~
_..i PAO-n'-C,
MEMORANDUM
Date: 10/30/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates r!:::ff/5b
To: RAY DOYLE
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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.ATTACHMENT
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If you have any
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INORGANIC DATA QUALIFIERS REPORT
Case Nurnber:__,2~5~6~3"--"4 ______________ _
Project Nurnber:~9~7~-~0~3~5=3 ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Slement
A. Waters
Sb, P.s 1 Be, Cd,
C=, ?b, Mn, Ag,
Tl
Ba 1 Ca, Fe, Mg,
K
Se
Al
Ba
Ca
Mg
K
Hg
Co
Cu
Mg
Ni
Flaa
u
u
J
J
J
J •
J
J
J
J
J
J
J
J
J
Samoles Jl.ffected
.nil positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12726, 12728, 12730
12726, 12728, 12730
12738, 12740, 12742, 12743,
12746
12726, 12728, 12730
12726, 12728, 12730
12 7 2 6, 12728, 12730
12726, 12728, 12730
12726, 12728, 12730
127 2 6, 12728, 12730, 12738,
12740, 12742, 12743, 12746
12743
12 7 2 6, 12728, 12730, 12738,
12746
12730, 12740, 12 7 42, 12743
127 42
12726, 12730, 12738, 12740
Reason
Baseline instability
Positives in blanks
Matrix spike recovery = 27.1%
Matrix duplicate R?D = 85.6%
Seri.al dilution percent difference
20.2%
Serial dilution percent difference =
12. 2%
Serial dilution percent difference
21. 5%
Serial dilution percent diffe=ence
32.4%
Serial dilution percent difference =
36.6%
Serial dilution percent difference
20. 4%
Blind spike recovery< warning limit
Only analysis of 2X CRDL
required by contract SOW
analysis
standard
for ICP
Only analysis of 2X CRDL standard
required by contract
analysis
Only analysis of 2X
required by contract
analysis
Only analysis of 2X
required by contract
analysis
O:1.ly analysis of 2X
required by contract
analysis
sow
CRDL
SOW
CRDL
SOW
CRDL
sow
for ICP
standard
for ICP
standard
for IC?
standard
for IC?
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:--'2~5~6~3~4e._ _____________ _
Project Nwnber:.....e9~7_-~0~3~5~3=-------------
Site: Rease= Chemical, Castle Hayne, SC
Element Flaa Samnles /l.ffected
V J 12726, 12728, 12 7 3 0,
12740, 127 4 6
B. Soils
Sb, As, Be, Cd, u All positives > IDL,
c= / Pb, Mn, Ag, < CRDL
Tl
Ba, Ca, Fe, Mg, u .n.11 positives > IDL,
12738,
but
but
K < lOX contaminant level
As
?b
Se
Se
.n.l
Cr
:e
Fe
Ba
Ca
Mg
J
J
J
J
J
J
J
J
J
J
J
•
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 1271 7, 12718,
12719, 12720, 12721, 12 722,
12723, 12724, 12725, 12732
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12711, 12712, 12713, 12 714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 127?2,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
12733, 12734, 12735, 12736
Reason
Only analysis of 2X CRDL standard
required by contract sow for
ICP analysis
Baseline instability
Positives in blanks
Matrix spike recovery 54.1%
Matrix spike recovery = 180.8%
Matrix duplicate RPD = 116. 7%
Matrix spike recovery 65%
Mat=ix spike recove=y 71. 6%
Matrix duplicate RPO 47.2%
Matrix duplicate RPO 54.3%
Matrix duplicate RPO 4 6. 5%
Matrix duplicate RPO 141.9%-
Serial dilution percent difference=
47.19%
Serial dilution percent difference=
113. 7%
Blind spike recovery> warning limit
Serial dilution percent difference=
7 3. 8 ,.
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Nurnber:___;;2~5~6~3~4:,_ _____________ _
Project Nurnber:~9~7~--0=3=5=3 ___________ _
Site: Reasor Chemical, Castle Hayne, SC
Element Flaa
K J
Ca J
Cu J
K J
•
Co V
Ni V
Se V
V V
Na J
Cr J
Co J
Ni J
Samoles Affected
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, !2735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12724, 12725, 12732,
12733, 12734, 12735, 12736
12711, 12712, 12713, 12714,
12715, 12716, 12717, 12718,
12719, 12720, 12721, 12722,
12723, 12 72 4, 11725, 12732,
12733, 12734, 1:·: 35, 12736
12725
12723, 12724
12736
12711
12713, 12714, 12718
12718
12712, 12713, 12715, 12716,
12720, 12723, 12724, 12735
12712, 12714, 12719, 12720,
12725, 12735, 12736
Reason
Serial dilution percent difference=
24.5%
Blind spike recovery> action limit
Blind spike recovery> wa=ning limit
Blind spike recovery> action limit
Blind S?ike recovery> action limit
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
ex?osures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposu.:es
20% for
and results
2 0% for
and results
20% for
and results
20% for
and resul t.s
20% for
ICP multiple
> IDL, but <
ICP multiple
> IDL, but <
ICP multiple
> IDL, but <
IC? multiple
> IDL, but <
ICP multiple
Only analysis
.:-equired by
analysis
of 2X CRDL standard
contract SOW for IC?
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standa.:d
required by contract SOW for ICP
analysis
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:_,2~5~6~3~4:,_ _____________ _
Project Number:-'9~7~-~0~3~5"-='3 ___________ _
Site: Reasor Chemical, Castle Bayne, SC
Element Flaa Samoles Affected
V J 12712, 12713, 12714,
12717, 12718, 12719,
12 721, 12722, 12725,
12733, 12716
Zn J 12721
•
12715,
12720,
12732,
Reason
Only analysis of 2X CRDL standard
required by contract SOW for IC?
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
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MEMORANDUM
I Date: 11/10/97
tt~(/[P?i
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0355 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: Keith Bates ;c-✓;?t:
To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
luestions, please contact me.
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ITTACHMENT
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I -= :; :~ ~ \1;7 ~ II
,J J ~-,
V0 11 r-:
• :: ,' •e ._, / -·-. ...,
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645 Project Number 97-0355 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Flag
Affected Samples Compound or Fraction Used Reason
Volatiles
12775
12781,12786,
12787,12817,
12820,12822,
12824
12813,12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene J
ethylbenzene J
acetone N
chloromethane J
styrene J
acetone N
xylene J
acetone N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< guantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal s~andard recovery
I
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.,, ORGANIC DATA QUALIFIER REPORT I Case Number 25645
Flag
Affected Samples Compound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
chrysene J < quantitation lirni t I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno{l,2,3-cd)pyrene J < quantitation limit
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit I 12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
12801 pyrene J < quantitation limit I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
12802 phennathrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit I benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
12804 phennathrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
12805 acenaphthylene J < quantitation limit
fluorene J < quantitation limit
I anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quant i tat ion limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I dibenz(a,h)anthracene J < quantitation limit
12806 J < quantitation limit pyrene
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Affected Samples
12807
12809
12812
12813
12814,12815
12816
12817
12819
ORGANIC
Case
DATA QUALIFIER
Number 25645
Compound or Fraction
phennathrene
fluoranthene
Flag
Used
J
J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
naphthalene J
2-methylnaphthalene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno{l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
phenanthrene J
naphthalene J
acenaphthylene J
anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo{g,h,i)perylene J
phenanthrene J
fluoranthene J
pyrene J
chrysene J
benzo(b/k)fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
phenanthrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
phenanthrene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
limit
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Samples Compound or Fraction Used Reason
12821,12822 phenanthrene J < quantitation
fluoranthene J < quantitation
pyrene J < quantitation
benzo(a)anthracene J < quantitation
chrysene J < quantitation
benzo(b/k)fluoranthene J < quantitation
benzo(a)pyrene J < quantitation
12824 phenanthrene J < quantitation
pyrene J < guantitation
Pesticides
None
limit
limit
limit
limit
limit
limit
limit
limit
limit
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I ~"wsr,.,~
. ft .
!~~
¾,:: <'/ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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'ftpqo~ Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 11/10/97
Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
From:
97-0355 REASOR CHEMICAL
CASTLE HAYNE, NC
Keith Bates ~ ~
To: RAY DOYLE
Thru: QA Office
I
Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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ITTACHMENT
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If you have any
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645 Project Number 97-0355 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Flag
Affected Samples Compound or Fraction Used Reason
Volatiles
12775
12781,12786,
12787,12817,
12820,12822,
12824
12813, 12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene
ethylbenzene
styrene
xylene
1,1,1-trichloroethane
carbon tetrachloride
bromodichloromethane
1,2-dichloropropane
J
J
J
J
J
J
J
J
trans-1,3-dichloropropene
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene J
ethyl benzene J
acetone N
chloromethane J
styrene J
acetone N
xylene J
acetone N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
J
J
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low,internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
common lab contaminant
low internal standard
low internal standard
low internal standard
recovery
recovery
recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
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I ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Samples Compound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation lirni t
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation l irni t
I benzo(b/k)fluoranthene J < quantitation limit
12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
I 12801 pyrene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12802 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo{a)anthracene J < quantitation limit
chrysene J < quantitation limit I benzo(b/k)fluoranthene J < quantitation limit
benzo{a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quant.itation limit
benzo(b/k)fluoranthene J < quantitation limit I benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
12804 phennathrene J < quantitation limit I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit I benzo(b/k)fluoranthene J < quantitation limit
12805 acenaphthylene J < quantitation limit
fluorene J < quantitation limit I anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno{l,2,3-cd)pyrene J < quantitation limit I dibenz{a,h)anthracene J < quantitation limit
12806 pyrene J < quantitation limit
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ORGANIC DATA QUALIFIER REPORT
I Case Number 25645
Flag
Affected Sam2les Comoound or Fraction Used Reason
12807 phennathrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12809 naphthalene J < quantitation limit
2-methylnaphthalene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I benzo(a)anthracene J < quant.itation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quantitation limit
benzo(g,h,i)perylene J < quantitation limit
12812 phenanthrene J < quantitation limit
I 12813 naphthalene J < quantitation limit
acenaphthylene J < quantitation limit
anthracene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno{l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
I benzo(g,h,i}perylene J < quanti tat ion limit
12814,12815 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
I pyrene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12816 pyrene J low internal standard recovery
butylbenzylphthalate J low internal standard recovery
3,3'-dichlorobenzidine J low internal standard recovery
benzo(a)anthracene J low internal standard recovery
I bis(2-ethylhexyl)phthalate J low internal standard recovery
chrysene J low internal standard recovery
12817 phenanthrene J < quantitation limit
I pyrene J < quantitation limit
benzo(a)pyrene J < quantit.ation limit
benzo(g,h,i)perylene J < quantitation limit
I 12819 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
chrysene J < quantitation limit
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag Affected Samples Compound or Fraction Used Reason
12821,12822 phenanthrene J < quantitation
fluoranthene J < quantitation
pyrene J < quantitation
benzo(a)anthracene J < quantitation
chrysene J < quantitation
benzo(b/k)fluoranthene J < quantitation
benzo(a)pyrene J < quantitation
12824 phenanthrene J < quantitation
pyrene J < guantitation
Pesticides
None
limit
limit
limit
limit
limit
limit
limit
limit
limit
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MEMORANDUM
Date: 11/10/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of EXTRACTABLES ORGANIC Sample Analysis
97-0355 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: Keith Bates ,t;,,#~
To: RAY DOYLE
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project If you have any
.questions, please contact me. ,-.,L
. <> it~D~:.j~: __ [ttf P., r
I .,,\., .. -,.,,~ .,,,,,,~, ''.' ,,.,---,n COi'~,. :-,,'.,--' -
DOC;J\,\LI ,
.I
ITTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case
Site
Number 25645 Project Number 97-0355 SAS Number
ID. Reasor Chemical, Castle Hayne, NC
Affected Samples
Volatiles
12775
12781,12786,
12787, 12817,
12820, 12822,
12824
12813,12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
Flag
Compound or Fraction Used
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene
ethylbenzene
styrene
xylene
J
J
J
J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene J
ethylbenzene J
acetone N
chloromethane J
styrene J
acetone N
xylene J
acetone N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo{a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
Reason
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< guantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< guantitation limit
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
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ORGANIC DATA. QUALIFIER REPORT
I Case Number 25645
Flag
Affected sam12les Com12ound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
12801 pyrene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
12802 phennathrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
12804 phennathrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < guantitation limit
12805 acenaphthylene J < quantitation limit
fluorene J < quantitation limit
I I anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < guantitation limit
I dibenz(a,h)anthracene J < quantitation limit
12806 pyrene J < quan~itation limit
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Affected Samples
12807
12809
12812
12813
12814,12815
12816
12817
12819
ORGANIC
Case
DATA QUALIFIER
Number 25645
Compound or Fraction
phennathrene
fluoranthene
Flag
Used
J
J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo (a) pyrene J
indeno(l,2,3-cd)pyrene J
naphthalene J
2-methylnaphthalene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
phenanthrene J
naphthalene J
acenaphthylene J
anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
phenanthrene J
fluoranthene J
pyrene J
chrysene J
benzo(b/k)fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
phenanthrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
phenanthrene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
limit
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
lo~ internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
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I
I
I
I
I
I
I
I
I
I
Affected Samples
12821,12822
12824
Pesticides
None
ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Com12ound or Fraction Used Reason
phenanthrene J < quantitation
fluoranthene J < quantitation
pyrene J < quantitation
benzo(a)anthracene J < quantitation
chrysene J < quantitation
benzo(b/k)fluoranthene J < quantitation
benzo(a)pyrene J < quantitation
phenanthrene J < quantitation
pyrene J < quantitation
limit
limit
limit
limit
limit
limit
limit
limit
limit
I
I
I
I
I
I
MEMORANDUM
Date: 11/10/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
I
I
I
I
97-0355 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates
To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
ruestions, please contact me.
I
I
lrrACHMENT
I
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645 Project Number 97-0355 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Flag
Affected Samples Compound or Fraction Used Reason
Volatiles
12775
12781,12786,
12787,12817,
12820,12822,
12824
12813,12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane
toluene J
chlorobenzene J
ethyl benzene J
styrene J
xylene J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene J
ethyl benzene J
acetone N
chloromethane J
styrene J
acetone N
xylene J
acetone N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
J
J
J
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
I
I
I ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected SamQles Com2ound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
I 12801 pyrene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12802 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12804 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
12805 acenaphthylene J < quantitation limit
I fluorene J < quantitation limit
anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
12806 pyrene J < quantitation limit
I
I l\ ~
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Affected Samples
12807
12809
12812
12813
12814,12815
12816
12817
12819
ORGANIC
Case
DATA QUALIFIER
Number 25645
Compound or Fraction
phennathrene
fluoranthene
Flag
Used
J
J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
naphthalene J
2-methylnaphthalene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
phenanthrene J
naphthalene J
acenaphthylene J
anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz{a,h)anthracene J
benzo(g,h,i)perylene J
phenanthrene J
fluoranthene J
pyrene J
chrysene J
benzo(b/k)fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
phenanthrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
phenanthrene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
liIT\it
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Samples Compound or Fraction Used Reason
12821,12822 phenanthrene J < quantitation
fluoranthene J < quantitation
pyrene J < quantitation
benzo(a)anthracene J < quantitation
chrysene J < quantitation
benzo(b/k)fluoranthene J < quantitation
benzo(a)pyrene J < quantitation
12824 phenanthrene J < quantitation
pyrene J < quantitation
Pesticides
None
limit
limit
limit
limit
limit
limit
limit
limit
limit
I
I
I
I
I
MEMORANDUM
Date: 11/10/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of VOLATILES ORGANIC Sample Analysis
I
I
I
I
97-0355 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates
To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
ruestions, please contact me.
I
I
lnACHMENT
I
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I yi1
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I
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ORGANIC DATA QUALIFIER REPORT
Case Number 25645 Project Number 97-0355 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Flag
Affected Samples Compound or Fraction Used Reason
Volatiles
12775
12781,12786,
12787,12817,
12820,12822,
12824
12813,12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene
ethylbenzene
acetone
chloromethane
styrene
acetone
xylene
J
J
N
J
J
N
J
acetone N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery·
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
I
I
I ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Sa.m;gles Com12ound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
I 12801 pyrene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12802 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12804 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
12805 acenaphthylene J < quantitation limit
I fluorene J < quantitation limit
anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
12806 pyrene J < quantitation limit
I
I 5\
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Affected Samples
12807
12809
12812
12813
12814,12815
12816
12817
12819
ORGANIC
Case
DATA QUALIFIER
Number 25645
Compound or Fraction
phennathrene
fluoranthene
Flag
Used
J
J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
naphthalene J
2-methylnaphthalene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
phenanthrene J
naphthalene J
acenaphthylene J
anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
phenanthrene J
fluoranthene J
pyrene J
chrysene J
benzo(b/k)fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
phenanthrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
phenanthrene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
limit
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Samples Compound or Fraction Used Reason
12821,12822 phenanthrene J < quantitation
fluoranthene J < quantitation
pyrene J < quantitation
benzo(a)anthracene J < quantitation
chryaene J < quantitation
benzo(b/k)fluoranthene J < quantitation
benzo(a)pyrene J < quantitation
12824 phenanthrene J < quantitation
pyrene J < quantitatiOn
Pesticides
None
limit
limit
limit
limit
limit
limit
limit
limit
limit
I
I
I
I
I
I
MEMORANDUM
Date: 11/10/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
.Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of EXTRACTABLES ORGANIC Sample Ana_lysis
97-0355 REASOR CHEMICAL
I CASTLE HAYNE, NC
From: Keith Bates I To: RAY DOYLE
I
I Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any f uestions, please contact me.
I
I
lnACHMENT
I
I
I
I ~'\
I
I
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I
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I
I
ORGANIC DATA QUALIFIER REPORT
Case Number 25645 Project Number 97-0355 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Flag
Affected Samples Compound or Fraction Used Reason
Volatiles
12775
12781,12786,
12787,12817,
12820,12822,
12824
12813,12814
12793
12794,12795
12795
12802
12808
12811
12815
12816,12817,
12820,12824
Extractables
12776,12819
acetone N
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
1,1,1-trichloroethane J
carbon tetrachloride J
brornodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cis-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
toluene
ethylbenzene
acetone
chloromethane
styrene
acetone
xylene
acetone
J
J
N
J
J
N
J
N
di-n-octylphthalate J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
common lab contaminant
< quantitation limit
common lab contaminant
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
I
I
I ORGANIC DATA QUALIFIER REPORT
Case Number 25645
Flag
Affected Sarn:Qles Com2ound or Fraction Used Reason
I 12790 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12795,12796 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
12795 benzo(a)pyrene J < qunatitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12800 pyrene J < quantitation limit
chrysene J < quantitation limit
I 12801 pyrene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
I 12802 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12803 pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantit-ation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
I 12804 phennathrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
12805 acenaphthylene J < quantitation limit
I fluorene J < quantitation limit
anthracene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
12806 pyrene J < quantitation limit
I
I s-v
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Affected Samples
12807
12809
12812
12813
12814,12815
12816
12817
12819
ORGANIC
Case
DATA QUALIFIER
Number 25645
Compound or Fraction
phennathrene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b/k)fluoranthene
benzo(a)pyrene
indeno(l,2,3-cd)pyrene
Flag
Used
J
J
J
J
J
J
J
J
naphthalene J
2-methylnaphthalene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
phenanthrene J
naphthalene J
acenaphthylene J
anthracene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
dibenz(a,h)anthracene J
benzo(g,h,i)perylene J
phenanthrene J
fluoranthene J
pyrene J
chrysene J
benzo(b/k)fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichloiobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
phenanthrene
pyrene
benzo(a)pyrene
benzo(g,h,i)perylene
phenanthrene
fluoranthene
pyrene
chrysene
J
J
J
J
J
J
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
limit
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
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Affected Samples
12821,12822
12824
Pesticides
None
ORGANIC DATA QUALIFIER
Case Number 25645
Flag
Compound or Fraction Used
phenanthrene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
phenanthrene
pyrene
J
J
REPORT
Reason
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
< quantitation
limit
limit
limit
limit
limit
limit
limit
< quantitation limit
< quantitation limit
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I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
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MEMORANDUM
Date: 11/17/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0352 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates ~-1-t/S-L
To: RAY DOYLE
· .Thru: QA Office
lttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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ITTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25619 Project Number 97-0352 SAS Number
Site IO. Reasor Chemical, Castle Hayne, NC
Affected Samples Compound or Fraction
Volatiles
12848 acetone
12865 chloromethane
13166 acetone
Ext::-actables
12850,12851,
12860
12853
12856
Pesticides
13183
13184
phenol
acenaphthylene
anthracene
carbazole
fluoranthene
benzo(a)anthracene
benzo(a)pyrene
indeno(l,2,3-cd)pyrene
benzo(g,h,i)perylene
2-methylnaphthalene
endosulfan II
4,4'-DDT
endrin
methoxychlor
Flag
Used Reason
J erratic response factor
J < quantitation limit
N common lab contaminant
J < quantitation limit
J < cruantitation limit
J < q1-lantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation 1 irni t
J < quantitation limit
J < quantitation limit
N difference in columns
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I ::,,i,-tED sr,.,e.J'
. ft .
I~~ I ~ y % •
'?",it Pl'IO'f'I:,~
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
I MEMORANDUM
I Date: 11/17/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
97-0352 REASOR CHEMICAL
CASTLE HAYNE, NC
I From: Keith Bates r:,J!/::L
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I
To: RAY DOYLE
,Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project. If you have any
~uestions, please contact me. I
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ITTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25619 Project Number 97-0352 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Affe~ted Samples Compound or Fraction
Volatiles
12848 acetone
12865 chloromethane
13166 acetone
Extractables
12850,12851,
12860
12853
12856
Pesticides
13183
13184
phenol
acenaphthylene
anthracene
carbazole
fluoranthene
benzo(a)anthracene
benzo(a)pyrene
indeno(l,2,3-cd)pyrene
benzo(g,h,i)perylene
2-methylnaphthalene
endosulfan II
4,4'-DDT
endrin
methoxychlor
Flag
Used Reason
J erratic response factor
J < quantitation limit
N common lab contaminant
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < guantitation limit
J < guantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < guantitation limit
N difference in columns
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t~i UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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~ .
1l ~AO~c<.9
MEMORANDUM.
Date: 11/17/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I . Subject: Results of EXTRACTABLES ORGANIC Sample Analysis
97-0352 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: Keith Bates ;:::.-.JI /4.£::::::
To: RAY DOYLE
Thru: OA Office
I Attached are the results of analysis of samples collected as part of the subject project.
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questions, please contact me.
rTTACHMENT
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If you have any
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ORGANIC DATA QUALIFIER REPORT
Case Number 25619 Project Number 97-0352 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Affected Samples
Volatiles
12848
12865
13166
Extract ables
12850,12851,
12860
12853
12856
Pesticides
13183
13184
Comoound or Fraction
acetone
chloromethane
acetone
phenol
acenaphthylene
anthracene
carbazole
fluoranthene
benzo(a)anthracene
benzo(a)pyrene
indeno(l,2,3-cd)pyrene
benzo{g,h,i)peryl~ne
2-methylnaphthalene
endosulfan II
4,4'-DDT
endrin
methoxychlor
J
J
N
J
J
J
J
J
J
J
J
J
J
J
J
J
J
N
Flag
Used Reason
erratic response factor
< quantitation limit
common lab contaminant
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
difference in columns
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
MEMORANDUM
Date: 11 /20/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0386 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates
To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project.
.questions, please contact me.
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tTTACHMENT
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If you have any
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_,2~5~6~4=8 _____________ _
Project Number:~9~7,_-~0~3~8~6~-----------
Site: Reasor Chemical, Castle Hayne, NC
Element Flag Samples Affected
Sb, As, Be, Cr, u All positives > IDL1 Pb, Mn, Tl < CRDL
Ba, Ca, Fe, Mg, u All positives > IDL,
but
but
K < lOX contaminant level
As JN 12999
Tl JN 12 9 99
Al J 12993, 12994, 12995, 12 9 9 6
12997, 12998, 12999
Fe J 12993, 12994, 12 995, 12996,
12997, 12998, 12999
Se J 12993, 12994, 12995, 12 9 9 6,
12997, 12998, 12999
Pb J 12993, 12994, 12995, 12996,
12997, 12998, 12999
Ca J 12993, 12 9 9 4, 12995, 12996,
12997, 12999, 12999
Mg J 12993, 12994, 12995, 12996,
12997, 12998, 12999
K J 12993, 12994, 12995, 12996,
12997, 12998, 12999
Cd, Ni JN 12999
Cd u 12993, 12994, 12998
Ni u 12997, 12998
Se u 12994
Reason
Baseline instability
Positives in blanks
suspected positive interference as
noted in the contractor ICS
Suspected positive interference as
noted in the contractor res
Matrix spike recovery= 73.8%
Serial dilution percent difference
16. 7%
Matrix spike recovery= 62.1%
Blind spike recovery< warning limit
Matrix spike recovery= 61.2%
Matrix duplicate R?D = 43.3%
Blind spike recovery> action limi~
Serial dilution percent difference=
21.8%
Se=ial dilution pe=cent difference
22.6%
Serial dilution percent difference
10.8%
Suspected positive interference from
high concentrations of A.l (> 180,000
ug/LJ and Fe(> 200,000 ug/L) in
solution
% RSD
exposures
CRDL
>
% RSD >
exposures
CRDL
% RSD >
exposu=es
CRDL
20% for
and results
20% for
and results
20% for
and =esults
ICP multiple
> IDL, but <
ICP multiple
> IDL, but <
ICP multiple
> IDL, but <
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:__,2~5~6~4~8"---------------
Project Number:__;,9~7~-~0~3~8~6 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
Ag
As
Cd
Co
cu
Ni
V
Flag
u
J
J
J
J
J
J
Samples Affected
12997, 12999
12994
12995, 12996, 12997
12994, 12999
12995
12994
12993, 12 9 9 6, 12 9 9 7, 12998
Reason
% RSD > 20% for
exposures and results
CRDL
ICP multiple
> IDL, but <
% RSD > 20% for ICP
exposures
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract sow
ana~ysis
Only analysis of 2X CRDL
required by contract sow
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
multiple
standard
for ICP
standard
for ICP
standard
for ICP
standard
for ICP
standard
for ICP
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[~2 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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-1( PRO'f'c.~ Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 11/20/97
Subject: Results of METALS INORGANIC Sample Analysis ·-J;',.
. -
;-11~· I --,
97-0386 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates (<::;_,_/.8 6"-L,,_
To: RAY DOYLE
Thru: OA Office
' /
,..----. '
'\l,
I • \
I-• I
Attached are the results of analysis of samples collected as part of the subject project.
.questions. please contact me. ~ (,-{)
If you have any
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tTTACHMENT
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h.' \ \\\\\)
'"' : ,s/-:" c::>' ,,u-, , .
1-\j),tJ~.:.
\'.-'-'-it
By_
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INORGANIC DATA QUALIFIERS REPORT
Case Number:~2~5~6~4~8~--------------
Project Number:~9~7_-~0~3~8=6 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
Sb, As, Be, Cr,
Pb, Mn, Tl
Ba, Ca, Fe, Mg,
K
As
Tl
Al
Fe
Se
Pb
Ca
Mg
K
Cd, Ni
Cd
Ni
Se
flag
u
u
JN
JN
J
J
J
J
J
J
J
JN
u
u
u
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12999
12999
12993, 12994, 12995, 12996
12997, 12998, 12999
12993, 12994, 12995, 12996,
12997, 12998, 12999
12993, 12994, 12995, 12996,
12997, 12998, 12999
12993, 12994, 12995, 12996,
12997, 12996, 12999
12993, 12994, 12995, 12996,
12997, 12998, 12999
12993, 12994, 12995, 12996,
12997, 12998, 12999
12993, 12994, 12995, 12996,
12997, 12998, 12999
12999
12993, 12 9 9 4, 12998
12997, 12998
12994
Reason
Baseline instability
Positives in blanks
Suspected positive interference as
noted in the contractor res
Suspected positive interference as
noted in the contractor res
Matrix spike recovery= 73.8%
Serial dilution percent difference
16. 7%
Matrix spike recovery= 62.1%
Blind spike recovery< warning limit
Matrix spike recovery= 61.2%
Matrix duplicate RPD = 43.3%
Blind spike recovery> action limit
Serial dilution percent difference=
21. 8%
Serial dilution percent difference
22.6%
Serial dilution percent difference=
10.8%
Suspected positive interference from
high concentrations of Al (> 180,000
ug/LJ and Fe(> 200,000 ug/L) in
solution
% RSD > 20, for ICP multiple
exposures and results > IDL, but <
CRDL
% RSD > 20, for ICP multiple
exposures and results > IDL1 but <
CRDL
% RSD > 20% for ICP multiple
exposures and results > IDL, but <
CRDL
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number: _,2=5"6,.:4,_8,a_ ____________ _
Project Number:_e9~7~-~0=3~8~6'-----------
Site: Reasor Chemical, Castle Bayne, NC
Element Flaa
Ag u
As J
Cd J
Co J
Cu J
Ni J
V J
Samples Affected
12997, 12999
12994
12995, 12996, 12997
12994, 12999
12995
12994
12993, 12996, 12997, 12998
Reason
% RSD >
exposures
CRDL
201 for ICP multiple
and results > IDL, but <
% RSD > 20% for ICP multiple
exposures
Only analysis of 2X CRDL standard
required by cont.::-act sow for ICP
analysis
Only analysis of 2X CRDL standard
required by cont.::-act sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standa_
required by contract sow for ICP
analysis
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I ~"IED sr-1rt,r
. ft .
~~~ t &
I ~ ,/
~l PRO~~
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I MEMORANDUM
I Daie: 11 /20/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of CLASSICALS/NUTRIENTS INORGANIC Sample Analysis
97-0357 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: Keith Bates
To: RAY DOYLE
·, Thru: QA Office
.Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me. J-
I ·.· ,-,;';?,;_Ri!M~tl.C .-'1'"'1-,', ~ \.)';. I ,--~ -:. ·, .. ,;-:,.J· (·'.'_)}: \ ;\V•-
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INORGANIC DATA QUALIFIERS REPORT
Case Number:~~5~6~5=5 _____________ _
Project Number:~9~7~-~0~3~5~7 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
A. Waters
As, cu, Se, Tl,
Zn
Al, Ca, Fe
Hg
Ni
Be
Cr
Be
Co
V
B. Soils
As, Cu, Se, Tl,
Zn
Al, Ca, Fe, Mg
Sb
Sb
As
Flag
u
u
J
J
JN
u
J
J
J
u
u
R
R
J
Samples Affected
A.11 positives> IDL, but
< CRDL
A.ll positives> IDL, but
< l0X contaminant level
12954, 12955, 12958, 12959,
12 9 6Q / 12961, 12966, 12976,
12982, 12985, 12 9 8 6, 12987
12958, 12982, 12986
12958
12954, 12985
12 98 6
12958, 12986
12954, 12959, 12982, 12985
12 9 67
A.11 positives> IDL, but
< CRDL
A.11 positives> IDL, but
< l0X contaminant level
12949, 12950, 12951_; 12952,
12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977
12978, 12979, 12980, 12981,
12983, 12984
12949, 12950, 12951, 12952,
12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 69%
Blind spike recovery> warning limit
Suspected positive interference from
high levels of Al(lS0,000 ug/L) and
Fe(l20,000 ug/L) in solution
% RSD > 20% for _ICP multiple
exposures and reported results> IDL,
but< CRDL
Only analysis of 2X CRDL standa ·
required by contract sow for
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
standard
for ICP
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Baseline instability
Positives in blanks
Matrix spike recovery 13.0%
Matrix spike recove=y = 25.5%
Matrix S?ike recove=y = 56.7%
Bli~d spike recovery> action limit
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INORGANIC DATA QUALIFIERS REPORT (continued)
I . ..:ase Number: 25655
Project Number: 97-0357
I Site: Rea:sor Chemical, Castle Bayne, NC
~J.ement Flag Sarngles 8ffe~t~d Begsgn
As J 12 97 8, 12979, 12 980, 12981 Matrix spike recovery= 58.6%
I 12983, 12984 Blind spike recovery> action limit
Pb J 1294 9, 12950, 12951, 12952, Matrix spike recovery= 74.3%
12953, 12956, 12957, 12 962,
I 12963, 12964, 12965, 12968,
12 9 69, 12970, 12971, 12973,
12 97 4, 12975, 12976, 12977
I Pb J 12978, 12979, 12980, 12981, Blind spike recovery > warning limit
12983, 12983
Se J 12 9 4 9, 12950, 12957, 12962, Matrix spike recovery 21. 0% I 12 9 64, 12970, 12976
R 12951, 12952, 12 953, 12956
12 9 62, 12963, 12 9 65, 12968,
I 12 9 69, 12 971, 12973, 12 97 4,
12 9 7 5, 12977
Se J 12978, 12979, 12980, 12981, Matrix spike recovery = 68.9%
I 12983, 12 9 84
Al J 12949, 12950, 12951, 12952, Blind spike ::-ecovery > action limit
12953, 12956, 12957, 12 9 62,
I 12 963, 12964, 12 9 65, 12968,
12 969, 12970, 12971, 12973,
12974, 12 97 5, 12976, 12977,
12978, 12979, 12980, 12981,
I 12983, 12984
12 9 4 9, 12950, 12951, 12952, Blind spike action limit Mg J recovery >
12953, 12956, 12957, 12962, I 12963, 12 9 64, 12 9 65, 12968,
12969, 12 97 0, 12971, 12973,
12974·, 12975, 12976, 12 977,
I 12978, 12979, 12 9 8 0, 12981,
12983, 12984
Mn J 12949, 12950, 12951, 12952, Blind spike recovery > action limit
I 12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12 97 3,
12974, 12 97 5, 12976, 12977,
I 12978, 12 97 9, 12980, 12981,
12983, 12984
K J 12951, 12952, 12953, 12956, Blind spike recovery> action limit
I 12957, 12 9 62, 12964, 12965,
12968, 12969, 12970, 12971,
12973, 12 97 4, 12978, 12979,
12 981
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INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number:_,2~5~6~5~5,,_ ____________ _
Project Number:_,9~7~-~0~3~5"--'-7 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
V
Be
Co
Ni
V
K
Be
Cd
Cr
Co
Ni
Zn
Flag
J
u
u
u
u
J
J
J
J
J
J
J
samples Affected
12949, 12950, 12951, 12952,
12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977,
12978, 12979, 12980, 12981,
12983, 12984
12971
12956, 12971
12956
12963
12 9 65, 12970, 12976, 12977
12975
12956
12953
12949, 12950, 12983
12964, 12973
12953, 12 9 64, 12 97 3
12962
Reason
Blind spike recovery> action limit
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
e;,.:posures
CRDL
20% for
and results
20% for
and results
20% for
and results
2 0% for
and results
ICP multiple
> IDL, but <
ICP rnul tiple
> IDL, but <
ICP rnul tip le
> IDL, but <
ICP multiple
> IDL, but
% RSD > 20% for ICP multiple
exposures
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
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:rNORGANIC DATA QUALIFIERS REPORT
Ca3e Number:_,~5~6~5~5"---------------Project Nu.mber:2 9~7~-~0~3~5~7 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element Flag Samples Affected
A. Waters
Sb, As, Be, Cr, u All positives > IDL, but
Pb, Mn, Tl < CRDL
Ba, Ca, Fe, Mg, u All positives > IDL, but
K < lOX contaminant level
Be
Cd
Al
Sb
As
Fe
Se
Ca
Mg
K
Na
CN
JN
JN
J
J
J
J
R
J
J
J
J
J
12871
12871
All
All
All
All
12868,
12872,
12886,
12868,
12 8 72,
12886,
12 8 68,
12872,
12886,
12868,
12872,
12886,
12 8 68,
12872,
12886,
12870
12869, 12870, 12871,
12 8 8 3, 12884, 12885,
12887
12869, 12870, 12 8 71,
12883, 12884, 12885
12887
12869, 12870; 12871,
12883, 12884; 12885
12887
12869, 12870, 12871,
12883, 12884, 12885
12887
12 8 69, 12870, 12871,
12883, 12 8 8 4, 12885
12887
Reason
Baseline instability
Positives in blanks
Suspected positive interference from
high levels of Al and/or Fe (>180,000
ug/L) in solution
Suspected positive interference from
high levels of Fe (>180,000 ug/L) in
solution
Matrix spike recovery= 63.8%
Matrix duplicate RPD 22.7%
Serial dilution percent difference
14.8%
Mat::-ix spike recovery = 60.1%
Matrix spike recovery = 33. 7%
Matrix spike recovery 64.2%
Matrix duplicate RPD 26.8%
Serial dilution percent diffe=ence
17. 9%
Matrix spike recovery = 0%
Serial dilution percent difference
29%
Serial dilution percent difference=
25.3%
Serial dilution percent diffe=ence =
43.6;
Serial dilution percent difference=
15.8%
Sample pH < 12 when received by
laboratory for analysis
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Case Number: 25655
Project Number: 97-0357 I Site: Rea5or Chemical,
~lemeot [lag
I Ag u
I Cd u
I Cd J
I Co J
I Cu J
I Ni J
I V J
I B. Soils
Sb, As, Be, Cr, u
Pb, Mn, Tl
I Ba, Ca, Fe, Mg, u
I Pb JN
I Tl JN
Cd, Ni, Ag JN
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Se J
I Sb J
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INORGANIC DATA QUALIFIERS REPORT (continued)
Castle Bayne, NC
sam2les n.f{ected
12870, 12871
12870, 12883, 12885
12872, 12886
12870, 12883, 12885, 12886,
12S87
12 8 58, 12869, 12886, 12 887
12870, 12886
12868, 12869, 12884, 12887
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
12873
12873
12873
12873
12 8 7 3,
12877,
12 8 81,
12874,
12878,
12882
12875,
12 8 7 9,
12876,
12 8 8 0,
BeasQn
% RSD > 2 0% for ICP multiple
exposures and reported result > IDL,
but < CRDL
% RSD > 20% for ICP multiple
exposures and reported result > IDL,
but < CRDL
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW foe rr
analysis
Only analysis of 2X CRDL standard
=equired by contract sow for ICP
analysis
Baseline instability
Positives in blanks
Suspected positive interference as
noted in the contractor !CS
Suspected positive interference as
noted in the contractor ICS
Suspected positive interference from
high levels of Fe (> 350,000 ug/LJ in
solution
Suspected over correction as noted in
the contractor res
Matrix spike recovery 57. 9%
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• Case Number: 5655
Project Number: 97 0357
Site: Reasor Chemical,
Element Flag
Se J
Pb J
Ba J
Ca J
Mg J
Mn J
K J
Cd u
Cd J
Co J
Cu J
Ni J
V J
INORGANIC DATA QUALIFIERS REPORT (continued)
Castle Bayne, NC
Samples Affected
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12880,
12881, 12882
12873, 12874, 12 87 5, 12876,
12877, 12878, 12879, 12 8 8 0,
12881, 12882
12873, 12874, 12875, 12876,
12 877, 12878, 128 7 9, 12 8 8 0,
12881, 12882
12873, 12874, 12875, 12876,
12877, 12 8 7 8, 12 8 7 9, 12 8 8 0,
12 8 81, 12882
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12 8 8 0,
12881, 12 8 82
12 87 3, 12 8 7 4, 12875, 12876,
12877, 12878, 12879, 12380,
12 8 81, 12 8 82
12873, 12874, 12875, 12 8 7 6,
12877, 12878, 12879, 12880,
12 8 8 l, 12882
12874, 12876
12877, 12878, 12879, 12881
12873, 12874, 12877, 12878,
12875
12876, 12879, 12880, 12881,
12882
12874, 12875, 12877, 12878
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12880,
12881, 12882
Reason
Matrix spike recovery 53.5%
Erix duplicate RPD = 49. 7% /
Serial dilution percent difference
23%
serial dilution percent difference
10.6%
Serial dilution percent difference=
63.3%
Serial dilution percent difference
51%
Blind spike recovery> warning limit
% RSD > 20% for ICP multiple
exposures and reported =esult > IDL,
but< CRDL
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for
ICP analysis
Only analysis
required by
analysis
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
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~~~} UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
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◄t PAO~C,.,_
MEMORANDUM
Date: 11/20/97
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Sample Analysis
97-0357 REASOR CHEMICAL
CASTLE HAYNE, NC
From: Keith Bates J:t-ff lJ,~
To: RAY DOYLE
Thru: OA Office
.Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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'TTACHMENT
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BY-~
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INORGANIC DATA QUALIFIERS REPORT
;ase Number:~=6~5~5~-------------
Project Number:~9~7_-~0~3~5~7~-----------
Site: Reasor Chemical, Castle Bayne, NC
Element
A. Waters
As, Cu, Se, Tl,
Zn
P..l, Ca, Fe
Hg
Ni
Be
Cr
Be
Co
V
B. Soils
P.s, Cu, Se, Tl,
Zn
Al, Ca, ~Q Mg . -'
Sb
Sb
P..s
Flag
u
u
J
J
JN
u
J
J
J
u
u
R
R
J
samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12954, 12955, 12 9 5 8, 12959,
12 960, 12961, 12966, 12976,
12 9 8 2, 12985, 12986, 12 987
12958, 12982, 12 98 6
12958
12954, 12985
12986
12958, 12986
12954, 12959, 12982, 12985
12967
All positives> IDL, but
< CRDL
All positives> IDL, but
< l0X contaminant level
12949, 12950, 12951_; 12952,
12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977
12978, 12979, 12980, 12981,
12983, 12984
12949, 12950, 12951, 12952,
12953, 12956, 12957, 12962,
12963, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 69%
Blind spike recovery> warning limit
Suspected positive inte=fe=ence from
high levels of Al(l80,000 ug/L) and
Fe(l20,000 ug/L) in solution
% RSD > 20% for ,ICP multiple
exposures and reported results> IDL,
but< CRDL
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
standard
for ICP
standard
for ICP
Only analysis
requirec:! by
analysis
of 2X CRDL standard
~ontract sow for ICP
Baseline instability
Positives in blanks
Matrix spike recovery 13.0%
Matrix spike recovery 25.5%
Matrix spike recovery= 56.7%
Blind spike recovery> action li~~t
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INORGANIC DATA QUALIFIERS REPORT (continued) I Case Number: 5655
Project Number: 97-0357
I Site: Reasor Chemical, Castle Bayne, NC
~lement Flag Sam:gles A{{ec:!;,ed Bea~on
As J 12978, 12979, 12980, 12981 Matrix spike recovery= 58.6%
I 12983, 12984 Blind spike recovery > action limit
Pb J 12949, 12950, 12951, 12952, Matrix spike 74.3% recovery=
12 953, 12956, 12957, 12962,
I 12 9 63, 12964, 12965, 12968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977
I Pb J 12978, 12979, 12980, 12981, Blind spike recovery> warning limit 12 983, 12983
I Se J 12949, 12950, 12957, 12 962, Matrix spike recovery 21.0%
12964, 12970, 12976
R 12951, 12952, 12953, 12956
12962, 12963, 12965, 12 968,
I 12969, 12971, 12973, 12974,
12975, 12977
Se J 12 97 8, 12979, 12980, 12981, Matrix spike recovery 68.9%
I 12983, 12984
Al J 12949, 12950, 12951, 12952, Blind spike recove.:-y > action limi..,..
12953, 12956, 12957, 12 9 62 /
I 12963, 12 964, 12965, 12968,
12 9 69, 12970, 12971, 12973,
12 97 4, 12975, 12976, 12977,
12978, 12979, 12980, 12981, I 12983, 12984
Mg J 12949, 12950, 12951, 12952, Blind spike recovery> action limit
I 12953, 12956, 12957, 12962,
12963, 12964, 12 965, 12968,
12969, 12970, 12971, 12973,
12 97 4, 12 97 5, 12 9 7 6, 12977,
I 12978, 12979, 12980, 12981,
12983, 12984
Mn J 12949, 12950, 12951, 12952, Blind spike recovery > action limit
I 12 953, 12956, 12957·, 12962,
12963, 12964, 12965, 12 968,
12969, 12970, 12971, 12973,
12974, 12975, 12976, 12977,
I 12978, 12979, 12980, 12981,
12983, 12984
K J 12951, 12952, 12953, 12956, Blind spike recovery> action limit I 12957, 12 962, 12964, 12 9 65,
12968, 12969, 12970, 12 971,
12973, 12974, 12978, 12979,
I 12981
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I Case Number: 25655
Project Number: 97-0357
I Site: Rea:,or Chemical 1
Element Flag
V J
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I Be u
I Co u
I Ni u
I V u
I K J
I Be J
I Cd J
I Cr J
I Co J
I Ni J
I Zn J
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INORGANIC DATA QUALIFIERS REPORT (continued)
Castle Bayne, NC
samples Affected
12949, 12950, 12 9 51,
12953, 12956, 12957,
12 9 63 I 12964, 12965,
12 969, 12970, 12971,
12974, 12975, 12976,
12978, 12979, 12980,
12983, 12984
12971
12956, 12971
12956
12963
12965, 12970, 12976,
12975
12956
12953
12949, 12950, 12983
12964, 12973
12953, 12 964, 12973
12962
12952,
12962,
12968,
12973,
12977,
12981,
12 977
Reason
Blind spike recovery> action limit
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
% RSD >
exposures
CRDL
20% for
and results
20% for
and results
20% for
and results
20% for
and results
ICP multiple
> IDL 1 but <
ICP rnul tiple
> IDL, but <
ICP multiple
> IDL, but <
ICP rnul tiple
> IDL, but <
% RSD > 2 0% for ICP multiple
exposures
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract SOW for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis of 2X CRDL standard
requi~ed by contract SOW for ICP
analysis
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_,2~5~6~5~5"----------------
Project Number:~9~7~-~0~3~5=7 __________ _
Site: Reasor Chemical, Castle Hayne, NC
Element flag Samples Affected
A. Waters
Sb, As, Be, Cr, u All positives > IDL, but
Pb, Mn, Tl < CRDL
Ba, Ca, Fe, Mg, u All positives > IDL, but
K < lOX contaminant level
Be
Cd
Al
Sb
As
Fe
Se
Ca
Mg
K
Na
CN
JN
JN
J
J
J
J
R
J
J
J
J
J
12871
12 871
All
All
All
All
12 8 68,
12872,
12886,
12868,
12872,
12886,
12868,
12872,
12886,
12868,
12872,
12886,
12868,
12872,
12886,
12870
12869, 12870, 12 871,
12883, 12884, 12885,
12887
12869, 12870, 12871,
12883, 12884, 12885
12887
12869, 12 87 0; 12 8 71,
12883, 12884, 12 8 85
12887
12869, 12870, 12871,
12883, 12 8 8 4, 12885
12887
12869, 12870, 12871,
12883, 12884, 12885
12887
Reason
Baseline instability
Positives in blanks
Suspected positive interference from
high levels of Al and/or Fe (>180,000
ug/L) in solution
Suspected positive interference from
high levels of Fe (>180,000 ug/L) in
solution
Matrix spike recovery= 63.8%
Matrix duplicate RPD 22.7%
Serial dilution percent difference=
14.8%
Matrix spike recovery 60.1%
Matrix spike recovery 33. 7%
Matrix spike recovery 64.2%
Matrix duplicate RPD 26.8%
Serial dilution percent difference
17.9%
Mat=ix spike recovery 0%
Serial dilution percent difference=
29%
Serial dilution percent difference
25.3%
Serial dilution percent difference
43.6%
Serial dilution percent difference=
15.8%
Sample pH < 12 when received
laboratory for analysis
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INORGANIC DATA QUALIFIERS REPORT (continued)
;ase Number: _.2.,S"-"6~Ss,S,_ _____________ _
Project Number:_;9~7~-=0~3~5~7,__ ___________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
Ag
Cd
Cd
Co
Cu
Ni
V
B. Soils
Sb, As, Be, Cr,
Pb, Mn, Tl
Ba, Ca, Fe, Mg,
Pb
Tl
Cd, Ni, Ag
Se
Sb
Flag
u
u
J
J
J
J
J
u
u
JN
JN
JN
J
J
Samples .Z\ffected
12870, 12871
12870, 12883, 12885
12872, 12886
12870,
12887
12 8 S 3, 12885, 12 8 8 6,
12868, 12869, 12886, 12887
12870, 12886
12868, 12869, 12884, 12887
~il positives> IDL, but
< CRDL
Afl positives> IDL, but
< lOX conta~inant level
12 87 3
12873
12873
12873
12873,
12877,
12881,
12874,
12878,
12882
12875,
12879,
12876,
12880,
Reason
% RSD > 20% for ICP multiple
exposures and reported result> IDL,
but< CRDL
% RSD > 2 0% for ICP multiple
exposures and reported result> IDL,
but< CRDL
Only analysis of 2X CRDL
required by contract sow
analysis
standard
for ICP
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract SOW
analysis
Only analysis of 2X CRDL
required by contract sow
analysis
Baseline instability
Positives in blanks
standard
for ICP
standard
for ICP
standard
for ICP
Suspected positive interference as
noted in the contractor ICS
Suspected positive interference as
noted in the contractor ICS
Suspected positive interference from
high levels of Fe (> 350,000 ug/L) in
solution
Suspected over correction as noted in
the contractor res
Matrix spike ~ecovery 57. 9%
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Case Number: 25655
Project Number: 97-0357
Site: Reasor Chemical,
Element Flag
Se J
Pb J
Ba J
Ca J
Mg J
Mn J
K J
Cd u
Cd J
Co J
Cu J
Ni J
V J
INORGANIC DATA QUALIFIERS REPORT (continued)
Ca:stle Hayne, NC
Sam12les Affected
12873, 12 87 4, 12875, 12 876,
12877, 12878, 12879, 12880,
12881, 12882
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12 8 8 0,
12 8 81, 12882
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12 8 8 0,
12881, 12882
12873, 12874, 12 87 5, 12876,
12877, 12878, 12 879, 12880,
12 8 81, 12882
12873, 12874, 12 87 5, 12 87 6,
12877, 12878, 12879, 12880,
12881, 12882
12873, 12874, 12875, 12876,
12877, 12 8 7 8, 12879, 12880,
12881, 12882
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12880,
12881, 12882
12874, 12876
12877, 12878, 12879, 12881
12873, 12874, 12877, 12878,
12875
12876, 12879, 12880, 12881,
12882
12874, 12875, 12877, 12878
12873, 12874, 12875, 12876,
12877, 12878, 12879, 12880,
12881, 12882
Reason
Matrix spike recovery = 53.5%
Matrix duplicate RPD 49. 7%
Serial dilution percent difference
23%
Serial dilution percent difference
10.6%
Serial dilution percent diffe=ence =
63.3%
Serial dilution percent difference
51%
Blind spike .:-ecovery > warning limit
% RSD > 2 0% for ICP multiple
exposures and
but < CRDL
Only analysis
required by
analysis
repo.:-ted result > IDL,
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standard
required by contract sow for
ICP analysis
Only analysis of 2X CRDL standard
required by contract sow for ICP
analysis
Only analysis
.r-equired by
analysis
of 2X CRDL standard
contract SOW for ICP
Only analysis of 2X CRDL standard
required by contract SOW for IC?
analysis
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I MEMORANDUM
I Date: 12/01/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I
Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0386 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Thru: OA Office
'ttached are the results of analysis of samples collected as part of the subject project.
luestions, please contact me.
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ITTACHMENT
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It you have any
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ORGANIC DATA QUALIFIER REPORT
Case Number 25648 Project Number 97-0386 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Affected Samples
Volatiles
12997
12998
Extractables
all samples
Pesticides
all samples
·comDound or Fraction
benzene J
toluene J
ethylbenzene J
acetone J
N
3-nitroaniline J
endosulfan II R
Flag
Used Reason
< quantitation limit
< guantitation limit
< quantitation limit
erratic response factor
common lab contaminant
warning low on PE sample
missed on PE sample
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::,,i~~ 57-41~.!' . ft . I
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
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MEMORANDUM
Date: 12/01/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
97-0386 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Th ru: QA Office
I Attached are the results oi analysis of samples collected as part of the subject project.
questions, please contact me.
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I ATTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25648 Project Number 97-0386 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Affected Samoles ·compound or Fraction
Volatiles
12997 benzene J
toluene J
ethylbenzene J
12998 acetone J
N
Extractables
all samples 3-nitroaniline J
Pesticides
all samples endosulfan II R
Flag
Used Reason
< quantitation limit
< quantitation limit
< quantitation limit
erratic response factor
common lab contaminant
warning low on PE sample
missed on PE sample
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~-;ED sr"-rc.r . ft .
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'°'i PAO~c;'-
MEMORANDUM
Date 12/01/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject Results of EXTRACTABLES ORGANIC Sample Analysis
97-0386 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To RAY DOYLE
. Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project. If you have any
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questions, please contact me.
.ATTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25648 Project Number 97-0386 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
Affected Samples
Volatiles
12997
12998
Extractables
all samples
Pesticides
all samples
·compound or Fraction
benzene J
toluene J
ethylbenzene J
acetone J
N
3-nitroaniline J
endosulfan II R
Flag
Used Reason
< quantitation limit
< quantitation limit
< quantitation limit
erratic response factor
common lab contaminant
warning low on PE sample
missed on PE sample
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Region 4
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MEMORANDUM
Date: 12/03/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
7) I() Yr/JS
Subject: Results of DIOXINS ORGANIC Sample Analysis
97-0358 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
, Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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I ATTACHMENT
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DATA QUALIFIER REPORT
97-0358 Project No.
Site Name: Reasor Chemical, Castle Hayne, NC
Affected
Samples
All
Analvte
Total congeners
Flag
.D.s..e..d
J
Reason
As.:;umed Resp.
Factors/ Cal. Stds
not available for
all congeners
13005 1,2,3,6,7,8-HxCDD, J Low internal
standard recovery 1,2,3,7,8,9-HxCDD, HpCDD,
TCDF
13006
13007
13008
13009
13010
13011
OCDD
HpCDD
HpCDD
OCDD
OCDD
HpCDD
1,2,3,7,8,9-HxCDD
J
J
J
J
J
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2
1
1
1
1
1
1
TEQ's : The Toxic Equivalent (TEQ) represents a summation of values from the
individual equivalents that are calculated for each of the 2,3,7,8 containing
isomers. If 10% or greater of the TEQ value was from data considered to be
estimated, then the TEQ is reported as estimated (J flag) ..
Abbreviation Kev:
TCDD Tetrachlorodibenzodioxin TCDF
PeCDD
HxCDD
HpCDD
OCDD
IS
Pentachlorodibenzodioxin
Hexachlorodibenzodioxin
Heptachlorodibenzodioxin
Octachlorodibenzodioxin
= Internal Standard
Reason Codes=
?eCDF
1-'.xCDF
HpCDF
OCDF
Tetrachlorodibenzofuran
Pentachlorodibenzofuran
Hexachlorodibenzofuran
Heptachlorodibenzofuran
Octachlorodibenzofuran
1. Results lower than the minimum quantitation limit
2. Results higher than the maximum calibration limit
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I MEMORANDUM
I Date: 12/08/97
Subject: Results of DIOXINS ORGANIC Sample Analysis I 97-0370 REASOR CHEMICAL
CASTLE HAYNE, NC
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From: John Mcconney
To: RAY DOYLE
Thru: QA Office
Y1()X!AJ5 "
~~IL
lttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
If you have any
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ATTACHMENT I
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I DATA QUALIFIER REEQRT
Project No.: 97-0370
I Site Name: Reasor Chemical, Castle Hayne, NC
Affects:d Flag
I Samgles Arn,lyte Used Reason
l.\.ll Total congeners J Assumed Resp.
Factors/ Cal. Stds I not available for
all congeners
I 13 013 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE
PeCD?, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in Pi::
I sample
l,2,3,4,6,7,8-HpCDD J 1
13014 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE ,I PeCDF, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in PE
I sample
1,2,3,6,7,8-HxCDD, J 1
1,2,3,7,8,9-HxCDD
I 13015, 13016 TCDD, Total TCDD,PeCDD, UR Low recovery in p~
-J:,
2,3,4,7,8-PeCDF, sample
2,3,4 1 6,7 1 8-HxCDF I 13016 OCDD J Low recovery in PE
sample
I HpCDD J 1
13017 TCDD, 2,3,4,7,8-PeCDF, UR Low recovery in PE
2,3,4,6,7,8-HxCDF sample
I OCDD J Low recovery in PE
sample
PeCDD, HpCDD J 1 I 13018 TCDD, Total TCDD,PeCDD, UR Low recovery in PE
2,3,4,7,8-PeCDF, sample
I 2,3,4,6,7,8-HxCDF
OCDD J Low recovery in PE
sample
I HpCDD, 1,2,3,4:6,7,8-J 1
HpCD?
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I \ DATA QUALIFIER REPORT
Project No.: 97-0370
I Site Name: Reasor Chemical, Castle Hayne, NC
Affected Flag
I S9mole:,; Analvt;e Used Reason
13019 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE
I
PeCDF, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in PE
sample
I HpCDD J 1
13020 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE
PeCDF, 2,3,4,6,7,8-HxCDF sample
I OCDD J Low recovery in PE
sample
I OCDF J 1
13021 TCDD, PeCDD, 2,3,4,718-UR Low recovery ln PE
PeCDF, 2,3,4,6,7,8-HxCDF sample
I OCDD J Low recovery in PE
sample
1,2,3,7,8,9-HxCDD J 1
I 13022 TCDD, 2,3,4,7,8-PeCDF, UR Low recovery in PE
2,3,4,6,7,8-HxCDF sample
I OCDD J Low recovery in PE
sample
PeCDD J 1
I 13023 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery ln PE
PeCDF, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in PE
I sample
HpCDD J 1
I 13024 TCDD, PeCDD UR Low recovery in PE
sample
OCDD, 2,3,4,6,7,8-HxCDF, J Low recovery ln PE
I 1,2,3,4,7,8,9-HpCDF, OCDF sample
All HxCDD, All PeCDF J 1
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I )2ATA QU?.LIFIER !l,EPQRT
Project No.: 97-0370
I Site-Name: Reasor Chemical, Castle Hayne, NC
Affected Flag
I Samoles .21.naly!;e Used Rea:.Qn
13025 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE
PeCDF sample
I OCDD, OCDF J Low recovery in PE
sample
I 1,2,3,4,7,8-HxCDF, J Low recovery in PE
2,3,4,6,7,8-HxCDF sample
13026 TCDD, Total TCDD, PeCDD, UR Low recovery in PE
I 2,3,4,7,8-PeCDF sample
OCDD, OCDF J Low recovery in PE
sample
I HpCDD, TCDF, 1,2,3,4,7,8-J 1
HxCDF, 2,3,4,6,7,8-HxCDF
I 13027 TCDD, PeCDD, 2,3,4,7,8-UR Low recovery in PE
PeCDF sample
OCDD, 2,3,4,6,7,8-HxCDF, J Low recovery in PE
I OCDF sample
1,2,3,6,7,8-HxCDD, J 1
l,2,3,7,8,9-HxCDD, TCDF,
I 1,2,3,7,8-PeCDF,
1,2,3,4,7,8,9-HpCDF
I 13028 TCDD, Total TCDD, PeCDD UR Low recovery in PE
sample
OCDD, OCDF J Low recovery in PE
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HpCDD, TCDF, 2,3,4,7,8-J 1
PeCDF, 1,2,3,4,7 1 8-HxCDF,
I 2,3,4,6,7,8-HxCDF,
1,2,3,4,7,8,9-HpCDF
13029 TCDD, 2,3,4,7,8-PeCDF, UR Low recovery in PE
I 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in PE
I sample
PeCDD, HpCDD, J 1
1,2,3,4,6,7,8-HpCDF, OCDF
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\ DATA QUALIFIER REPORT
Project No. 97-0370
Site Name: Reasor Chemical, ·Castle Hayne, NC
Affected Flag
Samglea; bnal.,:J;e Used R(aa§Qn
13030 TCDD, Total TCDD, PeCDD UR Low recovery in
sample
OCDD J Low recovery in
sample
1,2,3,6,7,8-HxCDD, TCDF, J 1
2,3,4,7,8-PeCDF,
2,3,4,6,7,8-HxCDF, OCDF
13031 TCDD, PeCDD, 2,314,7,8-UR Low recovery in
PeCDF, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in
sample
1,2,3,7,8,9-HxCDD J 1
13 032 TCDD, PeCDD, 2,314,7,8-UR Low recovery in
PeCDF, 2,3,4,6,7,8-HxCDF sample
OCDD J Low recovery in
sample
HpCDD J 1
TEQ 1 s : The Toxic Equivalent (TEQ) represents a summation of values from the
individual equivalents that are calculated for each of the 2,3,7,8 containing
isomers. If 10% or greater of the TEQ value was from data considered to be
estimated, then the TEQ is reported as estimated {J flag).
.~breviation Kev:
TCDD Tetrachlorodibenzodioxin
PeCDD Pentachlorodibenzodioxin
HxCDD Hexachlorodibenzodioxin
HpCDD Heptachlorodibenzodioxin
OCDD Octachlorodibenzodioxin
IS = Internal Standard
Reason Codes:
TCD?
PeCDF
HxCD?
HpCDF
OCD?
Tetrachlorodibenzofuran
Pentachlorodibenzofuran
Hexachlorodibenzofuran
Heptachlorodibenzofuran
Octachlorodibenzofuran
1. Results lower than the minimum quantitation limit
2. Results higher than the maximum calibration limit
PE
PE
PE
PE
PE
PE
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MEMORANDUM
Date: 12/11/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0357 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Thru: QA Office
<S
Attached are the results of analysis of samples collected as part of the subject project. If you have any I questions, please contact me.
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ORGANIC DATA QUALIFIER REPORT
case Number 25655 Project Number97-0357 SAS Number
Site ID.Reasor Chemical, Castle Hayne, NC
Affected.Samples
Volatiles
12870
12871
12875
12886
12888,12892,
12913, 12932,
12935,12941,
12949,12952,
12975,12983
12889
12890,12893,
12900,12906
12913
12915
12916
12917,12923,
12924,12925,
12953,12984
12917
Compound or Fraction
benzene
carbon disulfide
toluene
toluene
xylene
Flag
Used
J
J
J
J
J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
ethylbenzene
xylene
xylene
chloroform
ethylbenzene
chloromethane
J
J
J
J
J
J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
1,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cie-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
chloroform J
Reason
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
< quantitation limit
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ORGANIC DATA QUALIFIER REPORT
Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
12918
12920
12927,12929,
12930
12935,12936
12936
12939
12942,12944
12955
12956
12962
12963
12967
12969
12973
12974
12979
12980
12981
12982
12983
12985,12986,
12989,12991,
13776
13683
ethylbenzene
xylene
all volatiles
chloromethane
methylene chloride
acetone
chloroform
benzene
xylene
all volatiles
chloromethane
2-butanone
xylene
tetrachloroethene
chloromethane
toluene
carbon disulfide
benzene
acetone
trichloroethene
benzene
toluene
xylene
toluene
xylene
chloromethane
benzene
chloromethane
toluene
J
J
J
J
N
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
common lab contaminant
outside calibration range
< quantitation limit
< quantitation limit
< quantitation limit
low surrogate recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
erratic response factor
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
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Affected Samples
Extractablee
12868-12884,
12886-12893,
12895-12897,
12899-12903,
12905,12906,
12910,
12934-12946
12871,12884,
12906
12873
12888
12888,12891
12899
12901
12906
12913
12915,12918
12918
12919
12927-12929
12932
ORGANIC DATA QUALIFIER
case Number 25655
Flag
Compound or Fraction Used
2,4-dimethylphenol J
4-bromophenyl-phenylether J
all base/neutrals J
phenanthrene J
anthracene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
4-methylphenol
phenanthrene
f 1 uoranthene
pyrene
acenaphthylene
phenanthrene
anthracene
fluoranthene
benzo(a)pyrene
naphthalene
2-methylphenol
naphthalene
2-methylnaphthalene
phenanthrene
fluoranthene
chrysene
4-methylphenol
2-methylnaphthalene
naphthalene
acenaphthene
dibenzofuran
fluorene
phenanthrene
fluoranthene
pyrene
all compounds
4-methylphenol
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
REPORT
Reason
warning low on PE sample
warning low on PE sample
low surrogate recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitati~n limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quan~itation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
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ORGANIC DATA QUALIFIER REPORT I Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
I 12935 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I 12936 2-methylphenol J < quantitation limit
4-methylphenol J < quantitation limit
phenanthrene J < quantitation limit
I 12938 acenaphthylene J < quantitation limit
phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I 12939 acenaphthylene J < quantitation limit
phenanthrene J < quantitation limit
anthracene J < quantitation limit
I fluoranthene J < quantitation limit
12940 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
I pyrene J < quantitation limit
12941 acenaphthylene J < quantitation limit
anthracene J < quantitation limit
I benzo{a}anthracene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quantitation limit
dibenzo(a,h)anthracene J < quantitation limit
benzo(g,h,i)perylene J < quantitati:m limit
I 12943 fluoranthene J < quantitation limit
pyrene J < quantitation limit
12944 phenanthrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
I benzo(g,h,i)perylene J < quantitation limit
12967 pyrene J low internal standard recovery
butylbenzylphthalate J low internal standard recovery
I 3,3'-dichlorobenzidine J low internal standard recovery
benzo(a)anthracene J low internal standard recovery
bis(2-ethylhexyl)phthalate J low internal standard recovery
chrysene J low internal standard recovery
I di-n-octylphthalate J low internal standard recovery
benzo(b/k)fluoranthene J low internal standard recovery
benzo(a)pyrene J low internal standard recovery
indeno(l,2,3-cd)pyrene J low internal standard recovery
dibenz(a,h)anthracene J low internal standard recovery I benzo(g,h,i)perylene J low internal standard recovery
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ORGANIC DATA QUALIFIER REPORT
Case Number 25655
l"lag
Affected Samples Compound or Fraction Used Reason
12984
13776
pesticides
12941
12949
12956
13776
phenanthrene J
fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate
chrysene J
all compounds J
4,4'-00T N
endrin ketone J
endrin N
4,4'-00T N
all compounds J
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
J low internal standard recovery
low internal standard recovery
exceeded holding times
difference in columns
< quantitation limit
difference in columns
difference in columns
exceeded holding times
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
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MEMORANDUM
Date: 12/11/97
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
97-0357 REASOR CHEMICAL
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CASTLE HAYNE, NC
From: John Mcconney ~~
To: RAY DOYLE
Thru: QA Office
.Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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rTTACHMENT
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If you have any
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I ORGANIC DATA QUALIFIER REPORT
Case Number 25655 Project Number97-0357 SAS Number
Site ID.Reasor Chemical, castle Hayne, NC
I Flag
Affected·samples Compound or Fraction Used Reason
I Volatiles
12870 benzene J < quantitation limit
12871 carbon disulfide J < quantitation limit
toluene J < quantitation limit I 12875 toluene J < quantitation limit
12886 xylene J < quantitation limit
I 12888, 12892, 4-rnethyl-2-pentanone J low internal standard recovery
12913,12932, 2-hexanone J low internal standard recovery
12935,12941, tetrachloroethene J low internal standard recovery
I 12949,12952, 1,1,2,2-tetrachloroethane J low internal standard recovery
12975,12983 toluene J low internal standard recovery
chlorobenzene J low internal standard recovery
ethylbenzene J low internal standard recovery
I styrene J low internal standard recovery
xylene J low internal standard recovery
12889 ethylbenzene J < quantitation limit
I xylene J < quantitation limit
12890,12893, xylene J < quanti tat ion limit
12900,12906
I 12913 chloroform J < quantitation limit
12915 ethylbenzene J < quantitation limit
I 12916 chloromethane J < quantitation limit
12917,12923, 1,1,1-trichloroethane J low internal standard recovery
I . 12924,12925, carbon tetrachloride J low internal standard recovery
12953,12984 bromodichloromethane J low internal standard recovery
1,2-dichloropropane J low internal standard recovery
trans-1,3-dichloropropene J low internal standard recovery
I trichloroethene J low internal standard recovery
dibromochloromethane J low internal standard recovery
1,1,2-trichloroethane J low internal standard recovery
benzene J low internal standard recovery
I cie-1,3-dichloropropene J low internal standard recovery
bromoform J low internal standard recovery
4-rnethyl-2-pentanone J low internal standard recovery
2-hexanone J low internal standard recovery
I tetrachloroethene J low internal standard recovery
1,1,2,2-tetrachloroethane J low internal standard recovery
toluene J low internal standard recovery
chlorobenzene J low internal standard recovery
I ethylbenzene J low internal standard recovery
styrene J low internal standard recovery
xylene J low internal standard recovery
I 12917 chloroform J < quantitation limit
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ORGANIC DATA QUALIFIER REPORT
Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
12918
12920
12927,12929,
12930
12935,12936
12936
12939
12942,12944
12955
12956
12962
12963
12967
12969
12973
12974
12979
12980
12981
12982
12983
12985,12986,
12989,12991,
13776
13683
ethylbenzene
xylene
all volatiles
chloromethane
methylene chloride
acetone
chloroform
benzene
xylene
all volatiles
chloromethane
2-butanone
xylene
tetrachloroethene
chloromethane
toluene
carbon disulfide
benzene
acetone
trichloroethene
benzene
toluene
xylene
toluene
xylene
chloromethane
benzene
chloromethane
toluene
J
J
J
J
N
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
< guantitation limit
< guantitation limit
exceeded holding ti.mes
< guantitation limit
common lab contaminant
outside calibration range
< guantitation limit
< quantitation limit
< guantitation limit
low surrogate recovery
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
erratic response factor
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
I
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Affected Samples
Extract ables
12868-12884,
12886-12893,
12895-12097,
12899-12903,
12905,12906,
12910,
12934-12946
12871, 12884,
12906
12873
12888
12888,12891
12899
12901
12906
12913
12915,12918
12918
12919
12927-12929
12932
ORGANIC DATA QUALIFIER
Case Number 25655
Flag
Compound or Fraction Used
2,4-dimethylphenol J
4-bromophenyl-phenylether J
all base/neutrals J
phenanthrene J
anthracene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chryeene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo(g,h,i)perylene J
4-methylphenol J
phenanthrene
fluoranthene
pyrene
acenaphthylene
phenanthrene
anthracene
fluoranthene
benzo(a)pyrene
naphthalene
2-methylphenol
naphthalene
2-methylnaphthalene
phenanthrene
fluoranthene
chrysene
4-methylphenol
2-methylnaphthalene
naphthalene
acenaphthene
dibenzofuran
fluorene
phenanthrene
fluoranthene
pyrene
all compounds
4-methylphenol
J
J
J
J
J
J
J
J
\
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
REPORT
Reason
warning low on PE &ample
warning low on PE sample
low surrogate recovery
< quantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitati~n limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< guantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< guantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
I
I
ORGANIC DATA QUALIFIER REPORT
I Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
12935 phenanthrene J < quantitation limit I fluoranthene J < quantitation limit
pyrene J < quanti tat ion limit
12936 2-methylphenol J < quantitation limit I 4-methylphenol J < quantitation limit
phenanthrene J < quantitation limit
12938 acenaphthylene J < quantitation limit I phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I 12939 acenaphthylene J < quantitation limit
phenanthrene J < quantitation limit
anthracene J < quantitation limit
fluoranthene J < quantitation limit I 12940 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit I 12941 acenaphthylene J < quantitation limit
anthracene J < quantitation limit
benzo(a)anthracene J < quantitation limit
I chryeene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit I dibenzo(a,h)anthracene J < quantitation limit
benzo(g,h,i)perylene J < quantitation limit
12943 fluoranthene J < quantitation limit
I pyrene J < quantitation limit
12944 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
I pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit n benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz(a,h)anthracene J < quantitation limit
benzo(g,h,i)perylene J < quantitation limit
R 12967 pyrene J low internal. standard recovery
butylbenzylphthalate J low internal standard recovery
3,3'-dichlorobenzidine J low internal standard recovery
I benzo(a}anthracene J low internal standard recovery
bis(2-ethylhexyl)phthalate J low internal standard recovery
chrysene J low internal standard recovery
di-n-octylphthalate J low internal standard recovery
I benzo(b/k)fluoranthene J low internal standard recove:r-y
benzo(a)pyrene J low internal standard recovery
indeno(l,2,3-cd)pyrene J low internal standard recovery
dibenz(a,h}anthracene J low internal standard recovery
I benzo(g,h,i)perylene J low internal standard recovery
I \ '0%
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R
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I
Affected Samples
12984
13776
Pesticides
12941
12949
12956
13776
ORGANIC DATA QUALIFIER
Case Number 25655
Flag
Compound or Fraction Used
phenanthrene J
fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate J
chrysene J
all compounds J
4,4'-DDT N
endrin ketone J
endrin N
4,4'-DDT N
all compounds J
REPORT
Reae:m
< quantitation limit
< quantitation limit
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
exceeded holding times
difference in columns
< quantitation limit
difference in columns
difference in columns
exceeded holding times
I
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~~Bl
• ~~ UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
I Date: 12/11 /97
I Subject: Results of EXTRACTABLE$ ORGANIC Sample Analysis
97-0357 REASOR CHEMICAL
I
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CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Thru: QA Office
Attached are the results of analysis of samples collected as part of the subject project If you have any
~uestions, please contact me.
I
I .
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ITTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25655 Project Number97-0357 SAS Number
Site ID.Reasor Chemical, Castle Hayne, NC
Affected Samples
Volatiles
12870
12871
12875
12886
12888,12892,
12913,12932,
12935,12941,
12949,12952,
12975,12983
12889
12890,12893,
12900,12906
12913
12915
12916
12917,12923,
12924,12925,
12953,12984
12917
Compound or Fraction
benzene
carbon disulfide
toluene
toluene
xylene
J
J
J
Flag
Used
J
J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
ethylbenzene J
xylene J
xylene J
chloroform J
ethylbenzene J
chloromethane J
1,1,1-trichloroethane J
carbon tetrachloride J
bromodichloromethane J
l,2-dichloropropane J
trans-1,3-dichloropropene J
trichloroethene J
dibromochloromethane J
1,1,2-trichloroethane J
benzene J
cie-1,3-dichloropropene J
bromoform J
4-methyl-2-pentanone J
2-hexanone J
tetrachloroethene J
1,1,2,2-tetrachloroethane J
toluene J
chlorobenzene J
ethylbenzene J
styrene J
xylene J
chloroform J
Reason
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
low internal standard
< quantitation limit
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
recovery
\ \ \
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ORGANIC DATA QUALIFIER REPORT
Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
12918
12920
12927,12929,
12930
12935,12936
12936
12939
12942,12944
12955
12956
12962
12963
12967
12969
12973
12974
12979
12980
12981
12982
12983
12985,12986,
12989,12991,
13776
13683
ethylbenzene
xylene
all volatiles
chloromethane
methylene chloride
acetone
chloroform
benzene
xylene
all volatiles
chloromethane
2-butanone
xylene
tetrachloroethene
chloromethane
toluene
carbon disulfide
benzene
acetone
trichloroethene
benzene
toluene
xylene
toluene
xylene
chloromethane
benzene
chloromethane
toluene
J
J
J
J
N
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
common lab contaminant
outside calibration range
< guantitation limit
< quantitation limit
< guantitation limit
low surrogate recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation iimit
< quantitation limit
< quantitation limit
< quantitation limit
erratic response factor
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
I
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B
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I
Affected Samples
Extract ables
12868-12884,
12886-12893,
12895-12897,
12899-12903,
12905,12906,
12910,
12934-12946
12871,12884,
12906
12873
12888
12888,12891
12899
12901
12906
12913
12915,12918
12918
12919
12927-12929
12932
ORGANIC DATA QUALIFIER
Case Number 25655
Flag
Compound or Fraction Used
2,4-dimethylphenol J
4-bromophenyl-phenylether J
all base/neutrals J
phenanthrene J
anthracene J
fluoranthene J
pyrene J
benzo(a)anthracene J
chrysene J
benzo(b/k)fluoranthene J
benzo(a)pyrene J
indeno(l,2,3-cd)pyrene J
benzo{g,h,i)perylene J
4-methylphenol J
phenanthrene
fluoranthene
pyrene
acenaphthylene
phenanthrene
anthracene
fluoranthene
benzo(a)pyrene
naphthalene
2-methylphenol
naphthalene
2-methylnaphthalene
phenanthrene
fluoranthene
chrysene
4-methylphenol
2-methylnaphthalene
naphthalene
acenaphthene
dibenzofuran
fluorene
phenanthrene
fluoranthene
pyrene
all compounds
4-methylphenol
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
J
REPORT
Reason
warning low on PE sample
warning low on PE sample
low surrogate recovery
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitati=>n limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< quantitation limit
< qua·ntitation limit
< quantitation limit
< quantitation limit
< quantitation limit
exceeded holding times
< quantitation limit
I
I
ORGANIC DATA QUALIFIER REPORT I Case Number 25655
Flag
Affected Samples Compound or Fraction Used Reason
I 12935 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I 12936 2-methylphenol J < quantitation limit
4-methylphenol J < quantitation limit
phenanthrene J < quantitation limit
I 12938 acenaphthylene J < quantitation limit
phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
pyrene J < quantitation limit
I 12939 acenaphthylene J < quantitation limit
phenanthrene J < quanti~ation limit
anthracene J < quantitation limit
I fluoranthene J < quantitation limit
12940 phenanthrene J < quantitation limit
fluoranthene J < quantitation limit
I pyrene J < quantitation limit
12941 acenaphthylene J < quantitation limit
anthracene J < quantitation limit
I benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
I indeno(l,2,3-cd)pyrene J < quant i tat ion limit
dibenzo(a,h)anthracene J < quantitation limit
benzo(g,h,i)perylene J < quantitati,:,n limit
I 12943 fluoranthene J < quantitation limit
pyrene J < quantitation limit
12944 phenanthrene J < quantitation limit
I fluoranthene J < quantitation limit
pyrene J < quantitation limit
benzo(a)anthracene J < quantitation limit
chrysene J < quantitation limit
I benzo(b/k)fluoranthene J < quantitation limit
benzo(a)pyrene J < quantitation limit
indeno(l,2,3-cd)pyrene J < quantitation limit
dibenz{a,h)anthracene J < quantitation limit
I benzo(g,h,i)perylene J < quantitation limit
12967 pyrene J low internal standard recovery
butylbenzylphthalate J low internal standard recovery
I 3,3'-dichlorobenzidine J low internal standard recovery
benzo{a)anthracene J low internal standard recovery
bis(2-ethylhexyl)phthalate J low internal standard recovery
chrysene J low internal standard recovery
di-n-octylphthalate J low intern&l standard recovery I benzo(b/k)fluoranthene J low internal standard recovery
benzo(a)pyrene J low internal standard recovery
indeno(l,2,3-cd)pyrene J low internal standard recovery
dibenz{a,h)anthracene J low internal standard recovery I benzo(g,h,i)perylene J low internal standard recovery
I \\~
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I ORGANIC DATA QUALIFIER REPORT
Case Number 25655
Flag
Affected Samples Compound or Fraction peed Reas~n I 12984
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D
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13776
Pesticides
12941
12949
12956
13776
phenanthrene J
fluoranthene J
pyrene J
butylbenzylphthalate J
3,3'-dichlorobenzidine J
benzo(a)anthracene J
bis(2-ethylhexyl)phthalate
chrysene J
all compounds J
4,4'-DDT N
endrin ketone J
endrin N
4,4'-DDT N
all compounds J
< quantitation limit
< quantitation limit
low internal atandard recovery
low internal standard recovery
low internal standard recovery
low internal standard recovery
J low internal standard recovery
low internal standard recovery
exceeded holding times
difference in columns
< quantitation limit
difference in columns
difference in columns
exceeded holding times
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MEMORANDUM
Date: 12/15/97
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of EXTRACTABLES ORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me. If you have any
I
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ATTACHMENT
I
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I ORGANJC DATA QUALIFIER REPORT
Project
Case Number: 25634 Number 97-0353 SAS Number NIA
I Site ID. Reasor Chemical, Castle Hayne, NC
I Flag
Affected Samples Compound or Fraction !ill!i Reason
YQA
I 12752, 12757, tetrachloroethene J < quantitation limit
12717
I 12756, 12715 ethylbenzene J < quantitation limit
12712 All J low recovery of all IS
I BNA
12739 4-methylphenol J < quantitation limit
I 12727 naphthalene, 2-methylnaphthalene, J < quantitation limit
phenanthrene
I 12729 phenanthrene J < quantitation limit
12731 2-methylnaphthalene J < quantitation limit
I 13319 phenanthrene, fluoranthene, pyrene, J < quantitation limit
benzo(a)anthracene, chrysene,
I benzo( a )pyrene, indeno( 1,2,3-cd)pyrene,
dibenz( a,h )anthracene, benzo(g,h,i)perylene
13323 4-methylphenol J < quantitation limit
I 13466 acenaphthylene, phenanthrene, anthracene, J < quantitation limit
fluoranthene, pyrene, benzo(a)anthracene,
I chrysene, benzo(b )fluoranthene,
benzo(a)pyrene, indeno( I ,2,.'-cd)pyrene
n 13467 acenaphthylene, phenanthrene, anthracene, J < quantitation limit
fluoranthene, pyrene, benzo(a)anthracene,
chrysene, benzo(b)fluoranthene,
I benzo( a)pyrene, indeno(J ,2,3-cd)pyrene,
benzo(g,h,i)perylene
13468 chrysene J < quantitation limit
m I 3468, 134 71 di-n-octylphthalate, benzo(b )fluoranthene, J Internal standard
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene, retention times and
I dibenz( a,h )anthracene, benzo(g,h,i)perylene areas outside limits
I \ \ -1
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Case Number:
Site ID.
Affected Samples
13470
13474
13475
13344
13346
Pesticides
13342
13346
ORGANJC DATA QUALIFIER REPORT
Project
25634 Number
Reasor Chemical, Castle Hayne, NC
Compound or Fraction
naphthalene, 2-methylnaphthalene,
acenaphthylene, fluorene, anthracene,
fluoranthene, benzo(a)anthracene, chrysene,
benzo(b )fluoranthene, benzo( a)pyrene
phenanthrene, fluoranthene, pyrene,
benzo(a)anthracene, chrysene,
benzo(b )fluoranthene, benzo( a)pyrene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
naphthalene, 2-methylnaphthalene,
acenaphthylene, fluorene, phenanthrene,
anthracene, benzo(b )fluoranthene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
Naphthalene, acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno( 1,2,3-
c,d)pyrene, benzo(g,h,i)perylene
Naphthalene, 2-methylnaphthalene,
acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno(l ,2,3-c,d)pyrene
4,4'-DDD, 4,4'-DDT
4,4'-DDT
Methoxychlor
97-0353 SAS Number NIA
Flag
~ Reason
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
N % Difference between
columns
JN < quantitation limit, %
Difference between
columns
I
~1ai sr~,f"..r . ft . I
I \ l~;, UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
I MEMORANDUM
I Date: 12115197
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of PESTICIDES/PCB ORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
I From: John Mcconney ~U...~
To: RAY DOYLE
I
• · ·. Thru: QA Office
&Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
I
I
I
rTTACHMENT
I
I
I
I
If you have any
I
I
·-.
I ORGANJC DATA QUALIFIER REPORT
Project
I Case Number: 25634 Number 97-0353 SAS Number NIA
Site ID. Reasor Chemical, Castle Hayne, NC
I Flag
Affected Samples Compound or Fraction !.!.lli! Reason
I VOA
12752, 12757, tetrachloroethene J < quantitation limit
12717
I 12756, 12715 ethyl benzene J < quantitation limit
I 12712 All J low recovery of all JS
BNA
I 12739 4-methylphenol J < quantitation limit
12727 naphthalene, 2-methylnaphthalene, J < quantitation limit
R
phenanthrene
12729 phenanthrene J < quantitation limit
I 12731 2-methylnaphthalene J < quantitation limit
13319 phenanthrene, fluoranthene, pyrene, J < quantitation limit
benzo(a)anthracene, chrysene,
I benzo(a)pyrene, indeno( 1,2,3-cd)pyrene,
dibenz(a,h)anthracene, benzo(g,h,i)perylene
I 13323 4-methylphenol J < quantitation limit
13466 acenaphthylene, phenanthrene, anthracene, J < quantitation limit
I fluoranthene, pyrene, benzo(a)anthracene,
chrysene, benzo(b)fluoranthene,
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene
I 13467 acenaphthylene, phenanthrene, anthracene, J < quantitation limit
fluoranthene, pyrene, benzo(a)anthracene,
chrysene, benzo(b )fluoranthene,
I benzo( a)pyrene, indeno( 1,2,3-cd)pyrene,
benzo(g,h, i )pery I ene
I 13468 chrysene J < quantitation limit
13468, 13471 di-n-octylphthalate, benzo(b )fluoranthene, J Internal standard
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene, retention times and
I dibenz(a,h)anthracene, benzo(g,h,i)perylene areas outside limits
I \XO
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Case Number:
Site ID.
Affected Samples
13470
_13474
13475
13344
13346
festicide~
13342
13346
ORGANIC DATA QUALIFIER REPORT
Project
25634 Number
Reasor Chemical, Castle Hayne, NC
Compound or Fraction
naphthalene, 2-methylnaphthalene,
acenaphthylene, fluorene, anthracene,
fluoranthene, benzo(a)anthracene, chrysene,
benzo(b)fluoranthene, benzo(a)pyrene
phenanthrene, fluoranthene, pyrene,
benzo( a )anthracene, chrysene,
benzo(b )fluoranthene, benzo( a)pyrene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
naphthalene, 2-methylnaphthalene,
acenaphthylene, fluorene, phenanthrene,
anthracene, benzo(b )fluoranthene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
Naphthalene, acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno(l ,2,3-
c,d)pyrene, benzo(g,h,i)perylene
Naphthalene, 2-methylnaphthalene,
acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno( 1,2,3-c,d)pyrene
4,4'-DDD, 4,4'-DDT
4,4'-DDT
Methoxychlor
97-0353 SAS Number NIA
Flag
.!.!.llii Reason
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
N ¾ Difference between
columns
JN < quantitation limit, ¾
Difference between
columns
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
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MEMORANDUM
Date: 12/15/97
Science and Ecosystem Support Division
980 College St~tion Road
Athens, Georgia 30605-2720
Subject: Results of VOLATILES ORGANIC Sample Analysis
97-0353 REASOR CHEMICAL
CASTLE HAYNE, NC
From: John Mcconney
To: RAY DOYLE
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
I
n
n
I ATTACHMENT
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If you have any
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I ) ORGANJC DATA QUALIFIER REPORT
Project
I Case Number: 25634 Number 97-0353 SAS Number NIA
Site ID. Reasor Chemical, Castle Hayne, NC
I Flag
Affected Samples Compound or Fraction Used Reason
I VOA
12752, 12757, tetrachloroethene J < quantitation limit
12717
I 12756, 12715 ethyl benzene J < quantitation limit
I 12712 All J low recovery of all JS
BNA
I 12739 4-methyiphenol J < quantitation limit
12727 naphthalene, 2-methylnaphthalene, J < quantitation limit
I
phenanthrene
12729 phenanthrene J < quantitation limit
I 12731 2-methylnaphthalene J < quantitation limit
13319 phenanthrene, fluoranthene, pyrene, J < quantitation limit
I
benzo(a)anthracene, chrysene,
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene,
d ibenz( a,h )anthracene, benzo(g,h,i)perylene
I 13323 4-methylphenol J < quantitation limit
13466 acenaphthylene, phenanthrene, anthracene, J < quantitation limit
I fluoranthene, pyrene, benzo(a)anthracene,
chrysene, benzo(b )fl uoranthene,
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene
I 13467 acenaphthylene, phenanthrene, anthracene,. J < quantitation limit
fluoranthene, pyrene, benzo(a)anthracene,
chrysene, benzo(b )fluoranthene,
I benzo(a)pyrene, indeno( 1,2,3-cd)pyrene,
benzo(g,h, i )pery lene
n 13468 chrysene J < quantitation limit
13468, 13471 d i-n-octylphthalate, benzo(b )fl uoranthene, J Internal standard
benzo(a)pyrene, indeno( 1,2,3-cd)pyrene, retention times and
D dibenz( a,h )anthracene, benzo(g,h, i)perylene areas outside limits
m
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Case Number:
Site ID.
Affected Samples
13470
13474
13475
13344
13346
Pesticides
13342
13346
ORGANIC DATA QUALIFIER REPORT
Project
25634 Number
Reasor Chemical, Castle Hayne, NC
Compound or Fraction
naphthalene, 2-metbylnaphthalene,
acenaphthylene, fluorene, anthracene,
fluoranthene, benzo(a)anthracene, chrysene,
benzo(b )fluoranthene, benzo( a)pyrene
phenanthrene, fluoranthene, pyrene,
benzo(a)anthracene, chl)·sene,
benzo(b )fluoranthene, benzo( a)pyrene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
naphthalene, 2-methylnaphthalene,
acenaphthylene, fluorene, phenanthrene,
anthracene, benzo(b )fluoranthene,
indeno( 1,2,3-cd)pyrene, benzo(g,h,i)perylene
Naphthalene, acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno( 1,2,3-
c,d)pyrene, benzo(g,h,i)perylene
Naphthalene, 2-methylnaphthalene,
acenaphthene, dibenzofuran,
benzo(b )fluoranthene, indeno( 1,2,3-c,d)pyrene
4,4'-DDD, 4,4'-DDT
4,4'-DDT
Methoxychlor
97-0353 SAS Number NIA
Flag
.!.!.ill! Reason
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
J < quantitation limit
N % Difference between
columns
JN < quantitation limit, %
Difference between
columns
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MEMORANDUM
Date: 02/17/98
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of DIOXINS ORGANIC Chemistry Section Sample Analysis
98-0109 Reasor Chemical
Castle Hayne, NC
From: John Mcconney celLG----o-
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
llttached are the results of analysis of samples collected as part of the subject project. If you have any
-.·uestions, please contact me.
I
ATTACHMENT
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DATA QUALIFIER REPORT
Project No.: 98-0109
Site Name: Reasor Chemical, Castle Hayne, NC
Affected
Samoles
All
Analvte
Total congeners
Flag
~
J
Reason
Assumed Resp.
Factors/ Cal. Stds
not available for
all congeners
TEQ's : The Toxic Equivalent (TEQ) represents a summation of values from the individual equivalents that are calculated for each of the 2,3,7,8 containing isomecs. If 10% or greater of the TEQ value was from data considered to be estimated, then the TEQ is reported as estimated (J flag).
Abbreviation Kev:
TCDD Tetrachlorodibenzodioxin
PeCDD = Pentachlorodibenzodioxin
HxCDD Hexachlorodibenzodioxin
HpCDD
OCDD
IS
Heptachlorodibenzodioxin
Octachlorodibenzodioxin
= Internal Standard
Reason Codes:
TCDF
PeCDF
HxCDF
HpCDF
OCDF
Tetcachlorodibenzofuran
Pentachlorodibenzofuran
Hexachlorodibenzofuran
Heptachlorodibenzofuran
Octachlorodibenzofuran
1. Results lower than the minimum quantitation limit 2. Results higher than the maximum calibration limit
! '. (
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I MEMORANDUM
I Date: 02/24/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of DIOXINS ORGANIC Chemistry Section Sample Analysis
I
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98-011 0 Reasor Chemical
Castle Hayne, NC
From: John Mcconney
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
ij~~~ij:~~\
\\ft FEB 2 6 ,99o \::. ,
I
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IAttached are ti1e results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
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'TTACHMENT
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Project No.
Site Name:
DATA QUALIFIER REPORT
98-0110
Reasor Chemical, Castle Hayne, NC
Flag Affected
samoles
All
Analyte ~ Reason
Total congeners J Assumed Resp.
Factors/ Cal. Stds
not available for
all congeners
TEQ's : The Toxic Equivalent (TEQ) represents a summation of values from the individual equivalents that are calculated for each of the 2,3,7,8 containing isomers. If 10\ or greater of the TEQ value was from data considered to be estimated, then the TEQ is reported as estimated (J flag).
Abbreviation Kev:
TCDD Tetrachlorodibenzodioxin
PeCDD
HxCDD
HpCDD
OCDD
IS
Pentachlorodibenzodioxin
= Hexachlorodibenzodioxin
Heptachlorodibenzodioxin
Octachlorodibenzodioxin
= Internal Standard
Reason Codes:
TCDF
PeCDF
HxCDF
HpCDF
OCDF
=
=
Tetrachlorodibenzofuran
Pentachlorodibenzofuran
Hexachlorodibenzofuran
Heptachlorodibenzofuran
Octachlorodibenzofuran
1. Results lower than the minimum quantitation limit 2. Results highe~ than the maximum calibration limit
I
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I MEMORANDUM
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Date: 02/26/98
Subject: Results of DIOXINS ORGANIC Chemistry Section Sample Analysis
98-0111 Reasor Chemical
Castle Hayne, NC
From: John Mcconney
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
·hru: QA Office
lttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
n
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ITTACHMENT
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If you have any
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Project No.
Site Name:
Affected
Samoles
All
DATA QUALIFIER REPORT
98-0111
Reasor Chemical, Castle Hayne, NC
Flag
Anal vte Used Reason
Total congeners J Assumed Resp.
Factors/ Cal.
not available
all congeners
Stds
for
TEQ's : The Toxic Equivalent (TEQ) represents a summation of values from the
individual equivalents that are calculated for each of the 2,3,7,8 containing
isomers. If 10% or greater of the TEQ value was from data considered to be
estimated, then the TEQ is reported as estimated {J flag)
Abbreviation Key:
TCDD Tetrachlorodibenzodioxin TCDF
PeCDD
HxCDD
HpCDD
OCDD
IS
Pentachlorodibenzodioxin
Hexachlorodibenzodioxin
Heptachlorodibenzodioxin
Octachlorodiber.zodioxin
= Internal Standard
Reason codes:
PeCDF
HxCDF
HpCDF
OCDF
Tetrachlorodibenzofuran
Pentachlorodibenzofuran
Hexachlorodibenzofuran
Heptachlorodibenzofuran
Octachlorodibenzofuran
1. Results lower than the minimum quantitation limit
2. Results higher than the maximum calibration limit
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I MEMORANDUM
I Date: 03/02/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of METALS INORGANIC Chemistry Section Sample Analysis
I 98-0105 Reasor Chemical
Castle Hayne, NC
I
m
I
From: Keith Bates
To: Jennifer Wendel
WMDINSMB
CC: Ray Doyle
. WESTON
·hnu: QA Office
llached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
D
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rACHMENT
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If you have. any
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_,~5~9=0~2 _____________ _
Project Number:_,9~8~-~0~l...,,0~S __________ _
Site: Reasor Chemical, Castle Hayne, NC
Element
A. Waters
Be, Cr, Cu, Mn,
Ni, Se, Ag, V,
Zn
Al, Ca, Fe, Mg,
K, Na
Al
Na
Sb
B, Soils
Be, Cr, Cu, Mn,
Ni, Se, Ag, V,
Zn
Al, Ca, Fe, Mg,
K, Na
Se
Al
Ca
Fe
K
Tl
Sb
Co
flag
u
u
J
J
u
u
u
J
J
J
J
J
u
J
J
Samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
1243,
1251,
1255
1243,
1251,
1255
1250
1244,
1252,
12 4 4,
1252,
1249,
1253,
12 4 9,
1253,
1250,
1254,
1250,
1254,
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
1245
1245, 1246, 1247, 1248
1245, 1246, 1247, 1248
1245, 1246, 1247, 1248
1245, 1246, 1247, 1248
1245
1245
1247, 1248
Reason
Baseline instability
Positives in blanks
Serial dilution percent difference
17. 8
Serial dilution percent diffe~ence =
19 .1%
% RSD >
exposures
CRDL
20% for
and results
?
Baseline ir)s_.tabil'i ty
Positives in blanks
ICP multiple
> IDL, but <
Suspected over correction as noted
in the contractor ICS
Blind spike recovery> action limit
Serial dilution percent difference=
29.6%
Serial dilution percent d\ifference =
17. 7%
Blind spike recovery> warning limit
Blind spike recovery> action limit
RSD >
exposures
CRDL
20% for
and results
Only analysis of 2X
required by contract
analysis
Only analysis of 2X
required by contract
analysis
ICP multiple
> IDL, but <
CRDL standard
sow for ICP
CRDL standard
sow for IC"
I
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
I MEMORANDUM
I Date: 03/02/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of METALS INORGANIC Chemistry Section Sample Analysis
98-0107 Reasor Chemical
Castle Hayne, NC
I
I
From: Keith Bates
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
· ;Thru: QA Office
~/~
l1tached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
I
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I r TTACHMENT
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If you have any
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INORGANIC DATA QUALIFIERS REPORT
case Number:---=2~5~9~1~0,__ ____________ _
Project Nwnber:-=9~8~-~0~l~0"-'-7 __________ _ site: Reasor Chemi.cal,
Element
Cr, V, CN
Na
Pb
Hg
cu
Al
CN
Be
co
Sb
Be
Ni
Flag
u
u
J
J
J
J
J
u
u
u
J
J
Castle Hayne, NC
samples Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
1406, 1407, 1408, 1410,
1411
1406, 1407, 1408, 1409,
1410, 1411, 1412, 1413
1406, 1407, 1408, 1409,
1410, 1411, 1412, 1413
1410, 1411, 1412, 1413
1406, 1407, 1408
1410
1410, 1411
1408, 1411
14 06, 1407, 14 09, 1411
1410
Reason
Baseline instability
Positives in blanks
Matrix spike recovery= 130.2%
Matrix spike recovery= 72.9%
Matrix duplicate RPO = 200%
Blind spike recovery> action limit
Blind spike recovery> action limit
Technical holding time exceeded with 16 days elapsing between sampling and analysis
% RSD > 20% for ICP mul tipl h exposures and reported results> IC but< CRDL
% RSD > 20% for ICP multiple
exposures and reported results > IDL, but < CRDL
% RSD > 20% for ICP multiple
exposures and reported results > IDL, but < CRDL
Only analysis of 2X CRDL standard re qui red by contract sow for ICP analysis
Only analysis of 2X CRDL standard required by contract sow for ICP analysis
I
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
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MEMORANDUM
Date: 03/02/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of PESTICIDES/PCB ORGANIC Chemistry Section Sample Analysis I 98-0108 Reasor Chemical
Castle Hayne, NC
I
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From: Denise Goddard C\l:?--
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
-Thru: QA Office
lttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
I
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rTTACHMENT
I
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If you have any
17/ :J)
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
MEMORANDUM
Date: 03/02/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of EXTRACTABLES ORGANIC Chemistry Section Sample Analysis
98-0108 Reasor Chemical
Castle Hayne, NC
From: Denise Goddard 0'9-
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project. questions, please contact me. If you have any
I
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rTTACHMENT
I
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I \ju
I
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
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I
MEMORANDUM
Date: 03/02/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of VOLA Tl LES ORGANIC Chemistry Section Sample Analysis
98-0108 Reasor Chemical
Castle Hayne, NC
I From: Denise Goddard ~
I
I
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
Jttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
I
I
I
'TTACHMENT
I
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If you have any
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ORGANIC DATA QUALIFIER REPORT
Case Number 25933 Project Number 98-0l0S SAS. Number Site ID. Reasor Chemical, Castle Hayne, NC
Flag Affected Samples Compound or Fraction Used Reason
Volatiles
l658 ethylbenzene J < quantitation limit xylene J < quantitation limit
l659 xylene J < quantitation limit
Extractables
l652 naphthalene J < quant.itation limit 2-methylnaphthalene J < quantitation limit
l658 2,4-dimethylphenol J < guantitation limit
Pesticides
all samples endosulfan II .. R action low on PE sample endrin aldehyde R action low on PE sample endosulfan sulfate R missed from PE sample endrin ketone R missed from PE sample
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
I
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I MEMORANDUM
I Date: 03/02/98
I Subject: Results of METALS INORGANIC Chemistry Section Sample Analysis
98-0108 Reasor Chemical
I
I
I
Castle Hayne, NC
From: Keith Bates
;::,1-1(]✓.-==--
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
ltached are the results of analysis of samples collected. as part of the subject project.
questions, please contact me.
I
i
If you have any
I
I A~~~,~:~~r\
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rTACHMENT
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INORGANIC DATA QUALIFIERS REPORT
Case Number:_~2~5~9~3~3=--------------
Project Number:-'9~8~-~0~1=0~8 __________ _
Site: Reasor Chemical, Castle Bayne, NC
Element
Se
Al, Ca, Fe, Mg,
Na
Cr
Co
Cu
Ni
Co
Cu
Ni
V
Zn
Flaa
u
u
u
u
u
u
J
J
J
J
J
Samnles Affected
All positives> IDL, but
< CRDL
All positives> IDL, but
< lOX contaminant level
1658
1658
1653, 1655, 1659
1658
1655
1652, 1657, 1658, 1663
1663
1656, 1662, 1663
1652, 1653, 1657, 1658,
1662, 1663
Reason
Baseline instability
Positives in blanks
% RSD >
exposures
CRDL
20% for ICP multiple
and results > IDL, but <
% RSD > 20% for
exposures and results
CRDL
% RSD > 2 0% for
exposures and results
CRDL
% RSD >
exposures
CRDL
2 0% f'5r
and results
Only analysis of 2X
required by contract
analysis
Only analysis of 2X
required by contract
analysis
Only analysis of 2X
required by contract
analysis
Only analysis of 2X
required by contract
analysis
ICP multiple
> IDL, but <
ICP rnul tip le
> IDL, but <
ICP rnul tip le
> IDL, but <
CRDL stand<
sow for :c
CRDL standard
sow for ICP
CRDL standard
SOW for ICP
CRDL standard
sow for ICP
Only analysis
required by
analysis
of 2X CRDL standard
contract SOW for ICP
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
MEMORANDUM
Date: 01/27/98
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of PESTICIDES/PCB ORGANIC Chemistry Section Sample Analysis
98-0105 Reasor Chemical
Castle Hayne, NC
From: Denise Goddard S[B--
To: Jennifer Wendel
WMDINSMB
CC: Ray Doyle
WESTON
Thru: QA Office
Jttached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
If you have any
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'TTACHMENT
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MEMORANDUM
Date: 01/27/98
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of EXTRACT ABLES ORGANIC Chemistry Section Sample Analysis
98-0105 Reasor Chemical
Castle Hayne, NC
From: Denise Goddard ~
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Th ru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project. If you have any questions, please contact me.
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ATTACHMENT
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MEMORANDUM
Date: 01/27/98
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
Subject: Results of VOLATILES ORGANIC Chemistry Section Sample Analysis
98-0105 Reasor Chemical
Castle Hayne, NC
From: Denise Goddard W
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
lttached are the results of analysis of samples collected as part of the subJect project
questions, please contact me.
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'TTACHMENT
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ORGANIC DATA QUALIFIER REPORT
Case Number 25902 Project Number 98-0105 SAS Number Site ID. Reasor Chemical, Castle Hayne, NC
Flag Affected Samoles Comoound or Fraction Used Reason
Volatiles
1245 toluene J < quantitation limit
Extractables
1245 acid fraction R unacceptable surrogate recovery 1248 benzo(a)anthracene
chrvsene
ben~o(b/k)fluoranthene
1251,1252 di-n-octylphthalate
Pesticides
benzo(b/k)fluoranthene
benzo(a)pyrene
indeno(l,2,J-cd)pyrene
dibenz(a,h)anthracene
benzo(g,h,i)perylene
1254 heptachlor
alpha-chlordane
J < quantitation limit J < quantitation limit J < quantitation limit
J
J
J
J
J
J
low
low
low
low
low
low
internal standard
internal standard
internal standard
internal standard
internal standard
internal standard
J < quantitation limit J < quantitation limit
recovery
recovery
recovery
recovery
recovery
recovery
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
MEMORANDUM
Date: 01/29/98
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
I Subject: Results of PESTICIDES/PCB ORGANIC Chemistry Section Sample Analysis
98-0107 Reasor Chemical
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Castle Hayne, NC
From: Denise Goddard QO'
•)
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: QA Office
I Attached are the results of analysis of samples collected as part of the subject project.
questions, please contact me.
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I ATTACHMENT
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If you have any
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 01/29/98
Subject: Results of EXTRACT ABLES ORGANIC Chemistry Section Sample Analysis
From:
To:
CC:
Thru:
98-0107 Reasor Chemical
Castle Hayne, NC
Denise Goddard ~
Jennifer Wendel
WMD/NSMB
Ray Doyle
WESTON
QA Office
I Attached are the results of analysis of samples collected as part of the subject project. If you have any questions, please contact me.
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ATTACHMENT
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 4
Science and Ecosystem Support Division
980 College Station Road
Athens, Georgia 30605-2720
MEMORANDUM
Date: 01/29/98
Subject: Results of VOi/\ TILES ORGANIC Chemistry Section Sample Analysis
98-0107 Reasor Chemical
Castle Hayne, NC
From: Denise Goddard ~
To: Jennifer Wendel
WMD/NSMB
CC: Ray Doyle
WESTON
Thru: OA Office
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Attached are the results of analysis of samples collected as part of the subject project. If you have any
questions, please contact me.
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ATTACHMENT
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ORGANIC DATA QUALIFIER REPORT Case ·;;;,.imber 25910 Project Number 98-0107 SAS Number
Site ID. Reasor Chemical, Castle Hayne, NC
[\.ffE,ct'.=d Snrnoles
None
Extractables
1410
1411
Pesticides
None
Compound or Fraction
naphthalene
acenaphthene
phenanthrene
fluoranthene
pyrene
naphthalene
2-methylnaphthalene
acenaphthene
phenanthrene
J
J
J
J
J
J
J
J
J
Flag
Used Reason
< quantitation limit < quantit.ation limit < quantitation limit < quantitation limit < quantitation limit
< guantitation limit < quantit.ation limit < quantitation limit < quantitation limit
j!ii11.L51iM1PLillllljAL..,. ---~RE-IV-,,A._S, .. --Sample 1250 FY 1998 Project: 98--0105
METALS SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE90 Id/Station: RCSW13
Media: GROUNDWA
RESULTS
2200J
5U
6U
30
1U
1U
13000
4U
2U
110
8800
13
2100
50
0.20U
4U
370U
3U
44
4900J
6U
10U
95
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
D Number: NE92
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
CYANIDE
lnorg Contractor: CHEM
Org Contractor: DA TAC
Produced by: Keith Bates
Requester: Jennifer Wendel
Project Leader:
Beginning: 12102197 15: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence or presence of materfal.
K-actual value is k~ · ·· 'to be less than value given. L-actual value is knO'M1 to be greater than value given. •teria\ was analyzed for but not detected. the number is the minimum quantitation lirr
R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis is ne. y for verification.
C-confinned by get,, __ 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites ur technical chlordane
Sample 1250 . FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE90 Id/Station: RCSW13
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE92
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANtLINE
ACENAPHTHENE
2,4-DINtTROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
lnorg Contractor: CHEM
Org Contractor: DA TAC
Beginning: 12/02/97 15: 15
Ending:
RESULTS UNITS
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-esllmated value. N-presumptive evidence of presence of material. K-actual value is known to be less than value given. L-actual value is known to be greater than value giv,--U-malerial was analyzed for but not detected. the number is the minimum quan1· 'n limit. R-qc indicates tha' unusable. compound may or may not be present. resampling and reanalysis i' ssary for verification . .,..... ..... ,....onfirmed by gc. ,.when no value is reported, see chlordane constituents 2.constituents or metaL. .j of technical chlordane I~--
-Sample 1250 FY 1998 Project: 98-0105
PESTICIDES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE90 Id/Station: RCSW13
Media: GROUNDWA D Number: NE92
RESULTS UNITS ANALYTE
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.50U
0.10U
0.10U
0.050U
0.050U
5.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE}
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA}
DIELDRIN
4,4'-DDE (P,P'-DDE}
ENDRIN
ENDOSULFAN 11 (BETA}
4,4'-DDD (P,P'-DDD}
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: CHEM
Org Contractor: DAT AC
Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 15:15
Ending:
A-average value. NA-not analyzed. NAl-interfereOces. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
~ ~onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--ra.RE-IV_, A ... S, <al -od..., D.-1,~--G:2-
Sample ··._,v FY 1998
VOLATILES SCAN
Project: 98-0105
Facility: Reasor Chemical
Program: SSF
Castle Hayne. NC
Case Number: 25902
MD Number: NE90 Id/Station: RCSW13
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
18
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE92
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
1.1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/9715:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confimied by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE91 Id/Station: RCSW1
Media: GROUNDWA
RESULTS
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.50U
0.10U
0.10U
0.050U
0.050U
5.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE94
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
- ---
lnorg Contractor: CHEM
Org Contractor: DAT AC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-equ-Jen--.,en~
Project Leader:
Beginning: 12/02/97 09:15
Ending: --
K-actual value is ·n to be less than value given. L-actua1 value is known to be greater than value' U-material was analyzed for but not detected. the number is the minimum qua·
R-qc indicates th .a unusable. compound may or may nol be present. resampling and reanalysis ..:essary for verification.
-~onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metaboutes of technical chlordane
R:.qc iridicates tha. ·-unusable. compound may or may not be present. resampfing and reanalySiS j' ':Ssary·,o~v~rificatio~.
C-confirmed by gc I .when no value is reported, see chlordane constituents 2.constituents or metab ...... ..:s of technical chlordane
--
1n limit.
----Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE91 Id/Station: RCSW1
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
1DU
10U
10U
10U
10U
10U
25
10U 1ou 1ou
10U
10U
10U
10U
10U 1ou
10U
10U
10U
1DU
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE94
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor. DATAC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
_,ro,...by: r_, Go-
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 09:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary ror.verification. r.-conflrmed bY gems: 1.when no value is reported. see chlordane constltuents 2.constltuenls or metaborrte~ or t&hnir.:'41 r.hlnrrfainp.
~
- -
Sample 1251 FY 1998 Project: 98--0105
METALS SCAN
Facility: Reasor Chemical
Program: SSF
ld/Station:RCSW1
Castle Hayne, NC
Media: GROUNDWA
Case Number. 25902
MD Number. NE91
D Number. NE94
RES UL TS UNITS ANAL YTE
990J
4U
6U
12
1U
1U
4300
3U
2U
33
680
4
1100
19
0.20U
3U
110U
3U
· 31
3700J
6U
3U
26
10U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
CYANIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
Ei"' A--average value. NA-not analyzed. NAl.-lnterferences. J-estlmated value. N-presumptfve evidence or presence or materfal.
- -
Produced by: Keith Bates
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 09:15
Ending:
• K..actual value Is knO'M'l to be less than value given. l--actual value Is known lo be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantitatlon Umit.
-R-qc Indicates that data unusable. compound may or may not be present. resampllng and reanalysls Is necessary for verification.
C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites or technical chlordane
jjijALlllilW"1Pl.aiilfJAL----Sample 1252 FY 1998 Project: 98--0105
METALS SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE92 Id/Station: RCSW2
Media: GROUNDWA D Number. NE95
RESULTS UNITS ANALYTE
880J UG/L ALUMINUM
4U UG/L ANTIMONY
6U UG/L ARSENIC
10 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
4500 UG/L CALCIUM
2U UG/L CHROMIUM
2U UG/L COBALT
31 UG/L COPPER
510 UG/L IRON
4 UG/L LEAD
1300 UG/L MAGNESIUM
42 UG/L MANGANESE
0.20U UG/L TOTAL MERCURY
3U UG/L NICKEL
420 UG/L POTASSIUM
3U UG/L SELENIUM·
18 UG/L SILVER
3400J UG/L SODIUM
6U UG/L THALLIUM
3U UG/L VANADIUM
33 UG/L ZINC
10U UG/L CYANIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence or material.
--Produced by: Keith Bates
Requestor. Jennifer Wendel
Project Leader:
Beginning: 12/02197 10:15
Ending:
K-actual value is k'" ·· ·, to be less than value given. L-actual value is known to be greater than value given. 1terial was analyzed for but not detected. the number is the minimum quantitation tin R...qc indicates the unusable. compound may or may not be present. resampling and reanatysis Is ne,. .y for verification. C---confirmed by gc• .. --1.When no value is reported, see chlordane constituents 2.constituents or metabolites or technical chlordane
I -Sample 1252 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE92 Id/Station: RCSW2
Media: GROUNDWA D Number: NE95
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2.4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U -:s;> 10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
2,4-DINITROTOLUENE
DIETHYL PHTHALATE \
cA
lnorg Contractor: CHEM
Org Contractor: DA TAC
RESULTS
10U
10U
25U
25U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
A-average value. NA-not analyzed. NAl-interlerences. J--estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: Jennifer W~ndel
Project Leader:
Beginning: 12/02/97 10:15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitalion limit.
R-qc indicates that data unusable. compound may or may not be present. resarnpling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 1252 FY 1998 Project: 98-0105
PESTICIDES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE92 Id/Station: RCSW2
Media: GROUNDWA
RESULTS UNITS
0.050U UG/L
0.050U UG/L
0.050U UGIL
0.050U UGIL
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UGIL a.sou UGIL
0.10U UG/L
0.10U UGIL
0.050U UGIL
0.050U UG/L
5.0U UGIL
1.0U UGIL
2.0U UGIL
1.0U UGIL
1.0U UGIL
1.0U UG/L
1.0U UGIL
1.0U UG/L
D Number: NE95
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: CHEM
Org Contractor: DATAC
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 10:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampfing and reanalysis is necessary for verification.
~ -r:onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
y ULA I !Lt:::, :>AM~AN~IS ----------Eii8 RE-IV lili', A __ S, ~ ---od~ oalllll112-ias:2~
Sample 1252 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE92 Id/Station: RCSW2
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE95
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1,1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1,1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-inlerterences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 1210219710:15
Ending:
K-actual value is kn"'"'" to be less than value given. L-adua/ value is known to be greater than value g;· LI-material was analyzed for but not detected. the number is the minimum quar n limit. R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis i !Ssary for verification. C-confirmed by gc.. 1.when no value is reported, see chlordane constituents 2.constituents or metab1., .. ,.:s of technical chlordane
---EiaRE .. IV.-i,A--S, .. --Sample 1254 FY 1998 Project: 98-0105
METALS SCAN
Facility: Reasor Chemical
Program: SSF
Id/Station: RCSW3
Media: GROUNDWA
RESULTS UNITS ANALYTE
790UJ UG/L ALUMINUM
4U UG/L ANTIMONY
6U UG/L ARSENIC
32 UG/L BARIUM
1U. UG/L BERYLLIUM
1U UG/L CADMIUM
6200 UG/L CALCIUM
1U UG/L CHROMIUM
2U UG/L COBALT
30 UG/L COPPER
410 UG/L IRON
3U UG/L LEAD
1400 UG/L MAGNESIUM
39 UG/L MANGANESE
Castle Hayne, NC
Case Number: 25902
MD Number: NE94
D Number: NE97
0.20U UG/L TOTAL MERCURY
1U UG/L NICKEL
840 UG/L POTASSIUM
4U UG/L SELENIUM
11 UG/L SILVER
4200J UG/L SODIUM
6U UG/L THALLIUM
2U UG/L VANADIUM
23 UG/L ZINC
10U UG/L CYANIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: Jennifer Wendel
Project Leader: -
Beginning: 12/02/97 12:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number ls the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
t.:A I n..A\,., IAOLt::::, :::>A.Mt-'Lt:. 8..t;i8J._Y!:i,U;i___ ----- -
Sample 1254 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE94 Id/Station: RCSW3
Media: GROUNDWA
RESULTS
10U 1ou
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U 1ou
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE97
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Produced by: Denise Goddard
· Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 12:00
Ending: lnorg Contractor: CHEM
Org Contractor: DAT AC
RESULTS UNITS
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
4°CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material. K-actual value is kn0•·-.... to be less than value given. L-actual value is known lo be greater than value giv,. 'J-material was analyzed for but not detected. the number is the minimum quanf -limit. R-qc indicates that-·nusable. compound may or may not be present. resampling and reanalysis is ,sary for verification. C-confinned by gw,. .when no value is reported, see chlordane constituents 2.constituents or metaboi ..... ., of technical chlordane
-TIC-PC-MP'lllflA~ ---R~IVlllb,A .. S, ..
Sample 1254 FY 1998 Project: 98-0105
PESTICIDES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE94 Id/Station: RCSW3
Media: GROUNDWA D Number: NE97
RESULTS UNITS ANALYTE
o.osou o.osou
0.OS0U
0.0S0U
0.0095J
0.0S0U o.osou o.osou
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U a.sou
0.10U
0.10U
0.019J
0.OS0U
5.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: CHEM
0 rg Contractor. DA TAC
A-average value. NA-not analyzed. NAl-interferences. J~stimated value. N-presumptive evidence of pri:>sence of material.
--Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 12:00
Ending:
K-actual value is-' ., to be less than value given. L-actual value is known to be greater than value f U-material was analyzed for but not detected. the number is the minimum qua1 n limit. R-qc indicates th. J unusable. compound may or may not be present. resampfing and reanalysis , .essary for verification. r--r:onfirmed by gCfl,s: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--E-REcllll IV-• A ... S, clllll --Sample ·,,;4 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE94 Id/Station: RCSW3
Media: GROUNDWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: NE97
ANALYTE
CHLOROMETHANE
BROM OM ETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 12:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed tor but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
---ElilllfEGiililV 5ii1 ATillilf,, ~ --Sample 1255 FY 1998 Project: 98-0105
METALS SCAN
Facility: Reasor Chemical
Program: SSF
Id/Station: RCSW4
Media: GROUNDWA
RESULTS UNITS ANALYTE
290UJ UG/L ALUMINUM
4U UG/L ANTIMONY
6U UG/L ARSENIC
8 UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
1100 UG/L CALCIUM
1U UG/L CHROMIUM
2U UG/L COBALT
28 UG/L COPPER
180U UG/L IRON
3U UG/L LEAD
1800 UG/L MAGNESIUM
34 UG/L MANGANESE
Castle Hayne, NC
Case Number: 25902
MD Number: NE95
D Number: NE98
0.20U UG/L TOTAL MERCURY
1U UG/L NICKEL
2200 UG/L POTASSIUM
3U UG/L SELENIUM
12 UG/L SILVER
1700J UG/L SODIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
45 UG/L ZINC
10U UG/L CYANIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
Produced by: Keith Bales
Requester. Jennifer Wendel
Project Leader:
Beginning: 12/02/97 12: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence or presence of material.
K-actual value is knov...., to be less than value given. L-actual value is known lo be greater than value given. U · ~terial was analyzed ror but not detected. the number Is the minimum quantitation limit
R--qc indicates that' 1nusable. compound may or may not be present. resampling and reanalysis is neci for verification.
C-<:onfirmed by gcfl. .'Nhen no value is reported, see chlordane constituents 2.constituents or metabolites ... ~hnical chlordane
Sample L. . FY 1998
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Project: 98-0105
Castle Hayne, NC
Case Number: 25902
MD Number: NE95 Id/Station: RCSW4
Media: GROUNDWA
RES UL TS UNITS ,au UG/L
10U UG/L
10U UG/L
10U UG/L ,au UG/L
1ou UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: NE98
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4 ,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: DATAC
RESULTS
10U
10U
25U
25U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
A-average value. NA-not analyzed. NAl-lnterferences. J-eslimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader: ·
Beginning: 12/02/97 12: 15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituenls or metabolites of technical chlordane
--~RE<IMil IV~. A--S, c:1(1111 - -
Sample 1255 FY 1998 Project: 98-0105
PESTICIDES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE95 Id/Station: RCSW4
Media: GROUNDWA
RESULTS UNITS
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
.10U UG/L
0.10U UG/L
0.50U UG/L
0.10U UG/L
0.10U UG/L
0.050U UG/L
0.050U UG/L
5.0U UG/L
1.0U UG/L
2.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
D Number: NE98
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: CHEM
Org Contractor: DA TAC
Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02197 12: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-aciual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r-..r.onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 1255 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NE95 Id/Station: RCSW4
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE98
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence or presence of material.
--Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12102/97 12: 15
Ending:
K-actual value is kn""''l to be less than value given. L-actual value is known to be greater than value gi'-' U-material was analyzed for bul not detected. the number is the minimum quan' 'l limit. R-q_c indicates Iha' unusable. compound may or may not be present. resampling and reanalysis ii ssary for verification. C-confirmed by gei. 1.when no value is reported, see chlordane constituents 2.constituents or metabv ... .o:s of technical chlordane
-Sample 1257 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Casile Hayne, NC
Case Number: 25902
Id/Station: RCSWS
Media: SURFACEWA
RES UL TS UNITS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE90
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANJLINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DJNITROTOLUENE
0/ETHYL PHTHALATE
-Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:20
Ending:
Org Contractor: DATAC
RESULTS UNITS
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A}ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
!NDENO (1,2,3-CD) PYRENE
DIBENZO(A,H}ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. K-actual value is kn0'"" to be less than value given. L-actual value is known to be greater than value giv· IJ-malerial was analyzed for but not detected. the number is the minimum quan' 1 limit. R-qc indicates that musable. compound may or may not be present. resampting and reanalysis is isary for verification. C-confirmed by gci-, .. when no value is reported, see chlordane constituents 2.constituents or metabo ... -.> of technical chlordane
',wTILiiW-M'ilil'N~S --Sample ·, -A FY 1998 Project: 98-0105
. VOL.ATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW5
Media: SURFACEWA D Number: NE90
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: DAT AC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UGIL
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: Denise Goddard
Requester: Jennifer Wer.del
Project Leader: -
Beginning: 12/02197 14:20
Ending:
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actua\ value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitalion limit.
R-qc indicates that data unusable. compound may or may not be present. resarnpling and reanalysis ls necessary for verification.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constltuents or metabolites of technical chlordane
-Sample 12,tl FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW8
Media: SUF;{FACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE91
ANALYTE
PHENOL
BIS(2-CHLOROETHYL} ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL} ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY}METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
-~du,-Dat'-"r-·'IIM:35-
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:50
Ending:
Org Contractor: DAT AC
RESULTS UNITS
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UGIL
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB}
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE.
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A}ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL} PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K}FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD} PYRENE
DIBENZO(A,H}ANTHRACENE
BENZO(GHl}PERYLENE
A•average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resamp!ing and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites or technical chlordane
'If VLJ-\ I ILC;:> ;:>AJYU--Lt: ANAL Y ~l::i - - - - --Sample 1258 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW8
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: NE91
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: DAT AC
10U UG/L
10U UG/L
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
~ \
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U .UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:50
Ending:
K-actual value is kn"·"ri lo be less than value given. L-actual value is known to be greater than value gi•· · U-material was analyzed for but not detected. the number is lhe minimum quan' 1 limit. R-qc indicates tha' unusable. compound may or may not be present. resampling and reanalysis i: ssary for verification. C-confirmed by gei. I .when no value is reported, see chlordane constituents 2.constituents or metabl,, .. ..,s of technical chlordane
-Sample 1259 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW14
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: NE93
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER (3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: DA TAC
RESULTS
1DU
10U
25U
25U
10U
10U
10U
25U
1DU
10U
10U
10U
1DU
10U
10U
1DU
10U
1DU
10U
1DU
10U
10U
10U
10U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:_
Beginning: 12/02/97 15:15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE ·
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
81S(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-adual value is known to be less than value given. L-actual value is known to be greater than value givp-.U-material was analyzed for but not detected. the number is the minimum quanf 1 limit. R-qc indicates that unusable. compound may or may not be present. resampling and reanalysis is ssary for verification. C-confirmed by go .when no value is reported, see chlordane constituents 2.constituents or metab1.:., . J of technical chlordane
-Sample 1259 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Casile Hayne, NC
Case Number: 25902
ld/Stalion: RCSW14
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE93
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: DATAC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -
Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader: ·
Beginning: 12102197 15:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantilation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlord::i.nA
Sample 1261 FY 1998 Project: 98--0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW6
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NE99
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: DAT AC
RESULTS
10U
10U
25U
25U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
":R
~age value. NA-not analyzed NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:10
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-actual value is knr····-to be less than value given. L-actual value is known to be greater than value giv 'I-material was analyzed for but not detected. the number ls the minimum quanr R-qc indicates that 1nusable. compound may or may not be present. resampling and reanalysis is .osary for verification. C-confirmed by gen,_ ,.when no value is reported, see chlordane constituents 2.constituents or metabo111c:s of technical chlordane
limit.
-Sample ·,-a1 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW6
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25 UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: NE99
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: DA TAC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimaled value. N-presurnptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:10
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confim,ed by gems: 1.when no value is reported, see chlordane consliluents 2.constituents or metabolites of technical chlordane
E .. CT-=S !llll'LE-L Y~ -Sample 1262 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical Castle Hayne, NC
Program: SSF Case Number: 25902
Id/Station: RCSW9
Media: SURFACEWA D Number: NFOO
RESULTS UNITS ANALYTE
10U UG/L PHENOL
10U UG/L BIS(2-CHLOROETHYL) ETHER
10U UG/L 2-CHLOROPHENOL
10U UG/L 1,3-DICHLOROBENZENE
10U UG/L 1,4-DICHLOROBENZENE
10U UG/L 1,2-DICHLOROBENZENE
10U UG/L 2-METHYLPHENOL
10U UG/L BIS(2-CHLOROISOPROPYL) ETHER
10U UG/L (3-AND/OR 4-)METHYLPHENOL
10U UG/L N-NITROSODI-N-PROPYLAMINE
10U UG/L HEXACHLOROETHANE
10U UG/L NITROBENZENE
10U UG/L ISOPHORONE
10U UG/L 2-NITROPHENOL
10U UG/L 2,4-DIMETHYLPHENOL
10U UG/L BIS(2-CHLOROETHOXY)METHANE
10U UG/L 2,4-DICHLOROPHENOL
10U UG/L 1,2,4-TRICHLOROBENZENE
10U UG/L NAPHTHALENE
10U UG/L 4-CHLOROANILINE
10U UG/L HEXACHLOROBUTADIENE
10U UG/L 4-CHLOR0-3-METHYLPHENOL
10U UG/L 2-METHYLNAPHTHALENE
10U UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10U UG/L 2,4,6-TRICHLOROPHENOL
25U UG/L 2,4,5-TRICHLOROPHENOL
10U UG/L 2-CHLORONAPHTHALENE
25U UG/L 2-NITROANILINE
10U UGIL DIMETHYL PHTHALATE
10U UG/L ACENAPHTHYLENE
10U UG/L 2,6-DINITROTOLUENE
25U UG/L 3-NITROANILINE
10U UG/L ACENAPHTHENE
25U UG/L 2,4-DINITROPHENOL
25U UG/L 4-NITROPHENOL
10U UG/L DIBENZOFURAN
~ 10U UG/L 2,4-DINITROTOLUENE
10U UG/L DIETHYL PHTHALATE
Produced by: Denise Goddard
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:50
Ending:
Org Contractor: DATAC
RES UL TS UNITS
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J...estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that dala unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-wnfirmed by gems: 1.when no.value is reported, see chlordane constituents 2.conslituenls or metabolites of technical chlordane
----odi-. D,,_,/2.,..6:2-
Sample 1262 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Station: RCSW9
Media: SURFACEWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NFOO
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: DATAC
1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 14:50
Ending:
K-actual value is kr~·..,n lo be less than value given. L-actual value is known to be greater than value gf· U-material was analyzed for but not detected. the number is the minimum quar R-qc indicates th.: : unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification. C-confinned by QL. 1.when no value is reported, see chlordane constituents 2.constituents or metab,., .. ,~s of technical chlordane
,n limit.
Sample 12!>uti FY 1997 Project: 97 -0357
EXTRACT ABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA D Number: MY55
RESULTS UNITS ANALYTE
10U UG/L PHENOL
10UJ UG/L BIS(2-CHLOROETHYL) ETHER
10U UG/L 2-CHLOROPHENOL
10UJ UG/L 1,3-DICHLOROBENZENE
10UJ UG/L 1,4-DICHLOROBENZENE
10UJ UG/L 1,2-DICHLOROBENZENE
5J UG/L 2-METHYLPHENOL
10UJ UG/L BIS(2-CHLORDISOPROPYL) ETHER
36 UG/L (3-AND/OR 4-)METHYLPHENOL
10UJ UG/L N-NITROSODI-N-PROPYLAMINE
10UJ UG/L HEXACHLOROETHANE
10UJ UG/L NITROBENZENE
10UJ UG/L ISOPHORONE
10U UG/L 2-NITROPHENOL
10UJ UG/L 2,4-DIMETHYLPHENOL
10UJ UG/L BIS(2-CHLOROETHOXY)METHANE
10U UG/L 2,4-DICHLOROPHENOL
10UJ UG/L 1,2,4-TRICHLOROBENZENE
10UJ UG/L NAPHTHALENE
10UJ UG/L 4-CHLOROANIUNE
10UJ UG/L HEXACHLOROBUTADIENE
10U UG/L 4-CHLORO-3-METHYLPHENOL
10UJ UG/L 2-METHYLNAPHTHALENE
10UJ UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10U UG/L 2,4,6-TRICHLOROPHENOL
25U UG/L 2,4,5-TRICHLOROPHENOL
10UJ UG/L 2-CHLORONAPHTHALENE
25UJ UG/L 2-NITROANILINE
10UJ UG/L DIMETHYL PHTHALATE
10UJ UG/L ACENAPHTHYLENE
10UJ UG/L 2,6-DINITROTOLUENE
25UJ UG/L 3-NITROANILINE
10UJ UG/L ACENAPHTHENE
25U UG/L 2,4-DINITROPHENOL
25U UG/L 4-NITROPHENOL
10UJ UG/L DIBENZOFURAN
~ 10UJ UG/L 2,4-DINITROTOLUENE
10UJ UG/L DIETHYL PHTHALATE
Org Contractor: AA TS
-Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
RESULTS UNITS ANALYTE
10UJ UG/L
2J UG/L
25UJ UG/L
25U UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25U UG/L
3J UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the-number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12906 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA
RES UL TS UNITS
200JN UG/L
60JN UGIL
20JN UG/L
500J UG/L
300JN UG/L
200JN UG/L
20JN UG/L
D Number: MY55
ANALYTE
PROPYLPHENOL
METHYL(METHYLETHYL) PHENOL
PHENYLHEXANONE
ALKANES
(PHENYLETHYL) PHENOL
ETHENYLPHENANTHRENE
(PHENYLETHENYL)PHENOL
Org Contractor: AA TS
60JN UG/L
30JN UGIL
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
ANTHRONE
3000J UG/L 27 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -llllill'd u'IIII Da'tlllli/11 /iilM :16 -
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
K-actuat value is 1-'wn to be less than value given. L-actual value is known to be greater than value 9;. .... U-material was analyzed for but not detected. the number is the minimum quar>"' -•ion limit.
R-qc indicates tt :a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by g_ .,_ 1.when no value is reported, see chlordane constituents 2.constituents or meta .... ~s of technical chlordane
-Sample 12906 FY 1997 Project: 97 -0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA D Number: MY55 Org Contractor: AA TS
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
76 UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
23 UG/L
10U UG/L
10U UG/L
10U UG/L
1J UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1,1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1.1.2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
K-actual value is kn"''"° to be less than value given. L-actual value is known to be greater than value giV"'"' U-material was analyzed for but not detected. the number is the minimum quantit-·''ln limit.
R--qc indicates th.: · unusable. compound may or may not be present. resampling and reanalysis i: •ssary for verification.
C-confirmed by Qt._ 1.when no value is reported, see chlordane constituents 2.constituents or metat. _ .; of technical chlordane
-Sample 12906 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA
RESULTS
400J
1000JN
6JN
900J
UNITS
UG/L
UG/L
UG/L
UG/L.
0 Number: MY55
ANALYTE
CYCLOALKANE
METHYL(METHYLETHYL)BENZENE
METHYL(METHYLETHENYL)BENZENE
2 UNIDENTIFIED COMPUONDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
K-actual value is kri'"''"n to be less than value given. L-actual value is known to be greater than value giv,,.-LI-material was analyzed for but not detected. the number is the minimum quanti1-·,...,n limit.
R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis i~ ssary for verification.
C-confirmed by gc 1.when no value is reported. see chlordane constituents 2.constituents or metab~ ., of technical chlordane
--E~EGilaVS-AT..,,G_ --~e.-oat-02/-:50 -
Sample 12906 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA D Number: MY55
RESULTS UNITS
10U UG/L
10UJ UG/L
10U UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
5J UG/L
10UJ UG/L
36 UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10U UG/L
10UJ UG/L
10UJ UG/L
10U UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10U UG/L
10UJ UG/L
10UJ UG/L
10U UG/L
25U UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
25U UG/L
25U UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
RESULTS UNITS ANALYTE
10UJ UG/L
2J UG/L
25UJ UG/L
25U UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25U UG/L
3J UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r -r:onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--E~EG-VS-AT~,G---Sample 12906 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA
RESULTS
200JN
60JN
20JN
500J
300JN
200JN
D Number: MY55
ANALYTE
PROPYLPHENOL
METHYL(METHYLETHYL) PHENOL
PHENYLHEXANONE
ALKANES
(PHENYLETHYL) PHENOL
ETHENYLPHENANTHRENE
(PHENYLETHENYL) PHENOL
Org Contractor: AA TS
20JN
60JN
30JN
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
ANTHRONE
3000J 27 UNIDENTIFIED COMPOUNDS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampting and reanalysis is necessary for verification.
r:--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12906 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
P1ogram: NSF Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA D Number: MY55 Org Contractor: AA TS
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
76 UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/l
10U UG/L
23 UG/L
10U UG/L
10U UG/L
10U UG/L
1J UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRIGHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. N~-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
K-actual value is •n to be less than value given. L-actual value is known to be greater than valuer· U-material was analyzed for but not detected. the number is the minimum quar· ·,n limit.
R-qc indicates tt. .a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
r':-confirmed by gc111s: 1.when no value is reported, see chlordane constituents 2.constituents or metabvutes of technical chlordane
""'TIL ... ll/li""-NA"""5 --Sample 12906 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSW10
Media: SURFACEWA
RESULTS UNITS
400J UG/L
1000JN UG/l
6JN UG/L
900J UG/L
D Number: MY55
ANALYTE
CYCLOALKANE
METHYL(METHYLETHYL)BENZENE
METHYL(METHYLETHENYL)BENZENE
2 UNIDENTIFIED COMPUONDS
Org Contractor: AA TS
- -
~er..-:,at<lllll(l2/~20 -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:05
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
iMF"lilit::,-t'L'iii'L y. Sample 12910 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA D Number: MY64
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10UJ
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2.4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2.4-DICHLOROPHENOL
1,2.4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
10U
10U
25U
25U
10U
10UJ
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-actual value is known to be less than value given. L-actual value is known to be greater than value givPn_ U-material was analyzed for but not detected. the number is the minimum quantit;:,tion limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i: ~ssary for verification.
C-confirmed by Ql 1.when no value is reported, see chlordane constituents 2.constituents or metal ; of technical chlordane
-Sample 1 L~10 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW11
Media: SURFACEWA
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY64
ANALYTE
METHYL(METHYLETHYL)BENZENE
ALKANES
Org Contractor: AA TS
RESULTS
6JN
50J
50JN
3JN
900J
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACIDS (3 ISOMEF
NORTRACHELOGENIN
8 UNIDENTIFIED COMPOUNDS
A-average vatue. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader:.DOYLE
Beginning: 08/25/97 08: 15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~IL~MFalaNA_, ---EFWIISEG-.'S-AT .... ,G .... --Sample 12~1 0 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA D Number: MY64 Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
20U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
. UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLO RO BENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:15
Ending:
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
'WTILii1i""MJWNAiiii5 --Sample 1291 O FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA D Number: MY64 Org Contractor: AA TS
RES UL TS UNITS ANALYTE
80J UG/L 3 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:15
Ending:
K-actual value is'·· ·vn to be less than value given. L-actual value is known to be greater than value p;. ~. U-material was analyzed for but not detected. the number is the minimum qua11•=·-•1on limit.
R-qc indicates tf a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by g._. ___ ..,; 1.when no value is reported, see chlordane constituents 2.constituents or metaL .<!S of technical chlordane
--EiiiaRE<alVSjiiAT-,G--
Sample 12910 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA D Number: MY64
RESULTS
10U
·10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10UJ
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2.4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:15
Ending:
RESULTS UNITS ANALYTE
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10UJ UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1, -vn to be less than value given. L-actual value is known to be greater than value gi· · U-material was analyzed for but not detected. the number is the minimum quanP "'1n limit.
R-qc indicates th' a unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification.
f:-confirmed by QL ....... 1.when no value is reported, see chlordane constituents 2.constituents or metaL~ .. .::s of technical chlordane
-Sample 12910 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA
RESULTS UNITS
6JN UG/L
S0J UG/L
D Number: MY64
ANALYTE
METHYL(METHYLETHYL)BENZENE
ALKANES
Org Contractor: AA TS
S0JN UG/L
3JN UGIL
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACIDS (3 ISOMEF .
NORTRACHELOGENIN
900J UGIL 8 UNIDENTIFIED COMPOUNDS
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08125197 08:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12910 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW11
Media: SURFACEWA D Number: MY64 Org Contractor: AA TS
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
20U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
s.~ - -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
~-r:onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
...,.Tll.illiAMiilirN"iriliiS ---E~ECMM!IV5ililAT..,,G_ - -
Sample 12910 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW11
Media: SURFACEWA
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY64
80J UG/L 3 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:15
Ending:
K-actual value is_' · -'n to be less than value given. L-actual value is known to be greater than value g: U-material was analyzed for but not detected. the number is the minimum quari•·· ·,n limit.
R-qc indicates th a unusable. compound may or may not be present. resampling and reanalysis :ssary for verification.
r:.confirmed by gc. .... : 1.when no value is reported. see chlordane constituents 2.constituents or metab~ .. ,es of technical chlordane
-E~EG-VS .. AT-,G--
Sample 12927 FY 1997 Project: 97-0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW12
Media: SURFACEWA D Number: MY88
RESULTS UNITS ANAL YTE
1 0UJ UG/L PHENOL
10UJ UG/L BIS(2-CHLOROETHYL) ETHER
10UJ UG/L 2-CHLOROPHENOL
10UJ UG/L 1,3-DICHLOROBENZENE
10UJ UG/L 1,4-DICHLOROBENZENE
10UJ UG/L 1,2-DICHLOROBENZENE
10UJ UG/L 2-METHYLPHENOL
10UJ UG/L BIS(2-CHLOROISOPROPYL) ETHER
10UJ UG/L (3-AND/OR 4-)METHYLPHENOL
10UJ UG/L N-NITROSODI-N-PROPYLAMINE
10UJ UG/L HEXACHLOROETHANE
10UJ UG/L NITROBENZENE
10UJ UG/L ISOPHORONE
10UJ UG/L 2-NITROPHENOL
10UJ UG/L 2,4-DIMETHYLPHENOL
10UJ UG/L BIS(2-CHLOROETHOXY)METHANE
10UJ UG/L 2,4-DICHLOROPHENOL
10UJ UG/L 1,2,4-TRICHLOROBENZENE
10UJ UG/L NAPHTHALENE
10UJ UG/L 4-CHLOROANILINE
10UJ UG/L HEXACHLOROBUTADIENE
10UJ UG/L 4-CHLORO-3-METHYLPHENOL
10UJ UG/L 2-METHYLNAPHTHALENE
10UJ UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ UG/L 2,4,6-TRICHLOROPHENOL
25UJ UG/L 2,4,5-TRICHLOROPHENOL
10UJ UG/L 2-CHLORONAPHTHALENE
25UJ UG/L 2-NITROANILINE
10UJ UG/L DIMETHYL PHTHALATE
1 0UJ UG/L ACENAPHTHYLENE
1 0UJ UG/L 2,6-DINITROTOLUENE
25UJ UG/L 3-NITROANILINE
10UJ UG/L ACENAPHTHENE
25UJ UG/L 2,4-DINITROPHENOL
25UJ UG/L 4-NITROPHENOL
10UJ UG/L DIBENZOFURAN
10UJ UG/L 2,4-DINITROTOLUENE
10UJ UG/L DIETHYL PHTHALATE
:f_ HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
Org Contractor: AA TS
RESULTS
10UJ
10UJ
25UJ
25UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09: 10
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE ·
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
Dt-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
}average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12927 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW12
Media: SURFACEWA
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY88
RESULTS UNITS
2JN UG/L
ANALYTE
TETRAMETHYLPHENANTHRENE
Org Contractor: AA TS
A-average value. NA-not analyzed. NAt-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:10
Ending:
K-actual value is k,.-,-•,,m to be less than value given. L-actual value is known to be greater than value giv--U-material was analyzed for but not detected. the number is the minimum quant•• ·=..,n limit.
R-qc indicates th:' 1 unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification.
C-confirmed by 91.._ 1.when no value is reported, see chlordane constituents 2.constituents or metal.. ~s of technical chlordane
--E~EG_, SIJllll'ATl-all, G~ --aaJuc...Vat"llal 119illiil49 -
Sample 12927 FY 1997 Project: 97 -0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF
Id/Station: RCSW12
Media: SURFACEWA
RESULTS UNITS
2J UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
Case Number: 25655
D Number: MY88
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
1; 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:10
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12927 FY 1997 Project: 97 -0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW12
Media: SURFACEWA D Number: MY88
RESULTS UNITS
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
25UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2.4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
-=:f_ HOLDING TIMES EXCEEDEO(40 CFR 136,OCTOBER 26,1984)
c:P--
Org Contractor: AA TS
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:10
Ending:
RESULTS UNITS ANALYTE
10UJ UG/L
10UJ UG/L
25UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~~ ··•r, to be less than value given. L-actual value is known to be greater than value gi1·· U-material was analyzed for but not detected. the number is the minimum quant•· ·-.,limit.
R-qc indicates th;: unusable. compound may or may not be present. resampling and reanalysis i: ssary for verification.
C-confirmed by gc... . 1.when no value is reported, see chlordane constituents 2.constituents or metab .... ____ ,s of technical chlordane
Sample 12927 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW12
Media: SURFACEWA D Number: MY88
RESULTS UNITS
2JN UG/L
ANALYTE
TETRAMETHYLPHENANTHRENE
Org Contractor: AA TS
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09: 1 O
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-.estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12927 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW12
Media: SURFACEWA D Number: MY88
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
2J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1. 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:10
Ending:
K-actual value is I-1 to be less than value given. L-actual value is known to be greater than value gi• U-material was analyzed for but not detected. the number is the minimum quanti' , limit.
R-qc indicates th; , unusable. compound may or may not be present. resampling and reanalysis i~ .ssary for verification.
r. .r:onfirmed by gCI1,::,,;· 1 .when no value is reported, see chlordane constituents 2.constituents or metabv ... 1::s of technical chlordane
-Sample 12928 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW16
Media: SURFACEWA D Number: MY89
RESULTS UNITS ANALYTE
10UJ UG/L PHENOL
10UJ UG/L BIS(2-CHLOROETHYL) ETHER
10UJ UG/L 2-CHLOROPHENOL
10UJ UG/L 1,3-DICHLOROBENZENE
10UJ UG/L 1,4-DICHLOROBENZENE
10UJ UG/L 1,2-DICHLOROBENZENE
10UJ UG/L 2-METHYLPHENOL
10UJ UG/L BIS(2-CHLOROISOPROPYL) ETHER
10UJ UG/L (3-AND/OR 4-)METHYLPHENOL
10UJ UG/L N-NITROSODI-N-PROPYLAMINE
10UJ UG/L HEXACHLOROETHANE
10UJ UG/L NITROBENZENE
10UJ UG/L ISOPHORONE
10UJ UG/L 2-NITROPHENOL
10UJ UG/L 2,4-DIMETHYLPHENOL
10UJ UG/L BIS(2-CHLOROETHOXY)METHANE
10UJ UG/L 2,4-DICHLOROPHENOL
10UJ UG/L 1,2,4-TRICHLOROBENZENE
10UJ UG/L NAPHTHALENE
10UJ UG/L 4-CHLOROANIUNE
10UJ UG/L HEXACHLOROBUTADIENE
10UJ UG/L 4-CHLORO-3-METHYLPHENOL
10UJ UG/L 2-METHYLNAPHTHALENE
10UJ UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ UG/L 2,4,6-TRICHLOROPHENOL
25UJ UG/L 2,4,5-TRICHLOROPHENOL
10UJ UG/L 2-CHLORONAPHTHALENE
25UJ UG/L 2-NITROANILINE
10UJ UG/L DIMETHYL PHTHALATE
10UJ UG/L ACENAPHTHYLENE
10UJ UG/L 2,6-DINITROTOLUENE
25UJ UG/L 3-NITROANILINE
1 0UJ UG/L ACENAPHTHENE
25UJ UG/L 2,4-DINITROPHENOL
25UJ UG/L 4-NITROPHENOL
10UJ UG/L DIBENZOFURAN
10UJ UG/L 2,4-DINITROTOLUENE
10UJ UG/L DIETHYL PHl'HALATE
~HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984) -
Org Contractor: AA TS
RESULTS
10UJ
10UJ
25UJ
25UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
K-actual value is kri"'"n to be less than value given. L-actual value is known to be greater than value giv<>-U-material was analyzed for but not detected. the number is the minimum quantit-•=-,n limit.
R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis i~ ssary for verification.
C-confirmed by gc.. 1.when no value is reported, see chlordane constituents 2.constituents or metab... j of technical chlordane
-Sample 1.o28 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW16
Media: SURFACEWA
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY89
40J UG/L 1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
- -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
\IIIIITIL ...... IVlllllf,N~S ---E~E~VS-AT .. ,G_ --Sample 12~28 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW16
Media: SURFACEWA O Number: MY89 Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r:-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
WJ! ::y p: EWPL'ilMtf<Lvall
Sample 12928 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW16
Media: SURFACEWA D Number: MY89
RESULTS UNITS ANALYTE
10UJ UG/L PHENOL
10UJ UG/L BIS(2-CHLOROETHYL) ETHER
10UJ UG/L 2-CHLOROPHENOL
1 0UJ UG/L 1,3-DICHLOROBENZENE
10UJ UG/L 1,4-DICHLOROBENZENE
10UJ UG/L 1,2-DICHLOROBENZENE
1 0UJ UG/L 2-METHYLPHENOL
10UJ UG/L BIS(2-CHLOROISOPROPYL) ETHER
10UJ UG/L (3-AND/OR 4-)METHYLPHENOL
10UJ UG/L N-NITROSODI-N-PROPYLAMINE
10UJ UG/L HEXACHLOROETHANE
10UJ UG/L NITROBENZENE
10UJ UG/L ISOPHORONE
10UJ UG/L 2-NITROPHENOL
10UJ UG/L 2,4-DIMETHYLPHENOL
10UJ UG/L BIS(2-CHLOROETHOXY)METHANE
1 0UJ UG/L 2,4-DICHLOROPHENOL
10UJ UG/L 1,2,4-TRICHLOROBENZENE
1 0UJ UG/L NAPHTHALENE
10UJ UG/L 4-CHLOROANILINE
10UJ . UG/L HEXACHLOROBUTADIENE
1 0UJ UG/L 4-CHLORO-3-METHYLPHENOL
10UJ UG/L 2-METHYLNAPHTHALENE
10UJ UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ UG/L 2,4,6-TRICHLOROPHENOL
25UJ UG/L 2,4,5-TRICHLOROPHENOL
1 0UJ UG/L 2-CHLORONAPHTHALENE
25UJ UG/L 2-NITROANILINE
10UJ UG/L DIMETHYL PHTHALATE
1 0UJ UG/L ACENAPHTHYLENE
10UJ UG/L 2,6-DINITROTOLUENE
25UJ UG/L 3-NITROANILINE
10UJ UG/L ACENAPHTHENE
25UJ UG/L 2,4-DINITROPHENOL
25UJ UG/L 4-NITROPHENOL
10UJ UG/L DIBENZOFURAN
10UJ UG/L 2,4-DINITROTOLUENE =:S? 10UJ UG/L DIETHYL PHTHALATE
_::1-HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
-me-Da-/02,_:50-
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
Org Contractor: AA TS
RESULTS UNITS
10UJ UG/L
10UJ UG/L
25UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
25UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
10UJ UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
OI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA.not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~ ··n to be less than value given. L-actual value is known to be greater than value gi• U-material was analyzed for but not detected. the number is the minimum quan1· ·n limit.
R-qc indicates th. 1 unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
r.-cOnfirmed by gc,. .. ~.-1.when no value is reported, see chlordane constituents 2.constituents or metabl, ... ~s of technical chlordane
~c-c'>-PL~L~ -Sample 12928 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF .
Id/Station: RCSW16
Media: SURFACEWA
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY89
40J UG/L 1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
,...._r,onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12SJ / FY 1997 Project: 97-0357
EXTRACT ABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW7
Media: SURFACEWA D Number: MY18
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10UJ
10U
10U
IUU ·
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS ANAL YTE
UG/L PHENOL
UG/L BIS(2-CHLOROETHYL) ETHER
UG/L 2-CHLOROPHENOL
UG/L 1,3-DICHLOROBENZENE
UG/L 1,4-DICHLOROBENZENE
UG/L 1,2-DICHLOROBENZENE
UG/L 2-METHYLPHENOL
UG/L BIS(2-CHLOROISOPROPYL) ETHER
UG/L (3-AND/OR 4-)METHYLPHENOL
UG/L N-NITROSODI-N-PROPYLAMINE
UG/L HEXACHLOROETHANE
UG/L NITROBENZENE
UG/L ISOPHORONE
UG/L 2-NITROPHENOL
UG/L 2,4-DIMETHYLPHENOL
UG/L BIS(2-CHLOROETHOXY)METHANE
UG/L 2,4-DICHLOROPHENOL
iJG,-t:__,._-·'i.,L.4-TRi(;HLOROtst:NzE~N=E~. ==
UG/L NAPHTHALENE
UG/L 4-CHLOROANILINE
UG/L HEXACHLOROBUTADIENE
UG/L 4-CHLORO-3-METHYLPHENOL
UG/L 2-METHYLNAPHTHALENE
UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
UG/L 2,4,6-TRICHLOROPHENOL
UG/L 2,4,5-TRICHLOROPHENOL
UG/L 2-CHLORONAPHTHALENE
UG/L 2-NITROANILINE
UG/L DIMETHYL PHTHALATE
UG/L ACENAPHTHYLENE
UG/L 2,6-DINITROTOLUENE
UG/L 3-NITROANILINE
UG/L ACENAPHTHENE
UG/L 2,4-DINITROPHENOL
UG/L 4-NITROPHENOL
UG/L DIBENZOFURAN
UG/L 2,4-DINITROTOLUENE
UG/L DIETHYL PHTHALATE
Org Contractor: AA TS
-ii11f uctall'ale lliili1119iii116 -
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:45
Ending:
RESULTS UNITS ANALYTE
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10UJ UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is lhe minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-- -·-- - -
EPA -REGION IV f'-~o, ATHENS, GA --- - - - -
Production Date: 1 r · ·· '97 07:49
Sample 12937 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW7
Media: SURFACEWA D Number: MY18
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10I I
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U.
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
-UG!!....-
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UGIL
UG/L
UGIL
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
.:1. '1 n,,-,.u1.0nr.r:,,...,_,...,..,. A.,,... . --·,-..... , ...... , ,1-:.....,,,=, ,,vrnl\lC
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08124197 10:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12937 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW!
Media: SURFACEWA
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY18
10J UG/L 1 UNIDENTIFIED COMPUND
Org Contractor: AA TS
- -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
· 11.-lTILlall/llllllall\N.AIIIIIS ---E~EC,-VS-AT..,,G_ --; .
Sample 12937 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW7
Media: SURFACEWA D Number: MY18 Org Contractor: AA TS
RESULTS UNITS
10U UG/L
IOU UG/L
10U UG/L
IOU UG/L
10U UG/L
10U UG/L
10U UG/L
IOU UG/L
10U UG/L
10U UG/L
IOU UG/L
IOU UG/L
IOU UG/L
IOU UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
IOU UG/L
IOU UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
IOU UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actuaf value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
"Wi1111TILii1111'MlliitNA'IMIW3 --Sample 12937 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW7
Media: SURFACEWA D Number: MY18 Org Contractor: AA TS
RESULTS UNITS ANALYTE
10J UG/L 1 UNIDENTIFIED COMPUND
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:45
Ending:
K-actual value is_' ·n to be less than value given. L-actual value is known to be greater than value gi· U-material was analyzed for but not detected. the number is the minimum quant=· -,.,n limit
R-qc indicates th ~ unusable. compound may or may not be present. resampling and reanalysis i Jssary for verification.
r, -r.onfirmed by gc1 ,...,,; 1.when no value is reported, see chlordane constituents 2.constituents or metab,:. ..• .::s of technical chlordane
--Sample 12954 FY 1997 Project: 97-0357
METALS SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW18
Media: SURFACEWA
RESULTS UNITS ANALYTE
3U UG/L SILVER
2U UG/L ARSENIC
51 UG/L BARIUM
1U UG/L BERYLLIUM
2U UG/L CADMIUM
3U UG/L COBALT
6U UG/L CHROMIUM
6U UG/L COPPER
10U UG/L NICKEL
9 UG/L LEAD
50U UG/L ANTIMONY
1U UG/L SELENIUM
2U UG/L THALLIUM
8J UG/L VANADIUM
30 UG/L ZINC
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36
D Number: MY83
0.2UJ UG/L TOTAL MERCURY
4900 UG/L ALUMINUM
46 UG/L MANGANESE
13000 UG/L CALCIUM
1600 UG/L MAGNESIUM
13000 UG/L IRON
12000 UG/L SODIUM
1900 UG/L POTASSIUM
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumplive evidence of presence of material.
- -
Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R:-<ic indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r -r:onfirmed bv acms: 1.when no value is reported. see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12954 FY 1997
SPECIFIED TESTS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW18
Media: SURFACEWA
RES UL TS UNITS
SU UG/L
ANALYTE
CYANIDE
Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36
D Number: MY83
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Keith Bales
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09:15
Ending:
K-actual value is·~-vn to be less than value given. L-actual value is known to be greater than value U-material was analyzed for but not detected. the number is the minimum qu.-R-qc indicates ti :a unusable. compound may or may not be present. resampling and reanalysis .;essary for verification. C---confirmed by g ...... ,:;: 1.when no value is reported, see chlordane constituents 2.constituents or metabuutes of technical chlordane
on limit.
Sample 12954 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36 Id/Station: RCSW18
Media: SURFACEWA D Number: MY83
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL} ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL} ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP}
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
10U
10U
25U
25U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
Produced by: J.ohn Mcconney
Requestor: RAY DOYLE
Project L~ader: DOYLE
Beginning: 08/26/97 09: 15
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB}
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A}ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL} PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K}FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD} PYRENE
DIBENZO(A,H}ANTHRACENE
BENZO(GHl}PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kn"wn to be less than value given. L-actual value is known to be greater than value gi"~"-U-material was analyzed for but not detected. the number is the minimum quani:• ·•ion limit.
R-qc indicates th ·a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by {I 1.when no value is reported, see chlordane constituents 2.constituents or meta. ..:s of technical chlordane
-Sample 12954 FY 1997
PESTICIDES SCAN
Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36 Id/Station: RCSW18
Media: SURFACEWA D Number: MY83
RESULTS UNITS ANALYTE
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.050U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.50U
0.10U
0.10U
0.050U
0.050U
5.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: ARI
Org Contractor: AA TS
--Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09: 15
Ending:
A-average value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kpnwn to be less than value given. L-actual value is known to be greater than value gi•·--U-material was analyzed for but not detected. the number is the minimum quan•· ·,n limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification.
C-confirmed by g(_ . 1.when no value is reported, see chlordane constituents 2.constituents or metal .. ..:S of technical chlordane
-Sample 12954 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36 Id/Station: RCSW18
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
D Number: MY83
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
---uct-ate-1/91IIIF9 -
Produced by: John· Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26197 09:15
Ending:
K-actual value is J<.--· ··11 to be less than value given. L-actual value is known to be greater than value giv-U-material was analyzed for but not detected. the number is the minimum quant;• ·· "n limit.
R-qc indicates th; unusable. compound may or may not be present. resampling and reanalysis i: ssary for verification.
r.-r:onfirmed by gc... . 1.when no value is reported, see chlordane constituents 2.constituents or metab ... __ .;; of technical chlordane
-Sample 12954 FY 1997 Project: 97-0357
EXTRACT ABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW18 MD Number: MY36
Media: SURFACEWA D Number: MY83
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09:15
Ending:
RESULTS UNITS ANALYTE
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
- --· -·-PESTICIDES/P~'3 SAMPLl:ANAL YS'TS'"" -Sample 12954 FY 1997 Project: 97-0357
PESTICIDES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW18 MD Number: MY36
Media: SURFACEWA D Number: MY83
RESULTS UNITS
0.050U UG/L
0.050U UGIL
0.050U UGIL
0.050U UG/L
0.050U UG/L
0.050U UGIL
0.050U UGIL
0.050U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L a.sou UGIL
0.10U UG/L
0.10U UG/L
0.050U UG/L
0.050U UG/L
5.0U UG/L
1.0U UG/L
2.0U UG/L
1.0U UG/L
1.0U UGIL
1.0U UGIL
1.0U UG/L
1.0U UGIL
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: ARI
Org Contractor: AA TS
--alllrne,..Dat-"~'-:40 -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: .DOYLE
Beginning: 08/26/97 09: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r,-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--- -
VOLATILES SJI UPLE ANALYSIS - -
Sample 12954 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY36 Id/Station: RCSW18
Media: SURFACEWA
RES UL TS UNITS
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UGIL
D Number: MY83
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
10U UGIL
10U UGIL
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UGIL
10U UG/L
10U UG/L
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
,.... ---nnfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
----- --METALS sAr···· E ANALYSIS
Sample 12955 FY 1997 Project: 97-0357
METALS SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW15
Media: SURFACEWA
RESULTS UNITS ANALYTE
3U UG/L SILVER
2U UG/L ARSENIC
31 UG/L BARIUM
1U UG/L BERYLLIUM
2U UG/L CADMIUM
3U UG/L COBALT
5U UG/L CHROMIUM
2U UG/L COPPER
10U UG/L NICKEL
3U UG/L LEAD
sou UG/L ANTIMONY
1U UG/L SELENIUM
2U UG/L THALLIUM
3U UG/L VANADIUM
29 UG/L ZINC
CASTLE HAYNE. NC
Case Number: 25655
MD Number: MY37
D Number: MY84
0.10UJ UG/L TOTAL MERCURY
690 UG/L ALUMINUM
59 UG/L MANGANESE
10000 UG/L CALCIUM
1800 UG/L MAGNESIUM
11000 UG/L IRON
7900 UG/L SODIUM
1700 UG/L POTASSIUM
-----EPA-REGION IV~--'J, ATHENS, G~ --
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
A-average value. NA-not analyzed. NAl-interlerenccs. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r".-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12955 FY 1997
SPECIFIED TESTS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSW15
Media: SURFACEWA
RESULTS UNITS
5U UG/L
ANALYTE
CYANIDE
Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY37
D Number: MY84
lnorg Contractor: ARI
Org Contractor: AA TS
--Produced by: Keith Bates
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1· •1n to be less than value given. L-actual value is known to be greater than valuer· U-material was analyzed for but not detected. the number is the minimum qua·
R-qc indicates 1~-a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by 91... __ ..,_ 1.when no value is reported, see chlordane constituents 2.constituents or metabv11l€S of technical chlordane
Sample 12955 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW15 MD Number: MY37
Media: SURFACEWA D Number: MY84
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Jo.hn Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
RESULTS UNITS ANALYTE
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is. 1,,---,...,n to be less than value given. L-actual value Is known to be greater than value g;· -U-material was analyzed for but not detected. the number is the minimum quar··· •:on limit.
R-qc indicates tt a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by 9~ . . 1.when no value is reported, see chlordane constituents 2.constituents or mela1.,. __ --~s of technical chlordane
-Sample 12955 FY 1997 Project: 97 -0357
PESTICIDES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY37 Id/Station: RCSW15
Media: SURFACEWA
RESULTS
o.osou
0.0S0U o.osou
0.0S0U
0.050U
0.050U
0.0S0U
0.0S0U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U a.sou
0.10U
.10U
0.050U
0.0S0U
5.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
1.0U
UNITS
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/l
UG/L
UG/l
UG/l
D Number: MY84
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumplive evidence of presence of material.
--Produced by: John Mcconney
Requester: RAY DOYLE
Project leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
K-actual value is kr>"'-Vn to be less than value given. L-actual value is known to be greater than value giv-~ LI-material was analyzed for but not detected. the number is the minimum quan*" -,,n limit.
R-qc indicates th~ 1 unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification.
C-confirmed by QL _ _ 1.when no value is reported, see chlordane constituents 2.constituents or metal ~s of technical chlordane
-Sample 12955 FY 1997
VOLATILES SCAN
Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY37 Id/Station: RCSW15
Media: SURFACEWA D Number: MY84
RES UL TS UNITS ANAL YTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
2J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A~average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
K-actual value is knew,., to be less than value given. L-actua1 value is known to be greater than value giveri U-material was analyzed for but not detected. the number is the minimum quantitatinn limit.
R-qc indicates that •_musable. compound may or may not be present. resampling and reanalysis is :sary for verification.
C-confirmed by gcr. . .when no value is reported, see chlordane constituents 2.constituents or metabt. of technical chlordane
-Sample 1 i~ss FY 1997
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL
Program: NSF
Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY37 Id/Station: RCSW15
Media: SURFACEWA
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
D Number: MY84
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
RESULTS UNITS ANALYTE
10U UG/L
10U UG/L
25U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
25U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actua1 value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ICl~<'"l-PLiaao.L~ -Sample 12955 FY 1997 Project: 97-0357
PESTICIDES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW15 MD Number: MY37
Media: SURFACEWA D Number: MY84
RESULTS UNITS
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.050U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
0.10U UG/L
a.sou UG/L
0.10U UG/L
.10U UG/L
0.050U UG/L
0.050U UG/L
5.0U UG/L
1.0U UG/L
2.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
1.0U UG/L
ANALYTE
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P,P'-DDE)
ENDRIN
ENDOSULFAN 11 (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
ALPHA-CHLORDANE /2
GAMMA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
lnorg Contractor: ARI
Org Contractor: AA TS
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08126/97 10:25
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~Tlt.alfAM~N,,..IS -
· Sample 12955 FY 1997 Project: 97 -0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW15 MD Number: MY37
Media: SURFACEWA D Number: MY84
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
2J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BRDMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
---Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
A-ave,og~ value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value i:; lrnown to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates thal r.otz. unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
!:-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--Sample 13;,, FY 1998 Project: 98-0109
DIOXIN SCAN
Facility: Reasor Chemical Castle Hayne, NC
Program: SSF
Id/Station: RCSW1
Media: WATER
RESULTS
0.020U
0.04UJ
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.0SOUJ
0.050U
0.050UJ
0.10U
0.020U
0.020UJ
0.050U
0.050U
0.050UJ
0 .. 050U o .. osou
0 .. 050U
0 .. 050U
0.050UJ
0.050U
0.050U
0.050UJ
0.10U
0.0
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
D Number: SW1
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL)
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3, 7 ,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL)
1,2,3.4,6,7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL)
OCTACHLORODIBENZODIOXIN
2,3, 7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (TOTAL)
1,2,3, 7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL)
1,2,3.4, 7 ,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,6, 7 ,8-HEPTACHLORODIBENZOFURAN
1,2,3,4 ,7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL)
OCTACHLORODIBENZOFURAN
TEQ (TOXIC. EQUIV. VALUE, FROM I-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
llatuc!llll)at.-,7 '~-43 -
Produced by: John Mcconney
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02/97 09: 15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-malerial was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resarnpling and reanalysis is necessary for verification.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-ll't~-lt"L111111AL Y. --Sample 1333 FY 1998 Project: 98-0109
DIOXIN SCAN
Facility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Id/Station: RCSW2
Media: WATER
RESULTS UNITS
0.020U
0.020UJ
0.050U
0.OS0UJ
0.0S0U
0.0S0U
0.050U
0.050UJ o.osou
0.050UJ
0.10U
0.020U
0.020UJ
0.050U
0.0S0U
0.050UJ
0.050U
0.050U o.osou
0.050U
0.0S0UJ
0.0S0U
0.0S0U
0.0S0UJ
0.10U
0.0
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
. NG/L
D Number: SW2
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL)
1,2,3, 7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7 ,8-HEXACHLORODIBENZODIOXIN
1,2,3, 7,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL)
OCTACHLORODIBENZODIOXIN
2,3, 7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (TOTAL)
1,2 ,3,7 ,8-PE NTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,7 ,8-HEXACHLORODIBENZOFURAN
1,2,3,6, 7 ,8-HEXACHLORODIBENZOFURAN
1,2,3, 7 ,8,9-HEXACHLORODIBENZOFURAN
2,3 ,4 ,6,7 ,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (TOTAL)
1,2,3,4 ,6, 7 ,8-HEPTACHLORODIBENZOFURAN
1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL)
OCTACHLORODIBENZOFURAN
TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
A-average value. NA-not analyzed. NAl-"tnterlerences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John McConney
Requester: Jennifer Wendel
Project Leader:
Beginning: 12102197 10:15
Ending:
K-actual value is krinu,,n to be less than value given. L-adual value Is known to be greater than value gi· U-material was analyzed for but not detected. the number Is the minimum quar R-qc indicates lh< 1 unusable. compound may or may not be present. resampling and reanalysis i .!ssary for verification. C-confirmed by gL. 1.when no value is reported, see chlordane constituents 2.constiluents or metab ...... ~S of technical chlordane
·n limit.
~NS..,Lf:mtLY---
Sample tJA FY 1998 Project: 98-0109
DIOXIN SCAN
Facility: Reasor Chemical Castle Hayne, NC
Program: SSF
Id/Station: RCSW3
Media: WATER
RESULTS
0.020U
0.020UJ
O.0S0U
0.0SOUJ
O.0SOU
O.OSOU o.osou
O.0SOUJ
O.0SOU
0.0SOUJ
0.10U
0.020U
0.020UJ
O.OSOU
O.OSOU
0.OSOUJ
0.0S0U
0.0SOU
O.0SOU
O.OS0U
0.0S0UJ
0.0SOU
0.0SOU
0.OSOUJ
0.10U
0.0
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
D Number: SW3
ANALYTE
2,3,7,8°TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL)
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3, 7 ,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL)
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (TOTAL)
1,2,3, 7 ,8-PENTACHLORODIBENZOFURAN
2,3,4, 7 ,8-PENT ACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (TOTAL)
1,2,3,4 ,6, 7 ,8-HEPTACHLORODIBENZOFURAN
1,2,3,4, 7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL)
OCTACHLORODIBENZOFURAN
TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
Produced by: John Mcconney
Requestor: Jennifer Wendel
Project Leader: ·
Beginning: 12/02/97 12:00
Ending:
A-average value. NA-not analyzed. NA\-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-·-·····------~•-.. ---t:~t:\;-VS-AT,.,G_ ---du'i) D~t-17/-:43-~ Sample 1335 FY 1998 Project: 98-0109 DIOXIN SCAN Facility: Reasor Chemical Castle Hayne, NC Program: SSF Id/Station: RCSW4 Media: WATER RESULTS 0.020U 0.020UJ 0.050U 0.050UJ 0.050U 0.050U 0.050U 0.050UJ 0.050U 0.050UJ 0.10U 0.020U 0.020UJ 0.050U 0.050U 0.050UJ 0.050U 0.050U 0.050U 0.050U 0.050UJ 0.050U 0.050U 0.050UJ 0.10U 0.0 UNITS NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L NG/L D Number: SW4 ANALYTE 2,3,7,8-TETRACHLORODIBENZODIOXIN TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3, 7 ,8-PENT ACHLORODIBENZODIOXIN PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZODIOXIN 1,2,3,6, 7 ,8-HEXACHLORODIBENZODIOXIN 1,2,3, 7 ,8,9-HEXACHLORODIBENZODIOXtN HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLORODIBENZODIOXIN 2,3,7,8-TETRACHLORODIBENZOFURAN TETRACHLORODIBENZOFURAN (TOTAL) 1,2,3, 7 ,8-PENTACHLORODIBENZOFURAN 2,3,4,7,8-PENTACHLORODIBENZOFURAN PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4, 7 ,8-HEXACHLORODIBENZOFURAN 1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN 1,2,3,7,8,9-HEXACHLORODIBENZOFURAN 2,3,4,6,7,8-HEXACHLORODIBENZOFURAN HEXACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN 1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN HEPTACHLOROOIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89) SAS Number:DIOX Org Contractor: SWOK A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: John McConney Requester: Jennifer Wendel Project Leader: Beginning: 12/02/97 12:15 Ending: K-actual value is known lo be less than value given. L-actual value is known to be greater than value givf>.. U-malerial was analyzed for but not'detected. the number is the minimum quanti• 1 limit. R-qc indicates that unusable. compound may or may not be present. resampling and reanalysis is >sary for verification. C-confirmed by ga, .when no value is reported, see chlordane constituents 2.conslituents or metab1.. ~ of technical chlordane
-Sample 12928 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSW16
Media: SURFACEWA D Number: MY89 Org Contractor: AA TS
RESULTS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 14:40
Ending:
K-actual value is ' ~ ·•n to be less than value given. L-actual value is known to be greater than value gi• U-material was analyzed for but not detected. the number is the minimum quan"' •:,m limit.
R-qc indicates th 3 unusable. compound may or may not be present. resampling and reanalysis e-ssary for verification.
r -r:onfirmed by QL.. ...... 1.when no value is reported, see chlordane constituents 2.constituents or meta1.,_ .~s of technical chlordane
-IN~PL-AL'ta -Sample 13006 FY 1997 Project: 97-0358
DIOXIN SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF
Id/Station: RCSW18
Media: GROUNDWA
RESULTS
0.020U
0.020UJ
0.050U
0.050UJ
0.050U
0.050U
0.050U
O.OSOUJ
0.019J
0.042J
0.20
0.020U
0.020UJ
O.OSOU
0.OS0U
0.OSOUJ
0.050U o.osou
0.0SOU
0.OS0U
0.OSOUJ o.osou
O.OS0U
0.OS0UJ
0.10U
0.0004J
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
D Number: SW18
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL)
1,2,3, 7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4, 7 ,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3, 7 ,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL)
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (TOTAL)
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL)
1,2,3,4, 7 ,8-HEXACHLORODIBENZOFURAN
1,2,3,6, 7 ,8-HEXACHLORODIBENZOFURAN
1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,6, 7 ,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL)
OCTACHLORODIBENZOFURAN
TEO (TOXIC. EQUIV. VALUE, FROM I-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 09: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence or presence of material.
K-actual value is kr~-.,n to be less than value given. L-actual value is known to be greater than value gi· U-material was analyzed for but not detected. the number is the minimum quan' n limit.
R-qc indicates th< · unusable. compound may or may not be present. resampling and reanalysis i !ssary for verification.
C-confirmed by gc., ... 1.when no value is reported, see chlordane constituents 2.constituents or metab ....... ..::s of technical chlordane
--Sample 13009 FY 1997 Project: 97-0358
DIOXIN SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF
Id/Station: RCSW15
Media: GROUNDWA D Number: SW15
RESULTS
0.020U
0.020UJ
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050UJ
0.049J
0.020U
0.020UJ
0.050U
0.050U
0.050UJ o.osou
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050U
0.050UJ
0.10U
0.00005
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL)
1,2,3. 7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4, 7 ,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7 ,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL)
1,2,3,4,6, 7 ,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL)
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (TOTAL)
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2.3,4,7,8-PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6, 7 ,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (TOTAL)
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL)
OCTACHLORODIBENZOFURAN
TEO (TOXIC. EQUIV. VALUE, FROM 1-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/26/97 10:25
Ending:
K-acluat value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 1329 FY 1998 Project: 98-0109
DIOXIN SCAN
Facility: Reasor Chemical Castle Hayne, NC
Program: SSF
Id/Station: RCSW13
Media: WATER
RESULTS
0.020U
0.020UJ
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050UJ
0.10U
0.020U
0.020UJ
0.050U
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050U
0.050UJ
0.10U
0.0
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
D Number: SW13
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (fOTAL)
1,2,3, 7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (fOTAL) 1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7 ,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (fOTAL)
1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (fOTAL) OCTACHLORODIBENZODIOXIN
2,3, 7,8-TETRACHLORODIBENZOFURAN
TETRACHLORODIBENZOFURAN (fOTAL)
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2 ,3,4 ,7 ,8-PENTACHLORODI BENZOFURAN PENTACHLORODIBENZOFURAN (fOTAL) 1,2,3,4, 7,8-HEXACHLORODIBENZOFURAN
1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN
1,2,3, 7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
HEXACHLORODIBENZOFURAN (fOTAL)
· 1,2,3,4,6, 7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4 ,7 ,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (fOTAL) OCTACHLORODIBENZOFURAN
TEO (fOXIC. EQUIV. VALUE, FROM I-TEF/89)
SAS Number:DIOX
Org Contractor: SWOK
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
-_,du-Dalllll/17~:43-
Produced by: John McConney
Requester: Jennifer Wendel
Project Leader:
Beginning: 12/02197 15:15
Ending:
K-actual value is kn,...-. ., lo be less than value given. l-actual value is known to be greater than value gh· •J-material was analyzed for but not detected. the number is the minimum quanl · Jimlt. R-qc indicates that 'Jnusable. compound may or may not be present. resampling and reanalysis is 5Sary for verification. C-confirmed by gcr,. , .when no value is reported, see chlordane constituents 2.constituents or metabo111cs of technical chlordane
<:::ro· -
- --·--1!!!1! - - - -
EPA -REGIONlV S'" '1, ATHENs, GA
Sample 12911 FY 1997 Project: 97.0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE7
Media: SOIL D Number: MY70
RESULTS UNITS ANALYTE
530U UG/KG PHENOL
530U UG/KG BIS(2-CHLOROETHYL) ETHER
530U UG/KG 2-CHLOROPHENOL
530U UG/KG 1,3-DICHLOROBENZENE
530U UG/KG 1,4-DICHLOROBENZENE
530U UG/KG 1,2-DICHLOROBENZENE
530U UG/KG 2-METHYLPHENOL
530U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
530U UG/KG (3-AND/OR 4-)METHYLPHENOL
530U UG/KG N-NITROSODI-N-PROPYLAMINE
530U UG/KG HEXACHLOROETHANE
530U UG/KG NITROBENZENE
530U UG/KG ISOPHORONE
530U UG/KG 2-NITROPHENOL
530U UG/KG 2,4-DIMETHYLPHENOL
530U UG/KG BIS(2-CHLOROETHOXY)METHANE
530U UG/KG 2,4-DICHLOROPHENOL
530U UG/KG 1,2,4-TRICHLOROBENZENE
530U UG/KG NAPHTHALENE
530U UG/KG 4-CHLOROANILINE
530U UG/KG HEXACHLOROBUTADIENE
530U UG/KG 4-CHLORO-3-METHYLPHENOL
530U UG/KG 2-METHYLNAPHTHALENE
530U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
530U UG/KG 2,4,6-TRICHLOROPHENOL
1300U UG/KG 2,4,5-TRICHLOROPHENOL
530U UG/KG 2-CHLORONAPHTHALENE
1300U UG/KG 2-NITROANILINE
530U UG/KG DIMETHYL PHTHALATE
530U UG/KG ACENAPHTHYLENE
530U UG/KG 2,6-DINITROTOLUENE
1300U UG/KG 3-NITROANILINE
530U UG/KG ACENAPHTHENE
1300U UG/KG 2,4-DINITROPHENOL
1300U UG/KG 4-NITROPHENOL
530U UG/KG DIBENZOFURAN
530U UG/KG 2,4-DINITROTOLUENE
530U UG/KG DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
RESULTS UNITS ANALYTE
530U
530U
1300U
1300U
530U
530U
530U
1300U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
38
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12911 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE7
Media: SOIL
RESULTS UNITS
300JN UG/KG
3000J UG/KG
300JN UG/KG
7000J UG/KG
D Number: MY70
ANALYTE
METHYL (METHYL ETHYL) PHENANTHRENE
ALKANES
CARBOXYLIC ACID
4 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
K-actual value is" ·..,n to be less than value given. L-actual value is known to be greater than value gr LI-material was anatyzed for but not detected. the number is the minimum quan•·· ·,n limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis ~ssary for verification.
C-confirmed by Q1.. ____ , 1.when no value is reported, see chlordane constituents 2.constituents or metab ....... G!·s of technical chlordane
-Sample 12911 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE7
Media: SOIL D Number: MY70
RESULTS UNITS ANALYTE
530U UG/KG PHENOL
530U UG/KG BIS(2-CHLOROETHYL) ETHER
530U UG/KG 2-CHLOROPHENOL
530U UG/KG 1,3-DICHLOROBENZENE
530U UG/KG 1,4-DICHLOROBENZENE
530U UG/KG 1,2-DICHLOROBENZENE
530U UG/KG 2-METHYLPHENOL
530U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
530U UG/KG (3-AND/OR 4-)METHYLPHENOL
530U UG/KG N-NITROSODI-N-PROPYLAMINE
530U UG/KG HEXACHLOROETHANE
530U UG/KG NITROBENZENE
530U UG/KG ISOPHORONE
530U UG/KG 2-NITROPHENOL
530U UG/KG 2,4-DIMETHYLPHENOL
530U UG/KG BIS(2-CHLOROETHOXY)METHANE
530U UG/KG 2,4-DICHLOROPHENOL
530U UG/KG 1,2,4-TRICHLOROBENZENE
530U UG/KG NAPHTHALENE
530U UG/KG 4-CHLOROANILINE
530U UG/KG HEXACHLOROBUTADIENE
530U UG/KG 4-CHLORO-3-METHYLPHENOL
530U UG/KG 2-METHYLNAPHTHALENE
530U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
530U UG/KG 2,4,6--TRICHLOROPHENOL
1300U UG/KG 2,4,5-TRICHLOROPHENOL
530U UG/KG 2-CHLORONAPHTHALENE
1300U UG/KG 2-NITROANILINE
530U UG/KG DIMETHYL PHTHALATE
530U UG/KG ACENAPHTHYLENE
530U UG/KG 2,6-DINITROTOLUENE
1300U UG/KG 3-NITROANILINE
530U UG/KG ACENAPHTHENE
1300U UG/KG 2,4-DINITROPHENOL
1300U UG/KG 4-NITROPHENOL
530U UG/KG DIBENZOFURAN
€:Jo" 530U UG/KG 2,4-DINITROTOLUENE
~ 530U UG/KG DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
530U
530U
1300U
1300U
530U
530U
530U
1300U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
38
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-adual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12911 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE7
Media: SOIL
RESULTS UNITS
300JN UG/KG
3000J UG/KG
300JN UG/KG
7000J UG/KG
D Number. MY70
ANALYTE
METHYL(METHYLETHYL)PHENANTHRENE
ALKANES
CARBOXYLIC ACID
4 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
;4 --Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k----.. n to be less than value given. L-actual value is known to be greater than value giv---U-material was analyzed for but not detected. the number is the minimum quantit~•:,..n limit.
R-qc indicates th; , unusable. compound may or may not be present. resampling and reanalysis i· "issary for verification.
C-confirmed by gc.._ ./ 1.when no value is reported, see chlordane constituents 2.constituents or metaL, ... ~$ of technical chlordane
-
-Sample 12912 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSEB
Media: SOIL D Number: MY71
RESULTS
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
870U
350U
870U
350U
350U
350U
870U
350U
870U
870U
350U
350U
350U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6--TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6--DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
350U
350U
870U
870U
350U
350U
350U
870U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
5
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
¾MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
EX.-:;TPJA-it;; S .... E ~SI ... -Sample 12912 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSEB
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY71
RESULTS UNITS
100JN UG/KG
ANALYTE
CARBOXYLIC ACID
Org Contractor: AA TS
300JN UG/KG
500JN UG/KG
5000J UG/KG
METHYL (METHYL ETHYL) PHENANTHRENE
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
7 UNIDENTIFIED COMPOUNDS
1000J UG/KG ALKANES
-Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is krv·""'" to be less than value given. L-actual value is known to be greater than value giVP" U-material was analyzed for but not detected. the number is the minimum quanm~•:.,n limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis if ssary for verification.
C-confirmed by gc...._ I.when no value is reported, see chlordane constituents 2.constituents or metab, .; of technical chlordane
-
-Sample 12912 FY 1997 Project: 97-0357
EXTRACTABLESSCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE8
Media: SOIL D Number: MY71
RESULTS
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
350U
870U
350U
870U
350U
350U
350U
870U
350U
870U
870U
350U
350U
350U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENT ADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2,CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
RESULTS UNITS ANALYTE
350U UG/KG
350U UG/KG
870U UG/KG
870U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
870U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
350U UG/KG
5 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
1-l( :T S,.._E A"-_,,fSI--Sample 12912 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSEB
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY71
RESULTS UNITS
100JN UG/KG
ANALYTE
CARBOXYLIC ACID
Org Contractor: AA TS
300JN UG/KG
500JN UG/KG
5000J UG/KG
METHYL (METHYL ETHYL) PHENANTHRENE
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
7 UNIDENTIFIED COMPOUNDS
1000J UG/KG ALKANES
- -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J..-estimated value. N-presumptive evidence of presence of material.
K-actual value is kr ··, to be less than value given. L-actual value is known to be greater than value giv' LI-material was analyzed for but not detected. the number is the minimum quantif ·· 1 limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis i:: ssary for verification.
r,-confirmed by gc:,,, __ . 1.when no value is reported, see chlordane constituents 2.constituents or metabL ... ...:s of technical chlordane
E--CT.111!"s ~LE --YSll!!IIII -Sample f2~13 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE9
Media: SOIL D Number: MY72
RESULTS
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
5100J
17000U
17000U
17000U
8400J
17000U
17000U
44000U
17000U
44000U
17000U
17000U
17000U
44000U
17000U
44000U
44000U
17000U
17000U
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE a::s 17000U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG DIETHYL PHTHALATE
_St
Org Contractor: AA TS
RESULTS
17000U
17000U
44000U
44000U
17000U
17000U
17000U
44000U
11000J
17000U
17000U
17000U
8400J
20000
17000U
17000U
17000U
14000J
17000U
17000U
17000U
17000U
17000U
17000U
17000U
24
A-average value. NA-not analyzed. NAl-interferences. J.estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported. see chlordane constituents 2.constituents or metabolites of technical chlordane
.c S _, LE liiiilL Y~ -Sample 12913 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE9
Media: SOIL
RESULTS UNITS
60000JN UG/KG
50000JN UG/KG
1 00OO00J UG/KG
40000JN UG/KG
60000JN UG/KG
50000JN UG/KG
1000000J UG/KG
D Number: MY72
ANALYTE
DIMETHYLNAPHTHALENE
TRIMETHYLNAPHTHALENE
ALKANES
METHYLDIBENZOTHROPHENE
DIMETHYLNAPHTHOTHIOPHENE
DIMETHYLPHENANTHRENE
15 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J..estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requestor: RAY OOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
K-adual value is l< ... ,.,.wn to be less than value given. L-actual value is known to be greater than value 9•---.,_ U-material was analyzed for but not detected. the number is the minimum quar•·· -•;on limit.
R-qc indicates U· a unusable. compound may or may not be present. resampling and reanalysis' ":essary for verification.
C-confirmed by f, _ 1.when no value is reported, see chlordane constituents 2.constituents or meta. . .. cs of technical chlordane
Sample ti'!i13 FY 1997 Project 97 -0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE9
Media: SOIL D Number. MY72
RESULTS UNITS
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
17000U
5100J
17000U
17000U
17000U
8400J
17000U
17000U
44000U
17000U
44000U
17000U
17000U
17000U
44000U
17000U
44000U
44000U
17000U
ANALYTE
PHENOL
BIS{2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS{2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS{2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE {HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5--TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
~ 17000U
-17000U -
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
-IIIIIW.eniaate:-?/9~0 -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
RESULTS UNITS ANALYTE
17000U
17000U
44000U
44000U
17000U
17000U
17000U
44000U
11000J
17000U
17000U
17000U
8400J
20000
17000U
17000U
17000U
14000J
17000U
17000U
17000U
17000U
17000U
17000U
17000U
24
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE {HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO{A)ANTHRACENE
CHRYSENE
BIS{2-ETHYLHEXYL) PHTHALA TE
D1-N-OCTYLPHTHALA TE
BENZO{B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO{A,H)ANTHRACENE
BENZO{GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
liiiil
Sample 12913 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE9
Media: SOIL
RESULTS UNITS
60000JN UG/KG
50000JN UG/KG
1000000J UG/KG
40000JN UG/KG
60000JN UG/KG
50000JN UG/KG
1 000000J UG/KG
D Number: MY72
ANALYTE
DIMETHYLNAPHTHALENE
TRIMETHYLNAPHTHALENE
ALKANES
METHYLDIBENZOTHROPHENE
DIMETHYLNAPHTHOTHIOPHENE
DIMETHYLPHENANTHRENE
15 UNIDENTIFIED COMPOUNDS
Org Contractor: MTS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
K-actual value is i----·...-n to be less than value given. L-actual value is known to be greater than value!?;. -U-material was analyzed for but not detected. the number is the minimum quafl•·· -•.,n limit.
R-qc indicates tt a unusable. compound may or may not be present. resampling and reanalysis ·essary for verification.
C-confirmed by Qo... .. .,_ 1.when no value is reported, see chlordane constituents 2.constituents or meta1.. __ .es of technical chlordane
C liiil
Sample 12914 FY 1997 Project: 97-0357
EXTRACT ABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE6
Media: SOIL D Number: MY73
RESULTS UNITS ANALYTE
430U UG/KG PHENOL
430U UG/KG BIS(2-CHLOROETHYL) ETHER
430U UG/KG 2-CHLOROPHENOL
430U UG/KG 1,3-DICHLOROBENZENE
430U UG/KG 1,4-DICHLOROBENZENE
430U UG/KG 1,2-DICHLOROBENZENE
430U UG/KG 2-METHYLPHENOL
430U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
430U UG/KG (3-AND/OR 4-)METHYLPHENOL
430U UG/KG N-NITROSODI-N-PROPYLAMINE
430U UG/KG HEXACHLOROETHANE
430U UG/KG NITROBENZENE
430U UG/KG ISOPHORONE
430U UG/KG 2-NITROPHENOL
430U UG/KG 2,4-DIMETHYLPHENOL
430U UG/KG BIS(2-CHLOROETHOXY)METHANE
430U UG/KG 2,4-DICHLOROPHENOL
430U UG/KG 1,2,4-TRICHLOROBENZENE
430U UG/KG NAPHTHALENE
430U UG/KG 4-CHLOROANILINE
430U UG/KG HEXACHLOROBUTADIENE
430U UG/KG 4-CHLOR0-3-METHYLPHENOL
430U UG/KG 2-METHYLNAPHTHALENE
430U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
430U UG/KG 2,4,6-TRICHLOROPHENOL
1100U UG/KG 2,4,5--TRICHLOROPHENOL
430U UG/KG 2-CHLORONAPHTHALENE
1100U UG/KG 2-NITROANILINE
430U UG/KG DIMETHYL PHTHALATE
430U UG/KG ACENAPHTHYLENE
430U UG/KG 2,6-DINITROTOLUENE
1100U UG/KG 3-NITROANILINE
430U UG/KG ACENAPHTHENE
1100U UG/KG 2,4-DINITROPHENOL
1100U UG/KG 4-NITROPHENOL
430U UG/KG DIBENZOFURAN
rF 430U UG/KG 2,4-0INITROTOLUENE -430U UG/KG DIETHYL PHTHALATE
\.r>,
Org Contractor: AA TS
RESULTS
430U
430U
1100U
1100U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
23
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evfdence of presence of material.
-Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
D1-N-OCTYLPHTHALA TE
BENZO(B ANO/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12914 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE6
Media: SOIL
RESULTS
500JN
2000J
1000J
UNITS
UG/KG
UG/KG
UG/KG
D Number: MY73
ANALYTE
CARBOXYLIC ACIDS
ALKANES
2 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
--Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1<----"Vn to be less than value given. L-actual value is known to be greater than value gi•·_-... _ U-material was analyzed for but not detected. the number is the minimum quan•,.-•ion limit.
R-qc indicates tt a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by g .. ____ . 1.when no value is reported, see chlordane constituents 2.constituents or meta .. _, .JS of technical chlordane
Sample 12914 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE6
Media: SOIL D Number: MY73
RESULTS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
430U
430U
430U
1100U
430U
1100U
1100U
430U eFJ 430U
-430U ~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor. AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
RESULTS UNITS ANALYTE
430U
430U
1100U
1100U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
23
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12914 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE6
Media: SOIL
RESULTS UNITS
500JN UG/KG
2000J UG/KG
1000J UG/KG
-
D Number: MY73
ANALYTE
CARBOXYLIC ACIDS
ALKANES
2 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--llllllllllllendl!ll!Jate: ""2,ss~o -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
K-actual value is~-··n to be less than value given. L-actual value is known to be greater than value gi•• U-material was analyzed for but not detected. the number is the minimum quant'" ··-.n limit.
R-qc indicates th, 1 unusable. compound may or may not be present. resampling and reanalysis i :ssary for verification.
C-confirmed by ge,,._.., _ _.. 1.when no value is reported, see chlordane constituents 2.constituents or metab1.. ..• ..;:s of technical chlordane
EJIIII.CT .... S S---E ..tllll.YSI---EPi11!91:G1dlllsEalla.THtiiil!IGA--·· -.a.,cti ... te:-19711116 -
Sample 12915 FY 1997 Project: 97-0357
EXTRACT ABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE10
Media: SOIL D Number: MY74
RESULTS UNITS
61000U UG/KG
61000U UG/KG
61 000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61 000U UG/KG
1 0000J UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61 000U UG/KG
61 000U UG/KG
61 000U UG/KG
61 000U UG/KG
61 000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
61 000U UG/KG
61000U UG/KG
61 0O0U UG/KG
150000U UG/KG
61000U UG/KG
150000U UG/KG
61000U UG/KG
61000U UG/KG
61000U UG/KG
150000U UG/KG
61000U UG/KG
150000U UG/KG
150000U UG/KG
61000U UG/KG
61000U UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALA TE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE tN° 61000U UG/KG DIETHYL PHTHALATE -~
Org Contractor: AA TS
RESULTS
61000U
61000U
150000U
150000U
61000U
61000U
61000U
150000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
24
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
E) -Sample 12915 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facilily: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE10
Media: SOIL
RESULTS
200000JN
500000J
90000JN
70000JN
900000JN
80000JN
5000000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY7 4
ANALYTE
METHYL(METHYLETHYL)BENZENE
ALKANES
PROPYL PHENOL
CARYOPHYLLENE
(PHENYL ETHYL) PHENOL
PINENE ISOMER
19 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
A iilil -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:15
Ending:
K-actual value is knnwn to be less than value given. L-actual value is known to be greater than value givP" U-materiat was analyzed for but not detected. the number is the minimum quantit-•;'ln limit.
R-qc indicates thf · unusable. compound may or may not be present. resampling and reanalysis i~ !Ssary for verification.
C-confirmed by QL . 1.when no value is reported, see chlordane constituents 2.constituents or metat, .,; of technical chlordane
-.. _.../
Sample 12915 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE10
Media: SOIL D Number: MY74
RESULTS UNITS
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
10000J
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
150000U
61000U
150000U
61000U
61000U
61000U
150000U
61000U
150000U
150000U
61000U
61000U
\;j:)" 61000U
~
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
IIJllend""3te:·•9S"'-'lo -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader. DOYLE
Beginning: 08124/9713:15
Ending:
RESULTS UNITS ANALYTE
61000U
61000U
150000U
150000U
61000U
61000U
61000U
150000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
61000U
24
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-adual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantrtation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis ls necessary for verification.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
E,..CTJIIIIIS S--E 41111YSI--~P,..GlcmlSE-TH~GA ----_,nd ... te:...,9Bllia> -
Sample 12915 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE10
Media: SOIL D Number: MY7 4
RESULTS UNITS ANALYTE
200000JN
500000J
90000JN
70000JN
900000JN
80000JN
5_D0QOO0J
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
METHYL(METHYLETHYL)BENZENE
ALKANES
PROPYL PHENOL
CARYOPHYLLENE
(PHENYL ETHYL) PHENOL
PINENE ISOMER
19 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is ~ ... -.• m to be less than value given. L-actual value is known to be greater than value gi,.-~ U-material was analyzed for but not detected. the number is the minimum quanti•-•:,,n limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification.
C-confirmed by QL . , 1.when no value is reported, see chlordane constituents 2.constituents or metat.. ___ . ..:s of technical chlordane
E ... CT.1111='> silllJLE --vsl!IJIII -Sample 12917 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE11
Media: SOIL D Number: MY75
RESULTS UNITS
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
1400U
570U
1400U
570U
570U
570U
1400U
570U
1400U
1400U
570U 0:::, 570U
<µ 570U
;....--
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5--TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
--- --- -
Amended Date: 02/0?/98 12:50
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
RESULTS UNITS ANALYTE
570U
570U
1400U
1400U
570U
570U
570U
1400U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
42
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL .
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resarnpling and reanalysis is necessary for verification.
C:-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12917 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE11
Media: SOIL
RESULTS UNITS
40000JN UG/KG
50000JN UG/KG
5000JN UG/KG
5000J UG/KG
1 0000JN UG/KG
20000JN UG/KG
200000J UG/KG
D Number. MY75 Org Contractor: AA TS
ANALYTE
DIHYDRODIHYDROXYPHENYLBENZOPYRANONE
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACIDS (2 ISOMEF .
METHYL(METHYLETHYL)PHENANTHRENE
ALKANES
TRIHYDROXYPHENYL BENZOPYRANONE
NORTRACHELOGENIN
23 UNIDENTIFIED COMPOUNDS
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is' ·,n to be less than value given. L-actual value is known to be greater than value 9; U-material was analyzed for but not detected. the number is the minimum quan•· ··,n limit.
R-qc indicates tt: 3 unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by gl.. . .-.,. 1.when no value is reported, see chlordane constituents 2.constituents or meta:L,,.. ..• es of technical chlordane
-
-Sample 12917 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE11
Media: SOIL D Number: MY75
RESULTS
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
. 570U
1400U
570U
1400U
570U
570U
570U
1400U
570U
1400U
1400U
570U
Q-:1 570U
~ 570U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
OIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
570U
570U
1400U
1400U
570U
570U
570U
1400U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
42
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
0I-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIOINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
D1-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--=P~Gl~SE
Sample 12917 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE11
Media: SOIL
RESULTS
40000JN
50000JN
5000JN
5000J
10000JN
20000JN
200000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY75 Org Contractor: AA TS
ANALYTE
DIHYDRODIHYDROXYPHENYLBENZOPYRANONE
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACIDS (2 ISOMEF .
METHYL(METHYLETHYL)PHENANTHRENE
ALKANES
TRIHYDROXYPHENYL BENZOPYRANONE
NORTRACHELOGENIN
23 UNIDENTIFIED COMPOUNOS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
;Aiiii ·-
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
K-actual value is kr"'wn to be less than value given. L-actual value is known to be greater than value gi•·--U-material was analyzed for but not detected. the number is the minimum quant .. ··,n limit.
R-qc indicates th; -1 unusable. compound may or may not be present. resampling and reanalysis i ·~ssary for verification.
C-confinned by 91. _ .· 1.when no value is reported, see chlordane constituents 2.constituents or metal..~ ... .:s of technical chlordane
-Sample 12918 FY 1997 Project: 97-0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE12
Media: SOIL D Number: MY76
RESULTS
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
8300J
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
12000J
28000U
28000U
71000U
28000U
71000U
28000U
28000U
28000U
71000U
28000U
71000U
71000U
28000U
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
· 28000U (:Fl 28000U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
~ ~
Org Contractor: AA TS
-Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
RESULTS UNITS ANALYTE
28000U
28000U
71000U
71000U
28000U
28000U
28000U
71000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
53
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
D1-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-l!IIS>A--IOf'allES11li81-lE:N, -IAA -~ -
Sample 12918 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facilily: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE12
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY76
RESULTS
700000JN
ANALYTE
METHYL(METHYLETHYL)BENZENE
PROPYLPHENOL
THYMOL
Org Contractor: AA TS
1000000JN
100000JN
500000JN
200000JN
200000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
METHYL(METHYLETHYL) PHENOL
HEXAHYDRODIMETHYL(METHYLETHYL)NAPHTHALENE (2 ISOM
(PHENYL ETHYL) PHENOL
5000000J 18 UNIDENTIFIED COMPOUNDS
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kn,.,,.,., to be less than value given. L-actual value is known to be greater than value give,.. U-material was analyzed for but not detected. the number is the minimum quantit?•=-., limit.
R-qc indicates that unusable. compound may or may not be present. resampling and reanalysis is isary for verification.
C-confirmed by gc,, ,.when no value is reported, see chlordane constituents 2.constituents or metabc... , of technical chlordane
-
Sample 12918 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF Case Number: 25655
Id/Station: RCSE12
Media: SOIL
RESULTS
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
8300J
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
12000J
28000U
28000U
71000U
28000U
71000U
28000U
28000U
28000U
71000U
28000U
71000U
71000U
28000U
,-,,,. 28000U
~ 28000U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY76
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5--TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
RESULTS UNITS ANALYTE
28000U
28000U
71000U
71000U
28000U
28000U
28000U
71000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
28000U
53
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYLPHENYLETHER
FLUORENE
4-NITROANIUNE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value given.• LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verffication.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
s.-_E Pl!!!!YSll!!!!!!l---1!1!11
Sample 12918 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE12
Media: SOIL
ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY76
METHYL(METHYLETHYL)BENZENE
PROPYLPHENOL
THYMOL
Org Contractor: AA TS
RESULTS
700000JN
1000000JN
100000JN
500000JN
200000JN
200000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
METHYL(METHYLETHYL) PHENOL
HEXAHYDRODIMETHYL(METHYLETHYL)NAPHTHALENE (2 ISOM
(PHENYL ETHYL) PHENOL
5000000J 18 UNIDENTIFIED COMPOUNDS
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1r-··vn to be less than value given. L-actual value is known to be greater than value gr·· -U-material was analyzed for but not detected. the number is the minimum quanP .,,..n limit.
R-qc indicates th 3 unusable. compound may or may not be present. resampling and reanalysis· ,ssary for verification.
C-confrrmed by g.._.____. 1.when no value is reported, see chlordane constituents 2.constituents or metal. .. __ .:!S of technical chlordane
Sample 1-2919 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE13
Media: SOIL O Number: MY77
RES UL TS UNITS
430U UGIKG
430U UGIKG
430U UGIKG
430U UG/KG
430U UG/KG
430U UG/KG
430U UG/KG
430U UG/KG
430U UGIKG
430U UGIKG
430U UGIKG
430U UGIKG
430U UG/KG
430U UG/KG
430U UGIKG
430U UGIKG
430U UG/KG
430U UG/KG
59J UGIKG
430U UG/KG
430U UGIKG
430U UG/KG
430U UG/KG
430U UG/KG
430U UG/KG
1100U UG/KG
430U UG/KG
1100U UG/KG
430U UG/KG
430U UGIKG
430U UG/KG
1100U UG/KG
82J UG/KG
1100U UG/KG
1100U UG/KG
54J UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
,-<1 430U UG/KG 2,4-OINITROTOLUENE
~ 430U UG/KG
~
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: John Mcconney
Requestor: RAY OOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:40
Ending:
----------
RES UL TS UNITS ANALYTE
430U
78J
1100U
1100U
430U
430U
430U
1100U
150J
430U
430U
430U
63J
80J
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
24
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
%
4-CHLOROPHENYLPHENYLETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
OI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12919 FY 1997 Project: 97-0357
EXTRACTABLESSCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE13
Media: SOIL D Number: MY77
RESULTS UNITS ANALYTE
430U UG/KG PHENOL
430U UG/KG BIS(2-CHLOROETHYL) ETHER
430U UG/KG 2-CHLOROPHENOL
430U UG/KG 1,3-DICHLOROBENZENE
430U UG/KG 1,4-DICHLOROBENZENE
430U UG/KG 1,2-DICHLOROBENZENE
430U UG/KG 2-METHYLPHENOL
430U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
430U UG/KG (3-AND/OR 4-)METHYLPHENOL
430U UG/KG N-NITROSODI-N-PROPYLAMINE
430U UG/KG HEXACHLOROETHANE
430U UG/KG NITROBENZENE
430U UG/KG ISOPHORONE
430U UG/KG 2-NITROPHENOL
430U UG/KG 2,4-DIMETHYLPHENOL
430U UG/KG BIS(2-CHLOROETHOXY)METHANE
430U UG/KG 2,4-DICHLOROPHENOL
430U UG/KG 1,2,4-TRICHLOROBENZENE
59J UG/KG NAPHTHALENE
430U UG/KG 4-CHLOROANILINE
430U UG/KG HEXACHLOROBUTADIENE
430U UG/KG 4-CHLORO-3-METHYLPHENOL
430U UG/KG 2-METHYLNAPHTHALENE
430U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
430U UG/KG 2,4,6--TRICHLOROPHENOL
1100U UG/KG 2,4,5--TRICHLOROPHENOL
430U UG/KG 2-CHLORONAPHTHALENE
1100U UG/KG 2-NITROANILINE
430U UG/KG DIMETHYL PHTHALATE
430U UG/KG ACENAPHTHYLENE
430U UG/KG 2,6--DINITROTOLUENE
1100U UG/KG 3-NITROANILINE
82J UG/KG ACENAPHTHENE
1100U UG/KG 2,4-DINITROPHENOL
1100U UG/KG 4-NITROPHENOL
54J UG/KG DIBENZOFURAN
tfl 430U UG/KG 2,4-DINITROTOLUENE
'0 430U UG/KG DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:40
Ending:
RESULTS UNITS ANALYTE
430U
78J
1100U
1100U
430U
430U
430U
1100U
150J
430U
430U
430U
63J
B0J
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
24
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYLPHENYLETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6--DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
------
E~T.• S :; ...... E ,..YSI--_ _,,l' ... GI~ SEll!l!ITHJ ; G!. m---------~ndililte: a.lt/98 IBII> -----------=------------·-::-
Sample 12919 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE13
Media: SOIL
RESULTS
500JN
300JN
800JN
D Number: MY77
ANALYTE
BENZALDEHYDE
METHYL(METHYLETHYL)BENZENE
BORNEOL
CARBOXYLIC ACIDS
Org Contractor: AA TS
1000JN
900JN
30000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
21 UNIDENTIFIED COMPOUNDS
-
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:40
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kr-·••n to be less than value given. L-actual value is known to be greater than value gi,__.-, -LI-material was analyzed for but not detected. the number is the minimum quanti•-··--n limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i: 1ssary for verification.
C-confirmed by gt.. ___ . 1.when no value is reported, see chlordane constituents 2.constituents or metab .. ,.Js of technical chlordane
Sample 12920 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE14
Media: SOIL D Number: MY78
RESULTS
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
7200U
2800U
7200U
2800U
2800U
2800U
7200U
2800U
7200U
7200U
2800U
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANIUNE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANIUNE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANIUNE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN o:i 2800U
~ 2800U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
Org Contractor: AA TS
RESULTS UNITS
2800U UG/KG
2800U UG/KG
7200U UG/KG
7200U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
7200U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
2800U UG/KG
42 %
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k,.-.. ., to be less than value given. L-actual value is known to be greater than value giv-· U-material was analyzed for but not detected. the number is the minimum quantit-•·~11 limit.
R-qc indicates ths unusable. compound may or may not be present. resampling and reanatysis i~ ssary for verification.
r.-confirmed by get. __ . ·1.when no value is reported, see chlordane constituents 2.constituents or metabi... __ $ of technical chlordane
-
Exaa;TAl.•-s;: S ..... E ~SI---=cr>AallGIOl!!!l!!!!ISE -------------H
Sample 12920 FY 1997 Project: 97-0357
EXTRACTABLE$ SCAN
F~cility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE14
Media: SOIL D Number: MY78
RESULTS
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2B00U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
7200U
2800U
7200U
2800U
2800U
2800U
7200U
· 2800U
7200U
7200U
2B00U
..-c-\ 2800U ~ 2800U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSOOI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METi-lYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
2800U
2800U
7200U
7200U
2800U
2800U
2800U
7200U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
2800U
42
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/OIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is 1<-··.,n to be less than value given. L-actual value is known to be greater than value gr··-U-material was analyzed for but not detected. the number is the minimum quanP ·•ion limit.
R-qc indicates th· 1 unusable. compound may or may not be present. resampling and reanalysis :!ssary for verification.
C-confirmed by g\... _ .. · 1.when no value is reported, see chlordane constituents 2.constituents or metai. . ..:s of technical chlordane
---~---
EMcTJl!lllls S--E -Ys1!11!11!' __ 1111111[1_ --EP~Glcn SF~ TH.GA-----:--------.;;i-te: -/97-6 -----·------~----' "
Sample 12920 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE14
Media: SOIL
ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY78 Org Contractor: AA TS
RESULTS
10000JN
300000J
30000J
UNITS
UG/KG
UG/KG
UG/KG
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
25 UNIDENTIFIED COMPOUNDS
ALKANES
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis ls necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12s,1 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE15
Media: SOIL D Number: MY79
RES UL TS UNITS
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
1300U
530U
1300U
530U
530U
530U
1300U
530U
1300U
1300U
530U
530U ~ 530U
\
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
530U
530U
1300U
1300U
530U
530U
530U
1300U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
38
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-N/TROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
.PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
----
E~CT ..... ~ ~--E Jll!!!BYSll!!III-----:liiiiia=P ... G~ S-E-TH-A---Sample 12921 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE15
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY79 Org Contractor: AA TS
3000JN UG/KG
400000J UG/KG
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
26 UNIDENTIFIED COMPOUNDS
20000J UG/KG ALKANES
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kri"wn to be less than value given. L-actual value is known to be greater than value giv'"-U-material was analyzed for but not detected. the number is the minimum quanti1-·'-.,n limit.
R-qc indicates th, 1 unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confirmed by Qt.,._ , 1.when no value is reported, see chlordane constituents 2.constituents or metat. .. __ -1,::; of technical chlordane
-
Sample 12921 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE15
Media: SOIL D Number: MY79
RESULTS UNITS ANALYTE
530U UG/KG PHENOL
530U UG/KG BIS(2-CHLOROETHYL) ETHER
530U UG/KG 2-CHLOROPHENOL
530U UG/KG 1,3-DICHLOROBENZENE
530U UG/KG 1,4-DICHLOROBENZENE
530U UG/KG 1,2-DICHLOROBENZENE
530U UG/KG 2-METHYLPHENOL
530U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
530U UG/KG (3-AND/OR 4-)METHYLPHENOL
530U UG/KG N-NITROSODI-N-PROPYLAMINE
530U UG/KG HEXACHLOROETHANE
530U UG/KG NITROBENZENE
530U UG/KG ISOPHORONE
530U UG/KG 2-NITROPHENOL
530U UG/KG 2,4-DIMETHYLPHENOL
530U UG/KG BIS(2-CHLOROETHOXY)METHANE
530U UG/KG 2,4-DICHLOROPHENOL
530U UG/KG 1,2,4-TRICHLOROBENZENE
530U UG/KG NAPHTHALENE
530U UG/KG 4-CHLOROANILINE
530U UG/KG HEXACHLOROBUTADIENE
530U UG/KG 4-CHLORO-3-METHYLPHENOL
530U UG/KG 2-METHYLNAPHTHALENE
530U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
530U UG/KG 2,4,6-TRICHLOROPHENOL
1300U UG/KG 2,4,5-TRICHLOROPHENOL
530U UG/KG 2-CHLORONAPHTHALENE
1300U UG/KG 2-NITROANILINE
530U UG/KG DIMETHYL PHTHALATE
530U UG/KG ACENAPHTHYLENE
530U UG/KG 2,6-DINITROTOLUENE
1300U UG/KG 3-NITROANILINE
530U UG/KG ACENAPHTHENE
1300U UG/KG 2,4-DINITROPHENOL
1300U UG/KG 4-NITROPHENOL
530U UG/KG DIBENZOFURAN
c;::i· 530U UG/KG 2,4-DINITROTOLUENE w 530U UG/KG DIETHYL PHTHALATE
~
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
RESULTS UNITS ANALYTE
530U
530U
1300U
1300U
530U
530U
530U
1300U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
530U
38
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
D1-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
D1-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be Jess than value given. L-actual value is known to be greater than value given. U-malerial was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constrtuents or metabolites of technical chlordane
-Sample 12921 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE15
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY79 Org Contractor: AA TS
3000JN UGIKG
400000J UGIKG
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
26 UNIDENTIFIED COMPOUNDS
20000J UG/KG ALKANES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
K-actual value is kr· · ·, to be less than value given. L-actual value is known to be greater than value givr U-material was analyzed for but not detected. the number is the minimum quantit· ·· , limit.
R-qc indicates tha unusable. compound may or may not be present. resampling and reanalysis is ;sary for verification.
<>confirmed by get,. ___ Lwhen no value is reported, see chlordane constituents 2.constituents or metabc,, ___ J of technical chlordane
-
---------.----
--PA aa1oralaES-HE~A -
Sample 12922 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE17
Media: SOIL D Number: MY81
RESULTS
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
860U
340U
860U
340U
340U
340U
860U
340U
860U
860U
340U o::i 340U
<.,_f:. 340U
__.Sl,
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
RESULTS UNITS ANALYTE
340U UG/KG
340U UG/KG
860U UG/KG
860U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
860U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
3 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k .. -···n to be less than value given. L-actual value is known to be greater than value gi'· U-material was analyzed for but not detected. the number is the minimum quant;• .. "'" limit.
R-qc indicates th< unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confirmed by gc.. . .. 1.when no value is reported, see chlordane constituents 2.constituents or metab ..... __ s of technical chlordane
-
Sample 12922 FY 1997 Project: 97-0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE17
Media: SOIL · D Number: MY81
RESULTS UNITS
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
340U
860U
340U
860U
340U
340U
340U
860U
340U
860U
860U
340U
340U
340U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
----------
Org Contractor: AA TS
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
RESULTS UNITS ANALYTE
340U UG/KG
340U UG/KG
860U UG/KG
860U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
860U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
340U UG/KG
3 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
K-actual value is kr-·•,n to be less than value given. L-actual value is known to be greater than value giv---U-rnaterial was analyzed for but not detected. the number is the minimum quanu•-~'.,n limit.
R-qc indicates th.: · unusable. compound may or may not be present. resampfing and reanalysis i: issary for verification.
C-confirmed by gc. ,_ .. --1.when no value is reported, see chlordane constituents 2.constituents or metat.,._ .. 1S of technical chlordane
Gi ...r:
Sample 12922 FY 1997 Project: 97 -0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE17
Media: SOIL
ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY81
RESULTS UNITS
4000J UG/KG 3 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
- -
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
--E~•C~A•~ ;aE A212v~,,-------
Sample 12923 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE18
Media: SOIL D Number: MY82
---------
Org Contractor: AA TS
-Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11 :20
Ending:
RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE
780U UG/KG PHENOL
780U UG/KG BIS(2-CHLOROETHYL) ETHER
780U UG/KG 2-CHLOROPHENOL
780U UG/KG 1,3--DICHLOROBENZENE
780U UG/KG 1,4-DICHLOROBENZENE
780U UG/KG 1,2-DICHLOROBENZENE
780U UG/KG 2-METHYLPHENOL
780U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
780U UG/KG (3--AND/OR 4-)METHYLPHENOL
780U UG/KG N-NITROSODI-N-PROPYLAMINE
780U UG/KG HEXACHLOROETHANE
780U UG/KG NITROBENZENE
780U UG/KG ISOPHORONE
780U UG/KG 2-NITROPHENOL
780U UG/KG 2,4-DIMETHYLPHENOL
780U UG/KG BIS(2-CHLOROETHOXY)METHANE
780U UG/KG 2,4-DICHLOROPHENOL
780U UG/KG 1,2,4-TRICHLOROBENZENE
780U UG/KG NAPHTHALENE
780U UG/KG 4-CHLOROANILINE
780U UG/KG HEXACHLOROBUTADIENE
780U UG/KG 4-CHLORO-3--METHYLPHENOL
780U UG/KG 2-METHYLNAPHTHALENE
780U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
780U UG/KG 2,4,6--TRICHLOROPHENOL
2000U UG/KG 2,4,5-TRICHLOROPHENOL
780U UG/KG 2-CHLORONAPHTHALENE
2000U UG/KG 2-NITROANILINE
780U UG/KG DIMETHYL PHTHALATE
780U UG/KG ACENAPHTHYLENE
780U UG/KG 2,6--DINITROTOLUENE
2000U UG/KG 3-NITROANILINE
780U UG/KG ACENAPHTHENE
2000U UG/KG 2,4-DINITROPHENOL
2000U UG/KG 4-NITROPHENOL
780U UG/KG DIBENZOFURAN
~ 780U UG/KG 2,4-DINITROTOLUENE
780U UG/KG DIETHYL PHTHALATE
~
780U
780U
2000U
2000U
780U
780U
780U
2000U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
58
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6--DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis_ is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
------------~. ----
-EX·T~~ ~-; ~~s,,----. -. --------.. _ .. ------------------------Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11 :20
Ending:
Sample 12923 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE18
Media: SOIL
RESULTS
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
780U
2000U
780U
2000U
780U
780U
780U
2000U
780U
2000U
2000U
780U
,-,'\ 780U S 780U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY82
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS UNITS
780U UG/KG
780U UG/KG
2000U UG/KG
2000U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
2000U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
780U UG/KG
58 %
A-average value. NA-not anafyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
8I$(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
--PAlllll,10.-,ES-HE-A -- -
Sample 12923 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE18
Media: SOIL
ANALYTE
CAMPHOR
ALKANES
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY82
RESULTS
300JN
20000J
20000J
UNITS
UG/KG
UG/KG
UG/KG 7 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11 :20
Ending:
K-actual value is i,---· .... n to be less than value given. L-actual value is known to be greater than value gi•·· -U-material was analyzed for but not detected. the number is the minimum quant;• .,..,n limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis i !ssary for verification.
C-confirmed by QL ___ .· 1.when no value is reported, see chlordane constituents 2.constituents or metaL~ _ . ..is of technical chlordane
-
-PA..a,10-,;E HE
Sample 12925 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE20
Media: SOIL D Number. MY87 Org Contractor: AA TS
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 16:20
Ending:
RESULTS UNITS ANALYTE RESULTS UNITS ANALYTE
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
1100U
440U
1100U
440U
440U
440U
1100U
440U
1100U
1100U
440U o-i 440U
,.J:. 440U v'\
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE.
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
440U
440U
1100U
1100U
440U
440U
440U
1100U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
26
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k ... --,,n to be less than value given. L-actual value is known to be greater than value giv~ -U-material was analyzed for but not detected. the number is the minimum quanu•~·· ... n limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i: 1ssary for verification.
C-confinned by gc... ..... · 1.when no value is reported, see chlordane constituents 2.constituents or metab.. __ ...;S of technical chlordane
-
Sample 12925 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE20
Media: SOIL D Number: MY87
RESULTS
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
440U
1100U
440U
1100U
440U
440U
440U
1100U
440U
1100U
1100U
440U
..-= 440U ..._,-440U
-C
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08125/97 16:20
Ending:
RESULTS UNITS ANALYTE
440U UG/KG
440U UG/KG
1100U UG/KG
1100U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
1100U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
440U UG/KG
26 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k,.. .... .,n to be less than value given. L-actual value is known to be greater than value giv· · U-material was analyzed for but not detected. the number is the minimum quanP ·· 'n limit.
R..qc indicates the unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confirmed by gc... ___ ~ 1.when no value is reported, see chlordane constituents 2.constituents or metat, .. _ _,s of technical chlordane
-
-Sample -, l925 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE20
Media: SOIL
RESULTS
600JN
5000J
2000JN
500JN
300JN
500JN
500JN
300JN
700JN
200JN
3000JN
6000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY87 Org Contractor: AA TS
ANALYTE
PINENE ISOMER
ALKANES
CARYOPHYLLENE
HEXAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
TETRAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
CARYOPHYLLENE OXIDE
COPAENE
DIMETHYL(METHYLETHYL)NAPHTHALENE
CARBOXYLIC ACIDS
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
CINNAMYL CINNAMATE
6 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 16:20
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of tec~nical chlordane
--Sample 12925 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE20
Media: SOIL D Number: MY87 Org Contractor: AA TS
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
40U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
30J UG/KG
14UJ UG/KG
26 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
- -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 16:20
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is ~r-··•r:i to be less than value given. L-actual value is known to be greater than value giv~~ U-material was analyzed for but not detected. the number is the minimum quantit;itirm limit.
R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis i' 'Ssary for verification.
C-confirmed hy gC.;. ____ 1.when no value is reported, see chlordane constituents 2.constituents or metal,._ .; of technical chlordane
-Sample 12932 FY 1997 Project: 97 -0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE21
Media: SOIL D Number. MY94
RESULTS
850U
850U
850U
850U
850U
85DU
850U
850U
94J
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
21D0U
850U
2100U
850U
850U
850U
2100U
850U
2100U
2100U
850U
850U
850U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6--TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
850U
850U
21D0U
2100U
850U
850U
850U
2100U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
61
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 15:35
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6--DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4--BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO·A-PYRENE
INDENO (1,2,3-cCD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actua1 value is known to be less than value given. L-actua1 value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
d}
~
-Sample 12932 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE21
Media: SOIL
RESULTS
1000JN
2000JN
3000JN
4000J
3000JN
40000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY94
ANALYTE
PINENE ISOMER
CARYOPHYLLENE
CARBOXYLIC ACID
ALKANES
CINNAMYL CINNAMATE
17 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -
._ -.icu.aate:..,/97-6 •
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 15:35
Ending:
K-actual value is kriflwn to be less than value given. L-actual value is known to be greater than value gi1"'ri. LI-material was analyzed for but not detected. the number is the minimum quan1:•-•ton limit.
R-qc indicates tt-'a unusable. compound may or may not be present. resampling and reanalysis -essary for verification.
C-confirmed by~ 1.when no value is reported, see chlordane constituents 2.constituents or met~. _.:s of technical chlordane
------....---- - ---... ------mnenmffl"tlate-'2.19ir-r=O
Sample 12932 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE21
Media: SOIL D Number: MY94
RESULTS UNITS ANALYTE
850U UG/KG PHENOL
850U UG/KG BIS(2-CHLOROETHYL) ETHER
850U UG/KG 2-CHLOROPHENOL
850U UG/KG 1,3-DICHLOROBENZENE
850U UG/KG 1,4-DICHLOROBENZENE
850U UG/KG 1,2-DICHLOROBENZENE
850U UG/KG 2-METHYLPHENOL
850U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
94J UG/KG (3-AND/OR 4-)METHYLPHENOL
850U UG/KG N-NITROSODI-N-PROPYLAMINE
850U UG/KG HEXACHLOROETHANE
850U UG/KG NITROBENZENE
850U UG/KG ISOPHORONE
850U UG/KG 2-NITROPHENOL
850U UG/KG 2,4-DIMETHYLPHENOL
850U UG/KG BIS(2-CHLOROETHOXY)METHANE
850U UG/KG 2,4-DICHLOROPHENOL
850U UG/KG 1,2,4-TRICHLOROBENZENE
850U UG/KG NAPHTHALENE
850U UG/KG 4-CHLOROANILINE
850U UG/KG HEXACHLOROBUTADIENE
850U UG/KG 4-CHLORO-3-METHYLPHENOL
850U UG/KG 2-METHYLNAPHTHALENE
850U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
850U UG/KG 2,4,6-TRICHLOROPHENOL
2100U UG/KG 2,4,5-TRICHLOROPHENOL
850U UG/KG 2-CHLORONAPHTHALENE
2100U UG/KG 2-NITROANILINE
850U UG/KG DIMETHYL PHTHALATE
850U UG/KG ACENAPHTHYLENE
850U UG/KG 2,6-DINITROTOLUENE
2100U UG/KG 3-NITROANILINE
850U UG/KG ACENAPHTHENE
2100U UG/KG 2,4-DINITROPHENOL
2100U UG/KG 4-NITROPHENOL
850U UG/KG DIBENZOFURAN
(JJ 850U UG/KG 2,4-DINITROTOLUENE
'-1\_ 850U UG/KG DIETHYL PHTHALATE -
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 15:35
Ending:
RESULTS UNITS ANALYTE
850U
850U
2100U
2100U
850U
850U
850U
2100U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
850U
61
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of t~~p!cal chlordane
-Sample 12932 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE21
Media: SOIL
RESULTS UNITS
1 000JN UG/KG
2000JN UG/KG
3000JN UG/KG
4000J UG/KG
3000JN UG/KG
40000J UG/KG
D Number: MY94
ANALYTE
PINENE ISOMER
CARYOPHYLLENE
CARBOXYLIC ACID
ALKANES
CINNAMYL CINNAMATE
17 UNIDENTIFIED COMPOUNDS
Org Contractor: MTS
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 15:35
Ending:
K-actual value is i--· -·n to be less than value given. L-actual value is known to be greater than value gr· U-material was analyzed for but not detected. the number is the minimum quanf" ··._n limit.
R-qc indicates th:' 1 unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confirmed by gc.. ____ .· 1.when no value is reported, see chlordane constituents 2.constituents or metab... ... .:s of technical chlordane
-
-Sample 12933 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE22
Media: SOIL D Number: MY95
RESULTS
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
3200U
1300U
3200U
1300U
1300U
1300U
3200U
1300U
3200U
3200U
~ 1300U
V" 1300U ~ 1300U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 17:10
Ending:
Org Contractor: AA TS
RESULTS UNITS
1300U UG/KG
1300U UG/KG
3200U UG/KG
3200U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
3200U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UGIKG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
1300U UG/KG
74 %
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--PA 111111,10,_ES-HE-A --Sample 12933 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number. 25655
Id/Station: RCSE22
Media: SOIL
RESULTS
2000JN
600JN
800JN
700JN
4000JN
10000J
50000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY95 Org Contractor: AA TS
ANALYTE
CARYOPHYLLENE
HEXAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
TETRAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
DIMETHYL (METHYL ETHYL) NAPHTHALENE
CARBOXYLIC ACIDS
ALKANES
13 UNIDENTIFIED COMPOUNDS
-A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 17:10
Ending:
K-actual value is kn,.,···t1 to be less than value given. L-actual value is known to be greater than value give-" U-material was analyzed for but not detected. the number is the minimum quantit~:,:--: limit.
R-qc indicates thal unusable. compound may or may not be present. resampling and reanalysis is ,sary for verification.
C-confirmed by gc. ~ ... , .when no value is reported, see chlordane constituents 2.constituents or metab1., . of technical chlordane
-
Sample 129.33 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE22
Media: SOIL D Number: MY95
RESULTS UNITS
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
3200U
1300U
3200U
1300U
1300U
1300U
3200U
1300U
3200U
3200U
-1300U
V" 1300U
~oou
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 17:10
Ending:
RESULTS UNITS ANALYTE
1300U
1300U
3200U
3200U
1300U
1300U
1300U
3200U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
1300U
74
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYLPHENYLETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed .. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems_: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12933 FY 1997 Project: 97-0357
· MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE22
Media: SOIL
RESULTS
2000JN
600JN
B00JN
700JN
4000JN
10000J
50000J
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY95 Org Contractor: AA TS
ANALYTE
CARYOPHYLLENE
HEXAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
TETRAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
DIMETHYL (METHYL ETHYL) NAPHTHALENE
CARBOXYLIC ACIDS
ALKANES
13 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 17: 10
Ending:
K-actual value is I< . ., to be less than value given. L-actual value is known to be greater than value gi--LI-material was analyzed for but not detected. the number is the minimum quanti' , limit.
R-qc indicates the_ . unusable. compound may or may not be present. resampling and reanalysis ir. ssary for verification. .
C-confrrmed by gc.____ 1.when no value is reported, see chlordane constituents 2.constituents or metab1., .. ~..:s of technical chlordane
E .. CT .. S ~LE --ysll!JIII -Sample 12949 FY 1997 Project: 97 -0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE1 MD Number: MY31
Media: SOIL D Number: MY65
RESULTS UNITS ANALYTE
370U UG/KG PHENOL
370U UG/KG BIS(2-CHLOROETHYL) ETHER
370U UG/KG 2-CHLOROPHENOL
370U UG/KG 1,3-DICHLOROBENZENE
370U UG/KG 1,4-DICHLOROBENZENE
370U UG/KG 1,2-DICHLOROBENZENE
370U UG/KG 2-METHYLPHENOL
370U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
370U UG/KG (3-AND/OR 4-)METHYLPHENOL
370U UG/KG N-NITROSODI-N-PROPYLAMINE
370U UG/KG HEXACHLOROETHANE
370U UG/KG NITROBENZENE
370U UG/KG ISOPHORONE
370U UG/KG 2-NITROPHENOL
370U UG/KG 2.4-DIMETHYLPHENOL
370U UG/KG BIS(2-CHLOROETHOXY)METHANE
370U UG/KG 2.4-DICHLOROPHENOL
370U UG/KG 1,2.4-TRICHLOROBENZENE
370U UG/KG NAPHTHALENE
370U UG/KG 4-CHLOROANILINE
370U UG/KG HEXACHLOROBUTADIENE
370U UG/KG 4-CHLORO-3-METHYLPHENOL
370U UG/KG 2-METHYLNAPHTHALENE
370U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
370U UG/KG 2.4.6-TRICHLOROPHENOL
930U UG/KG 2,4,5-TRICHLOROPHENOL
370U UG/KG 2-CHLORONAPHTHALENE
930U UG/KG 2-NITROANILINE
370U .UG/KG DIMETHYL PHTHALATE
370U UG/KG ACENAPHTHYLENE
370U UG/KG 2,6-DINITROTOLUENE
930U UG/KG 3-NITROANILINE
370U UG/KG ACENAPHTHENE
930U UG/KG 2,4-DINITROPHENOL
930U UG/KG 4-NITROPHENOL
370U UG/KG DIBENZOFURAN
Gl 370U UG/KG 2.4-DINITROTOLUENE
~ 370U UG/KG DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
370U
370U
930U
930U
370U
370U
370U
930U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
11
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE ·
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BI5(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12949 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY31 Id/Station: RCSE1
Media: SOIL
RESULTS UNITS
700JN UG/KG
90JN UG/KG
200JN UG/KG
D Number: MY65
ANALYTE
PINENE ISOMER
BENZOIC ACID
CARBOXYLIC ACIDS
lnorg Contractor: ARI
Org Contractor: AA TS
100JN UG/KG
1000JN UG/KG
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
CINNAMYL CINNAMATE
100JN UG/KG COPAENE
3000J UG/KG 4 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
- -
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
K-actual value is lcnnwn to be less than value given. L-actual value is known to be greater than value p;. ... .,_ U-material was analyzed for but not detected. the number is the minimum quar•·· -•;on limit.
R-qc indicates U '.a unusable. compound may or may not be present. resampling and reanalysis :essary for verification.
C-confirmed by h 1.when no value is reported, see chlordane constituents 2.constituents or meto, -~s of technical chlordane
C -Sample ··,:,~49 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE1 MD Number: MY31
Media: SOIL D Number: MY65
RESULTS UNITS
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
370U
930U
370U
930U
370U
370U
370U
930U
370U
930U
930U
370U
370U
370U
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1.4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2.4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2.4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2.4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2.4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08124197 08:05
Ending:
RESULTS UNITS ANALYTE
370U UGIKG
370U UG/KG
930U UG/KG
930U UG/KG
370U UG/KG
370U UGIKG
370U UGIKG
930U UG/KG
370U UG/KG
370U UGIKG
370U UG/KG
370U UG/KG
370U UGIKG
370U UGIKG
370U UG/KG
370U UGIKG
370U UG/KG
370U UGIKG
370U UGIKG
370U UG/KG
370U UG/KG L 370U UG/KG
370U UGIKG
370U UG/KG
370U UG/KG
11 %
4-CHLOROPHENYLPHENYLETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12949 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY31 Id/Station: RCSE1
Media: SOIL
RESULTS UNITS
700JN UG/KG
90JN UG/KG
200JN UG/KG
D Number: MY65
ANALYTE
PINENE ISOMER
BENZOIC ACID
CARBOXYLIC ACIDS
lnorg Contractor: ARI
Org Contractor: AA TS
100JN UG/KG
1 00OJN UG/KG
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
CINNAMYL CINNAMATE
100JN UG/KG COPAENE
3000J UG/KG 4 UNIDENTIFIED COMPOUNDS
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1<--,,n to be Jess than value given. L-actual value is known to be greater than value gr·· U-material was analyzed for but not detected. the number is the minimum quanf' ..... n limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification.
C-confinned by Qt... ____ 1.when no value is reported, see chlordane constituents 2.constituents or metab ... __ ~s of technical chlordane
-Sample 12~,o FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY32 Id/Station: RCSE2
Media: SOIL
RESULTS UNITS
380[U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
960U
380U
960U
380U
380U
380U
960U
380U
960U
960U
380U
380U
380U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY66
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
380U
380U
960U
960U
380U
380U
380U
960U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
3B0U
380U
380U
380U
14
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANIUNE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
K-actual value is known to be less than value given. L-actual Value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
EX~TA-S ... E A_.,SI~ -
CP
Sample 12950 FY 1997 Project: 97..()357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY32 Id/Station: RCSE2
Media: SOIL
RESULTS
300JN
3000J
UNITS
UG/KG
UG/KG
D Number: MY66
ANALYTE
CARBOXYLIC ACIDS
4 UNIDENTIFIED COMPOUNDS
~
lnorg Contractor: ARI
Org Contractor: AA TS
-Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kri .... ...,n to be less than value given. L-actual value is known to be greater than value giVP" LI-material was analyzed for but not detected. the number is the minimum quantif:,,tion limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis if 1ssary for verification.
C-confirmed by gl. 1.when no value is reported, see chlordane constituents 2.constituents or metaL .s of technical chlordane
-
--EPP-IEG1Rs~TH-GA---
Sample 12950 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE2 MD Number: MY32
Media: SOIL D Number: MY66
RESULTS UNITS
380[U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
380U
960U
380U
960U
380U
380U
380U
960U
380U
960U
960U
380U
380U
380U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANIUNE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
RESULTS UNITS ANALYTE
380U UG/KG
380U UG/KG
960U UG/KG
960U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
960U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
380U UG/KG
14 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZ¥LBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents-or.metabolites of technical chlordane
-Sample 12950 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY32 Id/Station: RCSE2
Media: SOIL
RESULTS UNITS
300JN UG/KG
3000J UG/KG
D Number: MY66
ANALYTE
CARBOXYLIC ACIDS
4 UNIDENTIFIED COMPOUNDS
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
K-actual value is,., ·11 to be less than value given. L-actual value is known to be·greater than value gi· U-material was analyzed for but not detected. the number is the minimum quanr· 'fl limit.
R-qc indicates th; J unusable. compound may or may not be present. resampling and reanalysis i !Ssary for verification.
C-confinned by gt., . ...,;· 1.when no value is reported, see chlordane constituents 2.constituents or metabt,,.,c,s of technical chlordane
-Sample 12951 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33 Id/Station: RSCE3
Media: SOIL
RESULTS
390U
390U
390U
390U
390U
.390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
390U
980U
390U
980U
390U
390U
390U
980U
390U
980U
980U
390U
390U
390U
UNITS
UGIKG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UG/KG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
D Number: MY67
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24197 08:50
Ending:
RESULTS UNITS ANALYTE
390U UG/KG
390U UG/KG
980U UG/KG
980U UGIKG
390U UG/KG
390U UG/KG
390U UG/KG
980U UGIKG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UGIKG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UGIKG
390U UGIKG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UGIKG
390U UG/KG
15 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is llecessary for verification.
C-confirrned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12951 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33 Id/Station: RSCE3
Media: SOIL D Number: MY67
ANALYTE
PINENE ISOMER
LIMONENE
BENZOIC ACID
BORNEOL
CARYOPHYLLENE
CARBOXYLIC ACID
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
1000JN
200JN
200JN
600JN
700JN
700JN
600JN
4000JN
3000J
4000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
CINNAMYL CINNAMATE
200JN
20000J
ALKANES
NORTRACHELOGENIN
COPAENE
6 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
K-actual value is kri"".in to be less than value given. L-actual value is known to be greater than value givr-U-material was analyzed for but not detected. the number is the minimum quanu,-·-.,,., limit.
R--qc indicates the unusable. compound may or may not be present. resampling and reanalysis i: ,ssary for verification.
C-confirmed by gc.. _ _ 1.when no value is reported, see chlordane constituents 2.constituents or metab'"---~.:> of technical chlordane
-Sample 12951 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RSCE3 MD Number: MY33
Media: SOIL D Number: MY67
RESULTS UNITS ANALYTE
390U UG/KG PHENOL
390U UG/KG BIS(2-CHLOROETHYL) ETHER
390U UG/KG 2-CHLOROPHENOL
390U UG/KG 1,3-DICHLOROBENZENE
390U UG/KG 1,4-DICHLOROBENZENE
390U UG/KG 1,2-DICHLOROBENZENE
390U UG/KG 2-METHYLPHENOL
390U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
390U UG/KG (3-AND/OR 4-)METHYLPHENOL
390U UG/KG N-NITROSODI-N-PROPYLAMINE
390U UG/KG HEXACHLOROETHANE
390U UG/KG NITROBENZENE
390U UG/KG ISOPHORONE
390U UG/KG 2-NITROPHENOL
390U UG/KG 2,4-DIMETHYLPHENOL
390U UG/KG BIS(2-CHLOROETHOXY)METHANE
390U UG/KG 2,4-DICHLOROPHENOL
390U UG/KG 1,2,4-TRICHLOROBENZENE
390U UG/KG NAPHTHALENE
390U UG/KG 4-CHLOROANILINE
390U UG/KG HEXACHLOROBUTADIENE
390U UG/KG 4-CHLORO-3-METHYLPHENOL
390U UG/KG 2-METHYLNAPHTHALENE
390U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
390U UG/KG 2,4,6-TRICHLOROPHENOL
980U UG/KG 2,4,5-TRICHLOROPHENOL
390U UG/KG 2-CHLORONAPHTHALENE
980U UG/KG 2-NITROANILINE
390U UG/KG DIMETHYL PHTHALATE
390U UG/KG ACENAPHTHYLENE
390U UG/KG 2,6-DINITROTOLUENE
980U UG/KG 3-NITROANILINE
390U UG/KG ACENAPHTHENE
980U UG/KG 2,4-DINITROPHENOL
980U UG/KG 4-NITROPHENOL
390U UG/KG DIBENZOFURAN
G3 390U UG/KG 2,4-DINITROTOLUENE
~ 390U UG/KG DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
RESULTS UNITS ANALYTE
390U UG/KG
390U UG/KG
980U UG/KG
980U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
980U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
390U UG/KG
15 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not anatyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanatysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12951 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
-=P~Gl~SE H
Id/Station: RSCE3
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
MD Numbe~ MY33
D Number: MY67
lnorg Contractor: ARI
Org Contractor: AA TS
RES UL TS UNITS
1000JN UG/KG
200JN UG/KG
200JN UG/KG
600JN UG/KG
700JN UG/KG
700JN UG/KG
600JN UG/KG
4000JN UG/KG
3000J UG/KG
4000JN UG/KG
200JN UG/KG
20000J UG/KG
ANALYTE
PINENE ISOMER
LIMONENE
BENZOIC ACID
BORNEOL
CARYOPHYLLENE
CARBOXYLIC ACID
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
CINNAMYL CINNAMATE
ALKANES
NORTRACHELOGENIN
COPAENE
6 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J...estimated value. N-presumptive evidence of presence of material.
A-- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
K-adual value is kn"''"'" to be less than value given. L-actual value is known to be greater than value givi:>:-U-material was analyzed for but not detected. the number is the minimum quantit.--··~11 limit.
R-qc indicates th.; unusable. compound may or may not be present. resampling and reanalysis is ssary for verification.
C-confinned by gc.. ~ 1 when no value is reported, see chlordane constituents 2.constituents or metab1. _ ., of technical chlordane
-Sample 1l~52 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE4 MD Number: MY34
Media: SOIL D Number: MY68
RESULTS
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
1100U
430U
1100U
430U
430U
430U
1100U
430U
1100U
1100U
430U
430U
430U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
8I$(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5--TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
OIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS
430U
430U
1100U
1100U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
23
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r,.confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12952 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
~P~Gl~SE H
Id/Station: RCSE4
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34
D Number: MY68
lnorg Contractor: ARI
Org Contractor: AA TS
RESULTS UNITS
4000JN UG/KG
2000JN UG/KG
4000JN UG/KG
500JN UG/KG
700JN UG/KG
1000J UG/KG
6000JN UG/KG
30000J UG/KG
ANALYTE
PINENE ISOMER
BORNEOL
CAMPHENE
CARBOXYLIC ACID
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
ALKANES
NORTRACHELOGENIN
14 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
A---ia.icticllllte: -/97 --
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
K-actual value is 1<---·.,,n to be less than value given. L-actual value is known to be greater than value gi•·--U-material was analyzed for but not detected. the number is the minimum quant;•-•;on limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis ; ?ssary for verification.
C-confirmed by QL~--. 1.when no value is reported, see chlordane constituents 2.constituents or me_tat. __ . .:s of technical chlordane
-Sample 12952 FY 1997 Project: 97-0357
EXTRACTABLE$ SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE4 MD Number: MY34
Media: SOIL D Number: MY68
RESULTS UNITS ANALYTE
430U UG/KG PHENOL
430U UG/KG BIS(2-CHLOROETHYL) ETHER
430U UG/KG 2-CHLOROPHENOL
430U UG/KG 1,3-DICHLOROBENZENE
430U UG/KG 1,4-DICHLOROBENZENE
430U UG/KG 1,2-DICHLOROBENZENE
430U UG/KG 2-METHYLPHENOL
430U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
430U UG/KG (3-AND/OR 4-)METHYLPHENOL
430U UG/KG N-NITROSODI-N-PROPYLAMINE
430U UG/KG HEXACHLOROETHANE
430U UG/KG NITROBENZENE
430U UG/KG ISOPHORONE
430U UG/KG 2-NITROPHENOL
430U UG/KG 2,4-DIMETHYLPHENOL
430U UG/KG BIS(2-CHLOROETHOXY)METHANE
430U UG/KG 2,4-DICHLOROPHENOL
430U UG/KG 1,2,4-TRICHLOROBENZENE
430U UG/KG NAPHTHALENE
430U UG/KG 4-CHLOROANILINE
430U UG/KG HEXACHLOROBUTADIENE
430U UG/KG 4-CHLORO-3-METHYLPHENOL
430U UG/KG 2-METHYLNAPHTHALENE
430U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
430U UG/KG 2,4,6-TRICHLOROPHENOL
1100U UG/KG 2,4,5-TRICHLOROPHENOL
430U UG/KG 2-CHLORONAPHTHALENE
1100U UG/KG 2-NITROANILINE
430U UG/KG DIMETHYL PHTHALATE
430U UG/KG ACENAPHTHYLENE
430U UG/KG 2,6-DINITROTOLUENE
1100U UG/KG 3-NITROANILINE
430U UG/KG ACENAPHTHENE
1100U UG/KG 2,4-DINITROPHENOL
1100U UG/KG 4-NITROPHENOL
c:;:;i 430U UG/KG DIBENZOFURAN
430U UG/KG 2,4-DINITROTOLUENE ~ 430U UG/KG DIETHYL PHTHALATE
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
RESULTS UNITS ANALYTE
430U
430U
1100U
1100U
430U
430U
430U
1100U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
430U
23
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C--confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--PA lilll:;10..,ES-HE~A -- -
Sample 12952 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34 Id/Station: RCSE4
Media: SOIL
RESULTS UNITS
4000JN UG/KG
2000JN UG/KG
4000JN UG/KG
500JN UG/KG
D Number: MY68
ANALYTE
PINENE ISOMER
BORNEOL
CAMPHENE
CARBOXYLJC ACID
lnorg Contractor: ARI
Org Contractor: AA TS
700JN UG/KG
1000J UG/KG
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
ALKANES
6000JN UG/KG NORTRACHELOGENIN
30000J UG/KG 14 UNIDENTIFIED COMPOUNDS
Produced by: Denise Goddard
Requestor. RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is•· "" to be less than value given. L-actual value is known to be greater than value gi-U-material was anatyzed for but not detected. the number is the minimum quan•'· .. "" limit.
R-qc indicates tt.' a unusable. compound may or may not be present. resampling and reanalysis · !ssary for verification.
C-confirmed by 91......... 1.when no value is reported, see chlordane constituents 2.constituents or metat. ....... ~s of technical chlordane
t:X-IA-:SA-=A .... :Sl:S---PA ~IU._t::S-Ht:'allllA ---.,_,t,o-e: ,lllill, ,.
Sample 12953 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE16 MD Number: MY35
Media: SOIL D Number: MYB0
RESULTS UNITS ANALYTE
570U UG/KG PHENOL
570U UG/KG BIS(2-CHLOROETHYL} ETHER
570U UG/KG 2-CHLOROPHENOL
570U UG/KG 1,3-DICHLOROBENZENE
570U UG/KG 1,4-DICHLOROBENZENE
570U UG/KG 1,2-DICHLOROBENZENE
570U UG/KG 2-METHYLPHENOL
570U UG/KG BIS(2-CHLOROISOPROPYL} ETHER
570U UG/KG (3-AND/OR 4-)METHYLPHENOL
570U UG/KG N-NITROSODI-N-PROPYLAMINE
570U UG/KG HEXACHLOROETHANE
570U UG/KG NITROBENZENE
570U UG/KG ISOPHORONE
570U UG/KG 2-NITROPHENOL
570U UG/KG 2,4-DIMETHYLPHENOL
570U UG/KG BIS(2-CHLOROETHOXY)METHANE
570U UG/KG 2,4-DICHLOROPHENOL
570U UG/KG 1,2,4-TRICHLOROBENZENE
570U UG/KG NAPHTHALENE
570U UG/KG 4-CHLOROANIUNE
570U UG/KG HEXACHLOROBUTADIENE
570U UG/KG 4-CHLORO-3-METHYLPHENOL
570U UG/KG 2-METHYLNAPHTHALENE
570U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP}
570U UG/KG 2,4,6-TRICHLOROPHENOL
1400U UG/KG 2,4,5-TRICHLOROPHENOL
570U UG/KG 2-CHLORONAPHTHALENE
1400U UG/KG 2-NITROANILINE
570U UG/KG DIMETHYL PHTHALATE
570U UG/KG ACENAPHTHYLENE
570U. UG/KG 2,6-DINITROTOLUENE
1400U UG/KG 3-NITROANILINE
570U UG/KG ACENAPHTHENE
1400U UG/KG 2,4-DINITROPHENOL
1400U UG/KG 4-NITROPHENOL
570U UG/KG DIBENZOFURAN
570U UG/KG 2,4-DINITROTOLUENE
O:'.l 570U UG/KG DIETHYL PHTHALATE
~
I norg Contractor: AR I .
Org Contractor: AA TS
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
RESULTS UNITS ANALYTE
570U UG/KG
570U UG/KG
1400U UG/KG
1400U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
1400U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
570U UG/KG
42 %
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB}
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A}ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL} PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K}FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD} PYRENE
DIBENZO(A,H}ANTHRACENE
BENZO(GHl}PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantit.lti,m limit.
R-qc indicates the: unusable. compound may or may not be present. resampling and reanalysis 1s· ssary for verification.
C-confirmed by gc.. ,.when no value is reported, see chlordane constituents 2.constituents or metab , of technical chlordane
-
-------EXTRACTAB! -'.SAMPLE ANAl:YSIS--
Sample 12953 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE16 MD Number: MY35
Media: SOIL D Number: MYB0
RESULTS UNITS ANALYTE
570U UG/KG PHENOL
570U UG/KG BIS(2-CHLOROETHYL) ETHER
570U UG/KG 2-CHLOROPHENOL
570U UG/KG 1,3-DICHLOROBENZENE
570U UG/KG 1,4-DICHLOROBENZENE
570U UG/KG 1,2-DICHLOROBENZENE
570U UG/KG 2-METHYLPHENOL
570U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
570U UG/KG (3--AND/OR 4-)METHYLPHENOL
570U UG/KG N-NITROSODI-N-PROPYLAMINE
570U UG/KG HEXACHLOROETHANE
570U UG/KG NITROBENZENE
570U UG/KG ISOPHORONE
570U UG/KG 2-NITROPHENOL
570U UG/KG 2,4-DIMETHYLPHENOL
570U UG/KG BIS(2-CHLOROETHOXY)METHANE
570U UG/KG 2,4-DICHLOROPHENOL
570U UG/KG 1,2,4-TRICHLOROBENZENE
570U UG/KG NAPHTHALENE
570U UG/KG 4-CHLOROANILINE
570U UG/KG HEXACHLOROBUTADIENE
570U UG/KG 4-CHLORO-3--METHYLPHENOL
570U UG/KG 2-METHYLNAPHTHALENE
570U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
570U UG/KG 2,4,6-TRICHLOROPHENOL
1400U UG/KG 2,4,5-TRICHLOROPHENOL
570U UG/KG 2-CHLORONAPHTHALENE
1400U UG/KG 2-NITROANILINE
570U UG/KG DIMETHYL PHTHALATE
570U UG/KG ACENAPHTHYLENE
570U UG/KG 2,6-DINITROTOLUENE
1400U UG/KG 3-NITROANILINE
570U UG/KG ACENAPHTHENE
1400U UG/KG 2,4-DINITROPHENOL
1400U UG/KG 4-NITROPHENOL
570U UG/KG DIBENZOFURAN
~ 570U UG/KG 2,4-DINITROTOLUENE
570U UG/KG DIETHYL PHTHALATE
~
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
RESULTS UNITS ANALYTE
570U
570U
1400U
1400U
570U
570U
570U
1400U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
570U
42
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE .
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
D1-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3--CD) PYRENE
DIBENZO(AH)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~ ~
-Sample 12953 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE16
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY35
D Number: MYB0
lnorg Contractor: ARI
Org Contractor: AA TS
2000JN UG/KG
4000J UG/KG
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
ALKANES
B0000J UG/KG 27 UNIDENTIFIED COMPOUNDS
~
- -
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
Sample 12956 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE19 MD Number: MY38
Media: SOIL D Number: MY85
RESULTS UNITS ANALYTE
1600U UG/KG PHENOL
1600U UG/KG BIS(2-CHLOROETHYL) ETHER
1600U UG/KG 2-CHLOROPHENOL
1600U UG/KG 1,3-0ICHLOROBENZENE
1600U UG/KG 1,4-0ICHLOROBENZENE
1600U UG/KG 1,2-0ICHLOROBENZENE
1600U UG/KG 2-METHYLPHENOL
1600U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
1600U UG/KG (3-AND/OR 4-)METHYLPHENOL
1600U UG/KG N-NITROSODI-N-PROPYLAMINE
1600U UG/KG HEXACHLOROETHANE
1600U UG/KG NITROBENZENE
1600U UG/KG ISOPHORONE
1600U UG/KG 2-NITROPHENOL
1600U UG/KG 2,4-DIMETHYLPHENOL
1600U UG/KG BIS(2-CHLOROETHOXY)METHANE
1600U UG/KG 2,4-DICHLOROPHENOL
1600U UG/KG 1,2,4-TRICHLOROBENZENE
1600U UG/KG NAPHTHALENE
1600U UG/KG 4-CHLOROANILINE
1600U UG/KG HEXACHLOROBUTADIENE
1600U UG/KG 4-CHLOR0-3-METHYLPHENOL
1600U UG/KG 2-METHYLNAPHTHALENE
1600U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
1600U UG/KG 2,4,6-TRICHLOROPHENOL
4000U UG/KG 2,4,5-TRICHLOROPHENOL
1600U UG/KG 2-CHLORONAPHTHALENE
4000U UG/KG 2-NITROANILINE
1600U UG/KG DIMETHYL PHTHALATE
1600U UG/KG ACENAPHTHYLENE
1600U UG/KG 2,6-DINITROTOLUENE
4000U UG/KG 3-NITROANILINE
1600U UG/KG ACENAPHTHENE
4000U UG/KG 2,4-DINITROPHENOL
4000U UG/KG 4-NITROPHENOL
1600U UG/KG DIBENZOFURAN
~ 1600U UG/KG 2,4-DINITROTOLUENE
1600U UG/KG DIETHYL PHTHALATE
.c--
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
RESULTS UNITS ANALYTE
1600U
1600U
4000U
4000U
1600U
1600U
1600U
4000U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
79
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is knnwn to be less than value given. L-actual value is known to be greater than value giv,,..,_ U-material was analyzed for but not detected. the number is the minimum quantit ... +ion limit.
R-qc indicates th: l unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification.
C-confirmed by g., 1.when no value is reported, see chlordane constituents 2.constituents or meta... .s of technical chlordane
-Sample 12956 FY 1997 Project: 97 -0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE19 MD Number: MY38
Media: SOIL D Number:.MY85
RESULTS
3000JN
20000J
400000J
UNITS
UG/KG
UG/KG
UG/KG
ANALYTE
METHYL(METHYLETHYWPHENANTHRENE
ALKANES
28 UNIDENTIFIED COMPOUNDS
lnorg Contractor: ARI
--Org·Contractcir: MTS
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actuar value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
-Sample 12956 FY 1997
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL
Program: NSF
Project: 97--0357
CASTLE HAYNE. NC
Case Number: 25655
MD Number: MY38 Id/Station: RCSE19
Media: SOIL
RESULTS
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
1600U
4000U
1600U
4000U
1600U
1600U
1600U
4000U
1600U
4000U
4000U
1600U
1600U
1600U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
D Number: MY85
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2.4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2.4-DINITROTOLUENE
DIETHYL PHTHALATE
lnorg Contractor: ARI
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
. _ Qrg _Contractor: AA TS -
RESULTS UNITS
1600U UG/KG
1600U UG/KG
4000U UG/KG
4000U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
4000U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
1600U UG/KG
79 %
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k,.-.. ,n to be less than value given. L-actual value is known to be greater than value gir ·· U-material was analyzed for but not detected. the number is the minimum quantit~"'"'n limit.
R-qc indicates th< unusable. compound may or may not be present. resampling and reanalysis i: ssary for verification.
C-confirmed by gc.. ___ 1.when no value is reported, see chlordane constituents 2.constituents or metab ... __ ~.:> of technical chlordane
-Sample 12956 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY38 Id/Station: RCSE19
Media: SOIL
RESULTS
3000JN
20000J
400000J
UNITS
UG/KG
UG/KG
UG/KG
D Number: MY85
ANALYTE
METHYL (METHYL ETHYL) PHENANTHRENE
ALKANES
28 UNIDENTIFIED COMPOUNDS
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor. RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was anafyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
-Sample 13683 FY 1997 Project: 97--0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RSCE5
Media: SOIL D Number: MY69
RESULTS
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
1700U
660U
1700U
660U
660U
660U
1700U
660U
1700U
1700U
660U
660U ~ 660U
~
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BI5(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
660U
660U
1700U
1700U
660U
660U
660U
1700U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
50
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYLPHENYLETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BEN2YLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BI5(2-ETHYLHEXYL) PHTHALA TE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 13683 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RSCE5
Media: SOIL
RESULTS UNITS
4000JN UG/KG
10000J UG/KG
10000J UG/KG
D Number: MY69
ANALYTE
CARBOXYLIC ACIDS
ALKANES
9 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
K-actual value is kr"'·~n to be less than value given. L-actual value is known to be greater than value givr"' U-material was analyzed for but not detected. the number is the minimum quanti•-··..,.n limit.
R-qc indicates th< · unusable. compound may or may not be present. resampling and reanalysis i: ssary for verification.
C-confirmed by gc.._. . 1.when no value is reported, see chlordane constituents 2.constituents or metab..._ _. 1.i of technical chlordane
Sample 13683 FY 1997 Project: 97 -0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RSCE5
Media: SOIL D Number: MY69
RESULTS UNITS
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
1700U
660U
1700U
660U
660U
660U
1700U
660U
1700U
1700U
660U c:y:::i· 660U
~ 660U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Org Contractor: AA TS
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
RESULTS UNITS ANALYTE
660U
660U
1700U
1700U
660U
660U
660U
1700U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
660U
50
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL--4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENlYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 13683 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RSCE5
Media: SOIL
RESULTS UNITS
4000JN UG/KG
10000J UGIKG
10000J UG/KG
D Number: MY69
ANALYTE
CARBOXYLIC ACIDS
ALKANES
9 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J..estimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
K-actual value is j(r -··ri to be less than value given. L-actual value is known to be greater than value giv---U-material was analyzed for but not detected. the number is the minimum quanti' , limit.
R-qc indicates th; unusable. compound may or may not be present. resampling and reanalysis i~ ·ssary for verification.
C-confirmed by gc.. ____ 1.when no value is reported, see chlordane constituents 2.constituents or metabc... ___ .> of technical chlordane
-