NCD980840409_19891101_Charles Macon Lagoon & Drum_FRBCERCLA RI_RI FS Study Remedial Investigation Report - Volume IV-OCR

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MACON/00:::KERY NPL SITE
REMEDIAL INVESTIGATION/
FEASIBILITY STUDY
REMEDIAL INVESTIGATION REPORT
VOLUME IV
--·
.:I ~tc•
.I /,u(/ "t111eD
S(I~ "U '8
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Wb '9/ ~(CJJat
I Macon/Dockery Site ' ' I _ Remedial Investigation/ ~.
' -Feasibility Study I
I
I Remedial. Investigation Report
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I Volume IV
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I 1990
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I SIRRINE
ENVIRONMENTAL
11 CONSUL TAN TS
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CDMPUCHEM
lABOAATORJES
INORGANIC CASE SUMMARY NARRATIVE
CASE# 24520 SDG# 18160A
CONTRACT# 787
SAMPLE NUMBERS: TR-1-1, TR-11-1, TR-2-1, TR-2-2,
TR-3-1, TR-4-1, TR-5~1, TR-6-1, TR-7-1,
TR-8-1, TR-9-1
This portion of case 24520 was received in good
condition with the appropriate chain-of-custody documents,
on October 18,19,20, 1989. The SDG consists of eleven soil
sample for the analysis of complete HSL metals and cyanide.
The enclosed cover page reflects both Sirrine Enviro"nmental
and CompuChem Sample Identifiers.
The associated quality control sample spike, TR-5-1S,
was outside the control limits for antimony, cadmium,
copper, and •elenium, therefore the values were flagged with
an 'N'in all of the samples. The associated quality control
duplicate, TR-5-lD, was outside the control limits for
copper and zinc, therefore the values were flagged with an '*' in all' of the samples.
Method of Standard Addition was done for arsenic in
samples TR-1-1, TR-3-1, TR-4-1, TR-7-1, TR-8-1, and TR-5-1.
The value of arsenic was flagged with an 'S' or a'+' in
these samples.
A serial dilution was done on sample TR-9-lL. The
adjusted sample concentrations of barium, calcium,
manganese, and vanadium were not within 10% of their
original values, therefore the values were flagged with an
'E', in all of the samples.
The concentrations of antimony, calcium, magnesium,
silver and sodium fell between the Instrument Detection
Limits (IDLs) and the Contract Required Detection Limits
(CRDLs) in the majority of the samples. The concentrations
of mercury, selenium, cyanide and thallium fell below the
IDL, while the remaining analytes had concentrations above
the CRDL.
Release of the data contained in this hard copy data
package has been authorized by the Laboratory Manager or.his
designee, as verified by the---rG~lowing sign ture
nne c. Alson
chnical Reviewer
Note: This report is paginated for reference and
accountability in decreasing numerical sequence.
Page-1
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 (919) 549•8263
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 -'-----
Lab Code: COMPU Case No.: 24520 SAS No.:
CLIENT SAMPLE NO.
I TR-4-1 I
SDG No.: 18160A
Matrix (soil/water): SOIL Lab Sample ID: 296039
Level (low/med):
% Solids·,
LOW
86.4
Date Received: 10/18/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
74Z -'Ju-,
/44 -Jb-U
74~,-,a-z
7440-39-3
144U-41-I
7440-43-9
7440-70-Z
7440-4/-j
7440-48-4
/44U-oU-8
7439-89-6
14J'J~'JZ-l
7439-95-4
74J9-96-o
7439-'J 1-b
7440-0Z-U
7440-U'J-I
77BZ-49-Z
144U-,ll-4
7440-23-,
744U-.l8-U
744U-bl.-l.
7440-66-c
Color Before:· BROWN
Color After: YELLOW
Comments:
fORM l -PAGE l
I Analyte !ConcentrationlCI Q
Aluminum lc900
Antimony b. l u N Arsenic 3. 7 s
Barium I. I. • , B E
Beryllium .oB B
Caamium I. • b N
Calcium 08.0 B E
Cnromium 14 . I.
Coba!t 5.0 B
Copper l 4 . I N•
Iron 170uu
Leaa 'J . u
Magnesium .l 0 8 B
Manqanese 08. 7 E
Mercury .!O
Nicke! 8.6 u
Potassium 4 j '-B
Se!enium l. 3 u WN
Silver .bB u
Saa1um Zl3 u
Tna11ium .4b u vanaaium 4U.4 E
Zinc Jl..l • Cyaniae . , " u
Clarity Before:
Clarity After:
FORM I -IN
18610A INORGANICS CASE
IM I
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Texture: MEDIUM
Artifacts:
7/88
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U.S. EPA -CLP
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INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 .c....;:..=._ __ _
Lab Code: COMPU Case No.: 24520 SAS No. :
CLIENT SAMPLE NO.
I TR-3-1 I
SDG No.: 18160A
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
89.4
Lab Sample ID: 296047
Date Received: 10/18/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
/4 ~9-90-5
74 40-36-0
/440-38-2
7440-39-3
/440-41-7
1400-43-9
/440-70-2
1400-47-3
/440-48-4
1440-50-8
/439-89-6
1439-92-1
7439-95-4
I q 39-96-5
7 4 3 -97-6
/ 4 4 -02-0
/44 -09-7
77H2-49-2
/400-22-4
7440-23-5
/400-28-0
7440-62-2
/440-66-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 2
I Analyte IConcentrationlCI Q
Aluminum 16300
Antimony 6.o u N
Arsenic 3. 2 s
Barium .l l. 6 B E
Beryllium . 62 B
Cadmium l. l u N
Calcium 740 B E
Chromium 15. 7
Cobalt 5. 4 B
Coccer 8. 7 N*
Iron 12700
Lead 30 .1
Magnesium 3.,,.,, B
Manqanese 82.2 E
Mercury . 11 u
Nickel 8.4 u
Potassium 879 B
Selenium 2. 2 u WN
Silver .66 u
Sodium 350 B
Thallium . 49 B
Vanadium 33. 0 E
Zinc 3 7 • 4 • Cyanide . ~/; u
Clarity Before:
Clarity After:
FORM I -IN
18610A INORGANICS CASE
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Texture: COARSE
.Artifacts:
7/88
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 c....c__;:_ __ _
Lab Code: COMPU Case No.: 24520 SAS No.:
CLIENT SAMPLE NO.
I TR-2-2 I
SDG No.: 18160A
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
88.5
Lab Sample ID: 296048
Date Received: 10/18/89
.
Concentration units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
7429-90-5
7 4·if!J-]6-lr
7440-38-2
TI, ,IT-311-3
T<l 10-41-7 TI, 10-43-9
74 4

□
-70-2
T<l 40-(7-3
7U0-48-4
~0--S, -8'
TI39-H -6
71 , 19-9 -1
T<l 139-9";-4
7<,j~-96-5
TITI-<J -6
T440-0 -0
1a □-o -7
TI82-4 -2
7 44□-2 -4
T440-2 -5
7< □-2 -o
" 0-6 -2
7< 0-6 -6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 3
I Analyte IConcentrationlCI Q
Aluminum 5180 Antimonv 6. 1 u N Arsenic 2.2 B Barium 27.7 B E Berv!lium .47 B Cadmium 1.1 u N Calcium 279 B E Chromium 4.7
Cobalt 3.6 B Cooner 3. 8 B N* Iron 3620
Lead 15.0
Maanesium 181 B
Manaanese . 84. 9 E Mercurv . 1 u
Nickel 8. u
Potassium 73 B Selenium . 4' u WN Silver • oB u Sodium 251 B
Thall1um • 4 u Vanadium 12.' E· Zinc 31.. • Cvaniae • c;,:; u
Clarity Before:
Clarity After:
FORM I -IN
INORGJ:lNICS CJ:lSE ..
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Artifacts:
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 .:....::..::.._ __ _
Lab Code: COMPU Case No.: 24520 SAS No.:•
CLIENT SAMPLE NO.
I TR-1-1
SDG No.: 18160A
Matrix (soil/water): SOIL
~evel (low/med):
% Solids:
LOW
91.1
Lab Sample ID: 296050
Date Received: 10/18/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
/4 19-90-5
74 10-36-0
/4 10-38-2
/440-39-3
/440-41-7
7440-43-9
/440-/U.-2
/440-47-3
1440~48-4
1440-~u-8
/4j9-89-6
t4J9-92-l
74j9-95-4
/4J9-96-5
7439-~1-6
1440-02-0
t440-u~-7
771!2-4'1-2
1440-22-4
7440-Z3-5
/440-28-0
1440-62-Z
/440-66-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM 1 -PAGE 4
I Analyte IConcentrationtCI Q
Aluminum 10300
Antimony ., . 9 u N
Arsenic 4. 0 s
Barium 4Z. 4 B E
Berv11ium . 22 u
Cadmium Z3. 8 N
Calcium 1830 E
Chromium 8. 3
CoDalt 5,4 B
Conner 10.6 N*
Iron 6670
Lead ZB.4
Maqnesium 41! B
Manaanese 124 E
Mercury . ll u
Nicke1 8. 3 u
Potassium 5Z8 B
Selenium . 45 B WN
Silver . 65 u
Sodium 204 u
Tllall ium . 4 3 u
Vanadium 17. 4 E
Zinc 34. 2 *
Cyantde . .,., u
Clarity Before:
Clarity After:
FORM I -IN
18610A INDRGANICS CASE
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Artifacts:
7/88
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U.S. EPA -CLP
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INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 --'----
Lab Code: COMPU Case No.: 24520 SAS No.:
CLIENT SAMPLE NO.
I TR-2-1 I
SDG No.: 18160A
Matrix (soil/water): .SOIL
Level (low/med):
% Solids:
LOW
88.5
Lab Sample ID: 296049
Date Received: 10/18/89·
Concentration Units (ug/L or mg/kg dry weight); MG/KG
ICAS No.
74~9-90-5
1440-36-0
1440-, .. -2
1440-3 -3
74<10-4 -7
/440-4 -9
7440-70-2
/440-47-3
74 40-• -4
14 40--8
/ 4 39--6
14 3 --1
14 3 --4
/43 --5
1439-',1/-6
1440-02-0
7440-09-7
t 1112-49-2
140-''-4 7<
140-23-5 11
7440-'A-O
/440-62-2
7440-66-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 5
I Analyte IConcentrationlCI Q
Aluminum 6410 Antimony 7. 4 B N Arsenic 2, 3
Barium 52. 4 E
Berv11ium .l. 1
Cadmium 29.8 N Calcium 4Z6 B E Chromium 23. 4
Cot>alt 18,2
Conner 34. 4 N*
Iron 4430
Leaa 38.5
Maanesium 458 B
Manaanese 106 E
Mercury .11 u
Nickel r2.o
Potassium 1540
Selenium . 4 4 u WN
Silver 1.0 B
Sodium 925 B Tna11ium . 44 u
vanadium 22.9 E
zinc 6 3. B • Cvanide -~6 u
Clarity Before:
Clarity After:
FORM I -IN
18610A INORGANICS CASE
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Texture: COARSE
Artifacts:
7/88
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
TR-5-1 Lab Name: COMPUCHEM LABORATORIES Contract: 788 I I -----
Lab Code: COMPU case No.: 24520 SAS No.: SDG No.: 18160A
Matrix (soil/water): SOIL
Level ( loJw/med):
% Solids:
LOW
86.4
Lab Sample ID: %96300
Date Received: 10/19/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
14.l~-~u-5
7440-36-0
144U-,o-.l
7440-39-3
144U-4l-l
7440-43-9
144U-IU-.l
7440-47-3
744U-46-4
I 4 ,o-,u-8
74 19-89-6
14 1!1-.!IZ-l
1439-95-4
74.l!l-!lb-,
7439-97-6
144U-U.l-U
7440-09-7
776.l-49-.l
7440-22-4
144U-.l.l-,
1440-28-0
7440-62-.l
144U-bb-b
Color Before: BROWN
Color After: YELLOW
Comments:
FORM 1 -PAGE 6
I Analyte I Concentration IC I O
Aluminum .lJ,UU
Antimonv 6. 2 u N Arsenic l. .l B + Barium ll. 5 B E Beryllium • .l .l u Cadmium l.2 u N Calcium 4bo B E
Chromium 3 5. 7
CoCalt 6. 1 B
Coooer 7 I . l N* Iron 25300
Leaa I. 4
Ma<mesium 611 B Manganese U/ E Mercurv . lZ u Nickel J,.b
Potassium 1450
Selenium • 14 B WN Silver .69 u Soa1um ll V I B
Tnallium . 4 5 u
vanaa1um b I . .l E
zinc 34 • ..: • cvanide .58 u
Clarity Before:
Clarity After:
FORM I -IN
18610A INORGANICS CASE
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Artifacts:
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.... 3-,, ..; '
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 _;;..:::..._ __ _ I 9168TR121 I
Lab Code: COMPU Case No.: 24520 SAS No.: ___ SDG No.: 18210B
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
85.0
Lab Sample ID: 297269
Date Received: 10/23/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte I Concentration IC I Q I r-i I
74 !9-90-~ Aluminum 11100 • p
/4 10-36-0 Antimonv 6. 4 u N p
/ 4 10-,11-2 Arsenic 1. 7 B SN F
/4 10-39-3 Barium 22.6 B p
/ 4 10-41-7 Bervllium .66 B p
/4 10-43-9 Cadmium l. 2 u p
/ 4 10-70-2 Calcium 225 B * p
/4 10-47-3 Chromium 85.7 p
/4 0-48-4 Cobalt 8.4 B p
144 -~0-8 Conner 27.8 * p
/4 -89-6 Iron .ll9o □ p
14 -92-1 Lead 6 .1 F
/ 4 -95-4 Maqnesium 400 B p
74 -':lo-5 Manqanese 134 p
14 -':I t-6 Mercury .11 u CV
/4 -02-0 Nickel 23.5 p
74 ,0-09-7 Potassium 139 u p
I I 12-49-2 Selenium ,41> u WN F 74 10-22-4 Silver . 71 u p
/4 10-23-5 Sodium 221 u p
744 --Tna11ium .46 u w F
/44 - -vanadium 104 p
/44 --Zinc 27.2 p
Cvanide . 59 UN• AS
Color Bef'ore: BROWN Clarity Before: Texture: COARSE
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 2
FORM I -IN 7/88
r r.:o rf" 157
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CbMPUCHEM
lABORATORJES
Case Narrative
Sirrine Environmental
Case No. 24520 SDG No. 1877JA
Contract No. 788
Cli,mt Sample No.: MW-lR, MWl-1-1, MWl0-1-1, MWll-1-1,
MW12-l-l, MW12-l-2, MW19-l-l, MW27l-l,
MW20-l-l, MW21-l-l, MW22-l-l, MWJ-1-1,
MW.4-1-1, PB-1, TB-4
This case consisted of fifteen water samples analyzed for the
Inorganic Target Analyte List (TAL) met~ls and cyanide. The
samples were received intact on December 21, 22; and 2J, 1989
with the Chain-of-Custody (COC) Records. The enclosed cover
page reflects Sirrine Environmental and Co~puChem sample
identifiers.
The associated quality control sample spike, MWJ-1-lS, was
outside the control limits for arsenic and selenium, therefore
the concentrations were flagged with an 'N'. The duplicate,
MWl0-1-lD, was outside the control limits for aluminum,
cadmium, and chromium, therefore the concentrations were
flagged with an'*'·
Method
sample
an 'S' .
of Standard Addition (MSA) was done for thallium in
MW21-l-l, therefore the concentration was flagged with
A serial dilution was done on sample
sample concentrations were within
concentrations for all of the analytes
MW22-l-l.
10% of
tested.
The adjusted
the original
Please refer to the enclosed laboratory notice concerning
arsenic results for sample MW22-l-l. Due to the presence of
considerable amounts of aluminum and iron, arsenic is being
reported from the GFAAS analysis.
In one or more of the samples, the concentrations of analytes
fell between, below, and above the Instrument Detection Limits
(IDLs) and the Contract Required Detection Limits (CRDLs).
Anna Feather
Technical Reviewer
February 2, 1990
Note: This report is paginated for reference and
accountability in decreasing numerical sequence.
COMPUCHEM LABORATORIES. INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Res.earcn Triangle Park, NC 27709 (919)549•8263
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Laboratory Notice
SDG: 18773A
Element: As
Upon an exam1nat1on of the arsenic results for ComcuChem
number 311200 (Client ID# MW22-1-1 I, a difference in the ICP
and GFAAS analysis is seen. The ICP result is 273 ug/1, and
the GFAAS result is oelow the detection limit. By ICP, the
sample was found to contain considerable amounts of aluminum
and iron which are known to enhance the arsenic signal. This
phenomenon is not seen by GFAAS. Furthermore, the GFAAS
analysis exhibited good recovery on the cost-digestion sci~e.
This indicates minimal interference. It is for these
reasons arsenic 1s oeing reported from the GFAAS data.
MarK E. Crews
Inorganics Data Review
2/1/90
QA accrova l # _J_J~~---.
I( ~~'-'-JI ~
Q,4~*
J../;./90
INORGANICS CASE 18773A
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES MW-lR Contract: 788 _;_;;..::.._ __ _ I I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
\ Solids:
LOW
0. 0
Lab Sample ID: 310369
Date Received: 12/21/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/4l':l-::,u-,
7440-36-0
7440-38-2
7440-39-3
7440-41-/
7440-43-9
744U-/U-l
7440-47-3
7440-4ts-4
7440-50-8
7439-ts':l-t>
7439-9Z-l
7439-':l,-4
74J':l-::,o-,
7439-':l l-6
7440-02-0
1440-U':I-I
7 ltlZ-49-Z
7440-ll-4
7440-Z3-5
7440-lB-0
7440-c..:-..:
7440-oo-6
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE l
I Analyte IConcentrationfCI Q
Aluminum· 34. l
Antimonv ll. 0
Arsenic 3.0
Barium 1.0
Berv1lium 1.0
Cadmium 5. 0
Calcium 101
cnromium 5. 0
Cobalt 3. 0
Conner 15.9
Iron l3. 3
Lea□ 2.0
Mac:mesi um 90.4
Manaanese 1. u
Mercurv . zo
Nickel l':I. U
Potassium 1Z60
Se1enium Z. 0
Silver 4. 0
Sodium 1490
Tna11ium 2.0
Vanadium z.o
Zinc 26.4
Cvan1de 10.0
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
B • u
u N
u
u
u •
B
u • u
B
B u
B
u u
u u
u N
u
u
u
u
u
IM I
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Artifacts:
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INORGANICS CRSE 18773A 216
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Contract: 788 -~---
SAS No.:
.I __ M_w_1_-_1_-_1 __ _.I
SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 310372
Date Received: 12/21/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/42~ -~u-:,
744C -36-0
144~-Jt!-Z
744 -l-3
144 --I
744 -3-9
7440-70-2
744U-47-J
7440-48-4
744U-!:>0-8
7439-t!~-o
7439-92-1
74J~-9!:>-4
7439-96-5
74J ·-~/-0
744 -02-0
144 -U9-I
7782-49-2
144U-ZZ-4
7440-23-5
/44U-Zt!-U
7440-62-2
7440-66-6
Color Before: BROWN
Color After:. COLORLESS
-Comments:
FORM 1 -PAGE 2
I Analyte IConcentrationlCI Q
Aluminum 4~10
Antimony Zl. 0
Arsenic 3.u
Barium 101
Bervllium l. 4
Caomium 5.0
Ca1cium 1780
cnromium :,.o
Cobalt 3.0
Coooer 15.2
Iron ll2uu
Lead J. l
Macmesium 1380
Manaanese lll
Mercurv .20
Niclte--i 29.0
Potassium 12ou
Se enium 10.0
Si J.ver 4. 0
So ~ium ll 5UOuu
Tnallium 2. 0
Vanacfi um 8.0
z1nc 52.4
Cvanide 10.0
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
• u u N
B
B
u •
B u • u
B
B
u
u
u u WN
u
u
B
u
IM I
p
p
P'
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
P'
p
p
P'
p
p
AS
Texture:
Artifacts:
7/88
INORGANICS CASE 18773A 215
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
CLIENT SA~PLE NO.
Lab Name:: COMPUCHEM LABORATORIES Contract: 788 _;._:c..:;_ __ _ I MWl0-1-1 I
Lab Code: COMPU case No.: 24520 SAS· No.: SDG No.: 18773A
Matrix (Heil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
. Lab Sample ID: 310367
Date Received: 12/21/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-5
7440-36-0
.7440-38-2
7440-39-3
7440-41-7.
7440-43-9
7440-70-2
7440-47-j
744 -48-4
744 -~0-8
743 -89-6
74,~-9l-l
74J -95-4
74, -9b-~
743 -97-6
7440-Ul-U
7440-09-7
778l-49-Z
7440-22-4
7440-ZJ-5
7440-28-0
7440-62-2
7440-bb-b
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE 3
I Analyte IConcentrationlCI Q
Aluminum . U600
Antimony ---n .7l
Arsenic 3.0
Barium . Tlll!1I
Bervl1ium 5. 0
Cadmium 5,0
Calcium 121()0
cnromium n.--s
Cobalt 57.9
Coaaer 40.8
Iron ,5.,\.10
Lead 13. 8
Maanesium 8670
Manaanese 1480
Mercury ,20
Nickel 50.5
Potassium 10400
Selenium 10.0
Silver 4.0
Sodium .B 1110
Tna11ium 2. 0
vanadium J4. l
z1nc 238
Cvan1de Tlr,4
Clarity Before: CLOUDY
Clarity After: CLEAR
l"ORM I -IN
• u
u N
B
u •
•
u
u WN
u
u
B
IM I
p
p
P'
p
p
p
p
p
p
p
p
l"
p
p
CV
p
p
F
p
P.
l"
p
p
AS
Texture:
Artifacts:
7/88
INO,RGRNICS CASE 18773A 214
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: _7~8~8 ___ _ I MWll-1-1 I
Lab Code: COMPU Case No.: 24520 SAS No.: SOG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample IO: 310371
Date Received: 12/21/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
14 -90-5
I q' -36-0
14 • -38-2
I q' -H-3
14 • -41-7
7 -rJ-<j
I -'0-Z
I -7-3
74• -48-4
14 -50-8
14 -!l!f-6
74 19-92-1
14 19-95-4
74 19-,,o-5
14 19-!f 1-6
I q 10-0Z-O
14 -U'l-7
I I -•!f-2
14 -22-4 ,. -Z3-5
14 -2R-0
14 -6Z-2
74 10-bb-6
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE 4·
I Analyte IConcentrationlCI O
Aluminum 1540
Antimony Zl.0
Arsenic .3.0
Barium !! l. 5
Bervllium 1.0
Cadmium I .
Calcium 1 1
Chromium
Cobalt 3. a
Conner 13. 0.
Iron 4410
Lead 2.5
Maanesium 1030
Manaanese 61. 2
Mercury .zo
Nickel 29.0
Potassium 1260
Selenium .2. o
Silver 4. 0
Sodium 2 7.00
Thallium z.o
Vanadium 2.0
zinc ou.8
Cyanide 1 n. o
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
• u u N
B
u
u • B
u • u
B
B
B
u
u u
u WN
u
B
u u
u
IM I
p
p
F
p
p
p
p
p
p
p
p
F'
p
p
CV
p
p
F .. p
p
F
p
p
AS
Texture:
Artifacts:
7/88
INDRGRNICS CASE J8773A 213
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 -"-'-------
I . MW12-l-l I
Lab Code: COMPU Case No.: 24520 SA S No.: SDG No.: 18773A
Matrix (soil/water): WATER
Leve 1 ( 1 ClW/med) :
% Solids:
LOW
0. 0
Lab Sample ID: 311190
Date Received: 12/23/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-!>
/44U-J0-0
7440-Jll-l
7440-39-3
/440-41-/
7440-43-9
/44U-/U-2
7440-47-3
144U-41:1-4
7440-50-8
/4J9-1:19-b
7439-92-1
74n-95-4
14J9-:,o-!>
743 -'11-6
/44 -Ul-U
744 -u:,-7
/ idJ.-.. '3-I.
7440-ZZ-4
/44U-2J-!>
7440-Zll-O
/4~u-CJ.-J.
7440-66-6
Color Be:Eore: BROWN
Color After: COLORLESS
Comments:
FORM l -PAGE 5
I Analyte I Concentration IC I O
Aluminum 8600
Antimonv 21. 0
Arsenic j. 0
Barium 99.5
Beryllium l. I
Cadmium 5.0
Ca1cium lO:,v
cnromium 33.7
Coca1t '1. l
Coccer 37.8
Iron lJ!>UU
Lead 15.8
Maqnesium 1470
Manganese Jll
Mercurv .,o
Nicxe1 J.'1.0
Potassium J9!>U
Selenium 10.0
Silver 4. U
Sodium 4370
Tna1uum l.U
vanaaium 11. 5
Zinc I!> . l
cvaniae 10.0
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
• u
u N
B
B
u •
B •
B
B
u
u
B
u N u
B
u
B
u
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture:
Artifacts:
7/88
INORGANICS CASE 18773A 212
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: 788 -e..c.._ __ _ I MW12-l-2 I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Level ( l,Jw/med):
% Solids:
LOW
0.0
Lab Sample ID: 311193
Date Received: 12/23/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-~
7440-36-
744U-Jtl-
7440-J,,-
7440-4!-I
744U-4J-9
7440-70-2
/44U-41-J
7440-48-4
744U-~0-8
7439-tl!I-O
74H-9Z-l
7439-95-4
7 4 J9-,,o-5
7439-97-o
744U-02-0
7440-u -I
77112-4' -2
/44U--' -4
7440-2 -5
/4~u-J. -U
7440-62-2
7440-00-0
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM l -PAGE 6
I Analjte IConcentrationlCI Q
Aiuminum 11800
Antimonv Zl. 0
Arsenic 3.0
Barium 102
Bervllium l. 7
Cadmium ~. 0
Calcium 2400
cnromium Jo. 7
Cobalt 6. 0 Conner Jo.s
Iron 1~7.00
Leaa 15.4
MaQnesium 1600
Mariaanese H9
Mercurv .20
Nickel j j . I!
Potassium 3 70
Selenium l . 0
Silver . 0
Sodium j/90
Tnallium 2.0
Vanadium 9.8
zinc 70.8
Cvan i ""'e 10.0
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
• u
u N
B
B
u •
.B •
B
B
u
B
B
u N
u
B
u
B
u
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture:
Artifacts:
· 7/88
INORGANICS CASE 18773A 211
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I MW19-l-l
.c..cc...::..._ __ _
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (,;oil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 310370
Date Received: 12/21/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
jCAS No.
742'1-90-5
1440-3 -0
744!1-3 _---,:
7440-3 -3
,T4lr-4T-7
7440-43-9
,T40-Tll-2
744 □-47-3
144 '-48-4
744 -50-8
,TI ~-89-6
743'-92-1
14l-if-7Pi-4
TI39-96-5
7 4 .f9-7<7-1i
7~40-U.l-0
"744lr-09-7
7782-49-2
7440-22..:-~
7~40-23-5
744ll-21 -lJ
1440-6. -2
744 □-oc -6
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE 7
I Analyte jConcentrationlCI Q
Aluminum 7360
Antimonv · 21. 0
Arsenic 3.0 Barium 212 Bervllium l. 0
Cadmium 5.0 Calcium u,ooo
Chromium 80.l Coba-It 110
Coccer 56.8
Iron 252uo
Lead 3.6
Maanesium 15000
Manaanese 3250 Mercurv . zo
Nickel 91. 5
Potassium 1560
Selenium 10.0
S11ver 4.o
Sodium 19700
Tnallium Z. C Vanadium 3 5.,
Zinc 6 'I • ' Cvanide 10.0
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
• u
u N
u
u •
•
u
B
u WN
u
u
B
u
IM I
p
p
P"
p
p
p
p
p
p
p
p
P"
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture:
Artifacts:
7/88
INORGANICS CASE 18773A
I
210
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Nam!!: COMPUCHEM LABORATORIES Contract: 788 l MW2-l-l
.c....;;..o.... __ _
Lab Codi!: COMPU case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
,·solids::
LOW
0.0
Lab Sample ID: 311195
Date Received: 12/23/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
JCAS No.
I ' 129-90-5
7< 140-.36-0
,, 40-38-2
7440-H-3
1440-41-7
7440-43-9
1440-70-2
7440-41-3
1440-48-4
7' 14n-~n-e
I ' 39-89-6
7• 39-92-1
I ' 39-95-4
7• 39-96-~ ,, ,39-97-6
7, ,40-0 -o
/•,40-0 -7
I '82-4 -2
I· 140-22-4
I 140-23-5 ,, 140-28-0 ,, 140-62-2
I 140-66-6
Color Be:Eore: BROWN
Color After: COLORLESS
Comments,
FORM l -PAGE 8
I Analyte JConcentrationJCI Q IM I
Aluminum 8720
Antimony ll.O
Arsenic 3.0
Barium . 248
Bervllium 1. 6
Cadmium 5.o
Calcium lu::10
cnromium 20.7
Cobalt 6.9
Coooer 27.7
Iron 17700
Lead 5. 2
Maanesium 3160
Manganese 322
Mercurv .20
Nickel 29.0
Potassium 4610
Selenium 10.0
Silver 4.0
Sodium 5490
Thal uum . 2.0
Vana<11um -., "' • ft
zinc 110
Cyanide 10.o
Clarity Before: CLOUDY
Clarity After: ·CLEAR
FORM I -IN
I NO,RGAN I cits CRSE
I ,
• p
u p
u N r
p
B p
u • p
B p
• p
B p
p
p
r
B p
p
u CV
u p
B p
u N r u p
p
u r
B p
p
u AS
Texture:
Artifacts:
7/88
1877:JR
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name•: COMPUCHEl'I LABORATORIES Contract: 788 -----I MW21-l-l I
.Lab Code·: COl'IPU case No.: 24520 SAS No.: SOG No.: 18773A
Matrix (soil/water): WATER
Leve 1 ( 1 ow/med) :
% Solids:
LOW
0. 0
Lab Sample ID: 311188
Date Received: 12/23/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-5
744U-j0-U
74•u-Ja-l
7440-H-J
7440-41-1
7440-4J-"
744U-IO-.l
7440-47-J
7440--48-4
7440-5 -c,
74J,,-8 -
74J"-" -
74J>P-9 -·
74J"-10-,
74J>P-7-b
74.u-1.t-u
7440-09-7
''"'-4"-" 744 -ZZ-4
14~ -,tj-,
744 -zs-o
/44 -bl-.t
744 _.,.,_6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORl'I 1 -PAGE 10
I Analyte IConcentrationlCI O
Aluminum 793
Antimony l 411
Arsenic .<U. 6
Barium 1411
Berv11ium 1.4 Caamium 4." Ca1c1um I . 0
Cnromium l,,.,
Co0a1t 411 . Z
Couuer 04.4 Iron 498
Leaa 1,." l'lagnesium '"' l'langanese ,g.
l'lercurv l . Nicxe1 4" . Potassium llbO
Se1enium 1,.u
Si.1.ver 4.0
Soaium l I" U Tna.1..1.ium l . l
Vanaaium . " Zinc . ~
Cvaniae .. u. u
.
Clarity Before: CLEAR
Clarity After: CLEAR
FORl'I I -IN
•
N
B
• u •
B
B
u
N
u
u
s
u
I II I
p
p
F
p
p
p
p
p
p
p
p
I'
p
p
CV
p
p
I'
p
p
I'
p
p
AS
Texture:
Artifacts:
7/88
INORGRNICS CASE 18773A :208
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Nan1e: COMPUCHEM LABO RA TORI ES Contract: ~7~8~8 ___ _ I MW20-l-l I
Lab Code: COMPU case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Leve 1 ( 1 ow/med) :
% Solids:
LOW
0. 0.
Lab Sample ID: 311186
Date Received: 12/23/89
Concentration Units (ug/L or mg/kg dry ~eight): UG/L
ICAS No.
142g-90-5
7440-36-0
7440-c -2
7440-3 -7440-4 -
7440-43-'
7440-70-.
7440-47-3
TITI!-411-4
7440-50-8
TITI _ --irg--l'i
74j~-92-l
TITI -"5"-4
74H-96-5
TI 3 <i-<rT-l'i
7440-02-0
7440-09-7
TTJIL-~-L
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66.,;6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 9
I Analyte IConcentrationlCI O IM I
Aluminum 22.6 B * p
Antimonv 21,0 u p
Arsenic 3.0 u N F
Barium 1.0 u p
Bervllium 1.0 u p
Cadmium ~. 0 u * p
Calcium 17.0 u p
Chromium ~. 0 u * p
Cobalt 3.0 u p
Coooer 4. 0 u p
Iron 58.8 B p
Lead 2. 0 u F
Maonesium 56.0 u p
Manoanese 1.0 u p
Mercurv . 20 u CV
Nickel 29.0 u p
Potassium 1260 u p
se--ienium 2. 0 u N F
Silver 4. 0 u p
Sodium 1490 u p
T1ia1Tium 2.0 u F
Vanarllum 2. 0 u p
Zinc 3.5 B p
Cvanide 10.0 u AS
Texture: Clarity Before: CLEAR
Clarity After: CLEAR Artifacts:
FORM I -IN
INORGRNICS CASE 18773R
I
7/88
207
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U.S. EPA -CLP
1 CLIENT SAMPLE NO
INORGANIC ANALYSIS DATA SHEET
MW22-l-l Lab Name: COMPUCHEM LABORATORIES ContracJ. 788 _;__::_.::_ __ _ I
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
SAS No.: SDG No.: 18773A
Lab Sample ID: 311200
Date Received: 12/23/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I . ICAS No. I Analyte IConcentrationlCI O IM I I TI29-9O---S A--r umi num 98600 • p
7440-36-0 Antimonv 21. 0 u p
TI40-38-2 Arsenic -. a u WN P" T440-TI-1" Barium . 0 u p
TI40-41-7 Be rvrI i um .a u p
TI-.nr-4'J _--q Cadmium . 0 • p
7440-70-2 Calcium 1 . a u p
TTTir-47-3 Chromium . 0 u • p
7440-48-4 Cobalt .1 B p
TTTir ----.,0 -11 Conner . 0 u p
7-.J39-89-6 Iron 97 :oo p
7439.-92-l Lead .. 0 u P"
1439-95-4 Maanesium ,09 B p
7439-96-5 Manaanese . 0 u p
TIT'l-97-b Mercurv .1 zo u CV
7440-02-0 Nickel 29.0 u p
744a-ag_, Potassium Z0~u B p
7182-49-2 Selenium .. 0 u WN P"
TIT0-72-4 Silver . a u p
7440-23-5 Sorllum l ,90 u p
TITO -'1ll -lJ TnaTiium 2. 0 u P"
7440-62-2 Vanadium Z. 0 u p
TI40-""-!i Zinc I • 7 B p
Cvanide AS
Color Before: COLORLESS I Clarity Before: CLEAR Texture:
Color After: COLORLESS Clarity After: CLEAR Artifacts:
Comments:
FORM l -PAGE 11
FORM I -IN 7/88
INORGANICS CAS~ 18773A I
ffl U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATt
Lab Name: COMPUCHEM LABORATORIES· Contrac ·
SHEET
788 I TR-6-1 I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18160A
R
I Matrix (soil/wa
Level· (low/med) I % Solids:
ter): SOIL Lab Sample IO 296301
n
R
I
I
I
I
I
I
I
I
I
I
I
I
: LOW --
79.0
Con cent ration
l
ICAS No.
7429-90-5
TI4CJ-~-O
7440-38-2
i 140-,9"-3
7 140-41-7
i 140-(:J-9
7 40-70-2
TI4CJ-O-J
7440-48-4
7440-50--S
TI 39-89-6
7439-92-1 143g_;g,,_4
74~~-96-5
TI39-"7-6
7~40-02-0
144lr-og_;7
7782-49-2
744 -2, -4
TI4 -2. -S
744 -2!-0
7 44IT-b2 .. i2
1440-66-6
Color Bel:ore: BROWN
color After: YELLOW
Comments:
FORM 1 -PAGE 7
Date Received 10/19/89
C
Units ( ug/L or mg/kg dry weight):
I I I I I Analyte IConcentra tionlCI Q
Aluminum 2 4:4 0 0 Anti mon-v . 0 B N · Arsenic . 1 B Bari um 4 •. l B E Bervllium . 25 u Cadmium 11.1 N Calcium ) 70 E en romi um 1 . 5 Cobalt . 8 B Conner . 6 5 N* Iron 20 100
Lead 5 . 9 Maanesium 1 :9 3 B ManQanese 8 .8 E Mer cu iv .114
Nickel ( . 5 u Potassium I 140 B Selenium .. 5 u WN sfTver .1 '5 u Sodium 7116 u Thallium .58 B vanarhum 521. 3 E zinc 1n • CVanide • 6 3 u
I
Clarity Before:
Clarity After:
FORM I -IN
18610A INORGANit!S CASE I
MG/K G
I I
I 11 I
p
p
F
p
p
p
p
p
p
p
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p
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AS
Texture: COAR.SE
Artifacts:
7/88
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DAT~ SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 -----
Lab Cod,e: COMPU Case No.: 24520 SAS o.:
CLIENT SAMPLE NO.
I TR-7-1 I
SDG No.: 18160A
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
89.8
.Lab Sample ID: 296302
Date Received: 10/19/89
Concentration Units (ug/L or mg/kg dry weight):
. I I
ICAS No.
7429-90-5
744U-Jo-u
7440-Jll-L
7440-J9-j
7440-41-7
1440-4.l-~
7440-70-
744U-47-J
14QU-Qll-~
7440-50 ·B
14J~-ll~-0
7439-92-1
14J~-9,-4
7439-~0-~
74J9-97-0
7 4 011-11,-u
7440-09-7
I /H,-~:,-,t
7440-22-4
144 -,J-~
744 -28-0
144 -b.t-,
7440-00-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM 1 -PAGE 8
I
I Analyte I I I I IConceritrationJCI Q I Aluminum
Antimony
Arsenic
Barium
Bery1J.ium
caamium
CaJ.cium
encomium
Cooa1t
Co1,.11,.1er
Iron
Leaa
Magnesium
Manganese
Mercury
NicKel
Potassium
Se1enium
Silver
Soa1um
Tna111um
Vanaa1um
zinc
cvan1ae
Clarity Before:
Clarity After:
FORM I -IN
lo, IUU
I,. 0
•'· 0
. I . 0
,ILL
, 1. 9
Q!lU
I. B
:! • 4
. 3
~, '.U
38 '· 9
4 >l
l ,j
.. l
ll '~ , 9
. 4
I
L I~
. ' 4
LL -1 ll
l :B . ,,b
-+
I
u N
s
E
u
N
B E
B
N*
B
E
u
u
B
u WN
u
u
u w
E • u
1861~A INORGANiqS CASE
MG/KG
I I IM I.
p
p
F
p
p
p
p
p
p
p
p
p
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture: COARSE
Artifacts:
7/88
235
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U.S. EPA -CLP
INORGANIC
Lab Nan1e: COMPUCHEM LABORATORIES
l
ANALYSIS DATA SHEET
I Contract: 788 -'-C_:._ __ _
CLIENT SAMPLE NO.
TR-8-1 I I
Lab Cocle: COMPU Case No.: 24520 SAS No.: SDG No.: 18160A
Matrix (soil/water): SOIL
Level (low/med):
\ Solids:
LOW
84.9
Lab Sample ID: 296303
Date Received: 10/19/89
Col
Col
Com
Concentration Units (ug/L or mg/kg rry weight):.
I
ICAS No. I I Analyte I · I I I
1concentrafion1c1 Q
14Z9-90-5 Aluminum 21 100 1440-36-0 Antimony . 2 u N 1440-Ja-Z Arsenic . ' . 5 s 1440-39-3 Barium RI , 2 E 1440-41-7 Berv11ium , 2 3 u 1440-43-9 Caamium . 2 N
1440-70-2 Calcium l 70 E 7< 140.-47-3 cnromium l . 1
140-4R-4 I ' Cobalt . 2 B J• 4O-50-B Coo □er li • 0 N*
I < 39-a~-6 Iron 19 100 7, J9-9Z-l Lead 4 . 6
I• 19-95-4 Maanesium ;21 B
I ' l'l-~o-5 Manaanese 215 E
I , 19-97-6 Mercury .\12 u
I ' 40-02-0 Nickel L I. 3 7. 40-09-7 Potassium 96 B
I R2-49-2 Selenium • i. 3 u WN
I ' ,40-ZZ-4 Silver .16 9 u
I• 4n-23-5 Soaium , 115 u
I ' , 40-ZB-0 Tnalllum • I 16 B 7. 14n-!Ll-Z vanaaium 44 . l E
f, 140-66-6. Zinc 1 .lo *
cvaniae .59 u
I
or Before: BROWN Clarity Before:
or Afl:er: YELLOW Clarity After:
ments::
FORM l. -PAGE 9
FORM I -IN
A NORGANICS CASE
MG/KG
I I
IM I
p
p
F
p
p
p
p
p
p
p
p
p
p
p
CV
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p
F
p
p
F
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AS
Texture: co
Artifacts:
7/88
ARSE.
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Nam<!: COMPUCHEM LABORATORIES Contract: 788
Lab Cod<!: COMPU Case No.: 24520
1---
SAS No.:.
CLIENT SAMPLE NO.
I TR-11-1
SDG No.: 18160A
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
85.4
Lab Sample ID: 296728
Date Received: 10/20/89
Col
Col
Com
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte I Concentration IC I Q IM I
TI29-90~5 Aluminum 15 100 p
7440-36-0 Antimonv . 3 u N p
TI40-38-2 Arsenic 1. o B w F
7440-39-3 Barium 30.4 B E p
TI40-41-7 BervIIium jlJ u p
7440-43-9 Cadmium . 9 N p
TI40-70-2 Calcium , 41 B E p
7440-47-3 Chromium • 1. .8 p
TTTir--U-4 CooaTt I 92 B p
7440-50-8 Cooner 1. 6 u N• p
7439-89-6 Iron 13600 p
TIH-92-1 Lead . 4 F
7439-95-4 Maqnesium ;95 B p
TI39-96-5 Manaanese 5 . 2 E p
7439-97-6 Mercurv ·' 12 u CV
TI<f0-02-0 Ni clce'I 8.8 u p
7440-09-7 Potassium 577 B p
7782-49-2 Selenium ·' 46 u WN F
7440-22-4 Silver .'70 u p
7 440-2 -5 Sodium U8 u p
TI40-?l -0 Thallium ·' 4 I, u F
7440-6;-2 Vanadium 3' . 0 E p
Tr.10-IHi-6 Zinc 5 . 2 • p
Cvanide .158 u AS
or Before: BROWN Clarity Before: Texture: co
or After: YELLOW Clarity After: Artifacts:
ments:
FORM 1 -PAGE 10
FORM I -IN 7/88
J86J0A INORGAN~CS CASE
ARSE
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U.S. EPA -CLP
INORGANIC
Lab Na1ne: COl'IPUCHEl'I LABORATORIES
1
ANALYSIS DATi SHEET
Contract: 788
CLIENT SAMPLE NO.
I TR-9-1 I
Code: COl'IPU Case No.: 24520 SAS No.: SDG No.: 1816 OA Lab
Matr
Leve
ix (soil/water): SOIL Lab Sample ID: 296730
1 (low/med): LOW
% So lids: 87.4
Col
Col
Com
Concentration
I ICAS No.
7429-~u-,
7440-36-0
144U-3tl-,
7440-H-3
7440-41-/
7440-43-9
7qqu-,u-,
7440-47-3
7440-4tl-4
7440-50 ·B
14~:,-tl9-0
7 4 J.9-9 2-l
74H-95-4
7439-~o-~
7439-97-1:1
7440-0 -u
7440-u - I
I I 14-4 -,
74 0-22-4
74 O-l3-~
744u--u
74qu--l
/44U--o
or Be:fore: BROWN
or After: YELLOW
ments:·
FORK l -PAGE 11
Date Received: 10/20/89
Units (ug/L or mg/kg dry weight): MG/KG
: I
. : : I I Analyte IConcentr ation C 0 IM I
Aluminum "' IUU p
Antimony . 2 u N p
Arsenic ILj B F Barium 19.0 E p
BeryJ.J.ium 1. 4j u p
Cadmium l.9 N p
Ca1cium jtl~ B E p
Chromium l . 9 p
Coca1t . " B p
co..,..,er • 6 B N* p
Iron ,1 .uu p
Leaa 4 . q p
Magnesium '>91:1 B p
Manganese ""~ E p
Mercurv .Ill u CV NicKe1 ·1, • I p
Potassium l 110 B p
Se1enium ' .. j u WN F SiJ.ver .69 u p
Sodium , u9 B p
Tna11ium . q~ u F
vanadium , 1., E p
Zinc J. I ' • p
cvaniae ·" u AS
Clarity Before:' Texture: co ARSE
Clarity After: Artifacts:
FORK I -IN 7/88
J8610A INORGANICS CASE I
232
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CDMPUCHEM
lABOMTO :Es
CASE NARRATIVE --SIRRIN
CASE# 245201-18160
CONTRACT#
Sample Numbers: MW12-1S-1,
MW12-4S-1,
ENVIRONMENTAL
7 sl~G# 10160B
MW12-1S-",, MW12-2S-1, MW12-JS-1,
MW12-5S-1
This Case consisted of six (06) soil samples to be
analyzed for complete metals. The samples were received
intact on November 17, 1989 withj Chain of Custody (COC)
Records in order. The enclosed co er page reflects Sirrine
and CompuChem sample identifiers.
The associated quality control sample spike, MW12-2S-1S
/ CCN 303069, was outside the control limits for antimony,
arsenic, cadmium, and selenium. Th~se elements were flagged
with the "N" footnote. The associatled duplicate, MW12-2S-1D
/ CCN 303070, was within the control limits for all elements
tested. ·
A serial dilution was performed on sample MW12-5S-1L /
CCN 303080. The adjusted sample concentrations were within
10% of the original concentrations fbr all of the elements
tested. I '
In one or more of the samples the concentration of
arsenic, barium, calcium, cobalt,I magnesium, and silver
were between the Instrument Detection Limit (IDL) and the
contract Required Detection Llmit (CRDL). The
concentrations of aluminum, chromium I iron, lead, manganese,
vanadium, and zinc were above the CRDL, while the
concentrations of the remaining e ements fell below the
( IDL) .
Note:
~~tl~ Betty J. Andershock
Technical Reviewer
January 27, 1990
This report is paginated for reference and account-
ability in decreasing numeric 11 sequence.
COMPU_CHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/ Nelson Highway Rleaearch Triangle Park. NC 27709 (9191 :•9-8263
' .> I ~ . .
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Lab Name: COMPUCHEM
Lab Code: COMPU
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
LABORATORIES Contract: 788 -----
case NO.: 24520 SAS No.:
CLIENT SAMPLE NO.
I MW12-2S-l I
SDG No.: 18160B
Matrix ( soil/water) :
Level (low/med):
SOIL
LOW
Lab Sample ID: 303068
Date Received: 11/17/89
% Solids: 87.1
Concentration Units (ug/L or mg/kg dry weight):
I I CAS No ..
I
I Analyte I I I I JConcentrationJCI Q I 14 l.':l-':IU-~ Aluminum .. ltl~U 7440-36-U Antimony 6 '· Z u N 1440-Js-Z Arsenic • It, B N 7 ,40-3 -3 Barium 10 . 3 B
I ,4U-4 -7 Be rv Lll um ' .. .j u 7 ,40-4 -':I Cadmium l'.l u N /44U-/U-Z Calcium J.4'.4 B 7440-47-3 Chromium B,B
144U-4S-4 Cooa1t HU B 7440,--B Coooer . 9 B
{43:,--e Iron 0 IQU
74J':I--l Lead '4 7439-95-4 Mac:inesium 106 B /4J':l-~o-~ Manganese J.~\L 74H-97-6 Mercurv .10 u /44U-UL-U N1CKeJ. S \ I u 7440-09-7 Potassium l . 6 u 77Sl-4':l-l Selenium . ,b u WN
7 ,40-Z -4 Silver . ,9 u
7• ,40-Z -~ Sodium L .6 u / ,4U-l -U ThaJ.uum • Qt, u 7440-62-2 vanadium 17! 6 /44U-bb-b z1nc ':I " cvanide 7 u
Col
Col
Com
or Before: RED Clarity Before:
or After: COLORLESS Clarity After:
ments:
FORM l. -PAGE l
FORM I -IN
18168B INORGANICS PACKAGE
.. • ..... .,,, -' ,..., f I -: ., l-,i ..... • • • . . l◄ l l .... -.. _, z:::.
MG/KG
I I IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
Ii'
CV
p
p
P'
p
p
P'
p
p
AS
Texture: FI
Artifacts:
7/88
NE
195
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA HE:E:T
Lab Name: COMPUCHE:M LABORATORIES Contract: 788 -'--'----
CLIENT SAMPLE: NO.
I MW12-3S-l I
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med): LOW
SAS N SDG No.: 18160B
Lab Sample ID: 303076
Date Received: 11/17/89
% Solids: 78.7
Col
Col
Com
· Concentration Units (ug/L or mg/kg d y weight):
I
ICAS No. I Analyte IConcentrat 1ionlCI Q I /4 19-90-5 Aluminum 76 o
74 10-11;-0 Antimony 6 • g u N 14 10-38-2 Arsenic . , .. B N /440-J -3 Barium 2G I. B 7440-4 -7 Berv~lium • ·2 u
1440-4-9 Cadmium 11-u N 1440-70-2 Calcium 6S . 7 B /440-47-3 Chromium zc • 9 1440-4A-4 Cooa1t . a B 1440-50-8 Conner 2 • B 14 H-89-6 Iron 6 :4 □ 14.>9-92-1 Lead 51. 3
/4.J9-95-4 Maqnesium 3:44 B
/4.>9-\:I0-5 Manaanese ZB . 0
74jlif-"11-6 Mercury . 1 u /440-01-0 Nickel C . 7 u
744 □-u~-7 Potassium I i 1 B ttd2-49-2 Selenium , 1. 5 u WN
7440-22-4 Silver .176 u /440-2 -5 Sodium 2139 u
7440-' -o Thallium • ~ 1 u /440-6 -2 Vanadium 181. 7 7440-ftft-!, z1nc 91. 4
cvanide .,64 u
I
or Before: YELLOW Clarity Before:
or After: COLORLESS Clarity After:
ments:
FORM 1 -PAGE 2
FORM I -IN
.
• 181608 INORGANICS PACKAGE
MG/KG
IM I
p
p
r
p
p
p
p
p
p
p
p
r
p
p
CV
p
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F
p
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AS
Texture: ME DIUM
Artifacts:
7/88
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U.S. EPA -CLP
INORGANIC
l CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
ANALYSIS DAT1 SHEET
Contrac : ~7~8~8 ___ _
MW12-1S-l I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18160B
Matrix (soil/water): SOIL
Level (low/med): LOW
% Solids.: 90.2
Lab Sample ID: 303077
Date R•ceived: 11/17/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Col
Col
Com
ICAS No.
7429-90-5
/440-36-0
7< 40-•"-2
/ I 40-39-3
1<40-41-7
/440-43-9
1440-70-2
1440-47-3
144 -48-4
I< ,4 -~u-8
I 3 i-89-6
I 3~-92-1
I 39-95-4
1439-~o-5
1439-97-6
I 40-02-0
I 40-09-7
I 82-49-2
7 40-22-
I 40-23-'
7• 140-28-
I 40-62-2
7440-oo-6
or Before: RED
or After: COLORLESS
ments:
FORM l -PAGE 3
I Analyte IConcentrationlCI O I IM I
Aluminum <]BBQ p
Antimonv 6. 0 u N p
Arsenic 1. 2 B N F Barium a.a B p
BerylJ.ium 1. 22 u p
Cadmium 11.1 u N p
CaJ.cium ' !14 . .l B p
Chromium 6. 3 p
Collalt • 6 B p
Conner •. 6 u p
Iron , • 3 o p
Lead 3. 7 F Maanesium 150 B p
Manaanese ~ ~. 7 p
Mercury .11 u CV Nickel :~. 4 u p
Potassium 31 u p
Selenium . 4 4 u WN F
Silver . 67 u p
Sodium .oa u p
Tna11ium .44 u ,
vanadium 2 :~. 2 p
Zinc ~. 6 p
cvan1de . 55 u AS
Clarity Before: Texture: FI NE
Clarity After: Artifacts:
FORM I -IN 7/88
I
181608 INORGANICS PACKAGE 193
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U .·S. EPA -CLP
1 .
INORGANIC ANALYSIS DA A SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES ContraJt, 788 -----
MW12-1S-2 I I
Lab Code: COMPU Case No.: 24520 · SAS No.: SDG No.: 18160B
Matrix (soil/water):· SOIL Lab Sample ID: 303078
Level (low/med): LOW Date Received: 11/17/89
% Solids: 89.3
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Col
Col
Com
ICAS No. I Analyte IConcentrationlCI Q I 74l9-,:,u-, Aluminum ,10u
744u-,o-u Antimonv o.u u N 7440-JB-l Arsenic 1.l B N 7440-J,,-J Barium LO B 7440-41-1 Bery.1.1ium 1.u. u 7440-43-9 Cadmium ll.l u N /44U-IU-l Ca.1cium j .l . ~ B 7440-47-j cnromium I!> . 7 7440-48-4 Cooa.1t IL" B /44U-,O-tl Copper 11.0 u 7439-89-6 Iron 98lu
74J9-9l-.l Leaa IJ. I 7439-15-4 Magnesium 150 B 74H-16-, Manqanese ,, . 4
14J"-'1-0 Mercury . .l .l u
7440-02-0 Nicke.1 18., u
7440-09-1 Potassium ll Jl u 71t12-4,,-l Se.1enium 1-4 5 u WN 7440-l2-4 Silver I. " I B 7440-,J-~ Soaium ILll u
744U-l!I-U Tna.1.1ium 1-4~ u
7440-62-2 vanaaium ,:4.
1440-ob-l! Zinc .l.U •
cvaniae 1-, u
I
or Before: RED Clarity Before:
or After: COLORLESS Clarity After:
ments:
FORM 1 -PAGE 4
FORM I -IN
181608 INORGANICS PACKAGE
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture: FI
Artifacts:
7/88
NE
192
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U.S. EPA -CLP
INORGANIC
1
ANALYSIS DA ( SHEET
CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
74.5
Contract: 788 c....:;..::..._ __ _
MW12-4S-l I
SAS No.: SDG No.: 18160B
Lab Sample ID: 303079
Date Received: 11/17/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte 1concentrrtion1c1 Q IM I'
14,9-90-5 Aluminum 8990 p
/440-36-0 Antimonv I 7. 2 u N p
/440-38-2 Arsenic .54 u WN F /440-39-3 Barium 27.9 B p
1440-41-7 Berv11ium . 76 B p
74•0-43-9 Cadmium l.3 u N p
/440-70-2 Calcium . 5 B p 7440-47-3 cnromium . 0 p
/440-48-4 Cobalt . a B p
7< 40-">0-B Copper 1.9 u p
H H-89-6 Iron ':uo p
7 < 3 -92-l Lead . 0. o F
/lj -95-4 Maanesium I 4 58 B p
/43 -96-5 Manaanese 3 5. 4 p
/4J'l-97-6 Mercury I .12 u CV /440-02-0 Nickel ~0.2 u p
1440-09-7 Potassium 1583 B p
t/62-49-2 Selenium 12. 7 u WN F 1440-22-4 Silver 1. 81 u p
/440-23-5 Sodium 12-,2 u p
1440-28-0 Tna.11ium 1. 54 u F /'140-62-2 Vanadium 19. 5 B p
1440-66-6 zinc 210. 6 p
cvanide .f>7 u AS
I
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or Before: YELLOW Clarity Before: Texture: ME DIUM
or After: COLORLESS Clarity After: Artifacts:
ments:
FORM 1 -PAGE 5
FORM I -IN 7/88
160B INOR GAHICS PACKAGE
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA S EET
I Lab Name: COMPUCHEM LABORATORIES Contract: rf_8_8 ___ _
Lab Code: COMPU Case No.: 24520 SAS No
CLIENT SAMPLE NO.
I MW12-5S-l I
SDG No.: 181608
Matrix ( SClil/water): SOIL
Level (low/med):
% Solids:
LOW
77.8
Lab Sample ID: 303080
Date Received: 11/17/89
Col
Col
Com
Concentration Units (ug/L or mg/kg dry weight): . I .
I
ICAS No. I I I I Analyte 1concentrati1n1c1 Q
14..:~-~0-5 Aluminum 1u,uo 1440-30-0 Antimony 6. 9, u N 1440--z Arsenic . 511 u WN /44U--j Barium j 4. II B 7440-• -7 Beryllium l. l B 1440-43-9 Cadmium l. I u N 1440-IU-..: Calcium o o. , I B 7440-47-3 Chromium 4. 11 /440-1:5-4 Coca1t ,. Ll B 7440-10-8 Copper l.B u /4j!:l-,1~-I) Iron t!J~u 743 -12-1 Lead 8. 3 14 3 -1:,-4 MaQnesium 4vo B
/ 4 j -,0-:, Manganese 4:,. t5 7439-'7-6 Mercury . l J u 144U-JL-U NicKel ~-8 u 1440-)9-7 Potassium o 4:, B 711:1..:-,9-..: Selenium ..: . 6 u WN 7440-,2-4 Silver . 7 I u l4•v-j-:, Sooium ..:4z u 7440-~8-o Thallium . :, l u w
144U-02-..: Vanaoium ~l. 3 B 74 4 o-oe-e z1nc ..:11. j I
1,;vanioe • 6 4 I u
I
or Before: YELLOW Clarity Before:
or After: COLORLESS Clarity After:
ments:
FORM l -PAGE 6
FORM I -IN
MG/KG
I .IM
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
AS
Texture: ME
Artifacts:
7/88
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CDMPUCHENi1
lABORATORJES
I INORGANIC CASE SUMMARY 1ARRATIVE CASE# 24520 SDG# 18 60C
CONTRACT# 787
SAMPLE NUMBERS: SB-lR, TAP]l, TB-4
This portion of case 24520 was r ceived in good
,:::ondi tion with the appropriate chain-d,f-custody documents,
on November 17, 1989. The SDG consists of three water
samples for the analysis of complete ~SL metals and cyanide.
'.rhe enclosed cover page reflects both Sirrine Environmental
and CompuChem Sample Identifiers.
The associated quality control sample spike, SB-lRS, was
within the control limits for all of _the analytes. The
associated quality control sample spik'e for cyanide, TAP-lS,
was within the control limits ·for cyanlide. The associated
quality control duplicate, SB-lRD, was outside the control
limit mercury, therefore the value was flagged with an'*'
in all of the samples. The associated quality control
duplicate for cyanide, TAP-lD, was within the control limit
for cyanide. I-
A serial dilution was done on sample TAP-lL.
adjusted sample concentration of mangahese was not
1.0% of its original value, therefore tpe value was
The
within
flagged
r,rith an 'E', in all of the samples. [
The concentrations of arsenic, calcium, magnesium,
potassium-and vanadium fell between the Instrument Detection
Limits (IDLs) and the Contract Require? Detection Limits
(CRDLs) in the majority of the samples. The concentrations
of aluminum, copper, iron, lead, manganges, sodium, and
zinc were-above the CRDL, while the remaining analytes had
concentrations below the IDL. I
Release of the data contained in this hard copy data
package has been authorized by the Lab6ratory Manager or his
designee, as verified by the following Is· gnaturer.·,.,..,.,...,_
Note: This report is paginated for re erence and
accountability in decreasing numerical sequence.
Page -1
COM PUC HEM L',BORA TORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 {919) 549-8283 I .
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IJ. S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC
Lab Name: COMPUCHEM LABORATORIES
ANALYSIS DATA IHEET
Contract: 1~7~8~8 ___ _ I TAP-1 I
Lab Code: COMPU Case No.: 24520 SAS No.: SOG No.: 18160C
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 303015 ;
Date Received: 11/17/89
Concentration Units (ug/L or mg/kg d y weight): I . UG/L
ICAS No. I Analyte I Concentratilon IC I Q
I IM I
7429-~u-5 Aluminum q9710 p
744U-,c-U Antimony L7 ,10 u p
7440-38-2 Arsenic 2 ,17 B w f'
744U-.l9-.l Barium L ,I B p
7440-41-7 Bervllium . ' u p
7440-43-9 Cadmium u p
7440-70-l Calcium B<l B p
7440-47-3 Chromium 6. u p
7440-48-4 Cobalt '·· u p
74qu-~u-8 Cooner L 9. 6 p
7439-89-6 Iron 2470 p
7439-92-1 Lead .r. a f'
7439-95-4 Maanesium 323 B p
7439-96-5 Manaanese ,!IT E p
74,:,-~/-o Mercury .20 u • CV
7440-02-0 Nickel 38. a U· p
7440-09-7 Potassium 1870 B p
7782-49-2 Selenium Tir .ll" u w F
7440-L:l-4 Silver 3. 0 u p
7440-23-5 Sodium 200000 p
7440-26-0 Thallium 2.0 u F
7440-62-2 vanaaium 4.6 B p
7440-66-6 Zinc 2~R p
Cvaniae 10.0 u AS
I
Color Before: COLORLESS I Clarity Before: CLEAR Texture:
Color After: COLORLESS I Clarity After: CLEAR Artifacts:
I Comments:
FORM l -PAGE 1
f'ORft I -IN 7/88
18160C INORGANifS CASE 162
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1.l.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Namu: COMPUCHEM LABORATORIES Contract: 788 I.:...::.:: __ _ I SB-lR I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18160C
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 303022
Date Received: 11/17/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No. I Analyte IConcentraJionlCI
I 0 IM I .
74:l'l-'IU-~ Aluminum 1!6 4 B p
7440-36-0 Antimony L71.ll" u p
7440-38-l Arsenic ,1. 9 B F 7440-39-3 Barium -r:1.1 B p
7440-41-7 Bervl1ium. , 1. 6 B p
7440-43-9 Cadmium s1. n u p
744 -70-Calcium 5179 B p
744 -47-Chromium 61. 0 u p
744 -48-Cotlalt 31. 0 u p
744u-~u-8 Conner 281. 4 p
7 4 39-69-o Iron 3U p
7439-92-1 Lead l'.9 B F
7439-95-4 Maqnesium 183 B p
7439-16-5 Manganese uo u E p
7439-7-6 Mercury . 2 <r u • CV 744 --u Nic1<e1 111 l 0 u p
744 --7 Potassium TTI1r B p
7 "'· --2 Selenium 2!0 u F
744 -J -Silver 3 ! 0 u p
744 -2 _, Sodium 142000 p
744 -LI -Tna11ium 2 JO u F
7440-62-2 Vanadium -., !l!" B p
7440-oo-6 Zinc 26!8 p
cvanide T1l" ill" u AS
I
Color Before: COLORLESS Clarity Before: Texture:
Color After: COLORLESS Clarity After: Artifacts:
Comments:
FORM l -PAGE 2
FORM I -IN 7/88
C NORGRNICS CASE 161
g
0
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rJ.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I _;:_;; __ _ I TB-4 I
Lab Code: COMPU .Case No. : 24520 SAS o.: SDG No.: 18160C
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 303023
Date Received: 11/17/89
Concentration Units (ug/L or mg/kg dry weight):
I UG/L
ICAS No. I Analyte I Concentra~ion IC I O
I
IM I
7429-90-5 Aluminum 611• 3 B p
7440-,~-o Antimony n, .7l u p
7440-38-2 Arsenic 2.0 u r
7440-39-3 Barium I!. O u p
7440-41-7 Bervllium 11. 0 u p
7440-43-9 Cadmium --s:.7l u p
7440-/U-.l Calcium l 71. 0 u p
7440-47-3 Chromium li1.7l u p
7440,-48-4 Cobalt ll. 0 u p
7440-50-8 Cooner 71. 0 u p
7439-89-6 Iron 2 51. l B p
7439-92-1 Lead l I. 0 u. r
74~~-95-4 Maqnesium 5~ 1. 0 u p
/4j~-96-5 Manganese l I. 0 u E p
74H-97-6 Mercury .,:ro u • CV
7440-U.l-U Nickel 381. 0 u p
7440-09-7 Potassium 70"J B p
7782-49-2 Selenium 21. 0 u w r
· 7440-22-4 Silver 31. D u p
7440-23-5 Sodium 940 u p
7440-28-0 Thalllum 2 0 u r
7440-62-2 Vanadium 2 0 u p
.7440-66-6 Zinc 8 <j B p
Cyanide 10 0 u AS
Color Before: COLORLESS Clarity Before: CLEAR Texture:
Color After: COLORLESS Clarity After: I CLEAR Artifacts:
Comments: I FORM l -PAGE 3
FORM I -IN 7/88
18160C INORGANJCS CASE 160
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CDMPUCHENl1
lABOPATORIES
I INORGANIC CASE SUMMARY NARRATIVE
CASE#2452O SDG#l82~0A
CONTRACT# 787 I
SAMPLE NUMBERS: 9168TB3-l
. h. · i Tis case consisted of one sampl[ to be analyzed for
complete HSL metals and cy. anide. The sample were received
intact on October 23, 1989 with Chain of custody (COC)
Records in order. The enclosed cover page reflects both
Sirrine and CompuChem sample identifiers.
h . i· I . Te associated qua ity control s?mple spike, 9168TB3-
1S, was not within the control limit for selenium, therefore
the value was flagged with an 'N'. The associated
duplicate, 9168TB3-1D, was within thelcontrol limits for all
of the analytes. ·
A serial dilution was performed n sample 9168TB3-1L.
The adjusted sample concentrations of]all of the analytes
were within 10% of their original concentrations.
Th t . f . bl . . . d . e concen rations o arsenic, arium, iron, an zinc
fell between the instrument detection]limits and the
contract required detection limits. he concentrations of
the remaining analytes fell below the IDL.
Release of the data contained in this hard copy data
package has been authorized by the La oratory Manager or his
designee, as verified by the followinl signature.
'-~ C ,.,t;l /J l/·Y}
nne C! Alston -
. echnicai Reviewer
. . . d f If . d Note: This report is paginate or r~ erence an
accountability in decreasing numerica sequence.
Page - 1
COMPUCHEM LABORATORIES. INC. P.O. Box 12652 3306Chapel Hill/Nelson Highway RI rch Triangle Park. NC 27709 [phone]
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U.S. EPA -,CLP
INORGANIC
l
ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES I Contract: 788 I 9168TB3-l
Lab Code: COMPU Case No.:
I----
24s20 SAS No.: SDG No.: 18210A
Matrix (soil/water): WATER
Level (low/med):
\ Solids:
LOW
a.a
Lab Sample ID: 297270
Date Received: 10/23/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
74 ~-90-~ 14 u-Jo-u
74 0-38-Z
744U-j~-j
744u-4l-7
74~u-4j-~
7440-70-Z
14~u-4/-j
7440-48-4
1440-,u-11
7439-11~-6
74H-9Z-l
14~~-~,-4
74~:,-:,o-,
7439-111-0
744U-OZ-U
7440-u ~-I
77112-4 9-Z
144 -,t,-'-4
744 -Z3-,
/4~ --'11-U
7440-6Z-Z
/ 4 4 u-00-11
Color Before: COLORLESS
Color Al:ter: COL01!LESS
Comments:
FORM l -PAGE l
I Analyte IConcentr1tionlCI I A1uminum l7. u
Antimonv ,t, I. U
Arsenic I z. 5
Barium I , • u
Berv1iium 11.0
Caamium 1~.u
Calcium 17.0
Cnromium 10. U
Co0a1t I J. o Couoer I I . U
Iron 115.,
Leaa 11.u
Magnesium ~:o. u Manganese 11.u Mercury 1-2u Nickel j' LU
Potassium ,91
Selenium · . .:.u
Si1ver t3 • u soa1um ~4U
Tna11ium z.u
Vanaa1um ,I,. u
zinc Z. I
.. van1ae .1 U. U
I
I Clarity Before: CLEAR
I Clarity After: CLEAR
I
FORM I -IN ·
u
u
B
B
u
u
u
u
u
u
B
u
u
u
u u
u
u
u
u u
u
B
u
0
WN
-. •-------·. ------· ---
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
t'
CV
p
p
F
p
p
F
p
p
AS
Texture:
Artifacts:
7/88
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CDMPUCHEM
lABOMTORlE:s
Case Narrative l
Sirrine Environment 1
Case# 24520 SDG # 18210B
Contract# 788
Samples: 9168TR101, 9168TR121
This case consisted of two soil sam_les analyzed for TAL
metals. The samples were received intact on October 23, 1989
with the Chain-of-Custody (COC) Record'. The enclosed cover
page reflects Sirrine Environmental and CompuChem sample
identifiers.
The associated quality control sample spike, 9168TR101S, was
outside the control limits for antimony, arsenic, selenium, and
cyanide, therefore the concentrations wee flagged with an 'N'.
Please refer to the enclosed laboratory notice concerning the
post digestion spike for cyanide. Thelduplicate, 9168TR101D,
was outside the control limits for alu,inum, calcium, copper,
lead, and cyanide~ therefore the concentrations were flagged
with an '*' I
Method of Standard Addition (MSA) was done for arsenic in
sample 9168TR121, and the concentration was flagged with an
, s, . j
A serial dilution was done on .sample 9 68TR121. The adjusted
sample concentrations were within ]0% of the original
concentrations for all of the elements t~sted.
I In both of the samples, the concentrations of analytes fell
between, below, and above the InstrJment Detection Limits
(IDLs) and the Contract Required Detectidn Limits (CRDLs).
/20011 JilJrµ Anna Feather
Technical Reviewer
December 31, 1989
Note: This report is ~aginated ~or refer1ence and
accountability in decreasing numerical sequence.
COMPUCHEM LABO RA TORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway R aaarch Triangle Park, NC 27709 (919) 5•9-8263
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LABORATORY NOTICE
SDG: 18210B
SAMPLE ID:297261
The EPA sow 788 states that when the pre-distillation
spike recovery exceeds the control limits and the sample
results are less than 4x spike added ,then a post-
distillation spike is needed. This spike must be 2x the
CRDL or 2x the indigenous value whichever is larger.
The cyanide sample needed a spike at 2x it's value, but
this was not done during the time of analxsis. It was spiked
at 2x CRDL as indicated. on the raw data. Due to the fact that
the holding times for the sample expired 'nd the sample i~ no
'longer available, reanalysis was not done.
~------,-,...,<;. ~ . Id Lin a Jones
Ch~mist III
December 30, 1989
QA i ___ _
lNORGRNlCS CRSE 182018 l 6'1
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract. 788
Lab Code: COMPU Case No.: 24520
1---
SAS No.:
CLIENT SAMPLE NO. I 9168TR101 I
SDG No.: 18210B
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
85.9
Lab Sample ID: 297261
Date Received: 10/23/89
Col
Col
Com
Concentration Units (ug/L or mg/kg dry weight): MG/KG . . I
. . . I
JCAS No. I Analyte IConcentrationJCI Q IM I , I
/4l9-90-5 Aluminum 6230 • p
7qq0-36-0 Antimony 6:. 3 u N p
/4Q0-38-2 Arsenic 11. 7 B N F /qq0-39-3 Barium HI. 7 B p
/4'10-41-7 Bervl1ium .12 3 u p
7440-43-9 Cadmium l I. 2 u p
/440-70-2 Calcium 4 5100 • p
7440-47-3 Chromium 111. 3 p
/4'10-4H-4 CoOalt 21. 3 B p
/qq0-50-8 Coooer 1 71. 6 • p
/439-89-6 Iron 131:0 o p
/439-92-1 Lead 331.4 • p
7439-95-4 Maqnesium 206 B p
/439-96-5 Manaanese 391. 5 p
7439-97-o Mercury o.~1 u CV
/Q'I0-02-0 Nickel 8 . 8. u p
74 10-09-7 Potassium 1' !A u p
I I 7-49-2 Selenium • ,Hi u WN F /4 10-22-4 Silver 0 I 0 u p
7440--Soa1um .. 219 u p
/4'10-. -1 Thallium . ~6 u F /Q40--Vanadium 3 7 '· 4 p
/440-66-6 zinc 27 '· 2 p
Cvan1de 22 '· 4 N* AS
I
or Bef'ore: BROWN Clarity Before: Texture: co
or Aft.er: YELLOW Clarity After: Artifacts:
ments:
FORM 1 -PAGE l
FORM I -IN 7/88
I GA CS C
ARSE
158
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
IIW3-1-1 Lab Name: COMPUCHEM LABORATORIES Contract: 788 I -----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Leve 1 ( 1 ow/med) :
% Solids:
LOW
0.0
Concentration
ICAS No.
/4l':l-':IU-o
7441-36-0
/44U-j6-l
744 -39-3
/44 -41-/ ·
744 -43-9
7440-70-Z
/44U-4/-j
7440-48-4
/44U-o0-ll
7439-89-6
/4j':l-9Z-l
/4.l9-1: -4
74H-,, -,
/4j':I-, -o
7440-02-0
/440-u,,-/
I /112-4':I-Z
/44U-lZ-4
74q0-Z3-5
744U-l6-0
1440-0..:-2
14~u-bb-O
Color Beftlre: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE 12
Lab Sample ID: 310361
Date Received: 12/21/89
Units (ug/L or mg/kg dry weight): UG/L . I .
I I Analyte IConcentrationlCI O IM I
I Aluminum ""lO * p Antimony · ZllO u p
Arsenic j l 0 u WN F Barium 307 p Bery11ium j I l B p
Cadmium 5 l 0 u * p Calcium l3lU B p
Cnromium 4 / ! fj * p
Cobalt 5 ! 3 B p Coooer l> .1l p
Iron 20900 p
Lead o .1 s w F Maanesium l ':14 u B p
Manaanese JZ p
Mercury • l· u CV Nickel Z9 -10 u p
Potassium l jllU B p
Selenium l ., u N F Si1ver ., u p
Sodium l ,Z B p
Tna1uum l. u I" Vanadium J3.' B p
Zinc 75.2 p
Cvanide 10.0 u AS
I
Clarity Before: 1:exture:
Clarity After:
CLOUbY
I CLEAR Artifacts:
I
FORM I -IN 7/88
INORGANICS CASE 18773A I
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U.S. EPA -CLP
INORGANIC CLIENT SAMPLE: NO. l
ANALYSIS DATA [HE:E:T
Lab Name, COMPUCHEM LABORATORIES I MW4-l-l I Contract: 788 -----
Lab Code: COMPU Case No.: 24520 SAS N .: SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
. % Solids:
LOW
0.0
Lab Sample ID: 311196
Date Received: 12/22/89
Concentration Units (ug/L or mg/kg dry weight): UG/L
I
ICAS No.
7429-90-5
I 44U-jt,-U.
7440-38-Z
744U-j~-j
744U-4l-1
7440-43-9
144U-10-Z
7440-47-j
7440-48-4
74 o-,u-1:1
74 9-"\1-6
14 ~-~l-l
7439-95-4
14J~-\IO-~
7439-\lt-6
144U-Ul-U
7440-U\l-7
I 10,i.-~7-J.
7440-22-4
I U-J.j-,
7 0-28-
7 o-oz-
/44U-oo-
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM 1 -PAGE 13
I Analyte IConcentratJonlCI Q
I IM I
AJ.uminum 24luu
Antimony ,1. i .1u
Arsen1c J .10
Barium jb,i
BeryJ.J.ium l .14
Caamium 5 .1u
Calcium ,~u,o
Cnromium ,I. j .10
Co0a1t l l .ll Couuer 4 /. :o Iron ~000:0 Leaa i~ .. ~
Magnesium IU\l,U
Manganese l:S i 11 Mercury .lU NlCKei l~.U
Potassium ,1, J
Selenium l u. ,
Silver 4 . I
Soa1um l:S, jU
TnaJ.J.ium l.O
vanacaum I I.~
zinc 14~
Cvaniae lU.O
I
I Clarity Before: CLOUDY
I Clarity After: CLEAR
I
FORM I -IN
I NORGRN I C:_5 CAS I ' I
• p
u p
u N F
p
B p
u • p
p • p
B p
p
p
F
p
p
u CV
u p
p
u WN F
u p
p
u F
p
p
u AS
Texture:
Artifacts:
7/88
18773A 204
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: ~7~8~8 ___ _
I
I PB-1 I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med):
\ Solids:
LOW
0. 0
Lab Sample ID: .311198
Date Received: 12/23/89
Concentration Units (ug/L or mg/kg ry weight):
. I UG/L
ICAS No.
7429-90-5
7440-36-0
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440~48-4
7440-50-B
7439-89-6
7439-9Z-l
7439-95-4
7439-96-5
7440-0Z-0
7440-09-7
t/8Z-49-Z
7440-ZZ-4
7440-23-5
7440-28-0
74~0-c,c,-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 14
I Analyte I ConcentraJion IC I Q
I Aluminum
Antimony
Arsenic
Barium
Berv11ium
Cadmium
Calcium
Chromium
Cobalt
Coooer
Iron
Lead
Maqnesium
Manoanese
Mercurv
Nickel
Potassium
Selenium
Silver
Thallium
vanaa1um
Cvan1ae 10!0 U
I Clarity Before: CLEAR
I Clarity After: CLEAR
I
FORM I -IN
IM I
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AS
Texture:
Artifacts:
7/88
IN6RGRNICS CA~E 18773A 203
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
TB-4 I Lab Name: COMPUCHEM LABORATORIES Contract: _7_8_8 ___ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 18773A
Matrix (soil/water): WATER
Level (low/med) : LOW
% Solids: 0.0
Lab Sample ID: 310716
Date Received: 12/22/89
Concentration units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7 4 2<1"-90-7>
7440-36-0
iTIO-JS-2
7440-39-3
iTIO-IT-7
7440-43-9
iTIO-T0-2
7440-47-3
iT40--U-4
7440-~u-B
i4J9--lflJ-6
7439-92-1
7 4 .f9 ---g--., -4
TTH-96-5
7 4--,-g_g 7-7,
TT4U-02-0
7440-09-7
TT82-4, -2
744 -2. -4
144 -2, -5
744 -2!-0
iT40-e2-Z
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM 1 -PAGE 15
I Analyte IConcentrationlCI Q I IM I
ALuminum ,6.0 u • p Antimonv 21. 0 u p
Arsenic 13. o u N F Barium 11.0 u p
Bervllium 11. u p
Cadmium 15 . u • p
Calcium ~7. u p
Chromium 15 .. 0 u • p
coEa--rt l.l.O u p
Coooer 14. 0 u p Iron 17 .1 8 p
Lead . 12. 0 u F Maanesium '>,6 • 0 u p
Manaanese 11.0 u p
Mercurv 1. 20 u CV Nickel 29.0 u p
Potassium l·Z60 u p
Selenium 2. 0 u N F Silver ,4. 0 u p
Sodium 14'1U u p
Thallium 2.0 u F Vanadium 2. 0 u p
Zinc Z.2 B p
Cvanide 10.0 u AS
I
I Clarity Before: CLEAR Texture:
I Clarity After: CLEAR Artifacts:
I
FORM I -IN
INORGANICS CASE 18773A
I
7/88
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Sample Numbers:
COMPUCH[M
lABORATORlES
I CASE NARRATIVE--CASE# 20937
Contract# 2-88 (REVS) SDG# 05
CompuChem Laboratories, \Inc.
MW13-7S-1, MW14-2S-l, MW16-2S-1, SBl-1-1, SBl-2-1,
SB2-l-l, SB2-2-l, SB3-l-1, S83-2-l
Case# 20937, SDG# 05 consisted of 9 soil samples for volatile and
semivolatile analysis. The samples were rec~ived intact on 7-21-90,
7-25-90, and 7-27-90 in properly sealed I shipping containers with
chain-of-custody documents. The pH values of\ ·the samples were within
the range specified in EPA protocols. Moisture content of the samples
ranged from 7% to 24%.
VOLATILES:
All volatile fractions were initially. analyzed within holding time
requirements. Sample S83-2-l required reanalysis which could not be
performed within the holding time requirements. TCL compounds were
present in all samples, some of which were also present at acceptable
levels in the associated method blanks. Non~ of the samples contained
any tentatively identified compounds. All sufrogate recovery criteria
were met. The QC matrix spike/matrix spike duplicate re·sults were
acceptable.
SEMIVOLATILES:
All semivolatile fractions were extracted and analyzed within holding
time requirements. Five of the samples contailned TCL compounds. All
samples contained tentatively identified comii
1
ounds, some of which were
attributable to solvent contaminants or aldol condensation. All
surrogate recovery criteria were met. The QC lnatrix spike/matrix spike
duplicat,~ results were acceptable. The repoveries of phenol and
2,4-dinitrotoluene exceeded QC limits in the MSD.
I I certify that this data package is in compliance with the terms and
conditions of the contract, both technically ahd for completeness, for
other than the conditions detailed above.\ Release of the data
contained in this hardcopy data package has been authorized by the
Laboratory Manager or his des°ignee, as v~rified by the following
signature.
Note: This report was paginated for reference and accountability in
decreasing numerical sequence.
Sr. Quality Assurance
8-24-90
Specialist
COMPUCHEM LABORATORIES. INC. P.O. Box 1_2652 3308 Chapel Hill/Nelson Highway Reiarch Triangle _Park, NC 27709 [phone] / () 6
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VOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-7S-l Lab Name: COMPUCHEM,RTP Contract: C2-88l-REVS
Lab Code: COMPU Casa No.: 20937 SAS No.: SDG No. : ~os __
Matrix: ( soil/water) SOIL Lab Sample ID: .,.J..,_5.,._8.._l,,_35.,_ __ _
Sample wt:/vol: s,o (g/mL) ~ Lab Fila ID: GH058135Cll
Leval: (low/mad) LOW
t Moisture: not dee. ---2.Q
Data Received: 07/21/90
Data Analyzed: 07/J0/90
Dilution Factor: .._1~,o.__ __ Column: (pack/cap) CAP
CA.S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethana
74-83-9-------~-Bromomethana
75-01-4---------Vinyl Chloride
75-00-3---------Chloroathana
75-09-2---------Mathylana Chloride
67-64-1---------Acetona
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroathena
75-34-3----~----l,l-Dichloroathana
540-59-0--------1,2-oichloroathena (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroathana
78-93-3---------2-Butanona
71-55-6--------1,1,1-Trichloroethana
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromathana
78-87-5---------1,2-0ichloropropana
10061-0l-S------cis-l,3-Dichloropropana
79-O1-6---------Trichloroathana
124-48-1--------Dibromochloromethana
79-oo-s---------1,1,2-Trichloroethana
71-43-2---------Banzena
10061-02-6------Trans-l,3-Dichloropropana __
75-25-2---------Bromoform
1oa-1O-1--------4-Mathyl-2-Pantanona
591-78-6--------2-Haxanona
127-18-4--------Tatrachloroathana
79-34-5---------1,1,2,2-Tetrachloroethana __
1O0-aa-J--------Toluana
108-90-7--------Chlorobenzena
1OO-41-4--------Ethylbanzena
1OO-42-s--------styrana
1330-20-7-------Total Xylanas
Q
12 u
12 u
12 u
12 u
6 BJ
19 B
6 u
6 u
6 u
6 u
6 u
6 u
12 u
6 u
6 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
12 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA 1/87 Rav.
20937 05 SAMPLE DATA SUMMARY
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u. EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
HW13-7S-l
Lab NamEl: COMPUCHEM.RTP contract: c2-aa1-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: S 0G No , : .,._o 5"'---
Matrix: (soil/water) SOIL Lab Sample IO: . .,._J.,._58,._l._J._,5.__ __ _
sample wt/vol: 5,0 (g/mL) Ii__ Lab File ID:· GH058135Cll
Level: (low/med) .,.LO ... w'--_
% Moistu.re: not dee. _ll
Column (pack/cap) CAP
Number TICs found: __o_
CAS NUMBER COMPOUND NAME
Date Received: 07/21/90
Date Analyzed: 07/30/90
Dilution Factor: &1~1 0._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q =•=============~ nmmmu=========-=======~====== =======::::11 ==========:a=-• =-===-=
FORM I VOA-TIC l/87 Rev.
20937 ~5 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
MWl4-2S-l
Lab Cod.a: COMPU Case No.: 20937 SAS No.: SDG No.: .,._05,.___
Matrix: ( soil/'Water) SOIL Lab sample ID: 358142
Sample 'Wt/vol: 5.0 (g/mL) !a__ Lab File IO: GH058l42Cll
Level: (lo'W/med) LOW Date Received: 07 /21/90
% Moisture: not dee. _..il Date Analyzed: 07 /J0/2Q
Column: (pack/cap) CAP Dilution Factor: .1L10,._ __
. CAS NO. COMPOUND CONCENTRATION UNITS:·
(ug/L or ug/Kg) UG/KG • Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u
75-0l-4---------Vinyl Chloride 13 u
75-00-3---~-----Chloroethane 13 u
75-09-2---------Methylene Chloride 21 B 67-64-1---------Acetone 24 B
75-15-o---------carbon Disulfide 7 u
75-35-4---------1,l-Dichloroethene 7 u
75-34-3---------1,l-Oichloroethane 7 u
540-59-0--------1,2-oichloroethene (total)_ 7 u
,s7-66-3---------Chloroform 7 u
107-06-2--------1,2-oichloroethane 7 u
78-93-3---------2-Butanone 13 u
71-55-6---------l,l,l-Trichloroethane 7 u
56-23-5---------carbon Tetrachloride 1· u
108-05-4--------Vinyl Acetate 13 u
75-27-4----.;.----Bromodichloromethane 7 u
78-87-5---------1,2-Dichloropropane 7 u
10061-0l-s------cis-l,3-Dic~loropropene 7 u
79-01-6---------Trichloroethene 7 u
124-48-1--------Dibromochloromethane 7 u
79-oo-s---------l,l,2-Trichloroethane 7 u
71-43-2---------Benzene 7 u
10061-02-6------Trans-l,3-0ichloropropene __ 7 u
75-25-2--.;.------Bromoform 7 u
1os-10-1----~---4-Methyl-2-Pentanone 13 u
!59 l-7 8-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 7 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 7 u
108-88-3--------Toluene 7 u
108-90-7--------Chlorobenzene 7 u .
100-41-4--------Ethylbenzene 7 u
100-42-5--------styrene 7 u·
1330-20-7-------Total Xylenes 7 u
FORM I VOA l/87 Rev.
20937 05 SAMPLE DATA SUMMARY ?5
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TEN.TATIVELY IDENTIFIED COMPOUNDS
EPA SAMP4= NO .
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS MWl4-2S-l
.
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: .,._0..._5 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: ( low/med) LOW
t Moist.ure: not dee. _il
Column (pack/cap) CAP
Number TICs found: _Q
CAS NUMBER
(g/mL) !i...,;_
COMPOUND NAME
Lab Samp 1 e ID: .,._3 .,._5 8,._1"'4..,2.__ __ _
Lab File ID: GH058142Cll
Date Received: 07/21/90
Date Analyzed: 07/30/90
Dilution Factor: .1~1 ~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
===-c==:=====z:i==== ==========--•============•== a•====== ===-========•=-=-====
FORM I VOA-TIC 1/87 Rev.
20937 05 SAMPLE DRtR SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW16-2S-l Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No,: S CG No , : .,._O 5..___
Matrix: (soil/water) SOIL Lab Sample ID: 358992
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH058992B10
Level: (low/med) LOW Date Received: 07/25/90
\ Moisture: not dee. __ 7 Date Analyzed: 07 £'.J0,:'.90
Column: (pack/cap) C6P Dilution Factor: ~i~.o,._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u 74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane 11 u
75-09-2---------Methylene Chloride 12 B
67-64-1---------Acetone 21
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 11 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 5 u
7 8-8 7-5----------1, 2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
lJJo-·20-1-------Total Xylenes 5 u
FORM I VOA 1/87 -Rev.
20937 05 SAMPLE DATA.SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
EPA SAMPLE NO.
MW16-2S-l
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: .,..0,._5 __
Matrix: ( soil/water) SOIL
Sample 1..t/vol: 5.0 (g/mL) L_
Level: (low/med) LOW
t Moisture: not dee. __ 7
Column (pack/cap) Cllf
Number TICs found: __Q
CAS NUMBER COMPOUND.NAME
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG{'.KG
RT EST.
358992
QH05822~!H0
01ast:20
07{'.3Q{'.2Q
l,0
CONC. Q .:a=============== ::1::::::::::::::::::::::::::::::::::::::1==========aa::::::::::::== ========-============a =-====
FORM I VOA-TIC l/87 Rev.
20937 05 SAMPLE.DATA SUMMARY \ ~
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name·: COMPUCHEM, RTP Contract: 12-881-REVS
SBl-1-1
Lab Code: COMPU Case No.: 20937 SAS No,: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 359872
sample wt/vol: 5.0 (g/mL) !i..__ Lab File ID: GH059872B12
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. _u Date Analyzed: 08/0§/90
Column:
-
(pack/cap) CM! Dilution Factor: Al~,~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 32 B 67-64-1---------Acetone 18 B 75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-Dichloroethene 6 u 75-34-3-----~---l,l-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3-~-------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u 78-93-3---------2-Butanone 3 BJ
71-55-6---------1,l,l-Trichloroethane 6 u 56-23-5---------carbon Tetrachloride 6 u
108-05-4------~-Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u 78-87-5---------1,2-Dichloropropane 6 u
10061-0l-5·-----cis-1,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
l.24-48-1--------Dibromochloromethane 6 u
79-00-5----~----1,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromotorm 6 u
1oe-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
20937 05 SAMPLE DATA SUMMARY 91
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP contract: /2-88)-REVS
Lab cod,e: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SBl-1-1
No.: 05
359872
Sample 1.rt/vol: 5.0 (g/mL) L_ Lab File ID: GH059872B12
Level: (low/med) LOW
\ Moisture: not dee. ___ll
Column (pack/cap) CAP
Number 1'.ICs found: ___Q
CAS NUMBER COMPOUND NAME
Date Received: 07/27/90
Date Analyzed: 08/0§/90
Dilution Factor: .1~1 0,.__ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
ia:amamm=i:a=•======-•====-======-=============== ======== =-=========a•• --===
FORM I VOA-TIC 1/87 Rev.
20937 05 SAMPLE DATA SUMMARY ?8
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS SBl-2-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ~0-5 __
Matrix: (soil/water) SOIL Lab Sample ID: 359871
Sample wt/vol: s.o (g/mLJ ~ Lab File IO: GH059871Bl2
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. __il Date Analyzed: 08/0~/90
Column: (pack/cap) Dilution Factor: 1.0
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UGl!';G Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 69 B 67-64-1---------Acetone 62 B 75-15-o---------carbon Disultide 6 u 75-35-4---------1,1-Dichloro~ene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3-----~---Chlorofonn 2 J 107-06-2--------1,2-Dichloroethane 6 u 78-93-3---------2-Butanone 4 BJ 71-55-6---------1,1,1-Trichloroethane 6 u 56-23-5---------carbon Tetrachloride 6 u 108-05-4--------Vinyl Acetate 13 u 75-27-4---------Bromodichloromethane 6 u 78-87-5---------1,2-Dichloropropane 6 u 10061-01-5------cis-l,3-Dichloropropene 6 u 79-01-6---------Trichloroethene 6 u 124-48-1--------Dibromochloromethane 6 u 79-00-s---------·1, 1, 2-Trichloroethane 6 u 71-43-2---------Benzene 6 u 10061-02-6------Trans-l,3-Dichloropropene __ 6 u 75-25-2---------Bromotonn 6 u 108-10-1--------4-Methyl-2-Pentanone 13 u 591-78-6-~------2-Hexanone 13 u 127-18-4--------Tetrachloroethene 3 J 79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u 108-88-3--------Toluene 6 u 108-90-7--------Chlorobenzene 6 u 100-41-4--------Ethylbenzene 6 u 100-42-s--------styrene 6 u 1330-20-7-------Total Xylenes 6 u .
FORM I VOA 1/87 Rev.
20937 0S SAMPLE DATA SUMMARY ;:w
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
EPA SAMPLE NO.
SBl-2-1
Lab Cc,de: COMPU Case No.: 20937 SAS No.: SOG No.: .,._05..__
MatriK: (soil/water) SOIL
Sampl11 wt/vol:
Level: ( low/med)
5.0 (g/mL) !i......_
LOW
\ Moie;ture: not dee. --2..l
Columrl (pack/cap)
Number· TICs found: __o_
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
359871
GH059!Flfll.2
07/27/90
9!1(9§(29
1.0
CONC. Q ============-=== •*==========•=============== ======== ==========•m=-•=-===
FORM I VOA-TIC 1/87 Rev.
20937 05 SRMPLE DATA SUMMRRY
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VOLATILE ORGANICS ANALYSIS DATA SHEET· EPA SAMP.LE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
SB2'-l-l
Lab c,~de : COMPU Case No.: 20937 SAS No.: SOG No.: ,..OS.,___
Matri:c (soi 1/wa tar) SOIL Lab Sample IO: 359870
Sample wt/vol: 5.0 (g/mL) !:i___J Lab File IO: GH059870Bl2
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. _ll Date Analyzed: 08/06/90
Column: (pack/cap) Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. ·coMPOUND (ug/L or ug/Kg) !,!G/!SG Q
74-87-3---------Chloromethane 13 u
74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u
75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 27 B
67-64-l---------Acetone 9 BJ 75-15-o---------carbon Disulfide 6 u
75-~5-4---------1,l-Dichloroethene 6 u
75-34-3---------l,l-Dichloroethane 6 u
540-59-o--------l,2-0ichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 . u
107-06-2-------l,2-0ichloroethane 6 u
78-93-3---------2-Butanone 13 u
71-55-6---------l,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------l,2-Dichloropropane 6 u
10061-0l-S------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------l,l,2-Trichloroethane 6 u
71-43-2----~----Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
ioa-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------l,l,2,2-Tetrachloroethane __ 6 u
108-88-3-~------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------Styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA l/87 Rev.
?A937 05 iSAMPLE DATA SUMMARY
.m
D
D
D
n
I
I
I
D
D
u
m
m
I -
lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Namu: COMPUCHEM.RTP Contract: (2-881-REVS
EPA SAMPLE NO.
SB2-l-l
Lab Cod,a: COMPU Case No.: 20937 SAS No.: SDG No.: ,._o,,_s __
Matrix: (soil/water) SOIL Lab Sample ID: 359870
Sample wt/vol: 5,0 (g/mL) !...._
LOW
Lab File ID: GH059870B12
Level: (low/med)
% Moisture: not dee. --2.l.
Column (pack/cap)
Number TICs found: __Q
CAS NUMBER COMPOUND NAME
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
07/27/90
08/06/90
l,Q
RT EST. CONC.
FORM I VOA-TIC l/87 Rev.
20937 05 SAMPLE DATA SUMMARY
Q
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I
g
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m
lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SB2-2-l Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: ( soil/water) SOIL Lab Sample ID: 359875
Sample wt/vol: 5.0 (g/mL) !L__ Lab File ID: !:iHQ59875!H2
Level: (low/med) I.QW Date Received: 07 /27 /90
t Moisture: not dee. _u Date Analyzed: 08/0§/90
Column: (pack/cap) cap Dilution Factor: -1~,0,.__ __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
1s-1s-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------l,l-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-S------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroetha~e
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
-
Q
13 u
13 u
13 u
13 u
27 B
13 B
6 u
6 u
6 u
6 u
6 u
6 u
4 BJ
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA 1/87 Rev.
20937 OS SAMPLE DATA SUMMARY
I
I
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I
I
g
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u
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: f2-88l-REVS
EPA SAMPLE NO.
SB2-2-l
Lab Cclde : COMPU Case No.: 20937 .SAS No.: SDG No.: ...,05...__
Matrix: ( soil/water) SOIL
sample wt/vol: 5.0 (g/mL) !i__
Level: ( low/med) t.QW
I Moisture: not dee. _u
Column (pack/cap) CAP
Number TICs found: ___Q
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
·(ug/L or ug/Kg) UG/KG
RT EST.
359875
GHO:i987:i!H2
07/27/90
08/06/90
l,O
CONC. Q ==-============== :a=======================-====---======-•:a==-========-= •====
FORM I VOA-TIC 1/87 Rev.
20937 05 SAMPLE DATA SUMMARY
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COHPUCHEH.RTP Contract: <2-88)-REVS
Lab Code: COHPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID:
Level: ( low/med) LOW Date Received:
EPA SAMPLE NO.
SBJ-1-1
No.: 05
359874
GH059874Bl2
07/27/90 g I Moisture: not dee. ---2..0. Date Analyzed: Q!l/0§/90
I
D
D
m
m
m
0
I
Column: (pack/cap) ~CnA£P __ Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-J---------Chloromethane 12 u 74-83-9--------~aromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-J---------Chloroethane 12 u
75-09-2---------Methylene Chloride 45 a
67-64-1---------Acetone 31 a
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,l-Dichloroethene· 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93~3---------2-Butanone 3 BJ
71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2-----~---Benzene 6 u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oe-10-1--------4-Methyl'-2-Pentanone 12 u
591-78-6--------2-Hexanone ·12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-J--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
-
FORM I VOA l/87 Rev.
.-.. -.-..--.-..-.-,-.-,-,1 r-r-.1-.T1~ ~IIMMt~Ol.l ,-, ~ .-. ·-·.
D
D
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rn
m
I
m
D
I
D
I
I
I
I
lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
SBJ-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: ( soil/water) SOIL Lab Sample ID: 359874
Sample wt/vol: 5.0 (g/mL) G..._ Lab File ID.: GH059874B12
Level: (low/med) LOW
\ Moisture: not dee. _.ll
Column (pack/cap) CAI:!
'Number TICs found: __Q.
CAS NUMBER COMPOUND NAME
Date Received: 07/27/90
Date Analy:z:ed: 08/0§/90
Dilution Factor: ~i~-~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
'
RT EST. CONC. Q =a=••=========== •=a=======s================= a======= ==-==::s======•:a =-•====
FORM . I VOA-TIC 1/87 Rev.
? 937 05 •SAMPL~ DATA SUMMARY
g
g
D
D
m
m
m
m
m
0
D
u
D
I
I
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: -COMPUCHEM. RTP Contract: (2-88)-REVS
SBJ-2-1
Lab Code: COMPO Casa No.: 20937 SAS No.: SDG No.: 05
Matrix: ( soil/water) SOIL Lab Sample ID: 359873
Sample wt/vol: 5.0 (g/mL) L_ Lab File ID: GR059873Al9
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. -1.9. Date Analyzed: 08/13/90
Column: (pack/cap) CAP Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride. 36 B
67-64-1---------Acetone 65 B 75-15-o---------carbon Disulfide 6 u
7 5-35-4----------1, 1-Dichloroethene 6 u
75-34-3---------1,l~Dichloroethane 6 u
540-59-o--------l,2-Dichloroethene (total)_ 6 u 67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 4 J
71-55-6---------1,1,l~Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u / 10061-0l-5------cis-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1os-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
-
FORM I VOA 1/87 Rav.
20937 05 SAMPLE D~T~ SUMMARY 81
g
I
u
D
D
B
g
I
lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: [2-BBl-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
SBJ-2-1
No.: 05
359873 Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GR05987JAl9 Level: (low/med) LOW
t Moisture: not dee. _n
Column (pack/cap) Cl!P
Number TICs found: __.Q.
CAS NUMBER COMPOUND NAME
Date Received: 07 /27 /90
Date Analyzed: 08/13/90
Dilution Factor: 41~,o.__ __
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ==-:ag===i==========-============================ -Zl-:::S::::1::::1::U::S ::r:11:a::::a=:::a::a:a:a•• •=====
FORM I VOA-TIC 1/87 Rev,
20937 05 SAMPLE DATA SUMMARY 80 -
I
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0
m
m
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D
I
I
m
m
g
D
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-7S-1MS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Cocle: COMPU Case No.: 20937 SAS No.: SOG No.: 05
Matrix:: (soil/water) SOIL Lab Sample ID: 358139
Sample wt/vol: s.o (g/mL) L-Lab File ID: GH0581J9Cll
Level: (low/med) LOW Date Received: 07/21/90
'I; Moisture: not dee. _ll Date Analyzed: 07/30/90
Column: (pack/cap) Cl,P Dilution Factor: &l~.o.__ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 16 B
67-64-1---------Acetone 25 B
75-15-o---------carbon Disulfide 6 u
75-35-4---------l,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
940-59-0--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chlorotorm 6 u
107-06-2--------l,2-Dichloroethane 6 u
78~93-3---------2-Butanone 12 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-0l-S------cis-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6· u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromotorm 6 u
1os-10-1-~------4-Methyl-2-Pentanone. 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
'79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
A 5 MAR'r'
I
B
D
D
m
m
D
u
E
I
m
w
D
lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
MWll-7S-lMSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ,.,OS.,___
Matrh:: ( soil/water) SOIL Lab Sample ID: 358140
Sample, wt/vol: s,o (g/mL) L_ Lab Fila IO: GH058140Cl l
Level: (low/med) LOW Date Received: 07/21/90
% Moisture: not dee. -2.li Date Analyzed: 07/30/90
Column: (pack/cap) CAP Dilution Factor: ~i~1 ,.,o __
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
1s-1s-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
lS-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethana
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethana
78-87-5---------1,2-Dichloropropane
10061-0l-S------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethana
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzana
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
100-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5-----~---l,l,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbanzana
100-42-s--------styrene
1330-20-7-------Total Xylenes
Q
12 u
12 u
12 u
12 u
16 B
22 B
6 u
6 u
6 u
6 u
6 u
6 u
12 u
6 u
6 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
12 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA 1/87 Rev.
ATA SUMMARV
I
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0
m
m
m
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u
e
I
m
m
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
MW1J-7S-l
Lab Co,:le: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample IO: 358135
Sample wt/vol: 30,0 (g/mL) L._ Lab File ID: GH058 l3 5B21
Level: (low/med) LOW Date Received: 07 /21/90
t Moisture: not dee.~ dee. Date Extracted: Q1IHl9Q
Extraction: (SepF/Cont/Sonc)
(Y/N) li.._
~
pH:~
Date Analyzed: 08/Q8/9Q
GPC Cleanup: Dilution Factor: _1~·=0~0 __
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 410
lll-44-4--------bis(2-Chloroethyl)Ether 410
95-57-8---------2-Chlorophenol 410
541-73-1--------1,J-Dichloroben:i:ene 410
106-46-7--------1,4-Dichloroben:i:ene 410
100-51-6--------Ben:i:yl Alcohol 410
9 s-s·o-1---------1, 2-oichloroben:i:ene 410
95-48-7---------2-Methylphenol 410
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410
106-44-5--------4-Methylphenol 410
621-64-7--------N-Nitroso-Di-n-Propylamine_ 410
67-72-1---------Hexachloroethane 410
98-95-3---------Nitroben:i:ene 410
78-59-1---------Isophorone 410
88-75-5---------2-Nitrophenol 410
105-67-9--------2,4-Dimethylphenol 410
65-85-o---------Ben:i:oic Acid 20.00
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 410
120-83-2--------2,4-Dichlorophenol 410
120-a2-1--------1,2,4-Trichloroben:i:ene 410
91-20-3---------Naphthalene 410
106-47-8---~----4-Chloroaniline 410 .
87-68-3---------Hexachlorobutadiene 410
59-50-7---------4-Chloro-3-Methylphenol 410
91-57-6---------2-Methylnaphthalene 410
77-47-4---------Hexachlorocyclopentadiene __ 410
88-06-2--~------2,4,6-Trichlorophenol 410
95-95-4---------2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 410
88-74-4---------2-Nitroaniline 2000
131-11-3--------oimethyl Phthalate 410
208-96-8--------Acenaphthylene 410
606-20-2--------2,6-Dinitrotoluene 410
-
Q
u u u u u u u
u u u u u u u u u u
u u u u u u
u u u u u u u u
u u
FORM I sv-1 1/87 Rev.
20937 05 SAMPLE DATR SUMMARY
I
I
I
I
I
m
I
g
D
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I
m
ffl·
m
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW13-7S-l Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 05
Matri>:: (soil/water) SOIL Lab Sample IO: 358135
SamplEt wt/vol: 30.0 (g/mL) ~ Lab File IO: GH05Ql35ll21
Level: ,( low/med) LOW Data Received: 07 /21/90
t Mois,ture: not dee. _lQ dee. Data Extracted: 07/24/90
Extrac:tion: (SepF /Cont/Sonc)
(Y/N) li,_
Data Analyzed: 08/08/90
GPC Cleanup: pH: ...2...2 Dilution Factor: ·1.00 ~~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroanilina 2000
83-32-9---------Acenaphthana 410
51-28-5---------2,4-0initrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------0ibenzofuran 410
121-14-2---~----2,4-Dinitrotoluene 410
84-66-2---------Diethylphthalate 410
7005-72-3-------4-Chlorophenyl-phenylether_ 410
86-73-7---------Fluorene 410
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000
86-30-6---------N-Nitrosodiphenylamine (l)_ 410
101-55-3--------4-Bromophenyl-phenylether_ 410
118-74-1--------Hexachlorobenzena 410
87-86-5---------Pentachlorophenol 2000
as-01-s---------Phenanthrene 410
120-12-1--------Anthracene 410
84-74-2---------oi-n-Butylphthalate 410
206-44-0--------Fluoranthene 410
129-00-0--------Pyrene 410
85-68-7---------Butylbenzylphthalata 410
91-94-1---------3,3'-0ichlorobenzidine 820
56-55-3---------Benzo(a)Anthracene 410
218-01-9--------Chrysena 410
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 410
117-84-o--------oi-n-octyl Phthalata 410
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthena 410
50-32-8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 410
53-70-3---------Dibenz(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
(1) -cannot be separated from Oiphenylamine
Q
u u u
u
u
u
u u u
u u
u
u
u
u u u
u
u
u
u
u
u
u u
u
u
u
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u u
u
FORM I sv-2 1/87 Rev.
r, 76
m
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R
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u
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Na1ne: COMPUCHEM. RTP Contract: 12-881-REVS
MW13-7S-l
Lab Coc:l.e : COMPU Case No.: 20937 SAS No.: SDG No.: ,,_0.._!5 __ ,
Matrix: (soil/water) SOIL
sample wt/vol: 30.0 (g/mL) ~
Level: ( low/med) LOW
% Moisture: not dee. ---2..Q dee.
Extraction: (Sepl"/Cont/Sonc) ~
GPC Cl•aanup: (Y/N) Ji_ pH: ...L..1
Number TICs tound: __l.
CAS NUMBER COMPOUND NAME
Lab Sample ID: .,_3..,_5.,._9..._1.._35.,_ __ _
Lab File ID: GH058135B21
Date Received: 07/21/90
Date Extracted: 07/24/90
Date Analyzed: 08/08/90
Dilution Factor: al~,o~o.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
:=asa::ss•===a:aa:1:::11::s::11 --========•======------=====-• a:mua:::s:amaa •===-==~==-•--••===
1. SOLVENT CONTAMINANT 5.07 500 J
FORM I SV-TIC 1/87 Rev.
---. ------------• .............. .
m
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u
1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW14-2S-l Lab Name: COMPUCHEM, RTP Contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample IO: 358142
Sample ·,rt/vol: 30,l (g/mL) ~ Lab File ID: GJQ58142B21
Level: (low/med) LOW Date Received: 07/21/90
t Moisture: not dee. __2j_ dee. Date Extracted: 07/H/9Q
Extract ion: ( S,epF /Cont/ Sonc) SQliC Date Analyzed: Q8/08l9Q
GPC Cleanup: (Y/N) li,_ pH: -2.J. Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 430 u
lll-44-4--------bis(2-Chloroethyl)Ether 430 u
95-57-8---------2-Chlorophenol 430 u
541-73-1--------1,3-Dichlorobenzene 430 u
106-46-7--------1,4-Dichlorobenzene 430 u
100-51-6--------Benzyl Alcohol 430 u
95-50-1---------1,2-Dichlorobenzene 430 u
~5-48-7---------2-Methylphenol 430 u
39638-32-9------bis ( 2-Chlor.oisopropyl) Ether_ 430 u
106-44-5--------4-Methylphenol 430 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 430 u
67-72-1---------Hexachloroethane 430 u
98-95-3---------Nitrobenzene 430 u
78-59-1---------Isophorone . 430 u
88-75-5---------2-Nitrophenol 430 u
105-67-9--------2,4-Dimethylphenol 430 u
65-85-0---------Benzoic Acid 2100 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 430 u
120-83-2--------2,4-Dichlorophenol 430 u
120-s2-1--------1,2,4-Trichlorobenzene 430 u
91-20-3---------Naphthalene 430 u
106-47-8--------4-Chloroaniline 430 u
87-68-3---------Hexachlorobutadiene 430 u
59-50-7---~-----4-Chloro-J-Methylphenol 430 u
91-57-6---------2-Methylnaphthalene 430 u
77-47-4---------Hexachlorocyclopentadiene __ 430 u
88-06-2---------2,4,6-Trichlorophenol 430 u
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalene 430 u
88-74-4----~----2-Nitroaniline 2100 u
131-11-3--------Dimethyl Phthalate 430 u
208-96-s--------Acenaphthylene 430 u
606-20-2--------2,6-Dinitrotoluene 430 u
FORM I SV-1 1/87 Rev.
I
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I
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m
m
m
m
m
m
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW14-2S-l
Lab Na1ne: COMPUCHEM. RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample IO: 358142
Sample wt/vol: 30,1 (g/mL) !:i...._ Lab File ID: GJ058142B2l
· Level: (low/med) LOW Date Received: 07 /21/90
% Mois·ture: not dee. _ll dee. Date Extracted: 01 a4120
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/08/90
GPC Cleanup: (Y/N) Ii,_ pH: _iJ_ Dilution Factor: ~i~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2100
83-32-9---------Acenaphthene 430
51-28-5---------2,4-Dinitrophenol 2100
100~02-1--------4-Nitrophenol 2100
132-64-9--------Dibenzofuran 430
121-14-2-~------2,4-Dinitrotoluene 430
84-66-2---------Diethylphthalate 430
7005-72-3-------4-Chlorophenyl-phenylether_ 430
86-73-7---------Fluorene 430
100-01-6--------4-Nitroaniline 2100
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2100
86-30-6---------N-Nitrosodiphenylamine (l)_ 430
101-55-3--------4-Bromophenyl-phenylether __ 430
118-74-1--------Hexachlorobenzene 430
87-86-5---------Pentachlorophenol 2100
85-01-8---------Phenanthrene 430
120-12-1--------Anthracene 430
84-74-2---------Di-n-Butylphthalate 430
206-44-o--------Fluoranthene 430
129-oo-o--------Pyrene 430
85-68-7---------Butylbenzylphthalate 430
91-94-1---------3,3'-Dichlorobenzidine 870
56-55-3---------Benzo(a)Anthracene 430
218-01-9--------Chrysene 430
ll7-8l-7--------bis(2-Ethylhexyl)Phtha1ate_ 430
117-84-0--------Di-n-octyl Phthalate 430
205-99-2--------Benzo(b)Fluoranthene 430
207-08-9--------Benzo(k)Fluoranthene 430
50-32-8---------Benzo(a)Pyrene 430
193-39-5--------Indeno(l,2,3-cd)Pyrene 430
53-70-3---------Dibenz(a,h)Anthracena 430
191-24-2--------Benzo(g,h,i)Perylene 430
(1) -Cannot be separated from D1phenylamine
Q
u u u u u u u u u u
u u u u u
u u u u u u u u u u u u u
u
u
u u
FORM I sv-2 l/87 Rev.
m
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m
m
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m
m
m
m
m
I
I
D
I
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ii
I -
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
Lab Name: COMPUCHEM.RTP MWl4-2S-l
Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 358142
Sample wt/vol: 30.1 (g/mL) L_ Lab File ID: GJosa142e21
Level: ( low/med) LOW
\ Moisture: not dee. --2.! dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ii,_ pH: ..id
Number TICs found: ---2.
CAS NUMBER COMPOUND NAME
Data Received: 07 /21/90
Date Extracted: 07tHt90
Date Analyzed: 08i08/9Q
Dilution Factor: ~i~,~o __ _
CONCENTRATION UNITS:
(ug/L or ug/KgJ UGiKG
RT EST. CONC. Q =•====•========= ••=m======================== ======== •==========a= =====
1. SOLVENT CONTAMINANT 5.08 480 BJ
2. SOLVENT CONTAMINANT 5.15 310 BJ
FORM I SV-TIC l/87 Rev.
.-. TI
m
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m
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D
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D.
I
I
I
I
m
g
1B
SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW16-2S-l Lab Na1ne: COMPUCHEM, RTP Contract: C2-88l-REVS
Lab Code: COMPU Casa No.: 20937 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: Jo.1 (g/mL) li,__
Level: ( low/med) LOW
\ Moisture: not dee. ___J_ dee.
Extrac1:ion: (SepF /Cont/Sonc) .so.fil:
GPC Cleanup: (Y/N) tL,_ pH:~
SOG No.: ~95 __
Lab Sample ID: ..,J,...5,,_89,,_9 .. 2..._ __ _
Lab File ID: GH058992BOB
Date Received: 07/25/90
Date·Extracted: 07/27/90
Data Analyzed: 08/03/90
Dilution Factor: _1_,o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 350 u
lll-44-4--------bis(2-Chloroethyl)Ether 350 u
95-57-8---------2-Chlorophanol 350 u
541-73-1--------1,3-Dichlorobenzene 350 u
106-46-7----~---l,4-Dichlorobenzena 350 u
100-51-6--------Benzyl Alcohol 350 u
95-50-1---------1,2-Dichlorobenzene 350 u
95-48-7---------2-Methylphenol 350 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 350 u
106-44-5--------4-Methylphenol 350 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 350 u
67-72-1---------Hexachloroethana 350 u
98-95-3---------Nitrobenzena 350 u
78-59-1---------Isophorona 350 u
88-75-5---------2-Nitrophenol 350 u
105-67-9--------2,4-Dimethylphenol 350 u
65-85-o---------Benzoic Acid 1700 u
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 350 u
120-83-2--------2,4-Dichlorophenol 350 u
120-a2-1--------1,2,4-Trichlorobenzene 350 u
91-20-3---------Naphthalene 350 u
106-47-8--------4-Chloroaniline 350 u
87-68-3---------Hexachlorobutadiena 350 u
59-50-7---------4-Chloro-3-Methylphenol 350 u
91-57-6---------2-Methylnaphthalene 350 u
77-47-4---------Hexachlorocyclopentadiene __ 350 u
88-06-2---------2,4,6-Trichlorophenol 350 u
95-95-4---------2,4,5-Trichlorophenol 1700 u
91-58-7---------2-Chloronaphthalene 350 u
88-74-4---------2-Nitroaniline 1700 u
131-11-3--------Dimethyl Phthalata 350 u
208-96-8--------Acenaphthylene 350 u
606-20-2--------2,6-Dinitrotoluane 350 u
-
FORM I sv-1 1/87 Rev.
I
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m
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D
D
D
D
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP MWl6-2S-l
Contract: (2-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 358992
sample wt/vol: 30,1 (g/mL) ~ Lab File ID: GHO:iB992BQB
Level: ( low/med) LOW Date Received: 07/25/9Q
% Moisture: not dee. __ 7 dee. Date Extracted: 07/27/90
Extraction:
·GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li.._
5.QHC
pH: ....§....2
Date Analyzed: 08/03/90
Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1700
83-32-9---------Acenaphthene 350
51-28-5---------2,4-Dinitrophenol 1700
100-02-7--------4-Nitrophenol 1700
132-64-9--------Dibenzoturan 350
121-14-2--------2,4-Dinitrotoluene 350
84-66-2---------Diethylphthalate 350
7005-72-3-------4-Chlorophenyl-phenylether_ 350
86-73-7----~----Fluorene 350
100-01-6--------4-Nitroaniline 1700
534-52-1--------4,6-Dinitro-2-Hethylphenol_ 1700
86-30-6---------N-Nitrosodiphenylamine (l)_ 350
101-55-3--------4-Bromophenyl-phenylether __ 350
118-74-l--------Hexachlorobenzene 350
87-86-5---------Pentachlorophenol 1700
85-01-8---------Phenanthrene 350
120~12-1--------Anthracene 350
84-74-2---------Di-n-Butylphthalate 350
206-44-o--------Fluoranthene 350
129-00-0--------Pyrena 350
85-68-7-----~---Butylbanzylphthalate 350
91-94-1---------3,3'-Dichlorobenzidine 710
56-55-3---------Benzo(a)Anthracene 350
:218-01-9--------Chrysene 350
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 620
117-84-0--------Di-n-Octyl Phthalata 350
205-99-2--------Benzo(b)Fluoranthene 350
207-08-9--------Benzo(k)Fluoranthene 350
50-32-8---------Benzo(a)Pyrena 350
193-39-5--------Indeno(l,2,3-cd)Pyrene 350
53-70-3---------Dibenz(a,h)Anthracena 350
:L91-24-2--------Benzo(g, h, i) Perylena 350
(l) -cannot be separated trom Diphenylamina
u u
u u u u u
u u
u u
u u
u
u
u
u u u u u u
u
u
u u u
u
u u
u
FORM I SV-2 1/87 Rev.
Q
I
m
m
m
m
m
m
I
B
D
m
I
lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
MW16-2S-l Lab Name: COMPUCHEM,RTP Contract: 12-ea1~REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ___ SOG No.: ,.,0.,_5 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) !L__
Level: ( low/med) LOW
% Moisture: not dee. __ 7 dee.
Extraction:-(SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H.,_ pH:~
Number TICs tound: _.J.
CAS NUMBER COMPOUND NAME
Lab Sample ID: .,.3.,.5.,.,8...,99,,_.2..._ __ _
Lab File ID: GH058992B08
Date Received: 07/25/90
Date Extracted: 07/27/90
Date Analyzed: 08/03/90
Dilution Factor: .i~,,.,o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=mma======••=•m~ ea==•=•========•======••==•• =•=-111•:iz::az:11 •••-===a=-=••a =-==== -1. SOLVENT CONTAMINANT 4,32 430 BJ
2. SOLVENT CONTAMINANT 4.40 290 BJ
3. ALOOL 5.33 210 ABJ
FORM I SV-TIC 1/87 Rev.
m
m
m
m
m
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R
D
I
I
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBl-1-1 Lab Nan1e: COMPUCHEM, RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL) L_
Level: (low/med) LOW
% Moisture: not dee. _ll
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL_
dee.
SQliC
pH: ..i..1.
SDG No.: 05
Lab Sample ID: 359872
Lab File IO: G2,J:5987U,21
r
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/12/90
Dilution Factor: .i~-~o __ _
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 420 u
lll-44-4--------bis(2-Chloroethyl)Ether 420 u
95-57-8---------2-Chlorophenol 420 u
541-73-1--------l,3-Dichlorobenzene 420 u
106-46-7--------1,4-Dichlorobenzene 420 u
100-51-6--------Benzyl Alcohol 420 u
95-50-1---------1,2-Dichlorobenzene 420 u
95-48-7---------2-Methylphenol 420 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 420 u
106-44-5--------4-Methylphenol 420 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 420 u
67-72-1---~-----Hexachloroethane 420 u
98-95-3---------Nitrobenzene 420 u
78-59-1---------Isophorone 420 u
88-75-5---------2-Nitrophenol 420 u
105-67-9--------2,4-Dimethylphenol 420 u
65-85-o---------Benzoic Acid 2100 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 420 u
120-83-2--------2,4-Dichlorophenol 420 u
120-s2-1--------l,2,4-Trichlorobenzene 420 u
91-20-3--~------Naphthalene 420 u
106-47-8--------4-Chloroaniline 420 u
87-68-3---------Hexachlorobutadiene 420 u
59-50-7---------4-Chloro-J-Methylphenol 420 u
91-57-6---------2-Methylnaphthalene 420 u
77-47-4-------~-Hexachlorocyclopentadiene __ 420 u
88-06-2---------2,4,6-Trichlorophenol 420 U·
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalena 420 u
88-74-4---------2-Nitroanilina 2100 u
131-11-3--------Dimethyl Phthalate 420 u
208-96~8-----~--Acenaphthylene 420 u
606-20-2--------2,6-Dinitrotoluana 420 u
FORM I sv-1 1/87 Rav.
m
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m
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m
m
m
m
m
m
m
m
m
m
m
m
m
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Nan1e: CQMPUCHEM, RTP Contract: 12-88)-REVS
SBl-1-l
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 359872
Sample wt/vol: 30.4 (g/mL) L_ Lab File ID: G2JS9872A21
Level: (low/med) ~LO¥.,,_w_ Date Received: 07/27/90
\ Moisture: not dee. _n dee. Date Extracted: 07/30/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/12/90
GPC ClE!anup: (Y/N) H__ pH: ~ Dilution Factor: .i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or_ug/Kg) UG/KG Q
99-09-2---------3-Nitroanilino 2100 u 83-32-9---------Acenaphthene 420 u s1-20-s---------2,4-Dinitrophenol 2100 u 100-02-1--------4-Nitrophenol 2100 u
132-64-9--------Dibenzofuran 420 u
121-14-2--------2,4-Dinitrotoluene 420 u
84-66-2---------Diethylphthalate 420 u
7005-72-3-------4-Chlorophenyl-phenylether_·_ 420 u
86-73-7---------Fluorene 420 u
100-01-6--------4-Nitroanilino 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2100 u
86-30-6---------N-Nitrosodiphenylamine 0-l_ 420 u
101-55-3--------4-Bromophenyl-phenylether __ 420 u
118-74-1--------Hexachlorobenzene 420 u
87-86-5---------Pentachlorophenol 2100 u
85-01-8---------Phenanthrene 51 .J
120-12-1--------Anthracene 420 u
84-74-2---------Di-n-Butylphthalate 420 u
206-44-0--------Fluoranthene 420 u
12 9-oo-o----.----Pyrene 420 u
85-68-7---------Butylbenzylphthalate 420 u
91-94-1---------3,J'-Dichlorobenzidine 850 u
56-55-3---------Benzo(a)Anthracene 420 u
218-01-9--------Chrysene 420 u
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_ 130 .J
117-84-o--------Di-n-octyl Phthalate 420 u
205-99-2--------Benzo(b)Fluoranthene 420 u
207-08-9--------Benzo(k)Fluoranthene 420 u
50-32-8---------Benzo(a)Pyreno 420 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 420 u
53-70-3---------Dibenz(a,h)Anthracene 420 u
191-24-2--------Benzo(g,h,i)Perylene 420 u
-(l) -Cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
D
m
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m
m
I
g
D
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab Cod.e: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SBl-1-1
No.: 05
359872
sample wt/vol: 30,4 (g/mL) L_ Lab File ID: G2,I:i9872A~l
Level: (low/med) ~LO"""W.,___
\ Moisture: not dee. _n dee.
Extract.ion:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li.._
~
pH: ....2.&.l
Number TICS tound: __i.
CAS NUMBER COMPOUND NAME
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/12/90
Dilution Factor: .1L,o.._ __
CONCENTRATION UNITS:
(ug/L.or ug/Kg) UG/KG
RT EST. CONC. Q
=••m=======•=m=• ••===================n====== •=====au •••a:a::u=•~==-•• •=-•==
1. SOLVENT CONTAMINANT 5.42 430 BJ
2. UNKNOWN OXYGENATED AI.KANE 5.50 340 J
3. ALDOL 6.35 1400 ABJ
4. PROPENYLBENZODIOXOLE 9.52 170 J s. UNKNOWN HYDROCARBON 12.10 260 J
6. UNKNOWN 13.69 170 J
7. UNKNOWN. 26.19 340 J
FORM I SV-TIC 1/87 Rev.
-------............. --•·
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET. EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: l2-8Bl-REVS
SBl-2-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: ( soil/water) SOIL Lab Sample ID: 359871
Sample wt/vol: 30.8 (g/mL) L_ Lab File ID: GH059871c21
Level: (low/med) LOW Data Received: 07/27/90
' Moisture: not dee. _u dee. Date Extracted: 07/30/90
Extrac:tion: (SepF/Cont/Sonc) S,OHS;
GPC Cleanup: (Y/N) li__ pH: ....L..2.
Date Analyzed: 08/11/90
Dilution Factor: .1~,~0~0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 410
lll-44-4--------bis(2-Chloroethyl)Ether 410
95-57-8---------2-Chlorophenol 410
541-73-1--------l,3-Dichlorobenzene 410
106-46-7--------l,4-Dichlorobenzene 410
100-51-6--------Benzyl Alcohol 410
95-50-1---------l,2-Dichlorobenzene 410
95-48-7-~--~----2-Methylphenol 410
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410
106-44-5--------4-Methylphenol 410
621-64-7--------N-Nitroso-Di-n-Propylamine_ 410
67-72-1---------Hexachloroethane 410
98-95-3---------Nitrobenzene 410
78-59-1-----.----Isophorone 410
88-75-5---------2-Nitrophenol 410
105-67-9--------2,4-Dimethylphenol 410
65-85-o---------Benzoic Acid 43
lll-9l-l--------bis(2-Chloroethoxy)Methane_ 410
120-83-2--------2,4-Dichlorophenol 410
120-e2-1----~---1,2,4-Trichlorobenzena 410
91-20-3---------Naphthalena 410
106-47-8--------4-Chloroanilina 410
87-68-3---------Hexachlorobutadiene 410
59-50-7---------4-Chloro-3-Methylphanol 410
91-57-6---------2-Methylnaphthalene 130
77-47-4---------Hexachlorocyclopentadiene __ 410
88-06-2---------2,4,6-Trichlorophenol 410
95-95-4---------2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 410
88-74-4---------2-Nitroaniline 2000
131-11-3--------Dimethyl Phthalate 410
208-96-8--------Acenaphthylene 51
606-20-2--------2,6-Dinitrotoluene 410
u u u u u u u u u u u u u u u u
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u u u u u
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FORM I sv-1 l/87 Rev.
Q
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
581-2-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix:: ( soil/water) SOIL Lab Sample ID: 359871
Sample wt/vo_l: 30.8 (g/mL) ~ Lab File ID: GH059871C21
Level: (low/med) LOW Date Received: 07/27/90
'II ·Moisture: not dee. __ll dee. Date Extracted: 07 /J0/90
Extraction: (SepF/Cont/Sonc)
(Y/N) li..._
SOH.C
pH: ...L..2.
Date Analyzed: 08/11/90
GPC Cleanup: Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------J-Nitroaniline 2000 83-32-9---------Acenaphthene 410 51-28-5---------2.4-Dinitrophenol 2000
100-02-1--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 410
121-14-2--------2,4-Dinitrotoluene 410
84-66-2-----~---Diethylphthalata 410
7005-72-3-------4-Chlorophenyl-phenylethar_ 410
86-73-7---------Fluorane 86
100-0l-6~-------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000
86-30-6---------N-Nitrosodiphanylamina (l)_ 410
101-55-3--------4-Bromophenyl-phenylether __ 410
118-74-1--------Hexachlorobenzene 410
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthrene 250
120-12-1--------Anthracene 69
84-74•2---------Di-n-Butylphthalate 410
206-44-0--------Fluoranthene 82
129-00-o--------Pyrene 170
85-68-7---------Butylbenzylphthalate 410
91-94-1---------3,3'-Dichlorobenzidine BlO
56-55-3--~------Benzo(a)Anthracene 66
218-01-9--------Chrysene 71
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 110
117-84-o--------oi-n-octyl Phthalata 410
205-99-2--------Benzo(b)Fluoranthene 61
207-08-9--------Benzo(k)Fluoranthane 61
50-32-8---------Benzo(a)Pyrane 50
193-39-5--------Indeno(l,2,J-cd)Pyrene 410
53-70-3---------Dibenz(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
(1) -cannot be separated from Diphanylam1ne
Q
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FORM I sv-2 1/87 Rev.
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Nan1e: COMPUCHEM. RTP Contract: 12-881-REVS
EPA SAMPLE NO.
SBl-2-1
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 05
Matrix:: (soil/water) SOIL
sample wt/vol: 30.8 (g/mL) L_
Level: (low/med) LO..,._,W,___
\ Moisture: not dee. ---1.l
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li,_
dee.
~
pH: ....§.J.
Lab Sample ID: 359871
Lab File ID: GH059871C21
Date Received: 07/27/90
Date Extracted: 07/30/20
Date Analyzed: 08/11/20
Dilution Factor: &1~,o~o.___
Number TICs found: .....2..2.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
=~a========m=a== =-•========•================-======== =-----=-==-=•--a====
1. SOLVENT CONTAMINANT 5.48 700· BJ
2. ALOOL 6.42 1600 ABJ
3. UNKNOWN 7.52 1100 J
4. UNKNOWN HYDROCARBON 8.75 580 J
5. UNKNOWN HYDROCARBON 9.54 990 J
6. 94-59-7 1,3-BENZODIOXOLE, 5-(2-PROPE 9,62 580 J
7. UNKNOWN HYDROCARBON 10.10 490 J
8. UNKNOWN HYDROCARBON 10.27 1200 J
9. UNKNOWN HYDROCARBON 10.70 990 J
10. UNKNOWN HYDROCARBON 10.97 1400 J
11. UNKNOWN HYDROCARBON 11.64 1800 J
12. UNKNOWN HYDROCARBON 11.92 700 J
13. UNKNOWN HYDROCARBON 12,24 2200 J
14. UNKNOWN .HYDROCARBON 12,82 1400 J
15. UNKNOWN HYDROCARBON 13.39 1100 J
16. UNKNOWN HYDROCARBON 13.92 780 J
17. UNKNOWN HYDROCARBON 14.42 580 J
18. UNKNOWN 14.62 740 J
19. UNKNOWN HYDROCARBON 15.44 450 J
20. UNKNOWN HYDROCARBON 15.64 1200 J
21. UNKNOWN HYDROCARBON 16.24 1500 J
22. UNKNOWN 16.92 1100 J
FORM I SV-TIC 1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab N11me: COMPUCHEM, RTP Contract: 12-881-REYS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
se2-1-1
No.: 05 I Matri>c: (soil/water) SOIL Lab Sample ID: 359870
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Samplu wt/vol: 30.7 (g/mL) lL_ Lab File ID: GH059870C21
Level: ( low/med) LOW Date Received: 07/27/90
'I; Moi!1ture: not dee. ~ dee. Date Extracted: 07 (l0/90
Extrac:tion: (SepF/Cont/Sonc) Date Analyzed: 08/11/90
GPC Cleanup: (Y/N) li._ pH: ...L.! Dilution Factor: ..,1~,0,...,0.___
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,J-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
J9638-J2-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
<ss-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-ss-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-J-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
FORM I sv-1
• ,.
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
2200 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
450 u
2200 u
450 u
2200 u
450 u
450 u
450 u
1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
.se2-1-1 Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab C:ode: CQMPU Casa No.: 20937 SAS No.: SDG No.: 05
MatrJ.x: (soil/water) SOIL Lab Sample ID: 359870
Sample wt/vol: 30.7 (g/mL) ~ Lab Fila· ID: GH05987oc21
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. ___il dee. Date Extracted: 07/30/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: 0 (Y/N) lL_
S.Qfil:
pH: jJ,
Data Analyzed: 08/11/90
Dilution Factor: Al~,o~o..___
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroanilina 2200
83-32-9---------Acenaphthene 450
51-28-5---------2,4-Dinitrophenol 2200 100-02-1--------4-Nitrophenol 2200
132-64-9--------Dibenzoturan 450
121-14-2--------2,4-Dinitrotoluena 450.
84-66-2---------Diethylphthalate 450
7005-72-3-------4-Chlorophenyl-phenylether_ 450
86-73-7---------Fluorene 450
100-01-6--------4-Nitroaniline 2200
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2200
86-30-6---------N-Nitrosodiphenylamine (l)_ 450
101-55-3--------4-Bromophenyl-phenylether __ 450
118-74-1--------Hexachlorobenzena 450
87-86-5---------Pentachlorophenol 2200
85-01-s---------Phenanthrena 450
120-12-7--------Anthracena 450
84-74-2---------Di-n-Butylphthalate 450
206-44-o--------Fluoranthene 450
129-00-0--------Pyrene 450
85-68-7---------eutylbanzylphthalate 450
91-94-1---------3,J'-Dichlorobenzidina 910
56-55-3---------Banzo(a)Anthracene 450
218-01-9--------Chrysene 450
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 450
117-84-o--------Di-n-octyl Phthalate 450
205-99-2--------Benzo(b)Fluoranthe~a 450
207-08-9--------Benzo(k)Fluoranthena 450
50-32-8---------Benzo(a)Pyrena 450
193-39-5--------Indeno(l,2,J-cd)Pyrene 450
53-70-3---------Dibenz(a,h)Anthracena 450
191-24-2--------Benzo(g,h,i)Perylena 450
(1) -Cannot be separated trom Diphenylamina
u
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u u u u
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FORM I sv-2 1/87 Rav.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
SB2-l-l
Lab cc,de: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL
Samplo wt/vol: 30,7 (g/mL) L_
Level:: ( low/med) LOW
I Moi11ture: not dee. ~ dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li,_
~
pH: ..i...!
Number TICS tound: ~
CAS NUMBER COMPOUND NAME
Lab Sample ID: 359870
Lab File ID: GH059870C21
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/11/90
Dilution Factor: -1-,0_o~_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
=-=-=i==::::===:c:1-=-• =-=========================== ======== :a============ •====
1. SOLVENT CONTAMINANT 5.47 640 BJ
2. SOLVENT CONTAMINANT 5.53 600 BJ
3. ALDOL 6.38 550 ABJ
4. UNKNOWN 10.74 180 J
5. UNKNOWN 12.50 830 J
6. UNKNOWN 13.85 460 J
FORM I SV-TIC l/87 Rev.
•--•··---.-..-.-.-.. .... -• -,.._.-..,-.-a ~IIMM,-.OlJ
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
SB2-2-l
Lab code: COMPY case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 359875
Sample wt/vol: J0,5 (g/mL) Ii__ Lab File ID: GH059875A21
Level: (low/med) LOW Date Received: 07/27/90
% Moisture: not dee. _u dee. Date Extracted: 07/J0/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/12/90
GPC Cleanup: (Y/N) li__ pH:~ Dilution Factor: .1~1 0,._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 420 u
lll-44-4--------bis(2-Chloroethyl)Ether 420 u 95-57-8---------2-Chlorophenol 420 u
541-73-1--------l,3-Dichlorobenzene 420 u
106-46-7--------l,4-Dichlorobenzene 420 u
100-51-6--------Benzyl Alcohol 420 u
95-50-1---------1,2-Dichlorobenzene 420 u
95-48-7---------2-Methylphenol 420 u
J9638-32-9------bis(2-Chloroisopropyl)Ether_ 420 u
106-44-5--------4-Methylphenol 420 u
621-64-7-~------N-Nitroso-oi-n-Propylamine_ 420 u
67-72-1---------Hexachloroethane 420 u
. 98-95-3---------Nitrobenzene 420 u
78-59-1---------Isophorone 420 u
88-75-5---------2-Nitrophenol 420 u
105-67-9--------2,4-Dimethylphenol 420 u
65-85-0---------Benzoic Acid 2000 u
lll-9l-l---~----bis(2-Chloroethoxy)Methane_ 420 u
120-83-2----~---2,4-Dichlorophenol 420 u
120-82-1--------l,2,4-Trichlorobenzene 420 u
91-20-3---------Naphthalene 420 u
106-47-8--------4-Chloroaniline 420 u
87-68-3---~-----Hexachlorobutadiene 420 u
59-50-7---------4-Chloro-3-Methylphenol 420 u
91-57-6---------2-Methylnaphthalene 420 u
77-47-4---------Hexachlorocyclopentadiene __ 420 u
88-06-2---------2,4,6-Trichlorophenol 420 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---.------2-Chloronaphthalene 420 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 420 ·u
208-96-8--------Acenaphthyleno 420 u
606-20-2--------2,6-Dinitrotoluene 420 u
-
FORM I SV-1 1/87 Rev.
D
w
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m
m
m
m
m
m
0
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Na1ne: COMPUCHEM, RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SQII:. Lab Sample ID: 359875
Sample wt/vol: 30.5 (g/mL) ~ Lab File ID: GH059875A21
Level: (low/med) LOW Date Received: 07,!27,!90
% Moisture: not dee. -2..3. dee. Date Extracted: 91l'.39L99
Extraction: (SepF/Cont/Sonc) SQHl: Date Analyzed: 08,!12,!9Q
Dilution Factor: &l~,o....._ __
CONCENTRATION UNITS:
GPC Cleanup: (Y/N) li...._ pH: ..§....1
CAS NO. COMPOUND (ug/L or ug/Kg) UG,!KG Q
99-09-2---------3-Nitroaniline 2000 u
83-32-9---------Acenaphthene 420 u
51-28-5---------2,4-Dinitrophenol 2000 u
100-02-1--------4-Nitrophenol 2000 u 132-64-9--------Dibenzofuran 420 u
121-14-2--------2,4-Dinitrotoluene 420 u
84-66-2---------Diethylphthalate 420 u
7005-72-3-------4-Chlorophenyl-phenylether_ 420 u
86-73-7----.-----Fluorene 420 u
100-01-6--------4-Nitroaniline 2000 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 420 u
101-55-3--------4-Bromophenyl-phenylether __ 420 u
118-74-1--------Hexachlorobenzana 420 u
87-86-5---------Pentachlorophenol 2000 u
85-01-8---------Phenanthrene 420 u
120-12-1--------Anthracene 420 u
84-74-2---------Di-n~Butylphthalate 420 u
206-44-0--------Fluoranthene 420 u
129-oo-o--------Pyrena 420 u
85-68-7---------Butylbenzylphthalata 420 u
91-94-1---------3,J'-Dichlorobenzidina 840 u
56-55-3---------Benzo(a)Anthracane 420 u
218-01-9--------Chrysena 420 u
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 87 j
117-84-o--------Di-n-octyl Phthalata 420 u
205-99-2--------Benzo(b)Fluoranthane 420 u
207-08-9--------Benzo(k)Fluoranthene 420 u
50-32-8---------Benzo(a)Pyrana 420 u
193-39-5--------Indano(l,2,J-cd)Pyrene 420 u
53-70-3---------Dibanz(a,h)Anthracene 420 u
191-24-2--------Benzo(g,h,i)Perylena 420 u
' (.L) -cannot be separated from Diphenylamina
FORM I sv-2 1/87 Rev.
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ID
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lP' EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SB2-2-l Lab Name: COHPUCHEM,RTP Contract: C2-BBl~REVS
Lab Code: COHPU Case No.: 20937 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.5 (g/mL) L_
Level: ( low/med) LOW
I Moisture: not dee. ---13.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li._
dee.
~
pH: ....L.2.
SDG No.: _o_s __
Lab Sample ID: ._3._59"8._7...,5'-----
Lab Fila ID: GH059875A21
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/12/90
Dilution Factor: _1-1 0 __ _
Number TICS found: __i
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
•••-==m=--•--=== ---=-=-•=======-=---=-=--=--------==== ------=--=-=-=------== 1. SOLVENT CONTAMINANT 5.42 470 BJ
2. SOLVENT CONTAMINANT 5.50 JOO BJ
J. ALDOL 6.JS JOO ABJ
4. UNKNOWN HEXANEDIOIC ACID EST 15.67 170 J
FORM I SV-TIC 1/87 Rev.
u
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBJ-1-1
Lab Na1ne: COMPUCHEM. RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: S DG No. : .,.0.,.5 __
Matrix: (soil/water) SOIL Lab Sample ID: _3_59~8,._7._4.__ __ _
Sample wt/vol: 30.5 (g/mL) li_ Lab File ID: GJ059874A21
Level: (low/med) ~LO~W..,,__
\ Moisture: not dee. _ll dee.
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/12/90
Dilution Factor: 1.0
Extraction:
GPC Cl,!anup:
(SepF/Cont/Sonc)
(Y/N) li,_
~
pH:~ ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 410
lll-44-4--------bis(2-Chloroethyl)Ether 410
95-57-8---------2-Chlorophenol 410
541-73-1----~---l,J-Dichlorobenzene 410
106-46-7--------1,4-Dichlorobenzene 410
100-51-6--------Benzyl Alcohol 410
95-50-1---------1,2-Dichlorobenzene 410
95-48-7---------2-Methylphenol 410
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410
106-44-5--------4-Methylphenol 410
621-64-7--------N-Nitroso-Di-n-Propylamine_ 410
67-72-1---------Hexachloroethane 410
98-95-3---------Nitrobenzene 410
78-59-1---------Isophorone 410
88-75-5---------2-Nitrophenol 410
105-67-9--------2,4-Dimethylphenol 410
65-85-0---------Benzoic Acid 2000
lll-9l-l-~------bis(2-Chloroethoxy)Methane_ 410
120-83-2--------2,4-Dichlorophenol 410
120-s2-1-------~1,2,4-Trichlorobenzene 410
91-20-3---------Naphthalene 53
106-47-8--------4-Chloroaniline 410
87-68-3---------Hexachlorobutadiene 410
59-50-7---------4-Chloro-3-Methylphenol 410
91-57-6---------2-Methylnaphthalene 410
77-47-4---------Hexachlorocyclopentadiene_ 410
88-06-2---------2,4,6-Trichlorophenol 410
95-95-4----~----2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 410
88-74-4---------2-Nitroaniline 2000
131-11-3--------Dimethyl Phthalate 410
208-96-s-~------Acenaphthylene 410
606-20-2--------2,6-Dinitrotoluene 410
Q
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u u u u u u
u u u u
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u u u
J u u u
u u u
u u u u u
u
FORM I sv-1 1/87 Rev.
--··--· --.-. ..-. --· ·-.'""lol"'\,11
,
0
0
m
D
0
D
0
I
D
0
D
D
D
D
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D
D
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBJ-1-1 Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU Casa No.: 20937 SAS No.: SDG No.: .,.0.,.5 __
Matrix: (soil/water) SOIL Lab Sample ID: ..,_3..,_59~8._7i.;4L-__ _
Sample wt/vol: 30.5 (g/mL) !i'..__ Lab File ID: GJ059874A2l •
Level: (low/med) -LO=W __ Date Received: 07/27/90
t Moisture: not dee. __l,Q dee. Date Extracted: 07/30/90
Extraction: (SepF/Cont/Sonc) S,OHC Date Analyzed: 08/12/90
GPC. Cleanup: · (Y/N) Ii_ pH: j...i Dilution Factor: Al~, ... o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------J-Nitroaniline 2000
83-32-9---------Acenaphthene 410
51-28-s--~------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 410
121-14-2--------2,4-Dinitrotoluene 410
84-66-2---------Diethylphthalate 410
7005-72-3-------4-Chlorophenyl-phenylether_ 410
86-73-7----~----Fluorene 410
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000
86-30-6---------N-Nitrosodiphenylamine (l)_ 410
101-55-3--------4-Bromophenyl-phenylether __ 410
118-74-1--------Hexachlorobenzene 410
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthrene 410
120~12-1--------Anthracene 410
84-74-2---------Di-n-Butylphthalate 410
206-44-0--------Fluoranthene 410
129-oo-o-~------Pyrena 410
85-68-7-----~---Butylbenzylphthalate 410
91-94-1---------3,3'-Dichlorobenzidine 810
56-55-3---------Benzo(a)Anthracene 410
218-01-9--------chrysene 410
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 410
117-84-0--------Di-n-octyl Phthalate 410
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 410
50-32-a---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 410
53-70-3---------Dibenz(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
-(l) -cannot be separated from Diphenylamine
Q
u u u u u u u u u u u u u u
u u u u u u u u u u u u u u u u u u
FORM I sv-2 1/87 Rev.
m
m
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0
D
0
g
g
I
g
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEM.RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
SBJ-1-1
Lab Code: COHPU Case No.: 20937 SAS No.: SDG No.: os
Matrix: (soil/water) SOIL
Sample wt/vol: 30.5 (g/mL) L_
Level: (low/med) _LO~W~-
I Moisture: not dee. ___l,Q
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti_
Number TICS found: __l
dee.
SOliC
pH: --5.....§.
CAS NUMBER COMPOUND NAME
Lab Sample ID: 359874
Lab File ID: GJQ59874A21
Date Received: 07/27/90
Date Extracted: 07/30/90
Date Analyzed: 08/12/90
Dilution Factor: alL.o,.._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
••••:a:••=-=-•==-•a•• ---===-=====-===-====-•==-==-==•=-:::s::::a:a::111=-•== :a=====-==-=-==•= ---== 1. ALDOL 6.35 490 ABJ
2. UNKNOWN 10.22 250 J
3. TETRAMETHYLBUTYLPHENOL ll.64 290 J
::::A
FORM I SV-TIC 1/87 Rev.
.-.-. ~ r-..-.T, -11MM u r:;
'
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m
n
R
m
m
0
D
I I
D
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u
•
1B
SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-BBJ-REVS
SBJ-2-1
Lab Code: COMPU Case No.: 20937 SAS.No.: SDG No.: 05
Matrix: ( soil/water) sou, Lab Sample ID: 359873
Sample \ wt/vol: 30.8 (g/mL) !L._ Lab File ID: GJ059873A21
Level: (low/med) LOW Date Received: 07/27/90
t Moisture: not dee. ---1..9. dee. Date Extracted: 07/30/90
Extraction: (SepF/Cont/Sonc) .s.9fil: Date Analyzed: 08/12/90
Dilution Factor: ~i~,~o~o __
CONCENTRATION UNITS:
GPC ClE1anup: (Y/N) lf_ pH: -5J
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 400 u lll-44-4--------bis(2-Chloroethyl)Ether 400 u 95-57-8---------2-Chlorophenol 400 u 541-73-1--~-----l,3-Dichlorobenzene. 400 u
106-46-7--------1,4-Dichlorobenzene 400 u 100-51-6--------Benzyl Alcohol 400 u
95-50-1---------1,2-Dichlorobenzene 400 u
95-48-7---------2-Methylphenol 400 u
39638-32-9------bis(2-Chloroisopropyl)Et~er_ 400 u
106-44-5--------4-Methylphenol 400 u
521-64-7--------N-Nitroso-Di-n-Propylamine_ 400 u
57-72-1---------Hexachloroethane 400 u
98-95-3---------Nitrobenzene 400 u
78-59-1---------Isophorone 400 u
88-75-5---------2-Nitrophenol 400 u.
105-67-9--------2,4-Dimethylphenol 400 u
65-85-o---------Benzoic Acid 1900 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 400 u
120-sJ-2--------2,4-Dichlorophenol 400 u
120-s2-1--------1,2,4-Trichlorobenzene 400 u
91-20-3---------Naphthalene 400 u
106-47-8--------4-Chloroaniline 400 u
!17-68-3---------Hexachlorobutadiene 400 u
59-50-7.---------4-Chloro-3-Methylphenol 400 u
91-57-6---------2-Methylnaphthalene 400 u
77-4 7.-4---------Hexachlorocyclopentadiene __ · 400 u
88-06-2-----~---2,4,6-Trichlorophenol 400 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
91-58-7---------2-Chloronaphthalene 400 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalat• 400 u
208-96-8--------Acenaphthylene 400 u
506-20-2--------2,6-Dinitrotoluene 400 u
FORM I sv-1 1/87 Rev.
D
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g
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u
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBJ-2-1 Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 359873
Sample wt/vol: 30.8 (g/mL) g__ Lab File ID: Si,Z05987JA21
Level: (low/med) LOW Date Received: 07/27/90
% Moisture: not dee. ---1.9. dee. Date Extracted: 07/30/90
Extraction: (SepF/Cont/Sonc) Date Analyzed: 08112/90
GPC Cleanup: (Y/N) Ii._ pH:~ Dilution Factor:l A~•~o~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------J-Nitroaniline 1900 u
83-32-9---------Acenaphthene 400 u
51-28-5---------2,4-Dinitrophenol 1900 u
100-02~1--------4-Nitrophenol 1900 u
132-64-9--------Dibenzofuran 400 u
121-14-2--------2,4-Dinitrotoluene 400 u
84-66-2---------Diethylphthalate 400 u
7005-72-3-------4-Chlorophenyl-phenylether_ 400 u
86-73-7---------Fluorene 400 u
100-01-6--------4-Nitroaniline 1900 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 1900 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 400 u
101-55-3--------4-Bromophenyl-phenylether __ 400 u
118-74-1--------Hexachlorobenzene 400 u
87-86-5---------Pentachlorophenol 1900 u
ss-01-s---------Phenanthrene 400 u
120-12-1--------Anthracene 400 u
84-74-2---------Di-n-Butylphthalate 400 u
206-44-o--------Fluoranthene 400 u
129-00-0--------Pyrene 400 u
85-68-7---------Butylbenzylphthalate 400 u
91-94-1---------3,3'-Dichlorobenzidine 790 u
56-55-3---------Benzo(a)Anthracene 400 u
218-01-9--------Chrysene 400 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 400 u
117-84-0--------Di-n-Octyl Phthalat• 400 u
205-99-2--------Benzo(b)Fluoranthene 400 u
207-08-9--------Benzo(k)Fluoranthene 400 u
50-32-8---------Benzo(a)Pyren• 400 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 400 u
53-70-3---------Dibenz(a,h)Anthracene 400 u
191-24-2--------Benzo(g,h,i)Perylene 400 u
(1) -cannot be separated from Diphenylamine
FORM I SV-:Z 1/87 Rev.
.1
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
583-2-1
No.: 05
359873
sample, wt/vol: 30.8 (g/mL) L_ Lab File ID: GJ059873A21
Level: (low/med) LOW ' Date Received: 07{'.27{'.90
\ Moisture: not dee. ----1.9. dee. Date Extracted: 07 ,:'.30{'.90
Extraction: (SepF/Cont/Sonc) SQfil: Date Analyzed: 08,:'.12{'.90
GPC Cleanup: (Y/N) li,._ pH:~ Dilution Factor: Al~,O~O.__
CONCENTRATION UNITS:
Number TICs found: --3. (ug/L or ug/Kg) UG{'.KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
=•z====•======== •=•======~========•====-----•:a:a•=•=-•••••===m•••• ---== l. SOLVENT CONTAMINANT 5.43 360 BJ
2. ALDOL 6.35 480 ABJ
3. UNKNOWN 13.69 200 J
FORM I SV-TIC 1/87 Rev.
51
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MWll-7S-lMS Lab Name: COMPUCHEM,RTP Contract: /2-881-REVS
Lab cc,de: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matri>:: (soil/water) SOIL Lab Sample ID: 358136
SamplEI wt/vol: 30.1 (g/mL) L_ Lab File IO: GH058136B21
Level: (low/med) LOW Data Received: 07/21/90
% Moisture: not dee.~ dee. Date Extracted: 07/2~/90
Extraction: (SepF/Cont/Sonc)
(Y/N) li,_
~
pH: ....2.a..1
Date Analyzed: 08/08/90
GPC Cleanup: Dilution Factor: .1~1~0 __ _
.
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 410
lll-44-4--------bis(2-Chloroethyl)Ether 410
95-57-8---------2-Chlorophenol 410
541-73-1--------1,3-Dichlorobenzene 410
106-46-7--------1,4-Dichlorobenzene 410
100-51-6--------Benzyl Alcohol 410
95-50-1---------1 2-Dichlorobenzene . , 410
95-48-7---------2-Methylphenol 410
39638-32-9-~----bis(2-Chloroisopropyl)Ether_ 410
106-44-5--------4-Methylphenol 410
621-64-7--------N-Nitroso-Di-n-Propylamine __ 410
67-72-1---------Hexachloroethane 410
98-95-3---------Nitrobenzene 410
78-59-1---------Isophorone 410
88-75-5------~--2-Nitrophenol 410
105-67-9--------2,4-Dimethylphenol 410
65-85-o---------Benzoic Acid 2000
111·-91-1--------bis ( 2-Chloroethoxy) Methane_ 410
120-83-2--------2,4-Dichlorophenol 410
120-82-1-~------1,2,4-Trichlorobenzene 410
91-20-3---------Naphthalene 410
106-47-8--------4-Chloroaniline 410
87-68-3---------Hexachlorobutadiene 410
59-50-7---------4-Chloro-3-Methylphenol 410
91-57-6---------2-Methylnaphthalene 410
77-47-4---------Hexachlorocyclopentadiene_ 410
88-06-2---------2,4,6-Trichlorophenol 410
95-95-4---------2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 410
88-74-4---------2-Nitroaniline 2000
131-11-3--------Dimethyl Phthalate 410
208-96-8--------Acenaphthylena 410
606-20-2--------2,6-Dinitrotoluene 410
Q
u u u u
·U
u
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u
u
u
u u u
u
u
u
u
u
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
FORM I sv-1 1/87 Rev.
.-.. -.-. ,-I
u
H
I
I
m
ffl
m
m
D
lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM, RTP Contract: (2-881-REVS
MW13-7S-1MS
Lab code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 358136
Sample wt/vol: 30.1 (g/mL) L_ Lab File ID: GH0581J6B21
Level: .(low/med) LOW Date Received: 07/21/90
% Moisture: not dee. _.2.Q dee. Date Extracted: 01tHt20
Extraction: Date Analyzed: 08/08/90
GPC Cluanup:
(SepF/Cont/Sonc)
(Y/N) ti_
S.Qfil:
pH:~ Dilution Factor: ~1~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------J-Nitroaniline 2000
83-32-9---------Acenaphthene 410
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 410
121-14-2--------2,4-Dinitrotoluene 410
84-66-2---------Diethylphthalate 410
7005-72-3-------4-Chlorophenyl-phenylether_ 410
86-73-7---------Fluorene 410
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000
86-30-6----~----N-Nitrosodiphenylamine (l)_ 410
101-55-3--------4-Bromophenyl-phenylether __ 410
118-74-1--------Hexachlorobenzene 410
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthrene 410
120-12-1--------Anthracene ' 410
84-74-2---------Di-n-Butylphthalate 410
206-44-o--------Fluoranthene 410
129-00-0--------Pyrene 410
85-68-7---------Butylbenzylphthalate 410
91-94~1---------3,J'-Dichlorobenzidine 820
56-55-3---------Benzo(a)Anthracene 410
218-01-9--------Chrysene 410
117-8l-7--------bis(2-Ethylhexyl)Phthalate_ 410
117-84-o--------Di-n-octyl Phthalate 410
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 410
50-32-8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 410
53-70-3---------Dibenz(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
-(l.) -cannot be separated from Diphenylamin•
Q
u u u u
u
u u u
u
u u u u
u u u u u
u u u u
u
u u u u u
u
u u u
•
FORM I sv-2 1/87 Rev.
......... -.'"'I,, -· ·-.-. ..... ,11 ,::..
I
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iR
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS MWll-7S-lMSD
Lab Code: COMPU Case No.: 209,37 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 358137
Sample wt/vol: 30,1 (g/mL) L-Lab File ID: GH0581J7B2L
Level: (low/med) LOW Date Received: 07/21/90
t Moisture: not dee. ---2Jl. dee. Date Extracted: 07/2~/9Q
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/08/9Q
GPC Cleanup: (Y/N) li.,_ pH: ....i....1 Dilution Factor: ,.1.,.. • .,.0 __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 410 u lll-44-4--------bis(2-Chloroethyl)Ether 410 u 95-57-8---------2-Chlorophenol 410 u
541-73-1--------1,l-Dichlorobenzene 410 u 106-46-7--------1,4-Dichlorobenzene 410 u 100-s1~6--------eenzyl Alcohol 410 u
95-50-1---------1,2-Dichlorobenzene 410 u
95-48-7---------2-Methylphenol 410 u l9638-l2-9------bis(2-Chloroisopropyl)Ether_ 410 u
106-44-5--------4-Methylphenol 410 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 410 u
67-72-1---------Hexachloroethane 410 u
98-95-3---------Nitrobenzene 410 u
78-59-1---------Isophorone 410 u
88-75-5---------2-Nitrophenol 410 u
105-67-9--------2,4-Dimethylphenol 410 u
65-85-o---------eenzoic Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 410 u
120-83-2--------2,4-Dichlorophenol 410 u
120-e2-1--------l,2,4-Trichlorobenzene 410 u
91-20-3---------Naphthalene 410 u
106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7---------4-Chloro-l-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47-4---------Hexachlorocyclopentadiene __ · 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 410 u
88-74-4---------2-Nitroaniline 2000 u
131-11-J--------Dimethyl Phthalate 410 u
208-96-8--------Acenaphthylene 410 u
606~20-2--------2,6-Dinitrotoluene 410 u
-
FORM I sv-1 1/87 Rev.
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u
g
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: {2-88)-REVS MW13-7S-1MSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 05
Matrix: (soil/water) SOIL Lab Sample ID: 358137
Sample wt/vol: 30.1 (g/mL) !......_ Lab Fila ID: GH058137B21
Level: (low/med) LOW Data Received: 07/21/90
I Moisture: not dee. ---2..Q dee. Data Extracted: 07/2~/20
Extract,ion: (SepF/Cont/Sonc) SOfil: Date Analyzed: 08/08/90
Dilution Factor: ~i~,o.._ __
CONCENTRATION UNITS:
GPC ClE1anup: (Y/N) tl,_ pH: ~
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
-
99-09-2---------3-Nitroaniline 2000 u
83-32-9---------Acenaphthene 410 u
51-28-5---------2,4-Dinitrophenol 2000 u
100-02-1--------4-Nitrophenol 2000 u
132-64-9--------Dibenzofuran 410 u
121-14-2--------2,4-Dinitrotoluena 410 u
84-66-2---------Diethylphthalate 410 u
7005-72-3-------4-Chlorophenyl-phenylether __ 410 u
86-73-7---------Fluorene 410 u
100-01-6--------4-Nitroanilina 2000. u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 410 u
101-55-3--------4-Bromophenyl-phanylethar __ 410 u
118-74-1--------Hexachlorobenzana 410 u
87-86-5---------Pentachlorophenol 2000 u
85-01-8---------Phenanthrana 410 u
120-12-1--------Anthracane 410 u
84-74-2---------Di-n-Butylphthalate 410 u
206-44-0--------Fluoranthena 410 u
129-00-0--------Pyrana 410 u
85-68-7---------Butylbanzylphthalate 410 u
91-94-1---------J,J'-Dichlorobenzidine 820 u
56-55-3---------Benzo(a)Anthracene 410 u
218-01-9--------Chrysana 410 u
117-81-7--------bis(2-Ethylhexyl)Phthalata_ 410 u
117-84-o--------Di-n-octyl Phthalate 410 u
205-99-2--------Benzo(b)Fluoranthena 410 u
207-08-9--------Banzo(k)Fluoranthene 410 u
50-32-8---------Benzo(a)Pyrene 410 u
193-39-5--------Indano(l,2,J'-cd)Pyrena 410 u
53-70-3---------Dibanz(a,h)Anthracena 410 u
191-24-2--------Benzo(g,h,i)Perylene 410 u
(1) -Cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rav.
20937 05 SAMPLEt DATA SUMMARY
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SAMPLE: TB-6-1
Q)MPUCHEM
IABORATORIES
CLP CASE NARRATIVE CASE# 20937
CONTRACT# 2-88 (REVS) SDG# 07
COMPUCHEM LABORATORIES INC.
This portion of Case# 20937 consisted of one liquid sample
It was received intact on
a properly sealed shipping for volatile analysis only.
7/25/90 via Federal Express in
container with a traffic reports.
VOLATILES:
All volatile fractions were analyzed within holding time
requirements. The sample contained methylene chloride (also
detected in the associated instrument blank) at less than
CRQL. All surrogates met recovery criteria. Because the
sample was designated as a blank, there were no QC spikes.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than the conditions detailed
above. Release of the data contained in this hardcopy data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
Note: This report was paginated for reference and
accountability .in decreasing numerical sequence.
Sarah A. Hubbard 8/30/90
Technical Reviewer
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
m Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
TB-6-1
Lab Code: COMPU .case No.: 20937 SAS No.: SDG No, :" ~07..___
Matrix: (soil/water) WATER Lab Sample ID: 359035
m Sample wt/vol: 5,0 (g/mL) Ml,__ Lab File ID: CN059035Al8
Level: (low/med) LOW Date Received: 07/25/90
m \ Moisture: not dee. Date Analyzed: 08/02/90
m
m
m
m
m
n
D
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Column: (pack/cap) CAP Dilution Factor: .1L1~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 3 BJ
67-64-1------~--Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3------~--Chlorotorm 5 u
107-06-2--------1,2-Dichloroethane 5 u
~B-93-3---------2-Butanone 10 u
71-55-6--~------l,l,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
100-os-4--------vinyl Acetate 10 u
75-27-4---------Bromodichloromethane . 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------ci~-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------eanzene 5 u
10061-02-6------Trana-l,3-Dichloropropene __ 5 u
75-25-2---------Bromotorm 5 u
100-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone -10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---~-----1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
-
FORM I VOA 1/87 Rev.
D Ti=I SUM i=IR'·' _
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Na111e: COMPUCHEM, RTP Contract: 12-88)-REVS
TB-6-l
Lab Code: COMPU Case No.: 20937 SAS No. : ___ SDG No. : .,..o.,_7 __
Matrix: (soil/water) WATER
Sample wt/vol: 5.0
Level: (low/med) ,..LO...,w,..__
I Moisture: not dee.
Column (pack/cap) ,..CAci,P.___
Number TICs found: _Q
Lab Sample IO: ,._3,._5,._90,._3._5.__ __ _
(g/mL) ~ Lab File IO: CN059035Al8
Date Received: 07/25/90
Date Analyzed: 08/02/90
Dilution Factor: .1~1 0,._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
----------------•-••••••=========•m===•s•••• ------------------------==
'\
FORM I VOA-TIC l/87 Rev.
20937 07 SAMPLE DATA SUMMAR~ l ,
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SAMPLE NUMBERS:
WMPUCHEM
lABORATORlES
CASE NARRATIVE CASE #20937
SDG #22 CONTRACT #(2-88)REVS
COMPUCHEM LABORATORIES, INC.
MW2A-6S-l
SBS-1-1
SB9-l-l
SB12-l-l
SBS-2-1
SB9-2-l
SB4-l-l
SB6-l-l
SB4-2-l
SB6-2-l
The samples listed above were received intact on 7-28-90 and
8-1-90 with the chain-of-custody documents in order and all
shipping containers properly sealed. This narrative
summarizes the analysis• of these ·ten solid samples for
volatiles and semivolatiles.
Volatiles:
All sample and QC fractions were extracted within holding
times except for the repeat analyses of SB4-l-l, 5B4-2-1,
SBS-1-1, SBS-2-1, SB6-l-l, and the medium level analysis of
SB9-l-l. The samples co~tained a variety of target list
compounds (TCLs) including methylene chloride, acetone,
2-butanone, 4-methyl-2-pentanone, 2-hexanone, 1,1-
dichloroethane, toluene, and 1,2-dichloroethene (reported as
total isomers). Few samples contained tentatively
identified compounds (TICs). Repeat analyses were performed
for samples SB4-l-l, SB4-2-l, and SBS-2-1 because the
surrogate D4-1,2-dichloroethane initially failed surrogate
recovery criteria. These initial analyses were performed
within holding times; however, the repeat analyses could not
be. Also for sample SB4-l-l, tetrachloroethene showed
possible inhomogeneous results. Sample SBS-1-1 initially
had a noise peak and required reanalysis. The reanalysis
could not be prerformed within holding times, but the
results bwetween the two analyses agreed well. Samples SB6-
l-l, SB6-2-l, and SB9-2-l required repeat anal¥ses due to
TCLs being outside the upper limit of the analytical range.
For sample SB6-l-l when the sample was reanalyzed undiluted
using a different bottle, the TCLs, 2-butanone and 4-methyl-
2-pentanone(initially outside the analytical range) were not
detected. This discrepancy was attributed to differences
between the two bottles. Samples SB6-2-l and SB9-2-l
required reanalyses at medium levels. Discrepancies between
the TCLs detected between the two analyses of these two
samples have been attributed to differences between the low
level solid purge and trap method and the medium level
methanol extraction procedure and/or sample inhomogeneity.
Page - 1
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 [phone]
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CbMPUCHEM
IABOAATORJES
For sample SB9-2-l this resulted in 2-butanone being
reported with a value outside the analytical range.
All sample and QC fractions met the surrogate recovery
criteria except those previously mentioned. Both the medium
and low level matrix spike duplicates met all accuracy and
precision criteria. All associated method 'blanks met all QC
criteria. ·
Semi volatiles:
All sample and QC fractions were extracted within holding
times. Few samples contained TCLs at concentrations greater
than the contract required quantitation limit (CRQL). Many
samples contained numerous TICs. For sample SBS-1-1 the
sixthe internal standard, d12-perylene, had a slightly high
response. The extract went to dryness before a suitable
confirmational injection was made, and insuficient sample
remained to reextract. 'All sample and QC fractions met the
surrogate recovery criteria. However in sample SB9-l-l
tribromophenol showed a high recovery. The matrix spike
duplicates met all accuracy and precision criteria. All
associated method blanks met all QC criteria.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than conditions detailed above.
Release of the data contained in the hardcopy data package
and in the computer-readable data submitted on the floppy
diskette has been authorized by the Laboratory Manager or
his designee, as verified by the following signature.
ELISABETH ROBINS NOWELL
DATE 08/31/90
TECHNICAL REVIEWER
Note: This report is paginated for reference and
accountability in decreasing numerical sequence.
Note: The "X" footnote denotes the coelution of
indi'stinguishable isomers.
Page -2
f"'("\l..tDI lf""UC:i,,.,t I liCl.l""ICATl"\OIC:C 1'-11"" D l"'I c .... v 1".lt:.i:::".I 'l'llnJ:tt"'h<11nal 1-1aI111.1 .. 1 ......... u: ........ , ..... o ........... ,.h T•innnr ... 0 ... 1, "-lf""'l77na 10101 "-AO_Q'}l::'l
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: C2-88l-REVS MW2A-6S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matri>c: (soil/water) SOIL Lab Sample ID: 360294
Samplu wt/vol: s,o (g/mL) ~ Lab File ID: GHO§Q294Cl2
Level: (low/med) LOW Date Received: 07/28/90
, Moi~1ture: not dee. ---22 Date Analyzed: 08(Q8(90
Column: (pack/cap) CAP Dilution Factor: al~1~Q __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 39 B 67-64-1---------Acetone 47 B 75-15-0---------carbon Disulfide 7 u 75-35-4---------1,1-Dichloroethene 7 u 75-34-3---------1,1-Dichloroethane 7 u 540-59-0--------1,2-Dichloroethene (total)_ 7 u 67-66-3---------Chloroform 7 u 107-06-2--------1,2-Dichloroethane 7 u 78-93-3---------2-Butanone 4 BJ 71-55-6----~----l,l,l-Trichloroethane 7 u 56-23-5---------carbon Tetrachloride ·7 u 108-05-4---~----Vinyl Acetate 13 u 75-27-4---------Bromodichloromethane 7 u 78-87-5---------1,2-Dichloropropane 7 u 10061-01-s------cis-l,3-Dichloropropene 7 u 79-01-6---------Trichloroethene 7 u 124-48-1--------Dibromochloromethane 7 u 79-00-5---------l,l,2-Trichloroethane 7 u 71-43-2---------Benzene 7 u 10061-02-6------Trans-l,3-Dichloropropene __ 7 u 75-25-2---------Bromoform 7 u 1oa-10-1--------4-Methyl-2-Pentanone 13 u 591-78-6--------2-Hexanone 13 u 127-18-4--------Tetrachloroethene 7 u 79-34-5---------1,1,2,2-Tetrachloroethane __ 7 u 108-88-3--------Toluene 7 u 108-90-7--------Chlorobenzene 7 u 100-41-4--------Ethylbenzene 7 u 100-42-5--------styrene 7 u 1330-20-7-------Total Xylenes 7 u
-
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP
Lab cc,de: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dee. --ll
Column (pack/cap) CAP
Number TICs found: __Q
CAS NUMBER COMPOUND
MW2A-6S-l Contract: 12-881-REVS
SAS No.: SDG No.: -.22.,__
L_
NAME
Lab Sample ID: .._3 ,._6 o,,_2,..9,_,4L-__ _
. Lab File ID: GH060294Cl2
Date Received: 07/28/90
Date Analyzed: 08/08/90
Dilution Factor: .1L,o,._ __
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ••:a===:==-•=•a==:a• =-•========================== ••===:a:aa =-=====:;z•=:11••= =-====
FORM I VOA-TIC l/87 Rev.
.-""' .... ,.., r-"-1"'\T'l"'II eJ 1MMnou -----.......... .
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VOLATILE ORGANICS ANALYSIS DATA SHEET · EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS S812-1-1
Lab Cede: CQMPU Case No.: 20937 SAS No.: SDG No.: .2_2~-
Matrix: ( soil/water) SOIL Lab Sample ID: 360858
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GR060858Al~
Level: (low/med) LOW Date Received: 08/01/90
t Moisture: not dee. ___u Date Analyzed: 08/10/90
Column: (pack/cap) CAP Dilution Factor: &1~1 0,._ __
CAS NO. COMPOUND
74-87-3---------Chlorcmethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,l-Dichlorcethane
,540-59-0--------1,2-Dichlorcethene
67-66-3---------Chlorcform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------1,l,l-Trichlorcethane
56-23-5----~----carbcn Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Brcmcdichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,J-Dichlorcpropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2~Trichloroethahe
71-43-2---------Benzene
10061-02-6------Trans-l,J-Dichlorcpropene __
75-25-2---------Bromoform
1os-10-1--------4-Methyl-2-Pentancne
591-78-6--------2-Hexanone
127-18-4--------Tetrachlorcethene
79-34-5---------1,1,2,2-Tetrachloroethana __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
15 u
15 u
15 u
15 u
28 B
70 B
8 u
8 u
4 J
8 u
8 u
8 u
12 BJ
8 u
8 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
52
3 J
8 u
8 u
5 J
8 u
8 u
8 u
8 u
FORM I VOA 1/87 Rev.
,.. ..... ,-,ou
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.1..0: EPA SAMPU NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: coMPUCHEM,RTP Contr'act: (2-88)-REVS SB12-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _2_2 __
Matrix: (soil/water) SQIL
samplu wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. __.ll
ColUJD.1'11 (pack/cap) CAP
Number TICs round: _3_
CAS NUMBER
(g/mL) L_
COMPOUND NAME
Lab Sample ID: ,,_3,._6,._0 8,._5...,8.__ __ _
Lab File IO: GR06oasai',12
Date Received: 08/01/90
Date Analyzed: 08/10/90
Dilution Factor: _1~1 0 __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ••=••=a••======= •=•--z:::1•=•=======•===-•======•. 11:n::a=ia===-::a ==~=======-•=-=-===== 1. ALCOHOL 10.00 29 J 2. UNKNOWN HYDROCARBON 14. 74 22 J 3. LABORATORY ARTIFACT 1.00 15 J
FORM I VOA-TIC , 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88l-REVS SB4-l-l
Lab Code: COMPU case No.: 20937 SAS No.: SOG No.: .2_.2 __
Matrix: (soil/water) SOIL Lab Sample IO: ,.J.,.6.,._0_.,.2,._8"'-2 __ _
Sample wt/vol: S,O (g/mL) SL__ Lab File IO: GH060282Cll Level: (low/med) LOW
I Moisture: not dee. ---1.0.
Date Received: 07/28/90
Date Analyzed: 08/07/90
Dilution Factor: ~i~·~0c....... __
Column: (pack/cap) ca_p
CONCENTRATION UNITS: CAS NO, COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u 74-83-9---------Bromomethane 12 u' 75-01-4---------vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u ~5-09-2---------Methylene Chloride 22 B 67-64-1---------Acetone 35 B 75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-0ichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-oichloroethene (total)_ 6 u 67-66-3---------chlorofot111 6 u 107-06-2--------1,2-0ichloroethane 6 u 78-93-3---------2-Butanone 12 u 71-55-6---------1,1,1-Trichloroethane 6 u 56-23-5---------carbon Tetrachloride 6 u 108-05-4--------Vinyl Acetate ·12 u 75-27-4---------Bromodichloromethane 6 U. 78-87-5---------1,2-Dichloropropane 6 u 10061-01-s------cis-l,J-Oichloropropene 6 u 79-01-6---------Trichloroethene 6 u 124-48-1--------0ibromochloromethane . 6 u 79-00-5---------1,1,2-Trichloroethane 6 u 71-43-2--------~Benzene 6 u 10061-02-6------Trans-l,3-0ichloropropene_ 6 u 1s-2s-2---------Bromofot111 6 u 1oa-10-1--------4-Methyl-2-Pentanone 12 u 591-78-6--------2-Hexanone 12 u 127-18-4--------Tetrachloroethene 21 79-34-5---------1,1,2,2-Tetrachloroethane_ 6 u 108-88-3--------Toluene 6 u 108-90-7--------Chlorobenzene 6 u 100-41-4--------Ethylbenzene 6 u 100-42-5--------styrene 6 u lJJo-20-1-------Total Xylenes 6 u
FORM I VOA 1/87 Rav.
14?
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: ( soil/water) SOIL Lab Sample ID:
S84-1-l
No.: 22
360282'
SamplB wt/vol: 5.0 (g/mL) ~ Lab File IC: GH0602s2c11
Level: · (low/med) LOW
t Moisture: not dee. -1.Q
Column (pack/cap) CAP
Number TICs tound: ~
CAS NUMBER COMPOUND NAME
Data Received: 07/28/90
Data Analyzed: Q8/Q7/90
Dilution Factor: &1~1 0._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q =a•======••=~=== •m========================•• •==•=•== aa====-=-•=•=n• --===
FORM I VOA-TIC l/87 Rav.
-

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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REVS SB4-l-1RE
Lab Cclde: CQMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrilc: (soil/water) SQIL Lab Sample ID: 360282
Sampl11 wt/vol: 5.0 (g/mL) L_ Lab File ID: 1i3R60282CU
Level: (low/med) LOW Date Received: 07 /28/90
% Moi!1ture: not dee. _ll Date Analyzed: 08/23/90
Column: (pack/cap) CAP Dilution Factor: .i~,-0 __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) Uli(KG Q
74-87-3---------Chloromethane 12 u 74-83-9---------Bromomethane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride 6 BJ 67-64-1---------Acetone 28 B · 75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-Dichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3---------Chloro!orm 6 u 107-06-2--------1,2-Dichloroethane 6 u 78-93-3---------2-Butanone 12 u 71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon'Tetrachloride 6 u 108-05-4--------vinyl Acetate 12 U·
75-27-4---------Bromodichloromethane 6 u 78-87-5---------1,2-Dichloropropane 6 u
10061-0l-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------l,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromotorm 6 u
1O0-1O-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
F.ORM I VOA 1/87 Rev.
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EPA SAMPLE NO .
Lab Name: COMPUCHEM,BTP
Lab Code: COMPU Case No.: 20937
Matri>c: (soil/water) SOIL
Samplia wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
, Moisture: not dee. -2..Q
Column (pack/cap) CAP
Number TICs found: .__Q
CAS NUMBER COMPOUND
SB4-l-1RE Contract: C2-88l-REVS
SAS No.: SOG No.: -.22..___
!£..._
NAME
Lab Sample IO: 360282
Lab File IO: G3R60282Cll
Date Received: 07/28/90
Date Analyzed: 08/23/90
Dilution Factor: &1~1 0._ __
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ---•===========-m•=•======================== •=-=====ua =====••-=-=•== ===== •.
FORM I VOA-TIC 1/87 Rev.
l. ---L---JI• -----_,,_ .... ~r'\-11 t "'!' Q
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB4-2-l Lab Name: COMPUCHEM,RTP Contract: C2-BBl-Reys
_Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample IO: 360289
Samplca wt/vol: 5.0 (g/mL) L-Lab File ID: ' GH060289Cll
Level: (low/med) LOW Date Received: 07/28/90
t Moisture: not dee. ___li Date Analyzed: os10119Q
Column: (pack/cap) CAP Dilution Factor: _1~1 _0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane ~ 12 u
75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 21 B
67-64-1---------Acetone 54 B
75-15-0---------carbon Disulfide 6 u
75-35-4-----~---l,l-Dichloroethene 6 u
75-34-3---------1,l-Dichloroethane 6 u
540-59-o--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-oichloroethane 6 u
78-93-3---------2-Butanone 3 BJ
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------Carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------l,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6---~~-Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oe-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------l,l,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-1-------Total Xylenes 6 u
.
FORM I VOA l/87 Rev.
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EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS S84-2-l
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
SAS No.: SDG No.: _2._2 __
Lab Sample ID: A3-6Ao_2s_9~---
Sample wt/vol: 5,0 (g/mL) G,__ · Lab File ID: GH060289Cll
LeveJ.: (low/med) ,..LO""Wl-...._
I Mol.sture: not dee. --1.9_
Column (pack/cap) ,..CA..,P....__
Number TICs found:~
CA s NUMBER COMPOUND NAME
Date Received: 07/28/90
Date Analyzed: 08/07/90
Dilution Factor: .1~1 _0 __
CONCENTRATION UNITS:
(ug/L or ug/l<g) UG/KG
RT EST. CONC. Q ----•:m:m•a=••a••= :a•===•======m=•===••==•••••• •===:a•:a• ••:a••:a•------:a:am==
I
FORM I VOA-TIC 1/87 Rev.
II 2~7 2j SAMPL~..£ATA SUMMARY 137
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS SB4-2-1RE
Lab code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360289
Sample wt/vol: 5.0 (g/mL) !L._ Lab File ID: G3R§0289Cll
Level: (low/med) 1,QW Date Received: 07/28/90
, Moisture: not dee. --1..i Date Analyzed: 08/23/90
Column: (pack/cap) CAP Dilution Factor: .i~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u 74-83-9---------Brornornethane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride 9 B 67-64-1---------Acetone 33 B 75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-Dichloroethene 6 u 75-34-3-------~-l,l-Dichloroethane 6 u
540-59-o--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u 75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6. u
79-01-6---------Trichloroethene . 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4-Methyl-2-Pentanone 12 u
591~78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-1-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
. Level: (low/med) LOW
I Moisture: not dee. _li
Column (pack/cap) CAii!
Number TICs found: __Q
CAS.NUMBER COMPOUND
S84-2-lRE contract: 12-88)-REVS
L_
NAME
SAS No.: SOG No.: 22
Lab Sample IO: 360289
Lab File ID: G3R60289Cll
Date Received: 07/28/90
Date Analyzed: 08/23/90
Dilution Factor: .1~1 ~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
.z:n:ac::===========m •========================a== --====== =:a==-=====•--=-====
FORM I VOA-TIC 1/87 Rev.
--... ~1"'11,
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS SB5-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: ( soil/water) SQJ:I:. Lab sample ID: 360290
Sample wt/vol: s.o (g/mL) ~ Lab File ID: GH06029oc11
Level: (low/med) 1:.QW Date Received: 07/28/90
I Moisture: not dee. ___l.l Date Analyzed: 08/Q7/9Q
Column:-(pack/cap) CAP Dilution Factor: .i~·~o __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67~64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------l,l-Dichloroethene
75-34-3---------1,l-Dichloroethane
540-59-o--------l,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------l,2-Dichloroethane
"78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------l,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1------~-0ibromochloromethane
79-00-s---------l,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1.os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
ll u
ll u
ll u
ll u
20 B
34 B
6 u
6 u
6 u
6 u
6 u
6 u
2 BJ
6 u
6 u
ll u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
ll u
ll u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA l/8_7 Rev.
-----
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VOLATILE ORGANICS ANALYSIS DATA SKEET
TENTATIVELY IDENTIFIED COMPOUNDS.
EPA SAMPLE NO.
Lab Name: COHPUCHEM,RTP
Lab Code: COMPU Case No.: 20937
Matri>C: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee. ---11
Column (pack/cap) Cl.P
Number TICs found: --1
CAS NUMBER COMPOUND
SB5-l-l Contract: 12-881-REVS
SAS No.: SDG No.: 22
tab Sample ID: 360290
~ Lab File ID: GH060290Cll
Date Received: 07/28/90
Date Analyzed: 08/07/90
Dilution Factor: &l~,o.__ __
NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT, EST. CONC. Q ••::::1•1•=-=-==•==•=-==-•••=:a•:oc211=a=•=========•====•· •m==i:a:a::ua •==••==••=-=-~ •==== 1. INSTRUMENT NOISE 1.98 14 J 2. INSTRUMENT NOISE 2.05 6.9 J
3. INSTRUMENT NOISE 2.15 3.4 J
FORM I VOA-TIC 1/87 Rev.
tlT ,,,., RY 133
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO,
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS S85-1-lRE
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (aoil/water) so;i:i;. Lab Sample ID: 360290
Sample, wt/vol: 5,0 (g/mL) L_ Lab File ID: GR06029QA19
Level: (low/med) i:.ow Date Received: 07,:'.28,:'.90
I Moisture: not dee. _u Date Analyzed: 08,:'.l,3,:'.90
Column: (pack/cap) CAP Dilution Factor: l,,O ----
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG Q
74-87-3---------Chloromethane ll u 74-83~9---------Bromomethane 11 l1 75-01-4---------Vinyl Chloride 11 l1 75-00-3---------Chloroethane 11 l1 75-09-2---------Methylene Chloride 14 B 67-64-1---------Acetone 46 B 75-15-o---------carbon Disulfide 6 l1 75-35-4---------l,l-Dichloroethene 6 l1 75-34-3---------1,1-Dichloroethane 6 l1 540-59-0--------1,2-Dichloroethene (total)_ 6 l1 67-66-3---------Chloroform 6 l1 107-06-2--------1,2-Dichloroethane ' 6 l1 78-93-3---------2-Butanone 11 l1 71-55-6---------1,1,1-Trichloroethane 6 l1 56-23-5---------carbon Tetrachloride 6 l1 '108-05-4--------Vinyl Acetate 11 l1 75-27-4---------Bromodichloromethane 6 l1 78-87-5---------1,2-Dichloropropane 6 l1 10061-01-5------cis-l,3-Dichloropropene 6 l1 79-01-6---------Trichloroethene 6 l1 124-48-1--------Dibromochloromethane 6 l1 79-oo-s---------1,1,2-Trichloroethane 6 l1 71-43-2---~-----Benzene 6 l1 10061-02-6------Trans-l,3-Dichloropropene __ 6 l1 75-25-2---------Bromoform 6 l1 1oe-10-1--------4-Methyl-2-Pentanone ll u 591-78-6--------2-Hexanone 11 l1 127-18-4--------Tetrachloroethene 6 l1 79-34-5---------1,1,2,2-Tetrachloroethane_ 6 l1 108-88-3--------Toluene 6 u 108-90-7--------qhlorobenzene 6 l1 100-41-4--------Ethylbenzene 6 l1 100-42-5--------styrene 6 l1 1330-20-7-------Total Xylenes 6 l1
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: coMPUCHtM.RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
SB5-l-1RE
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: ._22...__
Matrix: ( soil/water) SOIL
Sample wt/vol: s.o (g/mL) i...._
Level: (low/med) LOW
I Moisture: not dee. ·___u
Column (pack/cap) !:AP
Number TICs found: ___Q
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab Fila IO:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG£'.KG
RT EST.
360290
GR060290Al9
07£'.28£'.90
08£'.13£'.90
1.0
CONC. Q :::s:i::::1:::s••=a•=••=====-====-==-==--=--=--=--------== ==-=-====-•============= =•===
FORM I VOA-TIC 1/87 Rev.
.....
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP contract: 12-88)-REVS sas-2-1
Lab cc,de: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix:. (soil/water) SOIL Lab Sample IO: 360291
Sample wt/vol: 5.0 (g/mL) L_ Lab File ID: GH060291c11
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. -ll Date Analyzed: 08/07/9Q
Column: (pack/cap) CAP Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1, 1-0.ichloroethene
75-34-3---------1,1-0ichloroethane
540-59-0--------1,2-0ichloroethene
67-66-3---------Chloroform
107-06-2------~-1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-0ichloropropane
10061-01-S------cis-l,3-0ichloropropene
79-01-6---------Trichloroethene
124-48-1--------0ibromochloromethane
79-00-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-0ichloropropene __
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-s---------l,l,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
lJJo-20-1-------Total Xylenes
-
13 u
13 u
13 u
13 u
24 B
36 B
6 u
6 u
6 u
6 u
6 u
6 u
13 u
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA 1/87 Rev.
-............ --··-..
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VOLATILE ORGANICS ANALYSIS DATA SHEET .. EPA SAMPLE NO.
TENTATIVELY IDENTIFIED COMPOUNDS
SB5-2-l Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) IL_
Level: (low/med) LOW
t Moisture: not dee. _u
Column (pack/cap) CAP
Number TICs found: _J2
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: .2_2 __
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
360291
!.H060291CU
07/28/90
08/07/90
1.0
CONC. Q ~-=~~u=•==•a=•=• •==============•===========a •=•===== ••::taa:::;am••••a =====
FORM I VOA-TIC 1/87 Rev.
----I --1 --·""" 1 ,... " ,..,, .-.~1 f ,.,
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPL.E NO.
Lab Name: COMPUCHEM.RTP contract: c2-ee1-Rzys S85-2-1RE
Lab Code: CQMPU Case No.: 20937 SAS No.: ----SDG No.: 22 ---
Matrix: (soil/water) SOIL Lab Sample ID: . &3_6_0_2_9_1 __ _
Samplo wt/vol: s,o (g/mL) L_ Lab File ID: G3R60291Cll
Level: (low/med) LOW
I Moisture: not dee. ---2.1
Date Received: 07/28/90
Date Analyzed: 08/23/90
Dilution Factor: 1.0 Column:
-
(pack/cap) !::AF •
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-o--------l,2-Dichloroethene (total)_
67-66-3---------Chlorotorm
107-06-2--------l,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------l;l,l-Trichloroethana
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-5------cis-l,3-Dichloropropena
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromathane '' 79-00-5---------1,l,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromotorm
1os-10-1--------4-Methyl-2-Pentanona.
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroathane
79~34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-1-------Total Xylenes
-~--
Q
13 u
13 u
13 u
13 u
12 8
32 B
6 u
6 u
6 u
6 u
6 u
6 u
13 u
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6, u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA l/87 Rev.
-----,..,,
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EPA SAMPLE ~O. VOLATILE ORGANICS ANALYSIS DATA.SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP
Lab Code: COMPU Case.No,: 20937
Matrix: ( soil/water) SOIL
Samplo wt/vol: 5,0 (g/mL)
Level: (low/med) LOW
t Moisture: not dee. ----21.
Column (pack/cap) CM!
Number TICs found: _..Q
CAS NUMBER COMPOUND
S85-2-lRE Contract: (2-88)-REVS
SAS No.: SDG No.: -.22.___
~
NAME
Lab Sample ID: a3..,.6..,.0._29-1._ __ _
Lab File ID: GJR60291Cll
Date Received: 07/28/90
Date Analyzed: 08/23/90
Dilution Factor: .i~,o._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q az:ns::::1=•====-::a::a:a=== ============================ ======== 2:1•lCll=a"::::1::::l:a::::ll::::1a•::t:1 =•=s==
FORM I VOA-TIC 1/87 Rev.
20937 22 SAMPLE DATA SUMMARY 1 ,....., ·-' ..
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab N~tme: COMPUCHEM, RTP contract: 12-881-REVS SB6-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360292
sample, wt/vol: 5.0 (g/mL) !.,_ Lab File ID: GH0§0292Cll
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. __ll Date Analyzed: 011101190
Column: (pack/cap) Cll,P Dilution Factor: .i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG(KG Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 25 B 67-64-1---------Acetone 130 B
75-15-o---------carbon Disulfide 6 u·
75-35-4---------1,1-Dichloroethene 6 u 75-34-3---------1,l-Dichloroethane 6 u
540-59-0----~---l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u
78-93-3-~-------2-Butanone 850 BE
71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oe-10-1-~------4-Methyl-2-Pentanone 1300 E
591-78-6--------2-Hexanone 5 J
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
-
FORM I VOA l/87 Rev.
u
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
El?A SAMl?U: NO.
Lab Narae: COMPUCHEM.RTP Contract: (2-881-REVS SB6-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) sort
Sample wt/vol: 5.0 (g/mL) ~
Level: (low/med) LQW
I Moisture: not dee. _,ll
Column (pack/cap) Clr,P
Number TICs found: __i
CAS NUMBER COMPOUND NAME
Lab Sample ID: 360292
Lab File ID: GH0§Q292Cll.
Date Received: Q7/28/9Q
Date Analyzed: Q8/QZ/9Q
Dilution Factor: l,.Q ~---
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
•••===::a:a::::::::i:a:m:::::i:=•::s •==========================-===•=•=---==•=-==•==-----•== 1. UNKNOWN ALCOHOL 3.58 100 J 2. BUTANOL 7.08 17 J 3. UNKNOWN HYDROCARBON 4.40 1.3 J 4. UNKNOWN ALCOHOL 10.67 15 J
FORM I VOA-TIC . 1/87 Rev.
.-_ -· ·--••
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS S86-l-1RE
Lab code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360292
Sample wt/vol: 5.0 (g/mL) SL__ Lab File ID: G4R60292Ctt
Level: (low/med) tb!W Date Received: 07/28/90
I Moisture: not dee. _u Date Analyzed: 08/23/90
Column:
-
(pack/cap) CAP Dilution Factor: ~i~-~0c._ __
CONCENT~TION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 lJ 74-83-9---------Bromomethane 13 lJ 75-01-4---------Vinyl Chloride 13 lJ 75-00-3---------Chloroethane 13 lJ 75-09-2---------Methylene Chloride 21 B 67-64-1---------Acetone • 120 B 75-15-o---------carbon Disulfide 6 lJ 75-35-4---------1,1-Dichloroethene 6 lJ 75-34-3---------1,1-Dichloroethane 6 lJ 540-59-0--------1,2-Dichloroethene (total)_ 6 lJ 67-66-3---------Chloroform 6 lJ 107-06-2~-------l,2-Dichloroethane 6 lJ 78-93-3---------2-Butanone 13 lJ
71-55-6---------1,1,1-Trichloroethane 6 lJ 56-23-s---------carbon Tetrachloride 6 lJ
108-05-4--------Vinyl Acetate 13 lJ
75-27-4---------Bromodichloromethane 6 lJ
78-87-s---------l,2-Dichloropropane .6 lJ
10061-0l-S------cis-l,3-Dichloropropene 6 lJ
79-01-6---------Trichloroethene 6 lJ
124-48-1--------Dibromochloromethane 6 lJ
79-oo-s---------1,1,2-Trichloroethane 6 lJ
71-43-2----..;----Benzene 6 lJ
10061-02-6------Trans-1,3-Dichloropropene __ 6 lJ
75-25-2---------Bromotorm 6 lJ
1oa-10-1--------4-Methyl-2-Pentanone 13 lJ
591-78-6--------2-Hexanone 13 lJ
127-18-4--------Tetrachloroethene 6 lJ
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 lJ
108-88-3--------Toluene 6 lJ
108-90-7--------Chlorobenzene 6 lJ
100-41-4--------Ethylbenzene 6 lJ
100-42-5--------Styrene 6 lJ
1330-20-7-------Total Xylenes 6 lJ
FORM I VOA 1/87 Rev.
t.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
sas-1-uu:
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.·: _2_2 __
Matrix:: (soil/water) SOIL
sample wt/vol: 5.0 (g/mL) ~
Level: (low/med) LOw·
I Moisture: not dee. ---2..2.
Column (pack/cap) cap
Number TICS tound: __o_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGlKG
360292
G4R§0292c11
07 £'.28l90
08['.2Jl90
1,0
CAS NUMBER COMPOUND NAME RT EST. CONC. . Q -====~~===•==== =a•==•---=-==-=----=-=-===== ==•:a•=== =====-a======= =====
FORM I VOA-TIC 1/87 Rev.
0937 2 SAMPLE DATA SUMMARY 123
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VOLATILE ORGANICS ANALYSIS CATA SHEET EPA SAMPL.E NO,
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS SB6-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _2_2 __
Matrix: (soil/water) SOIL Lab Sample ID: 360293 Sampl,a wt/vol: 5,0 (g/mL) L-Lab File ID: GHQ§029'.lAll
Level:: (low/med) LOW Date Received: 07/28/90
I Moi11ture: not dee. -3.3. Cate Analyzed: 08/Q7/90
Columr1: (pack/cap) !::AP Dilution Factor: l,o -~--
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 15 u 74-83-9---------Bromomethane 15 u 75-01-4---------Vinyl Chloride 15 u 75-oo-3~--------Chloroethane 15 u 75-09-2---------Methylene Chloride 28 B 67-64-1---------Acetone 84 B 75-15-o---------carbon Disulfide 7 u 75-35-4---------1,1-Dichloroethene 7 u 75-34-3---------1,1-Dichloroethane 7 u 540-59-0--------1,2-Dichloroethene (total)_ 4 J 67-66-3---------Chloroform 7 u 107-06-2--------1,2-Dichloroethane 7 u 78-93-3------·---2-Butanone 4300 BE 71-55-6---------1,1,1-Trichloroethane 7 u 56-23-5---------carbon Tetrachloride 7 u 108-05-4--------Vinyl Acetate 15 u 75-27-4---------Bromodichloromethane 7 u 78-87-5---------1,2-Cichloropropane 7 u 10061-0l-5------cis-l,3-Cichloropropene 7 u 79-01-6---------Trichloroethene 7 u 124-48-1--------Cibromochloromethane 7 u 79-00-5---------1,1,2-Trichloroethane 7 u 71-43-2--~------Benzene 7 u 10061-02-6--~---Trans-l,3-Dichloropropene __ 7 u 75-25-2---------Bromoform 7 u 108-10-1--------4-Methyl-2-Pentanone 1300 E 591-78-6--------2-Hexanone 5 J 127-18-4--------Tetrachloroethene 7 u 79-34-5---------1,1,2,2-Tetrachloroethane_ 7 u 108-88-3--------Toluene 7 u 108-90-7--------Chlorobenzene 7 u 100-41-4--------Ethylbenzene 7 u 100-42-5--------styrene 7 u 1330~20-1-------Total Xylenes 7 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
EPA. SAMPLE NO.
SB6-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No, : .._2._2 __
Matrix: (soil/water) SOIL
Sample wt/vol: s.o (g/mL) !L_
Level: (low/med) LQH
, Moisture: not dee. _J_l
Column (pack/cap) CAP
Number TICs tound: ---2.
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
360293
GH0§0293All
07/28/90
08/07/90
1,0
CONC. Q
-••=a=====-•--===m=================m====== am=a==== =-•=====•==•--::a::.:•=•
1. BUT.ANOL 6.30 15 J
2. METHYLPENT.ANOL 10.65 13 J
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab N21me: COMPUCHEM. RTP Contract: (2-88)-REVS SB6-2-lRE
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG ·No.: ,.2_..2 __
Matrix: (soil/water) SOIL Lab Sample ID: 360293
Sample, wt/vol: 4.0 (g/mL) ~ Lab File ID: CR060293B14
Level: (low/med) MED Date Received: 07/28/90
\ Moisture: not dee. __u Date Analyzed: 08/07/90
Column: (pack/cap) CAP Dilution Factor: alL1~0 __
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 1900 u 74-83-9---------Bromomethane 1900 u 75-01-4---------Vinyl Chloride 1900 u 75-00-3---------Chloroethane 1900 u 75-09-2---------Methylene Chloride 1000 BO 67-64-1---------Acetone 1900 u 75-15-o---------carbon Disulfide 930 u 75-35-4---------1,1-Dichloroethene 930 u 75-34-3---------1,1-Dichloroethane 930 u 540-59-o--------l,2-Dichloroethene (total)_ 930 u 67-66-3---------Chloroform 930 u 107-06-2--------1,2-Dichloroethane 930 u 78-93-3---------2-Butanone 16000 D 71-55-6---------1,1,1-Trichloroethane 930 u 56-23-5---------carbon Tetrachloride 930 u 108-05-4--------Vinyl Acetate 1900 u 75-27-4---------Bromodichloromethane 930 u 78-87-5---------1,2-Dichloropropane 930 u
10061-0l-5------cis-l,3-Dichloropropene 930 u
79-01-6---------Trichloroethene 930 u
124-48-1--------Dibromochloromethane 930 u
79-oo-s---------1,1,2-Trichloroethane 930 u
71-43-2---------Benzene 930 u 10061-02-6------Trans-l,3-Dichloropropene __ 930 u
75-25-2---------Bromoform 930 u
lOa-10-1--------4-Methyl-2-Pentanone 4900 D
591-78-6--------2-Hexanone 1900 u
127-18-4--------Tetrachloroethene 930 u
79-34-5---------1,1,2,2-Tetrachloroethane __ . 930 u
108-88-3--------Toluene 930 u
108-90-7--------Chlorobenzene 930 u
100-41-4--------Ethylbenzene 930 u
100-42-5--------Styrene 930 u
1330-20-7-------Total Xylenes 930 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET ·
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: coMPUCHEM,RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
SB6-2-lRE
Lab C:ode: COMPO Case No.: 20937 SAS No.: SOG No.: ._2._2 __
MatrJ.x: (soil/water) SOIL
sample wt/vol: 4,0 (g/mL) L_
Level: (low/med) MED
I Moisture: not dee. -1.l
Column (pack/cap) CAP
Number TICs found: _,2
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab File IO:
Date Receive~:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG<'.'.KG
RT EST.
360293
CR0§0293B14
07£'.28<'.'.90
0B<'.'.07£'.2Q
;i,,o
CONC, Q ••••••==z===-===:a --=--=-----=---=-========= ======== •=-======:a=-•--=====
FORM I VOA-TIC l/87 Rev.
.,.,.. e IMM OU f I ,=
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VOLATILE ORGANICS ANALYSIS DATA SHEET Lt'A "Al'IPU: NO.
Lab Name: CQMPUCHEM,RTP Contract: (2-88)-REVS SB9-l-l
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360850
Sample wt/vol: 4.0 (g/mL) L-Lab File IO: C3R§oesoc10
Level: (low/med) MED Date Received: 08/01/90
I Moisture: not dee. -li Date Analyzed: 0BlU/9Q
Column: (pack/cap) CAP Dilution Factor: al~1~0c_ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGlKG Q
74-87-3---------Chloromethane 1500 u 74-83-9---------Bromomethane 1500 u 75-01-4---------Vinyl Chloride 1500 u 75-00-3---------Chloroethane 1500 u 75-09-2---------Methylene Chloride 450 BJ 67-64-1---------Acetone 3400 B 75-15-o---------carbon Disulfide 730 u 75-35-4---------1,1-Dichloroethene 730 u 75-34-3---------1,l-Dichloroethane 730 u 540-59-0--------1,2-Dichloroethene (total)_ 730 u 67-66-3---------Chloroform 730 u 107-06-2--------1,2-Dichloroethane 730 u 78-93-3---------2-Butanone 1500 u 71-55-6---------1,l,l-Trichloroethane 730 u
56-23-5---------carbon Tetrachloride 730 u
108-05-4--------Vinyl Acetate 1500 u
75-27-4---------Bromodichloromethane 730 u
78-87-5---------1,2-Dichloropropane 730 u
10061-0l-5------cis-l,3-Dichloropropene 730 u
79-01-6---------Trichloroethene 730 u 124-48-1--------Dibromochloromethane 730 u
79-oo-s---------1,1,2-Trichloroethane 730 u
71-43-2---------Benzene 730 u
10061-02-6------Trans-l,3-Dichloropropene_ 730 u
75-25-2---------Bromotorm 730 u
1os-10-1--------4-Methyl-2-Pentanone 1500 u
591-78-6--------2-Hexanone 1500 u
127-18-4--------Tetrachloroethene 360 BJ
79-34-5---------1,1,2,2-Tetrachloroethane __ 730 u
108-88-3--------Toluene 9600
108-90-7--------Chlorobenzene 730 u
100-41-4--------Ethylbenzene 210 J
100-42-5--------styrene 730 u
1330~20-1-------Total Xylenes 550 J
FORM I VOA 1/87 Rev.
~ 937 22 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
SB9-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,.2..._2 __
Matrix: (soil/water) SOIL
Sample wt/vol: 4,0
Level: (low/med) MED
% Moisture: not dee. _li
Column (pack/cap) CAP
Number TICs tound: _i
CAS NUMBER
(g/mL) SL_
COMPOUND NAME
Lab Sample ID: &3~6~0~85~0,i_ __ _
Lab File ID: CJR6oesoc10
Date Received: 08/01/90
Date Analyzed: 08/14/90
Dilution Factor: .1~·~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q •===~•m•=•===-••= -=---=---=------------=----= ======== ===::.:====••=-== ===== 1. UNKNOWN HYDROCARBON 11.92 3100 J 2. UNKNOWN 12.80 1300 J 3. UNKNOWN 13. 52 2300 J
4. UNKNOWN 13.79 1500 J 5. UNKNOWN 14 .10 2500 J
FORM I VOA-TIC 1/87 Rev.
--.-.... --.............. .-.. ·--~ _J
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS S89-2-l
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360853
Sampl11 wt/vol: 5.0 (g/mL) ~ Lab File ID: l,H060853Cll
Level: (low/med) LOW Date Received: 00101/90
, Moisture: not dee. ---1.Q Date Analyzed: 08/10/90
Column: (pack/cap) ca,P Dilution Factor: .1~.o,._ __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 14 74-83-9---------Bromomethane 14 75-01-4---------Vinyl Chloride 14 75-00-3---------Chloroethane 14 ,,-09-2---------Methylene Chloride 19 67-64-1---------Acetone 98 75-15-o---------carbon Disulfide 7 75-35-4---------1,l-Dichloroethene 7 75-34-3---------1,l-Dichloroethane 5 540-59-o--------l,2-Dichloroethene (total)_ 7 67-66-3-.--------Chloroform 7
107-06-2--------1,2-Dichloroethane 7
78-93-3---------2-Butanone 340 71-55-6---------1,l,l-Trichloroethane 7 56-23-5---------carbon Tetrachloride 7
108-05-4--------Vinyl Acetate 14
75-27-4---------Bromodichloromethane 7
78-87-5---------1,2-Dichloropropane 7
10061-0l-5------cis-l,3-Dichloropropene 7
"79-01-6---------Trichloroethene 7
124-48-1--------Dibromochloromethane 7
79-oo-s---------1,l,2-Trichloroethane 7
71-43-2---------Benzene 7
10061-02-6------Trans-l,J-Dichloropropene __ 7
75-25-2---------Bromoform 7
108-10-1--------4-Methyl-2-Pentanone 770
591-78-6--------2-Hexanone 14
127-18-4--------Tetrachloroethene 2
79-34-5---------l,l,2,2-Tetrachloroethane_ 7
108-88-3--------Toluene . 120
108-90-7--------Chlorobenzene 7
100-41-4--------Ethylbenzene 7
100-42-5--------styrene 7
1330-20-7-------Total Xylenes 2
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FORM I VOA 1/87 Rev.
.-11M .-.~t_l
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
.EPA SAMPLE NO.
589-2-1 Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code : CQMPU Case No.: 20937 SAS No.: SOG No.: ... 2.._2 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) !:i...._
Level: (low/med) LOW
I Moisture: not dee. __lQ
Column (pack/cap) CAP
Number TICs round: --2
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Data Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
360853
GH060853Cll
08/01/90
08/10/90
l,0
CONC. Q
=••••••=-•=•a=-••• ••=2::1:a---==--=---=--==-=--==-==----=-= •:1111•====-===-=== •====
FORM I VOA-TIC 1/87 Rav.
--.-. ~· ~llM O V
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS SB9-2-lRE
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: a.22,.___
Matrix: (soil/water) SOIL Lab Sample ID: 360853
Sample wt/vol: 4,0 (g/mL) L_ Lab File IO: C2R60BSJC10
Level: (low/med) MED Date Received: 08/01/90
I Moisture: not dee. ____ll Date Analyzed: oa1u120
Column: (pack/cap) CAP Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane · 1800
74-83-9---------Bromomethane 1800
75-01-4---------Vinyl Chloride 1800
75-00-3---------Chloroethane 1800
75-09-2---------Methylene Chloride 510
67-64-1---------Acetone 1800
75-15-o---------carbon Disulfide 890
75-35-4---------1,1-0ichloroethene 890
75-34-3---------1,1-0ichloroethane 890
540-59-0--------l,2-0ichloroethene (total)_ 890
67-66-3---------Chloro!orm 890
107-06-2--------1,2-oichloroethane 890
78-93-3---------2-Butanone 1800
71-55-6---------1,1,1-Trichloroethane 890
56-23-5---------carbon Tetrachloride 890
108-05-4--------vinyl Acetate 1800
75-27-4---------Bromodichloromethane 890
78-87-5---------1,2-Dichloropropane 890
10061-0l-5------cis-l,J-Oichloropropene 890
79-01-6---------Trichloroethene 890
124-48-1--------0ibromochloromethane 890
79-00-5---------1,1,2-Trichloroethane 890
71-43-2---~-----Benzene 890
10061-02-6------Trans-l,3-0ichloropropene __ 890
75-25-2---------Bromo!orm 890
108-10-1--------4-Methyl-2-Pentanone 1800
591-78-6--------2-Hexanone 1800
127-18-4--------Tetrachloroethene 890
79-34-5---------1,1,2,2-Tetrachloroethane __ 890
108-88-3--------Toluene 890
108-90-7--------Chlorobenzene 890
100-41-4--------Ethylbenzene 890
100-42-5--------styrene 890
1330-20-7-------Total Xylenes 890
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FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: ·coMPUCHEM,RTP Contract: 12-88)-REVS SB9-2-lRE
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: .,,.2.,._2 __
Matrix: (soil/water) SOIL
sample wt/vol: 4.0 (g/mL) L-
Level: (low/med) MED
, Moisture: not dee. _lQ.
Column (pack/cap) CM!
Number TICs tound: __o_
CAS NUMBER COMPOUND-NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
360853
C2R60853Cl0
08/01/90
08/14/90
1,0
CONC. Q •••••n•••••••••• --==--•-======••=========•------==•:t .aa•••2a•m••••• •=-==
FORM I VOA-TIC 1/87 Rev.
20~37 22 SAMPLE DATA SUMMARY 11J
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEM.RTP contract: C2-88l-REVS
SB5-l-1MS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No,: _.2_..2 __
Matrix: ( soil/water) SOIL Lab Sample ID: 360286
Samplo wt/vol: 5.0 (g/mL) ~ Lab File IO: G2R60286All
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. __ll Date Analyzed: 08/21/90
Column: (pack/cap) CAP Dilution Factor: .l~•~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u 74-83-9---------Bromomethane 11 u 75-01-4---------Vinyl Chloride ll u 75-00-3---------Chloroethane ll u 75-09-2---------Methylene Chloride 15 B 67-64-1---------Acetone 23 B 75-15-o---------carbon Disulfide 6 u
75-35-4---------l,l-Dichloroethene 6 u 75-34-3---------1,1~Dichloroethane 6 u 540-59-o--------l,2-Dichloroethene (total)_ 6 u
67-66-3----~----Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone ll u
71-55-6---------1,l,l-Trichloroethane 6 u
56-23-5---------Carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate ll u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-S------cis-l,3-Dichloropropene 6 u
79~01-6-~-------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5--~------l,l,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromofotm 6 u
1O0-1O-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone ll u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
.-.-..... --· ......... -.. ,-. r""II I I
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11 I_
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: ~OMPUCHEM,RTP Contract: 12-881-REVS S86-2-1REMS
Lab Code: C,;lMPU Case No.: 20937 ·SAS No.: SDG No.: a..22..___
Matrix: ( sell/water) SOIL Lab Sample ID: 362732
Sample wt;v,,l: 4.0 (g/mL) L_ Lab File ID: CN0627J2Cl4
Level: (low/med) HEP Date Received: 07/28/90
I Moisture: not dee. -1.3. Date Analyzed: 08/08/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS: CAS 110. COMPOUND (ug/L or ug/Kg) U!:itK!:i Q
74-87-3---------Chloromethane 1900 u 74-83-9---------Bromomethane 1900 u 75-01-4---------Vinyl Chloride 1900 u 75-00-3---------Chloroethane 1900 u 75-09-2---------Methylene Chloride 500 BJ 67-64-1---------Acetone 1200 BJ 1s-1s-o---------carbon Disultide 930 u
75-35-4---------1;1-Dichloroethene 930 u
75-34-3---------1,1-Dichloroethane 930 u 540-59-o~-------l,2-Dichloroethene (total)_ 930 u 67-66-3---------Chloroform 930 u 107-06-2--------1,2-Dichloroethane 930 u 78-93-3---------2-Butanone 15000
71-55-6----~----l,l,l-Trichloroethane 930 u
56-23-5---------carbon Tetrachloride 930 u
108-05-4--------Vinyl Acetate 1900 u
75-27-4---------Bromodichloromethane 930 u
78-87-5---------1,2-Dichloropropane 930 u
10061-01-5------cis-l,3-Dichloropropene 930 ·U
79-01-6---------Trichloroethene 930 u
124-48-1--------Dibromochloromethane 930 u
79-oo-s---------1,1,2-Trichloroethane 930 u
71-43-2---------Benzene 930 u
10061-02-6------Trans-l,3-Dichloropropene __ 930 u
75-25-2---------Bromoform 930 u
1oa-10~1--------4-Methyl-2-Pentanone 5200
591-78-6--------2-Hexanone 1900 u
127-18-4--------Tetrachloroethene 930 u
79-34-5---------1,l,2,2-Tetrachloroethane_· _ 930 u
108-88-3--------Toluene 930 u
108-90-7--------Chlorobenzene 930 u
100-41-4--------Ethylbenzene 930 u
100-42-5--------styrene 930 u
1330-20-7-------Total Xylenes 930 u
FORM I VOA 1/87 Rev.
CII MO V I I I
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS SBS-1-lMSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360287
Samplo wt/vol: 5.0 (g/mL) ~ Lab File ID: G2R60287All
Level: (low/med) I,QW Date Received: 07/28/90
I Moisture: not dee. ___u Date Analyzed: 08/21/90
Column: (pack/cap) CAP Dilution Factor: ~1~-~0c_ __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane _______ _
74-83-9---------Bromomethane -,--------75 - 0 l - 4 - - - - - - - - -Vinyl Chloride ______ _
75-00-3---------Chloroethane
75-09-2---------Methylene Ch-~l_o_r~i~d~e------
67-64-1---------Acetone
75-15-o---------carbon ·=D~i_s_u~l~f~i~d-e--,-----
75-35-4---------1,l-Dichloroethene ____ _
75-34-3---------1,1-Dichloroethane.....,_-,-.,....,... __
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform ~07-06-2--------1,2-Dichlo_r_o_e~t~h_a_n_e ____ _
78-93-3---------2-Butanone 71-55-6---------1,1,l-Tric.~h~l-o_r_o_e~t~h_a_n_e ___ _
56-23-5---------carbon Tetrachloride. ____ _
108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloro_m_e~th~a_n_e ____ _
78-87-5---------1,2-Dichloropropane-'-----
10061-0l-5------cis-l,3-Dichloropropene __ _
79-01-6---------Trichloroethena 124-48-1--------Dibromochlorome.~t~h~an~e-----
79-oo-s---------l,l,2-Trichloroethane ___ _
71-43-2---------Benzene,_,,....,,-,-~-------
l0061-02-6---~--Trans-l,3-Dichloropropene __
75-2s-2---------Bromoform . .,,....-=--:----,-----1oa-10-1--------4-Methyl-2-Pentanone._· ___ _
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene. _ _,.~----
79-34-5---------1,l,2,2-Tetrachloroethane __
108-88-3--------Toluene __________ _
108-90-7---~----Chlorobenzene. _______ _
100-41-4--------Ethylbenzene _______ _
100-42-5--------styrene, __________ _
1330-20-7-------Total Xylenes, _______ _
11 U
11 U
11 U
11 U
15 B
33 B
6 U
6 U
6 U
6 U
6 U
6 U
11 U
6 U
6 U
11 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
11 U
11 U
6 U
6 U
6 U
6 U
6 U
6 U
6 U
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS S86-2-1REMSD
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 362733
SamplE1 wt/vol: 4 ,.o (g/mL) L_ Lab File ID: CNQ627JJC14
Level: (low;.med) MED Date Received: 07/28/90
% Moi!l,ture: not dee. -11 Date Analyzed: 08/08/90
Column: (pack/cap) CAP Dilution Factor: ~i~·~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 1900
74-83-9---------Bromomethane 1900
75-01-4---------Vinyl Chloride 1900
75-00-3---------Chloroethane 1900
75-09-2---------Methylene Chloride 380
67-64-1---------Acetone 1900
75-15-o---------carbon Disulfide 930
75-35-4---------1,1-Dichloroethene 930
75-34-3---------1,1-Dichloroethane 930
540-59-0--------1,2-Dichloroethene (total)_ 930
67-66-3---------Chlorotorm 930
107-06-2--------1,2-Dichloroethane 930
78-93-3---------2-Butanone 6400
71-55-6---------1,1,l-Trichloroethane 930
56-23-5---------carbon Tetrachlorid~ 930
108-05-4--------vinyl Acetate 1900
75-27-4-------..:-eromodichloromethane 930
78-87-5---------1,2-0ichloropropane 930
10061-01-5------cis-l,3-Dichloropropene 930
79-01-6---------Trichloroethene 930
124-48-1--------0ibromochloromethane 930
79-00-5---------l,l,2-Trichloroethane 930
71-43-2---------Benzane 930
10061-02-6------Trans-1,3-Dichloropropene __ 930
75-25-2---------Bromotorm 930
108-10-1--------4-Methyl-2-Pentanone 4700
591-78-6--------2-Hexanone 1900
127-18-4--------Tetrachloroethene ' 930
79-34-5---------1,l,2,2-Tetrachloroethane __ 930
108-88-3--------Toluene 930
108-90-7--------Chlorobenzene 930
100-41-4--------Ethylbenzene 930
100-42-s--------styrene 930
1330-20-7-------Total Xylenes 930
u u u
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u
u
FORM I VOA 1/87 Rev.
2093? 22 SAMPbE DATA SUMMARY
'
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1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name:_COMPUCHEM.RTP Contract: (2-881-REVS MW2A-6S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22 Matrix: (soil/water) SOIL Lab Sample IO: 360294 Sample wt/vol: 30.1 (g/mL) ~ Lab File ID: GH060294B15 · Level: (low/med) LOW Date Received: 07128/90
t Moisture: not dee.~ dee. Date Extracted: 01131120
Extraction: (SepF/Cont/Sonc)
(Y/N) li_
~
pH: -2..,..l
Date Analyzed: 08/13/90
GPC Cleanup: Dilution Factor: •1~,~0 __ _
ii
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
'
108-95-2--------Phenol 440 lll-44-4--------bis(2-Chloroethyl)Ether 440 95-57-8---------2-Chlorophenol 440 541-73-1----~---l,3-Dichlorobenzene 440 106-46-7--------1,4-Dichlorobenzene 440 100-51-6--------Benzyl Alcohol 440 95-50-1---------1,2-Dichlorobenzene 440 95-48-7---------2-Methylphenol 440 39638-J2-9------bis(2-Chloroisopropyl)Ether 440 106-44-5--------4~Methylphenol -440 621-64-7--------N-Nitroso-Di-n-Propylamine_ 440 67-72-1---------Hexachloroethane 440 98-95-3---------Nitrobenzene 440 78-59-1---------Isophorone 440 88-75-5---------2-Nitrophenol 440 105-67-9--------2,4-Dimethylphenol 440 65-85-0---------Benzoic Acid 2100 lll-9l-l--------bis(2-Chloroethoxy)Methane_ 440 120-83-2--------2,4-Dichlorophenol 440 120-s2-1--------1,2,4-Trichlorobenzene 440 91-20-J----~----Naphthalene 440 106-47-8--------4-Chloroaniline 440 87-68-3---------Hexachlorobutadiene 440 59-50-7---------4-Chloro-J-Methylphenol 440 91-57-6---------2-Methylnaphthalene 440 77-47-4---------Hexachlorocyclopentadiena_ 440 88-06-2---------2,4,6-Trichlorophenol 440 95-95-4---------2,4,5-Trichlorophenol 2100 91-58-7---------2-Chloronaphthalene 440 88-74-4---------2-Nitroaniline 2100 131-11-3--------Dimethyl Phthalate 440 208-96-8--------Acenaphthylene _440 606-20-2--------2,6-Dinitrotoluena 440
u u u u u u u u
u
u u u u
(J
u u u u u u u u u u u u
u u u u u
u u
• FORM I sv-1 1/87 Rev.
_, as 70:U..7' 76\ $AMPLE DATA SUMMARY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW2A-6S-l Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360294
Sample wt/vol: 30.1 (g/mL) L-Lab File ID: GH06Q294B15
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. _l..2 dee. Date Extracted: O:Z/31/90
Extrac·tion: (SepF/Cont/Sonc)
(Y/N) li,_
~
pH: ....2....l
Date Analyzed: 08/13/90
GPC Cleanup: Dilution Factor: &l~.o._ __
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2100 lJ 83-32-9---------Acenaphthene 440 lJ 51-28-5--~------2,4-Dinitrophenol 2100 lJ 100-02-1--------4-Nitrophenol 2100 lJ 132-64-9--------Dibenzofuran 440 u 121-14-2--------2,4-Dinitrotoluene 440 u 84-66-2---------Diethylphthalate 440 u 7005-72-3-------4-Chlorophenyl-phenylether 440 u 86-73-7-P--~----Fluorene -440 u 100-01-6--------4-Nitroaniline 2100 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 2100 u 86-30-6---------N-Nitrosodiphenylamine (1)_ 440 u 101-55-3--------4-Bromophenyl-phenylether __ 440 u 118-74-1--------Hexachlorobenzene 440 u 87-86-5---------Pentachlorophenol 2100 u as-01-8---------Phenanthrene 440 lJ
120-12-1--------Anthracene 440 u
84-74-2---------Di-n-Butylphthalate 440 u
206-44-o--------Fluoranthene 440 u
129-oo-o--------Pyrene 440 u
85-68-7---------Butylbenzylphthalate 440 u
91-94-1---------3,3'-Dichlorobenzidine 880 u
56-55-3---------Benzo(a)Anthracene 440 u
218-01-9--------Chrysene 440 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 440 u
117-84-0--------Di-n-Octyl Phthalate 440 u
205-99-2--------Benzo(b)Fluoranthene 440 u
207-08-9--------Benzo(k)Fluoranthene 440 u
50-32-8---------Benzo(a)Pyrene 440 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 440 u
53-70-3---------Dibenzo(a,h)Anthracene 440 u
191-24-2--------Benzo(g,h,i)Perylene 440 u
(1) -Cannot be separated from D1phenylam1ne
FORM I sv-2 1/87 Rev,
I M,-, l •'
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Namu: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Codo: .COMPU Case No.: 20937 SAS No.: -SOG
Matrix: (soil/water) SOIL Lab Sample ID:
sample .rt/vol: 30,1 (g/mL) ~ Lab File ID:
Level: ( low/med) LOW Date Received:
I Moisture: not dee.~ dee. Date Extracted: <
EPA SAMPLE NO.
MW2A-6S-l
No.: 22
360294
!.H0§0294Bl~
07/28/20
071'.J 1/20
Extraction: (SepF/Cont/Sonc) ~
GPC Clea.nup: (Y/N) H__ pH: ..i.J.
Date Analyzed: 08/13/90
Dilution Factor: 1,0 ~---
Number TICs found: ---2.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) U!;i/K!;i
RT EST. CONC. ::u::s'lll••==========• •••=•========n=============n •=z====== -a••••=a==••=-
1. SOLVENT CONTAMINANT 5,28 220 2. ALOOL 6.18 270
FORM I SV-TIC 1/87 Rev.
I t:: 0 ~1/M
Q
••===
BJ
A.J
1136
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18
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEM.RTP SB12-l-l Contract: (2-881-REVS
Lab Code : COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360858
Sample wt/vol: 30.0 ( g/mL) !,i___ Lab File ID: GH060858CQ7
Level: (low/med) LOW Date Received: 08/01/90
I Moisture: not dee.~ dee. Date Extracted: 08/03/90
Extraction: (SepF/Cont/Sonc) S,QHC
GPC Cleanup: (Y/N) tL.. pH: ....2.......2.
Date Analyzed: 08/15/90
Dilution Factor: •l~,o~o.,___
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
1
1
9
5
1
1
9
9
3
1
6
6
9
7
8
1
6
1
1
1
9
1
8
5
9
7
8
9
9
8
1
2
6
08-95-2--------Phenol
ll-44-4--------bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
41-73-1--------1,3-Dichlorobenzene
06-46-7-------~l,4-Dichlorobenzene
00-51-6--------Benzyl Alcohol
5-50-1---------1,2-Dichlorobenzene
5-48-7---------2-Methylphenol
9638-32-9------bis(2-Chloroisopropyl)Ether_
06-44-5--------4-Methylphenol
21-64-7--------N-Nitroso-Di-n-Propylamine_
7-72-1---------Hexachloroethane
8-95-3---------Nitrobenzene
S-59-1---------Isophorone
S-75-5---------2-Nitrophenol
05-67-9--------2,4-Dimethylphenol
5-85-o---------eenzoic Acid
ll-9l-l--------bis(2-Chloroethoxy)Methane_
20-83-2--------2,4-Dichlorophenol
20-a2-1--------l,2,4-Trichlorobenzene.
l.-20-3---------Naphthalene
06-47-8--------4-Chloroaniline
7-68-3---------Hexachlorobutadiene
9-50-7---------4-Chloro-3-Methylphenol
1-57-6---------2-Methylnaphthalene
7-47-4---------Hexachlorocyclopentadiene __ .
8-06-2---------2,4,6-Trichlorophenol
5-95-4---------2,4,5-Trichlorophenol
1-58-7---------2-Chloronaphthalene
8-74-4---------2-Nitroaniline
31-11-3--------Dimethyl Phthalat•
08-96-8--------Acenaphthylene
06-20-2--------2,6-Dinitrotoluene
510
510
510
510
510
510
510
510
510
510
510
510
510
510
510
510
2500
510
510
510
510
510
510
510
510
510
510
170
510
2500
510
510
510
u u
u
u
u u
.U u
u u
u
u u u
u
u u u
u u
u
u
u
u u u u
J
u
u u u
u
FORM I sv-1 1/87 Rev.
2 937 ,.. 5AMP DATA SUMMAR'r'
Q
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lC SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPU NO.
5812-1-1 Lab Name: COMPUCHEM.RTP Contract: 12-BBl -REVS
Lab Coda: COMPU Case No.: 20937 SAS No.: SDG No.: 22 Matrix: (soil/water) SOIL Lab Sample ID: 360858 Sample ~rt/vol: 30.0 (g/mL) ~ Lab File ID: GH060858C07 Level: (low/med) LOW Date Received: 08/01/90 t Moisture: not dee. _is. dee. Date Extracted: 08/0JL90 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ti__ pH:~
Date Analyzed: 08/15/90
Dilution Factor: .• 1 .... ,.0,.0 __
CAS NO. COMPOUND CONCENTRATION UNITS: (ugiL or ug/Kg) UG/KG
99-09-2---------J-Nitroaniline
2500 83-32-9---------Acenaphthene
510 51-28-5---------2,4-Dinitrophenol
2500 100-02-7--------4-Nitrophenol
2500 132-64-9--------Dibenzoturan
510 121-14-2--------2,4-Dinitrotoluene
510 84-66-2---------Diethylphthalate
510 7005-72-3-------4-Chlorophenyl-phenylether_
510 86-73-7---------Fluorene
510 100-01-6--------4-Nitroaniline
2500 534-52-1--------4,6-Dinitro-2-Methylphenol_ 2500 8 e;-J 0-6---------N-N i trosodiphenylamine (l)_ 510 101-55-3--------4-Bromophenyl-phenylether __ 510 118-74-1--------Hexachlorobenzene
510 87-86-5---------Pentachlorophenol
300 85-01-8---------Phenanthrene
510 120-12-7--------Anthracene
510 84-74-2---------Di-n-Butylphthalate
510 206-44-0----~---Fluoranthene
510 129-00-0--------Pyrene
510 85-68-7---------Butylbenzylphthalate 510 91-94-1---------3,J'-Dichlorobenzidine 1000 56-55-3---------Benzo(a)Anthracene
510 218-01-9--------Chrysene 510 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 88 117-84-o--------Di-n-octyl Phthalate 510 20!5-99-2--------Benzo (b) Fluoranthene 510 20·1-08-9--------Benzo (k) Fluoranthene 510 50··32-8---------Benzo (a) Pyrene 510 19J-39-5--------Indeno(l,2,J-cd)Pyrene 510 53-70-3---------Dibenzo(a,h)Anthracene 510 19l.-24-2--------Benzo (g ,h, i) Perylene 510
· ( 1) -· cannot be separated trom D1phenylam1ne
u
u u u u u u u u u u
u u u
J u u u u u u u u u
J u u
u u
u u u
FORM I sv-2 1/87 Rev.
'1.-v-,I I L..... a R
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Nam,,: CQMPUCHEM, RTP Contract: 12-881-REVS SB12-l-l
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: ( soil/water) SQIL Lab Sample ID: 360858
Sample ._t/vol: 30.0 (g/mL) L_ Lab File ID: GH060958C07
Level: (low/med) LOW
% Moisture: not dee. ~ dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li.,_ pH:~
Number TICs found: __ll
CAS NUMBER COMPOUND NAME
Date Received: 08/01/90
Date Extracted: 08/03/90
Date Analyzed: 08/15/90
Dilution Factor: &l~,o~o"--_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST, CONC. Q aa:a=•••:••-••••• •••caaa•===••=======m===•=•• •=-••====-•:=-•------=---•=-•== 1. SOLVENT CONTAMINANT 5.17 200 BJ 2. ALDOL 5.92 · 510 AJ 3; ALDOL 6.25 360 AJ
4. UNKNOWN HYDROCARBON 9.59 200 J
5. UNKNOWN HYDROCARBON 10.14 610 J
6. TETRACHLOROPHENOL 10.24 360 J 7. UNKNOWN HYDROCARBON 10.65 1400 J
8. UNKNOWN HYDROCARBON 11.14 510 J
9. UNKNOWN HYDROCARBON 11.60 560 J 10. UNKNOWN 13.54 200 J
11. UNKNOWN 13.57 200 J
12. UNKNOWN ' 13.72 360 J
13. UNKNOWN 13.85 310 J
14. UNKNOWN 13.94 310 J
15. UNKNOWN PHTHALATE 16.99 310. J
16. UNKNOWN 17. 12 360 J
17. UNKNOWN HYDROCARBON 17.42 360 J
18. UNKNOWN 17.57 920 J
19. UNKNOWN PHTHALATE 17.72 920 J
20. UNKNOWN 17.89 460 J
FORM I SV-TIC 1/87 Rev.
20937 22 SAMPLE DATA SUMMARY 103
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP 5B4-1-1 Contract: <2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360282
Sample wt/vol: 30,0 (g/mL) L_ Lab File ID: GH0§0282lll:i
Level: (low/med) _LO=W~-Date Received: 07/28/90
t Moisture: not dee. ~ dee. Date Extracted: 07/31/90
Extracticm: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL,_ pH: ....2..,..9,
Date Analyzed: 08/13/90
Dilution Factor: 1,00
CJ\S NO. COMPOUND
CONCENTRATION UNITS:
(ug~L or ug/Kg) UG/KG
l
1
9
5
1
1
9
9
3
1
6
6
9
7
8
1
6
1
1
1
9
1
8
5
9
7
8
9
9
8
1
2
6
,
08-95-2~~------Phenol
ll-44-4--------bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
,1-73-1--------1,3-Dichlorobenzene
06-46-7--------1,4-Dichlorobenzene
00-51-6--------Benzyl Alcohol
5-50-1---------1,2-Dichlorobenzene
5-48-7---------2-Methylphenol
9638-32-9------bis(2-ChloroisopropylJEther_
06-44-5----·----4-Methylphenol
21-64-7--------N-Nitroso-Di-n-Propylamine_
7-72-1---------Hexachloroethane
8-95-3---------Nitrobenzene
8-59-1---------Isophorone
8-75-5---------2-Nitrophenol
05-67-9--------2,4-Dimethylphenol
5-ss-o---------Benzoic Acid
ll-91-l--------bis(2~Chloroethoxy)Methane_
20-83-2--------2,4-Dichlorophenol
20-s2-1--------1,2,4-Trichlorobenzene
1-20-3---------Naphthalene
06-47-8--------4-Chloroaniline
7-68-3---------Hexachlorobutadiene
9-50-7---------4-ch·loro-3-Methylphenol
l-57-6---------2~Methylnaphthalene '
7-47-4---------Hexachlorocyclopentadiene __
8-06-2---------2,4,6-Trichlorophenol
5-95-4---------2,4,5-Trichlorophenol
1-58-7---------2-Chloronaphthalene
8-74-4---------2-Nitroaniline
31-11-3--------Dimethyl Phthalate
08-96-8--------Acenaphthylene
06-20-2--------2,6-Dinitrotoluene
.
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
410
2000
410
410
410
410
410
410
410
410
410
410
2000
410
2000
410
410
410
u u
u
u u
u
u u.
u
u
u
u
u
u
u
u
u
u
u u
u
u u
u
u
u u
u
u
u
u u
u
FORM I sv-1 1/87 Rev.
20937 22 SAMPLE DATA SUMMARY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-BBl-REVS SB4-l-l
Lab Code: CQMPU case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360282
Sample 111t/vol: 30.0 (g/mL) ~ Lab File IO: GHoso2e2s1s
Level: (low/med) LOW Date Received: 07/28/90
' Moisture: not dee. -ll dee. Date Extracted: oz;31;90
ExtractJ.on:
GPC Cleimup:
(SepF/Cont;sonc)
(Y/N) li._
SQt!C
pH:~
Date Analyzed: 08/13/90
Dilution Factor: .1~1~0~0 __
C:AS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
9-09-2---------3-Nitroaniline
3-32-9---------Acenaphthene
1-2s-s---------2,4-Dinitrophenol
00-02-1--------4-Nitrophenol
32-64-9--------Dibenzofuran
21-14-2--------2,4-Dinitrotoluene
4-66-2------~--Diethylphthalate
9
8
5
1
1
1
8
7
8
1
5
8
1
1
8
8
005-72-3-------4-Chlorophenyl-phenylether __ 6-73-7-~-------Fluorene
00-01-6-~------4-Nitroaniline
34-52-1--------4,6-Dinitro-2-Methylphenol_
6-30-6---------N-Nitrosodiphenylamine (l)_ 01-55-3--------4-Bromophenyl-phenylether_
18-74-1--------Hexachlorobenzene
7-86-5---~-----Pentachlorophenol
5-01-8---------Phenanthrene
120-12-1--------Anthracene
8
2
4-74-2---------Di~n-Butylphthalate
06-44-o--------Fluoranthene
1:29-00-0--------Pyrene
8 5-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
515-55-3---;.-~---Benzo ( a) Anthracene 2 :Le-o l-9--------Chrysene
l:L 7-81-7--------bis (2-Ethylhexyl) Phthalate_ 117-84-o--------oi-n-octyl Phthalate 2()5-99-2--------Benzo(b)Fluoranthene
2 (>7-08-9--------Benzo ( le) .Fl uoranthene 5Cl-32-s---------Benzo ( a) Pyrene 1513-39-5--------Indeno ( 1, 2, 3-cd) Pyrene 53-70-3---------Dibenzo(a;h)Anthracena
1511-24-2--------Banzo (g, h, i) Perylene
(1)-CaMot be separated trom D1phenylam1ne
2000
410
2000
2000
410
410
410
410
410
2000
2000
410
410
410
2000
410
410
410
410
410
410
820
410
410
410
410
410
410
410
410
410
410
u u u u u u u u
u
u
u
u
u u
u
u u u u u
u u·
u
u u
u u u
u
u u u
FORM I sv-2 l/87 Rev.
-•• Zt19lZ. ?2 5RMPLE DRTR SUMMAR'r'
Q
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1131
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lF EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88l-REVS
Lab Code:: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SB4-l-l
No.: 22
360282
Sample wt/vol: 30.0 (g/mL) !i__ Lab File ID: GH060282B15
Level: ( low/med) _LO,..w.___
'I Moistuz·e: not dee. ---2..Q dee.
Extractic,n: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL_ pH: ....2.....2.
Number TICS found: ---1
CAS NUMBER COMPOUND NAME
Date Received: 07/29/90
Date Extracted: Q7 /)l/90
Date Analyzed: QB/13/90
Dilution Factor: .i~,0~Q.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC, Q •••a•==-==•====-aa• ••a=-=----==---=--========-=• =-=-=-=== :mc:111•==-••:m=••• •==== 1, 4-(TETRAMETHYLBUTYL)PHENOL 11,59 250 J
FORM I SV-TIC l/87 Rev.
20937 22 SAMPLE DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Nam~: COMPUCHEM.RTP Contract: 12-881-REVS SB4-2-l
Lab Coda: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/water) SOIL Lab Sample IO: 360289
Sample wt/vol: 30,1 (g/mL) ~ Lab File IO: GH0§0289B15
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. _..l,i dee. Date Extracted: 07/Jl/20
Extracti.on: (SepF/Cont/Sonc) ~ Date Analyzed: 08/lJ/90
GPC Cleanup: (Y/N) li._ pH: ~ Dilution Factor: .1~-~o __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 410 u lll-44-4--------bis(2-Chloroethyl)Ether 410 u 95-57-8---------2-Chlorophenol 410 u 541-73-1--------1,3-0ichlorobenzene 410 u 106-~6-7--------1,4-0ichlorobenzene 410 u
100-51-6--------Benzyl Alcohol 410 u 95-50-1---------1,2-0ichlorobenzene 410 u 95-48-7---------2-Methylphenol 410 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u 106-44-5--------4-Methylphenol 410 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 410 u
67-72-1---------Hexachloroethane 410 u
90-95-3---------Nitrobenzene 410 u
78-59-1---------Isophorone 410 u
88-75-5---------2-Nitrophenol 410 u
105-67-9--------2,4-0imethylphenol 410 u
65-85-o---------Benzoic Acid 2000 u
l l. 1-91-1--------bis ( 2-Chloroethoxy) Methane_ 410 u
120-83-2--------2,4-0ichlorophenol 410 u
120-e2-1----~---1,2,4-Trichlorobenzene 410 u
91.-20-3---------Naphthalene 410 u
106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7~--------4-Chloro-3-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47~4---------Hexachlorocyclopentadiene_ 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene . 410 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------oimethyl Phthalate 410 U.
208-96-8--------Acenaphthylene 410 u
606-20-2--------2,6-0initrotoluene 410 u
FORM I sv-1 1/87 Rev.
,
--L ~ -• "":;.. -. .--.-.-I I .... -•"""' r"I, I f
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS SB4-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/water) SOIL Lab Sample IO: 360289
Sample 1.rt/vol: 30,1 (g/mL) ~ Lab File IO: GHQ !i o 2 B 2 al~
Level: (low/med) LOW Date Received: 07/28/90
I Moisture: not dee. ~ dee. Date Extracted: 07/31/90
Extraction:
GPC Cle~1nup:
(SepF/Cont/Sonc)
(Y/N) li.._
~
pH:~
Date Analyzed: 08/13/90
Dilution Factor: .1~.o,._ __
CONCENTRATION UNITS:
C:AS NO. COMPOUND (ug/L or ug/Kg) UG/KG
9
8
9-09-2---------3-Nitroaniline
3-32-9---------Acenaphthene
1-28-5---------2,4-0initrophenol
00-02-1----•---4-Nitrophenol
32-64-9--------0ibenzofuran
21-14-2--------2,4-0initrotoluene
4-66-2---------0iethylphthalate
005-72-3-------4-Chlorophenyl-phenylether_
6-73-7---------Fluorene
00-01-6--------4-Nitroaniline
34-52-1--------4,6-Dinitro-2-Methylphenol_
6-30-6---------N-Nitrosodiphenylamine (l)_
Ol-55-3--------4-Bromophenyl-phenylether __
18-74-l--------Hexachlorobenzene
'7-86-5---------Pentachlorophenol
!5-0l-8---------Phenanthrene
20-12-1--------Anthracene
4-74-2---------Di-n-Butylphthalate
06-44-0--------Fluoranthene
29-oo-o--------Pyrene
5-68-7---------Butylbenzylphthalate
l-94-1---------3,3'-Dichlorobenzidine
li-55-3---------Benzo ( a) Anthracene
l.8-0l-9--------Chrysene
l.7-8l-7--------bis(2-Ethylhexyl)Phthalate_
l.7-84-0--------oi-n-octyl Phthalate
05-99-2--------Benzo(b)Fluoranthene
07-08-9--------Benzo(k)Fluoranthene
0-32-8---------Benzo(a)Pyrene
93-39-5--------Indeno(l,2,J-cd)Pyrene
J-70•3---------0ibenzo(a,h)Anthracene
·S
l
l
l
8
7
8
l
5
8
l
l
8
8
l
8
2
l
8
9
5
2
l
1
2
2
5
1
5
l 91-24-2--------Benzo(g,h,i)Perylene
(~-cannot be separated from Oiphenylamine
FORM I sv-2
2000 u
410 u
2000 u
2000 u
410 u
410 u
410 u
410 u
410 u
2000 u
2000 u
410 u
410 u
410 u
2000 u
410 u
410 u
410 u
410 u
410 u
410 u
810 u
410 u
410 u
410 u
410 u
410 u
410 u
410 u
410 u
410 u
410 u
1/87 Rev.
Q
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Nam«1: COMPUCHEM, RTP Contract: 12-881-REVS SB4-2-l
Lab Code: COMPU Casa No.: 20937 SAS No.: SDG No. : ..,.2.,._2 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) lL._
Level: (low/med) LOW
I Moisture: not dee. __l.9. dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) ·H__ pH: -5......§.
Number T:[Cs found: __o
CAS NUMBER COMPOUND NAME
Lab Sample ID: ..,3.,.6,._0 2"'8._9.__ __ _
Lab Fila ID: GH060289B15
Date Received: 07/28/90
Date Extracted: 07/31/90
Date Analyzed: . 08/13/90 ·
Dilution Factor: ~1 •. ~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
•••••o•nDn====•• a=========•=============••== =•====== m============ =====
FORM I SV-TIC 1/87 Rev.
I
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: C2-88)-REVS
Lab Code!: COMPU Casa No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
SB5-l-l
No.: I Matrix: (soil/water) SOIL
22
Lab Sample ID: 360290
I
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B
R
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Sample wt/vol: 30,1 (g/mL) ~ Lab Fila ID: !:iH06029QE!l~
Leval: ( low/med) LOW Date Received: 071'.281'.90
I Moisture: not dee. --1.J. dee. Date Extracted: 071'.311'.90
ExtractJ.on: (SepF/Cont/Sonc) Data Analyzed: 081'.131'.90
GPC Cleanup: (Y/N) .IL_ pH:~ Dilution Factor: _1~,o __ _
CONCENTRATION UNITS:
C:AS NO. COMPOUND (ug/L or ug/Kg) U!:il'.K!:i Q
108-95-2--------l?henol 380 u lll-44-4--------bis(2-Chloroethyl)Ether '380 u 95-57-8---------2-Chlorophenol 380 u 541-73-1--------1,3-Dichlorobenzene 380 u 106-46-7--------1,4-Dichlorobenzena 380, u 100-51-6----~---Benzyl Alcohol 380 u 95-so-1---------1,2~Dichlorobenzene 380 u 95~48-7---------2-Methylphenol 380 u 39638-32~9------bis(2-Chloroisopropyl)Ether_ 380 u 106-44-5--------4-Methylphenol 380 u 621-64~7--------N-Nitroso-Di-n-l?ropylamine_ 380 u 67-72-1---------Hexachloroethane 380 u 98-95-3---------Nitrobenzene 380 u 78-59-1---------Isophorone 380 u 88-75-5---------2-Nitrophenol 380 u 105-67-9--------2,4-Dimathylphenol 380 u 65-85-o---------Benzoic Acid 1800 u
1.11-91-1--------bis ( 2·-chloroethoxy) Methane_ 380 u 120-83-2--------2,4-Dichlorophenol 380 u
120-82-1--------1,2,4-Trichlorobenzene 380 u
91-20-3---------Naphthalene 380 u 11)6-4 7-8--------4-Chloroanil ina 380 u 8".7-68-3----~·----Hexachlorobutadiena 380 u
59-50-7---------4-Chloro-3-Methylphenol 380 u
9:L-57-6---------2-Methylnaphthalene 380 u
77-47-4---------Hexachlorocyclopentadiene __ 380 u
86-06-2---------2,4,6-Trichlorophenol . 380 u
9!i-95-4---------2, 4, 5-Trichlorophenol 1800 u
9l.-58-7---------2-Chloronaphthalena 380 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl l?hthalata 380 u
208-96-8--------Acenaphthylene 380 u
606-20-2--------2,6-Dinitrotoluene 380 u
FORM I sv-1 1/87 Rav.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab NamE1: COHPUCHEH, RTP Contract: (2-881-REVS SB5-l-l
Lab Code: CQHPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360290
Sample wt/vol: 30.1 (g/mL) L-Lab File ID: GH060290B15
Level: (low/med) LOW Date Received: 07/28/90
, Moisture: not dee. --1.l dee. Date Extracted: OZ/31/90
Extracti,Jn:
GPC Clea1,up:
( SepF /Cont/ Sonc)
(Y/N) li._ pH:~
Date Analyzed: 08/13/90
Dilution Factor: ~i~,o._ __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
-09-2---------3-Nitroaniline
3-32-9---------Acenaphthene
1-28-5---------2,4-Dinitrophenol
0-02-1--------4-Nitrophenol
32-64-9--------Dibenzoturan
1-14-2--------2,4-Dinitrotoluene
-66-2---------Diethylphthalate
99
8
5
10
1
12
84
7 005-72-3-------4-Chlorophenyl-phenylether_
8
1
5
6-73-7-~-------Fluorene
8
1
1
8
8
1
8
2
1
8
9
5
2
1
1
2
,2
5
1
00-01-6--------4-Nitroaniline
34-52-1-------~4,6-Dinitro-2-Methylphenol_
6-30-6---------N-Nitrosodiphenylamine (1)_
01-55-3--------4-Bromophenyl-phenylether
1,8-74-1--------Hexachlorobenzene · --
7·-86-5---------Pentachlorophenol
5·-01-8---------Phenanthrene
21)-12-1--------Anthracene
4 .• 7 4-2---------Di-n-Butylphthalate
06-44-o~-------Fluoranthene
29-00-0--------Pyrene
5··68-7---------Butylbenzylphthalate
1-94-1---------3,3'-Dichlorobenzidine
6··55-3---------Benzo ( a) Anthracene
lS-01-9--------Chrysene
17-81-7--------bis(2-Ethylhexyl)Phthalate_
17-84-0--------Di-n-Octyl Phthalate
05-99-2--------Benzo(b)Fluoranthene
07-08-9--------Benzo(k)Fluoranthene
0-32-8---------Benzo(a)Pyrene
93-39-5--------Indeno(l,2,3-cd)Pyrene
J-70-3---------Dibenzo(a,h)Anthracene 5
1 91-24-2--------Benzo(g,h,i)Perylene
<If""= Cannot be separated trom D1phenylamine
1800
380
1800
1800
380
380
380
380
380
1800
1800
380
380
380
1800
380
380
380
380
380
380
760
380
380
100
380
380
380
380
380
380
380
u
u u u
u
u u u
u
u
u u
u u. u
u u u u u
u u u u
J u
u u
u u
u u
FORM I sv-2 1/87 Rev.
Q
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name,: COMPUCHEM, RTP Contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample ID:
SB5-l-l
No.: 22
360290
Sample wt/vol: 30.1 (g/mL) L-Lab File IO: GH060290B15
Level: (low/med) ,.LQ...,W..___
I Moisture: not dee. _l.J.
Extracti-on:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H._
Number T:ccs tound: .....U.
dee.
~
pH: .....L.i
CAS NUMBER COMPOUND NA.ME
Date Received: 07/28/90
Date Extracted: 07/31/90
Date Analyzed: 08/13/90
Dilution Factor: &1~1 0.,_ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q a•••=••a•=-==-•:aa::z::r ••a====-===-a•====•===-=======:::11 :aaa•=r:::11::za::=s ••:::11==•:::11••---=-a:a:a== l. ALOOL 6. l8 270 AJ 2. 29Ell2-i9-l HYOROXYLAMINE, 0-0ECYL-• 10.67 340 J 3. 54105-67-8 HEPTADECANE, 2,6-DIMETHYL--ll.34 990 J 4. 6251-78-7 HEPTADECANE ll.97 2300 J 5. UNKNOWN HYDROCARBON 12.57 1100 J 6. UNKNOWN HYDROCARBON 12.64 460 J 7. 541.05-67-8 HEPTAOECANE, 2,6-0IMETHYL-13.15 1700 J 8. UNKNOWN 13.25 420 J 9. UNKNOWN lJ. 62 690 J 10. UNKNOWN HYDROCARBON 13.69 760 J ll. UNKNOWN 14.09 500 J 12. UNKNOWN HYDROCARBON l4. 20 690 J 13. UNKNOWN 14.40 610 J l4. UNKNOWN HYDROCARBON 15.37 1100 J 15. UNKNOWN 15.67 730 J 16. UNKNOWN HYDROCARBON 15.84 730 J 17. UNKNOWN 16.00 690 J 18. TRIMETHYL OECANE 16.17 380 J 19. UNKNOWN 16.22 310 J 20. UNKNOWN HYDROCARBON 16.35 380 J 2l. UNKNOWN HYDROCARBON· 16.94 380 J
FORM I SV-TIC 1/87 Rev.
' ' ..,.~o"T, '"'.'l...,i ~,..,MOf.'""r:~ naT~ ~JJMMOOU
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEH.RTP Contract: (2-88)-REVS SB5-2-l
Lab Code: COMPU Case No.: 20937
Matrix: (■oil/water) SOIL
Sample wt/vol: 30.2 (g/mL) ~
· Level: (low/med) LOW
I Moisture: not dee. _u
Extract:Lon:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) tL_
dee.
~
pH:~
SAS No.: SOG No. : .2_2~-
Lab Sample IO: &3&60,._2,._9~1..._ __ _
Lab File IO: GH060291B15
Date Received: 07/28/90
Date Extracted: 07/31/90
Date Analyzed: 08/13/90
Dilution Factor: 1.00
C:AS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
.08-95-2--------Phenol
ll-44-4--------bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
41-73-1--------1,3-0ichlorobenzene
06-46-7--------1,4-0ichlorobenzene
00-51-6--------Benzyl Alcohol
5-50-1---------1,2-oichlorobenzene
5-48-7---------2-Methylphenol
l
l
9
5
l
l
9
9
3
1
6
6
9
7
8
1
6
1
1
1
9
9638-32-9------bis(2-Chloroisopropyl)Ether_
06-44-5--------4-Methylphenol
21-64-7--------N-Nitroso-oi-n-Propylamine __
7-72-1---------Hexachloroethane
B-95-3---------Nitrobenzene
8-59-1---------Isophorone
8-75-5---------2-Nitrophenol
05-67-9-------.-2, 4-0imethylphenol
5-ss-o---------Benzoic Acid
:Ll-91-1--------bis ( 2-Chloroethoxy) Methane_
:zo-83-2--------2, 4-0ichlorophenol
20-s2-1--------l,2,4-Trichlorobenzene
l-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
7-68-3---------Hexachlorobutadiene
9-50-7---------4-Chloro-3-Methylphenol
8
5
9
7
8
l-57-6---------2-Methylnaphthalene
7-47-4---------Hexachlorocyclopentadiene __
s-06-2---------2,4,6-Trichlorophenol
9~-95-4---------2,4,5-Tiichlorophenol
9
8
l.-58-7---------2-Chloronaphthalene
8-74-4---------2-Nitroaniline
131-11-3--------oimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-0initrotoluene
FORM I sv-1
a ~1 r
430 u
430 u
430 u
430 u 430 u
' 430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
2100 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
2100 u l 430 u
2100 u
430 u
430 u
430 u
1/87 Rav.
a V 93
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM,RTP Contract: (2-88l-REVS SB!!-2-1
Lab Code : COMPU Cas• No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/wat•r) SOIL Lab Sample ID: 360291
Sample wt/vol: 30.2 (g/mL) ~ Lab File ID: !:iH060291E!l2
Level: (low/med) LOW Date Received: 07/28/90
% Moisture: not dee. ____u dee. Date Extracted: Q7131/9Q
Extracti,:m: (SepF/Cont/Sonc)
(Y/N) H_
~
pH: ...i..l.
Date Analyzed: 08/1J/9Q
GPC Clea11up: Dilution Factor: 1.00
CONCENTRATION UNITS:
CJ~S NO. COMPOUND (ug/L or ug/Kg) U!:j/K!:j
J-09-2---------3-Nitroaniline
3-32-9---------Acenaphthene
1-2e-s---------2,4-Dinitrophenol
10-02-7--------4-Nitrophenol
32-64-9--------Dibenzofuran
21-14-2--------2,4-Dinitrotoluene
4-66-2---------Diethylphthalate
005-72-3-------4-Chlorophenyl-phenylether_
6-73-7---------Fluorene
gc
8
5
lC
1
1
8
7
8
1
5
8
1
1
8
8
1
8
2
1
8
9
5
2
1
1
2
2
5
1
5
1
00-01-6---~----4-Nitroaniline
34-52-1--------4,6-Dinitro-2-Methylphenol_
6-30-6---------N-Nitrosodiphenylamine (1)_
01-55-3--------4-Bromophenyl-phenylether __
18-74-1--------Hexachlorobenzene
7-86-5---------Pentachlorophenol
!5-01-e-------~-Phenanthrene
20-12-1--------Anthracene
4-74-2--~------Di-n-Butylphthalate
06-44-o--~-----Fluoranthene
29-oo-o--------Pyrene
5-68-7---------Butylbenzylphthalate
1-94-1---------3,3 1 -Dichlorobenzidine
6-55-3---------Benzo(a)Anthracene
18-01-9--------chrysene .
17-81-7--------bis(2-Ethylhexyl)Phthalate_
1'7-84-o--------Di-n-Octyl Phthalate
05-99-2--------Benzo(b)Fluoranthene
07-08-9--------Benzo(k)Fluoranthene
0·•32-8---------Benzo (a) Pyrene
9:l-39-!5--------Indeno ( 1, 2, 3-cd) Pyrene
3·•70-3---------Dibenzo (a, h) Anthracene
91-24-2--------Benzo(g,h,i)Perylen•
( 1) •· Cannot be separated from Diphenylamin•
FORM I sv-2
2100 u
430 u
2100 u
2100 u
430 u
430 u
430 u
430 u
430 u
2100 u
2100 u
430 u
430 u
430 u
2100 u
430 u
430 u
430 u
430 u
430 u
430 u
850 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
430 u
1/87 Rev.
u
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
·TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab NamEI: COMPUCHEM.RTP Contract: 12-88)-REVS SB.5-2-1
Lab CodEt: COMPU Case No.: 20937 SAS No.: SOG No.: ..,2.._2 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) L_
Level: (low/med) LOW
I Moisture: not dee. --2.3.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li_
Number T:ccs tound: __J.
dee.
.S,OliC
pH: ....iJ.
CAS NUMBER COMPOUND NAME
Lab Sample IO: ,,_J.,.6,..0.._29,,._1.._ __ _
Lab File IO: GH060291B15
Date Received: 07128/90
Date Extracted: 07/31/90
Date Analyzed: 08/13/90
Dilution Factor: .1~.o~o.___
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ••-•=•a1:a:aaaa:m=:::::11= =================•==•=-===••= aa:a::11==== ::1·1:::n::=zz===-•=•==---==== 1. SOLVENT CONTAMINANT
FORM I SV-TIC
' -.
5.28 170 BJ
1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
SB6-l-l
Lab Coda: CQMPU Case No.: 20937 SAS NO.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360292
Sample wt/vol: 30,1 (g/mL) ~ Lab File ID: GJ060292A20
Leval: (low/med) LOW Date Received: 07/28/90
' Moisture: not dee. ___ll dee. Data Extracted: oz131190
Extracti,:in: (SepF/Cont/Sonc) ~ Data Analyzed: 08/22/90
GPC Cleanup: (Y/N) L_ pH: --2....l Dilution Factor: .ii,~0 __ _
Cl\S NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
18-95-2--------Phanol
l-44-4--------bis(2-Chloroethyl)Ether
i-57-8---------2-Chlorophenol
,1-73-1--------1,J-Dichlorobenzena
16-46-7--------1,4-Dichlorobenzene • 0-51-6--------Benzyl Alcohol
-50-1---------1,2-Dichlorobenzena
-48-7---------2-Methylphenol
1(
ll
9!
54
lC
10
95
95
39
10
62
67
98
78
88
10
6
1
1
1
9
1
8
5
9
7
8
9
9
8
1
2
6
638-32-9------bis(2-Chloroisopropyl)Ether_
6-44-5--------4-Mathylphenol
1-64-7--------N-Nitroso-Di-n-Propylamine_
-12-1---------Hexachloroethana
-95-3---------Nitrobenzena
-59-1---------Isophorona
-75-5---------2-Nitrophenol
5-67-9--------2,4-Dimethylphenol
5-85-o---------Benzoic Acid
ll-91-l--------bis(2-Chloroethoxy)Methane_
20-83-2--------2,4-Dichlorophenol
20-82-1--------1,2,4-Trichlorobenzene
1·20-3---------Naphthalene
06-47-8--------4-Chloroaniline
7·-68-3---------Hexachlorobutadiena
9-50-7---------4-Chloro-J-Methylphenol
1·•57-6---------2-Methylnaphthalene
7··47-4---------Hexachlorocyclopentadiene __
8··06-2---------2, 4, 6-Trichlorophenol
5-95-4---------2,4,5-Trichlorophenol
1··58-7---------2-Chloronaphthalena
8••7 4-4---------2-N i troanil ina
31-11-3--------Dimethyl Phthalata
08-96-8--------Acenaphthylene
06-20-2--------2,6-Dinitrotoluena
420
420
420
420
420
420
420
420
420
420
420
420
420
420
420
·420
2000
420
420
420
420
420
420
420
420
420
420
2000
420
2000
420
420
420
u u
u u u
u u u
u u u u
u
u
u u u
u
u
u
u u u
u u u u
u u u
u u u
FORM I sv-1 1/87 Rav.
20937 22 sAnPLE DATA SUMMARY
Q
91:1
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SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
SB6-l-l
Lab Code1: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: ( soil/water) SOIL Lab Sample ID: 360292
Sample wt/vol: 30,1 (g/mL) L_ Lab File ID: GJ060292A20
Level: (low/med) LOW Data Received: 07/28/90
' Moisture: not dee. _ll dee. Date Extracted: 07/31/90
Extraction:
GPC Clea:nup:
(SepF/Cont/Sonc)
(Y/N) li___
~
pH:~
Date Analyzed: 08/22/90
Dilution Factor: &1~1 0._ __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
9
8
5
1
1
1
8
7
8
1
5
8
1
1
8
8
1
8
2
1
8
9
5
2
1
1
2
2
5
1
5
1
9-09-2---------3-Nitroaniline
J-32-9---------Acenaphthene
1-28-5---------2,4-Dinitrophenol
OO-Q2-7--------4-Nitrophenol
32-64-9--------Dibenzoturan
21-14-2--------2,4-Dinitrotoluene
4-66-2---------Diethylphthalate
c,os-12-3-------4-Chlorophenyl-phenylather_
6-73-7---------Fluorene
00-01-6--------4-Nitroaniline
34-52-1--------4,6-Dinitro-2-Hethylphenol_
6-30-6-~-------N-Nitrosodiphenylamine (1)_
01-55-3--------4-Bromophenyl-phenylether_
18-74-1--------Hexachlorobenzene
7-86-5---------Pentachlorophenol
5-01-8---------Phenanthrene
20-12-1--------Anthracene
4-74-2---------Di-n-Butylphthalate
06-44-0--------Fluoranthene
29-00-o--------Pyrene
5-68-7---------eutylbenzylphthalate
l·-94-1---------3, 3 1 -Dichlorobenzidine
6··55-3---------Benzo ( a) Anthracene
113-01-9--------Chrysene
1'7-81-7--------bis(2-Ethylhexyl)Phthalate_
17-84-0-----~--Di-n-Octyl Phthalata
0!5-99-2--------Benzo(b) Fluoranthene
07-08-9--------eenzo(k)Fluoranthena
0··32-8---------eenzo ( a) Pyrene
9:1-39-5-----.;--Indeno ( 1, 2, 3-cd) Pyrene
3··70-3---------Dibenzo ( a, h) Anthracene
91.-24-2--------Benzo(g,h,i)Perylene
( 1) •· cannot be separated __ from Diphenylamina
2000
420
2000
2000
420
420
420
420
420
2000
2000
420
420
420
2000
420
420
52
420
420
420
840
420
420
180
420
420
420
420
420
420
420
u u
u u u u
u u u
u u
u u u
u
u
u
J u u u
u u u
BJ u
u u u
u u
u
FORM I sv-2 1/87 Rav.
t --~~--· --------.......... .--..
Q
,., ,..
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
SB6-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: a2.a.2 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) li....__
Level: (low/med) LOW
t Moistu.re: not dee. __n dee.
GPC Clea1,up:
(SepF/Cont/Sonc)
(Y/N) .ti_
~
pH: ~
Number TJ:Cs found: ....2..0.
CAS NUMBER COMPOUND NAME
Lab Sample ID:
. Lab File ID:
Date Received:
Date Extracted:
Date Analyzed: l
Dilution Factor:
CONCENTRATION UNITS:
(ug/L·or ug/Kg) UG/KG
RT EST.
360292
GJ0§0292A20
07/28/90
07/31/90
08/22/90
1,0
CONC. Q ama=•=-=~•••a•=na --=-======================== --=====::::11 •••====-••:a=-•• --=== 1. DIMETHYLHEPTADECANE 11.19 1300 J 2. 629-78-7 HEPTADECANE 11.85 3500 J 3. UNKNOWN 12.50 2000 J 4. DIMETHYLHEPTADECANE 13.10 1700 J 5. UNKNOWN 15.92 1900 J 6. UNKNOWN 16.24 1900 J 7. UNKNOWN 16.74 1800 J 8. UNKNOWN 16.85 2900 J 9. UNKNOWN 17.00 2500 J 10. UNKNOWN 17.19 4700 J
11. 629-97-0 DOCOSANE 17.30 3600 J
12. UNKNOWN 17.45 2600 J 13. UNKNOWN 17.62 1900 J
14. UNKNOWN HYDROCARBON 17 .82 1400 J
15. UNKNOWN 18.00 1200 J
16. UNKNOWN 18.10 1400 J
17. UNKNOWN 18.25 1700 J
18. UNKNOWN 18.49 1400 J
19. UNKNOWN 19. 32 1400 J
20. UNKNOWN 19.99 1700 J
FORM I SV-TIC 1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB6-2-l Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab CodE1: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360293
sample wt/vol: 30.4 (g/mL) L_ Lab File ID: GH060293B15 .
Level: (low/med) LOW Date Received: 02,:'.28l'.90
I Moisture: not dee. ---11. dee. Date Extracted: 07l'.3ll'.90
Extraction: (SepF/Cont/Sonc)
(Y/N) H__
.s.oH.C
pH: ..2.,..l
Date Analyzed: 08l'.13l'.90
GPC Cleanup: Dilution Factor: &1~1 0,._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGl'.KG
08-95-2--------Phenol 1
1
9
5
1
1
9
9
3
1
6
6
9
7
8
1
6
1
1
1
9
1
8
5
9
7
8
9
9
8
1
2
6
ll-44-4--------bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
41-73-1--------1,3-Dichlorobenzene
06-46-7--------1,4-Dichlorobenzene
00-51-6--------Benzyl Alcohol
5-50-1---------1,2-Dichlorobenzene
5-48-7----~----2-Methylphenol
9638-32-9------bis(2-Chloroisopropyl)Ether_
06-44-5------~-4-Methylphenol
21-64-7--------N-Nitroso-Di-n-Propylamine_
7-72-1---------Hexachloroethane
8-95-3---------Nitrobenzene
8-59-1---------Isophorone
8-75-5--~------2-Nitrophenol
05-67-9--------2,4-Dimethylphenol
5-85-o---------Benzoic Acid
ll-91-l-~------bis(2-Chloroethoxy)Methane_
20-83-2----~--~2,4-Dichlorophenol
20-e2-1--------1,2,4-Trichlorobenzene
1-20-3---------Naphthalene
06-47-8--------4-Chloroaniline
7-68-3---------Hexachlorobutadiene
9-50-7---------4-Chloro-3-Methylphenol
1-57-6---------2-Methylnaphthalene
7-47-4---------Hexachlorocyclopentadiene __
8-06-2---------2,4,6-Trichlorophenol
5·•95-4---------2, 4, 5-Trichlorophenol
1··58-7-------...;-2-Chloronaphthalene
8-74-4---------2-Nitroaniline
31-11-3--------Dimethyl Phthalate
OB-96-8--------Acenaphthylene
06-20-2--------2,6-Dinitrotoluene
FORM I sv-1
150 J
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
2400 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
490 u
2400 u
490 u
2400 u
490 u
490 u
490 u
1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS SB6-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360293
Sample wt/vol: 30.4 (g/mL) L_ Lab File ID: GH06029JB15
Level: (low/med) LOW Date Received: 07/28/90
!Ii Moistu:re: not dee. _.1,3. dee. Date Extracted: 07 /31/90
Extractic)n: ( SepF /Cont/ Sonc)
GPC Cleanup: (Y/N) 1:L..
5..0fil:
pH: ....2...1
Date Analyzed: 08/13/90
Dilution Factor: ..,1,...0,._ __
CJ~S NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2400
83-32-9---------Acenaphthene 490
51-28-5---------2,4-Dinitrophenol 2400 100-02-1--------4-Nitrophenol 2400 132-64-9--~-----Dibenzofuran 490
121-14-2--------2,4-Dinitrotoluene. 490
84-66-2---------Diethylphthalate 490
7005-72-3-------4-Chlorophenyl-phenylether_ 490
86-73-7---------Fluorene 490 100-01-6--------4-Nitroaniline 2400
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2400
86-30-6---------N-Nitrosodiphenylamine (l)_ 490
101-55-3--------4-Bromophenyl-phenylether __ 490
118-74-1--------Hexachlorobenzene 490
87-86-5---------Pentachlorophenol 2400
85-01-8----------Phenanthrene 490
120-12-1--------Anthracene 490
84-74-2---------Di~n-Butylphthalate 490
206-44-o--------Fluoranthene 490
129-00-0--------Pyrene 490
85-68-7---------Butylbenzylphthalate 490
91-94-1---------3,3'-Dichlorobenzidine 970
56-55-3---------Benzo(a)Anthracene 490
218-01-9--------Chrysene 490
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 490
117-84-0--------Di~n-Octyl Phthalate 490
2015-99-2--------Benzo(b) Fluoranthene 490
207-08-9--------Benzo(k)Fluoranthene 490
50··32-8---------Benzo ( a) Pyrene 490
193-39-5--------Indeno(l,2,3-cd)Pyrene 490
53-70-3---------Dibenzo(a,h)Anthracene 490
19:L-24-2--------Benzo(g,h,i)Perylene 490
( 1) •· cannot be separated from Diphenylamine
u u u
u
u u
u
u
u u
u u
u u
u
u u u
u
u u u
u u
u
u u u
u
u u
u
FORM I sv-2 1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COHPUCHEM.RTP Contract: 12-881-REVS SB6-2-l
Lab Code,: COHPU Casa No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL) li.___
Laval: ( low/mad) LOW
I Moisture: not dac. --3..3. dac.
Extraction: (SapF/Cont/Sonc) ~
GPC Cleanup: (Y/N) tL__ pH:~
Number T:CCs found:~
CAS NUMBER COMPOUND NAME
SAS No.: __ _ SOG No. : .,.2_2 __
Lab Sample IO: ,.3""6"'0_.2.._9.._J __ _
Lab Fila IO: GH060293B15
Data Received: 07/28/90
Date Extracted: 07/31/90
Data Analyzed: 08/13/90
Dilution Factor: _1~,~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
-----••:a:■:a:a:::a=r-•=-=~==•=====:::s:a:::1:::1::::s::::aa:m:aaaa:a== •===-===--••m:a•••••=a•• ----= l. SOLVENT CONTAMINANT 5.30 250 BJ 2. UNKNOWN 6.68 830 J 3. UNKNOWN 6.72 690 J 4. UNKNOWN 13.80 250 J 5. 4337-65-9 HEXANEOIOIC ACID, MON0(2-ETH 15.74 440 J
FORM I SV-TIC 1/87 Rav.
...... .r91 IM , ... , oc:
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
SB9-l-l
Lab Code : COMPU Casa No.: 20937 SAS No.: SDG No.: ..,2_..,2 __
Matrix: (soil/water) SOIL · Lab Sample ID: 360850
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH06ossoco1
Level: (low/med) LOW Data Received: 08/01/90
t Moisture: not dee. __li dee. Data Extracted: 0§/03/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/14/90
Dilutio'n Factor: ,.1..,,.,.0.,.0 __
CONCENTRATION UNITS:
GPC Cleanup: (Y/N) tL_ pH: ...-2.Li
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
l(
l
9. s,
>8-95-2--------Phenol
11-44-4--------bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
ll-73-l--------l,3-Dichlorobenzene
l
l
9
9
3
l
6
6
9
7
8
l
6
l
l
l
9
l
8
5
9
7
8
9
9
8
l
2
6
06-46-7--------1,4-Dichlorobenzene
00-51-6--------Benzyl Alcohol
5-50-1---------1,2-Dichlorobenzene
~i-48-7---------2-Methylphenol
9638-32-9------bis(2-Chloroisopropyl)Ether_
06-44-5--------4-Methylphenol
:2. l-64-7--------N-Ni troso-Di-n-Propylamine __
7-72-1---------Hexachloroethane
8-95-3---------N i trobenzen·e
8-59-1---------Isophorone
8-7s-s---------2~Nitrophenol
05-67-9--------2,4-Dimethylphenol
5-85-o---------Benzoic Acid
ll-9l-l--------bis(2-Chloroethoxy)Methane_
20-83-2--------2,4-Dichlorophenol
20-82-1--------l,2,4-Trichlorobenzene
1-20-J---------Naphthalene
06-47-8--------4-Chloroaniline
7-68-3---------Hexachlorobutadiene
9-50-7---------4-Chloro-3-Methylphenol
1-57-6---------2-Methylnaphthalene
7-47-4---------Hexachlorocyclopentadiene __
S·-06-2---------2, 4, 6-Trichlorophenol
5·-95-4---------2, 4, 5-Trichlorophenol
l·-58-7---------2-Chloronaphthalene
8··74-4---------2-Nitroaniline
J:L-ll'."3--------Dimethyl Phthalata
OB-96-8--------Acenaphthylene
OtS-20-2--------2,6-Dinitrotoluena
..
FORM I SV-l
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
380 u
39 J
380 u
380 u
· 380 u
380 u
380 u
380 u
1900 u
380 u
380 u
380 u
150 J
380 u
380 u
380 u
490
380 u
380 u
1900 u
380 u
1900 u
380 u
380 u
380 u
1/87 Rev.
----.-.......... _ -·· ......
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
S89-l-l Lab Namll: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Cod11: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360850
Sample wt/vol: 30.0 (g/mL) !i...._ Lab File ID: GH060850C07
Level: (low/med) LOW Date Received: 08/01/90
I Moisture: not dee. _ll dee. Date Extracted: 08/0J/90
Extraction:
. GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ti..._
~
pH: ..i._i
Date Analyzed: 08/14/90
Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L.or ug/Kg) UG/KG Q
9
8
5
1
1
1
8
7
8
1
5
8
1
1
8
8
1
8
2
1
8
9
5
2
1
1
2
2
5
1
5
1
9-09-2-----~---3-Nitroaniline
3-32-9---------Acenaphthene
l-28-5-----~---2,4-Dinitrophenol
00-02-1--------4-Nitrophenol
32-64-9--------Dibenzoturan
Zl-14-2--------2,4-Dinitrotoluene
,-66-2---------Diethylphthalate
c,os-12-3--:-----4-Chlorophenyl-phenylether __
6-73-7---------Fluorene
00-01-6--------4-Nitroaniline
34-52-1--------4,6-Dinitro-2-Methylphenol_
6-30-6---------N-Nitrosodiphenylamine (1)_
01-55-3--------4-Bromophenyl-phenylether __
18-74-1--------Hexachlorobenzene
7-86-5---------Pentachlorophenol
5-01-8---------Phenanthrene
20-12-1--------Anthracene
4-74-2---------Di-n-Butylphthalate
06-44-0--------Fluoranthene
29-oo-o--------Pyrene
5-68-7---------Butylbenzylphthalate
1-94-1---------3,3'-Dichlorobenzidine
6-55-3---------Benzo(a)Anthracene
18-01-9--------chrysene
1'7-81-7--------bis (2-Ethylhexyl) Phthalate_
1'7-84-0--------Di-n-Octyl Phthalate
05-99-2--------Benzo(b)Fluoranthene
07-08-9--------Benzo(k)Fluoranthene
0··32-8---------Benzo ( a) Pyrene
93-39-5--------Indeno(l,2,3-cd)Pyrene
3··70-3---------Dibenzo (a, h) Anthracene
9].-24-2--------Benzo (g, h, i) Perylene
( 1) -· cannot be separated trom Dlphenylamina
FORM I sv-2
1900 u
.380 u
1900 u
1900 u
380 u
380 u
380 u
380 u
210 J
1900 u
1900 u
380 u
380 u
380 u
1900 u
410
380 u
380 u
380 u
380 u
380 u
770 u
380 u
380 u
920
380 u
380 u
380 u
380 u
380 u
380 u
380 u
1/87 Rav.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-88}-REVS SB9-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360850
Sample wt/vol: Jo.a (g/mL) L_ Lab File ID: GH060850C07
Level: (low/med) LOW Date Received: 08/01/90
\ Moisture: not dee. _li dee. D.tte Extracted: 08/0J/90
Extraction: Date Analyzed: 08/14/90
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...._ pH: ....5.,_9_ Dil~tion Factor: .1~,0~0.__
Number TICs found: _ll.
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT 'EST. CONC. Q
===-==n•m~===•~=• •m====---====---==----=-=--= ======== :=1=====-==-==•=-= =====
l. ALDOL 5.88 2200 AJ
2. UNKNOWN 5.95 2100 J
3. TRIMETHYLDECANE 6.25 7400 J
4. TRIMETHYLDECANE 6.43 2600 J
5. UNKNOWN 6.70 1800 J
6. UNKNOWN 6.75 3300 J
7. TRIMETHYLDECANE 7.02 12000 J
8. UNKNOWN 7.13 3600 J
9. UNKNOWN 7.72 3500 J
10. UNKNOWN 8.39 5000 J
11. UNKNOWN 8.77 2300 J
12. DIMETHYIJiEPTADECANE 9.00 '6200 J
13. UNKNOWN HYDROCARBON 9.35 4300 J
14. TRIMETHYLDECANE 9.57 8100 J
15. . UNKNOWN 9.97 1800 J
16. UNKNOWN 10.12 8500 J
17. DIMETHYLUNDECANE 10. 37 6600 J
18. 4-(TETRAMETHYLBUTYL)PHENOL 10.65 8900 J
19. DIMETHYLUNDECANE 11.14 2100 J
20. TRIMETHYLDECANE ll.60 7000 J
21. DIMETHYLUNDECANE 12. 05 2900 J
FORM I SV-TIC 1/87 Rav.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SKEET EPA SAMPLE NO,
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS SB9-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360853
Sample 1,t/vol: JQ.Q (g/mL) L_ Lab File ID: GH0608:!JA07
Level: (low/med) LOW Date Received: 08.:'.0l.:'.90
I Moisture: not dee. _ll dee. Date Extracted: 08,:'.03.:'.20
Extraction: (SepF/Cont/Sonc)
(Y/N) H_
.~
pH: ....L..i
Date Analyzed: os.::is.::20
GPC Cleanup: Dilution Factor: l,OO
CAS NO, COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG
108-95-2--------Phenol 82 lll-44-4--------bis(2-Chloroethyl)Ether 470 95-57-8---------2-Chlorophenol 470 541-73-1--------1,J-Dichlorobenzene 470 106-46-7--------1,4-Dichlorobenzene 470 100-51-6--------Benzyl Alcohol 470 95-50-1------.,.--1,2-Dichlorobenzene 470 95-48-7---------2-Methylphenol 470 J9638-J2-9------bis(2-Chloroisopropyl)Ether_ 470 106-44-5-~------4-Methylphenol 470 621-64-7--------N-Nitroso-Di-n-Propylamine __ 470 67-72-1---------Kexachloroethane 470 98-95-3---------Nitrobenzene 470 78-59-1---------Isophorone 470 88-75-5---------2-Nitrophenol 470 105-67-9--------2,4-Dimethylphenol 470 65-85-o---------Benzoic Acid 92 lll-91-l--------bis(2-Chloroethoxy)Methane __ 470 120-83-2--------2,4-Dichlorophenol 470 120-02-1--------l,2,4~Trichlorobenzene 470 91··20-3---------Naphthalene 470 106-47-8--------4-Chloroaniline 470 87·•68-3---.:..-----Kexact:ilorobutadiene 470 59··50-7---------4-Chloro-J-Methylphenol 470 91-57-6~--------2-Methylnaphthalene 470 77••47-4---------Kexachlorocyclopentadiene __ 470 88-06-2---------2,4,6-Trichlorophenol 470
95-95-4---------2,4,5-Trichlorophenol 61 91•·58-7---------2-,Chloronaphthalena 470
88-74-4---------2-Nitroaniline 2300 131-11-3--------Dimethyl Phthalata 470
208-96-8--------Acenaphthylene 470 606-20-2--------2,6-Dinitrotoluena 470
J
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
J
t1
t1
t1
t1
t1
t1
t1
t1
t1
t1
J
t1
t1
t1
t1
t1
FORM I sv-1 1/87 Rev.
Ttl IMMQ
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP S89-2-l Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360853
sample vt/vol: 30.0 (g/mL) !:i....._ Lab File ID: GH06085JA07
Level: (low/med) LOW Date Received: 08/01/90
I Moisture: not dee. ---1Q dee; Date Extracted: 08,'.0J/90
Extracti,,n:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) ?L..
~
pH: ....L1
Date Analyzed: 08/15/90
Dilution Factor: .1~1~0~0 __
CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) UG/KG
1-09-2---------3-Nitroaniline
1-32-9---------Acenaphthene
.-28-5---------2,4-Dinitrophenol
0-02-1--------4-Nitrophenol
2-64-9--------Dibenzofuran
l-14-2--------2,4-Dinitrotoluene
-66-2---------Diethylphthalate
9S
83
51
10
13
12
84
70
86
10
53
86
10
ll
87
85
12
84
20
12
8
9
5
2
1
l
2
2
5
l
5
1
05-72-3-------4-Chlorophenyl-phenylether_
-73-7---------Fluorene
0-01-6--------4-Nitroaniline
4-52-1--------4,6-Dinitro-2-Methylphenol __
-30-6---------N-Nitrosodiphenylamine (l)_
1-55-3--------4-Bromophenyl-phenylether __
8-74-1--------Hexachlorobenzene
-86-5---------Pentachlorophenol
-01-8---------Phenanthrene
0-12-1--------Anthracene
··74-2---------Di-n-Butylphthalate
,5-44-0--------Fluoranthene
9-oo-o--------Pyrene
5·-68-7---------Butylbenzylphthalate
l-94-1---------3,3'-Dichlorobenzidine
6··55-3---------Benzo ( a) Anthracene
18-01-9--------Chrysene
17-8l-7--------bis(2-Ethylhexyl)Phthalate_
17-84-0--------Di-n-octyl Phthalate
05-99-2--------Benzo(b)Fluoranthene
07-08-9--------Benzo(k)Fluoranthene
0··32-8---------Benzo ( a) Pyrene
93-39-5--------Indeno(l,2,3-cd)Pyrene
3··70-3---------Dibenzo (a, h) Anthracene
91-24-2--------Benzo(g,h,i)Perylene
( l) •· Cannot be separated from Diphenylam.1ne
2300
470
2300
2300
470
470
470
470
470
2300
2300
470
470
470
2300
470
470
470
470
470
470
940
470
470
120
470
470
470
470
470
470
470
u u
u u
u u u
u
u u u
u
u
u u u
u
u
u
u u u
u
u
j
u
u
u u
u
u u
FORM I sv-2 l/87 Rev.
? . 7 22 SQ TA SUMMARY
Q
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11"
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
SB9-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360853
Sample wt/vol: 30.0 (g/mL) !i__ Lab File ID: GH060853A07
Level: (low/med) LOW
I Moisture: not dee. -3..Q dee.
. Extractic,n:
GPC Cleanup:
( SepF /Cont/Sonc)
(Y/N) li.._
~
pH: .....L.i
Number TICS tound: .....2..0.
CAS NUMBER COMPOUND NAME
Date Received: 08/01/90
Date Extracted: 08/03/90
Date Analyzed: 08/15/90
Dilution Factor: ~l~,0~0,___
CONCENTRATION UNITS:
(ug(L or ug/Kg) UG/KG
RT EST. CONC. Q ==----•-=-:11::1=====-=-=-•a•===========•===========-=======• •==========-==-•==== 1. SOLVENT CONTAMINANT 5.13 290 BJ 2. ALDOL 5.88 570 AJ 3. UNKNOWN HYDROCARBON 6.25 290 J 4. UNKNOWN HYDROCARBON 7.02 430 J 5. UNKNOWN 7.48 290 J 6. UNKNOWN HYDROCARBON 8.99 190 J 7. DICHLOROPHENOL 9,22 240 J
8. UNKNOWN HYDROCARBON 9.57 380 J
9. UNKNOWN HYDROCARBON i 10.10 570 J 10. TETRACHLOROPHENOL 10.20 480 J
11. TETRAMETHYLBUTYL PHENOL 10.35 1000 J
12. UNKNOWN HYDROCARBON 10.62 ·1100 J 13. UNKNOWN HYDROCARBON 11.10 430 J
14. UNKNOWN HYDROCARBON 11,17 290 J
15. UNKNOWN HYDROCARBON 11.57 480 J
16. UNKNOWN HYDROCARBON 12.02 330 J
17. UNKNOWN HYDROCARBON 13.54 190 J
18. UNKNOWN HYDROCARBON 14. 02 290 J
19. UNKNOWN 14.39 240 J
20. UNKNOWN 14.60 330 J
FORM I SV-TIC 1/87 Rev.
-.J t. --· ............. -• •' .. ,.,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS 5B4-2-lMS
Lab Code : COMPU Case No.: 20937 SAS No.: SDG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360283
Sample wt/vol: 30.1 (g/mL) !:L_ Lab File ID: GH060~831U:i
Level: (low/med) LOW Date Received: 921'.281'.90
I Moisture: not dee. __li dee. Date Extracted: 071'.311'.90
Extraction: (SepF/Cont/Sonc) .5.QliC Date Analyzed: 081'.131'.90
GPC Cleanup: (Y/N) li__ pH: ....i.,_§. Dilution Factor: A1~1~0 __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UGl'.KG Q
108-95-2--------Phenol . 410 u lll-44-4--------bis(2-Chloroethyl)Ether 410 u 95-57-8---------2-Chlorophenol 410 u 541-73-1--------1,J-Dichlorobenzene 410 u 106-46-7----~---l,4-Dichlorobenzene 410 u 100-51-6--------Benzyl Alcohol 410 u 95-50-1---------1,2-Dichlorobenzene 410 u 95-48-7---------2-Methylphenol 410 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u 106-44-5--------4-Methylphenol 410 u 621-64-7--------N-Nitroso-Di-n-Propylamine __ 410 u 67-72-1---------Hexachloroethane 410 u 98-95-3---------Nitrobenzene 410 u 78-59-1---------Isophorone 410 u 88-75-5---------2-Nitrophenol 410 u 105-67-9--------2,4-Dimethylphenol 410 u 65-85-o---------Benzoic Acid 2000 u lll-91-l--------bis(2-Chloroethoxy)Methane_ 410 u
120-83-2--------2,4-Dichlorophenol 410, u 120-a2-1--------l,2,4-Trichlorobenzene 410 u
91.-20-3---------Naphthalene 410 u 106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7---------4-Chloro-3-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47-4---------Hexachlorocyclopentadiene __ 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 410 u
88-71-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 410 u
208-96-8--------Acenaphthylene 410 u
606~20-2--------2,6-Dinitrotoluene 410 u
FORM I sv-1 •l/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO,
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS SB4-2-1MS
Lab Code: CQMPU Casa No.: 20937 SAS No.: SOG No.: 4242 __
Matrix: (soil/water) SOIL Lab Sample IO: "'-3,.,60"'2..,B._,J.__ __ _
Sample wt/vol: 30.1 (g/mL) Si__ Lab File ID: GH06028JB15
Level: (low/med) LOW
I Moisture: not dee. --1.i dee.
Data Received: 07/28/90
Date Extracted: 07/31/90
Date Analyzed: 08/13/90 Extracticin:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li..,_
.soliC
pH:~ Dilution Factor: .1~1 ~0 __ _
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
-09-2---------3-Nitroaniline
-32-9---------Acenaphthene
-28-5---------2,4-Dinitrophenol
0-02-1--------4-Nitrophenol
2-64-9--------Dibenzoturan
1-14-2--------2,4-0initrotoluene
-66-2---------0iethylphthalate
99
83
51
10
13
12
84
70
86
10
53
86
10
11
87
85
12
84
20
12
85
91
56
21
l
1
20
20
50
19
5
19
05-72-3-------4-Chlorophenyl-phenylether_
-73-7---------Fluorene
0-01~6---~----4-Nitroaniline
4-52-1--------4,6-Dinitro-2-Methylphenol_
-30-6---------N-Nitrosodiphenylamine (l)_
1-55-3--------4-Bromophenyl-phenylether __
8-74-1--------Hexachlorobenzene
-86-5---------Pentachlorophenol
··O 1-8---------Phenanthrene
<)-.12~7--------Anthracene
-74-2---------oi-n-Butylphthalate
6-44-o--------Fluoranthene
9-oo-o----~---Pyrene
•·68-7---------Butylbenzylphthalate
-94-1---------3,3'-Dichlorobenzidine
•·55-3---------Benzo ( a) Anthracene
s-01-9--------Chrysene
l7-8l-7--------bis(2-Ethylhexyl)Phthalate_
17-84-0--------01-n-octyl Phthalate
5-99-2--------Benzo(b)Fluoranthene
7-08-9--------Benzo(k)Fluoranthene
-32-8---------Benzo(a)Pyrene
3-39-5--------Indeno(l,2,3-cd)Pyrene
3-70-3---------Dibenzo(a,h)Anthracena
1-24-2--------Benzo(g,h,i)Perylena
(l} -cannot be separated trom Diphenylam1ne
2000
410
2000
2000
410
410
410
410
410
2000
2000
410
410
410
2000
410
410
410
410
410
410
810
410
410
410
410
410
410
410
410
410
410
u u u
u
u u u u u
u u
u u
u u u
u u u u u
u u u u u u u u u u u
FORM I sv-2 1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEM.RTP Contract: 12-88)-REVS SB4-2-1MSD
Lab Coda: COMPU Case No.: 20937 SAS No.: SOG No.: 22
Matrix: (soil/water) SOIL Lab Sample ID: 360284
Sample lit/vol: 30.2 (g/mL) L_ Lab File ID: GH060284B15
Level: (low/med) LOW Date Received: 01 l28l90
I Moistu.re: not dee. ____u dee. Date Extracted: 07/3ll90
Date Analyzed: OBll3l90
Dilution Factor: .1~1~0~0 __
Extraction: (SepF/Cont/Sonc) ·~
GPC Cleanup: (Y/N) tL_ pH:~
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UGlKG
1
1
9
5
1
1
9
9
3
1
6
6
9
7
8
1
6
1
1
1
9
1
8
5
9
7
8
9
9
8
1
2
6
08-95-2--------Phenol
ll-44-4------~-bis(2-Chloroethyl)Ether
5-57-8---------2-Chlorophenol
41-73-1--------1,3-Dichlorobenzene
06-46-7--------1,4-Dichlorobenzene
00-51-6-----~--Benzyl Alcohol
5-50-1-----~---l,2-Dichlorobenzene
5-48~7---------2-Methylphenol
9638-32-9------bis(2-Chloroisopropyl)Ether_
06-44-5--------4-Methylphenol
21-64-7--------N-Nitroso-Di-n-Propylamine __
1-12-1---------Hexachloroethane
8-95-3---------Nitrobenzene
8-59-1---------Isophorone
8-75-5---------2-Nitrophenol
05-67-9--------2,4-Dimethylphenol
5·-85-o---------Benzoic Acid
ll-91-l--------bis(2;,.Chloroethoxy)Methane_
21)-83-2--------2, 4-Dichlorophenol
20-e2-1--------1,2,4-Trichlorobenzene
1··20-3---------Naphthalene
01;-4 7-8---'------4-Chloroani line
7••68-3---------Hexachlorobutadiene
9··50-7---------4-Chloro-3 -Methyl phenol
1••57-6---------2-Methylnaphthalene
7-·4 7-4 ---------Hexachlorocyclopentad iene __
8-06-2---------2,4,6-Trichlorophenol
5-95-4---------2,4,5-Trichlorophenol
1-58-7---------2-Chloronaphthalene
8-74-4---------2-Nitroaniline
31-11-3--------Dimethyl Phthalate
08-96-8--------Acenaphthylene
06-20-2--------2,6-Dinitrotoluene
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u u
u u u u
u u
u u u
u u u u
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u u u
u u
u u u
FORM I sv-1 1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REVS SB4-2-1MSD
Lab Coda: CQMPU Casa No.: 20937 SAS No.: SOG No.: ..,2.._2 __ I Matrix: (soil/water)-SOIL Lab Sample ID: 360284
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Sample lft/vol: 30.2 (g/mL) L-Lab File ID: GH0§0284B15
Level: (low/med) LOW Data Received: 07/28/90
\ Moisture: not dee. -1,i dee. Date Extracted: 07/31/90
Extracti.on: (SepF /Cont/Sonc) ~ Data Analyzed: 08/13/90
GPC Cleanup: (Y/N) lL_ pH:~ Dilution Factor: .i~.o~o.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (Ug/L or ug/l<g) UG/KG Q
99-09-2---------J-Nitroaniline 2000 u 83-32-9---------Acenaphthene 400 u 51-28-5---------2,4-Dinitrophenol 2000 u 100-02-7--------4-Nitrophenol 2000 u 132-64-9--------Dibenzoturan 400 u 121-14-2--------2,4-Dinitrotoluene 400 u 84-66-2---------Diethylphthalate 400 u 7005-72-3-------4-Chlorophenyl-phenylether_-_ 400 u 86-73-7---------Fluorene 400 u
100-01-6--------4-Nitroaniline 2000 u 534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 400 u
101-55-3--------4-Bromophenyl-phenylathar __ 400 u 118-74-1--------Hexachlorobenzene 400 u
87-86-5---------Pentachlorophenol 2000 u es-01-e---------Phenanthrena 400 u
120-12-1--------Anthracene 400 u 84-74-2---------Di-n-Butylphthalate 400 u
206-44-0--------Fluoranthene 400 u
129-00-0--------Pyrene 400 u
85-68-7---------Butylbenzylphthalate 400 u
91-94-1---------3,3'-Dichlorobenzidine 810 u
56-55-3---------Benzo(a)Anthracene 400 u
218-01-9--------Chrysene 400. u
11'7-81-7--------bis (2-Ethylhexyl) Phthalate_ . 400 u
11·1-e,-0--------Di-n-octyl Phthalate -400 u
20~~99-2--------Benzo(b)Fluoranthene 400 u
207-08-9--------Benzo(k)Fluoranthena 400 u
50 .. 32-e---------Benzo(a)Pyrene 400 u
19:1-39-5--------Indeno(l,2,J-cd)Pyrene 400 u
53··70-3---------Dibenzo (a, h) Anthracene 400 u
193.-24-2--------Benzo(g;h,i)Perylene 400 u
( 1) •· cannot ba separated trom Diphenylamina
FORM I sv-2 l/87 Rav.
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SAMPLE NUMBERS:
COMPUCHEM
lABORATORJES
CASE NARRATIVE CASE #20937
SDG #94 CONTRACT #(2-88)REVS
COMPUCHEM LABORA~O~IES, INC.
MW15-2S-1
MWS-4S-2
SBll-1-1
SB16-1-1
SB8-2-1
MW15-4S-1
MW9-4S-1
SBll-2-1
SB7-1-1
MW5-4S-1
SBl0-1-1
SBll-2-2
SB7-2-1
MW8-4S-l
SBl0-2-1
SB15-l-l
SB8-l-l
The samples listed above were received intact between 8-2-90
and 8-9-90 with the chain-of-custody documents in order and
all shipping containers properly sealed. Samples MW15-2S-l,
MW15-4S-l, SB7-l-l, and SB7-2-1 were received with pH values
below 5; however our DPO has instructed us to proceed with
analysis when samples are received with pH values which do
not fall within the 5 to 11 range. This narrative
summarizes the analysis of sixteen of these samples for
volatiles and semivolatiles and one for semivolatiles only.
Volatiles:
All samples were initially analyzed within holding times.
Samples MW15-2S-1, SBl0-1-1, SB7-l-l, and both the low and
medium level matrix spike duplicates required reanalyses
which could not be performed within holding times. Most
samples contained methylene chloride, acetone, and
2-butanone although benzene, toluene, ethylbenzene, and
xylenes (reported as total isomers), 4-methyl-2-pentanone,
2-hexanone, 1,1-dichloroethane, 1,2-dichloroethene (reported
as total isomers), trichloroethene, and tetrachloroethene
were also detected. Samples SB7-l-l and SB7-2-l contained
numerous tentatively identified compounds (TICs). Samples
which required both low and medium analyses in order to
maintain all target list compounds (TCLs) while reporting
all within analytical range sometimes showed disagreement
due to inhomogeneity and differences between the low level
purge and trap method and the methanol extraction procedure.
Additionally sample SB7-2-l did not meet the dilution
criteria of having at least analyte within the upper half of
the analytical range for the medium level analysis; however
the sample contained high levels of TICs and was not
reanalyzed at a lesser dilution in order to protect the
instrumentation. All sample and QC fractions met the
surrogate recovery criteria. Both the low and m~dium level
COMPUCHEM LAE,OAATORIES. INC. P.O. Box 12652 3308 Chapel Hil!/Neison Highway Research Triangle Park, NC 27709 [phone]
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lABORATORlES
matrix spike duplicates met all accuracy and prec1s1on
criteria.
Semi volatiles:
All sample and QC fractions were· extracted within holding
times. Mainly the samples contained phthalates and
polyaromatic hydrocarbons.Samples SBll-1-1, SBll-2-1, SBll-
2-2, 5B7-1-1, 5B7-2-1, and SBB-1-1 contained numerous TICs.
For sample SBB-1-1 a matrix effect which affected the
response of the fifth and sixth internal standards,
D12-chrysene and D12-perylene was confirmed by duplicate
analyses. All sample and QC fractions met the surrogate
recovery criteria; however, D5-nitrobenzene had high
recoveries for samples 5B7-1-1 and SB7-2-l. The matrix
spike duplicates met overall accuracy and precision
criteria; however, the results for pentachlorophenol were
low in both spikes, and the relative percent difference
failed.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than conditions detailed above.
Release of the data contained in the hardcopy data package
and in the computer-readable data submitted on the floppy
diskette has been authorized by the Laboratory Manager or
his designee, as verified by the following signature.
fl,. ~ ) ,idd= · k-. NL~ E ISABETH ROBINS NOWELL7./
DATE 09/10/90
TECHNICAL REVIEWER
Note: This report is paginated for reference and
accountability in decreasing numerical sequence.
Note: The "X" footnote denotes the coelution of
indistinguishable isomers.
COMPUCHEM LABORATORIES INC PO R□)( 12652 3308 Chapel Hill/Nelson Hiat1wav Researct1 Trianale Park. NC 27709 (9191549-8263
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lA EPA SAMPLE tlO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW15-2S-l
Lab Name: COMPUCHEM.RTP. Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: "'-9~4 __
Matrh:: (soil/water) SOIL Lab Sample ID: ]6]56]
Sample wt/vol: 5.0 (g/mL) _G __ Lab File ID: GH06J56JA12
Level: ( low/med) LOW Date Received: 08/09/90
% Moisture: not dee. _lQ Date Analyzed: 08/18/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-J---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-J-----·----Chloroethane 11 u
75-09-2---------Methylene Chloride 2] B
67-64-1---------Acetone 440 BE
75-15-0---------Carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0---~----l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethan~ 6 u
78-93-J~--------2-Butanone 660 BE
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
lOG61-0l-S------cis-l,J-Dichloropropen~ 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-l~-------4-Methyl-2-Pentanone lJO
591-78-6--------2-Hexanone 1 J
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------Styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
.-.. -.
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
MW15-2S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ~9~4 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. _l.Q.
Column (pack/cap) CAP
Number TICs found: _Q
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UGiKG
363563
GH06356jA12
08/09/90
08/18i90
1 0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ======·========== ============================ ======== =.:=::;;;=::.======= =====
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS MW15-2S-1DL
Lab Code: COMPU Case No.: 20937 SAS No.: ----SDG No.: ~9~4 __
Matrix: (soil/water) SOIL Lab Sample ID: 363563
Sample wt/vol: 1.0 ( g/mL) _G_ Lab File ID: GR063563Al3
Level: (low/med) LOW Date Received: 08/09/90
% Moisture: not dee. _..1Q Date Analyzed: 08/20,:'.90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG,:'.KG Q
74-87-3---------Chloromethane 56 u 74-83-9---------Bromomethane 56 u 75-01-4---------Vinyl Chloride 56 u 75-00-3---------Chloroethane 56 u 75-09-2---------Methylene Chloride 69 BD 67-64-1---------Acetone 840 BD 75-i5-o---------carbon Disulfide 28 u
75-35-4---------1,1-Dichloroethene 28 u 75-34-3---------1,1-Dichloroethane 28 u 540-59-0--------1,2-Dichloroethene (total)_ 2f u 67-66-3-------;_-Chloroform ~-u ,.
107-06-2--------1,2-Dichloroethane ' u .
78-93-3---------2-Butanone 71( BD
71-55-6---------1,1,l-Trichloroethane 28 u 56-23-5---------carbon Tetrachloride 28 u 108-05-4--------Vinyl Acetate 56 u 75-27-4---------Bromodichloromethane 28 u 78-87-5---------1,2-Dichloropropane 28 u
10061-01-5------cis-l,3-Dichloropropene 28 u
79-01-6---------Trichloroethene 28 u
124-48-1--------Dibromochloromethane 28 u
79-00-5----;_----l,l,2-Trichloroethane 28 u
71-43-2---------Benzene 28 u
10061-02-6------Trans-l,3-Dichloropropene __ 28 u
75-25-2---------Bromoform 28 u
108-10-1--------4-Methyl-2-Pentanone 61 D
591-78-6--------2-Hexanone 56 u
127-18-4--------Tetrachloroethene 28 u
79-34-5--~------l,l,2,2-Tetrachloroethane __ 28 u
108-88-3--------Toluene 28 u
108-90-7--------Chlorobenzene 28 u
100-41-4---~----Ethylbenzene 28 u
100-42~5--------styrene 28 u
1330-20-7-------Total Xylenes 28 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
.
Lab Name: COMPUCHEM.RTP contract: (2-88)-REVS
EPA SAMPLE NO.
MW15-2S-1DL
Lab Code: COMPU case No.: 20937 SAS No.: S 0G No . : .,_9.:,4 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 1.0 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. ___J,_Q
Column (pack/cap) ~~p
Number 'rICs found: ---1
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
363563
GR063563Al3
08/09/90
08/20/90
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================= ============================ ======== ============= ~====
1. LABORATORY ARTIFACT 0.75 28 J
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW15-4S-l
Lab Name: COMPUCHEM.RTP Contract: /2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ~9~4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 363564
Sample ·rt/vol: 4.0 (g/mL) _G_ Lab File ID: CR063564B14
Level: (low/med) MED Date Received: 08/09/90
t Moist11re: not dee. ---1.2. Date Analyzed: 08/19/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) J;,!G/EG Q
74-87-3---------Chloromethane 1500 u
74-83-9---------Bromomethane 1500 u
75-01-4---------Vinyl Chloride '1500 u
75-00-3-·--------Chloroethane 1500 u
75-09-2---------Methylene Chloride 770 u
67-64-1---------Acetone 9200
75-15-0---------Carbon Disulfide 770 u
75-35-4---------1.1-Dichloroethene 770 u
75-34-3---------1.1-Dichloroethane 770 u
540-59-0--------1,2-Dichloroethene (total)_ 770 u
67-66-3---------Chloroform 770 u
107-06-2--------1,2-Dichloroethane 770 u
78-93-3---------2-Butanone 4600
71-55-6---------1,1,1-Trichloroethane 770 u
56-23-5---------Carbon Tetrachloride 770 u
108-05-4--------Vinyl Acetate 1500 u
75-27-4---------Bromodichloromethane 770 u
78-87-5---------1,2-Dichloropropane 770 u
10061-01-5------cis-l,3-Dichloropropene 770 u
79-01-6---------Trichloroethene 770 u
1:2 4-4 8-1--------Dibromochloromethane 770 u
79-00-5--~------l,l,2-Trichloroethane . 770 u
71-43-2---------Benzene 770 u
10061-02-6------Trans-l,3-Dichloropropene __ 770 u
75-25-2---------Bromoform 770 u
108-10-1--------4-Methyl-2-Pentanone 940 J
591-78-6--------2-Hexanone 1500 u
127-18-4--------Tetrachloroethene 770 u
7St-34-5---------l,l,2,2-Tetrachloroethane __ 770 u
108-88-3--------Toluene 770 u
108-90-7--------Chlorobenzene 770 u
100-41-4--------Ethylbenzene 770 u
100-42-5--------styrene 770 u
1330-20-7-------Total Xylenes 770 u
FORM I VOA 1/87 Rev.
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW15-4S-l
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: L9~4 __
Matrix: (soil/water) SOIL
Sample 1-'t/vol: 4.0
Level: (low/med) MED
% Moisti1re: not dee. ___li
Column (pack/cap) !:M'.
Number TI Cs found: _...Q
CAS NUMBER
(g/mL) _G_
COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
363564
CR063564B14
08/09/90
08/19/90
l. o
RT EST. CONC. Q ================ ============================ ======== ============= =====
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
MW5-4S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : .,c9.:,;4 __
Matrix: (soil/water) SOIL Lab Sample ID: 361457
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GR061457Cl3
Level: (low/med) LOW Date Received: 08/02/90
% Moisture: not dee. --1.!!. Date Analyzed: 08/12/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!,/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride 55 B 67-64-1---------Acetone 140 B
75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-Dichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3---------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u 78-93-3---------2-Butanone 4 BJ
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--~-~---Vinyl Acetate 12 u 75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1----~---4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 6 u
I
108-88-J----~---Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
EPA SAMPLE tlO,
MW5-4S-l
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No. : _9_4 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 ( g/rnL) _G_
Level: (low/med) LOW
% Moisture: not dee. _ll
Column (pack/cap) Cb,P
Number TICs found: -1
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
361457
GR061457Cl3
08/02/90
08/12/90
l. o
RT EST. CONC. Q ----.-·----------==========================-= ======== ============= ===== 1. LAB. ARTIFACT 0.75 7. 3 J
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW8-4S-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,_9..:,4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362491
Sample ••t/vol: 5.0 (g/mL) _G __ Lab File ID: GH062491Al3
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. __ll Date Analyzed: 08/14/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 14 u
74-83-9---------Bromomethane 14 u
75-01-4---------Vinyl Chloride 14 u 75-00-3---------Chloroethane 14 u 75-09-2---------Methylene Chloride 19 B
67-64-1---------Acetone 110 B
75-15-o-----·---carbon Disulfide 7 u
75-35-4---------1,1-Dichloroethene 7 u
75-34-3---------1,1-Dichloroethane 7 u
540-59-0--------1,2-Dichloroethene (total)_ 7 u 67-66-3---------Chloroform 7 u
107-06-2--------1,2-Dichloroethane 7 u
78-93-3---------2-Butanone 9 BJ
71-55-6---------1,1,1-Trichloroethane 7 u
56-23-5---------carbon Tetrachloride 7 u
108-05-4--------Vinyl Acetate 14 u
75-27-4---------Bromodichloromethane 7 u
78-87-5---------1,2-Dichloropropane 7 u
10061-01-5------cis-l,3-Dichlorcpropene 7 u
79-01-6---------Trichloroethene 7 u
124-48-1--------Dibromochloromethane 7 u
79-oo-s---------1,1,2-Trichloroethane 7 u
71-43-2---------Benzene 7 u
10061-02-6------Trans-l,3-Dichloropropene __ 7 u
75-25-2---------Bromoform 7 u
108-10-1--------4-Methyl-2-Pentanone 14 . u
591-78-6--------2-Hexanone 14 u
127-18-4--------Tetrachloroethene 7 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 7 u
108-88-3--------Toluene 7 u
108-90-7--------Chlorobenzene 7 u
100-41-4--------Ethylbenzene 7 u
100-42-5--------styrene 7 u
1330-20-7-------Total Xylenes 7 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
MW8-4S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ~9~4 __
Matrix: (soil/water) SOIL Lab Sample ID: 362491
Sample ·wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062491A'l3
Level: ( low/med) LOW
\ Moisture: not dee. ---1..§.
Column (pack/cap) CAP
Number TICs found: __Q
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
08/04/90
08/14/90
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q =====
•
FORM I VOA-TIC 1/87 Rev.
-.. -.. -. --.-. .-.-. ~" r-. 1 ~ r"•. ,-, 'T ,-, ,-I J ,._,. ►,_.,-,I, I I
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW8-4S-2
Lab Name: COMPUCHEM.R'rP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 : SAS No.: SDG No. : -"-9.:,;4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362492
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062492B13
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ----2..§. Date Analyzed: 08/14/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 14 u
74-83-9---------Bromomethane 14 u
75-01-4---------Vinyl Chloride 14 u
75-00-3---------Chloroethane 14 u
75-09-2---------Methylene Chloride 24 B
67-64-1---------Acetone 48 B
75-15-0---------Carbon Disulfide 7 u
75-35-4---------1,1-Dichloroethene 7 u
75-34-3---------1,1-Dichloroethane 7 u
540-59-0---~----l,2-Dichloroethene (total)_ 7 u
67-66-3---------Chloroform 7 u
107-06-2--------1 2-Dichloroethane 7 u I
' , .
78-93-3-~-------2-Butanone 1 BJ
71-55-6-----~---l,l,l-Trichloroethane 7 u
56-23-5---------Carbon Tetrachloride 7 u
108-05-4--------Vinyl Acetate 14 u
75-27-4---------Bromodichloromethane · 7 u
78-87-5---------1,2-Dichloropropane 7 u
10061-01-5----~-cis-l,3-Dichloropropene 7 u
79-01-6---------Trichloroethene 7 u
124-48-1--------Dibromochloromethane 7 u
79-00-5---------1,1,2-Trichloroethane 7 u
71-43-2---------Benzene 7 u
10061-02-6------Trans-l,3-Dichloropropene __ 7 u
75-25-2---------Bromoform 7 u
108-10-1-~------4-Methyl-2-Pentanone 14 u
591-78-6--------2-Hexanone 14 u
127-18-4--------Tetrachloroethene 7 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 7 u
108-88-3--------Toluene 7 u
108-90-7--------Chlorobenzene 7 u
100-41-4--------Ethylbenzene 7 u
100-42-5--------Styrene 7 u
1330-20-7-------Total Xylenes 7 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Na.me: COMPUCHEM. RTP Contract: 12-88}-REVS
EPA SAMPLE NO.
MW8-4S-2
Lab .. code: COMPU Case No.: 20937 SAS No.: SDG No.: ,,_9.c,.4 __
Matrix: (soil/water) SOIL Lab sample ID: 362492
Sample wt/vol: 5.0 (g/mL) _G __ Lab File ID: GH062492Bl3
Level: ( low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ---1..§. Date Analyzed: 08/14/90
Column (pack/cap) CAP Dilution Factor: 1.0
Number TICs found: ---2. CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
=====:=========== ============================ ======== ====::;;=====:::== =====
1. LABORATORY ARTIFACT 0.37 220 J 2. 110-54-3 HEXANE 3.10 28 J
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-4S-l
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: =9~4 __
Matrix:: ( soil/water) SOIL Lab Sample ID: 363241
sample wt/vol: 5.0 ( g/rnL) _G __ Lab. File ID: GH063241Al3
Level: (low/med) LOW Date Received: 08/08/90
% Moisture: not dee. _lQ Date Analyzed: 08/17/90
Column: (pack/cap) CAP Dilution Factor: LO
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chlorornethane 14 u
74-83-9---------Bromomethane 14 u
75-01-4---------Vinyl Chloride 14 u
75-00-3---------Chloroethane 14 u
75-09-2---------Methylene Chloride 52 B
67-64-1---------Acetone 36 B·
75-15-0---------carbon Disulfide 7 u
75-35-4---------1,1-Dichloroethene 7 u
75-34-3------~--1,1-oichloroethane 7 u
540-59-0--------1,2-Dichloroethene (total)_ 7 u
67-66-3---------Chloroform 7 u
107-06-2--------1,2-Dichloroethane 7 u
78-93-3---------2-Butanone 2 BJ
71-55-6---------1,1,l-Trichloroethane 7 u
56-23-5~--------Carbon Tetrachloride 7 u
108-05-4--------Vinyl Acetate 14 u
75-27-4---------Brornodichloromethane 7 u
78-87-5---------1,2-Dichloropropane 7 u
10061-01-5------cis-l,3-Dichloroprop~ne 7 u
79-01-6---------Trichloroethene 7 u
124-48-1--------Dibrornochloromethane 7 u
79-00-5----~----l,l,2-Trichloroethane 7 u
71-43-2---------Benzene 7-u
10061-02-6------Trans-l,3-Dichloropropene __ 7 u
75-25-2---------Brornoform 7 u
108-10-1--------4-Methyl-2-Pentanone 14 u
591-78-6--------2-Hexanone 14 u
127-18-4----~---Tetrachloroethene 7 u
79-34-5---------1 1 2 2-Tetrachloroethane .. ' --7 u
108-88-3--------Toluene 7 u
108-90-7--------Chlorobenzene 7 u
100-41-4--------Ethylbenzene 7 u
100-42-5--------styrene 7 u
1330-20-7-------Total Xylenes 7 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED .COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM. RTP Contract: (2-881-REVS
MW9-4S-l
Lab Co,ie : COMPU case No.: 20937 SAS No.: S DG No. : _,,_9.:.4 __
Lab Sample ID: ~3~6~3~2~4~1~---Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. _lQ
Column (pack/cap) CAP
Number TICs found: ___J,
(g/mL) Q__ Lab File ID: GH063241Al3
Date Received: 08/08/90
Date Analyzed: 08/17/90
Dilution Factor: ~l~-~o'----
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
================ ==========================-= ======== ============= =====
1. LABORATORY ARTIFACT 0.40 73 BJ
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SBl0-1-1
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: ~9~4 __
Matrix: ( soil/water) SOIL Lab Sample ID: )62485
Sample wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GH062485Al2
Level: (low/med) LOW Date Received: 08/04/90
\ Moisture: not dee. ----1.§. Date Analyzed: 08/1)/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2----~----Methylene Chloride 15 B
67-64-1---------Acetone 1200 BE
75-15-0---------carbon Disulfide. 6 u
75-JS-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chlorofonn 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 8 J
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------Carbon Tetrachloride 6 u
108-05~4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,J-Dichloropropene __ 6 u
75-25-2---------Bromofonn 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u -
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane ' ' ' --6 u
108-88-J--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------Styrene 6 u
lJJ0-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SBl0-1-1
Lab Name: COMPUCHEM.R~P Contract: 12-88)-REVS
Lab Code : COMPU Case No.: 20937 SAS No.: SDG No. : .,_9.:,:4 __
Matrix: (soil/water) SOIL Lab Sample ID: 362485
sample wt/vol: 5.0 (g/mL) _G __ Lab File ID: GH062485Al2
Level: ( low/med) LOW
t Moisture: not dee. ___J,_§.
Column (pack/cap) CAP
Number TICs found: ---2.
CAS NUMBER COMPOUND NAME
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
08/04/90
08/13/90
1.0
RT EST. CONC. Q =====------===== =========================== ======== ============= =====
1. LAB. ARTIFACT 0.53 6.0 J
2. 67-63-0 2-PROPANOL l. 85 290 J
FORM I VOA-TIC 1/87 Rev.
j ·=·'
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBl0-1-lRE
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Cod.e: COMPU Case No.: 20937 SAS No.: SDG No.: .a.9.:,;4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362485
Sample wt/vol: 4.0 (g/mL) _G __ Lab File ID: C2R62485B10
Level: (low/med) MED Date Received: 08/04/90
% Moisture: not dee. _li Date Analyzed: 08/15/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !,!G/!',G Q
'
74-87-3---------Chloromethane 1500 u
74-83-9---------Bromomethane 1500 u
75-01-4---------Vinyl Chloride 1500 u
75-00-3-7-------Chloroethane 1500 u
75-09-2---------Methylene Chloride 740 u
67-64-1---------Acetone 3500 BO
75-15-0---------Carbon Disulfide 740 u
75-35-4---------1,l-Dichloroethene 740 u
75-34-3---------1,l-Dichloroethane 740 u
540-59-0--------1,2-Dichloroethene (total)_ 740 u
67-66-3---------Chloroform 740 u
107-06-2--------1,2-Dichloroethane 740 u
78-93-3---------2-Butanone 1500 u
71-55-6---------1,l,l-Trichloroethane 740 u
56-23-5---------carbon Tetrachloride 740 u
108-05-4--------Vinyl Acetate 1500 u
75-27-4---------Bromodichloromethane 740 u
78-87-5---------1,2-Dichloropropane 740 u
10061-01-5------cis-l,3-Dichloropropene 740 lJ
79-01-6---------Trichloroethene 740 u
124-48-1--------Dibromochloromethane 740 u
79-00-5---------1,1,2-Trichloroethane 740 u
71-43-2---------Benzene 740 u
10061-02-6------Trans-l,3-Dichloropropene __ 740 u
75-25-2---------Bromoform 740 u
108-10-1--------4-Methyl-2-Pentanone 1500 u
591-78-6--------2-Hexanone 1500 u
127-18-4--------Tetrachloroethene 740 u
. 79-34-5---------1,1,2,2-Tetrachloroethane __ · 740 u
108-88-3--------Toluene 740 u
108-90-7--------Chlorobenzene 740 u
100-41-4--------Ethylbenzene 740 u
100-42~5--------Styrene 740 u
1330-20-7-------Total Xylenes 740 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
SBl0-1-lRE
Lab Code: COMPU Case No.: 20937 SAS No.: S DG No . : .._9.:,4 __
Matrix: ( soil/water) SOIL
Sample wt/vol: 4.0 (g/mL) _G_
Level: ( low/med) MED
% Moisture: not dee. -1§_
Column (pack/cap) C~P
Number 'l'ICs found: __ o
CAS NUMBER
·Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
362485
C2R62485B10
08/04/90
08/15/90
1.0.
================ COMPOUND NAME · 1 RT ========== ==============·== ======== EST. CONC.
=============
Q
=====
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
. EPA SAMPLE NO.
SBl0-2-1
Lab Narne: COMPUCHEM.R'!'P Contract: 12-88}-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No. : 29..:,4 __
Matrix: (soil/water) SOIL Lab Sample ID: 362486
Sample wt/vol: 2.0 ( g/rnL) _G_ Lab File ID: GR062486B13
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _l.Q Date Analyzed: 08/14/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
C:AS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 28 u 74-83-9---------Bromomethane 28 u 75-01-4---------Vinyl Chloride 28 u
75-00-3---------Chloroethane 28 u
75-09-2---------Methylene Chloride 240 B
67-64-1---------Acetone 340 B
75-15-0----~----carbon Disulfide 14 u
75-35-4---------1,1-Dichloroethene 14 u
75-34-3---------1,1-Dichloroethane 14 u
540-59-0--------1,2-Dichloroethene (total)_ 14 u
67-66-3---------Chloroform 14 u
107-06-2--------1,2-Dichloroethane 14 u
78-93-3---------2-Butanone 10 BJ
71-55-6---------1,1,1-Trichloroethane 14 u
56-23-5---------carbon Tetrachloride 14 u
108-05-4--------Vinyl Acetate 28 u
75-27-4---------Bromodichloromethane 14 u
78-87-5---------1,2-Dichloropropane 14 u
10061-01-5------cis-l,3-Dichloropropene 14 u
79-01-6---------Trichloroethene 14 u
124-48-1--------Dibromochloromethane 14 u
79-oo-s---------1,1,2-Trichloroethane 14 u
71-43-2---------Benzene 14 u
10061-02-6------Trans-l,3-Dichloropropene __ 14 u
75··25-2---------Bromoform 14 u
108-10-1--------4-Methyl-2-Pentanone 28 u
591-78-6--------2-Hexanone 28 u
127-18-4--------Tetrachloroethene 14 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 14 u
108-88-3--------Toluene 14 u
108-90-7--------Chlorobenzene 14 u
100-41-4--------Ethylbenzene 14 u
100-42-5--------Styrene 14 u
1330-20-7-------Total Xylenes 14 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
EPA SAMPLE r;o.
SBl0-2-1
Lab Code: COMPU case No.: 20937 SAS No.: ____ SDG No.: ,,_9.:,:4 __
Matrix: (soil/water) SOIL
Sample wt/vol: 2.0
Level: ( low/med) LOW
% Moisture: not dee. ___lQ
Column (pack/cap) CAP
Number TICs found: --1
(g/mL) _G_
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
362486
GR062486Bl3
08/04/90
08/14/90
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
1. LABORATORY ARTIFACT 0.75 17 J
. \
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE t/0.
VOLATILE ORGANICS ANALYSIS DATA SHEET
SBU-1-1
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _,,_9.:,:4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362487
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062487Al2
Level: ( low/med) LOW Date Received: 08/04/90
% Moistu.re: not dee. ____ll Date Analyzed: 08/13/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CA.S NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
7!;-01-4---------Vinyl Chloride 12 u
7!;-oo-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 14 8
67-64-1---------Acetone 71 8
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 27
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
103-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5----~-cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
12~-48-1--------Dibromochloromethane · 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1-~------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane , , , --6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 1 J
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 3 J
•
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Na!De: COMPUCHE.M. R'rP Con tr.act: I 2-88 l -REVS
EPA SAMPLE NO.
SBll-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : .,.9.:,4 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 ( g/rnL) _G_
Level: (low/med) r.pw
% Moisture: not dee. _il_
Column (pack/cap) CAP
Number 'rICs found: ........l
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug(L or ug/Kg) UG/KG
362487
GH062487A12
08/04/90
08/13/90
LO
CAS I/UMBER COMPOUND NAME RT EST. CONC. Q
======~:========= ============================ ======== ============= =====
1. LAB. ARTIFACT 0.57 4.9 J
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.R'rP Contract: 12-881-REVS
SBll-2-1
Lab Code: COMPU Case No.: 20937· SAS No.: SDG No. : 29..:,4.....:.__
Matrix: ( soil/water) SOIL Lab Sample ID: 362488
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062488Bl2
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _ll Date Analyzed: 08/13/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg)
74-87-3---------Chloromethane _______ _
74-83-9---------Bromomethane ____ ~----
75-0l-4---------Vinyl Chloride ___ ~----
75-00-3---------Chloroethane~~-------75-09-2---------Methylene Chloride _____ _
67-64-1---------Acetone 7 5-.15-o---------carbon ·-D""'i_s_u""'l"""'f'"'i""'d'""e ______ _
75-35-4---------l,l-Dichloroethene._~----
75-34-3---------1,l-Dichloroethane. _____ _
540-59-0--------1,2-Dichloroethene (total) __
67-66-3---------Chloroform. __ ~-------
107-06-2--------l,2-Dichloroethane _____ _
78-93-3-----.----2-Butanone. _________ _
71-55-6---------1,1,1-Trichloroethane. ___ _
56-23-5---------carbon Tetrachloride. ____ _
108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloro_m_e~t~h_a_n_e ____ _
78-87-5---------1,2-Dichloropropane. ______ 1 10061-01-5------cis-l,3-Dichloropropene __ _
79-01-6---------Trichloroethene ______ _
124-48-1--------Dibromochloromethane ____ _
79-00-5---~-----l,l,2-Trichloroethane ___ _
71-43-2------·---Benzene __________ _
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform. _________ _
1oa-10-1--------4-Methyl-2-Pentanone ____ _
591-78-6--------2-Hexanone 127-18-4--~~----Tetrachlor_o_e~t~h_e_n_e _____ _
79-34-5---------1,1,2,2-Tetrachloroethane __
l.08-88-3--------Toluene __________ _
108-90-7--------Chlorobenzene _______ _
100-41-4--------Ethylbenzene ________ _
100-42-5--------styrene __________ _
1330-20-7-------Total Xylenes. ___ ~----
FORM I VOA
!,!G/KG
12 u
12 u
12 u
12 u
20 B
56 B
6 u
6 u
6 u
6 u
6 u
6 u
8 J
6 u
6 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
12 u
12 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP
Lab Code: COMPU Case No.: 20937
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dee. _ll
Column (pack/cap) CAP
Number TICs found: ___l
SBll-2-1
Contract: 12-881-REVS
_G __
SAS No.: SDG No.: "-9..:,:4 __
Lab Sample I D : ,.3cs6ce2c04cs8'-'8'------
Lab File ID: GH062488812
Date Received: 08/04/90
Date Analyzed: 08/13/90
Dilution Factor: 1.0 =~--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
=====:=========== ============================ ======== ============= =====
1. LAB. ARTIFACT 0.57 4.9 J
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
SBll-2-2
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ~9~4 __
Matrix: (soil/water) SOIL Lab Sample ID: 362489
Sample wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GH062489Cl3
Level: ( low/med) LOW Date Received: 08/04/90
% Moist.ure: not dee. ---1.§ Date Analyzed: 08/14/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q •
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 .u
75-01-4~--------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2---------Methylene Chloride 20 B
67-64-1---------Acetone 47 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------l,l-Dichloroethene 6 u
75-34-3---------l,l-Dichloroethane 6 u
540~59-0--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 9 BJ
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79~01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6-~----Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------Styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
1 -. ..
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
SBll-2-2
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,,_9.:i4 __
Lab Sample ID: ~3~62~4~8~9'-----Matrix: ( sciil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
% Moisture: not dee. _li
Column (pack/cap) CAP
Number TICs found:~
(g/mL) _G_ Lab File ID: GH062489Cl3
Date Received: 08/04/90
Date Analyzed: 08/14/90
Dilution Factor: ~l~-~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
1. LABO RA TORY ART! FACT O . 4 0 3 6 J
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
SB16-l-l
Lab Name: COMPUCHEM.RtP Contract: {2-88)-REVS
Lab Cc,de: COMPU Case No.: 20937 SAS No.: SDG No. : ~9~4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362481
SamplE! wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062481Al2
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _l.Q Date Analyzed: 08/13/90
Column: (pack/cap) CAP Dilution· Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 11 u
74-83-9---------Bromomethane 11 u
75-01-4---------Vinyl Chloride 11 u
75-00-3---------Chloroethane . 11 u
75-09-2---------Methylene Chloride 37 B
67-64-1---------Acetone 53 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 l!
78-93-3-------~-2-Butanone 6 J
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 11 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u·
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-1,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
-108-10-1--------4-Methyl-2-Pentanone 11 u
591-78-6--------2-Hexanone 11 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane 6 u . ' ' ' --. 6 u 108-88-3--------Toluene
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes· ·6 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.R'rP Contract: /2-88)-REVS
EPA SAMPLE NO.
SB16-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94 ~--
Matrix: ( soil/water) SOIL Lab sample ID: 362481
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062481Al2
Level: (low/med) rpw
% Moisture: not dee. _l.Q
Column (pack/cap) CAP
Number TICS found: __l
CAS NUMBER COMPOUND NAME
Date Received:
Date· Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGi'.KG
081'.041'.90
081'.131'.90
1.0
RT EST. CONC. Q ======·========== =============-============== ======== ==-========== =====
1. LAB. ARTIFACT 0.57 5.6 J
FORM I VOA-TIC 1/87 Rev.
20937 94 SAr1F·iE DATA 5l1MrlARI'
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAJ1PLE NO.
. SB7-l-l
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
I Lab code: COMPU Case No.: 20937 .SAS No.: ----SDG No.: ~9~4 __
Matrix: (soil/water) SOIL Lab S amp 1 e ID: ~J~6~2~4~8~J~---
Sample wt/vol: 5.0 {g/mL) _G __ Lab File ID: GH06248JA1J
Level: ( low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _2.Q Date Analyzed: 08/14/90
Column: (pack/cap) Cl',P Dilution Factor: 1.0 =~--
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u 74-83-9---------Bromomethane 12 u 75-01-4---------Vinyl Chloride 12 u 75-00-3---------Chloroethane 12 u 75-09-2---------Methylene Chloride 31 B 67-64-1---------Acetpne 1900 BE 75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 23 67-66-3---------Chloroform 6 u
107-06-2-~------l,2-Dichloroethane 6 u 78-93-3---------2-Butanone 6 BJ
71-55-6---------1,1,l-Trichloroethane 6 u 56-23-5---------Carbon Tetrachloride 6 u 108-05-4--------Vinyl Acetate 12 u 75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u 10061-01-5------cis-l,J-Dichloropropene 6 u
79-01-6---------Trichloroethene 5 J 124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u 7:l-43-2---------Benzene 1 J
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6-------~2-Hexanone 12 u 127-18-4--------Tetrachloroethene 54
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 170
108-90-7-------~Chlorobenzene 6 u
100-41-4--------Ethylbenzene 60 100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes JOO E
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SB7-l-l Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,_9c,4 __
Matrix: (soil/water) SOIL Lab Sample ID: .,3"'6"'2..:,4_,,8_,;_3 ___ _
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062483Al3
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ---2.Q Date Analyzed: 08/14/90
Column (pack/cap) CAP Dilution Factor: ~l~."'o __ _
Number 'rics found: ·--1.Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS IIUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== ============= ===== 1. ll.l-84-2 NONANE 11.05 41 J 2. UNKNOWN CYCLIC HYDROCARBON 11.90 72 J 3. ETHYLMETHYLBENZENE 12.07 41 J
4. UNKNOWN 12.79 64 J
5. UNKNOWN 12.99 190 J 6. TRIMETHYLBENZENE 13.14 120 J 7. ETHYLMETHYLBENZENE 13.40 240 J 8. UNKNOWN 13.74 390 J
9. ETHYLMETHYLBENZENE 14.40 300 J 10. UNKNOWN SUBST. BENZENE 14.67 68 J
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMPLE [~TR SUMMARY 1 74
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
SB7-l-1RE
Lab Code: COHPU Case No.: 20937 SAS No.: SDG No.: ,:9..:,4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362483
sample wt/vol: 4.0 (g/rnL) ~ Lab File ID: CR062483B10
Level: (low/med) MED Date Received: 08/04/90
% Moisture: not dee. ~ Date Analyzed: 08/15/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/!';G Q
74-87-3---------Chloromethane 1600 u 74-83-9---------Bromomethane 1600 u 75-01-4---------Vinyl Chloride 1600 u 75-00-3---------Chloroethane 1600 u
75-09-2---------Methylene Chloride 420 BDJ 67-64-1---------Acetone 3100 BO
75-15-o---------carbon Disulfide 780 u 75-35-4---------1,1-Dichloroethene 780 u 75-34-3-~-------l,l-Dichloroethane 780 u
540-59-0--------1,2-Dichloroethene (total)_ 780 u 67-66-3----7----Chloroform 780 u
107-06-2--------1,2-Dichloroethane 780 u
78-93-3---------2-Butanone 1600 u
71-55-67--------1,1,1-Trichloroethane 780 u 56-23-5---------carbon Tetrachloride 780 u 108-05-4--------Vinyl Acetate 1600 u
75-27-4---------Bromodichloromethane 780 u
78-87-5---------1,2-Dichloropropane 780 u
10061-01-5------cis-l,3-Dichloroproperie 780 u
79-01-6---------Trichloroethene 780 u
124-48-1--------Dibromochloromethane 780 u
79-00-5---------1;1,2-Trichloroethane 780 u
71-43-2---------Benzene 780 u
10061-02-6------Trans-l,3-Dichloropropene __ 780 u
75-25-2---------Bromoform 780 u
108-10-1--------4-Methyl-2-Pentanone 1600 u
591-78-6~-------2-He~anone 1600 u
127-18-4--------Tetrachloroethene 300 DJ
79-34-5---------1,1,2,2-Tetrachloroethane __ 780 u 108-88-3--------Toluene 1900 D
108-90-7--------Chlorobenzene 780 u
100-41-4--------Ethylbenzene 380 DJ
100-42-5--------styrene 780 u
1330-20-7-------Total Xylenes 1800 D
-
FORM I VOA 1/87 Rev.
20937 94 SAMPLE r~TA SUMMARY 1 ;:-:
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TENTATIVELY IDENTIFIED COMPOUNDS
SB7-l-1RE
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No. : SDG No. : .,__9.,_4 __
Matrix:: (soil/water) SOIL Lab Sample ID: _,,_3-"'6.,,_224,,._83"-------
Sample wt/vol: 4.0 (g/mL) _G_ Lab File ID: CR062483Bl0
Level: ( low/med) MED Date Received: 08/04/90
% Moisture: not dee. _IQ Date Analyzed: 08/15/90
Column (pack/cap) ciP Dilution Factor: ~1.,_.o,,_ __
Number TICs found: ....lQ
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== ====::;::======== ===== 1. TRIMETHYLCYCLOHEXANE 41.42 2700 J
2. UNKNOWN 48.44 3400 J 3. UNKNOWN CYCLIC HYDROCARBON 52.16 8100 J
4. UNKNOWN 54.29 3700 J 5. UNKNOWN HYDROCARBON 55.01 2200 J
6. UNKNOWN 55.98 2500 J 7. ETHYLMETHYLBENZENE 56.88 3900 J 8. TRIMETHYLBENZENE 57.44 8100 J 9. DECANE+UNKNOWN 58.81 19000 J
10. UNKNOWN SUBST. BENZENE 60.15 1,000 J
'
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMPLE [~TA SUMMARY 1 ?::
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
SB7-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: ----SDG No.: .,_9.:,:4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362484
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH062484B12
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ___u Date Analyzed: 08/13/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) l,!G/jSG Q
74-87-3---------Chloromethane 13 u
74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 19 B
67-64-1---------Acetone 520 BE
75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1 1-Dichloroethane . . , 4 J
540-59-0--------1,2-Dichloroethene (total)_ 51
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 43
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 49
124-48-1--------Dibromochloromethane 6 u
79-00-5---------l,l,2-Trichloroethane 6 u
71-43-2---------Benzene 2 J
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
7 i;-2 5-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 180
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 690 E
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 170
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 140
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 370 E
FORM I VOA 1/87 Rev.
SAMPLE· [~TA SUMMAR\) 1 7;
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Nan1e: COMPUCHEM. RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
S87-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ~94..,___
Matrix: (soil/water) SOIL
sample wt/:vol: 5.0 (g/mL)
Level: ( low/med) LOW
t Moisture: not dee. ___ll
Column (pack/cap) CAP
Number 1'ICs found: ....lQ
CAS NUMBER COMPOUND
i;;___
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
362484
GH062484B12
08/04/90
08/13/90
1.0
CONC. Q ===-----======== ============================ ======== =============== =====
1. UNKNOWN 6.23 330 J.
2. 111-84-2 NONANE 7.27 540 J
3. UNKNOWN HYDROCARBON' 7.80 880 J
4. UNKNOWN HYDROCARBON 7.82 280 J
5. UNKNOWN 7.93 230 J
6. UNKNOWN 8.25 1500 J
7. UNKNOWN 8.40 420 J
8. ETHYLMETHYLBENZENE 8.54 330 J
9. TRIMETHYLBENZENE + UNKNOWN 8.64 1300 J
10. DECANE + UNKNOWN 8.82 2100 J
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMPLE f~TA SUMMARY
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB7-2-1DL
Lab Name: COMPUCHEM~RTP Contract: (2-88}-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : .._9c,.4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 362484
Sample wt/vol: 4.0 (g/mL) ~ Lab File ID: C3R62484Cl4
Level: (low/med) MED Date Received: 08/04/90
t Moisture: not dee • .......ll ,Date Analyzed: 08/20/90
CollllllI1: (pack/cap> CAP Dilution Factor: 4.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !,11,/jSG Q
74-87-3---------Chloromethane 64,00 u
74-83-9---------Bromomethane 6400 u
75-01-4---------Vinyl Chloride 6400 u·
75-00-3---------Chloroethane 6400 u
75-09-2---------Methylene Chloride 900 DJ
67-64-1---------Acetone 6100 DJ
75-15-0---------carbon Disulfide 3200 u
75-35-4-~-------l,l-Dichloroethene 3200 u
75-34-3---------1,1-Dichloroethane 3200 u
540-59-0--------1,2-Dichloroethene (total)_ 3200 u
67-66-3---------Chloroform 3200 u
107-06-2--------1,2-Dichloroethane 3200 u
78-93-3---------2-Butanone 6400 u
71-55-6---------1,1,l-Trichloroethane 3200 u
56-23-5---------carbon Tetrachloride 3200 u
108-05-4--------Vinyl Acetate 6400 u
75-27-4---------Bromodichloromethane 3200 u
78-87-5---------1,2-Dichloropropane 3200 u
10061-01-5------cis-l,3-Dichloropropene 3200 u
79-01-6---------Trichloroethene 3200 u
124-48-1--------Dibromochloromethane 3200 u
79-00-5---------1,1,2-Trichloroethane 3200 u
71-43-2---------Benzene 3200 u
10061-02-6-.-----Trans-l, 3-Dichloropropene __ 3200 u
75-25-2---------Bromoform 3200 u
108-10-1--------4-Methyl-2-Pentanone 6400 u
591-78-6--------2-Hexanone 6400 u
127-18-4--------Tetrachloroethene 31000 D
79-34-5---------1 1 2 2-Tetrachloroethane , , , --3200 u
108-88-3--------Toluene 2100 DJ
108-90-7--------Chlorobenzene 3200 u
100-41-4--------Ethylbenzene 3000 DJ
100-42-5--------styrene 3200 u
1330-20-7-------Total Xylenes 15000 D
FORM I VOA 1/87 Rev.
20937 94 SAMPLE rqrA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SB7-2-1DL
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: z.91.4 __
Matrh:: (soil/water) SOIL Lab Sample ID: 362484
Sample wt/vol: 4.0 (g/mL) Y...._ Lab File ID: C3R62484C14
Level: (low/med) MED Date Received: 08/04/90
' Moisture: not dee. ____ll Date Analyzed: 08/20/90
Column (pack/cap) Cl',P Dilution Factor: 4.0
Number TICs found: ....l..Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ~=============== ========================= ======= ===========:::= ===== 1. ETHYLMETHYLCYCLOHEXANE 10.40 37000 J 2. l.11-.84-2 NONANE 10.75 57000 J 3. l.678-92-8 CYCLOHEXANE,PROPYL-11.50 31000' J 4. UNKNOWN HYDROCARBON 11.62 37000 J 5. UNKNOWN 12.15 130000 J 6. UNKNOWN 12;57 83000 J 7. ETHYLMETHYLBENZENE 12.80 100000 ~ u 8. TRIMETHYLBENZENE + UNKNOWN 12.92 160000 J 9. DECANE + UNKNOWN 13.24 180000 J 10. TRIMETHYLBENZENE 13.57 90000 J
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMPLE f lTA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE t!O.
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
SBB-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ~9-"'4 __
Matrix: (soil/water) SOIL Lab Sample ID: 361455
Sample wt/vol: 5.0 ( g/mL) _G_ Lab File ID: GR061455819
Level: ( low/med) LOW Date Received: 08/02/90
% Moisture: not dee. ----2.Q Date Analyzed: o·a111190
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u.
75·-09-2-----'----Methylene Chloride 7 B
67-64-1---------Acetone 15 B
75-15-0---------Carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6. u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 4 BJ
31-55-6-------~-l,l,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5----~-cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane , '' --6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
20937 94 SAMPLE DlTA SUMMARY 1 6 c
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VOLATILE ORGANICS ANALYSIS DATA SHEET --
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
EPA SAMPLE NO.
SB8-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ~9~4 __
Matrix: (soil/water) SOIL Lab Sample ID: 361455
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GR061455B19
Level: (low/med) LOW
% Moisture: not dee. __l_Q
Column (pack/cap) CAP
Number TICs found: __Q
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
08/02/90
08/11/90
1.0
Q CAS NUMBER COMPOUND NAME I RT EST. CONC. =======,========= ========================= .== ======== ============= =====
I
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMP4E DQTA SUMMARY
l
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lA EPA_ SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SBS-2-1 Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 · SAS No.: SDG No. : ~9~4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 361456
Sample wt/vol: 5.0 (g/mL) _G __ Lab File ID: GH061456ClJ
Level: (low/med) LOW Date Received: 08/02/90
% Moisture: not dee. _ll Date Analyzed: 08/ 11/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG,:'.KG Q
74-87-3---------Chloromethane 15 u 74~83-9---------Bromomethane 15 u 75-01-4---------Vinyl Chloride 15 u 75-00-3---------Chloroethane 15 u 75-09-2---------Methylene Chloride 22 B 67-64-1---------Acetone 57 B 75-15-0------~--carbon Disulfide 7 u 75-35-4---------1,1-Dichloroethene 7 u 75-34-3---------1,1-Dichloroethane 7 u 540-59-0--------1,2-Dichloroethene (total)_ 7 u 67-66-3---------Chloroform 7 u 107-06-2--------1,2-Dichloroethane 7 u 78-93-3---------2-Butanone 3 BJ 71-55-6---------1,1,1-Trichloroethane 7 u 56-23-5---------carbon Tetrachloride 7 u 108-05-4--------Vinyl Acetate 15 u 75-27-4---------Bromodichloromethane 7 u 78-87-5---------1,2-Dichloropropane 7 u 10061-01-5------cis-1,3-Dichloropropene 7 u 79-01-6---------Trichloroethene 7 u 124-48-1----"".---Dibromochloromethane 7 u 79-oo-s---------1,1,2-Trichloroethane 7 u 71-43-2---------Benzene 7 u 10061-02-6------Trans-l,3-Dichloropropene __ 7 u 75-25-2---------Bromoform .. 7 u 108-10-1--------4-Methyl-2-Pentanone 15 u 591-78-6--------2-Heianone 15 u 127-18-4--------Tetrachloroethene 7 u 79-34-5---------1 1 2 2-Tetrachloroethane , , ' --7 u 108-88-3--------Toluene 7 u 108-90-7--------Chlorobenzene 7 u 100-41-4--------Ethylbenzene 7 u 100-42-5------~-styrene 7 u 1330-20-7-------Total Xylenes 7 u
FORM I VOA 1/87 Rev.
20937 94 SAMPLE DQTA SUMMARV 1 ,• C e,._
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
' '
Lab Name: COMPUCHEK.RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
·Matrix: ( soil/water) SOIL Lab Sample ID:
SBS-2-1
No.: 94
361456
Sample wt/vol: 5.0 (g/mL) _G_ Lab File ID: GH061456Cl3
Level: (low/med) LOW
\ Moisture: not dee. ____ll
Column (pack/cap) C~P
Number 'I'ICs found: __J,_
CAS NUMBER COMPOUND NAME
Date Received: QBL02L90
Date Analyzed: Q8LllL90
Dilution Factor: ~l~-=o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGLKG
RT EST. CONC. Q
================ ============================ ======== ============= =====
1. LABORATORY ARTIFACT 0.75 5. 9 BJ
FORM I VOA-TIC 1/87 Rev.
20937 94 SAMPLE DlTA SUMMARY 1 6-
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW5-4S-1MS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94 ~--
Matrix: ( soil/water) SOIL Lab Sample IO: 361461
Sample wt/vol: 5.0 (g/mL) _G_ Lab File IO: GR061461All
Level: ( low/med) LOW Date Received: 08/02/90
% Moisture: not dee. _ll Date Analyzed: 08/12/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u
75-09-2--~------Methylene Chloride 8 B
67-64-1---------Acetone 21 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2---~----l,2-Dichloroethane 6 u
78-93-3--------~2-Butanone 12 u
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5~--------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------l,2-Dichloropropane 6 u
10061-01-5-----.-cis-l, 3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
7!i-25-2---------Bromoform 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane , , , --6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
20937 94 SAMPLE f~TA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
. MW5-4S-1MSD
Lab Na:me: COMPUCHEM,RTP Contract: 12-88!-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,,_9..:,4 __
Matrix: (soil/water) SOIL Lab Sample ID: 361462
Sample wt/vol: 5.0 (g/mL) _G __ Lab File ID: G2R61462All
Level: (low/med) LOW Date Received: 08/02/90
% Moisture: not dee. _ll Date Analyzed: 08/21/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) l,!G/KG Q
74-87-3---------Chloromethane 12 u
74-83-9---------Bromomethane 12 u
75-01-4---------Vinyl Chloride 12 u
75-00-3---------Chloroethane 12 u.
75-09-2---------Methylene Chloride 35 B 67-64-1---------Acetone 180 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 12 u
71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 12 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5----~-cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02~6------Trans-l,3-Dichloropropene __ 6 u
7 ~;-2 5-2---------Bromof orm 6 u
108-10-1--------4-Methyl-2-Pentanone 12 u
591-78-6--------2-Hexanone 12 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 l 2 2-Tetrachloroethane , , , --6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4-~------Ethylbenzene 6 u
100-42-5--------Styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
20937 94 SAMPLE D1TA SUMMARY 1 .· .-b...:.:
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
SB7-2-1DLMS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94 ~--
Matrix: (soil/water) SOIL Lab Sample ID: 364598
sample wt/vol: 4.0 (g/mL) _G __ Lab File ID: CN064598Al0
Level: (low/med) MED Date Received: 08/04/90
% Moist1Jre: not dee. _ii Date Analyzed: 08/16/90
Column: (pack/cap) CAP Dilution Factor: 4.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 6400 u 74-83-9---------Bromomethane 6400 u 75-01-4---------Vinyl Chloride 6400 u 75-00-3---------Chloroethane 6400 u 75-09-2--------~Methylene Chloride 2400 BDJ 67-64-1---------Acetone 11000 BO 7.5-15-o---------carbon Disulfide 3200 u
75-35-4---------1,1-Dichloroethene 3200 u 75-34-3---------1,1-Dichloroethane 3200 u
540-59-0--------1,2-Dichloroethene (total)_ 3200 u
67-66-3---------Chloroform 3200 u 107-06-2--------1,2-Dichloroethane 3200 u
78-93-3---------2-Butanone 6400 u
71-55-6---------1,1,1-Trichloroethane 3200 u 56-23-5---------carbon Tetrachloride 3200 u 108-05-4--------Vinyl Acetate 6400 u
75-27-4---------Bromodichloromethane 3200 u
78-87-5---------1,2-Dichloropropane 3200 u
10061-01-5------cis-l,3-Dichloropropene 3200 u
79-01-6---------Trichloroethene 3200 u
124-48-1--------Dibromochloromethane 3200 u
79-00-5---------1,1,2-Trichloroethane 3200 u
71··43-2---------Benzene ' 3200 u
10061-02-6------Trans-1,3-Dichloropropene __ 3200 u
75··25-2---------Bromoform 3200 u
108-10-1--------4-Methyl-2-Pentanone 6400 u
591-78-6--------2-Hexanone 6400 u
127-18-4--------Tetrachloroethene 28000 D
79-34-5---------1,1,2,2-Tetrachloroethane __ 3200 u
108-88-3--------Toluene 3200 u
108-90-7--------Chlorobenzene 3200 u
100-41-4--------Ethylbenzene 4300 D
100-42-5--------styrene 3200 u
1330-20-7-------Total Xylenes 17000 D
FORM I VOA 1/87 Rev.
94 SAMPLE D~TA SUMMARY 161
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SB7-2-1DLMSD Lab Name: COMPUCHEM.RTP Contract: (2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : .,_9.c,4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 364599
Sample wt/vol: 4.0 (g/mL) _G_ Lab File ID: CR064599B10
Level: (low/med) MED Date Received: 08/04/90
% Moisture: not dee. _n Date Analyzed: 08/16/90
Column: . (pack/cap) ~Af Dilution Factor:
C:AS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 6400
74-83-9---------Bromomethane 6400
75-01-4-~-------Vinyl Chloride 6400
75-00-3---------Chloroethane 6400
75-09-2---------Methylene Chloride 1200
67-64-1---------Acetone 8200
75-15-o---------carbon Disulfide 3200
75-35-4---------1,1-Dichloroethene 3200
75-34-3---------1,1-Dichloroethane 3200
540-59-0--------1,2-Dichloroethene (total)_ 3200
67-66-3---------Chloroform 3200
107-06-2--------1,2-Dichloroethane 3200
78-93-3---------2-Butanone 6400
71-55-6---------1,1,1-Trichloroethane 3200
56-23-5---------carbon Tetrachloride 3200
108-05-4--------Vinyl Acetate 6400
75-27-4---------Bromodichloromethane 3200
78-87-5---------1,2-Dichlcropropane 3200
10061-01-5------cis-l,3-Dichloropropene 3200
79-01-6---------Trichloroethene 3200
124-48-1--------Dibromochloromethane 3200
79-00-5---------1,1,2-Trichloroethane 3200
71·-4 3-2---------Benzene 3200
10061-02-6------Trans-1,3-Dichloropropene __ 3200
75·-25-2---------Bromoform 3200
108-10-1--------4-Methyl-2-Pentanone 6400
591-78-6--------2-Hexanone 6400
127-18-4--------Tetrachloroethene 26000
79-34-5---------1,1,2,2-Tetrachloroethane __ 3200
108-88-3--------Toluene 3200
108-90-7--------Chlorobenzene 3200
100-41-4--------Ethylbeniene ' 4200
100-42-5--------Styrene 3200
1330-20-7-------Total Xylenes 17000
4.0
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FORM I VOA 1/87 Rev.
94 SAMPLE DQTA SUMMARY 16(
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW15-2S-l Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Cod•~: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 36)56)
Sample wt/vol: )0.2 (g/mL) _G_ Lab File ID: GD063563B15
Level: (low/med) LOW Date Received: 08/09/90
% Moisture: not dee. --1.Q dee. Date Extracted: 08/15/90 ,
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/24/90
GPC Cleanup: (Y/N) li_ pH: _L..1 Dilution Factor: ~2~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 730
lll-44-4--------bis(2-Chloroethyl)Ether 730
95-57-8---------2-Chlorophenol 7)0
541-73-1--------1,3-Dichlorobenzene 730
106-46-7--------1,4-Dichlorobenzene 730
100-51-6--------Benzyl Alcohol 730
95-50-1---------1,2-Dichlorobenzene 730
95-48-7---------2-Methylphenol 97
39638-32-9------bis(2-Chloroisopropyl)Ether_ 730
106-44-5--------4-Methylphenol 7)0
621-64-7-~------N-Nitroso-Di-n-Propylamine __ 730
67-72-1---------Hexachloroethane 730
98-95-3---------Nitrobenzene 730
78-59-1---------Isophorone -730
88-75-5---------2-Nitrophenol ,730
105-67-9--------2,4-Dimethylphenol 730
65-85-o------~--Benzoic Acid 3500
lll-9l-l--------bis(2-Chloroethoxy)Methane __ 7)0
120-83-2--------2,4-Dichlorophenol 730
120-82-1--------1,2,4-Trichlorobenzene 730
91-20-3---------Naphthalene 730
106-47-8--------4-Chloroaniline 730
87·-68-3---------Hexachlorobutadiene 7)0
59-50-7---------4-Chloro-3-Methylphenol 730
91-57-6---------2-Methylnaphthalene 730
77-47-4---------Hexachlorocyclopentadiene __ 730
88-06-2---------2,4,6-Trichlorophenol 730
95-95-4---------2,4,5-Trichlorophenol )500
91-58-7---------2-Chloronaphthalene 730
88-74-4---------2-Nitroaniline 3500
131-11-3--------Dimethyl Phthalate 1500
208-96-8--------Acenaphthylene 7)0
606-20-2----~---2,6-Dinitrotoluene 730
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FORM I SV-1 1/87 Rev.
Q
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW15-2S-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: ( soil/water) SOIL Lab Sample ID: 363563
sample wt/vol: 30.2 (g/mL) _G_ Lab File ID: GD063563815
Level: (low/med) LOW Date Received: 08/09/90
% Moisture: not dee. _lQ dee. Date Extracted: 08/15/90
Extraction: (SepF/Cont/Sonc) S,OliQ Date Analyzed: 08/24/90
GPC Cleanup: (Y/N) I:!__ pH: ....L..1 Dilution Factor: ~2~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 3500
8:3-32-9---------Acenaphthene 730
51-28-5---------2,4-Dinitrophenol 3500
100-02-7--------4-Nitrophenol 3500
132-64-9--------Dibenzofuran 730
121-14-2--------2,4-Dinitrotoluene . 730
84-66-2---------Diethylphthalate 9500
7005-72-3-------4-Chlorophenyl-phenylether __ 730
86-73-7---------Fluorene 730
100~01-6--------4-Nitroaniline 3500
534-52-1--------4,6-Dinitro-2-Methylphenol __ 3500
86-30-6---------N-Nitrosodiphenylamine (l)_ 730
101-55-3--------4-Bromophenyl-phenylether __ 730
118-74-1--------Hexachlorobenzene 730
87-86-5---------Pentachlorophenol 3500
85-01-8---------Phenanthrene 730
120-12-7--------Anthracene 730
84 ·-7 4-2---------Di-n-Butylphthalate 730
206-44-0--------Fluoranthene 730
129-00-o--------Pyrene 730
85··68-7---------Butylbenzylphthalate 730
91-94-1---------3,3'-Dichlorobenzidine 1500
56-55-3---------Benzo(a)Anthracene 730
218-01-9--------Chrysene 730
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 88
117-84-0--------Di-n-Octyl Phthalate 730
205-99-2--------Benzo(b)Fluoranthene 730
207-08-9--------Benzo(k)Fluoranthene 730
50-32-8---------Benzo(a)Pyrene 730
193-39-5--------Indeno(l,2,3-cd)Pyrene 730
53-70-3---------Dibenzo(a,h)Anthracene 730
191-24-2--------Benzo(g,h,i)Perylene 730
(1) -Cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
Q
1 s:=
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lF EPA SAMPLE tlO. SEMIVOLATILE ORGANICS ANALYSIS "DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW15-2S-l
Lab Name: COMPUCHEM.RTP Contract: (2-88}-REVS
Lab Code: COMPU Case No.: 20937
Matrix: ( soil/water) SOIL
Sample ~rt/vol: 30.2 (g/mL) _G_
Level: (low/med) LOW
% Moisture: not dee. _.lQ dee.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: · (Y/N) N_ pH:. _i_._1
Number TICs found: __ 2
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: =9~4 __
Lab Sample ID: :3~6=3=5=6~3 __ _
Lab File ID: GD063563B15
Date Received: 08/09/90
Date Extracted: 08/15/90
Date Analyzed: 08/24/90
Dilution Factor: 2.0 ~---
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. ·Q ================ ============================ ======== ============= =====
1.
2.
UNKNOWN PHTHALATE
UNKNOWN PHTHALATE
FORM I SV-TIC
18.25
18.37
510
590
1/87 Rev.
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW15-4S-l
Lab Nam,~: COMPUCHEM. RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ,,_9.:,.4 __
Matrix: (soil/water) SOIL Lab Sample ID: ~3~6~3~5~6~4c_ __ _
Sample wt/vol: 30.1 (g/mL) _G_ Lab File ID: GH063564B15
Level: ( 1 ow /med) LOW Date Received: 08/09/90
% Moisture: not dee. _ll dee. Date Extracted: 08/15/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: · 08/23/90
GPC Cleanup: (Y/N) !i_ pH: J..,..a Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 410 u
lll-44-4--------bis(2-Chloroethyl)Ether 410 u 95-57-8---------2-Chlorophenol 410 u
541-73-1--------1,3-Dichlorobenzene 410 u
106-46-7----~---1,4-Dichlorobenzene 410 u
100-51-6--------Benzyl Alcohol 410 u
95-50-1---------1,2-Dichlorobenzene 410 u
95-48-7---------2-Methylphenol 410 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u
106-44-5--------4-Methylphenol 410 u
· 621-64-7--------N-Nitroso-Di-n-Propylamine __ 410 u
67-72-1-------~-Hexachloroethane 410 u
98-95-3---------Nitrobenzene 410 u
78-59-1---------Isophorone 410 u
88-75-5---------2-Nitrophenol 410 u
105-67-9--------2,4-Dimethylphenol 410 u
65-85-0---------Benzoic Acid 2000 u
111-91-1--------bis(2-Chloroethoxy)Methane __ •' 410 u
120-83-2--------2,4-Dichlorophenol 410 u
120-82-1--------1,2,4-Trichlorobenzene 410 u
91·-20-3---------Naphthalene 410 u
106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7---------4-Chloro-3-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47-4---------Hexachlorocyclopentadijne __ 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 410 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 1600
208-96-8--------Acenaphthylene 410 u
606-20-2--------2,6-Dinitrotoluene 410 u
FORM I SV-1 1/87 Rev.
1 ."i;.;
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW15-4S-l
Lab Name: COMPUCHEM RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : 94
Matrix: (soil/water) SOIL Lab Sample ID: 363564
Sample wt/vol: 30.1 ( g/mL) G __ Lab File ID: GH063564B15
Level: ( low/med) LOW Date Received: 08/09/90
% Moisture: not dee. --12 dee. Date Extracted: 08/15/90
Extraction: (SepF /Cont/Sonc) SONC Date Analyzed: 08/23/90
GPC Cleanup: (Y/N) !:L_ pH: ~ Dilution Factor: ~l~-~o __ _
C:AS NO. COMPOUND.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
9~-09-2---------3-Nitroaniline 2000
83-32-9---------Acenaphthene 410
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 410
121-14-2--------2,4-Dinitrotoluene 410
84-66-2---------Diethylphthalate 3800
7005-72-3-------4-Chlorophenyl-phenylether __ 410
86-73-7---------Fluorene 410
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000
86-30-6---------N-Nitrosodiphenylamine (1)_ 410
101-55-3--------4-Bromophenyl-phenylether __ 410
118-74-1--------Hexachlorobenzene 410
87-86-5---------Pentachlorophenol 2000
85-01-8 ----·-----Phenanthrene 410
120-12-7--------Anthracene 410
84-74-2---------Di-n-Butylphthalate 42
206-44-0--------Fluoranthene 410
129-00-o-~------Pyrene 410
85-68-7---------Butylbenzylphthalate 410
91-94-1---------3,3'-Dichlorobenzidine 810
56-55-3---------Benzo(a)Anthracene 410
218-01-9--------Chrysene 410
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 110
117-84-0--------Di-n-Octyl Phthalate 410
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 410
50-32-8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 410
53-70-3---------Dibenzo(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
(1) -Cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
94 SAMPLE D1TA SUMMARY
Q
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW15-4S-l
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Codi?: COMPU Case No.: 20937 SAS No. : SDG No. : ~94..,____
Matrix: (soil/water) SOIL Lab Sample ID: .._3 ... 6.,_3"-56s,c4:,__ __ _
Sample wt/vol: 30.1 (g/mL) _G_ Lab File IO: GH063564B15
Level: ( low/med) LOW Date Received: 08/09/90
% Moisture: not dee. _ll dee. Date Extracted: 08/15/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/23/90
GPC Cleanup: (Y/N) r!_ pH: _L_a Dilution Factor: ~l~-~o __ _
Number TICs found: ---2
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q =======•========== ============================ ======== ============= ==:::;;:==
1. SOLVENT CONTAMINANT 5.10 200 J
2. SOLVENT CONTAMINANT 5.77 250 J
3. UNKNOWN PHTHALATE 18. 30 250 J
4. UNKNOWN PHTHALATE 18.42 290 J
5. 74381-40-1 PROPANOIC ACID, 2-METHYL-, 1-,( 11.22 610 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE D~TA SUMMARY 154
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW5-4S-l Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ~9.,_4 __
Matrix: ( soil/water) SOIL Lab Sample ID: 361457
sample wt/vol: 30.5 (g/mL) _G_ Lab File ID: GH061457A08
• Level: (low/med) LOW Date Received: 08/02/90
% Moisture: not dee. ___JJ!_ dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) li...._ pH: --2...,.]_ Dilution Factor:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol. 400
lll-44-4--------bis(2-Chloroethyl)Ether 400
95-57-8---------2-Chlorophenol 400
541-73-1--------1,3-Dichlorobenzene 400
106-46-7--------1,4-Dichlorobenzene 400
100-51-6--------Benzyl Alcohol 400
95-50-1---------1,2-Dichlorobenzene 400
95-48-7---------2-Methylphenol 400
39638-32-9------bis(2-Chloroisopropyl)Ether_ 400
106-44-5--------4-Methylphenol . 400
621-64-7--------N-Nitroso-Di-n-Propylamine __ 400
67-72-1---------Hexachloroethane 400
98-95-3---------Nitrobenzene 400
7 8 ·-59-1---------Isophorone 400
88-75-5---------2-Nitrophenol 400
105-67-9--------2,4-Dimethylphenol ¼ 00
65-85-0---------Benzoic Acid 1900
lll-91-l--------bis(2-Chloroethoxy)Methane __ 400
120-83-2--------2,4-Dichlorophenol 400
120-82-1--------1,2,4-Trichlorobenzene 400
91-20-3---------Naphthalene 400
106-47-8--------4-Chloroaniline 400
87-68-3---------Hexachlorobutadiene 400
59-50-7---------4-Chloro-3-Methylphenol 400
91-57-6---------2-Methylnaphthalene 400
77-47-4---------Hexachlorocyclopentadiene __ 400
88-06-2---------2,4,6-Trichlorophenol 400
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 400
88-74-4---------2-Nitroaniline 1900
131-11-3--------Dimethyl Phthalate 400
208-96-8--------Acenaphthylene 400
606-20-2--------2,6-Dinitrotoluene 400
1.0
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FORM I SV-1 1/87 Rev.
Q
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW5-4S-1
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361457
Sample wt/vol: 30.5 (g/mL) _G_ Lab File ID: GH061457A08
Level: ( low/med) LOW Date Received:. 08/02/90
% Moisture: not dee. _ll dee. Date Extracted: 08/08i90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) li_ pH: -2..,.]_ Dilution Factor: ~1~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline .. 1900
83-32-9---------Acenaphthene 400
51-28-5---------2,4-Dinitrophenol 1900
100-02-7------~-4-Nitrophenol 1900
132-6~-9--------Dibenzofuran 400
121-14-2--------2,4-Dinitrotoluene 400
84-66-2---------Diethylphthalate 400
7005-72-3-------4-Chlorophenyl-phenylether __ 400
86-73-7---------Fluorene 400
100-01-6--------4-Nitroaniline 1900
534-52-1--------4,6-Dinitro-2-M,thylphenol __ 1900
86··30-6---------N-Nitrosodiphenylamine (l)_ 400
101-55-3--------4-Bromophenyl-phenylether __ 400
118-74-1--------Hexachlorobenzene 400
87-86-5---------Pentachlorophenol 1900
85-0l~a--------~Phenanthrene 400
120-12-7--------Anthracene .. 400
8 4 -· 7 4-2---------Di-n-Butylphthalate 40,0
206-44-0--------Fluoranthene 400
129-00-0-----.---Pyrene 400
85-68-7---------Butylbenzylphthalate 400
91-94-1---------3,3'-Dichlorobenzidine 790
56-55-3---------Benzo(a)Anthracene 400
218-01-9~-------Chrysene 400
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 400
117-84-0--------Di-n-Octyl Phthalate 400
205-99-2--------Benzo(b)Fluoranthene 400
207-08-9--------Benzo(k)Fluoranthene 400
50-32-8---------Benzo(a)Pyrene 400
193-39-5--------Indeno(l,2,3-cd)Pyrene 400
53-70-3---------Dibenzo(a,h)Anthracene 400
191-24-2--------Benzo(g,h,i)Perylene 400
(1) -cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
20937 94\ SQMP!t DnTQ SUMMQPV·
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.5 (g/mL) _G_ Lab File ID:
Level: (low/med) LOW Date· Received:
% Moistu.re: not dee. ____ll_ dee. Date Extracted:
EPA SAMPLE tlO.
MW5-4S-l
No.: 94
361457
GH061457A08
08/02/90
08/08/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) IL._ pH: ....2.,_]_ Dilution Factor: ~l~-~o __ _
Number TICs found: _7
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. ================ ============================ ======== ==============
1. SOLVENT CONTAMINANT 5.68 1700
2. VOA TCL 6.48 200
3. UNKNOWN 6.55 280
4. ALDOL 6.68 480
5. UNKNOWN 7.88 240
6. UNKNOWN PHTHALATE 20.10 160
7: UNKNOWN PHTHALATE 20.24 200
FORM I SV-TIC 1/87 Rev.
·-:> •'.> q, 7 q 4. ,-,-,/', :=-1 E. [·,QT,-, <:;L/ /'1/'1 1-•F· '·' ~ ~ _,. ...., I .., ~ M I ' I..R-. • • ,.., -r'f . )
Q
=====
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW8-4S-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: ( soil/water) SOIL Lab Sample ID: 362491
sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GH062491B15
Level: (low/med) rpw Date Received: 08/04/90
% Moisture: not dee. _il_ dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/22/90
GPC Cleanup: (Y/N) li._ pH: ---2...,.Q Dilution Factor: 1.00
CONCENTRATION UNITS:
CJ,S NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 460 u
lll-44-4--------bis(2-Chloroethyl)Ether 460 u
95-57-8---------2-Chlorophenol 460 u
541-73-1--------1,3-Dichlorobenzene 460 u
106-46-7--------1,4-Dichlorobenzene 460 u
100-51-6--------Benzyl Alcohol 460 u
95-50-1---------1.2-Dichlorobenzene 460 u
95-48-7---------2-Methylphenol 460 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 460 u
106-44-5--------4-Methylphenol 460 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 460 u
~7-72-1---------Hexachloroethane 460 u
98-95-3---------Nitrobenzene 460 u
78-59-1---------Isophorone 460 u
88-75-5---------2-Nitrophenol 460 u
105-67-9--------2,4-Dimethylphenol 460 u
65-85-0---------Benzoic Acid . 2200 u
111-.91-1--------bis ( 2-Chloroethoxy) Methane __ 460 u
120-83-2--------2,4-Dichlorophenol 460' u
120-82-1-------~l,2,4-Trichlorobenzene 460 u
91-20-3---~-----Naphthalene 460 u
106-47-8-----~--4-Chloroaniline 460 u
87-68-3---------Hexachlorobutadiene 460 u
.59-50-7---------4-Chloro-3-Methylphenol 460 u
91-57-6---------2-Methylnaphthalene 460 u
77-47-4---------Hexachlorocyclopentadiene __ 460 u
88-06-2---~-----2,4,6-Trichlorophenol 460 u
95-95-4---------2,4,5-Trichlorophenol 2200 u
91-58-7---------2-Chloronaphthalene 460 u
88~74~4---------2-Nitroaniline 2200 u
131-11-3--------Dimethyl Phthalate 460 u
208-96-8--------Acenaphthylene 460 u
606-20-2--------2,6-Dinitrotoluene 460 u
FORM I SV-1 1/87 Rev.
94 SAMPLE DQTA SUMMARY 1 50
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW8-4S-l Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Cod,i: COMPU Case No.: -20937 SAS No.: SDG No.: "'9..:,4 __
Matrix: (soil/water) SOIL Lab Sample ID: ~3~6~2~4~9~1'----
Sample wt/vol: 30.0 (g/mL) Q.____ Lab File ID: GH062491B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee.~ dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: ·08/22/90
GPC Cleanup: (Y/N) .t!__ pH: ....2..,_.Q Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2200
83~32-9------~--Acenaphthene 460
· 51-28-5---------2,4-Dinitrophenol 2200
100-02-7--------4-Nitrophenol 2200 132-64-9-.,.------Dibenzofuran 460
121-14-2--------2,4-Dinitrotoluene 460
84-66-2---------Diethylphthalate 460
7005-72-3-------4-Chlorophenyl-phenylether __ 460 86-73-7---------Fluorene 460
100-01-6--------4-Nitroaniline 2200
5J4-52-l--------4,6-Dinitro-2-Methylphenol __ 2200
86-30-6---------N-Nitrosodiphenylamine (l)_· -460
llll-55-3---~----4-Bromophenyl-phenylether __ 460
118-74-1--------Hexachlorobenzene 460
87-86-5---------Pentachlorophenol 2200
8!i-Ol-8---------Phenanthrene 460
1:10-12 -7--------Anthracene 460
8~-74-2---------Di-n-Butylphthalate 460
206-44-0--------Fluoranthene 460
1,:9-oo-o--------Pyrene 460
8~;-68-7---------Butylbenzylphthalate 460
91-94-1---------3,3'-Dichlorobenzidine 920
56-55-3---------Benzo(a)Anthracene 460
218-01-9--.------Chrysene 460
ll7-,.81-7--------bis(2-Ethylhexyl)Phthalate __ 51
117-84-0--------oi-n-Octyl Phthalate 62
205-99-2--------Benzo(b)Fluoranthene 460
207-08-9-----~--Benzo(k)Fluoranthene 460
50-32-8.,.--------Benzo(a)Pyrene 460
193-39-5--------Indeno(l,2,3-cd)Pyrene 460
53-70-3---------Dibenzo(a,h)Anthracene 460
191-24-2--------Benzo(g,h,i)Perylene 460
(1) -Cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
94 SAMPLE DATA SLIMMARY
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
MW8-4S-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ..,_9.:,4_· __
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee. ___ll dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H...._ pH:
Number TICS found: ---2.
CAS NUMBER COMPOUND
_G_
~
--2.,_0
NAME
Lab Sample ID: .,.3-"6.,,_2c,._49"'-"'..l __ _
Lab File ID: GH062491B15
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/22/90
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ================= =========================== ======== ============= ===== 1. UNKNOWN PHTHALATE 17.75 320 J 2. UNKNOWN PHTHALATE 17.85 510 J 3. UNKNOWN PHTHALATE 17.97 690 J
4. UNKNOWN PHTHALATE 18.09 650 J
5. UNKNOWN PHTHALATE 18.19 1000 J 6. UNKNOWN PHTHALATE 18.30 1200 J
7. UNKNOWN PHTHALATE 18.40 1200 J
8. UNKNOWN PHTHALATE 18.52 740 J
9. UNKNOWN PHTHALATE 18.64 370 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPL2 DQTA SUMM~RV 14S
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18 EPA SAMPLE llO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW8-4S-2
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362492
sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GH062492815
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _ll dee. Date Extracted: 08/08/90
Extracti()n: (SepF /Cont/Sane) SONC Date Analyzed: 08/22/90
Dilution Factor: 1.00 GPC Cleanup: (Y/N) Ii__ pH: ...2J.
CONCENTRATION UNITS:
CJlS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 460 u
lll-44-4--------bis(2-Chloroethyl)Ether 460 u
9~;-51-8---------2-Chlorophenol 460 u
541-73-1--------1,3-Dichlorobenzene 460 u
106-46-7--------1,4-Dichlorobenzene 460 u
100-51-6--------Benzyl Alcohol 460 u
95-50-1---------1,2-Dichlorobenzene 460 u
95-48-7---------2-Methylphenol 460 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 460 u
106-44-s~-------4-Methylphenol 460 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 460 u
67-72-1---------Hexachloroethane 460 u
98-95-3---------Nitrobenzene 460 u
78-59-1---------Isophorone 460 u
88-75-5---------2-Nitrophenol 460 u
105-67-9--------2,4-Dimethylphenol 460 u
65-85-0------~-~Benzoic Acid 2200 u
lll-91-1--------bis(2-Chloroethoxy)Methane __ 460 u
120-83-2--------2,4-Dichlorophenol . 460 u
120-a2-1--------1,2,4-Trichlorobenzene 460 u
91-20-3---------Naphthalene 460 u
106-47-8--------4-Chloroaniline 460 u
87-68-3---------Hexachlorobutadiene 460 u
59 -50-7---------4-Chloro-3-Me·thylphenol . 460 u
91-57-6---------2-Methylnaphthalene 460 u
77-47-4---------Hexachlorocyclopentadiene __ 460 u
88-06-2---------2,4,6-Trichlorophenol 460 u
95-95-4---------2,4,5-Trichlorophenol 2200 u
91-58-7---------2-Chloronaphthalene 460 u
88-74-4---------2-Nitroaniline 2200 u
131-11:3-~------Dimethyl Phthalate 460 u
208-96-8--------Acenaphthylene 460 u
606-20-2~-------2,6-Dinitrotoluene 460 u
FORM I SV-1 1/87 Rev.
20937 9~ SAMP~E DATA SUMMARY 1 4;:
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA.SAMPLE NO.
MW8-4S-2 Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Cod,~: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362492
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: •GH062492B15
Level: (low/med). LOW Date Received: 08/04/90
\ Moisture: not dee. ---1..!!. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) Date Analyzed: 08/22/90
GPC Cleanup: (Y/N) ,IL_ pH: ....2.....l Dilution Factor: 1.00 =~--
Number TICs found: _.l_Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ==========--==== ====================-======= ======== ============= =====
l. TRIMETHYLHEPTANE 5.10 180 J 2. UNKNOWN PHTHALATE 17.75 280 J 3. UNKNOWN PHTHALATE 17.85 460 J 4. UNKNOWN PHTHALATE 17.97 650 J 5. UNKNOWN PHTHALATE 18.09 600 J 6. UNKNOWN PHTHALATE 18.19 1100 J 7. UNKNOWN PHTHALATE 18.30 1200 J 8. UNKNOWN PHTHALATE 18.40 1200 J 9. UNKNOWN PHTHALATE 18.52 690 J 10. UNKNOWN PHTHALATE 18.65 320 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DQTA SllMMARV 1 4:
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-4S-l
Lab Name: COMPUCHEM.RTP contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 363241
Sample wt/vol: 30.4 (g/mL) _G __ Lab File ID: GH063241B15
Level: (low/med) LOW Date Received: 08/08/90
% Moisture: not dee. _].Q dee. Date Extracted: 08(15/90
Extraction: ( SepF /Cont/Sonc) SQliQ Date Analyzed: 08/23/90
GPC Cleanup: (Y/N) li_ pH: ~ Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 470
lll-44-4--------bis(2-Chloroethyl)Ether 470
95-57-8--~------2-Chlorophenol 470
541-73-1--------1,3-Dichlorobenzene 470
106-46-7--------l,4-Dichlorobenzene 470
100-51-6--------Benzyl Alcohol 470
95-50-1---------1,2-Dichlorobenzene 470
95-48-7---------2-Methylphenol 470
39638-32-9------bis(2-Chloroisopropyl)Ether_ 470
106-44-5--------4-Methylphenol 470
621-64-7--------N-Nitroso-Di-n-Propylamine __ 470
67-72-1---------Hexachloroethane 470
93-95-3---------Nitrobenzene 470
78-59-1---------Isophorone 470
88-75-5---------2-Nitrophenol 470
105-67-9--------2,4-Dimethylphenol 470
6!;-as-o---------Benzoic Acid 2300
lll-91-l--------bis(2-Chloroethoxy)Methane_ 470
120•83-2--------2,4-Dichlorophenol 470
120-a2-1--------1,2,4-Trichlorobenzene 470
91-20-3--~------Naphthalene 470
11)6-4 7-8--------4-Chloroanil ine 470
87-68-3-----.;.---Hexachlorobutadiene 470
S!l-50-7---------4-Chloro-3-Methylphenol 470
91-57-6---------2-Methylnaphthalene 470
77-47-4---------Hexachlorocyclopentadiene __ 470
811-06-2---------2,4,6-Trichlorophenol 470
95-95-4---------2,4,5-Tri~hlorophenol 2300
91-58-7---------2-Chloronaphthalene 470
88-74-4---------2-Nitroaniline 2300
131-11-3--------Dimethyl Phthalate 470
208-96~8--------Acenaphthylene 470
606-20-2--------2,6-Dinitrotoluene 470
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
Q
1 4-
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name:. COMPUCHEM. RTP Contract: 12-881-REVS
MW9-4S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : 94
Matrix: (soil/water) SOIL Lab Sample ID: 363241
Sample wt/vol: 30. 4' (g/mL) _G_ Lab File ID: GH063241B15
Level: (low/med) LOW Date Received: 08/08/90
\ Moisture: not dee. _]_Q dee. Date Extracted: 08/15/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/23/90
GPC Cleanup: (Y/N) lL_ pH: .--2..,_2_ Dilution Factor: ~i~-~o __ _
CJlS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2300
83-32-9---------Acenaphthene 470
51-28-5---------2,4-Dinitrophenol 2300
100-02-7--------4-Nitrophenol 2300
132-64-9--------Dibenzofuran 470
121-14-2--------2,4-Dinitrotoluene 470
84-66-2---------Diethylphthalate 470
7005-72-3-------4-Chlorophenyl-phenylether __ . 470
86-73-7------~--Fluorene 470
100-01-6--------4-Nitroaniline 2300
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2300
86-30-6--~------N-Nitrosodiphenylamine (l)_ 470
101-55-3--------4-Bromophenyl-phenylether __ 470
118-74-1--------Hexachlorobenzene 470
87-86-5---------Pentachlorophenol 2300
85-01-8---------Phenanthrene 470
120-12-7--------Anthracene 470
84-74-2---------Di-n-Butylphthalate 470
206-44-0--------Fluoranthene 470
129-oo-o--------Pyrene 470
85-68-7---------Butylbenzylphthalate 470
.91-94-1---------3,3'-Dichlorobenzidine 930
56-55-3----~----Benzo(a)Anthracene 470
218-01-9---:------Chrysene 470
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 110
117-84-0--------Di-n-Octyl Phthalate 470
20.5-99-2--------Benzo(b)Fluoranthene 470
207-08-9--------Benzo(k)Fluoranthene 470
50·-32-8---------Benzo (a) Pyrene 470
19:3-39-5--------Indeno(l,2,3-cd)Pyrene 470
53·-70-3---------Dibenzo (a, h) Anthracene 470
191-24-2--------Benzo (g, h·, i) Perylene 470
( 1) ·• Cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
94 SAMPLE DATA SUMrlARV
Q
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW9-4S-l
Lab Naml!: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Codi!: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL) _G_
Level: (low/med) LOW
\ Moistu:re: not dee. _.1Q dee.
' Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ii..... pH: ....2..,.,2_
Nwnber TICs found: --9.
CAS NUMBER COMPOUND NAME
SAS No.: SOG No.: -"9..:,4 __
Lab Sample ID: ~3~6~3~2..:,4~1~---
Lab File ID: GH063241Bl5
Date Received: 08/08/90
Date Extracted: 08/15/90
Date Analyzed: 08/23/90
Dilution Factor: £1~,~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ================ =========================== ======== ============= =====
1. SOLVENT CONTAMINANT 5.10 280 BJ
2. SOLVENT CONTAMINANT .S.77 240 BJ 3. BLANK CONTAMINANT 15.45 140 BJ
4. UNKNOWN PHTHALATE 17.87 240 J s. UNKNOWN PHTHALATE 17.99 280 J
6. UNKNOWN PHTHALATE 18.20 610 J 7. UNKNOWN PHTHALATE 18.30 800 J
8. UNKNOWN PHTHALATE 18.44 940 J
9. UNKNOWN PHTHALATE 18.55 470 J
FORM I SV-TIC _1/87 Rev.
20937 94 SAMPL~ DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
SBl0-1-1
Lab CodE!: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 3624!!5
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GJ062485B15
Level: (low /med) WW Date Received: 08/04/90
% Moisture: not dee. _li dee. Date Extracted: 08,'.08/90
Extraction: (SepF/Cont/Sonc) .5.QJ:!C Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) H.._ pH: ..i...Q Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
1<)8-95-2--------Phenol 390 u
111-44-4--------bis(2-Chloroethyl)Ether 390 u
9!i-57-8---------2-Chlorophenol 390 u 541-73-1--------1,3-Dichlorobenzene 390 u
106-46-7--------1,4-Dichlorobenzene 390 u
100-51-6--------Benzyl Alcohol 390 u 95-~0-1---------1,2-Dichlorobenzene 390 u 95-48-7---------2-Methylphenol 390 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 390 u 106-44-5--------4-Methylphenol 390 u 621-64-7--------N-Nitroso-Di-n-Propylamine __ 390 u 67-72-1---------Hexachloroethane 390 u
98-95-3-----~---Nitrobenzene 390 u 78-59-1---------Isophorone 390 u 88-75-5---------2~Nitrophenol 390 u
105-67-9--------2,4-Dimethylphenol 390 u
65-85-o---------Benzoic Acid 1900 u
lll-91-l7-------bis(2-Chloroethoxy)Methane __ 390 u
120-83-2--------2,4-Dichlorophenol 390 u
120-82-1--------1,2,4-Trichlorobenzene 390 u
91··20-3---------Naphthalene 390 u 106-47-8--------4-Chloroaniline 390 u
87-68-3---------Hexachlorobutadiene 390 u
59-50-7---------4-Chloro-3-Methylphenol 390 u 91-57-6---------2-Methylnaphthalene 390 u 77 ··4 7-4---------Hexachlorocyclopentadiene __ 390 u
88··06-2---------2, 4, 6-Trichlorophenol 390 u
95-95-4---------2,4,5-Trichlorophenol 1900 u
9 l-·58-7---------2-Chloronaphthalene 390 u
88-74-4---------2-Nitroaniline 1900 u
131-11-3--------Dimethyl Phthalate 390 u
208-96-8--------Acenaphthylene 390 u
606-20-2--------2,6-Dinitrotoluene 390 u
FORM I SV-1 1/87 Rev.
20937 91 SAMPtE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBl0-1-1 Lab Name: COMPUCHEM.RTP Contract: (2-BBl-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 49.:,.4 __
Matrix: (soil/water) SOIL Lab Sample ID: 362485
Sample wt/vol: 30.0 (g/mL) Q__ Lab File ID: GJ062485B15
Level: (low/med) IPW Date Received: 08/04/90
% Moist1Jre: not dee. --1..§. dee. Date Extracted: . 08/08/90
Extract.ion: ( SepF /Cont/Sonc) ~ Date Analyzed: . 08/25/90
GPC Cle,lnup: (Y/N) li..._ pH: _h2 Dilution Factor:
<::AS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1900 83-32-9---------Acenaphthene 390
51-28-5---------2,4-Dinitrophenol 1900
100~02-7--------4-Nitrophenol 1900
132-64-9----~---Dibenzofuran 390 121-14-2--------2,4-Dinitrotoluene 390
64-66-2---------Diethylphthalate 390
7005-72-3-------4-Chlorophenyl-phenylether __ 390
86-73-7---------Fluorene 390 100-01-6--------4-Nitroaniline 1900
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900
86-30-6---------N-Nitrosodiphenylamine (1) 390
101-55-3-~------4-Bromophenyl-phenylether-= 390
118-7 4-1--------Hexachloro.benzene 390
87-86-5---------Pentachlorophenol 1900
85-01-8---------Phenanthrene 390
120-12-7--------Anthracene 390
84-74-2-----~---Di-n-Butylphthalate 390
206-44-0--------Fluoranthene 390
129-00-0--------Pyrene 390
85-68-7---------Butylbenzylphthalate 390
91-94-1---------3,3'-Dichlorobenzidine 790
56-55-3---------Benzo(a)Anthracene .390
218-01-9--------Chrysene 390
117-81-7--------bis(2-Ethylhexyl)Phthalate 390
117-84-0--------Di-n-Octyl Phthalate --390
205-99-2--------Benzo(b)Fluoranthene 390
207-08-9--------Benzo(k)Fluoranthene 390
50-32-8---------Benzo(a)Pyrene 390
193-39-5--------Indeno(l,2,3-cd)Pyrene 390
53-70-3---------Dibenzo(a,h)Anthracene 390
l!H-24-2--------Benzo (g ,h, i) Perylene 390
(1) -Cannot be separated from D1phenylam1ne
l. 00
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FORM I sv-2 1/87 Rev.
20937 94 SAMP~E DATA SUMMARY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
. SBl0-1-1 Lab Name: COMPUCHEM.RTP Contract: {2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.:· ___ _ SDG No.: =9~4 __ I Matrix: (soil/water) SOIL Lab Sample ID: 362485
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sample wt/vol: 30.0 (g/mL) Q__
Level: (low/med) LOW
t Moisture: not dee. _l.§.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...._
Number TICS found: _2
dee.
~
pH: ....2..,_.Q
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
GJ062485B15
08/04/90
08/08/90
08/25/90
l. oo
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ===========.==== ================-====---===-======== ============= ===== 1. ALOOL 5.97 400 AJ 2. UNKNOWN PHTHALATE 18.22 280 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DQTA SUMMAR\'
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: /2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
SBl0-2-1
No.: 94 I Matrix: (soil/water) SOIL Lab Sample ID: 362486
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Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GJ062486B15
Level: (low/med) LOW Date Received: 08/04/90
t Moisture: not dee. _.lQ dee. Date Extracted: 08/08/90
Extraction: ( SepF /Cont/Sonc)
(Y/N) .Ii_
~
pH: ...2...1
Date Analyzed: 08/24/90
GPC Cleanup: Dilution Factor: 1.00
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 370 u
lll-44-4--------bis(2-Chloroethyl)Ether 370 u 95-57-8---------2-Chlorophenol 370 u
541-73-1--------1,3-Dichlorobenzene 370 u
106-46-7--------1,4-Dichlorobenzene 370 u
100-51-6--------Benzyl Alcohol 370 u
95-50-1---------1,2-Dichlorobenzene 370 u
95-48-7---------2-Methylphenol 370 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370 u
106-44-5--------4-Methylphenol 370 u
621-64-7-----..:--N-Nitroso-Di-n-Propylamine __ 370 u
67-72-1---------Hexachloroethane 370 u
98-95-3--~-~----Nitrobenzene 370 u
78-59-1---------Isophorone 370 u
88-75-5---------2-Nitrophenol 370 u
105-67-9--------2,4-Dimethylphenol 370 u
65-85-0---------Benzoic Acid 1800 u
lll-91-1--------bis(2-Chloroethoxy)Methane __ 370 u
120-83-2--------2,4-Dichlorophenol 370 u
120-82-1--------1,2,4-Trichlorobenzene 370 u
91-20-3-----~---Naphthalene 370 u·
106-47-8--------4-Chloroaniline 370 u
87-68-3---------Hexachlorobutadiene 370 u
59-50-7---------4-Chloro-3-Methylphenol 370 u
·91-57-6---------2-Methylnaphthalene 370 u
77-47-4---------Hexachlorocyclopentadiene __ 370 u
88-06-2---------2,4,6-Trichlorophenol 370 u
95-95-4---------2,4,5-Trichlorophenol 1800 u
91-58-7---------2-Chloronaphthalene 370 u
88-74-4---------2-Nitroaniline 1800 u
131-11-3--------Dimethyl Phthalate 370 u
208-96-8--------Acenaphthylene 370 u
606-20-2--~-----2,6-Dinitrotoluene 370 u
FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DQTA SLIMMARY l 3,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBl0-2-1
.Lab Name: COMPUCHEM.RTP contract: /2-88)-REVS
Lab Code: COMPU Case No.: 20937 .SAS No.: SDG No.: 94
Matrix: ( soil/water) SOIL Lab sample IO: 362486
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GJ062486B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ___lQ dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/24/90
Dilution Factor: 1.00 GPC Cleanup: (Y/N) lL.. pH: ~
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u 83-32-9---------Acenaphthene 370 u
51-28-5---------2,4-Dinitrophenol 1800 u 100-02-7--------4-Nitrophenol 1800 u
132-64-9--------0ibenzofuran 370 u 121-14-2--------2,4-0initrotoluene 370 u 84-66-2---------0iethylphthalate 370 u
7005-72-3-------4-Chlorophenyl-phenylether __ 370 u
86-73-7---------Fluorene 370 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800 u 86-30-6---------N-Nitrosodiphenylamine (1)_ 370 u
101-55-3--------4-Bromophenyl-phenylether __ 370 u
118-74-1--------Hexachlorobenzene 370 u
87-86-5~--------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 370 u
120-12-7-------•Anthracene 370 u
84-74-2---------Di•n-Butylphthalate 370 u
206-44-0--------Fluoranthene 370 u
129-00-0--------Pyrene 370 u
85-68-7---------Butylbenzylphthalate 370 u
91-94-1---------3,3'-0ichlorobenzidine 730 u
56-55-3---------Benzo(a)Anthracene 370 u
218-01-9---~----Chrysene 370 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 370 u
117-84-0--------Di-n-octyl Phthalate 370 u
205-99-2--------Benzo(b)Fluoranthene 370 u
207-08-9--------Benzo(k)Fluoranthene 370 u
50-32-8---------Benzo(a)Pyrene 370 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 370 u
53-70-3---------Dibenzo(a,h)Anthracene 370 u
191-24-2--------Benzo(g,h,i)Perylene 370 u
(1) -cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS.DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SBl0-2-1
No.: 94
362486
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GJ062486B15
Level: (low/med) .IP=W __
% Moisture: not dee. ---1.0. dee.
Extraction: (SepF/Cont/Sonc) .5QliC
GPC Cleanup: (Y/N) Ji._ pH: -2..a.l.
Number TICs found: ---1,.
CAS NUMBER COMPOUND NAME
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/24/90
Dilution Factor: .i~-~o~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
================ ============================ ======== ============= =====
1. UNKNOWN HYDROCARBON -5. 07 220 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMP~E DATA SUMMARY ' .. 1 3 t
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SBll-1-1 Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
-Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362487
Sample wt/vol: 30.1 (g/mL) Q__ Lab File ID: GJ062487A08
Level: (low/med) IPW Date Received: 081'.0~1'.90
t Moisture: not dee. ---1..8. dee. Date Extracted: Q81'.081'.90
Extraction: ( SepF /Cont/Sonc) ~ Date Analyzed: QSl'.311'.90
GPC Cleanup: (Y/N) H...._ pH: ....2.....2 Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGl'.KG
108-95-2--------Phenol 400
lll-44-4--------bis(2-Chloroethyl)Ether 400 95-57-8---------2-Chlorophenol 400 541-73-1--------1,3-Dichlorobenzene 400
106-46-7--------1,4-Dichlorobenzene 400
100-51-6--------Benzyl Alcohol 400
95-50-1---------1,2-Dichlorobenzene 400
9 5-4 8-7-----·----2-Methylphenol 400
39638-32-9------bis(2-Chloroisopropyl)Ether_ 400
106-44-5--------4-Methylphenol 400
621-64-7--------N~Nitroso-Di-n-Propylamine __ 400
67-72-1---------Hexachloroethane 400 98-95-3---------Nitrobenzene 400 78-59-1---------Isophorone . 400
88-75-5---------2-Nitrophenol 400 105-67-9--------2,4-Dimethylphenol 400
65-85-o---------Benzoic Acid 160
lll-91-l--------bis(2-Chloroethoxy)Methane __ 400
120-83-2--------2,4-Dichlorophenol 400
120-82-1--------1,2,4-Trichlorobenzene 400
91-20-3---------Naphthalene 650 106-47-8--------4-Chloroaniline 400
87~68-3---------Hexachlorobutadiene 400
59-50-7---------4-Chloro-J-Methylphenol 400
91-57-6---------2-Methylnaphthalene 750
77-47-4---------Hexachlorocyclopentadiene __ 400
88-06-2---------2,4,6-Trichlorophenol 400
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 400 88-74-4---------2-Nitroaniline 1900
131-11-3--------Dimethyl Phthalate 400
208-96-8--------Acenaphthylene 1800
606-20-2------~-2,6-Dinitrotoluene 400
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FO!<M I SV-1 1/87 Rev.
20937 94 SAMPLE DQTA SUMMARY
Q
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lC EPA SAMPLE !lO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBll-l-1
Lab Name: COMPUCHEM.RTP Contract: (2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: ( soil/water) SOIL Lab Sample IO: 362487
Sample wt/vol: 30.1 (g/mL) _G_ Lab File ID: GJ062487A08
Level: (low/med) LOW Date Received: 08/04/90
\ Moisture: not dee. _l.8. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ,S.Qfil; Date Analyzed: 08/31/90
GPC Cleanup: (Y/NJ lL_ pH:~ Dilution Factor: ~i~-=o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1900 u
83-32-9---------Acenaphthene 87 J
51-28-5---------2,4-0initrophenol 1900 u
100-02-7--------4-Nitrophenol 1900 u
132-64-9--------Dibenzofuran 400 u
121-14-2--------2,4-Dinitrotoluene 400 u
84-66-2---------Diethylphthalate 400 u
7005-72-3-------4-Chlorophenyl-phenylether __ 400 u
86-73-7---------Fluorene 820
100-01-6--------4-Nitroaniline 1900 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 400 u
101-55-3--------4-Bromophenyl-phenylether __ 400 u
118-74-1--------Hexachlorobenzene 400 u
87-86-5---------Pentachlorophenol 1900 u
85-01-8---------Phenanthrene 1400
120-12-7--------Anthracene 570
84-74-2---------Di-n-Butylphthalate 43 J
206-44-0--------Fluoranthene 1300
129~00-0--------Pyrene 2800
85-68-7---------Butylbenzylphthalate 400 u
91-94-1---------3,3'-Dichlorobenzidine 800 u
56-55-3---------Benzo(a)Anthracene 920
218-01-9----~---Chrysene 1300
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 66 J
117-84-0--------Di-n-Octyl Phthalate 190 J
205-99-2--------Benzo(b)Fluoranthene 2200 X
207-08-9--------Benzo(k)Fluoranthene 2200 X
50-32-8---------Benzo(a)Pyrene 2100
193-39-5--------Indeno(l,2,3-cd)Pyrene 730
53-70-3---------Dibenzo(a,h)Anthracene 240 J
191-24-2--------Benzo(g,h,i)Perylene 1000
(1) -cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SBll-1-l
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
-Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30.1 (g/mL) ~
Level: (low/med) LOW
% Moisture: not dee • .......11
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_
dee.
~
pH: ~
SAS No.: S DG No . : ..,9.:,4c___
Lab Sample ID: ~3~6~2.:,4~8~7 ___ _
Lab File ID: GJ062487A08
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/31/90
Dilution Factor: ~i~·~o'---
Number TICS found: .....2..2. CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ---======--=--====----=====-======== ~=========== ===== 1. ALDOL 6.77 2400 ABJ 2. ALDOL 7.23 1900 AJ 3. UNKNOWN 7.97 810 J
4. ETHYLNAPHTHALENE 11.55 930 J 5. METHYLANTHRACENE & UNKNOWN 15.04 810 J 6. DIMETHYLNAPHTHALENE 16.24 1300 J 7. UNKNOWN HYDROCARBON 16.75 1400 J 8. 243-17-4 llH-BENZO[BJFLUORENE 16.89 1500 J 9. METHYLPYRENE 16.99 850 J 10. METHYLPYRENE 17.07 1500 J 11. UNKNOWN HYDROCARBON 17.25 3800 J 12. UNKNOWN HYDROCARBON 17.79 2000 J 13. BENZONAPHTHOTHIOPHENE 17.90 1100 J 14. UNKNOWN PAH 18.00 850 J 15. UNKNOWN 18.67 3100 J 16. UNKNOWN HYDROCARBON 19.10 4900 J 17. UNKNOWN HYDROCARBON 19.94 5700 J 18. UNKNOWN PHTHALATE 20.25 2300 J
19. UNKNOWN PHTHALATE 20.37 1700 J
20. UNKNOWN PHTHALATE 20.54 2500 J 21. UNKNOWN HYDROCARBON 20.94 890 J
22. UNKNOWN HYDORCARBON 22.12 3200 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBll-2-1
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362488
Sample wt/vol: 30.0 (g/mL) l,___ Lab File ID: GJ062488B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _ll dee. Date Extracted: O!U08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) li._ pH:~ Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 400
lll-44-4--------bis(2-Chloroethyl)Ether 400
95-57-8---------2-Chlorophenol 400
541-73-1--------1,3-Dichlorobenzene 400
106-46-7--------1,4-Dichlorobenzene 400
100-51-6--------Benzyl Alcohol 400
95-50-1---------1,2-Dichlorobenzene-400
95-48-7---------2-Methylphenol 400
3963 8-32-9------bis ( 2-Chloroisopropyl) Eth_er_ 400
106-44-5--------4-Methylphenol 400
621-64-7--------N-Nitroso-Di-n-Propylamine __ 400
67-72-1---------Hexachloroethane 400
98-95-3---------Nitrobenzene 400
78-59-1---------Isophorone 400
88-75-5---------2-Nitrophenol 400
105-67-9--------2,4-Dimethylphenol 400
65-85-0---------Benzoic Acid 2000
lll-91-l--------bis(2-Chloroethoxy)Methane __ 400
120-83-2--------2,4-Dichlorophenol 400
120-s2-1--------l,2,4-Trichlorobenzene 400
91-20-3---------Naphthalene 130
106-47-8--------4-Chloroaniline 400
87-68-3---------Hexachlorobutadiene 400
59-50-7---------4-Chloro-3-Methylphenol 400
91-57-6---------2-Methylnaphthalene 250
77-47-4---------Hexachlorocyclopentadiene __ 400
88-06-2---------2,4,6-Trichlorophenol 400
95-95-4---------2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 400
88-74-4---------2-Nitroaniline 2000
131-11-3--------Dimethyl Phthalate 400
208-96-8---~----Acenaphthylene 320
606-20-2--------2,6-Dinitrotoluene 400
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FORM I SV-'l 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
Q
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBll-2-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362488
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GJ062488Bl5
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ___llt dee. Date Extracted: 08/0!;!/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li__
~
pH: -2..&.1
Date Analyzed: 08/25/90
Dilution Factor: .i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2000
83-32-9---------Acenaphthene ·-400
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 400
121-14-2--------2,4-Dinitrotoluene 400
84-66-2---------Diethylphthalate 400
7005-72-3-------4-Chlorophenyl-phenylether __ 400
86-73-7---------Fluorene 250
lOO-Ol-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000
86-30-6---------N-Nitrosodiphenylamine (l)_ 400
lOl-55-3--------4-Bromophenyl-phenylether __ 400
118-74-1--------Hexachlorobenzene 400
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthrene 630
120-12-1--------Anthracene 220
84-74-2---------Di-n-Butylphthalate 400
206-44-0--------Fluoranthene 240
129-00-0--------Pyrene 460
85-68-7---------Butylbenzylphthalate 400
91-94-1-----~---3,3'-Dichlorobenzidine 810
56-55-3---------Benzo(a)Anthracene 150
218-01-9--------Chrysene 220
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 400
117-84-0--------Di-n-octyl Phthalate 400
205-99-2--------Benzo(b)Fluor~nthene 190
207-08-9--------Benzo(k)Fluoranthene 240
50-32-8--------~Benzo(a)Pyrene 530
193-39-5--------Indeno(l,2,3-cd)Pyrene 300
53-70-3---------Dibenzo(a,h)Anthracene 100
191-24-2--------Benzo(g,h,i)Perylene 330
(1) -cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
{.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA.SAMPLE NO.
SBll-2-1
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30.0 (g/mL) Q.__
Level: (low/med) LOW
t Moisture: not dee. _ll dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_
~
pH: ~
Nwnber TICs found: _ll
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: ,,__9:,,.4 __
Lab S amp 1 e ID : ,,_3"'6.,.2 i4 8"'8"-----
Lab File ID: GJ062488Bl5
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/25/90
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q =============== =============-============== ======== ===-==:::====== ===== 1. UNKNOWN 5.83 320 J
2. ALDOL 6.00 1300 AJ
3. METHYLNAPHTHALENE 9.42 240 J
4. DIMETHYLNAPHTHALENE 10.20 530 J
5. UNKNOWN HYDROCARBON 11.10 240 J
6. UNKNOWN HYDROCARBON 12.90 240 J
7. UNKNOWN HYDROCARBON 13.44 280 J
8. UNKNOWN 13.54 240 J
9. UNKNOWN HYDROCARBON 13.95 410 J
10. UNKNOWN HYDROCARBON 14.44 610 J
11. UNKNOWN HYDROCARBON 14.92 1300 J
12. BENZOFLUORENE 15.09 280 J
13. UNKNOWN HYDROCARBON 15.37 2000 J
14. UNKNOWN HYDROCARBON 15.85 1800 J
15. UNKNOWN 16.19 280 J
16. UNKNOWN HYDROCARBON 16.99 1900 J
17. UNKNOWN 17.69 1900 J
18. UNKNOWN 17 .95 450 J
19. UNKNOWN 18.52 1800 J
20. UNKNOWN 19.50 1700 J
21. UNKNOWN 20.72 970 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DATA SUMMAR\' 1 3 l
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBll-2-2
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: ~62489
Sample wt/vol: 30.1 (g/mL) _G __ Lab File ID: GH062489B15
Level: (low/med) LOW Date Received: 08/04/90
t Moisture: not dee. __ll dee. Date Extracted: Q8/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: Q8/22/90
GPC Cleanup: · (Y/N) Ii_ pH: ~ Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 390
lll-44-4--------bis(2-Chloroethyl)Ether 390
95-57-8---------2-Chlorophenol 390
541-73-1--------1,3-Dichlorobenzene 390
106-46-7--------1,4-Dichlorobenzene 390
100-51-6--------Benzyl Alcohol 390
95-50-1---------1,2-oichlorobenzene 390
95-48-7---------2-Methylphenol 390
39638-32-9------bis(2-Chloroisopropyl)Ether_ 390
106-44-5--------4-Methylphenol 390
621-64-7--------N-Nitroso-Di-n-Propylamine __ 390
67-72-1---------Hexachloroethane 390
98-95-3---------Nitrobenzene 390
78-59-1---------Isophorone 390
88-75-5---------2-Nitrophenol 390
105-67-9--------2,4-Dimethylphenol 390
65-85-o---------Benzoic Acid 1900
111~91-l--------bis(2-Chloroethoxy)Methane __ 390
120-83-2--------2,4-Dichlorophenol 390
120-82-1--------1,2,4-Trichlorobenzene '. 390
91-20-3---------Naphthalene 51
106-47-8--------4-Chloroaniline 390
87-68-3---------Hexachlorobutadiene 390
59-50-7---------4-Chloro-3-Methylphenol 390
91-57-6---------2-Methylnaphthalene 160
77-47-4---------Hexachlorocyclopentadiene __ 390
88-06-2---------2,4,6-Trichlorophenol 390
95-95-4---------2,4,5-Trichlorophenol 1900
91-58-7---------2-Chloronaphthalene 390
88-74~4---------2-Nitroa~iline 1900
131-11-3--------Dimethyl Phthalate 390
208-96-8--------Acenaphthylene 180
606-20-2--------2,6-Dinitrotoluene 390
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DATA SUMMAR\'
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
SBll-2-2
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362489
Sample wt/vol: 30.l (g/mL) ~ Lab File ID: GH062489B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _ll dee. Date Extracted: 08/08/90
Extraction: ( SepF / Cont/ Sonc) Date Analyzed: 08/22/90
GPC Cleanup:_ (Y/N) lL_ pH: ~ Dilution Factor: .,l'--'-"-"o'----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1900 u
83-32-9---------Acenaphthene 390 u
51-28-5---------2,4-Dinitrophenol 1900 u
100-02-7--------4-Nitrophenol 1900 u
132-64-9--------Dibenzofuran 390 u
121-14-2--------2,4-Dinitrotoluene 390 u
84-66-2---------Diethylphthalate 390 u
7005~72-3-------4-Chlorophenyl-phenylether __ 390 u
86-73-7------;..--Fluorene 190 J
100-0l-6•-------4-Nitroaniline 1900 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900 u
86-30-6--;..--:--:.-N-Nitrosodiphenylamine (1) __ 390 u
101-55-3--------4-Bromophenyl-phenylether __ 390 u
118-74-1--------Hexachlorobenzene 390 u
87-86-5---------Pentachlorophenol 1900 u
85-01-8---------Phenanthrene 480
120-12-7--------Anthracene 140 J
84-74-2---------oi-n-Butylphthalate 390 u
206-44-0--------Fluoranthene 210 J
129-oo~o--------Pyrene 420
85-68-7---------Butylbenzylphthalate 390 u
91-94-1---------3,3'-Dichlorobenzidine 780 u
56-55-3---------Benzo(a)Anthracene 120 J
218-01-9--------Chrysene 170 J
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 53 J
117-84-0--------oi-n-octyl Phthalate 390 u
205-99-2--------Benzo(b)Fluoranthene 86 J
207-08-9--------Benzo(k)Fluoranthene 190 J
50-32-8---------Benzo(a)Pyrene 280 J
193-39-5--------Indeno(l,2,3-cd)Pyrene 390 u
53-70-3---------Dibenzo(a,h)Anthracene 390 u
191-24-2--------Benzo(g,h,i)Perylene 390 u
(1) -Cannot be separated from D1phenylam1ne
FORM I SV-2 _ 1/87 Rev.
20937 94 SAMPLE DATA SllMMARY
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SBll-2-2
No.: 94
362489
Sample wt/vol: 30,1 (g/mL) ~ Lab File ID: GH062489Bl5
Level: (low/med). LOW Date Received: 08/04/90
\ Moisture: not dee. -1§. dee. Date Extracted: Of.!.:'.08/90
Extraction:
Date Analyzed: 08,:'.22/90
GPC Cleanup:
( SepF /Cont/Sonc)
(Y/N) li.._ pH: ..i.,1 Dilution Factor: ~i~-~o __ _
Number TICs found: .....2.4
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG
RT EST. CONC. Q ===========-==== =========================== ======== =-=========== ===== 1. 3178-29-8 HEPTANE, 4-PROPYL-5.10 160 J 2. UNKNOWN 5.82 790 J 3. ALOOL 6.00 1100 AJ 4. ALOOL 6.42 240 AJ 5. UNKNOWN 6.67 590 J 6. UNKNOWN HYDROCARBON 13.42 360 .J 7. UNKNOWN HYDROCARBON 13.94 280 J 8 . 74764-11-7 IRON, TRICARBONYL.(N-(PHENYL-14.44 470 J 9. 74764-11-7 IRON, TRICARBONYL(N-(PHENYL-14.90 710 J 10. UNKNOWN PAH 15.09 200 J 11. UNKNOWN 15.37 1200 J 12. UNKNOWN PAH 15.42 160 J 13. 630-06-8 HEXATRIACONTANE 15.85 1100 J 14. UNKNOWN HYDROCARBON 16.39 1500 J 15. 74764-11-7 IRON, TRICARBONYL(N-(PHENYL-16.99 1100 J 16. UNKNOWN HYDROCARBON 17.69 1200 J 17. UNKNOWN PHTHALATE 17.95 280 J 18. UNKNOWN PHTHALATE 18.17 320 J 19. UNKNOWN PHTHALATE 18.29 320 J 20. UNKNOWN PHTHALATE 18.40 400 J 21. UNKNOWN 18.52 1100 J 22. UNKNOWN 19.52 950 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DQTA SUMMARY .. 'IWLP •• 1 .-, -
...::. '
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1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET_
Lab Name: COMPUCHEM,RTP Contract: (2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
SB15-l-l
No.: 94 I Matrix: (soil/water) SOIL Lab Sample ID: 362482
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Sample wt/vol: 30.0 (g/mL) .G._ Lab File ID: !,,;!062482B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee.___§. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc)
(Y/N) li_ ·
~
pH: ....JL..l
Date Analyzed: 08/25/90
GPC Cleanup: Dilution Factor: £1~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG
108-95-2--------Phenol
2100 lll-44-4--------bis(2-Chloroethyl)Ether
180 95-57-8---------2-Chlorophenol
1700 541-73-1--------1,3-Dichlorobenzene
350 106-46-7--------1,4-Dichlorobenzene
350 100-51-6--------Benzyl Alcohol 350 95-50~1---------1,2-Dichlorobenzene
350 95-48-7~--------2-Methylphenol
350 39638-32-9------bis(2-Chloroisopropyl)Ether_
350 106-44-5--------4-Methylphenol
2200 621-64-7--------N-Nitroso-Di-n-Propylamine __ 350 67-72-1---------Hexachloroethane
350 98-95-3---------Nitrobenzene
350 78-59-1---------Isophorone
1000 88-75-5---------2-Nitrophenol
350 105-67-9--------2,4-Dimethylphenol
350 65-85-o---------Benzoic Acid 170_0 lll-91-l--------bis(2-Chloroethoxy)Methane
350 120-83-2--------2,4-Dichlorophenol --350 120-a2-1--------1,2,4-Trichlorobenzene
350 91-20-3---------Naphthalene
350 106-47-8----~---4-Chloroaniline
350 87-68-3---------Hexachlorobutadiene
350 59-50-7--------~4-Chloro-3-Methylphenol
350 91-57-6---------2-Methylnaphthalene
350. 77-47-4---------Hexachlorocyclopentadiene __ 350 88-06-2---------2,4,6-Trichlorophenol
350 95-95-4---------2,4,5-Trichlorophenol
1700 91-58-7---------2-Chloronaphthalene
350 88-74-4---------2-Nitroaniline
1700 131-11-3--------Dimethyl Phthalate 350 208-96-8--------Acenaphthylene
350 606-20-2--------2,6-Dinitrotoluene
350
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FORM I SV-1 1/87 Rev.
SR/'IF'LE DQTR SU/'1/'IRR 'r' ~ •• □:I OMWI .. 126
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
SB15-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: ( soil/water) SOIL Lab Sample ID: 362482
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GJ062482B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ___§ dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) .5.0liC Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) li,_ pH: .....9...l Dilution Factor: ~l~-~o~o __
CAS NO.· COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
.
99-09-2---------3-Nitroaniline 1700
83-32-9---------Acenaphthene 600
51-28-5---------2,4-Dinitrophenol 1700
100-02-7--------4-Nitrophenol 1700
132-64-9--------Dibenzofuran 350
121-14-2----~---2 4-Dinitrotoluene 350 , .
84-66-2---------Diethylphthalate 350
7005-72-3-------4-Chlorophenyl-phenylether __ 350
86-73-7---------Fluorene 350
100-01-6--------4-Nitroaniline 1700
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1700
86-30-6---------N-Nitrosodiphenylamine (1)_ 350
101-55-3--------4-Bromophenyl-phenylether __ 350
118-74-1--------Hexachlorobenzene 350
87-86-5---------Pentachlorophenol 520
85-01-8---------Phenanthrene 1100
120-12-7;-------Anthracene 350
84-74-2---------Di-n-Butylphthalate 350
206-44-0--------Fluoranthene 350
129-0o-o--------Pyrene 1100
85-68-7---------Butylbenzylphthalate 350
91-94-1---------3,3'-Dichlorobenzidine 700
56-55-3---------Benzo(a)Anthracene 350
218-01-9--------Chrysene 350
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 350
117-84-0--------Di-n-octyl Phthalate 350
205-99-2--------Benzo(b)Fluoranthene 1100
207-08-9--------Benzo(k)Fluoranthene 350
50-32-8---------Benzo(a)Pyrene 350
193-39-5--------Indeno(l,2,3-cd)Pyrene .350
53-70-3---------Dibenzo(a,h)Anthracene 350
191-24-2--------Benzo(g,h,i)Perylene 870
(1) -Cannot be separated from D1phenylam1ne
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FORM I SV-2 1/87 Rev.
.... ,., Q -..,. ...::. 0.,. .j .. 94
Q
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
SB15-l-l
No.: 94
362482
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GJ062482B15
Level: (low/med) !PW
\ Moisture:
Extraction:
GPC Cleanup:
not dee. __§
(SepF/Cont/Sonc)
(Y/N) H.,_
Nwnber TICS found: _..1
dee.
~
pH: ..JL...l
CAS NUMBER COMPOUND NAME
Date Received: 08/04/90
Date Extracted: 08/08/20
Date Analyzed: 08/25/90
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q =======--====== ============================ ======== ============= ===== 1. UNKNOWN HYDROCARBON 5.08 250 J
2. UNKNOWN 8.02 2300 J
3. UNKNOWN PHTHALATE 12.87 780 J
FORM I SV-TIC 1/87 Rev.
SAMPL~ D~TA SUMMARY 1 .... -·_ .:..-
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB16-l-l
Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/wa~er) SOIL Lab Sample ID: 362481
Sample wt/vol: 30.2 (g/mL) !a.__ Lab File ID: GJ062481B15
Level: (low/med) LOW Date Received: 08/04/90
t Moisture: not dee. __.l..Q dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc)
(Y/N) li._
~
pH: --8....9.
Date Analyzed: 08/25/90
GPC Cleanup: Dilution Factor: ~i~-=o=o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 360
lll-44-4--------bis(2-Chloroethyl)Ether 360
95-57-8---------2~Chlorophenol 360
541-73-1--------1,3-Dichlorobenzene 360
106-46-7--------1,4-Dichlorobenzene 360
100-51-6--------Benzyl Alcohol 360
95-50-1---------1,2-Dichlorobenzene 360
95-48-7---------2-Methylphenol 360
39638-32-9---.---bis (2-Chloroisopropyl) Ether_ 360
106-44-5--------4-Methylphenol 360
621-64-7--------N-Nitroso-Di-n-Propylamine __ · 360
67-72-1---------Hexachloroethane 360
98-95-3--~------Nitrobenzene 360
78-59-1---------Isophorone 360
88-75-5---------2-Nitrophenol 360
105-67-9--------2,4-Dimethylphenol ' 360
65-85-o---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane __ 360
120-83-2--------2,4-Dichlorophenol 360
120-82-1--------1,2,4-Trichlorobenzene 360
91-20-3---------Naphthalene 360
106-47-8--------4-Chloroaniline 360
87-68-3---------Hexachlorobutadiene 360
59-50-7---------4-Chloro-3-Methylphenol 360
91-57-6---~-----2-Methylnaphthalene 360
77-47-4---------Hexachlorocyclopentadiene __ 360
88-06-2---------2,4,6-Trichlorophenol 360
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 360
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 360
208-96-8--------Acenaphthylene 360
606-20-2--------2,6-Dinitrotoluene 360
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DATA SUMMARV
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB16-l-l
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362481
sample wt/vol: 30. 2 (g/mL) _G_ Lab File ID: GJ062481B15
Level: (low/med) ~LO,=W __ Date Received: 08/04/90
% Moisture: not dee. _ll dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) S_Qli£ Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) li,__ pH:~ Dilution Factor: .i~-~o~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 1800 u
83-32~9---------Acenaphthene 360 u
51-28-5---------2,4-Dinitrophenol 1800 u
100-02-7--------4-Nitrophenol 1800 u
132-64-9--------Dibenzofuran 360 u
121-14-2--------2,4-Dinitrotoluene 360 u
84-66-2---------Diethylphthalate 360 u
7005-72-3-------4-Chlorophenyl-phenylether_ 360 u
86-73-7---------Fluorene 360 u
100-01-6--------4-Nitroaniline 1800 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 360 u
101-55-3--------4-Bromophenyl-phenylether __ 360 u
118-74-1--------Hexachlorobenzene 360' u
87-86-5---------Pentachlorophenol 1800 u
85-01-8---------Phenanthrene 360 u
120-12-7--------Anthracene 360 u
84-74-2---------Di-n-Butylphthalate 360 u
206-44-0--------Fluoranthene 360 u
129-00-0--------Pyrene 360 u
85-68-7---------Butylbenzylphthalate 360 u
91-94-1---------3,3'-Dichlorobenzidine 730 u
56-55-3---------Benzo(a)Anthracene 360 u
218-01-9--------Chrysene 360 u
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 79 J
117-84-0--------Di-n-octyl Phthalate 360 u
205-99-2--------Benzo(b)Fluoranthene 360 u
207-08-9--------Benzo(k)Fluoranthene 360 u
50-32-8---------Benzo(a)Pyrene 360 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 360 u
53-70-3---------Dibenzo(a,h)Anthracene 360 u
191-24-2--------Benzo(g,h,i)Perylene 360 u
(1) -Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
20937 94 SAMPLE DATA SUMt1ARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNbs
EPA SAMPLE NO.
SB16-l-l Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30.2 (g/mL) L-
Level: (low/med) LOW
% Moisture: not dee. _l.Q dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) .IL_
SONC
pH: -8...,_2
Number TICs found: ___l
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: =9~4 __
Lab Sample ID: ~3~6~2~4~8~1~---
Lab File ID: GJ062481B15
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/25/90
Dilution Factor: 1.00
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ==========::;;:;::::==== ============================ =::======= ============= ===== 1. UNKNOWN HYDROCARBON 5.08 180 J 2. UNKNOWN 14.99 220 J 3. UNKNOWN 15.39 220 J
FORM I SV-TIC 1/87 Rev.
20937 SAtlPGE [~TA SUMMAR\'
~ 121
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAM?LE NO.
SB7-l-l
Lab Name: COMPUCHEM.R~P Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No. : 94
Matrix: (soil/water) SOIL Lab Sample IO: 362483
Sample wt/vol: 30.2 ( g/mL) _G_ Lab File ID:
' \ G0062483B15
Level: ( low/med) LOW Date Received: 08/04/90
% Moisture: not dee. --2...Q dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) li...._ pH: ~ Dilution Factor: ~3~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS: .
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 3000
lll-44-4--------bis(2-Chloroethyl)Ether 1200
95-57-8---------2-Chlorophenol 1200
541-73-1--------1,3-Dichlorobenzene 1200
106-46-7--------1,4-0ichlorobenzene 1200
·100-51-6----~---Benzyl Alcohol 1200
95-50-1---------1,2-Dichlorobenzene 1200
95-48-7---------2-Methylphenol 1200
39638-32-9------bis(2~chloroisopropyl)Ether_ 1200
106-44-5--------4-Methylphenol 1200
621-64-7--------N-Nitroso-Di-n-Propylamine 1200 -67-72-1---------Hexachloroethane 1200
98-95-3---------Nitrobenzene 1200
78-59-1---------Isophorone 1200
88-75~5---------2-Nitrophenol 1200
105-67-9--------2,4-Dimethylphenol 1200
65-85-0---------Benzoic Acid . 6000
lll-91-l--------bis(2-Chloroethoxy)Methane __ 1200
120-83-2--------2,4~Dichlorophenol 1200
120-82-1--------1,2,4-Trichlorobenzene 1200
91-20-3---------Naphthalene 9600
106-47-8--------4-Chloroaniline 1200
87-68-3---------Hexachlorobutadiene 1200
59-50-7---------4-Chloro-3-Methylphenol 1200
91-57-6---------2-Methylnaphthalene 19000
77-47-4---------Hexachlorocyclopentadiene 1200
88-06-2---------2,4,6-Trichlorophenol --1200
95-95-4---------2,4,5-Trichlorophenol 6000
91-58-7---------2-Chloronaphthalene 1200
88-74-4---------2-Nitroaniline 6000
131-11-3-----,---Dimethyl Phthalate 1200
208-96-8--------Acenaphthylene 1200
606-20-2--------2,6-Dinitrotoluene 1200
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FORM I SV-1 1/87 Rev.
20937 94 SArlPLE r~rA.SUMMAP\'
Q
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lC EPA SAMPLE t!O.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB7-l-l
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362483
Sample wt/vol: 30.2 ( g/mL) _G_ Lab File ID: GD062483B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. -..£2 dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) li_ pH: __!_,__2_ Dilution Factor: =3~-=o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 6000
83-32-9---------Acenaphthene 780
51-28-5---------2,4-Dinitrophenol 6000
100-02-7--------4-Nitrophenol 6000
132-64-9---~----Dibenzofuran 1200
121-14-2--------2,4-Dinitrotoluene 1200
84-66-2---------Diethylphthalate 1200
7005-72-3-------4-Chlorophenyl-phenylether __ 1200
86-73-7---------Fluorene 900
100-01-6--------4-Nitroaniline 6000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 6000
86-30-6---------N-Nitrosodiphenylamine (l)_ 1200
101-55-.3--------4-Bromophenyl-phenylether __ 1200
118-74-1--------Hexachlorobenzene 1200
87-86-5---------Pentachlorophenol 6000
85-01-8---------Phenanthrene 1900
120-12-7------~-Anthracene 150
84-74-2---------Di-n-Butylphthalate 180
206~44-0--------Fluoranthene 410
· 129-oo-o--------Pyrene 420
85-68-7---------Butylbenzylphthalate 1100
91-94-1----~----3,3'-Dichlorobenzidine 2500
56-55-3---------Benzo(a)Anthracene 260
218-01-9--------Chrysene 280
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 1200
117-84-0--------Di-n-Octyl Phthalate 1200
205-99-2~-------Benzo(b)Fluoranthene 270
207-08-9--------Benzo(k)Fluoranthene 230
50-32-8---------Benzo(a)Pyrene 160
193-39-5--------Indeno(l,2,3-cd)Pyrene 1200
53-70-3---------Dibenzo(a,h)Anthracene 1200
191-24-2--------Benzo(g,h,i)Perylene 1200
(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
20937 94 SAMPLE pqrA SUMMARY
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.R1P Contract: /2-881-REVS
SB7-l-l
Lab Code: COMPU Case No.: 20937 SAS No.: ----SDG No.: "'-9.,_4 __
Matrix: (soil/water) SOIL
Sample wt/vol: 30. 2 (g/mL) _G_
Level: ( low/med) LOW
% Moisture: not dee. _lQ
Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) !L_
dee.
SONC
pH: ___!_,_a.
Lab S amp 1 e ID : ,,_3:,,.6..._2 :,_4 8><.c3,,__ __ _
Lab File ID: . GD062483Bl5
Date Received: 08/04/90
Date Extracted: 08/08/90
Date Analyzed: 08/25/90
Dilution Factor: ~3~-~o __ _
Number TICs found: --2..Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ==============--============ =======-:::::: ====--:;;;:;====== =:;;::::===
1. 124-18-5 DECANE 6.45 20000 J
2. UNKNOWN HYDROCARBON 6.67 20000 J 3. ETHYLMETHYLBENZENE 6.82 27000 J
4. UNKNOWN 7.02 27000 J
5. UNKNOWN 7.32 20000 J
6. HYDROCARBON+UNKNOWN 7.38 30000 J 7. UNKNOWN HYDROCARBON 8.25 37000 J
8. UNKNOWN CYCLIC HYDROCARBON 8.59 17000 J
9. UNKNOWN 8.65 20000 J
10. UNKNOWN HYDROCARBON 8.82 29000 J
11. UNKNOWN HYDROCARBON 9.04 31000 J
12. METHYLNAPHTHALENE 9.44 16000 J
13. UNKNOWN HYDROCARBON 9.60 19000 J
14. UNKNOWN HYDROCARBON 9.,77 32000 J
15. UNKNOWN HYDROCARBON 10.20 24000 J
16. UNKNOWN HYDROCARBON 10.47 25000 J
17. UNKNOWN HYDROCARBON 11.12 22000 J
18. UNKNOWN HYDROCARBON 11. 75 34000 J
19. UNKNOWN HYDROCARBON 12.34 24000 J
20. UNKNOWN HYDROCARBON 12.90 20000 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY 1 1 :;·
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1B EPA SAMPLE t/0.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB7-2-l
Lab Name: COMPUCHEM.R'l'P contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .,,_9_:,c4 __
Matrix: (soil/water) SOIL Lab Sample ID: :3~5~2~4~8~4'------
Sample wt/vol: 30.1 (g/mL) _G __ Lab File ID: GD062484B15
Level: ( low/med) LOW Date Received: 08/04/90
% Moisture: not dee. _____u dee. Date Extracted: 08/08/90
Extraction: (SepF /Cont/Sane) SONC Date Analyzed: 08/25/90
Dilution Factor: ~1~0--~ GPC Cleanup: (Y/N) H_ pH: __L_§_
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1800
lll-44-4--------bis(2-Chloroethyl)Ether 4200
95-57-8---------2-Chlorophenol 4200
541-73-1--------1,3-Dichlorobenzene 4200
106-46-7--------1,4-Dichlorobenzene 4200
100-51-6--------Benzyl Alcohol 4200
95-50-1---------1,2-Dichlorobenzene 4200
95-48-7---------2-Methylphenol 4200
39638-32-9------bis(2-Chloroisopropyl)Ether_ 4200
106-44-5--------4-Methylphenol 4200
621-64-7--------N-Nitroso-Di-n-Propylamine __ 4200
67-72-1---------Hexachloroethane 4200
98-95-3---------Nitrobenzene 4200
78-59-1---------Isophorone 4200
88-75-5---------2-Nitrophenol 4200
105-67-9--------2,4-Dimethylphenol 4200
65-85-0---------Benzoic Acid 20000
lll-91-l--------bis(2-Chloroethoxy)Methane __ 4200
120-83-2--------2,4-Dichlorophenol 4200
120-82-1--------1,2,4-Trichlorobenzene 4200
91-20-3---------Naphthalene 22000
106-47-8--------4-Chloroaniline 4200
87-68-3---------Hexachlorobutadiene 4200
59-50-7---------4-Chloro-3-Methylphenol 4200
91-57-6---------2-Methylnaphthalene 43000
77-47-4---------Hexachlorocyclopentadiene __ 4200
88-06-2---------2,4,6-Trichlorophenol 4200
95-95-4-----~---2,4,5-Trichlorophenol 20000
91-58-7---------2-Chloronaphthalene 4200
88-74-4---------2-Nitroaniline 20000
131-11-3--------Dimethyl Phthalate 4200
208-96-8--------Acenaphthylene 4200
606-20-2--------2,6-Dinitrotoluene 4200
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY
Q
1 1 ,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB7-2-l Lab Name: COMPUCHEM.RTP Contract: /2-88}-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ____ SDG No.: ~9..,_4 __
Matrix: (soil/water) SOIL Lab Sample ID: ~3~6~2~4~8~4c.._ __ _
Sample wt/vol: 30.1 (g/mL) _G __ Lab File ID: GD062484B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. -----11. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 08/25/90
GPC Cleanup: (Y/N) !:L_ pH: _±__,_§_ Dilution Factor: ~1~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline .... 20000
83-32-9---------Acenaphthene 1600
51-28-5---------2,4-Dinitrophenol 20000
100-02-7--------4-Nitrophenol 20000
132-64-9--------Dibenzofuran 1500
121~14-2--------2,4-Dinitrotoluene 4200
84-66-2---------Diethylphthalate 4200
7005-72-3-------4-Chlorophenyl-phenylether __ 4200
86-73-7---------Fluorene 1400
100-01-6--------4-Nitroaniline 20000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 20000
86-30-6---------N-Nitrosodiphenylamine (l) __ 4200
101-55-3--------4~Bromophenyl-phenylether __ 4200
118-74-1--------Hexachlorobenzene 4200
87-86-5---------Pentachlorophenol 20000
85-01-8---------Phenanthrene 47.00
120-12-7--------Anthracene 4200
84-74-2---------Di-n-Butylphthalate 4200
206-44-0--------Fluoranthene 1300
129-00-0--------Pyrene 1400
85-68-7----~----Butylbenzylphthalate 4200
91-94-1---------3,3'-Dichlorobenzidine 8400
56-55-3---------Benzo(a)Anthracene 4200
218-01-9--------Chrysene 490
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 440
117-84-0--------Di-n-Octyl Phthalate 4200
205-99-2--------Benzo(b)Fluoranthene 4200
207-08-9--------Benzo(k)Fluoranthene 4200
50-32-8---------Benzo(a)Pyrene 4200
193-39-5--------Indeno(l,2,3-cd)Pyrene 4200
53-70-3---------Dibenzo(a,h)Anthracene 4200
191-24-2--------Benzo(g,h,i)Perylene 4200
(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
20937 94 SAMPtE DATA SUMMARY
Q
1 1 r:
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM RTP Contract: /2-88)-REVS
SB7:-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ·94
Matrix: (soil/water) SOIL Lab Sample ID: 362484
Sample wt/vol: 30.1 (g/mL) _G_ Lab File ID: GD062484Bl5
Level: (low/med) LOW
% Moisture: not dee. ___n_ dee.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) li...._ pH: __!_,__§_
Number TICs found: _1.Q
CAS NUMBER COMPOUND NAME =========-======
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
08/04/90
08/08/90
0805/90
10
CONC. Q ============================ ======== ==--::;;:======== ====:::; 1. 124-18-5 DECANE 6.45 68000 J 2. UNKNOWN HYDROCARBON 6.67 68000 J 3. UNKNOWN 7,02 77000 J 4. HYDROCARBON & UNKNOWN 7.12 47000 J 5. UNKNOWN 7,32 68000 J 6. UNKNOWN HYDROCARBON 7.38 110000 J 7. UNKNOWN HYDROCARBON 7.85 51000 J 8. UNKNOWN HYDROCARBON 8.23 130000 J 9. UNKNOWN 8.59 55000 J 10. UNKNOWN 8.65 64000 J 11. UNKNOWN HYDROCARBON 8.82 64000 J 12. UNKNOWN HYDROCARBON 9.04 85000 J 13. METHYLNAPHTHALENE 9.44 41000 J 14. UNKNOWN HYDROCARBON 9.60 47000 J 15. UNKNOWN HYDROCARBON 9.77 81000 J 16. UNKNOWN HYDROCARBON 10.20 64000 J 17. UNKNOWN HYDROCARBON 10.47 60000 J 18. UNKNOWN HYDROCARBON 11.12 60000 J
19. UNKNOWN HYDROCARBON 11. 75 55000 J
20. UNKNOWN HYDROCARBON 12.34 40000 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY 1 1 .:
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-88l-REVS
SBS-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361455
Sample wt/vol: 30.4 (g/mL) _G_ Lab File ID: GJ061455A08
Level: (low/med) LOW Date Received: 08/02/90
% Moisture: not dee. --2.Q dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) l:!._ pH: ---hl Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 410 u
lll-44-4--------bis(2-Chloroethyl)Ether 410 u
95-57-8---------2-Chlorophenol 410 u
541-73-1--------1,3-Dichlorobenzene 410 u
106-46-7--------1,4-Dichlorobenzene 410 u
100-51-6--------Benzyl Alcohol 410 u
95-50-1---------1,2-Dichlorobenzene 410 u
95-48-7---------2-Methylphenol 410 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u
106-44-5--------4-Methylphenol 410 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 410 u
67-72-1---------Hexachloroethane 410 u
98-95-3---------Nitrobenzene 410 u
78-59-1---------Isophorone 410 u
88-75-5---------2-Nitrophenol 410 u
105-67-9--------2, 4-Dim·ethylphenol 410 u
65-85-0---------Benzoic Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ 410 u
120~83-2--------2,4-Dichlorophenol 410 u
120-s2-1--------l,2,4-Trichlorobenzene 410 u
91-20-3---------Naphthalene 410 u
106-47-8--------4-Chloroaniline 410 u
87-68-3---------Hexachlorobutadiene 410 u
59-50-7---------4-Chloro-3-Methylphenol 410 u
91-57-6---------2-Methylnaphthalene 410 u
77-47-4---------Hexachlorocyclopentadiene __ 410 u
88-06-2---------2,4,6-Trichlorophenol 410 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 410 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 410 u
208-96-8--------Acenaphthylene 410 u
606-20-2--------2,6-Dinitrotoluene 410 u
FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DATA SUMMARY 1 1 •
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
. SB8-l-l Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361455
Sample wt/vol: 30.4 (g/mL) _G __ Lab File ID: GJ061455A08
Level: ( low/med) rpw Date Received: 08/02/90
% Moist\,\re: not dee. _.lQ dee. Date Extracted: Q8/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) li.._ pH: ...i...3. Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2000
83-32-9---------Acenaphthene 410
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 410
121-14-2---~----2,4-Dinitrotoluene 410
8~-66-2---------Diethylphthalate 410
7005-72-3-------4-Chlorophenyl-phenylether __ 410
86-73-7---------Fluorene 410
100-01-6-----~--4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-M~thylphenol __ 2000
86-30-6--~------N-Nitrosodiphenylamine (l) __ 410
101-55-3--------4-Bromophenyl-phenylether __ 410
118-74-1--------Hexachlorobenzene 410
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthren_e 410
120-12-7--------Anthracene 410
84-74-2---------Di-n-Butylphthalate 410
206-44-0--------Fluoranthene 410
129-00-0--------Pyrene 410
85-68-7---------Butylbenzylphthalate 410
91-94-1---------3,3'-Dichlorobenzidine 810
56-55-3---------Benzo(a)Anthracene 410
218-01-9--------Chrysene 410
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 360
117-84-0--------Di-n-Octyl Phthalate 460
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 410
50-32-8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,3-cd)Pyrene 410
53-70-3---------Dibenzo(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
20937 94 SAMPLE DATA SUMMAR\'
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG
Matrix: (soil/water) SOIL Lab Sample IO:
Sample wt/vol: 30.4 (g/mL) lL;_ Lab File IO:
Level: (low/med) rpw Date· Received:
t Moisture: not dee. ___lQ dee. Date Extracted:
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed:
EPA SAMPLE NO.
SB8-l-l
No. : 94
361455
GJ061455A08
08/02/90
08/08/90
081io190
GPC Cleanup: (Y/NJ Ji._ pH: ..i,_]_ Dilution Factor: ~l~-~o __ _
CONCENTRATION UNITS:
Number TICs found: ...l.l (ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ============================ ======== --=========== ===== l. ALOOL 6.65 1800 ABJ 2. 544-76-3 HEXAOECANE 12.39 5800 J 3. 629-78-7 HEPTAOECANE 13.07 14000 J
4. OIMETHYLHEPTAOECANE 13.72 7800 J
5. UNKNOWN 14.25 4500 J
6. OIMETHYLHEPTAOECANE 14.34 6600 J 7. UNKNOWN 16.02 3200 J
8. UNKNOWN HYDROCARBON 16.72 4500 J 9. UNKNOWN 16.85 3200 J
10. UNKNOWN HYDROCARBON 17.04 7800 J
11. UNKNOWN HYDROCARBON 17.20 6200 J
12. UNKNOWN 17.35 4100 J
13. UNKNOWN HYDROCARBON 17.55 7000 J
14. UNKNOWN HYDROCARBON 17.77 4900 J 15. UNKNOWN HYDROCARBON 18.17 4500 J
16. UNKNOWN HYDROCARBON 18.39 7000 J 17. UNKNOWN HYDROCARBON 18.52 4500 J
18. UNKNOWN 18.69 3900 J
19. UNKNOWN HYDROCARBON .19.14 7800 J
20. PHTHALATE + UNKNOWN 20.00 4500 J
21. PHTHALATE + UNKNOWN 20.24 4000 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE DQTA SUMMARY
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB8-l-1RE Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No. : SDG No. : 94
Matrix: (soil/water) SOIL Lab Sample ID: 361455,
Sample wt/vol: 30.4
LOW
(g/mL) L_ Lab File ID: G2J61455A08
Level: ( low/med) Date Received: 08/02/90
% Moisture: not dee. _.z.Q dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/20/90
GPC Cleanup: . (Y/N) li_ pH: ....2...1 Dilution Factor: ~i~-~o'----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 410
lll-44-4--------bis(2-Chloroethyl)Ether 410
95-57-8---------2-Chlorophenol 410
541-73-1--------1,3-Dichlorobenzene 410
106-46-7--------1,4-Dichlorobenzene 410
100-51-6--------Benzyl Alcohol 410
95-50-1---------1,2-Dichlorobenzene 410
95-48-7---------2-Methylphenol 410
39638-32-9------bis(2-Chloroisopropyl)Ether_ 410
106-44-5--------4-Methylphenol 410
621-64-7--------N-Nitroso-Di-n-Propylamine __ 410
67-72-1~--------Hexachloroethane 410
98-95-3---------Nitrobenzene 410
78-59-1---------Isophorone 410
88-75-5---------2-Nitrophenol 410
105-67-9--------2,4-Dimethylphenol 410
65-85-0---------Benzoic Acid 20.00
lll-9l-l--------bis(2-Chloroethoxy)Methane __ 410
120-83-2--------2,4-Dichlorophenol 410
120-82-1--------1,2,4-Trichlorobenzene 410
91-20-3---------Naphthalene 410
106-47-8---~----4-Chloroaniline 410
87-68-3---------Hexachlorobutadiene 410
59-50-7---------4-Chloro-3-Methylphenol 410
91-57-6---------2-Methylnaphthalene 410
77-47-4---------Hexachlorocyclopentadiene __ 410
88-06-2---------2,4,6-Trichlorophenol 410
95-95-4-~-------2,4,5-Trichlorophenol 2000
91-58-7---------2-Chloronaphthalene 410
88-74-4---------2-Nitroaniline 2000
131-11-3--------Dimethyl Phthalate 410
208-96-8--------Acenaphthylene 410
606-20-2--------2,6-Dinitrotoluene 410
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FORM I SV-1 1/87 Rev.
20937 94 -' SAMPlE DATA SUMMAR\'
i -~
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: /2-881-REVS
SB8-l-1RE
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ... 9..:,4 __
Lab Sample ID: ~3~6~1~4~5~5'----Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL) ~ Lab.File ID: G2J61455A08
Level: ( low/med) LOW Date Received: 08/02/90
% Moisture: not dee. ___.l..Q dee. Date Extracted: 08/08/90
Date Analyzed: 08/20/90 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) .tL_ pH: ....2.....3. Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2000 u
83-32-9---------Acenaphthene 410 u
51-28-5---------2,4-Dinitrophenol 2000 u
100-02-7--------4-Nitrophenol 2000 u
132-64-9--------Dibenzofuran 410 u
121-14-2----~---2,4-Dinitrotoluene 410 u
84-66-2---------Diethylphthalate 410 u
7005-72-3-------4-Chlorophenyl-phenylether __ 410 u
86-73-7---------Fluorene 410 u
lOO-Ol-6~-------4-Nitroaniline 2000 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 410 u
101-55-3--------4-Bromophenyl-phenylether __ 410 u
118-74-1--------Hexachlorobenzene 410 u
87-86-5---------Pentachlorophenol 2000 u
85-01-8---------Phenanthrene 410 u
120-12-7--------Anthracene 410 u
84-74-2---------Di-n-Butylphthalate 49 J
206-44-0--------Fluoranthene 410 u
129-00-0--------Pyrene 410 u
85-68-7---------Butylbenzylphthalate 410 u
91-94-1---------3 3'-Dichlorobenzidine 810 u . . . 56-55-3-----~---Benzo(a)Anthracene 410 u
218-01-9--------Chrysene 410 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 340 J
117-84-0--------Di-n-Octyl Phthalate 440
205-99-2--------Benzo(b)Fluoranthene 410 u
207-08-9--------Benzo(k)Fluoranthene 410 u
50-32-8---------Benzo(a)Pyrene 410 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 410 u
53-70-3---------Dibenzo(a,h)Anthracene 410 u
191-24-2--------Benzo(g,h,i)Perylene 410 u
_(l) -Cannot be separated from D1phenylam1ne
FORM I SV-2 1/87 Rev.
20937 94 SAMRLE DQTA SllMr/AR\' 1 1 C
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SB8-l-1RE Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) SOIL
Sample wt/vol: 30. 4 (g/mL) _G_
Level: ( low/med) LOW
\ Moisture: not dee. -2..Q dee.
.Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) IL_ pH: -2..,..,1
Number TICs found: -..Z.1
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: .,,_9;;,,.4 __
Lab S amp 1 e I D : .,,,3.,,6.,;,l :,_4 "--5 5"-----
Lab File ID: G2J61455A08
Date Received: 08/02/90
Date Extracted: 08/08/90
Date Analyzed: 08/20/90
Dilution Factor: ~i~-~0c,_ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ================ ============================ ======== ============= ===== 1. ALDOL 6.65 1800 ABJ 2. 629-59-4 TETRADECANE 10.87 2500 J 3. 629-78-7 HEPTADECANE 11.65 3100· J 4 •. DIMETHYLHEPTADECANE 12.39 4500 J 5. DIMETHYLHEPTADECANE 13.07 14000 J 6. 593-45-3 OCTADECANE 13.70 8600 J 7. UNKNOWN 14.25 2700 J 8. UNKNOWN HYDROCARBON 14.34 6600 J 9. UNKNOWN HYDROCARBON 15.32 4900 J 10. UNKNOWN HYDROCARBON 15.47 2500 J 11. UNKNOWN HYDROCARBON 16.72 4100 J 12. UNKNOWN HYDROCARBON 16.90 4100 J 13. UNKNOWN HYDROCARBON 17.02 7800 J
14. UNKNOWN HYDROCARBON 17.19 5800 J 15. UNKNOWN 17.55 7800 J 16. UNKNOWN HYDROCARBON 17.75 4900 J 17. UNKNOWN HYDROCARBON 18.14 3700 J 18. UNKNOWN HYDROCARBON 18.37 5300 J 19. UNKNOWN HYDROCARBON 18.50 4500 J 20. UNKNOWN HYDROCARBON 19.12 6600 J 21. PHTHALATE + UNKNOWN 19.99 3400 J
FORM I SV-TIC 1/87 Rev.
20937 94 SAMPLE oqrA SUMrlARV
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE tlO.
-SB8-2-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code : COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361456
Sample wt/veil: 30,6 (g/mL) _G_ Lab File ID: GH061456A08
Level: (low/med) rpw Date Received: 08/02/90
.% Moisture: not dee. __ll dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) lL_ pH: _i._l Dilution Factor: ~i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg)0 UG/KG
108-95-2--------Phenol 480
lll-44-4--------bis(2-Chloroethyl)Ether 480
95-57-8---------2-Chlorophenol 480
541-73-1--------1,3-Dichlorobenzene 480
106-46-7--------1,4-Dichlorobenzene 480
100-51-6--------Benzyl Alcohol 480
95-50-1---------1,2-Dichlorobenzene 480
95-48-7~--------2-Methylphenol 480
39638-32-9------bis(2-Chloroisopropyl)Ether_ 480
106-44-5----~---4-Methylphenol 480
621-64-7--------N-Nitroso-Di-n-Propylamine __ 480
67-72-1---------Hexachloroethane 480
98-95-3---------Nitrobenzene 480
78-59-1---------Isophorone 480
88-75-5---------2-Nitrophenol 480
105-67-9----~---2,4-Dimethylphenol 480
65-85-0---------Benzoic Acid 2300
lll-91-1--------bis(2-Chloroethoxy)Methane __ 480
120-83-2---~----2,4-Dichlorophenol 480
120-82-1-----~--l,2,4-Trichlorobenzene 480
91-20-3---------Naphthalene 480
106-47-8--------4-Chloroaniline 480
87-68-3---------Hexachlorobutadiene 480
59-50-7---------4-Chloro-3-Methylphenol 480
91-57-6---~-----2-Methylnaphthalene 480
77-47-4---------Hexachlorocyclopentadiene __ 480
88-06-2---------2,4,6-Trichlorophenol 480
95-95-4---------2,4,5-Trichlorophenol 2300
91-58-7---------2-Chloronaphthalene 480
88-74-4---------2-Nitroaniline 2300
131-11-3--------Dimethyl Phthalate. 480
208-96-8--------Acenaphthylene 480
606-20-2--------2,6-Dinitrotoluene 480
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DQTA SUMrlARY
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lC EPA SAMPLE tlO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB8-2-1
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ____ SDG No.: "'-9.:.4 __
Matrix: (soil/water) SOIL Lab Sample ID: ~3~6~1"'4~5~6c_ __ _
Sample wt/vol: 30.6 (g/mL) ~ Lab File ID: GH061456A08
Level: (low/med) rpw Date Received: 08/02/90
% Moisture: not dee. ---1.z. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/20/90
GPC Cleanup: (Y/N) .IL_ pH: ..2..:...l Dilution Factor: ~i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2--~------3-Nitroaniline 2300
83-32-9---------Acenaphthene 480
51-28-5---------2,4-Dinitrophenol 2300
100-02-7--------4-Nitrophenol 2300
132-64-9--------Dibenzofuran 480
121-14-2--------2,4-Dinitrotoluene 480
84-66-2---------Diethylphthalate 480
7005-72-3-------4-Chlorophenyl-phenylether __ 480
86-73-7---------Fluorene 480
100-01-6--------4-Nitroaniline 2300
534-52-1--------4,6-0initro-2-Methylphenol __ 2300
86-30-6---------N-Nitrosodiphenylamine (l)_ 480
101-55-3----~-~-4-Bromophenyl-phenylether __ 480
118-74-1--------Hexachlorobenzene 480
87-86-5---------Pentachlorophenol 2300
85-01-8---------Phenanthrene 480
120-12-7--------Anthracene 480
84-74-2---------Di-n-Butylphthalate 480
206-44-0--------Fluoranthene 480
129-oo-o--------Pyrene 480
85-68-7---------Butylbenzylphthalate 480
91-94-1---------3,3'-Dichlorobenzidine 950
56-55-3---------Benzo(a)Anthracene 480
218-01-9--------Chrysene 480
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 480
117-84-0--------Di-n-Octyl Phthalate 480
205-99-2--------Benzo(b)Fluoranthene 480
207-08-9--------Benzo(k)Fluoranthene 480
50-32-8---------Benzo(a)Pyrene 480
193-39-5--------Indeno(l,2,3-cd)Pyrene 480
53-70-3---------Dibenzo(a,h)Anthracene 480
191-24-2--------Benzo(g;h,i)Perylene 480
(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: 12-88}-REVS
EPA SAMPLE NO.
SB8-2-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL
Sample wt/vol: 30.6 (g/mL) ~
Level: (low/med) IPW
t Moisture: not dee. --1.2. dee.
Extraction:
GPC Cleanup:
( SepF / Cont/ Sonc)
(Y/N) li...._
~
pH: ....2..,..l
Number TICs found: _.l.Q
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
361456
GH061456A08
08/02/90
08/08/90
08/20/90
1.00
CONC. Q ================ ==================-========-======== ==.:::=====:::::==== =:::::===
l. SOLVENT CONTAMINANT 5.68 960 BJ 2. 2216-34-4 OCTANE, 4-METHYL-5.75 670 J
3. ALOOL 6.68 530 BAJ
4. 2855:1-12-0 ·1,2-BENZENEDICARBOXYLIC ACID 19.70 380 J 5. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 19.84 340 J 6. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 19.97 430 J 7. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 20.07 770 J
8. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 20.22 820 J
9. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 20.37 430 j
10. 28553-12-0 1,2-BENZENEDICARBOXYLIC ACID 20.52 240 J
FORM I SV-TIC 1/87 Rev.
20937 SAMPlE r~TA SUMMAR\' ., 1 o,
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
. SB16-l-1MS Lab Name: COMPUCHEM.RTP Contract: 12-88}-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ____ SDG No.: ,,_9.:,c4 __
Matrix: (soil/water) SOIL Lab Sample ID: ~3~6~1~4~5~8,..._ __ _
Sample wt/vol: 30.0 (g/mL) _G_ Lab File ID: GH061458B15
Level: (low/med) LQW Date Received: 08/04/90
% Moisture: not dee. -1..0. dee. Date Extracted: 08/08/90
Date Analyzed: 08/22/90 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) .IL_ pH: ~ Dilution Factor: ~i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-9.5-2--------Phenol 370
lll-44-4-~------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------1,3-Dichlorobenzene 370
106-46-7----~---l,4-Dichlorobenzene 370
100-51-6----~---Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9------bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370 67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5------~-~2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol • 370
65-85-o---------Benzoic Acid 1800
lll-91-1--------bis(2-Chloroethoxy)Methane_ 370
120-83-2--------2,4-Dichlorophenol 370
120-82-1--------1,2,4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58~7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate 370
208-96-8--------Acenaphthylene 370
606-20-2--------2,6-Dinitrotoluene 370
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FORM I SV-1 1/87 Rev.
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SBl6-l-lMS
Lab Name: COMPUCHEM.RTP Contract: (2-BBl-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361458
Sample wt/vol: 30.0 (g/mL) £;__ Lab File ID: GH061458B15
Level: (low/med) I.OW Date Received: 08/04/90
% Moisture: not dee. __ll dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ji_ pH:~
Date Analyzed: 08/22/90
Dilution Factor: ~i~-~o~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
"99-09-2--------~3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-7--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 370
100-01-6--------4-Nitroaniline 1800
534-52-1-7------4,6-Dinitro-2-Methylphenol __ 1800
86-30-6---------N-Nitrosodiphenylamine (l)_ 370
101-55-3-~------4-Bromophenyl-phenylether __ 370
118-74-1--------Hexachlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-7--------Anthracene 370
84-74-2---------Di-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-00-0--------Pyrene 370
85-68-7---~-----Butylbenzylphthalate 370
91-94-1---------3,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 370
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 370
117-84-0--------Di-n-Octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benz6(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene 370
191-24-2--------Benzo(g,h,i)Perylene 370
(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 l/87 Rev.
2093 7 .9.4, 5 HNF'-L:..E:. OP.IA-SUNNHF' '/
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB16-l-1MSD
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361459
Sample wt/vol: 30.0 (g/mL) ~ Lab File ID: GH061459B15
Level: (low/med) LOW Date Received: 08/04/90
% Moisture: not dee. ---1.Q dee. Date Extracted: 08/08/90
Extraction: Date Analyzed: 08/22/90
GPC Cleanup:
( SepF / Cont/ Sonc)
(Y/N) li.....__
SQ!:!£
pH: J....l1. Dilution Factor: .1~1~0~0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 370
lll-44-4--------bis(2-Chloroethyl)Ether 370
95-57-8---------2-Chlorophenol 370
541-73-1--------l,3-Dichlorobenzene 370
106-46-7--------1,4-Dichlorobenzene 370
100-51-6--------Benzyl Alcohol 370
95-50-1---------1,2-Dichlorobenzene 370
95-48-7---------2-Methylphenol 370
39638-32-9--~---bis(2-Chloroisopropyl)Ether_ 370
106-44-5--------4-Methylphenol 370
621-64-7--------N-Nitroso-Di-n-Propylamine __ 370
67-72-1---------Hexachloroethane 370
98-95-3---------Nitrobenzene 370
78-59-1---------Isophorone 370
88-75-5---------2-Nitrophenol 370
105-67-9--------2,4-Dimethylphenol 370
65-85-0---------Benzoic Acid 1800
lll-91-l--------bis(2-Chloroethoxy)Methane __ 370
120-83-2--------2,4-Dichlorophenol 370
120-82-1----.----l, 2, 4-Trichlorobenzene 370
91-20-3---------Naphthalene 370
106-47-8--------4-Chloroaniline 370
87-68-3---------Hexachlorobutadiene 370
59-50-7---:-------4-Chloro-3-Methylphenol 370
91-57-6---------2-Methylnaphthalene 370
77-47-4---------Hexachlorocyclopentadiene __ 370
88-06-2---------2,4,6-Trichlorophenol · 370
95-95-4---------2,4,5-Trichlorophenol 1800
91-58-7---------2-Chloronaphthalene 370
88-74-4---------2-Nitroaniline 1800
131-11-3--------Dimethyl Phthalate . 370
208-96-8--------Acenaphthylene 370
606-~0-2--------2,6-Dinitrotoluene 370
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FORM I SV-1 1/87 Rev.
20937 94 SAMPLE DQTB SUMMBiV
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS. DATA SHEET
SB16-1-1MSD
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 361459
Sample wt/vol: 30.0 (g/mLJ _G_ Lab File ID: GH061459B15
Level: (low/med) WW Date Received: 08/04/90
% Moisture: not dee. _l.Q dee. Date Extracted: 08/08/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li,_
fillli.Q
pH: ......8.....l1.
Date Analyzed: 08/22/90
Dilution Factor: 1.00
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 1800
83-32-9---------Acenaphthene 370
51-28-5---------2,4-Dinitrophenol 1800
100-02-1--------4-Nitrophenol 1800
132-64-9--------Dibenzofuran 370
121-14-2--------2,4-Dinitrotoluene • 370
84-66-2---------Diethylphthalate 370
7005-72-3-------4-Chlorophenyl-phenylether __ 370
86-73-7---------Fluorene 370
i00-01-6--------4-Nitroaniline 1800
534-52-1--------4,6-Dinitro-2-Methylphenol __ 1800
86-30-6---------N-Nitrosodiphenylamine (l)_ 370
101-55-3--------4-Bromophenyl-phenylether __ 370
118-7 4 -1--------Hexa.chlorobenzene 370
87-86-5---------Pentachlorophenol 1800
85-01-8---------Phenanthrene 370
120-12-1--------Anthracene 370
84-74-2---------Di-n-Butylphthalate 370
206-44-0--------Fluoranthene 370
129-00-0--------Pyrene 370
85-68-7---------Butylbenzylphthalate 370
91-94-1---------3,3'-Dichlorobenzidine 730
56-55-3---------Benzo(a)Anthracene 370
218-01-9--------Chrysene 370
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 370
117-84-0--------Di-n-Octyl Phthalate 370
205-99-2--------Benzo(b)Fluoranthene 370
207-08-9--------Benzo(k)Fluoranthene 370
50-32-8---------Benzo(a)Pyrene 370
193-39-5--------Indeno(l,2,3-cd)Pyrene 370
53-70-3---------Dibenzo(a,h)Anthracene __ ._ 370
191-24-2--------Benzo(g,h,i)Perylene 370
-(1) -Cannot be separated from Diphenylamine
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FORM I SV-2 1/87 Rev.
94
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Q)MPUCHEM
l.ABC)fW'"C>RlES, ll'JC:. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC27709 (919)549•8263
CASE NARRATIVE CASE #20937 SDG #119 CONTRACT #(2-88)REVS COMPUCHEM LABORATORIES, INC.
SAMPLES: SB-26-1 SB-JR-1 TB-7-1 TB-8-1
The samples listed above were received intact on 8-6-90 and 8-9-90 with the chain-of-custody documents in order and all shipping containers properly sealed. This narrative summarizes the analysis of these two samples for volatiles and semivolatiles. The two trip blanks were analyzed for volatiles only. Please note that the trip blank TB-8-1 was used and supplied as an instrument blank due to a laboratory accident.
Volatiles:
All sample and QC fractions were analyzed within holding times except the repeat analyses of TB-7-1. The initial analysis was performed within holding times. Only chloroform was present at concentrations greater than the contract required quantitation limit (CRQL). One trip blank had no target list compounds (TCLs). The other contained only low levels of methylene chloride and acetone. No samples contained any tentatively identified compounds (TICs) other than laboratory artifacts. Sample TB-7-1 required reanalysis because DB-toluene initially failed recovery criteria. All surrogate recovery criteria were met in the repeat analysis. Sample SB-2R-l also failed recovery criteria for DB-toluene, but no repeat analysis could be performed because, due to a laboratory accident, insufficient sample remained. All other sample and QC fractions met the surrogate recovery criteria. The matrix spike duplicates met overall accuracy and prec1s1on criteria; however, in the matrix spike 1,1-dichloroethene had a low recovery. All associated instrument blanks met all QC criteria.
Semi volatiles:
All sample and QC fractions were extracted within holding times.. No TCLs or TICs were detected in these samples. All sample and QC fractions met the surrogate recovery criteria. The matrix spike duplicates met all accuracy and precision criteria. All associated method blanks met all QC criteria.
Page -1
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
SB-2R-l Lab Name: COMPUCHEM,RTP Contract: (2-88}-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: S DG No. : .,.1_.1.,,_9 __
Matrix: ( soil/water) WATER Lab Sample ID: 362521
sample wt/vol: 5.0 (g/mL) Ml._ Lab File ID: CN062521AI1
Level: (low/med) LOW Date Received: 08/06/90
I Moisture: not dee. Date Analyzed: 08/12/90
Column: (pack/cap) CAP Dilution Factor: ... i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00~J---------Chloroethane 10 u 75-09-2---------Methylene Chloride 1 BJ
67-64-1---------Acetone 2 J
75-15-0---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3----~----Chloroform 13
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5-----~---l,2-Dichloropropane 5 u
10061-0l-S------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s--~------1,1,2-Trichloroethane 5 u
71-43-2-----~---Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1oa-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane_._ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41~4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 119 SAMPLE DAT~ SUMMARY 5€
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SB-2R-1 Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ~1-19'-----
Matrix: (soi_l/water) WATER Lab Sample ID: 362521
Sample wt/vol: 5.0 (g/mL) Ml,_ Lab File ID: CN062521AI1
Level: (low/med) . ..,LO""W.,___ · Date Received: 08/06/90 I t Moisture: not dee. Date Analyzed: 08/12/90
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Column (pack/cap) ,..CA...,P~_
Number TICs found: _.1
CAS NUMBER ,COMPOUND NAME
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
1.0
CONC. ================ ============================ ======== ============= 1. LABORATORY ARTIFACT 3.22 13 2. LABORATORY ARTIFACT 20.64 20 3. LABORATORY ARTIFACT 23.59 12
FORM I VOA-TIC 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COHPUCHEM.RTP Contract: (2-88)-REVS SB-JR-1
Lab Code: COHPU case No.: 20937 SAS No.: S DG No. : .1-1=9 __
Matrix: (soil/water) WATER Lab Sample ID: 363565
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: CN063565AI1
Level: (low/med) LOW Date Received: 9!l.:'.09,:'.9o
t Moisture: not dee. Date Analyzed: 9!!<'.'.U.:'.90
Column: (pack/cap) CAP Dilution Factor: 1,0 -~--
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) lTG,:'.L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 5 B 67-64-1---------Acetone 2 BJ 75-15-o---------carbon Disulfide 5 u 75-35-4---------1,l-Dichloroethene · 5 u 75-34-3---------1,l-Dichloroethane 5 u 540-59-0---~----l,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 15 107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 5 u 56-23-s-~-------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane 5 u 78-87-5---------1,2-Dichloropropane 5 u 10061-01-S------cis-l,3-Dichloropropene 5 u 79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u 79-00-5---------1, l, 2-Trichlor.oethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 1l$ SAMP~~ DATR SUMMARY 54
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS SB-3R-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ll9
Matrix: ( soil/water) WATER Lab Sample ID: 363565
Sample wt/vol: 5.0 (g/mL) lili.._ Lab File ID: CN063565AI1
Level: (low/med) LOW
% Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: __l
CAS NUMBER COMPOUND NAME
Date Received: 08/09/90
Da·te Analyzed: 08/HIS!Q
. Dilution Factor: _.1_,_ . .,._o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q ================ =-=--==-------------===-===-======== ============= ===== 1. LABORATORY ARTIFACT 3.17 5.5 BJ
FORM I VOA-TIC 1/87 Rev.
20937 119 SAMPLE DATA SUMl'IAR'r'
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
TB-7-1
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 119
Matrix: ( soil/water) WATER Lab Sample ID: 362524
Sample wt/vol: 5.0 (g/mL) Ill,,__ Lab File ID: CN062524AI1
Level: (low/med) LOW Date Received: 08/06/90
I Moisture: not dee. Date Analyzed: 08/12/90
Column: (pack/cap) CAP Dilution Factor: .1~,~o __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q .
74-87-3---------Chloromethane 10 t1 74-83-9---------Bromomethane ' 10 t1 75-01-4---------Vinyl Chloride 10 t1 75-00-3---------Chloroethane 10 t1 75-09-2---------Methylene Chloride 5 t1 67-64-1---------Acetone 10 t1 75-15-o-----~---carbon Disulfide 5 t1 75-35-4---------1,l-Dichloroethene 5 t1 75-34-3---------1,1-Dichloroethane 5 t1 540-59-o--------l,2-Dichloroethene (total)_ 5 t1 67-66-3---------Chloroform 5 t1 107-06-2--------1,2-Dichloroethane 5 t1 78-93-3---------2-Butanone 10 t1 71-55~6---------1,1,1-Trichloroethane 5 t1 56-23-5---------carbon Tetrachloride 5 t1 108-05-4--------Vinyl Acetate 10 t1
75-27-4---------Bromodichloromethane 5 t1 78-87-5---------1,2-Dichloropropane 5 t1
10061-01-5------cis-l,3-Dichloropropene 5 t1
79-01-6---------Trichloroethene 5 t1
124-48-1--------Dibromochloromethane 5 t1 79-00-5---------1,1,2-Trichloroethane 5 t1
71-43-2---------Benzene 5 t1
10061-02-6------Trans-l,3-Dichloropropene __ 5 t1
75-25-2-----~---Bromoform 5 t1
1os-10-1--------4-Methyl-2-Pentanone 10 t1.
591-78-6--------2-Hexanone 10 t1
127-18-4--------Tetrachloroethene 5 t1
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 t1
108-88-3--------Toluene 5 t1
108-90-7--------Chlorobenzene 5 t1
100-41-4--------Ethylbenzene 5 t1
100-42-s--------styrene 5 t1
1330-20-7-------Total Xylenes 5 t1
FORM I VOA 1/87 Rev.
20937 JJ~ Si:IMPLQ OATA SIJNt1AR'-r' S2
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
EPA SAMPLE NO.
TB-7-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .._l._19.___
Matrix: (soil/water) WATER
Sample wt/vol: 5,0 (g/mL)
Level: (low/med) I.OW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: ___ii
ML___
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
362524
CN062524AI1
08/06/90
08/12/90
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY 51
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TB-7-lRE
Lab Name: COMPUCHEM.RTP Contract: ·r2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: S CG No. : ,.1..,1.,,_9 __
Matrix: ( soil/water) WATER Lab Sample ID: 362524
sample wt/vol: 5.0 (g/mL) Ml,_ Lab File ID: CR062524B51
Level: (low/med) LOW Date Received·: 08/06/90
\ Moisture: not dee. Date Analyzed: 0§(il2190
Column: (pack/cap) CAP Dilution Factor: .. i~-~o'----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 5 u 67-64-1---------Acetone 10 u
75-15-o----~----Carbon Disulfide 5 u
75-35-4~--------l,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00~s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
1s-2s-2---~-----BromofoI"111 5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY 5£
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM. RTP Contract: (2-BB)-REVS
EPA SAMPLE NO.
TB-7-lRE I
Lab Code: COMPU Case.No.: 20937 SAS No.: S 0G No . : ._1.,..19"---
Matrix: (soil/water) WATER
Sample wt/vol: 5,0 (g/mL) !il..c.._
Level: (low/med) LOW
% Moisture: not dee.
Column (pack/cap) CAP
Number TICS found: ___Q
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/·L or ug/Kg) UG/L
362524
CR062524B51
08/06/90
08/22/90
1.0
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
20937 119 SAMPLE OATA SUMMARY 45
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
SB-2R-1MS
Lab Code: COMPU Case No.: 20937 SAS No.: S 0G No . : .,.1...,1.z.9 __
Matrix: ( soil/water) WATER Lab Sample ID: 362528
Sample wt/vol: 5.0 (g/mL) Ml._ Lab File IO: CN062528AI1
Level: (low/med) LOW Date Received: 08/06/90
t Moisture: not dee. Date Analyzed: 08/12/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/1, Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ
67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 11
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2-----~---Benzene 5 u
10061-02-6------Trans-l,J-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-88l-REVS SB-2R-1MSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ..._1~19.___
Matrix: (soil/water) WATER Lab Sample ID: 362530
sample wt/vol: 5.0 (g/mL) m......,_ Lab File ID: CN062530Ail
Level: (low/med) LOW Date Received: 08/06/90 I % Moisture: not dee. Date Analyzed: 08/12/90
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Column: (pack/cap) CAP Dilution Factor: .l~-~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9-;::.::;_,:_;:,1----Bromomethane 10 u ·-·· 75-01-4-----~---Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone 10 u 75-15-o-----~---carbon Disulfide 5 u 75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene (tot~l) ___ 5 u 67-66-3---------Chloroform 12
107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u 1os~os-4--------vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-s------cis-l,J-Dichloropropene 5 u
79-01-6---------Trich_loroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------Styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 119 SRMP~E DATA SUMMARY 47
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS SB-2R-l
Lab code: COMPU Case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362521
Sample wt/vol: 500 (g/mL) HI..._ Lab File ID: GH062S21C07
Level: ( low/med) LOW Date Received: 08,:'.06,:'.90
% Moisture: not dee. dee. Date Extracted: 08/06/90
Extraction: (SepF/Cont/Sonc) gff
GPC Cleanup: (Y/N) H,_ pH:
Date Analyzed: 08,:'.10/90
Dilution Factor: ~9i,~5~0 __
CAS NO, COMPOUND
108-95-2~-------Phenol
CONCENTRATION UNITS:
(ug/_L or ug/Kg) UGLL
lll-44-4--------bis(2-Chloroethyl)Ether
9S-57-B---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7-----~---2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-S9-l---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
. 91-20-3-----~---Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2;4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
so u
10 u
10 u
·10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
so u
10 u
10 u
10 u
FORM I SV-1 1/87 Rev.
28937 119 5~MPLE DATA SUMMARY
Q
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
SB-2R-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ..,_l,...19.___
Matrix: (soil/water) WATER Lab Sample ID: 362521
Sample wt/vol: 500 (g/mL) t1l.,__ Lab File ID: GH062521C07
Level: (low/med) LOW Date Received: 08/06/90
t Moisture: not dee. dee. Date Extracted: 08/06/90
Extraction: (SepF/Cont/Sonc) Ilff Date Analyzed: · 08/10/490
GPC Cleanup: (Y/N) li...._ pH: Dilution Factor: O, 50
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4~Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3----~--4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1-~------4,6-Dinitro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-o--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---~-----Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2~Ethylhexyl)Phthalate_
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo (a) Pyren.e
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from D1phenylam1ne
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I SV-2 1/87 Rev.
20937 11? SRMPLi Q~TR SUMMRRV
Q
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS SB-2R-l
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362521
Sample wt/vol: 500 (g/mL) tll...c.._ Lab File ID: !:ili0625~1C07
Level: (low/med) LOW Date Received: 08/06/90
\ Moisture: not dee. dee. Date Extracted: 08/06/90
Extraction: (SepF/Cont/Sonc) S.E.U Date Analyzed: 08/10/90
GPC Cleanup: (Y/N) li.._ pH: Dilution Factor: =o~,s=o~-
CONCENTRATION UNITS:
Number TICs found:~ (ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q m=============== =========~================== ======== ============= =====
FORM I SV-TIC 1/87 Rev.
20937 JJ9 SAMPLE DATA SUMMARY 44
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS SB-JR-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 363565
Sample wt/vol: 500 (g/mL) Ml,_ Lab File ID: GH06J565Al5
Level: ( low/med) LOW Date Received: 08/09/90
t Moisture: not dee. dee. Date Extracted: QB/10/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) lL_ pH:
Date Analyzed: 08/11/90
Dilution Factor: .,,_o...._. ,,.s,._o __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether ·
95-57-8---------2-Chlorophenol
541-73-1---~----l,J-Dichlorobenzene
106-46-7--------l,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-l---------l,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine
67~72-1---------Hexachloroethane --
98-95-3---------Nitrobenzene
78-59-1---------Isophorone -
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-as-o~--------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-s2-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene'
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2~Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
Q
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
SB-JR-1 Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) WATER
SAS No.: S 0G No. : ..,1""1"'9 __
Lab Sample ID: .._J.,._6,,_35"'6""5"----
Sample wt/vol: 500 (g/mLJ Ml.,__ Lab File ID: GH06J565Al5
Level: (low/med) .LQ~W __
t Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) §.EU
Date Received: 08/09/90
Date Extracted: 08/10/90
Date Analyzed: 08/11/90
GPC Cleanup: (Y/N) Ji_ .pH: Dilution Factor: 0.50
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------J-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9----~---Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (1)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-a---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-o--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
111-a4-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32.-8---------Benzo ( a) Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -cannot be separated from Diphenylamine
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
2~937 119 SAMPLE DQTA SUMMRRY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
EPA SAMPLE NO.
SB-JR-1
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER
Sample wt/vol: 500 (g/mL). ~
Level: ( low/med) LOW
t Moisture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_
Number TICS found: ....:...Q
dee.
pH:
CAS NUMBER COMPOUND
gu
NAME
Lab Sample ID:
Lab File IO:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
363565
GH063565Al5
08/09/90
08/10/90
08/11/90
O, 50 ·
CONC. Q ====•=========== ==-------===---------=-=---= ==-====== ============= =====
FORM I SV-TIC 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY 41
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
SB-2R-1MS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362525
Sample wt/vol: 500 (g/mL) l1L._ Lab File ID: GH062525C07
Level: (low/med) LOW Date Received: 08/06/90
% Moisture: not dee. dee. Date Extracted: 08/06/90
Extraction: (SepF/Cont/Sonc) SE..P..E Date Analyzed: 08/10/90
GPC Cleanup: (Y/N) li...._ pH: Dilution Factor: ~9~-~s~o __
.CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
·~~•.i...i 1,.1!,:;__"':,"1..:i.,-..
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol.
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3-----~---Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic ·Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---~-----Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol•
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 l:
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY
Q
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB-2R-1MS Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362525
sample wt/vol: 500 (g/mL) tu._ Lab File ID: GH062525C07
Level: (low/med) ~LO~W,.,__ Date Received: 08/06/90
t Moisture: not dee. dee. Date Extracted: O!l/06/90
Extraction: (SepF/Cont/Sonc) Date Analyzed: 08/10/90
GPC Cleanup: (Y/N) IL_ pH: Dilution Factor: ~o~,s~o.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2--~------J-Nitroaniline 50 u 83-32-9---------Acenaphthene 10 u 51-28-5---------2,4-Dinitrophenol 50 u
100-02-7--------4-Nitrophenol 50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2-------~-Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-oo-o--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3 3'-Dichlorobenzidine 20 u Q , 10 u 56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------Di-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY 35
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
% Moisture: not dee.
500
LOW
(g/mL) !il....._
dee.·
SAS No.: SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
EPA SAMPLE NO.
SB-2R-1MSD
No.: 119
362526
GH062526C07
08/06/90
oa106190
Extraction: (SepF/Cont/Sonc) gff
GPC Cleanup: (Y/N) li...._ pH:
Date Analyzed: 08/10/90
Dilution Factor: ~o~,~s~o __
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1 4-Dichlorobenzene . ,
100-51-6-~------Benzyl Alcohol
95-50-1-~-------l,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4--------~Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 119 SAMPlE DATA SUMMARY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMB/CHEM,RTP Contract: (2-88)-REVS SB-2R-1MSD
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362526
Sample wt/vol: 500 (g/mL) tu._ Lab File ID: GH062526C07
Level: (low/med) LOW Date Received: 08/06/90
t Moisture: not dee. dee. Date Extracted: 08/06/90
Extraction: (SepF/Cont/Sonc) .s.n.r
GPC Cleanup: (Y/N) IL_ pH:
Date Analyzed: 08/10/90-
Dilution Factor: ~0~-~s~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4~Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120~12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,J'-Dichlorobenzidine ·
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32.-8---------Benzo ( a) Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-.24-2--------Benzo (g ,h, i) Perylene
(1) -cannot be separated from Diphenylamine
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I SV-2 · 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
SB-2R-1MS
No.: 119 I Matrix: (soil/water) WATER Lab Sample ID: 362525
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sample wt/vol: 500 (g/mL) HI....._ Lab File ID: GH062s2sco1
Level: (low/med) LOW Date Received: 08/06/90
I Moisture: not dee. dee. Date Extracted: 08/08/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) L.. pH:
llU Date Analyzed: 08/10/90
Dilution Factor: ~0~1~5~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
ioo-s1-6--------Benzyl Alcohol 10 u 95-50-1---------l,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5---~----4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-0---------Benzoic Acid 50 u
lll-9l-l-------~bis(2-Chloroethoxy)Methane __ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-a-~------4-Chloroaniline 10 u
87-68-3-----~---Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphth~lene 10 u
77-47-4---------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluena 10 u
FORM I sv-1 1/87 Rev.
•
20937 119 SAMPLE DATA SUMMARY
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
SB-2R-1MS
No.: 119 I Matrix: (soil/water) WATER Lab Sample ID: 362525
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sample wt/vol: 500 (g/mL) tu.__ Lab File ID: GH062s2sco1
Level: (low/med) I.OW Date Received: 08/06/90
I Moisture: not dee. dee. Date Extracted: 08/08/90
Extraction:
GPC Cleanup:
(SapF/Cont/Sonc)
(Y/N) li.._ pH:
Date Analyzed: 08/10/90
Dilution Factor: ~0~,~s~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroagjlin~ 50 u
83-32-9---------Acenaphthen~-10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-7--------4-Nitrophenol 50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2----~----Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether __ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l) __ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206~44-0--------Fluoranthena 10 u
129-00-o--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------Di-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-e---------aenzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrena 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY 3
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP · Contract: (2-88)-REYS SB-2R-1MSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 119
Matrix: (soil/water) WATER Lab Sample ID: 362526
Sample wt/vol: 500 (g/mL) til._ Lab File ID: GH062526C07
Level: ( low/med) LOW Date Received: 08/06/90
I Moisture: not dee, dee. Date Extracted: OB/08/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) tl_ pH:
Date Analyzed: 08/10/90
Dilution Factor: ~0~,~5~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 , u
lll-44-4--------bis(2-Chloroethyl)Ether 10 u 95-57-8---------2-Chlorophenol 10 u 541-73-1--------1,J-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u 95-50-1---------1,2~Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-ss-o---------Benzoic Acid 50 u
lll-91-1--------bis(2-Chloroethoxy)Methane __ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-s2-1--------1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8-~------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7-----~---4-Chloro-J-Methylphenol 10 u
· 91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 119 SAMPLE DRTR SUMMRRY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: 'COMPUCHEM. RTP Contract: 12-881-REVS SB-2R-1MSO
Lab code: COMPU Case No.: 20937 SAS No.: SOG No.: 119
Matrix: (aoil/water) WATER Lab Sample IO: 362526
Sample wt/vol: 500 (g/mL) tll...... Lab File ID: GH062526C07
Level: (low/med) LOW Date Received: 08/06/90
t Moisture: not dee. .--dee. Date Extracted: 08,:'.08,:'.90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li..._
ilPl
pH:
Date Analyzed: 08,:'.10/90
Dilution Factor: 0.50
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether __
86-73-7---------Fluorene
100-01-6---------4-Nitroaniline
534-52-1--------4,6-0initro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (1)_
101-55-3---------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-0l~a---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-o---~----Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3 ,.3 '-Dichlorobenz idine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from Diphenylamine
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I SV-2 1/87 Rev.
20937 119 SAMPLE DATA SUMMARY
Q
33
PLATINUM CASE SUM~~Rf NARRATIVE---CASE
:;oi; 1 Jz
COMPUCHEM LABORATORIES
-~ -\"'-2 1) ; 3;
1his case consisted of two soil samples for volat:l~ and s~1ni 110latil~ anal~sis.
The ~3mpl~s w~re r~ceived int-3Ct on 8-10-90 wi~h tr3ific r2p,1rt5.
Sample pH values f~r both samples ~ere within contr~ctu3l li~i:s.
VOLATILES
Both £amples were initially analy:ed within hol~i~; tim~ r;quir~ments, h~~;~~~
tt,a s.3mpl~s fail~d contr.actual 5urrogat~ r~cov~ry r~,~~ir~~~nt; j~a to s11
instrwm~nt pr~bl~~-The samples a~d matri•( spik9!m~tri~ ~~1ka •~uplicat~ ~e~~
rea~3lyzed out~ide of holdi11g tim~5 3nd all sur~~~at~ ~rit~ria p35~~j ~!~ i~~
r~p0r·ting both se!s of data.
Both S-i~ples contain~d low l~v~ls 0~ methyl~n~ ch!-,ri~; an1 a,:?t~n~: whi-:~
1..i ere ::1 l s v p :-· e-s-;. n t at comp a r ; b 1 .;, l e-v e l s i r, t he i r o ·s :-c1 ,: i. =it e-d iii;, : :--.. :. ,j b l a ri ;, :
Oth~r th3~ laborat~ry artif~•:t5 11c t~ntatively id¾~tifi~d ~omp~~n•~5 w~ra
present 1r1 tt-i~s:~ :.omp1es.
The ma:rii ;pike/m3trii spike ~1Jplic3te had 3Cc~ptibl@ s~ik? 3~1j a~rrc;3~~
r·e,co'Jer i es .
.Sl:MII/OL,;TILES:
BotM 5~:~i-Jclatile sa~?l~s w~re ~:<tr3cted and an~ly:ed ~ith~~ h:!~i~; t~.~?5
Nor:~ co~c0~Gd5 w~r~ pre;~nt 3t reportabl~ l~v~l;. 3nd ~t~er th3n bl!nk
contJ,nina~~s, only t~o tentati 1:ely identiF~ed comp~un~~ were prase~t :n
1: C ij 3,; 4 1 1) 3 .
Th~ m~tri~ spi~~.'m6tri:! spike duplicate had acc~ptible Eci~~ ~r.j ~~rr:s3:i
r•~•:o·,.:~r i ~-s.
I cert1i1 that this data pack3ge is in compliance with tne terms and c0n=i::,~s
~f th~ contr.3ct> both te~h~ically and for cample~en~55. fo~ oth~r thar t~i ·
candit~Jns detailed above. Release of the data c~ntain~1 in th1~ hard=·:~1 ~5:~
pac~3;~ h~s b~~n ~uthorized··bi the Laboratory Mana~~~ or his d~si~re~ -3~
veriF1•d by th~ Following signature ..
.&;_/A-~--------
Roy M. Sutton a-Jl-90
Oevelopm~n~ Chemi5t
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW6-4S-l Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : .,.l.,,_J..,_J __
Matrix: ( soil/water) SOIL Lab Sample ID: 364102 Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GHQ641Q2All
Level: ( low/med) LOW Date Received: 08/10/90 I Moisture: not dee. _ll Date Analyzed: 08£'.;?0,:'.20
Column: (pack/cap) CAP Dilution Factor: .i~-~o __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Acetone
75-15-0---------carbon Disulfide 7 5-3 5-4 ------·---1, 1-Dichl oroethene 75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_ 67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride 108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-1,3-Dichloropropene_
75-25-2---------Brcimoform
lOB-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4------~-Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane_
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
13 u 13 u 13 u
13 u
9 B
73 B
6 u
6 u
6 u
6 u
6 u
6 u
13 u
6 u
6 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13 u
13 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
FORM I VOA 1/87 Rev.
20937 133 SRMPLE DRTR SUMMRRY • II .l&NIZ liW
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG
Matrix: ( soil/water) SOIL Lab Sample ID:
HW6-4S-l
No.: 133
364102
Sample wt/vol: 5.0 (g/mL) L_ Lab File IO: GH064102All
Level: (low/med) LOW
% Moisture: not dee. _2]_
Column (pack/cap) CAP
Number TICs found: ___Q
CAS NUMBER COMPOUND NAME
Date Received: 9!U19L2Q
Date Analyzed:. QBL20L90
Dilution Factor: .1~1 Q,.__ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGLKG
RT EST. CONC.
FORM I VOA-TIC 1/87 Rev.
20937 133 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW6-4S-l
Lab Name: COMPUCHEM.RTP Contract: /2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No. : _.1,.3,.3 __
Matrix: (soil/water) SOIL Lab Sample ID: . ..,_3,..642.l""0._,2.__ __ _
Sample wt/vol: 30,1 (g/mL) !L._ Lab File IO: GH064102A2o
Level: (low/med) LOW Date Received: 08/10/90
, Moisture: not dee. _ll dee. Date Extracted: 08/17/90
Extraction: (SepF/Cont/Sonc) .s.o.tiC Date Analyzed: 08/21/90
GPC Cleanup: (Y/N) lL__ pH: ...L.i Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) l,!G/ISG Q
108-95-2--------Phenol 430 u
lll-44-4--------bis(2-Chloroethyl)Ether 430 u
95-57-8---------2-Chlorophenol 430 u
541-73-1--------1,3-Dichlorobenzene 430 . u
106-46-7--------1,4-Dichlorobenzene 430 u
100-51-6--------Benzyl Alcohol 430 u
95-50-1---------1,2-Dichlorobenzene 430 u
95-48-7---------2-Methylphenol 430 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 430 u
106-44-5--------4-Methylphenol 430 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 430 u
67-72-1---------Hexachloroethane 430 u
98-95-3---------Nitrobenzene 430 u
78-59-1---------Isophorone 430 u
88-75-5---------2-Nitrophenol 430 u
105-67-9--------2,4-Dimethylphenol 430 u
65-85-o---------Benzoic Acid 2100 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ 430 u
120-83-2--------2,4-Dichlorophenol 430 u
120-e2-1--------1,2,4-Trichlorobenzene 430 u
91-20-3---------Naphthalene 430 u
106-47-8--------4-Chloroaniline 430 u
87-68-3---~-----Hexachlorobutadiene 430 u
59-50-7---------4-Chloro-3-Methylphenol 430 u
91-57-6---------2-Methylnaphthalene 430 u
77-47-4---------Hexachlorocyclopentadiene __ 430 u
88-06-2---------2,4.6-Trichlorophenol 430 u
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalene 430 u
88-74-4---------2-Nitroaniline 2100 u
131-11-3--------Dimethyl Phthalate 430 u
208-96-8--------Acenaphthylene 430 u
606-20-2--------2.6-Dinitrotoluene 430 u
FORM I SV-1 1/87 Rev.
20937 133 SAMPLE DRTR SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW6-4S-l
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No,: SDG No.:. 133
Matrix: (soil/water) SOIL Lab Sample ID: 364102
Sample wt/vol: 30.l (g/mL) L_ Lab File ID: GH064102A20
Level: (low/med) _r,o=w~_ Date Received: 08/10/90
I Moisture: not dee. ___l,_3_ dee. Date Extracted: 08/17/90
Extraction: (SepF/Cont/Sonc) .5.Qm; Date Analyzed: 08/21/90
GPC Cleanup: (Y/N) li.,_ pH: ....§....i Dilution Factor: .1~·~0 __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2100
83-32-9---------Acenaphthene 430
51-28-5---------2,4-Dinitrophenol 2100
100-02-7--------4-Nitrophenol 2100
132-64-9--------Dibenzofuran 430
121-14-2--------2,4-Dinitrotoluene 430
84-66-2---------Diethylphthalate 430
7005-72-3-------4-Chlorophenyl-phenylether_. _ 430
86-73-7---------Fluorene 430
100-01-6--------4-Nitroaniline 2100
534-52-1--------4,6-Dinitro-2-Hethylphenol_ 2100
86-30-6---------N-Nitrosodiphenylamine (1) 430
101-55-3--------4-Bromophenyl-phenylether-= · 430
118-74-1--------Hexachlorobenzene 430
87-86-5---------Pentachlorophenoi 2100
85-01-8---------Phenanthrene 430
120-12-1--------Anthracene 430
84-74-2---------Di-n-Butylphthalate 430
206-44-o--------Fluoranthene . 430
129-00-0--------Pyrene 430
85-68-7---------Butylbenzylphthalate 430
91-94-1---------3,3'-Dichlorobenzidine 850
56-55-3~--------Benzo(a)Anthracene 430
218-01-9--------Chrysene 430
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 430
117-84-0--------Di-n-Octyl Phthalate 43·0
205-99-2--------Benzo(b)Fluoranthene 430
207-08-9--------Benzo(k)Fluoranthene 430
50-32-8---------Benzo(a)Pyrene 430
193-39-5--------Indeno(l,2,3-cd)Pyrene 430
53-70-3---------Dibenz(a;h)Anthracene 430
191-24-2--------Benzo(g,h,i)Perylene 430
(1) -Cannot be separated from Diphenylamine
Q
u u u u u u u u u u u u u u u u u u u u u
u u
u u u
u
u
u u
u u
FORM I sv-2 1/87 Rev.
20937 133 SAMPLE DRTR SUMMARY
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: (2-BSl-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
MW6-4S-l
No.: 133
364102
Sample wt/vol: 30.1 (g/mL) ~ Lab File ID: GH064102,a,20
Level: (low/med) LOW
' Moisture: not dee. ___u dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H__ pH: ....L.i
Number TICs found: ___l
CAS NUMBER COMPOUND NAME
Date Received: 08/10/90
Date Extracted: 08/12/90
Date Analyzed: 08/21/90.
Dilution Factor: .1 •• 0.._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q cam=====a=s:::::11:z=:a=• --========================== ==-====--====a=====••• •=•== l • SOLVENT CONTAMINANT 4.70 340 BJ
FORM I SV-TIC l/87 Rev.
20937 133 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO ..
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS MW6-4S-1RE
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No, : .,.1.,.3.,.3 __
Matrix: ( soil/water) SOIL Lab Sample ID: 364102
Sample wt/vol: 5.0 (g/mL) L_ Lab File ID: GR064102l,13
Level: (low/med) LOW Date Received: 08/10/90
\ Moisture: not dee. ---2.3. Date Analyzed: 0!!/21/90
Column: (pack/cap) CAP Dilution Factor: .li,~O __ _
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4--~------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 17 B
67-64-1---------Acetone 120 B 75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3---------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u 78-93-3---------2-Butanone 6 BJ 71-55-6---------1,1,l-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u 108-05-4--~-----Vinyl Acetate 13 u 75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u 10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u 124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u 10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4~Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1 1 2 2-Tetrachloroethane 6 u I I I , --108-88-3--------Toluene 6 u
1o8-90-7--------.Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev,
20937 133 SAMPLE DATA SUMMARY 4
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
EPA SAMPLE NO.
MW6-4S-1RE
Lab Code: COMPU case No.: 20937 SAS No.: SDG No. : ..,l,._3 3....__
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: ( low/med) LOW
I Moisture: not dee. _u
Column (pack/cap) CAP
Number TICs found: --1.
CAS NUMBER COMPOUND
L._
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
364102
GR064102A13
08/10/90
08/21/90
1,0
CONC. Q *•============== ============================ -====----•••=a======== =====
l. LABORATORY ARTIFACT 0.75 7.8 .J
FORM I VOA-TIC 1/87 Rev.
20937 133 SAMPLE DRTR SUMMRRY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW7-4S-l Lab Name: coMPUCHEM,RTP Contract: C2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 133
Matrix: ( soil/water) SOIL Lab Sample ID: 364103
Sample wt/vol: 5.0 (g/mL) ~ Lab File ID: GH064103B11
Level: (low/ined) LOW Date Received: 08/10/90
\ Moisture: not dee. ---2..2. Date Analyzed: 08/20/90
Column: (pack/cap) CAP Dilution Factor: .1~,~o'----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
. 74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u 75-09-2---------Methylene Chloride 10 B 67-64-1---------Acetone 43 B 75-15-o---------carbon Disulfide 6 u 7 5-35--4---------1, 1-Dichloroethene 6 u 75-34-3---------1,1-Dichloroethane 6 u 540-59-0--------1,2-Dichloroethene (total)_ 6 u 67-66-3---------Chloroform 6 u 107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 13 u 71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u 78~87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u ..
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,i,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans~l,3-Dichloropropene __ 6 u
75-25-2------~--Bromotorm 6 u
1oe-10-1--------4-Mathyl-2-Pentanone 13 u
591-78-6--------2-Hexanona 13 U·
127-18-4--------Tetrachloroethena 6 u
79-34-5---------1,1,2,2-Tatrachloroathana __ 6 u
1oe-ee-3--------Toluena 6 u
108-90-7--------Chlorobanzene 6 u
100-41-4--------Ethylbanzene 6 u
100-42-5~-------styrana 6 u
1330-20-1-------Total Xylanas 6 u
FORM I VOA 1/87 Rav.
20937 133 5AMPbE DATA SUMMARY ' .
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
EPA SAMPLE NO.
MW7-4S-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ..._1.._33.___
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee. __u
Column (pack/cap) CAP
Number TICs found: __Q
CAS NUMBER COMPOUND
L_
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
364103
GH064103B11
08/10/90
08/20/90
1,0
CONC. Q ••••a•••=••=•••• •==-=------=---=---=-=~~==-= =-==•••a •••-===aa::z::s••• =====
FORM I VOA-TIC 1/87 Rev.
20937 133 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW7-4S-l Lab Name: CQMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 133
Matrix: (soil/water) SOIL Lab Sample ID: 364103
Sample wt/vol: 30.l (g/mL) li.._ Lab File IO: GH06410J~,o
Level: (low/med) .-LO=W~-Date Received: 08/10/90
I Moisture: not dee. -12. dee. Date Extracted: 08/17/90
Extraction: (SepF/Cont/Sonc) SQH.C Date Analyzed: 08/21/90
GPC Cleanup: (Y/N) li,__ pH:~ Dilution Factor:, ..,l.._ • .,.o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 420 u
lll-44-4--------bis(2-Chloroethyl)Ether 420 u
95-57-8---------2-Chlorophenol 420 u
541-73-1--------1,3-Dichlorobenzene 420 u
106-46-7--------1,4-Dichlorobenzene 420 u
100-51-6--------Benzyl Alcohol 420 u
95-50-1---------1,2-oichlorobenzene 420 u
95-48-7---------2-Methylphenol 420 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 420 u
106-44-5--------4-Methylphenol 420 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 420 u
67-72-1---------Hexachloroethane 420 u
98-95-3---------Nitrobenzene 420 u
78-59-1---------Isophorone 420 . u
88-75-5---------2-Nitrophenol 420 u
105-67-9--------2,4-Dimethylphenol 420 u
65-as-o---------Benzoic Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ 420 u
120-aJ-2--~-----2,4-Dichlorophenol 420 u
120-a2-1--------1,2,4-Trichlorobenzene 420 u
91-20-3------~--Naphthalene 420 u
106-47-8--------4-Chloroaniline 420 u
87-68-3---------Hexachlorobutadiene 420 u
59-50-7---------4-Chloro-3-Methylphenol 420 u
91-57-6---------2-Methylnaphthalene 420 u
77-47-4---------Hexachlorocyclopentadiene __ 420 u
88-06-2---------2,4,6-Trichlorophenol 420 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 420 u
88-74-4---------2-Nitroanilina 2000 u
131-11-3--------Dimethyl Phthalata 420 u
208-96-8--------Acenaphthylene 420 u
606-20-2--------2,6-Dinitrotoluene 420 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW7-4S-l
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPO Case No.: 20937 SAS No.: SDG No.: 133
Matrix: (soil/water) SOIL Lab Sample ID: 364103
Sample wt/vol: Jo.1 (g/mL) L_ Lab File ID: GH064lOJc20
Level: (low/med) I.OW Date Received: 08/10/90
' Moisture: not dee. _u dee. Date Extracted: 08/17/90
Extraction: (SepF/Cont/Sonc)
(Y/N) l:L_
Date Analyzed: 08/21/90
GPC Cleanup: pH: -6....2. Dilution Factor: £1~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2000
83-32-9---------Acenaphthene 420
51-28-5---------2,4-Dinitrophenol 2000
100-02-7--------4-Nitrophenol 2000
132-64-9--------Dibenzofuran 420
121-14-2--------2,4-Dinitrotoluene 420
84-66-2---------Diethylphthalate 420
7005-72-3---..;---4-Chlorophenyl-phenylether __ 420
86-73-7---------Fluorene 420
100-01-6--------4-Nitroaniline 2000
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000
86-30-6---------N-Nitrosodiphenylamine (l)_ 420
101-55-3--------4-Bromophenyl-phenylether __ 420
118-74-1--------Hexachlorobenzene 420
87-86-5---------Pentachlorophenol 2000
85-01-8.---------Phenanthrene 420
120-12-1--------Anthracene 420
84-74-2---------Di-n-Butylphthalate 420
206-44-0--------Fluoranthene 420
129-oo-o--------Pyrene 420
85-68-7---------Butylbenzylphthalate 420
91-94-1---------3,3 1-Dichlorobenzidine 840
56-55-3---------Benzo(a)Anthracene 420
218-01-9--------Chrysene 420
. 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 420
117-84~0--------Di-n-octyl Phthalate 420
205-99-2--------Benzo(b)Fluoranthene 420
207-08-9--------Benzo(k)Fluoranthene 420
50-32-8---------Benzo(a)Pyrene 420
193-39-5--------Indeno(l,2,3-cd)Pyrene 420
53-70-3---------Dibenz(a,h)Anthracene 420
191-24-2--------Benzo(g,h,i)Perylene 420
(1) -Cannot be separated from Diphenylamine
Q
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u u u
u u u.
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u u u
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u u u
u u
u u
u u u u u u u
u u
u u
u
FORM I sv-2 1/87 Rev.
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lF . EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM « RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
MW7-4S-l
No.: 133
364103
Sample wt/vol: 30.l (g/mL) ~ Lab File ID: GH064lOJc20
Level: ( low/med) LOW
I Moisture: not dee.~ dee.
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) li_ pH:~
Number TICs found: ----1
CAS NUMBER COMPOUND NAME
Date Received: 08/10/90
Date Extracted: 08/17/90
Date Analyzed: 08/21/90
Dilution Factor: ~i~1 ~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q
•••==•=a•==•••=-•••z:====a====••==a••~•=====• •======a m=~:ai====z:==== --===
1. UNKNOWN 4.65 130 J
2. SOLVENT CONTAMINANT 4.70 380 BJ 3. PHTHALATE 18.09 170-J
FORM I SV-TIC 1/87 Rev.
20937 l 3~. 5/:U'IPLE~ TA .MMARY
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO,
MW7-4S-1RE Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 133
Matrix: (soil/water) SOIL Lab Sample ID: 364103
Sample wt/vol: 5,0 (g/mL) L-Lab File ID: GR064103Bl3
Level: (low/med) LOW Date Received: 08/10/90
I Moisture: not dee. _u Date Analyzed: 08/21/90
Column: (pack/cap) ~AE Dilution Factor: .1~1~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 u
74-83-9---------Bromomethane 13 u 75-01-4---------Vinyl Chloride 13 u 75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 17 B
67-64-1---------Acetone 41 B 75-15-o---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---~-----1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chlorotorm 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 5 BJ
71-55-6---------1,1,1-Trichloroethane 2 J
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane .6 u
10061-0l-5------cis-1,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane 6 u
71-43-2-----~---Benzene 6 u
10061-02-6------Trans-1,3-Dichloropropene_ 6 u
75-25-2---------eromotorm 6 u
1oa-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
,
-..;,,
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
MW7-4S-1RE
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ___ SDG No.: .._l,,,_33..____
Matrix: ( soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
, Moisture: not dee. ___ll
Column (pack/cap) Cl.P
Number TICS tound: ~
(g/mL) ~
Lab Sample .ID: ,3~6i4al~03,.__ __ _
Lab Fila ID: GR064103B13
Date Received: 08/10/90
Date Analyzed: 08/21/90
Dilution Factor: ·.1 ... ,0"'---
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
•••a••••-====•== ===a--=------------=--=---== ==••••=m ==i::::ua:::::=::r===m:a •===
1. LABORATORY ARTIFACT 0.75 5.1 J
FORM I VOA-TIC 1/87 Rev.
20937 133 SAMPLE DATA SUMMARY
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW6-4S-1REMS Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SOG No. : .1.,.3.,.3 __
Matrix: ( soil/water) SOIL Lab Sample ID: 364111
Sample wt/vol: s.o (g/mL) L_ Lab File ID: GRO/,i4 ll 1B l 3
-Level: · (low/med) LOW Date Received: 08/10/90
I Moisture: not dee. -2..3. Date Analyzed: 08/21/90
Column: (pack/cap) CAP Dilution Factor: .1~1~0'---
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 13 u
74-83-9-~-------Bromomethane 13 u
75-01-4---------Vinyl Chloride 13 u
75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 35 B 67-64-1---------Acetone 46 B
75-15-0---------carbon Disulfide 6 u
75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-o--------l,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 8 BJ
71-55-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-5------cis-l,3-Dichloropropene 6 u
79-01-6---------Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-00-5---------1,1,2-Trichloroethane . 6 u
71-43-2-~-------Benzene 6 u
10061-02-6------Trans-1,3-Dichloropropene __ 6 u
75-25-2---------Bromoform 6 u
1oa-10-1--------4~Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene . 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-5--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
.20937 133 SAMPLE DAT&, SUM~'r'
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW6-4S-1REMSD
Lab Name: COMPUCHEM.RTP Contract: 12-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ..,l,,_J J.___
Matrix: (soi 1/wa tar) SOIL Lab Sample ID: 364112
Sample wt/vol: 5,0 (g/mL) ~ Lab File ID: GR06411.l!l13
Level: (low/med) LOW Date Received: 08/10/90
I Moisture: not dee. ----2..J. · Date Analyzed: os1,1190
Column: (pack/cap) CAP Dilution Factor: .1~,-0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!,;i/K!,;i Q
74-87-3---------Chloromethane 13 u 74-83-9---------Bromomethane 13 u
75-01-4---------Vinyl Chloride 13 u
75-00-3---------Chloroethane 13 u
75-09-2---------Methylene Chloride 22 B
67-64-1---------Acetone 41 B
75-15-o---------carbon Disulfide 6 u 75-35-4---------1,1-Dichloroethene 6 u
75-34-3---------1,1-Dichloroethane 6 u
540-59-0--------1,2-Dichloroethene (total)_ 6 u
67-66-3---------Chloroform 6 u
107-06-2--------1,2-Dichloroethane 6 u
78-93-3---------2-Butanone 7 BJ
11-ss-6---------1,1,1-Trichloroethane 6 u
56-23-5---------carbon Tetrachloride 6 u
108-05-4--------Vinyl Acetate 13 u
75-27-4---------Bromodichloromethane 6 u
78-87-5---------1,2-Dichloropropane 6 u
10061-01-s------cis-l,3-Dichloropropene 6 u
79-01-6--------~Trichloroethene 6 u
124-48-1--------Dibromochloromethane 6 u
79-oo-s---------1,1,2-Trichloroethane 6 u
71-43-2---------Benzene 6 u
10061-02-6------Trans-l,3-Dichloropropene __ 6 u
75-25-2---~-----Bromoform 6 u
1os-10-1--------4-Methyl-2-Pentanone 13 u
591-78-6--------2-Hexanone 13 u
127-18-4--------Tetrachloroethene 6 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 6 u
108-88-3--------Toluene 6 u
108-90-7--------Chlorobenzene 6 u
100-41-4--------Ethylbenzene 6 u
100-42-s--------styrene 6 u
1330-20-7-------Total Xylenes 6 u
FORM I VOA 1/87 Rev.
20937 133 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW7-4S-1MS
Lab Name: CQMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol: 30.4 (g/mL). L_
Level: (low/med) _LO_W~-
\ Moisture: not dee . ....:...2.2. dee.
Extraction: (SepF/Cont/Sonc) ~
pH: _§_,_l GPC· Cleanup: (Y/N) Ii_
SDG No.: _1_3_3 __
Lab Sample ID: . _3~6~4-10-B ___ _
Lab File. ID: GH064108A2Q
Date Received: 08/10/90
Date Extracted: 08/17/90
Da.te Analyzed: 08/21/90
Dilution Factor: .1~1~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 420 u
lll-44-4--------bis(2-Chloroethyl)Ether 420 u
95-57-8---------2-Chlorophenol 420 u
541-73-1--------1,3-Dichlorobenzene 420 u
106-46-7--------1,4-Dichlorobenzene 420 u
100-51-6--------Benzyl Alcohol 420 u
95-50-1---------1,2-Dichlorobenzene 420 ·U
95-48-7---------2-Methylphenol 420 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 420 u
106-44-5--------4-Methylphenol 420 u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 420 u
67-72-1---------Hexachloroethane 420 u
98-95-3---------Nitrobenzene 420 u
78-59-1---------Isophorone 420 u
88-75-5---------2-Nitrophenol 420 u
105-67-9--------2,4-Dimethylphenol 420. u
65-85-0---------Benzoic Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 420 u
120-83-2--------2,4-Dichlorophenol 420 u
120-82-1--------1,2,4-Trichlorobenzene 420 u
91-20-3---------Naphthalene 420 u
106-47-8--------4-Chloroaniline 420 u
87-68-3---------Hexachlorobutadiene 420 u
59~50-7---------4-Chloro-3-Methylphenol 420 u
91-57-6---------2-Methylnaphthalene 420 u
77-47-4---------Hexachlorocyclopentadiene __ 420 u
88-06-2---------2,4,6-Trichlorophenol 420 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 420 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 420 u
208-96-8--------Acenaphthylene 420 u
606-20-2--------2,6-Dinitrotoluene 420 · u
FORM I sv-1 1/87 Rev.
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS MW7-4S-1MS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 133
Matrix: (soil/water) SOIL Lab Sample ID: 364108
Sample wt/vol: 30.4 (g/mL) ~ Lab File ID: GH06410BA20
Level: (low/med) LOW Date Received: 08/10/90
I Moisture: not dee. ~ dee. Date Extracted: 08/17l9Q
Extraction: (SepF/Cont/Sonc) ~ · Date Analyzed: 08l21l90
GPC Cleanup: (Y/N) lL_ pH: _.L.1 Dilution Factor: .1~1~0 __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UGlKG
99-09-2---------3-Nitroaniline 2000 83-32-9---------Acenaphthene 420 51-28-5---------2,4-Dinitrophenol 2000 100-02-1--------4-Nitrophenol 2000 132-64-9--------Dibenzofuran 420
121-14-2--------2,4-Dinitrotoluene 420
84-66-2---------Diethylphthalate 420 7005-72-3-------4-Chlorophenyl-phenylether __ 420 86-73-7---------Fluorene 420 100-01-6--------4-Nitroaniline 2000 534-52-1--------4,6-Dinitro-2-Methylphenol __ 2000 86-30-6---------N-Nitrosodiphenylamine (1)_ 420 101-55-3--------4-Bromophenyl-phenylether __ 420
118-74-1--------Hexachlorobenzene 420
87-86-5---------Pentachlorophenol 2000
85-01-8---------Phenanthrene 420 120-12-1--------Anthracene 420
84-74-2---------Di-n-Butylphthalate 420
206-44-0--------Fluoranthene 420
129-00-o--------Pyrene 420
85-68-7---------Butylbenzylphthalate 420
91-94-1---------3,J'-Dichlorobenzidine 830
56-55-3---------Benzo(a)Anthracene 420
218-01-9--------Chrysene 420
117-81-7--------bis(2-Ethylhexyl)Phthalate_. 420
117-84-0--------Di-n-octyl Phthalate 420
205-99-2--------Benzo(b)Fluoranthene 420
207-08-9--------Benzo(k)Fluoranthene 420
50-32-8---~-----Benzo(a)Pyrene 420
193-39-5--------Indeno(l,2,3-cd)Pyrene 420
53-70-3---------Dibenz(a,h)Anthracene 420
191-24-2--------Benzo(g,h,i)Perylene 420
(1) -Cannot be separated from Diphenylamine
u u u
U.
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u u
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u u . u
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FORM I SV-2 1/87 Rev.
20937 133 $AMF'Lf,t DRT£1T$UMMRRY.,c:.
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
HW7-4S-1MSD Lab Name: COMPUCHEM,RTP Contract: /2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 133
Matrix: (soil/water) SOIL Lab Sample ID: 364109
Sample wt/vol: 30.4 (g/mL) ~ Lab File ID: GH064109A20
Level: (low/med) LOW Date Received: 08£'.10£'.90
I Moisture: not dee. --1.2. dee. -Date Extracted: 08£'.17£'.90
Date Analyzed: 08£'.21£'.90 Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) H...._ pH: .....§....2. Dilution Factor: .1~1~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG£'.KG Q
•.
108-95-2--------Phenol 420 u lll-44-4--------bis(2-Chloroethyl)Ether 420 u 95-57-8---------2-Chlorophenol 420 u
541-73-1--------1,3-Dichlorobenzene 420 u 106-46-7--------1,4-Dichlorobenzene 420 u
100-51-6--------Benzyl Alcohol 420 u
95-50-1---------1,2-oichlorobenzene 420 u 95~48-7---------2-Methylphenol 420 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 420 u
106-44-5--------4-Methylphenol 420 u 621-64-7--------N~Nitroso-oi-n-Propylamine __ 420 u
67-72-1---------Hexachloroethane 420 u
98-95-3---------Nitrobenzene 420 u
78-59-1---------Isophorone 420 u
88-75-5---------2-Nitrophenol 420 u
105-67-9--------2,4-Dimethylphenol 420 u
65-85-o---------Benzoic Acid 2000 u
lll-91-l--------bis(2-Chloroethoxy)Methane __ 420 u
120-83-2--------2,4-Dichlorophenol 420 u
120-e2-1--------1,2,4-Trichlorobenzene 420 u
91-20-3---------Naphthalene 420 u
106-47-8--------4-Chloroaniline 420 u
87-68-3---------Hexachlorobutadiene 420 u
59-50-7-----~---4-Chloro-3-Methylphenol 420 u
91-57-6---------2-Methylnaphthalene 420 u
77-47-4---------Hexachlorocyclopentadiene __ 420 u
ee-06-2---------2,4,6-Trichlorophenol 420 u
95-95-4---------2,4,5-Trichlorophenol 2000 u
91-58-7---------2-Chloronaphthalene 420 u
88-74-4---------2-Nitroaniline 2000 u
131-11-3--------Dimethyl Phthalate 420 u
208-96-8--------Acenaphthylene 420 u
606-20-2--------2,6-Dinitrotoluene 420 u
FORM I sv-1 1/87 Rev.
20932~133 SAMPEE=DATArSUMMARY .:.
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I lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
I Lab Name: CQMPUCHEM. RTP
MW7-4S-1MSD
Contract: (2-88l-REVS
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Lab Code: COMPU case No.: 20937 SAS No.: SOG No.: ..,13...,3.___
Matrix: (soil/water) SOIL Lab. Sample IO: .3_§~4..,10.,_9.._ __ _
sample wt/vol: 30,4 (g/mL) L--Lab File ID: GH064109A20
(low/med) _to-w __
I Moisture: not dee. __u_ dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) L_ pH: JJ.
Date Received: 08/10/90
Date Extracted: 08/17/90
Date Analyzed: 08/21/90
Dilution Factor: _1~,o.._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline
2000 u
83-32-9---------Acenaphthene
420 u
51-28-5---------2,4-Dinitrophenol
2000 u
100-02-1--------4-Nitrophenol
2000 u
132-64-9--------Dibenzofuran
420 u
121-14-2--------2,4-Dinitrotoluene
420 u
84-66-2---------0iethylphthalate
420 u
7005-72-3-------4-Chlorophenyl-phenylether_

420 u
86-73-7---------Fluorene
420 u
100-01-6--------4-Nitroaniline
2000 u
534-52~1--------4,6-Dinitro-2-Methylphenol_

2000 u
86-30-6---------N-Nitrosodiphenylamine
(l)_ 420 u
101-55-3--------4-Bromophenyl-phenylether
__ 420 u
118-74-1--------Hexachlorobenzene
420 u
87-86-5---------Pentachlorophenol
2000 u.
85-01-8---------Phenanthrene
420 u
120-12-1--------Anthracene
420 u ..
84-74-2---------Di-n-Butylphthalate
420 u
206-44-0----~---Fluoranthene
420 u
129-oo-o------~-Pyrene
420 u
85-68-7---------Butylbenzylphthalate
420 u
91-94-1---------3,3'-Dichlorobenzidine
830 u
56-55-3---------Benzo(a)Anthracene
420 u
218-01-9--------Chrysene
420 u
117-Bl-7--------bis(2-Ethylhexyl)Phthalate_
96 J
111-s4-o--------oi-n-octyl Phthalate 420 u
205-99-2--------Benzo(b)Fluoranthene
420 u
207-08-9--------Benzo(k)Fluoranthene
420 u
· 50-32-8---------Benzo(a)Pyrene
420 u
193-39-5--------Indeno(l,2,3-cd)Pyrene
420 u
53-70-3---------Dibenz(a,h)Anthracene
420 u
191-24-2--------Benzo(g,h,i)Perylene
420 u
(1) -CaMot be separated from Diphenylamine
FORM I sv-2 1/87 Rav.
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