NCD980840409_19910201_Charles Macon Lagoon & Drum_FRBCERCLA RI_RI FS Study 1990 Remedial Investigation Report Volume III-OCR

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~iACON/DOCKERY NPL SITE REMEDIAL INVESTIGATION/
FEASIBILITY STUDY REMEDIAL INVESTIGATION REPORT
VOLUME III
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Macon/Dockery Site
ReIDedial Investigation/
Feasibility Study
Remedial Investigation Report
..
·volume III
-1990
SIRRINE
ENVl·RONMENTAL
CONSUL TAN TS
__ ,..---,~
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COMPUCHEM
lABOPATORJES
Case Narrative #17902
SDG #51
contract #(2-88)-REVS
CompuChem Laboratories, Inc.
SAMPLE IDENTIFICATIONS: 9168SED21, 9169SED81, 9169SED91,
SED-1-1, SED-3-1, SED-3-2, SED-4-1, SED-5-1, SED-6-1, SED-7-1,
SL-1-1, SL-2-1, SL-3-1, SL-4-1, SL-5-1, SL-6'-l, SL-7-1, SL-8-1,
SL-9-1, SL-2-2
These samples were received in good condition, with the
proper chains-of-custody (COC), sealed in a cooler on
September 22, 29, and 30, 1989. Analyses were scheduled in
accordance with the coc. Volatile, semivolatile and pesticide
analyses were performed as requested on these samples. Holding
time requirements were met for all of these samples.
All pertinent Quality Assurance and Laboratory notices for
CASE# 17~02, SDG# 51 are included in the sample data package.
VOLATILES:
There were Target Compound List (TCL) analytes identified
above the Contract·Required Quantitation Limits (CRQLs) in all
of the samples. Tentatively Identified Compounds (TICs) were
found in only one of these samples.
sample SL-9-1 was analyzed three times due to
inconsistencies in the recoveries of Methylene Chloride and
Acetone. These variations have been attributed to an
inhomogeneous matrix. Two of the sample analyses are being
reported to demonstrate the variations. This sample is reported
with reference to this qualifier.
The associated method blanks, matrix spike (MS), and matrix
spike duplicate (MSD) met all qtiality·control requirements.
SEIIIVOLATILES:
Five of these sam~les contained TCL analytes above the
CRQLs. TICS were found 1n all but one of these samples.
The "X" footnote is used on the Form I's to flag analytes
that coelute as indistinguishable isomers. •
The advisory surrogate atandard is flagged as an outlier in
samples 9168SED21 and 916SED81. Sample 916SED81 also had one
othe surrogate standard flagged as an outlier. one acid
surrogate and one base surrogate are allowed to fail recovery
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park. NC 27709 [phone]
~"SANPLc D/:lTR 5l.mMRR_Y -201
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-----Cotv1PLCHEM
lABOPATORIES
limits without requireing a repeat extraction and reanalysis as
long as the recoveries are greater than 10 percent.
The associated method blank, MS, and MSD met all quality
control requirements. The recovery of one analyte was flagged
as an outlier in the MS. One analyte in the spikes failed the
relative· percent difference criteria and was flagged as an
outlier. These samples are reported with reference to this
qualifier. ·
PESTICIDES:
There were TCL pesticide analytes confirmed in one of these
samples. The associated method blanks, MS, and MSD met all
quality control requirements.
I certify that this data package is· in compliance with the
terms and conditions of the contract, both technically and for
completeness, for other than conditions detailed above. Release
of the data contained in the hardcopy data package has been
authorized by the Laboratory Manager or his designee, as
verified by the following signature.
Note: This report
accountability
~~ <P--4, t.;fn/f:/
Daniel E. Boone, Jr. DATE 10/27/89
TECHNICAL REVIEWER (
is paginated
in decreasing
2
~CE-DAIR.
for reference and
nWlerical sequence.
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CDMPUCHEM
LABORATORIES
Case Narrative #17902
SDG #51
Contract #(2-88)-REVS
CompuChem Laboratories, Inc.
'
SAMPLE IDENTIFICATIONS: 9168SED21, 9169SE081, 9169SED91,
SED-1-1, SED-3-1, SED-3-2, SED-4-1, SE0-571, SED-6-1, SED-7-1,
SL-1-1, SL-2-1, SL-3-1, SL-4-1, SL-5-1, SL-6-1, SL-7-1, SL-8-1,
SL-9-1, SL-2-2
These samples were received-in good condition, ~ith the
proper chains-of-custody (COC), sealed in a cooler on
September 22, 29, and 30, 1989. Analyses were scheduled in
accordance with the COC. Volatile, semivolatile and pesticide
analyses were performed as requested on these samples. Holding
time requirements were met for all of these samples with the
only exceptions being for the pesticide samples SL-3-1, SL-4-1,
and SL-5-1. The pesticide samples that were outside of holding
time requirements were originally extracted within holding
time, but required re-extraction outside of holding time in
order to meet quality control requirements.
All pertinent Quality Assurance and Laboratory notices for
CASE# 17902, SDG# 51 are included in the sample data package.
VOLATILES:
There were Target Compound List (TCL) analytes identified
above the Contract Required Quantitation Limits (CRQLs) in all
of the samples. Tentatively Identified Compounds (TICs) were
found in only one of these samples.
Sample SL-9-1 was analyzed three times due to
inconsistencies in the recoveries of Methylene Chloride and
Acetone~ These variations have been attributed to an
inhomogeneous matrix. Two of the sample analyses are being
reported to-demonstrate the variations. This sample is reported
with reference to this qualifier.
The associated method blanks, matrix spike (MS), and matrix
spike duplicate (MSD) met all quality control requirements.
SEMIVOLATILES:
Five of these samples contained TCL analytes above the
CRQLs. TICs were found in all but one of these samples.
The "X" footnote is used on the Form I's to flag analytes
that coelute as indistinguishable isomers.
I COMPUCHEM LABO RA TORIES, INC. P.O. eo, 12652 -~~•-~ Hrn ',""''°" Highway Re,ea,ch _T<ia~g~ Po,k, NC 27709 [phone]
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-----COMPUCHEM
lABOPATORIES
The advisory surrogate atandard is flagged as an outlier in
samples 9168SED21 and 916SED8l. Sample 916SED81 also had one
othe surrogate standard flagged as an outlier. One acid
surrogate and one base surrogate are allowed to fail recovery
limits without requireing a repeat extraction and reanalysis as
long as the ~ecoveries are greater than 10 percent.
The associated method blank, MS, and MSD met all quality
control requirements. The recovery of one analyte was flagged
as an outlier in the MS. One analyte in the spikes failed the
relative percent difference criteria and was flagged as an
outlier. These samples are reported ~ith reference to this
qualifier.
PESTICIDES:
There were TCL pesticide analytes confirmed in one of these
samples. The as~ociated method blanks, MS, and MSD met ~11
quality.control requirements.
l
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and for
completeness, for other than conditions detailed above. Release
of the data contained in the hardcopy data package has been
authorized by ihe Laboratory Manager or his designee, as
verified by the following signature.
Note: This report
accountability
Daniel E. Boone, Jr. DATE 10/27/89
TECHNICAL REVIEWER
is paginated
in decreasing
2
for reference and
numerical sequence.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
9168SED21
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: =5..,.l __
Matrix: (soil/water) SOIL Lab Sample ID: 288545
Sample wt/vol: s.o (g/mL) ~ Lab File ID: GH088545Cl9
Level: (low/med) I..QW Date Received: 09/22/89
% Moisture: n·ot dee. _2i Date Analyzed: Q~/30LB9
Column: (pack/cap) CAP Diluti6n Factor: _l~,~Q __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGLKG Q
74-87-3---------Chloromethane 22 u
74-83-9--------~Bromomethane 22 u
75-01-4---------Vinyl Chloride 22 u
75-00-3---------Chloroethane 22 u
75-09-2---------Methylene Chloride 16 B
67-64-1---------Acetone 18 BJ
75-15-o---------carbon Disulfide 11 u
75-35-4---------1,1-Dichloroethene 11 u
75-34-3---------1,1-Dichloroethane 11 u
540-59-o--------l,2-Dichloroethene (total)_ 11 u
67-66-3---------Chloroform 11 u
107-06-2--------1,2-Dichloroethane 11 u
78-93-3---------2-Butanone 22 u
71-55-6---------1,1,1-Trichloroethane 11 u
56-23-5---------carbon Tetrachloride 11 u
108-05-4---~----Vinyl Acetate 22 u
75-27-4---------Bromodichloromethane 11 u
78-87-5---------1,2-Dichloropropane 11 u
10061-01-5------cis-l,3-Dichloropropene 11 u
79-01-6---------Trichloroethene 11 u
124-48-1-------~Dibromochloromethane 11 u
79-oo-s---------1,1,2-Trichloroethane 11 u
71-43-2---------Benzene 11 u
10061-02-6------Trans-l,3-Dichloropropene __ 11 u
75-25-2---------Bromoform 11 u
1os-10-1--------4-~ethyl-2-Pentanone 22 u
591-78-6--------2-Hexanone 22 u
127-18-4--------Tetrachloroethene 11 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 11 u
108-88-3--------Toluene 11 u
108-90-7--------Chlorobenzene 11 u
100-41-4--------Ethylbenzene 11 u
100-42-s--------styrene 11 u
1330-20-7-------Total Xylenes 11 u
FORM I VOA 1/87 Rev.
\
c:;EE~QijR~t□IJR· C551tleelJ. D-!lwlli-11¥!i•~·--~·,::· -=· :=:=----J 90
·:Je.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
EPA SAMPLE NO.
9168SED21
Lab Code: COMPU case No.: 17902
Ma~rix: (soil/water} SOIL
SAS No.: SDG No.: ..... 5 ..... 1 __
Lab Sample ID: -2.,._8~8-54~5~---
Sample wt/vol: 5,0 (g/mL} fi__
Level: (low/med} LOW
% Moisture: not dee.~
Column (pack/cap} _cA ... P __
Number TICs found: __Q_
Lab File IO:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
~H088545Cl9
09/22/89
09/30/89
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ============•=============== --====== ---=---=---=-=====
FORM I VOA-TIC 1/87 Rev.
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==-=±Ai·
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REV~
9169SED81
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: ..._5 .... 1 __
Matrix: (soil/water) SOIL Lab sample ID: 288558
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH08855Bc19·
Level: (low/med) LOW Date Received: 09/22/89
I Moisture: not dee. ---1 Date Analyzed: Q9/JQL89
Column:
±±::a.
(pack/cap) CA;e Dilution Factor: .1L,o~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane ll u
75-09-2---------Methylene Chloride 10 B
67-64-l~--------Acetone 13 B
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,l-Dichloroethane 5 u
540-59-0--------1,2-oichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------l,2-0ichloroethane 5 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 5 u
56~23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-oichloropropane 5 u
10061-01~s------cis-1,J-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane s. u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-0ichloropropene_ 5 u
75-25-2---------Bromoform 5 u
1oa-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 5 u
108-88-3--------Toluene 5 u
108-90-7-~------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrane 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
-

.

±EL SH PC?-.IHI Tll. --=----·. ---· -188
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88}-RpJS
EPA SAMPLE NO.
9169SE081
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: .-5_1 _· _
Matrix: (soil/water) SOIL
Sample wt/vol: S,O (g/mL) L-
Level: (low/med) _LO_w __
I Moisture: not dee. _..:J_
Column (pack/cap) CAP.
Number TI.Cs found: _2,
Lab Sample IO:
File
/
Lab ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
288558
GH088558Cl9
09/22/89
09/J0/89
l.dl
CAS NUMBER COMPOUND NAME ftT EST. CONC. Q ,
FORM I VOA-TIC 1/87_ Rev.
1"87
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-l-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.·: SDG No:: -5-1 __
Matrix: (soil/water) SOIL Lab Sample ID: 291036
Sample wt/vol: 5,0 (g/mL) SL_ Lab File ID: GH091036Cl4
Level: (low/med) LOW Date Received: 09/30189
I Moisture: not dee. ~ Date Analyzed: l0,l07,l89
Column: (pack/cap) CAf
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
~7-64-1------~--Acatone
75-15-o---------carbon Disulfide-
75-35-4---~-----l,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-o--------l,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
Dilution Factor: _1~,o,.__ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/XG Q
71 u
71 u ,. 71 u
71 u
39 B
200
36 u
36 u
36 u
(total)_ 36 u
9 J
36 u
71 u
-11-ss-6---------1,1,1-Trichloroethane 36 ·U
56-23-5---------carbon Tetrachloride 36 u
108-0S-4--------Vinyl Acetate 71 u
75-27-4---------Bromodichloromethane 36 u
78-87-s---------1,2-Dichloropiopane 36 · u
10061-0l-S------cis-1,3-Dichloropropene 36 u
79-01-6----.-----Trichloroethene 36 u
124-48-1--------Dibromochloromethane 36 u
79-oo-s---------1,1,2-Trichloroethane 36 u
71-43-2---------Benzene 36 u
10061-02-6------Trans-l,3-Dichloropropene__;_ 36 u
75-25-2---------Bromoform· 36 u
1oa-10-1--~-----4-Methyl-2-Pentanone 71 u
591-78-6--------2-Hexanone 71 u
127-18-4.---------Tetrachloroethene 36 u
79-34-5---------1,1,2,2-Tetrachloroethane_· _ 36 u
101-aa-J--------Toluene 36 u
108-90-7--------Chlorobenzene 36 u
100-41-4--------Ethylbenzene 36 u
100-42-s--------styr•n• 36 u
1330-20-7-------Total Xylenes 36 u
' FORM I VOA 1/87 Rev.
186
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SED-1-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: ___ SDG No.: -.51 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0
Level: (low/med) U>W
I Moisture: not dee. _li
Column (pack/cap) ~AE
Number TICS found: ___Q
(g/mL) L-
Lab Sample ID: ,..2._9.._l..._0 .... 36..__ __ _
Lab File ID: GH091036Cl4
Date Received: 09/30/89
Date Analyzed: 10/07/89
Dilution Factor: _1~,Q,.__ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
a::===
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS SED-3-1
Lab Code: COMPU case No.: 17902 SAS No.: SOG No.: _5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: 291034
Sample wt/vol: s.o (g/mL) .G__ Lab File ID: ~HQ9lQHCH
Level: (low/med) LOW · Date Received: 09/30/89
% Moisture: not dee. _u Date Analyzed: 10/07/89
Column: (pack/cap) CAf Dilution Factor: _1-,0=-----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane I 12 u
75-09-2---------Methylene Chloride 16 B
67-64-1---------Acetone 39
75-15-o---~-----carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-tiichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u.
67-66-3---------Chloroform 2 J
101-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-0ichloropropane 6 u
10061-0l-S------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Oibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l, 3-Dichlor.opropene_ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--~-----2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
1oa-90-1--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANics ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2~88l-REVS
Lab Code: COMPO case No.: 17902 SAS No.: SOG
Matrix: (soil/~ater) SOIL Lab Sample ID:
Sample wt/vol: 5,0 (g/mL) L-Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee. _ll Date Analyzed:
EPA SAMPLE NO.
SED-3-1
No.: 51
291034
GH091034Cl4
09/30/89
10/07/89
Column (pack/cap) CAf Dilution Factor: -l.~,o __ _
Number TICS found:~
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= =====
FORM I.VOA-TIC 1/87 Rev.
--· --__ -.--::---~ --&±-------~c::: ---=== ~-=--=SP ?LE-_llllt1£. SQIIBAR¥~ 183
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SED-3-2
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ""'5...,1 __
Matrix: (soil/water) SOIL Lab Sample ID: 291035
Sample wt/vol: s.o (g/mL) L-Lab File ID: GH091035Cl4
Level: (low/med) LOW Date Received: 09/30/89
I Moisture: not dee. _a Date Analyzed: 10/07/89
Column: (pack/cap) CAP Dilution Factor: 1,0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) YSitiG Q ~.
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
.75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 13 8-
67-64-1---------Acetone 19
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,l-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-o---•----l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 2 J
107-06-2--------l,2-Dichloroethane 6 u
78-93~3---------2-Butanone 12 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-s---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-0l-s------cia-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 ·U
10061-02-6------Trans-l,3-Dichloropropene_ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
' FORM I VOA 1/87 Rev.
1----
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: l2-88l-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample I.D:
Sample wt/vol: s.o (g/mL) L-Lab File ID:
Level: · (low/med) ' LOW Date Received:
I Moisture: not dee. ___ll Date Analyzed:
EPA SAMPLE NO.
SED-3-2
No.: 51
291035
GH091035Cl4
09/30/89
1Q/07L89
Column (pack/cap) C:Af Dilution Factor: _1-1 0..._ __
Number TICs found: __Q
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or. ug/Kg) UG/KG
RT EST. CONC. Q
••=~============ ============================ =====•=s ---s-==.===== =====
FORM I VOA-TIC 1/87 Rev.
'
llllfR SOPNPRY±,_-.. ..c,.:. 181
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VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SE0-4-1
Lab Code: COMPO Case No.: 17902 SAS No.: SOG No.: .._5._l __
Matrix: (soil/water) SOIL Lab Sample ID: 290814
Sample wt/vol: 5.0 (g/mL) G.__ Lab File ID: GH090814Cl9
Level: (low/med) I.OW Date Received: 09/29/89
% Moisture: not dee. ----12 · Date Analyzed: 10/0§/89
Column: (pack/cap) ~AE Dilution Factor: ·-1-,0 ___ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Xg) UG/KG Q
74-87-3---------Chloromethane 17 u
74-83-9---------Bromomethane 17 u
75-01-4---------Vinyl Chloride 17 u
75-00-3-----~---Chloroethane 17 u
75~09-2---------Methylene Chloride 45 B
67-64-1---------Acetone 85 B
75-15-o---------carbon Disulfide 8 u
75-35-4---------1,1-Dichloroethene 8 u
75-34-3---------1,1-Dichloroethane 8 u
540-59-o--------l,2-Dichloroethene '(total)_ 8 u
67-66-3---------Chloroform 3 J
107-06-2--------1,2-Dichloroethane 8 u
78-93-3---------2-Butanone 3 J
71-55-6---------1,l,l-Trichloroethane 8 u
56-23-5---------carbon Tetrachloride 8 u
108-05-4--------Vinyl Acetate 17 u
75-27-4---------Bromodichloromethane 8 u
78-87-5---------1,2-Dichloropropane 8 u
10061-01-5------cis-l,3-Dichloropropene 8 u
79-01-6---------Trichloroethene 8 u
124-48-1-~------Dibromochloromethane 8 u
79-00-5---------1,l,2-Trichloroethane 8 u
71-43-2---------Banzene 8 u
10061-02-6------Trans-l,3-Dichloropropene_ .a u
75-25-2---------Bromoform 8 u
1oa-10-1--------4~Methyl-2-Pentanone 17 u
591-78-6--------2-Hexanone 17 u
127-18-4--------Tetrachloroethene 8 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 8 u
108-88-3----~---Toluene 8 u
108-90-7--------Chlorobenzene 8 u
100-41-4--------Ethylbenzene 8 u
100-42-5--------styrene 8 u
1330-20-7-------Total Xylenes 8 u
' FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEK LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SED-4-1
Lab Code: COMPO Case No.: 17902 SAS No.: SOG No.: ..._5_1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0 (g/mL) G,__
Level: (low/med) LOW
I Moisture: not dee. ~
Column (pack/cap) CAf
Number. TI.Cs found: __Q
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
290814
GHQ9Q8lHa9
Q9/29/89
l0/0§/89
l.d2
RT ., EST. CONC. Q
================ ==========================.= ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
\
--;:;;~-------~------
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS SED-5-1
Lab Code: COMPO case No.: 17902 SAS No.: SDG No.: ..c.5.._1 __
Matrix: (soil/water) SOIL Lab Sample ID: 290816
Sample wt/vol: s,o (g/mL) ~ Lab File ID: GH090816Cl9
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. _u. Date Analyzed: 10/06/89
Column: (pack/cap) gf Dilution Factor: .1~,o~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/RG Q
74-87-3---------Chloromethane 13 u
74-8·3-9---------Bromomethane 13 u
75-01-4---------Vinyl Chloride 13 u
75-00-3------~--Chloroethane 13 u
75-09-2---------Methylene Chloride 29 B
67-64-1---------Acetone 52 B
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,l-Oichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-oichloroethene (total)_ 6 u
67-66-3---------Chloroform 3 J
107-06-2--------1,2-oichloroethane 6 u
78-93-3---------2-Butanone 13 u
71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-s---------1,2-oichloropropane 6 u
1~061-01-s------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5--------~l,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene_ 6 u
75-25-2---------Bromof~rm 6 u
1oe-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3~-------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u .
FORM.I VOA 1/8_7 Rev.
-178
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SE0-5-l
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: ___ SDG No.: ,_51 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. _ll
Column (pack/cap) ~f
Number TICs found: .....:..Q
CAS NUMBER
(g/mL) L-
COMPOUND NAME
Lab Sample IO: _2_90_8 ..... 1._6L...-__ -'-
Lab File IO: GH090816Cl9
Date Received: 09/29/89
Date Analyzed: 10/06/89
Dilution Factor: -1~,o __ _
CONCENTRATION UNITS:
(ug/L or ug/l<g) UG/KG·
RT EST. CONC. Q
=~-==-=---------=============================a=========~======•~••====
(
FORM I VOA-TIC l/87 Rev.
\
177
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SED-6-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ..._5..._l __
Matrix: (soil/water) SOIL Lab sample ID: 290820
Sample wt/vol: s.o {g/mL) ~ Lab File ID: GH090820Cl9
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. __:n Date Analyzed: 10/06/89
Column: (pack/cap) CAP Dilution Factor: LO
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !.l<iLK<i Q
74-87-3--~------Chloromethane 14 u
74-83-9---------Bromomethane 14 u
75-01-4---------Vinyl Chloride 14 u
75-00-3---------Chloroethane 14 u
75-09-2---------Methylene Chloride 28 8
67-64-1---------Acetone 44 B
75-15-o--------~carbon Disulfide· 7 u
75-35-4---------1,1-Dichloroethene 7 u
75-34-3---------1,1-Dichloroethane 7 u
540-59-0--------1,2-Dichloroethene {tC)tal)_ 7 u
67-66-3---------Chloroform 2 J
101-06-2--------1,2-oichloroethane 7 u
78~93-3---------2-Butanone 14 u
71-55-6---------1,l,l-Trichloroethane 7 u
56-23-5---------carbon Tetrachloride 7 u
108-05-4--------Vinyl Acetate 14 u
75-27-4---------Bromodichloromethane 7 u
78-87-5---------1,2-Dichloropropane 7 u
10061-0l-S------ci ■-l,3-Dichloropropene 7 u
79-01-6---------Trichloroethene 7 u
124-48-1--------Dibromochloromethane 7 u
79-oo-s---------1,1,2-Trichloroethane 7 u
71-43-2---------Benzene 7 u
10061-02-6------Trans-l,3-Dichloropropene_ 7 u
75-25-2---------Bromoform 7 u
1oa-10-1--------4-Methyl-2-Pentanone 14 u
591-78-6--------2-Hexanone 14 u !
127-18-4--------Tetrachloroethene 7 u
79-34-5---------1,1,2,2-Tetrachloroethane_·_ 7 u
108-88-3--------Toluene 7 u
108-90-7--------Chlorobenzene 7 u
100-41-4--------Ethylbenzene 7 u
100-,2-s--------styr•n• 7 u
1330-20-7-------Total Xylenes 7 u
\
\ FORM I VOA 1/87 Rev.
--=--=---.-~ --. ~~-. -:.:.-=--=--4 E QRIILSUftNRRfi:-----· . 176
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VOIATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SED-6-1
Lab Code: CQMPU Case No.: 17902 SAS No.: SDG No. : .._5_1 __
Matrix: (soil/water) SQII..
Sample wt/vol: 5.0 (g/mL) ~
Level: (low/med) LOW
I Moisture: not dee. _u
Column (pack/cap) CAf
Number TICS found:~
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
290820
GH090820Cl9
09/29/89
10/06/89
1,0
RT EST. CONC. Q
•=s•===========• s=========================== ======== ==~=-========= =====
FORM I VOA-TIC l/87 Rev.
\
1-----
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SED-7-1
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: .._s ... 1 __
Lab Sample ID: .,2"9.:.:..08~1-.9~---
.Lab File ID: · GH090819Cl9
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0 (g/mL) ·!i..._
Level: (low/med) 'LOW Date Received: 09/29/89
I Moisture: not dee. _ll Date Analyzed: 10/06/89
Column: (pack/cap) CAi! Dilution Factor: -1~,0 __ _
'
CAS NO. COMPOUND
CONCENTRATION UNITS-:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane _______ _
7 4-83-9---------Bromomethane. _______ _
75-01-4---------Vinyl Chloride ______ _
75-00-3---------Chloroethane. _______ _
75-09-2---~-----Methylene Chloride ____ _
67-64-1---~-----Acetone __________ _
75-15-o----~----carbon Disulfide ·------75-35-4---------1,l-Dichloroethene ____ _
75-34-3---------1,l-Dichloroethane ____ _
540-59-o--------l,2-Dichloroethene (total)_
67-66-3---------Chlorotorm. ________ _
107-06-2--------1,2-oichloroethane. ____ _
78-93-3---------2-Butanone. ________ _
71-55-6---------1,l,l-Trichloroethane. ___ _
56-23-5---------carbon Tetrachloride. ___ _
108-05-4--------Vinyl Acetate. _______ _
75-27-4---------Bromodichloromethane. ___ _
78-87-s---------l,2-Dichloropropane ____ _
10061~01-S------cis~l,3-Dichloropropene __ _
79-01-6---------Trichloroethene ______ _
124-48-1--------Dibromochloromethane ___ _
79-00-5---------1, 1, 2-Trichloroethane. ___ _
71-43-2---------Benzene _____________ _
10061-02-6------Trans-l,3-Dichloropropene_
75-25-2---------Bromoform. _________ _
101-10-1--------4-Methyl-2-Pentanone. ___ _
591-78-6--------2-Hexanone. ________ _
127-18-4--------Tetrachloroethene. _____ _
79-34-5---------1,1,2,2-Tetrachloroethane_
108-88-3--------Toluene. __________ _
108-90-7-~------Chlorobenzene. _______ _
100-41-4--------Ethylbenzene. _______ _
100-42-s--------styrene. __________ _
1330-20-7-------Total Xylenes. _______ _
FORM I VOA
. -=-~----~ ---·-=..;,-.---~~. ==---

-

-
14 U
14 U
14 U
14 U
19 a
47 B
7 U
7 U
7 U
7 U
3 J
7 U
14 U
7 U
· 7 U
14 U
7 U
7 U
7 U
7 U
7 U
7 U
7 U
7 U
7 U
14 U
14 U
7 U
7 · U
7 U
7 U
7 U
7 U
7 U
Q
1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name:· COMPUCHEM. LABS Contract: (2·-88) -REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. _J.i Date Analyzed:
EPA SAMPLE NO.
SED-7-1
No.: 51
290819
GH090819Cl9
09/29/89
10/06/89
Column (pack/cap) · CAP Dilution Factor: _1-1 0 ___ _
Number TICS found:~
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.
•==•=-----------============================ ======== =============
FORM I VOA-TIC
\
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1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPQCHEM LABS
SL-1-1
Contract: l2-88)-REYS
Lab Code: CQHPU case No.: 17902 SAS No.: SDG No.: 51
Matrix: ( soil/water) ~Qil. Lab Sample ID: · 290826
·Sample wt/vol: 5,0 (g/mL) ~ Lab File ·ID: GH090826Al9
Level:. (low/med) LOW Date Received: 09/29/89
t Moisture: not dee. _u Data Analyzed:· 10/06/89
Column: (pack/cap) CAP Dilution Factor: 1,0
CONCENTRATION UNITS: C
CAS NO. COMPOUND (ug/L or ug/Kg) Y~tG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 19 B·
67-64-1---------Acetone 19 B
1s-1s-o---------carbon Disulfide 6 u
75-35-4---------1,l-Dichloroethene 6 u
75-34-3----~----l,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chlorotorm l J
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-s---------l,2-Dichloropropane 6 u
10061-01-s------cis-l,J-Dichloropropene 6 u
79-01-6-------~-Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-1,3-Dichloropropene_ 6 u
75-25-2-~-------Bromotorm 6 u
1oa-10-1--------4-Methyl-2-Pentanona 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-1-------Total Xylenes 6 u
\ FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET·
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SL-1-1
Lab Name: COMPUCHEM LABS Contract: C2-88l-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: ___ SDG No.: '"'"5._l __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LQW
I Moisture: not dee. __u.
Column (pack/cap) CAi!
Number TICs found: _.Q.
CAS NUMBER
(g/mL) L-
COMPOUND NAME
Lab Sample ID: .249.:,c.08~211..;6-._ __ _
Lab File ID: GH090826Al9
Date Received:· 09/29/89
Date Analyzed: 10/06/89
Dilution Factor: al~,o ___ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
•a•=•================================================--=----=----=====
FORM I VOA-TIC 1/87 Rev.
\
zz -,~MSPPPt e IHI ta308Mllr.::-:._.L 171
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-2-1
Lab Name: COMPUCHEM LABS Contract: <2-88)-REVS
Lab Code: COMPO case No.: 17902 SAS No.: SDG·No.: ..._5._1 __
Matrix: (soil/water) SOIL Lab Sample ID: 290823
Sample wt/vol: 5,0 (g/mL) L_ Lab File ID: GH090823Cl9
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. _-1..Q Date Analyzed: l0/0§/89
Column:
'
(pack/cap) CAf Dilution Factor: _1-.0 __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75~15-o---------carbon Disulfide
75-35-4-~-------l,l-Dichloroethene
75-34-3---------1,l-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-oichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/KG
.
(total)_
71-55-6---------1,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-oichloropropane
10061-0l-S------cis-l,3-0ichloropropene
79~01-6--~------Trichloroethene ·
124-48-1--------Dibroaochloromethane
79-00-5--_.------1,1,2-Trichloroethane
71-43-2---------Benzene
19061-02-6------Trans-l,3-Dichloropropene_
75-2!5-2---------Bromoform
101-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4------~-Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane_
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5----~---styrene
1330-20-7-------Total Xylenes ,
FORM I VOA
11
11.
11
11
52
46
6
6
6
6
l
6
11
6
6
11
6
6
6
6
6
6
6
6
6
11
11
6
6
6
6
6
6
6
== =-c ~SIUIPC E D TR Sl#QIRRV-:,-7: . ___ . _
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u u u
B
B
u
u u u
J u
u
u
u
u
u
u u u u
u
u
u
u
u u
u u u u u
u u
1/87 Rev.
·170
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-2-1
Lab Name: COl'.fPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPO case No.: 17902 SAS No.: SDG No.: _51 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. __ll
Column (pack/cap) CAf
Number TICs found:~
CAS NUMBER
\
(g/mL) ~
COMPOUND NAME
Lab Sample ID: _2 .._9 0.._8=--2..._3,.__ __ _
Lab File ID: GH090823Cl9
Date Received: 09/29/89
Date Analyzed: 10/06/89
Dilution Factor: _1_,o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. . Q
FORM I VOA-TIC l/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-3-1
Lab Code: COMPU case No.: 17902 SAS No.: SOG No.: _5_1 __
Matrix: (soil/water) SQU,t Lab Sampl~ ID: 290849
sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GMQ9Q849Al9
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. _u Date Analyzed: 10/0§/89
Column: (pack/cap) CAf Dilution Factor: . _1_, o __ _
'
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
1s-1s-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-0ichloroethane
540-59-0--------1,2-oichloroethene
67-66-3--------~Chloroform
107-06-2--------1,2-0ichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Rg) UG/XG
(total)_
71-SS-6~--------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-s---------l,2-0ichloropropane
10061-0l-s------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Oibromochlor.omethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6----~-Trans-l,3-Dichloropropene_
75-25-2---------Bromoform
ioa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,l,2,2-Tetrachloroethane__;,_
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styren•
1330-20-7-------Total Xylenes
FORM I VOA
Q
11 u
11 u
11 u
11 u
24 B
20 B
6 u
6 u
6 u
6 u
5 J
6 u
11 u
6 u
6 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
-168
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-2-2
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) sou,. Lab Sample ID: 290829 .
Sample wt/vol: 5,0 (g/mL) L_ Lab File ID: GH090829Al9
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. __u Date Analyzed: 10/0§/89
Column: (pack/cap) ~f Dilution Factor: -1~,-o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/lCG -Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 18 B
67-64-1---------Acetone 21 B
1s-1s-o---------carbon Disulfide 6 u·
75-35-4---------1,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u '
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 2 J
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6~--------l,l,l-Trichloroethane 6 u
56-23-s--~------carbon Tetrachloride 6 u
108-05-4------~-Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-s------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene \ 6 u
10061-02-6------Trans-l,3-Dichloropropene_ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 11 u
591-78~6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5----~~---1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-1-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
-]67
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS,
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE. NO.
SL-2-2
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ....,51 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0 (g/mL)
Level: (low/med) LQW
I Moisture: not dee. -~
Column (pack/cap) CAP
Number TICs found: _J2
L-
Lab Sample ID:
· Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
290829
GH090829Al9
09/29/89
10/06/89
l.Q
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
===============================================a===~==================
\ FORM I VOA-TIC 1/87 Rev.
593PCE -DJITII .SUIIIUIR.y·~-=-· 166
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-3-l
Lab coda: CQMPU Case No.: 17902 SAS No.: SDG No.: ... 5_1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0
Leval: (low/med) LOW
I Moisture: not dee. __u
Column (pack/cap) CAP
Number TICS found: ---2
CAS NUMBER
\
(g/mL) L_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
290849
GH090849Al9
09/29/89
10/06/89
1,0
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC l/87 Rev.
1----···· 165
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-4-1
Lab Code: COMPU . Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab Sample ID: 290831
Sample wt/vol: 5, 0 { g/mL) .G.__ Lab File ID: ~HQ~Q83J.Al9
Level: (low/med) _u;,_,w ___ _ Date Received: 09/29/89
Date Analyzed: 10/0§/89 I Moisture: not dee. ---1.l
Column: (pack/cap) CAP Dilution Factor: _1~1 0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane -.. '1·. ~-.. .-.
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,l-Dichloroethane
540-59-0--------1,2-oichloroethene {total)_
67-66-3---------Chlorotorm
101-06-2--------1,2-oichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5----~----l,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1-~------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene_
75-25-2---------Bromotorm
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane_
1oa-aa-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes·
FORM I VOA
Q
11 u
11 u
11 u
11 u
31 B
16 B
6 u
6 u
6 u
6 u
2 J
6 u
11 u
6 u
6 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SL-4-l
Lab Name: CQMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ______ SDG No.: ..._5_1 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5,0
Level: · (low/med) I.OW
I Moisture: not dee. _ll
Column (pack/cap) CAf
Number TICS found:~
CAS NUMBER
(g/mL) L_
COMPOUND NAME
Lab Sample ID: ...,2.,._9.,._0Bx.3,.__l ____ _
Lab File ID: GH090831Al9
Date Received: 09/29/89
Date Analyzed: 10/06/89
Dilution Factor: _1~1 0,._ __
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/KG
RT· EST. CONC. Q
=•~••--=------=-============================ ======== =s=========== •====
FORM I VOA-TIC l/87 Rev.
-SPWPC E DR lll.. SUlfllllflr¥-: . ·_·-163
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-5-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: .._5 ... 1 __
Ma~rix: (soil/water) SOIL Lab Sample IO: .2.c.9i08~4~5'-----
Sample wt/vol: 5,0 (g/mL) SL_ LaD File ID: GH090845Al9
Level:· ( low/med) LOW
I Moisture: not dee. __u
Column: (pack/cap} CAP
Date Received: 09/29/89
Date Analyzed: 10/06/89
Dilution Factor: _1~1 0,._ __
CONCENTRATION UNITS:'
CAS NO. COMPOUND (ug/L or ug/Kg) UG/XG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75•00-3---------Chlorpethane 11 u
75-09-2---------Methylene Chloride 20 B
67-64-1---------Acetone 22 B
1s-1s-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
540-59-0--------1,2-oichloroethene (total)_ 6 u
67-66-3---------Chloroform 1 J
101-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-s------cia-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethena 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropena_ 6 u
75-25-2---------Bromofora 6 u
1oa-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
CIB!iPLI! DRTD SUIUBIRr:-.. __ _ . J62
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG
Matrix: ( soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) SL_ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. _ll Date Analyzed:
EPA SAMPLE .No.
SL-5-1
No.: 51
290845
GH090845Al9
09/29/89
lQ/Q§/89
Column (pack/cap) ~f Dilution Factor: _1_,o __ _
Number TICS found:~
.. , .. CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT ·EST. CONC.
====-----=----=~ ============================ ======== =============
\ FORM I VOA-TIC
Q
=====
1/87 Rev.
. ...:..:.. ™--:·---=-=--····---·-SRIIPC£. DEJIA. SDJIIMRV.~; ... -161
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-6-1
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPO case No.: 17902 SAS No.: SOG No.: ..._5_1 __
·Matri~: (soil/water) SOIL Lab .Sample IO: 291039
·sample wt/vol: 5,0 (g/mL) L_ Lab File IO: GH09l039Cl9
Level: ( low/med) · LOW Date Received: 09/30/89
Date Analyzed: 10£'.08£'.89 t Moisture: not dee. ----11
Column: (pack/cap) CAP Dilution Factor: _1~1 0...__ __
\
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
1s~1s-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2~-------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGLKG
(total)_
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-s------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanon•
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34•5---------1,1,2,2-Tetrachloroethane_,;._
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styren•
1330-20-7-------Total Xylenes
FORM I VOA
Q
11 u
11 u
11 u
11 u
11 B
5 at
6 u
6 u
6 u
6 u
6 u
6 u
11 u
6 u
6 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 ·u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
160
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM IABS Contract: (2-88}-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
Sample wt/vol: s,o (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee. _u Date Analyzed:
EPA SAMPLE NO.
SL-6-1
No.: 51
291039
GH091039Cl9
09/30/89
10£'.08£'.89
Column (pack/cap) CAE Dilution Factor: _1_,o..._ __
Number TICs found: _..2
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG£'.KG
RT EST. CONC. Q
--=======-=====----=-=---------------=---=-= •======= ============--=-==
FORM I VOA-TIC 1/87 Rev.
\
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
SL-7-1
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: ~5.._1 __
Matrix: (soil/water) SOIL .. Lab Sample IO: 291040
Sample wt/vol: 5.0 (g/mL) L_ Lab File IO: GH091040Cl9
Level: (low/med) LOW Date Received: 09/30/89
, Moisture: not dee. -ll Date Analyzed: 10/Q8f89
Column: (pack/cap) CAP Dilution Factor: .i~,o~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3~--------Chloroethane 11 u
75-09-2---------Methylene Chloride 14 B
67-64-1---------Aceton• 6 BJ
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u .,
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-oichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-oichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-SS-6-~-------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-0l-S------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1os-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34~5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styren• 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
158
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5,0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. _12 Date Analyzed:
. EPA SAMPLE NO.
SL-7-l
No.: 51
291040
GHQ91040Cl9
09/30/89
10/08/89
Column (pack/cap) CAf Dilution Factor: .1~1 0.._ __
Number TICs found: __o,
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KQ
RT EST. CONC. Q
===-============ ============================ •==•===• =-----------= •====
FORM I VOA-TIC 1/87 Rev.
,ail-lili·iii-iiiii. --------------==---.. S .. A=-a;.8u:P;;..L~£ D·RTR .. Slll'lll.ARV-· 157
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1A
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: £2-88}-REVS
SL-8-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ...,5_1 __
Matrix: ('soil/water) SOIL Lab sample ID: 291038
sample wt/vol: 5.0 (g/mL) L-Lab File ID: GR091038Cl9
Level: (low/med) I.OW Date Received: 09/30/89
I Moisture: not dee. ___u Date Analyzed: 10/10/89
Column: (pack/cap) .CAf Dilution Factor: _1~,0--__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/ICg) UG/KG Q
74-87-3--·-------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 29
67-64-1---------Acetone 67
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
540-59-o---~----l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chlorotorm 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-oi-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------l,l,2~Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene_ 6 u ,
75-25-2---------Bromoform 6 u
101-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tatrachloroethane_ 6 u
108-88-3--------Toluen• 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 ·u
100-42-s--------styrene 6 u
1330-20-1-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
I ----156
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET-
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS . Contra~t: (2-88)-REVS
EPA SAMPLE NO.
SL-8-1
Lab Code: COMPO Case No.: 17902 .SAS No.: SDG No.: ..._5-.1 __
Matrix: (soil/water) SOIL
Sample wt/vol: s.o (g/mL) Si__
Level: (low/med) LOW
I Moisture: not dee. ~
Column (pack/cap) . CAf
Number TICS found: __Q
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab File IO:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291038
~BQ91038Cl2
09/30/89
10/10/89
ld2
RT EST. CONC. Q
=====---------=z = ·========================== ======= ============= =====
FORM I VOA-TIC 1/87 Rev.
\
155
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-9-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab sample ID: 291037
Sample wt/vol: 1.8 (g/mL) ~ Lab File ID: ~BQ910371H9
Level: ( low/med) LOW Date Received: 09/30/89
I Moisture: not dee~ _u Date Analyzed: l.QI09l~9
Column: (pack/cap) caP Dilution Factor: .l-·-0.....,... __
'
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 32
74-83-9---------Bromomethane 32
75-01~4---------Vinyl Chloride 32
75-00-3---------Chloroethane 32
75-09-2---------Methylene Chloride 110
67-64-1---------Acetone 240
75-15-o---~-----carbon Disulfide 16
75-35-4---------1,1-Dichloroethene 16
75-34-3---------1,1-Dichloroethane 16
540-59-0--------1,2-Dichloroethene (total)_ 16
67-66-3--~------Chloroform 16
107-06-2--------1,2-Dichloroethane 16
78-93-3--------~2-Butanone 32
71-55-6---------1,l,l-Trichloroethane 16
56-23-5---------carbon Tetrachloride 16
108-05-4--------Vinyl Acetate 32
75-27-4---------Bromodichloromethane 16
78-87-5---------1,2-Dichloropropane 16
10061-0l-S------cis-l,3-Dichloropropene 16
79-01-6-------•-Trichloroethene 16
124-48-1--------Dibromochloromethane 16
79-oo-s---------l,l,2-Trichloroethane 16
71-43-2---------Benzene 16
10061-02-6------Trans-l,3-Dichloropropene_ 16
75-25-2---------Bromoform 16
1os-10-1--------4-Methyl-2-Pentanone 32
591-78•6--------2-Hexanone 32
127-18-4--------Tetrachloroethene 16
79-34-5---------1,1,2,2-Tetrachloroethane_ 16
108-88-3--------Toluene 16
108-90-7--------Chlorobenzene 16
100-41-4--------Ethylbenzene 16
100-42-5--------styrene 16
1330-20-7-------Total Xylenes 16
' • I
FORM I·voA
Q
u
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u
8
8
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u
u
u
u u
u u u u
u u u u u u u
u u
u u u u u u u
u
u
1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: £2-88)-REVS
EPA SAMPLE NO.
SL-9-1
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: ..._5._1 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 1.8 (g/mL) ~
Level: (low/med) LOW
% Moisture: not dee. -1.i
Column (pack/cap) CAP
Number TICs found: __o,
CAS NUMBER. COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG .
2910J7
~B09l037Bl9
09/30/89
10/09/89
1 I 0
RT EST. CONC. Q
================ ============================ ======== ============= =====
\ FORM I VOA-TIC 1/87 Rev.
--: .. -"" SRJIPL E DR TR Smut8R't~--153'
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-9-lRE
Lab Code: COMPO Case No.: 17902 SAS No.: SOG No.: ""'5._1 __
Matrix: (soil/water) SOIL Lab Sample ID: 291037
Sample wt/vol: s.o (g/mL) L__ Lab File ID: G2R91037Cl9
Level:• (low/med) LOW Date Received: 09/30/89
% Moisture: not dee. _li Date Analyzed: lO/l0/89
Column: (pack/cap) CAP Dilution Factor: l,O
CONCENTRATION UNITS: ,-
CAS NO. COMPOUND (ug/L or ug/Kg) tlGIKG Q
74-87-3---------Chloromethane ' 12 u
74-83-9---------Bromomethane 12 u
75-01-4------~--Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methy~ene Chloride 37 a.
67-64-1---------Acetone 79 B
1s-1s-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3~---~----l,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-SS-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4----~----Bromodichloromethane 6 u
78-87-s---------l,2-Dichloropropane 6 u
10061-0l-s------cis-l,3~Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene_ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetr~chloroethane_ 6 u
108-88-3--------Toluene 6· u
108-90-7---~----Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5----~---styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
152
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab sample ID:
Sample wt/vol: s.o (g/mL) L-Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. _li Date Analyzed:
EPA SAMPLE NO.
SL-9-lRE
No.: 51
291037
~2B9 J.03 7CJ.9
09/30/89
10/lQ/89
Column (pack/cap) ~AP Dilution Factor: -l.~•o..__ __
Number TICs found: __l
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
===-----------== ============================ ~======= ============= =====
1. INSTRUMENT ARTIFACT 1.27 5.8 J
' FORM I VOA-TIC 1/87 Rev.
1----w -Z=~------=---__ ,-___ ·-. --· SMPCE DRIil SU88RR¥.-:,._. 151
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~.r:·=== --•.<ii-~
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS 9l69SED81MS
Lab Code: COMPO case No.: 17902 SAS No.: SOG No.: ..._5_1 __
Matrix: (soil/water) SOIL. Lab Sample ID: 288566
Sample wt/vol: 5.0 (g/mL) L-Lab File ID: GH088566Cl9
Level: (low/med) I.OW ·Date Received: 09/22/89
I Moisture: not dee. ---1. Date Analyzed: 09/J0/89
Column: (pack/cap) CAf Dilution Factor: .i~, .... o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) OG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o------~--carbon Disulfide
75~35-4---~-----l,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2-~------l,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4-~-------Bromodichloromethane
1e-e1-s---------1,2-Dichloropropane
10061-0l-S------cis-l,3-Dichloropropene
79-01-.6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2--------.;.Bromoform
101-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane_
108-88-3---~----Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene '
l~Jo-20-1-------Total Xylene&
FORM I VOA
Q
11 · u
11 u
11 u
11 u
10 B
14 B ..
5 u
5 u
5 u
5 u
5 u
5 u
11 u
' 5 u
5 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
11 u
11 u
5 u
5 u
5 u
5 ·u
5 u
5 u
5 u
1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
9169SED81MSD
Lab Code: COMPU ·Case No.: 17902 SAS No.: SDG No. : .x.Sa.l __
Matrix: (soil/water) SOIL Lab, Sample ID: ..,2..._8..._8..._56.._7,__ __ _
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH088567Cl9
Level: (low/med) LOW
I Moisture: not dee. -1
Date Received: 09/22/89
Date Analyzed: 09/30/89
Column: (pack/cap) ~f Dilution Factor: .i~.o __ _
CONCENTRATION UN.ITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG . Q
74-87~3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl .Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 11 B
67-64-1---------Acetone 16 B
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-S------cis-l,3-Dichloropropene 5 u
79-01-6~--------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trana-l,3-Dichlor~propene __ 5 u
75-25-2--~------Bromoform 5 u
1oa-10-1--------4-Methyl-2-Pentanone ll u
591-78-6--------2-Hexanone 11 u
127-18~4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene I 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
\ FORM I VOA 1/87 Rev.
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
9168SED21
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ..._5 .. 1 __
Matrix: (soil/water) SOIL Lab Sample ID: ._2 :.:..8 8~5,4:1..:S"-----
Sample wt/vol: 30,0
LOW
(g/mL) L-Lab File ID: GH088545A22
Level: (low/med)
% Moisture: not dee.~
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL.
dee.
pH: 7.1
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/30/89
Dilution Factor: al4.0~0"'--
CONCEHTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG · Q
, 108-95-2--------Phenol 720 u
lll-44-4-----~--bis(2-Chloroethyl)Ether 720 u.
95-57-8---------2-Chlorophenol 720 u
541-73-1--------1,3-Dichlorobenzene. 720 U.
106-46-7--------1,4-Dichlorobenzene 720 u
100-51-6--------Benzyl Alcohol 720 u
95-50-1---------1,2-Dichlorobenzene 720 u
95-48-7---------2-Methylphenol 720 U·
39638-32-9------bis(2-Chloroisopropyl)Ether_ 720 u
106-44-5--------4-Methylphenol 720 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 720 u
67-72-1---------Hexachloroethane 720 u
98-95-3---------Nitrobenzene 720 u
78-59-1---------Isophorone 720 u
88-75-5---------2-Nitrophenol 720 u
105-67-9--------2,4-Dimethylphenol 720 u
65-85-o---------Benzoic Acid 270 BJ
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 720 u
120-83-2--------2,4-Dichlorophenol 720 u
120-e2-1--------1,2,4-Trichlorobenzene 720 u
91-20-3---------Naphthalene 720 u
106~47-8--------4-Chloroaniline 720 u
87-68-3---------Hexachlorobutadiene 720 u
59-50-7---------4-Chloro-3-Methylphenol 720 u
91-57-6---------2-Methylnaphthalene 720 u
77-47-4---------Hexachlorocyclopentadiene_ 720 u
88-06-2-~-------2,4,6-Trichlorophenol 720 u
95-95-4---------2,4,S-Trichlorophenol 3500 u
91-58-7---------2-Chloronaphthalene 720 u
88-74-4---------2-Nitroanilin• 3500 u
131-11-3--------Dimethyl Phthalate 720 u
208-96-e-----~--Acenaphthylene 720 u
606-20-2--------2,6-Dinitrotoluene 720 u
FORM I sv-1 1/87 Rev.
----------------·-----·-----•rffll---·-. .......... .-,_m_ .. a~-~cirr-...SuMma~PCE DRT8 SJJIUBIRlE-:.~ 148
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
9168SED21
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ...,5.._1 __
Matrix: (soil/water) SOIL Lab Sample ID: .2~8=8...,54~5,._ __ _
Sample wt/vol: 30.0 (g/mL) L-Lab File ID: GH088545A22
Level: ( low/med) LOW
% Moisture: not dee. _.5,i dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H_ pH: 7.1
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/30/89
Dilution Factor: _1~,o=oL-_
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 3500 u
83-32-9---------Acenaphthene 720 u
51-28-5---------2,4-Dinitrophenol 3500 u
100-02-1--------4-Nitrophenol 3500 u
132-64-9--------Dibenzofuran 720 u
121-14-2--------2,4-Dinitrotoluene 720 u
84-66-2---------Diethylphthalate 720 u
7005-72-3-------4-Chlorophenyl-phenylether_ 720 u
86-73-7---------Fluorene 720 u
100-01-6--------4-Nitroaniline 3500 U.
534-52-1---~----4,6-Dinitro-2-Methylphenol_ 3500 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 720 u
101-55-3--------4-Bromophenyl-phenylether_ 720 u
118-74-1--------Hexachlorobenzene 720 u
87-86-5---------Pentachlorophenol 3500 u
85-01-a---------Phenanthrene 720 u
120-12-1--------Anthracene 720 u
84-74-2---------Di-n-Butylphthalate 720 u
206-44-0--------Fluoranthene 720 u
129-00-0--------Pyrane 720 u
85-68-7---------Butylbenzylphthalate 720 u
91-94-1---------3,3'-Dichlorobenzidine 1400 u
56-55-3---------Benzo(a)Anthracene 720. u
218-01-9----~---Chrysene ; 720 u
·111-a1-1----~---bis(2-Ethylhexyl)Phthalate_ 720 u
117-84-o-------~Di-n-octyl Phthalate 720 u
205-99-2--------Benzo(b)Fluoranthene 720 u
207-08-9--------Benzo(k)Fluoranthene 720 u
50-32~8---------Benzo(a)Pyrene 720 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 720 u
53-70-3---------Dibenzo(a,h)Anthracene 720 u
191-24-2--------Benzo(g,h,i)Perylene 720 u
(1) -Cannot be separated from Diphenylamine
1/87 Rev.
I ----147
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lF.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
9168SED21
Lab code: COMPO Case No.: 17902 SAS No.: SOG No. : __ 5_1 __
Matrix: (soil/water) SOIL Lab Sample IO: 288545
Sample wt/vol: 30,0 (g/mL) ~ Lab File IO: ~HQ88545Ai2
Level: (low/med) ,_LO,._,W __ _ Date Received: 09/22/89
% Moisture: not dee. _2.1 dee. Date Extracted: 09/28/89
Extraction: Date Analyzed: 09/30/89
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li._ pH: 7.1 Dilution Factor: l,Qo
Number TICs found:~
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.
================ ============================ =•====== =====·=======
1. BLANK CONTAMINANT. 4.85 800
2. BLANK CONTAMINANT 4.95 510
3. r UNKNOWN 5.77 1400
4. 4889-83-2 BICYCL0[3.l.l]HEPT-2-ENE, 3, 5.87 3100
5. ALDOL 5.97 2100
6. ALDOL 6.50 580
7. aNKNOWN 6.75 1700
8. UNKNOWN SUBST. HYDROCARBON 7.20 1300
9. UNKNOWN 10.80 290
10. UNKNOWN 11.14 14000
11. UNKNOWN 11 .• 20 290
12. UNKNOWN 11.92 940
13. UNKNOWN 12.44 940
14. UNKNOWN 15.60 800
15. UNKNOWN 16.75 580
16. UNKNOWN 17.59 290
17. UNKNOWN 17.74 9400
18. UNKNOWN 19.70 360
19. UNKNOWN HYDROCARBON 20.00 1400
20. UNKNOWN 20.45 430
21. UNKNOWN 21.34 580
\
FORM I sv~TIC
DRTR SUlflUDlt._
Q
=====
BJ
BJ
J
J
AJ
AJ
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J
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J
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1/87 Rev.
146
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA_ SAMPLE NO.
9169SED81
Lab Name: COMPUCHEM LABS contract: (2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ____ SDG No._: ..._5._1 __
Matrix: (soil/water) SOIL Lab Sample ID: ..,2,.,..8-8 5...,5...,8,.__ __ _
Sample wt/vol: 30.0 (g/mL) L__ Lab File ID: GH088558A22
Level: ( low/med) LOW
% Moisture: not dee. ---7. dee.
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/30/89
Dilution Factor: ..,l~,0=0=---
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_ pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 350
lll-44-4--------bis(2-Chloroethyl)Ether 350
95-57-8---------2-Chlorophenol 350
541-73-1--------1,3-Dichlorobenzene 350
106-46-7--------1,4-Dichlorobenzene . 350
100-51-6--------Benzyl Alcohol 350
95-50-1---------1,2-oichlorobenzene 350
95-48-7---------2-Methylphenol 350
39638-32-9------bis(2-Chloroisopropyl)Ether_ 350
106-44-5--------4-Methylphenol 350
621-64-7--------N-Nitroso-Di-n-Propylamine_ 350
67-72-1--~------Hexachloroethane 350
98-95-3---------Nitrobenzene 350
78-59-1---------Isophorone 350
88-75-5-------~-2-Nitrophenol 350
105-67-9--------2,4-Dimethylphenol 350
65-ss-o---------Benzoic Acid 1700
lll-91-l--------bis(2-Chloroethoxy)Methane_ 350
120-83-2--------2,4-Dichlorophenol 350
120-s2-1--------1,2,4-Trichlorobenzene 350
91-20-3--------Naphthalene 350
106-47-8--------4-Chloroaniline 350
87-68-3---------Hexachlorobutadiene 350
59-50-7---------4-Chloro-3-Methylphenol 350
91-57-6---------2-Methylnaphthalene 350
77-47-4---------Hexachlorocyclopentadiene __ · 350
88-06-2---------2,4,6-Trichlorophenol 350
95-95-4---------2,4,5-Trichlorophenol 1700
91-58-7---------2-Chloronaphthalene 350
88-74-4---------2-Nitroaniline 1700
131-11-3--------Dimethyl Phthalate 350
208-96-8--------Acenaphthylene 350
606-20-2--------2,6-Dinitrotoluene 350
FORM I sv-1
'
Q
u u u
U. u u u u u u u u u u u u u u u u u u u
u u u
u u u
u u
u
u
1/87 Rev.
145
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
9169SE081
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No~: 51
Matrix: (soil/water) SOIL Lab Sample ID: 288558
Sample wt/vol: 30,0 (g/mL) L_ La}:j File ID: !.iHQ88558A22
Level: ( low/med) LOW Date Received: 09/22/89
% Moisture: not dee. __ 7 dee. Date Extracted: 09/28/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lL_ pH:
Date Analyzed: 09/30/89
Dilution Factor: 1.00
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700
83-32-9---------Acenaphthene 350
51-28-5---------2,4-Dinitrophenol 1700
100-02-1--------4-Nitrophenol 1700
132-64-9--~-----Dibenzoturan 350
121-14-2--------2~4-Dinitrotoluene 350
84-66-2---------Diethylphthalate 350
7005-72-3-------4-Chlorophenyl-phenylether_ 350
86~73-7---------Fluorene 350
100-01-6--------4-Nitroaniline 1700
534-52-1---~----.4, 6-Dinitro-2-Methylphenol_ 1700
86-30-6---------N~Nitrosodiphenylamine (1)_ 350
101-55-3--------4-Bromophenyl-phenylether_ 350
118-74-1--------Hexachlorobenzene 350
87-86-5---------Pentachlorophenol 1700
85-01-8---------Phenanthrene 42
120-12-1--------Anthracene 350
84-74-2---------Di-n-Butylphthalate 350
206-44-0--------Fluoranthene 350
129-oo-o-~------Pyrene 350
85-68-7---------Butylbenzylphthalate 350
91-94-1-----~---3, 3 '-Dichlorobenz.idine 710
56-55-3---------Benzo(a)Anthracene 350
218-01-9--------chrysene 350
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 350
117-84-o--------Di-n-octyl Phthalate 350
205-99-2--------Benzo(b)Fluoranthene 350
207-08-9---~----Benzo(k)Fluoranthene 350
50-32-8---------Benzo(a)Pyrene 350
193-39-5--------Indeno(l,2,3-cd)Pyrene 350
53-70-3---------Dibenzo(a,h)Anthracene 350
191-24-2--------Benzo(g,h,i)Perylene 350
(1) -cannot be separated trom Diphenylamin•
FORM I sv-2
DATA SUIUIIHl'Ei -·~
Q
u
u
u
U·
u u u u u u u u u u u
J u u u
u
u u u
u
u u
u
u
u u u
u
1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
·Lab Name: COMPUCHEM LABS Contract: C2~88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) L..._ ' Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee. ---2. dee. Date Extracted:
EPA SAMPLE NO.
9169SED81
No.: 51
288558
GH088558A22
09/22/89
09/281'.'.89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li__ pH:
Date Analyzed: 091'.'.30/89
Dilution Factor: -1-,0~Q~· __
Number TICS found: _,i
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(uq/L or ug/Kg) UG/XG
RT EST. CONC.
===============• -----==------=---------=--== ======== =========.a====
1. BLANK CONTAMINANT 4.93 430
2. ~LANK CONTAMINANT 5.03 2.90
3. UNKNOWN 5.85 320
4. ALDOL 6.05 320
5. 29812-79-1 HYDROXYLAMINE, 0-DECYL-).3.09 290
6. 17301-3'2-5 UNDECANE, 4,7-DIMETHYL-13.80 320
7. 7045-71-8 UNDECANE, 2-KETHYL-14.49 390
8. 54105-67-8 HEPTADECANE, 2,6-DIKETHYL-15.14 360
9. 17301-32-5 UNDECANE, 4,7-DIMETHYL-15.75 250
FORM I SV-TIC
. == =:-"."; SMP! E _ DR TA SU.l'IIIID<l~:.-~
Q
-====
BJ
BJ
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1/87 Rev.
143
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO·.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS 9169SED91
Lab Code: COMPU Case No.: 17902 . SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) L_
Level: ( low/med) LOW
% Moisture: not dee. _ll dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) L... pH: 7 1 8
SDG No.: __ 5_1 __
Lab Sample ID: 288574 -----=-'-'-----
Lab File ID: GH088574A22
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/29/89
Dilution Factor: _1_,-0_0 __
CAS NO. COMPOUND
CONCENTRATION UNITS: C
· (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 2300
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Berizyl·Alcohol 370 u
95-50-1---------1,2-oichlorobenzen• 370 u
95-48-7---------2-Methylphenol 2100
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3---------Nitrobenzene 790
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-0imethylphenol 370 u
65-85-0---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-a2-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u_
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene __ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1700 J
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene · 660
606-2Q-2--------2,6-Dinitrotoluene ·750
FORM I sv-1 1/87 Rev.
........ --....,,....~=------------,--..e~-.. n.,•-1:1.,,r-mt-n n Ta C'flMNDDV 142
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
9169SE091
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -=-5~1 __
Matrix: (soil/water) SOIL Lab Samp 1 e ID: ...,2.x.8 ~8 :::i:..5 7.:...:4::!..._ __ _
sample wt/vol: 30.0 (g/mL) Q__ Lab File ID: GH088574A22
Level: ( low/med) LOW
% Moisture: not dee. _ll dee.
Date Received: 09/22/89
Date Extracted: 09/28/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li....:... pH: 7.8
Date Analyzed: 09/29/89
Dilution Factor:·Al~-&o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5------~--2,4-Dinitrophenol 1800
100-02-7--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-66~2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 370
101-55-3--------4-Bromophenyl-phenylether_ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1500
ss-01-a---------Phenanthrene 40
120-12-1--------Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-o--------Fluoranthene 1100
129-oo-o--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1---------3,3'-Dichlorobenzidine 740
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 1300
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 180
117-84-0------~-Di-n-Octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370·
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 920
(l) -cannot be separated from D1phenylam1ne
FORM I sv-2
Q
u
u u u
u
u u
u
u u u
u
u u
J
J
u
u
u
u
u
u
BJ
u u
u u u
u
1/87 Rev.
141
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHE-ET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: CQMPU Case No._: 17902 SAS No. : SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee. ~ dee. Date Extracted:
EPA SAMPLE NO.
9169SED91
No.: 51
288574
GH088574A22
09/22/89
09/28/89
Extraction: (SepF/Cont/Sonc) S,,QHC Date Analyzed: 09/29/89
GPC Cleanup: (Y/N) li,__ pH: 7.8 Dilution Factor: _1_.o_o...__
CONCENTRATION UNITS:
Number TICs found:~ (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ============================ ======== ============= ----------
1. BLANK CONTAMINANT 5.20 260 BJ
2. DIMETHYLUNDECANE ISOMER 13.27 260 J
3. DIMETHYLHEPTAOECANE ISOMER 13.99 300 J
4. DIMETHYLHEPTADECANE ISOMER 14.67 370 J
5. DIMETHYLHEPTADECANE ISOMER 15.30 260 J
FORM I SV-TIC 1/87 Rev.
\
·::i:trir -SAftPC 4; -DJJ tJ;J_ ~y-· _ 140
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-1-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: . 30, o (g/mL) ~
Level: ( low/med) LOW
% Moisture: not dee. ___l§_ dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H,__ pH: 7,9
SDG No.: ""-5._1 __
Lab Samp 1 e ID: ... 2 .._9 ._l 0=3z...:6,.__ __ _
Lab File ID: GH091036C20
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: 1,00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or·ug/Kg) UG/KG Q
108-95-2--------Phenol 2400 u
lll-44-4--------bis(2-Chloroethyl)Ether 2400 u
95-57-8---------2-Chlorophenol 2400 u
541-73-1--------1, 3-Dichlorob.enzene 2400 u
106-46-7--~-----l,4-Dichlorobenzene 2400 u
100-51-6--------Benzyl Alcohol 2400 · u
95-50-1---------1,2-oichlorobenzene 2400 u
95-48-7---------2-Methylphenol 2400 ·u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 2400 .u
106-44-5--------4-Methylphenol 2400 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 2400 u
67-72-1---------Hexachloroethane 2400 u
98-95-3---------Nitrobenzene 2400 u
78-59-1---------Isophorone 2400 u
88-75-s---------2-Nitrophenol 2400 u
105-67-9--------2,4-Dimethylphenol 2400 u
65-85-o---------Benzoic Acid 11000 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 240,0 u
120-83-2--------2,4-Dichlorophenol 2400 u
120-s2-1--------i~2,4-Trichlorobenzene 2400 u
91-20-3---------Naphthalene 2400 u
106-47-8--------4-Chloroaniline 2400 u
87-68-3---------Hexachlorobutadiene 2400 u
59-50-7---------4-Chloro-J~Methylphenol 2400 u
91-57-6---------2-Methylnaphthalene 2400 u
77-47-4---------Hexachlorocyclopentadiene __ 2400 u
88-06-2---------2,4,6-Trichlorophenol 2400 u
95-95-4---------2,4,5-Trichlorophenol 11000 u
91-58-7---------2-Chloronaphthalene 2400 u
88-74-4---------2-Nitroaniline 11000 u
131-11-3~-------Dimethyl Phthalate 2400 u
208-96-8--------Acenaphthylene 2400 u
606-20-2--------2,6-Dinitrotoluene 2400 u
'
\ FORM I sv-1 1/87 Rev.
.... ~iiii-__ iiiii_iiii_iilio ___ ,;oii·.-.. ~;.,.~ii:,i·:.,_iii,;~---·-..... --------...... -.--iii,,ii.....,...,.........,;;__· .... -~-5 .... Rli--P .... l-E-DR TR .. SUl'lllHRt_ -... f39 -
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS Contract: l2-88l-REVS
SE0,-1-1
Lab Code: COMPu Case No.: 17902
Matrix: (soil/water) SOIL
SAS No.: SOG No.: .:..5_1 __
Lab Sample ID: ..,2"'9 .._l Ox.,;3"-'6=-------
Sample wt/vol: 30,0 (g/mL) L__ Lab File ID: GH091036C20
Level: ( low/med) I.OW Date Received: 09/30/89
I Moisture: not dee.~
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H.,_
dee.
pH: 7,9
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: _1~,0-0,.____
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 11000 u
83-32-9---------Acenaphthene 2400 u
51-28-5---------2,4-Dinitrophenol 11000 u
100-02-1--------4-Nitrophenol 11000 u·
132-64-9--------Dibenzoturan 2400 u
121-14-2--------2,4-Dinitrotoluene 2400 u·
84-66-2---------Diethylphthalate 2400 u
7005-72-3-------4-Chlorophenyl-phenylether_ 2400 u
86-73-7---------Fluorene 2400 u
100-01-6--------4-Nitroaniline 11000 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 11000 u
86-30-6-~-------N-Nftrosodiphenylamine (1)_ 2400 u
101-55-3--------4-Bromophenyl-phenylether __ 2400 u
118-74-1--------Hexachlorobenzene 2400 u
87-86-5---------Pentachlorophenol 11000 u
85-01-8---------Phenanthrene 2400 u
120-12-1--------Anthracene 2400 u
84-74-2---------oi-n-Butylphthalate 2400 u
206-44-0--------Fluoranthene 2400 u
129-00-o--------Pyrene 2400 u
85-68-7---------Butylbenzylphthalate 2400 u
91-94-1---------3,J'-Dichlorobenzidine 4700 u
56-55-3---------Benzo(a)Anthracene 2400 u
218-01-9--------Chrysene 2400 u
ll7-81-7-~------bis(2-Ethylhexyl)Phthalate_ 2400 u
117-84-o--------oi-n-octyl Phthalate 2400 u
205-99-2--------Benzo(b)Fluoranthene 2400 u
207-08-9--------Benzo(k)Fluoranthene 2400 u
so-J2-a---------Benzo(a)Pyrene 2400 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 2400 u
53-70-3---------Dibenzo(a,h)Anthracene 2400 u
191-24-2--------Benzo(g,h,i)Perylene 2400 u
(1) -cannot be separated trom Dip~enylamine
FORM I sv-2 1/87 Rev.
SA8PL£ DA TA S.LIIUIBR~-· 138
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REYS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG
Matrix: (soil/water} SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
' Moisture: not dee. _u dee. Date Extracted:
EPA SAMPLE NO.
SED-1-1
No.: 51
291036
GH091036C20
09/30/89
lQ/0~/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lf.._ pH: 7,9
Date Analyzed: 10/07/89
Dilution Factor; _1_,0~0---
Number TICs found: .-12
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. . ==----=----=---= ============================ =-=-••=a=z:a: =----=----=--
1. BLANK CONTAMINANT 4.42 1400
2. ALDOL 5.23 13000
3. ALDOL 5.47 10000
4. ALDOL 5.60 2100
5. ALDOL 6.02 3100
6. UNKNOWN 6.70 12000
7. VNKNOWN 6.77 4000
8. UNKNOWN a.so 1400
9. UNKNOWN 12.62 2600
10. TRIBROMOPHENOL ISOMER 13.04 1400
11. UNKNOWN 14.42 1900
12. UNKNOWN 18.69 3300
13. UNKNOWN 19.22 1400
. 14 ·• UNl(NOWN 22.80 3800
15. UNKNOWN 22.92 6700
\ FORM I SV-TIC
Q
•====
BJ
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AJ
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1/87 Rev.
137
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
SED-3-1
Lab code: COMPU case No.: 17902 SAS No.: SDG No.: .... 5 .... i __
Lab Sample ID: 291034 Matrix: (soil/water) SOIL -~~---
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH091034C20
Level: (low/med) _r.o_w ____ _
% Moisture: not dee. -1,i dee.
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: 1 1 00
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H.._ pH: 7,7
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 410 u
lll-44-4--------bis(2-Chloroethyl)Ether 410 u·
95-57-8---------2-Chlorophenol 410 u
541-73-1--------1,3-Dichlorobenzene 410 u
106-46-7--------1,4-Dichlorobenzene 410 u
100-51-6--------Benzyl Alcohol 410 u
95-50-1---------l,2-Dichlorobenzene 410 u
95-48-7---------2-Methylphenol. 410 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u
106-44-5--------4-Methylphenol 410 u
621-6(-7--------N-Nitroso-Di-n-Propylamine_ 410 u
67-72-1---------Hexachloroethane 410 u
98-95-3---------Nitrobenzene 410 u
78-59-1---------Isophorone 410 u
88-75-5---------2-Nitrophenol 410 u
105-67-9--------2,4-Dimethylphenol 410 u
65-ss-o---------Benzoic Acid 2000 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 410 u
120-83-2--------2,4-Di~hlorophenol 410 u
120-a2-1--------1,2,4-Trichlorobenzene 410 u
91-20-3---------Naphthalene 410 u
106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7---------4-Chloro-3-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47-4---------Hexachlorocyclopentadiene_ 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,S-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 410 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 410 u
208-96-8--------Acenaphthylene 410 u
606-20-2--------2,6-Dinitrotoluene 410 u
\ FORM I sv-1 1/87 Rev.
SA8P.L£ DATA SU88RRV: __ 136
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-3-1
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab Sample ID: 291034
sample wt/vol: 30,0 (g/mL) ~-Lab File ID: GH091034C20
Level: ( low/med) LOW Date Received: 09/30/89
t Moisture: not dee. _u dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc)
(Y/N) ti._
Date Analyzed: 10/07/89
GPC Cleanup: pH: 7,7 Dilution Factor: _1~.Q~O,.___
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2000 u
83-32-9---------Acenaphthene 410 u
51-28-5---------2,4-Dinitrophenol 2000 u
100-02-1--------4-Nitrophenol 2000 u
132-64-9--------Dibenzofuran 410 u
121-14-2--------2,4-Dinitrotoluene 410 u
84-66-2---------Diethylphthalate 410 u
7005-72-3-------4-Chlorophenyl-phenylether_ 410 u
86-73-7---------Fluorene 410 u
100-01-6--------4-Nitroaniline 2000 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 410 u
101-55-3--------4-Bromophenyl-phenylether __ 410 u
118-74-1---~----Hexachlorobenzene · 410 u
87-86-5---------Pentachlorophenol 2000 u
85-01-8.---------Phenanthrene 410 u
120-12-1--------Anthracene 410 u
84-74-2---------Di-n-Butylphthalate 410 u
206-44-o--------Fluoranthene 410 u
129-00-0--~-----Pyrene 410 u·
85-68-7---------Butylbenzylphthalate 410 u
91-94-1---------3,3'-Dichlorobenzidine 820 u
56-55-3---------Benzo(a)Anthracene 410 u
218-01-9--------Chrysene 410 u
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 410 u
117-84-o--------Di-n-octyl Phthalate 410 u
205-99-2--------Benzo(b)Fluoranthene 410 u
207-08-9--------Benzo(k)Fluoranthene 410 u
50-32-8---------Benzo(a)Pyrene 410 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 410 u
53-70-3---------Dibenzo(a,h)Anthracene 410 u
191-24-2--------Benzo(g,h,i)Perylene 410 u
(1) -cannot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
. .,
-----===-~--,,_,.~-:.. ..... ~ .... ·---~-----------------~•C'""Jlft-MD.-r1,li'-n•"""a-T..,,a-"C'_l,..,l"N-N"D-li'ny~-----135
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SED-3-1
Lab Code: COMPO Case No.: 17902 SAS No.:, __ _ SDG .No. : .-5_1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30,0 (g/mL) ~
Level: ( low/med) LOW
I Moisture: not dee.~ dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ti_ pH: 7,7
Number TICS found:~
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291034
~H091Q34C,o
09/30/89
10/04/89
10/07/89
1.00
RT EST. CONC. Q
=••============-============================ ============= •====
1. BLANK CONTAMINANT
2, BROMOHEXANE
3. ALDOL
4. UNKNOWN
' FORM I SV-TIC
4,33
5.27
5.50
6.75
210 BJ
490 J
660 'AJ
530 J
1/87 Rev.
________ .,._, __ ,--=i-==:-----·-· 134 ---......====~=-==~~~----s~a,..erzp71~rr~ DATA SWVIRKF' --. :.:..-
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS SED-3-2
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: _5_1 __
Matrix: (soil/water) SOIL Lab Sample IO: _2._9..,l.,._0.,._3'"'-5 __ _
Sample wt/vol: 30.0 (g/mL) L_ Lab File IO: GH091035C20.
Level: (low/med) _LO_w __
t Moisture: not dee. __a dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H__ pH: 7.5
Qate Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: l,OO
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 400 u
lll-44-4---~----bis(2-Chloroethyl)Ether 400 u
95-57-8---------2-Chlorophenol 400 u
541-73-1--------l,3-Dichlorobenzene 400 u
106-46-7--------1,4-Dichlorobenzene 400 u
100-51-6--------Benzyl Alcohol 400 u
95-50-1---------1,2-oichlorobenzene 400 u
95-48-7---------2-Methylphenol 400 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 400 u
106-44-5--------4-Methylphenol . 400 u
621-64-7--------N-Nitroso-oi-n-Propylamine_ 400 u
67-72-1---------Hexachloroethane 400 u
98-95-3---------Nitrobenzene 400 u
78-59-1-----~---Isophorone 400 u
88-75•5---------2-Nitrophenol 400 u
105-67-9--------2,4-0imethylphenol 400 u
65-as-o---------Benzoic•Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 400 u
120-aJ-2--------2,4-0ichlorophenol 400 u
120-a2-1--------1,2,4-Trichlorobenzene 400 u
91-20-3---------Naphthalene 400 u
106-47-8--------4-Chloroaniline 400 u
87-68-3---------Hexachlorobutadiene 400 u
59-5.0-7---------4-Chloro-3-Methylphenol 400 u
91-57-6---------2-Methylnaphthalene 400 u
77-47-4---------Hexachlorocyclopentadiene_ 400 u
88-06-2---------2,4,6-Trichlorophenol 400 u
95-95-4---------2,4,5-Trichlor~phenol 2000 u
91-58-7---------2-Chloronaphthalane 400 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 400 u
208-96-a--------Acenaphthylene 400 u
606-20-2--------2,6-0initrotoluene 400 u
\ FORM I sv-1 1/87 Rev.
--:-=-~ .... -.,.~.-:-:-: .. ~-""'."'.":"'----~---:-.-:-."'1!5~g,..9a2pnLrEr---DR TR SONNRRY _ 133
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SED-3-2
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : _5_1 __
Matrix: (soil/water) SOIL La.b Sample ID: _2...._9 ... l..._03""'5,.__ __ _
Sample wt/vol: 30,0 (g/mL) L-Lab File ID: GH091035C20
Level: ( low/med) LOW
% Moisture: not dee. ___li dee.
Extraction: (SepF/Cont/Sonc)
('i/N) IL_
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
GPC Cleanup: pH: 7.5 Dilution Factor: --1..._, O...,o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2000
83-32-9-~-------Acenaphthene 400
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Di.benzofuran 400
121-14-2--------2,4-Dinitrotoluene 400
84-66-2---------Diethylphthalate 400
7005-72-3-------4-Chlorophenyl-phenylether_ 400
86-73-7----~----Fluorene 400
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000
86-30-6---------N-Nitrosodiphenylamine (l)_ 400
101-55-3--------4-Bromophenyl-phenylether_ 400
118-74-1--------Hexachloro.benzene 400
87-86-5---------Pentachlorophenol 2000
es-01-e---------Phenanthrene 400
120-12-1--------Anthracene 400
84-74-2---------oi-n-Butylphthalate 400
206-44-0--------Fluoranthene 81
129-oo-o--------Pyrene 47
85-68-7---------Butyl.benzylphthalate 400
91-94-1---~-----3,3'-Dichloro.benzidine 810
56-55-3---------Benzo(a)Anthracene 400
218-01-9--------Chrysene 45
ll7-8l-7--------.bis(2-Ethylhexyl)Phthalate_ 400
117-84-o--------Di-n-octyl Phthalate 400
205-99-2--------Benzo(.b)Fluoranthene 400
207-08-9--------Benzo(k)Fluoranthene 400
50-32-e---------Benzo(a)Pyrene 400
193-39-5--------Indeno(l,2,3-cd)Pyrene 400
53-70-3---------Di.benzo(a,h)Anthracene 400
191-24-2--------Benzo(g,h,i)Parylene 400
(l) -Cannot .be separated from D1phenylam1ne
Q
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u
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u u u u
u u
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J u u u
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u u u u u u u u
FORM I sv-2
I
1------,---------===--... --_______________ 5_ps:a&<ft ...... ~LE -DRTR SUl'llfRRV. ·
l/87 Rev.
132
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) L-Lab File ID:
Level: (low/med) LOW Date Received:
' Moisture: not dee. _ll, dee. Date Extracted:
EPA SAMPLE NO.
SED-3-2
No.: 51
291035
GH09l035C20
09/30/89
10/0~/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti,_. pH: 7,5
Date Analyzed: 10/07/89
Dilution Factor: _1_,0-0....__
Number TICS found:~
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER
================
\
1.
2. 3377-87-5
3.
4.
5.
COMPOUND NAME ============================
BLANK CONTAMINANT
HEXANE, 3-BROMO-
_ALDOL
UNKNOWN
UNKNOWN
RT ========
4.35
5.28
5.52
6.77
8.84
FORM I SV-TIC
EST. CONC. =============
• 240
490
730
650
160
Q
=====
BJ
J
A]
J
J
1/87 Rev.
1----. -·-··:..,,..,.;;. ______ . ____ ...,.... ___ -_ .. _5,a:lu .. ftP.--l-E DATA SUMARY 131
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
SED-4-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ..._5.._l __
Matrix: (soil/water) SOIL Lab Sample ID: _2 ... 9..._0 ... 8_l4..a-... __ _
Sample wt/vol: JO,o (g/mL) L_ Lab File ID: GH090814C20
Level: (low/med) _LO_w __
% Moisture: not dee. _..iO. dee.
Date Received: 09/29/89
Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/06/89
Dilution Factor: l,00
CONCENTRATION UNITS:
GPC Cleanup: (Y/N) li..,_, pH: 7,8
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 550 u
lll-44-4--------bis(2-Chloroethyl)Ether 550 u
95-57-8---------2-Chlorophenol 550 u
541-73-1--------1,3-Dichlorobenzene 550 u
106-46-7--------1 4-Dichlorobenzene . , 550 u
100-51-6--------Benzyl Alcohol 550 u
95-50-1---------1,2-Dichlorobenzene 550 u
95-48-7---------2-Methylphenol 550 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 550 u
106-44-5-------~4-Methylphenol 5'50 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 550 u
67-72-1---------Hexachloroethane 550 u
98-95-3---------Nitrobenzene 550 u
78-59-1---------Isophorone 550 u
88-75-5---------2-Nitrophenol 550 u
105-67-9--------2,4-Dimethylphenol 550 u
65-85-0---------Benzoic Acid . 150 J
lll-9l-l--------bis(2-Chloroethoxy)Methane-550. u
120-83-2--------2,4-Dichlorophenol 550 u
120-s2-1--------l,2,4-Trichlorobenzene 550 u
91-20-3---------Naphthalene 550 u
106-47-8--------4-Chloroaniline 550 u
87-68-3---------Hexachlorobutadiene 550 u
59-50-7---------4-Chloro-3-Methylphenol 550 u
91-57-6---------2-Methylnaphthalene 550 u
77-47-4---------Hexachlorocyclopentadiene_ 550 u
88-06-2---------2,4,6-Trichlorophenol 550 u
95-95-4---------2,4,5-Trichlorophenol 2700 u
91-58-7-~-------2-Chloronaphthalene 550 u
88-74-4---------2-Nitroaniline 2700 u
131-11-3--------Dimethyl Phthalate 550 u
208-96-8--------Acenaphthylene 550 u
606-20-2--------2,6-Dinitrotoluene 550 u
\ FORM I sv-1 · 1/87 Rev.
I.----
-·--====
--:rirrni, -

.

=· -SRBPCE DRTR SwtNRRY 130
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS SED-4-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .-5-..l __
Matrix: (soil/water) SOIL Lab Sample ID: ... 2,&.9_,._0 ..... 8_14...__ __ _
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH090814C20
Level: (low/med) LOW Date Received: 09/29/89
% Moisture: not dee. _.iQ dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc)
(Y/N) li..._
~
7.8
Date Analyzed: 10/06/89
GPC Cleanup: pH: Dilution Factor: _l~.o_o ___ _
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2700
83-32-9---------Acenaphthene 550
51-28-5---------2,4-Dinitrophenol 2700
100-02-1--------4-Nitrophenol 2700
132-64-9--------Dibenzofuran 550
121-14-2--------2,4-Dinitrotoluene 550
84-66-2---------Diethylphthalate 550
7005-72-3-------4-Chlorophenyl-phenylether_·_ 550
86-73-7---------Fluorene 550
100-01-6--------4-Nitroaniline 2700
534-52-l--------4,6-Dinitro~2-Methylphenol_ . 2700
86-30-6---------N-Nitrosodiphenylamine (1)_ 550·
101-55-3--------4-Bromophenyl-phenylether_ 550
118-74-1--------Hexachlorobenzene 550
87-86-5---------Pentachlorophenol 2700
85-01-s---------Phenanthrene 550
120-12-1--------Anthracene 550
84-74~2---------oi-n-Butylphthalate 550
206-44-0--------Fluoranthene 550
129-oo-o--------Pyrene 550
85-68-7---------Butylbenzylphthalate 550
91-94-1---------3,3'-Dichlorobenzidine 1100
56-55-3---------Benzo(a)Anthracene 550
218-01-9--------chrysene 550
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 550
111-a4-o--------oi-n-octyl Phthalate 550
205-99-2--------Benzo(b)Fluoranthene 550
207-08-9--------Benzo(k)Fluoranthene 550
50-32-8---------Benzo(a)Pyrene 240
193-39-5-------~Indeno(l,2,3-cd)Pyrene 550
53-70-3---------Dibenzo(a,h)Anthracene 550
191-24-2---0 ----Benzo(g,h,i)Perylene 550
· (1) -Cannot be separated from Diphenylamine
FORM I sv-2
-----~=---"'."'."~==---=----~s~g,.,..--.:p'1crE~ DR TR SUlflfRRV_
Q
u u u u u u u u u u u u u u u u
u u u
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u
u u u
J
u
u
u
1/87 Rev.
.. 129
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-
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
.Lab Name: COMPUCHEM LABS contract: (2-88)-REYS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. __..!2 dee. Date Extracted:
EPA SAMPLE NO.
SED-4-1
No.:. 51
290814
GH090814C20
09/29/89
10/04/89
Extraction:
GPC Cleanup:
'(SepFtCont/Sonc)
(Y/N) tf_ pH: 7,8
Date Analyzed: 10/06/89
Dilution Factor: -1~,o~oL-_
Number TICS found: .....2J.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.
===============~ ======-===================== ======== =--==--------
1. BLANK CONTAMINANT 4.52 440
2. BLANK CONTAMINANT 4.63 330
3. UNKNOWN 5.43 3500
4. A1LDOL 5.68 2000
5. ALDOL 6.22 1700
6. UNKNOWN 6.83 1100
7. UNKNOWN 6.90 1200
8. UNKNOWN 7.00 1600
9. UNKNOWN 10.95 220
10. 483-77-2 N_APHTHALENE, 1, 2, 3, 4-T_ETRAHY 11.62 1700
11. 483-78-3 NAPHTHALENE, l,6-DIMETHYL-4-12.85 890
12. UNKNOWN 17.65 280
13. UNKNOWN 17.90 330
14. UNKNOWN 18.85 610
15. UNKNOWN 18.92 1400
16. l)EHTACOSANE ISOMER 19.79 940
17. PEHTACOSANE ISOMER 20.85 720
18. UNlCNOWN 21.34 390
19. UNKNOWN 22.65 560
20. UNKNOWN 23.20 1400
21. UNKNOWN 23.34 1300
22. UNKNOWN 23.45 440
23. UNKNOWN 23.55 830
24. UNKNOWN 23.77 560
\ FORM I SV-TIC
Q
=====
BJ
BJ
J
AJ
AJ
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1/87 Rev.
----------------r ..... --.... ----------5-A.,....ft ... PLC DR TA SUMAR'f ---128
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-5-1
Lab Name: COMPUCHEM LABS Contract: l2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS
Matrix: (soil/water) SOIL
· Sample wt/vol: 30,0 (g/mL) L_
( low/med) LQW
% Moisture:-not dee. _ll dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lf.._ pH: 7,8
No.: SDG No.: ,c.51..__
Lab Sample ID: .... 2.,._9..._0x.8a;l6-._ __ _
Lab File ID: GH0908l6C20
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: -1~,o_oL-_
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 430 u
lll-44-4--------bis(2-Chloroethyl)Ether 430 u
95-57-8---------2-Chlorophenol 430 u
541-73-1--------l,3-Dichlorobenzene .430 U·
106-46-7--------1,4-Dichlorobenzene 430 u
100-51-6-------~aenzyl Alcohol 430 u
95-50-1---------1 2-Dichlorobenzene 430 u , .
95-48-7---------2-Methylphenol 430 u
39638-32-9~-----bis(2-Chloroisopropyl)Ether_ 430 u
106-44-5--------4-Methylphenol 430 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 430 u
67-72-1---------Hexachloroethane 430 u
98-95-3---------Nitrobenzene 430 u
78-59-1---------Isophorone 430 u
88-75-5---------2-Nitrophenol 430 u
105-67-9--~-----2,4-Dimethylphenol . 430 u
65-85-o------~--Benzoi~ Acid 2100 u
lll-91-l--------bis(2-Chloroethoxy)Methane,_ 430 u
120-83-2--------2,4-Dichlorophenol 430 u
120-e2-1--------1,2,4-Trichlorobenzene 430 u
91-20-3---------Naphthalene 430 u
106-47-8--------4-Chloroaniline 430 u
87-68-3---------Hexachlorobutadiene 430 u
59-50-7---------4-Chloro-3-Methylphenol 430 u
91-57-6---------2-Methylnaphthalene 430 u·
77-47-4---------Hexachlorocyclopentadiene_ 430 u
88-06-2---------2,4,6-Trichlorophenol 430 u
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalene 430 u
88-74-4---------2-Nitroaniline 2100 u
131-11-3--------Dimethyl Phthalate 430 u
208-96-8--------Acenaphthylene 430 u
606-20-2--------2,6-Dinitrotoluene 430 u
.. \ FORM I sv-1 1/87 Rev.
1--------=-,----= .... --.......... -----=------------SJUIPL~ DRTir-SUIINARY 127
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: !2-88)-REVS SED-5-1
Lab Code: COMPU Case No.:
Matrix: (soil/water) SOIL
17902 SAS No.: SOG No.: .x.5.._1 __
Lab Sample IO: a2.L9~08x.l..:6~---
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH090816C20
Level: ( low/med) LQW
I Moisture: not dee. ----2,l
-Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) lL_
dee.
~ pH: 7,8
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: ·.1~,0~0~_
. \
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2100
83-32-9---------Acenaphthene 430
51-28-5---------2,4-Dinitrophenol 2100
100-02-1--------4-Nitrophenol 2100
132-64-9--------Dibenzofuran 430
121-14-2--------2,4-Dinitrotoluen• 430
84-66-2---~-----Diethylphthalate 430
7005-72-3-------4-Chlorophenyl-phenylether_ 430
86-73-7---------Fluorene 430
100-01-6--------4-Nitroaniline 2100
534-52-1--------4,6-Dinitro-2-Methylphenol~ 2100
86-30-6---------N-Nitrosodiphenylamine (l)_ 430
101-55-3--------4-Bromophenyl-phenylether __ 430
118-74-1-------~Hexachlorobenzene 430
87-86-5---------Pentachlorophenol 2100
ss-01-s---------Phenanthrene 430
120-12-1--------Anthracene 430
84-74-2.;;,--------oi-n-Butylphthalate 430
206-44-0--------Fluoranthene 430
129-oo-o--------Pyrene 430
85-68-7---------Butylbenzylphthalate 430
91-94-1---------3,3'-Dichlorobenzidine 860
56-55-3---------Benzo(a)Anthracene 430
218-01-9--------Chrysene 430
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 430
117-84-o--------oi-n-octyl Phthalate ---· 430
205-99-2--------Benzo(b)Fluoranthene --430
. 207-08-9.--------Benzo(k) Fluoranthene 430
50-32-8---------Benzo(a)Pyrene 430
193-39-5--------Indeno(l,2,3-cd)Pyrene 430
53-70-3---------Dibenzo(a,h)Anthracene 430
191-24-2--------Benzo(g,h,i)Perylene 430
(1) -Cannot be separated from Diphenylamine
FORM I sv-2
----5ANPC£ · DJITA SUNIDIRY
Q
u u u u u u u u
u u u u u u u u u u u u u u u u
u u u u u u u
u
1/87 Rev.
126
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS . Contract: C 2-88) -REVS
Lab Code: COMPQ Case No.: 17902 SAS No.: SOG
Matrix: ( soil/wa-ter) SOIL. Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID:
Level: '(low/med) LOW Date Received:
' Moisture: not dee. _ll dee. Date Extracted:
EPA SAMPLE NO.
SED-5-1
No.: 51
290816
GH090816C20
09/29/89
10/0~/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) L_ pH: 7,8
Date Analyzed: 10/06/89
Dilution Factor: -l~,0-0,.__
Number TICs found: ....1.Q
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGI.KG
RT EST. CONC.
=•============== ============~=============== ======== =============
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
\
---· -·· -· ·--~~-~~-
BLANK CONTAMINANT 4 •. 50 300
BLANK CONTAMINANT 4.62 260
UNKNOWN 4.90 170
UNKNOWN 5.43 2600
ALDOL 5.67 520
ALDOL 6.22 610
UNKNOWN 6.90 910
UNKNOWN 7.00 1400
UNKNOWN 9.00 220
UNKNOWN 13.77 170
FORM I SV-TIC
----~-....,.·=------S--A~N-.PL£ DR TA SUlfl'l.llRY ·
Q
=====
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: C2-88)-REVS
SED-6-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ...._5._1 __
Matrix: (soil/water) SOIL Lab Sample IO: .._2 ..._9 ..._O 8...,2L;O..__ __ _
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH090820C20
Level: ( low/med) LOW Date Received: 09/29/89
I Moisture: not dee.~ dee.
Extraction: . (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H.,_ pH: 7,7
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: .1 •• 0~0:a:.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
·-
108-95-2--------Phenol 450 u
lll-44-4--------bis(2-Chloroethyl)Ether 450 u
95-57-8---------2-Chlorophenol 450 u
541-73-1--------1,3-Dichlorobenzene 450 u.
106-46-7--~-----l,4-0ichlorobenzene 450 u
100-51-6--------Benzyl Alcohol 450 u
95-50-1---------1,2-oichlorobenzene 450 u
95-48-7---------2-Methylphenol 450 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 450 u
106-44-5--------4-Methylphenol 450 u
621-64~7--------N-Nitroso-Oi-n-Propylamine_. 450 u
67-72-1---------Hexachloroethane 450 u
98-95-3---------Nitrobenzene 450 u
78-59-1---------Isophorone 450 u
88-75-5---------2-Nitrophenol 450 u
105-67-9--------2,4-0imethylphenol 450 u
65-85-o---------Benzoic Acid 2200 u
lll-91-1--------bia(2-Chloroethoxy)Methane_ 450 u
120-83-2--------2,4-0ichlorophenol 450 u
120-s2-1--------1,2,4-Trichlorobenzene 450 u
91-20-3---------Naphthalene 450 u
106-47-8--------4-Chloroaniline 450 u
87-68-3---------Hexachlorobutadiene 450 u
59-50-7---------4-Chloro-3-Methyiphenol 450 u
91-57-6---------2-Methylnaphthalene 450 u
77-47~4---------Hexachlorocyclopentadiene_ 450 u
sa-06-2---------2,4,6-Trichlorophenol 450 u
95-95-4---------2,4,5-Trichlorophenol 2200 u
91-58-7---------2-Chloronaphthalene 450 u
88-74-4---------2-Nitroaniline 2200 u
131-11-3--------0imethyl Phthalate 450 u
208-96-8--------Acenaphthylene 450 u
606-20-2--------2,6-Dinitrotoluene 450 u
\ FORM I sv-1 1/87 Rev.
__; _______________ ..,.e.,.n-•n1::1-• -=.·t--~o Ta c-, •••oDo----f 24 --
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-6-1
Lab Name: COMPUCHEM LABS Contract: £2-88}-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab Sample ID: 290820
Sample wt/vol: 30,0 (g/mL) L-Lab File ID: ~H09o§,Qc,o
Level: ( low/med) LOW Date Received: Q9LZ9L89
% Moisture: not dee. __)J_ dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) l{__ pH: 7,7
Date Extracted: l.0/04/89
Date Analyzed: '10/06/89
Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Xg) UG/KG Q
99-09-2---------3-Nitroaniline 2200 u
83-32-9---------Acenaphthene 450 u
51-28-5---------2,4-Dinitrophenol 2200 u
100-02-1--------4-Nitrophenol 2200 u·
132-64-9--------0ibenzoturan 450 u
121-14-2-----~--2,4-Dinitrotoluene 450 U.
84-66-2---------Diethylphthalate 450 u
7005-72-3-------4-Chlorophenyl-phenylether_ 450 u
86-73-7---------Fluorene 450 u
100-01~6--------4-Nitroaniline 2200 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2200 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 450 u
101-55-3--------4-Bromophenyl-ph·enylether __ 450 u
118-74-1--------Hexachlorobenzene 450 u
87-86-5---------Pentachlorophenol 2200 u
85-01-8---------Phenanthrene 450 u
120-12-1--------Anthracene 450 u
84-74-2---------Di-n-Butylphthalate 450 u
206-44-0--------.Fluoranthene 450 u
129-00-0---~----Pyrene 450 u
85-68-7---~-----Butylbenzylphthalate 450 u
91-94-1---------3,3'-Dichlorobenzidine 900 u
56-55-3---------Benzo(a)Anthracene 450 u
218-01-9--------Chrysene 450 u
. ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 450 u
117-84-0--------Di-n-Octyl Phthalate 450 u
205-99-2--------Benzo(b)Fluoranthene 450 u
207-08-9--------Benzo(k)Fluoranthene 450 u
50-32-8---------Benzo(a)Pyrene 450 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 450 u
53-70-3---------Dibenzo(a,h)Anthracene 450 u
191-24-2--------Benzo(g,h,i)Perylene 450 u
(1) -Cannot be separated trom Diphenylam1ne
' FORM I sv-2 1/87 Rev.
........ -...... ......,, ......... .___..____,,------------S ... R .. 8-PLr DRTR SulfrtRR'I _ 123
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SED-6-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
.sample wt/vol: 30,0 (g/mL) ~
Level: ( low/med) LOW
I Moisture: not dee. _,ll dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup:• (Y/N) L_ pH: 7.7
SOG No. : _s_1 __
Lab Sample IO: ...,2_9..._08...,2 ... 0L.-__ _
Lab File ID: GH090820c20
Date.Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1~1 0_0 __
Number TICs found: _7
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q =•-==----------= =-=-----------=--------==--= --=-=-====-=========s=•• -====
l. BLANK CONTAMINANT 4.50 410 BJ
2. BLANK CONTAMINANT 4.62 320 BJ
3. UNKNOWN 5.45 1500 J
4. ALDOL 5.68 500 A,J
5. ALDOL 6.23 320 A,J
6. UNKNOWN 6.90 500 J
7. UNKNOWN 6.98 680 J
FORM I SV-TIC 1/87 Rev.
_, _____ ......... __________ 5_Q .... 8P~'.LC-DATTrSUNNl?IRY 122
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: l 2-88) -REVS SED-7-1
Lab Code: COMPO Case No.: 17902 · SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.Q (g/mL) ~
Level: ( low/med) LOW
I Moisture: not dee. --1.i dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N') li._ pH:
~
7,5
SDG No.: &.51-._
Lab Sample ID: .... 2 ..... 9~08......_19:a...-__ _
Lab File IO: GH090819C20
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1~,o~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol· 460 u
lll-44-4--------bis(2-Chloroethyl)Ether 460 u
95-57-8---------2-Chlorophenol 460 u
541-73-1--------1,3-Dichlorobenzene 460 u
106-46-7--------1,4-Dichlorobenzene 460 u
100-51-6--------Benzyl Alcohol 460 u
95-50-1---------1,2-oichlorobenzene 460 u
95-48-7---------2-Methylphenol 460 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 460 u
106-44-5--------4-Methylphenol 460 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 460 u
67-72-1---------Hexachloroethane 460 u
98-95-3---------Nitrobenzene 460 u
78-59-1---------Isophorone 460 u
88-75-5---------2-Nitrophenol 460 u
105-67-9--------2,4-Dimethylphenol 460 u
65-ss-o---------Benzoic Acid 2300 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 4.60 u
120-83-2--------2,4-Dichlorophenol 460 u
120-s2-1--------1,2,4-Trichlorobenzene 460 u
91-20-3---------Naphthalene 460 u
106-47-8--------4-Chloroaniline 460 u
87-68-3---------Hexachlorobutadiene 460 u
59-50-7---------4-Chloro-3-Methylphenol 460 u
91-57-6---------2-Methylnaphthalene 460 u
77-47-4---------Hexachlorocyclopentadiene_ 460 u
88-06-2---------2,4,6-Trichlorophenol 460 u
95-95-4---------2,4,5-Trichlorophenol 2300 u
91-58-7---------2-Chloronaphthalene 460 u
88-74-4---------2-Nitroaniline 2300 u
131-11-3-------~Dimethyl Phthalate 460 · u
208-96-8--------Acenaphthylene 460 u
606-20-2--------2,6-Dinitrotoluene 460 u
FORM I sv~1 1/87 Rev ..
------------=---=-----= ·==----_-_ ----:------s""'IAfll'Ulllp'BJTL£-P--·,,-11nrSUlfNRRY 121
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS SE0-7-l
Lab Code:. COMPU case No.: 17902 SAS No.: SOG No.: ... 5_1 __
Matrix: (soil/water) SOIL Lab Sample IO: 290819
Sample wt/vol: -30,0 (g/mL) ~ Lab File IO: GH090819C20
Level: ( low/med) LOW
I Moisture: not dee. ---2.2,
Extraction: (SepF/Cont/Sonc)
dee.
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
GPC Cleanup: (Y/N) li.._ pH: 7,5 Dilution Factor: _1~,o_o __ _
CONCENTRATION UNITS:
CAS NO. ·coMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline --, 2300 u ,,
83-32-9---------Acenaphthene 460 u
51-28-5---------2,4-Dinitrophenol 2300 u
100-02-7--------4-Nitrophenol 2300 u
132-64-9--------Dibenzofuran 460 u
121-14-2--------2,4-Dinitrotoluene 460 u
84-66-2---------0iethylphthalate 460 u
7005-72-3-------4-Chlorophenyl-phenylether_ 460 u
86-73-7---------Fluorene 460 u
100-01-6--------4-Nitroaniline 2300 u
534-52-1---.-----4, 6-Dinitro-2-Methylphenol_ 2300 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 460 u
101-55-3--~-----4~Bromophenyl-phenylether __ 460 u
118-74-1--------Hexachlorobenzene 460 u-
87-86-5---------Pentachlorophenol 2300 u
es-01-e---------Phenanthrene 460 , u
120-12-1--------Anthracene 460 u
84-74-2----------Di-n-Butylphthalate 460 u
206-44-0------~-Fluoranthene 460 u
129-00-0--------Pyrene 460 u
85-68-7---------Butylbenzylphthalate 460 u
91-94-1---------3,3'-Dichlorobenzidine 930 u
56-55-3---------Benzo(a)Anthracene 460 u
-218-01-9------~-Chrysene 460 u
117-81-7------~-bis(2-Ethylhexyl)Phthalate_ 460 u
117-84-0--------Di-n-Octyl Phthalate 460 u
205-99-2--------Benzo(b)Fluoranthene 460 u
207-08-9--------Benzo(k)Fluoranthene 460 u
50-32-8---------Benzo(a)Pyrene 460 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 460 u
53-70-3-~-------Dibenzo(a,h)Anthracene 460 u
191-24-2--------Benzo(g,h,i)Perylene 460 u
(l) -Cannot be separated from Diphenylamine
\
FORM I sv-2 l/87 Rev.
I ___ _
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-R£YS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. --2..i dee. Date Extracted:
EPA SAMPLE NO.
SED-7-1
No.: 51
290819
GH0908l9C20
09/29/89
l0/0i/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lL_ pH: 7,5
Date Analyzed: 10/06/89
Dilution Factor: _1_,o_o __
Number TICs found:___.§.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
--===--=-----=--=, -=---------------------==-:::::s======-= =============
1. BLANK CONTAMINANT 4.52 230
2. UNKNOWN 5.45 1200
3. ALOOL 5.68 610
4. ALOOL 6.23 380
5. UNKNOWN 6.90 380
6. UNKNOWN 6.98 660
FORM I SV-TIC
-----.... -.. -.. -·------------==------______ 5_.AIIPLE DRTA. S.OMARY
Q
=====
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET . EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-1-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : _S_l __
Matrix: (soil/water) SOIL I.ab Sample ID: 290826
Sample wt/vol: 30.0 (g/mL) ~ I.ab File ID: !:iH09082§C2Q
Level: ( low/med) LOW rDate Received: Q2L22LB2
I Moisture: not dee. __u dee~ Date Extracted: lOLQ4L82
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: lQLO§L89
GPC Cleanup: (Y/N) IL... pH: 7.9 Dilution Factor: L 00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGLJSG
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlotophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 U.
106-46-7----~---l,4-Dichlorobenzene 370 u
100-s1-6--·------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3--------~Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-0---------Benzoic Acid 1800 u
lll-91-l--------bia(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-82-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,S-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
\
FORM I sv-1
== SAliPLE DATA SOMRRY ....
Q
1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM. LABS Contract: (2-88}-REVS
SL-1-1
Lab Code: COMPU case No.: 17902 SAS No.: SDG No. : ..._5_1 __
Matrix: (soil/water) SOIL Lab Sample ID:, .2"""9.x.Ox.,;82111,;6:,t__ __ _
Sample wt/vol: 30,0 (g/mL) L_
LOW
Lab File IO: GH090826C20
Level: (_low/med)
% Moisture: not dee. -..J.2. dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) fi_ pH: 7,9
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1~,9-0,.___
\
CAS NO. COMPOUND
CONCENTRATION UNITS: ··
(ug/L or ug/Kg) UG/XG
99-09-2---------3-Mitroaniline 1800
83-32-9---------Acenaphthene 0 370
51-28-5------~--2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------0ibenzofuran 370
121-14-2--------2,4-0initrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether_ 370
86-73-7----~----Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthren• 370
120-12-1--------Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-0o-o_--------Pyrene 370
85-68-7------~--Butylbenzylphthalate 370
91-94-1---------3,3'-Dichlorobenzidine 75_0
56-55-3---------Benzo(a)Anthracene 370
218-01-9~-------Chrysene 370
ll7-81-7--------bia(2-Ethylhexyl)Phthalate_ 370
117-84-0--------oi-n-o~tyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthen• 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyren• 370
53-70-3---------Oibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 370
. (l) -Cannot be separated from D1phenylam1ne
Q
u u u u u
u
u u
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u u u u u
u
u u
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u u
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1----
FORM I sv-2 1/87 Rev.
-----_....._""""""""........,..........., _______ ::.s.A.ftPLE DRTlr SUNMR·Y 117
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample IO:
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID:
Level: (low/med) I.OW Date Received:
% Moisture: not dee. _ll dee. Date Extracted:
EPA SAMPLE NO.
SL-1-1
No.: 51
290826
GH090826C20
09/29/89
10/0~/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL_ pH: 7,9
Date Analyzed: 10/06/89
Dilution Factor: -1~,0=0~-
Number TICS found: __l.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC~ Q
1. BLANK CONTAMINANT 4. 50 2 3 0 BJ
FORM I SV-TIC 1/87 Rev.
\
1-----
--------------------------·-SRN.e.LE-DRTR SDNRARY 116
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA S~PLE. NO~
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS SL-2-1
Lab Code: COMPO Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30,0 (g/mL) L-
Level: ( low/med) LOW
I Moisture: not dee. _.l.Q dee.
Extraction: (Sep~/Cont/Sonc) ~
GPC Cleanup: (Y/N) L· pH: 7,9
SOG No.: .z..5.._1 __
Lab Sample IO: ...,249~08~21L;J'----
Lab File IO: GH09Q82JC20
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: -l~,0~0----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 3'70 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370 u
67-72-1---------Hexachloroethane 370 u
9-8-95-3-----.----Nitrobenzene . 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-o---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83_.2--------2,4-Dichlorophenol 370 u
120-a2-1--~-----1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u·
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95~4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------oimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
'
FORM I sv-1 1/87 Rev.
11 S
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: £2-88)-REVS SL-2-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ....,5._l __
Matrix: (soil/water) SOIL Lab Sample ID: ..,2.,._9.&.0..._8._2,._3 __ _
·Sample wt/vol: 30,0 (g/mL) G.__ Lab File ID: GH09082JC20
Level: (low/med) LOW Date Received: 09/29/89
% Moisture: not dee. _.l.Q.
Extraction: (SepF/Cont/Sonc)
dee. Date Extracted: 10/04/89
Date Analyzed: 10/06/89
GPC Cleanup: (Y/N) lL_ pH: 7,9 Dilution Factor: 1,00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u·
121-14-2--•-----2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-.3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7-------,-Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 370 ·u
101-55-3--------4-Bromophenyl~phenylether_ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
es-01-e---------Phenanthrene 370 u
120-12-1--------Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 u
129-oo-o--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1-----~---3,3'-Dichlorobenzidine 730 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chryaene 370 u
111-a1-1--------bia(2-Ethylhexyl)Phthalate_ 530
111-e4-o--------01-n-octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8------~--Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53~70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -Cannot be separated from Diphenylamine
' FORM I sv-2 1/87 Rev.
-----.. ---~--=-~-.-_---.5~gm9mp~cr-a:E~DATA SIJIDilARV I 14 ·-
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENT~TIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2~88)-REVS
Lab _Code: COMPU Case No.: 17902 SAS No.: SOG
EPA SAMPLE NO.
SL-2-1
No.: 51 I Matrix: (soil/water) SOIL Lab Sample ID: 290823
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Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: ~H09Q823C20
Level: ( low/med) I,DW Date Received: 09/29/89
I Moisture: not dee. --1.Q dee. Date Extracted: 10/0~/89
Extraction: Date Analyzed: 10/06/89
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ll_ pH: 7,9 Dilution Factor: _1~,o~o..__
Number TICS found:__.!
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q --===---=-------============================
l. -BI:.ANK CONTAMINANT
2. ALDOL .
3. UNKNOWN
4. UNKNOWN
--======
4.50
5.68
-13. 77
20.90
FORM I SV-TIC
'
=-==------=--=====
190 BJ
330 A,J
300 J
300 J
1/87 Rev.
---------------------~-----------S~A-N..-P--LE DATA SUIVIRRY._ 113
,_
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-~S
SL-2-2
Lab Code: COMPU Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30,0 (g/mL) ~
Level: (low/med) _r.o_w ___ _
I Moisture: not dee. _,ll dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H__ pH: 7,9
SDG No. : ... 5_1 __
Lab Sample IO: 29.0829 _ ......... ___ _
Lab File IO: GH090829C20
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1~,o~oL.-_
CONCENTRATION UNITS: -
CAS,NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8-~-------2-Chlorophenol ·370 u
541-73-1--------1,3-0ichlorobenzene 370 u.
106-46-7--------1,4-0ichlorobenzene 370 u
100-s1-6-.-------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44~5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370 u
67-72-1---------Hexa~hloroethane 370 u
98-95-3--~------Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-7S-s---------2~Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-o---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-82-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
· 59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalen• 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2----~----2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------oimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
' FORM I sv-1 1/87 Rev.
--------------s~R~8Pan·'Tt~E~-oRnrsul'll'UlRY 112
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-2-2
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: _5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: .. 2 .... 9.,._Q..._8._29..__ __ _
s·ample wt/vol: 30,0 (g/mL) L-Lab File ID: GH090829C2Q
Level: (low/med) _LO_w ___ _
I Moisture: not dee. _ll
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) If._
dee.
pH: 7,9
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: 1,00
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/RG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether_ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1-_.------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 370
101-55-3--------4-Bromophenyl-phenylether_ 370
118-74-1~-------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
es-01-e---------Phenanthrene :po
120-12-1----~---Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-00-0--------Pyrene 370
85-68-7------~--Butylbenzylphthalate 370
91-94-1---------3,3'-0ichlorobenzidine 740
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 370
111-a1-1--------bia(2-Ethylhexyl)Phthalate_ 79
117-84-o--------oi-n-octyl Phthalat•. 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------0ibenzo(a,h)Anthracene I 370
191-24-2--------Benzo(g,h,i)Perylene 370
(1) -Ca~ot be separated from Oiphenylamine
FORM I sv-2
--~--·--------------------------5-R-IJ.-PLE · Df.1TH SDMRRY
Q
u
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u·
u u
u
u u
u
u
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u u u u
u
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u u
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J u
u u u
u u u
1/87 Rev.
1 1 1
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-2-2
Lab Code: COMPO case No.: 17902 SAS No~: SDG No.: __ 5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: 290829
sample wt/vol: 30,0 (g/mL) L-Lab File IO: GH090829C20
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. --11 dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/06/89
GPC Cleanup: (Y/N) IL_ pH: 7,9 Dilution Factor: 1,00
CONCENTRATION UNITS:
Number TICs found: _l (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
1.. BLANK CONTAMINANT
2. BLANK CONTAMINANT
3. UNKNOWN
FORM I SV-TIC
'
4.50
4.60
22.80
220 BJ
190 BJ
710 J
1/87 Rev.
---~--""""'"'c:2™"'"'-.-.= ..... -.--'":."""'·· ~_ ........ -"'='"------,.§'.!""'DJIPIPI. ~l!"IITLE--r"_ ,_Ar-.T_A ___ : ~s-.u---N ... ,. .. _ 9-_ .... ,.:,.:vr.11. ,-----110
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS Contract: (2-88)-REVS SL-3-1
Lab Code: COMPU Case No.: 17902 SAS No.: ___ SDG No.: ....,5._1 __
Matrix: (soil/water) SOIL Lab Sample ID: .2..._9.,._0x.84;;1,.;9c,__ __ _
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:· GH090849B20
Level: (low/med) LOW
% Moisture: not dee. __ll
Extraction:
GPC Cleanup_:
(SepF/Cont/Sonc)
(Y/N) L_
dee.
7 I 8 ·
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: -1~,0~0"-_
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/KG
108-95-2--------Phenol 380
lll-44-4--------bia(2-Chloroethyl)Ether 380
95-57-8---------2-Chlorophenol 380
541-73-1--------1,3-Dichlorobenzene 380
106-46-7--------1,4-Dichlorobenzene 380
100-51-6--~-----Benzyl Alcohol 380
95-50-1---------1,2-Dichlorobenzene 380
95-48-7---------2-Methylphenol 380
39638-32-9------b·is ( 2-Chloroisopropyl) Ether_ 380
106-44-5--------4-Methylphenol 380
621-64-7--------N-Nitroso-Di-n-Propylamine_ 380
67-72-1---------Hexachloroethane 380
98-95-3---------Nitrobenzene 380
78-59-1---------Isophorone 380
88-75-s---------2~Nitrophenol 380
105-67-9--------2,4-Dimethylphenol 380
65-85-o---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane~ 380
120-83-2--------2,4-Dichlorophenol 380
120-82-1--------l,2,4-Trichlorobenzene 380
91-20-3---------Naphthalene 380
106-47-8--------4-Chloroaniline 380
87-68-3---------Hexachlorobutadiene 380
59-50-7---------4-Chloro-3-Methylphenol 380
91-57-6---------2-Methylnaphthalene 380
77-47-4---------Hexachlorocyclopentadiene_ 380
88-06-2---------2,4,6-Trichlorophenol 380
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 380
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate . 380
208-96•8---~----Acenaphthylene 380
606-20-2--------2,6-Dinitrotoluene 380
FORM· I sv-1
----.. -.-----==------~--~~~.r57u09~psLr-rE~DRTR SDNIIRRY
Q
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u u
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u u
u u
u u u
u
u
u
u u
u
u
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u
u u
u
u u
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u u u
u
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1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: c2~aa)-REVS SL-3-1
Lab Code: CQKftl Case No.: 17902 SAS No.: SOG No.: ..._5 .. 1 __
Matrix: (soil/water) SOIL Lab Sample ID: .2...,9.,._0....,8c...49:ic....._ __ _
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH090849B20
Level: (low/med) LOW Date Received: 09/29/89
I Moisture: not dee. _u dee. Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1~,o~oL-_
--·
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ~ pH: 7,8
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 380 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 U.
132-64-9--------Dibenzofuran 380 u
121-14-2--------2,4-Dinitrotoluene 380 u
84-66-2---------Diethylphthalate 380 u
7005-72-3-------4-Chlorophenyl-phenylether_ 380 u
8~-73-7---------Fluorene ·380 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,'6-Dinitro-2-Methylphenol_ 1800 u
86-30-6------~--N-Nitrosodiphenylamine (1)_ 380 u
101-55-3--------4-Bromophenyl-phenylether_ 380 u
118-74-1--------Hexachlorobenzene 380 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 380 u
120-12-1--------Anthracene 380 u
84-74-2---------oi-n-Butylphthalate 380 u
206-44-o--------Fluoranthene 380 u
129-oo-o--------Pyrene 380 u
85-68-7---------Butylbenzylphthalate 380 u
91-94-1---------3,3'-Dichlorobenzidine 760 u
56-,55-3---------Benzo (a) Anthracene 380 u
218'-01-9--------Chrysene 380 u
117-81-7-~------bis(2-Ethylhexyl)Phthalate_ 620
117-84-o--------Di-n-octyl Phthalate 3~0 u
205-99-2--------Benzo(b)Fluoranthene 380 u
207-08-9--------Benzo(k)Fluoranthene 380 u
50-32-8---------Benzo(a)Pyrene 380 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 380 u
53-70-3---------0ibenzo(a,h)Anthracene 380 u
191-24-2--------Benzo(g,h,i)Perylen• 380 u
(1) -Cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
-----------...... --.... ----·--.... -_....__ _____ ........, ___ 5_g_9_pL£ DRTR SUNNRRY -· 108
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-3-1 Lab Name: · COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ..._51 __
Matrix: (soil/water) SOIL Lab Sample ID: ...,2...,9 0.,._8,.,.4.a...9.,__ __ _
sample wt/vol: 30,0 (g/mL) L-Lab Pile ID: GH090849B20
Level: (low/med) _LO_w __
I Moisture: not dee. _ll
Extraction:
GPC Cleanup:
( SepF / Cont/ Sonc)
(Y/N) li_
Number TICS found: --1
dee.
pH:
CAS NUMBER COMPOUND
7,8
NAME
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: _1_,o_o...__
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/XG
RT EST. CONC. Q
••==•==========a •--=-----=--===---------=z-= --======---=========== -====
l. BLANX CONTAMINANT 4.32 310 BJ
2. BLANX CONTAMINANT 4.42 190 BJ
3. ALDOL 5.47 570 A,]
FORM I SV-TIC 1/87 Rev.
\
1-----
--=-·==--===------------S-A ... · ..-8eJ ... £ DR TR SUM~R'? . 107
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SEMIVOIATILE ORGANICS ANALYSIS DATA SHEEr EPA SAMPLE NO.
SL-4-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: ..._5._1 __
Matrix: (soil/water) SOIL · Lab Sample ID: 290831
Sample wt/vol: 30,0 (g/mL) L._ Lab File IO: GH090831C20
Level: (low/med) _to_w __ _ Date Received: 09/29/89
% Moisture: not' dee. _lJ. dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10/0§/89
GPC Cleanup: (Y/N) H.,_ pH: 7.9 Dilution Factor: _1~,-00 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
.95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3---------Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-o---------Benzoic Acid 1800 u
lll-91-l--------bia(2-Chloroethoxy)Methane_ 370 u
120-83-2~-------2,4-0ichlorophenol 370 u
120-s2-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 37Q u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2---------2,4,6~Trichlorophenol 370 u
95-95~4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
' FORM I sv-1 1/87 Rev.
-. .. . . . ~
---------------.s-Q--N~P~L~E--DATA SUMARY 106
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS SL-4-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ..._5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: _2.._9..._0._8...._31 ___ _
Sample wt/vol: 30,0 (g/mL) G.._ Lab File ID: GH09083lC20
Level: (low/med) LOW
I Moisture: not dee. _u 'dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lf_ pH: 7.9
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/06/89
Dilution Factor: 1,00
CONCENTRATION UNITS: ..
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2-~-------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370 u
51-28~5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u
121-14-2-----~--2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52~1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 370 u
101-55-3--------4-Bromophenyl-phenylether_ 370 u
118-74-1--~-----Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-e---------Phenanthrene 370 u
120-12-1---~----Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 u
129-00-0--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 740 u
56-55-3---------Benzo(a)Anthracene 150 Jx
218-01-9--------Chrysene 150 Jx
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 240 J
117-84-0---~----Di-n-Octyl Phthalate . 370 u
205-99~2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 .U
(1) -Cannot be_ separated from Diphenylamine
\ :: FORM I sv-2 1/87 Rev.
105
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 -SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID:
Level: ( low/med) LOW Date Received:
I Moisture: not dee. --11 dee. Date Extracted:
EPA SAMPLE NO •.
SL-4-1
No.: 51
290831
GHQ90831C2Q
Q9L29L89
lOLQ~L89
Extraction: (SepF,/Cont/Sonc) ~
GPC Cleanup: (Y/N.) lL_ pH: 7.9
Date Analyzed: lOL06L89
Dilution Factor: _1_,Q~Q,.___
Number TICS found: .-2.i
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGLKG
RT EST. CONC.
••=••===•==a==•• •=m•=•====•===•=a====•==••=~ -=--=a •==s====-•=-===
l. ALOOL 5.65 3600
2. ALOOL 6.20 2400
3. UNKNOWN 6.75 1300
4. UNKNOWN 10.37 750
s. UNKNOWN 11.14 1300
6. UNKNOWN 11.22 1200
7. UNKNOWN 11.84 1300
8. UNKNOWN 11.94 860
9. UNKNOWN 12.74 2400
10. UNKNOWN 12.90 1100
11. UNKNOWN 13.20 2200
12. UNKNOWN 13.32 1100
13. UNKNOWN 13.62 1600
14. UNKNOWN 13.80 1400
15. UNKNOWN 13.97 2500
16. UNlQfOWN 14.24 1900
17. UNlQfOWN 14.44 1500
18. UNlQfOWN 14.59 1800
19. UNlQfOWN 14.77 2000
20. ONICNOWN 15.22 1500
21. UNlQfOWN 15.57 1000
22. UNlCNOWN 16.60 1300
FORM I SV-TIC
-_= __ ----.=-.,=_ =-~=~-=--==_ -==~----,-:-~_-_-_ ~s~A"l'lft~PL.n, 1 Ec---noA TA -sUMARY
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•====
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-!84 --
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS
SL-5-1
Lab code: COMPU Case No.: 17902 SAS No.: SOG No. : ..._5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: 290845
Sample wt/vol: 30,0 (g/mL) G__ Lab File ID: GJ090845A20
Level: (low/med) LOW Date Receiyed: 09/29/89
% Moisture: not dee. ___li, dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/07/89
GPC Cleanup: (Y/N) R._. pH: 7,5 Dilution Factor: 1,00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or uq/Xg) UG/KG
108-95-2--------Phenol 370 u
111-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7----~---l,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-so-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7------.--N-Nitroso-Di-n-Propyla:mine_ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3---------Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Di:methylphenol 370 u
65-as-o---------Benzoic Acid 1800 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2~-------2,4-Dichlorophenol 370 u
120-a2-1--------t,2,4-Trichlorobenzene 370 u
91-20-3-~-------Naphthalene 370 U·
106-47-8--------4-Chloroaniline 370 .u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene~ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Di:methyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
FORM I sv-1
'
•, .. ,.· SARP£:£ DR TA· SOltftARY _
Q
1/87 Rev.
103'
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-5-1
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: 51
Matrix: ( soil/water) SOIL Lab Sample ID: 290845
Sample wt/vol: 30.0 (g/mL) L-Lab File ID: GJ090845A20
Level: (low/med) LOW Date R~ceived: 09/29/89
' Moisture: not dee. ___,ll dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) .~ Date Analyzed: 10/07/89
Dilution Factor: _1_,o_o __
CONCENTRATION UNITS:
GPC Cleanup: ('i/N) l:L,_ pH: 7,5
CAS NO. COMPOUND (ug/L or ug/Kg) UG/RG .Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370. u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
700S-72-3-------4~Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 370 u
101-55-3-~------4-Bromophenyl-phenylether_ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---~-----Phenanthren• 230 J
120-12-1--------Anthracene 67 J
84-74-2--~------Di-n-Butylphthalate 370 u
206-44-o--------Fluoranthen• 260 J
129-00-0--------Pyr•n• 230 J
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 750 u
56-55~3---------Benzo(a)Anthracene 140 J
218-01-9--------Chrysene 160 J
117-il-7------~-bi ■(2-Ethylhexyl)Phthalate_ 170 J
111-14-0--------oi-n-OCtyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 170 JX
207-08-9--------Benzo(k)Fluoranthene 170 . JX
50-32-8----~----Benzo(a)Pyrene 120 J
193-39-5--------Indeno(l,2,3-cd)Pyr•n• 73 J
53-70-3---------Dibenzo(a,h)Anthracene 49 J
191-24-2---~----Benzo(g,h,i)Perylen• 75 J
(1) -CaMot be separated from Diphenylamin•
~
\ FORM I sv-2 1/87 Rev.
-~--3lfflPLE DRTR SUlflfRRY 102
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
-Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample IO:
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID:
Level: (low/med) I.OW Date Received:
I Moisture: not dee. ~ dee. Date Extracted:
EPA SAMPLE NO.
SL-5-1
No.: 51
290845
GJQ9Q845A20
09/29/89
lQLQ4L89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL. pH: 7,5
Date Analyzed: 10L07L89
Dilution Factor: -1~,0~0,.___
Number TICS found:~
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
s=~=,=---------= ==-=-=--------------====~-~--== =-= •===========
l. UNKNOWN HYDROCARBON 4.20 260
2. UNKNOWN HYDROCARBON 4.30 190
3. ALDOL 5.35 2300
4. ALDOL 5.88 450
5. U'NRNOWN 6.43 190
FORM I SV-TIC
\
~.........._ _____________ =sJll!IPLE DATFr SUNPISRY
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1/87 Rev.
101
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SEMIVOLATILE ORGAN.ICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-6-1
Lab Name: COMPUCHEM LABS Contract: C2-88)-REVS
.Lab Code: CQMPU Case No.: 17902 SAS:·No.: SDG No.: _5_1 __
Matrix: (soil/water) SOIL Lab Sample ID: 290139
Sample wt/vol: 'Lab File ID: ~HQ9lQ39c,o
(low/med) _LO_w ____ _ Date Received: 09/30/89
% Moisture: not dee. __u dee. Date Extracted: lO/Qi/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: lQ/07/89
GPC Cleanup: (Y/N) L., pH: 8.0 Dilution Factor: 1.00
CAS NO. COMPOUND
.CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1-----~--l,3-Dichlorobenzene 370
10~-46-7--------1,4-Dichlorobenzene 370
100-51-6-~------Benzyl Alcohol 370
95-50-1---------1,2-Di~hlorobenzene 370
9 5-4 9·-1---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5-----~---2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol . 370
65-85-o---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane_. 370
120-83-2--------2,4-Dichlorophenol 370
120-82-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadien• 370
59-50-7---------4-Chloro-3-Methylphenol 370
91~57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
FORM I sv-1
u
u u u.
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U.
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u u u
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u u
u u u
u u u u
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1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-6-1
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
SAS No.: SDG No.: -5.-1 __
Lab Sample ID: · .,2..._9.,.,_01_3,._.9~---
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: GH091039C20
Level: (low/med) LOW Date Received: 09/30/89
, Moisture: not dee. _u dee. Date Extracted: 10/0~/89
Extraction: (SepF /Cont/Sonc) ~ Date Analyzed: 10!07/89
GPC Cleanup: (Y/N) lL.. pH: a,o Dilution Factor: l. oo
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !,l~!g~ Q
99-09-2---------3-Nitroaniline 1800 u
83~32-9---------Acenaphthene 370 u
Sl-28-s---------2,4-Dinitrophenol 1800 u
100-02-1-~------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u
121-14-2--~-----2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6--------~N-Nitrosodiphenylamine (1)_ 370 u
101-55-3--------4-Bromophenyl-phenylether_ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
ss-01-s-----~---Phenanthrene 370 u
120-12-1--------Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u·
206-44-0--------Fluoranthene 370 u
129-00-0--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 740 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chrysene 370 u
ll7-81-7---~----bia(2-Ethylhexyl)Phthalate_ 140 J
117-84-0--------Di-n-Octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene · 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
•
(1) -CaMot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
:_a.....· -SM?I E lUlTR S088ARV . -99 -
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS •
EPA SAMPLE NO.
SL-6-1
Lab Code: COMPO case No.: 17902 SAS No.: SOG No.: ...,5_1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30,0 {g/mL) G.,__;
Level: {low/med) LOW
I Moisture: not dee. _ll · dee.
Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) L......
Number TICs found: ----1.
pH:
~
8.0
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGLKG
290139
GH091039C20
09L3QL89
1QL04L89
10,01,ag
1.00
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
l. BLANK CONTAMINANT 4.32 260 BJ
2. BLANK CONTAMINANT 4. 42 220 BJ
FORM I SV-TIC 1/87 Rev.
\
· -···· SPSPCE DRIR-·SlHQIARV 7
,-_
9g· --
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SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88}-REV§ -SL-7-1
Lab Code: COMPU Case No.: 17902 SAS No.: ____ SDG No.: ..._5.._l __
Matrix: (soil/water) SOIL Lab Sample ID: _2.c..9.-.10...,4,i.;O,.__ __ _
Sample wt/vol: 30,0 (g/mL) L__ Lab File to: GH091040A20
Level: ( low/med) LOW Date Received: 09/30/89
% Moisture: not dee. ---1Q. dee. Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: _1_,o~o...__
· Extr·action: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) l:L,_ pH: 7,7
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8-----~---2-Chlorophenol 370
541-73~1--------1,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50-1---------1,2-oichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370,
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-o---------aen·zoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane_;_ 370
120-83-2--------2,4-Dichlorophenol_ 370
120-s2-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene_ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
\
FORM I sv-1
Q
u u
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1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-7-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : _5_1 __
Matrix: (soil/water) SOIL Lab Sample IO: _2~9_1~04~0..._ __ _
Sample wt/vol: 30,0 (g/mL) L-Lab File IO: GH091040A20
Level: (low/med) -.LO.._W __ _
% Moisture: not dee. ---12 dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lf_ pH: 7,7
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Rg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-0initrophenol 1800
100-02-1--------4-Nitrophen~l 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3------~4-Chlorophenyl-phenylether_ 370
86-73-7---------Fluorene 370
l00-0l-6~-------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 370
101-55-3--------4-Bromophenyl-phenylether_ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
es-01-e---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------Di-n-Butylphthalate 370
206-44-o--------Fluoranthene 370
129-oo-o--------Pyrene 370
85-68-7-------~-Butylbenzylphthalate 370
91-94-1-~-------J,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chryaene 370
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 370
117-84-o--------oi-n-octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylen• 370
0 (l) -Cannot be separated from Diphenylamine
FORM I sv-2
Q
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u u
U·
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u u u u
u
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u u u u u u u u u
u
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u u u u
1ia1 Rev.
1----96
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS )Contract: l2-88l-REVS
Lab Code: COMPU Case No.: 11902 SAS No.: SDG
Matrix: (soil/water)
( SOIL Lab Sample IO:
Sample wt/vol: 30,0 (g/mL) Si__ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. ---1.Q dee. Date. Extracted:
EPA SAMPLE NO.
SL-7-1
No.: ~l
291040
GH09l040A20
09/30/89
10/04/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/W) H,_ pH: 1,7
Date Analyzed: 10/07/89
Dilution Factor: -l-,O~O,.___
Number TICS found:__!.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/RG
RT EST. CONC. Q =---=-----------=----=--=---=-=-------=====~ --====--•=========--=
l. BLANK CONTAMINANT
2. BLANK CONTAMINANT
3. ALOOL
4. UNRNOWN
l
FORM I SV-TIC
4.20
4.32
5.37
6.45
300
220
440
150
BJ
BJ
BAJ'
J
1/87 Rev.
--95 ··-
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-8-1
La.b Name: COMPUCHEM LABS Contract:. (2-88)-REVS
La.b Code: COMPO Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL La.b Sample ID: 291038
Sample wt/vol: 30, O (g/mL) Si__ ' La.b File ID: GH091038C20
Level: (low/med) LOW Date Received: 09/30/89
% Moisture: not dee. ----12 dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) ~ · Date Analyzed: 10/07/89
GPC Cleanup: (Y/N) lL_ pH: 8,0 Dilution Factor: 1,00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Rg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------.bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichloro.benzene 370
106-46-7--~----~l,4-Dichlorobenzene 370
100-s1-6--------Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-0imethylphenol 370
65-85-o---------Benzoic Acid 1800
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 370
120-83-2--------2,4-0ichlorophenol 370
120-82-1---~----1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-5 7-6---------·2-Methylnaphthalene 370
77-47-4------~--Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroanilin• 1800
131-11-3--------Dimethyl Phthalat.e 370
.208-96-8--------Acenaphthylene 370
606-20-2--------2,6-0initrotoluene 370
u
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u u u u
u u u u u
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u u u u
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Q
FORM I sv-1 1/87 Rev.
-==--±AA-.: --_--±SR ,. r: E "DR ra St.ftllPIRt:'=·~~ 94
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS Contract: {2-88)-REVS
SL-8-1
Lab Code: COMPU Case No.: 17902 • SAS No.: SDG No.·: 51
Matrix: (soil/water) SOIL Lab Sample ID: 291038
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID: ~H091038c,o
Level: ( low/med) LOW Date Received: 09/30/89
% Moisture: not dee. __u dee. Date Extracted: 10/04/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/07/89
GPC Cleanup: (Y/N) lL_ pH: 8,0 Dilution Factor: _1~,0-0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2~--------3-Nitroan!line 1800 ·u
83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 370 u
101-55-3--------4-Bromophenyl-phenylether_ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-0---------Phenanthrene 370 u
120~12-1--------Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 u
129-0o-o--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 750 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chrysene 370 u
117-Bl-7--------bis(2-Ethylhexyl)Phthalate_ 410
117-84-0--------Di-n-Octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -Cannot be separated from Diphenylamine
\ FORM I sv-2 1/87 Rev.
----~ ----. .::-=----~ -93
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED. COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample IO:
Sample wt/vol: 30,0 (g/mL) L_ Lab File IO:
Level: (low/med) LOW Date Received:
% Moisture: not dee. _ll dee. Date Extracted:
EPA SAMPLE NO.
SL-8-1
No.: 51
291038
GH091038C20
09/30/89
10/0i/89.
Extraction: (SepF/Cont/Sone) ~
GPC Cleanup: (Y/N) fL_ pH: 8,0
Date Analyzed: 10/07/89
Dilution Factor: _1~,0-0,.____
Number TICs found: _.1
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= &====
\
1.
2.
3.
BLANK CONTAMINANT
BLANK CONTAMINANT
ALDOL
FORM I SV-TIC
4.33
4.42
5.50
230 BJ
230 BJ
340 AJ
1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-9-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30 · 0 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. ---1.i dee.
Extr~ction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti._ pH: 7.9
SDG No. : =-5 .. l __
Lab Sample ID: ..,.2"'"9_.._l.!:!..0~37.:...._ __ _
Lab File IO: GH091037C20
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: -1~,o~o'---
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--~-----Phenol 380 u
lll-44-4--------bis(2-Chloroethyl)Ether 380 u
95-57-8---------2-Chlorophenol 380 u
541-73-1--------1,3-Dichlorobenzene 380 u
106-46-7--------1,4-Dichlorobenzene 380 u
100-51-6--------Benzyl Alcohol 380 u
95~50-1---------1,2-Dichlorobenzene 380 u
95-48-7---------2-Methylphenol 380 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 380 u
106-44-5--------4-Methylphenol 380 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 380 u
67-72-1---------Hexachloroethane 380 u
98-95-3---------Nitrobenzene 380 u
78-59-1-~-------Isophorone 380 u
88-75-5---------2-Nitrophenol 380 u
105-67-9--------2,4-Dimethylphenol 380 u
65-85-0---------Benzoic Acid 1900 u
lll-91-l--------bls(2-Chloroethoxy)Methane_ 380 u
120-83-2--------2,4-Dichlorophenol 380 u
120-82-1--------1,2,4-Trichlorobenzene 380 u
91-20-3---------Naphthalene 380 u
106-47-8--------4-Chloroaniline 380 u
87-68-3---------Hexachlorobutadiene 380 u
59-50-7---------4-Chloro-3-Methylphenol 3.80 u
91-57-6---------2-Methylnaphth~lene 380 u
77-47-4---------Hexachlorocyclopentadiene_ 380 u
88-06-2---------2,4,6-Trichlorophenol 380 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
91-58-7---------2-Chloronaphthalene 380 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalate 380 u
208-96-8--------Acenaphthylene 380 u
606-20-2--------2,6-Dinitrotoluene 380 u
FORM I SV-1 1/87 Rev.
11 ____ _
91
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-9-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: .x.5.._l __
Matrix: (soil/water) SOIL Lab Sample ID: ..,2.c.9&1.x..O:L.37.:.__ __ _
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:. GH091037C20
Level: ( low/med) LOW Date Received: 09/30/89
% Moisture: not dee. ---1.i dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li__ pH:
~
7.9
Date Extracted: 10/04/89
Date Analyzed: 10/07/89
Dilution Factor: .1.,0~0"-_
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1900
83-32-9---------Acenaphthene 380
51-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
13i-64-9--------Dibenz~furan · 380
121-14-2--------2,4-Dinitrotoluene 380
84-66-2---------Diethylphthalate 380
7005-72-3-------4-Chlorophenyl-phenylether_ 380
86-73-7---------Fluorene 380
100-01-6--------4-Nitroaniline 1900
534-52-1------~-4,6-Dinitro-2-Methylphenol_ 1900
86-3.0-6---------N-Nitrosodiphenylamine (l)_ 380
101-55-3--------4-Bromophenyl-phenylether __ 380
118-74-1--------Hexachlorobenzene 380
87-86-5---------Pentachlorophenol 1900
85-01~8---------Phen~nthrene . 380
120-12-1--------Anthracene 380
84-74-2---------oi-n-Butylphthalate 380
206-44-o--------Fluoranthene 380
129-00-o--~-----Pyrene 380
85-68-7---------Butylbenzylphthalate 380
91-94-1---------3,3'-Dichlorobenzidine 770
• 56-55-3---------Benzo(a)Anthracene 380
218-01-9--------Chrysene 380
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 140
117-84-0--~-----Di-n-octyl Phthalate 380
205-99-2--------Benzo(b)Fluoranthen• 380
207-08-9--------Benzo(k)Fluoranthene 380
50-32-8---------Benzo(a)Pyrene 380
193-39-5-.;.------Indeno(l,2,3-cd)Pyrene 380
53-70-3---------0ibenzo(a,h)Anthracene 380
191-24-2--------Benzo(g,h,i)Perylene 380
(l) -Cannot be separated from Oiphenylamine
FORM I sv-2
r: SMPLE DR'CB. -·-..
' ·-
Q
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u
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J
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1/87 Rev.
·-90
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID:
Level: (low/med) _LO_w __ Date Received:
% Moisture: not dee. _li dee. Date Extracted:
EPA SAMPLE NO.
SL-9-1
No.: 51
291037
GH091037~20
090QL89
l.QLQ~L89
Extraction: , (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) !L.. pH: 7,9
Date Analyzed: 1QLQ7L89·
Dilution Factor: _1~,9-0..___
Number TICS found:~
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
--------===-=-=-=•========================a======•====================
\
FORM I SV-TIC 1/87 Rev.
89 -
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
9169SED91MS
Lab Code: COMPU Case No.: 17902 SAS
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) _G_
Level: (low/med) =r.p=-----w __
\ Moisture: not dee. __ll dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li...__ pH:
~
7.8
No. : SDG No.: ... 5 .... 1 __
Lab Sample ID: .2_8_8~5~6-2 ___ _
Lab File ID: GH088562A22
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/29/89
Dilution Factor: _l~-~o~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u·
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u·
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-so-1---------1 2-Dichlorobenzene 370 u , .
95-48~7---------2-Methylphenol 1800
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitros~-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3---------Nitrobenzene 530
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2;4-Dimethylphenol 370 u
65-85-0---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ 370 u
120-83-2~-------2,4-Dichlorophenol 370 u
120-02-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---~--~~-Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---~-----Hexachlorocyclopentadiene __ 370 u
88-06-2---------2,4,6-Trichlorophenol 1500
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 640
606-20-2--------2,6-Dinitrotoluene 570
\ FORM I SV-1
I
l----
1/87 Rev.
~--~--~-~=~·-□s.ie1111e21c::·aE=za1)!11.R□rr:aa:::sst1WP111W!111RJR¥~~~~--=-~·c·:::. :::-=--=..:.::__--• --.--:.;-==--= ---~-----

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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS
9169SED91MS
Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ____ SDG No.: =5 ... l __
Matrix: (soil/water) SOIL Lab Sample ID: .2-8~8~5~6~2 ___ _
Sample.wt/vol: JO.O (g/mL) ~ Lab File ID: GH088562A22
Level: (·low/med) LOW Date R~ceived: 09/22/89
% Moisture: not dee. _.ll dee. Date Extracted: 09/28/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_ pH:
SONC
7.8
Date Analyzed: 09/29/89
Dilution Factor: ... i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) QG/KG
99~09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-~6-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 37()
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-0initro-2-Methylphenol __ · 1800
86-30-6---------N-Nitrosodiphenylamine (1)_' 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol· 1800
85-01-8---------Phenanthrene 47
120-12-1--------Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-0-------~Fluoranthene 480
129-00-o--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1---------3,J'-Dichlorobenzidine 740
56-55-3---------Benzo(a)Anthracene 370
218~01-9~-------chrysene 350
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 190
117-84-0--------oi-n-Octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2-----~--Benzo(g,h,i)Perylene 280
(1) -cannot be separated from Oiphenylamine
FORM I SV-2
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1-----==•-·-&:=-_:::;-~=-._:::!·/.==.-=--,sue~-l!S:IIKll!IS.-[•£r""""_,Qr,;~7"1"'Trrgr-:--l:5l~I .... Sl!lrl:R,~s11~---;;;:::;;;·~-.=--. -~:__-. ---(17 -----~ --· -------
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: <2-88)-REVS
916.9SED91MSD
Lab Code: COMPU Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) ~
Level: (low/med) _LO_W __
% Moisture: not dee. __ll
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li,__
dee.
pH:
~
7.8
SDG No.: _5_1 __
Lab Sample ID: 288563 ......... -=---==----
Lab File ID: · GH088563822
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/29/89
Dilution Factor: _l~·~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
.-•;. ,,.:,: · ......... ' '.~ ' ',.'
108-95-2--------Phenol 370 u
lll-44-4--------pis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7---:-----1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 1600
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7---~----N-Nitroso-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3---------Nitrobenzene 430
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-0---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-82-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6-----~---2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene __ 370 u
88-06-2---------2,4,6-Trichlorophenol 1200
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--~-----Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 520
606-20-2--------2,6-Dinitrotoluene 5~0
FORM I SV-1 1/87 Rev.
86
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
9169SED91MSD
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ~5.._l __
Matrix: (soil/water) SOIL Lab Sample ID: ~2-·8_8_5~6=3 ___ _
Sample wt/vol: 30. 0 (g/mL) _G_ Lab File ID: GH088563822
Level: ( low/med) LOW
% Moisture: not dee. __u dee.
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/29/89
Dilution Factor: 11 00
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H__ pH: 7.8
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-7--------4-Nitrophenol 1800 u·
132-64-9--------Dibenzofuran 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether __ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 370 u
101-55-3--------4-Bromophenyl-phenylether __ ·370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 370 u
120-12~1--------Anthracene 370 u
84-74-2---------oi-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 590
129-oo-o---~----Pyrene 370 u
85-68-7---~---~-Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 740 u
56-55-3---------Benzo(a)Anthracene 420
218-01-9--------chrysene 450
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 220 BJ
117-84-0--------Di-n-Octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2---~----Benzo(g,h,i)Perylene 320 J
(1) -Cannot be separated from D1phenylam1ne
FORM I SV-2 1/87 Rev.
-iii----___ lllllliiiii ______ ..... -, ..... -liiiii ......... -...... S ... Rs.fla;&a;P;....il ....... £ DR Ill SDMRRY ===--""'"-85
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PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
SED-1-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ..,5=1 ____ _
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) ~
LOW
Lab Sample ID: =2_9 ..... 10"""3..._6..._ __
Lab File ID:
Level: (low/med)
% Moisture: not dee. _8_6_ dee.
Date Receiv~d: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ~-pH: ....1..:.i Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 57. U
319-85-7--------beta-BHC=-----------57. U
319-86-8--------delta-BHC_-------------.57. U
58-89-9-----~---gamma-BHC (Lindane)____ 57. u
76-44-8---------Heptachlor_________ 57. U
309-00~2-----,;.--Aldrin.~---...,.....,,-----57. U
1024-57-3-------Heptachlor epoxide_____ 57. u
959-98-8--------Endosulfan I________ 57. U
60-57-1---------Dieldrin_________ 110 u
72-55-9---------4,4'-DDE_________ 110 U
72-20-8---------Endrin 110 U
33213-65-9------Endosu~l~f-an___,,I~I~------110 U
72-54-8---------4,4'-DDD __ ~------110 U
1031-07-8-------Endosulfan sulfate 110 U
50-29-3---------4,4'-DOT,,__ ____ -_-_-_-_-_-_-_-:_-.110· U
72-43-5---------Methoxychlor 570 u
53494-70-5------Endrin keton_e _____ ......;..._ 110 u
5103-71-9-------alpha-Chlordane-,-_____ 570 u
5103-74-2-------gamma-Chlordane______ 570 u
8001-35-2-------Toxaphene~~-------1100 u
12674-11-2------Aroclor-1016 570 u --------11104-28-2------Aroclor-1221________ 570 U
11141-16-5------Aroclor-1232 570 U --------53469-21-9------Aroclor-1242_______ 570 U
12672-29-6------Aroclor-1248 .570 U --------11097-69-l------Aroclor-1254 1100 U --------11096-82-5------Aroclor-1260_______ 1100 IU
Q
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
SED-3-1
Lab Name: COMPUCHEM LABORATORIES Contract: l2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ___ SDG No.: .._5..._1 ___ _
Matrix: (soil/water) SOIL Lab Sample IO: ..._2..__91...,0..,.3~4 __ _
Sample wt/vol: Lab File ID:
Level:
30.0 (g/mL) L_
LOW
% Moisture: not dee. -19L-_
Extraction: (SepF/Cont/Sonc)
dee.
SQHC.
pH: ....L.J...
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) L_ Dilution Factor:
CAS NO •. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7----~---beta-BHC ---------3 l 9 -86 -8 -

-

-
-

-

-

-

-
delta -

B

H

C

________ _
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-a---------Heptachlor _______ _
309-00-2--------Aldrin ·,.....,..---....,.-,-----
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I -------
60-57-1---------Dieldrin ·---------
72-55-9-------~-4,4'-DDE ________ _
72-20-8---------Endrin.__,, ________ _
33213-65-9------Endosulfan II ______ _
•72-54-8---------4,4'-DDD_· _______ _
1031-07-8-------Endosulfan sulfate -----
50-29-3---------4,4'-DDT ________ _
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone -------
5103-71~9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene __________ _
12674-11-2------Aroclor-1016 ______ _
11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9~-----Aroclor-1242
12672-29-6------Aroclor-1248
--------------
11097-69-l------Aroclor~l254 ______ _
11096-82-5------Aroclor-1260 -------
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10 EPA SAMPLE NO .
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SED-3-2
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902· SAS No.: SDG No.: .... 5 ... 1 ____ _
Matrix: (s6il/water) SOIL Lab Sample ID: ...,2.._9 ..... l.,._0-35..__ __
Sample wt/vol:
Level: '( low/med)
30.0 (g/mL) L_
LOW
% Moisture: not dee. 18 dee.
Extraction: (SepF/Cont/Sonc) SQHC
Lab File ID:
Date Received: 09/30/89
Date Extracted: 10/17/89
Date Analyzed: 10/17/89
GPC Cleanup: (Y/N) H...._ pH: _L_i Dilution Factor: 1. 00 -
CAS NO. COMPOUND
CONCENTRATION UNITS: .
(ug/L or ug/Kg) UG/KG
I
319-84-6--------alpha-BHC_________ 9.8 IU
319-85-7--------beta-BHC..,,,....._________ 9.8 IU
319-86-8--------delta-BHC_________ 9.8 IU
58-89-9---------gamma-BHC (Lindane)____ 9. 8 I U
76-44-8---------Heptachlor_________ 9.8 IU
309-00-2-----~--Aldrin ____ _,....,_____ 9.8 IU
1024-57-3-------Heptachlor epoxide_____ 9.8 U
959-98-8--------Endosulfan I________ 9.8 U
60-57-1--~------Dieldrin_________ 20. U
72-55-9---------4,4'-DDE_________ 20. U
72-20-8---------Endrin 20. U
33213-65-9------Endosu."'""l"""fa_n_I ___ I_______ 20. U
72-54-8---------4,4'-DDD_________ 20. U
1031-07-8-------Endosulfan sulfate · 20. U -----50-29-3---------4,4'-DOT_________ 20. U
72-43-5---------Methoxychlor________ 98. U
53494-70-5------Endrin ketone_______ 20. U
5103-71-9-------alpha-Chlordane______ 98. u
5103-74-2-------gamma-Chlordane______ 98. !°U
8001-35-2-------Toxaphene 200 IU
12674-11-2------Aroclor-1~0~16,,,,....-------98. IU
11104-28-2~-----Aroclor-122 l 98. I u
11141-16-5----~-Aroclor-1232________ 98. IU
53469-21-9------Aroclor-1242 98. I U --------12672-29-6------Aroclor-1248_______ 98. IU
11097-69-1------Aroclor-1254 200 10 --------11096-82-5------Aroclor-1260_______ 200 IU
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10
PESTICIDE ORGANICS ANAf,YSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
SED-4-1
Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
,·Moisture: not dee. 40 dee. Date Extracted:
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed:
GPC Cleanup: (Y/N) H._ pH: ....L..a Dilution Factor:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
319-84-6--------alpha-BHC ______ .;.._ __
319-85-7--------beta-BHC 319-86-8--------delta-BH_C ________ _
58-89-9---------gamma-BHC ( Lindane ) __ . ___ _
76-44-8-------.--Heptachlor _ ___,. ______ _
309-00-2--------Aldrin ·----------1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin. _________ _
72-55-9---------4,4'-DDE _________ _
72~20-8---------Endrin . ._.., ________ _
33213-65-9----~-Endosulfan II -------72-54-8------~--4,4'-DDD ________ _
1031-07-8-------Endosulfan sulfate -----50-29-3---------4,4'-DDT ________ _
72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ .....;,_
8001-35-2-------Toxaphene ___ · _____ _
12674-11-2------Aroclor-1016 _______ _
11104-28-2------Aroclor-1221 _______ _
11141-16--5------Aroclor-1232 --------53469-21-9----~-Aroclor-1242 _______ _
12672-29~6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-12 60 ______ _
UGLI.G.
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PESTICI0E ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM ~BORATORIES
SED-5-1
Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ... 5.-l ____ _
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G.__
LOW
Lab Sample ID: .::.2_,._9.,._0.,._8-16,.__ __
Lab File ID:
Level: (low/med)
% Moisture: not dee. _2_3_ dee.
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/08/89 Extraction: (SepF/Cont/Sonc) SQHC
GPC Cleanup: (Y/N) H.._ pH: _L_B. Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 0
319-84-6--------alpha-B~C ________ _
319-85-7--------beta-BHC ---------3 l 9 -86 -8 -

-

-

-

-

-

-

-
delta -

B

H

C

---------5 8-8 9.-9---------gamma-BHC ( Lindane) ___ _
76-44-8---------Heptachlor ________ _
309-00-2--------Aldrin ____ ...,....., ______ _
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin -----------------72 -55 -9 -

-

-

-

-

-

-

-

-
4, 4 ' -DD E ________ _
72-20-8---------Endrin. _________ _
33213-65-9------Endosulfan II -------72-54-8---------4,4'-DDD ___ .,,.... _____ _
1031-07-8-------Endosulfan sulfate ·-----50-29-3---------4,4'-DDT ________ _
72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ________ _
12674-11-2------Aroclor-1016 _______ _
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 _______ _
53469-21-9------Aroclor-1242 _______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1-----~Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _______ _
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10. IU
10. IU
10. IU
10. IU
10. U
21. U
21. U
21. U
21. U
21. U
21. U
21. · U
100 U
21. U
100. U
100 U
210 U
100 U
100 U
100 U
100 U
100 U
210 U
210 U
........... w .... -•• 1.----------........ -.. ,,.-.. ,,... __ ..,.,. ___ ...,._...,. __ ,,... __ -. ,,..._ -........................ ~. -----,..----
-80
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
·Lab Name: COMPUCHEM LABORATORIES
SED-6-1
Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 51
Matrix: (soil/water) SOIL Lab Sample ID: 290820
Sample wt/vol: JO.Q (g/mL) G..._ Lab File ID:
Level: (low/med) :i;.ow Date Received: Q9L29L89
% Moisture: not dee. 27 dee. Date Extracted: 10 LP4 L89
Extraction: (SepF/Cont/Sonc) SQHC. Date Analyzed: 10Lo2La2
GPC Cleanup: (Y/N) L.. pH: -1..J.. Dilution Factor:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
319-84-6-----~--alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8-----~--delta-BH=c---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin.,....,,..~. ----=------
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin -------
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin
33213-65-9------Endosu~l~f-an---,I~I=--------
72-54-8---------4,4'-DDD
1031-07-8------~Endosulf'_a_n_su~l~f~a~t-e------
50-29-3---------4,4'-DDT,....,,.. _______ _
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-----:.--alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1=0~1~6-------
11104-28-2------Aroclor-1221
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242
12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 ______ _
UGLKG
I
11. IU
11. IU
11. IU
11. U
11. U
11. U
11. U
11. U
22. U
2,2. , U
22. U
22. U
22. U
22. U
22. U
110 U
22. U
110 U
110 U
220 U
110 U
110 U
110 U
110 U
110 U
220 U
220 U
1.00
Q
----------------•tll'l0..,.ltM""'4!..-•11!pMf'l!:!f'l'.-----------~1r,7~'87-i{ev.
79
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e
10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SED-7-1
Lab Name: COMPUCHEM LABORATORIES ' Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: •..c.5._1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: .:::..2 L..:9 O>L:18L:!!lut..9 __ _
Sample wt/vol: 30.0 (g/mL) L_
LOW
Lab File ID:
Level: (low/med)
% Moisture: not dee. -29-._ dee.
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) SQHC.
GPC Cleanup: (Y/N) H__ pH: -2...:..i Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
319-84-6--------alpha-BHC_________ 11. IU
319-85-7--------beta-BHC 11. I U
319-86-8--------delta-BH_C_________ 11. IU
58-89-9---------gamma-BHC -(Lindane)____ 11. I u
76-44-8---------Heptachlor________ 11. IU
309-00-2--------Aldrin.,........ ___ ----,--,,--____ 11. IU
1024-57-3-------Heptachlor epoxide_____ 11. IU
·959-98-8--------Endosulfan I_______ 11. IU
60-57-1---------Dieldrin_________ 22. IU
72-55-9---------4,l'-DDE_________ 22. IU
72-20-8---------Endrin...,....._________ 22. IU
33213-65-9------Endosulfan II_______ 22. \U
72-54-8---------4,4'-DDD __ ......,,...~-----22. IU
1031-07-8-------Endosulfan sulfate_____ 22. IU
50-29-3---------4,4'-DDT_________ 22. IU
0
72-43-5---------Methoxychlor_______ 110 I U
53494-70-5------Endrin ketone_______ 22. IU I
5103-71-9-------alpha-Chlordane______ 110 IU .I
5103-74-2-------gamma-Chlordane __ -'----110 IU I
8001-35-2-------Toxaphene_________ 220 I u I
12674-11-2------Aroclor-1016_______ 110 IU I
11104-28-2------Aroclor-1221 ______ --'-110 I U I
11141-16-5------Aroclor-1232_______ 110 IU I
53469-21-9------Aroclor-1242_______ 110 IU I
12672-29-6------Aroclor-1248_______ 110 IU I
11097-69-1------Aroclor-1254_______ · 220 IU I
11096-82-5------Aroclor-1260_______ 220 IU I
---------------------------'--' ...... ----., .... _
----------------...ORM -X -,!!:S'_T ___________ ""'IJ""il~'74Tte,J.
-·--78 ···-
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
· I I.
· Lab Name: COMPUCHEM LABORATORIES
I. SL-1-1 I
Contract: (2-88)-REVS 1-------1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .._5_1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: =-29_,0iu,8 ..... 2..,..6 __ _
Sample wt/vol: 30.0 (g/mL) .G.,__
LOW
Lab File ID:
Level: (low/med)
% Moisture: not dee . ....,12 __ dee.
Date Received: 09/29/89
Date ~xtracted: 10/04/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: ( Y /N) H.._ . pH: _Lj_ Dilution Factor: 1.00
'
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC ---------3 l 9 -86 -

8

-

-

-

-

-

-

-

-
delta -B H C ----,----,-------58-89~9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin ,....,_...---...,.....,.--------1024 -57 -

3

-

-

-

-
--

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endoaulfan I -------60-57-1---------Dieldrin ---------72 -55 -9 -

-

-

-

-

-

-

-

-
4, 4 ' -DD E ________ _
72-20-8---------Endrin ------------33213-65-9------Endosulfan II -------72-54-8---------4,4'-DDD 1031-07-8-------Endosulf_a_n_s_u~l~f~a-t_e ____ _
50-29-3---------4,4'-DDT,....,_... _______ _
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene __________ _
12674-11-2------Aroclor-1016 -------11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 -------
·'f'.;•;
..,, PdltR -i i'tSf
I 9 .1 IU
9 .1 I u
9 .1 IU
9 .1 IU
9 .1 I u
9 .1 I u
9. 1 IU
9 .1 I u
18. IU
18. IU
18. IU
18. IU
18. IU
18. IU
18. IU
91. IU
18. IU
91. IU
91. IU
180 IU
91. IU
91:. IU
91. IU
91. IU
91. IU
180 IU
180 · IU
. . ········· l.__,_,----·-----··-··---·
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-2-2 I
I
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS -----1.
Lab Code: COMPU Case No . : 17 9 0 2 SAS No.: SDG No. : _5.._l _-,--__
Matrix:. ( soil/water) SOIL Lab Sample ID: =2..._90....,8...,,2.._9 __ _
Sample wt/vol: 30.0 (g/mL) G...__
LOW
Lab File ID:
Level: (low/med)
% Moisture: not dee. _1_1_ dee.
Date Received: 09/29/89 ·
Date Extracted: 10/04/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanups (Y/N) IL_ pH: __L,j_ Dilution Factor: 1.00 ·
CONCENTRATION UNITS:
CAS. NO. COMPOUND (ug/L o~ ug/Kg) UG/KG Q
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH=c---------
s~-89-9------~--gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin ~---~~----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endosulfan I ______ _
60-57-1---------Dieldrin ________ _
72-55-9---------4,4'-DDE
72-20-8---------Endrin ---------
33213-65-9------Endosulfan II -------72-54-8---------4,4'-DDD 1031-07-8-------Endosulf_a_n_s_u~l~f~a~t-e ____ _
50-29-3---------4,4'-DDT....-:---------
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone
5103-71-9-------alpha-Chlorda_n_e _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1~0~1~6------------
11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242
12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 -------
9.0
9.0
9.0
9.0
9.0
9.0
9.0
9.0
18.
18.
18.
18.
18.
18.
18.
90.
18.
90.
90.
180
90.
90.
90.
90.
90.
180
180
I I
IU I
IU I
IU I
IU I
u I
u I
u I u
u u
u u u
u u
u
u u u
u
u
u
u u
u u
u
' -----------------..ipor'IIRRff"~=ti-t'Pl'l!ES'"'T~-----.-----•1,..rrca,.,1,..."'"'ft'lfAev~. --
76
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10
.PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-2-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .._5_1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: 290823
Sample wt/vol: Lab File ID:
Level: (low/med)
30.0 (g/mL) L_
LOW
% Moisture: not dee ...... 10 __
Extraction: (SepF/Cont/Sonc)
dee.
~
pH: -1..:..2.
Date Received: 09/29/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) L..
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 8.9 U
319-85-7--------beta-BHC 8.9 U
319-86-8--------delta-BH-c-. --------8.9 U
58-89-9---------gamma-BHC (Lindane)____ 8.9 U
76-44-8---------Heptachlor________ 8.9 U
309-00-2--------Aldrin 8.9 U ·----------1024-57-3-------Heptachlor epoxide_____ 8.9 U
959-98-8--------Endosulfan I_______ 8.9 U
60-57-1---------Dieldrin__________ 18. U
72-55-9---------4,4'-DDE_________ 18. U
72-20-8----~----Endrin___________ 18. U
33213-65-9------Endosulfan II 18. U -------72-54-8---------4,4'-DDD____________ 18. U
1031-07-8-------Endosulfan sulfate 18. U -----50-29-3---------4,4'-ODT_________ 18. U
72-43-5---------Methoxychlor_______ 89. u
53494-70-5------Endrin ketone_______ 18. u
5103-71-9-------alpha-Chlordane______ 89. u
5103-74-2----~--gamma-Chlordane______ 89. U
8001-35-2-------Toxaphene_________ 180 u
12674-11-2------Aroclor-1016 89. U -------11104-28-2------Aroclor-1221 89. U -------11141-16-s-~----Aroclor-1232_______ 89. u
53469-21-9------Aroclor-1242_______ 89. IV
12672-29-6------Aroclor-1248_______ 89. IU
11097-69-1------Aroclor-1254_______ 180 IU
11096-82-5------Aroclor-1260_______ 180 IU
1.00
0
---------------------------1--••-ON•,ou ___ ,
-------------~,.,RM--r--p-t-st __________ ..,...i/Pt19""'7~9f<"''1::iv,-.-•
-·-iiii,-==,liii=iii. ______ liii.-_ ...... ____ FF,lm=&' ...._ .. S .. ■m.1l'licu:P:.aC~E DR TEL S081fll#¥·;____ 75 -
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
SL-3-1
Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: ... 5..-1 ____ _
Matrix: (soil/water) SOIL Lab Sample IO: .... 2_90-8.....,4...,..9 __ _
Lab File IO: Sample wt/vol: .
Level: · (low/med)
30.0 (g/mL) G__
LOW
, Moisture: not dee. _13 __
Extraction: (SepF/Cont/Sonc)
dee.
Date Received: 09/29/89
Date Extracted: 10/25/89
Date Analyzed: 10/26/89
GPC Cleanup: (Y/N) fi.._ pH: .....1..:.i
CASNO. COMPOUND
Dilut,f.on Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC 9.2 U
319-85-7-~------beta-BHC 9.2 U
319-86-8--------delta-BHC 9.2 U
58-89-9-------~-gamma-BHC (Lindane) 9.2 U
76-44-8---------Heptachlor 9.2 u
309-00-2--------Aldrin 9.2 U
1024-57-3----~--Heptachlor epoxide 9.2 u
959-98-8--------Endoaulfan I 9.2 U
60-57-1---------Dieldrin 18. u
72-55-9--~------4,4'-DDE 18. U
72-20-8---------Endrin 18. U
33213-65-9------Endosulfan II· 18. IU
72-54-8---------4, 4' -ODD 18. I U
1031-07-8-------Endosulfan sulfate 18. IU
50-29-3---------4, 4 '-DDT · 18. I U
72-43-5-----~---Methoxychlor 92. IU
53494-70-5------Endrin ketone 18. IU
5103-71-9-------alpha-Chlordane 92. IU
5103-74-2-------gamma-Chlordane 92. IU
8001-35-2-------Toxaphene 180 1·u
12674-11-2------Aroclor-1016 92. IU
11104-28-2------Aroclor-1221 92. IU
11141-16-5------Aroclor-1232 92. IU
I. 53469-21-9------Aroclor-1242 92. I U
I 12672-29-6------Aroclor-1248 92. IU
I 11097-69-1------Aroclor-1254 180 IU
I 11096-82-5------Aroclor-1260 180 IU
1.00
0
. ···•--.......... :. '---------~~~------~-~ .~---~~= '--'--•·-"• -·•·-
' POMl-i'. i'!Sf
&--74
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-4-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COHPU Case No.: l79oi SAS No.: SDG No. : _5_1 ___ ____
Matrix: (soil/water) sou. Lab Sample ID: 290831
Sample wt/vol: JO.Q (g/mL) ~ Lab File ID:
Level: (low/med) LOH
% Moisture: not dee. ll dee.
Date Received: 09/29/89
Date Extracted: 10/18/89
Date Analyzed: 10/18/89 Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) t!._ pH: --L:_i . Dilution Factor:. -~i~-~0~Q
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
31~-84-6----~---alpha-BHC_________ 9.0 U
319-85-7--------beta-BHC 9.0 U
319-86-8--------delta-BH=c---------9.0 U
58-89-9---------gamma~BHC (Lindane)_.____ 9.0 U
76-44-8---------Heptachlor________ 9.0 u
309-00-2--------Aldrin 9.0 U ~----:-::-----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide_____ 9.0 U
959-98-8--------Endosulfan I_______ 9.0 U
60-57-1---------Dieldrin_________ 18. U
72-55-9---------4,4'-DDE_._________ 18. U
72-20-8---------Endrin 18. U
33213-65-9------Endosu~l~f-an----,I=I=-----,-----18. u
72-54-8---------4, 4 '-DOD 18. I U
1031-07-8-------Endosulf_a_n_s_u~l~f~a..,,.t_e_.______ 18. U
50-29-3---------4,4'-DDT 18. U
72-43-5---------Methoxyc~h~lo_r________ 90. U
53494-70-5------Endrin ketone_______ 18. U
5103-71-9-------alpha-Chlordane______ 90. U
5103-74-2-------gamma-Chlordane______ 90. U
8001-35-2-------Toxaphene 180 u
12674-11-2------Aroclor-l.,..0~l":'"6_______ 90. U
11104-28-2------Aroclor-1221 90. U
11141-16-5------Aroclor-1232_______ 90. U
53469-21-9------Aroclor-1242 90. U
12672-29-6------Aroclor-1248_______ 90. U
11097-69-1------Aroclor-1254_______ 180 U
11096-82-5------Aroclor-1260_______ 180 IU
Q
----, ..... -....... ----------,------------,------~~..,.,..J .. -. --. -, .. -, .. """'···=·· ·=····=··---,-, ___ J_ __ . __
' I
1----lE 73
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·1
;1
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
SL-5-1
Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: .._5..._1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: _2_90~8.....,4 ...... 5 __ _
Sample wt/vol: Lab File ID:
Level: (low/med)
30.0 (g/mL) ~
LOW
% Moisture: not dee. _12 __
Extraction: (SepF/Cont/Sonc)
dee.
~
pH: --1.:_5.
Date Received: 09/29/89
Date Extracted: 10/12/89
Date Analyzed: 10/12/89
GPC Cleanup: (Y/N) li__ Dilution Factor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8-------~delta-BHc=---------
58-89-9---------gamma-BHC (Lindane) ___ _ ;g9~~0~2:::::::::!~;1~hlor _______ _ :-,,----...,.....,-----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin -------
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin --....,,,..,~------332 l 3 -65 -9 -

-

-

-

-

-
Endo sulfa n II
72-54-8---------4,4'-DDD -------
1031-07-8-----~-Endosulfan sulfate -----50-29-3---------4,4'-DDT
72-43-5---------Methoxyc~h~lo-r---:------
53494-70-5------Endrin ketone
5103-71-9-------alpha-Chlorda-ne _____ _
5103-74-2-------gamma~Chlordane _____ _
8001-35-2-----~-Toxaphene
12674-ll-2------Aroclor-1~0~16~-------
11104-28-2-~----Aroclor-1221
11141-16-5------Aroclor-1232------~
53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 ______ _
I 9.1 U
9.1 U
9.1 U
9.1 U
9.1 U
9.1 U
9.1 U
9.1 U
18. U
18. U
18. U
18. U
18. U
18. U
18. U
91. U
18. U
91. U
91. U
180 U
91. U
91. U
91. U
91. U
91. U
180 U
180 U
1.00
Q
11096-82-5------Aroclor-1260 ______ _ I --·•··········•········•·
I
I
I
~;
<(' ----------------.~!~~T,.,_ __________ a.l!!Mf8"'1rY1•,~e~vr.--
I
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
SL-6-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .... 5 ... 1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: =2.-.91....,0....,3...,._9 __ _
Sample wt/vol: 30.0 (g/mL) G___ Lab File ID:
Level: (low/med) LOW
% Moisture: not dee. _11 __
Extraction: (SepF/Cont/Sonc)
dee.
SQHC
pH: ....LJ2.
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) lL_ Dilution Fatter:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC ~--------3 l 9 -86 -8 -

-

-

-

-

-

-

-
delta -

B

H

C

~=-:--.--~---58 -89 -

9

-

-

-

-

-

-

-

-

-
gamma -B H C (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin -:-:-----:--::-----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------0ieldrin -------
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin 33213-65-9------Endosu~l~fa-n----,I=I,,_ _____ _
72-54-8---------4,4'-OOD
1031-07-8-------Endosulf_a_n_s_u~l~f~a~t-e ____ _
50-29-3---------4,4'-O0T 72-43-5---------Methoxyc~h~lo_r _______ _
53494-70-5------Endrin ketone
510 3-71-9-------alpha-Chlorda_n_e__,,.. ____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene
12674-ll-2------Aroclor-1=0~16~-------
11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232
53469-21-9------Aroclor-1242 -------
12672-29-6----~-Aroclor-1248 ______ _
11097-69·-1------Aroclor-1254 11096-82-5------Aroclor-1260 ______ _
9.0
9.0
9.0
9.0
9.0
9.0
9.0
9.0
18.
18.
18.
18.
18.
18.
18.
90.
18.
90.
90.
180
90.
90.
90.
90.
90.
180
180
I
IU
IU
IU u u u
u u
u
u u u
u u
u
u
u u
u u u
u u
u
u
u
u
1.00
Q
····.._.._.,,. __ _ ---------,-------,-------------~---,J--....... -··-.. --.. --
'
------------71
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
SL-7-1
Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ...,5.._1 ___ _
Matrix: (soil/water) SOIL Lab Sample IO: 291040
Sample wt/vol: Lab File ID:
Level: (low/med)
30.0 (g/mL) G___
LOW
% Moisture: not dee. _10 __ · dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) IL_
~
pH: ....1...J..
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
Dilution Factor: -1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH=c---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2-~------Aldrin· -=--=------:--:-----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin -------
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin
33213-65-9------Endosu~l-f-an-I~I~------
72-54-8---------4,4'-DDD
1031-07-8-------Endosulf_a_n_s_u~l~f~a~t-e ____ _
S0-29-3---------4,4'-DD'l'-=--=---------
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone
5103-71-9-------alpha-Chlorda-ne _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene~~-------
12674-11-2------Aroclor-1016 11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248
11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 ______ _
8.9 U
8.9 U
8.9 U
8.9 U
8.9 U
8.9 U
8.9 U
8.9 U
18. U
18. U
18. U
18. U
18. U
18. U
18. U
89. U
18. U
89. U
89. U
180 U
89. U
89. U
89. U
89. U
89. U
180 U
180 U
........ --......... _____ __,.;.. _______________ ------
0
---------------.CR,X-r-,,~~S'l'------------... 1.,,1arr7,~7t""lr.::ev;,-. -
... --™iiil------liiiiiiiiii~-.... --"!!!!-!!!!!!!!!!!!!'""' __ ......,-...__.._........., .. :im;,_-·-S1111811118P-_ ..... l..,£-DR ta SDl'IIB1RV=~ --70
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lEiF
10
. PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
SL-8-1
Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 51 -----
Matrix: (soil/water) SOIL Lab Sample ID: -2_91_0_3_8 __ _
Sample wt/vol: 30.0 (g/mL) L-
Level: · (low/med) LOW
\ Moisture: not dee. ,.....12 __ dee.
Extraction: (SepF/Cont/Sonc) SQHC.
GPC Cleanup: (Y/N) H.,_ pH:~
CAS NO. COMPOUND
Lab File ID:
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG 0
I
319-84-6--------alpha-BHC_________ 9.1 U I
319-85-7--------beta-BHC 9.1 U I
319-86-8--------delta-BH.~C---------9.1 U I
58-89-9---~--~--gamma-BHC (Lindane)____ 9.1 U I
76-44-8---------Heptachlor________ 9.1 u I
309-00-2--------Aldrin-----:---:------9.1 U I
1024-57-3----~--Heptachlor epoxide_____ 9.1 U I
959-98-8--------Endosulfan I 9,1 U I
60-57-1---------Dieldrin -------18. U I
72-55-9--~--~---4,4'-DDE_________ 18. U I
72-20-8---------Endrin 18. U I
33213-65-9------Endosu-=-1-=fa-n---:I=-=1=--------18. u ·1
72-54-8---------4,4'-DDD 18. U I
1031-07-8-------Endosulf_a_n_s_u~l~f~a~t-e_____ 18. u I
50-29-3---------4,4'-DM-________ · 18, U I
72-43-5---------Methoxychlor 91.· U I
53494-70-5------Endrin keton_e_______ 18. u I
5103-71-9-------.alpha-Chlordane______ 91. U I
5103-74-2-------gamma-Chlordane______ 91. U I
8001-35-2-------Toxaphene 180 u I
12674-11-2------Aroclor-1~0~16::--------91. u I
11104-28-2------Aroclor-12.21_______ 91. u I
11141-16-5------Aroclor-1232 91. U I -------53469-21-9------Aroclor-1242 91. U I
12672-29-6------Aroclor-1248_______ 91. U I
11097-69-1------Aroclor-1254_______ 180 U I·
11096-82-5------Aroclor-1260_______ 180 IU I
--------~~~~------::~-::.-~ ... ~ ... ~ ... = ..... ,-.... ~ .. ~ ..... ~ .. -~-~ .... ~~~-:":'." .. ~-.I,,-,. -. -1
PURR i P!Sf i71!'Mev.
---~-s@ RlE .]lRtR .SU8ftmtr~--69
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10
PESTICI<OE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-9-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No,: SDG No.: ""'5.._l ___ _
Matrix1 (soil/water) SOIL Lab Sample ID: ..._2..._9la..i,OUll3~7 __ _
Sample wt/vol: Lab File ID:
Level: (low/med)
30.0 (g/mL) G__
LOW
I Moisture: not dee. 14 dee.
Extraction: (SepF/Cont/Sonc) .SQlK
Date Received: 09/30/89
Date Extracted: 10/04/89
Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) tL_ pH: _L_1 Dilution Factor:
\
·\
CAS NO. -COMPOUND
CONCENTRATION UMITS1
(ug/L qr ug/Kg) UG/KG
319-84-6--------alpha-BHc_· _______ _
319-85-7--------beta-BHC ________ _
319-86-8--------delta-BHC _ _,...--=-------
58-89-9---------gamma-BHC (Lindane)_· ___ _
76-44-8---------Heptachlor _______ _
309-00-2--~-----Aldrin. _________ _
1024-57-3-------Heptachlor epoxide_-___ _
959-98-8--------Endosulfan I ______ _
60-57-1---------Dieldrin. ________ _
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin._,,, ________ _
33213-65-9------Endosulfan II ______ _
72-54-8---------4,4'-DDD ________ _
1031-07-8-------Endosulfan sulfate -----50-29-3---------4,4'-DOT ________ _
72-43-5----~~---Methoxychlor ______ _
53494-70-5------Endrin ketone. ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2----~--gamma-Chlordane ___ .....;_ __
8001-35-2-------Toxaphene ________ _
12674-11-2------Aroclor-1016 ______ _
11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 ______ _
11096-82-s------Aroclor~l260 ______ _
9.3
9.3
9.3
9.3
9.3
9,3
9.3
9.3
19.
19.
19.
19.
19.
19.
19.
93.
19.
93.
93.
190
93.
93.
93.
93.
93.
190
190
1.00
0
I u I
u I
u I
u I
u I
u I
u I
u I
U I u
u
u
u
u u u
u u.
u
u u u
u
u
u
u
u
-----------------ou,..2t..-2i'"!i.1S"r------------..-1 7•'8irr1-r,"'l!lev.
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
I I
9168SED21 I Lab Name: COMPUCHEM LABORATORIES .Contract: (2-88)-REVS -------1
Lab Code.: COMPU Case No.: 17902 SAS No.: SDG No.: 51 -----
Matrix: (soil/water) SOIL Lab Sample ID: .,,.,2-88L>5._.4""""5 __ _
Sample wt/vol: 30.0 (g/mL) L-Lab File ID:
Level: (low/med) LOW
% Moisture: not dee ..... 54 __
Extraction: (SepF/Cont/Sonc)
dee.
,SQE
pH:~
Date Received: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/30/89
GPC Cleanup: (Y/N) ti_ Dilution Factor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC ---------3 l 9 -86 -

8

-

-

-

-

-

-

-

-
delta -B H C ---------58 -89 ~ 9 -

-

-

-

-

-

-

-
. ~gamma -B H C ( Lindane ) ___ _
76-4.4-8---------Heptachlor _______ _
309-00-2--------Aldrin .,....,,...----,-,,-----1024 -57 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---;..-----Dieldrin -------
72~55-9---------4, 4 '-DDE ________ _
72-20-8---------End.rin ----------332 l 3 -65 -9 -

-

-

-

-

-
Endo sulfa n II -------72-54-8---------4,4'-DDD __ ~------
1031-07-8----;..--Endosulfan sulfate -----50-29-3---------4,4'-DDT.,....,,... _______ _
72-43-5---------Methoxychlor ______ _
53494-70-5------End.rin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ________ _
12674-11-2----~-Aroclor-1016 -------11104-28-2------Aroclor-1221
11141-16-5-------Aroclor-1232 --------------53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 ______ _
11097-69-1~-----Aroclor-1254 ______ _
11096-82-5------Aroclor-1260
17.
17.
17.
17.
17.
17.
17.
17.
35.
35.
35.
35.
35.
35.
.35.
170
35.
170
170
350
170
170
170
170
170
350
350
1.00
Q
I I
IU I
IU .I
JU I
IU I
IU I
IU I
IU I
IU I
IU
IU
IU
IU
. IU
IU
IU u
u u
u
u
u
u
u I
u I
u I
u I
u I ----------------------------,-.-.-----,..,...,..--,-.,,,,,,.,..,..., ---. J.---·-···-••·-
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
\ I
I 9169SED81
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS I ______ _
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: 51
Matrix: (soil/water) SOIL Lab Sample IO: 288558
Sample wt/vol: 30.0 (g/mL) !L_ Lab File IO:
Level: (low/med) :t.OW Date Received: 09/22/89
% Moisture: not dee. 7 dee. Date Extracted: 09/28/89
Date Analyzed: 09/30/89 Extractions (SepF/Cont/Sonc) ~
GPC Cleanupi
CAS NO.
(Y/N) fi._ pH: _J_J_
COMPOUND
Dilution Factoi: ,
CONCENTRATION UNITSz
(ug/L o~ ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH.~C-~-------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin~---...,.....,-----
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin -------
72-55-9---------4,4'-DDE_-_______ _
72-20-8---------Endrin
33213-65-9------Endosu~l~fa-n--:I~I~------
72-54-8~--------4,4'-DDD 1031-07-8-------Endoaulf_a_n_s_u~l~f-a_t_e ____ _
50-29-3---------4,4'-DDT~--------
72-43-5---------Methoxychlor ______ _
53494-70-5------Endrin ketone -------5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2---.----Toxapherie~-=---------
12674-ll-2------Aroclor-1016 ______ .,...,_
11104-28-2------Aroclor-1221 11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 ~------
8.6 U
8.6 U
8.6 U
8.6 U
8.6 U
8.6 U
8.6 U
8.6 U
17. U
17. U
17. U
17. U
17. U
17. U
17. U
86. U
17. U
86. U
86. U
170 U
86. U
86. U
86. U
86. U
86. U
170 U
170 U
1.00.
Q
··---.. ·--· -. --~--------~-----------------
---------------trr1r0tUf"'t'""P!S'l' __________ ni-....,a1~ev.
· , · ·zrig .. SUPC E . DA Ill Jilll!ifDHlriF 66
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11
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
9169SED91
Lab.Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ... S._1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: ..... 28...,8....,5.....,7_._4 __ _
Sample wt/vol: 30.0 (g/mL) ~
LOW
Lab File ID:
Level: (low/med)
% Moisture: not dee . .-11 __ dee.
Date ~eceived: 09/22/89
Date Extracted: 09/28/89
Date Analyzed: 09/30/89 Extraction: (SepF/Cont/Sonc) ,S,QHC.
GPC Cleanup: (Y/N) L.. pH.: ~ Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
319-84-6--------alpha-BHC ________ _ 9.0 u
319-85-7--------beta-BHC 9.0 u ---------3 l 9 -86 -

8

-

-

-

-

-

-
~ -delta -B H C 9.0 u ---------58 -89 -

9

-

-

-

-

-

-

-

-

-
gamma -B H C (Lindane) ___ _ 15.
76-44-8-------~-Heptachlor _______ _ 12.
309-00-2--------Aldrin 9. O· u ,...,,...----,-,,-----1024 -S 7 -

3

-

-

-

-

-

-

-
Hep tac h lo r epoxide ____ _ .9. 0 u
959-98-8--------Endosulfan I 9.0 u -------60-57-1---------Dieldrin 26. ---------72 -S 5 -9 -

-

-

-

-

-

-

-

-
4, 4 ' -DD E ________ _ 18. u
72-20-8---------Endrin 31. -----------332 l 3 -65 -9 -

-

-

-

-

-
Endo sulfa n II 18. u
72-54-8---------4,4'-DDD -------18. u
1031-07-8-------Endosulfan sulfate 18. u -----50-29-3---------4,4'-DDT,....,,.. _______ _
72-43-5---------Methoxychlor 53494-70-5------Endrin keton_e ______ _
25.
90. u
18. u
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ___________ _
12674-11-2------Aroclor-1016 ______ _
·11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232
90. u
90. u
180 u
90. u
90. u
90. u
53469-21-9--~---Aroclor-1242 ______ _ 90. u
12672-29-6------Aroclor-1248 11097-69-1------Aroclor-1254 ______ _ 90. u
180 u
11096-82-5------Aroclor-1260 180 1u
I
I
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I
I
I
I
-------.............. ,. J ... "". J --1.
---------------•p~o~RMff"C!f.,.-P..,.,!'S~•f-----------~1M7"118'7""'Rev.
65
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11
11
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
SED-3-2MS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: _5_1 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: ...,2_88-5.....,6....,9 __ _
Sample wt/vol: 30, o (g/mL) ~ Lab File ID:
Level: · (low/med) LOW
% Moisture: not dee . ....,18 __
Extraction: (SepF/Cont/Sonc)
dee.
~
pH: ~
Date Received: 09/30/89
Date Extracted: 10/17/89
Date Analyzed: 10/17/89
GPC Cleanup: (Y/N) L.
CAS NO. COMPOUND
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 9.8 U
319-85-7--------beta-BHC 9.8 U
319-86-8--------delta-BH.~C---------9.8 U
58-89-9---------gamma-BHC (Lindane)____ 9.8 u
76-44-8---------Heptachlor________ 9.8 U
309-00-2--------Aldrin~----,--,-.----9.8 U
1024-57-3----~--Heptachlor epoxide_____ 9.8 U
959-98-8--------Endosulfan I 9.8 U
60-57-1---------Dieldrin -------20. u
72-55-9--~--~---4,4'-DDE 20. U
72-20-8---------Endrin ---------20. u
33213-65-9------Endosulfan II 20. U
72-54-8---------4,4'-DDD -------20. U
1031-07-8-------Endosulfan sulfate 20. U -----50-29-3---------4,4'-DM~--------· 20. U
72-43-5---------Methoxychlor_______ 98. U
53494-70-5------Endrin ketone_______ 20. u
5103-71-9-------alpha~Chlordane______ 98. U
5103-74-2-------gamma-Chlordane______ 98. u
8001-35-2-------Toxaphene 200 u
12674-11-2------Aroclor-1·-=o":"1':"6_______ 98. u
11104-28-2------Aroclor-1221_______ 98. U
11141-16-5------Aroclor-1232 98. U
53469-21-9------Aroclor-1242_______ 98. U
12672-29-6------Aroclor-1248_______ 98. u
11097-69-1-~----Aroclor-1254_-._____ 200 u
11096-82-5------Aroclor-1260________ 200 u
1.00
0
J . I -------.--.-.--~-.~------~-=-:-.. ~ .. .:.::':':' ... ·=-... -...................... ·-· .. -. --,--.................... ---
\
f"kk=t i'!'Sf lfih'itev.
64
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10
PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I
Lab Name: COMPUCHEM LABORATORIES
I SED-3-2MSD
Contract: (2-88)-REVS I -------
Lab Code: COMPO Case No.: 17902. SAS No.: SDG No.: ... 5.-1 ____ _
Matrix: {soil/water) SOIL Lab Sample ID: .... 2.._88 ... 5....,7...,.,0 __ _
Sample wt/vol: Lab File IO:
Level: (low/med)
30.0 (g/mL) L-
LOW
% Moisture: not dee. 18 dee.
Extraction: (SepF/Cont/Sonc) SQHC,
Date Received: 09/30/89
Date Extracted: 10/17/89
Date Analyzed: 10/17/89
GPC Cleanup: {Y/N) ti_ pH: -1...:.2 Dilution Factor: _ ___,l~_ -~P ...... O
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 9.8 U
-319-85-7--------beta-BHC 9.8 U
319-86-8--------delta-BH=c---------9.8 U
58-89-9---------gamma-BHC {Lindane)_-____ 9;9 U
76~44-8-------~-Heptachlor________ 9.8 u
309-00-2--------Aldrin.~----:-:~----9.8 U
1024-57-3-------Heptachlor epoxide 9.8 U
959-98-8--------Endosulfan I -----9.8 U
60-57-1---------Dieldrin 20. U ---------72 -55 -9 -

-

-

-

-

-

-

-

-
4, 4' -DD E _________ 20. U
72-20-8---------Endrin 20. U
33213-65-9------Endosu-=-l~f-an~I=-=I=--------I 20. u
72-54-8---------4,4'-DDD 20. U
1031-07-8-------Endosulf'_a_n_su~l~f~a~t-e_____ 20. U
50-29-3---------4,4'-D~~--------20. U
72-43-5---------Methoxychlor_______ 98. U
53494-70-5------Endrin ketone 20. U
5103-71-9---~---alpha-Chlorda-ne __________________ -_ -_ 98. IU
5103-74-2-------gamma-Chlordane______ 98. IU
8001-35-2-------Toxaphene 200 IU
12674-11-2------Aroclor-l-,:,0-:-l-:-6-------98. IU
11104-28-2------Aroclor-122 l_______ 98. I U
11141-16-5------Aroclor-1232 98. IU
53469-21-9------Aroclor-1242_______ 98. IU
12672-29-6------Aroclor-1248 98. IU
11097-69-1------Aroclor-1254__________ 200 IU
11096-82-5------Aroclor-1260_______ 200 IU
0
--~---·-.. 1---------~------~--~ ~-~~~-1 _ J_ ___ . --
' •
. ·---111, 9tev .
--63'
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CDMPUCHEM
lABORATORIES
CASE NARRATIVE --SIRRINE ENVIRONMENTAL CONSULTANTS
CASE# 17902 SDG# 70
CONTRACT I (2-88)-REVS
Sample Numbers: SL-10-1, SL-11-1, SL-12-1, SL-13-1, SL-14-1,
SL-15-1, SL-16-1, SL-17-1, SL-18-1, SL-19-1, SL-20-1, SL-21-1,
SL-22-1, SL-23-1, SL-24-1, SL-25-1, SL-28-1, SL-29-1, SL-30-1,
SL-30-2
This Case consisted of twenty soil samples analyzed for
volatiles, semi-volatiles, and pesticides/PCBs. The samples
arrived intact in sealed shipping containers on October 4 and 5,
1989 with Chain of custody (COC) Records. Federal Express was the
courier from the client to Compuchem Laboratories, Inc. Due to
limitations in the Formaster software, the sample numbers cannot
exceed nine digits. The prefix "9168-" was deleted from the sample
numbers, and the coc was footnoted with this change. The samples
were logged into compuChem's Laboratory Management System and were
stored at 4°C. The percent.moisture ranged from 3% to 23%, and the
detection limits were elevated to reflect the moisture content.
The pH of sample SL-18-1 was 4.9. Acting in accordance with the
technical guidance from CompuChem's DPO, the lab proceeded with the
analysis of this sample. The pH of the remaining samples ranged
from 5.2 to 7.3 and was within the acceptable range.
VOLATILES:
The samples were analyzed within holding time requirements for
volatiles. The instrument blanks contained low levels of 1-2
Target compound List (TCL) volatiles. With the exception of
VBLKBl, Tentatively Identified Compound (TIC) volatiles were not
detected. VBLKBl contained one. instrument artifact that was
identified-as a siloxane. This is a frequently observed laboratory
artifact and should not be considered an actual sample constituent.
While the peak has been included in the total number of Library
searches, it has not been counted as one of the ten most intense
TIC's requiring a Library Search. The data was reported with
reference to this qualifier.
The samples contained low to high levels of 1-8 TCL volatiles.
The instrument's analytical range was exceeded for toluene in SL-
29-1 (Low Level, undiluted) and SL-30-2 (Medium Level, undiluted).
These samples were re-analyzed, and all compounds were within the
multipoint: SL-29-lRE (Medium Level, undiluted) and SL-30-2DL
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 [phone]
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-----O)MPUCHEM
lABOPATORIES
(Medium Level, 13:1 dilution). Both sets of analyses were reported
for each sample.
The surrogate recovery for dB-Toluene did not meet acceptance
criteria in SL-29-lRE. All of the surrogates met recovery
acceptance criteria for the Low Level analysis. The sample was
then prepared and analyzed twice as a Medium Level Solid. In both
of the Medium Level analyses, dB-Toluene failed recovery acceptance
criteria. We have concluded that the surrogate failure in the
Medium Level analyses was due to a sample matrix effect in
combination with the differences between the purge and trap method
and the methanol extraction procedure. The Low Level and one of
the Medium Level analyses were reported with reference to this
qualifier.
The sample SL-2B-l was analyzed as a Medium Level soil with a
5:1 dilution. One surrogate, dB-Toluene, failed recovery criteria,
and the sample was re-extracted and re-analyzed as an undiluted
Medium Level soil. DB-Toluene failed recovery criteria in the same
manner, and we have concluded that this was due to the sample
matrix. Both sets of data were reported with reference to this
notice. Please note that three TCL volatiles were detected in the
undiluted analysis, and TCL volatiles were not detected in the 5:1
dilution of SL-2B-l (SL-2B~lRE):
The following samples contained 2-10 TIC volatiles:. SL-2B-l,
SL-2B-1RE, SL-29-lRE, SL-30-1, SLJ0-2, and SL-30-2DL. Two
instrument artifacts identified as siioxanes were detected in SL-
29-lRE.
The matrix spike/matrix spike duplicate (MS/MSD) generated
from SL-30-lMS was analyzed as a Medium Level Solid at a 10:1
dilution. As a result, most•of the surrogate and spike recoveries
were diluted below detection limits (except for toluene). We have
included the results from the blank spike (BS) extracted with these
samples to show that the analytical system was in control. The
data was reported with reference to this notice. All criteria were
met for the initial and continuing calibration standards, the
surrogate standards (except where previously noted), and the
internal standards.
SEMI-VOLATILES:
The samples were extracted and analyzed within holding time
requirements for semi-volatiles. The method blank, SBLKBl,
contained a low level of one TCL semi-volatile. The remaining
method blanks did not contain TCLs. All of the method blanks
contained three TIC semi-volatiles. The TICs included blank
contaminants, aldol compounds, and surrogate isomers. The aldol
condensation products could have arisen from in-house acetone or
2
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lABOPATORIES
from the reaction of the sample components with the acetone used in
the extraction procedure. All of the blank contaminants were well
within the contract QA/QC criteria.
With the exception of SL-16-1, the samples contained low to
medium levels of 1-18 TCL semi-volatiles. Although SL-16-1 did not
contain TCLs, the sample was diluted J:l to prevent saturation.of
the detector due to high levels of non-target compounds. A 5:1
dilution was performed on the following samples due to the viscous
nature of the matrix: SL-29-1, SL-30-1, and SL-30-2. All of the
samples contained 1-23 TIC's that included blank contaminants and
aldol compounds. The "X" footnote was used on Form I to indicate
co-elution of two compounds.
The sample SL-28-1 was diluted 10:1. Due to severe matrix
interferences present in this sample, the d12-Chrysene Internal
Standard had a response which varied considerably from the
associated Continuing Calibration Standard responses. This sample
was re-analyzed to confirm the matrix effect, and the initial
results were verified. Depending on the degree of the
interferenc~, surrogate recoveries may also be affected for those
compounds quantitated using the affected Internal standard. one
base/neutral surrogate standard did fail recovery criteria in the
re-analysis (SL-2B-lRE). According to EPA protocol, one acid and
one base/neutral surrogate standard was allowed to fail recovery
criteria. Both analyses were reported with reference to this
qualifier. ·
All criteria were met for the initial and continuing
calibration standards, the surrogate standards and the internal
standards (except where previously mentioned). The MS/MSD
generated from SL-16-1 had three %REC and three %RPO outliers on
Form III. These outliers were for advisory purposes only, and all
other spike recoveries were good.
PESTICIDES/PCBs:
All samples for pesticides/PCBs were extracted and analyzed
within holding time requirements, except the spikes were extracted
outside of holding times. The method blanks and the samples did
not contain TCL pesticides/PCBs. Due to high leve1s·of non-target
compounds, the following dilutions were performed: 20:1 for SL-
30-1 and· 50:1 for SL-30-2. The surrogate recoveries for these
samples were diluted below detection limits, and Form II was
footnoted with a "D".
Several outliers were present in the %D column of the Form
VIII's. These outliers were associated with the two diluted
samples mentioned above, analyses that were not reported, hexane
blanks, and samples that were not included in this Case. In
3
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----OJMPUCHEM
lABOAATORIE.S
addition, outliers were present in the %0 column of the Form IX's.
Because these were associated with INDA and INDB standards that
were run at the end of the sequence, these outliers were acceptable
according to EPA protocol. The surrogate standards had good ·
recoveries for all samples except the two diluted samples.
The MS/MSD generated from SL-10-1 had one %REC and one %RPO
outlier on Form III. These outliers were for advisory purposes
only, and all other spike recoveries were good. The surrogate
standard appears to have been added at twice the usual volume for
the MSD, since the surrogate recovery was approximately twice the
expected concentration. We have not adjusted the reported
recovery. Since there were no target compounds detected in this
sample (other than the spike compounds), there was no effect on the
usability of the data. Note that the DBC surrogate recovery
control limits are advisory only.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and for
completeness, for other than the conditions detailed above.
Release of the data contained in this hard copy data package has
been authorized by the Laboratory Manager or his designee, as
verified by the following signature.
Note: This report is paginated for reference and account-
ability in decreasing numerical sequence.
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET·
SL-10-1
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~70 __
Matrix: ( soil/water) SOIL Lab Sample ID: 291629
Sample wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GH091629B19
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _ll Date Analyzed: lQ/08/89
Column:
----·--·---····
(pack/cap) CAP Dilution Factor: 1.0 ~~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-15-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------li2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27~4---------Bromodichloromethane
78~87-5---------l,2-Dichloropropane
10061-01-5~-----cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene ' 79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7---~---Total Xylenes
.
FORM I VOA
-J.T'MIZ-7a SRIIPLE DRTR SU/1/IRllY
l.
11 u
11 u
11 u
11 u
19 B
5 BJ
6 u
6 u
6 u
6 u
6 u
6 u
11 u
6 u
6 u
ll u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 lJ
6 u
1/87 Rev.
215
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-10-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Mate-ix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: ( low/med) LOW
% Moisture: not dee. _u
Column (pack/cap) CAP
Number TICs found: ___Q
(g/mL) _G_
Lab Sample ID: 291629
Lab File ID: GH091629Bl9
Date Received: 10/04/89
Date Analyzed:-10/08/89
Dilution Factor: ~1~-~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ----==-----=-==-=--===-----==-=----=----=--= ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
-:-Cl?P z-~ SRIIPLE DRTR SLHAAli'r 214
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-11-l
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: S DG No . : ..,_7 O.___
Matrix: ( soil/water) SOIL Lab Sample ID: 291639
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GR0916J9Cl9
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _li Date Analyzed: 10/10/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) Y~LK!i Q
74-87-3---------Chloromethane ll u
74-83-9---------Bromomethane ll u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane ll u
75-09-2---------Methylene Chloride 39 B
67-64-1---------Acetone 51 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------l,l-Dichloroethene 6 u
75-34~3---------1,l-Dichloroethane 6 u
540-59-0--------l,2-Dichloroethene (total)_ 6 u
67-66-J---------Chloroform 6 u
107-06-2--------l,2-Dichloroethane 6 u
78-93-3---------2-Butanone ll u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate ll u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5-~-------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-1,J-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
100-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA l/87 Rev.
-z79112·-z• SRIIPLE DRTR SUIIIIRRV 21J
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-11-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-'70...__
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: ( low/med) LOW
% Moisture: not dee. _u
Column (pack/cap) !:~P
Number TICS found: __o_
(g/mL) G __
Lab Sample ID: ~2L9~16~3L9,_ __ _
Lab .File ID: GR091639Cl9
Date Received: 10/04/89
Date Analyzed: 10/ 10/89
Dilution Factor: ~l~-~0:..._ __
CONCENTRATION UNITS: .
(ug/L or ug/Kg) UG/KG
FORM I VOA-TIC 1/87 Rev.
212
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-12-1
Lab Name: COMPUCHEM LABS contract: 12-88)-REVS
., Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: 70 . .,,,
Matrix: (soil/water) SOIL Lab Sample ID: 291640
Sample wt/vol: 5.0 (g/mL) G __ Lab File ID: GH09l640Bl9
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. -1.Q Date Analyzed: 10/08/89
Column: (pack/cap) CAP Dilution Factor: al~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
'
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11· u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 15 B
67-64-1---------Acetone 4 BJ
75-15-0---------carbon Disulfide -6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
_78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4-~------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane_·_ 6 u
108-88-3----~---Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
Z 7.911:T 711 SRIIPLE DRTR SUlflfRlllV -211
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-12-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
SOIL• Matrix: (soil/water)
Sample wt/vol: s.J' (g/mL) _G_
Level: ( low/med) LOW
% Moisture: not dee. --1Q
Column (pack/cap) CAP
Number TICs found: _Q
CAS NUMBER COMPOUND NAME
,
Lab sample ID: 291640
Lab File ID: GH091640Bl9
Date Received: 10/04/89
Date Analyzed: 10/08/89
Dilution Factor: .1~-~o __ _
CONCENTRATION UNITS:
[uq/L or ug/Kg) UG/KG
RT EST. CONC. Q
FORM I VOA-TIC l/87 Rev.
--------i.711#12--:--n,·SRIIP'LE DRT.R ..... ·-.. . ---" . --·-------·---. . ·-SUlllfR/lY 218
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-lJ-1
Lab Name: COMPUCHEM LABS contract: (2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~7~0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 29164 l
Sample wt/vol: s.o (g/mL) G __ Lab File ID: GH091641B19
Level: (low/med) LOW Date Received: 10/04/89
\ Moisture: not dee. _u Date Analyzed: 10/08/89
Column: (pack/cap) CAP Dilution Factor: ~l~.o~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-J---------Chloromethane lJ u
74-83-9---------Bromomethane lJ u
75-01-4---------Vinyl Chloride 13 u
75-00-J---------Chloroethane lJ u
75-09-2---------Methylene Chloride 27 B
67-64-1---------Acetone lJ u
75-15-o----~----carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-J4-J---------l,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-J---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone lJ u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate lJ u
75-27-4---------Bromodichloromethane 6 u
78-87-s----~----l,2~Dichloropropane 6 u
10061-01-s------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone lJ u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
289
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
EPA SAMPLE NO.
SL-13-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~7~0 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: ( low/med) LOW
% Moisture: not dee. ~
Column (pack/cap} !:Ali!
Number TICs found: ____Q.
_G_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291641
GH091641B19
10/04/89
10/08/89
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
----.. -r-7$1112-79 SRIIPLE DRTR SlHUfRIIV 288
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-14-1
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : 70
Matrix: (soil/water) SOIL Lab sample IO: 291642
Sample wt/vol: 5.0 (g/mL) _G_ Lab File IO: GH091642Bl9
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _l.1. Date Analyzed: 10/Q!j/89
Column: (pack/cap) CAP Dilution Factor: ~i~-~o __ _
-----
CAS NO. · COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
.
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloro~thane
75-09-2---------Hethylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroetliane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3~--------2-Butanone
71-55-6--~------l,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
·71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
---=--~ r7SHl2 78 SRIIPL E DRTR SUll/ltRll'Y. -·
Q
12 u
12 u
12 u
12 u
27 B
12 u
6 u
6 u
6 u
6 u
6 u
6 u
12 u
6 u
6 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
.6 u
12 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
287
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS'
Lab Name : COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-14-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~7=0 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G __
Level: (low/med) LOW
% Moisture: not dee. _ll
Column (pack/cap) CAP
Number TICs found: __Q_
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291642
~HQ9l642B19
10/04/89
lQ/08l82
l.' 0
RT EST. CONC. Q
================ =----=------===-----=----=-= ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
IZ!IBZ--79-SRIIPLE DRTR SUIIIIRIIY--286
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-15-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .._7,._0 __
Matrix: (soil/water) SOIL Lab Sample ID: 291643
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH091643Cl9
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ~ Date Analyzed: 10/09/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) \,!G/!(;G Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 31 B
67-64-1---------Acetone 7 BJ
75-15-0---------carbon Disulfide 6 u
75~35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---~-----1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1O0-1O-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
1O8-88-3--------Toluene 6 u
1O8-9O-7--------Chlorobenzene 6 u
1OO-41-4--------Ethylbenzene 6. u
1OO-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA . 1/87 Rev.
285
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2-88}-REVS
EPA SAMPLE NO.
SL-15-1
Lab Code: COMPU Case No.: 17902 SAS No.: S 0G No . : ..:.;7 o.___
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) _G_
Level: ( low/med) LOW
% Moisture: not dee.
Column (pack/cap) ~cA..._P __
Number TICs found: __Q_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291643
GH09164JC19
10/04/89
10/09/89
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q -=-==-=-------== ----=-=----==--=-------===-= ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
·--···-~ --·----·. . --··---·-
- -.;;ga.::-;:,s· .. .. US JI 7'-SRlfPLE DRTR SS~VIIHBHlf.illilllfY-:: 284
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-16-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-7"0 __
Matdx: ( soil/water) SOIL Lab Sample ID: 291644
Sample wt/vol: s.o (g/mL) ~ Lab File ID: GH091644Cl9
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ___u Date Analyzed: 10/09/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/~!;i Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 25 B
67-64-1---------Acetone 7 BJ
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone ll u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
1os-os-4--------vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 5· u
10061-01-s------cis-1,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
19-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
28J
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
EPA SAMPLE NO.
SL-16-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .:..7"'-0 __
Matrix: (soi 1/wa ter j SOIL
Sample wt/vol: 5.0
Level: (low/med) !,QW
t Moisture: not dee. _.ll
Column (pack/cap} CAP
Number TICS found: _Q
(g/mL) G __
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: ..
(ug/L or ug/Kg) UG/KG
291644
GH091644Cl9
10/04/89
10/09/89
1.Q
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== =-=------=---=====
FORM I VOA-TIC 1/87 Rev.
-1·7gt12. 71T SRIIPLE DRTR SUIIIHll/nr 282
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. lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-17-l
Lab Name: COMPUCHEM LABS Contract: <2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7-"0 __
Matt"ix: ( soil/water) SOIL Lab Sample ID: ~2~9~1~6~4~5:.__ __ _
Sample wt/vol: s.o { g/mL) _G_ Lab File ID: GH091645Cl9
Leve 1: {low/med) LOW Date Received: 10/04/89
i Moisture: not dee. ~ Date Analyzed: 10/09/89
Column: {pack/cap) CAP Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane ll u
75-09-2---------Methylene Chloride 22 B
67-64-1---------Acetone 11 B
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,l-Dichloroethene 5 u
75-34-3---------1,l-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone ll u
71-55-6---------1,l,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate ll u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-s------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------l,l,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
1s-2·s-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone ll u
127~18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
--~?flB2 78 SRIIPLE DRTR SUlllfRRV 281
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEH LABS contract: 12-881-REVS
EPA SAMPLE NO.
SL-17-l
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: ~7~0 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. ---8.
Column (pack/cap) !:11.P
Number TICs found: __Q_
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or uq/Kg) UG/KG
291645
GH091645Cl9
10/04/89
10/09/89
1' Q
RT EST. CONC. Q
================ ========================-=== ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
------. -------. --. ' .. --,. -. 2BB ·
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lA EPA SAMPLE !10.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-18-l
Lab Name: COMPUCHEM LABS contract: {2-88)-REVS
Lab Code: COMPU Case No.: l 7902 SAS No.: SDG No.: .,_7c,.0 __
Matdx: ( soil/water) SOIL Lab Sample ID: 291646
Sample wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GH091646Cl9
Level: (low/med) LOW Date Received: 10/04/89
i Moisture: not dee. -1Q Date Analyzed: 10/09/89
Column: {pack/cap) CAP Dilution Factor: -i~-=o __ _
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/KG Q
.
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2--------~Methylene Chloride 32 B
67-64-1---------Acetone 14 B
75-15-0----~----carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0---~----l,2-Dichloroethene (total)_ 6 u
67-66-3---------ChlorofOI'111 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
1s-2s-2---------BromofoI111 6 u
108-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_· _ 6 u
108-88-3~-------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA l/87 Rev.
----· . -.... . -' -.,;~ -., ... ' . romrt: E ~0~11i.;r,J:'4•&,:;;;··-Ji.&B•••ec=====~ J 99 -
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: /2-881-REVS
E!,A SAMPLE NO.
SL-18-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7.:,;0 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G __
Level: ( low/med) LOW
% Moisture: not dee. --1.Q
Column (pack/cap) CAP
Number TICs found: __Q
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291646
GH091646Cl9
10/04/89
10/09/89
1.0
RT EST. CONC. Q
================ =========================-== ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
s I .. -. . _,,. -. ..-• _: • I ~ • • • a .. , .. ___ _
l 98
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-19-1
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7:,.0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 291647
Sample wt/vol: 5,0 (g/mL) _G_ Lab File ID: GH091647Cl9
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _li Date Analyzed: 10/09/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/l<g) ui;;11<;i;; Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 34 B
67-64-1---------Acetone 20 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-1---------2-Butanone 12 u
71-55-6--~------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-1,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-1,3-Dichloropropene __ 6 u
75-25-2---------Bromoform' 6 u
100-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 U,
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
133'0-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
-----------·-· ----. ·-·-"'-•-. , .. -. ,. _IJRTa, -. -' ---l9-7
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
EPA SAMPLE NO.
SL-19-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: ( low/med) LOW
% Moisture: not dee. _u
Column (pack/cap) ~AP
Number TICs found: ___.Q.
( g/mL) _G_
Lab Sample ID: 291647
Lab File ID: GH091647Cl9
Date Received: 10/04/89
Date Analyzed: 10/09/89
Dilution Factor: al~-~O __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q =-===-----------============================ ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
. . . ' . . ' --J 96
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-,-20-1
lab Name: COMPUCHEM LABS Contract: /2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ____ SDG No.: 70 ~--
Matrix: ( soil/water) SOIL Lab Sample ID: 291648
Silmple wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GH091648Cl9
Level: ( low/med) LOW Date Received: 10/04/89
l Moisture: not dee. __ll Date Analyzed: 10/09/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) QG/IS~ Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 20 B
67~64-1---------Acetone 11 BJ
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------Carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--~-----Dibromochloromethane 6 U.
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1os-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 2 J
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
-----------·----. --. -. -. .. . -.. 195
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-20-1
Lab Code: COMPU case No.: 17902 SAS No.: S DG No . : .,_7 0,.___
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. ____li
Column (pack/cap) C~P
Number TICs found: __a_
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
291648
GH091648C19
10/04/89
10/09/89
1.0
RT EST. CONC. Q
================ ============================ ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
-----. ----. ---~--..... -~--------.
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-21-1
LAb Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-7,,_0 __
Mat~ix: (soil/water) SOIL Lab Sample ID: 291649
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH091649Cl9
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _]_ Date Analyzed: 10/09/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!;i(l';!;i Q
74-87-J---------Chloromethane 10 u
74-8J-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-J---------Chloroethane 10 u
75-09-2---------Methylene Chloride 15 B
67-64-1---------Acetone 15 B .
75-15-0---------carbon Disulfide 5 u
75-)5-4---------1,1-Dichloroethene 5 u
75-J4-J---------l,l-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-J---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-9J-J---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-2)-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-oichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2-~-~-----Benzene · 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
100-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
100-aa-J--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7--~----Total Xylenes 5 u
FORM I VOA 1/87 Rev.
AZ& V Ii L6 .OIITR 51" 193
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VOLATILE ORGANICS .ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-21-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 291649
Sample wt/vol: 5.0 ( g/mL) G __ Lab File ID: GH091649Cl9
Level: (low/med) LOW Date Received: 10/04/89
\ Moisture: not dee. __l Date Analyzed: 10/09/89
Column (pack/cap) CAP Dilution Factor: ~i~-~o __ _
Number TICs found: __Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG •
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ====-=====--====---=====-=== ======== ============= =====
FORM I VOA-TIC 1/87 Re','.,
---~ ---------··--· ---C50RPF. . -. --~ ,. . . . -• I -...:. __ J S,2
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lA EPA SAMPLE NO.
VOLATILE ORGANICS AN.ALYSIS DATA SHEET
SL-i2-l
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: ----SDG No.: .,_7_,.0 __
Matrix: (soil/water) SOIL Lab Sample ID: 292316
Sample wt/vol: 5.0 ( g/mL) G __ Lab File ID: GH092316Al9
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. __u Date Analyzed: 10/13/82
Column: (pack/cap) CAP Dilution Factor: ~l~-~o __ _
CONCENTRATION UNITS:
CASNO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 31 B
67-64-1---------Acetone 18 B
75-15-0---------carbon Disulfide ·5 u
75-35-4---------1,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform l J
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87~5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-O1-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1O0-1O-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
1O8-88-3--------Toluene 6 u
1O8-9O-7--------Chlorobenzene 6 u
1OO-41-4--------Ethylbenzene 6 u
1OO-42-5--------Styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
-------·---. -~--------SJl■FC.S: 0 --· -191
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: /2-88)-REVS
EPA SAMPLE NO.
SL-22-l
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: ~79~-
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: ( low/med) LOW
\ Moisture: not dee. _u
Column (pack/cap) C~P
Number TICS found: __Q.
_G_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
292)16
GH092Jl6Al9
10/05/89
10/lJ/89
l.Q
CAS NUMBER COMPOUND NAME RT EST. CONC. Q '
FORM I VOA-TIC l/87 Rev.
------------. -. ----. . . -• 0$79 -... --~I • -I • -19B
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-2J-l
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: _,_7:,,.0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 292315
Sample wt/vol: 5.0 ( g/mL) G __ Lab File ID: GH092 Jl5Al 9
Level: (low/med) LOW Date Received: 10/05/89
\ Moisture: not dee. _u Date Analyzed: lO/lJ/89
Column: (pack/cap) CAP Dilution Factor: ~i~-:,,.0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2------~--Methylene Chloride 20 B
67-64-1---------Acetone 26 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 2 J
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5--------~carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-s------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1os-10-i--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s-~------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA l/87 Rev.
, ___ ---::-::, -----=-:;.__----;;;:--_ ----· --= D9,U ---. . -. , ..
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88l-REVS
EPA SAMPLE NO.
SL-23-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-7_..0 __
Matrix: ( soil/water) SOIL
sample wt/vol: 5.0
Level: ( low/med) LOW
% Moisture: not dee. _li
Column (pack/cap) CAP
Number TICs found: ___Q_
( g/mL) _G_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
292315
GH092Jl5Al9
10/05/89
10/lJ/89
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ========================-=== ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
---·· -·--...... ~-... ----.....--. ,, -.. -' JBS
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-24-1
Lab Name: COHPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 292321
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH092321Al9
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. __ll Date Analyzed: 10/lJ/89
Column: (pack/cap) CAP Dilution Factor: al~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG·
74-87-3---~-----Chloromethane 12
74-83-9---------Bromomethane 12
75-01-4---------Vinyl Chloride 12
75-00-3---------Chloroethane 12
75-09-2---------Methylene Chloride 23
67-64-1---------Acetone 25
75-15-0---------carbon Disulfide 6
75-35-4---------1,1-Dichloroethene 6
75-34-3---------1,1-Dichloroethane 6
540-59-0---~----l,2-Dichloroethene (total)_ 6
67-66-3---------Chloroform 6
107-06-2--------1,2-Dichloroethane 6
78-93-3~--------2-Butanone 12
71-55-6---------1,1,1-Trichloroethane 6
56-23-5---------carbon Tetrachloride 6
108-05-4--------Vinyl Acetate 12
75-27-4---------Bromodichloromethane 6
~•-s1-s---------1,2-Dichloropropane 6
•051-01-s------cis-l,3-Dichloropropene 6
.. 01-6---------Trichloroethene 6
4-48-1--------Dibromochloromethane 6
1~-oo-s---------1,1,2-Trichloroethane 6
71-43-2---------Benzene 6
10061-02-6------Trans-l,J-Dichloropropene __ 6
75-25-2---------Bromoform 6
108-10-1--------4-Methyl-2-Pentanone 12
591-78-6--------2-Hexanone 12
127-18-4--------Tetrachloroethene 6
79-34-5---------1,1,2,2-Tetrachloroethane __ 6
100-ss-J--------Toluene 6
108-90-7--------Chlorobenzene 6
100-41-4--------Ethylbenzene 6
100-42-s--------styrene 6
1330-20-7-------Total Xylenes 6
FORM I VOA
--------·--. ---· • A--• -J'4• ., __ , .. -
Q
u
u
u u
B
B u u
u
u
u u
u
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u u
u
u
u
u
u
u
u
u
u u
u
u u u u
u
u
u
1/87 Rev.
187
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-BBl-REVS
EPA SAMPLE NO.
SL-24-l
Lab Code: COMPU Case No.: l 7902 SAS No.: SDG No.: .._7 .. o __
Matrix: ( soil/water} SOIL
Sample _wt/vol: 5.0 (g/mL}
Level: (low/med} LOW
' Moisture: not dee. _li
Column (pack/cap} CAP
Number TICS found: __Q_
_G_
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/KG
292321
GH092J21Al9
10/05/89
10/lJ/89
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ -----=-----==-=----=----=--= ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
·------··-_._ ·---,-·~---.. -_, -,,_ 186
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lA EPA SAMPLE N'O.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-25-1
Lab N'ame: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPU Case No. : 17902 SAS No.: ____ SDG No.: 70 ~--
Matrix: ( soil/water} SOIL Lab Sample ID: 292322
Sample wt/vol: 5.0 (g/mL} _G_ Lab File ID: GR092J22B19
Level: ( low/med) LOW Date Received: 10/05/89
i Moisture: not dee. __ll Date Analyzed: 10/B/89
Column: (pack/cap) CAP Dilution Factor: ~i~•i9 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 9 B
67-64-1---------Acetone 13 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total}_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------l,2-Dichloropropane 6 u
10061-01-s------cis-1,J-Oichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------0ibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 U.
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2-~-------Bromotorm 6 u
1os-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
---·-----· -----·-· ·----·-. .--.. --,; -18!5
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-25-l
Lab Code: COMPU ·case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water} SOIL
Sample wt/vol: 5. 0 (g/mL} G __
Level: (low/med} ~LO~W,,__
% Moisture: not dee. _ll
Column {pack/cap} ~CQALP __
Number TICs found: ___Q_
Lab Sample_ ID: 292322
Lab File ID: GR092322Bl9
Date Received: 10/05/89
Date Analyzed: 101 U/89
Dilution Factor: .1~,~0 __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ --==-=--=--=-=-------------=========-------==a---=====
FORM I VOA-TIC l/87 Rev.
-------------' . -... . ---. --.. -~--... -
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-28-1
Lab Name: COMPUCHEM LABS contract: (2-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 292320
sample wt/vol: 4.0 ( g/mL) _G_ Lab File ID: CN09iP~OA12
Level: (low/med) MED Date Received: 10/05/89
% Moisture: not dee. _ll Date Analyzed: lQ/14189
·Column: (pack/cap) CAP Dilution Factor: ~5~,Q~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 7200 u
74-83-9---------Bromomethane 7200 u
75-01-4---------Vinyl Chloride 7200 u
75-00-3---------Chloroethane 7200 u
75-09-2---------Methylene Chloride 3600 u
67-64-1---------Acetone 7200 u
1s~1s-o---------carbon Disulfide 3600 u
75-35-4---------1,1-Dichloroethene 3600 u
75-34-3---------1,1-Dichloroethane 3600 u
540-59-0--------1,2-Dichloroethene (total) __ 3600 u
67-66-3---------Chloroform 3600 u
107-06-2--------1,2-Dichloroethane 3600 u
78-93-3---------2-Butanone 7200 u
71-55-6---------1,1,1-Trichloroethane 3600 u
56-23-5---------carbon Tetrachloride 3600 u
1oa-os-4--------vinyl Acetate 7200 u
75-27-4---------Bromodichloromethane 3600 u
78-87-5---------1,2-Dichloropropane 3600 u
10061-01-S------cis-l,3-Dichloropropene 3600 u
79-01-6---------Trichloroethene 3600 u
124-48-1--------Dibromochloromethane 3600 u
79-00-5---------1,1,2-Trichloroethana 3600 u
71-43-2---------Benzena 3600 u
10061-02-6------Trans-1,J-Dichloropropene __ 3600 u
1s-2s-2---------Bromoform 3600 u
1os-10-1--------4-Methyl-2-Pentanone 7200 u
591-78-6--------2-Hexanone 7200 u
127-18-4--------Tetrachloroethene 3600 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 3600 u
108-88-3--------Toluene 3600 u
108-90-7--------Chlorobenzene 3600 u
100-41-4--------Ethylbenzene 3600 u
100-42-s--------styrena 3600 u
1330-20-7-------Total Xylenes 3600 u
'
FORM I VOA 1/87 Rev.
Mr --p . 183
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-28-1
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: -'-'70,,___
Matrix: ( soil/water) SOIL Lab Sample ID: 292320
Sample wt/vol: 4.0 (g/mL) I,__ Lab File ID: CN092320Al2
Level: ( low/med) MED Date Received: 10/05/89
% Moisture: not dee. _u Date Analyzed: 10/14/89
Column (pack/cap) CAI! Dilution Factor: 5.0
Number TICs found: _iQ
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kgl UG/KG
RT EST. CONC.
-=----==-=--=-== ============================ ======== =============
l. UNKNOWN 13.60 5700
2. 6236-88-0 CYCLOHEXANE,l-ETHYL-4-METHYL 14.12 5700
J • UNKNOWN 14.75 11000
4. ~NKNOWN 14. 99 · 6500
5. UNKNOWN 15.50 17000
6. UNKNOWN 15.94 5700
7. UNKNOWN CYCLIC HYDROCARBON 16.14 14000
8. 124-18-5 DECANE 16.44 38000
9. 17302-28-2 NONANE,2,6-DIMETHYL-17.00 12000
10. UNKNOWN SUBST. CYCLOHEXANE 17. 35 10000
FORM I VOA-TIC
-------------. ---. ' . •• • - • -~ ~.-., I • -., -0110,:
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1/87 Rev.
-182
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-28-lRE
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: -'-7.,.0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 292J20
Sample wt/vol: 4.0 (g/mL) _G __ Lab File ID: CR092J20Al2
Level: (low/med) MED Date Received: 10/05/89
t Moisture: not dee. ___ll Date Analyzed: 10/15/89
Column: (pack/cap) CAP • Dilution Factor: l.O
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!:i/K~ Q
74-87-J---------Chloromethane 1400 u
74-SJ-9---------Bromomethane 1400 u
75-01-4---------vinyl Chloride 1400 u
75-00-J---------Chloroethane 1400 u
75-09-2---------Methylene Chloride 720 u
67-64-1---------Acetone 1400 u
75-15-0---------carbon Disulfide 720 u
75-JS-4---------1,1-Dichloroethene 720 u
75-34-3---------1,1-Dichloroethane 1400
540-59-0--------1,2-Dichloroethene (total)_ 720 u
67-66-3---------Chloroform 720 u
107-06-2--------1,2-Dichloroethane 720 u
78-93-3---------2-Butanone 1400 u
71-55-6---------1,1,1-Trichloroethane 470 J
56-23-5---------carbon Tetrachloride 720 u
108-05-4--------Vinyl Acetate 1400 · u
75-27-4---------Bromodichloromethane 720 u
78-87-5---------1,2-Dichloropropane 720 u
10061-01-s------cis-1,J-Dichloropropene 720 u
79-01-6---------Trichloroethene 720 u
124-48-1--------Dibromochloromethane 720 u
79-00-5-----~---l,l,2-Trichloroethane 720 u
71-43-2---------Benzene 720 u
10061-02-6------Trans-l,3-Dichloropropene __ 720 u
75-25-2---------Bromoform 720 · u
100-10-1--------4-Methyl-2-Pentanone 1400 u
591-78-6--------2-Hexanone 1400 u
127-18-4--------Tetrachloroethene 720 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 720 u
108-88-3--------Toluene 880
108-90-7--------Chlorobenzene 720 u
100-41-4--------Ethylbenzene 720 u
100-42-s--------styrene 720 u
1330-20-7-------Total Xylenes 720 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-28-lRE
Lab Code: COMPU Case No.: 17902 SAS No.: S DG No . : ..,_7-"0 __
Mate-ix: ( soil/water) SOIL Lab Sample ID: 292320
Sample wt/vol: 4.0 (g/mL) _G_ Lab File ID: CR092320Al2
Level: (low/med) MED Date Received: 10/05/89
% Moisture: not dee. _u Date Analyzed: 10/15/89
Column (pack/cap) Cl,P Dilution Factor: 1.0
Number TICs found: _l..Q.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST .. CONC.
----==----===-== =--m=-=------=--------===---======== =============
1. TRANS ETHYL METHYL CYCLOHEXA 13.60 7600
2. 111-84-2 NONANE 13.89 14000
3 . TRANS ETHYL METHYL CYCLOHEXA 14.15 10000
4. UNKNOWN 14.82 20000
5. UNKNOWN 15.05 13000
6. UNKNOWN HYDROCARBON 15.59 39000
7. UNKNOWN 16.00 7500
8. 1678-82-6 CYCLOHEXANE,l-METHYL-4-(1-ME 16.24 19000
9. 124-18-5 DECANE 16.54 110000
10. 17302-28-2 NONANE,2,6-DIMETHYL-17.10 22000·
FORM I VOA-TIC
--------·--. -. ----. -iii• · • e:ra:: nw•v:nr --• -- -•• • -' -• .• • I • •
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1/87 Rev.
JBB
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-29-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: .,_7,,_0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 292)19
Sample wt/vol: 5.0 ( g/mL) ~ Lab File ID: GH092Jl9Al9
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. _u Date Analyzed: 10/lJ/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !.!!al~!. Q
74-87-J---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 44 8
67-64-1---------Acetone 51 8
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-J4-3---------l,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 1 J
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5--~------l,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
100-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 2 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 940 E
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 7
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 34
FORM I VOA 1/87 Rev.
, --~-- --• .,--,:• .....,r -;
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88\-REVS
EPA SAMPLE NO.
SL-29-l
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: ~79~-
Matrix: (soil/water} SOIL
Sample wt/vol: 5.0 (g/mL}
Level: ( low/med} LOW
% Moisture: not dee. _ll
Column (pack/cap} CAP
Number TICs found: __Q_
_G_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/KG
292319
GH092Jl9Al9
10/05/89
10/13/89
1,0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q =====--========= ==-----=---=--=--------===== ======== ============= ~====
FORM I VOA-TIC 1/87 Rev.
-·-. -. --· ---• _ _,._ -• -• I "=-f" •"'-' ~ p 178
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-29-lRE
Lab Name: COMPUCHEM LABS contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-70,.___
Matrix: ( soil/water) SOIL Lab sample ID: 292)19
sample wt/vol: 4,0 (g/mL) L-Lab File ID: CR092Jl9Al2
Level: ( low/med) MED Date Received: 10/05/89
% Moisture: not dee. _ll Date Analyied: 10/15/89
Column: (pack/cap) ~Ai! Dilution Factor: al~,~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 1400 u
74-83-9---------Bromomethane 1400 u
75-01-4---------Vinyl Chloride 1400 u
75-0Q-J----~----Chloroethane 1400 u
75-09-2-~-------Methylene Chloride 720 u
67-64-1---------Acetone 1400 u
75-15-o---------carbon Disulfide 720 u
75-35-4---------1,1-Dichloroethene 720 u
75-34-3---------1,1-Dichloroethane 720 u
540-59-0--------1,2-Dichloroethene (total)_ 720 u
67-66-3---------Chloroform 720 u
107-06-2--------1,2-Dichloroethane 720 u
78-93-3---------2-Butanone 1400 u
71-55-6---------1,1,1-Trichloroethane 720 u
56-23-5---------carbon Tetrachloride 720 u
108-05-4--------Vinyl Acetate 1400 u
75-27-4---------Bromodichloromethane 720 u
78-87-5---------1,2-Dichloropropane 720 u
10061-01-5------cis-l,3-Dichloropropene 720 u
79-01-6---------Trichloroethene 720 u
124-48-1--------Dibromochloromethane 720 u
79-00-s---------1,1,2-Trichloroethane 720 u
71-43-2---------Benzene 720 u
10061-02-6------Trans-l,3-Dichloropropene __ 720 u
75-25-2---------Bromoform 720 0 u
1os-10-1--------4-Methyl-2-Pentanone 1400 u
591-78-6--------2-Hexanone 1400 u
127-18-4--------Tetrachloroethene 720 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 720 u
1os-ss-J--------Toluene 3100
108-90-7--------Chlorobenzene 720 u
100-41-4--------Ethylbenzene 720 u
100-42-s--------styrene 720 u
1330-20-1-------Total Xylene• 170 J
FORM I VOA 1/87 Rev.
. J77
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
L,ab Name: COMPUCHEM LABS Contract: (2-881-REVS
EPA SAMPLE NO.
SL-29-lRE
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL
53mple wt/vol: 4.0 (g/mL) _G_
Level: (low/med) uME...,.D __
% Moisture: not dee. --1.l
Column (pack/cap) %CMA~P __
Number TICs found: ~
CAS NUMBER COMPOUND NAME
Lab Sample ID: 292319
Lab File ID: CR092319Al2
Date Received: 10/05/89
Date Analyzed: lOilS/89
Dilution Factor: ~i~·~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGiKG
RT EST. CONC. Q
================ =====•======m=============== ======== ============= •====
l. INSTRUMENT ARTIFACT 11. 82 1000 BJ
2. INSTRUMENT ARTIFACT 16.34 46000 BJ
FORM I VOA-TIC 1/87 Rev.
176
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VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-J0-1
Lab Name: COMPUCHEM LABS Contract: 12-88)-R~VS
Lab Code: COMPU Case No.: 17902 SAS No.: ----SDG No.: 70 -'--"'--
Matrix: ( soil/water) SOIL Lab Sample ID: 292317 ===----
Sample wt/vol: 4.0 (g/mL) _G_ Lab File ID: CR092Jl7Cl2
Level: (low/med) MED Date Received: . 10/05/89
% Moisture: not dee. _ll Date Analyzed: 10/14/89
Column: (pack/cap )1 CAP Dilution Factor: =l=O __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 15000
74-83-9---------Bromomethane 15000
75-01-4---------Vinyl Chloride 15000
75-00-3---------Chloroethane 15000
75-09-2---------Methylene Chloride 7400
67-64-1---------Acetone . 15000
75-15-o---------carbon Disulfide 7400
75735-4---------1,l-Dichloroethene 7400
75-34-3---------1,1-Dichloroethane 7400
540-59-0--------1,2-Dichloroethene (total)_ 7400
67-66-3---------Chloroform 7400
107-06-2--------1,2-Dichloroethane 7400
78-93-3---------2-Butanone 15000
71-55-6---------1,1,1-Trichloroethane 7400
56-23-5---------carbon Tetrachloride 7400
108-05-4--------Vinyl Acetate 15000
75-27-4---~-----Bromodichloromethane 7400
78-87-5---------1,2-Dichloropropane 7400
10061-01-s------cis-l,3-Dichloropropene .7400
79-01-6---------Trichloroethene 7400
124-48-1--------Dibromochloromethane 7400
79-00-s---------1,1,2-Trichloroethane 7400
71-43-2---.------Benzene 7400
10061-02-6------Trans-l,3-Dichloropropene __ 7400
75-25-2---------Bromoform 7400
1os-10-1--------4-Methyl-2-Pentanone 15000
591-78-6--------2-Hexanone 15000
127-18-4--------Tet~achloroethene 7400
79-34-5---------1,1,2,2-Tetrachloroethane __ 7400
108-88-3--~-----Toluene 200000
108-90~7--------Chlorobenzene 7400
100-41-4--------Ethylbenzene 7400
100-42-s--------styrene 7400
1330-20-7-------Total Xylenes 1600
FORM I VOA
Q
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1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
EPA SAMPLE NO.
SL-J0-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~70~-
Matrix: ( soil/water) SOIL
Sample wt/vol: 4.0 (g/mL) _G_
Level: ( low/med) MED
% Moisture: not dee. ~
Column (pack/cap) CAP
Number TICs found: _-2
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
292)17
CR092Jl 7Cl2
10/05/89
10/14/89
10
CONC. Q
================ ============================ ======== =======::====== =====
1. UNKNOWN 14.79 10000 J
2. UNKNOWN 15.55 21000 J
J. 1)837-67-7 M-MENTHANE,(lS,JS)-(+)-16.15 16000 J
4. 124-18-5 DECANE 16.49 46000 J
5. ·UNKNOWN HYDROCARBON 17.05 12000 J
FORM I VOA-TIC 1/87 Rev.
-----·-. . . ----·-• c...·_J 74 -
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-30-2
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-70,.___
Matrix: ( soil/water) SOIL Lab Sample ID: 292318
Sample wt/vol: 4.0 (g/mL) g_ Lab File ID: CN'092318B12
Leve 1: ( low/med) MED Date Received: 10/05/89
' Moisture: not dee. --1.2. Date Analyzed: 10/13/89
Column: (pack/cap) CAf Dilution Factor: _1~,9~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 1400 u
74-83-9---------Bromomethane 1400 u
75-01-4-------~-vinyl Chloride 1400 u
75-00-3---------Chloroethane 1400 u
75-09-2---------Methylene Chloride 610 BJ
67-64-1-~-------Acetone 1400 u
75-15-o---------carbon Disulfide 710 u
75-35-4---------1,l-Dichloroethene 710 u
75-34-3---------l,l-Dichloroethane 340 J
540-59-0--------1,2-Dichloroethene (total)_ 710 u
67-66-3---------Chloroform 710 u
107-06-2--------l,2-Dichloroethane 710 u
78-93-3---------2-Butanone 1400 u
71-55-6---------1,l,l-Trichloroethane 1400
56-23-5---------carbon Tetrachloride 710 u
108-05-4--------Vinyl Acetate 1400 u
75-27-4---------Bromodichloromethane 710 u
78-87-5---------1,2-Dichloropropane 710 u
10061-0l-5------cis-l,J-Dichloropropene 710 u
'79-01-6---------Trichloroethene 440 J
124-48-1--------Dibromochloromethane 710 u
79-oo-s~--------1,1,2-Trichloroethane 710 u
71-43-2-~-------Benzene 710 u
10061-02-6------Trana-l,J-Dichloropropene_· __ 710 u
75-25-2---------Bromoform 710 u
1oe-10-1--------4~Methyl~2-Pentanone 1400 u
591-78-6--------2-Hexanone 1400 u
127-18-4--------Tetrachloroethene 1200
79-34-5---------1,l,2,2-Tetrachloroethane __ 710 u
108-88-3--------Toluene 100000 E
108-90-7--------Chlorobenzene 710 u
100-41-4--------Ethylbenzene 410 J
100-42-5--------styrene 710 u
1330-20-7-------Total Xylenes 2100
FORM I VOA 1/87 Rev.
o,ar11~sa,•-•••~►lliEs=::::.:..-173
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lE EPA SAMPLE NO.
VOLATILE.ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-30-2
Lab Name: COMPUCHEM,LABS contract: (2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ___ SDG No.: ~7=0 __
Matrix: ( soil/water) SOIL Lab Sample ID: -2~92-J~l~B~---
sample wt/vol: 4,0 (g/mL) _G_ Lab File ID: CN092318Bl2
Level: (low/med) MED Date Received: 10/05/89
i Moisture: not dee. _l..2. Date Analyzed: 10/13/89
Column (pack/cap) CAP Dilution Factor: _1~,o~--
Number TICS found: -1..Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ============================ ======== ============= =====
1. 111-84-2 NONANE 13.89 7400 J
2 . 6236-88-0 CYCLOHEXANE,l-ETHYL-4-HETHYL 14 .15 6700 J
3 . UNKNOWN 14.77 10000 J
4. UNKNOWN 15.00 8100 J
5. UNKNOWN 15.55 21000 J
6. UNKNOWN 16.15 4400 J
7. 124-18-5 DECANE 16.49 61000 J
8. UNKNOWN 16.82 3100 J
9. 62016-33-5 OCTANE,2,3,6-TRIMETHYL-17.04 20000 J
10. 7058-0l-7 CYCLOHEXANE,(1-METHYLPROPYL) 17.40 7100 J
FORM I VOA-TIC 1/87 Rev.
-----------------·-· ----., -. ---. .. ...... . . . --. -. ---J72
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VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
SL-J0-2DL
Lab Name: COMPUCHEM LABS contract: 12-88}-REVS
Li'lb Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Mat~ix: (soil/water) SOIL Lab Sample ID: 292318
Sample wt/vol: 4.0 (g/mL) L__ Lab File ID: CJR92Jl8Cl2
Level: ( low/med) MED Date Received: 10/05/89
% Moisture: not dee. _li
Column: (pack/cap) CAP
Date Analyzed: lO/U/89
Dilution Factor: ~l~J __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 18000
74-83-9---------Bromomethane 18000
75-01-4---------Vinyl Chloride 18000
75-00-3---------Chloroethane 18000
75-09-2---------Methylene Chloride 8900
67-64-1---------Acetone 18000
75-15-0---------carbon Disulfide 8900
75-35-4---------1,1-Dichloroethene 8900
75-34-3---------1,1-Dichloroethane 8900
540-59-0--------1,2-Dichloroethene (total)_ 8900
67-66-3---------Chloroform 8900
107-06-2--------1,2-Dichloroethane 8900
78-93-3---------2-Butanone 18000
71-55-6---------1,1,1-Trichloroethane 8900
56-23-5---------carbon Tetrachloride 8900
108-05-4--------Vinyl Acetate 18000
75-27-4---------Bromodichloromethane 8900
78-87-5---------1,2-Dichloropropane 8900
10061-01-5------cis-l,3-Dichloropropene 8900
79-01-6---------Trichloroethene 8900
124-48-1--------Dibromochloromethane ~900
79-00-s---------l,l,2-Trichloroethane 8900
71~43-2---------Benzene 8900
10061-02-6------Trans-l,3-Dichloropropene __ 8900
75-25-2---------Bromoform 8900
100-10-1--------4-Methyl-2-Pentanone 18000
591-78-6--------2-Hexanone 18000
127-18-4--------Tetrachloroethene 8900
79-34-5---------1,l,2,2-Tetrachloroethane __ 8900
108-88-3--------Toluene 230000
108-90-7--------Chlorobenzene 8900
100-41-4--------Ethylbenzene 8900
100-42-s--------styrene 8900
1330-20-7-------Total Xylenes 8900
FORM I VOA
-·---------___ .._ -----· ·-·-
---· -----•• --4 -D 9FJi':-Iii'
Q
u u u
u
u
u u u u u u u
u
u u u u u
u u u u
u u u u u
u u
D u u u u
1/87 Rev.
to· --J7J
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET.
TENTATIVELY IDENTIFIED COMPOUNDS
SL-30-2DL
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
Lab code: COMPU Case No,: 17902 SAS No,: SDG No.: 70
Matrix: ( soil/water) SOIL
Sample wt/vol: 4.0 (g/mL)
Level: (low/med) MED
t Moisture: not dee. ~
Column (pack/cap) CAP
Number TICS found: ----1
CAS NUMBER COMPOUND
_G_
NAME
Lab Sample ID: 292318
Lab File ID: C3R92318Cl2
Date Received: 10/05/89
Date Analyzed: lQ/14189
Dilution Factor: _1_3 __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST, CONC. Q
================ ==--=-------=-==-------=~~-= ==•===== ============= ====:::
1. UNKNOWN 15.55 20000 J
2. 124-18-5 DECANE 16.49 43000 J
3. UNKNOWN 17.05 14000 J
FORM I VOA-TIC 1/87 Rev.
-----------. ---' _,._ .. . -. ... ' ·---~ J7B
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-10-lMS
Lab Name: COMPUCHEM LABS Contrac't: I 2-88 l -REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7-"'0 __
Matrix: (soil/water) SOIL Lab Sample ID: 291633
Sample wt/vol: 5.0 (g/mL) G __ Lab File ID: GH091633819
Level: · ( low/med) rpw Date Received: 10/04/89
% Moisture: not dee. _u Date Analyzed: 10/08/89.
Column: (pack/cap) CAP Dilution Factor: LO
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/K!;i Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 25 B
67-64-1---------Acetone 6 BJ
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-riichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-0l-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
• 71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
ioa-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6, u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
·---• ... ---.. ~ . . I_,. ---::-:, - . ■Pl. :lr OIi,..--J651
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-10-lMSD
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : 70
Matrix: (soil/water) SOIL Lab Sample ID: 291634
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH0916J4B19
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _u Date Analyzed: 10/08/!!9
Column: (pack/cap) CAP Dilution Factor: ~1~,o._ __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-J---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-JS-4---------1,1-Dichloroethene
7 5-34'-3---------1, 1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-J---------Chloroform
107-06-2--------1,2-Dichloroethane
78~93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene ' 79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6~-----Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
Q
11 u
11 u
11 u
11 u
25 B
6 BJ
6 u
6 u
6 u
6 u
6 u '6 u
11 u
6 u
6 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
l/87 Rev.
168.
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-JO-UIS
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 294743
Sample wt/vol: 4,0 (g/mL) G __ Lab File ID: CN09474JC12
Level: ( low/med) MEP Date Received: 10/05/89
t Moisture: not dee. ___ll Date Analyzed: 10/14/~9
Column: (pack/cap) CAP Dilution Factor: ~i~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 15000
74-83-9---------Bromomethane 15000
75-01-4---------Vinyl Chloride 15000
75-00-3---------Chloroethane 15000
75~09-2---------Methylene Chloride 7400
67-64-1---------Acetone 15000
75-15-o---------carbon Disulfide 7400
75-35-4---------1,l-Dichloroethene 7400
75-34-3---------1,l-Dichloroethane 7400
540-59-0--------1,2-Dichloroethene (total)_ 7400
67-66-3----~----Chloroform 7400
107-06-2--------1,2-Dichloroethane 7400
78-93-3---------2-Butanone 15000
71-55-6~--~-----1,1,1-Trichloroethane 7400
56-23-5---------carbon Tetrachloride 7400
108-05-4--------vinyl Acetate 15000
75-27-4---------Bromodichloromethane 7400
78-87-5---------1,2-Dichloropropane 7400
10061-01-5------cis-l,3-Dichloropropene 7400
79-01-6---------Trichloroethene 7400
124-48-1--------Dibromochloromethane 7400
79-o·o-s---------1, l, 2-Trichloroethane 7400
71-43-2---------eenzene 7400
10061-02-6------Trans-l,3-Dichloropropene __ 7400
75-25-2---------Bromoform 7400
1os-10-1~-------4-Methyl-2-Pentanone 15000
591-78-6--------2-Hexanone 15000
121-18-4--------Tetrachloroethene 7400
79-34-5---------1,1,2,2-Tetrachloroethane __ 7400
108-88-3--------Toluene 7400
108-90-7--------Chlorobenzene 7400
100-41-4--------Ethylbenzene 7400
100-42-s--------styrene 7400
1330-20-7-------Total Xylenes 1900
FORM I VOA
LE oere::•
Q
u u
u
u u
u
u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u
u
u
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u
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u u
u
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u
J
1/87 Rev.
J67 -
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS
SL-30-lMSD
Contract: {2-88l-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 294744
Sample wt/vol: 4,0 (g/mL) \L_ Lab File ID: CN094744Cl2
Level: (low/med) MED Date Received: 10/05/89
t Moisture: not dee. ~ Date Analyzed: lQ/U/89
Column: (pack/cap) !d,\P Dilution Factor: .i~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 15000
74-83-9---------Bromomethane 15000
75-01-4---------Vinyl Chloride 15000
75-00-3---------Chloroethane 15000
75-09-2---------Methylene Chloride 7400
67-64-1---------Acetone 15000
75-15-o---------carbon Disulfide 7400
75-35-4---------1,1-Dichloroethene 7400
75-34-3---------1,1-Dichloroethane 7400
540-59-0--------1,2-Dichloroethene (total)_ 7400
67-66-3---------Chloroform· 7400
101-06-2--------1,2-Dichloroethane 7400
78-93-3---------2-Butanon• 15000
71-55-6---------.1, 1, 1-Trichloroethane 7400
56-23-5---------carbon Tetrachloride 7400
108-05-4--------Vinyl Acetate 15000
75-27-4---------Bromodichloromethane 7400
78-87-5---------1,2-Dichloropropane 7400
10061-01-5------cis-l,3-Dichloropropene 7400
79-01-6---------Trichloroethene 7400
124-48-1--------Dibromochloromethane 7400
79-00-5---------1,l,2-Trichloroethane 7400
71-43-2---------Benzene 7400
10061-02-6------Trana-l,3-Dichloropropene __ 7400
75-25-2---------Bromoform 7400
1os-10-1--------4·-Methyl-2-Pentanone 15000
591-78-6--------2-Hexanone 15000
127-18-4---~----Tetrachloroethene 7400
79-34-5---------1,1,2,2-Tetrachloroethane __ 7400
108-88-3--------Toluene ·1 7400
108-90-7--------Chlorobenzene 7400
100-41-4--------Ethylbenzene 7400
100-42-s--------styrene 7400
1330-20-7-------Total Xylenea 1800
Q
u u u u u u u u u u
u u u u u u u u
.U
u u u u u u u u u u
u u u u
J
FORM I VOA 1/87 Rev.
-~----------. . . ·--·--------~ -. . . . ·-166
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-10-l
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -'-7"-0 __
Matrix: (soil/water) SOIL Lab Sample ID: 291629 -~~---
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GH091629A04
Level: ( low/med) LOW Date Received: 10/04/89
·% Moisture: not dee. __JJ. dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) SQfil; Date Analyzed: 10/08/89
GPC Cleanup: (Y/N) Ji._ pH: 5.5 Dilution Factor: ~i~-9~9~-
CAS-NO. COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/Kq) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-o---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane __ 370
120-83-2--------2,4-Dichlorophenol 370
120-02-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalane 370
106-47-8--------4-Chloroaniline 370
87-68-3----~----Hexachlorobutadiene 370
59-50-7---------4~Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---~-----2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4-----~---2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
Q
u
u
u u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
U· u
u u
u
u
u
u
u
u
u
'
FORM I sv-1 1/87 Rev.
16!5
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-10-1
Lab Name: COMPUCHEM LABS Contract: 12-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 291629
Sa11'ple wt/vol: 30.0 (g/mL) G __ Lab File ID: GH091629A04
Leve 1: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. __u dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10/08/89
GPC Cleanup: (Y/N) Ii.,__ pH: 5.5 Dilution Factor: al~-~0~0 __
CONCENTRATION UNITS:
CAS·NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 370 u
121-14-2---~----2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether __ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 370 u
101-55-3--------4-Bromophenyl-phenylether __ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 370 u
120-12-1--------Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 u
129-oo-o--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 740 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chrysene 370 u
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 1000
117-84-o--------Di-n~octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(l) -Cannot be separated from Diphenylam1ne
FORM I sv-2 1/87 Rev.
. ·----
-------·-.-... -.....-----~------....... ~-. , L6 DR T._·JiSi'4.C.t,7 --!11=::::::::::=::::.:.=.;c.. -l ~4
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2-881-REVS
EPA SAMPLE NO.
SL-10-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dee. _u dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H...._ pH:
Number TICs found: __,l
CAS NUMBER COMPOUND
_G_
SQ.f:!!;
s.s
NAME
Lab sample ID: 291629
Lab File ID: GH091629A04
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/08/89
Dilution Factor: Ll~,o~o.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= •====
l. BLANK CONTAMINANT 5.40 340 BJ
2. BLANK CONTAMINANT 5.50 260 BJ
3. 4337-65-9 HEXANEDIOIC ACID, MON0(2-ETH 16.25 220 J
FORM I SV-TIC 1/87 Rev.
L~ --... . . . 't5J
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18 . EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-11-1
Lab Name: COMPUCHEM LABS Contract: {2-88l-REVS
Lab· Code: COMPU Case No.: 17902 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: JO.O (g/mL) G __
Level: (low/med) -LO~W,a...._
% Moisture: not dee. _li dee.
Extraction: (SepF/Cont/Sonc). s.ofil:
SDG No. : .,_70,.___
Lab Samp 1 e ID: s..2.z.9.,._l,,_6 3.,_9.,__ __ _
Lab File ID: GH091639A04
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/08/89
GPC Cleanup: (Y/N) IL_ pH: 5.2 Dilution Factor: £1~.o~o,,___
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol J70 u
lll-44-4--------bis(2-Chloroethyl)Ether J70 u
95-57-8---------2-Chlorophenol J70 u
541-73-1--------1,J-Dichlorobenzene J70 u
106-46-7--------1,4-Dichlorobenzene J70 u
100-51-6--------Benzyl Alcohol J70 u
95-50-1-~-------l,2-Dichlorobenzene J70 u
95-48-7---------2-Methylphenol J70 u
J96J8-J2-9--.----bis ( 2-Chloroisopropyl) Ether_ J70 u
106-44-5--------4-Methylphenol J70 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ J70 u
6 7 -7 2 -1-.--------Hexachl oroethane J70 u
98-95-J---------Nitrobenzene J70 u
78-59-1---------Isophorone J70 u
88-75-5------~--2-Nitrophenol J70 u
105-67-9--------2,4-Dimethylphenol J70 u
65-ss-o---------Benzoic Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ J70 u·
120-83-2--------2,4-Dichlorophenol J70 u
120-s2-1--------1,2,4-Trichlorobenzene J70 u
91-20-3---------Naphthalene J70 u
106-47-8--------4-Chloroaniline J70 u
87-68-3---------Hexachlorobutadiene J70 u
59-50-7---------4-Chloro-3-Methylphenol J70 u
91-57-6-~-------2-Methylnaphthalene J70 u
77-47-4---------Hexachlorocyclopentadiene __ J70 u
88-06-2---------2,4,6-Trichlorophenol J70 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene J70 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
FORM I sv-1 1/87 Rev.
-. ----· .. -~· ·-. ' ---. --·· -. .,, . -. . .,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEH LABS Contract: 12-88)-REVS SL-11-1
Lab Code: COHPU Case No.: 17902 SAS No. : SDG No. : 70
Matrix: ( soil/water) SOIL Lab Sample IO: 291639
Sample wt/vol: 30.0 (g/mL) _G_ Lab File IO: GH091639A04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. --1.2. dee. Date Extracted: lQ/QS/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: lO/QS/89
GPC Cleanup: (Y/N) IL_ pH: 5.2 Dilution Factor: l,OQ
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene -· 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-7--------4-Nitrophenol 1800 u
132-64-9--------Dibenzoturan 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether __ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitroeodiphenylamine (l)_ 370 u
101-55-3--------4-Bromophenyl-phenylether __ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 370 u
120-12-7--------Anthracene 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 0
129-00-o--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 750 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chrysene 370 u
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 780
117-84-0--------Di-n-Octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 37,0 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -Cannot be separated'trom Diphenylamine
FORM I sv-2 1/87 Rev.
► = J6I
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. lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-11-1
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: ~7~0 __
Matrix: (soil/water) SOIL
sample wt/vol: 30.0 (g/mL) ~
Level: ( low/med) r.,pw
% Moisture: not dee. ---1.2.
Extraction:
GPC Cleanup:
(SepF/Cont/Sone)
(Y/N) lL..
Number TICS found: --2.
dee.
pH:
CAS NUMBER COMPOUND
5.2
NAME
Lab Sample ID:
Lab File ID:
.Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
291639
GH091639A04
10/04/89
10/05/89
10/08/89
·1. 00
CONC. Q
================ ==============m============= ======== ============= =====
1. ALDOL 6.42 490 AJ
2. ALDOL 6.85 JOO AJ
'
FORM I SV-TIC 1/87 Rev.
-. .. ... '• • I _.
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18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-12-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: CQMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 291640
Sample wt/vol: 30.0 (g/mL) !:i___ Lab File ID: GH091640A04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _J.2 dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL_ pH: 5.5
Date Analyzed: 10/09/89
Dilution Factor: -1~.0~9~-
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1---~----l,3-Dichlorobenzene 370
106-46-7--~-----l,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-0---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370
120-83-2--------2,4-Dichlorophenol 370
120-82-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexaehlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
FORM I sv-1
-. . . --.... -.. --· . -. .. , ---.. . . . ...
Q
u
u u
u
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u
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u
u u
u
u
u u
u
u
u
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u u
u
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u u
u
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u u
u
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u
1/87 Rev.
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-12-1
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_70"---
Matrix: (soil/water) SOIL Lab s amp 1 e ID: .,.2.,._9 ._16:,,.;4:,.;0,.__ __ _
Sample wt/vol: 30.0 (g/mL) L__
LOW
Lab File ID: GH091640A04
Level: ( low/med) Date Received: 10/04/89
% Moisture: not dee. __l.O. dee. Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: .1~,~9~0 __
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li,_ pH: 5.5
CAS NO. COMPOUND
CONCENTRATION UNITS: '
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------Dibenzoturan 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether_ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (l)_· 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5----~----Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------Di-n-Butylphthalate 42
206-44-0--------Fluoranthene 370
129-00-o--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1---~-----3,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracena 370
218-01-9--------chrysene 370
117-Bl-7--------bis(2-Ethylhexyl)Phthalata_ 100
117-84-0--------oi-n-octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 370
(1) -Cannot be separated rrom Diphenylamine
Q
u
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u u u
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u u u
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BJ
u u u
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u u
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u u
u
FORM I sv-2 1/87 Rev.
::s • 158
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-12-l
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: ~7~0 __
Matrix: (soil/water) SOIL Lab Sample ID: ..._2 ,,_9 ._l 6"-'4i.:O,.__ __ _
Sample wt/vol: 30,0 (g/mL) !i__ Lab File ID: GH091640A04
Level: (low/med) LOW
% Moisture: not dee. ____ll
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL..
Number TICs found: ___,l
dee.
pH:
-
~
5,5
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: ._1~.o~o.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.· Q
================ =============-=============== =-•====== ============= =a====
l. ALOOL 6.25 220 AJ
· FORM I SV-TIC l/87 Rev.
------------· --... ,_ . --.. J !!17
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-13-l
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: ~7~0 __
Matrix: (soil/water) SOIL Lab Sample IO: .,.2.,_9..._16:,,.;4,._,l..__ __ _
Sample wt/vol: 30.0 (g/mL) L_
LOW
Lab File IO: GJ091641A04
Leve 1: ( low/med)
t Moisture: not dee. ___l,1 dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution.Factor: l,00
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...... pH: 5,6
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 430
lll-44-4--------bis(2-Chloroethyl)Ether 430
95-57-8---------2-Chlorophenol 430
541-73-1--------l,3-Dichlorobenzene 430
106-46-7--------1,4-Dichlorobenzene 430
100-51-6--------Benzyl Alcohol 430
95-50-l---------l,2-Dichlorobenzene 430
95-48-7---------2-Methylphenol 430
39638-32-9------bis(2-Chloroisopropyl)Ether_ 430
106-44-5--------4-Methylphenol 430
621-64-7--------N-Nitroso-oi-n-Propylamine_ 430
67-72-1---------Hexachloroethane 430
98-95-3---------Nitrobenzene . 430
78-59-1---~-----Isophorone 430
88-75-5---~-----2-Nitrophenol 430
105-67-9--------2,4-Dimethylphenol 430
65-ss-o---------Benzoic Acid 2100
lll-91-l--------bis(2-Chloroethoxy)Methane __ -430
120-83-2--------2,4-Dichlorophenol 430
120-a2-1--------l,2,4-Trichlorobenzene 430
91-20-3---------Naphthalene 430
106-47-8--------4-Chloroaniline 430
87-68-3---------Hexachlorobutadiene 430
59-50-7---------4-Chloro-3-Methylphenol 430
91-57-6---------2-Methylnaphthalene 430
77-47-4---------Hexachlorocyclopentadiene __ 430
88-06~2---------2,4,6-Trichlorophenol 430
95-95-4---------2,4,5-Trichlorophenol 2100
91-58-7---------2-Chloronaphthalene 430
88-74-4---------2-Nitroaniline 2100
131-11-3--------Dimethyl Phthalate 430
208-96-8--------Acenaphthylene 430
606-20-2--------2,6-Dinitrotoluene 430
FORM I sv-1
u u u u u
u u u u u
u u u u u u
u u u u u u u u u u
u u u u u u u
-,. • 3 SOW!f: E D QaJ-:::Sl.lili ... ili•Hl►e:i<=c::=--=-
Q
1/87 Rev.
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-13-l
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab code: COMPU Case No.: 17902 SAS No,: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291641
Sample wt/vol: 30.0 (g/mL) G_ Lab File ID: GJ091641A04
Level: ( low/med) LOW Date Received: 10/04/89
, Moisture: not dee. __ll dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) IL_ pH: 5.6 Dilution Factor: .i~-~P~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2100 u
83-32-9---------Acenaphthene •' 430 u
51-28-5---------2,4-Dinitrophenol 2100 u
100-02-1--------4-Nitrophenol 2100 u
132-64-9--------Dibenzoturan 430 u
121-14-2--------2,4-Dinitrotoluene 430 u
84~66-2---------Diethylphthalate 430 u
7005-72-3-------4-Chlorophenyl-phenylether_ 430 u
86~73-7---------Fluorene 430 u
100-01-6--------4-Nitroaniline 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2100 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 430 u
101-55-3--------4-Bromophenyl-phenylether __ 430 u
118-74-1--------Hexachlorobenzene 430 u
87-86-5---------Pentachlorophenol 2100 u
ss-01-s---------Phenanthrene 430 u
120-12-1--------Anthracene 430 u
84-74-2---------Di-n-Butylphthalate 75 BJ
206-44-0--------Fluoranthene 430 u
129-00-0--------Pyrene 430 u
85-68-7---------Butylbenzylphthalate 430 u
91-94-1---~-----3,3'-Dichlorobenzidine 860 u
56-55-3---------Benzo(a)Anthracene 430 u
210-01-9--------Chrysene 430 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 100 .J
117-84-0--------Di-n~Octyl Phthalate 430 u
205-99-2--------Benzo(b)Fluoranthene 430 u
207-08-9--------Benzo(k)Fluoranthene 430 u
50-32-8---------Benzo(a)Pyrene 430 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 430 u
53-70-3---------Dibenzo(a,h)Anthracene 430 u
191-24-2--------Benzo(g,h,i)Perylene 430 u
(1) -cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
--,-.. -.. -.. --~ -,.: .. -. --.. 155
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG
Matrix: (soi 1/water) SOIL Lab Sample ID:
SL-13-1
No. : 70
291641
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GJ091641A04
Level: ( low/med) I.DW
% Moisture: not dee. ---2.l dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: ( Y/N) li.._ pH: 5, 6
Number TICs found: _2_J_
CAS NUMBER COMPOUND NAME
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: ~l~.0~0,,____
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= =-==== .
1. BLANK CONTAMINANT 5.28 170 BJ
2. ALDOL 6.15 650 AJ
J . ALDOL 6.58 4JO AJ
4. UNKNOWN 17.67 JOO J
5. UNKNOWN 17.80 1000 J
6. UNKNOWN 18.64 JOO J
7. UNKNOWN 18.85 J50 J
8. UNKNOWN 19.09 480 J
9. UNKNOWN 19.19 260 J
10. UNKNOWN 19.22 610 J
11. UNKNOWN 19. JS JOO J
12. UNKNOWN 19.65 520 J
13. UNKNOWN 19.80 J50 J
14. UNKNOWN 20.54 JOO J
15. UNKNOWN 20.64 170 J
16. UNKNOWN 20.70 4JO J
17. UNKNOWN 20.85 560 J
18. UNKNOWN 21.52 J90 J
19. UNKNOWN 21.79 260 J
20. UNKNOWN 21.84 JOO J
21. UNKNOWN 22.95 990 J
22. UNKNOWN 24.80 220 J
2 J. UNKNOWN 24.87 260 J·
FORM I SV-TIC l/87 Rev.
= J 5.,
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lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: ( 2-88 l -REVS
SL-14-l
Lab Code: COMPU Case No.: 17902 SAS No.: ---SDG No.: .,_7.,_0 __
Matrix: (soil/water) SOIL Lab Sample ID: ~2~9•1~64~2,.___ __ _
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GH091642A04
Level: ( low/med) LOW
\ Moisture: not dee. ___ll dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) t:!........ pH: 5.6 Dilution Factor: 1,00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
lOB-95-2--------Phenol 400
lll-44-4--------bis(2-Chloroethyl)Ether 400
95-57-8---------2-Chlorophenol 400
541-73-1--------1,3-Dichlorobenzene 400
106-46-7--------1,4-Dichlorobenzene 400
100-51-6--------Benzyl Alcohol 400
95-S0-1---------1,2-Dichlorobenzene 400
95-48-7---------2-Methylphenol 400
39638-32-9------bis(2-Chloroisopropyl)Ether_ 400
106-44-5--------4-Methylphenol 400
621-64-7--------N-Nitroso-oi-n-Propylamine __ 400
67-72-1---------Hexachloroethane 400
98-95-3---------Nitrobenzene 400
78-59-1---------Isophorone 400
88-75-5---------2-Nitrophenol 400
105-67-9--------2,4-Dimethylphenol 400
65-as-o---------Benzoic Acid ' 1900
1.11-91-1--------bis ( 2-Chloroethoxy) Methane __ 400
120-83-2--------2,4-Dichlorophenol 400
120-02-1--------1,2,4-Trichlorobenzene 400
91-20-3•--------Naphthalene 400
106-47-8--------4-Chloroaniline 400
87-68-3---------Hexachlorobutadiena 400
59-50-7---------4-Chloro-J-Methylphenol 400
91-57-6---------2-Methylnaphthalene 400
77-47-4---------Hexaehlorocyclopentadiena_ 400
88-06-2---------2,4,6-Trichlorophenol 400
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 400
88-74-4---------2-Nitroaniline· 1900
131-11-3--------Dimethyl Phthalate 400
208-96-8--------Acenaphthylene 400
606-20-2--------2,6-Dinitrotoluane 400
FORM I SV-1
;,; z-,,. -
u u u u
u u u u
u u u u
u u
u u
u u u u
u u u u u u u u
u u u u u
Q
1/87 Rev.
15:S
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-14-1 Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 291642
Sample wt/vol: Jo.a (g/mL) li...._ Lab File ID: GH091642A04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ---11 dee. Date Extracted: 10/0:;i/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H...._ pH: :i,6
Date Analyzed: 10/09/89
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1900
83-32-9---------Acenaphthene 400
51-28-5~--------2,4-Dinitrophenol 1900 100-02-1--------4-Nitrophenol 1900 132-64-9--------Dibenzoturan 400
121-14-2--------2,4-Dinitrotoluene 400
84-66-2---------Diethylphthalate 400 7005-72-3-------4-Chlorophenyl-phenylether __ 400 86-73-7----~----Fluorene 400 100-01-6--------4-Nitroaniline 1900 534-52-1--------4,6-Dinitro-2-Methylphenol_ 1900
86-30-6~--------N-Nitrosodiphenylamine (1)_ 400 101-55-3--------4-Bromophenyl-phenylether __ 400
118-74-1--------Hexachlorobenzene 400
87-86-5---------Pentachlorophenol 1900
85-01-8---------Phenanthrene 400
120-12-1--------Anthracene 400
84-74-2---------Di-n-Butylphthalate 50 206-44-0--------Pluoranthene 400
129-00-0--------Pyrene 400
85-68-7---------Butylbenzylphthalate 400
91-94-1---------J,J'-Dichlorobenzidine 800
56-55-3---------Benzo(a)Anthracene 400
218-01-9~-------chrysene 400
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 520
117-84-0--------Di-n-Octyl Phthalate 400
205-99-2--------Benzo(b)Pluoranthene 400
207-08-9--------Benzo(k)Fluoranthene 400
50-32-8---------Benzo(a)Pyrene 400
193-39-5--------Indeno(l,2,3-cd)Pyrene 400
53-70-3---------Dibenzo(a,h)Anthracene 400
191-24-2--------Benzo(g,h,i)Perylene 400
(1) -Cannot be separated trom Diphenylamine
FORM I sv-2
--------. . ' -. . . . " ..._, __ .... -.. --~ .. -. . . ' 6-.0IITlr M =
Q
u u u u u u u u
u u u u u u u u u
BJ u u u u u u
u u u u u u u
1/87 Rev.
-152
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
SL-14-1
No.: 70
291642
Sample wt/vol: 30.0 (g/mL) g__ Lab File ID: GH091642A04
Level: ( low/med) LOW
% Moisture: not dee. -11. dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL_ pH: 5,6
Number TICs found: ---2
CAS NUMBER COMPOUND NAME
Date Received: 10/04/89
Date Extracted: 10/05/82
Date Analyzed: 10/09/82
Dilution Factor: ~i~-~9~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ===========-===----=---=-=== =====zi==-:a::r============ :11===::;;:
1. ALDOL 6.30 640 AJ
2. ALDOL 6.73 360 AJ
3 . UNKNOWN 21.65 280 J
4. UNKNOWN 22.69 560 J
5. UNKNOWN 24.04 320 J
FORM I SV-TIC 1/87 Rev.
mi. c~ DR.TR --SCiiiUIIF-•l .... 1"11...--==·==-=:,i;;;;;.-= 151
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-15-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_70,,___
Matrix: (soil/water) SOIL Lab Sample ID: s2~9...,l,._64"-3.__ __ _
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH091643C04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _ll dee. Date Extracted: 10/05/89
Extraction: ( SepF /Cont/Sonc)
(Y/N) H.,_
~
5.7
Date Analyzed: 10/09/89
GPC Cleanup: pH: Dilution Factor: 1.00
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2~-------Phenol 390
lll-44-4--------bis(2-Chloroethyl)Ether 390
95-57-8---------2-Chlorophenol 390
541-73-1--------l,3-Dichlorobenzene 390
106-46-7--------l,4-Dichlorobenzene 390
100-51-6--------Benzyl Alcohol 390
95-50-1---------l,2-Dichlorobenzene 390
95-48-7---------2-Methylphenol 390
39638-32-9------bis(2-Chloroisopropyl)Ether_ 390
106-44-5--------4-Methylphenol 390
621-64-7--------N~Nitroso-Di-n-Propylamine_ 390
67-72-1---------Hexachloroethane 390
98-95-3---------Nitrobenzene 390
78-59-1---------Isophorone 45
88-75-5---------2-Nitrophenol 390
105-67-9--------2,4-Dimethylphenol 390
65-as-o---------aenzoic Acid 140
lll-9l-l--------bia(2-Chloroethoxy)Methane_·_ 390
120-83-2--------2,4-Dichlorophenol 390
120-a2-1--------l,2,4-Trichlorobenzene 390
91-20-3--~------Naphthalene 390
106-47-8--------4-Chloroaniline 390
87-68-3---------Hexachlorobutadiene 390
59-50-7---------4·-chloro-3-Methylphenol 390
91-57-6---------2-Methylnaphthalene 390
77-47-4---------Hexa~hlorocyclopentadiene_ 390
88-06-2---------2,4,6-Trichlorophenol 390
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 390
88-74-4---------2-Nitroaniline 1900
131-11-3--------Dimethyl Phthalate 390
208-96-8--------Acenaphthylene 390
606-20-2--------2,6-Dinitrotoluene 390
u u u u u u u u u u u u u
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-
FORM I sv-1 1/87 Rev.
--·--_.,. .. __ -Ii J:SB
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE ·No.
Lab Name: COMPUCHEM LABS· ·contract: <2-88l-REVS
SL-15-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
. Matrix: ( soil/water) SOIL Lab Sample ID: 291643
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: GH091643C04
Level: (low/med) LOW Date Received.: 10/04/89
% Moisture: not dee. _ll dee. Date Extracted: 10/0~/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti..__ pH: 5.7
Date Analyzed: 10/09/89
Dilution Factor: 1.00
'
CAS NO. COMPOUND
CONCENTRATION UNITS: .
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1900
83-32-9---------Acenaphthene 390
51-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
132-64-9--------Dibenzofuran 390
121-14-2--------2,4-Dinitrotoluene 390
84-66-2---------Diethylphthalate 390
7005-72-3-------4-Chlorophenyl-phenylether_ 390
86-73-7---------Fluorene 390
100-01-6-~------4-Nitroaniline 1900
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1900
86-30-6---------N-Nitrosodiphenylamine (1)_ 390
101-55-3--------4-Bromophenyl-phenylether __ 390
118-74-1--------Hexachlorobenzene 390
87-86-5---------Pentachlorophenol 1900
ss-01-s---------Phenanthrene 390
120-12-1--------Anthracene 390
84-74-2---------Di-n-Butylphthalate 130
206-44-0--------Fluoranthene 390
129-00-0--------Pyrene 390
85-68-7---------Butylbenzylphthalate 390
91-94-1---------3,3'-Dichlorobenzidine 780
56-55-3---------Benzo(a)Anthracene 390
218-01-9--------Chrysene 390
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 260
117-84-0--------Di-n~Oetyl Phthalate 390
205-99-2--------Benzo(b)Fluoranthene 390
207-08-9--------Benzo(k)Fluoranthene 390
50-32-8---------Benzo(a)Pyren• 390
193-39-5--------Indeno(l,2,J-cd)Pyrene 390
53-70-3---------Dibenzo(a,h)Anthracene 390
191-24-2--------Benzo(g,h,i)Perylene 390
(l) -Cannot be separated from Diphenylamine
FORM I SV-2
-' -... -------.., .,;. ··-.· -=--_,.,,.,. .... s ~-DIITll:'-S4T p
Q
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1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12~aa1-REVS
EPA SAMPLE NO.
SL-15-1
Lab code: COMPU .Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) G __
Level: (low/med) LOW
% Moisture: not dee. _..ll dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ii,_ pH: s.·7
Number TICs found: _u
CAS NUMBER COMPOU!rn NAME
Lab Sample ID: 291643
Lab File ID: GH091643C04
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST, CONC. Q
================ ==---==---=--=--=--=-======= ========= ============= •====
1. ALDOL 6.23 550 AJ
2. ALOOL 6.68 510 AJ
3. UNKNOWN 13.44 1800 J
4. UNKNOWN 13.85 940 J
5. UNKNOWN 13.90 1200 J
6. UNKNOWN 13.97 940 J
7. UNKNOWN 14.40 1200 J
8. UNKNOWN 15.19 860 J
9. UNKNOWN 15.37 1700 J
10. UNKNOWN 15.57 2500 J
11. UNKNOWN 15.69 1700 J
12. UNKNOWN 15.79 1400 J
13. UNKNOWN 15.97 740 J
14. UNKNOWN 16.14 1200 J
15. UNKNOWN 16.30 740 J
16. UNKNOWN 16.49 1800 J
17. UNKNOWN 16.64 1400 J
18. UNKNOWN 16.75 740 J
19. UNKNOWN 16.80 940 J
20. UNKNOWN 17.22 1300 J
21. UNKNOWN 17. 37 710 J
22, UNKNOWN 17. 85 940 J
FORM I SV-TIC 1/87 Rev.
::::::;;:;~;a, p :sa 148
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-16-1
Lab Code: COMPO Case No.: 17902 SAS No.: SOG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291644
sample wt/vol: 30.0 (g/mL) _G_ Lab File IO: GD091§44C04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ---1.l dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) Ii._ pH: 5.4 Dilution Factor: ~3~1~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1100
lll-44-4--------bis(2-Chloroethyl)Ether 1100
95-57-8---------2-Chlorophenol 1100
541-73-1--------1,3-Dichlorobenzene 1100
106-46-7--------1,4-Dichlorobenzene 1100
100-51-6--------Benzyl Alcohol 1100
95-50-1---------1,2-oichlorobenzene 1100
95-48-7---~-----2-Methylphenol 1100
39638-32-9------bis(2-Chloroisopropyl)Ether_ 1100
106-44-5--------4-Methylphenol 1100
621-64~7--------N-Nitroso-Di-n-Propylamine_ 1100
67-72-1---------Hexachloroethane 1100
98-95-3---------Nitrobenzene 1100
78-59-1---------Isophorone 1100
88-75-5---------2-Nitrophenol 1100
105-67-9--------2,4-0imethylphenol 1100
65-85-o---------Benzoic Acid 5400
lll-91-l--------bia(2-Chloroethoxy)Methane_ 1100
120-83-2--------2,4-Dichlorophenol 1100
120-s2-1--------1,2,4-Trichlorobenzene 1100
91-20-3---------Naphthalene 1100
106-47-8--------4-Chloroaniline 1100
87-68-3---------Hexachlorobutadiene 1100
59-50-7~--------4-Chloro-3-Methylphenol 1100
91-57-6---------2-Methylnaphthalene 1100
77-47-4---------Hexachlorocyclopentadiene __ 1100
88-06-2---------2,4,6-Trichlorophenol 1100
95-95-4---------2,4,5-Trichlorophenol 5400
91-58-7---------2-Chloronaphthalene 1100
88-74-4---------2-Nitroaniline 5400
131-11-3--------oimethyl Phthalate 1100
208-96-8--------Acenaphthylene 1100
606-20-2--------2,6-Dinitrotoluene 1100
Q
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FORM I sv-1 1/87 Rev.
,,,7
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
L~b Name: COMPUCHEM LABS Contract: /2-881-REVS
SL-16-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_70"'---
Matz:-ix: (soil/water) SOIL Lab Sample ID: ~2~9Al6~4~4:,__ __ _
Sample wt/vol: 30,0 (g/mL) !;__ Lab File ID: GD091644C04
Level: (low/med) LOW Date Received: 10/04/89
\ Moisture: not dee. ---1J. dee. Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extz:-action: (SepF/Cont/Sonc) fillliC
GPC Cleanup: ( Y/N) li,_ pH: 5.4 Dilution Factor: ~3~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 5400 u
83-32-9---------Acenaphthene 1100 u
51-28-5---------2,4-Dinitrophenol 5400 u
100-02-7--------4-Nitrophenol 5400 u
132-64-9--------Dibenzoturan 1100 u
121-14-2--------2,4-Dinitrotoluene 1100 u
84-66-2---~-----Diethylphthalate 1100 u
7005-72-3-------4-Chlorophenyl-phenylether_ 1100 u
86-73-7---------Fluorene 1100 u
100-01-6--------4-Nitroaniline 5400 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 5400 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 1100 u
101-55-3--------4-Bromophenyl-phenylether __ 1100 ·U
118-74-1--------Hexachlorobenzene 1100 u
87-86-5---------Pentachlorophenol 5400 u
ss-01-s---------Phenanthrene 1100 u
120-12-1--------Anthracene 1100 u
84-74-2---------Di-n-Butylphthalate 1100 u
206-44-0--------Fluoranthene 1100 u
129-oo-o--------Pyrene 1100 u
85-68-7---------Butylbenzylphthalate 1100 u
91-94-1---------3,3'-Dichlorobenzidine 2200 u
56-55-3---------Banzo(a)Anthracene 1100 u
218-01-9--------Chrysene 1100 u
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 1100 u
117-84-0--------Di-n~octyl Phthalate 1100 u
205-99-2--------eanzo(b)Fluoranthene 1100 u
207-08-9--------Benzo(k)Fluoranthene 1100 u
50-32-8---------Benzo(a)Pyrene 1100 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 1100 u
53-70-3---------Dibenzo(a,h)Anthracene 1100 u
191-24-2--------Benzo(g,h,i)Perylene 1100 u
(1) -cannot be separated trom Diphenylam1ne
FORM I sv-2 1/87 Rev.
:I . .,_ SRWPL£ ORTR ·SIi I _..;;:.~ J 46
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
EPA SAMPLE NO.
SL-16-1
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: 70
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) L_
Level: (low/med) ~LO~W.!!...._
% Moisture: not dee. -1.l dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li,__ pH: 5,4
Number TICs found: ~
CAS NUMBER COMPOUND NAME
Lab sample ID: 291644
Lab File IO: GD091644C04
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: ~3~,~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
.. RT EST . CONC. Q
----=---=---=--= ======3===================== =-======= ============= ======
1. UNKNOWN 13.50 5400 J
2. UNKNOWN 13.94 5100 J
3 . UNKNOWN 14.49 3400 J
4. UNKNOWN HYDROCARBON l4, 57 2400 J
5. UNKNOWN 15,29 2700 J
6. UNKNOWN 15,35 3700 J
7. UNKNOWN 15.62 5300 J
8. UNKNOWN 15.77 8100 J
9. UNKNOWN 16.00 2700 J
10. UNKNOWN 16.07 3800 J
11. UNKNOWN 16. 20 5200 J
12, UNKNOWN 16.35 5400 J
13. UNKNOWN 16.59 7600 J
14. UNKNOWN 16.74 5600 J
15. UNKNOWN 16.95 2800 J
16. UNKNOWN 17.34 4900 J
17. UNKNOWN 17.50 3000 J
18. . UNKNOWN 17.57 2600 J
19. UNKNOWN 18.00 4700 J
20. UNKNOWN 18.29 2500 J
FORM I SV-TIC 1/87 Rev.
IJ 145
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1B
SEMIVOLATILE· ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-17-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab sample ID: 291645
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID: GH091645B04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _a dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc)
(Y/N) li...._
~
5.9
Date Analyzed: 10/10/89
Dilution Factor: l,oo GPC Cleanup: pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 360
lll-44-4--------bis(2-Chloroethyl)Ether 360
95-57-8---------2-Chlorophenol . 360
541-73-1--------1,3-Dichlorobenzene 360
106-46-7--------1,4-Dichlorobenzene 360
100-51-6--------Benzyl Alcohol 360
95-50-1---------1,2-Dichlorobenzene 360
95-48-7---------2-Methylphenol 360
39638-32-9------bis(2-Chloroisopropyl)Ether_ 360
106-44-5--------4-Methylphenol 360
621-64-7--------N-Nitroso-Di-n-Propylamine __ 360
67-72-1---------Hexachloroethane 360
98-95-3---------Nitrobenzene 360
78-59-1---------Isophorone 360
88-75-5---------2-Nitrophenol 360
105-67-9--------2,4-Dimethylphenol 360
65-85-0---------Benzoic Acid 1700
lll-91-l--------bis(2-Chloroethoxy)Methane __ 360
120-83-2--------2,4-Dichlorophenol 360
120-a2-1--------l,2,4-Trichlorobenzene 360
91-20-3---------Naphthalene 360
106-47-8--------4-Chloroaniline 360
87-68-3---------Hexachlorobutadiene 360
59-50-7---------4-Chloro-3-Methylphenol 360
91-57-6---------2-Methylnaphthalene 360
77-47-4---------Hexachlorocyclopentadiene __ 360
88-06-2---------2,4,6-Trichlorophenol 360
95-95-4---------2,4,5-Trichlorophenol 1700
91-58-7---------2-Chloronaphthalene 360
88-74-4---------2-Nitroaniline 1700
131-11-3--------Dimethyl Phthalate 360
208-96-8--------Acenaphthylene 360
606-20-2--------2,6-Dinitrotoluene 360
Q
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FORM I sv-1 1/87 Rev.
--SAJ'IPLE DR Ta .SSrlil,.7 --!lii!!i:::::::::;.;;::=~ -. . --,., .. ,,,,,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
·Lab Code: COMPU Case No.: 17902 SAS No.: SDG
EPA SAMPLE NO.
SL-17-l
No.: 70
I Matrix: (soil/water) SOIL Lab Sample ID: 291645
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Sample wt/vol: 30,0 (g/mL) L_ Lab File ID: GH091645B04
Level: (low/med) LOW Date Received: 10/04/89
\ Moisture: not dee.~ dee. Date Extracted: 10l05/89
Extraction: (SepF/Cont/Sonc)
(Y/N) ti,_
§.2li.C.
5,9
Date Analyzed: 10/10/89
GPC Cleanup: pH: Dilution Factor: Al~,o~o,___
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3'-Nitroaniline 1700
83-32-9---------Acenaphthene 360
s1-2e-s---------2,4-Dinitrophenol 1700
100-02-1--------4-Nitrophenol 1700
132-64-9--------Dibenzofuran 360
121-14-2--------2,4-Dinitrotoluene 360
84-66-2---------Diethylphthalate 360
7005-72-3-------4-Chlorophenyl-phenylether __ 360
86-73-7---------Fluorene 360
100-01-6--------4-Nitroaniline 1700
534-52-1--------4,6-0initro-2-Methylphenol __ 1700
86-30-6---------N-Nitrosodiphenylamine (1)_ 360
101-55-3--------4-Bromophenyl-phenylether __ 360
118-74-1--------Hexachlorobenzene 360
87-86-5---------Pentachlorophenol 1700
as-01-a---------Phenanthrene 360
120-12-1--------Anthracene 360
84-74-2---------Di-n-Butylphthalate 360
206-44-0--------Fluoranthene 360
129-00-0--------Pyrene 360
85-68-7---------Butylbenzylphthalate 360
91-94-1---------3,3'-Dichlorobenzidine 720
56-55-3---------Benzo(a)Anthracene 360
218-01-9--------Chrysen• 360
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 340
111-a,-o--------oi-n-octyl Phthalate 360
205-99-2--------Benzo(b)Fluoranthene 360
207-08-9-'-------Benzo(k)Fluoranthene 360
50-32-8---------Benzo(a)Pyrene 360
193-39-5--------Indeno(l,2,3-cd)Pyrene 360
53-70-3---------Dibenzo(a,h)Anthracene 360
191-24-2--------Benzo(g,h,i)Perylene 360
(l) -Cannot be separated from Diphenylamine
Q
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FORM I sv-2 1/87 Rev.
143
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS
Lab Code: COMPU Case No.: 17902
Matrix: ( soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Level: (low/med) LOW
% Moisture:
Extraction:
GPC Cleanup:
not dee. ~
(SepF/Cont/Sonc)
(Y/N) ti,_
Number TICs found: ---3.
dee_.
pH:
CAS NUMBER COMPOUND
SL-17-1
Contract: [2-BBl-REVS
SAS No.: SDG No.: 70
Lab Sample ID: 291645
_G_ Lab File ID: GH091645B04
2.9H.C
5.9
NAME
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/10/89
Dilution Factor: al~,~0~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. ' CONC. Q
=====•======•==--=-=•==---==~==-------=-==== am===•== m===========::11 =====
1. BLANK CONTAMINANT 5.25 180 BJ
2. ALDOL 6.15 510 AJ
3. ALDOL 6.60 250 AJ
FORM I SV-TIC 1/87 Rev.
'LE DRTII .SSIUII--EE:::;;.::--~"'-J42
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-18-l
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291646
Sample wt/vol: 30,0 (g/mL) _G_ Lab File ID: GH091646C04
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _l.Q. dee. Date Extracted: lQ/0~/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
{Y/N) IL.. pH: 4,9
Date Analyzed: 10/09/89
Dilution Factor: .1~,0~0"---
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_·_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370
67-72~1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-0---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane __ 370
120-83-2--------2,4-Dichlorophenol 370
120-a2-1--------l,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370·
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
Q
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FORM I SV-1 1/87 Rev.
-·-,.,,
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-18-l
Lab Name: COMPUCHEM LABS Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: ---SDG No.: ~7~0 __
Matrix: (soil/water) SOIL Lab Sample IO: .._2,._9..._16"-'4,_,6.__ __ _
Sample wt/vol: 30,0 .(g/mL) ~ Lab File ID: GH091646C04
_Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ___.l_O_ dee. Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) li___ pH: 4,9 Dilution Factor: Al~-~9~0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2--------~3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-7--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84~66-2---------Diethylphthalate 370
7005-72-3---~---4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-oo-o--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1--~------3,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 370
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 46
117-84-0--------oi-n-octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--·------Benzo(g, h, i) Perylene 370
(1) -Cannot be separated from Diphenylamine
Q
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u u u u u u u u u u u
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FORM I sv-2 1/87 Rev.
:ii;::='5,::=!iii:!i~::::=,_il!tl ■die.:··=-~lr.ta~a-P~L6-DR TR. ~-~ . ---
~
14B
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EP~ SAMPLE NO.
SL-18-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) ~
Level: ( low/med) LOW
% Moisture: not dee. -1.Q. dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ii,_ pH: 4,9
Number TICs found: ---2.
CAS NUMBER
: .. _:;;~•,,-:.,-.,.,-:::· -• COMPOUND~NAME
Lab Sample ID: 291646
Lab File ID: GH091646C04
Date Received: 10/04/89
Date Extracted: 10/0~/89
Date Analyzed: 10/09/89
Dilution Factor: &l~,o~o"--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
'. ' RT EST. CONC, Q
===============:a ==s••==================a==a::::1 :a•:a====-=-•=======::::1:::::1c:m= •====
l, BLANK CONTAMINANT 5.32 190 BJ
2. ALDOL 6.25 260 A.J
FORM I SV-TIC 1/87 Rev.
---· ----===-··· ~.,:jj1"!511!_.l&Ja_ c::--iiaZIPII_ o:::::ISR..,_ ·•~ .. -"P.~:LE DIITR. sum .. '"' .. J39
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lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SL-19-1
~ab Name: COMPUCHEM LABS Contract: {2-88)-REVS
L,1b Code: COMPU Case No.: 17902 SAS No. : S CG No. : -'-7.,.0 __
~atrix: (soil/water) SOIL Lab Sample ID: 22~9Al~6i47-'------
Sample wt/vol: 30.0 (g/mL) G __ Lab File ID: GH091647804
Level: ( low/med) LOW Date Received: 10/04/89
\ Moisture: not dee.~ dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/10/89
GPC Cleanup: (Y/N) IL_ pH: 5.4 Dilution Factor: 1,00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 380 u
lll-44-4---~----bis(2-Chloroethyl)Ether 380 u
95-57-8---------2-Chlorophenol 380 u
541-73-1--------l,3-Dichlorobenzene 380 u
106-46-7--------l,4-Dichlorobenzene 380 u
100-51-6--------Benzyl Alcohol 380 u
95-50-1---------1,2-Dichlorobenzene 380 u
95-48-7---------2-Methylphenol 380 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 380 u
106-44-5--------4-Methylphenol 380 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 380 u
67-72-1---------Hexachloroethane 380 u
98-95-3---------Nitrobenzene 380 u
78-59-1---------Isophorone 380 u
88-75-5---------2-Nitrophenol 380 u
105-67-9--------2,4-Dimethylphenol 380 u
65-85-o---------Benzoic Acid 1900 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 380 u
120-83-2--------2,4-Dichlorophenol 380 u
120-02-1--------1,2,4-Trichlorobenzene 380 u
91-20-3---------Naphthalene 380 u
106-47-8-~------4-Ctiloroaniline 380 u
87-68-3---------Hexachlorobutadiene ' 380 u
59-50-7---------4-Chloro-3-Methylphenol 380 u
91-57-6---------2-Methylnaphthalene 380 u
77-47-4---------Hexachlorocyclopentadiene __ 380 u
88-06-2---------2,4,6-Trichlorophenol 380 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
91-58-7---------2-Chloronaphthalene 380 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalate 380 u
208-96-8--------Acenaphthylene 380 u
606-20-2--------2,6-Dinitrotoluene 380 u
FORM I SV-l 1/87 Rev
JJS
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEM LABS Contract: C,2-88)-REVS
SL-19-l
Lab Code : · COHPU Case No.: 17902 SAS No.: S 0G No. : .,_7.,.0 __
I Matrix: (soil/water) SOIL Lab Sample ID: 291647
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sample wt/vol: 30,0 (g/mL) L_ Lab File ID: GH091647804
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ---1..4. dee. .Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/10/!19
GPC Cleanup: (Y/N) IL_ pH: 5,4 Dilution Factor: ~l~,_,.o_,.o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1_900
83-32-9---------Acenaphthene 380
Sl-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
132-64-9--------Dibenzoturan 380
121-14-2--------2,4-Dinitrotoluene 380
84-66-2---------Diethylphthalate 380
7005-72-3-------4-Chlorophenyl-phenylether_ 380
86-73-7---------Fluorene 380
100-01-6--------4-Nitroaniline 1900
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900
86-30-6---------N-Nitrosodiphenylamine (1)_ 380
101-55-3--------4-Bromophenyl-phenylether __ 380
118-74-1--------Hexachlorobenzene 380
87-86-5---------Pentachlorophenol 1900
85-01-8---------Phenanthrene 380
120-12-1--------Anthracene 380
84-74-2---------Di-n-Butylphthalate 380
206-44-0--------Fluoranthene 380
129-00-o--------Pyrene 380
85-68-7---------Butylbenzylphthalate 380
91-94-1---------3,J'-Dichlorobenzidine 770
56-55-3---------Benzo(a)Anthracene 380
218-01-9--------Chrysene 380
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 120
117-84-o--------Di-n-octyl Phthalate 380
205-99-2--------Benzo(b)Fluoranthene 380
207-08-9--------Benzo(k)Fluoranthene 380
50-32-8---------Benzo(a)Pyrene 380
193-39-5--------Indeno(l,2,3-cd)Pyrene 380
53-70-3---------Dibenzo (.a, h) Anthracene 380
191-24-2--------Benzo(g,h,i)Perylen• 380
(1) -Cannot be separated from Diphenylamine
Q
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FORM I SV-2 1/87 Rev.
--,.:_:_:--.· -·· .. -·-··--JJ7
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D
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name:-COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
30.0 (g/mL) _G_
LOW
% Moisture: not dee. ___li dee.
SAS No.: soc
Lab Sample ID:
Lab File IO:
Date Received:
Date Extracted:
EPA SAMPLE NO.
SL-19-l
No.: 70
291647
GHQ9l647B04
10/04/89
lQiQS/89
Extraction: _ (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) tL,, pH: 5.4
Date Analyzed: lOil0/89
Dilution Factor: l,OQ -~--
Number TICs found: ..J
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGiKG
RT EST. CONC.
===============::a ==n==-====================== =-=-====== :a=i===========
l. BLANK CONTAMINANT 5.23 230
FORM I SV-TIC
Q
=====
BJ
1/87 Rev.
----~-136 -------
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-20-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL· Lab Sample ID: 291§48
Sampl_e wt/vol: 30.0 (g/mL) Si_ Lab File ID: GH091648B04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. ---1.i dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~-Date Analyzed: 10/10/89
GPC Cleanup: (Y/N) Ii.._ pH: 5, 6 Dilution Factor: =l~,o~o.__
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 380
lll-44-4--------bis(2-Chloroethyl)Ether 380
95-57-8---------2-Chlorophenol 380
541-73-1--------l,3-Dichlorobenzene 380
106-46-7--------l,4-Dichlorobenzene 380
100-51-6--------Benzyl Alcohol 380
95-50-1---------l,2-Dichlorobenzene 380
95-48-7---------2-Methylphenol 380
39638-32-9------bis(2-Chloroisopropyl)Ether_ 380
106-44-5--------4-Methylphenol 380
621-64-7--------N-Nitroso-Di-n-Propylamine __ 380
67-72-1---------Hexachloroethane 380
98-95-3---------Nitrobenzene 380
78-59-1---------Isophorone 380
88-75-5---------2-Nitrophenol 380
105-67-9--------2,4-Dimethylphenol 380
65-85-o---------Benzoic Acid 1900
lll-9l-l--------bis(2-Chloroethoxy)Methane_. 380
120-83-2--------2,4-Dichlorophenol 380
120-02-1--------l,2,4-Trichlorobenzene 380
91-20-3---------Naphthalene 380
106-47-8--------4-Chloroaniline 380
87-68-3---------Hexachlorobutadiene 380
59-50-7---------4-Chloro-3-Methylphenol 380
91-57-6---------2-Methylnaphthalene 380
77-47-4---------Hexachlorocyclopentadiene __ 380
88-06-2---------2,4,6-Trichlorophenol 380
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 380
88-74-4---------2-Nitroaniline 1900
131-11-3--------Dimethyl Phthalate 380
208-96-8--------Acenaphthylene 380
606-20-2--------2,6-Dinitrotoluene 380
Q
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FORM I SV-1 1/87 Rev.
JJ5
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: 12-881-REVS
SL-20-l
Lab Code: COMPU Case No.: 17902 SAS No.: ___ SDG No.: .,_7.,,_0 __
Matrix: (soil/water) SOIL Lab Sample ID: ~2~9~1~6~4~8 __ _
Sample wt/vol: JO,O (g/mL) _G_
LOW
Lab File ID: GH091648B04
( low/med) Date Received: 10/04/89
% Moisture: not dee. _.l,i ·
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti_
dee.
pH:
~
5.6
Date Extracted: 10/05/89
Date Analyzed: 10/10/89
Dilution Factor: 1,00·
CAS NO. COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/Kg) UGIKG
.
99-09-2---------3-Nitroaniline 1900
83-32-9---------Acenaphthene 380
51-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
132-64-9--------Dibenzoturan 380
121-14-2--------2,4-Dinitrotoluene 380
84-66-2---------Diethylphthalate 380
7005-72-3-------4-Chlorophenyl-phenylether_ 380
86-73-7---------Fluorene 380
100-01-6--------4-Nitroaniline 1900
534-52-1--------4,6-Di~itro-2-Methylphenol __ 1900
86-30-6---------N-Nitrosodiphenylamine (l)_ 380
101-55-3--------4-Bromophenyl-phenylether_ 380
118-74-1--------Hexachlorobenzene 380
87-86-5---------Pentachlorophenol 1900
85-01-8---------Phenanthrene 380
120-12-1--------Anthracene 380
84-74-2---------oi-n-Butylphthalate 52
206-44-0--------Fluoranthene 380
129-oo-o--------Pyrene 380
85-68-7---------Butylbenzylphthalate 380
91-94-1---------3,3'-Dichlorobenzidine 770
56-55-3---------Benzo(a)Anthracene 380
218-01-9--------chrysen• 380
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 180
117-84-o--------oi-n-octyl Phthalate 380
205-99-2--------Benzg(b)Fluoranthene 380
207-08-9--------~nzo(k)Fluoranthene 380
so-32-0--------7Benzo(a)Pyrene 380
193-39-5--------Indeno(l,2,3-cd)Pyrene 380
53-70-3---------Dibenzo(a,h)Anthracene 380
191-24-2--------Benzo(g,h,i)Perylene 380
(l) -cannot be separated trom Diphenylamine
Cl
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FORM I sv-2 l/87 Rev·.
134
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: (2-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received:
'!; Moisture: not dee. ___..l.i dee. Date Extracted:
EPA SAMPLE NO.
SL-20-1
No.: 70
291648
GH091648804
10/04/89
10/05/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lf_ pH:
S.Qru;
5,6
Date Analyzed: 10/10/89
Dilution Factor: l,00
Number TICs found: --1,2.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. ----=-=----==-== ma===2==2--==-=----=--=~==== :g::::s===-== =•===========
1. ALDOL 6.15 270
2. ALDOL 6.60 230
3. UNKNOWN 13.54 350
4. UNKNOWN 13.62 430
5. UNKNOWN 15.14 460
6. UNKNOWN 15.30 1400
7. UNKNOWN 15.62 270
8. UNKNOWN 16.27 580
9. UNKNOWN 16.89 580
10. UNKNOWN 17.10 310
11. UNKNOWN 17.55 500
12. UNKNOWN 17.65 270
13. UNKNOWN 18.30 390
14. UNKNOWN 18.35 230
15. UNKNOWN 18.50 150
16. UNKNOWN 18.94 270
17. UNKNOWN 19.35 230
18. UNKNOWN 19.85 310
19. UNKNOWN 20.49 230
20 • UNKNOWN 21.17 270
21. UNKNOWN 22.19 310
22. UNKNOWN 23.52 390
FORM I SV-TIC
Q
-====
AJ
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1/87 Rev.
133
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
SL-21-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ..c7_,,0 __
Matrix: (soil/water) SOIL Lab Sample ID: .,2..,_9_.1.,.6_,.4.,,_9 ___ _
sample wt/vol_: JO.o (g/mL) ~ Lab File ID: GH091649C04
Level: ( low/med) LOW
% M_oisture: not dee. --1 dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/11/89 Extraction: SQtiC
GPC Cleanup:
( SepF / Cont/ sonc)
(Y/N) li._ pH: 5.6 Dilution Factor: ~1~1.,.0.,.0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 340
lll-44-4--------bis(2-Chloroethyl)Ether 340
95-57-8---------2-Chlorophenol 340
541-73-1--------1,3-Dichlorobenzene 340
106-46-7--------1,4-Dichlorobenzene 340
100-51-6--------Benzyl Alcohol 340
95-50-1---------1,2-Dichlorobenzene 340
95-48~7---------2-Methylphenol 340
39638-32-9------bis(2-Chloroisopropyl)Ether_ 340
106-44-5---~~---4-Methylphenol 340
621-64-7--------N-Nitroso-Di-n-Propylamine_· _ 340
67-72-1---------Hexachloroethane 340
98-95-3---------Nitrobenzene 340
78-59-1---------Isophorone -340
88-75-5---------2-Nitrophenol 340
105-67-9--------2,4-Dimethylphenol 340
65-85-0---------Benzoic Acid 1600
lll-9l-l--------bis(2-Chloroethoxy)Methane __ 340
120-83-2--------2,4-Dichlorophenol 340
120-s2-1--------1,2,4-Trichlorobenzene 340
91-20-3---------Naphthalene 430
106-47~8--------4-Chloroaniline 340
87-68-3---------Hexachlorobutadiene 340
59-50-7---------4-Chloro-3-Methylphenol 340
91-57-6--~------2-Methylnaphthalene 340
77-47-4---------Hexachlorocyclopentadiene __ 340
88-06-2---------2,4,6-Trichlorophenol 340
95-95-4---------2,4,5-Trichlorophenol 1600
91-58-7---------2-Chloronaphthalene 340
88-74-4---------2-Nitroaniline 1600
131-11-3--------Dimethyl Phthalate 340
208-96-8--------Acenaphthylene 340
. 606-20-2--------2,6~Dinitrotoluene 340
Q
u u u u
u u u u u u u u u u
u u u u u u
u u u
J u u u u u u u u
FORM I sv-1 1/87 Rev.
::... -ZZP■-Z:::.·7tr SRIIPLE DRT/¥ -::· -.... ---132
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88l-REVS
SL-21-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .!...70,,___
Matrix: (soil/water) SOIL Lab sample ID: .,.2_._9.a.l.,._6 419,,__ __ _
sample wt/vol: 30.0 (g/mL) li._
LOW
Lab File ID: GH091649C04
Level: ( low/med) Date Received: 10/04/89
% Moisture: not dee. -1 dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (¥/N) IL_ pH: 5.6
Date Extracted: 10/05/89
Date Analyzed: 10/11/89
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1600
83-32-9---------Acenaphthene 210
51-28-5---------2,4-Dinitrophenol 1600
100-02-7--------4-Nitrophenol 1600
132-64-9--------Dibenzoturan 170
121-14-2--------2,4-Dinitrotoluene 340
84-66-2---------Diethylphthalate 340
7005-72-3-------4-Chlorophenyl-phenylether __ 340
86-73-7---------Fluorene 250
100-01-6----~---4-Nitroaniline 1600
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1600
86-30-6---------N-Nitrosodiphenylamine (l)_ 340
101-55-3--------4-Bromophenyl-phenylether __ 340
118-74-1--------Hexachlorobenzene 340
87-86-5---------Pentachlorophenol 1600
' 1100 85-01-8---------Phenanthrene
120-12-1--------Anthracene 220
84-74-2---------Di-n-Butylphthalate 140
206-44-o--------Fluoranthene 1100
129-00-0--------Pyrene 690
85-68-7---------Butylbenzylphthalate 340
91-94-1---------3,3'-Dichlorobenzidine 680
56-55-3---------Benzo(a)Anthracene 570
218-01-9--------Chrysene 570
117-8l-7--------bis(2-Ethylhexyl)Phthalate_ 480
117-84-0--------Di-n-octyl Phthalate 340
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 320
50-32-8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 200
53-70-3---------Dibenzo(a,h)Anthracene 340
191-24-2--------Benzo(g,h,i)Perylene 180
(1) -_Cannot be separated trom Diphenylamine
Q
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FORM I sv-2 l/87 Rev.
J 31
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-21-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291649
Sample wt/vol: JO,O (g/mL) ~ Lab File ID: GH091649C04
•
Level: ( low/med) LOW Date Received: 10/04/89
i Moisture: not dee·. ----1 dee. Date Extracted: l0/Q5/89
Extraction: (SepF/Cont/Sonc)
(Y/N) lL,_
Date Analyzed: 10/11/89
GPC Cleanup: pH: 5,6 Dilution Factor: al~-~oo,.__
Number TICS found: ...l.J.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
-RT EST. CONC.
--==--=------=--==------=-==m-=------==--=== ======== =============
1. ALDOL 6.18 650
2. ALDOL 6.60 930
3. BLANK CONTAMINANT 6,. 70 580
4. UNKNOWN 7.63 2300
5. UNKNOWN HYDROCARBON 8.49 2400
6. UNKNOWN HYDROCARBON 8.60 3000
7. UNKNOWN HYDROCARBON 8.82 1600
8. UNKNOWN 8.92 1100
9. UNKNOWN SUBSTITUTED HYDROC~ 9.00 1000
10. UNKNOWN HYDROCARBON 9.07 1100
11. UNKNOWN SUBSTITUTED HYDROCAR 9.29 2600
12. 3891-98-3 DODECANE, 2,6,10-TRIMETHYL-9.87 1700
13. 629-59-4 TETRADECANE 10.04 1800
14. UNKNOWN 10.09 960
15. UNKNOWN HYDROCARBON 10.49 1800
16. UNKNOWN HYDROCARBON 10.74 2200
17. UNKNOWN HYDROCARBON 11.39 2000
18. TETRAMETHYLBUTYL PHENOL ISOM 11.57 2600
19. UNKNOWN SUBSTITUTED HYDROCAR 12.00 3000
20. UNKNOWN SUBSTITUTED HYDROCAR 13.15 1800
2L UNKNOWN HYDROCARBON 15.15 1100
22. UNKNOWN 15.24 1900
23. UNKNOWN 15.35 1300
FORM I SV-TIC
-=-·-.. __ ::_::=.:.._ U"P 2-ife -~ DRTR-SlJIIIIUlRV
i ~
Q
=====
AJ
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BJ
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1/87 Rev.
138
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: <2-88}-REVS
SL-22-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7,._0 __
Matrix: (soil/water) SOIL Lab Sample ID: ,._2.if..9.._2,,._J.;16"'----
Sample wt/vol: 30.0 (g/mL) L-Lab File ID: GH092Jl6A20
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ----11 dee. Date Extracted: 10/06/89
Date Analyzed: 10/16/89
Dilution Factor: 1,00
Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) Ii_ pH: 7,1
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--~-----Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-oi-n-Propylamine_ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-0---------Benzoic Acid 1800
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 370
120-83-2--------2,4-Dichlorophenol 370
120-82-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalen• 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
Q
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u u
u
FORM I sv-1 1/87 Rev
129
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: C2-BB)-REVS
SL-22-1
Lab Code: COMPU case No.: l 7902 SAS No.: SOG No.: .,_7,._0 __
Matrix: (soil/water) SOIL Lab Sample ID: .,.2"9.,..2,,_3a:l6,._ __ _
Sample wt/vol: 30.0 (g/mL) L__ Lab File ID: GH092316A20
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ---1.l dee. Date Extracted: 10/06/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(¥/N) Ii._ pH: 7,1
Date Analyzed: l0/16/89
Dilution Factor: ~i~-9~0"-_
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-7--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------oiethylphthalate 370
7005-72-3-------4-Chlorophenyl-phe~ylether_ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800
86-30-6---------N-Nitrosodiphenylamine (l)_ 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------Di-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-00-0--------Pyrene 370
85-68-7~--------Butylbenzylphthalate 370
91-94-1---~-----3,3'-Dichlorobenzidine 740
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 370
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 190
117-84-o--------oi-n-octyl Phthalate 370
205-99-2--------Benz6(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 370
(1) -Cannot be separated from Diphenylamine
Q
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u u u u u
u u u u u u
u u u u u u u u
J u u u u u u u
FORM I sv-2 1/87 Rev.
-----·-------'-_ UJ•Z 7• SR/fPLE DRTR SUIIIUHIV 128
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVEL'l IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG
Matrix: ( soil/water) SOIL Lab Sample ID:
Sample wt/vol: Jo.o (g/mL) L_ Lab File ID:
Level: ( low/med) LOW Date Received:
% Moisture: not dee. ---1.l. dee. Date Extracted:
EPA SAMPLE NO.
SL-22-1
No.: 70
292316
GH092316A20
10/05/89
10/06/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H_ pH:
~
7.1
Date Analyzed: 10/16/89
Dilution Factor: _1~1 0_o __
Number TICs found: __J_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.
================ m=======================-=== a=======· =============
1. BLANK CONTAMINANT 5.22 260
2. BLANK CONTAMINANT 6.23 1200
3 . UNKNOWN 19.04 150
FORM I SV-TIC
Q
=====
BJ
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J
1/87 Rev.
127
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lB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-23-l
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
SAS No.: SDG No.: -'-7,,_0 __
Lab Sample ID: .2~9~2~3~15"----
Sample wt/vol: 30,0 (g/mL) s;;__ Lab File ID: GH092315A20
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee, ----1.l dee.
Extraction: (SepF/Cont/Sonc)
(Y/N) li,_
~
6.5
Date Extracted: 10/06/89
Date Analyzed: 10/16/89
Dilution Factor: ~i •• ~o~o __ GPC Cleanup: pH:
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50~1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine_ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-0---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 .
120-83-2--------2,4-Dichlorophenol 370
120-s2-1--------l,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene_ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol ' 1800
91-58-7---------2-Chloronaphthalene 370
88~74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
Q
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u
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FORM I SV-l l/87 Rev.
~!ltnt ?e SRIIPLE DRTR SUJIYIIFM'1' -126
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-23-1
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
SAS No.: SDG No.: .._70,.___
Lab Sample ID: .._2 ,,_9 .._23,,._1"'5"-----
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: GH0923l5A20
Leve 1: ( low/med) LOW Date Received: 10/05/89
\ Moisture: not dee. __ll dee. Date Extracted: 10/06/89
Date Analyzed: 10/16/89 Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Ji._ pH: 6.5 Dilution Factor: ~1~1 ~0~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG(KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-7--------4-Nitrophenol 1800 u
132-64-9--------Dibenzoturan 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7065-72-3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 370 u
101-55-3--------4-Bromophenyl-phenylether __ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
as-01-0---------Phenanthrene 49 J
120-12-1-------~Anthracen• 370 u
84-74-2---------Di-n-Butylphthalate 370 u
206-44-0--------Fluoranthene 40 J
129-00-o--------Pyren• 69 J
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------J,J'~Dichlorobenzidine 750 u
56-55-3---------Benzo(a)Anthracena 370 u
210-01-9--------Chrysen• 48 J
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 410
117-84-0--------Di-n-Octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -Cannot be separated' from Diphenylamine
FORM I sv-2 1/87 Rev.
125
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
EPA SAMPLE NO.
SL-23-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Level: ( low/med) LOW
% Moisture: not dee. ---1.2. dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...._ pH:
Number TICs found: ~
CAS NUMBER COMPOUND
L-
6.5
NAME
Lab Sample IO: 292315
Lab File IO: GH092315A20
Date Received: 10/05/89
Date Extracted: 10l06l89
Date Analyzed: 10l16l89
Dilution Factor: ~i~-~9~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGlKG
RT EST. CONC. Q
============-==== ma::::::--=-=-=•-~=-------====== z:;11::::::::===== ============-m====
L BLANK CONTAMINANT 5.17 230 BJ
2. ALDOL 6.18 1500 AJ
FORM I SV-TIC l/87 Rev.
124
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
EPA SAMPLE NO.
SL-24-l
No.: 70
I Matrix: (soil/water) SOIL Lab Sample ID: 292321
I
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m
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D
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I
Sample wt/vol: 30,0 (g/lllL) L.._. Lab File ID: GH092321C20
Level: ( low/med) LOW Date Received: 10/05/89
\ Molsture: not dee. ----1.i dee. Date Extracted: 10/06/89
Extraction: (SepF/Cont/Sonc)
(Y/N) IL.
Date Analyzed: 10(19(89
GPC Cleanup: pH: 6,7 Dilution Factor: .1~1~0~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 380 u
lll-44~4--------bia(2-Chloroethyl)Ether 380 u
95-57-8---------2-Chlorophenol 380 u
541-73-1--------l,3-Dichlorobenzene 380 u
106-46-7--------l,4-Dichlorobenzene 380 u
lOO-Sl-6--------Benzyl_Alcohol 380 u
95-50-1---------1,2-oichlorobenzene 380 u
95-48-7---------2-Kethylphenol 380 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 380 u
106-44-5--------4-Kethylphenol 380 u
621-64-7--------N-Nitroao-Di-n-Propylamine __ 380 u
67-72-1---------Hexachloroethane 380 u
98-95-3---------Nitrobenzene 380 u
78-59-1---------Iaophorone 380 u
88-75-5---------2-Nitrophenol 380 u
105-67-9--------2,4-Dimethylphenol 380 u
65-85-o---------Benzoic Acid 45 J
lll-91-l--------bis(2-Chloroethoxy)Kethane_ 380 u
120-83-2--------2,4-Dichlorophenol 380 u
120-02-1--------1,2,4-Trichlorobenzene 380 u
91~20-3---------Naphthalene 380 u
106-47-8--------4-Chloroaniline 380 u
87-68-3---------Hexachlorobutadiene 380 u
59-50-7---------4-Chloro-3-Kethylphenol 380 u
91-57-6---------2-Methylnaphthalene 380 u
77-47-4---------Hexachlorocyclopentadiene_ 380 u
88-06-2---------2,4,6-Trichlorophenol 380 u
95-95-4---------2,4,S-Trichlorophenol 1900 u
91-58-7---------2-Chloronaphthalene 380 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalate 380 u
208-96-8--------Acenaphthylene 84 J
606-20-2--------2,6-Dinitrotoluene 380 u
FORM I sv-1 1/87 Rev.
17982--78 SRlll'LE DRTR SUIIIIRIIY 123
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lC :
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-24-1
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_70,.___
Matrix: (soil/water) SOIL Lab Sample IO: .._2.,_9.._23"'2._l..____ __ _
Sample wt/vol: 30,0
Level: (low/med) ~LO~W...__
( g/m.L) L_ Lab File IO: GH092321C20
Date Received: 10/05/89
\ Moisture: not dee. ---1.i dee. Date Extracted: 10/06/89
Extraction:
GPC Cleanup:
( SepF / cont/ Sonc)
(Y/N) H_ pH:
~
6,7
Data Analyzed: 10/19/89
Dilution Factor: 1,00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2--~------3-Nitroanilina 1900
83-32-9---------Acenaphthene 380
51-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
132-64-9--------Dibenzoturan 380
121-14-2--------2,4-Dinitrotoluene 380
84-66-2---------Diathylphthalata 380
7005-72-3-------4-Chlorophanyl-phanylathar __ 380
86-73-7---------Fluorane 380
100-01-6--------4-Nitroanilina 1900
534-52-1--------4,6-Dinitro-2-Mathylphanol __ 1900
86-30-6---------N-Nitroaodiphanylamine (1)_ 380
101-55-3--------4-Bromophanyl-phanylathar __ 380
118-74-1--------Hexachlorobanzene 380
87-86-5--~------Pantachlorophanol 120
85-01-8---------Phenanthrene 160
120-12-1--------Anthracene 380
84-74-2---------Di-n-Butylphthalate 380
206-44-0-----.---Fluoranthene 110
129-00-0--------Pyrene 170
85-68-7---------Butylbenzylphthalate 380
91-94-1---------3,3'-Dichlorobanzidine 770
56-55-3---------Benzo(a)Anthracana 81
218-01-9--------Chrysene 110
117-81-7--------bis(2-Bthylhexyl)Phthalate_ 55
117-84-o--------oi-n-octyl Phthalat• 380
205-99-2--------Benzo(b)Fluoranthene 120
201-oa-9--------BenzO(k)Fluoranthane 120
50-32-8---------Benzo(a)Pyrene 130
193-39-5--------Indeno(l,2,3-cd)Pyrena 64
53-70-3---------Dibenzo(a,h)Anthracane · 380
191-24-2--------Benzo(g,h,i)Perylana 79
(1) -cannot be separated from Diphenylamine
Q
u u u u u u u u u u u u u
U,
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JX
JX
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J u
J
FORM I sv-2 1/87 Rev.
122
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEM LABS contract: (2-881-REVS
l~ b Code: COHPU Case No.: 17902 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample ID:
Sar,,ple wt/vol: 30,0 (g/llL) ~ Lab File ID:
Level: (low/med) r..ow Date Received:
" Moisture: not dee. _ll dee. Date Extracted:
EPA SAMPLE NO.
SL-24-1
No.: 70
292321
GH092J21C20
10/05/89
10/0§/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H...._ pH: 6.7
Date Analyzed: 10/19/89
Dilution Factor: 1.00
Number TICs found: ~
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
===============-••==s======~•======•=-==-•• ••:a•=---a:i::z=========•u
l. ALDOL 6.02 1000
2. ALDOL 6.53 740
3. UNKNOWN 14.70 810
4. UNKNOWN 16.05 700
5. UNKNOWN 16.35 660
6. UNKNOWN 16.50 810
7. UNKNOWN 16.79 620
8. UNKNOWN 16.92 620
9. UNKNOWN 17.09 540
10. UNKNOWN 17,25 770
11. UNKNOWN 17,70 540
12. UNKNOWN 18.20 890
13. UNKNOWN 18.37 1600
14. UNKNOWN 18.52 1200
15. UNKNOWN 18.69 4300
16. UNKNOWN 18.84 1300
17. UNKNOWN 18.97 1100
18. UNKNOWN 19,19 1200
19. UNKNOW 19.39 620
20. UNKNOWN 19.52 620
21. UNKNOWN 19.77 660
22. UNKNOWN 21. 45 770
FORM I SV-TIC
Q
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l/87 Rev.
121
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18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-25-1
Lab Name: COMPUCHEM LABS contract: C2-88l-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ~79~-
Matrix: (soil/water) SOIL Lab Sample IO: 292322
Sample wt/vol: JO.O (g/mL) ~ Lab File IO: GH092J22c20
Level: (low/med) LO__,W,___ Date Received: 10/05/89
% Moisture: not dee •. ---1.1 dee. Date Extracted: 10/06/89
Extraction: ~ Date Analyzed: 10/19/89
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) If_ pH: 6.8 Dilution Factor: -1~-~9~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/I<G Q
108-95-2--------Phenol 400 ·u
lll-44-4--------bis(2-Chloroethyl)E!her 400 u
95-57-8---------2-Chlorophenol 400 u
541-73-1--------1,J-Dichlorobenzene 400 u
106-46-7-------~l,4-Dichlorobenzene 400 u
100-51-6--------Benzyl Alcohol 400 u
95~so-1---------1,2-oichlorobenzene 400 u
95-48-7---------2-Methylphenol 400 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 400 u
106-44-5--------4-Methylphenol 400 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 400 u
67-72-1---------Hexachloroethane 400 u
98-95-3---------Nitrobenzene 400 u
78-59-1---------Isophorone 250 J
88-75-5---------2-Nitrophenol 400 u
105-67-9--------2,4-Dimethylphenol 400 u
65-85-o---------aenzoic Acid 1900 u
lll-9l-l--------bis(2-Chloroethoxy)Methane __ 400 u
120-83-2--------2,4-Dichlorophenol 400 u
120-82-l--------l,2,4-Trichlorobenzene 400 u
91-20-3---------Naphthalene 400 u
106-47-8--------4-Chloroaniline 400 u
87-68-3---------Hexachlorobutadiene 400 u
59-50-7---------4-Chloro-J-Methylphenol 400 u
91-57-6---------2-Methylnaphthalene 68 J
77-47-4---------Hexachlorocyclopentadiene __ 400· u
88-06-2---------2,4,6-Trichlorophenol 400 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
91-58~7---------2-Chloronaphthalene 400 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------oimethyl Phthalate 400 u
208-96-8--------Acenaphthylene 400 u
606-20-2--------2,6-Dinitrotoluene 400 u
· FORM I sv-1 1/87 Rev.
JA.;
_-,---=---:_=..~ 2 7'.-SRIIPLE DRTR S.U/f/'IRRV ~
128
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: (2-881-REVS
SL-25-l
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 292322
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH092322C20
Level: (low/med) ~r.o,.,,.w __ Date Received: 10/05/89
% Moisture: not dee. ___l.1 dee. Date Extracted: 10/0§/89
Extraction: ( SepF /Cont/ Sonc) ~ Date Analyzed: 10/19/89
GPC Cleanup: (Y/N) H,__ pH: §,8 Dilution Factor: ~l~•~Q~Q __
CONCENTRATION 'UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1900 u
83-32-9---------Acenaphthene 400 u
51-28-5---------2,4-Dinitrophenol 1900 u .
100-02-7--------4-Nitrophenol 1900 u
132-64-9--------Dibenzoturan 400 u
121-14-2--------2,4-Dinitrotoluene 400 u
84-66-2---------Diethylphthalate 400 u
7005-72-3-------4-Chlorophenyl-phenylether_ 400 u
86-73-7---------Fluorene 400 u
100-01-6--------4-Nitroaniline 1900 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900 u
86-30-6--~------N-Nitrosodiphenylamine (1)_ 400 u
101-55-3--------4-Bromophenyl-phenylether __ 400 u
118-74-1--------Hexachlorobenzene 400 u
87-86-5---------Pentachlorophenol 1900 u
85-01-8---------Phenanthrene 400 u
120-12-1--------Anthracene 400 u
84-74-2---------Di-n-Butylphthalate 190 3
206-44-0--------Fluoranthene 400 u
129-oo-o--------Pyrane 400 u
85-68-7---~-----Butylbenzylphthalate 400 u
91-94-1---------3,3'-Dichlorobenzidine 800 u
56-55-3---------Benzo(a)Anthracene 400 u
218-01-9--------Chrysene 400 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 150 3
117-84-0--------Di-n-Octyl Phthalate 400 u
205-99-2--------Benzo(b)Fluoranthene 400 u
207-08-9--------Benzo(k)Fluoranthene 400 u
50-32-8---------Benzo(a)Pyrene 400 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 400 u
53-70-3---------Dibenzo(a,h)Anthracene 400 u
191-24-2--------Benzo(g,h,i)Perylene 400 u
(1) -cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
. -· ----·--z7ge2 78. SRIIPLE DRTR SUIIIIIHlV . 119
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: C2-88l -REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: . (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.0 (g/mL) f.i_ Lab File ID:
Level: (low/med) LOW Date Received:
% Moisture: not dee. -11. dee. Date Extracted:
EPA SAMPLE NO.
SL-25-1
No.: 70
29jp22
GH092322C20
10/05/89
10/06/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H,_ pH: 6.8
Date Analyzed: 10/19/89
Dilution Factor: al~,~o~o __
Number TICs found:_..§.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
===============-=---====----==-=------===----= =====-=-== =============
1. ALDOL 6.00 400
2. ALDOL 6.50 400
3. UNKNOWN 16.02 320
4. UNKNOWN 17.29 240
5. UNKNOWN 23.87 360
6. UNKNOWN 24.82 3500
FORM I SV-TIC
17"'2 7• SRIU"LE DRTR SU/f1UIRY
Q
=====
AJ
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1/87 Rev.
118
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18 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-28-l
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 292320
SaJT1ple wt/vol: 30.0 (g/mL) !i__ Lab File ID: G2D92320C20
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. _u dee. Date Extracted: 10/06/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/NJ li...._ pH:
~
6.9
Date Analyzed: 10/19/89
Dilution Factor: ~l~0~,~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/KgJ UG/KG
108-95-2--------Phenol 3800
lll-44-4--------bis(2-Chloroethyl)Ether 3800
95-57-8---------2-Chlorophenol 3800
541-73-1--------l,3-Dichlorobenzene 3800
106-46-7--------l,4-Dichlorobenzene 3800
100-51-6--------Benzyl Alcohol 3800
95-50-1---------l,2-Dichlorobenzene 3800
95-48-7---------2-Methylphenol 3800
39638-32-9------bis(2-Chloroisopropyl)Ether_ 3800
106-44-5--~-----4-Methylphenol 3800
621-64-7--------N-Nitroso-Di-n-Propylamine_ 3800
67-72-1---------Hexachloroethane 3800
98-95-S--~------Nitrobenzene 3800
78-59-1---------Isophorone 3800
88-75-5---------2-Nitrophenol 3800
105-67-9--------2,4-Dimethylphenol 3800
65-85-o---------senzoic Acid 18000
lll-91-l--------bis(2-Chloroethoxy)Methane __ 3800
120-83-2--------2,4-Dichlorophenol 3800
120-02-1--------1,2,4-Trichlorobenzene 3800
91-20-3---------Naphthalene 3800
106-47-8--------4-Chloroaniline 3800
87-68-3---------Hexachlorobutadiene 3800
59-50-7---------4-Chloro-3-Methylphenol 3800
91-57-6---------2-Methylnaphthalene 3800
77-47-4---------Hexachlorocyclopentadiene __ 3800
88-06-2---------2,4,6-Trichlorophenol 3800
95-95-4---------2,4,5-Trichlorophenol 560
91-58-7---------2-Chloronaphthalene 3800
88-74-4---------2-Nitroaniline 18000
131-11-3--------Dimethyl Phthalate 3800
208-96-8--------Acenaphthylene 3800
606-20-2--------2,6-Dinitrotoluene 3800
Q
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FORM I SV-l l/87 Rev.
.. Z7H2 7B SRIIPLE DRTR SUlfl'UlllY . 117
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lnb Name: COMPUCHEM LABS
SL-28-1
Contract: (2-88)-REVS
,.ab Code: COMPU Case No.: 17902 SAS No.: SOG No.: _,_7:,<0 __
:t..,trix: (soil/water) SOIL Lab Sample ID: ~2L9L23~2~o,._ __ _
,,.,"'ple wt/vol: 30.0 (g/mL) ~ Lab File ID: G2092320C20
level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ____u dee.
Extraction: (SepF/Cont/Sone)
Date Extracted: 10/06i89
Date Analyzed: 10/19/89
GPC Cleanup: (Y/N) li..._ pH: 6.9 Dilution Factor: 10.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/l<g) UG/KG Q
99-09-2---------3-Nitroaniline 18000 u
83-32-9---------Acenaphthene 3800 u
51-28-5---------2,4-Dinitrophenol 18000 u
100-02-1--------4-Nitrophenol 18000 u
132-64-9--------Dibenzo!uran 3800 u
121-14-2--------2,4-Dinitrotoluene 3800 u
84-66-2---------Diethylphthalate 3800 u I
7005-72-3-------4-Chlorophenyl-phenylether_ 3800 u
86-73-7---------Fluorene 3800 u
100-01-6--------4-Nitroaniline 18000 u
534-52-1----~---4,6-Dinitro-2-Methylphenol __ 18000 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 3800 u
101-55-3------~-4-Bromophenyl-phenylether __ 3800 u
118-74-1--------Hexaehlorobenzene 3800 u
87-86-5---------Pentachlorophenol 2800 .J
85-01-8---------Phenanthrene 3800 u
120-12-1--------Anthraeene 3800 u
84-74-2---------Di-n-Butylphthalate 3800 u
206-44-0--------Fluoranthene 3800 u
129-00-0--------Pyrene 3800 u
85-68-7---------Butylbenzylphthalate 3800 u
91-94-1---------3,3'-Dichlorobenzidine 7600 u
56-55-3---------Benzo(a)Anthraeene 3800 u
218-01-9--------Chrysene 3800 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 2800 .J
117-84-0--------oi-n-oetyl Phthalate 3800 u
205-99-2--------Benzo(b)Fluoranthene 3800 u
207-08-9--------Benzo(k)Fluoranthene 3800 u
50-32-8---------Benzo(a)Pyrene 3800 u
193-39-5--------Indeno(l,2,3-ed)Pyrene 3800 u
53-70-3---------Dibenzo(a,h)Anthraeene 3800 u
191-24-2--------Benzo(g,h,i)Perylene 3800 u
(1) -cannot be separated !rom D1phenylam1ne
FORM I sv-2 1/87 Rev.
-'f-79112 ·za SRIIPLE DRTR SUIIIIRlilY--116
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
L~b Name: COMPUCHEM LABS Contract: (2-881-REVS
~., b Code: COMPU Case No.: 17902 SAS No.: SDG
EPA SAMPLE NO.
SL-28-1
No.: 70
I ,1~trix: (soil/water) SOIL Lab sample IO: 292320
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30.0 (g/mL) l:i.__ Lab File IO: G2D92320C20
( low/med) LOW
; Moisture: not dee. ___ll dee.
Extraction: (SepF/Cont/Sonc) ~
:;re Cleanup: (Y/N) IL... . pH: 6.9
Number TICs found: ....2.Q
CA.S NUMBER COMPOUND NAME
Date Received: 10(0:;ii~9
Date Extracted: 10/06/89
Date Analyzed:· 10/19/89
Dilution Factor:· .,.1.,.0_._1.,,_o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
----------====== =====•======-============== =====-=== a=========s== =====
1. 17301-32-5 UNOECANE, 4,7-DIMETHYL-7.70 16000 ,1
2 . 17301-32-5 UNOECANE, 4,7-DIMETHYL-10.50 15000 ,1
3. 17301-32-5 UNOECANE, 4,7-DIMETHYL-11.32 20000 ,1
4 . 544,.:75-3 HEXADECANE 12.09 16000 ,1
5. 629-78-7 HEPTADECANE 12.82 22000 ,1
6. 54105-67-8 HEPTADECANE, 2,6-DIMETHYL-13.52 13000 ,1
7. 54105-67-8 HEPTADECANE, 2,6-DIMETHYL-14.19 22000 ,1
8. UNKNOWN HYDROCARBON 15.42 12000 ,1
9. 629-78-7 HEPTADECANE 16.20 23000 ,1
10. 17312-81-l UNOECANE, 3,5-DIMETHYL-16.77 26000 J
11. UNKNOWN 17.57 -13000 J
12. 630-06-8 HEXATRIACONTANE 17.74 13000 ,1
13. UNKNOWN 18.09 17000 J
14. 629-99-2 PENTACOSANE 18.22 17000 ,1
15. 629-99-2 PENTACOSANE 18. 34 16000 J
16. UNKNOWN 18.49 16000 J
17. 629-99-2 PENTACOSANE 18.69 46000 J
18. 629-99-2 PENTACOSANE 19.17 16000 ,1
19. UNKNOWN 21.42 ·16000 J
20. UNKNOWN 20.04 16000 ,1
FORM I SV-TIC 1/87 Rev.
-.-.,--.. -...:::._-.-,-·._. _ .. -_.· l:.T9tl2-7• SRlfP.LE DRTR. SUIIIIRRY 115
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS
. SL-28-lRE
Contract: [2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab sample ID: 292320
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: G3D92320A20
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ---11 dee. Date ·Extracted: 10/Q§/!!9
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti._ pH: !i, 9
Date Analyzed: l0/19/89
Dilution Factor: 10.o
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L.or ug/Kg) UG/KG
108-95-2--------Phenol 3800
lll-44-4--------bis(2-Chloroethyl)Ether 3800
95-57-8---------2-Chlorophenol 3800
541-73-1--------l,3-Dichlorobenzene 3800
106-46-7--------l,4-Dichlorobenzene 3800
100-s1-6--------Benzyl Alcohol 3800
95-50-1---~-----l,2-Dichlorobenzene 3800
95-48-7---------2-Methylphenol 3800
39638-32-9------bis(2-Chloroisopropyl)Ether_ 3800
106-44-5--------4-Methylphenol 3800
621-64-7--------N-Nitroso-Di-n-Propylamine __ 3800
67-72-1---------Hexachloroethane 3800
98-95-3---------Nitrobenzene 3800
78-59-1---------Isophorone 3800
88-75-5---------2-Nitrophenol 3800
105-67-9--------2,4-Dimethylphenol 3800
65-85-o---------Benzoic Acid 18000
lll-9l-l--------bis(2-Chloroethoxy)Methane __ 3800
120-83-2--------2,4-Dichlorophenol 3800
120-82-1--------l,2,4-Trichlorobenzene 3800
91-20-3---------Naphthalene 3800
106-47-8--------4-Chloroaniline 3800
87-68-3---------Hexachlorobutadiene 3800
59-50-7---------4-Chloro-3-Methylphenol 3800
91-57-6---------2-Methylnaphthalene 3800
77-47-4---------Hexachlorocyclopentadiene __ 3800
88-06-2---------2,4,6-Trichlorophenol 3800
95-95-4---------2,4,5-Trichlorophenol 1300
91-58-7---------2-Chloronaphthalene 3800
88-74-4---------2-Nitroaniline 18000
131-11-3--------Dimethyl Phthalate 3800
208-96-8--------Acenaphthylene 3800
606-20-2--------2,6-Dinitrotoluene -3800
Q
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FORM I sv-1 1/87 Rev.
--· ·--·---· ·· ----·----JJ,4
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-28-lRE
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
I Matrix: (soil/water) SOIL Lab Sample ID: 292320
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Sample wt/vol: 30.0 (g/mL) !:L_ Lab File ID: GJD92J20A20
Leve 1: (low/med) I.OW Date Received: 10/05/89
% Moisture: not dee. ----1.l dee. Date Extracted: 10/Q§/89
Extc-action: (SepF/Cont/so·nc) ~ Date Analyzed: 10/19/89
GPC Cleanup: (Y/N) H..._ pH: §,9 Dilution Factor: ~l~0~,~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 18000 u
83-32-9---------Acenaphthene 3800 u
51~28-5---------2,4-Dinitrophenol 18000 u
100-02-7--------4-Nitrophenol 18000 u
132-64-9--------Dibenzoturan 3800 u
121-14-2--------2,4-Dinitrotoluene 3800 u
84-66-2---------Diethylphthalate 3800 u
7005-72-3-------4-Chlorophenyl-phenylether_ 3800 u
86-73-7---------Fluoren• 3800 u
100-01-6--------4-Nitroaniline 18000 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 18000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 3800 u
101-ss-3--------4-Bromophenyl-phenylether_ 3800 u
118-74-1--------Hexachlorobenzene 3800 u
87-86-5---------Pentachlorophenol 5800 J
85-01-8---------Phenanthrene 3800 u
120-12-1--------Anthracene 3800 u
84-74-2---------oi-n-Butylphthalate 1200 J
206-44-0--------Fluoranthene 3800 u
129-00-0--------Pyrene 3800 u
85-68-7---------Butylbanzylphthalate 3800 u
91-94-1---------3,3'-Dichlorobenzidine 7600 u
56-55-3---------senzo(a)Anthracene 3800 u
218-01-9--------Chrysene 3800 u
ll7-8l-7--------bia(2-Ethylhexyl)Phthalate_ 4500
117-84-o--------oi-n-octyl Phthalate 3800 u
205-99-2--------Benze(b)Fluoranthene 3800 u
207-08-9--------Benzo(k)Fluoranthene 3800 u
50-32-e--·-------Benzo ( a) Pyrene 3800 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 3800 u
53-70-3---------Dibenzo(a,h)Anthracene 3800 u
191-24-2--------Benzo(g,h,i)Perylene 3800 u
(1) -Cannot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
:_:i.75H12._ 7• SR/fPLE DRTR SUIIIIRRY 1 JJ
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-28-lRE
Lab Code: COHPU case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL Lab Sample ID: 292320
sample wt/vol: 30,0 (g/mL) l,__ Lab File ID: G3D92320A20
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ---1.1 dee. Date Extracted: 10/06/89
Extraction: (SepF/Cont/Sonc) ~
GPC. Cleanup: (Y/N) tL_ . pH: 6,9
Date Analyzed: 10/19/89
Dilution Factor: 10,0
Number TICs found: .....2.0.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
======.::::111==-=11====-== ==============a============= aa:;1:11::::a::a m==========-==
1. DIMETHYL UNDECANE ISOMER 7.63 32000
2. DIMETHYL UNDECANE ISOMER 10.42 27000
3 . HEPTADECANE ISOMER 11.25 31000
4. HEXADECANE ISOMER 12.00 16000
5. HEPTADECANE ISOMER 12.75 42000
6. UNKNOWN 14.10 42000
7. UNKNOWN HYDROCARBON 14.75 35000
8. UNKNOWN HYDROCARBON 17 .19 26000
9. UNKNOWN 17.40 26000
10. UNKNOWN 17.55 38000
11. UNKNOWN 17.69 32000
12. UNKNOWN 18.04 32000
13. UNKNOWN HYDROCARBON 18.15 35000
14. UNKNOWN HYDROCARBON 18.30 42000
15. UNKNOWN 18.45 46000
16. UNKNOWN 18.62 77000
17. UNKNOWN 18.77 30000
18. UNKNOWN 19.10 32000.
19. UNKNOWN 19.65 27000
20. UNKNOWN 19.95 20000
FORM I SV-TIC
=-·-·-c:_.--·· ·c:..c. -17911~7/T °SRIIPLE ORT/ii ~
Q
•====
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1/87 Rev.
J 12
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS SL-29-l
contract: 12-88)-REVS
Lab Code: coMPU Case No.: 17902 SAS No.: SDG No.: -'-7.,,_0 __
Matcix: (soil/water) SOIL Lab Sample IO: .._2,,_9.._23._1._.9.__ __ _
Sample wt/vol: 30.0 (g/mL) _G_ Lab File IO: GD092319A21
Level: (low/med) LOW Date Received: 10/05/89
1; Moisture: not dee. ___ll dee. Date Extracted: 10/06/89
Date Analyzed: 10/17/89
Dilution Factor: ~5~,.,,_0'----
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) Ii_ pH: 7.3
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1900
lll-44-4--------bis(2-Chloroethyl)Ether 1900
95-57-8---------2-Chlorophenol 1900
541-73-l--------l,3-Dichlorobenzene 1900
106-46-7--------1,4-Dichlorobenzene 1900
100-51-6--------Benzyl Alcohol 1900
95-50-1---------1,2-oichlorobenzene 1900
95-48-7---------2-Methylphenol 1900
39638-32-9------bis(2-Chloroisopropyl)Ether_ 1900
106-44-5--------4-Methylphenol 1900
621-64-7--------N-Nitroso-Oi-n-Propylamine __ 1900
67-72-1---------Hexachloroethane 1900
98-95-3---------Nitrobenzene 1900
78-59-1---------Isophorone 1900
88-75-5---------2-Nitrophenol 1900
105-67-9--------2,4-0imethylphenol 1900
65-as-o---------Benzoic Acid 9200
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 1900
120-83-2--------2,4-0ichlorophenol 1900
120-02-1--------1,2,4-Trichlorobenzene 1900
91-20-3---------Naphthalene 1900
106-47-8--------4-Chloroaniline 1900
87-68-3---------Hexachlorobutadiene 1900
59-50-7---------4-Chloro-3-Methylphenol 1900
91-57-6---------2-Methylnaphthalene 1900
77-47-4---------Hexachlorocyclopentadiene_'_ 1900
88-06-2---------2,4,6-Trichlorophenol 1900
95-95-4---------2,4,5-Trichlorophenol 9200
91-58-7---------2-Chloronaphthalene 1900
88-74-4---------2-Nitroaniline 9200
131-11-3--------Dimethyl Phthalate 1900
208-96-8--------Acenaphthylene 1900
606-20-2--------2,6-0initrotoluene 1900
Q
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FORM I sv-1 1/87 Rev.
----=--.. ~---·--.. ~-ZII· SRIIPLE D11-TR·· SlHIA ev ',,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-29-1
Li'lb Code: COMPU case No.: 17902 SAS No.: SDG No.: .,_7.,.0 __
Matrix: (soil/water) SOIL Lab Sample ID: .2~9&2~31~9,..._ __ _
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: GD092319A21
Level: ( low/med) I,.PW
% Moisture: not dee. ___ll
Extraction: (SepF/Cont/Sonc)
('i/N) tL..
dee.
~
7.3
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/17/89
GPC Cleanup: pH: Dilution Factor: ~5~1.,.0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 9200
83-32-9---------Acenaphthene 1900
51-28-5--------~2,4-Dinitrophenol 9200
100-02-1--------4-Nitrophenol 9200
132-64-9--------Dibenzoturan 1900
121-14-2--------2,4-Dinitrotoluene 1900
84-66-2---------Diethylphthalate 1900
7005-72-3-------4-Chlorophenyl-phenylether __ 1900
86-73-7---------Fluorene 1900
100-01-6--------4-Nitroaniline 9200
534-52-1--------4,6-Dinitro-2-Methylphenol __ 9200
86-30-6---------N-Nitrosodiphenylamine (1)_ 1900
101-55-3--------4-Bromophenyl-phenylether __ 1900
118-74-1--------Hexachlorobenzene 1900
87-86-5---------Pentachlorophenol 9200
85-01-8---------Phenanthrene 1900
120-12-1--------Anthracene 1900
84-74-2---------Di-n-Butylphthalate 470
206-44-0--------Fluoranthene 1900
129-oo-o--------Pyrene 1900
85-68-7---------Butylbenzylphthalate 1900
91-94-1---------3,3'-Dichlorobenzidine 3800
56-55-3---------Benzo(a)Anthracene 1900
218-01-9--------Chrysene 1900
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 1900
117-84-0--------Di-n-octyl Phthalate 1900
205-99-2--------Benzo(b)Fluoranthene 1900
207-08-9--------Benzo(k)Fluoranthene 1900
50-32-8---------Benzo(a)Pyrene 1900
193-39-5--------Indeno(l,2,3-cd)Pyrene 1900
53-70-3---------Dibenzo(a,h)Anthracene 1900
191-24-2--------Benzo(g,h,i)Perylene 1900
(1) -Cannot be separated trom Diphenylamine
FORM I sv-2
Q
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u u u
1/87 Rev.
I ··-. .. -· · -Z::7.flllllZ=..:Za-:._ ·SRlfPLE DR TR SUIIIIRRV 118 ·--· ~.-·-----, ,,.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: <2-881-REVS
EPA SAMPLE NO.
SL-29-1
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: 70
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Leve 1: (low/med) LOW
% Moisture: not dee. __ll dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)·
(Y/N) Ii,_ pH:
Number TICS found: .....2..9.
L-
s..9liC
7,3
CAS NUMBER COMPOUND NAME ·
Lab Sample IO: 292319
Lab File ID: GD092319A2l
Date Received: 10/05/89
Date Extracted: 10/0§/Sll
Date Analyzed: 10/17/89
Dilution Factor: ~5~1 0,._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=======•=====2-= •=•a•••-••=n•a•===========•= ======== =:m=========== -====
1. TETRAMETHYLBUTYLPHENOL ISOME 12.14 15000 J
2. UNKNOWN 15.04 4000 J
3. UNKNOWN 15.19 1900 J
4. 10544-50-0 SULFUR, MOL. (SB) 15.45 4000 J
5. UNKNOWN 15.74 1900 J
6. UNKNOWN 16.64 4000 J
7. UNKNOWN 16.79 1900 · J
8. UNKNOWN 17.07 2300 J
9. UNKNOWN 17 .14 1500 J
10. UNKNOWN 18.14 1300 J
11. UNKNOWN 18,75 1300 J
12. UNKNOWN 18.99 1700 J
13. UNKNOWN 19.07 1200 J
14. UNKNOWN 19.14 1200. J
15. UNKNOWN 19.57 1200 J
16. UNKNOWN 19.89 1500 J
17. UNIOIOWN 19.95 3100 J
18. UNIQIOWN 20.05 3100 J
19. UNKNOWN 20.20 2100 J
20. UNIQIOWN 20.55 2100 J
FORM I SV-TIC 1/87 Rev.
JB9
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
SL-30-1
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 292317
Sample wt/vol: 30.0 (g/mL) !:i_' Lab File ID: G3J92317C21
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ----12. dee. Date Extracted: 10/06/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/20/89
GPC Cleanup: (Y/N) Ji._ pH: 7. 2 Dilution Factor: ~s~,0,._ __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1900
lll-44-4--------bis(2-Chloroethyl)Ether 1900
95-57-8---------2-Chlorophenol 1900
541-73-1--------1,3-Dichlorobenzene 1900
106-46-7--------1,4-Dichlorobenzene 1900
100-51-6--------Benzyl Alcohol 1900
95-50-1---------1,2-0ichlorobenzene 1900
95-48-7---------2-Methylphenol 1900
39638-32-9------bis(2-Chloroisopropyl)Ether_ 1900
106-44-5--------4-Methylphenol 1900
621-64-7--------N-Nitroso-Di-n-Propylamine_ 1900
67-72-1---------Hexachloroethane 1900
98-95-3---------Nitrobenzene 1900
78-59-1---------Isophorone 1900
88-75-5---------2-Nitrophenol 1900
105-67-9-----~--2,4-0imethylphenol 1900
65-85-0---------Benzoic Acid 9400
lll-91-l--------bia(2-Chloroethoxy)Methane_ 1900
120-83-2--------2,4-0ichlorophenol 1900
120-s2-1--------1,2,4-Trichlorobenzene 1.900
91-20-3---------Naphthalene 1900
106-47-8-~------4-Chloroaniline 1900
87-68-3---------Hexachlorobutadiene 1900
59-50-7---------4-Chloro-3-Methylphenol 1900
91-57-6---------2-Methylnaphthalene 240
77-47-4---------Hexachlorocyclopentadiene __ 1900
88-06-2---------2,4,6-Trichlorophenol 1900
95-95-4---------2,4,5-Trichlorophenol 9400
91-58-7---------2-Chloronaphthalene 1900
88-74-4---------2-Nitroanilin• 9400
131-11-3--------0imethyl Phthalate 1900
208-96-8--------Acenaphthylene 1900
606-20-2--------2,6-Dinitrotoluene 1900
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FORM I sv-1 1/87 Rev.
,1.7_g112 .78 SRIIPLE D11Tl1 SUIVIRIIY 188
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: {2-881-REVS
SL-J0-1
Lab Code.: COMPU Case No.: 17902 SAS No.: SDG No.: .:..;70,.___
Matrix: (soil/water) SOIL Lab Sample ID: a2,9~23Ll~7,__ __ _
Sample wt/vol: ·30,0 (g/mL) ~ Lab File ID: G3J92317C21
Level: ( low/med) LOW
% Moisture: not dee. ~ dee.
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/20/89 Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H...._ pH:
~
7.2 Dilution Factor: ~5~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------J-Nitroaniline 9400 u
83-32-9---------Acenaphthene 1900 u
51-28-5---------2,4-Dinitrophenol 9400 u
100-02-1--------4-Nitrophenol 9400 u
132-64-9--------Dibenzoturan 1900 u
121-14-2--------2,4-Dinitrotoluene 1900 u
84-66-2---------Diethylphthalate 1900 u
7005-72-3-------4-Chlorophenyl-phenylether __ 1900 u
86-73-7---------Fluorene 1900 u
100-01-6--------4-Nitroaniline 9400 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 9400 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 1900 u
101-55-3--------4-Bromophenyl-phenylether __ 1900 u
118-74-1-~------Hexachlorobenzene 1900 u
87-86-5---------Pentachlorophenol 3700 J
es-01-e---------Phenanthrene 1200 JX
120-12-1--------Anthracene 1200 JX
84-74-2---------Di-n-Butylphthalate 1900 u
206-44-0--------Fluoranthene 1900 u
129-00-o--------Pyrene 1900 u
85-68-7---------Butylbenzylphthalate 1900 u
91-94-1---------3,J'-Dichlorobenzidine )900 u
56-55-3---------Benzo(a)Anthracene 1900 u
218-01-9--------Chrysene 1900 u
117-Bl-7--------bis(2-Ethylhexyl)Phthalate_ 4700
117-84-o--------Di-n-octyl Phthalate 1900 u
205-99-2--------Benzo(b)Fluoranthene 1900 u
207-08-9--------Benzo(k)Fluoranthene 1900 u
50-32-8---------Benzo(a)Pyrene 1900 u
193-39~5--------Indeno(l,2,3-cd)Pyrene 1900 u
53-70-3---------Dibenzo(a,h)Anthracene 1900 u
191-24-2--------Benzo(g,h,i)Perylene 1900 u
(1) -cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
--·-L7!HIZ.:.71T SR"1PLE DRTR SUlll'fRR¼' 187
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: {2-88)-REVS
EPA SAMPLE NO.
SL-30-1
Lab Code: COMPU .Case No.: 17902 SAS No.: SOG No.: 70
Matrix: (soil/water) SOIL tab· Sample IO: 292317,
Sample wt/vol: 30,0 (g/mL) li__ Lab File IO: G3,Z9~317C21
Level: (low/med) ..,LO...,w,...__ Date Received: 10/05/89
% Moisture: not dee. ----1.2 dee. Date Extracted: 10/06/89
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H._ pH: 7. 2
Date Analyzed: 10/20/89
Dilution Factor: ~s~,Q~--
Number TICs found: ....2.Q
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:,
(ug/L or ug/Kg) UG/KG
RT EST. CONC.
===-============= =======-===================== ==-==-=-=•= =============
1. 124-18-5 OECANE 7.60 9000
2. 29812-79-1 HYOROXYLAMINE, 0-0ECYL-8.59 15000
3. 3913-02-8 1-0CTANOL, 2-BUTYL-11.94 9800
4. 54105-67-8 HEPTAOECANE, 2,6-0IMETHYL-12. 65 8800
5. TETRAMETHYLBUTYLPHENOL ISOME 12.87 37000
6. UNKNOWN HYDROCARBON 13.34 8100
7. UNKNOWN SUBSTITUTED HYOROCAR 14.55 29000
8. UNKNOWN 15.04 11000
9. UNKNOWN SUBSTITUTED HYOROCAR 15.14 12000
10. UNKNOWN 15.35 4500
11. UNKNOWN 15.45 7900
12. UNKNOWN 15;60 11000
13. UNKNOWN HYDROCARBON 15.67 11000
14. UNKNOWN 16.39 18000
15. UNKNOWN 16.50 31000
16. UNKNOWN 17.45 9200
17. UNKNOWN 17.85 8600
18. UNKNOWN 17.90 15000
19. UNKNOWN 19.75 13000
20. UNKNOWN HYDROCARBON 6.60 7900
FORM I SV-TIC
--···· ~··--·--·-· ---· -·----ug•2 711:. SR/fPLE DRTR SultlOW~ ::.
Q
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1/87 Rev.
186
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
SL-J0-2
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 292318
Sample wt/vol: 30.0 (g/mL) L-Lab File ID: GD092318A21
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ----1.1 dee. Date Extracted: 10/0~/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_ pH: 7,1
Date Analyzed: 10/17/89
Dilution Factor: ~s~1~0'----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1900
lll-44-4--------bis(2-Chloroethyl)E~her 1900
95-57-8---------2-Chlorophenol 1900
541-73-1--------1,J-Dichlorobenzene 1900
106-46-7--------1,4-Dichlorobenzene 1900
100-s1-6--------Benzyl Alcohol 1900
95•50-1---------1,2-Dichlorobenzene 1900
95-48-7---------2-Methylphenol 1900
J96J8-32-9------bis(2-Chloroisopropyl)Ether_ 1900
106-44-5--------4-Methylphenol 1900
621-64-7--------N-Nitroso-Di-n•Propylamine __ 1900
67-72-1---------Hexachloroethane 1900
98-95-3---------Nitrobenzene 1900
78-59-1---------Isophorone 1900
88-75-5---------2-Nitrophenol 1900
. 105-67-9--------2,4-Dimethylphenol 1900
65-85-o-----~---Benzoic Acid 9100
lll-91-l--------bis(2-Chloroethoxy)Methane __ 1900
120-83-2--------2,4-Dichlorophenol 1900
120-a2-1--------1,2,4-Trichlorobenzene 1900
91-20-3---------Naphthalene 1900
106-47-8--------4-Chloroaniline 1900
87-68-3---------Hexachlorobutadiene 1900
59-50-7---------4-Chloro-3-Methylphenol 1900
91-57-6---------2-Methylnaphthalene 250
77-47-4---------Hexachlorocyclopentadiene __ 1900
88-06-2---------2,4,6-Trichlorophenol 1900
95-95-4---------2,4,5-Trichlorophenol 9100
91-58-7--~------2-Chloronaphthalene 1900
88-74-4---------2-Nitroaniline 9100
131-11-3--------Dimethyl Phthalate 1900
208-96-8--------Acenaphthylene 1900
606-20-2--------2,6-Dinitrotoluene 1900
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FORM I SV-1 1/87 Rev.
185
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABS contrac·t: 12-BB)-REVS
Lab Code: COMPU Case No.: 17902 SAS No·.: SDG
EPA SAMPLE NO.
SL-30-2
No.:
I· Matrix: (soil/water) SOIL
70
Lab Sample ID: 292318
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Sample wt/vol: 30.0 (g/mL) ~
LOW
Lab File ID: GD092318A2l
Level: . ( low/med) Date Received: 10/05/89
% Moisture: not dee. ---1.2. dee. Date Extracted: 10/Q~/89
Extraction: (SepF/Cont/Sonc) Date' Analyzed: 10/17/89
GPC Cleanup: (Y/N) Ji._ pH: 7.1 Dilution Factor: &5~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 9100
83-32-9---------Acenaphthene 1900
Sl-28-5---------2,4-Dinitrophenol 9100
100-02-1--------4-Nitrophenol 9100
132-64-9--------Dibenzoturan 1900
121-14-2--~-----2,4-Dinitrotoluene 1900
84-66-2---------Diethylphthalate 1900
7005-72-3-------4-Chlorophenyl-phenylether __ 1900
86-73-7---------Fluorene 1900
100-01-6--------4-Nitroaniline 9100
534-52-1--------4,6-Dinitro-2-Methylphenol_ 9100
86-30-6---------N-Nitrosodiphenylamine (l)_ 1900
101-55-3--------4-Bromophenyl-phenylether __ 1900
118-74-1--------Hexachlorobenzene 1900
87-86-5---------Pentachlorophenol 3700
ss-01-s---------Phenanthrene 540
120-12-1----~---Anthracene 1900
84-74-2---------D1-n-Butylphthalate 1900
206-44-0--------Fluoranthene 1900
129-00-0--------Pyrene 1900
85-68-7---------Butylbenzylphthalate 1900
91-94-1---------J,J'-Dichlorobenzidine 3800
56-55-3---------Benzo(a)Anthracene 1900
218-01-9--------Chrysene 1900
117-8,1-7--------bis ( 2-Ethylhexyl) Phthalate_ 4400
117-84-0--------D1-n-Octyl Phthalate 1900
205-99-2--------Benzo(b)Fluoranthene 1900
207-08-9--------Benzo(k)Fluoranthene 1900
so-J2-e---------Benzo{a)Pyrene 1900
193-39-5--------Indeno(l,2,J-cd)Pyrene 1900
53-70-3---------Dibenzo(a,h)Anthracene 1900
191-24-2--------Benzo(g,h,i)Perylene 1900
(l) -cannot be separated from Diphenylamine
Q
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FORM I sv-2 l/87 Rev.
lB4
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: <2-88)-REVS
EPA SAMPLE NO.
SL-30-2
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: ( soil/water) SOIL
sample wt/vol: 30,0 (g/mL)
Level: ( low/med) I.OW
% Moisture:
Extraction:
GPC Cleanup:
not dee. _ll
(SepF/Cont/Sonc)
(Y/N) Ii.._
Number TICs found: _2..Q
dee.
pH:
~
7.1
CAS NUMBER COMPOUND NAME
Lab sample ID: 292318
Lab File ID: GD092318A2l
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/17/89
Dilution Factor: ~5~,9~--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
==•=====-======= ===~====•======a=========•== =-••:a=••= ========-==-= •====
l. UNKNOWN 6.08 6100 J
2. UNKNOWN HYDROCARBON ll.22 13000 J
3 . TETRACHLOROPHENOL ISOMER ll. 72 13000 ·J
4. UNKNOWN HYDROCARBON 12.07 18000 J
5. TETRAMETHYLBUTYLPHENOL ISOME 12.15 53000 J
6. UNKNOWN HYDROCARBON 12.89 10000 J
7. UNKNOWN 14.12 19000 J
8. UNKNOWN 14.80 8400 J
9. 10544-50-0 SULFUR, MOL. (S8) 15.50 10000 J
I 10. UNKNOWN 16.65 9100 J
ll. UNKNOWN HYDROCARBON 18.19 7600 J
12. UNKNOWN 19.60 9100 J .
lJ. UNKNOWN 19.95 9500 J
14. UNKNOWN 20.00 14000 J
15. UNKNOWN 20.19 8700 J
16. UNKNOWN 20.25 4900 J
17. UNKNOWN 20.40 17000 J
18. UNKNOWN 20.65 . 5700 J
19. UNRNOWH 21.52 18000 J
20. UNKNOWN 22.19 9300 J
FORM I SV-TIC . l/87 Rev.
183
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-16-lMS
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No,: 70
Matrix: (soi 1/wa ter) SOIL Lab Sample ID: 291630
Sample wt/vol: 30,0 (g/mL) _G_ Lab File ID: G00916JOA04
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _ll dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) L.. pH: 5.4 Dilution Factor: ~3~1~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1100
lll-44-4--------bis(2-Chloroethyl)Ether 1100
95-57-8---------2-Chlorophenol 1100
541-73-1--------l,3-Dichlorobenzene 1100
106-46-7--------l,4-Dichlorobenzene 1100
100-51-6--------Benzyl Alcohol 1100
95-50-1---------1,2-Dichlorobenzene 1100
95-48-7---------2-Hethylphenol 1100
39638-32-9------bis(2-Chloroisopropyl)Ether_ 1100
106-44-5--~-----4-Methylphenol 1100
621-64-7--------N-Nitroso-Di-n-Propylamine __ 1100
67-72-1---------Hexachloroethane 1100
98-95-3--~------Nitrobenzene 1100
78-59-1---------Isophorone 1100
88-75-5---------2-Nitrophenol 1100
105-67-9--------2,4-Dimethylphenol 1100
65-85-o---------Benzoic Acid 5400
lll-91-l--------bis(2-Chloroethoxy)Hethane __ 1100
120-83-2--------2,4-Dichlorophenol 1100
120-a2-1--------l,2,4-Trichlorobenzene 1100
91-20-3---------Naphthalene 1100
106-47-8--------4-Chloroaniline 1100
87-68-3---------Hexachlorobutadiene 1100
59-50-7---------4-Chloro-J-Methylphenol 1100
91-57-6---------2-Hethylnaphthalene 1100
77-47-4------:---Hexachl'orocyclopentadiene __ 1100
88-06-2---------2,4,6-Trichlorophenol 1100
95-95-4---------2,4,5-Trichlorophenol 5400
91-58-7---------2-Chloronaphthalene 1100
88-74-4---------2-Nitroaniline 5400
131-11-3--------Dimethyl Phthalate 1100
208-96-8--------Acenaphthylene 1100
606-20-2--------2,6-Dinitrotoluene 1100
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FORM I sv-1 1/87 Rev.
182
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS
SL-16-lMS
Contract: (2-881-REVS
Lab Code: COMPU Casa No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291630
Sample wt/vol: 30.0 (g/mL) li._ Lab File ID: GD0916JOA04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _u dee. Date Extracted: 10/05/89
Extraction: Date Analyzed: 10/09/89
GPC Cleanup:
( SepF /Cont/Sonc)
(Y/N) IL.. pH: 5.4 Dilution Factor: ~3~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND · (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 5400 u
83-32-9---------Acenaphthene 1100 u
51-28-5---------2,4-0initrophenol 5400 u
100-02-1--------4-Nitrophenol 5400 u
132-64-9--------oibanzofuran 1100 u
121-14-2--------2,4-Dinitrotoluene 1100 u
84-66-2---------0iethylphthalate 1100 u
7005-72-3-------4-Chlorophenyl-phenylether __ 1100 u
86-73-7---------Fluorene 1100 u
100-01-6--------4-Nitroanilina 5400 u
534-52-1--------4,6-0initro-2-Methylphenol __ 5400 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 1100 u
101-55-3--------4-Bromophenyl-phenylether __ 1100 u
118-74-1--------Hexachlorobenzene 1100 u
87-86-5---------Pentachlorophenol 5400 u
ss-01-s---------Phenanthrana 1100 u
120-12-1--------Anthracana 1100 u
84-74-2---------oi-n-Butylphthalate 820 BJ
206-44-0--------Fluoranthana 1100 u
129-oo-o--------Pyrane 1100 u
85-68-7---------Butylbanzylphthalate 1100 u
91-94-1---------3,3'-Dichlorobenzidine 2200 u
56-55-3---------Benzo(a)Anthracena 1100 u
218-01-9--------Chrysana 1100 u
117-81-7--------bis(2-Ethylhexyl)Phthalata_ 380 J
111-s4-o--------oi-n:octyl Phthalate 1100 u
205-99-2--------Banzo(b)Fluoranthena 1100 u
207-08-9-------~Benzo(k)Fluoranthana 1100 u
50-32-8---------Benzo(a)Pyrene 1100 u
193-39-5--------Indeno(l,2,3-cd)Pyrena 1100 u
53-70-3---------Dibanzo(a,h)Anthracena 1100 u
191-24-2--------Benzo(g,h,i)Perylena 1100 u
(1) -cannot be separated from Diphanylamine
FORM I sv-2 1/87 Rev.
181
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-16-lMSD
Lab Name: COMPUCHEM LABS Contract: C2-88l-REVS
Lab Code: COHPU Case No.: 17902 SAS No.:----SDG No.: .,_7.,.0 __
Matrix: (soil/water) SOIL Lab Sample ID: &2L9&16~3~1.__ __ _
Sample wt/vol: 30,0
Level: (low/med) LOW
(g/mL) ~ Lab File ID:
Date Received:
GDJ91631B04
10/04/89
\ Moisture: not dee. ---1.l dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) 5_0fil: Date Analyzed: 10/10/89
GPC Cleanup: (Y/N) IL_ pH: 5.4 Dilution Factor: ~3~,.,.o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol · 1100
lll-44-4--------bis(2-Chloroethyl)Ether 1100
95-57-8------~--2-Chlorophenol 1100
541-73-1--------1,3-Dichlorobenzene 1100
106-46-7--------1,4-Dichlorobenzene 1100
100-51-6--------Benzyl Alcohol 1100
95~50-1---------1,2-Dichlorobenzene 1100
95-48-7---------2-Methylphenol 1100
39638-32-9------bis(2-Chloroisopropyl)Ether_ 1100
106-44-5--------4-Methylphenol 1100
621-64-7--------N-Nitroso-Di-n-Propylamine __ 1100
67-72-1---------Hexachloroethane 1100
98-95-3---------Nitrobenzene 1100
78-59-1---------Isophorone 1100
88-75-5---------2-Nitrophenol 1100
105-67-9--------2,4-Dimethylphenol 1100
65-85-o---------Benzoic Acid 5400
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 1100
120-sJ-2--------2,4-Dichlorophenol 1100 ·
120-e2-1--------1,2,4-Trichlorobenzene 1100
91-20-3---------Naphthalene 1100
106-47-8-~------4-Chloroaniline 1100
87-68-3---------Hexachlorobutadiene 1100
59-50-7---------4-Chloro-3-Methylphenol 1100
91-57-6---------2-Methylnaphthalene 1100
77-47-4---------Hexachlorocyclopentadiene __ 1100
88-06-2-~-------2,4,6-Trichlorophenol 1100
95-95-4---------2,4,5-Trichlorophenol 5400
91-58-7---------2-Chloronaphthalene 1100
88-74-4---------2-Nitroaniline 5400
131-11-3--------Dimethyl Phthalate 1100
208-96-8--------Acenaphthylene 1100
606-20-2--------2,6-Dinitrotoluene 1100
Q
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FORM I sv-1 1/87 Rev.
-----.... ~ -=-:.. -• :. . .. -,.· . . . . -.. .£PW"t.E ORTIJ,.. SI . '· ' --
? ,..
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-16-lMSD
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: ..c7.>t.0 __
Matrix: (soil/water) SOIL Lab Sample ID: _,,_2.._9.,,.16"'3._l.._ __ _
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GDJ916J1B04
Level: ( low/med) LOW Date Received: 10/04/89
% Moisture: not dee. _ll dee. Date Extracted: 10/05/89
Date Analyzed: 10/10/89 Extraction: (SepF/Cont/Sonc) §..Qfil;
GPC Cleanup: (Y/N) ti__ pH: 5,4 Dilution Factor: £3~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 5400 u
83-32-9---------Acenaphthene 1100 u
s1-20-s---------2,4-Dinitrophenol 5400 u
100-02-1--------4-Nitrophenol 5400 u
132-64-9--------Dibenzofuran 1100 u
121-14-2--------2,4-Dinitrotoluene 1100 u
84-66-2--~------Diethylphthalate 1100 u
7005-72-3-------4-Chlorophenyl-phenylether_ 1100 u
86-73-7---------Fluorene 1100 u
100-01-6--------4-Nitroaniline 5400 u
534-52-1--------4,6-Dinitro-2-Methylphenol" __ 5400 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 1100 u
101-55-3--------4-Bromophenyl-phenylether __ 1100 u
118-74-1--------Hexachlorobenzene 1100 u
87-86-5---------Pentachlorophenol 5400 u
0s-01-a---------Phenanthrene 1100 u
120-12-1---~----Anthracene 1100 u
84-74-2---------oi-n-Butylphthalate 700 BJ
206-44-0--------Fluoranthene 1100 u
129-00-0--------Pyrene 1100 u
85-68-7---------Butylbenzylphthalate 1100 u
91-94-1---------3,3'-Dichlorobenzidine 2200 u
56-55-3---------Benzo(a)Anthracene 1100 u
218-01-9--------chrysene 1100 U.
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 480 J
117-84-0--------oi-n-octyl Phthalate 1100 u
205-99-2--------Benzo(b)Fluoranthene 1100 u
207-08-9--------Benzo(k)Fluoranthene 1100 u
50-32-8---------Benzo(a)Pyrene 1100 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 1100 u
53-70-3---------Dibenzo(a,h)Anthracene 1100 u
191-24-2--------Benzo(g,h,i)Perylene 1100 u
(1) -cannot be separated from 01phenylam1ne
FORM I sv-2 1/87 Rev.
....., . --.. ,, .. --ll!t 99
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-10-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No,: SDG No. : ,_7.,..0 ____ _
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) ~
LOW
Lab Sample ID: ~249-16~2~9"---
Lab File ID:
Level: (low/med)
\ Moisture, not dee . ..,..11~-dee.
Date Received: 10/04/89
Date Extracted: 10(05/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) SoNC.
GPC Cleanup: (Y/N) li_ pH: ....2...,...i Dilution Factor, 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC._________ 9.0 U
319-85-7--------beta-BHC 9.0 U
319-86-8--------delta-aH=c---------9.0 u
58-89-9---------gamma-BHC (Lindane)____ 9.0 U
76-44-8---------Heptachlor_________ 9.0 U
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309-00-2--------Aldrin.__________ 9.0 U . I
1024-57-3-------Heptachlor epoxide_____ 9.0 U
959-98-8--------Endosulfan I________ 9.0 U
60-57-1---------Dieldrin._________ 18. U
72-55-9---------4,4'-DDE_________ 18. U
72-20-8---------Endrin.__________ 18. u
33213-65-9------Endosulfan II_______ 18. U
72-54-8---------4,4'-DDD_________ 18. U
1031-07-8-------Endosulfan sulfate_____ 18. U
50-29-3---------4,4'-DDT_________ 18. U
72-43-5---------Methoxychlor________ 90. U
53494-70-5------Endrin ketone._______ 18. U
5103-71-9-------alpha-Chlordane.______ 90. U
5103-74-2-------gamma-Chlordane.______ 90. U
8001-35-2~------Toxaphene._________ 180 u
12674-11-2------Aroclor-1016________ 90. IU
11104-28-2------Aroclor-1221._______ 90. IU
11141-16-5------Aroclor-1232._______ 90. 1u
53469-21-9------Aroclor-1242:-------90. 1u
12672-29-6------Aroclor-1248._______ 90. 1u
11097-69-1------Aroclor-1254.________ 180 1u
11096-82-5------Aroclor-1260._______ 180 1u
---------------------------1--
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-·---------------oRJf"i-PEST''~ ------------1~ev.
-. ·---~••--r--" -...,. " ■ :.ii!~8illc. ~-IPl.l...lli~,OMR.llT.r..'R.t. stFM-.li'P ·· 98
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PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
SL-11-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.:. 17902
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
30.0 (g/mL) G__
LOW
i Moisture: not dee . ..,_12,.____ dee.
Extraction: (SepF/Cont/Sonc) s.QHC.
·GPC Cleanup: (Y/N) li,__ pH: --5..,_2_
SAS No.: SDG No. : .,_7,._0 ____ _
Lab Sample ID: ~2L9~16~3~9L-__
Lab File ID:
Date Received: .0/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
Dilution Factor: 1. 00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
319-84-6--------alpha-BHC 9.1 u
319-85-7--------beta-BHC 9. l u
319-86-8--------delta-BHC 9.1 u
58-89-9---------gamma-BHC (Lindane) 9.1 u
76-44-8---------Heptachlor 9.1 u
309-00-2--------Aldrin 9.1 u
1024-57-3-------Heptachlor epoxide 9.1 u
959-98-8----~-;.-Endosulfan I 9.1 u
60-57-1---------Dieldrin 18. u
72-55-9---------4,4'-DDE 18. u
72-20;.9_;. __ "." ____ gndrin 18. u
33213-65-9------Endosulfan II 18. u
72-54-8---------4,4'-DDD 18. u
1031-07-8-------Endosulfan sulfate 18. u
50-29-3---------4,4'-DOT 18. u
72-43-5---------Methoxychlor 91. u
I 53494-70-5------Endrin ketone 18. u
I 5103-71-9-------alpha-Chlordane 91. u
I 5103-74-2-------ga.auna-Chlordane 91. u
I 8001-35-2-------Toxaphene 180 u
I 12674-11-2------Aroclor-1016 91. u
I 11104-28-2------Aroclor-1221 91. u
I 11141-16-5------Aroclor-1232 91. u
I 53469-21-9------Aroclor-1242 91. u
I 12672-29-6------Aroclor-1248 91. IU
I 11097-69-1------Aroclor-1254 180 IU
I 11096-82-5------Aroclor-1260 180 !U
I I ............ ,.-·-·-·-
----------------•ORJI "1 PE:;'l' ____________ ,.._,~ .. 'lt--er.1.r-. --
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name:'COMPUCHEM LABORATORIES
SL-12-1
Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .,_7.,,_0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L9~1~64~0,._ __
Lab File IO: Sample wt/vol: 30.0 (g/mL) L._
LOW Level: (low/med)
\ Moisture: not dee. _..10,.___ dee.
Date Received: 10/04/89
Date Extracted: 10/0S/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li._ pH: --5..,_i Dilution Factor: 1.00
\
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 8.9 U
319-85-7--------beta-BHC.__________ 8.9 U
319-86-8--------delta-BHC_________ 8.9 U
58-89-9---------gamma-BHC (Lindane)____ 8.9 U
76-44-8---------Heptachlor_________ 8.9 U
309-00-2--------Aldrin.__________ 8.9 U
1024-57-3-------Heptachlor epoxide._____ 8.9 U
959-98-8--------Endo.sulfan I________ 8, 9 U
60-57-1---------Dieldrin.__________ 18. U
72-55-9---------4, 4-' -DOE.__________ 18. U
72-20-8---------Endrin.__________ 18. u
33213-65-9------Endosulfan II_______ 18, U
72-54-8~--------4,4'-DDD__________ 18. U
1031-07-8-------Endosulfan sulfate._____ 18. U
50-29-3-------~-4,4'-DOT__________ 18. U
72-43-5---------Methoxychlor________ 89. U
53494-70-5------Endrin ketone._______ 18. U
5103-71-9-------alpha-Chlordane.______ 89. U
5103-74-2-------gamma-Chlordane.______ 89. U
8001-35-2-------Toxaphene_________ 180 U
12674-11-2------Aroclor-1016._______ 89. u
11104-28-2------Aroclor-1221 I 89. fU
11141-16-5------Aroclor-1232 I 89. !U
53469-21-9------Aroclor-1242 I 89. IU
12672-29-6------Aroclor-1248 I 89. IU
11097-69-1------Aroclor-1254 I 180 IU
11096-82-5------Aroclor-1260 I 180 IU
0
----------------------1-.------'--
----------------""P"'O"'RM~"I-"'l'"""'!'""'------------,791 "Rev-:--
, p ... iWIZt:6 OIIT//1: A•• 1'1'J.: .. c_::c-.;...:_ _ 96
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-13-1
Lab Name: COMPUCHEM LABORATORIES Contract: r2-88J~REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7,,_0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L9~16~4~1._ __
Sample wt/vol: 30,0 (g/mL} L-
LOW
Lab File IO:
Level: (low/med}
% Moisture: not dee. ~2~3 __ dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc} ~
GPC Cleanup: (Y/N} H.,_ pH: ..i,_6_ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/KG
I
319-84-6--------alpha-BHC _____ ....:...___ 10. IU
319-85-7--------beta-BHC 10. I U
319-86-8--------delta-BH_C_________ 10. iU
58-89-9---------gamma-BHC (Lindane}____ 10. IU
76-44-8---------Heptachlor_________ 10. iU
309-00-2--------Aldrin.__________ 10, iU
1024-57-3-------Heptachlor epoxide._____ 10.. IU
959-98-8--------Endosulfan I________ 10. IU
60-57-1---------Dieldrin.__________ 21. iU
72-55-9---------4,4'-DOE__________ 21. iU
72-20-8---------Endrin.___________ 21. iU
33213-65-9------Endosulfan II._______ 21. iU
72-54-8---------4,4'-DDD__________ 21. IU
1031-07-8-------Endosulfan sulfate,_____ 21. iU
50-29-3---------4,4'-DDT_________ 21.. fU
72-43-s~--------Methoxychlor________ 100 fU
53494-70-5------Endrin ketone._________ 21. iU
5103-71-9-------alpha-Chlordane.______ 100 I U
5103-74-2-------gamma-Chlordane______ 100 fU
8001-35-2-------Toxaphene._~-------210 fU
12674-11-2------Aroclor-1016 100 tu
11104-28-2------Aroclor-1221________ 100 fU
11141-16-5------Aroclor-1232_______ 100 fU
53469-21-9------Aroclor-1242_______ 100 fU
12672-29-6------Aroclor-1248 100 fU
11097-69-1------Aroclor-1254·--------210 fU
. 11096-82-5------Aroclor-1260_______ 210 fU
Q
---------------------______ , __ , ................. •··•-
------------. --.. ~---.·---·-··
O'Rll: 't "PEST ij87 "'ReV.
-za. SIIIU"L ._ oar-.-=~•••••&==-====--"
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-14-1
Lab Name: COMPUCHEM LABORATORIES Contract: r2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .,_7.,._0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~29"--"-'16~4~2,_ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) !:,___
LOW Level: (low/med)
% Moisture: not dee. ~i~'--dee.
Date Received: 10/04/89
Date Extracted: 10(05/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanupi (Y/N) li._ pH: ..i,.i Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS1
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC 319-86-8--------delta-BH~C---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8-----~---Heptachlor ________ _
309-00-2--------Aldrin.,....,.. ___ ....,...., ____ _
1024-57-3-------Heptachlor epoxide, ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin. _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin 33213-65-9------Endosu·~l~f-a_n_I~I-------
9.6 U
9.6 U
9.6 U
9. 6 U
9.6 U
9.6 U
9.6 U
9.6 U
19. U
19. U
19. U
19. U
Q
72-54-8---------4,4'-DDD 19. U ·
1031-07-8-------Endosulf_a_n_su-rlfTa_t_e ____ _
50-29-3---------4,4'-DDT 72-43-5---------MethoxycrhTl_o_r_~------
53494-70-5------Endrin ketone 5103-71-9-------alpha-Chlorda_n_e _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ________ _
12674-11-2------Aroclor-1016 --------11104-28-2------Aroclor-1221 11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _______ _
19. U
19. U
96. U
19. U
96. U
96. u
190 U
96. U
96. u
96. U
96. U
96. U
190 U
190 U
----------------"'P""O"D-"'1~1'·1_.------------,7e;"il.eV·;-
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA _SHEET
I
Lab Name, COMPUCHEM LABORATORIES
I SL-15-1
Contract: 12-88\-REVS 1-------
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ... 7,,_0 ____ _
Matrix: (soil/water) SOIL Lab s amp 1 e Io : .,,,2.,,_9 ..._l ,._6 4:,..3..__ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) !:,__
Level: (low/med) LOW
% Moisture: not dee·. _l-5 __
Extraction, (SepF/Cont/Sonc)
dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
GPC Cleanup, (Y/N) li._ pH:~ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS1
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta~BHC=----------
319-86-8--------delta-BHC 58-89-9---------gamma-BHC-,,(L~i~-n-d~a-n-e~)-----
76-44-8---------Heptachlor ________ _
309-00-2--------Aldrin.~----------1024-57-3-------Heptachlor epoxide. ____ _
959-98-8--------Endoeulfan I _______ _
60-57-l---------Dieldrin:----------72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin 33213-65-9------Endoeu-~l~f_a_n_·~II _______ _
72-54-8---------4,4'-DDD 1031-07-8-------Endoeulf_a_n_e_u_l~f-=-a_t_e ____ _
50-29-3---------4,4'-DDT,..,,. ________ _
72-43-5---------Methoxychlor 53494-70-5------Endrin keton_e ______ _
510 3-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene 12674-11-2------Aroclor-1-=-o-=-1.,,.6 _______ _
11104-28-2------Aroclor-1221. _______ _
11141-16-5------Aroclor-1232. _______ _
53469-21-9------Aroclor-1242. _______ _
12672-29-6------Aroclor-1248. _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 ______ _
9.4
9.4
9.4
9.4
9.4
9.4
9.4
9.4
19.
19.
19.
19.
19.
19.
19.
94.
19.
94.
94.
190
94.
94.
94.
94.
94.
190
190
I 1u
IU
IU
IU u
u
u
u
u
u
u
u u u
u u
u u
u
u
u
u
u
u
u u
u
Q
···•----..I-.......,.---'--,------,---,-------,------------
---------------ORM-r,,EsT·-------------.·7e1'"11.e·~v-. -
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-16-1
Lab Name: COMPUCHEM LABORATORIES Contract: /2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ~7~0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~29"---"'16~4~4._ __
Lab File ID: Sample wt/vol:
Level: (low/med)
30.0 (g/mL) L_
LOW
% Moisture: not dee . ..,_11..___
Extraction: (SepF/Cont/Sonc)
dee.
.smK
pH: ..i,_!
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89
GPC Cleanup: (Y/N) lL_ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 9.0 U
319-85-7--------beta-BHC 9.0 U 319-86-8--------delta-BH~C---------9.0 U
58-89-9---------gamma-BHC (Lindane)____ 9.0 U
76-44-8---------Heptachlor_________ 9.0 U
309-00-2--------Aldrin,...... ___ ....,...-,------9.0 U
1024-57~3----~--Heptachlor epoxide_____ 9.0 u
959-98-8----~---Endosulfan I________ 9.0 U
60-57-1---------Dieldrin__________ 18. U
72-55-9-~-------4,4'-DDE__________ 18. U
72-20-8---------Endrin 18. U 33213-65-9------Endosu.,..l.,,.fa_n__,I::-:I=--------18. U
72-54-8---------4,4'-DD□_· _________ 18. U
1031-07-8-------Endosulfan sulfate_____ 18. U
50-29-3---------4,4'-DDT,......_________ 18. U
72-43-5---------Methoxychlor________ 90, u
53494-70-5------Endrin ketone_______ 18. U
5103-71-9-------alpha-Chlordane______ 90. U
5103-74-2-------gamma-Chlordane______ 90. U
8001-35-2-------Toxaphene 180 U 12674-11-2------Aroclor-l.~0~1~6--------90. U
11104-28-2------Aroclor-1221 90. U 11141-16-5------Aroclor-1232_______ 90. U
53469-21-9------Aroclor-1242 90. U 12672-29-6------Aroclor-1248________ 90. U
11097-69-1------Aroclor-1254_______ 180 U
Q
11096-82-5------Aroclor-1260_______ 180 IU
---------------------------1-... --.... ----•"""'
----------------'"•ORM~EST ____________ i..,7'1:18'"17-"'R11e"&v-.:-. -
IIPLE DRTIL .SSitl.Ml--!!IE~:=::;;;ac.. _:-..:. ,-..__.-,. _-:•, :-92
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0
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-17-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No. : l 7 9 0 2 SAS No.: SDG No. : .,_7,,_0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: 291645
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID:
Level: (low/med) LOW Date Received: 10/04/89
% Moisture: not dee. 8 dee. Date Extracted: 10/05/89
Extraction: (SepF/Cont/Sonc) .5.0HC. Date Analyzed: 10 /09 /89
GPC Cleanup: (Y/N) H...._ pH: -5......i Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC 319 :..06-8--------.del ta-sH-=c---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor ________ _
309-00-2--------Aldrin.,....,..-----:-:-----1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8------~--Endrin. __________ _
33213-65-9------Endosulfan II ______ _
72-54-8---------4,4'-DDD _________ _
1031-07-8-------Endosulfan sulfate ____ _
50-29-3---------4,4'-DDT~---------72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _ _;_ ___ _
8001-35-2-------Toxaphene 12674-ll-2------Aroclor-1~0~1~6--------
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 ______ _
lliil~
8.7 U
8. 7 U
8.7 U
8.7 U
8.7 U
8.7 U
8. 7 U
8. 7 U
17. U
17. U
17. U
17. U
17. U
17. U
17. U
87. U
17. U
87. U
87. U
170 U
87. U
87. U
87. U
87. U
87. U
170 U
170 U
Q
---------------••ORM-1-P'"t~S"'T------------,17ll7'ilev.
. El'Jl » _,. .tifif'F(.~ ORTR:., JiS-iil't•· --lft'l!i!:t::==.-91
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-18-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 70
Matrix: (soil/water) SOIL Lab Sample ID: 291646
S_ample wt/vol: 30.0 (g/mL) G.__ Lab File ID:
Level: (low/med) LOW Date Received: lOl0ilB9
,. Moisture: not dee. 10 dee. Date Extracted: l0l0SlB9
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/09l89
GPC Cleanup: (Y/N) li,_ pH: ....L..i Dilution Factor:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
319-84-6--------alpha-BHC _____ ....:,_ __ _
319-85-7--------beta-BHC _________ _
319-86-8--------delta-BHC. ________ _
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor __ ~------
·309-bo-2--------Aldrin ·-----------1024-57-3-------Heptachlor epoxide. ____ _
959-98-8--------Endosulfan I _______ _
60-57-1~--~-----Dieldrin. _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin. __________ _
33213-65-9------Endosulfan II. ______ _
72-54-8---------4,4'-DDD _________ _
1031-07-8-------Endosulfan sulfate, ____ _
50-29-3---------4,4'-DDT _________ _
72-43-5---------Methoxychlor _______ _
I 53494-70-5------Endrin ketone.~------! 5103-71-9-------alpha-Chlordane. _____ _
t 5103-74-2-------ganuna-Chlordane _____ _
I 8001-35-2---,,----Toxaphene ________ _
I 12674-11-2------Aroclor-1016 _______ _
I 11104-28-2------Aroclor-1221. ______ _
I 11141-16-5------Aroclor-1232 ______ _
t 53469-21-9------Aroclor-1242 ______ _
I 12672-29-6------Aroclor-1248 _______ _
I 11097-69-1------Aroclor-1254 _______ _
I 11096-82-5------Aroclor-1260 ______ _
UGliG
I
8. 9 I u
8. 9 IU
8. 9 1u
8. 9 IU
8. 9 U
8. 9 U
8. 9 U
8. 9 U
18, U
18, U
18. U
18, U
18. U
18. U
18. U
89. U
18. U
,89. u
89. U
180 U
89. U
89. U
89. U
89. U
89. U
180 U
180 U
1.00
Q
··'------------------------------··--··"'"''
----------------oRK"'t""'PEST------------.-'7~ev.
-_.,_ , ... --;. a,a ·a,: 5RIMIL E OR~JiSitl•••PIE;:=:=-
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98
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PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: r2-88)-REVS
SL-19-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7,,_Q ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L9~16~4~7,.._ __
Lab File IO: Sample wt/vol: 30.0 (g/mL) L-
Level: (low/med)
% Moistures not dee. A1~4 __ dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) I!__ pH: __i,,_4, Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS1
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC. ________ _
319-85-7--------beta-BHC 319-86-8--------delta-BH._C ________ _
58-89-9-----~---gamma-BHC (Lindane) ___ _
76-44-8~--------Heptachlor ________ _
309-00-2--------Aldrin.~----------
1024-57-J-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I. _______ _
60-57-1---------Dieldrin._· ________ _
72-55-9---------4,4'-00E. _________ _
72-20-8---------Endrin. __________ _
33213-65-9------Endosulfan II ______ _
72-54-8---------4,4'-DDD. _________ _
1031-07-8-------Endoaulfan sulfate ____ _
50-29-3---------4,4'-DDT _________ _
72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone. ______ _
5103-71-9-------alpha-Chlordane. _____ _
5103-74-2-------gamma-Chlordane. _____ _
8001-35-2-------Toxaphene 12674-11-2------Aroclor-1·~0-1-5 _______ _
11104-28-2------Aroclor-1221. _______ _
11141-16-5------Aroclor-1232
53469-21-9------Aroclor-1242·--------
12672-29-6------Aroclor-1248. _______ _
11097-69-1------Aroclor-1254. _______ _
11096-82-5------Aroclor-1260, _______ _
I
9. 3 IU
9. 3 iU
9. 3 U
9.3 U
9.3 U
9.3 U
9.3 U
9. 3 U
19. U
19, U
19. U
19. U
19. U
19. U
19. U
93. U
19. U
93. U
93. U
190 U
93. U
93. U
93. U
93. U
93. U
190 U
190 U
Q
----------------•,~o~nv-1•p~e~s~1~.------------,1,~7--itev-:--
:Si&mPC.1£ OlilTlf------------89
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-20-1
1b Name1 COMPUCHEM LABORATORIES Contract: {2-88}-REVS
1b Code I COMPU Case No.: 17902 SAS No.: SDG No.: ~7~0 ___ _
1trix: (soil/water) SOIL Lab Sample ID: ~2~91~6w4~8 __ _
unple wt/vol: 30.0 (g/mL) L-Lab File ID:
3vel 1 (low/med) LOW
Moisture1 not dee, ..._14~-
<tractioni (SepF/Cont/Sonc)
?C Cleanup1 (Y/N) IL_
dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
SQliC.
...L.§.
Date Analyzed: 10/09/89
pH1 Dilution Factor: 1.00
CAS NO, COMPOUND
CONCENTRATION UNITS1
(ug/L or ug/Kg) UG/RG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH~C---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor _______ _
309-00-2--------Aldrin 1024-57-3-------Heptac~hl~o-r_e_p_o_x~i~de ____ _
959-98-8--------Endoaulfan I
60-57-1---------Dieldrin -------
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin
33213-65-9------Endoau.~l~f-an-,I~I=--------
72-54-8---------4,4'-DDD 1031-07-8-------Endoaulf_a_n_a_u~l~f~a-t_e ____ _
50-29-3---------4,4'-DDT,..... _______ _
72-43-5---------Methoxychlor
53494-70-S------Endrin keton_e ______ _
S103-71-9-------alpha-Chlordane _____ _
S103-74-2-------gamma-Chlordane _____ _
8001-3S-2-------Toxaphene=-r--------
12674-ll-2------Aroclor-1016 ______ _
11104-28-2------Aroclor-1221 ______ ___
11141-16-s------Aroclor-1232 ______ _
S3469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-12~8 ______ _
11097-69-1------Aroclor-1254 ______ _
11096-82-S------Aroclor-1260 ______ _
, ...... -.... -. -----,----......,,.--,------,------.1 ..
9.3
9,3
9,3
9. 3
9.3
9,3
9.3
9.3
19.
19.
19.
19.
19.
19.
19.
93.
19.
93.
93.
190
93.
93.
93.
93.
9 3.
190
190
Q
I JU
IU
IU
IU
JU u
u
u u
u u
u u u u u
u u
JU
JU
JU
IU
IU
IU
IU
IU
IU
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--------------otur!""P!S'------------,--,~So/1~it~e~vr.-
·----· 88
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-21-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 .SAS No,: SDG No·.: -'--7,._0 ____ _
Matrix: (soil/water)
Sample wt/vol:
Level: (low/med)
SOIL
30.0
LO~
(g/mL) G.__
Lab S amp 1 e ID : ,._2 9"--"'l 6,.__4.,_,9.__ __
Lab File ID:
% Moisture: not dee. 3 dee.
Date Received: 10/04/89
Date Extracted: 10/05/89
Date Analyzed: 10/09/89 Extraction: (SepF/Cont/~onc) 5..0.l:fC.
GPC Cleanup: (Y/N) li_ pH: _Ll. Dilution Fa~tor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319~84-6--------alpha-BHC_________ 8.2 U
319-85-7--------beta-BHC 8.2 U
319-86-8--------delta-BH=c---------8.2 U
58-89-9---------gamma-BHC (Lindane)____ 8.2 U
76-44-8---------Heptachlor_________ 8.2 U
309-00-2--------Aldrin.___________ 8.2 U
1024-57-3-------Heptachlor epoxide_____ 8.2 U
959-98-8----~---Endosulfan I________ 8.2 U
60-57-1------.. ---Dieldrin. ______ ---'----16. U
72-55-9---------4,4'-DOE__________ 16. U
72-20-8---------Endrin 16. U 33213-65-9------Endosu·~l~f-a_n_I_I_______ 16. U
72-54-8---------4,4'-DDO__________ 16. U
1031-07-8-------Endosulfan sulfate_____ 16. U
50-29-3---------4,4'-D~---------16. U 72-43-5---------Methoxychlor________ 82. U
53494-70-5------Endrin ketone_______ 16. U
5103-71-9-------alpha-Chlordane.______ 82. U
5103-74-2-------gamma-Chlordane.______ 82. U
8001-35-2-------Toxaphene 160 U 12674-11-2------Aroclor-1·-=o-=-1"""6________ 82. u
11104-28-2------Aroclor-1221________ 82. U
11141-16-5------Aroclor-1232_______ 82. IU
53469-21-9------Aroclor-1242_______ 82. IU
12672-29-6------Aroclor-1248_---'------82. IU
11097-69-1------Aroclor-1254_______ 160 IU
0
11096-82-5------Aroclor-1260_______ 160 IU
---------------------------1---,-.... -.. -.......... -,
----------------,.ou-r,,ES"'T ___________ _,,ll"l7"'118r77-"it'llev.
·-,·pp » 7':;SCW!'LE DRTR'-.!iSill:iE••••v=:v=:=..::::=-._ .B7·
I 10
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I SL-22-1
ab Name 1 .COMPUCHEM LABORATORIES Contract: 12-880-REVS
I ab Code1 COMPU Case No.: 17902 SAS No.1 SDG No . : .,_7 O,.__ ___ _
I
atrix: (soil/water) SOIL Lab Sample ID: 292316
ample wt/vol: 30.0 (g/mL) fi.._ Lab File ID:
I evel: (low/med) LOW Date Received: 10/05/89
Moisture1 not dee. ll dee. Date Extracted: 10/06/89
I xtraction1 (SepF/Cont/Sonc) SQliC. Date Analyzed1 10 I 1·2 /89
PC Cleanup1 (Y/N) li..._ pH1 ...L..l Dilution Factor: 1.00
I CONCENTRATION UNITS1
CAS NO, COMPOUND (ug/L or ug/Kg) Pill~ Q
I
m
m
m
g
I
319-84-6--------alpha-BHC,_________ 9.0 IU
319-85-7--------beta-BHC 9.0 iU
319-86-8--------delta-BH~C,-----------9.0 IU
58-89-9---------gamma-BHC (Lindane)____ 9.0 IU
76-44-8---------Heptachlor ___ ....;....____ 9.0 IU
309-00-2--------Aldrin 9.0 1u
1024-57-3-------Heptac~h~lo_r_e_po_x~i~de_____ 9.0 IU
959-98-8--------Endosulfan I_______ 9.0 1u
60-57-1---------Dieldrin_________ 18. 1u
-72-55-9---------4,4'~DDE_________ 18. IU
72-20-8---------Endrin~---------18. IU
33213-65-9--~---Endosulfan II 18. 1u
72-54-8---------4,4'-DDD -------18. IU
1031-07-8-------Endosulfan sulfate_____ 18. U
50-29-3---------4,4'-DDT 18. U
72-43-5---------Methoxyc_h_lo_r________ 90. u
D
53494-70-5------Endrin ketone._______ 18. U
5103-71-9-------alpha-Chlordane.______ 90. u
5103-74-2-------gamma-Chlordane______ 90. U
8001-35-2-------Toxaphene 180 U
· 12674-11-2------Aroclor-1·""0-=-1-:-6----,----90. u
I 11104-28-2------Aroclor-1221:-------90. u
11141-16-5------Aroclor-1232 90. u
53469-21-9------Aroclor-1242·-------90. U
D 12672-29-6------Aroclor-1248._______ 90. U
11097-69-1------Aroclor-1254_______ 180 U
11096-82-5------Aroclor-1260 I 180 (U
D •••-~W••• .. .,.. ---------.,-----------'------'--
D
u --------------01U1-rr>!s·--------------,7e1""Reir--:--
I -·,r I --------86
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I
10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-23-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ~7~0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~29~2~3~1~5.__ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) !;i__
Level: (low/med) LOW
% Moisture: not dee. 41&2 __ dee.
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10(12/89
Dilution: Factor: l. 00
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ~ pH: ...L...5_
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--~-----alpha-BHC ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH~C---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-4.4-8---------Heptachlor ________ _
309-00-2--------Aldrin,....,... ___ ....,...,_ ____ _
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I
60-57-1---------Dieldrin --------
72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin 33213-65-9------Endosu~l~fa_n__,I~I=--------
72-54-8---------4,4'-DDD 1031-07-8-------Endosulfa_n_s_u~l~f~a~t-e ____ _
50-29-3---------4,4'-DDT-________ _
72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9---~---alpha-Chlordane. _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2--~----Toxaphene 12674-11-2------Aroclor-1~0~1~6--------
11104'-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 I 12672-29-6------Aroclor-1248 ______ _
I 11097-69-1------Aroclor-1254 _______ _
I 11096-82-5------Aroclor-1260 ______ _
9.1 U
9.1 U
9.1 U
9. l U
9.1 U
9.1 U
9.1 U
9.1 U
18. U
18. U
18. U
18. U
18. U
18. U
18. U
91. U
18. U
91. U
91. U
180 U
91. U
91. U
91. U
91. U
91. U
180 U
180 U
Q
·---...... .1 ---------
---------------,,oRM""'t-PEST ___________ .,..,'87Tev.
------·--. ... .. ' ----------· ,, -.. --85
I
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
I I SL-24-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS \ ______ _
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ~7~----
Lab S amp 1 e I D : _.,_2 .,,_9 ,,_2 3._,2""'1.__ __
Lab File ID:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) i;;__
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. 14 dee. Date Extracted: 10/06/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/12/89
GPC Cleanup: (Y/N) H.__ ' pH: _L_1. Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/!'iG Q
I
319-84-6--------alpha-BHC_________ 9.3 \U
319-85-7--------beta-BHC 9.3 \U 319-86-8--------delta-BH=c---------9.3 \U
58-89-9---------gamma-BHC (Lindane)____ 9.3 \U
76-44-8-----~---Heptachlor_________ 9.3 \U
309-00-2--------Aldrin,....,... ___ ....,...,-------9.3 \U
1024-57-3-------Heptachlor epoxide_____ 9.3 \U
959-98-8--------Endosulfan I________ 9.3 \U
60-57-1---------Dieldrin__________ 19. \U
72-55-9---------4,4'-DDE__________ 19. \U
72-20-8---------Endrin 19. I U 33213-65-9------Endosu~l=fa_n__,I~I=--------19. \U
72-54-8---------4,4'-DDD 19. \U 1031-07-8-------Endosulfa_n_s_u~l~f~a~t-e_____ 19. \U
50-29-3---------4, 4' -DDT,.....________ 19. I U
72-43-5---------Methoxychlor 93. \U
53494-70-5------Endrin ketone._______ 19. \U
5103-71-9-------alpha-Chlordane______ 93. \U
5103-74-2-------gamma-Chlordane______ 93. \U
8001-35-2-------Toxaphene 190 \U 12674-11-2------Aroclor-1=0~1~6-------93. \U
11104-28-2------Aroclor-122 l 93. I U 11141-16-5------Aroclor-1232_______ 93, \U
53469-21-9------Aroclor-1242________ 93, \U
12672-29-6------Aroclor-1248________ 93. \U
11097-69-1------Aroclor-1254________ 190 \U
11096-82-5------Aroclor-1260_______ 190 \U ,_, ___ ,,_1,---------------------______ \ __
---------------""'·OIU! i PEST------------, J'J7-ri.ev.
» _.,._ -SRIU"LE . DlilT,._ A yy--,.. 84
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D
10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-25-1
Lab Name: COMPUCHEM LABORATORIES Contract: {2-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7"'0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~?L92~3~2~2"---
Lab File ID: Sample wt/vol: 30.0 (g/mL) ~
LOW Level: (low/med)
% Moisture: not dee . ...,17-'---dee.
Date Received: 10/05/89
Date Extr.acted 1 10 /06 /89
Date Analyzed: 10/12/89 Extraction: (SepF/Cont/Sonc) 5_0liC_
GPC Cleanup: (Y/N) H__ pH:~ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC_________ 9.6 U
319-85-7--------beta-BHC.__________ 9.6 U
319-86-8--------delta-BHC_________ 9.6 U
58-89-9---------gamma-BHC (Lindane)____ 9.6 U
76-44-8---------Heptachlor_________ 9.6 U
309-00-2--------Aldrin.___________ 9.6 U
1024-57-3-------Heptachlor epoxide._____ 9.6 u
959-98-8--------Endosulfan I________ 9.6 u
60-57-1---------Dieldrin.__________ 19. u
72-55-9---------4,4'-DDE__________ 19. U
72-20-8---------Endrin.___________ 19. u
33213-65-9------Endosulfan II._______ 19. u
72-54-8---------4,4'-DDD__________ 19. U
1031-07-8-------Endosulfan sulfate._____ 19. u
50-29-3---------4,4'-DDT__________ 19. U
72-43-5---------Methoxychlor________ 96. U
53494-70-5------Endrin ketone.·________ 19. U
5103-71-9-------alpha-Chlordane.______ 96. U
5103-74-2-------gamma-Chlordane______ 96. u
8001-35-2-------Toxaphene_________ 190 IU
12674-11-2-~----Aroclor-1016________ 96. IU
11104-28-2------Aroclor-1221_______ 96. IU
11141-16-5------Aroclor-1232_______ 96. IU
53469-21-9------Aroclor-1242 96. IU
12672-29-6------Aroclor-1248________ 96. IU
11097-69-1------Aroclor-1254_______ 190 IU
11096-82-5------Aroclor-1260_______ 190 IU
Q
---------------------------------,---1---1 .. __ ,_ ....... -...
PORM "'1,,!ST ii& 111.ev.
-. . . . . -.. ----~-. -. -,, l W Oil Tac:. A YM/M'V -SJ
I
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m
n
H
I
lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-28-1
Lab Name: COMPUCHEM LABORATORIES Contract: l2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .,_7,,_0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L9~23~2~0._ __
Lab File ID: Sample wt/vol:
Level: (low/med)
30.0 (g/mL) \:i__
LOW Date Received: 10/05/89
% Moisture: not dee . ...,13.___ dee.
Extraction: (SepF/Cont/Sonc) SQHC.
Date Extracted: 10/06/89
Date Analyzed: 10/12/89
GPC Cleanup: (Y/N) IL_ pH: _hi Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC=----------
319-86-8--------delta-BHC 58-89-9---------gamma-BHC-.,.,(L~i~·n-d~a-n-e~)-----
76-44-8---------Heptachlor ________ _
309-00-2--------Aldrin.~----------1024-57-3-------Heptachlor epoxide ____ _
959-98-8----..;---Endosulfan I _______ _
60-57-1---------Dieldrin. _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8-~-------Endrin 33213-65-9------Endosu.~l~f_a_n-II _______ _
72-54-8---------4,4'-DDD __ ~~------1031-07-8-------Endosulfan sulfate ____ _
50-29-3---------4,4'-DOT~---------72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone. ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene 12674-ll-2------Aroclor-1TO~l~6--------
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 _______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _______ _
9.2
9.2
9.2
9.2
9.2
9.2
9.2
9.2
18.
18.
18.
18.
18.
18.
18.
92.
18.
92.
92.
180
92.
92.
92.
92.
92.
180
180
u u u
u
u
u
u
u
u
u
u
u u
u
u
u u
u
u
u
u
u
u
u
u
u
u
Q
.. _ _. .. ,_ --............... ---..,,....,, ....... -------------------------
---------------•1urT-PEST ___________ 7'd.,"Rev-:---
I .a . 1Wr: S:PYPl.E DR T.~RL.!Siii'al[~E--ll!lii=::=;::::......::;__ 82
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m
n
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-29-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88\-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: S 0G No . : .,_7.,._ ___ _
Matrix: (soil/water) SOIL Lab Sample ID: ~249~23~1L9L-__
Lab File ID: Sample wt/vol: 30.0 (g/mL) ~
LOW Level: (low/med)
% Moisture: not dee. ~1~3 __
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li_
dee.
pH:
~
--1..J
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/15/89
Dilution Factor: l. 00
CAS NO. COMPOUND•
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC=·---------
319-86-8--------delta-BHC_,...,..~-~----
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor ________ _
309-00-2--------Aldrin,...,.. ___ ...,....,------
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1------~--Dieldrin _________ _
72-55-9---------4,4'-DDE ________ _
72-20-8---------Endrin 33213-65-9------Endosu~l=fa_n__,I~I=-----'----
72-54-8---------4,4'-DDD 1031-07-8-------Endosulfa_n_s_u~l~f~a~t-e ____ _
50-29-3---------4,4'-DDT 72-43-5---------Methoxych~l~o-r _______ _
53494-70-5------Endrin ketone. ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene 12674-ll-2------Aroclor-1=0-1=6--------
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 _______ _
53469-21-9------Aroclor-1242 12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 ______ _
I I 9. 2 1u I
9. 2 I u I
9 .2 IU I
9 .2 IU I
9. 2 I u I
9 .2 iU I
9 .2 I u · I
9.2 IU I
18. I u I
18. u I
18. U
18. U
18. U
18. U
18. U
92. U
18. U
92. U
92. U
180 U
92. U.
92. U
92. U
92. U
92. U
180 U
180 U
.... ____ ...... I. --------
---------------•oiur"!-i>EST __________ ..,7B7tte=vc-.-
i 6'1F==---81
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i_
10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-30-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7.,.0 ____ _
Matrix: (soil/water) SOIL L,ab Sample ID 1 ,._2L9,._2 ,,_3 ._1 7,__ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) L_
LOW Level: (low/med)
% Moisture: not dee. ~1&5 __ dee.
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/15/89 ,-
Dilution Factor: 4.00
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H._ pH:~
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I 319-84-6--------alpha-BHC _________ I
319-85-7--------beta-BHC I
319-86-8--------delta-BHC I
58-89-9---------gamma-BHC (Lindane) I
76-t4-8---------Heptachlor I
309-00-2--------Aldrin I
1024-57-3-------Heptachlor epoxide I
959-98-8--------Endosulfan I I
60-57-1---------Dieldrin I
72-55-9---------4,4'-DDE I
72-20-8---------Endrin I
33213-65-9------Endosulfan II I
72-54-8---------4,4'-DDD I
1031-07-8-------Endosulfan sulfate I
50-29-3---------4,4'-DDT I
72-43-5---------Methoxychlor I
53494-70-5------Endrin ketone I
5103-71-9-------alpha-Chlordane I
5103-74-2-------gamma-Chlordane I
8001-35-2-------Toxaphene I
12674-11-2------Aroclor-1016 I
11104-28-2------Aroclor-1221 I
11141-16-5------Aroclor-1232 I
53469-21-9------Aroclor-1242 I
12672-29-6------Aroclor-1248 I
11097-69-1------Aroclor-1254 I
11096-82-5------Aroclor-1260 I
38.
38.
38.
38.
38.
38.
38.
38.
75.
75.
75.
75.
75.
75.
75.
380
75.
380
380
750
380
380
380
380
380
750
750
I ,u
IU ,u
IU IU IU ,u
IU IU ,u
IU u
u u
u
u u
u
u u
u
u u
u u
u
u
0
---------.....,..,-------,---,,.....,-----t___,~---,-___,,...,;..,..., ----
----------------p~u~aw-""t...,..~P"E''SMtr------------n17~1~ev-:---
-. -. -' ---.... ..., -...... ·------.. --... SASPLE DRTR SU. ,, .. :.-·-.. · SB
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10
·PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
I
Lab Name: COMPUCHEM LABORATORIES
I SL-30-2
Contract: 12-88)-REVS I ______ _
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,_7_,.0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L92~3Ll~8"---
Lab File ID: Sample wt/vol:
Level: (low/med)
30.0 (g/mL) G.__
LOW
% Moisture: not dee. ~i~2 __ dee.
Extraction: (SepF/Cont/Sonc) SQm;
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/15/89
GPC Cleanup: (Y/N) H___ pH: _1...1 Dilution Factor: 10. 00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG(KG
319-84-6--------alpha-BHC. ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH~C---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8-----~---Heptachlor ________ _
309-00-2--------Aldrin. __________ _
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin. __________ _
33213-65-9------Endosulfan II. ______ _
72-54-8---------4,4'-DDD _________ _
1031-07-8-------Endosulfan sulfate ____ _
50-29-3---------4,4'-DOT _________ _
72-43-5---------Methoxychlor. _______ _
53494-70-5------Endrin ketone. ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene. ________ _
12674-11-2------Aroclor-1016
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 _______ _
53469-21-9------Aroclor-1242 _______ _
12672-29-6------Aroclor-1248. _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _______ _
91.
91.
91.
91.
91.
91.
91.
91.
180
180
180
180
180
180
180
910
180
910
910
1800
910
910
910
910
910
1800
1800
I
1u
IU
JU
JU u
u
u
u
u u
u
u u u
u
u
u
u
u u u
u u
u
u
u
u
Q
---------------o'Rll..,.-PE'....,----------~1B7~e""v-. -
79
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-10-lMS
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88\-REVS
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
30.0 (g/rnL) IL--
LOW
% Moisture: not dee. 11 dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL_ pH: --1..:...i
SAS No.: SDG No. : .,_7.,._ ___ _
Lab Sample ID: ~2L9~1~6~36._ __
Lab File ID:
Date Received: 10/04/89
Date Extracted: 10/23/89
Date Analyzed: 10/25/89
Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) VGLKG Q
I I
I 319-84-6--------alpha-BHC 9.0 IU
I 319-85-7--------beta-BHC 9.0 IU
I 319-86-8--------delta-BHC 9.0 u·
I 58-89-9---------gamma-BHC (Lindane) 9.0 u
I 76-44-8---------Heptachlor 9.0 u
I 309-00-2--------Aldrin 9.0 u
I 1024-57-3-------Heptachlor epoxide 9.0 u
I 959-98-8--------Endosulfan I 9.0 u
I 60-57-1---------Dieldrin 18. u
I 72-55-9---------4,4'-DDE 18. u
I 72-20-8---------Endrin 18, u
I 33213-65-9------Endosulfan II 18. u
I 72-54-8---------4,4'-DDD 18. u I
I 1031-07-8-------Endosulfan sulfate 18. u I
I 50-29-3---------4,4'-DDT 18. u I
I 72-43-5---------Methoxychlor 90. u I
I 53494-70-5------Endrin ketone 18. u I
I 5103-71-9-------alpha-Chlordane 90. u I
I 5103-74-2-------gamma-Chlordane 90. u I
I 8001-35-2-------Toxaphene 180 u I
I 12674-11-2------Aroclor-1016 90. u I
I 11104-28-2------Aroclor-1221 90. u I
I 11141-16-5------Aroclor-1232 90. u I
I 53469-21-9------Aroclor-1242 90. u I
I 12672-29-6------Aroclor-1248 90. u I
I 11097-69-1------Aroclor-1254 180 u I
I 11096-82-5----~-Aroclor-1260 180 u I
--......... 1.
I . ..
---------------oRM'"'I~ES'l' ]87 '"Rev,
iliiii:iii=ii::::iiiiiiE'i:c==i::5ia:.i&liSl ■S:lt::=4,_.L~ OR TR ft~ -. -7S
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-10-lMSD
La~ Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No_.: ___ SDG No.: -'--7"------
Matrix: (soil/water) SOIL Lab Sample ID: ~2~9~16~3~7'----
Sample w_t/vol: 30.0 (g/mL) L-Lab File ID:
Level: (low/med) LOW
% Moisture: not dee. £1_1 __ dee.
Date Received: 10/04/89
Date Extracted: 10/23/89
Date Analyzed: 10/25/89 Extraction: (SepF/Cont/Sonc) .5..Qlli:.
GPC Cleanup: (Y/N) H...._ pH:~ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
319-84-6--------alpha-BHC_________ 9.0 IU
319-85-7--------beta-BHC 9.0 IU
319-86-8--------delta-BH""c--------~ 9.0 IU
58-89-9---------gamma-BHC (Lindane)____ 9.0 IU
76-44-8---------Heptachlor_________ 9.0 IU
309-00-2--------Aldrin.__________ 9.0 IU
1024-57-3-------Heptachlor epoxide_____ 9.0 IU
959-98-8--------Endosulfan I________ 9.0 IU
60-57-1---------Dieldrin__________ 18. IU
72-55-9---------4,4'-DDE__________ 18. IU
72-20-8---------Endrin 18. U 33213-65-9------Endosu-~l~f_a_n_I.,..I_______ 18. U
72-54-8---------4,4'-0DD 18. U 1031-07-8-------Endosulf_a_n--su-l~f-=-a_t_e_____ 18. U
50-29-3---------4,4'-D~---------18.· U 72-43-5---------Methoxychlor________ 90. U
53494-70-5------Endrin ketone_______ 18. U
5103-71-9-------alpha-Chlordane______ 90. U
5103-74-2-------gamma-Chlordane______ 90. U
8001-35-2-------Toxaphene 180 U
12674-11-2------Aroclor-1""0-=-1-=-6--------90. u
0
11104-28-2------Aroclor-1221_______ 90. U I
11141-16-5------Aroclor-1232_______ 90. IU I
53469-21-9------Aroclor-1242_______ 90. 1u I
i2672-29-6------Aroclor-1248_______ 90. I U I
11097-69-1------Aroclor-1254________ 180 IU I
11096-82-5------Aroclor-1260_______ 180 IU I
··-···-·-··" -----------------------______ J __ J
---------------·ORM""!-PEST"-----------.79;--ilev~
77
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m
u
0 ~-----·
COMPUCHEM
lABORATORJES
Case Narrative #17902
SOG #90
Contract #(2-88)-REVS
CompuChem Laboratories, Inc.
SAMPLE IDENTIFICATIONS: SL-26-1, SL-27-1, SL-31-1, SL 32-1,
SL-33-1, SL-34-1, SL-35-1, SL-36-1, SL-37-1
These samples were received in good condition, with the
proper chains-of-custody (COC), sealed in a cooler on October
05 and 06, 1989. Analyses were scheduled in accordance with
the COC. Volatile, semivolatile, and pesticides analyses were
performed as requested on these samples. Holding time
requirements were met for all of these samples with the only
two exceptions being for the semivolatile fraction of samples
SL-26-1 and SL-27-1. These samples were reanalyzed to met
quality control requirements.
All pertinent Quality Assurance and Laboratory notices for
CASE# 17902, SDG# 90 are included in the sample data package.
VOLATILES:
There were Target Compound List (TCL) volatile analytes
identified above the Contract Required Quantitation Limits
(CRQLs) in all of these samples. No Tentatively Identified
Compounds (TICS) were found in these samples.
The associated instrument blanks, matrix
matrix spike duplicate (MSD) met all
requirements.
SEMIVOLATILES:
spike
quality
(MS) and
control
There were TCL semivolatile analytes
CRQLs in only one of these samples. TICS
of these samples.
identified above the
were found in eight
Sample SL-27-1 was analyzed twice due to a failure of the
internal standard 012-Perylene. It failed in both analyses as
the responses varied considerably from the Continuing
Calibration standard response. The repeat analysis confirmed
that a matrix effect may be the source of the variation. The
surrogate standard 2,4,6-Tribromophenol also was flagged as an
outlier in both analyses. It too may have been effected by the
matrix problem. one acid surrogate and one base surrogate is
allowed to fail recovery criteria as long as the recoveries are
greater than or equal to ten percent. Both of these analyses
are reported for this sample with reference to this qualifier.
COMPUCHEM L.ABORATORIES. lNC. P.O. Box 12652 3308 Chapel Hill !Nelton Highway Research Triangte Park. NC 27709 [phone]
l-79B1.. N SRIIPLE DRTR Slbi/Bll'IF--.. 128
•
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g
0
u
m :::::c=-· .. •··
----COMPLCHEM
lABOAATORJES
The associated method blanks met all quality control
requirements. The spikes were extracted outside of holding time
requirements in order to met quality control requirements. The
spike are reported with reference to this qualifier.
The ''X" qualifier is used on the Form I's to flag analytes
that coelute as indistinguishable isomers.
The Form VII for standard HK891028A06 lists the percent
difference for Pentachlorophenol as being outside of the
acceptable limit (less than 25%) when in fact it is not. This
variation is due to the rounding conventions used by Formaster.
The raw data lists the true percent difference within the
specified limit. This form is reported with reference to this
qualifier.
PESTICIDES:
There were no TCL pesticide analytes confirmed above the
CRQLs in these samples. The associated method blanks, matrix
spike, and matrix spike duplicate met all quality control
requirements.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and for
completeness,· for other than conditions detailed above. Release
of the data contained in.the hardcopy data package has been
authorized by the Laboratory Manager or his · designee, as
v·erified by the following signature.
Note: This report
accountability
&~~l
Daniel E. Boone, Jr.
TECHNICAL REVIEWER
is paginated
in decreasing
2
for reference and
nllllerical sequence.
J 19
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lA EPA SAMPLE NO. VOIATILE ORGANICS ANALYSIS DATA SHEET
SL-26-1
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292323
Sample wt/vol: 5.0 (g/mL) L._ Lab File ID: GH092323Cl9
Level: (low/med) LOW Date Received: 10/05/89
't Moisture: not dee. _u_ Date Analyzed: 10/13/89
Column: (pack/cap) C~f Dilution Factor: alL,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75~34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chlorotorm
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5-----~---l,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromotorm
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
1os-as-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
--::...::.£?.Sez, g-,rSRltPLE DRTR SUIIIIRRY-
t ..
Q
13 u
13 u
13 u
13 u
67 B
26 B
6 u
6 u
6 u
6 u
6 u
6 u
13 u
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
189
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-26-1
Lab Name: COMPUCHEM LABS Contract: {2-881-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: ..._90,.__
Lab Sample ID: _29-2_J=2~J~---Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
'I; Moisture: not dee. ___u
Column (pack/cap) CAI:!
Number TICs found: ---2
CAS NUMBER
(g/mL) L_
COMPOUND NAME
Lab File ID: GH092J2JC19
Date Received: 10/05/89
Date Analyzed: 10/lJ/89
Dilution Factor: &1~,o.._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG·
RT EST. CONC. Q
================ ============================ ======== =----------== •====
·-·· . -·-·-------- --. -·· ·---. ------
· FORK I VOA-TIC
IZSl!IZ-'-flfl. SR1'PLE DRTR SU/fll/JIJ.!/.
1/87 Rev.
JBS
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA.SHEET
SL-27-1
Lab Name: COMPUCHEM LABS Contract: (2~881-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SOG No.: 90
Matrix: (soil/water) SOIL Lab Sample IO: 292333
Sample wt/vol: 5.0 (g/mL) !i..._ Lab File IO: GH092333Al9
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. --5.i Date Analyzed: lO/lJ/89
Column: (pack/cap) GAii! Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,l-Oichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride
1os-os-4--------vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
12.4-48-1--------Dibromochloromethane
79-00-5---------1,l,2-Trichloroethane
71-43-2---------Benzene
10061-02~6------Trans-l,3-Dichloropropene __
1s-2s-2----'---,--Bromoform
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
Q
22 u
22 u
22 u
i2 u
95 B
35 B
11 u
11 u
11 u
11 u·
11 u
11 u
22 u
11 u
11 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
22 u
22 u
11 u
11 u
11 u
11 u
11 u
11 u
11 u
1/87 Rev.
187
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lE EPA SAMPLE NO.
·VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-27-1
Lab Name: COMPUCHEM LABS contract: C2-BBl-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: ---SDG No.: .._90"---
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: ( low/med) LOW
% Moisture: not dee. ~
Column (pack/cap) CA2
Number TICs found: ~
.CAS NUMBER
(g/mL) L_
COMPOUND NAME
Lab Sample ID: .-.2.,._9...,2,,_3,,_33,._ __ _
Lab File ID: GH092333Al9
Date Received: 10/05/89
Date Analyzed: 10/13/89
Dilution Factor: ... i~,o._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=======•===-==== •=========================== ======== ============= =====
-·· ·•··· ··-· -. -· ---- -···-._
FORM I VOA-TIC 1/87 Rev ..
186
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lA EPA SAMPLE NO. VOLATILE ORGANICS. ANALYSIS DATA SHEET
SL-31-1
Lab Name: COMPUCHEM LABS Contract: /2-881-REVS
Lab Code: COMPO case No.: 17902 SAS No.: SOG No.: 90
Matrix: ( soil/water) SOIL Lab Sample IO: 292753
Sample wt/vol: s,o (g/mL) L__ Lab File ID: GH092753Cl9
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. ~ Date Analyzed: l0(Hie2
Column: (pack/cap) Cll,f Dilution Factor: ali-~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Oisultide
75-35-4---------l,l-Dichloroethene
75-34-3---------l,l-Dichloroethane
540--59-o--------l, 2-Dichloroethene (total)_
67-66-3---------Chlorotorm
107-06-2--------l,2-Dichloroethane
78-93-3---------2-Butanone
11~ss-6---------1,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4~--------Bromodichloromethane
78-87-5---------l,2-Dichloropropane
10061-01-5------cis-l,J-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------l,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l, 3-Dichlo_ropropene __
75-25-2---------Bromotorm ·
ios-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------l,l,2,2-Tetrachloroethane __
1os-sa-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene
lJJo-20-1-------Total Xylenes
FORM I VOA
J-7,BR g9 SRIIPLE DRTR SUIIIIRII,,,
Q
11 · u
11 u
11 u
ll u
16 B
ll B
5 u
5 u
5 u
5 u
5 u
5 u
ll u
5 u
5 u •
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5· u
11 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
105
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
EPA SAMPLE NO.
SL-31-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL
Sample wt/vol: 5,0
Level: (low/mad) LOW
% Moisture: not dee. ~
Column (pack/cap) CA2
Number TICs found: __g_
CAS NUMBER
(g/mL) !i__
COMPOUND.NAME
Lab Sample ID: 292753
Lab Fila ID: GH092753Cl9
Data Received: 10/06/89
Data Analyzed: 10/14/89
Dilution Factor:, ...,1.._1 o~--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
======•========= •=========================== ====•=== -===---------=====
FORM I VOA-TIC 1/87 Rev.
I. -=-c-""'--· ....:_::·:-~:-z=,-Z,~7~!--~-..-;aSRIIPL6 DRTR. SlJIUllilllY
t
184
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-32-1 Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lah Sample ID: 292754
Sample wt/vol: 5,0 (g/mL) L_ Lab File ID: GH092754Cl9
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. ~ Date Analyzed: 10/14,:'.~9
Column: (pack/cap) CAf Dilution Factor: Al~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG.
74-87-3---------Chloromethane 11
74-83-9---------Bromomethane 11
75-01-4---------Vinyl Chloride 11
75-00-3---------Chloroethane 11
75-09-2---------Methylene Chloride 15
67-64-1---------Acetone 16
75-15-o---------carbon Disulfide 5
75-35-4---------1,l-Dichloroethene 5
75-34-3------~--l,l-Dichloroethane 5
540-59-0--------1,2-oichloroethene (total)_ 5
67-66-3---------Chloroform 5
107-06-2--------1,2-Dichloroethane 5
78-93-3---------2-Butanone 11
71-55-6---------1,1,1-Trichloroethane 5
56-23-5---------carbon Tetrachloride 5
108-05-4--------Vinyl Acetate 11
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 5
10061-0l-5------cis-l,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79~00-s---------1,1,2-Trichloroethane 5
71-43-2---------Benzene 5
10061~02-6------Trans-l,3-Dichloropropene __ 5
75-25-2---------Bromoform 5
1os-10-1--------4-Methyl-2-Pentanone 11
591-78-6--------2-Hexanone 11
127-18-4--------Tetrachloroethene 5
79-34-5---------1,l,2,2-Tetrachloroethane __ 5
108-88-3--------Toluene 5
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzene 5
100-42-s--------styrene 5
1330-20-7-------Total Xylenes 5
FORM I VOA
Q
u
u
u u
8
B
u
u u u
U·
u
u u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
1/87 Rev.
1BJ
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-32-l
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab code: COMPO Case No.: 17902 SAS No.: ---SDG No.: .._90,.___
Matrix: ( soil/water) SOIL
sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dee. _i
Column (pack/cap) GAf
Number TICs tound: __o_
CAS NUMBER
(g/mL) li__
COMPOUND NAME
Lab Sample ID: ~294 2L7~5~41.--__ _
Lab File ID: GH092754Cl9
Date Received: 10/06/89
Date Analy_zed: 10/14/89
Dilution Factor: £1L,o"----
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
FORM I VOA-TIC l/87 Rev.
182
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
SL-33-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292755
Sample wt/vol: s,o (g/mL) L._ Lab File ID: GH092755C19
Level: (low/med) LOW Date Received: 10/06/89
t Moisture: not dee. --1. Date Analyzed: 10/UIBI!
Column: (pack/cap) GAf Dilution Factor: ~i~-~o __ _
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) QG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4-----~---Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone \ 75-15-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,l-Dichloroethane
540-59-0--------l,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2---~----l,2-Dichloroethane
78-93-3-------~-2-Butanone
71-55-6~--------l,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzen•
10061-02-6------Trana-l,3-Dichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,l,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
Q
11 u
11 u
11 u
11 u
12 B
10 BJ
5 u
5 u
5 u
5 u
5 u
.5 u
11 u
5 u
5 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
11 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
JBJ
I
I
lE
VOLATILE ORGANICS ANALYSIS DATA S.HEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab code: COMP!f Case No.: 17902 SAS No.:
EPA SAMPLE NO.
SL-33-l
I Matrix: (soil/water) SOIL
SDG No. : "-90,,___
Lab Sample ID: 292755
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Sample wt/vol: 5.0 (g/mL) !i...._
Level: (low/med) LOW
% Moisture: not dee._:,_
Column (pack/cap) CAP
Number TICs found: ___Q
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
GH092755Cl9
10/06/89
10/14/89
1,0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== ============= =====
FORM I VOA-TIC l/87 Rev.
188
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-34-1
Lab Name: COMPUCHEM LABS contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: S DG No. : -"9-"0'---
Matrix: ( soil/water) SOIL Lab Sample ID: 292756
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH092756Cl9
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. _lQ Date Analyzed: 10/14/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/1\;~ Q
74-87-3--------~Chloromethane ' 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75~09-2---------Methylene Chloride 15 B
67-64-1---------Acetone 20 B
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-s---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u.
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane· 6 u
79-oo-s---~-----l,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
-.: ~
... I 61FrT• S,...DR:rR.... SSit(MtNM-f!Wi!=..:C-:;..· _::::=-..:c......
t
99
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lE
VOLATILE ORGl\NICS l\NALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88}-REVS
EPA SAMPLE NO.
SL-34-1
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: ,,_9"--0 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) g_
Level: ( low/med) LOW
% Moisture: not dee. _.ll
Column (pack/cap) CAI!
Number TICs found: __o_
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L oi.-ug/Kg) UG/KG.
292756
GH092756Cl9
10/06/89
10/14/89
l.,Q
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ------=---=-==== ============================ ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
98
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-35-1
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292757
Sample wt/vol: 5.0 (g/mL) !i,__ Lab File ID: GH092757Cl9
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. __JJ. Date Analyzed: lO/U/89
Column: (pack/cap) C~f Dilution Factor: ~i~1~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------l,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,J-Dichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
1oa-aa-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4------~-Ethylbenzene
100-42-s--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
Q
11 u
11 u
11 u
11 u
13 B
15 B
6 u
6 u
6 u.
6 u
6 u
6 u
11 u
6 u
6 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
11 u
11 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
97
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I
I
lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS
Lab code: COMPU Case No.: 17902
Matrix: ( soil/water) SOIL
Sample wt/vol: s,o (g/mL)
Level: (low/med) LOW
\ Moisture: not dee. ~
Column (pack/cap) C6f
Number TICs found: __Q
SL-35-1
Contract: 12-88)-REVS
SAS No.: SDG No.: 90
L_
Lab Sample IO: 292757
Lab File ID: GH092757Cl9
Date Received: 10/06/89
Date Analyzed: 10/14/89
Dilution Factor: ~l~.o,._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC.· Q ================ =-------=----------=-=-==--= ======== ============ =====
. FORM I VOA-TIC 1/87 Rev .
----·----------~ -----· -.. 19 sa•1... E-ORTR . ifii6111--lfi il•E'::=:=-=-96
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I
lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-36-1
Lab Name: COMPUCHEM LABS Contract: 12-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ~9~0 __
Matrix: ( soil/water) SOIL Lab Sample ID: 292758
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH092758Cl9
Level: ( low/med) LOW Date Received: 10/06/89
% Moisture: not dee. _ll Date Analyzed: 10/14/89
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 14 B
67-64-1---------Acetone 10 BJ
75-15-o---------carbon Disulfide 6 u
75-35-4---------l,l-Dichloroethene 6 u
75-34-3---------l,l-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------l,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87~5---------1,2-Dichloropropane 6 u
10061-0l-S------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4---~----Ethylbenzene 6 u
100-42-s--------styrene .6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
Ii 8 . •• j %PL 6 ORTR-~:RlillFr,11•--!l►E.:· ==-95
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-36-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -90 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) rpw
% Moisture: not dee. ~
Column (pack/cap) CAf
Number TICs found: __o_
CAS NUMBER
(g/mL) _G_
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
292758
GH092758Cl9
10/06/89
10/14/89
1.0
COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
=··-=:a.:.....:::-·::-::·2· 5:::a:!,,, .. .::::i;;:ci:oiiii==z;IJ~7Q-»S:::ialll_,;_E·:;;jSQli ... r.i ... WTIIFl!! ... 'LL6 DR TR-JS4~!.~11111••·•11!1!1tr!il!CE::. ·a;;··::.::::=~-'---
t
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1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-37-1
Lab Name: coMPUCHEM LABS Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
·Matrix: ( soil/water) SOIL Lab Sample ID: 292759
Sample wt/vol: 5.0 (g/mL) L_ Lab File ID: GH092759Cl9
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. ---8. Date Analyzed: lO/H/§9
Column: (pack/cap) CM! Dilution Factor: _1~,o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
7 5-34-3----·-----l, 1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chlorotorm
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cia-l,J-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6--~---Trans-l,3-Dichloropropene __
75-25-2---------Bromotorm
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
1oa-aa-J~-------Toluene
108-90-7--------Chlorobenzene
100-41-4-----~--Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenea
FORM I VOA
Q -
11 u
11 u
11 u
11 u
12 B
9 BJ
5 u
5 u
5 u
5 u
5 u
5 u
11 u
5 u
5 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
11 u
11 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
1/87 Rev.
93
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
EPA SAMPLE NO.
SL-37-1
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL
sample wt/vol: s.o (g/mL)
Level: (low/med) LOW
t Moisture: not dee. ----8.
Column (pack/cap) Cll.f
Number TICs found: __a_
L_
Lab Sample ID: 292759
Lab File ID: GH092759Cl9
Date Received: 10/06/89
Date Analyzed: 10/U/89
Dilution Factor: £1~.o,._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ===========o===• •=========================== am====== ==--:i::11======== =====
FORM I VOA-TIC 1/87 Rev.
---.. -· .,, •----,.,,:;;,i._ --,. -. ----I SIIIIPCE Dl17R-JiSi,f;£MT--l!l.1=4 :;:::;::.'=.:::;__
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-26-lMS
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ..._90"---
Matrix: ( soil/water) SOIL Lab Sample ID: 292327
Sample wt/vol: 5,0 (g/mL) ~ Lab File ID: GH092327Cl9
Level: (low/med) LOW Date Received: 10/05/89
I Moisture: not dee. _,ll Date Analyzed: 10/13/89
Column: (pack/cap) CAf Dilution Factor: al~,o._ __
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
13
13
75-01-4---------Vinyl Chloride · 13
75-00-3---------Chloroethane 13
75-09-2---------Methylene Chloride 49
67-64-1---------Acetone 31
75-15-o---------carbon Disulfide 6
75-35-4---------1,l-Dichloroethene 6
75-34-3---------1,1-Dichloroethane 6
540-59-0--------l,2-Dichloroethene (total)_ 6
67-66-3---------Chloroform 6
107-06-2--------1,2-Dichloroethane 6
78-93-3---------2-Butanone 13
71-55-6---------1,1,1-Trichloroethane 6
56-23-5-------..:-carbon Tetrachloride 6
108-05-4--------Vinyl Acetate 13
75-27-4---------Bromodichloromethane 6
78-87-5---------1,2-Dichloropropane 6
10061-0l-5------cis-l,3-Dichloropropene 6
79-01-6---------Trichloroethene 6
124-48-1--------Dibromochloromethane 6
79-00-5---------1,1,2-Trichloroethane 6
71-43-2---------Benzene 6
10061-02-6------Trans-l,3-Dichloropropene __ 6
75-25-2---------Bromoform 6
100-10-1--------4-Methyl-2-Pentanone 13
591-78-6--------2-Hexanone 13
127-18-4--------Tetrachloroethene 6
79-34-5---------1,1,2,2-Tetrachloroethane __ 6
100-aa..:3-------.,-Toluen• 6
108-90-7--------Chlorobenzene 6
100-41-4--------Ethylbenzene 6
100-42-s--------styrene 6
1330-20-7-------Total Xylenes 6
Q
u
u
u u
B
B u u u u u u
u u u u u u
u
u u u u u u u u
u u u u u u u
FORM I VOA 1/87 Rev.
., 2· ,. ss•PL.. DR.TR-AF ,, 91
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SL-26-lMSD
Lab Name: CQMPUCHEM LABS Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292328
Sample wt/vol: s,o (g/lllL) li..._ Lab File ID: GH092J28Cl9
Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not dee. --2.l Date Analyzed: lO/lJ/89
Column: (pack/cap) C6i! Dilution Factor: al~1~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-oichloroethane
540-59-0--------1,2-Dichloroethene (total)_·_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
1a-a1-s---------1,2-oichloropropane
10061-01-s------cis-l,3-0ichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-s---~-----1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-1,3-0ichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1, 1, 2, 2-Te.trachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
FORM I VOA
Ii » ••
Q
13 u
lJ u
13 u
13 u
53 B
33 B
6 u
6 u
6 u
6 u
6 u
6 u
13 u
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
98
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1B EPA SAMPLE. NO. .SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-26-1.
Lab Name: COMPUCHEM LABS Contract: (2-881-REVS
Lab Code: COMPU Case No,: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292323
sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: G2R92323A06
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. --2..3. dee. Date Extracted: 10/24/89
Extraction:
GPC Cleanup:
( SepF / Cont/ Sonc)
(Y/N) IL.. pH: 6.4
Date Analyzed: 10/28/89
Dilution Factor: _1~,~RR~--
CAS NO. COMPOUND
CONCENTRATION. UNITS:
(ug/L or ug/Xg) UG/KG
108-95-2--------Phenol 430
lll-44-4--------bis(2-Chloroethyl)Ether 430
95-57-8---------2-Chlorophenol 430
541-73-1--------1,3-Dichlorobenzene 430
106-46-7--------1,4-Dichlorobenzene 430
100-51-6--------Benzyl Alcohol 430
95-50-1---------1,2-Dichlorobenzene 430
95~48-7---------2-Methylphenol 430
39638-32-9------bis(2-Chloroisopropyl)Ether_ 430
106-44-5--------4-Methylphenol 430
621-64-7--------N-Nitroso-Di-n-Propylamine __ 430
67-72-1---------Hexachloroethane 430
98-95-3---------Nitrobenzene 430
78-59-1---------Isophorone 430
BB-75-5-------~-2-Nitrophenol 430
105-67-9--------2,4-Dimethylphenol 430
65-85-o---------Benzoic Acid 2100
lll-91-l--------bis(2-Chloroethoxy)Methane_ 430
120-83-2--------2,4-Dichlorophenol 430
120-e2-1--------l,2,4-Trichlorobenzene 430
91-20-3---------Naphthalene 430
106-47-8--------4-Chloroaniline 430
87-68-3--~------Hexachlorobutadiene 430
59-50-7---------4-Chloro-3-Methylphenol 430
91-57-6---------2-Methylnaphthalene 430
77-47-4---------Hexachlorocyclopentadiene __ 430
BB-06-2---------2,4,6-Trichlorophenol 430
95-95-4---------2,4,5-Trichlorophenol 2100
91-58-7---------2-Chloronaphthalene 430
88-74-4---------2-Nitroaniline 2100
131-11-3--------Dimethyl Phthalate 430
208-96-8--------Acenaphthylene 430
606-20-2--------2,6-Dinitrotoluene 430
Q
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FORM I sv-1 1/87 Rev.
89
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABS Contract: /2-881-REVS
Lab Code: COMPU Case No.: 17902 sAS· No.: SOG
EPA SAMPLE NO.
SL-26-l
No.: 90 I Matrix: (soil/water) SOIL Lab Sample ID: 292323
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Sample wt/vol: 30,0 (g/mL) ~ Lab File IO: G2R92323A06
Level: (low/med) .,LO...,W,___ Date Received: 10/05/89
% Moisture: not dee. --2.3. dee. Date Extracted: 10/24/!!9
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10/28/89
GPC Cleanup: (Y/N) li.._ pH: 6,4 Dilution Factor: •l~,o~o.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
-99-09-2---------3-Nitroaniline 2100 u
83-32-9---------Acenaphthene 430 u
51-28-5---------2,4-Dinitrophenol 2100 u
100-02-1--------4-Nitrophenol 2100 u
132-64-9--------Dibenzoturan 430 u
121-14-2--------2,4-Dinitrotoluene 430 u
84-66-2---------Diethylphthalate 430 u
7005-72-3-------4-Chlorophenyl-phenylether_ . 430 u
86-73-7----~----Fluorene 430 u
100-01-6--------4-Nitroaniline 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2100 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 430 u
101-55-3------~-4-Bromophenyl-phenylether_-_ 430 u
118-74-1--------Hexachlorobenzene 430 u
87-86-5---------Pentachlorophenol 2100 u
85-01-8---------Phenanthrene 430 u
120-12-1--------Anthracene 430 u
84-74-2---------Di-n-Butylphthalate 430 u
206-44-0--------Fluoranthene 430 u
129-00-0--------Pyrene 430 u
85-68-7---------Butylbenzylphthalate 430 u
91-94-1---------3,3'-0ichlorobenzidine 860. u
56-55-3---------Benzo(a)Anthracene 430 u
218-01-9--------Chrysene 430 u
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 56 J
117-84-0--------Di-n-octyl Phthalate 430 u
205-99-2--------Benzo(b)Fluoranthene 430 u
207-08-9--------Benzo(k)Fluoranthene 430 u
50-32-8---------Benzo(a)PyrGne 430 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 430 u
53-70-3---------Dibenzo(a,h)Anthracene 430 u
191-24-2--------Benzo(g,h,i)Perylene 430 u
(l) -Cannot be separated from Diphenylamine
FORM I sv-2. l/87 Rev.
88
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-26-l
Lab Name: CQMPUCHEM LABS contract: 12-88)-REYS
Lab Code: COMPU Case No.: 17902 SAS. No.: SDG No.: .,_90,.___
Matrix: (soil/water) SOIL Lab Sample ID: _29.._2_3~2~3 ___ _
sample wt/vol: 30,0 (g/mL) !i,_ Lab File ID: G2R9232JA06
Level: (low/med) ..,LQ .... w,__ Date Received: 10/0518'9
t Moisture: not dee. --1.3. dee. Date Extracted: 10/24/89
Extraction: (SepF/Cont/Sonc) _s.ow= Date Analyzed: 10/28/89
GPC Cleanup: (Y/Nl tL_ pH: 6,4 Dilution Factor: _1~,o_o __
CONCENTRATION UNITS:
Number TICs found: ---2. (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
c••=m======••••• ••=========-=~==c=•====-=== --=-n••= -==========-== -====
l. BLANK CONTAMINANT 6.28 J90 BJ
2. BLANX CONTAMINANT 6.33 610 BJ
FORM I SV-TIC 1/87 Rev.
87
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-27-1
Lab Name: COMPUCHEM LABS Contract: 12-88}-REVS
Lab Code: COMPU Case No.: 17902 SAS No. : SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292333
sample wt/vol: 30.0 (g/mL) G __ Lab File ID: G2B92333C06
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. ---2! dee. Date Extracted: 1004/89
Extraction: ( SepF /Cont/ so·nc)
(Y/N) li........
§.Qli.C
6.2
Date Analyzed: 11/01/89
GPC Cleanup: pH: Dilution Factor: 1.00 ~~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol .720
lll-44-4--------bis(2-Chloroethyl)Ether 720
95-57-8---------2-Chlorophenol 720
541-73-1--------1,3-Dichlorobenzene 720
106-46-7--------1,4-Dichlorobenzene 720
100-51-6--------Benzyl Alcohol 720
95-50-1---------1,2-Dichlorobenzene 120
95-48-7---------2-Methylphenol 720
39638-32-9------bis(2-Chloroisopropyl)Ether_ 720
106-44-5--------4-Methylphenol 720
621-64-7--------N-Nitroso-Di-n-Propylamine __ 720
67-72-1---------Hexachloroethane 720
98-95-3---------Nitrobenzene 720
78-59-1---------Isophorone 720
88-75-5---------2-Nitrophenol 720
105-67-9--------2,4-Dimethylphenol 720
65-85-0---------Benzoic Acid 3500
lll-91-l--------bis(2-Chloroethoxy)Methane __ 720
120-83-2--------2,4-Dichlorophenol 720
120-s2-1--------l,2,4-Trichlorobenzene 720
91-20-3---------Naphthalene 360
106-47-8--------4-Chloroaniline 720
87-68-3---------Hexachlorobutadiene 720
59-50-7---------4-Chloro-3-Methylphenol 720
91-57~6---------2-Methylnaphthalene 270
77-47-4---------Hexachlorocyclopentadiene __ 720
88-06-2---------2,4,6-Trichlorophenol 720
95-95-4---------2,4,5-Trichlorophenol 3500
91-58-7---------2-Chloronaphthalene 720
88-74-4---------2-Nitroaniline 3500
131-11-3--------oimethyl Phthalate 720
208-96-8--------Acenaphthylene 530
606-20-2--------2,6-Dinitrotoluene 720
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FORM I SV-1 1/87 Rev.
.:119. -S.OW"t. E OIIU'•-SU • Lf -.: . S6
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-27-1
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292333
Sample wt/vol: 3Q.Q (g/mL) _G __ Lab File ID: G2R92333C06
' Level: ( low/med) LOW Date Received: 10/05/89
% Moisture: not _dee. _ll dee. bate Extracted: 1on41s9
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: ll/01/89
GPC Cleanup: (Y/N) li._ pH: 6.2 Dilution Factor: 1.00 ~~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 3500
83-32-9---------Acenaphthene 720
51-28-5---------2,4-Dinitrophenol 3500
100-02-7--------4-Nitrophenol 3500
132-64-9--------Dibenzofuran 720
121-14-2--------2,4-Dinitrotoluene 720
84-66-2---------Diethylphthalate · 720
7005-72-3-------4-Chlorophenyl-phenylether __ 720
86-73-7---------Fluorene 320
100-01-6--------4-Nitroaniline 3500
534-52-1--------4,6-Dinitro-2-Methylphenol __ 3500
86-30-6---------N-Nitrosodiphenylamine (1)_ 720
101-55-3--------4-Bromophenyl-phenylether __ 720
118-74-1--------Hexachlorobenzene 720
87-86-5---------Pentachlorophenol 3500
85-01-8---------Phenanthrene 1400
120-12-1--------Anthracene 260
84-74-2---------Di-n-Butylphthalate 720
206-44-0--------Fluoranthene 800
129-00-0--------Pyrene 1100
85-68-7---------Butylbenzylphthalate 720
91-94-1---------3,3'-Dichlorobenzidine 1400
56-55-3---------Benzo(a)Anthracene 490
218-01-9-------~Chryserie 640
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 250
117-84-0--------Di-n-Octyl Phthalate 720
205-99-2--------Benzo(b)Fluoranthene 610
2 07-08.-9--------Benzo ( k) Fluoranthene 610
50-32-8---------Benzo(a)Pyrene 530
193-39-5--------Indeno(l,2,3-cd)Pyrene 160
53-70-3---------Dibenzo(a,h)Anthracene 720
191-24-2--------Benzo(g,h,i)Perylene 200
(1) -Cannot be separated from D1phenylam1ne
Q
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u u
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JX
JX
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J
FORM I SV-2 1/87 Rev.
Ii I ,pa I CPL E -DRTII-St S&WJ 85
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: C2-88l-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
SL-27-1
No.: 90
2923JJ
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: G2R92JJJC06
Level: ( low/med) LOW
% Moisture: not dee. _M dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) lL. pH: 6.2
Number TICs found:~-
CAS NUMBER COMPOUND NAME
Date Received: 10/05/89
Date Extracted: 10/24,:'.89
Date Analyzed: ll,:'.Ol,:'.89
Dilution Factor: al~•=O=O __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= =====
l. . ALDOL 7.20 1500 AJ
2. ALDOL 7.67 1900 AJ
J. UNKNOWN PNA 17.29 3000 J
4. UNKNOWN 18.14 4600 J
5. UNKNOWN 18.34 6000 J
6. UNKNOWN 18.55 JOOO J
7. UNKNOWN 19 .14 5400 J
8. UNKNOWN 19.87 2900 J
9. UNKNOWN 20.02 6600 J
10. UNKNOWN 20.17 4200 J
11. UNKNOWN 20.69 J800 J
12. UNKNOWN 21.90 JSOO J
lJ. UNKNOWN 22.00 4600 J
14. UNKNOWN 22.40 7200 J
15. UNKNOWN 22.70 12000 J
16. UNKNOWN 23.24 8000 J
17. UNKNOWN 23.55 4000 J
18. UNKNOWN 2J.89 4JOO J
19. · UNKNOWN 24.45 5900 J
20. UNKNOWN 25.01 7200 J
21. UNKNOWN 25.12 '6JOO J
22. UNKNOWN 26. 41 8700 J
FORM I SV-TIC 1/87 Rev.
==a:...="'.=:s:=E--:;1,~ail!!ll-.::»~:ti•lll1t:IIE=:-$i5'Rai••r,..'LE DR TR -.!Sa.tl:AF--lllli!;;..:_. ---__ :·: __ -
t.
84
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1B
SEMIVOLATILE ORGANICS ANALYSIS' DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS contract: 12-881-REVS
SL-31-1
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No. : .,_9.,.0 __
Matrix: (soil/water) SOIL Lab Sample IO: 292753
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GHQ92753AQ4
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. --8. dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc)
(Y/N) li...._
Date Analyzed: 10/li/89
GPC Cleanup: pH: 7.1 Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/Kg Q
108-95-2--------Phenol 360 u
lll-44~4--------bis(2-Chloroethyl)Ether 360 u
95-57-8---------2-Chlorophenol 360 u
541-73-1--------1,3-Dichlorobenzene 360 u
106-46-7--------1,4-Dichlorobenzene 360 u
100-51-6--------Benzyl Alcohol 360 u
95-50-1---------1,2-Dichlorobenzene 360 u
95-48-7---------2-Methylphenol 360 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 360 u
106-44-5--------4-Methylphenol 360 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 360 u
67-72-1---------Hexachloroethane 360 u
98-95-3---------Nitrobenzene 360 u
78-59-1---------Isophorone 360 u
88-75-5---------2-Nitrophenol 360 u
105-67-9--------2,4-Dimethylphenol 360 u
65-85-0---------Benzoic Acid 1700 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 360 u
120-83-2--------2,4-Dichlorophenol 360 u
120-e2-1--------l,2,4-Trichlorobenzene 360 u
91-20-3---------Naphthalene 360 u
106-47-8--------4-Chloroaniline 360 u
87-68-3---------Hexachlorobutadiene 360 u
59-50-7---------4-Chloro-3-Methylphenol 360 u
91-57-6---------2-Methylnaphthalene 360 u
77-47-4---------Hexachlorocyclopentadiene __ · 360 u
88-06-2---------2,4,6-Trichlorophenol 360 u
95-95-4---------2,4,5-Trichlorophenol 1700 u
91-58-7---------2-Chloronaphthalene 360 u
88-74-4---------2-Nitroaniline 1700 u
131-11-3--------Dimethyl Phthalate 360 u
208-96-8--------Acenaphthylene 360 u
606-20-2--------2,6-Dinitrotoluene 360 u
.
FORM I sv-1 ·l/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS.DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: 12-881-REVS SL-31-1
Lab Code: COMPU . Case No.: 17902 SAS No.: SOG No.: ..._9,._0 __
Matrix: (soil/water) SOIL Lab Sample ID: 292753
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH09275JA04
Level: ( low/med) I.OW
% Moisture: not dee. --8.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL.
dee.
pH:
~
7,1
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/14/89
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700
83-32-9---------Acenaphthene 360
51-28-5---------2,4-Dinitrophenol 1700
100-02-1--------4-Nitrophenol 1700
132-64-9--------Dibenzoturan 360
121-14-2--------2,4-0initrotoluene 360
84-66-2---------Diethylphthalate 360
7005-72-3-------4-Chlorophenyl-phenylether_ 360
86-73-7---------Fluorene 360
100-01-6--------4-Nitroaniline 1700
534-52-1--------4,6-Dinitro-2-Methylphenol_ . 1700
86-30-6---------N-Nitrosodiphenylamine (l)_ 360
101-55-3--------4-Bromophenyl-phenylether __ 360
118-74-1--------Hexachlorobenzene 360
87-86-5---------Pentachlorophenol 1700
ss-01-s---------Phenanthrene 360
120-12-1--------Anthracene 360
84-74-2---------Di-n-Butylphthalate 360
206-44-o--------Fluoranthene 360
129-oo-o-~------Pyrene 360
85-68-7---------Butylbenzylphthalate 360
91-94-1---------3,3'-Dichlorobenzidine 720
56-55-3---------Benzo(a)Anthracene 360
218-01-9--------Chry•ene ' 360
117-81-7-~------bi•(2-Ethylhexyl)Phthalate_ 360
117-84-0--------Di-n-OCtyl Phthalate 360
205-99-2--------Bcanzo(b)Fluoranthene 360
207-08-9--------Benzo(k)Fluoranthene 360
50-32-8---------Benzo(a)Pyrene 360
193-39-5--------Indeno(l,2,3-cd)Pyrene 360
53-70-3---------Dibenzo(a,h)Anthracene 360
191-24-2--------Bonzo(g,h,i)Perylene 360
(l) -CaMot be separated trom Diphenylamine
Q
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FORM I sv-2 1/87 Rev.
S2
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS' DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-31-l
Lab Name: COMPUCHEM LABS Contract: (2-88)-REVS
Lab Code: COMPU Case No,: 17902 SAS No.: SDG No.: .,,_90,.___
Matrix: (soil/water) SOIL Lab Sample ID: .,.2.,,.9.._27.,_5"'3,__ __ _
Sample wt/vol: 30.0 (g/mL) L_
Level: ( low/med) LOW
\ Moisture: not dee. ____i dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL.. pH: 7,1
Number TICs tound: __Q
CAS NUMBER COMPOUND NAME
Lab File ID: GH092753A04·
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/14/89
Dilution Factor: .1~,o~o.__
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=•••a===m=a•-u• ••======•===============a=== •======-•=••========a •====
FORM I SV-TIC 1/87 Rev.
Bl
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SEMIVOLATILE ORGANICS ANALYSIS 'DATA SHEET EPA SAMPLE NO.
Lab Name: coMPtJCHEM LABS Contract: (2-88)-REVS
SL-31-lRE
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292753
Sample wt/vol: 30.0 (g/mL) L-Lab File ID: GJ092753A04
Level: (low/med) i;.QW Date Received: 10/06/89
"".,,-.,:,r.'-., •
% Moisture: not dee. ___.J: dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) SQH.C Date Analyzed: 10/15/89
GPC Cleanup: (Y/N) L. pH: 7.1 Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS. NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 360 u
lll-44-4--------bia(2-Chloroethyl)Ether 360 u
95-57-8---------2-Chlorophenol · · 36.0 U·
541-73-1--------1,3-Dichlorobenzene 360 u
106-46-7--------1,4-Dichlorobenzene 360 u
100-51-6--------Benzyl Alcohol 360 u
95-so-1---------1,2-Dichlorobenzene 360 u
95-48-7---------2-Methylphenol 360 u
39638-32-9------bia(2-Chloroisopropyl)Ether_ 360 u
106-44-5--------4-Methylphenol 360 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 360 u
67-72-1---------Hexachloroethane 360 u
98-95-3---------Nitrobenzene 360 u
78-59-1---------Isophorone 360 u
88-75-5---------2-Nitrophenol 360 u
105-67-9--------2,4-Dimethylphenol 360 u
65-85-o---------Benzoic Acid 1700 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 360 u
120-83-2--------2,4-Dichlorophenol 360 u
120-s2-1--------1,2,4-Trichlorobenzene 360 u
91-20-3---------Naphthalene 360 u
106-47-8--------4-Chloroaniline 360 u
87-68-3---------Hoxachlorobutadiene 360 u
59-50-7---------4-Chloro-3-Methylphenol 360 u
91-57-6---------2-Methylnaphthalene 360 u
77-47-4---------Hoxachlorocyclopentadiene __ . 360 u
88-06-2---------2,4,6-Trichlorophenol 360 u
95-95-4---------2,4,5-Trichlorophenol 1700 u
91-58-7---------2-Chloronaphthalene 360 u
88-74-4---------2-Nitroaniline 1700 u
131-11-3--------Dimethyl Phthalate 360 u
208-96-8--------Acenaphthylene 360 u
606-20-2--------2,6-Dinitrotoluene 360 u
FORM I sv-1 1/87 Rev.
•• • •• mn_s .. ORT/ii SU#IIUlli-'L'-::. -· ·--· . 88
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-31-lRE
Lab Name: COMPUCHEM LABS contract: {2-88\-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample IO: 292753
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GJ092753A04
Level: (low/med) LOW Date Received: 10/06/89
\ Moisture: not dee. dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc)
(Y/N) If_
.s.olil:
7.1
Date Analyzed: 10/15/89
GPC Cleanup: pH: Dilution Factor: .1L·~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700
83-32-9-~-------Acenaphthene 360
51-28-5---------2,4-Dinitrophenol 1700
100-02-7--------4-Nitrophenol 1700
132-64-9--------Dibenzofuran 360
121-14-2--------2,4-Dinitrotoluene 360
84-66-2---------Diethylphthalate 360
7005-72-3-------4-Chlorophenyl-phenylether __ 360
86-73-7---------Fluorene 360
100-01-6--------4-Nitroaniline 1700
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1700
86-30-6---------N-Nitrosodiphenylamine (l)_ 360
101-55-3--------4-Bromophenyl-phenylether __ 360
118-74-1--------Hexachlorobenzene 360
87-86-5---------Pentachlorophenol 1700
85-01-8---------Phenanthrene 360
120-12-1--------Anthracene 360
84-74-2---------oi-n-Butylphthalate 77
206-44-o--------Fluoranthene 360
129-00-0--------Pyren• 360
85-68-7---------Butylbenzylphthalate 360
91-94-1-------~-3,3'-Dichlorobenzidine 720
56-55-3---------Benzo(a)Anthracene 360
21a-01-9--------Chryaen• 360
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 360
111-a,-0--------01-n-octyl Phthalate 360
205-99-2--------Benzo(b)Fluoranthene 360
207-08-9--------Benzo(k)Fluoranthene 360
50-32-8---------Benzo(a)Pyrene 360
193-39-5-~------Indeno(l,2,3-cd)Pyrene 360
53-70-3---------Dibenzo(a,h)Anthracene 360
191-24-2--------eenzo(g,h,i)Perylene 360
(1) -cannot be separated from Diphenylamine
Q
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FORM I sv-2 1/87 Rev.
79
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
SL-31-lRE
Lab Code: COMPU Case No,: 17902
Matrix: (soil/water) SOIL
SAS No.: SDG No.: .,,_9,._0 __
Lab Sample ID: -2-92_7~5~3~---
Sample wt/vol: 30,0 (g/mL) IL_
Level: (low/med) .,.LO...,W:,___
% Moisture: not dee. __a_ dee.
Extraction: (SepF/Cont/Sonc) SOHC
GPC Cleanup: (Y/N) IL_ pH: 7,1
Number TICs found: __o_
CAS.NUMBER COMPOUND NAME
Lab File ID: GJ092753A04
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/15/89
Dilution Factor: .1L,o~o,.___
CONCENTRATION UNITS:"
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
===a=====•=••==• ===-===-=============--=-== -=-==== •••-===m==s --==
FORM I SV-TIC 1/87 Rev
78
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lB .
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS contract: C2-88)-REYS
SL-32-l
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab.Sample ID: 292754
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GJ092754A04
Level: (low/med) LOW Date Received: 10/06/89
,
% Moisture: not dee.~ dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10/1:;j/89
GPC Cleanup: (Y/N) L_ pH: 8.1 Dilution Factor: 1,00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 360
lll-44-4--------bis(2-Chloroethyl)Ether 360
95-57-8---------2-Chlorophenol 360
541-73-1--------1,3-Dichlorobenzene 360
106-46-7--------1,4-Dichlorobenzene 360
100-51-6--------Benzyl Alcohol 360
95-50-1---------1,2-oichlorobenzene 360
95-48-7---------2-Methylphenol 360
39638-32-9------bis(2-Chloroisopropyl)Ether_ 360
106-44-5--------4-Methylphenol 360
621-64-7--------N-Nitroso-Di-n-Propylamine __ 360
67-72-1---------Hexachloroethane 360
98-95-3---------Nitrobenzene 360
78-59-1---------Isophorone 360
88-75-5---------2-Nitrophenol 360
105-67-9--------2,4-Dimethylphenol 360
65-85-o---------Benzoic Acid 1800
lll-91-l--------bi ■(2-Chloroethoxy)Methane __ 360
120-83-2--------2,4-Dichlorophenol 360
120-a2-1--------1,2,4-Trichlorobenzene 360
91-20-3---------Naphthalene 360
106-47-8--------4-Chloroaniline 360
87-68-3~--------Hexachlorobutadiene 360
59-50-7---------4-Chloro-3-Methylphenol 360
91-57-6---------2-Methylnaphthalene 360
77-47-4---------Hexachlorocyclopentadiene_ 360
88-06-2---------2,4,6-Trichlorophenol 360
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 360
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 360
208-96-8--------Acenaphthylene 360
606-20-2--------2,6-Dinitrotoluene 360
u
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Q
FORM I SV-l l/87 Rev.
::c:: fi!p..,-.. Si'fll'IM.£-ORXIJ SCllflllillltE 77
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lC
SEMIVOLATILE ORGANICS ANALYSIS.DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-32-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292754
Sample wt/vol: J0,Q (g/mL) !i..._ Lab File ID: GJ092754A04
Level: ( low/med) LOW Date Received: 10/06/89
\ Moisture: not dee. __9 dee. Date Extracted: 10/11/!!9
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) IL_ pH: 8.1
Date Analyzed: 10/15/89
Dilution Factor: 1.00
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene . 360
51-28-5---------2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------Dibenzoturan 360
121-14-2--------2,4-Dinitrotoluene 360
84-66-2---------Diethylphthalate 360
7005-72-3-------4-Chlorophenyl-phenylether_ 360
86-73-7---------Fluorene 360
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800
86-30-6---------N-Nitrosodiphenylamine (1)_ 360
101-55-3--------4-Bromophenyl-phenylether __ 360
118-74-1--------Hexachlorobenzene 360
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 360
120-12-1--------Anthracene 360
84-74-2---------Di-n-Butylphthalate 360
206-44-o--------Fluoranthene 360
129-00-0--------Pyrene 360
85-68-7---------Butylbenzylphthalate 360
91-94-1---------3,3'-Dichlorobenzidine 730
56-55~3---------Benzo(a)Anthracene 360
218-01-9--------Chryaene 360
117-81-7--------bia(Z-Ethylhexyl)Phthalate_ 360
117-84-0--------Di-n-Octyl Phthalate 360
205-99-2--------Benzo(b)Fluoranthene 360
207-08-9--------Benzo(k)Fluoranthene 360
50-32-8---------Benzo(a)Pyrene 360
193-39-5--------Indeno(l,2,3-cd)Pyrene 360
53-70-3---------Dibenzo(a,h)Anthracene 360
191-24-2--------Benzo(g,h,i)Perylene 360
(1) -CaMot be separated from Diphenylamine
Q
u u u u u u u u
u u u u u u u
u u u u u u u u
u u u u u u u u u
FORM I sv-2 . 1/87 Rev.
76
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS·DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-32-1
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: ,._90,.___
Matrix: (soil/water) SOIL Lab Sample ID: *2~9&2~7L541-__ _
Sample wt/vol: 30.0 (g/mL) L_
Level: (low/med) LOW
I Moisture: not dee. __i
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL..
Number TICS tound: ---1
dee.
pH:
CAS NUMBER COMPOUND
8,1
NAME
Lab File ID: GJ092754A04
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/15/89
Dilution Factor: 41-'-'1 0,._,o.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=•=•••==•==m••== --==================-====== ---====-•amma•====-=== =====
1. 2216-34-4 OCTANE, 4-METHYL-5.08 260 j
2. 17302-33-9 UNDECANE, 6-METHYL-· 5.17 180 j
3. ALDOL 6.03 480 A3
FORM I SV-TIC 1/87 Rev.
75
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1B . EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-33-1
Lab Name: COMPUCHEM LABS Contract: 12-88}-REVS
Lab code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292755
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GHQ92755A04
Level: (low/med) _LO_w~-Date Received: 10£'.0§£'.89
% Moisture: not dee.__]_ dee. ciate Extracted: 10£'.11£'.89
Extraction: (SepF/Cont/Sonc) ~
7,6
Date Analyzed: 10£'.15£'.89
GPC Cleanup: (Y/N) H...._ pH: Dilution Factor: .l.~·~O~O __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG
108-95-2-------~Phenol 350
lll-44-4--------bis(2-Chloroethyl)Ether 350
95-57-8---------2-Chlorophenol 350
541-73-1--------1, 3-Dichlorobenzene· 350
106-46-7--------1,4-Dichlorobenzene 350
100-51-6--------Benzyl Alcohol 350
95-50-1---------1,2-Dichlorobenzene 350
95-48-7---------2-Methylphonol 350
39638-32-9------bis(2-Chloroisopropyl)Ether_ 350
106-44-5--------4-Methylphenol 350
621-64-7--------N-Nitroso-Di-n-Propylamine __ 350
67-72-1---------Hexachloroothane 350
98-95-3---------Nitrobenzene 350
78-59-1---------Iaophorone 350
88-75-5---------2-Nitrophenol 350
105-67-9--------2,4-Dimethylphenol 350
65-85-o---------Benzoic Acid 1700
lll-91-l--------bia(2-Chloroethoxy)Methane_ 350
120-83-2--------2,4-Dichlorophenol 350
120-a2-1--------l,2,4-Trichlorobenzene 350
91-20-3---------Naphthalene 350
106-47-8--------4-Cbloroaniline 350
87-68-3---------Hexachlorobutadiene 350
59-50-7---------4-Cbloro-3-Methylphenol 350
91-57-6---------2-Methylnaphthalene 350
77-47-4---------Hexachlorocyclopentadiene __ 350
88-06-2---------2,4,6-Trichlorophenol 350
95-95-4---------2,4,5-Trichlorophenol 1700
91-58-7---------2-Chloronaphthalene 350
88-74-4---------2-Nitroaniline 1700
131-11-3--------Dimethyl Phthalate 350
208-96-8--------Acenaphthylene 350
606-20-2--------2,6-Dinitrotoluene 350 .
Q
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u
u·
u
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u
u u
u
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u
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u u
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u u u
u
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u
FORM I sv-1 1/87 Rev.
74
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM IABS contract: 12-BQl-REVS SL-33-1
Lab Code: coMPU case No.: 17902 SAS No.: SOG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292755
sample wt/vol: 30.0 (g/mL) L_ Lab File IO: GH092755A04
Level: ( low/med) LOW Date Received: 10/06/89
\ Moisture: not dee. ___J_ dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) ~
7.6
Date Analyzed: 10/15/89
GPC Cleanup: (Y/N) L.. pH:
• COMPOUND
Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. (ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700 u
83-32-9---------Acenaphthene 350 u
51-28-5---------2,4-Dinitrophenol 1700 u
100-02-7--------4-Nitrophenol 1700 u
132-64-9--------Dibenzofuran 350 u
121-1·4-2--------2, 4-Dinitrotoluene 350 u
84-66-2---~-----Diethylphthalate 350 u
7005-72-3-------4-Chlorophenyl-phenylether_ 350 u
86-73-7---------Fluorene 350 u
100-01-6--------4-Nitroaniline 1700 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1700 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 350 u
101-55-3--------4-Bromophenyl-phenylether __ 350 u
118-74-1--------Hexachlorobenzene 350 u
87-86-5---------Pentachlorophenol 1700 u
85-01-8---------Phenanthrene 350 u
120-12-1--------Anthracene 350 u
84-74-2---------Di-n-Butylphthalate 350 u
206-44-0--------Fluoranthene 350 u
129-oo-o--------Pyren• 350 u
85-68-7---------Butylbenzylphthalate 350 u
91-94-1---------3,3'-0ichlorobenzidine 710 u
56-55-3---------Benzo(a)Anthracene 350 u
218-01-9--------Chryaene 350 u
ll7-Bl-7--------bia(2-Ethylhexyl)Phthalate_ 350 u
117-84-o--------oi-n-octyl Phthalate 350 u
205-99-2--------Benzo(b)Fluoranthene 350 u
207-08-9--------Benzo(k)Fluoranthene 350 u
50-32-8---------Benzo(a)Pyren• 350 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 350 u
53-70-3----~----Dibenzo(a,h)Anthracene 350 u
191-24-2--------Benzo(g,h,i)Perylene 350 u
(l) -cannot be separated from Diphenylamine
Q
FORM I sv-2 1/87 Rev.
7:J
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lF
SEMIVOLATILE ORGANICS ANALYSIS. DATA SHEET.
EPA SAMPLE NO.
TENTATIVELY IDENTIFIED COMPOUNDS
SL-33-1
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292755
Sample wt/vol: 30,0 (g/mL) ~ Lab File ID: GH092755A04
Level: (low/med) LOW Date Received: 10/06/89
' Moisture: not dee. __J_ dee. Date Extracted: 10/11/!19
Extraction: (SepF/Cont/Sonc) S.OW: Date Analyzed: 10/15/!19
GPC Cleanup: (Y/N) H...._ pH: 7.6 Dilution Factor: 1.00
CONCENTRATION UNITS:
Number TICs found: ___l (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
~---=======••=----=-==---===----=--=-===----====:c=== ==-=========== •====
l. 2216-34-4 OCTANE, 4-METHYL-5.08 210 J
FORM I SV-TIC 1/87 Rev.
. Sl/ll!lff..E. ORTR-JSl.ii.UtMMllii~a::IE..;... ----72
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1B
SEMIVOLATILE ORGANICS ANALYSIS 'DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: f2-88l-REVS
SL-34-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292756
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GHQ92756A04
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. _lJ2 dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: lOIU/89
GPC Cleanup: (Y/N) L. pH: 8.5 Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------l,3-Dichlorobenzene 370 u
106-46-7--------l,4-Dichlorobenzene '370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane :370 u
98-95-3---------Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-o---------Benzoic Acid 1800 u
lll-9l-1--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-82-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--------2,6-Dinitrotoluene 370 u
FORM I sv-1 l/87 Rev.
71
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-34-1
Lab Name: COMPUCHEM LABS contract: 12-88)-REVS
Lab Code: COMPU case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292756
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH092756A04
Level: ( low/med) .. LQ,..,W,__ Date Received: 10/06/89
\ Moisture: not dee. _l.Q dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc)
(Y/N) l:l,_
~
8.5
Date Analyzed: 10/14/!!9
GPC Cleanup: pH: Dilution Factor: .1~,~0~0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9----~----Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-7--------4-Nitrophenol 1800
132-64-9--------Dibenzoturan 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800
86-30-6---------N-Nitrosodiphenylamine (l)_ 370
101-55-3--------4-Bromophenyl-phenylether __ . 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------oi-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-oo-o--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1---------3,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene . 370
ll7-8l-7--------bia(2-Ethylhexyl)Phthalate_ 370
111-a,-o--------oi-n-octyl Phthalate 370
205-99-2~~------Benzo(b)Fluoranthene 370
207-08-~--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 370 .
(1) -CaMot be separated trom Diphenylamine
Q
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FORM I sv-2 1/87 Rev.
. . Ii • 4 •PL.6 DRTR Sl.!MIWM'V-78
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM LABS contract: (2-881-REVS
Lab Code: COMPO Case No.: 17902 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample IO:
SL-34-1
No.: 90
292756
Sample wt/vol: 30.0 (g/mL) L-Lab File IO: GH092756A04
· Level: ( low/med) • LOW
I Moisture: not dee. _ll
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H.,_
Number TICs tound: --2
dee •. __
~
pH: 8.5
CAS NUMBER COMPOUND NAME
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/14/89
Dilution Factor: al~,~00"-_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
----------=------••••••••==-==•===••s•••••-== -----==-=-----------=-----==-1.
2.
3.
4.
5.
BLANlC CONTAMINANT 5.13 300
BLANK CONTAMINANT 5.23 220
ALOOL 6.07 220
UNKNOWN 17.04 960
UNKNOWN 21.80 1000
FORM I SV-TIC
-'--=------.=--.~;l!9•1~2~--' SRllfl'LE. DRTR--.SS~C.MWM•is►IIE------=:-.
t
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BJ
AJ
J
J
1/87 Rev.
69
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
SL-35-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab sample IO: 292757
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH092757A04
Level: ( low/med) LOW Date Received: 10/06/89
I Moisture: not dee. --li dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) S.QliC Date Analyzed: 10/14/89
GPC Cleanup: (Y/N) IL_ pH: 7.9 Dilution Factor: .1~·=0~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis ( 2-Chloroethyl) Eth.er 370 u
95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---~-----l,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3--------~Nitrobenzene 370 u
78-59-1---------Isophorone . 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2 ,. 4-Dimethylphenol 370 u
65-85-o---------Benzoic'Acid 1800 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-02-1--------1,2,4-Trichlorobenzene 370 u
91-20-3---------Naphthalene 370 u
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene_ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------oimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2·--------2; 6-Dinitrotoluen• 370 u
FORM I sv-1 1/87 Rev.
68
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA· SAMPLE NO.
Lab Name: COMPUCHP:M LABS Contract: 12-88}-REVS
SL-35-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292757
sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH092757A04
Level: (low/med) LOW Date Received: 10/06/89
\ Moisture: not dee. _..l.l dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/U/!!9
GPC Cleanup: (Y/N) Ji_ pH: 7,9 Dilution Factor: 1,00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32-9------~--Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-1--------4-Nitrophenol 1800 u
132-64-9--------Dibenzoturan 370 u
121-14-2--------2,4-Dinitrotoluene 370 u
84-66-2---------Diethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether_ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1800 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 370 u
101-55-3--------4-Bromophenyl-phenylether_ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 370 u
120-12-1--------Anthracene 370 u
84-74~2---------01-n-Butylphthalate 370 u
206-44-o--------Fluoranthene 370 u
129-00-0--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-Dichlorobenzidine 740 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9--------Chryaene 370 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 370 u
117-84-o--------Di-n-octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -CaMot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
---.... _. +-:t?'-=---SR:IIPLE ORTR-St" Mir , ----67
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lF SEMIVOLATILE ORGANICS ANALYSIS.DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM LABS Contract: 12-881-REVS
EPA SAMPLE NO.
SL-35-l
Lab code: COMPU Case No.: 17902 SAS No.: SOG NO.: 90
Matrix: (soil/water) SOIL
sample wt/vol: 30,0 (g/mL) L._
Level: (low/med) LOW
t Moisture: not dee. _ll
Extraction:
GPC Cleanup:
(SapF/Cont/Sonc)
(Y/N) ti_
Number TICs tound: --2.
dee.
pH:
CAS NUMBER COMPOUND
7.9
NAME
Lab Sample ID: 292757
Lab File ID: GH092757,',04
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/14/89
Dilution Factor: ~1~,0~0.__
CONCENTRATION UNITS:
.(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ======•=====•m=• •========-=-============•=== ==xi:=====-•============-:a==== 1. BLANK CONTAMINANT s.10 300 BJ 2. BLANK CONTAMINANT 5.18 190 BJ
FORM I SV-TIC 1/87 Rev.
66
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18
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88}-REYS
SL-36-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292758
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH092758A04
Level: (low/med) LQW Date Received: 10/06/89
% Moisture: not dee. _ll dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) S.QH,C Date Analyzed: 10/U/!19
GPC Cleanup: (Y/N) H.._ pH: 7,7 Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 390 u
lll-44-4--------bis(2-Chloroethyl)Ether 390 u
95-57-8---------2-Chlorophenol 390 u
541-73~1--------1,J-Dichlorobenzene 390 u
106-46-7--------1,4-Dichlorobenzene 390 u
100-s1-6--------Benzyl Alcohol 390 u
95-50-1---------1,2-0ichlorobenzene 390 u
95-48-7---------2-Methylphenol 390 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 390 u
106-44-5--------4-Methylphenol 390 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 390 u
67-72-1---------Hexachloroethane 390 u
98-95-3---------Nitrobenzene 390 u
78-59-1---------Isophorone 390 u
88-75-5---------2-Nitrophenol 390 u
105-67-9--------2,4-0imethylphenol 390 u
65-as-o---------Benzoic Acid 1900 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 390 u
120-83-2--------2,4-0ichlorophenol 390 u
120-a2-1--------1,2,4-Trichlorobenzene 390 u
91-20-3---------Naphthalene 390 u
106-47-8--------4-Chloroaniline 390 u
87-68-3---------Hexachlorobutadiene · 390 u
59-50-7---------4-Chloro-3-Methylphenol 390 u
91-57-6---------2-Methylnaphthalene 390 u
77-47-4---------Hexachlorocyclopentadiene __ 390 u
88-06-2---------2,4,6-Trichlorophenol 390 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
91-58-7---------2-Chloronaphthalene 390 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalate 390 u
' 208-96-8--------Acenaphthylene 390 u
606-20-2--------2,6-Dinitrotoluene 390 u
FORM I·SV-1 1/87 Rev.
65
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.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS Contract: 12-BBl-REVS
SL-36-1
Lab Code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292758
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID: GH092758A04
Level: (low/med) LOW Date Received: 10/06/89
% Moisture: not dee. ~ dee. Date Extracted: 10,:'.ll,:'.89
Extraction: (SepF/Cont/Sonc) ~
7,7
Date Analyzed: 10,:'.14,:'.89
Dilution Factor: AlL,~oo.,__ GPC Cleanup: (Y/N) lL_ pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1900
83-32-9---------Acenaphthene 390
51-28-5---------2,4-Dinitrophenol 1900
100-02-1--------4-Nitrophenol 1900
132-64-9--------Dibenzoturan 390
121-14-2------~-2,4-Dinitrotoluene 390
84-66-2---------Diethylphthalate 390
7005-72-3-------4-Chlorophenyl-phenylether_ 390
86-73-7---------Fluorene 390
100-01-6--------4-Nitroaniline 1900
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1900
86-30-6---------N-Nitrosodiphenylamine (1)_ 390
101-55-3--------4-Bromophenyl-phenylether __ 390
118-74-1--------Hexachlorobenzene 390
87-86-5---------Pentachlorophenol 1900
85-01-8---------Phenanthrene 390
120-12-1--------Anthracene 390
84-74-2---------Di-n-Butylphthalate 390
206-44-0--------Fluoranthene 390
129-oo-o--------Pyrene 390
85-68-7---------Butylbenzylphthalate 390
91-94-1---------3,J'-Dichlorobenzidine 780
56-55-3--~------Benzo(a)Anthracene 390
218-01-9--------Chry■ene 390
117-81-7--------bi■(2-Ethylhexyl)Phthalate_ 390
117-84-o--~-----Di-n-Octyl Phthalate 390
205-99-2--------Benzo(b)Fluoranthene 390
207-08-9--------Benzo(k)Fluoranthene 390
50-32~8---------Benzo(a)Pyrene 390
193-39-5--------Indeno(l,2,3-cd)Pyrene 390
53-70-3---------Dibflnzo(a,h)Anthracene 390
191-24-2--------Benzo(g,h,i)Perylene 390
(1) -CaMot be separated trom Diphenylamine
Q
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u u u u u u u
u u u u u
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1/87 Rev.
~-17:PI/IZ'-fl#T.~£ DRTR-SUIUUl.et'--
-.. . ., . . . . .~. . 64
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. lF EPA SAMPU NO. SEMIVOLATILE ORGANICS ANALYSI~ DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SL-36-1
Lab Name: COMPUCHEM I.ABS Contract: 12-BBI-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .,,_9.,._0 __
Matrix: (soil/water) SOIL Lab Sample ID: .._2.ii..9..._27.,_5.,_,s.__ __ _
Sample wt/vol: 30,0 (g/mL) L_
Level: ( low/med) LOW
\ Moisture: not dee.~ dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H_ pH: 7,7
Number TICs found: _J.
CAS NUMBER COMPOUND NAME
Lab' File ID: GH092758A04
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10/14/89
Dilution Factor: .iL,o~o"--
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/KG
RT EST. CONC. Q
==•=a==========• ==--==----=--------~=-------=--==-==== =============-•====
1, ALDOL 6.07 940 AJ
FORM I SV-TIC 1/87 Rev
6J
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.I.D
SEMIVOLATILE ORGANICS ANALYSIS·. DATA SHEET "->'A :OAl'l,'LJ:; NO.
Lab Name: CQMPUCHEM LABS Contract: 12-BB)-REVS
SL-37-1
Lab Code: CQMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292759
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GHQ92759A04
Level: (low/med) LOW Date Received: 10/06/89
\ Moisture: not dee. ___i dee. Date Extracted: lQ/ll/89
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li.,_ pH:
som=
6.9
Date, Analyzed: 10/14/89
Dilution Factor: l,OO
CONCENTRATION.UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 360 u
lll-44-4--------bis(2-Chloroethyl)Ether 360 u
95-57-8---------2-Chlorophenol 360 u
541-73-1--------1,3-Dichlorobenzene 360 u
106-46-7--------1,4-Dichlorobenzene 360 u
100-51-6--------Benzyl Alcohol 360 u
95-50-1---------1,2-Dichlorobenzene 360 u
95-48-7---------2-Methylphenol 360 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 360 u
106-44-5--------4-Methylphenol 360 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 360 u
67-72-1---------Hexachloroethane 360 u
98-95-3---------Nitrobenzene 360 u
78-59-1---------Isophorone 360 u
88-75-5---------2-Nitrophenol 360 u
105-67-9--------2,4-Dimethylphenol 360 u
65-85-0---------Benzoic Acid 1700 u
111-91-1--------bis(2-Chloroethoxy)Methane_ 360 u
120-83-2--------2,4-Dichlorophenol 360 u
120-a2-1--------1,2,4-Trichlorobenzene 360 u
91-20-3---------Naphthalene 360 u
106-47-8--------4-Chloroaniline 360 u
87-68~3-----~---Hexachlorobutadiene 360 u
59-50-7~--~-----4-Chloro-3-Methylphenol 360 u
91-57-6---------2-Methylnaphthalene 360 u
77-47-4---------Hexacblorocyclopentadiene_ 360 u
88-06-2---------2,4,6-Trichlorophenol 360 u
95-95-4---------2,4,5-Trichlorophenol 1700 u
91-58-7---------2-Chloronaphthalene 360 u
88-74-4---------2-Nitroaniline 1700 u
131-11-3--------Dimethyl Phthalate 360 u
208-96-8--------Acenaphthylene 360 u
606-20-2----~---2,6-Dinitrotoluene 360 u
FORM I sv-1 1/87 Rev.
= . 1f?S 15 -Pfr SIIIIRt. E-OR TR-SlW .. 1-'C 62
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SEMIVOLATILE ORGANICS ANALYSIS·· DATA SHEET EPA SAMPLE NO ..
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
SL-37-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
. Matrix: (soil/water) SOIL Lab Sample ID: 292759
sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH092759A04
Level: (low/med) LOW Date Received: 10/06/89
t Moisture: not dee. _...i dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: .J.QiUl89
GPC Cleanup: (Y/N) li_ pH: 6,9 Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700
83-32-9---------Acenaphthene 360
51-28-5---------2,4-Dinitrophenol 1700
100-02-1--------4-Nitrophenol 1700
132-64-9--------Dibenzo!uran 360
121-14-2--------2,4-Dinitrotoluene 360
84-66-2---------Diethylphthalate 360
7005-72-3-------4-Chlorophenyl-phenylether_ 360
86-73-7---------Fluorene 360
100-01-6--------4-Nitroaniline 1700
534-52-1---.-----4, 6-Dinitro-2-Methylphenol_ 1700
86-30-6---------N-Nitrosodiphenylamine (l)_ 360
lOl-55-3---~~-~-4-Bromophenyl-phenylether __ 360
118-74-.l--------Hexachlorobenzene 360
87-86-5---------Pentachlorophenol 1700
es-01-e---------Phenanthrene 360
120-12-1--------Anthracene 360
84-74-2~--------Di-n-Butylphthalate j6o
206-44-o--------Fluoranthene 360
129-oo-o--------Pyrene 360
85-68-7---------Butylbenzylphthalate 360
91-94-1---------3,3'-Dichlorobenzidine 720
56-55-3---------Benzo(a)Anthracene 360
218-01-9--------Chry■ene 360
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 360
111-a,-o--------Di-n-octyl Phthalate 360
205-99-2~-------Ben:i:o(b)Fluoranthene 360
207-08-9--------Benzo(k)Fluoranthene 360
50-32-8---------Benzo(a)Pyrene 360
193-39-5--------Indeno(l,2,3-cd)Pyrene 360
53-70-3---------Dibenzo(a,h)Anthracene 360
191-24-2--------Benzo(g,h,i)Perylene 360
(l) -CaMot be separated from Diphenylamine
u u u
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Q'
FORM I sv-2 l/87 Rev.
61
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---·-lF SEMIVOLATILE ORGANICS ANALYSIS' DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SL-37-1 Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS
Lab Code : COMPU Case No.: 17902 SAS No.: SDG No.: 90 Matrix: (soil/water) SOIL Lab sample ID: 292759 Sample wt/vol: · 30,0 (g/mL) L-Lab File ID: GH092759A04
Level: (low/med) _rp,...w.,___ Date Received: 10/06/89
% Moisture: not dee. _.J. dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) SQHl: Date·Analyzed: 10/14/89
GPC Cleanup: (Y/N) L pH: 6.9 Dilution Factor: _14,0~0.___
CONCENTRATION UNITS: Number TICs tound: --3. (ug/L or ug/~g) UG/KG
CAS NUMBER COMPOUND NAME RT EST, CONC. Q ============a=-=rm ===~===--=--=--~--=-==--== a.:111:az:=s== -=;g:a=:======= ===== 1, BLANK CONTAMINANT 5.08 250 BJ 2, BLANl< CONTAMINANT 5.17 180 BJ 3. ALDOL 6,02 1100 AJ
FORM I SV-TIC 1/87 Rev.
68 --WWW
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18 EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SL-26-lMS
Lab Name: COMPUCHEM LABS Contract: C2-88l-REVS
Lab Code: COMPU Case No. : 17902 SAS No.: SDG No.: ,.9.,.0 __
Matrix: (soil/water) SOIL Lab Sample ID: _..2..z.9..._2,,.3...:24:,_ __ _
sample wt/vol: 30.0 (g/mL) ~ Lab File ID: G2R92324B06
Level: ( low/med) LOW Date Received: 10/05/89
\ Moisture: not. dee. ---2]_ dee. Date-Extracted: 10/24/89
Date Analyzed: 11/01/89 Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H...._ pH: 6.4 Dilution Factor: .1~1.,.0.,.0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
1oa_.9s-2--------Pheno1· 430 u
lll-44-4--------bis(2-Chloroethyl)Ether 430 u
95-57-8---------2-Chlorophenol 430 u
541-73-1--------1,3-Dichlorobenzene 430 u
106-46-7--------1,4-Dichlorobenzene 430 u
·100-51-6--------Benzyl Alcohol 430 u
95•50-1---------1,2-Dichlorobenzene 430 u
95-48-7---------2-Methylphenol 430 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 430 u
106-44-5--------4-Methylphenol 430 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 430 u
67-72-1----------Hexachloroethane 430 u
98-95-3----------Nitrobenzene 430 u
78-59-1---------Isophorone 430 u
88-75-5---------2-Nitrophenol 430 u
105-67-9--------2,4-Dimethylphenol 430 u
65-85-o---------Benzoic Acid 2100 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 430 u
120-e3-2--------2,4-Dichlorophenol 430 u
120-e2-1--------1,2,4-Trichlorobenzene 430 u
91-20-3---------Naphthalone 430 u
106-47-8--------4-Chloroaniline 430 u
87-68-3---------Hexachlorobutadiene 430 u
59-50-7---------4-Chloro-3-Methylphenol 430 u
91-57-6---------2-Methylnaphthalene 430 u
77-47-4---------Hexachlorocyclopentadiene __ 430 u
88-06-2---------2,4,6-Trichlorophenol 430 u
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalene 430 u
88-74-4---------2-Nitroaniline 2100 u
131-11-3--------Dimethyl Phthalate 430 u
208-96-8--------Acenaphthylene 430 u
606-20-2--------2,6-Dinitrotoluene 430 u
FORM I sv-1 1/87 Rev.
::::...:.:.... --=: · ·-.:~-~.JZP Ji··--·SRIUPLE DRTR SUJIWV .. · ------
t
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-881-REVS
SL-26-lMS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: ( soil/water) SOIL Lab Sample ID: 292324
·Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: G2R92324B06
Level: (low/med) LOW Date Received: 10/05/89
% Moisture: not dee. -2..3. dee. Date Extracted: 10/24/89
Extraction: (SepF/Cont/Sonc) Date Analyzed: 11(91/89
GPC Cleanup: (Y/N) li.._ pH: 6,4 Dilution Factor: .1L,o~o.__
CONCENTRATION UNITS:.
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG . Q
99-09-2---------3-Nitroaniline 2100 u
83-32-9---------Acenaphthene 430 u
51-28-5---------2,4-Dinitrophenol 2100 u
100-02-1--------4-Nitrophenol 2100 u
132-64-9--------Dibenzoturan 430 u
121-14-2--------2,4-Dinitrotoluene 430 u
84-66-2---------Diethylphthalate 430 u
7005-72-3-------4-Chlorophenyl-phenylether_ 430 u
86-73-7---------Fluoreno 430 u
100-01-6--------4-Nitroaniline 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2100 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 430 u
lOl-55-3--------4-Bromophenyl-phenylether __ 430 u
118-74-1--------Hexachlorobenzene 430 u
87-86-5---------Pentachlorophenol 2100 u
as-01-s---------Phenanthrene 430 u
120-12-1--------Anthracene 430 u
84-74-2---------Di-n-Butylphthalate 430 u
206-44-0--------Fluoranthene 430 u
129-00-o--------Pyrene 430 u
85-68-7---------Butylbenzylphthalate 430 u
91-94-1---------3,3'-Dichlorobenzidine 860 u
56-55-3---------Benzo(a)Anthracene 430 u
218-01-9--------Chrysene 430 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 99 J
117-84-0--------Di-n-octyl Phthalate 430 u
205-99-2--------Benzo(b)Fluoranthene 430 u
207-08-9--------Benzo(k)Fluoranthene 430 u
50-32-8---------Benzo(a)Pyrene 430 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 430 u
53-70-3---------Dibenzo(a,h)Anthracene 430 u
191-24-2--------Benzo(g,h,i)Perylene 430 u
-
(l) -cannot be separated from Diphenylamine
FORM I SV-2 l/87 Rev
···------·--------'---58
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET . EPA SAMPLE NO.
Lab Name: CQMPUCHEM LABS
SL-26-lMSD
Contract: C2~88l-REVS
Lab code: CQMPU Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab Sample ID: 292325
sample wt/vol: 30,0 (g/mL) L_ Lab File ID: G2R92325C06
Level: ( low/med) LOW Date Received: 10/05/89
\ Moisture: not dee. _u dee. Date Extracted: 10/24/89
Extraction: Date Analyzed: 11/01/89
GPC Cleanup:
(SepF/Cont/Sonc)
('i/N) li.._ pH: 6,4 Dilution Factor: 1,00
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 430
lll-44-4--------bis(2-Chloroethyl)Ether 430
95-57-8---------2-Chlorophenol 430
541-73-1----.----l, 3-Dichlorobenzene 430
106-46-7--------l,4-Dichlorobenzene 430
100-51-6--------Benzyl.Alcohol 430
95-50-1---------l,2-Dichlorobenzene 430
95-48-7---------2-Methylphenol 430
39638-32-9------bis(2-Chloroisopropyl)Ether_ 430
106-44-5--------4-Methylphenol 430
· 621-64-7--------N-Nitroso-Di-n-Propylamine_ 430
67-72-1---------Hexachloroethane 430
98-95-3---------Nitrobenzene 430
7 8-59-1------·---I ■ophorone 430_
88-75-5---------2-Nitrophenol 430
105-67-9--------2,4-Dimethylphenol 430
65-85-o---------eenzoic Acid 2100
lll-91-1--------bis(2-Chloroethoxy)Methane_ 430
120-83-2--------2,4-0ichlorophenol 430
120-s2-1--------1,2,4-Trichlorobenzene
. 430
91-20-3---------Naphthalane 430
106-47-8--------4-Chloroaniline 430
87-68-3---~-----Hexachlorobutadiene 430
59-50-7---------4-Chloro-3-Methylphenol 430
91-57-6---------2-Methylnaphthalene 430
77-47-4---------Hexachlorocyclopentadiene __ 430
88-06-2---------2,4,6-Trichlorophenol 430
95-95-4----~----2,4,5-Trichlorophenol 2100
91-58-7---------2-Chloronaphthalene 430
88-74-4---------2-Nitroaniline 2100
131-11-3--------Dimethyl Phthalate 430
208-96-8--------Acenaphthylene 430
606-20-2--------2,6-Dinitrotoluene 430
Q
u
u u
u
u
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u u
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u u
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u
u
FORM I sv-1 l/87 Rev.
--. ==:r;::::,=:--'75tQ,.' 5l'a SRJIIPLE DRTR SUlfllllUflF 57
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM LABS Contract: 12-88)-REVS SL-26-lMSO
· . Lab code: COMPO Case No.: 17902 SAS No.: SDG No.: 90
Matrix: (soil/water) SOIL Lab sample ID: 292325
sample wt/vol: 30.0 (g/mL) ~ Lab File IO: G2R92325C06
Level: ( low/med) LOW Date Received: 10,:'.Q5<'.'.ll9
% Moisture: not dee. _n dee. Date Extracted: 10,:'.24,:'.89
Date Analyzed: 11,:'.0l,:'.89 Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) L.. pH: 6,4 Dilution Factor: .1~.o~o..__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2100 u
83-32-9---------Acenaphthene 430 u
51-28-5---------2,4-Dinitrophenol 2100 u
100-02-1--------4-Nitrophenol 2100 u
132-64-9--------Dibenzofuran 430 u
121-14-2--------2,4-Dinitrotoluene 430 u
84-66-2---------Diethylphthaiate 430 u
7005-72-3-------4-Chlorophenyl-phenylether_ 430 u
86-73-7---------Fluorene 430 u
100-01-6--------4-Nitroaniline 2100 u
534-52-1----.----4, 6-Dinitro-2-Methylphenol_ 2100 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 430 u
101-55-3--------4-Bromophenyl-phenylether_ 430 u
118-74-1-~------Hexachlorobenzene 430 u
87-86-5---------Pentachlorophenol 2100 u
85-01-8---------Phenanthrene 430 u
120-12-1--------Anthracene 430. u
84-74-2---------Di-n-Butylphthalate 430 u
206-44-0--------Fluoranthene 430 u
129-00-0--------Pyrene 430 u
85-68-7---------Butylbenzylphthalate 430 u
91-94-1---------3,3'-Diehlorobenzidine 860 u
56-55-3---------Benzo(a)Anthracene 430 u
218-01-9--------Chryaene 430 u
ll7-81-7--------bia(2-Ethylhaxyl)Phthalate_ 48 j
111-a,-o--------oi-n-oetyl Phthalate 430 u
205-99-2--------Benzo(b)Fluoranthene 430 u
207-08-9--------Benzo(k)Fluoranthene 430 u
50-32-8---------Benzo(a)Pyrene 430 u
193-39-5--------Indeno(l,2,3-ed)Pyrene 430 u
53-70-3---------Dibenzo(a,h)Anthracene 430 u
191-24-2--------Benzo(g,h,i)Perylene 430 u
(l) -CaMot be separated from Diphenylamine
FORM I sv-2 l/87 Rev.
56
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-26-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No, : ,,_9.,._0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ,,_2L9,,_23"'2"'3,___ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) L-.
Level: (low/med) LOW
% Moisture: not dee. 2,._,3.___ dee.
Date Received: 10 /05 /89
Date Extracted: 10/06/89
Date Ana~yzed: 10(12(89 Extraction: (SepF/Cont/Sonc) SOfil:.
GPC Cleanup: (Y/N) li,__ pH:__§_,_! Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I 319-84-6--------alpha-BHC. _________ I 10. U
319-85-7--------beta-BHC I 10. U
319-86-8--------delta-BHC I 10. U
58-89-9---------gaJll!!la-BHC (Lindane) I 10, U
76-44-8---------Heptachlor I 10. U
309-00-2--------Aldrin I 10. U
1024-57-3-------Heptachlor epoxide I 10. U
959-98-8--------Endosulfan I I 10. U
60-57-1---------Dieldrin I 21. U
72-55-9---------4,4'-DDE I 21. U
72-20-8---------Endrin I 21. U
33213-65-9------Endosulfan II I 21. U
72-54-8---------4,4'-DDD I 21. U
1031-07-8-------Endosulfan sulfate I 21. U
50-29-3---------4,4'-DDT I 21. U
72-43-5---------Methoxychlor________ 100 u
53494-70-5------Endrin ketone 21. U -------5103-71-9-------alpha-Chlordane,______ 100 IU
5103-74-2-------gamma-Chlordane,______ 100 IU
8001-35-2-------Toxaphene 210 1u 12674-11-2------Aroclor-l""O,..l,...6_______ 100 I U
11104-28-2------Aroclor-1221_______ 100 IU
11141-16-5------Aroclor-1232_______ 100 IU
53469-21-9------Aroclor-1242________ 100 iU
12672-29-6------Aroclor-1248_______ 100 IU
11097-69-1------Aroclor-1254________ 210 iU
0
11096-82-5------Aroclor-1260_______ 210 iU
-----------------------------1--
f'ditl 191EST i/874Rev.
-:,; 55
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-27-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : _._9.,._0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: .,,_2.._9.,_2,._33 ... 3.,__ __
Lab File ID: Sample wt/vol: 30.0 (g/mL) L-
Level: (low/med) LOW
% Moisture: not dee. a5~4 __ dee.
Date Received: 10/05/89
Date Extracted: 10/06/89
Date Analyzed: 10/12/89 Extraction: (SepF/Cont/Sonc) SQlli:.
GPC Cleanup: (Y/N) Ii_ pH: _.Ll Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC 319-86-8--------delta-BHC _________ _
58-89-9---------gamma-BHC (Lindane) ___ _
76-44~8---------Heptachlor ________ _
309-00-2--------Aldrin~---~.,.------1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin _________ _
72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin 33213-65-9------Endosu.~l~f-a_n_II=--------
72-54-8---------4,4'-DDD 1031-07-8-------Endosulf_a_n_s_u_l~f~a-t_e ____ _
50-29-3---------4,4'-DDT~---------72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ________ _
12674-11-2------Aroclor-1016 _______ _
11104-28-2------Aroclor-1221 ______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 ______ _
11096-82-5------Aroclor-1260 ______ _
~ POD i P!ST
17.
17.
17.
17.
17.
17.
17.
17.
35.
35.
35.
35.
35.
35.
35.
170
35.
170
170
350
170
170
170
170
170
350
350
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ij97 ~ev.
-==:___:--:-_ ·-: ·:::--~ ?:-S;;"" ~~7~el2!.... M -SRRPL E DR TR SU/flUIII.Y --'----. --'--
t ---·--·
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I
10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-31-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: -9,._0 ___ _
Matrix: (soil/water) SOIL Lab Sample ID: -29~2~7~5.,.3 __ _
Sample wt/vol: 30.0 (g/mL) ~
LOW
Lab File IO:
Level: (low/med)
% Moisture: not dee. -'8.___ dee.
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analyzed: 10(13/89 Extraction: (SepF/Cont/Sonc) SQ:K
GPC Cleanup: (Y/N) :tL__ pH: _L_l Dilution Factor: l. 00
CAS NO. . COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I I
319-84-6--------alpha-BHC _________ I 8.7 iU
319-85-7--------beta-BHC I 8.7 IU
319-86-8--------delta-BHC I 8.7 1u
58-89-9---------gamma-BHC (Lindanel I 8.7 1u
76-44-8---~-----Heptachlor I 8.7 IU
309-00-2--------Aldrin I 8.7 !U
1024-57-3-------Heptachlor epoxide I 8.7 IU
959-98-8--------Endosulfan I I 8.7 U
60-57-1---------Dieldrin · I 17. U
72-55-9---------4,4'-DDE I 17. U
72-20-8---------Endrin I 17. U
33213-65-9------Endosulfan II I 17. U
72-54-8---------4,4'-DDD I 17. U
1031-07-8-------Endosulfan sulfate_____ 17. U
50-29-3---------4,4'-D~---------17. U
72-43-5---------Methoxychlor_______ 87. U
53494-70-5------Endrin ketone_______ 17. u
5103-71-9-------alpha-Chlordane______ 87. U
5103-74-2-------ganuna-Chlordane______ 87. U
8001-35-2-------Toxaphene . .,,..,..,,________ 170 U
12674-11-2------Aroclor-1016 87. U
11104-28-2----~-Aroclor-1221_______ 87. U
11141-16-5------Aroclor-1232_______ 87. IU
53469-21-9------Aroclor-1242_______ 87. IU
12672-29-6------Aroclor-1248_______ 87. IU
11097-69-1------Aroclor-1254_______ 170 IU
11096-82-5------Aroclor-1260_______ 170 IU
0
-----------------------....,.....--,1----,-, ················ _, ....
POIOI 1 PEST 1/871.ev.
53
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-32-1
Lab Name1 COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lrab Code: COMPU Case No.: 17902 SAS No.: SDG No. : .._9.,.0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: 292754
Sample wt/vol1 30.0 ( g/mL) (L__ Lab File ID:
Level: (low/med) LOW Date Received: 10 /06 /89
% Moisture: not dee. 9 dee. Date Extracted: 10/11/89
Extraction: (SepF/Cont/Sonc) SoliC. Date Analyzed: 10/13/89
GPC Cleanup: (Y/N) li._ pH: -8......l Dilution Factor:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
I
319-84-6--------alpha-BHC _________ I
319-85-7--------beta-BHC I
319-86-8--------delta-BHC I
58-89-9---------gamma-BHC (Lindane) I
76-44-8---------Heptachlor I
309-00~2--------Aldrin I
1024-57-3-------Heptachlor epoxide I
959-98-8--------Endosulfan I _______ _
60-57-l---------Dieldrin. ___ ~------
72-55-9---------4,4'-DDE, _________ _
72-20-8---------Endrin. __________ _
33213-65-9------Endosulfan II. ______ _
72-54-8---------4,4'-DDD, _________ _
1031-07-8-------Endosulfan sulfate, ____ _
50-29-3---------4,4'-DOT _________ _
72-43-5---------Methoxychlor. _______ _
53494-70-5------Endrin ketone, ______ _
5103-71-9-------alpha-Chlordane. _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene. ________ _
12674-11-2---.---Aroclor-1016 _______ _
11104-28-2------Aroclor-1221. _______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 ______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 ______ _
U!;i(l'.!;i
I 8. 8 U
8.8 U
8.8 U
8.8 U
8. 8 U
8.8 U
8.8 U
8.8 U
18. U
10·. U
18. U
18. U
18. U
18. U
18. U
88. U
18. U
88. U
88. U
180 U
88. U
88. u
88. U
88. U
88. U
180 U
180 U
1.00
Q
---·~· ______ ;_ __________ ...,... ______ ----------
POIOt I PEST i / 81 "itev.
52
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-33-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-881-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SOG No.: -9~0 ____ _
Matrix: (soil/water) SOIL ·Lab Sample IO: ~29~2~7~5u5.__ __
Lab File IO: Sample wt/vol: 30.0 (g/mL) ~
LOW Level: (low/med)
% Moisture: not dee. 7 dee.
Date Received: 10/06/89
Date Extracted: 10(11/89
Date Analyzed: 10/16/89 Extraction: (SepF/Cont/Sonc) SQliC.
GPC Cleanup: (Y/N) L.. pH: ...1.....i Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
319-84-6--------alpha-BHC_________ 8.6 IU
319-85-7--------beta-BHC 8.6 iU 319-86-8--------delta-BH=c---------8.6 U
58-89-9---------gamma-BHC (Lindane)____ 8.6 u
76-44-8---------Heptachlor_________ 8.6 U
309-00-2--------Aldrin,....... ___ -,-.,-------8.6 U
1024-57-3-------Heptachlor epoxide_____ 8.6 u
959-98-8--------Endosulfan I________ 8.6 U
60-57-1---------Dieldrin__________ 17. u
72-55-9---------4,4'-00E__________ 17. U
72-20-8---------Endrin 17. U 33213-65-9------Endosurl=fa_n__,I~I=---------17. U
72-54-8---------4,4'-000 17. U 1031-07-8-------Endosulf_a_n_s_u_lrf=a~t~e-----17. U
50-29-3---------4,4'-DDT 17. U 72-43-5---------Methoxycrh..-lo_r________ 86. U
53494-70-5------Endrin ketone._______ 17, U
5103-71-9-------alpha-Chlordane______ 86. U
5103-74-2-------gamma-Chlordane.______ 86. U
8001-35-2-------Toxaphene 170 u 12674-11-2------Aroclor-1~0~16,.....-------86. U
11104-28-2------Aroclor-1221_______ 86. U
11141-16-5-,-----Aroclor-1232 . 86. I U --------53469 -2 l -9 - --- - -Aro cl or -l242 _______ 86. IU
12672-29-6------Aroclor-1248_______ 86. iU
11097-69-1------Aroclor-1254_______ ·170 iU
Q
11096-82-5------Aroclor-1260_______ 170 IU
------------,---,,----------,-, ,.,.--,---,---1--
POD I P2ST 1/87 Rev.
51
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lD EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-36-1
Lab Name: COMPUCHEM LABORATORIES Contract: r2-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : 49~0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: =2~9=2~7-58 __ _
Sample wt/vol: 30.0 (g/mL) CI__ Lab File ID:
Level: (low/med) LOW
% Moisture: not dee. i4~3 __ dee.
Extraction: (SepF/Cont/Sonc) fillliC.
Date Received: 10/06/89
Date Extracted: 10(11/89
Date Analyzed: 10(13/89
GPC Cleanup: (Y/N) li.._ pH: ...:J...J... Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
319-84-6--------alpha-BHC ________ _
319-85-7--------beta-BHC
319~86-8--------delta-BH=c---------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44-8---------Heptachlor ______ _;__ __
309-00-2--------Aldrin,...... ___ ...,...., ____ _
1024-57-3-------Heptachlor epoxide ____ _
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin:----------72-55-9---------4,4'-DDE. _________ _
72-20-8---------Endrin 33213-65-9------Endosu·~l~f-a-n-=-I~I-------
72-54-8---------4,4'-DDD 1031-07-8-------Endosulf_a_n_s_u_l~f~a~t~e-----
50-29-3---------4,4'-DDT _________ _
72-43-5---------Methoxychlor _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene ________ _
12674-11-2------Aroclor-1016 _______ _
11104-28-2------Aroclor-1221 _______ _
11141-16-5------Aroclor-1232 ______ _
53469-21-9------Aroclor-1242 ______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1--~---Aroclor-1254 --------11096 -82 -5 - - - - - -Aro cl or -1260 _______ _
14.
14.
14.
14.
14.
14.
14.
14.
28.
28.
28.
28.
28.
28.
28.
140
28.
140
140
280
140
140
140
140
140
280
280
u u
u
u
u
u
u u u
u u
u u
u
u
u u
u
u u
u
u
u
u u
u
u
Q
................... --........ -.,.......---------------------------
----------------""""RHa-'1.,....,.,'p'!'ST ____________ "'lfri7ri:11r,1,..1t,r.;e;7v-. --
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PESTICIDE ORGANICS ANALYSIS DATA SHEET. EPA SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS SL-37-1
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No. : ~9~0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: =2~9=2~7~59~--
Lab File ID: Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
30.0 (g/mL) ~
LOW
8 dee.
Extraction: (SepF/Cont/Sonc) S,OHC.
Date Received: 10/06/89
Date Extracted: 10/11/89
Date Analy~ed: 10/13/89
GPC Cleanup: (Y/N) t!..._ pH:~ Dilution Factor: 1.00
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG(KG
319-84-6--------alpha-BHC. ________ _
319-85-7--------beta-BHC
319-86-8--------delta-BH:~c,----------
58-89-9---------gamma-BHC (Lindane) ___ _
76-44~8---------Heptachlor ________ _
309-00-2--------Aldrin 1024-57-3-------Heptac~h~lo_r_e_p_o~x~i~d~e-----
959-98-8--------Endosulfan I _______ _
60-57-1---------Dieldrin ----------72-55-9---------4,4'-DDE _________ _
72-20-8---------Endrin
33213~65-9------Endosu~l~fa_n_I=r~------
72-54-8---------4,4'-DDD 1031-07-8-------Endosulf_a_n_su-l~f~a_t_e ____ _
50-29-3---------4,4'-DDT~---------72-43-5---------Methoxychlor 53494-70-5------Endrin keton_e ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene
12674-11-2------Aroclor-l.~0~1~6--------
11104-28-2------Aroclor-1221
11141-16-s------Aroclor-1232----~---
53469-21-9------Aroclor-1242 _______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _______ _
8.7
8.7
8.7
8.7
8.7
8.7
8.7
8.7
17.
17.
17.
17.
17.
17.
17.
87.
17.
87.
87.
170
87.
87.
87.
87.
87.
170
170
u
u
u
u
u u
u u
u u u u u u
u
u u
u u
u
u
u
u
u
u
u u
0
--------------------------------....................... .
. PUkM 1 'p£St 1/87 4kev.
j 49
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PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-34-1
Lab Name: COMPUCHEM LABORATORIES Contract: (2-88)-REVS
La~ Code: COMPU Case No.: 17902 SAS No. : SDG No. : ,,_9.,._0 ____ _
Matrix: (soil/watet) SOIL Lab Sample ID: ..._2,,__92,._7""'5...,6.__ __
Sample wt/vol: 30.0 (g/mL) G...__
LOW
Lab File ID:
Level: (low/med)
\ Moisture: not dee. 10 dee.
Date Received: 10/06/89
Date Extracted: 10(11/89
Date Analyzed: 10(13/89 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li..._ pH: _a_,__s_ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I
319-84-6--------alpha-BHC _________ I 8.9 U
319-85-7--------beta-BHC I 8.9 U
319-86-8--------delta-BHC I 8.9 U
58-89-9---------gamma-BHC (Lindane) I 8.9 U
76-44-8------~--Heptachlor I 8.9 U
309-00-2--------Aldrin I 8.9 U
1024-57-3-------Heptachlor epoxide I 8.9 U
959-98-8--------Endosulfan I I 8.9 U
60-57-1---------Dieldrin I 18. U
72-55-9---------4,4'-DDE I 18. U
72-20-8--------.-Endrin I 18. U
33213-65-9------Endosulfan II I 18. U
72-54-8---------4, 4 '-DOD I 18. I U
1031-07-8-------Endosulfan sulfate I 18. IU
50-29-3---------4, 4' -DDT I 18. I U
72-43-5---------Methoxychlor I 89. IU
53494-70-5------Endrin ketone I 18. IU
5103-71-9-------alpha-Chlordane I 89. IU
5103-74-2-------gamma-Chlordane I 89. IU
8001-35-2-------Toxaphene I 180 IU
12674-11-2------Aroclor-1016 I 89. IU
11104-28-2------Aroclor-1221 I 89. IU
11141-16-5------Aroclor-1232 I 89. I U
53469-21-9------Aroclor-1242 I ·09. IU
12672-29-6------Aroclor-1248, I 89. IU
11097-69-1------Aroclor-1254 I 180 IU
11096-82-5------Aroclor-1260 · I 180 I U
0
--------------------1------1--1 ___________ ; __ _
PoiUi "1 .,EST l/974tev.
···--··------------4 7fNl2___ _. SRIIPLE DRTR SUIIIIIU1¥ -48
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PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-35-1
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No.: SDG No.: .._9,,_0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ,,_2L9,,_27"-'5,._7,___ __
Sample wt/vol: 30.0 (g/mL) (i__
LOW
Lab File ID:
Level: (low/med)
% Moisture: not dee. =1_1 __ dee.
Date Received: 10/06/89
Date Extracted: 10(11/89
Date Analyzed: 10/13/89 Extraction: (SepF/Cont/Sonc) SQHC.
GPC Cleanup: (Y/N) Ji_ pH: -1.......9. Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
I 319-84-6-~------alpha-BHC _________ I
319-85-7--------beta-BHC I
319-86-8-~---~--delta-BHC I
58-89-9---------gamma-BHC (Lindane) I
76-44-8---------Heptachlor · I
309-00-2--------Aldrin I·
1024-57-3-------Heptachlor epoxide I
959-98-8--------Endosulfan I I
60-57-1---------Dieldrin I
72-55-9---------4,4'-DDE I
72-20-8---------Endrin I
33213-65-9------Endosulfan II I
72-54-8---------4,4'-DDD I
1031-07-8-------Endosulfan sulfate ____ _
50-29-3---------4,4'-DDT 72-43-5---------Methoxyc~h~l-o_r _______ _
53494-70-5------Endrin ketone ______ _
5103-71-9-------alpha-Chlordane _____ _
5103-74-2-------gamma-Chlordane _____ _
8001-35-2-------Toxaphene 12674-ll-2------Aroclor-l.~0~1~6-------
11104-28-2------Aroclor-1221 11141-16-5------Aroclor-1232----'------
53469-21-9------Aroclor-1242 _______ _
12672-29-6------Aroclor-1248 _______ _
11097-69-1------Aroclor-1254 _______ _
11096-82-5------Aroclor-1260 _________ _
I
9 .0 IU
9. o I u
9. o I u
9. o 1u
9. O I u
9. 0 IU
9.0 U
9.0 U
18. U
18. U
18. U
18. U
18, U
18, U
18. U
90. u
18. U
90. U
90. u
180 U
90, U
90. U
90, U
90. U
90. U
180 U
180 U
Q
,_,_ .. _,1, .. ~.-------.,..,,.-.......-,........,........--.,.....------,----------------
PiJRJI "1 11ES'T 1/811lev.
47
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-33-lMS
Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902 SAS No. : SDG No. : ,,_9,,._0 ____ _
Matrix: (soil/water) SOIL Lab Sample ID: ~2L9~2~33~0,_ __
Sample wt/vol: 30.0 (g/mL) L-Lab File ID:
Level: (low/med) LOW
% Moisture: not dee. _7,___ dee.
Date Received: 10/05/89
Date Extracted: 10/20/89
Date Analyzed: 10/23/89 Extraction: (SepF/Cont/Sonc) .5.0.liC.
GPC Cleanup: (Y/N) H.._ pH: --1....,i Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND {ug/L or ug/Kg) UG/KG Q
I I 319-84-6--------alpha-BHC _________ I 8.6 U
319-85-7--------beta-BHC I 8.6 U
319-86-8--------delta-BHC I 8.6 U
58-89-9---------gamma-BHC {Lindane) I 8.6 U
76-44-8---------Heptachlor I 8.6 U
309-00-2--------Aldrin I 8.1 U
1024-57-3-------Heptachlor epoxide I 8.6 U
959-98-8--------Endosulfan I I 8.6 U
60-57-1---------Dieldrin I 17. U
72-55-9---------4,4'-DDE I 17. U
72-20-8---------Endrin I 17. u'
33213-65-9------Endosulfan II I 17, U
72-54-8---------4,4'-DDD I 17. U
1031-07-8-------Endosulfan sulfate I 17. U
50-29-3---------4,4'-DDT I 17. U
72-43-5---------Methoxychlor I 86. U
53494-70-s-~----Endrin ketone I 17. u
5103-71-9-------alpha-Chlordane I 86, U
5103-74-2-------gamma-Chlordane I 86. U
8001-35-2-------Toxaphene I 170 U
12674-11-2------Aroclor-1016 I 86. U
11104-28-2------Aroclor-1221 I 86. U
11141-16-s~-----Aroclor-1232 I 86. U
53469-21-9------Aroclor-1242 I 86. U
12672-29-6------Aroclor-1248 I 86. U
11097-69-1------Aroclor-1254 I · 170 U
11096-82-5------Aroclor-1260 I 170 JU
------------------1-----1 ····'•-····· ....... -
POD 1 PEST • . 1797 keV.
----· --. --· ----· Z7Sl#l2-fi6 SRIIPLE DRTR SUlflO#lil 46
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10 EPA SAMPLE NO.
PESTICIDE ORGANICS ANALYSIS DATA SHEET
SL-33-lMSD
· Lab Name: COMPUCHEM LABORATORIES Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 17902
Matrix: (soil/water) SOIL
SAS No.: ---·sDG No.: ,,_9,._0_~---
Lab Sample ID: ~2,,_9~23~3~1,__ __
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
30.0 (g/mL) L__
LOW
7 dee.
Extraction: (SepF/Cont/Sonc)· ~
GPC Cleanup: (Y/N) li.._ pH: ....1.,_6_
Lab File IO:
Date Received: 10/05/89
Date Extracted: 10/20/89
Date Analyzed: 10/23/89
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG 0
319-84-6--------alpha-BHC 8.6 u
319-85-7--------beta-BHC 8.6 u
319-86-8--------delta-BHC 8.6 u
58-89-9---------gamma-BHC (Lindane) 8.6 u
76-44-8---------Heptachlor 8.6 u
309-00-2--------Aldrin 8.6 u
1024-57-3-------Heptachlor epoxide 8.6 u
959-98-8--------Endosulfan I 8.6 u
60-57-1---------Dieldrin 17. u
72-55-9---------4,4'-DDE 17. u
72-20-8---------Endrin 17. u
33213-65-9------Endosulfan II 17. u
72-54-8---------4,4'-DDD 17. u
1031-07-8-------Endosulfan sulfate 17. u
I 50-29-3---------4,4'-DDT 17 •. u
I. 72-43-5---------Methoxychlor 86. u
53494-70-5------Endrin ketone 17. u·
5103-71-9-------alpha-Chlordane 86. u
5103-74-2-------gamma-Chlordane 86. u
8001-35-2-------Toxaphene 170 u
12674-11-2------Aroclor-1016 I 86. u
11104-28-2------Aroclor-1221 I 86. u
11141-16-5------Aroclor-1232 I 86. IU
53469-21-9------Aroclor-1242 I 86. IU
12672-29-6------Aroclor-1248 I 86. JU
11097-69-1------Aroclor-1254 I 170 iU
11096-82-5------Aroclor-1260 I 170 JU
I I ..
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ORM 1: P!ST ij8 I 9tev.
45