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HomeMy WebLinkAboutNCD980840409_19961210_Charles Macon Lagoon & Drum_FRBCERCLA RA_Monthly Progress and O & M Report November 1996-OCRI I R I I I m I I I I I I I I I I I I RECEIVED DEC 131996 SUPERFUNO SECTION MACON/DOCKERY SITE CORDOVA, NORTH CAROLINA MONTHLY PROGRESS AND O&MREPORT NOVEMBER 1996 6525 The Corners Parkway, Suite 400 • Norcross, Georgia 30092 • Tel: (770) 448-4911 • Fax: (770) 409-7893 B R I I I I I I I I I I I I I I I December I 0, 1996 Ms. Giezelle Bennett Remedial Project Manager US EPA, Region IV 345 Courtland Street Atlanta, Georgia 30365 Re: Macon/Dockery Site -Cordova, North Carolina Monthly Progress and O & M Report -November 1996 Dear Ms. Bennett: On behalf of the Macon/Dockery Site Group ("Group"), the November 1996 Monthly Progress and 0 & M Report is herewith submitted in accordance with SECTION XV -PROGRESS REPORTS of the Unilateral Administrative Order ( effective date a June 30, 1992) for the Macon/Dockery Site. This report describes activities which occurred during the month of November as part of the Remedial Design and Remedial Action phase of this project. PROJECT TASKS INITIATED OR COMPLETED THROUGH NOVEMBER 1996: • • Quarterly sampling of the twelve monitor wells and remediation systems Continue O & M of systems . RES UL TS OF SAMPLING AND TESTING AND OTHER DAT A RECEIVED: • Laboratory results for November sampling of the remediation systems is included in this progress report. Tables I to 4 record the analytical results for the four groundwater treatment systems. The acetone concentration of 2, I 00 µg/L in the influent at Upper Dockery was confirmed by GC/MS by Method 8260 at a concentration of 150 µg/L. All effluent concentrations are below the Remediation Performance Standard. • Table 5 records the analytical results for the 12 monitor wells. • Table 6 records the air quality sampling. All systems were below detection limits. • Table 7 records all groundwater elevations taken since system start up. All planned monitor wells and recovery wells were gauged except for MW-8 and MW-8A, which were covered by vegetation. Water levels were generally higher at Upper Dockery and Macon Source Area. 6525 The Corners Parkway, Suite 400 • Norcross, Georgia 30092 • Tel: (770)° 448-4911 • Fox: (770) 409-7893 D I n H D I I I I I I I I I I I I I I • Upper Dockery flow meter reading for November totaled 438,013 gallons. System was operational I 00% of the time averaging 11.7 GPM. Mass voe removal was 1.62 pounds for the month and the cumulative is 4.28 pounds. • • Lower Dockery flow meter reading for November totaled I 83,210 gallons. System was operational 93% of the time averaging 4.9 GPM. Mass voe removal was 0.22 pounds for the month and the cumulative is 2.50 pounds. Macon Source Area flow meter reading for November totaled 116,354 ga]lons. System was operational 100% of the time averaging 3.1 GPM. Mass voe removal was 0.04 pounds for the month and the cumulative is 0.89 pounds. • Upper/Lower Macon flow meter reading for November totaled 871,155 gallons. Combined system was operational 100% of the time averaging 23.3 GPM. Mass VOC removal was 0. I 8 pounds for the month and the cumulative is I. IO pounds. TASKS PLANNED FOR DECEMBER 1996: • Monthly sampling of the remediation systems effluent • Continue O &M of systems • Check Upper Dockery gallery. overflowing The gallery has been taking all of the effluent water and not PROBLEMS AND DELAYS: • • November 8 -SVE system was down due to high level in moisture separator. Drained and restarted system. The SVE timer was set to shut off for 15 minutes during the day to allow the moisture separator to drain. The system has not gone done since the timer was re-set. November 14 -Lower Dockery system down due to high level in the stripper sump. Drained the sump and restarted. I u u D I u I I I I I I I I I I I • Percent operational for each system: Upper Dockery Lower Dockery Upper Macon Lower Macon Macon Source Area SVE system Respectfully Submitted, )<cv,~/J -::s-. 0.J.J~c.,___ £,. /12_,._"-'-( C,/f.Jp-- Kenny Gulledge Project Coordinator cc: Macon/Dockery Site Group Members Paul Furtick, RMI, Inc. Ms. Norma Eichlin, COM Federal Programs David Lown, NC Super Fund Section 100% 93% 100% 100% 100% 93% ----1111!!9 I!!!!!!! 1!11!1 Im == Location (,g/L) UD Influent 2/13/96 4.8 !50E 1.3 1.3 54 8 2/13/96 7.7 130 33 2/14/96 4.3 89E 1.2 55 4.5 2/14/96 6.5 100 34 5.3 2/14/96 4.4 120E 1.4 1.3 50 7.9 2/14/96 4 110 48 7.8 2/15/96 4.5 130E 1.2 1.4 54 8.3 2/15/96 5.5 140 2 56 8.6 2.8 2/16/96 7.5 160 64 10 2/17/96 5.7 !SOE 1.7 2.1 62 9.4 2/17/96 5.5 120 42 6.4 2/22/96 5.4 150E 1.4 52 5.7 2/22/96 4.9 96 48 5.5 2/28/96 6.4 200E 1.9 19 5.3 2/28/96 6.8 240 50 3/8/96 5.2 l J0•F35 1.7 55 3.8 4/3/96 3.6 160E I.I 1.6 38 5.6 4/3/96 92 25 3.9 5/3/96 4 130 38 4.8 6/5/96 2 110 5.2 2.8 7/1/96 2 77 25 3.6 8/1196 6.1 220 52 5.7 1117/96 240 54 11/7/96 UD Effiuent 2/13/96 2/14/96 2/14/96 2115196 2/16/96 2/17/96 2/22/96 2/28/96 3/8/96 4/3/96 5/3/96 6/5/96 3.9 7/1/96 8/1/96 9/4/96 10/1/96 1117/96 Remediation Performance Standard 3500 7 70 200 2.8 1000 Note: A blank mearu; below detection limit Note: • Acetone oonlinned by Method 8260 -----1!!11!!!1 B!!!!I 1!11!1 -l!EI Location (,g/L) (,g/L) UD lnnuent 2/13/96 3,J 20 92 64 33 3.1 51 2/13/96 2/14/96 12 53 14 52 2/14/96 2/14/96 II 54 14 2/14/96 2/15/96 19 81 53 2/15/96 2/16/96 II 57 II 2/17/96 55 12 2/17/96 2/22/96 13 I 3 2/22/96 2/28/96 II 7.7 2/28/96 318196 8 4/3/96 11 52 4/3/96 5/3/96 16 58 615196 7/1/96 5 8/1/96 II 5.5 JO 11/7/96 2100 19 61 9.5 11/7/96 150• UD Effiuent 2/13/96 70*F32 16 71 40 22 14 2/14/96 35*F33 I 5 53 14 11 2/14/96 11 56 12 2/15/96 12 53 14 2/16/96 53 11 2/17/96 11 55 12 2/22/96 8.3 2/28/96 13 9.6 JO 3/8/96 25 6.9 4/3/96 28 11 50 5/3/96 52 6/5/96 7/1/96 811/96 20 14 5 I 7 8 9/4/96 55 10/1/96 5.9 11/7/96 I 5 59 Remediation Performance Standard 400 3500 50 1000 50 5000 15 Note; A blank means below detection limit , 'ote; • Aeet0ne confirmed by Method 8260 - LD Influent ---- LO Emuent 1111 Oatc Chlorofonn 1, I -Dichlorocthane (ug/L) (ug/L) 2/13/96 I.I 2/14/96 1.3 2/14/96 - . 2/ 14/96 . -----'"1.6 -· 2/14/96 ·2,i 5/96 2/16/96 1.2 3.3 80 !JOE 80 94E 64 -----------·------· 82 95 2.5 5.8 2/28/96 2(28/96 1.2 931~ 3/8/96 __ _ 2 "6/5/96 --· 811196---·- ll/7i96 ---- 2/13/96 2/14196 92 I JO 79 71 67 ------·---83 69 l!!!!!!!!I I, I -Dichloroethene (ug/L) 33 39 16 32 35 l!il!!!I Cis/trans-1,2-Dichloroethene --(ug/L) 1.7 26 Methylene chloride --(ug/L) == == I, I, I-Trichloroethane (ug/L) 40 37 39 18 29 31 100 ~ --------------------------·--------·-- ------·----·-----. --------·--------33 JO 35 30 47 36 30 32 27 28 1.7 I. I 2 34 28 40 42 54 38 1-----------11-~2,~1~4,~9~6-11-------l---------l------------l--------------·-----------------------·------ 2/15/96 l----------,e-,-,1~6/~9~6-111------11--------1--------1---------------------------------1------- 2/22/96 l----------lf-------11------1--------1-----------------------1-------2/28/96 ----------10-~--11-------1---------1-----------l-----------··----3/8/96 10/1/96 11/7/96 Remediation Performance Standard 3500 7 70 5 200 Nole: A blank mean~ ~low detection limit 111!1 ---11!111 l!!!!l!!!I &!!l!!!I l!li!!!I == ----------------2114196-6.6 ----··------6.5 ----. -240 ---11~0--I-------- ----------------------------·---------__ J_ ______ _ II----=-----' 2/15/96 8.4 2/16/96-8.7 ·-·s_3 ----i--------i----·-----________ 1-_-_-_--::_2-oo:_:_:_:__=11~--::_--::_--::_-8_4--::_--::_-:__-:--::_--::_--::_--::_--::_-:__-----11---------- 4_3 190 81 2/22/96 5.2 I _8 -1-j -2fifi96-"1_"'4 ___ _j __ -·------ 11----~---2/28/96 6.4 ~Fi6--ll----6-.7------l------------- 1------------------4/3/96 6.6 LD Effiuent 5/3/96 5.4 6/5/96 8/1/96 11/7/96 - 2/13/96 -2114/%"- 5 2 5.9 5.8 1.3 2.5 ---------ll2/14/96" J-----------n-~~--n----------l---------1---- 3.4 14 - -240 -240 16 63 200 0.91 230 46 110 -----·-·-----230 --------i-------1------------------------------·--------2/15/96 l----------+---'2'-'11"-6'-'19-=6-11--------1-----1-----1 ------l----11-----+------I------______ _ 1-----------1----11--------_____ J ___ __J -----1-----1-------------1---------1----2/22/96 -----1-----1-----1------1------l---- 5 II 5 2n8/96 1----------11~3~,8~19~6cc__+--------li-----t-----l-------l-------l-----l-----1----1-----1--------1 i-----------l~-4cc13cc1cc96o--ll---------li----l----+------1-----------I-----I---_______ 1 __________ _ 5/3/96 f----1------------1-------l 8/1/96 ----l-----------f----➔-----~--1~3--t-----l---0~.5~6~-l---- 1----------+~~~-II-----------1------l------l----l-------1--~--_,__ ___ __, __ _.ccc.c_ __ 1 ________ , 10/1/96 11 11/7/96 ---T4---------------------------l------1------0-----1--------1 Remediation Performance Standard 2.8 1000 400 50 1000 50 5000 5 Note. A blank means ~low detection limit l!i!!!!!!I l!!!!!!l!!I !!I!!! Ii=! -----· ______ ·---I, I. I -Trichloroethane Trichlorocthylcne (ug/L) (ug/L) (ug/L) - UMSA Influent 2/13/96 16 5.9 25 --------·-------2/14/96 I.I 7.3 7.2 10 2/14/96 -. 11 14 II 14 14 II ----·------------------------------·---1-----"17____ ____ 6.1 17 2/ I 5/96 ----12 ----111-==~II _I_I ______ 1 ___ __:18 5.9 ---f-----cc-16~--I 7.5 -·21 17 14 9.7·-25 ----2/16/96 9.7 ---------------ff ____ ---------16 ·-----·-----11 --'c.7'------l---~24c___----l =-+-~~--1--------'l'c-O---l------;-:17,.._ --_-_ -_ -_ -_1 1 _--_ -_ -_ -_ -_-_--_ -_ --'--,1~6=========t--l---clcc-5 __ --+ ___ ~7~.6:___ __ -J----2~5:___ __ 1 9.8 16 13 12 5.8 21 2/17/96 2/22/96 I.I 2/28/96 3/8/96 7.6 10 10 7.7 4.1 16 -----,---~~-------------- ~----ilf----------,----5._5 ___ -1 _____ 1_6 -------I----_8_.5____ 1 ____ 7.4 ___ 1 _________ --~~----·--· 18 4.8 12 6.9 5.7 -12 ---- 4/3/96 513196 ----6/5/96 -----7/1/96 7/30/96 8.7 22 ------------------6 --- 10 4.8 6.4 1117/96 15 9.2 7.5 2.3 UMSA Effiuent 2/13/96 --------------------2/14/96 -----2/14/96 -------2/15/96 2/16/96 2/17/96 2/22/96 2/28/96 3/8/96 -----4/3/96 ----513196 6/5/96 7/1/96 7/30/96 ,---------u-~97/4~/9~6~11------------------·---------------------------------------------------lf--- 1---------1>---~~-11-----1-------·-------· -·· ---------------------I0/1/96 1117/96 Remediation Perfonnance Standard 3500 7 70 Note. A blanh means below detection limi1 4.2 3.4 200 13 10 2.8 -- UMSA Effluent --- 7/30/96 4.5 11/7/96 2 I . ---- 2/13/96 16 2/14/96 150 330 ----------------- 110 190 74 20 B!!I !l!!I - 4.2 57 2/14/96 ~-1--------------1-----1-----1---------·--··---··--110 160 --1-----------1------1-----1---·----·--------·-·-· _,_ ______ --·------··------------·-------------·---------2/15/96 100 140 2/16/96 130 170 -0.26 ·fg-------------1------------------------------------------·---------------------2/17/96 2/22/96 2/28/96 ~-1-----1----1-----1-----<---1-2-0 -----~20 -----1---1-----------1-------11------120 70 ---l-----1----1-----1----1----1 ------------------------------130 51 -·-------------------3/8/96 120 37 ----------------------------4/3/96 110 27 5 ----------------5/3/96 120 26 ------6/5/96 2.9 130 22 6 ---7/1/96 12 110 14 ----7/30/96 200 110 41 9.2 23 ---9/4/96 II 170 68 26 66 16 -------I0/1/96 11/7/96 -------+----l----l-------1-----1------1-----1--130 13 0.47 24 140 13 26 Remediation Performance Standard IOOO 50 1000 50 5000 5 15 I. I Note. A blanh means below detec1ion limit ---Iii!!& 11!1!1 l!!lll9 ------------- 2122/96 2n2/96 2nJ196 2(24/96 2/25/96 2/28/96 -318/96 __ _ 1------------___ 6_15_/%_ 7/1/96 7/30/96 lln/96 LM Influent 2/21/96 ----·------· --------ll--271-2271-9'7, -I -znzm-,_ ___ ------i -·inJ/96- --2n-41%-- imm-· 2/28/96 - 318196 -- 3/16/96-- 4/3/96 513196 -- -615/96-- 7130/96 >---------------ll----- U/L Effiuent 11/7/96 2/21/96 2/22/96 2/22/96 10 ' 3.9 4.1 1.6 5.8 4.5 1.6 6.4 1.4 4.6 1.8 6,4 1.2 2.2 6.6 ·-3.5-----5.8 1.4 8.6 ------1----------4.7 1 8.6 1----~-------·- 5.5 1.8 ____ 90.2~----l-------4.4 I 6 ·--·--· 6.6 --------l----~----1-------4~ 1.8 7.7 4.6 ,_, 4_8 4.8 6 6.9 ' 3.8 4.6 3.8 __ -_I~. I~--------------~-c l ____ ___, ________ 1 ___ _c3ec-':_ __ -----1----•-_1 _________ }~!. ------·---------_8~-~·----3.3 5.3 1.9 6.6 2.3 17 " 15 5.5 2.1 1.1 -=--··----------22 14 26 ----jj·--1-----2-9 _____ -------· 8.9 ----· _____ ,._. 8.2 3 30 ---··· ---------·--. 31 32 8.4 3 3 1.7 ------------9.1 4.4 2 11 4.9 2.1 13 4.9 13 ' ,_, . ---·-----2.4 1.8 _____ , ______ ---•------------1-----------1 == 7.6 II 14 " 17 17 17 2., 2f24/% 1----------lf-~,ncc,cc/96~-ll------l-------1------------------•-----------1-------+--------I 1------------11 ~,n=8l~9~6---1,------I------·----1----·------------------1·---·------·------·-------'--- 1--------ll--"c,~~11------------------1------------------- 318196 11-------1----------1------... ----·-3/16/96-- l------------11-4/3196 11-------1 1.8 1---------11--5cc13c-19cc6c---ll--------------------,_ ____ _ 1------------11-'-'5196_11-------~--------1----- ---·-----------16 -----1----------1-------1 1------------11 _1.!J!J..?_11-----1130196 f-------------------1----- 9/4196 --1---------11--~,'c-.lcc,/96~-ll-----1--------1------------------1 -,-117/96 ------------1-------------1 ----------1----- Remediation Performance Scandarcl 3500 70 Noic· A bl;u,k mQttS hclcm dt.1cction limil 200 -----l!!!i!il l!!!!!!I l!!il!I !!Im 1!11111 -- Date I Trichlorocthylene --~~"l':'.'~e~e__ _ Zinc _____ Suspended Solids (u .) (u .) {m ) UM lnlluent 2nl/96 -----. ----------11-~~~ _____ 5_8 -----140 13 12 2/22/96 12 ~ 130 7.2 1----' -------2/22196 2/23/96 ' 12 12 2/24~f6-14 2ill/9& t is 2/28/96 14 -3/8196 ---- --·-12· ----- 3/16/96 12 -4/3196--ro -------------·--· -----------______ ,, ___ 6is196 ____ ,__ 9.s -JT I-----------------·-· f· ·---· ----------------·----- 1-------------11-'!~l_~ _______ 7~~------------------ 7/30/96 9.8 --11/7/96-,___ 8.3 LM Influent 2/21/96 2.2 ------11------9.3 2n2/96 3.2 ---------2/22/96 3.3 36 120 4.8 JI 110 4T __ _ 30 - . I 10 ----··---· -·-------· 3.6 34 68 70 28 110 18 13 20 9.3 40 so ,0 26 22 2/21/96 59 100 98 4 --------------~==~-c---------1----+----l-~---I U/L Effluent 2n2196 130 10 -·-120·--120 -· u-·-- io 13 ·2n2/%-•--------i --------------n-·· 120 120 -s_,-------- 2123/96 80 --,40·-130 ---4_9--l------- ------ll-~=~+--------1-----1-----1-~~-I 2/24/96 83 150 150 3.7 11-~=~ ,-----------------------1------1··-------1--~~--I -=~-,--=---------·------2nS/96 90 160 170 3.6 I--------------- -----------------1-----1--------1--~~-+-~~---l-~~-1 2fl8/96 32 59 ----------01-~~~-1--------------------------------3/8/96 39 56 -----------. ------·---=--1---=~--1 JI 51 8 1----------44 ~ 3.6 IO 1--------~----31 ______ J_~-= =-~-~)i== =~---------_______ , 1--------------11-...!!!~!__ -------1-----=2-~l--1-------·----___ _!_:.5 __ 1----------11--71-11~--'~-------1-----1-----1 ----+-----1-----1-----1-------1 f----------ll-7-B_O~f-------;----l-----~---9/4/96 ------1----1----1----1 f----------lf--"-'1=01c'1196~-+-------l-----f----l----l -----l-----f------l------'2"'4'---1 Jln/96 Remediation Performance Stand:ird 2.8 IOOO ,0 1000 50 5000 15 NOfC. A bb:ll mearu bcl°"' dcu:ction limi1 11!1:1! -B3 m!I I!!!!! Iii!! == 280 120 1----------•-s'~,21~'i''--J-----II---C'~'---I 630 7/JI/% 610 JO 170 210 (DcUP=)'---------11iJi/96 -1------1--------1----•c>cOc_ ___ -----------1----1 ln/% 29 1000 160 ~Q_r)-------- MW 25 ------------- Lower Dock MW16 Macon Source Arca -llh/<lf> --·--1 boo ______ _ viJ/% •-----+---,-,------1-------------------------l---~2c90~---I 1----'•000~---1------·------_____ 1:1_ 5/21% ------7/J I/% --,·in/%- --~---1------------·------------------_______ _, --12---1------~----------------1--------~---------_ -----·-_________ _ -----------·-· -----16 1-------1-------1--------- )6 7.4 22 Z.8 -4,7 ----------20 --------·--------l,c<W= 2 cA-------I ~=-~=========,======~~~======'1-:_-_-_-_-_-c;of=====~-~------_-_-_--~:-~i_-_-__ -_-_·_-_l_-_-_-_-_-_-_-_--___ ·1 J"(_D_UP_)~------Jc-c~'/2/%~~-J•l-----r---'ci----l---clc8 ___ 1-----''~lc_ ___ +-------e-------l----'c'---+---c'~'---'---~~~---·_,-------7/Jl/96 )A II S<W9 {DUP) MW19 (DL) 1116196 2/13/% 512/96 7/JI/% 7131/96 11/6/% 120 IJO 250 190 170 2.114/96 4.5 ~ 4,5 ') '-' '' I) " 160 HO 320 100 210E 3.2 86 2<0 100 s, 2) ,. 16 18 12 8.9 -----· 15 21 ---------IO " " 160 ,. 190 21 100 II 7.5 '·' '' I.I 8.5 '-' '·' 910E ,., 660 12 IOOE ., "'fl/%~~-1-----l----'~---l ----103---+-----_c•73 _____ 1------------1·7----___ c6c· 1c_ ___ , 7c';'9'~,c,.c6-11---------'-'----r---,~,---J-----~!!'-----1--------------,~,---11----,-,---+---""---l---"''--I 1116/96 ___ clcl0~---1------'120 _____ 1-------_-_-_-_-_-_ 7 _1 __ ====•ci,_-_-_-_-_-_1 1 ~---_-_-_-_-_-2• O•=======:,':=====~~======~-====~~=~- 7.8 " " 29 I ----,. 21 ----- MW21 ----------------2/14/'l6 5/2/96 7/30/96 JI 2.1 ---------·--- 1 ln/96 1.5 IMW=~,~,---------,-~1/~15~/Q~6c----J---------1-----",~, -·--·------~~---1 Sf)/% 2 8 l!!i!I 11!1!!1 ----~---- ~_!!.~) -------1-5/J/96___ 2.8 7/30/96 I-----I J I -------------· ----4,8 Lower Macon MW l3 --------·----(~L), _____ _ 11161%-------=---·-----=--~"!_. ____ ----· 2/14/96 2/14/96 -------- 80 76 ______ _ --·----·-----5121% 6J 15 -----------~------ ----------_ ---4.9 -----·--- ---__ 4J __ _ " -------------- ----------------1,J0/96 ---------··ss·----------24 4 11/6/96 ---i~-----___ 66 ______ --------·-· ··11-··-·· ---,",--- mm == == ,a;a 12 6.4 --------___ _, ______ ----- _, _____________ _li_ ________ , _____ -·------- 27 MW22---·------ui4/Q6--------s~S-------------6~_1·---------------__ !-~---__ ·-----------J.2 ______ -------·--··31··----·--··--------· ·-------·- ~-::__-~:----~-~~~~---_::__-----= --ll:t6 :=-~-----= -~-=~:~-=~~= -=--==--~~ir-=--·== -~~------~:-~--=~----IA ---------~~~:J~~~~-~= =~==~{J-~~= -~~~------~~~~ ~~~~-~ 11/6196 J.I l---~'c-'~--+------------_________________ _, ______ 1.9 ___________ ,_·~- Remediation Performance Standard • ,>C<. I, blanl. fflCIIM I><~-d<l..otion l,m,( !~IJ'-<q,l,c""="------11----_-_-_ -_ -_- UL-d,lutinn )500 70 200 28 _____ _[__ l~-~-------l----1--~'-~-1---- liillill 1!!11!1 !!Ill == == == == Gliliil Lower Docke MW16 J4 270 1100 61 100 150 11 2000 7/31/% 1------1-----+-----1·--4)----= J_~Q__ ---1300 10--120 150 . 12 -----------iiii)- 180 1100 68 5100 260 490 660 094 62 -------____ SI_OO lint% 1.1 -------q5--830 -3200 160 270 390 047 JS 2100 (DUP) ~/96---,-->-----l------c----l 89 -780 -2800 160 250 340 O 45 44 -----------1-----------1----1 -- MW 24 2/13/96 --------· __________ -~~---_ _3.2~--·-·· 3500 40 IJO ---~p___ _ __ _}_~---_______ --==--=il?Q:~-(i?_l!!'.).-_______ 2/IJ/% __ ___ _____________ 57 370 3700 !40 250 2~---__ _____ 19 __ , ______ IOI_?() ___ _ 512/% 65 2400 -------------··s/1/%-·-----------I---·---------g(j·----·----2soo " 79 11nl% ---~2 -82 2700 '" ---------------·- Macon Source A,ea MW2A 190 140 34 ----------------------------------------· 2/131% ·5,2/96-· -l==~-------1----------· '" (DUP) 5/2/96 150 26 " 7 ---------·----------------· -----1-----___________ l~Q ____________ _!_~--_____ ~-=-=-== =-·------. ----·---------·---·-1 -- 1111/% !20 25 JI ---·-------··--1.\ - c,ctw=,~--------1~~-_---------I-----__ -_-_--:-_,__160_'_Fl_l_l 1200 7141! 6.1 7~~ ----,-~=--+---_-c-=----~,--_--_-c-~---+----c-c _____ -j ______ --------~:---·- 512}% t---,c,~--+--,c_c,--i--190----300 --3300 ---i-~,"600=-+~=-+-~~-1--~~-i-~~-1--~--I 1700 1-----------1 7/31,W, ----2IO _I_J_OO_ ---1-~,0900oi--+--oc:CC-t-~c---+--'ccc--l-----t--cc--l 830 1800 ,oo 790 2.6 J5 ---·---- 520 140 210 12 --------- 290 78 140 12 (DUP) _______ ,__7c/cJlc/%=-I 120 170 1100 4700 940 11/6/96 13 220 47 530 5100 &4 JJ 260 230 61 130 96 Vl41% ------160-----85 -----------JO--J.2 400 5/2196 ----------------1-----I------,-,------1---,-,--1 23 -----~ ---9 1--------1---=~-, 1------1-------1-----1----------------f--~;---1------· ------1---~~----J 1----------t---:7'c13i0cc/%c'---l----+-----ll--------l-------__ _!_l_Q_ -----35----1----+--2-1--1-----+---a---------1---~3c2~--1 11/6/96 90 10 8 0MW=c1c9~------>-"u"i"J"l96~-l---------l------l--2c4,cFcJc2-1---2-IO---17-0------3-900~-+-8-7-I------------------0-_-,-1 --t-----t---c,cl---1 1,(~D~L),'-'-------+-c2/~l~J"l%c---l----l------l-------j------------· --------=-+-~~!----------------1--~-t---+--~~--1 MWII 512}% 59 170 3100 l--------l------1-------l·------------41 -----------------0 22 ----1----"-- 18 120 2900 78 --------------------23 -------------11/6/96 -_______ l_~----~----·-·-... _ 2500 -- --150 _ -----------_ ----~= ~-==-=-= =----==_39·-- lli!!l!!I !!El l!B l!!!!!il == == liiliil liliiiiiil liiliil , ______ --------------------------1--"'"'~- -------------------·---------------------------------·--·------------~~--------- 1----· -------· -------------------1-~~-I------·----- -_ _!~'!_ __ , ______ , -----·---------w----49 --2Jo s 3-1:-~ --------,-,-,---260--------18---·022-------·------,'-:oo'-' -- --__ -__ ------··------_ --_ 29 ---___ 170 __ -----900 --=== ____ si"" -=-·iso---~ ----21 ----=----=.=_,_-_-__ ,c•co~--, --=-------._ ____ ,----------. --------79 ---,, _____ ------35 --- --------------------------____ 4_9 ___ ------- Lower Macon Remediation Performance Standard l000 _":~~:~1:'_~~""""'t,,im..ie-1~,nlln~t ---1-____ _ l~~~-c-=•-----+----l-----1------lll. .J,/u1ion 3.5 38 -------------20 I I I I VE-01 I 2/22/96 6/5/96 7/1/96 11/8/96 I OW-I 2/22/96 6/5/96 7/1/96 11/8/96 OW-2 g OW-3 2/22/96 80 6/5/96 7/1/96 230 I 11/8/96 D OW-4 OW-5 2/22/96 380 6/5/96 11/8/96 D SVE Exhaust 2/14/96 45 2/15/96 43 2/16/96 73 4/3/96 D 6/5/96 7/1/96 I 8/1/96 SVE Inlet Line 6/5/96 57 D 7/1/96 Upper Dockery Air Stack 2/16/96 ! 4/3/96 6/5/96 I 7/1/96 8/1/96 ' 11/8/96 Lower Dockery Air Stack 4/3/96 I 8/1/96 11/8/96 Macon Source Air Stack 2/16/96 4/3/96 I 5/3/96 6/5/96 50 7/1/96 8/1/96 I i 11/8/96 i U/L Macon Air Stack 2/16/96 5/3/96 6/5/96 I 7/1/96 850 29 8/1 /96 11/8/96 Propeny Line 2/16/96 I 4/3/96 5/3/96 615196 7/1/96 I 8/1/96 11/8/96 ote. A blank meam below detection limit W-2 and OW-4 are 1101 connected to sysmn I SVE inlct line discon1inue.:! ! I I I g g n D H u I R I I I I -Number I I CHing ) Gn>undwater I Groundwater I I Elevation (ft) I (ft) I Elevation (ft) Upper i Dockery MWl5A MWIS MW20 UD-1 UD-2 tJD.J UD-4 UD-l UD-6 I 2/12/96 I : 2/14/96 I ! 2/15/96 I I 2/23/96 I I 2/28196 i i 5f2/96 I I 6/5/96 I ! 7/1/96 i I 7/31/96 I I 11/8/96 I I 2/12/96 I I 5/2/96 ! I 615/96 I I 7/1196 I i 7/31/96 : I 11/8196 I i 2112/96 I I 2/14/96 I : 2/15/96 I i 5/2/96 I 615/96 7/1/96 ! 7/31/96 i 1 11/8/96 1 ! 2112196 I ! 2114/96 I i 2/15/96 512196 6/5/96 I I i 711/96 i ! 1131196 I i 11/8/96 j I 2112/96 I I 2/14/96 I I 2/15/96 i I 2123/96 I 1 2/28/96 I I 5f2/96 I i 615196 I I 711196 I I 7/31/96 I I 11/8/96 I I 6/5/96 I I 711/96 I I 7/31/96 I i 11/8/96 I I 615196 I ! 711/96 I I 7/31/96 : I 11/8/96 ; I 615/96 ; i 711196 I I 7/31/96 j i 11/8/96 i ; 6/5/96 711/96 I ! 7/31/96 11/8/96 I 6/5/96 7/1/96 I 7/31/96 1 i 11/8/96 j I 6/5/96 I ! 7/1/96 i i 7/31196 I • 11/8/96 I 257.10 257.10 257.10 257.10 257.10 257. JO 257.10 257. JO 257.JO 257. 10 257.29 257.29 257.29 257.29 257.29 257.29 242.54 242.54 242.54 242.54 242.54 242.54 242.54 242.54 265.15 265.15 265. 15 265.15 265. 15 265.15 265.15 265.15 227.33 227.33 227.33 227.33 227.33 227.33 227.33 227.33 227.33 227.33 251.50 251.50 251.50 251.50 251.42 251.42 251.42 251.42 249.66 249.66 249.66 249,66 239.07 239.07 239.07 239.07 239,02 239.02 239.02 239.02 240.91 240.91 240.91 240.91 36.47 220.63 36.96 220.14 37.43 I 219.67 38.80 218.30 37.07 220,03 38.08 219.02 37.04 220,06 38.76 218.34 40.25 216.85 38.56 218.54 34.77 222.52 36.02 221.27 35.96 221.33 36,89 220.40 38.20 219.09 36.16 221.13 30.99 211.55 32.80 209.74 : 33.62 208.92 34.40 208.14 32.30 210.24 34.02 208.52 36.50 206,04 37.96 204.58 24.34 240.81 25.34 239.81 25.65 239.50 22.47 T 242.68 27 .25 237,90 27.80 237.35 28.78 236.37 20.12 245.03 26.90 200.43 26.79 200.54 26.83 200.50 27.80 I 199.53 26.09 201.24 25.43 201.90 25.55 201.78 26,26 201.07 27.38 199.95 26.29 201.04 169.72 43.30 208.20 83.70 167,80 79.02 172.48 38.27 213.15 38.91 I 212.51 41.15 210.27 41.06 210.36 86.42 163.24 44.52 I 205.14 86,69 162.97 65.81 183.85 92.60 146.47 35.82 203.25 92.37 I 146.70 83.45 155.62 28.01 211.01 32,35 206.67 35.00 204.02 34.81 204.21 29.60 211.3 I I 34.20 206.71 32.79 208.12 58.25 182.66 I I Number Casing Groundwater Groundwater Elevation (ft) (ft) Elention (ft) I UD-7 6/5/96 255.56 33.67 221.89 7/1/96 255.56 26.35 229.21 7/31/96 i 255.56 24.78 230.78 I 11/8/96 255.56 16.21 239.35 I UD-8 6/5/96 259 .43 34.43 225.00 7/1/96 259.43 40.21 219.22 ' 7/31/96 259.43 37 .50 221.93 11/8/96 259.43 34.24 225.19 D D D u I I I I I I I I I I • m I Lower Dockery MW 16• 2/12/96 I ! 59.97 31.18 128.79 2/14/96 I 159.97 31.40 128.57 • I 2/15/96 ! 159.97 31.72 128.25 2/23/96 159.97 32.87 127.10 5/2)96 159.97 32.70 127.27 6/5/96 159.97 31.79 128.18 7/1/96 I I 59.97 31.89 128.08 I 7/31/96 159.97 33.48 126.49 I 11/8/96 l 59.97 33.45 126.52 MW24• I 2/12/96 !32.99 5.74 127.25 2/14/96 132.99 5.75 127 ,24 H i 2/15/96 132.99 5.95 127.04 2/23/96 132.99 6.90 126.09 2/28/96 132.99 6.15 126.84 5/2/96 132.99 6.56 126.43 615196 132.99 6.35 126.64 H 7/1/96 132.99 6.15 126.24 8/1/96 132.99 6.91 126.08 I 11/8196 132.99 7.06 125.93 LD-1 6/5196 161.14 32.71 128.43 H 7/1/96 161.14 33.52 127.62 7/31/96 161.14 46.27 114.87 11/8/96 161.14 56.64 104.50 LD-2 615/96 154.80 26.93 127.87 7/1/96 154.80 26.98 127.82 D 7/31/96 154.80 35.50 I 19.30 11/8/96 154.80 55.39 99.41 LD-3 6/5/96 150.02 22.64 127 .38 7/1/96 150.02 22.70 127.32 I 7/31/96 150.02 27.75 122,27 11/8/96 150.02 35.18 114.84 LD-4 615/96 148.16 20.67 127.49 7/l/96 148.16 20.83 127.33 7/31/96 148.!6 24.50 123.66 I 11/8/96 \48.16 29.59 118.57 LD-5 6/5/96 !68.03 26.49 14!.54 7/1/96 168.03 34.66 133.37 7/31/96 168.03 45.48 122.55 I 11/8/96 168,03 45.86 122. I 7 • I I I I I I I I I I I I I I I g I n D D D I I I -Number l I Casing I Groundwater I Groundwater I I Elt~\·ation (ft) I (ft) I Elevation (fl) Macon Source Area I J I MW 2 : 2/12/96 I 231.39 I 37.20 i 1 4/2/96 I 231.39 I 38.33 1 I 5/1/96 I 231.39 l 38.78 I i 6/5/96 I 231.39 I 38.96 1 7/1/96 I 231.39 i 40.52 1 8/1/96 I 231.39 I 43.21 i 11/8/96 I 231.39 I 41.32 MW 2A" I 2/12/96 I 230.83 I 37.45 MW) MWl MW 6 MW7 MWS MWSA I 2/14196 I 230.83 I 37.56 : 2/23/96 I 230.83 I 39.78 1 2128/96 I 230.83 ! 39.00 1 5/1/96 I 230.83 I 38,68 I 6/5/96 I 230.83 i 39.18 7/1/96 ! I 7/30/96 i I 1/8/96 I I 2/12/96 ! 5/1/96 6/5/96 111196 I 8/1196 i I 11/8196 I 2/12/96 I i 4f2t96 ! I 5/1/96 I I 615196 i 7/\/96 i 8/1/96 ! I 11/8/96 I l 2/12/96 I I 4(2196 i I 5/1196 I I 6/5/96 I 7/1/96 : 7/30196 I 1118/96 I I 2112196 4/2/96 5/1/96 6/5/96 7/1/96 I I 8/1196 i 1118196 I I 2/12/96 I i 412196 I 511/96 I I 6/5/96 I 711/96 i I 8/1196 I I 2/12/96 i 412196 i 5/1/96 I 6/5/96 I 7/1/96 i 8/1/96 i , 2/12/96 i I 2/14196 i i 2/15/96 I I 2/23/96 I : 2/28196 I I 5/1/96 I ' 6/5/96 I I 111196 I I 7/30/96 I i 11/8/96 I I i 230.83 40.37 230.83 43.57 230.83 40.91 220.67 26.60 220.67 28.35 220.67 I 28.16 220.67 29.86 220.67 30.01 220.67 28.57 234.51 37.62 234.51 37.94 234.51 38.02 234.51 38.00 234.51 39.69 234.51 39.50 234.51 37.17 237.13 439.79 237.13 41.61 237.13 4 l.90 237.13 39.05 237.13 41.72 237. 13 44.27 237.13 I 44.05 228.41 35.57 228.4) 36.23 228.41 36.63 228.41 37.05 228.41 38.32 228.41 38.26 228.41 38.69 234.54 39.98 234.54 40.07 234.54 41.01 234.54 41.5 I 234.54 43.26 234.54 I 43.88 234.44 44.83 234.44 45.53 234.44 45.81 234.44 45.73 234.44 49.12 234.44 I 46.92 2.54.08 46.60 254.08 46.70 254.08 I 47.68 2.54.08 I 44.03 2.54.08 46.04 254.08 I 43 . .55 254.08 42.89 2.54.08 42.84 254.08 I 42.30 254.08 I 40.65 I I I I I I I I I i I I I I I 194.19 193.06 192.61 192.43 190.87 188.18 190.07 193.38 193.27 191.05 191.83 192.15 191,65 ]90.46 187.26 189.92 194.07 192.32 192.51 190.81 190.66 192.10 196.89 196.57 196.49 196.S I I 94.82 195.01 197.34 197.34 195.52 195.23 198.08 195.41 192.86 193.08 192.84 192.18 191.78 191.36 190.09 190.15 189.72 I 94.56 194.47 193.53 191.28 190.66 189.61 188.91 ]88,63 188.71 185.32 187.52 207.48 207.38 206.40 210.05 208.04 210.53 211.19 211.24 211.78 213.43 I I I g Macon Source Area MWIO 2/12/96 265.51 41.03 224.48 2/15/96 265.51 40.88 224.63 4/2/96 265.51 36.98 228.53 I 5/1/96 265.51 35.76 229.75 6/5196 265.51 35.90 229.61 7/1/96 265.51 35.96 229.55 7/30/96 265.51 35.98 229.53 11/8/96 265.5 l 33,31 232.20 I MWIJ• ! 2/12/96 271.92 30.72 241.20 2/23/96 271.92 31.00 240.92 2/28/96 271.92 30.00 241.92 5/1/96 271.92 30.31 241.61 I 6/5/96 271.92 31.41 240.51 711/96 271.92 32.92 239.00 7/30/96 271.92 34.42 237.50 11/8/96 271.92 27.60 244.32 MWIIA 2/12/96 270.28 30.22 240.06 D 4f2196 270.28 27.05 243.23 5/1/96 270.28 28.05 242.23 6/5/96 270,28 30.62 239.66 711196 270.28 32. 15 238,13 n 7/30/96 270.28 33.11 237.17 11/8/96 270.28 27.15 243.13 MW 19• 2/12/96 236.89 38.49 198.40 2/14/96 236.89 38.82 198.07 ' 2/23/96 236.89 40.90 195.99 D 2/28/96 ! 236.89 40.50 196.39 5/1/96 236.89 38.44 198.45 6/5/96 236.89 37.91 198.98 7/1/96 236.89 39.23 197.66 I 7/30/96 236,89 39.65 197.24 11/8/96 236.89 37. JO 199.79 UMS-1 615196 238.96 44.15 194.81 7/1/96 238.96 44.70 194.26 7/30/96 ' 238.96 58.60 180.36 I 11/8/96 238.96 58.88 180.08 UMS-2 6/5/96 236.31 64.75 171.56 7/1/96 236.3 I 57.60 178.71 7/30/96 236.3 I 64.58 171.73 I 11/8/96 236.3 I 65.40 170.91 UMS-3 615196 235.75 43.46 192.29 7/1/96 235.75 72.78 162.97 7/30/96 235.75 72.87 162.88 ' 11/8/96 235.75 73.13 162.62 I UMS-4 6/5/96 236.53 75.66 160.87 7/1/96 236.53 76.58 159.95 7/30/96 236.53 76.98 159.55 11/8/96 236.53 76.44 160.09 I UMS-5 6/5/96 257.62 82.55 175.07 7/1/96 257.62 81.00 176.62 7/30/96 257.62 82.87 174.75 11/8/96 257.62 79.92 177.70 I I I I I I I I Upper Macon MW21" 2/14/96 155.52 14.52 141.00 2/23/96 155.52 15.60 139.92 I 2/28/96 155.52 14.65 140.87 5f2196 155.52 14.38 141.14 6/5/96 155.52 15.47 140.05 7/30/96 155.52 7.02 148.50 I 11/7/96 155.52 14.62 140.90 MW23" ' 2/14196 155.54 4.45 15l.09 2/23/96 155.54 5.73 149.81 2/28/96 155.54 4.07 151.47 5/3/96 155.54 5. 19 ! 50.35 I 6/5/96 155.54 5.59 149.95 711/96 155.54 7,56 147.98 i 7/30/96 155.54 7.72 147.82 11/6/96 155 .54 6.19 149.35 I UM-I 6/5/96 I 83.68 37.01 146.67 7/1/96 183.68 36.47 147.21 7/30/96 183.68 41.l0 142.58 ! 11/8/96 183.68 39.44 144.24 UM-2 6/5/96 194.13 43.02 15 l.l l 8 7/1/96 194.13 47.95 146.18 7/30/96 ' 194. 13 47.33 146.80 11/8/96 194.13 45.41 148.72 UM-3 615/96 180.35 32.17 148.18 D 7/1/96 180.35 32. 18 148.17 7/30/96 180.35 32.36 147.99 11/8/96 180.35 32.31 148.04 UM-4 6/5/96 171.91 21.85 150.06 7/1/96 I 71.91 2LI0 150,81 I 7/30/96 I 71.91 27.55 144.36 11/8/96 171.91 24.52 147.39 UM-5 6/5196 168.32 11.77 156.55 7/1/96 i 168.32 12.13 156. 19 I 7/30/96 168.32 16.92 I 51.40 I 1/8/96 168.32 13.85 154.47 UM-6 6/5/96 173.05 11.72 161.33 711/96 173.05 13.23 159.82 7/30/96 I 73,05 I 7.58 155.47 • 11/8/96 173.05 14.40 158.65 UM-7 6/5/96 187.29 54.45 132.84 7/1/96 187 .29 54.58 132.71 7/30/96 187.29 54.59 132.70 I 11/8/96 187.29 55.00 132.29 I u I I I g I u I R I I I I I R I I I I I I -Sumber I C■sin~ I Groundwater ! Groundwater Lo~er Macon MW4 MW12 MWJJ• MW 14 MWl4R MW22° LM-1 LM-2 LM-3 LM-4 LM-5 I Elevation (ft) I (ft) I Ele\·ation (fti 2114/96 I 412196 I 512196 I 615196 I : 7/1/96 I ! 7/30/96 I 11/8/96 I I 2114196 I I 412/96 I i 512196 I 1 6/5/96 I I 7/1196 I I 7/30/96 I 111s196 I i 2/14/96 i 2123/96 I I 2128/96 4/2/96 5/2/96 6/5/96 i 7/1/96 I I 7/30/96 i 11/8/96 i 2/14/96 412196 I I 5/2/96 i 6/5/96 I I 7/1/96 I ! 7/30/96 ' 1118196 I i 2114/96 4/2/96 5/2/96 6/5/96 I 7/1/96 I 7/30/96 i 11/8196 I I 2114/96 I 2123196 i 2/28/96 5/2/96 ! ! 615196 I 1 7/1/96 I 7/30/96 I · 1118196 I I 6/5/96 I I 111196 1 7/30/96 I 11/8196 I '' 615196 I 7/1/96 I 7/30/96 I : 1118t96 I I 6/5/96 I i 7/1/96 ' 7/30/96 i 11/8/96 i 6/5/96 I I 111196 i 7/30/96 I I 118196 I 6/5/96 I I 111196 I : 7/30/96 I I I 1/8/96 I I I I 184.21 184.21 184.21 I 84.21 !&4.21 184.21 7 1&4.2] 171.98 171.98 l 171.98 171.98 I I 71.98 I 71.98 171.98 188.67 188.67 188.67 I 188.67 188.67 188.67 188.67 188.67 188,67 177.34 177.34 177.34 177.34 177.34 177.34 177.34 175.95 175.95 175.95 175.95 175.95 175.95 175.95 128.25 128.25 128.25 128.25 128.25 128.25 128.25 128.25 175.68 175.68 175.68 175.68 157.20 157.20 157.20 157.20 157.09 157.Q9 157.09 I 157.09 166.84 166.84 166,84 166,84 186.59 186.59 I 186.59 186.59 40.79 46.08 45.72 43.29 42.09 45.71 46.35 24.87 26.18 26.09 25.97 27.37 27.55 26.24 49.22 50.20 49,25 50.85 51.38 49.88 50.55 51.59 52.15 34.24 dry dry 35.19 d,y 34.50 38.81 39.27 38,85 37,98 40.03 40.39 5.73 6.76 5.59 6.87 7.05 6.78 2.31 6.96 69.79 38.61 69.78 70.04 62.06 25.08 58.36 62. 16 61.16 27.78 49.40 67.24 68.60 37.72 56.91 74.86 66.50 43.91 66.80 66.86 ' I : I I I i I i I I ! 143.42 138.13 138.49 140.92 142.12 138.50 137.86 147.11 145.80 145.89 146.01 144.61 144.43 145.74 139.45 138.47 139.42 137.82 137.29 138.79 138.12 137.08 136.52 143.10 d,y 142. 15 d,y dry d,y 141.45 137.14 136.68 137.10 137.97 135.92 135.56 122.52 121.49 122.66 121.38 121.20 121.47 125.94 121.29 105.89 137.07 105.90 105.64 95.14 132.12 98,84 95,04 95,93 129.31 107.69 89,85 98.24 129.12 109.93 91 ,98 120.09 142.68 119.79 119.73 I I m g I I I D D I I I I I I I I I , I I LA BORA TORY ANALYTICAL RES UL TS SAMPLED 11-6-96, 11-7-96, 11-8-96 I I I I I u I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES Page 1 DATE/ TIME SAMPLED ------------------------------------------------------------------------86602-1 86602-2 86602-3 86602-4 86602-5 MW-11 MW-9 MW-19 MW-2A MW-23 11-06-96/0900 11-06-96/1050 11-06-96/1140 11-06-96/1445 11-06-96/1600 ------------------------------------------------------------------------PARAMETER 86602-1 86602-2 86602-3 86602-4 86602-5 --------------------------------------------------------------------- ---------- Purgeable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 1.5 <1.0 5.8 ug/1 <l. 0 <2.0 <1.0 1.1 8.5 <1.0 7.6 10 76 % 12-152 % 11.14. 96 1. 0 1113B 1El114 --------------------------------------- <5.0 170 <5.0 100 <10 <5.0 7.0 11 7.5 59 50 118 % 12-152 \ 11.14. 96 5.0 1113B 1Elll4 ---------- <10 14 110 120 <20 16 44 21 <10 110 100 110 % 12-152 \- 11.14.96 10.0 1113B 1El114 ---------- <1.0 <1.0 3.0 4.3 4.0 <1.0 13 4.9 <2.0 <2.0 2.3 1.2 1.5 <1.0 21 12 <1.0 <1.0 10 9.3 10 10 100 % 93 % 12-152 \ 12-152 \ 11.14.96 11.15.96 1.0 1.0 1113B 1113B 1Elll4 1Elll5 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I J SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 2 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED 86602-1 MW-11 ll-06-96/0900 86602-2 MW-9 ll-06-96/1050 86602-3 MW-19 ll-06-96/1140 86602-4 MW-2A ll-06-96/1445 86602-5 MW-23 ll-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER 86602-1 I' 1rgeable Aromatics (8.020) Eenzene, ug/1 Tc,luene, ug/1 <l.0 <l.0 Total Xylenes, ug/1 <3.0 Acetone, ug/1 <10 Surrogate -a,a,a-Trifluorotoluene 34 Surrogate -Expected Value 30 Surrogate -% Actual Recovery 113 % Surrogate -Control Limit 41-150 % Date Analyzed 11.14.96 Dilution factor Batch ID Clock ID Barium (6010) l. 0 1113B 1Elll4 86602-2 <5.0 <5.0 13 220 84 150 56 % 41-150 % 11.14.96 5.0 1113B 1Elll4 86602-3 <10 <10 <30 <100 170 300 57 % 41-150 % 11.14.96 10.0 1113B 1Elll4 86602-4 <l.0 <l.0 <3.0 <10 18 30 60 % 41-150 % 11.14.96 1.0 1113B 1Elll4 86602-5 <l.0 1.0 <3.0 <10 33 30 110 % 41-150 % 11.15.96 1.0 1113B 1Elll5 Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 90 530 130 110 <50 11.11.96 11.11.96 11.11.96 11.11.96 11.11.96 11.12.96 11.12.96 11.12.96 11.12.96 11.12.96 1.0 1.0 1.0 1.0 1.0 llllE llllE llllE llllE llllE Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA , I ' . I I I m I • I I II II 11 II II II I I • s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. m 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I g u 0 D I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: 56-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 3 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED -------------------------------------------------------------------- 86602-1 MW-11 86602-2 MW-9 86602-3 MW-19 86602-4 MW-2A 86602-5 MW-23 11-06-96/0900 11-06-96/1050 11-06-96/1140 11-06-96/1445 11-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date JIJ1alyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-1 86602-2 <5.0 <5.0 11.11.96 11.11.96 11.12.96 11.12.96 1.0 1.0 llllE llllE <0.30 <0.30 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112J 1112J <10 47 11.11.96 11.11.96 11.12.96 11.12.96 1.0 1.0 llllE llllE 86602-3 86602-4 86602-5 -. -------- <5.0 <5.0 <5.0 11.11.96 11.11. 96 11. 11. 96 11.12.96 11.12.96 11. 12. 96 1.0 1.0 1.0 llllE llllE llllE <0.30 <0.30 <0.30 11.12.96 11.12.96 11.12.96 11.13.96 11.13.96 11 .13. 96 1.0 1. 0 1.0 1112J 1112J 1112J 240 <10 <10 11.11.96 11.11.96 11.11.96 11.12.96 11.12.96 11.12.96 1.0 1.0 1.0 llllE llllE llllE ------------------------------ 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES I & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 • Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES Page 4 DATE/ TIME SAMPLED ------------------------------------------------------------------------------------------ 86602-1 86602-2 86602-3 86602-4 86602-5 MW-11 MW-9 MW-19 MW-2A MW-23 11-06-96/0900 11-06-96/1050 11-06-96/1140 11-06-96/1445 11-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyze.d Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 8%02-1 ---------- 10 11.11.96 11. 12. 96 1.0 llllE <40 11.11.96 11.12.96 1.0 llllE <3.0 11.12. 96 11.13.96 1.0 1112J ---------- 86602-2 ---------- 5100 11.11.96 11.12. 96 1.0 llllE 84 11.11.96 11.12.96 1.0 llllE <3. 0 11.12.96 11.13.96 1.0 1112J ---------- 86602-3 86602-4 86602-5 ------------------------------ 25,'0 13 49 11.11_9; 11.11.96 11.11.96 11.12.96 11.12.96 11.12.96 1. 0 1.0 1.0 llllE llllE llllE 150 <40 <40 11.11.96 11.11. 96 11.11. 96 11.12.96 11.12. 96 11.12.96 1.0 1.0 1.0 llllE llllE llllE <3.0 <3.0 <3.0 11.12.96 11.12.96 11.12.96 11.13.96 11.13.96 11.13.96 1.0 1.0 1.0 1112J 1112J 1112J ------------------------------ Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D 0 m ffl I I I I I I I I I I g g D u D I I I I I SL-SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 5 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------------ 86602-l 86602-2 86602-3 86602-4 86602-5 MW-ll MW-9 MW-19 MW-2A MW-23 ll-06-96/0900 ll-06-96/1050 ll-06-96/1140 ll-06-96/1445 ll-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER 86602-l 86602-2 86602-3 86602-4 86602-5 ---------- ---------- ------------------------------A:1timony (7041) A~timony (7041), ug/1 Preparation Date Dat:e Analyzed Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Suspended Solids (160.2) Suspended Solids (160.2), mg/1 Date Analyzed Batch ID <10 ll.ll.96 ll.14.96 l.O llllM <50 ll. ll. 96 ll.12.96 l,0 llllE <20 ll.ll.96 ll .12. 96 1.0 llllE 8.0 ll.12.96 lll2A <10 ll.ll.96 11.14.96 l,O llllM <50 ll.ll.96 ll.12.96 l.0 llllE 33 ll.ll.96 ll.12.96 1.0 llllE 260 ll.12.96 lll2A ---------- <lO ll.ll.96 ll.14.96 l.O llllM <50 ll.11.96 ll.12.96 1.0 llllE <20 ll.ll.96 ll.12.96 1.0 llllE 39 ll.12.96 lll2A ---------- <10 <10 ll.ll.96 ll. ll. 96 ll .14. 96 11.14. 96 1.0 1.0 llllM llllM <50 <50 ll.ll.96 ll. ll. 96 ll.12.96 ll.12.96 1.0 1.0 llllE llllE <20 <20 ll.ll.96 ll. ll. 96 ll.12.96 ll.12.96 1.0 1.0 llllE llllE <5.0 20 ll .12. 96 11.12. 96 lll2A lll2A -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I I I I u 0 u I I I I B I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS LOG NO 86602-6 86602-7 86602-8 86602-9 86602-10 SAMPLE DESCRIPTION, LIQUID SAMPLES MW-13 MW-22 Macon Source Inf Macon Source Eff U Macon Inf. PARAMETER Purgeable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID 86602·6 1.5 66 17 ug/1 2.3 <2.0 <1.0 48 4.8 <1.0 9.8 10 98 \ 12-152 \ 11.15.96 1.0 1113B Clock ID 1Elll5 86602-7 <1.0 3.1 3.4 <l.0 <2.0 c::1.0 1.9 3.4 <1.0 9.0 10 90 \ 12-152,\ 11.15.96 1.0 1113B 1Ell14 86602-8 <1.0 ·;. 2 9 2 7.5 <2.0 2.3 3.4 10 2.0 9.9 10 99 \ 12-152 \ 11.15.96 1.0 1113B 1Ell14 -------------------- Page 6 DATE/ TIME SAMPLED 11-06-96/1630 11-06-96/1645 11-07-96/0700 11-07-96/0700 11-07-96/0715 86602-9 86602-10 <1.0 <1.0 <l.0 5.3 <l.0 1.9 <l.0 6.6 <2.0 <2.0 c::1.0 2.3 <1.0 <1.0 <l.0 8.3 <1.0 <1.0 8.2 9.5 10 10 82 \ 95 \ 12-152 \ 12-152 \ 11.15.96 11.15.96 1.0 1.0 1113B 1113B 1Elll4 1Elll4 -------------------- Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 131961125 REPORT OF RESULTS Page 7 DATE/ I I I LOG NO 86602-6 86602-7 86602-8 86602-9 86602-10 SAMPLE DESCRIPTION, LIQUID SAMPLES -------------------------------------------------- MW-13 MW-22 ==~: -:~~~:~ ----------D ll-06-96/1630 Macon Source Inf Macon Source Eff U Macon Inf. ll-06-96/1645 ll-07-96/0700 ll-07-96/070U ll-07-96/0715 0 -----------------------.--------------------------- PARAMETER 86602-6 86602-7 86602-8 ------------------------------------------------------------------------------- ----------------------0 86602-9 86602-10 Purge able Aromatics ( 8 02 0) Benzene, ug/1 l.4 <1.0 <l.0 <1.0 <l.0 Toluene, ug/1 <l.0 <l.0 1.0 <l.0 <l.0 Total Xylenes, ug/1 <3.0 <3.0 <3.0 <3.0 <3.0 Acetone, ug/1 <10 <10 <10 <10 <10 Surrogate -a,a,a-Trifluorotoluene 32 21 20 30 30 Surrogate -Expected Value 30 30 30 30 30 Surrogate -\ Actual Recovery 107 \ 70 \ 67 \ 100 \ 100 \ Surrogate -Control Limit 41-150 \ 41-150 \ 41-150 \ 41-150 % 41-150 \ Date Analyzed 11.15.96 11.15.96 ll.15.96 11.15.96 ll.15.96 Dilution factor l.0 1.0 l.0 l.0 l. 0 Batch ID 1113B 1113B 1113B 1113B 1113B Clock ID 1Elll5 1Elll4 1Elll4 1Elll4 1Elll4 Barium (6010) Barium (6010), ug/1 520 <50 140 140 <50 Preparation Date ll. ll. 96 ll. ll. 96 ll. ll. 96 11.11.96 ll.ll.96 Date Analyzed 11.12.96 ll.12.96 ll.12.96 11.12. 96 11.12. 96 Dilution factor l.0 l.0 l. 0 l.0 1.0 Bat.ch ID llllE lll1E llllE llllE llllE ------------------------------------------------------------------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA 0 I I I • s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. m 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I I g I I B H I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 8 LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES 86602-6 MW-13 86602-7 MW-22 86602-8 Macon Source Inf 86602-9 Macon Source Eff 86602-10· U Macon Inf. PARAMETER 86602-6 86602-7 86602-8 -----------------------------------------------··----------- Beryllium (6010) Beryllium (6010), ug/1 <5.0 <5.0 <5.0 Preparation Date 11.11. 96 11.11.96 11.11.96 Date Analyzed 11.12.96 11.12. 96 11.12.96 Dilution factor 1.0 1.0 l. 0 Batch ID llllE llllE llllE Cadmium (7131) Cadmium (7131), ug/1 <0. 30 <0.30 <0.30 Preparation Date 11. 12. 96 11.12.96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1.0 1.0 Batch ID lll2J 111:/J lll2J Chromium ( 6 010) Chromium (6010), ug/1 16 <10 <10 Preparation Date 11.11.96 11.11. 96 11.11.96 Date Analyzed 11.12.96 11.12. 96 11.12. 96 Dilution factor l. 0 1.0 1.0 Batch ID llllE llllE llllE ---------- DATE/ TIME SAMPLED ll-06-96/1630 ll-06-96/1645 ll-07-96/0700 ll-07-96/0700 ll-07-96/0715 86602-9 86602-10 -------------------- <5.0 <5.0 11.11.96 11.1:.96 11.12.96 11.12.96 1.0 1.0 llllE llllE <0.30 <0.30 11.12.96 11.12.96 11.13. 96 11.13.96 1.0 1.0 lll2J lll2J <10 <10 11.11.96 11.11.96 11.12.96 11.12.96 1.0 1.0 llllE llllE -------------------- I Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ' . ) ,_ , SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO 86602-6 86602-7 86602-8 86602-9 86602-10 REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES MW-13 Page 9 DATE/ TIME SAMPLED ll-06-96/1630 ll-06-96/1645 ll-07-96/0700 ll-07-96/0700 ll-07-96/0715 MW-22 Macon Source Inf Macon Source Eff U Macon Inf. ------------------------------------------------------------------------------------------ PARAMETER . 86602-6 86602:7 86602-8 86602-9 86602-10 Manganese (6010) Manga1°.ese (6010), ug/1 .' 760 270 9.8 13 <5.0 Preparation Date 11.11. 96 11.11. 96 11.11.96 11.11.96 11.11.96 Date Ar,lyzed 11.12. 96 11.12.96 11.12.96 11.12. 96 11.12.96 Dilution factor l. 0 1.0 1.0 1.0 1.0 Batch ID llllE llllE llllE llllE llllE Nickel (6010) Nickel (6010), ug/1 <40 <40 <40 <40 <40 Preparation Date 11.11.96 11.11. 96 11.11.96 11.11. 96 11.11.96 Date Analyzed 11.12.96 11.12. 96 11.12.96 11.12. 96 11.12.96 Dilution factor 1.0 1.0 1.0 l. 0 1.0 Batch ID llllE llllE llllE llllE llllE Lead (7421) Lead (7421), ug/1 13 4.3 <3.0 <3.0 <3.0 Preparation Date 11.12.96 11.12.96 11.12.96 11.12.96 11.12. 96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1.0 1.0 1.0 1.0 Batch ID lll2J lll2J lll2J lll2J lll2J ------------------------------------------------------------------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I D 0 D 0 I I I • s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I g I I I I D H D H I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 10 DATE/ LOG NO 86602-6 86602-7 86602-8 86602-9 86602-J.0 SAMPLE DESCRIPTION, LIQUID SAMPLES MW-13 MW-22 Macon Source Inf Macon Source Eff u Macon Inf. TIME SAMPLED ll-06-96/1630 ll-06-96/1645 ll-07-96/0700 ll-07-96/0700 ll-07-96/0715 PARAMETER 86602-6 86602-7 86602-8 86602-9 86602-10 Antimony (7041) Antimony (7041), ug/1 Preparation Date Date Analyzed- Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Suspended Solids (160.2) Suspended Solids (160.2), Date Analyzed Batch ID mg/1 <10 <10 11.11.96 11.11.96 11.14.96 11.14.96 1.0 1.0 llllM llllM 60 <50 11.11.96 11.ll.~6 11.12.96 11.12.96 1.0 l. 0 llllE llllE 110 39 11.11.96 11.11.96 11.12.96 11.12. 96 l. 0 l. 0 llllE llllE 730 170 11.12. 96 11.12.96 1112A 1112A ---------- <10 <10 <10 11.11.96 11.11.96 11.11.96 11.14. 96 11.14.96 11.14 .,96 1.0 1.0 l. 0 llllM llllM llllM <50 <50 <50 11.11.96 11.11.96 11.11.96 11 .12. 96 11.12.96 11.12.96 1.0 1.0 1.0 llllE llllE llllE <20 <20 <20 11.11.96 11.11.96 11.11.96 11.12. 96 11.12.96 11.12.96 1.0 1.0 1.0 llllE llllE llllE 10 26 <5.0 11.12.96 11.12.96 11.12. 96 1112A 1112A 1112A ------------------------------ Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I ,_) SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-0000l-Ol/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page ll DATE/ SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED I 0 86602-ll 86602-12 -------------------------------------------------- L Macon Inf U/L Macon Eff ----------------------0 ll-07-96/0715 ll-07-96/0720 --------------------------------------------------PARAMETER 86602-ll 86602-12 ----------------------0 Purgeable Halocarbons (8010) Chloroform, mg/kg dw l, l-Dichloroethane, mg/k,i dw l,l-Dichloroethene, mg/kg dw Cis/Trans-l,2-Dichloroethe~ e, mg/kg dw Methylene chloride (Dichloromethane), mg/kg dw Tetrachloroethene, mg/kg dw l,l,l-Trichloroethane, mg/kg dw Trichloroethylene, mg/kg dw Vinyl chloride, mg/kg dw Surrogate -Bromochloromethane .surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID <l.0 ll 3.3 2.2 <2.0 <l.0 5.2 4.5 <l.0 9.0 lO 90 % 12-152 \ ll.15.96 l.O lll3B lElll5 <1.0 <l.0 <l.0 <l.0 <2.0 <l.O <1.0 <l.O <l.0 8.2 lO 82 \ 12-152 \ ll.15.96 l.O lll3B lElll5 ------------------------------------------------- Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I 0 I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 L.aRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I a ft D B I B I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6·86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 12 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES -------------------------------------------------- 86602-11 86602-12 L Macon Inf U/L Macon Eff -------------------------------------------------- PARAMETER Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 86602-11 <1.0 <1.0 Total Xylenes, ug/1 <3.0 Acetone, ug/1 <10 Surrogate -a,a,a-Trifluorotoluene 29 Surrogate -Expected Value 30 Surrogate·% Actual Recovery 97 % Surrogate· Control Limit 41-150 % Date Analyzed 11.15. 96 Dilution factor 1.0 Batch ID 1113B Clock ID 1Elll5 Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID <50 11.11.96 11.12. 96 1. 0 llllE <5.0 11.11.96 11.12.96 1.0 llllE 86602-12 <1.0 <1.0 <3.0 <10 29 30 97 % 41-150'% 11.15.96 1.0 1113B 1Elll5 <50 11.11.96 11.12.96 1. 0 llllE <5.0 11.11. 96 11.12.96 1.0 llllE TIME SAMPLED ll-07-96/0715 ll-07-96/0720 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES -------------------------------------------------------------------- 86602-11 L Macon Inf 86602-12 U/L Macon Eff -------------------------------------------------------------------- PARAMETER Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-11 ---------- <0.30 11.12.96 11.13.96 1. 0 1112J <10 11.11.96 11.12. 96 1.0 llllE 6.4 11.11.96 11.12. 96 1.0 llllE <40 11.11.96 11.12. 96 1.0 llllE 8,602-12 ---------- <0.30 11.; 2. 96 11.L .96 ·'·. 0 111?.J <10 11.11. 96 11.12.96 1.0 llllE <5.0 11.11.96 11.12. 96 1. 0 llllE <40 11.11.96 11.12.96 1.0 llllE ------------------------------------------------- Page 13 DATE/ TIME SAMPLED 11-07-96/0715 11-07-96/0720 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D 0 0 0 D I I I g s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I B u 0 0 I H I I I I I I 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 14 DATE/ LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------------ 86602-11 86602-12 L Macon Inf U/L Macon Eff 11-07-96/0715 11-07-96/0720 ------------------------------------------------------------------------------------------ PARAMETEP Lead (7421) Lead (742i), ug/1 Preparation Date Date Analyz:,d Dilution factor Batch ID Antimony (7041) Antimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-11 ---------- <3.0 11.12.96 11.13.96 1.0 1112J <10 11.11.96 11.14.96 1.0 1111M <50 11.11.96 11.12.96 1.0 llllE <20 11.11.96 11.12.96 1.0 llllE ---------- 86602-12 ---------- <3.0 11.12.96 11.13.96 1.0 1112J <10 11.11.96 11.14.96 1.0 1111M <50 11.11.96 11.12. 96 1.0 llllE <20 11.11.96 11.12.96 1.0 llllE ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES Page 15 DATE/ TIME SAMPLED -------------------------------------------------------------------- 86602-11 L Macon Inf 86602-12 U/L Macon Eff ll-07-96/0715 ll-07-96/0720 ------------------------------------------------------------------------------------------PARAMETER 86602-11 Suspended Solids (160.2) Suspended Solids (160.2), mg/1 <5.0 Date Analyzed 11.12,96 Batch ID 1112A 86602-12 <5.0 ,.1.12.96 1112A --------------------------------------- ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ' -i '. , D D g D 0 I I I u s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. D 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 u u I I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: OB NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 16 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED 86602-13 MW-19 ll-06-96/1140 86602-14 MW-23 ll-06-96/1600 86602-15 MW-13 ll-06-96/1630 PARAMETER Mercury (7470) Mercury (7470), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-13 ---------- <0.20 11.11.96 11.12.96 1.0 llllS ---------- 86602-14 86602-15 -------------------- <0.20 0.65 11.11.96 11.11.96 11. 12. 96 11.12.96 1.0 1. 0 1111S llllS -------------------- 1 Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 17 LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES DATE SAMPLED ------------------------------------------------------------------------------------------ 86602-16 Trip Blank 11-07-96 ------------------------------------------------------------------------------------------ PARAMETER 86602-16 Purgeable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate Bromochloromethane Surrogate. -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID <1.0 <l. 0 <1.0 ug/1 <l. O <2. 0 <1.0 <1.0 <1.0 <1.0 6.7 10 67 % 12-152 % 11.15.96 1.0 1113B 1El115 ---------------------------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D 0 I I I I I I I I I: II I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I I I I B H I I E I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 18 DATE SAMPLED LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES ------------------------------------------------------------------------------------------ 86602-16 Trip Blank 11-07-96 ------------------------------------------------------------------------------------------ PARAMETER 86602-16 Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 <l.0 2.7 Total Xylenes, ug/1 <3.0 Acetone, ug/1 <10 Surrogate -a,a,a-Trifluorotoluene 28 Surrogate -Expected Value 30 Surrogate -\ Actual Recovery 93 % Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 41-150 \ 11.15.96 l.O 1113B 1Elll5 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-B6602 Received: OB NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 19 LOG NO 86602-17 86602-18 86602-19 86602-20 86602-21 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result !,CS Duplicate Result LCS Expected Value ----------------------------------------------------------------------------------- PARAMETER 86602-17 86602-18 86602-19 86602-20 86602-21 --------------------------------------- ---------- ------------------------------ Purgeable Halocarbons {8010) Chloroform, ug/1 1,1-Dichloroethane, ug/J 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Brornochloromethane Surrogate -Expected Value Surrogate \ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID ug/1 1.0 1.0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1:0 <1.0 <1.0 <1.0 7.9 10 79 % 12-152 % 11.14.96 1.0 1113B Clock ID 1Elll4 ------------------------------------------------- 13 13 20 15 16 20 8.7 9.1 10 10 87 % 91 % 12-152 % 12-152 % 11.14.96 11.15.96 1.0 1.0 1113B 1113B 1E1114 1E1115 ------------------------------ Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I D 0 I I II I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I I I I I I u B I I I I I I I I 5102 laRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 122161125 LOG NO 86602-17 86602-18 86602-19 86602-20 86602-21 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 20 PARAMETER 86602-17 86602-18 86602-19 86602-2(' 86602-21 Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Total Xylenes, ug/1 Acetone, ug/1 Surrogate -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -i Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Barium (6010) 1.0 1.0 3.0 10 Barium (6010), ug/1 50 Preparation Date Date Analyzed Dilution factor Batch ID <l.0 <1.0 <3.0 <10 36 30 120 i 41-150 i 11.14. 96 l. 0 1113B 1Elll4 <50 11.11.96 11.12.96 1.0 llllE ---------- 14 16 20 14 17 20 33 33 30 30 110 i 110 i 41-150 i 41-150 i 11.14.96 11.15.96 l. 0 1.0 1113B 1113B 1Elll4 1Elll5 948 972 1000 11.11.96 11.11.96 11.12.96 11.12.96 1.0 l. 0 llllE llllE ---------- ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA , i . , SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA' 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 21 LOG NO 86602-17 86602-18 86602-19 86602-20 86602-21 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value ----------------------------------------------------------------------------------- PARAMETER 86602-17 86602-18 86602-19 86602-20 86602-21 ----------------------------------------------------------- ---------- ---------- Beryllium (6G10) Beryllium (6L'l0), ug/1 rreparation DRte Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date J>.nalyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 5.0 0. 30 10 --------------------------------------- <5.0 11.11. 96 · 11.12.96 1:0 llllE <0.30 11.12.96 11.13.96 1.0 1112J <10 11.11.96 11.12.96 l. 0 llllE ---------- 0.921 0.943 1000 11.11. 96 11.11.96 11. 12. 96 11.12. 96 1.0 1.0 llllE llllE 4 .11 4.15 5.00 11.12.96 11.12. 96 11.13. 96 11.13.96 l. 0 l. 0 1112J 1112J 980 1000 1000 11.11.96 11.11.96 11.12. 96 11.12.96 1.0 1.0 llllE llllE -------------------- -Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I n 0 0 g g I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I I D B I I I I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-B6602 Received: OB NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO 86602-17 86602-18 86602-19 86602-20 86602-21 PARAMETER Manganese Manganese (6010) (6010), Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ------------------------------,------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value 86602-17 86602-18 ug/1 5.0 <5.0 11.11.96 11.11. 96 11.12.96 11.12.96 1. 0 1. 0 llllE llllE 86602-19 86602-20 956 977 11.11.96 11.11.96 11.12.96 11.12. 96 1.0 1. 0 llllE llllE Nickel (6010), ug/1 40 <40 963 990 Preparation Date 11.11.96 11.11. 96 11.11.96 11.11. 96 Date Analyzed 11.12.96 11.12. 96 11.12.96 11.12.96 Dilution factor 1. 0 1.0 1.0 1.0 Batch ID llllE llllE llllE llllE Lead (7421) Lead (7421), ug/1 <3.0 <3. 0 49.1 47.7 Preparation Date 11.12. 96 11.12.96 11.12.96 11.12.96 Date Analyzed 11.13.96 11.13. 96 11.13.96 11.13.96 Dilution factor 1.0 1.0 1. 0 1.0 Batch ID 1112J 1112J 1112J 1112J ----------------------------------------------------------- ---------- Page 22 86602-21 1000 1000 50.0 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. ·5102 LaRoche Avenue• Savannah, GA 31404 • (912) 3_54-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO 86602-17 86602-18 86602-19 86602-20 86602-21 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 23 ----------------------------------------------------------------------------------- p;,RAMETER 86602-17 86602-18 86602-19 86602-20 86602-21 ----------------------------------------------------------- --------------------Antimony (7041) Antcimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed. Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Suspended Solids (160.2) 10 50 20 Suspended Solids (160.2), mg/1 5.0 Date Analyzed Batch ID --------------------------------------- <~0 11.11.96 11.14.96 1.0 llllM <50 11.11. 96 11.12. 96 1.0 llllE <20 11.11.96 11.12. 96 1.0 llllE <5.0 11.12.96 1112A ---------- 40.5 43.1 50.0 11.11.96 11.11.96 11.14. 96 11.14.96 1.0 1.0 llllM 1111M 960 984 1000 11.11.96 11.11.96 11.12. 96 11.12.96 1.0 1.0 llllE llllE 925 941 1000 11.11. 96 11.11.96 11.12.96 11.12.96 1.0 1.0 llllE llllE 97 93 100 11.12. 96 11.12.96 1112A 1112A -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I D 0 0 D I I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. m 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I I I I I I I I I B I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 LOG NO 86602-17 86602-18 86602-19 l6602-20 86602-21 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 24 ----------------------------------------------------------------------------------- PAF-1\METER 86602-17 86602-18 86602-19 86602-20 86602-21 ---··--------------------------------------------------------------------------- Merc·,·.ry (7470) Merc-Jry (7470), ug/1 0.20 <0.20 2.75 2.75 3.00 Preparation Date 11.11.96 11.11.96 11.11.96 Date Analyzed 11.12.96 11.12.96 11.12.96 Dilution factor 1.0 1.0 1.0 Batch ID llllS llllS llllS ------------------------------ 1 Laboratories In Sav~ntah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. NO.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 25 LOG NO 86602-22 86602-23 86602-30 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES LCS/LCSD % Recovery LCS Control Limit Method Blank PARAMETER 86602-22 86602-23 86602-30 65/65 % 10-232'% <1.0 Purgeable Halocarbons (8010) 1,1-Dichloroethene, ug/1 Trichloroethylene, ug/1 Chloroform, ug/1 1,1-Dichloroethane, ug/1 Cis/Trans-1,2-Dichloroethene, ug/1 Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 75/80 % 28-196 % <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <l. 0 7.6 10 76 % 12-152 % 11.15.96 1. 0 1113B 1E1115 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I D 0 D D I I luAs L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I I I I a D n D I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 131861125 REPORT OF RESULTS V LOG NO 86602-22 86602-23 86602-30 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- LCS/LCSD % Recovery LCS Control Limit Method Blank ---------------------------------------------·---- PARAMETER 86602-22 86602-23 86602-30 --------------------------------------- -------------------- Purgeable Aromatics (8020) Benz·ane, ug /] Toluerie, ug/1 70/80 % 70/85 % Total .xylenes, ug/1 Acetone, ug/1 Surroga~e -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Barium (6010) Barium (6010) Beryllium (6010) Beryllium (6010) Cadmium (7131) Cadmium (7131) Chromium (6010) Chromium (6010) Manganese (6010) Manganese (6010) 95/97 92/94 82/83 98/100 96/98 t t % t t ---------- 23-168 % 33-167 % 80-120 t 80-120 % 80-120,% 80-120 t 80-120 % ---------- <1.0 <1.0 <3.0 <10 32 30 107 % 41-150 % 11.15.96 1. 0 1113B 1Elll5 ---------- Page 26 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES I & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I Mr. Ronald Wallace Applied Earth Sciences, Inc. LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 . Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 27 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86602-22 LCS/LCSD % Recovery 86602-23 LCS Control Limit 86602-30 Method Blank ----------------------------------------------------------------------------------- PARAMETER Nickel (6010) Nickel (6010) Lead (7421) Lead (7421) Antimony (7041) Antimony (7041) Vanadium (6010) Vanadium (6010) Zinc (6010) Zinc (6010) Suspended Solids (160.2) Suspended Solids (160.2) Mercury (7470) Mercury (7470), ug/1 86602-22 ---------- 96/99 % 98/95 % 81/86 % 96/98 % 92/94 % 97/93 % 92/92 % ---------- 86602-:l3 86602-30 -------------------- 80-120 % 80-120 % 80-120 % Ii,· 80-120 % 80-120 % 75-125 % 80-120 % ---------- ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I D D 0 D 0 0 I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I I I I I I I u 0 I I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 28 DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED 86602-24 86602-25 Matrix Spike (MW-23) Result Matrix Spike (MW-23) Duplicate Result PARAMETER Purgeable Halocarbons (8010) 1,1-Dichloroethene, ug/1 Trichloroethylene, ug/1 Surrogate -Bromochlorom1=thane Surrogate -Expected Value Surrogate -% Actual Recove ... -y Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Purgeable Aromatics (8020) 86602-24 13 12 8.9 10 89 % 12-152 % 11.16.96 1.0 1113B 1Elll5 Benzene, ug/1 14 Toluene, ug/1 18 Surrogate -a,a,a-Trifluorotoluene 28 Surrogate -Expected Value 30 Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 93 % 41-150 % 11.16.96 1.0 1113B 1Elll5 86602-25 13 12 8.9 10 89 % 12-152 % 11.16.96 1.0 111:lB 1Elll5 12 15 29 30 97 % 41-150 % 11.16.96 1. 0 1113B 1El115 11-06-96/1600 11-06-96/1600 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS Code: 102261125 Page 29 DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED -------------------------------------------------------------------- 86602-24 Matrix Spike (MW-23) Result 86602-25 Matrix Spike (MW-23) Duplicate.Result 11-06-96/1600 11-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID .. 86602-24 ---------- 1960 11.11. 96 11.12. 96 1.0 llllE 46.1 11.11.96 11.12.96 1.0 llllE 4.32 11.12. 96 11.13.96 1.0 1112J 1990 11. 11. 96 11.12.96 1.0 llllE ---------- 86602-25 ---------- 1920 11.11.96 11.12.96 1.0 llllE ' 46.1 11.11.96 11.12.96 1.0 llllE 4.31 11.12.96 11.13.96 1.0 1112J 1980 11.11.96 11.12. 96 1. 0 llllE ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D D D 0 0 0 D g 11 I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 0 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I 0 u I I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: OB NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 30 DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED 86602-24 86602-25 Matrix Spike (MW-23) Result Matrix Spike (MW-23) Duplicate Result 11-06-96/1600 11-06-96/1600 ------------------------------------------------------------------------------------------ PARAMETER Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Antimony ( 7 041) Antimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-24 ---------- 486 11.11.96 11.12.96 1.0 ll.llE 491 11.11.96 11.12.96 1. 0 llllE 48.9 11.12.96 11.13.96 1.0 1112J 47.1 11.11.96 11.14.96 1.0 llllM ---------- 8(,602-25 ---------- 474 11.11.96 11.1~.96 l.0 llllE 483 11.11.96 11.12.96 1.0 llllE 48.3 11.12.96 11.13.96 1.0 1112J 44.0 11.11.96 11.14.96 1. 0 11110 ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS LOG NO_ SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES 86602-24 Matrix Spike (MW-23) Result 86602-25 Matrix Spike (MW-23) Duplicate Result PARAMETER Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Mercury (7470) Mercury (7470), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86602-24 ---------- 495 11.11.96 11.12. 96 1.0 llllE 462 11.11.96 11.12.96 1.0 llllE 0.94 11.11.96 11.12.96 1.0 llllS ---------- 86602-25 ---------- :486 11.11. 96 11.12. 96 1.0 llllE 455 11.11.96 11.12. 96 1. 0 llllE 0.91 11.11.96 11.12.96 1,0 llllS ----------ADD'L SAMPLE VOLUME NOT SUPPLIED FORSS MS/MSD Page 31 DATE/ TIME SAMPLED ----------------------. ll-06-96/1600 ll-06-96/1600 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA u D 0 g Ii I' I I I II II II II II II • s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. m I I • I D I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: 56-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102961125 REPORT OF RESULTS Page 32 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86602-26 Matrix Spike (MS) Expected Value 86602-27 MS/MSD \ Recovery 86602-28 MS\ Recovery Limits 86602-29 MS\ RPD (Limits) ----------------------------------------------------------------------------------- PARAMETER Purgeable Halocarbons (8010) 1,1-Dichloroethene, ug/1 Trichloroethylene, ug/1 Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Barium (6010) Barium (6010), ug/1 Beryllium (6010) Beryllium (6010), ug/1 Cadmium (7131) Cadmium (7131), ug/1 Chromium (6010) Chromium (6010), ug/1 86602-26 ---------- 20 20 20 20 2000 50 5.00 2000 [06602-27 ---·------ 65/65 \ 60/60 \ 70/60 \ 90/75 \ 98/96 \ 92/92 \ 86/86 \ 100/99 \ 86602-28 86602-29 -------------------- 10-232 \ 0 (<20) \ 28-196 \ 0 (<2C) \ 23-168 \ 15(<34) \ 33-167 \ 18 (<34) \ 75-125 \ 2.1 (<20) \ 75-125 \ 0(<20) \ 75-125 \ 0 (<20) \ 75-125 \ l.0(<20) \ Manganese (6010) I Manganese (6010), ug/1 Nickel (6010) 500 97/95 \ 75-125 \ 2.1(<20) \ I I I I Nickel (6010), ug/1 Lead (7421) Lead (7421), ug/1 Antimony (7041) Antimony (7041), ug/1 500 50.0 50.0 ---------- 98/97 \ 98/97 \ 94/88 \ ---------- 75-125 \ l.0(<20) \ 75-125 \ l.0(<30) \ 75-125 \ 6 .6 (<20) t -------------------- 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH . LABORATORIES I & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah; GA 31404 • (912) 354-7858 • Fax (912) 352-0165 m Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86602 Received: 08 NOV 96 Reported: 20 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 102261125 REPORT OF RESULTS Page 33 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------- 86602-26 Matrix Spike (MS) Expected Value 86602-27 MS/MSD \ Recovery 86602-28 MS\ Recovery Limits 86602-29 MS \ RPD (Limits) -----------------------------------------------------------------------------------PARAMETER Vanadium (6010) Vanadium (6010), ug/1 Zinc (6010) Zinc (6010), ug/1 Mercury (7470) Mercury (7470), ug/1 Methods: EPA SW-846 86602-26 86602-27 86602-28 ------------------------------ 500 99/97 \ 75-125 \ 500 92/91 \ 75-125 \ 1.00 94/91 \ 75-125 \ ------------------------------ Final Page Of Report 86602-29 ---------- 2.0(<20) \ 1.1(<20) \ 3.3(<20) \ ---------- ."Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile_. AL • New Orleans, LA D 0 g I I I II II -------------IW!!I ~alNumoer 4~ljiiil - SL SAVANNAH LABORATORIES ~2 LaRocheAvenue, Savannah, GA31404 Phone: (912) 354-7858 Fax: (912) 352-0165 & ENVIRONMENTAL SERVICES, INC. D 2846 Industrial Plaza Drive, Tallahassee. FL 32301 Phone: (904) 878-3994 Fax: (904) 878-9504 D 414 SW 12th Avenue, Deerfield Beach, FL33442 Phone: (305) 421-7400 Fax: (305) 421-2584 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD D 900 Lakeside Drive, Mobile,AL36693 Phone: (205) 666-6633 Fax: (205) 666-6696 06712 Benjamin Road, Suite 100, Tampa, FL33634 Phone: (813) 885-7427 Fax: (813) 885-7049 D 100Alpha Drive, Suite 110, Destrehan, LA 70047 Phone: (504) 764-1100 Fax: (504) 725-1163 PROJECT REFERENCE PROJECT NO. P.O.NUMBER MATRIX l PAGE loF ()1Acc,,.l I '7>oe .. ,,.~, /9 o--o,:,r,, -01 TYPE I REQUIRED ANALYSES PROJECT LOC. SAMPLER(s) NAME PHONE 7?a-y,;Jl'-'('7/f I! ., (State) ' I:)~ ERtc FAX I ~ 0 t-Q.'r,"' fJ c., oi20ct 7 Jo -'(o</-7i' 9? .I' I\J ~ ~' {,.:. CLIENT NAME CLIENT PROJECT MANAGER " 0 .t; p STANDARD ~-\'\ " /, f\l 0 □REPORT Af(lt.~ p -~ .. ...i ~ f, 0 'i,/1\ DELIVERY ~Tli sc, ·---Vlk. <. A c (; it 'c,,,/ d' ' (\ ' f\ CLIENT ADDRESS (CITY, STATE, ZIP) A...A '"'1 J.~§ .:J O "v ~ 0 (. S-l.f Tlv.. C..rN-<, \\;. □ EXPEDITED REPCRT c),:~ 1./00 #Jo r~s.3,. c.. 30<.'l~ '£'~ .5' °ll l• DEL IVEAY(surcharge) J ~ 0 Jr,0& ii I I I I I I I I I / Date Due: SAMPLE SL J. ~ 'ti DATE TIME NO. SAMPLE IDENTIFICATION ,?:o NUMBER OF CONTAINERS SUBMITTED REMARKS "''SC 11/i../"11. 'i:oo mu-11 ~ X X ¥ "/<.('/ L /o:s-o /11 LI -'J J X' X: )( •·/ ~1 q1., I I :LI,-, mw -19 ~ ..v X r x 11/c(~,; "l...'Yr mt..1--,A I( X )(' ,i/,;.,,(, c/;oo /111\-Z,] /If :r/d,:J X X )(' K /1/4/21. '/:Ju /11, I-tJ X ')( )( I( X' 1, h 1111 l/'.'-15 rn ir1 -1. 1--" .f ,/ y ~ 11/7k. 7.'oo /IA S.,..,,c...-2" {:.. Ii ' -:It' y u/-,/t;L 7,~o ,1" s .. .,,c.,..r_. e..C.r:. v V X" x-, . , ,11/7/91-'J'.,~ Ii. IU .,c,,.... 7;...t ) 1,,-x-X' 1'/,.,111,, ,·,< I n.L--'T ~ .f' ) X X "l?ir~ 7: 2c Ult.. /11,~ p.f~ ' 'V )( ..-1" 11/?/{Jc 1fl. If h,J,:_ L" l .v RELINQUI ~ED BY: (Si,iNATURE) DAT ~ TIME RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME 4A.,,;, /) 11,, ✓I llh rq 1:30 RECEIVED BY: (SIGMTURE) DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME REC.EIVED BY: (SIGNATURE) DATE TIME LABORATORY USE ONLY RECEIVED FOR LABORATORY BY: (SIGNATURE) DATE TIME CUSTODY INTACT CUSTODY SEAL NO. SL LOG NO. LABORATORY REMARKS: , ·~1 ..\ JlcJ.,:,,,-:,.-. \ \• oi .q {: [X]YES □ ',-lot t! ;if t;·ii:·~ :~\_~.' .. ~. . '2fj Uf,O'J_ ,111\.,-~ .... >~ .. -.,. -_ . ··: , . q: l'l mv~--•,-,,.;· . ., ... ·. . ... . . ' •.-' ....J .,: z (') a: 0 I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. g 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I H I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 1 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED -------------------------------------------------- 86635-1 86635-2 86635-3 86635-4 86635-5 MW-21 U.Dockery Inf. U.Dockery Eff MW-15 MW-25 11-07-96/0945 11-07-96/1045 11-07-96/1045 11-07-96/1150 11-07-96/1445 ------------------------------------------------------------------------ P.\RAMETER 86635-1 86635-2 86635-3 86635-4 86635-5 ------------------------------------------------------------------------------- Pu,3eable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Traris-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value S~rrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID <1.0 1. 5 <1.0 ug/1 <l. O <2.0 <1.0 <1.0 <1.0 <1.0 8.9 10 89 \ 12-152 \ 11.18.96 1.0 1114B 1Blll8 <10 <10 240 <10 <20 <10 54 <10 <10 91 100 91 \ 12-152 % 11.16.96 10 1114B 1Blll5 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 8.1 10 81 % 12-152 \ 11.18.96 1. 0 1114B 1Blll8 <25 29 1000 <25 <50 <25 290 <25 <25 220 250 88 % 12-152 % 11.18.96 25 1114B 1Blll8 <1.0 <1.0 1.6 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 8.5 10 85 \ 12-152 % 11.15.96 1.0 1114B 1Blll5 --------------------------------------- ---------- ---------- -------------------- 1 Laboratories in s:;annah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA .9 L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO, S6-86635 Received, 11 NOV 96 Reported, 21 NOV 96 Client PO. No., 190-00001-01 Project, 190-00001-01/MACON DOCKERY Sampled By, Client REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES Code, 100061129 Page 2 DATE/ TIME SAMPLED --------------------------------------------------86635-1 86635-2 86635-3 86635-4 86635-5 MW-21 U.Dockery Inf. U.Dockery Eff MW-15 MW-25 11-07-96/0945 11-07-96/1045 11-07-96/1045 11-07-96/1150 11-07-96/1445 ------------------------------------------------------------------------PARAMETER 86635-1 86635-2 86635-3 8663!:-4 -------------------------------------------------------------------··- Purgeable Aromatics (8020) Benzene, ug/1 <1.0 Toluene, ug/1 1.4 Total Xylenes, ug/1 Acetone, ug/1 <3.0 <10 29 30 97 % Surrogate -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit 41-150 % Date Analyzed Dilution Batch ID Clock ID factor Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed .Dilution factor Batch ID 11.18.96 1. 0 1114B 1Blll8 <50 11.12.96 11.13.96 1. 0 1112K ---------- <10 <10 <30 2100* 280 300 93 % 41-150 % 11.16.96 10 1114B 1B1115 61 11. 12. 96 11.13.96 1.0 1112K ---------- <1.0 <25 <1.0 <25 <3.0 <75 <10 <250 30 730 30 750 100 % 97 % 41-150 % 41-150 % 11.18.96 11.18.96 1.0 25 1114B 1114B 1B1118 1B1118 59 140 11, 12. 96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112K 1112K -------------------- 866)5-5 ----------,, .-<1.0 <1.0 <3.0 <10 32 30 107 % 41-150 % 11.15.96 1.0 1114B 1B1115 140 11. 12. 96 11.13.96 1. 0 1112K ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I D D I I I II II II II 11 I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I g 0 I I I I I I I I I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-96635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES Code: 190161122 Page 3 DATE/ TIME SAMPLED --------------------------------------------------96635-1 86635-2 86635-3 86635-4 86635-5 MW-21 U.Dockery Inf. U.Dockery Eff MW-15 MW-25 ll-07-96/0945 ll-07-96/1045 ll-07-96/1045 ll-07-96/1150 ll-07-96/1445 ------------------------------------------------------------------------------------------ PARAMETER 86635-1 86635-2 86635-3 96635-4 96635-5 -------------------------------------------------------------------------------Beryllium (6010) Beryllium (6010), ug/1 <5.0 <5.0 <5.0 <5.0 <5.0 Preparation Date· 11.12.96 11.12.96 11.12.96 ·11.12. 96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1.0 1.0 l. 0 1.0 Batch ID 1112K 1112K 1112K 1112K 1112K Cadmium (7131) Cadmium (7131), ug/1 <0.30 <0.30 <0.30 <0.30 <0.30 Preparation Date 11.12. 96 11.12.96 11.12.96 11.12.96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor l. 0 1.0 1.0 1.0 1.0 Batch ID lll2L lll2L lll2L lll2L lll2L Chromium (6010) Chromium (6010), ug/1 <10 19 15 <10 <10 Preparation Date 11.12.96 11.12. 96 11.12.96 11.12.96 11.12. 96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1.0 1.0 1.0 1.0 Batch ID 1112K 1112K 1112K 1112K 1112K ------------------------------------------------------------------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I C' SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, _GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO, No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES Page 4 DATE/ TIME SAMPLED -------------------------------------------------- 86635-1 86635-2 86635-3 86635-4 86635-5 MW-21 U. Dockery Inf. U.Dockery Eff MW-15 MW-25 ll-07-96/0945 ll-07-96/1045 ll-07-96/1045 ll-07-96/1150 ll-07-96/1445 ------------------------------------------------------------------------------------------PARAMETER Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-1 ---------- 8.3 11.12.96 11.13.96 1.0 1112K <40 il.12.96 11.13.96 l. 0 1112K <3.0 11.12.96 11.13.96 l. 0 1112L ---------- 86635-2 ---------- 9.5 11.12. 96 11.13. 96 1.0 1112K <40 11.12.96 11.13.96 1.0 1112K <3.0 11.12. 96 11.13.96 1.0 1112L ---------- 86635-3 8663,5-4 86635-5 ------------------------------ <5.0 200 110 11.12.96 11.12. 96 11.12. 96 11.13.96 11.13.96 11.13.96 1.0 1.0 1.0 1112K 1112K 1112K <40 <40 <40 11.12. 96 11.12.96 11.12. 96 11.13,96 11.13.96 11.13.96 1.0 1.0 1.0 1112K 1112K 1112K <3.0 430 <3.0 11.12.96 11.12.96 11.12.96 11.13.96 11.14.96 11.13.96 l. 0 10 1.0 1112L lll2L lll2L ------------------------------ Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ,-,, ..:: I D I I II II II II II II I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I D I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS Code: 154761125 Page 5 LOG NO 86635-1 86635-2 86"35-3 86635-4 86635-5 PARAMETER DATE/ SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED -------------------------------------------------- MW-21 U.Dockery Inf. U.Dockery Eff MW-15 MW-25 ll-07-96/0945 ll-07-96/1045 ll-07-96/1045 ll-07-96/1150 ll-07-96/1445 ------------------------------------------------------------------------ 86635-1 86635-2 86635-3 86635-4 86635-5 --------------------------------------- ---------- ------------------------------ Antimor y (7041) Antimony (7041), ug/1 <10 <10 <10 <10 <10 Preparation Date 11.13. 96 11.13.96 11.13.96 11.13.96 11.13.96 Date Analyzed 11.14.96 11.14.96 11.14. 96 11.14.96 11.14.96 Dilution factor 1.0 l. 0 1.0 1.0 1.0 Batch ID 1113G 1113G 1113G 1113G 1113G Vanadium (6010) Vanadium (6010), ug/1 <50 <50 <50 <5.0 <50 Preparation Date 11.12.96 11.12.96 11.12.96 11.12.96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 l '. 0 1.0 1.0 1.0 Batch ID 1112K 1112K 1112K 1112K 1112K Zinc (6010) Zinc (6010), ug/1 <20 <20 <20 <20 20 Preparation Date . 11. 12. 96 11.12.96 11.12.96 11.12.96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor l. 0 l. 0 1.0 1.0 1.0 Batch ID 1112K 1112K 1112K 1112K 1112K Suspended Solids (160.2) Suspended Solids (160. 2), mg/1 11 <5.0 <5.0 9.0 45 Date Analyzed 11.12.96 11.12.96 11.12.96 11.12.96 11.12. 96 Batch ID lll2C lll2C lll2C lll2C lll2C ------------------------------------------------------------------------------- 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc .. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 6 LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES 86635-6 86635-7 86635-8 86635-9 L.Dockery·Inf. L. Dockery Eff MW-16 MW-24 PARAMETER Purgeable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethehe, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 86635-6 <2.0 69 28 ug/1 <2.0 <4.0 <2.0 38 5.8 <2.0 19 20 95 % 12-152 % 11.16.96 2.0 1114B 1Bll15 86635-7 86635-8 <1.0 <1.0 <1. 0 37 <1.0 24 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 <1.0 50 <1.0 2.6 <1.0 <1.0 8.5 9.8 10 10 85 % 98 % 12-152 % 12-152 % 11.15.96 11.15.96 1.0 1.0 1114B 1114B 1Blll5 1Blll5 -------------------- DATE/ TIME SAMPLED 11-07-96/1530 11-07-96/1530 ll-07-96/1540 11-07-96/1710 86635-9 <1.0 7.1 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 9.2 10 92 % 12-152 % 11.15.96 1.0 1114B 1Blll5 ---------- I 0 I' I, II II II II II I I I Laboratories in ;avannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA 1 " I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. m 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I D i I I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES Page 7 DATE/ TIME SAMPLED LOG NO 86635-6 86635-7 86635-8 86635-9 -------------------------------------------------- L. Dockery Inf. L.Dockery Eff MW-16 MW-;>4 11-07-96/1530 ll-07-96/1530 ll-07-96/1540 11-07-96/1710 -------------------------------------------------- PARAMETER 86635-6 --------------------------------------- Purgeable Aromatics (8020' Benzene, ug/1 Toluene, ug/1 Total Xylenes, ug/1 Acetone, ug/1 <2.0 <2.0 <6.0 <20 60 60 100 \ Surrogate -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit 41-150 \ Date Analyzed Dilution Batch ID Clock ID factor Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 11.16.96 2.0 1114B 1Blll5 <50 11.12.96 11.13.96 1.0 1112K ---------- 86635-7 <1.0 3.4 <3.0 <10 31 30 103 \ 41-150 \ 11.15.96 1.0 1114B 1Blll5 <50 11.12.96 11.13.96 1.0 1112K ---------- 86635-8 86635-9 <1.0 <1.0 1.1 l. 2 <3.0 <3.0 <10 <10 31 30 30 30 103 \ 100 \ 41-150 \ 41-150 ' 11.15.96 11.15.96 1.0 1.0 1114B 1114B 1Blll5 1B1115 830 82 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112K 1112K -------------------- 1 Laboratories in.}avannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Applied Earth Sciences, Inc. Client PO. NO.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS LOG NO 86635-6 86635-7 86635-8 r6635-9 SAMPLE DESCRIPTION, LIQUID SAMPLES L.Dockery Inf. L.Dockery Eff MW-16 MW-24 PARAMETER Ber:llium (6010) Ber_rllium (6010), ug/1 Pref~ration Date Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-6 ---------- <5.0 11.12.96 11.13.96 1.0 1112K <0.30 11.12.96 11.13.96 1. 0 1112L <10 11.12.96 11.13.96 1. 0 1112K ---------- 86635-7 86635-8 ---------- - - - - - - - - - - <5.0 <5.0 11.12.96 11.12.96 ll.i3.96 11.13.96 1. 0 1. 0 1112K 1112K <0.30 0.47 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112L 1112L <10 95 11.12. 96 11.12.96 11.13.96 11.13.96 1. 0 1.0 1112K 1112K -------------------- Page 8 DATE/ TIME SAMPLED 11-07-96/1530 ll-07-96/1530 11-07-96/1540 11-07-96/1710 86635-9 ---------- <5.0 11.12.96 11.13 .96 1.0 1112K <0.30 11.12. 96 11.13. 96 1.0 1112L <10 11.12.96 11.13.96 1.0 1112K ---------- I D 1· I II II II II I I I I I I Laboratories in }avannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC . • I I I I D D D I I I I I I H 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 9 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED -------------------------------------------------------------------- 86635-6 L.Dockery Inf. 86635-7 L.Dockery Eff 86635-8 MW-16 86635-9 MW-24 11-07-96/1530 11-07-96/1530 11-07-96/1540 11-07-96/1710 ------------------------------------------------------------------------------------------ PARAMETER Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-6 ---------- 230 11.12.96 11.13.96 1.0 1112K <40 11.12.96 11.13.96 1.0 1112K <3.0 11.12.96 11.13.96 1.0 lll2L ---------- 86635-7 ----· ----- r::5. 0 11.1.2.96 11.13. 96 1.0 1112K <40 11.12.96 11.13.96 1.0 1112K <3. 0 11.12.96 11.13.96 1.0 lll2L ---------- 86635-8 86635-9 -------------------- 3200 2700 11.12. 96 11.12.96 .,· 11.13. 96 11.13.96 1.0 1.0 1112K 1112K 160 <40 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112K 1112K 38 <3.0 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 lll2L l112L -------------------- I Laboratories infavannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. NO.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 181061122 REPORT OF RESULTS Page 10 DATE/ LOG NO 86635-6 86635-7 86635-8 86635-9 SAMPLE DESCRIPTION, LIQUID SAMPLES L.Dockery Inf. L.Dockery Eff MW-1.6 MW-24 TIME SAMPLED 11,07-96/1530 11-07-96/1530 11-07-96/1540 11-07-96/1710 PARAMETER 86635-6 86635-7 86635-8 866.15-9 Antimony (7041) Antimony (7041), ug/1 <10 <10 <10 <,.O Preparation Date 11.13.96 11.13.96 11.13.96 11.13 .9,, Date Analyzed 11,14.96 11.14.96 11.14. 96 11.14.96 Dilution factor 1.0 1. 0 1.0 1.0 Batch ID 1113G 1113G 1113G 1113G vanadium (6010) Vanadium (6010), ug/1 <50 <50 270 <50 Preparation Date 11.12. 96 11.12.96 11.12. 96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1. 0 1.0 1.0 Batch ID 1112K 1112K 1112K 1112K Zinc (6010) Zinc (6010), ug/1 <20 <20 390 <20 Preparation Date 11.12.96 11.12. 96 11.12. 96 11.12.96 Date Analyzed 11.13.96 11.13.96 11.13.96 11.13.96 Dilution factor 1.0 1. 0 1. 0 1.0 Batch ID 1112K 1112K 1112K 1112K ·Suspended Solids (160.2) Suspended Solids (160. 2), mg/1 <5.0 <5.0 2100 58 Date Analyzed 11.12.96 11.12.96 11.12.96 11.12. 96 Batch ID 1112C 1112c 1112C 1112C --------------------------------------- - - - - - - - - - - -------------------- u 0 0 u I, I I Laboratories in,~avannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 11 DATE/ SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-10 MW-15 ll-07-96/1150 ------------------------------------------------------------------------------------------ PARAMETER I ----------------------------- Mercury (7470) 86635-10 Mercury (7470), ug/1 I Preparation Date Date Analyzed I I I I a B I 0 Di;tution factor Batch ID r 3.5 11.12.96 11.13.96 1.0 1112S 0 Laboratories ln(~avannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA 'SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 12 DATE/ SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED -------------------------------------------------------------------- 86635-11 MW-15R 11-07-96/1200 11 ------------------------------------------------------------------------------------------II ·PARAMETER 86635-11 Purgeable Halocarbons (8010) Chloroform, ug/1 <50 1,1-Dichloroethane, ug/1 <50 1,1-Dichloroethene, ug/1 1600 Cis/Trans-1,2-Dichloroethene, ug/1 <50 Methylene chloride <100 (Dichloromethane), ug/1 Tetrachloroethene, ug/1 <50 1,1,1-Trichloroethane, ug/1 400 Trichloroethylene, ug/1 <50 Vinyl chloride, ug/1 <50 Surrogate -Bromochloromethane 420 Surrogate -Expected Value 500 Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 84 % 12-152 % 11.19.96 50 1114B 1Blll9 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I-~/ .:. . D D D D D D 0 0 0 0 0 I I I I I I I I D D D D I R I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 L.aRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES Page 13 DATE/ TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-11 MW-15R ll-07-96/1200 ------------------------------------------------------------------------------------------ PARAMETER Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Total Xylenes, ug/1 Acetone, ug/1 Surrogate - a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-11 <50 <50 <150 <500 1400 1500 93 % 41-150 % 11.19.96 50 1114B 1Blll5 140 11.12.96 11.13. 96 1.0 1112K <5.0 11.12.96 11.13.96 1.0 1112K Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ,"7 '- SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES Page 14 DATE/ TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-11 MW-15R 11-07-96/1200 ------------------------------------------------------------------------------------------PARAMETER Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-11 <0.30 11.12.96 11.13.96 1.0 1112L <10 11.12. 96 11.13.96 1.0 1112K 170 11.12. 96 11.13.96 1. 0 1112K <40 11.12.96 11.13.96 1.0 1112K Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA <. I 0 0 D D D I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. g I I I I B D D H B D I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS Code: 180161122 Page 15 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIMI:: SAMPLED ------------------------------------------------------------------------------------------ 86635-11 MW-15R ll-07-96/1200 ------------------------------------------------------------------------------------------ PARAMETER Lead (7421) Lead (74_21), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Antimony (7041) Antimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-11 340 11.12.96 11.14.96 10 lll2L <10 11.13.96 11.14.96 1.0 1113G <50 11.12.96 11.13.96 1.0 1112K <20 11.12.96 11.13.96 1.0 1112K I Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA v_., SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. NO.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 16 DATE/ TIME SAMPLED I D D LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES 86635-11 MW-15R ----------------------0 ll-07-96/1200 PARAMETER Mercury (7470) Mercury (7470), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-11 2.3 11.12. % 11.13 .9,i 1.0 lll2S Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA .. , :i.: 0 D D 1· I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I I I 0 D R B I w I I I I 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: ll NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 17 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-12 MW-l6R ll-07-96/1550 ------------------------------------------------------------------------------------------PARAMETER Purgeable Halocarbons (8010) Chloroform, ug/1 l,l-Dichloroethane, ug/1 l,l-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 l,l,l-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochlorornethane Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 86635-12 <l.0 32 19 ug/1 <l. 0 <2.0 <l.0 42 2.0 <l.0 9.5 10 95 \ 12-152 \ ll.15.96 l.O lll4B lBlll5 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES Page 18 DATE/ TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-12 MW-16R ll-07-96/1550 ------------------------------------------------------------------------------------------ PARAMETER 86635-12 Purgeable Aromatics (8020) Benzene, ug/1 <l.O Toluene, ug/1 2.0 Total Xylenes, ug/1 <3.0 Acetone, ug/1 <10 Surrogate -a,a,a-Trifluoroto.l.uene 31 Surrogate -Expected Value 30 Surrogate -% Actual Recovery 103 \ Surrogate -Control Limit 41-150 % Date Analyzed 11.15.96 Dilution factor 1.0 Batch ID 1114B Clock ID Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 1Blll5 780 11.12.96 11.13.96 1.0 1112K <5.0 11.12. 96 11,13.96 1.0 1112K n D D 0 0 u g I Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ~ 11 ~ . i I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I u I I I I u 0 D B R 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS Code: 180161122 Page 19 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------------ 86635-12 MW-16R 11-07-96/1550 ------------------------------------------------------------------------------------------ PARAMETER Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-12 0.45 11.12.96 11.13.96 1.0 1112L 89 11.12.96 11.13.96 1. 0 1112K 2800 11.12.96 11.13.96 1. 0 1112K U Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed 160 11.12.96 11.13.96 1.0 1112K I I DilU:tion factor Batch ID I Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 20 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED 86635-12 MW-l6R ll-07-96/1550 PARAMETER Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID A,timony (7041) Antimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-12 44 11.12.96 11.14. 96 1.0 l112L <10 11.13.96 11.14. 96 1.0 1113G 250 11.12.96 11.13.96 1.0 1112K 340 11.12.96 11.13.96 1.0 1112K Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D D D D 0 0 0 g I I I 0 I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client REPORT OF RESULTS Code: 180161122 Page 21 LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES DATE SAMPLED ------------------------------------------------------------------------------------------ 86635-13 Trip Blank 11-07-96 ------------------------------------------------------------------------------------------ PARAMETER 86635-13 Purgeable Halocarbons (8010) Chloroform, ug/1 1,1-Dichloroethane, ug/1 1,1-Dichloroethene, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,l-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID <l.0 <l.0 <l.0 ug/1 <l. 0 <2.0 <1.0 <l.0 <1.0 <l.0 8.5 10 85 \ 12-152 \ 11.15.96 1.0 1114B 1Blll5 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA .•, SL SAVANNAH LABORATORIES E & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 0 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 22 LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES DATE SAMPLED 86635-13 Trip Blank 11-07-96 PARAMETER Purgeable Aromatics (8020) Benzene, ug/1 Toluen~~, ug/1 Total Xylenes, ug / 1. Acetone, ug/1 86635-13 <l.0 4.6 <3.0 <10 30 30 100 % Surrogat1:.: -a, a, a-T1 ifluorotoluene Surrogate Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit 41-150 % 11.15.96 Date Analyzed Dilution factor Batch ID Clock ID 1.0 1114B 1Blll5 Laboratories in Sava~nnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I 1. I I II II II II II ll I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fa_x (912) 352-0165 D I I u I I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 23 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86635-14 Practical Quantitation Limits 86635-15 Method Blank Result 86635-16 86635-17 86635-18 Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value ----------------------------------------------------------------------------------- PARAMETER 86635-14 86635cl5 86635-16 ,86635-17 86635-18 --------------------------------------- ---------- ------------------------------ Purgeable Halocarbons (8010) Chloroform, ug/1 <l.O 1.0 1,1-Dichloroethane, ug/1 <1.0 1.0 l. 0 l, 1-Dichloroethene, ug/1 <l. O 11 11 20 Cis/Trans-1,2-Dichloroethene, <l.O ug/1 1.0 Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,l-Trichloroethane, ug/1 Trichloroethylene, ug/1 Vinyl chloride, ug/1 Chlorobenzene, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 2.0 1.0 1.0 1.0 1.0 1.0 --------------------------------------- <2.0 <l.0 <l.0 <1.0 <l.0 <l.0 7.7 10 77 \ 12-152 \ 11.15.96 1.0 1114B 1B1115 18 18 8.1 10 81 \ 12-152 \ 11.15.96 1.0 1114B 1Blll5 ---------- 17 17 8.0 10 80 \ 12-152 \ 11.18.96 1.0 1114B 1B1118 ---------- 20 20 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO, S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project, 190-00001-01/MACON DOCKERY Sampled By, Client Code, 180161122 LOG NO 86635-14 86635-15 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result 86635-16 Lab Control Standard (LCS) Result 86635-17 LCS Duplicate Resnlt 86635-18 LCS Expected Value -------------------------------------------------------------------- Page 24 PARAMETER 86635-,4 86635-15 86635-16 86635-17 86635-18 ------------------------------------------------------------------------------- Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Total Xylenes, ug/1 Acetone, ug/1 Surrogate -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 1.0 1.0 3.0 10 50 <1.0 <l.0 <3.0 <10 30 30 100 % 41-150 % 11.15.96 1.0 1114B 1Bll5 <50 11.12.96 11.13.96 1.0 1112K 15 17 30 30 100 % 41-150 % 11.15.96 1.0 1114B 1Blll5 1010 11.12.96 11.13.96 1.0 1112K 15 17 28 30 93 % 41-150 % 11.18.96 1.0 1114B 1Blll8 20 20 1020 1000 11.12.96 11.13.96 1.0 1112K ,Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA . .., g u I I. II II II II II 11 I I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I I D I I I I B I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 LOG NO 86635-14 86635-15 86635-16 86635-17 86635-18 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 25 ----------------------------------------------------------------------------------- PARAMETER 86635-14 86635-15 86635-16 86635-17 86635-18 --------------------------------------- ---------- ------------------------------Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 5.0 0.30 10 <5.0 11.12.96 11.13.96 1.0 1112K <0.30 11.12.96 11.13.96 1. 0 1112L <10 11.12.96 11.13.96 1. 0 1112K 974 979 1000 11.12. 96 11.12.96 11.13. 96 11.13.96 1.0 1.0 1112K 1112K 4.32 4.32 5.00 11.12.96 11.12. 96 11.13.96 11.13. 96 1.0 1.0 1112L 1112L 1010 1010 1000 11.12. 96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112K 1112K I ----------------------------------------------------------- 1 I I I Laboratories in Savcnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 LOG NO 86635-14 86635-15 86635-16 86635-17 86635-18 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 26 ----------------------------------------------------------------------------------- PARAMETER 86635-14 86635-15 86635-16 86635-17 86635-18 --------------------------------------- ------------------··---------------------Manganese (6010) Manganese (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 5.0 40 3.0 --------------------------------------- <5.0 11.12.96 11.13. 96 1. 0 1112K <40 11.12.96 11.13. 96 LO 1112K <3. 0 11.12.96 11.13.96 1.0 1112L ---------- 1020 1020 1000· 11.12.96 11.12.96 11.13.96 11.13.96 1.0 1.0 1112K 1112K 1030 1030 1000 11.12. 96 11.12.96 11.13.96 11.13. 96 1. 0 1.0 1112K 1112K 49.0 48.0 50.0 11.12.96 11.12.96 11.13. 96 11.13.96 1.0 1.0 1112L 1112L -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ,! ·- D D 0 I I I I I I II El II II II I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I D I B I I I I I I I I I I I LOG NO: S6-86635 Received: ll NOV 96 Reported: 21 NOV 96 Mr. Ronald Wallace Applied Earth Sciences, Inc. Client PO. No.: 190-00001-0l 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO 86635.-14 86635-15 86635-16 86635-17 866:35-18 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value Page 27 ----------------------------------------------------------------------------------- PARAJ.:ETER 86635-14 86635-15 86635-16 86635-17 86635-18 ------------------------------------------------- ------------------------------ Antimony ( 7 04 l) Ant~mony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Vanadium ( 6 010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID ----------------------------- 10 <10 ll.13.96 ll.14.96 l.0 lll3G 50 <50 ll.12.96 ll.13.96 l.0 lll2K 20 <20 ll.12. 96 ll.13.96 l.0 ll12K -------------------- 41. 3 ll.13.96 ll.14.96 l.0 lll3G 980 ll.12.96 ll.13.96 l.0 lll2K 994 ll .12. 96 ll .13. 96 l.0 lll2K ---------- 39.8 ll.13.96 ll.14.96 l. 0 lll3G so.a 984 1000 ll.12.96 ll.13.96 l.0 1112K 997 ll.12.96 ll.13.96 l. 0 lll2K 1000 ! 1. Laboratories in Sav?nah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Mr. Ronald Wallace Applied Earth Sciences, Inc. Client PO. No.: 190-00001-01 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 Project: 190-00001-0l/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS LOG NO 86635-14 86635-15 86635-16 86635-17 86635-18 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value --------------------------------------------------PARAMETER Mercury (7470) Mercury (7470), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Suspended Solids (160.2) 86635-14 86635-15 86635-16 -------------------- ---------- 0.20 <0.20 11, 12. 96 11.13.96 1.0 lll2S 2.63 11.12.96 11.13.96 1.0 lll2S Suspended Solids (160.2), mg/1 5.0 <5.0 11.12.96 lll2C 103 Date Analyzed 11. 12. 96 Batch ID lll2C --------------------------------------- 86635-17 2.51 11.12.96 11.13.96 1.0 lll2S 102 11.12.96 lll2C Page 28 86635-18 3.JO 100 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mo~ile, AL • New Orleans, LA D I I I, II II II II II II I I I I I I I R I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 29 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86635-19 LCS/LCSD % Recovery 86635-20 LCS Control Limits 86635-27 86635-28 Method Blank Method Blank ----------------------------------------------------------------------------------- PARAMETER 86635-19 ---------- Purgeable Halocarbons (8010) Chlorobenzene, ug/1 1,1-Dichloroether:e, ug/1 Trichloroethylene, ug/1 Chloroform, ug/1 1,1-Dichloroethane, ug/1 Cis/Trans-1,2-Dichloroethene, Methylene chloride (Dichloromethane), ug/1 Tetrachloroethene, ug/1 1,1,1-Trichloroethane, ug/1 Vinyl chloride, ug/1 Surrogate -Bromochloromethane Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 90/85 % 55/55 % 90/85 % ug/1 86635-20 ---------- 38-176 % 10-232 % 28-196 % ---------- 86635-27 86635-28 -------------------- <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 8.6 <1.0 10 8.1 86 % 10 12-152 t 81 t 11.18.96 12-152 % 1. 0 11.19.96 1114B 1.0 1Blll8 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA ··, SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO 86635-19 86635-20 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 093061125 REPORT OF RESULTS Page 30 SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- LCS/LCSD % Recovery LCS Control Limits D I 86635-27 Method Blank 1· 86635-28 Method Blank -----------------------------------------------------------------------------------PARAMETER Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Total Xylenes, ug/1 Acetone, ug/1 86635-19 75/75 % 85/85 % Surrogate -a,a,a-Trifluorotoluene Surrogate -Expected Value Surrogate -\ Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Barium (6010) Barium (6010) 101/102 % Beryllium (6010) Beryllium (6010) 97/98 % Cadmium (7131) Cadmium (7131) 86/86 % Chromium (6010) Chromium (6010) 101/101 % Manganese (6010) Manganese (6010) 102/102 % --------------------------------------- 86635-20 23-168 % 33-167_% -1' - 80-120 % 80-120 % 80-120 % 80-120 % 80-120 % ---------- 86635-27 <1.0 <1.0 <3.0 <10 31 30 103 % 41-150 % 11.19.96 1.0 1114B 1Blll5 ---------- 86635-28 <l.0 <l.0 <3. 0 <10 31 30 103 % 41-150 % 11.18.96 1.0 1114B 1Blll8 ---------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I II II II II II II 'I I I I I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I D I I D I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 31 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86635-19 LCS/LCSD \ Recovery 86635-20 LCS Control Limits 86635-27 Method Blank 86635-28 Method Blank ----------------------------------------------------------------------------------- PARAMETER Manganese (6010) Manganese (6010) Nickel (6010) Nickel (6010) Lead (7421) Lead (7421) Antimony (7041) Antimony (7041) Vanadium (6010) Vanadium (6010) Zinc (6010) Zinc (6010) 86635-19 ---------- 102/102 \ 103/103 \ 98/96 \ 83/80 \ 98/98 \ 99/100 \ 86635-20 86635-27 86635-28 ------------------------------ 80-120 \ 80-120 \ 80-120 \ 80-120 \ 80-120 \ 80-120 \ Mercury (7470) I Mercury (7470) suspended Solids (160.2) Suspended Solids (160.2) 88/84 \ 80-120 \ I I I I I 103/102 ' ---------- 75-125 ' ------------------------------ 1 Laboratories In Sa~a,nnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 32 DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED Matrix Spike (MW-25) Result 86635-21 86635-22 Matrix Spike (MW-25) Duplicate Result PARAMETER 86635-21 86635-22 Purgeable Halocarbons (8010) Chlorobenzene, ug/1 1,1-Dichloroethene, ug/1 Trichloroethylene, ug/1 Surrogate -Bromochloromethane Surrogate Expected Value Surrogate -% Actual Recovery Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID Purgeable Aromatics (8020) 19 16 20 7.6 10 76 % 12-152 % 11.18.96 1.0 1114B 1Blll8 Benzene, ug/1 16 Toluene, ug/1 18 Surrogate -a,a,a-Trifluorotoluene 30 Surrogate -Expected Value 30 Surrogate -i Actual Recovery 100 i Surrogate -Control Limit Date Analyzed Dilution factor Batch ID Clock ID 41-150 % 11.18.96 1.0 1114B 1Blll8 17 14 19 7.8 10 78 tl 12-152 i 11.19.96 1. 0 1114B 1Blll8 15 18 30 30 100 i 41-150 i 11.19.96 1. 0 1114B 1Blll8 ,. ' 11-07-96/1445 11-07-96/1445 -Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D I I I I II ll II II II II II I I s L SAVANNAH LABORATORIES I & ENVIRONMENTAL SERVICES, INC. g B I I I I I I I I I I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: ll NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-0l Project: 190-00001-0l/MACON DOCKERY Sampled By: Client LOG NO 86635-21 86635-22 PARAMETER REPORT OF RESULTS SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------- Matrix Spike (MW-25) Result Matrix Spike (MW-25) Duplicate Result -------------------------------------------------- A6G35-2l 86635-22 ----------------------------- Barium (6010) Barium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Beryllium (6010) Beryllium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Cadmium (7131) Cadmium (7131), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Chromium (6010) Chromium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 2020 ll.12.96 ll.13.96 l. 0 lll.2E 49.6 ll.12.96 ll. l3. 96 l. 0 lll2K 4.12 ll.12.96 ll.13.96 l.0 lll2L 2020 ll.12.96 ll,13.96 l.0 lll2K 2090 ll.12. 96 ll.13.96 l.0 lll2K 50.9 ll.12.96 ll.13.96 l.0 lll2K 4.18 ll.12. 96 ll.13.96 l.0 lll2L 2080 ll.12.96 ll.13.96 l.0 lll2K ------------------------------------------------- Code: 180161122 Page 33 DATE/ TIME SAMPLED ll-07-96/1445 ll-07-96/1445 I Laboratories in Savl!.nnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS Page 34 DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED -------------------------------------------------------------------- 86635-21 Matrix Spike (MW-25) Result 86635-22 Matrix Spike (MW-25) Duplicate Result -------------------------------------------------------------------- PARAMETER Manganese (6010) Manganese (6010), ug/1 Preparation L'ate Date Analyzed Dilution facto - Batch ID Nickel (6010) Nickel (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Lead (7421) Lead (7421), ug/1 Preparation Date Date Analyzed •nilution factor Batch ID Antimony (7041) Antimony (7041), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-21 ---------- 506 11.12.96 11.13.96 1.0 1112K 519 11.12.96 11.13.96 1.0 1112K 47.5 11.12.96 11.13.96 1.0 1112L 50.6 11.13.96 11.14. 96 1.0 1113G ---------- 86635-22 ---------- 524 11.12.96 il.13.96 1.0 1112K 533 11.12.96 11.13.96 1.0 1112K 47.5 11.12.96 11.13.96 1.0 1112L 51. 0 11.13.96 11.14.96 1. 0 1113G ---------- 11-07-96/1445 11-07-96/1445 Laboratories in Sav~nnah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA g D u I I II El II II II II II II I s L SAVANNAH LABORATORIES lll & ENVIRONMENTAL SERVICES, INC. U 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I D H I I I I I I I I I I I I Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES -------------------------------------------------------------------- 86635-21 Matrix Spike (MW-25) Result 86635-22 Matrix Spike (MW-25) Duplicate Result -------------------------------------------------------------------- PARAMETER Vanadium (6010) Vanadium (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID Zinc (6010) Zinc (6010), ug/1 Preparation Date Date Analyzed Dilution factor Batch ID 86635-21 ---------- 491 11.12.96 11.13.96 1.0 1112K 495 11.12.96 11.13.96 1.0 1112K ---------- 8H35-22 ---------- 506 11.12.96 11.13 ·. 96 1. 0 1112K 509 11.12.96 11.13.96 1.0 1112K ---------- Page 35 DATE/ TIME SAMPLED 11-07-96/1445 11-07-96/1445 I Laboratories In Sa;annah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635 Received: 11 NOV 96 Reported: 21 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 180161122 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES 86635-23 86635-24 86635-25 86635-26 Matrix Spike (MS) Expected Value MS/MSD % Recovery MS\ Recovery Limits MS% RPD (Limits) PARAMETER Purgeable Halocarbons (8010) Chlorobenzene, ug/1 1,1-Dichloroethene, ug/1 Trichloroethylene, ug/1 Purgeable Aromatics (8020) Benzene, ug/1 Toluene, ug/1 Barium (6010) Barium (6010), ug/1 Beryllium (6010) Beryllium (6010), ug/1 Cadmium (7131) Cadmium (7131), ug/1 Chromium (6010) Chromium (6010), ug/1 Manganese (6010) Manganese (6010), ug/1 Nickel (6010) Nickel (6010), ug/1 'Lead (7421) Lead (7421), ug/1 Antimony (7041) Antimony (7041), ug/1 86635-23 ---·------ 20 20 20 20 20 2000 50.0 5.00 2000 500 500 50.0 50.0 ---------- 86635-24 ---------- 95/85 % 80/70 % 100/95 % 80/75 % 90/90 % 101/104 % 99/102 % 82/84 % 101/104 % 101/105 % 104/107 % 95/95 % 101/102 % ---------- 86635-25 86635-26 --------------------- 38-176 % 11 (<30) % 10-232 % 13 .. <20) % 28-196 % 5 (<20) % 23-168 % 6 ( <34) % 33-167 % 0(<25) % 75-125 % 2.9(<20) % 75-125 % 3.0(<20) % 75-125 % 2 .4 (<20) % 75-125 % 2.9(<20) % 75-125 % 3.9(<20) % 75-125 % 2.8(<20) % 75-125 % 0 ( <2 0) % 75-125 % .99(<20) % -------------------- Page 36 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerlield Beach, FL • Mobile, AL • New Orleans, LA -, D D D I' I I Ir II II II II II I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31~04 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO, S6-86635 Received, ll NOV 96 Reported, 21 NOV 96 Client PO. No., 190-00001-0l Project, 190-00001-0l/MACON DOCKERY Sampled By, Client Code, 095961129 REPORT OF RESULTS Page 37 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES ----------------------------------------------------------------------------------- 86635-23 86635-24 86635-25 86635-26 Matrix Spike (MS) Expected Value MS/MSD \ Recovery MS\ Recovery Limits MS\ RPD (Limits) -------------------------------------------------------------------------··--------- PARAMETER Vanadium (6010) Vanadium (6010), ug/1 Zinc (6010) Zinc (6010), ug/1 86635-23 ---------- 500 500 ---------- 86635-24 ---------- 98/101 \ 99/102 \ ---------- 86635-25 86635-26 -------------------- 75-125 \ 3.0(<20) \ 75-125 \ 3.0(<20) \ -------------------- The presence of acetone was confirmed by GC/MS (method 8260) at a concentration of 150ug/l. Due to matrix interference, wher~by possible coelution of a non-target analyte occurred, the GC (method 8020) acetone concentration of 2100 ug/1 appears to be high biased. Lisa G. McLeod, Project Manager Final Page Of Report Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mob/le, AL • New Orleans, LA . -,••·· . . . ... Senal Numb0< ..> U ,J '-t 4 SL SAVANNAH LABORATORIES D 5102 LaRoche Avenue, Savannah, GA 31404 Phone: {912) 354-7858 Fax: {912) 352-0165 & ENViRONMENTAL SERVICES, INC. D 2846 Industrial Plaza Drive, Tallahassee. FL 32301 Phone: {904) 878-3994 Fax: {904) 878-9504 D 414 SW 12th Avenue. Deerfield Beach, FL 33442 Phone: {954) 421-7400 Fax: {954) 421-2584 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD D 900 Lakeside Drive, Mobile, AL 36693 Phone: (334) 666-6633 Fax: {334) 666-6696 D 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Phone: (813) 885-7427 Fax: (813) 885-7049 D 100 Alpha Drive, Suite 110, Destrehan, LA 70047 Phone: (504) 764-1100 Fax: (504) 725-1163 PROJECT REFERENCE . PROJECT NO. P.O.NUMBER 111 Ar ... ..il MATRIX I PAGE loF h~Fll-1 l1t:>-oo~ 01-01 TYPE REQUIRED ANALYSES . PROJECTLOC. SAMPLER{s) NAME PHONE 7>o -f;'c/,f-f''/// t /v-~ f,') {Stale) , IJ r:__. ER,.,_ oe.-c~ FAX 7,., v'of-7/73 I Ii ,I 't{ ,.,_, ,( CLIENT NAME CLIENT PROJECT MANAGER qi,t,,':' "' ~ANDARD EPORT lt('f'Lt £°0 l:'1Vi'ltl Sc1f'.Vt.i!f 'Ro.J IJ It ,:, 1.-A < IF Q s C) ' ELIVERY Q::.;; & 0 • ~-0 I\~ CLIENTADDRESS(CITY,STATE,ZIP) G,S L. ;,° ,i._ C..rr.A,I /'-,k,_, 1.~8 ✓ J. f .. , \°" □ EXPEDITED REPORT S. :,J...,voo LJaro,,,,,r.r, c_ 3 0 ., 77... 7 :<t~ !s ~ DELIVERY{surcharge) ~ 0 & &i I I I I / ···V · I I I / Date Due: SAMPLE ... SL /, ~ ~ DATE TIME NO. SAMPLE IDENTIFICATION 'J, tW NUMBER OF CONTAINERS SUBMITTED REMARKS "-IJk, ':<ti-111lJ-2./ 'i. y ,.,. )( ''h/1~ flj !If< f J, 'l) -l . ., , Tk .(:. -,.,, t l' l( •til•ll , .. :~{" u :])~ '6,L1 EC.[ '( "t, )( X 11/'II ~ l 11:sa ()11.\ -/ s V 'x V y )( "hla~ I l.!0o mu-t<R ~ y V ,I 0 h11t ?tyS /h, I 2-.J ll<S. I ~s·n I( X V N.lltJ/.,o ..r:._ r.r.r ,,/7f4c, 3.'3o L_ D .. e,/~,,,.,.., _J_,... r, l( !;' . V, u/J/5( 3,Jo L Doclcv(, e.(f \ V• \, y t</1/q, 3: 1/'D /11 t,J-/ (, 'f )/·· y K •·hl1t '3:50 fol 11-/{, R )( )( X ••/7/,, j :,o M w ·z.c./ I~ V '/. V ''hf"'., TR , P 'E ,._ A v..J J-... ~ X'. RE_f ~UISHED BY: (SI'(. y<TURE) J, 0 ~ 'rt TIME R"~✓-BuzE) DATE TIME RELINQUISHED BY: {SIGNATURE) DATE TIME ,.... ,-_.,. ' ~ •• I\ .o ~~4c: v£,,r, 3-.,.. I lfECI IVED BY: (SIG~ATURE) V DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: {SIGNATURE) DATE TIME LABORATORY USE ONLY '._-1: ,·•;,->··,C· · ·:~ -::-::';,!·;;•.f<. r-:~:-.:t~! 7 ~IVrA:2~BY0S0ATURE) DATE TIME CUSTODY INTACT CUSTODY SEAL NO. SLLOGT;to~ LABORATORY REMARKS: .. : ' ,?}: .. '/1/qu \\p) ,· ~□No tjg"i I ~ a ii: 0 I s L SAVANNAH LABORATORIES . & ENVIRONMENTAL SERVICES, INC. I I I I n I B D I I D I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635A Received: 11 NOV 96 Reported: 19 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 095161120 LOG NO REP0RT OF RESULTS SAMPLE DESCRIPTION, AIR SAMPLES Page 1 DATE/ TIME SAMPLED 86635A-l Property Line B6635A-2 Macon Source Area 86635A-3 OW-1 86635A-4 VE-1 86635A-5 OW-5 PARAMETER 86635A-1 86635A-2 86635A-3 ----r-----------·----------. __ ---------·· -------------------- Volatile Organic Compounds (NIOSH 1501) Vinyl chloride, mg/m3 <10 <10 <10 Methylene chloride <10 <10 <10 (Dichloromethane), mg/m3 Acetone, mg/m3 <20 <20 <20 1,1-Dichloroethene, mg/m3 <10 <10 <10 1,1-Dichloroethane, mg/m3 <10 <10 <10 1,2-Dichloroethene, mg/m3 <10 <10 <10 Chloroform, mg/m3 <10 <10 <10 1,1,1-Trichloroethane, mg/m3 <10 <10 <10 Trichloroethene, mg/m3 <10 <10 <10 Benzene, mg/m3 <10 <10 <10 Tetrachloroethene, mg/m3 <10 <10 <10 Toluene, mg/m3 <10 <10 <10 Xylenes, mg/m3 <10 <10 <10 ----------------------------------------------------------- 11-08-96/0700 11-08-96/0705 11-08-96/0710 11-08-96/0715 11-08-96/0720 86635J.-4 86635A-5 <10 <10 <10 <10 <20 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --------------.------ Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO, S6-86635A Received, 11 NOV 96 Reported, 19 NOV 96 Client PO. No., 190-00001-01 Project, 190-00001-01/MACON DOCKERY Sampled By, Client Code, 095161120 REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, AIR SAMPLES ------------------------------------------------------------- 86635A-6 OW-3 86635A-7 U/L Macon 86635A-8 U.Dockery 86635A-9 L.Dockery DATE/ TIME SAMPLED 11-08-96/0725 11-08-96/0740 ll-08-96/0750 11-08-96/0800 Page 2 ------------------------------------------------------------------------------------ PARAMETER 86635A-6 ------------------------------------------------- Volatile Organic Compounds (NIOSH 1501) Vinyl chloride, mg/m3 <10 Methylene chloride (Dichloromethane), mg/m3 <10 Acetone, mg/m3 1,1-Dichloroethene, mg/m3 1,1-Dichloroethane, mg/m3 1,2-Dichloroethene, mg/m3 Chloroform, mg/m3 1,1,1-Trichloroethane, mg/m3 Trichloroethene, mg/m3 Benzene, mg/m3 Tetrachloroethene, mg/m3 Toluene, mg/m3 Xylenes, mg/m3 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 86635A-7 86635A-8 ··---------------~--- <10 <10 <10 <10 <20 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 86635A-9 <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 --------------------------------------- ------------------------------ ---------- Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA 0 g I I D D n u u u 11 11 I I n I n I D I I I I n I g g I H D D SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635A Received: 11 NOV 96 Reported: 19 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 095161120 REPORT OF RESULTS Page 3 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR AIR SAMPLES 66635A-10 86635A-11 66635A-12 86635A-13 86635A-14 Practical Quantitation Limits Method Blank Result Lab Control Standard (LCS) Result LCS Duplicate Result LCS Expected Value ----------------------------------------------------------------------------------- PARAMETER 86635A-.10 Volatile Organic Compounds (NIOSH 1501) Vinyl chloride, mg/m3 10 Methylene chloride 10 (Dichloromethane), mg/m3 Acetone, mg/m3 1,1-Dichloroethene, mg/m3 1,1-Dichloroethane, mg/m3 1,2-Dichloroethene, mg/m3 Chloroform, mg/m3 1,1,1-Trichloroethane, mg/m3 Trichloroethene, mg/m3 Benzene, mg/m3 Tetrachloroethene, mg/m3 Toluene, mg/m3 Xylenes, mg/m3 20 10 10 10 10 10 10 10 10 10 10 ---------- 86635A--ll <10 <10 <20 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ---------- 86635A-12 86635A-13 86635A-14 92 86 100 100 99 100 81 82 100 100 94 100 Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Ronald Wallace Applied Earth Sciences, Inc. 6525 The Corners Parkway, Suite 400 Norcross, GA 30092 LOG NO: S6-86635A Received: 11 NOV 96 Reported: 19 NOV 96 Client PO. No.: 190-00001-01 Project: 190-00001-01/MACON DOCKERY Sampled By: Client Code: 095161120 REPORT OF RESULTS Page 4 LOG NO SAMPLE DESCRIPTION, QC REPORT FOR AIR SAMPLES 86635A-15 LCS/LCSD % Recovery 86635A-16 LCS Control Limits PARAMETER 86635A-15 86635A-16 Volatile Organic Compounds (NIOSH 1501) 1,1-Dichloroethene Trichloroethene Benzene Toluene Method: NIOSH-1501 92/86 % 100/99 % 81/82 % 100/94 % ---------- Final Page Of Report 75-125 % 75-125 % 75-125 % 75-125 % -------------------- 0 0 0 0 0 0 D D 0 0 D 0 u D D I D Labora.tories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA D l!!l!iil l!i!iii lill!I !iilii!I Im:! liiil 1111B Im !Im liiiiiii:I _, li:iiii!!I .:i mil IIIBeriallllllit,r M j 4je 11m SL SAVANNAH LABORATORIES D 5102 La Roche Avenue, Savannah, GA 31404 Phone: (912) 354-7858 Fax: (912) 352-0165 & ENVIRONMENTAL SERVICES. INC. D 2846 Industrial Plaza Drive. Tallahassee, FL 32301 Phone: (904) 878-3994 Fax: (904) 878-9504 0414 SW 12th Avenue, Deerfield Beach. FL33442 Phone: (305) 421-7400 Fax: (305) 421-2584 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD D 900 Lakeside Drive. Mobile, AL 36693 Phone: (205) 666-6633 Fax: (205) 666-6696 06712 Benjamin Road. Suite 100. Tampa, FL33634 Phone: (813) 885-7427 Fax: (813) 885-7049 D 100Alpha Drive, Suite t 10, Destrehan. LA 70047 Phone: (504) 764-1100 Fax: (504) 725:1163 PROJECT REFERENCE PROJECT NO. P.O.NUMBER A/Ac.v MATRIX loF Doc;t-e-n y l';'o · "'>u< 1 --t • TYPE REQUIRED ANALYSES PAGE PROJECT LOC. SAMPLER(s) NAME PHONE 7 7 ~-<N",P-l,'9,f , t' (State) ' llC e~,c. 73ilvc.E FAX 7?,.,-V.:,q-?.""" • I,,,• CLIENT NAME CLIENT PROJECT MANAGER }:-STANDARD D(fREPORT /tf'l°L I Ep '8irtn-H Jr I e~c.i:J" l?a ,J , . -,c.Ac-C" Q .. DELIVERY ~ 0 $'1 " CLIENT_ADDRESS(CITY,STATE,ZIP) '::, 2-'f" T1-,... C..i,.,..,.J p"" ;( <, ·1 !J." £9 ~ □ EXPEDITED REPORT -:,,.~ ~= ~,~, t C.. 3 '! "'~ !J DELIVERY(surcharge) <>o ,_.. "'rJ 9:, .;:; I I I I I I I I I / Dale Due: SAMPLE SL ' "% 0 DATE TIME NO. SAMPLE IDENTIFICATION /2 ~!ti~ NUMBER OF CONTAINERS SUBMITTED REMARKS '< il/4, '2,, ?;z,o -~---.I Lit C2. ) X "/P,I~, 7.'e.f ull l C ... 7E.u-IJ X •lr/1, ]!,10 Or 1-/ IX X "/1/-,, J:1,J" VE-I J y "/ti,, 7: z_;:, /Jt.J-5 l x ,,1,hc. 7.'2. <; Ow-.3 X I l<' "/1/u. ?:vo V/4 M"' __ Ir •·lt/1,. 7:So U, 'ua-1 -• t ••J,/,;c J":-.~ L. D -i . ! ~ y I Ry.....:;;;✓,(Su.~ D½ TIME RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME '~{9c:. 3: . .,o RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME .. ' LABORATORY USE ONLY i EIVED fi R LABORATOI 'j'BY/1 S~AT~RE) DJTE TIME CUSTODY INTACT CUSTODY SEAL NO. SL LOG NO. LABORATORY REMARKS: 'J/j1rri,1 i' "(q1.p ,1 :cP ~□No: «P'~t?J5 oiJ .=\ . I .. :-.. -~. /~'..' ... . ,,