NCD986187094_20010930_Reasor Chemical Company_FRBCERCLA SPD_HRS Documentation Package Volume III - Reference 4 (continued)-OCR

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Reasor Chemical
NCO 986 187 094
Castle Hayne, New Hanover Co., NC
HRS DOCUMENTATION PACKAGE
Volume III Reference 4 (continued)
vcaiLE ... ""t.a.iAL--
Sample 12956 FY 1997
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
Project: 97-0357
Id/Station: RCSE19
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY38
Produced by: Denise Goddard
Requester: RAY DOYLE
Project leader: DOYLE
Beginning: 08/25197 13:25
Ending:
lnorg Contractor: ARI ___________ ------------
Media: SOIL
RESULTS UNITS
48U UG/KG
48U UGIKG
48U UGIKG
48U UG/KG
48U UG/KG
130U UG/KG
48U UGIKG
48U UGIKG
48U UGIKG
48U UG/KG
48U UG/KG
48U UGIKG
33J UG/KG
48U UGIKG
48U UGIKG
48U UGIKG
48U UG/KG
48U UG/KG
48U UGIKG
48U UG/KG
48U UGIKG
48U UGIKG
48U UGIKG
48U UG/KG
48U UGIKG
48U UGIKG
48U UGIKG
48U UG/KG
48U UGIKG
48U UG/KG
48U UG/KG
48U UG/KG
48U UG/KG
79 %
D Number: MY85
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contrac_t_or·.AATS-------------
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-r,onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of !echnical chlordane
-.TI ... GW - -Sample 12956 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE19
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY38 lnorg Contractor: ARI
D Number: MY85 Org Contra~tQr:_AATS __ _
--------------------------
RESULTS
30JN
100J
UNITS
UG/KG
UG/KG
ANALYTE
METHYL (METHYL ETHYL) BENZENE
1 UNIDENTIFIED COMPOUND
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
--------------
K-actual value is."'· --,.,n to be less than value given. L-actual value is known to be greater than value 9=· -U-material was analyzed for but not detected. the number is the minimum quanF ·:"'n limit.
R-qc indicates th 3 unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by g..__ 1.when no value is reported, see chlordane constituents 2.constituents or metaL._ ... clS of technical chlordane
Sample 1 :.c,56 FY 1997
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
-Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
-Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 13:25
Ending:
Id/Station: RCSE19 MD Number: MY38 lnorg Contractor: ARI _____ _
D Number: MY85 ___ Org_Contractor;-AATS--------Media: SOIL --------------
RESULTS UNITS ANALYTE
48U
48U
48U
48U
48U
130U
48U
48U
48U
48U
48U
48U
33J
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
48U
79
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
---------
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed _by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-----
VIIITIL!illll\MPMiltNA~ ---Ef'IIIIEGW, -qp AT!-W, GJW --Sample 12923 FY 1997
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE18
Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11 :20
Ending:
Media: SOIL D Number: MY82 Org Contr~torJ\ATS ___ -------------
-----------------------·
-----
RESULTS UNITS
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
7J UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
58 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROM OF ORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 1-· ·n to be less than value given. L-actual value is known to be greater than value gr· U-material was analyzed for but not detected. the number is the minimum quanP ··.,,n limit.
R-qc indicates thi ·1 unusable. compound may or may not be present. resampling and reanalysis i !ssary for verification.
,... "onfirmed by gei,,.,; 1.when no value is reported, see chlordane constituents 2.constituents or metab ...... ~s of technical chlordane
,-.fl~l'l\11111119\N~S --Sample 12923 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE 18
CASTLE HAYNE, NC
Case Number: 25655
--Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11:20
Ending:
Media: SOIL D Number: MY82 Org_y_g[!_tr_actor:_AATS---------
----------
-----------------------------------
RESULTS UNITS
100JN UG/KG
100JN UG/KG
ANALYTE
METHYL (METHYL ETHYL) BENZENE
2 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
-----
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1. when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-----
Sample 12923 FY 1997
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
--Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
-Produced by: John Mcconney
-Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 11 :20
Ending:
Id/Station: RCSE18
Media: SOIL D Number: MY82 Org_Qq_~tra_ctor:_AATS-------------------------
------------------------
RESULTS UNITS
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24U UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
7J UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
24UJ UG/KG
58 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
-----
A-average value. NA•not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is½~ , to be less than value given. L-actual value is known to be greater than value giv~ LI-material was analyzed for but not detected. the number is the minimum quantit'°'''"" limit.
R-qc indicates the:. unusable. compound may or may not be present. resarnpling and reanalysis i: ssary for verification.
C-confrrmed by gO.,,.~-·· 1.when no value is reported, see chlordane constituents 2.constituents or metab ..... _~.s of technical chlordane
-----
-Sample 12922 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE17
Media: SOIL ____ D Number. MY81------0rg Contraclor:-AATS
------------------
RESULTS UNITS
20JN UG/KG
50J UG/KG
ANALYTE
METHYL (METHYL ETHYL) BENZENE
2 UNIDENTIFIED COMPOUNDS
-

-
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
--------------
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
------------
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis is necessary for verification.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12922 FY 1997
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE17
-Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
Media: SOIL D Number: MY81
----------------_Org.Contractor.-AATS----------------------------
RESULTS UNITS
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
10U UG/KG
3 %
ANALYTE
. CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k· 'to be less than value given. L-actual value is known to be greater than value gi\' U-material was analyzed for but not detected. the number is the minimum quanti' 1 limit.
R-qc indicates Iha unusable. compound may or may not be present. resampling and reanalysis is ssary for verification.
,... -r-onfirmed by gcrn_,; ·1.when no value is reported, see chlordane constituents 2.constituents or metabo1o .... s of technical chlordane
-----
V .... ILE-""P~Ai..a. --Sample 12922 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE17
Media: SOIL D Number: MY81
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
3
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
-Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 10:55
Ending:
A-average value. NA-not analyzed. NAl-interferences. J.-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
V--ILE-MPiaa,IAt.aa ---EP---=Glc_,SE-TH-GA---Sample 12953 -FY• 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF
Id/Station: RCSE16
Media: SOIL
RESULTS UNITS
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
30U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
9J UG/KG
17UJ UG/KG
17UJ UG/KG
10J UG/KG
17UJ UG/KG
42 %
Case Number: 25655
MD Number: MY35
D Number: MY80
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. N~~not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
K-actual value is ~ -, to be less than value given. L-actuar value is known to be greater than value gi· U-material was analyzed for but not detected. the number is the minimum quant:· , limit.
R-qc indicates the. . unusable. compound may or may not be present. resampling and reanalysis i. ,ssary for verification.
,.... -,...nfirmed by gcil,;;,. 1.when no value is reported, see chlordane constituents 2.constituents or metabom~s of technical chlordane
V--ILi:.-MP~AtalS ---EPalll!:Gl-.,S
Sample 129:,3 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE16
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY35
D Number: MY80
lnorg Contractor: ARI
Org Contractor: AA TS
2000JN UG/KG
2000J UG/KG
METHYL(METHYLETHYL)BENZENE (2 ISOMERS)
7 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constltuents or metabolites of technical chlordane
_,,.--:::
--El'aljEG'illlli" Siii1AT1-iMi, G... ---uc.,_iat"i11ii11/9iliM49 ·-
Sample 12953 FY 1997 . Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC.
Program: NSF Case Number: 25655
Id/Station: RCSE16 MD Number: MY35
Media: SOIL D Number: MY80
RESULTS UNITS
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
30U UG/KG
17U UG/KG
17U UG/KG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
17U UG/KG
17U UG/KG
1, 1-DICHLOROETHENE {1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
17U UG/KG
17U UG/KG
17U UG/KG
17U UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
17UJ UG/KG
9J UG/KG
17UJ UG/KG
17UJ UG/KG
10J UG/KG
17UJ UG/KG
42 %
1,2-DICHLOROETHENE {TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE {TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE {TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:50
Ending:
K-actual value is i--~-"'n to be less than value given. L-actual value is known to be greater than value gr·--U-material was analyzed for but not detected. the number is the minimum quant;• -••Qn limit.
R-qc indicates th' 1 unusable. compound may or may not be present. resampling and reanalysis ~ssary for verification.
C-confirmed by QL .... -1.when no value is reported, see chlordane constituents 2.constituents or meta .. _ .~s of technical chlordane
'11111TIL ... llll~NA-, ---EFailaEG~ S-ATltlll, G---Sample 12921 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE15
Media: SOIL D Number: MY79 Org Contractor: AA TS
RESULTS UNITS
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
ZOU UG/KG
30U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UGIKG
16U UG/KG
16U UGIKG
16U UGIKG
16U UG/KG
16U UG/KG
16U UGIKG
16U UG/KG
16U UG/KG
16U UG/KG
38 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
¾MOISTURE
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. .
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis is necessary for verification.
C-confrrmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~TIL'iiir'MFWNA~ --Sample 12921 , FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE15
Media: SOIL
ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY79
RESULTS UNITS
20000J UG/KG 13 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
- -Produced by: John Mcconney
Requestor. RAY DOYLE
Project leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is.1• • "" to be less than value given. L-actual value is known to be greater than value gf,· U-material was analyzed for but not detected. the number is the minimum quanti•-•:<'Jn limit.
R-qc indicates th' a unusable. compound may or may not be present. resampling and reanalysis · essary for verification.
C-~onfirmed by gc.. .. ~: 1.when no value is reported, see chlordane constituents 2.constituents or metat, •... ~s of technical chlordane
valllflL~IIIIF9illNA.., -
Sample 1 i921 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE15
Media: SOIL D Number: MY79
RESULTS UNITS
16U UG/KG
16U UG/KG
16U UG/KG
16U UGIKG
20U UGIKG
30U UGIKG
16U UGIKG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
16U UG/KG
16U UGIKG
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
16U UG/KG
16U UG/KG
16U UG/KG
16U UGIKG
16U UGIKG
16U UG/KG
16U UGIKG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UGIKG
16U UG/KG
16U UGIKG
16U UG/KG
16U UG/KG
16U UGIKG
16U UGIKG
16U UGIKG
16U UGIKG
16U UGIKG
16U UGIKG
16U UG/KG
38 %
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
-Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 09:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material ..
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirrned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
"IIIITIL ... MflatNAraf, ---EFWJ!SEG_, SIIIIIIATIIIIII, GJIIIII --Sample 12920 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE14
Media: SOIL D Number: MY78
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
34UJ
34UJ
34UJ
34UJ
34UJ
70UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
34UJ
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
6J
34UJ
34UJ
34UJ
500
42
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
EXCESSIVE HOLDING TIME
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
K-actual value is 1---· ·'1 to be less than value given. L-actual value is known to be greater than value gi,· U-material was anaTyzed for but not detected. the number is the minimum quanu· , limit.
R-qc indicates thi. ; unusable. compound may or may not be present. resampling and reanalysis i: ·ssary for verification.
r:-r:onfirmed by gc,, ..... --1.when no value is reported, see chlordane constituents 2.constituents or metab1., ... '?s of technical chlordane
.... TILIIIIFllll~NAIIIS, ---E~EG_.vS-AT ... ,G ... - -
Sample · 12920 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE14
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY78
RESULTS
100JN
4000J
UNITS
UG/KG
UG/KG
ANALYTE
METHYLETHYL}BENZENE
11 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-E~EGaif'S~T ... ,G,.. --._iuc'illt>at ... 1/9~9 -
Sample 12920 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE14
Media: SOIL D Number: MY78
RESULTS UNITS
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
70UJ UG/KG
34UJ UG/KG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
34UJ UG/KG
34UJ UG/KG
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
6J UG/KG
34UJ UG/KG
34UJ UG/KG
34UJ UG/KG
500 UG/KG
42 %
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
EXCESSIVE HOLDING TIME
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97 08:30
Ending:
K-actual value is i., ·•n to be less than value given. L-actual value is known to be greater than value 91,· U-material was analyzed for but not detected. the number is the minimum quant;• ··"'n limit.
R-qc indicates th, 1 unusable. compound may or may not be present. resampling and reanalysis i :ssary for verification.
C-confirmed by gC. .... ·· 1.when no value is reported. see chlordane constituents 2.constituents or metab ... , .. .:s of technical chlordane
-Sample 12919 FY 1997
VOLATILES SCAN
Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE13
Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
24 %
D Number: MY77
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3--DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:40
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~
-Sample 12919 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE13
Media: SOIL D Number: MY77 Org Contractor: AA TS
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
24 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE}
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
0
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--1i11f uc.-.,atea11f 119-_ig -
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:40
Ending:
K-actual value is J,· -· ···n to be less than value given. L-actual value is known to be greater than value gi,.· U-material was analyzed for but not detected. the number is the minimum quant1' · "'-,n limit.
R-qc indicates th:· 1 unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confirmed by gC.., ___ . 1.when no value is reported, see chlordane constituents 2.constituents or metaL~------s of technical chlordane
-Sample 12~, 8 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE12
Media: SOIL
RESULTS UNITS
20000JN UG/KG
ANALYTE
PINENE ISOMER
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY76
1000000JN UG/KG
300000J UG/KG
METHYL (METHYL ETHYL) BENZENE
8 UNIDENTIFIED COMPOUNDS
Ti--,GAall ---uci-,ate-119'allli9 -
Org Contractor: MTS
Produced by: John Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:·
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R--qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
llal\Tllllllf,A~AN .... 1S --Sample 12918 FY 1997 Project: 97--0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE12
Media: SOIL · D Number: MY76
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
2600U
7600
2600U
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
600J
2600U
2000J
53
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. _NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
K-actual value if vn to be less than value given. L-actual value is known to be greater than value_' ·. U-material was analyzed for but not detected. the number is the minimum qua~ •;on limit.
R-qc indicates t .ta unusable. compound may or may not be present. resampling and reanalysis. ;essary for verification.
C:-confirmed by gt:rnS: 1.when no value is reported, see chlordane constituents 2.constituents or meta1.1u11tes of technical chlordane
~T-"'"-.. At-.-slS--Sample 12918 FY 1997 Project: 97--0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE12
Media: SOIL D Number: MY76
RESULTS
20000JN
1000000JN
300000J
UNITS
UGIKG
UG/KG
UGIKG
ANALYTE
PINENE ISOMER
METHYL (METHYL ETHYL) BENZENE
8 UNIDENTIFIED COMPOUNDS
IV-.:>, AllialS, -
Org Contractor: AA TS
--Produced by: Denise Goddard
Requestor. RAY DOYLE
Project Leader: DOYLE
Beginning: 08124197 13:45
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12918 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE12
Media: SOIL D Number: MY76 Org Contractor: AA TS
RESULTS UNITS ANAL YTE
2600U UG/KG CHLOROMETHANE
2600U UG/KG BROMOMETHANE
2600U UG/KG VINYL CHLORIDE
2600U UG/KG CHLOROETHANE
2600U UG/KG METHYLENE CHLORIDE
2600U UG/KG ACETONE
2600U UG/KG CARBON DISULFIDE
2600U UG/KG 1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
2600U UG/KG 1,1-DICHLOROETHANE
2600U UG/KG 1,2-DICHLOROETHENE (TOTAL)
2600U UG/KG CHLOROFORM
2600U UG/KG 1,2-DICHLOROETHANE
2600U UG/KG METHYL ETHYL KETONE
2600U UG/KG 1,1,1-TRICHLOROETHANE
2600U UG/KG CARBON TETRACHLORIDE
--Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:45
Ending:
2600U UG/KG BROMODICHLOROMETHANE ---2600U-UG/KG-1,2-DICHl.:OROPROPANE'_::_:_:::_ ________________________________________ _
2600U UG/KG CIS-1,3-DICHLOROPROPENE
2600U UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
2600U UG/KG DIBROMOCHLOROMETHANE
2600U UG/KG 1,1,2-TRICHLOROETHANE
2600U UG/KG BENZENE
2600U UG/KG TRANS-1,3-DICHLOROPROPENE
2600U UG/KG BROMOFORM
2600U UG/KG METHYL ISOBUTYL KETONE
2600U UG/KG METHYL BUTYL KETONE
2600U UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
2600U UG/KG 1, 1,2,2-TETRACHLOROETHANE
7600 UG/KG TOLUENE
2600U UG/KG CHLOROBENZENE
600J UG/KG ETHYL BENZENE
2600U UG/KG STYRENE
2000J UG/KG TOTAL XYLENES
53 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is \<,..--._,n to be less than value given. L-actual value is known lo be greater than value gh•--LI-material was analyzed for but not detected. the number is the minimum quantit-•:"ln limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i !ssary for verification.
C-confirmed by g(.;_ .-1.when no value is reported, see chlordane constituents 2.constituents or metal. ..... :.s of technical chlordane
Sample 12917 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE11
Media: SOIL D Number: MY75 Org Contractor: AA TS
RESULTS UNITS ANALYTE
17U UG/KG CHLOROMETHANE
17U UG/KG BROMOMETHANE
17U UG/KG VINYL CHLORIDE
17U UG/KG CHLOROETHANE
20U UG/KG METHYLENE CHLORIDE
120 UG/KG ACETONE
17U UG/KG CARBON DISULFIDE
17U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
17U UG/KG 1,1-DICHLOROETHANE
17U UG/KG 1,2-DICHLOROETHENE (TOTAL)
4U UG/KG CHLOROFORM
17U UG/KG 1,2-DICHLOROETHANE
17U UG/KG METHYL ETHYL KETONE
s.~ - -
Produced by: Denise Goddard
Requestor. RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
17UJ UG/KG 1, 1, 1-TRICHLOROETHANE
17UJ UG/KG CARBON TETRACHLORIDE ____ 17UJ_UGIKG-BROMODICHLOROMETHANE---------------------------------------
17UJ UG/KG 1,2-DICHLOROPROPANE
17UJ UG/KG CIS-1,3-DICHLOROPROPENE
17UJ UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
17UJ UG/KG DIBROMOCHLOROMETHANE
17UJ UG/KG 1, 1,2-TRICHLOROETHANE
3J UG/KG BENZENE
17UJ UG/KG TRANS-1,3-DICHLOROPROPENE
17UJ UG/KG BROMOFORM
17UJ UG/KG . METHYL ISOBUTYL KETONE
17UJ UG/KG METHYL BUTYL KETONE
17UJ UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
17UJ UG/KG 1, 1,2,2-TETRACHLOROETHANE
10J UG/KG TOLUENE
17UJ UG/KG CHLOROBENZENE
17UJ UG/KG ETHYL BENZENE
17UJ UG/KG STYRENE
4J UG/KG TOTALXYLENES
42 % % MOISTURE
~ ~
/\-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
/ \ctual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
\indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
'firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
\
-Sample 12917 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE11
Media: SOIL D Number: MY75 Org Contractor: AA TS
RESULTS UNITS ANALYTE
100J UG/KG 3 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
--...,iucll!li)allllllli11/9illl4911111J
Produced by: Joh.n Mcconney
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
K-actual value is kr-.. •n to be less than value given. L-actual value is known to be greater than value giv~-U-material was analyzed for but not detected. the number is the minimum quantit~''"n limit.
R-qc indicates the_ _ unusable. compound may or may not be present. resampling and reanalysis i! ssary for verification.
C-confirmed by gc.-., .. o.·• -1.when no value is reported, see chlordane constituents 2.constituents or metab ... -... _.,:j of technical chlordane
~TIL~"'1r--.NA-.S ---Ei-.EG-VS-AT ... ,G .. --
Sample 12917 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE11
Media: SOIL D Number: MY75 Org Contractor: AA TS
RESULTS UNITS ANALYTE
17U UG/KG CHLOROMETHANE
17U UG/KG BROMOMETHANE
17U UG/KG VINYL CHLORIDE
17U UG/KG CHLOROETHANE
20U UG/KG METHYLENE CHLORIDE
120 UG/KG ACETONE
17U UG/KG CARBON DISULFIDE
17U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
17U UG/KG 1, 1-DICHLOROETHANE
17U UG/KG 1,2-DICHLOROETHENE (TOTAL)
4U UG/KG CHLOROFORM
17U UG/KG 1,2-DICHLOROETHANE
17U UG/KG METHYL ETHYL KETONE
17UJ UG/KG 1,1,1-TRICHLOROETHANE
17UJ UG/KG CARBON TETRACHLORIDE
Produced by: John McConney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:30
Ending:
____ 17UJ_UG/KG_BROMODICHLOROMETHANE-----------------------------------------
17UJ UG/KG 1,2-DICHLOROPROPANE
17UJ UG/KG CIS-1,3-DICHLOROPROPENE
17UJ UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
17UJ UG/KG DIBROMOCHLOROMETHANE
17UJ UG/KG 1,1,2-TRICHLOROETHANE
3J UG/KG BENZENE
17UJ UG/KG TRANS-1,3-DICHLOROPROPENE
17UJ UG/KG BROMOFORM
17UJ UG/KG METHYL ISOBUTYL KETONE
17UJ UG/KG METHYL BUTYL KETONE
17UJ UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
17UJ UG/KG 1, 1,2,2-TETRACHLOROETHANE
10J UG/KG TOLUENE
17UJ UG/KG CHLOROBENZENE
17UJ UG/KG ETHYL BENZENE
17UJ UG/KG STYRENE
4J UG/KG TOTAL XYLENES
42 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. ·
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12915 FY' 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE10
Media: SOIL
RESULTS UNITS
80000JN UG/KG
8000000JN UG/KG
2000000J UG/KG
D Number: MY7 4
ANALYTE
PINENE ISOMER
METHYL(METHYLETHYL)BENZENE
11 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
--Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is;' -·n to be less than value given. L-actual value is known to be greater than value g;· U-material was analyzed for but not detected. the number is the minimum quanw ·,n limit.
R-qc indicates th. a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
r.-confirmed by gC,,;.-:,:: 1.when no value is reported, see chlordane constituents 2.constituents or metab..;.-,.es of technical chlordane
-Sample 12915 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE10
Media: SOIL D Number. MY7 4 Org Contractor: AA TS
RESULTS UNITS ANALYTE
32000U UG/KG CHLOROMETHANE
32000U UG/KG BROMOMETHANE
32000U UG/KG VINYL CHLORIDE
32D00U UG/KG CHLOROETHANE
32000U UG/KG METHYLENE CHLORIDE
32000U UG/KG ACETONE
32000U UG/KG CARBON DISULFIDE
32000U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
32000U UG/KG 1, 1-DICHLOROETHANE
32DO0U UG/KG 1,2-DICHLOROETHENE (TOTAL)
32000U UG/KG CHLOROFORM
32000U UG/KG 1,2-DICHLOROETHANE
32000U UG/KG METHYL ETHYL KETONE
32000U UG/KG 1, 1, 1-TRICHLOROETHANE
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/9713:15
Ending:
32000U UG/KG CARBON TETRACHLORIDE 32000U UG/KG BROMODICHLORO_METHANE ______________________________________ _
---32ooou-UG)KG-1,2-DICHLOROPROPANE
32000U UG/KG CIS-1,3-DICHLOROPROPENE
3200DU UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
32000U UG/KG DIBROMOCHLOROMETHANE
32000U UG/KG 1, 1,2-TRICHLOROETHANE
32000U UG/KG BENZENE
32000U UG/KG TRANS-1,3-DICHLOROPROPENE
32000U UG/KG BROMOFORM
32000U UG/KG METHYL ISOBUTYL KETONE
32000U UG/KG METHYL BUTYL KETONE
32000U UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
32000U UG/KG 1, 1,2,2-TETRACHLOROETHANE
500000 UG/KG TOLUENE
32000U UG/KG CHLOROBENZENE
3800J UG/KG ETHYL BENZENE
32000U UG/KG STYRENE
34000U UG/KG TOTAL XYLENES
24 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12915 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE10
Media: SOIL
RESULTS
B0000JN
8000000JN
2000000J
UNITS
UGIKG
UG/KG
UG/KG
D Number: MY74
ANALYTE
PINENE ISOMER
METHYL(METHYLETHYL)BENZENE
11 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
--Produced by: John Mcconney
Requestor: RAY DOYLE
-Project Leader: DOYLE
Beginning: 08124197 13: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is k,. -···n to be less than value given. L-actual value is known to be greater than value giv,.._-U-material was analyzed for but not detected. the number is the minimum quantit..,•;'ln limit.
R-qc indicates th; unusable. compound may or may not be present. resampling and reanalysis ii ·ssary for verification.
C-confirmed by gc,.. 1.when no value is reported, see chlordane constituents 2.constituents or metab~. __ .. .s of technical chlordane
-Sample 1:d15 FY 1997 Project 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE10
Media: SOIL D Number: MY74 Org Contractor: AA TS
RESULTS UNITS ANALYTE
32000U UG/KG CHLOROMETHANE
32000U UG/KG BROMOMETHANE
32000U UG/KG VINYL CHLORIDE
32000U UG/KG CHLOROETHANE
32000U UG/KG METHYLENE CHLORIDE
32000U UG/KG ACETONE
32000U UG/KG CARBON DISULFIDE
32000U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
32000U UG/KG 1, 1-DICHLOROETHANE
32000U UG/KG 1,2-DICHLOROETHENE (TOTAL)
32000U UG/KG CHLOROFORM
32000U UG/KG 1,2-DICHLOROETHANE
32000U UG/KG METHYL ETHYL KETONE
32000U UG/KG 1,1,1-TRICHLOROETHANE
32000U UG/KG CARBON TETRACHLORIDE
-Produced by: John Mcconney
Requestor. RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 13:15
Ending:
32000U UG/KG BROMODICHLOROME:1T~HrA~N~E ________________________________________ _
32000U UG/KG 1,2-DICHLOROPROPA_l,JE
---32000U-UG!KG-CIS:1;3:DICH[OROPROPENE
32000U UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
32000U UG/KG DIBROMOCHLOROMETHANE
32000U UG/KG 1,1,2-TRICHLOROETHANE
32000U UG/KG BENZENE
32000U UG/KG TRANS-1,3-DICHLOROPROPENE
32000U UG/KG BROMOFORM
32000U UG/KG METHYL ISOBUTYL KETONE
32000U UG/KG METHYL BUTYL KETONE
32000U UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
32000U UG/KG 1, 1,2,2-TETRACHLOROETHANE
500000 UG/KG TOLUENE
32000U UG/KG CHLOROBENZENE
3800J UG/KG ETHYL BENZENE
32000U UG/KG STYRENE
34000U UG/KG TOTAL XYLENES
24 % % MOISTURE
A-average value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
\atTIL ... Mi-.NAIIIF5 --Sample 12913" FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE9
Media: SOIL
RESULTS UNITS
700JN UG/KG
20JN UG/KG
ANALYTE
PINENE ISOMER
LIMONENE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY72
100J UG/KG 1 UNIDENTIFIED COMPOUND
Org Contractor: MTS
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
A-average value. ·N~-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is 11n to be less than value given. L-actual value is known to be greater than valuer· U-materia1 was analyzed for but not detected. the number is the minimum quar · ··on limit.
R-qc indicates ti... ._.a unusable. compound may or may not be present. resampling and reanalysis. ,essary for verification.
--,mfirmed by QC,;ii,.S:: 1.when no value is reported, see chlordane constituents 2.constituents or metat,..,,,1es of technical chlordane
-Sample 12913 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF Case Number: 25655
Id/Station: RCSE9
Media: SOIL D Number: MY72 Org Contractor: AA TS
RESULTS UNITS ANALYTE
13U UG/KG CHLOROMETHANE
13U UG/KG BROMOMETHANE
13U UG/KG VINYL CHLORIDE
13U UG/KG CHLOROETHANE
20U UG/KG METHYLENE CHLORIDE
30U UG/KG ACETONE
13U UG/KG CARBON DISULFIDE
13U UG/KG 1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
13U UG/KG 1,1-DICHLOROETHANE
13U UG/KG 1,2-DICHLOROETHENE (TOTAL)
SJ UG/KG CHLOROFORM
13U UG/KG 1,2-DICHLOROETHANE
13U UG/KG METHYL ETHYL KETONE
13U UG/KG 1,1,1-TRICHLOROETHANE
-Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
13U UG/KG CARBON TETRACHLORIDE
13U UG/KG BROMODICHLOROMETHii,A~N~E ________________________________________ _
____ 13U-UG/KG-1,2-DICHLOROPROPANE:_
13U UG/KG CIS-1,3-DICHLOROPROPENE
13U UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
13U UG/KG DIBROMOCHLOROMETHANE
13U UG/KG 1, 1,2-TRICHLOROETHANE
13U UG/KG BENZENE
13U UG/KG TRANS-1,3-0ICHLOROPROPENE
13U UG/KG BROMOFORM
13UJ UG/KG METHYL ISOBUTYL KETONE
13UJ UG/KG METHYL BUTYL KETONE
21J UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
13UJ UG/KG 1,1,2,2-TETRACHLOROETHANE
13UJ UG/KG TOLUENE
13UJ UG/KG CHLOROBENZENE
13UJ UG/KG ETHYL BENZENE
13UJ UG/KG STYRENE
13UJ UG/KG TOTALXYLENES
24 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12913 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL-
Program: NSF
Id/Station: RCSE9
Media: SOIL
ANALYTE
PINENE ISOMER
LIMONENE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY72
RESULTS
700JN
20JN
100J
UNITS
UG/KG
UG/KG
UG/KG 1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -
llilfdu<tllDatlllllt'11/M:49 -
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
K-actual value is .I'-"vn to be less than vallle given. L-actual value is known to be greater than value gi,., -U-material was analyzed far but not detected. the number is the minimum quanl'' •:'ln limit.
R-qc indicates th 3 unusable. compound may or may not be present. resampling and reanalysis i ~ssary for verification.
C-confirmed by g.,_,_ ~:· 1.when no value is reported. see chlordane constituents 2.constituents or metal.~.--.:s of technical chlordane
-Sample 12913 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE9
Media: SOIL D Number: MY72 Org Contractor: AA TS
RESULTS UNITS ANALYTE
13U UG/KG CHLOROMETHANE
13U UG/KG BROMOMETHANE
13U UG/KG VINYL CHLORIDE
13U UG/KG CHLOROETHANE
20U UG/KG METHYLENE CHLORIDE
30U UG/KG ACETONE
13U UG/KG CARBON DISULFIDE
13U UG/KG 1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
13U UG/KG 1, 1-DICHLOROETHANE
13U UG/KG 1,2-DICHLOROETHENE (TOTAL)
8J UG/KG CHLOROFORM
13U UG/KG 1,2-DICHLOROETHANE
13U UG/KG METHYL ETHYL KETONE
13U UG/KG 1,1,1-TRICHLOROETHANE
13U UG/KG CARBON TETRACHLORIDE
-Produced by: John McConney
Req~estor: RAY DOYLE_
Project Leader: DOYLE
Beginning: 08/24/97 12:50
Ending:
13U UG/KG BROMODICHLOROMETHAA1N~E~--------------~-------------------------
____ 13U_UG/KG-1,2-DICHlOROPROPANE_:
13U UG/KG CIS-1,3-DICHLOROPROPENE
13U UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
13U UG/KG DIBROMOCHLOROMETHANE
13U UG/KG 1,1,2-TRICHLOROETHANE
13U UG/KG BENZENE
13U UG/KG TRANS-1,3-DICHLOROPROPENE
13U UG/KG BROMOFORM
13UJ UG/KG METHYL ISOBUTYL KETONE
13UJ UG/KG METHYL BUTYL KETONE
21J UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
13UJ UG/KG 1, 1,2,2-TETRACHLOROETHANE
13UJ UG/KG TOLUENE
13UJ UG/KG CHLOROBENZENE
13UJ UG/KG ETHYL BENZENE
13UJ UG/KG STYRENE
13UJ UG/KG TOTALXYLENES
24 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12912 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSEB
Media: SOIL D Number: MY71 Org Contractor: AA TS
RESULTS UNITS ANALYTE
10U UG/L CHLOROMETHANE
10U UG/L BROMOMETHANE
10U UG/L VINYL CHLORIDE
10U UG/L CHLOROETHANE
30U UG/L METHYLENE CHLORIDE
10U UG/L ACETONE
10U UG/L CARBON DISULFIDE
10U UG/L 1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
10U UG/L 1,1-DICHLOROETHANE
10U UG/L 1,2-DICHLOROETHENE (TOTAL)
10U UG/L CHLOROFORM
10U UG/L 1,2-DICHLOROETHANE
10U UG/L METHYL ETHYL KETONE
1 OU UG/L 1, 1, 1-TRICHLOROETHANE
10U UG/L CARBON TETRACHLORIDE
Produced by: Denise Goddard
Requestor: RAY_ DOY~E _
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
10U UG/L BROMODICHLOROl~M~E~TilHrA~N~E~----------------------------------------10U UG/L 1,2-DICHLOROPRQPANE
----10U-UG/l:--cIs:1:3-DICHLOR-OPROPENE
10U UG/L TRICHLOROETHENE (TRICHLOROETHYLENE)
10U UG/L DIBROMOCHLOROMETHANE
10U UG/L 1,1,2-TRICHLOROETHANE
10U UG/L BENZENE
10U UG/L TRANS-1,3-DICHLOROPROPENE
10U UG/L BROMOFORM
10U UG/L METHYL ISOBUTYL KETONE
10U UG/L METHYL BUTYL KETONE
10U UG/L TETRACHLOROETHENE (TETRACHLOROETHYLENE)
10U UG/L 1,1,2,2-TETRACHLOROETHANE
1 OU UG/L TOLUENE
10U UG/L CHLOROBENZENE
1 OU UG/L ETHYL BENZENE
10U UG/L STYRENE
5 UG/L % MOISTURE
10U UG/L TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is_· •n to be less than value given. L-actual value is known to be greater than value 9' LI-material was analyzed for but not detected. the number is the minimum quan·· ·,n limit.
R-qc indicates th_ .a unusable. compound may or may not be present. resampling and reanalysis. essary for verification.
r.-confirmed by gCmS·: 1.when no value is reported, see chlordane constituents 2.constituents or metab .... uleS of technical chlordane
-Sample 12912 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSEB
Media: SOIL D Number: MY71 Org Contractor: AA TS
RESULTS UNITS ANALYTE
10U UG/L CHLOROMETHANE
10U UG/L BROMOMETHANE
10U UG/L VINYL CHLORIDE
10U UG/L CHLOROETHANE
30U UG/L METHYLENE CHLORIDE
1 OU UG/L ACETONE
10U UG/L CARBON DISULFIDE
10U UG/L 1,1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1 OU UG/L 1, 1-DICHLOROETHANE
10U UG/L 1,2-DICHLOROETHENE (TOTAL)
10U UG/L CHLOROFORM
10U UG/L 1,2-DICHLOROETHANE
10U UG/L METHYL ETHYL KETONE
10U UG/L 1, 1,1-TRICHLOROETHANE
- -Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 11 :30
Ending:
10U UG/L CARBON TETRACHLORIDE 10U UG/L BROMODICHLOROMETHAAf':N_':E ________________________________________ _
____ 1ou_UG/L--1,2-DICHLOROPR0PANE·..:
1 OU UG/L CIS-1,3-DICHLOROPROPENE
10U UG/L TRICHLOROETHENE (TRICHLOROETHYLENE)
10U UG/L DIBROMOCHLOROMETHANE
1 OU UG/L 1, 1,2-TRICHLOROETHANE
1 OU UG/L BENZENE
10U UG/L TRANS-1,3-DICHLOROPROPENE
10U UG/L BROMOFORM
10U UG/L METHYL ISOBUTYL KETONE
10U UG/L METHYL BUTYL KETONE
10U UG/L TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1 OU UG/L 1, 1,2,2-TETRACHLOROETHANE
10U UG/L TOLUENE
10U UG/L CHLOROBENZENE
1 OU UG/L ETHYL BENZENE
10U UG/L STYRENE
5 UG/L % MOISTURE
1 OU UG/L TOT AL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
", Sample 12911 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number. 25655
Id/Station: RCSE7
Media: SOIL D Number: MY70
RESULTS UNITS
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
JOU UG/KG
20U UG/KG
16U UG/KG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
16U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
16U UG/KG 1, 1-DICHLOROETHANE
16U UG/KG 1,2-DICHLOROETHENE (TOTAL)
16U UG/KG CHLOROFORM
16U UG/KG 1,2-DICHLOROETHANE
16U UG/KG METHYL ETHYL KETONE
16U UG/KG 1, 1, 1-TRICHLOROETHANE
-Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
16U UG/KG
16U UG/KG
16U UG/KG
CARBON TETRACHLORIDE
BROMODICHLOROMETHAI\IN~E=---~-------------------------------------1,2:DICHLOROf'ROl?ANE-
----,16U UG/KG
s; -1-C __ 0
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
16U UG/KG
38 %
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is· ·•n to be less than value given. L-actual value is known to be greater than value 9' . U-material was analyzed for but not detected. the number is the minimum quan•·· ·,n limit.
R-qc indicates ft', a unusable. compound may or may not be present. resampling and reanalysis 8ssary for verification.
r:-confimied by Qt;,,,-,: 1.when no value is reported, see chlordane constituents 2.constituents or meta~ .... ~es of technical chlordane
-T~G~ --Sample 12911 FY 1997 Project: 97 -0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF Case Number: 25655
Id/Station: RCSE7
Media: SOIL D Number: MY70 Org Contractor: AA TS
RESULTS UNITS ANAL YTE
16U UG/KG CHLOROMETHANE
16U UG/KG BROMOMETHANE
16U UG/KG VINYL CHLORIDE
16U UG/KG CHLOROETHANE
30U UG/KG METHYLENE CHLORIDE
20U UG/KG ACETONE
16U UG/KG CARBON DISULFIDE
16U UG/KG 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
16U UG/KG 1, 1-DICHLOROETHANE
16U UG/KG 1,2-DICHLOROETHENE (TOTAL)
16U UG/KG CHLOROFORM
16U UG/KG 1,2-DICHLOROETHANE
16U UG/KG METHYL ETHYL KETONE
16U UG/KG 1, 1, 1-TRICHLOROETHANE
16U UG/KG CARBON TETRACHLORIDE
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97
Ending:
16U UG/KG BROMODICHLOROMET]Hf;l,A~N~EL _________________________ ---'----------------
----15u-uG/KG-1;2:DICHLORciPR-OPANE
16U UG/KG CIS-1,3-DICHLOROPROPENE
16U UG/KG TRICHLOROETHENE (TRICHLOROETHYLENE)
16U UG/KG DIBROMOCHLOROMETHANE
16U UG/KG 1,1.2-TRICHLOROETHANE
16U UG/KG BENZENE
16U UG/KG TRANS-1,3-DICHLOROPROPENE
16U UG/KG BROMOFORM
16U UG/KG METHYL ISOBUTYL KETONE
16U UG/KG METHYL BUTYL KETONE
16U UG/KG TETRACHLOROETHENE (TETRACHLOROETHYLENE)
16U UG/KG 1,1,2,2-TETRACHLOROETHANE
16U UG/KG TOLUENE
16U UG/KG CHLOROBENZENE
16U UG/KG ETHYL BENZENE
16U UG/KG STYRENE
16U UG/KG TOTAL XYLENES
38 % % MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K:actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12914 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE6
Media: SOIL
RESULTS UNITS
50JN UG/KG
ANALYTE
LIMONENE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY73
40J UG/KG 1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Re.questor: Rt>,. Y DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
K-actual value is 1.,, ··n to be less than value given. L-actual value is known to be greater than value 9!1• U-material was analyzed for but not detected. the number is the minimum quanti' 1 limit.
R-qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i: :ssary for verification.
r.-confirmed by gc.. ... 1.when no value is reported, see chlordane constituents 2.constituents or metab .... .-. ..:S of technical chlordane
-Sample 12914 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE6
Media: SOIL D Number: MY73 Org Contractor: AA TS
RES UL TS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
30U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
23 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: Denise Goddard
Requestor: RAY DOYLE --
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-rnaterial was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
f:-confirmed by Qcms: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
0 ...c:...
\
--Sample 12914 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE6
Media: SOIL
RESULTS UNITS
50JN UG/KG
ANALYTE
LIMONENE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY73
40J UG/KG 1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: John Mcconney
Requestor: RAY DQYLE _
Project Leader: DOYLE
Beginning: 08/24/97 10:00
Ending:
K-actual value is kr" . ., to be less than value given. L-actual value is known to be greater than value givr U-material was analyzed for but not detected. the number is the minimum quantil-·· , limit.
R-qc indicates tha: unusable. compound may or may not be present. resampling and reanalysis is ;sary for verification.
C-confirmed by gci;._ . ~·I.when no value is reported, see chlordane constituents 2.constituents or metabo ... -~ of technical chlordane
--E~EG-.,S-ATllllll,G,.. --~uc..,at.ii]i1119iiil49 -
Sample 12914 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE6
Media: SOIL D Number: MY73 Org Contractor. AA TS
RESULTS
13U
13U
13U
13U
30U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
23
UNITS
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UGIKG·
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UGIKG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
· DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 1 O:OO
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantltation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 13683 FY 1997 Project: 97-0357
_MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF _
Id/Station: RSCE5
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY69
700J UG/KG 4 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
K-actual value is ~-· . ., to be less than value given. L-actual value is known to be greater than value giv U-material was analyzed for but not detected. the number is the minimum quanti•· ·· ,., limit.
R-qc indicates th< unusable. compound may or may not be present. resampling and reanalysis j, :ssary for verification.
C-confirmed by gQ, ___ . 1.when no value is reported, see chlordane constituents 2.constituents or metab..:. .. c .... s of technical chlordane
_ Sample. 13683_ . FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RSCE5
Media: SOIL D Number: MY69 Org Contractor: AA TS
RESULTS UNITS
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
30U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
16J UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
20U UG/KG
50 %
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTALXYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
-Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~TILtiijAM1iiii1AN"i!ii'S ---E~E<WiilV 5i1ija ATliilllf>, G-- -Sample 13683 FY 1997 Project: 97-0357
MISC_ELLANEOUS COMPOUNDS .
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RSCE5
Media: SOIL
RES UL TS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY69
700J UG/KG 4 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requestor: AA Y DOYLE
Project leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
K-actual value is•· .... wn to be less than value given. L-actual value is known to be greater than valuer· .... U-material was analyzed for but not detected. the number is the minimum quar·· •:on limit.
R-qc indicates ti '.a unusable. compound may or may not be present. resampling and reanalysis :essary for verification.
C-confirmed by~---... : 1.when no value is reported. see chlordane constituents 2.constituents or meta .. _ .. ,es of technical chlordane
.... TIL..._..PJI ... NAlllls -
Sample 13683 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RSCE5
Media: SOIL D Number: MY69
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
RESULTS
20U
20U
20U
20U
20U
30U
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
ZOU
20U
16J
20U
20U
20U
ZOU
50
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Produced by: John Mcconney
-Requestor: RAY DOYLE ·
Project Leader: DOYLE
Beginning: 08/24/97 09:54
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
.... TILlll9\M~NAa!ll5 --Sample 12952 FY 1997
VOLATILE_$_ ~G_AN_.
Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34 Id/Station: RCSE4
Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
D Number: MY68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
13U UG/KG
13U UG/KG
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
6J UG/KG
13UJ UG/KG
23 %
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-0ICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
OIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-0ICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
Produced by: Denise Goddard
Requestor: RAY DOYLE_ ... _
Project leader: DOYLE
Beginning: 08/24/97 09: 15
Ending:
A-average value. NA_-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is_: ·n to be less than value given. L-actual value is known to be greater than value g· U-material was analyzed for but not detected. the number is the minimum quan'.. · '" limit.
R-qc indicates tt, .a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
,.... -r:onfirmed by Qai-,s: 1.when no value is reported, see chlordane constituents 2.constituents or metab1.,,1les of technical chlordane
--EPaiEGI., s957 a.n .. G,_ --Sample 12952 FY 1997 Project: 97-0357
-VOLATllES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34 Id/Station: RCSE4
Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
6J UG/KG
13UJ UG/KG
23 %
D Number: MY68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
. 1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-0ICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-0ICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOT AL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: John Mcconney
Requester: RAY _DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confinned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12951 FY 1997
VOLATILES sc_~N_ ----
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RSCE3
Project: 97-0357
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33
Media: SOIL D Number: MY67
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: MTS
12U
12U
12U
12U
20U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
15
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTALXYLENES
% MOISTURE
-11111f11nn' 'p-t'lllif2/~20 -
Produced by: Denise Goddard
Requestor: RAY f)OYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is y-·---,n to be less than value given. L-actual value is known to be greater than value g_;-U-material was analyzed for but not detected. the number is the minimum quant•'-'''"ln limit.
R-qc indicates U,1• ) unusable. compound may or may not be present. resampling and reanalysis: essary for verification.
C-confirmed by 9~-~.':i 1.when no value is reported, see chlordane constituents 2.COnstituents or metati-.-_. ... ~s of technical chlordane
Sample 12949
VOLATILES SCAN
FY 1997 -Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY31 Id/Station: RCSE1
Media: SOIL
RESULTS UNITS
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
SOU UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11U UG/KG
11UJ UG/KG
11UJ UG/KG
11UU UG/KG
11UJ UG/KG
10J UG/KG
11UJ UGIKG
11UJ UG/KG
11UJ UG/KG
2J UGIKG
11 %
D Number: MY65
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1. 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interierences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: John Mcconney
Requester. RAYDOYLE -
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
K-actual vatue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by Qcms: 1.when no value is reoorted. see chlordane constituents 2.constituents or mP.f;1hnlitP.~ nf tPr:hnir~I r.hlnrrfanP
--Sample 12949 FY 1997 Project: 97-0357
--VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY31 Id/Station: RCSE1
Media: SOIL
RESULTS
11U
11U
11U
11U
11U sou
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11U
11 U
11U
11U
11U
11U
11UJ
11UJ
11UU
11UJ
10J
11UJ
11UJ
11UJ
2J
11
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MY65
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE}
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL}
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE}
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE}
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: John Mcconney
·Requester: RAY DOYLE -
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
---PA ...,IOllllll;ES-HE .. A --Sample 12949 FY 1997 Project: 97-0357
__ MISCELLANEOUS COMPOUNDS ---~ - --
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY31 Id/Station: RCSE1
Media: SOIL
RESULTS UNITS
60JN UG/KG
10JN UGIKG
300J UG/KG
D Number: MY65
ANALYTE
PINENE ISOMER
3THYLDIMETHYLBENZENE
3 UNIDENTIFIED COMPOUNDS
lnorg Contractor: ARI
Org Contractor: AA TS
Produced by: John Mcconney
-Requestor: RAY DOYLE ----
Project Leader: DOYLE
_ Beginning: 08124197 08:05
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is i,.~ -·vn to be less than value given. L-actual value is known to be greater than value gi• -LI-material was analyzed for but not detected. the number is the minimum quan• .. ·="ln limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis · essary for verification.
C-confirmed by g__ • 1.when no value is reported, see chlordane constituents 2.constituents or metaL __ ..!S of technical chlordane
-
--Sample 12950 FY 1997 Project: 97-0357
-VOLATllES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY32 Id/Station: RCSE2
Media: SOIL
RESULTS UNITS
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
20U UG/KG
12U UG/KG
12U UGIKG
12U UGIKG
12U UG/KG
12U UG/KG
12U UGIKG
12U UGIKG
12U UG/KG
12U UG/KG
12U UG/KG
12U UGIKG
12U UG/KG
12U UG/KG
12U UG/KG
12U UGIKG
12U UGIKG
12U UG/KG
12U UG/KG
12U UGIKG
12U UG/KG
12U UGIKG
12U UG/KG
12U UG/KG
12U UGIKG
12U UG/KG
12U UG/KG
12U UGIKG
12U UGIKG
14 %
D Number: MY66
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1.1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1.1.2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
-Produced by: John Mcconney _
-Requestor: RAY DOYLE---
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-materia1 was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
VO--ES-PL~Lvallll -Sample 12950 FY 1997 Project: 97-0357
VOLATILESSCAN -------
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE2 MD Number: MY32
Media: SOIL D Number: MY66
RESULTS UNITS
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
20U UG/KG
12U UG/KG
12U UG/KG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
12U UG/KG
12U UG/KG
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
14 %
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
Produced by: Denise Goddard
_Re_qu_estor:_RAY_ DOYLE __
Project Leader: DOYLE
Beginning: 08/24/97 08:22
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. ·
K-actual value is'· vn to be less than value given. L-actual value is known to be greater than value~,; • U-material was analyzed for but not detected. the number is the minimum quani:..-•;'ln limit.
R-qc indicates H: a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
C-confirmed by 91....,J: 1.when no value is reported, see chlordane constituents 2.constituents or meta1..~ ... es of technical chlordane
-
Sample 12951
VOLATILES SCAN
--FY 1997 Project: 97-0357
-----------------
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33 Id/Station: RSCE3
Media: SOIL
RESULTS UNITS
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
20U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
12U UG/KG
15 %
D Number: MY67
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: John Mcconney
-Requestor:-RAY-DOYLE------
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
K-actual value is known to be less than value given. L-actuat value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
-Sample 12951 FY 1997 Project: 97-0357
_ _VOLATILES SCAN -------
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33 Id/Station: RSCE3
Media: SOIL
RESULTS
12U
12U
12U
12U
20U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
12U
15
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MY67
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: MTS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
Produced by: Denise Goddard
----Requestor:-RAYDOYlE --
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is t-·•n to be less than value given. L-actual value is known to be greater than value ff U-material was analyzed for but not detected. the number is the minimum quant:• · ",n limit.
R-qc indicates tti J unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification.
C-confirrned by gr.., __ .,: 1.when no value is reported, see chlordane constituents 2.COnstituents or metaL...-: ~s of technical chlordane
-
vm-Es "'PLi=.ia.L vWIII --Sample 12952 FY 1997 Project: 97-0357
VOLATILES SCAN
-----------~ --Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34
Program: NSF
Id/Station: RCSE4
Media: SOIL
RESULTS UNITS
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13U UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
13UJ UG/KG
6J UG/KG
13UJ UG/KG
23 %
D Number: MY68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
-1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
-Produced by: John McConney
____ R~~ll_~§tor: RAY DOYLE _ _ ---- --
Project Leader: DOYLE
Beginning: 08/24/97 09: 15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates. that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituentS or metabolites of technical chlordane
-
VO~ES-PL~L""" --Sample 12952 FY 1997 Project: 97-0357
VOLATILES SCAN
--Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34 Id/Station: RCSE4
Media: SOIL
RESULTS
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13U
13UJ
13UJ
13UJ
13UJ
13UJ
13UJ
13UJ
6J
13UJ
23
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MY68
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-0ICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Produced by: Denise Goddard
_!~equestor:_RAY DOYLE------
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is· ·n to be less than value given. L-actual value is known to be greater than value p· U-material was analyzed for but not detected. the number is the minimum quan' .. ·1n limit.
R-qc indicates tt, .a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
,... -confirmed by gcrns': 1.when no value is reported, see chlordane constituents 2.constituents or metabva,es of technical chlordane
\WliTILIM\M"iiltNA~ --Sample 12925 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: .B~SO_R_CHEMICAL------CASTLE HAYNE; NC -------
---Program: NSF Case Number: 25655
Id/Station: RCSE20
Media: SOIL
RESULTS UNITS
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
14U UG/KG
40U UG/KG
14U UG/KG
14U UGIKG
14U UG/KG
14U UG/KG
14U UG/KG
14U UGIKG
14U UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UG/KG
14UJ UGIKG
14UJ UGIKG
14UJ UG/KG
30J UG/KG
14UJ UG/KG
26 %
D Number: MY87
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: MTS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
-Produced by: Denise Goddard
Requestor: RAY DOYLE
-Project Leader. DOYLE ___ ----
Beginning: 08125197 16:20
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is} n to be less than value given. L-actual value is known to be greater than value g: U-material was analyzed for but not detected. the number is the minimum quanf" · .... n limit.
R-qc indicates th<_ J unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification.
r:-r:onfirmed by go .. .,: 1.when no value is reported, see chlordane constituents 2.constituents or metabv .. les of technical chlordane
-

-
Sample -12925 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSE20
Media: SOIL
RESULTS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY87
9JN UG/KG
60J UG/KG
METHYL (METHYL ETHYL) BENZENE
2 UNIDENTIFIED COMPOUNDS
-
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presurnptive evidence of presence of material.
--Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE-----
Beginning: 08/25/97 16:20
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-col'}firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
~C-·"'S-PL~LY--Sample 12925 FY 1997 Project: 97-0357
___ MISCELLANEO_US_COMl'OUNDS_. _______ ~ ---
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE20
Media: SOIL
RESULTS UNITS
600JN UG/KG
5000J UG/KG
2000JN UG/KG
500JN UG/KG
300JN UG/KG
500JN UG/KG
500JN UG/KG
300JN UG/KG
700JN UG/KG
200JN UG/KG
3000JN UG/KG
6000J UG/KG
D Number: MY87 Org Contractor: MTS
ANALYTE
PINENE ISOMER
ALKANES
CARYOPHYLLENE
HEXAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
TETRAHYDRODIMETHYL(METHYLETHYL) NAPHTHALENE
CARYOPHYLLENE OXIDE
COPAENE
DIMETHYL(METHYLETHYL)NAPHTHALENE
CARBOXYLIC ACIDS
SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID
CINNAMYL CINNAMATE
6 UNIDENTIFIED COMPOUNDS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
- -
~e,..Dat-"~'-:50 -
Produced by: Denise Goddard
__ Requestor: RAY_[)OYLE ____ .
Project Leader. DOYLE
Beginning: 08/25/97 16:20
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12932 FY 1997 Project: 97-0357·
VOLATILES SCAN
_ Facility· REASOR CHEMICAL-·---· CASTLE HAYNE~NC
Program: NSF Case Number: 25655
Id/Station: RCSE21
Produced by: Denise Goddard
Requestor: RAY DOYLE
--· ----·---Project l:eader: DOYLE~· ---
Beginning: 08/25/97 15:35
Ending:
Media: SOIL 0 Number: MY94 Org Contractor: AA TS
RESULTS
26U
26U
26U
26U
26U
140U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26UJ
26UJ
26UJ
26UJ
460J
26UJ
26UJ
26UJ
26UJ
61
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE}
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL}
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE}
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE}
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kr-·•'" to be less than value given. L-actual value is known to be greater than value gi•·· U-material was analyzed for but not detected. the number is the minimum quanti• · 1 limit.
R-qc indicates the unusable. compound may or may not be present. resampling and reanalysis i: :ssary for verification.
C-confinned by gc..-,."·'· --·1.when no value is reported, see chlordane constituents 2.constituents or metab\,... __ ..,s of technical chlordane
--Ei=-.EGall\/S-AT ... ,G .... --lllladuc..,_:>at'liii11 /9iiii49 -
Sample 12932 FY 1997 Project: 97-0357
_____ _r,1ISCELLANEOUS COMPOUNDS ___________ _
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE21
Media: SOIL
RESULTS UNITS
600JN UG/KG
200JN UG/KG
30J UG/KG
D Number: MY94
ANALYTE
PINENE ISOMER
METHYL(METHYLETHYWBENZENE
1 UNIDENTIFIED COMPOUND
Produced by: John McConney
Requester: RAY DOYLE
---~-Project Leader: DOYLE --· -------
Beginning: 08/25/97 15:35
Ending:
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verffication.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12933 FY 1997 Project: 97-0357
VOLATILES SCAN ---------------------------------FaciITty'. REASOR CHEMICAL
Program: NSF
Id/Station: RCSE22
Media: SOIL
RESULTS UNITS
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
140U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
42 UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
38U UG/KG
74 %
~
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY95
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
D1BROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
%MOISTURE
- -Produced by: John Mcconney
Requestor: RAY DOYLE
---Project leader: DOYLE -~---
Beginning: 08/25/97 17:10
Ending:
------------------
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-adual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatio·n limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 12932 FY 1997 Project: 97-0357 --Produced by: John Mcconney
Requester: RAY DOYLE
VOLATILES SCAN
-___ F'acility:_REASOR CHEMICAL-----GASTtE HAYNE~Nc---
-----___________ ------Project leader: DOYLE -----------
Program: NSF Case Number: 25655
Id/Station: RCSE21
Media: SOIL
RESULTS
26U
26U
26U
26U
26U
140U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26U
26UJ
26UJ
26UJ
26UJ
460J
26UJ
26UJ
26UJ
26UJ
61
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MY94
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
Beginning: 08/25/97 15:35
Ending:
-----
A-average value. NA-not analyzed. NAl-interferences. ·J-estimated value. N-presumptive evidence of presence of material.
K-actual value is ~ -· ·vn to be less than value given. L-actual value is known to be greater than value giv~... U-material was analyzed for but not detected. the number is the minimum quantit:ation limit.
R-qc indicates th 1 unusable. compound may or may not be present. resampling and reanalysis ; :!Ssary for verification.
C-confirmed by 91.... . .. · 1.when no value is reported, see chlordane constitue,nts 2.constituents or metaL _ · .;S of technical chlordane
-Sample 12932 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility:-REASOR CHEMICAL
Program: NSF
Id/Station: RCSE21
Media: SOIL
RESULTS UNITS
600JN UG/KG
ANALYTE
PINENE ISOMER
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY94
200JN UG/KG
30J UG/KG
METHYL (METHYL ETHYL) BENZENE
1 UNIDENTIFIED COMPOUND
--111111111en11ifate11if21911i111120 -
------------
Produced by: Denise Goddard
Requestor: RAY DOYLE
--~ -~ --Project Leader:-DOYLE----~ -----
Beginning: 08/25/97 15:35
Ending:
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification:
C-confirmed by gems: 1.when no value is reported. see chlordane constituents 2.constituents or metabolites of technical chlordane
Sample 12933 FY 1997
VOLATILES SCAN
Project: 97-0357
-----------------·
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
Id/Station: RCSE22
Media: SOIL
RESULTS
38U
38U
38U
38U
38U
140U
38U
38U
38U
38U
38U
38U
42
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
38U
74
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
D Number: MY95
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requester: RAY DOYLE
Project Leader. DOYLE ____ --~-~--
Beginning: 08/25/97 17: 10
Ending:
K-actual value is.' -·•n to be less than value given. L-actual value is known to be greater than value p' U-material was analyzed for but not detected. the number is the minimum quar,. '''>n limit.
R-qc indicates tt,_ a unusable. compound may or may not be present. resampling and reanalysis essary for verification.
r.-confrrmed by g·._ __ .;c.,: 1.when no value is reported, see chlordane constituents 2.constituents or metal.~ ..• es of technical chlordane
-- -
--R~ 1v.a:i, A~S, ..
Sample 12949 "FY 1997 Project: 97-0357
METALS SCAN ---~ --------------------· ---~ --------Facility:-REASORCHEMICAL -CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSE1 MD Number: MY31
Media: SOIL D Number: MY65
RES UL TS UNITS
0.67U MG/KG
0.22UJ MG/KG
3.1 MG/KG
0.22U MG/KG
0.44U MG/KG
0.67U MG/KG
1.9J MG/KG
0.44U MG/KG
2.2U MG/KG
5.1J MG/KG
20UR MG/KG
1UJ MG/KG
0.22U MG/KG
2.7J MG/KG
0.89U MG/KG
0.06U MG/KG
1100J MG/KG
3.9J MG/KG
.. 20U MG/KG
30UJ MG/KG
450 MG/KG
20U MG/KG
120U MG/KG
12 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: ARI
Org Contractor: AATS
A-average value. NA-not analyzed, NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Keith Bates
R_e_g~e_s_t9r:_~AY DOYLE ________ ----------~ --------
Project Leader: DOYLE
Beginning: 08/24/97 08:05
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indic_ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value ls reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--Sample 12950 FY 1997 Project: 97-0357
METALS SCAN
___ facility: REASOR.CHEMICAL----CASRE·HAYNE~NC
Program: NSF Case Number: 25655
Id/Station: RCSE2 MD Number: MY32
Media: SOIL D Number: MY66
RESULTS UNITS
0.68U MG/KG
0.23UJ MG/KG
2 MG/KG
0.23U MG/KG
0.46U MG/KG
0.68U MG/KG
1.7J MG/KG
0.46U MG/KG
2.3U MG/KG
2.8J MG/KG
20UR MG/KG
1UJ MG/KG
0.23U MG/KG
2.5J MG/KG
0.91U MG/KG
0.05U MG/KG
1400J MG/KG
2J MG/KG
· 60U MG/KG
20UJ MG/KG
880 MG/KG
20U MG/KG
120U MG/KG
14 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM·
ZINC
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
%MOISTURE
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material,
--Produced by: Keith Bates
Requester: RAY DOYLE
___ f'rojectLeader: DOYLE--~---
Beginning: 08/24/97 08:22
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R..qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value Is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
---E~E~IV S.-AT..,, G--Sample 12951 FY 1997 Project: 97-0357
METALS SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RSCE3
Media: SOIL
RESULTS UNITS ANALYTE
0.64U MG/KG SILVER
1UJ MG/KG ARSENIC -
7.2 MG/KG BARIUM
0.21U MG/KG BERYLLIUM
0.43U MG/KG CADMIUM
0.64U MG/KG COBALT
3.6 MG/KG CHROMIUM
2U MG/KG COPPER
2.1U MG/KG NICKEL
6.2J MG/KG LEAD
20UR MG/KG ANTIMONY
0.22UR MG/KG SELENIUM
0.22U MG/KG THALLIUM
4.1J MG/KG VANADIUM
7.5 MG/KG ZINC
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY33
D Number: MY67
0.05U MG/KG TOTAL MERCURY
2300J MG/KG ALUMINUM
12J MG/KG MANGANESE ,--;--~=-. ,, 1600 MG/KG CALCIUM
130J MG/KG MAGNESIUM
100 MG/KG IRON
20U MG/KG SODIUM
110J MG/KG POTASSIUM
10 % % MOISTURE
lnorg Contractor: ARI
Org Contractor: AATS
·-:i.lue. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 08:50
Ending:
·:,;known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitalion limit.
• data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
·· 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--Sample 12952 FY 1997
METALS SCAN
Project: 97-0357
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY34 Id/Station: RCSE4
Media: SOIL
RESULTS UNITS
0.77U MG/KG
1UJ MG/KG
12 MG/KG
0.26U MG/KG
0.51U MG/KG
0.77U MG/KG
5.8 MG/KG
2U MG/KG
2.6U MG/KG
7.9J MG/KG
20UR MG/KG
0.26UR MG/KG
0.26U MG/KG
6.4J MG/KG
10 MG/KG
0.07U MG/KG
4400J MG/KG
13J MG/KG
3300 MG/KG
250J MG/KG
1700 MG/KG
13 MG/KG
180J MG/KG
23 %
ANALYTE
SILVER
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
NICKEL
LEAD
ANTIMONY
SELENIUM
THALLIUM
VANADIUM
ZINC
D Number: MY68
TOTAL MERCURY
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
% MOISTURE
lnorg Contractor: ARI
Org Contractor: AA TS
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
-Produced by: Keith Bates
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 09:15
Ending:
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
I
I
I
I
I
I
I
I
I
I
I
I
I
I
1 ..
I
RE.lliSO~ CHEMJC/-IL
GP 10: ;saa17c-o3a
Cticnt !D: RCSE25
I Cwllectcd; 08/18.'98
l)i L.Jtion; \00
P.:irameter
bis ( 2-c, toroeth)"l )::th~r
Phenol
' 2 • Ch 1, oropf,enc-l
1,3-0i=hlooobe~z~nc
i ,!.-Oichlor::ibc:nzer,e
·,, 2-Di ch l orobcnzi:-ne
2, 2' -,:,;,,;ybi ~( 1 -ch\ .:iropropnne)
2-Mcti-iylph<;:nol
Hexacn :c,f\)C-rnane
~-IJ i trc~o-di -r,-propy L arni m:
41-~(:thy\phenol
Nitrobenzcn1.:
l::.~;,h.:>rC'lne
2-Nitro.:ih<..-nol
2,t.-Oir:icthylphenc\
bl s (2 • Ch l oro::thcJ,y }!ll~thane
2, l,-D i ch lorooi"-,cnol
I 1,2,4-Trichlorcbenz~n~
,"1aph th al enc
4-Ch l orcani t i_nc
Hexachl::robutac.Jie~
'4 ·Chi ore· 3-rrx . .'tl':ylpr,enol
2·Mc~hylnecht~alenc
He~ac~torccyclopent~c,ene
2,,,6-Tricrlcrop~~nol
2,➔,5·T~ic~lorophenol
2 • Ch l,-;;onaph thal ene
.2·.~i troar.i l inc
Accnoph thy l en~
Di 111ethylphtha: 2te
2, 6-D i rl ":rot c,\ 1.Jene
,A.ccnl.ipnthene
GP E:-.VIRO~l!ENTAL
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
Matrix: SEDI~ENl
~ethod: SU8G.6 827:JC
L'ni r.s: 1.Jg/Kg
SEMI\'OL,r.,TJLE TARGET COMPOONOS
Ret;Ult Rcp.~irn.
B0L 2s0000
BCl. 250000
£1:CL. 110000
BCL 2100cc
BOL 250000
so, 110000
BOL 150000
SOL 110:,00
5~'... 250000
f;;:JI. 250000
SOL 150000
3,CL 250000
BCL 2S0000
BQL 2socoa
SOL zscooo
SOL 2S0000
BOL 250000
80!. 2soooo
BOL 2500C□
SOL 250000
6Cl. 250000
SOL 250COO
SOL 250000
SOL 250000
aaL 250)00
BOL 12CJCOCJ
BOL 250000
BOL 1200000
OOL 210000
SOL 25 0000
BCL 210000
BOL 250000
Ar,aky$t: M~
An3ly:e~: U0/03/9G
Prc~-uri.:-d:
cu~l i ficr
~008
6
.:_:~~'::::·:.:•:•
,,~tW',1i)/J.9/ 10: 98 THU lJ: H F.-1.l:_ JOl HO 1209
i ,.,.l~lii'.:r#.i:4-'°!~· .• i .·
GP Pff IRO)(JIE:,/T.-\L
' I
-~Project: RE~SOR CHEMICAL 11
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GP 10: 980817b·U~8
Client JO: R:SE'.25
C◊llected: oa/18/98
Diluticr.: 1C0
3-Nitroan·:t.inc:
2,4-Dinitroi:r,enol
Dibcn:zofuran
2,t.-o·ini trotcluene
4-Ni trophc-noL
fluorene
4-Ch\o;opt,enyl·phcnylether
Di ct:hytph th Al :ate
.:.-t-1i:,-o.:>niLine
4, t:·O i ni tro-2-rr~tl"'. yl ~enol
N-n it r::isc.d i phcfffl mni ne
:.-Bromoph•.:nyl • pherwl ether
lte,.ach I crob:=nzcnc
Pcnt~chlarophenol
Phenanthrene
An:hracene
Curb:H:s)le
di ·n· Buty1. or. ~h 3 late
1 Fluor,nthene
Pyrcm..'
SutylbenzytphthJtate
1 3,3 1-Dir.hlorobE::nzidine
1 8ento~~Janthrnc~ne
ChrYS➔/"'il
1 bi::.~2-Et/":y\ne;w~)phthalo-::c
1 di ·n-Oc:tyl pri th3\iite
acnzor:J fl uor.a:-.thcne
Benz;o(\G fl\;ol"'a~th~nc,
s~n;:o (a) pyrcne
!ndcno(1,2,3·:d]pyrene
1 Dibenz (a,hl anthl"'acene
'Be:'"'.2,0[9,h, i]pe~ylene
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
Matri~: SEOlM~NT
Method~ SW8L6 827GC
Uni U: ug/K9
SF.~IVOLAHLE TARC.F.T COMPOJNDS
Resi..:l t Rep. L ini.
BOL : 2o□oco
sot 1200000
BOL 250000
BOL 250000
COL 1200000
BOL 250000
BOL 250000
BOL 25GO!JO
AOL i200000
BOL 1200000
BOL 250000
SOL 250000
BOL 250000
BOL 1200000
BOL 250000
BOL 250000
BOL 250C00
SOL 250000
BOL :zsoooo
BCL 250000
QOL 250000
BOL G90000
BOL 250000
BOL 250000
BOL 2'50000
SOL 250000
SOL 250000
SOL 2SOOOC
SOL 250000
SOL 250000
BOL 210000
BOL 250000
Ar-~lyst: MN
Analy-zcd; 09/03/98
t:1repared:
O•;al ificr
Page
~009
7
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11
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Project:•REASOR CH=MICAL
GP iD: 980S176·03A
Cli~nt to: RCSE25
Col tec~ed: 08/18/Q8
Di l•.1t iQn: :Z
~<!rarneter
Chloroo,echane
Br·crr.ometh:,ne
Vinyl chloride:
Chlcroerhane
Methylene ch lar ide
Acetone
Carbon Di~u(f'idP.
\, 1-Dichlcroethene
1, ·,•Di chi or~.:th<..inc.'
1, 2-0 i ch l oroethll!!"',e( total )
Chloroform
1,2-Dichloroethan~
2·llL..:tanonc!:
1, i, l·TrichloroetMne
C~rbon t~truchloridc
Sromcdi ch l □rometham:
1, 2-D i ch l oroprora~e
c is-1 , 3 · Di ch l or□propent!
Trichloroethene
Benz.em~
Dibrornochloromethane
lr..ins•l,3·oichlcroprcpene
1, 1,2-Trichlorocthanc
Sromotorr.i
l-Mcth yl · 2-pcn:.:inonc
2-Heitanone
Tetro ch l oroeH,ene
1 ,,,,2,2-retr~chlorocthone
lotL:ene
ct, to:-::i~n2.c:ic
Ethvtbenzen2
Styrene:
I )(y[ene-(tct.al)
GPL LABORP.TORIES, LLLP
ORGANIC ANALYSIS RESULTS
H~trix: SEDIMENT
Me:hoo: SU846 S260B
Units: us/P::g
VOLA.rll.E 'rARCET COMPOWJOS
fl'c:sul t Rcp.L im.
SaL 3700
OOL 3700
SQL 3700
3QL 3700
BOL 1900
BQl. 3700
BQL 1900
SOL 1900
SOL lQOO
SOL 1900
SOL 1t;'OO
SOL 190C
SOL 3700
SOL 1900
SOL 1900
SOL 1900
SOL 1900
SOL 1900
QQL 19u0
BQ!. 19C0
80!. 1900
BOL 1900
QCL 1900
SOL 1900
QDL 3700
OOL 3700
B::L 1,00
BOL 1900
29000 1900
SOL 1900
440 1900
BCL 1900
1200 ~900
Analys:: AD
An~lyzcd: 08/31/98
Prepared:
cu.:il ificr
Page 20
~
;-·;, '
"."t• ,.. •• , ___ ,
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li.t' t:."iY lKU.'lM...1::.l'iT:\L
TL! Project:
Client Sample:
46551
9808176-0JC=RCS E25
Method 8280-A PCDD/PCDF Analysis (b)
Analysis File: VI10700
! Clicnl Prujccl:
i S:1mr1c :vi~u·ix:
! TLI ID:
i .Somrk Size:
: Dry W~igilL:
I (·r· , .. I .1 ... ,\..1: umn:
. ' . Ana.lytes-:
2 .. ;. i ,K:1·( ~DD
l.2 .. i. 7 .. 'i-1'..:CDD
t .: . .t-i.: _;-;.1 i.~cun
1.2 .. \./,. 7 .,<. I Ix( '1)1)
t .2 .. t 7 .. ,:,1.J-l [~( '.DD
1.2 .. ,.l.!1.7.~-I lrCDD
1.2 .. ~.-!Ji. 7.s.;;.c JCDD
~ --~-7 --~--!'('DI:
\ .2.3. 7.~-l't.:C ])~:
~-?--L ,.:-:-t)L,(T)F
\ .. ":..:A.; .:..:.1 hCL>I-:
1.:.3,fo 7 .:~-[ tx:.11F
:::J.4_(1:7 .~-T-LxCD!.:
l .1.3. 7;,;,;_1J-( b:l~DF
1.2 . .1.~:.(,.7.S-HpCDI'
1.2.3.4.7 .:(1J-l TrC0r-
l .2.j.~.6.7 .i\.1J-OCDF
·Tat nls :·,, 1· ...
T,>t:d TCDD
r,,lal PcCD!::>
T.-,l:il HxC:DJ)
·i·()t:tl UpCDD
T111al TC!)['
T,il:li PcCDF
Total I t,CDr-
T,,l:il llpCDI'
'
Dioxin in sediment
SEDIMENT
216-56-3
10.000 g
7.870 g
DB-5
:•m
ND
Nu
ND
ND
ND
NJ)
ND
ND
ND
ND
ND
NU
ND
~1)
ND
NT>
ND
ND
ND
i','D
ND
ND
Tri,mgl~ Laboratories, lnc.:.1
Date Received: 08/25/98
Date Extracted: 08/26/98
Date Analyzed: 09/01/98
Dilution Factor: n/a
Blank File: V[10100
Analyst: DD
0.05
a.ox
0. l
(l.l
0.1
0.2
0.8
0.04
0.05
OJJ5
G.l
0.1
0.1
O.l
0.2
0.3
0.6
0
0 008
0 0.1
0 0.'.2
0
0 0.05
0 0.1
0 0.2
P~ge 1 oi 2
801 Capilcla Drive • Durh&m, North Carolina 27713
Phone: (919) 5,.4.5729 • Fax: [phone]
Spike File: SP828A50
!Cal: V85822A
ConCal: VI09700
% Moisture: 21.3
% Lipid: n/a
% Solids: 78.7
2.0
0.0S
9/03/98
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TL! Project:
Clien,t Sample:
Cii·.:n1. .Pwject:
Sumrk \-!Jtrix:
TU !D:
·1 Sampk Size:
Dr\' W.:i ~ht: i GC C<ilu~nn:
1 · I Analytes
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2..3.7.:~-T< 'DD
1.c .. i. "-~-I'd 'DI)
1.2.\-l. 7 -~ -I I, (''.J'.)
1.:. 3.6. 7 .:<-H "_-1)1)
1 .~.).-; .. ~. lJ. i1.,c DI)
:.:..:.3 . ..;..6.7 . .'i•Hrc :De
! .2 . .1.➔.C".; .:.::~1-( >CDU
::.J.-L6.~ -~ -f-f\c ·u1:
\ .2.\":.,'\.'J-HxCI .>!:
1.2 .. :..--1.('I_ 1 .-~-Hrl "UF
l .1.3.-L7 _:-,:_ 1)-Hr('DF
1.2 .. ~.➔.fl. :. ~-o:( )('DF
46551
9808176-03C=RCSE25
Dioxin in sediment
SEDIMENT Date Received: 08/25/98 216-56-3 Date Extracted: 08/26/98
Date Analyzed: 09/01/98
10.000 g
7.870 g
DB-5
.. . ... ,
Dilution Factor:
Blank File:
Analyst:
1
VI10100
DD
> .• Cone. (ppb)(f :, .L'\TEF,
ND X 1. = ND X 0.5 = ND X 0 l = ND X 0.l = ND X O.l = :,iD X O.DI = ND X 0.001 =
:-sn X 0.1 = ND X 0.05 = ND X 0.5 = ND X 0.1 = ND X O.l = :-.u X 0.1 = ND X 0.1 = ND X 001 = ND X O.Dl = ND X 0.001 =
Toxicity Equivalents Report
Analysis File: V110700
Spike File:
ICal:
ConCal:
% Moisture:
% Lipid:
% Solids:
SP828A50
V85822A
Vl09700
21.3
n/a
78.7
i Total 2,3,7,B-TCDD Toxicity (1989 ITF) Equivalents: 0. ppb I
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(1) Detection ~imits not used in calculations. Nata: 100% of cMPCs are used in the calculations.
I Triangle Laboratories, Inc.,
801 Ca;:,itola Driv~ • Durham, North Carolina 2TT13 I Phone [phone] • Fax: [phone]
Page I of 1
Printed: 15:24 09/03/98,
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09no,gs THU 13: 41 F.U 301 8~0 1209 GP ENVIRO'.>J!E:'<TAL
. -,•t;ij ect: REA!:3R CHeMl CAI.
: '
Gf'..' li): 0803176-048
Cl iem 10: RCSE26
CollecrE=d~ 08/laii:>8
Di lutlon:
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
~Jtrix: SE~lMfijf
Method: SU£l46 8270C
Unit::.: ug/Kg
SEM:i'JOLAll LE TA.RG~T COMPO.mos
AnJlyst: NM
Analyz.eCI: 09/04/98
Prepared:
P.:ir-11mec:.5e-'-c ______________ _,'-'-'"'-'·'-------"="'-'-'-'"'-·-----="-'-'-'-'"'-'-Re~wlt Rep.Lim. Quflt ifi=r
b 1 ~( 2-Ch l o,oerr,yt )er~er
Fhe-nol
2-C!'llorophenol
1 ,:S-Dichlorc~nzcoc
1,4-0ichlorobenzene
1,2-0ichlor~C<.·nzene
2,2' -oxybi!':( 1 ·ct-.lcropropanc/
2-Mcthylpt:enoL
~exach lot oc:tnrme
N-tn tr-:iso·di -n· propyl amine
4-Mettiv l ptn.•n')l
t.J i trotcr.zene
!!;apl,on,ne
2-Mi'°.roohcnol
2.~·Dimethylphcnol
bi~{ 2-Ch l.orcctho.-.y )methane
2, 4 ·O i ch t orophen::: l
1,2,4-Tr~chlorobcn~en~
N.:i;,hthale~
4·Chloi-oani l ir.c
Heu ch l or:)t.ut od i enl"
4-Chtaro-3-mctnylpnenol
2-Methyl napht nal.~ru.:
Hex.ad, Lor•;,.cyc l a~nl:tidi ene
2, {,., 6-Tr ich ! :iropheno\
2, 4, 5-Tt i ch l orophel"\O \
2·Chloronaphth~lene
2-~1itroor.ili11e
1 Ac~nai:)-. thyl cnt
1 Dimcthylpt:!hal~t~
2,$-Dini tro':"ol"Jerie
ACcrt3ph th1mc
SOL 5:0
BOL 510
SOL 510
SOL 510
SOL 5i0
SOL 510
SOL 5~0
SOL 510
BOL 510
SOL S1C
SOL )10
Bal 510
BOL 510
SOL 510
BQL s:o
SOL 510
BOL 510
Bot 510
BOL 510
BQL 510
SOL 510
BOL s:o
B:Jl 510
SOL 510
BDL 510
BOL 2600
BOL 110
BOL 2600
BOL 510
BOL 510
BQL 510
BOL 510
1iD010
I
/".'.'toject! REASOR CH'i:.MICAL • ··)
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GP tC, 9808116·046
r.~ le.rit IC: RCSi:26
col lectcd: 08/78/98
Di lt.:tivn:
3-Nitraanlline
2,4-0initrophcnol
L· 1 be:-.i.ofunm
?.,G-Dinitrotolucnc
· 4->,1itroph~cl
fl woren,.::
4-Chlorophenyl-phenylcthcr
0 i e-thyl pl, thJ t .'.l(e
G-.>,1itrol'lniline
l.., 6-D in it ro-2-mc:thy lphenct
N-nitrasodichenylamine
4-BrO'.l'IOphenyl-phenylether
He~achlorobe~zene
1 PentRc:h l orodH::no l
Phe~.:inth rene
~nt:iir.iccnc
curb-:no\ e
di -n-6uryl pl-: tnu L .:Jt e
F luor,mihene
Pyr@nit
Butyl bcnzyl pl tha late
3,3 1-Dichlorobenzidinc
Bcr.:o Lil ant ti r.)cene
Chry£.cr:c
bis ( 2-Ethy lhcxyt )pltha lute
di-n-Octylphthula~e
' Benz.o{b1 fluor;inthcnc
1 Bcnz.o [k) 1 l uor~ntt,e"lc
'Ben:!o[a".lpyrenc:
• Jndeno(1,2,3-cd]pyrcne
' O ibcnz [a, hJ un?:hr11:::ene
1 Be-.z:0{9,h, iloerylcne
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
M~tria: SEOlMEijT
M~tho□: 5~8~6 827GC
Unit~: ug/(g
SEMI VOlAT I LE T .\RGET COl":.POUIJDS
Resu\ t Rep.Lim.
3CL 2600
BQL 2600
SOL 510
SOL 510
BCL 2600
BQL ~10
SOL 510
BCL 510
BCL 2600
BOL 2600
BOL 510
BCL 510
BOL 510
SO! 2500,.
BOL 510
BQL 510
BOL 510
BOL 510
BCL 510
BOL 510
BCL 510
BQL 1000
BCL 510
BCL 510
BOL 510
SOL 510
BOL 510
BOL 510
BCL 510
BCL 510
BOL 510
BCL 510
Analyst: NM
Analyzed: 09/0l/98
Prepared:
Oualitier
lg)Ull
Page 9
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GP JD: 9806176-{}/,A
Client ID'. RCSE26
:ollect!:'d: 08/16/98
Oilutli:n:
Parameter
Cht~romethane
oromomcth.in-:-
Viny', chlcr\de
Chtaroethane
MC'thylcr-.c Ch lor idi::
Acetone
C;1r:J~n Di.sulfide
1, i ·Dic-,'1lorocthcn~
1, l·Dichlorocthane
1,2-DicnlorGethene{TotJl)
l.h toroform
1,2-Dichlor0eth~ne
2·Elutancne
1, 1, i -Tri ch! or.::icth.ine
Carbon !€'tracf1~::ride
6romaCi~hloromeThane
l,2·Dichlo~~pro~ne
ci~-1,3-Dich\oropropene
Tri ch Loroeth,me
Benzene
DibroTioc~ior~metha~e
t ra.ns-1, 3 ·Di ch l cr·,propenc
1, 1,2-lrichloroethane
9romoform
4-Metnyt-2-penta~one
2 · He ... anone
r ctr.:ch l or(;(: then(:
1, 1,?.,2·Tt!trnch',oroetha,'"le
1 oluene
C~ l orc,bcn::c:ic
E th·fl benzer;e
, S tyr(::ne
·,ylcnc (tot.JI>
GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
MJtrix: SEDIMENT
Method: SU81,6 82608
Unit!.'. ug/k'.g
VOLATILE TARGET CCNPOUNDS
Resut t Rep.Lim.
BOL 15
BQL 15
BOL 15
BOL 15
8 8
80L 15
BOL B
EIOl., 8
aoL 8
BOL ' BOL 8
BOL 8
BOL 15
BOL 8
BOL 8
:30L 8
BOL 8
30L 8
aaL 8
BOL B
BOL 8
BOL B
SOL 8
BQL 8
SCL 15
BOL 15
SOL 8
BOL 8
30L 8
BOL 8
SOL 8
BDL 8
SOL 8
An.3lyst; JAH
An.ilyzcd: 08/31/98,
Prepared:
Qu;,:il ific1·
Pagr: 21
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u~•l.v.:t," lQLI .1J:-.l1 i':\..\. JV.i. 11,-!U J.lll~
TL! Project:
, Client Sample:
46551
9808176-04C=RCSE26
Method 8280-A PCDD/PCDF Analysis !b)
Analysis File: VI10800
i Cli~r.L Prn_j~cl
I Sample \ilauu:
1 TLI ID:
Sample Size:
Dry WdghL:
: GC Clllun,n:
2.3. 7.,i-TCPD
L~,-~. 7.~-Pd.J)D
l.2 . .'.4.7 .~· H:<CD:l
l.:'.:.3.ti,"7.~-i i:<CD!)
!.2.3. 7 .8.9-i·h.CIJD
1.2 .. ~-l.6. 7.,,.HpCDD
1.: .. , .;,6, 7 .:,. 'l-0( Tl!)
2 .. •.7.K~TCUl'
1.2.J, 7)~-Pd '.Dl:·
2 .. ~."'t. 7 .'~-Pccni:
! .2 . .i.-1.7.~-HxCDF
1.2.3.C,.,' -~-H ,CJ)F
2 .. ::.-t.6. 7.~-1 LxCD::
l.:.:.; .;'l.{J.HxC :or
1.2.3.-1.6.7 _q[pCD:'
1.: _ _;.4_ 7 ,x. 9-llp( :ur
I.~ .. \.-L(i. 7 .s. ').()(J)F
·1·{1t:tl ·1'(,:DD
T,,1'11 PeCDD
T:ital I i,CDD
Tmal ll1!CDD
luL:u TGDF
To1a! !);;(l)l·
Total lhCDf'
T\1t,11 HrcDF
Dioxin in sediment
SEDIMENT Datt: R~ccivcd: 08/25/98
216-56-4 Dau: Extraci.ed: 08/26/98
Date Analyzed: 09/01198
10.010 g
6.316 g
DB-5
i'-11)
:-.rD
~'1/D
ND
.',1)
60 :)
ND
l'-1)
ND
ND
t,..1)
ND
'.\Tl
:-,I)
:'-ID
1'1)
0.25
'.\'D
l.6
ND
Nf.l
::-ID
Dilution Factor: n/a
v110100
DD
Blank Fik:
Analyst:
2
0
0
l
0
0
0
0
()_()4
0.07
0.1
0.10
0.1
004
0.0S
0.05
0.◊7
0.()7
0.07
o.os
O. l
0.2
0.5
0.07
0.05
0.07
0.1
Page I of2
Triangie'Labcratories, Inc.Go
801 Capitola Drive• Durham, North Carolina 27713
Ph:ine: (319\ 544-5729 • Fax: [phone]
? • --0
().l'i2
2. J
007
Spike File:
[Cal:
ConCal:
Sf MoisLure:
'~ Lipid:
'i'c Solids:
SP828A50
V85822A
VI09700
36.9
n/a
63.1
J
Printed: 12:03 09/03/98
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TL! Project:
Client S.'.lmple:
I 'j" p . I C.. ,era ~u 1eu:
S~mpk 'viaL,ix:
TL! ID:
' i Sa~1ple Size:
: Drv W:i~hr: I GC Coiu'n1n:
: . .1. 7:x-TCDD
1.2.3.-: .:< -f'L'CDD
! .~._;_4_: .• ~. !-1.\CDD
1.2. ;_1,_ ~ .s. ,I\Clll l
1 .:._:. '7 ,:,( i_1. i i:d_" l)!)
i.~ .. ~.J .. '.'i. 7 .. ~-1 Jrt 'DD
: -~--~,-1_.;..._~_:-:_1_1.( )( '[)!)
: .. '. 7.,,'.fl T)f
1.~.3. 7 --~·-Prl .'DF
2.3.-L 7 .,~-PeCDl:
1.2 .. '.·U.'i-HxCDF
l .2.3.t),; .1\. f I xCD r
2 .. l➔.n.~ .. ,.!--f.xCDF
1.:.5.~ . .\ "•lixC:DF
l.2._t_..!.(\_.-:--~-HrrDF
1.2. .. \ . .i_ ~ ;,;i,1 Li!;,( DF
t .~--~A.to. -:.~_t.1.ocor
46551
9808176-04C=RCSE26
Dioxin in sediment
SEDIMENT Date Received: 216-56-4 Dale Extracted:
10.010 g
6.316 g
08-5
Date Analyzed:
Oil u tion Fae tor:
Blank File:
AnaJysr:
08/25/98
08/26/98
09/01/98
I
VIlOlOO
DD
'' .:·.. Cone, (ppb) \/ :/TEF
ND X I. -ND X 0.5 = ND X 0.1 = ND X 0.1 = ND X 0.1 = i052] X O.U! = 60.0 X 0.001 =
ND X IJ. I = /\U X a.us = !\U X 0.5 = ND X 0.1 = ND X 0.1 = 1'D ,. 0.1 : l\'D ' 0.1 = ND ' 0.01 = ND X 0.01 = ND X 0.001 =
Toxicity Equivalents Report
Ana.lysis File: Vl10800
Spike Fil~:
!Cal:
ConCaJ:
% Moisture:
'k Lipid:
% Sul.ids:
<J 0052
0.()6/)0
SP828A50
V85822A
Vl09700
36.9
n/a
63.1
Total 2,3,7,8-TCDD Toxicity (1989 ITF) Equivalents: D.0652 ppb
(1) Detection Limits not used in calculations. Note; 100% of EMPCs are used in the calcu/atlons.
( .•• J indicates that the value is that of an EMPC.
' -· Triangle Laboratories, Inc.,. 801 Capitola Drive • Ducharn, North Carolina 27713 Phone: [phone] •_Fax: [phone]
Page J oi I
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tJI) 184
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. :,....._,_1ject: REASOR CHEHJ CAL
)
GP 10: 9808~76·055
Cl 1~nt ID: RCSF.27
Coll~cted: D81i3/Q8
Dilution: ",00
Parnrnetcr
bis(Z·Chlorc-ethyl M'ther
?h-:-nol
Z-c., t orophenot
1,3-Gic~~orcbenzenc
\,4-0ich\orotNnzene
1,2-Dicntarobcn2e~?
2,2' -owbi < 1-chloroprapur:i::)
2-!-t:thyl;:,h~nol
~exacr, \ o,-oethcm'?
N-~itra~o-di-~·~ropylamine
t.-Jr,11;-th·:, ~~CM I
t. i t ~ :Jbenunc
l s.ophor,;,ne
2-Nitruph~nol
2 1 4·D 1 oorMyl phenol
bi~{ 2· C!1 l oruetho:,,.y)meThar.e
2,4·DichlcrophP.not
1,2,4-irichlorot:>eniene
Napfiti-1;) l Ci,e
4-Chlcroarn ~ ine
ft~)(.:..::n to~ =:iutc:d i ~ne
4-Chlaro·3·rnethyl;:,hcnol
2··Methy l :1.iphtha l ene
Hc,ach l orc-=ye I 01.eiit adi !?f"IS:
2, 4. o-T r 1 r;h LoroFhenol
2,,,S-Trichlo~o~htno\
2· Ch t c:-on.:;,rit:ia '. ~ . .,e
2-Nitna:iili;,c
l,cenapn~hyler.C?
~i~ethyl.:fl,hal~:e
2 ,6· t:i iii~ rotol uc-r.e
Accn.iph-;her,e
GP ENV.IRO.~!IE:'<HL
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
M~triA: SED1MENT
Method: S~Bi.6 B270C
units: ug/'(9
SEMl\'CLATllE TARGET COMPOUNDS
Rcsut t Rco.lim.
l)OL 120000
BOL 120000
BQL 120000
BOL 120000
SOL 120000
BOL 120000
B~L ·,zooco
BCL 12COCO
BOL 120C00
SOL 120CDC
aar.. 120000
SOL 1200CO
SOL 12oor,o
BQL 120000
BCL 120000
BOL "1200~1C
BOL 12CCOO
BOL 120000
BQL 120000
8Qi. '.20000
BOL 120000
BOL 120000
SOL 1:;!0000
BQL 120000
BOL 120000
BOL 600000
BOL '20000
BOL 600000
BOL 120000
BQL 1200C0
SOL \20000
BOL 120000
A:"la l y:.t : tHI\
An~ly~ed: QQ/03/9B
P:-cpared:
cual ifier
Page 10
Till' lJ: 42 fil JUl 840 1209
Project: RE::I\S:'.lR ·cif::N!C/',!.. GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESIJLTS
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G? w~ r1s□s176-05a
ct ient 10;
Cal le:cttd;
Di {ut ion:
Por.:itr.eter
RCSE27
08/18/98
100
2, !.·Din~ t rophcn:.it
Di b..-ni.:JfLJrJn
2,~·~initrotoluer.~
:0-Ni:rc.:,i-:c:no\
Fl uorene
1, -:h L.:irophmyl -pner.y tether
o:ethylphth~lat~
4-1\it.-::.milinc
l,6-Din;tro-2-methylphcnol
t,;· r.: rro$odi ;:)1e'.l)'l a,ii ne
:. • B ·c:mophcny 1-phenylctht?r
Hcx.:i~h ! -:irobenzer,c
~cnLa:nloroohcn~l
P,-,enant'l.~cne
C,:irb..Jzole
di-n-Butylohthalst~
Flucr.inth~ne
?yrcme
8:.JtY lbcnz.ylphtr,a l.'.>t c
3,3•-oichlorobcnzidine
Senz□ '.a) .ar.!hrar.ene
Chryscnc
bi >'2·Ethyl hcxy L )pl-:thcd :'.3CC
di-~·octytphthalate
Semo (bJ 1 \. uo!"an:hcnc
6 criz:::, Ck] t ',vor-:nt.herie
, Benz.o(.::,Jpyrcne
. I ndcno (1, 2, 3 · cd) pyre"~
Di benz [;i, h) <Jr,C hrace:ie
1Benzoc9,h, il peryt~ne
Matrix: SEDfMENT
Method: SIJ.$46 82/0t
Units~ ug/Kg
SEMfVOLAJJ~E TARGET CONPo:JYDS
Jle>!'.:.il f l!eo, l im.
SOL 60D000
BQt. 600000
BOL 120000
SOL 12COOO
90l 600000
SOL '120000
BOL 120000
SOL 120000
SOL 600000
BOL 600000
Be:. 120000
OOL 120000
BOL 120000
BOL 600000
SOL 120000
BQl 120000
BOL 120000
,aL 120000
BOL 1ZDCIOO
BOL 120000
OOL 120000
BOL 240000
SOL i:20000
SQ!. 120000
BOL 120000
Bal. 12(,000
OOL 12000c
BOL 120000
BOL 120000
SOL ,20000
SOL 120000
BOL 110000
Analr:t: Nr-1
An~lyied; OQ/03/98
Pre;:i11rc:d:
Cue! i f;er
l,t],!13
JIJl b-AU l:.:U~ lit' t:.'i\' !KU.'."4M.J:..YL~L
I Project: REASOR CHEMICAL GPL LABORATORIES, LLLP
IF'l ORGANIC ANALYSIS RESULTS
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GP JD, 9808176·05A
Client ID: RCSE27
Co\lcct~d: oe11s;Q8
UilutiCn;
Par.;mctc-,-
C:i lorcmethiJn{;
Bro.--;;om~thane
Vinyl chloride
Chtorol!thoM
N~thylene chlorla~
Ac(•t Cine
Carbo'l Oisul f-ide-
'i, l·Dichloroetr.£>nc
,, l•Dichloroethane
1,2-0ichlorocttcneccotal)
Chloroform
1, 2-J i chlcroet~ane
2-0,•.Jtanone
1, 1, 1·T:-1trlioroethclnC
Carbon tCtrac~loride
B rc1,1od i ch lorc1ncth~ne
1 , 2· Di ch loropro::iane
ci~-1,3-Dichlo:-cproper.e
Tri (;n lorc,e:h :me
benzene
Di bromo:.h i or :,:;:c:h,1~
-.:r.ins-1 , 3 ·O 1 :h, ciropropcnc
1, 1,2·Trichlo1·;)e-thsne
1 Src»"noform
l.-Methyl • 2 · pe:'"'l'.:a,..,one
2·Hei<.:1none
T~tro:;:h l oroether.:
1, 1. 2. 2-Tc:: 1·.::ich I oroet~ant
ToluC'ne
Crilarobcnzene
Ethylbenze11-e
St/rcn·:
Xy'.ene ( tOt,H}
Ma~rix: SEDIMEWT
Method: SY84& a26□B
Unit~: ug/Kg
VOUHILE TARGET CDMPOU/lDS
Resut t Rcp.L im.
aoc 36
SOL 36
BCL :l6
BCL 36
'-• 16
lB 36
acL 18
aat. 18
BCL 18
BCL ;a
BOL 18
BCL 18
BCL 3S
BCL 18
SOL 18
SOL ,e
BOL 18
3QL 18
BOL 16
BOL 18
BOL 18
BOL 18
BOL 7B
BCL 18
t:1at 36
BOL 36
BOL 13
SOL 18
BOL 18
BOL 18
EOL 18
SOL 10
13 18
Pogc 22
Annly:a:.c: JAH
An~ iy;:ed; OS/31/98
Prei:iar~d:
Oual if ii:r"
·-:~:~-·:;: ~ .. -...... I ~f'\.~,~~1: .. t;~(.:_'.).i ~-~-· .l"tJL 1 J: 40 r-.-u .. Ju1 o~u 1iu~·-·
\[ ~:
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TL! Project:
Cl ienr Sarnple:
46551
9808176-0SCa= RCS E27
Method 8280-A PCDD/PCDF Analysis (b)
Analysis File: V110900
! Clil.!nt Pri.ij~ct:
i S~1mr:k ~v1aLri;,::
jTLI fD
I ,
I
2 .. 1.-; .:~-Tl ])i)
l .~ .. ·.1. 7 .:-.:.J\'.Cl)D
l .:.\'4_ 7 .:-:-! ! .'(CUD
1.1.~\.t\ /.X-!: '(CUD
I ',_ -") 'I ("l'I) •-·_-~.; .,'i,' ·l .'< ~
l .~ ).~.i,. 7 .. ~-HpCDD
~ .2 .. \A.(·. 7 . .:-:,1.1.(}{~f.)D
2J.7.'.\-'l"('!)!:
i ,2 . .l 7.~-PcC.:i)::
~J.~. 7.~-!"1:;( :1)1:
\ .2-..3A. 7 .. '<-i·I~C;)i:
1,:J.6.7 )<-1 f~CDi:
:.J ,4,i\ 7 .:.:-t-lxCDf:
l .:! .. ,.: .:\.1.l-({xCDF
I ,cJ.J.6.7.,:-1 lpCDI'
l .:2J,4.7 .~.'.J-HpClJI:
f .2 .. -~.-t.6. 7 .:-i.1J-< )(.]JF
TtJta\ ·1 c 'DD
T1Jt:1I PcCDD
Tn1al I hl':l)D
Tll<:,I llpCDI-,
l'rn:il TCDl:
Dioxin in sediment
SEDIMENT Date Received:
216-56-5
10.020g
2.876 g
DB-5
i',I)
Sn
~)
Nil
Ni)
;\ii)
NI>
NI)
N[)
:,,II)
ND
ND
ND
NI)
NI)
KD
ND
Ni)
ND
ND
Date Extracted:
Dale Analyzed:
Dtlutio~ Factor:
Bl&11k File:
Analyst:
0.08
0.1
0.2
0.2
0.2
0.3
l.2
007
009
0.0'!
0 I
0.1
0. l
0. l
0.2
0.3
LO
u
0 0.1
0 0.2
0 0.3
0
08/25/98
08/26/98
09/02198
n/a
v110100
DD
Ti..,la..l P1.'.C'DF
T1.,t;1\ H,-.('[)F
Tut:tl lipC:Uf-
ND 0 O.G~
NJ)
ND
Triangle Laboratories, Inc.~
801 Cap:tolz Drive• Durham. North Carolina 27713
Phooe: [phone] • Fax: [phone]
0
0
0. l
0.2
Pag.e 1 of 2
5.3
0.21
Spike File:
IC.ii:
C0nCa!:.
% Moisture:
%· LipiG:
% Soli<.1s:
SP828A50
V85822A
VI09700
71.3
n/a
28.7
Printed: 13:08 09/03198
:::~:·~~-
L'!:JUUO ,.-' I--·:: Vl:1' LI, l:10 J..Ol. J..➔ • ..> ... r.-,..l JV.1. 0-tV 1.,;,v:,
I
. ln:YH'::; ·••··.· i'i';+;lJ-s~1:t;;;c•••tiT:'1if;))'jH'J.fr::1u:fa~~l:~Wi~~~~.;iii\t~\lcl11•liK)m1."iiJlliiI·l. ·:;.::;·~;:0'.;:.:;.r:,1)i;!;rl".:Lll
TL! Project: 46551 Toxicity Equivalents Report I ·1Client Sample: 98D8176-05C=RCSE27 Analysis File: VI10900
Dioxin in sediment
SEDIMENT
216-56-5 I,
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Ciicnt Prnj~n•
Sample \1atrix:
TL! ID: .
I
· Sampk Sizr·.
Dr:.i \V~ighl:
GC Column:
! Analytef
2 .. ,.7.8-Tc~DD
1.2 .. ;. '.S-l'cl 'DI)
i .2 .. ' .. -C.X-H.,I DU
!..2 .. ~.n.i'.~-! '..\(]JC·
! . .2 .• ~. 7 .s_(). f-!.\CDD
I.~ J.-+/1.; .:-:-Hp( 'DO
! ,::'. __ :,_4_(). / ,,.:., l,i-( )( 'DD
; .2.?.. i .S-P,:CDf
~J.-1.; ): .. P,;CDF
1.2.3.-1. i -~-1 ~:,;CD!:
1.2.3.i~ .. i ,;\-HxCDF
2J.-!.6.7 .~-i'i:~cr;r
1.2.3.i .(1>-HxCDF
1.2.3.-Lfi.': -~~l ~prD~
1.2,1.-l. 0 .o.9· HrUW I 1.2 .. u.:;. ~.s.\•-OD)F
10.020 g
2.876 g
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Facwr:
Blank File:
Analyst:
08/25/98
08/26/98
09/02/98
1
VllOl00
DD
(;oile. (ppb) 11:F.••.• /'
ND X L = ND X 0.5 = ND X 0.1 = t\1) X 0.1 = !'m X 0.1 = 1-,l) X 0.01 = ~fl X 0.001 =
ND X 0.1 = )\1) X 0.05 = :SD X 0.5 = 1-;L) X 0,1 = :-.n X 0.1 = ND X 0.1 = ND X 0.1 = ND X 0.01 = ND X 0.01 = ND X 0.001 =
Spike File:
!Ciil:
ConCal:
SP828A50
V85822A
VI09700
% Moismre: 71.3
o/c Lipid: n/a
o/c Solids: 28.7
I Total 2,3,7,B-TCDD Toxicity (1989 ITF) Equivalents: O. ppb
(1) Detection Limits not used in calculations. I Note: 100% of EMPCs are used in the calculations.
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Triangle Laboratories, lnc.3
1801 Capitola D~·1e • Durh2m, North Carolina 2n13 Fh~ne: (919) 514·5729 • Fax: [phone]
Page I of l
Printed: 15:24 09103/~\(
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301 HO 1~09 GP nVJRO:-l!lDT.\L
GP [O: 980!!". 76 • 068
Client fO: RCSE28
c~l lectc-c:: 08/18/96
Ci lu:ion~
Paramer.cr
bi:;(2-Chlc,rOHhyl )Cthc:-r
Ph(mol
2-Chlorophenot
1.3·Dichtor-ritY.:"12ene
1,4-0i:h,or0bcnzene
1 ,2-;) icn lci-w"oenze·1c
2, 2 • · oxybi .s ( 1-ch laropropane)
2 ·/•1etnvlpncno l
Ii e xach ~ or:ie t,'l-lr"!F;
IJ ·Nit roso-di • n· i;r-cpyl M, i ,1e
, 4-MethyLpncnot
~itrot.enzene
,lsop:\::irane
_2-Ni trophen::il
12,t.. ·Di.'OC'thylphenot
bis( 2-Ch l ;1·octho,.,y}meth.:inc
2,G·Dicnlorc;:lnenot ' . l,2,4·TricML~rcbeni~ne
/Japhttl/llcne
4·CnLoroanl ~ inc-
H~x,1ch' or:ibu~.ic:i ~,,,.
4:·Ch lo1 o-3 ·:r.e-~ll'y lphenol
2-MethylnJ::ih<halene
Hex;,cM l crocycl QpC:ntadi ene
2 ,:4, 6· Tri ch t O.":"'lpt,erieol
2,4,S·Tricr.lcrop'lenol
2 · ~;, 1. orcnapr, tha Lene
(·Ni-Cr-oan\li,1e
l\ccna.ch thyi l ·1-:
D i~thy(_ch thal ai::e
2, 6· O i r: i trotol uc.~c
AcenRp,'ii::hcne
GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
Matrix: SECJMENT
Methcd: SW846 827DC
Uni t.s: U3/K9
SEMI\IOLATJLE TARGET COMPOWJDS
Re::;ul r Rep.L irn.
B01. 510
8QL 510
80L S 10
BCL 510
SOL 5t0
BOL 5i0
BCL 510
BOL 510
SOL 510
BQL ST3
BQL 510
· BO~ 510
OOL 510
BO!.. 510
SOL 510
BOL 5,0
SOL 5i0
Bt:i:... 510
BQL 510
BQL 510
SOL 510
BOL 510
BCL 510
BQL 510
SUL 51 a
SOL 260/J
BOL S ~ 0
OOL 2600
SOL 510
BOL 51D
SOL 510
ROL 510
Analyse: NM
An"lyzcd: 09/04/9D
Prepare:':
Qualifler
12
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Project: REASOR CHEMICAL
G? ID: Q808i76•066
Cl ie11t 10: RCSE2S
Collected: OBn1:n
~ilutior.:
Paramc-t er
3•Ni~ro.ani Line
2 ,L.-C i r. It roph~~.('I t
Dil:;cn2ofurJ;)
2,4-Dinitrot~l~en~
,,.~itroph~nol
Fi:.rcrcne
~-Chloropntnyi-pnenyl~ther
Disthylphtha:ace
k·Hitroani line:
~,6-Dinitro-2-me:hylpt,en~l
/.J ·nit rO!i::::di ph errtLa~ i ne
'-·Br011"10pi,cny!-pher,ylinher
Hex each lo--"r..e:1z '.::m:
P~ntachlo;op~er.:Jl
?henanthrene
~nthr;icenP.
Carbazolc
di·n•ButyLph:h~lJt~
::[uor.inthen<;!'
Pyrene
s~ryloenzylpnt~~\Jtc
3 ,3' ·Di ch I orcbcnzi dine
Bcnzo(ajJntn~acene
C:iry$C'OC
bi s~2· E thy1,h~xyt )ph th :,t .:itc
di-n·Octy! ~thal.itC
Benzo [bJ f luorJr.r.hen(:
; scn;:o(~l ~:uoro:,thene
, Ben~o(a)py:-~ne
1 t.1deno(1,2,.3·cdipy,e:ie
Di b~riz [;,i, hJ .;.,rch racene
Benzo[Q,h, i]perylen~
I-
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GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
M:H r ix: SEO IHENT
Method: SU846 627CC
Units: ug/l(g
::;cr,a rou, i I LE T ARGEI COMP()JNGS
Re-:;ul t Rep.l im.
BCL 2600
auL. 2600
SOL 510
SOL 510
BJL 2600
BOL 510
BCl 51C
BOL 510
BOL 2600
SCL 260G
BOL 510
B~l 510
6Ql 510
SOL 2600
£101, 510
BOL SiO
SC!. 510
BOL 510
SOL 510
BOL 510
SOL. 510
lOL 1000
6Jl 510
BOL 510
Bal 510
BCL 510
BO~ 510
BOl 510
SOL 510
BOL 510
SOL 510
SOL ';,~O
An:Jtyst: '-1"1
Anal /Zed: 09/04/98
Prepc1rcd:
Quali-ficr
lf1) U15
Peg<: 13
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Project: REASOR CHEMICAL
GP !D: 98□~176·06A
ct ient ID: RCSC:28
Colt~ct~d: 08/18/9e
Dili.rtio~: 1
Chloromcth.:inc
aro,"llornethan~
'Jinyt r.hloride
Chloi-~thanc
MCH1yler:e chloride
A-:,none
Ca;-bon Oi$ulfide
·,, 1·DichLor::ic.-t/-.en~
1 1,1-C.ichloroecrane
: , 2-D i ch! tiroett-,,::/"\c( total )
Chlo;-oforrn
1,2-Dichlo~oet~~ne
2-gutilnon-?:
1, 1, 1-Tri chi tif·:::cth,;n(I
1 :.'.lrbO!'"'I t1Hrachloride
5ranodichlororn~thnnc
1 , 2-D i ch l c-,·op:-~p.a"le
I c i ::.-1,3-::: i en l oro~rcpcnc-
, Tric:.,lorctrhc-,,c
BC'-n?Cl"IC
Ir i !:lromoch l or-::imeth,:m~
tr~r.~·1,3-Dichloropropene
,'., 1,2-Tric.hlo;-CJethbn~
Sr~form
I, -M'-'thyl -2-pent!llfiOfJe
2-HexanJt:~
T ~ tl';.JCh t croeH, f!'ne
1, 1,2,2-Tetrach{oroethdne
Toluf!'ne
Ch l crobcn2c:1e
E rr>yl benzene
Styrene
Xylene (!oral)
GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
M~trix: SEDIMENT
Method: SW3~6 82608
Uni tr.: ug/K3
VO~ATlLE TARGEf COMPOU~OS
Result Re::i.Lim.
BOL 15
SOL 15
BOL 15
SOL 15
' 8
;e 15
SOL 8
BOL 8
BOL 8
BO~ 8
SQ'. B
SCL 8
BOL 15
OOL 8
SOL 8
BOL 8
SOL 8
BOL 8
oOL B
BOL 8
BOL 8
9:·L 8
SOL 8
a~t ~
BOL 1 l
8,L 15
EICL " SOL 8
BCL 8
BOL B
SOL B
SOL 8
SOL 3
Analy~t: JAH
Ano{yzcd: 08/31/08
Prepi.ln::d:
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B
u .. I
I
i::':t\: ;.i;":~f,~l::•(~•:[rx~~i\~~~~~~~~i~~i~~~tM~~~~~~~i~,~~~~~~~i,\l~~,~~11
:
~
~
~

I
TLf Project:
Client Sample:
46351
9808176-06C=RCSE28
Method 8280-A PCDD/PCDF Analysis (b)
Analysis File: V111000
I Clicn: Pro1cct:
! Sarnrlc \,1a1rix:
• :fLI tD:
I:
I: ,S:1:npk Size:
L)~·v \,\' ~ t !.! :,, L:
1 ·c,l~ c,,1u~11n:
'.. AnatyteS·.''.."·:~:.
I ,
2 .. ,. ;_:-:.·r1 :DD
1.2 . .1. 7.:-:-!\FDlJ
I c . .',,l,7.X-1!.xl'Dl)
l·.2 .. ,.(,_-; -~-r-rxCDD
: '_:, __ ,_-; .S .'.l-i lx ( '.Dl)
I -~--'-•k<i.: )-'.-! !p('.DD
I .:::. .. , . .l.6. 7 .S. t_1.()Cl)U
I
2 .. '.,, K-'T!JF
1 , ~ ·, ~ ll • ··nr: .,J:--··7•~ ,, •) l~:, '
_,_, .• l-_ J,~-1 (.;I_ .,!./I·
L~ .. \.-1. 7 ,K-1 ixCf>f'
1.2.3.6.7.~~ihCDl~
2: __ l,-!.6.7 .~-H~C.DF
i:. ~-:,.1.~.lJ -1-Ix~:DF
I.2 .. \.4.f.:; .:c.I lpCDf
l ·.: .. ~.--+. i ,S, ~J-H pCDF
I c2.,.-l.6. 7 .. ~, •>.OCDF
T{l(:t.l i"l ~DD
l'i 11:.! :'c-CDD
Tn::li lhCDI)
T,111:d tipCDI)
·L,1:d T{ '.i)f
intal h.:CDF
l'nt:il l l:<.CDF
T;11:d llrc·or
'
'
Dioxin in sediment
SEDIMENT
216-56-6
10.000 g
6.260 g
DB-5
ND
t--m
NI)
!-;1)
ND
ND
ND
ND
Ni)
i-m
ND
I\;])
Nl)
~I)
,-,TJ
Nf.)
NI)
ND
:-<n
ND
1'D
ND
ND
)ID
Triangle Laboratories, Inc."
Date Received: 08/25/98
Dal~ Extractcu: 08/26/98
Date Analyzed: 09/02/98
Dilution Factor: n/a
Bl.mf: File: Vl10100
Analyst: DD
Q.O.~
0.0~
0 l
ll.09
O. I 0
0.2
0.5
0.ll4
0.06
0.06
0.06
0.06
0.06
007
0.0\)
0.1
0.4
0
0 ll.08
0 a.o9
0 0.2
0 o.,14
0 0.0o
0 0.06
0 0.09
Page I nf2
801 Capitola Drive• Durham, North Carolina 27713
Pt,one: ('.l19) 544-5729 • i=ax: [phone]
Spike: Fik: SP82BA50
!Cal: V85822A
ConCal: VI09700
% Moisture: 37.4
% Lipid: n/a
% Solii.ls: 62.6
2.4
Printed: 13:08 09103
,i,-•:-.>:;~ •.• '._-:: ••• ::::{,.-•. ---l •••
..••.• , I Vt' t:..,, J.KUl'i'li::..\l:\L l{lJ UU7 11If:i·.f.\:~~:~11,.J.{.'t,O i.nu .L°':Jo 1".-\.'!. JUJ. o'li.J 1~u::1
1
1
-·1
· =1 :;-c-:'->a:\-: · •.. ~--,------,-,-=.=r:=-}=:,)=,~~}=; :::=;:.~-,=j=,-:<=-c=P:=Eri=--~=-~~=~=L(Il=_~=,\,=~--=_ .. =. = __ = ___ -r=::,;::=ri:=v;;:=::w=Lm=I:::=:1:=iiit=::.=:::11
TLI1 Project: 46551 Toxicity Equivalents Report
1.,-"') Clie,nt S.:unple: 9808176-06C=RCSE28 Analysis File: Vlll000
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Cli~ni Prnjcc:L:
SJmpk \Lmix:
TL! ID:
Sarnpk Siz•::
Dry \Vc:ight:
GC C:,lu:nn:
j Analytes
c .. ,. 7.S;TC"l..'I!
1.2._;_ 7 .:-: • \>~(~DD
J .2 . .'.-l.;.S-1-1\('Jl[)
1.2.3.6.:. .:-:-i lxt 'DD
1.2.>.'i.N.l.l-HxCDD
1.2.3.~.¢,. 7 .K-Hr< '!.)!)
1.::.,;,-1,~,. 7 .~.i.,1-( )( :ou
' ~ .. ~.7.~-·1r·or:
1.2.\,j.J'c("l)i-'
2 .. 1-.• -L':.~-PL;C'l)F .
! .~ .. t-1.: .:-:. HxCDF
1.2 .. V,. 7 -~ -I h('flf'
2 .. ~ . .;.r,. -:·.:< -H x.C l)J:
l .2.3.: -~·.1)-!ix(·: ;1:
1.2 .. 1,.1.~.0 .~-I lpClJF
1..: .. ::.-t. :-:.-::1-! i;--! 'DF
1.2 .. ~.-U).-::-: ... (IJ.\ H 'DF
Dioxin in sediment
SEDIMENT
216-56-6
10.000 g
6.260 g
DB-5
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
Blank File:
Analyst:
08/25/98
08/26/98
09/02/98
1
VI10100
DD
... · Cone; (ppb) ···•••: /TEI"'·'.
ND X I. =
ND X 0.5 =
ND X 0.1 =
~1) X 0.1 =
ND X 0.l = ND ' 00\ =
NJ) ' 0.001 =
ND X O.J =
ND X 0.05 =
ND X 0.5 = ['.1) X 0.1 = :s;D X 0.1
r-.u X 0.1 =
ND X 0.1 =
ND X 0.01 =
Nl) X 0.01 =
)1,1) r. 0.001 =
Spi..l<~ File:
!Cal:
ConCal:
'7c Moisrnre:
'le Lipid:
% Sdlids:
SPS28A50
V85822A
VI09700
37.4
n/a
62.6
Total 2,3, 7,8-TCDD Toxicity (1989 ITF) Equivalents: 0. ppb
(1) Detection Limits not used in calculations.
Note: 100% of EMPCs are used in the calculations.
Triangle Laboratories, Inc.,,
801 Capitola Drive• Durham, North Carolina 27713
Phone: [phone] • Fax: [phone]
Page 1 of l CRY _TEF • 1m. M.11..ES ,.It-I}
Pnnted: 15:24 09/03198
261
l½i'-;-~--
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U~!lU/~ij J'HL' l~:H F.U JUl HO l~UU GP E.\l'!RO:-ll!El'ffAL
Project, REASOR CHEH[C" GPL LABORATORIES, LLLP
GP ID: 9B08176·10A
Cl ienr iD: TRJP EE.Alf)(
Co1.\c:.td: JB/18/96
Di l:,t ion: 1
P~ran•ete:--
c:-. lorornetnJn,;,-
Brom<,cr,.::,th,m~
Vi.i)"l cr'lloride
ChlorcethMC'
Methylent ~~lorice
t.cc:onc
c.:.i.-'::ion Oi~ulflcc
1, 1-Dichtorocthene
l, l·DichloroethAl"'l-e
: , 2-D i ch l :iroe::lcnc( t cit a i_)
Ch ~oraton:,
·,, 2·0 i ch lor~E:!::hane
2 · Cut 3nor1e,
i, 1, 1-Trich!oroc:trane
Carbon t~trachtoriae
3rorr.odichlorom~th~nc
1, 2·Dichlcrop:-opane
c i s-1 ,3 -0 i ch\ oropropcn~
r rich~ orocthene
B:!nlc"':1?
Oibron::ichtoro7'1cthane
t ro~-1. 3-o: ch l oropropenc
1, 1,2-Trichlorol'.!t:h.:ir":c-
a-on-ofcrm
f-~ethyl-2-~entar.one
2 -·~l!x.1,;one
Tet rach l crocth E:'ne
1, i,2,2-Tet.-.achlcroeth;mc
' Toluene
~hiorobCnlcnc
E.~hyl~m:erie
Styre~e
x_y:cn"' (tot.1l i
ORGANIC ANALYSIS RESULTS
M.:itrir.: '.JI\TER
Meth~: SW846 8260B
Units: ug/L
VO~AilLE TARGET COMPOU~DS
R•~S~ ( t ,.
BQL
BOL
SOL
SOL
4
BCL
BOL
BOL
B0L
SOL
BOL
BOL
B0L
BOL
SOL
BOL
Bo,
BQL
BO!.
BOL
BOL
•oc
BOL
BOL
BOL
BOL
SOL
SOL
BOL
SOL
SOL
BOL
BOL
-l ir:i,
10
10
10
10
5
10
5
5
5
5
5
5
10
s
5
5
5
5
s
5
' 5
5
s
10
10
' 5
5
' 5
5
5
Ar-i::ity~t: ij~H
Analyzed: 08/26/~8
Prepared:
,a
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GP E~VIRO~HE~TAL
GP Work Orc.er ;t 9808:!.76
Sk"PLE ANALYSIS REPO?.T
Prepared for:
ROY F. WESTON I I!'-":C .
5405 METRIC PLACE
NORCRCSS, GA 30092--2550
Prspa:r-ed By:
GPL Laboratories, L~LP
202 Perry Parkway
Gaithersburg, MD 20877
September 10, 1998
Sadoughi, Lab8~atory Vir~ctor
··········-•.·~~-:.~·--:.:~;.-;-,-_ · .. ::. -.. · ....:. . ·-··•-·----··---. u•~u•i,••~frii,i 1;i:,1u ~·.u JUI ~.u 1iu~ '} ~lf . ~~-~.\. '\: .. '"l'l•t\~i~~;-L~~--..... i,, : . ..'-;r,.,:f,: y· ' .\ '~: ...
;;;c:;,,. J• I Project: REASOR CHEMICAL
<1 I .. ·-, Proje-:t': REASOR CHEMIC.Al
I
I
IWY F. WESTON, INC.
5405 METRIC PLACE
NORCROSS, GA 3C092-2550
A.ttcn: DAVID NSLSON
<;P ESVIR01"!1E.\TAL
GPL LABORATORIES, LLLP
ANALYTICAL RESULTS
GPL U180RATORIES, LI.LP
202 Perry P~rkway
Cai ther-sbun~, MD 20877
A.tteri:
Phone:
Cl ier.t SN'licei-
(301) 926·6802
•/2···. ,'!.1/q-· ~ll'f't if i ed by: __ ...L<CJCC-'.....::·?•-~~-'-------
I SAMP~£ :DENTlflCATION
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GP ID
9808176·01A
~808176·0~1B
9808176·01C
9808176·02A
9808176· 02B
9808176·D2C
9808176·03A
9808176·038
9808176·03C
980a170·04A
9808176·048
9S00176·D4C
9808176-0SA
9808176·058
9S08176·05C
9808176-06A
98U!l1i'6·06fl
98C8176·06C
9808176·07A
980B176·08A
9808176·088
9808176·09A
9806176·098
9808176·09C
9808176-090
Q80S.176·□9e
9808176· lOA
050S176· 100
9808176·10C
ct i ent 10
R.C~E23
RCSE2t.
RCS:EZ5
RCSE26
RCS[27
RCSE28
RCSIJ19
RCS\./20
~CS:J21
TRI? BLANK
i4]00J
I ,:0
I ' '')
i !
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.· .·
BQL
J
p
B
E
u
D
+
#
=
•
@
$
GPL Laboratories, LLLP
Possible notes and definitions for this report:
= Below Quantitation Limit
= Value is less than the reporting limits but greater tnan zero
= Indicates that there is greater than 25% difference for detected pesticicie/Aroclor
resctl!s between the two GC c:olumns
= Indicates that the c:ompound was found in the associated blank
= Indicates that the concentration exceeded the calibration range of the instrumer,t
= Indicates that the compound was analyzed for but not detected, number indicales the
reponing limit
= Indicates that the compound was found in an analysis at a secondary di!ution factor
= Value obla'ned from a 1 :5 dilution
= Value obtained from a 1:10 dilution
= Value obtained from a 1 :20 d)lution
= Value obtained from a 1:25 dilution
= Value obrained from a 1 :50 dilution
= Value obtained from a 1:100 dilution
= Value obtained from a 1:250 dilution
= Va!ue obtained from a 1:125 dilution (medium level)
= Value oq:ained from a 1 :500 dilution
, & = Value obtained from a 1:1000 dilution
I N = Flashpoint not observed· heated to specified limit
R = Flammable at room temperature
TNTC = Too numerous to count
S.P. = Detec:ion limit taken from boiling point
F.F. = Sam;,le gave offilammable fumes
I ~tfi~v ·· l,.~~,.:.!u~,.1u::,, 1nu ;J;:-..... •, ... _1_~;-i~--t'-1.~ _JUl 0,iU .l~U~·-· ·t' i . . .. -. ---... . ·. l:rt' t..~ V_!_!:(~.'tru:__"'; 1:U, ~ G.J' .£,,-a?.0.'-.'3f£N,,,.!.. SU.VICES "11 uau -SA.MP.LE RECEIPT O' ..::.C.'<UST W.O. Ne, C!::.~t N.::.=: Ila:o R:c.:::,·1:.,; I q8~ri<, 17ft ,,-I IZ ~-,,:,-r,_ ,r (::Z o I 51f T !:'.:. R ::.::Yc::i q: 2$ Ar---...., F..:c.:...~:::. E:-1 ~ ~ :,.-...;;, ri..1~-:; ..... .,, ......... ,, ,r ___ ,_, __ ...,_ .. ..,.. _ _.i,., No. _________ _ .S:i~~:_:g C=:=.:z.:=:.: :.:. Gc-:id Co:.2cio!l? I ,-,.(•c,-·v c:,., : .. ?-.. .---~c,.. ~ .... ;_ : ..... ,...,.,_1.,;_,...,, .......... -..... -....... _ ........ _ -t; -....;_; ______ . C=~::!:i=:=-: Gc~.:l :ck:.=_ (:..~=--cr . ..-..,("O,.: .. ;::, ... ~ ... ,? - i .__ __ ·--;. ,. ____ , c;:~:-.c.[-C .. ~·:-.Cv .:.-••( .:.~··· <::~-... 1., .,;..,.t., --,._ , I•!:----o1-'-'--:-•• .i.....:....-->• C"·'·-cf-C .. ,.·~v s,·-.s, ----~---., .._ __ _ .?.!~ ';-.'"·-• ; ... S'-=--:-~ ,...._,..,.,;-... , , - . ------: :-5 '""'-'---·. 7,.,., c• ~,-i:::'.--i:7.,.L-.r.a/1 ,,v,vr> .,, •• " -V ~o _;/ -x: / / L_ ./ -D....,; c= N.=e ;::::;;; f-7"--lifx< l'r:par:d {Log,;:c fo} By r'rojc:ct __flz_.,_c;,.· n,,, !?<?'I 73' 12,1(?9 b0.h D>.t: C .<<c-: '=,;, I Site _____________ _ VOA Holfug B~ LD. No. _____ _ -· ~1 ~--. ':c10 -z.:h R-~,-, . -N~. o: S:~ -? ,.,, :·,,.-d_f ...,., 7 VOA V:iz2s Havi ~:-o :-:::6:;-?.::'? ✓ _ P::.s:rT~:.i;·:.s A::::::. to Sz.=;:::: y_ p:-, C=.ct ?,i:.~::::,~? ~ ?--'~--~-:,,, -s",..-----···--~-... -..,,;. ~ 1~ Fr~==-~ i:. S'.:.:~~L!:s Ccr.t~::? ✓-D!"lt ... ;-:~# Tc::~:!:-.::: YI --.?(, Cl v--C:.:!i:=Cy .:: .. ili C"" c~--: .. !kt•i ..... -, Co .. ..::.~: ... G; ... ;-----·-~,cwC: ~ /,-',;Z_ . o.:>t:::--'3, ~ .. -:--·--... ___ i.: ... __ Tc,zl Ni=:::: cf s~,1= Ec:-Jes ;? °I To.,1 "·=---~-ci ,, __ ,., 0 ·-.•1 --· ---r-~ --; S=p!::.: l=.:zcr: ✓-.S~::::t Sa.::;l: Vo:~e fo: lz:.'.i:c:,.td Tes:? J_ I Proj~ M:.::z.z:: C=:i:.:ze::;? Nme: J&-:.-j 6(: ,,/. (~,, Da:e C:::tacr::!: "1( /~-'i" .A;y ~-~ :~?O::.!: ::'..!!: :"e d::z.il~ i:. t.::: c:c.=:.:l!.S :=cloo below. lf itc:::.s ue :ct a~pliobl~ to F~...::-.. :.h.: ~pi~ e: r:::.::!.::: tbe1 ,l:.c0.c: be t=.z.:l:d N/A. I ' I /,' /-C0t-{.v.:2--."7S: ~T1t~ Qt:,,J: 1(a;,,:.ul. 1;.d .11£f 4)/4.,I ,'-k C!tJ~-' Cb··"fut G:::;:l:::~ bv.....-~----------D,t:-? /:J-I t?r 05
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Project: ~EASOR CHEHJCAL
GP JD: 9808176•07
:l ienr lD: RCSU10
::ii lver ' A lumi ni..1,1
Ar:;cni::;
3.irium
Be;yt I ii..•m
,:.:dcilJ'l1
C~drni'Jn1
tobal t
Chr,omi Lill
::opper
iron
1"11.Ufury
Pot.,,ssium
Mi'.JgAes i um
~angane~t
<:.odium
11ickel
Lead
Antiinony
Sclcni un ' ThalliU'll
Van:3d i wrr,
Zinc 1
Mc!hod
5U846 6010
S1-1846 6010
S'w8t.6 6010
S!.1846 6010
SUB,6 6010
S'M8L.6 6010
SUBL.6 601C
S\./846 6010
SU846 6010
S\./846 6010
S'.J8f,6 60TO
SU846 74 70
SW8.\6 6010
Sl./846 6010
S0346 6010
S\.1846 6010
S\J8t,6 6J10
SV846 6010
SW846 /.0,0
S'wgf.6 601G
SW84o 6010
S\.'846 6010
SW846 6C10
GP c:>Y !J\Ui\llE.\T.-\L
GPL LABORATORIES, LLLP METALS ANALYSIS RESULTS
Re,<:u: t Rep.Lim. Unl ts
SOL 3.o u:,/L
480 100 ug/l
BOL 5.0 ug/l
17. 7 10.C ug/L
SOL 3. O ug/l
18700 1000 ug/L
BOL 3.0 ug/L
BOL 5 .o ug/L
BOL j .c ug/l
BOL 5.0 vg/L
725 100 ug/t
BOL 0.2c •..,19/L
3080 500 ug/L
1;40 500 ug/1
16.J 5 ,o U9/L
11',00 500 ug/L
BOL ;.o U[l/l
EOl 3.0 :.JQ/L
&0[ s.o •..,19/l
BOL 5.0 ug/L
8QL 10.0 ug/L
BOL 5.0 ug/l
10.2 10.0 ug/l
l,z]026
~utrix: WATER
Colltctcd: 08/18/98
Di l. Prep.1red AnJlyzed By
09/02/98 09;0,/98 DOH
09/0Z/98 09/0:'../98 DOH
I 09/02/98 09/04/)"8 DOH
09/02/98 09/04/~8 DDrl
09/02/98 09/0t.;9e OOH
O)/OZ/98 09/0.'../98 DOH
09/02;98 09/04/98 DOH
09/02/98 09/0l./98 DDH
09/02/98 09J□l./t;>8 ODH
09/02/98 09/04/",8 OOH
09/02/0i!, 09/04/98 DOH
I 09/06.'~8 09 /Oo/98 LCM
09/02/9e 09/04/90 ODH
I 09/02/98 09/0t./98 DOH
09/02/98 09/04/98 DOH
09/02/98 0910,na OOH
09/02/98 09/0t./98 OOH
1 09/02/98 09/04/98 OOH
1 09/02/98 09/04/08 DOtl
09/02/98 09/04.'98 OOH
09i02J96 09/04/98 DOH
1 09/02/98 D9/04/98 OOH
09/0Z/98 09/0t./9S DOH
... , PrOji?c:t: REASOR Cr1EN1CAL
,_
..
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, GP !~: 9808176-0BS
Client JO: R~S~20
, Col cectcd: 08/18/98
Di luti◊n: 1
bis{2·ChloroP.-rl-.yl )ether
Phc.:nol
12-Ch'. a rooneno l
1,3·0ichlorobcn~~ne
1,1'..-Cichlorobenztn~
1,J-~jchloroben2cne
Z,2 1·o~ybis(l-chloropropaneJ
~-Methylphcnol
Hex~cnloro~thMne
~·Ni t,-o~o ·di· n·propy I !'1.'lll nc
~•·M!ethylphl)l'IO[
Ni trober.zcne
r ;;.opnorene
2·Nii:ropnenol
2; t. ·Di mG"th y I phenol
bi sc2 • Ch l crtJct hoxy)met/",c1ne
2, I.· Di ch lorophencl
1, 2, I'..· rr i er, loroben:!.enE::-
Naphthal CM
l.·Chloroani l inc
Hc~achlorobutadi~~e
~-~htoro-3-met~ylph~nol
2-MCthylnapl,rhalen~
Hexachlorocyclopent.idiene
2, l., 6· Tri en l oroph,::,r,ol
2 ,l,, :-1,-i chloroJY)1cnol
2-Ch l orcr.oph th al ene
2-idtroaniii."'le
Acc::rluphrhytenc::
Di mE'thytph: h.il ate
(,6-Cinitrototucnc
Acc:,a~thene
GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
Matrix: io!ATER
P.~thcd: SUB46 8270C
Unit:;: ug/!..
SEHIVGLATILE TARGET C0MPOIJ,ros
Re!':Ul ~ R~p.
ec:.
SOL
BCL
ROL
SOL
BCL
SOL
BCL
SOL
BOL
60L
BCL
SOL
SOL
ODL
SOL
60L
SOL
SOL
SOL
acL
BCL
BOL
BOL
BOL
BOL
BOL
BllL
BOL
SOL
BOl
BOL
l im.
;o
10
10
10
,o
10
1C
7.J
ID
10
10
10
10
'.O
10
10
10
10
·10
·, 0
10
10
10
10
10
52
10
52
10
10
10
10
An.:ilyst: CJO
Analyz~= 09/02/98
Prep.:i.-ed: 0S/2:5/98
Ou~litier
P.sgc 14
I ?roject: REASOR C'rlEMICAL
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CP ID: 9808;76-08B
1 c! icnt ID: R:::s~20
Cvttectec: 08/18/98
Di l•.Jtion:
i Paramc-c~r
3-Nitro;tr"li\inc
· 2 ,:.-Dini tro;:ticn□L
:Ji te'.lz:cfur.an
Z,4·0ir:itrot□luene
4-Ni ·.ro::ihenol
F l~orene
1
:0-Ch l c,rophcny I -phenyl eth i:r
Di,:: thy! phtMlati:
l-N:Ho::iniline
4, 6 -o i ni :ro-2-mcthylphenol
~-ni t:-::,s.odi ~enylllminc
<1-B rc::,op/,eny 1-pMenylr.-ther
hC?.-;ach L c:-r·obenzcnc
' Pertach l or·Dphenol
Ph,::riannreri.e
A.~:-!',rac~r>e
C~:-bazole
di· n-s;.:t y lc!"ltha late
~luuranct;~ne
Pyren~
8UtYlbcnzylphthR!at~
3, 3 • -o-:d l □,-'-'oen2 idine
Senzo[a)~nthrciCene
Chryl:>c:::ne
Oi s<2-Erhy l hc;..:yl )phthal ;ire
di,-n-Octy l ph':.h.1 Late
aciizc [l::J fl u::i:-anthcnc
Benzo[~J fl uor<.inthen4?
a en:o {;.i] PY~ ene
lnde~o(1,2,3•cdJpyrene
o;o.enzfJ,h]a~thracene
BC:'\Zo[g,h, il;:i<:?rylcnc
!
GP EWIRO!l"!!D"TAL
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
MatrlX: \.IATER
Method: S~846 8270C
Uni ts; ug/L
SEMfVO~ATJLE TARGEf COMPOUNDS
Re~ult Re .Lim.
BQL 52
BQL 52
SCL 10
8CL 10
BQL 52
BOL 10
BOL 10
BOL 10
SOL 52
SOL 52
SOL 10
SOL 10
SOL 10
BOL 52
SOL 10
SOL 10
80L 10
BOL 10
BCL 10
BOL 10
BQL 10
BOL 21
SOL 10
BOL 10
SOL 10
B:::!L 10
SOL 10
SOL 10
BOL 1G
BJL 10
OOL 10
BQ':.. 1C
Analy~~t: CJJ
Analyzed. 09/02/98
Prepared: 08/25/98
0:.-Jl ifi er
Pa9e
Hill 1:J: ~5 !'.U JUl HU 1209
I Project: REASOR CHEJl'!!CAL
I
I GP ID: 9508176-0B
Clien! ID: RCSW20
GP ENY IRON!!ENT AL
GPL LABORATORIES, LLLP
METALS ANALYSIS RESULTS
I P£11·;:i;nc~,~•~c---------==~-----'==~--~===---"==--.=-'--'. M~thod Result Rep.Lim. Uni :s Di l.
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Si lve-r
~LL.n::num
Ar5cni c
Barium
aerytll i urn
C3lciurn
c.:io11iun
Cobalt
C.hram:ui:
Coe-per
I rcn 1 Mer::ury
?•.lt.J~::iium
~iign~s,1urn
Mansanese
Sodium!
N'id:.el,
Lead
A~t i /00,1'1
scl:::nium
r:ial L. i:..m
-✓~n::!!jh.f
Zinc
S~Bt.6 6010
SU8[.6 6010
SW846 6010
S'.JB46 60i0
S:\J846 601 0
S~846 6010
SU846 6010
Sl.l9C.6 6010
SU846 6010
s1.1846 eo1c
Sl.1846 6010
S'-1846 7470
SU8t.6 6C1G
S.J846 6010
S..'81.6 6010
S\.11346 6010
S\./846 6010
S'..1546 6010
S~846 6010
50846 6010
S\J846 6D10
S\JS46 6□10
50846 6010
BOL 3.0 ug/L
998 200 ug/!..
SOL 5.0 ug/l
B.8 lG.0 UQ/L
BCL 3.0 u9/!..
16500 10'JO u9/L
9:lL 3.0 ug/L
BCL 5.0 ug/L
BOL 5.0 u9/L
BCL 5,0 ug/L
3690 100 U9/l
SOL 0.20 IJg/L
2840 500 ug/L
1700 500 ug/ L
79.8 5.0 ug/L
11400 500 ug/L
BOL 5.0 ug/t
BOL 3.0 ug/L
SQL 5.0 U9/l
801 .. 5.0 ug/'..
SOL 10.0 ug/l
BOL 5 .0 ug/L
2h.6 10.0 U!J/\.
Page 27
M.:itrii,,.: UATER
Collected; 08/H!/98
?rep.ired Analyzed Elv
09/02/98 09/04/98 DCH
09/02/98 09/04/98 DOH
1 00/02/98 09/04/98 DOH
09/02/98 09/04/9S DOH
00/02/93 09/04/98 OOH
□?1□219e 09/04/98 OOH
1 09/02/98 09/04/98 DDrl
09/02/98 (19/04/98 DOH
09/02/98 09/04/98 DOh
09/02/98 G9;Q4/9!1 DDH
1 09/02/98 09/04/98 DOit
09/06/98 09/06/98 LCM
09/02/98 09/04/98 OOH
09/02/98 09/D-1/98 DOH
09/02/98 09/0:../98 DOH
09/02/98 09/0G./QS OOH
09/02/98 09/04/98 DOH
1 C'i/02/98 09/04/98 DOH
09/02/98 09/04/98 OOH
09/02/98 09/04/98 OOH
09/02/98 09/C,',./98 DOH
09/02/98 09/04/9e 9DH
0>;/02/91:! OQ/IJ{,./98 DOH
. 09., 1iJ;9s rnv 1J: .i.i F.U: 301 s.io 12ot1
Project: REASOK CHEHIC~L
.-·,. i
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GP JO: 96C8176-09A
Client JO: ~CSU21
Coll~cted: 08/18/98
.-1if1..:tio:1:
C.'tlorc.metri.:,nc
6 tomo.,i,ei:h !):·.~
Vf~yt cl",loridi!
Ch l Cl'Oet~.l~e
1-lernyler,c chloride
Acetone
carbon 0;~1..\ fide
1, ~-[,ic!-\l(!rOc':.hene
1, 1 ·!) ichloroetharic
1,2-Dichloro~thcne(totat)
Chloroform
1,2·Dichl~rQetnane
2·Butun.:ine
·,, i,1-Tricntoro,e,thanc-
Carbcn tEtrachloridc
Br·cxmdi en l ,;,r~me thane
·1, 2·0 i ch l -=rcprap.::inc
, ci:.-1,3-Dichlorcpropene
Tr~ chi o:-octhe.-1e
1 9enzcnc
, Di bro-nccn l orW,l:th,rne
:-ra~s-i , 3-· Di ch l oropro~cn,:
'.1, 1,2-T.-.ia;;ll'.oroeth.ine
Bao111cform
't.-1-+erh·1:l ·2-per:tan.::ine
2·Hc,.Dnone
·retrach l or :,~thene
i, 1,2,2-htrac,'llorocthane
~ol1....-."!ne
CJ-.\ orobcnzc,ie
E, ::hy{ bcm.ene
Styrene
:<ylene (tutal)
GP E~YIRO~ME!'ITAL
GPL LABORATORIES, LLLP P,1ge z, ORGANIC ANALYSIS RESULl'S
Matrix: IJATE.~ Anuly-;t; /.IEH
.'-!et hod: SU846 82608 Analyzed; 08/2&,98 Llnito: ug/L PreP'ri.'d:
VOLATILE ~ARGET C04POUHDS
Rt!5ul t Rr:p.L i1n. Ouel if it!r
SOL 10
SOL 10
BQL 10
BCL 10
3 5 JB
BOL 10
BOL 5
ROL 5
BOL ' BDL 5
BCL 5
BOL 5
BQL 10
SOL s
SOL 5
BOl 5
Bal
BDL 5
BOL ' SOL 5
BDL 5
BQL 5
BCL 5
aa:.. 5
BQL 10
BOL 10
SOL 5
Bel 5
BOL s
BOL
BO~ ,
BOL s
2 5
I Project: PEASOR CHEMICAL
1/w.: .. ,.
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GP ID: ~~Q8176-09E
Client ro: RCSW21
:ol ~~cted: 0S/18/98
Dilution:
Param;ter
'bi ~a-::::h l orcet/wt ).::.:tiier
Phc-m>t
2-Chlor,;,pht:nol
1,3•ricnlor~benzene
1, l. ·Ci cM l orcberi.zenc
1,Z·Dichiorob~nzcn~
2, 2 1 -oxybi s( '1 -ch l orop:op,:;ne)
?-Me:hy(phcnol
H(?;,,:a.:h I oroct!i.me
l.i-.~ it roto· di ·n· prooyl a;ni ni::-
4 -Methyl ohcnol
ijj trobe,7z1me
{~ophorcne
2·f.litros:;henni.
l, 4 ·D imethylpiv.:nct
bis(2·Lhloroccho~y~mcth~ne
2;~·0ichlorophenol
1: 2, 4 ·Tri ch', orobcnzene
NilP,'lthalene
t.-Ch:oroaniline
HJxachlorobut~dicne
,: · Ch loro-3 ·rre ti,yl phcno l
2 ·'Mcthylnaphth.l I cne
lic.x ach l crocyc l opentttdi enc
2 ,l., 6· Tr icht::irophcr.ol
2,f,5-Trichlorophcncl
2-~hloronaphth~lene
2-Ni rroanil ine
f,co/1~p'nthylen~
O imethyl pt,thi'..ll .Jte
2,0·Dinitiotol~ene
Ace'n,.iph1.hene
GPL LABORATORIES, LLLP ORGANIC ANALYSIS REStJLTS
HEitrix: UATER
M_ethod: SU846 8270.:
Uni tl>: ug/L
SS.MIVOLATILE TMGET C□MPCUt.OS
Re!':ul C R~p. L iin.
sat 1 D
BCL 10
BQL 1 D
BOL 1C
3Ql 10
BOL 10
BCL 10
BQL 10
BQL 10
3Cl 10
BOL 10
BCL 10
BOL 10
BQl 10
BCL 1i)
bQl 10
BOL 10
BOL 10
BQL 10
BOL 10
BCL 1U
SOL 10
BOL 10
act 10
BOL 10
BOL 52
"°' 10
BOL 52
BQL 10
SOL 10
BOL 10
SOL 10
An.:J t ys t: CJD
An~lyz~d: C9J02/98
Prepared: 08/25/98
Ow('l l if i er
lf!'.j U.lO
Page 16
J.J:-lJ t.ti JIJl !).:JU L~Utt
Project: REASOR CHEHlCAL GPL LABORATORIES, LLLP ORGANIC ANALYSIS RESULTS
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GP JD: 9808176-~QC
Client J[l; RCSIJ21
Cot l(•c-rc:o: 08/18/98
Di t~tion:
Parameter
3·trd trO.af"'i line
2,l·Oini~ropt,cnot
D ibenzof\,1·,::u;
2,4·0initro:alue~e
~-fl i t,opi,en:>l
Fluor.;.n~
~-Chi. or-ophenyl -ph e-n}'lec-her
Oi:t~ytphthal~tc
4-Nltroani line
~.6-Dinitro-2-methyl;:,henol
N-nitro~od\ohcnylamine
~ -Bromopt:i::nyl -phenyl erh•.:r
Hex;ich lo:·obenzenc
P(.;r-~a=h lO-"Ophcnol
?ltenanth rem:
A.nth r <.1Ccr.i:
:u,~::iaz:it e
di •n-S•.1ty 1.pi--,:halote
r•.u~r;:in{hcne
Pyr-cne
Butylcenzylphth~Lat~
'),3'-Dichlorubenzidi~c
18cnzo[ala~t~rJc~nc
Chrysene
bi~( 2-E:hylhe:wl )pt,t11a late
kl: ·n-Dcryl~rhalate
'Ben:.o(b! fluoranrhl,!':,e
3cn2o[~;fluor3nthcne
'senzo [aJ pyr-::ne
J rdeno (1 , 2. 3·cdl pyr-e:1e
Dibenz [3, !'",) .i:ithracene
Ben2o(s,~. ilp&rylen(.;
,.,-itr'ix: WATEf?
Method: .il./846 8270:
uni-.:::;: ug/L
SENIVCLArtLE TAR.CET COM?CUNOS
Fh;sul t R~.Lim.
BOL s,
BCL 5,
8Cl 10
90L 10
BOL s,
BOL 10
SOL 10
BCL 10
BQL 52
BQl 52
BQL ;a
BOL 10
BOL 10
BOL '52
BOL 1(1
BOL 10
SOL 10
10
SOL 10
BOl 10
SOL 10
BOL 11
SOL 10
BOL 10
10
BQL " SOL 10
SOL 10
BQL 10
BOl 10
BCL 10
BQL 10
Analyst; c.:o
A~s!y~cd: CQ/02/98
Prcp.:ired: 08/25/98
CluJtifier
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Pr~jccr: kEASCR CHE~ICAL
'·
GP !O '. Q80B1"/6·09
~ti cr,t iD: RCSU21
;:.arametcr
Sil ._.er
Aluminum
Ar5eni c
G,ar:U'II
B,cr-:,'i l ivm
Calcium
c.~drni um
c_ob::il,
cr1:·omium
Co:;ip,!r
J ron
N~rcury
Pota1;.,:.:.UTI
M.i9n;:::si!..'!T,
~1Jnga:-1e~c:
Sodf 1.,.m
Ni c:1::cl
~e;;id
Arl:iroony
sJlcnium
rh.all iun
·,•.:=i.nsdium
l i'r.c
Methc<l
$WBt..6 601□
s~B46 6010
SIJS.:.6 60iC
;US..6 6!110
S'.'-Sli6 6010
SU846 601Q
SU~6 6010
S0846 6010
SW84t> 6010
SU846 6010
SW846 6010
S~84b 7{.,70
SI.J846 6010
S'l.'B,6 6010
S\.l8t,.6 60i0
$UlL6 6010
SiJ.g.:,6 6010
S~846 6010
swB46 oa:o
SWS46 6010
Sl..ai.6 6010
Sw'B,46 6010
~ SW846 6010
GPL LABORATORIES, LLLP
METALS ANALYSIS RESULTS
RCS:Jl t Rep.Lim. Unit':.
BQL 3.0 ug/1.
451 200 Ug/L
aoL ,.o u9/L
20.6 10.0 ug/L
BQL 3.0 ug/L
14700 1000 ug/L
BOL 3.0 u9/L
SOL 5.0 ug/L
BOL 5.0 us/t.
BCL !=. 0 u5/L
t060 1CO U!,/L
SOL 0.20 ug/L
3020 500 ug/L
1600 5CO ug/t
70.3 5.0 u9/L
11300 500 ug/l
BOL 5.0 U9/L
60L 3.0 ug;L
SQL 5.0 ug/L
SOL 5. 0 ug/L
Bat.. 1C.~ u~/L
BOL 5. 0 -.;g/L
19.3 10.0 ug/L
Matrix: ',/ATER
Collected: On/18/98
l); ~. Preccired Ana1.yzed Bv
09/02/98 09/04/98 DOH
09/02/98 09/0G/93 OOH
09/02/98 09/0l./QS OQK
u9r02/98 09/0~/9e ODH
09/02/98 09/04/98 DDH
09/02/98 09/0,,/98 OD<
09/02/98 09/0G/90 OOH
09/02/98 09/04/98 DOIi
Q':l/02/98 D9/0!,J9e DOH
09/02/98 0~/04/'v8 ODH
09/12/98 09/04/98 no~
09/0~/98 09/06/98 LCM
09/02/98 09/J4/9S ODH
09/02/98 09/04/98 OOH
09/02/98 D0/04/9t i)DH
09/02/98 09/04/98 DOH
1 09/02/98 09/04/98 OOH
09/02/98 09/04/98 DOH
09/02/98 09/04/98 OOH
09/02/98 09/04/98 OOH
09/02/98 09/0t,./9!!, OOH
09/02/98 09/04/VB CCI-I
09/02/98 09/04/98 DOH
'l_, ___ sr}iif~4'-· a.·-.· ......
•~I',, • _, u_:~_.✓._~0:198 THU JJ:'15 F.U 301 640 1209 GP D'VI RONME-;HL
~•.✓ •:..;."'1 '•·~··'' ••
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?~c-ji.:ct: IIEASC~ CKEMI::AL
G,P ID: 9BG8176·01
Cl i en: lD: RCSE23
;>arair.etcr
r-_e,c:ent Sol i :fa
CP !D: 9003176-02
Client IO: P.CS!:24
I
~•er.:ent Sol idt
O? ID, 980B17e·C3
Client fD: RtSE25
P.ir.imctcr
Per:::ent Sol ijs
G? !D: 98□Bl76-0l
Cl i •~rit l D; KC$E26
GPL LABORATORI8S, LLLP
WET CHEMISTRY ANALYSIS RESULTS
Method Re!>ul t Re~.L i;n.
HCAWW 160.3 55.1
Method Re,:;..:l t Uni ts Ci L.
•c•w 160.3 63.o
Method Result Rep.Lim. lJr.i t~ Di l.
MCAW'i.l 160.3 67.2
Matrik: SEDIMENT
~oltected: 08/iB/98
Mutrix: SEC:MENT
C~ll&c:ed: 08/18/96
08/2?/78 JH
Matrix: SE~IMENT
CoLlcctcd: 05/18i98
Prepared Analyi:ed By
08/29/9B JH
M.:itrix: SEDlt1ENT
Collected: 08/18/98
I ~P~o~,,~•~·~~1~•~'------~----'"~•~t~h~oo,,_ __ Resu~:~'---~'~'~"~·'~i~rn~·--'~'"~;~,~•~· --~~~;~t~-~-~P~r~c~p~•~r~c~d-~A~n~o~l~1~·z~c~d~•~Y~
Pcrccr,t S:>l ids
GPILD: 9e081f6-05
Client ID: RCS£2T
Parameter
Per.cent" So\ ict;
I
GP 'lD: 9806": 76-05
C~i~~t ID: RCSE28
MCAW 160.3 M.6 '.'{ 08/29/95 JI'\
~ct hod Result Rcp.i.. im. Units
MCAVJ 160.3 28.4
Method Resu\ t
MCAW 16□ .3 65. 2
Matrix: SEOJr,',l:N1'
Collectc:d: 08/18198
0~/29/98 JS
Hatrix: SEDIMENT
Cotle~ted: OS/18/98
Prepared Analy2:ed By
08/29/98 JK
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c;p IL:: 9806176-0la
rL ient ID; RCSE.23
Cc.lle-ctcd; 08/18/95
Di \ution: iO
bi,;( 2-C.!'l l.or·o~thyl )ether
?hmol
2•:hlorcph,·nol
· ,3-Dichlv:-obenzene
1,4-Dichlorob~nzene
',2-D~chioro~~nzene
2, 2 • • oxybi $ ( 1-ch l oropropnne)
'.?-Merhylphen::.l
Kexachlorcct~s~~
1 N·~itros.:,•di-n-p:-1.lp'{lamine
~-r-tr:thylpnenol
'-itrobnzme
ISophoronc
1 2-Nitropher,ol
2, 4 ·Dimethyl phcr,ol
:lis(2·:hlnro~tho,.y)m::::t1e.nt
2,b-Oich~crophenol
i,2,~·Trichlorebcnzene
Sa;::t, t!',.::;l srie
4-:ht~roeni l ir.e
!iexa:::h l ::i...-obut.1di ene
4-cr. t oro-3-meth)•lphcno t
2-t-'.~rhyl.riaph,:nat ime
Hex~ch Lar;:;cyc l opt:r:tadi ene
2 ,l., 6-T .~) ch t oropneno l
2,➔,5·Trlthloro~hP.nol
2·Chlor-cn.11phthalen~
2·1Jitroaniiine
Accnaph ttiy t eric
Cime~hylphthalate
2,6·Dinitrotolwenc
Acenaphthent"
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
~a!rix: SEDlMtHT
Mathod; $~846 B270C
Uni u,: ug/Kg
SEMlVOLAillE TARGET COMPOUNDS
Result Rep. L i,n_
BQL 6100
BOL 6rnO
BOL 6100
BOL b1:JO
BQL 6100
SOL 6!00
BOL 6100
BOL 6100
l>Oi. 6100
BOL 6100
BCL 610il
BCL 6100
SOL 6100
BOL 61GO
BOL 6100
BOL 0°100
I)□~ 6100
SOL 6100
aaL 610D
BOL 6100
BOL 0100
BQL 6100
BOi. 6100
60L 6100
SOL 6\00
BOL 30000
B::lL 6100
GOL 30000
SOL 6100
SOL 6100
60l 6rno
SOL 61UO
t,ns•.y~t: >lN
Anal)·Zed: 09/04/98
Prepared:
au ... tif1e,-
P:,ge 2
' .•• ❖~{t~::'M~,;_..j.~_-.,-_ -~:,::·· .. ··· .. --.. · :'::~~ii~{,l~/9b 'THl' 13:~J f.U 301 S40 12<J9 GP E~VIRIJ~!IENTAL
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Prc.hct: REASOR CfJCMICAL
GP JO: YB,J,9176-0IA
Client IO: .li':CSS:23
Collected· 08/18/98
Dilution:
Puramater
Ch 1. oromc t I": ane
Sr□ll"IClmt:--:h.ine
Vi.1yl :.+'.orid-e
r;:h L ::,roeth,:1r,t
MP.thyl~n..:-ch\oride
Acetone
carbon Di~ultide
i, 1 ·Dichlor-:ieth::-nc
<, l·Oi"chloroethane
1, 2·Dict'.lcr□ethe-nc(toul)
Chloroform
1 , 2·0 1 ch l ~roet ha,ne
2-But~non~
1, 1, 1-YrichlorfJethane
Carbon tetrachloride
0 romod i ch l ::;rorr.t!" t n.!l.1e
1,2-Dic~loroprop~ne
c.is·l ,3·Dic:ilorooroi;:ene
Trichloroethene
Benzene
Di bromocitl r::-o~eth<>r:C
'tram:-1,3-0ichlo:-oproperie
1,1,2-Tr\chloroethnne
' Bromoform
'lo ·Methyl· 2 ·pi:·nt;.inonu
1 2-He>tanon("
Tetrochloroe:hene
1, 1,2,2-jetr~cnlcroe~hane
1Toll.icnc·
Ch l orcb.enz P.n<>
!:thyl~mc.•nc
sty:-cr,e
Xylene (totol)
GPL LABORATORIES, LLLP
ORGi\NIC ANALYSIS RESULTS
Matri.;: SEDIMENT
H~rhod; SWB/.6 8260B
units: ug/Kg
VOLATILE 1A-'GET CQfl1POUNOS
Resul r "lcp. l im.
60L 13
BOL 18
BC!. 13
BOL 18
12 9
SOL 1a
SOL 9
BOL 9
SOL 9
SOL 9
SOL 9
SOL 9
BOL 18
BOL 9
BOL ?
SOL 9
SOL 9
SOL 9
BOL 9
BOL 9
SOL 9
SOL 9
BO!. 9
SOL 9
SOL 18
~QL 18
SOL 9
SOL 9
SOL 9
SOL 9
BOL 9
BOL 9
EOL 9
14;020
Page 18
Analyst: JAH
An.1lyzed: 08/31/98
PreparP,C;
oust ifier
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GP ID: 9B08~76·01~
Cl icnt [D! ~CSE23
Cotlec.:~d: 08/18/98
Oj lution: 10
P."l"nmeter
3·r.itroa:,ilint
2, l,-D i nit rop:1 e-n::.:L
Di bc:nz.ofur::in
2, l. ·Dini 't ro tell L.ene
f..-~itrophcnol
Fl vorene
t. · Ch luror;hi::ny ~-phenyl ether
Di erhy\ ph ti-: c1 l i'.ltC
l.-Mitro.'..lr,il ine
~,6-D~nitro-2-methylphencl
ll-n it ro~odi phenyl ami nc
4 -Bromopr.cnyl ·phen:'l ethe:-
He;,;.~cl, 1 oroOCn!tne
Pc:ncwch l oropher.o 1•
?henc'.lnthrene
Corbazole
di-n-Butylohtnsiat~
F luoranthen!::!
Pyrcnc-
su~ylben:y !phth~l3t~
3.~•-0icnlorobenzidinc
~enzo[a!~nthr~cer.e
C:hry!'.ene
bis(2·E:hylhexyl)p":i.:hala,e
di -r.-Octyl olitha lat~
G~nio:jJfluorJntr.ene
Bcn2o(~lfluar~nthene
Benz.a[~] pyrene
;nCeno(1.~,3-cdJ7yrene
Oibenz[J,h]Jnthraeenc
Bcnio[g,h,i]pcrylene
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
~atrix: SEOJME~T
Method: SU846 8270c
Units: u9/l(g
SEMIVGLAT!LS lARGCT COMPCUNDS
Re.<;ul t Rep __ ._~ i m.
SOL 3000C
SOL 300::lO
noL 6100
OOL 6100
BOL 30000
BOL 6100
BOL 6100
BOL 6i00
SOL 30000
BOL 30000
BOL 6100
BOL 6100
SOL 6100
BQL 30000
Bal 6100
BQL 6100
SOL 6100
BOL 6100
SOL 6100
SOL 6100
BOL 6100
BOL 12000
[301. 6100
BOL 6100
BOL 6100
SOL 6100
SOL 6100
BOL 6100
BOL 6100
SOL 6100
BOL 6100
OOL 6100
Anolyst: M'-1
.t..n<Jlyicd: 09/04/95
Prepared:
ouati:ier
~005
itf'".~;;;;l;~:+i~~1~~~\~~~Tuflfiti~~~;;:,
TLI Project: 46551 Method 8280-A PCDD/PCDF Analysis (b)
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Client Sample: 9808176-01C=RCSE23 Analysis File: V110500
ClienL !"roicct:
: Sample Matri,: l TU.ID:
1
1 Sampk Si1c:
f):y Wci~k:L:
1 c·c-: c·· t -I ., .u umr::
l.2.3.t .. ,.\\;( 'L)l)
1.2 .. t.i.'7 ,:--;-11,\( '.J:D
l .:.;.t\\: _:,,;. H:,;CDI)
t .::: .3.7 .:-:.:.1.1 hC!)D
! .:.:~.➔.6.7.~-H;-,CDD
! .2.\-4.•,\ 7 _;-:_9.()CDD
: .. ~.7.~;rcu1:
\.-2.}.7.S-Pd:J)F
2..' .·I.~ .~-PcCDI'
I .::. ~.4. 7,.~. !·l.'i.CDl:
1.2..3.(,. 7,,:-,. Ex('!)~
2.~_.l..f,.7-.~-i L,CDF
l.2,_;_ i .;,.'.<.i.J-L\l 'lJl:
1.2.\-1,ii:7.,1-llrUJF
I ." . .l.-1.7 .~.'J-Hp( TJP
l .2. 3,-i-.6.'7 .. ~. t.J .t )( 'D!:
T,.>ial TU)D
lnt~LI P-.:CVD
ToIaJ l·h('D[J
TrH:tl Clp<pD
·I-.1,al TCf>F
To1al f'cdl!-'
foI:il !h{'D:-·
r~)tal HpCDF
Dioxin in sediment
SEDIMENT
216-56-1
10.010 g
5.796 g
DB-5
ND
:s/1)
1',1)
ND
ND
ND
:'iD
'-ID
!\l)
ND
ND
ND
N1)
0 80
'ii)
2.9
ND
ND
ND
r-;o
NO
0.80
Triangle Laboratories, Inc.,_,
Date Received:
Date E.~tractecl:
Date Analyzed:
DiluLiL'n Factor:
Blank File:
Analyst:
0
{)
0
0
0
0 ·r 0
0 1
0.2 cu
0.4
O .➔
o.~
0.08
O.i
01
0.2
0.2
0.2
0.2
0.4
0.2
0.4
0.8
01
0.2
Page l of 2
801 Capitola Drive• D~rtiam, North Carc,li:ia 27713
08/25198
08126198
09/01/98
n/a
VIl0l00
DD
PhGM (9191;=}7,i ;z1,9)xq~/40/y Mc,])(}Ai1!J
I -'.i
3.0
0 [,
Spike File:
!Cal:
C11nC:iL
SPSZSA50
V85822A
VI09700
'Ji: :tvloisturc: -12.1
% Lipid: n/a
'k Solius: 57.9
32: 14 J
15:34 J_
~002 ,;, . ,i
l-1. J~ C'..-Li Jl.!1 i.14U li:::I.:~
u" / ~·-~ : "
0
._;\~ilt •·•· •... ·:c,_;; ;J:;1if ::ir1•~ii/;:j:1r:'1!60f i~if:' :c~~Ep#ittji;lifie#ti1:;i~;,i\J:;i~•;i•i;:;;:,!/·y:
u
:
~
c
:
;
:
:
7
?
:
'
:
:;nn:: ULN . I
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TLI Project: .. 46551
Client Sample: 9808176-0IC=RCSE23
I Cli~nt Project:
5'1in['k Matrix:
TU!D:
Scimpk Size:
I. Dry Weight:_
GC CutLl!TH:.
j Analytes .·
:.J. i .. i'.TCDU
1.2.J. 7.8-Pe<.'DU
~ .2 .. ,.~. 7 -~ -H x.(" OD
i .2 .. ~.6. ,.8-H.-.t 'DD
1.2 .. 1. 7.8.9-H.,CiJD
1.2.:<,-l.o.~ -~-llpCDD
I .:' . .1.-U,. :}.'i-CCDD
2 . .1. ,.,-TC Dr
t .2 .. ~. 7 .~-PcCDF
2.3A. 7 .S-PeCDF
1.:'..l.-l. 7.K-r!<CDF
1.2.3.n. 7.8-HxCDF
2 .. U.6.7,S-HxCDF
1.2.3. 7.o.9-P..,CDF
l .2.J.-l.6.7,S-HpCDF
1.2.J .... 7.8.9-HpCDF
1.2.J.-l.6.7 .8.9-OCDF
Dioxin in sediment
SEDIMENT Date Rcc~ived: 08/25/98 216-56-1 Date Extracted: 08/26/98
Date Analyzed: 09/01/98
10.010 g
5.796 g
DB-5
Dilution Factor: 1
Vl10100
DD
Blank File:
Analyst:
.... · C Cone; (ppb) /TEF' >.•. .'
ND X I. = ND X 0.5 = ND X 0.1 = NO X 0. l = ND X 0.1 = ND ' O.QI = [ 1.8\ X 0.00! =
ND X 0.1 = :S1) X 0.05 = ND X 0.5 = ND X 0.1 = ,S:D X 0.1 = ND X 0.1 = ND X 0.1 = 0.80 X 0.0l = ND ' 0.01 = 2.9 X 0.001 =
Toxicity Equivalents Repor
Analysis File: VI1050(
Spike File:
[Cal:
ConCat:
% i\'1c>islllre:
'lo Lipid:
'lo Sulids:
. • Equivalent
ll.001~
0.0080
SP82SA50
V35822A
V109700
42.l
n/a
57.9
Total 2,3.7,S-TCDD Toxicity (1989 !TF) Equivalents: 0.0127 ppb
(1) Detection Limits not used in calculations. Note: 100% of EMPCs are used in the calculations.
[ ... ] indicates that the value Is that of an EMPC.
Triangle labo_ratories, Inc.-, 801 Capitola Drive• Curharn. North Carolina 2n13 Phone: [phone] • Fax: [phone]
Page I of 1
Printed: 15:24 09/03/98
ib\ 67
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Project: REASOR C~CMICAL
. .:-:-~ .':.:.:·1
GP JD: 9BG8176-02A
Client !D: RCSE24
Collected: 08/18/98
Dilution:
C~ lor-one:hane
Bram::.methtme
Vin~-•-chl.oridc
Ch 1 orol? th.;,nc
Methylene chloride
At.cton::
C.arbon Disulfide
1, l·Dich\oroetnene
i, 1-?i:hlorocth.Jnc
1 ·r,2·Di::hloroethene(total)
Chloroform
t,2·DichlorocthJnc
I 2·Butanone
1 , 1, 1 ·Tr i!:td orof:t."lar.e-
C orb~n tc:rcchloridc
9 roo1odi ctl i. orOffM?thane
, 1,2-DichloropropRne
c is· l, 3-D i ch 1_ oropropc-nt
Tri ch lorocthcnc:
Benzene
Di b,~::,.1l0ch \ oromethanc
trans-1,3·Dichloropropene
i,1,2·Trichtoroethan~
Br001oforrn
'4 • Mc::hyl -2 ·p<.-nti'.lnonc
' 2·Hexanol"'e 1 etrach l oroe :h ,me
1,1,2,2-Tctr~chlorocthanc
To I •Jene
ch l orobenzene
E_':hylbc:nzcnc:
S :vrene
xylem~: (tor<1l >
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
Matrlx: S[OlMENT
Mc:thod: S\.1846 B.260B
Unit~: ug/(g
VOL.t.ilLE T.P.RGET COMPCWlDS
Re!.Ul t Rep.Lfo~.
SOL 16
SOL 16
so, 16
SOL 16
6 8
62 16
BOL 8
BOL 6
BOL 8
SOL 8
BOL 8
SOL 8
BQL 16
BOL 8
BOL s
ioL 8
BOL 8
BQL 8
BOL 8
SOL 8
BOL 8
SOL 5
BOL B
BOL e
SOL 16
SOL 16
BOL 8
BQL 8
SOL 8
SOL 8
BOL s
BOL 8
BOL 6
Analyst: JAH
Analyz~d: 08/31/QB
Pr-epared:
Qua~ifier
Pas~ 19
I
Projec~:
I . ".')
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GP :o: 9808176·028
:I 1ent 1D: RCSE2~
Ct;ille::te::!: ll8/18/98
I l)i ll!~iO:"',; 10
Pc1r.t.1,l11.!tCr
bi~(2·:hlorocthyl)ether
f'hmol
2-Ch l or0ci'lcno l
l ,J-D·:ct-:lorobcnzene
1,L.-~icnlorobenzcne
1,2-0icn\orobenzene
'~ • .2• -c..:ybi:,(1-chloror,rop.'.lnc) ' i 2 · M~:hytphcnol
Hcxochloroethane
1 "-Ni tr"osc· ·di ·n·propy l ,11ni ne
1 ~-Metny '. pl-:c, ,oi.
'I-! i trc.oenzene
1 J :.::i:f,crcnc
2-i-i i ::ropl-:e:-ial
'2, 4-D i1r.ct hYL;:t\eno! ' bis{2-Ch1.oocc-thoxy)methane
,2, 4 ·O i ch L or-op>lcnol
,1, 2, 4 · l r ·i ,:n ~arobe:n u:n~
1-aphth.Jlt."ne
L.-cr.\oroani l ir"lc
H~A~chlorabutadi~ne
~-Chloro·3-methylphenol
2~Meth1lnaP,thnlene
~e~acnlorocyclopentadicnt
2,~,6·Trichlcrophe~ol
2,4,S·Tric.hlorophcnol
~-Chlorona~hth~lcne
~.-Mi ~roani I i:ie
/'..cenapht!iylcric
D,ime~hyl;=ihtha l ut-::
2·, 6· o i ni trctct uenc
Acen.aphthcnc
GP E:-lV IRO"l!IE:-IT.'\L
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
Matri1.: SEOlMENT
Method: S\.1846 8270C
Uni-::i:.: u9/K9
SEMIVDLATIL~ TARGET COMPOUNDS
Result Rep.l i111.
SOL 5300
BC:L 5300
aoc '5~00
SOL 5300
SOL ~300
BOL 5300
BOL 130Q
BOL 5300
BQL 5300
BCL 5300
SOL 5300
BOL 5300
BOL 53CO
BOL 5300
BOL 5300
SOL 5300
SOL 5300
BOL 5300
BOL 5300
BCL 5300
BCL 5300
SOL 53CO
BCL 5300
BOL 5300
BQL 53(10
BOL 26000
SOL 5300
60L 26000
BOL 5300
BOL ~JOO
Bi:li. 5300
BCL 5300
Ant1lyst: J.IM
A;ialyzed: 09/04/98
Prepared:
Ouafifier
Ii/] 006
'fHll lJ: 41 t-· • ..1_..1 JUl i)-lU l:!U~ lit' t.'H lKU.'IM..t.tfl.'\.L
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·t~i'roject: REASOR CHEMICAL
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GP 10·: 9808176-028
Client iD: RCSE24
Col lect:-0: 08/18/9B
Gilutir.in: 10
;'.lnra_mctcr
3·Nitroanil"ine-
2, W ·Dini t-ropht:11,;,I
Di ben:.:cfuran
2, .;.-o i r.l t rote l uene
1. ·Nit rophcno l
Fl 1,;orene
1.-Chlorcpheny!-oh~nylcther
DietnvL~th;1late
4-Nitre,3niline
~.6-Din\:rc•2-methylphcno~
N-nitroscdiphenylarnin~
4-Bromophenyl-phcnylether
rleT.achlorobenzene
Pentachlorop~enol
?h•~nanthrenc
Ant,ir.:icene
Caroazolc
di·n-Butylphthal~te
ft~oranthe:,c
ry,cne
3utylbcnzylp~:h~tatc
3,3 1 -Dichlore,O~nzldinc
1 3.::nz.olJJ anthr.l:cn~
1 Chry:.t:.-ne
: ois(2-E::hyihexy1.)phtf1~!.Jte
'di ·n·Oc:tyLpl,t!H1l8te
I Bento [b] f \ uorant"lcn•~
I B~nzo!k] fi;.i,)r~nrhene
Benz.o {JJ pyren~
11nct~:io[:,2,3·cd;pyrent
i Di b-:nz re, h) .mth,•.iccne
Benzo [g ,h, i 1 per/le:,e
GPL LABORATORIES, LLLP
ORGANIC ANALYSIS RESULTS
Matrix: SEOIMENT
Method: S~Bf.6 B270C
Unit:s: ug/Kg
SEHlVOLAilLE 7ARGET CG.',.P(JJI.DS
Result Rec..l ',m ..
aoL 260CO
BOL 26000
BOL 5300
BCL 5:SGO
3::L 260)0
SOL 5300
801. 53D0
SOL 5300
BOL 26000
BOL 2t.OOO
BOL 5300
BOL 53JO
BOL 530G
BOL 26000
BOL 5300
SOL s~oo
SOL 5300
BOL 5300
8,Q~ 53CO
BOL 5300
~CL 5300
BCL 11000
s;.L 5300
sa,. 5300
SOL 53CO
SOL 5300
BDL 5300
BOL 5300
SOL 5300
SOL 5300
SOL 5300
bOL ~JOO
Anulyfit: I-IM
Anatyz:ed: 09/0(,./98
Pre-p;ired:
C.ua_l if i er
Page 5
,/,~}f~/'~~;~;· lJi~;-~·;;·~~ t'.~ JUl ij4~ HU9 GP DVlRU~!IE.~TAL 14)033
l!l' ,,., -.-· i~::r :t:m:~ri:1/[tliiftll~!tl-l~i~~li~Ji;~]J~j-tl:.~'tlmrnl!~iiii~~~Ilti~l~~tlilf:1~[t1ff WI:l:itt
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TLf Project: 46551 .l\.1ethod 8280-A PCOD/PCDF Analysis (b)
Cli~nt Sample: 9808176-02C=RCSE24 Analysis File: VI10600
Clii..'!1l Pruj~ct:
S:impk 11,iati'ix ·
TLIID
' S;,rnpk S',zc:
Dry Wt:igt,:
· GC G\1lumn:
Dioxin in sediment
SEDIMENT
216-56-2
10.040 g
6.406 g
DB-5
Date Re,:eivt:d:
Date Exrrncr.ed:
Dale Analyzed:
Dilution Factor:
Blank Fiie:
Analyse:
08/25/98
08/26/98
09/01/98
n/a
VI10100
DD
Spik~ Fik:
[Cai:
ConCal:
% CvlL,istul"'~:
% Lipid:
'k Snlids:
SP828ASO
V85822A
VI09700
36.3
n/a
63.8
Analyies _ " •• , -..>, cBiif,: (ppb), · ,,C:,/:!'C?'EMP.C -: --• .· Ratio. ,w • ::RT':.· :_F_la_ gs_· __ · • :.,, ... ,, . ._,,_.:_':·".
: __ ;_7_s:rcr.>D
t .2. -~-;_,\-!\;{.'.DI)
1 . .2 .. \..i.: 5-11:\(.l)I)
f -~-.',!-.. 7,,\'-! !x( :DD
l. ~-_\_: .:.,: __ :i-HxCI )D
1.2 .. ) . .!.h. 7 -~-!ire ~DD ' ! .2 .. t...:.<,.7 _;,:_q_()('.;)D
2 __ :;_ ;_~--l·'CDf:
l .2 .. ~. 7 . .'f-PL{:DF
2.3A. 7,,\~Pi.::CD!:
1.2.3.4. 7 ;:,:.1 !.-.CDF
! .2..1J,.7 .X-1 l:,::(J)l:
23.-1.t\. 7.~-fl,('[)f,
1.2 .. ;, i.:<.1)-C-[;,;( :ur-
1.2.~-➔-('),/ •. ~-H;:-CDr
! .2.J.-L7 .~:.'J-I t;-,(DF
'. .2. ;_ ... u-,. 7 .~.1)-0C.!JI:
To1a1 TCDD
fo1:iJ Pd'.DD
Tni:.J.! Hx( :DD ·,·,_,,,,1 HpCD[l
l'm:iJ T(TJc
l1llal PcC[)['
"l°ill:tl I lxCJJF
To1:tl I ipq:>F
Triangle Laboratories, Inc.,,
:--ID
:'W
ND
,'<D
ND
N[)
i.S-
:-,/!)
:-ID :n:,
'.'ID
'.'ID
'.'II)
ND
;'\i'U
ND
I\!)
r-;n
NJ)
ND
ND
ND
NT)
801 Capitola Olive• Durham, North Carolina 27713
Phone: (919) 54'1-5729 • Fax: [phone]
O.Ofi
G.10
O.~
Ii I
0.1
0.3
J
() 05
007
0.0i
() 2
II I
0.2
0.2
0,2
0.3
0.8
0
0 O.lO
0 0.J
0 0.3
0 0.09
0 0.07
0 0.1
0 0.2
Page I of 2
Printed: 12:02 09/03/98
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TL[ Project:
Clic~t Sample:
46551
9808176-02C"'RCSE24
l\.1ethod 8280-A PCDD/PCDF Analysis lb)
Analysis File: VI10600
Clic~I Prnj~cl:
Sam pk Matrix:
TUID
S;,mpk Size:
Dry Wt:igh1:
, CC Culumn:
2.,.:. S-'l'Cl'.>D
t .2. ,;. ; .:,;-!\.:( '.!)!)
I ,] __ ;A. 75-1 !x(.DD
{ .~ .. ~. t,. 7 .K-1 !x( :J)D
I. c .. 1.: .'-.'i'-1 M"I ll'>
I .~_.\.!.h. 7'.~-! tr< ~DD
i .2 . .'.-:.fl. 7 :,~-I.).{)( :;JD
2.3.? .~.'['C'[)f:
I.~ .. ~. 7):•PL{])F
~.3A. 7 ,;,;. Pi,;;CD r:
! -~-3.4. 7 .~. ! \,:( :01:
I.~. _1 _fi, 7 .1'<-I hCDI;
:2 .. ,.-1.6. 7.~-\lxr"!)f-
1. 2.3. 7 .:-<. ') · f"Ix( :ur-
1 "') ., t ... J 11 ('[)" , ___ .~ ... ,n.,.,.-· p. r·
[ .2.\-f.7 );_rj.f Ip( l)f
'. .2 __ -;_.u-.. 7 .~(:1.()(:f)F
Tnwl TCDD 1
focol Pd'.DD
Tnc.J..I H.\( '.DD
T:11:,I HpCDD
rm,1·rc.T1c '
rowJ PcC[!F .
Tot:cl I lxC:DF
Tot:JJ llp< 'DF
Dioxin in sediment
SEDIMENT Date Re,;~ived: 08/25/98 216-56-2 Dale Extrnci:ed: 08126/98
Date Analyzed: 09/01/98
10.040 g
6.406 g
DB-5
:m
ND
ND
ND
ND
ND
I ~-
.'ITJ
ND
Wl
NU
ND
ND
ND :-.u
ND
I\'!)
1-,'T)
ND
NT.J
ND
ND
rvn
Dilution Factor: n/a
Vl10100
DD
Blank Fiie:
Analyst:
0.06
G. I 0
()_~
tl.l
0.1
0.3
n.os
007
o.Oi
IJ.2
ll. I
o.~
().2
0,2
O,
0.8
0
0 0.10
0 0.1
0 0.3
0
0 ll.Q7
0 0.1
0 0.2
Page 1 of 2
Triangle Laboratories, Inc .. ,
B01 Cc1pitola Drive • Durham. North Caroiina 27713 Phone: (919) s'.4A-5729 • Fax: [phone]
1 -__ .,
0.09
Spiki; Fik:
[Cai:
ConCaJ:
% ML>ismrs:
% Lipid:
'7r. Snlids:
SP828AS0
V85822A
VI09700
36.3
n/a
63.8
I_
Printed: 12:02 09103/98
'•jftk r,ll
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TL[ Project:
Clie,nt Sample:
Client Prnj~c:L
! Sampk ~btrix: ITU 1,0 -
i SJnipk Si'l~: I Dry \V~i~hl:
i GC Column:
\ Analytes
2.J.7.':'--ll:DD
1.2 .. 1.;_~-PcCDD
1.2 .. 1 . .J,; -~-11\('l)J)
. 1.2 .. ,.~.7.i-Jh<'D!)
I .:: .. ,. 7., .'',I l ,1.TJ))
1.2 .. ~ . .l/,. :._.~-1 !p( 'DD
! .: .. 1 .-U1. ~:~. 'H H.'DD
2 .. 1. 7.~-TCDF
1.2._;, 7.zi-P~cui:
2 .. :..~. i .:,i-?::iCD/"
1.2..' . .J.7 .'<-HxCDF
l .~._;_fi_ 7.,\-HxlD~·
2 .. 1 .-1.!1. 7 .,-Hx<.'DF
1.2.~.1-~ .'.i-HxCL)F
1.2 .. 1..J.6.?. ,-i·lpCDF
1.2 .. 1 . .J." X 'J-1 lp(.'c)c"
1.2.. _;_.;.,ti.::-.. ,:.\'·( ,c :or-
46551
9808176-02C=RCSE24
Dioxin in sediment
SEDfMENT Date Received: OS/25/98 216-56-2 Date Extracted: 08/26/98
Date Analyzed: 09/01/98
10,040 g
6.406 g
DB-5
ND
:-,'I)
ND
r-.1)
NO
ND
I.~
t\'D
1\1)
ND
ND
NO
ND
ND
ND
t\'l)
ND
Dilution Factor: 1
Vl10100
DD
Blank File:
Analyst:
X
X
X
X
X
X
X
X
X
X
l.
0.5
0.1
0.1
0.1
001
0.001
0.1
0.05
0.5
0.1
0.1
0.1
O.l
0.01
0.01
0.001
=
=
=
=
=
;
=
= =
=
=
=
=
=
=
141 00 J
Toxicity Equivalents Report
Analysis File: VI10600
Spike File:
!Cal:
ConCal:
'7o Moisture:
% Lipid:
o/c Solids:
Equivalent
0.001 X
SP828A50
V85822A
V109700
36.3
n/a
63.8
I
I
I
I
I
I
I
I
Total 2,3,7,B-TCOD Toxicity (1989 ITF) Equivalents: 0.0018 ppb
(1) Detection Limits not used in calculations. Note: 100% of EM PCs are used in the calculations.
I
I , riangle Laboratories, Inc.,, 801 Capito:a Drive• Durham. North Carolina 2TT13 I Phone (913) 544,5729 • Fax: [phone]
Page l of l
Printed: 15:24 09103198(:,'v.,,{
. . 1 I)'.:;:
- - - - -
EXTRACTAB' -c; SAMPLE ANALYSIS -------EPA -REGION IV S<'-'1, ATHENS, GA ------Amended Date: 02/"~'98 12:50 -
Sample 12924 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Numb_!'!r:_25655
Id/Station: RCSEDUP1 -
Media: SOIL D Number: MY86
RESULTS UNITS ANALYTE
580U UG/KG PHENOL
580U UG/KG BIS(2-CHLOROETHYL) ETHER
580U UG/KG 2-CHLOROPHENOL
580U UG/KG 1,3-DICHLOROBENZENE
580U UG/KG 1,4-DICHLOROBENZENE
580U UG/KG 1,2-DICHLOROBENZENE
580U UG/KG 2-METHYLPHENOL
580U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
580U UG/KG (3-AND/OR 4-)METHYLPHENOL
580U UG/KG N-NITROSODI-N-PROPYLAMINE
580U UG/KG HEXACHLOROETHANE
580U UG/KG NITROBENZENE
580U UG/KG ISOPHORONE
580U UG/KG 2-NITROPHENOL
580U UG/KG 2,4-DIMETHYLPHENOL
580U UG/KG BIS(2-CHLOROETHOXY)METHANE
580U UG/KG 2,4-DICHLOROPHENOL
580U UG/KG 1,2,4-TRICHLOROBENZENE
580U UG/KG NAPHTHALENE
580U UG/KG 4-CHLOROANILINE
580U UG/KG HEXACHLOROBUTADIENE
580U UG/KG 4-CHLORO-3-METHYLPHENOL
580U UG/KG 2-METHYLNAPHTHALENE
580U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
580U -UG/KG 2,4,6-TRICHLOROPHENOL
1400U UG/KG 2,4,5-TRICHLOROPHENOL
580U UG/KG 2-CHLORONAPHTHALENE
1400U UG/KG 2-NITROANILINE
580U UG/KG DIMETHYL PHTHALATE
580U UG/KG ACENAPHTHYLENE
580U UG/KG 2,6-DINITROTOLUENE
1400U UG/KG 3-NITROANILINE
580U UG/KG ACENAPHTHENE
1400U UG/KG 2,4-DINITROPHENOL
1400U UG/KG 4-NITROPHENOL
580U UG/KG DIBENZOFURAN
" 580U UG/KG 2,4-DINITROTOLUENE -580U UG/KG DIEtHYL PHTHALATE
Org Contractor: AA TS
RESULTS
580U
580U
1400U
1400U
580U
580U
580U
1400U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
43
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beglnning: 08/25/97
Ending:
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE -
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitalion limit.
R-qc indicates that dala unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
£-;-confinned by gems: 1.when no value is reoorted. see chlordane constituents 2.consliluP.nts or metabolites of technical chlordane
-
EXTII -h-tAtl!lliSA_, A~IS --Sample 12924 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSEDUf:'1
Media: SOIL-D Number: MY86
RESULTS UNITS ANALYTE
580U UG/KG PHENOL
580U UG/KG BIS(2-CHLOROETHYL) ETHER
580U UG/KG 2-CHLOROPHENOL
580U UG/KG 1,3-DICHLOROBENZENE
580U UG/KG 1,4-DICHLOROBENZENE
580U UG/KG 1,2-DICHLOROBENZENE
580U UG/KG 2-METHYLPHENOL
580U UG/KG BIS(2-CHLOROISOPROPYL) ETHER
580U UG/KG (3-AND/OR 4-)METHYLPHENOL
580U UG/KG N-NITROSODI-N-PROPYLAMINE
580U UG/KG HEXACHLOROETHANE
580U UG/KG NITRO BENZENE
580U UG/KG ISOPHORONE
580U UG/KG 2-NITROPHENOL
580U UG/KG 2,4-DIMETHYLPHENOL
580U UG/KG BIS(2-CHLOROETHOXY)METHANE
580U UG/KG 2,4-DICHLOROPHENOL
580U UG/KG 1,2,4-TRICHLOROBENZENE
580U UG/KG NAPHTHALENE
580U UG/KG 4-CHLOROANILINE
580U UG/KG HEXACHLOROBUTADIENE
580U UG/KG 4-CHLORO-3-METHYLPHENOL
580U UG/KG 2-METHYLNAPHTHALENE
580U UG/KG HEXACHLOROCYCLOPENTADIENE (HCCP)
580U .UG/KG 2,4,6-TRICHLOROPHENOL
1400U UG/KG 2,4,5-TRICHLOROPHENOL
580U UG/KG 2-CHLORONAPHTHALENE
1400U UG/KG 2-NITROANILINE
580U UG/KG DIMETHYL PHTHALATE
580U UG/KG ACENAPHTHYLENE
580U UG/KG 2,6-DINITROTOLUENE
1400U UG/KG 3-NITROANILINE
580U UG/KG ACENAPHTHENE
1400U UG/KG 2,4-DINITROPHENOL
1400U UG/KG 4-NITROPHENOL
-'<:\ 580U UG/KG DIBENZOFURAN
580U UG/KG 2,4-DINITROTOLUENE
\ 580U UG/KG DIETHYL PHTHALATE
Org Contractor: AA TS
RESULTS
580U
580U
1400U
1400U
580U
580U
580U
1400U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
580U
43
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97
Ending:-
UNITS
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UGIKG
UG/KG
UGIKG
UGIKG
UG/KG
UGIKG
UG/KG
UG/KG
%
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINEIDIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENzyLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
% MOISTURE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is~ -~,...,..n to be less than value given. L-actual value is known to be greater lhan value g•·· ~ U-material was analyzed for but not detected. the number is the minimum quan"" "'•m limit.
R-qc indicales th a unusable. compound may or may not be present. resarnpling and reanalysis essary for verilication.
C-confirmed by g._ . --· 1.when no value is reported. see chlordane constituents 2.constituents or metaL. -· .cs of technical chlordane
- - - - -
EXTRACTAB' ' SAMPLE ANALYSIS ------·-EPA -REGION IV SF-"1, ATHENS, GA -Sample 12924 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility:· REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655 -
Id/Station: RCSEDUP1
Media: SOIL D Number: MY86
RESULTS
5000JN
6000J
ANALYTE
BORNEOL
ALKANES
25 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
100000J
10000JN
5000JN
UNITS
UG/KG
UG/KG
UG/KG
UG/KG
UG/KG
SUBSTITUTED PENANTHRENECARBOXYLIC ACID
NORTRACHELOGENIN
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97
Ending: . .
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R.qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r:-confirmed by Qcms: 1 .when no value is reoorted. see chlordane constituents 2.constituents or metabolites of technical chlordane
-
- - - -
VOLATILES SAMPLE ANALYSIS -
Sample 12924 FY 1997 Project: 97-0357
VOLATILES SCAN
-
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSEDUP1
Media: SOIL D Number: MY86
RESULTS UNITS
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
40U UG/KG
18U UG/KG
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
- - - - -
EPA -REGION IV SESD, ATHENS, GA
Org Contractor: AA TS
18U UG/KG
18U UG/KG
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
18U UG/KG
18U UG/KG
18U UG/KG
18U UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
18UJ UG/KG
43 %
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
. METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
% MOISTURE
- -------Production Date: 12/11/97 07:49
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25/97
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
K-actual value is kr-·••n to be less than value given. L-actual value is known to be greater than value giVP" LI-material was analyzed for but not detected. the number is the minimum quantit;ition limit.
R.qc indicates the unusable. compound may or may not be present. resampling and reanalysis ii ssary for verification.
C-confirmed by gc.. . 1.when no value is reported, see chlordane constituents 2.constituents or metab~ . _ .; of technical chlordane
--------EPA -REGION IV S►"O, ATHENS, GA - -- - - -
Amended Date: 021"~'98 11 :20
Sample 12924 FY 1997 Project: 97 -0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655 ..
Id/Station: RCSEDUP1
Media: SOIL D Number: MY86
RESULTS UNITS
40JN UGIKG
50J UGIKG
ANALYTE
METHYL (METHYL ETHYL) BENZENE
1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08125197 .
Ending:
K-actua1 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r .. r:onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-
--- - - - -
EPA -REGION IV SESD, ATHENS, GA --- - - - -
Production Date: 12/11197 07:49
Sample 12924 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Facility: REASOR CHEMICAL
Progr_am:_NSE _
Id/Station: RCSEDUP1
Media: SOIL
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY86
RESULTS
40JN
50J
UNITS
UG/KG
UG/KG
ANALYTE
METHYL(METHYLETHYL)BENZENE
1 UNIDENTIFIED COMPOUND
Org Contractor: AA TS
!\-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material.
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
_Beginning: 08/25/97 ..
Ending:
<-actual value is I<" , to be less than value given. L-actual value is known to be greater than value gi· LI-material was analyzed for but not detected. the number is the minimum quanf
~-qc indicates th< unusable. compound may or may not be present. resampling and reanalysis i( ssary for verification.
::-confirmed by go,. ___ · 1.when no value is reported, see chlordane constituents 2.constituents or metabo .. ,c:S of technical chlordane
1 limit.
-
--Sample 12929 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL
Progr_am: NSF
CASTLE HAYNE,_NC
Case Number: 25655
· Id/Station: RCSWDUP1
Media: SURFACEWA D Number: MY90
RESULTS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
2J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
_UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
-Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25197
Ending:
A-average value. NA-not analyzed. NA1-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantilation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or melabolites of technical chlordane
-
- - - - -
✓OLA TILES SAMPLE ANALYSIS
Sample 12929 FY 1997
VOLATILES SCAN
Project: 97-0357 -
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSWOUP1
CASTLE HAYNE, NC
Case Number: 25655
Media: SURFACEWA D Number: MY90
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
- - - - -
EPA -REGION IV SESD, ATHENS, GA
Org Contractor: AA TS
RESULTS
2J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U -1ou
10U
10U
10U .mu
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
1bu
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
OIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--- - - - -
Amended Date: 02/02/98 11 :20
Produced by: Denise Goddard
Requestor: RAY DOYLE_
Projecf Leader: DOYLE
Beginning: 08/25/97
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is!--, to be less than value given. L-actua1 value is known to be greater than value g(, U-material was analyzed for but not detected. the number is tt1e minimum quanti' '1 limit.
R-qc indicates th< , unusable. compound may or may not be present. resampling and reanalysis it ,ssary for verification.
1"'.-confimied by gen,:,: 1.when no value is reported, see chlordane constituents 2.constituents or metabo11,dS of technical chlordane
-
------------ri>A -~ION IV SF~t"J, ATHENS, GA - -- - - -
Amended Date: 02/fl.,198 12:50
Sample 12929 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: REAs·o-R CH.EMICAL-CASTLE HAYNE, NC
Program: NSF Case Number: 25655
ld/Slalion: RCSWDUP 1
Media: SURFACEWA D Number: MY90
RESULTS
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
.10UJ
10UJ
10UJ
25UJ
10UJ
25UJ
25UJ
10UJ
10UJ
10UJ
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-AND/OR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26, 1984)
Org Contractor: AA TS
RESULTS
10UJ
10UJ
25UJ
25UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ ·
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
Produced by: Denise Goddard
Requeslor: RAY DOYLE
Projecl Leader: DOYLE
Beginning: 08/25/97
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE .
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates thal data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituenls or metabolites of technical chlordane
-
Sample 12929 FY 1997 Project: 97 -0357
EXTRACT ABL~S S~AN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSWDUP1
Media: SURFACEWA D Number: MY90
RESULTS UNITS ANALYTE
10UJ UG/L PHENOL
10UJ UG/L BIS(2-CHLOROETHYL) ETHER
10UJ UG/L 2-CHLOROPHENOL
10UJ UG/L 1,3-DICHLOROBENZENE
10UJ UG/L 1,4-DICHLOROBENZENE
10UJ UG/L 1,2-DICHLOROBENZENE
10UJ UG/L 2-METHYLPHENOL
10UJ UG/L BIS(2-CHLOROISOPROPYL) ETHER
10UJ UG/L (3-AND/OR 4-)METHYLPHENOL
10UJ UG/L N-NITROSODI-N-PROPYLAMINE
10UJ UG/L HEXACHLOROETHANE
10UJ UG/L NITROBENZENE
10UJ UG/L ISOPHORONE
10UJ UG/L 2-NITROPHENOL
10UJ UG/L 2,4-DIMETHYLPHENOL
10UJ UG/L BIS(2-CHLOROETHOXY)METHANE
10UJ UG/L 2,4-DICHLOROPHENOL
10UJ UG/L 1,2,4-TRICHLOROBENZENE
10UJ UG/L NAPHTHALENE
10UJ UG/L 4-CHLOROANILINE
10UJ UG/L HEXACHLOROBUTADIENE
10UJ UG/L 4-CHLORO-3-METHYLPHENOL
10UJ UG/L 2-METHYLNAPHTHALENE
10UJ UG/L HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ UG/L 2,4,6-TRICHLOROPHENOL
25UJ UG/L 2,4,5-TRICHLOROPHENOL
10UJ UG/L 2-CHLORONAPHTHALENE
25UJ UG/L 2-NITROANILINE
10UJ UG/L DIMETHYL PHTHALATE
10UJ UG/L ACENAPHTHYLENE
10UJ UG/L 2,6-DINITROTOLUENE
25UJ UG/L 3-NITROANILINE
10UJ UG/L ACENAPHTHENE
25UJ UG/L 2,4-DINITROPHENOL
""'0 25UJ UG/L 4-NITROPHENOL
10UJ UG/L DIBENZOFURAN -10UJ UG/L 2.4-DINITROTOLUENE C) 10UJ UG/L DIETHYL PHTHALATE
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
Org Contractor: AA TS
RESULTS
10UJ
10UJ
25UJ
25UJ
10UJ
10UJ
10UJ
25UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
10UJ
- -
Produced by: John Mcconney
_ Requestor:_RAY DO_YLE _
Project Leader: DOYLE
Beginning: 08/25/97
Ending:
UNITS ANALYTE
UG/L 4-CHLOROPHENYL PHENYL ETHER
UG/L FLUORENE
UGIL 4-NITROANILINE
UG/L 2-METHYL-4,6-DINITROPHENOL
UG/L N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
UG/L 4-BROMOPHENYL PHENYL ETHER
UG/L HEXACHLOROBENZENE (HCB)
UG/L PENTACHLOROPHENOL
UG/L PHENANTHRENE
UG/L ANTHRACENE
UG/L CARBAZOLE
UG/L DI-N-BUTYLPHTHALA TE
UG/L FLUORANTHENE
UG/L PYRENE
UG/L BENZYLBUTYLPHTHALATE
UG/L 3,3'-DICHLOROBENZIDINE
UG/L BENZO(A)ANTHRACENE
UG/L CHRYSENE
UG/L BIS(2-ETHYLHEXYL) PHTHALATE
UG/L DI-N-OCTYLPHTHALA TE
UG/L BENZO(B AND/OR K)FLUORANTHENE
UG/L BENZO-A-PYRENE
UG/L INDENO (1,2,3-CD) PYRENE
UG/L DIBENZO(A,H)ANTHRACENE
UG/L BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-inlerferences. J--estimated value. N-presumptive eVidence of presence of material.
K-actual value is 1-:r-~·-,n to be less than value given. L-actual value is known to be greater than value gi·r" U-material was analyzed for but not detected. the number is the minimum quantiJ;:,lion limit.
R-qc indicates th< 1 unusable. compound may or may not be present. resampling and reanalysis i issary for verification.
C-confinned by QL. _ 1.when no value is reported, see chlordane constituents 2.constituents or metaL .. ::> of technical chlordane
EXTlll'1-AsSilllSAr1iW A~IS --Sample 12929 FY 1997 Project: 97-0357
MISCELLANECJUS ~QMJ>OUNDS
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSWDUP1
Media: SURFACEWA
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY90
RESULTS
20JN
. 30J
UNITS
UG/L
UG/L
ANALYTE
TETRAMETHYLPHENANTHRENE
2 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
--- - - - -
Production Date: 1211 1 197 10:16
Produced by: John McConney
Requestor: RAY DOYLE-
Project Leader: DOYLE
Beginning: 08/25/97
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence or presence of material.
K-actual value is known to be less lhan value given. L-actual Value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-conftrmed by gems: 1.when no value is reported, see chlordane constituents 2.constiluents or metabolites of technical chlordane
-
--------- - - - -
EPA -REGION IV SESD, ATHENS, GA Amended Date: 02/02/98 12:50
Sample 12929 FY 1997 Project: 97 -0357
MISCELLANEOUS COMPOUNDS-
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCSWDUP1
Media: SURFACEWA
CASTLE HAYNE, NC
Case Number: 25655
D Number: MY90
RESULTS UNITS
20JN UG/L
30J UG/L
ANALYTE
TETRAMETHYLPHENANTHRENE
2 UNIDENTIFIED COMPOUNDS
Org Contractor: AA TS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Denise Goddard
Requester: RAY DOYLE -
Project Leader: DOYLE
Beginning: 08/25/97
Ending:
K-actual value is 1<-··•n to be less than value given. L-actual value is known to be greater than value gi•· U-material was analyzed for but not detected. the number is the minimum quanF' ·"'"limit.
R--qc indicates th; 1 unusable. compound may or may not be present. resampling and reanalysis i: issary for verification.
C-confirmed by ge,,. ___ 1.when no value is reported, see chlordane constituents 2.constituents or metab ...... c:s of technical chlordane
-
- -
VOLATILES Se_l'{IPLE ANALYSIS EPA -REGION IV SF.<;O, ATHENS, GA Production Date: o": -.•gs 16:26 iJ27 '· I ' -----~-----------------------------------------------'"-' Sample f253 FY 1998
VOLATILES_S.CAN. _.
F acilily: Reasor Chemical
Program: SSF
Id/Station: RCSWDUP1A
Media: GROUNDWA
Project: 98-0105
Castle Hayne, NC
Case Number: 25902
MD Number: NE93
D Number: NE96
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISO BUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by:Denise ·Goddard
Requestor: Jennifer Wendel
Project Leader:
Beginning:
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence ot material. K-actual value is known lo be less than value given. L-actual value is known to be greater than value given. U-malerial was analyzed for but not detected. th·e number is the minimum quanlitation limit. 0 ,,,. i.-...fl,.-1 .. ~ lh~o _._,_ -•-••--L• • • •• · · · ·
--Sample 12774 FY 1997 Project: 97-0355
VOLATILES SCAN
Facility: REAS()R CH_EMIS::AL_. CASTLE HAYNE, NC
Program: NSF Case Number: 25645
Id/Station: RCSSEB2 MD Number: MX16
Media: WATER D Number: MW35
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
.. 10U
10U
10U
10U
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
-Produced by: Keith Bates
Requestor: RAY DOYLE
Project-Leader: DOYLE
Beginning: 08/21/97 10:45
Ending:
•¼.average value NA-not analyzed NA1-interferences J-estlrnated value N presumptive evidence of presence of matenal
'tt18i value 1s known to be less than value given L-actual value 1s known to be greater than value given U-matenal was analyzed for but not detected the number is the minimum quantitation limit.
~lcates that data unusable compound may or may nol be present resamphng and reanalysis 1s necessary for venfrcat1on
... ,~.by gems: 1.when no value 1s reported, see chlordane constituents 2.constltuents or metabohtes of techrncal chlordane
--- - --·--EPA-lTI:GicmlV SESD, ATHENS, GA --Sample 12774 FY 1997 Project: 97-0355
VOLATILES SCAN
Facility: REASOR CH_E
Program: NSF.
Id/Station: R~S/;ll2
Media: ~ ·
-CASTLE HAYNE, NC-.
Case Number: 256~·5
MD Number: MX16
D Number: MW35
lnorg Contraclor: CHEM
Org Conlractor: DA TAC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
1DU
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UGIL
UGIL
UGIL
UGIL
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL.
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UGIL
UG/L
UGIL
UGIL
UGIL
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UG/L
UGIL
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHANE
METHYL ETHYL KETONE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
METHYL ISOBUTYL KETONE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
BENZENE
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
CIS-1,3-DICHLOROPROPENE
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
METHYL BUTYL KETONE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material.
Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE·
Beginning: 08121/97 10:45
Ending:
- ---Production Date: 11/10/97 10:30
K-actual value is known to be less than value given. L-actual value is known to be greater than value g_iv--. U-material was analyzed for bu\ not detected. the number is lhe minimum quanr 1n limit.
R-Qc indicates tt1: 1 unusable. compound may or may not be present. resampling and reanalysis i ?ssary for verification_
C-conrirmed by g~.. . 1.when no value is reported, see chlordane constituents 2.constituents or metaL .. .:S of technical chlordane
-
-Sample 12774 FY 1997 Project: 97-0355
EXTRACTABLES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF_ Case Nu-rriber: 25645
Id/Station: RCSSEB2 MD Number: MX16
Media: WATER D Number: MW35
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
"10U
10U
10U
10U
10U
10U
10U
---\"\ 10U -6
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE (HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
H
lnorg Contractor: CHEM
Org Contractor: DA TAC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
A-average value. NA-nol analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material.
A--Produced by: Kei_th Bates
Requester: RAY DOYLE
Project.Leader: DOYLE
Beginning: 08/21/97 10:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2,4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
K-actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
r.-r.onfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
--- -- ----- ---- - - - -
EXTRACTABLE$ SAMPLE ANALYSIS EPA -REGION IV SESD, ATHENS, GA Production Date: 11/10/97 08:52
Sample 12774 FY 1997 Project: 97-0355
EXTRACTABLES SCAN
Fac(lilL _REASOR CHEMICA!c
Program: NSF
--CASTLE HAYNE, NC
Case Number: 25645
MD Number: MX 16 ld/Slation: RCSSEB2
Media: WATER
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
-10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MW35
ANALYTE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
BIS(2-CHLOROETHYL) ETHER
HEXACHLOROETHANE
BIS(2-CHLOROISOPROPYL) ETHER
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
HEXACHLOROBUTADIENE
2-METHYLNAPHTHALENE
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
BIS(2-CHLOROETHOXY)METHANE
ISOPHORONE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2-CHLORONAPHTHALENE
2-NITROANILINE
ACENAPHTHYLENE
ACENAPHTHENE
DIMETHYL PHTHALATE
DIBENZOFURAN
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
3-NITROANILINE
4-CHLOROPHENYL PHENYL ETHER
4-NITROANILINE
FLUORENE
DIETHYL PHTHALATE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
HEXACHLOROBENZENE(HCB)
4-BROMOPHENYL PHENYL ETHER
PHENANTHRENE
ANTHRACENE
D1-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYL BUTYL PHTHALATE
lnorg Contractor: CHEM
Org Contractor: DATAC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U 10U.
10U
10U
10U
10U
10U
10U
25U
10U
25U
25U
25U
25U
10U
Produced by: Keilh Bales
_ Requeslor: RAY DOYLE -
Projecl Leader: DOYLE
Beginning: 08/21/97 10:45
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
BIS(2-ETHYLHEXYL) PHTHALATE
BENZO(A)ANTHRACENE
CHRYSENE
3,3'-DICHLOROBENZIDINE
D1-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
2-CHLOROPHENOL
2-METHYLPHENOL
(3-AND/OR 4-)METHYLPHENOL
2-NITROPHENOL
PHENOL
2,4-DIMETHYLPHENOL
2.4-DICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2.4,5-TRICHLOROPHENOL
4-CHLORO-3-METHYLPHENOL
2.4-DINITROPHENOL
2-METHYL-4,6-DINITROPHENOL
PENTACHLOROPHENOL
4-NITROPHENOL
CARBAZOLE
•~erage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material. ~ value is _r ·n to be less than value given. L-actual value is known to be greater than value p' U-rnalerial was analyzed for but not detected. the number is the minimum quar n limit. 1~.ates th; t unusable. compound may or may not be present. resampling and reanalysis . essary for verification.
•· "·t,y gc.,,_; 1.when no value is reported, see chlordane constituents 2.constituenls or metabumes of technical chlordane
-
M-SS..._E ... YS--·-Sample 12774 FY 1997 Project: 97-0355
METALS SCAN
Facility: REASOR CHEMICAL·
Program: NSF
Id/Station: RCSSEB2
Media: WATER
RESULTS UNITS ANALYTE
.2U UG/L SILVER
7U UG/L ARSENIC
1U UG/L BARIUM
1U UG/L BERYLLIUM
1U UG/L CADMIUM
2U UG/L COBALT
1U UG/L CHROMIUM
1U UG/L COPPER
1U UG/L NICKEL
2U UG/L LEAD
SU UG/L ANTIMONY
SU UG/L SELENIUM
6U UG/L THALLIUM
1U UG/L VANADIUM
11J UG/L ZINC
CASTLE HAYNE, NC
Case Number: 25645
MD Number: MX16
D Number: MW35
0.20U UG/L TOTAL MERCURY
30U UG/L ALUMINUM
1U UG/L MANGANESE
200U UG/L CALCIUM
23U UG/L MAGNESIUM
22U UG/L IRON
100000J UG/L SODIUM
4900 UG/L POTASSIUM
lnorg Contractor: CHEM
Org Contractor: DATAC
- -
Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/21/97 10:45
Ending:
~~~rage value NA-not analyzed NAl-interferences J-est1mated value N presumptive evidence of presence of material.
~I value 1s known to be less than value given L-actual value is known lo be greater than value given U-matenal was analyzed for but not detected the number is the minimum quantilation limit.
~icates that data unusable compound may or may not be present resamphng and reanalysis 1s necessary for verification
, ...... b,:_ gems 1 when no value 1s repoited, see chlordane consl1tuents 2 constituents or metabohtes or technical chlordane
Sample 12774 FY 1997
SPECIFIED TESTS-
Facility: REASOR CHEMICAL
Program: NSF
ld/Stalion: RCSSEB2
Media: WATER
RES UL TS UNITS
10U -uGIL
ANALYTE
CYANIDE
------EPA~EGIONIV SESD, ATHENS, GA --Project: 97-0355
CASTLE HAYNE, NC
Case Number: 25645
MD Number: MX16
D Number: MW35
lnorg Contractor: CHEM
Org Contractor: DAT AC
Produced by: Keith Bates
-Requestor: RAY-DOYLE
Project Leader: DOYLE
Beginning: 08121197 10:45
Ending:
- - - - -
Production Date: 10/22/97 14:12
~-average value. NA-nol analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of .material.
~t<1ctual value is _k""v..rn to be less than value given. L-actual value is known to be greater than value 9>·-~. U-material was analyzed for but not detected. the number is the minimum quan•·· ''1n limit.
'""'1:,dicates th a unusable. compound may or may not be present. resampling and reanalysis essary for verification .
..... : .. d by g.._ 1.when no value is reported, see chlordane constituents 2.constituents or meta1.. . .:!S of technical chlordane "
--Sample 12961 FY 1997 Project: 97--0357
VOLATILES SCAN
Facility: REASORCHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY44 Id/Station: RCEB3
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UGIL
UGIL
UGIL
UGIL
UG/L
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MZ02
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: ARI
Org Contractor: AT AS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
-- - - - --· Production Date: 12/11/97 07:49
Produced by: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08_127197 14:40
Ending:
A-average value. NA-not analyzed. NAl-inlerferences. J-E!stimated value. N-presumptive evidence of presence of material.
~-actual value is ic .. ~.,.,n to be less than value given. L-actual value is known to be greater than value gi•· -U-material was analyzed for but not detected. the number is the minimum quant:• ·•"l_n limit.
"'c Indicates th l unusable. compound may or may not be present. resampling and reanalysis : ~ssary for verification .
.. ,..,., """'ctr".l_ed by g .... - . 1.when no value is reported, see chlordane constituents 2.constituenls or metal:-~ .. .::s of technical chlordane
--=PA-GIO_,E9S-E"IHElllll,A --
Sample 12961 FY 1997 Project: 97-0357
EXTRACTABLES SCAN
Facility: -REASOR CHEMICAt --cASTlE HAYNE, NC
Case Number: 25655
MD Number: MY 44
Program: NSF
Id/Station: RCEB3
Media: GROUNDWA
RESULTS
10U
10U
· 10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
D Number: MZ02
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-ANDIOR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
2,4,6-TRICHLOROPHENOL
2.4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
'
I norg Contractor: ARI
Org Contractor: AT AS
RESULTS
10U
10U
25U
25U
10U
10U
10U
25U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
Produced by: John Mcconney
Requestor: RAY DOYLE
Project leader: DOYLE -
Beginning: 08/27/97 14:40
Ending:
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE (HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALA TE
FLUORANTHENE
PYRENE
BENZVLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence or material.
K-actual value is known lo be less than value given. L-actual value is known lo be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported. see chlordane constituents 2.conslituenls or metabolites of technical chlordane
- - --METALS SAMPLE ANALYSIS --------EPA -REGION IV SESD, ATHENS, GA --Sample 12961 FY 1997 Project: 97-0357 Produced by: Keith Bates
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/27/97 14:40
Ending:
~ ~
METALS SCAN
Facility: REASOR CHEMICAL
Program: NSF
Id/Station: RCEB3
Media: GROUNOWA
RESULTS UNITS ANALYTE
3U UG/L SILVER
1U UG/L ARSENIC
1U UG/L BARIUM
1U UG/L BERYLLIUM
2U UG/L CADMIUM
3U UG/L COBALT
5U UG/L CHROMIUM
2U UG/L COPPER
10U UG/L NICKEL
2U UG/L LEAD
50U UG/L ANTIMONY
1U UG/L SELENIUM
1U UG/L THALLIUM
3U UG/L VANADIUM
6U UG/L ZINC
CASTLE HAYNE, NC
Case Number: 25655
MD Number: MY44
D Number: MZ02
0.10UJ UG/L TOTAL MERCURY
20U UG/L ALUMINUM
1U UG/L . MANGANESE
40U UG/L CALCIUM
20U UG/L MAGNESIUM
20U UG/L IRON
160000. UG/L SODIUM
7600 UG/L POTASSIUM
lnorg Contractor: ARI
Org Contractor: AT AS
----Production Date: 11/20/9711:32
lerage value. NA-nol analyzed. NAl-inlerterences. J-estimaled value. N-presumptive evidence of presence of material.
""-'ttial value is~ ---··•n to be less than value given. L-aclual value is known to be greater than value g: U-malerial was analyzed for but not detected. the number is the minimum quan'
-,., "~;;ites th 1 unusable. compound may or may not be present. resampling and reanalysis i essary for verification.
n limit.
••,• · · · ~,,._v_gc...,~. 1.when no value is reported, see chlordane conslituenls 2.constituenls or melab,., .. 1es of technical chlordane
-
Sample 12961 FY 1997 Project: 97-0357
SPECIFIED TESTS
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCEB3 MD Number: MY44
Media: GROUNDWA D Number: MZ02
RESULTS UNITS
5U UG/L
ANALYTE
CYANIDE
lnorg Contractor: ARI
Org Contractor: AT AS
--Produced by: Keith Bates
Reque_stor:_RA Y_ DOYLE _
Project Leader: DOYLE
Beginning: 08/27/97 14:40
Ending:
~-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumplive evidence of presence of material.
~./:.actual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
...._Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. ~e~ by gems: 1.when no value is reported, see chlordane constituents 2.conslituenls or metabolites of technical chlordane
--Sample 12996 FY 1997 Project: 97 -0386
VOLATILES SCAN
Facility: REASOR CHEMICAL
Program: NSF
CASTLE HAYNE, NC
Case Number: 25648
MD Number: MY74 Id/Station: RCEB4
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
·· 10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: LB79
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: SENTIN
Org Contractoi: CEIMIC
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-eslimaled value. N-presumptive evidence of presence of material.
-------Production Date: 12/01197 08:05
Produced by: John .McConney
Requeslor: RAY DOYLE
Project Leader: 'RAY DOYLE
Beginning: 09/02/97 15:00
Ending:
K-octua! value is knnwn to be less than value given. L-actual value is known to be greater than value gr,,-... _ U-material waS analyzed for but not detected. the number is the minimum quan•· ·,n limit.
R-qc indicates th: 1 unusable. compound may or may not be present. resampling and reanalysis' ':!ssary for verification.
C-confirmed by g, 1.when no value is reported. see chlordane constituents 2.constituenls or metai.. .. ..:s of technical chlordane
-Sample 12774 FY 1997
PESTICIDES SCAN
Project: 97-0355
Facility: REASOR.CHEMICAL
Program: NSF
CASTLE HAYNE, NC_
Case Number: 25645
MD Number: MX16 Id/Station: RCSSEB2
Media: WATER
RESULTS
0.050U
0.050U
0.050U o.osou
0.0S0U
0.050U
0.050U
0.050U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
0.10U
1.0U
1.0U
2.0U
1.0U
1.0U
1.0U
1.0U
5.0U
0.10U
0.050U
0.050U
0.50U
0.10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: MW35
ANALYTE
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
. GAMMA-BHC (LIN DANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDT (P,P'-DDT)
4,4'-DDE (P,P'-DDE)
4,4'-DDD (P,P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
ENDRIN ALDEHYDE
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
METHOXYCHLOR
ENDRIN KETONE
lnorg Contractor: CHEM
· Org Contractor: DAT AC
--- - - - -
Production Date: 11/10/97 10:18
Produced by: Keith Bates
Requester: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/21/97 10:45
Ending:
I
!~
"-A-average value. NA-not analyzed. NA\-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is kn< ·· · · •o be less than value given. L-actual value is known to be greater than value give· · -material was analyzed for but not detected. the number is the minimum quantit; '!mit.
R-qc indicates that:__ .nusable. compound may or may not be present. resampling and reanalysis is r, ;ary for verification.
r:-r.onfirmed by gcms:·.,-,-.when no value is reported, see chlordane constituents 2.constituents or metabolitt:. of technical chlordane
__ , _______ . ----~• , __ -.,,_ ":•\IH-GA---Sample
DIOXIN SCAN
FY 1998 Project: 98-0109
Facility: Reasor Ch~rn~cal
--Program: SSF
Castle Hayne, NC -
Id/Station: RCMWEB1A
Media: WATER D Number: EB1A
RESULTS
0.020U
0.03UJ
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050UJ
0.11U
0.020U
0_020UJ
0.050U
0.050U
0.050UJ
0.050U
0.050U
0.050U
0.050U
0.050UJ
0.050U
0.050U
0.050UJ
0.10U
0.0
UNITS
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
NG/L
ANALYTE
2,3,7,8-TETRACHLORODIBENZODIOXIN
TETRACHLORODIBENZODIOXIN (TOTAL) 1,2,3,7,8-PENTACHLORODIBENZODIOXIN
PENTACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6, 7,8-HEXACHLORODIBENZODIOXIN
1,2,3, 7 ,8,9-HEXACHLORODIBENZODIOXIN
HEXACHLORODIBENZODIOXIN (TOTAL) 1,2,3,4,6, 7,8-HEPTACHLORODIBENZODIOXIN
HEPTACHLORODIBENZODIOXIN (TOTAL) OCTACHLOROOIBENZOOIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
TETRACHLOROOIBENZOFURAN (TOTAL) 1,2,3,7 ,8-PENTACHLORODIBENZOFURAN
2,3.4, 7 ,8-PENTACHLORODIBENZOFURAN
PENTACHLORODIBENZOFURAN (TOTAL) 1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6, 7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
HEXACHLOROOIBENZOFURAN (TOTAL) 1,2,3,4 ,6,7 ,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
HEPTACHLORODIBENZOFURAN (TOTAL) OCTACHLORODIBENZOFURAN
TEQ (TOXIC. EQUIV_ VALUE, FROM I-TEF/89)
-----------------------
SAS Number:DIOX
Org Contractor. SWOK
Produced by: John McConney
Requestor: Jennifer Wendel
Project·Leadef:-
Beginning: 12104/97 11:00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estirnated value. N-presumptive evidence of presence of material. K-aclual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantil3tion limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. C-confinned by gems: 1.when no value is reported, see chlordane constituenls 2.constituenls or metabolites of technical chlordane
--=P~GiclllllSt::
Sample 1249 FY 1998 Project: 98-0105
PESTICIDES SCAN
Facility: Reasor Chemical·
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NF02 Id/Station: RCMWEBIA
Media: WATER D Number: NF10
RESULTS UNITS ANALYTE
0.050U UG/L ALPHA-BHC
0.050U UG/L BETA-BHC o.osou UG/L DELTA-BHC
0.050U UG/L GAMMA-BHC (LINDANE)
0.050U UG/L HEPTACHLOR
0.050U UGIL ALDRIN
O.OSOU UGIL HEPTACHLOR EPOXIDE o.osou UGIL ENDOSULFAN I (ALPHA)
0.10U UGIL DIELDRIN
0.10U UG/L 4,4'-DDE (P,P'-DDE)
0.10U UGIL ENDRIN
0.10U UG/L ENDOSULF AN 11 (BET A)
0.10U UG/L 4,4'-DDD (P,P'-DDD)
0.10U UG/L ENDOSULFAN SULFATE
0.10U UG/L 4,4'-DDT (P,P'-DDT) a.sou UG/L METHOXYCHLOR
0.10U UG/L ENDRIN KETONE
0.10U UG/L ENDRIN ALDEHYDE
O.OSOU UG/L ALPHA-CHLORDANE /2
O.OSOU UG/L GAMMA-CHLORDANE /2
5.0U UG/L TOXAPHENE
1.0U UG/L PCB-1016 (AROCLOR 1016)
2.0U UGIL PCB-1221 (AROCLOR 1221)
1.0U UG/L PCB-1232 (AROCLOR 1232)
1.0U UG/L PC_B-1242 (AROCLOR 1242)
1.0U UG/L PCB-1248 (AROCLOR 1248)
1.0U UGIL PCB-1254 (AROCLOR 1254)
1.0U UG/L PCB-1260 (AROCLOR 1260)
lnorg Contractor: CHEM
Org Contractor: DA TAC
---ctiftte: ~/98a1 liiiii
Produced by: Denise Goddard_
-Requesto·r:·Jennifer Wendel
Project Leader:
Beginning: 12/04197 11 :00
Ending:
A-average value. NA-not analyzed. NAl-interferences. J--estimaled value. N-presumptfve evidence of presence of material.
IIK,,.actuat value is known to be less lhan value given. L-actual value is known to be greater than value givr--c . _U-material was analyzed for but not detected. the number is the minimum quanti• · -~"1 limit.
,.Indicates tha' unusable. compound may or may not be present. resampling and reanalysis i( ssary for verification.
~ed by gc , .when no value is reported, see chlordane constituents 2.consUtuents or metab~-_,., of technical chlordane • ·---...: ·.
--Sample 1249 FY 1998 Project: 98--0105
METALS SCAN
Facility: Reasor-Chemicar -
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number: NF02 Id/Station: RCMWEBIA
Media: WATER D Number. NF10
RESULTS
60U
4U
6U
2
1U
1U
1500
1U
2U
30U
60U
3U
250
1U
0.20U
1U
60U
3U
3U
830J
6U
1U
20U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
MANGANESE
TOTAL MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
VANADIUM
ZINC
CYANIDE
lnorg Contractor: CHEM
Org Contractor: DATAC
-- -II!!!! -a.iii ilia.
Produced by: Keith Bates
R£!"quesfor:-jennifer Wendel
Project leader:
Beginning: 12/04/97 11:00
Ending:
Production Date: 03r-·qa 14:16
411t~erage value NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material.
~I value Is known lo be less than value given. L-actual value Is known to be grealer lhan value given. U-material was anatyzed for but not detected the number Is the minimum quantitation limit.
:.i1cates that data unusable. compound may or may not be present. resampting and reanatysls Is necessary for verilication.
'~ -~Y gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-..,A --IO~ESP,illlltHE~A --Sample 1249 FY 1998 Project: 98-0105
EXTRACTABLES SCAN
Facility: Reasor Chemical
Program: S.SF
Casile Hayne, NC
Case Number: 25902
MD Number: NF02 Id/Station: RCMWEBIA ·
Media: WATER D Number: NF10
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U fou
10U
10U
10U
10U
10U
10U
10U
25U
10U
25U
10U
10U
10U
25U
10U
25U
25U
10U
....-,.. 10U
'--\ 10U ~
UNITS
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UGIL
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UG/L
UGIL
UG/L
UGIL
UGIL
UGIL
ANALYTE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE
2-METHYLPHENOL
BIS(2-CHLOROISOPROPYL) ETHER
(3-ANDIOR 4-)METHYLPHENOL
N-NITROSODI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITROPHENOL
2,4-DIMETHYLPHENOL
BIS(2-CHLOROETHOXY)METHANE
2,4-DICHLOROPHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLOR0-3-METHYLPHENOL
2-METHYLNAPHTHALENE
HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2-CHLORONAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
3-NITROANILINE
ACENAPHTHENE
2,4-DINITROPHENOL
4-NITROPHENOL
DIBENZOFURAN
2,4-DINITROTOLUENE
DIETHYL PHTHALATE
Produced by: De_nis~ Goddard
Requeslor: Jennifer Wendel
Project Leader:
lnorg Contractor: CHEM
Org Contractor: DATAC
Beginning: 12/04197 11 :00
Ending:
RESULTS UNITS
10U UGIL
10U UGIL
25U UGIL
25U UGIL
10U UGIL
10U UGIL
10U UGIL
25U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UGIL
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
1 OU . UG/L
10U UG/L
10U UG/L
ANALYTE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
2-METHYL-4,6-DINITROPHENOL
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE(HCB)
PENTACHLOROPHENOL
PHENANTHRENE
ANTHRACENE
CARBAZOLE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BENZYLBUTYLPHTHALATE
3,3'-DICHLOROBENZIDINE
BENZO(A)ANTHRACENE
CHRYSENE
BIS(2-ETHYLHEXYL) PHTHALATE
DI-N-OCTYLPHTHALA TE
BENZO(B AND/OR K)FLUORANTHENE
BENZO-A-PYRENE
INDENO (1,2,3-CD) PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(GHl)PERYLENE
!l!a.verage value. NA-not analyzed. NAl-inlerferences. J-estirnated value. N-presumptive evidence of presence of material. ""Q,ltal value is known to be less than value given. L-actual value Is known lo be greater than value give~ ')-material was analyzed for but not detected. the number Is the minimum quanli' ...... ,
~...at_es that,-musable. compound may or may not be present. resampling and reanalysis is sary for verification . .... :.,_V gen .when no value is reported, see chlordane constituents 2.constituenls or melabo, ... -~ of technical chlordane · ,, ·limit.
--Sample \ _ .~ FY 1998 Project: 98-0105
VOLATILES SCAN
F·acility: Reasor Chemical
Program: SSF
Castle Hayne, NC
Case Number: 25902
MD Number. NF02 Id/Station: RCMWEBIA ·
Media: WATER D Number: NF10
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
lnorg Contractor: CHEM
Org Contractor: DAT AC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
.10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
----I!!!!!!! !!!!!!I == Production Date: 01'"-'98 16:26
Produced by: Denise Goddard·
Requester: Jennifer Wendel
Project Leader: ·
Beginning: 12/04/97 11 :00
Ending:
4'kav~rage value. NA-no! analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence or presence of material. -~ual value ls known to be less (han value given. L-actual value is known to be grealer than value given. U-material was analyzed for but not detected. 1'1dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary ror verification.
the number is lhe minimum quantitation limit. . ~d. by gems: 1.when no value is reported, see chlordane constituents 2.consliluents or metabolites ot technlcal chlordane · ·
,-.TILIIIIIIAM ... N~S --
---
Sample 12894 FY 1997 Project: 97-0357
VOLATILES SCAN . ----
Facility: REASOR CHEMICAL CASTLE HAYNE, l·)C
Program: NSF Case Number: 25655
Id/Station: RCSSTB 10
Media: WATER D Number: MY26
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
.UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
. 10U
10U
10U
10U
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPl,OPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--~en~at~219!!!!!!20 a=
Produced by: Denise Goddard
Requeslor: ·RAY-DOYLE
Project Leader: DOYLE
Beginning: 08/24/97 14:00
Ending:
A-average value. NA-nol analyzed. NAl-inlerferences. J--eslimated value. N-presumptive evidence of presence of material.
ctual value is J("~ . .,..n to be less than value given. L-actual value is known to be greater than value p: · ~ U-materiat was analyzed for but not detected. the number is the minimum quanti•-•;on limit.
'll)dicates th! J unusable. compound may or may not be present resampling and reanalysis; ~ssary for verification.
...... rmed by Qt... 1.when no value is reported, see chlordane constituents 2.constiluents or melaL .,s of technical chlordane
~ . ........
-Sample 12898 FY 1997 Project: 97-0357
-VOLATILES SCAN -
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCSSTB11
Media: WATER D Number: MY50
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U 1ou·
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (fOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (fRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (fETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
-

-
Produced by: Denise Goddard
Requestor:-RAY DOYLE.
Project Leader: DOYLE
Beginning: 08/24/97 14 :00
Ending:
A-average value. NA~not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
~ K-actual value is known to be less than value given. L-actual value is known to be weater than valu~ ~iven. U-malerial w~s a~alyzed for but not detected. the number is the minimum quantilation limit.
~R-gc Indicates that data unusable. compound may or may not be present. resampling and reanalysis 1s necessary for verification .
. ·· ......... """~tlnJlm1ed by gems: 1.when no value is reported, see ctilordane constituents 2.conslituenls or metabolites of technical chlordane
~TlljllifAMMAN ... IS ---E~EcallllV ~. A
Sample 12907 FY 1997 Project: 97-0357
VOLATILES SCAN
Fa"cilily: REASOR-CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 12
Media: SURFACEWA D Number: MY58 Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
Requestor; RAY DOYLE
Project Leader: DOYLE
Beginning: 08/25197 09: 15
Ending:
K-actual value is 1<---..,n to be less than value given. L-actual value is known lo be greater than value gi• U-material was analyzed for but not detecled. the number is the minimum quan1'' ·=1n limit.
R-qc indicates th: :1 unusable. compound may or may not be present. resampling and reanalysis· assary for verification.
f:-confirmed by 91... .. __ 1.when no value is reported, see chlordane constituents 2.constituents or metaL~ .. -~s of technical chlordane
-Sample 12931 FY 1997 Projecl: 97-0357
-VOlA TILES SCAN
Facilily: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 13
Media: GROUNDWA D Number: MY93 Org Contractor: AA TS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
. 10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-nol analyzed. NAl-interferences. J-estimaled value. N-presumptive evidence of presence of material.
--Produced by: John McConney
Req-uestor: RAY D-OYLE .
Project Leader: DOYLE
Beginoing: 08/25/97 09:15
Ending:
K-actua1 value is known to be less lhan value given. L-actual value is known to be grealer than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may no! be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported. see chlordane conslituents 2.conslituents or metabolites of technical chlordane
-Sample 12916 FY 1997 Project: 97-0357
-VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
ld/Slation: RCTBL 14
Media: GROUNDWA D Number: MY97 Org Contractor: AA TS
RESULTS
7J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UGIL
UGIL
UG/L
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UG/L
UGIL
UGIL
UGIL
UG/L
UG/L
UGIL
UGIL
UG/L
UGIL
UG/L
UG/L
UGIL
UGIL
UGIL
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: John Mcconney
Requesior:-RA y DOYLE
Project Leader: DOYLE
Beginning: 08126197 16:15
Ending:
. A•average value. NA•nol analyzed. NAl•interferences. J-estimated value. N-presumptive evidence of presence of material.
~K-.actual value is v---wn to be less than value given. L-actual value is known lo be greater than value 9i1'"'l. LI-material was analyzed for but not detected.
~;qc indicates ti' 1.8 unusable. compound may or may not be present. resampling and reanalysis :essary for verification.
. -Confirmed by ti ,: 1.when no value is reported, see chlordane constituents 2.constituents or mete-cs of technical chlordane
the number is the minimum quantil::ition limit.
·••, "·
-Sample 12926 FY 1997 Project: 97-0357
VOLATILES SCAN -
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 15
Media: GROUNDWA D Number: MY96
RESULTS UNITS ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AA TS
10U
10U
10U
10U
20U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UGIL
UGIL
UGIL
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UGIL
UG/L
UG/L
UG/L
UGIL
UGIL
UGIL
UGIL
UGIL
UGIL
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1,1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYLISOBUTYLKETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--~ro_du_ce_d 9y: John Mcconney
Requestor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08126197 16:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material.
~ K-actual value is known lo be less. than value given. L-actual value is known lo be greater than value given. U-malerial was analyzed for but not detected. the number is lhe minimum quanlitation limit.
'R-qc indicates that data unusable compound may or may not be present. resarnpling and reanalysis is necessary for verification.
•p ... ,. t'.'!~Lnfirmed by gems: 1.when no value is reported, see chlordane constituents 2.constiluents or metabolites of technical chlordane
Mr1L~MrMNA~ --Sample 12992 FY 1997 P,aject: 97-0357
VOLATILES SCAN-
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 16
Media: GROUNDWA D Number: MZ00
RES UL TS UNITS
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: AT AS
10U UG/L
10U UG/L
1, 1-DtCHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U . UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
10U UG/L
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOl<OETHANE
METHYL ETHYL KETONE
1,1,1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: John Mcconney
Requesfor: RAY DOYLE . .
Project Leader: DOYLE
Beginning: 08/27/98 13:50
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material.
K-actual value is y-··vn to be less than value given. L-actual value is known to be greater than value g; · U-malerial was analyzed for but not detected. the number is tile minimum quan•·· ··1n limit.
R-qc indicates 1~· a unusable. compound may or may not be present. resampling and reanalysis essary ror verification. \
C-confirmed by 91. ~-1.when no value is reported, see chlordane constituents 2.constituents or metaL_ .. t!S of technical chlordane
-Sample 12989 FY 1997 Project: 97-0357
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 17
Media: GROUNDWA
RESULTS
4J
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
.10U
10U
10U
10U
10U
10U
10U
UNITS
UGIL
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L -
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: LB55
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contractor: ATAS
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE [fETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: John McS:o~ney
Requestor:-RAY DOYLE
Project Leader: DOYLE
Beginning: 08128/98 12:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material.
K-actual value is known to be less than value given. L-aclual value is known to be greater than value given. U-malerial was analyzed for but not detected. the number is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-conrirmed by gems: l .when no value is reported, see chlord:me consljtuents 2.conslituenls or metabolites of lcchnical chlordane
.. TILillllt<IMflliltNAiillli5 ---E~EG_.v S-ATf911, G/11111 --~uc-ate-1/9_,9 -
Sample 12989 FY 1997 Project: 97-0357
MISCELLANEOUS COMPOUNDS
Produced by: John Mcconney
Requeslor: RAY DOYLE
Facility: REASOR CHE.MICAL
Program: NSF
ld/Slalion: RCTBL 17
Media: GROUNDWA
RES UL TS UNITS ANALYTE
CASTLE HAYNE, NC
Case Number: 25655
D Number: LB55
S0J UG/L 2 UNIDENTIFIED COMPUNDS
Org Contractor: AT AS
A-average value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material.
. Project Leader: DOYLE
Beginning: 08/28/98 12:15
Ending:
K-actual value is,~ --·vn lo be less than value given. L-aclual value is known to be greater than value Qi•· -U-material was analyzed for but not detected. the number is the minimum quanti•-•;'?n limit
R-qc indicates ti'. a unusable. compound may or may not be present. resamp!ing and reanalysis· :!ssary for verification.
C-confirmed by g.__ -· 1.when no value is reported, see chlordane conslituents 2.constituents or meta1., .-.:s of technical chlordane
-Sample 12990 FY 1997 Project: 97-0357
VOLATILES SCA!J
Facility: REASOR CHEMICAL CASTLE HAYNE, NC
Program: NSF Case Number: 25655
Id/Station: RCTBL 18
Media: GROUNDWA D Number: LB69 Org Contractor: ATAS
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U.
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
--Produced by: John McConney
Requeslor: RAY DOYLE
Project Leader: DOYLE
Beginning: 08/28/98 12:15
Ending:
A-average value. NA-not analyzed. NAl-interferences. J-estirna\ed value. N-presurnptive evidence of presence of material.
K-actual value is known to be less than value given. L-aclual value is known to be greater than value given. U-malerial was analyzed for but not detected. the number-is lhe minimum quantilation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.when no value is reported, see chlordane constituents 2.conslituenls or melaboliles of technical chlordane
.. TILIIIIIIAMrWllNA~S --
~ __s::::._.
Sample .13000 FY 1997 Project: 97-0386 ·
VOLATILES SCAN
Facility: REASOR CHEMICAL CASTLE HAYNE. NC
Program: NSF Case Number: 25648
Id/Station: RCTBL 19
Media: GROUNDWA D Number: LBBO Org Contractor: CEIMIC
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U .
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L.
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE (1, 1-DICI-ILOROETHYLENE)
1.1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICHLOROETHANE
CARBON TETl,ACHLORtDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1.1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2.2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
---

-

-

-
l!!!!!!I Production Date: 12/01/97 08:05
1='ro~uced by: John Mcconney -
Requestor: RAY DOYLE
Project Leader: RAY DOYLE
Beginning: 09/03/97 15:00
Ending:
A-average value. NA-not analyzed. NAt-interferences. J-estimated value. N-presurnplive evidence of presence of material. K-c1clual value is kr-"'"n to be less than value given. L-aclual value is known to be greater than valuer/ U-material was analyzed for but not detected. the number is the minimum quaJl· 1n limit. R-qc indicates lh( 1 unusable. compound may or may not be present. resampling and reanalysis essary for verHication. C-confirmed by Q;_ 1.when no value is reported, see chlordane constituents 2.conslituents or metaL ___ .t!S of technical chlordane
---TILl!!llll!l~M ...... NA"ls -- -
Sample 1263 FY 1998 Project: 98-0105
Casile Hayne, NC
VOLATILES SCAN.
Facility: Reasor Chemical
Program: SSF Case Number: 25902
Id/Sia lion: RCTBL2A
Media: SURFACEWA D Number: NF02
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Contraclor: DATAC
RESULTS
10U
10U
10U
10U
10U
1DU
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE)
1, 1-DICHLOROETHANE
1,2-DICHLOROETHENE (TOTAL)
CHLOROFORM
1,2-DICHLOROETHANE
METHYL ETHYL KETONE
1, 1,1-TRICHLOROETI-IANE
CARBON TETRACHLORIDE
BROMODICHLOROMETI-IANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETHYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
BENZENE
TRANS-1,3-DICHLOROPROPENE
BROMOFORM
METHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETI-IENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presurnplive evidence of presence of material.
--- - -
Production Date: 0,
Produced by: Deni~e Goddard_
· · Re(lUeStor: J;nnifer Wendel
Project Leader:
Beginning: 12/03/97 12:50
Ending:
- -
-,gs 1s:2s
K-actual value is known to be less than value given. L-actual value Is known lo be greater than value given. U-material was analyzed for but not delected. lhe number Is the minimum quantitation limit.
R-qc indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification.
C-confirmed by gems: 1.wtien no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane
-Sample 1256 FY 1998 Project: 98-0105
VOLATILES SCAN
Facility: Reasor Chemicai
Program: SSF
Castle Hayne, NC
Case Number: 25902
Id/Sia lion: RCT □3A
Media: GROUNDWA
RESULTS
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
10U
UNITS
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
D Number: NF05
ANALYTE
CHLOROMETHANE
BROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
Org Conlraclor: DATAC
1, 1-DICHLOROETI-IENE (1, 1-DICHLOROETHYLENE)
1, 1-DICI-ILOROETHANE
1,2-DICl·ILOROETHENE (TOTAL)
CHLOROFORM
1,2-DICI-ILOROETHANE
METHYL ETHYL KETONE
1, 1, 1-TRICI-ILOROETI-IANE
CARBON TETRACHLORIDE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
CIS-1,3-DICHLOROPROPENE
TRICHLOROETHENE (TRICHLOROETI-IYLENE)
DIBROMOCHLOROMETHANE
1, 1,2-TRICI-ILOROETHANE
BENZENE
TRANS-1,3-DICI-ILOROPROPENE
□ROMOFORM
MicTHYL ISOBUTYL KETONE
METHYL BUTYL KETONE
TETRACHLOROETHENE (TETRACHLOROETHYLENE)
1, 1,2,2-TETRACHLOROETHANE
TOLUENE
CHLOROBENZENE
ETHYL BENZENE
STYRENE
TOTAL XYLENES
A-average value. NA-not analyzed. NAl-inlerferences. J-eslimated value. N-presumptive evidence of presence of material.
--Produced by: Denise Goddard
-Hequestor: Jennifer Wender
Project Leader:
□eginning: 12/04/97 09:20
Ending:
K-actua/ value is 1< .. -• .,0 lo be less than value given. L-actua/ value is known to be greater than value p· LI-material was analyzed for but not detected. the number Is the minimum qua R-qc Indicates th( 1 unusable. compound may or may not be present. resampling and reanalysis essary for verification. C.confirmed by gt... 1.when no value is reported, see chlordane constituents 2 .constituents or metab..,,,.es of technical chlordane
?n limit.
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COMPUCHEM
a division of Liberty Analytical Corp.
03/JUN/99
Roy F. Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
[r.GMR
UN o 4 REC'D·
----------------
Subject: Report of Data -Account Number# 501223 Order# 34336
'· :, . , ,Enclosed are the results of analytical work performed in accordance
;·:1t)j"~with the referenced account number. :i'"''. ·"' . ! ::;\: )li~ii~~;
·· · This report covers 17 sample(s) appearing on the attached listing.
Thenk you for selecting CompuChem Environmental for your sa~ple
analysis. If you should have questions or require additional
analytical services please contact your representative at
1-800-833-5097.
Sincerely,
CompuChem Environmental
a division of Liberty Analytical
Attachment
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■. Fax: [phone]
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COMPUCHEM
a division of Liberty Analytical Corp.
I
OJ/JUN/99
Roy F. · Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
ACCOUNT#: 501223
;· · :."•)·CC#
:(}{;ft
SAMPLE-ID
938559 RC-TMW-4
938563 RC-RBL-1
938564 RC-TMW-2
93'8565 RC-TMW-1
938566 RC-MW-1
938567 RC-TMW-3
938568 RC-PW-3
938569 RC-PW-2
938638 RC-TMW-5
938639 RC-TMW-7
I 938646 .RC-TMW-7A
938647 RC-TMW-6
938648 RC-TMW-10
938649 TAR-POND3
938650 RC-TMW-8
938651 RC-TMW-9
I 938652 RC-TBL-01
TOTAL NUMBER OF SAMPLES
RECEIPT DATE
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
= 17
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: 919•379-4100 ■ Fax:[phone]
. . .),\(:,:·.
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.. ·~:n.: --:::c'tt~r~,
,, .,.. .... -.. -, • ,, t:Jz',;10. 0. -.~~ .. ,>" ::,"i\•✓,;j
The sample data summary package shall contain data for all samples
in one Sample Delivery Group (SDG) of the Case, as follows: . ·
A. SDG Narrative
B. Tabulated target compound results (Form I)c:\-... "--<, ··
Tentatively identified compounds (Form I, TIC) (VOA & SV only)
In order by fraction (VOA, SV, PEST) and by sample.·. ·
within each fraction.
C. System monitoring compound results (Form II -VOA only)
Surrogate spike analysis results (Form II -SV & PEST only)
By fraction (VOA, SV, PEST), matrix (Water or Soil),
and by concentration (Low or Medium) .
D. Matrix Spike/ Matrix Spike Duplicate results (Form III)
By fraction (VOA, SV, PEST)
E. Blank data {Form IV)
Tabulated blank results (Form I)
Tentatively identified compounds (Form I, TIC)
By fraction (VOA, SV, PEST)
F. Internal standard area response and retention time data (Form VIII)
By fraction (VOA & SV only)
LAB CODE : COMPU CONTRACT# : OLM03-REVS
CASE # : .Y./ 33l SDG#: Q.'.)GO/
.... ..
~ ~ • ·--~-S..C.
I A. SDG Narrative
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-;,~lQ~~:i!t~i~.'' -••· ···-• .:··
';_ #. ~,.._ • I •
~~:~!7$~ ,~\ COMPUCHEM
A division of Liberty Analytical Corporation
50 I Madison Ave.
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Cary, NC 27513
SDG NARRATIVE
CASE #34336
SDG #00001
CONTRACT #OLM03-REVS
SAMPLES: RC-TBL-01, RC-TMW-7, RC-TMW-7A, RC-TMW-8
The four (4) water samples listed above were received intact, properly refrigerated, with proper
. documentation, in a sealed shipping container, on May 15, 1999. The samples were scheduled for
tlie requested analyses of the volatile fractions. These samples were analyzed following the
current EPA Contract for the Laboratory Program, Document number OLM03.2 . ..
All pertinent Quality Assurance notices are included in the narrative section and all pertinent
Laboratory notices for Case #34336, SDG #00001 are included in the sample data sections.
SEMIVOLATILE
The semivolatile fractions were extracted and analyzed within the required holding time. No
Target Compound List (TCL) analytes were detected with concentrations above the Contract
Required Quantitation Limit (CRQL) in the samples.
One Tentatively Identified Compound (TIC) was detected in each of the samples. These TI Cs
were assessed as carbon dioxide (CO2) and are not included in the total number of reportable
T!Cs.
QC SUMMARY
The surrogates met recovery criteria for the semivolatile fractions. The internal standards met
area response and retention time criteria. The duplicate matrix spikes met accuracy and precision
criteria. The associated blanks, Initial Calibrations and Continuing Calibrations met Quality
Control criteria.
In the analyses of the Initial and Continuing Calibration standards, manual quantitations were
performed. The reasons have been coded with explanations provided in the notice included in the narrative section of the SDG.
I certify that this data package is in compliance with the terms and conditions of the contract,
both technically and for completeness, for other than_ the conditions detailed above. Release of
the data contained in this hardcopy data package and in the computer-readable data submitted on
diskette has been authorized by the laboratory manager or his designee, as verified by the
-...... ---·-··············· . .. . . . . :;ffigi~~iit;;;; .. ;;i~}f;:,;i:~·~,·:
"'·-1 ••• ,. COMPUCHEM ';, :· .·· I A division of Liberty Analytical Corporation
· .. • ,i 34.J36:oooo 1 .,
•.::_:':-!'·,·
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following signature:
Patricia B. ~ins 1
Final Technical Review
28 May 1999
Note: This report is paginated for reference and accountability in numerical sequence.
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' '
GC and GC/MS Column and Trap Specifications Table
.· COLUMNS
Brand Name 0 -::;;. Coating ID Film Thickness Length
Material (mm) (um) (m)
GC Laboratory
Restek RTX-1701 0.53 0.5 30
J&W DB-608 0.53 0.83 30
Restek CLPesticides 0.53 0.5 30
Restek CLPesticides II 0.53 0.42 30
GC Volatiles Laboratory
Rest~k RTX-1 0.53 0.5 105
Restek RTX-502.2 0.53 0.5 105
GC/MS Volatiles Laboratory
J&W DB-624 0.53 3.0 30/75
Supelco Equityn•-624 0.53 3.0 75
GC/MS Semivolatiles Laboratory
J&W DB-5.625 0,32 1.0 30
J&W D85-MS 0.25 0.25 30
Hewlett Packard HP5-MS 0.25 0.25 30
TRAP
; GC/MS Volatiles Laboratory
* 1 cm of methyl silicone packing (OV-1 coating)
* 8 cm of 2,6-diphenylene oxide polymer (Tenax)
* 8 cm of silica gel
* 7 cm of coconut charcoal
* 0.5 cm of silanized glass wool at each end
Rev. 6 5/10/99
.&%.;¼•i❖······•:-• .: "N::•:=..::::<~,. ~,:.:.;::.-..::.::;;:,;~:::,:_~ :,:.;_. __ ._·_ ..•..• h •• _"}!:,. . r~~1':ir,1e ,;.· ,· :.
'.;,,,.i,;,; CompuChem
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a di\·ision of Libert:, . ..\n:.il:,tical Corporation
Notification Regarding iVIanual Editing/Integration Flags
In some insta_nc_;~.--riianu-al adjusrments to the sofrware output are necessary co provide accurate Cara. These
adjustments afe p"erformed by che daca reviewer. GC/MS operator. or GC chemist. An Extracted Ion Currenr Profile
(EICP) Or a GC chromarographic peak has been provided for the manual integracion of each compound to
demonstrate the accuracy of that process. Adjustments are nagged on the quantitation repon in the far right column
beyond the FINAL concentration for GCMS analysis. and in the "Flags" column for GC analysis. The manual
editing/integration flags are:
M -Denotes tha! a manual integration has been performed for this compound. The manual integration was
performed in order to provide the most accurate area count as possible for che peak.
H -Denotes that the data reviewer. GC/i\.1S ope'rator, or GC Chemist has chosen an alternate peak within the
retention time window rr"om that· chosen by the sofrv.·are for that compound. No manual integration is
performed in choosing an alternate peak. The software still paforms the integration.
,\-1 H · ·· -Denotes that an a!tema1e peak has been chosen wi1hin the relention time window from that chosen by chc-
software for that compound and also a manual integration of the chosen peak has been performed. The.>
manual integration was performed in order ro provide the most accurate area count possible for the peak . ..
L -Denotes chat rhe data reviewer or GC-'.\.1S operacor has selected an alternate library search. This is
typically done when Jn additional 1entativel;· identified compound (TIC) has been added to the number of
peaks searched. No manual integration is performed in choosing an altema1e peak. The sofrv.·;:ire still
perfom1s the integration.
-Denotes that an alternate librar; search has been ~ .. ·lec1ed and J manu;:il integration has also been
performed. This is t,picallv done when Jn adJi" 1JI TIC has been added and the TIC peak also required a
manual integration.
With the introduction or' the current EP.-\ CLP SOW (Document Number OLMOJ.O. plus revisions) additions'.
explanations for manual editing.'integration are required. In the accompanying raw daca packages. addition.ii codes
have been applied to the ".\.-1" tlag and carry !he following me:>n 1ngs:
, ,',,1 I -The compound was noc found by the automatic integration routine.
M:! -The compound was incorrectly integrated by the automatic integration routine.
• The co-eluting compounds were incorrect I~ integrated by the automatic integration routine.
1 These codes will appear in the GC'~1S and GC datJ pacKages.
,Revision 4 ( I 0/8197)
Robert E. Meierer
Vice President
. -.~:)$:.: .-.
....... •.::.tu.'.l.:_..it'it;,:-;i.:._..~·~ ::.:' ... · ., lll:."r~l'.,~~-~''' ,,,;,, .. ;_~~1~ ..... , '
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CompuChem
.: ,!:\:~:,,n 1•:"I ::,~•r:: \::.ii~·:;..:.!: C,•r·;,,1r.1r:,•n
DATA REPORTING QUALIFIERS
()11 1/Jc h1rm /. tr11da ell,: Cldt111111 /:1bt:IL'd ··<y· (dr qualifit:r. L":1c!i rt..·.,u/1 I:-11:igg,:d \\itli d1t.· -'~1L'L·,ti,.: d:n:1 r1.:pt1rri11g qualiti-.·r., li:-ted bdO\\. a., ;1pprnpriatt..'. l:p rl, li\"t..' qualiti1.-r.-: 111.i~ he rqJ11nt..·d \111 h 1rn1 I f~1r c;1d1 1..·u,11plH1nJ. The.· _lJP:ilitic-r.s usecJ art.':
u
J :
·•
P·
C:
This tlaL; indicates the compound was analyzed for bw lllH dctCL'ted. The' Contract Required Quantita~ion Limit (CRQL) (or Reponing Limit\ will be adjusted to retlecr any dilution and for soils. the percent moisture.
This nag indicates an estimated value. The flag is used as derailed below:
I. \Vhen estimating a concentration for renrarive/y idernitied compounds (T/(:,J \\hac :1 response factor of! .0 is assumed for the:' TIC :rna/yrc:.
\Vhen rhe mass spc:c.:tral and reremion rim-: dnr.1 ill(JiL':Hc:' the prc:sc:1h.:c:' nf a c.:ornptHHHI 1li:1r mt:c-ts the vul.1tik anJ se111i\·l)latih: GC/.VIS it.k111itic:11ion i..:riraia and tht: result is lr:ss rh;w rhe CR()L (l)r Reporting L1111i1J hut );r-.:-arL'r 1lian 1.L'ro.
, \Vht:n thL' fL'IL'11ti1,1n ri111L· d~1t:i i11di...:~u1..·s 1ll1..· pr1..·se1K1..' lit' a 1.:nr11pl1u11d th:ll 1111.:t:ts r/11..· p1..·s1icit.k .-\rl1dl1r or lllh1..·r ( JC 11r 11/l!.l" idi.:r1tifii..::iti1,H1 i..:riraia and rh1..· rc::-ult is IL':i.S 1/Jan tlil.' CRC)L (,1r Ri.:purting !.i111i11 hu1 grt.:alL'r rli~111 /.L'r1.1. f-°Llr L'.\arnpk. if th1..· CRQL (l'f R.:p1,1rting l.i111itl is IO ug."L hut a i..:orH.:c:11rr:ilillll llf _\ ug. l. is i..:alcul.:itc:d. it is rt:p1H1 .. -U as 3.1.
This tlag i11Jicatt::--prc:--umpti\·1..· L'\ idL'n(c.' t1f:1 i..:om1h1L111J. This tlag is lHily Lbt.!d tlJr T!Cs. ,,!ia1.; 1!1t..: iJL'nti!i(atilirl i., ha.,L'ti°1111 a 111:i:-,:.-, ,rL'i..:tr:il lihra,_, SL':in.:h. Fl,r g1..'llL'ric 1.:haracterizatinn l1fa TIC ... u..:li a:--'t..:lil,iri11atLd h:dn,..::1d11111·_ rill.'>.: tbg i:--nlit u..;1..·d.
111 tilt.' EP.-\·-; l'tintract l.ahnrat11r: Prugra1111CL1·1. this tlag is us1.;d for ;.1 pe::;ti..:i<le/Arnclor target analyte. \,h .. ·n tht:re is ~reatt:r th:in :5~:0 differenct.: for derected concentrations between the [\\tl (iC 1.:t1lu1111i:-;_ The lower ufthe [\\l1 \·alues is repl)rtcd on Form I and flagged with a P. h1r S\\"-S-l6 (iC ;_rnd HPLC analys1..·s. wht.:11 the Relative Pen.:t:nt Difference (RPO) is greater than -lOq'o and 1li1..·re is ,w evidL'.nCL' nr clir0rnatt1~raphic arwmalies nr interferences. then the~ i..if tile 1wn \·;ilul..':. is re-paned and tlag.g.t.:J \\ ith :1 P. \\'hen the RPD is equal tu or kss than -l0°:;J. 1..1ur p1..ilicy i:, hi :tls11 report the ~ \lf the [\\11 \ :ilu1..·s. ;tlth0ugh the choici.: could be a proje..:t srK·1.:itii..: l_..;:-,u,.:.
This lhg applir..:s Ill CC 1.lr HPI.C rr..:-;ults \\h1..·rL' tilt.: idc.:11tit-1catinn li;b h1..·i..·11 continrn:<l b: GC!\IS. 1rcc·\1S ..:1..111lir111a1iLlfl \\:IS :!llt.:rnplt.'d hut \\:lS lllbd(L'L'S5t"ul. thi:-flag_ i:-; lhl[ appli~tL a 1~1h11rJll)r~-dL'll111..·d tb~ is usi.:d i11sti..::1d /:-ice.: thL· .\ ·y I ~u:ililii..:rl.
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DATA RF.PORTING QUALIFIERS ,,,,,1ti11"''''
/'hi, Jbc..: j..; l!.'t.:d ,\iiL'll rli1.· :111al_,tL' i:-,; t~)und i11 tht.: ;i..:-,,..:i:H,:d hl:111~ :1:-\\1,:II :i:-in the :;:1111p!1.:. !t
in,li...:;tll..'~ pr11h:ihk bl:111k Ll111tami11:1ti1,,l1J ;111d \\:Im.-. rh1.· dar:1 lhcr ftl 1al-.c appn1priafc :1L·til1r1. 1"11i:-
/l;i~ i:-u., .. :d !~1r :I 1·1c a:-\\'Cl! ;\:,i t~1r :1 pl1:-:iti\1.·ly id1.:111iti1.·J l:lf;!r..'[ Ctl11Jf1tllll!t!. ThL' cn111bi11:iri .. 1n ,.1(
rl:t~:, UL. (,r [ ·o i . ..; not an :tlhn\·abk· p1 1/icy. Bl:111~ ,.\11H:1rnin:111r., :11:L, tl:1~~1:d 13 t'lll_, \\hL'II 1/Jc_, :tr\:
dc!:'L"IL'J in t!i1.· :-:1J11pk.
E: :rhi:-tl:n.'. ilh:ntitics compound:,; whose: LLlllCt.:11tr:1r1L1ns c:.\:<.:ct:d t!ic upper lt.-n:l tlf th(..· calihrari,111
ran!!e nt':: rhc: i11s1rument tor tlwt spc:citic a11.1/ysi:--. I( \lac" or more co111pnu11ds hn\"t: a fL'Sf>tmsc
!.!rt:;ter than the upper level uf !ht: calibration range:. the: s:impk or c:xtra<.:[ \\·ill be dilureU and
;c:;:i.nalvzc:d. All such compounds \\"ith a n:sponse grc:.:ller than the uppc:r le\·d of rhc: calibr~llil)ll
range ~viii have the concentration flagged with an Eon Form l for the original analysis.
D ff :i sample nr e.xtract is reanalyzed at ;:i, higher <liluti011 factor. for ex;:i.mpk when rhe
c1)11centra1ion of an analyte exceeds the uppc:r calibration range. tht.: DL suffix is appended tn t!:~
sample number on Form I for the more dilured sample and all rc:ported concentrarions 011 that
Form 1 an: flagged \\"ith the D flag.. This flag alerts cbra l!St·rs [hat any discrepancies berwee'n the
rt:purted (l\/11.'.L'lltrarions may he..~ duL' rn dilution l1t" rhc: sample..· or ('.\tr.tct.
~fJTL 1. ThL' D !lag is nor applieJ !o curllpliu1ic.h \\hich an .. · Ill)[ dcteCtL'd in the sampk anal:,.-sis J.\..·.
ClHllJ)lHind-.. rq1,._irrc:J \\ irh tilt: CR()!. 11ir R.eporring Lim in and rlit: L: tlag .
•
\;{JI f·. ~: -.;t..·p:1r:1h.: 1·l1n11 1 :-; arc u:--ed t~1r rt_'f)ill"li11g lilt.· 11rigi11al :in:d_\si:--(Clit:11[ Sam pk :-.'l' .. \.\...\..\.\.) and
1lic 111,,rc di!utcd :-ample :111:il;·..;i:,; 1L"lil.'11I S:11nrk \"11 .. \ .. \.\.\.\DLJ i.e. rhc rt..·:--ulcs fr\1111 hiith
,rn;il; "'-"" :13.:1..· 11(11 c11rnhi11t.:d iHl :1 :--inglt: l-"lirrn I.
! Iii-.. lb:-'. 11i.!1,::tt1..·-.. 1liat :u1 :111:il;tc \\;is; d1..·tt..·-.·tl."d b; :1 ..;i11:'.k c11lu1n11 (;(." :111:il;:-i..; hut tht..· rl...' . ..;ult \\;i..;
[,d,,,, tll1..· l\1..,Tl'rt111:-l.i111it. !"hi:-; llag i-.. 11111; u..;l...'d ,,li .. ·n i.:!it:rll:-rt:~1ut::--1 :1 ~l.'-.·nnd (contirrn:itilHl)
...:,du11111 .111.il:-..1-.. :1r"lt:r dt:t1:cti11y. :111 :111:11:h.: :ihn,·1..· the Rq111rti11g l.i111it in the initial. .sin~k Cl1!u11111
.11u(, --.1--. ! hi-.. 11.ig :1krh 11!1.· dat:i Lh1.,:r that l11i!: :111 ;m:il:IL' ,,a.s dL·\1.·ctcd hchn\ tilt..' Rc..•p11rtin~
I 111111 .111d .1 ,1.·,.:1 111d 1\.·n11!in11:1ti1)1\) ;1nal::-i..; ,,;i:,; 111,t pcrl~1nnt.:d.
.\ Y / 1 >ther ,11,·c,1i, tbs, 111:i, be req11ir,·d ,,, properly dctii,c the rcs11lts. li'useu. the 11:igs "ill be full,
,k-..1..-rd1cd 111 lhr...' S!)(j \":irrati,c. Tile lah,1ratt)r:-Jctint..·J tbt'.s ~in.: limited tu X.Y an<l I...
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CompuChem
a di\·ision of Liberty Analytical Corporatio~
CompuChem's Pagination Convention
As required by the current EPA CLP Statement of Work (SOW) (Document Number OLM03.0.
plus revisions). data to be delivered must be paginated (by machine or hand). In the event that the
initial numbering is incorrect (a page numbered twice or a page skipped. for example). it is
ComjiuChem 's policy to add in an alphabetic suffix to a page number when necessary (e.g ..
I DOA. I 00B. etc.)
••
Forrn DC-2 presents an inventory of the contents of the CSF. including the page number
locations for the indexed items. There are concurrent delivery requirements for the Sample Data
Packages and the CSF. Because of this and the time required for the final technical review
process. we have instituted a policy to expedite assembly of the CSF. Items 2-6 on the Organic
Form DC-2 and items 2-26 on the Inorganic Forrn OC-2 contain those items which are part of the
Sample Data Packages. Those items will be paginated in ascending order. However. while
Sample Data Packages receive a final technical review, items 7-l O on the Organic Forni DC-2
and items 27-32 on the Inorganic Forrn DC-2 will be assembled and paginated. The first page
number for the first entry for item 7 on the Organic Forrn DC-2 and for item 27 on the Inorganic
Form DC-2 will always begin with page number I 0,000.
Revision 3 ( l 0/8/97)
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Quality Assurance Notice
The EPA CLP SOW (Document Number OLM03.0. plus revisions) requires. for tentatively
identified compound (TIC) assessment, that certain items should not be reported. These include.
for volatile organics, carbon dioxide and semivolatile TCL analytes and. for semivolatile
organics. volatile organics listed in Exhibit C.
In order to assist the data review/validation process by our clients. if we detect carbon dioxide or
semi volatile TCL analytes at or above I 0% of the closest internal standard we will report them
on the Form I VOA-TIC but not include them as part of the thirty (30) Tl Cs required. Similarly.
if _;e ·detect volatile TCL analytes from Exhibit C at or above I 0% of the closest internal
standard during the TIC assessment of the semi volatile analysis. we will report them on the Forni
[ · ~Y-TIC but not include them as part of the thirty (30) Tl Cs required. The library search ra\\
data for these T!Cs are also included. The total number of T!Cs listed on the Form [ in the
Number of Tl Cs field will include these items.
We feel this approach will aid the data review/validation process by our clients. siflce we will be
accounting for all peaks required to be: searched as "·ell as any other comparably sized peaks
present on the reconstructed ion chromatogram ( RIC).
Robert E. Meierer
Vice President
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;_;_,,1_t . .. '" ~
·1 ,-.• -.• ; ., .• ,,.c C -" • , :· ,,,,,.,, ""''1" ; .,., .. ya
_·:t-.ff:
B. Form I and Form I -TIC
Orgqnic Analysis Data Sheet (OADS) and·
Te~tatively Identified Compounds (TI Cs) ·
-All samples by fraction (VOA, SV, PEST) •· '· ·
-alphanumeric order within each fraction · ·
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
RC-'TBL-01
Lab Name: COMPUCHEM Contract: OLM03-REVS
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
SAS No.: SDG No. : 00001
Lab Sample ID: 938652
Sample wt/vol: 5.0 (g/mL) mL
LOW
Lab File ID: CN038652A57
Level: ( low/metli
% Moisture: not dee.
Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0 GC Column:EQUITY624 ID: 0.53 (mm)
Soil Extract Volume: (uL) -----Soil Aliquot Volume: -----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q
74-87-3---------Chloromethane 10 u
7 4 - 8 3 - 9 --· - - - - - - - B romome thane 10 u
7$~01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chlon.de 3 J
67-64-1---------Acetone 10 u
-~5-15-0---------Carbon Disulfi.de 10 u
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 10 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
56-23-5---------Carbon Tetrachloride 10 u
75-27-4---------Bromodichlorornethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-l,3-Dichloropropene 10 u
79-01-6---~-----Trichloroethene 10 u
124-48-1--------Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
10061-02-6------trans-l,3-Dichloropropene 10 u 75-25-2---------Bromoform --10 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 10 u
79-34-5---------1,1,2,2-Tetrachloroethane 10 u
108-88-3--------Toluene --10 u
108-90-7--------Chlorobenzene 10 u
100-41-4--------Ethylbenzene 10 u 100-42-5--------Styrene 10 u
1330-20-7-------Xylene (Total) 10 u
540-59-0--------1,2-Dichloroethene ( totaI) 10 u -
( ul
FORM I VOA OLM03.0
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lE
VOLATILE ORGANICS ANALYSIS
TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
EPA SAMPLE NO.
RC-TBL-01 Lab Name: COMPUCHEM Contract: OLM03-REVS
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
Sa':'ple wt/vol:
SAS No.: SDG No. : 00001
Lab Sample ID: 938652
Lab File ID: cn038652a57
I Level: (low/med')
5.0 (g/mL) mL
LOW Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0 I
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~ Moisture: not dee.
GC Column:EQUITY624 ID: 0.53 (mm)
Soil Extract Volume: ____ (uL)
Number TICs found: 1
CAS ' NUMBER COMPOUND NAME
Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
RT EST. CONC. Q
:;::;::;:;:::::;::;::;::;::;::;::;::;::;::;::;::;: -----------=:;:=-----======:;::;::;: ======== ============::: ===== 1. CO2 (NOT IN TIC TOTAL) 2 .53 42 J ·2 ..
3
4
5 •
6
7.
8
9
10
11.
12
13
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15
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18
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24.
25
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27.
28
29.
30
FORM I VOA-TIC OLM03.0
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lA
.. -~---w-.:,· ':"-. :"iS'f.~. EPA SAMPLE NO .. :·u,:
VOLATILE ORGANICS ANALYSIS DATA SHEET --------· 7l
Lab Name: COM PU CHEM
Lab· Code: COMPU
Matrix: (soil/water)
Sample wt/vol:
Case No.: 34336
WATER
RC-TMW-7
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938639
Lab File ID: CN038639A57
I Level: (low/med}
5. O (g/mL) mL
LOW Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0 I
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% Moisture: not dee.
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GC Column:EQUITY624 ID: 0.53 (mm)
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ____ (uL
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q
74-87-3---------Chloromethane 10 u
74-83-9--~------Bromomethane 10 u
75:Dl-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chlon.de 10 u
~7-64-1---------Acetone 10 u
· 5-15-0---------Carbon Disulfide 10 u
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 10 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
56-23-5---------Carbon Tetrachloride 10 u
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-1,3-Dichloropropene 10 u
79-01-6---------Trichloroethene 10 u
124-48-1--------Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
10061-02-6------trans-1,3-Dichloropropene 10 u
75-25-2---------Bromoform --10 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 10 u
79-34-5---------1,1,2,2-Tetrachloroethane 10 u --108-88-3--------Toluene 10 u
108-90-7--------Chlorobenzene 10 u
100-41-4--------Ethylbenzene 10 u
100-42-5--------Styrene 10 u
1330-20-7-------Xylene (Total) 10 u
540-59-0--------1,2-Dichloroethene (total) 10 u -
FORM I VOA OLM03.0
:,.:,-:.;;.:-.•-·J.,~~~-
----.' 'I'-'. l:t•l'''-'''s, 1 -..,.---•..:-·•·.,
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,,, ..
lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Ma_trix: (soil/water) WATER
Sample wt/vol:
Level: ( 1 ow/ med')
% Moisture: not dee.
GC Column:EQUITY624
5. O (g/mL) mL
LOW
ID: 0.53 (mm)
RC-TMW-7
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938639
Lab File ID: cn038639a57
Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0
Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ----
Number TICs found: 1
' CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
RT EST. CONC. ;:: :::; == =:;::;;:::;:: = == = = = ;:::;:; ===========::::::;::;::;::;:::::;:::::;::;:::::;::;::;::;::;:: ::;;:::====== ;::;::;:::::;;:;:::;;:::::::=====
1 . . CO2 (NOT IN TIC TOTAL) 5 95 114
2
3
'4
5 .,
' 0 ,7
8
'9
10
11
12
13
1:4
15
116
17
18
1.9
20
21
2_2
23
2.4
25
26
27
28
29
30
Q
::::::;:;:::;;:;::
JB
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FORM I VOA-TIC OLM03.0
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Contract: OLM03-REVS
SAS No.:
·-:'Ji EPA SAMPLE NO.·
RC-TMW-7A
I Mat~ix: (soil/water) WATER
SDG No. : 00001
Lab Sample ID: 938646
Sample wt/vol: Lab File ID: CN038646A57
I Level: ( 1 OW/ med·)
5.0 (g/mL) mL
LOW Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0 I
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% Moisture: not dee.
GC Column:EQUITY624 ID: 0.53 (mm)
'
Soi~ Extract Volume: _____ (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloriae
7~~00-3------~--chloroethane
75-09-2---------Methylene Chloride
67-64-1~--------Acetone
~5-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Sthylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (Total)
540-59-0--------1,2-Dichloroethene (total) -
FORM I VOA
10
10
10
10
2
4
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
____ (uL
Q
u
u
u
u
J
JB
u
u
u u
u
u
u
u
u
u
u
u
u
u u u u u u u u u
u
u
u
u
u
OLM03.0
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lE
VOLATILE ORGANICS ANALYSIS
TENTATIVELY IDENTIFIED
DATA SHEET
COMPOUNDS
Lab Name: COMPUCHEM Contract: OLM03-REVS
'
Lab Code: COMPU Case No.: 34336 SAS No.: SDG
Mat;rix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: Lab File ID:
\~~-........... :~:i.~·
.~:},'' EPA SAMPLE NO. ,:,,, --------~·-:;r
RC-TMW-7A
No.: 00001
938646
cn038646a57
I Le'-'el: (low./med)
5.0 (g/mL) mL
LOW Date Received: 05/15/99
Date Analyzed: 05/18/99
Dilution Factor: 1.0
% Moisture: not dee. I GC ,Column:EQUITY624 ID: 0.53 (mm)
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Soil Extract Volume: (uL) ----Soil Aliquot Volume: ____ (uL
Number TICs found: 1
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
RT EST. CONC.
------------------========================== ======== =;:;:_::::--=-----
i. CO2 (NOT IN TIC TOTAL) 5 .94 95 . 2
3
4
5. ·•
6
7.
8
9.
10
11.
12
13
14
15
16
17.
18
19
20
21.
22.
23
24
25.
26.
27
28
' 29
30
FORM I VOA-TIC
Q :::====
JB
OLM03.0
I lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
RC-TMW-8
I Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Contract: OLM03-REVS
SAS No.: I Matrix: (soil/water) WATER
SDG No. : 00001
Lab Sample ID: 938650
Sample wt/vol: 5.0 (g/mL) mL Lab File ID: CN038650A57
I Level: (low/med-).· LOW
% Moisture: not dee. I GC ·column:EQUITY624 ID: 0.53 (mm)
Date Received: 05/15/99
Date Analyzed: 05/19/99
Dilution Factor: 1.0
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Soi°l Extract Volume: (uL) -----Soil Aliquot Volume: ____ (UL
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
7S-01-4---------Vinyl Chloride 10 u
75~00-3---------Chloroethane 10 u
75-09-2---------Methylene Chlon.de 1 JB
67-64-1---------Acetone 7 J
15-15-0---------Carbon Disulfide 10 u
75-35-4---------1,1-Dichloroethene 10 u
75-34-3---------1,1-Dichloroethane 10 u
67-66-3---------Chloroform 10 u
107-06-2--------1,2-Dichloroethane 10 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 10 u
56-23-5---------Carbon Tetrachloride 10 u
75-27-4---------Bromodichloromethane 10 u
78-87-5---------1,2-Dichloropropane 10 u
10061-01-5------cis-1,3-Dichloropropene 10 u
79-01-6---------Trichloroethene 10 u
124-48-1---~----Dibromochloromethane 10 u
79-00-5---------1,1,2-Trichloroethane 10 u
71-43-2---------Benzene 10 u
10061-02-6------trans-1,3-Dichloropropene 10 u
75-25-2---------Bromoform --10 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 10 u
79-34-5---------1,1,2,2-Tetrachloroethane 10 u
108-88-3--------Toluene --10 u
108-90-7--------Chlorobenzene 10 u
100-41-4--------Ethylbenzene 10 u
100-42-5--------Styrene 10 u
1330-20-7-------Xylene (Total) 10 u
540-59-0--------1,2-Dichloroethene ( total j 10 u -
FORM I VOA OLM03.0
181.(-19
1,-
1
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM Contract: OLM03-REVS
,_;·,.;
EPA SAMPLE NO. ,;/:"
·;_.;.:,·
' RC-TMW-8
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
SAS No.: SDG No. : 00001
Lab Sample ID: 938650
Sample wt/vol: Lab File ID: cn038650a57
I Level: (low/medj
5.0 (g/mL) mL
LOW Date Received: 05/15/99
Date Analyzed: 05/19/99
Dilution Factor: 1.0
~ Moisture: not dee. I GC Column:EQUITY624 ID: 0.53 (mm)
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Soil Extract Volume: ____ (uL) Soil Aliquot Volume: ____ (uL
Number TICs found: 1
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) ug/L
RT EST. CONC. -----------------------------------========-=:;:;::;===== -------------1 CO2 (NOT IN . TIC TOTAL) 5. 97 124
2
3
4
5 ·•
6
7
8
9
10.
11.
12
13
14
15
16
17.
113 .
1~.
20.
21.
22
23
24
25
26
27.
28.
29
30
FORM I VOA-TIC
Q
=====
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OLM03.0
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
-.
RC-TMW-7MS
Lab: Name: COMPUCHEM Contract: OLM03-REVS
Lab Code: COMPU Case No.: 34336 SAS No.:· SDG No. : 00001
Matrix: (soil/water} WATER Lab Sample ID: 938640
Sample wt/vol: Lab File ID: CN038640A57 I Level: (low/med0)
5.0 (g/mL} mL
LOW Date Received: 05/15/99
Date Analyzed: 05/19/99
Dilution Factor: 1.0 I
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% Moisture: not dee.
GC Column:EQUITY624 ID: O. 53 (mm}
Soil Extract Volume: (uL}
I -----Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} ug/L
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75~01-4---------Vinyl Chloride
75~00-3---------Chloroethane
75-09-2---------Methylene Chlon.de
67-64-1---------Acetone
7'5-15-0---------Carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Bromoform --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (Total)
540-59-0--------l,2~Dichloroethene (total) -
FORM I VOA
10
10
10
10
2
9
10
46
10
10
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4
10
10
10
10
10
51
10
10
49
10
10
10
10
10
10
50
51
10
10
10
10
(uL -----
Q
u u u u
JB
J u
u u u
JB u u u
u u
u u
u
u u u
u
u
u
u u u
OLM03.0
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lA EPA.SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COM PU CHEM
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) mL
-.. -. --·--~ .... . -,·
RC-TMW-7MSD'
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938641
Lab File ID: CN038641A57
I Level: (low/med').. LOW Date Received: 05/15/99
Date Analyzed: 05/19/99
Dilution Factor: 1.0
% Moisture: not dee. I GC Column:EQUITY624 ID: 0.53 (mm)
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: _____ (uL
CONCENTRATION UNITS: I
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CAS NO. COMPOUND (ug/L or ug/Kg) ug/L Q
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74-87-3---------Chlorornethane
74-83-9---------Brornornethane
75-01-4---------Vinyl Chloride
7~:~o-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
.,5-15-0---------Carbon D1.sulf1.de
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
67-66-3---------Chloroforrn
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------Carbon Tetrachloride
75-27-4---------Brornodichloromethane
78-87-5---------1,2-Dichloropropane ·
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibrornochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------trans-l,3-Dichloropropene
75-25-2---------Brornoforrn --
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane
108-88-3--------Toluene --
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Xylene (Total)
540-59-0--------1,2-Dichloroethene (total) -
FORM I VOA
10
10
10
10
3
10
10
46
10
10
10
2
10
10
10
10
10
51
10
10
49
10
10
10
10
10
10
50
51
10
10
10
10
u u u u
JB
J u
u
u u
JB u u u
u u
u
u
u u u u u
u
u
u u
u
-
OLM03.0
21 r<'h c;t;
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COMPUCHEM
a division of Liberty Analytical Corp.
03/JUN/99
Roy F. Westcm
5405 Metric Pl.
suite 200
Norcross, GA 3009~
.. '
----------------
Subject: Report of Data -Account Number# 501223 Order# 34336
\~~~0Enclosed are the results of analytical work performed in accordance . ' { ,-,.,, [~• .. T:f\d.:1:;yi th the refer,;mced account number. •
~1t}\,:;~ii;~~i:
··· .. This· report covers 17 sample(s) appearing on the attached listing.
Thank you for selecting Compu~hem Environmental for your sample
ahalysis. If you should have questions or require additional
analytical services please contact your representative at
1-800-833-5097.
Sincerely,
l/ 1 ,,-Jl . . . . ·/ · , . , . r /,;(/ C . ...:;MtL __
CompuChem Environmental
a division of Liberty Analytical
Attachment
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: [phone]
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COMPUCHEM
a division of Liberty Analytical Corp.
03/JUN/99
Roy F. Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
ACCOUNT#: 501223
!i/~\:,f/ CC# SAMPLE-ID
:, ,.,;.,~1~·1:.I: \if: 1:i.!~;;: .
938559 RC-TMW-4
938563 RC-RBL-1
938564 RC-TMW-2
9~8565 RC-TMW-1
938566 RC-MW-1
938567 RC-TMW-3
938568 RC-PW-3
938569 RC-PW-2
938638 RC-TMW-5
938639 RC-TMW-7
938646 RC-TMW-7A
938647 RC-TMW-6
938648 RC-TMW-10
938649 TAR-POND3
938650 RC-TMW-8
938651 RC-TMW-9
938652 RC-TBL-01
TOTAL NUMBER OF SAMPLES
.i~./~:~ .. ~. ~ -··~:;r:0iit~r r::
. ·.,"":•e•:,;y_._., •· .. ::-• :._-··:-.•~·,;:;.~:r~-;-::_ -. -~---.-_. .
:· -::._,:;.,,.· .• ·. ..~--<--"-.-· .. ·.;..,. .. ,:.:, \: .
·-s;:.: ~ft?f, __ ~~)\i,:,;~.:~;~~-r::tr. ·._ ·
RECEIPT DATE
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
= 17
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: 919-379-i 100 ■ Fax: [phone]
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·. I
The sartip1e data summary package shall contain data for all samples
. in one Sample Delivery Group (SDG) of the Case, as follows:,
· A. SDG Narrative
B. Tabulated target compound results (Form I) .. -~:-"': < . · · , \ : __ •·
Tentatively identified compounds (Form I, TIC)(VO,'.\ & SV only)·
In order by fraction (VOA, SV, PEST) and by smiple ·-. . >
within each fraction. '· ·
C. System monitoring compound results (Form n ~ .. VOA only).·
Surrogate spike analysis results (Form II -S\(& PESTonly)
By fraction (VOA, SV, PEST), matrix (Water or Soil), .. · ..
and by concentration (Low or Mediwn) · ·
D. Matrix Spike/ Matrix Spike Duplicate results (Form Ill)
By fraction (VOA, SV, PEST)
E. Blank data (Form IV)
Tabulated blank results (Form I) ,
Tentatively identified compounds (Form I, TIC)
By fraction (VOA, SV, PEST) ··
F. Internal standard area response and retention time data (Form VIII)
By fraction (VOA & SY only)
LAB CODE : COMPU CONTRACT# : OLM03-REVS
CASE#: j;/JJ&
·.:.-,;;.;.;.;.. ··;; ... . '•-~:
. .-Yj!i
;~:.;;-?
'
.,
' .·•~~--; ........... .:.:....,.;,:.&:,.'.,:..•.;~.;:.~...::._:~-:'. ··-~·-·· -•-•:-.,.•:•:• :;-... ~ ..... ~:~-ri:,i'!l:,t,~.~~-.; ~ •~t:::,•--~~ ·~•~ •• ~ e
'
: ,_. ·~'.1 :i:t}/i;~;~~~\1!ifit~~~ ;'~.
I A. SDG Narrative
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--:;;·,·.
.';;
···,::f'"ll
2 I\ r/J-
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SDG NARRATIVE
CASE# 34336
SDG # 00001
CONTRACT #OLM03-REVS
SAMPLES: RC-TMW-7, RC-TMW-7A, RC-TMW-8, TAR-POND3
The four (4) water samples listed above were received intact, properly refrigerated, with proper
documentation, in a sealed shipping container; on May 15, 1999. The samples were scheduled for
the requested analyses of the semivolatile fractions. These samples were analyzed following the
current EPA Contract for the Laboratory Program, Document number OLM03.2.
All pertinent Quality Assurance notices are included in the narrative section and all pertinent
Laboratory notices for Case #34336, SDG #00001 are included in the sample data sections.
SEMIVOLATILE
The semivolatile fractions were extracted and analyzed within the required holding time. No
Target Compound List (TCL) analytes were detected with concentrations above the Contract
Required Quantitation Limit (CRQL) in the samples.
Two to thirty Tentatively Identified Compounds (TIC) were detected in the samples. These TICs
were assessed as unknowns, ketones, substituted benzenes, substituted phenols and
trichloropropene. Other TICs were detected and assessed as unknown alkanes in some of the
samples. The Tl Cs that were characterized as alkanes have been summarized on the Form I FAs
that are located in the narrative section of the data package. The TIC spectra for the alkanes are
located in the data section for the individual samples.
QCSUMMARY
The surrogates met recovery criteria for the semivolatile fractions, with some exceptions. The
recoveries of 2,4,6-tribromophenol failed acceptance criteria in samples RC-TMW-8 and RC-
TMW-7. The recovery of d5-nitrobenzene also failed acceptance criteria in RC-TMW-8.
The internal standards met area response and retention time criteria.
The duplicate matrix spikes met accuracy and precision criteria, with some exceptions. The
recoveries of 4-nitrophenol and pentachlorophenol failed acceptance criteria in the MS and MSD.
The associated blanks, Initial Calibrations and Continuing Calibrations met Quality Control
criteria.
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COMPUCHEM . :34336.00001
A division of Liberty Analytical Corporation
In the analyses of the Initial and Continuing Calibration standards and samples RC-TMW-7 and
TAR-POND3, manual quantitations were performed. The reasons have been coded with
explanations provided in the notice included in the narrative section of the SDG.
I certify that this ·data package is in compliance with the terms and conditions of the contract,
both technica:11y and for completeness, for other than the conditions detailed_ above. Release of
the data contained in this hardcopy data package and in the computer-readable data submitted on
diskette has been authorized by the laboratory manager or his designee, as verified by the
following signature:
Patricia B. Hopkins
Final Technical Review
2 June 1999
Note: This report is paginated for reference and accountability in numerical sequence.
I
I Client Sample ID: RC-TMW-7A Lab Sample ID: 938646 File ID: GH038646B~:f-
Compound RT Est. Cone. Q
I -------------------------------------------------------------------
Unknown Alkane 27.19 2.28 J
I Clie~t Sample .ID( T;;-POND3 Lab Sample ID: 938649 File ID: G2J38649A66
Compound RT Est. Cone. Q
Unknown Alkane 5.89 1433 J I ----~---------------------------------------------------------------
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••
m~~;,~~~t,f;::'.-.,-:·--:'., ... _ .. ,, ... -·------
.~t'f,~::.;bi .....:•.1 1' .
--... ;,;.·; _____ ····••· •·· ··•··----···-···· ·········--·----·-·· .... .. ·-·;H:4~
CompuChem, a· Division of Liberty Analytical Corporation :".;{.~ ,.,. ... -.
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. . .... . ··-:;;:;;~,
·:-::_qf_:\
GC and GC/MS Column and Trap Specifications Table
COLUMNS
Brand Name ~;; Coating .. -ID Film Thickness Length
Material (mm) (um) (m)
GC Laboratory
Restek RTX-1701 0,53 0,5 30
J&W DB-608 0,53 0,83 30
Restek CLPesticides 0.53 0,5 30
Restek CLPesticides II 0.53 0.42 30
GC Volatiles Laboratory
Restek RTX-1 0.53 0.5 105
Resfel( RTX-502.2 0.53 0.5 105
GC4MS Volatiles Laboratory
J & w DB-624 0.53 3.0 30/75
Supelco Equity™-624 0.53 3.0 75
GC/MS Semivolatiles Laboratory
J &W DB-5.625 0,32 1.0 30
J &W D85-MS 0.25 0.25 30
Hewlett Packard HP5-MS 0,25 0.25 30
TRAP
GC/MS Volatiles Laboratory
• 1 cm of methyl silicone packing (OV-1 coating)
• 8 cm of 2,6-diphenylene oxide polymer (Tenax)
• 8 cm of silica gel
• 7 cm of coconut charcoal
• 0.5 cm of silanized glass wool at each end
Rev. 6 5/10/99
· .:· ~;,;,..~ \J..rii~1~t~:~ft¢.::~~ft~)/:-:::::•~•:.:,:-::· .. · ·. !111£Jii'!~~-fR:e.ilws;r{t:<t:t· · · .. ·
_, .. --~-: CompuChem
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a <li\·ision of Liberty Anal_, tical Corporation
Notification Regarding i\tlanual Editing/Integration Flags
In some instancc"S:.·manu.a! Jdjustmi:::ncs co the sofm.-are ourpuc :ire necessary to provide accurate Cata. These
adjustments are-phformed by the data reviewer. GC:·Ms operator. or GC chemise. r\n E.xrracted Ion Currenr Profile
(EICP) ·or a GC chromatographic peak has been provided for the manual integration of each compound to
demonsrrate the accuracy of tha! process. Adjuscments are flagged on the quantit3.tion repon in the far right column
beyond 1he FfNAL concen1ra1ion for GC:MS analysis. and in 1he "Flags" column for GC analysis. The• manual
editing/integration flags are:
M
H
·•
L
-Denotes that a manual integration has been performed for this compound. The manual inregration was
performed in order to provide the most accurate area count as possible for the peak .
. Denotes that the data reviewer. GC/MS operaror. or GC Chemist has chosen an alternate peak within the
retention time windo\,1 from that· chosen by the soft'.A.·are for that compound. No manual integration rs
performed in choosing an alternate peak. The sofhvare still performs the integration.
-Oeno!es 1h.:it an alternate peak has been chosen \vithin the retention time \\.'indO\\." from !hat chosen b_\ th-.'
sofm·are for chat compound and also J manual integration of the chosen peak has been performed. The.·
manual integration \,.:as performed in order co provide the most .:iccuratt: .:irea counc possible for tht: pe.:ik.
-Denotes th:H the data rt::\'iC\\er or GC ".\1S oper.:iror has selt:ctcd an altemace !ibr.:iry search. Thi:i ts
cypicall: done when Jn additional tentati\·cly identified compound (TIC) has been added to the number of
peaks searched. No manual integr.:ition is performed in choosing an altema!e. peak. The software still
performs the incegrJtion.
-Denotes thJt .:in J!temate libr.:ir; search h.:is been ~,,lccted and J m::inu::il integration has also been
performeJ. This is 1vpicall,· done when an ad Ji:· .OJI TIC has been added and 1he TIC peak also required a
mJnual int-:gration
Wi1h the in1roduc1ion oi the curren1 EPA CLP SOW (Documeni ~umber OLM0J.0. plus revisions) addi1ionc:
e.xplana1ions for manual editing.'integration .:ire required. In 1he accompanying raw data packages . .:idditional codes
have been applied to the ··:,,.r tlag and carry the following meanings:
-The compound was not found by the aucomatic integration routine.
M:! -The compound w.:is incorrectly intt.'grated by the auwmatic integration routine.
. \13 -The co-eluting compounds were incorrect!: integr::ited by the auromatic integration routine .
Revision 4 (10/8/97)
Robert E. Meierer
Vice President
...._.~,.~~ • ,. I.
'•I"· -
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CompuChem
DATA REPORTING QUALIFIERS
( )11 tli1..· h1n11 1. u11d1..·r tli1..· ,:ulu11111 l:1hclcd ··(,) t~1r qualifi-.-r. i::1...:/i r1..•,..;ulr i:-: tb~~1..·d \\ i1li r/11..· :-111.·,:1/i,.: d:11;1 r1.:rl1ni11g liu:ditii.:r:--Ji:--tc:d hi.:llH\. ;1:-. ;1ppr\1pri:111..·. t.·p fl1 Ii\ 1..' qu:tliti1..·r., 111a; he rL·p11rt1:d ,111 Fl1n11 I f~1r i.::1...:/i
...:l1111pl1t!JJJ. Tho;.• qualitii:::-rs usi:::-J an::
L:
J :
f' .
C
This flag indicates the: comptH1rnJ \\:IS analyzt!d tix but 11nt dett.:l'.tc:d. The! Contract Rt..'quircd
Quantiration Limit (CRQL) (or Rc:porting Li111in will bc adjusti.:d tt1 rdh:ct any dilution and ti1r
soils. the percent moiswre.
This flag indicates an estimated value. The tlag is used as detailed below:
I. \Vhen estimating a concen1ratior1. for tentatively idt!ntitied cum pounds {T/Cs) whc:n.: a
response factor of 1.0 is assumed tor the TIC anahte.
\Vhc:n thc mass sp-:ctral and rc:t.:ntilHl tirn:.' dat.:i rnJiL:~llt.' the: prc:-st:"ncc: of ;:i conlplH!lld 1k11
rnt'.'c:t:,; thi::' vokHik aml -:.t.'llli\l)b1ik CC'\!S iJc:'ntiticati(111 -.:ri11..·ri:1 and rhl.' rt:;-;u!t i.-; lt.·ss 111,in
rhe CR()L (tH" Rc:pvning l.1rn11) hut grl.':l!t.:r tk1n 1:..-rv.
\\.ht.:11 tht.· rl.'ll.:11ti1 111 tirn-.· d:H:t indiL:lll.':-: tll¢. . .' pn.':it.'llcr.: .,11" :1 1.:(111tpliu11d that 1nt.'1..'I., !lit.·
p1:sti1.:idt.· .-\r .. 1.:l1)f 11r dlhL'r lil. ,1r 11/lL(" id1.·11ti1i,::ui1)11 critl.'ria and d1L.' rc:su!1 is k;-;:,; tli:in tlit.·
CR<)!. (1ir R-:poning l.lmitl rlui gn.:alc-r than /.1...-r11. FL1r .=.\alllplt.:. if tlit: CR()I. {t.'r Rc:p1.xring
l.i111itl is I() ug L hut a ClllH.:c.·111rati1111 uf _; ug l. i.-; ,::ik:ubt1:d. it i~ rcp11m .. ·d :1:-; 3J.
Thi:-tlat'. indiGllt::--rrcsurnpii\·i.; t.'\ idcih.:t: 11f a c11111 1h,urH..l. Thi:,; tlag is u1il) us.:d !l.1r TIC:;_\\ h1.-rt.:
1h1..· idt..'1llili...::iti1.111 i:-h;t..;t..'d 1111 :1 111:i:,;_-; ,p1.·...:1r:i! lihr:1r; "t.::1rch. FL,r g1..·n.:ri...: ...:h:irac1t..·rizatil,1l 11f ;1 TIC
,u..:li ;t, ·..:lil11ri11:1tcd h;drP..:;1rh1111·_ th-:~ tbg. 1:-. fll1t u.,-:d.
I 11 th-= FP.-\ ·, l°L1ntr:1ct l .aht1r:111.1r; Pr11gr:1111 1 Cl .1· 1. this tl.1g. i:-us.:d for a pe~ticiJe . .-.~\rLH,:lur larg_t:l
:uwl;t.:. \\h1 .. :11 tht.:re is greata than :5n;1 c.Jit"ft:rt:nct: ll"lr dl!tected com:e11tr.1tions hetwt:en the [\\1.,1
CIC ..:t1lum11s. fhe h."l\\t:r1.1ftht.: t\,11 \·;du1.·s i:,; rep1.1rted LHl Form I ~rnd tb.gged with a P.
l\1r S\\--S ➔6 (iC a11J HPLC anal;st:s. \\ht..'11 the Rt.:L:Hi\t Pert::t.:nt Differenct: (RPD) is greater than
40°n :111d tht..'rt: is 1h1 e,·idt.:11..:e n!" dm . .\111at1.1g.raph,i: a111.1malies t)r interferenc...:s. then the~ L'f the(\\()\ alu,:s is rt.:portt.:d :rnJ tlag.g.eJ \\ ith :1 P. \\"h-:11 tht: RPO is t..'qual tLl or less than -W0-'0. 1.lur
1wlicy is t1.1 :ils1.1 rt.:pon !ht..' hi\..'.ht..T 1.'t" tilt.:{\\() \;ilue-.. :Ilthciugh tht.: .:hnict.: ..:uuld be a prr1jt..'..:t
-;pt:l.'.i ti..: i_-;_-;ut.:.
l"hi:,; lb~ :ipp\ie:, tu (iC 11r HP\.L" rt:,ul1:s \\h1.-rt..' tht..' idi.:ntiti..:::1ti1111 ha:-ht.:t:11 contirmcc.1 hy GC:,\IS.
!t"( il' .\1S ,.;l)lltirrn:ilil,n \\;1:-. ;ttlt.:nq11;:d hut \\;J:-; llll:-.d..:S:t.::-i:-fu!. 1hi~ tb~ i.-. 111.)t :1ppli1.·d: :1 !:ihPrat1.)ry-
\kt"111t:d tbg i:-u,t:d 11l.'\it.::1J 1 .;1.•t: !lh.: \ Y /. qu:diliL"rJ.
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D:
D.-\ T..\ RE PORTING Q l'.-\LI Fl ERS ,,,.,,,;""'·i'
1111, tb~ j ... u .. 1.:,I \\111..·11 tli1..· :111al;11..· i:,; i'1 1u11d i1( !11,: .t.,,,1..:i:111.·1.l hl:t11/.. :1:, \\t.:ll :1...; in !111..: :-;:i111pk. !t
rridi,::11,:., pr,,luhk· hl;111k ...:1.1nr:1111i11ati1.1n :ind \,:1r11., tilt.· d:1r:i u_..;._,·r 11.1 r:1l,;1..· aprropri:1(1..' :11..·1iu11. Thi . ..:
lb~ i .... lh1,:d ,.l,r :i r·ic :i...; \\t.'11 :1...; /~1r ;t p11:--ici,1..·I., id1..·1ni/ic.:d wr~1..•[ Lll111p1ILJ1h.!. Th,: 1..'1,l!llhi11:iri1.111 ti,.
lb~:-!Jl. ,1r ( ·u j..; 111.1[ :ill :1l/1.l\\;1bk p1 1li...:;. B!:inl-. .. :111!f:1111in:111t.,·:1r1..· ll:1~gt:d B 1lfil_, ,,h1.·11 rl!1.·_, ;m.:
d...:1:•,:rcd in tli1..· :-:1111pk.
TJ11~..; tl;~g idcrHilic . ..; ...:1..11t1pl1ur1<J, ,,lhbt: L1..H1t:1..·111r:H1t111s t.'.\Lt:cd rile.: uppt:r k·,·c:l 1.if t!JL· ...:alihrati1.H1
ran!.!c.' 1.)f tht: i11sirn111c.:11t fur that :;per..:iti...: analy:-is. If l1;11;..• ur JJJori..· CL)lllpL)llllds ha\·c a rcsplHb, . .'
~ri..·;tc:-r than the upper k\·el t>f tilt: calibration range. rht sa111pk.-lll" cxtract \\ ill hi..· dilutt.'d and
rt:an.'.llyzt.'d. All such compounds \\·ith a rt.'sponst: grt!'.'.ltt'r than thi..· uppt:r Jt:,·L'l of the calihratillll
ranl.!t!' will ha\·e the corKentration tb\.!!.!t:d wirh an E l,n Form l tl1r rhi..· uri\.!ina! :1113h·sis. ----.
If :i sampk l,r extract is re:1nalyzed at a hight.'r dilution focror. for c:xampl•: \\·hen rhc.-
cn111.:t:ntra1iLm of an analyte t:xceeds the ,upper calibration range. thL' DL suftix is appended to the
:-.a111pk number on Forni ! for thL' more diluted sample and all reported concentrations 011 th:H
Fl)rm I.are tlaggc.'d \\ith the D tlag. This flag: alerts dJ.ta usc•rs that J.ny discrepancit:-s between 1/Ji.:
rt."rlmL'd L'llllCcntrations may he: due tl', dilution 1lf rite.' :-amplt: l1r extract.
\'{ )ll·: l. The [) lb:! j._ Jll.ll arrlit:d tl) L'lllllpllll!lds \\lii.:11 :lfL" 111.it J1;..•[1;..'C(L'd in tilt: :-ampk analysis l.l".
L1lrllJhHHld:-. l'l'plim:J \\ith rh.: CRt)I. (\,r Rcporting L11nit) and th,.-t_· tlag .
••
'\.( 1 J ! ~-'-\l·p:1r:trl· 1:,,nn 1 ... :1r ... : u..;l·d !l 1r rl·p1,rting !11l· 1lri:!i11:1I :rnal_\ _..;i:-: (Cli.:m S;1111pk· \;l, . .\.\.\.\.\ 1 and
till' 111\lfl" \.!ilLHl·d :-..11Jtpk· :111:d;,i:-tl"!i.:11{ S:1111pl,.; '-1' . .\.\.\.\.\()(.) i.\..·. tilt.· r.::-.ults rrlllll hl1th
.111:il:, ... L .... :1rl· lh'l ..:1,111hi11L·d dll ;i :--in:!k h1r111 I
I !11 ... rl.1~ 111-11,:.n:..· ... tli:11 :111 :111:il:, k \\:t"' 1k11..·..:tl·d h:, :1 ... 111:'.k ..:11lu11111 < iL. ;111:d:, :-i:-. hut 1!11;..• rL.'>ull \\;1._
i1\,.·l1•H rlil· .1-:, .. :p1•rt111":'. I i111it l'his tb~ t:-. ,1111; u-..;Ld \\ilL'll clii..:11h rt.·qui..:.'>t :t :-.c..:1111d (c11i11lrr11:1ti1llll
.__·,•lu111n ,111,il:, ... 1 .... 1111;..•r \kll·ct111~ :111 :u1;1l; IL :1h11\ l' 1h,.._· l{.:p11nin:! I .ir11i1 in tilt.' i11iti:1l. :-.ingk ..:1:lu11111
.111.11\ ... 1, llli-. tb~ Jk:n ... lilt: 1.!:il:! lht:r tha! ,111!:, .u1 .111,d;tt: \\;t.-. lkll'Ltt.·d h.._.km Ilic Rt.·p,11·ti11:-
I 111111 .11hl .1 "'l'L1•11d ILl111lirin:ttil111) :111:11; :-i:-\\;t:-, 11,,t pt.·rt~1n11L'd.
.\ Y /. 1 lthcr ... pl·c11·1._: 11:t:!:-. rn:1; h:...' r,._·quirL·d t11 pn1pcrh ddi1::: tht.· rt.::-tilt.-:. lfus .... ·J. thc tla!.!:-\\·ill ht: fulh
,k· ... ..:rihLd 111 th:.·_',!)( i ,:1rr:1ti,e. ThL' lat'l\1ratnr;.JdineJ tlags art.· li111i1LJ (n X.Y a1;d Z.
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. . ·_ ~ ..... '
,. ~ii'~~~.
CompuChem
a division of Libert~· Analytical Corporation
CompuChem's Pagination Convention
As required by the current EPA CLP Statement of Work (SOW) (Document Number OLM03.0.
plus revisions). data to be delivered must be paginated (by machine or hand). In the event that the
initial numbering is incorrect (a page numbered twice or a page skipped. for example). it is
(ornpuChem·s policy to add in an alphabetic suffix to a page number when necessary (e.g ..
100.-\. 1008. etc.I
Fom1 DC-2 presents an inventory of the contents of the CSF. including the page number
locations for the indexed items. There are concurrent delivery requirements for_ the Sample Data
Packac:es and the CSF. Because of this and the time required for the final· technical review
process. we ha,·e instituted a policy to expedite assembly of the CSF. Items 2-6 on the Organic
Ft,r111 DC-2 and items 2-26 on the Inorganic Fenn DC-2 contain those items which are part of the
S,1111ple Data Pacbges. Those items will be paginated in ascending order. Howe,·er. while
SJmple Data Packages receive a final technical re,·iew. items 7-\0 on the Organic Fom1 DC-2
JnJ items 17-32 on the Inorganic Fom1 DC-2 will be assembled and paginated. The first page
number for the fast entry for item 7 on the Organic Fom1 DC-2 and for item 27 on the Inorganic
Form DC-2 "ill always begin with page number 10.000.
Revision 3 ( l 0/l(r 6 (-{~
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CompuChem
a division of Libert~ A.naly1ical Corporation
Quality Assurance Notice
The EPA CLP SOW (Document Number OLM03.0. plus revisions) requires. for tentatively
identified compowid (TIC) assessment, that certain items should not be reported. These include.
for volatile organics, carbon dioxide and semivolatile TCL analvtes and. for semivolatik
organics. volatile organics listed in Exhibit C.
In order to assist the data review/validation process by our clients. if we detect carbon dioxide or
semi volatile TCL analy1es at or above I 0% of the closest internal standard we will report them
on the Form I VOA-TIC but not include them as part of the thirty (30) Tl Cs required. Similarly.
it' ~:e detect volatile TCL analytes from Exhibit C at or abo,·e 10% of the closest internal
standard during the TIC assessment of the semi volatile analysis. we will report them on the Forni
1 SV-TIC but not include them as part of the thirty (30) TICs required. The library search ra"
data for these TICs arc :ilso included. The total number of T!Cs listed on the Forni I in the
\'umber of TI Cs tie Id will include these items.
We feel this approach "·ill aid the data re, iew/validation process by our clients.-since we "·ill be
accounting for all peaks required to be searched as well as any other comparabl,· sized peaks
present on the reconstructed ion chromatograni ( RIC).
Robert E. Meierer
Vice President
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Organic Analysis Data Sheet (OADS) ariq, ·.· ·•
Tentatively Identified Compounds (TI Cs} .. /,_>
--All samples by fraction {VOA, SV; PEST);
-alphanumeric order within each fract1dri'··· ,. . ii
' . '·• ... •' '•, . -.
-, .. -·.:.
'. -.. ' -
1B I
I
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
I Matrix: (soil/water) WATER
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938639
Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: G2J38639A64
I Level: ( low/me-ct:) Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/25/99
Dilution Factor: 1.0
% Moisture: decanted: (Y /N)
I Concentrated Extract Volume: l000(uL)
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Injection Volume: 2.0(uL)
GPC,Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108095-2--------Phenol
1if-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
·\06-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4cDimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
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10 u
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10 u
10 u
10 u
10 u
10 u
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10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
~f~~~:~~::~{::~-~~:;.~,_-.. :'-..,..w_.; .:-·-.
l ~~~{,:j;-?!'. .
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,qr.;., ~. . ·-
-..
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab'.Name: COMPUCHEM
Lab-Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
Sample wt/vol:
RC-TMW-7·
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938639
Lab File ID: G2J38639A64
I Level: (low/med)
1000 (g/mL) ML
LOW Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/25/99
Dilution Factor: 1.0
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% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
5i~28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
·~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
25 u
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10 u
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10 u
10 u
10 u
25 u
25 u
·10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
. ····"'i;
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lF EPA SAMPLE NO.
SEMIVOLATil,E ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM
Lab Code: COMPO Case No.: 34336
-Matrix: ( soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/meElJ-LOW
% Moisture: decanted: (Y /N)
RC-TMW-7
Contract: OLM03-REVS
SAS No.: SDG No. : 00001
Lab Sample ID: 938639
Lab File ID: G2J38639A64
Concentrated Extract Volume: 1000 (uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/25/99
Dilution Factor: 1.0 Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH:
Number TICs found: 2
CAS-NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q . ============-=== ------==----====-=====------======== ============= ;;;::::;::;::::;;
1. TRICHLOROPROPENE (BC) 5.74 3 JB
·2 UNl'".NOWN 21. 27 5 J
3 •
4
5.
6.
7.
8.
9. :i:o.
11.
]: 2
13
]'4
15.
16
]7.
18
19.
20.
21.
2'2.
23
24
25.
26
27.
28
29.
30.
FORM I SV-TIC OLM03.0
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lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Contract: OLM03-REVS
SAS No.:
EPA SAMPLE NO.
.. ··:··::·.~~:::•:~~'.:~•·~-···-··
RC-;'_'I'.l'IW~]A.
I Matrix: (soil/water) WATER
SDG No.: 00001
Lab Sample ID: 938646
Sample wt/vol: ·Lab File ID: GH038646B64
I Level: (low/med·)
1000 (g/mL) ML
LOW Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
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% Moisture: decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2.0(uL)
GPC,Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
i~S,95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
1ii-44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
;41-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylarnine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenoi
105-67-9--------2,4-Dirnethylphenol
lll-91-l--------bis(2-Chloroethoxy)rnethane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-rnethylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dirnethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
-~·:/,{~i,-;;;.;.;,;.,
...
I
;.,•-•:, 1
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
.E;;t;,;;;,LB ;;i,': i
I Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
I Matrix: (soil/water) WATER
Contract: OLM03-REVS
SAS No.: SDG No. : 00001
Lab Sample ID: 938646
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Sample wt/vol: 1000 (g/mL) ML Lab File ID: GH038646B64
Level: (low/meo:) · :,ow
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
5}~28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate -117-84-0--------Di-n-octylphthalate
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
17 1; rr
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS RC-TMW-7A
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
· Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938646
Sample wt/vol: 1000 (g/mL) ML Lab File ID: GH038646B64
Level: (low/med·)· LOW
% Moisture: decanted:
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N
Number TICs found: 6
(Y/N)
l000(uL)
pH:
CAS N_T.JMBER COMPOUND NAME
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC.
============--== -=======--==--============== ========= =============
. l. UNKNOWN 5.61 11
2. TRICHLOROPROPENE (BC) 5.75 33
, 3' •• UNKNOWN (BC) 8.00 9
4. UNKNOWN 10.24 7
5. UNKNOWN (BC) 10.75 3
6. UNKNOWN 12.27 4
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20. -21.
22.
23.
24.
25.
26,
27,
28.
29.
30.
FORM I SV-TIC
Q
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JB
JB
J
JB
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OLM03.0
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lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET .
Lab Name: COMPUCHEM
Lab Code: COMPU
Matrix: (soil/water)
Case No. : 34336
WATER
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938650
Sample wt/vol: 1000 (g/mL) ML Lab File ID: GJ038650A64
Level: (low/med)
% Moisture:
Concentrated Extract
Injection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
l000(uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
10~~95-2--------Phenol
11i:44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
to6-46-7--------l,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
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10 u
10 u
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10 u
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10 u
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10 u
10 u
10 u
25 u
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OLM03.0
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SEMIVOLATII,E ORGANICS ANALYSIS DATA SHEET
:~'.~IJ
EPA SAMPLE NO. :IJ·
·R1·{:r}'i§t~f'·. '(} I Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
I Matrix: (soil/water) WATER
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938650
I Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: GJ038650A64
I Level: (low/med") Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
% Moisture: decanted: (Y/N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
GPc'c1eanup: (Y/N) N pH:
CAS NO. COMPOUND
si~.28-5--

-

-

-

-

-
--2, 4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
~21-14-2--------2,4-Dinitrotoluene
. 4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205--99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
25 u
25 u
10 u
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
.f
I
I
. lF
SEMIVOLATILS ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab: Name: COMPUCHEM Contract: OLM03-REVS
Lab Code: COMPU Case No.: 34336 SAS No.:
EPA SAMPLE NO.
RC-TMW-8
I Matrix: ( soil/water) WATER
SDG No.: 00001
Lab Sample ID: 938650
Lab File ID: GJ038650A64
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Sample wt/vol:
' Level: (low/med)
% MOisture:
1000 (g/mL) ML
:.,ow
decanted:
Concentrated Extract Volume:
(Y/N)
l000(uL)
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH: -
Number TICs found: 3
CAS NUMBER COMPOUND NAME . ..
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC.
========--===-----======---================= ======== =============
1. UNKNOWN 5.60 4
~-TRICHLOROPROPENE (BC) 5.74 16
3. .. UNKNOWN (BC) 7.98 3
4.
5. 6.
7.
8.
9.
10
11.
12
13.
14.
15.
16
17.
18
19.
20.
21.
22.
23
24
25.
26
27
28
29.
30
FORM I SV-TIC
Q
=====
J
JB
JB
OLM03.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
TAR-POND3·.' ·.
Contract: OLM03-REVS Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336 SAS No.: SDG No. : 00001
Lab Sample ID: 938649 Matrix: (soil/water) WATER
Sample-wt/vol: 1000
LOW
(g/mL) ML Lab File ID: G2J38649A66
Level: ( low/med)
% Moisture: decanted: (Y /N)
Concentrated Extract Volume: l000(uL)
Injection Volume: 2. 0 (uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/30/99
Dilution Factor: 1.0
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
1if~44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48°7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2 J
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
10 u
OLM03.0
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
I Mat~ix: (soil/water} WATER
Contract: OLM03-REVS
SAS No.: SDG No. : 00001
Lab Sample ID: 938649
Sample wt/vol: 1000 (g/mL} ML Lab File ID: G2J38649A66
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Level: (low/med·)
% MOisture: decanted:
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
(Y/N}
l000(uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/30/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
5i~28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
-~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---"-----Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218 -01-9 - - - - - ----Chrysene _
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-g--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h}anthracene
191-24-2--------Benzo(g,h,i}perylene
(1) -Cannot be separated rrom Diphenylamine
FORM I SV-2
Q
25 u
25 u
1 J
10 u
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
25 u
2 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
I
I
I
lF EPA SAMPLE NO.
SEMIVOLATII,E OP.GANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab, Name: COMPUCHEM
Lab Code: COMPU Case No. : 34336
I
Matrix: ( soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
TAR-POND3
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938649
Lab File ID: G2J38649A66
. I Level: (low/med) LOW Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/30/99
Dilution Factor: 1.0
%" Moisture: decanted: (Y/N)
I Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL) I GPC Cleanup: (Y/N) N pH:
Number TICs found: 30
CAS NUMBER COMPOUND NAME
-.... -·
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC.
I
I
I
I
I
I
I
I
I
I
I
I
==============--============================ :::::::::::;::::::::::::::::::::::::::: ======;::;======
1. SUBSTITUTED BENZENE 6.35 160
2. UNKNOWN KETONE 7.07 260
3. ·• UNKNOWN 7.73 510
4 . UNKNOWN 8.15 210
5. PROPYLPHENOL 8.64 100
6. UNKNOWN 9.24 100
7. UNKNOWN 13.80 86
8. UNKNOWN 13.88 100
9. UNKNOWN 13.97 140
10. UNKNOWN 14.09 400
11. UNKNOWN 14.25 420
12. UNKNOWN 14.34 490
13. UNKNOWN 14.55 1100
14. UNKNOWN 14.85 130
15. UNKNOWN 14.90 130
16. UNKNOWN 14.97 88
17. UNKNOWN 15.01 140
18. UNKNOWN 15.32 240
19. UNKNOWN 15.55 140
20. UNKNOWN 15.64 110
21. 90-44-8 ANTHRONE 15.73 110
22. UNKNOWN 16.02 96
23. UNKNOWN 16.22 190
24. UNKNOWN 16.37 120
25. UNKNOWN 16.44 100
26. UNKNOWN 16.55 90
27. UNKNOWN 17.13 190
28. UNKNOWN 17.44 650
29. UNKNOWN 17.69 920
30. UNKNOWN 18.02 1700
I
FORM I SV-TIC
Q
:::::::::::::::;::;:;;;:
J
J
J
J
J
J
J
J
J
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J
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J
J
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J
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J
J
J
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J
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OLM03.0
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I
I
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1B EPA SAMPLE NO.
SEMIVOLATILS OP.GANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
' Lab Code: COMPU Case No.: 34336 ·
Matrix: (soil/water) WATER
Sample wt/vol:
,' ,RC-TMW-.. 7AMS,;f
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938644
Lab File ID: GH038644B64
I Level: (low/med)
1000 (g/mL) ML
LOW Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
% Moisture: decanted: (Y /N) I Concentrated Extract Volume: l000(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
·108-95-2--------Phenol
lli~44-4--------bis (2-Chloroethyl) ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane -120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
88-74-4---------2-Nitroaniiine
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
76
10 u
61
10 u
32
10 u
10 u
10 u
10 u
43
10 u
10 u
10 u
10 u
10 u
10 u
10 u
38
10 u
10 u
10 u
72
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
41
OLM03.0
1--.
l. i
I
I
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Contract: OLM03-REVS
SAS No.:
EPA SAMPLE NO.
-RC-TMW-7AMS
I Matrix: (soil/water) WATER
SDG No. : 00001
Lab Sample ID: 938644
Sample wt/vol: 1000 (g/mL) ML
LOW
Lab File ID: GH038644B64
I Level: ( low/med) Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
% M~isture: decanted: (Y /N)
Concentrated Extract Volume: 1000 (uL)
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
51-28-5---------2,4-Dinitrophenol
100~02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
-~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(11 -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
25 u
80 E
10 u
47
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
100 E
10 u
10 u
10 u
10 u
10 u
46
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I I
I
lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM Contract: OLM03-REVS
EPA SAMPLE NO. :)11~:;
·~~t
RC-TMW-7AMSD
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) WATER
SAS No.: SDG No.: 00001 ·
Lab Sample ID: 938645
Sample wt/vol: 1000 (g/mL) ML Lab File ID: GH038645B64
Level: (low/med}··
';; Moisture:
Concentrated Extract
Injection Volume:
LOW
decanted:
Volume:
2.0(uL)
(Y/N)
1000 (uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
1r1=44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
1'06-46-7-- - - ----1, 4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78~59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-1--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
76
10 u
63
10 u
29
10 u
10 u
10 u
10 u
58
10 u
10 u
10 u
10 u
10 u
10 u
10 u
34
10 u
10 u
10 u
70
10 u
10 u
10 u
25 u
10 u
25 u
10 u
10 u
10 u
25 u
37
OLM03.0
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lC
-SEMIVOLATILE ORGANICS ANALYSIS_ DATA SHEET
RC-TMW~7AMSD
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Ma,trix: (soil/water) WATER
Contract: OLM03-REVS
SAS No.: SDG No.: 00001
Lab Sample ID: 938645
Sample wt/vol: 1000 (g/mL) ML Lab File ID: GH038645B64
Level: (low/med) · LOW
%-Moisture: decanted: (Y /N)
co'ncentrated Extract Volume: 1000 (uL)
Injection Volume: 2.0(uL)
Date Received: 05/15/99
Date Extracted:05/17/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
· 51-28-5---------2,4-Dinitrophenol
ro6-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated tram Diphenylamine
FORM I SV-2
Q
25 u
81 E
10 u
45
10 u
10 u
10 u
25 u
25 u
10 u
10 u
10 u
100 E
10 u
10 u
10 u
10 u
10 u
49
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
OLM03 .0
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COMPUCHEM
a division of Liberty Analytical Corp.
03/JUN/99
--;;·
Roy F._Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
('D:)r:?_n\l[lf?
JUN O 4 REC"O
----------------
Subject: Report of Data -Account Number# 501223 order# 34336
, ~Enclosed are the results of analytical work performed in accordance
"-,~: ,1 ·::-with the re_f erenced account number. :r.:\·.·;\:~;;;~(:
This·~eport covers 17 sample(s) appearing on the attached listing.
Thank you for selecting CompuChem Environmental for your sample
an~lysis. If you should have questions or require additional
analytical services please contact your representative at
1-800-833-5097.
Sincerely,
,... . Ii \ -~r ~-ML i . -
CompuChem Environmental
a division oi Liberty Analytical
Attachment
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: 919·379-4100 ■ Fax: [phone]
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COMPUCHEM
a division of Liberty Analytical Corp.
03/JUN/99
Roy F. -Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
.-~.--, .. }, CC# l,ii:r:• ·L·•·
::;/;"\i:f\!
938559
938563
938564
9:l'8565
938566
938567
938568
938569
938638
938639
938646
938647
938648
938649
938650
938651
938652
ACCOUNT#: 501223
SAMPLE-ID
RC-TMW-4
RC-RBL-1
RC-TMW-2
RC-TMW-1
RC-MW-1
RC-TMW-3
RC-PW-J
RC-PW-2
RC-TMW-5
RC-TMW-7
RC-TMW-7A
RC-TMW-6
RC-TMW-10
TAR-PONDJ
RC-TMW-8
RC-TMW-9
RC-TBL-01
RECEIPT DATE
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
5/15/99
TOTAL NUMBER OF SAMPLES= 17
501 Madison Avenue a Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: [phone]
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The-sample data package shall include data for all analyses of all samples
in one Sample Delivery Group (SDG), including field and analytical samples,
reanalyses, blanks, spikes, duplicates, and laboratory control samples. The
sample data package consists of the following:
A. Cover Page
·B. Sample Data
"
C. Chain-of-Custody (CoC) Documentation
LAB CODE : COMPU
CASE#: 3 C/J'J0
CONTRACT# : ILM04.0
SDG # : ~6,{j6 /
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A. Cover Page -,
Inorganic Analyses Data Package.
-.;:;.·
The Cover. Pa!:ie includes laboratory information, the Case and SDG numbers, the client ID
numbers in alphanumeric order showing the client ID numbers cross-referenced with Lab ID ·
numbers, comments, and completion of the statement on the use of ICP background and
· interelement correction for the samples. , · · · , . ' · , .·.· .·
On separate pages, the laboratory will include any problems encountered; both te~hnical and
administrative, the corrective action taken, and the resolution, This information is included in
. the Inorganic Case Summary Narrative which follows the Cover Page:,'>< . .
2 /'\
11':)
I Lab Name: COM PU CHEM Contract: ILM04.0
Lab Code: COMPU Case No.: 34336 SAS No.:
I sow No.: ILM04.0
I EPA S<a1mple No. Lab Sample ID
RG---'MW-1 938566
RC-PW-2 938569 -RC-PW-3 938568
I RC-RBL-1 938563
RC-TMW-1 938565
RC-TMW-10 938648
I RC-TMW-2 938564
RC-TMW-3 938567
RC-TMW-4 938559
I RC-TMW-4D --938561 -RC-TMW-4S 938560
RC-TMW-5 938638 -RC-TMW-6 938647 -I RC-TMW-7 938639 -RC-TMW-7A 938646
RC-TMW-8 938650
I ,. RC-TMW-9 938651 -TAR-POND3 938649
lwere ICP interelement corrections applied?
•
Were ICP background corrections applied?
If yes -were raw data generated before
application of background corrections?
SDG No. :00001
Yes/No YES
Yes/No YES
Yes/No NO
I Comments: ·
THE FOLLOWING ANALYTES HAVE BEEN FLAGGED WITH AN "E" TO INDICATE
--SERIAL DILUTION RESULTS WHICH WERE OUTSIDE CONTROL LIMITS: -----
•==SODIUM---
', 1 I certify that this data package is in compliance with the terms and
.conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
in this hardcopy data package and in the computer-readable data submitted I on floppy diskette has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature.
I Signature: ob~ /2, d j,,.t Name: ~
· Date: L,, /2-c 3 / 79f u J
Title:
I
COVER PAGE -IN ILM04.0
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~ --:-:,. •'
'• ~""-
Com uChem
a Division of Liberty Analytical Corp.
501 Madison Avenue Cary, NC 275IJ
INORGANIC CASE SUMMARY NARRATIVE
CASE# 34336 SDG # 00001
CONTRACT# ILM04.0
The indicated Sample Delivery Group (SDG) consisting of sixteen ( 16) water samples was received into
the laboratory information management system (LIMS) on May 14 and 15, 1999 intact and in good
condition with Chain of Custody (COC) Records in order, unless otherwise noted in any attachments or
Quality Assurance Notices. Sample !D's reported in this data package are noted by the receiving
department on the COC if they differ from those listed by the samplers on the COC.
The samples were analyzed, in accordance with EPA CLP Statement of Work (SOW) document ILM04.0
for the metallic ana\ytes contained in the Inorganic Target Analyte List (TAL).
jhe Form IO for the mercury IDL shows a reading of 0.0 ug/L. There is an inability to get the IDL: 0.048
ug/L to show on the form .
. • SAMPLE IDs:
The following customer IDs are associated with this SDG:
RC-TMW-1
RC-TMW-6
RC-PW-3
RC-TMW-10
RC-TMW-7
RC-RBL-l
RC-TMW-2 RC-TMW-3
RC-TMW-7A RC-TMW-9
TAR-POND3 RC-TMW-8
INSTRUMENTAL QUALITY CONTROL:
RC-TMW-4
RC-MW-I
RC-T!VfW-5
RC-PW-2
All calibration verification solutions (!CV & CCV), blanks (!CB, CCB) and interference check samples
(!CSA & ICSAB) associated with this data were confirmed to be within EPA CLP allowable limits.
SAMPLE PREPARATION QUALITY CONTROL:
The sample preparation procedure verifications (LCSW & PBW) were found to be within acceptable
ranges and all field samples were prepared and analyzed within the contract specified holding times.
MATRIX RELATED QUALITY CONTROL:
The sample marrix spike. CCN -938560 (RC-TMW-4S) was found to be inside CLP conrrol limits for the
requested analytes.
CLP control limits for matrix spike recoveries are set at 75% to 125% of the analyte quantity added unless
original sample concentrations exceed the true values of these "spikes" by a factor of four or more; in this
case effected analytes are not flagged even if recoveries fall outside percentage recovery control limits.
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The sample matrix duplicate, CCN = 938561 (RC-TMW-4D) was inside CLP control limits for the
requested analytes.
CLP control limits for duplicate determinations are+/-20% Relative Percent Difference (RPO) for
concentrations greater than or equal to five times the CRDL in both the original and duplicate samples, and
+/-the CRDL for concentrations less than five times the CRDL. The RPD is not calculated if both the
original and duplicate values fall below the IDL.
A five-fold-serial dilution of sample, CCN = 938559 (RC-TMW-4L) was performed in accordance with
CLP requirements for ICP analysis. '
The adjusted sample concentrations were outside CLP control limits for sodium, which is flagged with an
"E" on all associated Form I, the Cover Page and Form 9.
An "E" indicates that a chemical or physical interference effect was encountered during the analysis of the
flagged ana\yte. As a result of this interference, all values for the ana\yte in the same matrix must be
considered to be estimated quantities.
CLP control limits for serial dilution are defined as a deviation less than or equal to I 0% in the dilution-
adjusted concentrations from the original values for all analyte concentrations with values greater than fifty
(50) times their respective Instrument Detection Limit (IDL) in the original sample.
This SDG package was processed using the Ward Scientific software. This software package has a seven
character limitation on the Forms 13 and 14 --any sample [D's which exceed seven characters are truncated
. , from left to right on these fonns.
Release of the data contained in this hard copy data package has been authorized by the laboratory
manager or his designee, as verified by the following signature.
J ~<If. aL.
ThomasR.Cole
Chemist II
June 3, 1999
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~~;-i•~~~ij,~~gi:Ai~~;~;J~~i~;~~t~:~~.-,'.~~:C;•:·~-~----··_:· .. -.:;~-----·-· ---.· ·---·-···-
~~~1.~~~;)'.';~!\, . .j:~!~i~E;t ~ .· _;.·:-:.·_<\tt\~f\ -~!~·~ \ ~~~~:: '.' ·:;-~~.: ,{f;·tf;._--: -.. ::~\. ,-.'.·...:::· ·~ .,,,,
••
Com rnChcm
a Division of Liberty Analytical Corp.
501 ,\laJislm ,\\',.;nu,.; Cary. :--.:C :!7513
DATA REPORTING QUALIFIERS FOR INORGANICS
On Form L under lhc Clllumn labeled .. C .. for concentration 4ualiticr :md .. o·· for qualitic-r. c:ich rcsu/1 is !lagged with the specitic
Jaia rcponing qualifi~rs listed below. as :i.ppropri:ue. Up to live: qualitit:rs may be rcportc-d on Form I for each an::!yte.
•. ·----::;1
The C (concentration) qualifiers used are:
U:
B:
This nag indicates the analyte was analyzc-d for but not detected. This reponed value was obtained frcim a reading that
was less than the Instrument Detection Limit (IDL). The IOL will be adjustc-d to reflect any dilution and. for soils, the
percent moisture.
This nag indicates the analytc was analyzed for and the reportcd value was obtained from a reading that was less than the
Contract Required Detection Limit (CRDL} but greater than or equal lo the: Instrument Detection Limit {IDL).
The Q qualifiers used are:
E: This_ flag indicates an estimated value. This !lag is used:
M:
N:
S:
W:
I. When the: serial dilution {a live fold dilution for CLP anJ a live fold dilution for SW-846 method 60108) resullS are
not within I 0%. The :rnalyte concc:nuation must be su!liciently high (minimally a factor of50X above the !DL in
the original sample).
2. \Vhc-n thc analytical spiki:: recovery associated with the sample is below -W¾ after two successive dilutions by
Graphi1e Furnace Atomic Absorption (GFAA) .
This flag applies 10 GFAA analysc-s for concentrations grea1cr than tho: Contract Rcquiri;:d
Detection Limit (CRDL). This tlag is only used for GFAA if the analytical sampk or analytical
spike duplicate injection reading is not within 20% ofthc-Rdativc Standard Deviation (RSD).
This nag indicates the sa.mpk spike recovc-ry is oulSide of control limits:
This !lag is used for dup!icatc-analysis whc-n the sample and the sample duplicate results an! not
within control limits.
This rbg. applies to GFA,\ an:.ilysc-s 10 indicatc-tht: r.:p0nc-d value was dc-termined by th,.;
,\.kthod OfStandarrJ ,\dJitilln (MS.-\).
This tbg applies to GFAA analyses when the post-digestion spike: (analytic:i! spike:) is out of control limits (85% -115%).
whik sampk absorhancc-is kss 1han 50"/o of .. spike" al:lsorbance [ .. spike .. is defined as (absorbance or concenmnion of
spike: sample) minus (absorhancc or concentration of the sample:)[.
+: This !lag. :ipplii::s to GFA,\ analyses whc-n thi:: com.:lation codlicient for the :-.!SA is less than 0.995 after two MSA
ana!yscs.
.'\"OTE: Entering ·s· ··w ... rir ..... i~ mutu:illy c-xc!u~ivc-. S,1 comhin:uion rifthc-sc-qu~liticrs can appear in 1hi:: samc-ficld for an
ana!;>tc-.
The extensions: D, S, M. L.A., a<ltle<l to the en<l of the client ID represent as follows:
[): rn:itri.x duplicate
S ma1ri.x sr,ikc
.\1: m:i1rix spikc Jupli..::it..:
I.: ,;ai:il dilution
,\: pu:il digestion spikc-
.\lrthnJ Cntlts: r,
CV:
C,\:
F:
JCP PLAS:-.tA
:-.1F.RCURY COLO V.-\POR r\.-\
.\IID!-OISTILl.,\TIO~ SPECTROPf IUTO.\ 11iTR!C
Fl;R;-.l,\CF. :\.-\
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B. Sample Data
1. Results .... .-~
--::.·
2. -Quality Control Data
. 3. · Quarterly Verification of Instrument Performance·.
·. 4._ Raw Data
5. Digestion and Distillation Logs
LAB CODE : COMPU
CASE # : 5 '-/3 S {
CONTRACT# : ILM04.0
SDG #: (l)fi6f{(
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1 . Results
Sample results shall be arranged in packets. with the
lnorg_c)J1ic Analysis Data Sheet (Form I -IN) .. These sample ·
packets · shall be placed in increasing Clieht · Sample ID .
number order, considering both letters and numbers, and
shall include all the samples in the SDG.
-· .. '.}
--·-_.
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
Lab
I Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU Case No.: 34336 SAS No.: SDG No. : 00001
Lab Sample ID: 938566
Date Received: 05/14/99
I Matrix ( soil/wat
0
e:J..,,·WATER
Level (low/med): LOW
1% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L __
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1 Color
Color
••
Before:
After:
I Comments:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782~49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 672 -Antimony_ 1.0 u
Arsenic 1.4 u -Barium 112 B
Beryllium 0. 41 B
Cadmium 0.20 u
Calcium 5960
Chromium -2.1 B -Cobalt 9.7 B --Copper __ 0.82 B
Iron 1860 -Lead 2.5 B
Magnesium 2440 B
Manganese 142 -Mercury_ 0.05 u
Nickel 22.0 B
Potassium 1550 B
Selenium 1.6 u -Silver 0.40 u --Sodium 8980
Thallium 2.1 u
Vanadium-0.40 u -Zinc 18.0 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p
p -p -p -p -p
p -p -p -p -p -p -p -p
CV
p -p -p -p -E p ----p -p -p -
-
-
Texture:
Artifacts:
ILM04.0
~t»f
0 ~ C .. · . ••. .< •c/;f •~ •.:C-f~: IC C,~
I u . s . EPA -CLP. !". ,,{!::;~i,;~j~:;f': . , J{1i~
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
Lab
I Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU Case No.: 34336 SAS No.: SDG No.: 00001
Lab Sample ID: 938569
Date Received: 05/14/99
I Matrix ( soil/wat~~l-=.,·WATER
Level (low/med): LOW
I'-Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L __
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1 Color
Color
..
Before:
After:
I Comments:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 1710 -Antimony 1.0 u
Arsenic -1.4 u -Barium 107 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-28000
Chromium -1. 3 B -Cobalt 3.6 B --Copper __ 2.1 B
Iron 7640 -Lead 2.3 B
Magnesium 3700 B
Manganese 45.0 -Mercury_ 0.05 u
Nickel 0.50 u
Potassium 1180 B
Selenium 1. 6 u -Silver 0.40 u --Sodium 10300 -Thallium 2.1 u
Vanadium-4.1 B -Zinc 21.0 -
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -E p ---p -p -p -
-
-
Texture:
Artifacts:
ILM04.0 (}~{ 1oj
. -· . -· .'~--. . --·· _::: ____ -~---:.::~~:-~l~:~~:~ii
, " :~f;j,:,= · '-t~·~/''· : . · ~·gL~t~
U.S. EPA -CLP
1
_;S[if
EPA SAMPLE NO. · 'it(t I
I INORGANIC ANALYSES DATA SHEET
Contract: ILM04.0
[
Lab Name: COMPUCHEM
ab Code: COMPU_ Case No.: 34336 SAS No.: SDG No. : 00001
ratrix ( soil/wat
0
e~}.-:-·WATER
Level (low/med) LOW
1% Solids: 0.0
Lab Sample ID: 938568
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight) UG/L __
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I Color Before:
Color After:
I Comments:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782~49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 25.2 B
Antimony_ 1.0 u
Arsenic 1.4 u -Barium 63.4 B
Beryllium 0.10 u
Cadmium 0.54 B
Calcium-106000
Chromium -0.51 B -Cobalt 1. 2 B
Copper __ 0.67 B
Iron 9820 -Lead 1. 4 B
Magnesium 3170 B
Manganese 123 -Mercury_ 0.24 -Nickel 0.50 u
Potassium 1790 B
Selenium 1. 6 u -Silver 0.40 u
Sodium--18000 -Thallium 2.6 B
Vanadium-0.87 B -Zinc 32.2 -
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p --
-
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ILM04.0
: ;',:'~· -,,·;;~~~
U / ;•;: > -. CL:'' ' :i,>f ''"''":f !:::·~,
I INORGANIC ANALYSES DATA SHEET ________ -;,,:-,
-RC~RBL-1
Contract: ILM04.0 I Lab Name:. COMPUCHEM
Lab Code: COMPU_ Case No.: 34336 SAS No.: SDG No.: 00001
I Matrix ( soil/wat~~)-_.-WATER
Level (low/med) LOW
1% Solids: 0.0
Lab Sample ID: 938563
Date Received: 05/14/99
Concentration Units (ug/L or mg/kg dry weight): UG/L __
I
I
I
I .,
I
I
I
I
I
I Color Before:
Color After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 8.9 u
Antimony_ 1.0 u
Arsenic 1.4 u -Barium 0.10 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-8.5 u
Chromium 0.52 B -Cobalt 1.6 B --Copper __ 0.83 B
Iron 13.3 B
Lead 1.3 B
Magnesium 7.9 B
Manganese 0.12 B
Mercury_ 0.05 u
Nickel 0.50 u
Potassium 11.1 u
Selenium 1. 6 u -Silver 0.40 u
Sodium--425 B
Thallium 2.1 u
Vanadium 0.40 u -Zinc 5.1 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
Q M
p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ---p
p -p -
-
-
Texture:
Artifacts:
FORM I -IN ILM04.0
I
I
1 Lab Name : COM PU CHEM
Lab Code: COMPU
U.S. EPA ~-CLP
1
INORGANIC ANALYSES DATA SHEET
Contract: ILM04.0
Case No.: 34336 SAS No.:
. . .. -------·---·---··-· ------:.,•,· .. ___ •:.;.;..~ . -~ .... ".--,~ ·:·
'EPA SAMPLE NO.
RC-TMW-1
SDG No. : 00001
I Matrix ( soil/wat
0
e~.:-•·WATER
Level (low/med) LOW_
Lab Sample ID: 938565
Date Received: 05/14/99
1% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I ••
I
I
I
I
I
I Color Before:
Color After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 622 -Antimony_ 1.0 u
Arsenic 1. 4 u -Barium 112 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-5980
Chromium -2.5 B -Cobalt 10.8 B --Copper __ 2.9 B
Iron 1870 -Lead 2.0 B
Magnesium 2440 B
Manganese 144 -Mercury_ 0.05 u
Nickel 21.2 B
Potassium 1580 B
Selenium 1. 6 u
Silver 0. 40 u
Sodium--9320 -Thallium 2.8 B
Vanadium-0.96 B -Zinc 18.3 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p ---
Texture:
Artifacts:
ILM04.0
c,,{6 13 J
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RC~TMW-10
Contract: ILM04.0
1 Lab Name: COMPUCHEM
Lab Code: COMPU_ Case No.: 34336 SAS No.: SDG No.: 00001
I Matrix (soil/wat~~,_:.,·WATER
Level (low/med): LOW
I,. Solids: 0.0
Lab Sample ID: 938648
Date Received: 05/15/99
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I ••
I
I
I
I
I
I Color Before:
Color After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-2B-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 348
Antimony= -1.0 u
Arsenic 1.4 u -Barium 73.1 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-3210 B
Chromium 0.82 B -Cobalt 5.7 B
Copper __ 1. 9 B
Iron 3170 -Lead 2.2 B
Magnesium 1290 B
Manganese 89.l -Mercury_ 0.05 u
Nickel 9.6 B
Potassium 1970 B
Selenium 1.6 u -Silver 0.40 u
Sodium--9550 -Thallium 2.1 u
Vanadium-0.71 B -Zinc 14.5 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p ---
Texture:
Artifacts:
ILM04.0
I
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
EPA SAMPLE NO.
RC-TMW-2
.-,ab
lr.,ab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU Case No. : 34336 SAS No. : SDG No. : 00001
Lab Sample ID: 938564
Date Received: 05/14/99
ratrix ( soil/wat::;J-WATER
Level (low/med) LOW .. Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L __
I
I
I
I
I
I
I
I
I
I.Color
Color
·•
Before:
After:
I comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
743°9-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 202
Antimony= -1.0 u
Arsenic 1.4 u -Barium 38.7 B
Beryllium 0.13 B
Cadmium 0.20 u
Calcium-33400
Chromium -0.76 B -Cobalt 1.7 B --Copper __ 0.30 u
Iron 3680 -Lead 2.2 B
Magnesium 7000 -Manganese 103 -Mercury_ 0.05 u
Nickel 0.50 u
Potassium 948 B
Selenium 1.6 u -Silver 0.40 u
Sodium--10800 -Thallium 2.1 u
Vanadium 0.92 B -Zinc 4.7 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -E p ----p -p -p --
-
Texture:
Artifacts:
ILM04.0
U.S. EPA -CLP
1
.. -• . ... :,~,i-:·"' ·-.r)~f~t;\i:r~;·?.=-t~,;_,7:~ ....
EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RC-TMW-3
Contract: ILM04.0 .Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336 SAS No.: SDG No.: 00001
.Matrix (soil/wat~1;,;_,,WATER
Level (low/med): LOW
1% Solids: 0.0
Lab Sample ID: 938567
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I
I
I
I
I
I Color
Color
••
Before:
After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
BROWN
Analyte Concentration C Q
-Aluminum 14000 -Antimony 1.0 u
Arsenic -2.2 B -Barium 105 B
Beryllium 0.54 B
Cadmium 3.1 B
Calcium-247000
Chromium -18.1 --Cobalt 11.3 B
Copper __ 14.0 B
Iron 6510 -Lead 18.4 -Magnesium 6770 -Manganese 181 -Mercury_ 0.13 B
Nickel 15.8 B
Potassium 2760 B
Selenium 1.6 u -Silver 0. 40 u --Sodium 6300 E ----Thallium 2.5 B
Vanadium-27.6 B -Zinc 57.5 -
-
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -p -p -p -p -
-
-
Texture:
Artifacts:
ILM04.0
U.S. EPA -CLP
1 EPA··sAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
Contract: ILM04.0 rab Name: COMPUCHEM
'1,ab Code : COMPU · Case No.: 34336 SAS No.: SDG No.: 00001
t atrix (soil/water) ,_,WATER
,_&· ... ·...:--
Level (low/med) LOW
1% Solids: 0.0
Lab Sample ID: 938559
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I
I
I
I
I
.Color
Color
·•
Before:
After:
I comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 96.5 B
Antimony_ 1.0 u
Arsenic 1. 4 u -Barium 59.8 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-19900
Chromium -0.50 u -Cobalt 1.7 B --Copper __ 1. 2 B
Iron 1800 -Lead 2.4 B
Magnesium 716 B
Manganese 21. 7 -Mercury_ 0.05 u
Nickel 0.50 u
Potassium 927 B
Selenium 1.6 u -Silver 0.40 u
Sodium--6110 -Thallium 2.1 u
Vanadium-1.1 B -Zinc 0.40 u
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p -
-
-
Texture:
Artifacts:
I
Duplicate_(RC-TMW-4D) ___________________________ _
I FORM I -IN ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RC-TMW-5
•
Lab
Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU. Case No.: 34336 SAS No.: SDG No.: 00001
Lab Sample ID: 938638
Date Received: 05/15/99 •
Matrix (soil/water) ;/WATER
... "-""' -.:::,·
Level (low/med) LOW
1% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I
I
I
I
I
I
I Color
'Color
••
Before:
After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 638 -Antimony 1.0 u
Arsenic -1.4 u -Barium 43.4 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-5630
Chromium -0.99 B -Cobalt 3.9 B
Copper __ 0.30 u
Iron 11200 -Lead 1.7 B
Magnesium 1610 B
Manganese 79.5 -Mercury_ 0.15 B
Nickel 5.4 B
Potassium 1010 B
Selenium 1.6 u -Silver 0.40 u
Sodium--8980 -Thallium 4.8 B
Vanadium-1.6 B -Zinc 4.6 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p -
--
Texture:
Artifacts:
ILM04.0
1 EPA SAMPLE
I INORGANIC ANALYSES DATA SHEET
Lab
ILab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code : COMPU · Case No.: 34336 SAS No.: SDG No.: 00001
Lab Sample ID: 938647
Date Received: 05/15/99
.Matrix ( soil/wa_t~r;)"WATER
Level (low/med): LOW ... Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L __
I
I
I
I
I
I
I
I
I
1 Color
Color
••
Before:
After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782~49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
BROWN
Analyte Concentration C Q
-Aluminum 15100
Antimony_ 1.0 u
Arsenic 1.6 B -Barium 87.1 B
Beryllium 0.13 B
Cadmium 0.20 u
Calcium-6140
Chromium -10.8 --Cobalt 5.0 B --Copper __ 5.2 B
Iron 4760 -Lead 11.4 -Magnesium 1720 B
Manganese 90.7 -Mercury_ 0.08 B
Nickel 10.9 B
Potassium 1480 B
Selenium 1.6 u -Silver 0.40 u
Sodium--11400 E ----Thallium 2.1 u
Vanadium-9.9 B -Zinc 16.5 B
-
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
M
-p -p -p
p -p -p
p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p
p -
-
-
Texture:
Artifacts:
ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO.
I
I INORGANIC ANALYSES DATA SHEET
RC-TMW-7
Contract: ILM04.0 1 Lab Name: COMPUCHEM
Lab Code: COMPU· Case No.: 34336 SAS No.: SDG No.: 00001
I Matrix ( soil/w~~;:J .. =.-··WATER
Level (low/med) LOW_
I% Solids: 0.0
Lab Sample ID: 938639
Date Received: 05/15/99
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I Color
Color
Before:
After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 229 -Antimony_ 1.0 u
Arsenic 1.4 u -Barium 70.0 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-4440 B
Chromium 0.50 u -Cobalt 4.9 B --Copper __ 0.83 B
Iron 3810 -Lead 2.9 B
Magnesium 1510 B
Manganese 93.5 -Mercury_ 0.05 u
Nickel 6.9 B
Potassium 1190 B
Selenium 1.6 u -Silver 0.40 u --Sodium 6260 -Thallium 2.1 u
Vanadium-0.40 u -Zinc 6.4 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -E p ----p
p -p -
-
-
Texture:
Artifacts:
ILM04.0
G "'{ 2 0«1
u.s.· EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RC-TMW-7A
Lab
I Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU· Case No.: 34336 SAS No.: SDG No.: 00001
Lab Sample ID: 938646
Date Received: 05/15/99
I Matrix (soil/w~t;.~.:/WATER
Level (low/med): LOW_
1% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I •
I
I
I
I
I
I Color Before:
Color After:
I Comments:
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 238 -Antimony_ 1.0 u
Arsenic 1.4 u -Barium 67.8 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-4400 B
Chromium 0.74 B -Cobalt 5.3 B
Copper __ 0.37 B
Iron 3960 -Lead 1. 7 B
Magnesium 1510 B
Manganese 92.2 -Mercury_ 0.05 u
Nickel 7.9 B
Potassium 1200 B
Selenium 1.6 u -Silver 0.40 u --Sodium 6410 -Thallium 2.1 u
Vanadium-0.49 B -Zinc 7.4 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p
E p ----p -p -p -
-
-
Texture:
Artifacts:
ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
-· RC-TMW-8 I Lab Name: COMPUCHEM ________ _ Contract: ILM04.0
Lab Code: COMPU_ Case No.: 34336 SAS No.: SDG No. : 00001
Lab Sample ID: 938650
Date Received: 05/15/99
IMatrix (soil/wat~~i.,:WATER
Level (low/med) LOW
I% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight) UG/L __
I
I
I
I
I
I
I
I
·•
I Color Before:
I
I
I
Color After:
Comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 20600
Antimony_ 1.0 u
Arsenic 3.0 B -Barium 108 B
Beryllium 4.6 B
Cadmium 0.20 u
Calcium-47900
Chromium -2.0 B
Cobalt 41. 2 B --Copper __ 1.5 B
Iron 51600 -Lead 1. 2 B
Magnesium 12400 -Manganese 532 -Mercury_ 0.05 u
Nickel 36.9 B
Potassium 3420 B
Selenium 1. 6 u -Silver 0.40 u
Sodium--26200
Thallium -8.4 B
Vanadium-12.7 B
Zinc 156 -
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I ~ IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p
p -p ---
Texture:
Artifacts:
ILM04.0
U.S. EPA -CLP
1
I INORGANIC ANALYSES DATA SHEET
RC-TMW-9
Lab I Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU· Case No.: 34336 SAS No.: SDG No.: 00001
Lab Sample ID: 938651
Date Received: 05/15/99 I Matrix (soil/water) _:,,·WATER
,.& . --
Level (low/med): LOW ... Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight) UG/L __
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1 Color
Color
•
Before:
After:
I Comments:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
COLORLESS
COLORLESS
Analyte Concentration C
-Aluminum 299
Antimony 1.0 u
Arsenic -2.7 B -Barium 63.2 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium-5440
Chromium -1.1 B -Cobalt 6.5 B --Copper __ 1. 6 B
Iron . 1400 -Lead 1.8 B
Magnesium 1470 B
Manganese 68.5 -Mercury_ 0.05 u
Nickel 7.3 B
Potassium 1170 B
Selenium 1. 6 u -Silver 0.40 u
Sodium--10700 -Thallium 2.1 u
Vanadium-1. 2 B -Zinc 11. 5 B
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
p -p -p -p -p -p
p -p -p -p -p -p -p -p
CV
p -p -p -p
E p ----p -p -p -
-
-
Texture:
Artifacts:
ILM04.0
0f ,,.{£ 2 3~
U.S. EPA -CLP
1 EPA SAMPLE NO.
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I INORGANIC ANALYSES DATA SHEET
TAR-POND3
1 Lab
Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU Case No.: 34336 SAS No.: SDG No. : 00001
Lab Sample ID: 938649
Date Received: 05/15/99
I Matrix (soil/wa~~~-'/WATER
Level (low/med): LOW
1% Solids: 0.0
I
Concentration Units (ug/L or mg/kg dry weight): UG/L __
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I Color Before:
Color After:
I Comments:
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11
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
BROWN
Analyte Concentration C
-Aluminum 5140
Antimony--1.0 u
Arsenic -1.4 u -Barium 43.9 B
Beryllium 0.10 u
Cadmium 0.20 u
Calcium 9280
Chromium -7.1 B -Cobalt 4.2 B
Copper __ 692 -Iron 15100 -Lead 35.9 -Magnesium 1810 B
Manganese 88.7 -Mercury_ 0.05 u
Nickel 6.3 B
Potassium 1210 B
Selenium 1.6 u -Silver 0.43 B
Sodium--15800 -Thallium 2.1 u -Vanadium 27.6 B -Zinc 209 -
-
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -E p ----p -p -p ---
Texture:
Artifacts:
ILM04.0
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COMPUCHEM
a division of Liberty Analytical Corp.
04/JUN/99
Roy F. Wes-con
5405 Metric Pl.
Suite 200
Norcross, GA 30092
\ \
Subject: Report of Data -Account Number# 501223 Order# 34336
Ht\::-Enclosed .are the results of analytical work performed in accordance
~ .. ,., .. · . . .
,::'•?/i:with the ,referenced account number.
,(._t~t:/:}} . .
._This· report covers 11 sample ( s) appearing on the attached 1 isting.
Thank you for selecting CompuChem Environmental for your sample
a~alysis. If you should have questions or require additional
analytical services please contact your representative at
1-800-833-5097.
Sincerely,
ClwLS:~
CompuChem Environmental
a division of Liberty Analytical
Attachment
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: [phone]
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COMPUCHEM
a division of Liberty Analytical Corp.
04/JUN/99
Roy F. · Weston
5405 Metric Pl.
suite 200
Norcross, GA 30092
ACCOUNT#: 501223
CC# SAMPLE-ID
'
: 9385'70 RCSV0l
938577 RCSV02
938578 RCSS03
9~8579 RCSS0l
938580 RCSV03
938581 RCSE02POND2
938582 RCSE0lPONDl
938583 RCSE04POND4
938584 RCSE03POND3
938585 RCSS02
938766 DRUMDISPOS
TOTAL NUNBER OF SAMPLES
RECEIPT DATE
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/15/99
= 11
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: [phone]
,·:-:>. ,.: ,:.;~
. ;~~--~~}~:
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The sample data summary package shall contain data for all samples
·in one Sample Delivery Group (SDG) of the Case, as follows:
A. SDG Narrative
B. Tabulated target compound results (Form I) ._0 -:::::_
Tentatively identified compounds (Form I, TIC) 0/0A & SV only)
In order by fraction (VOA, SV, PEST) and by sample
within each fraction. ·
C. System monitoring compound results (Form II -VOA only)
Surrogate spike analysis results (Form II -SV & PEST only) ·
By fraction (VOA, SV, PEST), matrix (Water or Soil),
and by concentration (Low or Medium)
D. Matrix Spike/ Matrix Spike Duplicate results (Form III) ·
By fraction (VOA, SV, PEST)
E. Blank data (Form IV)
Tabulated blank results (Form I)
Tentatively identified compounds (Form I, TIC)
By fraction (VOA, SV, PEST)
F. Internal standard area response and retention time data (Form VIII)
By fraction (VOA & SV only)
LAB CODE • COMPU CONTRACT# : OLM03-REVS
CASE # • 3.I/.J3{fl
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A. SDG Narrative
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-:.:.-·:_-·-. ·':.:. .·<.:: -
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A division of Liberty Analytical Corporation
501 Madison Ave.
Cary.NC 27513
SDG NARRATIVE
CASE #34336
SDG #00002
CONTRACT #OLM03-REVS
SAMPLES: RCSV0I, RCSV02
The two (2) soil samples listed above were received intact, properly refrigerated, with proper
documentation, in a sealed shippingcontainer;on May 14, 1999. The samples were scheduled for
the requested analyses of the semivolatile fractions. These samples were analyzed following the
current EPA Contract for the Laboratory Program, Document number OLM03.2.
All pertinent Quality Assurance notices are included in the narrative section and all pertinent
Laboratory notices for Case #34336, SDG #00002 are included in the sample data sections.
SEMIVOLA TILE
The semivolatile fractions were initially extracted and analyzed within the required holding time.
Due to an error during the extraction procedure, a repeat extraction of the sample was required.
The repeat extraction, however, was performed outside of the required holding time. Only the
data from the repeat extraction of sample RCSV0 I is reported.
The percent moisture values for the samples were 19% and 14% and the pH values were 3.9 and
5.2 respectively.
No Target Compound List (TCL) analytes were detected with concentrations above the Contract
Required Quantitation Limit (CRQL) in the samples.
Six and twenty-four Tentatively Identified Compounds (TIC) were detected in the samples.
These TICs were assessed as unknowns, carboxylic acids and phthalates. Other TICs were
detected and assessed as unknown alkanes in some of the samples. The TICs that were
characterized as alkanes have been summarized on the Form I FAs that are located in the
narrative section of the data package. The TIC spectra for the alkanes are located in the data
section for the individual samples.
QC SUMMARY
The surrogates met recovery criteria for the semivolatile fractions. The internal standards met
area response and retention time criteria.
The duplicate matrix spikes met accuracy criteria, with some exceptions. The recovery of 2,4-
dinitrotoluene failed acceptance criteria in the MS and the recoveries of n-nitroso-di-n-
propylamine, 1,2,4-trichlorobenzene and pyrene failed acceptance criteria in the MSD. Although
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COMPUCHEM 34336.00002
A division of Liberty Analytical Corporation
a majority of the spike compounds met accuracy criteria, they did not compare well between the
duplicate matrix spikes, resulting in failing relative percent difference values for all of the spike
compounds.
The associated.--61anks. Initial Calibrations and Continuing Calibrations met Quality Control
criteria·. · ~--d-" ·
In the analyses of the Initial and Continuing Calibration standards and sample RCS VO I, manual
quantitations were performed. The reasons have been coded with explanations provided in the
notice included in the narrative section of the SDG.
I certify that this data package is in compliance with the terrns and conditions of the contract,
both technically and for completeness, for other than the conditions detailed above. Release of
the data contained in this hardcopy data package and in the computer-readable data submined on
diskene has been authorized by the laboratory manager or his designee, as verified by the
following signature:
Patricia B. Hopkins
Final Technical Review
3 June 1999
Note: This report is paginated for reference and accountability in numerical sequence.
. ------.... -----· .. _-{,\;f
I Client Sample ID: RCSV0l
Compound
.ALKANE NARRATIVE REPORT
Report date : 06/03/1999
SDG: 00002
\
·i·-s:<·;i . .-~.· -~.:,, .,, ·,,:i_;s:
.. -....
. '·:·_~;
Lab Sample ID: 938570 File ID: G3R38570B66
RT Est. Cone. Q I ------------------------------------------------------~----------;--
J Unknown Alkane
Unknown Alkane
20.76
22.46
177.9
158.6
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CompuChem. a Division of Liberty /\nalytical Corporation
GC and GC/MS Column and Trap Specifications Table
COLUMNS
Brand Name -,-.• Coating ID Film Thickness Length .. ~--Material (mm) (um) (m)
GC Laboratory
Restek RTX-1701 0.53 0.5 30
J&W DB-608 0.53 0.83 30
Restek CLPesticides 0.53 0.5 30
Restek CLPesticides II 0.53 0.42 30
GC Volatiles Laboratory
Restek RTX-1 0.53 0.5 105
Restek RTX-502.2 0.53 0.5 105
G<;/MS Volatiles Laboratory
J&W DB-624 0.53 3.0 30/75
Supelco EquityT"'-624 0.53 3.0 75
GC/MS Semivolatiles Laboratory
J&W DB-5.625 0.32 1.0 30
J &W DBS-MS 0.25 0.25 30
Hewlett Packard HPS-MS 0.25 0.25 30
TRAP
GC/MS Volatiles Laboratory
• 1 cm of methyl silicone packing (OV-1 coating)
• 8 cm of 2,6-diphenylene oxide polymer (Tenax)
* 8 cm of silica gel
* 7 cm of coconut charcoal
* 0.5 cm of silanized glass wool at each end
Rev. 6 5/10/99
'I"::·~-__ .. ,,,, ... :? .
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-~~.
CompuChem
a di\'ision of Liberty Ana lyrical Corporation
Notification Regarding Manual Editing/Integration Flags
In some inscances.,-'manu.a! adjustments co the sothvare ourput Jie necc!'ssa.ry ro provide accurate Cara. These: adjusrment_s are-pe'rformed by 1he data reviewer. GCiMS operawr. or GC chemise. An E:~rracted Ion Current Profile (EICP) .or a GC chroma1ographic peak has been provided for the manual imegra1ion of each compound <o demonstrate the accuracy of thar process. Adjustments are flagged on the quantication repon in the far right column beyond <he FfNAL concen<racion for GC/MS analysis. and in che "Flags" column for GC analysis. The manual editing/integration flags are:
M -Denotes that a manual integration has been performed for this compound. The manual integration was performed in order to provide the most accura1e area count as possible for the peak.
H . Denotes rhat the data reviewer, GCIMS operator. or GC Chemist has chosen an alternate peak within the retention time window from that· chosen by the software for !hat compound. No manual integration is performed in choosing an alternate peak. The software still performs the integration.
MH. • Denotes that an alternate peak has been chosen within the retention time v,:indow from that chosen by th~ softv..-are for that compound and also a manual integration of the chosen peak has been performed. The manual integration was performed in order 10 provide the most accurate area counr possible for rhe peak •• L • Denotes that the data revi_e\"·er or GC'MS operator has selected an alternate library search. This 1s typically done when an additional tenta1ively idenrified compound (TIC) has been added to the number of peaks searched. No manual integration is performed in choosing an alternate peak. The sofrware still performs the integration.
,\-1L • Denotes 1ha1 an alternate library search has been <=Plected and J manual integration has also been performed. This is typically done when an addi:: .,al TIC has been added and <he TIC peak also required a manual integration.
Wi<h ,he in<roduc,ion or <he curren< EPA CLP SOW (Documen< Number OLM03.0. plus revisions) addicion,,'. explanations for manual editing/integration are required. In the accompanying raw data packages. additional codes have been applied to the"~-['-r.ag and carry the following meanings:
:\-11 • The compound was not found by [he automa[ic integration routine.
M2 • The compound was incorrectly integrated by the automatic integration routine.
,u • The co•eluting compounds were incorrectly integrated by the automatic integration routine.
Thtse codes will appear in the GC'MS and GC dat.:i. packages.
Robert E. Meierer
Vice President
Revision 4 (10/8/97)
P!'~~t.: •c;~ ,_c·.··.·····. · ..
CompuChem
;1 \.ti, i:-ilnl 11!' l .ibcn~ .\11.11~ ri..:.1! C\1rpl1r:Hil111 .._, ~
~.;;.-~
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DATA REPORTING QUALIFIERS
On tilt.' FLlnll I. under chc: column !;1/:ldt:d ··() .. fvr qua!itia. t.::1ch rc:su~t is tlagg1..:d with [lit: spt..'citic d:1t:1
rt:porring qualifiers lisrc:d bdow. as appropriat1..·. l.!p {L) ti\·c qualifi1.:rs 111ay bt.· rL'pL1rtc:d llll fnnn I f,Jr each
.,,;ompounJ. The: qualifiers used are: ,
U : · This flag indicates 1he compound \\·as analyzed for but nor dc:tccted. The Contract Required
J :
••
r:
C:
Quantitation Limit (CRQL) (or Reporting Limit\ will be adjusted to retlect any dilution and for
soils, the percent moisture.
This flag indicates an estimated value.' The flag is used as detailed below:
I. When estimating a concentration for tentatively identified compounds (TICs) where a
response factor of 1.0 is assumed foi the TIC analyte.
\Vhen the mass spectral .:ind retention tirn-:: datJ indicate the presence: of a compound that
rneecs the volatile and semi\'l)latile GC/MS idemitication criteria and the result is lt:ss th.111
tht: CRQL (or Reporting Limit) hul gre.1tt:r 111:111 zi.:ro.
_,. \Vhen the rL'lt.'lltion time Ja1;i inJic:llt.'s cl1t.: prt:sc:nct: 1Jt" a l.'.lHllp(llJ11d that JIIL't:rs tilt.·
pesticiJL'.".-\roclnr or lHht:r CC ()J" HPl.l. idt:11tillcnio11 i..:riteria and tliL" result is kss than tht.·
CRQL (,>r Reporting Li111it) hut greater titan ;:cro. For e.,ample. it· the CRQL (or Reporting
Limit) is ! 0 ug./L but a cunct:n!ration of J ug:/L is calculated. it is reported as 3J.
This flag inc.Jicatt:s presumptivt: e\·iJi.:nce of a 1.'.0lll 1)lHinJ. This flag is unly used for Tl Cs. where
tht: iJt:r11ilic~1tio11 is based \)11 a mas:,; spectral libra:-~· search. For generic characterization ofa TIC
'>ul.'.ll ,:b ·i..:!Jll)rinated hydroc:1rh()11 . tilt.·:--,: flag is 11nt used.
!11 the EP.-\·s Contract Laboratory Progr.1111 (CL,·1. this flag is used for a pesticide/Aroclor target
:rnalyte. \\.htn there is gn:ata than 25°/o difference for detected concentrations between the twu
GC columns. The lower 01· the two values is reported on Form I and nagged with a P.
For S\li-8.J6 GC and HPLC analyses. when the Relative Percent Difference (RPD) is greater than
-lQ~/o and th.:rt: is no evidence of chromatographic anomalies or interferences. then the higher of
tlte two values is reported and tlagged with a P. When the RPD is equal to or less than 40%. our
policv is tu also report the hi~her of the two values. although the choice could be a project
specitic issue.
This !lag applies\() GC lH HPLC ri.:~ults where: the iJ-.:111iiication has been confirmed by GC/MS.
lfGC.-'\1S l.'.l)ntlrm;Hion ,,·as atternpto:.:d hut was uns111:cessfu1. this lbg is not applied: J laboratory-
JdlneJ !lag is ust..:d instt::..iU (st.·i.: the .\_.-y:z quali!icr).
·~~:f'
;_-.;;
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fl:
[:
D:
DATA REP.ORTING.:QlJALIFIERS {C,HHlllllCdl
Tl ii-; lb~ is u:-1..:d \dJL'll rl1c :111a1:,:ce i:-fnu11d in th1.· ;1:iSl1i..:iatl..'d b!:ink a:-\\ ..:II as in tilt.• s:11nph.:. ![
im!ii.::uc~ pn\b;ihk blank cunt.:rn1i11atiL111 anJ w:'1rn_..; the;> <bt:1 u:-1..•r fll ral,;..: appwpri,:ue .'.lcrio11. Thi:-
tla!.! j:; t1...;cd l°llr :i TIC a:,; well as t~1r a po:-iti\·dy idt.'11titit.'U targt.'t L"n111puu11d. The comhinatil111 of
tl.t~S 8L: llr L;I3 i:-mH an a!ILH,·ablc.· pl1lii..:y. Blank 1:urHar11i11ant:-.~11\: flagged B 0111; ,,·/Jt.'11 1/Jt:, art.'
dt.'t~cred i11 th1..· :-:11npk·.
This 11;·!.! iJi.:ntific's cornpoutH.ls whnst.' L'LlllCt:1Hrat1L1ns t:'.\Cec:d tlic:-uppt:r k•vd Llf the calibration
rJ.n~e ot7 the instrument for that specific analysis. It· u;ie or more compounds have:-a response
gre;ter than the upper level of the: calibration rangc. !ht: sarnp!t: or L'Xtracr will be diluted and
reanalyzed. All such compounds with a rt!sponse grearer than the upper level of the calibr.ition
range will have the concentration tlaggcd with an E nn Form l for thi:: original analysis.
If a sample or extract 1s reanalyzed at a higher dilution foe tor. for exam pk when the
concentra!ion of an analyte exceeds the upper calibration range. the DL suffix is appended to the
;ample number on Form I for the more diluted sample and all reponed concentrations 011 that
Form I :-ire flngged with the D tlag. This flag alerts data use-rs that any discrepancies between the
reported concentrations may be due to dilution ot·rhe sample or i::xtrnct.
N()°f-f I: The D tlag. is nor applied to cnmpounds which an.: not dc1t:cted in the sample ana!~·sis 1.c.
cdmplHllld:-rt:pvrred \\·i1h tht: CR()L for Reporting Limit) and tilt: lj th-1g . .. :'\OT!: .... Scµ:ir:H,: hir111 !."> an: uscJ for rt:r111·ting tilt:' nri~i11~11 analysis (Clit:"rlt Sample :---;l). XXXXX) and
.. \
the 11H1rt: di!u1i..:d .">ampk analysi::-(Client Sa111plL· ~l). XX.'<X.\DL) i.e. the results frvm bo(li
:111:i!; "i...::-i :1n.: 111.11 (llmhined 011 a :-.in'.:,'.lt: Flmll I
I hi-. lb~ i11dicllt.'"> cl1a1 :rn a11a!ytt: \\:IS d.:tt:L:!t.·U b~ a ..;in~lt.· L:l)lu11111 (IC ~111..ilysi::-hut the r.::..;ult \\:lS
bt:111\, thi..· l{t:ihlrli11~ Limit. This tbg i..; 1)nly u..;i...:d "hen dicnrs n:qth::-t a s.:comJ (i.:011tin11;1tiL)ll)
,.,;11lu111n :111.il>·"'i"' ;1f1cr Lk·11.:c1i11g an ;111~11:ti..: ah1n·i.,; thi..: Rt:pllrlin~ l.i111i1 in the initial. singk cnlu11111
.,11:d: .... i... I Iii ... tbg alats tht: data ust:r tlwt l)nl; an :111:11:tc \\:IS dt.·ti..:cci::d ht:lo,\ the Rq10ning
\.1111it :111d :1 ... 1..·..:,,nJ (ClllJtir111atilHl) analysi:-\\as 111)! pt:rfomlt.'LL
:,;,y /: I l1hcr ,r,·cilic !lags ma, he required to properly ddir.e 1he results. If used. the flags will be fully
~kscrihi...:d 111 tht: SDG ~arrative. Tlit.: laboratory•Lidined tlags are limited to X.Y and Z.
Rc,·isi\111 -l (8-19-98)
. ,.,_ ...... _, • ·:t••,
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Compu.Chem
a division of Liberty Analytical Corporation
CompuChem's Pagination Convention
As required by the current EPA CLP Statement of Work (SOW) (Document Number OLM03.0,
plus revisions), data to be delivered must be paginated (by machine or hand). In the event that the
initial numbering is incorrect (a page numbered twice or a page skipped, for example). it is
CornpuChem's policy to add in an alphabetic suffix to a page number when necessary (e.g.,
I OOA. I 00B. etc.). ..
Form DC-2 presents an inventory of the contents of the CSF, including the page number
locations for the indexed items. There are concurrent delivery requirements for the Sample Data
Packages and the CSF. Because of this and the time required for the final 1echnical review
process. we have instituted a policy to expedite assembly of the CSF. Items 2-6 on the Organic
Forni DC-2 and items 2-26 on the Inorganic Forro DC-2 contain those items which are pan of the
Sample Data Packages. Those items will be paginated in ascending order. However. while
Sample Data Packages receive a final technical review, items 7-10 on the Organic Forro DC-2
and items 27-32 on the Inorganic Forro DC-2 will be assembled and paginated. The fir3t page
number for the first entry for item 7 on the Organic Forro DC-2 and for item 27 on the Inorganic
Forni DC-2 will always begin with page number 10,000.
Revision 3 ( I 0/8/97)
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Quality Assurance Notice
The EPA CLP SOW (Document Number OLM03.0. plus revisions) requires. for tentatively
identified compound (TIC) assessment, that certain items should not be reported. These include.
for volatile organics, carbon dioxide 3.!)d semivolatile TCL analytes and. for semivolatile
organics, volatile organics listed in Exhibit C.
In order to assist the data review/validation process by our clients. if we detect carbon dioxide or
semi volatile TCL analytes at or above I 0% of the closest internal standard we will report them
on the Form I VOA-TIC but not include them as part of the thirty (30) Tl Cs required. Similarly.
if we-detect volatile TCL analytes from Exhibit C at or above I 0% of the closest internal
standard during the TIC assessment of the semi volatile analysis. we will report them on the Fom1
I_,SV-TIC but not include them as part of the thirtv (30) TICs required. The library search raw
data for these TICs are also included. The total number of TICs listed on the Form I in the
Number of Tl Cs field will include these items.
We feel this approach will aid the data review/validation process by our clients. since we will be
accounting for all peaks required to be searched as well as any other comparably sized peaks
present on the reconstructed ion chromatogram (RIC).
Robert E. Meierer
Vice President
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Organic Analysis Data Sheet (OADS) and
T~p!,atively Identified Compounds (TICs)
..: All samples by fraction (VOA, SV, PEST).
-alphanumeric order within each fraction·
.,._,.
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Contract: OLM03-REVS ~~v&~:::J
SAS No.: SDG No.: 00002
Lab Sample ID: 938570
Lab _File ID: G3R38570B66
I Level: (low/med)···' LOW .. -'· ~=-
% Moisture: ·19 decanted: (Y/N) N
500 (uL)
Date Received: 05/14/99
Date Extracted:05/28/99
Date Analyzed: 06/02/99
Dilution Factor: 1.0 I Injection Volume:
Concentrated Extract Volume:
2. 0 (uL) I GPC Cleanup: (Y/N) Y pH: 3.9
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CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--~-----Phenol
111~44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
1~6-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1--~------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-NitrophenoT
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naohthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7------~--4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaohthalene
--
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Contract: OLM03-REVS Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: ( soil/water) SOIL
SAS No.: SDG No.: 00002
Lab Sample ID: 938570
Sample wt/vol: 30.0 (g/mL) G Lab File ID: G3R38570B66
Level: (low/med),,,
_;.~·
," LOW Date Received: 05/14/99
.. • Moisture: ·19 · decanted: (Y/N) N Date Extracted:05/28/99
Concentrated Extract Volume: 500(uL) Date Analyzed: 06/02/99
Injection Volume: 2.0(uL) Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 3.9
CAS NO. COMPOUND
5~-28-5--0 ------2,4-Dinitrophenol
100:02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
121-14-2--------2,4-Dinitrotoluene
~4-66-2---------Diethylphthalate
· 005-72-3-------4-Chlorophenyl-phenyletner
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenyletner -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(ll -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
1000 u
1000 u
410 u
410 u
410 u
410 u
410 u
1000 u
1000 u
410 u
410 u
410 u
1000 u
63 J
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410 u
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44 J
66 J
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380 JB
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lF EPA SAMPLE NO. i/fj§_
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM I Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) SOIL
RCSV0l
Contract: OLM03-REVS
SAS'No.: SDG No. : 00002
Lab Sample ID: 938570
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Sample wt/vol: 30.0 (g/mL) G Lab File ID: G3R38570B66
Level: ( low /TTl_e_<V-·_,. LOW
% Moisture: · 19 · decanted:
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) Y
(Y/N) N
500 (uL)
pH: 3.9
Date Received: 05/14/99
Date Extracted:05/28/99
Date Analyzed: 06/02/99
Dilution Factor: 1.0
Number TICs found: 24
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS. NPMBER COMPOUND NAME RT EST. CONC.
-------.. .--------======~===================== ==::::===== =============
1. UNKNOWN (BC) 5.25 320
2. UNKNOWN CARBOXYLIC ACID (BC) 13.91 140
3. •• UNKNOWN 16.94 99
4, UNKNOWN (BC) 17.64 93
5. UNKNOWN PHTHALATE 17.78 190
6. UNKNOWN PHTHALATE 17.99 360
7. UNKNOWN PHTHALATE 18.38 920
8. UNKNOWN 18.41 880
9. UNKNOWN 18. 46 600
10. UNKNOWN PHTHALATE 18.52 1600
11. UNKNOWN PHTHALATE 18.55 1400
12. UNKNOWN PHTHALATE 18.66 1400
13. UNKNOWN PHTHALATE 18.80 720
14. UNKNOWN PHTHALATE 18.83 710
15. UNKNOWN PHTHALATE 18.95 2300
16. UNKNOWN 19.48 320
17. UNKNOWN 20.92 140
18. UNKNOWN 21.60 110
19. UNKNOWN 22.20 120
20. UNKNOWN 22.69 210
21. UNKNOWN 24.21 250
22, UNKNOWN 25.11 180
23. UNKNOWN 25.58 170
24. UNKNOWN 26.42 120
25.
26.
27.
28,
29.
30.
FORM I SV-TIC
Q
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1B EPA SAMPLE NO.
SEMIVOLATII,:~ ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU
Contract: OLM03-REVS
:'Iic§vo2
5«"::P a,,p,:;,.--,-
Case No.: 34336
Matrix: ( soil/water) SOIL
SAS No.: SDG No. : 00002
Lab Sample ID: 938577
Sample wt/vol: 30.0 (g/mL) G Lab File ID: GH038577A70
Level:
% Moisture: ·14 decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
(Y/N) N
500 (uL)
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 5.2
CAS NO. COMPOUND
10.8 - 9 5 - 2 -c - - - ---Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
lll•44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
_\06-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N"Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-NitrophenoT
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
960 u
380 u
960 u
380 u
380 u
380 u
960 u
380 u
OLM03.0
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: ( soil/water) SOIL
RCSV02
Contract: OLM03-REVS
SAS 'No.: SDG No. : 00002
Lab Sample ID: 938577
Sample wt/vol: 30.0 (g/mL) G Lab File ID: GH038577A70
Level:
% Moisture: ~14 decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
(Y/N) N
500(uL)
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 5.2
CAS NO. COMPOUND
. 51-28-5--·-- - - - --2, 4 -Dinitrophenol
10O-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
121-14-2--------2,4-Dinitrotoluene
.$4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3------c--Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(1) -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
960 u
960 u
380 u
380 u
380 u
380 u
380 u
960 u
960 u
·380 u
380 u
380 u
960 u
380 u
380 U,
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
72 J
380 u
380 u
380 u
380 u
380 u
380 u
380 u
OLM03. 0
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lF EPA SAMPLE NO.
SEMIVOLATIL3 ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS RCSV02
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: ( soil/water) SOIL
Contract: OLM03-REVS
SAS 'No.: SDG No.: 00002
Lab Sample ID: 938577
Sample wt/vol: 30. 0 (g/mL) G Lab File ID: GH038577A70
Level: (low/med)-·.,.-LOW
-'•' -~
% Moisture: ·14 · decanted:
Concentrated Extract Volume:
Injection Volume: 2. 0 (uL)
GPC Cleanup: (Y/N) Y
Number TICs found: 6
(Y/N) N
500(uL)
pH: 5.2
CAS.NUMBER COMPOUND NAME
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
---------. --------======-==================== ======== ;;;::;::;:::::;;:;::::;::;::;::::===
1. UNKNOWN (BC) 4.60 670
2. UNKNOWN (BC) 5. 41 190
3. •• UNKNOWN 15.60 160
4. UNKNOWN PHTHALATE 16.68 110
5. UNKNOWN PHTHALATE 16.98 94
6. UNKNOWN 21.99 320
7.
8.
9.
10.
11. -12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
29.
30.
FORM I SV-TIC
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OLM03.0
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1B EPA SAMPLE NO.
SEMIVOLATII,E ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G
Level: (low/med).,./ LOW
-~--✓
RCSV0lMS
Contract: OLM03-REVS
SAS No.: SDG No.: 00002
Lab Sample ID: 938575
Lab File ID: GH038575A70
% Moisture: ·19 · decanted: (Y/N) N
I Concentrated Extract Volume: 500 (uL)
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
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Injection Volume: 2.0(uL)
GPC Cleanup: (Y/N) Y pH: 3.9
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
111~44-4--------bis(2-Chloroethyl)ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
.106-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
2000
410 u
2000
410 u
1100
410 u
410 u
410 u
410 u
1400
410 u
410 u
410 u
410 u
410 u
410 u
410 u
1400
410 u
410 u
410 u
2400
55 J
410 u
410 u
1000 u
410 u
1000 u
410 u
410 u
410 u
1000 u
1900
OLM03.0
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
RCSV0lMS
Lab Name: COMPUCHEM
Lab Code: COMPU Case No.: 34336
Matrix: ( soil/water) SOIL
Contract: OLM03-REVS
SAS No.: SDG No.: 00002
Lab Sample ID: 938575
Sample wt/vol: 30.0 (g/mL) G Lab File ID: GH038575A70
Level: (low/med).-✓·" LOW ,·..:-·..-::;"'
%-Moisture: ·19 · decanted:
Concentrated Extract Volume:
Injection Volume: 2.0(uL)
(Y/N) N
500 (uL)
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 3.9
CAS NO. COMPOUND
51-28-5-~-------2,4-Dinitrophenol
10-0-02-7-- - - - - --4-Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
121-14-2--------2,4-Dinitrotoluene
~4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenyletner -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8---------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
(11 -Cannot be separated trom Diphenylamine
FORM I SV-2
Q
1000 u
3100
410 u
1900
410 u
410 u
410 u
1000 u
1000 u
-410 u
410 u
410 u
2300
97 J
410 u
410 u
410 u
67 J
1500
410 u
410 u
47 J
43 J
210 J
410 u
410 u
410 u
49 J
410 u
410 u
410 u
OLM03.0
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
RCSV0lMSD
Lab Name: COMPUCHEM
Lab Code: COMPU Case No. : 34336
Macrix: (soil/water) SOIL
Contract: OLM03-REVS
' SAS No.: SDG No. : 00002
Lab Sample ID: 938576
Sample wt/vol:· 30.0 (g/mL) G Lab File ID: GJ038576A70
Level: (low/med)-./ LOW
-..:-·-_;,,
% Moisture: ·19 · decanted: (Y/N) N
Concentrated Extract Volume: 500 (uL)
Injection Volume: 2.0(uL)
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 3.9
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol
111.-~44-4-- - - ----bis ( 2-Chloroethyl) ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
1~6-46-7--------1,4-Dichlorobenzene
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
108-60-1--------2,2'-oxybis(l-Chloropropane)
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-di-n-propylamine
67-72-1---------Hexachloroethane -
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
lll-91-l--------bis(2-Chloroethoxy)methane
120-83-2--------2,4-Dichlorophenol -
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene
88-06-2---------2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethylphthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
FORM I SV-1
Q
1000
410 u
970
410 u
580
410 u
410 u
410 u
410 u
610
410 u
410 u
410 u
410 u
410 u
410 u
410 u
570
410 u
410 u
410 u
1000
410 u
410 u
410 u
1000 u
410 u
1000 u
410 u
410 u
410 u
1000 u
640
OLM03.0
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM
Lab Code: COMPU
Matrix: ( soil/water)
Sample wt/vol:
Level: (low/med)·-''
,,
~-_,.,,.,
%-Moisture: ·19
Concentrated Extract
Injection Volume:
RCSVOlMSD
Contract: OLM03-REVS
Case No.: 34336 SAS No.:
SOIL
30.0 (g/mL) G
LOW
decanted: (Y/N) N
Volume: 500(uL)
2.0(uL)
SDG No. : 00002
Lab Sample ID: 938576
Lab File ID: GJ038576A70
Date Received: 05/14/99
Date Extracted:05/18/99
Date Analyzed: 05/24/99
Dilution Factor: 1.0
I GPC Cleanup: (Y/N) Y pH: 3.9
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( 1)
CAS NO. COMPOUND
51-28-5---------2,4-Dinitrophenol
100-0 02 -7--

-

-

-

-

-
-4 -Nitrophenol
132-64-9--------Dibenzofuran
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
121-14-2--------2,4-Dinitrotoluene
i4-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7---------Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-methylphenol
86-30-6---------N-nitrosodiphenylamine (1)-
101-55-3--------4-Bromophenyl-phenylether -
118-74-1--------Hexachlorobenzene --
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
86-74-8--·-------Carbazole
84-74-2---------Di-n-butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)phthalate
117-84-0--------Di-n-octylphthalate -
205-99-2--------Benzo(b)fluoranthene
207-08-9--------Benzo(k)fluoranthene
50-32-8---------Benzo(a)pyrene
193-39-5--------Indeno(l,2,3-cd)pyrene
53-70-3---------Dibenzo(a,h)anthracene
191-24-2--------Benzo(g,h,i)perylene
-Cannot be separated trom Diphenylamine
FORM I SV-2
Q
1000 u
1100
410 u
730
410 u
410 u
410 u
1000 u
1000 u
410 u
410 u
410 u
1100
62 J
410 u
410 u
410 u
410 u
660
410 u
410 u
410 u
410 u
170 J
410 u
410 u
410 u
410 u
410 u
410 u
410 u
OLM03.0
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COMPUCHEM
a division of Libeny Analytical Corp.
04/JUN/99
..,,..,:;·"'·'
Roy F. Weston
5405 Metric Pl.
Suite 200
Norcross, GA 30092
Subject: Report of Data -Account Number# 501223 Order# 34336
::i(f:(\.)Enclosed are the results of analytical work performed in accordance
t·\i~}:Wi th the referenced account number.
· · Thi's·report covers 11 sample(s) appearing on the attached listing.
Thank you for selecting CompuChem Environmental for your sample
an"alysis. If you shou_ld have questions or require additional
analytical services please contact your representative at
1-800-833-5097.
Sincerely,
~L
CompuChem Environmental
a division of Liberty Analytical
Attachment
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: 919--379-$050
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COMPUCHEM
a division of Liberty Analytical Corp.
'
04/JUN/99
Roy F.·weston
5405 Metric Pl.
suite 200
Norcross, GA 30092
ACCOUNT#: 501223
.i CC# SAMPLE-ID
93357·0 RCSVOl
938577 RCSV02
938578 RCSS03
93~579 RCSSOl
938580 RCSV03
938581 RCSE02POND2
938582 RCSEOlPONDl
938583 RCSE04POND4
938584 RCSE03POND3
938585 RCSS02
938766 DRUMDISPOS
TOTAL NUMBER OF SAMPLES
RECEIPT DATE
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/14/99
5/15/99
= 11
501 Madison Avenue ■ Cary, N.C. 27513 ■ Tel: [phone] ■ Fax: [phone]
.
. !
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. . .. .,...,.----.-.~.--.. .--------------·····-···-·····-·-----·--~w~~~tP't.:'1,'.i'~,~: . . . , ' .. . . - . ' '!5!f~,. ~~., .... ·"' . ,, . -~~:::·~\,: . -. , .
~-I ,·
The sample data package shall include data for all analyses of all samples ·:_ · · .
.. in.one Sample Delivery Group (SDG), including field and analytical samples,·. ·· :_ .·.· .. ·
. reanalyses, blanks, spikes, duplicates, and laboratory control samples: The : •. · ' . , '
. · sample data package consists of the following: · ·· · ·· · ·
A.· Cover Page · ··
s:· Sample Data
. . _;
. ' ..
· C: Chain-of-Custody (CoC) Documentation
LAB CODE : COMPU
CASE#: ]Y5J6
.I
CONTRACT# : ILM04.0
SDG # : (25 6,✓<lf 2-
· .. '. ;. _. ..... :
-/• ..
. ,-/
. ' I .
',:;:~;..;
I· ... , , ...
11
1 A. Cover Page -,
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Inorganic Analyses Data Package.
-· The Cover. P·age includes laboratory information, the Case and SDG numbers, the client ID
numbers in alphanumeric order showing the client ID numbers cross-referenced with Lab ID
numbers, comments, and completion of the statement on the use of ICP background and
interelement correction for the samples. ·
On separate pages, the laboratory will include any problems encounterecl; both tech~ical and
·· . administrative, the corrective action taken, and the resolution. This information is included in
. the Inorganic Case Summary Narrative which follows the Cover Pag"e,?~0 · .J •· ··... . ... ·· ·.
·-. -
••
I U.S. EPA -CLP
COVER PAGE -INORGANIC ANALYSES DATA PACKAGE
I Lab Name: COMPUCHEM ________ _ Contract: ILM04.0
SAS No.: Lab
I sow
Code: COMPU
No. : ILM04. 0
Case No.: 34336 SDG No. :00002
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EPA Sa,mple No.
DR.f,JMDISPOS
.-RCSEOlPOND_l_
-RCSE02POND2-
RCSE03POND3
-RCSE04POND4-
RCSS01 RCSS02 ___ _
-RCSS03 ----RCSV0l -RCSV02 ___ _
-RCSV03 RCSV03=D __ _
RCSV03S ----
Lab Sample ID
938766 -----938582 ____ _
938581 938584 ____ _
938583 938579 ____ _
938585 -----938578 938570 ____ _
938577 -----938580 938572 ____ _
938571 -----
I Were ICP interelement corrections applied? Yes/No YES
I Were ICP background corrections applied?
If yes -were raw data generated before
application of background corrections?
Yes/No
Yes/No
YES
NO
I Comments:
THE FOLLOWING ANALYTES HAVE BEEN FLAGGED WITH AN "E" TO INDICATE
--SERIAL DILUTION RESULTS WHICH WERE OUTSIDE CONTROL LIMITS: -----
I --

-

-
CALCIUM COPPER ---------------------------------
I I certify that this data package is in compliance with the terms and
conditions of the contract, both technically and for completeness, for
other than the conditions detailed above. Release of the data contained
I in this hardcopy data package and in the computer-readable data submitted
on floppy diskette has been authorized by the Laboratory Manager or the
Manager's designee, as verified by the following signature.
I Signature: vL£ d ~ Name: ~ e,.,J,.
Date: Jc~ 7 ( 1f1 Title: ~~ ///ltl,UcY'.'::8&'.'=
0 7 --/L 0 ,I
COVER PAGE -IN ILM04.0
&I°</, u
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Com uChem
a Division of Liberty Analytical Corp.
501 Madison Avenue Cary, NC 27513
INORGANIC CASE SUMMARY NARRATIVE
CASE# 34336 SDG # 00002
CONTRACT# ILM04.0
The indicated Sample Delivery Group (SDG) consisting of eleven (11) soil samples was received into the
laboratory information management system (LIMS) on May 14 and 15. 1999 intact and in good condition
with Chain of Custody (COC) Records in order, unless otherwise noted in any attachments or Quality
Assurance Notices. Sample 1D's reported in this data package are noted by the receiving department on the
COC if they differ from those listed by the samplers on the COC.
The samples were analyzed, in accordance with EPA CLP Statement of Work (SOW) document ILM04.0
for the metallic analytes contained in the Inorganic Target Analyte List (TAL).
The Form 10 for the mercury IDL shows a reading of 0.0 UG/1. There is an inability to get the IDL: 0.048
l}G/1 to show on the form.
SAMPLE IDs:
The following customer IDs are associated with this SDG:
DRUMDISPOS
RCSE04POND4
RCSV0I
RCSE0IPONDI
RCSS0I
RCSV02
INSTRUMENTAL QUALITY CONTROL:
RCSE02POND2
RCSS02
RCSV03
RCSE03POND3
RCSS03
All calibration verification solutions (ICY & CCV), blanks (ICB, CCB) and interference check samples
(!CSA & ICSAB) associated with this data were confirmed to be within EPA CLP allowable limits.
SAMPLE PREPARATION QUALITY CONTROL:
The sample preparation procedure verifications (LCSS & PBS) were found to be within acceptable ranges
and all field samples were prepared and analyzed within the contract specified holding times.
MATRIX RELATED QUALITY CONTROL:
The sample matrix spike, CCN = 938571 (RCSV03S) was found to be outside CLP control limits for
antimony. The reported concentration for this analyte is flagged with an "N" on all associated Form I and
on Form Sa.
An "N" indicates a matrix-related interference in the sample preparation procedure &/or analysis for the
flagged analyte. This is normally the consequence of a relatively high anionic content in the sample or (for
some sediments) an inconsistent sample matrix relative to that analyte.
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CLP control limits for matrix spike recoveries are set at 75% to 125% of the analyte quantity added unless
original sample concentrations exceed the true values of these "spikes" by a factor of four or more; in this
case effected analytes are not flagged even if recoveries fall'outside percentage recovery control limits.
Post-digestion spikes are mandatory for analytes demonstrating unsatisfactory matrix spike recoveries
during ICP analysis (excluding silver). The results of such spikes are presented on Form 5b.
Unsatisfactory rec~wery of post-digestion spikes of this type do not have bearing upon the aforementioned
"N" flag~. Qut-maY~indicate interference during analysis &/or a solution matrix which is hostile to the
analyte in question.
Satisfactory recovery ofan analyte in a post-digestion spike of this type implies interference by the
required preparation procedure or in the sample matrix itself. Lack of uniformity for an analyte in
sediments will also result in satisfactory recovery of post-digestion spikes after failure in the related matrix
spike.
The sample matrix duplicate, CCN = 938572 (RCSV03D) was outside CLP control limits for lead. The
reported concentrations for these analytes are flagged with a"•" on all associated Form I and on Fann 6.
A"*" indicates a non-homogeneous sample matrix in regard to the flagged analyte. This is normally the
¼Onsequence Of a relatively coarse texture or of a mixed-matrix in sediment samples.
CLP control limits for duplicate determinations are+/-20% Relative Percent Difference (RPD) for
concentrations greater than or equal to five times the CRDL in both the original and duplicate samples, and
••+/-the CRDL for concentrations less than five times the CRDL. The RPD is not calculated if both the
original and duplicate values fall below the IDL.
A five-fold serial dilution of sample, CCN = 938580 (RCSV03L) was performed in accordance with CLP
requirements for ICP analysis.
The adjusted sample concentrations were outside CLP control limits for calcium and copper, which are
flagged with an "E" on all associated Form 1, the Cover Page and Form 9.
An "E" indicates that a chemical or physical interference effect was encountered during the analysis of the
flagged analyte. As a result of this interference, all values for the analyte in the same matrix must be
considered to be estimated quantities.
CLP control limits for serial dilution are defined as a deviation less than or equal to I 0% in the dilution-
adjusted concentrations from the original values for all analyte concentrations with values greater than fifty
(50) times their respective Instrument Detection Limit (IDL) in the original sample.
This SDG package was processed using the Ward Scientific software. This software package has a seven
character limitation on the Forms 13 and 14 --any sample !D's which exceed seven characters are truncated
from left to right on these forms.
Release of the data contained in this hard copy data package has been authorized by the laboratory
manager or his designee, as verified by the following signature.
0£,--dY al
Thomas R. Cole
Chemist II
June 3, I 999
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Com uChem
a Division or Liberty Anal~·tical Corp.
501 ,\l:1JisM ,\\·crmi: C:1ry. SC 275 IJ
DATA REPORTING QUALIFIERS FOR INORG.ANICS
On Furm I. undt:r the ..:ulunrn \abckd ··c· for conci.:ntr~nion qualitkr and ··o·• for qualiticr. e:i.ch n:sult is llagg<:d with the specitic
Jata reporting qualili-c-,s listed bc:low, as appropriate:. Up to live qualilicrs may be rc:portcd on Fann I for each analytc. --The C (concentration) qualifiers used are:
ll:
B:
This Hag indii.:atcs the analytt." was analyzed for but not 1.ktcctec..l. This reported value was obtainc:d from a reading that
was h:ss th:in the Instrument Detection Limit (IDL). The IDL will be adjusted to reflect any dilution and. for soils. the
percent moisture.
This llag indicates the analyte was analyzed for and the reported value was obtained from a reading that was less lhan the
Contract Rt:quired Detection Limit (CRDL) but greater than or equal to the lns1rument Oi:tection Limit (IDL).
The Q qualifiers used are:
E: This tb.g indic:ucs an estim:i.tt:d value. This flag is usi:d:
M:
!. Whi:n 1ht: st:rial dilution (a tivt: fold dilution tOr CLP and a live fold dilution for SW•846 method 6010B) rt:sults are
not within 10%. The ana\yte concentration must bi: sullicient!y high (minimally a factor of 50X above the IDL in
• thi;: original s:i.mple).
2. When thi: analytical spike ri:eovcry associated with the s:i.mpk is below 40% at\cr two successive dilutions by
Gr:::iphitt: Furnace Atomic Absorption (GF,\A).
This nag applies to GFM analysi:s for concentrations gri:a:er than thc Contract Ri:quired
Detection Limit (CRDLJ. Thi:. !lag is only used for GFAA ifthc :::in:i.ly1ical sample or an:i.lytical
spike duplic:i.te injection reading is not within 20% of lhe-Rda{ive St:::indard De\·i:i.tion (RSD).
N: This llag indicati:s tht: sample spike recovery is outside of control limits:
S:
W:
This !lag is usl!d tOr duplicati: analysis whi:n the sample and the sample duplicate results are not
within control limits.
This 11:l.g. applil!s tll GF:\A analyses to indicate the reported value \\:LS determined by the
\.kthod OfSt:uidard ,\ddition p.tS.·\J.
This tlag applii:s lO GFAA analyses when the post-digestion spike (analytical spike) is out of control limits (85% -115%).
while sample absorbancc is less th:ln 50% or··spike·· absorbance [··spike .. is defined as (absorbance or concentration of
spike sample) minus (absorhancc or concentration of the sample)\
+: This !lag applit:s to GF,\A :uialyses when the corrc!:uion coetlicicnt for the MSA is less th:i.n 0.995 a!kr two MSA
analysi:s .
.'\'OTE: F.niering ·•s" .. w•·. or ..... is mutually exclusive. No cornbina.ti11n Clfthi:si:: qualitiers can appear in tht: same lit:ld for an
ana!ytl!.
The extensions: o: S. M, L.A. added to the end or the client ID represent as follows:
D: matri-.; duplic:itc
S: m:itri., spike
M: matri, spike Jup\icate
J.· ,;erial Jilution
,\: p11-;\ digcstion spikt'
_\lethnd Cot.I es:
!':
CV:
C,\·
F:
ICP PLAS:-.IA
\IERCLiR Y COLD VAPOR,\,\
.\1 IDI-DISTILL,\TION SPECTROl'f IOTO\IETR!C
FLR'.'/ACE AA
.. . }ffft:i~'<·<·'··-·--~--,..... ...... ·-· •···. ·:/:
• j
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t~ ~_: : . . . . .. :t·.
B. Sample Data,
1. Resu,lts ... .-:;,, -· ..
. 2. -Quality Control Data .
3. Quarterly Verification of lnstrum~nt P~rforrnance -
4. Raw Data
· 5. Digestion and Distillation Logs
'' . '.
LAB CODE : COMPU
CASE# : 3 'Ii JG
CONTRACT# : ILM04.0
SDG #: 0 rt5_6<7z._
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. _,,
1 . Results
. Sample results shall be arranged in packets with the
lnorgJ!nic Analysis Data Sheet (Form I ~ IN). These sample .•·• ..
_packets shall be placed in increasing Client Sample, ID . •
number order, considering both letters and numbers, and.. ··
shall include all the samples in the SDG. · · · , , .
,'I"
. ·-.....
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
DRUMDISPOS
.Lab Name: COMPUCHEM
Lab Code: COMPU_
Contract: ILM04.0
Case No.: 34336 SAS No.:
.Matrix (soil/wat~~_;/SOIL_
Level (low/med) LOW_
1% Solids: 79.3
SDG No.: 00002
Lab Sample ID: 938766
Date Received: 05/15/99
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Concentration Units (ug/L or mg/kg dry weight) MG/KG __
••
I Color Before:
Color After:
I Comments:
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CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 7.3
Antimony_ 0.25
Arsenic 0.35 -Barium 0.27
Beryllium 0.07
Cadmium 0.05
Calcium-14.9
Chromium 0.13 -Cobalt 0.10 --Copper __ 0.98
Iron 37.2
Lead 0.29
Magnesium 3.5
Manganese 0.66
Mercury_ 0.03
Nickel 0.96
Potassium 6.7
Selenium 0.40 -Silver 0.10 --Sodium 25.5
Thallium 1.1
Vanadium-3.1 -Zinc 0.89
Clarity Before:
Clarity After:
FORM I -IN
C Q M
--B p -u N p ----u p -B p -B p -u p -B E p ----u p -u p -B E p ----p --B * p ----B p -B p -u CV
B p -B p -u p -u p -u p
B p -B p -B p -
--
-
Texture: FINE
Artifacts:
ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO. I··
I INORGANIC ANALYSES DATA SHEET
. ··.·.,~=,·1,'.-· ... ,. __ :·
RCS_E0lPONDl
•
Lab
Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code: COMPU Case No.: 34336 SAS No.:
•
Matrix ( soil/wate_ r)_~.,SOIL_
-✓
Level (low/med). -LOW ,,,, Solids: 64.2
· SDG No.: 00002
Lab Sample ID: 938582
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight): MG/KG __
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I Color Before:
Color After:
Comments:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 12600
Antimony 0.29
Arsenic -2.4 -Ba.rium 15.8
Beryllium 0.18
Cadmium 0.06
Calcium-391
Chromium 21.1 -Cobalt 0.24 --Copper __ 5.2
Iron 28400
Lead 8.5
Magnesium 291
Manganese 5.0
Mercury_ 0.06
Nickel 1.5
Potassium 441
Selenium 0.47 -Silver 0.12
Sodium--61.8
Thallium 5.7
Vanadium-31.l -Zinc 28.7
Clarity Before:
Clarity After:
C Q M
--p -

-
u N p ----B p -B p -B p -u p -B E p ----p -

-
B p -B E p ----p -

-
* p -----B p -p -

-
B CV
B p -B p -u p -u p -B p -p -

-
p -

-
p -

-
--
--
Texture: FINE
Artifacts:
I Undecanted_Dry_Weights __ Container:l.29g_Wet:6.66g_Dry:4.74g ___ _
I
I FORM I -IN ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO. I
I INORGANIC ANALYSES DATA SHEET
'RCSE0 2 POND2
Contract: ILM04.0
I Lab Name: COMPUCHEM
Lab Code: COMPU_ Case No.: 34336 SAS No.:___ SDG No.: 00002
I Matrix (soil/wa_t~r;,;_.,SOIL_
Level (low/med) LOW_
1% Solids: 45.9
Lab Sample ID: 938581
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight): MG/KG __
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I Color Before:
Color After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 4220
Antimony_ 0.40
Arsenic 2.0 -Barium 11.7
Beryllium 0.17
Cadmium 0.33
Calcium-772
Chromium 6.9 -Cobalt 0 .. 58
Copper __ 208
Iron 4970
Lead 42.8
Magnesium 134
Manganese 10.3
Mercury_ 0.10
Nickel 20.9
Potassium 114
Selenium 0.65 -Silver 0.27
Sodium--94.8
Thallium 1.5
Vanadium-8.8 -Zinc 106
Clarity Before:
Clarity After:
C Q
-
-u N ---B
B
B
B
B E ---
-B
E -----* ----B
-B
-B
u
B
B
B
B
-
-
-
M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -p -p -p -p -
-
-
Texture: FINE
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.30g_Wet:6.42g_Dry:3.65g ___ _
I
I FORM I -IN ILM04.0
U.S. EPA -CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RCSE03POND3
lfab
~ab
Name: COMPUCHEM Contract: ILM04.0 ---------
Code: COMPU_ Case No.: 34336 SAS No.:
tatrix (soil/wate~_;..,·.SOIL_
Level (low/med) .. -· LOW
J. Solids: 78.3
SDG No.: 00002
Lab Sample ID: 938584
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight) MG/KG __
I
I
I
I
I
I
I
I
I Color
Color
•
Before:
After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
744D-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 4200
Antimony_ 0.26
Arsenic 1.1 -Barium 4.7
Beryllium 0.08
Cadmium 0.05
Calcium-238
Chromium 4.4 -Cobalt 0.21 --Copper __ 245
Iron 2720
Lead 4.5
Magnesium 77.1
Manganese 2.9
Mercury_ 0.03
Nickel 1. 4 --Potassium 82.9
Selenium 1.0 -Silver 0.10
Sodium--435
Thallium 0.66
Vanadium-6.8 -Zinc 4.3
Clarity Before:
Clarity After:
C Q M
--p --u N p ----B p -B p -B p -u p -B E p ----p --B p -E p -----p --* p -----B p -B p -u CV
B p -B p -B p -u p -B p -B p -B p -B p -
--
--
Texture: FINE
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.30g_Wet:7.39g_Dry:6.07g ___ _
I
I FORM I -IN ILM04.0
I
I
U.S.-· EPA CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: COMPUCHEM Contract: ILM04.0 ---------
Lab Code: COMPU Case No.: 34336 SAS No.:
Matrix (soil/water} _;_./SOIL
EPA'SAMPLE NO.
RCSE04POND4
Level (low/med}
I %_Solids:
LOW
69.1
SDG No. : 00002
Lab Sample ID: 938583
Date Received: 05/14/99
!
I
I
I
I
I
I
I
I
I
I
I
I
I I
Concentration Units (ug/L or mg/kg dry weight}: MG/KG __
CAS No. Analyte Concentration
7429-90-5 Aluminum 7270 -7440-36-0 Antimony 0.27
7440-38-2 Arsenic -3.1 -7440-39-3 Barium 15.8
7440-41-7 Beryllium 0.20
7440-43-9 Cadmium 0.10
·• 7440-70-2 Calcium-1620
7440-47-3 Chromium 15.1 -7440-48-4 Cobalt 0.80
7440-50-8 Copper __ 655
7439-89-6 Iron 9670
7439-92-1 Lead 58.9
7439-95-4 Magnesium 524
7439-96-5 Manganese 7.1
7439-97-6 Mercury_ 0.23
7440-02-0 Nickel 55.2
7440-09-7 Potassium 176
7782-49-2 Selenium 1.5 -7440-22-4 Silver 0.11
7440-23-5 Sodium--139
7440-28-0 Thallium 1.4
7440-62-2 Vanadium-22.0 -7440-66-6 Zinc 117
Color Before: BROWN Clarity Before:
Color After: YELLOW Clarity After:
Comments:
C Q
-
-u N ----B
B
B
E ----
-B
E ----
-* ----B
-
-
-B
-u
B
B
-
-
-
-
M
p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -p -p -p -p -
-
-
Texture: FINE
Artifacts:
Undecanted_Dry_Weights __ Container:l.29g_Wet:6.57g_Dry:4.94g ___ _
FORM I -IN ILM04.0
.· -·'' '-...-: :,t,:: • .:. ,· ~ "'.~, i ·,; ·.' .
U.S .. EPA -CLP
1
' -·-.1,:· ,f1~-t?:J.it•."' ;_; ?-~"-,: ,.
El? A'. {SAMPLE NO .
I INORGANIC ANALYSES DATA SHEET
.-,ab
... ab
Name: COMPUCHEM Contract: ILM04.0 ---------
Code: COMPU Case No.: 34336 SAS No.:
ratrix (soil/wate~: .. , .. SOIL_
Level (low/mes,r ·· · LOW_ • Solids: 76.2
SDG No.: 00002
Lab Sample ID: 938579
Date Received: 05/14/99
I
Concentration Units (ug/L or mg/kg dry weight): MG/KG __
I
I
I
I
I
I
I
I
·•
I Color Before:
Color After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440·-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 1290
Antimony_ 0.73
Arsenic 0.68 -Barium 3.4
Beryllium 0.11
Cadmium 0.09
Calcium-. 321
Chromium 2.9 -Cobalt 0.82 --Copper __ 24.9
Iron 1320
Lead 26.2
Magnesium 215
Manganese 3.1
Mercury_ 0.04
Nickel 2.4
Potassium 33.8
Selenium 0.40 -Silver 0.10
Sodium--79.7
Thallium 1.0
Vanadium-2.6 -Zinc 26.1
Clarity Before:
Clarity After:
C Q
--B N ---B
B
B
B
B E ---
-B
E ----
-* ----B
B
B
B
B
u
u
B
B
B
-
-
-
M
-p -p -p -p -p -p -p -p -p -p -p -p -p -p -CV
p -p -p -p -p -p -p -p -
Texture: FINE_
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.29g_Wet:7.39g_Dry:5.94g ___ _
I
••
FORM I -IN ILM04.0
Lab Name: COMPUCHEM
U.S._ EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
Contract: ILM04.0
EPA SAMPLE NO.
RCSS02
I Lab Code: COMPU ___ C_a_s_e_N_o __ -,-3-4336 SAS No.: SDG No.: 00002
Lab Sample ID: 938585
Date Received: 05/14/99 I Matrix (soil/water) -~_,-SOIL_ --Level (low/med) LOW
I % Solids: 81. 5
Concentration Units (ug/L or mg/kg dry weight) MG/KG __
I
I
I
I
I
I
I
I
I
I
I
I
I
CAS No. Analyte Concentration C Q M
--
7429-90-5 Aluminum 790 p -

-
7440-36-0 Antimony_ 0.25 u N p ----
7440-38-2 Arsenic 0.34 u p
--
7440-39-3 Barium 3.9 B p -
7440-41-7 Beryllium 0.09 B p -
7440-43-9 Cadmium 0.05 u p
•• 7440-70-2 Calcium--21.9 B E p
7440-47-3 Chromium ----1.1 B p --
7440-48-4 Cobalt 0.10 u p ---7440-50-8 Copper __ 1. 8 B E p ----7439-89-6 Iron 76.5 p -

-
7439-92-1 Lead 8.7 * p -----7439-95-4 Magnesium 11.8 B p -7439-96-5 Manganese 3.2 B p -
7439-97-6 Mercury_ 0.03 u CV
7440-02-0 Nickel 0.34 B p -7440-09-7 Potassium 19.4 B p -
7782-49-2 Selenium 0.39 u p --7440-22-4 Silver 0.10 u p
7440-23-5 Sodium---24.8 u p -
7440-28-0 Thallium 0.52 B p -
7440-62-2 Vanadium 1.8 B p --
7440-66-6 Zinc 5.9 p -

-
--
--
Color Before: GREY __ _ Clarity Before: Texture: FINE
Color After: YELLOW Clarity After: Artifacts:
Comments:
Undecanted_Dry_Weights __ Container:l.30g_Wet:6.66g_Dry:5.67g ___ _
FORM I -IN ILM04.0
Ct'~j~
•,-',,•:•:•.·.·N••• • •, ....• ,:_.
~\!!J~-~~~r
i~.tt.· U.S. EPA CLP
1 EPA SAMPLE NO.
I INORGANIC ANALYSES DATA SHEET
RCSS03;
Lab
ILab
Name: COMPUCHEM Contract: ILM04.0 ---------
Code: COMPU Case No.: 34336 SAS No.:
.Matrix (soil/wa_t~r_;.>·SOIL_
Level (low/med): LOW_
1% Solids: 86.3
SDG No.: 00002
Lab Sample ID: 938578
Date Received: 05/14/99
Concentration Units (ug/L or mg/kg dry weight): MG/KG __
I
I
I
I
I
I
I
I
I
•
1 Color Before:
Color After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1'
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 2360
Antimony-0.23 -Arsenic 0.32 -Barium 5.1
Beryllium 0.05
Cadmium 0.05
Calcium-562
Chromium 4.3 -Cobalt 0.24 --Copper __ 1. 6
Iron 742
Lead 3.2
Magnesium 51. 0
Manganese 1.8
Mercury_ 0.02
Nickel 0.48
Potassium 89.6
Selenium 0.37 -Silver 0.09
Sodium--23.2
Thallium 1.3 -Vanadium 6.4 -Zinc 2.1
Clarity Before:
Clarity After:
C Q
-
-u N ---u
B
B
u
B E ---
-B
B E ---
-* ----B
B
u
B
B
u
u
u
B
B
B
-
-
M
p -p -p -p -p -p -p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p -p ---
Texture: FINE
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.32g_Wet:6.85g_Dry:6.09g ___ _
I
I
FORM I -IN ILM04 iyt.,\
1~
·:ii-,
.. :,:-:::t'Z,i:: .JI: I
I
U.S. EPA -CLP
1 EPA SAMPLE NO. ~ff/
INORGANIC ANALYSES DATA SHEET
·. RCSV0l
Lab
I Lab
Name: COMPUCHEM ________ _ Contract: ILM04.0
Code : COMPU . Case No. : 34336 SAS No. :
I Matrix ( soil/water) ;,,,-SOIL_
__ ,..: .. 4'
Level (low/med): LOW_
1~ Solids: 80.5
SDG No.: 00002
Lab Sample ID: 938570
Date Received: 05/14/99
Concentration Units (ug/L or mg/kg dry weight): MG/KG __
I
I
I
I
I
I
I
I
I
·•
I Color Before:
Color After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
YELLOW
Analyte Concentration
Aluminum 2260
Antimony= 0.24
Arsenic 0.33 -Barium 5.1
Beryllium 0.12
Cadmium 0.05
Calcium-13.1
Chromium 2.6 -Cobalt 0.30 --Copper __ 1.4
Iron 198
Lead 2.6
Magnesium 43.9
Manganese 1.2
Mercury_ 0.03
Nickel 0.98
Potassium 37.3
Selenium 0.38 -Silver 0.10
Sodium--35.3
ThalliU111 0. 9.2 -Vanadium 3.3 -Zinc 2.6
Clarity Before:
Clarity After:
C Q
-
-u N ---u
B
B
u
B E ---
-B
B E ---
-* ----B
B
B
B
B
u
u
B
B
B
B
-
-
M
p -p -p -p -p -p
p -p -p -p -p -p -p -p
CV
p -p -p -p -p -p -p -p -
-
-
Texture: FINE
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.28g_Wet:6.72g_Dry:5.66g ___ _
I
I
FORM I -IN ILM04.0
,, .. '
I
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: COMPUCHEM ________ _ Contract: ILM04.0
SAS No_: .ab Code: COMPU Case No.: 34336
EPA SAMPLE NO.
RCSV02
SDG No.: 00002
Matrix ( soil/water) : .SOIL
ILevel (low/med). ---.:,-,,·-LOW
Lab Sample ID: 938577
Date Received: 05/14/99
Solids: 85.6 I" Concentration Units (ug/L or mg/kg dry weight) MG/KG __
I
I
I
I
I
I
I
I
I
Color
I color
..
Before:
After:
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
BROWN
. YELLOW
Analyte Concentration
Aluminum 3520
Antimony 0.74
Arsenic -0.31 -Barium 5.1
Beryllium 0.10
Cadmium 0.04
Calcium 177
Chromium 4.7 -Cobalt 0. 40 --Copper __ 593
Iron 574
Lead 35.0
Magnesium 375
Manganese 3.3
Mercury_ 0.04
Nickel 6_0
Potassium 42_4
Selenium 0.36 -Silver 0.09
Sodium--22.7
Thallium 0.51 -Vanadium 2-8 -Zinc 21. 8
Clarity Before:
Clarity After:
C Q M
--p --B N p ----u p -B p -B p -u p -B E p ----p_ --B p -E p -----p --* p -----B p -B p -B CV
B p -B p -u p -u p -u p -B p -B p -p --
--
--
Texture: FINE
Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.31g_Wet:7.75g_Dry:6.82g ___ _
I
I
FORM I -IN ILM04.0
-
I
I
U.S. EPA -CLP
1
INORGANIC ANALYSES DATA SHEET
EPA SAMPLE NO.
RCSV03
I Lab Name: COMPUCHEM. ________ _ Contract: ILM04.0
Lab Code: COMPU_ Case No.: 34336 SAS No.: SDG No. : 00002
Lab Sample ID: 938580
Date Received: 05/14/99 I Matrix (soil/water) ;_,,SOIL_
,.-·--~·
Level (low/med): LOW
I% Solids: 80.0
I Concentration Units (ug/L or mg/kg dry weight): MG/KG __
I
CAS No. Analyte Concentration C Q M
--
7429-90-5 Aluminum 2500 p -
I
Antimony 7440-36-0 0.25 u N p
Arsenic -
----
7440-38-2 1.2 B p
Barium --
7440-39-3 7.7 B p
Beryllium
-
7440-41-7 0.09 B p -
I
7440-43-9 Cadmium 0.06 B p
Calcium-
-
7440-70-2 533 B E p
7440-47-3 Chromium
----
3.5 p
--
7440-48-4 Cobalt 0. 31 B p
I 7440-50-8 Copper=
-6.0 B E p ----
7439-89-6 Iron 1720 p --
7439-92-1 Lead 7.5 * p -----
I 7439-95-4 Magnesium 75.2 B p -
7439-96-5 Manganese 8.2 p
7439-97-6 Mercury_ 0.04 B CV
I'
7440-02-0 Nickel 1.4 B p
7440-09-7 Potassium
-
41.6 B p
7782-49-2 Selenium
-1.1 B p
--
7440-22-4 Silver 0.10 u p
I 7440-23-5 Sodium--
-
31.7 B p
7440-28-0 Thalliuin
-
0.78 B p
7440-62-2 Vanadium-
-4.0 B p -
I.
7440-66-6 Zinc 9.3 p --
--
--
I Color Before: BROWN Clarity Before: Texture: FINE_
Color After: YELLOW Clarity After: Artifacts:
I Comments:
Undecanted_Dry_Weights __ Container:l.3Dg_Wet:6.55g_Dry:5.50g ___ _
I
1: FORM I -IN