NCD981021157_20050502_New Hanover County Airport Burn Pit_FRBCERCLA C_Correspondence, 1990 - 2005-OCR

•
May 2, 2005
Memorandum
TO: FILE
From: Kyle R. Hagen ~~
Environmental Engineer
NC Superfund Section
RE: Overview of Remedial Action Semi-annual Sampling
New Hanover County Airport Bum Pit
NCO 981 021 157
Wilmington, New Hanover County, NC
On May 2, 2005, one representative of the NC Superfund Section provided
overview of the semi-annual groundwater sampling for the pulsed air sparging system
at the New Hanover County Airport Burn Pit Superfund Site, located in Wilmington,
North Carolina. Observed Dimitri Talbert of Catlin Engineers and Scientists
recording parameter readings (pH, conductivity, temperature, Redox Potential, visual
turbidity) and collecting three vials for volatile organic samples at the monitoring
wells labeled CMW-013, MWD-002, PVSMW-002, and CMW-012. Well no.
PVSMW-002 was also used to collect monthly DO readings during the sampling
event.
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• •
Monitoring Well No. CMW-013 with equipment setup showing the peristaltic
pump used for low-flow pumping and a continuous parameter monitor connected
to the inline flow-through cell.
• •
Monitoring Well No. CMW-012 with equipment setup showing the peristaltic
pump used for low-flow pumping and a continuous parameter monitor connected
to the inline flow-through cell.
• • FILE ropy
North Carolina Department of Environment and Natural Resources
Dexter ?. i•/iailhews, Direstar
Ms. Beverly Hudson
Remedial Project Manager
US EPA Region fV
Division of Waste Management
June l 0, 2004
61 Forsyth Street, Eleventh (11) Floor
Atlanta, Georgia 30303
RE: Comments on the Monitoring Report, April 2004 Sampling Event
New Hanover County Airport Bum Pit, NCD 981 021 157
Wilmington, New Hanover County, North Carolina
Dear Ms. Hudson:
i~1icria::;: ;=-::dsley, G::)VernD;
V\lilliarn G. i=:.J:;s Jr., s~:ieLary
The Monitoring Report for the April 2004 Sampling Event of contaminated
groundwater at the New Hanover County Airport Bum Pit Superfund Site located in
Wilmington, North Carolina has been received and reviewed by the North Carolina
Superfund Section. The North Carolina Superfund Section offers the following comments.
Specific Comments:
I. In the first paragraph of Section 2.0, the first sentence states that "there are sixteen
monitoring wells selected to monitor groundwater characteristics on site (see Figure 2)."
When Figure 2 is consulted and all the bolded monitoring wells, both perfom1ance
verification and compliance, are counted there are I 7 total monitoring wells. This
becomes confusing when Table I is consulted and 21 total monitoring wells, both
performance verification and compliance, are tabulated. The confusion is compounded
further since Table I designates the wells, T-13, T-14, T-15, and T-16 as compliance
monitoring wells although Figure 2 does not designate them as such. Also the wells, T-
l 2, TMW-1, and TMW-2 are not listed in the Table 1 summary but are shown on Figure
2. Even if these three wells are not monitored during sampling events, please include
them in Table I and designate them as "not currently monitored". Please clarify these
discrepancies in Section 2.0, Table I. and Figure 2.
2. In the paragraph of Section 4.0, please define the acronym PAS in the second sentence
prior to its first occurrence in the last sentence of this section.
1646 Mail Service Center, Raleigh, North Caroiina 27699-1546
Phone ~19-733-4996 I FAX 9'19-7'1 5-3505 \ Internet hiip/iw2s1enotnc.org
,;;1 E.cua! Op;ioitunity: Affim1a1ive .:..::1:m E:;r::)bye, -?rinte:J ori Duai ?um::ise ~e:::vc:e:-1 ?::~--e;
Ms. Beverly Hudson
06-10-2004
Page 2 of2
• •
3. In the last p_aragraph in Section 7.0, the last sentence states that well, MWD-002, is
"screened to 27.5 feet BGS". This docs not coincide with Table 1, which lists the
screened interval for MWD-002 as 17 to 27 ft. BGS. Please clarify this discrepancy.
If you have any questions or comments, please contact me, at [phone], extension
299.
cc: File
Sincerely, ,z;;, /If!'/ J /
/ ijlt /, -, 1~,.,,_
Kyle R. Hagen
Environmental Engineer
NC Superfund Section
• &i~ •
NCDENR
North Carolina Department of Environment and Natural Resources
Deztsr F:. 1,,1atiriev1s. Direct:,r Division of Waste Management i·Aichael r. ~asiey, Govemr,,
Ms. Beverly Hudson
Remedial Project Manager
US EPA Region JV
May 3, 20(14
61 Fors11h Street, Eleventh (11) Floor
Atlanta, Georgia 30303
RE, Comments on the Monitoring Report, January 2004 Sampling Event
New Hanover County Airport Bum Pit, NCD 981 021 157
Wilmington, New Hanover County, North Carolina
Dear Ms. Hudson,
1Niliia;-r: G. Ross Jr., Se-:re:ciy
The Monitoring Report for the January 2004 Sampling Event of contaminated
groundwater at the New Hanover County Airport Bum Pit Superfund Site located in
Wilmington, North Carolina has been received and reviewed by the North Carolina
Superfund Section. The North Carolina Superfund Section offers the following comments.
Specific Comments,
1. In the first paragraph of Section 2.0, the first sentence states that "there are sixteen
monitoring wells selected to monitor groundwater characteristics on site (see Figure 2)."
\Vhen Figure 2 is consulted and all the monitoring wells, both performance verification
and compliance, are counted there are 17 total monitoring wells. This becomes confusing
when Table 1 is consulted and 21 total monitoring wells, both performance verification
and compliance, are tabulated. The confusion is compounded further since Table 1
designates the wells, T-13, T-14, T-15, and T-16 as compliance monitoring wells
although Figure 2 does not designate them as such. Also the wells, T-12, TMW-1, and
TMW-2 are not listed in the Table 1 summary but are shown on Figure 2. Even if these
three wells are not monitored during sampling events, please include them in Table 1 and
designate them as "not currently monitored". Please clarify these discrepancies in Section
2.0, Table 1, and Figure 2.
7 In the paragraph of Section 4.0, please define the acronym PAS in the second sentence
prior to its first occurrence in the last sentence of this section.
1646 Mail Service Center. Kaleigh l~orth Carolina 27S99-1645
Phone [phone] \ FAX [phone] \ lntemet httpliwasienoinc.org
.:..n :.q:.ial Opoo;rnniiy ! Affirmative A:;bn Em;Jr:'..'lye: -::..nn:e:: o:; Jc;a; ?u:-i:2se ?.e:y:lej ?2:>et
Ms. Beverly Hudson
05-03-2004
Page 2 of2
• •
3. In Section 5.0, please provide a better point of reference for groundwater flow instead of
just the "northeast region of the site" in the seventh sentence on page 4. From the map it
seems that the "northeast region of the site" could be around well, CWM-009, which
shows the groundwater flow direction to the southeast. This docs not coincide with th~
explanation in Section 5.0; therefore the flow direction depends on your point of
reference. Please clarify this discussion in Section 5.0.
4. ln the last paragraph in Section 7.0, the last sentence states that well, MWD-002, is
"screened to 27.5 feet BGS". This does not coincide with Table J, which lists the
screened interval for MWD-002 as 17 to 27 ft. BGS. Please clarify this discrepancy.
If you have any questions or comments, please contact me, at [phone], extension
299.
cc: File
Sincerely,
~4£~~
Kyle R. Hagen
Environmental Engineer
NC Superfund Section
• •
January 8, 2004
Memorandum
TO:
From:
RE:
FILE
·1/ /
Kyle R. Hagen tv/2-t(/-
Environmental Engineer
NC Superfund Section
Overview of Remedial Action Qua11erly Sampling
New Hanover County Airport Burn Pit
NCO 981 021 157
Wilmington, New Hanover County, NC
On January 7, 2004, two representatives of the NC Superfuncl Section
provided overview of the quarterly groundwater sampling for the pulsed air sparging
system at the New Hanover County Airport Burn Pit Superfund Site, located in
Wilmington, North Carolina. Met with Rick GaJTett and Bill Walsh of Catlin
Engineers and Scientists and one New Hanover County Health Department
representative and toured the site and the pulsed air sparging system. Observed the
air sparging system during nonnal operation in the Zone 8 wells. Observed the site
drainage and overland flow pathway. Observed Dimitri Talbert of Catlin Engineers
and Scientists collecting parameter readings and volatile organic samples for the
monitoring well labeled CMW-013.
A/s.D
NC Deputrnrn: of Environme11t,
HulU1, & N~rural RelOUrces
Solid Wute Mrn.acemenl Divi&ion
• SAivll'LE A.1'-IALYSIS REQUES' St.ate Labor.,,lory of Public Hu.Ith
P.O. Box 28047, 306 N. Wilmington St.
d'r Name of Site N<-w l\t'1il~"~l:: Co,. t\-hp.--it
SiteLDc:ition if«.i( br. ¢ &-anj ;19,y ))y,
Ra!eiJe:h, Nonh c.rolinl 27611-8047
Samplc!DNurnbcr/Namc r t4 ('2./{)C:,2_ ~ 2/0C:,3).
Date Collected I I 121:iio RECFI\/Fn Time //: 0 5 Ml . ; . ' -· -
Agency: Hazardous \Va.9te Solid Waste __ Superfund• NOV 2 O 2fJL~LP Compounds
Sample Type
Environmental
Ground Water (I)
Surface·Water (2)
Soil (3)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other ( 4) Other (8)
Comrnent5
SUP ~~§9n1pouncis
a.rsen1c
barium
cadmium
chromium
ie.1d
mercury
selenium
silver
Rcsulls(mg/1)
Organic Chemistry Inorganic Chemistry
P:1..r:m1eter
_./ P&T:GC/MS
Acid:B/N Ext.
2,4-D
2,4,5-Tr.:silvex)
chlordane
heptachlo,
hexachl oroben.z.eoe
Rcsulls (mg/I)
-------hexachlorobu"tad ieoe '-------endrin
lindane
mcthoxychlor
toxaphcne
L ~02 D~'-'=~----
· FOR LAB USE ONLY
Date Received //'-3-0 0 W&--
Date Reported ~N.~O~V ~0-.,.9,.2;\;IIOOm0'----
006039 · Lab Nuinber
l'i-oq~t5_°J1~ t;()6b/f2--~Hs"J.1.~r:-·(R~:--iscd ·12193),.-:._·_-.-·::." ::·~·:.. · ---.'
Parameter Resl!lts(mg/l)(mg/kg) .
antimony
arsenic
barium
beryllium
cad mi urn
chloride
cluomium
cobalt
copper
fluoride
iron
lead
manganese ______ _
mercury
nickel
nitrate
selenium
si!v~r
sulfates
thallium
vanadium
z.inc
pl-I
_conductivity ______ _
TDS
flash point
Organic Compounds
kn2ene
carbon tetrachloride
chlordane
chloroben.z.ene
chloroform·
o•cresol
m-cresoJ.
p-cresol
ere.sol
1,-~-dich..lor°obenz.ene
l ,'.2-dichloroetha..ne
Rcsults(mg/1)
I, 1-dichJoroethylene ______ _
2,4-dichloructhylene ______ _
hcptachlor
hexachloroben7...cne
hexachJorobutad iene
... hcxachloroe!haue
methyl ethyl ketone
nitroben.unc
penL.1.chlorophenol
pyridi.Jic
tetrachlorocthylene
trichloroethylcue
-------
2,4,5-trichlorophcnol_c_ ____ _
214,6-tricWoropbcnol_--'---~--
vinyl chlori~e
er.dri.n
!U1da.ne
me.thoxychlor
toxap_hene
2,;-D
2,4,5-TP (Silvcx) . ·
NC Department of Environment,
Hu.!lh, & Natuul RC.wurcci.
• SAMJ'LE A.i'l'ALYSIS REQUES, Sutc Ulbomory of Public Heallh
P.O. Box: 28047, 306 N. Wilmington St.
Solid Wut.e Muagcmenl Division Raleit;h, North Carolina 27611-8047
SiteNumber NC.D 't'i? \ 02. J I '5 7 Sample ID Number/Name T-/ j (2./ 0 (,4 ¢ 2/0b5)
Name of Site New \kia&v~'c: Cc, [\1 ,pcl Bcx/1follecte<l By ST v-«S,:;t p~-uy-ID# ____ _
SiteLocation £kif })y ? ?.,,,.,!fll,.IY ])-,,-DateCollecte<l / //;a/4'0 ' • • Time 12 i.4-7. Pm
Agency: Hazardous Waste Solid Waste __ Superfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environment.al Concentrate Comments arseruc -barium -Ground Water (I) Solid (5) cadmium ---chromium -Surface Water (2) Liquid (6) lead ---
-mercury
Soil (3) Sludge (7) selenium ---silver -Other (4) Other (8) ---
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/I) Para.meter Results(mg/l)(rng/kg) . Organic Compounds Results(mg/1) _,L' P&T:GC/MS antimony -benzene -Acid:B/N Ext. arseruc carbon tetrachloride ----2,4-D barium chlordane --2,4,5-TP(Silvex) beryllium chloroben..zene ---ch!o'rdane cadmium chloroform ----. heptachlor chloride o-cresol --hexachloro benzene -chromium m-cresol --hexachlorobu·tadiene cobalt p-cresol ---
-endrin copper cresol ---lindane flU<;>ride 1,4-dichlorobe11zene --
-methoxychlor. iron 1,2-dichloroethane --toxaphcne lead I, 1-dichJoroethylene --L <i,©2 12rg,5 manganese 2, 4-dichloruethylene ----mercury beptachlor ---nickel hexachlorobenzene -
'
.-nitrate bexachlorobutadienc --sclenjum ~ hexachloroelbane ---silv~r -methyl ethyl ketone
FOR LAB USE ONLY sulfates nitrobenune vJ(/ ---
I I -3-thallium pentachlorophenol .. D tJ ---Date Received vanadium pyridtne --zinc tetrachloroeth y lene --Date Extracted pH trichiorocthylene --
.
//-'jf-6l) ·1K1J-=' -_conductivity -2, 4 ,5-trichlorophenol
Date AnaJy.zed TDS 2, 4 ,6-trichloropbcnol --•.; flash pomt vinyl chloride -
Report~ By --
· endrin ' .. --
--lindane
Date Reported . methoxychlor 006040 --
-toxaphc0e
ub· Number -~ 2,4-D --.. ·;:--2,4,5-TP (Silvcx) DHS·fl9l•(Rc!vised 1219.3) . -
' . "'
NC Department of Environment,
Huhh, & Natural Re,ource~
Solid Wute Man.agcmcnt Divi,ion
• SA.tvll'LE At'IALYSIS REQUES. · St.ate Laboratory of Public Heallh
P.O. Box 28047, 306 N. Wilmington St.
Raki!Jh, North Carolina 27611-8047
SiteNurnber NC D q~ / 02. I 157 SampldDNurnber/Narne T2. B(~?/f>h(o f 2 /Ofn7)
Name of Site N f.VJ fln_w,yey C<2. Al ,(>.;t:&,..,P•'&nected By ST v,vq-Me:,-· ID# ' -. T ~~ /Vkl=t'\le'elii ~------
SiteLocation ·~.r1..,~II\IA1ew H-aitii+\1'1,Y cc> DateCollected 11/;z./oo Tirne_f,:!3•:,:~2 ' • ' . • -~ I 6,-0,,,r'J'\,"'./y b'l", I Ho-l,I
_Duperfund Agency: --Hazardous W a,te Solid Waste TCLP Compounds --
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments arseruc -
-barium
LGround Water (1) Solid (5) -cadmium -chromium -Surface Water (2) Liquid (6) -lead --
-mercury
Soil (3) Sludge (7) selenium ---silver -
-Other (4) -Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Parameter Results (mg/1) Parameter Results(mg/l)(mg/kg) . Organic Compounds Results(mg/l)
-~P&T:GC/MS -antimony -benzene
-Acid:B/N Ext. -arsenic -carbon tetrachloride
-2,4-D barium chlordane --2,4,5-TP(Silvex) -beryllium -chloroben.zene -chlordane cadmium . chlorofom:l ---
-heptachlor chloride o-cresol --hexachlorobenzene -chromium m-cresol ---hexachlorobu'tadiene cobalt p-cresol ---endrin c~pper cresol --
-lindane fluoride 1,4-dichlorobenzene ---methoxychlor -iron 1,2-dichloroethane -_ toxaphene -lead 1, 1-dichloroethylene Z l,02-orkc. -
-manganese -2, 4-dichloroethylene
-mercury -heptachlor
--nickel bexachloroben.zene --nitrate hexachlorobutadiene --selenium ~ hexachloroethane --
-silver methyl ethyl ketone -FOR LAB USE ONLY --sulfates nitrobenune -
// -3-Do w~ -thallium penlachlorophenol -Date Received vanadium pyridine --
-zinc tetrachloroethylene -Date. Extracted pH trichloroethyleue --
n1Jr -conductivity -2, 4 ,5-trichlorophenol
Date Analyzed ll-x:-6D -TDS 2, 4 ,6-trichlorophcnol -
-fla.sh point -vinyl chloride
Reported By endrin ' --
-lindane -Date Reporte<l methoxychlor ---006041 --toxaphene.
Lab Number 2,4-D ~ --
--2,4,5-TP (Silvex)
DHS 3191 (Revised )2/93)
.
NC Department oi Environment,
Hu.Ith, & Natural R~i.ourccs
Solid Wule Man .. gement Division
• SAlvll>LE A.1'1ALYSIS REQlm,S' SU.re La_boratory of Public Hc.ah.h
P.O. Box 28047, 306 N. Wilmington St.
Ralcii:h, North Carolina 27611-8047
Site Number N c.D jJi' \ 02. ( l'57 Samplc!D Number/Name Tr-i p Sla-w~ s (?1 oroi fZ/069}
Name of Site _,/\..,\ce."-'v.J=-.:.~=""n"'""'~t:L.>:Cc"'--!C, &I..Ll., 't,if"''""-it'-"--"B"'-,,.,-,_,,,_Pffollccted By _S=-..,Tc,cv-<:V...:.::c;(,:_··,,__.1.P.:::cv4.e!..ll'::c<c""'Y.,_ ____ ID# _____ _
iktl j)y t &-o,nl,i-,<Y )')y SitcLocation ' ' '
DatcColl,,;,ted / //:i!./&io Time //.' ('5 A-M
Agency: Haz.ardous Waste --Solid Waste __ Superfund TCLP Compounds --
Sample Type Inorganic Compow1ds Rcsults(mg/1)
EnvironrnenL1l Concentrate Comments arseruc -
barium -Ground Water (I) Solid (5) cadmium ---chromium . -Surface Water (2) Liquid (6) -l"'1d --
-mercury
Soil (3) Sludge (7) selenium ---silver -Other (4) --Other (8) -
-
-Organic Chemistry Inorganic Chemistry -
Paromctcr Results (mg/I) Parameter Rcsults(mgii)(mg/kg). Organic Compounds Results(rng/1) _L P&T:GC/MS -antimony -benuoc
-Acid:B/N Ext. arsen1c carbon tetrachloride ---
-2,4-D barium chlordane ---·
-2, 4,5· TP(Silvex) -beryllium --chloroben.z.cnc
-chlordane cadmium chlorofom1· --. heptachlor . -chloride o-cresol --hexachloroben.zene -cluom.ium m-cresoJ. ---bcxachlorobu.tadiene cobalt p-cresol --
-endrin copper cresol --
-lindane fluoride 1,4-dichlorobenzeoe ---methoxychlor -iron -1,2-dichlorocthane
toxaphene -lead 1, l ·dichloroethyiene L (Qe)Z. or~' -. -manganese -2, 4-diehloroetby Jene
--mercury -heptachlor
-nickel -hexachlorobenzene -.--nitrate hexachlorobuL1d iene -selenium -~ hexacWoroethane -
-silv~r -methyl ethyl ketone
· FOR LAB USE ONLY sulfates nilrobcnzcne --
lf-OJ-ooW(y --thallium penlach..lorophenol -Date Rccci ved vanadium pyridine --
-1_mc tetrachloroeth y !enc
Dat~ ·Ex.t.racted -
-pH -tricWoroethylcue
J/-9-olJ 101 -· __ conductivity -2, 4 ,5-trichlorophcnoi
· Date Analyzed TDS 2, 4 ,6-trichlorophenol --.... , .. flash point vinyl chloride
Reportt1By -,_ -
. . . ' cndrin .. .-, . --
--li.nd.ine
Date Reported -rncthoxychlor
006042 -
-.-toxaphene
Ltb Number 2,4-D
I
·._ ... ... --.. ·:, . 2,4,5:TP (Silvcx) ,,:-: :.,.·.··· ' • ..... .. ,. ¥ ,. ' '· . . --.. ·-. ,·-,· : ~-.--. ·, :It;• . OHS 3!91 ffiev1sed ].,./93).
.,C-()EH,,R
')ivi_;).{;;1 (l.f $o{id \Vaste Management
f0" Supcrfund Section
D Hazardous \Vastc Section
D Solid Waste Section
• 8rganits i~~il): ~ • Inorganics Lab: __ _
CHAIN OF CUSTODY RECORD
Project Name: New ~ev: Co, A:hAeYT &rot p;
Site JD# (NCD#) 9PI 02 I I 157
Location: Ha ti DY-. ( G-<tJrn~-r Pr, _
Address: w:11ny~/N:-e..w H:o,,.i cv~r C.,cluMy
Sampled by:__,S==''~;fi~v!.Q:!.~_L~~~05,~~~a:i~
Sampler ID 7?-z --1-=------=c-='-;t'--~~--~,------"--4---Telephone: ('I 1'1) 7 3 3' .2. 2 C X34-/
Date Sampled: oo
Time Sampled:
Sample Types: Soil Water V::::: Waste Other
:"""""----------~~---------------------"" i Relinquished by:_.£."..1.1.:Jl~lGcl-G,,~sl:::>:~'::'l.\.------Date: 1//o">jUoo Time:~
! (Signature)
.• Received by: -------/YI:~ C -~ --.n ---------. ---Date:/J /oi/20 -Ti me:--/0 :/Q1t7,,._, ----
• (Sigj1ature) . _. _ . =r . ~ . • .
/ Relinquished by: ______ ~-------'---Date:___ Tinie: . I
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(Signature)
I - -_..: .. __ -------------------------------• ____ • ------------------- - - - - - - - - - --------- - - - - - . -------------------.-. -----------------------------------
Received by:. ----~------------Date:· ----Time: -----
(~ignature) ·
Relinquished by: _______________ _
(Signature)
Date: __ _ Time: -----
;_.: ------· _· -----. -------------··---· -------··: . ----------_.;·:.:.::::..:. --~ :.·~ ---_ : ______ -----------~ ----------------_· ___ ------,----------------------------i' Received by: Date:_~--Time: ____ _
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(A\COc:'1i .. i•1w).
.ATE LABORATORY OF PUBLIC~
PO BOX 28047 -306 N. WILMINGTON ST .• RALEIGH, NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLE COMPOUNDS LAB NO lillfn0':°3CJ C<Ju()LJD COlo0 1.J-I c:()([>0 4-;;;).
FIELD NO t-/4--r-11 ,.J.B rn 'f' BlelYJi:.
COMPOUND TYPE ( ) ( ) ( ) ( ) (
t ~ti1 eppm ~ ppm 9ppm ~ppm ppb
CHLOROMETHANE :;..o i I
VINYL CHLORIDE
BROMOMETHANE
CHLOROETHANE
TRICHLOROFLUOROMETHANE
I ,
o.5 \ /
1,l•DICHLOROETHENE
ACETONE :Z,O rJ. ;J. :r,C-
IODOMETHANE 0.5 I ,
CARBON DISULFIDE
METHYLENE CHLORIDE
ACRYLONITRILE
TRANS·l,2-DJCHLOROETHENE
METHYL-t-BUTTL-ETHER
1, l·DICHLOROETHANE
ISOPROPYL ETHER
CIS-1,2-DICHLOROETHENE . , ' /
2-BtrrANONE .;z.o ri ·o.:.,c..
TETRAHYDROFURAN -} d I -
CHLOROFORM t),5
1, l, I-TRICHLOROETHANE
CARBON TETRACHLORIDE
BENZENE
1,2-DICHLOROETHANE
TRICHLOROETHENE
1,2-DICHLOROPROPANE
' . / DIBROMOMETHANE "
Possible lab contamination or background
Estimated value
-
I l I ' i I
...._ / ' / ' /
,~.9,' .5.8 :l,'--(p. 5;r,c.,
U-u.-I '
+.ace~
i J
,j ·, ,.
1g;9 .:L,5
/ A IA-
./--m r,O
I A -' I '-I
.3,0r,c.. ;/.3s,c J' 1.fJ,C..
il I, -2.~
I 1
'\ I I I
q.'] o7. I
I , -l-f'aL€-
I '
I ' '
C-
J -
K -
L -u -
NA -
l./ -
D -
Actual value is known to be lees than value given.
Actual value is known to be greater than value given.
Material was analyzed for but not detected. The number
Not analyzed.
is the Minimum Detection Limit.
Tontative identification.
SAMPLE DILUTED. MDL'S DO NOT APPLY.
DHHS 3065-1 (1/98)
<D
) ( )
ppm ppb ppm
PURGCOM2.0RC
.. ATE LABORATORY OF PUBLIC m:AH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLE COMPOUNDS LAB NO Ol¥P039 "Y'llnOLJO CX)u,Ol.fl 00 (pQI.I:)
FIELD T-1'-f-t-11 T;)_.B Tr I 'f}J/a nJ:.
NO
COMPOUND TYPE ( ) ( ) ( ) ( ) (
1 ~~)1 C§vppm @ppm cii9 ppm (§) ppm ppb
BROMODICHLOROMETHANE 0.5 I I -i J
CIS• l ,3-DICHLOROPROPENE I
4.-METHYL-2-PENTANONE -1/
TOLUENE /, 0
TRANS-1,3-DICHLOROPROPENE I I
l,l,2-TRICHLOROETHANE
TETRACHLOROETHENE
2-HEXANONE
DIBROMOCHLOROMETHANE
ETHYLENE DIBROMIDE
CHLOROBENZENE
l,l,l,2-TETRACHLOROETHANE ' I
ETHYL BENZENE d•~
XYLENES I. '7
STYRENE / J
BROMOFORM
1, 1,2,2-TETRACHLOROETHANE
1,2,3-TRICHLOROPROPANE -
1,4-DICHLOROBENZENE
1,2-DICHLOROBENZENE ' I
l,2,-DIBROM0-3-CHLOROPROPANE :i,.o ·, , ' /
.e:;u.h"'-J-/.f,,-).,,,.J ,L _" ,...,, ®}9 G (+)
C -Possible lab contamination or background.
J -Estimated value
K Actual value is known
L -Actual value is known
U -Material was analyzed
NA -Not analyzed.
to be less than value given.
to be greater than value given.
for but not detected. The number is
1/ -Tentative identification.
D -SAMPLE DILUTED. MDL'S DO NOT APPLY.
DlllIS 3065-2 (1/98)
I l /J
., +,..;;, ,0
I I
' /
() '"' {J. '7
I I
,/ \ /
(fj ( )
the Minimum Detection Limit.
(J)
) ( )
ppm ppb ppm
Ml)L
PURGCOM2.ORG
•
DATE:
TO:
FAX#:
FROM:
RE:
NORT.AROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
FAX TRANSMITTAL RECORD
R°""'&J M,Ehiee_v\
AV\_~ 'to c,J K--e :s 0 I ts
N·e_lu ~o-\.Je...Y
Superfund Section
Number of pages (including cover)
Comments:
Confirm receipt of document(s):
--------~ Superfund Section [phone], ext. __
SF/slb(C:IWPWIN601WPDOCSISFISF-FAX.FRM) utm ••·-••·• 1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUJTE 150, RALEIGH. NC 27605
PHONE [phone] FAX 9\9-715-3605 AN EQUAL OPPORTUNITY/ AF'FIRMATI\IE ACTION EMPLOYER -50% RECYCLED/10% POST-CONSUMER PAPER
.. -.. ' ; .
'·:id ~ P.. :,-•l B .. ·.~ ;: .:J: 1 .•· ·:-'\
. ---''' -;
~
~-.
•
DATE:
TO:
FAX#:
FROM:
NORT.AROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
FAX TRANSMITTAL RECORD
1«2~/2@a>(J)
~'~/ I),~ &s~ '"
K0v~ /:i,,c El\1-e_--Qy'\ . Superfund Section
RE: l\)..QJJ.J ~\J\.€>1..le_ --r C.O. fs:~ ~ f~\ ts 0-1' 'Ii\ ?~ t
P---1AoJ-.1t,ic"'--f ~svl~ 1-2-B 1 "T-ll, ( T-14
Number of pages (including cover) _Q=·-· __
Comments:
Confirm receipt of document(s):
--------~ Superfund.Section [phone], ext __
SF/slb(C:IWPWIN60\WPDOCS\SF\SF-FAX.FRM)
1646 MAIL SERVICE CENTER, RALEIGH, NORTH CAROLINA 27699-1646
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AF'FIRMATIVE ACTION EMPL.OYER • 50% RECYCLED/10% POST•CONSUMER PAPER
TRIP Jvl,.IFICA TION AND A VTHORIZA nl FORM
Program: D Federal D Brownficlds
g~
b:J'NPL/DOD
□ MPG
D Dry Cleaners
Site Name: e u-rn
ID Number:
Street Address:
City:
County:
Date(s) of Trip Trip Canceled: Trip Rescheduled (Date):
&oo
Reason For Trip: G "r"-<J.,.J\\..k.}<?:ct-e-v So.,vw /-es 3 I.,"-.) e_ll::, i"-'L\'tvv-1 <M:.//s -=-----=~'--'---'-;-:-,-----;-:------;--''-;----:----;--:---;---,------'t---+-( if sampling, check appropriate boxes below)
D Surface Soil
D Subsurface Soil
D Using Augers/Shovels to collect soil
D Using Little Beaver to collect soil
D Groundwater ( from tap)
Project Team Leader · Assistant
R a-,1, t~ 11\,\ [ E\ "e_,(l 'ST-e.u..>co.,::t PC!,//
I .
Authorized By:
D Groundwater (bailcrs)
~ndwater (pumps)
D Surface Water
D Sediment
Assistant .
,e,\--
I/J /7
Wdustrial Hygien~re
0 "fice,Usec,Onlyi,;;;::iU'.,,,(i ·'
CciirntyHealth Departm·ent Official C:ontac( ·: .. 'I':','',"' ·_·_'."_:·•: "' .•,,·; ... ,
· ··•·.·.· ... · .· . . . ·. . > .· JL(3. Ii tie: <.
IPho?e Nwnber: .. • ·· ... ('i.LQ__) 3:H' 4 3.(9,..tit{J.,, ''i'~;.v:'Ur«l/d
Health Department Official Contact.ed: y~5 ··• .. ~~~K,Yft~~:r ~Tq~i~eg?: · ' ·, ·-. ·, . ,, ·:·'I)tl,1ti.. /,.~ ,,, _-_ / , .. , ,, ' i;·,;,,,,, .. ,,,,1,,: ,.:t/·l": ,.:, ., ·,c, ,:·1:, .",•.,•,,': ... s, '"',;
Notes: 1,: ,A ,v (( 1//,.c)':.c;cl, 1/-)Ll L.
DUs/b(TRIP_NOT _ A UTJI.FRM)
Assistant
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Yes " /·No v--
Revised: 813100
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i
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
June 7, 2000
Memorandum
TO:
Through:
From:
Subject:
Dr. Ken Rudo, Toxicologist
Occupational and Environmental Epidemiology Section
Jack Butler, Chief
Superfund Section
Grover Nicholson, Branch Head
Environmental Engineering Supervisor
NC Superfund Section
Health Risk Evaluation Request
New Hanover County Airport Bum Pit
NCD 981 021 157
Wilmington, New Hanover County, NC
Please find attached a copy of the laboratory analyses for well samples collected by
the EPA Region IV around the subject site. Since these samples were collected from
private drinking water wells, the Superfund Section requests a health risk evaluation
and a recommendation on the continued use of these wells. This information will be
provided to the affected well users. If you have any questions regarding this matter,
please contact Randy McElveen or me at 733-2801.
Attachment
cc: File
Donna Keith
Randy McElveen, N.C. Superfund Section
. 401 0B E;RLJN ROAD, SUITE 1 SO, RALEIGH, NC 27605
PHONE:[phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER• 50% RECYCLE;D/10% Pos,T-CONSUMER PAPER
• • POTABLE WELL SAMPLING INVESTIGATION, 1/17-20/2000
NEW HANOVER BURN PIT, HERlTAGE PARK SUBDIVlSlON, WILMlNGTON, NC
)~1(u{
Table 1. Sample and Resident Information
·.itt\:sA&iilf Eti.OMi'i'.Eif: .-,-,,:,,,:,,: _' }}n:;'Iu:·~ n.~;;~:tN~ii~~3:.~ n ~~}IG{l~.f :1:: rt?~ Fffi:\Wiii>'llli'.s s '.tH;;;ttNU :-i:):tr:: ... ,
HP-00 I -PW English I 06 Bcnnutla Dr,
c✓' llP-002-PW Tryer 113 Bem1Uda Dr.
v r]{p.QQJ-PW Futch 114 Bermuda Dr.
y· HP-004-PW Robeson 118 Bermuda Dr.
HP-005-PW McKov 200 Bermuda Dr.
HP-DOG-PW Wilson 20 l Bermuda Dr.
V l·IP-007-PW Roland 230 Bermuda Dr.
HP-008-PW Hammes 2524 Castle Hayne fui ,,t, HP-009-PW Mav 2528 Castle Havne Rd. '
!,,-:--rn,,oio-rw Russell 110 Heritage Park Dr.
/ Hl'-01 I-PW Brock 114 Heritage Park Dr.
HP-012-PW Harrell 117 Heritage Park Dr,
HP-013-PW Miller 117 Heritage Park Dr.
\ _ _..,.-"Hl'-016-PW Withcrsnonn 142 Heritage Park Dr.
Hl'-017-PW B:imes 205 Heritage Park Dr.
HP-018-PW Garris 210 Heritage Park Dr.
HP-019-PW Howlett 217 Herilaee Park Dr.
HP-021-PW Prince 222 llerita~e Park Dr.
HP-022-PW Lanier 226 Heritage Park Dr.
HP-023-PW Gcr!!anOUS 230 lforitage Park Dr.
HP-024-PW Mathis 233 Heritage Park Dr.
HP-025-PW Wood 202 Heritage Park Dr.
HP-026-PW Swart 127 Pilgrim Circle
HP-027-PW Skipper 136 Pilgrim Circle
HP-028-PW McKov 139 Pi!griin Circle
HP-030-PW Lee 202 Pilgrim Circle
HP-031-PW Worlev 210 Pilgrim Circle
HP-032-PW Slaecr 217 Pilgrim Circle
HP-034-PW Baker 230 Piluitn Circle
HP-035-PW Gregory 243 Pilgrim Circle
HP-036-PW Neher 121 Spring Rd.
"" 0
0...
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2
Table 2-A. Rcsulu ofVolatile Organics Sample Analysis -Detected Compounds
Cis-.l.2-Dichloroethene µg/L 70 u u u u u Tetrachloroethene µg/L 5 u u u u u (fctrachloroethyle,ie) • Trichloroethene µg/L s 0.5 J 1 1 u 0.7 J (frichlorncthylcne)
Unknown µg/L u u u 2 J u
Cis-1,2-DichJorocthene µg/L 70 sRR-i 051 u lJ u
. Tetrachlorocthcne µg/L 5 0,7 u (T etrachl oroetJlj'lene) 2..L u • Tric-Woroetliene µg/L 5 2.'? 2 2 u (Trichloroethy!ene) Z.L
Unknom1 µg/L u u u 2J
,. ·t·
'·. DaLi_::~ri6-s: U -¼terial ""' ann.J;zoo for bur 110r dereclo:l, J -Estimarad Value
ill
0
Q_
" 0
0
0 z
N q.
0
''l 0
"
;:1· ..
!
lf)
>-a: :,::
i :o ,z
C =:,
Cont.
Aluminum
.ArS(:Il.lc
Barium
lkryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
lmn
uad
Magnesium
~anese
Potassium
Selenium
Silver
Sodiwn
Tiialliurn ~.
1,g/L
µg/L 50
µg!L 2000
4
µg!L ;
µg/L
µg!L 100
µg/L
µg/L TI~i
µg!L
µg!L Tl"'
µg/L
µgfL
µg!L 1 ()()C'l
µg!L
µg!L 50
µg!L
µg/L
µg/1.
u u u
u u u
32 24 28
u u u
u u u
86000 57000 81000
2 4 l .5 u
u u u
34 120 15
81 3700 260
u u u
2600 1400 2800
4.S 19 3.3
2 ; 12 u
1000 820 1100
u lJ u
u 0 lJ
12000 llOOO 12000
u u lJ
1 liil1ik1-,.-:-:-~-,:~,,'::_n_=_y_--+-:-=g/'-'.-------+-
2
-------+--------+-------+•-
u lJ lJ
(J u lJ
160 350 52
u u
u u
u 25
u u
u u •
3400 65000
u 2.1
u u
14 20
72 580
u 2.8
160 ]900
1.2 8.4
1.6 u
110 830 • u u
u lJ
62G()() 9100
7.8 u
lJ u
u u
)5 63
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
~".;, ?:' lli1.I ,, .. ; April 11, 2000
Mrs. Diane Barrett/ Ms. Beverly Hudson
~ ,, .~,
.'>,-o:
-,-:-
, . ., ,.. Mlt8 e: HUNT.J
OR
.
::,.-~--·:,,. :"0:: .·i·
·" •9
EMCDEVI ' RETARY ·· • ~ <ii~-. cf('). ,.
<> o,g • 0 'rJ'
0 ~ .',l,J1:;"o
LIAM L, MEYER~ ''.It" ECTOR d'T\:l
0
....
. . '
• <O ~ 0
~'l~
ei~ ~ a O Q
• ' ,I),, 1l"»•S
North Superfund Remedial Branch
US EPA Region IV
61 Forsyth Street, Eleventh (I I) Floor
Atlanta, Georgia 30303
RE: First Set of Analytical Results of Surface Water in the Vicinity of the Burn Pit
Site
New Hanover County Airport Burn Pit
NCD 981 021 157
Wilmington, New Hanover County, NC
Dear Mrs. Barrett and Ms. Hudson:
Attached please find two copies of the analytical results from the January 21,
2000 sampling event completed by Russ Colby with the NC DENR Division of Water
•· Quality, at the New Hanover County Airport Burn Pit Superfund Site, located in
Wilmington, North Carolina. Mr. Colby collected these samples without the
knowledge of the NC Superfund Section. When I discussed this with Mr. Colby he
indicated that he was in the area and chose on his own to collect a set of samples in
the areas that were agreed to be most representative the week before. I discussed with
him the sensitivity of the situation and he apologized. He also stated that he almost
always collects more than one set of samples from a site on different days.
As you can see all analytical results for contaminants of concern (COC) and
volatile organic compounds (VOCs) are non-detect (ND) except for bis(2-
ethylhexyl} phthalate at 17 ug/1. The surface water standard for bis-phthalate
defaults to the detection limit (I 0ug/1) since no numeric standard is listed. The
NCAC 2L Groundwater Standard for this contaminant is 3ug/l. As is noted on the
last sheet of the Laboratory Data Sheet for BP2, phthalates are common laboratory
contaminants. Since the laboratory reported the results as in compliance with
regulatory standards it was the labs opinion that this semi-volatile organic
0 contaminant was a laboratory contaminant. I verified this with Mr. Colby and with
other Chemists in the Superfund Section.
Bis-Phthalate was only detected at sample location BP2 located in the ditch on
the northeast side of the intersection of Hall Drive and Gardner Drive. This sample
location (BP2) was not collected during the 3 February sampling event since Mr.
Skipper requested a different sample location in the area off of Hall Drive. The
primary purpose for bis-phthalate is for use as a plasticizer in vacuum pumps such as
those used in a laboratory. It is also used as a plasticizer for rubber products such as
401 OBERLIN ROAD, SUITE 1 SO, RALEIGH, NC 27605
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER -50% RECYCLED/10% POST-CONSUMER PAPER
• •
rubber gloves used by environmental samplers. Therefore, it 1s not a suspected
contaminant of concern at this Site.
If you have questions about sampling locations or other details about the
sampling/analytical results, please contact me, at [phone], extension 341. Copies of the
attached analytical data was mailed to local residents who were present during all or part of the
sampling event and also to Bessie McKoy and Sharon Mathis who requested copies by phone.
Sincerely,
Randy McElveen
Environmental Engineer
NC Superfund Section
cc: Grover Nicholson, N.C. Superfund Section
Linda Russell, 110 Heritage Park Drive, Wilmington
Bessie C. McKoy, 139 Pilgrim Circle, Wilmington
Sharon Mathis, 233 Heritage Park Drive, Wilmington
Teresa Prince, 222 Heritage Park Drive, Wilmington
Charles M. Skipper, 4924 Woodcrest Drive, Castle Hayne
NOF<TH SUPERFUND
. ·~. .
ID: MRY 15'00 10:39 No.004 P.02
4SESU-Ell3
u s4'ivmoNMENTAL PROTECTION AINCY
REGION 4, SCIENCE ANl) ECOSYSTEM SUPPORT DIVISION
ATHENS, GEORGIA 30605-2720
APR 1 7 2000
.MEMORANDUM
SUBJECT
I'ROM
TO
Results of Potabk Well Sampling Investigation
New Hanover .Hurn Pit, Heritage Park Subdivision
Wilmington, NC
SESD Project No. 00-0235 / / ,
Ar~hie Lee, Chief ~
Superfund and Air Section
Beverly Hudson, RPM
North Site Management Branch
Waste Management Division
During the week of Jftnuary 17, 2000 personnel collected 3 J samples from potabk wells
in the Heritage Park Subdivision located near the New Hanover Burn Pit Site in Wilmington, NC.
Sample identification numbers, residents' names and addresses and are listed in Table]. Tables 2-
A and 2-B report a summarized version of the laborato1y results provided in Appendix A Only
results for dete~ted compounds were included in these tables.
The 31 potable wells sampled contained no organic or inorganic co11tami1rnms above the
maximum contaminant levels (MCL's) All preservative and trip blanks were free of
contamination.
If y1,u huvc any questions or comments, please call me at 706/15 5-8623
Attachment
ry,:; /)
r✓ORTH SUPEF,FUND iD: MRY 15'00 10:40 No .004 P.03 • •
POTABLE WELL SAMPLING INVESTIGATION, 1/17-20/2000
NEW HANOVER BURN PIT, HERITAGE PARK SUBDIVISION, WILMINGTON, NC
}Y/(ul
Table 1. Sample and Resident Information
?i:•·tr:sAhlI!i:.i(~.tiMBIBli]ff Xttl :-n}t~:~ ~}~ ~i~~rJtN~i~~;u n mnti :s;t ·:·,-·;:··,: '\\C::\(£1>iilisS"':F,'hiU:; .,.,.,:,., .. ,
,·; ~ ;.:,' ::·: ';:;', '. )' ,: ~:;, · . ,:_.~•~ i, t\.>t~ ~-1·1~:'f~'
HP-001-PW English I 06 Bcnnuda Dr,
,· c-' HP-002-PW Tryer 113 Bemrnda Dr.
v rill'-003-PW Futch 114 Dcnnuda Dr.
V .HP-004-PW Robeson 138 Bermuda Dr.
HP-005-PW McKov 200 Bcnnuda Dr.
HP-DOG-PW Wilson 201 Bermuda Dr.
V HP-007-PW Roland 230 Bermuda Dr.
HP-008-PW Hammes 2524 Castle Havnc Rd. 4, HP-009-PW May 2528 Castle Havne Rd.
/,,,-Hti>.OJO-PW Russell I 10 Herita2e Park br.
/ HP-OJ I-PW Brock 114 Heritage Park Dr.
HP-012-PW Harrell 117 Herilll•e Park Dr,
HP-013-PW Miller 137 Hcritaec Park Dr.
I · -HP-016-PW Withcrsooon 142 Heritage Park Dr.
HP-017-PW Barnes 205 Herilllee Park Dr.
HP-018-PW Garris 210 Herita•e Park Dr.
HP-019-PW Howlett 217 Hcritaee Park Dr.
HP-021-PW Prince 222 llerita~e Park Dr.
HP-022-PW Lanier 226 Hcritaec Park Dr.
HP-023-PW Gcrv;inous 230 llerita2e Park Dr.
HP-024-PW Mathis 233 Heritage Park Dr.
HP-025-PW Wood 202 Heritaee PRik Dr.
HP-026-PW Swart 127 Pilerim Circle
HP-027-PW Skinner 136 Pilgrim Circle
HP-028-PW McKov 139 Pileri1n C1rclc
IIP-030-PW Lee 202 Pileri,n Circle
HP-031-PW Worley Z!O Pilerim Circle
HP-032-PW Slaecr 2 I 7 Pikrim Circle
HP-034-PW Baker 230 Pil2rim Circle
HP-035-PW Grc2orv 243 Pil~rim Circle
HP-036-PW Neher 121 Sn ring Rd.
\
q
0
Q_
q
0
0
0 z
0
q
0
~
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2
Table 2-A. Remits ofVolatile Organics Sample Analysis -Detected Compounds
Cis-L2-Dichlorocthene µg/L 70 u u u u u
Tetrachloroethene µg/L 5 u u u u u
(f etrachloroethylene)
Trichlorocthenc µg/L 5 0.5 J 1 u 0.7 J
(f richlomethylene J
Unknown µg/L u u u 2 J u
Cis-1,2-Dichloroethene µg/L 70 0.5 J u lJ u
Tetrachloroethenc µg/L 5 u u
(T etrachl oroethylene)
Trichlorocthene µg/L 5 2 2 u
(T richloroetbyknc)
Unknov,,11 µg/L u li u 2J
Data Qualifiers. U -:½lterial v.as annl )200 for but ru,t dctcrted, J • Estimared Value
(I) Reference for the Primary Drinking \Varer Standards/MCL 's: 1Av.'•J,:.cp2..gov:OST!fu0-ls/fr,:st.:l.:s.h.d., US EPA Offiu of V/ata.
ln
0
Q__
q
0
0
0 z
q
0 -
0
0
ln -~
>-er:
L
0 z
::::,
LL
"' w
Q_
::::,
(f)
I t-.·
"' D z
•
Alwninwn µg/L
Ar=c µg/L
Barium µg/L
llcrylliwn µglL
Cadmium µg/L
Calcium µg/L
Chromium µg/L
Cobalt µg/L
Copper µglL
Iron µg/L
L=I µg/L
Magnesium µg/L
Mlmgaru,se µg/L
NLCl:el µglL
Potassium µg/L
Selenium µglL
Silvcr µg/L
Sodium µglL
Thallium µ.glL
([ otal) Mercury µglL
Vanadium µ.glL
Zinc µg/L
3
Table 2-B. Results of Metal, Sample Analysis -Detected Compound,
u u lJ u u
50 u SA 5.6 u u
2000 19 31 34 32 33
4 IJ lJ r; u u
5 IJ u u lJ lJ
62000 83000 65000 82000 68000
100 u lJ 32 u lJ
u u u u u
14 12 16 38 36
150 850 810 500 u
u u u u u
1900 2600 2400 2900 2500
2 3 13 23 62 u
100-"'.l) lJ u 2.6 u u
720 940 1400 1100 1400
50 lJ lJ u u u
[J lJ u u u
9700 12000 13000 13000 12000
lJ lJ u u IJ
2 u lJ u u IJ
u lJ lJ u l.l
45 SJ 20 85 66
u)
0
Q_
"" 0
0
0 z
0J
SCJ
0
.-;
0
0
Lf)
.-;
>-a: >=
0
0 :z ::::,
LL
cY
u.J
Q_
::::,
(J)
I
f-
lY
0 z
•
•
Cont.
Allllllinum
Arsenic
Barium
Beryllium
Ca.dmitm1
Calcium
Chromium
Cobalt
Copper
lnm
Load
Magnesi\Dll
Manganese
Kiclccl
Potassium
Sdeniwn
Silver
Sodium
Thallium'
(Total) Mercury
Vanadmrn
Zinc
µ.g/L u
µgil. 50 u
µ.g/L 2()()() 32
µ.g/L 4 u
µg/.L j u
µ.g/L 86000
µg/L JOO 2.4
µg/L u
µg/L 34
µg/L 81
µg/L u
µg/L 2600
µg/L 4.S
µ.g/L 2.S
µg/L 1000
µ.g/L 50 u
µg/1, u
µg/L 12000
µg/1. 2 CT
µg/1, 2 u
µgfl. Li
µg/l. 160
4
u u u u
u u u u
24 28 u 25
u u u u
u u u u
57000 81000 3400 65000
1.5 u u 2. l
u u u u
120 15 14 20
3700 260 72 580
u u u 2.8
1400 2800 160 1900
19 3.3 12 8.4
12 u 16 u
820 1100 110 830
u u u u
0 u u u
11000 12000 62000 9100
0 lJ 7.8 u
0 lJ lJ u
0 lJ u u
350 52 15 63
I'-
0
Q_
" 0
0
0 z
"' "
0 -
0
0
LJ) • ,-<
>-CI: :~
Cl z
::) "-"' w
Q_
::)
(/)
:r:
f-..
"' D z
Cont.
Aluminum
Ar=ic
Barium
Beryllium
Cadrruum
Calcium
Chromiwn
Cobalt
Copper
Iroo
Lead
Magnesium
Manganese
Nici;el
Potassium
Selenium
Sih:er
Sodium
Thallium
(Tot.al) Mcrcury
Vanadium
Zinc
µg/1. u
µg/I. 50 u
µg/L 2000 36
µg/I. 4 lJ
µg/L 5 u
µg/L 92000
µg/L 100 3.1
µglL u
µglL 29
µglL 830
µglL lJ
µglL 2500
µg/L 20
µg/L u
µg/L 1100
µg/L 50 IT
µglL u
µg/L 10000
µgfL 2 u
µg/L 2 u
µgfL u
µg/L 22
5
u u u u
u (J u u
26 36 34 30
u u u u
u u u u
73000 99000 96000 85000
2.6 u u C
u u u u
11 19 26 36
250 130 360 190
u u u u
2300 2600 2.600 2400
5.4 3.8 26 2.1
[J u [J C
900 1100 I JOO !000
C u u u
u G lJ u
1000 1!000 11000 9700
lJ u u u
u u u [J
[J u u u
71 16 51 46
00
0
Q_
"' 0
0
D z
sq
""
0 -~
0
0
lf)
d
>-a: :,::
H
Cl z ::::,
LL
"' w
Q_
::::,
(/)
:r >-
"' D z
•
•
Cont.
Aluminum
Arsenic
Barium
Be,yllium
Cadmium
Calcium
Chromium
C-Obalt
Copper
Iron
l.<:ad
Magnesium
Manganese
Nickel
Potassium
Seh:nium
Silver
Sodium
Thallium
(Total} Mmury
Vanadium
Zinc
µg/L u
µg/L so 6.3
1,g/L 2000 }4
µ.g/L 4 u
µg/L 5 u
µg/L 93000
µg/L u
µg/L u
µg/L 49
µg/L u
µg/L Tl'" u
µg/L 2700
µg/L 5.8
µg/L u
µ.g/1. 1100
µg/L so u
µg/L u
;,g/L 12000
µg/L 2 u
µg/L 2 u
,qft, u
µg/L 56
6
u u u u
u u u u
37 33 30 32
u u u u
u u u u
93000 84000 72000 62000
15 u u 3.8
u u u u
28 38 46 60
87 u u 70
u u IJ u
2700 3000 2700 2700
20 u u 1.4
u u u u
1200 1600 1700 1900
u u u u
u u u u
12000 15000 14000 12000
u u u u
u u u u
U-\J u u
!JG 100 I IO !00
o,
0
Q_
'" 0
0
0 z
LI)
,q
0
~
0
0
1/1
,-;
>--a: :~
c:, z =>
\.L
Q'
Ld o_
=> (f)
:r:
f-'
Cle
D z
•
Cont.
Aluminum
Arsenic
Barium
Beryllium
Cadmium
Calciwn
Chromium
Cobalt
O,ppcr
Jron
Lead
Magnesium
Manganese
Nickel
Potassium
Selenium
S?lver
Sodium
Thallium
(Total) Mcmrry
Vanadium
Zinc
7
µg/L u
µg/L 50 u
µg/L 2000 33
µg/L u
µg/L 5 u
µg!L 66000
µg/L 100 u
µg!L u
µg!L 25
µg!L u
µg/L u
µg/L 3)00
µg/L
µg/L 10'1'1 u
µg/L 2000
µg/L 50 u
µg/L u
µg/L 13000
µg/L 2 u
µg/L 2 u
µg!L u
µg/L 20
u u lJ u
u u 5.9 u
24 22 31
u u u u
u u u u
93000 76000 70000 83000
u u u
u u L' u
35 26 15 18
540 230 480 870
u u u u
2600 2600 2400 2900
7_7 u 2.2 96
u u u u
1100 JOO() 84() 1000
u u u
u u u u
10000 11000 8100 9100
u lJ u u
u u u u
u u u u
170 25 30 26
0
d
(L
._,
0
0
D z
,n ._,
0
.-;
0
0
en
,-;
>--ff >=
r::l z => LL
°' w
CL =>
(/)
:r: ~.·
"' D z
•
Cont
Aluminum
Arsemc
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
l=l
Magnesium
Milllganese
Nickel
Pota.ss:ium
Selenium
Silva-
Sodium
Thallium
(Total) Men:ury
Vanadium
Zinc
µglL
µ.g/L
µ.g/L
µglL
µ.g/L
µg/"L
µglL
µg/L
µg/L
µ.g/L
µ.g/L
µglL
µg/L
µg!L
µg!].
µ.g/L
;,gll.
µ.g/L
µg/"L
µglL
µg!L
µg/L
8
0
50 6
2000 30
4 u
5 u
89000
u
u
15
990
u
2500
59
I C,00> u
1100
50 e
u
10000
2 I)
2 I)
u
56
u 0 0 0
u u e u
30 25 35 79
0 u u u
u u u u
86000 81000 79000 68000
16 0 u u
u u r: u
38 32 34 64
u u 130 2200
u u u u
2400 2300 3100 3300
1.3 u u 12
u u u u
1200 1100 2000 2000
u u u u
u u u I)
10000 9900 13000 10000
u u I) u
u u u u
u u u I)
190 70 !60 140
NORTH SUPERFUND ID: MAY 15'00 10:45 No.004 P.11 • 9 •
Aluminum µ~IL u
Arsenic ,,g/L 50 \)
Rllrium µglL 20011 59
1Je1ylii1"n µi;JL 4 1J
CuJmium ,,g/L 5 u
Cukium µg/L 20000
Chromium ,,g/L 100 ll
Cohalt µwl, u
Cuppcr ,,g/J, 'J"J'\7) 1 l
lrun ,,g/L 5400
Lcud 1,J;'L u
Ma.gncsiwn µg/L 1200
Ma11gane,;e µ~IL 55
Nickel µ~IL JOO''' u
l1otr1.~sium µg/L SGU
Selenium ,,g/1, 50 u
Silv..:r ,,g/L ll
sodium µglL 941)1)
'J'hnlliurn µg/L 2 ll
(Tow!) Mercury ,,g/L 2 u
Vum1dium /ig/J, u
Zini..: ,,glL 180
Dntll QllLllili..:ni: U -M;th:rnd WH3 mrnly.tcd for hut not detected, J -Ust1:nated Volue
(I) Reference for the PrimfH)' Drinking W11tl:r St1mdards / MCL's: www.ep;1.gov/()ST(ro(,lti/dw::ild:d1lmi, US EPA Office of
Water.
(2) TT• TrcHlmcnt Technique l•'or r:opptr, \he Attion U.?wl h 1300 µg/L For Lc~cl. th(! Aclion Lc,,cl i~ 15 ug/L
( ~) LkiuM R1,;mHmk:d
~WRTH SUPERFUND ID: •
Appendix A
Laboratory Results
MRY 15'00 10:47 No.004 P.12 •
i✓DRTH SUPERFU~rn ID: MRY 15'00 10:57 No .005 P.02 • •
NEW HANOVER COUNTY AIRPORT BlJRN PIT
SUPERFUND SITE
AMENDED RECORD OF DECISION
MARCH 2000
United States Environment•! Prulec!lou Agency
Region 4
i✓□.'1TH SUPERFUi\lD ID: MRY 15'00 10:57 i\lo.005 P.03 • •
TABLE OF CONTENTS
Section Page
THE DECLARATION ...... , , . , ....... , .... : ........... , .................... I
DECISION SUMMARY ...................................................... 1
1.0 INTRODUCTION ..................................... , . , ............. 1
1.1 Site Location ........................................................ 1
1.2 Affected Population ................................................. , .. I
1.3 Adjacent Land Uses ................................... , ................ I
1,4 Natural Resources ............................................ · ......... 1
1.5 Site Operational Histo1y ...... , ....... , .................................. 2
J .6 Highlights of Community Participation .................................. , ... 3
2.0 REASONS FOR ISSUING THE'ROD AMENDMENT ........................ 4
2. l Description of Original Selected Remedy .................... , ............... 4
2.2 Rationale for Changing New Selected Remedy .. : . .' .' ... .'. . . . . . . : · ... : ...... 6
' . '·•" ' ,,
3.0 DESCRIPTION OF NEW ALTERNATIVES ................................ 8
4.0 COMPARATIVE ANALYSIS OF NEW ALTERNATIVE REMEDIES ........... 11
4.1 Overall Protection of Human Health and the Environment ..................... , 11
4.2 Compliance with ARARS ............................. , . , . , , ............ 12
4.3 Long-Term Effectiveness and Permanence ............................. , .... 12
4.4 Reduction of Toxicity, Mobility or Volume through Treatment .................. 12
4.5 S11011-Tenn Effectiveness ............................................... 12
4.6 Implementability ...................................... , ............... 12
4.7 State Acceptance , , .. , ............... , , ............................... 12
4. 8 Community Acceptance ......................................... , ...... 12
4. 9 Cost ....................................................... , ....... J 3
5.0 STATUTORY DETERMINATIONS ................. , , .................. 13
List of Figures
Figure l Site Location Map , . , , , . , . , .................................. , , , , , , , , 2
Figure 2 Estimated Extent of Concentrations in Groundwater ....... , ................ , .5
,
/
I
NORTH SUPERFUND ID: •
List of Tables
Table l . Groundwater Remediation Levels
Table 2 -Institutional and Land Use Restrictions
APPENDICES
MAY 15'00 •
Appendix A • North Carolina Division of Supcrfund Letter of Concurrence
Appendix B • Summary of Cost Estimates for Evaluated Alternatives
" .•
' (
I
/
10:58 No .005 P.04
;✓ORTH SUPER'FU;,rf
TO:
OFFICE:
MRY 15'00 10:39 No.004 P.01
FAX PHONE I: q;
RETUR.i"{ FAX#: [phone]
,
COUNTY
Rl\'ER BASIN:
RF.PORT 10
Othrr :
COLLECTOR(S)
RECEIVED)
MAR O 8 2000 I
BY: Dw-o
□
DIVISION OF WATER QUALIT\'
Chemhlry Laboratory Report I Water Qu.lity
PJllilRIIX
AMBIENT E]QA
WI RO Regional Oma: (u COMPLIANCE
□ EMERGENCY
D CHAIN OF CUSTODY
COLBY
!ill
El
rECEIVEO
APR 07 2000
SAMPI ETYPSUPERFUND SECTION
STREAM □ EFFLUENT 1
□ LAKE □ INFLUENT
□ ESTUARY D
S1111ion Lou1io11: 0B0U0RN=0P01T~-------
Sttd:
BOD 310
COO lliRh 3~0
COD Low JH
Coliform: MF Fecal 3!616
Coliform: MF loial 3\SQ.i
Coliform: rube Fecal 31615
Coliform: Fecal Strep 31673
Residue: Total 500
Volatik SOS
Fixed SJO
Residue: Susoended 530
Volatile: 535
Fixed 540
oll 403
Aciditv to oll 4.5 436
Acidity to pl! 8.3 435
Alkalinitv to oil 8.3 415
Alkali nit\" to r,11 4.n 10
TOC680
Turbiditv 76
Coliform Total Tube
COMMENTS:
Chlorin~1ed:
Dalt lki:in (n/m,n/tld)
20000121
Date End (nlmm/dd)
nut!L Chloride 940
m1t/L Chi a: Tri 32217
m1t/L Chi a: Corr 32209
/IOOml Phcoohvtin a 32213
/IOOml Color: True 80
1100ml Color. (OH ) 83 DH"'
/J00ml Color: pH 7.6 82
mg/L Cyanide 720
mo/L Fluoride 951
miz/L Forma!dchvdc 71880
miz/L Grease and Oils 556
mg/L Hardness Total 900
m11/L S,_,.,..;fic Cond. 95
units MBAS 38260
m1s/l Phenols 32730
mglL Sulfate 945
miz/l Sulfide 74S
mR/L Boron
mg/l l"annin & LiPnin
NTU lkxavalcnt Chromium
w/100 mis
Time lkgin
1510
Time End
mg/L
ug/L
ug/L
uiz/L
c.u.
c.u.
c.u.
mg/L
miz/L
moll
m11./L
moll
umhos/cm.2
moll
ug/L
miz/L
miz/L
uR/L
urz/L
Depth. UM, DB, DBM Value Type. A, II, L
NH3 as N 610 mz/L
TKN anN 625 m1</l
N02 plus N03 as N 630 moll
P: Total as P 665 m11/L
PO4 as P 70S07 miz/L
P: Diuolved as P 666 m1</L
K-Potassium moll
Cd-Cadmium 1027 u11/L
Cr-Chromium:Total 1034 u2/L
Cu-Con,...r 1042 "oil
Ni-Nickel 1067 . u1</L
Pb-Lead JOSI u11JL
Zn-Zinc 1092 ue./L
V-Vanadium "oil X
Ag-Silver 1077 ug/L
Al-Aluminum I !OS "'IL
Be-Ber.·llium l012 Ul!/L X
Ca-Calcium 916 m1<IL
Co-Cobalt 1037 u11/L
Fe-Iron 104S "oil
Lab Number
Dale Received:
11me Received :
Received By :
Data Released :
Date Rtported:
Li-Lilhium 1132
M1<-,._fa1<nesium 927
Mn-Manganese JOSS
Na-Sodium 929
Arsenk:To1al 1002
Sc-Selenium 1147
H1<-MerCUry 71900
Ba Barium
YW0378
1/31/2000
11:45AM
HMW
AR
2/23/2000
Orizanochlorine Pesticides
Orunoohosohorus Pesticides
Acid Herbicides
",JL
m1</L
ug/L
m11/L
uiz/L
u1</L
",IL
u11/L
Base/Neutral&Acid Extractable Oritanics
·r PU Diesel Range
Pur£eable Outanics (VOA bottle rea"d)
TPII Gasoline Range
TPH/BTEX Gasoline Ranize
Ph\1.oolankton •
DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALIT'l Fllo~lJ-LAll FOHM (DMI)
COUNTY . tlr. '--<--' \j c, V\ 0 VI',✓
RIVER BASIN C.c..
REPORT TO: ARO FRO M
AT BM
Other
Shipped by: Bu11 ~ St11f;, Other ________ _
COLLECTOR(S), L 6 / 0 f
E•tlmated BOD Range: 0•5/5·25/25·65/40-130 or 100 plus
PRIORITY
i:::ly-,a1ENT
~COMPLIANCE
□EMERGENCY
□ QA
□ CHAIN
OF CUSTODY
STATION LOCATION:
I
SAMPLE TYPE
~EAM □ □ LAKE □ □ESTUARY
B+-
EFFLUENT
INFLUENT
Rec'd
DATA ENTRY BY:
DATE REPORTED:
5
CK:
Seed: Yes O No O Chlorinated: Yes D No O 0R~E~M"A=R'-'K"'S"-'----------------------------------------------------
Station # bP I IDate Begin (yy/mm/dd) I Time Begin I Date End !Time EndlDepth OM DB DBM I Value .Type Composite Sample~
CJ O . D I . 2 \ I 5'"1 0 . , A H L T s B C G GNXX
1 8OD5 310 mg/I Chloride 940 mg/I NH3 as N 610 mg/I LI-Lithium 1132 ug/1
2 COD High 340 mg/I Chi a: Tri 32217 ug/1 TKN as N 625 mg/I Mg-Magnesium 927 ' 3 COD Low 335 mg/I Chi a: Corr 32209 ug/1 N02 plus N03 us N 630 mg/I Mn-Manganese 1055
4 Coliform: MF Fecal 31616 1100ml Pheophytln a 32213 ug/1 P: Total as P 665 mg/I Na-Sodium 929 mg/I
5 Coliform: MF Total 31504 /lO0ml Color: True 80 Pt-Co P04 as P 70507 mg/I Arsenlc:Total 1002 ug/1
6 Coliform: Tube Fecal 31615 1100ml Color:(pH ) 83 ADMI P: Dissolved as P 666 mg/I Se-Selenium 1147 ug/1
7 Coliform: Fecal Strep 31673 /IOOml Color: ptl 7.6 82 ADMI Hg-Mercury 71900 ug/1
8 Ri!'sldue: Total 500 mg/I Cyanide 720 mg/I Cd.cadmium 1027 ug/1 Organochlortne Pesticides
9 Volatlle 505 mg/I Fluoriifo 951 mg/I Cr-Ouomlum:Total 1034 ug/1 Organopho6phorus Pesticides
10 Flxi!'d 510 mg/I Formaldehyde 71880 mg/I Cu<:opper 1042 ug/1
11 Residue: Suspended 530 mg/I Grease and Olis 556 mg/I NI-Nickel 1067 ug/1 Acid Hl!'rblcldes
12 Volatile 535 mg/I Hardness Total 900 mg/I Pb-Lead 1051 ug/1
13 Fixed 540 mg/I SpecUlc Cond. 95 uMhos/cm 2 Zn-Zinc 1092 ug/1 V JMse/ Neutral Extractable Organics
14 pH 403 units MBAS 38260 mg/I V Acid Extractable Organics
15 Acidity to pH 4.5 436 mg/I Phi!'nols 32730 ug/1 Ag-ollver 1077 ug/1
16 Acidity to pH 8.3 435 mg/I Sulfate 945 mg/I AI-Aluminum 1105 ug/1 V Purgeable Organics (VOA bottle reg'd)
17 Alkallnlty to pH 8.3 415 mg/I Sulfide 745 mg/I Be-Berylllum 1012 ug/1 • 18 Alkallnlty to pH 4.5 410 mg/I Ca-Calcium 916 mg/I I
19 TOC 680 mg/I Co-Cobalt 1037 ~ ug/1 ..
20 Turbidity 76 NTU Fe-Iron 1045 ll l•g11 Phytoplafton
.-.... ' .. ..::
Sampling Point~ Conductance at 25 C Water Temperature IC) 0.0. mg/I pH Alkalinity ~ \ Acidity ' Air Temperature (C)
~ 3002,.s~
pH 8.3 pH4.5 pH 8.3
94 262, 1--1, -
2 10 400 I• 82244 431 ··~ -· 82243 182242 20
Salinity~ Preclpltlon On/day) Cloud Cover ~ Wind Direction (Deg) Stream Aow Severity Turbidity Severity Wind Velocity M/H ~ean Stream Depth ft. Stream Width ft.
480 o. I 45 32 36 1351 1350 35 64 4
DMt/Revlsed 10/86
ENRIDWQ LABORATORY LAB NO. YW0378
~ VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY DATE
REVIEWED BY
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RES UL TS DATE D
75.35.4 1, 1-Dichloroethene 0.75 u 96-18-4 1.2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1.1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2.2-Dichloropropane 0.25 u 541-73-1 1,3-Dich1orobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene 0.25 u 106-46-7 1.4-Dichlorobenzene 0.25 u • 67-66-3 Chloroform 0.25 u 95-50-1 1.2-Dichlorobenzene 0.25 u
74-97-5 Bromochlorome\hane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u B7-61-6 1,2.3-Trichlorobenzene 0.75 u
107-06-2 1.2-Dichloroethane 0.25 u 1634-04--4 Methyl-tert-butyl ether 5 u
79-01-6 T richloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Oibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95--47-6 a-Xylene u
10061-02-6 trans-1.3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1.2-Trichtoroethane 0.25 u 98-82-8 1sopropylbenzene u
127-18-4 T etrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1.3-Dichloropropane 0.25 u 108-67-B 1.3.5-Trimethylbenzene u
124--46-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1.2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u • 630-20-6 1. 1.1.2-T etrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79-34-5 1.1.2.2-Tetrach!oroethane 0.75 u 91-20-3 Naphthalene u
mg!L mgll
TOL-Target Ouantitation Limit-Subject to 0.20 N
change due to instrument sensitivity
T-Tentatively Identified. not confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D-Detected below quantilation limit DETECTED BY GC/ELCOIPID.
M-GCIMS Analysis performed
' )MMENTS ) '----___,
~ ENR/DWQ LABORATORY LAB NO. YW0378
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR~ CHECKED BY DATE
REVIEWED BY /nJ ENTERED BY ·
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE 7----;2 7;.--lf!J
62-53-3 ANILINE 10 u 606-20-2 2,6-DINITROTOLU ENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANIUNE 50 u
111-44-4 BIS(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-0INITRO PHENOL 50 u
541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1,4-DICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u • 100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE 10 u
95-50-1 1,2-DICHLOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
95.49.7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 81$(2-CHLOROISOPROPYL) ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NlTROANIUNE 50 u
621-64•7 N·NITROSO-Dl•N-PROPYLAMINE · 10 u 534-52·1 4,6·DINITR0·2·METHYL PHENOL 50 u
67-72•1 HEXACHLOROETHANE 10 u 86-30-6 N·NITROSODIPHENYLAMINE 10 u
98·95-3 NJTROBENZENE 10 u 101.55.3 4•BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u 118•74-l HEXACHLOROBENZENE 10 u
88-75-5 2-NITRO PHENOL 10 u 37.95.5 PENTACHLORO PHENOL 50 u
105·67,9 2.4-0IMETHYL PHENOL 10 u 85·01·8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 5D u 120.12.7 ANTHRACENE 10 u
111-91·1 81S(2·CHLOROETHOXY) METHANE 10 u 94.74.2 OI-N•BUTYL PHTHALATE 10 u
120-83·2 2,4•DICHLORO PHENOL 10 u 206·44·0 FLUORANTHENE 10 u
120-82-1 1.2,4-TRICHLOROBENZEN E 10 u 129-00-0 PYRENE 10 u
91·20·3 NAPHTHALENE 10 u 85·68-7 BUTYLBENZYL PHTHALATE 10 u
106-47•8 4•CHLOROANIUNE 20 u 91·94-1 3,3' -OICHLOROBENZJDINE 20 u
87-68-3 HEXACHLOROBUTADIENE 10 u 56-55-3 BENZO{A)ANTHRACENE 10 u
59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218·01-9 CHRYSENE 10 u
91•57-6 2-METHYL NAPHTHALENE 10 u 117•81-7 BIS(2·ETHYLHEXYL) PHTHALATE 10 u • 77.47.4 H EXACHLOROCYCLOPENT AD!EN E 10 u 117•84·0 Ol•N-OCTYL PHTHALATE 10 u
88-06-2 2.4,6-TRICHLORO PHENOL 10 u 205·99-2 8 ENZO( B )FL UO RAN TH ENE 10 u
95.95.4 2,4.5-TRICHLORO PHENOL 10 u 207•08-9 8 ENZO(K)FL VORA NTH ENE 10 u
91·58-7 2-CHLORO NAPHTHALENE 10 u 50·32·8 BENZO(A)PYRENE 10 u
88-74-4 2-NITROANIUNE 50 u 193.39.5 INDENO{I ,2,3·CD)PYRENE 10 u
131-11·3 DIMETHYL PHTHALATE 10 u 53-70-3 DI BENZO{A,H)ANTHRACENE 10 u
208·96-8 ACENAPHTHYLENE 10 u 191-24•2 8 ENZO{G, H, l )PERY LENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. YW0378 -~==~
TQL· Target Quantitation limit-Subject to
change due to instrument sensitivity
T · Tentatively ldenlffied, estimated concentration
E-Estimated Value
U-Saf!1ples analyzed for this compound but not detected
N· Sample nol analyzed for this compound
0-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: ______________________________________________ _
•
•
___)
RECEIVED
' .... MAR O 8 2000
DIVISION OF WATER QUA.LIT\' BY: bW:%)
l.!::!c=-.'..:=:::~~::::;:::;=:;::;:::;:::::::::~brmislry Llboratory Rrport / W•ltr Qualily
COUNTI'
RJVER BASIN:
NEWIIANOVER
REPORT TO WIRO Regional om~
Othrr :
COL~ECTOR(S) : 0C"O"L~B"Y ___ _
Sttd:
S111io11 #
BP2
BOD JIO
COD Ui<l'h 340
COD low 335
Coliform: MF Fecal 31616
Coliform: MF Total 3150-I
Coliform: rube Fecal 31615
Coliform: Fecal Strrn 31673
Residue: Total 500
Volatile 505
Fixed 510
Residue; Susr>ended 530
Volatik 535
Fixed 540
I Dll 403
Aciditv to nH 4.5 436
Aciditv to nll 8.3 43S
Alkalinitv 10 nH 8.3 41 S
Alkalinity to oil 4.5 410
TOC:680
Turbiditv 76
Coliform Total Tube
COMMENTS:
Chlorinalrd:
Dale Br,:in (n/mm/dd)
20000121
mg/L
n112/L
m2/L
/IOOml
1100ml
1100ml
/JOOml
m.ct/L
ml!/L
m2/L
m11./L
m11tl
m2/L
unils
0111/L
m2/L
m2/L
m11./L
m11.IL
NTU
-1100 mis
= □ AMBIENT
El COMPLIA~CE
□ E~IERGENCY
'j
i
Date End (yy/mm/dd~
Chloride 940
Chi a: Tri 32217
Chi a: Corr 32209
Pheooh,tin a 32213
Color. True 80
Color: (nll \ 83 nH-
Color: DH 7.6 82
Cyanide 720
Fluoride 951
Formaldehvde 71880
Grease and Oils 556
Hardness Total 900
S,_,.;fic Cond. 95
MBAS 38260
Phcuols 32730
Sulfate 945
Sulfide 745
Boron'
Tannin & Lignin
Hexavaknt Chromium
D QA
D CHAIN OF CUSTODY
Rcmuks:
Time Begin
1540
Time End
mg/L
""'' u11/L
u11/L
c.u.
c.u.
c.u.
mg/L
mg/L
m,!L
m11!L
mg/L
umhos/cm2
m.11./L
ug/L
m11./L
m11./L
""'' ""''
Lab Number YW0379 ~ SAME! EIYEE Date Received : 1/31/2000
lime Received : 11:45AM
1£] STREAM □ EFFLUENT Received By HMW
□ LAKE □ INFLUENT
□ ESTUARY D Dal.a Released : AR
Date Reported : 2/23/2000
~plh -DM, DB, DBM Value Type• A, II, L Composite-T, S, 8 Samplc Type
NHJ as N 610 mg/L Li-Lithium 1132 "'IL
TKN an N 625 mg/L Mg-Magnesium 927 m11/L
NO2 ~ !us NOJ as N 630 mg/L Mn-Manganese 1055 u11./L
P: Total as P 665 m11./L Na• Sodium 929 m11/L
PO4 as P 70507 mg/L Arsenic:Total 1002 "'IL
P: Diuolved as P 666 mg/L Sc· Selenium 1147 u2/L
K-Potassium m,!L H2-Mercurv 71900 ""'L
Cd-Cadmium 1027 ug/L Ba_Barium ua/L
Cr-Chromium:Total 1034 ""'' Organochlorine Pesticides
Cu-co~-r 1042 ""'' Or11.anoohosohorus Pesticides
Ni-Nickel 1067 u11./L
Pb--Lead 1051 ,g1L Acid lle1bicides
Zn-Zinc 1092 ug/L
V-Vanadium URIL X Base/Neutral&Acid Extracta.ble OrAAnics
Ag-Silver 1077 ug/L ·1 PII lJiescl Range
Al-Aluminum 110S ""'' Be-Bervllium 1012 u11/L X Pur11.eable Or.ctanics (VOA bottle reQ'd)
Ca-Calcium 916 mg/L TPII Gasoline Range
Co-Cobalt 1037 ug/L TPH/BTEX Gasoline Range
Fe-hon 1045 ,g!L Phytoplanl:ton
ENVIHUNMENTAL MANAGEMENT UIVISIUN or
COUNTY /Vc.,_t,....,,
WATER QUALITY FIELU·LAB FORM (DMI) He1no ?
RIVER BASf't"~·. cs
REPORT TO: ARO FRO MR
AT BM
Othu
Shipped by: Bus@, Staff, OJher ________ _
COlLECTOR(S), Co f b V
E•tlmated BOD Range: 0·5/5-25/25·/s:0-130 or 100 plus
PRIORITY
□AMBIENT
~MPLIANCE
□EMERGENCY
□ QA
□ CI-IAIN
OF CUSTODY
STATION LOCATION:
I
SAMPLE TYPE
~REAM □ □ LAKE □ □ESTUARY
EFFLUENT
INFLUENT
Rec'd b :
DATA ENTRY BY:
DATE REPORTED:
Del
CK:
Seed: Yes O No O Chlorinated: Yes O No O 0R~E~M~A=R~K~S~'----------------------------------------------------I Station # ~ 3P 2-!°ate Begin (yy/mm/dd) I Time Begin I Date End !Time EndlOepth OM DB DBM 'Value Type Composite ISam~le~ cJO .rJ/ ,"2( /S-l/0 , A H L T s 8 GNXX
1 BOO5 310 mg/I Chloride 940 mg/I NH3 as N 610 mg/I LI-Lithium 1132 • 2 COD High 340 mg/I Chi a: Tri 32217 ug/1 TKN as N 625 mg/I Mg-Magnesium 927
3 COD Low 335 mg/I Chi a: Corr 32209 ug/J N02 plus N03 as N 630 mg/I Mn-Manganese 1055 ug/1
4 Coliform: MF Fecal 31616 /100ml Pheophytln a 32213 ug/1 P: Total as P 665 mg/I Na-Sodium 929 mg/I
5 Coliform: MF Total 31504 1100ml Coloi-: True 80 Pt-Co P04 as P 70507 mg/I Arsenfc:Total 1002 ug/1
6 ColHorm: Tube Fecal 31615 1100ml Color:(pH ) 83 AOMI P: Olssolved as P 666 mg/I Se-Selenium 1147 ug/1
7 Coliform: Fecal Strep 31673 1100ml Color: pH 7.6 82 ADMI Hg-Mercury 71900 ug/1
8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd-cadmium 1027 ug/1 Organochlorine Pesticides
9 Volatile 505 mg/I Fluoride 951 mg/I Cr-Chromlum:Total 1034 ug/1 Organophospx,rus Pestk:kles 10 Fixed 510 mg/I Formaldehyde 71880 mg/I Cu-COppe_r 1042 ug/1
11 Residue: Suspended 530 mg/) Grease and Olis 556 mg/I NI-Nickel 1067 ug/1 Acid Herbicides
12 Volatlle 535 mg/I Hardness Total 900 mg/I Pb-Lead 1051 ug/1
13 Fixed 540 mg/I Specific Cond. 95 uMhos/cm 2 Zn-Zinc 1092 ug/1 v Base/ Neutral Extractable Organics 14 pH 403 units MBAS 38260 mg/I V Acid Extractable.Organics
15 Acidity to pH 4.5 436 mg/I Phenols 32730 ug/1 A9-;:1llver 1077 ug/1 , 16 Acidity to ptl 8.3 435 mg/I Sulfate 945 mg/I Al-Aluminum 1105 'I ug/1 IV Purgeall e Org lcs (VOA bottle r. 17 Alkallnlty to pH 8.3 415 mg/I Sulfide 745 mg/I Be-Berylllum 1012 / g/1 J 18 Alkallnlty to pH 4.5 410 mg/I Ca-Calcium 916 ' • I 19 TOC 680 mg/I Co-Cobalt 1037 J ' I
20 Turbidity 76 NTU ------·---· ------------Fe-Iron 1045 -u 1 Phytoplan I"
Sampling Point !l Conductance at 25 C Water Temperature(: D.O. mg/1 pH Alkalinity Acidity Air TelTlperature t(:) pH 8.3 pH 4.5 pH 4.5 pH 8.3
2 94 11. l IO /L{_ 0 300 61,60 400 I• 82244 431 82243 182242 20 Salinity ,:; Preclpltlon On/day) Cloud Cover !l Wlnd Dlrecdon (Deg) Stream Flow Severity Turbidity Severity Wind Velocity M/H Mean Stream Depth fL Stream Wklth fL
480 0,0 45 32 36 1351 1350 35 64 4
. ____ ;
DMI/Revbed 10/86
REPORTED BY
•-CHECKED BY
REVIEWED BY
SAMPLE TYPE·
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
WATER
1, 1-Dichloroethene
Methylene Chloride
trans-1.2-Dichloroethene
1, 1-Dichloroelhane
2.2-0ichlorop,opane
cis-1.2-Dichloroethene
Chloroform
Bromochloromethane
1, 1-Trichloroe1hane
1-Dichloropropene
Carbon Tetrachloride
1.2-Dichloroethane
T richloroethene
1.2-Dichlornpropane
B,omodichloromethane
Oibromomethane
cis-1,3-0ichloropropene
lrans-1,3-Dichloropropene
1.1.2-Trichloroethane
Tetrachlo,oethene
1,3-0ichloropropane
Dibromochloromethane
1.2-Dibromoethane
Ch!orobenzene
1.1.1.2-1 etrachloroethane
Bromoform
1.1,2,2-Tetrachloroethane
la1get Ouantitation limit-Subject to
change due to instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
0.75
10
0.75
0.25
0.25
0.25
0.25
0.75
0.25
.0.25
0,75
0.25
0.25
0.25
0.25
0.25
0,25
0.25
0.25
0.25
0,75
0.25
0.25
0.5
0.75
U-Samples analyzed for this compound but not detected
N-
D-
M-
Sample not analyzed for this compound
Detected below quanlitation limit
GCIMS Analysis performed
ENRIOWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RES UL TS
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
96-18-4 1,2,3-TrichlOropropane
108-86-1 Bromobenzene
95-49-8 2-Chlorotoluene
106-43-4 4-Chlorotoluene
541-73-1 1,3-Dichlorobenzene
106-46-7 1,4-Dichlorobenzene
95-50-1 1,2-Dichlorobenzene
96-12-8 1,2-Dibromo--3-Chloropropane
120-82-1 1,2,4-Trichlorobenzene
87-68-3 Hexachlorobutadiene
87-61-6 1.2.3-Trichlorobenzene
1634-04-4 Melhyl-tert-butyl ether
71-43-2 Benzene
108-88-3 Toluene
100-41-4 E.thyl benzene
108-38-3 m,p-Xylenes
95-47-6 o-Xylene
100-42-5 Styrene
98-82-8 lsopropylbenzene
103-65-1 n-Propylbenzene
108-67-8 1.3.5-Trimethylbenzene
98-06-6 tert-Butylbenzene
95-63-6 1,2,4-Trimethylbenzene
135-98-8 sec-Butylbenzene
99-87-6 p-isopropyltoluene
104-51-8 n-Buty1benzene
91-20-3 Naphthalene
---~
~.::~ :f;~·l~.a~~~ -Esti~~ie:d
Other purgeab1es detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GCfELCO/PID.
)MMENTS: ------------------------------
DATE • 'V
ENTERED BY (
LAB NO. YW0379
SUPERVISOR=!t,.
DATE :;i.. -7 :..01)
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u • 0.25 u
u
0.25 u
0.25 u
0.75 u
5 u
u
u
u
2 u
u
u
u
u
u
u
u
u • u
u
u
------------
mg/L mg/l
0.20 N
Detected
ug/L
ENR/DWQ LABORATORY LAB NO. YW0379
SEMI-VOLATILE ANALYTICAL REPORT
'""'"''""~ REPORTED BY
CHECKED BY DATE e,
REVIEWED BY '· ENTERED BY L
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE ;l-~ },.'?;-'iJO
62·53·3 ANILINE IO u 606·20-2 2,6-DINl~R0TOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITR0ANIUNE 50 u
111-44-4 8I5{2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE IO u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITRO PHENOL 50 u
541-73•1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1,4-0ICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u • 100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE 10 u
95-50-1 1,2-DICHLOROBENZENE IO u 84-66-2 DIETHYL PHTHALATE IO u
95-48-7 2-METHYL PHENOL IO u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 815(2-CHLOROISOPROPYL) ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NITROANIUNE 50 u
621•64,7 N-NITROS0,0I,N,PROPYLAMINE 10 u 534.52.1 4,6•0INITR0·2·METHYL PHENOL 50 u
67-72-1 HEXACHLOROETHANE IO u 86·30·6 N-NITROSODIPHENYLAMINE 10 u
98,95·3 NITROBENZENE IO u 101.55.3 4-BROMOPHENYL PHENYL ETHER IO u
78-59-1 ISOPHORONE IO u 113.74.1 HEXACHLOROBENZENE 10 u
88·75-5 2-NlTRO PHENOL 10 u 87-86·5 PENTACHLORO PHENOL 50 u
105-67-9 2.4-0IMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE IO u
65-85-0 BENZOIC ACID 50 u 120-12·7 ANTHRACENE 10 u
111.91.1 8I5(2,CHLOROETHOXY) METHANE 10 u 34.74.2 Ol•N-BUTYL PHTHALATE 10 u
120-83·2 2,4-DICHLORO PHENOL 10 u 206,44-0 FLUORANTHENE 10 y
120-82·1 1,2,4• TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
I 06-4 7-8 4-CHLOROANILINE 20 u 91.94.1 3,3'-DICHLOROBENZIDI NE 20 u
87-68-3 HEXACHLOROBUT ADI ENE 10 u 56,55-3 BENZO(A)ANTHRACEN E 10 u
59-50-7 4•CHLOR0-3·METHYL PHENOL 20 u 218·01·9 CHRYSENE 10 u
91-57-6 2·METHYL NAPHTHALENE 10 u 117•81•7 81S(2·ETHYLHEXYL) PHTHALATE IO 17
77 .4 7-4 HEXACHLOROCYCLOPENTADfENE 10 u 117-84-0 DI-N·OCTYL PHTHALATE 10 u
88-06-2 2.4,6·TRICHLORO PHENOL 10 u 205-99·2 BENZO(B)FLUORANTHENE 10 u
95.95.4 2.4,5• TRICHLORO PHENOL 10 u 201.oa.9 BENZO(K)FLUORANTHENE IO u
91-58-7 2-CHLORO NAPHTHALENE IO u 50·32-8 BENZO(A)PYRENE 10 u
88-74-4 2•NITROANIUNE 50 u 193·39-S INOENO(l ,2,3·CD)PYRENE 10 u
131-11-3 DIMETHYL PHTHALATE 10 u 53-70-3 DI BENZO(A,H)ANTHRACEN E IO u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 BENZO(G,H,l)PERYLENE IO u
SEMIVOLATILE ORGANICS REPORT-DWQ LAB PAGE 2
COMMENTS: Phthalates are commom laboratory contaminants.
LAB NO. YW0379 -------
TQL· Target Quantitation limit-Subject to
change due to inslrument sensitivity
T-Tentatively Identified, estimated concentration
£. Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded •
•
._)
COUNTI'
Rl\'[R BASIN:
RHORTTO
Other :
COLL[CTOR(S)
DIVISION OF WATER QUALITY
RECEIVED
MAR O 8 2000
BY: D WQ Chemistry L1bontory Report/ Waler Qu.lily
~NOVER = □ ~MBIENT □QA
WJRO Regional Office f (K] ~9MPLIANCE D CHAIN OF CUSTODY
□ EMERGENCY
COLBY
El SAMfl EIYfE
5J STREAM
□ LAKE
□ ESTUARY
[stimalcd BOD Ran.:c: Station Location: BURN PIT SIDE BLUE CLAY RD
Station#
BPJ
BOD JIO
COD lli2h 340
COD Low 33S
Colirorm: MF Fecal 31616
Coliform: MF Total 3150-I
Coliform: tul;,c Fccal 3161S
Coliform: Fecal Strrn 31673
Residue: Total 500
Volatile 505
Fixed 510
Residue: Susvcnded 530
Volatile 535
Fixed 540
I oH 403
Acidi1v 10 oll 4.5 436
Aciditv to oll 8.3 435
Alkalinirv to nH 8.3 415
Alkalinitv to olf 4.5 410
TOC680
Turbiditv 76
Coliform Total Tube
COMMENTS:
Chlorin11ted:
Dale &gin (yy/mm/dd)
I 20000 J 21
m2/L
m2/L
mg/L
1100ml
1100ml
/IOOnll
1100ml
m,_,L
mg/L
miz/L
m11./L
mg/L
miz/L
units
m11./L
mg/L
miz/L
miz/L
miz/L
NTU
"/100 mis
Dale End (n/mm/dd)
Chloride 940
Chla:Tri32217
Chi a: Corr 32209
Pheonhvtin a 32213
Color: True 80
Color: (pl I ) 83 di=
Color: nil 7.6 82
Cvanide 720
Fluoride 951
Formaldchvdc 71880
Grease and Oils 556
Hardness Total 900
S--'fk Cond. 95
MBAS 38260
Phenols 32730
Sulfate 945
Sulfide 745
Boron
Tannin & Ll1min
Hexavalent Chromium
Remarks:
Time lkgin
1550
lime End Depth -OM, DB, DBM
m11./L Nll3 as N 610
u11./L TKN an N 625
ug/L N02 olus N03 as N 630
,g/L P: Total as P 66S
c.u. P04 as P 70507
c.u. P: Dinolved as P 666
c.u. K-Potassium
m2/L Cd-Cadmium 1027
m,IL Cr-Chromium:Total 1034
mg/L Cu-Connt"r 1042
m11./L Ni-Nickel 1067
mJ.?./L Pb-Lead 1051
umhoslcm2 Zn-Zinc 1092
miz/L ¥-Vanadium
UJ.?./L Aiz-Silver 1077
mJ,?.IL Al-Aluminum 1105
mg/L Be-R,,r.llium 1012
Ca-Calcium 916
u11./L Co-Cobalt 1037
,,vL Fe-Iron 1045
Lab Number ' YW0380
Date Received: I/Jl/2000
Time R~ived : ll:4SAM □ EFFLUENT Received By ' HMW
□ INFLUENT
D Data Releai.ed : AR
Date Reponed : 2/23/2000
Value Tyl)I:'. A, 11, L Composit"'T, S, B Sample Type
mg/L Ll-Lllhium 1132 muL
mg/L Mg-Magnesium 927 m2/L
mJ.?./L Mn-Manizanese 105S "°'L
mg/L Na-Sodium 929 m,,L
mg/L Arsenic:Tot.al 1002 URIL
m11.IL Sc-Selenium 1147 ua/L
mg/L Hg-Mercury 71900 uiz/L
!JSIL Ba_Barium u11./L
u2/L Or2anochlorine Pesticides
ug/L O,ganophosphorus Pesticides
ug/L
u11./L Acid Herbicida
ug/L
ug/L X Base/Neutral&Acid Extractable Organics
uiz/L TPI I Diesel Rani.e
,,JL
,g;L X Pur111!able Organics (VOA bottle req'dl
mg/L TPH Gasoline Range
ug/L TPH/BTEX Gasoline Rani.e
,,1L Phvtoc lankton
I
DJ:;;SION OF ENVIRONMENTAL
coJ..TY ';,/ e_i,,.,. I..J: """ o ve,,,.--
MANAGEMENT WATER QUALIT FIELD·LAB FORM (DMI) For L11.b Use ONLY
RIVER BASIN
REPORT TO: ARO FRO M
AT BM
Olher
WSRO TS
Shipped by: Bus er, Stall, Other ________ _
COLLECTOR(S), Cc) / b ✓
I E■Umated BOD Range: 0-5/5-25/25-65/40-130 or 100 plus
PRIORITY
□AMBIENT □QA
~MPLIANCE □ CHAIN
□EMERGENCY OF CUSTODY
STATION LOCATION:
SAMPLE TYPE
I ~REAM
□ LAKE
□ESTUARY
□ □
EFFLUENT
INFLUENT
Lab Number:
Date Recel
Rec'd b :
DATA ENTRY BY: CK:
DATE REPORTED:
Seed: Yes O No O Chlorinated: Yes O No O 0R~E~M=A~R~K~S~,'---------------------------------------------------------
Station # BP3 ,Date Begin (yy/mm/dd) I Time Begin I Date End 'Time End,Depth OM DB DBM !Value Type Composite 1Sam~le6) D O , 6 / , 2 I J _s-c;-o , A If L T s B GNXX
1 BODS 310 mg/I Chloride 940 mg/I NH3 as N 610 mg/I LI-Lithium 1132 i 2 COD lllgh 340 mg/I Chi a: Tri 32217 ug/1 TKN as N 625 mg/I Mg-Magnesium 927
3 COD Low 335 mg/I Chi a: Corr 32209 ug/1 N02 plus N03 as N 630 mg/I Mn-Manganese 1055 ug/1
4 Coliform: MF Fecal 31616 /100ml Pheophytln a 32213 ug/1 P: Total as P 665 mg/I Na-Sodium 929 mg/I
5 Coliform: MF Total 31504 1100ml Color: True 80 Pt-Co P04 as P 70507 mg/I Arsenlc:Total 1002 ug/1
6 Coliform: Tube Fecal 31615 1100ml Color:(pH I 83 AOMI P: Dissolved as P 666 mg/I Se-Selenium 1147 ug/1
7 Coliform: fecal Strep 31673 1100ml Color: pH 7 .6 82 ADMI Hg-Mercury 71900 ug/1
8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd-cadmium 1027 ug/1 Organochlorlne Pesticides
9 Volatile 505 mg/I Fluoride 951 mg/I Cr-Ouomfum:Total 1034 ug/1 Organophosphorus Pestiddes
10 Fixed 510 mg/I Formaldehyde 71880 mg/I Cu-COpper 1042 ug/1
11 Residue: Suspended 530 mg/I Grease and Olis 556 mg/I NI-Nickel 1067 ug/1 Acid Herbk:ldes
12 Volatile 535 mg/I Hardness Total 900 mg/I Pb-Lead 1051 ug/1
13 Fixed 540 mg/I Specific Cond. 95 uMhos/cm 2 Zn-Zinc 1092 ug/1 V Base/ Neutral Extractable Organics
14 pH 403 units MBAS 38260 mg/I V f'\cld Extractable Organics
15 Acidity to pH 4.5 436 mg/I Phenols 32730 ug/1 A~llver 1077 ug/1 / 16 Acidity to pit 8.3 435 mg/I Sulfate 945 mg/I Al-Aluminum 1105 ug/1 v · t'urgeable 0'1 anlcs (VOA bottle re.
17 Alkallnlty to pH 8.3 415 mg/I Sulfide 745 mg/I Be-Beryllium 1012 JI!.
18 Alkallnlty to pit 4.5 410 mg/I Ca-Calcium 916 pg/I ' \ 19 TOC 680 mg/I Co-Cobalt 1037 ~~/I \
20 Turbidity 76 NTU Fe-Iron 1045 ug/1\ \ Phytoplanklt
J ' ' Sampling Point !I; Conductance at 25 C Water Temperature fC 0.0. mg.,1 pll Alkallnlty -Addi ' Air Tempetature fC)
300 3 ,.4(
pH 8.3 pH4.5 pH 4.5 pH 8.3
2 94 l I Z.S--10 6, ~ 400 I• 82244 431 82243 82242 20 Sallnlty !I; Preclpltlon On/day) Cloud Cover ~ Wind Dlrecdon (Deg) Stream Aow Severity Turbidity Severity Wind Velocity M/H Mean Stream Depth f t. Strl?am Width ft.
480 0. ( 45 32 36 1351 1350 35 64 •
!
DMl/Revtsed 10/86
ENR/DWQ LABORATORY LAB NO. YW0380 ' VOLATILE ANALYTICAL REPORT
f-EPORTED BY ~ SUPERVISOR
CHECKED BY DATE
REVIEWED BY
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE ---'ll D
75-35-4 1. 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 trans-1.2-Dichloroethene 0.75 u 95-49-8 2-Chlorototuene 0.25 u
75-34-3 1.1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2,2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1,2-Oichtoroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chlorororm 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u • 74-97-5 Bromochloromethane 0.75 u 96-12-8 1, 2-Dibromo-3-Chloropropane u
71-55-6 1. 1-Trichloroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobutadiene 0.25 u
56-23-5 Ca1bon Tetrachloride 0.75 u 87-61-6 1.2.3-Trichlorobenzene 0.75 u
107-06-2 1.2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-butyl ether 5 u
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1,2-Dichloropropane 0 25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomethane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1.3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 tians-1,3-0ichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1.1.2-Trichloroethane 0.25 u 98-82-8 tsopropylbenzene u
127-18-4 T etrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-0ichloroprapane 0.25 u 108-67-8 1.3.5-Trimethylbenzene u
124-48-1 Oibromochloromethane 0.75 u 98-06-6 tert-Butytbenzene u
106-93-4 1.2-Oibromoethane u 95-63-6 1,2.4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u
630-20-6 1.1.1.2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u • 75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene u
79.34.5 1.1.2.2-Tetrachloroethane 0.75 u 91-20-3 Naphthalene u
:·:, .. mg/L mg/l
TOL-Target Quantitation limit-Subject to Gasoline Range Estimated :'rotiit Pe_trcit_~_L_~:H;~~6carbon 0.20 N
change due to instrument sensitivity . · .
T-Tentatively Identified, not confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ugtl
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D-Detected below quantitation limit DETECTED BY GC/ELCD/PID.
M-GC/MS Analysis performed
)MMENTS _/ ~
ENR/DWQ LABORATORY LAB NO. YW0380
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR~
CHECKED BY DATE ~
REVIEWED BY
ENTERED BY i1..-l ff/
SAMPLE TYPE: WATER ANALYSIS RESULTS OATE ~ / ~ ,'l:,,,"3-0l)
62-53-3 ANILINE 10 u 606-20-2 2,6-DINITROTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANILINE 50 u
111-44-4 BIS(2,CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITRO PHENOL 50 u
541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1,4-DICHLOROBENZENE 10 u 132-64-9 DIBENZOFURAN 10 u • 100-51-6 BENZYL ALCOHOL .20 u 121-14-2 2,4-0INITROTOLUENE 10 u
95-50-1 1,2· OJCHLOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 BIS(2-CHLOROISOPROPYL) ETHER 10 u 86-73-7 FLUORENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NfTROANILINE 50 u
621•64-7 N-NITROS0-0I-N-PROPYLAMINE 10 u 534-52-1 4,6-0lNITR0-2-METHYL PHENOL 50 u
67-72-1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSOOIPHENYLAMINE 10 u
98-95-3 NITROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u ll8-74-l HEXACHLOROBENZENE 10 u
55.75.5 2-NITRO PHENOL 10 u 87-86-5 PENTACHLORO PHENOL 50 u
105-67•9 2.4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZO!C ACID 50 u 120·12-7 ANTHRACENE 10 u
111-91-1 BIS(2-CHLOROETHOXY) METHANE 10 u 84-74-2 D1-N-BUTYL PHTHALATE 10 u
120-83-2 2,4-DICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u
120-82·1 1,2.4-TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOROANILINE 20 u 91-94-1 3,3'-0ICHLOROBENZIDINE 20 u
87-68-3 HEXACHLOROBU T ADIENE 10 u 55.55.3 BENZO(A)ANTHRACENE 10 u
59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u • 91.57.5 2-METHYL NAPHTHALENE 10 u 117-81-7 8IS(2-ETHYLHEXYL) PHTHALATE 10 u
77.47.4 H EXACHLOROCYCLOPENT ADI ENE 10 u 117-84-0 DI-N-OCTYL PHTHALATE 10 u
88-06-2 2.4.6-TRICHLORO PHENOL 10 u 205.99.2 BENZO(B)FLUORANTHENE 10 u
95.95.4 2.4.5-TRICHLORO PHENOL 10 u 207-08-9 BEN ZO(K)F L UORANT HEN E 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO(A)PYRENE 10 u
88-74-4 2-NITROANILINE so u 193-39-5 IN DENO( 1,2,3-CO)PYRENE 10 u
131-11·3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZO(A,H)ANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 BENZO(G,H,l)PERYLENE 10 u
r 1 ;
' J ~
SEMIVOLATILE ORGANICS REPORT-DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
COMMENTS:
LAB NO. YWO38O ---~~
TQL· Target Quantitation Limit-Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding lime exceeded
-------------------------------------------------------
•
•
COUNTI'
Rl\'[R BASIN :
REPORT TO
01htr :
COLLtCTOR(SJ :
Eslim•tNI BOD R1n1f:
Sttd:
RECEIVED
MAR O 8 2000
DIVISION OF \VATER QUALITY
BY:
!Kl SAMel EIHE
~NOVER CRIQRlIY □ AMDIENr D QA El STREAM
WIRO Regional Office El COMPLIANCE D CHAIN OF CUSTODY □ LAKE
□ !:MERGENCY
COLBY □ ESTUARY
Station Loc11ion: HERITAGE PARK RD AND IJLUE CLAY RD
Chlorinated: Rcmuks:
□ EFFLUENT
□ INFLUENT
D
Lab Number
Date Received:
Time RCC"eivcd:
Rec-eived By
Data Rckased :
Date Reponcd :
YW0381
1/31/2000
11:45AM
BMW
AR
2/23/2000
D11t Btgln (yy/mm/dd) Dale End (yy/mm/dd) Time lkgin Time End Depth -DM, DB, DBM Value Typc-. A, H, L Compo1ltt-T, S, B Sample T)'pe •
,B~P~•~---------~---~'0000=~1~2~!-----~~---------~~~1600=---~----~------------~----------~------~------~
Stuion #
BOD 310 m~/L Chloride 940 m•IL NHJas N 610 m,vl Li-Lithium 1132 "'IL
COOlfiah 340 rng/L Chi a: Tri 32217 UJZ/L TKN an N 625 mg/L Mg-Magnesium 927 m11:/L
COD low JlS mgtL Chi a: Corr 32209 UJZ/L N02 clus N03 as N 630 m"L Mn-Manganese l055 "<IL
Coliform: MF Fecal 31616 1100ml Phcoohytin a 32213 UJZ/L P: Total as P 665 m'"L Na-Sodium 929 mvl
Coliform: MF Total 3150.t /IOOml Color. True 80 c.u. P04 as P 70507 m'"L Arsenic:Total 1002 ,.1L
Coliform: tube Fecal 3161S 1100ml Color: (CJH) 83 tiH= c.u. P: Dissolved as P 666 m,vl Sc-Selenium 1147 "'/L
Coliform: Fecal Su~ 31673 1100ml Color: pH 7.6 82 c.u. K-Potassium mg/L Hg-Mercury 71900 u11./L
Residue: Total 500 mg/L Cyanide 720 mvl Cd-Cadmium 1027 ""L Ba_Barium "<IL
Volatile 505 mg/L Fluoride 951 mJZIL Cr-Chromium:Total 1034 ""L Orl!..l nochlorinc Pesticides
Fixed 510 m11./L Formaldehvde 71880 m2/L Cu• Con,.....r 1042 "'"L Or2.a nophosphorus Pesticides
Residue: Susr,cndcd 530 m11./L Grease and Oils 556 m2/L Ni-Nickel 1067 ",vl
Volatile 53S m1:VL Hardness Total 900 m<>/L Pb-Lead 1051 "g/L Acid Herbicides
Fixed S40 mg/L Sn-rific Cond. 95 umhos/cml Zn• Zinc 1092 u11./L
I nH 403 unit! MBAS 38260 m'"L V-Vanadium u2/L X Base/Neutral&Acid Extractable Or.izanics
Aciditv 10 oil n 436 m11./L Phenols 32730 u2/L Ast· Sih·er 1077 u2/L TPH Diesel Range
Acidi1v to till 8.3 435 m)!tL Su!fale 945 ml!./L Al• Aluminum 1 \OS ui:i/L
Alblinitv 10 nit 8.3 415 mg/L Sullidc 745 m11./L Be· Ber.-llium 1012 "'"L X Pur~able Or2.anics (VOA bottle rea'd)
Alblinitv 10 nit 4.5 410 m11./L
TOC680 miz/L
Boron
Tannin & Li~in u<>/L
Ca-Calcium 916 m,vl
Co-Cobalt 1037 "WL
TPH Gasoline Range
TPHIBTEX Gasoline Range • Turbiditv 76 NTU llexavalcnl Chromium ui:i/L Fe-Iron 1045 ui:i/L Phvtoplankton
Coliform To1al Tube ~1100 mis
COMMENTS:
DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALIT ·t FIELU·LAB FORM (DM 1)
COUNTY . !Jt._
RIVER BASIN
REPORT TO:.ARO FRO MR
AT BM
Othar
WSRO TS
Shipped by: Bus cQstaff, 9,Jrer~+,--------
COLLECTOR(S): l-c? I 'o
E■tlmated BOD Range: 0·5/5·25/25-65/40-1 plus
PRIORITY
□AMBIENT
~MPLIANCE
□EMERGENCY
□ □
STATION LOCATION:
QA
CHAIN
OF CUSTODY
SAMPLE TYPE
I i:ii-i;;;EAM
□ LAKE
□ESTUARY
□ □
EFFLUENT
INFLUENT
Lab Number:
Date Recel
Rec'd b :
DATA ENTRY BY:
DATE REPORTED:
CK:
Seed: Yu O No D Chlorinated: Yes O No O REMARKS: ===~------------------------------------------
Station # GP4 l°Oe~e~lo(;y/mlzt' 11•ze;in I Daiei End • I Time End I Depth DM DB DBM 'Value Type Composite ISam~leGJ A H L T s B GNXX
1 BODS 310 mg/I Chloride 940 mg/) Nli3 aa N 610 mg/I LI-Lithium 1132 ii 2 COD l-llgh 340 mg/I Chi a: Tri 32217 ug/1 TKN as N 625 mg/I Mg-Magnesium 927
3 COD Low 335 mg/I Chi a: Corr 32209 ug/1 N02 plus N03 as N 630 mg/I Mn·Manganese 1055 ug/1
4 Coliform: MF Fecal 31616 1100ml" Pheophytln a 32213 ug/1 P: Total as P 665 mg/I Na·Sodlum 929 mg/I
5 Coliform: MF Total 31504 1100ml Color: True 80 Pt·Co P04 as P 70507 mg/I Arsenlc:Total 1002 ug/1
6 ColHorm: Tube Fecal 31615 1100ml Color:(pH ) 83 AOMI P: Dissolved as P 666 mg/I Se·Selenlum 1147 ug/1
7 Collform: Fecal Strep 31673 1100ml Color: pH 7 .6 82 AOMI Hg·Mercury 71900 ug/1
8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd-Cadmium 1027 ug/1 Organochlortne Pesticide.
9 Volatile 505 mg/I Fluoride 951 mg/I CrChromlum:Tota.11034 ug/1 OrganophosplOrus Pesticides
10 Fixed 510 mg/I Formaldehyde 71880 mg/I Cu..COpper 1042 ug/1
II Re11ldue: Suspended 530 mg/I Grease and Olis 556 mg/I NI-Nickel 1067 ug/1 Acid Herbkkles
12 Volatile 535 mg/I Hardness Total 900 mg/I Pb·Lead 1051 ug/1
13 Fixed 540 mg/I Specific Cond. 95 uMhos/cm 2 Zn--Zlnc 1092 ug/1 V Base/ Neutral Extractable Organics
14 ptl 403 units MBAS 38260 mg/I V Acid Extractable Organics
15 Acidity to pH 4.5 436 mg/I Phenols 32730 ug/1 Ar,::,llver 1077 ug/1
16 Acidity to pH 8.3 435 mg/I Sulfate 945 mg/I Al·Alumlnum 1105 ug/J V 'Purgeable Organlc11 (VOA bottle reg.
17 Alkalinity to pH 8.3 415 mg/I Sulflde 745 mg/I B~Berylllum 1012 ug/1
18 Alkallnlty to pf-I 4.5 410 mg/I Ca-Calcium 916 mg/I
19 TOC 680 mg/I Co-Cobalt 1037 ug/1 ' 20 Turbidity 76 NTU Fe·lron 1045 ,. fhytop nkton \
I ' ,
Sampllng Point ,t Conductance at 25 C lwater Temperature K: D.0. mg/I pH Alkallnlty
_)"• 3,
Alr1 .. 1u .. 1'.:l
oi.l c, 300 S-:.23
pH 8.3 pH4.5 pH 4.5 pH 8.3
2 94 I 10 ' I 400 I• 82244 431 82243 182242 20
Salinity ,t Preclpltlon On/day) Cloud Cover ~ Wind Direction (Deg) l,Stream Flow Severity Turbidity Severity Wind Velocity M/H r-,:ean Stream Depth ft. Sueam l,:ith ft.
CJ' ( .
480 45 32 36 1351 1350 35 64 4
DM111tP.vl~d 10/M --
ENRIDWQ LABORATORY LAB NO. YW0381
~ VOLATILE ANALYTICAL REPORT
REP.ORTE □ BY SUPERVISOR
CHECKED BY DATE
REVIEWED BY
ENTERED BY.
SAMPLE TYPE: WATER ANALYSIS RE SUL TS DATE
75-35---4 1, 1-Dichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
75-09-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 trans-1,2-Dichloroethene 0.75 u 95-49-8 2-Chlorotoluene 0.25 u
75-34-3 1. 1-Dichloroethane 0.25 u 106-43-4 4-Chlorotoluene o.25 u
590-20-7 2.2-Dichloropropane 0.25 u 541-73-1 1,3-Dichlorobenzene 0.25 u
156-59-4 cis-1.2-Dichloroethene 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u • 67-66-3 Chloroform 0.25 u 95-50-1 1,2-0ichlorobenzene 0.25 u
74-97-5 Bromoch!oromethane 0.75 u 96-12-8 1.2-Dibromo-3-Chloropropane u
71-55-6 1-Trichlo_roethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 Dichloropropene 0.25 u 87-68-3 Hexachlorobuladiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1.2-Dichloroethane 0.25 u 1634-04-4 Methyl-tert-bulyl ether 5 u
79-01-6 Trichloroelhene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Brornodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomethane u 108-38-3 m,p-Xytenes 2 u
10061-01-5 cis-1.3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1.3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1. 1,2-T richloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachloroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1. 3-Dichloropropane 0.25 u 108-67-8 1,3,5-Trimethylbenzene u
124-48-1 Oibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1.2-Dibromoethane u 95-63-6 1,2.4-Trimethylbenzene u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u • 630-20-6 1.1.1.2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromolorm 0.5 u 104-51-8 n-Bulylbenzene u
79-34-5 1. 1.2.2-Tetrachtoroethane 0.75 u 91-20-3 Naphthalene u
.. _::· ··.· mg/L mgtL . .
TQL-Target Quantitation limit-Subject to Gasc;,ii~~ Range _ESti~~ied_fota1,P~trOr~~-iri. Hyd;~ciiibon 0.20 N
change due to instrument sensitivity
T-Tentatively Identified. not confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D-Detected below quantitation limit DETECTED BY GCIELCD/PID.
M-GCIMS Analysis performed
)MMEN1S· -~
~ ENR/DWQ LABORATORY LAB NO. YW0381
SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY . SUPERVISOR~
CHECKED BY jfrtr DATE ~ ~;:2
REVIEWED BY
ENTERED BY tr ,ie u
SAMPLE TYPE: WATER ANALYSIS RESULTS DATE I R, J, 'J;---0
62·53-3 ANILINE 10 u 606·20·2 2,6-DINJTROTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANIUNE 50 u
111-44-4 81S(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-DINITRO PHENOL 5D u
541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NlTRO PHENOL 50 u
106-46-7 1,4-0ICHLOROBENZENE lD u 132-64-9 DIBENZOFURAN 10 u • 100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINlTROTOLUENE lD u
95-50-1 1,2· DICHLOROBENZENE 10 u 84-66-2 DIETHYL PHTHALATE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-1 81S(2-CHLOROISOPROPYL) ETHER 10 u 86-73-7 FLUORENE lD u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NITROANIUNE 5D u
621-64-7 N-NITROSO-DI -N-PROPYLAMI NE 10 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 5D u
67-72-1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSODIPHENYLAMINE lD u
98-95-3 NITROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u 118-74-1 HEXACHLOROBENZENE 1D u
88-75-5 2-NITRO PHENOL lD u 87-86-5 PENTACHLORO PHENOL 5D u
105-67-9 2,4-DIMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 5D u 120-12-7 ANTHRACENE 1D u
111-91-1 BIS(2-CHLOROETHOXY) METHANE 10 u 84-74-2 DI-N-BUTYL PHTHALATE 1D u
120-83-2 2,4-0ICHLORO PHENOL lD u 206-44-0 FLUORANTHENE 10 u
120-82-1 1,2,4-T RICHLOROBENZENE lD u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE lD u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOROANILINE 20 u 91-94-1 3,3" · DICHLOROBENZI DI NE 20 u
87-68-3 HEXACHLOROBUTAOIENE 10 u 56-55-3 BENZO(A)ANTHRACENE 10 u
59-50-7 4-CHLOR0-3-METHYL PHENOL 20 u 218-01-9 CHRYSENE lD u • 91-57-6 2-METHYL NAPHTHALENE 10 u 117-81-7 BIS(2-ETHYLHEXYL) PHTHALATE 10 u
77-47-4 HEXACHLOROCYCLOPENTADIENE 10 u 117-84-0 DI-N-OCTYL PHTHALATE 1D u
88-06-2 2,4.6-TRlCHLORO PHENOL 10 u 205-99-2 BENZO(B)FLUORANTHENE 10 u
95.95.4 2,4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(K)FLUORANTHEN E 10 u
91-58-7 2-CHLORO NAPHTHALENE lD u 50-32-8 BENZO(A)PYRENE 10 u
88-74-4 2-NITROANILINE 50 u 193-39-5 INDENO(l,2,3-CD)PYRENE 10 u
131-11-3 DIMETHYL PHTHALATE 1D u 53-70-3 DIBENZO(A,H)ANTHRACENE lD u
208-96-8 ACENAPHTHYLENE 1D u 191-24-2 BENZO(G,H,l)PERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. YWO381 -----
TQL· Target Quantitation Limit• Subject to
change due to instrument sensitivity
T· Tentatively Identified, estimated concentration
E· Estimated Value
u. Samples analyzed for this compound but not detected
N· Sample not analyzed for this compound
D· Detected below quantitation limit
H· Holding lime exceeded
COMMENTS: __________________________________________________ _
•
•
' -··· '
~ '". -·;
'IJ -:;
:L::.== .1~
. ' . . • :t.a· . .
~ ;.,, ~~-:~ -~~ ... ~
NORTH .ROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
April 3, 2000
Mrs. Diane Barrett/ Ms. Beverly Hudson
DIVISION OF WASTE MANAGEMENT
North Superfund Remedial Branch
US EPA Region IV
61 Forsyth Street, Eleventh (11) Floor
Atlanta, Georgia 30303
RE: Analytical Results of Surface Water in the Vicinity of the Bum Pit Site
New Hanover County Airport Bum Pit
NCD 981 021 157
Wilmington, New Hanover County, NC
Dear Mrs. Barrett and Ms. Hudson:
Attached please find two copies of the analytical results from the February 3,
2000 sampling event completed by Russ Colby with the NC DENR Division of Water
Quality, at the New Hanover County Airport Bum Pit Superfund Site, located in
Wilmington, North Carolina. As you know I was present along with 3 representatives
of the Heritage Park Subdivision during sampling of these areas. Those present from
the Heritage Park Subdivision appeared to agree with the general locations that the
samples were taken from. In fact, Mr. Charlie Skipper recommended the sample
location off Hall Road (BPS).
As you can see all analytical results for contaminants of concern (COC) and
volatile organic compounds (VOCs) are non-detect (ND). If you have questions
about sampling locations or other details about the sampling/analytical results, please
contact me, at [phone], extension 341. Copies of the attached analytical data
was mailed to local residents who were present during all or part of the sampling
event and also to Bessie McKoy and Sharon Mathis who requested copies by phone.
Sincerely,
<:::ru. {:, · 1~1L ce~'\
Randy McElveen
Environmental Engineer
NC Superfund Section
cc: Grover Nicholson, N.C. Superfund Section
Linda Russell, 110 Heritage Park Drive, Wilmington
Bessie C. McKoy, 139 Pilgrim Circle, Wilmington
Sharon Mathis, 233 Heritage Park Drive, Wilmington
Teresa Prince, 222 Heritage Park Drive, Wilmington
Charles M. Skipper, 4929 Woodcrest Drive, Castle Hayne
401 OBERLIN ROAD, SUITE 1 SO, RALEIGH, NC 27605
PHONE 9!9•733-4996 FAX 919•715-3605
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER -50% RECYCLED/I 0% POST-CONSUMER PAPER
A/sp
I
i:tR~~:~~D; N e-\)j 't\ Q\1\.(1) '-' -~ '< c.~ . A'°'" P,.;t
~ \Y'I \'\ r' \ .°T S. It e
DIVISION OF WATER QUALITY
Chr.miJlry Labor■lory Report/ W•lcr Quality J3Y: .DlAJ Q
=-· @] SAMPI ETYPE COUNTY
RIVER BASIN:
NEW HANOVER
R£r0RTTO WlRO Rt"gional Office
Oth.-r :
COLLECTOR{S) :
[Jtimaled BOD Range:
Sttd,
Station#
BPI
BODJJO
COO Hi~h 3-lO
COD Low 33S
COLBY
Coliform: MF Fecal 31616
Coliform: MF Tot.al 31504
Coliform: tube Fecal 31615
Coliform: Fecal Strm JJ61J
Residue: Total 500
Volatile 505
Fixed 510
Residue: Susr><:nded 530
Vol.1.tile SJS
Fixed 540
I oH 403
Aciditv to nil 4,S 4)6
Aciditv to oll 8.3 43S
Alhlinitv 10 oil 8.3 415
Alhlinitv to nil 4.5 -110
TCX:680
Turbiditv 76
Coliform Tota.I Tube
COMMENTS:
Chlorina1Nl:
Dale lkgln (yy/mm/dd)
fRJ.QJUIY □ AMBIENT
□ COMPLIANCE
5] EMERGENCY
Uale End {n/Jnrn/dd)
m~/L Chloride 940
mg/L Chi a: Tri 32217
mll/L Chi a: Corr 32209
1100ml Pheoohv1in ,1 322 I 3
1100ml Color. True 80
/JOOml Color: {oil) 83 _pH=
/IOOml Color: tit 7.6 82
mg/L Cy.1.nide 720
m.11:/L Fluoride 951
m2/L Formaldehvde 71880
mit/L Grease and Oils 556
mg/L H.1.rdness Total 900
m.11:/L Soecific Cond. 95
units MBAS 38260
m~/L Phenols 32730
ml!IL Sulfate 945
mi;i;/L Sulfide 745
mg/L Boron
m21L Tannin & Ugnin
NTU llexavaknt Chromium
"/JOO mis
D QA 5] STREAM
D CHAIN OF CUSTODY □ LAKE
□ ESTUARY
'
Statl n Loution: 0B0U0R0Nc.,_P01 f,_ _____ ::,.L
Remar
lime lkgin
1220
Time End
m11./L
"°'L
u11/L
uiz/L
c.u.
c.u.
c.u.
m"L
m11/L
mi:i/L
m~/L
mo/L
umhos/cm2
mo/L
U<>ll
m11/L
m"/l
u2/L
UJ!:/l
Deptb • DM, DB, DBM
NIIJ asN 610
TKN an N 625
NO2 nlus NOJ as N 630
P; Total as P 665
P04 a:! P 70507
P: Dissolved as P 666
K-Powsium
Cd-Cadmium 1027
Cr-Chromium:Total 1034
Cu-Co.,~r 1042
Ni-Nkkd 1067
Pb-lead 1051
Zn-Zinc 1092
Y-V.1.n.1.dium
Ao-Silver 1077
Al-Aluminum 1105
Be-Beryllium 1012
Ca-C.1\cium916
Co-Cobalt 1037
Fe-Iron 1045
I
RECEIVED A/sb
MAR 812000
SUPt:.RFUNO SECTION
□ EFFLUENT
□ INFLUENT
[:]
Value Type-A, U, L
mg/L
m2/L
mg/L
m11./L
mg/L
mg/l
m11/L
ug/l
,wL
,vL
,,JL
,wL
Ul!./L
URIL X
,wL
u11./L
Ug/L X
Ub Number YW0592
Date Rl"'CCived: 2/4/2000
Time Recrived: IIMW
Received By : HMW
Data Released : AR
Date Reported: 2/29/2000
Composile-T, S, B Sample Type
Li-Lithium 1132 uc,/L
M11.-Mai:inesium 927 m11ll
Mn-Manganese 1055 u<>/l
Na-Sodium 929 mo,L
Anenic:Total 1002 tr"/l
Sc-Selenium 1147 u111L
1111-Merr;urv 71900 ug/L
Ba_Barium UR/L
Organochlorine Pesticides
O1ganophosphorus Pesticides
Add l le1bicides
Base/Neutral&Acid Extract.able O111.anics
TPII Diesel Range
Pur11.e.1bk Orunics {VOA bottle rea'dl
mg/L TPII Gasoline Rang,:
u11./L TFII/BTEX Gasoline R.1.nge
UR/L Phvtoolankton
•
•
DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALIT"s FIELD-LAB FORM (DMI) ® ··cbumv
AT BM
Other
WSRO TS
Shipped by: Bu•G• Staff, Other ________ _
COLLECTOR(S), Co I ~f
E•tlmated BOD Range: 0-5/5•25/25-65/40-130 or 100 plus
PRIORITY
□AMBIENT
OcoMPLIANCE D CHAIN
~ERGENCV
OF CUSTODY
STATION LOCATION: Bu"n
SAMPLE TYPE
I oa-;.;:;;;AM
□ LAKE
□ESTUARY
□ □
EFFLUENT Rec'd b :
INFWENT DATA ENTRY BY: CK,
DATE REPORTED:
Seed: Yea D No D Chlorinated: Yu O No D 0R~E~M~A=R~K~S~'----------------------------------------------------
'Station #
'
Value Type
A H L
Composite
T S GNXX
1
2
3
BODS 310
COD High 340
COD Low 335
mg/I Chlor1de 940 mg/I
mg/I Chi .ii: Tri 3221 7 ug/1
mg/I Chi a: Corr 32209 ug/1
NH3 as N 610 LI-Lithium 1132
TKN as N 625 mg/I
NO2 plu• NO3 as N 630 mg/I
ug/1 • f--+,M7n--~M7a_n_g_a_n_e-,-.-:,~0~5~5,------~ug/l
Mg-Magne•lum 927
4 Collform: MF Fecal 31616 1100ml PheophyUn a 32213 ug/1 P: Total a■ P 665 mg/I Na-Sodium 929 mg/I
5 Coliform: MF Total 31504 1100ml Color: True 80 Pt·Co P04 as P 70507 mg/I Arsenlc:Total 1002 ug/1
6 Coliform: Tube Fecal 31615 1100ml Color:(pH ) 83 ADMJ P: Dlasolved as P 666 mg/I Se-Selenium 1147 ug/1
7 Coliform: Fecal Strep 31673 /l0Dml Color: pH 7 .6 82 ADMI Hg-Mercury 71900 ug/1
8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd-<:admlum 1027 ug/1 Organochlo.-lne Pestlcldea
9 Volatile 505 mg/I Fluoride 951 mg/I Cr-Chromlurn:Tolal 1034 ug/1 Organophc16phorus Pestkkles
10 Fixed 510 mg/I Formaldehyde 71880 mg/I Cu--COpper 1042 ug/1
11 Residue: Suspended 530 mg/I Grease and OIi• 556 mg/I NI--Nlckel 1067 ug/1 Add Herbk:ldes
12 VolaCIJe 535 mg/I Hardnesa Total 900 mg/I Pb•Lead 1051 ug/1
13 Fixed 540 mg/I Specific Cond. 95 uMho•/cm 2 Zn-Zinc 1092 ug/1 I/ Base/ Neutral Extractable Organic•
14 pH 403 unlls MBAS 38260 mg/I V n.cld Extractable Organics
15 Acidity lo pH 4.5 436 mg/I Phenol• 32730 ug/1 Ag--Sllver 1077 ug/1
16 Acidity to pH 8.3 435 mg/I Sulfate 945 mg/I Al·Alumlnum 1105 ug/1
17 Alkallnlty to pH 8.3 415 mg/I Sulfide 745 mg/I Be--Berylllum 1012 ug/1
18 Alkallnlty to pit 4.5 410 mg/I Ca-Calcium 916 mg/I
19 TOC 680 me/I Co-Cobalt 1037 ug/1
20 Turbidity 76 NTU Fe•lron 1045 ug/1 ,. ~toplzmkton
Sampllng Point ,i;; Conduc1ance at 25 C Water Tempemture tC1 0.0. mg/1 pH Alkalinity Acidity Air Temperature K:)
300 ~.3 b <J
pit 8.3 pH 4.5 pH 4.5 pH 8.3
2 94 14 S 10 <g . I 4003 I• 82244 431 82243 182242 20 Sallnlly ,i;; Preclpltlon On/day) Cloud Cover ,i;; Wind Dlrttllon O)eg) Stream Flow Severity Turbidity Severity Wind Veloclly M/H Mean Stream Depth fL Stream Width IL
480 0 I I 45 0 32 cs-36 1351 1350 35 64 4
ENRfOWQ LABORATORY LAB NO, YW0592 AB,~ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY __a((:_ DATE
REVIEWED BY --4t<&
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RES UL TS DATE
75-35-4 1.1-0ichloroethene 0.75 u 96-18-4 1,2,3-Trichloropropane 0.25 u
7~9-2 Methylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 lrans-1.2-Dichloroethene 0.75 u 95-49-6 2-Chlorotoluene 0.25 u
75-34-3 1, 1-Dichloroelhane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2.2-Dichloropropane 0.25 u 541-73-1 1,3-0ichlorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene fo2s u 106-46-7 1,4-Dichlorobenzene 0.25 u • 67-66-3 Chloroform 0.25 u 95-50-1 1,2-Dichlorobenzene 0.25 u
74-97-5 Bromochloromethane 0.75 u 96-12-8 1,2-Dibromo-3-Chloropropane u
71-55-6 1, 1, 1-Trich!oroethane 0.25 u 120-82-1 1,2,4-Trichlorobenzene 0.25 u
563-58-6 1.1-Dichloropropene 0.25 u 87-68-3 HeKachlorobutadtene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2.3-Trichlorobenzene 0.75 u
107-06-2 1,2-0ichloroethane 0.25 u 1634-04-4 Melhyl-tert-bulyl ether 5 u
79-01-6 Trichloroelhene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Dibromomelhane u 108-38-3 m,p-Xylenes 2 u
10061-01-5 cis-1,3-Dichloropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1, 3-Dichloropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1,2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-16-4 Telrachloroelhene 0.25 u 103-65-1 n-Propytbenzene u
142-28-9 1,3-Dichloropropane 0.25 u 108-67-8 1.3,5-Trimethylbenzene u
124-48-1 Dibromochloromethane 0.75 u 98-06-6 tert-Butylbenzene u
106-93-4 1,2-Dibromoethane u 95-63-6 1,2,4-Trimethylbenzene u
108-90-7 Chlorobenzene 0,25 u 135-98-B sec-Butylbenzene u • 630-20-6 1, 1, 1,2-T etrachloroethane 0.25 u 99-87-6 p-lsopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Butylbenzene · u
79-34-5 1, 1,2.2-Tetrachloroelhane 0.75 u 91-20-3 Naphthalene u
Ga:s~'l;~e-R~~g~-~i;;'~-~i;~ )~,a; ·Pe:1~o;eu~ -~ydrirbo~
mg/L mgll
TQL-Target Ouanlitalion limit-Subject to 0.20 N
change due to inslrumenl sensitivity
T-T entativety ldenlified. nol confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ug/L
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound NO VOLATILE ORGANIC COMPOUNDS
D-□elected below quantilalion limil DETECTED BY GC/ELCO/PID.
M-GC/MS Analysis performed
\.____ )MMENTS·
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-53-3
108-95-2
II 1-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67•72•1
95.95.3
78-59-1
as.75.5
105-67-9
65·85-0
111·91·1
120-83-2
120-82-1
91-20·3
106-47-8
87-68·3
59.50.7
91-57-6
77.47.4
88-06-2
95.95.4
91-58-7
88-74-4
131·11·3
208-96-8
Pc...
~ I
WATER
ANILINE
PHENOL
815(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
l,3-01CHLOROBENZENE
1,4-DICHLOROBENZENE
BENZYL ALCOHOL
1.2-DICHLOROBENZENE
2-METHYL PHENOL
815(2-CHLOROISOPROPYL) ETHER
4-METHYL PHENOL
N-NITROSO-Dl•N•PROPYLAMINE
HEXACHLOROETHANE
NJTROBENZENE
ISOPHORONE
2-NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOIC ACID
BIS(2-CHLOROETHOXY) METHANE
2,4-0ICHLORO PHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTAOIENE
4•CHLOR0·3-METHYL PHENOL
2-METHYL NAPHTHALENE
H EXACHLOROCYC LOPE NT ADIE NE
2,4,6-TRICHLORO PHENOL
2,4,5-TRICHLORO PHENOL
2-CHLORO NAPHTHALENE
2•NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
I
ENR/DWQ LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
10 u 606-20-2
10 u 99-09-2
10 u 83-32-9
10 u 51-28-5
10 u 100-02-7
10 u 132-64-9
20 u 121-14-2
10 u 84-66-2
10 u 7005-72-3
10 u 86-73-7
10 u 100-01-6
10 u 534-52-1
10 u 86·30-6
10 u 101.55.3
10 u 118•74•1
10 u 87•86-5
10 u 85·01-8
50 u 120-12•7
10 u 94.74.2
10 u 206-44-0
10 u 129-00-0
10 u 85-68-7
20 u 91•94•1
10 u 56-55-3
20 u 218-01·9
10 u 117-81-7
10 u 117-84-0
10 u 205-99·2
10 u 207-08-9
10 u 50-32-8
50 u 193.39.5
10 u 53.70.3
10 u 191-24·2
2,6-DINITROTOLUENE
3-N1TROAN1LINE
ACENAPHTHENE
2,4-DINITRO PHENOL
4-NITRO PHENOL
DIBENZOFURAN
2,4,0INITROTOLUENE
DIETHYL PHTHALATE
4-CHLOROPHENYL PHENYL ETHER
FLUORENE
4-NITROANILINE
4,6·DINITR0·2·METHYL PHENOL
N•NITR0S001PHENYLAMINE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PENTACHLORO PHENOL
PHENANTHRENE
ANTHRACENE
01-N•BUTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYL PHTHALATE
3,3'-0ICHLOROBENZIOINE
BENZO(A)ANTHRACENE
CHRYSENE
8IS(2•ETHYLHEXYL) PHTHALATE
Dl•N•OCTYL PHTHAL.ATE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO(A)PYRENE
INOENO(l,2,3·CD)PYRENE
OIBENZO(A,H)ANTHRACENE
BENZO(G,H,l)PERYLENE
LAB NO, YW0592
SUPERVISOFfff
DATE _✓
ENTERED BY . I §1 r)
DATE .?. -2' ~o .
10 u
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
._•10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
. 10 u
•
•
SEMIVOLATILE ORGANICS REPORT· DWQ LAB PAGE 2 LAB NO. -~YW=0~5~9~2
NO BASE /NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
__________ TQL-Target Quanlitation limit• Subject to
change due to instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
0-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: ______________________________________________ _
•
•
RECEIVED
MAR O 8 2000
BY:
DIVISION OF WATER QUALITY
Cbtmiltry Laboratory Report !Waler Qualily
SAMfl EmE COUNTY
RIVER BAS(N :
~NOVER
□ = ~
REPORT TO WIRO
Olhtt :
COLLECTOR(S) : COLBY
Estimaltd BOD R.ngt:
..... ,
BPl
BODJI0
COD Hi2h .k0
CODl.owJH
Colifoun: MF Fecat ]1616
Coliform: MF Tot.11 31504
Colirorm: tube Fecal 31615
Coliform: Fecal 5,....., 31673
Residue: Total SOO
Volatile SOS
Fixed SIO
Residue: Sus,._,,,1.-..1 SJO
Volatile S3S
Fixed S40
I DII 403
Aciditv to oil 4.S 436
Ariditv 10 DH 8.3 435
AIUlinirv to pH 8.l 41S
Alb.linihl to pH 4.S ◄ 10
TOC 680
Turbiditv 76
Coliform Toul Tube
COMMENTS:
Regional Office
Chlorinatrd:
Datt •gin (yy/mm/dd)
2000020]
mg/L
mall
mg!L
1100ml
1100ml
/JOOml
1100ml
mg/L
mg/L
mg/L
m11/l
mRIL
m'1L
units
mgll
m,JL
m,JL
mg/l
mgtL
NTU
"/100 mis
AMBIENT
□ COMPllANCE
{KJ EMERGENCY
Dalt End (yy/mm/dd)
Chloride 940
Chla:Tril2217
Chi a: Corr 32209
Pheoohvtin a 322IJ
Color. True 80
Color. (oil l 83 nil::
Color. oH 7.6 82
"'anide 720
Fluoride 9SI
Formald(hvde 71880
Grease and Oils SS6
Hardness Total 900
S -'lie Cond. 9S
MBAS 38260
Phenols 32730
Sulfate 94S
Sullide 70
Boron
Tannin & u~in
Hexavaknt Chromium
□QA Lu STREAM
D CHAIN OF CUSTODY □ I.AKE
□ ESTUARY
Slatlon Location: BP SIDE OF BLUE CU Y RD
Rtmulu:
Tlmt Begin
1250
Time End
m,JL
URIL
u_1t/L
u2/L
c.u.
c.u.
c.u.
m,JL
m.ct/L
mg/L
m11/L
m11./L
umhostcm2
mgtL
URIL
mRIL
mRIL
ug/L
URIL
lkplh. DM, DB, DBM
NHl asN 610
TKN anN 62S
NO2 o1us NO3 as N 630
P: Total as P 66S
PO4 as P 70507
P: Dissolved as P 666
K-Potasslum
Cd-Cadmium 1027
Cr-Chromlum:Total 1034
Cu-Connt"r 1042
Ni-Nickel 1067
Pb-lead I OS I
Zn-Zinc I 092
V-Vanadium
Ag-Silver 1077
Al-Aluminum 1 I0S
Be-Ber.Ilium 1012
Ca-Calcium 916
C~Cobalt 1037
Fe-hon 104S
□ EFFLUENT
□ INFLUENT
G
Value Type• A, II, L
mML
ma/L
m11/L
ma/L
m11/L
mg/L
mo/L
,,JL
,'1L
"'IL
,o/L
u<IL
ug/L
ua/L X
URIL
u2/L .. ug/L X
m•IL
ua/L
URIL
Lab Number
Date Received :
Time Received:
Recrivcd By :
Data Released :
Date Rq,oned :
YW0593
2/4/2000
9:40AM
HMW
AR
2/29/2000
Composite-T, S, D Sample Type
LI-Lithium 1132
Ma-Ma2neslum 927
Mn-Mani.:ancse 1055
Na-Sodium 929
Arscnic:Total 1002
Se-Selenium 1147
HR-Mercurv 71900
Ba_Barium
Oriµnochlorinc Pesticides
Organophosphorus Pesticides
Arid Herbicides
"'/L
m2/L
u~/L
mo/L
,,,t
uiz/L
u,JL
u•/L
Base/Neutral&Acid Extractable Organics
TPII Diesel RanRe
Pur;::eable Ori;:anics (VOA bottle ....,,'d)
TPH Gasoline Range
TPH/BTEX Gasoline Rans::e
PhvtnnJankton
DIVISION OF ENVIRONMENTAL MANAGEMENT
N(l_.__, WATER QUALITY FIELD-LAB FORM (DM I) CID ·t:OUNTY
RIVER BASIN
REPORT TO: ARO FRO MR0 ARO Wan
AT BM
Othar
PRIORITY
WSRO TS
SAMPLE TYPE
□QA
□ CHAIN
□ □
EFFLUENT
INA.UENT
Shipped by: Bu•~• Stall, 0tf'er--,-______ _
□AMBIENT
OcoMPLIANcE
~ERGEN~Y
OF CUSTODY I ~EAM
□LAKE
OesTUARY
coLLEcT0•1s>, Co I b {
I
Estimated BOD Range: 0•5/5-25/25-65/4CH30 or 100 plus STATION LOCATION:
5Hd: YH O No D Chlorinated: YH D No D REMARKS:
I Station # 3P3 l°ate Begin {yy/mm/dd) I Time Begin I Dale End I Time End I Depth OM OB DBM I Value Type 0O.oz,03,zs-o , . ·AH
1 80D5 310 mg/I Chlor~de 940 mg/I NH3 H N 610
2 COD High 340 mg/I Chi 11: Tri 32217 ug/1 TKN 1111 N 625
3 COD Low 335 mg/I Chi 11: Corr 32209 ug/1 N02 plu• N03 111 N 630
4 Coliform: MF Fecal 31616 1100ml Pheophytln a 32213 ug/1 P: Total aa P 665
5 Collform: MF Total 31504 1100ml Color: True 80 Pt-Co P04 HP 70507
6 Coliform: Tube Fecal 31615 1100ml Color:(pH ) 83 ADMI P: Dl11olved H P 666
7 Coliform: Fecal Strep 31673 1100ml Color: pH 7 .6 82 ADMI
8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd~dmlum 1027
9 Volatile 505 mg/I Fluoride 951 mg/I CrChromlum:TotaJ 1034
10 Fixed 510 mg/I Formaldehyde 71880 mg/I Cu-COpper 1042
11 Ruldue: Su•pended 530 mg/I Grease and Olis 556 mg/J NI-Nickel 1067
12 Volatile 535 mg/I Hardnesa Total 900 mg/I Pb-Lead 1051
13 Fixed 540 mg/I Specific Cond. 95 uMhos/cm 2 Zn-Zinc 1092
14 pH 403 units MBAS 38260 mg/I
15 Acidity to pH 4.5 436 mg/I Phenol• 32730 ug/J Ag-Sliver 1077
16 Acidity to pH 8.3 435 mg/I Sulfate 945 mg/I Al-Aluminum 1105
17 Alkallnlty to pH 8.3 415 mg/I Sulllde 745 mg/I Be-Berylllum 1012
18 Alkallnlty to pH 4.5 410 mg/I Ca-Calcium 916
19 T0C 680 mg/I Co-Cobalt 1037
20 Turbidity 76 NTU Fe-Iron 1045
Sampling Point " Conductance at 25 C fwater Tempenitun!! J:; D.0. mg/I pH Alkallnlty
11 er, f.s 300~ ,.1~ 400 4 ,.5 pl-f 8.3 pft 4.5 pH 4.5
2 94 10 82244 431 82243
DATA ENTRY BY: CK:
DATE REPORTED:
Compo•lte 1Sam~le035 L T s B GNXX
mg/I LI-Lithium 1132 ""n I
mg/I Mg-Magnesium 927 • mg/I Mn-Manganese 1055
mg/I Na-Sodium 929 mg/I
mgn Arsenlc:Total 1002 ug/1
mgn Se-Selenium 1147 ug/1
Hg-Mercury 71900 ue/1
ugn 0rganochlorlne Pe•tlclde•
ug/1 Organophospxm..is Peslkld.es
ug/1
ug/1 Acid Herbkldes
ugn
ug/1 V Base/ Neutral Extractable Organics
v 11\cld Extractable Organics
ug/1 -
ug/1 V Purgeable Organics (VOA bollle reg'd) .
ug/1 .,-.1. ~
mg/I .. , • I
ug/1 ll...oll" .. ~ II
ug/1 Phytoplankton •
Acidity Air Temperature IC)
pli 8.3
182242 20
Salinity " Preclpltlon On/day) Cloud Cova S
'7s-
Wind Direction (Deg) Stream Row Severity Turbidity Severity Wind Veloclty M/H Mean Stream Depth ft. Stream Width ft.
480 C) . I 45 0 32 36 1351 1350 35 64 •
DMI/R«vtwd 10/86
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75.34.3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-58-6
56-23-5
107-06-2
79-01-6
78-87-5
75-27-4
74.95.3
10061-01-5
10061-02-6
79-00-5
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
75-25-2
79.34.5
TOL-
T-
E-
WATER
1, 1-Dichloroelhene
Methylene Chloride
trans-1,2-0ichloroethene
1, 1-Dichloroelhane
2.2-Dichloropropane
cis-1,2-Dichloroethene
Ch1orororm
Bromochloromelhane
1, 1, 1-Trichloroethane
1.1-0ichloropropene
Carbon Tetrachloride
1.2-Dichloroe\hane
T richloroethene
1.2-Dichloropropane
Bromodichtoromethane
Dibromomethane
cis-1,3-Dichloropropene
trans-1, 3-0ichloropropene
1.1.2-Trichloroelhane
T etrachloroethene
1,3-0ichloropropane
Dibromochtoromelhane
1.2-Dibromoethane
Chlorobem:ene
1, 1, 1,2-Tetrach1oroelhane
Bromolorm
1.1,2.2-Tetrachloroethane
Target Quantilation limit-Subject to
change due to Instrument sensitivily
Tentatively Identified, not confirmed
Estimated Value
0.75
10
0.75
0.25
I'-''
0.25
0.25
0.75
0.25
0.25
0.75
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
0.25
0.25
0.5
0.75
U-Samples analyzed for this compound but not detected
N-
D-
M-
JMMENTS;
Sample nol analyzed for this compound
□elected below quantitation limit
GC/MS Analysis performed
ENRfDWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RES UL TS
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
96-18-4
108-86-1
95-49-8
106-43-4
541-73-1
106-46-7
95-50-1
96-12-8
120-82-1
87-68-3
87-61-6
1634-04-4
71-43-2
108-8B-3
100-41-4
108-38-3
95-47-6
100-42-5
98-82-8
103-65-1
108-67-8
98-06-6
95-63-6
135-9B-8
99-87-6
104-51-8
91-20-3
1,2,3-Trichloropropane
Bromobenzene
2-Chlorotoluene
4-Chlorotoluene
1,3-0ichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Ch1oropropane
1,2,4-Trichlorobenzene
Hexachtorobutadiene
1,2,3-Trichlorobenzene
Methyl-tert-butyl ether
Benzene
Toluene
Ethyl benzene
m,p-Xylenes
o-Xylene
Styrene
lsopropylbenzene
n-Propy1benzene
1,3,5-Trimethylbenzene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-lsopropyltoluene
n-Butylbenzene
Naphthalene
Other purgeables detected
(up lo 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
---------------~~-----~
LAB NO. YW0593
SUPERVISOR~
DATE
ENTERED BY 1 f
DATE {)0-/lp,,..Q LJ
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.25
0.75
5
2
mg/L
0.20
mg/L
Detected
ug/L
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
N
•
•
ENR/DWQ LABORATORY LAB NO, YW0593 Pc.. SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY ~ SUPERVISOR~ · CHECKED BY DATE ' f,J
REVIEWED BY
ENTEREDBY~ SAMPLE TYPE: WATER ANALYSIS RESULTS DATE --o 0
62-53-3 ANILINE IO u 606-20-2 2,6-DINITROTOLUENE 10 u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANILINE 50 u
111-44-4 8IS(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE 10 u
95-57-8 2-CHLOROPHENOL IO u 51-28-5 2,4-0INITRO PHENOL 50 u
541-73-1 1,3-DICHLOROBENZENE 10 u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1,4-DICHLOROBENZENE IO u 132-64-9 DIBENZOFURAN 10 u • 100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE 10 u
95-50-1 1,2-0ICHLOROBENZENE IO u 84-66-2 DIETHYL PHTHALATE IO u
95-48-7 2-METHYL PHENOL IO u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
108-60-J 8IS(2-CHLOROISOPROPYL) ETHER IO u 86-73-7 FLUORENE 10 U·
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-NITROANILINE 50 u
621-64-7 N•NITROS0-01-N-PROPYLAMINE 10 u 534-52-1 4,6-DINITR0-2-METHYL PHENOL 50 u
67-72-1 HEXACHLOROETHANE 10 u 86·30-6 N-NITROSODIPHENYLAMINE 10 u
98-95-3 NITROBENZENE 10 u 101-55-3 4-BROMOPHENYL PHENYL ETHER 10 u
78-59-1 ISOPHORONE 10 u 118-74-1 HEXACHLOROBENZENE 10 u
88•75-5 2-NITRO PHENOL 10 u 87-86-5 PENTACHLORO PHENOL 50 u
105-67-9 2,4,0IMETHYL PHENOL 10 u 85-01-8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120-12-7 ANTHRACENE 10 u
111-91-1 815(2-CHLOROETHOXY) METHANE 10 u 84-74-2 01-N-BUTYL PHTHALATE 10 u
120-83-2 2,4-0ICHLORO PHENOL 10 u 206-44-0 FLUORANTHENE 10 u
120-82-1 1,2,4-TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91-20-3 NAPHTHALENE 10 u 85-68-7 BUTYLBENZYL PHTHALATE 10 u
106-47-8 4-CHLOROANILINE 20 u 91-94-1 3,3'-0ICHLOROBENZIDINE 20 u
87-68-3 HEXACHLOROBUTAOIENE 10 u 56-55-3 BENZO(A)ANTHRACENE ..... ·10 u
59-50-7 4-CHLOR0-3•METHYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
91-57-6 2-METHYL NAPHTHALENE IO u 117-81-7 818(2-ETHYLHEXYL) PHTHALATE 10 u • 77.47.4 HEXACHLOROCYCLOPENTA01ENE 10 u 117-84-0 01-N-OCTYL PHTHALATE 10 u
88-06,2 2.4,6-TRICHLORO PHENOL IO u 205-99·2 BENZO(B)FLUORANTHENE . 10 u
95.95.4 2,4,5-TRICHLORO PHENOL 10 u 207-08-9 BENZO(K)FLUORANTHENE 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO(A)PYRENE 10 u
88-74-4 2•NITROANIUNE 50 u 193-39-5 INDENO(l,2,3·CO)PYRENE 10 u
131-J 1-3 DIMETHYL PHTHALATE 10 u 53-70-3 DIBENZO(A,H)ANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191-24-2 B ENZO(G, H, l)PERYL ENE 10 u
SEMIVOLATILE ORGANICS REPORT· DWQ LAB PAGE 2 LAB NO. _ ___,YW=0-"'5-"-93=.
NO BASE/ NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
__________ TQl• Target Quantitation limit-Subject to
change due to instrument sensitivity
T· Tentatively Identified, estimated concentration
E-Estimated Value
U· Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: ______________________________________________ _
•
7--1
I
I
I I i COUNn'
Rl\'f.R B.\SIN:
REPORT TO
Olhrr :
COLUCTOR(S) :
l
«.t<~CEIVED !
MAR OB 2000 /
. I BY: I DIVISION OF WATER QUALITY
I Chrmlrll'J' Labor•lory Rrrort I \V•trr Q11allty
NEW HANOVER P.RIQB.IIX □ AMDIENT D QA
~ SAMPI ETVPE
(R] STREAM
~ Regional Office □ COMPLIANCE D CHAIN OF CUSTODY □ LAKE
COLBY
[!] EMERGENCY □ ESTUARY
St•tlon Localion: HERITAGE PARK AND BLUE CLAY RD
St1lio11 •
BP4
BOD 310
COD Hi~ J.io
COD low HS
Coliform: MF Fecal 31616
Colirorm: MF Total JI 504
Colfronn: tube Fecal 31615
Coliform: Fecal Su..., 31673
Residue: Toul 500
Vola1ile SOS
Fixed SIO
Residue: Susnrndc:d 530
Volatile 535
Fi~ed 540
I nil 403
Acidirv 10 r ti ,U 436
AcidilV lo ell 8.3 435
Alkalinirv to tiff 8.3 415
Allalinirv to nil 4.5 410
TOC680
Turbidirv 76
Coliform Total Tube
CO/11/ll[NTS:
Chlorfn•lrd:
Dalt IN,gln (yy/mm/dd)
20000203
mR/L
mlo!IL
mall
1100ml
1100ml
/IOOml
/IOOml ·
m11:/L
m0 'L
m"/L
mi,/L
ml!/L
mn/L
uniu
m11:/L
m0tl
m<>/L
ml!/L
m11/L
NTU
"/IOOmls
Remnks:
Dalt End (yy/m dd) Tlmt End Dtplb -DM, DD, DBM
Chloride 940 m11/L NHl asN 610
Chi a: Tri 32217 URIL TKN anN 62S
Chi a: Corr 32209 u0 /L NO2 olus NOJ as N 630
Phconh.,tin a 32213 uo-/L P: Total as P 66S
Color. True 80 c.u. PO4 as P 70507
Color. (oll ) 83 011-c.u. P: Diuolved as P 666
Color. nH 7.6 82 c,u. K•Potas.slum
Cvanidc 720 m11/L Cd-Cadmium l027
Fluoride 951 m0/L Cr--Chromium:To1al lOJ4
Formaldehyde 71880 mo/L Cu-Con..,..,.1042
Grease and Oils S56 mo/L Ni•Nickcl 1067
Hardness Total 900 m11/L Pb-Uad 1051
s.....,..;r.c Cond. 95 umhos/em2 Zn. Zinc 1092
MBAS 38260 m11/L V-Vanadium
Phenols 32730 Ul!'.IL Ao-Silver 1077
Sulfate 94S m0 /L Al• Aluminum 1105
Sulfide 745 m11/L lk-&rvllium 1012
Doro, ea. Calcium 916
Tannin & Li11nin U"/L Co-Cobalt 1037
llexavalc:nt Chromium u<>/L Fe-hon 10.U
□
□
F.FFLUJ:NT
INFLUENT
G
Value Type. A, JI, L
m11:/L
mRIL
m11/L
mo/L
m11/L
mo,L
mo/L
u11/L
U<'/L
"''L
UR/L
U.R/L
U<'/L
UR/L
u2/L
u11/L
UR/L
m11/L
"°'L
UR/L
X
. X
Lab Number ' YW0586
Date Received: 2/4/2000
11me Received: 9:40AM
Received By : IIMW
Data Released : AR
DatcReponed: 2/24/2000
Comporile-T, S, B Sample Type
li·Llthium 1132 u11/L
MR· Ma1U1csium 927 m<'/L
Mn-Manganc:sc JOSS UR/L
Na-Sodium 929 m"/L
Arsc:nic:Total 1002 "°'L
Sc-Sc:lc:nium 1147 ,oJL
HR• Mcrcurv 71900 uo/L
Ba_Barium u11/L
Organochlorinc Pesticides
Orizanooho$ohorus Pesticides
Acid Hclbicides
Basc/Nc:ulral&Add Extractable or~anics
TPH Dic:scl Rani::e
Pur11eablc OrRania (VOA bottle rcn'd)
TPH Gasoline: Ran11c
TPII/BTEX Gasoline Range ~ Phvtoolanlcton
DIVISION
COUNTY
RIVER BASIN
OE ENVIRONMENTAL MANAGEMENT WATER QUALITY FlloLU·LAB FORM (OM!) For Lab Use ONLY ,..,
Lab Number:
REPORT TO: ARO FRO M
AT BM
Other
WSRO TS
Shipped by: Bus Qr, Staff, Other ________ _
couEcTORIS), C.o / bf
E,tlmated BOD Range: 0·5/5·25/25-65/40-130 or 100 plus
PRIORITY
OcoMPLJANcE
~ERGENCY
□QA
□ CHAIN
OF CUSTODY
STATION LOCATION:
SAMPLE TYPE
I ~EAM
□ LAKE
□ESTUARY
□ □
EFFLUENT
INFLUENT DAT A ENTRY BY:
DATE REPORTED:
Seed: Yu D No O Chlorlnated: Yes D No O ,R,cEe:M=Ae.R:,Kc:Scc'c_ __________________________________________________
_
(Station # GPL/ !Date Begin (yy/mm/dd) I Time Beg I~ I Date End I Time EndlDepth OM DB DBM !Value Type Composite ISam~e~ oo .oz._ ,o":> 13 Z.S-. , A H L T s 8 GNXX
1 BODS 310 mg/I C~lorlde 940 mg/I Nll3 u N 610 mg/I LI-Lithium 1132 ug/1
2 COD High 340 mg/I Chi 11: Tri 32217 ug/1 TKN as N 625 mg/I Mg-Magnesium 927 E.'. 3 COD Low 335 mg/I Chi a: Corr 32209 ug/1 NO2 plus NO3 na N 630 mg/J Mn-Manganese 1055 ug/1 4 Coliform: MF Fecal 31616 1100ml Pheophytln a 32213 ug/1 P: Total as P 665 mg/I Na-Sodium 929 mg/I
5 Colllorm: MF Total 31504 1100ml Color: True 80 Pt-Co PO4 as P 70507 mun Arsenlc:Total 1002 ug/1 6 Collform: Tube Fecal 31615 1100ml Color:(pH ) 83 ADMI P: Dissolved as P 666 mg/I Se-Selenlum 1147 ug/1 7 Coliform: Fecal Strep 31673 1100ml Color: pit 7 .6 82 ADMI Ilg-Mercury 71900 ug/1 8 Residue: Total 500 mg/I Cyanide 720 mg/I Cd<;admlum 1027 ug/1 Organochlortne Pesticides 9 Volallle 505 mg/I Fluoride 951 mg/I CrChromlum:Total 1034 ug/1 Organophosphorus Pesdck!es 10 Fixed 5IO mg/I Formaldehyde 71880 mg/I Cu-Copper 1042 ug/1
ti Residue: Suspended 530 mg/I Grease and Oils 556 mg/I NI-Nlckel 106 7 ug/1 Acid Herbicides
12 Volatlle 535 mg/I flardneu Total 900 mg/I Pb-Lead 1051 ugn
, 13 Fixed 540 mg/I Specific Cond. 95 uMhos/cm 2 Zn-Zinc 1092 ug/1 v Base/ Neutral Extractable Organics 14 pH 403 units MBAS 38260 mg/I v Acid Extractable Organics
15 Acidity to pH 4.5 436 mg/I Phenols 32730 ug/1 Ag-Sliver 1077 ug/1 --
16 Acidity to pH 8.3 435 mg/I Sulfate 945 mg/I Al-Aluminum 1105 Ug/1 v Purgeable Organics (VOA bottl~ 17 Alkallnlly to pl-I 8.3 415 mg/I Sulfide 745 mg/I Be-Berylllum 1012 ug/1
18 Alkalinity to pll 4.5 410 mg/I Ca-Calcium 916 mg/I
19 TOC 680 mg/I Co-Cobalt 1037 ug/1
20 Turbidity 76 NTU Fe-Iron 1045 ug/J Phytoplankton
Sampllng Point X Conductance at 25 C !Water Temperature tc; D.O. mg/1 pH Alkallnlty Acidity Air Temperature fC)
0~ G 1-400 ~ s pit 8.3 pH 4.5 pH 4.5 pH 8.3
2 94 I 10 ' c; ,. 'D (,
I• 82243 82242 20 300 82244 431 Sallnl1y X Preclpltlon (In/day) Cloud Cover X Wind Direction (Deg) Stream Flow Severity Turbidity Severity Wind Velocity M/H .,_.ean Stream Depth It . Stream Wklth fL 0, I D 6') 480 45 32 36 1351 1350 35 64 4
DMl/Revt~d 10/86
REPORTED BY
• CHECKED BY
REVIEVVED BY
SAMPLE TYPE:
75-35-4
75-09-2
156-60-5
75-34-3
590-20-7
156-59-4
67-66-3
74-97-5
71-55-6
563-5B-6
56-23-5
107-06-2
79-01-6
78-B7-5
75-27-4
74-95-3
10061-01-5
10061-02-6
79-00-5
127-18-4
1<12-2B-9
124-48-1
106-93-4
10B-90-7
630-20-6
75-25-2
79-34-5
TOL-
T-
E-
U-
N-
D-
M-
)MMENTS·
WATER
1.1-Dichloroethene 0.75
Methylene Chloride 10
lrans-1,2-Dichloroethene 0.75
1.1-Dichloroethane 0.25
2,2-Dich1orop10pane 0.25
cis-1,2-Dichloroethene I 0.25
Chloroform 0.25
Bromochloromethane 0.75
1, 1-Trichloroethane 0.25
1-Dichloropropene 0.25
Carbon Tetrachlorioe 0,75
1.2-Dichloroethane 0.25
Trichloroethene 0.25
1.2-Dichloropropane 0.25
Bromodich1oromethane 0.25
Dibromomelhane 1
cis-1,3-Dichloropropene 0.25
trans-1, 3-Dichloropropene 0.25
1, 1,2-Trich1oroethane 0.25
Tetrachloroethene 0.25
1.3-Dichloropropane 0.25
Dibromochloromethane 0.75
1,2-Dibromoethane
Chlorobenzene 0.25
1, 1, 1,2-Tetrachloroelhane 0.25
Bromororm 0.5
1.1.2.2-Telrachloroethane 0.75
Target Quantitation Limit-Subject to
change due lo instrument sensitivity
Tentatively Identified, not confirmed
Estimated Value
Samples analyzed for this compound but not detected
Sample not analyzed for this compound
Detected below quantilalion limit
GC/MS Analysis performed
ENRfDWQ LABORATORY
VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 96-18-4
u 108-86-1
u 95-49-8
u 106-43-4
u 541-73-1
u 106-46-7
u 95-50-1
u 96-12-8
u 120-82-1
u 87-68-3
u 87-61-6
u 1634-04-4
u 71-43-2
u 108-8B-3
u 100-41-4
u 108-38-3
u 95-47-6
u 100-42-5
u 98-82-8
u 103-65-1
u 108-67-8
u 98-06-6
u 95-63-6
u 135-98-8
u 99-87-6
u 104-51-8
u 91-20-3
1,2,3-Trichloropropane
Bromobenzene
2-Chlorotoluene
4-Chlorotoluene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
1,2-Dibromo-3-Chloropropane
1.2.4-Trichlorobenzene
Hexach!orobutadiene
1.2.3-Trichlorobenzene
Melhyl-lert-butyl ether
Benzene
Toluene
Ethyl benzene
m.p-Xylenes
o-Xylene
Styrene
tsopropylbenzene
n-Propylbenzene
1,3,5-Trimethytbenzene
tert-Butylbenzene
1,2,4-Trimethylbenzene
sec-Butylbenzene
p-isopropylloluene
n-Butylbenzene
Naphthalene
·••·.
GaS0iiiie R3rige Estimated Toial Petrore·~;,, H;~~rbori.
· .... . ..
Other purgeables detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
LAB NO. YW0586
SUPERVISOR re DATE ~
ENTERED BY l (
· DAT.E #, -,s-o {J
0.25 u
u
0.25 u
0.25 u
0.25 u
0.25 u
0.25 u • u
0.25 u
0.25 u
0.75 u
5 u
u
u
u
2 u
u
u
u
u
u
u
1. • u
u
u • u
u
mg/L mg/L
0.20 N
□elected
ug/L
·-
I I-'
REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE:
62-53·3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-l
106-44-5
621-64-7
67-72-1
99.95.3
78-59-1
00.15.5
105•67•9
65-85-0
111·91·1
120-83-2
120-82-1
91-20-3
106-47,8
87-68-3
59.50.7
91•57•6
77.47.4
88-06-2
95.95.4
91·58•7
aa.74.4
131-11·3
208·96·8
WATER
ANILINE
PHENOL
815(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-0ICHLOROBENZENE
1,4-otCHLOROBENZENE I BENZYL ALCOHOL
1,2-DICHLOROBENZENE
2-METHYL PHENOL
8I5(2-CHLOROISOPROPYL) ETHER
4-METHYL PHENOL
N•NlTROSO-Dl•N•PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2·NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOIC ACID
81S(2·CHLOROETHOXY) METHANE
2,4-0ICHLORO PHENOL
1 ,2,4• TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANIUNE
HEXACHLOROBUTAOIENE
4-CHLOR0·3·METHYL PHENOL
2·METHYL NAPHTHALENE
HEXACHLOROCYCLOPENTADIENE
2,4.6-TRICHLORO PHENOL
2,4,5-TRICHLORO PHENOL
2-CHLORO NAPHTHALENE
2•NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
IO
10
10
10
IO
10
20
10
10
10
IO
10
IO
IO
IO
IO
10
50
IO
IO
IO
IO
20
10
20
10
10
IO
10
10
50
10
IO
ENR/DWQ LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
u 606,20-2
u 99-09-2
u 83-32-9
u 51-28-5
u 100-02•7
u 132-64-9
u 121-14-2
u 84-66-2
u 7005-72-3
u 86-73-7
u 100-01-6
u 534-52·1
u 86·30-6
u 101.55.3
u 119.74.1
u 87-86-5
u 85·01·8
u 120·12•7
u 94.74.2
u 206-44•0
u 129-00·0
u 85-68•7
u 91-94•1
u 56·55,3
u 218·01·9
u 117-81•7
u 117.94.0
u 205,99·2
u 207•08-9
u 50·32·8
u 193.39.5
u 53.70.3
u 191·24·2
LAB NO. YW0586
SUPERVISO;ft DATE
ENTERED BY I I (}
DATE -,..{)
2,6-DINITROTOLUENE 10 u
3-NITROANILINE 50 u
ACENAPHTHENE IO u
2,4-DINITRO PHENOL 50 u
4-NITRO PHENOL 50 u
DIBENZOFURAN 10 u
2,4-0lNITROTOLUENE IO u • DIETHYL PHTHALATE IO u
4-CHLOROPHENYL PHENYL ETHER IO u
FLUORENE IO u
4-NITROANIUNE 50 u
4,6•0INITR0-2·METHYL PHENOL 50 u
N-NITROSODIPHENYLAMINE IO u
4•BROMOPHENYL PHENYL ETHER IO u
HEXACHLOROBENZENE IO u
PENTACHLORO PHENOL 50 u
PHENANTHRENE ID u
ANTHRACENE 10 u
Ol•N•BUTYL PHTHALATE IO u
FLUORANTHENE 10 u
PYRENE IO u
BUTYLBENZYL PHTHALATE IO u
3,3'•0ICHLOROBENZIOINE 20 u
BENZO(A)ANTHRACENE IO u
CHRYSENE IO u
815(2-ETHYlHEX.Yl) PHTHALATE IO u • OI-N-OCTYL PHTHALATE 10 u
BENZO(B)FLUORANTHENE IO u
BENZO(K)FLUORANTHENE 10 u
BENZO(A)PYRENE 10 u
INOENO(I ,2,3·CD)PYRENE IO u
DIBENZO(A,H)ANTHRACENE IO u
BENZO(G,H,l)PERYLENE IO u
! :1
:!
I
' .l
'
:,
l --
SEMIVOLATILE ORGANICS REPORT· DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
I
LAB NO. YW0586 ------
TQL-Target Quantitation limit-Subject to
change due to Instrument sl!nsitivtly
T-Tentatlvely Identified, estimated concentration
E-Eslimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time el(Ceeded
COMMENTS: __________________________________________________ _
I -.J
•
•
COUNTI'
Rl\'ER BASIN:
R[PORTTO
Olhtr :
COLLECTOR(S)
~NOYER
RECEIVED
MAR O 8 2000
BY:
□
WIRO Regional Office □
ID COLBY
DIVISION OF WATER QUALITY
Chemhlry L.abonlory Report I \Valer Quality
= AMBIENT □QA
COMPLIANCE D CHAIN OF CUSTODY
EMERGENCY
~ =
ID STREAM
□ LAKE
□ ESTUARY
[1tlmalrd BOO Ran,:r: S11tion Lonlion: OFF HALL ROAD
Sttd:
BPS
BOD 310
COD Hi11h 340
COD Low JJS
Coliform: MF Feat )1616
Coliform: MF Total 31S04
Coliform: tube Fecal 31615
Coliform: Feal StrC1l 31673
Residue: Tot.al 500
Vola1ile SOS
Fixed 510
Residue: Susnrnded 530
Vol.atile 53S
Fixed S40
I DH40l
Acidirv to oll 4.S 436
Acidity 10 t II 8.3 435
Alk.alinirv to nll 8.3 415
Alk.alinitv 10 nll 4.5 410
TOC680
Turoiditv 76
Coliform Tot.al Tube
CO/IIMENTS:
Ch1Drln1trd:
Dair lk,:ln (yy/mm/dd)
20(X)(}203
mRIL
mg/L
m11/L
1100ml
1100ml
1100ml
1100ml
m"L
mRIL
m"L
mg/L
m11/L
m1VL
units
mi:IL
m11/L
mg/L
mg/L
m11/L
NTU
•1100 mis
Dalt End (yy/mmldd)
Chloride 940
Chla:Tri32217
Chi a: Corr 32209
Pheoohviin a 3221 J
Color: True 80
Color. (pH ) 83 pH::
Color. oH 7.6 82
Cvanide 720
Fluoride 951
Formaldehyde 71880
Grc:a~ and Oils 556
llardni:ss Total 900
s....,.;nc Cond. 95
MBAS 38260
Phenols 32 730
Sulfate 945
Sulfate 74S
Boron
Tannin & Li11.nin
Heuvalent Chromium
Rrm■rlu:
Timr 8q:l11
1410
Tlmt End Dtplh. DM, DD, DOM
m11/L NHJ as N 610
URIL TKN an N 62S
uo/L NO2 nlus NO) as N 630
u11./L P: Total as P 665
c.u. P04 as P 70507
c.u. P: Dissolved as P 666
c.u. K-Pot.assium
m11./L Cd-Cadmium 1027
m11:/L Cr.Chromium:Total 1034
mo/L Cu-Connrr 1042
mi:r/L Ni-Nield 1067
m11./L Pb-Lead !OS I
umhos/cm2 Zn-Zinc 1092
mo/L V-Vanadium
u11./L Ao.-Sil\'er 1077
m<>/L Al• Aluminum 1105
mir/L Be-Bervllium 1012
Ca-Calcium 916
u11./L Co-Cobalt 1037
uo-/L Fe-Iron 1045
Lab Number ' YW0587
Date Received: 2/4/2000
Timc Reccived : 9:40AM □ EFFLUENT Rcttivcd By ' HMW
□ INFLUENT
Data Rekaud : AR
Dale Reported: 2/24/2000 G
Vah1e Type• A, II, L Compo1i1e-T, S, B Sample Ty~
m11./L Li-Lithium 1132 u.11./L
m2/L MR-MaR11i:sium 927 mo/L
mg/L Mn-Manganese IOSS "''L mg/L Na-Sodium 929 m11./L
m,:/L Arscnic:Total 1002 ,oil
mg/L Se-Selenium 1147 ""L mg/L Ilg-Mercury 71900 usz/L
URIL Ba_Barium ur/L
u2/L Organochlorine Pesticides
u2/L Organophosphorus Pesticides
UR/L
""L Add Herbicides
URIL
ug/L X Base/Ncutral&Acid Extracuble Oriranics
u.11./L Tl'H Diesel Ram!e
ug/L
ug/L -X Purgeable Organics (VOA bottle rea'd)
m11./L
""L
ug/L
TPH Gasoline Range ~ TPH/BTEX Gasoline RanRC
Phytoplankton
DIVISION OF ENvll!ONMENTAL MANAGEMENT WATEII QUALITY FIELU·LAU FORM (DMI)
COUNTY N r2t.,.., )-\ c. 1-1 o ve,
RIVER BASIN
REPORT TO: ARO FRO
AT BM
Other
WSRO TS
Shipped by: Bus (;;;:?r, Slaff, Other ________ _
cou,crn•1s>, Co I l:,f
Estimated BOD Range: 0-5/5-25/25-65/40--130 or 100 plus
Sud: Yu O No D Chlorinated: Yu D No D
PRIORITY
□AMBIENT
OcoMPUANCE
~ERGENCY
□QA
□ CHAIN
OF CUSTODY
STATION LOCATION:
REMARKS: I St•tlon # t>Y s-,Doeoe:IOylm.m~d3 I ~4mi agln I Date' End
1 BODS 310 mg/I Chloride 940 .
2 COD High 340 mg/I Chi a: Tri 32217
3 COD Low 335 mg/I Chi a: Corr 32209
4 Coliform: MF Fecal 31616 1100ml Pheophytln a 32213
5 ColHorm: MF Total 31504 /lOOml Color: True 80
6 Coliform: Tube Fecal 31615 /IOOml Color:(pH ) 83
7 Colllorm: Fecal Strep 31673 1100ml Color: pll 7.6 82
8 Residue: Total 500 mg/I Cyanide 720
9 Volatile 505 mg/I Fluoride 951
10 Fixed 510 mg/I Formaldehyde 71880
11 Residue: Suspended 530 mg/I Grease and Olis 556
12 Volatile 535 mg/I llardness Total 900
Fixed 540
. SAMPLE TYPE
I ~REAM
□ LAKE
□ESTUARY
□ □
EFFLUENT.
INFLUENT
I Time EndlDeplh DM DB DBM 'Value Type
A H
mg/I NH3 ae N 610
ug/1 TKN III N 625
ug/1 N02 plus N03 as N 630
ug/1 P: Total as P 665
Pt-Co P04 as P 70507
ADMI P: 0lssolved III P 666
ADMI
mg/I Cd<&dmlum 1027
mg/I Cr-Chromlum:Total 1034
mg/I Cu-COpper 1042
mg/I NI-Nlckel 1067
mg/I Pb-Lead 1051
13 mg/I Specific Cond. 95 uMhos/cm 2 Zn-Zinc 1092
14 pft 403 units MBAS 38260 mg/I
' 15 Acidity to pl-I 4.5 436 mg/I Phenols 32730 ug/1 Ag-Sliver 1077
16 Acidity lo pH 8.3 435 mg/I Sulfate 945 mg/I Al-Aluminum 1105
17 Alkallnlty to pH 8.3 415 mg/I SuHlde 745 mg/I Be-Beryllium 1012
18 Alkallnlty to pH 4.5 410 mg/I Ca-Calcium 916
19 TOC 680 mg/I Co-Cobalt 1037
20 Turbidity 76 NTU Fe-Iron 1045
Sampling Point lt Conduclance at 25 C lwater Temperature,::::: D.O. mg/1 pH Alkalinity
6 -+ <t. 0 400 ~ I•+ pl! 8.3 pH 4.5 pH 4.5
2 94 10 300 ~ l•l.( 82244 431 82243
Rec'd b :
DATA ENTRY BY: CK:
DATE REPORTED:
Composite I Sample Type
L T s B c@ GNXX
mg/I LI-Lithium 1132 ug/1
mg/I Mg-Magnesium 927 ~ mg/I Mn-Manganese 1055 I
mg/I Na-Sodium 929 mg/I
mg/I Anenlc:Total 1002 ug/1
mg/I Se·Selenlum I 147 ug/1
Ilg-Mercury 71900 ug/1
ug/1 Organochlorlne Pestlcldee
ug/1 0rganophosrixnus Pestk:ldes
ug/1
ug/1 Acid Herbicides
ug/1
ug/1 v Base/ Neutral Extractable Organic•
V ncld Extractable Organics
ug/1 / -ug/1 v rurgeable Organics (VOA bottle reg'd)
ug/1 1t= mg/I
ug/1
ug/1 Phytoplankton
Acidity Air Temperature fC)
pft 8.3
182242 20
Salinity )l Preclpltlon On/day) Cloud Cover )l Wind Direction (Deg) Stream Flow Severity Turbidity Sevedty Wind Velocity M/H Mean Stream Depth rt. Strum Width IL
0 . I 0 6) 480 45 32 36 1351 1350 35 64 4
DM1'11ev1Hd 10/86'"···~--------------------------------=------------------------~--------------
ENRIDWQ LABORATORY LAB NO. YWOS87
~ VOLATILE ANALYTICAL REPORT
REPORTED BY SUPERVISOR
CHECKED BY DATE
REVIEWED BY ~
ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
75-35-4 1, 1-Dichloroethene 0.75 u 96-18-4 1.2.3-Trichloropropane 0.25 u
75-09-2 Melhylene Chloride 10 u 108-86-1 Bromobenzene u
156-60-5 trans-1.2-Dichloroethene 0.75 u 95-49-8 2-Chlorololuene 0.25 u
75-34-3 1.1-0ichloroethane 0.25 u 106-43-4 4-Chlorotoluene 0.25 u
590-20-7 2.2-0ich1oropropane 0.25 u 541-73-1 1,3-Dichtorobenzene 0.25 u
156-59-4 cis-1,2-Dichloroethene I 0.25 u 106-46-7 1,4-Dichlorobenzene 0.25 u
67-66-3 Chloroform 0.25 u 95-50-1 1.2-Dichlorobenzene 0.25 u • 74-97-5 Bromochloromelhane 0.75 u 96-12-8 1, 2-Dibromo-3-Chloropropane u
71-55-6 1.1-Trichloroethane 0.25 u 120-82-1 1.2.4-Trichlorobenzene 0.25 u
563-58-6 1-Dichloropropene 0.25 u 87-68-3 Hexachlorobuladiene 0.25 u
56-23-5 Carbon Tetrachloride 0.75 u 87-61-6 1,2,3-Trichlorobenzene 0.75 u
107-06-2 1.2-Dichloroelhane 0.25 u 1634-04-4 Methyl-tert-bulyt ether 5 U.
79-01-6 Trichloroethene 0.25 u 71-43-2 Benzene u
78-87-5 1.2-Dichloropropane 0.25 u 108-88-3 Toluene u
75-27-4 Bromodichloromethane 0.25 u 100-41-4 Ethyl benzene u
74-95-3 Oibromomethane u 108-38-3 m,p-Xylenes , u
10061-01-5 cis-1.3-0ichtoropropene 0.25 u 95-47-6 a-Xylene u
10061-02-6 trans-1.3-0ichtoropropene 0.25 u 100-42-5 Styrene u
79-00-5 1, 1.2-Trichloroethane 0.25 u 98-82-8 lsopropylbenzene u
127-18-4 Tetrachtoroethene 0.25 u 103-65-1 n-Propylbenzene u
142-28-9 1,3-0ichloropropane 0.25 u 10B-67-B 1,3,5-Trimethylbenzene u
124-4B-1 Oibromochloromelhane 0.75 u 98-06-6 lert-Bulylbenzene u
95-63-6 1,2,4-Trlmethylbenzene 1 -u 106-93-4 1.2-0ibromoethane u
108-90-7 Chlorobenzene 0.25 u 135-98-8 sec-Butylbenzene u • 630-20-6 1, 1.1.2-Tetrachloroethane 0.25 u 99-87-6 p-isopropyltoluene u
75-25-2 Bromoform 0.5 u 104-51-8 n-Bulylbenzene u
79-34-5 1.1.2.2-T etrach1oroethane 0.75 u 91-20-3 Naphthalene u
mgll mgll
TOL-Targel Ouanti1ation Limit-Subject to Gasoline Range Estimated Tolal Pelroleuni Hydr~rbon . 0.20 N
change due to instrumenl sensitivity . . > .,:•::::<,'
T-Tenlalively Identified, not confirmed Other purgeables detected Detected
E-Estimated Value (up to 10 highest peaks) ug/l
U-Samples analyzed for this compound bu! not detected
"· Sample not analyzed lor lhis compound NO VOLATILE ORGANIC COMPOUNDS
D-Delecled below quan1ilation limit DETECTED BY GC/ELCOIPID.
M-GCIMS Analysis performed
'MMENTS·
ENR/DWQ LABORATORY LAB NO. vwosa1 pc., . SEMI-VOLATILE ANALYTICAL REPORT
REPORTED BY
CHECKED BY Aw= REVIEWED BY /(ff-ENTERED BY
SAMPLE TYPE: WATER ANALYSIS RESULTS
62·53-3 ANILINE IO u 606-20-2 2,6-DINITROTOLUENE IO u
108-95-2 PHENOL 10 u 99-09-2 3-NITROANILINE 50 u
111-44-4 8IS(2-CHLOROETHYL) ETHER 10 u 83-32-9 ACENAPHTHENE IO u
95-57-8 2-CHLOROPHENOL 10 u 51-28-5 2,4-0INITRO PHENOL 50 u
541-73-1 1,3-0ICHLOROBENZENE IO u 100-02-7 4-NITRO PHENOL 50 u
106-46-7 1,4-0ICHLOROBENZENE 10 u 132-64-9 OIBENZOFURAN IO u
100-51-6 BENZYL ALCOHOL 20 u 121-14-2 2,4-DINITROTOLUENE IO u • 95-50,1 1,2-0ICHLOROBENZENE IO u 84-66-2 DIETHYL PHTHALATE 10 u
95-48-7 2-METHYL PHENOL 10 u 7005-72-3 4-CHLOROPHENYL PHENYL ETHER 10 u
IOB-60-1 8IS(2-CHLOROISOPROPYL) ETHER IO u 86-73-7 FLUOAENE 10 u
106-44-5 4-METHYL PHENOL 10 u 100-01-6 4-N1TROAN1LINE 50 u
621-64-7 N-NITROS0-0I-N-PROPYLAMINE 10 u 534.52.1 4,6·DINITR0-2-METHYL PHENOL 50 u
67•72•1 HEXACHLOROETHANE 10 u 86-30-6 N-NITROSODIPHENYLAMINE 10 u
98-95-3 NITROBENZENE 10 u 101.55.3 4-BROMOPHENYL PHENYL ETHER 10 u
78·59·1 ISOPHORONE 10 u 118-74-1 HEXACHLOROBENZENE 10 u
88-75-5 2-NITRO PHENOL 10 u 87-86-5 PENTACHLORO PHENOL 50 u
105-67·9 2,4-DIMETHYL PHENOL 10 u 85-01·8 PHENANTHRENE 10 u
65-85-0 BENZOIC ACID 50 u 120·12•7 ANTHRACENE 10 u
111·91·1 BIS(2·CHLOROETHOXY) METHANE 10 u 94.74.2 Dt•N•BUTYL PHTHALATE 10 u
120-83-2 2.4·DICHLORO PHENOL 10 u 206•44•0 FLUORANTHENE 10 u
120-82·1 1,2,4• TRICHLOROBENZENE 10 u 129-00-0 PYRENE 10 u
91·20-3 NAPHTHALENE 10 u 85-68•7 BUTYLBENZYL PHTHALATE 10 u
106-47•8 4-CHLOROANIUNE 20 u 91•94-1 3,3'-DICHLOROBENZIDINE 20 u
87-68-3 HEXACHLOROBUT ADIENE 10 u 56-55·3 BENZO(A)ANTHRACENE 10 u
59-50-7 4•CHLOR0·3·METHYL PHENOL 20 u 218·0l-9 CHRYSENE 10 u
91·57·6 2-METHYL NAPHTHALENE 10 u 117-81•7 BIS(2-ETHYLHEXYL) PHTHALATE 10 u • 77.47.4 HEXACHLOROCYCLOPENTAOIENE 10 u 117-84-0 Dl•N-OCTYL PHTHALATE 10 u
88-06-2 2,4,6•TRICHLORO PHENOL 10 u 205·99-2 BENZO(B)FLUORANTHENE 10 u
95.95.4 2,4,5•TRICHLORO PHENOL 10 u 207-08-9 BE NZO(K)FL UORANTH ENE 10 u
91-58-7 2-CHLORO NAPHTHALENE 10 u 50-32-8 BENZO(A)PYRENE 10 u
sa.74.4 2-NITROANIUNE 50 u 193.39.5 INDENO{l,2,3·CD)PYRENE 10 u
131•11·3 DIMETHYL PHTHALATE 10 u 53-70-3 DI BENZO(A,H)ANTHRACENE 10 u
208-96-8 ACENAPHTHYLENE 10 u 191·24·2 BENZO(G, H,l)PERYLENE 10 u
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
LAB NO. -~YW~0~5_8~7
TQL-Target Quantilation limit-Subject to
change due to Instrument sensitivity
T-Tentatively Identified, estimated concentration
E-Estimated Value
U-Samples analyzed for this compound but not detected
N-Sample not analyzed for this compound
D-Detected below quantitation limit
H-Holding time exceeded
COMMENTS: __________________________________________________
_
•
•
•
NOV_.15.1999 NCDENR WIRO • • St.ate of North Carolina
Depurtment of Environment and Natural Resources Wilmington Regional Office
N {:,t.U li\-cwt, (~--u-or CQ, . 6\-t ~ iB-<J..-rA f'rt. James B. HW1t, Govemor
T-· · Bill Holman, Secrntary
FAX COVER SHEET
No. Of r:i)s: --"-· ...,.J------From: lG<.l'-L fus; co: vw d ~ &ws
FAX#: [phone]
REMARKS: ~-3:-"-'F~-"----"7~r-=-t---:'---':~-.,.--J-'"-'-'-=----
'
-
½
~
=
-
-
=
-
,
,
,
-
-
--ro/
r--'0 t' /,i, IA)L_..---~ 127 Cnrdin11! Drive E.\:tcn,~iou\ Wilmington, N,C, !8405-J84S TL'li;•nhonc (910) J!>S-J!J00 li'i1:i.: (910) JS0~2U04 1\n Ecprnl Or,narn1riity Affirmnti\/C A(:t[on 1:;mplo,r"r
I
f'-' (\J
[L
f'-U~ '\JNTY :
r---:rAO NC>;
0 z RlTt)Ri "TD
OJLJ_[CTDR{S)
DATE-
H}\E:.
PlfRf'C6C •
Nf.W llAt'o'On-:R
LABORATORY ANALYSIS
OCIDJID
COD ili.-t.3-40
CODl...aw"'DS
CoWumr t.rFfn:-;,,l]l6H,
CoMunn.: MFTut.J 31.SOf
'rc,C
Twb"L1i1.1·
~\H!., ~--.ltd 530
Tat.,,15"!5.-.-.df'rl....,lids
0
Ck' ,H
H
3 Alkalini~v lo vH 4-S
Ck' i\..1Wini1,-to11H l'-3
z: ~·· l~-'" YO, o,_J-C.,d-, dLO,.ide_
I Chkn..k
C.1rromw..m.: Hz-;,i 1.IDJ. ,_ Culoo-,1m.e.eo [l_ N IS) C\·,.n.OlkTID
m,/L
•n"/l
=IL
/lOOml
/100ml-
~,n
Nlll
-'L . m"/L
--:.;":.,.""'-,-..:..~
111\lf§
mR/L
-'L
1uR/L
rnr,/L
m,;/L
m,/ L
u,/L
•"..ll.
ms(L
Ownrr.
l.o<ca100Put5ill'-:
VIVJSIUN OFWAI EH {J_Ui\Lff\'
SAMPLE C'RlO~frY
□ROUTINE
5:1 Cl-L'\JN CJE ClliTIJOY
~ 5,MWLE.TYl'E
BAllllt'\RA ENGL'r:5l I
o~'51l:rip!Wn .,f ',,.1Jf1plin~ [VU,t ___________________________ _
S..mp!mg-.&.l~hod:
Rv:a:.uJ..-,:
rN& So~70JOO p-lL A11:~<;i.tV"Er%.S66
Fluoritk-'151 m,/l Al-Al.i.uniuum. 4(i'n7
rfu.dr=l.ol..1900 m•/L As--~46.",:il
lfu~(nr;rn<..ub)902 m,/L B,i-5a.ti,.im_4i,.55a
Ph..-nob JT7.30 u,/L C&--Gilru.,.m 4.fRrl
<:.., Lrific. Cnod. "5 LJ~/o:n2 Gt.-G.diwn .fb559
SuU.,t,,, m,IL C..---0:lroTJU.Um 46560
S"cl.(~745 mr-/1 Cu--G>~-lOU.
MBAS m,IL Fe--lrun-1.MS
-;-;;:,; Oil u.d"Gcuu:;; ---------mr/L----1:1-l\.fnnu,,· 719(){]
5ilh . . . •··~· -;;~ ... il~Jl~J .... ~4 -. -
llonin ~1~.:11,1~..,-iutn 917
fo""""l,Jch,·d.e. mp;/L ~!n--M.n1r.im=cc lt.1&5
NUJ.o..,N !>l.lJ ~•IL N•-Sodlum '1B
rKN"• N !u5 -IL Ni-NirJ::e.l:
N02 • N03 a~n l',JO n1d"L X. Fl>-l£;ul46564.
r':Tobl ,u r@ 111r./L c~o;..,1,.r,iuDl.
POI mdl LJt Zi.w::::46.5'67
L..,t, N.,n,L...r ')(; I IJ9
o.,!~ R<'«';,•crl : 6JTJJ~'JI
li1ru-.Rnei,ro,,.I 9;]0
[k,,ci>cJ llr 115
fu.Se.,,;rJ By [,S
U..tt,crm1~..c1: ar.i.,wJ
•,Le_ a "'·"•lllod-00.-W I\.~ ici&s
u</L Ch.~nlcr,,ihorus ~•m~~-
..,/L Niil__..,.n~l.iddo
""'L
-------
-•'L Acid.Utt~
••/L
u 0 IL X xou,·o.4~
"PJL f'f'l {-0~1 Ra-e
u,:/L
u.</L X ~~·~:~.~-t~~) --~-1:11
--' ---m11:I~---TI'l u:; .. ~1111.., Rir, ~ --
u-fL frll-ll'CE< Go..uluw::: tl~•u
a.,.JL
rJr./L
<JO u,JL
ug.l!:__
ngll.
rn-----------------------------------------------------------------------
~-------------------------------------------------------------------------------
-
-
-
-
··-----------------------------------------------------------------------
-
-
'o'"'.",ll n JU/0
,..;_--,.,
•-· "1'.-' ~:•¥ -----

-
~ ' ,~
n.
~ 0)
~
0 z:
--------
REPORlED BY
CHEC1<ED BY
R(Vl[WEO BY
SAMPLE TIP[:
6253-3
•::
95"57-8
541-73-l
106-46-7
L0051 Ii
106445
62.1-64-7
~ -J?,,$-
~-
WA.lER
ANILINE
PHENOl
BIS(?cCHLOHOETHYI.) ETHER
2.CHLOROPH[N()L
1...3-0ICH\.OROBENZENE
L4-DICf1LOR08ENZENE
UENZ.YLALCOHOL
4-MEJH'tLPHENOL
N-NITROS0-01-N-PROPYLAMlNE
67-72-1 HEXAC~lLOROETHANE
ENR/DWQ LABORATORY
SEMI-VOLATILE ANALYTICAL REPORT
LAB NO. 9Glll9
ANALY 51 S. RESULTS
SUPERVIS
DA
~!-i!l~~~\~J~\11~lt:5~;jlf&~!fr•~-~-111f!lll
lO U 606-20-2 2,GDlNITROlULUENE l.O . U
10 U 99 09 2 3-NITROANILINE 50 U
10 U !i3-3?a9 ACENAPIHHENE LO U
lO
JO
LO
20
to
lQ
lO
u
u
51.•28-5
L00·02-7
U ¥32,64--9
U 12L-l4-2
2.4DINITRO PHENOL
4-NITRO PHENOL
OIB'ENZOFURAN
2,4D!NITROTOLU[NE
50
50
LO
LO
u
u
u
u
Li 84-66-2 DIElH'tl P~tTt-iALATE 10 u
_
0
_ UU·_ .. -~.Jl_,.,._Q._3 ____ t [ 4-CHLOROP.rENYLPHEJ.:IYLE.!HER _ _ _ _ 10 _ _ __ ____::E,_ -=,,J.,_. _. _ it~c1,L-::-#=;;;; __ ~· =c3..: ___ L]i_.__'.J, _!38=ltill.?m!.IL1f;;
4-NITROAtULINE _50 ___ -----··u~-~ ·· u
u
u
u
IOO-Ol-6
534-52.-l
Bo-30-6
4,6'0,NITR0-2.-MITHYL PHENOL 50 U
IO u
u
· 91!-95-3_ _ NlffiOBENl.ENE - _ . . . __
N -NI IROS.ODI PHENYL.AM I NE
4BROMOPHENYL PflENYL ETHER
H ~1,~r~~~~~~~~1r~'.~ ··::=="""=
:{ 105-67-9 -2.-4-DIMETHYLPHENOL [l'. 65-85 O 8£NZOIC ACID SO U ! Z0-12----•-1./i' • ... ~--
~: ~~~-~~"c-~-'::2=1'"'_•~,,,-~_-~~------~::;'-e:~~~::::~~;:N~; .-~tf<"c-~~:;~~~~~"~:,:*:~r ii%~™~~~~:{~;~i:;;t,!iif?~~Ji:5w;#@_Rj~ef-Ltg1~
9120-3 NAPHTHAUNE 10 U 8568-7 BUTILBENZYLPHTHAIJ\TE 10 -. U _____ ,.., .
,:: 106-47-8
Q. N 87-6B-3
(SJ 59-50-7
" 91-57-6
I 77-4/-4
en 88-06-2 0) 95-95-4 en _, 91 58-7
ul 88-74-4 _,
131-11-3 >· 208-96B 0
4-CHLOOOANILINE 20 u 91-94--1 J.3'-0ICHLOROBENZIDINE 20 u
HEXACll LOROBUTADIEN E' 10 u 56-55-3 BENZO(_A)AN THAACENE 10 u
4-CHLORO 3-MEHlYL PHENOL 20 u 218-01-9 CHRYSENE 10 u
Z•ME.H-i'tLNAPHTHALENE" 10 u U7-8L-7 91S(2ETHYLHEXYL) PHIBALATE lO u
t1EXACt-iLOROCYCLDPENTA01ENE IO u U7-840 D1-N-OCT'IL P HnlALA TE JO V
2.4.6-TRICHLORO PHENOL 10 u 205-99-2 BENZO(B)FLUORJ\NTHENE lO u
2_4,5-TRICHLORO PHENOL 10 u 207-03-9 BENZO(_K)FLUORANTHf.NE 10 u
2 CHLORO NAPHTHALENE. IO u 50-32-8 B[NZ!}(A)PYRENE rn u
:?_-N ITROAN1UNE 50 u 193-39-5 IN DENO( 1,2.3 CO)PYRENE 10 u
DIMElH'tl PHTHALATE lO u 53-70-3 D18ENZO(A.H)ANTHRACf.NE IO u
AU.NAPHU .. Yl.£NE 10 u 19L-24-2 BENZ.O(GJI.IJPERYLENE 10 u
r
:E ll. (\J
IS)
'1
['-
U\
['-
0 z:
•
SEMIVOLATILE ORGANICS REPORT -DWQ LAB PAGE 2
NO BI\SEiNEUTRALOR ACID EXTRACTABLE.ORGANICS
DEfECTEO BY GC/MS .
LAB NO. 9Gl139 ------
·rQL· r.a,get Quantitation Untit--Subfed to
cha.I1ge due lo inslrumenl sen~it.Ni-ty
T -·rentativefy Wenltfied, e:':.1imat-ed com:.cntration
E l:stimaled Valu~
U-Sarnp!es analyl.M for tn·,.._ compou:nd but nol delccled
N -Sample not .analyi.ed !or u1•s compo1.Jnd
__ _ _ 0-Detecled below quantitalica hmit-----
: -~i,;,L~~: .. , .. M::: .--:;m ii~~;~~]::,_~7;~~=..![_~!1¢=:~.--!.]l~~
--------------------------
COMMENTS: _________________________________________________
~=~~
1-_··
I'-"' l'-
0 z:
REPOR fEO B<
CHECKED BY
REVIEWl:::O BV
SA~,Pl.£ TYPE.:
75-3'>4
75-09·2
J 56-()()-5"
75-34--3
590-20-7
156-59-4
67-66-3
74-97-5
7)-55-6
1.I-Dicftloroel~ne
Methyla1e CNoride
hans--J .2-Di chlo1oethene-
l. I -O ic.hlaroel hane
z.2.0ichloropropa.ne
c·1'S'-l .2Dichlornethe11e
Chlo1o[orm
Bmmochl ofomellldne
I. l. l-Trich,orotlhaoe
ENR/OWQ LAsonill.TORY
VOLA T llE ANAL YT IC.Al R f:PORl.
0.75
10
ANALYSIS nESUL1S
u
u
OJ5 U
0.25 U
0.25 U
0.2S U
96-18-4
)0886-1.
95-•9 8
!06-43-4
54-1-73-l
106-46-7
95-50-1
l..2.3--Tdchloropropane
Brnrnobenlefle
2-Chlorololuene
4-Chlomlotuene
I .3-Dich1orobenrene
J .4-0ichlomberu.ene
L2.-DLchlorobenze11e
0.25 U
0. 75 LI 96-L2-8 1."2:Dibrorno-3-Chlompropane
0_25 U 120-82·1 l.2.4-nichloroben.une-
0.25 U 87-68-3 Hexachlombuladiene
0. 75 U 87-6\.-6 l .2.3-rrichlorobeJ1zene
----l07-06•2 ___ l.2-0ici1loroeU1.al"lec 0.25 U 1.634-04-4 Me:lhyl-lerl-butyl eU1er
~-:'~ ·--7!Ml~.~TjjdilomeUa;ne .. ---~-:~:-. ,~;"'-__ JJ.;?5;_~ =---=-'---'-.-0 -_-_,;,g~--~-~·· · ·
0
-••
563 58-6
'>6-23 5
l l .Oid1,aroprope11e
C.!rboo TelractiloriO'e
DX?. MkJJ.;U#@WJ-:1rna11~~P'OP·a'~~---~-~~---~-~:---: .
7 5-27-4 Bromodicf-llorome\ha.ne-
74-95· 3 Dibrnmorn~Utan.e
1006l-01-5 cis-LJ Olchrorop ropene
10061-02=6 t.ran.s.-L.3-Didlloropropen.e
9-rn?-5 ~ .. LL,2-lric:f:l~roetllane
,:. . • ---~~~'..c,h,.I>< ... ,, • .';.;,..
3: ·• :90!7,.lr~:ct,fol'"Ooenz.eni ;.j_£4,"f~,>c--:-
• -

•

--·.-s ·•·/:-~--·. -~ ....... -· -.:-.,..., __ "
O:'. 3O:20:0--::__~t,.:1_-:l .E2-.Telr.id11oroettia _:_
-e,~~~~r.n,,•~-;; ;-· ·, .':'
' J}fZ2:fetraCt,foftiettia ·, ,,:.. :->F:r~-. -:_: .. _ ':
,:
(L
I\J
[SJ
TQL ·Target Qua/\!ilaHan Umil-Sub}ect to ~he-_
challgedue lo ·m.strument sens.it.i•iily ·.,;,':
l
"
Tentau ... e,y ldefltitied. ootoonlirmed
E\iotimated V~tJe
Samples. anal_y2e-d ror lhis compoa11d buf nol detectf'd
Sample nol a.talyzed !or this compou~;
u
u
u
u
95-47-6
100-42-5
98-82-B
o-X.ylene
Sly,ene-
\sopropylbenzene.
Gast)line Rang_e Es.limaled o a . . -£.~----::~~:~~--: ---
Otherpurgeable-s delecled·",;l~--~--··· -,....:C_·.
(up lo 10 highest peaks) · ~[~-~ · ':
No VOLATILE ORGANIC coMPaoUNOS
LA'B NO. !JG1U'3
SUPEP.VISQPW1=
UATE .., --
ErJTl:RED Brns_~-.A---
0~ TE :ta~µ_9=
0.25 u
I u
0.25 u
0.25-u
0.25" u
0.25 • 0.25
0.25 u
tJ
u
u
. u
u
L. u
7."'!'0elicled ..c-
__ __:_· :..c_· -. Ug/L ,
~ ~-,:
I ~ "' rl
UJ rl
T-
E·
U-
N·
D·
"4-
Detected below quanti\aiiot1 limit
GC/MS Analysis per1om1ed
D8ECTED BY GC/ELCO/P,ID.7. . ',• , v·
·,::~~,;;~ ·'.:~' --~:~~ _F:$;~~~~-~--~~-=~~E~~r~~,
COMMENTS: --------------------------------------------,'-'~=c:-~~~,_-· ___ _;.,.. ______ "~•--.-_·_~-~--••c..c___;--;'.-_··_,~ __ .-·_-,~'!~_.
>
f
,i. ~ Map P mn Cham .in rat o Corpo .IJITLN.C-:i::im"i -~ ,il_
·-.--NOV, 15.
. ' .
N0.757 •. .. ' • " I • , ..
C.,1r
I .
. I
I, I ii •.
. I;-
1I . i ! I , ..
--~~
FROM ; Ge□Chem, Incarparate:ct • •
Client Projecl Manager
Gary McSmith
Site Name:
Burn Pit
94040
GeoChem, Incorporated
Environmental Laboratories
N~ \4;:wtc,.vW-C..(!;).uvvt:1 P--~Y~ \suyn Pit
fCtrtifitb ilnulptirnl Jl.ntu,rutorp
NC# 377-15 ,NC fl JJ6, NC# 461, EPA ID II 155
R. Catlin & Assoc.
P.O. Box 102i9
Wilmington NC
28404-0279
GCI Project#: 9812•061
i!'_111111nurp of requtdttb mulptillll loorlt
Report Date
Tuesday, January 05. 1999
PO II 981223-4
Date Received in /ah:
Wednesdt,y, December 23, 1998
SaMpi• type coU #r ~
Field .V14mber: T-lj
I =. ,c,6'! •amp/a,• 2 = liquul 1ampla: J ~ Air •ampl~•; 4 -r/.utgu.lunknO'l,WU 1.AbID Sj92 Sample T;,'J'c: 2 D'1rfl.Analyzsd: l/4/98 fOr 601 602 DtllC Samplsd 121.23/98
FiiJJd Numbflr: T-14
Datc&miplo::d 12/23.'98
Field ,'Vumbt!r: T-13
DateSampled l2,'2Jrn
1/ ,,.--..,__
l,,b ID 8593
Lab/I) 8594
Sampfo Type: 2
Sample Type: 2
ProJ>fff Pn:ervauon y.,.
Dat.Ana/yt:.ed: 12~0/?8 /Or 601 602
Proper J'reJervanon ·
Dat~.Analyz": 12-'30198 for 61./1 602
PMpr.r Preservation
;/Qrrr hp rrrti(p t!Jnt 31 ~abr i,rbirtnrb anb approbc tfJIS barn !i'rt
2500 Gale Way Centre 81vd., Suite 300 • Morrisville, NC 27560 Telephone: [phone] • FAX: [phone]
flepo~~~}\ ,-: 'y ,·lJ i., 5,,~J IT
c· .r) -r~ .. ..,-,,.,,J
GeoChem, lncorporclted Bill To: , .. , . I •. ,,~-•t ·
PROJECT SITE NUMBER
, ' . / •·:/'
.-, • _; ;r• ,. -_f ; p
SITE NAME -

·

" ..., • • l ~
, .. .· ....... ,
COLLECTED BV 1s;gnalure)
f:~ .... · v;. .•
FIELD TURNAROUND
Environmental Laboratories
2500 Gate-Way Centre Blvd., Suite300
Morrisville, NC 27560
Chain of Custody Record
. ' . POI .I\ /GE°c,?~EPit P"ROJEC;: # · _-·
</312..23-t/ ., At4ALYSES •• o, ,,S-,!,S-< J( r, I a: ' . IIJZ v/,' ---20 /DATE DUE
i..:::, J i :! ~ >, zu . )
/1 gg "; /VERBAUFAX/HARDCOPY
/1 :· ;-· r (l :..__,/-···u,.... ILC: .,:~-:., OIIJ
SAMPLE DATE AND o"'
I ........... ; .
.
Page 1 of ___ _;_____
. • .
LAB IDNO. ~ I z
SAMPLE ID IN DAYS MATRIX TIME COLLECTED I REMARKS (for lab use only)
<1{-v
.
--.. ---~:-,-v 12-2.·7:,.9y -710 'Z... v· f P,~r:-;;. 1·V/' fl-"-/ <'. r-:-,::~::::,:;~
I -/ ,_.) I -:, 0 i
j-1--/··/ 1~15 J .... e1--:=:)cl .)
. . ' ;
.. -/ I ,[/ ,J; / ID/5 '-\.i \.,• g,:·:;--:i q ; ~ " ., •. J -----
•
f;>-;i';
\: ;
·-
--.
'· ~, .
REMARKS '1.t_C, RELINQ'tjHED /-'.2~6 DATE TlllE
, J •Cuv [,v. tlt1'4 -.,;:v (1-1~-•; II_.,,. -
RE<;E,J~ED 2JY ,,.J.t,ATE ~ TIME tEUNQUISHED BY: DATE TIME· RECEIVED BY: I DATE I TIM~ I RELINQUISHED BY: DATE Tll•E
, ~!:~.,,,.,.~;:_.-,.-: /. ',fY ~5,:-.
GeoChem, Incorporate. PHOHE HO. Jan. 85 1999 02:56PM P2
'1Jeo(![!Jem Jf1rrorpor11te1J €.ertlfleb ilnnlpticHl 'J!11/Jorntorp
NC# 3ii45, NC# 336, NC# 461, EPA ID# 1 SJ
T11esday, January 05, 1999
Site Name: Burn Pit
9812-061 Cone:. PQL Dilution :0.CAC2L GCI ProJecr lnui:11 in ug,1 factor in ugtl
Field ID T-IS DateAnoly:ed:
Lab/D 8S92 J/V/8
601 602
Dich.lorodifluoromethane RDL O.l I. 1,400, Chlorornethane BDL o., I. 2.6
Vinyl Chloride BDL O.l I. .Oil Brom0mothnne BDI, 0.S I. NIA
Chloroethane llDL O.l 1. 2,800.
Trichlorofluoromethanc BDL 0.5 I. 2.100. l, 1-Dichlor~c BDL o., I. 7.
Me\hyli:nc chloride BDL o.s I. 5.
trans-1,2-Oichloroethene RDL o.s I. 70.
1,1-Dicltloroatiane BDJ. o., I. 700.
Chlorofom, BDL 0.5 I. .19
l, l, 1 • T richloroeth.anc BDL O.S I. 200.
Cubon tetrachloride DDL o., I. 3
1,2-Didiloro~c BDL o., I. .38
Trichloroahcnc DDL o.s I. 2.8
1.2-Dichloroprol'anO BDL o.s I. .56
Brnmodicliloromethsni: BDJ. o.s I. .6
2-Chlcrroethylvinylether BDL 0.5 I. N/A
cis-1,3-Dichloropropc:nc BDL o.s I. ' ..
tr:i.rn:-1.3 ~ichloropropc.':',: BDL 0.5 I. . 2
I, 1,2· Trichloroctlun,: DDL 0.5 I. ~IA
T c1.n.chloroe1hene BDI, o.s I. .7
Dibromochloromc1hanc BDL O.l I. WA
Chlnl"('lbffl::.ene BDL 0.5 I. 50.
Btomoform DDL 0.15 I. .19
l, 1,2,2, T ett;1chlorocth:mo BDL 0.5 I. NIA
1,.1-Di~hlorobou:cnc IIDL 0.5 l. 620.
1.4,Dichlorobenzcnc DDL 0.5 I. 75.
I ,']:-Dichlorobcnzenc BDL 0.5 I. 620.
lknzcnc BDL 0.5 I. J,
Toluc:nc BDL O I l. 1.000. Chloro~n;i:ene BDJ, 0.5 I. 50.
Ethylb.:nzen~ BDL M I. 29.
Pa;_t!lf. I fh, 9S!J-D(,J ug•1 tiala secnon
FROl'I GeaO·,ern. Incorparat. PH□t,E el□. 1 +919+4600. Jan. 05 1999 02:56PM P3
(J10€{Jt1n JJnrorpornft/J <!trtflirll fffnnlptfral ll.n/Jorntorp
Site Name: Burn Pil
GCI Prnject 9812-061
:Xylenc1
1,3-DlchJorobenzcnc
J ,4-Dichlorobenzcnc
1,2-Dichlorobenu:nc
Esd T-1S
NC# 37745_, NC#336, NC#461, EPA 1/J 11155
1'ut!Sday, January 05, 1999
Cone. PQL Dilulion in ug/J in ug/1 Factor
BDL 1.5 J.
BDL 0.5 I.
BDL 0.S I.
BDL 0.5 I.
E•d of 601 602
:S:CAC2L
in ug/1
530.
620.
75.
620.
FROM GeoO·,ern. Incorporated. PHOHE 1·10. 1+919+460016. Jan. 05 1999 02:5-:'PM P4
ie.eo(![!J.em ,J/ncorpornt.tb €rrtffitb fllnnlpticul l!nbor,1t.orp
NC II 377./5, NC# 336, NC# 461, EPA ID# 155
Tuesday, Januar}' 05, l 999
Sile Nam~: /Jurn Pit
Cone.. PQL Dilutic,n NCAC2l, GCI Project 9812-061 in •='1 in ug,1 Factor inugti
Fidel ID T-1' D(Jte Analyzed:
Lab ID 8595 12/3/J/98
601 602
Dichlorodiiluoromethmc DDL M 1. 1,400.,
Chforomethane BDL o.s 1. 2.6
Vinyl Chloride BDL o.s 1. .015
Bromomcthana RDL 0.S 1. NIA
Chtoroethana BDL 0.5 1. 2,800.
T richlorofluoromtthanc BDL o.s 1. 2,100 ..
1,1-Di~hlorocthcnc BDL o.s 1. 7.
Methylene chloride BDL 0.5 l. 5.
trans-1,2-Dichloroethene BDL o.s 1. 70.
l, 1-Dichlorocthanc BDL o.s l. 700.
Chloroform BDL o.s 1. .19
l. l, l • Trichloroetharic BDI, O.S I. 200.
CMbon trnacl>.loride BDI. 0.5 l. .)
I .2•Diehloroethane 8DL o.s 1. .38
Tri,hlorocthcne RDL o.s I. 2.8
1,2-0ichloroprop.:iru: BDL 0.5 I. .56
Bromodichloromcthanc DDL O.S 1. .6
2-Chloroethyl\inylethi:'r JIDL 0.5 I. NIA
cis, J ,3-Di-;hloropropcne BDL 0.5 .2
tr:uu-IJDichloropropmc RDL 0.5 .2
1.1,2-Trichloroethane DDL 0.5 I. ':{IA
Tctrachloroethcnc BDL 0.5 I. .7
Oibromochloromcthanc BDL o.s I. NIA
Chlorobattcnc ROI. 0.5 1. 50.
Bromoform DDL O.J5 I. .19
I, l .2,2-Tctrachlorocthane BDL 0.5 I. NIA
l .J.J)i..:hlorobcru:cnc BDL 0.5 I. 620.
1.4-DichlorobcnzCIJc BDI., 0.5 I. 75.
l .2·Pichlorobc:nzcnc BDL o., 620.
Bcl\1.cno DDL 0,!1 I. I.
1"olucnc DDL 0.5 I. 1,000.
Chlorobcrucnc IIDL 0.5 I. 50.
Ethylhcnzcnc IU>I. o., I. 29.
?a.~c rt fnr 9RJ 'J-0~) i.:gll rk1rn u.::r:011
FROM GeoChem, Incorporated. PHONE 1-10. 1+319+460016. Jan. 05 1339 03:00PM Pl
(!pro(l[!Jrm l!ntorporntr)) (l[rrtiffr)) fflnnlptital ll.auorntorp
Site Name: Burn Pit
GCl Project 9812-061
Xylcn~
1,3•Dicblorobenzeno
1,4-Oichloroh~J\7..e:tJ0
1,2-Dichlombcnzcne
End T-14
NC# 37745, NC# 336, NC# Jlil, EPA ID# 15.'i
foesdur, Januar_v 05, 1999
Cone. PQL Dilution
lnui:il in ug:'l Factor
BD~ u I.
Rnt. O.l I.
BDL 0.5 I.
BDL o.s I.
End of 601 601
530.
620.
75.
620.
FP.01'1 GeoChem, Incorporat. PH□flE 1·10. Jan. 05 1999 03:00PM P:2
'1/Jeoii!Jrm .i/ncorporiltr/J <!irrflfir/J ff/nalptical Jl,nboriltorp
Site Name: Burn Pit
GCI Project 9812-061
:Field IO T-JJ
Lab ID 8594
601 602
DlchJoroditluoromcthane:
Chloromcthanc
Vinyl Chloride
Bromomcthanc
Chlorocthllnc:
Trichlorotluoromerha.t1e
1, 1-Di~hluroeth=ie
~!ethylene chloride
tran.s-1.2-Oichlorocthcnc
l, 1-Diehlorocth.ane
Chlorofom1
l, l ,l • TrichtorC1ethilne
Carbon tetr.tehloride
1,2-Dichlorocthanc
Trichloro~then,:
l,Z•Diehloroprop"ne
Brmm:1di,;hloromc:th;uie
2-Chloro.:lh~•lvinylelhcr
ci~•l,3,Dichlott)Vrc,pene
tr:i.ns:-i ,30ichlor1'rropcnc
l. l .2-Trichlorocth:u1c
Tetrachloroi.:thene
Dibromochloromcth:1.ne
Chlorobenzene
Bromc,form
Dau,, Analyzed:
12/J0/98
I, 1,l,2• Tclr:i.-:hlorocth.nnc
l ,J.l)j,:.hlorobcnzcnc
1.4-Dkhlorobcru:enc
Bcru:cn::
NC# 3'7J5, NC# 336, NC# 461, EPA ID# 155
Tuesda.1•, Januarr 05, /999
Cone.
in ue/l
BDL
BDL
BDL
BDI.
BDL
BDL
BDL
DDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
RDL
BDL
BDI.
BDL
BDI.
BDL
BDL
BDL
DDL
IIDL
BDJ.
BDL
7.6
BDJ,
B01.
J->agc 11 ·'
PQL
111 us''
o.s
O.l
o.,
o.s
o.s
0.5
o.,
o.,
o.s
0.5
o.,
o.,
o.,
o.s
0.5
o.,
o.,
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.15
0.5
0.5
0.5
o.,
0.5
0.5
0.5
l)J
,u,. 9{::J).,)(_;J
Dilution
Factor
I.
I.
l.
I.
I.
I.
l.
l.
I.
1.
l.
l.
l.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
I.
l.
l.
ugl/ dote. JCCl:(Jn
!<CAC2L
in ug/1
1,400.
2.6
.01,
':-1/A
2.800.
2,100.
7. ,.
70.
700.
.19
200.
.3
.38
2.8
.>6
.6
N.'A
.2
.2
N!A
.7
NIA
50.
.10
~-'A
610.
75.
620.
I.
1,000.
50.
29.
GeoChern, 1 ncorpura ted PHOl·IE IH
Jan. 05 lSSS o::;:01PM • '1PtoiCl;tm .J/ntorporuttb €trtifit/J N11nlptical J!nbqrntqrp
Si'tt: Name! Burn Pit
GCI Project 9812-061
Xylencs
l .3-Dichlorobenlene
1,4-Dichlorobcnz.cnc
1.2.Dichlorobcnu:nc
End T-13
NC# 377-15, NC# 336, NC# 461, EPA ID# HS Tuesday, January OS, 1999
Cone, PQL Dilution tn ug/1 in ug/J Fa~r
BDL u I. BDL 0.5 1. BDL 0.5 L BDL o.,
L End of 60/ 601
NCAC 2L
inug.d
530.
620.
7S.
620.
GeoChern, Incorp,:ir-3.. PHOl•IE 110. Jan. 05 1999 03:0lPi'I P4
'9.to'1t{Jem 3/nrorporoteb ~1111/itp '1tontrol lR.eff11ltD'
GCI Project II 9812-061
601 60~
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomcthanc
Chloroetliane
Trichlorofluoromethane
l, 1-Dich!oroethene
Methylene chloride
trans-1,2-Dichloroethene
1,1-Dic:hloroethane
Chloroform
I, I°. I· Trichloroethane
Carbon tetrachloride
1,2-Dichloroethaue
Trichlorocthcnc
1,2-Dichloropropaue
Bromodichloromethane
2-Chlorocthylvinylcthcr
cis-1,3-Dichloropropcnc
trans-l ,3Dichloropropcnc
1.1,2-Trichlorocthane
Tetrachloroethene
Dibromochloromethane
Chlorobcn2cnc
Bromoform
NC# 37i.J5, NC/13315, NC#461_, EPA ID# 155
Tuesday, Jan11ar)• 05, 1999
Percent
Recovery L,b Blaruc
84 0
94 0
94 0
9S 0
82 0
93 0
92 0
84 0
94 0
94 0
89 0
95 0
96 0
92 0
96 0
94 0
92 0
94 0
98 ()
92 0
82 0
92 0
89 0
100 0
109 0
l0Wt15l deliJClion @ ideal condtrtoni
X1DL in
ilg,1
0.2
0.2
0.2
0.63
0.09
0.2
0.16
Oll
0.05
0.12
0.11
0.16
' O.IS
0.43
0.09
0.08
0.07
0.2
0.22
0.06
◊09
0.17
0.06
0.06
II.OS
FROM GeoChem, I ncorpora. PHDl•IE 1·10. Jan. 05 1999 03:02PM PS
'1Jrot[[Jem Jf nrorporntrJJ <!1111nlffp i[ontrol l{rJJ'11ltd
GC/ Project II 9812-061
I, 1,2,2 • Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobcnzene
1,2-Dichlorobcnzene
Benzene
Toluene
Chlorobenzene
Ethylbcnzcne
Xylenes
1,3-Dichlorobcnzcnc
J,4-Dichlorobenunc
1,2-Dichlorobenzene
NC# 37745, NC# 336, NC# ./61, EPA ID# 155
Tuesday, January 05, 1999
93 0
98 0
109 0
93 0
98 0
98 0
96 0
97 0
91 0
101 0
102 0
100 0
Encl of 60/ 602
0.05
0.07
0.07
6.13
0.2
0.13
0.16
0.2
0.6
6.34
0.14
0.06
Geothem, • • Incorporated
Client Project Manager
Gary McSmith
Site Name:
NHC Burn Pit
94040
SampU! type code #s :
Field Number: T\V-11
Date Sampled 12/4/98
Field Number: TW-12
Date Sampled 12/4/98
Field Number: Trip Blank
Dare Sampled 12/4/98
€trtifitll ilnalptiral 'Jla/Joratorp
NC# 37745 ,NC# 336, NC# 461, EPA ID# 155
R. Catlin & Assoc.
P.O. Box 10279
Wilmington NC
28404-0279
GCI Project#: 9812-016
iiJ,ummnrp of requesteb nanlptirnl Joor/;
3 -Air samplu;
Report Date
Friday, December I I, 1998
PO#
Date Received in lab:
Monday, December 07, 1998
4 = sludges/unknowns 1 =mli.dsampla;
Lab JD 8429
2 -liquid. sampla;
Sample Type: 2 Date Analyzed: 12/10/98 for 601602
Proper Preservation Yes
Lab ID 8430 Sample Type: 2 Date Analyzed: 12/10/98 far 601602
Proper Preservation Yes
Lab/D 8431 Sample Type: 2 Date Analyzed: 12/10/98 for 601 602
Proper Preservation Yes
+K~'"'<~~~.!:::::::.::::::. =-~-\~="~s,"'Q~\==•.,_,_ _ _y_~trt bp certifp tl)at 3l l)abt fubittutb anb approbt t!Jis bata set
2500 Gate Way Centre Blvd., Suite 300 • Morrisville, NC 27560
Telephone: [phone] • FAX: [phone]
• •
f!§ro(![l;tm 3/ncorporattll (![rrtifitll ilnalptital Jl.a/Joratorp
NC#37745, NC#336, NC# 461, EPA ID# 155
Friday, December II, 1998
Site Name: NHC Burn Pit
Cone. PQL Dilution NCAC2L
GCI Project 9812-016 in ug/1 in ug/1 Factor inug/1
Field ID TW-11 Date Analyzed:
lab ID 8429 12110/98
601 602
Dichlorodifluoromethane DDL 0.5 I. 1,400.
Chloromethane BDL 0.5 I. 2.6
Vinyl Chloride BDL 0.5 I. .Oil
Bromomethane BDL 0.5 I. N/A
Chloroethane BDL 0.5 I. 2,800.
Trichlorofluoromethane BDL 0.5 I. 2,100.
1.1-Dichloroethene DDL 0.5 I. 7.
Methylene chloride DDL 0.5 I. 5.
trans-1,2-Dichloroethene DDL 0.5 I. 70.
1,1-Dichloroethane DDL 0.5 I. 700.
Chloroform BDL 0.5 I. .19
l, l, I-Trichloroethane BDL 0.5 I. 200.
Carbon tetrachloride BDL 0.5 I. .3
1,2-Dichloroethane BDL 0.5 I. .38
Trichloroethene BDL 0.5 I. 2.8
1,2-Dichloropropanc BDL 0.5 I. .56
Bromodichloromethanc BDL 0.5 I. .6
2-Chlorocthylvinylether DDL 0.5 I. NIA
cis-1,3-Dichloropropcne BDL 0.5 I. .2
trans-1,3 Dichloropropene BDL 0.5 I. 2
l, 1,2-Trichlorocthane BDL 0.5 I. NIA
Tetrachloroethcne BDL 0.5 I. .7
Dibromochloromethane DDL 0.5 I. NIA
Chlorobenzene BDL 0.5 I. 50.
Bromofonn BDL 0.15 I. .19
1, 1,2,2-T etrachloroethane DDL 0.5 I. NIA
1,3-Dichlorobenzene DDL 0.5 I. 620.
1,4-Dichlorobenzenc BDL 0.5 I. 75.
1,2-Dichlorobcnzene BDL 0.5 I. 620.
I3cnzenc 36.5 0.5 I. I.
Toluene 4.8 0.5 I. 1,000.
Chlorobcnzene BDL 0.5 I. 50.
Ethylbenzcne 13.0 0.5 I. 29.
Page# I fo, 9812-016 ugil data secC/on
• •
(!§roitbtm l/11Corpor11tt/J ittrlifit/J iln11lptic11l Jl11/Jor11torp
Site Name: NHC Burn Pit
GCI Project 9812-016
Xylenes
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
End TW-11
NC#37745, NC# 336, NC# 461, EPA ID# 155
Friday, December II, 1998
Cone. PQL Dilution
in ugn in ug/1 Factor
18.2 u I.
BllL 0.5 I.
BDL 0.5 I.
BDL 0.5 I.
End of 601 601
Page fl :! for 9812-016 ug!l data section
NCAC2L
in ug/1
530.
620.
75.
620.
• •
(!§1o(![f;tm 3/nrorpornttlr (![1rtffftlr fflnnlptfcnl Jl.nborntorp
NC# 37745, NC# 336, NC# 461, EPA ID# 155
Friday, December II, 1998
Site Name: NHC Burn Pit
Cone. PQL Dilution NCAC2L
GC1 Project 9812-016 in ug/1 in ugll Factor in ug/1
Field ID TW-12 Date Analyzed:
lab ID 8430 12/10198
601 601
Dichlorodifluoromethane BDL o.s I. 1,400.
Ch1oromcthane BDL o.s I. 2.6
Vinyl Chloride BDL O.l I. .Oil
Bromomcthane BDL o.s I. NIA
Chloroethane BDL O.l 1. 2,800.
Trichlorofluoromethane BDL O.l 1. 2,100.
l, 1-Dichloroethene BDL O.l 1. 7.
Methylene chloride BDL O.l 1. S.
trans-1,2-Dichloroethene BDL o.s 1. 70.
l, l-Dichloroethane BDL o.s 1. 700.
Chloroform BDL o.s 1. .19
l, 1,1-Trichloroethane BDL O.l I. 200.
Carbon tetrachloride BDL O.l 1. .3
1,2-Dichlorocthane BDL O.l 1. .38
Trichloroethcne BDL o.s 1. 2.8
1,2-Dichloropropane BDL O.l 1. .56
Bromodichloromethane BDL O.l 1. .6
2-Chloroethylvinylether BDL O.S I. NIA
cis-1.3-Dichloropropene BDL O.l 1. .2
trans-l .3Dichloropropene BDL O.l 1. .2
l, 1,2-Trichloroethane BDL O.S 1. NIA
T etrachloroethene BDL O.S 1. .7
Dibromochloromethane BDL O.l 1. NIA
Chlorobenzene BDL o.s 1. so.
Bromofonn BDL O.ll 1. .19
I, 1,2,2-Tetrachloroethane BDL O.l I. NIA
1,3-Dichlorobenzene BDL o.s I. 620.
1,4-Dichlorobenzcne DDL O.l 1. 75.
1,2-Dichlorobcnzcne BDL O.l 1. 620.
Benzene BDL O.l 1. 1.
Toluene DDL O.l I. 1,000.
Chlorobenzenc BDL O.l 1. SO.
Ethylbenzene BDL O.l I. 29.
Page ff J fo, 9812-016 ugtl data secrion
• •
l§ro{f[/Jrm 3/ncorpornttb (f[rrtifitb ilnnlpticnl Jlnborntorp
Site Name: NHC Burn Pit
CCI Project 9812-016
Xylencs
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
End TW-12
NC# 37745, NC#336, NC# 461, EPA ID# 155
Friday, December 11, 1998
Cone. PQL Dilution
in ug/1 in ug/1 Factor
BDL 1.5 I.
BDL 0.5 I.
BDL 0.5 I.
BDL O.S I.
End of 601 601
Page n .J /Or 9S12-016 ug;l data secrwn
NCAC2L
in ug/1
530,
620.
75.
620.
• •
(!§10(/[/Jtm lf ntorporattll (![1rtifitll fflnalptical ll.aboratorp
NC# 37745, NC# 336, NC# 461, EPA JD# 155
Friday, December 11, 1998
Site Name: NHC Burn Pit
Cone. PQL Dilution NCAC2L
GCl Project 9812-016 in ug/1 in ug/1 Factor in ug/1
Field ID Trip Blank Date Analyzed:
Lab ID 8431 12/10198
601 602
Dichlorodifluoromethane BDL 0.5 I. 1,400.
Chloromethane BDL 0.5 I. 2.6
Vinyl Chloride BDL 0.5 L .015
Bromomethane BDL 0.5 I. NIA
Chloroethane BDL 0.5 L 2,800.
Trichlorofluoromethane BDL 0.5 I. 2,100.
I, 1-Dichloroethene BDL 0.5 I. 7.
Methylene chloride BDL 0.5 L 5.
trans-1.2-Dichloroethene BDL 0.5 I. 70.
l, 1-Dichlorocthane BDL 0.5 I. 700.
Chloroform BDL 0.5 I. .19
l, 1,1-Trichloroethane BDL 0.5 I. 200.
Carbon tetrachloride BDL 0.5 I. .3
1,2-Dichloroethane BDL 0.5 I. .38
Trichloroethene BDL 0.5 I. 2.8
1,2-Dichloropropane BDL 0.5 I. .56
Bromodichloromcthane BDL 0.5 I. .6
2-Chloroethylvinylether BDL 0.5 I. NIA
cis-1.3-Dichloropropcne DDL 0.5 I. .2
trans-1,3 Dichloropropene BDL 0.5 I. .2
1.1,2-Trichloroethane BDL 0.5 I. NIA
Tctrachloroethene BDL 0.5 I. .7
Dibromochloromethane BDL 0.5 I. NIA
Chlorobenzene BDL 0.5 I. 50.
Bromoform BDL 0.15 I. .19
l, 1,2,2-T ctrachlorocthane BDL 0.5 I. NIA
1.3-Dichlorobenzcne BDL 0.5 I. 620.
1,4-Dichlorobcnzcne BDL 0.5 I. 75.
1,2-Dichlorobenzene DDL 0.5 I. 620.
Benzene BDL 0.5 I. I.
Toluene DDL 0.5 I. 1,000.
Chlorobcnzcnc DDL 0.5 I.. 50.
Ethylbcnzcne BDL 0.5 I. 29.
Pager. 5 fo, 9812-016 ugd data section
• •
t!§ro€f;rm lf nrorporntrlJ €rrtifirl1 ilnnlpticnl Jl.nborntorp
Site Name: NHC Burn Pit
GCJ Project 9812-016
Xylenes
1,3-Dichlorobenzene
1,4-Dichlorobenzcne
1,2-Dichlorobenzene
End Trip Blank
NC# 37745, NC# 336, NC# 461, EPA ID # 155
Friday, December 11, 1998
Cone. PQL Dilution
ln ug/1 in ug/1 Factor
BDL 1.5 l.
BDL 0.5 l.
BDL 0.5 I.
BDL 0.5 l.
End of 601 602
Page It 6 for 9812-016 ugil data .section
NCAC2L
in ug/1
530.
620.
75.
620.
• •
(§rotf{Jtm l!nrorpornttlr (!f}unlitp tfontrol latlf11ltlf
GCI Project# 9812-016
601 602
Dichlorodifluoromethane
Chloromcthane
Vinyl Chloride
Bro mo methane
Chloroethane
Trichlorofluoromethane
I, 1-Dichloroethene
Methylene chloride
trans-1,2-Dichloroethene
1, 1-Dichlorocthane
Chloroform
1, I, I-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane
Trichloroethene
1,2-Dichloropropane
Bromodichloromethane
2-Chloroethylvinylether
cis-1,3-Dichloropropene
trans-l ,3Dichloropropene
1, 1 ,2-Trichlorocthane
Tetrachloroethene
Dibromochloromethanc
Chlorobcnzene
Bromoform
NC# 37745, NC#336, NC# 461, EPA ID# 155
Friday, December 11, 1998
Percent
Recovery
87
109
91
99
87
100
91
109
91
87
96
101
106
100
99
102
100
102
107
105
102
103
102
100
100
Lab Blank:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
lowest detection @ideal conditions
MDL. in
ug/t
0.2
0.2
0.2
0.63
0.09
0.2
0.16
0.11
0.05
0.12
0.11
0.16
0. 15
0.43
0.09
0.08
0.07
0.2
0.22
0.06
0.09
0.17
0.06
0.06
0.05
• •
letoit/Jtm lf morpornltlr C!l}unlitp ttontrol lR.tffultff
GCI Project# 9812-016
l, 1,2,2-Tetrachloroethane
1,3-Dichlorobcnzcne
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzene
Toluene
Chlorobenzene
Ethyl benzene
Xylenes
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,2-Dichlorobenzene
NC# 37745, NC# 336, NC# 46/, EPA ID# 155
Friday, December ll, 1998
108 0
99 0
104 0
105 0
104 0
104 0
103 0
103 0
99 0
104 0
106 0
104 0
End of 601 602
0.05
0.07
0.07
0.13
0.2
0.13
0.16
0.2
0.6
0.34
0.14
0.06
Bill To: Report To:
r-,r:,r,, !Vic Soidh
GeoChem, Incorporated ( f(/L'J-1)
Lu /,'1tl l~l rv 7
PROJECT SITE NUMBER PO# 9 :1()1.-16
SITE NAME
1/f/c fJu,n t7,+
COLLEC~D Br;Signature)
. -;,,-I".'. -0 0 -/ f) -. AELD TURNAROUND SAMPLE
,,,
Environmental Laboratories
2500 Gate Way Centre Blvd., Suite 300
Morrisville, NC 27560
Chain of Custody Record
$/ ti A~ALYSE;S / GEOCHEM ~VI~# I <I) Ct , -/\ \ n a: wz ·~io /DATE DUE \ zo ~fi zu 00 . /VERBAUFAXIHARDCOPY U.J u. a: ~ ow ci 11.
DATE AND z SAMPLE ID IN DAYS MATRIX TIME COLLECTED l(jl{[ I REMARKS
-n0-1 I 5 6. aj. I 2/ 4 /cr;., -l)'J"'i 1 r_, I'., /o;r/rar-t-!£,v-,:vt-lMt-1
' T\.J-12 5 c.. \,V, o--1~µ 'l /j?,/( ?._ ~mo(o\
-,,, ,J /2; l:,,,1, s=:; G .. iv. )___; ,~,~ Ii ~J() x, --
V I I
..
REMARKS RELINIJUISHED~Jl //_: //4 I . W·, .. C,h?r,
RECEIVED BY: 1-DATE I Tl~E, I RELINQUISHED BY: I DATE TIME RECEIVED BY: I DATE I /TIME I RELINQUISHED BY:
Thi,-""''"'"I.., ,.,.f ,...,,..,,,..,1,, Ir. rnr,.-lrin,.n,i n ,.,,.J♦t,..n ,..,..ntrnrt ff\ r,r,rlnrm fhr, e:r,ruirnc:: rnr,11nc::fnrl in fhr, ~n~luc::~~ ~pr.finn nf thl~ rlnr.11rnPnf
•
LAB IDNO.
(for lab use only)
'6° CI~ cl
Kl 17 ... _ j( )
s::-~1-::;: l
:1'/{!, TIME
F~J
DATE TIME
.l::Oct-20"99 04:49pm Frcm-CATLIN ENGINEERS AND SCIENTISTS [phone] T-5'1 P 02/01 F-520 : . --• • ·AjsJJ
Richard Catlin & Associates, Inc.
ENVIRONMENTAL ENGINEERS ANO HYOROGEOLOGISTS
January 6, 1997
bAf£ R ~Ei\Ji=b :
Ms. Beverly Hudson
Remedial Project Manager
United States Environmental Protection
Agency, Region IV
OcT e0BE:R 20 1 / <Ht
A1'.l ;...L '\,Tl CAL R t::-'5l; i-T5
r-R.CM Low FLb LU
SAM\:=Lil\J6-1E:c/lJ I QVEs . 345 Courtland Street, l\TE
Atlanta, Georgia 30365
Re: Monthly Progress Report
New Hanover County Airport Bum Pit Superfund Site
Wilmington;·New Hanover County, North Carolina
Docket No. 94-20-C
RC&A Project No. 94040-G
Dear Ms. Hudson:
Pursuant to Section XIV of the Unilateral Administrative Order for the above site,
attached is the December 1996 monthly progress report describing actions and activities
undertaken pursuant to the Order. If you have any comments or questions, please do
not hesitate to give me a call at [phone]. ~ L()\.1..'.) ~Leu .. ~ ~NALY"rlOtl..
p..1=.-::,u1-Ts I R:>~ 'RcR A. ME;TJ\t.$,
Sincerely,
4f..4~
G. Richard Garrett, P.G.
RC&A Project Manager
Enclosu!es
cc: Mark M. Davis, EPA ORC, w/enc.
Catherine Sanders, US Army Corps of Engineers, w/enc.
Wanda M. Copley, New Hanover County Attorney, w/enc.
Lonnie B. Williams, Jr., Esq.,
Attorney for Cape Fear Community College, w/enc.
Ray Church, New Hanover CoW1ty Director of
Environmental Management, w / enc.
Thomas C. Pollard, Wilmington City Attorney, w / enc.
P.O. Box 10219 :!20 Old Oa;rv RoJd
Wilrr,1ngron, NC 28405•3755
Telephone: [phone]·5861 Fax: (9 I 01 452,7S63
Wifmingron • Atlanta • Charfesron • Chi1rlorre • Americus
Oct-20-99 04:49pm From-CATLIN ENGINEERS AND SCIENTISTS +910<521563 T-591 P 03/07 f-520 • • PROGRESS REPORT DATED JANUARY 6, 1997
REMEDIAL DESIGN/ REl'vlEDIAL ACTION
NEW HANOVER COUNTY AIRPORT BURN PIT SuPERFUND SITE
WILMINGTON, NEW HANOVER COUNTY, NOR1H CAROLINA
This monthly progress report is submitted pursuant to Section XIV of the Unilateral
Administrative Order for the referenced site.
I. ACTIONS TO COMPLY WITH ORDER
Ground water samples were collected from monitoring wells MWS-002 and
MWD-002 using a low flow sampling technique.
II. RESULTS OF SAMPLING AND ANALYSIS
Results indicate no occurrence of RCRA metals above Federal or State standards.
These results suggest that the previous occurrence of RCRA metals was associated
with preservative leaching of trace metals from the high concentrations of high
solids found in previous samples.
ill. PLANS, REPORTS, AND OTI-IER DELIVERABLES
No deliverables are submitted as of this time period other than RCRA metals
laboratory analyses.
IV. WORKPlAN FOR NEXT MONTI-I
It is proposed that work commence on remedial design which employs an in-situ
air sparging treatment approach. This should follow USEPA approval and PRP
budget approval.
V. PROBLEMS ENCOUNTERED
No additional problems were encountered during this period of time.
Respectfully submitted this the 6th day of January, 1997.
G. Richard Garrett, P.G.
RC&A Proiect Manager
N~w Hanovt!r County A,'rpon Burn Pu, 4U4URG22.LT8 Richard Carlin & A.Hocllltes, foe.
RC&A Project No. 94040-G ENVIRONMENTAL ENGINEERS AND HYDROGEOLOGl$TS
Oct-20-9i 04:4lpm from-CATLIN ENGINEERS AND SCIENTISiS [phone] T-5" P 04/01 F-520 Ge~nem, Incot~rated-~-
Env ronmental Laboraror es
Client Projec1 Manager
.Hr Rick Garre//
Site Name:
€trflfieiJ ffnalptical 'J[a/Joratorp
NC# 377./5 ,NC# 336, NC# 461, EPA ID# 155
R. Carlin & Assoc.
P.O. Box 10279
Vew Hanover Co. Airport/ Burn Pit Superfimd Site
Wilmingwn NC
28405 040402
Sa1tsplc (ypr: codlf tit:
fi«ld Number: MWS.p02
Dare Sainplrd 111'211?6
Fltld Numbtr: MWS--002
Datt :Wmplt1a 11/21196
F/t1ldN1,mb11r: r..lWD-002
Q(J/1!1 Somplaa lll'H/96
freta .,\"u111o~r· .'-IW0-002
Va1t1 :::,a111pl~d I I '7!/96
GCI Project#: 9611-048
/$,ummarp uf requtSttlJ annlptiral /uorft
I • roJul IQttrpla: l -t..,...i ,-pi-.-1 • AW ,amp/.b;
lab ID 4423 Sa,.pi< Type: l Dat•AnPl;Y%ec:i: \ !/2'1')6
al J6:JJ
~b ID 4423 Sampl• Typ«: 2 O(Jtc AnaJyzsd: 12/4196
ar 16:5!
Lab ID 4424 Sgmplt Typ..:.-2 Dore Analy:cd: 11/2$/96
QI /1:Jj
[QO/D ~'t'24 S~mpte Type: Dare Ana(y:ed: 111;196
a{ J/_•J5
Report Dale
Wednesdav, December 04, / 996
PO# 96// 22-2
Dtlte Received in /ai,;
Friday, November 22, 1996
-' • rWG(Jc:stU/IAnatwJI
for ~CRA mt1ol:s
far TSS
for RC::M inata/J
;0, TSS
3.l ;L ~-,__;__ .,. K & ~.,.'._-----, l!Jrrr tJv rrm(v tt,nr 3J hnnr i-trtlirtDtb nnb itppr□nr r1Jili hara srt
2:;00 Gat" Way Centre Blvd., Suite 300 • M0msv1lle, NC 27560
Telephone: [phone] • FAX: [phone]
Oct-10-99 04:<9pm Fram-CATLIN ENGINEERS ANO SCIENTISTS •910'517563 T-:i I p 05/07 F-:10 • • '5to'1:{Jtm Jlnrorporlltt/J (!{rrtifit/J illllliptitlli 1lt1/Jor4torp
NC# 377J5, NC# 336, NC# 461, EPA ID# 155
W,,tncsduy, December 04, 1996
SiJ,-Name: Ne,, Hanover Co. Airpon • Burn Pit Sup
CCI Project# 9611-048 Com~. Pl PQLin DBu.tion NCAC2L
met] m,;/1 F'1ctor in mg.Ii
Ficl4 10 ~1ws..002 lab 10 .J..12]
Dart! Anaty:11d: ! /IJSl96
RCRA rmnals
,'ln<nlc BDL 0.01 1,0 0.0l
Barium BQL o,, l0,0 2.0
Ca4nµum BQL 0.00"li 1.0 0.OOl
Chtomiwm OQL 0.0l :.o O.Ol
t....d nQL 0.0ll i,O 00ll
Mercury BQL 0.001 1.0 0.0011
Selenium BQL 0.D2 1.0 0.0l
Silver BQL 0.01 1.0 0.OIB
TSS
Tota.I Su~pmdcd Solith ODL l.0 1.0 NIA
Fiold 10 MWP-002 !..ab/D JJ].I
Dot~ A naly;~d: //l2H96
RCRAll'l~III~
Amnic BQL 0.01 1.0 0.0l
Blll'Wm 0.Jl 0.l -io,o 2.0
C~um OQL 0.00~ 1.0 0,005
Chromium OQL 0 0l 1.0 0,05
l.,ad BDL O.Ol"li 1.0 0,0ll
Mercury OQL. 0.001 \.0 0.0011
Sclcmum DQL 0.02 1.0 0.05
Silvc-r DQL 0.DI 1.0 0.018
TSS
To1.ilil Su,pcndc:d Solidi. UDL J,0 ID NlA
Oct-20-ii 0<,49pm From-CATLIN ENGINEERS AND SCIENTISiS +9i04527563 i-S~i P.Q6/G7 F-520 • •
~ro(![f;rm lfntorpornttlJ C(f}lllJlltp (![ontrol J!ir11ultd
GC/ Projecr # 961 I-0.JS
RCRArncu.b
Arseruc
Barium
Cadmium
Clvomium
Lead
Mercury
Scleniurn
Silver
Total Suspended Solids
NC# J7i.J5, NC# 336, NC# 461, EPA ID# I 55
Wednesdu.v, December 04, I 996
L.ab alonk,
!OS 0
99 u
100 0
101 0
101 0
82 0
108 0
96 0
9J 0
lowa1 detection llITlit@ idilal concliuoru
MDL. i11
m8/I
o oos
0.005
0,0005
0,0005
0,001
0.0004
0.005
0.0005
5
Geoct1en1, lncorporc1ted o/;;t:J {a~ t-1~ ~ l.4f-At ~ &rt· (uf'4':i F.nvironrnerital Laboralories
Bil!To:4 (A-
m ' ~ 2500 Gate Way Centre Blvd., Suite 300
Morrisvllle, NC 27560
Chain of Custody Record
•
..
Page 1 of _/_ _
Pfl°t}'I'/ITENUMBER PO, r . . . / GEOCHEMPROJECTI~ /2 tJ r./-O 2.. CJ(,fll7..--Z.. "' -..;: ANALYSES l/-0' B a: UIZ
WNAME ~ P,f-zo .~ / OATEOUE ~ Uimm.M. G,. ~ ........ + ~~ /2 2 ?0
COLLECTE'/!1;1:;_ ']i;_l7 oo ,·~ / VERBAlJFAXIHAROCOPY u .. k .,, -, u.a: ow
FIELD TURNAROUND S~PlE DATE AND
ci .. I LAB IDNO. z ,~ i/ SAMPLE ID IN DAYS. IJATR1X TIME COLLECTED REMARKS (for lab use only)
Mt,J~~2. /0 ~ ll/21/-11, /IJ s--; I I I\ '--'10· TT 1 I • l~.,Ki (~oW <1123
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BEMARKS RELINQUISHED BY: OAJ"E TIME_
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Oct-20-99 04:46pm frcm-CAillN ENGINEERS ANO SCIENTISTS [phone] • FAX Transmi.s,ion from. ..
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ENGINEERS and SCIENTISTS
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·:·:•
;.
GROUND-WATER SAMPLING INVESTIGATION
NEW HANOVER BURN PIT SITE
WILMINGTON, NEW HANOVER COUNTY, NORTH CARO
ESD PROJECT NUMBER 93-0122
DECEMBER 1992
INTRODUCTION
Q,urw () ii
D ,. ----· ,..... "'l n .
1l FE3 2 3 199~
1U'G l3 L:::; u Li
EPA. -REGION IV
ATLANTA, GA
On December 9, 1992, Roger E. Carlton and Tracela Vaden of
the Environmental Services Division collected a total of six
ground water samples from permanently installed monitoring wells
located at the New Hanover Burn Pit Site near Wilmington, North
Carolina. These samples were analyzed for the presence of
volatile organics as requested by the Waste Management Division.
Temperature, conductivity, and pH of the ground water were
determined during purging.
BACKGROUND
The site is located on Gardner Drive, west of the New
Hanover County Airport. Although termed a "pit", the burn pit
does not extend below land surface, and is of earthen-berm
construction, roughly 2.5 fe,~t above the ground. The pit is
located in the north·east corner of a four-acre tract once used
for fire training exercises. The north side of the pit contains
a valve which was formerly used to drain water from the pit onto
the ground.
RESULTS AND DISCUSSION
Purgeable organic compounds were detected in four of the six
wells sampled (Table 1). Benzene, the compound of concern, was
detected at concentrations ranging from 6.0 ug/1 in MWS-001 to
100 ug/ 1 in MWD-002.. Additional compounds detected included
other benzenes, toluene, and xylenes. Tables 2a, 2b, 2c,and 2d
reflect results of the five sampling events since April 1991.
Note that the concentrations for the individual compounds did not
vary greatly.
1
•• •
Complete data reports for the December 1992 sampling event
are included as Appendix A .
. SAMPLING METHODOLOGY
Groundwater samples were collected from six on-site
permanent monitoring wells. six sets of samples were collected
for VOA analyses after the wells were purged with peristaltic
pumps. The purge water was poured onto the ground away from the
wells.
The samples were labeled using the previous well
designations, MWS-001, MWD-001, MWS-002, MWD-002, MWD-003, AND
MWS-004 as identifiers. Samples were returned to the ESD
laboratory on December 10, 1992.
Samples were collected and handled in accordance with the
US-EPA, Region IV, Environmental Services Division, Environmental
Compliance Branch Standard Operating Procedures and Quality
Assurance Manual, February 1, 1991. Samples were analyzed
according to the Analytical Support Branch, Laboratory Operations
and Quality Control Manual, September 1990.
2
• •
TABLE 1
VOLATILE ORGANIC AKALYTICAL DATA stfoMARY
NEU HANOVER BURN PIT SITE
UILMINGTON. troRTH CAROLINA
DECEHBER 1992
MYS-001 MIID-001 MYS-002
12/09/92 12/09/92 12/09/92
1620 1630 1525
PURGEABLE ORGANIC COMPOUNDS µg/l µg/l µg/l
CARBON OISULFIOE 5_0J
METHYL ISOBUTYL KETONE
BENZENE 6.0 9.4J 66
TOLUENE 1. 1J 1.0J ETHYL BENZENE 12 10 26 (M-AND/OR P-)XYLENE 6.9 10 2.4J 0-XYLENE 15 20 5.4J
P-ISOPROPYLBENZENE 0.74J
P-ISOPROPYLTOLUENE 1. 2J ETHYLETHER 200JN
ETHYLMETHYLBENZENE (2 ISOMERS) 30JN
1,3,5-TRIMETHYLBENZENE 9. 1 9.4J 4.2J
METHYLPROPANOL 30JN
METHOXYMETHYLPROPANE BOJN TETRAHYDROTHIOPHENE 20JN ETHYLMETHYLBENZENE 10JN
ISOPROPYLBENZENE 1.BJ 1.6J 3.4J
N-PROPYLBENZENE 2.9J 3.0J 6.BJ
1,2,4-TRIMETHYLBENZENE 31 36 18
ETHYLMETHYLBENZENE (3 ISOMERS) 50JN
PETROLEUM PRODUCT N
FOOTNOTES:
J ESTIMATED VALUE
N PRESUMPTIVE EVIOENCE OF PRESENCE OF MATERIAL
MATERIAL YAS ANALYZED FOR BUT NOT OETECTED
3
M\.ID-002 MYS-003 MYS-004
12/09/92 12/09/92 12/09/92
1555 1720 1730
µg/l µg/l µg/l
5.2J
100
3.4J
43
23
30
4.3J
7.5J --.
64
90JN
N
•
I I
MWS
001
12/92 6.0
07/92 5.2
1.1/91 4.2
05/91 1.1
04/91 3.5
FOOTNOTES:
J • ESTIMATED VALUE
•
TABLE 2a
NEW HANOVER BURN PIT
WILMINGTON,NORTH CAROLINA
BENZENE (µg/1)
MWD MWS MWD MWS
001 002 002 003
9.4J 66 100 ---
14 88 96 ---
7.7 74 110 ---
7.7 31 94 ---
7.9 110 110 ---
~ MATERIAL ~AS ANALYZED FOR BUT NOT DETECTED
4
MWS
004
---
---
---
---
---
•
I I MWS
001
12/92 12
07/92 7.1
11/91 4.5
05/91 1.2
04/91 3.3
FOOTHOTES:
•
TABLE 2b
NEW HANOVER BURN PIT
WILMINGTON,NORTH CAROLINA
ETHYL BENZENE (µg/1)
MWD MWS MWD MWS
001 002 002 003
10 26 43 ---
16 39 39 ---
8.8 28 37 ---
7.4 9.2 30 ---
8.5 43 34 ---
----MATERIAL UAS ANALYZED FOR BUT NOT DETECTED
5
MWS
004
---
---
---
---
---
•
I II
MWS
I 001
12/92 1.1
07/92 0.51
11/91 ---
05/91 ---
04/91 ---
FOOTNOTES:
•
TABLE 2c
NEW HANOVER BURN PIT
WILMINGTON,NORTH CAROLINA
TOLUENE (µg/1)
MWD
I
MWS
I
MWD·
I
MWS
001 002 002 003
1.0 3.4 ---
1.4 0.85 2.8 ---
1.1 ---5.9 ---
1.5 2.5 13 ---
2.0 5.8 14 5.8
··· -MATERIAL YAS ANALYZED FOR BUT NOT DETECTED
6
I
MWS
I 004
---
---
---
---
0.89
•
I I
MWS
001
12/92 21. 9
07/92 14 .1
11/91 13.1
05/91 4.1
04/91 10.8
FOOTNOTES:
•
TABLE 2d
NEW HANOVER BURN PIT
WILMINGTON,NORTH CAROLINA
TOTAL XYLENES (µg/1)
MWD MWS MWD MWS
001 002 002 003
30 7.8 53 ---
41 10.9 38 ---
25 7.8 76 ---
21. 9 9.1 82 0.77
25.3 19.4 82 ---
··· · MATERIAL YAS ANALYZED FOR BUT NOT DETECTED
7
MWS
004
---
---
---
---
---
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD. ATHENS. GA.
**•. * •••••••••••••••••••••••••••••• • • • • • • • • • PROG ELEM: SSF • • • • • • • • • • • • • • • • • •
COLLECTED BY: R CARLTON
•• PROJECT NO. 93-0122 . SAMPLE NO. 73509 SAMPLE TYPE: GROUNDWA
•• SOURCE: NEW HANOVER BURN PIT
•• STATION ID: MWS-001
CITY: WILMINGTON
COLLECTION START: 12/09/92
ST: NC 1620 STOP: 00/00/00
12/30/92
• • •
•••••••••••••••• * •••••••••••••••••••••••••••••••••••••••••••••••• --~
UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
5.0U 5.0U 5.0U 5.0U 5.0U 5.0U sou 5.0J
5.0U 5.0U 5.0U 5.0U 5.0U 50U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 6.0 5.0U·
5.0U 5.0U 5.0U
CHLOROMETHANE
VINYL CHLORIDE
BROMOMETHANE
CHLOROETHANE
TRICHLOROFLUOROMETHANE
1 .1-DICHLOROETHENE(1 .1-DICHLOROETHYLENE)
ACETONE
CARBON DISULFIDE
METHYLENE CHLORIDE
TRANS-1.2-DICHLDROETHENE
1 .1-DICHLORDETHANE
CIS-1 .2-DICHLOROETHENE
2.2-DICHLOROPROPANE
METHYL ETHYL KETONE
BROMOCHLOROMETHANE
CHLOROFORM
1 .1 .1-TRICHLOROETHANE
1.1-DICHLOROPROPENE
CARBON TETRACHLORIDE
1 .2-DICHLOROETHANE
BENZENE TRICHLOROETHENE(TRICHLOROETHYLENE)
1.2-DICHLOROPROPANE
DIBROMOMETHANE
BROMODICHLOROMETHANE
•*•REMARKS•••
••-FOOTNOTES•••
5.0U 12U
1 . 1 J 5.0U 5.0U 5.0U 5.0U 12U 5.0U 5.0U 5.QU 12 6.9 15 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U s.ou
CIS-1 .3-DICHLOROPROPENE
METHYL ISOBUTYL KETONE
TOLUENE TRANS-1 .3-DICHLOROPROPENE
1. 1 .2-TRICHLOROETHANE
TETRACHLDROETHENE(TETRACHLOROETHYLENE)
1 .3-DICHLOROPROPANE
METHYL BUTYL KETONE
DIBROMOCHLORDMETHANE
CHLOROBENZENE
1 .1. 1 .2-TETRACHLOROETHANE
ETHYL BENZENE
(M-AND/OR P-)XYLENE
0-XYLENE STYRENE BRDMOFORM
BROMDBENZENE
1 .1.2.2-TETRACHLOROETHANE
1 .2.3-TRICHLOROPRDPANE
0-CHLDROTOLUENE
P-CHLDROTOLUENE
1 .3-DICHLDROBENZENE
1 .4-DICHLOROBENZENE
1.2-DICHLOROBENZENE
-••REMARKS•••
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTIJAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERJAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER JS THE MINIMUM QUANTJTATION LIMIT.
•
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION IV ESD. ATHENS. GA. 12/30/92
*** *. * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * * * * * • * * * * * * * • * *
•• PROJECT NO. 93-0122 SAMPLE NO. 73509
· ,, SOURCE: NEW HANOVER BURN PIT SAMPLE TYPE: GROUNDWA PROG ELEM: SSF COLLECTED BY: R CARLTON
,, STATION ID: MWS-001
~~•FOOTNOTES•••
1.8J 2.9J 9.1 31 0.74J 50JN
N
ANALYTICAL RESULTS UG/L
!SOPROPVLBENZENE
N-PROPYLBENZENE
1 .3.5-TRIMETHVLBENZENE
1 .2.4-TRIMETHYLBENZENE
P-ISOPROPYLBENZENE
ETHYLMETHVLBENZENE (3 ISOMERS)
PETROLEUM PRODUCT
CITY: WILMINGTON ST: NC
COLLECTION START: 12/09/92 1620 STOP: 00/00/00
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAJ-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER!AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•
•
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION JV ESD, ATHENS, GA.
?URGEABLE ORGANICS DATA REPORT ..
" ••
PROJECT NO. 93-0122 SAMPLE NO. 73508 SAMPLE TYPE: GROUNDWA
SOURCE: NEW HANOVER BURN PIT STATION JD: MWD-001
PROG ELEM: SSF COLLECTED BY: R CARLTON CITY: WILMINGTON ST: NC COLLECTION START: 12/09/92. 1630 STOP: 00/00/0D
12/22/92
•• ••
" •• ••• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • * * ••••••••••••••••••••••••••• -~-
UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
10U 10U
10U 10U 10U 10U 100U 25U 10U 10U 10U iDU 10U 1DDU 10U 1DU 1DU
10U 1DU 10U 9.4J
lDU 10U lDU 1DU
CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRJCHLOROFLUOROMETHANE 1, 1-DICHLOROETHENE(1, 1-DJCHLOROETHYLENE}
ACETONE CARBON DISULFIDE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE 1 ,1-DJCHLOROETHANE CJS-1 .2-DICHLOROETHENE 2.2-DICHLOROPROPANE METHYL ETHYL KETONE BROMOCHLOROMETHANE CHLOROFORM 1 ,1 ,1-TRJCHLOROETHANE 1 .1-DICHLOROPROPENE CARBON TETRACHLORIDE 1 .2-DJCHLOROETHANE BENZENE TRJCHLOROETHENE(TRJCHLOROETHYLENEJ 1.2-DICHLOROPROPANE DIBROMOMETHANE BROMDDJCHLOROMETHANE
10U 25U 10U 10U lOU 10U 10U 25U 10U 1DU 10U 10 10 20 1DU 10U lOU 10U 10U 10U 10U lOU lOU lOU
CIS-1 .3-DJCHLOROPROPENE METHYL JSOBUTYL KETONE TOLUENE TRANS-1 ,3-DJCHLOROPROPENE 1,1,2-TRJCHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENE}
1,3-DJCHLOROPROPANE METHYL BUTYL KETONE DIBROMOCHLOROMETHANE CHLOROBENZENE 1 ,1 ,1.2-TETRACHLOROETHANE
ETHYL BENZENE (M-AND/OR P-}XYLENE 0-XYLENE STYRENE BROMOFORM BROMOBENZENE 1 .1 ,2,2-TETRACHLOROETHANE 1,2.3-TRICHLOROPROPANE 0-CHLOROTOLUENE P-CHLOROTOLUENE 1,3-DJCHLOROBENZENE 1,4-DICHLOROBENZENE 1 ,2-DICHLOROBENZENE
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAJ-JNTERFERENCES •J-ESTJMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE JS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER JS THE MINIMUM QUANTJTATION LIMIT.
•
•
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION JV ESD. ATHENS. GA. 12/22/92
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * * * * * * * * * * * * *
•• PROJECT NO. 93-0122 SAMPLE NO. 73508 SAMPLE TYPE: GROUNDWA
n SOURCE: NEW HANOVER BURN PIT
•• STATION ID: MWD-001
"'**FOOTNOTES**"'
1 ,6J 3.0J 9,4J 36 ,. 2J
200JN 30JN
ANALYTICAL RESULTS UG/L
JSOPROPYLBENZENE
N-PROPYLBENZENE
1 .3.5-TRIMETHYLBENZENE 1 ,2,4-TRIMETHYLBENZENE
P-ISOPROPYLTOLUENE
ETHYLETHER
ETHYLMETHYLBENZENE ( 2 I SOMERS)
PROG ELEM: SSF COLLECTED BY: R CARLTON
CITY: WILMINGTON ST: NC
COLLECTION START: 12/09/92 1630 STOP: 00/00/00
•A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE Of MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM OUANTJTATJON LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•
•
PURGEABLE ORGANICS DATA REPORT • * • • * * • • • * • • • • • • * • * •
PROJECT NO. 93-0122 SAMPLE NO. 73506 SOURCE: NEW HANOVER BURN PIT STATION ID: MWS-002
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
• • * • * • • • * * • • • SAMPLE TYPE: GROUNDWA PROG ELEM: SSF COLLECTED BY: R CARLTON
CITY: WILMINGTON COLLECTION START: 12/09/92
ST: NC 1525 STOP: 00/00/00
12/22/SL
••• * •••••••• *. * ••• * •••••• * ••••• *. * * •••• * *. * * * * •• * ••• *. * * * •••••• *. -~-UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
10U 10U 10U 10U ,ou
10U 100U 25U 10U 10U 10U 10U 10U 100U 10U 10U 10U 10U 10U 10U 66 10U
10U 10U
1 OU
CHLOROME THANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE 1, 1-DICHLOROETHENE(l ,1-DICHLOROETHYLENE)
ACETONE CARBON DISULFIDE METHYLENE CHLORIDE TRANS-1 ,2-DICHLOROETHENE 1,1-DICHLOROETHANE CIS-1 .2-DICHLOROETHENE 2.2-DICHLOROPROPANE METHYL ETHYL KETONE BROMOCHLOROMETHANE CHLOROFORM 1,1,1-TRICHLOROETHANE 1 ,1-DICHLOROPROPENE CARBON TETRACHLORIDE 1 ,2-DICHLOROETHANE BENZENE TRICHLOROETHENE(TRICHLOROETHYLENE) 1 .2-DICHLOROPROPANE DIBROMOMETHANE BROMODICHLOROMETHANE
10U 25U 1. OJ 10U ,ou 10U 10U 25U 10U ,ou 10U 26 2.4J 5.4J 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U
CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1 ,3-0ICHLOROPROPENE 1 ,1 ,2-TRICHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1,3-DICHLOROPROPANE METHYL BUTYL KETONE DIBROMOCHLOROMETHANE CHLOROBENZENE 1. 1, 1 ,2-TETRACHLOROETHANE ETHYL BENZENE (M-AND/OR P-)XYLENE 0-XYLENE STYRENE BROMOFORM BROMOBENZENE 1,1,2,2-TETRACHLOROETHANE 1,2.3-TRICHLOROPROPANE 0-CHLOROTOLUENE P-CHLOROTOLUENE 1 ,3-DICHLOROBENZENE 1,4-D!CHLOROBENZENE 1 ,2-DICHLOROBENZENE
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•
•
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION JV ESD, ATHENS, GA. 12/22/92
*** * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * * • * * * * * * * * * * * • * * * * * * * * * * * * * * * * * *
•• PROJECT NO. 93-0122 SAMPLE NO. 73506
•• SOURCE: NEW HANOVER BURN PIT
SAMPLE TYPE: GROUNDWA PROG ELEM: SSF COLLECTED BY: R CARLTON
•• STATION ID: MWS-002
•••FOOTNOTES•••
3.4J 6.8J 4.2J 18 30JN SOJN 20JN 10JN
ANALYTICAL RESULTS UG/L
ISOPROPYLBENZENE
N-PROPYLBENZENE
1,3,5-TRIMETHYLBENZENE
1,2.4-TRIMETHYLBENZENE
METHYLPROPANOL
METHOXYMETHYLPROPANE
TETRAHYDROTH!OPHENE
ETHYLMETHYLBENZENE
CITY: WILMINGTON ST: NC
COLLECTION START: 12/09/92 1525 STOP: 00/00/00
•A-AVERAGE VALUE •NA-NOT ANALYZED •NA!-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTJVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER JS THE MINIMUM QUANTlTATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS JS NECESSARY FOR VERIFICATJO~.
•
•
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD, ATHENS, GA.
PURGEABLE ORGANICS DATA REPORT • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • ••• PROJECT NO. 93-0122 SAMPLE NO. 73507 SAMPLE TYPE: GROUNDWA SOURCE: NEW HANOVER BURN PIT STATION ID: MWD-002
PROG ELEM: SSF COLLECTED BY: R CARLTON CITY: WILMINGTON ST: NC COLLECTION START: 12/09/92 1555 STOP: 00/00/00
12/22/92
• • • ... .. .. .. ..
••• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • ••• UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
ZOU 20U 20U 20U 20U 20U 200U 50U 20U 20U 20U ZOU ZOU 200U ZOU ZOU ZOU 20U ZOU ZOU ;oo
20U ZOU 20U ZOU
CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE 1. 1-DJCHLOROETHENE(l ,1-DJCHLOROETHYLENE)
ACETONE CARBON DISULFIDE METHYLENE CHLORIDE TRANS-1 ,2-DICHLOROETHENE 1 ,1-DICHLOROETHANE CIS-1 ,2-DICHLOROETHENE 2.2-DICHLOROPROPANE METHYL ETHYL KETONE BROMOCHLOROMETHANE CHLOROFORM 1 ,1 ,1-TRICHLOROETHANE 1. 1-DICHLOROPROPENE CARBON TETRACHLORIDE 1.2-DICHLOROETHANE BENZENE TRJCHLOROETHENECTR!CHLOROETHYLENEJ 1 .2-DICHLOROPROPANE DIBROMOMETHANE BROMODICHLOROMETHANE
20U 5.2J. 3.4J 20U ZOU ZOU ZOU 50U ZOU ZOU ZOU 43 23 30 20U 20U ZOU ZOU ZOU ZOU ZOU 20U ZOU 20U
CIS-1,3-D!CHLOROPROPENE METHYL JSOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1 ,1,2-TRICHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENEJ
1,3-DICHLOROPROPANE METHYL BUTYL KETONE DIBRDMOCHLOROMETHANE CHLOROBENZENE 1. 1 ,1 ,2-TETRACHLOROETHANE ETHYL BENZENE CM-AND/OR P-)XYLENE 0-XYLENE STYRENE BROMOFORM BROMOBENZENE 1,1.2.2-TETRACHLOROETHANE 1 .2.3-TRICHLOROPROPANE O-CHLOROTOLUENE P-CHLOROTOLUENE 1 .3-DICHLOROBENZENE 1 ,4-DJCHLOROBENZENE 1,2-DICHLOROBENZENE
•••FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAJ-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF M~TERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•
•
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM
EPA-REGION JV ESD, ATHENS. GA.
MISCELLANEOUS PURGEABLE ORGANICS -DATA REPORT ,,, **l< *. * * * * * * * * * *. * *. * * * * * * * *"' * * * *
PROJECT NO. 93-0122 SAMPLE NO. 73507 SAMPLE TYPE: GROUNDWA
SOURCE: NEW HANOVER BURN PIT
STATION ID: MWD-002
4.3J 7.5J 64 90JN
N
ANALYTICAL RESULTS UG/L
JSOPROPYLBENZENE N-PROPYLBENZENE
1.2.4-TRIMETHYLBENZENE ETHYLMETHYLBENZENE (3 ISOMERS)
PETROLEUM·PRODUCT
*••FOOTNOTES••*
PROG ELEM: SSF COLLECTED
CITY: WILMINGTON
COLLECTION START: 12/09/92
BY: R CARLTON ST: NC 1555 STOP: 00/00/00
12/22/92
•A-AVERAGE VALUE •NA-NOT ANALYZED •NA!-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPT!VE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTJTATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•
•
?URGEABLE ORGANICS DATA REPORT * • • * • * • * * • * • • * • • • • * • PROJECT NO. 93-0122 SAMPLE NO. 73510 SOURCE: NEW HANOVER BURN PIT
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA.
* • * • • • * • * • • * * SAMPLE TYPE: GROUNDWA PROG ELEM: SSF CITY: WILMINGTON COLLECTION START: 12/09/92
12/24/92
•••
STATION ID: MWS-003
*** *. *. *. * •• *. * ••• *. * ••• * * * *. * * * •• * * * ••• *. *. * * •• * * * * * ••• * *. * * •• * * -~· UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
5.0U
5.0U S.OU S.OU s.ou
5.0U sou 12U 5.0U
5.0U s.ou s.ou
5.0U sou 5.0U s.ou s.ou s.ou S.OU 5.0U 5.0U 5.0U 5.0U 5.0U s.ou
CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE 1. 1-DICHLOROETHENE(l. 1-D!CHLOROETHYLENE)
ACETONE CARBON DISULFIDE METHYLENE CHLORIDE TRANS-1 .2-DICHLOROETHENE 1 .1-DICHLOROETHANE CIS-1 .2-DICHLOROETHENE 2.2-DICHLOROPROPANE METHYL ETHYL KETONE BROMOCHLOROMETHANE CHLOROFORM 1. 1. 1-TRI_CHLOROETHANE 1 .1-D!CHLOROPROPENE CARBON TETRACHLORIDE 1.2-DICHLOROETHANE BENZENE TRICHLOROETHENE(TRICHLOROETHYLENE) 1 .2-DICHLOROPROPANE DIBROMOMETHANE BROMODICHLOROMETHANE
s.ou 12U s.ou 5.0U s.ou 5.0U 5.0U 12U s.ou s.ou 5.0U s.ou 5.0U 5.0U s.ou s.ou s.ou 5.0U 5.0U s.ou 5.0U 5.0U s.ou s.ou
CIS-1 .3-D!CHLOROPROPENE METHYL ISOBUTYL KETONE
TOLUENE TRANS-1.3-DICHLOROPROPENE
1. 1 .2-TRICHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1 .3-DICHLOROPROPANE METHYL BUTYL KETONE DIBROMOCHLOROMETHANE CHLOROBENZENE 1. 1. 1 ,2-TETRACHLOROETHANE
ETHYL BENZENE (M-AND/OR P-)XYLENE 0-XYLENE STYRENE BROMOFORM BROMOBENZENE 1 ,1.2.2-TETRACHLOROETHANE 1 ,2.3-TRICHLOROPROPANE 0-CHLOROTOLUENE P-CHLOROTOLUENE 1 ,3-DICHLOROBENZENE 1 .4-DICHLOROBENZENE 1.2-DICHLOROBENZENE
***FOOTNOTES••• •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-EST!MATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUM6ER IS THE MINIMUM QUANTITATION LIMIT.
•
•
PURGEABLE ORGANICS DATA REPORT
* • • * * * * * • * • * * * * * * * • * PROJECT NO. 93-0122 SAMPLE NO. 73511 SOURCE: NEW HANOVER BURN PIT STATION ID: MWS-004
SAMPLE AND ANALYSIS MANAGEMENT SYSTEM EPA-REGION IV ESD. ATHENS. GA.
* * * * * * * * * * * * * SAMPLE TYPE: GROUNDWA PROG ELEM: SSF COLLECTED BY: R CARLTON
CITY: WILMINGTON COLLECTION START: 12/09/92
ST: NC 1730 STOP: 00/00/00
12/24/92
*** •• * * *. * *. * * *. * * * * * * * * *. * * * * * * * * * * * * * * * * * * *. * * * * * * * * * * * * * * * * * * * *** UG/L ANALYTICAL RESULTS UG/L ANALYTICAL RESULTS
S.OU S.OU S.OU S.OU S.OU
5.0U sou 12U S.OU S.OU S.OU S.OU S.OU sou 5.0U 5.0U S.OU 5.0U 5.0U
5.0U
5.0U s.ou·
5.0U ~.;. OU S.OU
CHLOROMETHANE VI NVL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE 1 .1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
ACETONE CARBON DISULFIDE METHYLENE CHLORIDE TRANS-1 .2-DICHLOROETHENE 1,1-DICHLOROETHANE CIS-1 .2-DICHLOROETHENE 2.2-DICHLOROPROPANE METHYL ETHYL KETONE BROMOCHLOROMETHANE CHLOROFORM 1,1,1-TRICHLOROETHANE 1. 1-DICHLOROPROPENE CARBON TETRACHLORIDE 1 .2-DICHLOROETHANE BENZENE TRICHLOROETHENE(TRICHLOROETHYLENE) 1 .2-DICHLOROPROPANE DIBROMOMETHANE BROMODICHLOROMETHANE
**•REMARKS•••
S.OU 12U 5.0U S.OU S.OU S.OU 5.0U 12U S.OU 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U
CIS-1 ,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1 .3-DICHLOROPROPENE 1 ,1 .2-TRICHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENE)
1 .3-DICHLOROPROPANE METHYL BUTYL KETONE DIBROMOCHLOROMETHANE CHLOROBENZENE 1. 1, 1 ,2-TETRACHLOROETHANE
ETHYL BENZENE (M-AND/OR P-JXYLENE
0-XYLENE STYRENE BROMOFORM BROMOBENZENE 1 ,1 .2.2-TETRACHLOROETHANE 1.2,3-TRICHLOROPROPANE 0-CHLOROTOLUENE P-CHLOROTOLUENE 1.3-DICHLOROBENZENE 1 ,4-DICHLOROBENZENE 1 ,2-DICHLOROBENZENE
*••FOOTNOTES*"* •A-AVERAGE VALUE •NA-NOT ANALYZED •NAI-INTERFERENCES •J-ESTIMATED VALUE •N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL •K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN •L-ACTUAL VALUE JS KNOWN TO BE GREATER THAN VALUE GIVEN •U-MATERJAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•
•
• •
State of North Carolina
Department of Environme11t, Health, and Natural Resources
512 North Salisbury Street • RBleigh, North Carolina 27604
James B. Hunt, Jr., Governor Division of Solid Waste Management
Telephone [phone]
Jonathan B. Howes, Secreta,y
February 19, 1993
Mr. David Schaer, Project Manager
Ebasco Environmental
145 Technology Park
Norcross, Georgia 30092-2979
RE: Comments on Final Engineering Report on Soil and Groundwater Testing at Two
Former Landfills at New Hanover International Airport, North Carolina
Dear Mr. Schaer:
The referenced Final Engineering Report for the New Hanover International Airport
has been received and reviewed by this office. The following comments are offered by the
North Carolina Superfund Section.
1.
2.
3.
Page 6, Section 1.4. Last Sentence
The basis for concluding that the groundwater flow direction was South towards
Smith Creek was not provided.
Page 10. Section 4.3. 2nd Paragraph
The first two sentences indicate that the 15 foot deep soil borings were sampled at
five foot intervals implying 4 samples were taken at 0, 5, 10, 15 foot depths. The last
sentence in the paragraph indicates however that the samples stop at the 10 foot
depth.
FIGURE 4.1
The SW-1 sample does not appear to be far enough upstream from the landfill site
to provide suitable background values.
4. FIGURE 4.2
r.O. Box 17687, Raleigh, Nunh GrolinJ 27611•76S7 Tdephunt· 919-733-4964 Fa:../ 919-733-0513
An Equ.i! Opportunity Afifrm~:ivi: . .\::ion Employc:r
Mr. David Schaer
February 19, 1993
Page 2 ·
• •
There appears to be only 1 sample (from MW-4) completely downgradient of Landfill # 2. Also, samples from MW-2 and MW-3 might see some contamination
migration but they appear to be in a less than optimum location. Also, the basis for not taking any surface water /sediment.samples in Smith Creek at the Landfill # 2 location should be indicated.
5. Page 16, Section 4.6, list of sample sets
Same comment on Set No. 1 as noted in comment number 3 above. Set No. 2 is indicated to be between the landfills in Smith Creek however Figure 4.1 shows sample Set No. 2 approx. 500 feet north of Smith Creek.
6. FIGURE 5.1/FIGURE 4.1
Both figures are supposed to indicate the same SB /MW locations for Landfill # 1 yet the figures show them in significantly different locations. Both figures are drawn to a particular scale therefore the SB/MW locations should be consistent.
7. FIGURE 5-1
SB-1 is shown to be -25 feet away (north) from the suspected boundary of landfill # 1. Since this location is intended to be the upgradient location and since the landfill boundary is approximate and to some degree uncertain, it would have been prudent to put more distance between the SB-1 and the landfill. This would have
provided more assurance that this location is clearly upgradient of the landfill site.
8. FIGURE 5.2/FIGURE 4.2
Same comment as noted in comment number 6 regarding graphical consistency for the SB/MW locations shown on the two figures.
9. Page 21. Section 5.1. 3rd Paragraph
Regarding Landfill # 2, it is not clear what is meant by the statement that the portion used during the 1960's " .. .is otherwise not related to Landfill # 2 ... ".
10. Page 21. Section 5.1, Last Paragraph
The location of SB-1 is upgradient of the 1940's portion of Landfill# 2 but appears to be downgradient of the newer segment of this landfill which could affect comparisons of upgradient versus downgradient sample data. Also, the locations of SB-2 and SB-3 may be less than optimum \vith regard to detecting contamination
migration from Landfill # 2.
11. ALL ANALYTICAL RESULTS TABLES
While one can eventually deduce what the various sample location names mean, it would help the reader to provide a clear explanation of the sample ID scheme to avoid misinterpreting the results. Also, it would be much clearer if separate data
• •
Mr. David Schaer
February 19, 1993
Page 3
12.
13.
14.
15.
16.
17.
18.
tables were used for each landfill.
TABLE 5-5, Page 31
The table shows elevated semi volatile soil analysis values (PAI-ls) for SD-1 which is
supposed to be the upstream or background sample. The explanation on page 33
concludes that since this location was labelled as background, this cannot be
attributed to site conditions. It would appear to be premature to make such a
conclusion without first conducting some past and present land use investigations and
further upstream sampling to conclude that this is in fact a valid background location.
TABLE 5-8, Page 36
The relatively higher inorganic soils analysis values for L2-SB1-5 appear to indicate
that maybe. this was a less than optimum background location due to its close
proximity to the newer portion of Landfill # 2. The potential influence of the 1960's
portion of the landfill is noted on page 40 however the L2-SB 1-5 sample is still used
as the background. Also, except for the Lead analysis for L2-SB3-2, the values for
the SB-2 and SB:3 location do not show any contamination which may be a function
of sample location as opposed to a lack of contamination in the landfill.
TABLE 5-8, Page 37
The NH-SDI sample is supposed to be the upstream background sample yet there
are elevated values for several of the metals analyses relative to the other sediment
samples. This could indicate that maybe this sample was not taken far enough
upstream.
TABLE 5-9, Page 38
The Ll-MWl sample is supposed to be the upgradient sample for Landfill # 1
however it has high values for As, Cr, Cu, and Pb. As was previously indicated,
maybe this location was too close to the landfill site to be a true upgradient location.
Also, the location of samples L2-MW2 and L2-MW3 may have a bearing on why they
do not show any contaminants.
Page 40, Section 5.7. Explosives Results
The background value used for the explosives results is not provided.
Page 41. Section 5.8
There is no discussion of the quantitative impact of the excessive holding times ( over
4 days) for the pesticides/PCBs analyses noted on page 33.
Page 43. Section 6.0
In view of the potentially questionable sampling locations previously noted it may be
premature to draw the conclusioqs and recommendations noted in this section. The
Mr. David Schaer
February 19, 1993
Page 4
• •
most notable is the blanket conclusion that there is no significant contamination at Landfill # 2.
The State of North Carolina appreciates the opportunity to comment on this Final Engineering Report for the subject site, and we look forward to working with you on this site.
Sincerely,
Patrick Watters
Environmental Engineer
Superfund Section
cc: Jack Butler, NC Superfund Section
Commander, U.S. Army District, Savannah, Ga.
File
'
• • UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
345 COURTLAND STREET. N.E.
ATLANTA. GEORGIA 30365
JUN 3 1992
4WD-NCRS
Mr. John Walch
North Carolina Department of Environment,
Health and Natural Resources
401 Oberlin Road
Raleigh, NC 27605
RE: Third Round Sampling Report for the
New Hanover County Airport Burn Pit Superfund Site
Dear Mr. Walch:
Enclosed for your information and file are three (3) copies of
the above referenced report. The samples were collected in
November 1991, however, this data was not incorporated into the
final New Hanover Remedial Investigation Report dated January
1992.
If you have any questions, please call me at [phone].
Sincerely yours, r '~ ~
Jon K. Bornholm
Remedial .Project Manager
enclosure
cc: Bill Meyer, NCDEHNR (w/o encl.)
ftECt\VED
JUN 08 1992
stJPERRfMD SECTfflft
.Printed on Recycled Paper
• • UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
345 COURTLAND STREET. N.E.
ATLANTA. GEORGIA 30365
OCT 2 9 19:}1
4WD-NCRS
Ms. Charlotte Jesneck
North Carolina Department of Environment,
Health and Natural Resources
401 Oberlin Road
Raleigh, NC 27605
RE: Third Round of Groundwater Sampling at the New Hanover county Airport
Burn Pit Superfund Site
Dear Ms. Jesneck:
A third round of groundwater level measurements and samples will be collected
at the above referenced site from on-site monitoring wells during the week of
November 18, 1991. This effort is to address several comments raised during
the review of the draft Remedial Investigation report. These groundwater
samples will b~ analyzed for volatile organics, semi-vo~atile organic.a and
metals. It is also the Agency's intention to sample s~ver~l nearby private,
potable wells located either laterally or downgradient of· the Site with
respect to the regional groundwater flow direction. The regional flow
direction is generally to the southeast. These samples will be analyzed for
the same range of constituents as the other groundwater samples. The .Agency
requested the he'ip of the New Hanover County in locating nearby private,
potable wells-in a correspondence dated October 18, 1991.
In addition to collecting samples from existing monitoring wells, the Agency
will also install a temporary well northwest of the burn pit at the boundary
of the site. If sufficient groundwater can be extracted from this well, then
the sample will be analyzed for the constituents listed above. If limited
groundwater is obtained from this well, then the sample·collected will only
be analyzed for volatile organics.
Along with collecting a groundwater sample northwest of the burn pit, an
additional surface soil sample will also be collected at this location to
augment the site perimeter data. It is anticipated that the data from this
soil sample will help confirm that surface contamination has not.extend
beyond Site boundary. '
Printed on Recycled Paper
•
-2-
' '.
'' Due to the local geology and hydrogeology, the Agency's Ground-Water ';
Technology Support Unit feels it is important to insure that the sandy'
aquifer underlying the five-foot clay layer has not been adversely impacted
by site activities. A blue-gray clay layer was e~countered in four different
locations across the site at an approximate depth of 28 feet. It is the
Agency's belief that this clay layer is continuous across the entire ·slte.
' Data collected during the remedial investigation field effort documents that
the shallow, sandy aquifer has been adversely impacted with elevated 1evels
of benzene. Because the levels of benzene detected at the site are above the
Preliminary Remediation Goal (PRG) of 1.0 micrograms/liter (ug/1) for
benzene, the Agency anticipates some type of groundwater remediation w\11 be
warranted at the Site. PRGs for the New Hanover County Airport Burn Pit
superfund site were established in January 1991 by the Agency. The Risk
Assessment will make the final determination if remediation of this shallow
aquifer ·is necessary.
If the shallow aquifer has not been impacted significantly enough to warrant
remediation, then it is the Agency's stance, based on site specific
geological and geophysical data, that the underlying sandy aquifer could not
have been impacted to a degree that would require remediation. If
remediation of the shallow aquifer is warranted, then a minimum of two
monitoring wells, doubled cased, will be installed into the deeper sandy
aquifer to insure that this underlying sandy aquifer has not been
detrimentally impacted. These additional monitoring wells, if required, are
necessary because the deeper sandy aquifer sits on top the Castle Hayne
limestone formation and therefore these two geologic formation are
hydraulically interactive. Consequently, if contamination reaches the
underlying sandy formation, this contamination would eventually affect the
Castle Hayne limestone formation. These wells will be installed as part of
the Remedial Design.
If you have any questions, please ca11· me at [phone].
Sincerely yours,
Remedial Project Manager
cc: Lee Crosby, NCDEHNR
William Meyer, NCDEHNR
',.
Date
ROUTING AND TRANS AL SLIP P.t/?o • TO: (Name, office symbol, room number, Initials Date
bulidlng; Agericy/Posl} '
1. 2.-C:Rt?SBY
2. "1-J,$'A/k:;.t'.:
'
3.
4. . '
5.
Action
Approval
As Requested
Circulate l<
Comment
Coordination
,,
.
File
For Clearance
F:nr r:orrection
-l"5i' Your lnformati~ -
11nvesugate
Justify
-~t{l;tU ~ IEO
SEP 11 1990
SUPERFUND SECTION
Not& and Retu m
Per Conversation
Prepare Reply
See Me
Slgr,atUre
DO NOT use this form as a RECORD of approvals, concurrences. disposals,
clearances, and similar actions
FROM: /Name, org. symbol, Ageilcy/Posl} ·
'
* U.S. GPO: 1990-254-313
Room No.-Bldg,
Phone No.
· ,,t'77'l/
OPTIONAL FORM 41 (Rev. 7-76)
P111e1ib•d b1 GSA .FPMR(41 CFR) 101-p.208
j'. S. ENVIRONMENTAL PROTECTION .CY
REGION IV, ATHENS, GEORGIA
MEMORANDUM
::..
DATE: AUG 24 1990
SUBJECT: New Hanover County Burn Pit
New Hanover County, Wilmington,
ESD Project No. 90-416
North Carolina
FROM: John D. Schoolfield
Hazardous Waste Section
Environmental Compliance Branch
Environmental Services Division
TO: James Kopotic, OSC
Site Control Section
THRU:
Superfund Emergency Response and Removal Branch
Waste Management Division
M. R. Carter, P.E., Acting Chief
Hazardous Waste Section
Environmental Compliance Branch
Environmental Services Division
7t/ ;f'
SEP
The Field Investigation Report for the New Hanover County Burn Pit site,
Wilmington, North Carolina is attached.
If you have any questions, please contact me at (FTS) 250-3317.
Attachment
cc: Finger/Wright
Carter/Bokey
__]S_nJg~t
ii~~andler }
/.
INTRODUCTION
•
SITE SAMPLING INVESTIGATION
NEW HANOVER BURN PIT
WILMINGTON, NORTH CAROLINA
ESD PROJECT No. 90-416
MAY, 1990
During the week of April 9, 1990, John Schoolfield, Environmental Services
Division (ESD), Hazardous Waste Section, and Jim Kopotic, Superfund Emergency
Response and Removal Branch (SERRB), collected surface water, sediment, and
sludge samples at the New Hanover County Burn Pit site, located near Wilmington,
North Carolina. This investigation was requested by the Waste Management
Division, SERRB, US-EPA, Region IV.
BACKGROUND
The site is located on Gardner Drive, west of the New Hanover County Airport,
Wilmington, North Carolina (see Figure 1). Although termed as a "pit" (i.e.,
a relatively deep hole in the ground) the burn pit does not extend below land
surface, and is of earthen-berm construction, roughly 2.5 feet above the ground.
The pit is located in the northeast center of a four•acre tract once used for
fire training exercises. The north side of the pit contains a valve which was
formerly used to drain water from the pit onto the ground.
SITE HISTORY
The New Hanover Burn Pit was constructed around 1968 and was used from approxi-
mately 1968 to 1979 by the Cape Fear Technical Institute for fire training
purposes. The institute burned jet fuel and gasoline in the pit. Water was used
to extinguish the fires. The Wilmington Fire Department also used the Burn Pit
from 1968 to 1976. The Fire Department burned jet fuel and drainage from
petroleum fuel tanks, and used water, CO2 , and dry chemicals to extinguish the
fires. Fuel oil, kerosene, and oil from oil spill cleanups were also reportedly
burned in the pit. The pit has not been used since 1979.
At· the time of this investigation, standing water was observed in the pit. An
air monitoring survey, taken with a photoionization detector (PID), conducted
. ar.o_und pit and within the pit, did not register a reading above background.
GEOLOGY AND SOILS
The New Hanover Burn Pit lies within the southeastern part of the Coastal Plain
of North Carolina, at an elevation of approximately 31 feet above NGVD. Local
soils are representative of Lower Coastal Plain soil conditions. Leon sands
comprise the main soil series at the Burn Pit site. This soil has a rapid
infiltration rate with moderate to high hydraulic conductivity, estimated to
'• - 2 -•
be greater than 10-3 cm/sec. The hydraulic conductivity of the subsoil, however,
is dependent on the degree of development of the organic hardpan that is commonly
present. There are two sources of ground water in the area of the site. One
source is the upper surficial groundwater, which is approximately five feet below
land surface. The other source of water is from the sandstone aquifer in the
PeeDee formation. This aquifer is approximately 50 to 80 feet below land surface
in the area of the site. There is no continuous confining layer between the
sandstone aquifer and the upper surficial groundwater.
ANALYTICAL RESULTS
A surface water sample (SW-01) was collected from apparent rain water that had
accumulated in the pit, and a sediment sample (SD-01) was collected from the bot-
tom of the burn pit. A tank sludge sample (TS-01) was collected from "bottoms"
residue that remained in an above ground storage tank located on the east side
of the property. Sample locations are shown in Figure 2. The data are sum-
marized in Table 1 and Table 2. The complete data are attached as Appendix A.
The pit surface water sample was analyzed for volatile and extractable organic
constituents, PCBs, pesticides, metals, BOD5 and COD. The pit sediment sample
and tank sludge sample were analyzed for volatile and extractable organic
constit~ents 1 PCBs, pesticides, metals, and the toxicity characteristic leaching
procedure (TCLP) constituents. The samples were collected and handled in
accordance with the Engineering Support Branch Standard Operating Procedures
and Quality Assurance Manual (April 1986). Samples were analyzed according to
the Analytical Support Branch Operations and Quality Control Manual (June 1985).
Alphabetic letters attached to the right of some of the reported analytical data
values are .data qualifiers indicating the following:
J ESTIMATED VALUE
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
A AVERAGE VALUE
U MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER
IS THE MINIMUM QUANTITATION LIMIT
In the following discussion, "NPDWRs MCL listed metals" refers to those metals
which have drinking water "Maximum Contaminant Levels (MCL)" standards listed
in the National Primary Drinking Water Regulations (NPDWRs).1
TARGET ANALYTE LIST RESULTS
Sample SW-01: The surface water sample collected from the pit had a BOD 5 of 17
mg/1 and a COD of 510 mg/1. Three NPDWRs MCL listed metals were detected i.e.,
arsenic (44 ug/1), barium (260 ug/1), and lead (180 ug/1). The lead value
exceeded the NPDWRs MCL standard of 50 ug/1. Two extractable organic compounds
were detected; hexadecanoic acid, methyl ester· (lOOJN ug/1), and
methylheptadecanoic acid, methyl ester (50JN ug/1). One purgeable organic
compound was detected at a trace concentration (0.66J ug/1 trichloroethylene).
No pesticides or PCBs were detected in the sample.
1 40 CFR, P.srt 16.l, National Primar:: Drinking Water Regulations,
- 3 -•
Sample SD-01: The sediment sample collected from the burn pit contained six
NPDWRs MCL listed metals ranging in concentrations from 0.10 mg/kg of mercury
to 540 mg/kg of lead. No extractable organic constituents were detected (at
minimum detection limits of 100,000 ug/kg). Five purgeable organic compounds
were detected ranging in concentrations from 45, OOOJ ug/kg ethyl benzene to
900,000JN ug/kg trimethylbenzene. No pesticide or PCB compounds were detected.
Sample TS-01: The tank sample contained six NPDWRs MCL metals ranging in
concentrations from O .10 mg/kg of mercury to 860 mg/kg of· lead. Fifteen
extractable organic constituents were detected in the sample ranging in
concentrations from 300,000JN ug/kg of (dimethypropyl)benzene to 20,000,000JN
ug/kg of dimethylnaphthalene. Five purgeable organic compounds were detected
ranging in concentrations from 26, OOOJ ug/kg o-xylene to 300, OOOJN ug/kg
trimethylbenzene. No pesticide or PCB compounds were detected.
TCLP RESULTS
SD-01 METALS ANALYSIS: The TCLP metals analysis of sediment sample SD-01
detected three NPDWRs MCL listed metals in the extract i.e., arsenic (21 ug/1),
barium (1,800 ug/1), and lead (20 ug/1).
SD-01 EXCTRACTABLE ORGANICS ANALYSIS: During the TCLP extractable organics
analysis procedure, sample SD-01 was found to separate into a solid phase and
a liquid phase, each of which were analyzed separately. The solid phase TCLP
extract contained 20 extractable organic constituents ranging in concentrations
from 4J ug/1 of fluorene and phenanathrene to 200JN ug/1 of atrazine. The liquid
phase TCLP organics analysis detected no extractable organic compounds.
SD-01 PURGEABLE ORGANICS ANALYSIS: During the purgeable organics TCLP analysis
of the sediment sample SD-01, a solid phase and a liquid phase were encountered
and both analyzed. The solid phase TCLP purgeable organics analysis detected
nine purgeable organic compounds ranging in concentrations from 59 ug/1 ethyl
benzene to 900 ug/1 acetone. The liquid phase analysis detected ten purgeable
organic compounds ranging in concentrations from 7JN ug/1 diethylmethylbenzene
to 300JN ug/1 dimethylundecane.
SD-01 PESTICIDES/PCBs ANALYSIS: No pesticide or PCB compounds were detected in
the TCLP analysis of sample SD-01.
TS-01 METALS ANALYSIS: During the TCLP metals analysis of sample TS-01, an
aqueous phase and an oily phase were analyzed. The aqueous phase analysis
detected three NPDWRs MCL listed metals i.e., barium (1900 ug/1), arsenic (32
ug/1), and lead (950 ug/1). The oily phase contained two NPDWRs MCL listed
_me_t~ls i.e., lead (5.6J mg/kg2) and barium (14J mg/kg).
TS-01 EXTRACTABLE ORGANICS ANALYSIS: During the TCLP extractable organics
analysis, three phases were encountered, a solid phase, an aqueous phase, and
an oily phase. The TCLP analysis of the solid phase identified 11 extractable
organic compounds ranging in concentrations from 28 ug/1 of pyrene to 2,000JN
ug/1 of methylcyclohexanamine in addition to 16 unidentified compounds. The TCLP
analysis of the aqueous phase detected nine extractable organic compounds ranging
- 4 -•
in concentrations from 230J ug/1 of chrysene to 25,000 ug/1 of 2-metyl-
naphthalene in addition to 19 unidentified compounds. The TCLP analysis of the
oily phase identified eight extractable organic compounds ranging in
concentrations from 140, OOOJ ug/1 pyrene to 30,000, OOOJN ug/1 dime thylnaphthalene
in addition to· 18 unidentified compounds.
TS-01 PURGEABLE ORGANICS ANALYSIS: For the TCLP purgeable organics analysis,
a solid phase and a liquid phase were analyzed. Nine purgeable organic compounds
were detected in the solid phase ranging in concentrations from 17J ug/1 benzene
to 3000JN ug/1 dimethylundecane in addition to four unidentified compounds. The
liquid phase contained eight purgeable organic compounds ranging in
concentrations from 35,000 ug/1 ethyl benzene to 400,000JN ug/1 trimethylbenzene
in addition to ·s unidentified compounds.
TS-01 PESTICIDES/PCBs ANALYSIS: No pesticide or PCB compounds were detected in
the TCLP analysis of sample TS-01.
11EPA
NEW HANOVER
Sil£
l
FIGURE 1
GENERAL LOCATION MAP
NEW HANOVER BURN PIT
WILMINGTON, NORTH CAROLINA
APRIL, 1990
PIPELINE
BERM / ROAD
·iiEPA
'-
Qw_:, '-
APPROXIMATE
/ SITE BOUNDARY
BURN SD-01
APPROXIMATE SCALE
150 o 75 k-~ --,
( IN FEET )
1 Inch = 150 ft.
PIT
SUPPLY~
TANK /
TS-01
150
'
FIGURE 2
SAMPLE LOCATION MAP
NEW HANOVER BURN PIT
WILMINGTON, NORTH CAROLINA
APRIL, 1990
.,
•<'··~?!~
PAGE ,,
• TABLE 1 •
TARGET ANALYTE LIST ANALYTICAL DATA SUMMARY
NEW HANOVER BURN PIT
NPOWRs MCL HETALS1
ARSENIC
BARIUM
CADMIUM
CHROMIUM
LEAD
-MERCURY
SELENIUM
SILVER
INORGANIC ELEMENTS
COBALT
COPPER
MOLYBDENUM
NICKEL
TIN
STRONT !UH
TITANIUM
VANADIUM
ZINC
ALUMINUM
MANGANESE
CALCIUM
MAGNESIUM
IRON
SODIUM
GENERAL ORGANIC PARAMETERS
BIO-CHEMICAL OXYGEN OEMAN0,5 DAY
CHEMICAL OXYGEN DEMAND
***FOOTNOTES***
WILMINGTION, NC
APRIL 10, 1990
SW-01
BURN PIT
WATER
04/10/90
1230
UG/L
44
260
180
UG/L
36
20
190
550
MG/L
8.7
1.8
35
26
MG/L
17
510
SD-01
BURN PIT
SEDIMENT
04/10/90
1320
MG/KG
6.8
520
3.2
25
540
0.10
MG/KG
3.0
120
8.6
11
9.2
33
33
18
310
1500
170
MG/KG
5400
420
12000
110
MG/L
NA
NA
1 -40 CFR, Part 141, National Primary Drinking Water Regulations,
Maxinun Contaminant Levels, (July 1, 1989).
NA NOT ANALYZED
J ESTIMATED VALUE
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
TS-01
TANK
SLUDGE
04/10/90
1420
MG/KG
3.3
450
0.54
8.5
860
0. 10
MG/KG
1.2
17
1.4
3.8
2.9
7.8
14
12
180
180
53
MG/KG
800
130
3400
940
MG/L
NA
NA
PAGE 2 • • TABLE 1
TARGET ANALYTE LIST ANALYTICAL DATA SUMMARY
NEW HANOVER BURN PIT
~ILMINGTION, NC
EXTRACTABLE ORGANIC COMPOUNDS
2-METHYLNAPHTHALENE
NAPHTHALENE
FLUORENE
PHENANTHRENE
Hexadecanoic acid, methyl ester
Methylheptadecanoic acid,methyl ester
(Dimethylpropyl)benzene
.1-Methylnaphthalene
Ethenylnaphthalene
Dimethylnaphthalene(S-isomers)
Trimethylnaphthalene(6·isomers)
Propenylnaphthalene
Methylphenanthrene(4-isomers)
Dimethylphenanthrene(4·isomers)
Trimethylphenanthrene
Petroleum product
2-Unidentified Compounds
PURGEABLE· ORGANIC COMPOUNDS
TRICHLOROETHENE(TRICHLOROETHYLENE)
TOLUENE
ETHYL BENZENE
(M-AND/OR P-)XYLENE
O-XYLENE
TRIMETHYLBENZENE (3 ISOMERS)
ETHYLMETHYLBENZENE
TRIMETHYLBENZENE
PETROLEUM PROOUCT
***FOOTNOTES***
NA NOT ANALYZED
J ESTIMATED VALUE
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
APRIL 10, 1990
SW·D1
BURN PIT
I/ATER
04/10/90
1230
UG/L
100JN
SOJN
N
UG/L
.66J
so-01
BURN PIT
SEDIMENT
04/10/90
1320
UG/KG
UG/KG
45000J
47000J
900000JN
100000JN
N
TS-01
TANK
SLUOGE
04/10/90
1420
UG/KG
4.2E6
680000J
340000J
700000J
300000JN
3E6JN
1E6JN
20E6JN
1 OE6JN
2E6JN
3E6JN
3E6JN
200000JN
N
4E6J
UG/KG
100000J
60000J
26000J
300000JN
N
PAGE j • • TABLE 2
TCLP DATA SIJl4MARY
NEW HANOVER BURN PIT
WILMINGTON, NC
APRIL 10, 1990
SD-01 TS-01 TS-01
BURN TANK TANK
PIT SLUDGE SLUDGE
SEDIHEKT AQIJEOOS OILY
SAMPLE PHASE PHASE
04/10/90 04/10/90 04/10/90
1320 1420 1420
INORGANIC ELEMENTS UG/L UG/L MG/KG1
ARSENIC 21 32
BARIUM 1800 1900 14J
COBALT 24 18
NICKEL 41 37 2.5
LEAD 20 950 5.6J
VANADIUM 8 25 7.6
ZINC 500J 850J
ALUMINUM 340 400
MANGANESE 1600 210
CALCIUM 210000 19000 62J
MAGNESIUM 5300 4800 23
IRON 94000J 12000J
SOOIUM2 1400000 1500000
POTASSIUM 4000
***FOOTNOTES***
1 _ • THE RESULTS FOR THIS SAMPLE WERE REPORTED IN MG/KG BECAUSE THE DENSITY OF THE MATERIAL WAS NOT SIMILAR TO WATER.
2 SOOIUM VALUES FOR THE EXTRACTS ARE LIKELY BIASED HIGH DUE TO THE SOOIUM CONTRIBUTION FROM THE EXTRACTION FLUID.
NA NOT ANALYZED
J ESTIMATED VALUE
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
-·
\
,: .I
PAGE 2 )'. TABLE 2
TCLP DATA SUM11ARY
NEW HANOVER BURN PIT
WILMINGTON, NC
APRIL 10, 1990
... c:_ SD-01 SD-01
PIT PIT
SEDIMENT SEDIMENT
SOLID LIQUID
PHASE PHASE
04/10/90 04/10/90
1320 1320
EXTRACTABLE ORGANIC COMPOUNDS UG/L UG/L
2-METHYLNAPHTHALENE 67
NAPHTHALENE 64
ACENAPHTHENE
FLUORENE 4J
PHENANTHRENE 4J
PYRENE
CHRYSENE
2-METHYLPHENOL
DIMETHYLCYCLOHEXANAMINE 100JN
ETHYLDIMETHYLPYRIDINE 30JN
CYCLOHEXANEMETHANOL 20JN
TRIMETHYLPHENOL 20JN
OIBUTYLACETAMIOE 20JN
TRIMETHYLPHENYLETHANONE (2 ISOMERS) 90JN
DIMETHYLBENZENEDICARBOXALDEHYDE 20JN
ATRAZINE 200JN
1-METHYLNAPHTHALENE 70JN
DIMETHYLNAPHTHALENE 40JN
TRIMETHYLNAPHTHALENE
METHYLCYCLOHEXANAMINE 60JN
PETROLEUM PRODUCT
OIMETHYLNAPHTHALENE (2 ISOMERS)
16 UNIDENTIFIED COMPOUNDS
'19 UNIDENTIFIED COMPOUNDS
18 UNIDENTIFIED COMPOUNDS
5 UNIDENTIFIED COMPOUNDS 100J
••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••
***F09TNOTES•**
NA NOT ANALYZED
J ESTIMATED VALUE
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
•
TS-01 TS-01 TS-01
TANK TANK TAN~
SLUDGE SLUDGE SLUDGE
SOL!O AQUEOUS OILY
PNASE PHASE PHASE
04/10/90 04/10/90 04/10/90
1420 1420 1420
UG/L UG/L UG/L
1400 25000 6500000
330 4500 1100000
1100 350000JN
170 700000
270 5900 2300000
28 580 140000J
230J
110 570
1000JN
1 OOOJN
1000JN
2000JN 8000JN
N N N
3E+07JN
30000J
300000J
3E+08J
• ..
PAGE 3 ,f
·--~ .
PURGEABLE ORGANIC COMPOUNDS
ACETONE
METHYL ETHYL KETONE
BENZENE
2-CHLOROETHYLVINYL ETHER
TOLUENE
ETHYL BENZENE
TOTAL XYLENES
ETHYLOIMETHYLBENZENE (2 ISOMERS)
BUTANOIC ACID, HETHYLETHYLESTER
HETHOXYHETHYLPROPANE
TETRAMETHYLBENZENE (2 ISOMERS)
OIHETHYLUNDECANE (2 ISOMERS) ETHYLOIMETHYLBENZENE
TETRAMETHYLBENZENE
OJETHYLMETHYLBENZENE
D IMETHYLUNDECANE
METHYLOOCECANE
DIHYDROMETHYLINDENE
DIETHYLBENZENE
METHYLOCTANE (2 ISOMERS)
TRIMETHYLBENZENE
METHYLNONANE
ETHYLMETHYLBENZENE
4 UNIDENTIFIED COMPOUND ·s UNIDENTIFIED COMPOUNDS
•**FOOTNOTES***
NA NOT ANALYZED
ESTIMATED VALUE
•
N PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL MATERIAL WAS ANALYZED FOR BUT NOT DETECTED
• TABLE 2
TCLP DATA SUMMARY
NEW HANOVER BURN PIT
WILMINGTON, NC
APRIL 10, 1990
SD-01 SD-01 TS-01 TS-01 TCLP TCLP TCLP TCLP SOLIDS LIQUID SOLIDS LIQU!O
PHASE PHASE PHASE PHASE 04/10/90 04/10/90 04/10/90 04/10/90 1320 1320 1420 1420
UG/L UG/L UG/L UG/L
900 830J
SOUR SOUR 130000J 67 17J 17J
NA NA NA NA
150J 160000
59 23J 35000 72 250000
200JN
200JN
20JN
60JN
300JN
90JN
100JN SOOJN
7JN 100JN
3000JN
1000JN
200JN 100JN 400JN
1000JN
100000JN
200JN 80JN 400000JN
80000JN
20,!N 100000JN
1000J
1000000J
U MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT R QUALITY CONTROL INDICATES-THAT DATA ARE UNUSEABLE, COMPOUND HAY OR HAY NOT BE PRESENT RESAMPLING AND REANALYs1s·1s NECESSARY FOR VERIFICATION, THE VALUE IS THAT REPORTED BY THE LABORATORY