NCD980840409_19980320_Charles Macon Lagoon & Drum_FRBCERCLA RA_Monthly Progress and O & M Reports March - December 1997-OCR

,. ·, ..
•NA
MCDEMR
JAMES 8. HUNT JR.
GOVERNOR
WAYNE MCDEVITT
., SECRETARY
t,: <~· \:.: ·-. -.
• •' ! •-,) l.
WJLL~M L. MEYER
: DIRECTOR
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-· .,
. ",:-.~
. ;;·;
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• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Ms. Giezelle Bennett
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
61 Forsyth Street, l Ith Floor
Atlanta, Georgia 30303
.
DIVISION OF WASTE MANAGEMENT
March 20, 1998
RE: Response to Comments -November & December 1997 Monthly Progress
and O&M Reports
February 1998 Monthly Progress and O&M Report
Macon/Dockery NPL Site
Cordova, Richmond County
Dear Ms. Bennett:
The Sjperfund Section of the North Carolina Department of Environment and
Natural Resources (NC DENR) has received and reviewed the above documents ' for thelMacon/Dockery National Priority List (NPL) Site. The Superfund Section
offers the attached comments. Please note that the NC DENR did not receive the
JanuaJi' Monthly Progress and O&M Report. The January Monthly Progress and
O&M Report should be submitted immediately.
The Sjperfund Section of the NC DENR appreciates the opportunity to comment
on theJe documents. If you have any questions or comments, please feel free to
call m~at [phone], extension 349 .
Attach ent
Sincerely, ?.Ys //l-£s, (-~ ,<(~{
David B. Mattison, CHMM
Environmental Engineer
NC Superfund Section
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX 919-71 S·360S r EOUAL 0PPORTUN,T<, AmRMrnVC AcnON EMPLOYCR • 50% RCCYCLC0/10% POST-CONSUMCR PAPCR
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Ms. Giczclle Bennett
Comments
March 20, 1998
Page I
RESPONSE TO CO1'fMENTS -
NOVEMBER & DEGEMBER 1997 MONTHLY PROGRESS AND O&M REPORTS
I
Attachment 2 Table 6 -Air Quality Summary
1. Table 6 indicatJs that the air sample VE-01 collected on November 13, 1997 contained no
detectable conc~ntrations of 1,2-dichloroethene (1,2-DCE). However, laboratory
documentation indicates that air sample VE-OJ contained 2.3 milligrams per cubic meter
2.
I
(mg/m3) 1,2-DG:E. Please clarify this discrepancy.
Table 6 indicatjs that the Upper Dockery Air Stack air sample collected on August 7,
I 997 contained 2 mg/m3 toluene. However, laboratory documentation indicates that the
Upper Dockery Air Stack air sample contained no detectable concentrations of toluene.
Please clarify this discrepancy.
I Attachment 4 Table 4 -Groundwater Quality Summary
3. Table 4 indicatjs that the Upper/Lower Macon System effluent sample collected on
I February 5, 199
1
8 contained no detectable concentrations of barium. However, laboratory
documentation indicates that the Upper/Lower Macon System effluent sample contained
56 micrograms per liter (µg/1) barium. Please clarify this discrepancy.
I Attachment 5 Table 5 -Groundwater Quality Summary
4. Table 5 indicatel that the groundwater sample collected from the groundwater monitoring
well MW-15 onlFebruary 5, 1998 contained 0.4 µg/1 mercury. However, laboratory
documentation indicates that the MW-I 5 groundwater sample contained 0.66 µg/1
mercury. Pleas6 clarify this discrepancy.
5.
6.
Table 5 indicate~ that the groundwater sample collected from the groundwater monitoring
well MW-9 on I[ebruary 5, 1998 contained no detectable concentrations of acetone above
a laboratory quantitation limit of 50 µg/1. However laboratory documentation indicates
that this groundjvater sample was analyzed at a laboratory quantitation limit of I 00 µg/1.
Please clarify this discrepancy.
Table 5 indicatJ that the groundwater sample collected from groundwater monitoring
well MW-19 oniFebruary 5, 1998 contained 82 µg/1 zinc. However, laboratory
documentation indicates that the MW-19 groundwater sample contained no detectable
concentrations cif zinc. Please clarify this discrepancy .
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Ms. Giczellc Bennett
Comments
March 20, I 998
Page 2
7.
8.
Table 5 indicates that the February groundwater sample collected from groundwater I monitoring wen MW-21 was collected on February 5, 1998. However, laboratory
documentation knd chain of custody documentation indicate that the MW-21 groundwater
sample was collbcted on February 6, I 998. Please correct this oversight.
I Table 5 does not reflect the results of the groundwater sample collected from groundwater
monitoring welllMW-23 on February 5, 1998. Please correct this oversight.
Attachment 8 fable 2 -Groundwater Quality Summary
9. Table 2 indicatJ that the Lower Dockery effluent sample collected on December 5, 1996
was not analyzed for zinc content. However, laboratory documentation indicates that the
Lower Dockery !effluent sample contained no detectable concentrations of zinc. Please
clarify this discrepancy.
10. Table 2 indicatel that the Lower Dockery effluent sample collected on December 5, 1997
contained no detectable concentrations of zinc. However, laboratory documentation
indicates that thJ Lower Dockery effluent sample was not analyzed for zinc content.
Please clarify thil discrepancy .
FEBRUARY 1998 MONTHLY PROGRESS AND O&M REPORT
Results of Sampling aiid Testing and Other Data Received
I. The third sentenle in this section states that the effluent concentrations have been below
the Remedial Performance Standard. However, Table 2 -Summary oflnfluent and
Effluent Analytic~! Results indicates that the Lower Dockery effluent exceeded the
performance staridard concentration for manganese in February 1998. The Superfund
Section recogniz~s that the March 28, 1995 letter from Ms. Giezelle Bennett to Mr.
Kenny Gulledge provides for the discharge of treated groundwater to the onsite infiltration
gallery without tteating for manganese. However, this section should be revised to reflect
the manganese eiiceedance as well as the discharge requirements of the NC DENR
Division ofWatet Quality.
T•ble I Grn••'+" Q••J;1y S•mm,,y
2. Table I indicates that the Upper Dockery effluent sample collected on November 13, 1997
contained 55.6 µ!VJ barium. However, laboratory documentation indicates that the Upper
Dockery effluent 'ample contained 67.9 µg/1 barium. Please clarify this discrepancy .
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Ms. Giezelle Bennett
Comments
March 20, 1998
Page 3
3. Table I indicates that the Upper Dockery effluent sample collected on December 5, 1997
contained no dbtectable concentrations of zinc. However, laboratory documentation
indicates that the Upper Dockery effluent sample was not analyzed for zinc content.
Please clarify this discrepancy.
I Table 2 Groundwater Quality Summary
4. Table 2 indicatls that the Lower Dockery effluent sample collected on December 5, I 997
contained no dJtectable concentrations of zinc. However, laboratory documentation
indicates that tlie Lower Dockery effluent sample was not analyzed for zinc content.
Please clarify tliis discrepancy.
I
Table 3 Groundwater Quality Summary
5. Table 3 indicatJs that the Upper Macon Source Area effluent sample collected on
I
December 5, l 9i97 contained no detectable concentrations of zinc. However, laboratory
documentation indicates that the Upper Macon Source Area effluent sample was not
analyzed for zinb content. Please clarify this discrepancy.
I Table 4 Groundwater Quality Summary
6. Table 4 indicatel that the Upper/Lower Macon System effluent sample collected on April
8, I 997 contain~d 200 µg/1 barium. However, laboratory documentation indicates that the
7.
8.
I
Upper/Lower Macon System effluent sample contained no detectable concentrations of
barium. Please tlarify this discrepancy.
Table 4 indicatJ that the Upper/Lower Macon System effluent sample collected on April
8, 1997 containcid 30 µg/1 manganese. However, laboratory documentation indicates that
the Upper/Low~r Macon System effluent sample contained no detectable concentrations I
of manganese. ,lease clarify this discrepancy.
The note at the bottom of Table 4 indicates that the Upper/Lower Macon System effluent
sample collected on July 25, 1997 was analyzed for manganese only. However Table 4
indicates that no detectable concentrations of the other parameters were detected. Please
correct this table to reflect that no analyses, other than that for manganese, were
conducted .
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Ms. Giezelle Bennett
Comments
March 20, I 998
Page 4
9.
10.
Table 4 indicat s that the Upper/Lower Macon System effluent sample collected on I
December 5, 1 ~97 contained no detectable concentrations of zinc. However, laboratory
documentation indicates that the Upper/Lower Macon System effluent sample was not
analyzed for ziric content. Please clarify this discrepancy.
Table 4 indicaJs that the Upper/Lower Macon System effluent sample collected on
I
February 5, 19~8 contained no detectable concentrations of barium. However, laboratory
documentation 'ndicates that the Upper/Lower Macon System effluent sample contained
56 µg/1 barium. Please clarify this discrepancy.
Table 5 Groundwater Quality Summary
11. The duplicate rlsults (DUPLICATE 1) for the groundwater sample collected on
November 12, 1]997 from groundwater monitoring well MW-15 were inadvertently
omitted. Pl easel correct this oversight.
12. The duplicate results (DUPLICATE 2) for the groundwater sample collected on
November 12, J'997 from groundwater monitoring well MW-2A were inadvertently
• omitted. Please correct this oversight.
13.
14.
15.
16.
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Table 5 indicates that the groundwater sample collected from groundwater monitoring I
well MW-15 onlNovember 12, 1997 contained 356 µg/1 barium. However, laboratory
documentation indicates that the MW-15 groundwater sample contained 128 µg/1 barium.
Please clarify thi's discrepancy.
Table 5 indicatJ that the groundwater sample collected from groundwater monitoring
I
well MW-15 on February 5, 1998 contained 0.4 µg/1 mercury. However, laboratory
documentation ihdicates that the MW-15 groundwater sample contained 0.66 µg/1
mercury. Pleasei clarify this discrepancy.
Table 5 indicates that the groundwater sample collected from groundwater monitoring I
well MW-24 on November 12, 1997 contained no detectable concentrations oflead.
However, laboratory documentation indicates that the MW-24 groundwater sample
contained 4.3 µg/1 lead. Please clarify this discrepancy.
Table 5 indicates! that the February groundwater sample collected from groundwater
monitoring well MW-21 was collected on February 5, 1998. However, laboratory
documentation ahd chain of custody documentation indicate that the MW-21 groundwater
sample was collebted on February 6, 1998. Please correct this oversight.
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Ms. Giczcllc Bennett
Comments
March 20, 1998
Page 5
17.
I 8.
19.
20.
21.
Table 5 does not reflect the results of the groundwater sample collected from groundwater
' monitoring well MW-23 on February 5, 1998. Please correct this oversight.
Table 5 indicatl that the groundwater sample collected from the groundwater monitoring I
well MW-9 on February 5, 1998 contained no detectable concentrations of acetone above
a laboratory qu~ntitation limit of 50 µg/1. However laboratory documentation indicates
that this ground~ater sample was analyzed at a laboratory quantitation limit of 100 µg/1.
Please clarify this discrepancy.
Table 5 indicatel that the groundwater sample collected from the groundwater monitoring
well MW-I I oniNovember 13, 1997 contained 45 µg/1 zinc. However, laboratory
documentation irdicates that the MW-I I groundwater sample contained 20.7 µg/1 zinc.
Please clarify this discrepancy.
Table 5 indicatel that the groundwater sample collected from the groundwater monitoring
' well MW-19 on1February 5, 1998 contained 82 µg/1 zinc. However, laboratory
documentation ihdicates that the MW-19 groundwater sample contained no detectable
concentrations df zinc. Please clarify this discrepancy.
Table 5 indicatJ that the groundwater sample collected from the groundwater monitoring I
well MW-13 on November 11, 1997 was not analyzed for suspended solids content.
However, Iabonitory documentation indicates that the MW-13 groundwater sample
contained 84 mg1/I suspended solids. Please clarify this discrepancy.
I Table 6 Air Quality Summary
22. The note at the Jottom of Table 6 indicates that blank entries signify analysis results that
are beneath laboiatory detection limits. As stated in previous correspondence, please
denote the actual] detection limit (e.g., <10, <2.0) in order to prevent any confusion or
misrepresentations of the data. Entries in which no analyses were conducted should be
clearly indicated bn the tables as well. Please make the appropriate modifications.
23.
24.
The results ofthjNovember 13, 1997 and February 6, 1998 air sampling activities at air
sampling Iocatioris VE-01, OW-1, OW-3 and OW-5 have been inadvertently omitted from
Table 6. Please dorrect this oversight.
Table 6 indicates lhat the Upper Dockery Air Stack air sample collected on August 7,
1997 contained 2 lmg/m3 toluene. However, laboratory documentation indicates that the
Upper Dockery ~r Stack air sample contained no detectable concentrations of toluene.
Please clarify this discrepancy .
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Ms. Giczcllc Bennett
Commcnlc;
March 20, I 998
Pagc6
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Table 7 Groun water Level Data
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25. Table 7 indicatL that, on August 5, 1997, groundwater monitoring well LM-5 had a depth
to groundwatet of 66.68 feet (ft) and a corrected groundwater elevation of 119.91 ft.
Previous docuriientation indicates that the depth to groundwater was 66.84 ft and the
corrected groubdwater elevation was 119.75 ft. Please clarify this discrepancy.
Table 8 Summl-y of Mass voe Removal Estimates
26. The values protded for Average Total voe Concentration and Pounds ofVOC
Removed For Nfonth are incorrect in some cases. Please correct these oversights .
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R~CEtVEo
JAN 2 B 7998
SUPfRFUND Si:CTtoN
MACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
MONTHLY PROGRESS AND
O&MREPORT
DECEMBER, 1997
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Macon/Do<tkery Site
Richmond CounJ, North Carolina
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January 9, 1998
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 30365
Re: Macon/Docke Site -Cordova, North Carolina
Monthly Progr~ss and O & M Report -December 1997
Reply to: Technical Committee
c/o David L. Jones
Ingersoll-Rand Company
114 Spencer Road
Cassopolis, Michigan
Phone: [phone]
Fax: [phone]
Dear Ms. Bennett: 1
On behalf of the Maco , ockery Site Group ("Group"), the December 1997 Monthly Progress and
0 & M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS ' of the Unilateral Administrative Order (effective date -May 30, 1992) for the Macon/Dockery Site.
This report describes cictivities which occurred during the month of December as part of the
Remedial Action phase rf this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH DECEMBER 1997:
• Mooilily •=plig of<he w,c, effio~, from ilie =edia<ioo sysloms.
• Continued O & M of systems.
RESULTS OF SAMPILING AND TESTING AND OTHER DAT A RECEIVED:
• A summary of Je laboratory results for December sampling of the remediation systems is
included in this Jrogress report. Tables 1 through 4 summarize the analytical results for the
four groundwat~r treatment systems. The reported effluent concentrations are below the ' remediation performance standard except for the manganese concentration reported in the
effluent samples ~ollected December 5, 1997 from the Lower Dockery Remedial System and
Macon Source .f.rea Remedial System. The manganese concentrations reported by the
laboratory for both sites was 160 micrograms per liter (ug/L). The Remedial Performance
Standard for the~e sites is 50 ug/L .
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Ms. Giezelle Bennett
January 9, 1998
Page No. 2
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Upper Dockery flow meter reading for December totaled 78,332 gallons. The system was
operational 69% bf the time averaging 1.88 gallons per minute (GPM). Mass VOC removal
was 0.07 poundJ for the month and the cumulative is 7.54 pounds.
I
Lower Dockery flow meter reading for December totaled 272,079 gallons. The system was
operational 79% bf the time averaging 6.51 GPM. Mass VOC removal was 0.14 pounds for
the month and tlie cumulative is 6.44 pounds.
Macon Source jea flow meter reading for December totaled 114,452 gallons. The system
was operational 1100% of the time averaging 2.75 GPM. Mass VOC removal was 0.12
pounds for the month and the cumulative is 2.13 pounds.
Upper/Lower Mlon flow meter reading for December totaled 844,299 gallons. The Upper
Macon system wils operational 97% of the time in December. The Lower Macon system was
operational 97% bf the time in December. The combined system flow averaged 20.21 GPM.
Mass VOC rem6val was 0.11 pounds for the month and the cumulative is 2.90 pounds.
I .
TASKS PLANNED FOR JANUARY 1998:
• Monthly samplijg of the remediation system effluents
• Continue O &M lof systems
• Request regulatol approval to treat the Upper/Lower Macon infiltration galleries with either
hydrogen peroxide, acetic acid or citric acid
I PROBLEMS AND DELAYS:
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I December 4-5, 1997 -The Upper/Lower Macon System and Lower Dockery metals treatment
units were backwkhed in an attempt to prevent channeling and plugging of the filter media.
The backwash abpears to have improved the metals treatment unit performance at the
Upper/Lower Macon System. The Lower Dockery System still appears to have flow
restrictions throu~h the primary metals filter unit. As a result, flow has been temporarily
diverted to only the secondary treatment unit.
I
December 12, 1997 -The Upper/Lower Macon infiltration galleries were discovered to be
in an overflow sthtus. Groundwater extraction wells UM-2, UM-4, and UM-6 were taken
' . off-line to allow the water level in the infiltration galleries to drop. On December 18, 1997,
wells UM-2 and UM-4 were placed back into operation. Groundwater extraction well UM-6 ' remained in an ot'f-line condition at the end of the December reporting period.
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Ms. Giezelle Bennett
January 9, 1998
Page No. 3
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In a letter dated I1ovember 17, 1997 The MDSG requested approval from the EPA to treat
the Upper/Lower Macon infiltration galleries with commercial bleach (sodium hypochlorite).
The EPA approvdd the dosage recommendation on December 3, 1997. The North Carolina
Department ofN~tural Resources (DENR) disapproved the use of commercial bleach in a
letter dated Deceriiber 18, 1997. The D ENR requests that the infiltration galleries be treated
with either hydrdgen peroxide, acetic acid, or citric acid. The MDSG is considering the
vaious options and the appropriate dosages. A recommendation should be made to the EPA,
under separate co~er, in January regarding this issue.
December 12, 18l 23, 1997 -The Upper Dockery Remedial System was down on each of
these days because of a high water level alarm in the airstripper sump. The alarm water
levels were adjus/ed and the system was running when the O&M contractor left the site.
I December 12, 18, II 997 -The Lower Dockery Remedial System was down on these dates due
to a high water le✓el alarm in the airstripper sump. The reason for the high water level alarm
condition was restl-icted flow through the metals treatment units. The metals treatment units ' were backwashed and their performance was only slightly improved. On December 18,
1997, the primaij metals treatment unit was turned off and the flow was directed only
through the secondary unit. The metals treatment unit manufacturer is being consulted for
information to coi'rect the problem with flow in the primary unit.
Percent operationli for each system: Upper Dockery 69%
spectfully Submitted,
Lower Dockery 79%
Upper Macon 97%
Lower Macon 97%
Macon Source Area
SVE system
100%
100%
David Jones f"O 1\....:
Project Coordinator
cc: Macon/Dockery Site Group Members
I
Paul Furtick, RM1, Inc.
David Mattison, NC Super Fund Section
Mike Profit, CDM Federal
Sample Date
Location
UD Effluent 2/13/96
2/14/96
2/14/96
2/15796
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
8/1/96
9/4/96
I 0/1/96
11/7/96
12/5/96
1/6/97
2/5/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
8/7/97
9/5197
10/2/97
11/13/97
12/5/97
Remediation Performance Standard
NA"' Not Analyud
Note: • Acetone confirmed by Method 8260
I, I -Dichloroethane
(ug/L)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
3500
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Table I
Groundwater Quality Summary
Upper Dockery
Macon/ Dockery Site
Richmond County, North Carolina
· 1, I -Dichloroethene Cis/trans-1,2-Dichloroethene Tetrachloroethene
(ug/L) (ug/L) (ug/L)
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <LO--
<l.0 <1.0 <1.0
<l.0 <1.0 <1.0
<1.0 <l.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <l.0 <1.0
<1.0 <l.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <l.0 <1.0
<1.0 <LO <1.0
<1.0 <l.0 <1.0
<1.0 <1.0 <1.0
1.5 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
7 70
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I, 1, 1-Trichloroethane Trichloroethylene Toluene
(ug/L) (ug/L) (ug/L)
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
---<1.0 --1~0----<1~0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 3.9
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <l.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<l.O <1.0 <l.O
<l.O <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 • <1.0
200 2.8 1000
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Sample Date
Location
UD Effiuent 2/13/96
2/14/96
2/14/96
2/rs/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
8/1/96
9/4/96
I0/1/96
I 1/7/96
12/5/96
1/6/97
2/5/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
8/7/97
9/5/97
10/2/97
I 1/13/97
12/5/97
. . Remediation Performance Standard
NA~ Nol Analyzed
Note: • Acetone confirmed by Method 8260
Total Xylenes
(ug/L)
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<1.0
<1.0
400
•
Table I (Continued)
Groundwater Quality Summary
Upper Dockery
Macon/Dockery Site
Richmond County, North Carolina
Acetone Chromium Barium Manganese
(ug/L) (ug/L) (ug/L) (ug/L)
70•F32 16 71 40
35•F33 15 53 14
<IO II 56 12
<IO 12 53 14
<IO <IO 53 II
<IO II 55 12
<IO <IO <50 8.3
<IO 13 <50 9.6
25 <10 <50 6.9
28 II 50 <5.0
52 <10 <50 <5.0
<IO <10 <50 <5.0
<IO <IO <50 <5.0
20 14 51 7
<IO <IO 55 <5.0
<IO <IO <50 5.9
<IO 15 59 <5.0
<IO 12 54 5.1
<IO 13 54 <5.0
<IO 15 61 5.9
<IO <10 69 <5.0
<10 <IO 63 <5.0
<IO <IO 60 7.2
<IO <IO 52 <5.0
<IO <IO 55 <5.0
<IO <IO <50 <5.0
<IO <IO 110 5.2
<IO <IO SO.I <5.0
<1.0 12.1 ~ -~ 18.6
<l.Q. <10 • <50• <5.0 •
3500 50 1000 50
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Zinc Lead Suspended Solids
(ug/L) (ug/L) (mg/L)
22 <3.0 14
<20 <3.0 II
<20_ _<J.Q_ --<5.0
<20 <3.0 <S.O
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 :<3.0 IO
<20 <3.0 <5.0
<20 <3.0 5
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 8
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <S.O
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
24.8 <3.0 <5.0
(§}? <3.0 • <5.0 •
. ,ooo 15
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Sample Date
Location
LD Influent 2/13/96
2/14/96
2/14/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
2128/96
3/8/96
4/3/96
5/3/96
6/5/96
8/1/96
1117/96
3/12/97
5/14/97
817/97
11/13/97
Remediation Pcrfonnance Standard
Note: A blank means below detection limit
Chlorofonn
(ug/L)
I.I
1.3
<1.0
1.6
<1.0
1.2
3.3
2.5
1.2
<1.0
2
<1.0
<1.0
<1.0
<2.0
<2.0
<5.0
<1.0
<1.0
<1.0
• Table 2
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond County, North Carolina
I, I -Dichloroethane 1, 1 -Dichloroethene Cis/trans-1,2-Dichloroethene
(ug/L) (ug/L) (ug/L)
80 33 <1.0
IJ0E 43 <1.0
80 13 <1.0
94E 39 1.8
64 16 2.2
82 32 I. 7
95 35 2.6
5.8 ID0 <1.0
93E 33 <1.0
92 35 <1.0
I ID 47 <1.0
79 36 <1.0
71 30 1.7
67 32 I.I
83 27 <4.0
69 28 <2.0
66 21 <5.0
62 25 <1.0
47 15 <1.0
33 13 <1.0
3500 7 70
•
Methylene chloride I, I, I-Trichloroethane
(ug/L) (ug/L)
<2.0 40
<2.0 37
<2.0 15
1.7 39
2.5 18
<2.0 29
<2.0 31
<2.0 54
<2.0 30
<2.0 30
<2.0 34
<2.0 28
<2.0 40
2 42
<2.0 54
<4.0 38
<ID 23
<2.0 23
<2.0 18
<2.0 12
5 200
•
Sample Date
Location
LD Influent 2/13/96
2/14/96
2/14/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
8/1/96
11/7/96
3/12/97
5/14/97
8/7/97
11/13/97
Remediation Pcrfonnance Standard
Note: A blank means below detection limit
Trichloroethylene Benzene
(ug/L) (ug/L}
6.4 <2.0
8.6 <2.0
<5.0 <2.0
9 <2.0
6.6 <2.0
8.4 <2.0
8.7 <2.0
5.2 1.8
7.4 <2.0
6.4 <2.0
6.7 <2.0
6.6 <2.0
5.4 <2.0
5.2 <2.0
5.9 <2.0
5.8 <2.0
<5.0 <5.0 F34
6.2 <1.0
4.1 <1.0
3.5 <1.0
2.8
• TABLE 2 (Continued)
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond County, North Carolina
Toluene Total Xylenes Chromium
(ug/L} (ug,1..) (ugiL)
17 <3.0 <IO
8.3 <3.0 <IO
<2.0 <3.0 <IO
8.3 <3.0 <IO
6.5 <3.0 <IO
5.3 <3.0 <IO
4.3 <3.0 <IO
13 3.4 14
1.3 <3.0 <IO
<2.0 <3.0 <IO
<2.0 <3.0 <IO
<2.0 <3.0 <IO
<2.0 <3.0 <IO
2.5 <3.0 <IO
<2.0 <6.0 <IO
<2.0 <6.0 <IO
<5.0 <15 <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
1000 400 50
•
Barium Manganese Zinc Cadmium Suspt::nded Sc!id~
(ug/L) (ug/L) (ug/L) (ug/L) (mgiL)
<50 260 270 <0.30 <5.0
<50 250 120 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 240 110 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 200 84 <0.30 <5.0
<50 190 81 <0.30 <5.0
<50 240 240 <0.30 <5.0
<50 120 77 <0.30 8
<50 <5.0 <20 <0.30 <5.0
<50 95 30 <0.30 <5.0
<50 160 39 <0.30 <5.0
16 63 200 0.91 <5.0
<50 230 46 <0.30 <5.0
<50 110 <20 <0.30 5
<50 230 <20 <0.30 <5.0
<50 76 <20 <0.30 <5.0
<50 150 <20 <0.30 <5.0
<50 130 <20 <0.30 <5.0
<50 200 <20 <I <5.0
1000 50 5000 5
•
Sample Date
L:,.;:.;tiu11
UMSA Effiuent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
11/7/96
12/5/96
1/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
7/2/97
gn;91
9/5/97
10/2/97
11/13/97
12/5/97
Remediabon Perfonnance Standard
Note: NA= Not Analyzed
DUP -duplicate
Chloroform I, I -Dichloroethane
(:.:g/L) (ug.n_)
<l.O <1.0
<LO <l.O
<1.0 <1.0
<1.0 <1.0
<I.0 <I.0
<LO <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <l.O
<1.0 <1.0
<1.0 <LO
<1.0 <LO
<1.0 <1.0
<1.0 <I.0
<1.0 <LO
<1.0 <l.O
<1.0 <l.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <J.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
3500
•
Tablc3
Groundwater Quality Summary
Upper Macon Source Area
Macon/ Dockery Site
Richmond County, North Carolina
l, 1 • Dichloroethene Cisltrans-1,2-Dichloroethene Tetrachloroethene
(1_1g!L) (ug/L) (ug/L)
<LO <l.O <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <I.0
<1.0 <1.0 <LO
<I.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0 <1.0 <LO
<l.O <1.0 <1.0
<LO <1.0 <1.0
<l.0 <1.0 <LO
<LO <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <I.0 <1.0
<1.0 <I.0 <l.O
<LO <l.O <l.O
<1.0 <1.0 <1.0
<I.0 <I.O <1.0
<1.0 <LO <1.0
<1.0 <LO <1.0
<LO <LO <1.0
<1.0 <1.0 <l.O
<1.0 <LO <J.O
<1.0 <1.0 <1.0
<I.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <l.O <1.0
<1.0 <1.0 <LO
<1.0 <LO <LO . <l.O . <1.0 <1.0
7 70
•
I, I, I-Trichloroethane Trichloroethylene
(ug/L) (ug/L)
<1.0 <1.0
<1.0 <1.0
<1.0 <I.O
<1.0 <1.0
<l.O <LO
<l.O <1.0
<l.O <1.0
<LO <l.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<l.O <LO
<J.0 <1.0
<1.0 <I.O
<1.0 <1.0
<1.0 <l.O
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<LO <i.O
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <1.0 . <1.0 <1.0
200 2.8
•
Sample Date
Location
U/1.lSA Etllucnt 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
7130/96
9/4/96
I0/1/96
11/7/96
12/5/96
I/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
712/97
8/7/97
9/5/97
1012/97
11/13197
12/5/97
Remedianon Perfonnance Standard
Note: NA a Nol Analyzed
DUP -duplicate
Vinyl chloride
(uglL)
<I.O
<1.0
<1.0
<l.O
<1.0
<1.0
<1.0
<l.0
< 1.0
<l.O
<1.0
<1.0
<l.O
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<1.0
<LO
<1.0
<LO
<LO
<LO
<LO
<LO
<LO
<1.0.
Benzene Toluene
(uglL) (uglL)
<I.O <l.O
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <l.O
<1.0 <LO
<I.0 <l.O
<I.O <1.0
<1.0 <LO
<1.0 2.9
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <I.0
<LO <1.0
<LO <1.0
<LO <1.0
<LO <LO
<LO <LO
<LO <LO
<1.0 <1.0
<l.O <LO
<1.0 <LO
<_1.0 <LO
<1.0 • <LO.
1000
•
Table 3 (Continued)
Groundwater Quality Summary
Upper Macon Source Area
Macon/Dockery Site
Richmond County, North Carolina
Chromium Barium Manganese
(uglL) (uglL) (uglL)
16 i50 330
<IO 110 190
<IO 110 160
<IO 100 140
<IO 130 170
<IO · 120 120
<IO 120 70
<IO 130 51
<IO 120 37
<IO 110 27
<IO 120 26
<IO 130 22
12 110 14
<IO 200 110
II 170 68
<IO 130 13
<IO 140 13
<IO 170 17
<IO 200 46
<IO 160 29
<IO 130 30
<IO 200 30
12 210 95
<IO 240 74
<IO 180 41
II 230 250
<IO 130 27
<IO 185 31.5
<IO 129 84.2
<IO, 150• 160-
50 1000 50
• . '
Zinc Cadmium Lead Mercury Suspended Solids
(uglL) (uglL) (uglL) (uglL) (mglL)
i'+ <G.30 4.2 , .. M
20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 0.26 18
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3,0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3,0 <.2 5
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 6
<20 <0.30 <3,0 NA <5.0
41 <0.30 9.2 NA 23
26 <0.30 66 NA 16
<20 0.47 <3.0 NA 24
<20 <0.30 <3.0 NA 26
<20 <0.30 <3.0 <0.20 5
25 <0.30 3.5 NA 120
<20 <0.30 <3.0 NA 8
<20 <0.30 <3.0 NA <5.0
<20 <0.30 <3.0 NA 7
35 <0.30 <3.0 NA 100
<20 <0.30 <3.0 NA <5.0
<20 <0.30 <3.0 NA <5.0
40 <0.30 4.8 NA NA
<20· <0.30 <3.0 NA 22
<20 <0.30 <3.0 NA II
<20 <I <3.0 NA 8 @) <0.30 ~ 6,5 • NA-<5.0 ,
5000 5 15 I.I
•
Sample Date
Location
U/L Effiuent 2/21/96
2/22/96
2/22/96
2/23/96
2/24/96
2/25/96
2/28/96
3/8/96
3/16/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
11/7/96
12/5/96
1/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
7/2/97
7/25/97
817/97
9/5/97
10/2/97
11/13/97
12/5/97
Remed1auon Perfonnance Standard
Note. 7/25/97 Sampled for Manganese only.
DUP -duplicate
NA= Not Analyzed
Chlorofonn l,I • Dichloroethane
(ug/L) (ug/L)
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<l.0 1.8
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<l.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 < 1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 2.4
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0 , <1.0 -<1.0
3500
•
Table 4
Groundwater Quality Summary
Upper/Lower Macon System
Macon/ Dockery Site
Richmond County, North Carolina
1,1-Dichloroethene Cis/trans-1,2-Dichloroethene Methylene chloride
(ug/L) (ug/L) {ug/L)
<1.0 <1.0 <2.0
1.8 <1.0 16
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<l.O <1.0 <2.0
<l.0 <1.0 <2.0
<l.0 1.6 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<l.0 <LO <2.0
<1.0 <1.0 <2.0
<l.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 1.8 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0 . <1.0 -<1.0 -<2.0
7 70 5
•
Tetrachloroethene I, I, 1-Trichloroethane
(ug/L) {ug/L)
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <J.0
<LO <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
. <LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
. <1.0 . <1.0
200
•
Sample Date
Location
U/L Effiuent 2/2 J/96
2/22/96
2/22/96
2nJ/96
2124/96
2/25/96
2/28/96
3/8/96
3/16/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
I ln/96
12/5/96
1/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
7/2/97
7/25/97
8/7/97
9/5/97
10/2/97
I 1/13/97
1215197
Remed1at1on Performance Standard
Note: 1ns197 Sampled for Manganese only
DUP · duplicate
NA= Not Analyzed
Trichloroethylene
(ug/L)
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
1.9
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0'
2.8
•
Toluene Chromium
(ug/L) (ug/L)
<1.0 <JO
<1.0 130
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
2.1 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <JO
<1.0 <10.
1000 50
Table 4 (Continued)
Groundwater Quality Summary
Upper/Lower l\.facon System
Macon/Dockery Site
Richmond County, North Carolina
Barium Manganese Zinc
(ug/L) (ug/L) (ug/L)
59 JOO 98
70 120 120
72 120 120
80 140 130
83 150 150
90 160 170
<50 32 59
<50 39 56
<50 31 51
<50 44 54
31 JO 21
<50 1.5 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
39 <5.0 <20
<50,(s-p <5 o,<-< <20
(@) © <20
<50 <5.0 <20
<50 <5.0 <20
<50 19 <20
<50 36 <20
<50 5.4 <20
<50 <5.0 <20
<50 6.3 <20
<50 <5.0 <20
<50 • <5.0 • @, .
1000 50 5000
•
Lead Suspended Solids
(ug/L) (mg/I.)
4 <5.0
5.2 <5.0
5.1 <5.0
4.9 <5.0
3.7 <5.0
3.6 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
3.6 JO
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 24
<3.0 <5.0
<3,0 <5.0
<3.0 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
3.1 NS
<3.0 <5.0
<3.0 25
<3.0 <5
<3.0 . <5.
15
•
System Month
Upper Dockery Mar-96
Apr-96
May-96
Jun-96
Jul-96
Aug-96
Sep-96
Oct-96
Nov-96
Dec-96
Jan-97
Feb-97
Mar-97
Apr-97
May-97
Jun-97 • Jul-97
Aug-97
Sep-97
Oct-97
Nov-97
Dec-97
Lower Dockery Mar-96
Apr-96
May-96
Jun-96
Jul-96
Aug-96
Sep-96
Oct-96
Nov-96
Dec-96
Jan-97
Feb-97
Mar-97
Apr-97
May-97
Jun-97
Jul-97
Aug-97 • Sep-97
Oct-97
Nov-97
Dec-97
TABLES
SUMMARY OF MASS voe REMOVAL ESTIMATES
MACON/DOCKERY SITE
RICHMOND COUNTY, NORTH CAROLINA
PAGE 1 OF 2
Average Total
Monthly Flow voe Pounds of voe
Volume Concentration Removed For Month
(gallons) (ug/L) (Pounds)
400,155 197 0.63
286,151 140 0.32
66,826 337 0.18
97,350 128 0.10
163,426 107 0.14
218,330 344 0.60
149,420 293 0.35
140,191 293 0.33
438,013 444 1.62
161,903 444 0.60
294,071 131 1.09
267,596 131 0.29
250,068 131 0.27
276,556 75.5 0.30
289,938 78 0.18
135,575 78 0.08
99,896 78 0.06
70,967 54 0.03
56,256 54 0.03
277,505 54 0.12
143,168 108 0.13
78,332 108 0.07
328,448 186 0.49
191,090 65 0.10
245,715 92 0.18
8,619 145 0.01
151,827 222 0.27
126,232 475 0.48
63,833 196 0.10
460,379 176 0.65
183,210 140.8 0.22
137,594 140.8 0.16
286,202 140.8 0.34
90,912 100 0.11
277,823 100 0.12
180,560 116.2 0.26
684,855 120 0.66
501,987 120 0.48
581,027 120 0.56
414,199 84 0.29
481,049 84 0.34
457,604 84 0.32
308,483 62 0.16
272,079 62 0.14
Cumulative voes
Removed
(Pounds)
0.63
0.95
1.13
1.22
1.37
1.97
2.33
2.66
4.28
4.88
5.97
6.26
6.54
6.84
7.02
7.10
7.16
7.19
7.22
7.34
7.47
7.54
0.49
0.59
0.77
0.78
1.05
1.53
1.63
2.28
2.50
2.66
3.00
3.11
3.23
3.49
4.15
4.63
5.19
5.48
5.82
6.14
6.30
6.44
•
System Month
Macon Source Area Mar-96
Apr-96
May-96
Jun-96
Jul-96
Aug-96
Sep-96
Oct-96
Nov-96
Dec-96
Jan-97
Feb-97
Mar-97
Apr-97
May-97
Jun-97 • Jul-97
Aug-97
Sep-97
Oct-97
Nov-97
Dec-97
U/L Macon Mar-96
Apr-96
May-96
Jun-96
Jul-96
Aug-96
Sep-96
Oct-96
Nov-96
Dec-96
Jan-97
Feb-97
Mar-97
Apr-97
May-97
Jun-97
Jul-97
Aug-97 • Sep-97
Oct-97
Nov-97
Dec-97
TABLES
SUMMARY OF MASS voe REMOVAL ESTIMATES
MACON/DOCKERY SITE
RICHMOND COUNTY, NORTH CAROLINA
PAGE2OF 2
Average Total
Monthly Flow voe Pounds of voe
Volume Concentration Removed For Month
(gallons) (ug/L) (Pounds)
426,083 50 0.17
364,772 38 0.11
257,720 34 0.07
114,048 66 0.06
202,477 43 0.07
207,503 139 0.23
209,649 54 0.09
101,512 62 0.05
116,354 42.6 0.04
137,045 42.6 0.05
146,036 63.9 0.05
215,730 63.9 0.12
223,222 63.9 0.12
253,167 81.7 0.14
223,177 84 0.15
234,669 84 0.16
117,736 84 0.08
50,248 124.9 0.05
36,264 124.9 0.04
70,207 124.9 0.07
102,326 122.5 0.10
114,452 122.5 0.12
375,318 23 0.07
709,726 18 0.1
482,220 13 0.05
48,305 104 0.04
759,920 26 0.16
638,400 51 0.26
302,505 21 0.05
640,760 33 0.17
871,155 25.3 0.18
725,549 25.3 0.15
596,131 23.1 0.13
795,239 23.1 0.15
939,710 23.1 0.18
918,080 24.2 0.18
999,040 25 0.2
605,792 25 0.12
223,859 25 0.05
911,679 23 0.18
917,631 23 0.18
821,135 23 0.16
140,796 16 0.02
844,299 16 0.11
Cumulative voes
Removed
(Pounds)
0.17
0.28
0.35
0.41
0.48
0.71
0.8
0.85
0.89
0.94
0.99
I.II
1.22
1.36
1.51
1.67
1.75
1.80
1.84
1.91
2.02
2.13
0.07
0.17
0.22
0.26
0.44
0.7
0.76
0.92
I.IO
1.25
1.38
1.53
1.71
1.89
2.09
2.21
2.26
2.44
2.61
2.77
2.79
2.90
. ,
•
•
•
DEC-16-1997 12:03 SAVAtltlAH LABS P.02/12
SL SAVANNAH LABORATORIES
· & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord. NC 28025
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: l0277l2:!.6
REPORT OF RESULTS Pagel
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
76882-l
76882-2
76882-3
76882-4
PARAMETER
Lowery Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad E=fluent
Purgeable Halocarbons (8010)
Chloroform, ug/1
l,1-Oichloroethane, ug/1
l,l-Dichloroethene, ug/1
Cis/Trane-1,2-Dichloroethene, ug/1
Methylene chloride (Dichloromethane),
Tetrachloroethene, ug/1
l,l,l-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution fact.or
Batch !D
Clock ID
76882-1
<1.0
<1.0
<1.0
<l.0
ug/1 <2.0
<l.0
<1.0
<l.O
<1.0
SH
12.10.97
l.0
12091\
2B1209
7688:2-2 ---------·
<1.0
<1.0
<1.0
<1.0
<2.0
<l.O
<1.0
<l.0
<l.0
80\
12.10.97
1.0
1209A
2B1209 -------··-
DATE/
TIME SAMPLED
12-05-97/1315
12-05-97/1320
12-05-97/1530
12-05-97 /1135
76882•3 76882-4
---------------·----
<l.O <l.O
<l.O <l.O
<1.0 <l.0
<1.0 <1.0
<2.0 <2.0
<l.O <:l. 0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
92\ 84%
12.10.97 12.10.97
l.0 l.O
12091\ 12091\
2B1209 2B1209 --------------------
Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
DEC-16-1997 12:03 SAl!ANNAH LABS P. 03/12 . s L SAVANNAH LABORATORIES
. & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue •Savannah.GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 2B025
LOG NO: 57-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Pa9e 2
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
76B82-1
76882-2
76882-3
76882-4
Lowery Dockery Effluent
Upper Dockery Effluent
Macon Source £ffluent
Macon Pad Effluent
PARAMETER
Pu~geable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
suspended Solids (160. 2)
Suspended Solids, mg/1
Preparation Dace
Date Analyzed
Dilution factor
!latch ID
Barium (601.0)
Barium, ug/l
Preparation Dat:e
Date Analyzed
Dilut.ion factor
Batch ID
-----------------------·---------------
76882-1
<1.0
<l.. 0
d.O
<10
87%
12.10.97
1.0
1209A
2B1209
<5.0
12.10.97
12 .11. 97
1.0
1210A
<50
12.09.97
12.10.97
l.0
1209G
----------
76882-2
<l.O
<1.0
<3.0
<10
83%
12.10.97
1.0
1209A
2Bl209
<5.0
1.2.10.97
12.11.97
1.0
1210A
<50
12.09.97
12.10.97
l.O
1209G
--------··
DATE/
TIME SAMPLED
12-05-97/1315
12-05-97 /1320
12-05-97/1530
12-05-97 /1135
76882-3
<1.0
<1.0
<3.0
<10
83%
12.10.97
1.0
1209A
261209
<5.0
12.10.97
12 .11. 97
l.O
1210A
150
12.09.97
12.10.97
l.O
1209G
76882-4
<1.0
<1.0
<3.0
<10
83%
12.10.97
1.0
1209A
2Bl209
<5.0
12.10.97
12 .11. 97
1.0
1210A
<50
12.09.97
1.2.10.97
]. . 0
1209G --------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
. ,
•
•
•
DEC-16-1997 12:03 SAlJAt !MAH LABS P.04/12 . s L SAVANNAH LABORATORIES
. & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Xr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
concord, NC 28025
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 1027712:r.6
REPORT OF RESULTS Page 3
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
76882-1 Lowery Dockery Effluent
76882-2 Upper Dockery Effluent
76882-3 Macon Source Effluent
76882-4 Macon Pad Effluent
PARAMETER
Beryllium {6010)
Beryllium, ug/1
Preparation Date
Date A.-ialyzed
Dilution factor
Batch ID
Chromium (6010)
Chromium, ug/1
Preparation Date
Date Analyzed
Dilution fact.or
Batch ID
Manganese {6010)
Mang,:mese, ug/1
Preparation Dat.e
Date Analyzed
Oilucion factor
Batch ID
----------
----------
76882-l
----------
<5.0
12.09.97
12.10.97
1.0
1209G
<10
12.09.97
12.10.97
1.0
1209G
160
12.09.97
12.10.97
1.0
1209G ----------
76882-2
•••'"'••r-••
.::5. 0
12.09.97
12.10.97
1.0
1209G
<10
12.09.97
12.10.97
1.0
1209G
<5.0
12.09.97
12.10.97
1.0
1209G
----------
DATE/
TIME SAMPLED
12-05-97 /l3l5
12-05-97/1.320
12-05-97/1530
12-05-97/U35
76882-3 76882-4 --------------------
<5.0 <5.0
12.09.97 12.09.97
12.10.97 12.10,97
1.0 1. 0
1209G 1209G
<10 <10
12.09.97 12.09.97
12.10.97 12.10.97
1.0 1.0
1209G l:l09G
160 <5.0
12.09.97 12.09.97
l2.10.97 12.10.97
1.0 l.O
1209G 1209G
--------------------
Laboratories in Savanna/I, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans. LA
. ,
•
•
•
DEC-16-1997 12:04 SAtJAtltJAH LABS . s L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
P.05/12
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
concord, NC 28025
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
76882-l
76882-2
76882-3
76882-4
PARAMETER
Lowery Dockery Errluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
vanadium [6010)
Vanadium, ug/1
Preparation oac.e
Dace Analyzed
Dilution factor
Batch ID
Nickel [6010)
Nickel, ug/1
Preparation Dat:.e.
Date Analyzed
Dilution factor
Batch ID
cadmium [71.31)
cadmium, ug/1
Preparac.ion Date
Date Analyzed
Dilution fact.or
Batch ID
76882-1
<50
12.09.97
12.10.97
1.0
1209G
<40
12.09,97
12.10.97
1.0
1209G
<0.30
12.09.97
12 .11. 97
1.0
1209H
----------
LOG NO: $7-76882
Received: 06 DEC 97
Repor~ed: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
76882-2
<50
12,09.97
12.10.97
1.0
1209G
<40
12.09.97
12,10,97
1.0
1209G
<0.30
12.09.97
12 .11. 97
1.0
1209H
----------
Page 1
DATE/
TIME SAMPLED
12-05-97/1315
12-05-97/1320
12-05-97/1530
12-05-97/1135
76882-3
<50
12.09.97
12,10.97
1.0
1209G
<40
12.09.97
12.10.97
1.0
1209G
<0.30
12.09.97
12 .11. 97
1.0
1209H
76882-4
<SO
12.09.97
12.10.97
1.0
1209G
<40
12,09.97
12.10.97
1.0
1209G
c:0.30
12,09.97
l.2 .11. 97
1.0
1209H
--------------------
Laboratories in Savanna/!, GA • Ta//a/!assee, FL • Tampa, FL • Deerfield Beach, FL • Mobile. AL • New Orleans, LA
. ,
•
•
•
DEC-16-1997 12:04 SAVAflNAH LABS
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
P. 06/12
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project:: Macon/Dockery 109564-0_4
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page S
LOG NO
76882-1
76882-2
76882-3
76882-4
SAMPLE DESCRIPTION, LIQUID SAMPLES
Lowery Dockery Effluent:
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
--------------------------------------------------
PARAME':'ER
Lead (7421)
Lead, ug/1
Preparation Date
Date Ar.alyzed
Dilution factor
Bat.ch ID
I\Iltimony (7041)
Antimony, ug/1
Preparation Date
oa::.e Analyzed
Dilution factor
Bacch ID
76882-1 ------·---
<3.0
12.09.97
12. 10. 97
1.0
1209H
<10
12.09.97
12.11.97
1.0
120n
----------
76882-2 ---------..
<3.0
12.09.97
12.10.97
·1.0
1209H
<10
12.09.97
12.ll.97
1.0
1209I
----------
DATE/
TIME SAMPLED
12-05-97/1315
12-05-97/1320
12-05-97/1530
12-05-97/1135
76882-3 76882-4 --------------------
6.5 <3.0
12.09.97 12.09.97
12.10.97 12.10.97
1.0 1.0
1209H 1209H
<10 <10
12.09.97 12.09.97
12.11.97 12.11.97
1.0 1.0
1209I 1209I --------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
DEC-16-1997 12:04 SAVAtlt1AH LABS
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRocha Avenue• Savannah. GA 31404 • [phone] • Fax [phone] ;
Mr. Sceve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
P.07/12
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page 6
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
-----------------------------------------------------------------------------------
76882-5 Trip Blank
PARAMETER
Purgeable ttalocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride (Dicbloromethane), ug/1
Tetrachloroechene, ug/1
l,l,1-Trichloroethane, ug/1
Trichloroechylene, ug/1
Vinyl chloride, ug/1
Surrosate -Bromochloromethane
Date Analyzed
Dilution factor
76882-5
<1.0
<1..0
<1.0
<1. 0
<2.0
<l.0
<1.0
<l. 0
<l.O
84%
12.10.97
1.0
Ba.ch ID 1209A
Clock ID 2B1209
Purgeable Aromatics (8020)
Benze:ie, ug/l
Toluene, ug/1
Total Xylenes, '.J.g/1
Acetone, ug/l
Surrogate -a,a,a-Trifluorotoluene
Date. Analyzed
Dilution factor
Batch ID
Clock ID
<l.O
<l.O
<3.0
<10
871:
12.10.97
1.0
1209A
2B1209
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, I.A
.. •
•
•
•
DEC-16-1997 12:05 SAVAtlNAH LABS
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
P.08/12
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page 7
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
76882-6
76882-7
76882-8
PARAMETER
Method Blank.
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane. ug/1
l,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/l
Methylene chloride (Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Cilution factor
Bacch ID
Clock ID
76882-6
<l.O
<1.0
<1.0
<1.0
<2.0
<l.0
<1.0
<1.0
<1.0
80%
12.10.97
1.0
l209A
2Bl209
76892-7 76892-9
100 \ 10-232 \
105 % 28-196 %
Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, Fl • Mobile, AL • New Orleans, LA
•
•
•
DEC-16-1997 12:05 SAVAflNAH LABS P.09/12 . s L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • {912) 354-7858 • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Streec
Concord, NC 28025
LOG NO: £7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
76882-6
76882-7
76882-8
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Acc•~racy Control Limit ( %R)
Purgeable Aromacics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Bacch ID
Clock ID
Barium (6010)
Barium, ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Beryllium (6010)
Beryllium, ug/1
Preparation Date
Ca.ta Anal yze.d
Dilution factor
Batch ID
76882-6
<l.0
<.:1.0
<3. a
<l.0
93%
l.2.10.97
l.O
l209A
2B1209
<50
12.09.97
12.10.97
1.0
J.209G
<S.O
12.09.97
12.10.97
1.0
l209G
76882-7
110 %
115 %
100 \
96 %
93 \
76882-8
23-168 %
33-167 %
40-130 %
80-120 \
80-120 \
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Moblle, Al. • New Orleans, LA
•
•
•
DEC-16-1997 12:05 SAVAtltlAH LABS P. 10/12
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaAoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earch Sciences
751 Arbor Straet
Concord, NC 28025
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page 9
LOG NO
76882-6
76882-7
76882-8
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (\R)
Chromium (6010)
Chromium, ug/1
Preparation Dace
Date Analyzed
Dilution factor
Bat:ch ID
Manganese (6010)
Manganese. ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
vanadium, ug/l
Preparat.ion Oate
Date Analyzed
Dilution factor
Batch ID
76992-6
<10
J.2.09.97
12.J.0.97
J..0
l209G
<5.0
J.2.09.97
12.10.97
J..O
1209G
<SO
12.09.97
12 .10. 97
1.0
1209G
76882-7 76982-8
100 % 80-120 t
97 t 90-120 t
98 % 80-120 t
Laooralories In Savannah, GA • Tallahassee, FL • Tampa. Fl • Deerfield Beach, FL • Mob/le, AL • New Orleans, LA
,.
•
•
•
DEC-16-1997 12:05 SAl'At JNAH LABS P.11/12
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SEFIVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102111216
REPORT OF RESULTS Page lO
LOG NO
76882-6
76882-7
76882-8
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
PARAMETER
Method Blank
Lab Control Seandard t Recovery
LCS Accuracy Control Limit (%R)
Nickel (6010)
Nickel. ug /1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmium (7131)
Cadmium, ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead, ug/1
Prepa?:"ac.ion Date
Date Analyzed
Dilution fact.or
Batch ID
76882-6
<40
12.09.97
12.10.97
1.0
l209G
<0.30
12.09.97
12.11.97
1.0
1209!!
<3.0
12.09.97
l2.l0.97
1.0
1209!!
76882-7 76882-8
99 'tr 80-120 \
88 \-80-120 'tr
80-120 %
Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mob/le, AL • New Orleans, LA
0
•
•
DEC-16-1997 12:06 SAVAtltlAH LABS
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
P. 12/12
5102 LaRoehe Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
LOG NO: S7-76882
Received: 06 DEC 97
Reported: 16 DEC 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Project: Macon/Dockery 109564-04
Sampled By: Client
Code: 102771216
REPORT OF RESULTS Page ll
LOG NO
76882-6
76882-7
76882-8
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
PARAMETER
Method Blank
Lab Control Standard\ Recovery
LCS Accuracy Control Limit (\R)
Antimony (7041)
Antimony, ug/l
Preparation Date
Date Analyzed
Dilution fa.ctor
Batch IO
Suspended Solids (160.2)
Suspended Solids, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Methods: EPA SW-846 and 40 CFR Part 136.
76882-6
<10
12.09.97
12.ll.97
1.0
1209I
<5.0
12.10.97
12.ll.97
1.0
1210A
Final Page Of Report
76882-7 76882-8
95 % 80-120 \-
101 % 75-125 %
Laboratories rn Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
TOTAL P.12
•
RECEIVED
NOV 121997
SUPERFUND SECTION
!VIACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
!VIONTHL Y PROGRESS AND
0 & lW REPORT
OCTOBER, 1997
•
•
Macon/Dockery Site
Richmond County, North Carolina
November 7, 1997
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 3 03 65
Re: Maconffiockery Site -Cordova, North Carolina
Monthly Progress and O & M Report -October 1997
Dear Ms. Bennett:
Reply to: Technical Committee
c/o David L. Jones
Ingersoll-Rand Company
114 Spencer Road
Cassopolis, Michigan
Phone: [phone]
Fax: [phone]
On behalf of the Macon/Dockery Site Group ("Group"), the October 1997 Monthly Progress and 0
& M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS of
the Unilateral Administrative Order (effective date -May 30, 1992) for the Macon/Dockery Site .
This report describes activities which occurred during the month of October as part of the Remedial
Action phase of this project.
PRO.JECT TASKS INITIATED OR COMPLETED THROUGH OCTOBER 1997:
• Monthly sampling of the water effluent from the remediation systems.
• Continued O & M of systems.
RESULTS OF SAMPLING AND TESTING AND OTHER DATA RECEIVED:
• A summary of the laboratory results for October sampling of the remediation systems is
included in this progress report. Tables 1 through 4 summarize the analytical results for the
four groundwater treatment systems. The reported effluent concentrations are below the
remediation performance standard .
•
•
Ms. Giezelle Bennett
November 7, 1997
Page No. 2
• Upper Dockery flow meter reading for October totaled 277,505 gallons. The system was
operational 100% of the time averaging 7.71 gallons per minute (GPM). Mass VOC
removal was 0.12 pounds for the month and the cumulative is 7.34 pounds.
• Lower Dockery flow meter reading for October totaled 457,604 gallons. The system was
operational 100% of the time averaging 12.71 GPM. Mass VOC removal was 0.32 pounds
for the month and the cumulative is 6.14 pounds.
• Macon Source Area flow meter reading for October totaled 70,207 gallons. The system was
operational 100% of the time averaging 1.95 GPM. Mass VOC removal was 0.07 pounds
for the month and the cumulative is I.91 pounds.
• Upper/Lower Macon flow meter reading for October totaled 821,135 gallons. The Upper
Macon system was operational 100% of the time in October. The Lower Macon system was
operational 100% of the time in October. The combined system flow averaged 22.81 GPM.
Mass VOC removal was O 16 pounds for the month and the cumulative is 2. 77 pounds.
TASKS PLANNED FOR NOVEMBER 1997:
• Quarterly sampling of the remediation systems influent and etlluent
• Quarterly sampling and gauging of designated monitoring wells
• Continue O &M of systems
• Request regulatory approval to chlorinate Upper/Lower Macon infiltration galleries
PROBLEMS AND DELAYS:
• October 9 -The Upper/Lower Macon System infiltration gallery was discovered to be in an
overflow status. Groundwater extraction well UM-6 was taken off-line to allow the water
level in the infiltration galleries to drop. On October 23, 1997, wells UM-2 and UM-4 were
also taken off-line since the infiltration galleries still appeared to be near an overflow level.
The three groundwater extraction wells remained in an off-line condition at the end of the
October reporting period.
Based on the results of chlorination treatment at the Upper Dockery site last year, the Group
proposes similar treatment of the Upper/Lower Macon infiltration galleries. The proposal
will be made under separate cover to the EPA
·•
•
Ms. Giezelle Bennett
November 7, 1997
Page No. 3
• Percent operational for each system: Upper Dockery
Lower Dockery
Upper Macon
Lower Macon
100%
100%
100%
100%
Macon Source Area I 00%
Respectfully Su~
(t__ /(-~'
~es fO
Project Coordinator
cc: Macon/Dockery Site Group Members
Paul Furtick, R.i\1T, Inc.
SVE system I 00%
David Mattison, NC Super Fund Section
Mike Profit, COM Federal
•
Sample Date
l.rn.:ation
I 11> EOlucnl 2/13/%
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28196
3/8/96
4/3196
5/3/96
6/5/96
7/I/%
8/1/96
9/4/96
10/1/96
Jlnl96
12/5/')(,
1/6/97
2/5/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
8/7/97
9/5/97
10/2/97
Ri:mcd1at1on l'i:rlonnan...:i: Standard
NA -Not ,\nJ!p.:,l
Not~: • 1\c,:tu11c· ..:outiuncJ l,y 11.lcthoJ M::'t,O
I, I -Dichlm11..:than..:
(ug/1,)
<J.O
<1.0
<I.fl
<1.0
<1.0
<1.0
<1.0
<I.II
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
...:1.0
< 1.0
<I.CJ
<1.0
<1.0
..:: J.()
<I.U
<J.()
<1.0
< 1.0
3500
•
Table I
(iroundwatcr Q11ality Summa1y
Upper Dockery
Macon/ Dockery Site
Richmond County, North Carolina
1, I -Did1loroc1hc11c Cis/trans-1,2-l)ichloroclhcne T drachloroethcne
(u~fl.) (ug/1.) (ugll,)
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <l.O <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<]_{) <1.0 <1.0
<1.0 <1.0 <1.0
<I.fl <!.0 <LO
<1.0 <1.0 <LO
<1.0 ..:::1.0 <i.0
<1.0 <LO <1.0
<1.0 <1.0 <1.0
...:::1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <i.O <1.0
1.5 ..:: 1.0 ..:: 1.0
...::1.0 ...:::1.0 ..:: 1.0
<1.U ...:: 1.0 <1.0
<1.0 <1.0 <1.0
<J.O <1.0 <LO
..::1.0 <1.0 <1.0
<1.0 ...:: 1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0· <1.0 <1.0
7 70
•
I, I, I-Trichloroethane 'l'richlorocthylcnc Toluene
(ug/L) (ug/L) (ug/L)
<1.0 <LO <1.0
<l.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<I.O <LO ..::1.0
<LO <LO <LO
<LO <LO <1.0
<l.O <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 3.9
<1.0 <LO <1.0
<LO <1.0 <i.O
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <J.O
<1.0 <1.0 ,1.0
<1.0 ...::1.0 <1.0
<1.0 <LO ..:.:1.0
<LO <1.0 <1.0
<1.0 <i.O -.::1.0
<1.0 <1.0 <.1.0
<LO <1.0 <LO
<LO -.:: 1.0 <1.0
<1.0 <1.0 <1.0
< 1.0 <1.0 <1.0
<1.0 <LO <1.0
200 2.8 1000
•
Sample lhtc
J .ocation
I JI) Efllucnl 211.11')(,
2/1·11%
2/1-11')(,
2/1 Si'JG
2/ 1(11')6
2117:')6
21221')(,
2/2X19(,
3/81%
4/119(,
S/11%
(,/5!'){,
7/11%
S/l 1•H,
9/--119(,
IOll1')(,
I I /71'JC,
12l51'Jc,
l/(,•'J7
2/5,97
3/12197
4/8.'97
5/Hl97
6/6197
112,•n
817197
9/5197
10/2/97
Rcmcd1at1on l'crlonnancc Standard
NA .. Not ,\n.ilyic,I
Note;• Acdonc co11ti1111cd by Mc1ho.[ 112(,(J
Total Xyh:ncs
(ugll.)
<3.0
<3.0
<3.0
<J.O
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<].O
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
400
•
Table I (Cunlinucd)
Groundwater Qualily Summary
Upper Dockery
M,~con/Dockcry Sitt.:
Richmond County, North Carolina
Acdonc Chromium Barium t-.fangan.:sc
(ug/L) (ug/L) (ugll.) (ugll.)
7o•F32 16 71 40
35*F33 15 53 14
<IO II 56 12
<10 12 53 14
<10 <10 53 II
<10 II 55 12
-::JU <10 <50 8.3
<ID 13 <50 9.6
25 <10 <50 6.9
28 II 50 <5.0
52 <10 <50 <5.0
<ID <10 <50 <5.0
<JO <10 <50 <5.0
20 1·1 5 I 7
<IO <10 55 <5.0
-.:: IO <]{) -::so 5 9
<10 15 59 <5.0
<10 12 54 5.1
...:::10 I.I 54 <5.0
<10 15 61 5.9
<10 <JO 69 <5.0
<10 <10 63 <5_o·
<10 <10 60 7.2
<JO <10 52 <5.0
<JO <JO 55 <5.U
<10 <10 <50 <5.0
<10 <10 I IO 5.2
<10 <10 50.1 <5.0
}500 50 l000 50
Zinc Lead Suspended Solids
(ug/L) (uglL) (mglf.)
22 <3.0 14
<20 <3.0 II
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 10
<20 <3.0 <5.0
<20 <J.O 5
<20 <3.0 <5.0
<20 <3.U <5.0
<20 <3.0 <5.0
<20 <3.0 8
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 ...::J.O <5.0
<20 <.l.0 <5.0
<20 ...:::3.0 <5.U
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
<20 <3.0 <5.0
5000 15
•
Sample l)a\c
l.ucation
I .I) Efilucnt 2/13/1)(,
2/1,t/9(1 2n,,,9c,
2/15/96
2/ I (1196
2/22/96
2/28196
3/8/96
4/3/96
5/3/96
8/1/96
9/4/96
10/1/96
11/719(1
12/5196
J/6/97
3/12197
·1/8197
5/14197
6/6/97
7/2/97
817/97
9/5/97
I 0/2197
RcmcJm\11111 J1c1hiru1.111ce StanJa1d
Note: A blank means bdow detection limit
Chlorofiirm
(ugiL)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<I.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
-.:::\.0
<l.0
<l.0
<1.0
<1.0
<I .0
• Table 2
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond County, North Carolina
I, I -Dichlomcthanc I, I • Dichlorocthcnc Cis/trans-1,2-Dichloroethcnc
(ugiL) (ug/J,) (ug/L)
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 ..::1.0
<1.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
< I .0 <1.0 <LO
<1.0 <1.0 <1.0
-:::1.0 <LO <1.0
<I.O <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<],() <LO <1.0
<] O ..:.J .0 <],0
<],(] <1.0 <],0
<],() , LO <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
3500 7 70
•
Methylene chloride I, I, I -Trichloroethane
(ug/L) (ugiL)
<2,0 <1.0
<2,0 <1.0
<2,0 <1.0
<2,0 <1.0
<2.0 <1.0
<2,0 <1.0
<2,0 <1.0
<2,0 <1.0
<2,0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2,0 <1.0
<2,0 <1.0
<2,0 <1.0
<2.0 <1.0
<2.0 <1.0
<LO <1.0
<2.0 -::1.0
<2.0 -::1.0
<2,0 <1.0
<2.0 <1.0
<2,0 <1.0
<2,0 <1.0
5 200
•
Sample Date
l.ncation
I .I> Efilucnt 2/13/96
2/14/9(1
2/J,lt96
2/15196
2/16196
2/22/96
2/28/96
3/8/96
4/3/96
5/3196
8/1/96
9/•1/96
I0/1/96
11n,%
12/5196
1/6/97
3/12/117
4/8197
5/1,111)7
6/6197
7/2197
Bn/97
915197
10/2/97
Rcn1c<l1atmn l1c1 lli111wncc Stan<la,J
Note:,\ blank 111cans l>!!low Jctcction limil
·1·richlorocthylcnc lknzcnc
(ug/1.) (ug/1.)
<1.0 <1.0
<1.0 <1.0
<1.0 --:1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 ..::1.0
<1.0 <1.0
<1.0 <1.0
<l.0 <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<J.0 <1.0
<1.0 <1.0
<1.0 -..::).0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
2.8
• TABLE 2 (Continuctl)
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond County, Nonh Carolina
'J'oluc11c Total Xylcncs Chromium
(ug/L) (ugll.) (ug/L)
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <HJ <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
<1.0 <3.0 <IO
<LO <3.0 <10
<1.0 <3.0 <10
3.4 <3.0 <IO
<1.0 <3.0 <JO
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <3.0 <IO
-..::1.0 <3.0 -..::10
<1.0 <3.0 -..::10
<1.0 <3.0 <10
<1.0 <3.0 <10
<1.0 <J.O <IO
<1.0 <3.0 <JO
!000 400 -,o
•
Barium Manganese Zinc Cadmium Suspended Solids
(ug/L) (ug/1.) (ug/L) (ug/1.) (mg/I.)
<SO <5.0 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<SO <5.0 <20 <0.30 II
<SO <5.0 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<SO <5.0 <20 <0.30 5
<SO <5.0 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<SO <5.0 <20 <0.30 <5.0
<SO <5.0 <20 <0.30 <5.0
<SO 14 <20 <0.30 <5.0
<SO 13 <20 0.56 <5.0
<50 II <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
<50 35 <20 <0.30 19
<50 6 <20 <O.JO <5.0
70 <5.0 <20 <0.JO <5.0
<50 <5.0 <20 <0.30 <5.0
<50 <5.0 <20 ..::0.JO -.:.:5.0
<50 <5.0 <20 ..::O.JO <:5.0
<50 <5.0 <20 <0.30 <5.0
<SO <:5.0 <20 <0.)0 <5.0
· <50 <5.0 <20 <0.30 <5.0
<50 <5.0 <20 <0.30 <5.0
-IOOO 50 5000 '
•
Samplc Date
l.1ication
ll~ISA Elllu.:111 2/13/%
2/14/96
2/14/96
2/15/%
2/16/96
2/17/%
2/22/%
2/28/9Ci
3/8/96
4/3/96
513/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
lln/96
12/5/96
1/6/97
214197
J/12/97
4/8/97
5112197
6/6/97
7/2/97
Bn/97
9/5197
10/2/97
kcmc<l1.11Jon l'c1h•1m,mcc S1.m,!Jr1I
N<1lc: NA ~ No1 A11,,IYfcd
])l !I' -duplicJlc
Chlorofonn I, I -l>id1lon><.:thanc
(ug/1 ,) (ugll .)
<1.0 <I.()
-:;: I.fl <1.0
<I.O <1.0
<1.0 <1.0
<1.0 <I.fl
<1.0 I.II
<1.0 <1.0
<1.0 <I.ti
<1.0 <J.U
<].0 <J.()
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<J.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 --1.0
•. l.O •,[_()
<1.0 ·-1.0
<LO -..1.0
<1.0 -:: 1.0
<1.0 <LO
<Lil <1.0
<1.0 ..;: 1.0
<1.0 <1.0
<1.0 <1.0
1500
•
Tahlc 3
Groundwater Quality Summary
Upper Macon Source Arca
Macon/ Dockery Site
Richmond County North Carolina
I, I -Dichloroclhcnc Cis/trans-1,2-l)ichlorocthi:nc T ctrachlorocthcnc
(ug/1.) (ugll,) (ug/1.)
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <1.0 <LO
<1.0 <1.0 <I.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
'1.0 <1.0 <1.0
..:. J.Q <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
..::1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <LO <1.0
<UJ <LO <I.0
...:1.0 <I.Cl <l.O
..:.1.0 <LO <1.0
-::1.0 <1.0 <1.0
<LO <1.0 <1.0
-:: 1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <LO
7 70
I, I, 1-Trichloro..:thanc Trichloroethyh:nc
(ugll,) (ug/1.)
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<l.(J <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<l.0 <1.0
<1.0 <1.0
<1.0 < 1.0
<).0 <1.0
<1.0 <1.0
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 ...: 1.0
<LO ...:1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
<LO <1.0
<1.0 <1.0
200 2.8
•
Sampk 1);11.:
Location
UMS,\ Elllui:nt 2113/9(,
2/14196
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
318/96
4/3/96
5/3/96
6151')6
7/1/96
7/30/96
9/4/96
10/1/%
11/7/%
12/51')(,
1/6/97
2/4197
3/12/97
4/8/97
5/12197
G/G/97
7/2197
811197
?15197
10/2/97
lkmc,h.,1i,,n l'crfo1111,mcc S1,,ml.ud
Nuk: NA .. Nut ,\11.ity.-:cd
D\JI' -duplic.ilc
Vinyl d1lo1 id.: lk,u.:nc Tulu.:nc
(ugfl,) {uglL) (ug/1,)
<1.0 <1.0 <LO
<I.CJ <-1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <LO <J.O
<1.0 <1.0 <1.0
<1.0 <1.0 <:1.0
<1.0 <1.0 -.:.:1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 '1.0
<I.CJ <1.0 <1.0
<1.0 ..::1.0 2.9
<1.0 <J.O <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <I.0
..::1.0 <1.0 <I.O
...:: 1.0 ·,1.0 <1.0
..:: I.ti <1.0 ...:: 1.0
<1.0 <1.0 <1.0
<I.() <1.0 <1.0
<1.0 <1.0 <1.0
..::1.0 <1.0 ...::1.0
<l.O ·-I.II <I.O
<1.0 <1.0 <1.0
<1.0 ·.1.0 <l.O
1000
•
Table 3 (Conlinucd)
( iroun<lwatcr Qua lily Summary
Upper Macon Source Arca
Macon/l )ockcry Site
Richmond County, North Carolina
Chromium Barium t..·langanesi:
(ug/L) (ug/L) (ug/L)
16 150 330
<JO I JO 190
<JO 110 160
<JO JOO 140
<JO 1)0 170
<JO 120 120
<JO 120 70
<JO 130 SJ
<JO 120 37
<JO I JO 27
<JO 120 26
<JO 130 22
12 I JO 14
<JO 200 I JO
II 170 68
<JO !JO 13
<JO HO 13
<JO 170 17
<JO 200 46
<IO 160 29
<IO 130 30
<JO 200 30
12 210 95
<JO 2•W 74
<JO ISO 41
II 2JO 250
<IO 1)0 27
<JO 185 31.5
50 1000 50
•
Zinc Cadmium I.A!ad Mercury Suspcnd.:d Solids
(ug/L) (ug/L) (uglL) (ug/L) (mg/L)
74 <0.30 4.2 <.2 57
20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 0.26 18
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 5
<20 <0.30 <3.0 <.2 <5.0
<20 <0.30 <3.0 <.2 6
..::20 <0.30 <3.0 NA <5.0
41 <0.30 9.2 NA 23
26 <0.30 66 NA 16
<20 0.47 <3.0 NA 24
<20 <0.30 <3.0 NA 26
<20 <0.30 <3.0 <0.20 j
25 <0.30 3.5 NA 120
<20 <0.30 <3.0 NA 8
<20 <0.30 <3.0 NA <5.0
<20 <0.30 <3.0 NA 7
35 <0.30 <3.0 NA JOO
<20 <0.30 <3.0 NA ·~5.0
<20 <0.30 <3.0 NA <5.0
40 <0.30 4.8 NA N:\
<20 <0.30 <3.0 NA 22
<20 <0.30 <3.0 NA II
5000 5 I 5 I.I
•
Sample Date
Location
1111. Efllucnt 2/21196
2fl21'>6
irn..1'J6
2/23196
W-1196
2125•96
2/28196
3181')6
3116196
4/3196
5/3196
615196
7/1196
7/Ji),196
9/-11%
10/1196
11171%
12/5196
1/6197
2/4197
3/12197
4/8,97
5/12197
6/6197
7rlJ97
1(251')1
8/7,97
9/5197
I0rlJ97
lh:mcd1ahon l'crfonnancc StandarJ
:--:u1~: 1n5191 s~111pk<! fi>1 M~ngancsc rnilr.
I llJP . dupli.:al~
N:\ "' Not Analp.cd
c:hlorofonn I, I -Di..:hlorocthanc
l"glL) (ugll.)
<1.0 <1.0
<1.0 <I.()
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 _<LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 1.8
<1.0 <1.0
<i.O -~1.0
<1.0 <LO
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 -:1.0
<1.0 ·-1.0
<1.0 <1.0
<1.0 1.0
<1.0 LO
<1.0 ·-1.0
<1.0 ·-1.0
<1.0 2.-1
<1.0 <1.0
..::1.0 •:I.O
<1.0 <1.0
..:I,() -;I.()
'
•
Table 4
Groundwater Quality Summary
Upper/Lower Macon System
Macon/ Dockery Site
Rii.:hmond County North Carolina
I, I -Dichloroclhcm: Cis1trans-l ,2-Dichlorocll11:m: Methylene: chloride
("g/1,) ("g/1-) ("g/1.)
<1.0 <1.0 <2.0
1.8 <1.0 16
<1.0 <1.0 <2.0
<1.0 ...::1.0 <2.0
<1.0 <1.0 <2,0
<1.0 <:I.O <2.0
<1.0 <1.0 <2.0
<1.U <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 1.6 <20
<1.0 <LO <2.0
<1.0 <LO <2.0
<1.0 <1.0 <2.0
..::1.0 <1.0 <2.0
<LO <1.0 <20
<LO <1.0 <2.0
<LO ...:1.0 <2.0
<1.0 ..:1.0 <..."2.0
<1.0 ..:J.0 <2.0
<1.0 <LO <2.0
<1.0 <LO <2.0
..:1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 ..::1.0 <2.0
<1.0 1.8 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<I.U <1.0 <2.0
7 70 5
•
Tctrach\orocthcnc I, I, I-Trichloroethane
(uglL) (ug1l.)
<LO <1.0
<1.0 <LO
<1.0 ..::1.0
<1.0 <1.0
<1.0 <J.0
<1.0 <1.0
<1.0 <].0
<1.0 <1.0
<LO <1.0
<1.0 <).0
<1.0 <1.0
<1.0 ..::1.0
<1.0 ..::1.0
<1.0 -.:1.0
<1.0 <1.0
...:1.0 <1.0
..::1.0 <1.0
<1.0 ..:1.0
<1.0 ..:1.0
<1.0 <1.0
<1.0 <1.0
..:1.0 <1.0
..:..1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
,1.0 <1.0
<LO <1.0
200
•
Sample D.1tc
Location
U/1, Effiucnl 2/21/96
1fl21%
2121.;%
2/2)/'J(J
2/24196
21251%
2/2!!196
3/8/96
31161')6
4/3/96
5/3196
615196
7/1/96
7/30196
9141%
10/l;W,
11171%
12151%
l/6197
2/4,'>7
3/121~17
418•'l7
5/12•'J7
6/6l!J7
1n,!n
7/2511)7
8/7;'>7
9.151'>7
1()/21'.l?
Rcmcd"atio I Pcrfonn::mcc Slamlanl
Nut~: 7125/97 S.<mpkd fo1 ~l~ngmc~c onl}
DtJI' -duplkalc
N,\ = Nol t\n;t\p.c<l
Trichloroclhylcnc
(,g/L)
<1.0
<1.0
<).0
<LO
<1.0
<1.0
<l.O
<1.0
<1.0
1.9
<LO
<LO
<LO
<LO
..::1.0
<1.0
<1.0
<LO
<LO
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
2.8
•
Toluene Chromium
(,g/L) (uglf.)
<1.0 <10
<1.0 130
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <JO
..::1.0 <IO
<1.0 <IO
<1.0 <I()
<LO <10
2.1 <10
<LO <10
<1.0 <10
<1.0 <10
<1.0 <J(l
<).0 <10
<LO <IO
<LO <10
<1.0 <10
<1.0 <J()
<1.0 <JO
<1.0 <I()
..::1.0 <10
..::1.0 <!{)
...:1.0 <10
<1.0 ...::10
<1.0 <IO
<1.0 <JO
1000 50
Table 4 (Conlinued)
Groundwater Quality Summary
Upper/Lower Macon System
Macon/I )ockcry Site
Riclunon<l County North Carolina
Barium Manganese Zinc
(ug/J.) (ug.,L) (,g/L)
59 100 98
70 120 120
72 120 120
80 i,o 130
83 150 150
90 160 170
<50 32 59
<50 39 56
<50 3 I 51
<50 44 54
31 10 21
<50 7.5 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
39 <5.0 <20
<50 <5.0 <20
200 30 <20
..::50 <5.0 <20
<50 <5.0 <20
<50 79 <20
<50 36 <20
<50 5..1 <20
<50 ...:5.0 <20
<50 6.3 <20
1000 50 . 5000
e
Lead Sw.pcndcd Solids
(ug/J.) (mgil.)
4 <5.0
5.2 <5.0
5.7 <5.0
4.9 <5.0
3.7 <5.0
3.6 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
3.6 10
<3.0 <5.0
<3.0 <5.0
<3.0 -~s.o
<3.0 ..::5.0
<3.0 <5.0
<3.0 ,.
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
3. I l\S
..::3.0 ...:5.0
<3.0 2;
15
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC
t>(.1 5102 La Roelle Avenue. Savannah, GA 31404
1·_ l 2846 Industrial Plaza Drive. Tallahassee, FL 32301
r· i -t 14 SW 12111 Avenut.;. Deerlield Beach, FL 33442
Serial Number
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD I I ~OU l.akes1Lle Drive. Mot11le. AL 36693
l I !)/1?. Ben1arnin Road. Swte 100. Tampa. FL 33634
! I 100 A!pt1a Drive. Suite 110, Destrehan. LA 70047
Phone: (9 I 2) 354-7858
Phone· [phone]
Pt1one: (954 J 421-7400
Phone: [phone]
Phone: [phone]
Phone: (50-li 764-1100
Fa,: [phone]
Fax: [phone]
Fa..:: [phone]
Fa, [phone]
Fax: (813) 885· 7049
Fax: [phone]
SAMPLE
DATE TIME
SL
NO. SAMPLE IDENTIFICATION
1,t'-'-1_'-'· ·,cc.'-_1.,_/~l';-'-·;-'-t/"-s'+----1--'-M...'..:..'l\_,.,C"'o=tJ. S VSTE t1 _ E.IT. _
!JJ~"~~--,~/~~--... ~-::~·;r-cl,;,--l~MACOI-.J 5Dul'.C.£ ~~
K': l-:_ 1 ·, '-1<:_ t...OVJ£e t>oc..l:'.Ee'I E;:FF.
!.i' .' -! ·.::?_', ~-_ l) pPE;e. . %c..t:'.€£.y £:F"F.
LL>;_.,_:, ___ , __ --~-IP_ES~~( ___
--·--•---.+------------·---
-------+----!--------. ------.. -----
PAGEi IOFI
REMARKS ---. ~l-..... 3 --_ I ___ I__------~---·!--+--: i __ .
___ ~ ,_ _ ..2 I ____ , _ ------f------1--, I i ----------··
[ .. _ 3 I 1 _ ---·---~ _____ J~----·--··-----
./i J I L ·--··-·--·----· - _ I __ -
,I 3
A '
i ' .. ----~-·-------.. I -
1---+---1-----l---1------•---·I----------
·--·----------·•-•l---+--·--·--•---l~--1----_! __ , ________ _ I
I --r-·-·1-·· ---------•!--..+---,--l
, -l----+---1---+---',-------1--+---------
. ··-.. ----· . . ·------+--[ ___ _! __ ---------
-1----+----l--..._j---:i ____ _i __ , _________ _
i -------l--+---~--1-----!---I•--------
1
DATE Tlt.1E
LABORATORY REMARKS:
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
75642-1 Macon System Eff
75642-2 Macon Source Eff
75642-3 Lower Dockery Eff
75642-4 Upper Dockery Eff
10-0-2-97/1545
10-02-97/1530
10-02-97/1515
10-02-97/1505
PARAMETER 75642-1 75642-2 75642-3 75642-4
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1.
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
·Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
<1.0
<l, 0
<1.0
ug/1 <l.0
<2.0
<1.0
<1.0
<1.0
<1.0
86 %
10.09.97
1. 0
1008A
1Bl009
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
7 8 \-
10.09.97
1.0
1008A
1B1009
<1.0
<1.-0
<1.0
<1.0
<2.0
<1.0
<l. 0
<l. 0.
<1.0
80 t
10.09.97
1.0
1008A
1B1009
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
79 %-
10.09.97
1. 0
1008A
1B1009
Laboratories in Savannah, GA • Tallahassee. FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 160971016
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES-TIME SAMPLED
-------------------·-------------------------------------------------
75642-1 Macon System Eff
75642-2 Macon Source Eff
75642-3 Lower Dockery Eff
75642-4 Upper Dockery Eff
10-02-97/1545
10-02-97/1530
10-02-97/1515
10-02-97/1505
PARAMETER 75642-1 75642-2 75642-3 75642-4
Purgeable Aromatics
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -
(8020)
a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<1.0
<1.0
<3.0
<10
97 \-
10.09.97
1.0
1008A
1Bl009
<50.0
10.07.97
10.10.97
1.0
1007D
<1.0
<1.0
<3. 0
<10
97 1r
10.09.97
1.0
1008A
1Bl009
185
10.07,97
10.10.97
1.0
1007D
<1.0
<1.0
<3. 0
<10
9 3 \-
10.09.97
1.0
1008A
1Bl009
<50.0
10.07.97
10.10.97
1.0
1007D
<1.0
<1.0
<3.0
<10
93 1r
10.09.97
1.0
1008A
1Bl009
50.1
10.07.97
10.10.97
1.0
1007D
Laboratories in Savannah. GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile. AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone] •
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7•75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO, No.: 190·00001-01
Project: 115046·01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 3
DATE/
LOG NO
75642·1
75642·2
75642·3
75642·4
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME. SAMPLED
Macon System Eff
Macon Source Eff
Lower Dockery Eff
Upper Dockery Eff
PARAMETER
Beryllium (6010)
Beryllium (6010), ug/1
Preparation Date
• Date Analyzed
Dilution factor
Batch ID
Chromium (6010)
Chromium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Manganese (6010)
Manganese (6010), ug/1
Preparacion Date
Date Analyzed
Dilution factor
Batch ID
•
75642·1
----------
<5.0
10.07.97
10.10.97
1. o
1007D
<10 .0
10,07.97
10.10.97
1.0
1007D
6.3
10.07.97
10.10.97
1.0
1007D
----------
75642·2
----------
<5.0
10.07.97
10.10.97
1.0
1007D
<10. 0
10.07.97
10.10.97
1.0
1007D
31. 5
10.07.97
10.10.97
1.0
1007D
----------
75642-3
----------
<5.0
10.07.97
10.10.97
1.0
1007D
<10.0
10.07.97
10.10.97
1.0
1007D
<5.0
10.07.97
10.10.97
1.0
1007D
----------
10·02·97/1545
10-02-97/1530
10·02·97/1515
10-02-97/1505
75642-4
----------
<5.0
10.07.97
10.10.97
1.0
1007D
<10.0
10.07.97
10.10.97
1.0
1007D
<5.0
10.07.97
10.10.97
1.0
1007D
----------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach. FL • Mobile. AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------
75642-1
75642-2
75642-3
75642-4
Macon System Eff
Macon Source Eff
Lower Dockery Eff
Upper Dockery Eff
PARAMETER
Nickel (6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
75642-1
----------
<40. 0
10.07.97
10.10.97
1.0
1007D
<3.0
10.08.97
10.09.97
1.0
1008H
<50.0
10.07.97
10.10.97
1.0
1007D
----------
75642-2 75642-3
--------------------
<40.0 <40.0
10.07.97 10.07.97
10.10.97 10.10.97
1.0 1.0
1007D 1007D
<3.0 <3.0
10.08.97 10.08.97
10.09.97 10.09.97
1.0 1.0
1008H 1008H
<50.0 <50.0
10.07.97 10.07,97
10.10.97 10.10.97
1.0 1. 0
1007D 1007D
--------------------
10-02-97/1545
10-02-97/1530
10-02-97/1515
10-02-97/1505
75642-4
----------
<40.0
10.07.97
10.10.97
1.0
1007D
<3.0
10.08.97
10.09.97
1.0
1008H
<50.0
10.07.97
10.10.97
1.0
1007D
----------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach. FL • Mobile. AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
REPORT OF RESULTS Page 5
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
75642-1 Macon System Eff
75642-2 Macon Source Eff
75642-3 Lower Dockery Eff
75642-4 Upper Dockery Eff
DATE/
TIME SAMPLED
10-02-97/1545
10-02-97/1530
10-02-97/1515
10-02-97/1505
------------------ --------------------------------------------------
PARAMETER
Zinc (6010)
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmium (7131)
Cadmium (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
75642-1
----------
<20.0
10.07.97
10.10.97
1.0
1007D
<0.30
10.08.97
10.16.97
1.0
1008H
<10 .0
10.08.97
10.15.97
1.0
1008G
----------
75642-2
----------
<20.0
10.07.97
10.10.97
1.0
1007D
<0.30
10.08.97
10.16.97
1.0
1008H
<10 .0
10.08.97
10.15.97
1. 0
1008G
----------
75642-3 75642-4
--------------------
<20.0 <20.0
10.07.97 10.07.97
10.10.97 10.10.97
1.0 1.0
1007D 1007D
<0. 30 <0.30
10.08.97 10.08.97
10.16.97 10.16.97
1.0 1. 0
1008H 1008H
<10. 0 <10. 0
10.08.97 10.08.97
10.15.97 10.15.97
1.0 1.0
1008G 1008G
--------------------
•
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
75642-1
75642-2
75642-3
75642-4
Macon System Eff
Macon Source Eff
Lower Dockery Eff
Upper Dockery Eff
10-02-97/1545
10-02,97/1530
10-02-97/1515
10-02-97/1505
------------------------------------------------------------------------
PARAMETER 75642-1
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1 25
Preparation Date
Dace Analyzed
10.07.97.
10.08.97
Dilution factor 1.0
Batch ID 1007A
75642-2
----------
11
10.07.97
10.08.97
1.0
1007A
----------
75642-3 75642-4
--------------------
<5.0 <5.0
10.07.97 10.07.97
10.08.97 10.08.97
1.0 1.0
1007A 1007A
--------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa, FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 7
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES DATE SAMPLED
75642-5 Trip Blank 10-02-97
------------------ ------------------------------------------------------------------------
PARAMETER 75642-5
<1.0
<1.0
<1.0
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene,
• Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
ug/1 <1.0
<2.0
•
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
<1.0
<1.0
<1.0
<1.0
84 %
10.09.97
1.0
1008A
181009
---------------------------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • ,Deerfield Beach. FL • Mobile. AL • New Orleans. LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 160971016
Page 8
LOG NO SAMPLE DESCRIPTION, LIQOID SAMPLES DATE SAMPLED
75642-5 Trip Blank 10-02-97
PARAMETER 75642-5
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -
a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor'
Batch ID
<1.0
<1.0
<3.0
<10
100 %
10.09.97
1.0
1008A
Clock ID 1Bl009
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO
75642-6
75642-7
75642-8
75642-9
75642-10
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
------------------ ------- --- ----------------------------------------
PARAMETER 75642-6 75642-7 75642-8 75642-9 75642-10
------------------------------------------------- ------------------------------
.Purgeable Halocarbons (8010)
Chloroform, ug/1 1.0 <1.0
<1.0
<1.0
<1.0
<2.0
•
1,1-Dichloroethane, ug/1 1.0
1,1-Dichloroethene, ug/1 1.0
Cis/Trans-1,2-Dichloroethene, ug/1 1.0
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
2.0
1.0
1.0
1. 0
1. 0
<1.0
<1.0
<1.0
<1.0
78 \'
10.09.97
1.0
1008A
1Bl009
22
25
100 "' 10.09.97
1. 0
1008A
1Bl009
----------
23 20
24 20
92 %
10.10.97
1. 0
1008A
1Bl010
--------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
LOG NO
75642-6
75642-7
75642-8
75642-9
75642-10
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. -No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75642-6 75642-7 75642-8 75642-9 75642-10
•
Purgeable Aromatics (8020)
Benzene, ug/1 1.0 <l.0
<1.0
<3.0
22
23
24
25
20
20
•
Toluene, ug/1 1.0
Total Xylenes, ug/1 3.0
Acetone, ug/1 10
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Dace
Date Analyzed
Dilution factor
Batch ID
50.0
<10
103 %
10.09.97
1.0
1008A
1Bl009
<50.0
10.07.97
10.10.97
1.0
1007D
320
90 %
10.09.97
1.0
1008A
1Bl009
1970
10.07.97
10.10.97
1.0
1007D
340
103 %
10.10.97
1. 0
1008A
1Bl010
1910
10.07.97
10.10.97
1.0
1007D
400
2000
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach. FL • Mobile. AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
Page 11
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
75642-6
75642-7
75642-8
75642-9
75642-10
Reporting Limit (RL)_
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
PARAMETER 75642-6 75642-7 75642-8 75642-9 75642-10
Beryllium (6010)
Beryllium (6010), ug/1 5.0 <5.0 46. 9 45.2 50.0
Preparation Date 10.07.97 10.07.97 10.07.97
Date Analyzed 10.10.97 10.10.97 10.10.97
Dilution factor 1.0 1.0 1.0
Batch ID 1007D 1007D 1007D
Chromium (6010)
Chromium (6010) , ug/1 10.0 <10 .0 204 199 200
Preparation Date 10.07.97 10.07.97 10.07.97
Date Analyzed 10.10.97 10.10.97 10.10.97
Dilution factor 1.0 l. 0 1.0
Batch ID 1007D 1007D 1007D
Manganese (6010)
Manganese (6010), ug/1 5.0 <5.0 509 500 500
Preparation Date 10.07.37 10.07.97 10.07.97
Date Analyzed 10.10.97 10.10.97 10.10.97
Dilution factor 1.0 1.0 1.0
Batch ID 1007D 1007D 1007D
---------------------------------------------------------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach, FL • Mobile. AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
REPORT OF RESULTS Page 12
LOG NO
75642-6
75642-7
75642-8
75642-9
75642-10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75642-6 75642-7 75642-8 75642-9 75642-10
Nickel ( 6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
40.0
3.0
so.a
<40·. a
10.07,97
10.10.97
1.0
10070
<3. a
10.08.97
10.09.97
1.0
1008H
<50.0
10.07.97
10.10.97
1.0
10070
----------
524 521 500
10.07.97 10.07.97
10.10.97 10.10.97
1.0 1.0
10070 10070
48.4 so.a
10,08.97
10.09.97
l. a
1008H
524 514 500
10.07.97 10.07.97
10.10.97 10.10.97
1.0 l. 0
10070 10070
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerlield Beach, FL • Mobile. AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone] •
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKE°RY
Sampled By: Client
Code: 151771016
Page 13
LOG NO
75642-6
75642-7
75642-8
75642-9
75642-10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
PARAMETER 75642-6 75642-7 75642-8 75642-9 75642-10
Zinc (6010)
Zinc (6010), ug/1
• Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmium (7131)
Cadmium (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
•
Date Analyzed
Dilution factor
Batch ID
20.0 <20.0
10.07.97
10.10.97
1.0
1007D
0.30 <0.30
10.08.97
10.16.97
1.0
1008H
10.0 <10.0
10.08.97
10.15.97
1.0
1008G
----------
491 481 500
10.07.97 10.07.97
10.10.97 10.10.97
1.0 1.0
1007D 1007D
4.31 5.00
10.08.97
10.16.97
10
1008H
48.2 so.a
10.08.97
10.15.97
1.0
1008G
--------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354•7858 • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Cli,;nt
Code: 151771016
REPORT OF RESULTS Page 14
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
75642-6
75642-7
75642-8
75642-9
75642-10
Lab Control Standard Duplicate Result
LCS Expected Value
PARAMETER
Suspended Solids (160.2)
Suspended Solids (160.2), rng/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
75642-6
5.0
75642-7 75642-8
<5.0 99
10.07.97 10.07.97
10.08.97 10.08.97
1.0 1.0
1007A 1007A
--------------------
75642-9
96
10.07.97
10.08.97
1. 0
1007A
----------
75642-10
100
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach, FL • Mobile. AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 151771016
REPORT OF RESULTS Page 15
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
75642-11
75642-12
75642 -13
LCS/LCSD \-Recovery
LCS Accuracy Control Limit (\-R)
Method Blank
PARAMETER 75642-11 75642-12 75642-13
Purgeable Halocarbona (8010)
1,1-Dichloroethene, ug/1
Trichloroethylene, ug/1
Chloroform, ug/1
1,1-Dichloroethane, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,l-Trichloroethane, ug/1
Vinyl chloride, ug/1
Surrogate• Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
110/115 'Ir
125/120 'Ir
ug/1
10-232 'Ir
28-196 \-
<1.0
<l.0
<l.0
<l.0
<1.0
<2.0
<l.0
<l.0
<l.0
89 'Ir
10.10.97
1.0
1008A
lBl0l0
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile. AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 160971016
Page 16
LOG NO
75642-11
75642-12
75642 -13
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
LCS/LCSD \-Recovery
LCS Accuracy Control Limit (\-R)
Method Blank
PARAMETER 75642-11 75642-12 75642-13
Purgeable Aromatics (8020)
Benzene, ug/1 110/120 \-23-168 \-<l.0
Toluene, ug/1 115/125 \-33-167 \-<1.0
Acetone, ug/1 80/85 \-40-130 \-<10
Total Xylenes, ug/1 <3 .0
Surrogate -a,a,a-Trifluorotoluene 100 \-
Date Analyzed 10.10.97
Dilution factor 1.0
Batch ID 1008A
Clock ID 131010
Barium (6010)
Barium (6010) 98/96 Ir 80-120 \-
Beryllium (6010)
Beryllium (6010) 94/90 %-80-120 %-
Chromium (6010)
Chromium (6010) 102/100 i-80-120 \-
Manganese (6010)
Manganese ( 6010) 102/100 \-80-120 \-
Nickel (6010)
Nickel (6010) 105/104 \-80-120 lr
Lead (7421)
Lead (7421) 97 \-80-120 \-
-----------------------------------------------------------
Laboratories in Savannah. GA • Tallahassee. FL • Tampa, FL • Deerlield Beach. FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-01
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 160971016
REPORT OF RESULTS Page 1 7
LOG NO
75642 -11
75642-12
75642-13
PARAMETER
Vanadium ( 6010)
Vanadium (6010)
Zinc (6010)
SAMPLE DESCRIPTION, QC REPORT FOR LIQOID SAMPLES
LCS/LCSD t Recovery
LCS Accuracy Control Limit ('1-R)
Method Blank
75642-11 75642-12
--------------------
105/103 \ 80-120 'I-
75642-13
----------
• Zinc (6010)
Cadmium (7131)
98/96 'I-80-120 %
•
Cadmium (7131)
Antimony (7041)
Antimony (7041)
Suspended Solids (160.2)
Suspended Solids (160.2)
86 'I-
96 'I-
99/96 'I-----------
80-120 'I-
8 0 -12 0 'I-
75-125 i-
--------------------
Laboratories in Savannah, GA • Tallahassee. FL • Tampa, FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
'
REPORT OF RESULTS
LOG NO: S7-75642
Received: 06 OCT 97
Reported: 16 OCT 97
Client PO. No.: 190-00001-0l
Project: 115046-01/MACON DOCKERY
Sampled By: Client
Code: 160971016
Page 18
LOG NO
75642-14
75642-15
SAMPLE DESCRIPTION, QC REPORT FOR LIQOID SAMPLES
Matrix Spike t Recovery
Matrix Spike Duplicate% Recovery·
PARAMETER 75642-14 75642-15
Lead (7421)
Lead (7421) 108 % 108 %
Cadmium (7131)
Cadmium (7131) 89 ~ 88 ~
.Antimony (7041)
Antimony (7041) 92 % 93 %
Methods: EPA SW-846 and 40 CFR Part 136.
Lisa G. McLeod, Project Manager
• Final Page Of Report
Laboratories in Savannah. GA • Tallahassee. FL • Tampa. FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
•
State of North Carolina
Department of Environment,
Health, and Natural Resources
Division of Waste Management
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
William L. Meyer, Director
Ms. Giezelle Bennett
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
6 I Forsyth Street, I Ith Floor
Atlanta, Georgia 30303
November 7, 1997
RE: September 1997 Monthly Progress and O&M Report
Macon/Dockery NPL Site
Cordova, Richmond County
Dear Ms. Bennett:
The Superfund Section of the North Carolina Department of Environment and Natural Resources
(NC DENR) has received and reviewed the September 1997 Monthly Progress and O&M Report
for the Macon/Dockery National Priority List (NPL) Site. The Superfund Section offers the
following comments.
Table 4 Groundwater Quality Summary -Upper/Lower Macon System
I. This table indicates that the Upper/Lower Macon System effluent sampling event yielded a
lead concentration of3. l micrograms per liter (µg/L). However, the laboratory
documentation indicates that the Upper/Lower Macon System effluent contained no
detectable lead concentrations above 3.0 µg/L. Please clarify this discrepancy.
2. This table indicates that the Upper/Lower Macon System effluent was not sampled and
analyzed for suspended solids content. However, the laboratory documentation indicates
that the Upper/Lower Macon System effluent was sampled yet contained no detectable
lead concentrations above 5.0 milligrams per liter (mg/L). Please clarify this discrepancy .
P.O. Box 29603. Raleigh. North Caronna 27611-9603 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmolive Aclion Employer .m Recycled/ 10% Post-Consumer Poper
•
•
Ms. Giezelle Bennett
November 7, 1997
Page2
The Superfund Section of the NC DENR appreciates the opportunity to comment on this
document. If you have any questions or comments, please feel free to call me at (919) 733-
2801, extension 349.
Sincerely,
;l1ZJf(Jb;:µ1111
David B. Mattison, CI-IMM
Environmental Engineer
NC Superfund Section
•
•
•
MACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
MONTHLY PROGRESS AND
O&MREPORT
SEPTEMBER 1997
1iECEIVED
OCT 201997
SUPERFUND SECTION
L
r
• Macon/Dockery Site
•
•
Richmond County, North Carolina
October 9, 1997
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 30365
Re: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress and O & M Report -September 1997
Dear Ms. Bennett:
Reply to: Technical Committee
c/o David L. Jones
Ingersoll-Rand Company
114 Spencer Road
Cassopolis, Michigan
Phone: [phone]"
Fax: [phone] I
On behalf of the Macon/Dockery Site Group ("Group"), the September I 997 Monthly Progress and
0 & M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS
of the Unilateral Administrative Order (effective date -May 30, 1992) for the Macon/Dockery Site.
This report describes activities which occurred during the month of September as part of the
Remedial Action phase of this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH SEPTEMBER 1997:
• Monthly sampling of the water effluent from the remediation systems.
• Continued O & M of systems.
RESULTS OF SAMPLING AND TESTING AND OTHER DATA RECEIVED:
• A summary of the laboratory results for September sampling of the remediation systems is
included in this progress report. Tables I through 4 summarize the analytical results for the
four groundwater treatment systems. The reported effluent concentrations are below the
remediation performance standard.
• Water samples were collected from the sump of the airstripper and between the metals filter
canisters at the Upper/Lower Macon System. The water samples were sampled for
manganese only for filter maintenance information purposes. The results of the analyses are
included in Table 5 .
•
•
•
Ms. Giezelle Bennett
October 9, I 997
Page No. 2
• Upper Dockery flow meter reading for September totaled 52,256 gallons. The system was
operational 100% of the time averaging 1.29 gallons per minute (GPM). Mass VOC
removal was 0.03 pounds for the month and the cumulative is 7.22 pounds.
• Lower Dockery flow meter reading for September totaled 481,049 gallons. The system was
operational 100%, of the time averaging 11.93 GPM. Mass VOC removal was 0.34 pounds
for the month and the cumulative is 5. 82 pounds.
• Macon Source Area flow meter reading for September totaled 36,264 gallons. The system
was operational 97% of the time averaging 0.90 GPM. Mass VOC removal was 0.04
pounds for the month and the cumulative is I . 84 pounds .
• Upper/Lower Macon flow meter reading for September totaled 917,631 gallons. The Upper
Macon system was operational I 00% of the time in September. The Lower Macon system
was operational 97% of the time in September. The combined system flow averaged 22.76
GPM. Mass VOC removal was 0.18 pounds for the month and the cumulative is 2.61
pounds.
TASKS PLANNED FOR OCTOBER 1997;
• Monthly sampling of the remediation systems effluent
• Continue O &M of systems
PROBLEMS AND DELAYS
• September I 8 -The Upper/Lower Macon System infiltration gallery was discovered to be in
an overflow status. Groundwater extraction wells UM-2, UM-( and UM-6 were taken off-
line to allow the water level in the infiltration galleries to drop. On September 26, 1997, wells
UM-2 and UM-4 were restarted since the infiltration galleries appeared to be operating within
their normal operating range. Well UM-6 was restarted during the next site visit on October
2, 1997.
9ct-09-97 05:SlA Applied Earth Sciences 704 795-7076
•
•
•
Ms. Giezelle Bennett
October 9, 1997
Page No. 3.
• September 26 -Macon Source Area System was down due to an electrical surge. The
electrical surge had turned off the pump motor protectors at each of the groundwater
extraction wc:lls. The: pump motor protectors were manually re5et and the system restarted
on the same day. The reason for the electrical surge is suspected to be lightning.
• Percent operational for each system: Upper Dockery
Lower Dockery
Upper Macon
Lower Macon
100%
100%
100%
100%
Macon Source Area 97%
SVE system 100%
Respectfully Submitted,
~~;?~
David Jones
Project Coordinator
cc: Macon/Dockery Site Group Members
Paul Funick, RMT, Inc.
David Mattison, NC Super Fund Section
Norma Eichlan, CDM Federal
P.04
• SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
PROJECT REFERENCE PROJECT NO. P.O.NUMBER
/J1('/l'C,,,,. / Oo,/,J /tJ"i )b'l-cJ<, ,
•
D 5102 LaRoche Avenue, Savannah, GA 31404
D 2846 Industrial Plaza Drive, Tallahassee, FL 32301
D 414 SW 121h Avenue, Deerfield Beach, FL 33442
D 900 Lakeside Drive, Mobile, AL 36693
D 6712 Benjamin Road, Suite 100, Tampa, FL 33634
D 100 Alpha Drive, Suite 110, Destrehan, LA 70047
Serial Number
Phone: [phone]
Phone: (904) 878,3994
Phone: [phone]
Phone: (334) 666·6633
Phone: [phone]
Phone: [phone]•1100
MATRIX
TYPE /REO,IJIRED ANALYSES
PROJECTLOC. SAMPLER(sl"'AME PHONE · ·,,1,, /1.c {I-I 5 IV ~ J ,.,,, '
1-::-:-:::ccr/=c-'L--ccc:::-'--"j"'-( ).;,.:,(lc.::.<._c"<.:_··~/_c,,ij:.c);:::.,..:,I CC~-"~"'. ,'l/,--,,-,---LF_AX_:6°"'7_:_,'S-:,::,)'-'-J-"5'-'8'--.:."..:.'..:,'-'cs~ __ -//
CLIENT NAME CLIENT PROJECT MANAGER
/17(..'!,V,, j}=I,, .,-.4 ,,;;;,, •
75.6
Fax: [phone]
Fax: [phone]
Fax: [phone]
Fax: [phone]
Fax: (813) 885·7049
Fax: [phone]
I PAGE \oF
STANDARD
□REPORT DELIVERY
CLIENT ADDRESS (OITY, STATE, ZIP) □ EXPEDITED REPORT
DE L!VE RY{ surcharge)
A
RELl"t9'UIS~ II' BY: (SIGNATUI E)
s::A./ l"'l -I)[/ 0
~ ' ,~" l
--.,,
"" ll'J -i
....
~1(.. ;M~ ~ C, RELINQUISHED BY: (SIGNATURE)
DA'rE' TIME RECEIVED BY: (SIGNATURE)
I I -
I I
I I
I I
DATE TIME
DATE TIME
LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY: (SIGNATURE) DATE TIME CUSTODY INTACT CUSTODY SEAL NO. SLLOGNO. ' L .. • ~
()\, l,l~11 • l l I 9. 6· '1") Id ,Lf f, ~YES 0No
/ Date Due:
REMARKS
J V ' >--=fu.,\,('._; .... 1..
"'\. '>-.::\-" -\'o -
~~ n
U•' C.~-'\ ·'let-
dt
I
RELINQUISHED BY: (SIGNATURE) DATE TIME
RECEIVED BY: (SIGNATURE) DATE TIME
LABORATORY REMARKS:
_J
4'.
~
Q a: 0
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
•
•
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client _PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
75024-1
75024-2
75024-3
75024-4
PARAMETER
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
Lower Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
--------------------------------------------------
75024-1 75024-2
DATE/
TIME SAMPLED
09-05-97/1450
09-05-97/1500
09-05-97/1520
09-05-97/1540
75024-3
Page 1
75024-4 --------------------------------------- ----------------------------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride (Dichloromethane),
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochlororn~thane
Date Analyzed
Dilution factor
Batch ID
Clock ID
ug/1
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
so %
09.09.97
1.0
0909A
1B0909
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<l.0
<1.0
55 'Ir
09.09.97
1. 0
0909A
1B0909
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<l. 0.
<1.0
<l. 0
57 %
09.09.97
1.0
0909A
1B0909
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
48 %
09.10.97
1.0
0909A
1B0910 --------------------------------------- ---------- -------------------- ----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
•
•
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
75024-1
_75024 -2
75024-3
75024-4
Lower Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
--------------------------------------------------
PARAMETER
-- - ------- -------- ---·----- - --
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Bi!,tCh ID
Beryllium (6010)
Beryllium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
75024-1
<l.0
<1.0
<3.0
<10
97 'l-
09.09.97
1. 0
0909A
1B0909
<50
09.09.97
09.10.97
1. 0
0909J
<5.0
09.09.97
09.10.97
1.0
0909J
75024-2
<1.0
<l.0
<3.0
<10
100 %-
09.09.97
1.0
0909A
1B0909
110
09.09.97
09.10.97
1.0
0909J
<5.0
09.09.97
09.10.97
1.0
0909J
DATE/
TIME SAMPLED
09-05-97/1450
09-05-97/1500
09-05-97/1520
09-05-97/1540
75024-3
<l. 0
<1.0
<3.0
<10
100 'l-
09. 09. 97
1.0
0909A
1B0909
130
09.09.97
09.10.97
1.0
0909J
<5.0
09.09.97
09.10.97
1.0
0909J
Page 2
75024-4
<l.0
<l.0
<3.0
<10
103 %-
09.10.97
1.0
0909A
1B0910
<50
09.09.97
09.10.97
1.0
0909J
<5.0
09.09.97
09.10.97
1. 0
0909J
--------------------------------------- ------------------------------ ----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve ~rminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
75024-1
75024-2
75024-3
75024-4
Lower Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
--------------------------------------------------
PARAMETER
Chromium (6010)
Chromium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Date Analyzed
oiiution factor
Batch ID
Nickel (6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
----------
----------
75024-1
----------
<10
09.09.97
09.10.97
1.0
0909J
<5.0
09.09.97
09.10.97
1. 0
0909J
<40
09.09.97
09.10.97
1.0
0909J
----------
75024-2
----------
<10
09.09.97
09.10.97
1.0
0909J
5.2
09.09.97
09.10.97
1.0
0909J
<40
09.09.97
09.10.97
1.0
0909J
----------
Page 3
DATE/
TIME SAMPLED
09-05-97/1450
09-05-97/1500
09-05-97/1520'
09-05-97/1540
75024-3 75024-4
--------------------
<10 <10
09.09.97 09.09.97
09.10.97 09.10.97
1. 0 1. 0
0909J 0909J
27 <5.0
09.09.97 09.09.97
09.10.97 09.10.97
1.0 1.0
0909J 0909J
<40 <40
09.09.97 09.09.97
09.10.97 09.10.97
1.0 1.0
0909J 0909J
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-0l
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
75024-1
75024-2
75024-3
75024-4
Lower Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
--------------------------------------------------
PARAMETER
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Zinc (6010)
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
----------
----------
75024-1
----------
<3.0
09.10.97
09 .11.97
1.0
0910G
<50
09.09.97
09.10.97
1.0
0909J
<20
09.09.97
09.10.97
l. 0
0909J
----------
75024-2
----------
<3.0
09.10.97
09.11.97
1.0
0910G
<50
09.09.97
09.10.97
1.0
0909J
<20
09.09.97
09.10.97
l. 0
0909J
----------
DATE/
TIME SAMPLED
09-05-97/1450
09-05-97/1500
09-05-97/1520
09-05-97/1540
75024-3
Page 4
75024-4
--------------------
<3.0 <3.0
09.10.97 09.10.97
09.11.97 09.11.97
1.0 1.0
0910G 0910G
<50 <50
09.09.97 09.09.97
09.10.97 09.10.97
1.0 1.0
0909J 0909J
<20 <20
09.09.97 09.09.97
09.10.97 09.10.97
1.0 l. 0
0909J 0909J
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Page 5
DATE/
TIME SAMPLED
75024-1
75024-2
75024-3
75024-4
PARAMETER
Lower Dockery Effluent
Upper Dockery Effluent
Macon Source Effluent
Macon Pad Effluent
Cadmium (7131)
Cadmium (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
75024-1
----------
<0.30
09.10.97
09.11.97
1. 0
0910G
<10
09.10.97
09.11.97
1. 0
09091
<5.0
09.09.97
09.10.97
1. 0
0909A
----------
75024-2
----------
<0.30
09.10.97
09.11.97
1.0
0910G
<10
09.10.97
09.11.97
1.0
09091
<5.0
09.09.97
09.10.97
1.0
0909A
----------
09-05-97/1450
09-05-97/1500
09-05-97/1520
09-05-97/1540
75024-3 75024-4
----------

-
-
-
-
-
-
-
-
-
-
<0.30 <0.30
09.10.97 09.10.97
09.11.97 09 .11.97
1.0 1.0
0910G 0910G
<10 <10
09.10.97 09.10.97
09.11.97 . 09.11.97
1.0 1. 0
09091 09091
22 <5.0
09.09.97 09.09',97
09.10.97 09.10.97
1.0 1. 0
0909A 0909A
--------------------
Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA.
I
•
•
•
,.
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irrninger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
REPORT OF RESULTS Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
75024-5 Macon Pad Sump 09-05-97/1550
75024-6 Macon Pad Midfluent 09-05-97/1555
PARAMETER 75024-5 75024-6
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<5.0
09.09.97
09.10.97
1. 0
0909J
15
09.09.97
09.10.97
1. 0
0909J
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
, .
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354:7858 • Fax [phone]
•
•
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irrninger
·Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
75024-7 Trip Blank
--------------------------------------------------
PARAMETER 75024-7
------------------------------------------------- ----------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1, 1-Dichloroethane, ·ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride (Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
<1.0
<1.0
<1.0
<l.0
<2.0
<1.0
<1.0
<1.0
<1.0
57 %
09.10.97
1. 0
0909A
1B0910
<1.0
<1.0
<3.0
<10
100 %
09.10.97
1,0
0909A
1B0910
Page 7
------------------------------------------------- -------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
REPORT OF RESULTS Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
------------------------------------------------------------------------
75024-8
75024-9
75024-10
75024 · 11
75024-12
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75024-8 75024-9 75024-10 75024-11 75024-12
--------------------------------------------------------------------- ----------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,l-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochlorornethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
1.0
1.0
1. 0
1.0
2.0
1.0
1.0
1.0
1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
68 %
09.09.97
1.0
0909A
180909
19
20
72 %
09.09.97
1.0
0909A
1B0909
----------
19 20
20 20
76 %
09.10.97
1.0
0909A
1B0910
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
75024-8
75024-9
75024-10
75024-11
75024-12
REPORT OF RESULTS
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
--------------------------------------------------
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
Page 9
------------------------------------------------------------------------
PARAMETER 75024-8 75024-9 75024-10 75024-11 75024-12
------------------------------ ---------- ----------
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
1.0
1.0
Total Xylenes, ug/1 3.0
Acetone, ug/1 10
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
so
<1.0
<l.O
<3.0
<10
107 'Ir
09.09.97
1.0
0909A
1B0909
<50
09.09.97
09.10.97
1. 0
0909J
22
23
390
100 'Ir
09.09.97
1.0
0909A
1B0909
1840
09.09.97
09.10.97
1.0
0909J
22
23
370
100 'Ir
09.10.97
1.0
0909A
1B0910
1880
09.09.97
09.11.97
1.0
0909J
20
20
400
2000
--------------------------------------- ---------- ---------- --------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-7°5024
Received: 06 SEP 97
Repor.ted: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
REPORT OF RESULTS Page 10
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
75024-8
75024-9
75024-10
75024 -11
75024-12
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75024-8 75024-9 75024-10 75024-11 75024-12
-------------------------------------------------------------------------------
Beryllium (6010)
Beryllium (6010), ug/1 5.0 <5.0 44.9 46.0 50.0
Preparation Date 09.09.97 09.09.97 09.09.97
Date Analyzed 09.10.97 09.10.97 09.10.97
Dilution factor 1.0 1.0 1. 0
Batch ID 0909J 0909J 0909J
Chromium (6010)
Chromium (6010), ug/1 10 <10 193 197 200
Preparation Date 09.09.97 09.09.97 09.09.97
Date Analyzed 09.10.97 09.10.97 09.10.97
Dilution factor 1. 0 1.0 1.0
Batch ID 0909J 0909J 0909J
Manganese (6010)
Manganese (6010), ug/1 5.0 <5.0 480 491 500
Preparation Date 09.09.97 09.09.97 09.09.97
Date Analyzed 09.10.97 09.10.97 09.10.97
Dilution factor 1. 0 1.0 1. 0
Batch ID 0909J 0909J 0906J ---------------------------------------------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
LOG NO
75024-8
75024-9
75024-10
75024-11
75024-12
REPORT OF RESULTS
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
--------------------------------------------------
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
--------------------------------------------------
Page 11
PARAMETER
Nickel (6010)
75024-8 75024-9 75024-10 75024-11 75024-12
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium ( 6010)
Vanadium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
--------------------------------------------------
40 <40 508 517 500
09.09.97 09.09.97 09.09.97
09.10.97 09.10.97 09.10.97
1.0 1.0 1. 0
0909J 0909J 0909J
3.0 <3.0 50.2 52.0 50.0
09.10.97 09.10.97 09.10.97
09.11.97 09.11.97 09.11.97
1.0 1.0 1.0
0910G 0910G 0910G
50 <50 464 475 500
09.09.97 09.09.97 09.09.97
09.10.97 09.10.97 09.10.97
1.0 1.0 1.0
0909J 0909J 0909J
------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
REPORT OF RESULTS Page 12
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-------------------------------------------------- ------- ---------------
75024-8
.75024-9
75024-10
75024-11
75024 -_12
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75024-8 75024-9 75024-10 75024-11 75024-12
-------------------------------------------------------------------------------
Zinc (6010)
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadrni urn ( 7131)
Cadmium· (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
20 <20
09.09.97
09.10.97
1.0
0909J
0.30 <0.30
09.10.97
09.11.97
1.0
0910G
10 <10
09.10.97
09.11.97
1.0
0909I
----------
494 506 500
09.09.97 09.09.97
09.10.97 09.10.97
1. 0 1.0
0909J 0909J
4.99 4.99 5.00
09.10.97 09.10.97
09.11.97 09.11.97
1.0 1.0
0910G 0910G
47.6 47. 4 50.0
09.10.97 09.10.97
09.11.97 09.11.97
1. 0 1. 0
0909I 0909I
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 115870916
REPORT OF RESULTS Page 13
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
75024-8
75024-9
75024-10
75024-11
75024-12
Reporting Limit (RL)
Method Blank
Lab Control Standard Result
Lab Control Standard Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 75024-8 75024-9 75024-10 75024 -11 75024-12 -------------------------------------------------------------------------------
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
5.0 <5.0
09.09.97
09.10.97
1. 0
0909A
----------
94 97 100
09.09.97 09.09.97
09.10.97 09.10.97
1.0 1.0
0909A 0909A
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-75024
Received: 06 SEP 97
Reported: 16 SEP 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 133070916
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
--------------------------------------------------
75024-13
75024-14
LCS/LCSD % Recovery
LCS Control Limits
--------------------------------------------------
PARAMETER
--------------------------------------- ----------
Purgeable Halocarbons (8010)
1,1-Dichloroethene
Trichloroethylene
Purgeable Aromatics (8020)
Benzene
Toluene
Acetone
Barium (6010)
Barium (6010)
Beryllium (6010)
Beryllium (6010)
Chromium (6010)
Chromium (6010)
Manganese (6010)
Manganese (6010)
Nickel (6010)
Nickel (6010)
Lead (7421)
Lead (7421)
vanadium (6010)
Vanadium (6010)
Zinc (6010)
Zinc (6010)
--------------------
75024 -13
95/95 %
100/100 %-
110/110 %
115/115 %-
98/92 %-
92/94 %-
90/92 %
96/98 %
96/98 %
102/103 %
100/104 %
93/95 %
99/101 %
----------
Page 14
75024-14
10-232 %-
28-196 %
23-168 %-
33-167 %-
40-130 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-75024
Recei,ved: 06 SEP 97
Reported: 16 SEP 97
Client PO. No.: 190-00001-01
Project: 190-109564.04/MACON DOCKERY
Sampled By: Client
Code: 133070916
REPORT OF RESULTS Page 15
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
75024-13
75024-14
LCS/LCSD %-Recovery
LCS Control Limits
-----------------------------------------------------------------------------------
PARAMETER 75024-13 75024-14
----------------------------------------------------------- ---------- ----------
Cadmium (7131)
Cadmium (7131)
Antimony (7041)
Antimony (7041)
Suspended Solids (160.2)
Suspended Solids (160.2)
100/100 %-
95/95 %-
94/97 %-
80-120 %-
80-120 %-
75-125 %-
------------------------------------------------- ------------------------------
Methods: EPA SW-846 and 40 CFR Part 13£.
Lisa G. McLeod, Project Manager
Final Page Of Report
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
Sample °"' Location
UD Influent 2/13/96
2/13/96
2/14/96
2/14/96
2/14/96
2/14196
2/15/96
2/15/96
2/16196
2/17/96
2/17/96
2122196
2122196
2128/96
2/28/96
318/96
413/96
413196
513196
615/96
7/1196
8/1/96
I1nl96
lln/96
2/5/97
5114191
sn191
UD Effiuent 2/13/96
2/14/96
2/14/96
2/15/96
2/16196
2/17/96
2122196
2128/96
3/8/96
413/96
S/3/96
615196
7/1/96
8/1/96
9/4196
10/1/96 ·
Itn/96
12/5/96
1/6197
2/5/97
3/12197
4/8/97
5114191
616197
7'2/97
8nm
9/5197
RemedraUon Perfonnancc Standard
NA~ Not Analyzed
N01.e: • Acetcnc err.finned by McthDd 1260
1,1-Dicblorocthanc
, ... n)
4.8
7.7
4.3
6.5
4.4
4
4.5
S.5
1.S
5.7
S.5
S.4
49
6.4
6.8
52
3.6
3
4
2
2
6.1
<10
NA
<2S
<1.0
<LO
<1.0
<1.0
<1.0
<1.0
<l.0
<1.0
<l.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
3500
Table 1
Groundwater Quality Summary
Upper Dockery
Macon/ Dockery Site
Richmond County North Carolina
1, I . Dichlorocthenc Cis/trans-1, 2-Dichlorocthcne T etrachlorocthenc
("O'l,) (uglL) ("•")
!SOE L3 L3
130 <1.0 <1.0
89E 1.2 <1.0
100 <1.0 <1.0
120E 1.4 L3
110 <1.0 <1.0
130E 1.2 1.4
140 2 <LO
160 <1.0 <1.0
180E 1.7 2.1
120 <1.0 <1.0
\SOE 1.4 <1.0
96 <1.0 <1.0
200E 1.9 I
240 <1.0 <1.0
130"F35 1.7 <1.0
160E I.I 1.6
92 <1.0 <1.0
130 <1.0 <l.O
110 <1.0 <1.0
77 <l.O <1.0
220 <5.0 <5.0
240 <10 <10
NA NA NA
100 <25 <2S
56 <1.0 <l.0
39 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<l.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <l.O <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
1.5 <1.0 <1.0
<1.0 <1.0 <1.0
<l.O <l.0 <1.0
<1.0 <l.O <1.0
<1.0 <l.O <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
70
•
I, l,l •Trichlorocthanc T ricbloroethyl.cno Toluene Total Xyleoea
(,wfl) (.,.JI) ,,~fl) (=fl)
54 8 3 3.1
33 <1.0 <1.0 <3.0
55 4.5 <1.0 <3.0
34 S.3 <1.0 <3.0 so 7.9 <1.0 <3.0
48 7.8 <1.0 <3.0
S4 8.3 <1.0 <3.0
S6 8.6 2.8 <3.0
64 10 <1.0 <3.0
62 9.4 <1.0 <3.0
42 6.4 <1.0 <3.0
52 5.7 <1.0 <3.0
48 ,., <1.0 <3.0
19 5.3 <1.0 <3.0
50 <1.0 <1.0 <3.0
" 3.8 <1.0 <3.0
38 5.6 <1.0 <3.0
" 3.9 <1.0 <3.0
38 4.8 <1.0 <3.0
S.2 <1.0 2.8 <3.0
" 3.6 <1.0 <3.0
52 S.1 <5.0 <15
S4 <10 <10 <30
NA NA NA NA
31 <25 <25 <15
16 3.5 <1.0 <3.0
13 2.2 <1.0 <3.0
<1.0 <l.O <1.0 <3.0
<1.0 <1.0 <l.O <3.0
<1.0 <1.0 <LO <3.0
<1.0 <1.0 <1.0 <3.0
<l.O <1.0 <1.0 <3.0
<l.0 <l.O <l.O <3.0
<1.0 <1.0 <l.0 <3.0
<l.0 <1.0 <1.0 <3.0
<1.0 <l.O <1.0 <3.0
<l.O <1.0 <LO <3.0
<l.0 <1.0 <l.O <3.0
<1.0 <1.0 3.9 <3.0
<l.O <1.0 <1.0 <3.0
<1.0 <1.0 <l.O <3.0
<1.0 <1.0 <1.0 <3.0
<1.0 <1.0 <1.0 <3.0
<l.O <1.0 <1.0 <3.0
<l.O <1.0 <1.0 <3.0
<l.O <LO <1.0 <3.0
<l.O <LO <1.0 <3.0
<l.O <1.0 <l.0 <3.0
<l.O <1.0 <1.0 <3.0
<l.O <1.0 <l.O <3.0
<1.0 <1.0 <l.O <3.0
<1.0 <l.O <1.0 <3.0.
<LO <1.0 <1.0 <3.0
<l.O <l.O <1.0 <3.0 .·.
200 2.8 400 -;'! -:, .. -
-~d~:·~-~~j;;i~ij~~~ ~:~-
e Swnpl, °'" Location UD Influent 2/13/96 2/13/96 2/14/96 2/14/96 2/14/96 2/14/96 2/15/96 2/15/96 2/16/96 2/17/96 2/17/96 2/22/96 2/22/96 2/28196 2/28/96 3/8/96 4/3/96 413196 513196 6/5196 7/1/96 ' 8/1/96 11n195 lln/96 2/5/97 S/14/97 Bn/97 UDEffiucnt 2/13/96 2/14/96 2/14/96 2/15/96 2/16/96 2/17/96 2/22/96 2/28/96 3/8/96 413196 5/3/96 615196 111196 8/1/96 9/4/96 1011/96 lln/96 12/5/96 1/6/97 2/5/97 3/12/97 41'8/97 SI\ 4191 616191 7/2/97 Bn/97 9/5/97 Remediation Performance Standard NA• Not Ana!yiod Noto:• AcCUIIIO cooflllllOd by Method 8260 Table 1 (Continued) Groundwater Quality Summary Upper Dockery Macon/Dockery Site RiC::hmond County, North Carolina --Acetone Chromium ----(ug'L) (ug/L} (ug/L) (u"n) <10 20 92 64 <10 <10 <50 <S.O <10 12 53 14 <10 <10 <50 <S,O <10 11 54 14 <10 <10 <50 <5.0 <10 19 81 53 <10 <10 <50 <5 0 <10 11 57 11 <10 <10 55 12 <10 <10 <50 <5.0 <10 13 <50 13 <10 <10 <50 <5.0 <10 11 <50 1.1 <10 <10 <50 <S.O <10 <10 <50 <5.0 <10 11 52 <5.0 <10 <10 <50 <S.O <10 16 58 <5.0 <10 <10 <50 <50 <10 <10 <50 <S.O <50 11 <50 5.5 2100 19 61 9.5 1so· NA NA NA <250 12 51 <5.0 <10 <10 58 5.3 <10 <10 <50 <5.0 70"F32 16 11 40 3S"F33 15 53 14 <10 11 56 12 <10 12 53 14 <10 <10 53 11 <10 11 55 12 <10 <10 <50 83 <10 13 <50 9.6 25 <10 <50 6.9 28 II 50 <S.O 52 <10 <50 <5.0 <10 <10 <50 <S.O <10 <10 <50 <S.O 20 14 51 1 <10 <10 55 <S.O <10 <10 <50 5.9 <10 15 59 <S,O <10 12 54 5.1 <10 13 54 <5.0 <10 15 61 5.9 <10 <10 69 <5.0 <10 <10 63 <5.0 <10 <10 60 1.2 <10 <10 52 <5.0 <10 <10 55 <S.O <10 <10 <50 <S.O <10 <10 110 5.2 3500 50 1000 50 • Zinc L<,d Suspended Solids (,wfl) , ... n) (-fl) 33 3.1 SI <20 <JO <5.0 <20 <3.0 52 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <30 8 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 8 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 5 <20 <3.0 10 <20 <3.0 <5.0 NA NA NA <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 22 <3.0 14 <20 <3.0 11 <20 <3.0 <5.0 <20 <30 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 10 <20 <3.0 <5.0 <20 <3.0 5 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 8 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <3.0 <5.0 <20 <30 <5.0 <20 <30 <5.0 5000 15 7. -~ , ··"" .-'1" .~ .... , •• . _':,11i~~~tll:i:~_:_'., ·
Sample Date
Location
LO Influent 2/13/96
2/14/96
2/14/96
2/14196
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
2/28/96
3/8/96
4/3196
513/96
6/5196
8/1/96
llnl96
3/12/97
5/14/97
8nl97
Remediation Performance Standard
/\ate: A blank means below detection !imit
•
Chloroform
(ug/L)
1.1
1.3
<l.0
1.6
<1.0
1.2
3.3
2.5
1.2
<1.0
2
<1.0
<1.0
<1.0
<2.0
<2.0
<5.0
<1.0
<1.0
Table 2
Groundwater Quality Swnmary
Lower Dockery
Macon/ Dockery Site
Richmond Countv, North Carolina
I, 1 -Dichloroethane 1, I -Dichlorocthene Ci s/trans-1,2-Dichloroethenc
(ug/L) (ug/L) (ug/L)
80 33 <l.O
llOE 43 <1.0
80 13 <1.0
94E 39 1.8
64 16 2.2
82 32 1.7
95 35 2.6
5.8 100 <1.0
93E 33 <1.0
92 35 <1.0
110 47 <1.0
79 36 <1.0
71 30 1.7
67 32 1.1
83 27 <4.0
69 28 <2.0
66 21 <5.0
62 25 <1.0
47 15 <1.0
3500 7 70
•
Methylene chloride 1,1,l-Tric~orocthane
(ug/L) (ug/L)
<2.0 40
<2.0 37
<2.0 15
1.7 39
2.5 18
<2.0 29
<2.0 31
<2.0 54
<2.0 30
<2.0 30
<2.0 34
<2.0. 28
<2.0 40
2 42
<2.0 54
<4.0 38
<10 23
<2.0 23
<2.0 18
5 200
Sample Date
Location
LD Influent 2/13/96
2/14/96
2/14/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
2/28/96
3/8/96
4/3/96
5/3/96
615196
8/1/96
1 ln/96
3/12/97
5/14/97
8n/97
Remediation Performance Standard
~etc: A blank means below detection limit
T richlorocthylene Benzene
(ug/L) (ug/L)
6.4 <2.0
8.6 <2.0
<5.0 <2.0
9 <2.0
6.6 <2.0
8.4 <2.0
8.7 <2.0
5.2 1.8
7.4 <2.0
6.4 <2.0
6.7 <2.0
6.6 <2.0
5.4 <2.0
5.2 <2.0
5.9 <2.0
5.8 <2.0
<5.0 <5.0 F34
6.2 <1.0
4.1 <l.O
2.8
TABLE 2 (Continued)
Groundwater Quality Sununary
Lower Dockery
Macon/ Dockery Site
Richmond Countv, North Carolina .
Toluene Total X ylenes Chromium
(ug/L) (ug/L) (ug/L)
17 <3.0 <10
8.3 <3.0 <10
<2.0 <3.0 <10
8.3 <3.0 <10
6.5 <3.0 <10
5.3 <3.0 <10
4.3 <3.0 <10
13 3.4 14
1.3 <3.0 <10
<2.0 <3.0 <10
<2.0 <3.0 <10
<2.0 <3.0 <10
<2.0 <3.0 <10
2.5 <3.0 <10
<2.0 <6.0 <10
<2.0 <6.0 <10
<5.0 <15 <10
<1.0 <3.0 <10
<l.0 <3.0 <10
1000 400 50
•
..
Barium Manganese Zinc Cadmium • Suspended .Solids
(ug/L) (ug/L) (ug/L) (ug/L) (mg!LJ
<50 260 270 <0.30 . <5.0 .
<50 250 120 <030 .<5.0
<50 <5.0 <20 <0.30 <5.0 ..
<50 240 110 <030 <5.0
<50 <5.0 <20 <O.J°O <5.0
<50 200 84 <0.30 <5.0
<50 190 81 <0.30 <5.0
<50 240 240 <0.30 <5.0
<50 120 77 <0.30 8
<50 <5.0 <20 <0.30 <5.0
<50 95 30 . <0.30 <5.0
<50 160 39 <0.30 <5.0
16 63 200 0.91 <5.0
<50 230 46 <0.30 <5.0
<50 110 <20 <0.30 5
<50 230 <20 <0.30 <5.0
<50 76 <20 <0.30 <5.0
<50 150 <20 <0.30 . <5.0
<50 130 <20 <0.30 <5.0
1000 50 5000 5
Sample Date
Location
LD Effiuent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
8/1/96
9/4/96
lO/l/96
lln/96
12/5/96
l/6/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
8n/97
9/5/97
Remed1at1on Performance Standard
'.\'otc: A blank means below detection limit
Chlorofonn
(ug/1..)
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<l.O
<1.0
<1.0
<l.O
Table 2
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond Countv North Carolina . ,
1,1 -Dichloroethane I, 1 -Dichloroethene Cis/trans-1,2-Dichloroethene
(ug/1..) (ug/1..) (ug/1..)
<l.O <1.0 <l.O
<l.O <l.O <l.O
<l.O <1.0 <1.0
<1.0 <l.O <l.O
<1.0 <l.O <1.0
<l.O <1.0 <1.0
<1.0 <l.O <1.0
<l.O <l.O <1.0
<l.O <l.O <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<1.0 <1.0 <l.O
<1.0 <1.0 <l.O
<l.O <1.0 <l.O
<1.0 <1.0 <l.O
<1.0 <1.0 <1.0
<1.0 <1.0 <l.O
<l.O <l.O <l.O
<l.O <l.O <l.O
<l.O <l.O <l.O
<1.0 <l.O <l.O
<l.O <l.O <l.O
<1.0 <l.O <l.O
3500 7 70
•
Methylene chloride 1, l, l • Tri.chl~ane . (ug/1..) (ug/1..) .· .
<2.0 <l.0
<2.0 <l.O ' <2.0 <i.O-
<2.0 <l.O ..
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.0
<2.0 <l.O
<2.0 .,:LO
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O
<2.0 <l.O·
<2.0 <l.O
<2.0 <l.0
<2.0 <l.O
<2.0 <l.O
5 200 ..
••;;· -.. ·«.
-t~~,f 1\~~--~~.;
Sample
Location
LD Elluent
Date
2/13196
2/14196
2/14/96
2/15/96
2/16/96
2/22196
2/28/96
3/8/96
4/3196
5/3/96
8/1/96
9/4196
10/1/96
lln/96
12/5/96
1/6/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
8nt97
9/5/97
Remediation Performance Standard
Xote: A blank means below detection limit
T richloroethylene
(ugll,)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
2.8
Benzene
(ugll,)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<1.0
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
TABLE 2 (Continued)
Groundwater Quality Summary
Lower Dockery
Macon/ Dockery Site
Richmond County North Carolina
Toluene
(ug/L)
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.O
<1.0
<1.0
3.4
<1.0
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
IO00
Total X ylcnes
(ugll,)
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
<3.0
400
•
Chromium
(ugll,)
<10
<10
<10
<10
<10
<10
<10
<IO
<10
<IO
<IO
<IO
<IO
<IO
<IO
<IO
<10
<10
<10
<10
<10
<10
<10
50
Barium
(ugll,)
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
<50
70
<50
<50
<50
<50
<50
<50
IO00
Manganese
(ugll,)
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
14
13
11
<5.0
35
6
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
50
Zinc
(ugll,)
<20
:<20
<20
<20
<20
<20 '.
<20,
<20
<20
<20 -
<20
<20
<20,
<2_0:
<20
<20·
<20'. ~o··:
<20.;
<20
<20,
<20
5000 ·
. --' -. -·
Cadmium
(ugti;)
Suspended_ Solids
(mg/l) .
<(l.30.
<(l.30
A).30· . ' .<0.30
.<tl.30
·<0.30 . ·•
='°•3.0
... <5.0
<5.0 ·. 11 ·,.
. <5.o. ' . ;.<5.0 .' '· ,·
s .,
<5.0 . :::-.
<S.0-~. ·-: .,s.o ·.'
.. <5.0 •
. ,<0.30
· <0.30
<0.30
<0.30 -· O.s6· ~.--'.
• 5: '<5,0 •
~ <5.0 . . . . '.'5.0 > . <0.3_0 :
<0.30,
<0.30· :' •
<0.30
.• ,s:0:J_9.: ~
•• <0.30. .. ~.30:' .
·. <Cl.Jo' '.' .
<030 . '·
~}O
. <0,30 .•
s.
;<5.0·.-•'
19 '· ..
.·<5.0.·','·
. <5.0· ·;:;:~.o'.. ' . <.5.0 .
~ .<5.o .
. <5.0
<5.0 • <5,0
-, .
,i;,~.:~:1~~~#11':
Sample Date
Table 3
Groundwater Quality Swnma,y
Upper Macon Source Area
Macon/ Dockery Site
Richmond County, North Carolina
---... -. '.-·· ---·. ... -.. .~ •:: . •:".
-·.:-•.· -·-·· _: .. -.
Chloroform I, I -Dichloroethanc 1, 1 -Dichloroethene Cis/trans-1,2-Dichloroethene Tctra.chlorocthene 1 1 I Trichloroethane TrichI~CDe ~ .. , .
Location
lJ'11SA Influent 2/t3/96
(uglL) (uon) (uglL) (uglL) (u"1Ll ••• (u.JLl ' .. ' ··,-,. (u~:i~:-c-;: ~,,--,-----1-:==--+-~~--4--...l::!':!"l--+--~~--+-------l~~---!--~.::J.---4--~~"--+;___-,1!:~~..,f.l · .. .-,, , a <LO 15 14 19 16 , -5.9 _ ~--25 -~ :.::-·.;, .
2/14/96
2/t4/96
2it5/96
2it6/96
2/17/96
2/22/96
2/28/96
;/o :~ :! :~ ~-; ~:! -. : \r.::t}) i;:{:•, ___ :".:_.:··:··,··· <LO 12 14 11 18 :·S.9 ., -1 .•. r .:: 1_6· . ._:,.:.~~~ t-; ,,. ?·: _ ~
<1.0 1.s 21 11 14 9.1·-. · :,,,, ·zs .--3~:-._ ...;·
<t.O 9.7 t8 t6 ti 7 .• ;: 24-_::: ~,:. ·:.
I.I 10 17 16 15 7.6 ; ·25 ... -·,· .• 7
<1.0 9.8 16 13 12 5.8 . · ··~·2):· .:'_ ' -~
3/8/96
4/3/96
<t.O 7.6 ID 10 7.7 "4.1 ,16-; . 0 ,
<LO 5.5 16 8.5 7.4 5.4 ~ -· 18 ~ ' ~ ·...-· "'
5/3/96 <1.0 4.8 12 6.9 5.7 ~1.0 : 12 ,. ~
6/5/96 ' <LO 8.7 22 6 <LO .6 -13· -
7/t/96 <t.O 3.8 11 6.9 4.8 4.3 • -·12
7/30/96 <t.O 7.9 15 ID 6.4· 4.l°'C •· 13.
ttn/96
2/4/97
(DUP) 2/4/97
5/12/97
<LO 7.2 9.2 7.5 2.3 3.4. · :;._ ·. · •-1 -IQ, _
:: ~ ~:~ ;; ~:~ !:; ~:: . :' .. . . :; ·_:! :.: . ' :
<t.O 3.8 26 16 8.9 5 • 22· ..
(DUP) 5/12/97
8/7/97
<1.0 4.6 21 16 8.2 3.7' .,., ·/~ · ... -~.18 ~ ;-:;~~·:-, .
<LO 11.0 55 23 12 6.9 • ,, -:0\>·11~:.r.~•.:.;.
Remediatmn Performance Standard 3~0 7 M 200
Note: :--:A• Not Analyzed
DUP -duplicate
., t'
• • ' + •• '• -~----------------.. ~.,.
Sample Date
Location
UMSA Influent 2/13/96
2/14/96
2/14/96
2/ll/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
lrJ/96
6/l/96
7/1/96
7rJ0/96
lln/96
2/4/97
(DUP) 2/4/97
l/12/97
(DUP) l/12/97
Vinyl chloride Benzene
(u•/1) (uo/1)
Table 3 (Continued)
Groundwater Quality Summary
Upper Macon Source Area
Macon/Dockery Site
Richmond County North Carolina
Toluene Chromium Barium Manganese Zinc
(uo/1) (uglL) (ug/L) (uglL) (uo/1)
Cadmium Lead M
(uo/1.\ (uo/1_\ (;::;;'{:
<LO <LO 1.9 <10 140 300 5.5 <0.30 3.5 .<.l..,.
<1.0 1.5 <1.0 <10 I 10 180 <20 <0.30 <3.0 <.2
<1.0 I <I.0 <10 110 160 20 <0.30 <3.0 "<.2
<1.0 1.3 I <10 100 140 <20 <0.30 <3.0 <.2' ·
<1.0 <1.0 <1.0 <10 120 160 <20 <0.30 <3.0 ,0.22·_
-21-.·
<S,o ...
-,5.0: :_'
<S.0.
<s.o·
<LO <1.0 <LO <IO 110 110 <20 <0.30 <3.0 <.2. , <5.0 •.
<LO <1.0 <I.0 <10 120 65 <20 <0.30 <3.0 <.2 ·., <;5.0 · •
<1.0 <1.0 <1.0 <10 130 52 <20 <0.30 <3.0 <.2 •. ?:.. .. -__
<LO <1.0 <1.0 <IO 130 41 <20 <0.30 <3.0 <.2'._ _<S.O, ·
<LO <1.0 <1.0 <10 110 27 <20 <0.30 8.2 <.2•· -·<5.0
<1.0 <1.0 <1.0 <to 97 21 <20 <a.Jo <J.Q <.2 -· · ifo ..
1.1 <1.0 3.6 <IO 130 19 <20 <0.30 <3.0 <.2 -. S ,-<1.0 <1.0 <1.0 11 I IO 13 <20 <0.30 <3.0 1 . NA,~· '-S -.. .,
4.5 <1.0 <LO <IO 130 13 <20 <0.30 <3.0 NA, ~ --6 ,:._
2 <1.0 I <IO 140 9.8 <20 <0.30 <3.0 .NA_· . ,rs . •iO.~~~
<LO <1.0 <1.0 <10 150 24 <20 <0.30 <3.0 . NA :..,.--36,. -...
<LO <1.0 <1.0 <10 140 17 <20 <0.30 <3.0 NA _ . /~ :-'~r~ t~ _ .. r-4:
<1.0 <1.0 <1.0 <IO 120 68 <20 <0.30 <3.0 ·. N~i--~'. 1"-· ···<S.0. ·•
<1.0 <LO <1.0 <IO 150 55 <20 <0.30 <3.0 ·NA._' 1\{~-• •:1'. , ·~.
8n/97
Rcmcdialion Performance Standard
<1.0 <LO <1.0 34 210 93 <20 <0.30 7.4 -NA -NS ·-.
---'-"'-''-'-'-.L..-"7''----L--;"--L-1'"0::,o"o-''---';,lO::---L--,lc;;O:;:OO;:---'---,l,::O--L-l"o"'o"o--'-....;':'l"'-_._.,l;,l,-'--,1".1""_ -'--'-':.=;...-,--' .
Note: NA -Not Analyzed
DUP -duplicate
• •
Sample Date
Location
1.J'11SA Effiuent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
615196
7/1/96
7/30/96
9/4/96
10/1/96
lln/96
12/5/96
1/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
7/2/97
8n/97
9/5/97
Remed.tallon Performance Standard
Note: NA • Not Analyzed
DUP • duplicate
•
Chloroform 1,1 -Dichloroethane
(u,n., (u•n)
<l.O <1.0
<1.0 <1.0
<LO <1.0
<LO <LO
<LO <1.0
<LO <1.0
<LO <1.0
<1.0 <1.0
<LO <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <LO
<1.0 <LO
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
3500
Table 3
Groundwater Quality Summary
Upper Macon Source Area
Macon/ Dockery Site
Richmond County, North Carolina
1,1 • Dichloroethene Cis/trans-1,2-Dichloroethene Tetrachloroethenc
(uoll) (u,.tL) (u,n.\
<1.0 <1.0 <1.0
<LO <i.O <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<LO <LO <1.0
<1.0 <1.0 <LO
<1.0 <1.0 <LO
<1.0 <LO <1.0
<l.O <LO <1.0
<l.O <LO <1.0
<1.0 <1.0 <1.0
<1.0 <I.0 <1.0
<1.0 <LO <1.0
<1.0 <LO <1.0
<l.O <1.0 <1.0
<l.O <1.0 <1.0
<LO <l.O <1.0
<1.0 <l.O <LO
<LO <1.0 <LO
<1.0 <1.0 <LO
<I.0 <1.0 <l.O
<LO <LO <1.0
<1.0 <1.0 <1.0
<LO <1.0 <1.0
<1.0 <1.0 <LO
7 70
•
--=--.,...::..•. -· ·' ... ... ~-. .. . . : ... _.
' '-~
1, 1,1: Trichloroethane Trichlorocthylene
.. ·c (u•n.\: ·"(u•li.\ ;...
<1.0 . . . . ~-, <1.0~ · <to' ;·· .. · .-<i:o• .
-· lit:'· : :JjII1 '." :
<;1.0 .. : =:<I-.~·----.....
<1.0
<Lo:
. -<l.O -<1.6' ,: ·• -.
. <1.0 . ..,_. -(
--<~.'~
r
Table 3 (Continued)
Groundwater Quality Summary
Upper Macon Source Area
Macon/Dockery Site
Richmond County, North Carolina
Sample Date Vinyl chloride Benzene Chromium Barium
Location (u ) (ug/L) {ug/L)
m.1SA Effluent 2/13/96 16 150
2/14/96 <1.0 <1.0 <1.0 <10 110 190
2/14/96 <1.0 <1.0 <LO <10 110 160
2/15/96 <1.0 <1.0 <1.0 <10 100 140
2/16/96 <1.0 <1.0 <LO <10 130 170
2/17/96 <1.0 <1.0 <1.0 <10 120 120
2/22/96 <1.0 <1.0 <LO <10 120 70
2/28/96 <1.0 <1.0 <LO <10 130 51
3/8/96 <1.0 <1.0 <1.0 <10 120 37
4(3196 <1.0 <1.0 <1.0 <10 110 27
5(3/96 <1.0 <1.0 <1.0 <10 120 26
615196 <LO <1.0 2.9 <10 130 22
7/1/96 <LO <LO <1.0 12 110 14
1(30196 <l.0 <1.0 <1.0 <10 200 110
9/4/96 <1.0 <LO <LO 11 170 68
10/1/96 <1.0 <LO <1.0 <10 130 13
lln/96 <LO <LO <1.0 <10 140 13
12/5/96 <1.0 <LO <1.0 <10 170 17
1/6/97 <1.0 <1.0 <1.0 <10 200 46
2/4/97 <LO <1.0 <1.0 <10 160 29
3/12/97 <1.0 <1.0 <1.0 <10 130 30
4/8/97 <1.0 <1.0 <l.O <10 200 30
5/12/97 <1,:..0 <1.0 <l.0 12 210 95
6/6/97 <1.0 <1.0 ' <1.0 <10 240 74
7/2/97 il.O <1.0 <1.0 <10 180 41
8nm <LO <1.0 <1.0 II 230 250
9/5/91 <1.0 <1.0 <1.0 <10 130 27
Remediation Performance Standard I I 1000 50 1000 50
Note: NA -Not Analyz.ed
DUP -duplicate
e ::i-:, '
• .¥'Cl.;! m·, Ai~½ftNr'Jr · ··~·-!;· .. ~ •
Zinc Cadmium Lead
20 <0.30
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.o·
<20 <0.30 <J.9
41 <0.30 9.2
26 <0.30 66.
<20 0.47 <3.0
<20 <0.30 <3.0.
<20 <0.30 <3·.o
25 <0.30 3.5
<20 <0.30 <3.~
<20 <0.30 <3.0
<20 <0.30 <3.0
35 <0.30 <3.0
<20 <0.30 <3.0
<20 <0.30 <3.0
40 <0.30 4.8
<20 <0.30 <3.0
5000 5 15
-~ }~;i~l i:~d~-~~-~~-~-'.: ·::
· -~ :44 ,~/;, __ ,~}i~"'fr;:..i• ~ :.: : ·
Merwry ~~~~~~;;~~;~£{t:~·~.~ .:-·
) &>$11!"~---;,;,;;.; """tr'''<'••. ' _:~· ::';~ti~:_~: r·!::"ff,; 1it > , .. , -,,,,,rrli,
~f 1.!~_t:.t_: .-. . ~ .. ~~~' ·::_, '. .
.... .:.
;~--,:.7
~
-,~
:{(.~.
:'NA.· .NA-·
. •.,-..
'J ~--•""k •·. -•-
;'i~:..::<· :·
I•-~~
, .
1,f::.,., -• -.. J5?~\·· .. ;:. ..
Sample
Location
UM Influent
LM Influent
(DUP)
2121/96
2122/96
2122/96
2/]3/96
2124/96
2125/96
2128/96
318196
3/16196
413/96
615196
7/1196
7/30/96
lln/96
214/97
5/12/97
8nt97
2121/96
2122/96
2122/96
2/]3/96
2124/96
2125/96
2128/96
3/8196
3/16/96
4/3/96
5/3/96
615196
7/30/96
l tn/96
2/4197
214197
5/12197
Sn/97
Rcmcd1at10n Perfornuncc Standard
DUP -duplicate
NA= Not Analyzed
•
Chlorofonn
(u.tl)
16
10
6
3
1.4
1.2
3.5
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<LO
<l.0
<1.0
17
15
14
13
8.9
8.2
3
<1.0
<1.0
<1.0
<1.0
<LO
<LO
<1.0
1.6
1.5
<1.0
<1.0
1
1,1 -Dichlorocthanc
(u.tl)
3.1
3.9
4.1
4.5
4.6
<1.0
5.8
4.7
5.5
4.4
4.9
3.8
4.1
5.3
5.5
11
5.8
15
22
26
29
30
31
32
9.5
8.1
7.3
8.6
12
17
11
9.8
9.0
5.3
13.0
3500
Table 4
Groundwater Quality Summary
Upper/Lower Macon System
Macon/ Dockery Site
Richmond County, North Carolina
1,1 -Dichlorocthene Cis/trans-1,2-Dichlorocthenc Methylene chloride
(uo/1.) (u•" )
1.1 4.6
1.5 5.5
1.6 5.8
1.6 6.4
1.8 6.4
2.2 6.6
1.4 8.6
1 8.6
1.8 9.2
1.6 6.6
1.8 7.7
1.1 6.1
2.1 8.6
1.9 6.6
1.6 7
2.5 1.8
1.8 7
5.5 2.1
8.4 3.3
9.1 4.4
II 4.9
13 4.9
13 5
15 5.6
1.6 2.4
1.8 2.4
2.6 2.3
2.7 2.9
4.7 3.4
6.6 <1.0
3.3 2.2
2.1 2.4
1.8 2.1
2.4 6.4
<1.0 1.2
7 70
•
(uo/1).
<20 ·'.
<20
<2.0
<20
<20
<20
<20
<2.0
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<20
<2.0
<20
<2.0
<2.0
<20
<2.0
<2.0
<2.0
<20
<2.0·
<2.0
<2.0
<20
<2.0
5
-1.7.
2·
·• 21
·27
"26
2.4
.. t-";..:" . . :..,,.
11
14
15
17
17
17
'
'ti;;~ .... -_;{~·~ ✓ ,e.t, ·:, 4'\· , .. ~:.. -~ ~ • -" ·Cf1i:,d/.-·-.) iifj)41/_.k,1~:~'-/'. -~?~~ ~~:1/.:_J:..__ ~~~;~, ..
Sample D,te
Location
UIL Effiuent 2121/%
2121196
2121196
2f13/%
2124/%
2125/%
2128/%
3/8196
3/16196
4/3/%
513/%
6/5196
7/1196
7{30/96
914196
10/1196
lln/96
12/5196
1/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
7fl197
7(15/97
8/7/97
915191
Note: 7/25197 Sampled for Mmganese only.
DUP -duplieate
NA= Not Analyzed
•
Chloroform l,l -Dichloroc:thanc
(u,vl) (u,vl)
<l.O <1.0
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 1.8
<1.0 <LO
<LO <1.0
<LO <1.0
<LO <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
<1.0 <1.0
<1.0 <l.O
<LO <1.0
<1.0 <LO
<1.0 <LO
<1.0 2.4
<LO <LO
<1.0 <1.0
<LO <1.0
3500
Table 4
Groundwater Quality Summary
Upper/Lower Macon System
Macon/ Dockery Site
Richmond County North Carolina
1,1 -Dichlorocthenc Ci!.l'traru-1,2-Dichlorocthcnc Methylene chloride
(ug,L) (ug,L) (u•n)
<1.0 <1.0 <2.0
1.8 <1.0 16
<1.0 <1.0 <2.0
<l.O <LO <2.0
<1.0 <1.0 <2.0
<1.0 <LO <2.0
<l.O <1.0 <2.0
<l.O <1.0 <2.0
<LO <1.0 <2.0
<1.0 1.6 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<1.0 <1.0 <2.0
<LO <1.0 <2.0
<LO <1.0 <2.0
<1.0 <1.0 <2.0
<LO <LO <2.0
<1.0 <1.0 <2.0
<1.0 <LO <2.0
<LO <1.0 <2.0
<l.O <1.0 <2.0
<1.0 <LO <2.0
<1.0 1.8 <2.0
<1.0 <1.0 <2.0
<1.0 <l.O <2.0
<1.0 <1.0 <2.0
7 70 5
•
Tctrzchlorocthenc --(••·)
'
'
-
.•.
~1.0
<l.O
<1.0
<1.0
<1.0
<1.0•·
_<1.0
. <1.0
<1.0
<1.0
.<1.0
<1.0.
<1.0
<1.0
<1.0
<1.0
<I.0
<1.0
<1.0
<1.0
<l.0-
<1.0
:.<1.0
<r.o
<1.0
"<LO
<_l~O
<1.0"
-1
'
l,1,1-Trichlorocthmc
(~) ..
-•• -
. ,;<1.0
-:!:~}.
<l.O,"
<l.0·--
.<1.0 '.
<1.0"'.'"· . -.. ~:
~-·_5 .. ~-~---.'.
,:':1.0_ .-~r.
~<1.0~ .
<1.0
<1.0
<1.0
<l.9
<1.0
_<LO
«:-"1.0
·•<1.0
. <1.0
<i.o
,. ~1.0 ....... ·-
'_ .. ~:-<_'.~~;'
-:~~:; __ :~>7~}~/~. !4.,
'
.... ;~ ~l~tif 1;,li~;··
Sample Date TrichlOll)Cthylcnc Toluene
Location (us,/L) (ug/L)
UM Influent 2121/96 11 13
2/22/96 12 16
2/22/96 12 IS
2/23/96 12 12
2/24/96 14 9.7
2/25196 IS 9.2
2/28/96 14 2.9
3/8/96 12 <1.0
3/16/96 12 <LO
4/3/96 10 <1.0
615196 9.8 3.2
7/1196 7.6 <1.0
7(30196 9.8 <1.0
un/96 8.3 <1.0
114191 8.2 <1.0
5/11197 4.1 <LO
Sn/97 8.1 <1.0
LM Influent 2/21/96 2.2 9.3
2/22/96 3.2 12
2/22/96 3.3 IS
2/23/96 3.6 18
2/24/96 4.5 17
2/25/96 4.4 IS
2/28/96 4 4.2
3/8/96 1.1 <1.0
3/16196 1.4 <1.0
4/3/96 4.7 <1.0
5/3/96 4.6 <1.0
615196 4.9 4.6
7(30/96 4.1 <1.0
I tn/96 4.5 <1.0
114191 3.7 <1.0
(DUP) 114191 3.1 <1.0
5/12197 8.3 <LO
sn191 3.3 <1.0
Remed1allon Performance Standard 2.8 1000
DUP · duplicate
NA= Not Analyzed
• ,_
Chromium
(ug/L)
<IO
<10
<10
<10
<10
<IO
<10
<10
<10
<10
<10
<10
<10
<10
<IO
<IO
<10
<IO
<IO
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<IO
<10
<10
<10
<IO
so
Table 4 (Continued)
Groundwater Quality Summary
Upper/Lower Macon System
Macon/Dockery Site
Richmond County, North Carolina
Barium M.angancsc Zmc
(ug/L) (uon ) (uon)
<SO 58 140
<SO 39 130
<SO 36 120
<SO 31 110
<SO 30 110
<SO 28 110
<SO 18 40
<SO 13 50
<SO 20 so
<SO 9.3 26
<SO <5.0 22
<SO <5.0 <20
<SO <5.0 <20
<SO <5.0 <20
36 <S.O <20
<SO 12 <20
<SO 7.2 <20
68 110 120
70 120 120
77 130 120
81 140 130
86 160 160
86 160 160
100 ISO 240
<50 72 52
<SO 53 57
<50 72 44
24 31 27
<SO 21 24
<SO 20 <20
<SO 6.4 <20
34 19 <20
34 16 <20
<SO <5.0 <20
<SO <5.0 <20
1000 so 5000
•
-Lead Su,pcndcd Solid,
(us,/L) -(m,/1) +
13 12.
7.2 ·1
4.8 <5.0
4.5 <5.0
3.6 <5.0
3.4 <5.0
<3.0 <5.0
<3.0 <S.O
<3.0 <S.O
3 10
<3.0 13
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 NA
5.1 IS
5.6 5
5.5 <5.0
5 <5.0
4.4 <5.0
3.2 <5.0
3.3 <5.0
<3.0 7
<3.0 <5.0
<3.0 7
<3.0 <5.0
<3.0 5
<3.0 6
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 NA
IS
•
Sample Date
Location
UIL Effiuent 2/21/96
1121J96
1121J96
2/23/96
1124196
2/25/96
1128/96
3/8196
3/16/96
413196
5(3/96
6/5196
7/1/96
7/30/96
9/4196
10/1/96
Iln/96
1215196
1/6/97
2/4/97
3/12197
4/8/97
5/11197
6/6/97
7/7J97
7(25197
Sn/97
915191
Remed1alion Performance Standard
Note: 7125/97 Sampled for Ma.ngane~ only.
DUP -duplicate:
NA= Not Analyzed
Trichlorocthylcnc Toluene
(ug'L) (ug'L)
<1.0 <l.0
<1.0 <1.0
<LO <l.0
<1.0 <I.O
<I.0 <I.0
<1.0 <1.0
<1.0 <l.0
<1.0 <l.0
<1.0 <1.0
1.9 <l.O
<1.0 <I.0
<1.0 2.1
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<LO <1.0
<LO <1.0
<1.0 <1.0
<l.0 <LO
<l.0 <LO
<LO <LO
<LO <1.0
<LO <1.0
<LO <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <LO
<1.0 <1.0
2.8 1000
Chromium
(ug'L)
<10
130
<10
<IQ
<IQ
<10
<10
<10
<IQ
<IQ
<10
<10
<10
<10
<10
<10
<10
<IQ
<10
<IQ
<10
<10
<10
<10
<10
<10
<10
<IQ
50
Table 4 (Continued)
Groundwater Quality Summary
Upper/Lower Macon Syst~m
Macon/Dockery Site
Richmond Cowity North Carolina ' Barium Manganese Zinc
(ug'L) (ug'L) (ug/I..,)
59 100 98
70 120 120
72 120 120
80 140 130
83 150 150
90 160 170
<50 32 59
<50 39 56
<50 31 SI
<50 44 54
31 IQ 21
<50 1.5 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
<50 <5.0 <20
39 <5.0 <20
<50 <5.0 <20
200 30 <20
<50 <5.0 <20
<50 <~i.0 <20
<50 79 <20
<50 36 <20
<50 5.4 <20
<50 <5.0 <20
1000 50 5000
•
Lad Suspended Solids
(uo/J.) {m•fl)
4 <5.0
5.2 <5.0
5.7 <5.0
4.9 <5.0
3.7 <5.0
3.6 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
3.6 10
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 24
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 8
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
<3.0 <5.0
3.1 NS
3.1 NS
15
•
•
•
Date
2/21/96
2/22/96
2/22/96
2/23/96
2/24/96
2/25/96
2/28/96
3/8/96
3/16/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
11/7/96
12/5/96
l/6/97
2/4/97
3/12/97
4/8/97
5/12/97
6/6/97
6/23/97
7/2/97
7/25/97
8/7/97
9/5/97
NS = Not Sampled
Table 5
MANGANESE CONCENTRATIONS
Macon Dockery Site
Rockingham, North Carolina
(all concentrations are in ug/L)
UM Influent LM Influent Midfluent
58 110 NS
39 120 NS
36 130 NS
31 140 NS
30 160 NS
28 160 NS
18 150 NS
13 72 NS
20 53 NS
9.3 72 NS
<5.0 <5.0 NS
<5.0 31 NS
<5.0 21 NS
<5.0 20 NS
NS NS NS
NS NS NS
<5.0 6.4 NS
NS NS NS
NS NS NS
<5.0 19 NS
NS NS NS
NS NS NS
12 <5.0 30
NS NS NS
5.7 .5.7 <5.0
NS NS NS
47 47 86
7.2 <5.0 8.2
<5 <5 15
Bold = Concentration greater than standard
italics = sample collected from airstripper sump port.
U/L Effluent '
100
120
120
140
150
160
32
39
31
44
NS
IO
7.5
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
30
<5.0
<5.0
NS
79
36
5.4
<5
•
•
•
\
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 4
61 Forsyth Street, S.W.
Atlanta, Georgia 30303-3104
4WD-NSMB
Technical Committee
c/o David L. Jones
Ingersoll-Rand Company
114 Spencer Rd
Cassopolis, Ml 49031
SUBJ: Macon/Dockery NPL Site
Cordova, North Carolina
Dear Mr. Jones:
September 17, 1997
RECEIVED
SEP 2 21997
SUPERFUND SECTIO~I
Attached are comments on monthly progress reports and the annual summary status report. These comments were received from the NC DEHNR. Please prepare a · response to these comments and submit them to the Agency no later than October 10, 1997. Please be mindful of these comments when submitting the next monthly progress report.
If you have any questions, please give me·a call at 404/562-8824.
cc: David Mattison, NCDEHNR
Norma Eichlin, COM
Steve lrminger, AES
Since
Gi elle . Bennett
Remedial Project Manager
L
•
•
•
• State of North Carolina
Department of Environment,
Health, and Natural Resources
Division of Waste Management
James B. Hunt, Jr., Governor
Wayne McDevill, Secretary
William L. Meyer, Director
September 19, 1997
Ms. Giezelle Bennett
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
61 Forsyth Street, I Ith Floor
Atlanta, Georgia 30303
RE: August 1997 Monthly Progress and O&M Report
Macon/Dockery NPL Site
Cordova, Richmond County
Dear Ms. Bennett:
The Superfund Section of the North Carolina Department of Environment and Natural Resources
(NC DENR) has received and reviewed the August 1997 Monthly Progress and O&M Report for
the Macon/Dockery National Priority List (NPL) Site. The Superfund Section offers the attached
comments.
The Superfund Section of the NC DENR appreciates the opportunity to comment on this
document. If you have any questions or comments, please feel free to call me at [phone],
extension 349.
Attachment
P.O. Box 29603, Raleigh, North Carolina 27611-9603
Sincerely,
1}JEI(~;,;~~
David B. Mattison, CHMM
Environmental Engineer
NC Superfund Section
Telephone [phone] FAX [phone]
An Equal Oppor1unlty Aff1rmollvo Action Employer $o,I, Recycled / 1 Cl';\ Posl-Consumer Paper
•
•
•
Comments
Page I
•
Monthly Progress and O&M Report
August 1997
Results of Sampling and Testing and Other Data Received
•
I. The fourth item of this section indicates that the Lower Dockery groundwater treatment
system was operational 96% of the time. However, the third item in the section entitled
Problems and Delays indicates that the Lower Dockery groundwater treatment system
was operational 94% of the time. Please clarify this discrepancy.
Table 2 Groundwater Quality Summary
2. Table 2 indicates that the Lower Dockery groundwater treatment system effluent was not
sampled during the August sampling event. The Superfund Section recognizes that the
Lower Dockery groundwater treatment system was down for repairs August 6 through
August 8 while sampling events were occurring on August 5 through August 7.
However, the Lower Dockery groundwater treatment system effluent must still be
sampled monthly. Please provide justification for not collecting an effluent sample to
comply with the monthly sampling of the Lower Dockery groundwater treatment system .
Table 3 Groundwater Quality Summary
3. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system influent and effluent were not sampled
and analyzed for mercury during this monitoring period. Please indicate in Table 3 that
the influent and effluent were "not analyzed" for mercury. This will avoid
unintentionally stating that groundwater samples were collected and laboratory analysis
was unable to detect mercury above the detection limits.
4. Laboratory documentation included in the Monthly Progress and O&M Report does not
include the results of the suspended solids analysis for the Upper Macon Source Area
system influent and effluent samples. However Table 3 indicates that laboratory analysis
did not detect suspended solids above detection limits. Please provide complete
documentation of the suspended solids analysis or note in Table 3 that the samples were
"not analyzed" for suspended solids. This will avoid unintentionally stating that influent
and effluent samples were collected and laboratory analysis was unable to detect
suspended solids above the detection limits .
•
•
•
• •
Comments
Page 2
5. Although no mention of system performance was provided in the text, Table 3 indicates
that the Upper Macon Source Area system effluent exceeded the performance standard
concentration for manganese in August 1997. The Superfund Section recognizes that the
March 28, 1995 letter from Ms. Giezelle Bennett to Mr. Kenny Gulledge provides for the
discharge of treated groundwater to the onsite infiltration gallery without treating for
manganese. However, this report should be revised to reflect the manganese exceedance
as well as the discharge requirements of the NC DENR Division of Water Quality.
Table 4 Groundwater Quality Summary
6. Laboratory documentation included in the Monthly Progress and O&M Report does not
include the results of the suspended solids analysis for the Upper Macon system influent,
the Lower Macon system influent and the Upper/Lower Macon system effluent samples.
However Table 4 indicates that laboratory analysis did not detect suspended solids above
detection limits. Please provide complete documentation of the suspended solids analysis
or note in Table 4 that the samples were "not analyzed" for suspended solids. This will
avoid unintentionally stating that influent and effluent samples were collected and
laboratory analysis was unable to detect suspended solids above the detection limits .
Table 5 Groundwater Quality Summary
7. This section states that the monitoring well MW 7 13 sampling event yielded a cis/trans-
1,2-dichloroethene concentration of2.2 micrograms/liter (µg/L). However, the
laboratory documentation indicates that monitoring well MW-13 contained no detectable
cis/trans-1,2-dichloroethene concentrations above 2 µg/L. Please clarify this discrepancy.
8. Laboratory documentation included in the Monthly Progress and O&M Report does not
include the results of the ethylbenzene analysis for any of the monitoring well samples.
However Table 5 indicates that laboratory analysis did not detect ethylbenzene above
detection limits. Please provide complete documentation of the ethylbenzene analysis or
note in Table 5 that the samples were "not analyzed" for ethylbenzene. This will avoid
unintentionally stating that monitoring well samples were collected and laboratory
analysis was unable to detect ethylbenzene above the detection limits .
•
•
• •
Comments
Page 3
9. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, no monitoring wells were sampled and analyzed for cyanide during this
monitoring period. Additionally, monitoring wells MW-2A, MW-9, MW-I I, MW-16,
MW-21, MW-22, MW-24 and MW-25 were not sampled and analyzed for mercury
during this monitoring period. Please indicate in Table 5 that the samples were "not
analyzed" for those constituents: This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect those constituents
above the detection limits.
Table 6 Air Quality Summary
I 0. Provide a justification for not conducting air sampling at the Lower Dockery air stack.
Provide a timeframe for completing this portion of the quarterly air sampling event.
Laboratory Analytical Results
11. The laboratory documentation indicates that two additional samples (LD and LIU Macon)
were collected and analyzed for manganese. However there is no indication where these
samples originated. Please provide details as to where these groundwater samples were
collected.
12. The laboratory documentation indicates that duplicate samples (DUP-1 and DUP-2) were
collected on August 5 and August 6, respectively. However, there is no indication where
these samples originated. Please provide details as to where these duplicate groundwater
samples were collected. Although the groundwater sampling personnel may not indicate
on the chain of custody documentation where the duplicate samples originated,
groundwater sampling records should be maintained to document duplicate sampling
activities.
13. The cleanup concentrations are less than 10 µ,g/L for many contaminants of concern at
this site. Therefore, to make any assumptions regarding achieving the groundwater
cleanup standards, laboratory analysis of groundwater samples at quantitative levels
beneath the groundwater cleanup criteria must be made. Separate laboratory runs for
the various compounds may be required so that contract laboratory program detection
limits are maintained for all analytes. In some cases, Table 3, Table 4 and Table 5
imply that several contaminants are no longer present when the detection limit was
increased an order of magnitude. Please make sure that all future analyses are
conducted with the appropriate detection limits .
I
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•
• State of North Carolina
Department of Environment,
Health, and Natural Resources
Division of Waste Management
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
William L. Meyer, Director
Ms. Giezelle Bennett
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
6 I Forsyth Street, I Ith Floor
Atlanta, Georgia 30303
September 8, I 997
RE: Monthly Progress and O&M Reports
March through July 1997
Macon/Dockery NPL Site
• Cordova, Richmond County
•
Dear Ms. Bennett:
The Superfund Section of the North Carolina Department of Environment, Health and Natural
Resources (NC DEHNR) has received and reviewed the Monthly Progress and O&M Reports for
March, April, May, June and July 1997 for the Macon/Dockery National Priority List (NPL) Site.
The Superfund Section offers the attached comments.
The Superfund Section of the NC DEHNR appreciates the opportunity to comment on this
document. If you have any questions or comments, please feel free to call me at (919) 733-
2801, extension 349.
Attachment
Sincerely,
J)JZI/JL:e~~
David B. Mattison, CHMM
Environmental Engineer
NC Superfund Section
P.O. Box 29603, Raleigh. North Carolina 27611-9603 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmollvo Action Employer 5°" R&eycled / 10,. Post-Consumer Poper
•
•
•
•
Comments
Page I
Monthly Progress and O&M Report
March 1997
Table 3 Groundwater Quality Survey
I. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system effluent was not sampled and analyzed
for mercury during this monitoring period. Please indicate in Table 3 that the effluent
was "not analyzed" for mercury. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect mercury above the
detection limits.
Monthly Progress and O&M Report
April 1997
Problems and Delays
2. Please correct the spelling of "water" in the second item of this section .
Table 3 Groundwater Quality Survey
3. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system effluent was not sampled and analyzed
for mercury during this monitoring period. Please indicate in Table 3 that the effluent
was "not analyzed" for mercury. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect mercury above the
detection limits.
Monthly Progress and O&M Report
May 1997
Table 3 Groundwater Quality Summary
4. Although no mention of system performance was provided in the text, Table 3 indicates
that the Upper Macon Source Area system effluent exceeded the performance standard
concentration for manganese in May 1997. The Superfund Section recognizes that the
March 28, I 995 letter from Ms. Giezelle Bennett to Mr. Kenny Gulledge provides for the
discharge of treated groundwater to the onsite infiltration gallery without treating for
manganese. However, this report should be revised to reflect the manganese exceedance
as well as the discharge requirements of the NC DEHNR Division of Water Quality.
•
•
•
•
Comments
Page 2
5. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system effluent was not sampled and analyzed
for mercury during this monitoring period. Please indicate in Table 3 that the effluent
was "not analyzed" for mercury. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect mercury above the
detection limits.
Table 5 Groundwater Quality Summary
6. The title of this table should be corrected to read "Groundwater Quality Summary."
7. Laboratory documentation included in the Monthly Progress and O&M Report does not
include the results of the ethylbenzene analysis for any of the samples collected and
analyzed. However Table 5 indicates that laboratory analysis did not detect ethylbenzene
above detection limits. Please provide complete documentation of the ethylbenzene
analysis or note in Table 5 that the samples were "not analyzed" for ethylbenzene. This
will avoid unintentionally stating that groundwater samples were collected and laboratory
analysis was unable to detect ethylbenzene above the detection limits .
8. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, no monitoring wells were sampled and analyzed for cyanide during this
monitoring period. Additionally, monitoring wells MW-2A, MW-9, MW-11, MW-16,
MW-21, MW-22, MW-24 and MW-25 were not sampled and analyzed for mercury
during this monitoring period. Please indicate in Table 5 that the samples were "not
analyzed" for those constituents. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect those constituents
above the detection limits.
Laboratory Documentation
9. The laboratory documentation indicates that a duplicate sample (DUP-2) was collected on
May 12, 1997. However, there is no indication where this sample originated. Please
provide details as to where this groundwater sample was collected. Although the
groundwater sampling personnel may not indicate on the chain of custody documentation
where the sample originated, groundwater sampling records should be maintained to
document sampling activities .
•
•
•
• •
Comments
Page 3
I 0. The laboratory documentation indicates that two additional samples (Macon MN MID
and Lo MN MID) were collected and analyzed for manganese. However there is no
indication where these samples originated. Please provide details as to where this
groundwater sample was collected.
11. The chain of custody documentation for the groundwater treatment system sampling
event was inadvertently omitted. Please correct this oversight.
Monthly Progress and O&M Report
June 1997
Table 3 Groundwater Quality Survey
12. Although no mention of system performance was provided in the text, Table 3 indicates
that the Upper Macon Source Area system effluent exceeded the performance standard
concentration for manganese in May 1997. The Superfund Section recognizes that the
March 28, 1995 letter from Ms. Giezelle Bennett to Mr. Kenny Gulledge provides for the
discharge of treated groundwater to the onsite infiltration gallery without treating for
manganese. However, this report should be revised to reflect the manganese exceedance
as well as the discharge requirements of the NC DEHNR Division of Water Quality.
13. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system effluent was not sampled and analyzed
for mercury during this monitoring period. Please indicate in Table 3 that the effluent
was "not analyzed" for mercury. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect mercury above the
detection limits.
Table 6 Air Quality Summary
14. Provide a justification for not conducting air sampling at all air stacks and along the
property line. Provide a timeframe for completing this portion of the quarterly air
sampling event. Please note that pages I, 2 and 3 of the laboratory report have been
inadvertently omitted from the June 1997 Monthly Progress and O&M Report.
Laboratory Documentation
15. The chain of custody documentation for the sampling activities was inadvertently
omitted. Please correct this oversight.
•
•
•
Comments
Page 4
•
Monthly Progress and O&M Report
July 1997
Results of Sampling and Testing and Other Data Re~eived
•
16. The first item of this section states that the Upper/Lower Macon groundwater treatment
system effluent exceeded the performance standard concentration for manganese in July,
1997. The sample which indicated a manganese exceedance was collected from the
Upper/Lower Macon remedial system on July 2, 1997. However, the following section,
Problems and Delays, states that the Upper/Lower Macon remedial system was out of
service from June 30, 1997 to July 18, 1997. Please clarify this discrepancy.
Nevertheless, the Superfund Section recognizes that the March 28, 1995 letter from Ms.
Giezelle Bennett to Mr. Kenny Gulledge provides for the discharge of treated
groundwater to the onsite infiltration gallery without treating for manganese. Please
revise this report to reflect the manganese exceedance as well as the discharge
requirements of the NC DEHNR Division of Water Quality.
17. This section states that the resampling of the Upper/Lower Macon remedial system was
conducted on July 28, 1997. The laboratory documentation states that the resampling
activities occurred on July 25, 1997. Please clarify this discrepancy .
18. This section states that the second Upper/Lower Macon system sampling event yielded an
effluent manganese concentration of 32 micrograms/liter (µg/L). However, the
laboratory documentation indicates that the Upper/Lower Macon system effluent
contained 36 µg/L manganese. Please clarify this discrepancy.
19. The mass volatile organic compound (VOC) monthly removal totals for the Lower
Dockery and Macon Source Area remedial systems are 0.56 pounds and 0.08 pounds,
respectively. Please correct these typographical errors.
Table 3 Groundwater Quality Summary
20. In accordance with the July 17, 1996 letter from Ms. Giezelle Bennett to Mr. Kenny
Gulledge, the Upper Macon Source Area system effluent was not sampled and analyzed
for mercury during this monitoring period. Please indicate in Table 3 that the effluent
was "not analyzed" for mercury. This will avoid unintentionally stating that groundwater
samples were collected and laboratory analysis was unable to detect mercury above the
detection limits .
•
•
•
Comments
Page 5
•
Table 4 Groundwater Quality Summary
•
21. The portion of Table 4 summarizing the effluent analytical results for the Upper/Lower
Macon remedial system effluent was inadvertently omitted. Please submit this
documentation.
Laboratory Analytical Results
22. Please include a readable copy of the chain of custody documentation with the respective
laboratory reports. The chain of custody documentation for the resampling of the
Upper/Lower Macon remedial system effluent was inadvertently omitted .
•
•
•
! ,,,...
MACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
MONTHLY PROGRESS AND
O&MREPORT
JULY 1997
RECEIVED
AUG 19 1997
SUPERFUND SECTION
• ;o • "
e Macon/Dockery Site
Richmond County, North Carolina
August 8, 1997
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 30365
Re: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress and O & M Report -July 1997
Dear Ms. Bennett:
Reply to: Technical Committee
c/o David L. Jones
Ingersoll-Rand Company
114 Spencer Road
Cassopolis, Michigan
Phone: 6 l 61445-885 l
Fax: [phone] l
On behalf of the Macon/Dockery Site Group ("Group"), the July 1997 Monthly Progress and O &
M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS of the
Unilateral Administrative Order ( effective date -May 30, 1992) for the Macon/Dockery Site. This
report describes activities which occurred during the month of July as part of the Remedial Action
• phase of this project.
•
PROJECT TASKS INITIATED OR COMPLETED THROUGH ,JULY 1997:
• Monthly sampling of the water effluent from the remediation systems
• Continued O & M of systems.
RESULTS OF SAMPLING AND TESTING AND OTHER DAT A RECEIVED:
• Laboratory results for July sampling of the remediation systems is included in this progress
report. Tables I to 4 summarize the analytical results for the four groundwater treatment
systems. The reported effluent concentrations are below the remediation performance
standard except for manganese in the effluent water sample collected July 2, 1997 from the
Upper/Lower Macon remedial system. The reported manganese concentration in this sample
was 79 ug/L. The manganese performance standard is 50 ug/L. The Upper/Lower Macon
system was resampled on July 28, 1997 to confirm the July 2, 1997 analytical results. The
July 28, 1997 samples were reported by the laboratory to have a manganese concentration
of 32 ug/L, which is below the performance standard .
•
•
•
Ms. Giezelle Bennett
August 8, 1997
Page No. 2
• Upper Dockery flow meter reading for July totaled 99,896 gallons. The system was
operational 100% of the time averaging 2.04 gallons per minute (GPM). Mass voe
removal was 0.06 pounds for the month and the cumulative is 7.2 pounds.
• Lower Dockery flow meter reading for July totaled 581,027 gallons. The system was
operational 96% of the time averaging 11.86 GPM. Mass voe removal was 0 .. 56 pounds
for the month and the cumulative is 5 .20 pounds.
• Macon Source Area flow meter reading for July totaled 117,736 gallons. The system was
operational 100% of the time averaging 2.40 GPM. Mass voe removal was 0 .. 08 pounds
for the month and the cumulative is 1.75 pounds.
• Upper/Lower Macon flow meter reading for July totaled 223,859 gallons. The Upper Macon
system was operational 42% of the time in July. The Lower Macon system was operational
42% of the time in July. The combined system flow averaged 4.57 GPM. Mass VOC
removal was 0.05 pounds for the month and the cumulative is 2.26 pounds.
TASKS PLANNED FOR AUGUST 1997:
• Monthly sampling of the remediation systems effluent
• Quarterly sampling of the remediation systems influent. Sampling of designated quarterly
monitor wells. Air sampling of off-gas at the remediation systems. Measurement of water
levels in the monitor and recovery wells.
• Continue O &M of systems
PROBLEMS AND DELAYS:
• June 30 to July 18, 1997 -Upper/Lower Macon System was down because of a failed transfer
pump on the effluent water line. The transfer pump was removed from the site on July 7,
1997 and delivered to the manufacturer's authorized repair facility for diagnosis and repair.
. ,
•
•
•
Ms. Giezelle Bennett
August 8, 1997
Page No. 3
The mechanical seal and labyrinth oil seals were replaced and the Upper/Lower Macon
system was restarted on July 18, 1997.
• July 8 -The Lower Dockery system was down due to a low water level alarm condition in
the equalization tank. The system was restarted on July 8, 1997. The reason for the low
water level condition is being evaluated.
• Percent operational for each system: Upper Dockery
Lower Dockery
Upper Macon
Lower Macon
Macon Source Area
SVE system
Respectfully Submitt(ld, _
-!l\--c;_ ~
~rv.
David Jones
Project Coordinator
cc: Macon/Dockery Site Group Members
Paul Furtick, RMT, Inc.
David Lown, NC Super Fund Section
100%
96%
42%
42%
100%
100%
• •
Sample Date I.I• Dichlorocthanc I.I• Dicblorocthcnc Ciil'tram-1,2-Dichlorocthcnc Tcttachloroclhene 1,1,1-Trichlorocthanc Trichlorocthvlc:nc Toluene Toi.al X}'lcncs Location ----(i;n,)--~----c'(,=,;IVII~ .. ) -='-j-~~~~(~,'IVI•· ~-~l ~=~-1-=~cc,=,,._~)=~ 1~=~,f,.':';;n~)=~ci-~=,c,.=,._-c-,=-1-(c""~"';;-',-) (u11ll )
UD Inn~~'--· 2/IJ/96:----11---'=·='------ISOE 1.3 1.3 54 8 3.1 -----2/IJ/% ---~'-~'---t---~''"'='----l---~~---+------f---'3"c3---ll---c~--f---t-----l 2/14/96 4.3 ---~""E'---l----'~-2'----l-------l---~"'---·f---'c'·~'---1----1-----1
-----11---~21cc\'.'_~ ---~-~-------l---c1c'00"=---1----~----1--~~--1---~'~'---l---c'·cc3 __ +--+----1 2/14/96 4.4 l---'1~20~E'---f---~'~-•----l---''~·'--+--~'~'---t---c'·cc• ___ 1 ____ 1-----I 2/14/96 ----··-!._·_ I to 48 7.8
2/IS/96 .U l---'~'~•=E---l----c'-~2----1---~'~-''---l---~5~4---f---~•~·',---ll-=,-t-----l 2/15/96 S.5 ___ 1~•~•---l----~----+------l---~'~''---+--~•~•:---1-~'~·8'-+----1 2/16/96 1.S 160 6-1 10 2117/96 5.7 ---,cc870E:C---t----,cc_7c----t---c,~_,,---l--~,c:2---l---c9~.4,---l---+-----I
11171% S.S 120 42 6.4 2122196 5.4 1---~IS~O"E---+----71.~,----l-------l---~,~2---l---~,~-71---11---t-----l
------n--=211=2196=--111---4·9 -----=·~•cc---+----c~----1---~--+---4~8:---+--~'~-':---1---2/28/96 6.4 200E 1.9 19 5.J 2/28196 6.8 240 50 J/S/96 S.l l---,~,~,~ •• ~,~,,--+-----cl.~J----l-------lf---~,~,---t---~
3~_,,---ll---
l------lll--'-:~=::-:--ll---33c6----1--=1~~c2cE ___ , ____ cl.~l ____ , ___ c1c•6c__-l ___ c:~:---l---~;c::---I---I-----I --------------_____ _,, __ cSc/Jc/%~--11 4 130 38 4.8 615196 110 5.2 2.8 7/1/96 2 77 2.S 3.6 ---·=---1----------e------t---~~--+--~~---1
----------H--=8=/l=/9=~--ll---~•~·~'---l---~2~2~0---l---------·l-------ll---~'=2---1----5-·7---1---1-----lln/96 --~'~•~•---t---------+------t----'~''---+------t---+----·I 11n/96
2/.S/97 100 31 1------11---c,~11",19:ci7~-11-------,---~,cc,,c_--1---------1------·1---'c-16:c---+---,=.=,--+--+----1
LID Effiuenl 2/JJ/%
2/14/96 1------11--~21=14~/%0=--ll,-------
2/I .. S/%~--ll ·------l·------I ---------1------1-------1------1---I----~ ------ll--=2116/96 -
2117/96
2/12/%
2/181%
l/81%
4/3/96
Sfl/96
6/S/% 39 7/1/96
8/1196
9W96
10/1/96
11/7/96
12/5/96 LS
1/6/9~
2/.S/97
3/12197 ---------------------+------1-------4-------1---+-----I
RcmeJiation Perfonnancc S1a11dard 3500 7 70 200 2.8 1000 400
r"==='=A='=''="'=•='="="=~=•c•-"=~="'="='""=''--11-----------/-------+----------f--------+--------+--------+---+------1
NOie: • Acc10nc coofirmed by Melhod 1160
•
Sampsl~'----11
Location
UD l111luc111
UD Effiuent
Date
2/ll/96
2/1)/96
2/14/96
2/14/96
2/14/96
2/14/96
2/15/96
2/IS/96
2/16/96 -----2/17/96
2/17/96
2122/96
2f22/96
2/28/96
2/28/96
3/8/96
4/3/96
4/3/96
S/3/96 .,,/96 -----7/1/96
811/96
11n/96
11n/%
215197
S/14/97
2/13/96
2/14/96
2/14/96
2/15196
2/16196
2/17196
2/22/96
2/28/96
3/8196
4/3/96
S/J/96
6/S/96
711/96 ---------811/96
9/4/96
I0/1/96
11n/96
1215/96
1/6197
215191
l/12197
4/8/97
S/14/97 ----------616197
1(2191
Remediation Pc1fonnancc Standard
•
I Acetone Chromium Barillm
(unll) (U"/1) (u11/L)
20 92
12 "
II "
19 81
----------II 51 -------"
13
-----II ---
II S2
" " -----
-------II
2100 19 61
1so•
12 " " 70"F32 16 71 -----3S"F33 " " II ,6
12 " " II "
13
" 28 II 50
"
-------20 14 " " -------
" 59
12 " -------13 " " 61
69
63
60 -----" ----".
3500 50 1000
• ..
Manj!:&nCS(: Zinc L<0d Susl>f'ndcd Solids
(u•II \ {uo/1 ) (unfl) (m ) .. 33 3.1 "
14 "
14
"
II
12
13
7.7
'
,., 10
9.,
,.3
40 22 14
14 II
12
14
II
12
8.3
9.6 10
6.9
'
5.9
5.1
,.9
7.2
so ,000 "
•
Sample Date Chlorofonn I, I -Dichloroethane
Location (ug/L) (ug/L)
LD Influent 2/13/96 I. I 80
2/14/96 1.3 IIOE
2/14/96 80
2/14/96 1.6 94E
2/14/96 64
2/15/96 1.2 82
2/16/96 3.3 95
2/22/96 2.5 5.8
2/28/96 1.2 93E
2/28/96 92
3/8/96 2 110
4/3/96 79
5/3/96 71
6/5/96 67
8/1/96 83
11/7/96 69
3/12/97 66
5/14/97 62
Remediation Pcrfom1ance Standard 3500
Nole: A blank means below dc1cction limit
•
I, I -Dichloroethene Cis/trans-1,2-Dichloroethene
(ug/L) (ug/L)
33
43
13
39 1.8
16 2.2.
32 I. 7
35 2.6
IO0
33
35
47
36
30 I. 7
32 I.I
27
28
21
25
7 70
Methylene chloride
(ug/L)
I. 7
2.5
2
5
•
•.
I, I, I-Trichloroethane
(ug/L)
40
37
15
39
18
29
31
54
30
30
34
28
40
42
54
38
23
23
•
Sample D
Location
LO Innucnt 2/13/96
2/14/96
2/14/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
8/1/96
lln/96
3/12/97
5/14/97
Remediation Pcrfonnance Standard
Note: A blank means below detection limit
richloroethylene
(ug/L)
6.4
8.6
9
6.6
8.4
8.7
5.2
7.4
6.4
6.7
6.6
5A
5.2
5.9
5.8
6.2
2.8
Benzene
(ug/L)
1.8
Toluene
(ug/L)
17
8.3
8.3
6.5
5.3
4.3
13
1.3
2.5
IO00
• •
I
Total Xylencs Chromium Barium Manganese Zinc Cadmium Suspended Solids 1-~=~1-~'-=-c~-1----c=~~1--=~=---1---'====='--1 (ug/L) (ug/L) (ug/L) {ug/L) (ug/L) (ug/L) (mg/L)
260 270
250 120
240 I 10
200 84
190 81
3.4 14 240 240
120 77 8
95 30
160 39
16 63 200 0.91
230 46
110 5
230
76
150
400 50 IO00 50 5000 5
• • •
Sample Date Chlorofonn I, I -Dichlorocthane I, I -Dichlorocthene Cis/lrans-1,2-Dichloroethene Methylene chloride I, 1, 1-Trichloroelhane
Location (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L)
LD Effluent 2113/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
8/1/96
10/1/96
11/7/96
12/5/96
1/6/97
3/12/97
4/8/97
5/14/97
6/6/97
7/2/97
Remediation Performance Standard 3500 7 70 5 200
Note: A blank mclllls below detection limit
• • •
Sample ~ Trichlorocthylene
Location (ug/L)
Benzene Toluene
(ug/L) (ug/L)
Total Xylenes Chromium Barium Manganese Zinc Cadmium Suspended Solids ,-~~~-,--~~~-,-~-~-,--~~~-,--~-~~--, (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (mg/L)
LD Effluent 2/13/96
2/14/96
2/14/96 II
2/15/96
2/16/96
2/22/96 5
2/28/96
3/8/96
4/3/96
5/3/96
8/1/96 13 0.56
I0/1/96 II
11/7/96 3.4
12/5/96 35 19
1/6/97 6
3/12/97 70
4/8/97
5/14/97
6/6/97
7/2/97
Remediation Perfomrnnce Standard 2.8 IO00 400 50 IO00 50 5000 5
Note: A blank means below detection limit
•
7
S_a,_n,p
7
lc ______ 11 __ D_at_e_ I Chloroform
Locution . . (ug/1.)
UMSA lnllucnt 2/13/96
2/14/96 I. I
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96 I.I
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
11/7/96
2/4/97
(DUCP)~----ll -c'c2/7.4CC/9~7~11----5/J2/97
I! I -D\chloroethane
(ug/L)
15
14
II
12
7.5
9.7
10
9.8 -7.6
5.5
4.8
8.7
3.8
7.9
7.2
3.0
2.4
3.8
4.6
•
I, I -Dichlorocthtne Cis/trans-1,2-Dichloroethene
(ug/L) (ug/L)
14 19
11 10
14 II
14 II
21 17
18 16
17 16
16 13
10 ID
16 8.5
12 6.9
22 6
II 6.9
15 10
9.2 7.5
27 7.8
25 6.2
26 16
21 16
•
Tetrachloroetht:ne I ,I, I-Trichloroethane Trichloroethylene
<•·" I (ug/L) (ug/L)
16 5.9 25
7.3 7.2 10
17 6.1 17
18 5.9 16
14 9.7 25
II 7 24
15 7.6 25
12 5.8 21
7.7 4.1 16
7.4 5.4 18
5.7 12
6 13
4.8 4.3 12
6.4 4.2 13
2.3 3.4 10
2.3 8.8 15
1.8 7.9 14
8.9 5 22
8.2 3.7 18
3500 7 70 I 200 2.8
(DlJP) 5/12/97
Remediation Pcrfonn~iiaaa==l~==?==~~~===la=====~===iaaa====a:,;;=====iaaa==~===aia===~~===al===~;;;,,==~
No1c: A blank mca.ns bclow~i
DUP -duplicalc II
• •
-1_S_a_n~ip_le ______ 11 __ D_a_le __ 1_V_iny!.£.hl~~ Benzene Toluene
Localion (ug/L) (ug/L) (ug/L)
Chromium
(ug/L)
UMSA lnfluenl 2113196 1.9
2/14/96 1.5 2/14/96 l--l----
2/15/96 I 3 --------11-----1-----1--·~-+-~--1-----1 2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96 I. I 3.6
711196 II
7/30/96 4.5
11/7/96 2
2/4/97
(DUP) 2/4/97
5/12/97
(DUP) 5/12/97
Remediation Perfonnancc Standard IO00 50
Note: A bl1111k means below detection limit
DUP · duplicate
Barium
(ug/L)
140
110
I IO
100
120
110
120
130
130
110
97
130
110
130
140
150
140
120
150
IO00
Manganese Zinc Cadmium Lead Mercury Suspended Solids
(ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (mg/L)
300 55 3.5 21
180
160 20
140
160 0.22
I IO
65
52 7
41
27 8.2
21
19 5
13 5
13 6
9.8 10
24 36
17
68
55 5
50 5000 5 15 I.I
•
• • •
-~~pie ~ Chlorofom1 I, I -Dichlorocthane I, 1 -Dichloroelhene Cis/lrans-1,2-Dichloroethene Tetrachloroelhene I, I, I-Trichloroethane Trichloroethylene -------·
Location (ug/L) (ug/1.) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L)
UMSA Enluent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
413/96
513/96
615/96
711/96
7/30/96
9/4/96
I0/1/96
lln/96
12/5/96
1/6/97
2/4/97
3112/97
418/97
5/12/97
·6/6/97
7/2/97
Remediation Pcrfonnance Standard 3500 7 70 200 2.8
Nole. A blank means below detect.ion limit
UUP · duplicate
• •
-i:S='"""''Pc;l.c.e ______ 11 __ .cDcca=te-'----l-'V-'in"'y'cl-'c"h"-lo=r-'id=1=llenzcne
Locution (ug/1.) (ug/L)
UMSA Effiucnt 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
I0/1/96
I 1/7/96
12/5/96
1/6197
2/4/97
3/12/97
4/8/97
5/12/97
616/97
7/2197
Remediation Performance Standard
Note: A blwik mC1111S below detection limit
11UP • duplicate
Toluene
(ug/L)
2.9
1000
Chromium Barium Manganese Zinc Cadmium Lead Mercury Suspended Solids (ug/L) ~(~ug/•'c1=,)~1~{=ug/"""L)=i--c{u=g/Lc'c-)+=c{~ug/L=)-'-l-{o-'u~g/L,_)c-J-'-,{u~,.c:n_7)01 -=c,{~m~g/L,_)c'-~I
16 150 330
I IO 190
110 160
IO0 140
130 170
120 120
120 70
130 51
120 37
110 27
120 26
130 22
12 110 14
200 110
II · 110 68
130 13
140 13
170 17
200 46
1600 29
130 30
200 30
12 210 95
240 74
·180 41,
50 1000 50
74
20
41
26
25
35
5000
0.47
5
4.2
9.2
66
3.5
15
57
0.26 18
5
6
23
16
24
26
5
120
8
7
IO0
I.I
•
• • •
S11J1plc
Location
Chlorofo,m Toluene
{u {u ~}
1,1. Dichlorocth.&nc I, I -Dichlorocthenc Ci,luans-1, 2-Diehlorocthenc Mcthvlcnc chloride T euachlorocthc:nc I, l,l•Trichloroethanc Trichloroeth• lcnc
(ug/1 ) (uu/1) (u-") ,, ) ,, ) ,, (u·")
UM Jnflm:nt 2121/96 16 IJ )_I LI 4.6 ◄6 II
l--------1-=212=219c6+--1c;0~-l---"c"---l,---"'"---l----"'"----l-------l------''7---l-------l---"---+-1~6~-I 2f21196 6 IS
).9 u 5 5 52 12
4.1 1.6 5' .. 12
2/23196 12 4 5 1.6 64 48 12
2/2.i/96 1.4 9.7 46 18 64 • 14
2/25196 1.2 9,2 22 66 69 15
2/2&/96 3.S 2.9 ,. 1.4 8.6 5 14
J/81%
J/16/96
4D/%
4.7
5 5
44
I
'' 1.6
8.6 ,., 12
9.2 46 12
66 10
6/S/96 l.2 l-------l--';71"1,,."--l-----l-----'~---l----""---l-----"'----ll------+--~---1-------1----"''--+---'"'---I ,_9 LB 7_7 '·' ,.. LI 6.1 l.l 7_6
LM Influent
7(30/96
\ln/96
2/4197
4.1
51
5 5
II
15
2.1
L9
1.6
25
5_5
86 l l ,_,
66 21 ,_,
25 8.2
LB 4 5 ,_1
21 LI 7_6 22
2122/% 15 12 22 84 l l 1.7 II l.2
2/22/96 14 IS 26 9.1 44 2 14 l.l
2121/96 13 IS 29 II 4.9 2.1 15 l 6
2/24196 8.9 17 ]O I] ,.9 2.7 17 " 2/25/96 8.2 15 ]I I] 5 26 17 ,,
l--------11-=212c8~19~6~1--~--ll---'-c----l----''-c----l-----c"'----+-------l-----"'-----l----'-'c---l----,C'-----l--'4~2-I J/8/96
l2 15 56 2.4 17 4
95 1.6 2A 2 5 LI
(DUP)
)/16196
5n/96
615/96
7/30/96
lln/96
2/4/97
214/97
S/12/97
Rcmi:diation Performance Standard
Nu1e, A blln.l. ,nun• b<kM ddeclion limil
l)llP • dupliulo I
16
u
8.1 1.8
7 l 2.6
" 27
12 ,_1
17 66
II l l
9B 2.1
90 LB
5 l " )500 7
24 l 4 L4
21 4 ,_1
2.9 ,.2 4.6
14 5 l 4_9 46
67 ,_1
22 5 2 '5
" 4.4 l 7
2.1 l B l.l
6A • l
70 200 ,. 1000
•
•
•
', .
•
•
•
,,
SL SAVANNAH LABORATORIES
. & ENVIRONME.NTAL. SERVICES, INC.
lU 917047957076 P.02
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Eanh sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-73744
Received: 03 J1:7L 97
Reported: 15 JUL 97
Client PO. No.: 190-00001-0l
Project: 190-00001·01/MACON DOCKERY
Sampled By: Client
Code: 095870716
l!l!PORT OF RESULTS Page l
LOG NO
73744·1
73744-2
73744•3
73744·4
SAMPLE DESCRIPTION , LIQUJ'.D SAMPLES
Macon system Eff.
Macon Source Eff
Lower Dockary Eff
Opper Dockery Eff
PARAMETER
Purgeable Halocarbons (8010)
Clllorofom. ug/1
l,l-Oichloroethane, ug/1
l,l·Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/l
Methylene chloride (Dichloromethane),
Tetrachloroethene, ug/1
1,1,l•Trichloroethane, ug/1
Trichloroethylene. ug/1
Vinyl chlori<1e, ug/1
Surrogate • Bromochloromethane
Date Analyzed
Oilueioo tac-:or
Batch ID
Clock IO
73744-l
cl.O
2.4
<l.0
l. 8
ug/l <2.0
<l,0
<l.O
<1.0
<1.0
110\-
07.08.97
1.0
0707A
l.80708
73744·2
<1.0
<l.0
<l.0
<1.0
<2 .o
<l.0
<l.O
<1.0
<1.0
78 t
07.08.97
1.0
0707A
180708
DA'tt/
TIMI! SAMPLED
07-02•97/lllS
07-02-97/1130
07-02-97/1205
07-02-97/1150
73744•3
<l.0
<1.0
<l.O
<l,0
<2~0
<l.0
<tl.O
<l.0
<1.0
77 1
07.08.97
1.0
0707A
1130708
7)744-4
<l.0
<1.0
<l.0
<1.0
<2.0
<1.0
<1.0
<1.0
<l.0
79 \-
07.08.97
l.0
0707A
180708
Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
••
•
IU 917047957076 P.03
' SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SDIVICES, INC.
5102 LaROChe Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irmingar
Applied Ear1:h Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7•73744
Received: 03 JUL 97
Reported: 15 JUL 97
Client PO. No.: 190·00001·01
Project: l90·00001·01M(:Ol'I DOCKERY
Sampled By: Client
Code: 095870716
LOG NO
REPORT OIi' RESULTS
SAMPLE DESCRIPTION, LIQOID SAMPLSS
Page 2
DATE/
TIME SAMPLED
73744·1
737'11 •2
73744·3
73744•4
PARAMETER
Macon System l!ff.
Macon Source Eff
Lower Dockery Eff
Upper Dockery Eff
Purgea.ble Aromatics (8020)
Ben,:ene, ug/l
Toluene , ug /1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate· a,a,a-Trifluoroeoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Suspended Solids; (160.2)
suspended Solids (160.2), mg/1
Preparaciott oat.e:
Date Analyzed
Dilution factor
Batch IO
!!arium (6010)
Barium 16010), ug/l
?reparation Cate
Date Analyzed
Dilution factor
Bat.eh ID
73744-1
<l.0
<1.0
<3.0
<10
103 \-
07.08.97
1.0
0707A
180708
<5. 0
07.03.97
07.04.97
1.0
0703C
<50
07.07.97
07.08.97
1.0
07078
73744·2
<l.O
<1.0
<3. 0
<10
100 t
07.08.97
1.0
0707A
180708
<5.0
07.03.97
07.04.97
1.0
0703C
180
07.07.97
07.08.97
1.0
07078
07·02-97/1115
07·02·97/ll30
07·02-97/1205
07·02-97/1150
73744·3
<l.O
<1.0
<3 .o
<10
103 t
07.08.97
1.0
0707A
180708
<5.0
07.03.97
07.04.97
1.0
0703C
<50
07.07.97
07.08.97
1.0
0707B
73 744 •-1
<l.0
<1.0
<J.0
<10
107 \-
07.08.97
l. 0
0707A
180708
<5.0
07.03.97
07.04.97
1.0
0703C
55
07.07.97
07.08.97
1.0
07078
Laboratories In Sannnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orl1111ns, LA
•
•
•
IU
S' L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Sarr.h Sci,.nces
751 Arbor Street
Concord, NC 28025
LOO NO: S7-73744
Received: 03 JUL 97
Reported: 15 JUL 97
Client PO. No.: 190-00001-0l
Projact: l90-0000l-Ol/MACON DOCKERY
Sampled By: Client
Cod!O: 095870716
REPORT OF RESULTS Page 3
DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SJIMPLES TIME SJ\MPLE.t>
737U-l
73744-~
73744-3
7374' ·4
PARAMSTER
Macon System Sff.
Macon Source Iliff
Lower Dockery Ett
Upper Dockery Eff
Berylliuin (6010)
Beryllium (6010), ug/l
Preparation Dat:e
Date Analy,ed
Dilution factor
Batch ID
Cadmium (7131)
Cadmium (7131), ug/1
Preparation Date
Date Analy:oed
Dilution fa.ct.or
Batch ID
Chromium (6010)
ChraniUl!I (6010), ug/1
Prepfi:::ation Date
Date Analyied
Dilution factor
Batch ID
,. _________
····------
73744-l -----·----
<S.O
07.07.97
07.08.97
l.O
0707B
<0.30
07.07.97
07.08.97
l.O
0707F
<10
07.07.97
07.08.97
l.O
0707B ----------
73744•2 ·---------
<5.0
07.07.97
07.08.97
l.O
0707B
<0.30
07.07.97
07.08.97
l.0
0707F
<10
07.07.97
07.08.97
l.O
07078 -------·--
07-02-97/1115
07-02-97/1130
07-02-97/1205
07-02-97/1150
73744-3 73744-4 _____ ,. ____ ............
<5.0 <5.0
07.07.97 07.07.97
07.08.97 07.08.97
l.O l.0
0707B 07078
<0.30 <0.30
07.07.97 07.07.37
07.08.97 07.08.97
1.0 l.0
0707P 0707F
<10 <10
07.07.97 07.07.97
07.08.97 07.08.97
l.O l.O
0707B 07078 -----------····-----
Laboratorlos In S..vannal,, GA • Tal/111tes&ec, FL • Tempo, FL • Oeerfletd Beach, FL • Mobile, AL • New OrleanB, LA
•
•
TU ~17047'357075 P.05
SL SAVANNAH LABORATORIES
. & ENVIRONMENTAL SERVICES, INC. ·
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone] ·
Mr. Stave Irm.inger
Applied Earth Sciences
751 Arbor Streee
Concord, NC 28025
1,0G NO: S7·73744
Received: 03 JUL 97
Reported: 15 JOL 97
Client PO. No.: 190-00001-0l
Project: 190·00001-0l~CON DOCKERY
Sampled By: Client
Code: 095870716
REPORT OF RESULTS Page 4
DATi/ LOG NO SAMPLE DESCRIPTION, LIQUID SJ\MPLES TIME SAMPLED
73744-l
73744-2
73744-3
73744·4
PARAMETER
Macon SyQcem Eff.
Macon Source Sff
Lower Ooelcery &:ff
Uppar oockary Eff
Manganese (6010)
Manganese {6010), ug/l
Preparaeion Date
Date Analyzed
Dilution fact:.or
Batch IO
Ni.ck@l {6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilut:ion fact.OX'
Baech ID
73744·1 ----............ ......... ____
7'
07.07.97
07.08.37
l.O
07078
dO
07.07.97
07.08.97
l.O
0707B
<3:o
07.07.97
07.08.97
l.O
0707F --------------------
73744•2
-.... -.... ----
4l
07.07.97
07.08.97
l.0
07078
<40
07.07.97
07.08.97
1.0
07078
<3.0
07.07.97
07.08.97
l.0
0707F
-------···
07-02-97 /1115
07-02-97/l.130
07•02-97/1205
07•02-97/1150
73744•3 73744-4 ····--------···-----
<5.0 <5.0
07.07.97 07.07.97
07.08.97 07.08.97
1.0 l. 0
07078 07078
<40 <40
07.07.97 07.07.97
07.08.97 07.08.97
l.O l.0
0707B 07078
<3. 0 d.O
07.07.97 07.07.97
07.08.97 07.08.97
1.0 l. 0
0707F 0707F -----····-..............
• u,boratorles In Sa'lllnnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
. JU... -l b-l :J:J? l 2: 4::> ~ ROM 5/:<VANNAH LHBS TO 917047957076 P.06
S' L SAVANNAH LABORATORIES
& l!.NVIRONMENTAL SERVICES, INC.
5102 LaRodie Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irmingar
Applied Earth Sciencaa
751 Arbor Street
Concord, NC 28025
LOG NO: S7•73744
Received: 03 JOI. 97
Reported: 15 JUL 97
Client PO. No.: 190•00001•01
Project: 190•00001·01/lal.CON DOCKERY
Sampled _By: Client
Code: 095870716 REPORTOF RESULTS Page 5
DATE/ LOG NO
737H·l
737.44 ·2
73 7U • 3
73744·4
SAMPLE DESCRIPTION, LIQUID SAMPLES
Macon System F.ff.
TIME SAMPLED
07•02-97/lllS
07-02-97/1130
07•02-97/1205
07-02·97/llS0
Macon Source Eff
Lower Dockery F.ff
Upper Dockexy F.ff
PARAMETER 73744-1 7374,-2 7374,-3 73744.4
Ant.imony (7041)
Antimony (7041), ug/l <10. <10 <10 <10 Pr6i!paration Dace 07.08.97 07.08.97 07.08.97 07,08.97 Date Analyzed 07.09.97 07,09,97 07.09.97 07.09.97 Dilution factor 1.0 1.0 l.0 l.0 Batch ID 07081C 07081C 07081C 0708K vanadium 16010)
Vanadium (6010), ug/1 <50 <~0 <50 <50 Preparaeion Date 07.07.97 07.07.97 07.07.97 07.07.97 Date ..nalyzed 07.08.97 07.08.97 07.08.97 07.08.97 Dilution factor l.0 l.0 l.0 l.0 Batch ID 07078 0707B 07078 07078 Zinc (6010)
Zinc (6010), ug/l <20 <20 <20 <20 Preparation Date 07.07.37 07.07.97 07.07.97 07.07.97 Date Analyzed 0.7.08.97 07.08.97 07.08.97 07.08.97 Oilut.ioo factor 1,0 l.0 1.0 1.0 Batch ID 07078 0707B 07078 07078 ------------·-------··----•·"' ------------·-------.. -. ----... -------··· -----•----
l.al)oratorl11s In Savannafl, GA • Ta//allassee, FL • Tampa, FL • Oeerlield Beecll, FL • Mobile, AL • New Orl1111ns, LA
•
•
IU
' SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaAOChe Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Stave Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-7J744
R.eceived, 03 Jt1L 97
Reported: 1S JT]L 97
Client PO. No.: 190·00001-01
Project: 190-00001·01/MACON DOCKIIRY
Sampled By: ·client
Cod'": 095870716 REPORT OF RESULTS Page 6
LOG NO SAMPLJ:: DESCRinION, LIQUID SAMPLES DATE SAMPLED
73744·5 Trip Blank 07•02-97
PARAMETER
Purgeable Halocarbons (8010)
Chloroform, ug/1
l,l·Dichloroethane, ug/1
l,1-Dichloroechene, ug/1
Cis/Trans·l,2•Dichloroethene, ug/1
Methylene chloride (Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1.l-Trichloroethane, ug/1
Trichloro,,thylene, ug/l
Vinyl chloride, ug/l
Surrogate· Bromoch.l.oromethane
Date Analy•ed
Oilution factor
Bacch ID
Clock ID
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/l
Acetone, ug/1
Surrogate -a,a,a-Tritluorotoluene
Date Analy,ed
Dilution factor
Batch ID
Cloe>< ID
73744•5
<1.0
<1.0
<1.0
<l.O
<2.0
<1.0
<1.0
<l ,0
<LO
79 ~
07.09.97
1.0
0707A
1B0708
<l,0
<l.0
<3.0
<lO
103 t
07.08.97
1.0
0707A
180708
Laboratories In Sa"31Jnah. GA • Ta/lahasme, FL • Tempo, Fl. • Oeerlield Beach, fL • MoOl/e, AL • New Orteans, LA
•
•
•
S. L SAVANNAH LABORATORIES
& ENIIIRONMENTAL SERVICES, INC.
IU r-.~o
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
concord. NC 28025
LOG NO: S7·73744
Received: 03 JOL 97
Reported: 15 JUL 97
Client PO. No.: 190•00001•01
Pro;ect: 190·00001·01/MACON DOCKERY
Sampled By: Client
Code: 095870716
REPORT or RESULTS Page 7
LOG NO
73744 · 6
737H •7
737H-8
73744•9
73744·10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLSS
Practical Quantitation Limits
Method Blank
Lab Control Standard Result
LCS Expected Value
Lab Control Standard t Recovery
PARAMSTER 73744-6 73744•7 73744·8 73744·9 73744·10
Purgea.ble Halocarbons (8010)
Chloroform. ug/1 1.0
l,l•Dichloroethane, ug/1 1.0
1,1-Dichloroethene, ug/1 l.0
Cis/Trans-1,2-Dichloroethane, ug/1 1,0
Methylene chloride 2.0
(Dichloromethane), ug/1
Tetrachloroethene, ug/1 1.0
1,1,l·Trichloroethane, ug/1 1.0
Trichloroethylene, ug/l l.0
Vinyl chloride, ug/l 1.0
Surrogate• Bromochloromethana
Date Analyaed.
Dilueion :factor
Batch ID
Clock ID
<1.0
<l.O
<1.0
<l.0
<2.0
<1.0
<l.O
<l.0
<l.O
78· t
07.0B.n
1.0
0707A
150708
25 20 l25lr
24 20 120 t
BO t
07.08.97
l.0
0707A
180708
-.... -----••'"'----··· ----····--
laboratories In Satiannah, GA • Tallahassee, FL • Tampa, FL • Dttrlleld Beach, FL • MoOilo, AL • New Orleans, LA
•
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL. SVfVICES, INC.
IU
5102 LaRoche AV11nue • Savannah, GA 31404 • (912) 354•7858 • Fax [phone]
LOG NO
Mr. Steve Irminger
.Applied Earth Sciences
751 Arbor Street
Concord, NC 280~5
LOG NO: S7·73744
Received: 03 JUL 97
Reported: 15 JUL 97
Client PO. No.: 190·00001·01
Project: 190-00001·01/MACON DOCKSRY
Sa111pled By: Client
Code: 095870716
REPORT OF RESULTS Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ·-----···---------------------··---------------------------·-----------------------73744•6
73744-7
73744•8
73744·9
73744•10
Practical Quantication Lunits
Method Blanlc:
Lab Control Standard Result
LCS Expected Value
Lab Control Standard% Recovery ------------------------------····---------------------------------------............ . PARAMETER 73744·6 · 73744-7 73744-8 73744•9 73744-10
Barium (6010)
Bariu.~ (6010), ug/l
Preparation Date
Date Analyzed
Dilution fa.ctor
Batch ID
Beryllium (6010)
Beryllium (6010), ug/l
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmil.llU (7131)
Cadmium (7131), ug/l
Preparaeion Date
Date Analyz<ld
Dilution faceor
Batch ID
so
5.0
0 .30
-::SO
07.07.97
07.08.!17
1.0
07078
<5.0
07.07.97
07.08.97
l.O
0707B
<0.30
07.07.97
07.08.97
l.0
0707F ----------
2040 2000 102 t
07.07.97
07.08.97
l.O
07078
t9.4 50.0
07.07.97
07.08.97
1.0
07075
5 .17 5.00 103 t
07.07.97
07.08.!17
1.0
0707F
-------···
Laboratories In Savannah, GA • Tallahassee, FL. • Tampa, FL • Deerfield Beach, FL. • Mobile, AL. • New 0;1e11na, LA
IU 1-'.lll
t j ' I
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord. NC 28025
LOG NO: S7•73744
Received: 03 JUL 97
Reported: is JUL 97
Client PO. No.: l90·0000l-Ol
Pro;act: 190-00001-0l/W.CON DOCKERY
Sa,opled By: Client
Code: 095870716
REPORT OF RBSULTS Page 10
LOG NO
73744-6
73744•7
73744-8
73744-9
73744 •lO
SAMPLE DESCRIPTION, QC.REPORT FOR LIQUID SAMPLES
Practical Quaneitation Limits
Method Blank
La.b control Standard Result
LCS Expected Value
Lab Control Standard t RecOV9ry
P~R 73744-6 73744•7 73744·8 73744-9 73744·10
Chromium (6010)
Chromium (6010). ug/l 10 <lO 210 200 105 \-Preparation Date 07.07.97 07.07.97
Data Analyzed 07.08.97 07.08.97
Dilution tact:or l.O l.O
Batch IO 070713 070713
Manga.."1.ese (6010)
Manganese (6010), ug/l s.o <5.0 Sl3 500 103 \-rreparation Date 07.07.97 07.07.97
Date Analyzed 07.08.97 07.08.97
Dilution !actor 1.0 1.0
Bat.ch ID 0707B 07078 Nickel (6010)
Nickel ( 6010) , ug/1 40 <40 521 500 104 \-Preparation Date 07.07.97 07.07.97
Date Analyzecl 07.08.97 07.08.97
Dilution factor l.0 1.0
Batch ID 07078 070711 --·----------·-------··-·----................... . .. . -. ---------.. ---..
Laboratories in SaYannah, GA • Tallahassee, FL •. Tampa, FL • D~rlleid Beach. FL • Mobile, AL • New Orleans, LA
•
S.' L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC. ··
IU ,., . .11
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: 57-73744
Received: 03 JUL 97
Reported: 15 JUL 97
Client PO. NO.: 190·00001•01
Projact: 190•00001·01/MACON DOCKERY
Sampled BY: CHent
Code: 095870716
REPORT OP' IUlSUl.TS Page 11
LOG NO
73744•6
73744•7
737H·8
73744·9
73 744-10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Practical Quantitation Limits
Me'thod Blank
Lab Control Standard Result
LCS S,q,ected Value
Lab Control Standard t Recovery
PARJIMET&R 73744·6 73744•7 73744·8 73744·9 73744•10
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
t>ilution faccor
Batch ID
Antimony (7041)
Antimony (7041). ug/1
c'repar_ation Cate
Date.Analy~ed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium (6010). ug/1
Preparation Oate
Date Analyzed
Dilution factor;
Batch ID
3.0
10
50
<LO
07.07.97
07.08.97
l.0
07071'
<10
01.00.n
07.09.97
l.0
07081C
<50
07.07.97
07.08.97
l.0
0707B
----------
48.6 50.0
07.07.97
07.08.97
l.0
0707F
53.2 50.0 106 t
07.08.97
07.09.97
1.0
0708K
508 500 102 t
07.07.97
07.08.97
1.0
0707B -...... ---
• Labo,atorles In.Savannah, GA • Ta//:tt,.,ssee, FL• Tempo, FL• Oeerlield Beoc/1, FL• MoDile, AL.• New Orleans; L.A
•
~Hl'11'1Hn L...H.C::> r-. ..1..::::
~
SL SAVANNAH LABORATORIES
& ENV/RONM~TAL SDtVICES, INC.
5102 L.aAOChe Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. StavQ Irtning"er
AppliQd Rarth ScienCQ~
751 Arbor Street
Concord, ~c 28025
LOG NO: S7·73744
Received: 03 JUL ,1
Reported: 15 JUL.37
Client PO. No.: 190-00001·01
Project: 190·00001·01/MACON DOCKllRY
Sampled By: Client
Code: 095870716
REPORT OF RESULTS Page 12
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES ------------.... --------......... ---------.. --------------. -... ------- -----------.... --. ------
73144-6
73744-7
73744-8
73744•9
73744-.10
Practical Quantitation Limits
M<1thod Blank
Lab Control Standard Result
LCS Expected Value
Lab Control Standard t Recovery
-----.----------------.. ·--------------------------------------................. ·--·---------
PARAMETER 73744•6 73744·7 73744·8 73744•9 73744·10
Zinc: 16010)
Zinc (60·10), ug/1
Preparation Oate
Date Analyzed
Dilut.ion factor
Batch ID
20 <20
07.07.97
07.08.97
l.O
0707B
515
07.07.97
07.08.97
1,0
0707B
500 103 l
• Laboratories in Sarannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orte&ni, I.A
•
JUL-.10-.1J✓t .1,:;;.,•-.r rro;:ua·1 ;:)H'Jl"'INr'tHl"1 LHOO .
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
,u
5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354•7858 • F'ax [phone]
LOG NO
Mr. Seeve Irminger
Appli•d EU'th Sciences
751 Arbor Street
concord, NC 28025
LOG NO: S?-73744
Received: 03 JUL 97
Reported: 15 JUL 97
Client PO. No.: 190-00001•01
Project: 130-00001·01/Mi<CON DOCICERY
Sampled By: Client
Code: 035870716
REPORT OF RESULTS Page 14
SAMPLE DSSCRIPTION, QC REPORT FOR LIQUID SAMPLES .... ---. --. -...... -------......... --------.... --------.. --------------............... ------........... -· --
73744•11 LCS Accuracy Control Limit. (lrR) .. --............................... ·--------.. --.......... --.... ·----------····-····----------··-'"·"-·
PARAMB':'l!R
Vanadium (6010)
vanadium. (6010)
Zinc (6010)
Zinc (6010)
_73744 •ll
80-1:ZO t
80•120 \-
Methods: EPA SW-846 and 40 CFR Part 136.
Lisa G. McLeod, Project Manager
Final Page o~ Report
• Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach. Fl • Mobile, Al • New Orleens, LA
TOTAL P.13
•
•
•
•
HU1..r,-1J::>-1~·:fr 1~;uu ~HVHNNHH LHb:::i
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
P.02
5102 LaAoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Barth sciences
751 Arbor S1:.reet
Concord, NC 28025
LOG NO: S7-74199
Received: 28 JOL 97
Reported: OS lllJG 97
Clienc PO. No.: 190-00001-0l
Project: 190-00001·01/MACON DOCKERY
Sampled By: Client
Code: 14507085
RBPORT OF RBSUI.TS Pagel
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
74199-1 Macon System Swnp
74199-2 Macon Syscen Mid
74199-3 Macon System &ff1ugnt ···-·----------------------........... ___________________________ _
PARAMETER
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Cate Analyzed
Dilution factor
Bacch ID
74199-1
47
07.28.97
07.29.97
l.0
07281
----------
DATB/
TIMB SAMPLED
07-25-97/1250
07-25-97/1251
07-25-97/12S2
741.99-2
86
07.28.97
07.29.97
LO
07281
74199-3
36
07.28.97
07.29.97
l.0
07:lBI .. .. --..... -----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deertleld Baach, FL • Mobile, AL • New Orleans, LA
•
•
•
~HNNHH LHt:1:::i . s L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue •Savannah.GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Barch Sciences
751 Arbor Screec
Concord, NC 28025
l.OG NO: S7-74199
Received: 28 JUL 97
Reported: OS AUG 97
Client PO. No.: 190-00001-0l
Project: 190·00001-01/MACON DOCKERY
Sampled By: Client
Code: 14507085
REPORT OF RESULTS Paga 2
LOG NO
74199-4
74199-5
74199-6
74199-7
74199-8
SAMPLE DESCRIPTION, QC REPORT FOR LIQO'ID SAMPLES
Practical Quantitation Limit
Method Blank
Lab Control Standard Result
LCS ExpQCtQd ValuQ
Lab Control Standard% Recovery
PARAMETER 74199-4 74199-5 74199-6 74199-7 74199-8
Manganese (6010)
ManganQsa (6010), ug/1
Pre~aration Date
Pate Analyzed
Dilution factor
llacch ID
5.0 <5.0 533 500 107 t
07.28.97 07.28.97
07.29.97 07.29.97
l.0 LO
0728I 0728I
Laboraro,ies in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mooi/e, AL • New Orleans, LA ·
•
•
•
:,HVHNNHH LH~ •. ··s L SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
I-' .1;:'.14
5102 LaRoche Avenue •Savannah.GA 31404 • [phone] • Fax [phone]
Mr. sceve Irminger
Applied Earth Sciences
751 Arbor Screet
concord, NC 28025
LOG NO: 57-74199
Received: 28 JUL 97
Reported: 05 ArJG 97
Client PO. No.: 190·00001-01
Project: 190·00001-01/MACON DOCKERY
Sampled By: Client
Code: 14517085
REPORT OF RESULTS Page 3
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
74199·9
PARAMETER
LCS Accuracy Control Limit (tR)
Manganese (6010)
Manganese (6010)
Methods: EPA $W•846
Lisa G. McLeod, Project Manager
74199·9
80·120 .-
Final PagQ Of Report
LAboratorlH In Sa.,.,,,nah, GA • Ta/Jaha,;see, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
TOTAL P.04
Serial Number 1 3 2 ~--SL AVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES. INC
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
PROJECT REFERENCE PROJECT NO. P.O.NUMBEA
H!\(ci I I c)C.( (EJ'.'/ I ,l' fJ,A :· ,4
DATE
tv11\( ( t-1 <.:-..~,--_:,rt:. r-1 C. rr .I
I'-!,\ I .. {'f'\I <:.,o-...;i'(C F-r-~ -·
cJ;1A·:(' ,,. i~ (J( r c:· •• ·I' l:. ' ·-,.... .-,.
7/l :...__1Pf-'(:_ ,, t":>C·( f ~ . ... ' ... ,f~ c·. ,-·
r-c,P hu\~1K •
51021.aRoche Avenue, Savannah, GA 31404
0 2&16 Industrial Plaza Drive, Tallahassee. FL 32301
0414 SW 121h AVOflue, Oeerfiek1 Beach, FL 33442
0 900 l.alteside Drive, Mobile, AL 36693
06712 Be~in Road, SUite 100, Tampa, FL 33634
0100 Alpha Drive, Suile 110, Deslrehan, LA 70047
Phone: [phone]!
Phone: (904) B78-3994
Phone: [phone]
Phone: (334) ~
Phone: [phone]
Phone: [phone]
:: ,~EOUIREDANALYSES
NUMBER OF CONTAINERS SUBMITTED
-~ ! I
I i
., I
" ' I :,
. :; ' ~ I .\' '
'
•
RE~!IIUISHED BY: (S)GfTURE) _ ; / ,'
,_{J A-, (-'.i :I'-•,., I{,.-_.,. I
D~1i . TIME RE,llN<;P!SHEt (Sl':'i/,'ci DATE TIME RELINQUISHED BY: (SIGNATURE) "! }(; -· '\ , ... .· -, 1/~--t.'/:-'__,: . ..L I _ /..._.,.<,J_(. -.w ·;7 i--
RECEl)IED ll,Y: (SIG)'iATURJJ f/_ _
/(,,/·, ,./ -"~-'/; _DfTE _ TIME AECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (SIGNATURE)
1(it/:1 !/ ''('
. / LABORATORY USE ONLY
REC~IVED FO_ R LABORAT/:,, BY:{SIGNATURE}
. ' ~ ~:Jc;.,,,, {
DATE TIME
'1/3/17 /D'J-'S
CUSTODYINTACT CUSTOOYSEALNO. SLLOGNO. ~RATORY REMARKS:
Fax: [phone]
Fax: [phone]
Fax: [phone]
Fax: (334) ~
Fax:[phone]
Fax: [phone]
TA~OAAO
EPORT
ELIVERY
REMARKS
D4TE TIME
DATE TIME
'
•
•
•
State of North Caroli~
Department of Envir9nent.
Health and Natural Resources
Division of Waste Management
James B. Hunt. Jr .. Governor
Jonathan B. Howes. Secretary
William L. Meyer. Director August 4, 1997
Ms. Giezelle Bennett
Remedial Project Manager
Superfund Branch
Waste Management Division
US EPA Region IV
61 Forsyth Street, 11th Floor
Atlanta, Georgia 30303
RE: Comments on June 1997
Monthly Progress and O&M Report
Macon/Dockery Site
Cordova, Richmond County
Dear Ms. Bennett:
filf COPY
The Superfund Section of the North Carolina Department of Environment, Health and Natural
Resources (NC DEHNR) has received and reviewed the June 1997 Monthly Progress and O&M
Report for the Macon/Dockery National Priority List (NPL) Site and offers the following comments.
1. Please include the chain of custody documentation with the respective laboratory reports.
2. Provide a justification for not conducting air sampling at all air stacks and along the property
line. Provide a timeframe for completing this portion of the quarterly air sampling event.
Please note that pages 1, 2 and 3 of the laboratory report have been inadvertently omitted
from the June 1997 Monthly Progress and O&M Report.
The Superfund Section of the NC DEHNR appreciates the opportunity to comment on this
document. If you have any questions or comments, please feel free to call me at (919) 733-
2801, extension 349.
P.O. Box 27687.
Raleigh. North Carolina 27611-7687
Voice 919-733-4996
Sincerely, PJ $(/6:C,HHM
David B. Mattison, CHMM
Environmental Engineer
NC Superfund Section
fkffiAJII~ $£2,YIJI
FAX [phone]
An Equal Opportunity Affirmative Action Employer
50% recycled/lO"h post-consumer paper
•
•
MACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
MONTHLY PROGRESS AND
O&MREPORT
APRIL 1997
L
•
•
•
May 8, 1997
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 30365
Re: Maconillockery Site -Cordova, North Carolina
Monthly Progress and O & M Report -April 1997
Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group"), the April 1997 Monthly Progress and O &
M Report is herewith submitted in accordance with SECTION X\/ -PROGRESS REPORTS of the
Unilateral Administrative Order ( effective date -June 30, 1992) for the Macon/Dockery Site. This
report describes activities which occurred during the month of April as part of the Remedial Design
and Remedial Action phase of this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH APRIL 1997:
• Monthly sampling of the remediation systems effluent.
• Continue O & M of systems.
RESULTS OF SAMPLING AND TESTING AND OTHER DAT A RECEIVED:
• Laboratory results for April 1997 sampling of the remediation systems is included in this
progress report. Tables I to 4 record the analytical results for the four groundwater treatment
systems. All effluent concentrations are below the Remediation Performance Standard.
• Upper Dockery flow meter reading for April totaled 276,556 gallons. System was
operational 100% of the time averaging 6.9 GPM. Mass VOC removal was 0.30 pounds for
the month and the cumulative is 6.84 pounds.
• Lower Dockery flow meter reading for April totaled 180,560 gallons. System was
operational I 00% of the time averaging 4.5 GPM. Mass VOC removal was 0.15 pounds for
the month and the cumulative is 3.49 pounds .
• Macon Source Area flow meter reading for April totaled 253,167 gallons. System was
operational I 00% of the time averaging 6.3 GPM. Mass VOC removal was 0.14 pounds for
the month and the cumulative is 1.36 pounds.
751 Arbor Street• Concord. North Carolina 28025 • Tel: [phone] • Fax: [phone]
•
•
•
Ms. Giezelle Bennett
April IO, 1997
Page No. 2
• Upper/Lower Macon flow meter reading for April totaled 918,080 gallons. Combined
system was operational l 00% of the time averaging 22. 76 GPM. Mass VOC removal was
0.18 pounds for the month and the cumulative is 1.89 pounds.
TASKS PLANNED FOR MAY 1997:
• Monthly sampling of the remediation systems effluent.
♦ Quarterly sampling of designated monitoring wells and system influents.
♦ Quarterly air sampling ofSVE influents, system effluents, and the ambient air at the property
line .
• Continue O &M of systems.
• Check Upper Dockery gallery. The gallery has been talcing all of the effluent water and not
overflowing.
♦ Check Upper and Lower Macon infiltration gallery.
PROBLEMS AND DELAYS:
• April 8, 1997 -Soil Vapor Extraction (SVE) system motor was removed because of
excessive noise and vibration. The motor has been diagnosed by the manufacturer as having
failed bearings. A replacement motor has been ordered.
• April 18, 1997 -Upper Macon extraction well UM-6 was restarted following a drop of the
waer level within the Macon infiltration gallery to a normal operating range.
♦ April 24, 1997 -Upper Macon Source Area extraction well UMS-4 was put placed back into
service after one (I) week off for repair of a motor saver.
•
•
Ms. Giezelle Bennett
April I 0, 1997
Page No. 3
• Percent operational for each system: Upper Dockery
Lower Dockery
Upper Macon
Lower Macon
100%
100%
100%
100%
Macon Source Area I 00%
SVE system 27%
Respectfully Submitted,
Jb-<Q~
David Jones
Project Coordinator
fo!U
cc: Macon/Dockery Site Group Members
Paul Furtick, RMT, Inc.
Ms. Norma Eichlin, COM Federal Programs
David Lown, NC Super Fund Section
• •
UD lnnuent 2/13/96 " 2/13/96 7.7 130 33
2/14/96 4.3 89E 1.2 55 4.5
2/14/96 6.5 100 34 5.3
2/14/96 4.4 120E 1.4 u 50 7.9
2/14/96 4 110 48 7.8
2115196 4.5 IJOE 1.2 1.4 54 8.3
2/15/96 5.5 140 " 8.6 2.8
2/16/96 7.5 160 64 lO
2/17/96 5.7 !SOE 1.7 2.1 62 9.4
2/17/96 5.5 120 42 6.4
2122/96 5.4 !SOE 1.4 52 5.7
2/22/96 4.9 96 48 5.5
2/28/96 6.4 200E 1.9 19 5.3
2/28/96 6.8 2<0 50
3/8/96 5.2 l)0•FJ5 1.7 55 3.8
4/3/96 3.6 160E I.I 1.6 38 5.6
4/3/96 92 " 3.9
513/96 130 38 4.8
6/5/96 2 110 5.2 2.8
7/1196 2 77 " 3.6
8/1/96 6.1 220 52 5.7
I 1/7/96 240 54
11/7/96
215197 IOO J]
UD Effluent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2122196
2/lS/96
3/8/96
,HJ/96
5/3/96
6/5196 3.9
7/1/96
8/1/96
9/4/96
10/1/96
lln/96
12/5/96 1.5
1/6/97
2/5/97
l/12197
4/8/97
Remediation Pcrfonnance Standard 3500 70 200 2.8 1000 400
Noie: A blaJl.k mcut ~low dCIC<:tion li,,,it
Noie: • Acetone confiJ111ed bv Method 8260
• •
2/13/96
2/14/96 12 53 14 52
2/14/96
2/14/96 II 54 14
2/14/96
1115196 19 81 S3
2/15/96
2/16/96 II 57 II
2/17/96 " 12
2/17/96
2/22196 13 13
2/22/96
2/28/96 II 7.7
2/28/96
3/8/96
4/3/96 II 52
4/3/96
5/3/96 16 " 615196
7/1/96
8/1/96 II s.s 10
1 ]n/96 2IOO 19 61 9.5
11/7/96 ISO•
2/5/97 12 SI
UD Emuent 2/13/96 I 70"F32 16 71 40 22 14
2/14/96 JS•FJJ IS 53 14 II
2/14/96 II 56 12
2/15/96 12 53 14
2/16/96 53 II
2/17/96 II " 12
2/22/96 8.3
2/28/96 13 9.6 10
3/8/96 25 6.9
4/3/96 28 II so
5/3/96 52
615196
7/1/96
8/1/96 20 14 SI 7
9/4/96 " 10/1/96 5.9
I ln/96 IS 59
12/5/96 12 54 5.1
J/6/97 13 54
215191 IS 61 5.9
3/12197 69
4/8/97 63.
Remediation Performance Standard 3500 so 1000 so 5000 IS
Note: A blanl mca,,J below dctcctio,, limit
Sole:• Atclom: confirmed by Method 1260
• •
Sample I, I -Dichloroethane Cis/trans-1,2-Dichloroelhene
Location (ug/L) (ug/L)
LD Influent 2113/96 I. I 80 33 40
2/14/96 1.3 II0E 43 37
2/14/96 80 13 15
2/14/96 1.6 94E 39 1.8 1.7 39
2/14/96 64 16 2.2 2.5 18
2/15/96 1.2 82 32 1.7 29
2/16/96 3.3 95 35 2.6 31
2/22/96 2.5 5.8 100 54
2/28/96 1.2 93E 33 30
2/28/96 92 35 30
3/8/96 2 I lO 47 34
4/3/96 79 36 28
5/3/96 71 30 I. 7 40
6/5/96 67 32 I.I 2 42
8/1/96 83 27 54
1117196 69 28 38
3/12/97 66 21 23
LO Effluent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
8/1/96
I 0/1/96
11/7/96
12/5/96
1/6/97
3/12/97
4/8/97
Remediation Performance Standard 3500 7 70 5 200
Nole: A blank means below detection limit
• •
Manganese
Location (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L)
LD Influent 6.4 17 260 270
8.6 8.3 250 120
2/14/96
2/14/96 9 8.3 240 I IO
2/14/96 6.6 6.5
2/15/96 8.4 5.3 200 84
2/16/96 8.7 4.3 190 81
2/22196 5.2 1.8 13 3.4 14 240 240
2128/96 7.4 1.3 120 77 8
2/28/96 6.4
3/8/96 6.7 95 30
4/3/96 6.6 160 39
5/3/96 5.4 16 63 200 0.91
6/5/96 5.2 2.5 230 46
8/1/96 5.9 I IO 5
11/7/96 5.8 230
3/12/97 76
LO Effluent 2/13/96
2/14/96
2/14/96 II
2/15/96
2/16/96
2/22/96 5
2/28/96
318/96
4/3/96
5/3/96
8/1/96 13 0.56
10/1/96 II
I 1/7/96 3.4
12/5/96 35 19
1/6/97 6
3/12197 70
4/8/97
Remediation Performance Standard 2.8 1000 400 50 1000 50 5000 5
Note: A blank means below detection limil
• •
Location (ug/L)
UMSA Influent 2/13/96 15 14 19 16 5.9 25
2/14/96 I.I 14 II 10 7.3 7.2 10
2/14/96 II 14 II 17 6.1 17
2/15/96 12 14 II 18 5.9 16
2/16/96 7.5 21 17 14 9.7 25
2/17/96 9.7 18 16 II 7 24
2/22/96 I.I 10 17 16 15 7.6 25
2/28/96 9.8 16 13 12 5.8 21
3/8/96 7.6 10 10 7.7 4.1 16
4/3/96 5.5 16 8.5 7.4 5.4 18
513/96 4.8 12 6.9 5.7 12
6/5/96 8.7 22 6 6 13
7/1/96 3.8 II 6.9 4.8 4.3 12
7/30/96 7.9 15 10 6.4 4.2 13
11/7/96 7.2 9.2 7.5 2.3 3.4 10
2/4/97 3.0 27 7.8 2.3 8.8 15
(DUP) 2/4/97 2.4 25 6.2 1.8 7.9 14
UMSA Effluent 2/13/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
513/96
6/5/96
7/1/96
7/30/96
9/4/96
10/1/96
11/7/96
12/5/96
1/6/97
2/4/97
3/12/97
4/8/97
Remediation Perfonnance Standard 3500 7 70 200 2.8
Note: A blank means below detection limit
OUP -duplicate
• • e
Location (ug/L) (ug/L) (ug/L) (ug/L)
UMSA Influent 2/13/96 1.9 140 300 55 3.5 21
2/14/96 1.5 110 180
2/14/96 I 110 160 20
2/1 5/96 1.3 100 140
2/16/96 120 160 0.22
2/17/96 110 110
2/22/96 120 65
2/28/96 130 52 7
3/8/96 130 41
4/3/96 110 27 8.2
5/3/96 97 21
6/5196 I.I 3.6 130 19 5
7/1/96 11 110 13 5
7/30/96 4.5 130 13 6
11/7/96 2 140 9.8 10
2/4/97 150 24 36
(DUP) 2/4/97 140 17
UMSA Effluent 2/13/96 16 150 330 74 4.2 57
2/14/96 I JO 190 20
2/14/96 110 160
2/15/96 100 140
2/16/96 130 170 0.26 18
2/17/96 120 120
2/22/96 120 70
2/28/96 130 5 I
3/8/96 120 37
4/3/96 110 27 5
513196 120 26
6/5/96 2.9 130 22 6
7/1/96 12 110 14
7/30/96 200 110 41 9.2 23
9/4/96 II 170 68 26 66 16
10/1/96 130 13 0.47 24
11/7/96 140 13 26
12/5/96 170 17 5
1/6/97 200 46 25 3.5 120
2/4/97 1600 29 8
3/12/97 130 30
4/8/97 · 200 ,JO ,, .. 7
Remediation Performance Standard 1000 50 1000 50 · 5000 5 15 I. I
Note: A blank means below detection limit
DUP. duplicate
• • •
UM lnnucnt 2121196 IJ ~ IO 3.9 1.5 S.5 12 16
2fll/96 6 4.1 1.6 S.8 4.8 12 IS
2f23/96 4.5 L6 64 4.8 12 12
2/24/96 1.4 4.6 LS 6.4 6 14 9.7
2/25/96 1.2 2.2 6.6 6.9 IS 9.2
WS/96 3.S 5.8 1.4 8.6 s 14 2.9 3M6 4.7 I 8.6 3.8 12
3/16/96 S.5 LS 9.2 4.6 12
4/3/96 4.4 L6 66 10 6/5196 4.9 L8 7.7 9.8 3.2 ~ 3.8 LI 6.1 3.3 7.6
?n0/96 4.1 2.1 8.6 3.3 9.8
lln/96 S.3 L9 6.6 2.3 8.3
2/4/97 S.S L6 7 2.5 u
LM lnnuent 2/21/96 17 15 5.5 2.1 LI 7.6 2.2 9.3
2122/96 IS 22 8.4 3.3 L7 II 3.2 12
2/2V96 14 26 9.1 4.4 2 14 3.3 IS 2/23196 13 29 II 4.9 2.1 IS 3.6 18
2/1.4196 8.9 JO ll 4.9 2.7 17 4.5 17
2/25/96 8.2 31 ll 5 2.6 17 4.4 IS
2/28/96 32 IS S.6 2.4 17 4 4.2
3/8196 9.5 1.6 2.4 2 s LI
3/16/96 8.1 L8 2.4 3.4 1.4 ~ 7.3 2.6 2.3 4.7 ~ 8.6 27 2.9 4.2 46
6/5/96 12 4.7 3.4 S.3 4.9 4.6
7!30196 17 66 6.7 4.1
I tn/96 II 3.3 2.2 5.2 4.S ~ L6 9.8 2.1 2.4 4.4 3.7 (DUP) ~ 1.5 9.0 L8 2.1 3.8 3.1
U/L Effiuent 2121/96
2fll/96 LS 16
2fll/96
2123196
2/24/96
2/25/96
2/28/96
J/8/96
3/]6196
~ LS L6 L9 ~
615196 2.1 ~
7/30/96
9/4/96
10/1/96
11/7196
12/5/96 ~ ~
J/12/97
418/97
Remediation Performance Standard 3500 70 200 2.8 11\00
Nole, A blonl. means l><low J<te,;lica limll
IJUl' . dupbeale
• • •
UM Innuent 2/21/96 140 1l
ll21196 )9 ll0 7.2
2/22/96 J6 120 4.8
2ill/% 31 110 4.5
V24/96 30 110 3.6
2/25/96 18 110 3.4
ll28/96 18 40
3/8/96 1l 50
3/\6/96 20 50
413/96 9.3 26 10
6/5/96 22 1l
7/1/96 ----7/J0/96
lln/96
2/4197 J6
LM Jnf1ucn1 2/21/96 68 110 120 5.1 15
2/22/96 70 120 120 5.6
2/22/96 77 130 120 5.5
2/23/96 81 140 130
2/24/96 86 160 160 ,,
2/25/96 86 160 160 3.2
2/28/96 100 150 240 3.3
3/8/96 72 52
3/16196 53 51
4/3/96 72 " 513196 24 31 27
615196 " 24
7/30/96 20 6
lln/96 6.4
214197 34 19
(OUP) 214197 34 16
U/L Effiucnt ll21/96 59 100 98 4
2/22/96 130 70 120 120 5.2
2121196 72 120 120 5.1
VW96 80 140 130 ,.,
1124/96 83 150 llO 3.7
2/25/96 90 160 170 3.6
2/28/96 32 59
3/8/96 )9 56
3/16196 31 " 4D/% " 54 3.6 10
5/3/96 31 10 " 6/5/96 1.5
7/1/96
7/30/96
9/4/96
10/1/96 24
nn/96
12/5/96
1/6/9"1
214/97 39
3/12197
418/97
Remediation Performance Standard 50 1000 50 50011 15
No<e: A bt.nl. 1t1<on> bckM detection limit
DUP•dupli<ai..
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 La Roche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 1
LOG NO
71977-1
71977-2
71977-3
71977-4
PARAMETER
SAMPLE DESCRIPTION, LIQUID SAMPLES
Upper Macon
Lower Macon
Upper Dockery
Lower Dockery
71977-1 71977-2
DATE/
TIME SAMPLED
04-08-97/1515
04-08-97/1530
04-08-97/1550
04-08-97/1600
71977-3 71977-4
-------------------------------------------------------------------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride (Dichloromethane),
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
ug/1
<1.0
<l.O
<1.0
<1.0
<2.0
<1.0
<l.O
<l.0
<1.0
100 %
14 .18. 97
1.0
0417A
1B0418
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<l.O
<l.0
<1.0
96 %
04.18.97
1.0
0417A
1B0418
<1.0
<1.0
<1.0
<l.O
<2. 0
<1.0
<1.0
<1.0
<1.0
110 %
04.18.97
1.0
0417A
1B0418
<1.0
<1.0
<1.0
<l.0
<2.0
<1.0
<1.0
<1.0
<1.0
100 %
04.18.97
1.0
0417A
1B0418
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach. FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO, S7-71977
Received: 10 APR 97
Reported, 21 APR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 150770421
REPORT OF RESULTS Page 2
LOG NO
71977-1
71977-2
71977-3
71977-4
PARAMETER
SAMPLE DESCRIPTION, LIQUID SAMPLES
Upper Macon
Lower Macon
Upper Dockery
Lower Dockery
71977-1 71977-2
DATE/
TIME SAMPLED
04-08-97/1515
04-08-97/1530
04-08-97/1550
04-08-97/1600
71977-3 71977-4
-------------------------------------------------------------------------------
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Beryllium (6010)
Beryllium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<1.0
<1.0
<3. 0
<10
100 %
04.18.97
1.0
0417A
1B0418
200
04.11.97
04.14.97
1.0
0411L
<5.0
04.11.97
04.14.97
1. 0
0411L
<1.0
<1.0
<3.0
<10
100 %
04.18.97
1.0
0417A
1B0418
<50
04.11.97
04.14.97
1.0
0411L
<5.0
04.11.97
04.14.97
1.0
0411L
<1.0
<1.0
<3.0
<10
100 %
04.18.97
1.0
0417A
1B0418
63
04.11.97
04.14.97
1.0
0411L
<5.0
04.11.97
04.14.97
1.0
0411L
<1.0
<1.0
<3. 0
<10
97 %
04.18.97
1.0
0417A
1B0418
<50
04.11.97
04.14.97
1.0
0411L
<5.0
04.11.97
04.14.97
1.0
0411L
-------------------------------------------------------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
· & ENVIRONMENTAL SERVICES, INC,
ft 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
0
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
71977-1
71977-2
71977-3
71977-4
PARAMETER
Upper Macon
Lower Macon
Upper Dockery
Lower Dockery
71977-1 71977-2
04-08-97/1515
04-08-97/1530
04-08-97/1550
04-08-97/1600
71977-3 71977-4
------------------------------------------------- --------------------
Cadmium ( 7131}
Cadmium (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Chromium (6010)
Chromium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<0.30
04.11.97
04.14.97
1.0
0411F
<10
04.11.97
04.14_97
1.0
0411L
30
04.11.97
04.14.97
1.0
0411L
<0_30
04-11.97
04.14.97
1.0
0411F
<10
04.11_97
04.14.97
1.0
0411L
<5.0
04.11.97
04.14.97
1.0
0411L
----------
<0.30 <0.30
04.11.97 04.11.97
04.14_97 04.14.97
1.0 i.o
0411F 0411F
<10 <10
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
<5.0 <5.0
04-11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
71977-1
71977-2
71977-3
71977-4
Upper
Lower
Upper
Lower
Macon
Macon
Dockery
Dockery
04-08-97/1515
04-08-97/1530
04-08-97/1550
04-08-97/1600
------------------------------------------------------------------------------------
PARAMETER 71977-1 71977-2 71977-3 71977-4
-------------------------------------------------------------------------------
Nickel (6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<40
04.11.97
04.14.97
1.0
0411L
<3.0
04.11.97
04.14.97
1.0
0411F
<10
04.11.97
04.16.97
1.0
0411F
<40
04.11.97
04.14.97
1. 0
0411L
<3.0
04.11.97
04.14.97
1.0
0411F
<10
04.11.97,
04.16.97
1. 0
0411F
----------
<40' <40
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
<3.0 <3.0
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411F 0411F
<10 <10
04.11.97 04.11.97
04.16.97 04.16.97
1. 0 1.0
0411F 0411F
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
Client PO. No.: 190-00001-0l
Project: 190-00001-0l/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
71977-1
71977-2
71977-3
71977-4
Upper
Lower
Upper
Lower
Macon
Macon
Dockery
pockery
04-08-97/1515
04-08~97/1530
04-08-97/1550
04-08-97/1600
------------------------------------------------------------------------------------
PARAMETER
Vanadium (6010)
Vanadium, ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Zinc (6010)
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
71977-1
----------
<50
04.11.97
04.14.97
1.0
0411L
<20
04.11.97
04.14.97
1.0
0411L
7.0
04.11.97
04.12.97
1.0
0411B
----------
71977-2
----------
<50
04.11.97
04.14.97
1.0
0411L
<20
04.11.97
04.14.97
1.0
0411L
<5.0
04.11.97
04.12.97
1.0
0411B
----------
71977-3 71977-4
--------------------
<50 <50
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
<20 <20
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
<5.0 <5.0
04.11.97 04.11.97
04.12.97 04.12.97
1.0 1.0
0411B 0411B
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO:
Received:
Reported:
S7-71977
10 APR 97
21 APR 97
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
LOG NO
71977-5
PARAMETER
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
--------------------------------------------------
Trip Blank
--------------------------------------------------
71977-5
Page 6
--------------------------------------- ----------------------------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene, ug/1
Methylene chloride (Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochlorornethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
<1.0
<1.0
<1.0
<1.0
<2. 0
<1.0
<1.0
<1.0
<1.0
100 %
04.18.97
1.0
0417A
1B0418
<1.0
<1.0
<3. 0
<10
100 %
04.18.97
1.0
0417A
1B0418
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
LOG NO ' SAMPLE DESCRIPTION
REPORT OF RESULTS
QC REPORT FOR LIQUID SAMPLES
-------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
Page 7
------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10
----------------------------------------------------------- --------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
<l.O
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
98 %
04.18.97
1.0
0417A
1B0418
15
19
100 %
04.17.97
1.0
0417A
180417
14
20
100 %
04.18.97
1.0
0417A
1B0418
--------------------------------------- ------------------------------
20
20
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value_
-----------------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10
Purgeable Aromatics (8020)
Benzene, ug/1 1.0 <1.0 20 19 20
Toluene, ug/1 1.0 <1.0 14 14 20
Total Xylenes, ug/1 3.0 <3. 0
Acetone, ug/1 10 <10
Surrogate -a,a,a-Trifluorotoluene 110 % 103 % · 103 %
Date Analyzed 04.18.97 04.17.97 04.18.97
Dilution factor 1.0 1.0 1.0
Batch ID 0417A 0417A 0417A
Clock ID 180418 18041 7 1B0418
Barium (6010)
Barium (6010), ug/1 50 <50 2150 2180 2000
Preparation Date 04 .11. 97 04.11.97 04.11.97
Date Analyzed 04.14.97 04.14.97 04.14.97
Dilution factor 1.0 1.0 1.0
Batch ID 0411L 0411L 0411L --------------------------------------- ----------------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO, S7-71977
Received, 10 APR 97
Reported, 21 APR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 150770421
REPORT OF RESULTS Page 9
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Contr61 Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10
-------------------------------------------------------------------------------
Beryllium (6010)
Beryllium (6010) , ug/1 5.0 <5.0 48.4 49.6 so.a
Preparation Date 04,11.97 04.11.97 04.11.97
Date Analyzed 04,14.97 04.14.97 04.14,97
Dilution factor 1.0 1.0 1.0
Batch ID 0411L 0411L 0411L
Cadmium (7131)
Cadmium (7131), ug/1 0.30 <0.30 5.54 5.58 5.00
Preparation Date 04.11.97 04.11.97 04.11.97
Date Analyzed 04.14.97 04.14.97 04.14.97
Dilution factor 1.0 1.0 1.0
Batch ID 0411F 0411F 0411F
Chromium (6010)
Chromium (6010), ug/1 10 <10 206 213 200
Preparation Date 04.11.97 04.11.97 04.11.97
Date Analyzed 04.14.97 04.14.97 04.14.97
Dilution factor 1.0 1. a 1.0
Batch ID 0411L 0411L 0411L
------------------------------
' Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
Cl 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO:
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
S7-71977
Received: 10 APR 97
Reported: 21 APR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 10
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10
-------------------------------------------------------------------------------
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Nickel (6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
5.0
40
3.0
<5.0
04.11.97
04.14.97
1.0
0411L
<40
04.11.97
04.14.97
1.0
0411L
<3.0
04.11.97
04.14.97
1.0
0411F
519 531 500
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
523 539 500
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411L 0411L
50.2 49.7 so.a
04.11.97 04.11.97
04.14.97 04.14.97
1.0 1.0
0411F 0411F
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71977
Received: 10 APR 97
Reported: 21 APR. 97
LOG NO
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 150770421
REPORT OF RESULTS Page 11
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10
----------------------------------------------------------- --------------------
Antimony (7041) • Antimony (7041), ug/1 10 <10 48.l 50.4
Preparation Date 04.11.97 04.11.97 04.11.97
50.0
Date Analyzed 04.16.97 04.16.97 04.16.97
Dilution factor l.O l.O 1.0
Batch ID 0411F 0411F 0411F
Vanadium (6010)
Vanadium, ug/1 so <50 516 526 500
Preparation Date 04.11.97 04.11.97 04.11.97
Date Analyzed 04.14.97 04.14.97 04.14.97
Dilution factor 1.0 1.0 l.O
Batch ID 0411L 0411L 0411L
Zinc (6010)
Zinc (6010), ug/1 20 <20 504 518 500
Preparation Date 04.11.97 04.11.97 04.11.97
Date Analyzed 04.14.97 04.14.97 04.14.97
Dilution factor l.O 1.0 l.O
Batch ID 0411L 0411L 0411L ---------------------------------------------------------------------
•
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
•
•
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO, S7-71977
Received, 10 APR 97
Reported, 21 APR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 150770421
REPORT OF RESULTS Page'l2
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-6
71977-7
71977-8
71977-9
71977-10
Practical Quantitation Limits
Method Blank Liquid
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value·
-----------------------------------------------------------------------------------
PARAMETER 71977-6 71977-7 71977-8 71977-9 71977-10 --------------------------------------------------------------------- ----------
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
5.0 <5.0
04.11.97
04.12.97
1.0
0411B
----------
104 102 100
04.11.97 04.11.97
04.12.97 04,12.97
1.0 1.0
0411B 0411B
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO, S7-71977
Received: 10 APR 97
Reported, 21 APR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 150770421
REPORT OF RESULTS Page 13
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-11
71977-12
LCS/LCSD % Recovery
LCS Control Limits
-----------------------------------------------------------------------------------
PARAMETER 71977-11 71977-12
-------------------------------------------------------------------------------
Purgeable Halocarbons (8010)
1,1-Dichloroethene, %
Trichloroethylene, %
Purgeable Aromatics (8020)
75/70
95/100
% 10-237 %
% 28-196 %
•
Benzene, %
Toluene, %
Barium (6010)
100/95
70/70
%
%
23-168 %
33-167 %
•
Barium (6010), %
Beryllium (6010)
Beryllium (6010), %
Cadmium (7131)
Cadmium (7131), %
Chromium (6010)
Chromium (6010), %
Manganese (6010)
Manganese (6010), %
Nickel (6010)
Nickel (6010), %
Lead (7421)
Lead (7421), %
Antimony (7041)
Antimony (7041), %
Vanadium (6010)
Vanadium, %
-------------------------------------------------
108/109 %
97/99 %
111/112 %
103/106 %
104/106 %
105/108 %
100/99 %
96/101 %
103/105 %
----------
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC .
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences
751 Arbor Street
Concord, NC 28025
LOG NO: S7-71977
Received: 10 APR' 97
Reported, 21 APR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 1507704'21
REPORT OF RESULTS Page 14
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71977-11
71977-12
LCS/LCSD % Recovery
LCS Control Limits.
-----------------------------------------------------------------------------------
PARAMETER 71977-11 71977-12
-------------------------------------------------------------------------------
Zinc (6010)
Zinc (6010), %
Suspended Solids (160.2)
Suspended Solids (160.2), %
101/104 %
104/102 %
80-120 %
75-125 % ------~~~~~~:~-;~~-;~:;~~-----
Lisa G. McLeod, Project Manager
• Final Page Of Report
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
5enal NumlHI< ::, i::'. t5 j:'. LJ ...---------~~--
Cl. (\I
0
a.
S I .AVANNAH LABORATORIES
... & ENVIRONMENTAL SERVICES, INC.
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
D 5102 LaRoche Avenue, Savannah. GA 3140..
D 2846 lndusnial Plaza 04ive, Ta!l.aha&se&, FL 32301 G .& I 4 SW I 2th Avenue, Oeerield Beach. fl J:W42
D 900 Lake~do Driw>. Mobile. AL 36693
D 6712 Benjamin Ao.ad, Suile 1 00, Tamp.a. FL 13634
D 100 Alpha Drive, Su~e 11 0, Oes1tehjl'\ LA 70047
})-
Phone: [phone]
Phone: [phone],4
PhOne: (~◄) 421•7400
Phone: (33◄) 666·8633
Phone: [phone]
Phone: (504) 764• I 100
Fa,: (912) 352•0165
Fax: (904) 878·9504
Fax: (954) 421•2584
F"": [phone]
Fu (813) 885•7049
Fax: (504) 725•1183
PROJECT REFERENCE PFIOJECT NO. P.O. \'UMBER l-:-:=::::--...-------,1<1-,f-TO'---------------,----r--t M4~-D~etl/ l-=:--c--~=-~'-..L.LJ'-4..~>L/ "'tl[;!/ I .,..,,i-AEOUIREDANALYSES PAOE loF D
' )
' I
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PROJECTLOC. SAMPLERja)NAME • PHONE-,-d<+ .,inn!,!) i ,~ ''f (Sla',e)NC.. E"r,'r, Rl-uce.., FAX -,r-.',uf.7 i. (,g t7
CLIEN1NAMEA. s CLIENTPROJECTMANAGER 'II. i 1,') _lJ I . xf;" i\tt.J/1' un,;-A,,__ (t s s, -"7 ~ ~1 ,_
CLIENTADDRESS(CITY.STATE.ZIPI V ,fi! :c:;; J "7". . ~·.. ..
SAMPLE , •.. sL· ro1 ,'!I I I I··/.· .... ;,. ··./.•·I I O.,.TE TlliE }~'· SAMl'l.E IDENTIFICATION I ;;/~I NUMBER OF CONTAINERS SUBMITTED 'f-fy.'f1 ~,'i." uAA~ M .. '6YI a ,
I
SIAAI0ARD
□REPORT DELIVERY
□E-PEOITEOREPORI
DEL 'NE RV(1u«1Wge)
/ o,i.Oue:
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.
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5' AEBiW:"SHEOBY:(S11":'T "'':l. ' I) Ii Pmi/ TIME,'>-. RE~l'!l'tDBY:(SIGNATUAE) .~'f...E/ 11ME RELINOIJ!SHEOBY•(SIGNATUREJ DATE TIME ); l\ VA"', °"·" \. (),. · · I;\ /j-j 1 7/ ,lt7 J : 1 t l 7_,. /'-· A A .u -7/',/if: /140 .,
" AkCE1vti,ev:(SIGNA11Jt1tJ DATE TIME RECEl\jEO'BY: (SIGNATURE) \ / OATI TIME ': · · r::dx ~· ·. , .. . . . . .. • U\BORATORYUSEONLY
1 RECEIVED1<pLABORATOIIYBY:! ~TlJRE) DATE~ : : TIME:. CUSTI:>DYINTACT CUSTODYSEALNO. ,SL LOON<>:. : fVl: ~ rir.nrfYYLY) . ¼0/~ ";0::t Bes O~o . ~~q:n -l
(
. J
RECEIVED BY: (SIGNATURE) DATE 11NE
. -.. •,:·. . . _., . ·-. ..
;_··
•
•
•
RECEIVED
AUG 2 9 7997
SUPERFUNO SECTION
MACON/DOCKERY SITE
CORDOVA, NORTH CAROLINA
MONTHLY PROGRESS AND
O&MREPORT
MARCH 1997
•
•
April 10, 1997
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, Georgia 30365
Re: Maconillockcry Site -Cordova, North Carolina
Monthly Progress and O & M Report -March 1997
Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group"), the March 1997 Monthly Progress and O
& M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS of
the Unilateral Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site.
This report describes activities which occurred during the month of March as part of the Remedial
Design and Remedial Action phase of this project.
PRO.JECT TASKS INITIATED OR COMPLETED THROUGH MARCH 1997:
• Monthly sampling of the remediation systems effluent.
• Continue O & M of systems.
RESULTS OF SAMPLING AND TESTING AND OTHER DATA RECEIVED:
• Laboratory results for March 1997 sampling of the remediation systems is included in this
progress report. Tables I to 4 record the analytical results for the four groundwater treatment
systems. All effluent concentrations are below the Remediation Performance Standard.
• Upper Dockery flow meter reading for March totaled 250,068 gallons. System was
operational 100% of the time averaging 6.2 GPM. Mass VOC removal was 0.27 pounds for
the month and the cumulative is 6.54 pounds.
• Lower Dockery flow meter reading for March totaled 277,823 gallons. System was
operational 58% of the time averaging 6.89 GPM. Mass VOC removal was 0.12 pounds for
the month and the cumulative is 3.23 pounds .
• Macon Source Area flow meter reading for March totaled 223,222 gallons. System was
operational 100% of the time averaging 3.8 GPM. Mass VOC removal was 0.12 pounds for
the month and the cumulative is 1.22 pounds.
751 Arbor Street• Concord, North Carolina 28025 • Tel: [phone] • Fox: [phone]
•
•
•
Ms. Giezelle Bennett
April 10, 1997
Page No. 2
• Upper/Lower Macon flow meter reading for March totaled 939,710 gallons. Combined
system was operational I 00% of the time averaging 23.31 GPM. Mass VOC removal was
0.18 pounds for the month and the cumulative is 1.71 pounds.
TASKS PLANNED FOR APRIL 1997:
• Monthly sampling of the remediation systems effluent.
• Continue O &M of systems.
• Check Upper Dockery gallery. The gallery has been taking all of the effluent water and not
overflowing .
♦ Check Upper and Lower Macon infiltration gallery. Return extraction well RW-6 to service
once water levels in this gallery have receded to the normal operating range (see problems
below).
PROBLEMS AND DELAYS:
• February 27, 1997 -Lower Dockery groundwater remediation system was off due to the
malfunction of the motor to the air stripper blower. The motor was removed from the site,
repaired, and the system re-started on March I 0, 1997.
• March 20, 1997 -Lower Dockery groundwater remediation system was off because of a high
level alarm in the air stripper sump. The sump was drained and the system restarted on
March 20, 1997.
♦ March 20, 1997 -Upper and Lower Macon groundwater infiltration gallery was observed to
be overflowing. Groundwater extraction wells RW-2, RW-4, and RW-6 were turned off to
reduce the flow to the infiltration gallery. On March 27, 1997, the infiltration gallery was
observed to not be flooding and wells R W-2 and R W-4 were re-started. Because the
•
•
•
Ms. Giezelle Bennett
April I 0, 1997
Page No. 3
infiltration gallery's water level was higher than the normal operating range, well RW-6
remains in an off position. A seasonal high water table and recent precipitation events are
suspected causes for the gallery flooding. At this time no correctional methods are
recommended other than temporarily reducing the flow and observing the water level in the
infiltration gallery on a weekly basis.
• Percent operational for each system: Upper Dockery
Lower Dockery
Upper Macon
Lower Macon
100%
58%
100%
100%
Macon Source Area I 00%
SVE system I 00%
J;:~·p
David Jones .fO
Project Coordinator
cc: Macon/Dockery Site Group Members
Paul Furtick, RMT, Inc.
Ms. Norma Eichlin, CDM Federal Programs
David Lown, NC Super Fund Section
• • •
2/13/96 7.7
2/14/96 4.3 S9E 1.2 " 4.5
2/14/96 6.5 100 34 5.3
2/14/96 4.4 J20E 1.4 1.3 50 7.9
2/14/96 110 48 7.8
2/15/96 4.5 130E 1.2 1.4 54 8.3
2/JS/96 5.5 140 2 56 8,6 2.8
2/16/96 7.5 160 64 10
2/17/96 5.7 !SOE 1.7 2.1 62 • 9.4
2117/96 5,5 120 42 6.4
2122196 5.4 ISOE 1.4 52 5.7
2/22/96 4.9 96 48 5.5
2/28/96 6.4 200E 1.9 19 5.3
2/28/96 6.8 240 50
3/&/96 5.2 130°F35 1.7 55 3.8
4/3/96 3,6 160E 1.1 1.6 38 5.6
4/3/96 3 92 25 3.9
513/96 4 130 38 4.8
615196 110 5.2 2.8
7/1/96 77 25 3,6
8/1/96 6.1 220 52 5.7
11nl96 240 54
lln/96
2/5/97 100 31
UD Efiluenl 2/13/96
2/14/96
2/14/%
2/15/96
2/16/96
2/17/96
2/22/96
Z/28/96
3/8/96
4/3/96
5/3/96
6/5/96 3.9
7/1/96
8/1/96
9/4/96
10/1/96
11n/%
12/5/96 1.5
1/6/97
215197
3/12/97
Remediation Performance Standard 3500 7 70 200 2.8 1000 400
Note: A bbnl mean, below <U=tion limit
No~:• Acctoac coaf1n11cd by Melhod 1260
•
Samolc
Location
UD Influent
Date
2/13/96
2/13/96
•
Acetone Chromium
(uo/1 \ (uo/1)
20
Bariwn
'" 92
Mam!anese
(Ulfll)
64
Zinc
'" 33
Lead
'" 3.1
:;; .. :
:::::/{/;"~:
Susocnded Solids
(moll)
SI
2/14/96 [_ 12 53 14 52 l------,,1--~21~14~19~6~-----<11----,1----+-----+----<1---1---~----,
2/14/96 11 14
2/14/96
2115/96 19 81 " 2115196
2/16/96 11 S1 11
2/17/96 " 12
2/17/96
2122196 13 13
1122/96
2/28/96 11 7.7
2128/96
J/8/96
4/3/96 11 " 413/96
5/3/96 16 58
6/5196
7/1/96
8/1/96 11 s.s
11/7/96 2100 19 61 9.S
lln/96
215/97 12 SI
UD Effiuent 2/13/96 70°F32 16 71 40 22 14
2/14/96 " " 14 11
2/14/96 11 " 12
2/15/96 12 " 14
2/16/96 SJ 11
2/17/96 11 " 12
2/22/96 8.3
2/28/96 13 9.6 10
3/8/96 25 6.9
413196 28 11 so
513196 S2
6/5/96
7/1/96
8/1/96 20 14 SI 7
9/4/96 " 10/1/96 S.9
1111196 IS S9
12/5/96 12 S4 S.l
116191 13 S4
215197 " 61 S.9
3/12/97 • 69
Remediation Pe1fonnance Standard 3500 so 1000 so sooo IS
Noie: A blank mc,1.111 below dc1Cctio11 limit I
Nou,: • Acetone C011fu:med by Method 1260 I
•
•
~~pie Date Chloroform
Location ' L)
LO Influent 2/13/96 I.I 1--==---------11--~~---1 2/14/96 1.3
2/14/96
2/14/96
2/14/96
1.6
--·--· --------------------·---------2/15/96 1.2 -----~----·----2/ I 6/96 3.3
2/22/96 2.5 --------2/28/96 1.2
2/28/96 -----------·---
I, I -Dichlorocthanc
(ug/L)
80
I IOE
80
94E
64
82
95
5.8
9][
92
3/8/96 2 1111 -·----·-----ll--4/3-/9-6 --------79
1---------11--'5'-'/3"-/9:..:6:_11 __ -:__-:__-:__-:__-:__-1 · ----• -1 ·1
6/5/96 67 -------11-~,-.c,~11------1--------··--8/1/96 83 l---------ll-c-lccl/cc7/"'976-II------I ----69-
3/12/97 66-
LO Effluent 2/13/96 ------ll-2~/-14-/9-6c-ll------------------
--------ll·-2c:1c-14cc/cc96c-ll-----l-------
2/15/96 ·----------ll~2cc/1~6-;:/9~6-ll·----
1---------ll--c2-;:/2:::2-c/9c:6~II------I
2/28/96
3/8/96
•
1.1 -Dichloroethenc --(ug/L)
33 --~----43
13
39
16
32
35
100
33
35
47
36
JO
32
21 ·
------11-------------4/3/96
5/3/96 1---------11-__c_'----'-c_l_ -----1------·-------8/1/96 -------ll·-cc=~-11-----··------·--·--· 10/1/96 ------ll-c-l :-CI/CC7/"'976-II--------. ----···
1----------------11----12/5/96 ll--1~/6c-/c-9-7-II------------
-------I -3/-1-2/-97------
Remediation Pcrfonnance Stamlard
Note: A blank means below detection limit
3500 7
Cis/ir:ms-1.2-Dichlorocthcnc
(ug/1.)
1.8
2.1
1.7
2.(1
1.7
I.I
_!'-'i:!!l_!?~cne chloride
(ug/L)
•
I, I, I-Trichloroethane
(ug/L)
40 ------·l----3c:7~---1
·---·--------------1 15 ----------~~---1 1.7 39
2.5 18
29
l 1
54
30 30c-----l
34
28
40
23 .
-----··---1--------1
.. ----·----------1--------1
--·------1-------1
-.. --·-----------1
711 5 200
•
~~l~pJc ______ _ __ Date Tric_hlorocthylenc.
Location (ug/L)
Benzene
(ug/L)
Tol111.:1h:
(ug/1.)
LD lnl1uent 2/13/96 6.4 ----------2/14/96 8.6
-211-4/96-II---
I--------------------------------------2/14/96 9 -------------------·11---~~-----·-··---2/14/96 6.6 ------11--cc==-11----oc-c----·--------2/15/96 8.4 ---------------11-"-'=-'--II----"-------------· 2/16/96 8.7 ------------------11-==c-ll---c-c----------2/22/96 5.2 1.8
2/28/96 7.4 ---------•11-~~~-11----~--2/28/96 6.4 -------------3/8/96 6. 7
----·---------·----------· 4/3/96 6.6 --------·-···----513196 5.4
6/5/96 5.2 -------------------·
8/1/96 5.9 -----------·----11-------------·--· 11/7/96 5.8
3/ 12/97
LD Effluent 2/13/96 ------ll--2-/-1-4/~9-6_11 ______ _
2/14/96 --------11-----JI-------------2/15/96
2/16/96 · · ·----------ll--c2cc12'"2cc19cc6~11-------I----I
l---------11-==-'--11-------1---------·----2/28/96 -------11-==~11-------1---------3/8/96
4/3/96
5/3/96 ---------ll--=-g/ccl-::c/9:-c6-II---------------------
I 0/1 /96 ll-~=c-11-----------11/7/96
12/5/96 ------------------11-----11----·------l/6/97
-Jti2FJ1
Remediation Pcrfomiance Standard 2.8
Noti:: A blauk 111eans below dete~tion limit
17
8.3
iu
6.5
5.3
4.3
13
1.3
3A
IOIIII
•
Tot;il_Xy\cnes_ Cbromi111n
(ug/L) (ug/1.)
3.4
400. 50
I l;iri11111
(ug/L)
II,
70
]()00
i\·\a11ga11t:sc
( ug/L)
260
250
2,1()
200
190
2,10
120
1)5
I (10
(13
230
110
230
7(1 •
13
11
35
I,
50
Zinc
(ug/L)
270
120
110
84
81
•
Ca<lmium_ -~~pended Solids
(ug/L) (mg/L)
240-------i--------i
77
200
46
0.91
5
------------:1-:-1---I
-------------1--------1
----------1----
0.56
---·-· ·-·-··-1-------1
19 -----------1
51100 5
• • •
Location
UMSA Influent 2/13/96 15 14 19 16 5.9 25
2/14/96 I.I 14 II 10 7.3 7.2 10
2/14/96 II 14 II 17 6.1 17
2/15/96 12 14 II 18 5.9 16
2/16/96 7.5 21 17 14 9.7 25
2/17/96 9.7 18 16 II 7 24
2/22/96 I.I 10 17 16 15 7.6 25
2/28/96 9.8 16 13 12 5.8 21
3/8/96 7.6 10 10 7.7 4.1 16
4/3/96 5.5 16 8.5 7.4 5.4 18
5/3/96 4.8 12 6.9 5.7 12
6/5/96 8.7 22 6 6 13
7/1/96 3.8 II 6.9 4.8 4.3 12
7/30/96 7.9 15 10 6.4 4.2 13
11/7/96 7.2 9.2 7.5 2.3 3.4 10
2/4/97 3.0 27 7.8 2.3 8.8 15
(DUP) 2/4/97 2.4 25 6.2 1.8 7.9 14
UMSA Enluenl 2113/96
2/14/96
2/14/96
2/15/96
2/16/96
2/17/96
2/22/96
2/28/96
3/8/96
4/3/96
5/3/96
6/5/96
7/1/96
7/30/96
9/4/96
I 011196
11/7/96
12/5/96
116197
2/4/97
3/12/97
Remediation Performance Standard 3500 7 70 200 2.8
Note: A blank means below drtection limit
DUP. duplicate
•
("g/1.)
IJMSA lnllm:nt 2/13/96 1--------11-----1-------------· 1.9
2/14/96 1.5 ------ll·-c-2/"14cc/cc96c--l-----l-------·-···-·
l--------;1-~2/c.:l75/,c9.:..6_f----+-~l~.3-I-----·-.. -
~2,i-6/-961----
-------11---'==-1-------------
1 ________ 11 _ __.c2/c.:l.c7/c:9.::.6_1 ___________ --·
2/22/96 ·--------ll--2-,2-8196·1-----1
ll--cJc:c1s'=19'=6~1~---
-------,1-~~~-1----·----------
1--------11--4/3_/_96_1---
5/3/96 ------------------------· -·--6/5/96 I. I .... ------·
7/1/96
7/30196
1117196
4.5
2
==-----11-214_19_7 -------(OUP) 2/4197
Ul'v1SA Efllucnt 2/13/96
_______ 11 _ __.c2/c.:l..c4/c:9.::.6_1. _____ 1 ·-·-----·
2/14/96
------------
----·-------------
2115/96
2/16196
2117/96
2/22/96
2/28/96
318/96
4/3/96 ·-----ll-5-/3-19_6 __ -----·
J.6
6/5/96 2.9 1--------11---------· ~-------·-7/1/96
7/30/96 -------111-cc-91cc41cc9c-6-1-------
l-------ll-71 O~l-'l/c'96c--l-----------
l-------ll--'1"11"7/c'-96'---1---------. ---
1-------11-=c-c-'-I-------·---
-------lll-"12cc1':..:-l.:..96c___1 _____ I-·-----. -----
l---------ll-"1/::::61.c:9.:._7---l-----l-----______ _
2/4/97 I-------H-cc-3/"12"'1cc97=-I---------·-·--
Remediation Performance Standanl
Nore: A blank means below detection limit
DUI' -duplicate I I ---·-·1··--
1000
•
(ug/L) (ug/1.)
140
110 --------110 ------·-· 100 . ---------120 -----·----110 ----------· 120
130
130
110
97
]J()
11 110
130
140
150 -.,_
140
16 150
110 ·---------110 -------100
130
120
120
130
120
110
120
130
12 I 10 ·------200
II 170
130 ··-------. 140 ·-------170 -------200 ---1600 --~-----· , 130
50 1000
--1-
(ug/L)
]00
! 8()
160
l•IO
I(,()
110
(i;i
52
ll
'.!.7
21
I'/
13
1:,
9.8
20
17
330
190
!(10
1-10
170
I.~()
7ll
:'ii
37
'".!. 7
26
22
Is
I 10
68
13
13
17
46
29
· 30
50
Mercury Suspended_ Solids
(ug/1.) (ug/1.) (ug/L) (ug/L) (mg/L)
55 3.5 21
20
74
20
-II
26
25
5000
0.4 7
8.2
-t.2
9.2
66
3.5
15
·----1-------1
·-· ·-----1------1 0.22
5
---·----1--------1 0.26 18
5
6
23
16
24 . -·---·1--~2'c6~--1
5
120
8
I. I
-1----j-~-1---~-1
•
• • •
UM Influent 2/21/96 II ll
2122196 IO l.9 1.5 S.S 12 16
'2122196 6 4.1 1.6 S.8 4.8 12 IS
2/2)/96 4.S 1.6 6.4 4.8 12 12 ~ 1.4 4.6 1.8 6.4 6 14 9.7
2/2S/96 1.2 2.2 66 6.9 IS 9.2
2/28/96 J.S S.8 1.4 8.6 s 14 2.9 ~ 4.7 I 86 J.8 12
J/16/96 S.S 1.8 9.2 4.6 12
4/J/96 4.4 1.6 66 4 IO ~ 4.9 1.8 7.7 9.8 J.2 ~ J.8 LI 6.1 J.l 7.6
7/30/96 4.1 2.1 86 l.l 9.8
Jln/96 S.J 1.9 6.6 2.l 8.J
V4f91 '·' 1.6 7 2.S 8.2
LM Influent 2/21/96 17 IS S.S 2.1 LI 7.6 2.2 9.J
2/22/96 IS " 84 l.l 1.7 II 3.2 12
2/22/96 14 26 9.1 44 2 14 J.J IS
2/23/96 ll 29 II 49 2.1 IS J.6 18
2/24196 8.9 JO ll 4.9 2.7 17 4.S 17 ~ 8.2 31 ll s 2.6 17 4.4 IS
Z/28/96 l l2 IS S.6 2.4 17 4.2 ~ 9.S 1.6 2.4 2.S LI ~ 8.1 1.8 2.4 ).4 1.4 ~ 7.l 2.6 2 l 4 4.7 ~ 8.6 2.7 2.9 4.2 4.6
6/5/96 12 4.7 ·14 S.J 4.9 4.6
7/30/96 17 66 6.7 4.1
11/7/96 II l.l 2.2 S.2 4.S
214/97 1.6 9.8 2.1 l.4 4.4 l.7
COUP) 214191 LS 9.0 1.8 2.1 l.8 l.l
UA. Effiuent 2/21/96
2/22/96 1.8 16
2122196
212)/96
1124/96
2/25/96
2128/96 ~
3/16/96
4/3/96 1.8 1.6 1.9
513196
615/96
711/96 2.1
7/J0/96
9/4/96
10/1/96
11/7/96
12/5/96
11619'1
2/4/97
3/12197
Remediation Perfonnance Standard JSOO 70 200 2.8 1000
Noto, A bl.o.nl. muns b<lo" dc1cction limil
DUJ'. duplicate
•
Sample
Loca1ion
UM Influent
•
:A>·· ·······•··•·• ......
Date Chromium Barium ManRtnc:se Zinc Lead Sus dcd Solids
(u'(.11) '" '" (u<rll) (u-n) (mQ/l)
2/21/96 13 12 SB 140
39 2/22/96 .f----t---+--'ic--+-~::-----t---c'7.2 t----------.~212=21°,~6 4.8 \JO
36 120
2/231% ~---t---+-7.e-+-~::-----t---c'· t----------.~:zn=,,,.=, ). i--------t-cc21""",,.,,-+---f----t---,a--t----i;;;--t----s,.
JI 110
JO 110
1/28/96
3/8/96
28
18
13
110
'° 50
3/16196 •----t---+-~-+--cc~-t-~c--t--~~--1 t----------.~,"n"l96~' JO 20 50
') 26
6/5/96 \) 22
7/1/96
7/30/96
I In/96 .f----j--,,-+---+----j------1------j .-----------~2/"4"~;;7,--36
LM Influent
(DUP)
U/L Effiuent
2/21/96
1122/96
2/22/96
2/23/96
2/251%
2/28/96
3/8/96
3/16/96
413/96
513196
615196
7/30/96
lln/96
2/4/97
2/4197
2/21/96
2/22/96
2122/96
2/23/96
2/24/96
2/25196
2/28/96
J/8/96
3/16/96
4/J/96
S13196
615196
7/1/96
7/30/96
9/4/96
JOll/96
11n/96
12/5/96
J/6/97
214/97
3/12197
Rcmedi11ion Performance Standard
NO!<: A blank""'""' btlow d<uctioq limil
DUP -d"Jllic•te I
68
70
77
81
86
86
JOO
24
H
H
" 130 70
72
80
SJ
90
JI
39
50 1000
I JO 120 S.\ IS
120 120 5.6
\JO 120 S.S
140 130
160 160 '·' 160 160 ) 2
150 240 JJ
72 52 7
53 57
72 " 7
JI 27
21 " 20 6
6.4
19
16
JOO 98 ' 120 120 5.2
120 120 5.7
J<O \JO ,.,
150 150 3.7
160 170 36
32 " 39 56
JI SI
54 ) 6 JO
JO 21
7.S
"
5000 IS
•
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irrninger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
LOG NO
71454-1
71454-2
71454-3
71454-4
71454-5
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
Pagel
DATE/
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/1130
03-12-97/1115
PARAMETER 71454-1 71454-2 71454-3 71454-4 71454-5
-------------------------------------------------------------------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
<1.0
<1.0
<1.0
ug/1 <1.0
<2.0
<1.0
<1.0
<1.0
<1.0
87 %
03.19.97
1.0
0318A
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
82 %
03.19.97
1.0
0318A
<1.0
<1.0
<l.O
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
85 %
03.19.97
1.0
0318A
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
83 %
03.19.97
1.0
0318A
<5.0
66
21
<5.0
<10
<5.0
23
<5.0
<5.0
86 %
03.20.97
5.0
0318A
Clock ID 1B0319 1B0319 1B0319 1B0319 1B0320
----------------------------------------------------------- --------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach .. FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
Project: 190-00001-0l/MACON DOCKERY
Sampled By: Client
Code: l 75970321
REPORT OF RESULTS Page 2
DATE/
LOG NO
71454-l
71454-2
71454-3
71454-4
71454-5
SAMPLE DESCRIPTION, LIQUID SAMPLES
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/l-130
03-12-97/1115
PARAMETER 71454-l 71454-2 71454-3 71454-4 71454-5
-------------------------------------------------------------------------------
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -
a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
<1.0
<1.0
<3. 0
<10
83 %
03.19.97
1.0
0318A
lB03l9
130
03.14.97
03.17.97
l.0
0314M
<l.0
<1.0
<3.0
<10
97 %
03.19.97
1.0
0318A
1B0319
<50
03.14.97
03.17.97
1.0
0314M
<1.0
<1.0
<3.0
<10
97 %
03.19.97
1.0
0318A
1B0319
69
03.14.97
03.17.97
l.0
0314M
<1.0
<1.0
<3.0
<10
97 %
03.19.97
l.0
0318A
1B0319
70
03.14.97
03.17.97
1.0
0314M
<5.0*F34
<5.0
<15
<50
93 %
03.20.97
5.0
0318A
1B0320
<50
03.14.97
03.17.97
1.0
0314M
--------------------------------------------------------------------- ----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
REPORT OF RESULTS Page 3
LOG NO
71454-1
71454-2
71454-3
71454-4
71454-5
PARAMETER
Beryllium
Beryllium
(6010)
(6010),
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmium (7131)
SAMPLE DESCRIPTION, LIQUID SAMPLES
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
71454-1
----------
ug/1 <5.0
03.14.97
03.17.97
1.0
0314M
71454-2 71454-3
--------------------
<5.0 <5.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1. 0
0314M 0314M
Cadmium (7131), ug/1 <0.30 <0.30 <0.30
Preparation Date 03.14.97 03.14.97 03.14.97
Date Analyzed 03.19.97 03.19.97 03.19.97
Dilution factor 1.0 1.0 1.0
Batch ID 0314Z 0314Z 0314Z
Chromium (6010)
Chromium (6010), ug/1 <10 <10 <10
Preparation Date 03.14.97 03.14.97 03.14.97
Date Analyzed 03.17.97 03.17.97 03.17.97
Dilution factor 1.0 1.0 1. 0
Batch ID 0314M 0314M 0314M
------------------------------
DATE/
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/1130
03-12-97/1115
71454-4 71454-5
--------------------
<5.0 <5.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<0.30 <0.30
03.14.97 03.14.97
03.19.97 03.19.97
1.0 1.0
0314Z 03142
<10 <10
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1. 0
0314M 0314M
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
71454-1
71454-2
71454-3
71454-4
71454-5
PARAMETER
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
71454-1
---------------------------------------
Manganese (6010)
Manganese (6010), ug/1 30
Preparation Date 03.14.97
Date Analyzed 03.17.97
Dilution factor 1.0
Batch ID 0314M
Nickel (6010)
Nickel (6010) , ug/1 <40
Preparation Date 03.14.97
Date Analyzed 03.17.97
Dilution factor 1. 0
Batch ID 0314M
Lead (7421)
Lead (7421), ug/1 <3.0
Preparation Date 03.14.97
Date Analyzed 03.17.97
Dilution factor 1.0
Batch ID 03142
---------------------------------------
71454-2 71454-3
--------------------
<5.0 <5.0
03.14.97 03.14.97
03.17.97 03.17.97
1. 0 1.0
0314M 0314M
<40 <40
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<3. 0 <3.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
03142 03142
--------------------
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/1130
03-12-97/1115
71454-4 71454-5
--------------------
<5.0 76
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<40 <4 0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<3.0 <3.0
03.14.97 03.14.97
03.17.97 03.17.97
1. 0 1.0
03142 03142
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO, S7-71454
Received: 14 MAR 97
Reported, 21 MAR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
71454-1
71454-2
71454-3
71454-4
71454-5
PARAMETER
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
71454-1
----------
Antimony (7041)
Antimony (7041), ug/1
Preparation Date
<10
03.17.97
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium, ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Zinc (6010)
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution .factor
Batch ID
03.20.97
1. 0
0317K
<50
03 .14. 97
03.17.97
1.0
0314M
<20
03.14.97
03.17.97
1.0
0314M
----------
71454-2 71454-3
--------------------
<10 <10
03.17.97 03.17.97
03.20.97 03.20.97
1. 0 1.0
0317K 0317K
<50 <50
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<20 <20
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
--------------------
Page 5
DATE/
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/1130
03-12-97 /1115
71454-4 71454-5
--------------------
<10 <10
03.17.97 03.17.97
03.20.97 03.20.97
1.0 1.0
0317K 0317K
<50 <50
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
<20 <20
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO, S7-71454
Received, 14 MAR 97
Reported, 21 MAR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 6
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
71454-1
71454-2
71454-3
71454-4
71454-5
PARAMETER
UMSA Effluent
U/L Macon Effluent
Upper Dockery Effluent
Lower Dockery Effluent
Lower Dockery Influent
71454-1
---------------------------------------
Suspended Solids (160. 2)
Suspended Solids (160. 2), mg/1 <5.0
Preparation Date 03.14.97
Date Analyzed 03.17.97
Dilution factor 1.0
Batch ID 0314C
---------------------------------------
71454-2 71454-3
--------------------
<5.0 <5.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314C 0314C
--------------------
DATE/
TIME SAMPLED
03-12-97/0847
03-12-97/0940
03-12-97/1035
03-12-97/1130
03-12-97 /1115
71454-4 71454-5
--------------------
<5.0 <5.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314C 0314C
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO, S7-71454
Received: 14 MAR 97
Reported, 21 MAR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Client PO. No., 190-00001-0l
Project, 190-00001-0l/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 7
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-6 Trip Blank
-----------------------------------------------------------------------------------
PARAMETER 71454-6
Purgeable Halocarbons (8010)
Chloroform, ug/1
l,l-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Date Analyzed
Dilution factor
Batch ID
Clock ID
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -
a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
<1.0
<l.0
<l.0
ug/1 <l.O
<2.0
<1.0
<1.0
<l.0
<1.0
03.20.97
l.0
0318A
lB0320
<1.0
<1.0
<3. 0
<10
103 %
03.19.97
1.0
0318A
lB0320
Laboratories in Savannah, GA • Tallahassee. FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
LOG NO, S7-71454
Received: 14 MAR 97
Reported, 21 MAR 97
•
•
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
·Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page B
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-11
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71454-7 71454-8 71454-9 71454-10 71454-11
-------------------------------------------------------------------------------
Purgeable Halocarbons (8010)
Chloroform, ug/1
1,1-Dichloroethane, ug/1
1,1-Dichloroethene, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
(Dichloromethane), ug/1
Tetrachloroethene, ug/1
l,l,1-Trichloroethane, ug/1
Trichloroethylene, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
ug/1
1.0
1.0
1.0
1.0
2.0
1.0
1. 0
1.0
1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
82 %
03.19.97
1.0
0318A
1B0319
26
27
87 %
03.19.97
1.0
0318A
1B0319
----------
23 20
26 20
77 %
03.20.97
1.0
0318A
1B0320
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO, S7-71454
Received, 14 MAR 97
Reported, 21 MAR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
--------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-11
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
Page 9
-----------------------------------------------------------------------------------
PARAMETER 71454-7 71454-8 71454-9 71454-10 71454-11
----------------------------------------------------------- --------------------
Purgeable Aromatics (8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
1.0
1. 0
3.0
10
<1.0
<1.0
<3.0
<10
107 %
03.19.97
1.0
0318A
lB0319
23
24
103 %
03.19.97
1.0
0318A
180319
20
21
100 %
03.20.97
1.0
0318A
lB0320
20
20
Barium (6010)
•
Barium (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
50 <50
03.14.97
03.17.97
1.0
0314M
----------
1860 1860 2000
03.14.97 03.14.97
03.17.97 03.17.97
1. 0 l.O
0314M 0314M
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
REPORT OF RESULTS Page 10
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-11
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71454-7
Beryllium (6010)
Beryllium (6010), ug/1
• Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cadmium (7131)
Cadmium (7131), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Chromium (6010)
Chromium (6010), ug/1
Preparation Date
•
Date Analyzed
Dilution factor
Batch ID
5.0
0. 3 0
10
71454-8
----------
<5.0
03.14.97
03.17.97
1.0
0314M
<0.30
03.14.97
03.19.97
1.0
0314Z
<10
03.14.97
03.17.97
1. 0
0314M
----------
71454-9 71454-10 71454-11
------------------------------
44.l 43.9 so.a
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
5.18 5.18 5.00
03.14.97 03.14.97
03.19.97 03.19.97
1.0 1.0
0314Z 0314Z
176 177 200
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irrninger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
Client PO. No.: 190-00001-01
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
REPORT OF RESULTS Page 11
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-11
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER
Manganese (6010)
Manganese (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Nickel (6010)
Nickel (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Lead (7421)
Lead (7421), ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
71454-7
----------
5.0
40
3.0
----------
71454-8
----------
<5.0
03.14.97
03.17.97
1.0
0314M
<40
03.14.97
03.17.97
1.0
0314M
<3.0
03.14.97
03.17.97
1.0
03142
----------
71454-9 71454-10 71454-11
------------------------------
467 466 500
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
481 481 500
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314M 0314M
52.3 51.7 50.0
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
03142 03142
------------------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
LOG NO,
Received:
Reported,
S7-71454
14 MAR 97
21 MAR 97
Applied Earth Sciences, Inc. Client PO. No., 190-00001-0l
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Project, 190-00001-0l/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 12
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-ll
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71454-7 71454-8 71454-9 71454-10 71454-ll
-------------------------------------------------------------------------------
Antimony (7041)
Antimony (7041), ug/1
• Preparation Date
Date Analyzed
Dilution factor
Batch ID
Vanadium (6010)
Vanadium, ug/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Zinc (6010)
•
Zinc (6010), ug/1
Preparation Date
Date Analyzed
Dilution factor
~atch ID
10
50
20
<10
03.17.97
03.20.97
l.O
0317K
<50
03.14.97
03.17.97
l.O
0314M
<20
03.14.97
03.17.97
l.O
0314M
----------
47.8 49.7 50.0
03.17.97 03.17.97
03.20.97 03.20.97
l.O l.O
0317K 0317K
442 440 500
03.14.97 03.14.97
03.17.97 03.17.97
l.O l.O
0314M 0314M
476 474 500
03.14.97 03.14.97
03.17.97 03.17.97
l.O l.O
0314M 0314M
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
•
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
LOG NO, S7-71454
Received: 14 MAR 97
Reported, 21 MAR 97
Client PO. No., 190-00001-01
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 13
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-7
71454-8
71454-9
71454-10
71454-11
Practical Quantitation Limit
Method Blank
Lab Control Standard (LCS) Result
LCS Duplicate Result
LCS Expected Value
-----------------------------------------------------------------------------------
PARAMETER 71454-7 71454-8 71454-9 71454-10 71454-11 -------------------------------------------------------------------------------
Suspended Solids (160.2)
Suspended Solids (160.2), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
5.0 <5.0
03.14.97
03.17.97
1.0
0314C
----------
101 103 100
03.14.97 03.14.97
03.17.97 03.17.97
1.0 1.0
0314C 0314C
--------------------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Steve Irminger
LOG NO,
Received:
Reported,
S7-71454
14 MAR 97
21 MAR 97
Applied Earth Sciences, Inc. Client PO. No., 190-00001-01
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Project, 190-00001-01/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 14
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-12
71454-13
71454-14
LCS/LCSD % Recovery
LCS Control Limits
Method Blank
-----------------------------------------------------------------------------------
PARAMETER
Purgeable Halocarbons (8010)
1,1-Dichloroethene, ug/1
Trichloroethylene, ug/1
Chloroform, ug/1
•
1,1-Dichloroethane, ug/1
Cis/Trans-1,2-Dichloroethene,
Methylene chloride
{Dichloromethane), ug/1
Tetrachloroethene, ug/1
1,1,1-Trichloroethane, ug/1
Vinyl chloride, ug/1
Surrogate -Bromochloromethane
Date Analyzed
Dilution factor
Batch ID
Clock ID
71454-12
130/115 %
135/130 %
ug/1
71454-13
10-232 %
28-196 %
71454-14
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
76 %
03.20.97
1.0
0318A
1B0320
-----------------------------------------------------------
•
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S7-71454
Received: 14 MAR 97
Reported: 21 MAR 97
•
Mr. Steve Irminger
Applied Earth Sciences, Inc. Client PO. No.: 190-00001-01
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Project: 190-00001-01/MACON DOCKERY
Sampled By: Client
Code: 175970321
REPORT OF RESULTS Page 15
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-12
71454-13
71454-14
LCS/LCSD % Recovery
LCS Control Limits
Method Blank
-----------------------------------------------------------------------------------
PARAMETER 71454-12 71454-13 71454-14
-----------------------------------------------------------
Purgeable Aromatics {8020)
Benzene, ug/1
Toluene, ug/1
Total Xylenes, ug/1
Acetone, ug/1
115/100 %
120/105 %
Surrogate -a,a,a-Trifluorotoluene
Date Analyzed
Dilution factor
Batch ID
Clock ID
Barium (6010)
Barium (6010)
Beryllium (6010)
Beryllium (6010)
Cadmium (7131)
Cadmium (7131)
Chromium (6010)
Chromium (6010)
Manganese (6010)
Manganese (6010)
Nickel (6010)
Nickel (6010)
93/93 %
88/88 %
104/104 %
88/88 %
93/93 %
96/96 %
----------
23-168 %
33-167 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
80-120 %
----------
<1.0
<1.0
<3.0
<10
103 %
03.20.97
1.0
0318A
180320
----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
1·
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
• 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO, S7-7l454
Received, 14 MAR 97
Reported, 21 MAR 97
LOG NO
Mr. Steve Irminger
Applied Earth Sciences, Inc.
6525 The Corners Parkway, Suite 400
Norcross, GA 30092
Client PO. No., 190-00001-0l
Project, 190-00001-0l/MACON DOCKERY
Sampled By, Client
Code, 175970321
REPORT OF RESULTS Page 16
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
-----------------------------------------------------------------------------------
71454-12
71454-13
71454-14
LCS/LCSD % Recovery
LCS Control Limits
Method Blank
-----------------------------------------------------------------------------------PARAMETER 71454-12 71454-13 71454-14
------------------------------
Lead (7421)
Lead (7421)
Antimony (7041)
Antimony (7041)
.Vanadium (6010)
Vanadium
105/103
96/99
88/88
% 80-120 %
% 80-120 %
% 80-120 %
Zinc (6010)
Zinc (6010)
Suspended Solids (160.2)
Suspended Solids (160.2)
Methods, EPA SW-846
95/95 %
101/103 %
----------
80-120 %
75-125 %
--------------------
*F34 = Due to the abundance of organics in the sample, dilution was required.
Lisa G. McLeod, Project Manager
• Final Page Of Report
Laboratories in Savannah, GA • Tallahassee, FL • Tampa. FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA
•
llLLING CONTROL NUMBER (FOR LAB USE ONLY)
FOR LAB USE ONLY AC(#
•
.elinquishcd by: (Signature)
elinquished by: (Signature) •
SAMPLE DESCRIPTION
U M .s, A-
u
£.ffi(fe1
-;-12--17
f-
Received by: (Signature)
Received by: (Signature)
Date/ Time Received by: (Signature)
Dace/ lime Received by: (Signature)
PROJECT •
I/ :J
I;, ' .
{lv;,,'J
"' "' "' 0
A_
X
1'A
X
'f-
"
• .
-o
2960 Foster Creighton Drive
Nashvil!e, TN 37204
615-726-0177
FAX [phone]
P.O.,
ANALYSIS REQUESTED
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