NCD980840409_20051230_Charles Macon Lagoon Drum_FRBCERCLA RA_Quarterly Progress and O & M Report August - October 2005-OCR

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Macon/Dockery Site
Richmond County, North Carolina 1 , ~ ,-
~ · Rep1Y, to: Technical Committee
... ; ~ti "' \ c/o Ken Gulledge j( -, '), '!, l\\ Crown, Cork & Seal Company, Inc.
·-. \ I ')[,_~ . P.O. Box 887 ~ . ,.. •. Cheraw, SC 29520
· ~ , . ' Phone: [phone]
December 30, 2005
Ms. Giezelle S. Bennett
Remedial Project Manager
1 United States Environmental Protection Agency, Region IV
61 Forsyth Street, S.W.
Atlanta, Georgia 30303-3104
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Fax: [phone]
Re: Progress and O&M Report of Quarterly Activities -August 1, 2005 through October 31,
2005 I
' Macon/Dockery Site -Cordova, North Carolina
I IC Project Number 0004-001 1
Dear Ms. Bennett:
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On behalf of the Macon/Dockery Site Group (MDSG), the Progress and O&M Report of
Quarterly Activities for August I, 2005 through October 31, 2005 is herewith submitted in
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accordance with SECTION XV -PROGRESS REPORTS of the Unilateral Administrative Order
(effective date -June 30, 1992) for the Macon/Dockery Site. Additionally, the report includes the
provisions included in the recommendations section of the United States Environmental Protection
I Agency (USEPA) -Region IV Five Year Review ,Report dated September 2000. This report
describes activities, which occurred during the period August 1, 2005 through October 31, 2005 as
part of the Remedial Action phase of this project. Specifically, this report describes the operational
status of the groundwater remediation systems and: the results of the quarterly system cffiuent
sampling event conducted for the period.
PROJECT TASKS INITIATED OR COMPLETED THROUGH OCTOBER 31, 2005:
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• Weekly operation and maintenance of the systems; and,
• Quarterly effluent sampling of the remediation systems.
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RESULTS OF SAMPLING AND TESTING AND OTHER DAT A RECEIVED:
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Tables 1 through 4 summarize the effluerit analytical results for three operational
groundwater treatment systems, Upper Dockery, Uppe~ Macon Source Area, and the Upper/Lower
Macon remediation systems, and one suspended remediation system, Lower Dockery. No
' exceedances were observed during the reporting period. Air samples were collected from the
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Ms. Giczcllc Bennett
December 30, 2005
Page No. 2
exhaust stacks of the remediation systems and fro~ the eastern property line. The results of the air
sample analyses are summarized on Table 5. Mass removal estimates were calculated based on total
volatile influent concentration and the total flow re~orded for the period at each remediation system.
A summary of the mass removal estimate is provided on Table 6.
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The following table summarizes the remedial systems performance for the period August 1,
I 2005 through October 31, 2005: 1
Remediation Total Gallons Average Flow
System Removed For Rate For
Location Period Period
Upper/Lower 1,990,745 15.02 GPM,
Macon Gallons
Lower 0 Gallons 0GPM
Dockery
Upper 493,146 Gallons' 3.72 GPM •
Dockery
Upper Macon 451,29 I Gallons . 3.41 GPM .
Source Area
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,1 MassVOC
Removal For
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'10.79 pounds'
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10.0 pounds
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0.41 pounds •
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0.40 pounds,
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Total voe Percent
Removal Since Operational
Start-Up For Period
16.3 I pounds • 79%/76%
12.98 pounds· System
Suspended*
29.0 I pounds · 87%
51.19 pounds · 61 %
GPM -Gallons per mmute 1 VOC -Volatile Orgamc Compounds
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TASKS PLANNED FOR PERIOD NOVEMBER 11. 2005 THROUGH JANUARY 31. 2006
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• Weekly O&M of systems; :
• Quarterly sampling of groundwater remediation system effluent in January 2006;
• Quarterly sampling of remediation system off gas stacks and at the property line in January 2006;
• Semi-annual sampling of the designated monitoring wells in January 2006;
• Semi-annual sampling of the groundwater remedi1tion system influent in January 2006; and,
• Gauging of water levels in January 2006.
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I OPERATIONAL DIFFICULTIES AND DELAYS:
' • July 23, 2005 -August 12, 2005 -The Upper Dockery, Upper Macon Source Area, and Upper
and Lower Macon systems were down because ',of power outages resulting from damage \ 1---
sustained by lightning. On August 12, 2005, the power was restored and all the systems
restarted. '
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• August 13, 2005 -August 20, 2005 -The Upper Macon Source Area was down due to a tripped 1
circuit breaker. The breaker was reset and the system restarted on August 20, 2005. '
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Ms. Giezellc Bennett
December 30, 2005
Page No. 3
• September 7, 2005 -September I 0, 2005-The Lower Macon remediation system was down due
to a broken shear element on the recirculation pump. The shear element was replaced and the Z,,..
system restarted on September 10, 2005. 1
• October I, 2005 -October 18, 2005 -The Upper Macon Source Area and Upper and Lower
Macon groundwater remediation systems wereidown because of the loss of three phase power I 7
supply. On October 18, 2005, Pee Dee Electric restored 3-phase power and the systems were I
restarted. I
The MDSG appreciates the USEPA's cooperation with this project. If you have any
questions or comments, please feel free to contact ti~ at [phone].
Sincerely,
IRMINGER CONSULTING, INC.
Steven E. lrminger, P .E.
Project Manager
cc: Macon/Dockery Site Group Members
Mike Profit, COM Federal Programs
David Mattison, NC Superfund Section
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I, 1-Dichloro-1,1-Dichloro-Cis/trans-I ,2-
Sample Date ethane ethene Dichloroethene
Location (u.tl ) (ug/L) (u"'1)
UD Effiuent 5/3/1996 <1.0 <1.0 <1.0
6/5/1996 <1.0 <1.0 <1.0
7/1/1996 <1.0 <1,0 <1.0
8/1/1996 <1.0 <1.0 <1.0
9/4/1996 <1.0 <1.0 <1.0
10/1/1996 <1.0 <1.0 <1.0
11/7/1996 <1.0 <1.0 <1.0
12/5/1996 <1.0 1.5 <1.0
1/6/1997 <1.0 <1.0 <1.0
2/5/1997 <1.0 <1.0 <1.0
3/12/1997 <1.0 <1.0 <1.0
4/8/1997 <1.0 <1.0 <1.0
5/14/1997 <1.0 <1.0 <1.0
6/6/1997 <1.0 <1.0 <1.0
7/2/1997 <1.0 <1.0 <1.0
8/7/1997 <1.0 <1.0 <1.0
9/5/1997 <1.0 <1.0 <1.0
l0/2/1997 <l.O <1.0 <1.0
11/13/1997 <1.0 <1.0 <1.0
12/5/1997 <1.0 <1.0 <1.0
1/9/1998 <1.0 <1.0 ~-D_ ---------2/5/1998 --·<1.0· --<ro <1.0
3/5/1998 <1.0 <1.0 <1.0
4/3/1998 <1.0 <1.0 <1.0
5/7/1998 <1.0 <1.0 <1.0
6/5/1998 <1.0 25 <1.0
7/9/1998 <1.0 <1.0 <1.0
8/7/1998 <1.0 <1.0 <1.0
9/10/1998 <1.0 <1.0 <1.0
]0/2/1998 <1.0 <1.0 <1.0
11/4/1998 <1.0 <1.0 <1.0
12/1/1998 <1.0 <1.0 <1.0
1/11/1999 <1.0 <1.0 <1.0
2/11/1999 <1.0 <1.0 <1.0
3/5/1999 <1.0 <1.0 <1.0
4/8/1999 <1.0 <1.0 <1.0
5/12/1999 <LO <1.0 <1.0
6/10/1999 <1.0 <1.0 <1.0
7/8/1999 <1.0 <1.0 <1.0
8/5/1999 <1.0 <1.0 <1.0
9/9/1999 <1.0 <1.0 <1.0
I0/14/1999 <1.0 <1.0 <1.0
11/3/1999 <1.0 <1.0 <1.0
12/3/1999 <1.0 <1.0 <1.0
RPS 3500 7 70
RPS: Remediation Perfonnance Standard
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Tetra-
-l!l!!!I !!Ill
TABLE 1 (Page 1 of 2)
EFFLUENT Analytical Results
UPPER DOCKERY
Macon Dockery Site
Richmond County, North Carolina
1, I, 1-Trichloro-. Trichloro-
liiii liiiliil iiiil
chlorocthene ethane ethlene Toluene Total Xylenes Acetone Chromium Barium
(ug/L) (ug/L) (u""-) (ug/L) (ug/L) (u.tl) (u•n) (ug/L)
<1.0 <1.0 <1.0 <1.0 <3.0 52 <10 <50
<1.0 <1.0 <1.0 3.9 <3.0 <IO <IO <50
<1.0 <LO <1.0 <1.0 <3.0 <IO <10 <50
<1.0 <1.0 <1.0 <1.0 <3.0 20 14 51
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <IO 55
<1.0 <LO <LO <1.0 <3.0 <10 <10 <50
<LO <1.0 <1.0 <1.0 <3.0 <IO 15 59
<1.0 <1.0 <1.0 <1.0 <3.0 <IO 12 54
<1.0 <1.0 <1.0 <1.0 <3.0 <10 13 54
<1.0 <1.0 <1.0 <1.0 <3.0 <IO 15 61
<1.0 <1.0 <1.0 <1.0 <3.0 <10 <10 69
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <IO 63
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <10 60
<1.0 <1.0 <1.0 <1.0 <3.0 <10 <IO 52
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <IO 55
<1.0 <1.0 <1.0 <l.O <3.0 <10 <IO <50
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <IO I 10
<1.0 <1.0 <1.0 <1.0 <3.0 <10 <JO 50.1
<1.0 <1.0 <1.0 <1.0 <3.0 <IO 12.1 67 9
<1.0 <LO <1.0 <1.0 <3.0 ":.!0_ _:-:::IO_ -_<50-:--------~1.0_ --"""<LO ---<1.0-"""'. -<1:0--= <3.0 <IO II <50
<LO <1.0 <1.0 <1.0 <3.0 <IO <IO <50
<1.0 <1.0 <1.0 <1.0 <3.0 <10 <JO <200
<1.0 <1.0 <1.0 <1.0 <3.0 <IO <10 <200
<1.0 <LO <1.0 <1.0 <3.0 <IO 10 <50
<1.0 5.5 <1.0 <1.0 <3.0 <10 <10 57
<1.0 <1.0 <1.0 <1.0 <3.0 <10 <IO 51
<1.0 <1.0 <1.0 <1.0 <3.0 <10 13 53
<1.0 <1.0 <1.0 <1.0 <3.0 <IO II 58
<1.0 <1.0 <1.0 <1.0 <3.0 <25 <IO 54
<1.0 <1.0 <1.0 <1.0 <3.0 <10 II 63
<1.0 <1.0 <1.0 <1.0 <3.0 <25 14 63
<1.0 <1.0 <1.0 <1.0 <3.0 <10 II 55
<1.0 <1.0 <i.O <1.0 <3.0 <IO 15 73
<1.0 <1.0 <1.0 <1.0 <3.0 <25 II 62
<1.0 <1.0 <1.0 <LO <3.0 <10 II 54
<1.0 <1.0 <1.0 <1.0 <3.0 <IO 12 57
<l.0 <1.0 <1.0 <1.0 <3.0 <JO 13 66
<l.O <1.0 <1.0 <1.0 <3.0 <10 10 64
<1.0 <LO <LO <1.0 <3.0 <IO 14 66
<l.O <1.0 <1.0 <1.0 <3.0 <LO 14 61
<1.0 <1.0 <1.0 <1.0 <3.0 <IO 14 60
<1.0 <1.0 <1.0 <1.0 <3.0 <10 13 58
<LO <LO <1.0 <1.0 <3.0 <10 13 64
200 2.8 1000 400 3500 50 1000
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Suspended
Manganese Zinc Lead Solids
(u,n.) (ug/L) (ug/L) (mg/L)
<5.0 <20 <3.0 <5,0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
7 <20 <3.0 8
<5.0 <20 <3.0 <5.0
5.9 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
5.1 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
5.9 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
7.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
5.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
18.6 24.8 <3.0 <5.0
<5.0--..... <20--<3.o-:--<5:o -· -
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<15 <20 <3.0 <5.0
5.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<10 <20 <3.0 <5.0
6.3 <20 <3.0 12
40 <20 <3.0 <5.0
<5.0 <20 <3.0 <5,0
23 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 5.2 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
50 5000 15
-l!!!l!!!I l!!!!!!!I l!!!!l!I
I, 1-Dichloro-1, 1-Dichloro-Cis/trans-1,2-Tetra-
Sample Date ethane ethene Dichloroethene chloroethene
Location (u,/L) (uon) (uon) (u,/L)
UD Effiuent 3/9/2000 <1.0 2.1 <1.0 <1.0
4/7/2000 <1.0 <1.0 <1.0 <1.0
5/9/2000 <1.0 <1.0 <1.0 <1.0
6/9/2000 <1.0 <1.0 <1.0 <1.0
7/7/2000 <1.0 <1.0 <1.0 <1.0
813/2000 <1.0 <1.0 <1.0 <1.0
9/25/2000 <1.0 <1.0 <1.0 <1.0
I 0/12/2000 <1.0 <1.0 <1.0 <1.0
1/18/2001 <1.0 <1.0 <1.0 <1.0
5/3/200 I <1.0 <1.0 <1.0 <1.0
7/11/2001 <1.0 <1.0 <1.0 <1.0
10/18/2001 <1.0 <1.0 <1.0 <1.0
1/16/2002 <1.0 <LO <1.0 <1.0
7/31/2002 <1.0 <1.0 <1.0 <1.0
10/30/2002 <1.0 <1.0 <1.0 <1.0
1/28/2003 NOT SAMPLED SYSTEM
3/14/2003 NOT SAMPLED SYSTEM
4/3/2003 <1.0 <1.0 <1.0 <1.0
7/10/2003 <1.0 <1.0 <1.0 <1.0
_ 10/3!)/2003_ ~<\.O _ -<1.0 --<1.0-~ -<1.0_-----' 1/13/2004 <1.0 <1.0 <2.0 <1.0
4/5/2004 <1.0 <1.0 <2.0 <1.0
6/28/2004 <1.0 <1.0 <2.0 <1.0
10/21/2004 <1.0 <1.0 <2.0 <1.0
1/27/2005 <1.0 <1.0 <2.0 <1.0
5/4/2005 <LO <1.0 <1.0 <1.0
8/25/2005 <1.0 <1.0 <1.0 <1.0
I 0/30/2005 • <1.0 <1.0 <1.0 <1.0
RPS 3500 7 70
RPS: Remediation Performance Standard
liiiiiill liiiil lliiil iiiil
TABLE 1 (Page 2 of 2)
EFFLUENT Analytical Results
UPPER DOCKERY
Macon Dockery Site
Richmond County, North Carolina
I, I, 1-Trichloro-Trichloro-
liiiill iilll -
ethane ethlene Toluene Total Xylenes Acetone Chromium Barium
(ug/L) (ug/L) (u,/L) (u,JL) (ug/L) (ug/L) (u,/L)
<1.0 <1.0 <1.0 <3.0 <10 14 74
<1.0 <1.0 <1.0 <3.0 <10 <10 160
<1.0 <1.0 <1.0 <3.0 <10 14 69
<1.0 <1.0 <1.0 <3.0 <10 <10 79
<1.0 <1.0 <1,0 <3.0 <10 <10 95
<1.0 <1.0 <1.0 <3.0 <10 <10 78
<1.0 <1.0 <1.0 <3.0 <10 <10 85
<1.0 <1.0 <LO <3.0 <10 <10 84
<1.0 <1.0 <1.0 <3.0 <10 <10 100
<1.0 <1.0 <1.0 <3.0 <10 14 80
<1.0 <1.0 <1.0 <3.0 <10 27 79
<1.0 <1.0 <1.0 <3.0 <10 14 74
<1.0 <1.0 <1.0 <3.0 <10 18 130
<1.0 <1.0 <1.0 <3.0 <IO <10 55
<1.0 <1.0 <1.0 <3.0 <10 <10 99
DOWN NOT SAMPLED
DOWN NOT SAMPLED
<1.0 <1.0 <1.0 <3.0 <10 <10 83
<1.0 <1.0 <1.0 <3.0 <10 -:10 --% ---C ----·<J.O --<co---<CO-<3~0 <10 <10 55
<1.0 <1.0 <1.0 <2.0 <25 II 71
<1.0 <1.0 <1.0 <2.0 <25 12 68
<1.0 <1.0 <1.0 <20 <25 <10 54
<1.0 <1.0 <1.0 <2.0 <25 <10 85
<1.0 <1.0 <1.0 <3.0 <10 <10 72
<1.0 <1.0 <1.0 <3.0 <10 NA 62
<1.0 <1.0 <1.0 <3.0 <10 10 69
<1.0 <1.0 <1.0 <3.0 <10 14, 75 ·
200 2.8 1000 400 3500 50 1000
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Suspended
Manganese Zinc Lead Solids
(ug/L) (u,JL) (ug/L) (mg/L)
9.3 <20 <3.0 <5.0
8.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
10 <20 <3.0 <5.0
<5.0 <20 <3_0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
6.3 <20 <3.0 <5.0
5.7 <20 <3.0 <5.0
43.0 27 <3.0 8.0
5.4 <20 <3.0 <5.0
120 35 5 <5.0
5.6 <20 <3.0 <5.0
7.3 <20 <3.0 <5.0
SYSTEM DOWN
SYSTEM DOWN
5.1 <20 <3.0 <5.0
-19_ -<20 --<3.0 -<5.0 -
<5.0 <20 <3.0 <5.0
15 24 <3.0 14.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
NA <20 <1.5 <5.0
<5.0 <20 NA <5.0
<5.0 • <20. <1.5 , <5.0
50 5000 15
l!!!!!!!I l!!!.!!I 11!!1
Chloro-I, 1-Dichloro-I, 1-Dichloro-Cis/trans-1.2-
Sample Date form ethane ethene Dichloroethene
Location (ue/1 l (uon ) (uon ) (ue/L)
LD Effluent 2/15/1996 <l.0 <1.0 <1.0 <1.0
211611996 <1.0 <1.0 <1.0 <1.0
212211996 <1.0 <1.0 <1.0 <1.0
2/28/1996 <LO <1.0 <1.0 <1.0
31811996 <1.0 <1.0 <1.0 <1.0
4/3/1996 <1.0 <1.0 <1.0 <1.0
5/3/1996 <l.O <1.0 <1.0 <1.0
8/1/1996 <1.0 <1.0 <1.0 <1.0
9/4/1996 <1.0 <1.0 <1.0 <1.0
1011/1996 <1.0 <1.0 <1.0 <1.0
I ln/1996 <1.0 <1.0 <1.0 <1.0
12/5/1996 <1.0 <1.0 <1.0 <1.0
1/6/1997 <1.0 <1.0 <1.0 <1.0
311211997 <1.0 <1.0 <1.0 <1.0
4/8/1997 <1.0 <1.0 <1.0 <1.0
5/14/1997 <LO <1.0 <1.0 <1.0
61611997 <1.0 <1.0 <1.0 <1.0
7/2/1997 <1.0 <1.0 <1.0 <1.0
8/7/1997 <1.0 <1.0 <1.0 <1.0
9/5/1997 <1.0 <1.0 <1.0 <1.0
10/2/1997 <1.0 <1.0 <1.0 <1.0
-1111311997· <J..O -<LO -:--<J·.o---<1.0-----
12/5/1997 <LO <1.0 <1.0 <1.0
11911998 <1.0 <1.0 <1.0 <1.0
2/5/1998 <1.0 <1.0 <1.0 <1.0
31511998 <1.0 17 3.2 <1.0
41311998 <1.0 <1.0 <LO <1.0
517/1998 <1.0 <1.0 <1.0 <1.0
61511998 <1.0 <1.0 <1.0 <1.0
7/9/1998 <1.0 <1.0 <1.0 <1.0
8/7/1998 <1.0 <1.0 <1.0 <1.0
911011998 <1.0 <1.0 <1.0 <1.0
10/2/1998 <1.0 <1.0 <1.0 <1.0
11/4/1998 <1.0 <1.0 <1.0 <1.0
12/1/1998 <1.0 <1.0 <1.0 <1.0
1/11/1999 <l.O <1.0 <1.0 <1.0
•2111199 <1.0 <1.0 <1.0 <1.0
3/5/1999 <1.0 <1.0 <1.0 <1.0
4/8/1999 <1.0 <1.0 <1.0 <1.0
5/1211999 <1.0 <1.0 <1.0 <1.0
6/1011999 <LO <1.0 <1.0 <1.0
7/8/1999 <1.0 <1.0 <1.0 <1.0
8/5/1999 <LO <1.0 <1.0 <1.0
9/9/1999 <1.0 <1.0 <1.0 <1.0
10/14/1999 <1.0 <1.0 <1.0 <1.0
11/2/1999 <1.0 2.5 <1.0 <1.0
12/3/1999 <l.O 2.8 <1.0 <1.0
RPS: 3500 7 70
RPS: Remediation Perfonnance Standard
liiiiiil liillil liiiiiil iiiiil
TABLE 2 (Page I of2)
EFFLUENT Analytical Results
LOWER DOCKERY
Macon Dockery Site
Richmond County, North Carolina
Methylene l,1.1-Trichlor Trichloro-.
chloride ethane ethene Benzene Toluene
(uglL) (uglL) (uon ) (ug/L) (uon)
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <LO <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 3.4
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <i.O <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <l.O <1.0 _<1.0_ .~1.0_ -<2:0 " -<1.0 -<1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 5.5 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<5.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <l.O <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <LO
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 <1.0 -:::1.0 <1.0 <1.0
<2.0 <1.0 <1.0 <1.0 <1.0
<2.0 1.2 <1.0 <1.0 <1.0
5 200 2.8 1000
-
Total Suspended
Xylenes Chromium Barium Manganese Zinc Cadmium Solids
(uglL) (ug/L) (ue/L) (ue/L) (ue/1 l (ue/L) (me/1 l
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 5
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 14 <20 <0.30 <5.0
<3.0 <10 <50 13 <20 0.56 <5.0
<3.0 <10 <50 11 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 35 <20 <0.30 19
<3.0 <10 <50 6 <20 <0.30 <5.0
<3.0 <10 70 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
::::3.0 __ _ <JO -<50 ---<5.0--:-<20--<0.30--<5.o:-
<3.0 <10 <50 <5.0 <20 <1 <5.0
<3.0 <10 <50 160 <20 <0.30 <5.0
<3.0 <10 <50 34 <20 <0.30 <5.0
<3.0 <10 <50 250 <20 <0.30 58
<3.0 <10 <200 85 <20 <0.30 <5.0
<3.0 <10 <200 39 <20 <0.30 <5.0
<3.0 <10 <50 17 <20 <0.30 <5.0
<3.0 <10 <50 6.3 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 17 140 <20 <0.30 <5.0
<3.0 <10 <50 10 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 5.2 <20 <0.30 <5.0
<3.0 <10 <50 15 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 52 9.5
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 5.0 <20 <0.30 <5.0
<3.0 <10 72 520 31 <0.30 <5.0
<3.0 <10 93 470 38 <0.30 <5.0
<3.0 <10 <50 11 <20 <0.30 <5.0
<3.0 <10 <50 110 <20 <0.30 <5.0
400 50 1000 50 5000 5
-
Sample
Location
LO Effluent
---
RPS:
RPS:
- -
I!!!!!!!!!
Chloro-I, 1-Dichloro-
Date form ethane
(ug/L) (ue/L)
2/25/2000 <LO 6.2
3/9/2000 <1.0 <1.0
417/2000 .. System
5/9/2000 <LO <1.0
6/9/2000 <LO <1.0
7/7/2000 <1.0 <1.0
8/3/2000 <1.0 <1.0
9/25/2000 <LO <1.0
10/12/2000 <1.0 <1.0
1/18/2001 .. System
4/24/2001 <LO I <1.0
5/11/2001 <1.0 <1.0
7/11/2001 .. System
10/18/2001 <1.0 <1.0
1/16/2002 System
7/31/2002 System
10/30/2002 <1.0 <1.0
1/28/2003 System
3/14/2003 <1.0 <1.0
4/3/2003 <1.0 <1.0
7/10/2003 <1.0 <1.0
I 0/30/2003 <1.0 <1.0
1/13/2004 --<1".0 --<1.0 --
4/5/2004 (_ ~System
6/28/2004 f-System
1/27/2005 System
5/4/2005 System
8/25/2005 System
I 0/30/2005 System
3500
Remediation Perfonnance Standard
l!!!!!I I!!!!! ~
I, 1-Dichloro-Cis/trans-1,2-
ethene Dichloroethene
(ue/L) (uon)
<1.0 <1.0
<1.0 <1.0
Dov.n Not
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
Do"n Not
I <1.0 I <1.0 I <1.0 <1.0
Dov.n Not
<1.0 <1.0
Do"n Not
Do"n Not
<1.0 <1.0
Do"n Not
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO -..51.0_ ----<l.o-· <2.0
Do"n Not
Suspended Not
Suspended Not
Suspended Not
Suspended Not
Suspended Not
7 70
== liiiilil liiiiiil iiiil iiiil
Methylene
chloride
(uon)
<2.0
<2.0
Sampled
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
Sampled
<2.0 I <2.0
Sampled
<2.0
Sampled
Sampled
<2.0
Sampled
<2.0
<2.0
<1.0
~I.O_
<5.0
Sampled
Sampled
Sampled
Sampled
Sampled
Sampled
5
TABLE 2 (Page 2 of2)
EFFLUENT Analytical Results
LOWER DOCKERY
Macon Dockery Site
Richmond County_ North Carolina
I, I, 1-Trichloro Trichloro-.
ethane ethene Benzene Toluene
(ug/L) (ug/L) (ug/L) (uon)
2.6 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 .. ... System
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <LO <LO
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<LO <LO <1.0 <1.0 .. ... System
<1.0 <1.0 I <1.0 I <1.0
<1.0 <l.O <1.0 <1.0 .. ... System
<1.0 <1.0 <1.0 <1.0
System
System
<1.0 <1.0 <1.0 <1.0
System
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
-.<J.Q,_ -<1.0 --<1.0~ -<1.0-=-
<1.0 <1.0 <1.0 <1.0
System
System
System
System
System
System
200 2.8 1000
Total
Xylenes Chromium
(uon) (ue/L)
<3.0 <10
<3.0 <IO
Dov.n
<3.0 <IO
<3.0 <IO
<3.0 <10
<3.0 <IO
<3.0 <10
<3.0 <IO
Do"n
I <3.0 I <10
<3.0 <IO
Do\m
<3.0 <IO
Dov.n Not
Do= Not
<3.0 <IO
Do"n Not
<2.0 <IO
<3.0 <10
<3.0 <IO
·<3.o-~<10-
<2.0 <10
Do"n Not
Suspende< Not
Suspende, Not
Suspende< Not
Suspende, Not
Suspende< Not
400 50
- - -..
Suspended
Barium Manganese Zinc Cadmium Solids
(ue/L) (ug/L) (ue/L) (ue/L) (mg/L)
<50 320 <20 <0.30 <5.0
<50 53 <20 <0.30 <5.0
Not Sampled ...
<50 180 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 100 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 <5.0 97 <0.30 <5.0
<50 <5.0 97 <0.30 <5.0
Not Sampled ...
I <50 I <5.0 I <20 I <0.30 I <5.0
<50 <5.0 <20 <0.30 <5.0
Not Sampled ...
<50 <5.0 <20 <0.30 <5.0
Sampled
Sampled
<50 58 <20 <0.30 <5.0
Sampled
<50 <5.0 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 <5.0 go -~0.30_ -<5.0 --<so~ -<5--:0 --<20 <0.30 <5.0
<50 <5.0 <20 <0.30 10
Sampled
Sampled
Sampled
Sampled
Sampled
Sampled
1000 50 5000 5
l!!!!l!!l l!!!!!I I!!!!!
Chloro-I, l •Dichloro-I, -Dichloro-
Sample Date lorn> ,than, ethene
Location (ug/L) (uofl) (u"n)
UMSAEffiuent 2/1711996 <1.0 <1.0 <1.0
2/22/1996 <1.0 <1.0 <1.0
2/28/1996 <1.0 <1.0 <1.0
3/8/1996 <1.0 <l.0 <1.0
4/3/1996 <1.0 <1.0 <1.0
5/3/1996 <1.0 <1.0 <1.0
6/5/1996 <1.0 <1.0 <1.0
7/1/1996 <i.0 <1.0 <1.0
7/30/1996 <1.0 <1.0 <1.0
9/4/1996 <1.0 <1.0 <1.0
10/1/1996 <1.0 <1.0 <1.0
1117/1996 <1.0 <1.0 <1.0
12/5/1996 <1.0 <1.0 <1.0
l/6/1997 <1.0 <1.0 <1.0
2/4/1997 <1.0 <1.0 <1.0
3/12/1997 <1.0 <1.0 <1.0
4/8/1997 <1.0 <1.0 <1.0
5/12/1997 <J.0 <1.0 <1.0
6/6/1997 <1.0 <1.0 <1.0
712/1997 <1.0 <1.0 <1.0
817/1997 <LO <1.0 <LO
9/5/1997 <1.0 <1.0 <1.0
1012/1997 <1.0 <1.0 <LO ----. ----11/13/1997 ·<1.0 <1.0 <1.0
12/5/1997 <1.0 <1.0 <LO
119/1998 <1.0 <1.0 <1.0
2/5/1998 <1.0 <1.0 <1.0
3/5/1998 <1.0 <1.0 <1.0
4/3/1998 <1.0 <1.0 <1.0
517/1998 <1.0 <LO <1.0
6/5/1998 <1.0 <1.0 <1.0
7/9/1998 <1.0 <LO <1.0
8/7/1998 <1.0 <1.0 <1.0
9/10/1998 <1.0 <1.0 <1.0
1012/1998 <1.0 <1.0 <1.0
11/4/1998 <LO <1.0 <1.0
12/1/1998 <LO <1.0 <1.0
1/11/1999 <1.0 <1.0 <1.0
2/11/1999 <1.0 <1.0 <1.0
3/5/1999 <1.0 <1.0 <1.0
4/8/1999 <1.0 <1.0 <1.0
5/13/1999 <1.0 <1.0 <1.0
6/10/1999 <1.0 <1.0 <1.0
7/Bf\999 <1.0 <LO <LO
8/511999 <1.0 <LO <1.0
9/9/1999 <1.0 <LO <LO
10/14/1999 <1.0 <1.0 <1.0
11/2/1999 <1.0 <1.0 <LO
12/3/1999 <1.0 <LO <1.0
RPS 3500
RPS Remediation Performance Slandard
NA: Not Analyz.ed
Cis/trans-1,2-Tetrachloro-
Dichloroethene """'' (ucr/1) (uo/1)
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
_51.0_ __ <1.0_
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
70
lilil lliiil
TABLE 3 (Page 1 of 2)
EFFLUENT Analytical Resul1s
UPPER MACON SOURCE AREA
Macon Dockery Site
Richmond County, Nroth Carolina
1,1.1-Trichloro-Trichloro-Vinyl
<than, ethene chloride Benzene
(ug/1) (uo/1) (uo/1) (ug/L)
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <l.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
-<1.0 -<!.0 . -<1.0--<LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
200 2.8
Toluene
(uon)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
2.9
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<LO
<1.0
-<1.0"-
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<i.0
<i.0
<1.0
<1.0
<1.0
<1.0
1000
---..
Suspended
Chromium Barium Manganese Zinc Cadmium Lead Mercury Solids
(uo-11) (u2iL) (ug/L) (ug/L) (ua/l) (ug/L) (uofl) (moll)
<10 120 120 <20 <0.30 <3.0 <.2 <5.0
<10 120 70 <20 <0.30 <3.0 <.2 <5.0
<10 130 51 <20 <0.30 <3.0 <.2 <5.0
<!O 120 37 <20 <0.30 <3.0 <2 <5.0
<10 110 27 <20 <0.30 <3.0 <.2 5
<10 120 26 <20 <0.30 <3.0 <.2 <5.0
<10 130 22 <20 <0.30 <3.0 <.2 6
12 110 14 <20 <0.30 <3.0 NA <5.0
<10 200 110 41 <0.30 9.2 NA 23
11 170 68 26 <0.30 66 NA 16
<10 130 13 <20 0.47 <3.0 NA 24
<10 140 13 <20 <0.30 <3.0 NA 26
<10 170 17 <20 <0.30 <3.0 <0.20 5
<10 200 46 25 <0.30 3.5 NA 120
<10 160 29 <20 <0.30 <3.0 NA 8
<!O 130 30 <20 <0.30 <3.0 NA <5.0
<!O 200 30 <20 <0.30 <3.0 NA 7
12 210 95 35 <0.30 <3.0 NA 100
<10 240 74 <20 <0.30 <3.0 NA <5.0
<10 180 41 <20 <0.30 <3.0 NA <5.0
11 230 250 40 <0.30 4.8 NA NA
<10 130 27 <20 <0.30 <3.0 ~NA --22 --<10--1s5 ---31:5 -<20 -<0.3O <3.0 NA 11
<10 129 84.2 <20 <1 <3.0 NA 8
<10 150 160 26 <0.30 6.5 NA <5.0
<10 180 33 <20 <0.30 <3.0 NA <5.0
<10 200 20 <20 <0.30 <3.0 NA 6
11 210 160 25 <0.30 4.1 NA <5.0
<10 <200 64 <20 <0.30 <3.0 NA <5.0
<10 210 310 29 <0.30 5 NA 13
<10 160 46 <20 <0.30 <3.0 NA <5.0
<10 240 110 <20 <0.30 <3.0 NA <5.0
<10 190 37 <20 <0.30 <3.0 NA <5.0
<10 200 56 <20 <0.30 <3.0 NA 33
<10 190 110 <20 <0.30 <3.0 NA 12
10 220 450 48 <0.30 4.6 NA 180
<10 160 68 <20 <0.30 <3.0 NA <5.0
<10 150 120 <20 <0.30 <3.0 NA <5.0
<10 230 120 22 <0.30 <3.0 NA <5.0
<10 180 100 25 <0.30 <3.0 NA <5.0
<10 170 72 <20 <0.30 <3.0 NA <5.0
<10 170 66 <20 36 <3.0 NA 8 5
<10 180 100 <20 <0.30 <3.0 NA <5.0
<10 170 160 <20 <0.30 3.3 NA <5.0
<10 140 13 <20 <0.30 8.7 NA <5.0
<10 150 340 24 <0.30 <3.0 NA <5.0
<10 200 37 <20 <0.30 <3.0 NA <5.0
<10 180 13 <20 <0.30 <3.0 NA <5.0
<!O 180 18 <20 <0.30 <3.0 NA <5.0
50 1000 50 5000 15 LI
!!!!!!I l!!!l!I ==
Sample
Location
-
RPS
RPS
NA:
-
Chloro-I, 1-Dichloro-
Date fonn """" (ugil..) (ul!!l )
2/16/2000 <1.0 <LO
3/9/2000 <1.0 <1.0
4/7/2000 <1.0 <1.0
5/8/2000 <1.0 <1.0
6/9/2000 <1.0 <1.0
7/7/2000 <LO <1.0
8/2/2000 <1.0 <1.0
9/25/2000 <1.0 <1.0
10/12/2000 <1.0 <1.0
1/18/2001 <1.0 <1.0
5/3/2001 <1.0 <1.0
7/11/2001 <1.0 <1.0
10/18/2001 <1.0 <1.0
12/28/2001 <1.0 <1.0
1/15/2002 <1.0 <1.0
7/30/2002 <1.0 <LO
10/30/2002 <1.0 <1.0
1/28/2003 NOT
3/14/2003 <LO <1.0
4/3/2003 <LO <LO
7/10/2003 <LO _<1.0_
. -I0/30/26of -<1.0 <1.0
J/13/2004 <1.0 <1.0
4/5/2004 <1.0 <l.O
6/28/2004 <1.0 <1.0
l0/21/2004 <1.0 <1.0
ln712005 <1.0 <1.0
5/4/2005 <1.0 <1.0
8/25/2005 <1.0 <1.0
l0/30/2005 • <1.0 <1.0
3500
Remediation Performance Standard
Not Analyzed
llliiiiil liiiilil liiiil liiiiil iiiil liiiil ---
I, -Dichloro-Cis/trans-1,2-Tetrachloro-
ethene Dichloroethene ethene
(ug/L) (ug/L) (u"fl )
<1.0 <1.0 <1.0
16 <1.0 1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
9.9 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
SAMPLED SYSTEM DOWN
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
-<1.0_ ·-~I.◊~-_<J.O'--
<1.0 <LO <1.0
<1.0 <2.0 <1.0
<1.0 <2.0 <1.0
<1.0 <2.0 <1.0
<1.0 <2.0 <1.0
<1.0 <2.0 <1.0
1.2 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
70
TABLE 3 (Page 2 of 2)
EFFLUENT Analytical Results
UPPER MACON SOURCE AREA
Macon Dockeiy Site
Richmond County Nroth Carolina
I, I, 1-Trichloro-Trichloro-Vinyl
ethane ethene chloride Benzene
(U"/1) (U"/1 ) (unfl ) (U"/1)
<LO <1.0 <1.0 <1.0
2.6 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <LO
1.4 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <LO <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <J.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
NOT
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
Toluene
(ug/L)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
!-;AMPLED
<LO
<LO
-<1.0 -·<1-.0 --<I-.0 ·-<J.O --<1'.0
<1.0 <1.0 <1.0 <1.0 <l.O
<1.0 <J.0 <1.0 <1.0 <l.O
<1.0 <1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 <l.O
<LO <1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <l.O <1.0
<LO <1.0 <1.0 <1.0 <1.0
200 2.8 l000
Chromium Barium
(u"fl ) (u"n )
<10 240
<10 230
<IO 210
<IO 410
<IO 180
<IO 220
<IO 190
<IO 280
14 180
<10 200
28 440
15 360
60 450
II 360
<10 36-0
21 370
20 370
SYSTEM
17 410
II 350
-<10-~37◊-
<10 360
76 400
<10 230
<10 160
<10 180
<10 170
NA 140
<5.0 160
<5.0 150 ·
1000
-- - -
liiiiiil
Suspended
Manganese Zinc Cadmium Lead MerCUJ)' Solids
(u:11 ) (U"/1) (unfl ) (u·,11) (ug/L) (mg/L)
300 40 <0.30 5.3 NA 130
47 <20 <0.30 <3.0 NA 5.0
40 <20 <0.30 <3.0 NA <5.0
54 <20 <0.30 <3.0 NA <5.0
61 <20 <0.30 <3.0 NA <5.0
250 32 <0.30 3.8 NA <5.0
80 <20 <0.30 4.1 NA 38.0
83 <20 <0.30 <3.0 NA <5.0
84 <20 <0.30 3.7 NA 6.0
36 <20 <0.30 <3.0 NA 8.5
350 29 <0.30 19 NA <5.0
110 <20 <0.30 3.7 NA 38
900 47 <0.30 21 NA <5.0
110 <20 <0.30 <3.0 NA 8.0
35 <20 <0.30 <3.0 NA 8.0
130 <20 <0.30 3.0 NA 11.0
98 <20 <0.30 4.0 <0.20 6.0
DOWN
240 43 <0.30 480 <0.20 <5.0
44 <20 <0.30 -280 -<0.20 -7----<20 -71 <0.30 <3.0 <0.20 42
170 120 <0.30 <3.0 <0.20 <5.0
1800 210 0.47 62 NA 23
64 <20 <0.30 <3.0 NA 33
6.2 <20 <0.30 <3.0 NA <5.0
18 <20 <0.30 <3.0 NA <5.0
8.5 <20 <0.30 <3.0 NA <5.0
NA <20 <0.30 <1.5 NA <5.0
44 <20 <0.30 NA NA <5.0
8,2 , <20 , <0.30 · <l.5· NA <5.0 ~
5000 15 I.I
- - - -
l!!l!!!I l!!!!!!!l!!!I l!!9
Chloro-1,1-Dichloro-1, 1-Dichloro-Cis.ltrans-1,2-Methylene
Sample Date fonn ethane ethene Dichloroethene chloride
Location (uo/1) (u•") (uo-11 ) (uo/1) (u<>fl)
U/L Effluent 2/24/1996 <1.0 <1.0 <1.0 <l.O <2.0
2/25/1996 <1.0 <l.0 <1.0 <1.0 <2.0
2/28/1996 <1.0 <1.0 <1.0 <1.0 <2.0
3/8/1996 <1.0 <1.0 <1.0 <1.0 <2.0
3/16/1996 <1.0 <1.0 <1.0 <1.0 <2.0
4/3/1996 <1.0 1.8 <1.0 1.6 <2.0
5/3/1996 <1.0 <1.0 <1.0 <1.0 <2.0
6/5/1996 <1.0 <1.0 <1.0 <1.0 <2.0
7/1/1996 <1.0 <LO <1.0 <1.0 <2.0
7/30/1996 <1.0 <1.0 <1.0 <1.0 <2.0
9/4/1996 <1.0 <LO <1.0 <1.0 <2.0
10/1/1996 <1.0 <1.0 <l.O <1.0 <2.0
11/7/1996 <1.0 <1.0 <!.O <LO <2.0
12/5/1996 <1.0 <1.0 <1.0 <1.0 <2.0
1/6/1997 <1.0 <1.0 <1.0 <1.0 <2.0
2/4/1997 <1.0 <1.0 <1.0 <1.0 <2.0
3/12/1997 <1.0 <1.0 <1.0 <1.0 <2.0
4/8/1997 <1.0 <1.0 <LO <1.0 <2.0
5/12/1997 <1.0 <1.0 <1.0 <1.0 <2.0
6/6/1997 <1.0 <1.0 <1.0 <1.0 <2.0
7/2/1997 <1.0 2.4 <1.0 1.8 <2.0
7n5/1997 NA NA NA NA NA
811/1997 <1.0 . -~LO_ .. -_<LO_ . ---'-<1.0 --<2.0·-----9/5/1997 -<fo <1.0 <1.0 <1.0 <2.0
10/2/1997 <1.0 <1.0 <1.0 <1.0 <2.0
11/13/1997 <1.0 <1.0 <1.0 <1.0 <2.0
12/5/1997 <LO <1.0 <1.0 <1.0 <2.0
1/9/1998 <LO <1.0 <J.0 <1.0 <2.0
2/5/1998 <LO <1.0 <1.0 <1.0 <2.0
3/5/1998 <LO <1.0 <J.0 <1.0 <2.0
4/3/1998 <1.0 <1.0 <1.0 <1.0 <2.0
5/7/1998 <1.0 <1.0 <1.0 <1.0 <2.0
6/5/1998 <1.0 <1.0 <1.0 <1.0 <2.0
7/9/1998 <1.0 <1.0 <1.0 <1.0 <2.0
81111998 <1.0 <1.0 <1.0 <1.0 <2.0
9/10/1998 <1.0 <1.0 <1.0 <1.0 <2.0
10/2/1998 <1.0 <1.0 <1.0 <1.0 <2.0
11/4/1998 <1.0 <1.0 <1.0 <1.0 <2.0
12/1/1998 <LO <1.0 <1.0 <1.0 <2.0
1/11/1999 <1.0 <1.0 <1.0 <1.0 <2.0
2/11/1999 <1.0 <LO <1.0 <1.0 <2.0
3/5/1999 <1.0 <1.0 <1.0 <1.0 <5.0
4/8/1999 <1.0 <1.0 <1.0 <1.0 <2.0
5/13/1999 <1.0 <1.0 <1.0 <1.0 <2.0
6110/1999 <1.0 <1.0 <1.0 <1.0 <2.0
RPS. 3500 70
RPS: Remediation Performance Standard
NA: Not Analyzed
lliiiil liiiil liliil
TABLE 4 (Page I of 2)
EFFLUENT Analytical Results
UPPER/LOWER MACON
Macon Dockery Site
Richmond County, North Carolina
Tetrachloro-I, I, 1-Trichloro-Trichloro-
ethene ethane ethene
(uof ) (uoO ) (uoll)
<l.O <LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 1.9
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
NA NA NA
-<LO-~ <1.0--<1.0--=-
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <l.O <l.O
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
200 2.8
TABLE 4 (Page 2 of 2)
Toluene
(uoll )
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
2.1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
NA
-<1.0-
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1000
liiiil liiiil ---.. lllil iilil
S"'P"'ded
Chromium Barium Manganese Zinc Cadmiwn Lead Solids
(uo-11) (uofl ) (uo/1) (ug/L) (u•< ) (u,-,11) (moll)
<10 83 150 150 <0.30 3.7 <5.0
<10 90 160 170 <0.30 3.6 <5.0
<10 <50 32 59 <0.30 <3.0 8
<IO <50 39 56 <0.30 <3.0 <5,0
<IO <50 JI 51 <0.30 <3.0 <5.0
<IO <50 44 54 <0.30 3.6 IO
<IO 31 10 21 <0.30 <3.0 <5.0
<IO <50 7.5 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 24
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <10 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 39 <5.0 <20 <0.30 <3.0 8
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<IO <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 79 <20 <0.30 <3.0 <5.0
NA . -l'!t-. . -"'-36_ . -NA -<0.30--NN -NA --<10 <50 5.4 <20 <0.30 3.1 NS
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 6.3 <20 <0.30 <3.0 25
<10 <50 <5.0 <20 <0.30 <3.0 <5
<10 <50 <5.0 <20 <0.30 <3.0 <5
<IO <50 <5.0 <20 <0.30 <3.0 <5
<10 56 <5.0 <20 <0.30 <3.0 <5
<10 <200 <15 <20 <0.30 <3.0 <5.0
<10 <200 <5.0 <20 <0.30 <3.0 <5.0
<IO <50 <5.0 <20 <0.30 <3.0 NA
<IO <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 9.2 <20 <0.30 <3.0 <5.0
<IO <50 6.7 <20 <0.30 <3.0 <5.0
<IO JI <10 <20 <0.30 <3.0 <5.0
<IO <50 6.2 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <10 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<IO <50 <5.0 <20 <0.30 <3.0 <5.0
50 1000 50 5000 15
== == liiiiiiiiil liiiiil liiiilil liiil
Chloro-I , I -Dichiaro-I , 1-Dichloro-Cis/trans-1,2-Methylene
Sample
Location
U/L Effluent
--
Date fonn ethan,
(ug/L) (u,n)
7/8/1999 <1.0 <1.0
8/5/1999 <1.0 <1.0
9/9/1999 <1.0 <1.0
10/14/1999 <1.0 <1.0
11/3/\999 <1.0 <1.0
12/3/1999 <1.0 <1.0
2/17/2000 <1.0 <1.0
3/9/2000 <1.0 <1.0
4/7/2000 <1.0 <1.0
5/8/2000 <1.0 <1.0
619/2000 <1.0 <1.0
7/7/2000 <1.0 <1.0
812/2000 <1.0 <1.0
9/25/2000 <1.0 <1.0
10/12/2000 <1.0 <1.0
1/18/2001 ... Not
4/24/2001 <1.0 <1.0
5/3/2001 <1.0 <1.0
7/20/2001 <1.0 <1.0
10/18/2001 <1.0 <1.0
12/28/2001 <1.0 <1.0
1/15/2002 <1.0 <1.0
7/3In002 Not
-1013012002 -<rn ·~1.0--
\/28/2003 <1.0 <1.0
4/3/2003 <1.0 <1.0
7/10/2003 <1.0 <1.0
10/30/2003 <1.0 <1.0
1/13/2004 <1.0 <1.0
4/5/2004 <1.0 <1.0
6/28/2004 Not
10/21/2004 <1.0 <1.0
1/27/2005 <1.0 <1.0
5/4/2005 <1.0 <1.0
8/25/2005 <LO <1.0
10/30/2005 <1.0 <1.0
3l00
Remediation Petfonnance Standard
Not Analyzed
ethene Dichloroethene chloride
(ug/L) (ua/l.) (ug/L)
<1.0 <1.0 <2,0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <LO <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<LO <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<LO <1.0 <2.0
<LO <1.0 <2.0
<1.0 <1.0 <2.0
Sampled System
<LO <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
Sampled _ 2y_sten_:i_ ----<ro-<1.0--<2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
( <1.0 <2.0
9.8 <2.0 <5.0
<1.0 <2,0 <5.0
Sampled System
8.5 LO <5.0
<1.0 <2,0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
70 5
llii1 iiiil liiiiil
EFFLUENT Analytical Results
UPPER/LOWER MACON
Macon Dockery Site
Richmond County, North Carolina
Tetrachloro-I .I, 1-Trichloro-Trichloro-
<th~, <than, ethene
(ullfl) (u.JI) (ug!L}
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <i.O <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <I.0
<1.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
Do= ... ...
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
-Do~---------<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
L9 <1.0 <1.0
(.6 <1.0 <1.0
Do= u <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
200 2.8
Toluene
(ug/L)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<I.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
--
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1000
-- - -
Suspended
Chromium Barium Manganese Zinc Cadmium L<ad Solids
(u,n) (u11/I.) (u11/I) (UPII) (ug/L) (uwL) (m<>fl)
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO 47 <20 <0.30 3.7 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <OJO <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<ID <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO 20 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 27 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
Not Sampled System Oo•n ...
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <lO <5.0 <20 <0.30 <3.0 <5.0
<10 <,0 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
-Not . Sampled ----·System --0o .... 11----
<10 64 <5.0 <20 <0.30 <3.0 <5.0
<10 <lO 30 <20 <0.30 7.5 J
<10 <lO (( <20 <0.30 <3.0 <5.0
<(0 <lO 30 <20 <0.30 <3.0 <5.0
<(0 <lO (8 <20 <0.30 <3.0 <5.0
<(0 <lO 29 24 <0.30 <3.0 20
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
Not Sampled System Oo•n
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
<(0 <lO <5.0 <20 <0.30 <3.0 <5.0
NA JO NA <20 <0.30 <1.5 <5.0
<5.0 34 <5.0 <20 <0.30 NA <5.0
<5,0 37 · <5.0 , <20. <0.30 · <l.5 · <5.0-
50 1000 lO lOOO 15
I
I
I
!Sample
:Location
VE-01
I
I
OW-1
I
I
I OW-3
I
I
g OW-5
D
D
SVE Exhaust
I
I
I
I
TABLE 5
Air Quality Summary
Macon/Dockery Site -Richm<ind County, North Carolina
Page11
II
Dale
I
Chloroform 1,2-Dichloroethene Trichloroethene
me/mJ I me/mJ IDl!/mJ
2122/1996 <10 I <10 <10
6/5/1996 <10 <JO <10
7/1/1996 <10 ' <10 <10
11/8/1996 <10 <10 <10
6/23/1997 <10 <10 <10
I 1/13/1997 <2.0 I 2.3 <2.0
6/19/1998 <2.0 <2.0 <2.0
11/4/1998 <2.0 I <2.0 <2.0
5/13/1999 <2.0 ' <2.0 <2.0
11/3/\999 <2.0 ' <2.0 <2.0
5/8/2000 <1.0 ' <1.0 <1.0
2/22/1996 <10 I, <10 <10
6/5/1996 <10 <10 <10
7/1/1996 <10 I' <10 <10
11/8/J 996 <10 <10 <10
6/23/1997 <10 ' <10 <10
11/13/1997 <2.0 I <2.0 <2.0
6/19/1998 <2.0 <2.0 <2.0
11/4/1998 <2.0 I• <2.0 <2.0
5/13/1999 <2.0 <2.0 <2.0
I 1/3/1999 <2.0 I <2.0 <2.0
5/8/2000 <1.0 ' <LO <1.0
I
2/22/1996 <10 I 80 <10
6/5/1996 <10 <10 <10
7/1/1996 230 I <10 <10
11/8/\996 <10 <10 <10
6/23/1997 <10 I <10 <10
11/13/1997 <2.0 ' <2.0 <2.0
6/19/1998 <2.0 <2.0 <2.0
11/4/1998 <2.0 I <2.0 <2.0
5/13/1999 <2.0 <2.0 <2.0
11/3/1999 <2.0 I <2.0 <2.0
5/8/2000 <1.0 <1.0 <1.0
'
2/22/1996 <10 I 380 <10
6/5/1996 <10 <10 <10
11/8/1996 <10 I <10 <10
6/23/1997 <10 <10 <10
l l/13/1997 <2.0 I <2.0 <2.0
6/19/1998 <2,0 <2.0 <2.0
11/4/1998 <2,0 <2.0 <2.0
5/13/1999 <2.0 I <2.0 <2.0
11/3/\999 <2.0 <2.0 <2,0
5/8/2000 <1.0 I <1.0 <1.0
2/14/1996 <10 I <10 <10
2/15/1996 <10 ' <10 <10
2/16/1996 <10 <10 <10
4/3/1996 <JO I <10 <10
6/5/1996 <10 <10 <10
7/1/1996 <10 I <10 <10
8/1/1996 <10 <10 <10
2/5/1997 <10 :1 <10 <10
6123/1997 <10 I <10 <10
8n11991 <2.0 I <2.0 <2.0
11/13/1997 <2.0 I <2.0 <2.0
2/6/1998 <2.0 <2.0 <2.0
5/7/1998 <2.0 I <2.0 <2.0
8n/1998 <2.0 I <2.0 <2.0
11/4/1998 <2,0 I <2.0 <2.0
2/11/1999 <2.0 ;1.<2.0 <2.0
5/13/1999 <2.0 '<2.0 <2.0
8/5/1999 <2.0 1'<2.0 <2.0
I 1/3/1999 <2.0 . <2.0 <2,0
5/8/2000 <1.0 i<I.0 <1.0
8/3/2000 <1.0 1<!.0 <1.0
Toluene
m1!/m3
<10
<10
<10
<ID
<10
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
<10
<10
<10
<10
<10
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
<10
<10
<10
<10
<10
<2,0
<2.0
<2.0
<2.0
<2,0
<1.0
<10
<10
<10
<10
<2,0
<2.0
<2.0
<2.0
<2.0
<LO
45
43
73
<10
<10
<10
<10
<10
<10
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2,0
1.2
<I.Cl
/
I
I
I
I
I
I
I
I
n
D
I
I
I
I
I
I
I
I
I
TABLE 5
Air Quality Summary
Macon/Dockery Site -Richm6nd County, North Carolina
Page12
I
I
I•
lj
!Sample II
Date
I
Chloroform 1,2-Dichlorodhene Trichloroethene Toluene
Location me/mJ ' m1!/m3 m1lfm3 m2/m3
SVE Inlet Line 6/5/1996 57 <10 <10 <10
7/1/1996 <10 <10 <10 <10
Unrv•r Dockerv Air Stack 2/16/1996 <10 <10 <10 <10
4/3/1996 <10 ' <10 <10 <10
6/5/1996 <10 I <10 <10 <10
7/1/1996 <10 I <10 <10 <10
8/1/1996 <10 I <10 <10 <10
\ l/8/1996 <10 I <10 <10 <10
2/5/1997 <10 I <10 <10 <10
5/12/1997 <10 I <10 <10 <10
8n/1997 <2,0 ' <2.0 <2.0 <2.0
11/13/1997 <2.0 ' <2.0 <2.0 <2.0
2/6/1998 <2.0 <2.0 <2.0 <2.0
5/7/1998 <2.0 <2.0 <2.0 <2.0
8/7/1998 <2.0 <2.0 <2.0 <2.0
11/4/1998 <2.0 <2.0 <2.0 <2.0
2/11/1999 <2.0 ' <2.0 <2.0 <2.0
5/13/1999 <2.0 I <2.0 <2.0 <2.0
8/5/1999 <2.0 I <2.0 <2.0 <2.0
11/3/1999 <2.0 I <2.0 <2.0 <2.0
5/9/2000 <1.0 I <1.0 <1.0 <1.0
8/3/2000 <1.0 I <1.0 <1.0 <i.0
1/18/2001 <1.0 I <1.0 <1.0 <i.0
7/11/2001 <1.0 I <1.0 <1.0 <1.0
1/16/2002 <1.0 ' <i.0 <1.0 <1.0
7/31/2002 <1.0 <1.0 <1.0 <1.0
1/28/2003 Svstem Down -Not Samnled
7/16/2003 System Down -Not Sampled
1/13/2004 <1.0 <1.0 <1.0 <1.0
6/28/2004 <1.0 <1.0 <1.0 <i.0
1/27/2005 <1.0 I <i.Q <1.0 <1.0
8/25/2005 <1.0 I <J.Q <i.0 <1.0
10/30/2005· <1.0 I <1.0 <1.0 <1.0
I
Lower Dockerv Air Stack 4/3/1996 <10 l<JO <10 <10
8/1/1996 <10 1·<10 <10 <10
11/8/1996 <ID 1<10 <ID <10
5/12/1997 <10 1<10 <10 <10
11/13/1997 <2.0 ,<2.0 <2.0 <2.0
2/6/1998 <2.0 ,<2.0 <2.0 <2.0
Sn/1998 <2,0 .<2.0 <2.0 <2.0
8/7/1998 <2.0 '<2.0 <2.0 <2.0
11/4/1998 <2.0 '.<2.0 <2.0 <2.0
2/11/1999 <2.0 '<2.0 <2.0 <2.0
5/13/1999 <2.0 :<2.0 <2.0 <2.0
8/5/1999 <2.0 '<2.0 <2,0 <2.0
11/3/1999 <2.0 :<2.0 <2.0 <2.0
5/9/2000 <i.0 :<1.0 <1.0 <1.0
8/3/2000 <1.0 <:1.0 <1.0 <1.0
1/00/01 iSvstem Down -Not Sampled
4/24/2001 <1.0 I <1.0 I <i.0 <1.0
7/11/2001 System Down -Not Sampled
7/31/2002 Svstem Down -Not Samnled
1/28/2003 System Down -Not Sampled
7/16/2003 <1.0 I <1.0 I <1.0 <1.0
1/13/2004 <1.0 I <1.0 I <1.0 <1.0
6/28/2004* Remediation Svstem Sus.,..nded -Sample Not Collected
1/27/2005* Remediation Svstem Sus,....nded -Samnle Not Collected
8/25/2005 Remediation Svstem Sus ..... nded -Samnle Not Collected
10/30/2005 Remediation Svstem Sus.,..nded -Samele Not Collected
I I I I
Lower L>o.:kery Gmondwata Remed1at10n System Suspended on J/19/04 Sample 001 collected or analy;red
/
I
I
I
I
I
I Sample
...,.ation
Macon Source Air Stack
I
n
D
I
I
I
I
I
TABLE 5
Air Quality Summary
Macon/Dockery Site• Richmorid County, North Carolina
Page _3
Dale Chloroform 1,2 Dichloroethene Trichloroethene .• , 3 I m!!/mJ me/mJ
2/16/1996 <10 I <10 <10
4/3/1996 <10 <10 <10
5/3/1996 <10 I <10 <10
6/5/1996 50 <IO <10
7/1/1996 <10 <10 <10
R/1/1996 <10 I <10 <10
11/8/1996 <10 <10 <10
2/5/1997 <10 : <10 <10
5/12/1997 <10 ' <10 <10
8/7/1997 <2.0 <2.0 <2.0
11/13/1997 <2.0 I <2.0 <2.0
2/6/1998 <2.0 <2.0 <2.0
5/7/1998 <2.0 ' <2.0 <2.0
8/7/1998 <2.0 ' <2.0 <2.0
11/4/1998 <2.0 <2.0 <2.0
2/11/1999 <2.0 I <2.0 <2.0
5/13/1999 <2.0 <2.0 <2.0
8/5/1999 <2.0 ' <2.0 <2.0
11/3/1999 <2.0 1 <2.0 <2.0
2/17/2000 <2.0 <2.0 <2.0
5/8/2000 <1.0 I <1.0 <1.0
8/2/2000 <1.0 <1.0 <1.0
1/18/2001 <1.0 <1.0 <1.0
7/11/2001 <1.0 I <1.0 <1.0
1/16/2002 <1.0 <1.0 <1.0
7/31/2002 <LO I <1.0 <1.0
1/28/2003 I Svstem Down -Not Samoled
7/16/2003 <1.0 <1.0 <1.0
1/13/2004 <1.0 I· <1.0 <1.0
6/28/2004 <1.0 1.2 <LO
1/27/2005 <1.0 r <1.0 <1.0
8/25/2005 • <1.0 i <1.0 <1.0
I·
Toluene
m~/mJ
<10
<10
<10
<10
<10
<10
<10
<10
<10
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
<1.0
<1.0
<LO
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
✓
I
I
I
1sample
:l..ocallon
U/L Macon Air Stack
I
I
I
I
I
I PronPnv Line
g
n
D
D
I
I
TABLE 5
Air Quality Summary
Macon/Dockery Site -Richmond County, North Carolina
Page:4
II
0.1,
I
Chloroform 1,2-Dichloroethene Trichloroethene
m11:/m3 I m11:/m3 m11:/m3
2/16/1996 <10 I <10 <10
5/3/1996 <10 <\0 <10
6/5/1996 <10 I <10 <10
7/1/1996 850 ' <10 29
8/1/1996 <10 <10 <10
11/8/1996 <10 I <10 <10
215/1997 <10 <10 <10
5/12/1997 <10 I <10 <10
sn,1991 <2.0 <2.0 <2.0
11/13/1997 <2.0 I <2.0 <2.0
216/1998 <2.0 <2.0 <2.0
517/1998 <2.0 I <2.0 <2.0
sn/1998 <2,0 <2.0 <2.0
11/4/1998 NS I NS NS
2/11/1999 <2.0 <2.0 <2.0
5/13/1999 <2.0 I <2.0 <2.0
8/5/1999 <2.0 <2.0 <2.0
11/3/1999 <2.0 I <2.0 <2.0
2/17/2000 <2.0 ' <2.0 <2.0
5/8/2000 <1.0 ' <1.0 <1.0
8/212000 <1.0 I <1.0 <1.0
1/00/00 Svstem Down -Not Samoled
4/24/2001 <1.0 <1.0 <LO
7/11/2001 <1.0 <1.0 <1.0
1/16/2002 <1.0 I <1.0 <1.0
7/31/2002 NOT 1SAMPLED SYSTEM
1/28/2003 <1.0 r <1.0 <1.0
7/16/2003 <1.0 <1.0 <1.0
1/13/2004 <1.0 I <1.0 <1.0
6/28/2004 Svstem Down -Not Sampled
1/27/2005 <1.0 I <1.0 <1.0
8/25/2005 <1.0 <1.0 <1.0
I 0/30/2005 · <1.0 I <1.0 <1.0
2/16/1996 <10 I <10 <10
4/3/1996 <10 <10 <10
5/3/1996 <10 I <10 <10
6/5/1996 <10 <10 <10
7/1/1996 <10 ' <ID <ID
8/1/1996 <10 <10 <ID
11/8/1996 <10 <ID <10
2/5/1997 <10 ., <10 <10
5/12/1997 <10 <10 <10
817/1997 <2.0 I <2.0 <2.0
11/13/1997 <2.0 <2.0 <2.0
2/6/1998 <2.0 I <2.0 <2.0
51711998 <2.0 <2.0 <2.0
8/7/1998 <2.0 I <2.0 <2.0
11/4/1998 <2.0 <2.0 <2.0
2111/1999 <2.0 I <2.0 <2.0
5/13/1999 <2.0 <2.0 <2.0
8/5/1999 <2.0 I <2.0 <2.0
11/3/1999 <2.0 <2.0 <2.0
2/17/2000 <2.0 I <2.0 <2.0
5/8/2000 <1.0 <1.0 <1.0
Toluene
m11:/mJ
<10
<10
<10
<10
<10
<ID
<10
<10
<2.0
<2.0
<2.0
<2.0
<2.0
NS
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
DOWN
1.3
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<10
<ID
<ID
<10
<10
<10
<10
<2.0
<2,0
<2.0
<2.0
<2,0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
8/3/2000 .. Not anal•,.,.-Tedlar bag deflated durin~ sample shipment••
1/18/2001 <1.0 <1.0 <1.0 <1.0
7/11/2001 <1.0 <l.0 <1.0 <1.0
1/16/2002 <1.0 <1.0 <1.0 <1.0
7/31/2002 <1.0 <1.0 <1.0 <1.0
1/28/2003 <1.0 I <1.0 <1.0 <1.0
7/16/2003 <1.0 <1.0 <1.0 <1.0
1/13/2004 <1.0 I <1.0 <1.0 <1.0
6/28/2004 <1.0 <1.0 <1.0 <1.0
1/27/2005 <1.0 f"<l.0 <1.0 <1.0
8/25/2005 <1.0 <1.0 <1.0 <1.0
I 0/30/2005 • <1.0 I <1.0 <1.0 <1.0
✓
I
I
S,,,=
I Upper Dockery
I
I
I
I
I
I 12-1-911 to 12-11-911
12-31-911!0 1-27-99
1-27-99 lo 2•2l-99
2-23-99 to l-31).!l!I
l-l0-99 lo 4-29·!19 I 4-2ll-!19to S.27-119
S.27·99 to 6-2,-1111
6-24•99to7-2ll-99
7-29--99 to 11-27-99
ll-27·!19lo!1--2Hl!I
!1--27-!l!lto 10-29--99
10-29--99 to 11.24.99
11.2,.99 to 12.3,0.99
12-30-W lo 1,21.00 g 1-21•!1!1 to 2-25---00
l-1.00tol-31.00
3-31..QO to •-27.00
4-27.00 to S-2$--00
S-2$--00 lo 6-30--00
0 6--30-00 lo 7 .26--0()
7•2&-00106-2!1--00
6-29--00 lo 9--25.0Q
!l--2S-OO to 10-26-00
10-26-00to 1-2S-01
D 1-26-01 to ,.20.01
4-20-01 to7-19-01
7-19-01 to 10-18---01
11-6--01 to02..Q8..Q2
5--1-02107-31-02
D B/1/02 to 1 0/31/02
1111.00 lo 1131/0l
2/1/03 to '413Mll
511/03 to 7131/03
1111/03 to 10/31/0l
1111/03 to 1/31/0,t
2/1/0,t to 4/30I04
511104 to 07131/0-4
0713T/04to 10/31/0-4
I 11/01/CM to 01131/05
2/1/0510 04/3Ml5
511/05 to 7131/05
8/1/05to10/31/05
I
TA.BLE6
SUMMARY OF MASS voe REMOVAL ESTIMATES
MACON/DOCKERY SITE
RICHMOND COUNTY, NORTH CAROLINA
I
PAGE 1 OF.t
' Average Total
Flow Volume ror ""° """"' '"""' """'°"""' R:=;:~IKI< CumulaM voes Removed
(gallom) '""" (Pounds) (Pounds)
Ma,-96 400.155 , .. 0.65 0.15S .,, ... 286,151 ~10 0,,0 1.15
May-96 ""' m 0.10 1.25
Jur,..96 97,350 ;,. 0.10 '" Jul-96 163,426 "' 0.15 1.50
A_,.o, 218,330 "" 0'2 '" ,. ... 149,420 , .. 0.35 2.37
Oct96 140,191 , .. 0.33 2.70
Nov-96 438,013 ,.. 1.07 3.77
""""" 161,903 ~ .. , 4.17
Jan-97 29-t,071 ,.. 0.72 <.89
Feb--97 267,596 1,31 '·" 5.18
Mar-97 2S0,068 1_31 0.27 "' A?-97 2711,5M '" 0,0 "' May-97 289,938 78 0.18 5.93
Jun-97 135,575 78 0.09 '" Ju~7 "·"' 78 000 "' Aug-97 70,967 ;. oo, e.11 ,. .. , ,..,., ;. 0.03 6.14
Oct-97 277,505 " 0,12 "' N<:N-97 1-tJ.166 '08 0.13 "' 0.,.0, 78,332 '" 0.07 , ...
Jen-98 103,968 108 0.09 8"
Feb--93 "'·"' ... , ,,, 8.00
Mar-98 326.~s ... , "' "' """ 419,475 99.3 '" 7.<42 ...,.,. .., ... 'l' 0.90 '" Jun-98 200,192 'l' .. , "' Jul-98 337,048 , .. 089 9.42
Aug..98 432,719 14~.4 0.53 9.95
""•" ,tt1,677 1-te.• 0,,0 10,s
""'·" 0!1,378 1~.• 0.5< 10.99
Nov•!l8 "'·"' '" .. , 11-t8
0.,.,0 500,•50 11!1 0.67 12.15 ..... 552,nl6 18,1 0.1, '"' , .... 52,,380 " ,., 1131
Mar.!l!I 81-t,6'1 '! .. , 13.60
Apr-99 571.1'8 " 0" t,t25 ... ,.., 5:14,3,4$ ,,.. 0.81 1,.86
Jun-!l!I ,31,7•2 139,. O.SO 15"
Jul-99 3!12,518 139 .• "' "" "<·" 190,,t07 "! "' '"" "'•" 303,!110 '" "' "" 0099 36-4,211 ,,. "' 1681
Nov-99 277,055 181, 0.,2 17.23
0.,.,0 36!1.9'3 "' 0.5!1 17.62
Joo-00 236,733 '" ,,. 18.18
Feb-00 0 181 0.00 1818 .,.,.,. 176,609 1s1 0.27 18,tS
A,,,·00 16',!11,t 161, 0,, 18.70 -41!1.'1l0 m ,,, "" ,,..., 104.858 n., "' 1901
Jul.OQ 60,000 12.9 0.05 '908 ... .,. 133,575 no 008 19.1'
S.,.00 129,206 no 0.00 19.22
00.00 14ll,'°'4 no "" 19.31
Jnn-01 615,761 '" 0,45 19,76
Apr-01 526,,t27 880: 0.39 20.15 .... , 580,547 101.!I , .. 2(1.!13
Ocl·01 764,060 101.!I "' 21.30 ' ,,.., 529,867 !11.0 0<0 21.70
"''"' 78,922 ,soo 0.10 "00
Qct.O, 101,1,0 150.0 0.1l 21.!ll .... , Sl.345.2 ,so, 0.07 ,,00
""~' 127,6730 150.0 0.16 22,16
Jul-03 60,5160 179.7 0 09 "" ""'~' 1,097,205 4 n11.1l ' .. '"' Jen-0' 681.1!1!1.0 133.3 0.78 2465 ..... 521.9'5.0 133.3 0 S8 ,,,,
Jan-0' 637,264.0 133.3 0.71 25.94 ... " ... "" ' 617,l!e:2,0 ... "'" >m-OS 708.87,t,0 115 0 '" 27.31
Jar,..05 !110,3150 1150! 0.87 28.18
""'"' 508,5580 ... , ,., "" ,...,,. 493,1,460 t "' I' .. , 29 01 '
I I I • I I n u D D I I I I I I I I I I I TABLE 6 SUMMARY OF MASS V~ REMOVAL ESTIMATES S,.,= ...,. Lower Oock&fY Mar-96 ,.,,. ... ....,. .. Jun-96 Jul-96 ,.,,.., Sep-96 ""·" Nov-96 _., Jan-97 Fel>-97 Mar-97 Apr-97 Moy-97 Jun-97 Jul-97 Aug-97 _., Oct-97 Nov-97 0.,.0, Jan-116 Fel>-9'1 Mar-9/1 ...... Mlly-118 J=90 Jul-98 Aug-96 -""" N1111-98 12-1,98 lo 12-31-98 09c•98 12-3 1-118 lo 1.27 .(iO __,, 1-27•99 lo 2-23-99 Feb-99 2-23-99 lo 3--30--a!il ...... 3-~ to -4-29-99 .,,..,. .(..211-~loS-27-Qlil -5-27-99 lo &.2-4-99 Jun-99 &.24-91, to 7.29-99 Jul,99 7-2$-91, to 8-27•99 Aug-99 8-27-1,9 to 9-27,fiO ..... 9-27-99 to 10-29-99 ""·" 10-29-9910 \1-24·99 N1111-99 11-24-9910 12-30-99 0.0.9' 12-30-99 lo t-2M)O Joo-00 t-21--00 to 02-25-00 Fol>-00 3-1--00103-31--00 .. ,-00 3-31-00 lo 4-27-00 ""-00 -4-27-00 lo 5-26--00 -5-26-00 to &.30-00 Jun-00 6-30-00 lo 7-28-00 uoo 7-26-00 lo a.n-oo Aug-00 8-29--00 lo 9-25-00 -9-25-00 lo 10-26--00 Od-00 10-26-00lo 1-:26-01 ... .,,, 1·26-01 lo .(..20-01 ""-0' 4-20-01 to 7-19·01 Jul-01 7-19-01 to 10-18-01 Oct-OJ 11--06-01 to 02,08·02 Jen-02 5-1-02 lo 7-31-02 Jul-02 811/02 to 10/31/02 Od02 1111/021o 1'31/03 Jan-03 1111 /02 lo 3/14/03 Mar-DJ 211/03 to 4/30,'03 ""-03 511 /03 10 713 1 /03 J"-03 6J1/03 lo 10/31/03 Od-03 1111/0310 1131/04 ....... "211 /04 to 3/19/04 .,,..,,. MACON/DOCKERY SITE RICHMOND COUNTY, NORTH CAROLINA PAGE,2 OF 4 Averag•Total Flow Volume r01 voe R:=:!r~ ,.,,., ~ (gellons) ,...._, _ .. , 328,448 "' 0.55 191,090 ,,. "' 245,715 1•'e '"' 8,619 )52 0.01 151,827 )52 0.19 ,,.,,, "' 0.18 63,833 "' 0" 460,379 ,,. "' 183,210 ,,.o,a 0.22 137,594 140.8 0.10 286.202 140,a 03' 90,912 140.8 0.11 m.m "' '·" 180,5&0 ,,4, 0.17 SIU,855 11~ 006 501,987 ))0 "' 581,027 ,,6 0.56 414,199 "I '·" 4111.049 ,., 0.3' 457,1504 :1 '" 308,483 0.16 2n.0111 02 0.14 786,54a ., I '" 123,013 57.9 "" 287,027 57.9, 0" '452,535 57.9 on 141,936 56.0 0" ' 453.014 '" '" "'·"" 56.0 0,. 453,131 62 ,' 023 591,431 "'1 0.31 -471,729 '" 0.2-4 6-42,213 '" 020 -415,550 5261 0.18 361,051 526 0.16 522,107 35 21 0.15 622,1M "·' 0.18 704,292 35.211 02) 581,688 " 023 -427,lilOS ., I 0,17 473,9118 " 0.19 226,628 36,1, '' '" 459,303 311 9 f 0,14 591217 "" 0.18 464,502 ,, 1· 009 «7,951 22 000 503,520 :1 '" 95,167 002 235,556 22 I '" 212,336 " '·" 485,789 ,., I 0.12 382,997 30.3 0.10 500,84SI 303 0.13 284,722 37.5 I 0 09 587,633 37,5 o.u, 512,427 37.5 I 0.16 769,926 "' ,,. 125,989 37.5 I '" 927,723 37,5 0.2' 162,133 37.5 I '" 1,705 37.5 000 5TT.043 37.5 0,16 160,-412 37.5 I 0.05 7,031 37.5 000 10,624 28.7 I 000 513.265 26.7 0.12 1,042,9354 '' I 0 09 218,037.103 " '·" 659,633.5 " I '·" 553,193.290 05 0.03 Cumula!Mt voes RIH'l'MMKI (Pounds) 0.55 "' '" 1.10 '" "' )56 22' "' 2.59 2.93 30< 32' 3.., 4.12 "' 5.17 ,., "" e.12 020 ,., 003 "' 7.03 '" 7.32 rn 1.17 0 00 8.31 8.55 003 90) Q,17 9.32 , ... 9.71 "' 10.11 10.30 10.37 10.51 10.~ 10 78 10,156 10,&5 10,97 11 01 11.05 11.17 11 27 11 40 1149 tU17 11.83 12.07 12.11 1240 12.45 12.45 1263 12.M "" 1268 12.80 12.89 12.91 12.95 12.98 Used October 2000 innuent analybcal data 1o calculate mass removal ostl~al&S for pe<lod of 10,26-00 lo 1-26--01 due to system apem111,mel problems. "Lawer Oock11,y urounclwate, remedilllion system ahut down on 3119/04 f • ✓
I
I S,.=
I Macon Sou<ce AIN
I
I
I
I
I
12-1411 lo 12-31-118 9 \2-31-118 lo 1-27-99
1-27-99 lo 2-23-99
2.23-99 lo 3-30-99
3-30-99 to 4-29-99
0 4-29-99 lo 5-27 -99
5-27-99 lo 6-24-99
8-24-99 to 7-29-99
7 -2!Wlll to &-27 -00
8-27-991D9.27-99
D 9.27-99 lo 10-29-99
10-29-99 lo 11-24-99
11-24-0lllo 12-30-W
12-30-99 to 1-21-00
1-21-00 to 2-25-00
3-1-00 to 3-31-00
l-31-00 lo 4-27-00
4-27--00 to 5-26--00
5-26--00 ID 6--30--00
6-30--00 to 7-21>--00
I 7 .26-0() lo &-2Q.OO
&-29--00 lo !<-25-00
9-25-00 to 10-26-00
10-26-00 lo 1-26--01
1-26--01 lo 4-20--01 I 4-20--01 to 7-19---01
7-19---011010-18--01
11-06-011002--08--02
5-1-02 lo 7-31-02
I 8/1102 to 1001/02
1111/021o1f31/03
1111102 to l/1-4m
2/1!03 lo -4/3DI03
SJ1/03to 7'31/03
I 811/0310 \0131/03
11/1/0310 1'31/04
2/1/04 to 4/30,'IM
511/04 lo 07'31/04
0Ml1/04 lo 1001/04
I 11/01/04 to D1'31/05
02/01A>5 to 04/30I05
511/0510 7'31/05
1111/05to100111)5
I
TABLE 6
SUMMARY OF MASS yQC REMOVAL ESTIMATES
MACON/DOCKERY SITE
RICHMOND COUNTY, NORTH CAROLINA
PAGE 30F 4
IAverege T<ifiil
Fk>wVolume ltK voe Pounds of voe .... ,..,. eo-nm Remowd For Period Cumu'-IMI VOIA Ro,moved ' (gallons) (""'-l """""' _,
Mar-116 428,083 1' 0,0 020 ...... ~.772 " 0.19 0.39
May-96 ~7,720 ., oo, 0'8
Ju,>.96 114,G«I io "" O.S<
Jul-96 202.•11 1' 00, 06' -201,sro I' 0.11 o.n
"'•" 209,649 " 0.11 00,
°"" 101,512 ',' 005 o"
""""" 116,354 42.6 o" '·" 0.0.9' 137,045 42.6 005 0.117
Jan.97 1.e,036 ,2.o 005 "' Feb-97 215,730 "·' 0.11 1.13
Mer..-97 m:= 63_9 0.12 125
Ap,-97 253,167 63.& 0.13 1.38 ...,.1 223,177 "' 0" 1.53
Jun-97 23-4,669 62[ 0.16 1.69 ,,..., 111.ne 'l '·" 1.77
Aug-97 .,, .. 124.9 0 05 1.82 _,, 3626< 124,.9 0.,. '" Od-97 70,207 124.9 007 1.93
Nov-97 102,32e 122,s "' 2.03
0.0.91 114,452 122.5 0.12 2.15
Jan-98 178.387 122.S 0.18 2.33
' , ... ,. 178,387 201.6 "' 2.63
Mar-98 145,521! 201.6 0,. 2.87 ' ...... l!I00,075 201.tl 1.01 '" Mey-98 410,905 139.6 "' <.36
J, ... 431.380 139.6 0 5<> ....
Jul-98 329,!!'.J' TJ!UI "' 5.24 ...,.., 473,093 ''1 , ... "' "'•" 513,MB "' 0'1 "' Oct-98 493,849 "' 0.56 '" •=" 4118,870 203 '"' ,.,
""°" 371,824 ,., 0.83 ...
Jan-99 337,877 203 0.57 "' Fab-99 384,124 "', '60 1063
Mar-99 539,m "' 225 '"' Apr-1111 431,729 ' 499j 1.80 "" ... ,.,, 338,«3 .. , '" 16.11
Jun-99 409,066 .. ,1 1.5<> 17.61
JuJ.-99 502,412 .. , 1.85 '"' -228,824 ,..1 ,.,. 20"
"'•" 820.215 "'I "' 24 42
Qct.89 530,478 566 2.51 '"' ""'" 390,353 5751 1.87 28.80
""°" 543,545 "' 2.61 3141
Jan-00 170,316 5751 062 32.23
"""' 357,840 184.5 055 32.78
Mo,.00 335,782 184.SI 0.52 33 30 ..,..., 331,270 1114.S 0.51 33.61 ... ,..,,, 151.212 154 .I 0.19 "00
Jun-00 300,123 , .. 0.39 34.39
J,f-00 231.991 ,,. I '·"' "" ... ..., 186,494 "" I 0.78 3547
"'•" 84,780 "'' 036 "·" Od-00 180,071 "'' I 0.76 36"
Jan--Ot 526,024 65 0.37 "" ... ~, 261,860 " I 0.19 37.15
Jul--01 220260 527 '·" 38.14
Oct-01 208,250 527 I 0.91 3905
J,.., 120,992 "' "' 39.74
Jul-02 166,455 "' I 052 -40.26
Od.-02 262,381 "' 0.62 41.08
Jan--03 109,119 "' I 0" -41.-42
Mai--03 18,977 '" I 0.0, 41.51 .,,.., &e,452 '" O.,S 42.04
Jul--03 2-4,733 70.9 I 0 01 -42.05
°""' 66,«0.3 709 o" -42.09
J,,,.,. 1,061,901 '" 0 I 1.81 -43.90 .,.,_ 704,057.1 "'' "' 45.20
Jan-Of 1,126.293 "" I 1.92 47.12 ... ,,.,. 912,927 "'·' 1.55 .. .,
Jan--05 848,IM0 160.5 ! 067 -49,54 .,..., 428,952 1110,5 0.57 5<>" ...,.,,, 775,057 105.4 I 06' 50.79
""""' 451,291 '"' ·1! 040 , S1.19
I.
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.,.,_,_,,
I
I
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I 12-1-INlto 12-31-INI
12-31-98 to 1-27-99
1-27-99 to 2-23--99
2-23--99 to 3--30-99
3--30-gg to 4-29-99
I 4-~99 to $-27-99
S-27-99 to 6-24-99
8--24-99 to 7-~99
7-29-UU to 8-27-99
8-27-99 tu 9-27-99
I 9-27-99 to 10-29-99
10-~99 to 11-24-99
11-24-(IQ to 12-3~9
12-30-9910 1-21-00
1-21-00to2-2S---OO
I 3--1-00to:l--31-00
3--31-00 to 4-27-00
4-27 -00 to $-26--00
$-26--00 to 6-30-00
e.-30-00 tu 7-26--00
I 7-26--00 lo 6-29-00
a-~ tu 9-2S-OO
9-2$-00 to 10-26--00
1 0-26--00 to 1-26--01
I 1-26-01 to 4-20-01
4-20-01 to 7-19-01
7-19-01 to 10-16-01
11-06--01 to 02-08-0.2
$-1--02to7-3Ul2
811/02 tu 1001/02
1111/02 to 1 /31 /03
211 l03 to 4/JM)J
5J1A'.l3 tu 7/JMl3
811/00 to 1001/00
D 1111/0310 1/31/04
2J1Al4 to 4/30/04
511,tM to 07131/0'I
OMll/04 to 1001Al4
11 /01 /04 to 01 /31/05
D 02/01/0S to 0413DJOS
511/05 to 7131/05
811/0S to 1001/05
rAeLE6
SUMMARY OF MASS \foe REMOVAL ESTIMATES
MACON/DOCKERY SJTE
RICHMOND couNTY, NORTH CAROLINA
PAGE40F4 ' AV9f8011 Iola
Flow Volume for ,voe
Mornh '""" """'"""""" R:=:~~ CumulatlY9 voes Removed
(gallOl'l!I) ,...,_, (Pounds) (Pounds) ....... 375,318 24,0 008 oo, ,.,._., 709,126 ' 24.0 0.14 0.22 ... , ... ..,,,, 230 0.09 0.31
Jun-96 48,305 31.0 0,01 0.32 ' , ..... 758,920 22.0 0.14 "' Aug-96 638,-400 ,31.0 0.16 oe, ,...., "'·"' 31.0 0.00 0.70
Oct-,0 640,760 31.0 0.17 0.87 ....... 1'71,155 025.3 O.HI '" [),o.96 725,50 2s.3 0.15 1.20
Jan-97 596,131 25.3 0.13 ,.,,
Feb-97 795,239 24.4 0.16 "' Mar-97 1139,710 24.4 0.19 , ..
Apr-97 918,000 24,4 0.19 1.87 ... ,.., 999,040 2,.o 0.20 ,01
Jun-97 605,792 ~•.o 0.12 2.19
-""-" 223,959 24.0 0,0, "' Aug-97 911,679 23.0 0.17 2.40 .... , 917,631 23.o 0.18 '"' Oct-97 821,135 fO 0.16 2.74 ,.,._,, 140,79e 111.0 0,0, 2.76
Dec-97 "'"" 111 0 0,11 2.87 ' ...... 531,1192 16.0 007 '" Fet>-98 1,051,002 22., 0.20 3.14
Mar-9e ,,,, .. 22.9 0.111 3.3'
""''" 662,272 22.9 0.13 3.45
...,.98 876,945 22.3 0.18 3.81
Jun-IN! «8.056 22.3 0.00 3.69 ,,,._,. 776,1~ 22.3 0.14 ,.,
Aug-IN! 857,122 "·' 0.16 3"
Sop-98 921,424 22.5 0.15 4.H
Oct-98 718,543 22.s 0.13 4.27
Nov-9'1 251,141 ,,., 0.03 '30
Dec-96 713.232 1~.s 0.10 uo ...... 8l5,Wt, 16.5 0.11 4,51
Feb-99 586,579 2~.3 0.10 4.61 ... , ... 1,035,1193 20.3 0.18 4.79
""'" 894,763 20.3 0.15 ... -e:28,049 21·.o 0.14 508
Jun-99 809,334 21'.o 0.14 '·" ""' 5e2J10 21;0 0.10 5.3' ,,,,-,,, 8l5,226 11,0 00, "' ..... 768,831 17.0 0.11 '" Oct-99 894,735 11:0 0.13 sos ,_,. 646,405 u,s 0.07 s.n ._,, 575,397 13.5 000 "' ,,o-00 261,658 13.5 0.03 5.61
'""" 161,156 1.ii 0.01 '·" M,,-00 306,952 " 00, 5 ..
.... -00 416,31W 1.8 0.03 5.87
"'"" 127,597 14.8 0,0, "' Jun-00 607,951 14.B 0.o7 '·" """ 425,691 14.8 0.05 B.01 ·-380,931 33.2 0.11 '" Sop-00 919,139 "·' 0.25 6.37
Oct-00 242,990 332 0" ,~ , ... , 200,3'< 33.2 0 06 6 SO
,.,.-0, 145.019 332 oo, '" Jul--01 45-4,18\ ... , 0.18 '" Oct-01 1,966,749 46.5 0.76 7.48 ,..., 7.215.4111 ··1 0,,0 7.74
M-0, 1,300,7l6 .. 0.05 7.79
Od-02 sn.«o .. 0,0,
' 7.81
Jan-03 390,408 12.4 oo, 7.85
Ap-03 2,5,45,412 12.4 0,0 8.11 ,,,,_,, 1,016,735 o.o I 0.00 8.11
Od-03 432,785 00 0.00 8.11
Jen-CM 2,375,008 31 e1 0'3 8.74 , .... 4,041,045 31 61 1.00 '" ,..,,. 1,807,409 31 el o .. 1020 ... , ... 2,645,862 31 61 0.70 10.98
Jan-OS 2.171,719 sos 1.02 12.00 , .... 4.5-47,1191 56,5 l 2.14 14.14 ,,._,,, 3,~.177 474.1 ,,. 15.52 -1,990,745 • 47.4 .-I' 0.79 16.31
II
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Severn Trent Laboratories, Inc.
I
ANALYTICAL REPORT
Job Number: 680-10010-1
Job Description: MacL Dockery
I
For:
lrminger Consulting. Inc.
7015 Erinbrook Drive
Concord, NC 28025
Attention: Mr. Steve,lrminger
Project Manager I
[e-mail]
11/10/2005 ,
STL Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.s«-inc.com
Page 1 of 23
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METHOD SUMMARY
Client: lrminger Consulting, Inc.
Description
Matrix: Alr-Tedlar
Volatile Organic Compounds in Air
Matrix: Water
Volatile Organic Compounds by GC/MS
Purge-and-Trap
Inductively Coupled Plasma -Mass Spectrometry
Acid Digestion of Waters for Total Recoverable or
Residue, Non-Filterable (Gravimetric, Dried at 103-105C)
LAB REFERENCES:
STL-SAV = STL-Savannah
METHOD REFERENCES:
EPA -US Environmental Protection Agency
Lab Location
I
STL-SAV
STL-SAV
I
STL-SAV
STL-SAV
I STL-SAV
Job Number. 680-10010-1
I
Method Preparation Method
Ill
Ill
EPA EPA-18
· SW846 82608 Ill SW846 50306
SW846 6020 Ill
SW846 3005A
MCAWN 160.2
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MCAWN-"Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And 1'
Subsequent Revisions. I
' SW846 -''Test Methods For Evaluating Solid Waste, PhysicaVChemical Methods", Third Edition, November 1986
And Its Updates. I
I
STL Savannah
Page 2 of 23
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Client: lrminger Consulting, Inc.
Lab Sample ID Client Sample ID
680-10010-1 UD Elf
680-10010-2 UMSA Elf
680-10010-3 U/l Macon Eff
680-10010-4 UD Stack
680-10010-5 UMSA S1ack
680-10010-6 U/L Macon Stack
680-10010-7TB Trip Blank
680-10010-8 Property Line
STL Savannah
I SAMPLE SUMMARY
I
Client Matrix
Water
Water
I
Water I
Air -Tedlar Bag
Air. Tedlar Bag'
Air - T edlar Bag
Water •1
Air -Tedlar Bag
I
I Page 3 of 23
Date/Time
Sampled
10/30/2005 0900
10/30/2005 1000
10/30/2005 1100
10/30/2005 0910
10/30/2005 1010
10/30/2005 1110
10/30/2005 0000
10/30/2005 1200
11
iii
iii
Job Number: 680-10010-1
' ,I
Dat~fTime
ReCeived
l'I
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
11/01/2005 0912
ll!
ill
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111
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Client: lrminger Consulting, Inc.
Client Sample ID: UD Ell
Lab Sample ID:
Client Matrix:
680-10010-1
Water
I
'
Analytical Data
:1
Job Number: 680-10010-1
Date Sampled:
Date Received:
111
11
10/30/2005 0900
11/01/2005 0912
"'
82606 Volatile Organic Compound& by GC/MS i\l
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
11/07/2005 2036
11/07/2005 2036
'
Analysis Batch: 680-27663 Instrument ID: GC/MS Volatiles -P
Lab File ID: p1057.d :11
Initial WeighWolume: 5 ml
Final WeighWolume: 15 ml II ,,
I
' iii
RL Analyte --·······---· -·· ........ Result (ug/L) I Qualifier ·-·--·· ........... ···· ···· 10 --····1-··-·-u···•····-·----·---·--··-·--------··-···:;·ci··· Acetone
Benzene
Chloroform
1, 1-Dichloroethane
1,2-Dichloroethene, Total
1, 1-Dichloroethene
Methylene Chloride
T etrachloroethene
Toluene
1, 1, 1-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
STL Savannah
1.0 u 'io
1.0 U ,1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
3.0
I
Page 4 of 23
'
I
u
u u
u
u
u
u
u
u
u
,J.0
iJ-0
,1.0
2.0
1.0
1.0 i.o
1 .0
1, 0
3.0
I
Acceptance li~its
. 77-120 11.
75 • 123
79 -122
I~ ,,
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Client: lrminger ConsuHing, Inc.
Client Sample ID: UMSA Eff
Lab Sample ID:
Client Matrix:
680-10010-2
Water
I
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II
'I
I'
ii
Analytical Data
1:1 Job Number: 680-10010-1
II
I
Date Sampled:
Date Received:
10/30/2005 1000
"' 11/01/2005 0912 II
8260B Volatile Organic Compounds by GC/MS II
:1
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
82608
50308
1.0
11/07/2005 2105
11/07/2005 2105
Analyte ............ _ ----· _ .............. -. ________ . ., ..
Benzene
Acetone
Chloroform
1, 1-Dlchloroethane
1,2-0ichloroethene, Total
1, 1-Dichloroethene
Methylene Chloride
Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
Analysis Batch: 680-27i3
Result_(uil"\-)
1.0
10
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
3.0
%Rec ... ··-·· .......... ,, .. -·---·········-··•-·--·-----------«--• ---4-Bromofluorobenzene
Dlbromofluoromethane
Toluene-dB
STL Savannah
102
99
101
I
Page 5 of 23
Instrument ID: GC/MS Vola1iles -P
Lab File ID: p1059.d II
Initial WeighWolume: 1~ ml
Final WeighWolume: 5 ml
ij
Qualifier RL
U 1.0
u 10
u 1.0
U ).0
U 1.0 u i.o
U 2.0
u j.o
U 1.0 u 1.o
U 1,.0
U 1.0
U 3.0
11 Acceptance Limits · -· -·-· ----·---ii---,20--, ............ ..
75-123 ',,
79-122 l!I
11
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Client lrminger Consulting. Inc.
Client Sample 10: U/L Macon Eff
Lab Sample ID:
Client Matrix:
680-10010-3
Water
i
' I
j'
~nalytical Data !i
Jab Number: 680-10010-1
II
I
Date Sampled:
Date Received:
10/30/2005 1100
"' 1110112005 0912 "
8260B Volatlle Organic Compound& by GCfMS
I
" II
Method: 82608
50308
1.0
Analysis Batch: 680-27663
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
11/07/2005 2133
11/07/2005 2133
Analyle ____ . ···---·-·-•·---·-······--· -·-··-.... R_es_ult(ugl~)
Benzene 1.0
Acetone 10
Chlorofonn 1.0
1, 1-Dichloroethane 1. O
1,2-Dichloraethene, Total 1.0
1,1-0ichloroethene 1.0
Methylene Chloride 2.0
Tetrachloroethene 1.0
Toluene 1.0
1, 1, 1 ·Trichloroethane 1. 0
Trichloroethene 1.0
Vinyl chloride 1. 0
Xylenes, Total 3.0
I·
Instrument ID: GC/MS Volatiles· P
Lab FIie ID: p1061.d (!
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
I
111
Qualifier RL
u
u
u
u
u
u
u
u u
u
u
u
u
1.0 io
i.o
1.0
1.0
i.o
2.0
J..O
1.0
Surrogate _______ --.............. -
f.o
1.0
11.o
:i'.o
::i %Rec Acceptance Limits
4--Bromofluorobenzene
Dlbromofluoromethane
Toluene-dB
STL Savannah
. ~~~ -·l··--·. ·-· --·-· --. t~: ~~~. f
100 79 -122
I
I
Page 6 of 23
!i]
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Client: lrminger Consulting, Inc.
Client Sample ID: T~p Blank
Lab Sample ID: 680-10010-HB
Client Matrix: Water
"
111
·.I
II
:11 Analytical Data 'i
'" Job Number. 680-10010-1 !I
ii
Date Sampled: 10/30/2005 0000
Date Received: 1110112005 0912
Ci
82606 Volatlle Organic Compounds by GC/MS
I Iii
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
8260B
5030B
1.0
1110712005 1939
11/07/2005 1939
Analyt~ ··-·· ····----····-.. --··--·-·-··· ... Benzene
Acetone
Chloroform
1, 1-Dichloroathane
1,2-Dichtoroethene, Total
1, 1-Dichloroethene
Methylene Chloride
Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
T richloroethene
Vinyl chloride
Xylenes, Total
Analysis Batch: 680-27663
I
I
Resutt (ug/L)
Instrument ID: GC/MS Volatiles -P
Lab File ID: p1053.d ii
Initial WeighWolume: 5 ml
Final WeighWo!ume: 5 ml
l'I
111
Qualifier RL ·-· --·--·-··---·1 ......... _ .. _·--····---·······-·-·--··-······· ·. . ........ . 1.0 U ).-0
10 U 1,0
;g ! ~ jg
1~ U 1.0
1.0 I u 1o
2~ u io
;! I ~ }g
1.0 U 1'.0
I I 1.0 U 1.0
1.0 u {o
ll U ll
11
1 Acceptance Limits ·· ·1 --··-···-n-120 II · Surrogate-·-·-··-·--······--··-..... __ ,_ .... __ ... ____ ··--·--·-·---·%~-~:_.
4-Bromofluorobenzene 104
Dlbromofluoromethane 103
Toluene-dB 100
I
1·
I
I
STL Savannah Page 7 of 23
I
75-123
11
.1
79-122 'I
11 ,,
Ill
'
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D
D
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I
I
I
Client lrminger Consulting, Inc.
Client Sample ID: UO Stack
Lab Sample ID:
Client Matrix:
Method:
Preparauon:
Dilution:
680--10010-4
Air-Tedlar
EPA·18
N/A
1.0
EPA-18 Volatile Organic Compotiflds In Air
I
Analysis Batch: 680--27140
i
Date Anatyzed:
Date Prepared:
11/01/2005 1807
NIA I
I
Analytical Data
111
Job Number: 680-10010-1
:11
Date Sampled:
Date Received:
10/30/2005 0910
'" 11101/2005 0912
"
I! Instrument ID: GC/MS Volatiles -B
Lab File ID: b1084.d ii
lniual WeighWolume: 5 ml
Final WeighWolume: 5 ml
Injection Volume: l!I
Analyte --·-·•· .. ·····-··-···-·····-····--·-................ ___ Result (mg/m3) ..... _ ()~a!i~".'
Chloroform
cls-1,2-Dichloroethene
trans-1,2-Dichloroethene
Toluene
Trtchloroethene
STL Savannah
1.0
1.0
1.0
1.0
1.0
I
I
I
Page 8 of 23
I
u
u
u
u
u
111
I
Ill ,,
1i
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'
Ill
11
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Client: lrminger Consulting, Inc.
Client Sample ID: UMSA Stack
Lab Sample ID: 680-10010-5
Client Matrix: Air -T edlar
Method:
Preparation:
Dilution:
EPA-18
N/A
1.0
EPA-18 Volatile Organic CompoJnds in Air ,,
Analysis Batch: 680-27140
I
Date Analyzed:
Date Prepared:
11/01/2005 1829
N/A
I!
II
1i1
i1~I
r.1 A1 nalytical Data
I'
"' Job Number. 680-10010-1
!'I
:1
111
Date Sampled:
Date Received:
10/30/2005 1010 " 11/01/2005 0912
"' 1'1
111 ,,
lnstrumenl ID: GC/MS Volatiles • B
''I Lab File 10: b1085.d II
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Injection Volume: 11
1
'" i1
iii
Analyte -·····-----... ________________ ., ____ ----------___________ ... Result (mg/m3/ Qualifier RL
Chloroform 1.0
cls-1,2-Dlchloroethene
trans-1,2-Dichloroethene
Toluene
Trichloroethane
STL Savannah
1.0
1.0
1.0
1.0
Page 9 of 23
u
u
u
u
u
11.o
110
1'!!0
"I 1.0
{o
II "I
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n
D
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I
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I
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I
I
Client: lrminger Consulting, Inc.
Client Sample 10: U/L Macon Stack
Lab Sample 10: 680-10010-6
Client Matrix: Air -Tedlar
I
I
I
Ii
II
1']
ti\
Analytical Data
11
Job Number: 680-10010-1
'I
Date Sampled:
Date Received:
1i'1
11
1 0130/2005 1110
1110·112005 0912
"'
EPA-18 Volatile Organic Compounds In Air 1,1
'I Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
EPA-18
NIA
1.0
11102/2005 0037
NIA
cls-1,2-Dlchloroethene
trans-1,2-Dichloroethene
Toluene
Trichloroethane
STL Savannah
I
Analysis Batch: 680-271,40 Instrument ID: GCIMS Volatiles -B
Lab File ID: b1090.d ti
Jnrtial WeighWolume: 5 ml
Fined WeighWolume: 5 ml
Injection Volume: lfl
111
I I
Result (mglm3)t Qualifier ~L
1.0 I - U .-. 1''.0 -
10 U ~
1.0 I U 1''.o
1.0 1· u lo
1.0 I u 1110
I
I
Page 10 of 23
"I
jt
'I
111
•1
'I
111
II
!,\
11
':\
:1
"I
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I
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I
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I
I
I
Client lrminger Consulting, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Property Line
680-10010-8
Air-Tedlar
EPA-18 Volatile Organic Compounds In Air
I
EPA-18
NIA
1 0
11102/2005 0059
NIA
Analysis Batch: 680-27140
fl l'I
''I
"I 11
i!
" "I ,, .
Analytical Data
~.I Job Number: 680-10010-1
Date Sampled:
Date Received:
,,
"I ,1 ,,,
it'1
10/30/2005 1200
11101/2005 0912 ,:
11
''I 11 Instrument 10: GCIMS Volatiles • B
Lab File ID: b1091.d 11;\
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
"' Injection Volume: 111
"I ,,,
I
' An~ltte ···-· -·· --·--· . -·•····· ·--··· ... ·-··· _ ........ ____ Resutt (mgtrn3)1 •••• 9~_ali~".'._ .. __ ........ .
11 RL
Chlorofonm 1 0 1
. I
cis-1,2-Diehloroethene
trans-1,2-Dichloroethene
Toluene
Trichloroethene
STL Savannah
1.0 I
1.0
1.0
1.0
Page 11 of23
u
u
u
u
u
' I·
I
11'.o
1!0
1''0
1\'o
1 IQ ,,
1,:1
"I " 11'1
i,
•Ii
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11'1
"I
"I NI
ill
::1 II ,,,
'11°1
"' ,,
''\ " ,,,
'1:\
'" 111
:1
''I "I
"' l'i
"I ''I "I "I
"' ,1'1
111
"I ,I
Iii
1/1
:1
"I ''I ,,,
'I ''I ,,
,,,
''I
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Client: lrminger Consulting, Inc.
Client Sample 10: UD Elf
Lab Sample ID: 680-10010-1
Client Matrix: Water
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Lead
Vanadium
Zinc
STL Savannah
6020
3005A
1.0
11/0512005 1717
11/0312005 1234
\11
1:\
11\
i11
\I ~nalytical Data
'I
11 Job Number: 680-10010-1
"I
Date Sampled:
Date Received:
111 ,1
1:1
111
10/3012005 0900
11/0112005 0912
6020 Inductively Coupled Plas~~ -Mass Spectrometry 111
11'1 ,1 I
Analysis Batch: 680-27650
Prep Batch: 680-27224 :
Result (ug/L)
75
0.50
0.30
14
5.0
3.4
1.5
5.0
20
Page 12 of 23
I
I,
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
'" IC;P MS
N/A
50 ml
250 ml
1;1
"I II
Ill ltRL
'" (\5.o ·
~p.50
IIQ.30 ;.·~.o
15.0
11.0 II 111,5
5.0
20
:1
111
111
11
1
"I
!1\
111
'I 111
111
"' •'1
,11
"I
111
111
"I
"'1
\
11
i1
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,11
111
,11
111
,11
"I
11
111 11
::1
i11 ,,
111
11'1
111
~11
Ii Ill
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,,1
1_11
,11
,11
111
Ill
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Client: lnninger Consulting, Inc.
Client Sample ID: UMSA Elf
Leb Sample ID:
Client Matrix:
Method:
Preparation:
DIiution:
Date Analyzed:
Date Prepared:
Analyte
Barium
Beiyllium
Cadmium
Chromium
Manganese
Nickel
Lead
Vanadium
Zinc
STL Savannah
680-10010-2
Water
6020
3005A
1.0
11/05/2005 1753
11/03/2005 1234
~ 11
111
''I
:•1
'trnalytical Data
1•1
Job Number: 680-10010-1
Dete Sampled:
Date Received:
6020 Inductively Coupled Plasma -Mass Spectrometry
I
' Analysis Batch: 680-27650
Prep Batch: 680-27224
Result (ug/L)
150
0.50
0.30
5.0
8.2
8.7
1.5
5.0
20
Page 13 of 23
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
11\
;1
l'I 10/30/2005 1000
11/01/2005 0912
111
11\
ICPMS
NIA 50 ml
z5() ml
" 11
1
•1
111
11RL •••• r:.""•~•• • • ••• -••• ••»••••-S••
,1ls o
10:50
1;,030
i,~.O
1~.o
1,,.0
11.5
5.0 Io
,11
"I
:1
111
11]
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Ill ,I
,,1
i1 ,11
111
·:1 II
:1'1
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,11
111
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,11
,:1
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Client: lrminger Consulting, Inc.
Client Sample ID: U/L Macon Eff
Lab Sample ID:
Client Matrix:
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Lead
Vanadium
Zinc
STL Savannah
680-10010-3
Water
6020
3005A
1.0
11/0512005 1800
11 /0312005 1234
rl l'i
!1
1
''I
\\ I' ~nalytical Data l'I
'" Job Number: 680-10010-1
Date Sampled:
Date Received:
6020 Inductively Coupled Plasma -Mass Spectrometry
'
Analysis Batch: 68()..276~0
Prep Batch: 680-27224
Resull (ug/L) ,
37
0.50
0.30
5.0
5.0
1.3
1.5
5.0
20
I'
Page 14 of 23
Instrument ID:
Lab File ID:
Initial Weig~Wolume:
Final WeighWolume:
Qualifier
u
u
u
u
u u u
11\
!!I
l'.i
1 013012005 1100
11/01/2005 0912
:1 II
1qPMS
~/A
50 ml
250 ml "I
"I
'" ' ''I 111RL ,,,
115_0 ·
''I 1,,0.50
!i10.30
1>15.0
,5.0
'110 11,1.5
il5_0
1'20 I''
''I
''I "I ,,,
Ii
:I !I
111
l'I
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n
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I
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Client: lrminger Consulting, Inc.
Client Sample ID: UD Ell
Lab Sample ID: 680-10010-1
Client Matrix: Water
Analyte Result
Total Suspended Solids 5.0
Anly Batch: 680-27106
Client Sample ID: UMSA Ell
Lab Sample ID: 680·10010-2
Cllent Matrix: Water
Analyte Result
Total Suspended Solids 5.0
Anly Batch: 680-27106
Client Sample ID: U/L Macon Ell
Lab Sample ID: 680-10010-3
Client Matrix: Water
Analyte Result
Total Suspended Solids 5.0
Anly Batch: 680-27106
STL Savannah
I
I•
I
I
I General Chemistry
I
Qual Units
U mg/L I Date Analyzed 11101/2005 1410 I
Qual Units
U mg/L
Date Analyzed 11/0112005 141 0
I
Qual Units
U mg/L
DateAnalyzed 11/01/2005 1410
Page 15 of 23
\\
111 'j
lnalytical Data
iii Job Number: 680-10010-1
'I
Date Sampled:
Date Received:
RL
5.0
Dete Sampled:
Date Received:
RL
5.0
Date Sampled:
Date Received:
RL
5.0
111
1'1
111
1;1
1 p130/2005 0900
111/01/2005 0912
111 Dil,
1 91
111
''I Ill
' ''I
,1
Method
160.2
10130/2005 1000
11/01/2005 0912
:,1
Dil 1'.I Method
1 0 ,/1 160.2
111
"I
''I II ,i
10/3012005 1100
11I01/2005 0912
'I
111
Di! 11I
,.a :1r
11
i1
111
111
\1
,II
' ,11
11
111
j
Method
160.2
11
1
1
1
,1
Ii
,11
"I
·:1
,11
1i1
II
,11
' ill
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Ill
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Client: lrminger Consulting, Inc.
Lab Section Qualifier
GC/MSVOA
u
Air Toxics
u
Metals
u
General Chemistry
u
STL Savannah
\I
ill 'I
i DATA REPORTING1QUALIFIERS
111
iii
111
I
I
Description 1
111
Job Number: 680-10010-1
"I
11
111
11
1i1
111
111
'
Analyte was not detected at or above the reporting 1h1it.
I I
I·
i ~ Analyte was not detected at or above the reporting limit.
I l'I
,1'1
I 111
Analyte was not detected al or above the reporting li~it. 'I
!1
ii
I ' Analyte was not detected at or above the reporting lirilit.
Page 16 of 23
''I
11'1
111
'I
,11
I
111
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Iii
'I
111
11
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1i1
II
,1
111
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I
g
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I
I
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Client: lrrninger Consulting, Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds by GCIMS
Client Matrix: Water
Lab Sample ID Client Samele
LCS 680-27663115 LCS
MB 660-27663/16 MB
680-10010-1
680-10010-2
680-10010-3
680-10010-7TB
Surrogate
(BFB)
(DBFM)
(TOL)
STL Savannah
UD Eff
UMSA Eff
U/L Macon Eff
Trip Blank
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB
(BFB) (DBFM) (TOL)
(¾Rec) (%Rec) (¾Rec)
108 98 94
109 99 96
I
103 102 101
I
102 99 101
I
' 102 101 100 ' ' 104 10_3 100
I
Acceptance Limits
77 -120
75 -123
79 -122
I·
Page 17 of 23
rl
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' II
Quality Control Results
~ i, Job Number 680-10010-1
fl ~I
1i1
Ill
i!\
,11
'I
l'I
11,
111
"I
I"
111 Ill
•!
~I
"I
111
11'1
"I
111
"I ,,
111
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1
1.1
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,11
i1
11
:11 ,,
,11
111
ill
i1
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11'1
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,11
111
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Client: lrminger Consulting, Inc.
Method Blank -Batch: 680-27663
Lab Sample ID: MB 680-27663/16
Client Matrix:
Dilution:
Date Analyzed:
Water
1.0
11/07/2005 1303
Date Prepared: 11/07/2005 1303
Analyte
-···-~---····-----•---•··-" Acetone
Benzene
Chloroform
1, 1-Dichloroethane
1,2-Dichloroethene, Total
1, 1-Dichloroethene
Methylene Chloride
T etrachloroethene
Toluene
1, 1, 1-Trichloroethane
T richloroethene
Vinyl chloride
Xylenes, Total
Su rrog,a~: .. _ ·-~ ·-·-· __ ,. _ . . ,. . ,.
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB
Analysis Batch: 680-27663
Prep Batch: NIA I
Units: ug/L
Result
10
1.0
1.0
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
3.0
. -·· 1, ..... _ • .,
Oual
u
u u
u
u
u
u
u
u u
u
u
u
11
,I
n1
:1
Quality Control Results
111
Job Number: 680-10010-1
1,
ii'1
Method: 82608 111
Preparation: 5030B
!I Instrument ID: GCIMS Vola~les -P
Lab Fite ID: pq6011d
Initial WeighWolume1!1 5 ml
Final WeighWolume:\[ 5 m L
)i
i
iii
_)I ____ R~--
I1[ 10
''I 1.0
111 1.0
111 1.0 1.0
'I 1.0
11, 2.0
11 : ~
l'I 1.0
I 1.0
!I 1.0
11 3.0 i,
% Rec Acceptance Limns 111 --i~----: ------------___ .... ·tr~if ---·11 -
96 19 -122 111
,11
'I
!'I
111
''I
''I
111
II ,1
''I
11
11
!'I [II
Ii
1!
Calculations are performed before rounding to avokl round-off errors in calc!,Jlaled results.
STL Savannah ' Page 18 of 23
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I
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I
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Client: lrminger Consulting, Inc.
Laboratory Control Sample -Batch: 680-27663
Lab Sample ID: LCS 680-27663/15
Client Matrix:
DIiution:
Date Analyzed:
Date Prepared:
Analyte
Benzene
Acetone
Chloroform
Water
1.0
11107/2005 1112
11107/2005 1112
1, 1-0ichloroethane
1,2-Dichloroethene, Total
1, 1-Dichloroethene
Methylene Chloride
Tetrachloroethene
Toluene
1, 1, 1-Trichloroethane
T richloroethene
Vinyl chloride
Xylenes, Total
Analysis Batch: 680-27663
Prep Batch: NIA I
Units: ug/L I
Spike Amount Result
50.0 45 I
100 100 I
50.0 48 I
50.0 50
100 98 I
50.0 50
50.0 53
50.0 52
50.0
50.0
50.0
50.0
150
47
47 I
78
51
100 I
I
it
ill
II
11
Quality ~ontrol Results
II ,,
Job Number: 680-10010-1 II
II
Method: 8260B :\
Preparation: 5030B
111
m Instrument ID: GCIMS Volatiles -P
Lab FIie ID: pq595!1d
Initial WeighWolumel'] 5 mL
Final WeighWolume:i1s ml
II
%Rec. Limit
1/1
1
1
1 Dual
90
101
95
gg
98
100
106
103
93
94
156
103
106
. . 74 -122 11 . .
20-183 I
74 -124
70-127 I
70-130 I'
54.132 i,
67-128 111
70 -133
75 -122 111
70-132 I
75-122 11
59-136 111
77 -121 ,
111
111
111
11
11
!1
II
Ii
I
,,I
Calculations are performed before rounding to avoid round-off errors in calculated results.
STL Savannah
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Page 19 of 23
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Client: lrminger Consulting, Inc.
Method Blank -Batch: 680-27140
Lab Sample ID: MB 680-27140/2
Client Matrix: Air -T edlar Bag
Dilution: 1.0
Date Analyzed: 11/01/2005 1644
Date Prepared: NIA
Analyte
·-•······-·----·-·-···---.-••-·~·-···-· -·---· ·--Chlorofonn
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
Toluene
T richloroethene
I:
I Analysis Batch: 680-?7140
Prep Batch: N/A
Units: mg/m3
Result
1.0
1.0
1.0
1.0
1.0
Laboratory Control/
Laboratory Control Duplicate Recovery Report -Batch: 680\27140
LCS Lab Sample ID: LCS 680-27140/3
Client Matrix:
Dilution:
Date Analyzed:
Data Prapar8d:
Air -T edlar Bag
1.0
11101/2005 1724
NIA
LCSD Lab Sample ID: LCSD 680-27140/4
Client Matrix: Air -T edlar Bag
Dilution: 1.0
DateAnalyzed: 11/01/2005 1745
Date Prepared: N/A
Analysis Batch: 680-27140
Prep Batch: N/A I
Units: mg/m3
Analysis Batch:
Prep Batch: N/A
Units: mg/m3
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,,
I
680-27140
I
Qual
u u
u
u
u
II
11
:1
11
Quality Control Results
llj
Job Nur\\ber: 680-10010-1
111
111
Method: EPA-18 i]
Preparation: NIA :1
it,
Instrument ID: GC/MS Volatiles - B
Lab File ID: bq0341d
Initial WeighWoluml 5 ml
Final WeighWolume~·l1 5 ml
Injection Volume: Ill
111
11
1 RL ,,, · · j ·-ut ··-·· ~ ·--·
, 1.0
111 1.0
1! 1.0
111 1.0
Method: EPA-18 1
,::
Preparation: N/A 111
,1
11,
Instrument ID: GCIMS1)iolatiles -B
Lab File ID: bq035.d
Initial VVeighWolume: ~15 ml
Final WeighWolume: 11! 5 ml
Injection Volume· 11
:1\
Instrument ID: GC/MS Volatiles -B
Lab FIie ID: bq036.d lt'I
Initial WeighWolume: ~I ml
Final WeighWolume: 5[ ml
Injection Volume: ;i'1
11
ii Analyte
Toluene
Trichloroethane
LCS
92
102
~
LCSD Limit RPO RPD Limit LCS,ilual LCSD Qual ······--·-·--·•·-····---------•--·•·---··-·--·· 87
97
60,-140
60-140
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I
6
4
Calculations are performed before rounding to avoid round-off errors in calculated results.
[·
STL Savannah Page 20 of 23
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30
30
11!
111
111
111
it'1
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11
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Client: lrminger Consulting. Inc.
Method Blank. Batch: 680-27224
Lab Sample ID: MB 680-27224I12-A
Client Matrix:
Dilution:
Date Analyzed:
Water
1.0
11105/2005 1656
Date Prepared: 11/03/2005 1234
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Analysis Batch: 680-27650
Prep Batch: 680-27224
Units: ug/L I
Result Qual
'I
)]
111
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II
Quality Control Results
1I Job Number: 680-10010-1
11
Method: 6020 '1
Preparation: 3005A
'I
\1 Instrument ID: ICP MS
I lab File ID: NIA Ii
Initial WeighWolume: 50 ml
Final WeighWolume'' 250 ml ,.,
'
111 RL Analyte
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
,--··-·---·---·-------·-·--·-·--··--·-·-.. --.-· .. ·.,--.--.-·--·----··
Lead
Vanadium
Zinc
5,0 U
0.50 U
0.30 U
5.0
5.0
1.0
1.5
5.0
20 I
u
u
u u
u
u
Laboratory Control Sample • Batch: 680-27224
Lab Sample ID: LCS 680-27224/13-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 11105/2005 1703
Oat~ Pr-QparQCf: 11/03./2005 1234
Analyte
I Analysis Batch: 680-27650
Prep Batch: 680-27221
Units:ug/L
I'
Spike Amount
-----·-·--·-· ··-----• ··"•->•• •·••• .•• -··---~· ·--·· ·-·····~ ., ·--------·-.. --····--.. Barium 200 180 I
Beryllium 50.0 47
Cadmium 50.0 46
Chromium 200 180
Manganese 500 480
Nickel 200 190
Lead 50.0 48
Vanadium 200 180
Zinc 200 100
,1 5.0
11 ~~~
I 5,Q Ii 5.o l 1.0 ,I 1.5
5.0
111 20
111 Method: 6020 ,,
Preparation: 3005A 'I
II Instrument ID: ICP MS
Lab File ID: NIA Ii[
Initial WeightNolume: ;~o ml
Final WeighWolume: 250 ml
1/1
% Rec. Umit j
88
95
92
92
97
95
96
91
00
75 -125 1'1 ,,
75 -125 II 75 -125
75 -125
75 -125
75 -125
75 -125
'I
11!
75 -125 111 75 -125
'I
!I]
Ii[
1
11
l1i
Calculations are performed before rounding to avoid round-off errors in ca!culated results. !11
STL Savannah Page 21 of 23
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Client: lnninger Consulting, Inc.
Matrix Spike/
iii
Quality Control Results
1:1
' Job Number: 680-10010-1
Ill
Matrix Spike Duplicate Recovery Report • Batch: 680-27224 I
Method: 6020 !i
Preparation: 3005A
II
MS Lab Sample ID: 680-10010-1
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepar&d:
1.0
11/05/2005 1739
11103/2005 1234
MSD Lab Sample ID: 680-10010-1
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte ..... ____ ..
Barium
Beryllium
Cadmium
Chromium
Manganese
Nickel
Lead
Vanadium
Zinc
Water
1.0
11/05/2005 1746
11/03/2005 1234
Analysis Batch: 680-27650
Prep Batch: 680-27~24
Analysis Batch: 680-27650
Prep Balch: 680-27i;24
% Rec.
MS MSD
I
Limit
!i
Instrument ID: ICPi1'MS
Lab File ID: NIA f
Initial Weight/Velum~: 50 ml
Final WeighWolum8': 250 ml
111
'
Instrument ID: ICP rJls
lab File ID: N/A ,1
Initial WeighWolume: 50 ml
Final WeighWolumJ! 250 ml
11
11
RPO RPO Limit MS Qual MSD Qual
90 . 86 . 75-125 3 20 . 11·· ..... .. .... ---..
98 96 7,5 -125 3 20 ij'
95 91 75 -125 5 20 I
95 90 75-125 5 20
98
97
98
93
100
94
92
94
90
96
75. 125
' 75 -125 ' 75 -125
75 -125
75 -125
I
I
I
3
4
4
4
4
20
20
20
20
20
.i
ii
1!
ill
"i
ii ,I
I\
ii
11
'
iii
Calculations are performed before rounding to avoid round-off errors in ~lculated results.
iii
11
STL Savannah Page 22 of23
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Client: lrminger Consulting, Inc.
Method Blank· Batch: 680-27106
Lab Sample ID: MB 680-27106/1
Client Matrix:
Dilution:
Date Analyzed:
water
1.0
11101/2005 1410
Date Prepared: NIA
Analysis Batch: 680127105
Prep Batch: N/A '
Units: mg/L I
I
Qual
Ii
ii[
Quality Control Results
II Job Number: 680-10010-1
II
I
Method: 160.2 HI
Preparation: NIAii
Instrument ID: No Etuipment Assigned
Lab File ID: NIA Ii
Initial WeighWo!ume: 200 ml
Final WeighWolum61
: 200 ml
i
I RL
·1'1 5.0 . --
Laboratory Control Sample -Batch: 680-27106 Method: 160.2 j
Lab Sample ID: LCS 680-27106/2
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Water
1.0
11/01/2005 1410
NIA
Total Suspended Solids
Preparation: Ni A I
I
Analysis Batch: 680-27106 Instrument ID: No Etipment Assigned
Prep Batch: NIA
Units:mg/L
Spike Amount
Lab File ID: NIA Ii
Initial WeighWolume: 100 ml
Final WeighWolume:' 100 ml
Ii
Result % Rec. Limit 11'
' ' Qual
-'100 ___ . 99 99 80-120·11 - -----.. --
1
II
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Iii ,,
I
111
I' I
I
Calculations are performed before rounding to avoid round-off errors in calculated results.
111 I
11
!
STL Savannah Page 23 of 23
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iliiil - - -------iiiil iiiiiil liiiil liiiiiil liiiil
Serial Number 6 U 7 4 7
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ~ STL Savannah Website: www.stl-inc.com
Phone: [phone]
Fax: 19121352-0165
•
PROJECT REFERENCE
STL ILABI PROJECT MANAGER
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STL
PROJECT NO. I C)0(::-'1-r1,, 1
P.O. NUMBER
PROJECT LOCATtoN MATRIX
(STATE) IJ/· · TYPE ' -.• -
i,
.... _
c'
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v
V
5102 LaRoche Avenue
Savannah, GA 31404
C) Alternate Laboratory Name/location
REQUIRED P.NALYSIS
f2·, ,-t,) 0 -· 1..--J ' ' CJ' <;,'1) D e ' :;-~) )'-j · -Isl '=?. ·-,?'.{ ,f) ;;4 r: •O
<i: ...-:: • L_ ~ '?.. 4-1"'' r-
~-~ \1 ··.:~ _, ' < .. ,
IJ.;J ~-' " U}
NUMBER OF CONTA!'IERS SUBMITTED
? 2. i i ,_, ' 2. '? \ ' ,.~ '.
-2. ,.-~ \--I t -G,~-\·
'' l--) +--·
Phone:
Fax:
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1h.1 ?{,~'") lo. lJ( .. \ (?.tJL'/ 1
• -'?'!=.·I-=""'=-=---=-::..--~ c..__-== ===-=--....., ----~~ ~,-~ -~-~=~~ -----
RELINQUISHED BY: !SIGNATURE) DATE TIME RELINQUISHED BY: !SIGNA~D
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