NCD980840409_20041210_Charles Macon Lagoon Drum_FRBCERCLA RA_Quarterly Progress and O & M Report August - October 2004-OCR

I
I
I
I
Macon/Dockery Site
Richmond County, North Carolina
Reply to: Technical Commitlc-c
c/o Ken Gulledge
Crown, Cork & Seal Company, Inc.
P.O. Box 887
Cheraw, SC 29520
Phone: [phone]
Fax: [phone] I December I 0, 2004
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Ms. Giezelle S. Bennett
Remedial Project Manager
United States Environmental Protection Agency, Region IV
61 Forsyth Street, S. W.
Atlanta, Georgia 30303-3104
Re: Progress and O&M Report of Quarterly Activities
August I, 2004, through October 31, 2004
Macon/Dockery Site -Cordova, North Carolina
IC Project No. 0004-00ltm
Dear Ms. Bennett:
r {BJ & @ m a w &Jni
lfDJ DEC 2"3 2004 ~j
SUPERFUND SECTION
On behalf of the Macon/Dockery Site Group (MDSG), the Progress and O&M Report of
Quarterly Activities for August I, 2004, through October 31, 2004, is herewith submitted in
accordance with SECTION XV -PROGRESS REPORTS of the Unilateral Administrative Order
(effective date -June 30, 1992) for the Macon/Dockery Site. The report includes the provisions
included in the recommendations section of the United States Environmental Protection Agency
(USEPA) -Region JV Five Year Review Report dated September 2000. In addition, this report
includes the tasks required in the US EPA letter dated March I 6, 2004, regarding groundwater
sampling at the Lower Dockery system.
This report describes activities, which occurred during the period August I, 2004, through
October 31, 2004, as part of the Remedial Action phase of this project. This report describes the
operational status of the groundwater remediation systems and the results of the quarterly system
effluent sampling event conducted for the period.
PROJECT TASKS INITIATED OR COMPLETED THROUGH OCTOBER 31, 2004:
•
•
•
Weekly operation and maintenance of the systems;
Quarterly effluent sampling of the remediation systems; and,
Quarterly sampling of Lower Dockery monitoring wells MW-16 and MW-24 .
RESULTS OF SAMPLING AND TESTING AND OTHER DATA RECEIVED:
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Ms. Giezelle Bennett
December I 0, 2004
Page No. 2
A copy of the laboratory reports and chain-of-custody records for the quarterly water effluent
sampling of the remediation systems and groundwater samples collected from wells MW-16 and MW-
24 are included in Appendix A. Tables 1 through 4 summarize the water effluent analytical results
for the four groundwater remediation systems. The effluent concentrations for the collected
groundwater samples were below the Remediation Performance Standard except for the following
parameters:
Sample Location Parameter Result (ug/L) Remediation PS
lu!!/Ll
Upper/Lower I, 1-Dichloroethene 8.5 7
Macon
Upper/Lower Tetrachloroethene 1.3 I
Macon
ug/L -micrograms per liter PS -Performance Standard
The Macon System effluent exceedances for 1, 1-Dichloroethene (I, 1-DCE) and
tetrachloroethene (PCE), are being investigated. The following diagnostic and preventative steps will
be conducted prior to the January effluent sampling event:
I. Airflow at the airstripper stack will be measured to verify that the air to water ratio for the
airstripper is within design specifications;
2. An influent water sample will be collected to determine if influent sample analyses are within
the design specifications of the airstripper.
3. The temperature of the influent water will be recorded to verify that this parameter is within
the air stripper design specifications.
4. A visual inspection of the air stripper trays during operation has been conducted. The trays
appeared to be free of scale, however, a slight film was felt on wetted parts. If determined
necessary, the airstripper trays will be dismantled, washed, and brushed.
The following table summarizes the remedial systems' performance for the period August I,
2004, through October 31, 2004:
Remediation Total Gallons Average Flow MassVOC TotalVOC Percent
System RcmO\'cd For Rate For Removal For Rerncwal Since Operational
Location Period Period Period Start-Up For Period
U pper/Lowcr 2,648,590 19.78 GPM 0.69 pounds 9.43 pounds 77% /95%
Macon Gallons
Lower Docker~· 0 Gallons 0GPM 0.0 pounds 0 pounds 0%
Upper 653,755 Gallons 4.88 GPM 0.83 pounds 25.48 pounds 100%
Docker~·
Upper Macon 999,394 Gallons 7.46 GPM 1.78 pounds 45.68 pounds !00%
Source Arca
GPM -Gallons p!.!r mmute VOC -Volatile Orgamc Compounds
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Ms. Giezelle Bennett
December I 0, 2004
Page No. 3
The analytical results for the quarterly groundwater samples collected from wells MW-16 and
MW-24 at the Lower Dockery system, are summarized on Table 5. The groundwater samples were
collected using the low-flow well sampling method. Based on the analytical report, the manganese
concentration in the sample collected from well MW-24 was reported to be 2,000 micrograms per
liter (ug/L), which is greater than the performance standard of50 ug/L. The laboratory reported the
other tested parameters in the water samples collected from wells MW-16 and MW-24, to be at
concentrations below the sample detection limit or below the performance standard. Water level
measurements recorded for the Lower Dockery site are summarized in Table 6.
TASKS PLANNED FOR PERIOD NOVEMBER I, 2004 THROUGH JANUARY 31, 2005:
• Weekly O&M of systems;
• Quarterly sampling of groundwater remediation system effluent in January 2005;
• Quarterly sampling of groundwater in wells MW-16 and MW-24 in January 2005;
• Semi-Annual sampling of groundwater remediation system influent in January 2005; and,
• Semi-Annual sampling of all monitoring wells in January 2005.
OPERATIONAL DIFFICULTIES AND DELAYS:
• July 29, 2004 -August 18, 2004 -The Upper Macon system was down due to a recirculation
pump malfunction. The recirculation pump was repaired and the system was restarted on Aub'llst
18, 2004.
• July 29, 2004 -August 3, 2004 -The Lower Macon system was down due to a high level alarm
in the airstripper. The alarm was cleared and the system restarted on August 3, 2004.
The MDSG appreciates the USEPA's cooperation with this project. If you have any questions or
comments, please feel free to contact us at [phone].
Sincerely,
/RMI GER CONS TING, INC.
Steven E. Irminger, P.E.
Senior Engineer
cc: Macon/Dockery Site Group Members
Mike Profit, CDM.Eederal.P.rograms __ _
·oavid Mattison, NC Superfund Section
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
TABLES
------
1.1-Dichloro-L l -Dichiaro-Cis1trans-I .2-Tetra-
Sample Date ethane ethene Dichloroethcnc chlorocthenc
Location (unll ) (ugiL) (ugiL) (UQll,}
UD Effluent 5/311996 <J.0 <LO <LO <1.0
6/5/1996 <1.0 <1.0 <1.0 <1.0
7/1/1996 <1.0 <1.0 <LO <LO
8/J/1996 <1.0 <1.0 <1.0 <l.O
9/411996 <LO <1.0 <l.O <LO
10/1/1996 <I.0 <l.0 <LO <1.0
11/7/1996 <l.O <1.0 <1.0 <1.0
12/5/1996 <LO Ll <l.O <LO l/611997 <1.0 <LO <LO <l.O
2/5/1997 <1.0 <1.0 <1.0 <LO
3/12/1997 <1.0 <1.0 <1.0 <1.0
418/1997 <1.0 <1.0 <1.0 <LO
5/1411997 <1.0 <1.0 <1.0 <1.0
6/6/1997 <1.0 <1.0 <1.0 <l.O
7/2/1997 <I.0 <1.0 <1.0 <1.0
817/1997 <1.0 <1.0 <LO <1.0
9/5/1997 <1.0 <LO <1.0 <l.O
10/2/1997 <1.0 <1.0 <1.0 <1.0
11/13/1997 <1.0 <1.0 <1.0 <1.0
12/5/1997 <1.0 <LO <1.0 <1.0
119/1998 <1.0 <1.0 <1.0 <1.0
2/5/1998 <l.0 <l.0 <LO <1.0
3/5/1998 <1.0 <LO <1.0 <1.0
4/3/1998 <1.0 <1.0 <l.O <1.0
517/1998 <LO <l.0 <LO <1.0
6/5/1998 <1.0 2l <1.0 <LO
7/9/1998 <1.0 <1.0 <1.0 <1.0
817/1998 <1.0 <1.0 <1.0 <LO
9/10/1998 <1.0 <1.0 <1.0 <1.0
10/2/1998 <1.0 <1.0 <LO <l.O
11/411998 <1.0 <1.0 <LO <LO
12/l/1998 <1.0 <1.0 <1.0 <LO
1/1 i/1999 <1.0 <1.0 <1.0 <l.O
2/11/1999 <1.0 <l.0 <LO <1.0
3/5/1999 <1.0 <LO <1.0 <1.0
4/8/1999 <1.0 <1.0 <1.0 <1.0
5/12/1999 <LO <1.0 <LO <LO
6110/1999 <1.0 <1.0 <1.0 <1.0
7/8/1999 <1.0 <1.0 <1.0 <1.0 815/1999 <1.0 <1.0 <LO <1.0
9/9/1999 <1.0 <1.0 <1.0 <l.O
10114/1999 <1.0 <1.0 <l.O <LO
11/3/1999 <1.0 <1.0 <LO <1.0
12.13/1999 <1.0 <l.0 <1.0 <l.O
RPS 3500 7 70
RPS: Remediation Performance Standard
-------TABLE 1 (Page 1 of 2)
EFFLUENT Analytical Results
UPPER DOCKERY
Macon Dockery Site
Richmond County, North Carolina
I. 1.1-Trichloro-Trichloro-
eth:me ethlene Toluene Total Xylencs
(uon J (uP.tl,) (u,'1..J (ugiL)
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 3.9 <3.0
<LO <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <LO <3.0
<1.0 <i.O <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <LO <1.0 <3.0
<1.0 <i.O <1.0 <3.0
<1.0 <LO <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<l.O <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<l.O <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <i.O <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <i.O <1.0 <3.0
<1.0 <1.0 <LO <3.0
<1.0 <1.0 <LO <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <LO <3.0
<1.0 <1.0 <1.0 <3.0
l.5 <1.0 <1.0 <3.0
<l.O <i.O <1.0 <3.0
<1.0 <i.O <1.0 <3.0
<LO <I.0 <1.0 <3.0
<1.0 <LO <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <I.0 <LO <3.0
<1.0 <LO <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <LO <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <LO <3.0
<LO <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <l.O <3.0
200 2.8 1000 400
Acetone Chromium Barium
(u111L) (uglL) (uQ/L)
52 <JO <lO
<10 <JO <lO
<IO <JO <lO
20 14 51
<10 <10 5l
<10 <IO <lO
<10 15 59
<10 12 l4
<IO 13 54
<IO 15 61
<10 <10 69
<IO <JO 63
<10 <10 60
<10 <JO l2
<10 <10 5l
<10 <10 <50
<10 <10 110
<10 <JO 50.1
<10 12.l 67.9
<10 <JO <50
<10 II <50
<10 <IO <50
<10 <10 <200
<10 <10 <200
<10 10 <50
<10 <JO 57
<10 <IO 51
<10 13 l3
<10 II 58
<25 <IO l4
<IO II 63
<25 14 63
<IO II l5
<10 ll 73
<25 II 62
<IO II 54
<10 12 57
<10 13 66
<10 10 64
<10 14 66
<l.0 14 61
<10 14 60
<IO 13 58
<10 13 64
3500 50 ]000
-- ---
Suspended
!-,.langanesc Zinc Lead Solids
(u••) (ugiL) (ug/J,) (mg/L)
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
7 <20 <3.0 8
<5.0 <20 <3.0 <5.0
5.9 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
l. l <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
5.9 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
7.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
l.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
18.6 24.8 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<15 <20 <3.0 <5.0
5.2 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5,0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<10 <20 <3.0 <5.0
6.3 <20 <3.0 12
40 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
23 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 5.2 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
50 5000 "
--- --- -
1, 1-Dichlorn-l,1-Dichloro-Cisitrans-1.2-Tetra-
Sample Date ethane ethenc Dichloroethcm: chlorocthenc
Location (ug/L) (ug,L) (ug/L) (ug,l,)
UD Effluent 3/9/2000 <1.0 2.1 <1.0 <l.O
417/2000 <1.0 <LO <1.0 <1.0
5/9/2000 <1.0 <LO <1.0 <LO
61912000 <1.0 <LO <1.0 <1.0
7/7/2000 <1.0 <LO <1.0 <l.O
8/3/2000 <LO <LO <l.O <l.O
9/25/2000 <LO <LO <1.0 <1.0
10/12/2000 <1.0 <l.O <1.0 <LO
l/18'2001 <l.O <l.O <1.0 <LO
5/3'200 I <1.0 <1.0 <1.0 <LO
7/11/2001 <1.0 <1.0 <1.0 <l.O
10/18'2001 <1.0 <LO <1.0 <l.O
1/16'2002 <1.0 <LO <1.0 <1.0
7/31/2002 <1.0 <1.0 <LO <1.0
10/30'2002 <LO <LO <1.0 <1.0
l/28'2003 NOT SA.\fPLED SYSTEM
3/14'2003 NOT SA~fPLED SYSTE:\.1
413/2003 <LO <1.0 <1.0 <LO
7/10(2003 <LO <LO <1.0 <LO
10/30/2003 <LO <LO <1.0 <LO
1/13/2004 <1.0 <LO <2.0 <1.0
4/5/2004 <1.0 <1.0 <2.0 <1.0
6'28/2004 <1.0 <1.0 <2.0 <1.0
10/21/2004 <1.0 <1.0 <2.0 <1.0
RPS 3500 7 70
RPS: Remediation Performance Standard
- ------
TABLE 1 (Page 2 of 2)
EFFLUENT Analytical Results
UPPER DOCKERY
Macon Dockery Site
Richmond County, North Carolina
I, l, 1-Trich\oro-Trichloro-
ethane ethlene Toluene Total Xylenes
(ll"/1 ) (uo1L) (u"") (u"" )
<1.0 <1.0 <l.O <3.0
<1.0 <LO <l.O <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <l.O <LO <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <LO <3.0
<LO <1.0 <l.O <3.0
<LO <1.0 <1.0 <3.0
<LO <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3,0
<1.0 <1.0 <1.0 <3.0
DOWN
DOWN
<1.0 <LO <1.0 <3,0
<1.0 <LO <LO <3,0
<LO <1.0 <1.0 <3.0
<LO <1.0 <l.O <2.0
<LO <1.0 <1.0 <2.0
<LO <1.0 <1.0 <2.0
<1.0 I <1.0 <LO <2.0
200 2.8 1000 400
Acetone Chromium Barium
(ug/L) (ug1L) (uo'L)
<10 14 74
<10 <10 160
<10 14 69
<10 <10 79
<10 <IO 95
<IO <IO 78
<IO <IO 85
<10 <IO 84
<IO <IO 100
<IO 14 80
<10 27 79
<10 14 74
<10 18 !30
<10 <10 55
<10 <10 9}
l\"OT SA.VIPLED
NOT SA.\IPLED
<IO <IO 83
<IO <IO 96
<10 <IO 55
<25 II 71
<25 12 68
<25 <10 54
<25 <10 85
~500 50 1000
---- -
Suspended
Manganese Zinc Lead Solids
(u:11) (ugil,) (ugil,) (mgil,)
9.3 <20 <3.0 <5.0
8.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
10 <20 <3.0 <5.0
<5.0 <20 <3.0 <S.O
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
6.3 <20 <3.0 <5.0
5.7 <20 <3.0 <5.0
43.0 27 <3.0 8.0
5.4 <20 <3,0 <5.0
120 35 5 <5.0
5.6 <20 <3.0 <5.0
7,3 <20 <3.0 <5.0
SYSTEM OOWN
SYSTElvl DOW1'.'
5, I <20 <3.0 <5.0
19 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
15 24 <3.0 14.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
<5.0 <20 <3.0 <5.0
50 5000 15
----- --
Chloro-1.1-Dichloro-1.1-Dichloro-Cis.itran~-1.2-
Sample Date form ethane cthene Dich1oroethene
Location (ugiL) (u2/L) (uoll) (uoll,)
LD Effluent 2/15/1996 <1.0 <l.0 <LO <1.0
2116/1996 <1.0 <1.0 <LO <1.0
212211996 <1.0 <1.0 <1.0 <1.0
2/28/1996 <1.0 <l.0 <1.0 <1.0
3/8/1996 <1.0 <1.0 <l.0 <1.0
4/3/1996 <1.0 <1.0 <l.0 <1.0
5/J/1996 <1.0 <1.0 <1.0 <1.0
811/19% <LO <1.0 <LO <1.0
9/4/1996 <1.0 <1.0 <1.0 <1.0
10/1/1996 <1.0 <1.0 <LO <1.0
I V?/1996 <1.0 <LO <LO <LO
12/5/1996 <LO <1.0 <LO <LO
1/6/1997 <1.0 <LO <LO <LO
3/12/1997 <1.0 <1.0 <1.0 <1.0
418/1997 <1.0 <1.0 <1.0 <1.0
5/141l997 <LO <1.0 <1.0 <1.0
61611997 <LO <1.0 <1.0 <1.0
7!2Jl997 <LO <1.0 <1.0 <1.0
817/1997 <LO <1.0 <LO <1.0
9/5/1997 <LO <1.0 <LO <1.0
10/2/1997 <LO <1.0 <1.0 <1.0
11/13/1997 <LO <1.0 <1.0 <1.0
12/5/1997 <1.0 <1.0 <1.0 <1.0
l/9/1998 <1.0 <1.0 <1.0 <1.0
21511998 <l.O <1.0 <1.0 <1.0
3/5/1998 <1.0 17 3.2 <1.0
4/3/1998 <LO <1.0 <1.0 <1.0
5/7/1998 <1.0 <1.0 <LO <l.O
6/5/1998 <LO <1.0 <LO <1.0
719/1998 <LO <l.O <LO <1.0
817/1998 <1.0 <1.0 <LO <1.0
9/10/1998 <1.0 <LO <1.0 <l.0
10/2/1998 <1.0 <LO <LO <LO
ll/4/1998 <l.O <LO <LO <1.0
121111998 <1.0 <l.O <1.0 <1.0
1/11/1999 <1.0 <LO <1.0 <1.0
•2)11/99 <1.0 <1.0 <l.0 <1.0
3/5/1999 <LO <1.0 <1.0 <1.0
418/1999 <1.0 <1.0 <1.0 <1.0
5/12/1999 <LO <1.0 <1.0 <1.0
6/10/1999 <1.0 <1.0 <LO <1.0
7/8/1999 <1.0 <1.0 <1.0 <l.O
815/1999 <LO <1.0 <LO <l.O
9/9/1999 <LO <1.0 <1.0 <1.0
10/14/19.)1) <LO <LO <1.0 <l.O
1112}1999 <1.0 2.5 <1.0 <l.O
12/3/1999 <l.O 2.8 <1.0 <l.O
RPS. 3500 7 70
RJ>S: Remediation Pcrfonnance Sundard
-
Methylene
chloride
(ui,,L)
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<5.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
-- --TABLE 2 (Page I of 2)
EFFLUENT Analytical Results
LOWER DOCKERY
~!aeon Dockery Site
Richmond County, North Carolina
Ll,l-Trichloro Trichloro-
ethane ethene Benzene Toluene
(ua/1,) (ug/L) (ug/L) (u11/l,)
<l.O <1.0 <l.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <l.0 <LO
<1.0 <l.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <:1.0 <1.0 <l.O
<l.O <1.0 <1.0 3.4
<l.O <1.0 <1.0 <1.0
<1.0 <l.O <1.0 <1.0
<1.0 <1.0 <LO <LO
<1.0 <l.O <LO <LO
<1.0 <1.0 <LO <LO
<1.0 <l.O <LO <LO
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <l.O <1.0 <1.0
<LO <LO <1.0 <l.O
<1.0 <LO <1.0 <1.0
<LO <1.0 <l.O <l.0
<LO <1.0 <LO <1.0
<1.0 <1.0 <1.0 <LO
5.5 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<l.O <1.0 <1.0 <LO
<l.O <1.0 <1.0 <l.O
<l.O <1.0 <1.0 <1.0
<l.O <1.0 <1.0 <1.0
<l.O <l.O <1.0 <l.O
<l.O <1.0 <1.0 <1.0
<LO <l.O <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <LO <l.O
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <l.O <1.0 <l.O
<1.0 <l.O <1.0 <1.0
<1.0 <l.O <1.0 <1.0
<1.0 <LO <1.0 <1.0
1.2 <LO <LO <1.0
200 2.8 1000
- ------
Total Suspended
Xykncs Chromium Barium ~langancse Zinc Cadmium Solids
(u~/L) (uall,) (u11/I ) (UglL) (u,/L) (ug/L) (mg/L)
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 5
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 14 <20 <0.30 <5.0
<3.0 <10 <50 13 <20 0.56 <5.0
<3.0 <10 <50 11 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 3S <20 <0.30 19
<3.0 <10 <50 6 <20 <0.30 <5.0
<3.0 <10 70 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <I <5.0
<3.0 <10 <50 160 <20 <0.30 <5.0
<3.0 <10 <SO 34 <20 <0.30 <5.0
<3.0 <10 <50 250 <20 <0.30 58
<3.0 <10 <200 85 <20 <0.30 <5.0
<3.0 <10 <200 39 <20 <0.30 <5.0
<3.0 <10 <50 17 <20 <0.30 <5.0
<3.0 <10 <50 6.3 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <SO <5.0 <20 <0.30 <5.0
<3.0 <IO 17 140 <20 <0.30 <5.0
<3.0 <10 <50 10 <20 <0.30 <5.0
<3.0 <10 <SO <5.0 <20 <0.30 <5.0
<3.0 <10 <SO S.2 <20 <0.30 <5.0
<3.0 <10 <SO 15 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 52 9.5
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 <5.0 <20 <0.30 <5.0
<3.0 <10 <50 5.0 <20 <0.30 <5.0
<3.0 <10 72 520 31 <0.30 <5.0
<3.0 <10 93 470 38 <0.30 <5.0
<3.0 <10 <50 11 <20 <0.30 <5.0
<3.0 <10 <50 110 <20 <0.30 <5.0
400 so 1000 50 5000
--------
Ch\oro-1.1-Dichloro-1.1-Dichloro-Cis/tram-1.2-~1cth:,.·lene
Sample Date fonn ethane ethonc Dichloroethene chloride
Location (uglL) (ug/L) (u~/L) (u•" ) (uwL)
LD Effiucnt 2/25/2000 <1.0 6.2 <1.0 <1.0 <2.0
319/2000 <l.0 <1.0 <1.0 <1.0 <2.0
417/2000 .. System Do•n Not Sampled
519/2000 <1.0 <1.0 <LO <1.0 <2.0
619/2000 <1.0 <1.0 <LO <1.0 <2.0
7/7/2000 <1.0 <1.0 <1.0 <1.0 <2.0
8/3/2000 <1.0 <1.0 <1.0 <1.0 <2.0
9/25/2000 <1.0 <LO <LO <1.0 <2.0
10/12/2000 <1.0 <LO <1.0 <1.0 <2.0
1/18/2001 .. System Do•n Not Sampled
4/24/200 I <1.0 I <1.0 I <1.0 I <1.0 I <2.0 I 5/11/2001 <1.0 <1.0 <1.0 <1.0 <2.0
7/11/2001 .. System Do•n Not Sampled
10/18/2001 <1.0 <1.0 <1.0 <1.0 <2.0
1/16/2002 System Down Not Sampled
7/31/2002 System Do•n Not Sampled
10/30/2002 <1.0 <1.0 <1.0 <1.0 <2.0
1/28/2003 System Do"n Not Sampled
3/14/2003 <1.0 <1.0 <1.0 <1.0 <2.0
4/3/2003 <1.0 <1.0 <1.0 <1.0 <2.0
7/10/2003 <i.O <1.0 <1.0 <1.0 <1.0
10/30/2003 <1.0 <i.O <1.0 <1.0 <l.O
1/13/2004 <1.0 <1.0 <1.0 <2.0 <5.0
4/5/2004 System Suspended Not Sampled
RJ>S: 3500 7 70 5
RPS: Remediation Performance Standard
------- -
TABLE 2 (Page 2 of2)
EFFLUENT Analytical Results
LOWER DOCKERY
Macon Docker)' Site
Richmond County. North Carolina
L 1.1-Trichloro TrichJoro-
ethane elhene Betll.ene Toluene
(unn,) (uglL) (uglL) (u.,L)
2.6 <LO <\.O <l.O
<1.0 <LO <1.0 <1.0
•• .. . System
<1.0 <LO <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0 .. ... System
<1.0 <1.0 I <l.O I <1.0
<l.O <1.0 <l.O <1.0 .. ... System
<I.0 <l.O <1.0 <1.0
System
System
<1.0 <1.0 <1.0 <1.0
System
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
System
200 2.8 1000
Total
Xylenes
(ug/L)
<3.0
<3.0
Do•n
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
Dmm
I <3.0
<3.0
Do•n
<3.0
Do•n
Do•n
<3.0
Do•n
<2.0
<3.0
<3.0
<3.0
<2.0
Suspended
400
Chromium Barium ~fanganese Zinc
(ug!L) (ug,L) (mvL) (ug/L)
<JO <50 320 <20
<10 <50 53 <20
Not Sampled
<IO <50 180 <20
<IO <50 <5.0 <20
<IO <50 100 <20
<IO <50 <5.0 <20
<10 <50 <5.0 97
<10 <50 <5.0 97
Not Sampled
I <IO I <50 I <5.0 I <20
<IO <50 <5.0 <20
Not Sampled
<10 <50 <5.0 <20
Not Sampled
Not Sampled
<IO <50 58 <20
Not Sampled
<10 <50 <5.0 <20
<10 <50 <5.0 <20
<IO <50 <5.0 <20
<IO <50 <5.0 <20
<IO <50 <5.0 <20
Not Sampled
50 IOOO 50 5000
---
Suspended
Cadmium Solids
(uglL) (mwL)
<0.30 <5.0
<0.30 <5.0 ...
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0 ...
I <0.30 I <5.0
<0.30 <5.0 ...
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 <5.0
<0.30 IO
----
Sample
Location
UMSA E!lluent
RPS
RPS
NA:
Chiaro-1, 1-Dichloro-
Dak fonn '""'" (ug/L) (ug/L)
2/1711996 <LO <1.0
2/22/1996 <LO <1.0
2/28/1996 <1.0 <1.0
3/811996 <1.0 <1.0
413/1996 <LO <1.0
5/3/1996 <1.0 <1.0
6/5/1996 <1.0 <1.0
7/1/1996 <1.0 <1.0
7/30/1996 <1.0 <1.0
9/4/1996 <1.0 <1.0
\0/1/1996 <1.0 <1.0
11/711996 <1.0 <1.0
1215/1996 <1.0 <1.0
1/6/1997 <1.0 <1.0
2/4/1997 <1.0 <1.0
3/\211997 <1.0 <LO
4/8/1997 <1.0 <l.O
5/12/1997 <1.0 <l.O
61611997 <1.0 <l.O
7/2/1997 <1.0 <l.O
8/7/1997 <1.0 <l.O
91511997 <1.0 <l.O
10/2/1997 <1.0 <1.0
11/13/1997 <1.0 <1.0
12/5/1997 <1.0 <1.0
1/9/1998 <1.0 <1.0
2/5/1998 <1.0 <1.0
3/5/1998 <1.0 <1.0
413/1998 <l.0 <1.0
5/7/1998 <1.0 <1.0
615/1998 <1.0 <1.0
7/9/1998 <1.0 <1.0
817/1998 <l.0 <1.0
9/10/1998 <1.0 <1.0
10/2/1998 <1.0 <1.0
1114'1998 <1.0 <1.0
12/1/1998 <1.0 <1.0
1/11/1999 <1.0 <1.0
2/11/1999 <1.0 <1.0
3/5/1999 <1.0 <1.0
418/1999 <1.0 <1.0
5/13/1999 <1.0 <1.0
6110/199') <1.0 <1.0
7/8/1999 <1.0 <J.0
81511999 <1.0 <1.0
9/9/1999 <1.0 <1.0
\0/1411999 <1.0 <1.0
11/211999 <1.0 <1.0
12/3/1999 <1.0 <1.0
3500
Remedillim Pcrforman~ Standard
Not Analyzed
-
l, -Dichiaro-
cthcne
(ug/L)
<l.0
<l.0
<LO
<1.0
<1.0
<l.O
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<I 0
<1.0
<1.0
<I 0
<LO
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<I 0
<1.0
<1.0
<1.0
<\.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
7
------
Cis.ltrans-1,2-Tetrachloro-
Dichloroc1hcne ethene
(""'1,) (,g!L)
<I 0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<LO <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <l.O
<1.0 <l.O
<I 0 <1.0
<IO <I 0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <LO
<1.0 <l.O
<1.0 <l.O
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <1.0
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <1.0
<1.0 <l.O
<1.0 <i.O
<1.0 <J.0
<1.0 <l.O
70
TABLE 3 (Page 1 of 2)
EFFLUENT Analytical Results
UPPER MACON SOURCE AREA
Macon Dockery Site
Richmond County, Nroth Carolina
I. I, 1-Trichloro-Trichloro-\'inyl
ethane ethene chloride Benzene
(ugll) ("on) (,g!L) ("on )
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <l.O <1.0
<1.0 <1.0 <l.O <1.0
<1.0 <1.0 <l.O <1.0
<1.0 <1.0 <l.O <1.0
<1.0 <1.0 <l.O <1.0
<LO <1.0 <1.0 <l.O
<l.O <LO <1.0 <1.0
<1.0 <1.0 <1.0 <!.O
<1.0 <1.0 <1.0 <1.0
<l.O <l.0 <1.0 <1.0
<l.O <1.0 <1.0 <1.0
<1.0 <l.0 <10 <1.0
<LO <1.0 <10 <1.0
<1.0 <1.0 <l.0 <1.0
<1.0 <1.0 <l.0 <1.0
<1.0 <1.0 <l.O <1.0
<1.0 <1.0 <l.O <LO
<1.0 <1.0 <l.O <LO
<IO <l.O <l.O <LO
<10 <l.O <1.0 <1.0
<1.0 <LO <1.0 <1.0
<LO <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
<1.0 <l.0 <10 <1.0
<1.0 <1.0 <10 <1.0
<1.0 <1.0 <10 <1.0
<l.O <1.0 <10 <1.0
<1.0 <1.0 <1.0 <1.0
<l.O <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<l.O <1.0 <1.0 <IO
<1.0 <1.0 <1.0 <I 0
<1.0 <1.0 <LO <l.O
<1.0 <1.0 <l.O <LO
<1.0 <1.0 <l.O <LO
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <LO <l.O <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0 , _()(] , -.8
--
Toluene Chromiwn Barium
(,g!L) (""'1,) (ug/L)
<1.0 <10 120
<1.0 <10 120
<1.0 <10 130
<1.0 <10 120
<1.0 <IO 110
<l.O <10 120
2.9 <10 130
<1.0 12 110
<1.0 <10 200
<1.0 II 170
<1.0 <IO 130
<1.0 <IO 140
<1.0 <ID 170
<1.0 <10 200
<1.0 <10 160
<1.0 <10 130
<I 0 <10 200
<1.0 12 210
<1.0 <IO 240
<1.0 <10 180
<1.0 II 230
<1.0 <IO 130
<1.0 <IO 185
<1.0 <10 129
<1.0 <10 150
<1.0 <10 180
<1.0 <10 200
<l.O II 210
<1.0 <10 <200
<1.0 <10 210
<1.0 <ID 160
<1.0 <10 240
<1.0 <10 190
<l.O <IO 200
<1.0 <IO 190
<1.0 10 220
<1.0 <IO 160
<1.0 <IO 150
<1.0 <IO 230
<1.0 <10 180
<1.0 <IO 170
<1.0 <IO 170
<1.0 <IO 180
<1.0 <10 170
<1.0 <10 140
<LO <10 150
<1.0 <IO 200
<1.0 <IO 180
<l.O <IO 180
1000 50 1000
------
Suspended
M,ngMeS, Zll1c Cadmium L,ad Mercury Solids
(u,/1) (<¢) (ug/L) (,wl) (ug/L) (mg/L)
120 '20 <O JO <3.0 <.2 <5.0
70 <20 <030 <3.0 <.2 <5.0
51 <20 <0.30 <3.0 <.2 <5.0
37 <20 <0.30 <3.0 <.2 <5.0
27 <20 <0.30 <3.0 <.2 5
26 <20 <0.30 <3.0 <.2 <5.0
22 ,20 <0.30 <3 0 <.2 6
14 <20 <0.30 <3 0 NA <5.0
110 41 <0.30 9.2 NA 23
68 26 <0.30 66 NA 16
13 <20 0.47 <3.0 NA 24
13 <20 <0.30 <3.0 NA 26
17 <20 <0.30 <3.0 <0.20 5
46 25 <0.30 3.5 NA 120
29 <20 <0.30 <3.0 NA ' JO <20 <0.30 <3.0 NA <5 0
JO <20 <0.30 <3.0 NA 7
95 35 <0.30 <3.0 NA 100
74 <20 <0.30 <3.0 NA <5.0
41 <20 <0.30 <3.0 NA <5.0
250 "' <O 30 4.8 NA NA
27 <20 <O 30 <3.0 NA 22
31.5 <20 <0.30 <3.0 NA II
84.2 <20 <I <3.0 NA 8
160 26 <0.30 6.5 NA <5.0
33 <20 <0.30 <3.0 NA <5.0
20 <20 <0.30 <3.0 NA 6
160 25 <0.30 4.1 NA <5.0
64 <20 <0.30 <3.0 NA <5.0
310 29 <0.30 5 NA 13
46 <20 <0.30 <3.0 NA <5.0
110 <20 <0.30 <3.0 NA <5.0
37 <20 <0.30 <3.0 NA <5.0
56 <20 <0.30 <3.0 NA 33
110 <20 <0.30 <3.0 NA 12
450 48 <0.30 4.6 NA 180
68 <20 <0.30 <3.0 NA <5.0
120 <20 <0.30 <3.0 NA <5.0
120 22 <0.30 <3.0 NA <5.0
100 25 <0.30 <3.0 NA <5.0
72 <20 <0.30 <3.0 NA <5.0
66 <20 36 <3.0 NA 8.5
100 <20 <0.30 <3.0 NA <5.0
160 <20 <0.30 3.3 NA <5.0
13 <20 <0.30 8.7 NA <5 0
340 24 <0.30 <3.0 NA <5.0
37 <20 <0.30 <3.0 NA <5.0
13 <20 <0.30 <3.0 NA <5.0
18 <20 <0.30 <3.0 NA <5.0
50 5000 5 II
Sample
Location
RPS
RPS
NA:
---
Chloro-1,1-Dichloro-
Date form ethane
('"'IL) (ug/L)
2/16/2000 <1.0 <1.0
3/9/2fXXJ <1.0 <1.0
417/2000 <1.0 <1.0
5/8/2000 <1.0 <1.0
6/9/20CXJ <1.0 <1.0
7/7/20CiJ <1.0 <1.0
8/2/2000 <1.0 <1.0
9/25/2000 <1.0 <1.0
10/1212000 <l.0 <1.0
1/18/2001 <l.0 <1.0
5/3/2001 <1.0 <1.0
7111/2001 <1.0 <1 0
10/18/2001 <1.0 <1 0
12128/2001 <LO <1.0
1/15/2002 <1.0 <1 0
7/30/2002 <1.0 <1.0
10/30/2002 <1.0 <1 0
J/28/2003 NOT
3/1412003 <1.0 <1.0
413/2003 <1.0 <1.0
7/10/2003 <1.0 <1.0
10/30/2003 <1.0 <1.0
1/13/2004 <l.0 <1.0
4/5/2004 <1.0 <1.0
6/2812004 <1.0 <1.0
10/21/2004 <LO <1.0
" ,,oo
Remedulion ~onunce Standard
Not Analyzed
-
1, -Dichloro-
ethene
(ug'L)
<LO
16
<l.O
<1.0
<l.O
9.9
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
SAfvfPLED
<1 0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
--------
Cisltrnns-1,2-Tetrachloro-
Dichlorocthene ethcnc
(ug'L) (nol!,)
<1.0 <1.0
<1.0 LO
<1.0 <LO
<1.0 <1.0
<LO <1.0
<l.O <1.0
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <l.O
SYSTEM DOWN
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
70
TABLE 3 (Page 2 of 2)
EFFLUENT Analytical Results
UPPER MACON SOURCE AREA
Macon Dockery Site
Richmond County, Nroth Carolina
1,1,1-Trichloro-Trichloro-Vinyl ,t!um, ethene chloride Benzene
("•") ("on) (ug'L) ("on)
<1.0 <LO <LO <1.0
2.6 <LO <1.0 <1.0
<1.0 <LO <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
14 <1.0 <1.0 <1.0
<LO <1.0 <l.0 <1.0
<1.0 <l.0 <l.O <1 0
<1.0 <l.0 <LO <LO
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <LO <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <l.0 <1.0
<1.0 <1.0 <1.0 <1.0
NOT
<1.0 <1.0 <1.0 <1.0
<1.0 <l.O <1.0 <1.0
<1.0 <l.O <1.0 <1.0
<1.0 <1.0 <1.0 <1.0
<1.0 <1.0 <1.0 <l.O
<1.0 <1.0 <1.0 <LO
<1.0 <1.0 <1.0 <1.0
<LO <1.0 <1.0 <1.0
200 ' __ 8
Toluene Chrom1wn Barium
(ug'L) (ug/L) (.,,;L)
<LO <10 240
<LO <10 230
<1.0 <10 210
<1.0 <10 410
<1.0 <10 180
<LO <10 220
<LO <10 190
<1.0 <10 280
<1.0 14 180
<l.O <10 200
<1.0 28 -WO
<1.0 15 360
<1.0 60 450
<1.0 11 360
<1.0 <10 360
<1.0 21 370
<1.0 20 370
~A.\.fPLED SYSTEM
<1.0 17 410
<1.0 11 350
<1.0 <10 370
<l.O <10 360
<1.0 76 400
<1.0 <10 230
<1.0 <10 160
<1.0 <10 180
1000 50 1000
----
Suspended
Manganese Zinc Cadmium Lead ~viercwy Solids
("""1) (ug/L) (ug'L) ("""1) (ug/L) (mg'[.)
300 40 <0.30 5.3 NA 130
47 <20 <0.30 <3.0 NA 5.0
40 <20 <0.30 <3.0 NA <5.0
54 <20 <0 30 <3.0 NA <5.0
61 <20 <0.30 <3.0 NA <5.0
250 32 <0.30 3.8 NA <5.0
80 <20 <0.30 41 NA 38.0
8.3 <20 <0.30 <3.0 NA <5.0
84 <20 <0.30 3.7 NA 6.0
36 <20 <0.30 <3.0 NA 8.5
350 29 <0.30 19 NA <5.0
110 <20 <0.30 3.7 NA 38
900 47 <0.30 21 NA <5.0
110 <20 <0.30 <3.0 NA 8.0
35 <20 <0.30 <3.0 NA 8.0
130 <20 <0.30 3.0 NA 11.0
98 <20 <0.30 4.0 <020 6.0
DOWN
240 43 <0.30 480 <0.20 <5.0
44 <20 <0.30 280 <0.20 7
71 <20 <0.30 <3.0 <0.20 42
170 120 <0.30 <3.0 <0.20 <5.0
1800 210 0.47 62 NA 23
64 <20 <0.30 <3.0 NA 33
6.2 <20 <0.30 <3.0 NA <5.0
18 <20 <0.30 <3.0 NA <5.0
,o 5000 15 LI
--- - ----- --
Chloro-1.1-Dichloro-1.1-Dichloro-
Sample Dat, form 01han, '"""' Location (uglI..) (,g/L) ("'•L)
U/L Effluent 2'2411996 <1.0 <1.0 <1.0
2'25/1996 <1.0 <1.0 <1.0
2'28/1996 <1.0 <LO <1.0
3/8/1996 <LO <1.0 <1.0
3'16/1996 <1.0 <1.0 <1.0
,V]/1996 <1.0 18 <1.0
5/3/1996 <1.0 <1.0 <1.0
615/1996 <1.0 <1.0 <1.0
7/1/1996 <1.0 <1.0 <1.0
7/30/1996 <1.0 <1.0 <10
9/4/)996 <1.0 <1.0 <10
J0/1/1996 <1.0 <1.0 <10
11/7/1996 <1.0 <1.0 <1.0
12/5/1996 <1.0 <1.0 <1.0
]/6/1997 <1.0 <1.0 <1.0
l/411997 <1.0 <1.0 <1.0
3/12/1997 <1.0 <1.0 <1.0
418/1997 <l.O <1.0 <1.0
5112/1997 <l.O <1.0 <1.0
6/6/1997 <1.0 <1.0 <1.0
7/2/1997 <1.0 2.4 <1.0
7/25/1997 NA NA NA
81711997 <1.0 <1.0 <10
91511997 <l.0 <1.0 <10
J0/2/1997 <l.0 <1.0 <10
11/13/1997 <1.0 <1.0 <1.0
12/5/1997 <1.0 <1.0 <1.0
J/9/1998 <1.0 <1.0 <1.0
2/5/1998 <1.0 <i.O <1.0
3/5/1998 <l.O <J.0 <1.0
413/1998 <1.0 <1.0 <1.0
51711998 <1.0 <1.0 <1.0
6/5/1998 <LO <l.0 <1.0
719/1998 <1.0 <1.0 <1.0
S/711998 <1.0 <1.0 <1.0
9'10/1998 <1.0 <1.0 <l.O
10/2/1998 <1.0 <1.0 <l.O
11/4/1998 <1.0 <1.0 <l.O
12/1/1998 <LO <1.0 <1.0
1/11/1999 <LO <1.0 <l.O
2/11/1999 <1.0 <1.0 <LO
J/5/1999 <1.0 <1.0 <1.0
418/1999 <1.0 <1.0 <1.0
5113/1999 <l.0 <1.0 <1.0
6'10/1999 <l.0 <1.0 <1.0
RPS 3)00
RPS: Remediation Performance Standard
NA: Not Analyzed
CiMrans-1.2-Methylene
Dichlor~then<! chloride
("ofl) (rn,/1)
<l.O <2.0
<l.O <2.0
<LO <2.0
<LO <2.0
<l.O <2.0
16 <2.0
<l.O <2.0
<LO <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<l.0 <2.0
<l.O <2,0
<l.O <2,0
<1.0 <2,0
<1.0 <2,0
<1.0 <2,0
1.8 <2,0
NA NA
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<l.O <2.0
<l.O <2.0
<l.O <2,0
<1.0 <2.0
<l.O <2.0
<l.O <2.0
<1.0 <2,0
<1.0 <2,0
<1.0 <2,0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <5.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
70 5
TABLE~ (Page, I of 2)
EFFLUENT Analytical Results
UPPER/LOWER MACON
Macon Docker)' Site
Richmond County, North Carolina
Teirachloro-1, l, 1-Trichloro-Trichloro-
ethcnc <lhru>< <lhrn,
{""'1 ) ("on) (u<>1L)
<l.0 <1.0 <l.O
<l.0 <1.0 <1.0
<l.O <1.0 <1.0
<l.O <1.0 <1.0
<l.O <1.0 <1.0
<1.0 <1.0 19
<1.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
<1.0 <l.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
NA NA NA
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <10
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <I 0
<1.0 <1.0 <10
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<LO <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
200 2.8
Toluene
("'"1,)
<1.0
<1.0
<1.0
<l.O
<l.O
<LO
<l.O
2.1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA
<LO
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1000
------- -
Suspended
Ou-omium Ban= Manganese Zinc Cadmiwn L=l Solids
(Ul\'L) (,g/LJ (ug'L) (11011...) (ugfL) (ug/L) (=")
<JO 83 150 15-0 <0.30 3.7 <5.0
<JO <JO 160 170 <0.30 3.6 <5.0
<JO <50 32 59 <0.3-0 <3.0 8
<JO <50 39 56 <0.30 <3.0 <5.0
<JO <50 31 51 <0.30 <3.0 <5.0
<JO <50 44 54 <0.30 3.6 10
<10 31 JO 21 <0.30 <3.0 <5.0
<10 <50 7.5 <20 <0.30 <3.0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 24
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<IO <50 <5.0 <20 <0.30 <3.0 <5.0
<IO <50 <5.0 <20 <0.30 <3.0 <5.0
<IO 39 <5.0 <20 <0.30 <3.0 8
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 79 <20 <0.30 <3.0 <5.0
NA NA 36 NA <0.30 NA NA
<10 <50 54 <20 <0.30 3.1 NS
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 6.3 <20 <0.30 <3.0 25
<10 <50 <5.0 <20 <0.30 <3.0 <5
<IO <50 <5.0 <20 <0.30 <3.0 <5
<JO <50 <5.0 <20 <0.30 <3.0 <5
<IO 56 <5.0 <20 <0.30 <3.0 <5
<IO <200 <15 <20 <0.30 <3.0 <5.0
<10 <200 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 NA
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 9.2 <20 <0.30 <3.0 <5.0
<10 <50 6.7 <20 <0.30 <3.0 <5.0
<10 31 <10 <20 <0.30 <3.0 <5.0
<10 <50 6.2 <20 <0.30 <3,0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 <5 O <20 <0.30 <3.0 <5.0
<JO <50 <5 0 <20 <0.30 <3.0 <5.0
50 1000 ,o 5000 5 15
- -
Sample
Location
U/L Effiuent
RPS.
RPS:
NA:
- -- - -- ---
Chloro-l, 1-Dichloro-
°"" form '"""" (ug/L) ("&'!-)
7/8/1999 <l.O <I 0
8/5/1999 <1.0 <J.0
9/9/1999 <1.0 <J.0
10/14/1999 <l.O <J.0
]J/311999 <LO <J.0
12'3/J999 <1.0 <1.0
2/17/2000 <1.0 <1.0
3/9/2000 <1.0 <1.0
4/7/2000 <1.0 <1.0
5/8/2000 <1.0 <1.0
6/9/2000 <1.0 <1.0
7/7/2000 <1.0 <1.0
8/2/2000 <1.0 <1.0
9125/2000 <1.0 <1.0
10/12/2000 <l.O <1.0
1/18/2001 ... Not
4124/2001 <l.O <1.0
5/3/2001 <1.0 <1.0
7/20/2001 <1.0 <1.0
10/18/2001 <LO <1.0
12/28/2001 <l.O <1.0
1/15/2002 <l.O <1.0
7/31/2002 }.;ot
10/30/2002 <1.0 <1.0
1/28/2003 <1.0 <1.0
413/2003 <1.0 <1.0
7/10/2003 <1.0 <1.0
10/30/2003 <1.0 <1.0
1/13/2004 <1.0 <1.0
415/2004 <1.0 <J.0
6128/2004 Not
10/21/200-l-<1.0 <1.0
3,00
RemedJatirn Perfonnance Standard
Not Analyzed
I, 1-Dichloro-Cis/trans-1.2-
ethene Dichloroethene
(11£1.) ("<>'L)
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <l.0
<LO <l.0
<LO <l.O
<1.0 <l.O
<1.0 <l.O
<1.0 <l.O
<l.O <l.O
<1.0 <1.0
<1.0 <LO
<l.O <LO
<1.0 <1.0
<l.O <1.0
Sampled
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<l.O <1.0
<l.O <1.0
Sampled
<LO <1.0
<LO <LO
<l.O <1.0
<l.O <1.0
I <1.0
9., <2.0
<1.0 <2.0
Sampled
!.5 LO
7 70
Methylene
chloride
(""" )
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2,0
<2.0
Sy,tcn
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
System
<2.0
<2.0
<2.0
<2.0
<2.0
<5.0
<5.0
System
<5.0
TABLE -I (Page 2 of 2)
EFFLUENT Analytical Results
UPPER/LOWER MACO/I'
Macon Docke,y Site
Richmond County, North Carolina
T etrachloro-1,1,1-Trichloro-Trichloro-
cthene ,Ihm,, ethmc
(""") (""" ) (•~")
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<LO <1.0 <LO
<LO <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <10
<1.0 <1.0 <10
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
Dom, ... ...
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<l.O <l.0 <1.0
Do•n
<1.0 <l.O <LO
<1.0 <l.O <LO
<1.0 <l.O <1.0
<1.0 <1.0 <LO
<l.O <1.0 <1.0
1.9 <1.0 <1.0
1.6 <1.0 <1.0
Do=
1.3 <1.0 <LO
200 2.,
Toluene
(ug•L)
<LO
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<JO
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<l.O
<l.O
<1.0
<1.0
1000
-- ----- -
Suspended
Chromium Bruium Manganese Zinc Cadmium L~d Solids
(""" ) (ug/l) (ug'l...) (1.m.lL) (=fl) (uglL) (m•/L)
<JO <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 47 <20 <0.30 3.7 <5.0
<JO <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <030 <3.0 <5.0
<10 <50 <5.0 <20 <0 30 <3.0 <5.0
<10 <50 <5.0 <20 <0 30 <3 0 <5.0
<10 <50 <5.0 <20 <0 30 <3 0 <5,0
<10 <50 <5.0 <20 <0.30 <3 0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 20 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 <5.0 27 <0.30 <3.0 <5.0
<JO <50 <5.0 <20 <030 <30 <5.0
Not Sampled Sy,tem Do= ...
<10 <50 <5.0 <20 <030 <3.0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5,0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<10 <50 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 <5.0 <20 <0.30 <3.0 <5.0
Not Sampled System Do,n
<JO 64 <5.0 <20 <0.30 <3.0 <5.0
<JO <50 30 <20 <0.30 7.5 7
<JO <50 11 <20 <0.30 <3.0 <5.0
<10 <50 30 <20 <0.30 <3.0 <5.0
<JO <50 18 <20 <O 30 <3.0 <5.0
<JO <50 29 24 <0.30 <3.0 20
<10 <50 <5.0 <20 <0 30 <3.0 <5.0
Not Sampled System Down
<JO <50 <5.0 <20 <0.30 <3.0 <5.0
50 1000 ,o 5000 5 "
-
Lower Dod;ery
MWl6
(DUPJ
--
:.'1311996
51:!.'l9%
713111996
11n11996
111711996
1:5/lm
5!1311997
8,'6']997
11112/1997
215/19911
i-'611998
&'611998
1\13,'1?98
Z'll/1999
5}\~1999
&'611999
ll/~1999
5,'8/2000
S/3,1200()
111&/2001
7111/:!00\
JIJ6l:ro2
7130,'~
\~2003
l,ow,r De<l<•tJ 7/:'.!41:?003
R•--s,._._ 111312004 s..., ...... J.'lt,~ 415/2004
&ZS.·~
IOl21!2004
Remedilltion Perfonnance Staruard
NA• N<'I AnBly~
-
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<l.0
<].0
<1.0
<1.0
<LO
<2.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0 -<i.O
<1.0
<1.0
S1
" " 37
32
" " " " 68
" " " " I)
I)
" "
IO
-
" 0.9
5.7
"" \\'rl wen. ,,
""' ""' ""' 2.2
<1.0 -rs-
u
Li
<IO
<1.0
<l.0
<IO
<IO
<l.0
<1.0
<20
<l.0
<l.0
<l.O
<1.0
<1.0
<1.0
<2.0
<l.0
<l.0
<1.0
NO
N•
No
<1.0
"""""' _,.., _,..,
<20
<2.0 <.ro-
<2.0
<1.0
3SOO 70
DI..= Dilution DUI'.~-
-
<2.0
<2.0
<20
<2.0
<2.0
<2.0
<Zh
<2.0
<2.0
"'' <20
<2.0
<2.0
Sampled
Sampled
Samphtd
<20 ....... ....... .......
<,0
<5'
<~ii <" <2.0
-
<l.O
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<:?-0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<20
<LO
<:1.0
<1.0 18
Dae To :>blo"uruon
Dae To :>~on
Due To '.:lbtlrnction
<1.0 28
Well Went
Well Went wen Went
<l O 6 2
<1.0 3.8 -;j.'0 -:r.s-
<LO 3.9
<1.0 3.6
200
- -- -
• 3.8 2,
26
2
0
3.2
21
39
23
1.9
1.2
<:LO
<:LO
<:2.0
<:1.0
<:1.0
<1.0
3.4
Dr;
Dr;
Dr;
1.2
TABLE 5
Summary of Groundwater Analyses
Wells MW-16 and MW-24
Lower Dockery System
<1.0
<LO
<LO
<l.O
<1.0
<1.0
<l.O
<:.o
<LO
<LO
<l.O
<LO
<1.0
<LO
.::: 0
<LO
<:LO
<:LO
<10
<l.O
<1.0
<1.0
<1.0
<LO
<:LO
<l.O
<LO
<:LO
<2.0
<1.0
<:1,0
<1.0
<LO
<LO
.;LO
<2.0
.;1.0
"'-0
.;].Q
.;LO
Page 1 of 2
<LO
<LO
--1.0
II
2
<l.O
.;].Q
<2.0
« 0
<:1,0
.;!,Q
<:J.0
<10
<:1,0
<:2,0
<10
<:LO
<:LO
<:].0
<;l,Q
NA
<:3,0
<30
<3,0
<3.0
<:3.0
.;3_0
<3.0
<:6.0
<3.0
<30
<3.0
<3.0
<30
<3,0
<:6,0
<:3,0
<30
<:3,0
<3,0
<30
'"' ,.
'" '" 3,0
11
--
270
310
1100
8)<1
"" 170
19<1
89<1
633
<50
,10
"' JOO uo
"' 300
'80
39<1
<lO
<,0
<:5,0
<:5,0
<,0
<5.0
<5.0 ,,
<lO
<,0
<,0
<5.0 ._,_o
<:.'1,0
<5.0 ,.,
<lO
<:.'1,0 w,o
Well w,u
64 <.'1.0
Sampled
Sampled
Sampled
120 <1.0
.;50 <l.O
1100
1100
»oo
3200
'800
670
810
HOO
319<1
"'oo
930
"' 1100
1)00
3300
"" 1900
Not
No
NO
"' -""""' .,_
m
<LO -<To-
<1.0
<1.0
--::ro-
.;LO
NA ~i".o -~:o _!:!_A_
<20
<:.o
.;3_0
<,0
NA -._25--i'i--NA--NA _2_:_
19
,so
<:SJ)
<1.0
<:1.0
<:1.0
<1.0
<1.0
<1,0
IOOO
<:25
<IO
3500
"' <10
33
NA
100-0
<1.0
NA
50
-
" 30
"' ,., ,.,
" " ,<0
193
«o
'" " " " " ,10
"'' '" -·--Sampled
«o
Well wen
WeD ,.,
«o -NA-
"'" NA
100
'" '"' 230
25-0
" .,.,
<,0
'" <S,
,10
81
" " 110
"' "' 130
-
'" '" "' 390
3.0
110
" '3-0
"' " 3011
12-0
" '" 1'0
'30
"' 270
Due To Ob«ruction
Due To Obstrnction
Due To Ob!tmction ,. '" w~ Dr;
We111 Dry
We111 Dry
100 1100
<50 .;Z(J -w.--NA-
.;50 44
NA NA
,00-0
-
<O ,i
--o.30
o ...
OA1
0A5
<:0.30
<o,i
.;Q 30
<I
<O 30
<0.30
<0"'
<O 3<1
<0,30
2.7
.;0.30
<0.30
0.37
19
" 031
OAS
II
<:0.30
11
" " " " 9.9
11 ., ,,
8.7
22
11
,.9
9.0
90
330
"1.0
1.'1.0
,.,
120.0
<3.0 -~-0
<30
<J.O
"
-
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
<O.ZO
NA -NA-
NA
NA
I.I
-
<10
<10
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA -NA-
NA
NA
,000
1800
5300
'100
NA
"" ,.,
"" 1900
'" '"" '" 270
"" ''° '"" 13011
1100
1'00
"O
" " 190
.;5_0
-
-
Lowot Dockery
MW24
(DUP)
--
2/lJ/!996
2/IJ/1996
512/1996
&'l/1996
l!nll996
2/.'i/1997
5/l)/1997
8/j,/1997
!!ll::11997
21Yl998
516/1998
816/1998
llf3/l998
21!1/1999
5.'1211999
81611999
llf2/l999
2117/2000
""""' ""2000
1118/2001
7111/2001
Ill~
7131r.!002
U28/2003
i-..-o.&,ry 7110'2003
R---•SJ>tao ____ JJ\Y20()4
s..,.-, .. J'1'M 415/2004
"""""' 10/21/2004
Renladilbon Perfommnce SUindsrd
Ni\-N..,.~7.00
-
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<J,0
<l.0
<1.0
<1.0
<1.0
<1.0
<1.0
<:1.0
<:i.O
<Io
<1.0
<l.O
<1.0
<I 0
<1.0
<:LO
<LO
<1.0 -<i.O
<I 0
<1.0
'' '' 1., '7 7.1
" 1,
17
19
" " " 33
" " " 1,
" " 1,
" I<
" 1,
10 1,
_.!}_
13 1,
i,
-
<l.O
<1.0
<l.O ..,
<l.O
<],0
<l.O
1,
<l.0
<LO
<1.0
<1.0
<1.0
<1.0
<:1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<:1.0
<l.0
<1.0
<\.0
<I 0
<1.0
«'
<JO
<I 0
-
<2.0
<2.0
<20
<2.0
<2.0
<W
<2.0
<2.0
<2.0
<2.0
<W
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0
<2.0 <5.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<LO
<LO
<:LO
<LO
<LO
<LO
<1.0
<1.0
<1.0
J.,O
<LO
<LO -4-:o-
<l.O
<1.0
<20--<sO
<2.0
«'
<5.0
<2.0
3500 70
DL"' Dilutioo DUP -~
-
<LO
<1.0
<LO
5.2
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<I 0
<1.0
<I 0
<l.O
<1.0
<1.0
<1.0
<l.O
<l.0
<l.0
<1.0
<1.0
<1.0 -:?i.O
<l.O
<1.0
<I 0
<1.0
<I 0
1.7
<1.0
<L.O
<I 0
<I 0
<10
<I.O
<1.0
<JO
<1.0
<10
<10
<1.0
<10
<10
<10
<10
<I 0
<I 0
<l.O
<l.O
<I 0
<I 0
<1.0 -<""iO
<l.0
<l.0
- ---- -
<1.0
<LO
<l.0
" <l.0
<l.0
<1.0
<LO
<!.0
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0 -<TO
<l.O
<1.0
2.8
TABLE 5
Summary of Groundwater Analyses
Wells MW-16 and MW-24
Lower Dockery System
<1.0
<1.0
<1.0
<l.O
<l.O
<l.O
<l.O
<1.0
<!.O
<LO
<IO
<L.O
<L.O
<\.O
<\.O
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<1.0
<1.0
<l.O
<l.O
<l.O
<1,0 <i:o-
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<l.O
<l.O
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
NA --:;;:1:0
NA
<LO
Page 2 of 2
<J.0
<LO
<LO
<1.0
'' <I 0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<J.0
<L.O
<1.0
<1.0
<LO
<1.0
<LO
<1.0
<1.0
<1.0
<LO
<1.0
NA --;-1:0
NA
<1.0
1000
<3.0
<3.0
<3,0
<)O
<J.0
<3.0
<)O
<3.0
<)O
<3,0
<3,0
<3.0
<)O
<3,0
<3,0
<)O
<)O
<3,0
<JO
<).0
<3.0
<3,0
<30
<JO
<3,0
<3,0
NA -~.O
NA
<)O
,oo
<JO
<10
<JO
<JO
<JO
<JO
<JO
<JO
<JO
<JO
<JO
<JO
<10
<10
<JO
<10
<10
<JO
<JO
<10
<10
<JO
<JO
<10
<JO
<JO
:-.A
<0,
NA
<10
""'
" " <10
<JO
<JO
<10
<10
<JO
<JO
<JO
<JO
<JO
"
<JO
<JO
JO
<JO
II
" <JO
<10
<JO
<JO
<JO
II
:-.A -<To-
<w
<IO
"
"' )70
" " " " "' " l<O
79
130
110
JIO
190
110
llO
160
IW
160
J,O
J,O ,oo
" 120
" 240 <\.0
.2'.:! __ E".!.
1'A NA
NA
<1.0
NA
3,00
3700
"00
2'00
'700
2500
2'00
<5.0
"" ""' '-"' "00
3000
""' 2'00
::,00
"OO ::,00
""' ""' "OO = "00
2200
"' ""' NA -noo
2100
2000
"
-
" <,0
'°" '°'' <,0
«o
'°'' <00
«o
'°'' <00 «o
<,0
«JO
'°'' <,0 .,,
'°'' <00
«o
'°'' «o
<,0
<,0
'°'' «o
NA -;;A-
<,0
NA
100
-
130
J,O
<lO
<lO
<lO
<lO
<lO
<lO
<lO
<lO
<lO
<,0
" <lO
<lO
<lO
<lO
<lO
<lO
<lO
<lO
<lO
<50
<50
<lO
<50
NA -NA-
<50
NA
"
no
"' <20
" <20
<20
<20
20
"I
<20
30
<20 uo
" " " " <20
,1
" <20
<,0
<20
<20
<,0
<,0
NA -:"IA-
<" NA
"""'
-
<0.3(1
<0.3(1
<0.30
<0.3(1
<0.3(1
<0,3(1
<0.30
<0.30
<I
<0.30
<0.30
<(1_3(1
u
<0.30
<0.3(1
<0.3(1
<0,30
<0.3(1
<0.30
<0.3(1
<0.30
<0.30
0.91
0.91
<0.30
'' 1-~
<0.30
NA
<0,30
J2
" <3.0
<)O
,:;J_0
,:;J_0
<3.0
,:;3_0
0
" ,.1 ,.,
u ,.1
<)O
''
<3.0
,:;3,0 ,.,
<30
<;J_o
,:;J_O
<J.O
<3.0
<3.0
NA -730
NA
<;3,0
-
NA
!'!A
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
SA
NA
NA
NA
NA
NA
NA
NA -NA-
NA
NA
-
<JO
19
<10
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
SA
NA
NA
NA
NA
NA
NA -NA-
NA
NA
1100
1000
15
79
" " " " J,O
IJ
91
" '" IW
30
130
130
,1
100
170 ..
" ,1
II
-
I
I Table 6
(iroundwater Level Data
Lower Dockery Sill-
Richmond Count~·, North Carolina
I Wl'il Date Sun-·uyc>d D,•pth to Corr,•,·kd
. Number Casing Groundwater Gro.
Elevulion (ft) 'ft)
LD-4 615/1996 14/U6 20.67 127.49
I 7/1/1996 20.83 127 .. H
7/31/1996 24.50 12.1.66
11/8/1996 29.59 118.57
21511991 Ut.% 129.20
I 5/1311997 29.08 119.08
815/1997 :m.04 111U2
11/1211997 32.79 115.37
2/4/1998 18.50 129.66
I 5/5/1998 29.36 118.80
815/1998 JJ.11 117.05
I 1/311998 30.63 117.53
2/10/J()(.)9 31.09 117.07
I 5/12/1999 31.92 116.24
81511999 32.77 115.39
11/2/1999 36.77 IIU9
2/16/2000 19.J7 121(79
I 5/8/2000 35.31 112.85
8/3/2(k)O 36.74 111.42
1/\8/2001 20.40 127.76
7/11/2001 21.93 126.23
I 1/16/2002 21.93 126.23
7/3012002 148.16 22.78 125.38
1/28/2003 20.07 1211.(19
7/1012003 45.44 102.72
I 1/1312004 28.60 119.56
6/28/2004 Not Mca!mred -System Suspended
11/20/2004 21.22 126.94
I LD-5 6/5/1996 1611.03 26.49 141.54
7/1/1996 34.66 lJJ.37
7/31/1996 45.48 122.55
11/8/1996 45.86 122.17
I 2/5/1997 25.51 142.52
5/1311997 50.26 117.77
8/5/1997 45.75 122.28
11/12/1997 45.75 122.28
I 214/1998 18.73 149.30
5/5/1998 45.39 122.64
8/5/1998 45.76 122.27
11/3/1998 4:5.78 122.25
I 2)10/1999 45.78 122.25
5/12/1999 45.74 122.29
8/5/1999 45. 75 122.28
11/2/1999 45. 74 122.29
2/1612000 25.()6 142.97 I 5/8/2000 45.42 122.61
8/312000 4S.77 122.26
1/18/2001 29.85 138.18
7/11/2001 26.65 141.JK I 1/16/2002 34.35 133.68
7/30/2002 168.03 29.72 138.31
l/28/200J 29.48 138.SS
7/10/2003 42.30 125.73 I J/1.1/2004 35.9S 132.011
6/2812004 Nol Mcasw-ed -System Su.~nded
11/20/2004 34.10 133.93
I
I
I I I I I I I I I I I I I I I I I 11 I I Well Number LD-2 LD·3 Table 6 Groundwaler U'"·cl l>·,da Lower Dockery Site l<khmontl Countv, North Carolina D~t,, Sun·t•yNI Dl'pth to Curn•cted Casing Groundwatrr Groundwater Elevation (ft) (0) l<:levatlon (R) 615/1996 154.80 26.93 127.87 7/1/1996 26.98 127.82 7/31/1996 35.50 119.30 11/8/1996 55.39 99.41 2/5/1997 25.28 129.52 5/13/1997 S4.45 100.35 8/5/1997 55.49 99.31 11/12/1997 55.48 99.32 2/4/1998 25.12 129.68 5/5/1998 55.02 99.78 8/5/1998 55.45 99.35 11/311998 55.43 99.37 2/10/1999 55.40 99.40 5/1111999 55.39 99.41 8/5/1999 55.43 99.37 11/2/199') 55.40 99.40 ])16/2000 25.42 129.38 5/8/2000 57.% 96.84 8/3/2000 NIA NIA 1/18/2()()\ 26.66 128.14 7/11/2()()\ 28.13 126.67 1/16/2002 28.26 126.54 7/30/2002 154.80 29.32 125.48 1/28/2003 26.25 128.55 7/10/2003 48.60 106.20 1/13/2004 47.95 106.85 G/28/2004 Nut Measured • System Suspended I Jn0/2004 27.35 127.45 6/5/1996 150.02 22.64 127.38 7/1/1996 22.70 127.32 7/31/1996 27.75 122.27 11/8/1996 35.18 114.84 715/1997 20.97 129.05 5113/1997 34.81 115.21 815/1997 36.92 113.10 11/1711997 44.76 105.26 714/1998 20,64 129.38 51511998 37.44 112.58 815/1998 39.58 \ I0A4 1113/1998 38.87 111.1 j 7110/1999 40.25 109.77 5/IVl999 42.65 107.37 8/5/1999 43.35 106.67 11/211999 50.98 99.04 2/16/200() 20.93 129.09 5/8/2()()() 50.64 99.38 8/3/200() 51.(1() 99.02 1/18/2001 22.37 127.65 7/11/2001 23.56 126.46 1/1612()()2 21.85 126.17 7/30/2()()2 150.02 24.55 125.47 lf281200J 22.05 127.97 7/10/2003 41.79 Hl8.23 1/13/2004 24,86 125. 16 6/28/2()()4 Not Measured • System Suspended 11/20/2()()4 23.25 126.77
I Table 6
Groundwater IA"vel Data
I
Lower Dockery Site
Uichmond County, North Carolina
\\'('JI IJatc Sun-·cyl'd Dl'pth to Corrected
Number Casing Groundwater Groundwater
I I<:levation (R) (ft\ Elc~·ation (ft)
1-IW 24* 2/14/1996 132.99 5.75 127.24
2/15/1996 5.95 127.04
YZJ/1996 6.9(1 126.09
I 2/21111996 6.15 126.84
Sn.11996 6.56 126.43
615/1996 6.35 126.64
7/1/1996 6.75 126.24
I
8/1/1996 6.91 126.08
1 l/lV1996 7.()6 125.93
2/5/1997 5.44 127.55
5/13/1997 6.65 126.34
8/5/1997 7,61 125.38 I 11/12/1997 6.86 126.13
2/4/1998 4.98 128.01
515/1998 6.37 126.62
8/5/1998 7.76 125.23
I 11/311998 7.JS 125.64
?110/1999 6.59 126.40
5/1211999 7.50 125.49
8/5/1999 8.31 124.68
I 11/2/1999 8.12 124.87
2/16f2000 5.()1 127.98
5/8/2000 7.47 125.52
8/312000 9.15 12.l.k4
I 1/1812001 6.03 126.96
7/11/2001 7.36 125.63
1/16/2002 7.01 125.98
7/31/2002 IJ2.99 8.28 124.71
I 1/2812003 6.00 126.99
7/10/2003 7.65 125.34
1/IJ/2(Kl4 6.67 126.32
6/211/2004 7.42 125.57
I 10/21/2004 6.47 126.52
LD-1 6/5/] 996 161.14 32.71 128.43
7/1/1996 33.52 127.62
I 7/31/1996 46.27 114.87
11/8/\996 56.64 104.50
215/1997 31.13 \30.01
5/13/1997 56.46 104.68
I 8/5/19'J7 56.45 104.69
11/1211997 56.47 104.67
2/4/1998 30.48 130.66
5/5/1998 55.3 105.84
I 8/5/1998 56.45 104.69
11/3/1998 56.42 104.72
2110/1999 56.40 104.74
5112/1999 56.40 104.74
I 8/5/1999 56.43 104.71
11/2/1999 56.43 10-t.71
211612000 31.32 129.82
5/8/2000 56.38 104. 76
I l:;/3'2000 NIA NIA
]/] 8/2001 32.59 128.55
7/11/2001 34.95 126.19
1/16/2002 34.00 127.14
I 7/30/2002 161.14 35.12 126.02
1/28/2003 32.09 129.05
7/10/2003 31.99 129.15
1/1312004 33.40 127.74
I 6/28/2004 Not Mea.-.urcd -System Suspended
11/20/2004 33.18 127.96
I
I
Table 6
I
Groundwater J,e,,el Data
Lower Dock{'!)' Sill'
H.ichmontl County, Norlh Carolina
\\'"II Dah• Surn•Jod D,,pth tu Curn•ct1>d
I
Numbt•r Casing Groundwater Groundwater
Klevalion (R) (ft) li:lcvation (ft\
l,m,-·l'r
Dock(•!)·
MW16 2/14/1996 159.97 31.40 128.57
I 2/15/19% 31.72 128.25
2/2311996 32.87 127.10
512/1996 32.70 127.27
6/5/1996 31.79 128.18
I 7/1/1996 31.89 128.08
7/31/1996 33.48 126.49
11/811996 :B.45 126.52
2/5/1997 30.13 129.84
I 5/1311997 33.01 126.96
815/19<)7 33.74 126.2.1
I J/12/1()()7 33.23 126.74
2/4/1998 29.63 130.:14
I 5/5/1998 32.22 127.75
815/1998 JJ.88 126.09
1 J/3/1998 33.43 126.54
2/10/1999 32.76 127.21
I 5/12/1999 33.35 126.62
8/5/1999 34.12 125.85
I J/2/1999 34.56 I ZS.41
2/16/2000 30.21 129.76
I 5/8/2000 NIA NIA
8/3/2000 NIA NIA
1/18/2001 Nol ~lca_,;ured -Obstruction
7/11/2001 32.62 127.35
I 1/16/2002 33.08 126.89
7/31/2002 159.97 34.26 125.71
i/2812003 31.06 128.91
7/1012003 32.72 127.25
I 1/13/2004 32.58 127.39
6/28/2004 32.45 127.52
10121/2004 32.34 127.63
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
APPENDIX A
LABO RA TORY REPORTS AND
CHAIN OF CUSTODY RECORDS
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Client
Report to:
STL Log#
Client Project #
Project Description Report Date
Mr. Steve Irminger
Irminger Consulting, Inc. 7015 Erinbrook Drive Concord, NC 28025
5450208
0004-00ltm
Macon Dockeryy
11-04-04
w~~Q,4LJ,,,
Weimerskirk, Project Manager
STL Savannah
5102 LaRoche Ave Savannah, Ga 31404
Page 1 of 10
iiiiiri# iU#@W M STL
I
I
I llillr&I
111911~111 STL
STL Savannah
I Client Irminger Consulting, Inc.
Work Order ID Macon DockerYY
Labor.:atory ID S450208*1
Sample ID UMSA EFF
I Matrix LI Sampled ' 10-21-2004
Percent Solids Received: 10-22 .:2004
RESULTS SUMMARY REPORT
I Pararmtar Method Batcl, Prep Analysis Analyst Result (),al Units Df RL Wl
Date Date
Acetone 8021 1B1029 10-30-04 10-30-04 EC 10 < ug/1 1.0 10 7.6
I Benzene B021 1B1029 10-30-04 lo-30-04 EC 1.0 < ug/1 1.0 1.0 0.1◄
Toluene 8021 1B1029 10-30-0'1 10·30-04 EC 1.0 < ug/1 1.0 1.0 0.lS
Total Xylenes B0'21 1B1029 10-)0-04 10-30-04 EC J.0 < ug/1 1.0 J.O 0.44
Surrognc> -
I ,1,,1, a-fr i floort1to711t•ll(? 8021 181029 f0-30-().1 10-30•0-1 cc ']i .. J 0
Chloroform 8021 1Bl029 10-30-04 10-30-04 lC LO < ug/1 1.0 1.0 012
1,1-Dichloroethane 6021 1Bl029 lo-30-04 10-30-04 EC LO < ug/1 1 0 1.0 0.19
I
1,1-Dichloroethene 8021 1B1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0.2]
1,2-0ichloroethene (total) 802] 1B1029 10-30-04 ID-30-04 EC 1.0 < ug/1 1.0 1.0 0 41
Me.thy1 ene chloride
(Di ch loromet:hane) 8021 181029 10-30-04 10-30-04 EC 2.0 < ug/1 1.0 2.0 0.10
I 1,1, I-Trichloroethane 8021 181029 10-30-04 10-30-04 EC 1.0 < ug/l LO 1.0 0.2'1
Trich1oroethene 6021 181029 10--10-04 10-30-04 EC 1.0 < ug/1 LO 1.0 0.14
Tetractiloroethene 6021 181029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0.17
Vinyl chloride 8021 181029 10-30-04 l0-30-04 EC 1.0 < ug/1 1.0 1.0 o.:m
I Sw ,·og,n~ -
Hromncll 1orn,ic rh,111(! 8021 181029 10-30-0:l I0-30-0-1 [( 110 :~ ·r o
Barlun 6010 1026M 10-26-04 10-26-04 UV 160 ug/1 1 50 1.0
I
Chrnmi"" 6010 1026H 10-?6-04 10-26-04 UV 10 < ug/1 l 10 1.1
llaf9"'0SC 6010 1026M 10-26-04 10-26-04 LN 18 ug/1 1 5.0 1 0
Lead 7421 1026) lQ-26-04 11-02-04 N>'ll 3.0 < ug/1 1 3.0 0.6B
Zinc 6010 10261-1 10-26-{)4 lo-26-04 UV 20 < ug/1 1 20 1.3
I Cadl'liull 7131 1026) 10-26-04 ll-01-04 ,:.1) O.JO < ug/1 1 0.30 0.21
Suspended Sol1ds 160.2 1022B 10-22-04 10-22-04 HP s.o < n-g/1 1 5.0
I
I
I
I
I Page 2 of 10
I
I
I
I 111ilil§il STL lllill§I El
STL Savannah
I Client Irminger Consulting, Inc.
Work Order ID Macon DockerYY
Laboratory ID S450208*2
Sl£Unpla ID MACON EFF
Matrix LI Sampled ' 10-21-2004
I Percent Solids Received: 10-22-2004
RESULTS SUMMARY RE.PORT
Par.mEtcr MethOd Batch Prep Analysis Analyst Result Qual U,,its OF RL IEL
I Date Date
Acetone 8021 181029 10-30-04 10-30-04 EC 10 < ug/1 LO 10 7 6
I Ben,ern, 8011 181029 10-30-04 10-JD-04 EC LO < ug/1 LO LO 0.14
Toluene 8021 181029 10-30-04 10-30-04 EC 1-0 < ug/1 1.0 LO 0.15
Total Xylenes 8021 IB1029 10-30-04 10-30-04 EC l 0 < ug/7 1.0 3.0 0.4'1
5urr0g:11:c -
I a,,1, a-Tri fluo,·oru·1ue11c SDn 181029 .10-30-Q.1 JO-30-0.1 f( 113 .. 1.0 .
Chloroform 8021 1Bl029 10-l0-04 10-3D-04 EC 1.0 < ug/1 1.0 1.0 0.12
1, 1-Di chloroethane 8021 181029 lD-l0-04 10-lD-04 EC LO < ug/1 1.0 1.0 0.19
1.1-Dic:hloruethene 8021 1BTD29 10-30-ot 10-30--<M EC B-5 ug/I 1.0 1.0 0.23
I 1,2-Dlchlorocthene {total) 8021 181029 10-30-04 10-30-04 EC 1.0 ug/I I 0 1 0 0.41
Methylene chloride
(Dichloromethane) 8021 1Bl029 10-30-04 lD-l0-04 EC 2.0 < ug/1 1.0 2.0 0.10
I 1,1,l-Trichloroethane 8021 181029 10-30-04 lD-30-04 EC l-0 < ug/1 1.0 1.0 0.24
Trichloroeth!!fle 8021 181029 10-)0-04 10-30-04 EC 1.0 < ul)/1 1-0 1.0 0.14
Tetrnchloroethcne 8021 101029 10-30-04 10-30-04 EC 1 3 ug/I 1.0 1 0 0.17
V1nyl chloride 6021 l.B1029 10-30-04 10-30-0<I EC l.O < ug/1 LO 1.0 O,lO
I ~wrng.1rc -
f'rror,;l)t:/11on;....., r.h,1n,, J!{)l,J 1/11()29 10-30-0--I 10-30-0-1 !X 120 ,, 1 .0
Barium 6010 1026M ll}-26-04 10-26--04 LJV so < ug/1 1 50 LO
Chromium 6010 1026M 11}-26-04 10-26-04 LJV 10 < ug/1 1 10 1.1
I Manganese 6010 1026M 11}-26-04 10-26·04 LJV s.o < ug/1 1 s.o 1.0
Learl 7421 1026) 10-26-04 11-02-04 WO 3 0 < ug/1 1 J.O 0-68
Zinc 6010 1026M 10-26-04 10-26-04 LJV 20 < ug/1 1 20 1-3
Cachium 7131 JD26] 10-26-04 11-01-04 ,..., O,lO < ug/1 1 0, JO 0,21
I Suspended Solids 160-2 10228 10-22·04 10-22-04 HP 5.0 < mg/1 l s.o
I
I
I
I
I Page 3 of 10
I
I
I
I IIUlrlll
lnl&II~ STL
STL Savannah
I Client Irminger Consulting, Inc.
work Order ID Macon Dockeryy
Laboratory ID 5150208*3
Sample ID UD EFF
I
Matr.ix LI Sampled ' 10-2]-2001
Percent Solids Received: 10-22-:2004
RESULTS SUMMARY REPORT
I
Pnranicter -Batth Prep Analysis Analyst Result Quo! lmits OF RL IIIL
Date Date
Acetone 8021 181029 10-30-04 10-30-04 EC 10 < ug/1 1.0 10 7.6
I Benzene 8021 181029 10-30-04 1D-30--04 EC 1.0 < ugfl LO 1.0 0.1-1
Toluene 8021 IB1029 10-30-04 10-30-04 EC 1.0 < ugf] 1 0 1.0 0-15
Total Xylenes 8021 181029 10-30-04 10-30-04 EC 3.0 < ug/l LO 3.0 OA4
.'iUftfJ!}dte •
I .1, .1. ,1-T 1· 1 fl110roro iuf'n.:• son IBJD29 W-30-IJ.I 10-30-(),1 EC 110 .. .LO
Chlorofom 8021 181029 10-30-04 10-30--04 EC 1.0 < ug/1 1.0 LO 0.12
1, 1-0ichloroethar:e 8011 181029 10-30-04 10-30-04 EC LO < ug/1 LO 1.0 0.19
1,1-0ichloroethene 8021 1Bl029 10--30-04 10-30-04 EC 1.0 < ug/1 1-0 1.0 0.23
I 1,2-0ichloroethene (total) 8021 1B1029 10-30-04 lD-30-04 EC 1.0 < ugf] 1.0 l.0 0.41
Methylene chloride
(Dichloromethane) 8021 181029 10-30--04 10-30-04 EC 2.0 < ug/1 1.0 ' 0 0.10
I 1, l,1-Trichloroethane 8021 lB1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 LO Q,24
Tri ch loroethene 8021 IB1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0.14
Tetrachloroethene 8021 IB1029 10-30-0, 10-30-04 EC 1.0 < ugfl 1.0 1.0 0.17
Vinyl chloride 8021 IB1029 10-30-04 10-30-o,t EC 1.0 < ug/1 1.0 1.0 0. 30
I 5urrvg,nt• -
Br omorhlt..-0~~1.f.,,1ne 80(.1 18.10.?9 10-JO-O,; 10-30•0:I ff 120 ,: 10
Bariun 6010 1026M 10-26-04 10-26-04 LN 85 U!l"I , 60 , 0
01romiU111 0010 1026M 10-26-04 10-26-04 LlV 10 < ugf] 1 10 11
I 1-tlnganese 6010 1021>1 10-26-04 10-26-04 LJV s.o < ug/l 1 s.o 1.0
Lead 7421 1026] 10-26-04 11-02-04 r,.1) 3 .0 ' ug/l 1 3.0 Q.68
Zinc 6010 102611 10-26-04 10-26-04 UV 20 ' ug/1 1 20 1..3
I Camrium 7131 1026] 10--26-04 11-01-04 ~'[I 0.30 < ug/1 1 O.JQ 0.21
Suspended Solids 160.2 1022B l0-22-04 10-22-04 HP s.o < mg/1 l s.o
I
I
I
I
I Page 4 of 10
I
I
I
I IIUlrllfl STL lilill~m
STL Savannah
I Client Inninger Consulting, Inc.
Woi:k Orde1: ID Macon DockerYY
t.aboratory ID S450208*4
Sample ID MW-16
Matrix LI Sampled ' 10-21-2004
I Percent Solids Received: 10-22-2004
RESULTS SUMMARY REPORT
Parn111eter ,.,trod Bat"1 Prep Analysis Analyst Rest! It Qual !liits DF Rl ml
I Date Date
Acetone 8021 lll1029 10-30-04 10-30-04 EC 10 < ug/1 1.0 10 7.6
I Benzene 8021 IB1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0-14
Toluene. 8021 181029 10-30-04 10-30-0t EC ,.o < ug/1 1.0 1.0 0.15
Total Xylenes 8021 1Bl029 10-30-04 10-30-Oi EC J.O < ug/1 1.0 3.0 0.4'1
5u,n:.'!'._).11e •
I a,.,,..1-T, Jf·Juo,·otoloern:.• ·· 8021 181029 i(}-30-0:I J0-30-1,1 EC 100 " 1.0
Chlorofonn 8021 lll1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0.12
1.1-0lchloroethane 8021 1B1029 10-30-04 10-30-04 EC 14 ug/1 1.0 1.0 0.19
1, 1-0ichloroetheno 8021 181029 10-30-04 10-30-04 EC 1.7 ug/1 1 .o 1 0 0 23
I 1,2-Dichloroethene (total) 8021 1B1029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1 .. 0 0.41
Methylene chloride
(Di ch lora:iethane) 8021 1B1029 10-3D-04 10-30-04 EC 2.0 < ug/1 1-0 2.0 0.10
I 1.1,1-Trichloroethane 8021 181029 10-30-04 10-30-04 EC 36 ug/1 1.0 1 0 0 24
Trichloroethcne 8021 lll1029 10-30·04 10-30-04 EC ,.o < ug/1 1.0 1,0 0.14
Tetrachloroethene B021 IB1029 10-30-04 10-30-04 EC 1.0 < ug/l LO 1.0 0.11
Vinyl chlorid~ 8021 181029 10-30-04 l.0-30-04 EC 10 < ug/1 l.D 1.0 0.30
I Surrog.JrC' -
Hro.mt:11 /mu1:~•f l1-1,1,• !l02J 16101!) 10-.W-0:1 10-30-0.1 EC 110 ., l D
Suspended Solids 160.2 10226 10-22-04 10-22-04 HP s.o < mg/1 l 5.0
Chrcnium 6010 1026M 10-26-04 10-26-04 LJV 10 < ug/1 1 10 1-1
I Manganese 6010 102&1 10-26-04 10-26-04 LJV s.o < ug/1 l s.o 1-0
Cad:tiuri 7131 1026) 10-26-04 11-01-04 NI-I) 0.30 < ug/1 1 0.30 o. 21
Lead 7421 1026) 10-26-04 11-02-04 tM) J.O < ug/1 1 l 0 0 68
I
I
I
I
I
I Page 5 of 10
I
I
I
I
11Bla111
@;§@@& STL
STL Savannah
I
Client I:raingor Consulting, I.nc.
Work Ox:der ID Macon DockerYY
1,aboratory ID $450208"'5
s:mnpl~ tn MW-.24
Matrix LI
Sampled : 10-21-2004
I Percent Solids
Received: 10-22-200·1
RESULTS SUMMARY REPORT
Parameter
lletllod Batch Prtp AnalysJs Analyst Result QIJal \.nits OF RL lll)t.
I
Date Dato
8011 181029 10-30-04 10-31>-04 EC 10 < ug/1 1.0 10 7.6
Acetone
I
8011 181029 10-30-IJ.1 10-30--04 EC 1.0 < Ug/1 l.0 1.0 0.14
Benzene
Toluene II021 181029 10-30-04 10-30--04 EC 1.0 < ug/1 l.O ).0 0.15
lotal Xy1enes 6021 181029 .U,..J0-04 10-3(N)4 EC 3,0 < ug/1 1.0 l O 0,44
J111ic•9.11e -
I
,1,,1,,i-f1•it-Juor!'>t,1luen(.!
· 8011 lf!U>:!9 10-30-01 10-JD-o,J re 101 " 1.0 ·"
Ch'l..,.,...._fu,•
.li!O:U l8l02Q 10-30-04 ]J}-30·04 EC 1.0 < ug/1 1.0 1.0 0.12
1, 1-Dichloroethane 8021 18102.9 10-30-04 10-30-04 EC 12 ug/1 1.0 1.0 0.19
I
I
l.1-0ichloroethene
8021 181029 10-30-04 10-30·04 EC 1.0 < ug/1 1.0 LO 023
1,2-Dichloroethene [total) 8D2l 181029 lD-30-04 10-30-04 EC 1.0 < ug/1 LO 1.0 0.41
Methy)ene chloride
(Oich lon:tll:!thane) 8021 181029 11>-30-04 10-30-04 EC z.o < ug/1 1.0 2.0 0.10
1,1,1~Trichloroethane 8021 lBl0W 11>-30-04 ll>-30·04 EC LO < ug/1 1.0 1.0 0. 24
Trichloroethene 8021 JB1029 lD-30-01 10·30-04 EC 1,0 < ug/1 1.0 1.0 0.14
Tttrachloroethene 8021 1Bl029 10-30-04 10·30-04 EC 1.0 < ug/1 1.0 1.0 0,17
Vinyl chloride 6021 l.131029 10-30-01 10-30-0◄ EC 1 O < ug/1 1.0 1.0 O.JV
Surru;;,:nc -
I
I
(1r(!lt;t,>1;hl111 v:'Jll;'thl'T"C 802J uuo:,g 10-JO.../J:: ID-.i'0-0-1 ff 110 $' 1 0
Suspended Solids 160,1 1022B 10-22-04 10-22-04 1W s.o < mg/1 1 5,0
Otr-lu-, 60JO 1029,f lD-26-04 10-27-04 LJV 10 < ug/1 1 10 1 1
~ 6010 10261,1 10-26-,04 10-27-04 UV 2000 ug/1 5.0 1 0
C.:uhi1.1'1 7Ul 1026) .U,..26--0< 11-01-04 N>,J) 0.30 < ug/1 1 0.J0 0.21
lead 7421 10263 10-26--04 11-02-04 Nffi 3.0 < ug/1 l 3.0 0.68
I
I
I
I
I
I Page 6 of 10
I
I
I
I El ii !lbRffl STL liillll~llffl
STL savannah
I Client ' Irminger Consulting, Inc.
work Order ID Mac:on Oockeryy
Laboratory ID S4.50208*6
Sample ID Trip Blank
Matrix LI Sampled ' 1 o-21-2 004
I Percent Sol.ida Received; 10-22-2004
RESULTS SUMMARY REPORT
Paramter Method Batch Prep Analysis Analyst Result O.,al Units Of RL 11ll
I Date Da.tc
Acetone 8021 161029 10-30-04 lD-30-04 EC 10 < ug/1 1.0 10 7,6
I
Benzene 8021 161029 10-30-04 lQ-l0-04 EC 1.0 < ug/1 1.0 1 0 0.14
Toluene 8021 151029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 10 0 .. 15
Total Xylenes 8021 181029 10-30-04 10-30-04 EC 3.0 < ug/1 1.0 3.0 0.114
-~ur ,vg~, te -
I ..1,.1,a-T, iflw,orolHenc SO~J l/J.10!9 10-30-01 10-30-0•l ff 113 ' 1.0
Chloroform 8021 161029 10-30-04 10-3Q-04 EC 1.0 < ug/1 1.0 1.0 0.12
1, 1-Dichlorocthane 8021 1Bl029 10-30-04 10-30-04 EC l 0 < ug/1 LO 1.0 0.19
1,1-Di chloroethene 8021 1Bl029 10-30-04 10-30-04 EC 1.0 < UjJ/1 1.0 1.0 0.23
I 1,2-Dichloroethene (total) 8021 IB1029 10-30-04 10-30-04 EC 1.0 < ug/1 LO 1.0 D-41
~~thylene chloride
(Di ch loroo:ethane) 8021 1BI029 10-30-04 10-30-04 EC 2.0 < ug/1 1.0 2-0 0.10
1,1, l-Trlchloroethanc B021 181029 10-30-04 10-30-04 EC 1.0 < Ug/1 1.0 1.0 0.24
I Trichloroethl!fle 8021 1Bl0Z9 10-30-04 10-30--04 EC 1.0 < ug/1 1.0 1.0 0.14
Tetrachloroethene 8021 161029 10-30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0.17
'11ny1 chloride 80>1 1910~9 ID--30-04 10-30-04 EC 1.0 < ug/1 1.0 1.0 0,30
I
Sur rC1g,1 tf..' -
Rrrmx:l1 lo, t..0111.'l"hrllli? SiJ!.I 16/029 10-.10-fi:I 10-30-0:/ ff JJO ·-J () .
I
I
I
I
I
I
I Page 7 of 10
I
I
I
I 11111 lal§II STL lililsll~IIJ
STL Savannah
I Client Irminger Consulting, Inc.
work Order ID Macon Dockeryy
Laboratory ID S450208"'7
Sample ID Method Blank
Matrix LI Sampled '
I Percent Solids Received:
RESULTS SUMMARY REPORT
Parnneter -Batth Prep Analysis Analyst Result (µII units OF R\_ wt.
I Date Date
Acetone 8021 1.81029 10·29-04 10-29-04 EC 1D < ug/1 1.0 lO '.6
Benzene 8021 1Bl029 10-29-04 10-29-04 EC 1.0 < ug/1 1.0 1.0 D.14
I Toluene 8021 IB1029 10-29-011 10-29-04 EC 1.0 < ug/1 1.0 l .. D O.IS
Total Xy1enes 8021 lB1029 10-29-04 10-29-04 EC 3.0 < ug/1 1.0 3.0 0,44
Stu rOf/,1 t@ ·
I ,1,,1,,1-Tri fJ1.101 owluenc 60::!1 1BJOi9 10-29-01/ 10-29-04 EC .'}J ., 1.0
Chloroform 8021 181029 10-29-04 10-29-04 EC 1.0 < ug/1 1.0 1.0 0.12
1,1-Dlchloroethane 8021 181029 10-29-04 10-29-01 EC 1.0 < ug/1 1.0 1.0 0.19
1,1-0ichloroethene 8021 1Bl029 10-29-04 10-29·04 EC 1.0 < ug/1 1.0 1.0 o. 23
I 1,2-0ichloroethene (total) 8021 1Bl029 10-29-04 10-29-04 EC 1.0 < ug/1 1.0 1.0 0 .41
Methylene chloride
(Dichlormethane) 8021 181029 10-29-()4 10-29-04 EC 2.0 < ug/1 1.0 2.0 0.10
1, 1,1-Trichloroethane 8021 181029 10-29-04 10-29-04 EC 1.0 ' ug/1 LO 1.0 0.2•
I Trichloroethene 8021 11U029 10·29·04 10-29-0'1 EC 1-0 ' ug/1 1.0 1.0 0.14
Tctrachloroethene 8021 181029 10-29·04 10-29-04 EC 1.0 < ug/1 1.0 l.O 0.17
Vinyl chloride 8021 1B1029 10-29-o-t 10-29-04 EC 1.0 < ug/1 1.0 1.0 0. 30
I
Stwrog.ne -
//romocf1 )oro1~ t/:,111(' 81121 JRjiJ]!) l0-2!J.i).1 111--?9-D,1 ff 110 ·:: I 0
BariUnt 6010 1026H 10-26-04 10-26-04 UV 50 < ug/1 1 50 1.0
Chr'omiu11 6010 1029! 10-26-04 10-26-04 UV 10 < ug/1 1 10 1.1
I Mar.ganese 6010 102f#,I 10-26-04 10-26-04 UV 5.0 < ug/1 1 5.0 LO
Lead 7'121 1026) 10-26-04 11-02-04 ,...., 3.0 ' ug/1 1 J.0 0.68
Zinc 6010 10261-1 10-26-04 10-26-04 LJV 20 < ug/I 1 20 1.3
CaOllium 7131 1026) 10-26-04 ll·0l-04 1W 0-30 < ug/1 1 0.J() 0.21
I Suspended Solids 160.2 10228 10·22·04 10-22-0'1 HP 5.0 ' ,rg/1 1 5.0
I
I
I
I
I Page 8 of 10
I
I
I
I HDiUl~D STL fliiU11~m
STL Savannah
I Client Irminger Consulting, Inc.
work Order ID Macon Dockeryy
Laboratory ID S4S0208*9
Sample ID Lab Control Standard Result
Matrix LI Sampled ' I Percent Solids Received:
LCS RESULTS SUMMARY REPORT
Parameter Metlwld Batch Spike Expected Units Spike l Ra:uracy
I Result Value Recovery Limit
Benzene 8021 1Bl029 18 20 ug/1 90 79-123
Toluene 8021 1B1029 18 20 ug/1 90 78-123
I Surrog.i.te -
a,a,a-Trifluoroto1uene -8021 181029 29 JO ug/1 97 71-124
1,1-Dichlorocth~ne 8021 191029 20 20 ug/1 100 70-130
I Trich1oroethene 8021 1Bl029 l!l 10 ug/1 95 70-llO
Surrogate -
Broroochloranethane ~ 8021 181029 12 10 ug/1 120 57-127
Barium 6010 1026M 2090 2000 ug/1 105 75-125
I ChrOfflum 6010 1026M 204 200 ug/1 102 75-125
Manganese 6010 1026M 517 500 ug/1 103 75-125
lead 7421 1026) 53.6 50.0 ug/1 107 80-120
Zinc 6010 1016M 502 SOD ug/1 100 75-125
I Cadm1u:n 7131 1026) 5.07 s.oo ug/1 101 80-120
Suspended Solids 160.2 lOUB 99.0 100 mg/1 99 80-120
I
I
I
I
I
I
I
I Page 9 of 10
I
I
I
I lillBUIII STL JUillliffll
STL Savannah
I
Client Irminger Consulting, Inc.
Work Order ID Macon DockerYY
Laboratory ID S450208•10
Sample ID Lab Control Standard Duplicate Result
Matrix LI Sampled
I Percent Solids Received:
LCS RESULTS SUMMARY REPORT
I
Para1Jater Method Batch Spike D<pected lklits Spike% Accuracy
Result Value Recovery Limit
Benzene 8021 Jlll029 18 20 ug/1 90 79-123
Toluene 8021 181029 18 20 ug/1 90 78-123
I Surrogate -
a,a,a-Ttifluorotoluene ~ 8021 Jll1029 31 30 ug/1 103 71-U4
l,1-0ich1oroethene: B021 181029 18 20 ug/1 90 70-130
I Trichloroethene 8021 181029 lB 20 ug/1 90 70-130
Surrogate -
BromochlurO'l'lethane 8021 181029 11 10 ug/1 110 57-127
Barium 6010 1026'1 2070 2000 ug/1 104 75-125
I Chromium 6010 1026M 201 200 ug/1 101 75·125
Manganese 6010 1026M 512 500 ug/1 102 75-125
Lead 742.1 1026] 51.0 50.0 ug/1 102 B0-120
Zinc 6010 1026'1 499 500 ug/1 100 75-125
I Cacbriun 7131 1026J 5.31 5.00 ug/1 106 80-120
Susperded Solids 160.2 1022B 103 100 "".1/1 103 80-120
I
I
I
I
I
I
I
I Page 10 of 10
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
STL SAVANNAH-STL Log# S450208
8
E
N
s u
w
•
8
D
•F33
E
p
u
<
*F53
•F54
•F36
XI
X
y
Data Qualifiers
Inorganic Data
The reported result is an estimated concentration that is less than the PQL, but greater thnn OJ
equal to the MDL
The reported value is an estimated because of the presence of matrix inle1ference.
The man ix spike recovery is not within contrnl limits See case narrative.
The result was detennined by Method of Standard Addition (MSA).
The compound wns analyzed for, but was not detected nt or above the MDL/PQL
The compound was analyzed for, but was not detected at or above the PQL-
The post~digestion spike for furnace AA analysis wns out of control limits, while samph:
absorbancc was less than 50% of spike absorbance
Duplicate analysis is not within control limits .
Organic Data
The analyte was found in the associated melhod blank
The reported result is fiom a secondary dilution
Control limits are established only for smrngate concentration levels specified by EPA methods
Because the sample was diluted pr-ior to rmolysis, st11Togatc recoveries are not 1eported
The reported result exceeded the calibration range of the instrument.
The reported result is an estimated concenuation that is less than the PQL, but greater than or
equal to the MDL.
The GC or HPLC confinnation criteria was exceeded °fhc Iclative percent difference is greater
than 40% between the two GC columns or HPLC detectors.
The compound was analyzed for, but was not detected at or above the MDllPQL.
The compound was analyzed f01 but was not detected at or above the PQL.
Because sunogate rccovc1ies were outside established limits the sample was re-extracted and/or
tc:analyzcd Compnrnble results were obtained
Because sunogate recoveties were outside established limits, the sample wns re~cxtracted and/or
rean::ilyzed. Both sets of datn are provided.
Smrogatc recovery was outside of established limits due to a coeluting matrix interference present
in the sample,
Internal standards recovered outside of adviso1y limits
Surrogate recovery was outside of advisory limits
Spike rec:oveiy was outside ofadviso1y limits
Universal
*F6 l The recoveries of the rnntrix spikes nre outside advisory limits due to the abundance o[ the target
analyte in the sample
*F65 Elevated detection limits were reported due to sample mntrix interfotence which required sample
or extract dilution.
*F73 Matrix spike 1ecoveries were outside advisory limits due to nmrrlx interference present in the
sample
*F82 Insufficient sample volume was available to pe1fo1m batch specific man·ix spikes
The analytical results for the above referenced STL Log# have been reported to the reporting limil (RL)
The lest results in this report meet all NEL-AP requirements for parameters for which ilCCreditation is
required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP,
this report may not be reproduced, except in full, without the written approval of the laboiat0ty.
I
I
I
( • COOLER RECEIPT AND INSPECTION FORM
Log Number: ,;> c;r;-~208
Number of Coolers Received: _ _;_/ __
Received By: --~/l'-'''-1"-'-f __ _
I
Project Mana/r:
Courier: __ Fed £X
Date: /~ 112/f <(
_Client: e /fJ C,. -
Client /,(,:,
Cooler Temperaturc(s) Upon Receipt: _______ L-f_..:._ ____ _
__ UPS __ Other
I
I
YES NO*
ls cooler te~perarure _56°C, with no frozen samples? ✓ NOTE: Jf>6"C and/or samples arc frozen AND multiple coolers arc received, list all
samoles associated with out-of-temo cooler(s\.
Circle One: Did the samples alTive ~tic,. hlu.-"ice, no ice, or other? ·-·-· . -··--· -•·-··-•
If other, then list . ·.:-•... .. . .~.-··-·
I
Are custody seals intact, if used? Al 'it If no seals are used then write NA In soacc orovldcd:
Did samples arrive in good condition with no breakage? ✓I
-Circle One: Type of packing used is: vermlcu1if€'buht1Je wra_Jl,,,(lr other.
I If other. then list: -
Is there a COC?
Circle On¢: ls the COC ~TL SavannDb COO or a client COCl ------. ••••••A•••
. :.~. --~-: . --:_;__ . ··-· ·-
I ls the COC filled out completely? ·-v
Is the COC filled out in ink and signed? ✓
I
Are all sample containers labeled? v
Are aJI sample labels legible? ---
Are all samples listed on COC illcluded in cooler? V ,
;
I Are ill! sample5 included in cooler listed on COC? ✓
Do sample IDs on contWnerS match sample IDs on COC? ,./
I Do containers contain sufficient volumes?
'Ill All boxes checked 'NO• require rill ,iotification and completioft of next 1 seclion1.
I 1d11 I-
I
I l'MSTAFF:
Client Contacted:
Contact;_________ Date: ________ _ YES_NO
I :::~~
I FCU046:07 22 04: I
I
I
- --
PROJECT REFERENCE
R I UISHEO BY:
----- --ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
STL
PROJECT LO_CplON
!STATE! N,
CONTRACT NO.
MATRIX
TYPE
RELINQUISHED BY: <gGHAJUREI
RECEIVED BY: IS<GNATURO
--- ---Serial Number 4 2 7 5 0 -~ STL Savannah
5102 laRoche Avenue
Savannah. GA 31404
Website: WWV!.st~inc.com
Phone: [phone]
fax: [phone]
0 Alternate Laboratory Name/1..ocation
Phone:
Fax:
DATE TIME RELINQUISHED BY: <S<GNATUREI
DATE TIME RECEIVED BY: CS!GHATUREI
PAGE OF
STANDARD REPORT
DELIVERY ~
DATE DUE. ____ _
EXPEDITED REPORT
DELIVERY 0
!SURCHARGE!
DATE DUE
NUMBER Of COOLERS SUBMITTED
PER SHIPMENT:
REMARKS
DATE TIME
DATE TIME
-
LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY:
lN\ 3
CUSTODY INTACT
Yl'S 0
NO 0
CUSTODY
SEAL NO.
LABORATORY REMARKS
STL8240-6&J (12/021