NCD980840409_19891101_Charles Macon Lagoon & Drum_FRBCERCLA RI_RI FS Study Remedial Investigation Report - Volume IV Continued-OCR

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MACON/DOCKERY NPL SITE
REMEDIAL INVESTIGATION/
FEASIBILITY STUDY
REMEDIAL INVESTIGATION REPORT
VOLUME IV CONTINUED
)
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Q)MPUCHEM
l.AroMrC>RJES, INC. P.O. Box 12652 3308 Chapel Hill/ Nelson Highway Res•~arch Triangle Park. NC 27709 (919) ~49-8263
CLP CASE NARRATIVE CASE# 20937
.CONTRACT# 2/88 (REVS) SDG# 148
COMPUCHEM LABORATORIES INC.
SAMPLES: FB-02-1
This portion of Case# 20937 consisted of one liquid sample
for volatile and semivolatile analysis. It was received
intact on 8/10/90 in a properly sealed shipping container
with a traffic report. Because the sample, was designated as
a blank, there are no associated QC spikes.
VOLATILES:
All volatile
requirements. fractions were analyzed within holding time
The sample contained methylene chloride
the associated instrument blank) and
chloroform was deter~ined not to be
(also detected in
chloroform. The
carryover from a
recovery cri ter_ia.
previous sample. All surrogates met
SEMIVOLATILES:
All semivolatile fractions were extracted a.nd analyzed within
holding time requirements. The sample contained· no target
compounds. All surrogates met recovery criteria.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than the conditions detailed
above. Release of the data contained in this hardcopy data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
Note: This report was paginated for reference and
accountability in decreasing numerical sequence.
-·-"
G2>()J~Ql~
Sarah A. Hubbard 9/28/90
Technical Reviewer
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: il.=-eS)-REVS
FB-02-1
Lab Code: COMPU Case No.: 20937 SAS No.: S DG No. : ..._14....,8..___
Matrix: (soil/water) WATER Lab Sample ID: 364104
Sample wt/vol: 5.0 (g/mL) M!,__ Lab File ID: CN064104AI1
Level: (low/med) .,,LO.,_,w,___ Date Received: 08/10/90
Date Analyzed: O!l/16/90 \ Moisture: not dee.
Column: (pack/cap) CAP Dilution Factor: .1~1 .0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or uc;'jl<g) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 11 B
67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_, 5 u
67-66-3---------Chloroform 16 -107-06-2--------1,2-Dichloroethane -5 u
78-93-3---------2-Butanone 10 u -71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u -78-87-5---------1,2-Dichloropropane -.5 u
10061-01~5------cis-l,3-Dichloropropene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ : 5 u
79-01-6---------Trichloroethene 5 .U -124-48-1--------Dibromochloromethane 5 u
79-00-5.---------1, 1, 2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
75-25-2---------Bromoform 5 u -1oa-10-1--------4-Methyl-2-Pentanone -10 u
591-78-6--------2-Hexanone 10 u -127-18-4--------Tetrachloroethene 5. u
79-34-5---------1,1,2,2-Tetrachloroethane ___ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene s u -100-41-4--------Ethylbenzene 5 u -100-42-5--------styrene s u -1330-20-7-------Total Xylenes s u --
FORM I VOA 1/87 Rev.
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM, RTP Contract: l.1=!!8)-REVS
EPA SAMPLE NO.
FB-02-1
Lab Code : COMPU · Case No.: 20937 SAS No.: S 0G No• : ..,1~4..,.8 __
Matrix: ( soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ~
Level: ( low/med) LOW
t Moisture: not dee.
Extraction:
GPC C~eanup:
(SepF/Cont/Sonc)
(Y/N) lL_
Number TICS found: ---1
dee ..
pH:
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab :rile IO:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or u9/Kg) UG/L
R'r EST.
364104
CN064104AI1
08/10/90
08/16/90
1,0
CONC. Q ===========~==== =-=----------==---=-------=-========= ----=--===---===== 1. 102-24-9 LABORATORY ARTIFACT 3.20 8.0 J
FORM I SV-TIC 1/87 Rev.
20937 148 SAMPLE DATA PACKAGE 20
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP contract: /2-88)-REVS FB-02-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 148
Matrix: (soil/water) WATER Lab Sa!llple ID: 364104
Sample wt/vol: 500 (g/mL) MI,_ Lab File ID: GH064104A07
Level: ( low/med) LOW Date Received: 08/10/90
t Moisture: not dee. dee. Date Extracted: 08/11,/90
Extraction: (SepF/Cont/Sonc) SEPF
GPC Cleanup: (Y/N) li,__ pH:
Date Analyzed: 08/12/90
Dilution Factor: 0.50
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene '
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--~-----2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane __
120-83-2--------2,4-Dichlorophenol
120-a2-1--------1,2,4-Trichlorobenzene
91-20-3-----~---Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I SV-1 1/87 Rev.
20937 1is SAMPLE DATA PACKAGE
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EFA SAMPLE NO,
FB-02-1 Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 148
Matrix: (soil/water) WATER Lab Sample ID: 364104
Sample wt/vol: 500 (g/mL) lil,_ Lab File ID: GH0641C4A07
Level: (low/med) ~LO~W.!!__ Date Received: 08/10/90
% Moisture: not dee. dee. Date Extracted: 08/11(90
Extraction: (SepF/Cont/Sonc) 5_E.P.E Date Analyzed: 08/12/90
GPC Cleanup: (Y/N) li...._ pH: Dilution Factor: 0.50
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline so u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3---~~--4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6----~----N-Nitrosodiphenylamine (1)_ 10 u
101-55-3--------4-Bromophenyl-phenyl_ether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
ss-01-s---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-00-0--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--~----~chrysene 10 u
. 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------Di-n-Octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3------~--Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev.
20937 148 SAMPLE DATA PACKAGE
Q
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab·Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 500 (g/mL) lil..._ Lab File ID:
Level: ( low/med) LOW Da-te Received:
t Moisture: not dee. dee. Date Extracted:
EPA SAMPLE NO.
FB-02-1
No.: 148
364104
GH064104A07
08/10/90
Q!Ull/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li.,_ pH:
Date Analyzed: 08/12/90
Dilution Factor: 0.50
Number TICs found: _Q_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I SV-TIC 1/87 Rev.
20937 148 SRMPEE)DRTR PACKAGE 1 7
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,
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW8-4S-2
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 94
Matrix: (soil/water) SOIL Lab Sample ID: 362492
Sample wt/vol: 30.0 (g/mL) L_ Lab File ID: GH062492B15
Level: (low/med) rpw Date Received: 08/04/90
% Moisture: not dee.~ dee. Date Extracted: 0§/08/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 08/22/90
GPC Cleanup: (Y/N) lL_ pH: ...2...,_,1 Dilution Factor: zl~-~o~o __
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Nitroaniline 2200
83-32-9---------Acenaphthene 460
51-28-5-------~-2,4-Dinitrophenol 2200
100-02-7--------4-Nitrophenol 2200
132-64-9--------Dibenzofuran 460
121-14-2----~---2,4-Dinitrotoluene 460
84-66-2---------Diethylphthalate 460
7005-72-3-------4-Chlorophenyl-phenylether __ 460
86-73-7---------Fluorene 460
100-01-6-------~4-Nitroaniline · 2.200
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2200
86-30-6---------N-Nitrosodiphenylamine (l)_ 460
101-55-3--------4-Bromophenyl-phenylether __ 460
118-74-1--------Hexachlorobenzene 460
87-86-5~--------Pehtachlorophenol 2200
85-01-8---------Phenanthrene 460
120-12-1--------Anthracene 460
84-74-2---------Di-n-Butylphthalate 460
206-44-0--------Fluoranthene 460
129-00-0--------Pyrene 460
85-68-7------~--Butylbenzylphthalate 460
91-94-1---------3,3'-Dichlorobenzidine 920
56-55-3---------Benzo(a)Anthracene 460
218-01-9--------Chrysene 460
117-81-7--------bis(2-Ethylhexyl)Phthalate __ 460
117-84-o~-------oi-n-Octyl Phthalate 60
205-99-2--------Benzo(b)Fluoranthene 460
207-08-9--------Benzo(k)Fluoranthene 460
50-32-8---------Benzo(a)Pyrene 460
193-39-5--------Indeno(l,2,3-cd)Pyrene 460
53-70-3---------Dibenzo(a,h)Anthracene 460
191-24-2--------Benzo(g,h,i)Perylene 460
(1) -Cannot be separated from D1phenylam1ne
u
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u
FORM I SV-2 1/87 Rev.
20937 ~4 SUNNHR\., ,·.;..
Q
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COMPUCHEM
lABORATORlES
CLP CASE NARRATIVE CASE# 20937
CONTRACT# 2-88 (REVS) SDG# 150
COMPUCHEM LABORATORIES INC.
SAMPLES: PW-02-1, PW-03-1, PW-03-2, PW-04-1, PW-05-1,
PW-06-1, PW-07-1
This portion of Case # 20937 consisted of eight liquid
samples for volatile and semivolatile analysis. They were
received intact on 8/17/90 and 8/21/90 via Federal Express in
properly sealed shipping containers with traffic reports.
VOLATILES:
With the exception of the reanalysis of sample PW-02-1 and
the matrix spike duplicate, all volatile fractions were
analyzed within holding time requirements. Samples PW-03-01,
PW-03-2, and PW-05-1 contained no target compounds. Two
analyses were reported for sample PW-02-1 in order to have
one reported analysis with in holding time requirements. The
first analysis had no reportable target compounds and the
second had methylene chloride and acetone, which were also
detected in the associated instrument blank. Sample PW-04-1
contained methylene chloride and acetone (detected in the
associated fnstrument blank). Sample PW-06-1 contained
methylene chloride, total 1,2-dichloroethene, 1,2-
dichloroethane, 1,1,1-trichloroethane, bromodichloromethane,
dibromochloromethane, cis-and trans-1,3-dichloropropene,
tetrachloroethene, toluene, and chlorobenzene. Sample PW-07-1
contained trichloroethene, which was also detected in the
associated instrument blank. All surrogates met recovery
criteria. The matrix spike/matrix spike duplicate results
were acceptable. The %RPO for 1,1-dichloroethene exceeded QC
limits.
SEMIVOLATILES:
With the exception of the sample spikes, all semivolatile
fractions were extracted and analyzed within holding time
requirements. Samples PW-02-1, PW-3-1, and PW-05-1 contained
no target compounds. Samples PW-04-1 and PW-07-1 contained
bis (2-ethylhexyl) phthalate. Sample PW-06-1 contained
phenol, bis ( 2-chloroethyl) ether, 2-chlorophenol, 4-
methylphenol, hexachloroethane, isophorone, 2,4-
dinitrophenol, pentachlorophenol, acenaphthene, phenanthrene,
pyrene, bis ( 2-ethyLhe>:yL) phthalate, and benzo (b)
fluoranthene. All surrogates met recovery criteria. The
matrix spike/matrix spike duplicate results were acceptable.
COMPUCHEM LABORATORIES. INC. P.O. Box 12652 3308 Chapel Hi!I/Nelson Highway Research Triangle Park_. NC 27709 [phone] I ·_' I
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----CbMPUCHEM
lABOAATORJES
I c~rtify that this data package is in compliance with the
terms and conditions of the contract, both iechnically and
for completeness, for other than the conditions detailed
above. Release of the data contained in this hardcopy data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
Note: This report was paginated for reference and
accountability in decreasing numerical sequence.
?age -2
;
__,,,,Ja1LOU
Sarah A. Hubbard 9/11/90
Tech~ical Reviewer
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-02-1
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab sample ID: 365249
Sample wt/vol: s.o (g/mL) tu..._ Lab File ID: CN065249AOJ
Level: (low/med) LOW Date Received: 08/17/90
Date Analyzed: 08/25/9Q I Moisture: not dee.
Column: (pack/cap) CAP Dilution Factor: ~l~•~Q'---
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane ·10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 5 u 67-64-1---------Acetone 10 u 75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u 56-23-5---------carbon Tetrachloride 5 u 108-05~4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ . 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylene& 5 u
FORM I VOA l/87 Rev.
209i7 150 SAMPLE DATR SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RT°P contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: ( soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) Hl,,_ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. Date Analyzed:
EPA SAMPLE NO.
PW-02-1
No.: 150
365249
CN065249AQJ
08/17/90
08/25/90
Column (pack/cap) CAP Dilution Factor: .i~·~o __
Number TICs found: __Q
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. •••••••~==ma==•• --=-====---=-==-----=-==-=== --------•••••==-••a:ama
FORM I VOA-TIC 1/87 Rev.
20937 l50.SAMPLE QATA SUMMARY
,1 i ~• :;,.4 -_;t1r ..=,:._;
Q
--===
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-02-lRE Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .._15...,0.___
Matrix: (soil/water) WATER Lab Sample IO: 365249
Sample wt/vol: 5.0 (g/mL) ~
LOW
Lab File IO: CR065249C03
Level: ( low/med) Date Received: 08/17/90
\ Moisture: not dee.
Column: (pack/cap) CAP
Date Analyzed: 08/30/90
Dilution Factor: ~i~·~O:..._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 1 BJ
67-64-1---------Acetone 8 BJ 75-15-o---------carbon Disulfide 5 u
75-35-4-----~---l,l-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u
540-59-o--------l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-oichloroethane 5 u 78-93-3---------2-Butanone 10 u .
71-55-6~--------l,.l,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u 78-87-5---------1,2-Dichloropropane 5 u
10061-0l-S------cis-l,J-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,J-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Kexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 15~ SAMPLE DATA SUMMARY
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88}-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab sample IO:
Sample wt/vol:, 5.0 (g/mL) lil,__ Lab, File ID:
Level: (low/med) LOW Date Received:
\ Moisture: not dee. Date Analyzed:
EPA SAMPLE NO.
PW-02-lRE
No.: 150
365249
CRQ65249C03
08/17/90
08/301'.90
Column (pack/cap) CAP Dilution Factor: .i~,o,._ __
Number TICs found: _l
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC.
an============== ============================ a======= ========•==1111=
l. LABORATORY ARTIFACT 9.19 e.o
•
FORM I VOA-TIC 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY '""!' _ _ _,It r
Q
c====
:r
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-03-1
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No. : ,.1.,.5.,.0 __
Matrix: (soil/water) WATER Lab sample ID: 365254
Sample wt/vol: 5.0 (g/mL) Ml,__ Lab File ID: CN065254A03
Level: (low/med) LOW Date Received: 08/17/90 I 'Moisture: not dee. Date Analyzed: oaa§l'.29
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I
Column: (pack/cap) CAP Dilution Factor: ,.1~0.,.0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG,:'.L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64-1---------Acetone 10 u
75-15-o-------~-carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,l-Dichloroethane 5 u
540-59-o--------l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6----~----l,l,l-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-s~--------l,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
ios-10-1--------4-Methyl-2-Pentanone 10 u
59.1-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 150 SAMPCE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
PW-03-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ..,1""50...__
Matrix: (soi 1/wa ter) WATER
Sample wt/vol: 5,0 (g/mL) m....._
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Nwnkler TICS tound: ---2.
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
365254
CN065254A03
08/17/90
08/26/90
1,0
CONC. Q
•••••••••=•=n==• •nammma=------=--=•==-=-===• ••az:s=•a• •••a=•••••••• ---==
FORM I VOA-TIC 1/87 Rev.
20937 -15.0 SA/'1PL.£.. DATA SLJ_mrtARY.-·
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-03-2 Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ,.1..,.5.x0 __
Matrix: ( soil/water) WATER Lab Sample ID: 365260
Sample wt/vol: 5.0 (g/mL) Ml,_ Lab File IO: CN065260AOJ
Level: (low/med) I.OW Date Received: 08/17/90
I Moisture: not dee. Date Analyzed: 08/26/90
Column: (pack/cap) CAP Dilution Factor: .. i~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L . Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 5 u
67-64~1---------Acetone 10 u
75-1~-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chlorotorm 5 u
107-06-2--------1,2-oichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-S------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5-----~---l,l,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromotorm 5 u
ioe-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,l,2,2-Tetrachloroethane __ 5 u
108-BB-J--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
lJJo-20-1-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
I • ' 1501SAMPL~ DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
PW-OJ-2
Lab Code: COMPU Case No.: 20937 SAS No.: S DG No • : .._15...,0..___
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LQW
\ Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: __o_
CAS NUMBER COMPOUND
tU.,_
NAME
Lab Sample ID: 365260
Lab File ID: CN06526QA03
Date Received: 08/17/90
Date Analyzed: O!l/26/90
Dilution Factor: .i~,~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
------=--•-====-acaaa-=-------==-====--=-==• •amazn::u::::::::a CIICa:a==m::u:::•••• •==-=•
FORM I VOA-TIC 1/87 Rev.
20937 15~, SAMPLE DR.TA. S,UMMARY,.,
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-04-1
Lab Name: CQMPUCHEM,RTP Contract: (2-881-REVS
Lab code: COMPU case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365991
Sample wt/vol: 5.0 (g/mL) tu...._ Lab File ID: CN065991A03
Level: (low/med) LOW Date Received: 08/21/90
I Moisture: not dee. Date Analyzed: 08/30/90
Column: (pack/cap) CAP Dilution Factor: .1~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q •
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 1 J
67-64-1---------Acetone 7 BJ
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-o----~---l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---.------1, l, 2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6--~---Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromotorm 5 u
1oa-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5----'-----l 1 2 2-Tetrachloroethane , , , --5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
I 1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-BBl-REVS
EPA SAMPLE NO.
PW-04-l
Lab Code: COMPU Case No.: 20937 SAS No.: S 0G No • : .,15...,o.___
Matrix: (soil/water) WATER
sample wt/vol: s,o (g/mL)
Level: (low/med) I,PW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: ----2
CAS NUMBER COMPOUND
!il....,_
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
365991
CN065991A03
08/21/90
08/30/90
1.0
CONC. Q •=--•-====----=-••=-m-----=----------------= ======== •======-----== •====
FORM I VOA-TIC 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY
; ,., ;-· . ' ' - ' ,j /'I ,1( y
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·1
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MWSA-01-1
Lall Name: CQMPUCHEM,RTP contract: r2-eel-REVS
Lab Code: COMPU Ca■e No.: 20937 SAS No.: SDG No,: -.2-15.__
Matrix: (■oil/water) WATER Lab Sample ID: 367830
Sample wt/vol: 1000 (g/mL) m..._ Lab File ID: GH067830A07
Level: (low/med) LOW Date Received: 08/31/90
\ Moisture: not dee. dee. Date Extracted: 08/31/90
• Extraction: (SepF/Cont/Sonc) .$lll Data Analyzed: 09/04/90
GPC Cleanup: (Y/N) lL._ pH: Dilution Factor: ~1~,~o __
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Xg) UG/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bis(2-Chloroathyl)Ethar 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzena 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5----~---4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3-~-------Nitrobenzene 10 u
78-59-1---------Isophorone 10. u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,,-Trichlorobenzene 10 u -
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4----------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Ch_loronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPO Caae No.: 20937 SAS No.: ___ SDG No.: . ..,2..,15.___
Matrix: (aoil/water) WATER Lab Sample ID: .,.J.,.6.._7.,..8.._30,._ __ _
Sample wt/vol: 1000 (9/mL) ML..._ Lab File ID: GH0§7830A07
Level: (low/med) LOW Date Received:. 08/31/90
I Moisture: not dee. dee. Date Extracted: 08/31/90
Date Analyzed: 09/04/90
Dilution Factor: al.._1 0,._ __
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) Ii_
ilU
pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:.
(ug/L or u9/K9) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzoturan
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether_
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3 1 -Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene .
218-01-9--------Chrysene
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------Di-n-octyl Phthalat•
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyren•
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(l) -Cannot be separated from Diphenylamin•
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
-
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••
lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPQCHEM.RTP Contract: 12-88)-REVS
Lab Code: CQMPQ Ca■■ No.: 20937 SAS No.: ___ SDG No.: _21,..5.___
Matrix: (■oil/water) WATER Lab Sample ID: al&§~ZB~J~o._ __ _
Sample vt/vo;: 1000 (g/mL) ~ Lab File ID: GH0§78J0A07
Level: (low/med) LOW
I Moisture: not dee.
Extraction:
GPC Cleanup:
( SepF /Cont/sonc)
(Y/N) .tL_
Number TICS tound: __,O
dee.
pH:
CAS NUMBER COMPOUND
.s.E.Pl
NAME
Date Receive.Jl:_ 0B/31/90
Date Extracted.: 0B/31/90
Date Analyzed: 09/04/90
Dilution Factor: .1~,o._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
----------------------------===-----------------------------
FORM I SV-TIC 1/87 Rev.
20937 215\ SAMP~t DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-0l-l Lab Name: CQMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: CQMPU caae No.: 209J7 SAS No.: ___ SOG No.: ,11.21...,5,...___
Matrix: (■oil/water) WATER Lab Sample ID: .,3.,67""'8..,3.._7.__ __ _
Sample wt/vol: 1000 (g/mL) m._ Lab File ID: GH067837A07
Level: (low/med) LOW
I Moi ■ture: not dee. dee.
Date Received~ 08/31/90
Date Extracted: 08/31/90
Date Analyzed: 09/04/90
Dilution Factor: .1~1 0.,_ __
Extraction: (SepF/Cont/Sonc) llP[
GPC Cleanup: (Y/N) L-pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether . 95-57-8---------2-Chlorophenol
541-73-1--------1,3-0ichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol 95-50-1-----~---1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic Acid lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1--------1,2,4~Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47~4---------Hexachlorocyclopentadiene_
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-J--------Dimethyl Phthalate 208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2 J
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 215 SAMPLE DATA SUMMRRY
Q
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-0l-l
Lab Name: COMPQCHEM « RTP Contract: (2-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ._2.,15......__
Matrix: (■oil/water) WATER Lab Sample IO: .J.,.6.,_7,._83,._7.,__ __ _
sample wt/vol: 1000 ( g/mL) Ml«...... Lab File ID: GH067837A07
Level: (low/med) LOW
I Moisture: not dee.
Extraction: (SepF/Cont/Sonc)
dee.
Date Received~ 08/31/90
Date Extracted: OB/31/90
Date Analyzed: 09/04/90
GPC Cleanup: (Y/N) Ji_ pH: Dilution Factor: _1~,o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acenaphthene ' 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7-~-------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether_ 10 u
118-74-1------~-Hexachlorobenzene 10 u
87-86-5----~----Pentachlorophenol 50 u
ss-01-s---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u -129-00-0--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1--~------J,3 1-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9----~---Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 4 J
117-84-o--------Di-n-Octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-B---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -Cannot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
2093? 215 SAMPLE DATA SUMMARY
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lF EPA.SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
I.ab Name: CQMPUCHEM,RTP Contract: 12-88}-REYS
MW9-0l-l
Lab Code: CQMPY Ca■e No.: 20937 SAS No.: ___ SDG No.: ... 2.._1sot.--_
Matrix: (■oil/water) WATER Lab Sample ID: &J.,..67,_8,._3._7'-----
Sample wt/vol:· 1000
LOW
(g/mL) Ml._ Lab File ID: GH067837A07
· Level: (low/med)
I Moi ■ture: not dee.
Extraction:
GPC Cleanup:
( SepF /Cont/Sonc)
(Y/N) u_
Number TIC• found: ---2
dee.
uu
pH:
CAS NUMBER COMPOUND NAME
Date Received~ 08/31/90
Date Extracted: 08/31/90
Date Analyzed: 09/04/90
Dilution Factor: .1.._.o.._ __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
-••••••••••a••• ------------=--=--=--=-2••----------------------===
1. 20324-32-7 2-PROPANOL, 1-(2-METHOXY-l-M 6.33 24 J
2. UNKNOWN 17.69 12 J
3. UNKNOWN 17.85 12 J -
FORM I SV-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
-
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REYS MW2A-Ol-1MS
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: _.2,.1..,5 __
Lab Sample ID: 3§7§4§· Matrix: (aoil/vatar) WATER
Sample wt/vol: · 500 (g/111L) tlL_ Lab File ID: GH0§7§46A07
Level: ( low/med) LOW
I Moisture: not dee. dee.
Date Receive4:-08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/01/90
Dilution Factor: 0.50
Extraction: (SepF/Cont/Sonc) gu
GPC Cleanup: (Y/N) tL_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u lll-44-4--------bis(2-Chloroethyl)Ether 10 u 95-57-8---------2-Chlorophenol 10 u 541-73-1--------1,3-Dichlorobenzene 10 u 106-46-7--------1,4-Dichlorobenzene 10 u 100-.51-6--------Benzyl Alcohol 10 u 95-50-1---------1,2-Dichlorobenzene 10 u 95-48-7---------2-Methylphenol 10 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u 106-44-5--------4-Methylphenol 10 u 621-64-7--------N-Nitroso-Di-n-Propylamine __ 10 u
67-72-1---------Hexachloroethane 10 u 98-95-3---------Nitrobenzene 10 u 78-59-1---------Isophorone 10 u 88-75-5------~--2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u lll-91-l--------bis(2-Chloroethoxy)Methane_ 10 u 120-83-2--------2,4-Dichlorophenol 10 u -120-e2-1--------1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u 106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-J-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47~4---------Hexachlorocyclopentadiene __ 10 u
88-06-2~--------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO, SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW2A-01-1MS
Lab Name: CQMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: S 0G No • : ..,2 1....,5.___
Matrix: (soil/water) WATER Lab Sample ID: .3~§L7&§4~§,._ __ _
Sample wt/vol: 500 (g/mL) Ml._ Lab File ID: GH0§7§4§A07
Level: (low/med) leQH
I Moisture: not dee. dee.
Date Received: 08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/01/90
Dilution Factor: &o~,5~oL-_
Extraction: (SepF/Cont/Sonc) .slll
GPC Cleanup: (Y/N) li.,_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9-~-----~-Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophanol 50 u
132-64-9--------Dibanzoturan 10 u
121-14-2--------2,4-Dinitrotoluena 10 u
84-6~-2---------Diathylphthalate 10 u
7005-72-3-------4-Chlorophanyl-phanylathar_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1----·----4, 6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphanylamine (1)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1------~-Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-00-0--------Pyren• 10 u ..
85-68-7---------Butylbenzylphthalate 10 u
91-94-1-----~---3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------oi-n-octyl Phthalat• 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
_ 193-39-5--------Indeno ( 1, 2, 3-cd) Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylen• 10 u
(1) -Cannot be aeparatad trom Diphenylamin•
FORM I sv-2 1/87 Rev.
20937 21~ SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO.
SE:MIVOLATILE ORGANICS ANALYSIS DATA SHEET \
MW2A-Ol-1MSD
Lab Name: CQMPUCHE'M,RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: ___ SDG No.: ._2..,15.___
Matrix: (■oil/water) WATER Lab Sample ID: ,.3.,.§.._7.,.§:,,.47,..._ __ _
Sample wt/vol: 500 (g/mL) m,__ Lab File IO: GH0§7647f,07
Level: (low/med) UlW
I Moisture: not dee. dee.
Oat• Receive4:-08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/01/90
Dilution Factor: 0.50
Extraction:
GPC Cleanup:
CAS NO.
(SepF/Cont/Sonc)
(Y/N) L_ pH:
COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8-------~-2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1-----~---1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
111-91-1--------bia(2-Chloroethoxy)Methane_
120-eJ-2--------2,4-Dichlorophenol
120-e2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2~Methylnaphthalene ·
77-47-4---------Hexachlorocyclopentadiene __
BB-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7----~----2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-e--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
. 10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
--
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW2A-Ol-1MSD
Lab Name: CQMPYCHEM, RTP Contract: C2-BB)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ._2 .. 15....__
Matrix: (soil/water) WATER Lab Sample ID: .,3.,.6.,_7,.;64,._7,__ __ _
Sample wt/vol: 500 (g/mL) Ml,._ Lab File ID: GH067647A07
Level: (low/med) LOW
I Moisture: not dee. dee.
Date Receiv~:-08/30/90 ·
Date Extracted: OB/31/90
Data Analyzed: 09/01/90
Dilution Factor: .,.o.._,5...,o....__
Extraction: (SepF /Cont/Sonc) .ilPl
GPC Cleanup: (Y/N) H_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2-~-------J-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------oiethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether_ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-e---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------oi-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u -129-00-0--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1--~------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9----~---Chryaen• 10 u
111-s1-1--------bia(2-Ethylhexyl)Phthalate_ 10 u
117-84-0--------Di-n-Octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207.-08-9--------Benzo (k) Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylena 10 u
(l) -CaMot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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COMPUCHEM
~, {f\JC:. P.O. Bo• 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park. NC 27709 [phone]
CLP CASE NARRATIVE CASE# 21492
CONTRACT# 2-88 (REVS) SDG# 01
COMPUCHEM LABORATORIES INC.
SAMPLES: MW18-15-l, MW20-35-l, SB18-35-l, SB19-3S-l,
SB20-3S-l, SB21-3S-l, SB22-3S-l
This portion of Case# 21492 consisted of seven solid samples
for volatile and semivolatile analysis. They were received
intact between 10/10/90 and 10/13/90 via Federal Express in
properly sealed shipping containers with traffic reports.
Moisture content of the samples ranged from 10% to 82%. With
the exception of sample MW20-35-l, the pH values of the
samples were outside the range specified in EPA protocols.
VOLATILES:
All volatile fractions were analyzed within holding time
requirements. Sample SB21-3S-l was analyzed as a Medium
Level Solid due to the level of target compounds present. It
contained methylene chloride, acetone, 2-butanone, 4-methyl-
2-pentanone, tetrachloroethene, toluene, and total xylenes.
The remaining samples were all analyzed as Low Level Solids.
With the exception of sample SB22-3S-l, they all contained
methylene chloride and acetone, which were also detected in
the associated method blanks. Sample SB22-3S-l contained
methylene chloride (also detected in the associated method
blank) and 1,1,1-trichloroethane. All surrogates met
recovery criteria. Both the Low and Medium Level matrix
spike/matrix spike duplicate results were acceptable. The
recovery for toluene exceeded QC limits in the Low Level MSD.
SEMIVOLATILES:
All semivolatile fractions were extracted and analyzed within
holding time requirements. The only samples containing
target compounds were SB20-3S-l and SB21-3S-l, in which
small amounts of isophorone were detected. All surrogates
met recovery criteria. The matrix spike/matrix spike
duplicate results were acceptable.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than the conditions detailed
above. Release of the data contained in this hardcopy data
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COMPUCHEM
IABoAATORJES, INC.
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
Note: This report was paginated for reference and
accountability in decreasing numerical sequence.
Page - 2
Sarah A. Hubbard 10/31/90
Technical Reviewer
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lA
VOLATILE ORGANICS ANALYSIS DATA.SHEET E: .\ SAMPLE NO.
MWlS-15-1 Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab code: COMPU Case No.: 21492 SAS No.: SDG No.: .,.0_1 __
Matrix: (soil/water) SOIL Lab Sample ID: 373516
Sample wt/vol: s,o (g/mL) L.._ Lab File ID: GH073516B13
Level: (low/med) LOW Date Received: 10/12/90
I Moisture: not dee. __ll Date Analyzed: 10/16/90
Column: (pack/cap) CAP Dilution Factor: .1L,O"---
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9------~--Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone.
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67~66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3----~----2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------1,1,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-S------cis-l,3-Dichloropropene
79-01-6-----.----Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromoform
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenz~ne
100-42-5--------styrene
1330-20-7-------Total Xylenes
15 u
15 u
15 u
15 u
12 B
23 B
8 u
8 u
8 u
8 u
8 u
8 u
15 u
8 u
8 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
15 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
FORM I VOA 1/87 _Rev.
21492 01 SAMPLE DATA SUMMARY
Q
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u;
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: C2-88l•REVS
EPA SAMPLE NO.
HW18-15-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. _.ll
Column (pack/cap) CAP
Number TICS found: ---1
(g/mL) ~
Lab Sample ID: 373516
Lab File ID: GH073516Bl3
Date Received: 10/12/90
Date Analyzed: lQ/16/90
Dilution Factor: .1~1 ~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q ================ ==============================================a•======
1. LAB. ARTIFACT 0.85 7.6 J
FORM I VOA-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: /2-881-REVS MW20-35-l
Lab Code: COMPU Case No.: 21492 SAS No.: SOG No. : ><O.._l __
Matrix: (soil/water) SOIL Lab Sample ID: 373140
Sample wt/vol: 5.0 (g/mL) L-Lab File ID: GH073140Cl2
Level: (low/med) LOW Date Received: 10/10/90
Date Analyzed: 1Q/U/9Q t Moisture: not dee. _n
Column:. (pack/cap) CAP Dilution Factor: ~1~1~0 __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
.75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6-----~---l,l,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4~-------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cis-l,3-Dichloropropene
79-01-6-~-------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene __
75-25-2---------Bromotorm
100-10-1--------4.-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5--~------1,1,2;2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene
1330-20-7-------Total Xylenes
15 u
15 u
15 u
15 u
33 B
22 B
8 u
8 u
8 u
8 u
8 u
8 u
15 u
8 u
8 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
15 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
FORM I VOA · 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
Q
103
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
J:.,'A ::iAl'\P LE ~C.
MW20-35-l
Lab Code: COMPU case No.: 21492 SAS No,: SDG No.: ..,0._l __
Matrix: (soil/water) SOIL
Sample wt/vol: 5,0
Level: (low/med) LOW
% Moisture: not dee. -12
Column (pack/cap) CAf
Number TICs found: _J2
CAS NUMBER
(g/mL) L._
COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
373140
GH07 3 U QCl~
10/10/9Q
10/11/90
1.Q
RT EST. CONC. Q
FORM I VOA-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS SB18-35-l
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample IO: 373362
Sample wt/vol: 5.0 (g/mL) L-Lab File ID: GB073362!Hl
Level: (low/med) LOW Date Received: 10/11/90
t Moisture: not dee. _u Date Analyzed: 10/17/90
Column: (pack/cap) CAP Dilution Factor: 1,0 ~~--
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 56 u 74-83-9---------Bromomethane 56 u 75-01-4---------Vinyl Chloride 56 u 75-00-3---------Chloroethane 56 u 75-09-2---------Methylene Chloride 76 B 67-64-1---------Acetone 120 B 75-15-0---------carbon Disulfide 28 u 75-35-4---------1,l-Dichloroethene 28 u 75-34-3---------1,l-Dichloroethane 28 u 540-59-0--------1,2-Dichloroethene (total)_ 28 u 67-66-3---------Chloroform 28 u 107-06-2--------1,2-Dichloroethane 28 u 78-93-3---------2-Butanone 56 u 71-55-6---------1,1,l-Trichloroethane · 28 u 56-23-5---------carbon Tetrachloride 28 u 108-05-4--------Vinyl Acetate 56 u 75-27-4---------Bromodichloromethane 28 u 78-87-5---------1,2-Dichloropropane 28 u 10061-01-5------cis-l,3-Dichloropropene 28 u 79-01-6---------Trichloroethene 28 u 124-48-1--------Dibromochloromethane 28 u 79-oo-s---------1,1,2-Trichloroethane 28 u
71-43-2---------Benzene 28 u 10061-02-6------Trans-l,3-Dichloropropene __ 28 u
75-25-2---------Bromoform 28 u 108-10-1--------4-Methyl-2-Pentanone 56 u
591-78-6--------2-Hexanone 56 u 127-18-4--------Tetrachloroethene 28 u 79-34-5---------1,1,2,2-Tetrachloroethane __ 28 u · 108-88-3--------Toluene 28 u
108-90-7--------Chlorobenzene 28 u
100-41-4--------Ethylbenzene 28 u
100-42-5--------styrene 28 u
lJJ0-20-7-------Total Xylenes 28 u
FORM I VOA 1/87 Rev.
21492 01 SRMPLE DRTR SUMMRRY 101 _, -~
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEK,RTP Contract: (2-88)-REVS
Lab Code: COMPU case No.: 21492 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 5,0 (g/mL) L.._ Lab File ID:.
Level: (low/med) -L9~W~-Date Received:
t.?A SAMPLE NO.
SB18-J5-l
No.: 01
373362
GBQ73362!H3
I \ Moisture: not dee. -~
10/11/90
Date Analyzed: 10/17/90
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Column (pack/cap) ,..CA,..P.___
Number TICS found: __o
CAS NUMBER COMPOUND NAME
Dilution Factor: -l~,~Q __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q ================ ============================ ======== =------=-=---=====
FORM I VOA-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 10f.
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS SB19-3S-l
Lab Code: CQMPU case No.: 21492 SAS No.: SOG No.: 01
Matrix: (soil/water) SOIL Lab sample IO: 373518
Sample wt/vol: 3.1 (g/mL) li...__ Lab File ID: G2R73518Al3
Level: . (low/med) LOW Date Received: 10/12/90
t Moisture: not dee. _1.8. Date Analyzed: 10/19/90
Column: (pack/cap) CAP Dilution Factor: .l~-~o~o __
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
20
20
20
20
30
67-64-1---------Acetone 270
75-15-o---------carbon Disulfide 10
75-35-4---------1,1-0ichloroethene 10
75-34-3---------1,1-0ichloroethane 10
540-59-0--------1,2-oichloroethene (total)_ 10
67-66-3---------Chloroform 10
107-06-2--------1,2-Dichloroethane 10
78-93-3---------2-Butanone 20
71-55-6---------1,1,1-Trichloroethane 10
56-23-5---------carbon Tetrachloride 10
108-05-4--------Vinyl Acetate 20
75-27-4---------Bromodichloromethane 10
78-87-5---------1,2-0ichloropropane 10
10061-0l-S------cis-l,3-Dichloropropene 10
79-01-6---------Trichloroethene 10
124-48-1--------Dibromochloromethane 10
79-oo-s---------1,1,2-Trichloroethane 10
71-43-2---------Benzene 10
10061-02-6------Trans-l,3-Dichloropropene __ 10 ·
75-25-2-~-------Bromoform 10
108-10-1---~----4-Methyl-2-Pentanone 20
591-78-6--------2-Haxanone 20
127-18-4--------Tetrachloroethene 10
79-34-5---------1,1,2,2-Tetrachloroethane __ 10
108-88-3--------Toluene 10
108-90-7--------Chlorobenzene 10
100-41-4--------Ethylbenzene 10
100-42-5--------styrene 10
1330-20-7-------Total Xylene■ 10
0
u u u u
B
B u u u u u u u u u
u u u u u u u u u u u u
u u u u u u u
FORM I VOA 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
5B19-3S-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373518
sample wt/vol: 3,1 (9/mL) .!i...._ Lab File ID: G2R735l8Al3
Level: (low/med) rpw
t Moisture: not dee. --1.S.
Column (pack/cap) CAP
Number TICs found: _J.
CAS NUMBER COMPOUND NAME
Date Received: 10/12/90
Date Analyzed: 10/19/20
Dilution Factor: -l~-~00~-
CONCENTRATION UNITS:
(u9/L or u9/K9) UG/KG
RT EST. CONC. Q amm===:a======:::1a •==========-•=============== ========---=====•-==----===-= 1. LABORATORY ARTIFACT 0.45 14 J
FORM I VOA-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 98
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCH~.RTP Contract: 12-881-REVS SB20-3S-l
Lab Code: COMPU Case No.: 21492 ;
SAS No.: SDG No.: ~0-1 __
Matrix: (soil/water) ~QII. Lab Sample ID: 373:i2Q
Sample wt/vol: :i. Q (g/mL) L-Lab File ID: GHQ73520B13
Level: (low/med) :t.QW Date Received: 10/12/90
, Moisture: not dee. ---4! Date Analyzed: 10/lfi/90
Column: (pack/cap), CAP Dilution Factor: ~l~•JO'----
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/KgJ UG/KG
74-87-3---------Chloromethane · 13 74-83-9---------Bromomethane 13 75-01-4---------Vinyl Chloride 13 75-00-3---------Chloroethane 13 75-09-2---------Methylene Chloride 13 67-64-1---------Acetone 49 75-15-o---------carbon Disulfide 7 75-35-4---------1,l-Dichloroethene 7 75-34-3---------1,l-Dichloroethane 7 540-59-o--------l,2-Dichloroethene (total)_ 7 67-66-3---------Chloroform 7 107-06-2--------1,2-Dichloroethane 7 78-93-3---------2-Butanone 13 71-55-6---------1,1,l-Trichloroethane 7 56-23-5---------carbon Tetrachloride 7 108-05-4--------Vinyl Acetate 13 75-27-4---------Bromodichloromethane 7 78-87-5---------1,2-Dichloropropane 7 10061-01-5------cia-l,3-Dichloropropene 7 79-01-6---------Trichloroethene 7 124-48-1--------Dibromochloromethane 7 79-00-5---------l,l,2-Trichloroethane 7 71-43-2---------Benzene 7 10061-02-6------Trana-l,3-Dichloropropene __ 7 75-25-2---------Bromoform 7 1oa-10-1--------4-Methyl-2-Pentanone 13 591-78-6--------2-Hexanone 13 127-18-4--------Tetrachloroethene 7
79-34-5---------1,1,2,2-Tetrachloroethane __ 7 108-88-3--------Toluene 7 108-90-7--------Chlorobenzene 7
100-41-4--------Ethylbenzene 7
100-42-5--------styrene 7
1330-20-7-------Total Xylenea 7
u u u
u
B
B
u
u
u u
u
u u
u u u
u
u u u u
u u u u
u u u
u u
u u u u
FORM I VOA 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
Q
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... ,·n. ..Jn.."lr......c. r-,u, VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
S820-3S-l Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: .,._O._l __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee. _li
Column (pack/cap) CAP
Number TICs found: ---1
(g/mLJ ~
Lab Sample ID: -32~3-5~2...,0.._ __ _
Lab File ID: GH073520Bl3
Data Received: 10/12/90
Date Analyzed: 10/16/90
Dilution Factor: .1~,oL..._ __
CONCENTRATION UNITS:
(ug/L or ·ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
l. LAB. ARTIFACT O. 85 29 J
FORM I VOA-TIC 1/87 Rav.
2149.2 0,1 SB.M.FJLE. 0.4T.Q 5.1.!}1.t:f~~
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-BBl-REVS SB2l-3S-l
Lab Code: CQMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373780
Sample wt/vol: 4,0 (g/mL) ~ Lab File ID: C2R73780B13
Level: (low/med) MED Date Received: 10/13/90
\ Moisture: not dee. ___li Date Analyzed: 10/22i9Q
Column: (pack/cap) CAP Dilution Factor: ~i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
74-87-3---------Chloromethane 1600 u 74-83-9---------Bromomethane 1600 u 75-01-4---------Vinyl Chloride 1600 u 75-00-3---------Chloroethane 1600 u 75-09-2---------Methylene Chloride 500 BJ 67-64-1---------Acetone 3000 75-15-o---------carbon Disulfide 800 u 75-35-4---------l,l-Dichloroethene 800 u 75-34-3-----~---l,l-Dichloroethane 800 u 540-59-o--------l,2-Dichloroethene (total)_ 800 u 67-66-3---------Chloroform 800 u
107-06-2--------1,2-Dichloroethane 800 u
78-93-3--------2-Butanone 16000
71-55-6---------1,1,l-Trichloroethane 630 J
56-23-5---------carbon Tetrachloride 800 u 108-05-4--------Vinyl Acetate 1600 u
75-27-4---------Bromodichloromethane 800 u
78-87-5---------1,2-Dichloropropane 800 u
10061-0l-5------cis-l,3-Dichloropropene 800 u
79-01-6---------Trichloroethene 530 J
124-48-1--------Dibromochloromethane 800 u
79-oo-s---------1,1,2-Trichloroethane 800 u
71-43-2---------Banzene 800 u
10061-02-6------Trana-l,3-Dichloropropene __ 800 u
75-25-2---------Bromoform 800 u
108-10-1--------4-Methyl-2-Pentanone 5000
591-78-6----~---2-Hexanone 1600 u
127-18-4--------Tetrachloroethene 540 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 800 u
108-88-3--------Toluen• 460 J
108-90-7--------Chlorobenzene 800 u
100-41-4--------Ethylbenzene 800 u
100-42-s--------styrane 800 u
1330-20-7-------Total Xylenes 390 J
FORM I VOA 1/87 Rev.
21 92 1 MP D A AR
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
EPA SAMPLE NO.
SB2l-JS-l
Lab code: COMPU Case No. : 21492 SAS No.: SDG No. : .,._0._1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 4.0
Level: (low/med) MED
I Moisture: not dee. _ii
Column (pack/cap) CAP
Number TICs tound: _Q
CAS NUMBER
(g/mL) L_
COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
373780
C2R73780B13
10/13/90
10/22/90
1.0
RT EST. CONC.
FORM I VOA-TIC l/87 Rev.
21492 01 SAMPLE DATA SUMMARY 94
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VOLATILE ORGANICS ANALYSIS DATA SHEET c..c-" .:lA.M.r'l...t:: NO.
Lab Name: COMPUCHEM, RTP Contract: 12-88)-REVS S822-3S-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No. : .,.0.1 __
Matrix: (soil/water) :iiOil, Lab Sample ID: 373784
sample wt/vol: 5.0 (g/mL) L._ Lab File ID:· GH073784Cl3
Level: (low/med) 1,0W Date Received: 10/13/90
\ Moisture: not dee. --12 Date Analyzed: 10/19/90
Column: · (pack/cap) CAP Dilution Factor: ~1~,~o'----
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4-~-------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3------~--2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
(total)_
71-55-6---------1,l,l-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4-~------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-5------cia-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,J-Dichloropropene __
75-25-2---------Bromoform
1os-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34•5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styrene
1330-20-7-------Total Xylenes
11 l1
11 l1
11 l1
11 l1
13 8
11 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
11 l1
1 J
6 l1
11 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
11 l1
11 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
6 l1
FORM I VOA 1/87 Rev.
14 SRMP DRTR SUMMARY
Q
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VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM,RTP contract: 12-88)-REYS
.... ri. ..,n.i'l.r....c. l'IU.
SB22-JS-l
Lab Code: COMPU case No.: 21492 SAS No.: SDG No.: ..._0._1 __
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee. ~
column (pack/cap) CAP
Nwnber TICS found: _Q
L-
Lab Sample ID: 373784
Lab File ID: GHQZ37!H~ll
Date Received: lQ/13/90
Date Analyzed: 1Q/19/9Q
Dilution Factor: _1~,o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER COMPOUND NAME RT EST, CONC, Q
FORM I VOA-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS MW20-35-lMS
Lab Code: COMPU Case No,: 21492 SAS No.: SDG No,: 01
Matrix: ( soil/water) SOIL Lab Sample ID: 373176
sample wt/vol: 5,0 (g/mL) !....._ Lab File ID: GH07Jl76Cl2
Level: (low/med) t,OW Date Received: 10/10/90
% Moisture: not dee, _n Date Analyzed: 10/11/90
Column: (pack/cap) CAP Dilution Factor: ~i~-~o __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-0---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trich+oroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-0ichloropropane
10061-01-5------cis-l,J-Dichloropropene
79-01-6--------~Trichloroethene ,
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6-----~Trans-l,J-Dichloropropene __
75-25-2---------Bromoform
108-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-s--~------l,l,2,2-Tetrachloroethane __
108-88-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s~-------styrene
1330-20-1-------Total Xylenes
15 u
15 u
15 u
15 u
35 B
24 B
8 u
8 u
8 u
8 u
8 u
8 u
15 u
8 u
8 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
15 u
15 u
8 u
8 u
8 u
8 u
8 u
8 u
8 u
FORM I VOA 1/87' Rev,
1 g 0 M ,., _y
Q
91
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VVLA'!'!W: ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS MW20-35-1MSD
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: Ql
Matrix: (soil/water) so;i:i. Lab Sample ID: 373177
Sample wt/vol: :i IQ {g/mL) Si__ Lab File ID: GHQ7Jl77b,12
Level: (low/med) l&li Date Received: lQ/lQ/90
\ Moisture: not dee. _ll Date Analyzed: 12111190
Column: (pack/cap) CAP Dilution Factor: .i~,JQ __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG 0
74-87-3---------Chloromethane 15 u 74-83-9---------Bromomethane 15 u 75-01-4---------Vinyl Chloride 15 u 75-00-3---------Chloroethane · 15 u 75-09-2---------Methylene Chloride 46 B 67-64-1---------Acetone 36 B '
75-15-0---------carbon Disulfide 8 u 75-35-4---------1,1-Dichloroethene 8 u 75-34-3---------1,1-Dichloroethane 8 u 540-59-0----•---l,2-Dichloroethene (total)_ 8 u 67-66-3---------Chloroform 8 u 107-06-2--------1,2-Dichloroethane 8 u 78-93-3---------2-Butanone '5 BJ 71-55-6----~----l,l,l-Trichloroethane 8 u 56-23-5---------carbon Tetrachloride 8 u 108-05-4--------Vinyl Acetate 15 u 75-27-4---------Bromodichloromethane 8 u 78-87-5---------1,2-Dichloropropane 8 u 10061-0l-5------cis-l,3-Dichloropropene 8 u 79-01-6---------Trichloroethene 8 u 124-48-1--------Dibromochloromethane 8 u 79-00-5---------1,1,2-Trichloroethane 8 u 71-43-2---------Benzene 8 u 10061-02-6------Trana-l,3-0ichloropropene __ 8 u 75-25-2---------Bromoform 8 u 1os-10-1--------4-Methyl-2-Pentanone 15 u 591-78-6--------2-Hexanone 15 u 127-18-4--------Tetrachloroethene 8 u 79-34-5---------1,1,2,2-Tetrachloroethane __ 8 u 1oa-aa-J--------Toluene 8 u 108-90-7-~------Chlorobenzene 8 u 100-41-4--------Ethylbenzene 8 u 100-42-5---~----styrene 8 u 1330-20-7-------Total Xylenes 8 u
FORM I VOA 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 90
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS SB2l-3S-lMS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No. : .,.0..,1 __
Lab Sample ID: ..._3.,_741· 7.!.eO,.,S'----Matrix: (soil/water) SOIL
Sample wt/vol: 4.0 (g/mL) L.__ Lab File ID: CN074705Cl3
Level: (low/med) M;EQ
\ Moisture: not dee. _ll
Date Received: 10/13/90
Date Analyzed: 10/23/90
Dilution Factor: Alu,~0'----Column:
•
(pack/cap) CAP
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 1600 74-83-9---------Bromomethane 1600 75-01-4---------Vinyl Chloride 1600
75-00-3---------Chloroethane 1600 75-09-2---------Methylene Chloride 270 67-64-1---------Acetone 1600 75-15-0---------carbon Disulfide 800
75-35-4---------1,1-Dichloroethene 800
75-34-3---------1,1-Dichloroethane 800 540-59-0--------1,2-Dichloroethene (total)_ 800 67-66-3---------Chloroform 800
107-06-2--------1,2-Dichloroethane 800
78-93-3---------2-Butanone 18000
71-55-6---------1,1,1-Trichloroethane 800 56-23-5---------carbon Tetrachloride 800
108-05-4--------Vinyl Acetate 1600
75-27-4---------Bromodichloromethane 800
78-87-5---------1,2-Dichloropropane 800 10061-01-5------cis-l,3-Dichloropropene 800
79-01-6---------Trichloroethene 800
124-48-1--------Dibromochloromethane 800
79-00-5---------1,1,2-Trichloroethane 800
71-43-2---------Benzene 800
10061-02-6------Trans-l,3-Dichloropropene __ 800
75-25-2---------Bromoform 800
108-10-1-------~4-Methyl-2-Pentanone 6800
591-78-6--------2-Hexanone 1600
127-18-4--------Tetrachloroethene 800
79-34-5---------1,l,2,2-Tetrachloroethane __ 800
108-88-3--------Toluene 800
108-90-7--------Chlorobenzene 800
100-41-4--------Ethylbenzene 800
100-42-5--------styrene 800
1330-20-7-------Total Xylene& 800
u u u u
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FORM I VOA 1/87 Rev.
? 92 PL AT SUM RY
Q
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: /2-88)-REVS SB21-3S-1MSD
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 374706
Sample wt/vol: 4,0 (g/mL) ~ Lab File IO: CN074706Cl3
Level,: (low/med) MED Date Received: 10/13/90
I Moisture: not dee. ---2..
Column:-(pack/cap) CAP
Date Analyzed: 10/23/~0
Dilution Factor: alL«~0 __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
74-87-3---------Chloromethane 1600 74-83-9---------Bromomethane 1600 75-01-4---------Vinyl Chloride 1600 75-00-3---------Chloroethane 1600 75-09-2---------Methylene Chloride 200 67-64-1---------Acetone 3700 75-15-0---------carbon Disulfide 800 75-35-4---------1,1-Dichloroethene 800 75-34-3---------1,1-Dichloroethane 800 540-59-0------~-1,2-Dichloroethene (total)_ 800 67-66-3---------Chloroform 800 107-06-2--------1,2-Dichloroethane 800 78-93-3-----~---2-Butanone 18000 71-55-6---------1,1,1-Trichloroethane 800
56-23-5---------carbon Tetrachloride 800 108-05-4--------Vinyl Acetate 1600
75-27-4--------~Bromodichloromethane 800
78-87-5---------1,2-Dichloropropane 800 10061-0l-5-~----cis-l,3-Dichloropropene 800 79-01-6---------Trichloroethene 800
124-48-1--------Dibromochloromethane 800
79-00-5---------1,l,2-Trichloroethane 800
71-43-2---------Benzene 800
10061-02-6------Trans-l,J-Dichloropropene __ 800
75-25-2---------Bromoform 800
108-10-1-------~4-Methyl-2-Pentanone 7200
591-78-6--------2-Hexanone 1600
127-18-4--~-----Tetrachloroethene 800
79-34-5---------1,1,2,2-Tetrachloroethane __ 800
108-88-3--------Toluene 800
108-90-7--------Chlorobenzene 800
100-41-4--------Ethylbenzene 800
100-42-5--------styrene 800
1330-20-7-------Total Xylenes 800
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FORM I VOA 1/87 Rev. ·
49 01 SAMPLE DATA SUMMARY BE
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS MW18-l5-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373516
Sample wt/vol: . 30 I 5 (g/mL) G...._ Lab File ID: GH073516B06
Level: ( low/med) I.OW Date Received: 10/12/90
I Moisture: not dee. __3_i dee. Date Extracted: 10/15/90
Extraction: ( SepF /Cont/Sonc) Date Analyzed: 10/23/90
GPC Cleanup: (Y/N) H.,__ pH: ....L..J. Dilution Factor: .1~0~0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 490 u lll-44-4--------bis(2-Chloroethyl)Ether 490 u 95-57-8---------2-Chlorophenol 490 u 541-73-1--------l,3-Dichlorobenzene 490 u 106-46-7--------l,4-Dichlorobenzene 490 u 100-51-6--------Benzyl Alcohol 490 u 95-50-1---------l,2-Dichlorobenzene 490 u 95-48-7---------2-Methylphenol 490 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 490 u 106-44-5--------4-Methylphenol 490 u 621-64-7--------N-Nitroso-Di-n-Propylamine __ 490 u 67-72-1---------Hexachloroethane 490 u 98-95-3---------Nitrobenzene 490 u 78-59-1---------Isophorone 490 u 88-75-5---------l~Nitrophenol 490 u 105-67-9--------2,4-Dimethylphenol 490 u 65-85-o---------Benzoic Acid 2400 u
lll-9l-l--------bia(2-Chloroethoxy)Methane __ 490 u
120-83-2--------2,4-Dichlorophenol 490 u 120-e2-1--------1,2,4-Trichlorobenzene 490 u 91-20-3---------Naphthalene 490 u
106-47-8--------4-Chloroaniline 490 u
87-68-3---------Hexachlorobutadiene 490 u
59-50-7---------4-Chloro-37Methylphenol 490 u
91-57-6---------2-Methylnaphthalene 490 u
77-47-4---------Hexachlorocyclopentadiene __ 490 u
ee-06-2---------2,4,6-Trichlorophenol 490 u
95-95-4---------2,4,5-Trichlorophenol 2400 u
91-58-7---------2-Chloronaphthalene 490 u
88-74-4---------2-Nitroanilin• 2400 u
131-11-3--------Dimethyl Phthalate 490 u
208-96-8--------Acenaphthylene 490 u
606-20-2--------2,6-Dinitrotoluene 490 u
I FORM I sv-1 1/87 Rev.
I
21492 01 SAMPLE DATA SUMMARY 87
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
EPA SAMPLE NO.
MW18-15-l
No.: I Matrix: (soil/water) SOIL
01
Lab Sample ID: 373516
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Sample vt/vol: 30,5 (g/mL) L_ Lab Pile ID: GH073:!16~Q!i
Level: (low/med) LOW Date Received: 10/12/90
t Moisture: not dee . .--1J. dee. Date Extracted: 1Qll:il90
Extraction: (SepP/Cont/Sonc)
(Y/N) H___
Date Analyzed: 10l2ll9Q
GPC Cleanup: Dilution Factor: .1-1_0 __ _
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UGlKG
99-09-2---------3-Nitroaniline 2400 83-32-9---------Acenaphthene 490 51-28-5---------2,4-Dinitrophenol 2400 100-02-1--------4-Nitrophenol 2400 132-64-9--------Dibenzoturan 490 121-14-2--------2,4-Dinitrotoluene 490 84-66-2---------Diethylphthalate 490 7005-72-3-------4~Chlorophenyl-phenylether __ 490 86-73-7---------Fluorene 490 100-01-6--------4-Nitroaniline 2400 534-52-l~-------4,6-Dinitro-2-Methylphenol_ 2400 86-30-6---------N-Nitrosodiphenylamine (1)_ 490 101-55-3--------4-Bromophenyl-phenylether_ 490 118-74-1--------Hexachlorobenzene 490 87-86-5---------Pentachlorophenol -2400 85-01-8---------Phenanthrene 4.90 120-12-1--------Anthracene 490 84-74-2---------Di-n-Butylphthalate 490 206-44-o-----~--Pluoranthene 490 129-oo-o--------Pyrene 490 85-68-7---------Butylbenzylphthalate 490
91-94-1---------3,3'-Dichlorobenzidine 980 56-55-3---------Benzo(a)Anthracene 490
218-01-9--------chrysena 490
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 490 117-84-o--------Di-n-octyl Phthalate 490 205-99-2--------Benzo(b)Pluoranthene 490
207-08-9--------Benzo(k)Pluoranthene 490 50-32~8---------Benzo(a)Pyrene 490
193-39-5---·-----Indeno( 1, 2, 3-cd) Pyrene 490
53-70-3---------Dibenzo(a,h)Anthracene 490
191-24-2--------Benzo(g,h,i)Perylene 490
(1) -CaMot be separated trom Diphanylamine ,,.
u u u u
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u
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u u
u u
u
FORM I sv-2 1/87 Rev.
?f ,f ' 11
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
EPA SAMPLE NO.
MW18-15-l
No.: 01 I ·Matrix: (soil/water) SOIL Lab sample ID: 373516
Sample wt/vol: JO I 5 (g/mL) L_ Lab File ID: GH07JS16B06 I Level: · (low/med) LOW Date Received: 1!21'.lal'.90
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I Moisture: not dee. ___l_i
Extraction:
GPC Cleanup:
( SepF /Cont/Sonc)
(Y/K) H......
Number TICS found:~
dee.
~
pH: ....L..1
CAS NUMBER COMPOUND NAME·
Date Extracted: 1!21'.15/90
Date Analyzed: . 10i23i90
Dilution Factor: alL,o"'---
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGiKG
RT EST. COKC. Q
=•======•=•a•=•• -==-===--=------=--=--==-=== =•===== ======-====== a====
1. SOLVENT CONTAMINANT 3.88 500 BJ
2. ALOOL 4.95 300 ABJ
FORM I SV-TIC 1/87 Rev.
21492 0l SAMPLE DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPO case No.: 21492 SAS No.:
Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
30.7
LOW
(g/mL) ~
SDG
Lab Sample IO:
Lab File ID:
Date Received:
EPA SAMPLE NO.
MW20-35-l
No.: 01
373140
GH07Jl40AS2
10£'.10£'.90
% Moisture: not dee. --1.5_ dee. Date Extracted: 10£'.10£'.90
Extraction: (SepF/Cont/Sonc) Date Analyzed: 10£'.12£'.90
GPC Cleanup: (Y/N) lf.._ pH:-~ Dilution Factor: _1~,~o~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG£'.KG Q
108-95-2--------Phenol 500 u
lll-44-4--------bis(2-Chloroethyl)Ether 500 u
95-57-8---------2-Chlorophenol 500 u
541-73-1--------1,3-Dichlorobenzene 500 u
106-46-7--------1,4-Dichlorobenzene 500 u
100-51-6----~---Benzyl Alcohol 500 u
95-50-1---------1,2-Dichlorobenzene 500 u
95-48-7---------2-Methylphenol 500 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 500 u
106-44-5--------4-Methylphenol 500 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 500 u
67-72-1---------Hexachloroethane 500 u
98-95-3---------Nitrobenzene 500 u
78-59-1---------Isophorone 500 u
88-75-5---------2-Nitrophenol 500 u
105-67-9--------2,4-Dimethylphenol 500 u
65-85-o---------Benzoic Acid 2400 u
lll-91-1--~-----bis(2-Chloroethoxy)Methane_ 500 u
120-83-2-----.---2, 4-Dichlorophenol 500 u
120-e2-1--------1,2,4-Trichlorobenzene 500 u
91-20-3---------Naphthalene 500 u
106-47-8--------4-Chloroaniline 500 u
87-68-3---------Hexachlorobutadiene 500 u
59-50-7---------4-Chloro-3-Methylphenol I 500 u
91-57-6---------2-Methylnaphthalene 500 u
77-47-4---------Hexachlorocyclopentadiene __ 500 u
88-06-2---------2,4,6-Trichlorophenol 500 u
95-95-4---------2,4,5-Trichlorophenol 2400 u
91-58-7---------2-Chloronaphthalene 500 u
88-74-4---------2-Nitroaniline 2400 u
131-11-3--------Dimethyl Phthalate 500 u
208-96-8--------Acenaphthylene 500 u
606-20-2--------2,6-Dinitrotoluene 500 u
FORM I sv-1 l/87 Rev.
•
-, f ..t O? at <::DMP/ t:' l"IDTD <::I /MMOPV
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
•
Lab Name: COMPUCHEM,RTP contract: C2-88l-REVS MW20-35-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG Ho.: 01
Matrix: (soil/water)·SOIL Lab Sample ID: 373140
Sample wt/vol: 30,7 (g/mL) Si__ Lab File ID: GH073l40A52
Level: (low/med) I.OW Date Received: 10/10/90
' Moisture: not dee. _,ll dee. Date Extracted: 10/10/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/NJ lL..
~
pH: ~
Date Analyzed: 10/12/90
Dilution Factor: 1,00
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q .
99-09-2---------3-Nitroaniline 2400 u 83-32-9---------Acenaphthene 500 u 51-28-5---------2,4-Dinitrophenol 2400 u 100-02-1--------4-Nitrophenol 2400 u 132-64-9--------Dibenzoturan 500 u 121-14-2--------2,4-Dinitrotoluene 500 u 84-66-2------..;--Diethylphthalate 500 u 7005-72-3-------4-Chlorophenyl-phenylether_ 500 u 86-73-7---------Fluorene 500 u 100-01-6----"'."---4-Nitroaniline 2400 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 2400 u 86-30-6---------N-Nitrosodiphenylamine (l)_ 500 u 101-55-3--------4-Bromophenyl-phenylether __ 500 u
118-74-1--------Hexachlorobenzene 500 u
87-86-5---------Pentachlorophenol 2400 u 85-01-8---------Phenanthrene 500 u 120-12-1--------Anthracene 500 u
84-74-2---------Di-n-Butylphthalate 500 u
206-44-0--------Fluoranthene 500 u
129-00-0-------~Pyren• 500 u
85-68-7---------Butylbenzylphthalate 500 u
91-94-1---------3,3'-Dichlorobenzidine 990 u
56-55-3---------Benzo(a)Anthracene 500 u
.218-01-9--------Chrysene 500 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 500 0
117-84-0--------Di-n-Octyl Phthalate 500 0
205-99-2--------Benzo(b)Fluoranthen• 500 u
207-08-9--------Benzo(k)Fluoranthene 500 0
50-32-8---------Benzo(a)Pyr•n• 500 0
193-39-5--------Indeno(l,2,3-cd)Pyrene 500 0
53-70-3---------Dibenzo(a,h)Anthracene 500 0
191-24-2--------Benzo(g,h,i)Perylene 500 0
(1) -cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: /2-881-REVS
EPA SAMPLE NO.
MW20-35-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL
Sample wt/vol: 30,7 (g/mL) L-..
Level: (low/med) LOW
% Moisture: not dee.~
Extraction:
GPC Cleanup:
(SepP'/Cont/Sonc)
(Y/N) R._
dee.
SQliC
pH: ....2......2.
Lab Sample ID: 373140
Lab File ID: GH073140A52
Date Received: 10/10/90
Date Extracted: 10/10/90
Date Analyzed: 10/12/90
Dilution Factor: ...,l.a.,;, o,.,o.___
Number TICs tound: ~
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
CAS NUMBER ·COMPOUND NAME RT EST. CONC. Q ==============•= ••2=--=ss===•==========n====== =-•:a::::sz:=== •a=•========= ===== 1. SOLVENT CONTAMINANT 5.23 3400 BJ 2. SOLVENT CONTAMINANT 5.32 2400 BJ 3. ALDOL 6.40 550 ABJ
4. UNKNOWN PHTHALATE 21.34 650 3
5. UNKNOWN PHTHALATE 21.45 600 3
6. UNKNOWN PHTHALATE 21.54 750 3
7. UNKNOWN PHTHALATE 21.64 900 3
8. UNKNOWN PHTHALATE 21.67 900 3
9. UNKNOWN PHTHALATE 21.77 500 3
10. UNKNOWN PHTHALATE 21.89 250 3
FORM I SV-TIC 1/87 Rav.
9 s PL D/:IT s RY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS SB18-35-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373362
Sample wt/vol: 30.2 (g/mL) SL_ Lab File IO: liH0ZJJ§ZA!l7
Level: (low/med) LOW Date Received: 10/11/90
t Moisture: not dee. _ll dee. Date Extracted: 10/11/90
Extraction: (SepF/Cont/Sonc)
(Y/N) H..,_
~
pH: ~
Date Analyzed: 10/13/90
GPC Cleanup: Dilution Factor: 1.00
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 1800 lll-44-4--------bis(2-Chloroethyl)Ether 1800 95-57~8---------2-Chlorophenol 1800 541-73-1--------1,3-Dichlorobenzene 1800 106-46-7--------1,4-Dichlorobenzene 1800 100-51-6--------Benzyl Alcohol 1800 95-50-1---------1,2-Dichlorobenzene 1800 95-48-7---------2-Methylphenol 1800 39638-32-9------bis(2-Chloroisopropyl)Ether_ 1800 106-44-5--------4-Methylphenol 1800 621-64-7------~-N-Nitroso-Di-n-Propylamine __ 1800 67-72-1---------Hexachloroethane 1800 98-95-3---------Nitrobenzene 1800 78-59-1---------Isophorone 1800
88-75-5---------2-Nitrophenol 1800 105-67-9--------2,4-Dimethylphenol 1800 65-85-o---------Benzoic Acid 8800 111-91-1-----.---bi■ ( 2-Chloroethoxy) Methane __ 1800
120~83-2------~-2,4-Dichlorophenol 1800
120-82-1--------1,2,4-Trichlorobenzene 1800 91-20-3---------Naphthalene 1800
106-47-8--------4-Chloroaniline 1800
87-68-3---------Hexachlorobutadiene 1800 59-50-7---------4-Chloro-3-Methylphenol 1800
91-57-6---------2-Methylnaphthalene 1800
77-47-4---------Hexachlorocyclopentadiene __ 1800 88-06-2---------2,4,6-Trichlorophenol 1800
95-95-4---------2,4,5-Trichlorophenol 8800
91-58~7---------2-Chloronaphthalene 1800
88-74-4---------2-Nitroaniline 8800
131-11-3--------Dimethyl Phthalate 1800
208-96-8--------Acenaphthylene 1800
606-20-2--------2,6-Dinitrotoluene 1800
.,. ..
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u
FORM I sv-1 1/87 Rev.
♦ ?f f\ D ,.,
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP contract: (2-88)-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
EPA SAMPLE NO.
SB18-35-l
No.: 01 I Matrix: (soil/water) SOIL Lab Sample ID: 373362
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Sample wt/vol: 30. 2 (g/mL) L._ Lab Pile ID: GH07JJ6U,Q7
Level: ( low/med) LOW Date Received: lQ/11190
\ Moisture: not dee. __u_ dee. Date Extracted: 1Q/ll/9Q
Extraction:
GPC Cleanup:
(SepP/Cont/Sonc)
(Y/N) lL._
~
pH: ....L.2
Date Analyzed: 10/13/9Q
· Dilution Factor: l. 00
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 8800 u 83-32-9---------Acenaphthene 1800 u 51-28-5------~--2,4-Dinitrophenol 8800 u 100-02-7--------4-Nitrophenol 8800 u 132-64-9--------Dibenzoturan 1800 u 121-14-2--------2,4-Dinitrotoluene 1800 u 84-66-2---------Diethylphthalate 1800 u 7005-72-3-------4-Chlorophenyl-phenylether_ 1800 u 86-73-7---------Fluorene 1800 u 100-01-6--------4-Nitroaniline 8800 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 8800 u 86-30-6---------N-Nitrosodiphenylamine (1)_ 1800 u 101-55-3--------4-Bromophenyl-phenylether __ 1800 u 118-74-1--------Hexachlorobenzene 1800 u 87-86-5---------Pentachlorophenol 8800 u 85-01-8---------Phenanthrene 1800 u 120-12-7--------Anthracene 1800 u 84-74-2---------oi-n-Butylphthalate 1800 u 206-44-o--------Pluoranthene 1800 u 129-00-0--~-----i?yrene 1800 u 85-68-7---------Butylbenzylphthalate 1800 u 91-94-1---------J,J'-Dichlorobenzidine 3600 u 56-55-3---------Benzo(a)Anthracene 1800 u 218-01-9--------Chrysene 1800 u 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 1800 u 117-84-o--------oi-n-Octyl Phthalate 1800 u 205-99-2--------Benzo(b)Pluoranthene 1800 u 207-08-9--------Benzo(k)Pluoranthene 1800 u 50-32-8---------Benzo(a)Pyrene 1800 u 193-39-5--------Indeno(l,2,J-cd)Pyrene 1800 u 53-70-J---------Dibenzo(a,h)Anthracene 1800 u
. 191-24-2--------Benzo(g,h,i)Perylene 1800 u
(1) -CaMot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 80
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lP'
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: COMPUC:HEM. RTP . SB18-35-l Contract: (2-881-REVS
Lab Code: CQMPU case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SQIL Lab Sample ID: 373362
Sample wt/vol: 30,2 (g/mL) L-Lab File ID: GH07JJ62A07
Level: (low/med) LOW
' Moisture:
Extraction:
GPC Cleanup:
not dee. ___u
( SepP' / Cont/ Sonc)
(Y/N) lL._
Number TICs found: __.l
dee.
~
pH: ....!....2
CAS NUMBER COMPOUND NAME
Date Received: 10/11/90
Date Extracted: 10/11/90
Date Analyzed: 10/13/90
Dilution Factor: &l~,0~0"---
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC. Q =~~============= ============================ ======== ============:m -==:a
1. SOLVENT CONTAMINANT 5.10 920 BJ
FORM I SV-TIC 1/87 Rev.
?14Q? ~1 ~QMPL~ DQTQ SLJMMQRY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP contract: (2-88l-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
EPA SAMPLE NO,
S819-3S-l
I Matrix: (soil/water) SOIL
No.: 01
Lab Sample ID: 373518
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Sample wt/vol: 30.4 (g/mL) Ii_
LOW
Lab File ID: liH0Z3:il81lQ!i
Level: (low/med) Date Received: 10/12/90
I Moisture: not dee. _ll dee.· Date Extracted: 10/15/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/23£'.90
GPC Cleanup: (Y/N) li...._ pH: ....L..§. Dilution Factor: .1~,-0'-----
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) Yli£'.Kli
108-95-2--------Phenol 400 lll-44-4--------bis(2-Chloroethyl)Ether 400 95-57-8---------2-Chlorophenol 400 541-73-1--------1,J-Dichlorobenzene 400 106-46-7--------1,4-Dichlorobenzene 400 100-51-6-----~--Benzyl Alcohol 400 95-50-1---------1,2-Dichlorobenzene 400 95-48-7---------2-Methylphenol 400 39638-32-9------bis(2-Chloroisopropyl)Ether_ 400 106-44-5--------4-Methylphenol 400 621-64-7--------N-Nitroso-Di-n-Propylamine_ 400 67-72-1---------Hexachloroethane 400 98-95-3---------Nitrobenzene 400 78-59-1---------Isophorone 400 88-75-5---------2-Nitrophenol 400 105-67-9--------2,4-Dimethylphenol 400 65-85-o---------Benzoic Acid 1900 111-91-1--------bis(2-Chloroethoxy)Methane_ 400 120-83-2--------2,4-Dichlorophenol 400
120-s2-1--------1,2,4-Trichlorobenzene 400
91-20-3---------Naphthalene 400 106-47-s---~----4-Chloroaniline 400 87-68-3---------Hexachlorobutadiene 400
59-50-7---------4-Chloro-3-Methylphenol 400
91-57-6---------2-Methylnaphthalene 400 77-47-4---------Hexachlorocyclopentadiene __ 400
88-06-2---------2,4,6-Trichlorophenol 400
95-95-4---------2,4,5-Trichlorophenol 1900 91-58-7---------2-Chloronaphthalene 400
88-74-4---------2-Nitroaniline 1900
131-11-3--------Dimethyl Phthalate 400 208-96-8--------Acenaphthylene 400
606-20-2--------2,6-Dinitrotoluene 400
u u u
0 u u u u u u u u u u u u u u u u u u u u u u u u u u u u u
FORM I sv-1 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
Q
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-05-1
Lab Name: CQMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: CQMPU case No.: 20937 SAS No.: SDG No.: ,.1.,,_s..,_o __
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) ~
LOW
Lab
Lab
Date
Date
Sample IO: 365992
File ID: CN065992A03
Received: 08/21/90
Analyzed: 011/30/90 I Moisture: not dee.
Column: (pack/cap) CAP Dilution Factor: .i~-~9'---
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 5 u · 67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------l,l-Dichloroethene 5 u
75-34-3-~-------l,l-Dichloroethane 5 u 540-59-o--------l,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 5 u
107-06-2-~------1,2-Dichloroethane 5 u
78-93-3-~-------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene_ 5 u
75-25-2---------Bromoform 5 u
1os-10-1--------4~Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,l,2,2-Tetrachloroethane_ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene -5 u
100-42-5--------styrene -5 u
1330-20-7-------Total Xylenes 5 u·
FORM I VOA l/87 Rev.
20937 150 SAMPLE DATA SUMMARY
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
PW-05-l
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No• : .._l...,50....__
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: _Q.
CAS NUMBER COMPOUND
Ml._
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
365992
CN065992AOJ
08/21/90
08/J0/90
1,0
CONC. Q
-----====--=•=--•••••m•=•m=••======~•===a=•• -----=---•••a=••••=•=• --===
FORM I VOA-TIC l/87 Rev.
20937 J~@;SAMP~g OAT~ SUMMAR~
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-06-1 Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Coda: COMPU Casa No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365273
Sample wt/vol: 5,0 (g/mL) Ml.__ Lab Fila ID: CN065273A03
Level: (low/med) LOW Date Received: 08/17/90
I Moisture: not dee. Date Analyzed: 08/26/90
Column: (pack/cap) CAP Dilution Factor: ~1~-~o'--__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 t1
74-83-9---------Bromomethane 10 t1
75-01-4---------Vinyl Chloride 10 t1 75-00-3---------Chloroethane 10 t1 75-09-2---------Methylene Chloride 32 67-64-1---------Acetona 10 t1
75-15-o---------carbon Disulfide 5 t1
75-35-4---------1,1-Dichloroethene 5 t1
75-34-3---------1,1-Dichloroethane 5 t1 540-59-o--------l,2-Dichloroethene (total)_ 30
67-66-3---------Chloroform 5 t1
107-06-2--------1,2-Dichloroethane 46
78-93-3---------2-Butanone 10 t1
71-55-6---------1,1,1-Trichloroethana 30
56-23-5---------carbon Tetrachloride 5 t1
108-05-4--------Vinyl Acetate 10 t1
75-27-4---------Bromodichloromethane 41
78-87-5---------1,2-Dichloropropane 5 t1
10061-0l-5------cis-l,3-Dichloropropene 29
79-01-6---------Trichloroethene 5 t1
124-48-1--------Dibromochloromethane 42
79-oo-s---------1,1,2-Trichloroethane 5 t1
71-43-2---------Benzene 5 t1
10061-02-6------Trans-l,3-Dichloropropene_ 42
75-25-2---------Bromoform 5 t1
1os-10-1--------4-Methyl-2-Pentanone 10 t1
591-78-6--------2-Hexanone 10 t1
127-18-4--------Tetrachloroethene. 40
79-34-5---------1,l,2,2-Tetrachloroethane_ 5 t1
108-88-3--------Toluene l J
108-90-7--------Chlorobenzene 2 J
100-41-4--------Ethylbenzena 5 t1
100-42-5--------styrene 5 t1
1330-20-7-------Total Xylenes 5 t1
FORM I VOA 1/87 Rev.
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: coMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: ( soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) Ml._ Lab File ID:
Level: (low/med) LOW Date Received:
I Moisture: not dee. Date Analyzed:
EPA SAMPLE NO.
PW-06-1
No.: 150
365273
CN065273A03
08/17/90
08/2§/90
Column (pack/cap) CAP Dilution Factor: .1~1 ~0 __
Number TICS found: --2
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. •a••=•=•==•===•m •ma2•m==-=-==---==---=-==••a ---===== c:::sz:n:zcz;===•=••
FORM I VOA-TIC 1/87 Rev.
20937 150 SAMPLE DQTA SUMMARY
Q
--•=s=
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
PW-07-1
Lab Name: COMPUCHEM.RTP Contract: <2-88)-RtyS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ..,15...,0"--
Matrix: (soil/water) WATER Lab Sample ID: 365281
Sample wt/vol: 5.0 (g/mL) Ml...._ Lab File ID: CN065281B13
Level: (low/med) I.OW Date Received: 08/17/90
t Moisture: not dee. Date Analyzed: 08/27/90
Column: (pack/cap) !:;AP Dilution Factor:' .. 1 ... ,,,_o __ _
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9---------Bromomethane 10 u
75~01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2~--------Methylene Chloride 5 u 67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-o----".'---l,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3--.-------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------Carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,J-Dichloropropene 5 u
79-01-6---------Trichloroethene 2 BJ
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,J-Dichloropropene_ 5 u
75-25-2---------Bromoform 5 u
1oe-10-1--~-----4-Methyl-:-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
7 50SAMPLE DATA UMMRRY
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
I.ab Name: CQMPUCHEM,RTP Contract: 12-881-REVS
EPA SAMPLE NO.
PW-07-1
I.ab Code: CQMPU Case No.: 20937 SAS No.: S DG No • : ,._l ...a5 0,.___
Matrix: (soil/water) WATER
Sample wt/vol: 5,0 (g/mL) lilL..
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICS found: ___..l2
CAS NUMBER COMPOUND NAME
Lab sample I-D:
Lab File ID:
Date Received;
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L ·
RT EST.
365281
CN0652BlB13
08/17/90
08/27/90
1 I 0
CONC. Q
-------==-=-=•=--••oma--------==----==---a•== •======= ==-•-==-••--.a• •==a=
FORM I VOA-TIC 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY -.,..
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COKPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: ( soil/water) WATER Lab Sample ID: 365282
Sample wt/vol: 5.0 (g/mL) Kl._ Lab File ID: CN065282A03
Level: (low/med) LOW Date Received: 08/17/90
\ Moisture: not dee. Date Analyzed: 0!1£'.25/90
Column: (pack/cap) CAP Dilution Factor: .i~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 6 B 67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5-----~cis-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s-----~---1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-1,3-Dichloropropene __ 5 u
75-25-2~--------Bromoform 5 u
1oe-10-1--------4~Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-s--------styrene 5 u
1330-20-7-------Total Xylene& 5 u
FORM I VOA 1/87. Rev.
20937 158\SAMPLi DQTA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM,RTP Contract: (2-881-REVS
EPA SAMPLE NO.
TB-O9-01
Lab Code: CQMPU Case No,: 20937 SAS No.: S DG No • : ..,.1....,5 o,.___
Matrix: (soil/water) WATER
sample wt/vol: 5.0 (g/mL)
Level: (low/med) LOW
% Moisture: not dee.
Column (pack/cap) CAP
. Number TICS found: __..l2
CAS NUMBER COMPOUND
ML.
NAME
Lab sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
365282
CN065282A03
08/17/90
08/25/90
1,0
CONC. 0 ••••a=======•==• •========================•== m==•~m•:a m:=========•=-za -~==
FORM I VOA-TIC 1/87 Rev.
20937 150 SAMP~g DAT~ SUMMARY'
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lA
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water).WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) Ml._ Lab File ID:
Level: (low/med) LOW Date Received:
EPA SAMPLE NO.
PW-OJ-2MS
No.: 150
365261
CN065261A03
08{'.17{'.90 I I Moisture: not dee. Date Analyzed: 08{'.26{'.90
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Column: (pack/cap) CAP Dilution Factor: al~,~o __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2-----~---Methylene Chloride
67-64-1---------Acetone
1s-1s-o---------carbon Disulfide
75-35-4---------1,l-Dichloroethene
75-34-3---------1,l-Dichloroethane
540-59-0--------l,2-Dichloroethene
67-66-3-----~---Chlorofom
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG{'.L
(total)_
71-55-6---------1,l,l-Trichloroethane
56-23-s~--------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-5------cis-l,J-Dichloropropene
79-01-6---------Trichloroethene
124~48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2--~------Benzene
10061-02-6------Trans-l,J-Dichloropropene __
1s-2s-2---------Bromofot111
1oe-10-1--------4~Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------Styrene
1330-20-7-------Total Xylenes
Q
10 u
10 u
10 u
10 u
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
5 u
5 u
10 u
5 u
5. u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
FORM I VOA 1/87 Rev.
20937 150 SAMPL~ DATA. ~UMMARV
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· lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REYS
PW-OJ-2MSD
Lab Code: COMPU Case No.: 20937 SAS No.: SOG No.: 150
Matrix: ( soil/water) WATER Lab Sample ID: 365262
Sample wt/vol: s,o (g/mL) Ml,__ Lab File IO: CR065262C03
Level: (low/med) LOW Date Received: 08/17/90
I Moisture: not dee. Date Analyzed: 08/30,:'.90
Column: (pack/cap) CAP Dilution Factor: .1~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u
74-83-9-----~---Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 1 BJ
67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
75-35-4----~----l,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-0----~---1,2-oichloroethene (total)_ 5 u
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-J-~-------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
1os~os-4--------vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-5------cis-l,J-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,J-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1os-10-1-~------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
1os-90-1--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
lJJo-20-1-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
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1B EPA. SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-02-1
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365249
Sample wt/vol: 500 (g/mL) m.....:_ Lab File ID: GH065249CQ7
Level: (low/med) I.OW Date Received: 08/17/90
\ Moisture: not dee. dee. Date Extracted: 08/20/90
Extraction: (SepF/Cont/Sonc) .s.,E,Pf Date Analyzed: 08/22/90
GPC Cleanup: (Y/N) ti_ pH: Dilution Factor: ¥R~·~s~o __
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4------~-bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,J-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-s2-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4------~--Hexachlorocyclopentadiene
88-06-2------~--2,4,6-Trichlorophenol --
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
so u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
.;: MC'l i:f' f"lOTO IIMM
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-02-1
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Casa No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365249
Sample wt/vol: 500 (g/mL) Ml._ Lab File ID: GH065249C07
Level: (low/med) IpW Date Received: 08/17/90 ·
, Moisture: not dee. dee. Date Extracted: Q8l20l90
Extraction: (SepF/Cont/Sonc) gu
GPC Cleanup: (Y/N) J:L pH:
Date Analyzed: 08/22/90
Dilution Factor: 0.50 ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGlL
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene ·
51-28-5---~-----2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-~4-9--------Dibenzoturan
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
· 534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
lOl-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------oi-n-Butylphthalate
20~-44-o--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-0ichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------oi-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------eenzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------0ibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(l) -cannot be separated from 01phenylamine
Q
50 u
10 u
50 u
50 u
10 u
i"o u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
· 10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
37 sa\ C::QMP!.:E. DATA SUMMARY
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP contract: 12-88)-REVS
Lab Code: CQMPU Case No.: '20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab sample ID:
PW-02-1
No.: 150
365249
Sample wt/vol: 500 (g/mL) Ml.__ Lab File ID: GH065249C07
Level: (low/med) _r,o=w~_
I Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) .5.Eff
GPC Cleanup: (Y/N) IL_ pH:
Number TICs found: __o_·
CAS NUMBER COMPOUND NAME
Date Received: 08/17/90
Date Extracted: 08/20/90
Date Analyzed: 08/22/90
Dilution Factor: ~9~,s_o~_
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
•••z=========m== -~===---=-----=-------=----= a======= =====m=Zll::::11:SZ&•--••:m=
FORM I SV-TIC 1/87 Rev.
20937 1 S0 SAMPLE~ DATA SUMMARY:
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP . Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 20937
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
I Moisture: not dee.
500
LOW
(g/mL) M.L...._
dee.
SAS No.: SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
EPA SAMPLE NO.
PW-OJ-1
No.: 150
365254
GH065254C07
08/17/90
08/20/90
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup:' (Y/N) lL_ pH:
Date Analyzed: 08/22/90
Dilution Factor: ~9~-~5~0 __
CAS NO. COMPOUND
109.;95-2----.:.---Phenor
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis('2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,J-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-oichlorobenzene
95-48-7-----~---2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-s2-1--------l,2,4-Trichlorobenzene
91-20-3----------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-J-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 150 SAMPLk D~TA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
\ PW-03-1
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SDG No.: _15~9~. _
·Matrix: (soil/water) WATER Lab Sample ID: ·&3&6~5L25~4.__ __ _
Sample wt/vol: 500 (g/mL) Ml,_ Lab File ID: GH065254C07
Level: ( low/med) LOW Date Received: 08/17/90
, Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) $.EP.f:
GPC Cleanup:_ (Y/N) H__ pH:
Date Extracted: 08/20/90
Date Analyzed: 08/22/90
Dilution Factor: ~9~•&5&0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,~-Dinitrophenol
100~02-7--------4-Nitrophenol
132-64-9------~-Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3----~--4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1-~------4,6-Dinitro-2-Methylphenol_
86-30-6----~----N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
. 84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -cannot be separated from Diphenylamine
0
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
20937 150 SAMPL~ DATA SUMMARY
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
sample wt/vol: 500 (g/mL) !1l........_ Lab File ID:
Level: (low/med) LOW Date Received:
' Moisture: not dee. dee. Date Extracted:
EPA SAMPLE NO.
PW-03-1
No.: 150
365254
GHQ65254CQ7
08/17/90
oaao190
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...._
gff
pH:
Date Analyzed: O!J/22/90
Dilution Factor: ~9~,5-9~-
Number TICs tound: __Q
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I SV-TIC 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY
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1-
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·is EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-OJ-2
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No.: 150
M_atrix: ( soil/water) WATER Lab Sample ID: 365260
Sample wt/vol: 500 (g/mL) Ml._ Lab File ID: GH065260C07
Level: ( low/med) LOW Date Received: 08/17/90
I Moisture: not dee. dee. Date Extracted: 08/20/90
Extraction: (SepF/Cont/Sonc) gu
GPC Cleanup: (Y/N) tL... pH:
Date Analyzed: 08/22/90
Dilution Factor: ~o~,~5~0 __
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,J-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-so-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-0imethylphenol
65-85-o---------Benzoic Acid
lll-9l-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---~-----Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,S-Trichlorophenol
91-58-7-.--------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------oimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
l_O u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u . 10 u
FORM I sv-1 1/87 Rev.
20937 150 \SAMPLE DATA SUMMARY
Q
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-03-2
Lab Name: COMPUCHEM,RTP Contract: {2-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365260
Sample wt/vol: 500 (g/mL) ~ Lab File ID: GH065260C07
Level: (low/med) LOW Date Received: 08/17/90
' Moisture: not dee. dee. Date Extracted: 08/20/90
Extraction: (SepF/Cont/Sonc) s..E.ff
GPC Cleanup: (Y/N) H..,_ pH:
Date Analyzed: 08/22/90
Dilution Factor: o,so
CAS NO, COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--~-~---2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101~55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-s---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32~8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
_(l) -Cannot be separated from Diphenylamine
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY
Q
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
PW-03-2
No.: 150
365260
sample wt/vol: 500 (g/mL) M1L_ Lab File ID: GH065260C07
Level: (low/med) LOW
I Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) .s..E.P.r
GPC Cleanup: (Y/N) Ii._ pH:
Number TICs found: ---2.
CAS NUMBER COMPOUND NAME
Date Received: 08/17/90
Date Extracted: 00ao120
Date Analyzed: 08/22/90
Dilution Factor: 0.50 ~~--
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
•=•=n•===•mm==n• ••••••===•==========aa=c==== •••=m=== ••==••=•a•a.:a: ==z:z=:a
FORM I SV-TIC 1/87 Rev.
20937 150 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: coMPUCHEM,RTP Contract: (2-881-REVS
PW-04-1
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365991
Sample wt/vol: 1000 (g/mL) Ml._ Lab File ID: GH065991C07
Level: (low/med) _LO=W __ Date Received: 08/21(90
I Moisture: not dee. dee. Date Extracted: 08/21/90
Extraction: (SepF/Cont/Sonc) gu Date Analyzed: 08/24/90
GPC Cleanup: (Y/N) Ji_ pH:-Dilution Factor: _1~,~o __ _
CAS NO. COMPOUND
108-9S-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
9S-S7-8-~----~--2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-Sl-6--------Benzyl Alcohol
9S-so-1---------1,2-Dichlorobenzene
9S-48-7---------2-Methylphenol
39638~32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-9S-3---------Nitrobenzene
78-S9-l---------Isophorone
88-7S-s---------2-Nitrophenol
lOS-67-9--------2,4-Dimethylphenol
6S-ss-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
S9-S0-7--~------4-Chloro-3-Methylphenol
91-S7-6---------2-Methylnaphthalene
7 7-4 7-4---------Hexach·l orocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-SS-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-_96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
.10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
so u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
so u
10 u
so u
10 u
10 .u
10 u
FORM I sv-1 l/S7·Rev.
20937 150 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-04-l
Lab Name: COMPUCHEM.RTP Contract: (2-88}-REVS
Lab Code: COMPU Casa No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365991
sample wt/vol: 1000 (g/mL) Ml._ Lab File ID: GH065991C07
Level: (low/med) LOW Date Received: 08/21/90
, Moisture: not dee. dee. Date Extracted: 08/21/90
Extraction: Date Analyzed: 08/24/90
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) L_ pH: Dilution Factor: .1~,o"----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
Sl-28-S---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzoturan
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
~OOS-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
S34-52-l--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-SS-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
ss-01-s---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrane
BS-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-Bl-7--------bis(2-Ethylhexyl)Phthalate_
117-84-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
5,0-32-8---------Benzo (a) Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracena
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from Diphenylamina
Q
so u
10 u
so u
so u
10 u
10 u
10 u
10 u
10 u
so u so u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
3 BJ
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
PW-04-l
No.: 150
365991
Sample wt/vol: 1000 (g/mL) MI....._ Lab File ID: GH065991C07
Level: (low/med) LOW
' Moisture:
Extraction:
GPC Cleanup:
not dee.
(SepF/Cont/Sonc)
(Y/N) li_
Number TICs tound: ~
dee.
pH:
CAS NUMBER COMPOUND NAME
Date Received: 08/21/90
Date Extracted: 08/21,:'.90
Date Analyzed: 08/24/90
Dilution Factor: .1~,~o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) QG/L
RT EST. CONC. Q
•••=•aa===m=•=== aaau==-===================m== =-======= ======-======== =====
• 0
FORM I SV-TIC l/87 Rev.
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18 EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-05-1
Lab NalJle: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab sample ID: 365992
Sample wt/vol: 1000 (g/mL) Ml....._ Lab File ID: GH065992C07
Level: (low/med) LOW Date Received: 08/21/90
, Moisture: not dee. dee. Date Extracted: 08/21/90
Extraction: ilU Date Analyzed: 08/24/90
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H...._ pH: Dilution Factor: .1~1~0 __ _
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UGiL
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6-----~--aenzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-e2-1-~------l,2,4~Trichlorobenzene
91.-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91~57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58~7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 t1
10 t1
10 t1
10 t1
10 u
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10. t1
10 t1
10 t1
10 t1
50 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
10 t1
50 t1
10 t1
50 t1
10 t1
10 t1
· 10 t1
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-05-1
Lab Name: COMPUCHEM.RTP Contract: /2-BBl-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab sample ID: 365992
Sample wt/vol: 1000 (g/mL) Ml,_ Lab File ID: GH065992C07
Level: (low/med) LOW Date Received: 08/21/90
' Moisture: not dee. dee. Date Extracted: 0£1/21/90
Extraction: (SepF/Cont/Sonc) .s..E..P.r Date Analyzed: 0£1/24/90
GPC Cleanup: (Y/N) lL_ pH: Dilution Factor: .1~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether
86-73-7-----~---Fluorene -
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,J'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-8l-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0-.-------Di-n-Octyl Phthalate ·
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrena
53-70-3---------Dibenzo(a,h)Anthracana
191-24-2--------Benzo(g,h,i)Parylana
( 1) -Cannot be separated from Diphenylamin.e
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
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: 1
lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP contract: /2-88l-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample IO:
PW-05-1
No.: 150
365992
Sample wt/vol: 1000 (g/mL) Ml...... Lab File IO: GH065992C07
Level: (low/med) LOW
' Moisture:
Extraction:
GPC Cleanup:
not dee.
(SepF/Cont/Sonc)
(Y/N) li,_
Number TICs found: ---2
dee.
pH:
CAS NUMBER COMPOUND
Sll.E
NAME
Date Received: 08/21/90
Date Extracted: 08/21/90
Date Analyzed: 08/24/90
Dilution Factor: .1~,~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q --===•--=-=•==== --===================••===== ======== ==•mac:zz:zm:za:ac m:::u;:i:cc
~. ~ FORM I SV-TIC 1/87 Rev.
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
PW-06-1
Lab Name: COMPUCHEM.RTP contract: (2-881-REVS
Lab Code: CQMPU Case No:: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365273
Sample wt/vol: 500 (g/mL) Ml...,_ Lab File ID: GH06527JC07
Level: (low/med) LOW Date Received: 08/17/90
' Moisture.: not dee. dee. Date Extracted: 08/20/9Q
Extraction: (SepF/Cont/Sonc) &Pl ·Date Analyzed: 08/22/90
GPC Cleanup: (Y/N) Ii,_ pH: .__ Dilution Factor: o. 50
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) ·uq/L Q
108-95-2--------Phenol 61
lll-44-4--------bis(2-Chloroethyl)Ether 28
95-57-8---------2-Chlorophenol 75
541-73-1--------1,J-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 U·
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
396JB-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 64
621-64-7--------N-Nitroso-Di-n-Propylamine __ 10 u
67-72-1---------Hexachloroethane 15
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 31
BB-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 10 u
120-83-2--~-----2,4-Dichlorophenol 10 u
120-e2-1-------~1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50.:7---------4-Chloro-·3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene __ 10 u
BB-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM,RTP contract: 12-881-REVS
PW-06-1
Lab code: COMPU Case .No.: 20937 SAS No.: SOO No.: .1,,_5.,.0 __
Matrix: (soil/water) WATER Lab sample ID: · ·..._3.,._65.,..2._7,_,3.__ __ _
Sample wt/vol: 500
LOW
(g/mL) Ml...._ Lab File ID: GH065273C07
Level: (low/med) Date Received: 08/17/90
I Moisture: not dee. dee. Date Extracted: 08/20/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H,_
.s.E.ff
pH:
Date Analyzed: 08/22/90
Dilution Factor: 0,50
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
. -
99-09-2---------3-Nitroaniline .
83-32-9---------Acenaphthene
s1-2s-s---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
ss-01-s---------Phenanthrene
120-12-1--------Anthracene
84-74-2---~-----Di-n-Butylphthalate
206-44-o-----~--Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55.-3---------Benzo ( a) Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalata_
117-84-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthena
50-32-8---------Banzo(a)Pyrana
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Parylena
(1) -cannot be separated from Diphenylamina
50 u
27
64
50 u
10 u
10 u
10 u
10 u
10 u
so u
50 u
10 u
10 u
10 u
63
31
10 u
10 u
10 u
25
10 u
20 u
10 u
10 u
5 J
10 u
4 J
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
PW-06-1
Lab Name: coMPUCHEM,RTP Contract: (2-BBl-REVS
Lab Code: COMPU case No.: 20937
Matrix: (soil/water) WATER
sample wt/vol: 500 (g/mL) Ml,__
Level: (low/med) LOW
I Moisture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li_
Number TICs found: --2.
dee.
pH:
CAS NUMBER COMPOUND NAME
SAS No.: S 0G No. : ,.1..,5.,.0 __
Lab Sample IO: ,.J_,.6..,s,.,_2.,_7.,_3 __ _
Lab File IO: GH065273C07
Date Received: -08/17/90
Date Extracted: 08/20/90
Date Analyzed: 08/22/90
Dilution Factor: ~O~,&s~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
•••••••=====-••=a m=====--------=-=--=====-=am ----==== ==•--====----•=-=a• 1. UNKNOWN 13.60 12 J 2. UNKNOWN 13.89 10 J
FORM I SV-TIC 1/87 Rev.
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
PW-07-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: ( soil/water) WATER Lab Sample ID: 365281
Sample wt/vol: 500 (g/mL) ML_ Lab File ID: GH0652§1C07
Level: (low/med) LOW Date Received: 08/17/90
I Moisture: not dee. dee. Date Extracted: 08/2Q/9Q
Extraction: (SepF/Cont/Sonc) Slll Date Analyzed: 08/22/90
Dilution Factor: Q.50-GPC Cleanup: (Y/N) H_
CAS.NO. COMPOUND
108-95-2--------Phenol
pH:
CONCENTRATION UNITS:
(ug/L or ug/Kg) QG/L
lll-44-4--------bis(2-Chloroethyl)Ether
9S-S7-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-Sl-6--------Benzyl Alcohol
9S-So-1---------1,2-Dichlorobenzene
9S-48-7---------2-Methylphenol
39638-32-9--~---bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7-------~N-Nitroso-Di-n-Propylamine_·_
67-72-1---------Hexachloroethane
98-9S-3---------Nitrobenzene
78-S9-l---------Isophorone
88-7S-s---------2-Nitrophenol
lOS-67-9--------2,4-Dimethylphenol
6S-ss-o---------Benzoic Acid
lll-9l-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-s2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
S9-S0-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
so u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
so u
10 u
10 u
· 10 u
FORM I sv-1 1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SOG
EPA SAMPLE NO.
PW-07-1
No.: 150 I Matrix: (soil/water) WATER Lab Sample ID: 365291
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Sample wt/vol: 500 (g/mL) Ml._ Lab File IO: GH065281C07
. Level: (low/med) LOW Date Received: 08/17/90
\ Moisture: not dee. dee. Date Extracted: 09/jil0/90
Extraction: (SepF/Cont/Sonc) Date Analyzed: 09/22/90
GPC Cleanup: (Y/N) li_ pH: Dilution Factor: ¥0~1~5~0 __
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u 83-32-9---------Acenaphthene 10 u 51-28-5---------2,t-oinitrophenol 50 u 100-02-7--------4-Nitrophenol 50 u
132-64-9--------0ibenzofuran 10 u 121-14-2--------2,4-Dinitrotoluene 10 u 84-66-2---------Diethylphthalate 10 u 7005-72-3-------4-Chlorophenyl-phenylether __ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
as-01-a---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------oi-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-oo-o--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 4 J
117-84-0--------oi-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
( 1) -cannot be separated _from Oiphenylamine . . ' ·::-·
FORM I sv-2 1/87 Rev.
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP contract: !2-88}-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
PW-07-1
No.: 150
365281
Sample wt/vol: 500 (g/mL) Ml,_ Lab File ID: GH065281C07
Level: (low/med) LOW
' Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) s..t.P.E
GPC Cleanup: (Y/N) JL_ pH:
Number TICs found:~
CAS NUMBER COMPOUND NAME
Date Received: 08/17/90
Date Extracted: 08/20/90
Date Analyzed: 08/22/90
Dilution Factor: 0.50
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
•••=========•a•• ••.••=m====maaa============== ======== •m=•=-=-==-===za=-•====
FORM I SV-TIC 1/87 Rev.
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REYS
PW-04-lMS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
• Matrix: (soil/water) WATER Lab Sample ID: 365255
Sample wt/vol: 500 (g/mL) Ml._ Lab File ID: GR065255B21
Level: ( low/med) LOW Date Received: 08/17/90
I Moisture: not dee. dee. Date Extracted: OBIH/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li...._
Slll
pH:
Date Analyzed: 08/24/90
Dilution Factor: _o~,~5~0 __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone.
88-75-5---------2-Nitrophenol <
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-e2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-.4---------2, 4, 5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
2oa·-96-a--------Acenaphthylene
606~20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u.
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
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lC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: (2-881-REVS
PW-04-lMS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab sample ID: 365255
Sample wt/vol: 500 (g/mL) tu.__ Lab File ID: GR06s2ssa21
Level: (low/med) I.OW Date Received: 08/17/90
' Moisture: not dee. dee. Date Extracted: 08/24/90
Extraction: (SepF/Cont/Sonc) 5_EH Date Analyzed: 08/24/90
GPC Cleanup: (Y/N) li,_ pH: Dilution Factor: 0,50
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline so u 83-32-9---------Acenaphthene 10 u Sl-28-5---------2,4-Dinitrophenol 50 u 100-02-1--------4-Nitrophenol so u
132-64-9--------Dibenzofuran 10 u 121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2------~--Diethylphthalate 10 u
700S-72-3-------4-Chlorophenyl-phenylether __ 10 u 86-73-7---------Fluorene 10 u 100-01-6-~------4-Nitroaniline so u
S34-S2-l--------4,6-Dinitro-2-Methylphenol __ so u
86-30-6----~----N-Nitrosodiphenylamine (l)_ 10 u lOl-SS-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol so u
es-01-a---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
"84-74-2---------Di-n-Butylphthalate 10 u
206-44-o--------Fluoranthene 10 u
129-00-o--------Pyrene 10 u
SS-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 20 u
S6-SS-3--------~Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bis(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------Di-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1)--Cannot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
PW-04-lMSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab sample IO: 365256
Sample wt/vol: 500 (g/mL) Ill,__ Lab File ID: GR065256B21
Level: (low/med) LOW Date Received: 08/17/90
I Moisture: not dee. dee. Date Extracted: 08/H/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li...._ pH:
ilf.E Date Analyzed: 08/24/90
Dilution Factor: ~0~,-5-0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bis(2-Chloroethyl)Ether-10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------l,3-Dichlorobenzene· 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1------~--l,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9--~---bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Ni trobenz.ene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2.4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bis(2~Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------l,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 U'
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 ·u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylena 10 u
606-20-2--------2,6~Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM.RT'.P Contract: (2-881-REVS
PW-04-lMSD
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: 150
Matrix: (soil/water) WATER Lab Sample ID: 365256
Sample wt/vol: 500 (g/mL) Ml.,__ Lab File IO: GR065256B21
Level: (low/med) LOW Date Received: 08,:'.12,:'.90
I Moisture: not dee. dee. Date Extracted: 08£'.24£'.90
Extraction: (Sep°F/Cont/Sonc)
GPC Cleanup: (Y/N) H.,_
_gp_[
pH:
Date Analyzed: 08£'.24£'.90
Dilution Factor: ~o-.s~o~_
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------0iethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol __
86-30-6-----~---N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
as-01-a---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------oi-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-o----~---Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3 1-0ichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------chrysene
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_
111-a4-o--------oi-n-octyl Phthalate
205-99-2------~-Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8~--------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from Oiphenylamine.
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 .U
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
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COMPUCHEM
LABOAATORJES
CLP CASE NARRATIVE --CASE 20937
SDG NO. 166
Contract No. (2-88) REVS
Compuchem Laboratories, Inc.
Samples: FB-03-1, MW-2R-l, MW05-l-l, MW06-l-l, MW08-l-l,
MW13-l-l, MW16-l-l, TB-10-1
Attached are pertinent Quality Assurance Notices dealing
with the analysis of eight (08) water samples associated
with Case 20937, SDG No.166. The samples were received
intact on August 24 and 25, 1990 in properly sealed shipping
containers with the corresponding chain-of~custody
documents. The courier was Federal Express. The samples
were logged into the Compuchem Laboratory Management system
and scheduled for the analysis of the volatile and the semi-
volatile fractions.
VOLATILES
The samples were analyzed within the proper holding time
requirements. EPA target compound list (TCL) analytes were
found in all of the samples ranging in number per fraction
from one (1) to ten (10). Sample FB-03-1 was identified as
a field blank. The analysis of 5ml of this sample confirmed
the presence of Methylene Chloride and Chloroform. Since
the preceding sample did not contain elevated levels of the
above two compounds, we do not believe the reported values
to be the result of carryover .. we are reporting these data
with reference to the enclosed qu9-1ifier. In sample MW0S-1-
1, three (3) tentatively identified compounds (TIC) were
found. None of the remaining samples contained any TICs.
In the volatile fractions, recovery and RPD values met QC
limits in. the matrix spike, MWlJ-1-1 MS, and the matrix
spike duplicate, MWlJ-1-1 MSD. In addition to the spiking
compounds, Methylene Chloride, Acetone, 1,1-Dichloroethane,
cis-1,2-Dichloroethene, 1,1,1-Trichloroethane, and
Tetrachloroethene were present in the MS and the MSD.
Spiking compounds 1,1-Dichloroethene and Trichloroethene
were present in the original sample, MWlJ-1-1, from which
the duplicate sample spikes were prepared. Volatile
instrument blank VBLKIV did not contain any TCL compounds.
TCL analytes were present in the remaining three blanks
ranging in number per blank from one (1) to two (2). There
were no TICs present in any of the four blanks. Surrogate
recovery values for the samples, the instrument blanks, and
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 (919) 549·8263 (i 0
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----COMPIJCHEM
IABOAATORIES
the duplicate sample spikes passed contract required QC
limits.
SEMI-VOLATILES
The samples were extracted and analyzed within holding time
limits. Surrogate recovery values for 2-Fluorophenol and
05-Phenol fell outside of the quality control limits in both
the original and the repeated extraction procedures in
sample MW05-l-1. Results were comparable. between the two
analyses. Since all other QC criteria associated with these
analyses were met, we have attributed the out-of-control
surrogate recovery values to the particular sample matrix
rather than to deficiencies in the laboratory's analytical
system. We are reporting both sets of data for sample MW05-
1-1 with reference to the enclosed qualifier.
Samples FB-03-1, MW-2R-1, MW06-l-1, and MW-08-1-1 did not
contain any TCL compounds. TCL compounds were, however
present in the remaining samples ranging in number per
fraction from one (1) to three(3). Bis (2-Ethylhexyl)
phthalate was found in all of the samples were TCL compounds
were present. There were no TICs found in samples FB-03-1,
MW06-1-1, and MWOB-1-1. TICs were present in the remaining
samples ranging in number per fraction from pne (1) to eight
( 8) •
In the semi-volatile fractions, recovery and RPO values met
QC requirements in the matrix spike, MW-13-1-1 MS and the
matrix spike duplicate, MW13-l-1 Mso; In addition to the
spiking compounds, 2-Nitrophenol and Bis (2-Ethylhexyl)
phthalate were ~resent in the MS and the MSD. None of the
three semi-volatile method blanks contained any TCL analytes
or TICs. In samples MW05-1-1 and MW-05-1-1 RE, surrogates
2-Fluorophenol and 05-Phenol failed recovery criteria. In
sample MW-16-1-1, 2-Fluorophenol failed recovery limits.
Surrogate· recovery values for the remaining samples, the
method blanks, and the sample spikes were acceptable. In
both the volatile and the semi-volatile fractions~ initial
and continuing calibration criteria were met.
I certify that this data package is in compliance with the
terms and conditions of the contract, both technically and
for completeness, for other than the conditions detailed
above. Release of the data contained in this hardcopy data
2
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----Q),\,,1PUCHEM
IABOMTORIES
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature:
iewer
1990 09 / 1~10'0
Note: This report is paginated for reference and
accountability in decreasing numerical sequence.
3
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
I.ab Name: CQMPUCHEM,RTP Contract: f2-88}-REVS FB-03-1
Lab Code : COMPO -· .
Case No.: 20937 SAS No.: SDG No. : ,.1,si6,si6 __
Matrix: (soil/water) WATER I.ab Sample IO: 367035
sample wt/vol: 5,0 (g/mL) Ml.,._ I.ab File ID: CN067035B0J
Level: (low/med) LOW Date Received: I , Moisture: not dee.
08/25/90
Date Analyzed: 09/03/90
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ColUJ1111: (pack/cap) CAP Dilution Factor: .i~,~o'----
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 t1 74-83-9---------Bromomethane 10 t1 75-01-4---------Vinyl Chloride 10 t1 75-00-3---------Chloroethane 10 t1 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone 10 t1 75-15-o---------carbon Disulfide 5 t1 75-35-4---------1,1-0ichloroethene 5 t1 75-34-3---------1,1-0ichloroethane 5 t1 540-59-0--------l,2-Dichloroethene (total)_ 5 t1 67-66-3---------Chloro!orm 12 107-06-2--------1,2-oichloroethane 5 t1 78-93-3----•----2-Butanone 10 t1 71-55-6---------1,1,1-Trichloroethane 5 t1 56-23-5---------carbon Tetrachloride 5 t1 108-05-4--------Vinyl Acetate 10 t1 75-27-4---------Bromodichloromethane 5 t1 78-87-5---------1,2-0ichloropropane 5 t1 10061-01-5------cis~l,3-0ichloropropene 5 t1 79-01-6---------Trichloroethene 5 t1 124-48-1--------0ibromochloromethane 5 t1 79-oo-s---------1,1,2-Trichloroethane 5 t1
71-43-2-----~---Benzene 5 t1
10061-02-6------Trans-l,3-0ichloropropene_ 5 t1 75-25-2---------Bromotorm 5 t1 1oe-10-1--------4-Methyl-2-Pentanone 10 t1 591-78-6-------~2~Hexanone 10 t1 127-18-4--------Tetrachloroethene 5 t1
79-34-5---------1,1,2,2-Tetrachloroethane_ 5 t1 108-88-3--------Toluene 5 t1
108-90-7--------Chlorobenzena 5 t1
100-41-4--------Ethylbenzene 5 t1 100-42-s--------styrene 5 t1
1330-20-7-------Total Xylene11 5 t1
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
FB-03-1 Lab Name: CQMPUCHEM.RTP Contract: C2-BB}-REVS •·
Lab Code: CQMPU Caee No.: 20937 SAS No.: SDG. No.: ...,l..,66...__
Matrix: (soil/vater) WATER Lab Sample ID: .,.3.,.6.._7.,,.0.._35il-__ _
Sample vt/vol: 5.0 (g/mL) ~ Lab File ID: CH0§703SBOJ
Level: (lov/med) LOW
I Moisture: not dee.
Colllllln (pack/cap) CAP
Number TIC• found: ___g_
CAS NUMBER COMPOUND NAME
Date Received: 08/25/90
Date Analyzed: 09/03/90
Dilution Factor: .i~·~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q ==========-=== ===------==----=----=--=-=== •m=a=• ---=====-:a •:::it=-==
FORM I VOA-TIC 1/87 Rev.
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EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
KW-2R-l Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS Lab code: coMPU _. case No.: 20937 SAS No.: SDG No.: ,.1.,.6.,.6 __ Matrix: (soil/water) WATER Lab Sample ID: ,._l.,.67'"'0"'3.._7.___ __ _ sample wt/vol: 5.0 (g/mL) Hl._ Lab File IO: C2R67037CO:J Level: ( low/med) LOW
I Moisture: not dee.
Column: (pack/cap) CAP
Date Received: OB/25/90
Date Analyzed': 09/04/90
• Dilution Factor: .1~1.,.0 __ _
CONCENTRATION UNITS: CAS NO, COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane
10 u 74-83-9---------Bromomethane
10 u 75-01-4~--------Vinyl Chloride
10 u 75-00-3--~------Chloroethane
10 u 75-09-2---------Methylene Chloride
5 u 67-64-1---------Acetone
4 J 75-15-o---------carbon Disulfide
5 u 75-35-4---------1,1-Dichloroethene
5 u 75-34-3---------1,1-0ichloroethane
5 u 540-59-0--------1,2-oichloroethene
(total)_ 5 u 67-66-3---------Chlorotorm
10 107-06-2--------1,2-oichloroethane
5 u 78-93-3---------2-Butanone
10. u 71-55-6---------1,1,1-Trichloroethane
5 u 56-23-5---------carbon Tetrachloride
5 u 1oe-os-4--------vinyl Acetate 10 u 75-27-4---------Bromodichloromethane
5 u 78-87-5---------1,2-Dichloropropane
5 u 10061-0l-5------cis-l,J-Dichloropropene
5 u 79-01-6---------Trichloroethene
5· u 124-48-1--------Dibromochloromethane
5 u 79-00-5---------1,1,2-Trichloroethane
5 u 71-43-2---------Benzene
5 u 10061-02-6------Trans-1,J-Oichloroprop
e
n
e
_

5 u 75-25-2---------Bromotorm
5 u 100-10-1--------4-Methyl-2-Pentanone
10 u 591-78-6--------2-Hexanone
10 u 127-18-4--------Tetrachloroethene
5 u 79-34-5-----~---l 1 2 2-Tetrachloroethane , , , -5 u 108-88-J--------Toluene
5 u 108-90-7--------Chlorobenzene
5 u 100-41-4--------Ethylbenzene
5 u _100-42-s--------styrana
5 u 1330-20-7-------Total ·Xylanes
5 u
FORM I VOA 1/87 Rev.
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: ·c2-aa1-_Rzys .· Lab Code : COMPU case No.: 20937 SAS No.: SOG Matrix: ( 11oil/water) WATER Lab Sample ID: Sample wt/vol: 5,0 (g/mL) Jil._ Lab File IO: Level: (low/med) LOH Date Received: t Moisture: not dee. Date Analyzed:
EPA SAMPLE NO.
MW-2R-1
No.: 166
367037
C2R67037CQ3
QB/25/90
09/0~/90 Column (pack/cap) CAP Dilution Factor: .1.1 0,._ __
Number TICs tound: --2
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
RT EST. CONC. •a===•••===-==== ==•a====================••=a •••===•a ••••••a-••••
)
FORM I VOA-TIC 1/87 Rev.
Q =====
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MWOS-1-l Lab Name: CQMPUCHEM,BTP Contract: (2-88)-REVS . ,
Lab Code: CQMPIJ case No.: 20937 SAS No.: SDG No.: ,..1.,.6.,.6 __
Matrix: (soil/water) WATER Lab Sample ID: 366940 Sample wt/vol: 5.0 (g/mL) m....._ Lab File ID: !:N06§94QAQ3 Level: (low/med) LOW Date Received: 08/24/90 I Moisture: not dee. Date Analyzed: 09101190 Column: (pack/cap) !:AP Dilution Factor: .1~,.,.o __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane
10 u 74-83-9---------Bromomethane 10 u· 75-01-4---------Vinyl Chloride 8 J 75-00-3-------~-Chloroethane
10 u 75-09-2---------Methylene Chloride 3 J 67-64-1---------Acetone
10 u 75-15-o---------carbon Disulfide 5 u 75-35-4---------1,1-Dichloroethene 23 75-34-3---------1,l-Dichloroethane
24 540-59-0--------1,2-Dichloroethene (total)_ 150 67-66-3---------ChlorofoI"lll
5 u 107-06-2--------1,2-Dichloroethane
5 u 78-93-3---------2-Butanone
10 u 71-55-6---------1,1,1-Trichloroethane
29 56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane
5 u 78-87-5---------1,2-Dichloropropane
5 u 10061-0l-5------cis-l,J-Dichloropropene
5 u 79-01-6---------Trichloroethene 45 ,, 124-48-1--------Dibromochloromethane
5 u 79-00-5---------1,1,2-Trichl'oroethane
5 u 71-43-2---------Benzene 1 J 10061-02-6------Trans-l,J-Dichloropropene_
5 u 1s-2s-2---------BromofoI"111
5 u 1oa-10-1--------4-Kethyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene
44 79-34-5---------1,1,2,2-Tetrachloroethane_
5 u 1oa-aa-J--------Toluene
5 u 108-90-7--------Chlorobenzene
5 u 100-41-4--------Ethylbenzene
5 u 100-42-s--------styrene
5 u 1330-20-7-------Total Xylene■ 2 J
FORK I VOA 1/87 Rev.
' ........ ' ' .. '.
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM,RTP Contract: <2-88)-REVS
EPA SAMPLE NO.
Lab code: CQMPU Case No.: 20937 SAS No.: S DG No. : _16_6..__ Matrix: (soil/water) WATER
sample wt/vol: 5,0 (g/mL) ML_
Level: (low/med) LOW
t Moisture: not dee.
column (pack/cap) S::AP
Number TICs found: -1.
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
RT EST, --
366940
CN06§940A03
08/24/90
09/01/90
i,o·
CONC. Q ----------------••••••••~•••••••m•••a••••••• ---------------------••a•= l. 76-13-1 ETHANE,l,l,2-TRICHLOR0-1,2,2 1.52 240 J 2. ETHYLMETHYLBENZENE 12.92 11 J 3. TRIMETHYLBENZENE 13.25 29 J
·,FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW06-l-l Lab Name: COMPUC~EM,_RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _.1.,.6.,.6 __ Matrix: (soil/water) WATER Lab Sample ID: ...,3...,67.,_0,...2,._7,__ __ _ Sample wt/vol: s,o
LOW
(g/mL) lila.-Lab File ID: CN067027COJ Level: (low/med) Date Received: 08/25/90
Date Analyzed: 09/04/90
t Moisture: not dee.
column: (pack/cap) CAP Dilution Factor: .1~1~0 __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Acetone
75-15-o---------carbon Disulfide 75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
(total)_
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride 108-05-4--------Vinyl Acetate 75-27-4---------Bromodichloromethane
78-87-s---------1,2-oichloropropane
10061-01-s------cis-l,l-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--~-----Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethane
71-43-2---------Benzene . 10061-02-6------Trans-l,3-Dichloropropene_
75-25-2---------Bromoform
1oe-10-1--------4~Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tatrachloroethane_
1oe-se-J--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-,2-s--------styrena
1330-20-7-------Total Xylenes
10 u
10 u
10 u
10 u
5 u
10 u
5 u
6
4 J
6
5 u
5 u
10 u
6
5 u
10 u
5 u
5 u
5 u
38
5 u
5 u
5 u
5 u
5 u 10 u
10 u
13
5 u
5 u
5 u
5 u
5 u
5 u
FORM I VOA 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
0
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHf:M,RTP Contract: (2-88)-REYS
EPA SAMPLE NO.
MW06-l-l
Lab code : COMPO ca■e No.: 20937 SAS No.: SDG No.: ,.1,..6.,.6 __
Matrix: (■oil/water) WATER
Sample wt/vol: 5.0 (g/mL) tu...._
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TIC• tound: ~
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File IO:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Xg) UC/L
RT EST.
367027
CN067Q27CQ3
08/25/90
Q9/Q~/90
l,Q
CONC. Q ----------------•••••-••m••••••••••••••••••• -------------------------
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW0S-1-1 Lab Name: CQMPUCHEM,BTP Contract: (2-88\-REVS
Lab Code: coMpu Case No.: 20937 SAS No.: SDG No. : .1.,.6.,.6 __
Lab Sample ID: ~3~67~0~2~9"----
Matrix: (soil/water) WATER
sample wt/vol: !5.0 (g/mL) tU.,_ Lab File ID: CNQ67029C0J
Level: (low/med) I.OW Date Received: 08/25/90
I Moisture: not dee. Date Analyzed: 09/04/90
Column: (pack/cap) CllP I Dilution Factor: .1~1~0 __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
-74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 J 67-64-1---------Acetone 10 u 75-15-o---------carbon Disulfide 5. u 75-35-4---------1,1-Dichloroethene 2 J · 75-34-3-----~---l,l-Dichloroethane 26 540-59-0--------1,2-Dichloroethene (total)_ 3 J 67-66-3---------Chlorotorm 5 u 101-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane
• 6 56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane 5 u 78-87-5---------1,2-Dichloropropane 5 u 10061-0l-S------cis-l,3-Dichloropropene 5 u 79-01-6---------Trichloroethene 5 124-48-1--------Dibromochloromethane 5 u 79-00-5---------1,1,2-Trichloroethane 5 u 71-43-2---------Benzene 5 u 10061-02-6------Trans-l,3-Oichloropropene __ 5 u 75-25-2---------Bromotorm 5 u 1oa-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 1 J 79-34-5---------1,1,2,2-Tetrachloroethane_ 5 u 108-88-3--------Toluene 5 u 108-90-7--------Chlorobenzene 5 u 100-41-4--------Ethylbenzene 5 u 100-42-s--------styrene 5 u . 1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
MWOB•l·l Lab Name: CQMPUCH~M,BTP contract: C2•88\•REVS
Lab Code: c;QMPU . Case No.: 20937 SAS No.: SOG No.: ...,1.,.66.....__ Matrix: (soil/water) WATER Lab Sample ID: ,.3.,.6.._7...,0.._29..._ __ _ Sample wt/vol: 5.0 (g/mL) m.._ Lab Fil• ID: CN067029CQ3 Leval: (low/mad) LOW
I Moisture: not dee.
Column (pack/cap)· CAP
Number TICs found: _J2
CAS NUMBER COMPOUND NAME
Data Received: OB/25/90.
Date Analyzed: 09/04/90
Dilution Factor: Al_._.o..__ __
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
RT EST. CONC. Q ----------------•••m••••====•=~••••••••••••• ----------------------
FORM I VOA-TIC 1/87 Rav.
----------· ------··----.....
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-l-l Lab Name: COMPUCHfoM,RTP Contract: (2-88)-REVS
Lab Code: COMPU case No.: 20937 SAS No.: SDG No. : _.1.,.6.,.6 __
Matrix: (soil/water) HATER Lab Sample ID: .3_6_6.._9..,5~4 ___ _ Sample wt/vol: 5.0 (g/mL) m._ Lab File ID: CR066954A03 Level: (low/med) LOW
t Moisture: not dee.
Date Received: 08/24/90
Date Analyzed: 09/01/90
Column: (pack/cap) Ct.P Dilution Factor: .1~1.,.0 __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane
10 u 74-83-9---------Bromomethane .. 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane
10 u 75-09-2---------Methylene Chloride 1 J 67-64-1---------Acetone
7 BJ 75-lS-o---------carbon Disulfide 5 u 75-35-4---------1,1-Dichloroethene
28 75-34-3---------1,1-Dichloroethane 30 540-59-0--------1,2-Dichloroethene (total)_ 2 J 67-66-3---------Chloroform
5 u 107-06-2---~----l,2-Dichloroethane
5 u 78-93-3---------2-,Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 94 56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane
5 u 78-87-5---------1,2-Dichloropropane
5 u 10061-01-5------cis-l,3-Dichloropropene
5 u 79-01-6---------Trichloroethene
17 124-48-1--------Dibromochloromethane
5 u 79-oo-s---------1,1,2-Trichloroethane 5 u 71-43-2---------Benzene 5 u 10061-02-6------Trans-l,3-Dichloropropene_
5 u 75-25-2--------,-Bromoform
5 u 1os-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene 2 J 79-34-5---------1 1 2 2-Tetrachloroethane , , , -5 u 108-88-3--------Toluene 5 u 108-90-7--------Chlorobenzene
5 u 100-41-4--------Ethylbenzene 5 u 100-42-5--------styrene 5 u 1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
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lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP . . contract: 12-88)-REYS
EPA SAMPLE NO,
HWlJ-l-l
Lab Code: CQMPU case No.: 20937 SAS No.: SDG No.: _16_6 __
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) Ml._
Level: (low/med) LQW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs tound: __Q
CAS NUMBER COMPOUND NAME
Lab Sample IO:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Xg) UG/L
RT EST.
366954
CR066954A03
08/24/90
09/01/90
1,0
CONCa· ·. ·""Q •=============== ========•=============•=•==• ----------====•------====
FORM I VOA-TIC. 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW16-l-l Lab Name: CQMPUCHEM,BTP contract: c2-esl-REVS
Lab code: COMPU Case No.: 20937 SAS No.: SOG No.: 166 Matrix: (soil/water) WATER Lab Sample IO: 366956 Sample wt/vol: 5,0 (g/mL) m..._ Lab File IO: C2R66956AOJ Level: ( low/med) LOW Date Received: 08/24/90 \ Moisture: not dee. Date Analyzed: 09/0i/90 Column: (pack/cap) CAP Dilution Factor: al~,~O'----
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Aeetone
75-15-0---------carbon Disulfide 75-35-4------~--l,l-Oiehloroethene
75-34-3---------1,1-Diehloroethane
540-59-0--------1,2-oiehloroethene
67-66-3---------Chloroform
107-06-2--------1,2-Diehloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(total)_
71-55-6---------1,1,1-Triehloroethane
56-23-5---------carbon Tetrachloride 10a-05-4--------vinyl Acetate 75-27-4---------Bromodiehloromethane
78-87-5---------1,2-Diehloropropane
10061-01-5------eis-l,3-Diehloropropene
79-01-6---------Triehloroethene
12,~,a~1--------Dibromoehloromethane
79-oo-s---------1,1,2-Trienloroethane
71-43-2---•-----Benzene
10061-02-6------Trana-l,3-0iehloropropene_
75-25-2---------Bromoform
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetraehloroethene
79-34-5---------1,1,2,2-Tetraehloroethane_
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-s--------styrene
1330-20-1-------Total Xylene•
Q
10 u 10 u
10 u
10 u
4 BJ
10 u
5 u
18
43
5 u
2 J
5 u
10 u
51
5 u
10, u
5 u
5 u
5 u
2 J
5 u
5 u
5 u
5 u
5 u
10 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
FORM I VOA 1/87 Rev.
1 ,:.,:. COM/:'/ ,: r,oTO CI/MMOl:>V
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
MW15-l-l Lab Name: COMPUCHfOH,RXP Contract: 12-BBl-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _1_66 __
Matrix: (soil/water) WATER
Sample wt/vol: 5.0
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs tound: __!2
,•
CAS NUMBER
(g/mL) tfi.._
COMPOUND NAME
Lab Sample ID: ..,3..,6.,..69,._5""6..._ __ _
Lab File ID: C2R66956AOJ
Date Received: 08/24/90
Date Analyzed: 09/02/90
Dilution Factor: .1~1 0,._ __
CONCENTRATION UNITS: (ug/L or ug/Kg) ·uG/L
RT EST. CONC. Q •••••••••a•••=-.•• ••••••z•••••••••==••==-•••••• ------------------------=--
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SKEET
TB-10-1 Lab Name: COMPUC~EM.~TP Contract: (2-88)-REVS
Lab Code: CQMPU case No.: 20937 SAS No.: ----SOG No.: ,.1.,.6.,.6 __ Matrix: (soil/water) WATER Lab Sample ID:. ..i3j/.6.,i.6.il..9a.5851.-__ _ sample wt/vol: 5.0 (g/mL) HL.. Lab File ID: CN0669SBA03 Level: (low/med) LOW Date Received: 08/24/90 I Moisture: not dee. Date Analyzed: 09/01/90 Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) Y!itL Q
74-87-3---------chloromethane
10 lJ 74-83-9---------Bromomethane
10 lJ . _.75~_01-4---------Vinyl Chloride 10 u 75-00-3---------chloroethane
10 lJ 75-09-2---------Methylene Chloride 2 J 67-64-1---------Acetone
10 lJ 75-15-o---------carbon Disulfide 5 u 75-35-4---------1,1-Dichloroethene
s u 75-34-3---------1,l-Dichloroethane
s lJ 540-59-0--------1,2-Dichloroethene (total) ___ 5 u 67-66-3---------Chloroform
5 u 107-06-2--------1,2-Dichloroethane
5 u 78-93-3---------2-Butanone
10 u 71-55-6---------1,1,1-Trichloroethane
5 u 56-23-s---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acet.ate 10 u 75-27-4---------Bromodichloromethane
5 u 1a-a1-s---------1,2-Dichloropropane
5 u. 10061-0l-s-----~cis-l,J-Dichloropropene
5 u 79-01-6---------Trichloroethene
5 u .. 124-48-1--------Dibromochloromethane
5 u 79-00-s---------1,1,2-Trichloroethane
5 u 71-43-2---------senzene
5 u 10061-02-6------Trans-l,3-Dichloropropene_
5 u 1s-2s-2---------Bromotorm
5 u 1oa-10-1--------4-Methyl-2-Pentanone
10 u 591-78-6--------2-Kexanone
10 u 127-18-4--------Tetrachloroethene
5 u 79-34-5---------1 l 2 2-Tetrachloroethane 5 u . It I -108-88-3--------Toluene
5 u 108-90-7--------chlorobenzene
5 u 100-41-4--------Ethylbenzene
5 u 100-42-5--------styrene
5 u 1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rav.
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1-
lE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPQCHJ;M,iTP contract: (2-88}-REVS
EPA SAMPLE NO.
TB-10-i
Lab Coda: COMPIJ Caaa No.: 20937 SAS No.: SOG No. : .,16 ... 6.___ Matrix: ( soil/water) WATER
Sample wt/vol: 5.0 (g/mL) MI,,__
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) ,a2
. Number TICs tound: ___!2
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
RT EST.
36§958
CN0t56958A03
08/24/90
09/01/90
1.0
CONC. Q ===========•==== aa:a=======~=====m=z=====•=== a======= --=-=•:a==•=• =-::a==
FORM I VOA-TIC 1/87 Rev.
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lA EPA SAMPLE NO. ' VOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-l-1MS Lab Name: COMPUCHEM,BIP contract: (2-BBl-RE;YS
Lab Code: COMPU caae No.: 20937 SAS No.: SDG No.: 16§ Matrix: (soil/water) WATER Lab Sample ID: 366945 Sample wt/vol: s,o (g/mL) Ml.._ Lab File ID: CR0§6945AOJ Level: (low/med) LOW Date Received: 08/24/90 I Moisture: not dee. Date Analyzed: 09/02,:'.90 Column: (pack/cap) CAP Dilution Factor: .1~1~0 __ _
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane
10 u 74-83-9---------Bromomethane
10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane
10 u 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone
6 J 75-15-o---------carbon Disulfide 5 u 75-35-4---------1,l-Dichloroethene
5 u 75-34-3---------1,l-Dichloroethane
32 540-59-0--------1,2-Dichloroethene (total)_ 2 J 67-66-3---------Chloroform
5 u 107-06-2--------1,2-Dichloroethane
5 u 78-93-3---------2-Butanone
10 u 71-55-6---------1,l,1-Trichloroethane
100 56-23-5---------carbon Tetrachloride 5 u 1oe-os-4·--------vinyl Acetate 10 u 75-27-4---------Bromodichloromethane
5 u 78-87-5---------1,2-Dichloropropane
5 u 10061-0l-5------cia-1,J-Dichloropropene
5 u 79-01-6---------Trichloroethene
5 u .. 124-48-1--------Dibromochloromethane
5 u 79-00-5---------1,1,2-Trichloroethane
5 u 71-43-2---------Benzene
5 u 10061-02-6------Trans-1,3-Dichloropropene_
5 u 75-25-2---------Bromoform
5 u 1oe-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u 127-18-4--------Tetrachloroethene
2 J 79-34-5---------1,1,2,2-Tetrachloroethane_
5 u 108-88-3--------Toluene 5 u 108-90-7--------chlorobenzene
5 u 100-41-4--------Ethylbenzen•
·5 u 100-42-5--------styrene 5 u 1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-l-1MSO Lab Name: CQMPUCl!EM.RTP Contract: C2-88)-BEYS
Lab Code: CQMPU Case No.: 20937 SAS No,: SDG No.: 166 Matrix: (soil/water) WATER Lab Sample IO: 366946 Sample wt/vol: 5.0 (g/mL) Ml._ Lab File ID: CN066946AOJ Level: (low/med) LOW Date Received: !181'.,B l'.90 I Moisture: not dee.-Date Analyzed: !191'.021'.90 Column: (pack/cap) CAP Dilution Factor: al~,~o __ _
CAS NO. COMPOIJND
74-87-3---------chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride 75-00-3---------Chloroethane
75-09-2---------Methylene Chloride 67-64-1---------Acetone
75-15-o---------carbon Disulfide 75-35-4---------1,1-0ichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-oichloroethene
67-66-3---------Chlorotonn
107~06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS: (ug/L or ug/Kg) YGl'.L
(total)_
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride 108-05-4--------Vinyl Acetate 75-27-4---------Bromo~ichloromethane
78-87-5---------1,2-0ichloropropane
10061-0l-5------cis-l,3-0ichloropropene
79-01-6---------Trichloroethene
124-48-1-~------Dibromochloromethane
79-oo-s-----~---1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-l,3-Dichloropropene_
75-25-2---------Bromotorm
1oa-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,:z-Tetrachloroethane_
108-88-3--------Toluene
108-90-7--------chlorobenzene
100-41-4--------Ethylbenzene
100-4:z-s--------styrene
1330-20-7-------Total Xylenes
Q
10 u
10 u 10 u
10 u
2 BJ
7 J
5 u
5 u
33
2 J
5 u
5 u
10 u
97
5 u
10 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
5 u
10 u
10 u
:z J
.5 u
5 u
5 u
5 u
5 u
5 u
FORM I VOA 1/87 Rev.
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1B
SEMIVOL\TILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHEM,RtP Contract: r2-aa1-REVS
EPA.SAMPLE NO.
, . FB-03-1
Lab Code: CQMPY caae No.: 20937
Matrix: (■oil/water) WATER
Sample wt/vol: 1000 (g/mL) ISL..
Level: (low/med) I.OW
I Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) .$I.fl
GPC Cleanup: (Y/N) H,_ pH:
SAS No.: S 0G No • : _.1,.,6 6..___
Lab Sample ID: ,..J .. 6.L.2Pw.3,1.,5L-__ _
Lab File ID: GH067035A05
Date Received: 08/25/90
Date Extracted: 08/27/90
Date Analyzed: 09/01/90
Dilution Factor: .1~1~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Xg) UG/L Q
108-95-2--------Phenol 10 u lll-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u 541-73-1--------1,3-Dichlorobenzene 10 u 106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u 95-50-1---~-----1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine_·_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u 65-es-o---------Benzoic Acid 50 u
lll-91-l--------bi■(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-e2-1-------.-1, 2, 4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u 91-57-6 ______ ..; __ 2.;.Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 u
ee-0,-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroanilin• 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-a--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene . 10 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO.
SEKIVOLATILE ORGANICS ANALYSIS DATA SHEET
FB-03-1
Lab Name: CQMPUAJE!1, RTP contract: CZ-BBi-REYS
' Lab Code: CQMPU Case No.: 20937 SAS No.: __ _ SDG No.: 1§§
Matrix: (soil/water) WATER Lab Sample ID: &3~§7~0~3~5._ __ _
Sample wt/vol: 1000 (g/aL) lllL_ Lab File ID: GH0§7035A05
Level: (low/med) LOW Date Received: 08/25/90
Date Extracted: 08/27/90
Date Analyzed: 09/01/90
Dilution Factor: &1~,o,._ __
, Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) llP.[
GPC Cleanup: (Y/N) Ji_ pH:
CONCENTRATION UNITS:·
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------J-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 1J
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-1,-2--------2,4-Dinitrotoluene· 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
a&-73-7---------Fluorane 10 u
100-01-6--------4-Nitroaniline 50 U·
534-52-1--------,,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (1)_ 10 1J
101-55-3--------,-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-a---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
a,-1,-2---------Di-n-Butylphthalate 10 u " 206-44-0--------rluoranthen• 10 u
129-00-0--------Pyr•n• 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidin• 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
117-81-7--------bia(2-Ethylhexyl)Pbthalate_ 10 u
111-a,-o--------Di-n-OC:tyl Phthalate 10 1J
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 1J
50-32-8---------Benzo(a)Pyren• 10 u
193-39-5--------Indeno(l,2,3-cd)Pyren• 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-2,-2--------Benzo(g,b,i)Perylene 10 1J
(1) -Cannot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
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lF
SEKIVOU.TILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM, RTP Contract: 12-88)-REVS
.· Lab Code: COMPU Ca11e No.: 20937 SAS No.: SOG
Matrix: (aoil/vater) WATER Lab Sample ID:
Sample vt/vol: 1000 Lab File IO:
Level: (lov/med) LOW Date Received:
I Moisture: not dee. dee. Date Extracted:
Extraction: (SepF/Cont/Sonc) llU Date Analyzed:
EPA SAMPLE NO.
FB-03-1
No.: 166
367035
CH067035A05
08/25/90
08/27/90
09/01/90
GPC Cleanup: (Y/N) H-pH: Dilution Fact:or: 1,0
NWllber TICS found: ___..l2
CAS NUMBER COMPOUND NAME
CONCENTRATION UNITS:
(ug/L or ug/Kg) UC/L
. RT EST. CONC.
--------------------------------------------------------
· •.. FORM I SV-TIC 1/87 Rev.
Q ----
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-05-1-1
Lab Name: CQMPUCHEM.RTP Contract: 12-BB)-REYS .·
Lall Coda: CQMPU Ca11a No.: 20937 SAS No.: SDG No.: 166
Matrix: (11oil/vatar) WATER Lab Sample ID: 366940
Sample vt/vol: 1000 (g/mL) Ml._ Lall Fila ID: GH066940AQ5
Level: (lov/med) LOW Data Received: 08/24/90
I Moisture: not dee. dee. Data Extracted: 08/25/90
Extraction:
GPC Cleanup:
(SapF /Cont/Sonc)
(Y/N) IL.. pH:
Data Analyzed: OB/27/90
Dilution Factor: alL,o,.__ __
CONCENTRATION UNITS:
CAS NO. COMPOUND . (ug/L or ug/lCg) UG/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bia(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1 3-Dichlorobenzene . , 10 u
106-46-7--~-----l,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bi11(2-Chloroi110propyl)Ether 10 u
106-44-5--------4-Mathylphanol 10 u
621-64-7--------N-Nitro110-Di-n-Propyla11_ine_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorona 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bia(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-82-1--~-----1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalen• 5 J
106-47-8--------4-Chloroanilin• 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 7 J
77-47-4---------Hexachlorocyclopentadiene_ 10 u
88-06-2---------2., 4, 6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol __ 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroanilin• 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-05-1-1
Lab Name: CQMPUCH~,J3'.tP Contract: (2-88)-REVS
Lab code: COMPU ca■• No.: 20937 SAS No.: SDG No.: 166
Matrix: (aoil/vatar) WATER Lab Sample ID: 366940
Sample wt/vol: 1000 (g/mL) m._ Lab Fila ID: GH066940A05
Level: (low/med) LOW Date Received: 08/24/90
I Moisture: not dee. dee. Date Extracted: QBl2:ll2Q
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H..,_
$.E.Pl
pH:
Data Analyzed: 08/27/90
Dilution Factor: .1~,o._ __
CAS NO. COMPOUND
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7005-72-3-------4~Chlorophenyl-phanylathar_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (1)_
101-55-3--------4-Bromophenyl-phenylather __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrane
120-12-1--------Anthracena
84-74-2---------Di-n-Butylphthalata
206-44-o--------Fluoranthana
129-00-0--------Pyrane
85-68-7---------Butylbanzylphthalata
91-94-1---------3,3'-Dichlorobanzidina
56-55-3---------Benzo(a)Anthracana
218-01-9--------Chryaana
111-e1-1--------bia(:Z•Ethylhaxyl)Phthalata_
117-84-o--------Di-n-OCtyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthena
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrana
53-70-3---------Dibenzo(a,h)Anthracena
191-24-2-------·Benzo(g,h,i)Parylana
(1) -CaMot be aeparatad from Diphanylamina
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
· 10 u
19
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I SV-2 1/87 Rav.
20937 166 SAMPLE DATA SUMMARY
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name.: CQMPUCHEM, RTP Contract: (2-88)-REVS
Lab Code: CQMPU caae No.1 20937 SAS No,: SDG
Matrix: (■oil/water) WATER Lab Sample ID:
Sample wt/vol: 1000 (g/mL) Ml....... Lab Fila ID:
Level: (low/med) U>W Data Received:
I.Moisture: not dee. dee. Data Extracted:
Extraction: (SepF/Cont/Sonc) s.tU Data Analyzed:
EPA SAMPLE NO.
MW-05-1-1
No.: 16§
366940
GH0§§940Aos
08/24/90
0B/2::i/22
0B/27/90
GPC Cleanup: (Y/N) H.._ pH: Dilution Factor: .1.._.o,._ __
CONCENTRATION UNITS:
Number TICS tound: _I (ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST, CONC. Q -=----===~ ----m•---==••========m=•=-•n:m.::a•••• -=•azi:zz:c=z:::s.••u -===
l. UNlQlOWN 6.50 38 J
2. UNlQlOWN 6.58 54 J
3, UNlQlOWN 6,73 32 J
4. TRIMETHYLBENZENE 6.90 12 J s. UNJ(NOWN 7.95 18 J
6. TETRAMETHYLBENZENE 8.10 22 J
7. UNKNOWN 8.95 50 J
8. UNlQlOWN 20.22 12 J
FORM I SV-TIC 1/87 Rav.
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-05-1-lRE
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS .
Lab Code: COMPU Ca■• No.: 20937 SAS Mo.: SDG No. : ..,1 §...,§.___
Matrix: (■oil/water) WATER Lab Sample ID: .r.l.,.§.,.§9"'4,..o ___ _
Sample wt/vol: 500 (g/mL) m...._ Lab File ID: CR0§§940A05
Level: (low/med) LOW
I Moisture: not dee. dee.
Date Received: 08/24/90
Date Extracted: 0B/29/90
Date Analyzed: 09/01/90
Dilution Factor: AP~,5~0.__
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) L.. pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UC/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,J-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 0
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-0ichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 0
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 0
621-64-7--------N-Nitroso-Di-n-Propylamine_ 10 u
67-72-1---------Hexachloroethan• 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------I ■ophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 0
65-85-0---------Benzoic Acid 50 u
111-91-1--------bi.s (2-Chloroethoxy) Methane_ 10 0
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 0
106-47-8--------4-Chloroaniline 10 0
. 87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2.-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 0
88-06-2---------2,4,6-Trichlorophonol 10 u
95-95-4---------2,4,5-Trichlorophonol 50 u
91-58-7---------2-Chloronaphthalene 10 0
88-74•4•--------2-Nitroaniline !SO 0
131-11-3--------oimethyl Phthalate 10 0
208-96-8--------Acenaphthylene 10 0
606-20-2--------2,6-Dinitrotoluene 10 0
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOL.\TILE ORGANICS ANALYSIS DATA SHEET
KW-0!5-l-lRE
Lab Nllllle: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU -· Case No.: 20937 SAS No.: SDG No.: 166
Matrix: (aoil/vater) WATER Lab Sample ID: 366940
Sample wt/vol: !500 (g/111.L) Ml._ Lab File ID: GR06694oAos
Level: (low/med) LOW Date Received: 08/24/90
, Moi■ture: not dee. dee. Date Extracted: 08/29/90
Extraction: (SepF/Cont/Sonc) llll
GPC Cleanup: (Y/N) H..,_ pH:
Date Analyzed: 09/01/90
Dilution Factor: &o~,s~oL-_
CONCENTRATION UNITS:
. CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline so u
83-32-9---------Aeenaphthene 10. u
!51-28-5---------2,4-Dinitrophenol !50 u
l00-02-7~-------4-Nitrophenol !50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
700!5-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline so u
S34-S2-l--------4,6-Dinitro-2-Methylphenol_ so u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-!SS-3--------4-Bromophenyl-phenylether_ 10 u
118-74-1--------Hexaehlorobenzene 10 u
87-86-5---------Pentachlorophenol !50 u
es-01-e---------Phenanthrone . 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-o--------Fluoranthene 10 u
129-oo-o----~---Pyrene 10 u
8!5-68-7---------Butylbenzylphthalate 10 u
91-94-1---------J,J'-Dichlorobenzidine 20 u
!56-S!S-J---------Benzo(a)Anthracene 10 ·U
21e-01-9--------chryaene 10 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ J J
117-84-0--------Di-n-octyl Phthalate 10 u
20!5-99-2---~----Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
!50-J2-B---------Benzo(a)Pyrene 10 u
193-39-!S--------Indeno(l,2,J-cd)Pyrene 10 u
!SJ-70-J---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -CaMot be aeparated from Diphenylamin•
FORM I sv-2 1/87 Rev.
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM,BIP Contract: 12-88)-REVS
EPA SAMPLE NO.
MW-05-1-lRE
Lab Code: COMPO Case No,: 20937 SAS No.: SOG No.: ..,1...,66....__
Matrix: (■oil/water) WATER Lab Sample ID: 366940
sample wt/vol: 500 (g/mL) m....._ Lab Fil■ ID: GR066940A05
Leval: (low/mad) LOW
I Moisture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H._
Number TICa found: ___J_
dee.
pH:
CAS NUMBER COMPOUND NAME
Oat■ Received: 08/24/90
Data Extracted: 011129190
Date Analyzed: 09/01/90
Dilution Factor: 0.50
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT · EST, CONC, Q·
------------------------------------~--------------------------1, UNIOIOWN 6.60 16 J
2. METHOXYMETHYLETHOXYPROPANOL 6.68 12 J
3, METHOXYMETHYLETHOXYPROPANOL 6,72 8,0 J
4, UNKNOWN 6,83 18 J
5, UNKNOWN 8,07 16 J
6, UNKNOWN 8.22 12 J
7. UNKNOWN 9,09 24 J
8. UNKNOWN 20,57 4,0 J
FORM I SV-TIC 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-16-1-l
Lab Name: coMPUCHEM,RTP I
Lab Code: COMPU Ca11e No.: 20937
. contract: {2-88)-REVS
SAS No.: SDG No.: 1§§
Matrix: (■oil/water) WATER Lab Sample ID: .,.J.,.§.,.§,,_95,o;§,._ __ _
Sample wt/vol: 500 (g/lDL) in._ Lab File ID: GH0§§95§A05
Level: (lov/11ed) LOW Date Received: 08/24/90
, Moisture: not dee. dee. Date Extracted: 08/25/90
Date Analyzed: 08/27/90
Dilution Factor: .,.04.5~0.__
Extraction: (SepF /Cont/Sonc) ilPf
GPC Cleanup: (Y/N) IL_ pH:
CONCENTRATION t.lNITS:
CAS NO. COMPOllND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 0
lll-44-4--------bis(2-Chloroethyl)Ether 10 0
95-57-8---------2-Chlorophenol 10 0
541-73-1--------1,J-Dichlorobenzene 10 0
106-46-7--------1,4-Dichlorobenzene 10 0
100-51-6--------Benzyl Alcohol 10 0
95-SO-l---------l,2•Dichlorobenzene 10 0
95-48-7---------2-Methylphenol 10 0
39638-32-9------bi11(2-Chloroi11opropyl)Ether_ 10 0
106-44-5--------4-Methylphenol 10 0
621-64-7--------N-Nitroso-Di-n-Propylamine_ 10 0
67-72-1---------Hexachloroethane 10 0
98-95-3---------Nitrobenzene 10 0
78-59-1---------Isophorone 10 0
88-75-5---------2-Nitrophenol 10 0
105-67-9--------2,4-Dimethylphenol 10 0
65-85-o---------Benzoic Acid 50 u
111-91-1--------bi11(2-Chloroethoxy)Methane 10 0
120-83-2--------2,4-Dichlorophenol ' -10 u ..
120-a2-1--------1,2,,-Trichlorobenzen• 10 u
91-20-3---------Naphthalene 10 u
106-4 7-8--.------4-Chloroanil in• 10 u
87-68-3-----~---Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 0
88-06-2---------2,4,6-Trichlorophenol 10 0
95-95-4---------2,4,5-Trichlorophenol 50 0
91-58-7---------2-Chloronaphthalene 10 0
88-74-4---------2-Nitroanilin• 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 0
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-16-1-1
Lab Name: CQMPUCHEM,RTP Contract: 12-BB)-IU;YS
Lab Code: CQMPU Caae No.: 20937 SAS No.: __ _ S DG No , : ,.1""6 6,.___
Matrix: (aoil/vater) WATER Lab Sample ID: &3...,6,.,69""5""6.__ __ _
Sample wt/vol: ,oo (g/lllL) m..._ Lab File ID: GHQ66956AQ5
Level: (low/med) LOW Date Received: OB/24/90
, Moisture: not dee. dee. Date Extracted: QB/25/90
Extraction: (SepF /Cont/Sonc)
GPC Cleanup: (Y/N) H..,_ pH:
ilU Date Analyzed: OB/27/90
Dilution Factor: ...,o~,s ... oL,,__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or uq/Kq) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u
51~28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylather_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether_ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-00-0--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidin• 20 u
56-55-3---------Benzo(a)Anthracen• 10 u
218-01-9--------Chryaene 10 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 3 J
111-a,-0--------Di-n-octyl Phthalate · 10 u
205-99-2--------Benzo(b)Fluoranth•n• 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------13enzo(9,h,i)Peryl•n• 10 u
(1) -CaMot be ae~)arated trom Diphenylamin•
FORM I sv-2 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lF
SEMIVOUTILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED. COMPOUNDS
EPA SAMPLE NO.
MW-16-1-1 Lab Name: CQMPUCHEM,RTP Contract: C2-8Bl-REVS -·
Lab Code: COMPO
Matrix: (aoil/vater)
Sample vt/vol:
Level: (lov/111ed)
I Moisture: not dee.
caae No.: 20937
lfATEB
!500 (g/m.L) m..._
LOW
.dee.
Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) H_
au
pH:
SAS No,: SDG No,: ..._16...,6.....___
Lab Sample ID:
Lab File IO:
Date Received:
]66956
GH0§§95§A05
08/24/90
Data Extracted: 08/25/90
Date Analyzed: 08/27/90
Dilution Factor: 0.50
Number TICa found: ---1 CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q -••••-•••==•••a• -•a=-•m••••==~=•====•~•=•s• ----•=z:s• -••==n===-• --1. UNKNOWN 6.52 12 J
FORM I SV-TIC 1/87 Rev.
20937 l 66 SAMPLE ·DATA SUMMARY \ ,..:
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1B EPA.SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW-2R-l
Contract: {2-BB)-BEYS
Lab Code: COMFY Case No.: 20937 SAS No,: SOG No.: _1_66...__
Matrix: (aoil/vatar) WATER Lab Sample ID: al,..6.._7.,._03..._7,__ __ _
sample wt/vol: 1000 (g/mL) JU._ Lab Fila ID: GH067037A05
Level: (low/med) LQW Data Received: 0B/25/90
I Moi11ture: not dee. dee. Data Extracted: 08/27/90
Data Analyzed: 09/01/90
Dilution Factor: .1.._.0,._ __
Extraction: (SepF/Cont/Sonc) llU
GPC Cleanup: (Y/N) lL. pH:
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L o~ ug/Kg) UG/L Q
108-95-2--------Phenol 10 u
111-44-4--------bia(2-Chloroethyl)Ether· 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
3 9638-32-9------bis ( 2-Chloroisopropyl ).Ether_ 10 u
106-44-5-------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
111-91-1--------bi11(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-12-1--------1,2,,-Trichlorobenzene 10 u
91-20-3---------Naphthalena 10 0
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2~Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 0 •
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalana 10 0
88-74-4---------2-Nitroanilin• 50 u
· 131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acan~phthylena_ -10 u
606-20-2--------2,6-Dinitrotolurna -10 u
FORM I sv-1 1/87 Rav.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
HW-2R-l
Lab Name: CQMPUCHEM,RTP Contract: (2-881-REVS
Lab Code: CQMPU Ca ■• No.: 20937 SAS No.: SDG No.: 16§
Matrix: (■oil/water) WATER Lab Sample ID: 3§7037
Sample vt/vol1 1000 (g/mL) m.__ Lab File ID: GH067037A05
Level: (lov/med) LOW Date Received: oe125190
I Moiature: not dee. dee. Date Extracted: oe12z190
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H,_
llPl
pH:
Date Analyzed: 09/01/90
Dilution Factor: £1L-~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2--~------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthenu 10 u ..
129~00-0--------Pyren• 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,J'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
111-a1-1--------bi■(2-Ethylhexyl)Phthalate_ 10 u
111-a,-o--------Di-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluorantheno 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-a---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Peryleno 10 u
-· (1) -Cannot be separated from Diphenylamin•
FORM I sv-2 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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H SEMIVOLATILE ORGANICS ANALYSIS ·oATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
MW•2R·l Lat> Name: CQMPUCKEH,BIP contract: 12•88l•REVS
lab Code: COMPU -· Case No.: 2S)937 SAS No.: S DG No • : .,,l ""6 6,.___ Matrix: (soil/water) WATER
Sample vt/voli 1000 (9/lllL) tu.__
Level: (low/med) LOW
I Moiatura: not dee. dee.
Extraction: (SepF/Cont/Sonc) UU
GPC Cleanup: (Y/N) ti_ pH:
Nw.iber TIC• found: --1
CAS NUMBER COMPOUND NAME
Lab Sample ID: _3_6.._70-3._7.__ __ _
Lab File ID: GHQ67037AQ5 ·
Date Received: 08/25/90
Date Extracted: 08/27/90
Date Analyzed: 09/01/90
Dilution Factor: _1 __ ,o __ _
CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L
RT EST. CONC. Q -·------------------------------=-------~ ------------=-------l. UN](NOWN 20.20 2.0 3
FORM I SV·TIC l/87 Rev.
28937 166 SAMPLE DATA SUMMARY
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CQMPUCHt:', B1.:P · Contract: 12-88}-REVS
Lab Code: CQMPU caae No.: 20937 SAS No.: SDG
EPA SAMPLE NO.
MW06-l-1
No.: 1§§ I Matrix: (■oil/water) WATER Lab Sample ID: 3§7027
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Sample wt/vol: 1000 (g/lllL) ~ Lab File ID: !iH0§70271lQ:i
Level: (low/med) LOW Date Received: 08/25/90
I Moieture: not dee. dee. Date Extracted: 08/27(20
Extraction: (SepF/Cont/Sonc) llU Date Analyzed: 08/27/90
GPC Cleanup: (Y/N) ll,_ pH: Dilution Factor: .i~,o,._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!;i/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bi■(2-Chloroethyl)Ether 10 u ' 95-57-8----~----2-Chlorophenol 10 u·
541-73-1--------1,J-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bia(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroeo-Di-n-Propylamine_ 10 u
67-72-1---------Kexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-0---------Benzoic Acid 50 u
111-91-1--------bie(:Z-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,4-Trichlorobenzene 10 u
· 91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiane __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Di■ethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW06-l-l
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REYS
Lab Code : CQMPU Ca■• No.: 20937 SAS No.: SDG No.: _1_66 __
Matrix: (■oil/water) WATER Lab S amp l • IO: .,.3.,.(i.,_7.,.0._2 7..__ __ _
Sample vt/vol: 1000 (g/mL) m,_ Lab File IO: GH067027B05
Level: (low/med) LQW Date Received: OB/25/90
I Moi ■ture: not dee. dee.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) H,_ pH:
Date Extracted: OB/27/90
Date Analyzed: 08/27/90
Dilution Factor: .1~,o,._ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2 4-Dinitrotoluene . , 10 u
84-6.6-2---.. -----oiethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
as-01-a---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-o--------Fluoranthene 10 u
129-00-0--------Pyrene 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1----~----3,l'-Dichlorobenzidin• 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chry■ene · 10 u
ll7-8l-7--------bi■(2-Ethylhexyl)Phthalate_ 10 u
111-14-0--------01-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9------~~Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 ·u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -Cannot be ■eparated from Diphenylamin•
FORM I sv-2 1/87 Rev.
20937 166 SAMPLE~DATA SUMMARY ; ~
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,R;P Contract: (2-88)-REYS MW06-l-l
Lab Code: COMPO Ca•• No.: 20937
Matrix: (aoil/vater) WATER
SAS No.: S 0G No • : .,16,..,6.____
Lab Sample ID: .,.3.,.6.,_7..,0..,27,..__,;___
sample wt/vol: 1000 (c;/mL) m._ Lab File ID: GH067027B05
Level: (low/med) LOW
, Moisture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lf_
Wlllllber 'TIC• round: __.l!,
dee.
pH:
CAS NUMBER COMPOUND
au
NAME
Date Received: 08/25/90
Date Extracted: 08/27/90
Date Analyzed: 08/27/90
Dilution Factor: .1L,o,._ __
CONCENTRATION UNITS:
(uc;/L or uc;/Kc;) UG/L
RT EST. CONC. Q
-------------------------------------------------------------ZI=
FORM I SV-TIC 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW08-l-l
Lab Name: CQMPUCHEM,RTP Contract: 12-881-REVS .·
Lab Cod•: COMPO Ca•• No,: 20937 SAS No,: SDG No.: 166
Matrix: (•oil/water) WATER Lab Sample ID: 367029
Sample wt/vol: 1000 (g/mL) Ill<.._ Lab File ID: GH067029B05
Level: (low/med) LOW Date Received: 08/25/90
I Moisture: not dee, dee. Date Extracted: 011121190
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li,_ pH:
ilPl Date Analyzed: 0S/28/90
Dilution Factor: .1~1 0,._ __
CAS NO, COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Banzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(Z-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Banzoic Acid
lll-91-l--------bi•(2-Chloroethoxy)Methane_
· 120-83-2--------2,4-Dichlorophenol
120-a2-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroanilin•
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene __
606-20-2--------2,6-Dinitrotol~~ne
Q
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
!50 u
10 u
10 u
10 0
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MWoa-1-1
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REYS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 166
Matrix: (■oil/water) WATER Lab Sample ID: 3§7029
Sample wt/vol: 1000 (g/llL) m._ Lab File ID: GH067029B0S
Level: (low/med) LOW Date Received: 08/25/90
I Moisture: not dee. dee. Date Extracted: 08/27/90
Extraction:
GPC Cleanup:
( SepF / Cont/ Sonc)
(Y/N) J:L_
llU
pH:
Date Analyzed: 08/28/90
Dilution Factor: .1~,~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorane
100-01-6--------4-Nitroanilina
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitroaodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobanzene
87-86-5----~----Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------D1-n-Butylphthalate
206-44-o--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidina
56-55-3---------Benzo(a)Anthracane
218-01-9--------Chry■ene
111-a1-1--------bia(2-Ethylhexyl)Phthalata_
111-14-0--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-J---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -cannot be separated from Diphenylamine
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 , 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
..
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: C2-BBl-REVS •·
MW08-l-l
Lab Code: COMPO caae No.: 20937 SAS No.: SDG No.: -l-66L--_
Matrix: (aoil/vater) WATER Lab Sample IO: 367029
Sample vt/vol: 1000 (g/mL) tll._ Lab File IO: GH067029B05
Level: (lov/med) LOW
I Moiature: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL_
Number TIC• found:~
dee.
pH:
CAS NUMBER COMPOUND
llPl
NAME
Date Received: 08/25/90
Date Extracted: 08/27/90
Date Analyzed: 08/28/90
Dilution Factor: _1_.o __ _
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
--••---•-•a• m-:a===••••••ma=s•m•=•-• ---==•a::i -••:a•a••-•• •===
FORM I SV-TIC 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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SEMIVOU.TILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MWll•l-1
Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REYS
Lab Code : CQMPU Ca■e No.: 20937 SAS No.: S 0G NO • : .,16,..6...__
Matrix: (■oil/water)
Sample wt/vol:
Level: (low/med)
WATER
500
LOW
(g/mL) ~
Lab Sample IO: 366954
Lab File IO: GHQ66954A0S
Date Received: 08/24/90
t Moi ■ture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL..
dee.
pH:
Data Extracted: 08/25/90
Data Analyzed: 08/27/90
Dilution Factor: 0.50
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
l00-51•6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48•7---------2-Methylphenol
39638-32-9------bia(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroao-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimathylphenol
65-85-o---------Banzoic Acid
lll-91-l--------bi■(2-Chloroethoxy)Methane
120-83-2--------2,4-0ic:hlorophenol -
120-s2-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalen•
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiane_
ss-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7-------··-2-Chloronaphthalane
88-74-4---------2-Nitroanilin•
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3 J
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u.
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
)
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Q
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g
lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MWll-1-1
Lab Nam•: CQMPUCHEM, RTP contract: {2-88)-REVS . . .
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: _16-6...__
Matrix: (soil/water) WATER Lab Sample ID: .,.3.,.6.,.69.._5""4:a...... __ _
Sample vt/vol: 500 (g/m.L) ~ Lab Pile ID: GH066954A05
Level: (lov/med) LOW
I Moisture: not dee. dee.
Date Received: OB/24/90
Date Extracted: 08/25/90
Date Analyzed: 08/27/90
Dilution Factor: ~OL,5~0.__
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H......
llU
pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9------·--oibenzoturan
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3---~---4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1---~----4,6-Dinitro-2-Hethylphenol_
86-30-6---------N-Nitrosodiphenylamine (1)_
101-55-3---~----4-Bromophenyl-phenylether_
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-e---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Pluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,J'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
111-a,-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,b,i)Perylene
(1) -cannot be separated trom Diphenylamine
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
14
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM, RTP Contract: (2-BB)-REYS
EPA SAMPLE NO.
KWlJ-1-1
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: ..,l~66il,..__
Matrix: (soil/water) WATER
Sample wt/vol: !00 (g/mL) ~
Level: (low/med) LOW
I Moisture: not dee.
Extraction:
GPC Cleanup:
(SepP/Cont/Sonc)
(Y/N) H_
Number TICS tound: ~
dee.
pH:
CAS NUMBER COMPOUND
ilU
NAME
Lab Sample ID:
Lab Pile ID:
· Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
366954
GHQ66954AQ5
08/24/90
08/25/90
08/27/90
o,so
CONC. Q _ .. _________
---=------==========--------•=z•=-=•---=---=-=------== 1. UNKNOWN 6.50 18 J 2. UNKNOWN 7.95 8.0 J 3. UNKNOWN 8.10 10 J
4. UNKNOWN 8,95 30 J 5. UNKNOWN 9.97 32 J
FORM I SV-TIC 1/87 Rev.
20937 166.SAMPLE DATA SUMMARY
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1B
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPU:·No.
Lab Name: CQMPUCHEM,RTP Contract: (2-88)-REVS MWlJ-1-lMS
Lab Code: CQMPU Case No.: 20937 SAS No.: SOG No.: 166
Matrix: (■oil/vater) WATER Lab Sample IO: .,.J...,6...,69,..;4:,.,l.._ __ _
Sample vt/vol: 500
LOW
(g/mL) Ml,._ Lab File IO: GH066941A05
Level: (lov/med) Date Received: 08/24/90
I Moisture: not dee. dee. Date Extracted: 08/25/90
Date Analyzed: 08/27/90
Dilution Factor: o,so
Extract.ion: (SepP'/Cont/Sonc) nu
GPC Cleanup: (Y/N) H..,_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u lll-44-4--------bie(2-Chloroethyl)Ether 10 u 95-57-8---------2-Chlorophenol 10 u 541-73-1--------1,3-0ichlorobenzene 10 u 106-46-7--------1,4-0ichlorobenzena 10 u 100-51-6--------Benzyl Alcohol 10 u 95-50-1---------1,2-0ichlorobenzene 10 u 95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u 106-44-5--------4-Methylphenol 10 u 621-64-7----~---N-Nitro■o-Oi-n-Propylawine_ 10 u 67-72-1---------Hexachloroethane 10 u 98-95-3---------Nitrobenzane 10 u
78-59-1-~-------I ■ophorone 10 u
88-75-5---------2-Nitrophenol 5 J
105-67-9--------2,,-oimethylphenol 10 u 65-85-0---------Benzoic Acid 50 u
111-91-1--------bia(l-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-0ichlorophenol 10 u
120-a2-1--------1,2,,-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 u
88-06-2--~------2,,,6~Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------oimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW13-l-1MS
Lab Name: CQMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: CQMPU •· Ciae No.: 20937 SAS No.: SOG No.: ·166
Matrix: (■oil/water) WATER Lab sample IO: 366941
Sample vt/vol1 !00 Lab File IO: GH0§6941Aos
t,evel: (lov/med) LOW Date Received: 08/24/90
I Moisture: not dee. dee. Date Extracted: 08/25/90
Extracti'on:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) JL_ pH:
Date Analyzed: 08/27/90
Dilution Factor: &OL.s~o.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or u9/K9) UG(L Q
99-09-2---------3-Nitroaniline 50 u 83-32-9---------Acenaphthene 10 u 51-28-5---------2,4-0initrophenol 50 u
100-02-1--------4-Nitrophenol 50 u 132-64-9--------0ibenzoturan 10 u 121-14-2--------2,4-0initrotoluene 10 u
84-66-2---------Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u 86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitroaodiphenylamine (1)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10. u
84-74-2---------oi-n-Butylphthalate 10 u
206-44-o--------Fluoranthene 10 u
129-00-0--------Pyrena 10 u
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-0ichlorobenzidine 20 u
56-55-3---------Benzo(alAnthracene 10 u
218-01-9--------Chryaena 10 u
117-81-7--------bia(Z-Ethylhexyl)Phthalate_ 7 J
117-84-o--------oi-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Pluoranthene 10 u
50-32-a---------Benzo(a)Pyrene -10 u
193-39-5--------Indeno(l,2,3-cd)Pyrena 10 u
53-70-3---------Dibanzo(a,h)Anthracene 10 u
191-24-2-~------Benzo(9,b,i)Perylene -10 tJ
-(1) -Cannot be separated trom Dipbenylamine
FORM I sv-2 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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18
SEKIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MWl3-l-lMSD
Lab Name: CQMPUCHEK,RTP contract: {2-BB)-REYS .
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No. : 416,,..,6.___
Matrix: <•oil/water) WATER Lab Sample ID: ... J,..6.,..69,._4""2.__ __ _
Sample wt/vol: 500 (g/mL) HL.. Lab File ID: GH06§942A05
Level: (lov/111ed) LOW
I Moisture: not dee. dee.
Date Received: 08/24/90
Date Extracted: 08/25/90
Oat• Analyzed: 08/27/90
Dilution Factor: ... o~,~50,.__
Extraction: (SepF /Cont/Sonc)
GPC Cleanup: (Y/N) H..,__ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
lOB-95-2-'.-------Phenol 10 u lll-44-4--------bia(2-Chloroethyl)Ether 10 u 95-57-8---------2-Chlorophenol 10 u 541-73-1--------l,3-Dichlorobenzene 10 u
106-46-7--------l,4-Dichlorobenzene 10 u 100-51-6--------Benzyl Alcohol 10 u
95-50-1---------l,2-Dichlorobenzene 10 u 95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u 106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-D1-n-Propylamine_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Iaophoron• 10 u
88-75-5---------2-Nitrophenol 4 J
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u ..
120-a2-1-----~--1,2,4-Trichlorobenzene 10 u
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthaleno 10 u
77-47-4:..-----~--Hexachlorocyclopentadiene_ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95:..4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroanilin• 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthyl•n• • 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv~1 1/87 Rev.
20937 166 SAMPLE DATA SUMMARY
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SEMIVOU.TILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Hue: CQMPUCJJEM,RTP Contract: (2-88)-RE;YS MWll-1-lMSD
.·
Lab Code: CQMPU caae No.: 20937
Matrix: (aoil/vater) WATER
SAS No.: SDG No.: ...,16,._,6.___
Lab Sample ID: .J.,.6.,.6z.94s.2"-----
Sample vt/vol1 !500 (g/aL) m._ Lab File ID: GH066942AQ5
Laval: (low/mad) LQW
I Moisture: not dee. dee.
Data Received: 08/24/90
Date Extracted: 08/25/90
Data Analyzed: 08/27/90
Dilution Factor: 0.50
Extraction: (SepPiCo_nt/Sone) llU
GPC Cleanup: (Y/N) ll.,_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u 83-32-9---------Aeanaphthana 10 u 51-28-5---------2,4-Dinitrophanol 50 u 100-02-1--------4-Nitrophanol 50 u 132-64-9--------0ibenzoturan 10 u 121-14-2--------2,4-Dinitrotoluene • 10 u 84-6~-2-----~---Diethylphthalate 10 u 7005-72-3-------4-Chlorophenyl-phenylether_ 10 u 86-73-7---------Fluorene 10 u 100-01-6--------4-Nitroaniline 50 u 534-52-1---~----4,6-Dinitro-2-Methylphenol_ 50 u 8_6-30-6---------N-Ni troaodiphenylamin• ( l) _ 10 u 101-55-3---~----4-Bromophenyl-phenylether __ 10 u 118-74-1--------Haxaehlorobanzana 10 u 87-86-5---------Pantaehlorophenol 50 u 85-01-e---------Phenanthrene 10 u
120-12-7--------Anthraeene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-oo-o--------Pyr•n• 10 u
85-68-7---------Butylbenzylphthalat• 10 u
91-94-1-----~---3,3'-0ichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthrac•n• 10 u
211-01-9--------Chryaene 10 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 13 111-a,-o--------oi-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Pluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthena 10 u
50-32-a---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------0ibenzo(a,h)Anthracene 10 u
·191-2,-2--------Benzo(g,h,i)Perylene 10 u
(l) -CaMot be separated from Oiphenyluine
FORM I sv-2 l/87 Rev.
20937 166 SpMPLE ~ATA SUMMARY
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COMPUCHEM
lABOMTORIES
CASE NARRATIVE--CASES 20937
Contracts 2-88 <REVS) SOGS 215
Co~puChe~ Laboratories, Inc.
Sa~le Nu~bera: LABPURE, MW14R01 I, MW15011, MW15012, MW2A-01-1,
MW7-01-I, MW8A-01-I, MW9-01-I
Case# 20937 consisted of 7 water saMples for volatile and oeMivolatile
analysis and I water saMple for volatile only analyois. The saMp[es
were received intact on 8-30-90 and 8-31-90 in properly sealed shipping
container• with chain-of-custody docuMenta. Hyphens were reMoved as
needed froM soMe saMple identifiers due to the nine digit liMil.
VOLATILES:
All volatile fractions were analyzed within holding, tiMe requireMents.
TCL coMpounds were present in all saMples, ooMe at high levels. Four
seMpleo contained tentatively i~nlified coMpounds, two of which were
attributable to a laboratory artifact. A qualifier was included with
these two saMples. The laboratory artifacts were aloo preoent in the
asoociated Method blanks. SaMples MW15011 and MWl5012 each required
dilutions due to the high levela of 1 ,1-dichloroethene and
1 ,1 ,I-trichloroethane. Two analyses of saMple MW9-01-1 were reported.
In the initiel 5 Ml analysis, the level of vinyl chloride excaeded the
Multipoint range. The saMple was reanalyzed using only I Ml and both
analyses were reported due lo the loss of soMe ~oMpounds in the
dilution. All surrogate recovery criteria were Met. The QC Matrix
spike/Matrix spike duplicate results were acceptable.
SEMIVDLATILES:
All seMivolatile fractions were extracted and analyzed within holding
tiMe requireMents. One saMple, MW9-01-I, contained two TCL coMpounds.
None of the other saMples contained any TCL coMpounds. Four saMples
contained tentatively identified coMpounds. The 2-fluorobiphenyl
surrogate recoveries in saMples MWl4R011, MW7-01-I, and MW2A-01-IMSD
fell below QC liMits. All other surrogate recovery criteria were Met.
The QC Matrix spike/Matrix spike duplicate results were acceptable.
The acenaphthene recovery fell·below QC liMits in the MSD.
I certify that this data package is in coMpliance with the terMs and
conditions of the contract, both technically and for coMpleteness, for
other than the conditions detailed above. Release of the data
contained in this hardcopy data package has been authorized by the
Laboratory Manager or his designee, aa verified by the following
signat~re.
Note: This report was paginated for reference and accountability in
decreasing nuMerical sequence.
net G. Livingsto
Sr. Quality Assurance Specialist
COMPUCHEM LABORATORIES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Resea~ch Triangle Park, NC 27709 {919) 549·8263
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP Contract: {2-BBl-REVS LABPURE
Lab Code: COMPO ca■e Ho.: 20937 SAS No.: SOG No.: 215
Matrix: (eoil/water) WATER Lab Sample ID: 3§7§54
Sample wt/vol: 5.0 (g/mL) tllL_ Lab File IO: CH0§7654Cl8
Level: (low/med) LOW Date Receive4i. 08/30/90
I Moisture: not dee. Date Analyzed: 09/06/90
Column: (pack/cap) ~E Dilution Factor: ~i~·~o'---
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L . Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 9 B 67-64-1---------Acetone 10 u 75-15-o---------carbon Disulfide 5 u 75-35-4---------1,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 5 u
540-59-o--------l,2-Dichloroethene (total)_ 5 u 67-66-3-----~---Chloro!orm 5 u 101-06-2--------1,2-oichloroethane 5 u
78-93-3---------2-Butanone 10 u 71-55-6-~-------l,l,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-5------cis-l,3-Dichloropropene 5 u 79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u -79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene_ 5 u
75-25-2---------Bromotorm 5 u 1oe-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6-~------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
1oe-ee-J--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-,2-s--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
,., ... ,., IMM _ lJ
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lE EPA.SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: l2-88l-REVS LABPURE
Lab Code: CQMPU case No.: 20937 SAS No.: SOG No.: .._2..,15,.___
Matrix: (■oil/water) WATER
Sample wt/vol: 5.0
IAvel: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICa found: _..Q
.CAS NUMBER
(9/mL) ~
COMPOUND NAME
Lab Sample ID: ,.3..,6.,_7.,..6_.54:a_ __ _
Lab Fil• ID: CN0§7§54C18
Date Received: 08/30/90
Date Analyzed: 09/0§/90
Dilution Factor: ~i~,.,..o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST, CONC. Q
----------------•••••••=-•••====a•••=••••••• ---------••a::a••-•:a•• ---
FORM I VOA-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MWl4ROll
Lab Name: CQMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: CQMPU Ca•• No.: 20937 SAS No.: SDG No.: 215
Matrix: (aoil/vatar) WATER Lab Sample ID: 3§7§45
Sample wt/vol: :s' 0 (g/mL) Hl,_ Lab File ID: C2R§7§4 5A18
Level: (low/med) LOW Date Receiva4:-08/30/90
, Moisture: not dee. Date Analyzed: 09/06/90
Column: (pack/cap) ~2 Dilution Factor: .i~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 t1
74-83-9---------Bromomethane 10 u
75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane -10 t1
75-09-2---------Methylene Chloride 3 BJ 67-64-1---------Acetone 10 u
75-15-o---------carbon Disulfide 5 u
7 5-3 5.-4---------l, 1-Dichloroethene 4 J
75-34-3---------1,l-Dichloroethane 6
540-59-0--------1,2-Dichloroethene (total)_ 6
67-66-3---------Chlorot:orm 5 u
107-06-2----·----l, 2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 7
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cia-1,3-Dichloropropene 5 u
79-01-6---------Trichloroethene. 6
124-48-1--------Dibromochloromethane 5 u -
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2-----~---Benzene 5 u
10061-02-6------Trana-1,3-Dichloropropene __ 5 u
75-25-2---------Bromotorm 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 t1
127-18-4--------Tetrachloroethene 3 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluen• 5 u
1os-90-1--------chlorobenzene 5 u
100-41-4--------Ethylbenzane 5 u
100-42-s--------styrene 5 u
1330-20-1-------Total Xylanea 5 u
FORM I VOA 1/87 Rev.
209 215\ S MP ! D A SU MARY·
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lE EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIWLY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM, RTP
Lab Code: COMPO Case No.: 20937
Matrix: <•oil/water) WATER
Sample wt/vol: 5,0 (g/mL)
Level: (low/med) I.OW
I Moisture: not dee.
Column (pack/cap) !;AP
Number TICs found: __o
CAS NUMBER COMPOUND
MW14R011
Contract: 12-88)-REVS
m..,_
NAME
SAS No.: __ _ S DG No , : a.2 ..,_15"'---
Lab Sample ID: ..,_3.,._67,._6,.;4,_5.__ __ _
Lab File ID: C2R67645A1B
Date Received:-08/30/90
Date Analyzed: 09/06/90
Dilution Factor: .1.._,,._o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
·-------=------••••••c•••••a••-=•==••••••-------------------------
FORM I VOA-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lA EPA SAMPLE NO.
VOLATILE: ORGANICS ANALYSIS DATA SHEET
MW15011
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REVS
Lab Code: COMPV ca■e.No.: 20937 SAS No,: SDG No.: a2,.1,,,_5 __
Matrix: (■oil/water) WATER Lab Sample ID: .,.3.,.§.1..Z.11.§.i.50.,_ __ _
sample vt/vol: 1,0 (g/mL) Ill.,_ Lab File ID: C3R§7§50A1B
Level: (low/med) LOW
I Moisture: not dee.
Date Received:-. 08/30/90
Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .i~,~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 50 u
74-83-9---------Bromomethane 50 u
75-01-4-~-------Vinyl Chloride 50 u
75-00-3---------Chloroethane 50 u
75-09-2---------Methylene Chloride 9 BJ
67-64-1---------Acetone 34 BJ
75-15-o---------carbon Disulfide 25 u
75-35-4---------1,1-Dichloroethene 640
75-34-3---------1,1-Dichloroethane 26
540-59-o--------l,2-Dichloroethene (total)_ 25 u
67-66-3---------Chloroform 25 u
107-06-2--------1,2-Dichloroethane 25 u
78-93-3---------2-Butanone 50 u
71-55-6---------1,1,1-Trichloroethane 500
56-23-5---------carbon Tetrachloride 25 u
108-05-4--------Vinyl Acetate 50 u
75-27-4---------Bromodichloromethane 25 u
78-87-5---------1,2-Dichloropropane 25 u
10061-01-5------cis-1,3-Dichloropropene 25 u
79-01-6---------Trichloroethene 25 u
124•48-1--------Dibromochloromethane 25 u -
79-00-5---------1,1,2-Trichloroethane 25 u
71-43-2---------Benzene 25 u
10061-02-6------Trans-1,3-Dichloropropene_ 25 u
75-25-2---------Bromotorm 25 u
1oa-10-1--------4-Methyl-2-Pentanone 50 u
591-78-6--------2-Hexanone 50 u
127-18-4--------Tetrachloroethene 25 u
79-34-5-----~---1 1 2 2-Tetrachloroethane I I I --25 u
108-88-3--------Toluene 25 u
108-90-7--------Chlorobenzene 25 u
100-41-4--------Ethylbenzene 25 u
100-42-5--------styrene 25 u
1330-20-7-------Total Xylene■ 25 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
MW15011
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPQ Ca■• No.: 20937 SAS No.: ___ SOG No.: ..,2._15.___
Matrix: (■oil/water) WATER
Sample wt/vol: 1.0 (9/IIIL} KL_.
Level: (low/med) LOW
I Moi■ture: not dee.
Column (pack/cap) CAP
Number TICs found: _1
CAS NUMBER COMPOUND NAME
Lab Sample IO: .,.3.,.§.,_7.,._6,._50"----
Lab File ID: C3R§7§50A1B
Date Receivedr. 08/30/90
Date Analyzed: 09/0§/90
Dilution Factor: .i~,o"---
CONCENTRATION UNITS:
(u9/L or u9/K9) UG/L
RT EST. CONC. Q
------------------~---=-----------=---------------------------D 1. LABORATORY ARTIFACT 0.88 35 BJ
FORM I VOA-TIC 1/87 Rev.
I'\ T l"l I IMM lJ
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW15012
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: S00 No.: ._2._15..__
Matrix: (soil/water) WATER Lab Sample ID: 367653
sample wt/vol: 0.70 (g/mL) Ml...:.. Lab File ID: CR067653B1B
Level: (low/med) LOW Date Received: 08/30/90
t Moisture: not dee. Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .1~1~0~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 71 u
74-83-9---------Bromomethane 71 u
75-01-4---------vinyl Chloride 71 u
75-00-3---------Chloroethane 71 u
75-09-2---------Methylene Chloride 12 BJ
67-64-1---------Acetone 36 J
75-15-o---------carbon Disulfide 36 u
75-35-4---------1,1-Dichloroethene 950
75-34-3---------1,1-Dichloroethane 33 J
540-59-0--------1,2-Dichloroethene (total)_ 36 u
67-66-3---------Chloroform 36 u
107-06-2--------1,2-Dichloroethane 36 u
78-93-3---------2-Butanone 71 u
71-55-6---------1,1,1-Trichloroethane 790
56-23-5---------Carbon Tetrachloride 36 u
108-05-4--------Vinyl Acetate 71 u
75-27-4---------Bromodichloromethane 36 u
78-87-5---------1,2-Dichloropropane 36 u.
10061-0l-5------ci11-l,3-Dichloropropene 36 u
79-01-6---------Trichloroethene '36 u -
124-48-1--------Dibromochloromethane 36 u
79-00-5---------1,1,2-Trichloroethane 36 u
71-43-2---------Benzene . 36 u
10061-02-6------Trans-l,3-Dichloropropene __ 36 .U
75-25-2---------Bromoform 36 u
1oe-10-1--------4-Methyl-2-Pentanone 71 u
591-78-6--------2-Hexanone 71 u
127-18-4--------Tetrachloroethene 36 u
79-34-5---------1,1,2,2-Tetrachloroethane __ · 36 u
108-88-3~-------Toluene 36 u
108-90-7--------Chlorobenzene 36 u
l00-4t-4--------Ethylbenzene 36 u
100-42-5--------styrene 36 u
1330-20-7-------Total Xylenes 36 u
FORM I VOA 1/87 Rev.
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
EPA SAMPLE NO.
MW15012
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .._2...,15.____
Matrix: ( soil/water) WATER
Sample wt/vol: 0.70 (g/mL) ML..
Level: (low/med) LOW
\ Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: ___.l
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
367653
CR067653B18
08/30/90
09/06/90
1.00
CONC. Q
--------------------=======•--==•=-•===-----------------•=z::11•------•-=:::z
1. LABORATORY ARTIFACT 0.90 36 BJ
FORM I VOA-TIC 1/87 Rev.
20937 215\SAMPLE DATA SUMMARY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM,RTP contract: 12-88)-REVS MW2A-Ol-l
Lab Code: CQMPU case No.: 20937 SAS No.: SDG No.: 215
Matrix: (■oil/vater) WATER Lab Sample ID: 367644
Sample vt/vol: 5,0 (g/mL) m._ Lab File ID: CR067644Cl8
Level: (lov/med) LOW Date Received:-08/30/90
I Moisture: not dee. Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .i~,~0c_ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone 10 u 75-15-o-~-------carbon Disulfide 5 u 75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 1 J
540-59-0--------1,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 5 u 107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 2 J 56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-0ichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 16 124-48-1--------Dibromochloromethane 5 u -
79-00-5---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Tran■-1,3-Dichloropropene __ 5 u
75-25-2---------Bromotorm 5 u
1oa-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tatrachloroethene 5 0
79-34-5---------1,1,2,2-Tetrachloroethane_ 5 0
1oa-aa-J--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 0
100-42-5--------styrane 5 0
1330-20-1-------Total Xylenas 5 0
-
FORM I VOA 1/87 Rev.
?tl9. 7 ? _ C: M I r: T
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lE EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW2A-Ol-l
Lab Name: CQMPUCHEM,RTP Contract: l2-BB)-REYS
Lab Code: CQMPU ' caae No.: 20937 SAS No.: ---SOG No.: ._2.,.15....__
Matrix: (■oil/water) WATER Lab Sample ID: .J_§~Z-§4~4 ___ _
Sample wt/vol: 5.0 (g/mL) Hl,__ Lab File ID: CR0§7644Cl8
Level: (low/med) LOW
I Moiature: not dee.
CollllDn (pack/cap) CAP
Nwnber TICS tound: --1
CAS NUMBER COMPOUND NAME
Date Received~ 0B/30/90
Date Analyzed: 09/06/90
Dilution Factor: _1~,o __ _
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/L
RT EST. CONC. Q
-•-•=•••aa:a•• --=•=======-============-=------~=-------------------=--1. 76-13-1 ETHANE,l,l,2-TRICHLOR0-1,2,2 2.oa 14 J
FORM I VOA-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMM~BY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP Contract: £2-881-REVS MW7-0l-l
Lab Code: COMPO Caae No.: 20937 SAS No.: ----SDG No.: 215
Matrix: (■oil/water) WATER Lab Sample ID: .J,..6.._7..,64;:1..3,.__ __ _
Sampla vt/vol: 5.0 (g/mL) KL_ Lab File ID: CR0§764JC18
Level: (lov/med) LOW
I Moisture: not dee.
Date Received:-08/30/90
Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .i~, ... o __ _
CAS NO. COMPOUND
74-87-3---------Chloromethane
74-83-9---------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene
67-66-3---------Chlorotorm
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
(total)_
71-!55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4-------~-Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-01-s------cis-1,J-Dichloropropene
79-01-6---------Trichloroethana
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Banzena
10061-02-6------Trans-1,3-Dichloropropena __
75-25-2---------Bromotorm
1oe-10-1--~-----4-Methyl-2-Pentanone
591-78-6--------2-Hexanona
127-18-4--~-----Tetrachloroethena
79-34-!S---------l,1,2,2-Tetrachloroethane_
1oe-ee-J--------Toluena
108-90-7--------chlorobanzene
100-41-4--------Ethylbenzene
100-42-5--------styrane
1330-20-7-------Total Xylene■
10 u
10 u
10 u
10 u
9 B
10 u
!S u
!S u
5 u
5 u
5 u
!5 u
10 u
5 u
5 u
10 u
!S u
!S u
!S u
!S u
!S u
!S u
!S u
!S u
!S u
10 u
10 u
!S u
!S u
!S u
!S u
!S u
!S u
!S u
FORM I VOA 1/87 Rav.
20937 5 MP DAT RY
Q
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lE
VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: 12-881-REVS
EPA SAMPLE NO.
MW7-0l-l
Lab Code: COMPO Caae No.: 20937 SAS No.: SDG No.: 215
Matrix: (■oil/water) WATER
Sample wt/vol: !LO (g/lllL) Ill...._
Level: (low/med) LOW
I Moi11ture: not dee.
Column (pack/cap) ,a.E
Number TICa found:~
CAS NUMBER COMPOUND NAME
Lab Sample ID:
Lab File IO:
Date Receivedr
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/L
RT EST.
367643
CR067643C18
08/30/90
09/06/90
1.0
CONC. Q
-------------••••••-•===••=••=====•a•-• ••a•-:a• ---------------
FORM I VOA-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MWSA-01-1
Lab Name: coMPUCHEM, RTP Contract: 12-881-REVS
Lab Code: COMPO Caae No.: 20937 SAS No.: SDG No.: 215
Matrix: (■oil/water) WATER Lab Sample ID: 3§7830
Sample wt/vol: 5,0 (g/mL) m..._ Lab File ID: CN0§7830B18
Level: (low/med) LOW Date Receive:" 08/31/90
I Moisture: not dee. Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .1~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------chloromethane
74-83-9---------Bromomethane
75-01-4---------vinyl Chloride
75-00-3---------Chloroethane
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-o--------l,2-Dichloroethene (total)_
67-66-3---------chlorotorm
107-06-2---~----1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5---------1,2-Dichloropropane
10061-0l-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-oo-s---------1,1,2-Trichloroethan•
71-43-2---------Benzene
10061-02-6------Tran■-1,J-Dichloropropene __
75-25-2---------Bromotorm
1oa-10-1--------4-Methyl-2-Pentanon•
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane_
108-88-3--------Toluene
108-90-7--------Chlorobenzene
100-41-4--------Ethylbenzene
100-42-5--------styren•
1330-20-7-------Total Xylenes
Q
10 u
10 u
10 u
10 u
5 B
4 J
5 u
6
23
9
5 u
3 J
10 u
4 J
5 u
10 u
5 u
5 u
5 u
10
5 u
5 u
5 u
5 u
5 u
10 u
10 u
4 J
5 u
5 u
5 u
5 u
5 u
5 u
FORM I VOA 1/87 Rev.
'2 9 A S MARY
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lE EPA· SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPQCHEM,RTP
Lab Code: CQMPU Ca■e No.: 20937
Matrix: (■oil/water) WATER
Sample wt/vol: 5.0 (g/m.L)
Level: (low/med) LOW
I Moisture: not dee.
ColWlln (pack/cap) CAP
NWDber TICs tound: _j2
CAS NUMBER COMPOUND
MWBA-01-1
Contract: (2-88)-REVS
lil...._
NAME
SAS No.: SOG No.: 215
Lab Sample ID: .J_..6.,_7,._8.i;J0.,_ __ _
Lab File ID: CN0§7830B18
Date Received:-08/31/90
Date Analyzed: 09/0§/90
Dilution Factor: .i~,,..o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q ----------------------------=--=------------------------------
FORM I VOA-TIC 1/87 Rev.
09 7 SA LE AT SUM RY
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lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-0l-l
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Coda: COMPO case No.: 20937 SAS No.: SDG No.: .,2..,15...__
Matrix: (soil/water) WATER Lab Sample ID: 367837
sample wt/vol: 5,0 (g/mL) Ml...,_ Lab File ID: C?:!0§7837~18 -· Level: (low/med) LOW Date Received: 08/31/90
Ii Moisture: not dee. Data Analyzed: 09/0§/90
Column: (pack/cap) CAP Dilution Factor: .1~,o~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
74-87-3---------Chloromethane
74-83-9-~-------Bromomethane
75-01-4---------Vinyl Chloride
75-00-3---------Chloroethana
75-09-2---------Methylene Chloride
67-64-1---------Acetone
75-15-o---------carbon Disulfide
75-35-4---------1,1-Dichloroethene
75-34-3---------1,1-Dichloroethane
540-59-0--------1,2-Dichloroethene (total)_
67-66-3---------Chloroform
107-06-2--------1,2-Dichloroethane
78-93-3---------2-Butanone
71-55-6---------1,1,1-Trichloroethane
56-23-5---------carbon Tetrachloride
108-05-4--------Vinyl Acetate
75-27-4---------Bromodichloromethane
78-87-5--------~l,2-Dichloropropane
10061-0l-5------cis-l,3-Dichloropropene
79-01-6---------Trichloroethene
124-48-1--------Dibromochloromethane
79-00-5---------1,1,2-Trichloroethane
71-43-2---------Benzene
10061-02-6------Trans-1,3-Dichloropropene __
75-25-2---------Bromoform
1oe-10-1--------4-Methyl-2-Pentanone
591-78-6--------2-Hexanone
127-18-4--------Tetrachloroethene
79-34-5---------1,1,2,2-Tetrachloroethane __
108-88-3--------Toluena
108-90-7--------Chlorobanzena
100-41-4--------Ethylbenzena
100-42-5--------styrene
1330-20-7-------Total Xylanas
Q
10 u
10 u
540 E
60
5 B
10 u
5 u
5
190
100
5 u
5 u
10 u
8
5 u
10 u
5 u
5 u
5 u
15
5 u
5 u
5
5 u
5 u
2 J
10 u
19
5 u
7
5 u
2 J
5 u
6
FORM I VOA 1/87 Rav.
OT
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: C2-8Bl-REVS
EPA SAMPLE NO.
MW9-0l-l
Lab Code: COMPU case No,: 20937 SAS No,: SDG No.: _2_1s...__
Matrix: (soil/water) WATER
Sample wt/vol: 5,0 (g/mL)
Level:. (low/med) 1,QW
\ Moisture: not dee.
Column (pack/cap) CAP
Number TICS found£ __.l
CAS NUMBER COMPOUND
m....._
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
367837
CN067837B18
08/31/90
09/06/90
1.0
CONC. ·Q
----=•===2••----••••••••••••==·=••=•m===-==z::11:r:11 -----=--••=-c===•••••• •==-==
1, 76-13-1 ETHANE,l,l,2-TRICHLORO-1,2,2 2.10 360 J
FORM I VOA-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
MW9-0l-1RE
Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No. : ..,2,.1,..5 __
Lab . Sample ID: _3_§7~8~3~Z~---Matrix: (soil/water) WATER
sample wt/vol: 1.0 (g/mL) Ml....,;_ Lab File ID: CR067837B18
Level: (low/med) LOW
I Moisture: not dee.
Date Received: 08/31/90
Date Analyzed: 09/06/90
Column: (pack/cap) CAP Dilution Factor: .1~,-0 __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/I<g) UG/L · Q
74-87-3---------Chloromethane 50 u
74-83-9---------Bromomethane 50 u
75-01-4---------Vinyl Chloride 510 D
75-00-3---------Chloroethane 56 D
75-09-2---------Methylene Chloride 19 BDJ
67-64-1---------Acetone "74 D
75-15-0---------carbon Disulfide 25 u
75-35-4---------1,l-Dichloroethene 25 u
75-34-3------~--l,l-Dichloroethane 200 D
540-59-0--------1,2-oichloroethene (total)_ 100 D
67-66-3---------Chloroform 25 u
107-06-2--------1,2-Dichloroethane 25 u
78-93-3---------2-Butanone 50 u
71-55-6---------1,l,l-Trichloroethane 7 DJ
56-23-5---------carbon Tetrachloride 25 u
108-05-4--------Vinyl Acetate so u
75-27-4---------Bromodichloromethane 25 u
78-87-5---~-----l,2-Dichloropropane 25 u
10061-0l-S------cis-l,3-Dichloropropene 25 u
79-01-6---------Trichloroethene 15 DJ -
124-48-1-------~Dibromochloromethane 25 u
79-oo-s---------1,1,2-Trichloroethane 25 u
71-43-2---------Benzene 25 u
10061-02-6------Trans-l,3-Dichloropropene __ 25 u
75-25-2---------Bromoform 25 u
1oa-10-1--------4-Methyl-2-Pentanone 50 u
591-78-6--------2-Hexanone 50 u
127-18-4--~-----Tetrachloroethene 18 DJ
79-34-5---------1,1,2,2-Tetrachloroethane __ . 25 u
108-88-3--------Toluene 7 DJ
108-90-7--------Chlorobenzene 25 u
100-41-4--------Ethylbenzene 25 u
100-42-5--------styrene 25 u
1330-20-7-------Total Xylenes 25 u
FORM I VOA 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
I
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
EPA SAMPLE NO.
MW9-0l-lRE
Lab Code: COMPU Caae No.: 20937 SAS No.: SDG No.: _2_15 __
Matrix: (soil/water) WATER
Sample wt/vol: 1.0 (g/mL)
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: --1.
CAS NUMBER COMPOUND
Ml.._
NAME
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.
367837
CR0§7837lll8
08/31/90
09/06/90
1,0
CONC. Q
----------------•••••••~==:a~a==========~m=~P ••a••••• •••:aa:111:1:::11::z::z•a•• ---== l. 76-13-1 ETHANE,l,l,2-TRICHLOR0-1,2,2 2.08 350 J
FORM I VOA-TIC 1/87 Rev.
20937 215\SAMPLE DATA SUMMARY
I
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lA EPA SAMPLE NO. VOLATILE ORGAN_ICS ANALYSIS DATA SHEET
MWSA-01-lMS
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS
Lab Code: COMPU Case No.: 20937 SAS No.: SDG No.: .2_.1.,,_s __
Matrix: (soil/water) WATER Lab Sample ID: 367649
Sample wt/vol: 5,0 (g/mL) ~ Lab File ID: CN067649B18
Level: (low/med) LOW Date Received: 08/31/90
Date Analyzed: 09/06/20 I Moisture: not dee.
Column: (pack/cap) CAP Dilution Factor: ~i~·~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u
75-00-3---------Chloroethane 10 u
75-09-2---------Methylene Chloride 7 B
67-64-1---------Acetone 6 J
1s-1s-o-----~---carbon Disulfide 5 u 75-35-4-----~---l,l-Dichloroethene 5 u
75-34-3---------1,1-Dichloroethane 20
540-59-0--------1,2-Dichloroethene (total)_ 7
67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 3 J
78-93-3--·-------2-Butanone 10 U.
71-55-6---------1,1,1-Trichloroethane 3 J
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5-----~cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 5 u -124-48-1--------Dibromochloromethane 5 u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,J-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 3 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzena 2 J
100-42-s--------styrene 5 u
1330-20-1-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
0 37 5 c_ Pl~ TO JMM RV
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~\
lA EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
KWBA-01-lMSD
Lab Name: CQMPUCHEM,RTP Contract: (2-88)-REVS
~ Code: CQMPY Case No.: 20937 SAS No.: SDG No. : ..,2,..1..,_5 __
Matrix: (■oil/water) WATER Lab Sample IO: 367651
Sample vt/vol: 5,0 (g/mL) ~ Lab File ID: CN06765lBlB
Level: (lov/med) LOW Date Received:-08/31/90
I Moisture: not dee. Date Analyzed: 09/06/90
Colwnn:
'
(pack/cap) !:AP Dilution Factor: 1,0
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L'
74-87-3------~--Chloromethane 10
74-83-9---~-----Bromomethane 10
75-01-4---------Vinyl Chloride 10
75-00-3---------Chloroethane 10
75-09-2---------Methylene Chloride 8
67-64-1---------Acetone 7
75-15-0---------carbon Disulfide 5
75-35-4---------1,1-Dichloroethene 5
75-34-3---------1,1-Dichloroethane 18
540-59-0--------1,2-Dichloroethene (total)_ 7
67-66-3---------Chlorotorm 5
107-06-2--------1,2-Dichloroethane 3
78-93-3---------2-Butanone 10
71-55-6---------1,1,1-Trichloroethane 3
56-23-5---------carbon Tetrachloride 5
108-05-4--------Vinyl Acetate 10
75-27-4---------Bromodichloromethane 5
78-87-5---------1,2-Dichloropropane 5
10061-01-5------cis-l,3-Dichloropropene 5
79-01-6---------Trichloroethene 5
124-48-1--------Dibromochloromethane 5
79-00-5---------1,1,2-Trichloroethane 5
71-43-2---------Benzena 5
10061-02-6------Trans-1,3-Dichloropropene __ 5
75-25-2---------Bromotorm 5
108-10-1--------4-Methyl-2-Pentanone 10
591-78-6--------2~Hexanone 10
127-18-4--------Tetrachloroethene 3
79-34-5---------1,1,2,2-Tetrachloroethane_ 5
108-88-3--------Toluane 5
108-90-7--------Chlorobenzene 5
100-41-4--------Ethylbenzen• 2
100-42-5--------styrene 5
1330-20-7-------Total Xylenes 5
Q
u
u u u
B
J u
u
u
J
u
J u
u u
u u u
u u u u u
u u
J u
u u
J u
u
FORM I_VOA 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
-
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW14ROll
Lab Name: COMPUCHEM,RTP Contract: (2-88)-REYS
Lab code: COMPU Case No.: .20937 SAS No.: SOG No.: 215
Matrix: (■oil/water) WATER Lab Sample ID: 367645
Sample wt/vol: 500 (q/mL) tu.._ Lab Pile ID: GH067645AO7
Level: (low/med) LOW Date Received: 08/30/90
I Moisture: not dee. dee. Date Extracted: 08/31/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) lL_ pH:
Date Analyzed: 09/01/90
Dilution Factor: 0.50
CONCENTRATION UNITS:
CAS NO, . COMPOUND (uq/L or uq/Kq) UG/L Q
108-95-2--------Phenol 10 u
111-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7-----·---N-N i troso-Di-n-Propylamlne_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1--:.------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
111-91-1--------bis(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-s2-1--------1,2,4-Trichlorobenzene 10 u -
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline . 10 u
87-68-3----~----Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4--~------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 ti
91-58-7---------2-Chloronaphthalene 10 ti
BB-74-4---------2-Nitroaniline 50 ti
131-11-3----~---Dimethyl Phthalate 10 . ti
208-96-8--------Acenaphthylene 10 ti
606-20-2--------2,6-Dinitrotoluene 10 ti
FORM I sv-1 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW14R011
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REYS
Lab Code: CQMPU Case No.: 20937 SAS No.: SOG No.: 215
Matrix: (soil/water) WATER Lab Sample ID: 3§7§45
Sample wt/vol: 500 (g/mL) Ml._ Lab File IO: ·s.HQ§7§45APZ
Level: (low/mad) LOW Date Received: 08/30/90
I Moisture: not dee. dee. Date Extracted: 08/31/90
Ertraction: Date Analyzed: 09/Ql/9Q
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) li..,_ pH: Dilution Factor: &Q~-~5Q,.___
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) Y!i/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acanaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2---------oiathylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether_ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phananthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------oi-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u -129-oo-o--------Pyrene 10 u
85-68"".7---------Butylbenzylphthalate 10 u
91-94-1---------3,3'-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
111-e1-1--------bi11(2-Ethylhexyl)Phthalate_ 10 u
117-84-0--------Di-n-Octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Parylene 10 u
(1) -cannot be separated from Diphenylamina
FORM I sv-2 1/87 Rev.
7 5 5 MP AT S MMARY
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lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REYS
Lab Code: COMFY ca■• No.: 20937 SAS No.: SOG
Matrix: (■oil/wat■r) WATER Lab Sample IO:
MWl4ROll
No.: 215
3§7§45
Sample wt/vol: 500 (g/mL) Ill,_ Lab File IO: GH0§7§45A07
Level: (low/med) LQW
I Moisture: not dee. dee.
Extraction: (SepF /Cont/Sonc) llU
GPC Cleanup: (Y/N) H...,_ pH:
NUlllber TICS tound: ----2.
CAS NUMBER COMPOUND NAME
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
' -RT EST. ..
08/30/90
08/31/90
09/01/90
0 I 50
CONC. Q
-•••n=•••••••• •••••••~••••a••a••••••••=••• -----------------------=
FORM I SV-TIC 1/87 Rev.
2 937 2 AT UMMARV·
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1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW150ll Lab Na.me: CQMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ,..21..,5.___
Matrix: (soil/water) WATER Lab Sample ID: ,.J..,.6.,_76,._5""0"-----
Sample wt/vol: 500 {g/mL) Ml._ Lab File ID: GH0§76SOA07
Level: (low/med) LOW
I Moi■turo: not dee. dee.
Date Received: 08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/02/90
Dilution Factor: ..,.o~,,.5..,.o __
Extraction: (SepF/Cont/Sonc) s.tU
GPC Cleanup: (Y/N) Ji_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u
11l-44-4--------bi ■(2-Chloroethyl)Ether 10 u -95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,J-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 -U
106-44-5-----~--4-Methylphenol 10 · u
621-64-7--------N-Nitroso-Di-n-Propylamine __ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
111-91-l--------bis(2-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-e2-1--------1,2,4-Trichlorobenzene 10 u -
91-20-3---------Naphthalene _ 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-J-Methylphenol 10 u
91-57-6---------2-Mothylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10. u
FORM I sv-1 1/87 Rev.
209 7 21S S /'1P DA A SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW15011
Lab Name: CQMPUCHEM,RTP Contract: C2-BB)-REVS
Lab Code: CQMPU case Ho.: 20937 SAS Ho.: ---S00 Ho.: _2_1_5 __
Matrix: (soil/water) WATER Lab Sample ID: ,3~§.7§~5~0._ __ _
Sample wt/vol: 500
LOW
(g/mL) lil,_ Lab File ID: GH0§7§50A07
Level: (low/med)
I Moisture: not dee. dee.
Date Received: OB/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/02/90
.Dilution Factor: 0.....,.5~0...__
Extraction:
GPC Cleanup:
CAS HO.
(SepF/Cont/Sonc)
(Y/H) Ji_ pH:
COMPOUND
SEU
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Hitrophenol
132-64-9--------Dibenzoturan
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Hitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------H-Hitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129~00-0--------Pyrane
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidina
56-55-3---------Benzo(a)Anthracane
218-01-9--------Chryaene
117-81-7--------bia(2-Ethylhexyl)Phthalate_
117-84-o--------Di-n-octyl Phthalata
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthena
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated trom Diphenylamine
Q
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
2 937 2 SAMP E ATA SUMMARY
-
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lF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
MW15011
Lab Name: CQMPUCHEM,RTP Contract: t2-88l-REVS
Lab Code: CQMPU ca■e No.: 20937 SAS No,: SDG No,: 215 I Matrix: (ooil/vater) WATER Lab Sample ID: 367650
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Sample wt/vol: 500 (g/mL) m._
Level: (low/med) 1.pW
I Moisture: not dee. dee.
Extraction:
GPC Cleanup:
( SepF /Cont/ Sonc)
(Y/N) H..,_ .
llU
pH:
NWllber TICS tound: ___.J.
CAS NUMBER COMPOUND NAME
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/L
RT EST,
GH0676S0A07
08/30/90
08/31/90
09/02/90
0,50
CONC, Q
--------------•••a•••-••a••••n•=~••••=•=• -------------------------1. UNKNOWN 6.32 16 J
2. METHOXYMETHYLETHOXYPROPANOL 6.35 30 J
3. METHOXYMETHYLETHOXYPROPANOL 6.38 28 J
FORM I SV-TIC 1/87 Rev •.
20937 215 SAMPLE DATA SUMMARY
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lB EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MWl50l2
Lab Name: COMPUCHEM.RTP Contract: C2-BB}-REVS
Lab Code: CQMPU case No.: 20937 SAS No.: SDG No.: 215
Matrix: (soil/water) WATER Lab sample ID: 367653
Sample wt/vol: 500 (g/mL) m...._ Lab File ID: !:iH0676:!3A07
Level: (low/med) I.OW Date Received: 08/30/90
I Moisture: not dee. dee. Date Extracted: 08/31/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL_
5.EU
pH:
Data Analyzed: 09/02/90
Dilution Factor: x0~,a5x0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) U!;i/L Q
108-95-2--------Phenol 10 u
lll-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-.8---------2-Chlorophenol 10 u
541-73-1--------1.3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1.2-Dichlorobenzene 10 u
95-48-7------~--2-Kethylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Kethylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine:::::...._ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3--~------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-0---------Benzoic Acid 50 u
lll-91-l--------bia(2-Chloroethoxy)Kethane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120~82-1--------l,2,4-Trichlorobenzene 10 u -
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroanilin• 10 u
87-68-3---------Haxachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Kethylphanol 10 u
91-57-6---------2-Kethylnaphthalen• 10 u
77-47-4---------Hexachlorocyclopentadiene_ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalen• . 10 u
88-74-4---------2-Nitroanilin• 50 u
131-11-3--------Dimethyl Phthalat• 10 u
208-96-&--------Acenaphthylen• 10 u
606-20-2--------2,6-Dinitrotolu•n• 10 u
FORM I sv-1 1/87 Rev.
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW15012
Lab Name: CQMPUCHEM.RTP Contract: {2-88)-REVS
Lab Code: COMPU Caae No.: 20937 SAS No.: SDG No.: ..._2..,15.___
Matrix: (aoil/vater) WATER Lab Sample ID: .. 3_..6.,_7.11.§,._53..__ __ _
·Sample vt/vol: 500 (g/mL) tu._ Lab File ID: GH0§7§53A07
Level: (low/med) I.Ow
I Moisture: not dee. dee.
Date Received: 08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/02/90
Dilution Factor: ¥0.._.s...,o.___
Extraction: (SepF /Cont/Sonc) llPl
GPC Cleanup: (Y/N) JL_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
99-09-2---------3-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u 51-28-5---------2,4-Dinitrophenol ·-50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzofuran 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-6~-2------~--Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
85-01-8---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-o--------Fluoranthene 10 u
129-oo-o--------Pyrerte 10 u -
85-68-7---------Butylbenzylphthalate 10 u
91-94-1-----.----3, 3 '-Dichlorobenzidine 20 u
56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
ll7-81-7--------bia(2-Ethylhexyl)Phthalate_ 10 u
117-84-o--------Di-n-octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(1) -CaMot be separated from Diphenylamine
FORM I sv-2 1/87 Rev.
20937 2151 SAMPUE DATA · SUMMARY
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP contract: 12-BBI-REVS MWl50l2
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ..,.21.,..5.___
Matrix: (uoil/water) WATER Lab Sample ID: ,.J.,.6..,7.,._6,,_53..__ __ _
Sample wt/vol: 500 (9/IIIL) HL.. Lab File ID: GH067653A07
Level: (low/med) LOW
I Moisture: not dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) lL_
NUIDber TICS tound: ___J_
dee.
pH:
CAS NUMBER COMPOUND NAME
Date Received:_ 0B/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/02/90
Dilution Factor: 0.50
CONCENTRATION UNITS:
(ug/L or u9/K9) UG/L
RT EST, CONC, Q
-•-•s•••••-• •••===•=g••--a=•m•••=•••••---=-•-=s:a ------==•---------l, UNKNOWN 6,32 18 J
2. METHOXYMETHYLETHOXYPROPANOL 6.35 24 J
3. METHOXYMETHYLETHOXYPROPANOL 6.37 24 J
FORM I SV-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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1B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW:ZA-01-1
Lab Name: CQMPUCHE'M.RTP Contract: C2-BBI-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: 215
Matrix: (■oil/water) WATER Lab Sample ID: 367644
sample wt/vol: !500 (g/l'IL) Ml.._ Lab File ID: GH067644A07
Level: (low/med) ..,LO...,W,..__ Date Received: 08/30/90
I Moiature: not dee. dee. Date Extracted: 08/31/92
Extraction: (SepF/Cont/Sonc) ilU Date Analyzed: 09/Ql/9Q
GPC Cleanup: (Y/N) l{_ pH: Dilution Factor: -9~,5~9~-
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2--------Phenol 10 u
111-44-4--------bis(:Z-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10 u
100-51-6--------Benzyl Alcohol 10 U.
95-50-1---------1,2-Dichlorobenzene 10 u
95-.48-7---------2-Methylphenol 10 u
39638-32-9------bis(:Z-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine_, _ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 u
65-85-o---------Benzoic Acid 50 u
111-91-1--------bia(:Z-Chloroethoxy)Methane_ 10 u
120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,4-Trichlorobenzene 10 u -
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-3-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47-4---------Hexachlorocyclopentadiene __ 10 u
88-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-8--------Acenaphthylene . 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 . 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW2A-Ol-l
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: CQMPU Case No.: 20937 SAS No.: SDG No.: ..._2..,15L-._
Matrix: (ooil/water) WATER Lab Sample ID: 367644
Sample wt/vol: 500 (g/mL) m..._ Lab File ID: GH0§7§44A07
Level: (low/med) I.OW Date Received: 08/30/90
I Moisture: not dee. dee. Date Extracted: 08/31/90
Extraction:
GPC Cleanup:
(SepF /Cont/Sonc)
(Y/N) l:I.,_
SIU
pH:
Date Analyzed: 09/01/90
Dilution Factor: ¥oL,~5o.,___
CAS NO. COMPOUND
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9---~----Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether_
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01.-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-oo-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3 1 -Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chryaene
ll7-8l-7,--:-----bia(2-:Ethylhexyl)Phthalate_
117-84-o--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9------.--Benzo (k) Fluoranthene
50-32-s---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
{l) -Cannot be separated from Diphenylamin•
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10· u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
Q
..
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW2A-Ol-l
Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPO case No.: 20937 . SAS No.: SDG No.: 4.2....,lSiL-_
Matrix: (soil/water) WATER
Sample wt/vol: 500 (g/mL) ~
Level: (low/med) LOW
I Moiature: not dee._ dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) L,_
$.EU
pH:
Number TICs tound: _J
CAS NUMBER COMPOUND NAME
Lab Sample ID: .,.J.,.6.,_7.,.§144,._ __ _
Lab File ID: GH0§7§44A07
Date Receivedt 08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/01/90
Dilution Factor: 0.50
CONCENTRATION UNITS:
(ug/L or ug/Xg) UG/L
RT EST. CONC. Q
------==-------••••====•=m••••••2••••••=• ----------••:a•----------1. 105-60-2 CAPROLACTAM 8.39 96 J
2. UNXNOWN 17.72 10 J
FORM I SV-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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lB EPA SAMPLE NO,
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW7-0l-l
Lab Name: COMPUCHEM,RTP Contract: 12-BBl-REVS
Lab Code : COMPU Case No.: 20937 SAS No.: SDG No.: -2-15~-
Matrix: (■oil/water) WATER Lab Sample ID: .3..,.6.._7..,6;a.43.._ __ _
Sample wt/vol: 500 (g/m.L) ML. Lab File ID: GH067643A07
Level: (low/med) LOW
, Moisture: not dee. dee.
Date Received: 08/30/90
Date Extracted: 08/31/90
Date Analyzed: 09/01/90
Dilution Factor: ..,0~.5~0.___
Extraction: ( SepF / Cont/ Sonc) uu
GPC Cleanup: (Y/N) Ii.,_ pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-95-2----~---Phenol 10 u
lll-44-4--------bis(2-Chloroethyl)Ether 10 u
95-57-8---------2-Chlorophenol 10 ·u
541-73-1--------1,3-Dichlorobenzene 10 u
106-46-7--------1,4-Dichlorobenzene 10· u
100-51-6--------Benzyl Alcohol 10 u
95-50-1---------1,2-Dichlorobenzene 10 u
95-48-7---------2-Methylphenol 10 u
39638-32-9------bis(2-Chloroisopropyl)Ether_ 10 u
106-44-5--------4-Methylphenol 10 u
621-64-7--------N-Nitroso-Di-n-Propylamine_ 10 u
67-72-1---------Hexachloroethane 10 u
98-95-3---------Nitrobenzene 10 u
78-59-1---------Isophorone 10 u
88-75-5---------2-Nitrophenol 10 u
105-67-9--------2,4-Dimethylphenol 10 U·
65-85-o---------Benzoic Acid 50 u
lll-91-l--------bis(2-Chloroethoxy)Methane_ 10 u
.120-83-2--------2,4-Dichlorophenol 10 u
120-a2-1--------1,2,4-Trichlorobenzene 10 u -
91-20-3---------Naphthalene 10 u
106-47-8--------4-Chloroaniline 10 u
87-68-3---------Hexachlorobutadiene 10 u
59-50-7---------4-Chloro-J-Methylphenol 10 u
91-57-6---------2-Methylnaphthalene 10 u
77-47~~---------Hexachlorocyclopentadiene_ 10 u
aa-06-2---------2,4,6-Trichlorophenol 10 u
95-95-4---------2,4,5-Trichlorophenol 50 u
91-58-7---------2-Chloronaphthalene 10 u
88-74-4---------2-Nitroaniline 50 u
131-11-3--------Dimethyl Phthalate 10 u
208-96-a------~-Acenaphthylene 10 u
606-20-2--------2,6-Dinitrotoluene 10 u
FORM I sv-1 1/87 Rev.
20937 215\ SAMPLJ DATA SUMMARY
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lC EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Noe: CQMPUCHEM.RTP Contract: (2-BBl-REVS
Lab Code: COMFY Case No.: 20937 SAS No.: SDG No.: 2 J,5
Matrix: (moil/water) WATER Lab Sample ID: 367643
Suple vt/vol1 500 (9/IIIL) HI._ Lab File ID: GH0§7643A07
Level: (low/med) I.OW Date Received: 08/30/90
I Moisture: not dee. dee. Date Extracted: OB/JJ,/90
Extraction: (SepF/Cont/Sonc) llU Date Analyzed: 09/0J,/90
GPC Cleanup: (Y/N) li_ ·pH: Dilution Factor: ~o~,5~0.__
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or u9/K9) UG/L Q
99-09-2---------J-Nitroaniline 50 u
83-32-9---------Acenaphthene 10 u
51-28-5---------2,4-Dinitrophenol 50 u
100-02-1--------4-Nitrophenol 50 u
132-64-9--------Dibenzoturan 10 u
121-14-2--------2,4-Dinitrotoluene 10 u
84-66-2-----~---Diethylphthalate 10 u
7005-72-3-------4-Chlorophenyl-phenylether_ 10 u
86-73-7---------Fluorene 10 u
100-01-6--------4-Nitroaniline 50 u
534-52-1--------4,6-Dinitro-2-Methylphenol_ 50 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 10 u
101-55-3--------4-Bromophenyl-phenylether __ 10 u
118-74-1--------Hexachlorobenzene 10 u
87-86-5---------Pentachlorophenol 50 u
as-01-a---------Phenanthrene 10 u
120-12-1--------Anthracene 10 u
84-74-2---------Di-n-Butylphthalate 10 u
206-44-0--------Fluoranthene 10 u
129-00-0--------Pyren• 10 u -
85-68-7---------Butylbenzylphthalate 10 u
91-94-1---------3 3'-Dichlorobenzidine · 20 u , ' 56-55-3---------Benzo(a)Anthracene 10 u
218-01-9--------Chrysene 10 u
ll7-8l-7--------bia(2-Ethylhexyl)Phthalate_ 10 u
117-84-0--------Di-n-Octyl Phthalate 10 u
205-99-2--------Benzo(b)Fluoranthene 10 u
207-08-9--------Benzo(k)Fluoranthene 10 u
50-32-8---------Benzo(a)Pyrene 10 u
193-39-5--------Indeno(l,2,J-cd)Pyrene 10 u
53-70-3---------Dibenzo(a,h)Anthracene 10 u
191-24-2--------Benzo(g,h,i)Perylene 10 u
(l) -CaMot be separated trom Diphenylamin•
FORM I sv-2 1/87 Rev.
20937 215 SAMPLE DATA SUMMARY
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·lF EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMFY ca■e No.: 20937 SAS No.: SOG No.: ._2..,15....__
Matrix: ·(■oil/water) WATER
Sample wt/vol: !500
Level: (low/med) LOW
I Moisture: not dee.
(g/mL) Ml._
dee.
Lab Sample ID: _3_§~2-§4~3 ___ _
Lab F.ile ID: GH067643A07
Date Received: 08/30/90
Date Extracted: 08/31/90
Extraction: (SepF/Cont/Sonc) llU Date Analyzed:. 09/01/90
GPC Cleanup: (Y/N) H..._ pH: Dilution Factor: &0~1 ,50,.__
CONCENTRATION UNITS:
NWllber TICs found:~ (ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
•••••••a••=••••• •••••=•==ma•a=•=••m•••-••------------=--------==
FORM I SV-TIC 1/87 Rev.
20937 215 SAMPLE DATA SUMMARV
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB19-JS-l Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPO Case Ho.: 21492 SAS Ho.: SDG Ho.: 01
Matrix: (soil/water) SOIL · Lab Sample ID: 373518
Sample wt/vol: 30,4
LOW
(g/mL) !L.__ Lab File ID: GH073~18BO§
Level: (low/med) Date Received: 10/12/90
t Moisture: not dee. --1.l dee .. Date Extracted: 10/15(20
Extraction: (SepF/Cont/Sonc) SQl:lC Date Analyzed: 10/23(20
GPC Cleanup: (Y/H) lL,_ pH: ....L.§ Dilution Factor: .1-,~o __ _
CAS HO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
99-09-2---------3-Hitroaniline 1900 83-32-9-------;..-Acenaphthene 400 51-28-5---------2,4-Dinitrophenol 1900 100-02-1--------4-Hitrophenol 1900 132-64-9--------Dibenzoturan 400 121-14-2--------2,4-Dinitrotoluene 400 84-66-2---------Diethylphthalate. 400 7005-72-3-------4-Chlorophenyl-phenylether_ 400 86-73-7---------Fluorene 400 100-01-6--------4-Hitroaniline 1900 534-52-1--------4,6-Dinitro-2-Methylphenol __ 1900 86-30-6---------N-Hitrosodiphenylamine (1)_ 400 101-55-3-------.-4-Bromophenyl-phenylether __ 400 118-74-1--------Hexachlorobenzene 400 87-86-5---------Pentachlorophenol 1900 as-01-a---------Phenanthrene 400 120-12-1--------Anthracene 400 84-74-2------_.--Di-n-Butylphthalate 400 206-44-0--------.Fluoranthene 400 129-00-0--------Pyrene 400 85-68-7---------Butylbenzylphthalate 400 91-94-1---------3,3'-Dichlorobenzidine 790 56-55-3---------Benzo(a)Anthracene 400 218-01-9--------Chrysene 400 117-81-7--------bis(2-Ethylhexyl)Phthalate_ 400 117-84-0--------Di-n-Octyl Phthalate 400
205-99-2--------Benzo(b)Fluoranthene 400 207-08-9--------Benzo(k)Fluoranthene 400
50-32-8---------Benzo(a)Pyrene 400
193-39-5--------Indeno(l,2,3-cd)Pyrene 400
53-70-3---------Dibenzo(a,h)Anthracene 400
191-24-2--------Benzo(g,h,i)Perylene 400
(1) -Cannot be separated trom Diphenylamine
u u
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u u u
u u u u
FORM I sv-2 1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP contract: (2-881-REVS
EPA SAMPLE NO.
S819-3S-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373518
Sample wt/vol: 30.4 (g/mL) L-Lab File ID: GH073518B06
Level: ( low/med) LOW Date Received: 10/12/90
I Moisture: not dee. _.11 dee. Date Extracted: 10/15/90
Extraction: (SepF/Cont/Sonc) ~ Date.Analyzed: lQ/23/90
GPC Cleanup: (Y/N) H..._ pH:~ Dilution Factor: 41L,a,.__ __
Number TICS found: __l
CONCENTRATION UNITS:
(ug/~ or ug/Kg) UG/KG
• CAS NUMBER COMPOUND NAME RT EST. CONC. Q
ma============== --=-=-------=--===---=-----= =-======= a============ --=== 1. SOLVENT CONTAMINANT 3.92 480 BJ 2. ALDOL 4.97 440 BAJ 3. HEXANEDIOIC ACID,MON0(2-ETHY 16.10 160 J '
FORM I SV-TIC 1/87 Rev.
92 1 ~ MP Dd.T SUM 76
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Lab Name: COMPUCHEM.RTP SB20-3S-l Contract: (2-88)-REVS
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample IO: 373520
sample wt/vol: 30.2 (g/mL) Si,___ Lab File ID: GH073520B06
Level: ( low/med) LOW Date Received: 10/12/90
t Moisture: not dee. _l,! dee. Date Extracted: 10/15/90
Extraction: (SepF/Cont/Sonc) S.Q.1iC
GPC Cleanup: (Y/N) JL_ pH: ....L..1
Date Analyzed: 10/26/90
Dilution Factor: 1,00
CONCENTRATION UNITS:
CAS NO; COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 430 u lll-44-4--------bis(2-Chloroethyl)Ether 430 u 95-57-8---------2-Chlorophenol 430 u 541-73-1--------1,3-Dichlorobenzene 430 u 106-46-7--------1,4-Dichlorobenzene 430 u 100-51-6--------Benzyl Alcohol 430 u 95-50-1---------1,2-oichlorobenzene 430 u 95-48-7---------2-Methylphenol 430 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 430 u 106-44-5--------4-Methylphenol 430 u 621-64-7--------N-Nitroso-Di-n-Propylamine_ 430 u 67-72-1---------Hexachloroethane 430 u 98-95-3----~----Nitrobenzene 430 u 78-59-1---------Isophorone 60 J 88-75-5---------2-Nitrophenol. 430 u 105-67-9--------2,4-Dimethylphenol 430 u 65-85-o---------Benzoic Acid 2100 u lll-91-l--------bis(2-Chloroethoxy)Methane_ 430 u 120-83-2--------2,4-Dichlorophenol 430 u
120-82-1--------1,2,4-Trichlorobenzene 430 u 91-20-3---------Naphthalene 430 u 106-47-8--------4-Chloroaniline 430 u
87-68-3---------Hexachlorobutadiene 430 u
59-50-7---------4-Chloro-3-Methylphenol 430 u 91-57-6---------2-Methylnaphthalene 430 u 77-47-4---------Hexachlorocyclopentadiene __ 430 u
88-06-2---------2,4,6-Trichlorophenol 430 u
95-95-4---------2,4,5-Trichlorophenol 2100 u
91-58-7---------2-Chloronaphthalene 430 u
88-74-4---------2-Nitroaniline 2100 u
131-11-3-------~Dimethyl Phthalate 430 u
208-96-8--------Acenaphthylene 430 u
606-20-2--------2,6-Dinitrotoluene 430 u
FORM I sv-1 1/87 Rev.
? ? 1 ~ MP/ ()QT ~II RY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET .. ::-n ~n.M.r.L...C. ~v.
SB20-3S-l Lab Name: COMPUCHEM.RTP contract: 12-88)-REVs
Lab Code: COMPO Case No.: 21492 SAS No.: SOG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373520
Sample wt/vol: 30,2 (g/mL) Si...._ Lab File ID: GH073520B06
Level: (low/med) LOW Date Received: 10/12/90
I Moisture: not dee. _-2.J. dee. Date Extracted: lQ/15/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) li,_
SQHC
pH: ....L..3.
Data Analyzed: 10/26/90
Dilution Factor: ~l~•~0~0 __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2100 u 83-32-9---------Acenaphthene 430 u 51-28-5---------2,4-Dinitrophenol 2100 u 100-02-1--------4-Nitrophenol 2100 u 132-64-9--------Dibenzoturan 430 u
121-14-2--------2,4-Dinitrotoluene 430 u
84-66-2---------Diethylphthalate 430 u 7005-72-3-------4-Chlorophenyl-phenylether_ 430 u 86-73-7---------Fluorene 430 u
100-01-6--------4-Nitroaniline 2100 u
534-52-1--------4,6-Dinitro-2-Methylphenol __ 2100 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 430 u 101-55-3--------4-Bromophenyl-phenylether __ 430 u
118-74-1--------Hexachlorobenzene 430 u
87-86-5---------Pentachlorophenol 2100 u
85-01-8---------Phenanthrene 430 u
120-12-1--------Anthracene 430 u
84-74-2---------Di-n-Butylphthalate 430 u
206-44-0--------Fluoranthene 430 u
129-.oo-o--------Pyrene 430 u
85-68-7---------Butylbenzylphthalate 430 u
91-94-1---------3,3'-0ichlorobenzidine 860 u
56-55-3---------Benzo(a)Anthracene 430 u
218-01-9-----~--chry■ene 430 u
117-8l-7--------bia(2-Ethylhexyl)Phthalate_ 430 u
111-e4-o--------01-n-0c:tyl Phthalate 430 u
205-99-2--------Benzo(b)Fluoranthene 430 u
207-08-9--------Benzo(k)Fluoranthene 430 u
50-32-8---------Benzo(a)Pyrena 430 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 430 u
53-70-3---------0ibenzo(a,h)Anthracene 430 u
191-24-2--.------Benzo (g ,h, i) Perylane 430 u
(1) -CaMot be ■eparated from Diphenylamine
FORM I sv-2 1/87 Rav.
? ? 1 c;c, Pl J: T UMM 74
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: 12-88)-REVS
EPA SAMPLE NO.
SB20-JS-l
Lab Code: COMPU Case No.: 21492 SAS No,: SDG No.: 01
Matrix: (soil/water) SOIL
Sample wt/vo.l: 30,2 (g/mL) ~
Level: (low/med) .,LO,._,W...__
I Moisture: not dee. _2.J. dee.
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) IL..
SQHC
pH: __L_1
Number TICs found: ___J_
CAS NUMBER COMPOUND NAME
Lab Sample IO: 373520
Lab File IO: GH073520B06
Date Received: 10/12/90
Date Extracted: 10/15/90
Date Analyzed: 10/26/90
Dilution Factor: .1~1 0,._,o.__
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST. CONC, Q :zm====•••==•===• ••m=----=-=-=--=-------==----======-•====-===-=-=-= =-==== ,
1. UNJQIOWN AI.KANE 5,85 390 J 2. UNKNOWN AI.KANE 5,93 740 J J. ALOOL 6,92 440 AJ
FORM I SV-TIC 1/87 Rev,
21492 01 SAMPLE DATA SUMMARY
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM, RTP Contract: 12-88)-REYS S821-3S-l
Lab Code: COMPU case No.: 21492 SAS No.:· __ _ SOG Ko.: ~0_1 __
Matrix: (soil/water) SOIL Lab Sample IO: 373780
Sample wt/vol: 30.7 (g/mL) ~
LOW
Lab File ID: GH073780C07
Level: (low/med) Date Received: l!2".l3,:'.9Q
I Moisture: not dee. _.1.2, dee. Date Extracted: 10,:'.l§<'.'.90
Extraction: (SepF/Cont/Sonc) SQH.C
....L..1
Date Analyzed: 10,:'.lB,:'.90
GPC Cleanup: (Y/N) lL.._ pH: Dilution Factor: 1,00
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG,:'.KG Q
108-95-2--------Phenol 410 u lll-44-4--------bis(2-Chloroethyl)Ether 410 u 95-57-8---------2-Chlorophenol 410 u 541-73-1--------1,J-Dichlorobenzene 410 u 106-46-7--------1,4-Dichlorobenzene 410 u 100-51-6--------Benzyl Alcohol 410 u 95-50-1---------1,2-oichlorobenzene 410 u 95-48-7---------2-Methylphenol 410 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 410 u 106-44-5--------4-Methylphenol 410 u 621-64-7--------K-Kitroso-Di-n-Propylamine_ 410 u 67-72-1---------Hexachloroethane 410 u 98-95-3---------Kitrobenzene 410 u 78-59-1---------Isophorone 76 J· 88-75-5---------2-Kitrophenol 410 u •105-67-9--------2,4-0imethylphenol 410 . u 65-85-o---------Benzoic Acid 2000 u lll-91-l--------bis(2-Chloroethoxy)Methane_ 410 u 120-83-2--------2,4-0ichlorophenol 410 u 120-s2-1--------i,2,4-Trichlorobenzene 410 u 91-20-3---------Kaphthalene 410 u 106-47-8--------4-Chloroaniline 410 u 87-68-3---------Hexachlorobutadiene 410 u 59-50-7---------4-Chloro-3-Methylphenol 410 u 91-57-6---------2-Methylnaphthalene 410 u 77-47-4---------Hexachlorocyclopentadiene __ 410 u 88-06-2---------2,4,6-Trichlorophenol 410 u 95-95-4---------2,4,5-Trichlorophenol 2000 u 91-58-7---------2-Chloronaphthalene 410 u
88-74-4---------2-Kitroanilin• 2000 tJ
131-11-J--------oimethyl Phthalate 410 0
208-96-8--------Acenaphthylene 410 u
606-20-2--------2,6-Dinitrotoluene 410 u
FORM I sv-1 1/87 Rev.
1 TO V ..,...., , ,·
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
SB21-3S-l Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373780
Sample wt/vol: 30,7 (g/mL) ~ Lab File ID: GII073780CQ7
Level: (low/med) LOW Date Received: 10/13/90
% Moisture: not dee. ---2..2. dee. Date Extracted: l.Otl!it20
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) tL_
~
pH: ....L..3.
Date Analyzed: 10/18/90
, Dilution Factor: 1.00
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L·or ug/Kg) UG/KG
99-09-2---------J-Nitroaniline 2000 83-32-9---------Acenaphthene 410 51-28.-5---------2, 4-Dinitrophenol 2000 100-02-7--------4-Nitrophenol 2000 132-64-9--------Dibenzoturan 410 121-14-2--------2,4-Dinitrotoluene 410 84-66-2---------Diethylphthalate 410 7005-72-3-------4-Chlorophenyl-phenylether __ 410 86-73-7---------Fluorene 410 100-01-6--------4-Nitroaniline 2000 534-52-1--------4,6-Dinitro-2-Methylphenol_ 2000 86-30-6---------N-Nitrosodiphenylamine (1)_ 410 101-55-3--------4-Bromophenyl-phenylether __ 410 118-74-1--------Hexachlorobenzene 410 87-86-5---------Pentachlorophenol 2000 85-01-8---------Phenanthrene 410 120-12-1--------Anthracene 410
84-74-2-----~---Di-n-Butylphthalate 410 206-44-0--------Fluoranthene 410 129-00-0--------Pyreno 410
85-68-7---------Butylbenzylphthalate 410
91-94-1---------J,J'-Dichlorobenzidine 830
56-55-3---------aenzo(a)Anthracene 410 218-01-9--------Chrysene 410 117-81-7--------bia(2-Ethylhexyl)Phthalate_ 410
111-a,-o--------oi-n-octyl Phthalate 410
205-99-2--------Benzo(b)Fluoranthene 410
207-08-9--------Benzo(k)Fluoranthene 410
50-32~8---------Benzo(a)Pyrene 410
193-39-5--------Indeno(l,2,J-cd)Pyrene 410
53-70-3---------Dibenzo(a,h)Anthracene 410
191-24-2--------Benzo(g,h,i)Perylene 410
(1) -Cannot be separated trom Diphenylamine _,
u
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u u u
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u
u u u u u u
u u u u
u u u
FORM I sv-2 1/87 Rev.
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CQMPUCHEM.RTP Contract: (2-88\-REVS
EPA SAMPLE NO.
SB21-JS-l
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL
sample wt/vol: 30.7 (g/mL) L_
Level: (low/med) LOW
% Moisture: not dee. _n dee.
Extraction: (SepF/Cont/Sonc) ~
'GPC Cleanup: (Y/N) .IL_ pH: ....L.l
Number TICS tound: --2.
CAS NUMBER COMPOUND NAME
Lab sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
RT EST.
373780
GH07J7BOC07
lO/lJ/90
10/15/90
10/18/90
1.00
CONC. Q ~============== -=========================== =-======= ============-= •===-= 1. SOLVENT CONTAMINANT 5.08 290 BJ 2. ALDOL 5.83 290 ABJ
FORM I SV-TIC 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 7(
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18 EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP SB22-3S-l Contract: C2-88l-REVS
Lab Code: COMPU case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab sample IO: 373784
Sample wt/vol: 30,5 (g/mL) ~ Lab File ID: GH07J784C07
Level: (low/med) LOW Data Received: 10/13/90
% Moisture: not dee. _1..0 .dee. Data Extracted: l0/l!i/90
Extraction: (SepP/Cont/Sonc)
(Y/N) H...._
.5.QHC
pH: .....L..1
Date Analyzed: 10/18/90
GPC Cleanup: Dilution Factor: .1~,~o __ _
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-95-2--------Phenol 360
lll-44-4--------bis(2-Chloroethyl)Ether 360
95-57-8---------2-Chlorophenol 360
541-73-1--------1,3-Dichlorobenzene 360
106-46-7--------1,4-Dichlorobenzene 360
100-51-6--------Benzyl Alcohol 360
95-50-1---------1,2-Dichlorobenzene 360
95-48-7---------2-Methylphenol 360
39638-32-9------bis(2-Chloroisopropyl)Ether_ 360
106-44-5--------4-Methylphenol 360
621-64-7--------N-Nitroso-Di-n-Propylamine_ 360
67-72-1---------Hexachloroethane 360
98-95-3---------Nitrobenzene 360
78-59-1---------Isophorone 360
88-75-5---------2-Nitrophenol 360
105-67-9--------2,4-Dimathylphenol 360
65-85-o---~-----Benzoic Acid 1700
lll-91-l--------bis(2-Chloroethoxy)Methane __ 360
120-83-2--------2,4-Dichlorophenol 360
120-82-1--------1,2,4-Trichlorobenzena 360
91-20-3---------Naphthalene 360
106-47-8--------4-Chloroaniline 360
87-68-3---------Hexachlorobutadiene 360
59-50-7---------4-Chloro-3-Methylphenol 360
91-57-6---------2-Methylnaphthalene 360
77-47-4---------Hexachlorocyclopentadiene __ 360
88-06-2---------2,4,6-Trichlorophanol 360
95-95-4---------2,4,5-Trichlorophenol 1700
91-58-7---------2-Chloronaphthalene 360
88-74-4---------2-Nitroaniline 1700
131-11~3--------Dimethyl Phthalate 360
208-96-8----~---Acenaphthylene 360
606-20-2--------2,6-Dinitrotoluene 360
u u
u u u
u u u u
u u u u
u u u u u u u u
u u u
u u u
u u u u u
u
FORM I sv-1 1/87 Rev.
..... II 0
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM, RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
EPA SAMPLE NO.
S822-3S-l
No.: 01 I Matrix: (soil/water) SOIL Lab sample ID: 373784
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Sample wt/vol: 30.5 (g/mL) ~ Lab File ID: GH07J784CQ7
Level: (low/med) I.OW Date Received: 10/13/90
I Moisture: not dee. --1.2 dee. Date Extracted: l,0/1§£'.90
Extraction: (SepF/Cont/Sonc) Date Analyzed: l,O/l,8/90
GPC Cleanup: (Y/N) l:f....._ pH: ---1L2 Dilution Factor: 41.._, o.,__ __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGlKG Q
99-09-2---------3-Nitroaniline 1700 u 83-32-9---------Acenaphthene 360 u 51-28-5---------2,4-Dinitrophenol 1700 u 100-02-7--------4-Nitrophenol 1700 u 132-64-9--------Dibenzoturan 360 u 121-14-2--------2,4-Dinitrotoluene 360 u 84-66-2---------Diethylphthalate 360 u 7005-72-3-------4-Chlorophenyl-phenylether_ 360 u 86-73-7---------Fluorene 360 u 100-01-6--------4-Nitroaniline 1700 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 1700 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 360 u 101-55-3--------4-Bromophenyl-phenylether __ 360 u 118-74-1--------Hexachlorobenzene 360 u
87-86-5---------Pentachlorophenol 1700 u 85-01-8------~--Phenanthrene 360 u 120-12-1--------Anthracene 360 u 84-74-2---------Di-n-Butylphthalate 360 u
206-44-0--------Pluoranthene 360 u
129-00-0--------Pyrene 360 u
85-68-7---------Butylbenzylphthalate 360 u
91-94-1---------3,3'-Dichlorobenzidine 720 u
56-55-3---------Benzo(a)Anthracene 360 u
218-01-9--------Chrysene 360 u
117-81-7--~-----bis(2-Ethylhexyl)Phthalate_ 360 u
117-84-0--------Di-n-Octyl Phthalate 360 u
205-99-2--------Benzo(b)Pluoranthene 360 u
207-08-9--------Benzo(k)Pluoranthene 360 u
50-32-8---------Benzo(a)Pyrene 360 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 360 u
53-70-3---------Dibenzo(a,h)Anthracene 360 u
191-24~2--------Benzo(g,h,i)Perylene 360 u
(1) -cannot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY
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lF SEMIVOLATILE 'ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTp Contract: (2-881-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
Matrix: (soil/water) SOIL Lab Sample ID:
Sample wt/vol: 30.5 (g/mL) L_ Lab File ID:
( low/med) LOW Date Received:
I Moisture: not dee. ---1..Q dee. Date Extracted:
Extraction: (SepF/Cont/Sonc) ~ Data Analyzed:
EPA SAMPLE NO.
SB22-JS-l
No.: 01
373784
GH07J784C07
l,OllJl'.90
101'.16/90
l,Oll,8l90
GPC cleanup: (Y/N) IL_ pH: _L..1 Dilution Factor: -l.~,9~--
CONCENTRATION UNITS: Nlllllber TICs toundi ~ (ug/L or ug/Kg) UGlKC
CAS NUMBER COMPOUND NAME RT EST. CONC. Q 3am••==~=======• ----=--=--==-=------==-===== =-======= --=========== •=-=== l. SOLVENT CONTAMINANT 5.10 470 BJ 2. ALDOL 5.85 360 ABJ
FORM I SV-TIC 1/87 Rev.
21492 01 SAMPLE ORTA SUMMARY 67
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18
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS MW20-35-lMS
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373179
Sample wt/vol: 30.7 (g/mL) L-Lab File ID: GH073179AS2
Level: (low/med) LOW Date Received: 10/10/90
' Moisture: not dee. _li dee. Date Extracted: 10/l,0/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sonc)
(Y/N) H_
~
pH: __5,._2_
Date Analyzed: 10(12(90
Dilution Factor: .1~-~0¥0 __
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 500 u lll-44-4--------bis(2-Chloroethyl)Ether 500 u 95-57-8---------2-Chlorophenol 500 u 541-73-1--------l,3-Dichlorobenzene 500 u !06-46-7--------1,4-Dichlorobenzene 500 u 100-51-6--------Benzyl Alcohol ' 500 u 95-50-1---------1,2-Dichlorobenzene 500 0 95-48-7---------2-Methylphenol 500 0 39638-J2-9------bis(2-Chloroisopropyl)Ether_ 500 u 106-44-5--------4-Methylphenol 500 0 621-64-7--------N-Nitroso-Di-n~Propylamine __ 500 u 67-72-1---------Hexachloroethane 500 u 98-95-J-~-------Nitrobenzene 500 u 78-59-1---------Isophorone 500 u 88-75-5---------2-Nitrophenol 500 u 105-67-9--------2,4-Dimethylphenol 500 u 65-85-o---------Benzoic Acid 2400 0 lll-91-l--------bis(2-Chloroethoxy)Methane __ 500 u 120-sJ-2----~---2,4-Dichlorophenol 500 u 120-82-1--------.1, 2, 4-Trichlorobenzene 500 0
91-20-3---------Naphthalene 500 u
106-47-s---~----4-Chloroaniline 500 u
87-68-3---------Hexachlorobutadiene 500 u 59-50-7---------4-Chloro-J-Methylphenol 500 0 91-57-6---------2-Methylnaphthalene 500 u
77-47-4---------Hexachlorocyclopentadiene __ 500 u
88-06-2---------2,4,6-Trichlorophenol 500 u
95-95-4---------2,4,5-Trichlorophenol 2400 0
91-58.-7---------2-Chloronaphthalene 500 0
88-74-4---------2-Nitroaniline 2400 0
131-11-3--------Dimethyl Phthalate 500 0
208-96-8--------Acenaphthylene 500 0
606-20-2--------2,6-Dinitrotoluene 500 0
FORM I sv-1 1/87 Rev.
• ? 1 .d.Q? Cl 1 C:OMPl ,:: f'HlTO C:IIMJrlQ~V 6t
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: CQMPUCHEM.RTP. Contract: (2-88)-REVS MW20-J5-lMS
Lab Code: CQMPU Case No.: 21492 SAS No.: SOG No.: .,.0""l~-
Matrix: · (soil/water) SOIL Lab Sample ID: .._J.,_7.,,_J._17£.;9z__ __ _
Sample.wt/vol: 30.7 (g/mL) !i__ Lab File ID: GH073179A52
Level: ( low/med) I,PW
\ Moisture: not dee.~ dee.
Date Received: 10/10/90
Date Extracted: 10/10/90
Date Analyzed: 10/12/90 Extraction: (SepF /Cont/Sonc)
GPC Cleanup: (Y/N) L.. pH: ..2J, Dilution Factor: .i~·~o~o __
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------J-Nitroaniline 2400 u 83-32-9---------Acenaphthene 500 u 51-28-5---------2,4-Dinitrophenol 2400 u 100-02-1--------4-Nitrophenol 2400 u 132-64-9--------Dibenzoturan 500 u 121-14-2--------2,4-Dinitrotoluene 500 u 84-66-2---------Diethylphthalate 500 u 7005-72-3--~----4-Chlorophenyl-phenylether_ 500 u 86-73-7---------Fluorene 500 u 100-01-6--------4-Nitroaniline 2400 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 2400 u
86-30-6---------N-Nitrosodiphenylamine (l)_ 500 u 101-55-3--------4-Bromophenyl-phenylether __ 500 u 118-74-1--------Hexachlorobenzene 500 u 87-86-5---------Pentachlorophenol 2400 u
85-01-8---------Phenanthrene 500 u 120-12-1--------Anthracene 500 u 84-74-2---------Di-n-Butylphthalate 500 u 206-44-0--------Pluoranthene 500 u
129-00-0--------Pyrene 500 u 85-68-7---------Butylbenzylphthalate 500 u
91-94-1---------3,3'-Dichlorobenzidine 990 u
56-55-3---------Benzo(a)Anthracene 500 u
218-01-9--------Chrysene 500 u
ll7-8l-7--------bis(2-Ethylhexyl)Phthalate_ 500 u
117-84-o--------Di-n-Octyl Phthalate 500 u 205-99-2--------Benzo(b)Fluoranthene 500 u
207-08-9--------Benzo(k)Fluoranthene 500 u
50-32-a---------Benzo(a)Pyrene 500 u
193-39-5--------Indeno(l,2,3-cd)Pyrene 500 u
53-70-3---------Dibenzo(a,h)Anthracene 500 u
191-24-2-~------Benzo(g,h,i)Perylene 500 u
(1) -CaMot be separated trom Diphenylamine
FORM I sv-2 1/87 Rov.
21492 01 SAMPLE DATA SUMMARY'
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18
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM, RTP . Contract: (2-88)-REVS KW20-J5-1MSD
Lab Code: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (soil/water) SOIL Lab Sample ID: 373180
Sample wt/vol: 30 I 2 (g/mL) L_ Lab File ID: GH073180A52
Level: ( low/med) LOW Date Received: 10/10/90
I Moisture: not dee. _ll dee. Date Extracted: 10/10/90
Extraction: ( SepF / Cont/ Sonc) SQfil:
...2...2.
Date Analyzed: 10/12/90
GPC Cleanup: (Y/N) H__ pH: Dilution Factor: 1,00
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-95-2--------Phenol 500 u lll-44-4--------bis(2-Chloroethyl)Ether 500 u 95-57-8---------2-Chlorophenol 500 u 541-73-1--------1,3-Dichlorobenzene 500 u 106-46-7--------1,4-Dichlorobenzene 500 u 100-51-6--------Benzyl Alcohol 500 u 95-50-1---------1,2-Dichlorobenzene 500 u 95-48-7---------2-Methylphenol 500 u 39638-32-9------bis(2-Chloroisopropyl)Ether_ 500 u 106-44-5--------4-Methylphenol 500 u 621-64-7--------N-Nitroso-Di-n-Propylamine_ 500 u 67-72-1---------Hexachloroethane 500 u 98-95-3---------Nitrobenzene , 500 u 78-5--1---------Isophorone 500 u 88-75-5---------2-Nitrophenol 500 u 105-67-9--------2,4-Dimethylphenol 500 u 65-85-o---------Benzoic Acid 2400 u lll-91-l--~-----bia(2-Chloroethoxy)Methane_ 500 u 120-83-2--------2,4-Dichlorophenol 500 u 120-s2-1--------l,2,4-Trichlorobenzene 500 u 91-20-3---------Naphthalene 500 u 106-47-8--------4-Chloroaniline 500 u 87-68-3---------Hexachlorobutadiene 500 u
59-50-7---------4-Chloro-3-Methylphenol 500 u
•91-57-6---------2-Methylnaphthalene 500 u 77-47-4---------Hexachlorocyclopentadiene __ 500 u
88-06-2---------2,4,6-Trichlorophenol 500 u 95-95-4---------2,4,5-Trichlorophenol 2400 u 91-58-7---------2-Chloronaphthalene 500 u
88-74-4---------2-Nitroaniline 2400 u
131-11-3--------Dimethyl Phthalate 500 u
208-96-8--------Acenaphthylene 500 u
606-20-2--------2,6-Dinitrotoluene 500 u
FORM I sv-1 1/87 Rev.
21492 01 SAMPLE DATA SUMMARY 64
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP · Contract: (2-88)-REVS MW20-35-1MSD
Lab Coda: COMPO Case No.: 21492 SAS No.: SDG No.: 01
Matrix: (■oil/water) SOIL Lab Sample ID: 373180
Sample wt/vol: 30,2 (g/lllL) Si,__ Lab File ID: GH073180AS2
Level: (low/med) LOW Date Received: 10/10/90
' Moisture: not dee. _ll dee. Date Extracted: J,0/10/90
Extraction:
GPC Cleanup:
(SepF/Cont/Sone)
(Y/N) IL_
SQHC
pH: ~
Date Analyzed: 10/12/90
Dilution Factor: .1~,o~o.___
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
99-09-2---------3-Nitroaniline 2400 0 83-32-9-----,---Acenaphthene 500 0 51-28-5---------2,4-Dinitrophenol ·2400 0 100-02-1-----~--4-Nitrophenol 2400 u 132-64-9--------Dibenzoturan 500 u 121-14-2-----7--2,4-Dinitrotoluene 500 u 84-66-2---------Diethylphthalate 500 u 7005-72-3-------4-Chlorophenyl-phenylether __ 500 0 86-73-7--7------Fluorene 500 u 100-01-6--------4-Nitroaniline 2400 u 534-52-1--------4,6-Dinitro-2-Methylphenol_ 2400 u 86-30-6---------N-Nitrosodiphenylamine (l)_ 500 u
101-55-3--------4-Bromophenyl-phenylether_ 500 u
118-74-1--------Hexachlorobenzene 500 u 87-86-5---------Pentachlorophenol 2400 u 85-01-8---------Phenanthrene . 500 u
120-12-1--------Anthraeene 500 u
84-74-2---------Di-n-Butylphthalate 500 u 206-44-0--------Fluoranthene 500 0 129-00-0--------Pyrene 500 u
85-68-7---------Butylbenzylphthalate 500 u
91-94-1---~-----3,3'-Diehlorobenzidine 1000 u 56-55-3---------Benzo(a)Anthraeene 500 u 21s-01-9--------Chrysene 500 u
117-81-7--------bia(2-Ethylhexyl)Phthalate_ 500 u
117-84-o--------oi-n-octyl Phthalate 500 u
205-99-2--------Benzo(b)Fluoranthene 500 u
201-oa-9--------Benzo(k)Fluoranthene 500 0
~0-32-a---------Benzo(a)Pyrene 500 0
193-39-5--------Indeno(l,2,3-ed)Pyrene 500 u
53-70-3---------Dibenzo(a,h)Anthraeene 500 0
191-24-2--------Benzo(g,h,i)Perylene 500 u
(1) -CaMot be separated trom Diphenylamine
FORM I sv-2 1/87 Rev.
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CDMPUCHEM
IABoRATORlES, !['.IC.
CLP CASE NARRATIVE CASE# 21492
CONTRACT# 2-88 (REVS) SDG# 21
COMPUCHEM LABORATORIES INC.
SAMPLES: MW15A01-1, MW18-01~1, MW20-01-1
This portion of Case # 21492 consisted of three liquid
samples for volatile and semivolatile analysis. They were
received intact on 10/17/90 and 10/18/90 via federal Express
in properly sealed shipping containers with traffic reports.
VOLATILES:
All volatile fractions were analyzed within holding time
requirements. All three samples contained methylene
chloride, which was also detected in the associated
instrument blank.· In addition, sample MW15AD1-l contained
carbon disulfide, a variety of chlorinated hydrocarbons,
benzene, toluene, ethylbenzene, and total xylenes. Sample
MW18-0l-1 contained acetone and chloroform. Sample MW2D-Dl-l
contained acetone and a variety of chlorinated hydrocarbons.
All surrogates met recovery criteria. The matrix
spike/matrix spike duplicate results were acceptable. The
recovery for trichloroethene exceeded QC limits in both the
MS and MSD.
SEMIVOLATILES:
All semivolatile fractions were extracted and analyzed within
holding time requirements. The only sample containing any
target compounds was MW15A01-l, in which bis (2-ethylhexyl)
and di-n-octyl phthalates were found. All surrogates met
recovery criteria. The matrix spike/matrix spike duplicate
results were acceptable.
I certify that this data package is in compliance with the
terms and conditions of the contra~t, both technically and
for completeness, for other than the· conditions detailed
above. Release of the data contained in this hardcopy data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
Note: This report was.
accountability in decreasing
paginated fcir reference and
numerical sequence.
)'_)J_o_~
Sarah A. Hubbard 10/29/90
Technical Reviewer
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEH,RTP Contract: /2-881-REVS
MW15A01-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: .,.2_.1 __
Matrix: ( soil/water) WATER Lab Sample ID: 374584
sample wt/vol: 5.0 (g/mL) Mk_ Lab File ID: CN074584A53
Level: (low/med) LOW Date Received: 10/18/90
't Moisture: not dee. Date Analyzed: 10/19/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) !,!!,/ I. Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---~-----Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ
67-64-1------~--Acetone 10 u
75-15-0---------carbon Disulfide 1 J
75-35-4---------1,1-Dichloroethene 11
75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 1 J
67-66-3---------Chloroform 1 J
107-06-2---:----1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10 u
71-55-6---------1,1,1-Trichloroethane 16
56-23-5---------carbon Tetrachloride l J
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane ·5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
79-01-6---------Trichloroethene 3 J
124-48-1--------Dibromochloromethane 5 u
79-oo-s----~----l,l,2-Trichloroethane 5 u
71-43-2---------Benzene 1 J
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
108-10-1--------4-Methyl-2-Pentanone 10 IJ
591-78-6--------2-Hexanone 10 IJ
127-18-4--------Tetrachloroethene 2 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5
108-90-7--------Chlorobenzene 1 J
100-41-4--------Ethylbenzene 2 J
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5
FORM I VOA 1/87 Rev.
,,, . lJ
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP Contract: 12-881-REVS
Lab Code: COMPU case No.: 21492 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 5.0 (g/mL) !il.,_ Lab File ID:
Level: (low/med) LOW Date Received:
EPA SAMPLE NO.
HW15A01-l
No.: 21
)74584
CN074584A5J
10/18/90 I t Moisture: not dee. Date. Analyzed: 10/19/90
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Column (pack/cap) CAP
Number TICs found: --1
CAS NUMBER COMPOUND NAME
Dilution Factor: ~l~-~o __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST.' CONC. Q =~============== ============================ ======== ===-========= =====
1. 124-19-6 NONANAL 2J.60 5.1 J
FORM I VOA-TIC 1/87 Rev.
21492 21 SAMPLE DATA SUMMARY 44
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-881-REVS MWlB-01-1
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: ( soil/water) WATER Lab sample ID: 374418
Sample wt/vol: 5.0 (g/mL) tu....._ Lab File ID: CN074418A53
Level: (low/med) LOW Date Received: 10/17/90
, Moisture: not dee. Date Analyzed: 10/19/90
Column: (pack/cap) CAP Dilution Factor: ~l~-~o __ _
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone 8 J 75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u
540-59-0--------1,2-Dichloroethene (total)_ 5 u
67-66-3---------Chloroform l J 107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u
71-55-6---------1,1,l-Trichloroethane 5 u
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-0l-S-----~cis-l,3-Dichloropropene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-s--~------1,1,2-Trichloroethane 5 u
71-43-2-----~---Benzene 5 u
75-25-2---------Bromoform 5 u
100-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
100-ee-J--------Toluene 5 u
108-90-7--------chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
21492 21 SAMPLE DATA SUMMARY 4.3
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VOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COHPUCHEM.RTP Contract: (2-88)-REVS
Lab code: COHPU Case No.: 21492
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
t Moisture: not dee.
5.0
LOW
(g/mL) Ml,_
SAS No.: SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
EPA SAMPLE NO.
MWlS-01-1
No.: 21
374418
CN074418A53
10/17/90
10/19/90
Column (pack/cap) CAP Dilution Factor: ~i~-~o __ _
Number TICs found: __a.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME · RT EST. CONC.. Q .
FORM I VOA-TIC 1/87 Rev.
?f4Q? ?f SQMPL~ DQTQ SLJMMQRY
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: /2-88)-REVS MW20-0l-l
Lab Code: COMPU Case No.: 21492 SAS No.: SOG No.: .2~1 __
Matrix: ( soil/water) WATER Lab Sample ID: J744J5
Sample wt/vol: 5.0 (g/mL) Ml.:_ Lab File ID: CN0744JSASJ
Level: ( low/med) LOW Date Received: 10/17/90
% Moisture: not dee. Date Analyzed: 10/19/90 \
Column: (pack/cap) CAP Dilution Factor: LO
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) U~/L Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---~-----Chloroethane 10 u 75-09-2---------Methylene Chloride 1 BJ 67-64-1---------Acetone 59 75-15-0---------carbon Disulfide 5 u 75-35-4---------1,l-Dichloroethene 2 J 75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 7
107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 4 J 56-23-5---------carbon Tetrachloride 5 u 108-05-4--------Vinyl Acetate 10 u 75-27-4---------Bromodichloromethane 5 u 78-87-5---------1,2-Dichloropropane 5 u 10061-01-5------cis-l,3-Dichloropropene 5 u 10061-02-6------Trans-l,3-Dichloropropene __ 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
75-25-2---------Bromotorm 5 u
1os-10-1--------4-Methyl-2-Pentanone 10 u 591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 1 J
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
l00-41-4-------7Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
? 1 4Q? ? 1 ,tlMPI ► naTtl ,11"1"1tlPV 4 I
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lE EPA SAMPLE tlO. VOLATILE ORGANICS ANALYSIS DATA-SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM,RTP ·contract: 12-88)-REVS MW20-0l-l
Lab Code: COMPU Case No.: 21492 SAS No. : SDG No.: 21
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) Ml,_
Level: (low/med) LOW
I Moisture: not dee.
Column (pack/cap) CAP
Number TICs found: _Q
CAS NUMBER COMPOUND NAME
Lab Sample ID: 374435
Lab File ID: CN0744:i5A53
Date Received: 10/17/90
Date Analyzed: 10/19/90
Dilution Factor: 1.0 -"-'--"----
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q . . ---.. , "'• ~ ., ... ===--=----------=========================~== ======== ------========: '=====
FORM I VOA-TIC 1/87 Rev ..
2 92 2 SA: L MMARY 4E
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: COMPUCHEM,RTP Contract: /2-88)-REVS
Lab Code: COMPU Case No.: 21492
Matrix: (soil/water) WATER
Sample wt/vol:
Level: (low/med)
5.0
LOW
(g/mL) H1,._
SAS No.: SDG
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
EPA SAMPLE NO.
MWlSAOl-lMS
No.: 21
374430
CN074430A53
lQOSL90
1009L90 I Moisture: not dee.
Column: (pack/cap) CAP Dilution Factor: l,O =~--
CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UGLL Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 2 BJ 67-64-1---------Acetone 10 u 75-15-o----~----carbon Disulfide 1 J 75-35-4--~------l,l-Dichloroethene . 5 u 75-34-3---------1,1-Dichloroethane 5 u 540-59-0--------1,2-Dichloroethene (total)_ 1 J 67-66-3---------Chloroform 1 J 107-06-2--------1,2-Dichloroethane 5 u 78-93-3---------2-Butanone 10 u 71-55-6---------1,1,1-Trichloroethane 17 56-23-5---------carbon Tetrachloride 2 J
108-05-4--------Vinyl Acetate 10 u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u 79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-oo-s---------1,1,2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
75-25-2---------Bromoform 5 u
1oa-10-1--------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene l J
79-34-s---------l,l,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 1 J
100-42-5--------Styrene 5 u
1330-20-7-------Total Xylenes 3 J
FORM I VOA 1/87 Rev.
21492 21 SAMPLE DAT~ SUMMARY 39
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VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS MW15A01-1MSD
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No, : ...,2,.1 __
Matrix: ( soil/water) WATER Lab Sample ID: )744)1
sample wt/vol: 5.0 (g/mL) Ml._. Lab File ID: CN0744JlA5J
Level: ( low/med) LOW Date Received: 10/18/90
t Moisture: not dee. Date Analyzed: 10/19/90
Column: (pack/cap) CAP Dilution Factor: 1.0
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) Y!dt!. Q
74-87-3---------Chloromethane 10 u 74-83-9---------Bromomethane 10 u 75-01-4---------Vinyl Chloride 10 u 75-00-3---------Chloroethane 10 u 75-09-2---------Methylene Chloride 1 BJ 67-64-1---------Acetone 10 u 75-15-o---------carbon Disulfide 5 u
75-35-4---------1,1-Dichloroethene 5 u 75-34-3---------1,1-Dichloroethane 5 u 540-59-0-----~--l,2-Dichloroethene (total)_ 5 u 67-66-3---------Chloroform 5 u
107-06-2--------1,2-Dichloroethane 5 u
78-93-3---------2-Butanone 10. u
71-55-6---------1,l,l-Trichloroethane 17
56-23-5---------carbon Tetrachloride 5 u
108-05-4--------Vinyl Acetate 10 . u
75-27-4---------Bromodichloromethane 5 u
78-87-5---------1,2-Dichloropropane 5 u
10061-01-5------cis-l,3-Dichloropropene 5 u
10061-02-6------Trans-l,3-Dichloropropene __ 5 u
79-01-6---------Trichloroethene 5 u
124-48-1--------Dibromochloromethane 5 u
79-00-5-----.----1, 1, 2-Trichloroethane 5 u
71-43-2---------Benzene 5 u
75-25-2---------Bromoform 5 u
1oa-10-1~-------4-Methyl-2-Pentanone 10 u
591-78-6--------2-Hexanone 10 u
127-18-4--------Tetrachloroethene 5 u
79-34-5---------1,1,2,2-Tetrachloroethane __ 5 u
108-88-3--------Toluene 5 u
108-90-7--------Chlorobenzene 5 u
100-41-4--------Ethylbenzene 5 u
100-42-5--------styrene 5 u
1330-20-7-------Total Xylenes 5 u
FORM I VOA 1/87 Rev.
? 1 dQ? ? 1 C::01•111::>I ,:: f'IOTO C::IIMMOPV
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
MW15A01-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: ( soil/water) WATER Lab Sample ID: 37459·4
Sample wt/vol: 1000 (g/mL) ML.. Lab File ID: GH074584A05
Level: (low/med) LOW Date Received: 10/18/90
' Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) ~
GPC Cleanup: (Y/N) Ii._ pH:
·Date Analyzed: 10/20/90
Dilution Factor: ~l~.O,._ __
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9--~---bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1-~-------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-0--.-------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1-~------l,2,4-Trichlorobenzene
91-20-3--------~Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88~74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
io u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I sv-1 1/87 Rev.
4 21 SAMPLE DATA SUMMARY
Q
37
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS MW15A01-l
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: (soil/water) WATER Lab Sample ID: 374584
Sample wt/vol: 1000 (g/mL) tu._ Lab File ID: GH074584A05
Level: ( low/med) LOW Date Received: 101'.181'.90
t Moisture: not dee. dee. Date Extracted: lQl'.l8L90
Extraction: (SepF/Cont/Sonc) g_pr
GPC Cleanup: (Y/N) li._ pH:
Date Analyzed: 101'.201'.90
Dilution Factor: 1.0 -~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) QGLL
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9----~---Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether __
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol __
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-0--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-.39-5--------Indeno ( 1, 2, 3-cd) Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from D1phenylam1ne
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10
3 J
10 u
10 u
10 u
10 u
10 u
10 u
FORM I sv-2 1/87 Rev.
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG
Matrix: (soil/water) WATER Lab Sample ID:
Sample wt/vol: 1000 (g/mL) Ml..._ Lab File ID:
Level: ( low/med) LOW Date Received:
t Moisture: not dee.· dee. Date Extracted:
EPA SAMPLE t;o.
MWl5AOl-l
No.: 21
374584
GH074584A05
10/18/90
10/18/90
Extraction: (SepF /Cont/Sonc)
(Y/N) H..._
§E_ff Date Analyzed: 10/20/90
GPC Cleanup: pH: Dilution Factor: ~l~-~o-~_
Number TICs found: ___..z.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. ====-====---==== ============================ ======:;;:= ============== 1. 134-62-3 BENZAMIDE, N,N-DIETHYL-3-MET 11.27 150
2. UNKNOWN 15.45 8.0
FORM I SV-TIC 1/87 Rev.
' 214.9-2 21 SAilP-LE DATA. SUMMARY-
Q
=====
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: C2-88l-REVS
MW18-0l-l
Lab Code: COMPU Case No. : 21492 SAS No.: SOG No.: 21
Matrix: (soil/water) WATER Lab Sample ID: 374418
Sample wt/vo~ :. 500 (g/mL) Ml.,_ Lab File ID: GH074418B05
Level: (low/med) LOW Date Received: 10/17/90
% Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) §.EH
GPC Cleanup: (Y/N) li.,_ pH:
Date Analyzed: 10/24/90
Dilution Factor: ~0~-~5~0 __
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-ss-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---~-----Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-4 7-4---------Hexachlorocyclop·entadiene __
88-06-2-------~-2,4,6-Trichlorophenol
95-95-4---------2,4,S-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
50 u
10 u
50 u
10 u
10 u
10 u
FORM I SV-1 1/87 Rev.
? f ? ? f 0 I ,:: V
Q
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MWlS-01-1 Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: (soil/water) WATER Lab Sample ID: 374418
Sample wt/vol: 500 (g/mL) tu.._ Lab File ID: GH074418B05
Level: (low/med) LOW Date Received: 10/17/90
' Moisture: not dee. dee. Date Extracted: 10/1~/90
Extraction: (SepF/Cont/Sonc) gu
GPC Cleanup: (Y/N) t:!..._ pH:
Date Analyzed: 10/24/90
Dilution Factor: 0.50 "-'-=--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
ioo-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
ss-01-e---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------oi-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-o-~------Pyrene
85-68-7-----~---Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------Di-n-Octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -cannot be separated from D1phenylam1ne
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
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10 u
10 u
10 u
10 u
20 u
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10 u
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10 u
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10 u
10 u
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FORM I SV-2 1/87 Rev.
?f ? ? f C: MJ:>
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lF EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
MW18-0l-l Lab Name: CQMPUCHEM,RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 21492_ SAS No.: SDG No.: _21 __
Lab Sample ID: ~J-'-7"-44,._1=8~---Matrix: (soil/water) WATER
Sample wt/vol: 500 (g/mL) M.l._ Lab File ID: GH074418B05
Level: ( low/med) LOW Date Received: 10/17/90
I Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) s.E.U Date Analyzed: 10/24/90
GPC Cleanup: (Y/N) H.._ pH: Dilution Factor: ~0~-~s~o __
CONCENTRATION UNITS: Number TICs found: __Q (ug/L or ug/Kg) UG/L
CAS NUMBER COMPOUND NAME RT EST. CONC. Q
FORM I SV-TIC 1/87 Rev.
21492 21 SAMPLE DATA SUMMARY 32
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS MW20-0l-l
Lab Code: COMPU case No.: 21492 SAS No.: SDG No.: 21
Matrix: (soil/water) WATER Lab Sample ID: )744)5
Sample wt/vol: 500 (g/mL) tll.c__ Lab File ID: GHQ744J5!;!QS
Level: ( low/med) LOW Date Received: 10/17/90
% Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) g_pr Date Analyzed: 10/24/90
GPC Cleanup: (Y/N) J:L_ pH: Dilution Factor: ~0~-~s~o __
CAS NO. COMPOUND CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
108-95-2--------Phenol
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-so-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine_
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-85-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-s2-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol .
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
10 u
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10 u
10 u
10 u
10 u
10 u
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10 u
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10 u
10 u
10 u
10 u
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FORM I SV-1 1/87 Rev.
49 S MP MA
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lC EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
MW20-0l-l
Lab Name: COMPUCHEM.RTP Contract: (2-88l-REVS
Lab Code: COMPU case No.: 21492 SAS No.: SDG No.: 21 ---
Matrix: (soil/water) WATER Lab Sample ID: ~3~7~44,.3""'5'-----
Sample wt/vol: 500 (g/mL) Ml.,_ Lab File ID: GH074435B05
Level: (low/med) LOW Date Received: 10/17/90
I Moisture: not dee. dee. Date Extracted: 10/18/90
Date Analyzed: 10/24/90
Dilution Factor: ~0~.s~o'--_
Extraction: (SepF/Cont/Sonc) s..E.Pf
GPC Cleanup: (Y/N) lf.._ pH:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-1--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluehe
84-66-2---------Diethylphthalate
7005-72-3-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1-----~--Hexachlorobenzene
87-86-5---------Pentachloropheno~
85-01-8---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129~00-0--------Pyrene
85-68-7----~----Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
210-01-9--------Chrysene
ll7-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-0--------oi-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -cannot be separated from D1phenylam1ne
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u
50 u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
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10 u
10 u
10 u
10 u
10 u
10 u
10 u
10 u
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FORM I SV-2 1/87 Rev.
,,. ,, ,, OM ♦ f'l TO /MM
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
MW20-0l-1 Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS
Lab Code: COMPU Case No.: 21492
Matrix: (soil/water) WATER
Sample wt/vol: 500 (g/mL) Ml,_
Level: (low/med) LOW
't Moisture: not dee. dee.
Extraction: (SepF/Cont/Sonc) s.E.ff
GPC Cleanup: (Y/N) Ii_ pH:
Number TICs found: ___Q.
CAS NUMBER COMPOUND NAME
SAS No.: SDG No.: 21
Lab Sample ID: 374435
Lab File ID: GH074435805
Date Received: 10/17/90
Date Extracted: 10/18/90
Date Analyzed: 10/24/90
Dilution Factor: ~0~ .. ~5~0 __
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
RT EST. CONC. Q
================ ============================ ======== ============= =====
FORM I SV-TIC 1/87 Rev.
?t T IIM V
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
MW18-0l-1MS Lab Name: COMPUCHEM.RTP Contract: (2-881-REVS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: (soil/water) WATER Lab sample ID: 374427
Sample wt/vol: 500 (g/mL} Ml.__ Lab File ID: G!:1074427B05
Level: ( low/med} LOW Date Received: 10/17/90
% Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF(Cont/Sonc} .§_E_P_E Date Analyzed: 10/24/90
GPC Cleanup: (Y/N} !!.___ pH: Dilution Factor: o.so ==--
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg} UG/L
lll-44-4--------bis(2-Chloroethyl}Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--~-----Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7-------~-2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl}Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-0imethylphenol
65-85-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy}Methane __
120-83-2--------2,4-0ichlorophenol
120-82-1--------1,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131-11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
Q
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10 u
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10 u
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10 u
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10 u
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10 u
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FORM I SV-1 1/87 Rev.
.... .... ",.. ... e'I JM OlJ
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SEMIVOLATILE ORGANICS ,ANALYSIS DATA SHEET EPA SAMPLE NO,
Lab Name: COMPUCHEM.RTP Contract: (2-88)-REVS MWlS-01-lMS
Lab Code: COMPU Case No.: 21492 SAS No.: SDG No.: 21
Matrix: (soil/water) WATER Lab Sample IO: 374427
Sample wt/vol: 500 (g/mL) MI.__ Lab File ID: GH074427805
Level: ( low/med) LOW Date Received: 10/17 /90
% Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) li.,_ pH:
gu Date Analyzed: 10/24/90
Dilution Factor: ~0~-~s~o __
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
99-09-2---------3-Nitroaniline
83-32-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121-14-2--------2,4-Dinitrotoluene
84-66-2---------Diethylphthalate
7005-72-3---.----4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-l~-------4,6-Dinitro-2-Methylphenol_
86-30-6---------N-Nitrosodiphenylamine (l)_
101-55-3--------4-Bromophenyl-phenylether __
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
ss-01-s---------Phenanthrene
120-12-7--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-00-o--------Pyrene
85-68-7---------Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7---~----bis(2-Ethylhexyl)Phthalate_
117-.84-0--------Di-n-Octyl Phthalate
205-99-2--------Be~zo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-32-8---------Benzo(a)Pyrene
193-39-5--------Indeno(l,2,3-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo(g,h,i)Perylene
(1) -Cannot be separated from Diphenylamine
50 u
10 u
50 u
50 u
10 u
10 u
10 u
10 u
10 u so u
50 u
10 u
10 u
10 u
50 u
10 u
10 u
10 u
10 u
10 u
10 u
20 u
10 u
10 u
10 u
10 u
10 u
10 u
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10 u
10 u
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FORM I sv-2 1/87 Rev.
,, f ,, ,, T /MM V
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS MW18-0l-1MSD
Lab code: COMPU Case No.: 21492 SAS No.: SOG No.: 21
Matrix: (soil/water) WATER Lab Sample ID: 374428
Sample wt/vol: 500 (g/mL) ~ Lab File ID: GH07442BB05
Level: ( low/med) LOW Date Received: 10/17/90
I Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) s..E.fr
GPC Cleanup: (Y/N) l:L_ pH:
Date Analyzed: 10/24/90
Dilution Factor: 0.50
CAS NO. COMPOUND
108-95-2--------Phenol
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
lll-44-4--------bis(2-Chloroethyl)Ether
95-57-8---------2-Chlorophenol
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
100-51-6--------Benzyl Alcohol
95-50-1---------1,2-Dichlorobenzene
95-48-7---------2-Methylphenol
39638-32-9------bis(2-Chloroisopropyl)Ether_
106-44-5--------4-Methylphenol
621-64-7--------N-Nitroso-Di-n-Propylamine __
67-72-1---------Hexachloroethane
98-95-3---------Nitrobenzene
78-59-1---------Isophorone
88-75-5---------2-Nitrophenol
105-67-9--------2,4-Dimethylphenol
65-as-o---------Benzoic Acid
lll-91-l--------bis(2-Chloroethoxy)Methane_
120-83-2--------2,4-Dichlorophenol
120-a2-1--------l,2,4-Trichlorobenzene
91-20-3---------Naphthalene
106-47-8--------4-Chloroaniline
87-68-3---------Hexachlorobutadiene
59-50-7---------4-Chloro-3-Methylphenol
91-57-6---------2-Methylnaphthalene
77-47-4---------Hexachlorocyclopentadiene __
88-06-2---------2,4,6-Trichlorophenol
95-95-4---------2,4,5-Trichlorophenol
91-58-7---------2-Chloronaphthalene
88-74-4---------2-Nitroaniline
131--11-3--------Dimethyl Phthalate
208-96-8--------Acenaphthylene
606-20-2--------2,6-Dinitrotoluene
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FORM I sv-1 1/87 Rev.
,.. ,.. ,.. _,.. ,.. ... -.. ..
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SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE t/0.
Lab Name: COMPUCHEM.RTP Contract: 12-88)-REVS MWlB-01-lMSD
Lab Code: CQMPU Case No.: 21492 SAS No.: SDG No.: 21 Matrix: (soil/water) WATER Lab Sample ID: 374428
Sample wt/vol: 500 (g/mL) Ill._ Lab File ID: GH074428B05
Level: (low/med) LOW Date Received: 10/17 /90
t Moisture: not dee. dee. Date Extracted: 10/18/90
Extraction: (SepF/Cont/Sonc) ~ Date Analyzed: 10/24/90
GPC Cleanup: (Y/N) li_ pH: Dilution Factor: ~0~.5~0.____
CAS NO, COMPOUND
99-09-2---------J-Nitroaniline
BJ-J2-9---------Acenaphthene
51-28-5---------2,4-Dinitrophenol
100-02-7--------4-Nitrophenol
132-64-9--------Dibenzofuran
121~14-2--------2,4-Dinitrotoluene
_84-66-2---------Diethylphthalate
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
7005-72-J-------4-Chlorophenyl-phenylether_
86-73-7---------Fluorene
100-01-6--------4-Nitroaniline
534-52-1--------4,6-Dinitro-2-Methylphenol_
86-J0-6---------N-Nitrosodiphenylamine (1) 101-55-3~-------4-Bromophenyl-phenylether-=
118-74-1--------Hexachlorobenzene
87-86-5---------Pentachlorophenol
ss-01-s---------Phenanthrene
120-12-1--------Anthracene
84-74-2---------Di-n-Butylphthalate
206-44-0--------Fluoranthene
129-oo-o~-------Pyrene
85-68-7----~----Butylbenzylphthalate
91-94-1---------3,3'-Dichlorobenzidine
56-55-3---------Benzo(a)Anthracene
218-01-9--------Chrysene
117-81-7--------bis(2-Ethylhexyl)Phthalate_
117-84-o--------Di-n-octyl Phthalate
205-99-2--------Benzo(b)Fluoranthene
207-08-9--------Benzo(k)Fluoranthene
50-J2-8---------Benzo(a)Pyrene
19J-J9-s--------Indeno(l,2,J-cd)Pyrene
53-70-3---------Dibenzo(a,h)Anthracene
191-24-2--------Benzo (g, h, i).Perylene
(1) -Cannot be separated from Diphenylam1ne
50 u
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FORM I SV-2 1/87 Rev.
21492 21
Q
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COMPUCHEM
lABC)pAJC>RIES, {NC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC27709 (919) 549~8263
INORGANICS CASE NARRATIVE SUMMARY
CASE# 24520 SDG# 039779
The above indicated SDG consisted of two (2) soil samples which were
received on August 10, 1990, intact and in good condition with the Chain of
Custody (COC) Records in order. The samples were analyzed, adhering to the
EPA 788 Statement of Work (SOW), for the Inorganic·Target Analyte List
(TAL) which consists of twenty-three (23) metals.
SAMPLE IDs:
The following customer IDs are associated with this SDG.
MW6-4S-l MW7-4S-l
The enclosed Cover Page reflects both SIRRINE Environmental
~nsultant's and CompuChem's sample Identifiers (CCNs).
QUALITY CONTROL:
All calibration verification standards and verification blanks were
within the EPA-CLP acceptance criteria.
The laboratory control sample and interference check samples met all
EPA established criteria.
The preparation blank met EPA requirements, with all elements being
determined below the Contract Required Detection Limit (CRDL), but
aluminum, barium, calcium, iron, and sodium were determined at
concentrations greater than their respective Instrument Detection Limits
( IDLs) .
The sample spike, CCN = 364120 (MW6-4S-1S) was outside the control
limits for antimony, arsenic (F), and selenium, therefore, all the
concentrations for these analytes were flagged with an "N" on all Form ls
and Form 5. The control limit for sample spike recoveries is 75 to 125% of
the amount added, unless the original sample concentration of analyte
exceeds the spike amount by a factor of four or more. In the latter case,
the analyte is not flagged if the recovery is beyond the control limits.
As required by the Statement of Work, antimony was post digestion
spiked and was recovered at 106.5%.
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CbMPUCHEM
IABoRATORJES, INC.
The sample duplicate, CCN = 364121 (MW6-4S-1D) was in control for all
analytes except cadmium, therefore, all concentrations for this one analyte
were flagged with a"*" on all Form ls and Form 6. The control limit for
duplicate determinations is+/-20% Relative Percent Difference (RPO) for
analyte concentrations greater than or equal to five times the CRDL in both
the original .and the duplicate solutions. If the analyte concentrat:1ons are
less than five times the CRDL, then+/-the CRDL will be the limit. The RPO
is not calculated if both the original and duplicate values fall below the
IDL.
MSAs were not required for the determination of any GFAAS element.
The serial dilution was performed on sample, CCN = 364106 (MW7-4S-l)
and the adjusted sample concentrations were within the control limits for
all analytes, therefore, no sample concentrations were flagged with an "E" I on Form ls and Form 9. The control limit for the serial dilution is that
the adjusted sample concentration for all analytes with values greater than
fifty (50) times its IDL in the original sample, must agree within 10% of
the original values. I
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Release of the data contained in this hard copy data package has been
authorized by the Laboratory Manager or his designee, as verified by the
following signature.
:B~iJ 0cJ«lL Bruce H. Rohrbach
Technical Reviewer
October 15, 1990
I Note: This report is paginated for reference and accountability.
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U. S,. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
% Solids:
LOW
77.1
MW6-4S-l Contract: 788 ------I
SAS No.: ___ SDG No.: 093779
Lab Sample ID: 364105
Date Received: 08/10/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
jCAS No. I Analyte IConcentrationjCI Q IM I
l4LY-YU-, Aluminum LJLUU p 1440-36-0 Antimony 9. 1 u N p /44U-J/j-L Arsenic l. U B N F 1440-39-3 Barium 187 p /44U-41-/ Bery11ium l. b p 1440-43-9 Cadmium 1. 3 • p 1440-IU-2 Ca1cium Jlb B p 1440-47-3 Chromium 6. 8 p /44U-4/j-4 CoDalt l /. l p 7440-50-8 Copper 14. 9 p /4JY-/j9-b Iron J!HlUO p 7439-92-1 Lead 10.6 F /4JY-Yo-4 Magnesium LJ4U p 1439-96-S Manqanese 670 p /4JY-Y/-b l".ercury .lJ u CV 7440-02-0 Nickel l O. l u p /440-UY-/ Potassium l j I U p
I /82-49-2 Selenium 2. 6 u WN F 1440-Ll-4 Silver L. l u p 7440-LJ-, Soaium LJL B p 7440-28-0 Thallium . ,2 u F l44U-oL-L Vanaaium 4U.L p 7440-60-6 Zinc 68.8 p· Cyaniae NR
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Color Before: BROWN Clarity Before: Texture: ME:DIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE l
FORM I -IN 7 /88
T kJ ,-, n ,-. ,-i, a. I T ,-. ,-. ,-. ,--.-. -.-. ----
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
M~trix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
78.4
Contract: 788 -'-'-----I MW7-4S-l
SAS No.: ___ SDG No.: 093779
Lab Sample ID: 364106
Date Received: 08/10/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
JCAS No. I Analyte I Concentration IC I Q JM I
742 -90-5 Aluminum 2630 p
144 -jb-U Antimonv t!. u N p 144 -38-L Arsenic . " B WN P' 1440-39-3 Barium lb t! p
1440-41-1 Berv,1ium j .1 p
1440-43-~ Cadmium l.j u • p 7440-70-2 Calcium 119 B p 144U-4 /-j Cnromium I. 4 p 7440-48-4 Cobalt 4 2. 6 p /44U-jU-8 Copper l / . I p
7439-8\i-6 Iron 48600 p /4j~-\iL-l Lead lL.4 F' 7439-95-4 Maanesium 2280 p /4j\i-\ib-j Manqanese 12 70 p
7439-97-b Mercurv . l j u CV 144U-02-U Nickel \i . 9 u p
1440-U~-I Potassium LjjU p
7 82-4\i-L Selenium .ol u WN F'
I 4U-LL-4 Silver L. U u p
7 .40-23-5 Sodium 230 B p /44U-Lt!-U Tna11ium . j J. u w P' 7440-62-Z Vanadium 43.8 p /44U-bb-b Zinc 8 4 . 4 p
Cvanide NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 2
FORM I -IN 7/88
' ... ' .. -.----• .. --
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Q)MPUCHEM
lABC:>fW'()RJES, 11\JC:. P.O. Box 12652 3308Chapel Hill/Ne+son Highway Research Triangle Park. NC 27709 ·[phone]
INORGANICS CASE NARRATIVE SUMMARY
CASE# 24520 SDG# 093775
I The above indicated SDG consisted of seventeen (17) soil samples which
were received on August 02, 04, and 09, 1990, intact and in good condition
with the Chain of Custody (COC) Records in order. Eleven samples were
physically received by CompuChem on August 04, 1990, but not entered into I the system until August 06, 1990 which became the official VTSR. The
samples were analyzed, adhering to the EPA 788 Statement of Work (SOW), for
the Inorganic Target Analyte List (TAL) which consists of twenty-three (23) I metals.
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SAMPLE IDs:
The following customer IDs are associate~ with this SDG.
MW15-2S-l MW15-4s-1· MW5-4S-l MW8-4S-l
MW9-4S-1 SBl0-1-1 SBl0-2-1 SBll-1-1
SBll-2-2 SB13-1-1 SB14-1-1 SB16-1-1
SB7-2-1 SB8-2-1
The enclosed Cover Page reflects both SIRRINE Environmental
Consultant's and CompuChem's sample Identifiers (CCNs).
MW8-4S-2
SBll-2-1
SB7-1-1
I QUALITY CONTROL:
All calibration verification standards and verification blanks were I within the EPA-CLP acceptance criteria.
The laboratory control sample and interference check samples met all
EPA established criteria.
I The preparation blank met EPA requirements, with all elements being
determined below the Contract Required Detection Limit (CRDL), but
I aluminum, calcium, iron, and zinc were determined at concentrations greater
than their respective Instrument Detection Limits (IDLs).
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CDMPUCHEM
IABOIWORJES, INC.
The sample spike, CCN = 361466 (S916-1-1S) was outside the control
limits for selenium, therefore, all the concentrations for this analyte
were flagged with an "N" on all Form ls and Form 5. The control limit for
sample spike recoveries is 75 to 125% of the amount added, unless the
original sample concentration of analyte exceeds the spike amount by a
factor of four or more. In the latter case, the analyte is not flagged if
the recovery is beyond the control limits.
No post digestion spikes were required.
The sample duplicate, CCN = 361467 (S916-1-1D) was in control for all
analytes, therefore, no concentrations were flagged with a"*" on Form ls
and Form 6. The control limit for duplicate determinations is+/-20%
Relative Percent Difference (RPD) for analyte concentrations greater than
or equal to five times the CRDL in both the original and the duplicate
solutions. If the analyte concentrations are less than five times the CRDL,
then+/-the CRDL will be the limit. The RPD is not calculated if both the
original and duplicate values fall below the IDL.
MSAs were required for the determination of lead for the following
samples: MW15-2S-l, MW15-4S-1, MWB-4S-2, MW9-4S-l, and SB14-1-l. All MSAs
displayed correlation coefficients greater than 0.995, thus all MSA results
on Form ls were flagged with an "S".
The serial dilution was performed on sample, CCN = 361465 (SBB-2-1-1)
.1d the adjusted sample concentrations were within the control limits for
all analytes except zinc, therefore, all sample concentrations for this
analyte were flagged with an "E" on Form ls and Form 9. Also, a statement
indicating this fact is found on the Cover Page. The control limit for the
serial dilution is that the adjusted sample concentration for all analytes
with values 9reater than fifty (50) times its IDL in the original sample,
must agree within 10% of the original values.
Release of the data contained in this hard copy data package has been
authorized by the Laboratory Manager or his designee, as verified by the
following signature.
]vJJWJL
Bruce H. Rohrbach
Technical Reviewer
October 16, 1990
Note: This report is paginated for reference and accountability.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab ·Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1s Solids:
LOW
90.0
Contract: 788 ------I SB16-l-l
SAS No. : SDG No.: 093775
Lab Sample ID: 362495
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-90~5 Alum1num . 687 p
/44U-.lo-O Antimonv I. 8 u p
7440-38-L Arsenic .63 B F
1440-.l9-.l Bari um l. 8 B p
7440-41-1 Bervllium .LL u p
1440-4.l-9 Cadmium 1.1 u p
7440-iU-L Calcium 190 B p
1440-41-3 Chromium l. 3 u p
·7440-48-4 Cobalt .89 u p
1440 ·o0-8 Conner l. 8 u P·
7439 ·o~ ·o Iron 260 p
l4.l9-92-l Lead .61 B F
7439-95-4 Maonesium 20.0 u p
l4.l9-9o-, Manoanese 3. 4 p
7439-97-o Mercurv .11 u CV
7440-02-0 Nicl<e1 8 . 7 u p
/44U-U9-I Potassium 601 u p
7782-49-2 Se7:enium .44 u WN F
/44U-LL-4 Silver l. 8 u p
74 40-2 3-5 Soai um 100 u p
14•u-~o-U Tnallium .44 u F
7440-62-2 Vanadium 1.8 B • p
1440-oo-o Zinc L. 0 B E p
Cvanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: COLORLESS Clarity After: Artifacts:
Comments:
FORM l -PAGE 14
FORM I -IN 7/88
9
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
M~trix (soil/water): SOIL
Level (low/med):
i Solids:
LOW
67.7
Contract: 788 ------I SB8-2-l
SAS No.: ---SDG No.: 093775
Lab Sample ID: 361465
Date Received: 08/02/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/QLY-YU-o Aluminum 29000 p
74Q0-36-0 Antimonv l U . .l u p
744U-.ltl-L Arsenic .59 u F
7440-39-3 Barium jj/ p
/44U-Ql-l Bervllium 2.6 p
7440-43-9 Caamium l. 5 u p
/Q4U-IU-L Calcium 204 B p
7440-47-3 Cnromium 11. 2 p
744U-4tl-4 Cobalt 40. 7 p
7440 ·oO -8 Conner 2 0. 0 p
7439-tlY-b Iron 59700 p
7439-92-1 Lean 2 o. 7 F
/Qo~-Yo-Q Maanesium 6110 p
7439-96-5 Manaanese . 1810 p
7439-Yl-b Mercurv .15 u CV
7440-02-0 Nu:lie·r 11 . o u p
/44U-U9-/ Potassium 6110 p
7782-49-L Selenium 3.0 u WN F
/44U-2L-Q Silver 2 . q u p
7440-23-5 Soa1um 16] B p
l4QU-Ltl-O Thallium .09 u w F
7440-62-L Vanadium 68. 7 p
74Q0-66-6 Zinc lLO E p
Cvanide NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 17
FORM I -IN 7/88
; 1. .. ' .-..... ---.-.... ---.--. ---------...... ----
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.:
Matrix (soil/water): SOIL
L~vcl (low/med):
1-Sol ids:
LOW
81. 8
24520
MW5-4S-l Contract: 788 ------I
SAS No.: ---SDG No.: 093775
Lab-Sample ID: 361469
Date Received: 08/02/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. Analyte jConcentrat'ionjCI Q IM I
7429-:iu-5 Aluminum 31200 p /44U-.Jb-U Antimony y. u B p 7440-38-2 Arsenic · 2. 4 u F /44U-.JY-.J Barium oL. L p 7440-41-7 Beryllium • j 5 B p 7440-43-9 Cadmium 1. '-u p /44U-7U-2 Calcium 73. 0 B p 144U-41-.J Cnromium lLo p /44U-48-4 Cobalt 5. 5 B p 144U-~U-tl Coooer I l . L p /4.l':1-89-6 Iron 83700 p 14.JY-YL-l Leaa .l.4 F 1439-9,-4 Maqnesium ~uz B p 14.JY-Yb-~ Manganese l ti'-p 14.lY-97-6 Mercury .12 u CV /44U-UL-U NicKel I .l . .l p 7440-09-7 Potassium 728 u p I /tlL-4Y-L Selenium L. 4 u WN F 7440-22'-4 Silver 2. 0 u p /44U-L.l-o soaium 111 B p 7440-28-0 Tha.L1ium . 4 9 u w F 7440-t,2-2 vanadium 20Y p 144U-bb-b Zinc L~.b E p
Cyanide NR
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Color Before: RED Clarity Before: Texture: MEDIUM '----"----
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 3
FORM I -IN 7/88
au ,a. w rm.-• 1 1
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 ------I SB7-l-l I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 093775.
Matrix (soil/water): SOIL
Level (low/med):
t Solids:
LOW
79.5
Lab Sample ID: 362497
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-90-5 Aluminum 51400 p
1440-36-0 Antimony 8. 8 u p
7440-38-L Arsenic l. 6 B w F /440-39-3 Bari um 54. 6 p
7440-41-1 Berv111um L6 p
/440-43-9 Cadmium 1. 3 u p
1440-70-2 Calcium 142 B p
1440-47-3 Chromium 2 Ub p
1440-d~ ·4 Cobalt 9.8 B p
1440-50-8 Coooer lu~ p
7439-89-o Iron / 102000 p
/439-92-1 Lead 12.2 F
7439-9~-4 Maqnesium 923 B p
1439-~o-5 Manaanese 394 p
74.3Y-Y7-o Mercury . Hi CV
1440-02-0 Nickel 112 p
7440-09-1 Potassium 749 u p
I /82-49-2 Selenium 1.0 u WN F
/q4U-22-4 Silver 2.0 u p
/440-23-5 Sodium 525 B p
1440-28-U Thallium • Su u w F
1440-62-2 vanaaium 190 p
1440-66-6 Zinc 80.6 E p
Cvaniae "NR
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
,ORM l -PAGE 15
,ORM I -IN 7/88
TNnR~QNT~~ CQSE 093775
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.:
Matrix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
78.0
24520
Contract: 788 ------I SB7-2-l
SAS No.: ---SDG No.: 093775
Lab Sample ID: 362499
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight):, MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/4L~-~U-~ Aluminum 71100 p
7440-jf:>-0 Antimonv 9.0 u p
7440-jtl-L Arsenic 2. 6 u w I' /44U-39-3 Barium 182 p
7440-41-7 Bervllium 3. 4 p
/44U-43-9 Cadmium l.j u p
7440-70-2 Calcium 345 B p
/44U-4 /-j cnromium 46Z p
7440-48-4 Cobalt 119 p
/44U-~U-t! Conner l / o p
7439-89-6 Iron 112000 p
7439-92-1 Leao 12. J F
74j~-9~-4 Maonesium 2150 p
7439-90-S Manaanese 1100 p
7439-~/-b Mercurv . 13 u CV
7440-02-0 Ni clie1 2bJ p
7440 ·vo I Potassium 763 u p
178,-49-2 Selenium 2.b u WN F
7440-LL-4 Silver 2. 1 u p
7440-23-5 SOdium 815 B p
7440-Ltl-U Tnallium . 51 u w F
7440-6:Z-Z vanactium 208 p
/44U-bb-b Zinc 60.b E p
Cvanide NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After:· Artifacts:
Comments:
FORM 1 -PAGE 16
FORM I -IN 7/88
'r 1.1.-,,-. •• -.• -.1.1 "P .-..-.-..-..-,-,"'";l,,'"'I,~---
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
83.9
SBl0-1-1 Contract: 788 ------I
SAS No.: SDG No.:'093775
Lab Sample ID: 362500
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte /Concentration/Cl Q IM I
7429-'!U-5 Aluminum 13400 p 7440-30-0 Antimony l:j. j u p /44U-J8-2 Arsenic /. • j B F 7440-39-,3 Bari um 23.5 B p /44U-4l-/ Bervu.ium ' ./.b B p 7440-43-9 Cadmium l. 2 u p /440-70-2 Calcium ~4.:, B p 14 4 0-4 1-3 Chromium 39.2 p /44U-48-4 Cooa1t :, • j B p 1440-:,u-e Cooner 11. 0 p 7439-89-6 Iron 248uu p /43'1-'l/.-l Lead 4 . I F 7439-95-4 Maqnesium 195 B p /4J'i-'ib-o Manqanese l .l /. p 7439-97-6 Mercury . 12 u CV 7440-02-0 Nickel 'I . .l u p /44U-09-i Potassium / u '! u p 7782-49-2 Selenium .48 u WN F /44U-i/.-4 Silver l . '! u p 7440-23-5 Sodium 108 u p 1440-21:l-0 Thallium • 4 8 u F /440-62-2 Vanadium 4 2. 2 p 7440-66-o Zinc 14. U E p cvanide NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 7
FORM I -IN 7/88
1 .·1
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
M~trix (soil/water): SOIL
L~vel (low/med):
i Soli9s:
LOW
89.8
Contract: 7.88 ~-----I SBl0-2-1
SAS No.: ---SOG No.: 093775
Lab Sample ID: 362504
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry .weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-90-~ Aluminum 5420 p
7440-36-0 Antimony ./ . 8 u p
744U oo-2 Arsenic . 79 B P'
7440-39-J Barium 11 . 4 B p
7440-41-/ Bervllium . 2 2 u p
/44U-4J-Y Cadmium l. 1 u p
7440-70-2 Ca1cium 36. 0 B p
/44U-41-3 cnromium y. ~ p
7440-48-4 Cohalt 10.0 B p
/44U-~u-tl Cooner 5. l B p·
74 39-89-6 Iron 7890 p
/4JY-Y2-1 Lead l. 4 w f 7439-95-4 Maonesium 71. 8 B p
1439-96-~ Manaanese 123 p
7439-Y/-b Mercurv . 11 u CV
7440-02-0 Niclce1 8. 7 u p
/44U-UY-/ Potassium 653 u p
17t!L-49-2 Selenium .. 4 ~ u WN f 7440-22-4 Silver l. 8 u p
7440-ZJ-5 soaium 106 B p·
/44U-2tl-U Tnallium • 4 5 u w f
7440-62-2 Vanaif1um 12. 2 p
/44U-bb-b Zinc 7. 9 E p
Cvanide NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: COLORLESS Clarity After: Artifacts:
Comments:
fORM l -PAGE 8
fORM I -IN 7/88
\ t.. .. ' •·------. . :. ----. --· ---.-. .-. ---.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case l'!O-: 24520
M3trix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
81. 8
Contract: 788 --'-----I SBll-1-1
SAS No.: ---SDG No.: 093775
Lab Sample ID: 362507
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
1429-90-5 Aluminum 149uu p·
/440-Jb-0 Antimony 8.6 u p
/440-lA -L Arsenic '1.1 B F /440-39-3 Barium 34. 0 B p
/440-41-7 Berv111um . 30 B p
7440-43-9 Cadmium 1. 2 u p
/440-70-2 Calcium 668 B p
1440-41-3 Chromium JU.4 p
/440-48-4 Cobalt 1. 8 B p
7440-50-8 Copper 4. 9 B p
/439-89-6 Iron 10100 p
I 09-92-1 Lead 9. 3 P"
/439-95-4 Maqnes1um 4 71 B p
1439-96-5 Manoanese 41. 5 · p
/439-97-6 Mercury . 1 L u CV
/ 4 40-02-0 Nickel 9.5 u p
,40-09-7 /4 .Potassium 728 u p
/ itl2-49-2 Selenium .49 u WN F /440-22-4 Silver 2. 0 u p
/440-23-5 Sodium 11 7 B p
1440-28-0 Thallium . 4 9 u w P"
/440-62-2 Vanadium 2 3. 3 p
/4'10-66-6 Zinc 18. 5 E p
Cyaniae NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 9
FORM I -IN 7/88
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
MLltrix (soil/water): SOIL
L0vel (low/med):
I Solids:
LOW
81. 7
Contract: 788 ..c..:c...:... ___ _ I SBll-2-1
SAS No.: ---SDG No.: 093775
Lab Sample ID: 362509
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
JCAS No. I Analyte I Concentration IC I Q IM I
7429-90-5 Aluminum 14700 p
744U-jb-U Antimony 8.6 u p
7440-38:...z Arsenic . 77 B F
744U-j':/-j Barium 31. 0 B p
7440-41-7 Bervllium • ]q B p
7440-43-':I Caamium 1. 2 u p
14 4 U-I 0-2 Calcium TlrS B p
7440-47-3 Chromium l 7. 1 p
7440-48-4 Cobalt 1. 2 B p
7440-~0-8 Copper 3. 3 B p
7439-89-6 Iron 9030 p
/4j':1-':ll-l Leaa 12. 4 F
7439-95-4 Maonesium J3 3 B p
/4j':l-':lb-~ Manoanese 19. 2 p
7439-97-6 Mercurv . lZ u CV
1440-02-0 Nickel 9.5 u p
7440-09-7 Potassium 729 u p
· 7782-49-2 Selenium . 4<, u WN F
7440-22-4 Silver '. 0 u p
7440-23-5 Sodium 131 B p
7440-28-u Tna11ium .49 u F
7440-62-2 Vanadium Ll".2 p
744U-bb-b Zinc 12. 7 E p
Cvan1de NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: COLORLESS Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 10
FORM I -IN 7/88
1 ~
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No. :
Matrix (soil/water): SOIL
L~vel (low/med):
1 Solids:
LOW
84.0
24520
.contract: 788 ------I SBll-2-2
SAS No.: ---SDG No.: 093775
Lab Sample ID: 362512
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
fCAS No. I Analyte fConcentrationfCI Q IM I
1qL9-90-5 Aluminum 11200 p
1440-36-0 Antimony 8. 3 u p
/Q40-38-2 Arsenic .48 u F
1440-39-3 Barium 4 4. 6 B p
/440-41-7 Bery1lium .48 B p
1440-43-9 Cadmium 1. 2 u p
7440-70-2 Calcium 169 B p
1440-47-3 Chromium 11. 9 p
1440-48-4 Cobalt 2 .1 B p
/4Q0-50-8 Cooner 2.7 B p
/ 4 ,-c,-6 Iron 9040 p
14 19-92-1 Lead 6. 6 · F
74 1',-9~-4 Maonesium 614 B p
I 4 19-90-5 Manqanese 67.6 p ,. 19-97-6 Mercury . 12 u CV
14 10-02-0 Nickel 9.3 u p
IQ40-09-7 Potassium 709 u p
I 182-49-2 Selenium .48 u WN F
/440-22-4 Silver 1. 9 u p
1440-23-5 Sodium 118 B p
1440-28-0 Thallium .48 u F
/Q40-62-2 Vanadium 10.4 B p
1440-66-6 Zinc 20.7 E p
Cyanide NR
I
Color Before: RED ;:.;.;:;.;:;__ __ Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 11
FORM I -IN 7/88
" .-.
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U.S. EPA -CLP
1 CLIENT SAI1PLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
L~vel (low/med):
1 Solids:
LOW
80.0
Contract: 788 ------I 5813-1-1
SAS No.: ---SDG No.: 093775
Lab Sample ID: 362513
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-90-5 A.1 um1 num 16luu p
7440-,o-O Antimonv 8 . 8 u p
7440-38-2 Arsenic 1.1 B I'
/440-39-j Barium 19. 3 B p
7440-41-7 BervTiium . 82 B p
/440-43-9 Cadmium l. L u p
7440-IU-2 Calcium 146 B p
1440-41-J cnromium U.9 p
7440-48-4 Cobalt 5. 2 B p
7440-:,u-8 Cooner 8. 6 p
7439-89-b Iron 33700 p
7439-92-1 Lead 4 . 7 I'
143':i-9:>-4 Maonesium 116 B p
7439-96-o Manaanese n.o p
7439-91-b Mercurv .12 u CV
1440-0L-0 Nickel 9. 8 u p
7440-09-7 Potassium 744 u p
178L-49-l Selenium . ::,o u WN F
7440-LL-4 Silver 2. 0 u p
7440-23-S Sodium 115 B p
/440-LB-O Tnallium . so u F
7440-62-2 Vanaaium 42.3 p
1440-66-6 Zinc 19.l E p
Cvanide NR
I
.Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 12
FORM I -IN 7/88
T .l.l•"'\r""l,.-..-i,1.1 T--.-..-.--.-,._...,. __ _ .....
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
90.0
Contract: 788 -----'---'-----I SB14-l-l
SA S No.: SDG No.: 093775
Lab Sample ID: 362514
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
l4L':i-";Ju-o A.lum1num 25luu p
7440-36-0 Antimonv 7.8 u p
/44U-38-L Arsenic 2. ':i l"
7440-39-3 Barium 28. 3 B p
744U-41-I Be rvl1 i um . 30 B p
7440-43-':i Cadmium 1.1 u p
1440-10-2 Caicium 208 B p
7440-47-3 Cnromium 28.5 p
1440-48-4 col:iait 2.0 B p
7440-50-8 Coooer 9. 4 p
/4j':J-B':i-o Iron L2o00 p
7439-92-1 Lead 11. 8 s l" 143':i-':io-4 Maanesium 300 B p
7439-96-5 Manqanese 78.8 p
l4j':i-':i 1-0 Mercurv .13 CV
7440-02-u Nickel 8. 7 u p
74 4 0-09-7 Potassium 061 u p
I IBL-4':i-L Selenium 2.L u WN f
7440-22-4 Si1ver 1. 8 u p
7440-L3-o Sodium 1 O':i B ·p
7440-28-0 Thallium . 4·4 u f
144U-oL-2 Vanadium 4 3. I p
7440-66-6 Zinc 24.1 E p
Cvanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 13
l"ORM I -IN 7/88
0.0RGA f,.cs CAS 28
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
71. 7
MWB-4S-l
Contract: ~7~8~8:_ __ _ I
SAS No. : SDG No.: 093775
Lab Sample ID: 362515
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte jConcentrationlCI Q IM I
7429-90-5 Aluminum 4TIOD p
744U-jb-U Antimony 16. 3 B p
7440-38-2 Arsenic 4.L B F
744U-39-j Barium 3 2. 1 B p
7440-41-7 Beryllium 4.L p
7440-43-9 Cadmium 1. 4 u p
7440-70-2 Calcium 41) .-1 B p
7440-41-j Chromium 376 p
7440-48-4 Cobalt 11. 4 B p
144U-,U-!l Conner 123 p
7439-89-6 Iron 118000 p
/4j9-<;L-l Lead 5. 0 F
7439-95-4 Maonesium 1200 B p
7439-90-, Manqanese . 197 p
7439-97-6 Mercury .14 u CV
144U-UL-U NicKel 83.2 p
7440-09-7 Potassium 1rN u p
77!lL-4<;-L Selenium . 56 u WN F
7440-22-4 Silver 2. 2 u p
744U-<!j-, Sodium 139. B p
7440-28-0 Thallium .56 u w F
7440-62-2 Vanadium 21>4 p
7440-66-b Zinc 5 3. ff E p
Cyanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 4
FORM I -IN 7/88
71
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1. Solids:
LOW
71. 5
Contract: 788 -=-=------
SA S No.:
I MW8-4S-2
SDG No.: 093775
Lab Sample ID: 362518
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/429-90-5 Aluminum 00400 p
/440-36-u Antimony 9. 8 u p
/440-38-2 Arsenic 2. 8 B I' /440-39-.J Barium 4 3. 1 B p
/440-41-7 Bervllium 2. 7 p
1440-4.J-9 Cadmium 1. 4 u p
/440-70-2 · Calcium 69.l B p
7440-47-3 Chromium 196 p
/440-48-4 CoOalt 9.5 B p
74 IU-50-8 Conner 89.2 p
/4 j9-89-6 Iron ~4400 p
74 ,9-9L-l Lead 6 .1 s I' /4 j9-9 5-4 Maonesium 1590 p
74 ,9-96-5 Manqanese 192 p
/4 j9-97-6 Mercurv . 14 u CV
74qQ-02-o Nickel 92.6 p
/440-09-7 Potassium 832 u p
I t<>L-49-2 Selenium 2.8 u WN F
/440-22-4 Silver 2.2 u p
/440-23-5 Sodium 126 u p
7440-~8-U Thallium .56 u F
/440-62-2 Vanadium 182 p
/440-66-6 Zinc 47.9 E p
Cvanide NR
I
Color Before: RED ==----Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 5
FORM I -IN 7/88
INORG NIC5 CRSE 093775
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U.S. EPA -CLP
l CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1. Solids:
LOW
69.5
Contract: 788 ------I MW9-4S-l
SAS No.: ---SDG No.: 093775
Lab Sample ID: 363243
Date Received: 08/08/90
Concentration.Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. Analyte I Concentration IC I Q IM I
7TI9-90-5 ATuminum 766uu p
7440-36-0 Antimonv 10.1 u p
7440-38-2 Arsenic 2.9 u F T4-40-39-3 Bari um 256 p
7440-41-7 Bervllium 1. 9 p
7440-43-9 Cadmium 1. 4 u p
iTTIT-7IT-7: CaTcium 121 B p
7440-47-3 Chromium snA p
iTT0-48-4 ConaTt 90.8 p
7440-50-8 Conner 214 p
mg_: e<r ..:-5 Iron 120000 p
7439-92-1 Lead 6. 8 s I' mg_g-5_4 Maqnesium 1550 p
7439-96-5 Manqanese 894 p
m9-<TT-o Mercurv . 14 u CV
7440-02-0 Nickel 382 p
/41fIT-lf9°-7 Potassium 8:,b u p
7T82-49-2 Selenium 2.9 u WN F
7440-22-4 Silver 2.3 u p
7440-23-5 Sodium 181 B p
7440-28-0 Thallium .58 u F
iTT0-62-2 Vanadium 257 p
7440-66-6 Zinc 56.6 E p
Cvanirte NR
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I
Color Before: RED ==----Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 6
FORM I -IN 7/88
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
89.9
Contract: 788 ------I MW15-2S-l
SAS No.: SDG No.: 093775
Lab Sample ID: 363568
Date Received: 08/09/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. Analyte IConcentrationlCI Q IM I
/4,!'i-'iU-~ Aluminum 4bLU p
7440-36-0 Antimony 7.8 u p
1440-J~-,! Arsenic .44 u F 144U-39-J Barium Z.9 B p
7440-41-7 Bervllium . j 4 B p
144U-4j-~ Cadmium 1.1 u p
1440-IU-L Calcium JJ.8 B p
144U-47-J Chromium 12.2 p
7400-,-4~-4 Cooa1t l. b B p
/44U-~U-8 Coooer 7. 6 p
7439-8:1-6 Iron l'iUUU p
143~-'92-l Lead 6.8 s r /4j.'i-'i~-4 Magnesium LB.B B p
7439-96-~ Manqanese 2 3. 4 p
14J'i-'i 1-b Mercury .11 u CV 7440-02-0 Nickel 8.7 u p
/44U-U'i-/ Potassium bbL u p -7782-49-2 Selenium . 4 4 u WN F /44U-LL-4 Silver l.B u p
7440-23-5 Sodium 101 ·U p
/44U-l8-U Tna11ium • 4 4 u F 7440-62-2 vanadium 2J.8 p
144U-bb-b zinc ~.U E p
Cvanide NR
I
.Col.or Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 1
FORM I -IN 7/88
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
i Solids:
LOW
80.6
MW15-4S-l
Contract: _7~8~8 ___ _ I
SAS No.: SDG No.: 093775
Lab Sample ID: 363570
Date Received: 08/09/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
JCAS No. I Analyte JConcentrationJCI Q IM I
142Y-YU-~ Aluminum 18200 p
7440-36-0 Antimony 8 . 7 u p
744U-38-l Arsenic • ',1) u f
7440-39-3 Barium 17. 3 B p
144U-4l-l Beryllium .94 B p
7440-43-9 Cadmium 1. 2 u p
7440-70-2 Calcium 79.S B p
7440-47-3 Chromium 24 .1 p
7440-48-4 Cobalt 6. 5 B p
7440-50-8 Conner 18.2 p
74JY-8Y-o Iron SD 8 D IT p
7439-92-1 Lead 5. 8 s f
74JY-9~-4 Maonesium -STir B p
7439-96-5 Manganese 39. 4 p
74JY-91-o Mercury .TL u CV
7440-02-0 NicKel 9. 7 u p
744U-09-7 Potassium T'l8 u p
7782-49-2 Selenium . 50 u WN r
144U-ll-4 Silver 2 .-IT u p
7440-23-5 Sodium 145 B p
144U-28-U Thallium .so u f
7440-62-2 Vanadium 111 p
7440-oo-6 Zinc 22.7 E p
Cyaniae NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
rORM l -PAGE 2
P-ORM I -IN 7/88
' J
T .&.Ir. -..-.a.a,..,-.~ ,-..r.i:""r-.~r,..,.;1-,c-
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,._;;_ t.,,.. ...... d.
WMPUCHEM
~C>RlES, INC. P.O. Box 12652 3308 Chapel Hill/ Net son Highway Research Triangle Park, NC 27709 [phone]
INORGANIC CASE SUMMARY NARRATIVE
CASE# 24520 SDG# 209373
CONTRACT# 788
SAMPLE ID's: MW13-7S-l, MW14-2S-l, MW16-2S-l, MW2A-6S-l,
SBl-1-1, SBl-2-1, SB12-l-l, SB2-l-l, SB2-2-l, SB3-l-l,
SB3-l-l, SB3-2-l, SB4-l-l, SB4-2-l, SB5-l-l,
SB5-2-l, SB6-l-l, SB6-2-l, SB8-l-l, SB9-l-l, SB9-2-l
This SDG consisted of twenty soil samples to be
analyzed for the Inorganic Target Analyte Lists (TAL)
metals. The samples were received intact on July 21 thru
August 1, 1990 with Chain of Custody (COC) Records in
order. The enclosed cover page reflects both Sirrine
Enviromental and CompuChem sample identifiers.
The associated quality control sample spike, MW16-2S-
1S, was outside of the control limits for antimony,
selenium, therefore these values were flagged with an 'N' on
the Form i's and the Form 5. The control limits for the
spike recoveries are 75-125%, unless the original sample
concentration exceeds the amount of spike added by a factor
of four or more, in this case the value is not flagged even
if the per·cent recovery is outside of the control limits.
The associated quality control duplicate sample, MW16-
2S-1D, was not within the control limits· for aluminum, iron,
and lead (F). The control limits for comparison of the
duplicate sample with the original sample are +/-20
Relative Percent Difference (RPD) for analytes with
concentrations greater than or e911al to five times the
Contract Required Detection Limit (CRDL) in both the
original and duplicate samples, and +/-CRDL if either the
original or duplicate value is less than five times the
CRDL. The RPD is not calculated if both the ori~inal and
duplicate values fall below the Instrument Detection Limit
( IDL) •
The concentration of arsenic was determined by Method of
Standard Addition (MSA) in samples MW16-2S-l. These values
were flagged with an 'S'on the Form l's if the correlation
coefficient was greater than 0.995. The values were flagged
with a'+' on the Form l's if the correlation coefficient
was less than 0.995.
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11
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COMPUCHEM
lABC)~C)RJES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC27709 [phone]
A serial dilution was performed on sample MW13-7S-1L.
The adjusted sample concentration of calcium was not within
10% of its original value, therefore the data were flagged
with an 'E' on the Form l's and the Form 9. The adjusted
sample concentrations for all other analytes with
concentrations greater than fifty times the IDL in the
original sample, were within 10% of their original values.
Release of the data contain.ed in this hard copy data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature.
chnical Reviewer
September 15, 1990
Note: This report is paginated for reference and
accountability.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
81. 3
Contract: 788 ------I MW13-7S-l
SAS No.: SDG No.: 209373
Lab Sample ID: 358144
Date Received: 07/21/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
14~,:,-90-~ Aluminum L3100 E• p
7440-36-0 Antimonv !l. b u N p
1440-38-I Arsenic .49 0 F
7440-39-3 Barium . 1,:, 4 E p
/440-41-7 Bervllium l. 4 p
1440-43-9 Cadmium 1. z u p
7440-70-2 Calcium 5,, B p
/440-47-3 Chromium 9. 4 p
/ 4 4 0,-4 8-4 Cobalt 15.6 p
14•11-i;n-a Conner 14. j p
7439-89-6 Iron SjUUU E• p
/439-92-1 Lead 9. L • F
7439-95-4 Maqnesium jObU p
/439-96-5 Manaanese b8o E p
7439-97-6 Mercurv .12 u CV
1440-02-0 Nic:keT 11. 9 p
/440-09-7 Potassiu·m LU4U p
7782-49-2 Selenium 2. 5 u WN F
7440-22-4 Silver L.U u p
1440-23-5 Sodium 190 B p
7440-28-0 Thallium . 4,:, u w F
7440-62-2 Vanadium 50.9 p
/440-66-6 Zinc / U. 4 p
cvan1de NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 1
fORM I -IN 7 /8,8
INORGANICS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
L,Jh. N.ime: COMPUCHEM LABORATORIES
Lob Code: COMPU Case No.: 24520
11.,trix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
76.7
Contract: 788 ------I MW14-2S-l
SAS No.: SDG No.: 209373
Lab Sample ID: 358149
Date Received: 07/21/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-'1U-5 Aluminum 433uu E* p
/44U-,o-U Ant1monv 9.u u N p
7440-38-Z Arsenic Z. 6 u w I'" 7440-H-j Barium 104 E p
144U-41-I Bervll1um . 9U B p
7440-43-9 Cadmium l. 3 u p
/44U-/U-L Ca1c1um I, . I B p
7440-47-j Cnrom1um 2Z. 3 p
7440-48-4 Cobalt 4. J B p·
t44u-,u-ll Conner 19.5 p
7439-89-6 Iron 61ouu E* p
l43'1-'1L-l Lead 17.2 • F
7439-9S-4 Maanes1tim l Z I 0 B p
74.i9-'1b-, Manqanese 95.3 E p
7439-97-6 Mercurv .13 u CV
144U-UL-U Nickel lU.l u p
1440-09-1 Potassium lLjQ B p
7782-49-L Se en1um 2. 6 u EN F
7440-l.l-4 51 ver L. l u p
744U-.lj-, So ]lUffl 157 B p
7440-28-0 ThaTI1um . ol u w F
14ou-o~-.l Vanadium I j. L p
7440-66-b Zinc 38.0 p
c.yan1de NR
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Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 2
THE FOLLOWING FURNACE ANALYTES ARE ESTIMATED DUE TO INTERFERENCE:
SELENIUM
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
MW16-2S-l
L~b Name: COMPUCHEM LABORATORIES Contract: 788 ------I I
L~b Code: COMPU Case No.: 24520 SAS No.: SDG No.: 209373
r1.1Lcix (soil/water): SOIL
Level (low/med):
1. Sol ids·:
LOW
92.9
Lab Sample ID: 358994
Date Received: 07/25/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No.
7429-90-5
iTI1r ---:, t, -1!
7440-38-2
7440-39-3
7440-41-7
IT<f0-43-9
7440-70-2
7440-47-3
7440-48-4
74.f0-50-8
7 4 ,g_,rg-_5
7439-92-1
TI,'l-'-~-4
7439-96-5
~-97-o
7440-02-0
7440-09-7
T7R2-49-2
7440-22-4
iTI1r ..:TI ---S
7440-28-0
TI41r-b2----Z
7440-66-6
Color Before: BROWN
Color After: COLORLESS
Comments:
FORM l -PAGE 3
I Analyte IConcentrationlC/ Q
Aluminum 5350 E*
Antimonv 7. 4 u N
Arsenic .97 B s
Barium 7. 9 B E
Bervllium .21 u
Cadmium 1.1 u
Calcium 2 26' B
Chromium 9.r
Cobalt l. l B
Conner 4.8 B
Iron 6140 E*
Lead .3.0 •
Maqnesium 142 B
Manaanese 20.7 E
Mercury .11 u
Nickel 8. 2 u
Potassium 628 u
Selenium .42 u WN
Silver 1. 7 u
Soaium Iu B
Thallium .42 u w
vanaai um 19.1
Zinc 6.4
Cvaniae
Clarity Before:
Clarity After:
FORM I -IN
'-. ,-. ..,
l'M I
p
p
P"
p
p
p
p
p
p
p
p
P"
p
p
CV
p
p
P"
p
p
I"
p
p
NR
Texture:. MEDIUM
Artifacts:
7/88
1 1
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
T.~b Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
75.8
Contract: 788 ------I MW2A-6S-l
SAS No.: SDG No.: 209373
Lab Sample ID: 360302
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/4L~-~U-~ A.1uminum 40700 e;. p
7440-j()-0 Antimonv ':i.L u N p
/440-3tl-L Arsenic l. z B ("
7440-j':J-3 Barium b8.o E p
/44U-4.l-/ Bervllium l. 4 p
7440-43-9 Ca-dmi um l. 3 u p
7440-/U-L Calcium 109 B p
7440-47-3 Chromium ll. 2 p
7440-4tl-4 Cobalt 4. 2 B p
7440-~0-8 Conner l j. ':/ p
7439-89-6 Iron 4,;,uu E• p
14~:,-':/L-l Lead 10. 3 • F
7439-95-4 Maqnesium 549 B p
/43':i-':ib-~ Manqanese lJl E p
7439-97-6 Mercurv . 13 u CV
1440-02-0 Nickel 10.J u p
7440-U':i-I Potassium 785 u p
1182-4':i-2 Selenium 2.6 u WN. F
7440-ZL-4 Silver 2.1 u p
7440-23-~ Sodium 141 B p
7440-✓-tl-U Tnallium . 53 u w F
l4•v-o.c-2 Vanact1um q I . 4 p
744U oo-b Zinc 26.9 p
1...:van1de NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 4
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
L~b Name: COMPUCHEM LABORATORIES
r,,J h Code: COM PU case No.: 24520
Matrix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
77.4
SBl-1-1
Contract: 788 I
' I
------
SAS No.: SDG No.: 209373
Lab Sample ID: 359878
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
fCAS No. I Analyte fConcentrationfCI Q IM I
/4l9-90-" Aluminum n100 e:• p
7440-36-0 Antimony 9. 0 u N p
/440-jl:l-l Arsenic : "I B w l"
1440-39-3 Barium 89.6 E p
1440-41-/ Bervllium 2.4 p
1440-43-9 Cadmium 1. j u p
7440-70-2 Calcium 65.J B p
/440-4 /-j cnromium 8. 8 p
7440-48-4 Cobalt 5. 2 B p
/440-"0-t! Cooner 9.5 p
7439-89-6 Iron 40800 e:• p
/439-9l-1 Lead 13. I • l"
7439-95-4 Maqnesium 191 B p
14 39-~o-~ Manqanese l9.5 E p
7439-97-6 Mercury .13 u CV
7440-02-0 Nickel 10.0 u p
/4sv-U<,i-7 Potassium 161 u p
1182-49-2 Selenium 2.6 u WN l"
/44U-l2-4 Silver 2.0 u p
1440-LJ-~ Sodium 149 B p
7440-28-0 Thallium .01 u w F.
/440-62-L Vanadium 49.6 p
1440-66-6 Zinc 19. 3 p
Cyanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
i:0lor After: YELLOW Clarity After: Artifacts:
Comm~nts:
FORM 1 -PAGE 5
7 /88
INORGAN~CS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lob Name: COMPUCHEM LABORATORIES
r ... ,h Code: COMPU Case No.: 24520
rintrix (soil/water): SOIL
Level (low/med):
t Solids:
LOW
79.3
SBl-2-1
Contract: 788 -----I
SAS No.: SDG No.: 209373
Lab Sample ID: 359877
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationJCI O IM I
7429-90-5 Aluminum 215uu E• p
/44U-jb-U Antimony. !j • " u N p
7440-38-2 Arsenic .52 B w F
/44U-jY-j Barium 8,.Y E p
1440-41-/ Beryllium j. j p
7440-43-9 Cadmium 1. 2 u p
/44U-IU-L Calcium 15 I B p
7440-47-3 Chromium 7.8 p
1440-48-4 Cobalt J.9 B p
/44U-,U-!l Coooer l /. y p
7439-89-b Iron 59uUO E• p
/4jY-YL-l Lead Ll.Y • F
7439-95-4 Maqnes1um 843 B p
/4jY-Yb-5 Manganese lYl E p I
7439-97-6 Mercury .13 u CV
/44U-UL-U NicKel y." u p
1440-09-1 Potassium Ill u p
I l!lL-49-L Selenium L., u WN f
1440-LL-4 Silver l. 9 u p
/44U-23-5 Sodium lj7 B p
7440-28-U Tnall1um . -~ u w f
/44U-bL-L Vanaaium 4 /. 4 p
1440-00-6 Zinc 42.3 p
L.van1oe NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 6
FORM I -IN 7/88
INORGANICS CASE 209373 1 4
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
M,itrix (soil/water):. SOIL
L~v~l (low/med):
1. Solids:
LOW
66.0
Contract: 788 __c__;__ ___ _ I SB12-l-l
SAS No.: SDG No.: 209373
Lab Sample ID: 360863
Date Received: 08/01/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/4L':!-':!U-o Aluminum 773vv E* p
7440-36-0 Antimonv 10.6 u N p
1440-Jtl-L Arsenic l.L u F
744u-39-J Barium L ,18 E p
1440-41-1 Bervllium . I 0 e· p
7440-43-9 Cadmium 1.5 u p
1440-IU-L Calcium o~v B p
7440-4 7-3 Chromium 252 p
/44U-4tl-4 Cooalt 99.L p
7440 ·OU ·8 Conner 167 p
74J:l-tl:l-b Iron 10LUUU E:. p
143'1-'IL-l Lead J. 4 • F
74J'l-':!:>-4 Maqnes1um 71 'IV p
7439-:io-5 Manaanese 1"480 E p
/4J':!-':! /-b Mercurv .lo u CV
7440-02-0 Nicl<e1 251 p
/44U-U':!-/ Potassium 902 u p
7782-49-2 Selenium 3.0 u WN F
/440-LL-4 S11ver 2 . 4 u p
7440-23-5 ·so'd1um :,H B p
144U-L8-U ·Tnallium . bl u w F
744V-6L-L Vanadium 232 p
1440-oo-b Zinc ,l.'I p
Cyanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
fORM 1 -PAGE 7
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
L~b Name: COMPUCHEM LABORATORIES
r,a b Code: COM PU Case No.: 24520
r•atcix (soil/water): SOIL
L~vel (low/med): LOW
78.7
Contract: ~7~8~8 ___ _ I SB2-l-l
SAS No.:, ---SDG No.: 209373
Lab Sample ID: 359876
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
747.9-90-5 Aluminum 31100 E• p
TIT0-36-0 Antimonv 8.B u N p
14'11l -'1r -2 Arsenic Z. 5 u w F
7440-39-3 Barium 68.5 E p mo...:n-T Be rv 1T i um 2.0 p
7440-43-9 Cadmium 1. 3 u p
7<140-70-2 Calcium ll~ B. p
7440-47-, Chromium 18.9 p
7440-48-4 Cobalt 4.9 B p
7440-50-8 Conner 12. 1 p
7439-89-6 Iron 418uu E* p
7439-92-1 Lead 12.9 • F
7TT9 """"-4 Maanesium 710 B p
7439-96-5 Manaanes" 64".2 E p
TTT9-Tl-o Mercury . 13 u CV
7440-02-0 Nickel 9.8 u p
7440-o<r-7 Potassium 749 u p
7782-49-2 Selenium 2. 5 u EN F mo...:2-z--4 SiTve r Z. 0 u p
7440-23-5 Sodium 169 B p
7<140-28-0 ThalTium .49 u w F
7440-62-2 Vanadium 60.7 p
TIT0-00-0 Zinc 30. 3 p
Cvanide NR
I
Color Before: BROWN
Color After: YELLOW
Clarity Before:
Clarity After:
.Texture: MEDIUM
Artifacts:
Comments:
,ORM 1 -PAGE 8
THE FOLLOWING FURNAc'E ANALYTES ARE ESTIMATED DUE TO. INTERFERENCE:
SELENIUM
FORM I -IN 7/88
INORGANICS CASE 209373 l 6
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U.S. EPA -CLP
l CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
L~b Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
riatcix (soil/water): SOIL
L~v~l (low/med):
'.. Solids:
LOW
77. l
Contract: 788 --"--'------I SB2-2-l
SA S No.: SDG No.: 209373
Lab Sample ID: 359881
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. Analyte I Concentration IC I Q IM I
1429-'IU-5 Aluminum 28100 E• p
7440-36-0 Antimonv 8.8 u N p
7440-38-2 Arsenic 2. 5 u w F
"'7"TTTI-l9-3 Barium 33. 2 B E p
7440-41-7 Bervllium 2.9 p
"'7"TTTI -TI ...:,r caamium l. 3 u p
7440-70-2 Calcium ~'I. I B p
"'7"TTTI -TI -' Chromium 8. 2 p
7440-48-4 Cobalt 3. 2 B p
7440-50-8 Conner 13. 0 p
7419-89-6 Iron 4 I /Ou E • p m -92-1 Lead 10:u • F
743 -95-4 Maanesium 374 B p
741 -<Jti...:, Manaanese 4 I. 8 E p
743 -97-6 Mercurv . lJ u CV T44o-o,...:o Nicl<el: 9.8 u p
7440-09-7 Potassium 749 u p
TilD: --49 --, Sel:enium 2 . :, u WN F
7440-22-4 Silver 2.0 u p
i44lJ -L] ---., soaium l:, 0 B p
7 440-7A-O Thallium . 50 u ;; F
7440-62-'2 Vanadium o7.0 p
1440-bb...:6 Zinc 3" . j p
Cvanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 9
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 --'-----I SB3-l-l I
Lab Code: COMPU Case No.: 24520 SAS No. : SDG No.: 209373
tL1trix (soil/water): SOIL
L0v~l (low/med):
1. Solids:
LOW
80.1
Lab Sample ID: 359880
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte JConcentrationJCI Q
14.!!:l-~v-~ Aluminum L8700 e:•
7440-lfi-O Antimony 8.6 u N
744U-J8-2 Arsenic 2. 4 u w
7440-39-3 Barium 1 A. 7 B e:
7440-41-1 Beryllium 1. 8
7440-43-9 Cadmium 1.2 u
1440-IU-L Calcium 136 B
7440-47-3 Chromium l 4. D
7440-4tl-4 CoOalt 5. 3 B
7440-,0-e Coooer 1 l. g
7439-89-b Iron ~7AQO e:.
74JY-!:IL-l Lead <r .1r •
7439-95-4 Magnesium 639 B
14 JY-96-o Manqanese 7,<f., E
7439-97-b Mercury . 12 u
7440-02-0 Nickel 9. 7 B
744U-0!:1-I Potassium 729 u
7782-49-2 Selenium 12. 2 u N
7440-LL-4 Silver 2. 0 u
7440-23-5 Sodium 176 B
744U-L8-U Thallium .49 u w
7440-62-2 Vanadium 59. 1
/44U-bb-b Zinc 37.9
Cvanide
Color Before: BROWN Clarity Before:
Color After: YELLOW Clarity After:
Comments:
,ORM 1 -PAGE 10
FORM I -IN
INORGANICS CASE 209373 '
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
f.
p
p
NR
Texture: MEDIUM
Artifacts:
7/88
l ,:,
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
L~b Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
Mntrix (soil/water): SOIL
L~vcl (low/med):
1. Solids:
LOW
81.l
5B3-2-1
Contract: 788 ------I
SAS No.: SDG No.: 209373
Lab Sample ID: 359879
Date Received: 07/27/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
JCAS No. I Analyte JConcentrationJCJ Q JM I
/4,,,-,,u-5 Aluminum ·,fi200 E• p
1440-.Jb-0 Antimony tl. '., u N p
7440-38-2 Arsenic .49 u w f
1440-.J9-.J Barium . 11 / E p
7440-41-7 Beryllium 4. l p
1440-4.J-9 caamium 1. L u p
7440-70-2 Calcium 52.2 B p
1440-4 /-.J cnrom1um I • tl p
7440-48-4 Cobalt 19.6 p
1440-:,u-tl Coµµer ,,;1 p
7439-89-6 Iron 51200 E • p
l4.J,,-9,-1 Leaa L4.t, • f
7439-95-4 Maqnesium lvo0 B p
14 .J9-'1o-'., Manganese 5 / / E p
7439-97-6 Mercury . lZ u CV
/440-UL-U NicKel l U. ;I p
7440-v,,-7 Potassium 7 27 u p
1182-49-2 Selenium L. 4 u WN f
/440-22-4 Silver 2. 0 u p
1440-2.J-S soaium 10s B p
7440-28-0 Thallium .49 u w f
1440-62-2 vanaaium 4 tl . 9 p
/44U-66-o Zinc 64. 3 p
c.vanicte NR
I
Color Before: BROWN Clarity Befor.e: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM l -PAGE 11
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA~ CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lub Name: COMPUCHEM LABORATORIES
Lub Code: COMPU case No.: 24520
r1,)trix (soil/water): SOIL
Level (low/med):
1 Solids:
LOW
79.8
SB4-1-1
Contract: 788 ------I
SAS No.: SDG No.: 209373
Lab Sample ID: 360295
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q JM I
/41.9-9U-~ Aluminum l.blUU e:·• p
7440-36-0 Antimony 8. 4 u N p
144U-Jll-l. Arsenic .49 u F
/440-39-j Barium ,o.8 E p
7440-41-7 Bery11ium 2. 6 p
144U-4J-Y Cadmium 1. I. u p
7440-,u-2 Calcium 75.6 B p
144U-4 /-j cnromium ll . 1 p
7440-48-4 Cobalt 6 .1 B p
144U-~U-ll Coooer l~.b p
7439-89-6 Iron 42300 E* p
14,,-Yl.-1 Leao 11..9 .. F
7439-95-4 Maqnes1um 1320 p
14,,-Yo-~ Manganese 1 I 4 E p
7439-97-6 Mercury .13 u CV
144U-UI.-U NicKel 9. 4 u p
7440-09-7 Potassium l 710 p
I 182-49-2 Selenium I..~ u WN F
1440-22-4 Silver l. 9 u p
144U-lJ-~ Sodium I. 4 y B p
7440-28-u Tna11ium .4~ u w F
144U-62-2 Vanadium 4b.l p
144U-t,b-b Zinc 4 / . I p
Cyanide NR
.
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
rORM 1 -PAGE 12
FORM I -IN 7/88
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U.S. EPA -CLP
l CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lob Name: COMPUCHEM LABORATORIES
t,1b Code: COMPU Case No.: 24520
Matrix (soil/water): SOIL
L~vel (low/med): LOW
t Solids: 73.5
SB4-2-l
Contract: _7~8~8 ___ _ I
SAS No.: SDG No.: 209373
Lab Sample ID: 360297
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte I Concentration IC I Q IM I
7429-90-:5 Aluminum 30200 E* p
TI41l"-J6-IT Antimoriv ~., u N p
7440-38-2 Arsenic .54 u r TI4ll -,-g -J Barium 2,1 E p
7440-41-7 Bervllium 3. 2 p
TI40-43-9 Cadmium 1. 4 u p
7440-70-2 Calcium 7 4. 8 B p
TI40-47-J Chromium ~. 4 p
7440-Ta"-4 Cobalt 5 3. 5 p
7440-50-8 Coooer 1,. r p
74Jg-sg-fi Iron 5nt!00 e:• p
7439-92-1 Lead 1 A. 6 • F
TIJ-g-<fS -4 Maqnesium 28 40· p
7439-96-5 Manaanese 1740 E p
7 4-r9-9 7-6 Mercurv .14 u CV
TI40-02-0 Nickel 10.6 u p
7440-u~-7 Potassium 2870 p
T782-49-2 se--ren1um 2. 7 u WN F
7440-]]-4 Silver 2.2 u p
TI40-23-5 Sodium 177 B p
7440-JR-0 Thallium .54 u F
TI40-62-2 Vanachum 53. 8 p
7440-oo-6 zinc 89. 4 p
Cvaniae NR
I
Color Before: BROWN Clarity Before:
•Clarity After:
Texture: MEDIUM
Color After: YELLOW Artifacts:
Comments:
FORM l -PAGE 13
FORM I -IN 7/88
INORGANICS CASE 209373 21
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET
L~b Name: COMPUCHEM LABORATORIES Contract: 788 ......:-'-----
r,~h Code: COMPU Case No.: 24520 SA S No.:
CLIENT SAMPLE NO.
I SB5-l-1 I
SDG No.: 209373
ri,,trix (soil/water): SOIL
L~vel (low/med):
i Solids:
LOW
86.4
Lab Sample ID: 360298
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte !Concentration!CI Q
T42 9-90 -S ATuminum zs ,oo· ...
7440-36-0 Antimonv 8.1 u N
744lr-"11!"-2 Arsenic z. j B
7440-39-3 Barium 54. 9 E
1440-41-7 BervlTium • ; I B
7440-4J°-9 Cacfm1um l. 2 u
7440-70-2 Calcium 261 B
1440-47-3 CFiromium Ll.b
7440-48-4 Cabal t· 4.5 B.
1440-50-8 Cooo·e r ,2. j
7439-89-6 Iron 23800 E•
7419-92"-I Leaa 9. l •
7439-95-4 Maanesium 5,, B
i 4 39-96-5 Manaanese llT E
Tir19-97-6 Mercurv . 12 -· u
7440-02-0 Nickel 15.5
1440-09-7 Potassium 689 u
77 8 2-49-2 Selenium 2. 3 u WN'
T440-22-4 Silver 1. 9 u
TI40-L3-5 Sodium 135 B
1440-28-0 Thallium . 46 IJ
iTI0-62-2 Vanadium 44.6
T4~0-66-6 Zinc 18.0
Cvanide
Color Before: BROWN Clarity Before:
Color After: YELLOW Clarity After:
Comments:
~ORM 1 -PAGE 14
FORM I -IN
INORGANICS CASE 209373
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
f
p
p
NR
Texture: MEDIUM
Artifacts:
7/88
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lc,b Nume: COMPUCHEM LABORATORIES
L,Jb Code: COMPU Case No.: 24520
M~r.r ix (soil/water): SOIL
Level (low/med):
, Solids:
LOW
76.0
Contract: 788 ------I SB5-2-l
SAS No.: SDG No.: 209373
Lab Sample ID: 360299
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
747.g_~u-5 Aluminum 41500 e:• p
7440-36-0 Ant1monv 9 .. 2 u N p
'7'Till" -,I! -2 Arsenic 2. 6 u w F
7440-39-3 Barium 107 e: p
,440-41-7 BeivT11um 2.o p
7440-43-g Cadmium. 1. 3 u p
7440-70-2 Calcium 41. 8 B p
7440-47-3 Chromium 8. 5 p
,4,10-48-4 Cobalt 11. 0 B p
7440-~v-8 Coooer 13. 7 p
,n g -8<l ..:1, Iron 410\J0 E* p
7439-92-1 Lead 14. 9 • F
"i"4'TI -<l73 -4 Maqnes1um 2~\J0 p
7439-;,o-5 Manaanese 236 E p
14T9-97-6 Mercurv .13 u CV
7440-02-0 Nickel 10. 3 u p
i440-0<i-7 Potassium 1400 p
7782-49-2 Selenium 2. 6 u WN F
i440-TI-4 s 1, ve r 2. 1 u p
7440-23-5 Sodium 170 B p
'7'Till" ,JI lY Tha~11um .SJ u w F
7440-62-2 Vanadium 60.8 p
7440-t>t>-6 zinc 59.2 p
Cvan1ae NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comments:
FORM 1 -PAGE 15
FORM I -IN 7/88
• I N()RCii=!N I CS Ci=!SE 2(19.373
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lt1b Name: COMPUCHEM LABORATORIES
Lab Code: COMPU Case No.: 24520
r1atcix (soil/water): SOIL
Level (low/med):
i Solids:
LOW
78: 0
SB6-l-1
Contract: 788 ------I
SAS No.: SDG No.: 209373
Lab Sample ID: 360300
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
jCAS No. I Analyte I Concentration IC I Q IM I
14L9-90-o Aluminum bL9UU E• p
/QQU-Jb-0 Antimony 13. 8 B N p
1440-.lB-L Arsenic l. b B F
/040-39-3 Barium 69.8 E p
1440-41-1 Beryllium l. l B p
74 40-4 3-9 Cadmium 1. .l u p
/QQU-/U-L Calcium JlQ B p
1440-47-.l Chromium .ll l p
I QQU.-48-q Cooalt 8.tl B p
1440-oU-B Copper· 9L.b p
/039-!!9-b Iron 8/bUU e;. p
1439-92-1 Lead 6.6 • F
/Qj9-9J-Q Magnesium llQU B p
7439-96-5 Manqanese 203 I E p
/Q.l9-9/-b Mercury . 1 j :u CV
7440-02-.0 Nickel 124 p
/440-09-/ Potassium I b J ,U p
7782-49-2 Selenium 2.6 IU WN f
1440-LL-.4 Silver L.1 u p
7440-23-5 Sodium 190 B p
/44U-Ltl-U Tna11ium .Jl u w f
7440-62-2 Vanadium 216 p
/440-oo-b Zinc L tl . , p
cvaniae NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comm~nts:
fORM 1 -PAGE 16
fORM I -IN 7/88
TNnR~QNIC5 CQ5E 209373
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U.S. EPA -CLP
l CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
L~b Code: COMPU Case No.: 24520
11,,trix (soil/water): SOIL
Lcv~l (low/med):
1 Solids:
LOW
67.5
SB6-2-l
Contract: ~7~8~8:___ __ _ I
SAS No.: SDG No.: 209373
Lab Sample ID: 360301
Date Received: 07/28/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
/4l9-9U-a Aluminum 03000 E • p
7440-36-0 Antimony IO. 4 u N p
7440-38-2 Arsenic 1. 2 u F
7440-39-3 Barium 150 E p
7440-41-7 Bervllium 2. J p
/44U-4.l-9 Caamium 1.5 u p
7440-70-2 Calcium T!,J B p
7440-41-.l cnromium 272 p
7440-48-4 Cobalt TI .---;i B p
144U-aU-1:! Conner l~R p
7439-89-6 Iron lU.JU0U r• p
7439-9l-l Lead 2.J • F
7439-95-4 Maanesium 2040 p
14 39-96-a Manaanese IS<T E p
7439-97-6 Mercury . 15 u CV
7440-02-0 Nickel. 17'9' p
7440-09-7 Potassium 882 u p
l78l-49-2 Selenium 3.0 u· WN F
7440-22-4 Silver 2. 4 u p
744U-L3-a Sodium 226 B p
7440-28-0 Thallium . 59 u w F
7440-62-Z Vanadium 258 p
7440-66-b zinc 31. 4 p
Cvanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW
Comments:
rORM l -PAGE 17
Clarity After:
fORM I -IN
Artifacts:
7/88
INORGANICS CASE 209373 -, C '
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
L,, b Code: COM PU Case No.: 24520
Matrix (soil/water): SOIL
L~v~l (low/med):
,. Sol ids:
LOW
79.5
SB8-l-l
Contract: 788 -----I
SAS No.: SDG No.: 209373
Lab Sample ID: 361464
Date Received: 08/02/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte jConcentrationlCI Q IM I
7429-~u-5 Aluminum ]69uu E* p
/44U-jb-U Antimony ti • ti u N p
74•u-38-2 Arsenic l. 6 B w !'
144U-j9-j Barium ,ov E p
7440-41-7 Beryllium 4.1 p
/44U-4.:!-9 Caamium l. j u p
7440-70-2 Calcium lo~ B p
1440-4 /-j Cnromium l I . ti p
7440-48-4 Cobalt 9. 4 B p
/44U-~v-tl Coµµer .,.u p
7439-89-6 Iron 87t1uO E* p
/4.:!9-9,-1 Leaa bl.9 p
7439~95-4 Maqnesium 805 B p
/4j9-~o-o Manqanese l,lU e: p
7439-97-6 Mercury .13 u CV
·/ 4 4U-U ,-U NicKel l J. o p
7440-09-7 Potassium 806 B p
I /tl,-49-, Selenium [., u WN' F
7440-22-4 Silver z.o u p
/44U-,j-o soaium l .:! ti B p
7440-28-0 Thallium . 50 u w !'
1440-62-l Vanaaium b I. J p
7440-66-6 Zinc 74.7 p
Cyaniae NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Cnlor After: YELLOW Clarity After: Artifacts:
Comm~nts:
FORM l -PAGE 18
FORM I -IN 7/88
INORGANICS CASE 209373
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U.S. EPA -CLP
l CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
L.:ib Code: COMPU Case No.: 24520
M~trix (soil/water): SOIL
Level (low/med): LOW
1; Solids: 86.0
Contract: 788 ------I SB9-l-l
SAS No.: SDG No.: 209373
Lab Sample ID: 360861
Date Received: 08/01/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
74ZY-YU-o Aluminum J2400 -E• p
7440-36-0 Antimony t!.---r u N p
7440-Jtl-i Arsenic 3.1 P'
744U-JY-J Barium S6.5 E p
7440-41-7 Bervllium .81 B p
7440-43-9 Cadmium 1. 2 u p
7440-70-2 Calcium 692 B p
7440-41-J Chromium 43.0 p
7440-48-4 Cobalt 6. 8 B p
1440-o0-8 Copper 2I .-S p
7439-89-6 Iron i3100 E* p
14H-Y2-l Lead l 7. 8 • P'
7 43~-9 5-4 Maonesium 499 B p
/4JY-Yb-o Manqanese 296 E p
7439-97-6 Mercury . 12 u CV
1440-02-0 Nickel 26.7 p
7440-09-7 Potassium 692 u p
7782-49-2 Selenium ,.1 u WN F
7440-22-4 Silver 1. 9 u p
7440-23-5 Sodium T51l B p
7440-28-0 Thallium· .47 u w F
7440-62-2 Vanadium 41.7' p
7440-66-6 Zinc tl 1. 2 p
Cyanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After: Artifacts:
Comm~nts:
FORM 1 -PAGE 19
FORM I -IN 7/88
INORGANICS CASE 209373 -, -
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES
L,1 b Code: COM PU Case No.: 24520
r,,,trix (soil/water): SOIL
L~vel (low/med):
". Sol ids:
LOW
68.0
Contract: 788 .;...::...:_ __ _ I SB9-2-l
SAS No. : SDG No.: 209373
Lab Sample ID: 360862
· Date Received: 08/01/90
Concentration Units (ug/L or mg/kg dry weight): MG/KG
ICAS No. I Analyte IConcentrationlCI Q IM I
7429-90-5 Aluminum 725uu e:• p
/44U-36-U Antimony lu. 3 u N p
7440-38-2 Arsenic 1..2 u w P'
/440-39-3 Barium 10~ E p
7440-41-7 Bervllium · . 79 B p
/440-43-9 Cadmium 1. 5 u p
7440-70-2 Calcium 53.8 B p
/440-4/-3 cnromium 4 4 7 p
7440-48-4 Cobalt 7.9 B p
7440-50-8 Coooer 119 p
/439-89-6 Iron 102000 . E"• p
7439-92-1 Lead 4. 3 • F
/439-9~-4 Maqnesium 851 B p
7439-96-5 Manganese 179 E p
1439-97-6 Mercury . 15 u CV
/44U-UL-U NicKel 193 p
7440-09-7 Potassium 875 u p
//82-49-2 Selenium 2.9 u WN F
7440-22-4 Silver 2. ·4 u p
/44U-L3-~ Sodium 329 B p
7440-lR-O Thallium 2.9 u w F
/44U-bL-L Vanadium 189 p.
7440-oo-6 Zinc 9 5. 7 p
Cyanide NR
I
Color Before: BROWN Clarity Before: Texture: MEDIUM
Color After: YELLOW Clarity After:
Comm~nts:
FORM 1 -PAGE 20
FORM I -IN
INORGANICS CASE 209373 ,
Artifacts:
7/88
-, ,-, ..;. ,_,
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WMPUCHEM
lABc)MrC>RJES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 (919) 549•8263
INORGANICS CASE NARRATIVE SUMMARY
CASE# 24520 SDG# 37227D
The above indicated SDG consisted of one (1) water sample which was
received on August 31, 1990, intact and in good condition with the Chain of
Custody (COC) Records in order. The sample was analyzed, adhering to the
EPA 788 Statement of Work (SOW), for the Inorganic Target Analyte List
(TAL) which consists of twenty-three (23) metals.
SAMPLE ID:
The following customer ID is associated with this SDG .
. MW9-0l-l
The enclosed Cover Page reflects both SIRRINE Environmental
~onsultant's and Comp~Chem's sample Identifiers (CCNs).
QUALITY CONTROL:
All calibration verification standards and verification blanks were
within the EPA-CLP acceptance criteria.
The laboratory control sample and interference check samples met all
EPA established criteria.
The preparation blank met EPA requirements, with all elements being
determined below the Contract Required Detection Limit (CRDL), but
aluminum, calcium, sodium, and zinc were determined at concentrations
greater than their respective Instrument Detection Limits (IDLs).
The sample spike, CCN = 367834 (MW-09-lS) was outside the control
limit for cadmium, mercury, iron, selenium and thallium, therefore, all
concentrations for these analytes were flag9ed with an "N" on all Form ls
and Form 5. The control limit for sample spike recoveries is 75% to 125% of
the amount added, unless the original sample concentration of analyte
exceeds the spike amount by a fa'ctor of four or more. In the latter case,
the analyte is not flagged if the recovery is outside the control limits.
As required by the SOW, cadmium and iron were post digestion spiked
and were recoverd at 131.5% and 101.6&% respectively.
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COMPUCHEM
lABoPATORJES, INC.
The sample duplicate, CCN = 367835 (MW-09-10) was outside the control
limit for aluminum, iron, and.zinc, therefore, all concentrations for these
analytes were flagged with a"*'' on all Form ls and Form 6. The control
limit for duplicate determinations is+/-20% Relative Percent Difference
(RPO) for analyte concentrations greater than or equal to five times the
CRDL in both the original and the duplicate solutions. If the analyte
concentrations. are less than five times the CRDL, then +/-the CRDL will be
the limit. The RPO is not calculated if both the original and duplicate
values fall below the IDL.
MSAs were not required for the quantitation of any GFAAS element
determination.
The serial dilution was performed on sample, CCN = 367833 (MW-09-1)
and the adjusted sample concentrations were within the control limits for
all analytes except aluminum, therefore, all sample concentrations for this
analyte were flagged with an "E" on Form ls and Form 9. Also, a statement
reflecting this fact can be found on the Cover Page. The control limit for
the serial dilution is that the adjusted sample concentration for all
analytes with values greater than fifty (50) times its IDL in the original
sample, must agree within 10% of the original values.
Release of the data contained in this hard copy data package has been
authorized by the Laboratory Manager or his designee, as verified by the
following signature.
Technical Reviewer
October 20, 1990
Note: This report is paginated for reference and accountability.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
MW9-0l-l
Lab Name: COMPUCHEM LABORATORIES Contract: ~7~8~8 ___ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 37227D
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: o.o
Lab Sample ID: 367833
Date Received: 08/31/90
Concentration Units (ug/L or mg/kg dry·weight): UG/L
ICAS No.
7429-90-5
744U-,o-U
7440-38-2
7440-JY-J
7440-41-7
7440-4J-Y
7,440-70-2
1440-4/-j
7440-48-4
144U-~u-l:l
74JY-l:lY-6
7439-92-1
7439-95-4
7439-96-5
7439-9/-b
7440-02-0
1440-09-1
7782-49-2
/44U-ll-4
7440-23-5
744U-l8-U
7440-62-2
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
fORM 1 -PAGE 1
I Analyte IConcentrationlCI Q
Aluminum 1970
Antimony 29.0
Arsenic 2. 0
Barium 57 7
Bervllium 1.0
Caamium 5. 0
Calcium 8960
cnromium 7. a
Cobalt 2 3. 4
Conner 4 .----□
Iron 1770
Lead T.--0-
Maqnesium 6 58 0
Manqanese 2 0 :,u
Mercury .20
Nickel 4 7. 5
Potassium 3160
Selenium 10.0
Silver 7. 0
Sodium .JOSOO
Tna~lium ,.□
Vanadium 4. 0
zinc 6-ir _--g
Cyaniae
Clarity Before: CLEAR
Clarity After: CLEAR
fORM I -IN
E•
u
u
u
u N
B
B
u
N•
uw
u N
u
u WN
u
u WN
u •
IM I
p
p
P'
p
p
p
p
p
p
p
p
f
p
p
CV
p
p
P'
p
p
P"
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 37227D
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Q)MPUCHEM
LA8()f¥J()R1ES, INC:.· P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 (919) 549•8263
INORGANICS CASE NARRATIVE SUMMARY
CASE# 24520 SDG# 937120
The above indicated SDG consisted of nine (9) water samples which were
received on August 06, 10, and 17, 1990, intact and in good condition with
the Chain of Custody (COC) Records in order. The samples were analyzed,
adhering to the EPA 788 Statement of Work (SOW), for the Inorganic Target
Analyte List (TAL) which consists of twenty-three (23) metals.
SAMPLE IDs:
The following customer IDs are associated with this SDG.
FB-02-1
PW-07-1
PW-:02-1
PW-08-1
PW-03-1
SB-2R-l
PW-03-2
SB-JR-1
The enclosed Cover Page reflects both SIRRINE Environmental
Consultant's and CompuChem's sample Identifiers (CCNs).
QUALITY CONTROL:
PW-06-1
All calibration verification -tandards and verification blanks were
within the EPA-CLP acceptance criteria'.
The laboratory control sample and interference check samples met all
EPA established criteria.
The preparation blank met EPA requirements, with all elements being
determined below the Contract Required Detection Limit (CRDL), but
aluminum, calcium, iron, and zinc were determined at concentrations greater
than their respective Instrument Detection Limits (IDLs).
The sample spike, CCN = 362534 (SB-3R-1S) was within the control
limits. for all analytes, therefore, no concentrations were flagged with an
''N'' on Form ls and Form 5. The control limit for sample spike recoveries is
75% to 125% of the amount added, unless the original sample concentration
of analyte exceeds the spike amount by a factor of four or more. In the
latter case, the analyte is not flagged if the recovery is beyond the
control limits.
No post digestion spikes were required.
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COMPUCHEM
lABo!WORIES, INC.
The sample duplicate, CCN = 362535 (SB-3R-1D) was in control for all
analytes except chromium, therefore, all concentrations for this analyte
were flagged with a"*" on all Form ls and Form 6. The control limit for
duplicate determinations is+/-20% Relative Percent Difference (RPO) for
analyte concentrations greater than or equal to five times the CRDL in both
the original and the duplicate solutions. If the analyte concentrations are
less than five times the CRDL, then+/-the CRDL will be the limit. The RPO
is not calculated if both the original and duplicate values fall below the
IDL.
MSA was required for the determination of selenium for the following
sample: PW-06-1. The correlation coefficient was greater than 0.995, thus
the data on Form 1 was flagged with an "S".
MSA was required for the determination of thallium for the following
sample: PW-06-1. Both MSAs displayed correlation coefficients less than
0.995, thus the data on Form 1 was flagged with a"+".
The serial dilution was performed ·on sample, CCN = 363567 (SB-3R-l)
and the adjusted sample concentrations were within the control limits for
all analytes, therefore, no sample concentrations were flagged with an "E"
on Form ls and Form 9. The control limit for the serial dilution is that
the adjusted sample concentration for all analytes with values greater than
fifty (50) times its IDL in the original sample, must agree within 10% of
'.he original values.
Release of the data contained in this hard copy data package has been
authorized by the Laboratory Manager or his designee, as verified by the
following signature.
:BuaWL
Bruce H. Rohrbach
Technical Reviewer
October 18, 1990
Note: This report is paginated for reference and accountability.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
f'B-02-1
Lab Name: COMPUCHEM LABORATORIES Contract: ~7~8~8 ___ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 364107
Date Received: 08/10/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-5
7440-Jo-O
7440-lA-2
7440-3':l-3
7440-41-7
1440-4.l-':I
7440-70-2
7440-·4 7-3
7440-48-4
7440-~0-8
7439-89-6
743':l-':12-l
7439-95-4
743':l-':16-~
7439-':li-6
. 74 4 0-0 2-0
7440-U':l-7
7782-49-Z
7 4 4 U-L2-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 1
I Analyte IConcentrationlCI Q
Aluminum 67.7
Antimo·nv 3; .a
Krse·nic 2. 0
Barium I. 8
Bervlliu·m l.O
Cadmiu·m s;o
Calcium 4 5. 7
Chromium 6 .-o
Cooalt 4. 0
Coooer 8.0
Iron 6.8
Lead 2. 0
Maanesium 90.0
Manaan·ese 3. 0
Mercury .20
Nick"el B.lY
Potassium 2980
Selenium 2.0
Silver 8. 0
Sodium 452
Thalli(fm 2. 0
van·aaium 4. 0
Zinc 8.J
Cvan·icte
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u
u
B u
u
B
u • u u
B u
u u u
u
u
u
u
u
u
u
·B
IM I
p
p
r
p
p
p
p
'p
p
p
p
r
p
p
CV
p
p
r
p
p
f'
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937120
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U.S. EPA -CLP
1 CLIENT SAMPLE. NO. INORGANIC ANALYSIS DATA SHEET
PW-02-1
Lab Name: COMPUCHEM LABORATORIES Contract: _7~8~8 ___ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix ( so.il/water): WATE:R
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 365285
Date Received: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
74l9-90-5
7440-1~-0
744U-.l8-2
7440-39-3
744U-41-I
7440-43-9
7440-/U-2
7440-47-3
7440-48-4
7440-S0-8
74.lY-BY-b
7439-92-1
74.lY-Y,-4
7439-96-5
74JY-Y7-6
7440-UL-U
7440-09-7
iltlL-4Y-L
7440-22-4
7440-23-5
7440-28-0
7440-62-L
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM 1 -PAGE 2
I Analyte IConcentrationlCI ·o
Alum·inum 8 3. 1
Antimonv 35.0
Arsenic 2. 0
Barium 50.2
Bervllium 1.0
Cadmium -s. 0
Calcium T660
Chromium o.O
Cob·a1 t 4. 0
Coooer 11:6
Iron 7 4·. 2
Leaa 2. 9
Maqnesium ~
Manganese 4 . 4
Mercurv .TI
Nick·e1 39.0
Potassium 2980
Selenium 2 . er
Silver 8. 0
Sodiu·m 5260
Thallium -z.o
va·naaiu·m 4. 0
Zin·c 3J.0
cvaniae
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u
u
B
u
u
u • u
B
B
B
B
B
u
u
u
u w
u
u w
u
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
·cv
p
p
F
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937120
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
PW-03-1 Lab Name: COMPUCHEM LABORATORIES Contract: 788 I -----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No. : 9 3 712 O·
Matr_ix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 365286
Date Received: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/4L'::l-'::IU-~
7440-36-0
1440-Jt!-L
7440-39-3
1440-41-1
7440-43-9
/44U-IU-L
I '140-4 7-3
/44U-4t!-4
7440-50-8
/4J'::l-t!';l-b
7439-92-1
/QJ'::1-'::I~ q
7439-'::IO-~
/4J'::l-'::I 1-b
7440-02-0
1440-u,:,-I
I /8L-4'::l-2
7440-22-4
/44U-LJ-~
7440-28-U
1440-bL-L
1440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 3
I Analyte I Concentration IC I Q
AJ.uminum I ti • J Antimony 35.0 Arsenic L • l Barium 59.l
BeryJ.J.ium l. l Cadmium 5. 0
Calcium ti 48 U Chromium 6.0 CooaJ.t 4. U
Copper 14.9
Iron ,: u . ';I
Lead 2.4 Magnesium L J. o u
Manqanese 3.0
Mercury • LU
Nickel 39.0
Potassium J4~U
Selenium J. u . u
Silver 8.0
Soaium J.U'::IUU
Thallium 2.0 Vanaaium q. u
Zinc 31. 2 Cvaniae
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u
u
B
u
u
u • u
B
B
B
B
u
u
u
B
u w
u
u w
u
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F'
p
p
NR
Texture:
Artifacts:
7/88
I NORGf:lN I{CS CASE 937120. '
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I PW-03-2
-----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 365289
Date Received: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
JCAS No.
/4•9 -~u-,
7440-36-0
/44U-38-•
7440-39-3
/44U-41-I
H40-43-9
744U-/U-•
7440-47-3
I 44.U-48-4
7440-50 ·8
1439-89-0
H39-92-l
1439-9,-4
7439-96-,
1439-91-b
744 □-u.-u
1440-09-1
l/8l-49-•
7440-22-4
7440-.3-,
7440-28-0
/44U-bl-l
7440-fifi-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 4
I Analyte JConcentrationJCI Q
A1uminum o •. ~
Antimony J,. 0
Arsenic •. u
Barium ·61.1
Bery11ium l. U
Cadmium ,.o
Ca1cium !D9U
cnromium o. 0
Cooa1t 4. U
COµµer 16.9
Iron 1,.u
Leaa 2. 0
Magnesium • l I U Manganese 3.0
Mercury . lU
NicKel 39. u
Potassium l~0U
S.e1enium lU. U
Silver 8.U
Soaium ll20u
Tna11ium l. U
Vanaaium 4. U
Zinc . l 9. 2
Cyan1ae
Clarity Before: CLEAR
Clarity After: CLEAR
!"ORM I -IN
B
u
u
B
u
u
u • u
B
B
u
B
u
u
u
u
u w
u
u w
u
IM I
p
p
F
p
p
p
p
p
p
p
p
l"
p
p
CV
p
p
l"
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937120
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D
· U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
PW-06-1 Lab Name: COMPUCHEM LABORATORIES Contract: 788 _ _c__ __ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 365290
Date Received: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
14L':l-':IQ-:,
144U-36-U
1440-JB-l
/440-J':/-j
1440-41-1
/44U-43-':I · /440-10-L
i44U-4 i-J
1440-48-4
7440-50-8
14.l':I-B':l-b
/439-92-1
14 J':1-':I :,-4
14.l':1-96-5
/439-':17-6
i44U-UL-U
7440-09-7
//Bl-4':l-l
7440-22-4
1440-lJ-:,
744U-28-0
7440-o.l-.l
/44U-bb-b
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM ·1 -PAGE .5
I Analyte I Concentration IC I Q
Aluminum 10B0 Antimonv lU:, Arsenic 12.4 Barium lUQ
Bervalium 10.2 Caomium l:,.L Calcium l4.0 Cnromium 16.6 CoOalt :>L.J Conner 37.6 Iron 834 Leaa ti • 8 Maqnesium 701 Manganese ., u. tl
Mercury . l:!l Nickel 11:,
Potassium 2980 Selenium . lJ. !l Silver 8.0 soaium 4:>l Tna11ium 4. 0 Vanadium l:, 2 zinc 4 4. L cvan1de
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u •
B
u
s
u
u
u +
IM I
p
p
F
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937120
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
PW-07-1
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I -----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 365291
Date Received: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-5
144U-jb-U
. 7440-38-Z
144U-j':/-j
7440-41-7
/44U-4j-':I
7440-70-Z
/44U-47-3
144U-4~-4
144u-:,u-8
7439-89-6
/4j':l-':IL-1
7439-95-4
/4j':l-':lb-a
74 39-9 7-6
144U-UL-U
7440-U':1-7
I /8L-4':I-L
7440-ZZ-4
144U-Lj-:,
7440-28-0
144U-6Z-L
/44U-b·b-b
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM 1 -PAGE 6
I Analyte IConcentrationlCI Q
Aluminum luq
Antimony 3:, . u
Arsenic · Z. 0
Barium 1. U
Beryllium 1.0
caamium :, . u
Calcium l4. 0
Cnromium 6. 0
Cobalt 4. 0
Coooer 9. ':I
Iron 6. 7
Leaa L. U
Maqnesium 90.0
Manganese J.U
Mercury . zo
Nicxe1 J':I.U
P6tassiu·m 2980
Selenium L. U
Silver 8.0
Sodium :, U I
Thallium 2. 0
vanadium 4. U
zi·nc .•. u
Cyanide
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u u
u
u
u
u u • u
B
B
u u
u u
u
u
u u
B
u
u
u
IM I
p
p
I'
p
p
p
p
p·
p
p
p
I'
p
p
CV
p
p
I'
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937120
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
PW-08-1
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I --'----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Leve~ (low/med):
~ Solids:
LOW
0.0
Lab Sample ID: 365292
Date Rec•ived: 08/17/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
142':l-':IU-o
7440-36-0
/44U-J5-L
744 -39-3
144 -41-I
744 -43-9
7440-70-2
744U-4 /-j
/44U-4tl-4
7440-50-8
143':l-o~-b
7439-92-1
143':l-':IJ-4
7439-96-5
143':l-':l l-b
7440-02-0
/44U-U9-I
7782-4':I-L
144U-L2-4
/44U-LJ-J
7440-28-0 ·
74•v-62-2
/44U-bb-b
Color Before: COLORLESS
Color After: YELLOW
Comments:
FORM 1 -PAGE 7
I Analyte I Concentration IC I Q
Aluminum 998uu
Antimonv 35.0
Arsenic 2. u
Barium 1. 4
Bervllium l.u
Caamium J. 0
Calcium 24:1
Chromium 6.0
Cobalt 4. 0
Conner 8.0
Iron 105000
Lead 2.0
Maane·siu·m 9u.O
Manaanese 3. 0
Me r·curv . 2u
Nickel 39. 0
Potassium 295U
Selenium 10. 0
Silver 5.0
Sodium 452
Tnallium 2. 0
Van·actium ':I:~
Zinc 6. 2
Cvaniae
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
u
u w
B u
u
B
u •
u
u
u
u
u
u u
u u w
u
u
u w
B
B
IM I
p
p
I'
p
p
p
p
p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORG~NICS C~SE 937120
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
SB-2R-l
Lab Name: COMPUCHEM LABORATORIES Contract: 788 -'--'-----I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937120
Matrix (soil/water): WATER
Level (low/med):
i Solids:
LOW
0.0
Lab Sample ID: 362533
Date Received: 08/06/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/4L':1-':IO-~
7440-36-0
/440-Jl:!-L
7440-39-3
/440-41-/
7440-43-9
/440-/0-L
7440-47-3
/440-41:!-4
7440-50-8
/4.l':l-tl':l-b
74 39-92-1
/4.l':l-':l~-4
7439-96-5
T4.39-~1-6
/44U-UL-U
7440-09-7
/ /tlL-4':I-L
7440-22-4
/440-L.l.-~
7440-28-0
/440-bL-L
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 8
I Analyte IConcentrationlCI Q
Aluminum ,:,j
Antimony 35.0
Arsenic L. 0
Bar lUffl 1. 9
Beryllium l. U
Cadm11im 5.0
Calcium Juo
Chromium 6.0
Cobalt 4. 0
Copper 9: 0
Iron lJb
Lead 3. 6
Maqnesium ':IU. 0 ·
Mang·anese 3.5
·Me·rtu·rv .20
Nic1<e1 j ':I. u
Potassium 2980
Selenium L.U
Silver 8.0
Soaium tl j ':I
Thallium 2. 0
vanaaium 4.U
Zinc 8. 1
Cyaniae
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B
u
u
B
u
u
B
u •
u
B
u
B
u
u
u
u
u
B
u
u
B
IM I
p
p
F
p
p
p
p
. ·p
p
p
p
F
p
p
CV
p
p
F
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANlCS CASE 937120 ' .
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 788 I SB-3R-l
-----
Lab Code: COMPU Case No.: 24520 SAS No. : SDG No.: 937120
Matrix (soil/water)_: WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 363567
Date Received: 08/09/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
· ICAS No.
742Y-YU-o
7440-36-0
744U-j~-..:
744U-39-J
7440-41-i
/44U-43-Y
7440-70-2
1440-41-J
7440-48-4
1440-oU-8
7439-89-6
143Y-9L-l
7439-Yo-4
7439-96-5
7439-Y 1-b
7440-02-0
7440-0Y-I
7782-49-2
144U-..:L-4
7440-23-5
/44U-L!l-U
744U o~-..:
7440-oo-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 9
I· Analyte I Concentration IC I Q
Aluminum 112
Antimonv 35.0
Arsenic ·2. 0
Barium z.o
Bervllium l.O
Cadmium s.u
Calcium 74.7
cnromium 11. 8
Cob·a1 t 4. 0
Conner !:!. u
Iron 75.0
Lead .l. 7
Maanesium 90.0
Manaanese 5.7
Mercurv . 20
Niclie7: J9. 0
Potassium 2980
Selenium 2. 0
Silver 8. 0
Sooium 544
Tn·a·11 i um L. U
va·nad·ium q. 0
Zin·c e·. o
Cvanide
Clarity Befoce: CLEAR
Clarity After: CLEAR
F'ORM I -IN
B
u
u
B
u
u
B •
u ·u
B
u B.
u
u
u
u
u
B
u
u
B
IM I
p
p
P'
p
p
p
p
p
p
p
p
P'
p
p
CV
p
p
r
p
p
r
p
p
NR
Texture:
Artifacts:
7/88
INORG~NICS C~SE 937120
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CDMPUCHEM
lABc:)MTC>RJES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC27709 [phone]
INORGANICS CASE NARRATIVE SUMMARY
CASE# 24520 SDG# 937164
The above indicated SDG consisted of.two (2) water samples which were
received on August 21, 1990, intact and in good condition with the Chain of
Custody (COC) Records in order. The samples were analyzed, adhering to the
EPA 788 Statement of Work (SOW), for the Inorganic Target Analyte List
(TAL) which consists of twenty-three (23) metals.
SAMPLE IDs:
The following customer IDs are associated with this SDG.
PW-04-1 PW-05-1
The enclosed Cover Page reflects both SIRRINE Environmental
·onsultant's and CompuChem's sample Identifiers (CCNs).
QUALITY CONTROL:
All calibration verification standards and verification. blanks were
within the EPA-CLP acceptance criteria.
The laboratory control sample and interferende check samples met all
EPA established criteria.
The preparation blank met EPA requirements, with all elements being
determined below the Contract Required Detection Limit (CRDL), but
aluminum, barium, calcium, and iron were determined at concentrations
greater than their respective Instrument Detection Limits (IDLs).
The sample spike, CCN = 365994 (PW-05-lS) was within.the control
limits for all analytes except selenium and.thallium, therefore, all
concentrations for these analytes were flagged with an "N" on all Form ls
and Form 5. The control limit for sample spike recoveries is 75% to 125% of
the amount added, unless the original sample concentration of analyte
exceeds the spike amount by a factor of four or more. In the latter case,
the analyte is not flagged if the recovery is beyond the control limits.
No post digestion spikes were required.
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CbMPUCHEM
lABo!WORJES, INC.
The sample duplicate, CCN = 365995 (PW-05-1D) was in control for all
analytes, therefore, no concentrations were flagged with a"*'' on Form ls
and Form 6. The control limit for duplicate determinations is+/-20%
Relative Percent Difference (RPD) for analyte concentrations greater than
or equal to five times the CRDL in both the original and the duplicate
solutions. If the analyte concentrations are less than five times the CRDL,
then+/-the CRDL will be the limit. The RPD is not calculated if both the
original and duplicate values fall below the IDL.
MSAs were not required for the quantitation of any GFAAS element
determination.
The serial dilution was performed on sample, CCN = 365997 (PW-05-1)
and the adjusted sample concentrations were within the control limits for
all arialytes, therefore, no sample concentrations were flagged with an ''E"
on Form ls and Form 9. The control limit for the serial dilution is that
the adjusted sample concentration for all analytes with values greater than
fifty (50) times its IDL in the original sample, must agree within 10% of
the original values.
Release of the data contained in this hard copy data package has been
authorized by the Laboratory Manager or his designee, as verified by the ·
following signature.
~ctJW~ Bruce H. Rohrbach
Technical Reviewer
October 19, 1990
Note: This report is paginated for reference and accountability.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES I PW-05-1
Contract: 788 -'-'-----
Lab Code: COMPU Case No.: 24520 .SAS No.: SDG No.: 937164
Matrix (soil/water): WATER Lab Sample ID: 365997
Level (low/med): LOW Date Received: 08/21/90
l Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
74l9-90-5
7440-36-0
7440-Jll-2
7 4 40-39-J
7440-41-7
7440-43-9
/440-/0-l
7440-47-3
/44U-41l-4
7440-50-8
/4J9-ll9-b
7439-92-l
7439-95-4
7439-":lb-~
t4J9-9t-o
7440-02-u
7440-u-,-I
7782-49-L
7 4 4 0-lZ-4
144U-LJ-~
7440-28-0
/44U-bL-L
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
P'ORM 1 -PAGE 2
I Analyte IConcentrationlCI Q
Alumtn\im b40
Antimonv 35.0
Arsenic 2. o
Ba Cl um 23.8
Bervllium · l. 0
Cadmium 5. 0
Calcium l44U
Chromium 6. 0
Cobalt 11. l
Conner 912
Iron I J Jou·
Lead lll. 2
Maon·esiU:m r-, iU
Manaanese 89.3
Mer cu r·v . lO
Nickel 39.0
Potassium l9ou
Selenium 10.0
Silver ll . 0
Sodium lLJUU
Tha"TI i um 2. 0
vanaaium 5. 2
Zinc ~44
Cvan·i-de
Clarity Before: CLEAR
Clarity After: CLEAR
!'ORM I -IN
u u
B
u
u
B u
B
u
u
u
u WN
u
u WN
B
IM I
·p
p
P" p.
p
p
p
p
p
p
p
P'
p·
p
CV
p
p
P'
p
p
F
p
p
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INORGANlfS CASE 937164
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: _7~8~8 ___ _ I PW-04-1
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937164
Matrix (soil/water): WATER Lab Sample ID: 365993
Level (low/med): LOW Date Received: 08/21/90
% Solids: 0. 0
Concentration Units (ug/L or mg/k~ dry weight): UG/L
ICAS No.
• /429-90-5
/440-36-0
I' 140-38-2
7' 140-39-3
,, 40-41-7
7440-43-9
/440-70-2
7440-47-3
/440-48-4
7' 140-S0-8
I ' 39-89-6
7 ' 39-92-1
I ' 39-95-4
7' 39-~o-5
I ' 39-97-6
I ' 40-02-0
I , 40-U'l-7
I 82-49-2
7' 40-22-4
I ' 40-23-5
7• 40-28-0
I ' 40-62-2
7• 40-06-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM 1 -PAGE l
I Analyte IConcentrationlCI Q
Alum·1num 2"63
Antimony lS.o
Arsenic 2. 0
Barium 4. 4
Bervllium I.O
Cadmium S.o
Cale tum 3880
Chromium b ; 0
Cobalt 4. 0
Co'pper 8. 0 -
Iron 483
Lead 6.g
Magnesium 2060
Manqariese 7.9
Mercury . 20
Nickel 39.0
Potass1(im 2980
Selenium 10. 0
Silver 8. 0
Sodium 62QU
Thallium 2. 0
Vanadium 5. 4
Zinc 293
Cvanide
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
u
u B.
0
u
B
u
u
u
B
B
u
u
u
u WN
u
u WN
B
IM I
·p
I:'
P' p·
p
p
p·
p
p
p
p
P'
p
p
CV
p
p
P'
p
p
F
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937164
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WMPUCHEM
lABC)MfC>RJ.ES, INC. P.O. Box 12652 3308 Chapel Hill/Nelson Highway Research Triangle Park, NC 27709 [phone]
INORGANIC CASE NARRATIVE-CASE 24520
SDG No. 937182
Contract No. 788
_Samples: FB-03-1. MW2R-l, MW05-l-l, MW06-l-l, MWOS-1-1,
MW13-l-1, MW14R011, MW015011, MW15102, MW16-l-l,
MW2A-01-l, MW7-0l-l, MWSA-01-1, MW9-0l-l, sw-11-1,
SW-12-1 .
Case No. 24520 consisted of sixteen (16) water samples which
were. scheduled for the analysis of _the target analyte list
(TAL) · metals and cyanide. The samples were received intact
on August 24, 25, and JO, 1990 with the corresponding chain-
of-custody documents. The courier was Federal Express.
The enclosed cover page reflects both Sirrine Environmental
and Compuchem sample identifiers.
The associated quality control sample spike, MW06-l-1S, was
outside of the control limits for Antimony, Beryllium, Lead
(by furnace AA), Selenium, Silver, Thallium, Zinc, and
Arsenic (by furnace AA). These values were flagged with an
'N' on the Form ones (1) and the form five (5). The control
limits for ~he spike recovery values are 75-125%, unless the
original sample concentration exceeds the amount of added
spike by a factor of four or more. In the later case, the
value is not flagged even when the percent recovery value is
outside of the control limits.
The associated duplicate, MW06-l-1D, was outside the control
limits for Aluminum, Arsenic, Beryllium, Chromium, Copper,
Iron, Magnesium, Manganese, Potassium, Vanadium, and Zinc.
These values were therefore flagged with an'*' on the Form
ones (1) and the form six (6). The control limits for
comparison of the duplicate sample with the original sample
are +/-twenty (20) relative percent difference (RPDl for
analytes with concentration values greater than or equal to
five times the contract required detection limit (CRDL) in
both the original and the duplicate samples, and+/-CRDL if
either the original or duplicate value is less than five
times the CRDL. The RPD is not calculated if both the
original and d~plicate values fall ~elow the instrument
detection limit (IDL).
In .the Inductively Coupled Plasma (ICP) analysis on October
16, 1990 for this SDG, the duplicate sample results for
Compuchem Number 366949 were outside of the control limits
for the elements listed above (with the '*' flag). The
sample results are being attributed to viscous sample matrix
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11
Q)MPUCHEM
l.ABoAArORIES, INC.
and sample inhomogeneity. Since, all other quality control
criteria were met.for this analysis, we are reporting the
data with reference to the enclosed qualifier.
A post digest spike was done for sample MW06-l-1A for the
following analytes: Antimony, Beryllium, and Zinc.
A serial dilution was performed on sample MW06-l-l L for all
analytes analyzed by ICP. The adjusted sample concentration
values for the analytes with concentrations greater than
fifty times the IDL in the original sample were within 10%
of their original values. None of the ICP analytes was
flagged with the 'E' footnote on the form ones (1) or the
form nine (9).
Method of standard addition was not required for any of the
samples in this case.
Release of the data contained in this hardcopy data packa9e
has been authorized by the Laboratory's Manager or his
designee, as verified byte following signature·
Note: This report is paginated for reference and
accountability.
2
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
FB-03-1 Lab Name: COMPUCHEM LABORATORIES Contract: _7~/~8~8 __ _ I
Lab Code: COMPU• Case No.: 24520 SAS No.: SOG No.: 937182
Matrix (soil/water): WATER
Leve 1 (low/med): LOW
\ Solids: 0.0
Lab Sample IO: 367036
Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
7429-90-5
TI4lr---:JD-lr
7440-38-2
7440-3 -,
7440-4 -7
74(0-4 -9
7440-TIT-2
7440-47-3
J44/l-dR-4
7440-,-50-8
TIT9-B9-0
74.l~-92-1 TIT9 _--.,-,, _ 4
74.l~-~o-5
/439-'l 1-0
7440-02-0
7440...:1r9_,
7782-49-2
7440-22-4
7440-23-5
744u-2R-O
1440-6'2-'2
744u-oo-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
!'ORM 1 -PAGE l
I Analyte IConcentrationlCI Q
Aluminum 7 7 . 9
·AntTmonv ~~-0
Arsenic .0
BarTum . 0
Bervllium .0
Cadmium ,.u
Calcium 96.8
Chromium 4.0
Cobalt 4.0
Coooer (.0
Iron 19.2
Lead J.O
Maanesium 48.0
Manaanese 1.0
Mercurv .20
Nickel j!,,O
Potassium 3100
Selenium .l.0
Silver 7. 0 ·so·dium 740
Thallium 2. 0
Vana-dTum 4,0
Zinc 4.0
CvanTde 10.u
Clarity Before: CLEAR
Clarity After: CLEAR
!'ORM I -IN
B •
0 N ·o N
u
0 N•
u
B
u • u
u •
B • u N a • u • u
u
u •
u WN
U N
B
U N
u •
0 N•
u
IM I
p
I'
F
p
p
p
p
p
p
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F
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<..:V
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.p
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Texture:
Artifacts:
7/88
INORGANICS CASE 937182 I ::-.
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U.S. EPA -CLP
1 CLIENT SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
MW-2R-l Lab Name: COMPUCHEM LABORATORIES Contract: _7~/_8_8 __ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG. No.: 937182
Matrix (soil/water): WATER
Level (low/med): LOW
\ Solids: 0.0
Lab Sample ID: 367038 ·
Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
TI29-90-S-
744U-<h-0
TI4n-3B-2
7 440-39-3
TU0-41-7
7440-43-9
7440-/U-2
7440-47-3
7440-48-4
TI4ll .:,[l-lr
7439-89-6
TI39-9--i-r
7439-95-4
"'74,9 -'I 6 ---S-
7439-~t-6
TI4ll-1TT---U
7440-u~-7
Tn!L.-4<1-L
7440-22-4
TI41l -LJ ---S-
7440-7R-O
TI4ll-TI-z
7440-bb-6
Color Before: COLOllLESS
Color After: COLORLESS
Comments:
FORM 1 -PAGE 2
I Analyte IConcentrationlCI Q
.
Aluminum 5 7, 0
Antimonv 29.0
ArsenTc 2. u
Barium 2.0
Bervllium I. o
Cadmium 5. 0
Calcium l U:>
Chromium 4. 0
Cobalt 4".I
Conner 4. I
Iron !:I.
Lead 3.0
Maanesium 4!:I. U
Manaanese 1.0
Mercurv .20
Nicl<e"T 35.0
Potassium 31 i, u
se--ienium 3.0
Silver 7.0
Soaium 40~
Thallium .. 2. 0
Vanarfl um 4.0
Zinc 4.0
cvanfi'le lU.0
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
B * u N
u N
u
u N*
u
B
u w
u
u *
B *
u N
u *
u * u
0
u *
u WN
0 N
B
0 N
u *
u N* u
IM I
p
p ..
p ..
p ..
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AS
Texture: -
Artifacts:
7/88
INORGANICS CASE 937182 1 1
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: ~7~/~8~8 __ _ I MW0S-1-1
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 366944
Date Received: 08/24/90
Concentration Units (ug/L or mg/kg dry weight): UG/L·
jCAS No.
14.l~-~u-~
7440-36-0
744U-JH-<
744U-a:,-3
7440-41-/
744U-4j-9
7440-70-Z
144U-4/-j
7440-48 ·4
744U-~U-8
7439-H~ ·f>
/439-9.l-l
7439-95-4
/4j~-~f)-~
7439-97-6
/44U-Ut-U
7440-09-7
I /Bt-49-.1
7440-ZZ-4
/44U-lJ-~
7440-28-u
7440-bl-Z
7440-f>f>-f)
Color Before: BROWN
Color Aft.er: YELLOW
Comments:
FORM 1 -PAGE 3
I Analyte IConcentrationjCI O
Aluminum j7~UUU
Ant.1monv <:,. 0
Arsenic 2.0 BarTum 3Zou
Bervll1um ll. I
Cac:1m1um ~. 0
Calcium 244UU
cnromium l~uu Cooalt JHH
Cooner 11ou
Iron 04vVUU
Lead Z3.6
Maanesium 51<UU
Manaanese bljU
Mercurv . <U
Nickel 149U
Potassium 4440
Selenium l ~. U
Silver 7.0
Sooium ~0/U
Tnallium 2. 0 Vana-dium bZ7
zinc 4:, ~
Cvanioe IO. 0
Clarity Before: OPAQUE
Clarity After: CLEAR
• u N
u N
N"
u
~
• •
N • •
0
B •
10 EN
10 N
:u N •
N*
u
IM I
p
p
r
p ..
p ..
p ..
p ..
r
p
p
CV
p
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p
p
A<>
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIM'A:TE'D DUE TO I°NTERFER°ENC:E:
SELENIUM
FORM I -IN 7/88
INORGANICS CASE 937182 l 2
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11
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
MW06-l-1 Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 I ~----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med) : LOW
% Solids: 0.0
Lab Sample ID: 367028
Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
14,Y-YU-:,
71 4 0-36-0
I < 4 U-J6-,
7140-39-
144U ·4.L
/44U-4J-'
7440-70-
144U-41-
/440-48-
1440 ·!:>U ·•
7 4 .:19.,-59-1
/4J'j-'j,-
74.:19-95-4
/4j'jC..'jt,-:,
7439-91-f,
/44U-U,-U
7440-09-7
I /1Ji-4'j-,
7440-ZZ-4
/44U-iJ-:,
7440-ZB-0
144U-b,-Z
7440-66-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 4
I Analyte IConcentrationlCI Q
A.Luminum .L.L6uuu
Antimony L"l O Q
Arsenic ,.u
Barium z ;40
Bery.L.Lium , . I
caam1um . 0 Calcium lOZOO
cnromium ~" . :, Cobalt 78.3
couuer YU.4
Iron UIVuVU
Leaa I I • :)
Maqnes1um ~j/UU
Manganese :, l • u Mercury . ~u
NicKe.L 4 4 . :,
Potassium l, '-' u u
Se.Len1um .L :, . 0
Silver 7. 0 soaium o::,ou·
Thallium 3. 7
vanaaium '7:>
zinc /jU
cvan1ae 10.0
Clarity Before: OPAQUE
Clarity After: CLEAR
*
u N
u N
"" u
*
*
*
r, • -* u
• u !Cr<
u N
B [,
•
N*
u
IM I
p
p
• II'
p
II' ..
II'
• II'
p
\.V ..
p
r
II'
p
r-..
p
AS
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE EStI'MAi'ED DUE TO INTERFERENCE: SELENIUM
FORM I -IN 7/88
INORGANICS CASE 937182
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U.S. EPA -CLP
l ' CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 ~----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0. 0
Lab Sample ID: 366955
Date Received: 08/24/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
jCAS No.
J4L.'1-':IU-':J
744U-Jo-U
/440-38-2
/44U-J!:1-J
7440-41-7
/44U-43-!:I
744u--,u-z
/440-41-3
7440-48-4
/440-50-8
14J!:1-H!:l-b
7439-92-1
14,,,-!:l,-4
74J:,,-:,,o-5
14,:,,-!:I 1-b
7440-02-0
/44U-U!:1-I
/ /tl2 ·49 .•
7440-ZZ-4
/44U-.lJ-,
7440-ZB-O
/ 44U-0.l-.l
7440-66-o
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 6
I Analyte IConcentrationlCI Q
A.luminum t!//vv Antimony Z:,,. 0 Arsenic •. u Barium .l.l4U Beryllium 7.9 !.;aOffllUffl ,.u
Calcium 16600 Cnromium ,4.U Cobalt 49. 9 Conner tl4.tl Iron lOv\JOU Lead Ll>.9
Magnesium ll4UU
Manaanese .·4 .u Mercury . ~v Nickel ~ •. u
Potassium 18 • v-u Se.lenium .l,. u Silver 7. 0 Soaium !:l~ou Tnallium 2. 0 Vanaaium .l,, Zinc ,.,
1.vaniae .lU. U
Clarity Before: OPAQUE
Clarity After: CLEAR
•
u N
u N
,..
u
•
B • •
N • •
u
• u En
u N
u "" • ,..
u
IM I
p ..
I'
p
p
p
p
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p
I:'
p
I' ..
p
Cv ..
p
I'
p
p
I'
p ..
A:;
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIMXTE~ DUi TO nfiriffi"h:R'i!:NCE: SELENIUM
FORM I -IN 7/88
INORGANICS CASE 937182 1 4
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
MW14R011 Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 ~----I
Lab Code: COMPU Case No.: 24520 SAS No.: soc; No.: 937182
Matrix (soil/water): WATER
Level (low/me~):
\ Solids:
LOW
0.0
Lab Sample ID: 367661
Date Received: 08/30/90
·concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/4,1. -0 ·5
/44 -. 10-U
744 -8-,
/44U-:,-' /440-l-,
7440-43-'J
1440-IU-,1.
7440 ·47-_
1440-48-1
1440-~0-!
140-:,-8'1-b
74n-92-l
140-:t-!:I~-•
7439-96-5
14,-,-'J 1-6
/440-02-0
1440-U'J-7
I /82-49-2
1440-.t.l-4
7440-23-5
/440-1.8-U
7440-62-2
/440-bb-b
Color Before: BROWN
Col·or After: YELLOW
Comments:
FORM 1 -PAGE 7
I Analyte IConcentrationlCI Q.
Aluminum ,;;;,iQuV
Antimony ,I. 'I • IJ Arsenic 2.u
Barium b!lU
Berv11ium ll. ~ caamium ~. u calcium I'-7 IJ Chromium
'" • I cooa1t ,~.l
Conner 84.2
Iron lUllUUU
Lead Jl. 0 Maqnes1um llouU
Manaanese lb4U
Mercury . ,.u
Nickel ,u.,
Potassium 8Z5U
Selenium 1,.u
Silver I. U Sodium ,-, I U
Tna11ium -,I.. u
vanadium l ,1.1
zinc ,. , ,I.
<:.vaniae lU.0
Clarity Before: OPAQUE
Clarity After: CLEAR
•
V N
u N
N•
u
-
D -•
N • •
u
•
u EN
u N
u " • ". u
IM I
Ii'
p
I!'
p ..
p ... ,,. .. ..
p
I!' ..
Ii'
<;.V
p
p
I'
p
p
I'
p
Ii'
A:;
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIMATED DOE TO fNTERl'ERENCE: SELENIUM
FORM I -IN 7/88
I NO.~: 6 H N I 1:>,_S C H 5 E ·:-1 3 7 1 8 2
1 -
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
CLIENT SAMPLE NO. I MW08-l-l I
SDG No.: 937182
Lab Name: COMPUCHEM LABORATORIES _Contract: 7/88 ~-----
Lab Code: COMPU Case No.: 24520 SAS No.:
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: a.a
Lab Sample IO: 367031
Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
74l9-9U-~
744 -36-0
/44 -Jtl ·l
144 -39-3
/440 4!-7
/44U-4J-':I
7440-70-Z
/440-4/-j
/440-41'-4
1440-SU-t!
/4J':l-tl':I ·O
74J9-92-l
/4J':l-':l,-4
74J9-':IO-~
/4~:,-'j ,_,,
744U-Ol-O
744(-U':l-7
I ltll-4':I l
7440-ZZ-4
/44U-lJ-~
7440-ZB-0
/440-62-l
/44U-66-0
Color Before: BROWN
Color After: -YELLOW
Comments:
FORM 1 -PAGE 5
I Analyte IConcentrationlCI Q
Aluminum ,,~vu
Antimony l Arsenic . Barium '~ Berv111um 5.l caamium , . u
Calcium 4!HU
Cnromium 2~,
Cobalt l ti. ':I
Co□aer lll Iron f VJ.VV Leaa 7.7 Maanesium ':14,U Manganese Zoo
Mercurv . 4':I Nlcl<ei loo
Potassium 7130
Se1enium 1,.u
Silver 7.0
Soaium ,iov
Thallium z.o
Vanaaium t!U. 4
zinc l I~
1.vanioe 10.U
Clarity Before: OPAQUE
Clarity After: CLEAR
FORM I -IN
•
u N
u N
n-
u
B •
B • ..
N • •
•
u '"" u N
u N •
N•
u
IM I
p
p
F
y
y
r
p
p
p
y
p
P'
I' I
p '
CV•
p
p
f' ..
p
t ..
p
A~
Texture:
Artifacts:
7/88
INORGANICS CASE.937182
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: ~7~/~8~8 __ _ I MW15011 I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water'): WATER
Level (low/med):
% Solids:
LOW
0. 0
Lab Sample ID: 367664
Date Received: 08/30/90
Concentration Units. (ug/L or mg/kg dry weight): UG/L
jCAS No.
/4.t9-':JI -5
7440-31 -o
/44U-JI -..:
1440-J' -j
/44U-4 -I
1440-4. -9
7440-,u-2
/44\J-4I-J
7440-48-4
1440-~U-~
74 19-8' -6
/4 ,-':J,
14 ,,_,, -4'
/4J':J-':Jb-5
7 4 H-97-6
/44U-U.t ·U
7440-U':J-7
/ /~.t-49-.t
, • 40 ·22-4
1440-lJ-~
7440-28-0
l44U-b2-l
/440-bb-b
Color Before: BROWN
Color After: YELLOW
Comments:
l'"ORM l -PAGE 8
I Analyte jConcentrationlCI O
Aluminum "~ uu Antimony " . 0 Arsenic .u Barium i~U
BerYllium • I caam1um • 0 Calcium ~o~u cnromium l.tU Cobalt 41.l Copper lU8 Iron 59uuc Leaa I . I Maqnes1um 660( Manqanese 004 Mercury .~U
Nickel 114 Potassium t!Oi\J se·1enium i0.0 Silver I • 0 soaium ~/lU Thallium ". 0 Vanaaium. "i • ,, zinc l,,,
1..vaniae
Clarity Before: OPAQUE
Clarity After: CLEAR
l'"ORM I -IN
•
u N
u N
N"
u
•
B • •
N • •
•
(J "" u ..
u "" •
N*
IM I ..
t'
r
p .. ..
t'
p
p
p
p
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t'
r
c:v
r
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r
t'
p
¥ ..
P.
""
Texture:
Artifacts:
7/88
INORGANICS CASE 937182
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U.S. EPA -CLP
l
INORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO. I MW15012 I
SDG No.: 937182
Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 ~-----
Lab Code: COMPU Case No.: 24520 SAS No.:
Matrix (soil/water): WATER
Level (low/med): LOW
Lab Sample ID: 367666
Date Received: 08/30/90
% Solids: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No. Analyte I Concentration IC I Q IM I
14.l~-~u-~ Aluminum lllOO • p 7440-36-0 Anc1monv Z9.0 u N p /44U-j!l-.l Arsenic .l.O u N ,
7 440-39-3 Barium ZZ' p /44U-4~ / BerV!~lUm L " ... p /44U-4j-~ caamium , . ( l1 p 1440-70-Z Calcium 4!!U B p /44U-4/-j Cnromium ~b.6 • p 7440-48 ·4 Cobalt l j, 0 B .. /44U-~U-!l Coooer '.>7.6 • I<' 74J,t tj';j ·6 Iron 2.QUvv • p /4j~-'1.t-l Leaa 4 • " WN r 1•39-95-4 MaanesiU.m J / !l l B • p 14 j~-''1b-~ Manqanese ' OU • p 7qJ9 ·'1 I ·b Mercury •• 1..V 7440 ·OZ ·O Nick.el tib, 3 .. /Q40-U'1-/ Potassium 44j0 B • p 178.l-49-.l Selenium 1s. a u tcN r 7440-Z2-4 Si!ver I. Q u N p 144U-,U-~ Soaium ,.uu p 7 440-Ze ·O Thallium Z. 0 u "" r 144U-b.l-.l Vanaaium jj. l B • p 7440-66-6 Zinc oo.9 N • p Cyaniae NI\
Color Before: BROWN Texture:
Color After: YELLOW
Clarity·eefore: OPAQUE
Clarity After: CLEAR Artifacts:
Comments:
FORM l -PAGE 9
THE FOLLOWING FURNACE ANALYTES ARE ESTIMAT'e:'D DtJ'E TO !N tERl'ERENCE :" SELENIUM
FORM I -IN 7/88
I NO f<: G H N I C: S CH SE 9 3 7 1 8 2 ·-· ·-·
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
MW16-l-l Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 -'-----I
Lab Code: COMPU
Matrix (soil/water):
Level (low/med):
% Solids:
Case No.:
WATER
LOW
0.0
24520 SAS No.: SDG No.: 937182
Lab Sample ID: 366957
Date Received: 08/24/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
JCAS No.
I' ,l':1-':I\J :,
7< ,40-36-0
/<4\J-j!l-l
7< ,4 0-3 l-3
I' 4 U-4 -I
7<40-43-9
144u 7u-,
1440-4/~j
/44U-48-4
/44U-:>U-ll
/439-ll!I-!>
l439-9Z-.l.
7439-95-4
/4j9-9(J-!>
7439-!I /-!)
144U-Ul-U
7440-U!l-7
I idl-4':l-l
7440-22-4
l4su-lJ-:,
7440-28-0
144\J-bl-l
/440-!>!>-!>
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 10
I Analyte JConcentrationJCI Q
A.1.um1num .1.·u I u u U Antimony l !1. 4 Arsenic l.U Barium I I , Be rv .1. .1.1 um j. ' Cadmium 5. ' Calcium j\J.l.UU
Cnrom1um lZ4 Coba.1.c ':I !l • l coooer 14 !> Iron 199000 Lead l I. I Maqnes1um :ulOO Manqanese J8.l.U Mercury .20 N1cJ<e.1. ~04 Potassium . H!IUU Se.1.en1um .1.:, . \) Silver I • 0 soe11um Yo,u Thallium · 2. 0 Vanaa1um J~o Zinc :, ju
Cyan1Cle 10.0
Clarity Before: OPAQUE
Clarity After: CLEAR
•
" N
u ""'
D N"
•
• -N • •
u
-u ""' u N
u N •
N*
u
111 I ..
p
~
I.' ..
p ..
p
p
p
p
P'
p
p
CV .. ..
f' .. ..
IC
p
p
A:>
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIMATE'D DUE TO INTERP'ERENC1!:! SELENIUM
FORM I -IN 7/88
INORGANICS CASE 937182
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U.S. EPA -CLP
l CLIENT SAMPLE NO. INORGANIC ANALYSIS-DATA SHEET
MW2A-01-1 Lab Name: COMPUCHEM LABORATORIES Contract: ~7~/~8~8c...... __ _ f
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 367658
.Date Received: 08/30/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
14l9-90-o
/ 44U-.H)-U
1440-.Hl-.l
74 -

-
14 -

-
14• -

-
1<14 0 I ·l
144 U-4 j
7440-4 -4
1440-oU-!l
7439-89-6
14J9-9:t-l
7439.,.,,, 4
14J9-:,o-o
74H-97-0
144U-u,-O
744U-U,,-7
I /8.l-49-.l
7440-LL-4
144U-.lJ-o
7440-2R-u
1440-6;!-.l
144U-oo-t>
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 11
I Analyte IConcentrationlCI O IM
Aluminum Jo,o
Anr.1monv .l~.u
Arsenic l • 0 Barium lo~ Bervi.i.1um J. • l Caom1um , . (
Cai.c1um O.l.~v cnrom1um 1L6 Cooalt 4.0 Couoer 4. 0 Iron HOIU Leao j. 8
Maqnes1um jJoU Manqanese , ..
Mercurv . .lU Nickel ,,.o
Potassium JolU Selenium . 15.0
Sii.ver I . U Soa1um /JlO -Tnai.i.1um 2. u Vanacttum U.B
Zinc ~o. !l c:van1oe
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
I NO~GHN I Ci c:i=isE
I •
• p
u N p
u N F
B p
u N • p
u p
p • r
u p
u • p • p
WN F
B • p • r
u I..V
u r
B • p
u WN F u N p
p
u "" P'
B • p
N* p
NR
Texture:
Artifacts:
7/88
937182
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U.S. EPA -CLP
l
iNORGANIC ANALYSIS DATA SHEET CLIENT SAMPLE NO.
MW7-0l-l Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 I ~-----
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample IO: 367655
Date Received: 08z30/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS NO.
/4l!:1-!:IU-:,
7440-36-0
/44U-.Hl ·l
1440-H-3
f<&...,U-4.1.-1
/44U-4J-!:I
7440-70 .z
/440-4/-j
/1140-48-4
/440-!>U-8
/1139-89-6
/4J9-!:ll-l
7, 39-'5-1
I ' j":f-'Cl-:
7, 39-7-1
/44U-Vl-U
7440-09-7
I I tll-4":l-l
1440-ll-4
/ 4,.u-l J-:,
7440-lB-O
/44U-Ol-l
/44U 00-0
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 12
I Analyte 1·concentration IC I O
Aluminum !> / / u u Antimony ~'1.0 Arsenic l, U Barium I I~ Berv11ium . I. l caam1um 5. 0 Calcium 4l4U cnromium :,1. 7
Cobalt 4U.l Coaaer I j • J Iron '1UlUU Leaa 18.0 Maqnesium lU!>VU
Manganese l!:I JU Mercury . zo NicKl!l J:,.u
Potassium ljlVV
Se..1.en1 um l:,.v Silver I. 0 soaium .. ,ov
Thal ll um ~.u vanaaium lZJ zinc j V '1
c.van1ae
Clarity Before: OPAQUE
Clarity After: CLEAR
FORM I -IN
• u N
u N
" . u
5 •
5 • •
N
• • u
u •
u "" u N B.
u N • ...
I,. I
" )!
r
)!
" )!
" )!
p
)!
p
I"
p
p
\,;V
" p
r
p
p
r
p
" NR
TeKture:
Artifacts:
7/88
INORGANICS CASE 937182
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11
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U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
CLIENT SAMPLE NO. I MW8A-01-l I
SOG No.: 937182
Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 ~----
Lab Code: COMPU Case No.: 24520 SAS No.:
Matrix (soil/water): WATER
Level (low/med): LOW
\ Solids: 0.0
Lab Sample IO: 367831
Date Received: 08/31/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
/4l:l-:IU-,
7440-36-
/44U-Jl:I-
7440-39-
/440-'ll-
/44U-4J-
7440-70-.
/44U-4 /-.
7440-48-•
144u-,u 1:1
/4J9 "" ·6 /4J:I :ll l
/4H-:l,-4
7439-:10,
7 4 .l9-::, /-6
/44U-Ul-U
7440 U:1 7
/ ltll 4:1 ·l
7440 22 4
l44U-.lJ-,
7440-28-0
144U-bl-.l
7440-oo-6
Color Before: BROWN
Color After: YELLOW
Comments:
FORM 1 -PAGE 13
I Analyte IConcentrationlCI Q
Aluminum 41:!JOU
Antimony Z9.0 Arsenic l.U Barium 790 Bery11ium l. U caam1um 5. 0 Calcium 25900 Cnromium lZl:I
Cobalt Z4. 9 Coooer i~o Iron ,,.Hvv
Leaa LU
Maqnesium 22:IUU
Manqanese ,v,
Mercury .20
Nickel ~ij Potassium·· 6 11:1\J Selenium 1,.u
Silver I • 0
soaium 4~QV
Thallium 2.0 vanaaium H.,
zinc 65.2 Cyaniae
Clarity Before: CLOUDY
Clarity After: CLEAR
• u N
u N
u ....
u
• .. .
•
u N • •
u
•
u ~n
u N
B
u N'
B •
N*
IM I
p
p
f'
p
p
p
p .,
p
p
p
• p
p
CV
p
r
P'
p
p
~
p
p
NR
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIMATED DUE TO' INTlffitiRENCE: SELENIUM
FORM I -IN , 7 /88
INORGANICS CASE 937182 .-, .-,
~ ....
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U.S. EPA -CLP
1
INORGANIC.ANALYSIS DATA SHEET CLIENT SAMPLE NO.
MW9-0l-l Lab Name: COMPUCHEM LABORATORIES Contract: ~7~/~8~8:_ __ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med): LOW
% Solids: 0.0
Lab Sample ID: 367832
Date Received: 08/31/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
74Z'1-'1U-:,
7440-36-0
1440-Jt!-l
7440-39-3
1440-41-/
7440-43-9
7440-/U-2
7440-47-3
7440-48-4
7440-:,U-B
7439 ·89-6
143'1-'1l-l
74J,:,-95-4
/4J<;-<;"-:,
7439-97-6
7440-Ul-U
7440-09-7
77Bl-4'1-l
7440-22-·4
144U-lJ-:,
7440-28-0
7440 ·6Z-l
7440-66-"
Color Before: BROWN
Color After: YELLOW
Comments:
FORM l -PAGE 14
I Analyte IConcentrationlCI O
Aluminum J91Ullfl
Antimonv 29.0
Arsenic z ."O
Barium 5710
Berv11ium 4.U
Cadmium 5.U
Calcium 1J.3uu
Chromium 1--:J 5 0
Cobalt l" '1
Cooner 757
Iron J76000
Lead 18.2
Maqnesium ',55uu
Manqanese 5920
Mercurv . 20
Nickel LllU
Potassium ~-46-U
Selenium 1:,. 0
Silver 7.0
s0<1i um ,o<;oo
Tnallium 2.0
Vanadium 461
Z1nc " " :, ,vani<le 1 o .er
Clarity Before: OPAQUE
Clarity After: CLEAR
• u N
IU N
iB N•
10
•
• • N • •
0
•
0 Vl\1
u N
u WN •
N•
lJ
IM I
p
p
F
p
p
1'
p
p
p
!P
p
F
p
p
r:;;v
p
p
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1'
p
f ..
p
A:;
Texture:
Artifacts:
THE FOLLOWING FURNACE ANALYTES ARE ESTIMATED DOE TO INTER?E°RENCE;
SELENIUM
FORM I -IN 7/88
INORGANICS CASE 937182
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
Lab Name: COMPUCHEM LABORATORIES Contract: 7/88 -'--'-----I SW-11-1
a Lab Code: COMPU Case No.: 24520 SAS No.: SDG No.: 937182
Matrix (soil/water): WATER
Level (low/med):
% Solids:
LOW
0.0
Lab Sample ID: 367032
.Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
ICAS No.
14:l':l-:,v-~
7440-6-(
144U-o-
1440-,,_
/4u,u-4l_-I
/44U-43-':I
74• 0-·u-,
/ 4. v-• I-
74• 0-•IB-•
/44U ·~U ·t,
/4J:,-o:,-o
74j9-92-l
/4J:,-9~-4.
7439-96-5
143':l-':l l-b
7440-02-u
7440-09-7
I /t,./.-4':I-./.
7440-22-4
/44U-lJ-~
144U-Gtl-V
1440-6:l-l
7440-00-0
Color Before: BROWN
Color After: YELLOW
Comments:
FORM 1 -PAGE 15
I Analyte IConcentrationlCI O
Aluminum lB~ Ant1monv 2 • 0 Arsenic • u Barium 00 Berv111um l. U caam1um . ~. u
Calcium 6 j I U cnrom1um 4. U Cobalt 4. 0 Couoer 4.U Iron 3UJU Leaa J.U Maqnes1um ./.q1u
Manqanese lG~U Mercury . "\J NlCKel J~.u Potassium lJ ,vu se1en1um J.U Silver 7.0
soa1um oqou
TnalllUm G. U vanaa1um 4.U
zinc 13.o 1.van1ae
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
B •
u N
u N
B
u N " u
u •
u
u • •
u w ..
" • •
u
u •
tJ WN
u N
u f'lN"
u •
" r,•
IM I
p
p
r
p
p
p
p
p
r .. ,
,v
p
P'
p ..
P'
J:'
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937182 . I (_ \ .,
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U.S. EPA -CLP
1 CLIENT SAMPLE NO. INORGANIC ANALYSIS DATA SHEET
SW-12-1 Lab Name: COMPUCHEM LABORATORIES Contract: ~7~/~8~8c.,_ __ _ I
Lab Code: COMPU Case No.: 24520 SAS No.: SOG No.: 937182
Matrix (soil/water): WATER
Level (low/med):
% Solids:
-LOW
0. 0
Lab Sample IO: 367033
Date Received: 08/25/90
Concentration Units (ug/L or mg/kg dry weight): UG/L
jCAS No.
Ta7g ~n...:c,
744U-jt>-0
74.fl!-"1-L
7440-39-3
,4dll-TI-7
'44 -4 -9
'44 -7 -2
'44 -4 -3
7440-48-4
TI40-50-8
7439-89-6
f4jY-9.l-1
74jY-95-4
1439-9() :c,
74jY-97-6
14 4l!-lf2-o
7440-09-7
'77BL-49-L
7440-22-4
TT40-L3-:,
7440-28-0
TT 4 0-0 2...: 2
7440-66-6
Color Before: COLORLESS
Color After: COLORLESS
Comments:
FORM l -PAGE 16
I Analyte jConcentrationlCI Q
ATuminum 99.
Antimonv · 29. Arsen1c z. Barium jtL
Be rvTl 1 um . cadmium 9.
Calcium 435 r:nromfum 4.0
Cobalt 4.0 Coooer 4. 0
Iron 539
Lead 3.0
Maanesium lYUU
Manaanese jj2
Mercurv • .l u Nickel 35.0
Potassium 5 .:~ u Se1enium j. 0
Silver 7. 0
Soaium ~040
Thallium z.o
Vana<11um 4'.0
Zinc 4. 0 Cvaniae
Clarity Before: CLEAR
Clarity After: CLEAR
!'ORM I -IN
•
N
N
B
UN"
B
u • u u • • a IN
B • • a
u •
U WN
tJ N
li WN
a •
0 N"
IM I
p
p
P' p
p
p
p
p
p
p
p
~
~
CV
p
p
P'
p
p
!'
p
p
NR
Texture:
Artifacts:
7/88
INORGANICS CASE 937182
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APPENDIX K
GROUND WATER MODEL CALCULATIONS AND
PARAMETER CALCULATIONS '
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I APPENDIX K
I GROUND WATER MODELING
-.Parameter estimation
I -Model calculations
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1) ACTUAL AND EFFECTIVE POROSITY:
The void ratio values presented in Table 4-3 were used to calculate values for actual
porosity of the materials sampled. The equation
n = _e_ (Freeze and Cherry, 1979, p. 38)
1 + e
was used to calculate actual porosity, where n = actual porosity and e = void ratio.
An average actual porosity of 0.52 was calculated (arithmetic average of calculated porosity
values for MW-11, MW-13, MW-14R, MW-08, MW-05, and MW--06). The effective porosity
of the media present is therefore anticipated to be less than 0.5.
The difference between the actual and effective porosity will be dependent on the degree
of sorting and cementation of the geologic medium. Porosities are reduced In poorly-sorted
materials. While it is true that the presence of fine particle sizes (silts and clays) will reduce
the porosity of a material, the porosity will remain fairly high where silts and clays comprise
a majority of the sample matrix. In general, silts and clays have higher porosities than
sands and gravels (Freeze and Cherry, 1979, p. 37 and Todd, 1980, p. 28).
Review of the grain size distribution curves indicated that for samples MW05-T1, MW08-
T1, and MW14R-T1, silts and clays comprise the majority of the matrix such that ground
water flow through fine-grained materials is expected to be dominant. For these samples,
the relatively higher porosity of the fine-grained materials has more of an effect on the
porosity than the degree of sorting. Sample MW11-T1 exhibits a poor degree of sorting
which would be expected to significantly reduce the porosity of the material.
Additionally, a review of published values of porosity, (Todd, 1980; Freeze and Cherry,
1979; and Mercer et. al., 1982) for various geologic media indicates that few materials have
reported porosity values on the order of 0.1. Materials having low reported porosities. are
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B
dissimilar to the saprolitic materials present at Macon/Dockery.· Therefore, a value of 0.2
for the effective porosity is considered to be conservative, yet reasonable.
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Calculated actual porosity values are as follows:
Reported
Well Number (Depth in Feet) Void Ratio
MW-11 (45) 1.13
MW-13 (58) 0.72
MW-14R (30) 0.93
MW-08 (38) 1.78
MW-05 (38.5) 1.74
MW-06 (39) 0.73
'
Calculated
Actual Porosity
0.53
0.42
0.48
0.64
0.64
0.42
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2) ORGANIC CARBON CONTENT:
NOTE:
foe = % organic carbon = (653)(10~)(100)
0.0653%
The materials present at the site have a wide range of Koc values. The
analytical model cannot accommodate a range, therefore the median value was
used.
Sample Number
MW-16-25-1
MW-14-25-1
MW-14-5-1
MW-7-45-1
Median
Site
L.D.
LM.
U.M.
U.M.
TOC (mg/kg)
1620
762
544
512
= 762 + 544 = 653
2
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3) ~ (DISTRIBUTION COEFFICIENT)
~ = l<ocfoc
Parameter
1, 1, 1-trichloroethane
1, 1-dichloroethene
1,2-dichloroethene
tetrachloroethene
trichlorethene
benzene
toluene
foe = 0.000653
!5oc... Jk_
178 0.116
65 0.042
59 0.039
363 0.237
126 0.082
83 0.054
250 0.163
Average = 0.105
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4) SOURCE TERM
Conceptually, the source of residual chemicals at the Site is best represented as an initial
concentrated slug (recharge to aquifer during active use of the lagoons) followed by a
continuous source at a lower concentration (continued loading to aquifer as infiltration
carries residual chemicals: downward to ground water).
Because of uncertainties in estimating the initial slug concentrations, the source term was
modeled as a continuous source having a single concentration over time. Toe source
concentration was set equal to the maximum ground water concentration (for •
tetrachloroethene at the Macon Site, for 1,1,1-trichloroethane at the Dockery Site, and for
a •generic' VOC intended to represent composite characteristics of seven VOCs). Source
flux was calculated by considering an idealized representative source area having a specific
amount of infiltration. moving through the source area to transport residual chemicals
downward.
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Source Concentrations:
Macon Site (from Table 5-50)
Tetrachloroethene
'Generic' voe•
Dockery Site (from Table 5-59)
1, 1, 1 ~ Trichloroethane
'Generic' VOC*
44 ug/L
549 ug/L
500 ug/L
1152 ug/L
* 'Generic' voe consists of the total of the maximum concentrations detected of the,
following seven compounds:
1, 1, 1-trichloroethane
1, 1-dichloroethene
1,2-dichloroethene
benzene
tetrachloroethene
toluene
trichloroethane
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Source Flux:
Macon Site:
Size: 21 o feet x 250 feet = 52,500 tt2
Recharge to Source Area:
Average annual precipitation
Average lake evaporation
6.2r = 0.52 feet per year
52,500 x 0.52 = 27,300 tt3tyear
Source distribution across 5 nodes:
48.2r (from RI text)
42.00" (approximate, from DeWiest, R.J. 1965.
6.2r Geohydrology, John Wiley and Sons,
NY)
27,300 tt3tyear = approximately 75 tt3/d = approximately 112 gpd/node
Dockery Site:
Size: 150 feet x 200 feet = 30,000 tt2
Recharge: 30,000 x 0.52 = 15,600 tt3tyear
Distribution across 4 nodes:
15,600 tt3tyear = approximately 43 tt3/d = approximately 80 gpd/node
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I CONMIG RESULTS .
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DATA BASE:
Number.of simulation periods for which contaminant
concentration distribution is to be calculated 2
Simulation period number• I
Simulation period duration in days• 1825.00
Simulation period number• 2
Simulation period duration in days= 3650.00
Number of grid columns= 20
Number of grid rows• 12
Grid spacing in ft= 50.00
X-coordinate of upper-left grid node in ft= 0.00
Y-coordinate of upper-left grid node in ft• 0.00
Aquifer actual porosity as a decimal• 0.400
Aquifer effective porosity as a decimal• 0.200
Simulation period number• I ·
Aquifer thickness in ft• 25.00
Aquifer·longitudinal dispersivity in ft= 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.21
Number of point sources• 5
Simulation period number• 2
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.21
Number of point sources• 5
Simulation·period number• I
Point source number·!
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 250.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in -,/1• 549.000
Time after continuous contaminant injection
started in days= 1825.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 300.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in)!g/1= -549.000
Time after continuous contaminant injection
started in days= 1825.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 350.00
·continuous point source injection rate in gpd= 112.00
Point source solute concentration in,M/1= 549.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft= 400.00
Continuous point source injection rate in gpd= 112.00
Point source solute concentration in1'i!/l• 549.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 5
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
' I.
V(X.,
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Continuous point source injection rate in gpd• 112.00
Point source solute concentration in il'9fl• 549.000
Time after continuous contaminant injection
started in days• 1825.00
Simulation period number• 2
Point source number I
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 250.00
Continuous point source injection rate in gpd= 112.00
Point source solute concentration in ~/1• 549.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 300.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in Jli'i/1• 549.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 350.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in i\ii/1• 549.000
Time after continuous contaminant infection ·
started in days• 3650.00
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd• 112.00.
Point source solute concentration in :,li/1• 549.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 5
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd= 112.00
Point source solute concentration in ~/1· 549.000
Time after continuous contaminant infection •
started in days= 3650.00
Bulk density of dry aquifer skeleton in g/cu cm• 1.50
Aquifer distribution coefficient in -rnl/g• .105
Number of monitor wells for which time-
concentration tables are desired• 0
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 1825.00
I VALUES OF CONTAMINANT CONCENTRATION (,MG/L) AT NODES:
J-ROW I-COLUMN
I 2 3 4 5 6 ·1 8
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 0.05 0.07 0. 10 0. 13 0. 14 0.00 0.00 0.00
4 1.00 I. 54 2.08 2.47 2.62 2.36 2.03 1.60
5 12.88 18.84 22.25 24.00 22.19 18.70 14. 71 10.76
I 6 284.90 130.28 IOI. 23 84.00 66.03 53.60 39.76 27.93
7 296.78 147.58 121. 40 105.53 85.60 69.94 52.44 37.09
8 297.69 148.98 123.27 107.75 87.93 72.30 54.47 38.69
9 296.78 147.58 121. 40 105.53 85.60 69.94 52.44 37.09
I 10 284.90 130.28 101.23 · 84.00 66.03 53.60 39.76 27.93
11 12.88 18.84 22.25 24.00 22. 19 18.70 14.71 10.76
12 1.00 1.54 2.08 2.47 2.62 2.36 2.03 1.60
I J-ROW I-COLUMN
9 10 11 12 13 . 14 15 16
4,,o 4,;.; 500 SSc
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 I. 15 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 5 7.32 3.87 2.25 0.00 0.00 0.00 0.00 0.00
6 18.46 10.66 6.12 0.00 0.00 0.00 0.00 0.00
7 24.63 14.53 8.38 0.00 0.00 0.00 0.00 0.00
8 25.78 14.53 8.38 0.00 0.00 0.00 0.00 0.00
I 9 24.63 14.53 8.38 0.00. 0.00 0.00 0.00 0.00
10 18.46 10.66 6. 12 0.00 0.00 0.00 0.00 0.00
II 7.32 3.87 2.25 0.00 0.00 0.00 o.oo 0.00
12 I. 15 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I J-ROW I-COLUMN
17 18 19 20 21 22 23 24
I I 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 '
I 4 0.00 0.00 0.00 0.00
5 0.00 o.oo 0.00 0.00
6 0.00 o.oo 0.00 0.00
7 0.00 0.00 0.00 0.00
I 8 0.00 0.00 0.00 0.00
9 0.00 0.00 0.00 0.00
10 0.00 0.00 0.00 0.00
11 0.00 0.00 0.00 0.00 ii 12 0.00 0.00 0.00 0.00
I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 3650.00
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I VALUES OF CONTAMINANT CONCENTRATION (JIG/L) AT NODES:
J-ROW I-COLUMN
I 2 3 4 5 6 7 8
I f(t.1/"" " Su /CC 1:::c.. Z.<., ... _,c ,3.... ... .!~<.:
I 0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 Sc 0.03 0.04 0.06 0.09 0 .12 0. I 5 0. 18 0.21
3 '"' 0. 28 0.44 0.65 0.91 I. 18 1.44 1.67 1.83
I 4 15, 2.28 3.57 5.09 6.68 8. 13 9.29 10.04 10.35
5= 16.74 25.06 31.85 37.95 40.11 40.53 39.60 37.57
6-'5J 292.83 143.60 119.10 109.71 IOI. 30 96.57 88.32 79.85
7 ,,,_, 307. 27 165.05 145.79-140.89 133.16 127.66 117. 69 106.87
I 8 JS, 309. 02 167.77 149.63 145.84 139.05 134.22 124.58 113.77
9 =307.27 165.05 145.79 140.89 133.16 127.66 117.69 106.87
10-<D 292.83 143.60 119.10 109.71 IOI. 30 96.57 88.32 79.85
I II ,i;u 16.74 25.06 31.85 37.95 40.11 40.53 . 39.60 37 .57
12 si:o 2.28 3.57 5.09 6.68 8.13 9.29 10.04 10.35
J-ROW I-COLUMN
I 9 10 II 12 13 14 15 16
i:::l'f' _, ➔~o ♦S'c So,.;, SSv (,o., 6!fC 7oc 7'5"-=
I 0.00 o.oo 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 1.68 1.67 ·I. 58 I. 43 0.00 0.00 0.00 0.00
4 9.98 9.43 8.57 7.50 5.08 · 4. 10 0.00 0.00
5 34.45 30.89 26.91 22.76 17 .41 13.77 7.34 0.00
6 70.83 61. 77 52.66 43. 77 34.14 26.72 17 .09 0.00
I 7 95.30 83.23 71 .00 59.02 46.46 36.39 24.43 0.00
8 IOI. 91 89.32 76.41 63.66 51.55 40.49 24.43 0.00
9 95.30 83.23 71.00 59.02 46.46 36.39 24.43 0.00
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10 70.83 61.77 52.66 43.77 34. 14 26.72 17.09 0.00
II 34.45 30.89 . 26.91 22.76 17 .41 13.77 7.34 0.00
12 9.98 9.43 8.57 7.50 5.08 4. 10 0.00 0.00
I J-ROW I-COLUMN
17 18 19 20 21 22 23 24
I 0.00 0.00 0.00 0.00
I 2 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00
5 0.00 0.00 0.00 0.00
I 6 0.00 0.00 0.00 0.00
7 0.00 0.00 0.00 0.00
8 0.00 0.00 0.00 0.00
I 9 0.00 0.00 0.00 0.00
10 0.00 0.00 0.00 0.00
II 0.00 0,00 0.00 0.00
12 0.00 0.00 0.00 0.00
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DAT-A BASE:
Number of simulation periods for which contaminant
concentration distribution is to be calculated 2
Simulation period number• I
Simulation period duration in days• 1825.00
Simulation period number• 2
Simulation period duration in days• 3650.00
Number of grid columns• 16
Number of grid rows• 16
Grid spacing in ft• 50.00
X-coordinate of upper-left grid node in ft• 0.00
Y-coordinate of upper-left grid node in ft• 0.00
Aquifer actual porosity as a decimal• 0.400
Aquifer effective porosity as a decimal• 0.200
Simulation period number• I
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.21
. Number of point sources• 5
Simulation period number• 2
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.21
Number of point sources• 5
Simulation period number• I
Point source number .I
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 350.00
Continuous point source injection rat1L,in gpd• 112.00
Point source solute concentration in tlij'/1• 44.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in "/1• 44.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in i/igyl-44.000
Time after continuous contaminant injection ·
started in days• 1825.00
Point source number 4
.X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 500.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in "/1• 44.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 5
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 550.00
PC£
5
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Continuous point source injection
Point source solute concentration
Time after continuous contaminant
started in days• 1825.00
Simulation period number• 2
Point source number 1
ratl\_.in gpd• 112.00
in Jtig/1• 44.000
injection
X-coordinate of point source in ft= 0.00
Y-coordinate of point source in ft• 350.00
Continuous point source injection rate in gpd= 112.00
Point source solute concentration in !Ag'/1= 44.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
·continuous point source injection rate in gpd• 112.00
Point source solute concentration in a,g/1· 44.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration inJtg/1• 44.000
Time after continuous contaminant injection
started in days= 3650.00
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 500.00
Continuous.point source injection rat~in gpd• 112.00
Point source solute concentration in,)11!1/l• 44.000
Time after continuous contaminant inJection
started in days-3650.00
Point source number 5
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 550.00
Continuous point source injection rate in gpd• 112.00
Point source solute concentration in~/1• 44.000
Time after continuous contaminant injection
started in days• 3650.00
Bulk density of dry aquifer skeletonJ~ g/cu cm= 1.50
Aquifer distribution coefficient inf'llg= .237
Number of monitor wells for which time-
concentration tables are desired• 0
6
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS:. 1825.00
I VALUES OF CONTAMINANT CONCENTRATION (~/L) ~T NODES:
J-ROW I-COLUMN
I I 2 3 4 5 6 7 8
~--0 50 \00 ,s:o .,., tso 300 = I <> 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 50 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 IC» 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 15<> 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 -0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 ""' 0.01 0.02 0.03 0.04 0.04 0.00 0.00 0.00
I 7 ,.., 0.57 0.95 I. 18 1.16 0.96 0.65 0.39 0.21
8'51> 27.53 11. 45 8.23 6.17 4.27 2.69 I. 53 0. 77
9 ~ 28.09 12.38 9.38 7.29 5.19 3.33 I. 92 0.98
I 10 4SO 28.10 12.40 9.41 7.33 5.23 3.33 1.92 0.98
II ... 28.09 12.38 9.38 7.29 5.19 3.33 I. 92 0.98
12 ss,, 27 .53 11.45 8.23 6. 17 4.27 2.69 1.53 0. 77
13 -0.57 0.95 I. 18 I. 16 0.96 0.65 0.39 0.21
I 14 i.so 0.01 0.02 0.03 0.04 0.04 0.00 0.00 0.00
15 .,.., 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
16 1So 0.00 0.00 0.00 0.00 o.cio 0.00 0.00 0.00
I J-ROW I-COLUMN
9 10 II 12 13 14 15 16
4oo
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
. 4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
7 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
8 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 9 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
10 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
11 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
12 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 13 0.00 0.00 0.00 0.00 : 0. 00 0.00 0.00 0.00
14 0.00 0.00 0.00 0.00 0.00 0.00 0.00 · 0.00
15 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 16 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 3650.00
I VALUES OF CONTAMINANT CONCENTRATION (~/L) AT NODES:
J-ROW I-COLUMN
I 1 2 3 4 5 6 7 8
1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 0.00 0.00 0.01 0.01 0.02 0.02 0.00 0.00
I 6 0.05 0.10 0.16 0.22 0.27 0.31 0.30 0.29
7 0.85 1.47 2.02 2.36 2.49 . 2. 44 2.22 I. 92
8 28.26 12.81 10.22 9.34 8.23 7.18 6.09 5.00
9 29.06 14.18 12.08 1 I. 49 10.45 9.30 8.00 6.63
I 10 29.10 14.27 12.22 11.68 10.69 9.58 8.31 6.91
11 29.06 I4.18 12.08 1 I. 49 10.45 9.30 8.00 6.63
12 28.26 12.81 10.22 9.34 8.23 7.18 6.09 5.00
13 0.85 I. 47 2.02 2.36 2.49 2:44 2.22 1.92
I 14 0.05 0.10 0.16 0.22 0.27 0.31 0.30 0.29
15 0.00 0.00 0.01 0.01 0.02 0.02 0.00 0.00
16 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I J-ROW I-COLUMN
9 10 11 12 13 14 15 16
4oo 4So Soo SSo -i,So -
I 1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 0.25 0.00 0.00 0.00 0.00 0.00 0.00 0.00
7 1. 57 1.00 0.71 0.00 0.00 0.00 0.00 0.00
8 3.93 2.73 1.92 0.00 0.00 0.00 0.00 0.00
I 9 5.24 3.73 2.63 0.00 0.00 · 0.00 0.00 0.00
10 5.49 3.73 2.63 0.00 0.00 0.00 0.00 0.00
11 5.24 3.73 2.63 0.00 0.00 0.00 0.00 0.00
12 3.93 2.73 1.92 0.00 0.00 0.00 0.00 0.00
I 13 1. 57 1.00 0. 71 0.00 0.00 0.00 0.00 0.00
14 0.25 0.00 0.00 0.00 0.00 0.00 0.00 0.00
15 0.00 o.oo 0.00 0.00 0.00 0.00 0.00 0.00
I 16 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
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DATA BASE:
Number of simulation periods for which contaminant
concentration distribution is to be calculated 2
Simulation period number• 1
Simulation period duration in days• 1825.00
Simulation period number= 2
Simulation period d\Jration•in days= 3650.00
Number of grid columns• 16
Number of grid rows• 12
Grid spacing in ft• 50.00
X-coordinate of upper-left grid node in ft• o;oo
Y-coordinate of upper-left grid node in ft• 0.00
Aquifer actual porosity as a decimal• 0.400
Aquifer effective porosity as a decimal• 0.200
Simulation period number• 1
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day-0.16
Number of point sources• 4
Simulation period number• 2
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft-70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.16
Number of point sources• 4
Simulation period number• 1
Point source number· 1
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft-350.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in ~/l• 1152.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in Jig/1 • 1152. 000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in ~/1= 1152.000
Time after continuous contaminant injection
· started in days• 1825.00
Point source number 4
X-coordinate of point source in i'• 0.00
Y-coordinate of point source in '! · 500.00
Continuous point source injectio:. rate in gpd• 80.00 ·
Point source solute concentration in plg/1· 1152.000
Time after continuous contaminant injection
started in days• 1825.00
Simulation period number• 2
Point source number 1
X-coordinate of point source in ft-0.00 q
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Y-eoordinate of point source in ft• 350.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in )llg/1• 1152.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 2
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd= 80.00
Point source solute concentration in ~/1• 1152.000
Time after continuous contaminant injection·
started in days• 3650.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd= 80.00
Point source solute concentration in -tlg/1• 1152.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 500.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in ,ift/1• 1152.000
Time after continuous contaminant injection
started in days• 3650.00
Bulk density of dry aquifer skeleton in g/cu cm• 1.50
Aquifer distribution coefficient in ml/g• .105
Number of monitor wells for which time-
concentration tables are desired• 0
ID
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 1825.00
I VALUES OF CONTAMINANT CONCENTRATION (p!G/L) AT NODES:
J-ROW I -COLUMN
I 2 3 4 5 6 7 8
I 0 ... -,,o -'-"' J<,, 3:so
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 0.00 0.00 0.00 0.00 0.00 0.00 Q_QQ 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 I.OS 1.64 2. 12 2.35 2.27 I. 91 1.42 0.00
I 7 20.56 29.37 31. 79 34.19 28.76 21.63 14.68 8.07
8 549.32 239. I 9 175. 20 134.67 99.67 69.46 44.50 25.31
9 568.80 266.92 204.87 166.51 126.16 89.18 57.75 33.38
IO 568.80 266.92 204.87 166.51 126.16 89.18 57.75 33.38
I II 549.32 239. 19 175.20 134.67 99.67 69.46 44.50 25.31
12 20.56 29.37 31. 79 34. 19 28.76 21.63 14.68 8.07
I
J-ROW I-COLUMN
9 IO II 12 13 14 ... 15 16
-WO ... 5i,o
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 6 0.00 0.00 0.00 0.00 0.00 0.00 o_oo 0.00
7 4.44 o_oo 0.00 0.00 0.00 0.00 0.00 0.00
8 13.61 4.45 0.00 0.00 0.00 0.00 0.00 0.00
9 18.06 4.45 0.00 0.00 0.00 0.00 0.00 0.00
I 10 18.06 4.45 0.00 0.00 0.00 0.00 0.00 0.00
II 13.61 4.45 0.00 0.00 0.00 0.00 0.00 0.00
12 4.44 0.00 0.00 0.00 0.00 0.00 0.00 0.00
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,.'
I , ,,.
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 3650.00
I VALUES OF CONTAMINANT CONCENTRATION (,IIG/L) AT NODES:
J-ROW I-COLUMN
2 3 4 5 6 7 8
I I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.02 0.03 0.05 0.00 0.00 0.00 0.00 0.00
5 0.33 0.53 0.76 0.96 1.19 1.38 1.48 1.49
6 3. 57 5.57 7.82 9.90 11. 57 12.54 12.70 12.09
I 7 30.69 45.68 57.07 65.75 66.95 64.41 59.17 52. 10
8 571. 84 275.44 224.26 200.82 178.45 161.89 139.66 117. 57
9 598.65 315.06 272.79 255. 71 232.63 212.38 184.65 156.09
10 598.65 315.06 272.79 255.71 232 .63 212.38 184.65 156.09
I II 571.84 275.44 224.26 200.82 178.45 161.89 139.66 117.57
12 30.69 45.68 57.07 65.75 66.95 64.41 59.17 52.10
J-ROW I-COLUMN
I 9 10 11 12 13 14 IS 16
4"" ♦So -SS'o ,.o •s"
l 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00· 0.00 0.00 0.00 0.00 0.00 0.00
s 1.41 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 6 10.87 7.99 6.41 4."88 0.00 0.00 0.00 0.00
7 44.01 34.38 26.58 19.65 10.35 0.00 0.00 0.00
8 96.06 74.59 56.62 41.28 25.30 0.00 0.00 0.00
9 127.78 100.98 76.79 56.05 35.65 0.00 0.00 0.00
I 10 127.78 100.98 76.79 56.05 35.65 0.00 0.00 0.00
II 96.06 74.59 56.62 41.28 25.30 0.00 0.00 0.00
12 44.01 34.38 26.58 19.65 10.35 0.00 0.00 0.00
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DATA BASE:
Number of simulation periods for which contaminant
concentration distribution is to be calculated 2
Simulation period number• 1
Simulation period duration in days= 1825.00
Simulation period number=·2
Simulation period duration in days= 3650.00
Number of grid columns= 16
Number of grid rows= 12
Grid spacing in ft• 50.00
X-coordinate of upper-left grid node in ft= 0.00
Y-coordinate of upper-left grid node in ft• 0.00
Aquifer actual porosity as a decimal• 0.400·
Aquifer effective porosity as a decimal• 0.200
Simulation period number• 1
Aquifer thickness in· ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day• 0.16
Number of point sources• 4
Simulation period number• 2
Aquifer thickness in ft• 25.00
Aquifer longitudinal dispersivity in ft• 70.00
Aquifer transverse dispersivity in ft• 7.00
Seepage velocity in ft/day-0.16
Number of point sources• 4
Simulation period number• 1
Point source number ·l
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 350.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in !WJ/1• 500.000
Time after continuous contaminant inJection
started· in days• 1825.00
Point source number 2
·x-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in )119/1= 500.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration inJ!!g/1= 500.000
Time after continuous contaminant injection
started in days• 1825.00
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 500.00
Continuous point source injection rate in gpd• 8,J 00
Point source solute concentration in ,1119/l• 500.000
Time after continuous contaminant injection
started in days= 1825.00
Simulation period number• 2
Point source number· 1
X-coordinate of point source in ft• 0.00
I I I· 1"CA I I
1),xwj ~iil
~CL /!,iu, > I¼. l"'<.LM
~RM w..+u ~'"'·""
13
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Y-coordinate of point source in ft• 350.00
Continuous point source injection rat\;.in gpd• 80.00
Point source solute concentration in 4ilg/l• 500.000
Time after continuous contaminant injection
started in days• 3650.00
Point source number 2
X-coordinate of point source in ft= 0.00
Y-coordinate of point source in ft• 400.00
Continuous point source injection rate in gpd= 80.00
Point source solute concentration in ~/l• 500.000
Time after continuous contaminant injection
started in days= 3650.00
Point source number.3
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 450.00
Continuous point source injection rate in gpd• 80.00
Point source solute concentration in 4/1• 500.000
Time after continuous contaminant injection
started in days• 3650.00 ·
Point source number 4
X-coordinate of point source in ft• 0.00
Y-coordinate of point source in ft• 500.00
Continuous point source· injection rate in gpd• 80.00
Point source solute concentration in ~/1= 500.000
Time after continuous contaminant injection
started in days• 3650.00
Bulk density of dry aquifer skeleton in g/cu cm• 1.50
Aquifer distribution coefficient in ml/g• .116
Number of monitor wells for which time-
concentration tables are desired• 0
J4
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I NODAL COMPUTATION RESULTS:
SIMULATION PERIOD DURATION IN DAYS: 1825.00
I VALUES OF CONTAMINANT CONCENTRATION (JIG/L) AT NODES:
J-ROW I-COLUMN
I 2 3 4 5 6 7 8
I 0 So -,.., ... .... -350
I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 0.40 0.61 0.79 0.88 0.84 0.69 0.50 0.00
I 7 8.38 12.05 12.87 14.11 11.72 8.65 5.72 3.07
8 242.66 104.54 75.68 57.43 42.50 28.66 17.88 9.88
9 250.64 115.98 87.75 70.66 53.39 36.61 23.09 12.96
10 250.64 115. 98 87.75 70.66 53.39 36.61 23.09 12.96
I II 242.66 104.54 75.68 57.43 42.50 28.66 17 .88 9.88
12 8.38 12.05 12.87 14.11 11. 72 8.65 5.72 3.07
I J-ROW I-COLUMN
9 10 II 12 13 14 15 16
4oo ·~ I 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 2 0.00 ·0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 o.oo
5 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 6 0.00 0.00 0.00 0.00 0.00 0.00 0.00 o.oo
7 1.6~ 0.00 0.00 0.00 0.00 0.00 0.00 0.00
8 5.11 0.00 0.00 0.00 0.00 0.00 0.00 0.00
9 6.74 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 10 6.74 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I I 5.11 0.00 0.00 0.00 0.00 0.00 0.00 0.00
12 1.63 0.00 0.00 0.00 0.00 0.00 0.00 0.00
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•• NODAL COMPUTATION RESULTS: .
SIMULATION PERIOD DURATION IN DAYS: 3650.00
I VALUES OF CONTAMINANT CONCENTRATION (jlG/L} AT NODES:
I J-ROW I-COLUMN
l 2 3 4 5 6 7 8
.1 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
t 2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
3 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
5 0.11 0.18 0.26 0.35 0.44 0.51 0.54 0.54
'
6 1.38 2.18 3.09 3.95 4.63 5.00 5.04 4.75
7 12.74 19. 18 24.09 27.84 28.29 27.09 24.70 21.52
8 252.57 120.61 97.77 87. 16 79.64 69.46 59.42 49.48
9 263.82 137.44 118.51 110.69 102.87 91.05 78.54 65. 71
I 10 263.82 137.44 118.51 110. 69 102.87 91.05 78.54 65. 71
11 252. 57 120.61 97.77 87.16 79.64 69.46 59.42 49.48
12 12.74 19. 18 24.09 27.84 28.29 27.09 24.70 21.52
I J-ROW I-COLUMN
9 10 11 12 13 14 15 16
4,<, 5,, sr.:.: <.GO ,so
I I 0.00 0.00 0.00 0.00 0.00 0.00 · 0.00 0.00
2 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ·
3 0.00 0.00 0:00. 0.00 0.00 0.00 0.00 0.00
4 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
I 5 0.51 0.00 0.00 0.00 0.00 0.00 0.00 0.00
6 4,22 3.09 2.43 0.00 0.00 0.00 0.00 0.00
7 17 .94 13.84 10.50 5.78 3.94 . 0.00 0.00 0.00
8 39.88 30.53 22.73 14.39 9.74 0.00 0.00 0.00
I 9 53.09 41.28 30.79 20.16 13.69 0.00 0.00 0.00
10 53.09 41. 28 30.79 20.16 13.69 0.00 0.00 0.00
11 39.88 30.53 22.73 14.39 9.74 0.00 0.00 0.00
I 12 17.94 13_.84 10.50 5.78 3.94 0.00 0.00 0.00
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~ t /J