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HomeMy WebLinkAboutNCD980799019_19961001_Cherokee Oil_FRBCERCLA PASI_Integrated Preliminary Assessment Site Inspection Volume II - References 1 - 42-OCRI I I I I I I I :., I" I I I I I I STATE OF NORTH CAROLINA Department of Environment, Health, and Natural Resources Division Waste Management Super.fund Section INTEGRAIED PRELIMINARY ASSESSMENT/SITE INSPECTION VOLUME II Cherokee Oil Company NCD 980 799 019 Charlotte, Mecklenburg Co.,NC Reference No. 06174 October 1996 Douglas Moore Environmental Engineer Division Waste Management Superfund Section I le I I I I I I I 1• I I I I I I •• I .I I. 2. 3. 4. 5. 6. 7. 8. 9. Cherokee Oil Company 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCO 980 799 019 References Latitude/Longitude Calculation worksheet for the Cherokee Oil Company Site, US EPA ID: NCD 980 799 019. August 2, 1995. United States Department of Commerce. Technical Paper No. 40: Rainfall Frequency Atlas of the United States. Issued 1961. United States Department of Commerce. Climatic Atlas of the United States. National Climatic Center, Asheville, NC. 1979. Real Estate Detail Summary. Map Book# 71, Block# 5 I, Parcel # I 6. Charlotte- Mecklenburg Tax Department Public Access System inquiry printout. August 09, 1995. Moore, Douglas B., Environmental Chemist, NC Superfund Section. Memo to File. Topic: Preliminary Assessment Site Reconnaissance: Cherokee Oil Company, 1201 Berryhill Road, Charlotte, Mecklenburg Co., NC. US EPA ID: NCO 980 799 019. August 11, 1995. Attachments. Summary of activities and violations (1985-1990). Cherokee Oil Company. Mecklenburg County Department of Environmental Protection files. Moore, Douglas B., Environmental Chemist, NC Superfund Section. Memo to File. Topic: Ownership Information. Cherokee Oil Company Site. 1201 Berryhill Road. Charlotte, Mecklenburg County, N.C. US EPA ID: NCO 980 799 019. August 11, 1995. {) Division of Solid Waste Management -Hazardous Waste Section files. Letter to O.W. Strickland from Keith Eidson, Southtec Corporation. September 24, 1983. South Carolina Department of Health and Environmental Control, Bureau of Solid and Hazardous Waste Management. Hazardous Waste Transporter Permit Conditions. October 23, I 987. Moore, Douglas B., Environmental Chemist, NC Suoerfund Section. Memo to File. Topic: Secretary of State -Business Information. Cherokee Oil Company, 1201 Berryhill Road, Charlotte, Mecklenburg Co., N.C. US EPA ID: NCD 980 799019. August 11, 1995. I le I I I I I I I 1• I I I I I I •• I I 10. II. 12. 13. 14. 15. 16. 17. 18. 19. Action Memorandum. Request for a Removal Action at the Cherokee Oil - Berryhill Road Site, Mecklenburg County, North Carolina. From: Steve Spurlin, OSC -Emergency Response and Removal Branch. To: Joseph R. Franzmathes, Director, Waste Management Division. September 19, 1994. Moore, Douglas B., Environmental Chemist, NC Superfund Section. Memo to File. Topic: Discharge Permits. Cherokee Oil Site, 925 South Summit Ave. Charlotte, NC NCO 986 190 239. May 18, 1993. United States of America v. Cherokee Resources, Inc., Keith Norland Eidson, Gene Wesley (Gabe) Hartsell and Theodore Karl Glauser. Criminal No. 3:93CR186. United States District Court, Western District of North Carolina (Charlotte). Criminal Docket for Case #: 93 -CR -186 -ALL. USA v. Cherokee, et al. Filed 08/05/93. Docket as of February 12, 1996 3:34 pm. Moore, Douglas B., Environmental Chemist, NC Superfund Section. Memo to File. Topic: Follow-Up On-Site Reconnaissance. Cherokee Oil Company, 1201 Berryhill Road, Charlotte, Mecklenburg Co., N.C. US EPA ID: NCO 980 799 019. December 22, 1995. AquaChem Environmental Laboratories, Inc. Pineville, N.C. Chain of Custody documents and analytical results for OHM Corporation's "Cherokee Oil" Project samples CO-WS-16 and CO-WS-17. Date shipped: October 24, 1995. Report Date: November 28, 1995. Moore, Douglas B., Environmental Chemist, NC Superfund Section. Memo to File. Topic: Site Inspection -Sampling Trip. Cherokee Oil Company, 1201 Berryhill Road, Charlotte, Mecklenburg County, N.C. US EPA ID: NCO 980 799 019. March 15, 1996. Superfund Chemical Data Matrix (SCDM). Appendix B-1, Tables for Non- Radioactive Hazardous Substances. August 19, 1996. Savannah Laboratories, and Environmental Services, Inc., Savannah Georgia. Chain of Custody documents and analytical results for OHM Corporation's "Cherokee Oil" Project samples CO-WS-33, CO-WS-34, CO-WS-35, CO-WS-36, CO-WS-37 and CO-WS-38. Date shipped: December 04, 1995. Report Date: December 07, 1995. AquaChem Environmental Laboratories, Inc. Pineville, N.C. Chain of Custody documents and analytical results for OHM Corporation's "Cherokee Oil" Project sample CO-WS-31. Date shipped: November 30, 1995. Report Date: December 14, 1995. I •• I I I I I I I •• I I I I I I •• I I 20. AquaChem Environmental Laboratories, Inc. Pineville, N.C. Chain of Custody ,documents and analytical results for OHM Corporation's "Cherokee Oil" Project sample CO-WS-28. Date shipped: November 21, 1995. Report Date: December 07, 1995 21. Moore, Douglas B. Letter to Mr. Tom Broom, Suburban Propane District Office. Subject: Soil Sample Analytical Results. Cherokee Oil Company, Charlotte, Mecklenburg County, NC US EPA ID: NCD 980 799 019. July 31, 1996. 22. North Carolina Geological Survey, Division of Land Resources, Department of Natural Resources and Community Development, Geologic Map of North Carolina, 1985. 23. The Hydrogeologic Framework and a Reconnaissance of Ground Water Quality in the Piedmont Province of North Carolina. with a design for future study. by Douglas Harned. U.S. Geological Survey, Water Resources Investigations Report 88-4130. Raleigh, North Carolina. 1989. 24. Phase III Assessment Exploration. General Electric Service Shop. Charlotte, North Carolina. Vol. I. Law Environmental. December, 1988 . 25. Law Environmental, Inc., Letter to Mr. John T. Harrsen. Manager, Remedial Programs. General Electric Company. Subject: Report of Ground-Water Sampling and Analyses. General Electric Appartus Service Shop. 2328 Thrift Road. Charlotte, North Carolina. Law Engineering and Environmental Services Project 13210-5-5010. March 31, 1995. 26. Moore, Douglas, Environmental Chemist, NC Superfund Section, Memo to File. Topic: Intakes for the Charlotte Mecklenburg Water System, Dynatech Industries, Inc., NCD 981014517. January 25, 1993. 27. Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Subj: Groundwater use within a 4.0 mile radius. Cherokee Oil Company, 1201 Berryhill Road, Charlotte, Mecklenburg Co., NC. US EPA ID: NCD 980 799 019. August 9, 1996. w/attachments. 28. Stanley, Jeanette. Environmental Chemist, NC Superfund Section. Memo to Superfund Section Staff. Subj.: Update on Status of Wellhead Protection Programs in N.C. January 2, 1996. 29. Federal Emergency Management Agency. Flood Insurance Rate Maps. City of Charlotte, Mecklenburg County, North Carolina. Community Panels No. 370159 0008B (February 26, 1982), 370159 0012C (January 6, 1994), and 370159 0013B (February 26, 1982). I •• I I I I I I I •• I I I I I I •• I I 30. 3 I. 32. 33. 34. 35 . 36. 37. 38. 39 . Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Subject: Flow calculations, Cherokee Oil Company Site, 1201 Berryhill Road, Charlotte, Mecklenburg County, NC US EPA ID: NCO 980 799 019. August 9, 1996. w/attachments. Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Subject: Fisheries in Stewart Creek. Cherokee Oil Company Site, 1201 Berryhill Road, Charlotte, Mecklenburg County, NC US EPA ID: NCO 980 799 019. August 4, 1995. U.S. Department of the Interior, Fish and Wildlife Service. 1:24000 scale National Wetland Inventory Maps of Charlotte East, NC, Charlotte West, NC, Derita, NC and Mountain Island Lake, NC. U.S. Department of Agriculture, Soil Conservation Service. Soil Survey of Mecklenburg County, North Carolina. Issued June 1980. U.S. Department of Agriculture, Soil Conservation Service. Hydric Soils of North Carolina. Technical Guidance, Section 11-A-2. June 1992. Lund, Steven, Project Manager, U.S. Army Corps of Engineers, Wilmington District. Notification of Jurisdictional Determination. 0.4 mile segment of an unnamed tributary to Stewarts Creek between Berryhill Road and the confluence with Stewarts Creek parallel to Freedom Road at Charlotte. November 07, 1995. Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Topic: NC Natural Heritage trip report. Cherokee Oil Site, NCO 986 190 239. June 3, 1993. Keferl, Eugene P. and Rowland M. Shelley, The Final Report on a Status SUrvey of the Carolina Heelsplitter, Lasmigona decorata and the Carolina Elktoe, Alasmindonta robusta. Prepared for the United States Department of the Interior, Fish and Wildlife Service and the North Carolina State Museum of natural Science. July 9, 1988. Attachment I: North Carolina Nautral Heritage Program, Observation reports for L. decorata, Carolina Heelsplitter for Irwin/Sugar Creek, Charlotte, Mecklenburg County, North Carolina. 1987. Moore, Douglas, Environmental Chemist, NC Superfund Section. Memo to File. Topic: Irwin/Sugar creek endangered species, Cherokee Oil Site, NCO 986 190 239. June 7, 1993. North Carolina State Center for Geographic and Information Analysis. Population table for distance rings within a 4 mile radius of the Cherokee Oil Company Site, US EPA ID: NCO 980 799 019. August 18, 1995. I •• I I I I I I I 1• I I I I I I •• I I 40. 41. 42. Spurlin, Steve, On-Scene Coordinator, US EPA Region IV. Letter to Mr. Dwayne Alexander, VP. Rhyne, Alexander and Mattox Realty Co., Re: EPA information related to property at 2401 Tuckaseegee Road owned by Mr. Gene Miller. March 08, 1995. North Carolina Hazardous Waste Management Rules, Title 15A, NCAC, Chapter 13, Subpart B, Section 261.24, January 1, 1996. Memorandum to State Directors, State Authorization Contacts, RPS Unit Chiefs, RCS Unit Chiefs From: Al Hanke, Chief, State Programs Section. Subject: Guidance on Residential Lead-Based Paint, Lead-Contaminated Dust, and Lead Contaminated Soil and Revised Interim Soil Lead Guidance for CERCLA sites and RCRA Corrective Action Facilities. November 16, 1994. I I I I I I I It I I I I I I I LATITUDE AND LONGITUDE CALC(}LATION WORKSHEET 1-2 LI USING ENGiNEER'S SCALE (l/60) SITE NAHE: {¼l"fl2h<< /J// ()z<"}oa,iy cERcLrs 1, NC]> qso 711 01'1 /\KA '---------------~--------SSID : _____________ _ ADDRESS: /:ZO/ ~rruh/// J?oac/ ) ZIP CODE: CITY: C/4,:,,r/CI lftc STATE:_/1/_C_. __ _ ---------- uses QUAD KAP NAH.E: (Al(r/ol/<.. Af-U-1 t',/C TOWNSHIP: N/S RANGE:. E/W SCALE:~· SECTION: 1/4 1/4 1/4 KER IO IAN: HAP DATUH: (29W 1983 (CIRCLE ONE) -------------·----- COORDINATES FROH LOWER RIGHT {SOUTHEAST) CORHER OF 7.5' HAP (.J.t.t.?...ch phor:ocopy): LONGITUDE: 80 ° 5',;;J.. ' 30 " LATITUDE: 35 o 07 ' 30 ., COORDINATES FROH LO½TR RIGHT (SOUTHEAST) CORNER OF 2.5' GRID CELL: LONGITUDE: LATITUDE: 35 o / ,;2. 30 " CALCULATIONS: LATITUDE (7.5' QUADRANGLE KAP) · ~30 A) NUMBER OF RULER GR .. ADUATIONS FROK LATITUDE GRID LINE TO SlTE REF POINT: 8) HULTIPLY (A) BY 0.3304 TO CONVERT TO SECONDS: AX 0.3304 C) E:XPRESS IN HI!WTES AND SECONDS (l'= 60"): 0/ '.tf·-/_. 00 " D) ADD TO STARTING LATITUDE: '35' 0 /J_ ' 30 .. 00 " ~ .EL_' n .. (!JO SITE LAT'TUDE: 35 o_ ftf ·.i__. Q?" CA.LCULAYIO!JS: LOl~GITUDE ( 7. S' QUA.DRANGLF: HJ\P) A) i/U!-iBER OF .AULER GRADUATIONS FROM _RIGHT Lot;GITUDE LIUE TO ST Tl·~ KEF' POI.NT: e) B) HULTI?LY (A) BY 0.JJO~ TO CONVERT TO SECONDS: C) E:XP?.ESS Ill ~.r:;uTSS .:..HO SECOi~D.S ( l · ;.~ SO" 1: O , o ___ q___ D) ,'.DD TO S'!';--..HTI:~G LO!iCITUDE: B"o·o.,..;t __ ·3o . OC) SITE LQJ:CJTVDE: -·----7 ,ao 0 >:l. ·3o .o"' " I ---• ___ _J -. I---- ) I I I I I I I I I I I I I ,- I T0POGR.'d'HIC ,\lAI' QUADRANGLE t<,\.',1E: __ lj4,,-./o-ffr ~-q/--f/C-~~-~---'--'--,'---'-_:_:::.__ ___ _ COORD!N.•\TE..) OF LO',VER RlGf-rI'-HA1",'D CORNf:R OF :1..5-,',iih'UTE GRID: LATiTUD:-: 35 ° f.?._· JU_· LOi','GfTUDE: fu_,;; f.;i. · 30 __ · ~-.-----------■------«;--On ·. l!f/',;:,i:,11:r;T OF co~1~11-:11cE ·•t""' :;. 11111,c;t ... ~ .. ,..,1_~r7 "l:ATlll•:1: 111/ltJ•:A,, r.-..·_ H,1111,1:,,111 1"_ 1 :.;,, ,, I TECIINICAL PAPEH NO. ,10 I ,' JfAINFALL FJ?EQUENCY A'J'LAS or 'f'J IE l JNl'l'EI) S'IA'l'ES fur Duratio11s fron1 30 Mi1111lc3 lo 2,1. 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I I I , I I I I I I It I I I I I I I ,, I Memo Date: August 11, 1995 To: File From: Douglas Moore /Jiu~ 6-(/4(--..._ Environmental Chemist NC Superfund Section Topic: Preliminary Assessment Site Reconnaissance Cherokee Oil Company 120 I Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCO 980 799 019 On Wednesday, August 9, 1995, Doug Moore and Doug Rumford of the NC Superfund Section traveled to Charlotte to conduct a preliminary assessment reconnaissance of subject site. We departed Raleigh at 0800 and arrived in Charlotte around 1100. At I 100, we drove to the Charlotte Mecklenburg Utilities Department (CMUD) on Brookshire Freeway and met with Bob Griffin of the Systems Protection Division. Mr. Griffin indicated that the principals, Gene Hartsell and Keith Eidson, have been convicted on charges of conspiracy to violate the Clean Water Act by violating their pre-treatment permit limitations. They are currently serving a 3-4 year active sentence. He indicated that the two principals of the site, Eidson and Hartsell, have appealed their conviction and the Department of Justice (DOJ) is fighting the appeal. Mr. Griffin stated that the DOJ has possession of CMUD's available historic files on the subject site. He indicated that their records include analytical results documenting releases from Cherokee to the CMUD sanitary sewer lines in excess of Cherokee's pre-treatment permit limitations. The releases to the sewer are believed to have originated from two sources: (a) still photos provided by a former employee of Cherokee showing a tanker truck being emptied through a 2 inch hose into a toilet at Berryhill Road and (b) a process tank located inside the main building at 1201 Berryhill Road which had a drain connected to the CMUD sewer. Mr. Griffin provided a copy of the CMUD sewer line map and marked the location of the tap line connections for the Melton's Tire Service, Cherokee Oil Company and GE Charlotte sites (attachment !). Mr. Griffin indicated that CMUD had received complaints from Suburban Propane that strong chemical odors caused Suburban Propane to evacuate the office building southeast of the site at least one time. The odors were believed to I I , I I I I I I I I I I , I originate from the sanitary sewer. Mr. Griffin believes that Cherokee Resources was the source of the chemicals disposed to the sanitary sewer. Doug Rumford and Doug Moore also reviewed CMUD's water line map and double- checked the windshield survey information provided by consultants for the GE-Charlotte site (attachment 2). No additional properties were identified on the CMUD maps that do not have a tap connection to the CMUD water lines within a 0.5 mile radius of the site. At 1200, we arrived at the Berryhill Road site. The site is located at 1201 Berryhill Road in a developed, urban, light industrial and residential area southeast of an intersection formed by Berryhill Road, Thrift Road and Tuckaseegee Road. EPA is currently using a vacant lot located southwest of the same intersection formed by Berryhill, Thrift and Tuckaseegee Roads, which is across Berryhill Road from the original site. EPA fenced and secured the lot with a chain link fence topped with concertina wire. There is a large gate located at the southeast corner of the fence. A small gate is located at the southwest corner of the fence. Upon our arrival, a rank chemical odor was noticed in the ambient air along Drum Street south of the drum staging area. The staging area contained a large quantity of drums, some in overpacks. There were two trailers located inside the fenced area; one for EPA and the other for the removal crew. We met with Federal On-Scene Coordinator Steve Spurlin and Roy Weston Technical Assistance Team member Lynorae Benjamin. Mr. Spurlin provided the following summary on the site activities to date and a map showing the site layout (attachment 3). In late 1994, EPA commenced a removal action at 1201 Berryhill Road. Due to the lack of space at the original site, EPA negotiated an agreement with a residential landowner who owns the vacant, grass-covered lot across Berryhill Road from the site. The lot is currently used to stage and open drums from the original site. EPA has contracted with a Roy Weston, Inc. Technical Assistance Team to oversee and document the site activities during the removal. EPA has contracted O.H.Materials Corporation to conduct the actual removal at the site. An earthen berm was constructed along three sides of the staging area. The berm is not present near the southeastern corner of the staging area, to allow access to roll-offs or drums by transport trucks and other equipment. The drums are placed two to a pallet and transported to the roll-off area. A concrete platform and containment enclosure were later constructed adjacent to the roll-off loading area due to spillages while transferring materials from the drums to the roll-offs. One crew member adjacent to the roll-off opens the drums. During the removal action, a drum-grappling device attached to a backhoe was observed emptying semi-solid, black materials from drums into a large roll-off container at the staging area. The emptied drums were piled next to the backhoe. Both the person opening the drums and the operator were observed in Level B dressout with supplied air. No liners were evident under the drums contained within the staging area. The following wastes were identified at 1201 Berryhill Road since commencement of the removal action: 2,856 drums located both inside the warehouse and on the parking lot 2 I I ,., I I I I I I It I I I I I I I , I between the warehouse and Berryhill Road, 2 tanker trailers filled with waste, 6 elevated black 25,000-30,000 gallon cylindrical horizontal tanks containing waste, 6 above-ground silver 10,000 gallon cylindrical horizontal tanks containing waste, 9 underground 10,000 gallon storage tanks located at the fuel station containing waste, 4 process tanks located inside the warehouse containing waste, two large steel rectangular open-top vats resting on a concrete platform which were used for handling waste and which are known to be nearly full with liquids and sludges containing polychlorinated biphenyls (attachment #4). Several plastic bags containing asbestos were also found at the site. In addition, there were 3 large concrete block containment basins constructed along the east boundary of the site; one under the main warehouse (see map#!, Area #3) which contained rainwater and waste oil, a second under the 6 black elevated tanks (see map #1, Area #2) which contained waste oil and rainwater and a third containment basin located on the south end of the platform (see Map #1, Area #1) which also contained waste oil and rainwater (attachment #5). EPA recontainerized leaking drums, completed hazardous. categorization testing of the drums, has identified I 8 separate hazardous and non-hazardous wastestreams for off-site disposal, segregated based upon compatibility and is in the process of bulking compatible waste types and shipping off-site to RCRA facilities. A sheet identifying the bulk groups identified for the site was provided by Lynorae Benjamin (attachment #6). Approximately 70,552.5 gallons of oil contaminated rainwater were pumped from the containment basins and removed for off-site disposal (attachment #5). The basin marked as area# I is currently being used as an mixing area where semi-solid sludges from drums and tanks are stabilized with kiln dust prior to off-site disposal. There are no indications that the basins had a liner or concrete floor. A site summary identifying the extent of the removal action was provided by Lynorae Benjamin (attachment #4). At 1310, we toured the site with Mr. Spurlin. There is a chain link fence with a gate on Berryhill Road in front of the site. EPA has posted the fence with no trespassing signs. The fence has a large gap at the southwest corner of the site. This gap is located at a railroad cut south of the site boundary. EPA plans to use this area to remove material from the site. Mr. Spurlin indicated that EPA has received permission from Suburban Propane, owners of the property to use this area and EPA plans to put a gate across this gap. The remainder of the site is secured by a chain link fence topped with concertina wire. The front of the site along Berryhill Road slopes to the southeast towards the warehouse. All of the drums once stored in front of the warehouse have been removed from the site. There are stained soils visible on the surface of the asphalt parking lot where the drums once stood. The warehouse is an older aluminum roof and sided structure with a loading dock on its west side facing Berryhill Road. There was a door on this side which was open and drums were visible inside the warehouse. There are 2 large capacity rectangular steel vats located on a concrete platform at the south end of the warehouse. These vats were identified by Mr. Spurlin as the ones 3 I I , I I I I I I ~ I I I I I I I , I containing the PCB liquids. Mr. Spurlin stated that the vats are open on top. The vats are covered by an aluminum roof. According to Ms. Benjamin, the dimensions of each individual vat is 15 feet Jong, 10 feet wide and 7.5 feet tall, or 1,125 cubic feet, or 41.7 cubic yards. A total once-filled volume for the two vats would be 83.4 cubic yards. Mr. Spurlin pointed out that materials contained within the vats leaked at the distribution fittings. He stated that EPA plans to remove the vats from the site. We proceeded to the east side of the platform. A total of 6 elevated, black, horizontal, cylindrical, bulk storage tanks are located approximately 10 feet off the ground. According to OHM Materials foreman John Bleshoy, each of the 6 tanks contains between 25,000 to 30,000 gallons of material. The tanks have distribution lines running along the platform to load and unload the tanks. One tank located near the center is compartmentalized into 6 sections. Each tank could hold a maximum waste quantity volume of roughly 150 cubic yards, or a total of 900 cubic yards for all 6. There is no roof over the tanks or their associated containment basin (area #2). Based upon stained soil, oily sludge and oil contaminated rainwater found under the tanks within containment area #2, it is believed that the tanks leaked material. The dimensions of the basin are marked on attachment #5. The containment walls are constructed of concrete cinderblocks and mortar. The walls are approximately 4 feet tall with black stains extending to approximately 3 feet from the base of the containment area. According to Mr. Bleshoy, no concrete floor was found while removing the sludge and liquid from containment area #2 that would prevent surface infiltration of materials. There were no visible liners or run-off prevention systems in place in this area. Based on the dimensions (attachment #5), the source could be considered an impoundment and a once-filled volume would be approximately 457.4 cubic yards. Mr. Spurlin indicated that at the time of the removal action, a gap was missing in the containment wall between containment area #2 and area #3, which allowed material to flow between the two areas. He also indicated that material in the containment area appears to have flowed underneath the platform and warehouse. Mr. Spurlin indicated that after removal of the 6 elevated tanks, EPA plans to remove the remaining containment basin structure and scrape the stained soil from Area #2. As we walked along the south end of the site, Mr. Spurlin pointed to two concrete pyramid-shaped structures near the southwest corner of the site along Berryhill Road. Fill pipes are visible at this location which are believed to be connected to 9 underground storage tanks. He stated that the tanks were filled with hazardous wastes including waste oil and solvents. EPA has pumped the tanks and shipped the contents off-site to RCRA facilities. Mr. Spurlin indicated that EPA plans to remove and dispose of the UST's from the fuel station area. According to Ms. Benjamin, each tank is estimated to hold approximately 10,000 gallons, or 50 cubic yards, giving a total of 450 cubic yards for all 9. We proceeded to the railroad cut south of the fuel station. From the cut, it appears that the tanks are located underneath a concrete slab which appears to rest on top of concrete blocks and fill dirt. EPA has bush-hogged and pushed soil in the railroad cut. From the 4 I I , I I I I I I Ii I I I I I I I , I cut, a black material was observed to have seeped from the contact point between the slab and fill dirt. Mr. Spurlin pointed out a concrete block containment area south of the platform which corresponds to area #l of attachment #5. Mr. Spurlin stated that the basin contained free- standing oil contaminated rainwater which EPA pumped out and removed off-site to RCRA disposal facilities. A front end loader was observed at this location. The removal crew was transporting a black material from inside the warehouse using a Bobcat loader and dumping the material off the south end of the platform into the basin at area #1. A large front-end loader was observed to be mixing the sludge-like material with a white powdery solid. Mr. Spurlin indicated that EPA was using this area to solidify and stabilize sludges from one of the tanks using cement kiln dust prior to off-site disposal. At 1400, we proceeded to identify and photograph the storm grates that received runoff from the site. The first storm grate is located on the east side of Berryhill Road at the southwest corner of the site near the railroad cut. A storm drainage map provided by Mecklenburg County Dept. of Environmental Protection (MCDEP) (see map #2) indicates that the runoff from Berryhill Road intercepted by this storm drain travels east under the railroad tracks towards Suburban Propane's main office building on Thrift Road. From a 1991 MCDEP video, another storm grate was visible at the fork in the railroad track. We proceeded to the southeast corner of the site, but were prevented from reaching the grate by a chain link fence across the railroad cut. A black material and stained soil were observed at the southeast corner of the concrete block containment wall of Area #1. The material entered a drainage ditch adjacent to the railroad track. The material was a semi-solid and the drainage ditch did not appear to be flowing. The drainage ditch carries runoff from this location east along the tracks to the storm grate in question. We traveled north on Berryhill Road and circled around the site to a parking lot adjacent to Suburban Propane's main office building on Thrift Road, southeast of the site. Mr. Spurlin indicated that this was an area that received runoff from the site. The asphalt parking lot is stained, providing evidence of a runoff pattern from the site southeast across the parking lot to a storm grate located near a loading dock. This is noted as grate #I on MCDEP storm drainage map (attachment #7). The concrete block containment wall for Area #3 is the point of origination of the runoff at this location. The distance from the wall to the grate is estimated to be 100-150 feet. Access to the site is prevented by a chain link fence located between Suburban's parking lot and area #3. Mr. Spurlin pointed to the remaining black stained soils inside Area #3. EPA has attempted to remove contaminated soils from under the warehouse at area #3. We proceeded south on Thrift Road to a truck maintenance shop at the southeast end of Suburban Propane's office building. Mr. Spurlin spoke with one of the people at the shop, who granted access to the rear of the building to locate the remaining storm grates. We walked northwest along the railroad tracks to a fork. The ditch leading from the site 5 I I , I I I I I I It I I I I I I I , I was visible and a storm grate was also observed at the fork in a heavily vegetated area. This is noted as grate #3 on MCDEP storm drainage map (attachment #7). The distance from the southeast corner of the site to the grate is estimated to be 100-150 feet. An additional storm grate was observed on the Suburban Propane property south of the site. It is unlikely that this grate received any runoff from the site, as it is located on the opposite side of the drainage ditch from the site and there is a earthen berm between the grate and the site which would direct runoff from the site away from the grate. This is noted as grate #4 on MCDEP storm drainage map (attachment #7). According to the 1991 MCDEP video, an additional storm grate was located along the southwest wall of Suburban Propane's office building that received runoff from the site. This is noted as grate #2 on the MCDEP storm drainage map (attachment #7). Runoff· from containment areas #1 and #2 would travel overland southwest between the northwest wall of Suburban Propane's office building and Cherokee and then southeast along the southwest wall of Suburban Propane's office building. The overland distance from the site to the grate is approximately 200-250 feet. At 1425, we arrived back at the EPA command trailer. Lynorae Benjamin provided a summary of the removal action to date (attachment), a copy of analytical results and a map showing the sample locations for several soil samples collected at the site, a map showing the current site layout and identifying source areas, a copy of the current bulk group wastestreams identified by EPA for off-site disposal and a map showing dimensions of the three containment areas. At 1430, Doug Moore and Doug Rumford departed the site and took a 0.5 hour break for lunch. At 1515, we arrived at the Harold Marshall building, 700 N. Tryon Street, Charlotte to review the available file information in the MCDEP files. Doug Moore conducted the file review and Doug Rumford drove to the County Government Center at 720 N. Fourth Street to review the tax assessors office and register of deeds information on prior site ownership. At 1520, Doug Moore met with John Gibson, Hazardous Waste Section and Tony Roux, Water Quality Section to discuss the site history. Mr. Gibson indicated that the site was built in the late 20's or early 30's by "City Service" company. According to Mr. Gibson, City Service used the site initially as a fuel distribution facility, but, could not maintain enough business and switched to solvent distribution. He indicated that solvents such as alcohols and chlorinated solvents were probably stored at the site. Mr. Gibson believed the site was operated by City Service until the late 1970's or early 1980's, when it was sold to Gene Hartsell. Hartsell operated the site as Spurrier Oil. He later became involved with Keith Eidson, who had recently arrived from Florida. The company later changed it's name to Cherokee Resources. 6 I I , I I I I I I It I I I I I I I , I Cherokee used the tanks located inside the building as oil/water separator units. He stated that Cherokee had filtration units inside the building, but that they did not use them. The waste oil was separated from the water in the tanks and the oil was pumped to large elevate bulk storage tanks located outside the building. Oil stored in the elevated tanks was shipped off site and sold to metal treaters who used the oil to "cure" the metal during extruding and tempering. One of the separator tanks located inside the building was connected to the city sewer system. Mr. Gibson indicated that MCDEP has received numerous complaints from area residents and businesses of illegal discharges and spills from the site affecting neighboring properties. He believed that MCDEP has documented roughly 11 separate spill events from the site. Mr. Roux indicated that the MCDEP -Water Quality has issued Notices of Violation (NOV) letters for several of the spills. Around 1992, a judgment was issued against Cherokee for an illegal discharge to the unnamed tributary of Stewarts Creek. An administrative order including a penalty was levied against the company. Mr. Gibson was not certain whether Cherokee had paid the fine. He believes that Cherokee did pay one fine of $5,000 for a spill that reached the unnamed tributary of Stewarts Creek. On December 21, 1990, MCDEP -Water Quality personnel conducted a dye trace of the storm grate system that receives runoff from the site beginning at Suburban Propane's parking lot (Grate #1 of MCDEP storm drainage map) downgradient to the UT of Stewarts Creek. Rusty Rozell and Walter Booker injected a yellow-green dye at grate #I and followed the dye trace along the line indicated on MCDEP storm drainage map to the UT of Stewarts Creek. Pictures taken at this time are located in MCDEP's files and provide strong proof of a storm drainage route from the site to the UT. A copy of the storm drainage map from the site to the UT, analytical results of samples collected at the site and several key pages of an attorney enforcement briefing were copied by Tony Roux. At 1700, Doug Moore departed the Harold Marshall building and waited for Doug Rumford to return. Mr. Rumford returned at 1750, having traced the site history .back to 1961. A discussion of the site ownership history will be provided in a separate memo. At 1750, we depart Charlotte for Raleigh and arrived at Raleigh at 2030. Attachments: 1. Photocopy of CMUD sewer line map showing municipal taps from Meltons Tire Service, Cherokee Resources and GE-Charlotte facilities. 2. Field Survey Findings for Properties without a Water Meter on City Water Maps. Private Water Well Survey, within 0.5 miles of Site. Remedial Investigation. General Electric Appartus Service Shop. Charlotte, North Carolina. Law Environmental Project No. 55-629260. 7 I I , I I I I I I It I I I I I I I , I 3. 4. 5. 6. 7. 8. Site Layout Map of the Cherokee Oil Company/Berryhill Road site. Terry Ryland/Lynorae Benjamin, TAT Region IV. Site Summary for Cherokee Oil Memorandum To: Steve Spurlin, Region IV EPA. Subject: Cherokee Oil Site, Charlotte, North Carolina. TDD# 04-94I0-0065. June I, 1995. Map showing dimensions of Containment Areas #1, #2 and #3. Map provided to Douglas Moore, NC Superfund Section, by Lynorae Benjamin, TAT Region IV, during August 1995 on-site reconnaissance. Groups identified for disposal at the Cherokee Oil Company site, 120 I Berryhill Road, Charlotte, N.C. Copy provided to Douglas Moore, NC Superfund Section, by Lynorae Benjamin, TAT Region IV, during August 1995 on-site reconnaissance. Mecklenburg County Department of Environmental Protection files. Cherokee Oil Company Site. 120 I Berryhill Road, Charlotte, North Carolina. Douglas Moore, NC Superfund Section Field Notes. Cherokee Oil Company Preliminary Assessment On-Site Reconnaissance. Wednesday, August 9, 1995. 8 I 67 691.e -591 7 X r---· . PARKING r '\ 590 :· I -I 5 1 ~::'.'.,, p -' ,--~~ { ,--- • I I L II FIELD SURVEY FINDINGS FOR PROPERTIES SHOWN WITHOUT A WATER METER ON CI1Y WATER MAPS PRIVATE WATER WELL SURVEY, WITHIN 0.5 MILES OF SITE REMEDIAL INVESTIGATION GENERAL ELECTRIC APPARATUS SERVICE SHOP Charlotte, North Carolina Law Environmental Project No. 55-629260 City Water Map W-17 1. Property between 3011 and 3021 Tuckaseegee Rd. (south side) -Property appears to be a part of lot 3011. No water meter or well visible. 2. Property at NE corner of'intersection of Parkway Ave. and Tuckaseegee Rd. - Property is occupied by Temple Baptist Church Property appears to be connected to 2910 Parkway Ave. Meter vault 1505 is located on Tuckaseegee Rd. in front of the church No water well visible. 3. Property between 2915 and 2923 Carol Ave. (west side) -Weeded, fenced lot. No water meter or well visible. 4. Property between 2821 and 2827 Morson St. (west side) -Properties at 2821 and 2827 are adjacent. 2825 and 2827 are a duplex on the same lot. No water well visible. 5. Property at 2637 Clydesdale Terrace -Part of lot 2643 Clydesdale Terrace. No water meter of well visible. 6. 7. Property between 2712 and 2720 Carol Ave. (east side) -Lot 2712 is adjacent to lot 2720. The property in question is actually a vacant lot south of 2712 carol Ave. The lot is fenced with an deteriorating garage. No water meter or well visible. Property between 1336 Parkway Ave, and 1510 Effingham Rd. -Property is 1500 Effingham Rd. Water meter is present. No water well visible. 8. Property between 911 and 917 State St. (south side) -Vacant lot. No water meter or well visible. 9. Property between 919 and 921 Ambassador St., (southeast side) -One lot is next to a lot with a three unit apartment building (913, 915, and 919). 921 Ambassador St. a 4 unit apartment building with 4 water meters. Between 921 Ambassador St and 1007 Ambassador St. is a large wooded lot with on visible water meters or water wells. 10. Property between 1007 and 1019 Ambassador St. (southeast side) -Property is a part of the lot at 1019 Ambassador St. No Water well visible. I I: , I I I ;I ·It I I I I ' I ' I ' ' , I 11. 12. 13. 14. 15. Property between 1732 and 1746 Camp Greene St. (next to Handy Pantry) -Property is a heavily wooded lot. No water meter or well visible. Property at 2521 Elon St. (west side) -Lot is part of adjacent lots. No water meter or well visible. Property at intersection of Tuckaseegee Rd., Berryhill Rd., and Drum St., bordering 2401 Tuckaseegee Rd. (west side) -Vacant lot. No water meter or well visible. Property at large lot on Freedom Dr. -Lot is occupied by Service Distributors Gas Station and Car Wash. The lot on the map that is labeled Service Distributors is actually CTR of Charlotte. The water meter vault number is 86 and is located on Berryhill Dr. No water well is visible. Property at large lot on Berryhill Dr. just south of the Texaco Station at 2337 Berryhill Rd. -This lot is part of Suburban Propane. A water meter is located on Berryhill Dr. No water well is visible. City Water Map E-17 1. Property between 317 and 715 Ambassador Ave. (east side) -Property consists of three lots. The lots are cleared but overgrown with weeds. No water meter or well visible. 2. Property between 715 and 811 Ambassador Ave. (east side) -Property consists of two lots. Both lots are wooded. No water meter or well visible. 3. 4. 5. Property at southeast comer of intersection of Tuckaseegee Rd. and Litaker Ave. - Litaker Ave does not exist between Tuckaseegee Rd. and Walnut Ave. The lot east of the railroad tracks on the south side of Tuckaseegee Rd. is wooded and there is not a water meter or well visible. Property at intersection of Heathcliff St. and Lela Ave. (southeast side) -Lot is wooded. No water meter or well visible. Property at intersection of Lela Ave. and Woodruff Ave, north of 604 Woodruff Ave. -Lot is wooded. No water meter or well visible. City Water Map W-16 1. Property just north of 1827 Garibaldi Ave. (east side) -Water meter vault is present at this lot. No water well is visible. ;I I , IJ I I ' I I ' ~ I , I I , I • I ' ~ ' 2. Property between 1506 and 1516 Noel Pl. (northeast side) -Lot is wooded with steep te"ain. No water meter or well visible. 3. Property bordering 1404 and 1424 Berryhill Rd. -Three lots are present. One lot has a large creek running through it, wooded on the east end and has a gravel parking area on the west end. One lot is connected to an adjacent lot occupied by Price Heating and Air Conditioning. The other lot is wooded. No water meters or wells are visible on the three lots. City Water Map E-16 1. Property just south of 733 Woodruff Pl. (east side) -Lot is wooded with no water meter or well visible. I I I I I I I It I I I I I I I ' I / #------"NCC ""1-------=----=a..=-~ =~~--- / / OFFICES DRUM STORAGE / / & EQUIPMENT I / f----' .............. J ... . 1111111 VATS DsHED • DIKED AREAS ~ I ROLLOFF ---------·----- TANKER TANKER TANKS 7-12 ' FUEL STATION t --·----------------------------J :RBGIOINIV'mOINICALASmSTANCBTBAM CHEROKEE OIL/BERRYHILL ROAD SITE CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA TDD# 04-9410-0072 I I , I I I I I I I I I I I I , I TO: FROM: SUBJECT: DATE: BACKGROUND ~ITE SUMMARY FOR CHEROKEE OIL Steve Souriin Reqion IVP EPA Terrv Rvland/Lvnorae Benjamin TAT, Region IV Cherokee Oil Site Charlotte, North Carolina TDD# 04-9410-0065 June 1. 199'..\ Cherokee Oil is Located at 1201 Berrvhill Road. The site is near the intersection of Berrvhill Road and Drum Street, aporoximatelv one mile north of downtown charlotte. The area consists of a large residential oooulation along with numerous warehouses and busine-:?sses. Cherokee Oil was an oil recycling operation that ille □allv accepted hazardous waste. The former operator of the facilit~ and current owner of the propertv have both been sentenced to 51 months in prison for the illegal discharge of hazardous materials to the citv sewer system. The site consisted of unknown waste in drums, ABTS, LISTS, two tanker trailers and other miscellaneous container-s. EPA assisted by TAT conducted a site investigation in August 1994 and verified the □resence of large quantities of hazardous substances on the site, which oosed a threat to nearbv residents. SUMMAF,Y When EPA first entered the Cherokee Oil facilitv, they found 2851 drums, twelve large above ground storage tanks, two tanker trailers, nine underground storage tanks, containment areas, and other miscellaneous containers all containing unknown waste liquids and sludges totalling in excess of 300,000 gallons. On 2 November 1995, EPA, OHM Corporation and TAT mobilized to the Cherokee Oil Site to begin removal action. To date, the following actions have been taken: l;:lci.:S"'i f ication of l>Jacste 1. All 2856 drums were staged and hazcated. Trak Program. OHM testing on the first transferred across the street, Data was entered into EPA's Drum Corporation has performed bulk 1400 drums and will perform bulk I I , I I I I I I I I I I I I , I testing on the remaining drums in the near futL1re. So far, there are nine bulk groups. Samoles of these nine bulk groups were composited by the chemists and sent to a local laboratory for analysis. Results should be in bv the beginning of next week. A disposal plan of the drums will be developed upon receipt of the analytical data. Samples of the sludges from the above tanks and the underground storage tanks local laboratory for analysis. At the OHM Corporation is developing a disposal sludges. ground storage were sent to a present time, plan for these Removal of Waste 1 . 2. Approximately 680 cubic vards of solidified sludge were sent off site to a facilitv in Columbia, South Carolina. Approximately 99,000 gallons of Non-Dot or RCRA regulated water contaminated with oil were sent to a facilitv in Charlotte, North Carolina. 0. Five rolloffs containing debris and PPE were sent to a facility in Columbia, South Carolina. 4. 5. Approximatelv 45,000 gallons of the hazardous flammable liquid waste stream from the aboveground storage tanks were sent off site to facilities in Baltimore and Ohio. Approximately 65,000 gallons of the hazardous flammable liquid waste stream from the underground storage tanks were sent off site to a facility in Reidsville, North Carolina. I I , I I I I I I ' I I I I I I I , I ~ITE SUMMARY FOR CHEROKEE OIL F·rofile of s.ite 2856 drums of unknown waste 6 silver aboveground storage tanks 6 black aboveground stor·age tanks 2 square vats 2 tankers 9 unde1rground storage tanks 4 tanks inside the warehouse F~ernovc,l Df Waste to d€! . .tE'. 1. Aoproximatelv 680 cubic vards of solidified sludge were sent off site to a landfill facility in Columbia, South Carolina. 4. 5. 6. 7. Aoproximatelv 99,000 gallons of Non-Dot or RCRA regulated water contaminated with oil were sent to a facilitv in Charlotte, North Carolina. Thirteen rolloffs containing debris/drums and PPE were sent to a facility in Columbia, South Carolina. Approximately 45,000 gallons of the hazardous organic neutral liquid waste stream from the onsite tanks were sent off site to facilities in Baltimore and Ohio. Aoproximatelv 65,000 gallons of the hazardous flammable liquid waste stream from the onsite tanks were sent off site to a facilitv in Reidsville, North Carolina. In excess of 792 tons onsite tanks was sent hazardous waste. of solidified sludge from the to Michigan Disposal as a In excess of 162 drum waste was hazardous waste. tons of solidified sludge from the sent to Chambers landfill as a non- I I 6' I - -------1)1"-e W,41.-cS J._ 1 'i,_"'c/ ~P/Tf/1 ,, fJre&. 2, .Siu clje /Jeft/, I , I ~I I - ----- I I I I I I I I I I I I I I I , I Jl,eA z /y ree. 3 Tu-r,qL- 30 gs:, Sf If- Y: /.3 av_,. tiepl{ l/tJtl/, '-/ eu. If ;i 1,5' 31 1 oto 5a I. / 800 ~ -f-1-( ~5+-) '/. I, (p a.v5. de.p-/-1, ;;-go ~-/I X 7,5' ;{!, tp&O gd 10, §~'2.. 5 5al. 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J r"--(_-1-~ fl re ~t" f·ct •· '"i)---·-;·-· ---------------------·- r-1, J\.<.e -14-.,-,.._-· ~e-v-. _1.-t~~ __c-i.,_"-~ __ lit?! _ -~ ~lkM_1 _p@'~--"'f! ___ _ fru~~ Ct..-,~~~ _ 0-,d:--0-. , ! , ·/( ,. --;/___ ' f• --··----------·-·-------·----, ' I ------/--, ' ---· -------,--·---------- ·,.,:.,i;;:,,i.NB~"t'. .. ~C.a;~.,1 ~ ¢:t.'I~· -• I -, / I i I I I I I I / I I I ,' / / /1 I / / L_: --.-------------: ____ _ ,,,. ~i ~- ·•1 / I ,, ./ // / / -· i ____ J ' ! I ,i , ,, •. ,,, . . ..Jf;t, I I I I I I I ' I I I I I I I r I SUMMARY This report documents violations of North Carolina General Statutes 143-215. 83, 143-215. 84 and 143-215. 85 by Cherokee Resources, Incorporated, for unauthorized discharges of oil onto the ground and into surface waters of the State, failure to restore those areas affected by the oil discharge and failure to immediately notify the Department. Cherokee Resources is an environmental cleanup company specializing in the recycling of industrial waste oils and waste waters, the removal of underground storage tanks, the cleanup of industrial waste on site, and the packaging of non-hazardous wastes for transportation to disposal facilities. On January 24, 1990, the Mecklenburg County Department of Environmental Protection (MCDEP) received a complaint from a citizen concerning an accumulation of barrels on property owned and occupied by Cherokee Resources, Incorporated, located at 1201 Berryhill Road in Charlotte (see Appendix B). In response to this citizen complaint, John Gibson, Program Manager of Solid and Hazardous Waste, and Debra Howell, Environmental Hygienist, both with MCDEP conducted an investigation at Cherokee Resources on January 29, 1990. The investigation revealed over a thousand 55 gallon drums at the facility which reportedly contained waste oil, bulk oil, residue from underground storage tank clean-ups and residue from chemical treatment facilities. They also observed areas on the property where soil had been contaminated from oil spillage. Runoff of emulsified oil into the storm sewer system was also obs~rved in a ditch along the railroad tracks adjacent to Cherokee Resources property (Area 1 on Appendix B) Straw bales soaked with oil were also observed in this ditch possibly remaining from a spill of 5000 gallons of waste oil which occurred on the property on December 28, 1989. Mr. Keith Eidson, president of Cherokee Resources, was contacted by John Gibson during this investigation and Hr. Eidson was advised that the drums of waste needed to be removed from the property along with all contaminated soil. John Gibson discussed with Mr. Eidson methods for improving the handling of oil on the property to prevent future spillage. Mr. Eidson indicated that by January 31, 1990 all drums would be removed from the property. He also indicated that he would address the problems with oil leakage. John Gibson also directed Mr. Eidson to remove oil contaminated soil and oil soaked straw bales from the ditch along the railroad track and to eliminate the discharge of emulsified oil. On February 1, 1990, John Gibson and Debra Howell inspected Cherokee Resources to determine if efforts were underway toward correcting the problems at the facility. This investigation revealed recent oil spillage into the ditch along railroad tracks behind Cherokee Resources (Area 2 on Appendix B). Mr. Eidson was informed of this spillage and he advised that a major cleanup of the property would be completed within 60 days. The spilled oil and oil soaked straw bales observed along the railroad tracks on January 29 (Area 1 on Appendix B) had been removed; however, soil contaminated with oil still remained in the ditch. ~, On February~ 1990, a notice of violation was issued to Cherokee Resources by the Mooresville Regional Office (MRO) in response to conditions observed by MCDEP at 1201 Berryhill Road. This notice requested that a written response be submitted by March 2, 1990 explaining the measures to be taken to prevent future discharges and restore all affected areas. MRO received a letter from Mr. Eidson dated March 19, 1990 which explained that oil had been discharged from Cherokee Resources' property to a storm drainage ditch and that no "significant traces" entered surface waters ( see Appendix C) . Mr. Eidson further explained that soil contaminated by the discharge had been removed from the property and hauled to GSX in Pinewood, S.C. He also stated in this letter that various modifications were being made to their facility to improve their capabilities for handling waste oil and prevent future spillage. Page 2 I I I I I I I , I I I I I I I , i ' I I I I I I I I It I I I I I I I r I On March 19, 1990, Debra Howell conducted an inspection at Cherokee Resources which revealed oily residue in the ditch where previous spills had occurred (Area 2 on Appendix B). Evidence indicated that the spills had not been adequately cleaned up. On April 3, 1990, John Gibson and Rusty Rozzelle, Program Manager of Water Quality for MCDEP, conducted an inspection at Cherokee Resources to assess progress toward cleanup of the facility. This investigation revealed two unauthorized discharges of oil from Cherokee Resources (Areas 1&2 on Appendix B) which flowed to ditches along railroad tracks adjacent to and behind the facility. It also entered the storm drain system which discharges to a tributary of Stewart Creek. Water sampl collected from the storm drain and Stewart Creek revealed th presence of oil (see Appendix D). Oil soaked absorbant materi 1 was observed along Berryhill Road in front of Cherokee Resources-..... _ __.- (Area 3 on Appendix B) which was reportedly left over from the cleanup of a previous spi 11. Mr. Eidson reported that the discharges from Areas 1 and 2 originated from a surge tank and from an oil sump both of which are located on Cherokee Resources' property. Mr. Eidson stated that he did not notify MRO or MCDEP_ of either of these discharges. John Gibson informed Mr. Eidson that both discharges must be stopped immediately and all affected areas restored to their original existing conditions. _, .------·-::":':· ···--.... by Follow-up investigations conducted on April 6 and ~_::_}J) representatives of MCDEP revealed that oil was still present in the ditch along the railroad tracks (Area 1 on Appendix B). Evidence indicated that oil was still discharging (seeping) to this ditch. Contaminated soil was still present along the railroad tracks at both Areas 1 & 2 and also on Cherokee Resources' property. Some drums, discharged oil and contaminated soil had been removed from the property, but a significant amount of clean up remained to Resources dated April 10, be done. A letter from . Cherokee 1990 stated that ''major construction projects'' should be completed by April 30, 1990, but no mention Page 3 was made concerning cleanup of contaminated soil and elimination of discharges (see Appendix C). Page 4 I I, I I I ti I I I I I I I , I I I I I I I I ' I I I I I I I r I h. removal of contaminated soil, proper disposal of soil, and implementation of necessary controls to prevent future discharges. The alleged violator's previous record in complying or not complying with the laws and implementing regulations of the Commission. February 7, 1985 -Soil contaminated by oil spillage was detected on property belonging to Cherokee Resources. Resources. Clean-up was accomplished by Cherokee June 26, 1986 -Approximately 30 gallons of reprocessed oil was spilled on Cherokee Resources property. Cleanup was accomplished by Cherokee Resources. July 25,198 6 -Cherokee Oil Company was assessed $3842 .17 for violations of North Carolina General Statute 143-215.83, .84 and .85. The Company paid $1342.17 on September 8, 1988 to close the case. Julv 27, 1986 -An undetermined amount of oil was spilled at Cherokee Resources reportedly due to vandalism. The oil entered the storm drain system and discharged to a tributary of Stewart Creek. Clean up was accomplished by Cherokee Resources. October 2, 1986 - A truck belonging to Cherokee Resources leaked oil on the road which splashed onto a passing car. Clean up was accomplished by Cherokee Resources. December 18, 1986 -An undetermined amount of oil was spilled at Cherokee Resources which discharged into the storm drain system. Oil was not observed in the creek. A complaint was received from a representative of Page 11 Suburban Propane. Cherokee Resources. Clean up was accomplished by January 15, 1988 - A complaint was received from Suburban Propane concerning oil in the storm sewer running through their property from Cherokee Resources. Investigation revealed no oil runoff from property. Cold weather had ruptured a pipe but all oil was collected in a retainment area. accomplished by Cherokee Resources. Cleanup was December 13, 1988 - A complaint was received from Suburban Propane concerning oil in the storm sewer running through their property from Cherokee Resources. Investigation revealed no oil runoff from the property. ~M~a~v--~3~,'-~1~9~8:..::.9 - A complaint was received from Suburban Propane concerning oil in the storm sewer running through their property from Cherokee Resources. Investigation revealed no oil runoff from the property. Februarv 20, 1989 - A complaint was received from Suburban Propane concerning oil in the storm sewer running through their property from Cherokee Resources. Investigation revealed no oil runoff from the property. December 28, 1989 -Approximately 5,000 gallons of waste oil was released from a tank at Cherokee Resources reportedly due to vandalism. Approximately 72 gallons reportedly entered the creek. The remainder of the oil was contained on the property. Cleanup was accomplished by Cherokee Resources. Februarv 1, 1990 - A complaint was received that Cherokee Resources was discharging oil and chemicals into the sanitary sewer system. This was referred to Page 12 I I I I I I I , I I I I I I I , I I I I I I I I I I I I I I I r I 12. i. the Charlotte Mecklenburg Utility Department, Industrial Waste Division. Februarv 7, 1990 -Approximately 55 gallons of motor oil was spilled from a drum over-turned due to human error. Clean up was accomplished by Cherokee Resources. March 22, 1990 -Approximately 138 gallons of waste oil was discharged at 1506 West Boulevard in Charlotte from a truck belonging to Cherokee Resources. The spill reportedly was caused by vandalism. The oil entered a storm drain where it was contained. Clean up was accomplished by Cherokee Resources. The amount of money expended by the alleged violator in complying with the provisions of G.S. 143-215.84. Unknown. MCDEP has not been provided cost figures for the amount of money spent to date for clean up of the property. j. The estimated damages attributed to the alleged violator under G.S. 143-215.90, including cost to restock such waters or replenish such resources, etc. No fish, animals or vegetation were reported killed by the discharges. Costs of the investigations, itemized Necklenburg County Department of Environmental Protection Manhours = $240 (12 hours at $20/hour) Vehicle Mileage= $200 (100 miles at $.20/mile) Laboratory Analyses= $100 (2 oil & grease analyses) Sub-Total Page 13 = = = $240.00 200.00 100.00 $540.00 I I I I I I I .• , • ~. ~·-o , • •• h) 11:cnCIIIUIIG COIJITT O(PAIMIIT 0, UYIIIClftNT.11. HEAi.Tl! VIY I IOIIOT .II. UIOIIA TORT Fl1ld 1.0. , _________________ _ SI ti S...,l1d , • I ~ 'ff¼ 7CL ~dress 0t.ecl;.,.,,, Q::, -'( rc<et I Dr1c1i:;i, -56, r o.,.,, I L•b 1.0., t-7{)9 Roc'd By r£;;) / Sourct ~-ltd 6!,_,_,.,_, {,1,d /4..fk. /f.2.i J S.ms,ltd Sy -:i--:r_·T .:';q: -~--r Cati ~led uf-,, i:.. Tl•,.·-"(,-~ I !!!!1[._ CAI. "-IIOP ERT! ES 0t I hertd to L•o On: OI t. Roe' d 1/ /3 /qQ , ~ Olt. ,d,1'f(; TIN J.·5t M Tl• /jQ0 I ~• Z:· Oal her-.d Sy -":(.·(.,,;;-.T?Lt: [;;C 11 KON-METAL J_ltORGAIIICS JlL_OR~ I CS Color Q __________ units Acidity Q _________ o_por +-----.,.._ ___ ,:,,. C.011<1UCt1vity LJ _______ _.,,-/an Alk1llnlty Q _________ por 011 l Grene =~ -----+----JissolvH Solids Q Vo1Hilt 17 _____ _,.;,a ______ .,.po FiuoQ _____ _,.PIii SuscendH Solids LJ _______ o.pca 'loht111 D _____ _,.Pl Fhed 17 -----~om 7ot•I Solids Li ______ _;pm '/OIH11t LJ _____ ....11>11 CH Q ____________ u.nlts Or~anlc Acldi ~/ ••... Chloride Q ________ _,op,o Ph1nol /7 Chlorine, Rtsidllll Q _____ ,0111 direct pnotcmwtric _______ ::r. Oissolvtd Oiygen tJ _____ ~PIII cnlorofom utractlon ••• Fluoride 17 BOO LJ ___________ ,.cm soadns _________ __,,p,o COO LJ ___________ .:on el ectroo, _________ _.,.pm Sur'flctints // __________ ::~. Kftrlt. tJ !V MlNERAL_ HEI,\LS UV spec __________ _,.pm Cu Ii ~::rn F luo Q _____ _.,por It ,....,.,atur-t 11 _________ •c chrcmatropl'l1c ac1d ______ _,,pm Ft ti ::~ >ur~tdlty L, __________ .JT\J Armonfl Nltrogtn tJ Mn // :::-, I rl1~dn1ss Li ___________ _,.po ---LJ _________ _ t1tr1metr1c _________ yo,m nassler1nt1an. _______ -JOIII Zn I! ______________ ,=~ "9 /! ______________ ,,~ I v1 ~,,w1CA1. ai~osrr:a~ On;anlc // __________ s. {Jtldlhl Nltroqtn Q _____ ,P" Bromide Q _______ __,oon, Cl / I •er., Ht It :o~ lnon;1nlc LJ __________ s. I ~1,wra LJ_""'"" ________ s. PlloSPIIONS 17 _______ _,.Pffl K Q ___________ __,o:,, Sulfate Q HI Q ____________ .>"11 .it IADIOAC7,V!TY ;ra•l•tr1c _______ ~""' _ 11 ____________ 01_,., I ••tor turt,ldl•trlc ______ __,oo,,, v TOXIC METALS ·cross Alolll LJ _______ _,.c1/1 Sulf1dt a ________ _,.po Ag LJ ___________ _,,~e I Gross 81t1 Q _______ .r-1/1 ___ Q ________ _,.po, As a ___________ ,.oo Air VII BACT!:R!OLOGICAI.S Bl tJ ___________ _,,oo Gron Alon& Q _______ .J"i/.,J Fecal Coltforw Q _____ __,1rCal (j LJ ___________ _.,.ro Gross Itta Q _______ _;~l/-3 Total Collfo,,. Q ______ /10Qol Cr LJ ___________ _,eoo I llon•Colffo,,. LJ _______ /100111 Hg LJ ____________ ,.o, I Fec~I Strap a-'-______ 1100,,1 Pb a::::::::::::::::::::::='°· , ,; ____ a • lll(al St a C------000 stlWIKS; I ' i/ ~--_."'I •_.... L-U t,-/J.. ........ I OAT£ a:N'U7ED: ua 01R1:croa .-I . _________ _, ... --,c,;c::::rnR ·-. . ....... . --------· .... ·------------ 1 . ...,., .. 4 Field I, 0. I t • •• • 9 . '. Sltl s ..... ttd -i'1./1( 1·1~J,1 /}_-;;;i lr.'r... /.,_, --, '/'/ .lcld"ss : • ·, /:,ctrl/1'• Soun:1 S-IK ,Sn;,,,, ;t,,,, "'( ·-7).,.-;r••~c SUolecs a, 1 !,,,, , -~ t:{]/t' CU1 s.itN </ /7 /'?'C• Tl• /. _;s· -,J: LabOij~i~)j D(pAfflOT 0, OVI IIOIIOTM. HE.AL TH UVIAOIIOTM. UIOIATORY I L•• 1.0.,_£'1 JO Rec ' d 8 y , \ C < ::t:zz-fu:a:::: 1 ' .. 0.1 fvtl'td ta LO On: Dita Rec'd" lf/!j lt?o p I -;,;·-~ I,~ Dita t · ~( Time ?: 5u N Tl• l,~::".f: w• -<,---. I ' 0.11 ...... 11 .cc,, : n ,-;r I PMTSICAI. P110PUTl£S II NON•M!:TAl IIIOIIGMICS Ill ORGAHICS ...,:---..... J Colar Q __________ .unlts Acidity 0 ________ _,,111 GC/IIS Scan 17_..,._ ______ ,. CIIIICNcthlty 0 _______ .. .-/cm Altallnlty a _______ _,.111 011 & Gn,ase -;------+---'] ~hsal .. d Solids Q _____ _,pa pH Q units Organic Acids ..._-==-----''' Vol1tl11 a _____ _,pa Chloride a ________ _,.111 Phenol /7 rlud a _____ _,pa Chlorine, Rnidull a ____ _,.,111 dln,ct ohotontric _______ ,1 Susotndld Sol1ds 0 _____ __,.pa Dissolved Oxygen a _____ _,.PII chlarafarm utractlan ,,o Volatl le a _____ _,ID Fhed Q _____ __,,pm Fluoride 17 BOO a ___________ ,o, ,padm _________ .,,,,.111 coo a ___________ ,:im Total Solids a _______ _,.pa 'lohtll1 a _______ lll elKtrade ________ _,.pa Surfactants 17 "1 N1tr1ta D IV N!N[RAl METALS rlud Q _____ __,.111 iemc,eraturw a ________ 0c UV SP« _________ _,.pa C.. c ____________ ?.:M chraaotraphlc acld _____ _,.111 Ft 17 ____________ • Adonla Nitrogen O Mn O .,,.. tltrlmetrlc _______ _,p,11 Zn a ___________ _,,~ TurOldi ty a _______ _,.;JTU Hlrdn1SS a _________ ..Jpa ___ LJ_________ ,.11lerlr1tlan_, ____ .,,111 _"9 /7 ___________ _,opa, VI Cl!Elllc.11. COMPOSITION l(jeldlhl Nltroqen a ____ _.,,111 Cl U-----------1 Organic a _________ ,. Bl'l!llide a ________ .,,,pa NI 17. ____ ,o,, Inorganic Q ________ l ""°1PIIONS a _______ _,,pm, K a ____________ p~ Noistu" 0-,,---------S S..lfaU a NI a ___________ J VII RADIOACTIVITY 9"••i•tr1c _______ __,.1'1 _ a ___________ _,;DP,,,I water turt,idl•trlc ______ __,PIII V TOXIC METALS -~rass Alpllt a __ ...;.. ___ ___,,.i/1 Sulfide 0 _______ __,ppo kj a __________ __,ooo Grass htl a ______ ..J"'i/1 __ a _______ __,.PII As a ____________ oool Air YII BACTl:RIOLOGIC-'LS Bl a __________ __,.00 FKal Callfo,. a _____ _,lCO.l Cd a __________ _,.rol Totll Callforw a _____ /1001111 Cr a ____________ oco Gran Alpllt Q ______ ___,,.11,.J Gress Btu Q _______ J"'i/-3 llan-Collforw a ______ /1001111 Hg a=====================•001 FKtl St"P a 1001111 Pb a ._------.. ~0•• ____ a _____ __,_1001111 s,a ·--~ ilOWllS: . ' -. , .' .· ;,.,--.:•>,-" :l J ...... . .--: DATt C!M'lETED: ____________ _ UI DIRECTOR U..EO:\,~ TORY Dlci.:.C',-cr, I I I I I I I I ' I I I I I I I r I - :2·~ ~ -•• . . . -!;'.' : i;:,, L ;...- -::':,._ .... ...~ ~1 ';L,' , :.; <.,, . /!AL < 2NVIRONMENTAL MANAGEl-!Em DIVISION SECTION: ,\Q 1=1 SHW :=: WQ I __,.i- ACTIVITY REPORT Page L of/_ Field Report Inspection ?hone Call TYPE OF ACTIVITY =j Consultation ::::+-6ffice Reper: =/ Ed. Presentation Other _______ 1 ============================================-=---=-=-=--=-=-===== = = - - - - = - Name (Facility/ Indv.): -(""/4,,-(11,, Cda,-q 'C Phone: ___ _ Address: /dlt)/ &oy, .{,// r?/ City: Lh'11C· Zip:_,_ __ ==========================================-=-=-=-=------===== ===------=-=-============-=-=================================----=== = = = = = Environmentalist: ~ Reviewed by: ----~--,'-,----,-S-u_p_e_r_v_i_s_o_r Date: ~#}z Date: Y, 1/87 I NE Cll.ElllUIIG COUNTT IVAml'.IIT (JI UVIIIOlf!ENTAI. HEAi.TM VIV I AOIMIIT Al UIORA TORY Field 1.0. '---------,"'°"------.i,;=- Slte s-l•d _..l.../Jt:.f.f!..t:,,Q~~~:.!L~~L.llli!i~:!!.'#':.!/ tff\ (Y\'r) ourc• S"{J_ s,1111111111 r;_'....t:i::..;,.~.1.r.1.""---- . Ptlhe ta •D On: in</ Ch.tr. c °" tt,..llil.""''¥-4,!..~ (jy l•D 1.0.I ~/0 Rec'd By >'-½k Dito Rec'd. 12./2.1 /qo Tl• l 3/0 5~ 1 Oltt S.,~led1_.e~'"'~ • g.-~ Otlfvtrtd I I I I I I PNYSICAI. PROPERTIES II NON•H!:TAl INORGANICS !II ORG.lll!CS Colar Q __________ .unlts Acidity Q ________ _.,,11111 Conductivity Q ....,/cm Alkallnlty Q _______ /'l"' Oil Jlssalvtd Sal Ids Q 11111 pH Q _________ ~un1ts.-0.-lk--Ae1«-r7 _______ .rPm Volatile Q 1111 Chlarldt Q _______ _,,1111 Phenol Q Fixed Q 1111 Chlorine, Re1ldu1l Q ____ _,,11111 d1roct photONtric _____ __,.Pffl Suspended Solids Q 1111 Ohsolved 01y91n Q _____ ..rllll chloroforn utractlan.:_...._ ___ ..rPb Valat11t D pno Fluoride 17 800 Q __________ _,opm Fixed Q pno spadns _________ ...rllll COO Q __________ _,.pm Tau I Sol Ids Q pa1 eltetrodt 1111 Surfactants /7 Qin Vaht11e Q pa1 Nitrate Q IV M!NERAl METALS Fl111<1 Q _____ _;,1111 ' Temporoturt Q ac UV spoc. ________ -1'1111 Cu G __________ __,.pm chromotrophlc acid pa1 Ft /7 __________ __,.i,,,- I I I I I I I , I Turb1dl ty Q _______ ____;JTU Hardneu Q ________ _,.1111 __ a ______ _ Vt CHEMICAL COl'IPOSITION Organic Q _________ s lnO"Janlc Q _________ s Moisture a ' VII RADIOACTIVITY Wattr ,.,,.,nh Nltragen Q Mn Q __________ __,.ll" t1trlmotr1c pa, Zn Q __________ __,pir nos1!1r1z1tlan. ______ ......,1111 "9 17 pa lt.ltldthl Nltl'09tn Q ____ _,.1111 C. Q Pl! Bromide Q 1111 NI 17 __________ __,.pr. Pllo1pharu1 Q 1111 K Q ___________ ..,.1111' Sulfate O Na Q pr. gravl•tric 11111 _ a __________ __,pr turt>idl•trlc pa1 V TOX!C METALS -~ran Alpha D---'-----'""1/1 Sulfide Q P110 Ag a __________ __,.pb Grau Beu Q ______ _p<1/1 ___ Q _______ _,11111 As Q pt Air Vil BACT£RIOlOGICALS la Q ~--·· pt l ) Grau Alpha a _______ pc1/n,l Foc1l eo11, ... D---~r.;_-.--' lCOIII Cd a-:-' ,1.-1. , prt Gros; Betl a _______ ,..11.,J Tout Collfara Q / I '-~~Ii'~ d'I' £,IV t·:OH. ppb llan•Collfara D \/ /lOOIII Jl!!.B:r.:..n.:..;.A..,-::...;P;;..I_R_!;;_C _____ __,ppb I ~S-./•·· / '"" Focal St"p a 100.1 Pb Q __________ _,.pb :...... _________ __,.pb _., ..... OAT£ ll)l'lETED: ____________ _ Sou rc1 S-1 td .-cnOIIUIIG COIIITY D[PAIMNT OI [NY! IIONOTAL HEAl llt VIV I IIOIIMOIT Al LJIORA TORY lab I.0.1 __ __,,-=,...;_...,. ___ _, Rae 'd By'_..;__2,L,j~~i..::::~---= 01 ta Rae' d, __ -J~...:::~,;.,::~-.,...,. I S•l!lllltd By "" t:' Olta1~~"4<~~.,.J~~la$~"4',:JA. 0.U SUipledl~~rL.:~TI• #,31$ Tl•·-----'-"-'-----..._._ I PMYS!CAI. PROPERT!ES ti NON-~TAL INORGANICS Ill ORGANICS I Color 0 _________ ....;unlts Acidity a ________ JPIII -?.~-:"==~s=:::::--iJ~r---.J'II" Conducth1ty D ....,,c,n Alkalinity a _______ JPIII I ~luolvtd Solids D pa pH a __________ u.nlts O,;:rg::-.::.:.1::-c-=rr-r-i ______ _,, Vol•t11t D pa Chloride D pa Plwnol 0 Fixed D PIii O,lor1ne, Residual D PIii dl~ct photoaatrtc _____ _,,I Suspondtd Solids Q _____ _,,PIII Olssolvtd Oxygen 0 _____ _,.PIII chlorofona utractlon . .:......._ ___ .,rPt Voht11e D pa Fluoride // 800 a __________ _;•I Fhed a _____ _,.PIII spadM _________ ..rPIII COO a __________ _,.p, Total Solids a _______ _,,pa electrode pa Surfactants a _______ __,., Vol1t111 Q _____ _,.pa N1trata O !V MINERAL METALS Fixed D pa UV spec. ________ _.,,pa C.. C J8. Temi,er1ture 0 ________ 0 c chromtroph1c acld, _____ _,.p,o Fe a __________ __,.,,_ Turbidity a ________ JTU Amonll Nltrog1n O Mn Q i Hardness a ________ _,11111 t1trlmetr1c pm Zn a __________ __, ___ a _______ _ VI CHEMICAi. COP!POS!T!Off O~anlc a _________ l lnorg1n1c Q ________ l Mo1stur1 a s VII RAO!OACT!V!TY Water nesslerhatlon. ______ _,1111 Ilg /1 __________ _,.p, Kj1ldlhl Nltl'Ck)ln a ____ _,ppm Cl a I 8l'Clllde a 11111 NI ,, p, Pllospllon,s D PIii K a ti Sulf1ta O NI D ~ grnl•tr1c ... _ a I tu1"11ldl•tr1c Ill V TOX!C METALS "Gross Alphl 0 __ _,.;.. ___ _.,,,1/1 Sulfld1 D PIii A9 0 __________ ..rPI Gn,u B1ta D 1/1 __ D pa As D ~-t Air Yll BACTERIOLOGICALS Bl D , pl • • Fecal Collfor1 a _____ ...,,,lCOail Cd D -! ; /1,.•1 ,/ ,. Total Coltfo ... D f /100.1 Cr g __ '...:ic..' __ IIV _ __,'=· .,.... __ __,P, i I_/ 11/V'AV .., REC\· .... ·•. lllln-Collfo,,. a ' /.lOOiil Hg a .-,;\'\': I)\ -. I Fecal St"110------10Qal Pb"fj_' ._,·"_· -----------,i; /?' ___ a c -,1~1 s.a • iIDW!kS: _ _,c_/4;.:;:v1!:'!..:.·1 ..... ,:...._~L@::....::;;~~~:::;.~~c";......,44i~<""i;:,,_,.::&,:a;.::1/:..,_.::a;;:.h=;~: .... 1'--_,c_/2~~:.:::LS'"=:2... _5.~e:?.;;.:'.,<";;;~~..!:f....----;,4-----~- Gross Alphl a ______ _,,,_1/.,l Gross Beu D 1/-3 \ (.\'-DATE Cllll'lETED: ________ ·;;., ____ _ I .f :.-., ·"l s·' '! r·) _l_ • .-'-:.;,_,_ ,_;,· ~Cll.EJIIUIIG COIJITY otPAIMIIT 0, DYi IIONl'IENTAI. HEAi. Tit VIV IAOIIOTAI. UIORA TORY Field 1.0. I ~ \ ~::.:~1~~/oz:i~ Yd-$ Gi/~if d aA~~_} Source SOllllll~Uife/1 {?f:.:Sc<!-l!i:)<~[hqf{ O.lhere'd to Lib On: ,~.,,.,.,/In,. ,,,_ .. "'" ~-v . (jy ~:.:·:~· s:t~:t; OltaRlc'd .....-1-,,, .... I ltA . -0l ta 4?V'3'.St ,v T ··-F -< n .... ~,NI yj.,... ;;: .'ff2.. S•mp1td By 'Cf /\ O{fCffL '-' I , 7 Oltfve"d ly fl./ l"'f:£C//k: I I -I -.. 1111 I PHYSICAL PROPERTIES II NON-METAL JNORGANJCS lll_OIIGAN_ I cs Color Q units Acidity Q ________ _,,111 ~ Conduct1v1ty a _______ ..... ,on Alkalinity a ______ _,.~_ 'l'lSliW,:, ~inolved Solids Q _____ _,.pa pH Q _________ --'units Organic Acids Q _______ .rP~ _ppn r;;. Volatile Q _____ _,.pa Chloride Q _______ _,.p:11 Phenol Q Flud Q _____ _,.p:a Chlorine, Residual Q ____ _,.p:a direct photo:netric, _____ __,p, Suspended Solids Q _____ __,.p:a Dissolved Oxygen Q _____ .JJ)III chlorofona utraction pt Volat1le Q _____ _,.po, Fluoride Q BOO a _________ _,.pn Fiud Q _____ _,.p:a spadM. __________ _, pat coo 0 _________ __,,pn Taul Solids Q ______ __,,pa 1tectrode _________ _,p111 Surf&ctonts Q _______ _.,pn Volatile Q po, N1trata D JV "INERAL MJJ_Al_S_ Flied Q _____ .rp111 UV spec _________ _,.pm eu a __________ _,.P-• Temper1ture Q ________ •c chroaotn,phic 1c1d. ______ rPII Ft Q __________ _,,i,, Turbidity Q _______ --'JTU Allooni& Nitrogen D ~a _________ _,."' Hardness Q ________ _,,pa, titrimetr1c. ________ _,.pm Zn Q __________ _,.pr __ a ____ _ ness1eriz1tion. _______ _,P1, lt;J /1 __________ _,.p, VI CHEMICAL COPV>OSIT!ON l(jtldlh1 Nit1'09tn a ____ _,.pm ~a ________ -✓p, Organic Q _________ l Bro111de a ________ pm Ni Q __________ _,,pi Inorganic Q ________ s Pllospllon,s Q ______ __,.pm, KQ _________ __,.p, "-1sture a_,-_______ s Sulfate a Na Q ____________ ,.... VII ~AOl9ACTIVITY 91"a• t•tr1c _______ _,.p111 _a ________ _,."' water turtlidi•tric ______ __,lllXI V TOXIC HETALS -~ross Alpllt Q __ ....;. ___ .....J,.._i/1 Sulfide Q ________ ..rPI Ag Q __________ _,.pt Gross Beta Q _______ _ri/1 __ a _______ ...,.om As a _________ _,.ot Air VII BACTERIOLOGICALS Ba Q __________ _,,pt Gron Alpllt Q _______ ,_1/.,l Fecal ColifoN Q ____ __, lCO.l Cd Q __________ _,.rt Gross Beta Q _______ _,..i/-3 Total Co11foffl Q _____ /1001111 Cr Q __________ _,.pt Jlon•ColifOffl Q ______ /100ml Hg Q __________ _,.pt Fecal Strep O _____ __, 100:ol Pb Q , pt * ---a ____ -'-.., ,00ro1 s. a . ---------KOOAKS, ..S:,•/./2,14 !/ :>? v I OAT{ C!M'lETED: ____________ _ UI DIRECTOR __________________ _ '·' I ~ I I I I I I Memo Date: August 11, 1995 To: File From: Douglas Moore 41!:,,(,u,,...____. Environmental Chemist NC Superfund Section Re: Ownership History Cherokee Oil Company Site 1201 Berryhill Road Charlotte, Mecklenburg Co., N.C. US EPA ID: NCO 980 799 019 On August 9, 1995, Doug Rumford visited the Mecklenburg County Tax Assessors Office, located in the County Government Center at 720 N. Fourth Street, downtown Charlotte to review the available deed information for ownership history of the subject site. Mr. Rumford was able to trace the site ownership history back to 1961. A summary of the ownership information is provided below: (I) Deed Book #5828, Page O 131. Quitclaim Deed for Tax Lot #071-051-16 transferring ownership from Billie M. Hartsell, grantor, to Gene W. Hartsell, grantee, on May 25, 1988. Being the property shown on the bou·ndary survey dated 06/05/58 showing property of the Arkansas Fuel Oil Corporation. (2) Deed Book #4651, Page 0338. Deed· for Tax Lot #071-051-16 transferring ownership of the property from Spurrier Oil Company, grantor, to Gene W. Hartsell, grantee, on April 14, 1983. (3) Deed Book #4800, Page 0985. Deed for Tax Lot #071-051-16 transferring ownership of the property from Gene W. Hartsell and Billie M. Hartsell, grantors, to Centennial, Inc., grantee, on April 14, 1983. 1 I I. I I I I I I ii (4) Deed Book #3985, Page 0859. Deed for Tax Lot #071-051-16 transferring ownership of the property from Union Oil Company (sucessor by merger to The Pure Oil Company), grantor, to Spurrier Oil Company, grantee, on August 25, 1977. (5) Deed Book #2265, Page 0204. Deed for Tax Lot #071-051-16 transferring ownership of the property from American Mineral Spirits Company, grantor, to The Pure Oil Company, grantee, on August 1, 1961. There is also a site map showing the historical site layout in Deed Book #3985, Page 0862. 2 I I N'-..V IL-'U'i'?IUi/ S C!'~)THTE~--';orp. Hr. O.W.Striclcland Department of Hw..an Resources 306 H. Wilnington St. fulei(;h 11._c. 27(;{.)2 . 1201 Berryhill htJ. - Charlotte, NC 28208 (704) 332-8663 24 Sept I' 1983 ·. C __.. ' ,I<;>,.~ J{.,<> Dear Br· Strickland, ., 1· ( 1-l 11 I . . , Enclosed are EPA forms B700-12 for our recently open ad pbnts in -T~a. an~ ?ort · Orange FL _along uith one for our Charlotte N.C. plant. . /.l · . · I The location in Chc.rlotte is in all .:i.::;)ccts the same) ot:}°;: t.'--__ '"' J1..e0_a=..J1• ting our oil r0cover:,-and 1rcistc oil colbcoion operations e1 · Chc~~--Oil Co ·-·-. opera- ., .. I I ·1 also .. haVe sent COiJies of the Flor-ic1.: operations to I:2J\ reGio:1 four .. If I have ; ~~}::·:.-:- missed · or --overlooked any .other D::!pt .. ·to no-Gify please 2dvic0 r.1e .I Follld like to em- phasize the foct that 110 have never ancl do not intend on tr2.ns(JDrtinc any hazc:rdous or tax:ic "H.3.ste · or chemicals_ .. Tho product th::.·.t. He a quire arc s lo~J crudes) virGin oil tra'nsr.ri.xes, diesel., cr,3.nkc2.3e 1-:i-as te oils) o.r!cl residua lfuels. These plants ·ore· in O!_)eration now,if t~ere is ,;;.n:rthinc; else th:i.t I need to do fer t..."rie Dept, of HUT:10.n R~ources., plea0e real free to c2ll 2.t our Ch.J.rlotte office, ·(704)332-B663 or at ho~s ( 704) 398-1701 I lit 1• /( ')· \lJ~CC:IT~. iCci th =:id.son South tee Corp.: >" SOUTHTEC , CORP. KEITH N. EIDSON 1 201 i3EARYH!LL F'l()A[:;, CHARLO-;-:"t:, N.C. 28/i :> I , , , .:·, •• 1·~,c", -· ·•... ,. Form Approved-OMS No. 158-S79016 ~:. ( 12 characters/inch) j 01_h_e_u_n_,_h_a_d_e_d_a,_e_a_,_· o_n_l~y_. --,.,--------,----G_s_A_1,__,?· 0246-£ PA-O T r1 •·,s. ENV/RONMEN,: ·•ROTECTION AGENCY ,r·,-,. / .JTI F:,vATI0N ·OF HAL mous WASTE AC,IJ,. ITY INSTR UC IS, If you recoived a pcepdnted -----,-----------~---,------------~-----1label, attix it iii the space at left. If any of the information on the label is incorrect, -draw a line through it and Supply the correct information in the appropriate section below. If the label is complete and correct, leave -Items I, II, and Ill below blank. If-you did not receive a preprinted label; complete alf items. "Installation" means a single site where hazardous waste is generated, treated stored and/or· disposed of, or -a trans- 1 place of business. Please refer NS FOR FILING NOTIFl- leting this form. The· rein is required by laW · urce Conservation and .. OWNERSHIP VI. TYPE OF HAZARDOUS WASTE ACTIVITY (en1er "X" in 1he epproprialc box/es)) FEDERAL NON-FEDERAL □A. GENERATION " . gB. TRANSPORTATION (complete item DC: ·:TRE~:T;STORE/DISPOSE: Do .. '" MODE OF.TRANSPORTATION (transporte,:s oniy -· enter "X" in the appropriate hox(cs}/ □A. AIR .. ·.Oe. RA1L·'· · " Oc. WATER .. OE. OTHER (spPcify): .. Il. FIRST OR SUBSEQUENT NOTJFICATION ,.~'~f&:~~jf~i1~UJ1:1t[~~~t£~~; rk "X" in the appropriate box to indicate whether this is your installation's first notificatiCJ11 0f !laZBrdou~ waste activity or a subsequent notification. his_ js not you; first notificatiOn, en~_er your lnsta/lati_on's ~PA. !.D. Number.in the srace provided below. DESCRIPTION OF HAZARDOUS WASTES asc go to the reVE!r~ of this form and provide the requested informdtio11._ Form 8700-12 (6--80) CONTINU~ ON REVi.:RSE i I_ F..::.· ..... I IX. DESCRIPTION Of HAZARDOUS WASTES (continued from front) ." HAZARDOUS WASTES FROM NON-SPECIFIC SOURCES. Enter the four-digit number from 40 CFR Part 261.31 for each listed hazardous waste from non-specific source~ your installation. handles. Use additional sheets if nece~ry. ' ' " ,, " • n·-,:-,:' ~{3:i .. • ... -·-:{ ,..f-.--r--r-•V: · .. :_~ -':1-,~~:--( .... =-~~-' u·------n· n----•··-N ,o . ZJ 24 26;,' 28 " 30 COMMERCIAL CHEMICAL PRODUCT HAZARDOUS WASTES. Enter the iour....:digit number from 40 CFR Part 261.33 for each chemical sub- stance your instaU.at~_handles which may ~.a hazardous Waste: Use additional sheets if necessary . ., •.. , '•----.... ---' .J,.... .. . . . ·i' :" . . . ... ;-;-c+-....-"'--,·./ ,, /',"" . ··..! 34 36 2)··--.----u ,. 40 " " 46 47 48 D. L1STeo:_1_NF-ECT·JduSvyAS0TES.· Enter the four-digit number from 40 CFR Part 261.34 for each listed hazardous was,e frorn hospitals, veterinary hospitaiS;·m.e~.i~l'a~5!._re·sea·rch lab6ratories Y0!.!r. in_stalliltion.handles. Use additional sheets if necessary. ,o " " " " " CHARACTERISTICS OF NON-LISTED HAZARDOUS WASTES. Mark "X" in the boxes corresponding to the characteristics of non-listed hazardous wastes your installation handles. (See 40 CFR Parts 261.21 -261.24.) D1. l~NIT~D~~ (0001) 0·2. CORROSIVE {DOOZ) 03. REACTIVC (0003) 04. TOXIC (0000) X. CERTIFICATION under penalty of law that I have personally examined and am familiar with :he information submirted in this and all documents, and that based on my inquiry of those individuals immediately responsible for obtaining the information, I beliei-e that the submitted information is true, accurarc, and complete. 1 am aware that there are significanr penalties for sub· mitring false information, including the possibiliry of fine and imprisonment. NAME&: OFFICIAL TITLE (type or print} DATE SIGNED :----.· \-tz_ ~ S \ D t._ 1-.3-;--\J C" --\ ..;_ ' \ \-\ EPA Form 8700--12 (6-80) REVERSE I , n I ,... I I , I I I I I SOOIH CAROLINA DEPARTMENT OF HEALTH AND ENVIRONMENT/lL OJNTROL BUREAU OF SOLID AND HAZARIXJUS WASTE MANAGEMENT Hazardous Waste Transporter Permit conditions Cherokee Resources, Inc. Conditions Permit# NCD980799019 October 23 1987 1. 2. 3. Operations should =nform to the information pertaining to your activities as described in the application for permit and all applicable provisions of the S.C. Hazardous Waste Management Regulations, of the S.C. Public Service Ccirmnission Regulations and of the Federal Department of Transportation Regulations. In the event of any change in the coverage of the policy concerned in the Certificate of Insurance, an up:lated Certificate of Insurance shall be signed by an authorized repres,,...ntative of the Insurance Corrpany who is authorized to sign such forms for the Insurance Corrpany and the form sent to the Department. The permittee will be responsible for the prepcL.----ation and submission of Quarterly and/or annual reports as required by the Department. Ill I I I I I It I I I I I I I Memo Date: August 11, I 995 To: File From: Douglas Moore Environmental Chemist NC Superfund Section Topic: Secretary of State -Business Information. Cherokee Oil Company 1201 Berryhill Road Charlotte, Mecklenburg Co., NC USEPAID: NCD9807990l9 On this day, I spoke with Dan Norris, Corporate Specialist with the NC Secretary of State's Office (733-420 I) regarding information available about prior businesses that operated at the subject site. The following information was provided by Mr. Norris: (]) Cherokee Resources Incorporated as a North Carolina Corporation on October 24, 1983. Registered Agent: Gene W. Hartsell 1201 Berryhill Road Charlotte, NC 28202 no annual reports filed. Administrative Dissolution issued on November 17, 1993. Revenue Suspension issued on December I, 1994. (2) Southtec. Incorporated as North Carolina Corporation on May 31, I 979. Registered Agent: Joseph W. McGuirt 3000 NCNB Plaza Charlotte, NC no annual reports filed. Administrative Dissolution issued on January 11, 1993 .. (3) Spurrier Oil Company Incorporated as a North Carolina Corporation on April 25, 1939 in Mecklenburg County. no registered agent. no annual reports filed Administrative Dissolution issued on December I, 1993 .. Revenue Suspension issued on May 31, 1989. I I I I II I I It ii I I I I I I r I I I I (4) Centennial, Inc. (5) (6) (7) Incorporated as a North Carolina Corporation on June 25, 1975. Registered Agent: Gene W. Hartsell no annual reports filed 6425 Springfield Drive Charlotte, NC Administrative Dissolution issued on March 7, 1979. Revenue Suspension issued on March 17, 1989. Union Oil Company Incorporated as a California Corporation on January 27, 1953. Registered Agent: C. T. Corporate Systems 225 Hillsborough Street Raleigh, NC 27603 Active and current status. Officers: Richard I. Stagemeier, CEO Roger C. Beach, President John F. Imle, Jr., Exec. V.P. Pure Oil Company Incorporated on July 19, 1965. Registered Agent: C.T. Corporate Systems (address same as above) active and current status Officers: R.C. Beach, Pres. R.E. Wright, V.P. D.P. Condon, Secretary D.D. Chessum, Treasurer. American Mineral Spirits Co. Incorporated on November 4, 1968. Registered Agent: C.T. Corporate Systems (address same as above) Officers: William F. Murphy, Pres. James W. Crase, V.P. D.B. Ezanik, Secretary Darrell D. Chessum, Treasurer Mr. Norris stated that there was no information available for the Arkansas Fuel Oil Company. 2 (A I; I I I I ~ I I I I I I I I 19 I I I I I I .. I I SDH' JW:E R R B ; 5-31-86 ; 15 :31 ; t:t'AKtulUN JV➔ ~I~ 733 4tlll:f 1/lU . . TO: (J. 0 EMERGENCY RESPONSE & REMOVAL BRANCH U.S. EPA REGION IV . RECEl\/!=D 345 COURTLAND STREET N.E. ATLANTA, GEORGIA 30~ PHONE: (404) 347-3931 FAX: (404) 3474«4 / REGIONAL RESPONSE CENTER FACSIMILE TRANSMITI' AL SHEET \~t)U·-3 'fv\.o~f e__ MAY 31 i996 SUPERFUND SECTiON TELEPHONE: FROM: TELEPHONE: . NUMBER OF PAGES INCLUDING COVER SHEET: MESSAGE: IF THE FOLLOWING MESSAGE IS RECEIVED POORLY OR INCOMPLETF., PLEASE NOTIFY SENDER. / ..,..,.,...,- I .. I •.• -i3Y:E R R B 15:32 319 733 481 J; # 2/10 I I I I I I .. I I I I I I I .. I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION IV 345 COURTLAND STREET, N.E. ATLANTA.. GEORGIA 30365 4WD-ERRB ACTION MEMORANDUM SUBJECT, Request for a Remova.l Action Berryhi11 Road Site,cf'U'kn,,, at the Cherokee Oil-CoWl.ty, North Carolina. FROM: TO: I. II. Steve Spurlin, osc~ EI11ergency Response & Removal Joseph R. Franzmathea, Director Waste ManagQillent Division Site ID: WD PURPOSE The purpose of this Action Memorandum is to request and document approval of the proposed removal action described herein for the Cherokee Oil-Berryhill Road Site (the Site), Mecklenburg County, Charlotte, North Caro1irul. SITE CONDITIONS AND BACKGROUND ,/ i' A. Site Description 1. Removal Site Evaluation -On August 26-27, 1994, the Emergency Response & Removal Bra.nch (ERlU3) conducted o site investigation at this facility which fonnerly operated as a waste oil handling facility which allegedly blended hazardous wastes with non-hazardous waste, Company official5 are currently awaiting sentencing after being convicted of Clean Water Act (CWA) violations for disposal of oil and chemicals into the city sewer. Approximately 1000 drumS in various stages of deterioration 'llrere observed closely stored and precariously stacked on the facility p,:oporty. ln addition to the drums, approximately 13 aboveground tanks, 2 tanker.trailers, lllld 1 roll-off, suspected to contain hazardous .substances, are abattdoned on-site, Dur!ng the investigation, a large quantity of oily waste material, suspected to have leaked.from the drums and tanks, was observed covering the ground on-site • There was eYidence that waste material is migrating onto adjolning properties, .. I I I I I I I .. I I I I I I / .. I I 2. 3. 4. ; 5-31-86 . ·,, , EPA REGION IV➔ ·-'\ 818 733 4811;# 3/10 Samples collected during the investigation confirmed the presence of numerous hazardous substances including ethylbenzene, 1,1,l trichloroethane, styrene, chlorobenzene, and numerous drU1ns containing corrosive liquids. Physical Location -The Site is located. at 1201 Berryhill Road, Mecklenburg County, North Carolina. Drums stored on-site are located within a few feet of a busy city street and the Site ia closely bordered by two operating businesses. During the investigation heavy pedestrian traffic was observed along the road bordering the facility. The area consists of urban mixed residential and light industry. Site Characteristics -The Site was fo:z:merly the location of the Cherokee Oil Company, who accepted waste oil and various hazardous substances for processing and shipment to other facilities. It"'"is auBpected, based on observations during the investigation, sample results from the BRRB investigation, and a previous RCRA investigation, that the facility was accepting hazardous substances and hazardous waste that it was not permitted to accept and blending this material with waste oils, The owner and operator of the facility were convicted cf CWA violations in Federal court and they are currently awaiting sentencing. J ' The Berryhill Road facility is associated with the Cherokee Oil-Summit Avenue superfund Removal Site at which EPA ERRS conducted an extenBive removal beginning in August 1991 and concluding in March 1993. The EPA spent in excess of$ 3 million to mitigate the i.lllmediate threats posed by the waste stored at the Summit Avenue location. The Berryhill Road facility wae used by Cherokee Oil as a waute processing facility, and the Summit Avenue site was used for storage of various waste. The operator of both · facilities, Keith Eidson, informed the OSC during the investigation that both facilities are no longer operating, Release or Threatened Release lnto tlK> KnviroliJllQnt of a Hazardous Substance, or Pollutant or Contaminant -EPA has determined that a release of a hazardous substance as ~efined by section 101(14) of CERCLA. has occurred at the Site.· Analytical data and field testing results indicate the preseru:,e of numerous hazardous substances including, but not limited to, chlorobenzene, . tetrachloroethene, 1,1,1-trichloroethalle, bis-phthalate, naphthalene, lead, and chrollli1I11t, I " ,/ .. I I I I I I I .. I I I I I I .. I I ..,.,,,,..--~/__..· .,.BY:E RR B s. -6. B, 1. 15:32 E P A REGI<lt IV_, "1 919 733 48]1;# 4/10 In addition to the hazardous substances detected in the ER.RB investigation samples, field testing during the investigation indicated that nine of sixteen drum samples collected during the investigation had pH levels below 2.0 units or exceeding 12.5 units which classifies this abandoned material a ha~ardous waste based on the characteristic of corrosivity. ·Hund.reds of other drums on-site have corrosive labels indicating that they likely contain materials similarly classified as a hazardous waste. The caustic and acid Li.quids contained in these drums are incompatible with the numerous drums containing organic materials stored on-site. Reaction between the two materials could result in fire or explosion, exposing nearby businesses and residents to hazardous fumes. In addition to the drums, an estimated 125,000 gallons of wa·ste oil contaminated with various hazardous-substances is currently stored 1n tanks, vats, tanker trailers, and tank dike areos on-site.· .11.n oily sludge covers the ground and two dike a:reas full of oily liquid are near over-topping. ~he osc observed staining and residue where an oily liquid was migrating off-site onto an operating business during rain events • Also, off-site cont!ffllinant migration could reach the city sewer system and pose an exp}osion hazard. } NPL Status -The Site is not currently listed on the NPL. rt is likely that once the removal is completed the Site will not have sufficient threats to warrant ranking on the NFL; however, all information generated during the removal will be made available to the EPA Site Assessment Branch for evaluation. Maps and Other Graphic Representations -All removal file information, which includes photos, sketches, maps, etc., will be maintained by the OSC, and rele<ll!ed to the EPA record center for incluaion in the 1i'ite file. Ql;her Actions to Date Previous Actipns -In July 1991, a orilllina.l investigation was conducted by the EPA Ha~ardous waete Section, the EPA Criminal Investigation Division, the Offlce of·the FBI, and several other supporting a.genci-,s. A ci:iminal search warrant was served to the operator of tha facility, and a site investigation wtl6 le I I I I I I I .. I I I I I I .. I I I Ill. 2. c. ; S-31-96 "') ' 1s:33 EPA REGION IV➔ .--.. ,. 919 733 4811;# 5/10 ! conducted at the both the Cherokee Oil-Berry Hi.J.l Road .location and the Cherokee Oil-Summit Avenue .location. From August 1991 to March 1993 the EPA ERRB conducted an extensive removal action at the Cherokee Oil-Summit Avenue location. As a result of the cr.iminal investigation, the owner and operator of Cherokee Oil were convicted of criminal charges for Clean Water Act violations related to discharge of hazardous substances to the Charlotte sewer system. They are currently awaiting sentencing. Current Actions -There are no current remediation or additional investigatory actions for this Site. The osc is aware that the Charlotte Fire Department has been attempting to gain access to the Site to conduct an inspection, but they have been denied access by the operator of the facility. State and Local Authorities Role 1. State and Local Actions to Date -The State of North Carolina Department of Environment, Health and Natural Resources (DEHNR) has issued Cherokee Oil a Notice of Violation for solid and hazardous waste regulation violations, The operator of Cherokee Oil has denied the DEHNR violations stated in the NOV, In a January 1994 letter, the DE:HNR requested that the EPA ER.RB evaluate the Sita £or a possible removal action. I The DEHNR, the Charlotte-Mecklenliurg Utility Department, and the Mecklenburg County Environmental Protection Agency participated in the July 1991 investigation of the Berryhill Road and Summit Avenue Cherokee Oil facilities. Several of these local agencies provided testimony and evidence for the , criminal trial that was concluded in August 1994. 2. Potential for Continued State/Local Response -The -DRH:NR has requested that EPA undertake a removal action at the Berryhill Road site. Since the criminal trial is over, and the ERRB will be conducting the removal action if this memorandum is approved, there will be 11ll1ited direct involvement by the state or local agonciea related·· to the EPA removal. The OSC will contact these agencies to determine what reaourcos they can provide to assist in the removal action. I . THR!iATS 'J,'O PUBLIC HBAI.TH OR WELFARE OR THE ENVIRONMENT A . Threat to Public Health or Welfara The EPA ERRB has determined that a release of a hazardous substance into the environment has occurred .. I I I I I I I .. I I I I I I -. I I .• 5-31-96 15:33 919 733 4811;# 6/10 at the Site, as defined by Section 101 of CERCLA and established .i.n Section 102, Part 302/'l'able 302. 4 of CERCLA. Summarized below are the specific criteria from Section 300.415(b)(2) of the National Contingency Flan (NCP) that the Site meets for initiating a removal action baaed on threats to public health or welfare. The Site poses an actual or potential exposure to hazardous substances by nearby populations. Over 1000 drums, many leaking, are stored in close proximity to a busy road. Drum samples indicated the presence of numerous hazardous substances including volatile and semi-volatile compounds such ae oonzene, methylene chloride, 1,1,1-trichloroethane, acetone, and naphthalene. Some of the drums, tanks, and vats on- site are suspected to have already leaked onto the ground. A sample from the waste material covering the ground indioated the presence of hazardous substances including benzene, chlorobenzene, methylene chloride, acetone, and xylene. During the investigation, tJi.e OSC observed an area on the back-side of the facility where waste material is migrating ott-site onto the adjacent business parking lot where exposure could occur. The Site also meets NCP criteria related to fire and explosion potential. Many of the drums contain corrosive materials which may be incompatible with the large quantity of organic liquids stored on-site. A fire or explosion would neceseitate the evacuation of hundreds of people from businesse~ and homes around the Site due to the potential for expos'lre to hazardous fU111es. There are hundreds of drums, numerous tanks, vats, dikes full of waste liquids, and'othor bulk storage containers, that pose a threat of release. There is . over 100,000 gallons of waste liquids and sludges stored in the open top vats and tanks. Several of these tanks appear to be leaking onto the ground ana into the unmaintained dikes. NU111erous drums are stacked precariously on pallets directly adjacent to the road and could easily fall during high winds or rain. As previously stated the ground in covered w1th waate liquid and sludge. 'l'he majority of the Site is believed to be covered with a concrete pad which facilitatesioff-site migration. Stormwater runoff carries contam1nat1on Off-site and eventual leads to the'city sewer syatem. The operator of the facility has been convicted for past illegal discharges to the city sewer. -. I I I I I I I .. I I I I I I ~ I I IV. v_ ; 5-31-96 )5:33 818 733 4811;# 7/10 • B. Threat to the Env.i.ronment There are hazardous substances in drums, tanks, vats, and other bulk storage containers that may pose a threat of reiea:;e. The containers are deteriorating ·and numerous containers are leaking. There is an actual or potential exposure to ha~ardous substances to nearby animals or the food chain. During the ERRB site investigation a bird was observed trapped in the oily liquids in a dike area, The bird was rescued and cleaned, but later died at the animal shelter due to exposure to the waste. ENDANGERMENT DETERMINATION The actual and tlu:-oatened releases of hazardous substances from the Site, if not addressed by il!lplementing the ~esponse action selected in this memorandum, will present an imminent and substantial endangennent to public health, or welfare, or the environment. PROPOSED ACTIONS AND ESTIMATED COSTS A. Proposed Actions 1 . Proposed Action Description -The ERRB will •itilize the ERCS contractor to eample, secure, and characterize the various waste streams on-site. }faterials deternunad to contain hazardous substances that pose a threat will be treated on-site and/or transported to and disposed of at a pennitted disposal/treatment facility. All off-site disposal will comply,with EPA's off-site disposal policy_ 2. Contribution to Remedial Perforniance -The Site is not currently on the NPL. The proposed removal actions will not impede future reiaedial responses based on the available information, and data generated during the removal will he forwardM to the Site Assessment· Branch for consideration. J. Description of Alternate Technologies -Disposal optiona will be _evaluated at a later date during the removal action .. 4. Applicable or Relevant and Appropriate Requirements (~) The potential Federal ARAR's for the proposed removal action at the Site are those portions of the Resource Conservation & Recovery Act (RCRA) dealing with land ·, disposal restrictions and storage of a hazardous waste. I / .. I I I I I I I .. I I I I I I ~ I I I 5. 6. B. ; 5-31-96 S19 733 4811;# 8/10 • The ERRB intends to comply, to the extent practicable, with the substantive requirement,; fo_r these ARAR's. The RCRA and Department of Transportation requirements for transportation of a hazardous waste were determined to be applicable to any off-site actions. Therefore, the ERRB will comply with the administrative and substantive requirements which may be applicable. No State ARAR's have been identified yet as substantively additional ARAR's. These requirements will be evaluated as they are identified during the removal and complied with if applicable, 8E/CA -This is a time critical removal not requiring an EB/CA. Project schedule -Upon approval of this memorandum, the ERRJl removal would be initiated within two weeks, The first phase of the projQct will involve sampl~ng and securing the drums, tanks, and other bulk containers on-site. Due to the large quantities of containers on-site and the limited working space, the first phase of the project will take approximately four months. The total project including ultimate treatment/disposal of any waRte matGrials is estimated to take approximately eleven months • E1>timated Costs Extramural Costs Regional Allowance Costs: Clean-up Contractor Costs (15% Contingency Applied) Other Extramural Costst TAT Costs: Subtotal, Extramural Costs: Extramural Contingency (20%) Total, Extramural Costs: Intramural costs , Direct Costsi Indirect Costs: Total, Intramural costs: Total Project Ceiling: $1,450,000 $ 75,000 $1,525,000 $ :rns,ooo $1,830,000 $ 15,000 $ 27,000 $ 42,000 $1,872,000 la I I I I I I I ff I I I I I I ' • ,5-31-96 E f A REG. IV-> 919 733 4811;# 9/10 VI. EXPECTED CHANGE IN THE SITUATION SHOULD ACTION BE DELAYED OR NOT TAKEN If action is delayed or not taken, the risks posed to the public health or welfare and the environment would increase. Delayed action will increase public health risks to the adjacent population through exposure to off..,,ite migration • of contaminants from leaking containers or via contact with airborne emissions should a fire occur. VII. OUTSTANDING POLICY ISSUES None. VIII. ENFORCEMENT Seo Enforoemont Sansitivo Information Attached. IX. RECOMMENDATION Because conditions at the Site meet the NCP Section 300.415 criteria for a removal, I recommend your approval of this removal request. The estimated total project costs are $1,872,000, of which $1,450,000 are for the extramural cleanup contractor costs. You may indicate your approval or disapproval by aigning below. •PP=~~~~:!c:: \\¼L Disapprove: _________ _ Date: ------ I .. I I I I I I I 119 I I I I I 5-31-96 15:34 919 733 4811;#10/10 • ENFORCEMENT SENSITIVE Mr. Keith Eidson and Mr. Gabe Hartsell, the operator and owner, respectively, of Cherokee Resources (Cherokee Oil) are responsible parties for the Berryhill Road Site, The EPA determined that both parties were not financially capable of undertaking the removal action at the Cherokee Oil Summit Avonuo Sito in 1991-19931 therefore, thoy aro not currently considered viable responsible parties to undertake the clean-up at the Cherokee Oil-Berryhill Road Site. Both parties are currently awaiting sentencing in Federal court for CWA violations. It is likely that both individuals will be serving jail time for these violations. During the removal at Cherokee Oil-Berryhill Road Site, EPA will be generating Potentially Responsible Party (PRP) information from drwn label information and other records available on-site. EPA will determine the viability cit any PRP's identified and undertako tho appropriato onforcrunont action. I L l I. I ' ' ' ' ~ ' Ip 11 '• 11 ~. '• 11 , .. 1,1 II MEMO Date: 05/ 18/93 To: File From: Topic: Douglas Moore Environmental Chemist NC Superfund Section Discharge Permits Cherokee Oil Site 925 S.Summit Ave. Charlotte, NC NCO 986 190 239 Ref. 13 Today, I Spoke with Dawn Padgett, Systems Protection Specialist with the Charlotte Mecklenburg Utilities Dept, Systems Protection Division (1-704-394-9284) regarding permit and sampling information on the Cherokee Oil Site. Ms. Padgett stated that Cherokee Oil (aka Cherokee Resources) did not have a permit to discharge contaminants to the sanitary sewer. She referred me to Bob Griffin for more information. Mr. Griffin stated that the FBI/DOI has all their files relevant to the site ior their upcoming criminal indictment. He stated that on December 18, 1990, CMUD inspected the second Cherokee facility at Berryhill Road. He stated that they were told by the owner, Keith Eidson, that the Hazardous wastes on site would be removed in the future to a new site at Summit Ave. He stated that at this time, CMUD notified the Mecklenburg County Environmental Protection about the new site. Mr. Griffin stated that there was evidence of Hazardous waste disposal to the sewer from the Berryhill Road site. The evidence is currently being held by the FBI in support of their federal grand jury indictment. \cherokee\cmud I .. I I I I I I I t' I I I I I I Ref. 41 IN THE UNITED STATES DISTRICT COURT FOR THE WESTERN DISTRICT OF NORTH CAROLINA CHARLOTTE DIVISION j, UNITED STATES OF AMERICA v. CHEROKEE RESOURCES, INC., KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL, and THEODORE KA.tcL GLAUSER INDICTMENT The Grand JUfY charges: INTRODUCTION Violations of: 33 U.S.C. 1317 (d), 1319 (c) (2) (A) and 1319(c)(4), 18 u.s.c. 1001, 18 u.s.c. 371 and 18 U.S.C. 2 At all times material to this indictment: 1. CHEROKEE RESOURCES, INC. [hereinafter "CHEROKEE"] Jwas a corporation incorporated under the la· .. s of the State of· North Carolina, with its principle place of business at 1202 Berryhill Road, Charlotte, North Carolina. CHEROKEE was in the business of, among other things, reclaiming waste oil for energy recovery and treating and disposing of oil-contaminated wastewaters, as well as treating other industrial wastewaters. 2. KEITH NORLAND EIDSON was President and chief operating officer of CHEROKEE. EIDSON had a fifty percent (50%) ownership interest in CHEROKEE. 3 • CHEROKEE. CHEROKEE. GENE WESLEY ("GABE") HARTSELL was Vice President of HARTSELL had a fifty percent (50%) ownership interest in HARTSELL is an environmental engineer. 4. THEODORE KARL GLAUSER was comptroller of CHEROKEE and handled the accounting and waste manifests for the corporation. 5. The Federal Water Pollution Control Act, 33 U.S.C. 1251, et seq., commonly referred to as the Clean Water Act, was enacted by Congress to restore and maintain the integrity of our nation's waters. ·Pursuant to Section 307 (b) of the Clean Water Act, 33 u.s.c. 1317(b), the Administrator of the United States Environmental Protection Agency (hereinafter "EPA"] promulgated National Pretreatment Standards for all ''industrial users'' who discharged industrial wastewaters into public sewer systems. I - I le I I I I I I I I 11 :I I I ... I I 6. Under the Clean Water Act, all industrial users are prohibited from operating a source of pollutants in violation of any effluent standard or prohibition or pretreatment standard, 33 U.S.C. 1J17(d) and 1319 (c) (2) (A). Where specific prohibitions or limits on pollutants are developed by a publicly owned treatment works [hereinafter "POTW"] in accordance with federal regulations, such limits are deemed pretreatment standards for the purposes of section 1J17(d), Title 40, Code of Federal Regulations (hereinafter ''C.F.R.~] Section 403.5(d). In addition, all persons are prohibited from knowingly violating any requirement imposed in an approved pretreatment program, 33 U.S.C. 1J19(c) (2) (A). The purpose of a pretreatment program is to prevent pollutants from passing through or interfering with the operation of the POTW, or causing sewage sludge contamination. 7. The Charlotte Mecklenburg Utility Department (hereinafter "CMUD"] operates a permitted POTW known as the Inain Creek Sewage Treatment Plant (NPDES Permit No. N.C. 0024945) and has an approved industrial pretqeatment program applicable to CHEROKEE whose wastewater discharge flows through the sewer system to the Irwin Creek plant. The treated effluent from the Irwin Creek plant runs into the Catawba River which is a navigable waterway of the United States. 8. Toxic pollutants of particular concern, whose discharge to the Irwin Creek POTW is regulated, include Cadmiur.i, Chromiur.i, Copper, Lead, Nickel and Zinc, because of their potential td cause sludge contamination (and resulting hazardous waste disposal problems for the POTW), as well as Oil and Grease (0 & G), Total Suspended Solids (TSS) and Biological oxygen Demand (BOD), because of their potential to be toxic to the microorganisms used to treat the raw sewage. 9. The permit limitations on these toxic pollutants were established by CMUD in accordance with federal regulations (40 C.F.R. Sections 40J.5(c) and 403.5(d). Thus, these local limits are considered National Pretreatment Standards for the purpose of federal enforcement of the prohibition in JJ U.S.C. Sections 1J17(d) and 1Jl9(c) (2) (A), and they are considered to be a requirement imposed in an approved pretreatment program for federal enforcement under JJ U.S.C. 1Jl9(c) (2) (A). 10. On May 15, 1990,. CMUD issued a permit to CHEROKEE (permit number 0202), which limited the concentrations of certain pollutants that could be placed by CHEROKEE into the local sanitary sewer. More specifically, this permit set the following limits (measured in, parts· per million, or "ppm") on the discharge of wastewater from CHEROKEE to the sewer: I .. I I I I I I I I I I I I ~ I I Pollutant Maximum daily allowable concentration [parts per million) Cadmium Chromium Copper Lead Nickel Zinc Oil and Grease Total Suspended Solids Biological Oxygen Demand COUNT ONE 0.07 0.20 0.27 0.53 0.84 0.70 328.00 333.00 1563.00 1. The allegations contained in the Introduction of this Bill of Indictmenu are realleged and incorporated in this Count by reference. 2. From on or about May, 199 o, and continuing thereafter until on or about April, 1993 within the Western District of North Carolina and elsewhere, CHEROKEE RESOURCES INC., KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL, THEODORE KARL GLAUSER and others, both known and unknown to the grand jury, did knowingly, willfully and unlawfully combine, conspire, confederate and agree with each other and with other persons, both known and unknown to the grand jury, to commit the following offenses against the United States and the laws thereof: a. to knowingly discharge wastewater from a point source into the sewer system which flowed into the CMUD Irwin Creek POTW in excess of the CMUD effluent limitations and the National Pretreatment Standards, in violation of Title JJ, United states Code, Sections 1317(d) and 1Jl9(c) (2) (A); and during the course and in furtherance of the conspiracy, a member of the conspiracy did commit or cause to be committed within the Western District of North Carolina, at least one overt act. A. PURPOSE OF THE CONSPIRACY The purposes of the conspiracy were to max1m1ze profits and minimize costs of CHEROKEE by illegally disposing of and otherwise handling wastewater in violation of permit limitations. B. MANNER AND MEANS OF THE CONSPIRACY The conspiracy to commit offenses against the United States and the laws thereof was, in substance, as follows: l I .. I I I I I I I I I I I I .. I I 1. As part of the conspiracy, from various clients industrial reprocessing and reclamation of oil. CHEROKEE would and did receive wastewaters for treatment, 2. It was further part of the conspiracy that KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER represented to the Charlotte Mecklenburg Utility Department that, in order to comply with the permit issued by the Charlotte Mecklenburg Utility Department, CHEROKEE was required to treat and filter the wastewater prior to discharging it into the local sanitary sewer. 3. It was further part of the conspiracy that, at the dir,2ction of and with the knowledge of KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, employees of CHEROKEE would and did accept volumes of industrial wastewater in excess of the capacity of CHEROKEE's filtration equipment and in excess of the storage capacity of CHEROKEE's storage tanks. 4. It was '4further part of the conspiracy that, at the direction of and with the knowledge of KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, er:iployees of CHEROKEE would and did dispose of industrial wastewaters directly into the sewer without adequate filtration or treatment. 5. It was further part of the conspiracy that KEITH N9RLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE Kldl.L GLAUSER would and did endeavor to conceal the fo,egoing disposal of these wastewaters by ordering employees not to conduct these activities while inspectors from local environmental agencies were present at CHEROKEE's Berryhill Road facility. c. OVERT ACTS In furtherance of the conspiracy and to effectuate the objects and purposes thereof, CHEROKEE RESOURCES, INC., KEITH NORLAND EIDSON', GENE WESLEY ("GABE") HARTSELL, THEODORE KARL GLAUSER and others, both known and unknown to the grand jury, did do and commit and cause to be done and committed, the following overt acts in the Western District of North Carolina on or about the times mentioned, during the conspiracy, to wit: 1. Throughout the course of the conspiracy, the exact dates unknown to the grand jury, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, routinely instructed and caused various CHEROKEE employees to directly dispose of the untreated wast,ewaters into the sewer by connecting a hose to wastewater holding tanks and wastewater tanker trucks and running untreated wastewater directly into the sewer through the employees' toilet • I le I I I I I I I ft I I I I I I It I I 2. ~hroughout the course of the conspiracy, the exact dates unknown to the grand jury, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, routinely instructed and caused various CHEROKEE employees to directly dispose of the untreated wastewaters into the se~er by opening a by-pass valve on the brine cell treatment tank which lead directly to the sewer. 3. On or about August 13, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Copper (182 ppm) and Biological Oxygen Demand (1,598 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 4. On or about August 14, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Copper (630 ppm) and Biological Oxygen Demand (17,688 ppm), inj;:o the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 5. On or about August 15, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Copper (123 ppm), Nickel (0.85 ppm), Oil & Grease (476 ppm) and Biological Oxygen Demand (3,120 ppm), in~o the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 6. On or about August 16, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Copper (92 ppm), Total Suspended Solids (526 ppm) and Biological Oxygen Demand ( 4, 53 O ppm) , into the sewer system flowing into the Charlotte Mecklenburg UtilityiDepart~ent Irwin Creek POTW. 7. On or about August 20, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge .and cause to be discharged wastewater containing pollutants, namely Copper (72 ppm) and Oil & Grease (598 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 8. On or about August 27, 1990, KEITH NORLAND EIDSON, GENE WESLEY {"GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.24 ppm), Copper (7.6 ppm), Zinc (4.1 ppm) and Biological Oxygen Demand {10,214 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. L ..• ,~;,.,. -,, 1 t: 'JP!;·i, ,~ .. ~ '~•-1.,, \.,.:"~i;d-~-~::1.;.;:-:r;;;f?'J,!j-A·' '.f:,;::. _-r ~;:..'.!1£;,_'., . .:..:.Lr.1 ~~.~It:.--,;, ~j1,:1'\-o1: r' ~ ,, ·. .ik :{.;t;; ~--.:~ .'f.: , ... :·::-.ri:..•.•!"'E1:ti:i~~·:f ~l,•~~-f:t2~'!: JiPS';'t/~(; Qi\~' ~~'t.rt,~·h~;:;f,0< ,?it-·,::~~~ 1' . I .. I I I I I I I I I I I I I .. I I 9. _ On or about August 28, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.46 ppm), Copper (3.4 ppm), Zinc (5.9 ppm), Oil & Grease (1,805 ppm) and Biological Oxygen Demand (9,913 ppm) into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 10. On or about August 29, 1990, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.42 ppm), Copper (0.29), Zinc (6.6 ppm), Oil & Grease (738 ppm) and Biological Oxygen Demand (8,983 ppm) into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 11. On or about February 11-12, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER' did knowingly discha~ge and cause to be discharged wastewater containing pollutants, namely Chromium (75 ppm), Copper (5.9 ppm), Lead (1.21 ppm), Nickel (1.21 ppm), Zinc (5.2 ppm), Oil & Grease (5,495 ppm), Tota·l Suspended Solids (836 ppm) and Biological Oxygen Demand (8,019 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 12. On or about February 12-13, 1991, KEITH NORLAND EJDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium ( O. 1 ppm) , Chromium ( 81 ppm) , Copper (10.5 ppm), Lead (3.22 ppm), Nickel (1.85 ppm), Zinc (10 ppm), Oil & Grease (1,900 ppm), Total Suspended Solids (1,933 ppm) ,and Biological Oxygen Demand (~1,802 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 13._ On or about February 13-14, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.8 ppm), Chromium (34.3 ppm), Cop~er (3.46 ppm), Lead (0.75 ppm), Nickel (1.29 ppm), Zinc (4.5 ppm), Oil & Grease (1,640 ppm) and Biological Oxygen Demand (9,559 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 14. On or about February 14-15, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge ~nd cause to be discharged wastewater containing pollutants, namely Chromium (11.7 ppm), Copper (0.79 ppm), Lead (0.57 ppm), Nickel (1.2 ppm), Zinc (4.6 ppm), Oil & Grease (1,559 ppm) and Biological Oxygen Demand (14,864 ppm) into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. . ' : ' I .. I I I I I I I ,. I I I I I I '-I I 15. On or about April 17, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.9 ppm), Chromium (20 ppm), Copper (6.5 ppm), Lead (2.4 ppm), Nickel (0.86 ppm) and Zinc 96.6 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 16. On or about April 18, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Chromium (0.49 ppm), Copper (0.46 ppm) and Zinc (0. 77 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 17. On or about April 2 9, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namelt Cadmium (0.2 ppm), Chromium (1.1 ppm), Copper (13 ppm), Lead (7 ppm), Nickel (J.1 ppm) and Zinc (23 ppm) into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 18. On or about April JO, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater cont~ining pollutants, namely Copper (0.58 ppm), Nickel (9.0 ppm) and Zinc ( J .1 ppm) , into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 19. On o::::-about May 1, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmipm (0.13 ppm), Chromium (0.23 ppm), Copper (J.J ppm), Lead (0.77 ppm), Nickel (17 ppm) and Zinc (6.4 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 20. On or about May 2, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Cadmium (0.75 ppm), Chromium (4.5 ppm), Copper (36 ppm), Lead (24 ppm), Nickel (18 ppm) and Zinc (430 ppm) into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 21. On or about May 3, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Chromium (0.26 ppm), Copper (1.6 ppm), Lead (0.6 ppm) and Zinc (9.8 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. I le I I I I I I I t' I I I I I I .. I I 22. On or about May 21, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Copper (0.7 ppm), Nickel (2.7 ppm), Zinc (12 ppm) and Biological Oxygen Demand (1,584 ppm) , into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 23. On or about May 22, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly disc~arge a~d cause to be discharged wastewater containing pollutants, namely Copper (0.3 ppm), Nickel (2.67 ppm) and Zinc (43 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 24. On or about May 23, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namel¥ Nickel (3.72 ppm) and Zinc (61 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 25. On or about May 24, 1991, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Nickel (4.39 ppm) and Zinc (76 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Cree~ POTW. 26. On or about July 15, 1991, KEITH NORLAND EIDSON did endeavor to conceal the illegal disposal of untreated wastewater by purchasing photographic negatives of the disposal from a CHEROKEE employee who had taken pictures depicting the insertion of a bypass hose into the employee's toilet for the purpose of discharging untreated wastes into the sewer. 27. On or about July 17, 1991, KEITH NORLAND EIDSON endeavored to conceal this illegal disposal of untreated wastewater by instructing a CHEROKEE employee to remove the oil stains surrounding the broken window that lead into the bathroom where the wastes were pumped down the toilet and into the sewer. 28. On or about July 18, 1991, KEITH NORLAND EIDSON endeavored to conceal evidence relating to the illegal discharges by directing the purchase of a one-way bus ticket from Charlotte, North Carolina to New York City, New York, and arranging for a CHEROKEE employee with incriminating information to be placed on that bus. 29. On or about February 4, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (8.J ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. I .. I I I I I I I I I I I I I JO. On or about March 25, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (5.7 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department In.in Creek POTW. 31. On or about March 26, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (15.8 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department In.in Creek POTW. 32. On or about March 27, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (18.5 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 33. On or about April 16, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (7. 7 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 34. On or about July 15, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Total Suspended Solids {TSS) (1,317 ppm), and Zinc (7.6 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. JS. On or about July 16, 1992, KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Oil and Grease (1,372 ppm), Lead (2.J ppm), and Zinc (11.4 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. 36. On or about September 16, 1992 KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER, did knowingly discharge and cause to be discharged wastewater containing pollutants, namely Zinc (4.1 ppm), into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW. In violation of Title 18, United States Code, Section 371 and Title 18, United States Code, Section 2. I [ l.: I .. . -. ' . , r: I .. I I I I I I I ,, I I I I I I I COUNTS TWO THROUGH SIX 1. The allegations contained in the Introduction Bill of Indictment are realleged and incorporated in this • of this Count by reference. 2. On or about the dates specified, within the Western District of North Carolina, defendants CHEROKEE RESOURCES, INC., KEITH NORLAND EIDSON, GENE WESLEY ("GABE") HARTSELL and THEODORE KARL GLAUSER did knowingly discharge and cause to be discharged wastewater containing the specified quantities of Cadmium, Chromium, Copper, Lead, Nickel, Zinc into the sewer system flowing into the Charlotte Mecklenburg Utility Department Irwin Creek POTW, in violation of the provisions of permit number 0202 and in violation of the National Pretreatment Standards: Count Date 4/29/91 Three 4/30/91 Four 5/1/91 Five 5/2/91 Six 5/3/91 Pollutant Cadmium Chromium Copper Lead Nickel Zinc Copper Nickel Zinc Cadmium Chromium Copper Lead Nickel Zinc Cadmium Chromium Copper Lead Nickel Zinc Chromium Copper Lead Zinc Permit Limitation (oprn) 0.07 0.20 0.27 0.53 0.84 0.70 0.27 0.84 0.70 0.07 0.20 0.27 0.53 0.84 0.70 0.07 0. 20 0.27 0.53 0.84 0.70 0.20 0.27 0.53 0.70 Level Sampled (oom) 0.2 1. 1 13.0 7.0 3. 1. 2 3 . 0 0.58 9.0 3. 1 0.13 0.23 3. 3 0.77 17. 0 6.4 0. 75 4 • 5 36.0 24.0 18. 0 430.0 0.26 1.6 0.6 9.8 I .. I I I I I I I ,, I I I I I I I In violation of Title 33, United States Code, Sections 1317(d) and 1319(c) (2) (A) and Title 18, United States Code, Section 2. COUNT SEVEN 1. The allegations contained in the Introduction of this Bill of Indictment are realleged and incorporated in this Count by reference. 2. On or about July 17, 1991, within the Western District of North Carolina, defendant CHEROKEE RESOURCES, INC., . THEODORE KARL GLAUSER and KEITH EIDSON did knowingly and willfully conceal and cover •..Jp by a trick, scheme and device and did make a false, fictitious and fraudulent statement of a material fact concerning a matter within the jurisdiction of the United States Environmental Protection Agency, in that THEODORE KARL GLAUSER signed a false name, "John Hardaway," on a hazardous waste manifest, thereby falsely certifying. personal knowledge of the information contained in the manifest, knowing the same to be false. In violation of Title 13, United States Code, Sections 1001 and 2. COUNT EIGHT 1. The allegations contained in the Introduction of this Bill of Indictment are realleged and incorporated in this Count by reference. 2. On or about January 27 ,-1993, within the Western District of North Carolina, defendants CHEROKEE RESOURCES, Il/C. and KEITH EIDSON did knowingly tamper with and render inaccurate and cause to be tampered with and rendered inaccurate a monitoring device required to be maintained under the Federal Water Pollution Control Act. In violation of Title 33, United States Code, Section 1319(c) (4) and Title 18, Un_ited States Code, Section 2. JERRY W. MILLER, UNITED STATES ATTORNEY NRAD, JR. Assistant nited States A TRUE BILL. -6;{~~ Foreperson , I I I le I I I I I I I .. I I I I I I .. I I Fr~~k G. Johns Clerk Terry T. Lettnor Chiel Deputy Ci<,rk UNITED STA TES DISTRICT COURT OFFICE OF nfE CLERK WESTERN 01sm1cn,F NORTH CAROLINA ROOM 204, CHARll:S R. JONAS FEDEl'lAL BUILDINO 401 WEST TRADE STRJ!ET CHARLOTT!!, NOl\l>t CAI\OUNA 20202 FAX TRANSMISSION COVER SHEET !=AX NUMBER (704)344-6703 DOCUMENT DESCRIPTION; _ --/2r' (Jr-It 1/s-(J;<?.rokt<' TOTAL NUMBER OF P~GEs/4_ COMMENTS: (excluding transmittal page) IF TH£RE ARE ANY PROSLJ{MS WITH Tf//S TRANSMISSION, PLEASE CALL(11U)34+6200, 100 \ 3111Jlcfd{) -1~no) 1)1~1s1a sn 9r;,,c:vc:0 ll04}J44-620:) FAX(704)34-1-6703 I Proceedings include Jvents between 6/20/94 and 2/12/96. I .,93cr186-ALL USA v. 'Cherokee, et al · MAG APPEAL CLOSED MAG APPEAL CLOSED . u.s. District court Western Dii:itrict of North Carolina (Charlotte) I I I I I CRIMINAL!DOCKET FOR CASE#: 93-CR-186-ALL USA v. Cherokee, et Jl Filed: OB/05/93 Dkt# in other court, !None 6/20/94 6/21/9,J 6/21/94 I 6/22/94 I 1• I r; /n I 94 I 6/24/94 I 6/?.7/94 I 6/28/94 I I lacket I I Jury trial as to Resources Inc. Cherokee, Keith Norland Bi.di:\on, Gene Wesley (Gabe) Hartsell held/continues w/ Govt' s evidence. (arg) [Entry date 07/11/94] Jury trial as to Resources Inc. Cherokee, Keith Norland Eid.ion, Gene Wesley (Gabe) Hartsell held/continues w/Govt'a evitjence. (srg) [Entry date 07/11/94] Jury trial as to Resou.rces Inc. Cherokee, Keith Norland Eid~on, Gene Wesley (Gabe) Hartsell held/continues w/Govt's evidence. (erg) [Entry date 07 /11/94] ,Jury trial as to Resources Inc. Cherokee, Keith Norland Eid~on, Gene Wesley (Gabe) Hartsell held/continues w/Govt's ,,vidence. At the concl1.1sion of Govt' s evidenoe, Def ts made the !following MOTIONS; 1) to DISMISS, 2) to STRIKE testimony of Mr. Cornelius, 3) to DISMISS and 4) for JUDGMENT OF ACQ. MOTIONS DENIED. DENIED. (srg) (Entry date 07/11/94] ! ,Jurj} trial as to Resources P.id~on, Gene Wesley (Gabe) prodeed to offer evidence. Inc. Cherokee, Keith Norland Hartsell held/continues. Defts (arg) [Entry date 07/11/94] Jury trial as to Resources Inc. Cherokee, Keith Norland Eid~on, Gene Wesley (Gabe) Hartsell held/continues w/Oefts' evidence. (srg) (Entry date 07 /11/94] i ,Jury trial as to Resources Inc. Cherokee, Keith Norland Eid~on, Gene Wesley (Gabe) Hartsell held/continues w/Defts' evidence. (See Defts' proffered evidence, Exhibit #BB, vid~o tapes.) (erg) [Entry date 07 /11/94] 1 Jury trial as to Resources !nc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell held/continues w/Defts' evidence. (See· Defts1 offer of proof ae recorded in the recdrd.) Defta rest. GOVT'S REBUTTAL EVIDENCE -The Govt prodeeds tq .. offer rebuttal testimony. At the conclusion of rebctttal evidence, the Govt rest. Defts renew Rule ~9 Mot~on, Motion to Dismiss. MOTIONS DENIED. Final Arg\\ments. (erg) [Entry date 07 /11/94] as of Februar~ 12, 1996 3:34 pm Page 1 ! C:00 3ll0l~~HJ -lclflOJ lJl~lSIC sn I I I Proceedings include events between 6/20/94 a~d 2/12/96. • : 93cr186-ALL USA v. ! .. Cherokee, et al · CLOSED MAG APPEAL I I I I I I 6/29/94 Jury trial as to Reaources Inc. Cherokee, Keith Norland Eid$on, G1mA Wesley (Gabe) Hartsell held/continU$8 w/the Judge's CHARGE. The Jury retires to deliberate at 10:15 a. m. and returns to open Court w/VERDICTS of GUILTY as to all Defts at 11,29 a. m. (Defts to remain on bond and was ordJred not to contact any of the wits. Sentencing def~rred to Oct. term.) Deft.#1, Guilty as to Cto 1-6, & 6/29/94 260 7 /11/94 8 .. Deft #2, Guilty as t.o Cts 1-6, & 8. Deft #3, Guilty as to Cts 1-6. (erg) [Entry date 07/11/94] JURY VERDICT ai, to Resources Inc. Cherokee, Keith Norland Eidson, Gene WeAley (Gabe) Hartsell Guilty: Resources Inc. Cheiokee (1) count(s) 1, 2-6, 8, Keith Norland Eidson (2) courit(s) 1, 2-6, A, Gene Wesley (Gabe) Hartsell (3) count (s) 1, 2-6 (srg) [Entry date 07/11/94) 8entlencing set for 9, 30 9/19/94 for Rssout·ces Inc. Cher;oke"', for. Keith Norland Eidson, for Gene Wesley (Gabe) Harr.sell , Resources Inc. Cherokee (1) count(s) 1, 2·6, a, Keir,h Norland Eidson (2) count(s) 1, 2-6, B, Gene Wesley (Gabe) Hartsell (3) count(s) l, 2-6 (srg) [Entry date 07/11/94] I 7/21/94 C.,TI'. i~o as to Theodore Karl Glauser Authorization to Pay H, M. Whit:esl.des $ 16,604.58 Voucher# 0678181] ( Signed by Judge Robert D. Potter) (mga) [Entry date 07/21/94] .. /31/9'1 262 I 8/31/94 263 I I 9/12/94 I 10/11/94 264 I 10/11/94 265 I .. ocket I as of I E00 CJA:21 as to Keith Norland Eidson Authorization to Pay Krisi '.l'ursl'!hm:ld $ 1,423.03 for Expert Services Voucher ff 016i140 ( Signed by Judge Robert D. Potter) (mga) [Entry date 09/01/94] C,TA :21 as to Theodore Karl Glauser Authorization to Pay Kri~ '.C'urschm.id $ 2,225.86 for Expert services Voucher ii 016~140 ( Signed by Judge Robert D. Potter) (mga) (Entry date 09/01/94) Deadline updated as to Resources Inc. Cherokee, Keith Nor~and Eidson, Gene Wesley (Gabe) Hartsell, set Sentencing for 4:00 9/21/94 for Resources Inc. Cherokee, for :Keith Norland Eidson, for Gene Wesley (Gabe) Ha:>:'tsell (ssh) [Entry date 09/12/94] MOTiON by Keith Norland Eidson, Gene Wesley (Gabe) Hartsell to Continue Sentencing Hearing (mga) [Entry date 10/12/94] MOTJ.jON by Ke:i.th Norland Eidson, Gene Wesley (Gabe) Hartsell £or ;New Trial (mga) [Entry date 10/12/94] 12, 1996 3:34 pm Page 2 i 1 I MAG I Prnce,ed\.11gs i.nclude ~vents between 6/20/94 and 2/12/96. .,93crl86-ALL USA v. [Cherokee, et al . , CLOSED l\l?PEAL I I I I I I I 10/11/94 --ORA~, ORDER ae to Keith Norland Eidson, Gene Wesley (Gabe) Hartsell denying [265-1) motion for New Trial as to Keith Noriand E:\.dson (2), Gene Wesley (Gabe) Hartsell (3), denying (264-1) mot.ion to Continue as to Keith Norland Eidson (2), Gene WARley (Gabe) Hartsell (3) ( Entered by Judge Robe.rt n. !?otter ) (mga) [Ent:t"y date 10/12/94] 10/11/94 -- 10/17./94 :16(i 10/17/94 267 10/17/94 ?68 S1>ntencing held Resources Inc. Cherokee (1) count(s) 1, 2-6; 8, Kej.th Norland Eidson (2) count(s) 1, 2-6, $1 Gene Wes:j.ey (Gabe) Har.taell (3) count(s) 1, 2-6 (srg) (Entry date 10/14/94] ' NOT+CE OF APPEAL by Gene Wesley (Gabe) Hartsell (3) cou,:it(s) 1, 2-6 cc: Counsel, USM and USPO (mga) [En~ry date 10/18/94] JUOOMF.NT Reaources Inc. Cherokee (1) count(s) 1, 2 -6 1 B . FOOii-(4) YEARS PROBATION, $50,000 FINE and $1,100 ASS~SSMENT ( Signed by Judge Robert D. Potter) ( Crim Judge Vol: 43 Page, 65) (mga) [Bntry date 10/18/9<1] ,JUDGMENT Keith Norland Eidson (2) ccunt(g) 1, 2 -6 , 8 FIFTY ONE (51) MONTHS IMPRISONMENT each count to run conqurrently, THREE (3) YEARS SUPERVISED RELEASE, $5,000 FINE and $350 ASSESSMENT ( Si.gned by Judge Robert D. Potter J c·crim Judge Vol: 46 Page: 66) (mga) [Entry date 10/18/94] .. 0/17/94 269 ; ,TITDqMF.N'l' Gene. Wesley (Gabe) Hartsell (3) count (s) 1. FIFTY ONE j (51) MONTHS IMPRT.SONMENT, THREE (3) YEARS SUPERVISED RELEASE each ct. to run ccnc\1rrently, $10,000 FINE on all cour)ts and $50 ASSESSMENT , Gene ~lesley (Gabe) Hartsell (3) count(s) 2-6. THIRTY SIX (36) MONTHS IMPRISONMENT ea ct to run'concurrently with ct. 1, THREE (3) YEARS SUPERVISED RELEASE each ct. to run concurrently, $10,000 FINE on all counts and $250 ASSESSMENT ( Signed by Judge Robert D. Pottier ) ( Crim Judge Vol: 46 Page: 67) (mga) I I I 10/111/94 :170 I 10/18/94 271 I 10/18/94 272 I 10/19/94 273 .. Docket as of I I 1'00 [En~ry date 10/18/94] MOTION by Keith Norland Eidson for Payment of Expert Fees (mg<'i) [Entry date 10/18/94] CJA:20 as to Gene Wesley (Gabe) Hartsell Authorization to P.ay:TN'l'BRIM PAYMENT Edward A. Fiorella$ 11,448.01 Voucher ff 0~19430 ( Signed by Judge Robert D. Potter) (cat) [Entjry date 10/18/94) C,TA \:lO as t:o··Ge.ne Wesley (Gabe) Hartsell : Appointment of Atttjrney Edward A. Florella (Fiorella has been paid interim paYD1ent, .so new/final voucher prepared), Voucher # 0619430 (catj) [Entry date 10/18/94) NOTiCE OF APPEi\!, by Keith Norland Eidson (2) count (s) 1 1 2-6,! 8 cc, Counsel, USM and USPO (mga) [Entjry date 10/19/94] i Februax,f 12, 1996 3:34 pm Paga 3 I i i' ' I I.Proceedings include ~vents between 6/20/94 arid 2/12/96. 3:93cr186-ALL USA v. 'Cherokee, et al : . ' MAO APPEAL I I I I I I 10/19/94 274 10/19/94 -- lO/::n/94 ?.75 10/21/94 -- 10/25/94 ?.76 lO/n/94 ?.77 I 10/n/94 fl10/~7/94 279 I I I I I I 10/27/94 280 10/27/94 281 10/27/94 10/27 /94 - - 10/31/94 -- CLOSED MOTtON by Keith Norland Eidson to be Released on Bond Pending Appeal from a Judgment of Conviction (mga) [Entry date 10/19/94] Notice of appeal and certified copy of docket as to Keith Norland Eidson, Gene Wesley (Gabe) Hartsell to USCA: (273-1] appeal, [266-1] appeal (mga) !Entry date 10/19/94] NOTICE OF APPEAL by Resources Inc. Cherokee (1) count(s) 1, 2-6; B cc: Counsel, USM c.nd USPO (mga) [Entry date 10/24/94] Notice of apps,il and certified copy of docket as to Resources Inc. Cherokee to USCA, [275-1] appeal (mga) [En~ry date 10/24/94] ORDER as to Keith Norland Eidson granting [270-1] motion as t.o Rel.th Norland Eidson (2) ( Signed by Judge Robert D. Potter ) (mga) [Entry date 10/26/94] PRESENTENCE INVESTIGATION R.E:POR'I' (Sealed) .is to Keith Norland Eidson (mga) [Entry date 10/27/91] PRRSRNTENCE INVESTIGATION REPORT (Sealed) as to Gene Wesley (Gabe) Hartsell (mga) [Entry date 10/27/94] PRESENTENCE INVESTIGATION RF.PORT (Sealed) as to Resources Inc.' Cherokee (mga) (Entry date 10/27/94] MOT±ON by Gene Wesley (Gabe) Hartsell to be Released Pendi.ng Appeal from Judgment on Bond (mga) [En~ry date 10/31/94] RES~ONSE by USA"" t.o Kei.thNorland Eidson, Gene Wesley (Gabe) Hartsell in opposition to (280-1] motion to be RelE>ased Pending Appeal from Judgment on Bond, [274··1) motion to be Released on Bond (mga) [Entry date 10/31/94] USC11-Case Number as to Gene Wesley (Gabe) Hartsell Re: (266-1) appeal USCA Number: 94-5796 (mga) [Entjry date 10/31/94] 1l.'1CA Case Number as to Keith Norland Eidson Ra: (273-1] app.ial. USCA Number: 94-5797 consolidated w/94-5796 (mga) (En~~y date 1_0/31/94] / USCA Case Number as to Resources Inc. Cherokee Re: [275-1] app.ial USCA Number: 94-5804 consolidated w/94-5796 (mga) [Entry date 10/31/94] .. Docket as of February 12, 1996 3:34 pm Page 4 I I 500 3110l~tl-lJ -l~nro lJI~lSIO sn ! ,. ', i ' 'i I \ ! I MAG APPO:AL I Proceedings include ~vents between 6/20/94 and 2/12/96. • . 93crl86-ALL USA v.!Cherokee, et al CLOSED I I I I I I 11/1/94 282 ORDER as to Gene Wesley (Gabe) Hartsell denying (280-1] motion to be Released PendJ.ng Appeal from Judgment on Bond as to Gene Wesley (Gabe) Hartsell (3) ( Signed by Judge Rob'!'rt D. Potter ) (mga) (Entry date 11/01/94] 11/2/94 283 11/4/94 284 11/8/94 285 11/22/94 286 MEM()RJI.Nnl.JM by Gene Wesley (Gabe) Hartsell in support of their Motion for Release Pending Appeal (mga) [En~ry date 11/03/94] MOTION by Keith Norland Eidson and Gene Wesley (Gabe) Hartsell for Reconsideration of [282-1) order (mga) (En~ry date 11/04/94] ORD~R as to Keith Norland Eidson, Gene Wesley (Gabe) Har~sell denying [284-1] motion for Reconsideration of (282-1] order as to Gene Wesley (Gabe) Hartsell (3), denying (274-1] motion to be Released on Bond as to Keith Norland Eidson (2) ( Signed by Judge Roberto. Potter) (mga) (Entry date 11/09/94] MOT!ON by Theodore. K;n.-1 Glauser for Payment of Expert Fees (mga) (Entry date 11/22/94] 112/9/91 TRANSCRIPT Trial f.-i.1.ed as to Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell for dates of 6/16/94 thru 6/27/94 Re, [275-1] appeal, [273-1] appeal, [266-1] appeal (mga) [Entry date 12/12/94] I [Edit date 12/12/94] TRANSCR1PT Sentencing filed as to Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell for date of i0/1.2/94 Re, (275-1) appeal, (273-1) appeal, (266-1] app~al (mga) (Entry date 12/12/94] [Edit date 12/12/94] I 12/19/94 287 Judgment Returned Executed as to Keith Norland Eidson on ll/~9/94 (mga) [Entry date 12/19/94] I I I 1/19/95 .. cket I I ,Judgment Returned Executed as to Gene Wesley (Gabe) Har.tisell ; on 11/30/94 (mga) (Entry date 12/19/94) C,Tll. .20 a,; to Ke.1.th Norland Eidson Authorization to Pay Dale Morrison$ 12,464.05 Voucher# 0619435 ( Signed by Judqe Robert D. Potter) (mga) (Entry date Ol/04/95] 290 C,TA :21 as to Resourc,;,s Inc. Cherokee, Ke:i.th Norland Eidson, Gen,j Wesley (Gabe.) Hart!'lell Authorization to Pay Kris H. Turschmid $ 940.00 for Expert Services Voucher# 0161152 Sigr\ed by Judge Robert D. Potter) (mga) [Entry date 01/04/95] i •• ! 291 ORD~R as to Resources Inc. Cherokee, Keith Norland Eidson, GAna WAAlAy (Gabe) Hartsell, Theodore Karl Glauser grantins [286-1) motion as to Theodore Karl Glauser (4) ( Signed by Jud~e Robert 0. Potter) (mga) [Entry date 01/19/515) as of Februar)f 12, 1996 3134 pm Page 5 ' 900 3110lci1:jH) -l~n□) l)l~lSJa sn i ! i I ' , :. i ; , , I Proceedings include ~vents between 6/20/94 .,93cr186-ALL USA v.,Cherokee, et al and 2/12/96. MAG APPSAL CLOSED I 1/19/95 I 3/22/95 I I I 4/7/95 I I S/S/9:i ~/15/95 I 2'/2/96 I I I I I .. Docket I I 292 293 294 296 C,TA: 21 as to Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell, Theodore Karl Glauser , App9i.ntment of Kris H. Turschmid as Expert. Voucher II 0161-162 ( Signed by Judge Rebert D. Potter ) (mga) [En~ry date 01/19/951 ORDtR re, payment of expert services provided by Steve Hartness of Acumen Investigative Rvc as to Keith Norland Eidson, Gene Wesley (Gabe) Hartsell, Theodore Karl Glauser, Voucher #0161138 dated 11./5/93 f.or Dft. Glauser is null&. void, Voucher. #0161139 dated 11/23/93 for Dft. Hartsell is null r. void, Voucher #645155 dated 4/4/94 for Dft Eidaon is null & void, Voucher #0161158 dated 11/2/93 for Dft:Glauser .ls APP.ROVED as amended and forwarded to Cirduit Judge subject to final approval ( Signed by Judge Robert O. ~otter ) (bsw) [Entry date 03/23/95) CJA.21 as to Resources Inc. Cherokee Authorization to Pay Kris TUrschmid $ 4,045.00 for Expert Services Voucher if 0161162 ( Signed by Judge Robert D. Potter ) (jll<:) (Entry date 04/10/95] CJA:?.1 as to Theodore Karl Glauser Authorization to Pay s~.eye Hartness $ 4104. 64 for Expert Services Voucher ii 0161-1.58 ( S:i.gned by Judge Robert D. Potter and Judge Sam Ervin, III) (jlk) (Entry date 05/05/95] 'l'rar:,smi.l:.t.ed Clerk's Certificate to USCA certifying record is complete re: (275-1] appeal by Resources Inc. Cherokee, [273-11 appeal by Keith Norland Eidson, [266-1) appeal by Gems Wesley (Gabe.) Hartsell (chh) [Entry date 05/18/95] MOTlON by Resources Inc. Cherokee, Keith Norland Eidson, Gen~ Wesley (Gabe) Hartsell for New Trial (jlk) [Entry date 02/02/96) as of February 12, 1996 3:34 pm i Page 6 l00 31101~11;:-:J -1~nm Dr ~is ia sn 96/c'.Vc'.0 ' I ,. I I I I I I I ,. I I I I I I '-I I Memo Date: December 22, 1995 To: File From: Douglas Moore 4 f?>-lu~ Environmental Chemist Re: NC Superfund Section Follow-Up On-Site Reconnaissance Cherokee Oil Company Site 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCD 980 799 019 On Wednesday, December 20, 1995, Doug Moore of the NC Superfund Section travelled to the subject site to conduct a follow-up on-site reconnaissance. At 10:45, I arrived at the subject site and met with EPA federal on-scene coordinator Steve Spurlin. Mr. Spurlin provided copies of analytical results from soil samples collected by EPA during the removal action. He also presented a discussion of the analytical results in relation to EPA's removal action. At 11:00, Jarrell Wootan of Mecklenburg County Department of Environmental Protection (MCDEP) arrived at the site. Mr. Spurlin provided a sampling grid map esrablished for the drum staging area located northwest of the site across Berryhill Road and analytical results that correspond to sample points as outlined on the map. The sampling map and analytical results are attached to the back of this memo. Mr. Spurlin indicated that Grids #1 and #2 correspond to the main staging areas for drums removed from the subject site. Grids #3 and #4 represent areas where materials removed from the drums were handled and transferred to appropriate shipping containers prior to removal off-site to RCRA facilities. The analytical results exhibit residual levels of BETX (benzene, ethylbenzene, toluene, and xylene), chlorinated solvents and polynuclear aromatic hydrocarbons (PAH) in soil samples removed from these locations. Mr. Spurlin believes the PAH's identified in the soil samples originated from a layer of coal that was encountered under the staging area when EPA scraped the surface of the site. He stated that the BETX and chlorinated solvents may have resulted from leaking drums that were staged on the property. He stated that EPA scraped surface soils from this location and removed visibly contaminated soils from the staging area. He indicated that the levels found in the 1 I .. I I I I I I I ft I I I I I I .. I I subsurface soils were well below regulatory levels for a removal action. EPA then brought in clean backfill, applied a surface layer of clean soil to the drum staging area, and reseeded the area. Mr. Spurlin stated that EPA removed three underground storage tanks (UST) from a refueling island located at the southwest corner of the site. In the process, EPA excavated approximately 100 cubic yards of soil from around and under the UST's and stockpiled on the site. A soil sample (CO-WS-28) collected from the bottom of the excavation at UST #8 exhibited elevated concentrations of BETX compounds, tetrachloroethene and two different phthalates in a tight red clay. Mr. Spurlin stated that the levels found at the base of the excavation pit were below EPA regulatory concerns for a removal action and that EPA backfilled the excavation with clean soil. A soil sample (CO-WS-38) collected from the stockpile exhibited elevated concentrations of ketones, BETX compounds, methylnaphthalene and several phthalates. Mr. Spurlin indicated that the levels of contaminants found in the soils were below EPA regulatory levels for a removal action. He stated that EPA plans to use the stockpile to regrade the site to route the surface drainage towards the southeast corner of the site. At 11:20, Jarrell Wootan, Steve Spurlin and Doug Moore toured the site. The site is surrounded by a chain link fence topped with concertina wire. A former gap in the fence at the southwest corner of the site has been fenced with a gate. There were several piles of soil visible over the surface of the site: some with plastic tarpaulines, some uncovered. In the center of the site is a rectangular warehouse. A muddy, open lot is located between the warehouse and Berryhill Road. I took a panoramic photograph of the site from the northwest corner entrance to the site. We walked across the open lot to a soil pile covered by a plastic tarpauline, located near the southwest corner of the site at the approximate location of the former refueling island. Steve Spurlin stated that this was the area where the UST's were located. A large front end loader was observed putting soil into a roll-off container at this location. Mr. Spurlin stated that this is the soil stockpile that corresponds to soil sample CO-WS-38. Mr. Spurlin said EPA removed three large, approximately 20,000 gallon underground storage tanks from this location. There was a 1-1.5 foot thick concrete pad and two concrete pyrimad shaped structures covering the UST's. The pyramid shaped structures had several uncapped fill pipes running into the ground. EPA demolished the concrete structures and pad in order to get to the UST's. Underneath the pad, they encountered a layer of oil saturated gravel that was approximately 1 foot thick. EPA removed the oily waste from the excavation, stockpiled, manifested and shipped it off-site. A red clay layer was encountered below the gravel. Mr. Spurlin stated that the UST's were aligned side by side in a direction parallel to Berryhill Road (see figure in field notes). EPA labeled the three USTs #7, #8 and #9 m 2 I .. I I I I I I I ,, I I I I I I .. I I order of location descending from furthest away to nearest Berryhill Road. Mr. Spurlin also stated that the oily layer was heaviest near UST #7 and believes that the material may have originated from leaky distribution pipes that connected to a loading platform located southeast of the UST's. He also indicated that a terracotta pipe was encountered at this location, which he thinks may be associated with a former sewer system drain field. He suggested that the oily material may also have come from the terra cotta pipe. The depth to the base of the excavation was approximately 14 feet. The soil from the excavation was stockpiled on site, sampled by EPA, and covered with a plastic tarpauline. EPA also collected a soil sample from the base of the excavation under UST #8. Later, EPA backfilled the excavation with clean soil. The materials contained inside the UST's were pumped out, manifested and shipped off-site lo RCRA disposal facilities. The UST's were cut into pieces and removed from the site. Mr. Spurlin indicated that the liST's contained waste oil and sludge. EPA plans to reuse the stockpiled soils from the UST excavation to regrade the overland drainage towards the southeast corner of the site. During the August 1995 on-site reconnaissance, an elevated concrete and wood loading platform was observed at the south end of the warehouse. The platform was covered by a tin roof and housed two large, steel-plated, square vats. At the east side of the loading platform there were 6 large, approx. 20,000 gallon above-ground storage tanks (AST). Under the AST's was a containment wall composed of cinderblocks, labeled "containment area #2" by EPA. Another cinderblock wall was located at the south end of the loading platform that was built to serve as a containment basin. This was labeled "containment area #I" by EPA. During the December 1995 on-site reconnaissance, the elevated platform and associated steel plated vats, the 6 above-ground storage tanks and containment areas #I and #2 have been demolished. One large stockpile of contaminated soil covered with a plastic tarpauline, one stockpile of clean soil (uncovered) and one large stockpile of broken concrete pieces (uncovered) was observed in the former location of these prior features. Mr. Spurlin stated that EPA plans to remove the stockpile of contaminated soil and use the stockpile of clean soil to grade the site. EPA plans to leave the concrete pile in place. I took a panoramic photo of the site from the southeast corner of the site showing the condition of the site and the general surface slope. We inspected containment area #3, located at the northeast corner of the warehouse. The containment area cinderblock wall was intact. There was residual stained soil in the crawl space under the warehouse and at the northeast corner of the warehouse within containment area #3. Mr. Spurlin indicated that EPA did not plan to remove any soil from this area, because the levels were not above EPA regulatory levels and because it would require EPA to demolish the warehouse in order to get to it. The northeast corner was heavily vegetated and impassable. Mr. Spurlin stated that there are two empty square cinderblock impoundments located in this area and a small diameter plastic pipe leading from the warehouse to the impoundments. Mr. Spurlin did not know where the pipe 3 I .. I I I I I I I ~ I I I I I I .. I I originated within the warehouse nor it's purpose. I took several photos of the containment area. We inspected the warehouse. There was a open roll-off container outside at the south end of the warehouse that was filled approx. halfway with metal debris. Mr. Spurlin stated that the roll-off was present on the site prior to the removal and that EPA was using it to store metal debris that could be salvaged. We inspected the inside of the warehouse. There were two large, empty, cylindrical tanks at the south end inside the warehouse. Mr. Spurlin said that these tanks were part of Cherokees wastewater treatment system. EPA· removed oily liquids and sludges from inside these tanks. There was also a device that appeared to be stacked tubes. There were roughly 5 or 10 tubes, each about 3-5 inches in diameter, roughly 10-12 feet long on each rack and stacked several racks high. The ends of the tubes had a tapered fitting with a small 0.5 inch diameter plastic tube connecting the larger tubes together, end to end fashion. Mr. Spurlin said this was some sort of filtration system. I _took a panoramic photo of the south end of the warehouse. There were numerous old desks, chairs, and furniture scattered along the east wall of the warehouse. There was a mens bathroom on the west wall. I observed a room through a open door at the north end of the warehouse that had a desk and chair and appeared to be a office. I did not see where the plastic pipe entered the warehouse from the previously mentioned impoundments at containment area #3. We walked outside the warehouse to the northwest entrance to the site. I walked down Berryhill Road to the southwest corner of the site. I took a panoramic photo of the site from Berryhill Road showing the new fence and gate and the south end of the warehouse. At 12: 10, we walked back to the command trailer at Drum Street and discussed the bulk analytical group data from the remova_l action. Mr. Spurlin pointed out that the majority of contaminants found at the site were BETX and chlorinated solvents. He stated that although PCB's were identified within the two vats located at the former loading platform, no levels were found above the Toxic Substances Control Act regulatory level of 5.0 ppm. Thus, they did not ship any bulk groups as PCB solids or PCB liquids from the site. I told Mr. Spurlin that our survey indicated that there were limited receptors that would be affected by a release from the site. As a resuit, only highly toxic, highly bioaccumulative and persistent contaminants would be capable of causing the site to score greater than 28.5 on the Hazard Ranking System and asked him if any of these contaminants were identified. Mr. Spurlin thought that some of the PCB data and PAH data may be useful. He agreed to review the results and provide copies of bulk group analytical results generated by EPA during the removal action to the NC Superfund Section. I gave Mr. Spurlin my current business address. At 12:40, Jarrell Wootan and Doug Moore departed the site. At 12:45, I broke for lunch. I arrived back at Raleigh at 16:30 . 4 ~-\_-Aitlt:~:~ LABORATORIES, INC. CHAl,,r CUSTODY • 11176 DOWNS ROAD 704/588-5076 PINEVlkLE,NC2e134 FAX704i58&-2454 Phone Number: 170~ l >9)-01]7 Cliern: OH!v') (ot{), Fax Number: (7D'I) ~-l9--'l-'-_-)-'--)-"'':/-']-'-------- Address: Poo DL . .,. C,f: Purchase Order Number: IO\ 001>';- Ctty {I,.,/ JJ" · State·/)/. Zrp J~ :OJ, _,_,~~~------ oJJ J 7 ~~---~~=------Certification Requirement: -~--------~- Contact Person IJ 01 K kJp4,i; ProJect Name .b_hc~C~c~K-o:~_O~,~) ________ _ Sampled By: J' t'} b anl Rush crarges Authorized p zes ~ No I / di (Jo'{ TAT ffq..,,'-,\(' By relinqLJ1shmg ttus sample(s) ro laboratory Personnel, I warrant that I am aulhonzed ro enter into rh1s agreement fOf the Cl~nl named abow and that I aulhonie 1hejt>elow a/la'!ysis subttef to d-ie f rms and cond1t1011S on the reV&<se Mre-11 This agreement 1s gover by lhe terms d cond1Dons on the reverse side hereol. Analysis charges sha/J be as included ,n the laboralones fee sctiedule in effect a1 the lime of the analysis. Reli°'.luished ~Yi1,4;:.c,,~.,_f"-'' ,.,·=""'-f-':,-'--,""',.""'-•--c-, ~-~-·""r),--__ --__________ _ Date: _/_0_-_;_l(~-9~\'--______ _ Time: --'-'I b'"--'O'-'V'-\---Received By:...;;.'___,_< '"'-'-'--+-'--'-~--"---'--'---'1 /'-_ cc(·c.;· !"-.\:...,.,-"'------------Date: /{' -/ '/ >-T. L \ ,me: ~/f _______ _ Relinquished By: _______________________ _ Date: ____________ _ Time: _______ _ Received By: ____ ~-------------------- Date: ____________ _ Time: _______ _ I!! Ji ,, Dale & Time . Sampi&ID Sampled Lab ID l0-\.,/5:_ l ~ !)i Jo-~ '1-1,; IIID A._ T,,. l~:)j-f )i, j ·t. a,e,, f'.>r{ ~J, i '1["\-L_,,f{aie . \ /o-{•/-'J, {.f)-'vJs-) 7 X X t 11 lh TA~ t .tls-t ,t ,-. p I'll 1"/1\ ""~' ., ,c \· ,--'J 5 C"·" .---,--,( _, AW!!llll tlllll~c Sampler Location Date Installed Time Installed Flow Date Picked Up Time Picked Up Flow Composite Type: □Flow □Time □Hand ------- ~ -1--~ 88~.fJ!Jfi/Jii!t1JJJ,&!t Samples received on ice? Yes □ No[] Q) (J .... ... ,., Q.. ..... (.) _, ~ ......:.1 :z: :z: .:i--.ra(J oo JE:I!:.t CF/GPO -- Field pH Result ____ _ Analyst Time/Da~te~------ -/QC-1rn1;__ . Other Analysis Presef"VatNe To~.l Vo/,,t/" -MJkc,) '1)'/D ',./.,~ IL/O} 101 .\ f..,_, \,,/J 1 -111,1ho./ q,$v ~ ~'i'Oe ci,-Rc~ti ,..,.tJ, ,{ r~t0 . T,L I V o/,J-/c 'i -)vi,,/ IM1/'\J Vo,! l½Orx T,,JJ <-: \/cl.JL-~1.-/1,,,.i'l~'2 { ~)0!/1 ~\. Re' /\A "' J,lc. ) /)l >o I t.t\ 4 .,1+ Bi'II ~IV L/4,00 Please sign and return the white and yellow copies to the Laboratory. ---- - - - - I I ' I I I I I I I I I I I I I I IJ I I NOV 28 •~ 1:5:02 TO 3911147 !lami Enyironm,,,tal Coamftaat•, Inc FROM AquaChem Envir. Lab OEC Certificate of Analysis T-71::i P.02 ' Client: OHM Col))Oration 2401 Tuckascegee Road Charloue, NC North Carolina Certification Number: 305 South Carolina Certification Number: 99032 Client#: Contact: Sample Date: SDG#: 381 Jack Kilbarger 24-0ct-95 SDG--000285 Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By: Lab Sample ID:LS!D--001095 Kenneth R Richardson Sample ID: CO-WS-16 Parameter Cadmium Chromium Lead Sliver Me=ry Selenium Project Mauger Reponlng Rerult Limit Unit Method Time 1.50 0.25 ppm EPA6010 23;!7 8.25 1.25 ppm EPA 6010 23:17 G.50 1.25 ppm EPA 6010 23:17 u 0.25 ppm EPA 6010 23:17 0.010 0.003 ppm EPA 7470 15:35 u 0.125 ppm EPA 7740 10:10 11116Dowlll Roo,1. Plaovllle, ~c 2113~ Pl,..,., (71M) Sfi&-~•m -FAX,('?~) Sla.1454 Page I Date 10/30/95 10/30/95 10/30/95 10/30/95 10/27/95 10127/95 AnaJy.u RCD RCD RCD RCD DRW RCD • • • I I I I I I I I I I I I I I I I I Qm.nJ. Environmental '1 Consultants. Inc Certificate of Analysis Client: Client#: Con!Jlct: Sample Date: SDG#: OHM Corporation 240 I Tuckaseegee Road Charloue, NC 381 Jack Kilbarger 24-0ct-95 SDO-000285 Lab Sample ID:LSID-001096 Sample ID: CO-WS-16 Parameter Result 1, I, I-Trichloroethane u 1,1,1-Trichlorocthane L' I, 1,2,2-Tctrachlorocthanc u I, 1,2,2-Tetrachloroethane u l. 1,2-Trichloroethane u I, 1.2-Trichloroelhane u I, 1-Dichlorocthane u I, 1-Dichloroethane u 1, 1-Dichlomethcnc u l, 1-Dichloroetlu:ne u 1,2-Dichlorobc=c u 1,2-Dich!oroben= u 1,2-DichJ orocthane u 1,2-Dichlorocthane u 1,2-Dichloroetlu:ne u 1,2-Dichloropropane u 1,2-DichJoropropane u 1,3-Dichlorobcnzcne u 1,3-Dichlorobcnzene u I, 4-Dichlorobcnzene u I, 4-Dichlorolx:azne u Reporting Limit Unit 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 3 I ppb 3] ppb 3 l ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb North Carolina Certificatlon Number: 305 South Carolina Certification Number: 99032 Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By: Kenneth R Richardson Project Manager Method Time Date EPA 8240 11/2195 EPA8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/219.l EPA 8240 11/2/95 EPA 8240 11/2195 EPA 8240 1112195 EPA8240 ll/2/95 EPA 8240 11/2195 EPA8240 11/2195 EPA 8240 1112195 EPA 8240 IJ/2195 EPA 8240 11/2/95 EPA 8240 11/2195 EPA 8240 l l/2/95 EPA 8240 l l/2/95 EPA 8240 11/2/95 EPA 8240 11/2!95 EPA 8240 1112/95 EPA 8240 1112195 EPA 8240 1112195 Analyst 1117' I>nma Ro.d -Ptn.eville. NC l8134 Phon.•1 (70-C) ~ro76 -F.UC: (7M) 5U-l"'64 Page 2 • • • r~un H',Uo1...n~m t:.nv,r. Lab T-715 P.04 I QmnJ. Enrlronmental 0 I C.rJ.aSJJ.ltarw, la~ E C preJ. ,",nlflq() • I Certificate of Analysis I Client: OHM Corporation North Carolina Certification Number: 30S 240 I Tuckaseegee Road South Carolina Certlflcatloo Number: 99032 I Charlotte. NC Qient Ir. 381 Rer.eipt Date: 24-0ct-95 I Contact: Jack Kilbarger Report Date: 28-Nov-95 I Sample Date: 24-0ct-95 SDG#: SDG-000285 Approved By: Lab Smmplc ID:LS!D--001096 Kenneth R. Richardson I Sample ID: CO-WS-16 Project Manager Reportin~ I Parameter Result Limit Unit Method Time Date Analyst 2-Butanone 57BJ 62 ppb EPA 8240 11/2/95 2-Butanone 57BJ 62 ppb EPA 8240 11/2/95 • I 2-Chloroethcylvinylether u 120 ppb EPA 8240 11/2/95 2-Chloroethylvinylclher u 120 ppb EPA 8240 11/2195 •2-Hexanonc 140B 31 ppb EPA 8240 11/2/95 I 2-Hexanone l"W'8,.,,8 31 ppb EPA 8240 11/2195 4-Methyl-2-pentanone u 62 ppb EPA 8240 1112195 I 4-Methyle-21)Cntanone u 62 ppb EPA 8240 11/2195 Acetone 4208 62 ppb EPA 8240 11/2/95 Acetone 420B 62 ppb EPA 824-0 11/2/95 I Benzene u 31 ppb EPA 8240 11/2/95 Benzene u 31 ppb EPA 8240 11/2/95 Bromodichloromethanc u 31 ppb EPA 8240 11/2/95 I BromcxJjchJoromethane u 31 ppb EPA 8240 11/2/95 Bromoform u 31 ppb EPA 8240 11;2195 · Bromoform u 31 ppb EPA 8240 11/2/95 I Bromomethane u 31 ppb EPA 8240 11/2/95 Bromomethanc ·U 31 ppb EPA 8240 11/2/95 I Carlxm disulfide u 31 ppb EPA R240 11/2/95 Carbon Disulfide u 31 ppb EPA 824-0 1112/95 Carbon tetrachloride u 31 ppb EPA 8240 11/2/95 I ) • - I 11176 0ow.u Roo,I -~vm., NC lJIJ.1 !'bone: (7CM) 58S-5076. FAX: (7{M) 588-24~ Paac: 3 I I Qo1lJ1 Environmental I. ,.consultanh. Inc I Client: OHM Col]lOration r-ns P. 0s OEC Certificate of Analysis North Carolina Certification Number: 305 I I I I I I I I I I I I I I · 240 I Tuckascegee Road Charlotte, NC South Carollna Certificalion Number: 99032 Client#: 381 Contact: Jack Kilbarger Sample Date: 24-0::!•95 SDG#: SDG-000285 Lab Sample ID: LSID-00 I 096 Sample ID: CO-WS-16 Paramour Re!Ult Carton Tetrachloride u Chlorobcrux:nc u i Chlorobcnzt:nc u Chloroethanc u Chloroethane u Chlorofonn u Chloroform u Chlorometliane u Chloromethane u ds-1,2, -Dichloroetlu:nc u cis-l ,3 ·Dichloropropcnc u cis• I ,3-Dichloropropcnc u Dibromochloromethane u Dibromochloromethane u Ethyl benzene S5°-'lr- Ethylbenznc 55 Methylene Chloride 191 Methylene chloride 19] Styn,nc u Styrene u Tctrachloroctbcnc u Reporting Limlt Unit 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 3 I ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb Receipt Date: 24-0ct-95 Report Date; 28-Nov-95 Approved By: Kenneth R RJcbard!on Project Manager Method Time Date EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 Jl/2/95 EPA 8240 11/2195 EPA 8240 1112195 EPA 8240 11/2/95 EPA 8240 J 1/2/95 EPA 8240 11/2/95 EPA 82>1-0 11/2/95 EPA 82,o l 1/2/95 EPA 82>1-0 IJ/2/95 EPA 8240 l l/2/9S EPA 82,0 ll/2/9S EPA 8240 1112195 EPA 8240 1112/95 EPA 8240 I 1/2/95 EPA8240 11/2/95 EPA 8240 1!12/95 EPA 8240 11/2'95 EPA 8240 IJ/2/95 EPA 8240 11/2195 IJ I 11176 Dowsu lload -l'h,,,IIJ., NC lfl:1-4 !'hon,, (7~ Sia.S076 -FAX, (71M) ga.2-454 Paae 4 I Analyst • • • I I ) I I I I I I I I I I I I I I I· ) I I • ' ..... I ' I.IV :, 0 E C l°tet,-,,,,,,, _______ , Certificate of Analysis Client: Client#: Contac1: Sample Date: SDG II: OHM Corporation 240 I Tuckasecgee Road C~arlotte, NC 381 Jack Kilbarger 24-0ct-95 SDG-000285 Lab Sample ID:LS!D-001096 Sample ID: CO-WS-16 Parameter Resclt Tetrachloroethenc u Tolnenc 74 Toluene 74 Total Xylenes 480 Total Xylcnes 480 trans-I , 2-<lichloroethene u trans-1,3-Dichloropropenc u rrans-1,3-Dichloropropene u Trichloroethenc u Trichloroetbene u Trichlorofluoromethanc u Tricltlorofluoromethanc u Vmyl acetltte u Vinyl Acetate u Vinyl chloride u Vinyl Chloride u 1,2 ,4-Trichlorobenzcne u 1,2-Dichlorobenzenc u I, 3-Dichlorobcnzcnc u 1,4-Dichloroocnzcnc u 2.4..S-Trichlorophenol u Reporting Limit Unit 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb :ll ppb 31 ppb 31 ppb 31 ppb 31 ppb 62 ppb 62 ppb 31 ppb 31 ppb 830 ppb 830 ppb 830 ppb 830 ppb 830 ppb North Carolina Certification ~umber: 305 South Carolina Certification Numbu: 99032 Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Appro,·ed By: Kenneth R. Richardson Project Manager Method Time Date EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 l l/2/95 EPA 8240 11/2/95 EPA 8240 I 1/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 l 1/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 l l/2/95 EPA 8240 11/2/95 EPA 8240 l 1/2/95 EPA 8270 I ln/95 EPA 8270 lln/9.l EPA 8270 lln/95 EPA 8270 I ln/95 EPA 8270 11n/9s Anaty,t JI 17' 0-. Rood . Pla.mllo, NC lllJ~ Phou, (704) 518-5076 • 1 AX, (704) S88-l-4~ Pqe 5 • • • I •w I • It.I/ I Qmn1 p~ Environmental OE C I Consultantt, lnc I~ • 7 I Certificate of Analysis 0 I ClieDt: OHM Corporation North Carolina Certlfkalion Number: 305 24-0 I Tuckasccgcc Road South Carolina Certification Number: 99032 .. I Charlot1e, NC 381 Client#: Receipt Date: 24-0ct-95 I Contact: Jack Kilbarger Report Date: 28-Nov-95 I Sample Date: 24-0ct-95 SDG#: SDG--000285 Approved By: Lab Sample ID: LSID-001096 Kenneth R. Richardson I Sample ID: CO-WS-16 Project Manaiier Reporting Parameter Result Limit Unit Method Time Date Analyot I 2,4,6-Trichlorophenol u 830 ppb EPA 8270 l lnt95 2,1-Dichlorophcnol u 830 ppb EPA 8270 llnt95 • I 2,4-Diw~lhylphcnol u 830 ppb EPA 8270 1 ln/95 2, 4-Dinitrophenol u 4200 ppb EPA 8270 lln/95 2, -!•Dinitrotol = u 830 ppb EPA 8270 1117195 I 2,6-Dinitrotoluene u 830 ppb EPA 8270 11/7/95 2-Chloronaphthalene u 830 ppb EPA 8270 11/7/95 2-Chlorophcnol u 830 ppb EPA 8270 11/7/95 I 2-Mcthlyphenol (o-cresol) u 830 ppb EPA 8270 l 1/7/95 2-Melhylnaphthalenc 3900 830 ppb EPA 8270 1 ln/95 I 2-Nitroaniline u 4200 ppb EPA 8270 11/7/95 2-Kitrophcool u 4200 ppb EPA 8270 1 ln/95 3 ,3-Dichlorobenzidine u 1600 ppb EPA 8270 lln/95 I 3-Nitroaniline u 4200 ppb EPA 8270 11/7/95 4,6-Dinitro-2-metbylphcnol u 4200 ppb EPA 8270 I ln/95 4-Bromophenyl phenyl ether u 830 ppb EPA 8270 1 ln/95 I 4-Chloraniline u 1600 ppb EPA 8270 11/7/95 4-Chloro-3-melhylphcnol u 1600 ppb EPA 8270 lln/95 4-Chlorophenyl phenyl ether u 830 ppb EPA 8270 I lnt9:!J I 4-Melhylphenol (p-=sol) u 830 ppb EPA 8270 I lnt95 4-Nitroaniline V 4200 ppb EPA 8270 I In/95 I • 1117, 0.-11,w,d. l't..vllo, NC l81J.I Phoae: (704) 588-5076-FA.X: (704) !!n-l45< I Page 6 I I Qmlli ;O~ Environmental OE C I ') Conn1ll.a11u, lni;_ ""/-, .~ • I Certificate of Analysis I Client: OHM Cmporatlon North Carolina Certification Number: 3-05 240 I Tuckaseegce Road South Carolina Ccrtlfkatioa Number: 99032 I Charlotte, NC Client#: 381 Receipt Date: 24-0ct-95 I Cool.act: Jack Kilbarger Report Date: 28-Nov-95 I Sample Date: 24-0ct-95 SDG#: SDG--000285 Approved By: Lab Sample ID:LSID-001096 l<concth R. Richardson I Sample ID: CO-WS-16 Project Manager Rq,ortin& I Parameter Result Limit Unit Method Time Date Analylt 4-Nitrophenol u 830 ppb EPA 8270 11/7/95 Accnaphthene u 830 ppb EPA 8270 l !/i/95 I Accnapbthy Jene u 830 ppb EPA 8270 11/7/95 • Anthracene u 830 ppb EPA 8270 lln/95 Benzo(a)anthracene u 830 ppb EPA 8270 I ln/95 I Be= (a) pyrene u 830 ppb EPA 8270 l ln/95 Be= (b) fluoranthene u 830 ppb EPA 8270 11/1195 I Benzo (ghi) perylcne u 830 ppb EPA 8270 1 ln/95 Bcnzo (k) fluoranthene u 830 ppb EPA 8270 lln/95 Benzoic acid u 4200 ppb EPA 8270 lln/95 I Bcnzyl alcohol u 1600 ppb EPA 8270 I ln/95 Bis (2-chloroethoxy) methane u 830 ppb EPA 8270 lln/95 Bis (2-chloroethyl) ether u 830 ppb EPA 8270 11/7195 I Bis (2-<:hloroisoprobyl) ether u 830 ppb EPA 8270 lln/95 Bis (2-ethylhexyl) phthalate 41000E 830 ppb_. EPA 8270 lln/95 Butyl bcnzyl phthalatc u 830 ppb EPA 8270 lln/95 I Chrysene u 830 ppb EPA 8270 llnl9S Di-n-bU!yl phthalate u 830 ppb EPA 8270 lln/95 I Di-n-octylphthalate u 830 ppb EPA 8270 11n19s Dibenzo (ah) anthracene u 830 ppb EPA 8270 11n/9s Dibcnzofuran u 830 ppb EPA 8270 )1/7/95 I ·, • -· I 11176 Do,n,. Road -Pln..-llt. NC 18134 I'll .... : (7{MJ 588-5<176 • FA.>;: (7{MJ 5U-l~ I Paee 7 I I !lmIJ1 ;0'21,'...,, , Environmmtal OE C /7 I ) C.aam.ltantJ., la, ~- I Certificate of Analysis I Client: OHM Corporation Nonb Carolina Certification Number: W-1 2401 Tuckasecgec Road South Carolina Certification Number: 99032 I Charlotte. NC Clienl #: 381 Receipt Date: 24-0ct-95 Contact: Jack Kilbarger Report Date: 28-Nov-95 I Sample Dau:: 24-0ct-95 I SDG#: SDG,000285 Approved By: Lab Sample ID: LSID-001096 Kenneth R. Richardson I Sample ID: CO-WS-16 Project Manager Reponl112 Pan.meter Rerult Um.it Unit Method Time Date Analyst I Diethylphthalate u 830 ppb EPA 8270 l!n/95 Di=lhylphthalatc u 830 ppb EPA 8270 lln/95 • I Fluornnthene u 830 ppb EPA8270 l!n/95 f1uorcnc u 830 ppb EPA 8270 lln/95 Hcxachlorobe~ u 830 ppb EPA 8270 ]Jn/95 I Hexachlorobutad.icne u 830 ppb EPA 8270 l!n/95 Hexachlorocycioperuadiene u 830 ppb EPA 8270 l!n/95 Hexachloroethanc u 830 ppb EPA 8270 lln/95 I lndeno (l,2,3«!) pyrene u 830 ppb EPA 8270 lln/95 lsopboronc u 830 ppb EPA 8270 Jln/95 N-Nitroso-<li-n-propylamine u 830 ppb EPA 8270 l!n/95 I N-Nitrosodipbenylamine u 830 ppb EPA 8270 l!n/95 N apbtha!J:nc 2400 830 ppb EPA 8270 lln/95 I Nitrobenzene u 830 ppb EPA 8270 11/7/95 Pentachlorophenol u 4200 ppb EPA 8270 11/7/95 Phcoantllrenc 1700 830 ppb EPA 8270 l!n/95 I Phenol u 830 ppb EPA 8270 I !n/95 Pyrene u 830 ppb EPA 8270 llnt95 I I ) • I 1176 no-llnod. l'tnmlk. NC 2HtJ• Ph....,, (71M) 588-5076 -PAX: ("70<) 588-264 I Paae 8 I I I I I I I I I I I I I I I I I I ) Qmm ;O~ -~-ns_viro_"ltan_nm_~_:.tgl_,nc ________ o __ E __ c ___________ ~_~ CUcnl: Clienl #: Conlact: Sample Dale: SDGN: Certificate of Analysis OHM Corporation 240 l Tuckasccga: Road Charlotte. NC 381 Jack Kilbarger 24-0ct-95 SDG-000285 Nor1h Carolina Ccrliflcatlon Number: 305 Soalh Carolina Ccrtlf'lcatloa Number: 99032 Receipt Dale: 24-0ct-95 Report Dale: 28-Nov-95 Appro,-ej! By: Lab Sample ID:LSID-001097 Kennclb R. lllihardaon Sample ID: CO-WS-17 Project Manager. Reporting Pll11Ullt:tcr-Reswt Limit Unit Method Time Date Analyl1 Arsenic 0.350 0.125 ppm EPA 7060 9:15 10/27/95 RCD Bariwn 25.5 D 2.S ppm EPA 6010 l0:25 10/26/95 RCD Cadmiwn uo 0.25 ppm EPA 6010 23:22 10/30/95 RCD Chromium 17.3 1.25 ppm EPA 6010 23:22 10/30/95 RCD Lead 3.00 1.25 ppm EPA 6010 23:22 10130/95 RCD Silver u 0.25 ppm EPA 6010 23:22 10/30/95 RCD Mercury 0.016 0.003 ppm EPA 7470 15:50 10127/95 DRW Sclcniwn u 0.125 ppm EPA 7740 10:10 10127/95 RCD 11176 Dowm Road -Pla<Vllt, NC 11113' P ..... , (704) -~. FAX: (704) 5811-l◄S. Paae 9 • • I I I I I I I I I I I I I I I I I I I Qmni Earironmental ) Consullanu. Inc Certificate of Analysis ) Client: Client#: Cuotact: Sample Date: SDG#: OHM Corporation 240 I Tuckascegcc Road Charlotte, NC 381 Jack Kilbarger 24-0ct-95 SDG--000285 Lab Sample ID:LSID--001098 . Sample ID: CO-WS-17 Parameter Result 1,1, 1-Trichloroethone u I, 1,1-Trichloro<thanc u I, 1,2,2-Tetrachlorocthane u I, 1,2,2-Tetrachloroethane u I, 1,2-Trichlorocthane u I, 1,2-Tricltlorocthane u I, l •Dichlorocthane u I, 1-Dich!oroethaoe u I, 1-Dichloroetheoe u 1,1-Dichloroethene u 1,2-Dichlorobeozene u 1,2-Dichlorobenzene u 1,2-Dicltlorocthanc u 1,2-Dichloroetbane u 1,2-Dichloroethene u 1,2-Dichloropropane u 1,2-Dichloropropane u 1,3-Dichlorobenunt u 1.3-Dich!orob--..nzene u I, 4-Dichlorobenzene u l, 4-Dichlorobcnzne u Reponiog Limit Unit 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 ppb 31 pph 31 ppb Nonh Carolina Ccrtif",catioa Number: 305 South Carolina Certlficatioo Number: 99032 Recdpt Date: 24-0ct-95 Report Date: 28-Nov-95 Apprond By: Kemoeth R. Richardson Project Manager Method Time Date EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/9S EPA 8240 11/2/9S EPA 8240 I V2/95 EPA 8240 11/2/9S EPA 8240 l V2/95 EPA 8240 11/2195 EPA 8240 1112195 EPA 8240 11/2/95 EPA 8240 I 1/2/95 . EPA 8240 I 1/2J95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 EPA 8240 11/2/95 Aoalyrt 11176 Dowm Rood. l'1an1lc. l'C 28134 PI-one: ('7~) 588-!0~6. f AX: ('7~) 511S-2454 . Page IC • • • I I I I I I I I I I I I I I I I Qmni Enrlrorimrntal ·~onsultantt, Inc OEC ,;O~ I~. 'o/~. ---------~ Certificate of Analysis Client: OHM COIJX)ratlon 240 I Tockaseegt<: Road Charlotte, NC North Carolina Certification Number: 305 South Carolina Certilicadoo Number: 99032 Client#: 381 Contact: Jack Kilbarger Sample Date: 24-0ct-95 SDG#: SDG-000285 Lab Sample ID: LSID-001098 SlDlple ID: CO-WS-17 Parameter 2-Butanonc /·Butr.none 2-Chloroet.hcylvinylcthcr 2-Cbloroethylviny !ether 2-Hexanonc 2-Hcxanone 4-Metllyl-2-pentanone 4-Mcthyle--2-pentanone Acetone Acetone Benunc Benzene Brornodichlorometbanc Bromodichloromethano Bromofonn Bromoform Bromom<thane Bromomethaoe Carbon Disulfide Catboo disulfide Carbon Tetrachloride Result 37BJ 31B] u u u u u u 320B 320B u u u u u u u u u u u Reporting Limit Unit 63 ppb 63 ppb 130 ppb 130 ppb 63 ppb 63 ppb 63 ppb 31 ppb 63 ppb 63 ppb 31 ppb 31 ppb 31 ppb 31 ppb 3 l ppb 31 ppb 3 l ppb 31 ppb 31 ppb 31 ppb 31 ppb R.eaipt Date: 24-0ct-95 R.:port Date: 28-Nov-95 Approved By: Kenneth R. R.icbardM>o Project Manager Method Time: Date EPA 8240 l l/'l/9~ EPA 8240 l 1/2/95 EPA 8240 l ln/95 EPA 8240 l 112/95 EPA8240 I In/95 EPA 8240 11/2/95 EPA8240 11/2/95 EPA 8240 11/2/95 EPA8240 11/2/95 EPA8240 11/2/95 EPA8240 11/2/95 EPA8240 1112/95 EPA8240 11/2195 EPA 8240 11/2/95 EPA8240 11/2/95 EPA 8240 11/2/95 EPA8240 11/2/95 EPA 8240 11/2/95 EPA8240 11/2/95 EPA8240 ll/219:5 EPA 8240 I J/2/95 I _j I I I 1,r. r>own, Road. PlDnllk, NC 1813-4 Pho"': (71).f) 58i-.l016 • YAX: (7114) SIIS-l<:14 Page 11 I Analyst • • I I ,1,..,1 lo J..,J I !lmn.l ,P~ Environmmtal • f ,' .. OEC IJ Qln~uLtana, inc / • "7,, I Certificate of Analysis J I Client: OHM Corporation North Camllna Cerdficatlon Number: 305 240 I Tucka sec gee Road South CarollDa Certification Number: 99032 I Charlotte, NC Client#: 38! Receipt Date: 24-0ct-95 I Contact: Jack Kilbarger Rtport Date: 28-Nov-95 I SllDlple Date: 24--0ct-95 SDG#: SDG--000285 Approved By: Lab Sampl• ID:LSID--001098 Kenneth R. Richardson I Sample ID: CO-WS-17 Project Manoger Reponini I Parameier Result Limit Unit Method Time Date Analyst Carbon tetrachloride u 31 ppb EPA 8240 11/2/95 ) Ch.lorobcruene u 31 ppb EPA 8240 11/2/95 • I Chlorobenzene u 31 ppb EPA 8240 I l/2J95 Ch.loroetbane u 63 ppb EPA 8240 l 1/2/95 Ch.loroethane u 31 ppb EPA 8240 l l/2/95 I Chloroform u 31 ppb EPA 8240 I ll".J95 Chloroform u 31 ppb EPA 8240 I ll".J95 I Chlorornethane u 63 ppb EPA 8240 l ll".J95 Chloromethanc u 63 ppb EPA 8240 I ll".J9S cis-1,2, -Dichloroethcnc u 31 ppb EPA 8240 11/2/95 I cis-1, 3-Dichloropropcnc u 31 ppb EPA 8240 11/2/95 cis-1,3-Dichloropropcnc u 31 ppb EPA 8240 11/2195 Dibromochloromethanc u 31 ppb EPA 8240 11/2/95 I Dibromocbloromethane u 31 :,pb EPA 8240 11/2/95 Ethylbe=c !SO 31 ppb EPA 8240 11/2/95 Ethylbenzne !SO 31 ppb EPA 8240 l 1/2/95 I Methylene Chloride 16) 31 ppb EPA 8240 l l/2/95 Methylene chloride 161 31 ppb EPA 8240 1112/95 I Styrene u 31 ppb EPA 8240 11/2/95 Styrcru: u 31 ppb EPA 8240 11/2/95 Terracliloroethcnc 9.9) 31 ppb EPA 8240 l l/2/95 I J • I 11176 0-.. Ro..! -Plntt1J1,0 NC ll!.1' Phoou, (70<) SBS-3'l76 -YAX, (70<) SBS-l-4~ Page 12 I I I I I I I I I I I I I I I I I I I I QmJii Environmental 'i Consultants, Inc Client: OHM: Corporation I ..... f o J. .. OEC Certificate of Analysis North Carollna Certification Number: JOS 240 I Tuckaseegec Road Sooth Carolina Certification Number: 99032 Charlotte, NC Client#: 381 Receipt Date: 24-0ct-95 Contact: Jack Kilbarger Report Date: 28-Nov-95 Sample Date: 24-0ct-95 SDG II: SDG-000285 Approved By: Lab Sample ID:LSJD-001098 Kenneth R. Richardson Sample ID: CO-WS-17 Project Manager Reporting Parameter Result Limit Unit Method Ti.mt.: Date Analyrt Tetrachloroethene 9.91 31 ppb . EPA 8240 llnl95 Toluene 2JOOE 31 ppb EPA 8240 l l/2/9j Toluene 2::b£¥li" 31 ppb EPA 824/l l 1/2/95 Total Xylenes 1350 JI ppb EPA 8240 11/2/95 Total Xylenes 1350 31 ppb EPA 8240 11/2/95 trans-1,2-dichloroethenc u 31 P!'O EPA 8240 11/2/95 trans-1,3-Dichloropropcne u 31 ppb EPA 8240 11/2/95 u-ans-J ,3-Dichloropropcne u 31 ppb EPA 8240 11/2/95 Trichloroethene u 63 ppb EPA 8240 11/2/95 Trichlorocthene u 31 ppb EPA 8240 1112195 Trichlorofluoromethane u 63 ppb EPA 8240 llMS Trichlorof!UO«lmetbane u 31 ppb EPA 8240 11/2/95 Vinyl Acetate u 63 ppb EPA 8240 11/219; Vinyl acetate u 63 ppb EPA 8240 11/2/95 V~yl chloride u 63 ppb . EPA 8240 llnl95 Vinyl Chloride u 63 ppb EPA 8240 11/2/95 1.2,4-Trichlorobcn,.ene u 860 ppb EPA 8270 11/6/95 1,2-Dichlorobcnzene u 860 ppb EPA 8270 1116/95 1,3-Dichlorobcnzcne u 860 ppb EPA 8270 1116195 I, 4-Dichlorobenzene u 860 ppb EPA 8270 1116/95 2,4,5-Trichlorophenol u 860 ppb EPA 8270 1116195 ) 11176 Do,nu RO¥! -Pinn-Ilk, NC ?813◄ Pboa,, (704) 583-5076 • f AX, (704) 5111-1-464 Paae 13 • • I I I I I I I I I I I I I I I I I I I ;O~ Qmni Environmental ": Consultants, Inc OEC (~ r .• ------------------------------ir,.,. Certificate of Analysis J Client: OHM Corporation Nortb Carolina Ccrtlflcat1on Number: 39! 240 I Tuckasccgee Road South Carolina Ccrtlllcatlon Nwnber: 99032 Charlo\te, NC Client ii: 381 Receipt Date: 24-0ct-95 Cootact: Jack Kilbarger Report Date: 28-Nov-95 Sample Date: 24-0ct-95 SDG#: SDG--000285 Approved By: Lab Sample ID:LSID-001098 Kenneth R. RlcbllrtOOo Sample ID: CO-WS-17 Project Manai,:r Reporting Parameter Rault Limit Unit Method Tune Date An&lyrt 2,4,6-Trichlorophenol u 86-0 ppb EPA 8270 11/6195 ) 2,4-Dichlorophenol u 860 ppb EPA 8270 11/6/95 • 2,4-0imclhylphcnol u 860 ppb EPA 8270 I 1/6/95 2,4-Diniu-ophcnol u 860 ppb EPA 8270 11/6/95 2,4-Diniu-otoluene u 860 ppb EPA 8270 11/6/95 2,6-Dinitrotoluene u 860 ppb EPA 8270 11/6/95 2-Chloronaphthalene u 860 ppb EPA 8270 11/6/95 2-Chlorophenol u 860 ppb EPA 8270 1116/95 2-Methlyphenol (o-cresol) u 860 ppb EPA 8270 11/6/95 2-Methylnapbthalcne 930 860 ppb EPA 8270 11/6/95 2-Nitronniline u 4300 ppb EPA 8270 11/6/95 2-Nitrophcool u 860 ppb EPA 8270 I 1/6/95 3 ,3-Dichlorobenzidinc u 1700 ppb EPA 8270 l 1/6/95 3-Nitroanilinc u 4300 ppb EPA 8270 11/6/95 4,6-Dinitro-2-methylphmol u 4300 ppb . EPA 8270 11/6/95 4-Bromophenyl phenyl ether u 860 ppb EPA 8270 11/6/95 4-Chloraniline u 1700 ppb EPA 8270 I l/6/95 4-Chloro-J-methylphenol u 1700 ppb EPA 8270 11/6/95 4-Chlorophenyl phenyl ether u 860 ppb EPA 8270 11/6/95 4-Methylphenol (p-cresol) u 860 PJXl EPA 8270 11/6/95 4-Nitroanilinc u 4300 ppb EPA 8270 ll/6/95 I • / ll 17, !ln,n,o R .... · l'tanill.. ~c l81J< Pboo<, ('71M) :11¥-50"/6 -FAX, ('7!>4) S88-l45-I Pag,, 14 I I,-, I I I I I I I I I I I I I I I I I ) Qmn1 EnvironmenJal Consu/tqnp. Inc DEC Certificate of Analysis Client: OHM Corporation 240 I Tuckaseegee Road Charlotte, NC Client#: 3~] Contact: Jack Kilbarger Sample Date: 24-0ct-95 SDG#: SDG--000285 Lab Sample ID:LSID-001098 Sample ID: CO-WS-17 Pana.meter Result 4-Nitrophenol u Acenaphthene u Acenaphth)·lcne u Anthraccne u Bcnzo (a) antluaccnc u Bcnzo (a) pyreuc u Bcnzo (b) Ouoranthcne u Bcn.zo (ghi) peiylcnc u Benzo (k) Ouoranthene u Be1120ic acid u Benzyl alcohol u Bis (2-ch!oroethoxy) methane u Bis (2-ch!orocthyl) ether V Bis (2-ch!oroisoprobyl) ether u Bis (2-ctliylhcxyl) phthalalc 16000E Butyl bcnxyl phthalate u Cluysenc u Di-n-butyl ph!halatc u Di-n-octylphtlwate u Dibenz.o (ah) antluaccr,c u Dibenzofuran u Reporting Limit Unit 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 4300 ppb 1700 ppb 860 ppb 860 ppb 360 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb North Carolina Certification Number: JOS Sooth Carolina Certlf!catlon Number: 99032 Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By: Kenneth R. Richardion Project Manager Method Time Date EPA 8270 11/6/9S EPA 8270 I 1/6/95 EPA 8270 11/6/95 EPA 8270 11/6/9S EPA 8270 11/6/95 EPA 8270 11/6/9S EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 l 1/6/95 EPA 8270 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA8270 11/6/95 EPA 8270 l l/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA8270 11/6/95 EPA 8270 11/fu<lS EPA 8270 11/6/95 EPA 8270 11/6/95 Analyst 11176 0-.. Road . PIM,,Ule, NC 2'11:M Phan,£ (704) ""'-'°" -FAX, (704) -.1454 P• 15 • • • I I I I I I I I I I I I I I I I I I I flmni Environmental 1 Consultants. Inc OEC Certificate of Analysis Client: OHM Corporation 240 I Tuckascegee Road Charlotte, NC North Carolina Certlftcatlon Number: 305 South CarollIJa Certification Number: 99032 Client#: 381 Coottct: Jack K.ilbarger Sample Date: 24-0ct-95 SDG#: SDG-000285 Lab Sample ID:LSID-001098 Sample ID: CO-WS-17 Parameter Result Diethylpbthalate u , Dimethylphthalate u ) Flu<iranthcne u F1uorene u Hcxachlorobenzcnc u Hcxachlorobutadiene u Hexachlorocyclopentadienc u Hcxachloroethane u lndcno (1,2,3~) pyrene u lsophorone u N-Nitroso-di-o-propylamine u N-Nitrosodiphenylamine u Naphthalene 1000 Nitrobenzene u Pcmachlorophcnol u Phcnanthrene u Phenol u Pyrcne u Reporting Limit Unit 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 4300 ppb 860 ppb 860 ppb 860 ppb Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By: Kenneth R. Richardson Project Manager Method Time Date EPA 8270 11/6/95 EPA 8270 11/6/95 !:PA 6270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 I J/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 · EPA 8270 1116195 EPA 8270 11/6/95 11116 l>owns Rau. PID,,1Dt, SC 211!~ Pho .. , ("11)4) -1'. FAX, (,o.) 518-lA5-4 Paae 16 Analyst • • I le I I I I I I I ft I I I I I I .. I I Memo To: File Date: March 15, 1996 From: Douglas Moore 4 /J-tt,{~ Environmental Chemist NC Superfund Section Topic: Site Inspection -Sampling Trip Cherokee Oil Company 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCD 980 799 019 On Tuesday, March 5, 1996, Douglas Moore of the NC Supefund Section departed the Raleigh Office for Charlotte, NC. Arrived Charlotte at 16:15 and finalized arrangements to collect surface water, sediment samples at E.F. Lombardi Co. Doug Moore also received permission from Jeff Meyer (or Mercer), the manager at Southern Electric Co. across from the site, to collect a background soil sample. Doug Moore then checked in at the Adams Mark Hotel for the night. On Wednesday, March 6, 1996, at 07:30 am, Doug Rumford, Jeanette Stanley and Harry Zinn from the NC Superfund Section departed the Raleigh Office for Charlotte, NC. At 08:30, Doug Moore met with Chief District Court Judge James Lanning to obtain an administrative search and inspection warrant for the purpose of collecting environmental samples at the subject site. Judge Lanning reviewed the affidavit and had Doug Moore swear to the facts contained in the affidavit. Judge Lanning then signed the administrative search warrant and provided a copy to be used at the site during the sampling event and a copy for our file. Judge Lanning and Doug Moore agreed that Doug Moore would return to his office at Suite 3304, Criminal Courts Building, 700 East Fourth Street, Charlotte, NC and meet with his secretary Pat Cheek, who would then sign the warrant, documenting that it was served at the site. A copy of the administraive search warrant is attached (attachment I). At 11 :00, Doug Moore drove to the site and met with the three staff members who arrived from Raleigh. At 11 :05, Tony Roux, Mecklenburg County Department of Environmental Protection -Water Quality Section, arrived at the site to observed the off-site sampling. A representative of AT&T arrived at the site at 11 :20 a.m. After discussing the sampling I I .. I I I I I I I I I I .. I I event with the representative, he indicated that there were no AT&T lines at the site. The AT&T representative departed the site. No additional utilities locators arrived at the site. Doug Moore discussed the sampling event with Tony Roux, outlining the on and off-site sample points to be collected. At 11:30, Team #1, consisting of Doug Rumford ("DR"), Jeanette Stanley ("JS") and Tony Roux (''TR"), departed the site to collect the off-site surface water and sediment samples. At 11 :35, Team #2, consisting of Doug Moore ("DM") and Harry Zinn ("HZ") walked to the front gate of the site at Berryhill Road and affixed a copy of the administrative search warrant to the front gate. A copy of the padlock key, previously provided to DM by John Custance of OHM Remediation Services.was used to open the gate. At 11 :45, HZ of Team #2 began augering a soil boring at Area #1. Soil is a red to orange, coarse grained clay with gravel intermixed. At 2 feet, HZ encountered a dark stained soil. Stained soil is a ash-gray to black coarse-grained clay. At 11 :50, HZ collected a soil sample from the stained soil at the 2-3 foot interval. HZ collected VOC from bottom of auger (2.5 -3 foot depth). The sample was then composited and collected for SVOC, inorganics and PCB/Pesticide analyses. No odors were detected in the soil sample. HNu readings indicated a slight deflection of the needle (0.1 meter units) in the sample borehole. No elevated readings were detected in the ambient air above the borehole. The sample was labeled "CO-002-SB". At 12:00, Team #I arrived back at the site to discuss the sampling plan. Due to the rainy conditions, Stewarts Creek is swollen, fast-flowing and hazardous. Thus, the surface water and sediment samples originally planned for Stewarts Creek will have to be postponed. Doug Moore told Team #I to collect the surface water and sediment samples from the Unnamed Tributary to Stewarts Creek ("UT"), and to document the stream conditions at Stewarts Creek and the UT. At 12:25, HZ of Team #2 augered soil boring at Area #2. The soil profile at this location consists of 0-4 inches of red clay, 4 inches to 2 feet of gray gravel, 2 + feet of dark red clay. The dark red clay has a iridescent sheen. HNu needle deflection of I meter unit in sample borehole. No elevated HNu readings in the ambient air above the sample borehole At 12:40, HZ of Team #2 collected subsurface soil sample from 2.5 feet below land surface from Area #2. No elevated HNu readings noted in soil sample. HZ collected VOC from bottom of auger. The remainder was then composited in a clean pyrex pan and samples were collected for SVOC, Inorganics and PCB/Pesticide analyses. Sample was labeled "CO-003-SB". At 12:30, JS of Team #I collected sediment sample CO-003-SD from the storm sewer drainage ditch, approximately I 00 feet south of storm grate near the intersection of Thrift Road and Freedom Road. The storm sewer flows from Freedom Road along Armin Products warehouse, under railroad spur to the UT. The sediment sample was collected 2 I .. I I I I I I I .. I I I I I I le I I from the 0-12 inch interval in the bed of the drainage pathway. The soil sample was a poorly sorted, silty sand and gravel. The bottom inch was composed of a dark gray material. JS collected VOC sediment sample from a clean pyrex sample pan prior to compositing. Then, the soil was sampled for SVOC, Inorganics and PCB/Pesticides analyses. At 13:05, HZ of Team #2 collected a surface soil sample from the rear of the warehouse at Area #3. The soil profile consists of 2 inch of black organic rich soil with sand to 6 + inches. HZ collected VOC soil sample prior to compositing in a clean pyrex pan. Then, soil samples were collected for SVOC, Inorganics and PCB/Pesticides analyses. The surface soil sample was labeled "CO-004-SL". At 13:35, HZ of Team #2 prepared to collect a surface soil sample from a vacant grass- covered lot in front of Southern Electronics, directly across Berryhill Road from the site. Mr. Jeff Meyer ( or Mercer?), manager of Southern Electronics, had previously granted us permission to collect the sample. The soil sample was abandoned at the request of a person identifying himself as the landowner. At 13:40, JS of Team #I collected a sediment sample from the unnamed tributary to Stewarts Creek ("UT"), at a point approximately 6 feet downstream of the storm sewer outfall. Due to the high flow of the UT, the sample was collected from the 3-6 inch profile of the stream bed using a hand auger. The sediment sample was a brownish-gray, silty clay that exhibited a pungent odor. The sediment was sampled for VOC first, then composited in a clean pyrex pan for SVOC, metals and PCB/Pesticide analyses. The sediment sample was labeled "CO-002-SD". At 13:50, JS of Team #1 collected a surface water sample from the UT at the same location as CO-002-SD. The surface water was sampled for VOC, SVOC and metals analyses. The surface water sample was labeled "CO-002-SW". The VOC sample was pre-acidified using 5 drops of 1: 1 HCL. The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3• At 14:00, Team #2 met with Suburban Propane office manager Tom Broom and yard manager Ralph Stewart to get access to the Suburban Propane soil sample locations downgradient of the site in the overland runoff path. At 14: 15, HZ of Team #2 collected a surface soil sample from the 0-6 inch profile in the overland runoff path near the west corner of the Suburban Propane building. According to the 1990 video, runoff from Area #2 was funnelled through this corridor. The top 4 inches are a dark-brown stained soil that grades to a red-orange clay. No odors were detected in the top 6 inchs of soil. HZ collected for VOC first, then composited the sample in a clean pyrex pan pnor to collecting samples for SVOC, metals and PCB/Pesticides analyses. The soil sample was labeled "CO-006-SL". 3 I .. I I I I I I I .. I I I I I I .. I I At 14:20, JS of Team #I collected a sediment sample at a point approximately 30 feet upstream of the storm sewer outfall on the UT. The sediment is a silty fine sand. The sediment was collected from the 0-6 inch profile of the streambed using a hand auger. The sediment was sampled for VOC first, then composited in a clean pyrex pan for SVOC, metals and PCB/Pesticide analyses. The sediment sample was labeled "CO-001- SD". At 14:30, JS of Team #I collected a surface water sample at the same location as CO- 001-SD. The surface water was sampled for VOC, SVOC and metals analyses. The surface water sample was labeled "CO-00 I-SW". The VOC sample was pre-acidified using 5 drops of I: I HCL. The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3• At 14:30, HZ of team #2 collected a surface soil sample from the intermittent drainage ditch that connects the Cherokee site to the storm sewer grate #3. The soil is a dark brown, sandy clay. The soil sample was collected from the top 4 inch soil profile. The soil was sampled for VOC analyses first, then composited in a clean pyrex pan prior to collecting soil samples for SVOC, metals and PCB/Pesticide analyses. The soil sample was labeled "CO-005-SL". At 14:45, JS of Team #I prepared a trip blank in the field using organic free water and 5 drops of I: I HCL. Because of the high water level and fast stream flow encountered in Stewarts Creek, Team #I was unable to collect surface water and sediment samples in Stewarts Creek. These samples were scheduled to be collecting the following week. At 15:01, HZ of Team #2 collected a surficial soil sample at serve as a background for the area. The soil sample was collected from a grass-covered yard directly behind a residential house located at 2415 Tuckaseegee Road near the comer of Thrift, Tuckaseegee and Berryhill Roads. The house is the Charlotte Office of Miller, Sherrill, Blake, CPA. Permission to collect the sample was obtained from Mr. Gene Miller. The soil sampleis a dark red, clayey sand. No odors were detected in the soil and no elevated HNu readings were detected inb the sample hole. HZ collected a soil sample for VOC analyses first, then composited the soil in a a clean pyrex pan prior to collecting soil samples for SVOC, metals, and PCB/Pesticide analyses. The soil sample was labeled "CO-001-SL". At 15:13, HZ of Team #2 collected a subsurface soil sample from the 2 foot depth to serve as a background from the same location as CO-00 I-SL. The soil is a dark red clayey sand. No odors were detected in the soil and no elevated HNu readings were detected in the sample boring, borehole or ambient air above the sample borehole. At 15: 15, HZ collected a soil sample for VOC analyses first, then composited the soil in a clean pyrex pan prior to collecting soil samples for SVOC, metals, and PCB/Pesticide analyses. The soil sample was labeled "CO-001-SB" . 4 I ,. I I I I I I I ,, I I I I I I .. I I Team #1 arrived back at the site at 15:30. We departed the site for downtown Charlotte. At 16:03, Doug Moore met with Mrs. Pat Cheek of Judge Lannings office, who signed for receipt of the administrative search warrant and provided a copy for our records. On Wednesday, March 13, 1996, Doug Moore and Stuart Parker of the NC Superfund Section conducted a follow-up sampling event in Stewarts Creek. The purpose of the trip was to gather the surface water and sediment samples that were unobtainable during the previous weeks rainstorm. We arrived at the Freedom Road bridge over Stewarts Creek at 17:45 and reconned the sample collection points. At 18:00, Doug Moore ("DM") used a hand auger to collect a sediment sample from the 0-6 inch profile of the stream bed of Stewarts Creek at a point approximately 30 feet downstream of the confluence of the unnamed tributary to Stewarts Creek ("UT") and Stewarts Creek. The sediment was a light gray, silty sediment with a small amount of coarse-grained sand intermixed. No odors were detected in the sediment. The material was transferred to a clean pyrex pan and handed up the bank to Stuart Parker ("SFP"). SFP collected a sediment sample from the pan for VOC analyses first, then composited the sediment sample and collected samples for SVOC, metals and PCB/Pesticides analyses. The sediment sample was labeled "CO-005-SD". At 18:05, DM collected a surface water sample from Stewarts Creek, at a point approximately 15 feet downstream of the confluence of the UT and Stewarts Creek. DM collected surface water samples for VOC, SVOC and metals analyses. The samples were labeled "CO-005-SW". The VOC sample was pre-acidified using 5 drops of 1: 1 HCL. The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3• At 18:07, DM noted fishing line and a sinker hanging on bank vegetation at the sampling site in Stewarts Creek. At 18: 15, DM used a hand auger to collect a sediment sample from the 0-6 inch profile of the stream bed of Stewarts Creek at a point approximately 63 feet upstream of the confluence of the unnamed tributary to Stewarts Creek ("UT") and Stewarts Creek. The sediment was a light gray, fine silty sediment. No odors were detected in the sediment. The material was transferred to a clean pyrex pan and handed up the bank to Stuart Parker ("SFP"). SFP collected a sediment sample from the pan for VOC analyses first, then composited the sediment sample and collected samples for SVOC, metals and PCB/Pesticides analyses. The sediment sample was labeled "CO-004-SD". At 18:23, DM collected a surface water sample from Stewarts Creek, at a point approximately 70 feet upstream of the confluence of the UT and Stewarts Creek. DM collected surface water samples for VOC, SVOC and metals analyses. The samples were labeled "CO-004-SW". The VOC sample was pre-acidified using 5 drops of 1: 1 HCL. The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3 . 5 I .. I I I I I I I "' I I I I I I .. I I At 18:45, SFP prepared a trip blank in the field using organic free water and acidified with 5 drops of 1: 1 HCL. At 18:50, DM prepared a preservative blank using deionized water and preserved to pH 2.0 with 40 drops of 50% HN03. Departed the site for Raleigh. 6 :( ., !: !i ' ! '.• I i -·····--... b-16 I . I ~l'lf':a.,.,_, I., 5 l...) Jr-... ' f--l v-l _0-h:~«. . --, .. .L ______ c.~1.v--lv. .. j>E":",./>:"/15 i-_ , ~ _ II~__,,_, n c.<>:--:½c,:~ ~ ~ JJ-3 i I . 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Environmental Consultanh, Inc OEC Certificate of Analysis Client: OHM ColJ)Oration 240 I Tucl<asecgec Road Ch.arloue, NC Oien! ii: 3~1 Contact: Jack Kilbarger Sample Date: 24-0ct-9j SDG#: SDG-000285 Lab S1.mple ID:LSID-001098 Sample ID: CO-WS-17 Parameter iwull 4-Nitrophenol u A=phthene u Acenaphthylcne u Anthracenc u Bcnzo (a) anthracc,c u Bemo (a) py~uc u Bcnzo (b) fiuoranthcne u Bcnzo (ghi) pe,ylcne u Bcnzo (k) finoranthcne u Benzoic acid u Ben:zyl alcohol u Bis (2-<:hlomotboxy) methane u Bi• (2-.:hloroethyl) ether u Bis (2<hloroisoprobyl) ether u Bis (2-<:thylhexyl) phthala1e 16000E Buiylben:zylphthalate u Chrysene u Di-n-butyl phthalate u Di-n-octylphthmte u Dibc= (ah) anthractnc u Dibcnzofuran u Reporting Lhnlt Unit 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 4300 ppb 1700 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 Pix> 860 ppb 860 ppb 860 ppb North Carolina Certification Number: 305 Sooth Carolina Certlflcation Number: 99032 Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By: Kenneth R. Richard.Ion Project Manager Method Time · Date EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 1116/95 EPA 8270 11/6/95 EPA 82i0 1116195 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 EPA 8270 11/6/95 EPA 8270 11/6195 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 1116195 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6195 Analyst 1117' 0-.U Rood -l'tnntDe. :.C 28134 Plu>n,: (704)-.!!07~-FAX: (704) -.1454 Pqe 15 ,r:;·,_ ... ,:.~ ): '--...c¾ .. ,.' ... : \ •~) II II II II II II ---II II II -I I I I I ' Qmn1 Envtronme11ttll ) Consultants, Inc OEC Certificate of Analysis Client: OHM C-Orporation 240 I Tuckascegee RDad Charlene, NC North Carolina Certification Number: 305 South Carolina Ccrtlficatlon Number: 99032 Client#: 381 Conuct: Jock Kilbarger Sample Date; 24-0ct-95 SDG#: SDG-000285 L:ob Sample ID:LSID-001098 Sample ID: CO-WS-17 Pan.meter Remit Diethylphthalate u , Dimethylphthala~ u ) Flaoranthcne u F1uorene u Hcxachlornbenzcne u Hexachlorobutadiene u Hexacltlorncyclopentadiene u Hexachloroethanc u Jrulcoo {1,2,J~) J)YTI:llC u Jsophorone u N-Nitrnso-<li-n-propylamine u N-Nitro<odiphenylamine u Naphthalene 1000 Niu-obenzene u Pcn:achlorophcnol u Phcnanthrene u Phenol u Pymie u Reporting Limit Unit 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 860 ppb 4300 ppb 860 ppb 860 ppb 860 ppb Receipt Date: 24-0ct-95 Report Date: 28-Nov-95 Approved By; Kenneth R. Richardson Project Manacer Method Time Dale EPA 8270 11/6/95 EPA 8270 11/6/95 lil'A 6270 11/6/95 EPA 8270 Il/6/95 EPA 8270 I 1/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 I 1/6/95 EPA 8270 11/6/95 EPA 8270 1116195 EPA 8270 1116/95 EPA 8270 1116/95 . EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 11/6/95 EPA 8270 I 1/6/95 11116 Duwna llaod -1'111mda. SC Ull:M Pho.,., {704) -.S,7'. FAX: ()04) 3aa-1"5.4 Pase 16 Analyst --:-:, ' -.) STATE OF NORTH CAROLINA In The General Court Of Justice --'Me=ck=lenb=ur=g..._ ____ County ADMINISTRATIVE INSPECTION WARRANT FOR PARTICULAR CONDITION OR ACTIVITY G.S. 15-27.2 '• TO ANY LAWFUL OFFICIAL EMPOWERED TO CONDUCT THE INSPECTION AUTHORIZED BY THIS WARRANT: Toa applicant named on the accompanying affidavit, being duly sworn, has stated to me that .there is a condition,. object, activity, or ciraimstance legaDy justifying an inspection of the property desaibed in that affidavit.. I have-examined this applicant under oath or affirmation and have verified the aa:uracy of the mall81S In the affidavit establishing the legal grounds for this Warrant. YOU ARE HEREBY COMMANDED TO INSPECT' THE PROPERTY DESCRIBED IN THE ACCOMPANYING AFFIDAVIT. This inspection is authorized to check or reveal the conditions, objects, activilies, or ciraimstances indicated in the accompanying affidavit. This Warrant must be served upon the owner or possessor of the property described in the accompanying affidavit. If the owner or possessor is not present on the property at the time of inspection and you have made reasonable but unsuccessful efforts to locate the owner or possessor, you may instead serve It by affixing this Warrant or a copy to the property. THIS WARRANT MAY BE EXECUTED ONLY BETWEEN THE HOURS OF 8:00 A.M. AND 8:00 P.M. AND ONLY WllHIN 24 HOURS AFTER IT WAS ISSUED. IT MUST BE RETURNED WITHIN 48 HOURS AFTER IT WAS ISSUED. HOWEVER, IF THIS WARRANT IS ISSUED PURSUANT TO A FIRE INVESTIGATION AUTHORIZED BY G.S. 69-1, IT MAY BE EXECUTED AT ANY TIME WITHIN 48 HOURS AFTER IT IS ISSUED. IT MUST BE RETURNED WITHOUT UNNECESSARY DELAY AFTER ITS EXECUTION OR AFTER 48 HOURS FROM THE TIME IT WAS ISSUED IF IT WAS . NOT EXECUTED. ~ I certify that this WARRANT was executed on the date and time shown below. Oats ot &scution 3 c; / 9 6 S/gna&IIV a J,s,»ctJ.., OHJcial Time Of &scution 1-,' (.) 3 0 AM g'PM I& ef.a-/:lU( lf7?.-..- : /:A:%1:::t:~tt.tmfl~ JrWJ#..f.fu1rd~::: .. --~· ·%.?f.Mt:t@ili@: ;/ CLERK'S ACCEPTANCE :\@fJ?lttWLt~~fM!NM14.%11@It@lHtMi1%t!M:¥1M This WARRANT has been returned to this office on the dale and time shown below. Oats Of Rstvm Time Ot Rstvm D AM r5il PM D Ass/slantCSC D Deputy csc □ C/erlc Of Superior GaJtt I • . <ld.r'ru.-1'--Ll)-/-rQ+, l,l-Z-.• LJw,.,•1._c.u1.-t ~• :&. <l.lu:L ___ -+-~_C.,tL-Or\..;, . ,/_' I /"2'.. .A,::,-)7'\J'.1..),__A:TJ....UU.C(_ U'---· fv-.d-;f~i ~c;,, .'... · ~-1 ... ,--f-...A.,~~ C . . () ' i ~ +i----' l)h,.J... IMPORTANT: AttachthsAffidavittothsWamntifnotonrwsrsssids. •, Cl 1 '7 uO E · t.J: u:;::;z, 1 ~R-913M,SldaTwo ;;;.(.,u..... 3J c;__j l Rw. 7185 (Rep,tnflld 1193) OJ .. ft.-,,J..Ji)L_, /Jc..... d---8d--O..)...---- STATE OF NORTHCAROLINA In The General Court Of Justice __ Me_· _c_k_l_eno_·_ur____;_g _____ County [See Attached Affidavit;) AFFIDAVIT TO OBTAIN · ADMINISTRATIVE INSPECTION' WARRANT FOR PARTICULAR CONDmON OR ACTIVITY I, ------------,-,,------,--,::--,-----------...,being (-,..... name and positJan/ duly swom and exarninined under oath, state under oath that there Is probable cause for beDeving that there Is (desaiJa r:ondJ/Jon, object. adMty, ar~ which the _,,,,11 lntsndsd ID ch8clcarl'IIIIB8/./ at the property owned or possessed by and described as follows: --------------------------,---- (pn,cis8/y desaib9 the~ ID be inspeclDd./ The facts which establish probable cause to beDeve this are: ________________ _ IS/gna/lJnl OI Applk:ant SWORN AND SUBSCRIBED TO BEFORE ME S/gnatw& O •s:: •• ,tcsc 1,,J ~csc 1,,J C/Btft.OISupsrlorCourt □ Mag/s1ratB □ Supsrlor Court.Judge □ D/stlct CourtJudm>- IMPORT ANT:· Attach the Affidavit to th9 WARRANT if not on mvers11 sid9. AOC-CR-913M Rev. 7185 (Ra!>rinlDd 1193) (Over) STATE OF NORTH CAROLINA In The General Court Of Justice __ Me_• _c_k_lenb __ ur_g;.._ ____ County [See Attached Affidavit;) AFRDAVITTO OBTAIN - ADMINISTRATIVE INSPECTION· WARRANT FOR PARTICULAR CONDmON OR ACTIVITY · · 1, ____________________________ _,being (writs your-end position/ duly swom and examlnined under oath, state under oath that there is probable cause for believing that there Is at the property owned or possessed by --'l and described as follows: -------------------------- (pnKise/y aormbe the ,,,_iy ID be /nspeclsd.) The facts which establish probable cause to belleve this are: _______________ _ SWORN AND SUBSCRIBED TO BEFORE ME Da& □ Assislant csc □ Deputf csc w. a.1c a SupsrlorCourt □ □ Superior Cautt Judge □ Dlsttct Court ...... IMPORTANT: Attach the Affidavit to the WARRANT if not on nwerse side. AOC-CR-913M Rev. 7/85 (Roprin1"d 11113) (Over) STATE OF NO.RTH CAROLINA In The General.Court Of Justice __ Me=ck=lenb=~=~g,___ ____ County ADMINISTRATIVE INSPECTION,· WARRANT FOR PARTICULAR CONDITION OR ACTIVITY. G.S. 15-27.2 ., TO ANY LAWFUL OFFICIAL EMPOWERED TO CONDUCT THE INSPECTION AUTHORIZED BY THIS WARRANT: Toa applicant named on the accompanying affidavit,. being duly sworn, has stated ~ me that there is.a condftlon, object. activity, or cif'QJmstance legally justifying an inspection of the property desaibed in that affklavl, I havit examined this. applicant under oath or afflrmatk)n and have verified the aa:uracy of the matters in the affidavit establishing the legal. grounds for this Warrant. YOU ARE HEREBY COMMANDED TO INSPECT THE PROPERTY DESCRIBED IN THE ACCOMPANYING AFFIDAVIT. , This inspection is authorized to check or reveal the condttions, objects, activtties, or cirrumstances indicated in the accompanying affidavtt. · · This Warrant must be served upon the owner or possessor of the property described in the accompanying affidavtt. If the owner or possessor is not present on the property at the time of inspection and you have made reasonable.but. unsuccessful efforts to locate the owner or possessor, you may instead serve tt by affixing this Warrant or a copy to the property. THIS WARRANT MAY BE EXECUTED ONLY BETWEEN THE HOURS OF 8:00 A.M. ANO 8:00 P.M. ANO ONLY WITHIN 24 HOURS AFTER IT WAS ISSUED. IT MUST BE RETURNED WITHIN 48 HOURS AFTER IT WAS ISSUED. HOWEVER, IF THIS WARRANT IS ISSUED PURSUANT TO A FIRE INVESTIGATION AUTHORIZED BY G.S. 69-1, IT MAY BE EXECUTED AT ANY TIME WITHIN 48 HOURS AFTER IT IS ISSUED. IT MUST BE RETURNED WITHOUT UNNECESSARY DELAY AFTER ITS EXECUTION OR AFTER 48 HOURS FROM THE TIME IT WAS ISSUED IF IT WAS, NOT EXECUTED. D ~ ;:sc D Deputy csc, □ Mag/sllat8 &JpetlorCouttJudga . I certify that this WARRANT was executed on the date and time shown below. Date Of E.uJaJtion Slgna&uu Ol /1-,:1/119 0/Jlcial Tims Of E.uJaJtion This WARRANT has been returned to this office on the date and time shown below. Date Of Return S/gnaJrll Tims Of Return o· AM □.PM o Assistant csc o Deputy csc □ C/llff< a SuperlorCoutt IMPORT ANT: Attach ths Affidavit to ths Wanant if not on rsvsrss side. AOC-CR-913M. Sida Two Rav. 7185 (~ntlld 1193) STATE OF NORTH CAROLINA in the General Court of Justice Mecklenburg County ) ) ) ) ) ) AFFIDAVIT TO OBTAIN ADMINISTRATIVE INSPECTION WARRANT FOR PARTICULAR CONDITION OR ACTIVITY 1. The undersigned is an Environmental Chemist with the CERCLA Branch of the Superfund Section, Division of Solid Waste Management, North Carolina Department of Environment, Health and Natural Resources appearing this day to request a administrative search warrant for the Cherokee Oil Company Site ("site"), 1201 Berryhill Road, Charlotte, Mecklenburg County, North Carolina. 2. The site is registered as parcel #16, block #51, tax map #71 of the Mecklenburg County Tax Assessors office. 3. The site is owned by Gene Wesley Hartsell, as recorded in Deed Book #5828, Page #0131 at the Mecklenburg County Register of Deeds. 4. The site was formerly operated by Cherokee Resources ("Cherokee"), a North Carolina corporation incorporated under the laws of the State of North Carolina with its principal place of business at 1201 Berryhill Road, Charlotte, North Carolina. 5. Keith Norland Eidson was President and chief operating officer of Cherokee and had a fifty percent (50%) ownership interest in Cherokee. Gene Wesley Hartsell was Vice President of Cherokee and had a fifty (50%) ownership interest in Cherokee. 6. Cherokee was in the business of, among other things, reclaiming waste oil for energy recovery and treating and disposing of oil-contaminated wastewaters, as well as treating other industrial wastewaters at the site. Cherokee Resources used the site as a waste oil processing facility. 7. In July 1991, a criminal investigation was conducted by the EPA Hazardous Waste Section, the EPA Criminal Investigation Division, the Office of the FBI, and 'several other state and local authorities. A criminal search warrant was served to the owner of the site and a criminal investigation was conducted at the Cherokee Oil's 1201 Berryhill Road facility and a Cherokee Oil facility at 925 South Summit Avenue locations. 8. As a result of the criminal investigation, Keith Norland Eidson, Gene Wesley Hartsell and Theodore Karl Glauser were indicted on charges of conspiracy to violate federal Clean Water Act regulations by illegally disposing of and otherwise handling wastewaters in violation of permit limitations. Affidavit for 1201 Berryhill Road Page2 9. In 1991, EPA determined the Summit Avenue location posed an imminent and substantial endangerment to public health, or welfare, or the environment. Between August 1991 and March 1993, the EPA Emergency Response and Removal Branch ("ERRB") conducted an extensive emergency removal action at the Cherokee Oil's 925 South Summit Avenue location. The Summit Avenue location was an unpermitted temporary storage facility operated by Cherokee Resources from August 1990 to August 1991. 10. EPA identified approximately 6,096 drums, 13 roll-off containers of contaminated soil, several tankers containing liquid waste and trailers containing drums stored at the Summit A venue site. The wastes stored at the Summit A venue location included polychlorinated biphenyls (PCB's), highly flammable solvents, cyanides, strong acids and bases, hazardous organic compounds and hazardous inorganic substances. 11. On June 29, 1994, Keith Norland Eidson and Gene Wesley Hartsell were convicted of conspiracy to violate federal Clean Water Act regulations. On October 17, 1994, Eidson and Hartsell were each sentenced to 51 months active imprisonment which they are currently serving at Seymour Johnson Air Force Base in Goldsboro, North Carolina. 12. Cherokee also used the Berryhill Road site as an unpermitted temporary storage facility housing drums, above-ground tanks, underground tanks, vats, tanker trailers and roll-offs containing hazardous substances, including polychlorinated biphenyls, flammable solids and liquids, strong acids and bases, hazardous organic compounds, hazardous inorganic compounds, waste oil and sludges. 13. Many of the 2,856 drums found at the site were stacked both inside and outside the warehouse with incompatible waste types stored adjacent to each other. A number of containers had corroded causing the contents to leak onto the floor of the warehouse and to the surface of the soil surrounding the warehouse. A large volume of free- standing oily liquid and sludge covered the surface soils within three diked basin areas on the site. In September 1994, EPA determined the 1201 Berryhill Road site posed an imminent and substantial endangerment to public health, or welfare, or the environment. 14. Between November 1994 and December 1995, EPA-ERRB conducted a second extensive emergency removal action at Cherokee Oil's 1201 Berryhill Road facility to remove the imminent threat. Affidavit for 1201 Berryhill Road Page3 15. In 1990, Mecklenburg County Department of Environmental Protection videotaped a release of an oily material leaving the site onto a neighboring property at Suburban Propane. The historic releases may have resulted in actual or potential exposure of workers to hazardous substances. 16. The overland runoff release was intercepted by three storm sewer manholes where it was directed south underground to an outlet on an unnamed tributary of Stewarts Creek ("UT"). The UT directs the runoff east to Stewarts Creek. Stewarts Creek is reportedly used for recreational fishing. The historic release may pose an actual or potential exposure to hazardous substances by nearby animals or food chain species and/or human beings. 17. Samples collected by EPA during the removal action demonstrate residual soil contamination at the site. Substances identified in soil samples from the site which are hazardous pursuant to the Comprehensive Environmental Response, Compensation and Liability Act ("CERCLA"), 42 U.S.C.§ 9601 et seq., include acetone, benzene, 2- butanone, 1,1-dichloroethane, ethylbenzene, 4-methyl-2-pentanone, tetrachloroethene, toluene, xylenes and bis (2-ethylhexyl) phthalate. Sampling of materials found stored at the site identified additional CERCLA hazardous substances including polychlorinated biphenyls and waste oils containing metals. However, additional samples need to be collected to confirm their presence in soils at the site. Releases from the site pose a potential threat to humans and/or food chain species. 18. On Tuesday, January 30, 1996, I contacted Gene Wesley Hartsell in an attempt to gain access to the site for the purpose of collecting environmental samples. Mr. Hartsell stated that before he allows anyone to enter his property, he wants to inspect the property following EPA's removal action. He stated that he would be willing to allow us to collect soil samples after he gets out of prison. When I asked him for a specific time, Mr. Hartsell responded that his conviction was under appeal and that he could be released as soon as Friday, February 2, 1996 or as late as August 1998. 19. I asked Mr. Hartsell if he could have a representative meet us at the site to observe the sampling event. Mr. Hartsell stated that he wants to have a representative at the site when any soil samples are taken from his property. We both agreed that he would attempt to locate a representative and that I would contact him on Tuesday, February 6, 1996 in order to discuss the sampling event. 20. I in fact telephoned Mr. Hartsell on February 6th, but was told by a Seymour Johnson official named Robin Woodard, who left the phone to tell Mr. Hartsell of my call, that Mr. Hartsell said that he would not speak to me, that his attorney had told him he does not have to assent to our going on the site, and that he will write me a Affidavit for 1201 Berryhill Road Page4 letter. Based on a call to the Fourth Circuit Court of Appeals on February 5th, oral argument on Mr. Hartsell's appeal was heard on February 2nd. 21. On February 9, 1996, I received a letter from Mr. Hartsell. In it, he requested copies of the statutes/regulations under which we seek access and a written explanation of my reasons for wanting access, argued there is no basis for entry, reiterated his position that access to the site should await his release from prison, and stated that he wants to be present should I request access from a judge. 22. On February 13, 1996, I complied with Mr. Hartsell's request for copies of relevant legal authorities and a written justification for access, but told him that, given the contamination cited in this affidavit, I would be going to Charlotte on March 6, 1996 to seek an administrative search warrant and sample the site. 23. Due to the hazardous nature of residual contamination remaining at the site, the potential threat posed by historic releases and the inability to coordinate the sampling event with Mr. Hartsell, the CERCLA Branch requests an administrative search warrant to collect additional environmental samples from the site as part of an environmental assessment of 1201 Berryhill Road. The samples will be used to determine the threat posed to human health and the environment from current or historic releases. The assessment will also be used to determine-the need for additional investigation under CERCLA and/or other legal authorities. Sworn and subscribed to before me. Date ' Douglas B. Moore V 811peFi;;; Court Judge $/",f'(C/ I' ,_. I I I I I I I .ft I I I I I I ,.. I I Appendix B-1 Tables for Non-Radioactive Hazardous Substances Page B-64 SCDM Data Version: JUN96 19 AUG 96 Substance Name Acenaphthene Acenaphthylene Acetaldehyde Acetone Acetonitri le Acctophcnonc Acetyl-2-thiourea, 1- Acrolein Acrylamide Acrylic acid Acrylonitri{e Adipic acid Aldicarb Aldrin Allyl alcohol Al lyl chloride** AllXllinum Aluminum phosphide Arrrnonia HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 000083-32-9 f4.7E+03! 000208-96-8 000075-07-0 000067-64-1 {["88'03*:) 000075-05-8 4.7E+02* 000098-86-2 7.8E+03* 000591-08-2 000107-02-8 l.6E+03* 000079-06-1 1.6E+01* 000079-10-7 3.9E+04* 000107-13-1 7.8E+01* 000124-04-9 000116-06-3 7.8E+01* 000309-00-2 2.3E+OO* 000107-18-6 3.9E+02* 000107-05-1 007429-90-5 020859-73-8 3.1E+01* 007664-41-7 7.6E+04* SOIL PATHi,JAY Cancer Risk Screen Cone (mg/kg) 1.4E-01* 1.2E+00* 3.BE-02* Indicates ** Indicates difference between previous version of chemical data ( ncw.ardous substance in current version of chemical JUN94) and current version of chemical data ( JUN96 ). data ( JUN96 ) . - - - - - - -- - -- - - -- --- -Page B-65 SCDM ·Data 19 AUG 96 ---• Version: JUN96 Substance 1./ame Arrmonium pi crate Arrmoniun sulfamate Aniline Anthracene Antimony Arsenic Asbestos Atrazine Azinphos-ethyl Azinphos-methyl Aziridine Barium Barium cyanide Benz(a)anthracene Benzene Benzene carbonyl chloride Benzidine Benzo(a)pyrene - ---- - --HAZAR{? RA,,. SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 000131-74-8 007773-06-0 1.6E+04* 000062-53-3 000120-12-7 @:3E+0·4:) 007440-36-0 3.1E+01* 007440-38-2 2.3E+01* 001332-21-4 001912-24-9 2.7E+03* 002642-71-9 000086-50-0 000151-56-4 007440-39-3 l5:5E+03:) 000542-62-1 000056-55-3 000071-43-2 000098-88-4 000092-87-5 2.3E+02* 000050-32-8 * SOIL PATH\JAY Cancer Risk Screen Cone (mg/kg) 1. 1 E+02* [:;lEc01!.J 2. 9E+00"' (B~Bro:i!) [2~2E§)3 2.BE-03* !tBE-02*:J - * Indicates difference between previous version of chemical data ( JUN94 ) and current version of chemical data ( JUN96 ). ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). -- ----• Page B-66 SCDM Data Version: JUN96 19 AUG 96 Substance Name Benzo(b)fluoranthene Benzo(g,h,·; )perylene Benzo(k)fluoranthene Benzoic acid Benzonitrile Benzothiazole, 1,2,- Benzyl alcohol** Semyl chlu;-ide Beryllium Biphenyl, 1, 1- Bis (2-ethylhexyl) phthalate Bis(2-chloroethoxy)methane Bis(2-chloroethyl)ether 8is(2-chloroisopropyl)ether** Bis(chloromethyl)ether Boron Bromodichloromethane Bromomcthane Bromophenyt-phenylether, 4-** /- HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Number (mg/kg) 000205-99-2 000191-24-2 C:=> 000207-08-9 000065-85-0 3.1E+05* 000100-47-0 000095-16-9 000100-51-6 2.3E+04 000100-44-7 00744,0-41-7 3.9E+02* 000092-52-4 3.9E+03* 000117-81-7 1.6E+03* 000111-91-1 000111-44-4 039638-32-9 3.1E+03 000542-88-1 007440-42-8 T.0E+03* 000075-27-4 1.6E+03* 000074-83-9 1.1E+02* 000101-55-3 SOI l PATH\.JAY Cancer Risk Screen Cone (mg/kg) ~8F01*( c=:; 8.8E+00* 3.BE+OO* 1 .SE-01* 5.BE-01* 9.1E+00 2.9E-03* l.[-OE+01 *) Ino'icates ** I ndi cat es difference between previous version of chemical data ( new.~rdoUs substance in current version of chemical JUN94) and current version data C JUN96 ) . /·• of chemical data ( JUN96 ). - ----- - -- - - -- -- - - - -?age B-67 SCDM Data 19 AUG 96 - -• Version: JUN96 Subs cance Name Bromoxyni l Butadiene, 1,3- Butanol Butylbenzyl fX!thalate - Sutyric acid, 4-(2,4-dichlorophenoxy) Cadmium Calcium** CatJtan Carbary[ Carb,nole** CMbofuran Carbon,disulfide Carbnn tetrachloride Carbophenoth ion Ces i UTI Chloral Chlordane Chlordane, alpha-~* Chlordane, garrma-•* - --- - HAZARD RAt,. SYSTEM Hazardous Substance Benchmarks 376 Substarlces Reference Dose Screen Cone CAS Number (mg/kg) 001689-84-5 1.6E+03~ 000106-99-0 000071-36-3 7.8E+03* ____......-, 000085-68-7 11..6E:t04* 000094-82-6 6.3E+02* 007440-43-9~ 007440-70-2 000133-06·"2 1. 0E+04* 000063-25-2 7.8E+03* 000086-74-8 001563-66-2 3.9E+02* 000075-15-0 7.8E+03* 000056-23-5 5.SE+01* 000786-19-6 007440-46-2 000075-87-6 1.6E+02* 000057-74-9 4.7E+OO* 005103-71-9 005566-34-7 SOIL PATHWAY Cancer Risk Screen Cone (mg/kg) 1 .8E+02* 3.2E+01 4.9E+OO* 4.9E-01* - • Indicates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ) . ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). --- - --• Page B-68 SCDM Data Version: JUN96 19 AUG 96 Substance Name Chlorine cyanide Chloro-3-methylphenol, 4- Chloroaniline, p- Chlorobenzcnc Chlorobenzilate** Chloroform Ch l oromethane ChloromethYl methyl ether Chloromethyloxirane, 2- Chloronaphthalene, 2- Chlorophenol, 2- Chlorophenyl-phenyl ether, 4-** Chloroprcne** Chlorpyrifos Chromiun ChromiUTI(lll) Chromi un(VI) Chrysenc HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Ncmber (mg/kg) 000506-77-4 3.9E+03* 000059-50-7 1.6E+05* 000106-47-8 3.1E+02* 000108-90-7(176E+033 000510-15-6 1.6E+03 000067-66-3 7.8E+02* 000074-87-3 000107-30-2 000106-89-8 1.6E+02* 000091-58-7 6.3E+03* 000095-57-8 3.9E+02* 007005-72-3 000126-99-8 002921-88-2 2.3E+02* 007440-47-3 3:-9E+o23 016065-83-1 7.8E+04* 018540-29-9 3.9E+02* 000218-01-9 SOIL PATH\.JAY Cancer Risk Screen Cone (mg/kg) 2.4E+OO (_1:0E+02".J 4.9E+01* 6.SE+01* * Indicates difference between previous version of chemical data ( JUN94 } and current version of chemical data ( .. Indicates new .:rdous substance in current version of chemical data ( JUN96 )_ ·• -- - -- -- -- - - - JUN96 ). - -- - - --• Page 8-69 SCDM D;:ita Version: 19 AUG 96 Substance Name Cobalt Copper Copper cyanide Counaphos Creosote Cresol, m- Cresol, o-** Crescl, p- Cumene Cyansn. ine Cyanid~ Cyanogen Cyanogen bromide Cyclohexane Cyclohexanone ;, ... -JUN96 Cyclotrimethylenetrinitriamine ODO ODE DDT - - ---- - -• HAZARD Rh. .,4G SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Number (mg/kg) 007440-48-4 007440·50·8 ~ 000544-92-3 3.9E+02* 000056·72·4 008001·58·9 000108-39-4 3.9E+03* 000095·48·7 3.9E+03 000106-44-5 3.9E+02* 000098-82-8 3.1E+03* 021725-46-2 1.6E+02* 000057-12-5 1.6E+03* 000460-19-5 3.1E+03* 000506-68-3 7.0E+03* 000110·82·7 000108·94·1 3.9E+05• 000072·54·8 000072-55·9 000050-29-3 3.9E+01* SOIL PATH\.JAY Cancer Risk Screen Cone (mg/kg) 7.6E-01* 5.8E+00* 2.7E+00* 1. 9E+00* 1. 9E+00* - * Indicates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ). ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). -- -- Page B-70 SCDM Data Version: JUN96 19 AUG 96 Substance Name DEF Di-n-butyl phthalate Di-n-octyl phthalate Dial late** Diazinon Di benz(,a, h )anth racene Di benzofuran Dibromo-3-chloropropane, 1,2- Dibromochloromethane Dibromoethane, 1,2- 0 l carrba Dichlorobenzene, 1,2- Dichlorobenzene, 1,3- Dichlorobenzene, 1,4- Dichtorobenzidine, 3,3- Dichlorodifluoromethane Dichloroethane, l, 1- Dichloroethane, 1,2- 0ic.hloroethylene, 1, 1- HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS NUOC>er (mg/kg) 000078·48-8 2.3E+OO* 000084-74-2 17..8E+03~ . 000117-84-ol1-=6E+03*) 002303-16·4 000053-70-3 000132-64·9 000096-12·8 000124-48-1 1.6E+03* 000106-93·4 001918-00-9 2.3E+03* 00009s-50-1 c.0E+o3•J 000541-73· 1 000106-46-7 000091-94-1 000075-71-8 1.6E+04* 000075-34-3 ~E+03j 000107-06-2 000075-35-4 7.0E+02* SOIL PATHWAY Cancer Risk Screen Cone (mg/kg) .. 1.0E+01 C878E::.Q29 4.6E-01* 7.6E+OO* 7.SE-03* 1.4E+OO* 1. 1 E+OO* Indicates .,,. Indicates difference bet~een previous version of chemical data ( ne-~rdous substance in current version of chemical JUN94 ) and current_&sion data C JUN96 ). ..11111 of chemical data ( JUN96 ). - -- -- - - - -- - --• -- -- -- -Page B-71 SCDM Data 19 AUG 96 - -• Version: JUN96 Substance !-lame Dichloroethylene, cis-1,2- - Dichloroethylene, trans-1,2- Dichlorophenol, 2,4- Dichlorophenoxyacetic acid, 2,4· Dichloropropane, 1,2- Dichloroprvpene, 1,3- Dichloropropene, cis-1_.3-** Dichloropropene, trans-:,3-** - ---- - - HAZARD RA,~ SYSTEM Hazardb°Gs' Substance Benchffiarks 376 Substances Reference Dose Screen Cone CAS NLKllber (mg/kg) 000156-59-2l7..8Et02Q 000156-60-5 1.6E+03* 000120-83-2 2.3E+02* 000094-75-7 7.8E+02* 000078-87-5 000542-75-6 2.3E+01* 010061-01-5 010061-02-6 SOIL PATH\./AY Cancer Risk Screen Cone {mg/kg) 9.4E+00* 3.6E+OO* Di ch l crvos 2. ZE+00 000062-73-7 3.9E+01* Dicofol Dieldrin Diethyl phthalate Diethylene glycol Diethylstibestrol** Diisopropylmethyl-phosphonate Dimethoate Dimethoxybenzidine, 3,3- Dimethyl phenol, 2,4- 000115-32-2 000060-57-1 3.9E+OO* 4.0E-02* 000084-66-2 6:3E•04*) 000111-46-6 000056-53-1 1.4E-04 001445-75-6 6.3E+03* 000060-51-5 1.6E+01* 000119-90-4 4.6E+01* 000105-67-9 1.6E+03* - • Indicates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ). ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). --- ---• Page 8-72 SCOH Data Version: JUN96 19 AUG 96 Substance Name Dimethyl phthalate Dimethyl sulfate Dimethytbenz(a)anthracene, 7, 12-** Dimethylbenzidine, 3,31 -** Dinitro-2-methylphenol, 4,6-** Dinitrobem:ene, 1,3- Dinitrophenol, 2,4- Dinitrotoluene, 2,4- Dinitrotoluene, 2,6- Dinoseb Dioxane, 1,4- Dioxathion Diphenylamine** Oiphenylhydrazine, 1,2- Diquat Di .~ut foton Diuron Endosulfan (I or Ii) Endosulfan sulfate HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber · (mg/kg) 000131-11-3 000077-78-1 000057-97-6 000119-93-7 000534-52-1 000099-65-0 000051-28-5 000121-'4-2 000606-20-2 000088-85· 7 000123-91-1 000078-34-2 000122-39-4 000122-66-7 000085-00-7 000298-04-4 000330-54-1 000115-29-7 001031-07-8 7.SE-+-00* 1 . 6E-+02* 1 .6E+02* 7.SE-+-01* 7 .BE-+-01* 2.0E-+03 1. 7E-+-02* 3.lE-+-00* 1.6E+02* 4.7E-+02* SOIL PATH\.JAY Cancer Risk Screen Cone (mg/kg) 7.0E-02 9.4E-01* 9.4E-01* 5.BE+0l* B.0E-01* * lndicat.es ** Indicates dif~ce between previ~us version of chemical data ( ne~~rdous substance 1n current version of chemical JUN94 ) and current .ion data ( JUN96 ) . .,- of chemical data ( JUN96 ). - - -- - - - - -- -- --- - -- - -·--• Page B-73 SCDM Data Version: JUN96 19 AUG 96 Substance Name Endothall Endrin Endrin aldehyde Endr in ketone** Ethion Ethyl acetate Ethyl benzene Ethyl chloride Ethyl ether Ethyl methacrylate** Ethyl methanesulfonate** Ethyldipropylthiocarbamat~, s- Ethylene glycol Ethylene glycol monoethyl ether Ethylene thiourea** Fenthion Ferrous sulfate Fluoranthene Fluorene -- ------• HAZARD RA1, .. ,G SYSTEM Hazardous Substance Benchmarks 376 Substances SOIL PATHl,./AY - Reference Dose Screen Cone CAS Number (mg/kg) Cancer Risk Screen Cone (mg/kg) 000145-73-3 1.6E+03* 000072·20·8 2.3E+01* 007421-93·4 053494·70·5 000563·12·2 3.9E+01• 000141 · 78· 6 l770E+04 *) 000100-41-4 7.8E+03* 000075·00·3 000060-29-7 1.6E+04* 000097-63-2 7.0E+03 000062-50·0 000759-94-4 2.0E+03* 000107-21·1 1.6E+0S* 000110-80-5 3.1E+04* 000096·45·7 6.3E+OO 000055·38·9 007720·78·7 000206·44 · 0 l3 .. 1E+03'' 000086· 73· 7 @71E+O~•- 5.BE+OO - • Indicates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ). ** !ndicates new hazardous·substance in current version of chemical data ( JUN96 ). -- - - --• Page B-74 SCOM Data Version: JUN96 19 AUG 96 Substance Name Fluorine Forma tdehyde Formic acid Furan Furfural Gl ye i dyta ldehyde Heptachlor Heptachlor epoxide Heptachlorinated dibenzo-p-dioxin, 1,2,3 Heptachlorinated dibenzofuran, 1,2,3,4,6 Heptachlorinated dibenzofuran, 1,2,3,4,6 Hexabromobenzene Hexachlorinated dibenzo-p-dioxin, 1,2,3, Hexachlorinated dibenzo p-dioxin, 1,2,3, Hexachlorinated dibenzo p-dioxin, 1,2,3, Hc:-:achlorinated dibenzofuran, 1,2,3,4,7, Hexachlorinated dibenzofuran, 1,2,3,6,7, Hexachlorinated dibenzofuran, 1,2,3,7,8, HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 007782-41-4 4.7E+03* 000050·00·0 1.6E+04* 000064· 18·6 1. 6E+05* 000110·00·9 7.8E+01* 000098·01 · 1 2.3E+02* 000765·34·4 3.1E+01* 000076·44·8 3.9E+01* 001024·57·3 1.0E+OO* 035822·46·9 067562·39·4 055673·89· 7 000087·82·1 1.6E+02* 039227·28·6 057653·85·7 019408·74·3 070648·26·9 057117·44·9 072918·21·9 SOIL PATHl,IAY Cancer Risk Screen Cone (mg/kg) 1.4E-01* 7.0E-02* 4. OE-04* 4.0E-04* 4.0E-05* 1.0E-04* 1.0E-04* 4.0E-05* 4.0E-05* 4.0E-05* • I ndi cat es ** i ndi cat es difference between previous version of chemical data ( ne·•:rdous substance in current version of chemical JUM94 ) and current .sion data ( JUN96 ) . ,,- of chemical data ( JUN96 ). -- -- - -- - ---- -- - - - - --· • :>age B-75 SCDM Data Version: JUN96 19 AUG 96 Substance Name - Hexachlcrinated dibenzofuran, 2,3,4,6,7, Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclohexane, alpha- Hexachlorocyclohexane, ~ta- Hexachlurocyclohexane, delta- Hexachlorocyclopentcdiene Hexachloroethane Hexach lorophe;1e Hexane Hexanone, 2-** Hydrazine Hydrochloric acid Hydrogen cyanide Hydrogen sulfide lr.deno(1,2,3-cd)pyrene loxyni L Iron Isobutanot ---- - ---• HAZARD RAt,,,. ,.,.; SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Number (mg/kg) 060851-34-5 000118-74-1 6.3E+01* 000087-68-3 1.6E+01* 000319-84-6 000319-85-7 000319-86-8 000077-47-4 5.5E+02* 0000(,7-72-1 '7.8E+01* 000070-30-/i 2.3E+01* 000110-54 3 4.7E-+-03* 000591-78-6 c:;:::::, 000302-01-2 007647-01-0. 000074-90-8 1.6E+03* 007783-06-4 2.3E+02* 000193'39-5 001689-83-4 007439-89-6 000078-83-1 2.3E+04* SOIL PATHw'AY Cancer Risk Screen Cone (mg/kg) 4.0E-05* 4.0E-01* 8.2E+00* 1.0E-01* 3.6E-01* 4.6E+01* ~ 2. 1E·01* - • Indicates difference between previous vers_ion of chemical data ( JUN94 ) and current version of chemical data ( JUN96 ). ** Indicates new hazardous substance in current version of chemical data·( JUN96 ). -- --·--• Page B-76 SCDM Data Version: JUN96 19 AUG 96 Substance Name lsophorone KENZENE** Keporle Lead Lindane Magnesium Malathion Maleic anhydride Maleic hydrazide Manganese Mercury Methacrylonitrile Methanol Methomyl Hethoxychlor Methyl chlorocarbonate Methyl ethyl ketone Methyl i sobutyl ketone Methyl methacrylate • I ndi cat es difference between previous ** I ndi cat es new.rdou·s substance in -- --version current - HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS NLrrber (mg/kg) 000078-59-1 1.6E+04* 00000000000 000143-50-0 007439-92-1 ~ 000058-89-9 2.3E+01* 007439-95-4 000121-75-5 1.6E+03* 000108-31-6 7.8E+03* 000123-33-1 3.9E+04* 007439-96-5 \1-:-1E•O~~ 007439-97-9-2c3E+01*) 000126-98-7 7.BE+OO* 000067-56-1 3.9E+04* 016752-77-5 2.0E+03* 000072-43-5 3.9E+02* 000079-22-1 000078-93-3[4 . .7E+04:) 000108-10-1 6.3E+03* 000080·62-6 6.3E+03* SOIL PATH\.JAY Cancer Risk Screen Cone (mg/kg) 6. 7E+02* · 4.9E-01* of chemical data ( JUN94 ) and current·-ion of chemical data ( JUN96 ). version of chemical data ( JUN96 ) . _,,..... --- - -- - - --• ------ -Page B-77 SCOH Data 19 AUG 96 - -• Version: JUN96 Substance Name Methylcholanthrene, 3-** - Methylene bis (2-chloroaniline), 4,4- Methylene bromide** Methylene chloride Methylenediphenyl diisocyanate, 4,4- Methylnaphthalene, 2- Metribuzin Mi rex Molyoclenun** N-nitroso-di-n-propylamine** N-nitrosopiperidine** Naphthalene Naph thyl amine** !-Jickel Nitric acid Nitric oxide Nitroaniline, 2-** Nitroaniline, 3-** - ---- - --HAZARD RAI\ .• SYSTEM • Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 000056-49-5 000101-14-4 5.SE+01* 000074-95-3 000075-09-2 4. 7E+03* 000101-68-8 000091-57-6 c::::, 021087-64-9 2.0E+03* 002385-85-5 1.6E+01* 007439-98-7 3. 9E+02 000621-64-7 000100-75-4 000091-20-3 ~~1E+03:) 000091-59-8 007440-02-0 Qt,o:i;> 007697-37-2 010102-43-?. 000088-74-4 000099-09-2 • SOIL PATH\./AY Cancer Risk Screen Cone Cmg/kg) 4.9E+00* c:=::, • 9. 1E-02 - • lndicates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ) . ** Indicates"new_hazardous substance in current version of chemical data ( JUN96 ). --- -- Page B-78 SCOM Data Version: JUN96 19 AUG 96 Substance Name Nitroani!ine, p- Nitrobcnzene Nitrogen dioxide Nitroglycerine Nitrophenol, 2-** Nitrophenol, 4- Nitropropane, 2-** Nitroso-di-n-butylamine, N- Nitroso-di-n-methylurethane, N- Nitrosodiethanolamine, N- Nitrosodiethylamine, N- Nitrosodimethylamine, N- Nitrosodiphenylamine, N- Nitros001ethylethylamine** Nitrosopyrrolidine, N- Nitrotoluene, 4- 0ctarnethylpyrophosphoramide** Oxybis (1-chloropropane), 2,3'-** Parathion, ethyl- HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 000100-01-6 000098-95-3 3.9E+01• 010102-44-0 000055-63-0 000088-75 -5 000100-02-7 000079-46-9 000924-16-3 000615-53-2 001116-54-7 000055-18-5 000062-75-9 000086-30-6 010595-95-6 000930-55-2 000099-99-0 000152-16-9 000108-60-1 000056-38-2 7.8E+02* 1. 6E+02 4. 7E+02* • SOIL PATHWAY Cancer Risk Screen Cone (mg/kg) 1.2E-01* 2.3E-01* 4.3E-03* 1.3E-02* 1. 3E+02* 2.9E-02 3.0E-01* • Indicates ** I ndi cat es diff~rence.bet~een previous version of chemical data ( ne-~~rdous substance in current version of chemical JUN94) and current version of chemical data ( JUN96 ). data ( JU,N96 ) . .• - -- -- ------ - - -- -- - -Page B-79 SCDM Data 19 AUG 96 - -• Version: JUN96 Substance Name Parathion n~thyl- PCBs - - Pentachlorinated dibenzo-p-dioxin, 1,2,3 Pentachlorinated dibenzofuran, 1,2,3,7,8 Pentachlorinated dibenzofuran, 2,3,4,7,8 P~ntachlorobcnzene Pentachloroethane Pentachloronitrobenzene Pentachlorophenol Phenanthrene !='henol Phenyl ~ul fide Phenylenediamine, m-** Phenylmercuric. acetate Phorate Phosgene Phosphamidon Phosphine Phosphonodithioic acid, phenyl-a-ethyl-a - - - - -- - HAZARD RA, .• SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Number· (mg/kg) 000298-00·0 2.0E+01* 001336-36-3 1.6E+OO* 040321-76-4 109719-77-9 057117-41-6 000608-93-5 6.3E+01* 000076-01 -7 000082-68-8 2.3E+02* 000087-86-5 2.3E+03* 000085-01-8 c . . . , 000108·95·2 4.7E+04* 000139-66-2 000108-45-2 4.7E+02 000062-38-4 6.3E+OO* 000298-02-2 1 ~6E+01* 000075-44-5 013171-21-6 007803-51-2 2.3E+01* 002104-64-5 7.8E-01* SOIL PATH\.JAY Cancer Risk Screen Cone Cmg/kg) {iiJE'02*::) 8.0E-06*. 8.0E·05* 8.0E-06* 2.SE+OO* 5.3E+OO* - • Indicates difference between previous version of chemical data C JUN94 ) and current version of chemical data C JUN96 ) . ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). -- -- --• Page B-80 SCDM Data Version: JUN96 19 AUG 96 Substance Name Phosphoric acid P~osphorous (elemental) Phthalic anhydride Plutoniun Polychlor}nated triphenyl Potassiun** Potassiu-n silver cyanide Pronamide Pyrene Pyridine Ouinol ine Radium Radon Resorcinol Ronnel Sairole** SeleniLXTI Selenourea HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 007664·38·2 007723-14-0 1.6E+00* 000085-44-9 1.6E+OS* 007440-07·5 012642·23-8 007440-09-7 000506-61-6 1.6E+04* 000129·00·0 1273E+03*:::i 000110-86-1 7.BE+01* 000091·22·5 007440-14-4 010043·92·2 000108-46·3 000299-84-3 3.9E+03* 000094·59·7 . -------007782·49·2 G-,.9E+02* 000630·10·4 3.9E+02* SOIL PATH~AY Cancer Risk Screen Cone (mg/kg) * Indicates ** Indicates difference between previous version of chemical data ( ne~.rdous substance in current version of chemical JUN94) anc:!'current version data ( JUN96 ) . ., -· of chemical data { JUN96 ). - -- - ---- ----- --- - -- -• Page B-81 SCOH Data 19 AUG 96 Version: JUN96 substance Name Silver Silver Cyanide Sodiun Strontiur1 Strychnine Styrene Sulfuric acid TB, 2,4,5- TCDO Tetrachlorobenzene, 1,2,4,5- Tetrachlorodibenzofuran, 2,3, 7,8- Tetrachloroethane, 1,1,1,2- Tetrachloroethane, 1,·1,2,2- Tetrachloroethylene Tetrachlorophenol, 2,3,4,6- Tetraethyl lead Tetraethyldithiopyrophosphate T et rahydrof uran Th£il l i UTI ----··---------- - --HAZARD RAh,. SYSTEM HazardOLis Substance Benchma·r_ks 376 Substances Reference Dose Screen Cone CAS Number (mg/kg) ---------------007440 -22 -4 ~02!1 000506-64-9 7.8E+03* 007440-23-5 007440-24-6 4.7E+04* 000057-24-9 2.3E+01* 000100-42-5 1.6E+04* 007664-93-9 000093-80-1 001746-01-6 000095·94-3 2.3E+01* 051207-31-9 000630-20-6 2.3E+03* 000079-34-5 000127-18-4 7.8E+02* 000058-90-2 2.3E+03* 000078-00-2 7.BE-03* 003689-24-5 3.9E+01* 000109-99-9 007440-28·0 SOIL PATHw'AY Cancer Risk Screen Cone (mg/kg) 4.0E-06* 4.0E-05* 2.5E+01* 3.2E+00* - * Indicates difference between previous version of chemi~al .data ( JUN94) and current version of.chemical data ( JUN96 ). ** Indicates new hazardous substance in current version of chemical data ( JUN96 ). --- -- Page B-82 SCOH Data Version: JUN96 19 AUG 96 Substance Name Thiourea Thi ram Toluene Toluene di isocyanate Toluenediamine, 2,4-** Toluidine, o-** Toluidine, p-** Toxaphene TP, 2,4,5- Tribromomethane Trichloro-1,2,2-Trifluoroethane, 1,1,2- Trichlorobenz.ene, 1,2,4- Trichloroethane, 1, 1, 1- Trichloroethane, 1, 1 ,2- Trichloroethylcne Trichlorofluoromethane Trichlorophenol, 2,3,5- Trichlorophenol, 2,3,6- ~ :-ichlorophenol, 2,4,5- HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose Screen Cone CAS Nunber (mg/kg) 000062-56-6 000137-26-8 3.9E+02* 000108-88-3 c.1 .• 6E:tO!+!l 000584-84-9 000095-80-7 000095-53-4 000106-49-0 008001-35-2 000093-72-1 6.3E+02* 000075-25-2 1.6E+03* 000076-13-1 2.3E+06* 000120-82-1 7 .8E+02* 000071-55-6 c? 000079-00-5 3.1E+02* 000079-01-6 000075-69-4 2.3E+04* 000933-78-8 000933-75-5 000095-95-4 7 .8E+03* SOIL PATHY'AY Cancer Risk Screen Cone (mg/kg) 2.0E-01 3.4E+00 5.BE-01* 8. 1E+01* C2:::) t1-;"1E+0'i°') L5 .. 8E+o.12! Indicates ** !ndicates difference between previous version of chemical data ( n.~ardous substance in current version of chemical JUN94) and current version of chemical data ( JUN96 ). data ( JUN96 ). ---- - -- --- - - --- --- -Page B-83 SCDM Data 19 AUG 96 Version: JUN96 Substance Name· Trichlorophenol, 2,4,6- - Trichlorophenol, 3,4,5- Trichlorophenoxyacetic acid, 2,4,5· Trichloropropane, 1,2,3- Triethanolamine Triflurat in Trinitrobenzene, 1,3,5- T;initrotoluene Tris (2,3-dibrc,mopropyl) phos~1ate VanadiUTI Vanadiun pentoxide Vinyl acetate Vinyl chloride \.Jarfarin Xylene, m- Xylene, o- Xylene, p- Zinc -- - ------HAZARD RAN. SYSTEM Hazardous Substance Benchmarks ·376 Substances SOIL PATHWAY - Reference Dose Screen Cone CAS Nunber (mg/kg) Cancer R·isk Screen Cone (mg/kg) 0000BB-06-2 000609-19-B 000093-76-5 7.8E+02* 000096-1B-4 4. 7E+02* 000102-71-6 001582-09-8 5.9E+02* 000099-35-4 3.9E+OO* 000113-96-7 3.9E+01* 000126-72-7 007440-62-2 5.5E+02* 001314-62-1 7 .0E+02* 000108-05-4 7 .8E+04* 000075-01-4 000081-81-2 2.3E+01* 000108-38-3 (r:"6E+05*J 000095-47-6 :~6E+05*"""") 000106-42-3 007440-66-6 z."3E+04*) 5 .8E+01* 9.1E-02* 8.3E+01* 2.1E+01* - * IndiCates difference between previous version of chemical data ( JUN94) and current version of chemical data ( JUN96 ). ** Intjicat_es new hazardous substance in current version of chemical data ( JUN96 ). -- - - - -• Page 8-84 SCDM Data Version: JUN96 19 AUG 96 Substance Name Zinc cyanide Zinc phosphide Zinc sulfate HAZARD RANKING SYSTEM Hazardous Substance Benchmarks 376 Substances Reference Dose screen Cone CAS Nunber (mg/kg) 000557-21-1 3.9E+03* 001314-84-7 2.3E+01* 007733-02-0 SOIL PATH\-JAY Cancer Risk Screen Cone (mg/kg) Indicates ** Indicates difference between previous version of chemical data ( n.zardous substance in current version of chemica( JUN94 ) and current version of chemical data ( JUN96 ). data ( JUN96 ). --- - - - -- - --- - - -- - -- I . ----· ·...-----·-·---. . ' ! I •• ) I ~ _, "?~£~iP ~ ~n .l: : __ : ' ' . ' . ' --···---·--------.. -····:. : __ : .. :~ ~. :_ : .. :~_i ~-WS~31-,-···: : :-;--_ j_-~----~-~~~--------------:- , ' i . . L. _: 58'-:-.. l:::.=======::::::.s1.=:::::===;:===:~. I I . -_: ·:·~-~----· - 1 I t ' )' : -:---. -: ·~-s-· _ _;_ ....... · .. '---·-'°······--. -------I I ► ' ' : l'l . 1. ---·-·-·----. -· . ··Ul -.. - 3 ' I I I I 0 I I 11,0' --------------'.. - ! ! j . t.. f'r;"'jcr h=e. .. - ' i I -,~AB~Y i-orm0019 Field Technical Services . '-'--_,--, cc,. r,;. -. .;v\_ c; v"E::G.,_ /\\) 151 4 2 8 Rev 08/BO O.H. MATERIALS CORP. P.O. BOX 551 " .J ::--, "? J • • FINDLAY, OH 40839-0551 419-423-3526 • -~~ ~ ' " PROJECT NAME ( \.v.m Kee rROJECT LOCATION jJ_c,Q brLA.~ > ~' o: \ lLa,L,.lt, Al,l. J9.JO'b ANALYSIS DESIRE-4 ~'/ // / //// PROJ. NO. !PROJECT CONTACT ·-{INDICATE ~ / / I h 9,17 .l~r I:: k' '/! .• ,/\ ,~:;~E~ T);t:N~: I ·7 V, SEPARATE ~ , / ½ ½ a: w CONTAINERS) / "}) ~ / , ,,/ a: z CLIENTS REPRESENTATIVE ! PRQJ~CT MANAGER/SUPERVISOR w-~ I // / / >+evt :>.ot.,a):,- a, ., j n /, • (,,f-.,1,,P :, c-. . ~ 1/~/ // ::,Z ci I --zO u z SAMPLE a. a, SAMPLE DESCRIPTION ~ '~ ~/~/~ :, :, <( 0 w NUMBER DATE TIME 0 a: (INCLUDE MATRIX ANO t u <:J POINT OF SAMPLE) REMARKS ,~-'-j-A ,,,; ~7. -1''r-,,l'.o,, c__ J_,_ 1 C O-LvS-)'> )50() I L/07... /I IX q, ),,~ · S' e '--~:,/ ti I ""f. ,f.,,. I -<J.., -z.. )( L 2 to -\J")->'-l ll-4-l4Lfo rx ~-f l,,o,'" '"·--4.1.'"·--c ,1 .. /-~oz., IX I)< ) .,,.. >,u .. < •., t ,',./ I} i _-"'f, . ,f. ;, -'J-, O'-· ll·'-1-rx .:;.·\-i •. r:,-.. L:o~ <.dL_/'t',/2'' 3 1w w<:.-:,c-/~~[\ lYoc. I~ X IX 9':, \--L,1J,. / ,,,,,,, ./+'1._ -<.1 _./._'" L" -<l - 4 :o-~ si n-i+ LJt,o 'x ' s : I I f ;, . J ,. ,, C J, /-'-l O'-' X x [X . o~ \'>,.. (, / A p f.. • '. ~ -!-l -,:_,f J,-' ·,-1-,.,' /l_~'-l-5 Co-v,1,:,,-"1,-, l'-l~ 'X <c. , .. I YoL )< x C>( "' Dr L ,i,..I., -p,_ 1: Ar., .. I l'.4...._ ,,I_) 1-'l,.:., 6 l/'i-1,,jt:..,-\4. /l·I.J :1s--~D rx " ~ _, I-J_.I t.<>'._) 11<"1.QJIL:JJ_ /-Y,-,__ [X 1-X -ilr IT' •, CT/, I -'b"~ 7 8 9 ' 10 •. I g ! ITEM TRANSFERS TRANSFERS REMARKS ! NUMBER REUNOU!SHEO UY ~LJ<t> h""'" T4 T rc:9,.,,,j_f ACCEPTED BY DATE TIME 1 01 -Ob I~ Lil,, reJ [)( tl-<j--no f'esew"i f"''J i)/c-/1, Cli> 1-5~;p(e4 fl l..f. {_ , 2 3 4 SAMP ll:~'llGNk:t.~ ' i r:EC-07-1995 17:34 FROM SAVf'.l--lNAH LABS TO 9'. 7043911!4~ P.02 I s L SAVANNAH LABORATORIES 5 ENVIRONMENTAL SERVIC", INC . .. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S5-56748 05 DiC 95 07 DEC 95 !~. John Rhyne OHM Corporacion 5335 Triangle Pkwy. Suite 450 Norcroaa, GA 30092 CC: Jack Kilbarger P.EPORT OF P.ESOLTS Received: Reporud: Purchase Order: 1016477 Project: 16817 Cherokee Oil Sampled By: ~lient OATE/ I I I I I I LOG NO SAMPLE DESCRIPT.ON, SOLID OR SEMISOLID SAMPLES TIME SAMPLED I 56748·1 SPH-:l S6748·3 56748·4 56748·5 PARAMETER \\., CO-WS-33 '\'•''---,. co -ws -J 1. ' \ \\ -' CO-WS-35 \\ " ~ CO-WS-36 " '·' A. co-;.,,5. 37 1,2-Dictloropropane, ug/kg dw 567<6·1 - trans-1,3-Dichloropropene, ug/kg dw · Trichloroethene, ug/kg ctw <5.7 <5.7 <5.7 <5.7 <5.7 <5.7 <S.7 <5.7 I I I I I I Dibromochloromethane, ug/kg dw 1.1.2-Trichloroethane, ug/kg dw Benzene, ug/kg dw cis-1,3-Dichloropropene, ug/kg dw srcmo:o:nn, ug/Xg aw 2-Hexanone, ug/kg d" 4 ... MAt:hyl .. ,. -.('lP.nt.~nc"'lnP (MIBK), ug/kg dw Tetrachloroethene, ug/kg dw Toluene, ug/kg dw Chlorobenzena, ug/kg dw ~~hylbQn2QnG, ug/r.g dw Sty=ene, ug/kg dw Xylwnes, ug/kg dw surrogaee Toluene•d8 Surrogate· 4-Branofluoroben,ene <28 c=-?.i:I llj <5.7 ~--;-9~. <5.7 e.•""\ SG ,-· 95 t Currogata • 1,~-Di~hloroethano-d• ~5 \ Date Analyied 12.06.9S -. I <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <6.0 <3 C <ln <6.0 <6.0 <6.Q ,. '. 0 <6.0 26 96't) 100 % 102 ' 1.:l.06.95 l:l-04-95/1500 12-04-~5/lHO 12-04·95/l420 12-04-95/1450 12 • 04 • 95/1430 <750 <6 .l <750 <6.l <750 <: 6. 1 <750 <6.l <750 <6.l <750 <6.1 <750 <6.l <7oU <Ii. l <3800 <30 <3800 <30 <750 <6.l <750 <6.1 <750 <6.1 ~iSO .-:, .1 <750 <6.1 <750 <6.l 100 \-1:0 \- 99 \-U2 t 88 ', l.::. 6 ., l:l.07.95 12.07.95 5G?49 5 <7.5 <7.5 c-.7.5 <7.S <7.5 <7.5 <7.5 <7.5 <37 d7 <7.5 <7.5 <7.5 <.7. !i <7.5 <7.S 98 \- 94 t g' ., 12.07.95 -. -.. --. -.. --...... -----. 1 Llboratorl .. In S•v•nnah, GA • Ta/lahaeeoo, ;:L • Tampa, l'L • o .. rlleld Beach, FL • Mobile, AL• New Orleans, LA • CEC -07-1 995 : 7: 35 FROM SR<J~NAH LABS TD 917043911147 P.03 I S. L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC . .. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (91.2) 352-0165 LOG NO: S5·5~748 Received: 05 DEC 95 Reported: 07 DEC 95 l'.r. John R.'.yne CHM Corporation 5335 Triangle Pk"Y, Suite 4S0 Norcro~s, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS rurch~3c Order: 1016177 Project: 16817 Cherokee Oil Sampled l'ly: Cl~er.c Pac;e 3 =! I I I I I I LCG N'O SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TntE SJUo!PLED 56748·1 CO-WS·33 56748-2 CO-WS-34 56749-3 CO-WS-35 56749·4 CO•WS-36 56748·5 CO-WS-37 I TCL Sernivolatiles (8270) ,. Phenol, ug/kg dw bis(2·Chloroethyl)ether, ug/kg ~-Chlorophcnol, ug/kg dw I I I I I 1,3-Dichlorobenzene, ug/:Cg dw 1,4-Dichloroben•ene, ug/:Cg dw 1,2-Dichlorobenzene, ug/:Cg dw 2-Methylphenol (o-cresol), · uS'/kg dw 2,2'-0xybia(l·Chloropropane ) (b:.s•2•chloroisoPrOPyl ether), ug/kg dw 3-Methylphenol/4-Methylphen ol(m&p•crtsol), ug/kg ctv N·Nitroso•di-n-propylarnine, ug/kg dw Hexachlcroetha.~e, ug/kg dw Nitrcbenzene, ug/kg dw lsopnorone, ug/kg ctv 2-Nitro~he~ol, ug/kg dw 5048-1 <380 dw <380 <380 <380 '.4l_0; · <380 <380 <380 <380 <380 <380 <380 <380 <380 56746-2 <400 <400 <400 <400 <400 <400 <400 <400 <.400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 .. -----.... -----..... -... - ................................ 12-04-95/1500 12-04-95/1440 12-04-95/1420 12-04-95/1450 12-04-95/,.430 d00· <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <4 DO <400 <430 <430 <130 <430 <430 <430 <430 <430 d3C <43C <430 <43C <430 <430 ................. . -.... ---.. -- 1 Laboratorl•s In S..v11nnah, QA • Tal/11h1<ue11, FL • T11mp11, FL • 0.•rll•ld S..Ch, FL • Mob/IA .. AL• N111w Orl••n•. LA CEC -07-1995 1 7: 35 FROM SAVi=N~IAH L.ABS TO 9:7043911147 P.04 I s L SAVANNAH LABORATORIES & !NVIRONMENTAL SU/VICES. INC . .. 5102_ LaRoche Avenue• Savannah. GA 31404 • (912) 354•7858 • Fax (912) 352-0165 Lex:; NO: S5•!6748 Received: OS DEC 95 Reported: 07 DSC 95 Mr. Jchn Rhyr:" OK'M Corpor~tion 5335 Triangle Pkwy. Suite 450 l'lorcrogg, GA 30092 Purcho.g<> Or<lg,:-: lOl-4 77 I I I I I I CC: Jack Kilbarger ?reject: 16817 Cherokee Oil S""'!'lCd By: Client REPORT CF ;tESULTS LOG l'lO 56748·1 56748•2 56748·3 56748·4 56748-5 SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES CC·WS·33 CO-WS·34 CO·WS·35 CO·WS·36 CC•WS·37 I :P ARAMETE?. 56748-1 56748•2 56748•3 2,4•Dimethylphenol, ug/kg dw l:)is (~ ·<:.'hloroecho,cy) ir,etnane, .. ug/kg dw ... 2,4•Dic:hlorophA:,n,, ug/kg c1w I I I I l,2,4·Trichlorobenzene, ug/kg dw Naphthal~ne, ug/kg dw 4•Chloroaniline, ug/kg dv Hexachlorobutadiene, ug/kg dw 4•Chloro•3-methylphGnol, ug/kg dw 2-Methylnaphthalene, ug/kg dw Hexachlorocyc:lopentadiene, ug/kg dw 2,4,6·Trichlorophenol, ug/kg dw 2,1,5-T~ichlorophc~ol, ug/kg dw 2·Chloronaphthalene, ug/kg dw 2·Nitro-.~iline, ug/kg dw Dimethylphthalate, ug/kg dw Acenaphthylene, ug/kg dw 3-Ni tro..,.,ilir:i~, u9/k!r1' r.lw I Acanaphthenw, ug/kg dw ···---··············-····-··· I .. •• <:380 <380 d80 <380 <3 80 <750 <380 <3 90 ~o <380 <380 ._Jao <380 <1900 <380 <3 80 <HOO <380 <400 <400 <400 <400 ...;400 .-:400 <400 <400 <400 <400 <800 <800 <400 <400 dOO <100 t.-fo-::> <400 <400 <400 <400 <400 ..;_-too ...:4:00 <400 <400 <2000 <2000 <400 <400 <400 <400 <2000 <lOOO <400 <400 -··--------·-----.--- DATE/ T.IME SAMP:..zo l2·04·95/l5CO 12-04-95/1440 12·04·95/1420 12-04-95/1450 l.2.·04·95/J.4.!0 56743•4 <400 <400 .-:4 00 <400 <400 <800 <400 <100 <400 <400 <400 ..;4;00 <400 <2100 <400 <400 <2100 <400 Page 4 56748•5 <430 <430 .-:430 <430 <430 <860 <430 <130 <430 <430 <430 ...:430 <430 <2200 <430 <430 <2200 <430 -..... --.. --... .. --....... - 1 Laboratorlea In S1nann11h, GA • Tallah11ue, FL • Tampa, FL• DHrlltld S.ach, FL • Mobile. ~L • New Or/eana, LA CEC-07-1995 :7:36 FROM SAIJeNNAH LABS TO 9: 7043911147 P.05 I SL SAVANNAH LABORATORIES ,1, ENVIRONMENTAL SERVICES, INC. ,_ 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354•7858 • Fax (912) 352-0165 LOG NO: S5·56748 Received: 05 DEC 95 RQported: 07 DEC SS I I I I I I I I I I I I I Mr. John R.".lyne OHM Co,:pox-ation 5335 Triangle Pkwy. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS Project: 16817 Cherokee Oil Sac,pled Hy: ~lie~t DATE/ LCG ~O SAMPLE DESCRI'TION, SOLID OR SEMISOLID SA.."!PLES TIME SAMPLED 56743-1 56749-2 56743-3 56749·4 56743-5 CO-WS-33 CO-WS-l4 CO-WS-35 CO-WS-36 CO-WS-37 ---------------------··----------------·--··--····- 2,4-Dinitrophenol, ug/kg dw 4-Nitrnphenol, ug/kg dw otbenao!ur11.n, ug/kg dw J,1-0initrotoluQne, ug/kg dw 2,6-Dinitrotoluene, ug/kg dw Die~hylphthalate, ug/kg dw 4-Chlorophenylphenyl ether, ug/kg dw Fluo~ene, u~/k~ uw· 4-Ni troaniline, ug/kg dw 4,6-oinitro-2-methylphenol. ug/kg dw N-Nitrosodiphenylamine/Diph enylamine, ug/kg aw 4-Bromophenyl phenyl ether, ug/kg dw Hexachlorobenzene, ug/kg dw Pen~ac::hloropr.enol, ug/kg dw ~henantllrene, ug/~g dw klth=acene, ug/kg dw -------------------- <1900 <iooo <1900 <2000 d80 <400 .;380 ,100 <380 <400 <380 <400 <380 <400 <380 <iOO <1900 <2000 <1900 <2000 <380 <400 <380 <400 <380 <400 <l900 <2COO 189.0.> • <400 <380 <400 56748·3 ---------- <2000 <2000 <400 ,'600 <400 c400 c400 <400 <2000 <2000 <400 c400 <400 <2000 <400 <400 ---------- 12·04·95/lSOO 12-o,-~s/1uo 12·04-95/1420 12·04 ·9S/1450 12-04-95/1430 S6748·4 SG?H-S -------------------- <2100 <2200 <2100 <2200 <400 <430 <400 <130 <400 <430 <400 <430 <400 <430 c,;00 <430 <2100 c2200 <2100 <2200 <400 <430 <400 <430 <400 <430 <2100 <2200 <400 <BO <400 <430 -------------------- 1 Laboratories In Savannah, GA • TallahaM:ott, FL • T11mp11, R • D<><>rfl•ld B<>aeh, FL • Mobil•, ~ t • N•w Ori••"•, LA CEC-0'7-l ':!'35 : 7: 37 FROM SRV!=NNAH LRBS TO 9: 7134391114? 1 s·L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. .. 5102 LaRcx:he Avenue• Sevannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S5·56H8 Roceived: 03 DE~ 95 Reported: 07 DE: 95 ' ' Mr. Joh.!: Rhyne OJ-CM C'r,rporat:ion 5335 Triangl• Pkwy. Suita 450 Norcross, GA 3009:. I I I I CC: Jack Kilba:rger Project: 16817 C:ierokee Ocl Ce.mpled Oy; Client REPORT OF RESIJLTS I I I LOG NO 56748·1 56748-2 56748-3 56748•4 56743·5 SA.'!PLE DESCRIPTION, SOLID OR s=soLID SAIIPLES CO-WS-33 CO-WS-34 CC•WS-35 CC•WS-36 CO·WS-37 PARAMETS1' Di•n·butyl?hthalate, ug/kg dw ,·1uoranthene, ug/Kg aw .A?yrene, ug/kg dw 56748·1 <400 <400 <400 <400 <800 <400 DATE/ TIME SAM?LE:, 12-04-95/1500 l2·N·95/l440 12-04-95/1420 12-04-95/1450 l2·04·95/H30 <400 <400 <400 <400 <800 <400 .... llueylhAn>.ylphth~ht,;,, ucr/k(I d"' 3,3'-Dichlorobenzidine, ug/kg dw Beru:o(a)ant:hracene, ug/kg dw bia(,•Bthylhexyl)phthalate, I <3B0 (8201 • rEioo) . (TT"o) • <750 <380 15600) · <,00 <400 <400 .-:<.00 <800 <400 .~1'4001 2 3 0.0.:) <1700 I I I I I ug/kg dw Chry~ono, ug/kg dw Di•n-octylphthalate, ug/kg dw Benzo(b).fl'.lo:anthene, ug/kg dw Benzo(k)!boranthene, ug/kg dw Benzo(a)pyrene, ug/kg dw Indono(l,2,J-cd)pyrene, ug/kg aw Dibenzo(a,h)anthracene, ug/kg dw Benzo(g,h,i)pecylene, ug/kg dw Carba:ole, ug/kg dw Surrogate· Phenol dS Surroga~e ,. l-~lu~zvphenol Surrogate 2,4,6·Tribromophenol Surrogate Nitrobenzen~ • dS Surrogate 2-Pluorobiphenyl Surrogate Ter.:,henyl • dl4 1390)' <380 @Q>' <380 <380 <380 <380 <380 c380 92 t H ~ 79 t 79 t 105 t 74 t t>11.ce Extrae,:el!l Dat~ Analy~ed 12.05.95 1:..06.llS <·-4.00 <400 <400 <400 <400 <400 <400 <400 <400 77 \ 6 6 \- 65 t 240 It 66 % 60 t 12.05.95 U.06.95 <~00 <•oo <400 <400 <400 <400 <400 <400 <400 <400 <400 <100 <400 <400 <400 <400 <400 <400 75 t 66 t ~J ., 58 t S6 t 44 t ~o" 5, % 78 % 72 t 58 t 52 t lJ.05.95 12.05.~5 12.06.llS 12.06.95 -----------.. ---.. -. -- Pag~ 6 <430 <430 <430 <4JO <860 <430 cnoo " • .) 0 <430 <430 <430 <430 <430 <430 <430 <430 77 t Sl l 32 t ~4. 64 t 45 % U.05.95 12.06.95 Laboratories In S1V1nt111h, GA • Tal/1hUHe, FL• Tampa, FL • 0.•rflP/d Beach. n • Mobile. AL • New Or/111n1, LA 'I . \ :EC-07--1995 : 7: 38 FROM SAlJeNNAH LABS ii] 9:?043911147 P.07 I s L SAVANNAH LABORATORIES. & l!NY/l'IONMt:NTAL 3EIIVIC~, INC. 'es,02 LaRoche Avenue• Savannah. GA 31404 • (9 1 2) 354-7858 • F~x (>l1?) .,:'i7-01nA LOG NO: S5-56749 Rocoivad: Os DaC 9S Roport8d: 07 DEC 95 Mr. John R.hyn• OHM Corporation S335 Trianil8 PkW"/, SuitQ 450 Norcro~~, GA J009j CC: Jack Kilbarger REPORT OF REStJLTS Purchase Order: 1016477 Project: 16817 Cherokee Oil Sampled By: Cl:.ent • DATE/ I I I I I LCG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SJ\Ml'LES TIME SAMPLED I I 55748•1 CO·WS-33 SG740-J CO-WS•34 56748-3 CO•WS-35 56743-4 S6748-5 PARAMKTI:R. Arsenic CO·WS-36 CO·WS-37 -- Arsenic (6010), mg/kg dw Date Analyzed ,iarium (GQlO) I I Bar:.1.:.11 (60:o), mg/kg d" Drlt'.11'! An.t1ly't1:?d Cadmium (6010) Cadtiium (6010), Date Analyzed Chr0t1ium (6010) mg/kg dw Chromium (,010), mg/kg dv Date Analy•8d I Mercury Mercuri (7470/7471), mg/kg dw Date Analysed I I I !:ilver ,(COlO) Silver (6010), mg/kg d~ Date Analysed Selenium S~leni·um (6010), mg/kg dw ----·------·--------. -----··-- .. I 15 12.06.95 l.l 12.06.95 Sl 12.06.95 0.1: 12.06.95 <l.l 12.06.95 56748·3 18 17 12.06.95 12.06.95 97 J.10 13,06.95 1a.os.9s <0.60 <0.60 12.06.95 12.06.95 46 38 12.05.95 12.06.95 0.11 0.071 12.06.95 12.06.95 <.l. :i <l.2 12.06.95 12.06.95, 12-04-95/1500 l~·04·95/J.i40 12-04-95/1420 12-04 · 95/1450 12-0,;-9S/1430 56748·4 56748-5 22 12.06.95 130 1J.06.9S <0.61 12.06.95 H 12.06.95 0.077 12.06.95 <1.2 12.06.95 <:l4•F65 12,06,95 17 12.06.95 77 ia.06.95 <0,75 12. 06 .95 29 12.06.95 0.091 12.06.95 <l.S 12.06.95 <30"F65 12.06.95 I LAl>oratorioa In Sorenneh, OA • T•llohonn, l'L • T•mpo, l'L • Da&rfleld ISaach, l'L • Mob/le, ~L • New Orleans, LA rEC-0'.'-1995 1 7: 39 FROM SAVl'NNAH LRBS TO 917043911147 P.00 I s L SAVANNAH LABORATORIES & l!NVIRON6fl!HTAL SERVICES, INC. ~5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: SS-56748 05 DEC 95 07 DEC 95 Mr. John Rhyne = Corporo.tl.on 5335 Trianile Pkwy. Norcross, GA 30092 Suite 450 CC: Jack Kilbarger REPORT OF RESULTS Received: Reported: Project: 16817 Cherokee Oil SampleQ Hy: Clie~t DATE/ I I I I I LOG NO 5674B•l 56748 •2 56748-3 56748-4 ~6·14~.5 SAMPLS DESCRIPTZON, SOLID OR Si::M!SOLID SAMPLES CO-WS-33 TIME SAMPLED 12·04·95/lSOO 12-04-95/14'0 12-04-95/1420 12-04-95/1450 12-04-95/1430 I I CO-WS-34 CO•WS•3S CO·WS-36 CO·WS-37 .... ___ --------··--·--------.... Lead (6010) Lead (6010), mg/kg dw .-;ate AnB\yzed ~ercent Solidc (lG0.3), ~ I I I I I I -----....... ----· -------....... - .. I 56749•1 .. .. --.... --.... 110 12.06.~S 00 -·-------- 5'748-~ 56718-J 5-718-1 H718-5 ----------.. ................ -.. -.. --..... ---......... -.... 140 75 62 150 12.06..95 12.06.95 12.06.95 12.06.95 83 83 82 67 ,.. _________ . ------------------------------ .• t..bol'ltorfos In Savannah. QA • T1//11h111HI, FL • T11mpJ1, FL • llNrll.,d ~JtCh, l'l • Mohll,t, Al • N,tW n,,,.,.n,., LA CEC-07-1995 :-;,:39 FROM SAVl'f'H,H LABS TO 9,7043911147 P,09 I SL SAVANNAH LABORATORIES & INVIRONMl!NTAL SaRV/C/it;, INC. ~ 5102 LaRoche Avenue• Savannah, GI>. 31404 • (9i2) 354-7858 • Fax (912) 352-0165 LOG 110: S5·!6748 OS DiC 95 07 DEC 95 Mr. Jol".n Rl,yne OHM Corpo.c: a L..i v1J S335 Triangle Pk>r/. Suite 450 Norcross. GA 30092 CC: Jack Kilbarger P.EPOP.T O, PJ.SULTS Received: Reported: PUrchase order: 1016477 Project: ~6817 Ch~rakee Oil Sampled By:, Client Page 9 DATE/ I I I I I I I LOO NO 56748-6 PARAMETER SAMPLE DESCRr?'I'ION, SOLID OP. s=sOLID SAMPLES TIME S.AMP!.EO I I I I I I Volatiles by GC/MS (8240) Chloromethane, ug/kg d~ Bro~orneth.'.1lle, ug/kg d~ Vinyl chlorice, ug/kg dw Chloroethane, ug/kg dw Methylene chloride IDich!oromethar.e), ug/kg dw Acetone, ug/kg dw C~rbor-q.isul!lU~, u~/kg dw l,l-Dich1or01ithene, ug/kg dw 1,1-Dichloroethane, ug/kg dw Cis/Trans•l,2-Dich1oroethene, ug/kg dw Chloroform, ug/kg dw l,~-Dichloroc~h:inc, ug/k~ dw 2-Butanone (MEK), ug/kg dw l,l,l·TrichloraQthar.i,, ug/kg dw Carbon t2trachloride, ug/kg dw Bromodichloromethane, ug/kg dw l,l,2,2-Tetrachloroethane, ug/kg dw 1,,-Dichloropropane, ug/~g dw trans-1,J-Dichloropropane, us/k~ dw Trichloroethene, ug/kg dv Dibr011',0Chlorometha.ne, ug/kg d·.-l, l, 2-Trichloroethane, ug/kg dw Benzene, ug/kg dw • .. I 56748-6 <1700 c:.1700 <l 700 <1700 <840 <8400 <840 <840 <840 <840 <840 'l.'.840 12·04·95/1530 ,2Q_O_Q_Q;,:,, ,:940 <840 <840 <840 <840 <840 <840 <840 <840 <840 1 Laboratorioe In S:~v:>nnalt, OA • Tai/aha.see, F'L • Tampa, F'L •. D••rlf•ld t:t.aclt, FL • Mob/lo, ~L • New Orl1111ns, LA I LEC-07-1995 !7: 40 FROM SAVf'N'IAH LABS SL SAVANNAH LABORATORIES & l!NVIRONMl!NTAL SERVICES, INC. TO 9,7043911147 P. 10 --102 '..aRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S5·55H8 05 DEC 95 07 DEC 95 I I I Mr. John Rhyne OHM Ccrr,cr-"t \or. 5335 Triangle Pkwy. Suite ,so Norcross, GA 30092 CC: Jack Kilbarger REPORT OF RESOLTS Received: Reportad: Project: 16817 Cherokee Oil Sampled By: Cll,.nL Paqe 10 DATE/ I LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES CO•WS•J8 TIMi SAMPLED • I I PARAMETER ---------------------------------------c:Ls-1,J-Dichloropi:.vf!t:,u~, ug/k:g c1w eromofor:n, ug/kg dw 2·Hexancne, ug/kg dw 4·Methyl•2-pentanone (MIBK), ug/kg dw Tetrac:hloroethene, ug/kg dw Toluene, ug/l<g dw · lorobenzene, ug/kg dw hylbsniP.nP, t>!,/<g dw Styrene, ug/kg dw Xylenes, ug/kg dw surrcgate Toluene-de Surrogate -4•Bromofluorobenzene Sv.rrogato • l,~•Diohlorooch~c d4 I Date Analyzed ................. ·····----·-· ......... . I I I I .. I 56748·6 <~-IV <840 <8400 <8400 <840 ~ <840 [280Cl) <840 [li0-0) 109 t 109 \- 1J3 t 12.06.95 -. ----...... -.. --.. --. --.. .. .... -. -.. --.. Laboratort111 In s,vannah, GA • TllllhllUff, FL • Tampa, FL • Detrlltfd Bffeh. FL • Mob/It, AL • New Orleans, LA I . . 1,EC-07-: 9'35 l7: 40 FROM SAVR-<flAH LABS TO 9, 7043911147 P.11 I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVIC~. INC. -.-,02 LaRoche Avenue• Savannah, GA 31404 • (9'.2) 354-7853 • Fax (912) 352-0165 LOO NO: 85-56748 05 DEC 95 07 DSC 95 I I I Mr. John Rhyne OH:-:1 corpor:i.t:ion 5335 Triangl• Pk•,y. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS Receivad: Reported: PUL'r.:l.Hll:Se Order: 101.6'4 77 ?reject: 16817 Cherokee Oil Sampled ~y: Client DATE/ I ux; NO SAMPLE DESCRIPTION, SOLID OR SE:-!ISOLID SAMPLES TIME SAMPLED CO-WS-38 12-04-95/1530 PARAM:i!TiR I 'l'C .. ~ernivclaciles (8270) :;:~encl, ·..tg/kg d·~ hi~(?-Ch1o~cethyl)eth•r, ug/kg dw 2-Chlcro~hencl, ug/kg dw 1,3-0ichlorobentene, ug/kg dw 1,4-Dicnlorobenzene, ug/kg dw I ... 2-Dichlorobenzena, ug/kg dw ~~Mo~hylphenCl (o-cxc3ol), ug/~g dw 2,2'-Cxybis(l-Chlorcpropane) I I I I (bis-2-chloroiioprcpyl ether), ug/kg dv 3-Methylphenol/¼-Methylphenol(m&p-cresol), ug/kg dw N-N~troso-di-n-propylamine, ug/kg dw Hexa~loroeth<ule, ug/kg dw Nitrobenzene, ug/kg dw rsophcrone, ug/kg dw •·Nitrophenol, ug/kg dw 2,4-0i:ne:hylphenol, ug/kg dw bis 1.2 •Chloroei:l'loxy) methane, ug/xg aw 2,4-Dichlorophenol, ug/kg dw l,2,4-TrichlorobenzanA, 119'/kg dw Naphtr41ene, ug/kg dw 4-Chloroa.niline, ug/kg dw H•xach10::¢0Utadiene, ug/kg dw I -~:~~~~:~:~:~~~~::~~~~~::_~::k=-~~-----· ·--------- I .. I 56748-6 <8900 ,<6900 <8900 <8900 <8900 <8900 d9CO <8900 <8900 <8900 <3900 <8900 <8900 <8900 <8900 <8900 <8900 d900 <8900 <18000 <8900 <8900 Laboraton.t In S•v•nn•h, GA • Tall•h•uoa, FL • 7Amfl", FL • O.•rfl.,ld S.aeh, i=L , Mob/I•, AL • New Orlunc, LA I U:C-07-1 995 : 7: 4 ! FROM SA\Jf'.:NNAH LRBS TO 9'.73-'l3911147 P.12 I s L SAVANNAH LABORATORIES S t!MV/f1ONMENTAL /Jt:l!VICES, INC. --5102 LaRoche Avenue• Savannah. GI>. 31404 • (912) 354,7R~A • F'ax (912) 352-0165 LOG NO: SS-56748 Received: 05 osc s~ Reportad: 07 DEC SS Mr. John Rhyne OHM Corporation 5335 Triangle Pkwy. Suite 450 Norcrosc, GI\ Z009a CC: Jack Kilbarger REPORT OF RKS!JLTS Purc:haee Order: 1016477_ Project: 16817 Cheroke9 Oil Sampled By: Client Pa.g• 12 DATE/ I I I I I LOO NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPL!!S TIME SAMPLJ::t> 56740·6 CO·WS-38 12-04-~S/1530 PARAMETER I I 2·Methylnaphtha.lene, ug/kg aw Hexachlorocyclopentadiene, ug/kg dw 2,4,6-Trichloropnenol, ug/kg clw 2,4,S·Trichlorophenol, ug/kg dw 2-Chlorc,nAphth"'l<>ne-, u!)/lcg-dw 2•Nitroani2ir.o, ug/kg dw .a>imethylphthalate, ug/kg aw ri:,.cenaphthy"ene, ug/kg dw 3-Nit=oanil~ne, ug/kg dw .A.cgnaphthene, Ui/kg dw 2,4•Dinitrophenol, ug/kg dw 4-Nitrophenol, ug/kg dw Dibenzofuran, u9'/k9 aw 2,4-Dinitrotcluene, ug/kg dw 2,~•Dinit•otQluene, ~g/kg ~w Diethylphthalata, ug/kg dw 4-Chlorophenylphenyl et:her, ug/kg dw Fluorene, ug/kg dw I I I 4-Nitroani:ine, ug/kg dw 4, &-D.iHitz;o-2-methylph•nol, ug/kg o.w I N•Nit=oeod~phenylamine/Diphenyl~~ine, ug/kg dw 4-Bromophenyl phenyl ether, ug/k11 dw Hexachlorobenzene, ug/kg dw I-~=~:~~=~=~~~~~~=:.::~~=-~~-----------------·--- I -. I 56748-6 ~ <3900 <9900 <8900 <9900 <45000 <8900 <8900 <46000 -:8::>00 <46000 <46000 <8S00 <8900 .s,oo 118000, <8900 <8900 <46000 <4b\JC\l <8900 c:"~SCO <8900 <46000 Laboratories in !1a•onn•h, GA • T~;fah11SS!N, l'L • Tampa, FL • Dff/1/Q/a BOICll, FL • Mobilt, AL • New OrlHnl, LA •• TO 9: 713a391114? P. 1.'3 1 ·s L SAVANNAH LABORATORIES II l!NVIRONMl!NTAL SERVICES, INC. I... 5102 L.aRoche Avenue• Savannah. GA 31404 • (9i2) 354-7858 • Fax (912) 352-0165. .. LOG NO: S5-56748 05 DEC S5 07 DiC % I I I I I I I I I I I I I Mr. John R.'1yne (;J-fM Cnyt?ori't£.-:m. 5335 Triangle Pkwy. Suite 450 Norcross, GA 3009• CC: Jack Kilbarger RSl'ORT OF RESULTS ReceiV9d: Reported: Purch~oc Order, iOi6477 Project: 16817 Cherokee Oil Sa.ruplea ny: Cll~11L Page 13 DATE/ LOG NO SAMPLE DESCRI?T!ON, SOLID OR SEMISOL!D SAMPLES TIMI! SAMPLED 56748-6 CO•WS-38 12·04·95/1530 PAAIIMETER 56748-6 Plii::ucu1ch;;-e:.e, ug/kg d.w A.~thracene, ug/kg dw Di•n·butylphthalate, ug/~g dw Fluoranthene, ug/kg dw l?yrene, ug/kg dw autyl~enzylphthalate, ug/kg dw ,3'-Diclllorobenzidine, ug/kg dw P.n:tn (;t) Ar')thr~.a.c:-,;,nll?, w,:r/k-, dw bis (2 •Bthylhexyl) phthalate, ug/kg Chrysene, ug/kg dw Di-n-octylphthalate, ug/kg dw Benzo (b) fluoranthene, ug/kg dw _lien=o (k) fl~o:r~thcne, 1,.lg/kg d.w- Benio (a) py,:ene, ug/kg dw Indeno(l,2,3-cd)pyrene, ug/kg dw Dibenzo(a,h)anthracene, ug/kg dw Benzo(g,h,i)peryl•ne, ug/kg dw Carba&ole, Ui/ki dw Sur=ogata Phenol dS Sur~ogate •·Fluorophenol Sur=ogate 2,4,6-Tribrornophenol Sur=ogate Nitrober.zene • dS Su.-.;;o~a.L~ Z • !'luoa:cobiphenyl Sur=o,ata Terph•nyl • d14 Date Bxtracted Date Analyzed dw <8~00 <3900 /,;ooo <8900) <8900 1ffo..Q9 <18000 d900 (120000 <8900 <8900 <8900 ,8900 <8900 <8900 <85100 <8900 .e,oo •F33 •F33 *Fl3 •F33 •n:s *F33 U.0,.9<; 12.07.95 ~ I Lllboratorlea In Snannah, QA • Tal/11he,no, FL • Tampa, FL • Deerlleld Beach, FL • Mob/la, AL • New Orleans, LA I I:EC-07-1995 l 7: 42 FKOM SAVFNNJC;H LABS TD 917043911147 I s L SAVANNAH LABORATORIES' 4 ENVIRON/Vt:NTAI. :svtVIC1!3, INC. ,..102 LaFloche Avenue• Savannah. GA 314°04 • (912) 354-7858 • FA< (91?.) 352-0185 LOG NO: S5•5674& Rcooivod, 05 ~SC 95 Raport,d: 07 DEC 95 I I I Mr. John Rhyne OHM Corporation 5335 Triangle Pkwy. Suite 450 Nox·croll's, CJ\ lCC9:J CC: Jack ~ilbarger REPORT OF RXS'IJLTS Purchase Order: 1016477 Project: 16817 Cherokee Oil Sampled By: Client Page 14 .DATE/ I LOG NO SAMPLE DESCRIPTION, SC!..ID OR SEMISOLID $1\MPLES Til!m SAMPLED CO·WS•38 PAAAMETBR I ··········-·················· Percent Solids (160.3), t I ,, I I I I I I le I 56748-6 74 iJ•04•95/l530 1 i..ix,,.torln In Sa•11nnoh, OA • T•llaha1soo, fL • Tamp,, Fl. •· DoerrtelCI BNcfl, FL • Mob/It, ~L • Ntw Or/e,n,, LA CEC-07-1995 17:43 FROr1 SAVf'tlNAH LABS TO 9, 71343911147 P, 15 I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. '9102 L.aRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: SS-56748 Rec&ived: OS DEC 95 RQportod: 07 DKC PS I I I· Mr. John Rhyne OIIM Corporation 5335 Triangle Pkvy. _Norcross, GA 30092 Suite 450 CC: Jack Kilbarger REPORT OF RESULTS Purchautt Or-<ler: 10Ui77 Project: 16817 Cherokee Oil ~an,pled By: ~lienc I LCG NO SAMPLE DESCP.I?TION, QC REPORT FOR SOLID/SEMISOLID I 56748-; 56748-8 56748·9 Method Blank Lah Ccmr.rnl ~t~nruo.rd (LCS) t Reec:,very/Duplicata LCS 't RPD I ··········· :PARAMETER 56748·7 56748·9 S6748·9 ----------------·----------.. I Vol~tilea b~ CC/MS (8240) Chloromethane, ug/kg dw Broll\Oltlethane, ug/kg dw Vinyl chlorice, ug/kg dw .A;ioroethane, ug/kg c:lw . .... Mcthyl~ne chloride (Dich"orometh=e), ug/kg d• I I I I Acetor.e, ug/kg dw Carbon disulfide, ug/kg dw l,l·Dichlorwthene, ug/kg dw l,l·Dichloroethane, ug/kg dw Cis/Tra.ns•l,2·Dic.:hlvx-outllene, ug-/kg dw Chloroform, ug/kg c:lw 1,2-Dichloroethane, ug/kg dw 2-Butanone (MEK), ug/kg dw l,l,1-Trichloroethar.e, ug/ki dw carbon eeerachloride, ug/kg dw Bromodichloromethan•, ug-/kg dw 1,l,,,2·Tetrachloroat:hano, ug/l<g <lw l,2·0ichloropropane, ug/kg dw trans-l,3-Dichloropropene, ug/kg dw ,Trichloroetnene, ug/kg c:lv I -~=~~~~~:~~~"."'.'~~~~'.-~:'.~~-d~---······ I <10 <10 <10 <10 <.5.0 <25 <5.0 <5.0 134/136 t <5.0 <5.0 <5.0 <5.0 <,5 <5.0 <5.0 <5.0 ~s.o <5.0 <5.0 cS.0 ll4/l20 t <5.0 1 't 3 ' l.aboNllorl•il in S11vannah, GA • 11//ahatNe, FL , Tampa, FL • Doerlleld lleaoh, FL • Mobil<>, AL • Now Orla•na, LA I. . . . r:€(-07-1995 ,7:44 FR01 SAVl'N'<AH LABS TD 917043911147 P.15 I SL SAVANNAH LABORATORIES & INVIRONll~TAL SallV/C/;;S, INC •. --5102 LaRocM Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NC: .Received: S5-56748 OS DiC % 07 DBC ;15 I I I I I I I Mr. John Rhyn11 Om-.t Cuz.1,1o;r;•eion 5335 Triangle Pkwy. Suite 450 Norcross. GA 30092 Reported: Purchase order: 1016477 CC: Jack Kilbarg-er Projact: 16817 Chet"okee O:.l Sampled By: Cl-ient LOG NO 56748-7 5'748-a 56748-;1 PA.RAMETER !Ui:PORT 011 ll.li~U..TS Slu'!FLE D&SCRIPTION, QC REPOR~ FOR SOLID/SE~ISOLID Method Blank L.ab Control St:>nd.:>.rd (LC~) t Recovo,:y/Duplicate LCS \ RFD 56748-7 l,l,~ Trichlo=oethd.ne, Ui/kg dw Benzene, ug/kg dw cis-l,3-Dich"oroproper.e, ug/kg dw 55748-8 56748•;1 l28/l2S t 0 t ,, Brc,no:o:c,n, ug/kg dw 2-Hexanone, ug/ks dv · 4·McL.h1l-~-1,1 .. utanone (M.IBlC), ug/kg dw Tetrachloroethene, ug/kg dw <,.o <5.0 <5.0 <5.0 <25 <l~ <5.0 ~~.o <5.0 <5.0 <5.0 <5.0 Ut I I I I I I Toluene, ug/kg dw Chlorobenzene, ug/kg dw Sthyll>enzene, ug/kg dv ·scyrene, UIJ /kg dw Xylenea, ug/kg dw Surrog;ar.~ -Toh1~n,;;1-d8 Surrogate -4•Bromo!luorobenzene Surrogate•· l,2•Dichloroethane·d4 Date Analyzed .. . ' I 104 t 94 t 12.06.95 Do/1 n t 132/130 t OG/Q' t 100/96 t 92/94 t 12.04.95 5 t 2 t Uboratorlea In Sav:u,nah, QA • TallahmHe, FL • Tampa, FL • Ooorllttld 8eeoh, FL, • Mob/la, AL • New Orluna, LA I . . [EC-07-l 995 :7: 44 FRD,1 SAVl'NNAH LABS TO 1 s· L SAVANNAH LABORATORIES .& l!NVIAONMl!NTAI. SERVICES, INC. --102 LaRor..he Avenue• Sllvannah. GA 31404 • (912) 354-7858 • rl!X (912) 352-0165 Mr. John Rhyne Olm Cor;,or:>tion !335 Triangl• Pkwy. Suite ~so No.rcross, GA 30092 9; 704391 l.147 P.17 LOG NO: Receivei:l.: R~portvd: SS-56748 os oi;c 95 07 DiC 95 I I I CC: Jack Kilbarger Project: l68l 7 Cher_okee Oil Sample~ 5y: Clie~" I LOO NO REP.'.lRT OF RESULTS Page 1 7 SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEJ:USOLIO Method Blank I S6748·7 56748-8 56748·9 Lab Control Standard (LCS) I R~=v~ry/n,_,pl;c~t~ LCS t RPD I .I' ARA.'IETI!R -·----------...................... . TC'.T, .S':'m;_v~lrtt..ilei:i {8270} I Phenol, u9/k9 ow bis(2·Chloroethyl)ether, ug/kg dw 2·Chlorophenol, ~g/kg i:l.w .A,3-Dichlorobenzene, ug/kg dw ~, 4 -!:lichlorobenacii.c,, ug/k:3" dw l,2-Dichlo:;obenzene, \19/k.9 dw 2-Methylphenol (o-cr~sol), ug/kg dw 2,2'•0xybis(l-Chloropropane) I (bis-2-chloroisopropyl ether), ug/kg dw 3-Methylphenol/~-Methylphenol(m&p·cc«~vl), u:1/k:~ clw I N·Nitroso-di-n-propylamina, ug/kg dw Hexachloroethane, ug/kg dw Nitrobenzene, ug/kg dw Isophorone, ug/kg dw I 2 • N l. l.JCVJ,llivuul , ug /l<g dlf 2,4•0imethylphenol, ug/kg dw bis(2-Chloroetho,cy)methane, ug/kg dw I 2,4-0ichlorophenol, ·ug/kg dw l,2,4•Trichloroben:ene, ug/kg dw Mphthalene, ug/~g dw I-~:~:~:~:~~~~: -~=~~= -~~ ----. --.. -......... -.. . I .. I 56748·7 <330 <330 <330 <330 ..:330 <330 <330 <330 <330 <330 <330 <330 <330 cJJ0 <330 c.HO <330 <330 <330 <660 56748·8 56748-9 67/76 t 67/73 t 70/70 ~ 70/76 t 65/70 ~ 8 t 0 \ 8 .. Ulbonttur/es In S1tvann11h, GA • T•ll11h11nee, FL • Tampa, FL• DHrfle/d Boach, FL• Mob/Jo, AL• New Ori.an., LA I TO 9: 7043911147 P.18 I s L SAVANNAH LABORATORIES & i!NVIRONMl!NTAL SERVICES, INC. Ls102 LaRocht Av,nue •Savannah.GA 31404 • (912) 354-7858 • Fax (912) 352-0165 .. LOO NO: I Mr. .; ohn R."iyne CHM Corpor~r..irm 5335 Triangle Pkwy. Suite 450 Norcross, GA 30032 Received: Reported: S5·56748 05 DE:C 95 07 OBC 95 I I CC: Jack Kilbarger Project: 16817 Cherokee Oil So.mpled By: Client REPORT OF RllS!JtTS Pag" 18 I LCG NO SAMPLE: DESCRii'TION, QC REPORT FOR SOLID/SEMISOLID . ----------------... --... -----. -...... -. -....................... --··------------ I 5674'·7 56748•8 56749·9 Method Blank Lab Control Standard (LCS) ~ Recover,-/OuPlicate LCS t RPO ------------..................................................................... ____ .,. ________________ _ I Hexachlorobutadiene, ug/kg dw 4-Chloro-3-methylphencl, ug/kg dw· 2-Methylnaphthalene, ug/kg dw Hexachloroc-;<:lopencadiene, ug/kg aw .. ,4,6-Trichlorephenol, ug/kg dw · ~, 4, 5-Trichlorq,h~nnl, llg/kcr dw I I I 2-Chloronaphtht,lene, ug/kg dw 2-Nitroaniline, ug/kg dw Dimethylphthalate, ug/kg dw Acenaphthyler.e, ug/kg dw 3-Nitroanilino, ug/kg dw Acenaphthene, ug/kg dw 2,4·0initroptenol, ug/ltg dw 4-Nitrophanol, ug/kg dw Dibensofuran, ug/kg dw ~,4-0initrotolv.eno, ug/kg dw 2,6-Dinitrotoluene, ug/kg dw Oie~hylphthalate, ug/kg dw I 4·Chlorophenylphenyl ether, ug/kg dw Fluorine, ug/kg dw ~-Nitr~iline. ug/Ag a~ I -~:::~:~::~:~:~~~:::~~~~::.u=~~=-~~--- 1 56748•7 56748•8 <330 <330 73/79 t <330 <330 <330 <330 <330 <l 700 <330 <330 <1700 <330 70/76 t <l 700 <1700 73/76 t <330 ,330 82/88' <330 <330 <330 <330 <1700 <1700 56748·3 a ' 8 t 7 ' la'bor,torlH In S,v,nnah, GA • 1'11,hntH, Fl • Tampa, Fl. • Dffrlltld Beech, FL • Mobil•, AL • New Or/Nnl, U I, [EC-07-1995 ,7:45 FROM SAVR-INAH LABS TO 9:7043911147 I s L SAVANNAH LABORATORIES & 5NVIRONMaNTAL $~V/Cft, INC, k;----------------------------• 2 LaRoche Avenue • Savannah. GA 31404 • (912) 354,7858 • Fax (912) 352-0165 I LCG NO: 95-56748 Received: 05 DBC ~5 Reported: 07 o.c 95 I I Mr. John Rhyne OKM Corporo.tion Purehase oraer: 1016477 5335 Trimgle Pkwy. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger Project: 16817 Cherokee Oil San,pled By: Client ILOG NO ·tG748-7 '748-8 56748 ·9 SAMPLE OESCRI;~ION, QC REPORT FOR SOLIO/SiMISOLID Method Blank Lal:, Control St,ond;,.rd {LCS) \ Radovery/D~plicate LCS t RPO l ·····----- AAAM!!TER I Surrogo.t:.e Phe:101 d.:; Surrogate 2-Fluorophenol Surrogate 2,4,6-Tribromophenol • . rogate Nitrobenzene -dS rogate 2-Fluorobiphenyl ' "·"'-":l•tv Te:r:phenyl -dl4 Da.te Extracted ■~ate. Analyud rsenic ?,rsenic (6010), mg/kg dw uat:a Analy;aa l arium (6010) · Barium {~010), mg/kg dY Date Analyzed ladmium (6010) Caooiium (6010), mg/kg dw Date Analyzed Chromium (•010) 10,,:-omium (6010), mg/kg dv Date Analyzed Me:-cury · ■Mercury (7470/7471), mg/kg dw .:>tc An:>lyHd ' 56748•7 82 t 73 \ 85 t 70 \ 76 % 7U t 12.05.95 '2.06.95 <l.0 12.06.~S <0.50 12.06.95 <l.0 12.06.95 <0.010 13,06.J!! -----------... --------- 56748·8 56748·9 ------·------------- 73/7' t 70/73 \ 82/85 ~ 65/70 t 70/76 \ 7U/7~ t 12.05.95 12.06.95 103/99 t 4.0 t 12.06.95 !"/U " ) -~ " 12.06.95 101(98 t 3.0 t 12.06.95 99/96 t 3.1 t 12.06.95 96/102 ~ 6.1 \ u.os.,s -boflltorloa In $<>v•nn•h, CA • T•ll~:,aace, FL • T•m(Ul, FL• Deerllo/d 8e11Ch, FL • lllobile, ~L • New Orle11na, LA [E,:-07-1995 ,7:~7 FROM ~ LABS TO 9:7043911147 P,21 1 ·s L SAVANNAH LABORATORIES l '1fVIRONM~NTAL SaRVICR, INC . .. 5102 LaRocne Avenue • Savannah, GA 31404 • .(912) 354-7858 • Fax (912) 352-0165 T .IJG pqo: s~-,~74~ OS DtC 9! 07 DEC 95 I I I I I I I I I I I I I Mr. John Rhyne OKM Cux.vut·• t ion SJJS 'h':i.angle Pk'")'-£uit• 4S0 Norcross, GA 30092 Received: Reported: C" · Jack !Cilbarger Project: 16817 Cherc~e Oil Sampled By: Clie~t LOG NO 567H·7 SG7U-8 56743-9 P.EPORT OF P.l!SULTS Sl.MPL? DESCRIPTION QC REPORT FOR SOLIO/SEMISOLn> Moslhw a1.,.ul< I.ab Control Standard (~) t Reoov,::,:y/Ouplic::,,t,: LCS t RFD PAAAMETBR 56748•7 56748·6 56748 · 9 -------·-· ---·------..... --..... -. Silver (6010) Silver (6010), m11/l<:g a,.. Date Analyzed Selen:.um Seltnium (6010), lllg/J<:g d'II' D•t• Analyzed 1 ..... o1 (6010) Lead (6010), lll!'l/1<:q dw Date Analy:ed Me1:ho<18: IU'A SW· 846 <l.0 12.06.95 <10 12.os.,s .s.o 12.06.95 99/9,; ,.. 3. 1 ll.06.95 96/94 ' 2. l 12.06.,5 99/98 ' 1.0 12.06.95 •F33 a Cont~~l limits a•e eatabli&hed gnly for sun:ogAte concentration levels sp11cifiRd hy llPA ,,...thnc1,.. ll•ct1use th<> sample va.a diluted pri= to analyaia, aurrogate recoveries are not reported. •F65 •·Eleva~ed detection limits were reported due to sample matrix interfu:ence "wb.i.c:h L·•qu.l1:vil Ample or extra.ce dilution. Steven J. White. Project Mar.ag,,r Q1P'r •. ' ' I le Final Paga Ot Report I Lltboratorl•• l,j S-,,,,all, QA • Tall•haasoo, FL • Tam,,., FL • D••rll•ld BNCh, R. • Mob/le, AL • N•w OrlHn11, LA ' . I TOTAL P.21 .. r:EC-07-1995 1?:45 FROM SAVf'tiNAH l.ABS TO 9: 7043911147 P.19 •s L SAVANNAH LABORATORIES :. l fNVIRONM.NTA~ SERVIC6S, INC. · C2 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • F!X (912) 352-0165 I I I I Mr. John Rhyne OHM Corporation 5335 TriMgle Pkwy. Suite 450 Nor.cross, GA 30092 CC: Jack ~ilbarger IU1P0RT OF REllULTS 'LOO !10: S5•567U Recei~d: 05 D6C 9S Reported: 07 DEC 95 Purch&ae Orc:ler: l0lo477 Project: 16817 Cherokee Oil Sa.:npled By: Client l'"gc 19 !.OG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID .~~;~~~;···· s,118-8 ·. 5€748·9 ·~~~;;;·· -----·--------------------------------------■------Method Blar.k L<U:> Control Cte.nclard {l,CS) ~ R-,covery/Dl.iplicate LCS 'I-RPD 56748-7 <330 <330 <330 56748•8 I . N-tti. tro!lodiphenyla.mine/Dlph~uylo.miutt, ug/kg dw ~ ·B:coi:,ophenyl pheny: ether, ug/kg d"' !!exa::hlorobenzene, uq/kq dv .ntachlorophenol, ug/kg dv <l 700 48/48 t l"!'.:enanth~·ene, ug/kg dw Ar,thracene, u,r/ks dw Di•n•butylpht.halate, ug/kg dw I Fluoranthene, ug/kg dw l'yrene, ug/kg dw ~utylbenzylphthalate, ug/kg dw I ~.J' •Di<:!lloroben,:idine, ug/ltg dw Benzo(a)anthracene, ug/kg dw bis(2-E~ylhexyl)phthalate, ug/~g dw Chrysene, ug/kg d~ I Di•n•octylphthalate, ug/kg dw Benzo(bl!luoranthene, ug/kg dw Benao(k)fluoranthene, ug/kg dw I Bcnco{~)pyrcne, ~g/kg dv Indeno(l,2,3-cd)py~ane, ug/kg d~ Diben~o(a,h)anthra.cene, ug/kg dw 8en,o(g,h,i)perylene, ug/kg dw I Carbur:,le, ug/kg dw · -----------·-------------··----------·--------·---- I -. I <330 <JJO <330 <HO <330 65/65 t <330 <650 <330 ~no <330 <330 <330 <330 ~no <330 <330 <330 <330 56748·9 0 t 0 t tbor;,lorie, In Savannah, QA • Tallahos,H, FL • Tampa, FL • Ottt1rlield BH~h, FL • Mob/la, Al. • Naw OrlHn,, I.A . f,V;·~·-·. :H~t:A<-~ . j_. ~/ ij:t\f:/_ --.... - -CHAlt•• CUSTODY ' Flel.d pH· Result I - Analyst_. ____ _ .. Time/Date_--'"'--- . · (QA/QC Separate) · -- -- ;.'Time: ~---~~-- -Time: ------- :.:.~•_/ . . ~ . . • Samples\eceived on ,c,.;? ·Yes~ Pre---Arvatiw ; Plea~e sign°~nd return the white and yellowcopie~ to the Laboratory. ·· -.. ·-. . . DEC 14 '95 iS:12 TO 3911147 I Omni OEC I I I I I I I ----------------------------- Certificate of Analysis Client: OHM Corporation 2401 Tuckaseegee Road Charlotte, NC North Carclina Certlflcatlon Number: 305 South Carolina Certific•tion Number: !19032 Client#: Contact: Sample Date: SDG II: 381 Jack K.ilbarger 30-Nov-95 SDG-000~02 Lab Sample ID: LSID-001951 Sample ID: CO-WS-31 Parameter ' .. I, 1. l-Trichlornethane · J,1,2,2-Tetrachloroethane 1,1,2-"fichloethane I. 1 -Dichloroethane I I, 1-Dichloroethene 1,2-Dichloropropane ' l I 1,2-Dichlorobenune 1,2-Dichloroethane 1,3-Dichlorobenzcne I 1,4-Dicltlorobenzcne 2-cltloroethyl vinyl ether Benzene I Bromodichloromethane Bromoform I Bromomethane Carbon tetrachloride Chlorobenzene I Chlorocthane Chlomform Chloromethane .. Dibromochloromethane Reporting Result Limit u 5 u 5 u 5 u 5 u 5 u 5 15 5 u 5 -U 5 u 5 u 5 u 5 u 5 u 5 u j u s u 5 u 5 u 5 u 5 u 5 Unit ppb ppb ppb ppb ppb ppb ppb pph ppb ppb ppb ppb ppb ppb ppt, ppb ppb ppb ppb ppb ppb Receipt D•te: 3U-Nov-9S Report Date: i 4-Dec-95 Approved By: Met!?ud RPA &010/8020 EPA ~O !Oi802G EPA 8010,8J20 EFA &O!Oi8G20 EPA 8010/8020 EPA SO lC/8020 EPA 8010/8020 EPA 8010/8020 EPA 80 l0/8020 , EPA 80!0/8020 EPA 80!0/S020 EPA 8010/8020 EPA 8010/8020 -EPA W!0/8020 EPA•00!0/8020 EPA 8010/8020 EPA 80 I 0/8020 EPA 8010/8020 EPA 80 l0/8020 EPA 8010/8020 EPA 8010/8020 Kenneth R. Richard80n Project Manager Time Date 20::l' 12/4/9, 20:3} 12/4/95 20:31 12/~/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12./4/95 20:31 12/4/9.5 20:31 12/4/95 · 20:31 12/4/95 20:31 12/4/95 20:3 I 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 12/4/95 20:31 1214/95 20:31 1214i95 I I 11176 Down• Road -Pineville-, KC 28134 Phone: ('10..) 588-5076 -FAX: (';04) 588-2454 Page ! Analyst SJ SJ SJ SJ S1 SJ SJ SJ SJ SJ SJ SJ SJ S.1 SJ SJ SJ SJ SJ SJ SJ DEC 1~ '95 LS: 12 TIJ 331114? FROM AquaChem E~uir. Lab T-810 P.03 I Qomi EnvironmmlJll le Consultants_. In,; I I Client: OHM Corporation OEC Certificate of Analysis North Carolina Certification Number: 305 I 240 l Tucbseegee Road South Carolina Certification Number: 99032 Charlotte, NC Client#: 381 Receipt Date: 30-Nov-95 I Contact: Jack Kilbarger Report Date: 14-Dec-95 I Sample Date: 30-]';ov-95 ® ill m ~ SDG#: SDG-000502 Approved By: I Lab Sample ID:LS!D-001951 Kenneth R. Richardson Sample ID: CO-WS-31 Project Manager Reporting I Parameter Result Limit Unit Method Time D•te Ethylbenzene 44 ppb EPA 8010/8020 20:3 I 12/4/95 5 ft Mo:nylene chloride u 5 ppb EPA 8010/8020 20:J I 12/4/95 T ctrachloroctheuc u 5 ppb EPA 8010/8020 20:31 12/4/95 Toluene 19 5 ppb EPA 8010/8020 20:J 1 ,2/4/95 I Total Xylones 226 5 ppb EPA 8010/8020 20:31 !2/4N5 trans-1,2-D ichloroethcne u 5 ppb EPA 8010/8020 20:31 12/4/95 trans-!. 3-Dlchloropropene u 5 ppb EPA 8010/8020 20:31 12/4/95 I Trichloroethene u 5 ppb EPA 8010/8020 20:31 12/4/95 Trichlorofluoromethane u 5 ppb EPA 80 10/8020 20:31 12/4/95 I Vinyl chloride · u 5 ppb EPA 8010/8020 20:31 12/4/95 ! ,2,4-Trichlorobenzene u 20 ppb EPA 8270 12/12/95 l,2~Dichlorobcnzene u 20 ppb EPA 8270 12/12/95 I 1,3-Dichlorobcnzcnc u 20 ppb EPA 8270 12/12/95 1,4-Dichlorobenzene u 20 ppb EPA 8270 12/12/95 2,4,5-Trichlorophenol u 20 ppb EPA 8270 12/12/95 I 2,4 ,6-Trichlorophenol u 20 ppb EPA 8270 12/12/95 2,4-Dichlorophcnol u 20 ppb EPA 8270 12/12/95 2. 4-Dimethylphenol u 20 ppb EPA 8270 12112195 I 2,4-Dinitrophenol u 20 ppb EPA 8270 12/12/95 2,4-DinitrotoJuene u 20 ppb EPA 8270 12112/95 .... 2,6-Dinitrotoluene u 20 ppb EPA 8270 12/12/95 I I 1117' Dowu R<?Sld -Pineville, NC 2913-4 Phoa.e: (704) 588•5076 FAX: (704) 588-24!4 Page 2 7J Analyst SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ SJ Sj SJ SJ SJ SJ DE( 14 '95 LS:13 IC! 391.1147 FROM AquaChe~ Enu~r. Lab T-810 P.0~ I Omni ~ I I Client: OHM Corporation OEC Certificate of Analysis North Carolina Certification Number: 305 I 240 I Tuckaseegee Road Soulh Carolina Certification Number: 99032 Charlotle, NC I Client#: 381 Receipl Date: 30-Nov-95 Contact: Jack Kilbarger Report Date: 14-Dec-95 I Sample Date: 30-Nov-95 [D w ffi ~ u SDG#: Approved By: SDG--000502 I Lab Sample JD:LSID-001951 Kenneth R. Richardson Sample ID: CO-WS-31 Project Manager I Reporting Parameter Result Limit Unit Method Time · Date Analyrt 2-Chloronaphthalene u 20 ppb EPA 8270 12/12/95 SJ ft 2-Chlorophcnol u 20 ppb EPA 8270 12/12/95 SJ 2-Methlyphenol (o-cresol) u 20 ppb EPA 8270 12/12/95 SJ 2-Metllylnaphthalene u 20 ppb EPA 8270 12/12/95 SJ I 2-Nitroaniline u 20 ppb EPA 8270 12/12/95 SJ 2-Nitrophenol u 20 ppb EPA 8270 12/12/95 SJ 3,3-Dichlorobenzidine u 20 ppb EPA 8270 12/12/95 SJ I 3-Nilroaniline u 20 ppb EPA 8270 12/12/95 SJ 4,6-Dinitro-2-methylphenol u 20 ppb EPA 8270 12/12/95 SJ I 4-Bromophenyl phenyl ether u 20 ppb EPA 8270 12/12/95 SJ 4-Chloraniline u 20 ppb EPA8270 12/12/95 SJ 4-CWoro-3-methylphcnol u 20 ppb EPA 8270 12/12/95 SJ I 4-Chlorophenyl phenyl ether u 20 ppb EPA 8270 12/12/95 SJ 4-Methylphenol (p-cresol) u 20 ppb EPA 8270 12/12/95 SJ 4-Nitroaniline u 20 ppb EPA 8270 12/12/95 SJ I 4-Nitrophenol u 20 ppb EPA 8270 12/12/95 SJ Acenaphthene u 2U ppb EPA 8270 12/12/95 SJ I Acenaphthylene u 20 ppb EPA 8270 12/12/95 SJ Anthracene u 20 ppb EPA 8270 12/12/95 SJ Benzo (a) anthracene u 20 ppb EPA 8270 12/12/95 SJ .. Benzo (a) pyrene u 20 ppb EPA 8270 12/12/95 SJ I 11176 Down, Road -Pineville, NC 281J4 Phone: (704) 5811-5076 -FAX: (704) 588-2454 Page 3 I DEC 14 '<:)5 15:14 iO 3911147 I Omn.i M!1vironme,w~1 .. 11sultants. Inc FROM HqL•aChem Env i r. Lab T-816 P. 05 OEC ·----------------- I I I I I Certificate of Analysis Client: Client#: Contact: OHM Corporation 240 I Tuckaseegee Road Charlotte, NC 381 Jack Kilbarger Sample Date: 30-Nov-95 SDG #: SDG-000502 Lab Sample ID:LS!D--001951 Sample ID: CO-WS-31 North Carolina Certification Number: 305 South Carolina Certification Number: 99032 Receipt D•te: 30-NoY-95 Report Date: 14-Dec-95 Approved By: Kenneth R Richardson Project Mar.ager I Parameter ___________________ _ Reporting Result Limit Unit Method Time Uate Analyst I I I I I I Benzo (b) fluoran!hene en1.o (ghi) pery;ene Benw (k) fluoranthene Benzoic acid Benzyl alcohol Bis (2-chloroethoxy) me1hane ' Bis (2-chloroethyl) ether Bis (2-chioroisoprobyl) ether Bis (2-ethylhexyl) phthalate Butyl benzyl phthalale Chrysene Di-n-butyl phthalate Di-n-octylphthalate Dibenzo (ah) anthraccne Dibenzofuran Diethylphthalate Dirncthylphthalate Fluoranthene Fiuorene Hcxacblorobenzene .. Hexachlorobutadicne u u u u u u u u 38541 24568 u 9754 u u u u u u u u u 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA8270 20 ppb EPA 8270 20 ppb EPA8270 20 ppb EPA8270 20 ppb EPA 8270 20 ppb EPA 8270 20 ppb EPA 8270 I I 11176 Dawna Rood. Plneville, NC 2i134 Phone: (704) :1811-5076 • FAX; (7M) 588-2454 Page 4 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12195 SJ 12112/95 SJ 12/12/95 . SJ 12/12/95 SJ 12/12195 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SJ 12/12/95 SI 12/12/95 SJ • l I I I •• I I I I I I DEC 14 '35 15: 14 TO ::,311147 0.!1111i Environmental Consultants. Inc FR0~1 Aql.!aChem r=.1vir. L..Jb T-810 P,06 OEC Certificate of Analysis Client: OHM Corporation North Carolina Certification Numher: 305 240 I Tuckasccgee Road South Carolina Certification Number: 99032 Charlolte, NC Client II: 381 Receipt Date: 30-Nov-95 Contact: Jack Kilbarger Repon Date: 14-Dec-95 Sample Date: 30-Nov-95 rn [~ ~ ~ u SDG/1: SDG-000502 Approved By: ·--Lab Santplc ID:LSID-001951 Kenneth R. Richardson Sample ID: CO-WS-31 Project Manager Reporting Parameter Result Limit Unit Method Time Date Analyst Hexachlorocyclopentadicne u 20 ppb EPA 8270 12/12/95 SJ Hel<lichloruetloane u 20 ppb EPA 8270 12/12/95 SJ lndeno ( 1,2,3-cd) pyrenc u 20 ppb EPA 8270 12/12/95 SJ lsophorone l' 20 ppb EPA 8270 12/12/95 SJ N-Nitroso-di-n-propylan:ine u 20 ppb EPA 8270 12/12/95 SJ N-Nitrosodiphenylamine u 20 ppb EPA 8270 12/12/95 SJ ·· Naphthalene u 20 ppb EPA 8270 12/12/95 SJ Nitrobenzene u 20 ppb EPA8270 12/12/95 SJ Pentachlorophenol u 20 ppb .EPA 8270 12/12/95 SJ Phenanthrene u 20 ppb EPA8270 12/12/95 SJ Phenol u 20 ppb EPA 8270 12/12/95 SJ Pyrene u 20 ppb EPA 8270 12/12/95 SJ re I 11116 0.-Ruad -l'tn<>lll,, NC l81H Pho"": (704) 51111,!5076. FAX: (704) 5118-2454 Page 5 I i_ AquoChem CHAIN OF CUSTODY EHVIRONMEHTAL LABORATORIES, INC. 11176 DOWNS ROAD 704/588-5076 PINEVILLE, NC 28134 FAX 704/58&-2454 Phone Number: ''-7'-'o'-~-1--')__,_3,LJIL,..,-.... oc,,i,__7.__7 _______ _ Client: OH:M (~ll. FaxNumber:(~ >1/-\IL{, Address: I !\00 DL: s+ Purchase Order Numb....,e'-.J.r:~10'-'-1---'-o-'o'---'h-'C ______ _ C~y (h,1lo~e State: P.l Zip:JiiJ01, CertificationRequiremerit:---""-'-''-"'-- u . . . , _ ______ _ Contact Person ,j~ct, K,')h.,)eJ Project Name: Che1ol;a 0.' l . ' . Sampled By: ,1 ,~i1i,u,lr Rush-shr:ges_~'j.~rized □ Yes ~ No By_ri:,linQuishing !his s..:imple(s) 10 Laboralory Per_so_nnel. I warran1 rha1 I am au1hori1ed 10 enter into !his aqre-ement for the C1ient named above and Thal I authorize~~ ~low f,fal.)sis subject to 1he rerms and condiriom1 on the reverse hereof. This agreement is governed hy !he :erms and conditions on the reverse side hereo/. Analysis charges shall bf! as included in 1he laboratories lee sdiedule in effect al the rime ol the analysis. Reiinquished By: Date: I\-;i cl ..tJ S-Time: Received By: Dale: Time: Relinquished By: Date: Time: Received By: Date: Time: "' ~ /;; J 1,71 Q Q ~ iffl1f1i~Ji~!JJJJJJf~¾!f Samples received on ice? Yes □ No □ g 8 t:? ,;i Q Date & Time <5 Q "{d(J ~ (J(J / df:e:f!: Sample 10 Sampled u lab ID 01her Analysis Preservative ~ 0-ws,-~<b [X (1-1..HS-lx Toti VJ.Jfl,,._(.,;.+lJ 2JtJO\ 1 '(v"l' 17nn no;, 1 \ . 11U~T<tiq, ,o~./.!,,,,,, IM rJ,\(..,\Vn!ni 11.,(~ AL .. /1,r11!1 jl;'I)' a -----. Sa"" .! , -c1.J "'", H \; -7 . ~ I \ it\ Awi, .+ &ill I 11 '.>qQ co !) / . Autosampler Sampler Location. ___ _ Date lnsi:.lled_____ Time Installed ____ _ Date Picked Up -~--Time Picked Up ___ _ Com:.Ty:.F:. □.T:. 0:: - Flow. ____ CF/GPD Flow. ___ _ -- - Field pH Result ___ ~_ ~~~ate=a.-·-:-i-• ~C-ate] Please sign and return the white a*ellow copies to the Laboratory. r,J///' ------ T-805 c'.02 I Environmental Inc 111:tsultants. OEC I Certificate of Analysis I Client: OH!v! Corporation 2401 Tu.ckaseegee Road Charlotte. NC North Carolina Certification Number. J05 South Carolina Certification Number. 990J2 I I I Client#'. 381 Contact: Jack i<.ilbarger Sample Date: SDG#: 21-Nov-9~ SDG-000477 Lab Sample ID,LSID-001875 Receipt Date: 22-Nov-95 Report Date: 07-Dec-95 I S:unple ID: CO-WS-28 (_ ~ S't 1);~ er-cc,cr.-\.,-. ~ ") Project Manager Pa.ramcter 1, l,l -Trichloroethane 2,2-T etrachloroethar.e . Trichloroethnne Dichloroethane 1,1-Dichloroethcnc 11,2-Dichlorob<nzene l ,2-Dichlorocthane I ,2-Dichloroethene I l,2-Dichloropropane 1,3-Dichlorobenzene 11,4-Dichlorobenzcne · 2-Butanono 2-Hex;,none 14-Mctbyl-2-pentanone Acetone !3enzcne ~romodichloromcthane llaromo.fonn Bromomcthane l:aroon Oir;ullide "c.ubon T ctrachloridc .. I I Reportin2 Result Limit Unit Method Tlme u 5 ppb EPA 8240 18:J4 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18'34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 95 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 lll76 D,,-,,,u Rood -Plnnfilo. SC 281J< Ploone: (7~ 588--1()76 • FAX, (70.) 5811-%4!4 Page I Date 12/4/95 12.'4/95 12'4195 12'-1195 12/4195 12/4/95 11/4195 12/4/95 12/4195 !2,'4/95 12,'4.195 1214195 1214/9.S 12/4/95 12/4195 l2i4/95 12/4195 1214/9.S 12/4/95 1214/95 1214/95 Analyrt DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW I .Qmni Envirenm§Jl{gj_ won,rnltants. Inc •,~=~'''-'" .._,,~ ,, , LOIJ OEC I Certificate of Analysis I I I I I I I I I I I I Client: OHM Corporation 240 l Tuckase,:gee :toad Charlotte, NC Client ij: 381 Contact: J?.ck Kifoarger Sample Date': 21-Nov-95 SDG #: SDG-0004 77 Lab Sample ID: LSID-001875 Sample ID: CO-WS-28 North Carolina Certification Numb-er: JO!! South Corolina Certification Number: 99032 Receipt Date: 22-Nov-95 Report Date: 07-Dec-95 "'"""' '" ~ ~7 Project Manager ---------------------------- Reporting Parameter Result Limit Unit Method Time Date Analyst Cltlorobenzcne !J 5 ppb EPA 8240 18:34 12/4/95 DRW u 10 ppb EPA 8240 18:34 12/4195 DRW u 5 ppb EPA 8240 18:34 12/4/95 DRW V 10 ppb EPA 8240 18:34 12'4195 DRW Cls-1,3 •D icblnnJ~JfOf~.nc " < ppb EPA 8240 18:34 12'4195 DRW ,, -:)ibromochlommethane u 5 ppb EPA 8240 18:34 12/4195 DRW El.hvibcmcne ' . ,70 5 ppb EPA 8240 18:34 12/4195 DRW .\,!ethylene Chlor.de u , ppb EPA 8240 18:34 1214/95 . DRW ; Styrene u s ppb EPA 8240 18:34 12/4/95 DRW Tetrach!orctthene 175 s ppb EPA 8240 18:34 1214/95 DRW Toluene 45 5 ppb EPA 8240 18:34 12/4/95 DRW Total Xylenes soo s ppb EPA 8240 18:34 12/4/95 DRW :,i-ans-1,3 -Dichloropropene u 5 ppb EPA 8240 18:34 12/4/95 DRW Trichloroethtne F ., 5 ppb EPA 8240 18:34 12/4/95 DRW Vinyl Acetate u 10 ppb EPA 8240 18:34 1214195 DRW Vinyl Chloride u 5 ppb EPA 8240 18:34 12/4/95 DRW l ,2,4-Trichlorobemcnc u 20 ppb EPA 8270 10:00 12/1/95 DRW 2,l,.5-Trich!oropbenol u 20 ppb EPA 8270 I0·.00 12/1/95 DRW 2. 4,6-Trich!orophenol u 20 ppb EPA 8270 10:00 12/1/95 DRW 2,4-Dichlorophencl u 20 ppb EPA 8270 10:00 12/1'95 DRW 2,4-Dimethylphen•Jl u 20 ppb EPA 8270 10:00 1211195 DRW .. I 11176 ~ R0111d -l"tnevill,t,, :,,iC 18134 Phone: (704) ~S076-FAX: (i04) ~AR-24~ Page 2 I I !lmlli Environmental -..orrsui/ants. Inc I OEC Certificate of Analysis I Client: OHM Corporation 2401 Tuckasccgee Road Charlotle, NC North Caroliu Certification Number: 305 South Carolina Certification :'fambcr: 990Jl I I I Client#: 381 Contact: Jack Kilbarger Sample Date: 21-Nov-95 SDG#: SDG--0004 77 Lab Sample ID:LSID--001875 Receipt Date: 22-Nov-95 Report Date: 07-Dec-95 Approved By: I Sample ID: CO-WS-28 Project Manager Parameter I 2,4-Dinitrophenol 2, 4--Dinitrotolucnc .as-Dinirrotolucnc ~Chloror.a9hthalene 2-Chlorophenol I 2-Methlyphenol (o-,;resol) 2-Methylnaphthalene ' 2-Ni troani Ii ne I 2-Nitrnphenol 3,3-DichJorobe!l2idine I 3-Nitroanilino 4,6-Dinitro-2-methylphenol 4-Bromophonyl phenyl ether I 4-Chlora.nilinc 4-Chloro-3-methylphenol I 4-Chlorophenyl phenyl :thcr 4-Methylphenol (p<resol) 4-Nitroanilinc 4-Nitrophcnol I Acenaphtbcnc Acenaphtbylene .. I I Reporting Result Limit Unit Method Time u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb :CPA 8270 10:00 u 20 ppb EPA 8270 l0:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u so ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 11176 I>owns Rood. Ptnnille. NC = Pllono: (70.)511'-507~ -FAX: (>IM) 5111-2-15' Page 3 Date 1211/9.l l2.'l/9j 12/I/95 12/1/95 12/1/95 12/1195 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 12/1/95 l2/li95 Analyst DRW DP,W DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW I Qmr.i Environmental ~nsultants. Inc I Client: OHM Corporation C..'-'V ·oEC Certificate of Analysis North Carolina Certification Number: 305 I 240 l Tuckaseegee Road South Carolina Certification Number: 99032 I Charlotte, l\'C Client#; 33l &:ceipt Date: 22-Nov-95 Contact: Jack Kilbargc: Report Date: 07-Dc:c-95 I tflfF.;?:J-Sample Date: 2 l-Nov-95 I SDG#: SDG-000477 App roved By: Lab Sample ID: LSID-001875 I Sample ID: CO-WS-28 Project Manager Report.in~ Parameter Re.ult Limit Unit Method Time Date I Arnhracene u 20 ppb EPA 8270 10:00 12/1/95 Benzidine u 50 ppb EPA 3270 10:00 12/1/95 ~ (a) a.nth,..cene u 20 ppb EPA 3270 10:00 12/1/95 (a) pyrene u 20 ppb EPA 8270 10:00 [2/1/95 Bcnzo (b) r1uoranthcnc u 20 ppb EPA 8270 10:00 12/1/95 I Bcnzo (ghi) perylene u 20 ppb EPA 8270 10:00 12/1/95 Benzo (k) Ouoranth::ne u 20 ppb EPA 8270 10:00 !2/1/95 I Benzoic acid u 20 ppb EPA 8270 l0:00 1211195 u 20 ppb EPA ~270 10:00 12/1/95 I Benzyl alcohol . Bis (2-chloroethoxv) methane u 20 ppb EPA 8270 10:00 12/1/9S Bis (2-chloroethyl) ether I Bis (2-chloroisoprobyl) ctruer Bis (2-ethylhe:<yl) phthalate 1 Butyl ben:zyl phthalate Cluyscne Di-a-butyl phlhala!C I Di-n-<>etylphthalate Dibcnzo (ah) antJuacene Dibcn.zofuran IDicthylphthalatc Dimethyl phll\alatc .. I I u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 3592 20 ppb EPA 8270 10:00 3355 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 JO:UO u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 u 20 ppb EPA 8270 10:00 :U76 ~ ROM -!'lnr,\lle. NC lllJ.4 Phone: (70.) 588-5016. FAX: (704) !IU-2454 Pace 4 [2/1/95 12/1/95 1211195 [2!1195 12/1195 [2/1195 12/1195 12/1/95 12'1195 12/1195 12!1195 Analy.,t DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW DRW ' '''"'' ' '' ·1 • .. , -• ,.._ ,,, L.. ',, '' • l...CI ~• I 1.;L'..! i , 1'.,/1..J I ·Qmfil Environmentgl '97°nsultants. Inc OEC I Certificate of Analysis I Olent: OHM Corporation 240 I Tuckascegce Road I I I I I Charlotte. NC Client#: 3& I Conta(t: Jae.I: Kilbarger Sample Date: 21-Nov-95 SDG#: SDG-000477 Lab Sample ID:LSID-001875 51.IIlple ID: CO-WS-28 Par::uneter Fluoranthene renc chJorobenzene . . HexachJorobutadiene HoxachJorocyclopentadienc I Hexachlorocthane ll)deno (1,2,3-cd) pyrene I lsophorone N-Nitroso-<li-n-propylarnine N-Nitrosodiphenylarnine I Naphthalene Nitrobenzene Pentachlorophenol I · Phenan~nc Phenol PyTene I I Result u u u u u u u u u u u u u u u u Reportini Limjt 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Unit ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb ppb North Carolina Certification Number: 305 South Corolina Certification Number: 99032 Receipt Date: 22-Nov-95 Report Date: 07-Dec-95 Approved By: t!f1f:!:._ ;,;;:;;f:-C:urry 0 Project Manager Method Time Date Analyst EPA 8270 10:00 12/1/95 DRW EPA 8270 10:00 12/1.'95 DRW EPA s2·;a 10:00 12/1/9'5 DRW EPA 8270 10:00 12/1/95 DRW EPA 8270 1000 12/1/95 DRW EPA 8270 10:00 12/1/95 DRW EPA 8270 10:00 1211/95 DRW EPA 8270 I0·.00 12/1/95 DRW EPA 8270 10:00 12/1/95 DRW EPA 8270. 10:00 12/1/95 DRW EPA 8270 10:00 l2Jl/95 DRW EPA 8270 10:00 12/1/95 DRW EPA 8270 10:00 12/1,'95 DRW EPA 8270 10.00 12/1/95 DRW EPA 8270 10:00 12/1/95 DRW EPA 8270 10:00 l2il/95 DRW -. I lll76 llowN Rou • Ptnevilk, ~c :UJl:34 Phone: (704) S88-5Ol6. FAX: (704) 588-Z•~· P1ge 5 I I I I -1 I I I · .. I I I I I I I ,,.,· , .. _ '(' State of North Carolina Department of Environment, Health and Natural Resources Division of Solid Waste Management James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary William L. Meyer, Director 0 NA DEHNR July 31, 1996 Mr. Tom Broom Suburban Propane District Office 1333 Berryhill Road Charlotte, N.C. 28208 Subject: Soil Sample Analytical Results Cherokee Oil Company 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCD 980 799 019 Dear Mr. Broom: As you are aware, the NC Superfund Section collected two soii samples (labeled CO-005-SL and CO-006-SL) from two drainage features located on the Subu~ban Propane property, southwest of the main office building on March 6, 1996. The approximate soil sample locations are represented in the attached figure. These samples were collected to determine if releases from the subject site had impacted soils along the overland runoff path from the site. As most soils have some measurable quantities of metals, a background soil was collected from a grass-covered residential lot northwest of the site (CO-001-SL), within the same soil type as the soils found at the site, to represent the typical background soil conditions. The soil samples were then submitted to the State Laboratory of Public Health for volatile organics, semi-volatile organics, metals and PCB's/Pesticide analyses. The soil sample results are summarized in the table attached to this letter. The analytical results of the two samples collected on Suburban Propanes' property were then compared to the background soil analytical results to determine if the contaminants concentrations exceed three times the levels found in background. The contaminants found at elevated concentrations are highlighted by shading in the table. These contaminant concentrations were then compared to their respective EPA published human health-based soil exposure screening benchmarks. Contaminants that exhibit concentrations above this standard are noted by bold lettering in the table. P.O. Box 27687. Raleigh. North Carolina 27611-7667 Telephone 919-733-4996 FAX 919-715-3605 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post+,.:onsumer paper _,.I r1·2) I I _:I ~~· I ~· !L_I , ... ·~:,,. ~ The results -found numerous polynuclear aromatic hydrocarbons compounds, typically associated with oily wastes, at levels significantly elevated above background. In addition, . the soil samples contained elevated concentrations of bis(2-ethylhexyl)phthalate, PCB-1254, lead and zinc. Of the contaminants found at elevated concentrations m the two soil samples taken from the Suburban Propane. property, PCB-1254 and benzo(a)pyrene were identified at concentrations that could pose a health risk to people who are routinely exposed to the contaminated soil. However, the two samples were collected in relatively inaccessible areas not normally used by workers, and not accessible to the public. Therefore, the current risk posed to workers and the public by contaminated soil at Suburban Propane is considered minimal. Nonetheless, you should advise your workers to avoid disturbing this area and regularly maintain the fence surrounding this area to prevent incidental contact by trespassers. Also, removal of the contaminated soil may be necessary, if changes in the future use of this area result in human contact. Thank you for your help during our recent sampling trip. If I can be of further assistance, please contact me at (9 I 9) 733-280 I, e:xt. 315. cc: File Pat DeRosa Sincerely, Douglas Moore Environmental Chemist NC Superfund Section - ' 2.500.000 20 JO 40 M.r~1 ·-~ ·o 30 40 so l:'..ilome«••• '"' ',"", - 'i' ,. ' J.I~,, PALEOZOIC METAMORPHIC FACIES :Jiled by J. Robert Buller, 1984 '. - -- ---- - --- - - - -- 0 / , '1ming1on GEOLOGIC MAP OF NORTH CAROLIN, 1985 Scale 1:500,000 1 inch equals appro,imat,ly 8 miles a::a:::a:s::a:r ,o7Ja:EX,o~="ee=C''===i'°~="e~'c'==:::::i'°a,aa="e'='50 ~ilometrn t_ ---------------- G E 11111 IR 1¥.o;,\:iID 1,,,, ... ,1 IRE CJ JS"- L. ----<••"·" -----Fault ~ Pre-me~e thrust fault ~ _Post-mei.rno~ thrust fault -+--"'--!--:-_~Yldne- ~-Ovenumed 1n1ictine ~ Direction of plunge, 1. 0 R G A EXPLANATION MURPHY BELT CJ INNER PIEDMONT BELT HOT SPRINGS WINDOW CJ KINGS MOUNTAIN BELT GRANDFATHER MOUNTAIN WINDOW CJ SAU RA TOWN MOUNTAINS ANTICLINORIUM SMITH RIVER ALLOCHTHON ~ ' CHARLOTTE BELT BLUE R!DGE BELT -MILTON BELT CHAUGA BELT l""':!I CAROLINA SLATE BELT rf' 1,' q:o.'<:--0.i'' :.-;;:k)•- . ·-:~-' ,. ' --,---- "" SYMBOLS . 17 Tectonic laatrrre ,.':'if ~ ,ifu 35•-, .,. Well locatloo and basemiint . rock type Scale 1 :2.500,000 10 0 10 10 30 40 Min 10 0 10 20 30 40 50 .Kik>melars Gneiss ;, Graoltt Schist Volcanic rock --7(}()()-Contour in feet billow mean sea l11Vel oo pre-Mesozoic basement rock 10. Unnamed fault ,nd 11. Unnamed fault MAP SHO\NING MAJOR UTHO-.TECTONIC FEATURES REFERENCES FOR TECTONIC FEATURES 18. Dan River fault 11111 TRIASSIC BASINS DURHAM } SUB-BASINS SANFORD WADESBORO BASIN DAN RIVER BASIN (ORB) DAVIE BASIN {DB) ~ RALEIGH BELT c=J EASTERN SLATE BELT i!mington .. p ,. 28. New London syncline and 29. Troy enticiine ,. I li ~ 'l ; • 1-35" ,. Rankin. D.W., E,penshade, G.H., alkl Neuln4Jl, RB., 1972, Geologic IDllp ol lhe west half of the Winston. Selem Quadrnngle, North Camllna, \llrgnla. and T~ US. Geologlcal Survev ~ Stone. RW., 1912. Coal on Ck,n River. North Carollno: U.S. Geological Survey Bulktin 471·8, p. 137-169. 19. Newton anti!orm ~-~962~~~~ Geo1o!PcaJ lnvestigal!oN Map I-709-A · 12. Unnamed fault Abbott, RN., Jr., and Raymond, LA. 1984. Thchhe ~Suite, narthwtst Nortl, Carollna: meta· ~is;;n~~:~284.~~lory. 13. Br11vard tauft lcne ~;,ut;:~fw~c· .. ~~~ ~~t In ~h and :5?-!h ~~: I.!.,~:.. ~al Coldsmith, Rld.ani, Milton. O.J., and HOl1on, J.W .• Jr., In press, GroioQlc:map otO>ariotte 1• ~ Z-Quadnin. gle. North Carolina and South Carol!na: U.S. Geolo-= ri~-~ Ceobjcal lnuestigallons 20. Eulola laull Goldsm!tht ~ Millon, O.J., and Horton, J. W., Jr .• ~ North c:l~'~~~~ gical ~ArnmcllAb.tr&cts'Mthprograms, v. 14, oos. I and 2. p. 20-21. 21. Kir,p~ Mo1.mt;,in ~h,,,., rnn,> Mlooral~Bullettn75,26p. 30. Cob, cross-s1n1c1ure Md 31. Jonesboro faul! Campbd, M.R, and KlrnbaD, K.W .• 1923, Th! Deep River C06I 8elcl of North Carolina: North c:...rollna l2. Raleigh~ and Economic Survey Bulletin 33. 95 p. F"'!:!.~~~~~:~~ ~~• ~ Carolina. North Carolina Sllllll ~1 Norn,,,~., r;,,..,~ h~• -- ),UGA BELT, Tl:!ON, AND -J, ~TICLINORIUM ' lCKS _;,_· ·scale" schist and phyllonite, ~ tasandstone, marble lenses ;ranular, locally abundant potas· nd gradational with calc-silicate ... ,.ii?\ and amphibolite. Contains .; ! :·~i .:;,'rigly foliated; minor layers of ~--:-,; .. i' : or sillimanite occur locally; _\_ ::.;eous quartzite, calc-silicate .Jhyllite • "-~erlayered; minor layers and -~ o, mica schist. and granitic L. .C extrusive and intrusive rock; ?r-of mica schist, calc-silicate -~: .-mall masses of metadiorite "Jrl):~~--~·ered to massive; mega- .. lf·f·\,: .:5ch1st. amphrbolite, and :•.•\:...;;.-" •• "J ::·· 'i~rTiuscovite schist. contains rnanite ., \IOTITE SCHIST -Meta· j gradational with muscovite- .c rock ,n.KYANITE SCHIST -Meta- .. ,d gradational with amphibo- _and granitic rock ·and microcline porphyroblasts , ;ilicate rock. metaconglomer- (_\;and granitic rock iyllonite and inte~layered biotite '.akly foliated to massive. con- · .... y. larger megacrysts of quartz o foliated. granodioritic, mig- With arnphibolite 12 my; 27i -Megacrys11c, in , 351 my; 20.21) -Massive to > hiurn•bearing on cast side '· y ;an to Situn.an. 409 my: i 31 - tv,vell fol1aicd: contains b,otiic 1 38 my; 1_7)-Poorly foEated: STATE OF NORTH CA·I JAMES G. MARTIN, GOV_Ej l!lllli BJIJ ~ tlll1 CZ!v CZq CZph CHARLOTTE AND MIL TON BEL TS METAMORPHIC ROCKS FINE-GRAINED BIOTITE GNEISS -Massive to strongly foliated: minor layers of amphibolite and muscovite schist FELSIC MICA GNEISS -lnterlayered with biotite and hornblende gneiss and schist · BIOTITE GNEISS AND SCHIST -lnequigranular and megacrystic: abun- dant potassic feldspar and garnet: interlayered and gradational with calc-silicate rock, sillimanite-mica schist. mica schist. and amphibolite . Contains small masses of granitic rock METAVOLCANIC ROCK-lnterbedded felsic to mafic tuffs and flowrock MAFIC METAVOLCANIC ROCK -Metamorphosed basaltic to andes1tic tufts and flows, grayish green to black. Locally includes hypabyssal intrusives and minor felsic metavolcanic rock 1 FELSIC METAVOLCANIC ROCK -Metamorphosed dacitic to rhyolitic flows and tuffs. light gray to greenish gray: minor ma fie and intermedi- ate metavolcanic rock · QUARTZITE -Massive to well foliated: contains andalusite, kyanite, or sillimanite, chloritoid, and pyrite PHYLLITE AND SCHIST -Minor biotite, pyrite, and sillimanite. includes minor quartzite INTRUSIVE ROCKS j··-jd-:=_~ DIABASE -Dikes, gray to black r Pl'g DSg 00gb DOg GRANITIC ROCK {Pennsylvanian to Permian, 265-325 my, I'.'.') Megacrystic to equigranular. Churchland Plutonic Suite ('v\/estern group) -Churchland, Landis, and Mooresville intrusives GRANITE OF SALISBURY PLUTONIC SUITE (Devonian to Silurian, 385- 415 my; 5) -Pink, massive to weakly foliated. Gold Hi!I, Kannapolis, Salisbury, Southmont. and Yadkin intrusives SYENITE OF CONCORD PLUTONIC SUITE {Silurian, 40d my: c:I -In• eludes the Concord ring dike GAB BRO OF CONCORD PLUTONIC SUITE (Devonian to Orclovician, 399. 479 my; 24) -Barber, Concord. Farmington. Mecklenburg, and 1/1/ed- dington intrusives GRANITIC ROCK -Locally pinkish gray, massive to weakly foliated: contains hornblende SHELTON GRAN.ITE GNEISS {Silurian, 429 rny: :' ii -Poorly foliated, lineated granitic to quartz monzonitic gneiss METAMORPHOSED QUARTZ DIORITE -Foliated to rrnss,ve PzZg ! METAMORPHOSED GABBRO A.NO DIO.RITE -Foliated to massive --METAMORPHOSED MAFIC ROCK -Metagabbro, metad,onte and maf1c plutonic volcanic complexes META-ULTRAMAFIC ROCK -Metamorohosed dunite and peridotite. serpentinite. soapstone, and other altered ultramafic rock. Only !arge:- bodies shown . ~ METAMORPHOSED GRANITIC locally contains hornblende ROCK -Megacrystic, we!I foliated; I I I I I I I I I I I I I I I I I SYMBOLS \ ' -- -.,,, ,---{. i'?E. ;)_:,' :._. -· I : l_j T l ,~~;, ~ :,-,, '·I ,I !;·· /_J , i CZ THE HYDROGEOLOGIC FRAMEIJORK AND A RECONNAISSANCE OF GROUND-WATER QUALITY IN THE PIEDMONT PROVINCE OF NORTH CAROLINA, \JITII A DESIGN FOR FUTURE STUDY By Douglas A. Harned U.S. GEOLOGICAL SURVEY \later-Resources Investigations Report 88-1,130 Raleigh, North Carolina 1989 Ref. 23 (Ragland and others, 1983; Farrar, 1985; Russell and others, 1985; \,Jehr and Grover, 1985). Various periods of plate tectonic activity, along with the associated formation of rift margins, ar~ believed to·be responsible for tl1ese events. The Piedmont can be divided into northeast trending parallel geologic belts. Traversing frorn the southeast, the major geologic belts are the Carolina slate belt, the Raleigh belt, the Charlotte belt, the Kings Mountain belt, and the Inner Piedmont belt (Daniel, 1987). 'fhe rock-type classification scheme based on lithologic and geohydrologic properties developed by Daniel (1987) for the Piedmont and Blue Ridge provinces of North Carolina has been used in this study. The near-surfBce earth materials of the Piedmont consist of a three-stage system which, from top to bottom, contains (1) a regolith zone, (2) a transition zone, and (3) underlying fractured crystalline bedrock (fig. 2). REGOLITH Regolith unsaturated zone Regolith saturated zone SOIL ZONE- Lowest water table FRACTURED BEDROCK I / I / I ( / I I ' I ' ' ' ____,__ ' ' ' Roots Unweathered bedrock Sheet joint Bedrock structure I ~ 1----+--Fracture I I I Figure 2.--Conceptual structure of the Piedmont ground-water system (modified from Heath, 1984). 8 • • Collectively, the uppermos~ layer is the regolith, whi.ch is co[tiposed o·f sRprolite, alluvium, and soil (DarLie1 and Sharpless, 1983). The regolith zone consists of an unconsolidated or semiconsolidaced mixture of clay and fragmcntal 1naterial ro.ngi:1g i.n grain si;:e from silt to boulders. Saprolite is the clay-rich. residual 1naterial derived from in-place weathering of bedrock. Saprolice deposits represent leached deposits and, being granular 1naterial with principal openings between grabens, differ significantly in texture and chernical co1nposition from the parent rock which is unweathered, crystalline rock having principal openings along fractures. Since saprolite is the prodLtct of in-place weathering of· the par~nt bedrock, some of the textural features -of that bedrock are retained ~ithin tl1e saprolite. Evidence of relic quartz veins, dikes, and shear zones are commonly seen in outcrops. Alluvial deposits are unconsolidated sediments deposited by streams and rivers. Soil is referred to as the natural medium for the growth of plants. Saprolite is the dominant deposit in this unconsolidated zone, with soil deposits generally restricted to the uppermost layer, and alluvium deposits restricted to locations of current and former stream channels and river beds. The transition zone is where unconsolidated material grades into bedrock and consists of saprolite and partially weathered bedrock. Here, partitle size ranges from silts and clays to large boulders of unweathered bedrock. The thickness of this zone depends a great deal on the texture and composition of the parent rock. The best defined transitional zones are usually associated with highly foliated metamorphic parentl rock, while those of massive igneous rocks are often poorly defined or nonexistent (C.C. Daniel, III, U.S. Geological Survey, oral commun., 1985). In the Piedmont, 90 percent of the records for cased bedrock wells show combined thicknesses of 97 feet or less for the regolith and transition zones (Daniel, 1987). The uppermost part of the Piedmont crystalline bedrock contains numerous closely spaced fractures which can be related to the local and ~egional tectonic history of the area. As a general rule, very few fractures occur in the Piedmont bedrock at depths greater than 400 feet (LeGrand, 1967) . 9 ' ' I I I I le I ' IIYD!WCEOIJJClC FVAM.DJORK AND CONCEPTUAL H.OIJEJ. OF '111E f'LOl,I SYSTEM l!eath's (1984) concept of the grottnd-wacer system for the Piedmont and B.Lue Ridge provi11ces has been adoptecl as the conceptual mode]. for this study with slight modifications to emphasize the transition zone between the regoJ.ith zone and the bedrock. The fundamental structure of the ground-water system is shown in figure 2. The components of the syste,n are: l. The unsaturated zdne in the regolith, which generally 5ontains the organic layers of the surface soil; 2. The saturated zone in the regolith; 3. The transition zone between the regolith and bedrock; and 4. The fractured crystalline bedrock system. Regolith Unsaturated Zone The unsaturated zone extends from the land surface down to the water table, which is the top of the saturated zone. The pore spaces of the rcgolitl1 in the unsaturated zone contain both air and water. The tinsaturated zone usually ranges from 5 to 50 feet in thickness. Daniel (1987) found a mean depth to the water table of 31.3 feet in an examination of 2, 3?..6 Piedmont wells. Water moves down from the land surface through the soil zone by intergranular flow through the larger pore spaces ~nd passages left by burro~s or decayed roots. Ro~ts from surface vegetation can grow to 30 feet below land surface but more commonly spread laterally near the surface. At the base of the soil zone, which is generally 3 to 8 feet thick, chi average grain size abruptly decreases with a corresponding decrease in pore size as the water enters· the saprolite (C.C. Daniel, III, U.S. Geological Survey, written commun .. 1985). At this point water movement may also be diverted somewhat by relic structures of foliation or folds in the saprolite, which are remnants from the parent rock. The total porosity of soil is commonly around 55 percent, and its specific yield is about 40 percent (Heath, 1983). Saprolite has a total porosity of 35 to 50 percent near land surface (fig. 3), which decreases at depth, and a specific yield of 20 percent (Daniel and Sharpless, 1983). 12 . / / ' ' 60 1/. • / / '-I I I I I I I ~ ' ~ ' I I I ~ ~- ' • 50 Porosity • • :. ---C-,-~ \&..!•----··", ~ 40 ' . • • \ • • • • • ' >-f-\ ui 0 \ a: 0 n. 30 ' ' ,... z \ w 0 a: w n. I I ' 20 I I I ' 10 I 0 0 10 20 30 40 50 60 70 DEPTH, IN FEET Figure 3.-·Relation of porosity of saprolite with depth (after Stewart, 1962). Topsoil in Piedmont soils to a depth of 7 to 10 inches was reported to have a mean hydraulic conductivity of 5.7 inches per hour (11.4 feet per day), and the subsoil, 7 to 20 inches below land surface, has a mean hydraulic conductivity 1.8 inches values are in line with per the hour (3.6 feet per day) (Lutz, 1969). These hydraulic condu6tivity values for saprolite reported by Heath (1980) that range from 0.5 to 10 inche~ per hour (1 to 20 feet per day). However, same in all directions. the hydraulic conductivity of saprolite is not the This anistropy may take the form of preferential permeability along the direction of relic structures within the saprolite. Regoiith Satur;it:ed Zone The regolith saturated zone is. that interval below the water table and above the transition zone. Daniel has calculated the median saturated 13 L .. -,. ~-~ -~---.. ·-· ... I I ~ -~ ' ,, ' ' ' I I I It I I, tl1ickness of the regolith and transition zone from records of 1,749 water- supply wells in the ?iedmont of North Carolina to be 13 feet (Dani.e.l, 1987). The rnedian saturated thickness was shown to be a fur1ction of topography. beneath cl raws and valleys, it was 28 feet thick: below slopes and flats, it ·.,;as 15 feet; and beneath hills and ridges,-it was 9 feet. The saturated regolith provides the bulk of the water storage within the Piedmont ground--"'ater system (Heath, 1980). This concept is illustrated in figure 4. In the Piedmont ground-water system, the regolith has a specific yield of around 20 percent (Daniel and Sharpless, 1983), whereas the porosity of the bedrock ranges from 0.01 to 2 percent (Heath, 1984), The depth-porosity relation described by Stewart (1962) i.s shown in figure 3. The a~ount of ground water in storage as a function of the saturated thickness of the regolith has been calculated by Daniel (C.C, Daniel, Ill, U. S, Geological Survey, written commun,, 1985) and is presented as figure 5. ' ' ,· STORAGE IN BEDROCK Figure 4,--Water storage within, and the reservoir-pipeline conceptual model of the Piedmont ground-water system (modified from Heath, 1984). 14 11 :1 I I le I / ~ < w _, 0) < f--w f-,, ;: 10 u, a: 0 < a: w 8 (L (fJ z 0 _, _, ·< 0 CL 0 V) z Q _, _J 6 4 0 0 ,... :J 0 0 UJ a: CL 0 uJ (fJ < en TOTAL W/\TER IN STORAGE BELOW THE WATER T1\BLE \ ID 20 30 40 1\VAILABLE WATER \ 50 60 >-~ " w < ---' m < 5 >-(fJ a: 0 w z >-< < ;; _, 70 SA TUR/\TED THICKNESS OF REGOLITH. IN FEcT Figure 5.--Relation of (after C.C. Daniel, Ill, ground-water storage and saturated thickness U.S. Geological Survey, written corrunun., 1986). As illustrated in figure 4, the regolith serves as a reservoir supplying water to interconnected fractures within the bedrock. wells in the Piedmont are cased through the regolith, with open In general, hole through enough of the bedrock to intercept enough fractures to furnish acceptable yields. regoli th The bedrock fractures serve as pipelines between the well and the reservoir. data The depth to water table is largely a function of topography. Based on from 2,326 water-supply wells, the median water level in wells located in draws and valleys is 20 feet, in slopes and flats 25 feet, and in hills and ridges 32 feet (Daniel, 1987). Depth to water table at varies with ground-water recharge and continual discharge. 15 any one place An example of )_ ____ ----------··-- IY 1,lt •• 11· " II II II ' , ' ' ' I I I '-I I I che. response of water level due to variation i_n rainfall is shown in figure 6. In this example, groL1nd-water recharge (in excess of discharge) resulting from heavy -rains in late winter, when evapotranspiration is low, is reflected by a peak in the water-table ~ydrograph appearing a few days after heav:1 rainfall in late March. The t:ime after a storm that t:he peak appears in the water level is directly related to the vertical hydraulic conductivity of the material in the unsaturated zone and the depth to water table. The hydrograph also shows that little grv,1j_ng season (April through September) even recharge took place during though the area received the significant rainfall during these months. The declining ~acer level indicates continui.ng ground-water discharge that is not.equaled or exceeded by rcchar-g,e until fall., when evapotranspiration is low. Similar seasonal 3 0 -' w en z -' w > w s -' 0: w ,... <t 3 a 4 "' w r u "' z z 2 0 ,... <t C: "' u w 0: n. 10002 Precipitation at Aflonlo 1980 Figure 6.--Response of water-level change to rainfall (from Gressler and others, 1983). 16 ,r of tl1e water cable are also showr1 in the hydrograph for a ~ell r_ll/ / fluctuations ' located in Iredell County, North Carolina (fig, ,t i ~ 7), " ~ la r, 1ft ~ I i I I ·I ~ I I :: t ,o I :: tL,___L_____,,___,,L____L__l__j__~__J______L___,_____,__j___' 19 ;· 2 I 9 7 3 1 9 7 -4 197 5 l976 1977 1978 19 79 1980 Figure 7. --Seasonal fluctua:ions in water-table depth in a well in Iredell County, North Carolina (from LeGrand, 1984), Transition Zone 198 1 At the base of the regolith there is generally a transition zone of weathered rock, boulders, and saprolite, Careful augering of three wells showed this transition zone to be approximately 15 feet thick at the Guilford County, North Carolina, test site shown in figure 8 (C.C. Daniel, Ill, U _ S, Geological Survey, written commun,, 1985), This zone has been found in Georgia, Maryland, and North Carolina and reported by Stewart (1962), Nutter and Otten (1959), and Daniel (C,C, Daniel, III, U,S, Geological Survey, written commun,, 1985), respectively, They describe this zone as being more permeable than the upper regolith and slightly more permeable than the soil zone, This observation is substantiated by reports from well drillers of so-called "first water" (C,C, Daniel, III, U,S, Geological Survey, written commun,, 1985) in drillers' logs (Nutter and Otton, 1969), The high permeability of the transition zone is probably due to incomplete weathering in the upper regolith, Chemical alteration of the bedrock has progressed to a stage of minute fracturing of the crystalline rock, yet it has not progressed so far that the rock minerals have been altered to clays, which would clog the tiny fractures (C,C, Daniel, III, 17 I I '1 11 11 11 11 11 11 I .. 11 11 11 !1 / / ' I Transition zone Soil zone Clay, silt, and sand Residual Weathered boulders Unaltered rock o.11/( 1\//1 'V 1~~11£ -:, . --·' :-_ ~-?; ~--:<: . .::::-::-. -.:. /- ·-:"::::::, .. ~ ---- -_:__C>-. <..___: / .-> -.·.L ~.· "' r ~~( . . . -... <~ ----· . . . .'/ c,·.· : .. J_,,-,. ~--.-.. (f) w (f) < w a: 0 ;;:; (.') ;;:; a: w I >-< llJ ,: LL 0 w w a: (J w 0 RELATIVE INCHE1\SES PERMAl31UTY I t: _j 0 (J w a: (f) w (f) < w a: 0 ;;:; Figure 9.--An idealized weathering profile through the regolith showing relative permeability (after Nutter and Otten, 1969). The presence of a high-permeability zone on top of the bedrock may create a zone of concentrated flow within.the ground-water system. Daniel (C.C. Daniel, III, U.S. Geological Survey, written cornmun., 1985) cites the case where well drillers find water in the transition zone, yet end up with a dry hole after setting casing through the regolith and transition zone into the unweathered bedrock. In this case, the ground water occurs primarily in the transition zone, where there is poor connection between the regolith reservoir, the bedrock fracture pipeline system, and the well. Daniel comments that the transition zone may serve as. an interval where relatively rapid movement of contaminated ground water can take place. 19 I ' ' ' ~ ~- ~ ~ ,,. '1 '• ,. '• 11 11 ! .. ·1 I / / Fractured Bedrock Ground-water flow within the crystalline bedrock occurs within fracture systems. LeGrand (1967) discussed what he_ considered to be the six common types of fracture patterns (fig. 10) that influence yields to wells. These fractures are reported to be more common near the surface and beneath valleys, draws, and surface depressions (rteath, 1980), and are considered to be zones of weakness that allowed the initial development of valleys and draws at these locations. Fracture openings are wider near the bedrock surface and decrease in size and number with depth due to increasing lithostatic pressure. >------------ ~ A Unlractured rock 3 percent '.1/J -< / "\ , // / / ' / / I / / D / ( 32 percenl -----_...,. ___ _ B 20 percent ----- E 25 percent EXPLANATION Water table Rock fracture C 1 s percent F 5 percent 5 percent -Frequency of occurance for each fracture system Figure 10.--Six common types of fracture systems in the Piedmont (from LeGrand, 1967). 20 I I I I I I .. I Heath indicates that few fractures below 300 to 400 feet from land surface contain substantial amounts of water, and that those which do bear water at depth are probably associated with faults. However, Gressler and others (1983) found that for the Atlanta, Georgia, area, nearly horizontal stress-relief fractures at depths of 400 fee~ or more were often associated with high-yielding wells. When surface material is removed by erosion, nearly horizontal stress-relief fractures develop and widen in response to the reduction in compressional stress. Daniel also reports high-yielding wells at depths over 500 feet in the North Carolina Piedmont (Daniel, 1987). Fractures are µlanar features oriented along zones of lithologic and structural weakness. Water can move along the fractures with relative ease to discharge points such as wells or to natural discharge areas in stream valleys. Non-horizontal fractures may account for dramatical_ly asymmetrical patterns of water-level decline that may be seen around a pumped well or the more rapid movement of water and contaminants in one direction than in another, creating aniostrophy in the bedrock aquifer. The hydrologic conductivity of the fractured bedrock is generally 0.001 to 3 feet per day (Heath, 1984). The primary porosity of the bedrock ranges from about 0.01 to 2 percent (Heath, 1984). In general, the mineral assemblages determine the degree to which water will dissolve aquifer material. For example, quartz is resistant to chemical weathering and will dissolve much more slowly than les? resistanc. ferromagnesium minerals such as biotite and hornblende and numerous iron minerals such as pyrite and magnetite. Generally, the mafic igneous rocks such as diorite-gabbro contain more ferromagnesium minerals and are more susceptible to chemical solution than the minerals of felsic rocks such as granite. Weathering of the ferromagnesium minerals produce solution openings and channels in the mafic rock units. Ground _water from a typical granite, composed largely of sodium and potassium feldspars, should have relatively high concentrations of sodium bicarbonate. Calcium and magnesium bicarbonate concentrations can be high in ground water moving through mafic rocks, such as gabbro, which is composed largely of calcium feldspars and ferromagnesium minerals. Ground water from certain rnetavolcanic and mica-schist units contain high concentrations of iron (Hem, 1970). However, these simple relationships are complicated if there is ·mixing of waters from adjacent rock types of different compositions or if the host rock is intermediate in composition . 21 I Because the natural chemical quality of ground water is affected by the minerals in the regolith and bedrock, which form the hydrogeologic framework for the Piedmont ground-water system, the natural water quality should -be considered when attempting to determine water-quality differences resulting from different land uses. The significance of the effects of geology and soils on the ground-water quality are described in the data-analysis section of the report. Flow Hypotheses Several aspects of the ground-water flow system in the Piedmont are particularly significant geochemically. In describing ground-water recharge and discharge and the functions of a ground-water system, Heath (1983, p. 14) states: Hydraulically, this system serves two functions: it stores water to the extent of its porosity, and it transmits water from recharge" areas to discharge areas. Thus, a ground-water system serves as both a reservoir and a conduit. Water enters ground-water systems in recharge areas and moves through them, as dictated by hydraulic gradients and hydraulic conductivities, to discharge areas. In the humid part of the country, recharge occurs in all interstream areas--that is, in all areas except along streams and their adjoining flood plains. The streams and flood plains are, under most conditions, discharge areas. These general conditions are assumed to apply in the Piedmont of North Carolina. The generalized flow system in the Piedmont as represented in figure 11 occurs within a closely-spaced network of streams typical of the mature topography of the Piedmont. Ground-water flow is toward these streams, and the shape of the water table mimics the topography of the land surface, 22 EXPLANATION ----+-General direction ol ground-water movement Sh~t Joints Tectonic Joints Water table Ground-waler d!acharo• area Figure 11.--Generalized ground-water flow system in the Piedmont (from Heath, 1980). although with subdued relief. Thus, surface topography can be used to predict the natural direction of ground-water flow. The distance between the point where a drop of water or waste enters the s~:stem and the point where it discharges into the stream down slope is commonly less than a half mile (LeGrand, 1958). Most of the natural flow in the system is probably confined to the upper 30 feet of bedrock, where fractures are concentrated, and the overlying transition zone, which apparently has the highest hydraulic conductivity of any part of the hydrogeologic system (C.C. Daniel, III, U.S. Geological Survey, written commun., 1985). However, flow probably also occurs in the deeper fractured system in a manner harder to predict by local surface topography. In the deeper system, regional topography or structural features may result in flow over long distances and long ground- water residence times in the fractured rock. The ground-water flow system in the Piedmont is directly connected to the surface-water system. The annual contribution of ground water to total streamflow for 11 streams flowing through the Piedmont is estimated to average 44 percent (Harned and Daniel; 1937). Consequently, it is a concern that ground-water contamination will eventually discharge to streams that are water-supply sources. 23 I .. I I Because of tl1e interconnection of the ground-and surface-water systems ir1 tl1e Piedmont, a drainage basin large enough to contain a perennial stream can serve as a basic unit for the description of ground-water quality (LeGrand, 1984). Each drainage basin is a flow-system cell similar co, and yet separate from, surrounding basins. Although not all of the ground-water fiow for a particular area is confined within a single drainage basin, it should be possible to generalize, with a reasonable degree of confidence, about ground-water quality of larger regions from data collected in small drainage basins. This is a basic assumption used in this study. Hypotheses about the Piedmont ground-water flow system relevant to this and future studies of the system include: 1. The transition zone between bedrock and regolith serves as a primary transmitter of contaminated ground water. The regolith serves as the principal reservoir of ground-water contamination. 2. Attenuation of ground-water contamination in the regolith is related to the degree of weathering and composition of regolith material and the hydraulic conductivity, gradient, and porosity of the material. 3. The velocity of contaminant movement can be highest within the fractured bedrock system, particularly under stressed conditions. l+. The deeper zones in basement rock generally contain the best quality water in the system due to contaminant attenuation in the regolith. 5. Geomorphological analysis can be used to identify fracture zones that help predict general subsurface-flow patterns of ground-water contamination: These. methods can be verified with surface geophysical techniques. Transition-Zone Stu.dies There have been some initial tests of the hypothesis that the transition zone is a principal conduit of ground-water movement and ground- water contamination. Daniel was the first· investigator to focus on the transition ·zone and has. done some initial test drilling, .well construction, and well logging to define its characteristics. In particular, temperature logs run in several wells located in Cary and in Guilford County, North 24 i le i I I ii I ' ' rf' ' ' ' I ' I le I I ·----=-------" LAW ENVIRONMENTAL PHASE Ill ASSESSMENT EXPLORATION GENERAL ELECTRIC SERVICE SHOP CHARLOTTE, NORTH CAROLINA VOLUME I PREPARED FOR GENERAL ELECTRIC COMPANY SCHENECTADY, NEW YORK DECEMBER, 1988 • • ' le. • • I I I PHASE III ASSESSMENT EXPLORATlON ' GENERAL ELECTRIC SERVICE SHOP CHARLOTTE, NORTH CAROLINA I ' • Prepared for ~ GENERAL ELECTRIC COMPANY • ~ ~ ~ Prepared by I LAW ENVIRONMENTAL, INC. ' I December, 1988 ' .. • ii I .,.·1 ) • ' I I ll I I I _. ' ' ' I ' ' --1 ti storage tanks. However, sand was used to '!:ill the excavations created during removal of the underground storage tanks. The residual soils consist primarily of sandy micaceous, sometimes clayey silts. Approximately B feet of clay was encountered in the boring for MW-7. The depth to the top of bedrock, as determined by auger refusal in MW-7, was 73. 8 feet below ground surface. Ground-water elevations were obtained from all monitoring wells on site on August 26 and 31, September 12 and November 3, 1988. The ground-water elevations measured in well D-3 are considered suspect owing to the amount of free product in the well. The floating product, being less dense than water, will result in a higher fluid level but a lower ground-water level. Electronic water-level indicators were used to measure water levels in the wells in August and September. The water-level elevations measured in well D-3 in those months are significantly lower than those measured in nearby wells D-1, MW-5 and MW-6 due to the electronic water-level indicator measuring the depth to water and not the depth to free product. The elevation measurements on November 3, 1988 were made with a chalked tape and resulted in a much higher fluid level elevation in well D-3. The differences in measurements for well D-3 indicates a product thickness of approximately 5 feet. The data are summarized on Table 2. The potentiometric surface, as determined from water level measurements on September 12, 1988 and illustrated on Figure 7, indicates the ground-water flow direction within the site area to be generally to the south-southeast. This trend is relatively 14 • • • " I II " " p 111 " 11 " ll ,1 ll Ii Ii II ~ I I! 4 consistent with the past potentiometric data base. The average ground-water gradient was calculated to be approximately o. 02 feet/feet in the site area. Ground-water elevations measured in well MW-7, with a screen depth of 63.8 to 73.3 feet, vary only slightly from ground-water elevations measured in the adjacent, shallow wells D-1, MW-4 and MW-6. This comparison indicates the lack of a significant vertical gradient. Data obtained from "slug" tests performed on six of the site wells indicate hydraulic conductivity (K) values ranging from -4 . -5 6.17 x 10 cm/sec in well MW-4 to 7.28 x 10 cm/sec in well MW- 7 (Table 3). The average K value for the wells tested, excluding well MW-7 as it is screened significantly deeper than the other wells, was calculated to be 3.68 x 10-4 cm/sec. Results of the physical tests performed on the two undisturbed samples collected from MW-4 are presented on Table 4. Permeability values 2.98 x 10-5 cm/sec for the two samples were calculated to be (15.5 -17.5 feet) -4 and 8. 09 x 10 cm/sec (30.5 31.5 feet). Total porosity was determined to be approximately 38%. Using the average K value calculated from in-situ hydraulic -4 conductivity tests (3.68 x 10 cm/sec), the calculated ground- water gradient (O. 02 feet/feet) and an effective porosity of approximately half the total porosity (0.20), the ground-water flow velocity was calculated to be approximately 38 feet/year. 15 • I a. I I I I I I .I _. Ii I I I • I .. I I TABLE 3 ( SUMMARY OF HYDRAULIC CONDUCTIVITY TESTS PHASE III ASSESSMENT GE SERVICE SHOP CHARLOTTE, NORTH CAROLINA HYDRAULIC CONDUCTIVITY SLUG-IN SLUG-OUT AVERAGE WELL NO. ( cmLsec) (cmLsec) ( cmLsec) D-1 3.90 X 10-4 5.13 X 10-4 4.52 X 10-4 MW-2 1. 63 X 10-4 1.97 X 10-4 1. 8 X 10-4 MW-4 5.83 X 10-4 6.51 X 10-4 6.17 X 10-4 MW-5 1.67 X 10-4 3.24 X 10-4 2.46 X 10-4 MW-6 2.98 X 10-4 3.90 X 10-4 3.44 X 10-4 MW-7 6.66 X 10-5 7.89 X 10-5 7.28 X 10-5 NOTES: 1) Hydraulic conductivity values were calculated using the Method of Bower and Rice (1976). 2) Table prepared October 5, 1988. ., I • • • ' f--:, ' ' ' ' ' ' I ,. ' ' ' I q q Cl fl March 3 I, I 99 5 Mr. John T. Harrsen Manager, Remedial Programs General Electric Company Building 2, Room B43 One River Road Schenectady, New York 12345 Subject: Report of Ground-Water Sampling and Analyses General Electric Apparatus Service Center 2328 Thrift Road Charlotte, North Carolina STATE FILt. RECEIVED JUN 2 6 1995 SUPERFUiW SECTION Law Engineering and Environmental Services Project 13210-5-5010 Dear Mr. Harrsen: Law Engineering and Environmental Services (LAW) is pleased to report the results of our ground- water sampling and analyses for the former General Electric (GE) Apparatus Service Center in Charlotte, .North Carolina (Figure I). The sampling and analyses were requested by Mr. Thomas Power of the State of North Carolina Department of Environmental Health and Natural Resources (DEHNR) in a letter dated 4 January 1995 to GE's Christopher Allen. GE retained LAW to. perform the work, which was done in accordance with Proposal 13210-5-0015, dated 24 January 1995. FIELD ACTIVITIES On 31 January 1995, the depth to static ground water was measured from the top of casing at each of the 14 wells (MW-I through MW-10, S-25, D-1, D-3, and 0-5). Ground-water elevations, referenced to an assigned datum, were calculated from the depth measurements. The 14 wells were also checked for siltation by measuring total well depths and comparing those to well installation records. No significant buildup of sediment was present in any of the wells. Table I presents the ground-water elevations measured. Table 2 presents the siltation measurements. Figure 2 presents the ground-water potentiometric surface map. LAW ENVIRONMENTAL, INC. 112 TOWNPAR:\ DR\VE • KENNESAW. GEORGIA 30144 (404\~21-3400 • FAX (404)421•3486 i I.\ 11 1: 11 Iii 11 1: 1i ' ' ' ' ' t ' 1 ' ' Report of Ground-Water Sampling and Analyses-CE Charlotte. :\'C Law Engineering and Environmental Services Projecl /32/0-5-50/0 Table 1: Fluid Level Measurements Monitoring TOC Depth to Depth to Free Oil Well Elevation Ground Water Free Oil Thickness MW-I 705.70 28.81 ND NA MW-2 700.77 28.24 ND NA MW-3 705.70 27.76 ND NA MW-4 699.06 24.60 ND NA MW-5 699.01 26.72 ND NA MW-6 699.27 24.45 ND NA MW-7 702.34 27.90 ND NA MW-8 698.56 30.06 ND NA MW-9 696.63 26.44 ND NA MW-10 697.83 26.08 ND NA D-1 703. 77 28.78 ND NA D-3 702.23 29.03 27.35 1.68 D-5 705.85 28.00 27.40 0.60 S-25 699.91 28.90 ND NA Prepared by: March 3/, 1995 Ground-Water Elevation 676.89 672.53 677.94 674.46 672.29 674.82 674.44 668.50 670.19 671. 75 674.99 674.68* 678.38* 671.01 1/H / 3-:/',-~,- All measured in feet Checked by: 1J>-J 'Ji 1-<.,:J.-rr Fluid levels measured on 31 January 1995 Notes: ND: Not detected NA: Not Applicable TOC: Top of Casing *· Corrected for free oil thickness, assuming S.G. of oil = 0.88 GW elev.= TOC elev. -Depth to free oil -0. 12 (free oil thickness) MEMO Date: To: From: Topic: 01/25/93 File Douglas Moore lbugi~-, Environmental Chemist NC Superfund Section Intakes for the Charlotte-Mecklenburg Water System Dynatech Industries Site -NCO 981 014 517 On Monday, January 25,1993, I spoke with Mr.Terry Gross, Water Treatment Plant Consultant with the Public Water Supply Section of the Mooresville Regional Office (1-704-663-1699). Mr.Gross stated that there are three intakes for the Charlotte Mecklenburg Water system; one at Mountain Island Lake, two at Lake Norman. He stated that there are no intakes along Irwin or Sugar Creek, or South of Charlotte. The town of Pineville gets its water directly from the Charlotte Mecklenburg system. DM\D2GROSS Ref. 25 I -. I I I I I I I .. I I I I I I .. I I Memo Date: August 9, 1996 To: From: File Douglas Moore Environmental Chemist NC Superfund Section Subj.: Groundwater use within a 4.0 mile radius Cherokee Oil Company site 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCD 980 799 019 During the August 9, 1995 on-site reconnaissance, no groundwater well users were identified within a 0.5 mile radius of the site. However, a survey map of groundwater use near Paw Creek (attachment 1), identified 43 houses within a 3.0 -4.0 mile radius of the site that currently have groundwater wells. Multiplying the number of houses ( 43) by the 1990 US Census average of persons per household for Mecklenburg Co. (2.50), an estimated 108 people use groundwater wells for the primary drinking water source within a 3.0 -4.0 mile radius of the site. According to the North Carolina Public Water Supply Section printout (attachment 2), there are five community wells within a 4 mile radius of the site. The numbers to the left of the system name correspond to the numbers on the site topographic map. Distance Rin<> Svstem Name Pooulation 1.0 -2.0 miles Mineral Springs 108 2.0 -3.0 miles Juniper Drive 94 Farminoton 109 3.0 -4.0 miles Trexler Park 114 Parkwood MHP 157 I I I I I I I .. I I I I I I .. I I Memo to File GWUse Page 2. Summing the population numbers for private and public water systems, Distance Housecount Private Well Community Community Radius Pooulation Wells Pooulation 1.0 -2.0 miles 0 0 Mineral 108 Snrinos 2.0 -3.0 miles 0 0 Juniper Drive 94 FarmimJton 109 3.0 -4.0 miles 43 108 Trexler Park 114 Parkwood 157 MHP Estimated GW Pooulation 108 203 379 ,, .• · ''w"'"•'e1'"''"1'1'' ' ., • . . .. s··· . ':•::: ' .: ,,; ,-,:::: :::;: ;!; -;: ~!i~-; -'.t[;~mim;~:: '' t I \M;J,~i~i t i~!!il ::' -·-:!r:: -_ ::--)\~m~mll;: r\;H;~\f" t!!,iii.'t ;; 'I '-'~1~;:le!!li,e:::,}:::ili!!th•···'·'·.····· il;j"i '',,, , f 7 •.• , . vYe!' S': over" e. uflAK.! ~ -.·. -I .. -; ,. . . ... I ,~" wi ;:::i\ji! [F](sc::%[ .Y:tt\~; '.fi:t:::::· _ ::frn: !\Ut;;;~;" _ _ _ _ : ::;l; ;rrr1? "'" ,.,, ••'-'"" """"'· I ts'urfi~~1::iWa~~r I ., ,· .. , ... , .. · .. ,. ·. ·· .. ' ! :;:.: ;f, 'f 's .. ·t. ··r.e' a· m·· >;sam·. . . .·. . . • ·1 ·1· m;. . . \ :,;-;_;· :-'.\ .--". . 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"!_C. 7t.>t':59i:.~':!,'7 l.JELL C5f'"0~· f -;:. •· 160668 DWYERS UNION •76 5(, .7C·43':-E,~S'.::-2 '.JEL!... · ··3. , __ 160672 GIBBON S'HOPPHJG CEt.;1~;:. l·i ~--:: i'C,-i':~~~<:C:.CS LJEL:.. c- --~!;,;··••1G06B0 OAKDALE BAPTIST C!i!..,1~:c;-1 r~ !2(: 7(•43-?:•n:·,.':; !~ELL -15:0681 ROCK OF AGES BAP-TI~7 c.~l (/ 5(' 7n.:53e,~..:';l•? 1,1.:::.t 160702 SHIRLEYS CHILD ChRE F so 7('~ss;:;;,s:·:;._; ,,Ji::/.:. 160707 160710 160717 160732 160763 160777 1607B2 160792 KINGDOM HhLL OF .JEHCVH'~C: SOUTH 21 T:-IRIFT ROP!) CHRISTIA!~ ;:>;:_,~'.CH RUMORS LOUrJGE " NORTHWEST AUTO AUCT l 0:-.: JAMISON r1EATS. I !K NIDSTATE AUTO AUCTiON GIBSON~, FOOD 510R£ CH;.Ri___ !J " • 7(-•;'~,91,,~;;,. 7,_ .:3-:-2f•. ·U~:.u;(,. _ '.ca 7,:,~537~::;,3 7('--1334~1. :-·G 7(,-l':,S'GC•: ·::: ! 11Cl ~ 1,iE~L .:F.:.s.. 1,1!::::LC- !JELL !,IEL:... t.lEi • IJEU_ :?-:-G .P G p G .. p G p G p G p G p G p G p G p G p G p G· p G p G p G p G p G F G p G p G p G p ,. p 351630"' 805300 351630 . 805300 351419" ,80502€1 · 2s 1 eoo--9,..rS,,?G· . ·.--; 0351618 805436 . .,,:.~ .. ~351618. 805436 ,,._ ·~ -1,_---~ . ..,.,...;.351700· 805200 351510 805510 351700 eos:::oo ·;,--.,-· ·:··351700 805500 .1 · . .-,:·; 351407 805635 =-.,,,::-:_ 351402 805630 ~351-404 805627 351"1(•5 805620 351250 805730 351256 805730 3~1755 805653 351641 804913 351335 805625 351700 805647 351746 804738 35!745 6•J48•)0 35; 7,;5 80'1800 3si 730 8(H745 ,'35!800 804815 351800 804830 35t8C"0 80483('1 351730 805407 3516-iS Bfl5(n:,o 3':-l7"'i5 E:J51 L"'IO 3Sl·715 e1)5E:. 37 351713 605.:27 351515 2os:::1s 351050 8051 15 35173.J 805-145 35152 . .; S048~4 351730 8051i-45 35174 ! 604738 - --- --- - ---- -- - .,_ >"t-,..,.;u,. - I I I I I le I I I I I I I •• I MEMO TO: FROM: DATE SUBJECT: Supcrfund Section Staff Jeanette Stanley · Environmental Chemist NC Supcrfund Section January 2, 1996 Update on Status of Wellhead Protection Programs in N:C. 1 spoke with Mr. Randy Prillaman, 1-lydrogeologist, NC DEM (919) 715-6187. He said that the Wellhead Protection Area implementation plan written by him and submitted to US EPA in late December 1994 has been approved. This plan calls for protection of a whole area based on a calculation using recharge rate and pumping rate as variables. North Carolina now has primacy in approval of wellhead protection areas. None have yet been implemented. The Rural Water Asso_ciation is preparing to submit several applications for wellhead proptcction, but none have yet been received or approved. Some areas he expects to be'thc first to have wellhead protection areas are Gaston County, the Town of Black Mountain, and numerous small communities affiliated with iiie North Carolina Rural Water Association. Gastoi1 County has ·delineated wells and completed ii contaminant source inventory. I I I I I I I t' I I I I I I la I I •• ,•, ---~• (i.><,,:,,•,. SJ, '.t.,•} .;",1. •! i, t•l f.'.,;,,1(,0~,l~c. . . '·'\'.:_;~.-{t) ;j;~~~f~r;1r:r~~~~~~1~~ ., ·.-:-t'<.;1 >t•··· :::rz.;.~•···~•:i:~•!-'~~ i-~~~'!' ::,i. :i;it/~-~~~~-:~1 ~tf~i: :-'\.k._{cr!~. . :.:~::-:rt/~~tti;~f~{~;i:;· ~rfi#t:~: .-:. ~!Ji.~-~~•:fvi. ~;t ~:}.~~·<. ,., . . , . .. ,.-, ·· ,)GJ'.C/::, NATIONAL FLOOD INSURANCE PROGRAM FLOOD INSURANCE RATE MAP CITY OF CHARLOTTE, NORTH CAROLINA MECKLENBURG COUNTY (SEE MAP INDEX FOP. f't,.f~[L; NOT PAINTED) PANEL 8 OF 31 COMMUNITY-PANEL NUMBER 370159 0008 B MAP REVISED: FEBRUARY 26. 1982 federal emergency management agency federal insurance administration \\ • I I ... •••••• I .. I I I 'O' \>ov ..,,., C,"' I I I ,. I 0 • t"' ! ; 1•-, f. i i 1111 lillll i I I CJ LEGEND SPECIAL FLOOD HAZARD AREAS INUNDATED BY 700-YEAR FLOOD ZONE A · No base flood elevations determined. ZONE AE Base flood elevations determined . ZONE AH Flood depths of 1 to 3 feet (usua. ol po'nding); base flood elevations de ed. ZONE Ab Flood depths of 1 to 3 feet (usually sheCt flow on sloping terrain); average depths deter- mined. ·For areas'"' of alluvial fan flooding; velocities also determined, ZONE A99 To be protected from 100-year flood by Federal flood protection system under con- struciion; no base flood elevations deter- mined. ZONE V Coastal flood with velocity hazard (wave action); no base flood elevations determi'ned. ZONE VE Coastal flood with velocity hazard (wave adion); base flood elevations determined. FLOODWAY AREAS IN ZONE AE OTHER FLOOD AREAS ZONE X Areas of 500-year flood; areas of 100-year flood with alierage depths of less than 1 foot or with drainage areas less than 1 square mile; and areas protec1ed by levees from 100-year flood. OTHER AREAS 2 ONE X Areas determined to be outside soo:year flood- plain. ZONED Areas in which flood hazards are undeter- mined. UNDEVELOPED COAST Al BARRIERS! Identified 1983 Identified 1990 or later Otherwise Pro1ec1ed Areas t(oastal barrier areas arc normally located within or adjacent to special flood hazard areas. ---513--- @-----@ IEL9871 Floodplain Boundary Floodway Boundary Zone O Boundary Boundary Dividing Special Flood Hazard Zones, and Boundary Dividing Areas of Dif-ferent Coastal Base Flood Elevations Within Special Flood Hazard Zones. Base flood Elevation Line; Elevation in Feet• Cross Section Line Base Flood Elevation in Feet Where Uniform Within Zone• Elevation Reference Mark Rivet Mile •Referenced lo the National Geode1ic Vertical Datum of 1929 NOTES This map is for use in administering the National Flood Insurance Program; it does not necessarily identify all areas subject to flooding, particularly from local drainage sources ol small size, or all planimetric feature5 outside Special Flood Hazard Areas: The community map reposi1oryshou!d be consulted for possible upda:ted flo".d hazard information prior to use of this map for property pllr ase or <.onstruct1on purposes. Coastal base flood elevations apply only landward of 0.0 NGVD,and incl e effects of wave action; these elevations may also differ significantly from those developed by the National Weather Service for hurricane evacuation planning. Areas of special flood hazard (100-year flood) include Zones A, AE, AH, AO, A99, V, and VE. CcrtJin areas not in Special Flood Hazard Areas may be protected by flood control structures. : ; ,,:::;,: , . >i :_j:;~: (:~~, >;;. :::,,:. ·•. · ,,;;,c~r;.,.:r,:1i?!J!.%11:'i'' .· · "'" "" " -"•·,,:;1;1:r•?!;.:/1\I(;tt~t;9ti';;1,:§:! I .:;_;,_-:: >t' I I I I I I I I I I I I • ·t• Jt ·i ,;:~.J~~iT·~!.J~ ... , ... . ~:.:.~?t::ui·f~~~FJ:i; -.. -: ~\~\::t}tt~{;?~tr. ·• .. ,,, • -;;· ! f,-;. ''l::Jf::..:;.1k~~~i r • ,· •,, • • ' ~'"'4.;, f}-1,; •,,,,tJi • ' • ' ~ ',, ::,_' l r;, ~;_,";!., ~'..{r/fH~ •.~.-. :~ ~~/-. _.·:f i;;J.~;;~1!1:t ., .. ~ ··~ ·~r .:,. -';t,;~·::t~:.:~·ifJ!~~ . ' -~· ~· ~-~.;; :.:· ·-1: :.!1-~;<;-:-}f,t~~~~· ~ :.I ,'{15(=·· ~ .. •.:;;;\·,'"•,.J,~t.'.-t~'.~A;k{;t.: : •• , •• !,,'•, '. ::-:~· •• ' .;.,;~~~i. .. :.;:-t:~t; ~~ .. t•''. );.'.,_ .... -;,' \£' •t•~ "'"<""'.4-1:;a,~.}• · · · .':· -.· "; ,.• 'rt,i:'1-:-•• ·l'..!i·r' n.t· ,, , • • ·, ·,·: ,·\-'t',;,••J:.§'ij.,\:~:t''' ~ •• ·. · -: · .::::.~' t;:-"j?y1;.;~:f" .. ::1Yf~~·-··•--. .. ;.,:•·~:1," :\ _ 1 ':.;. ··• ~·"-"'· ,t;1,~:\ r .. ~·.~y~\1f:;-;;•~'f,;, ))" .. ' ... <; :::: :.-~'.}?]::?--'~ ·-, . . -•---/-.· .. ,_·t1· )~;<·~.: . fjl' f ! \ " ' NATIONAL FLOOD INSURANCE PROGRAM FIRM FLOOD INSURANCE RATE MAP CITY OF CHARLOTTE, NORTH CAROLINA MECKLENBURG COUNTY PANEL 12 OF 31 !SEE MAP 1NDEX FOR PANELS NOT PAIN1EDl COMMUNITY-PANEL NUMBER 370159 0012 C MAP REVISED: JANUARY 6, 1994 Federal Emergency Management Agency ' ··•i~~ •. ' :-)~t~f~·:: • ... -:>•"-; -·~. li~T ~1iI:r1;~fa~{, -- ~_:. '• . . . ·:~. :, ~;~;-: ~~;/ ,••. I ZONE c ~ s\REE1' ,- I .,, ~ r ~ ... -<. ZONE B I ._ TUCKASEEGEE P.&N.RY J: ,. I I I I I I I t' I I I I I I I ~--"_-:;.. • ,: '. ': .;:-::;,· ~1 ,:: •• '.·.',-,',,,.·.:.~ •• '.·.·._.:_ :<· !~~t:'·~~ ., ' -: i- : :::-_-':; .. ATIONAL FLOOD INSURANCE PROGRAM FLOOD INSURANCE RATE MAP CITY OF CHARLOTTE, NORTH CAROLINA MECKLENBURG COUNTY (SEE MAP INDEX F(.JP. ~l-d<EL:; NOT PAINTED) PANEL130F31 COMMUNITY-PANEL NUMBER 370159 0013 B MAP REVISED: FEBRUARY 26. 1982 federal emergency management agency federal insurance administration dctcrminco. ,. • i I le I I I I I I I 1• I I I I I I •• I I "' 0 -.a 0 -z. --\ ZONE C I le I I I I I I I I I I I I •• I I Memo Date: August 9, 1996 To: File From: Douglas Moore ~ ~ Environmental Chemist NC Superfund Section Subj.: Flow Calculations Cherokee Oil Company Site 120 I Berryhill Road Charlotte, Mecklenburg County, NC US EPA ID: NCD 980 799 019. The flow for the unnamed tributary of Stewarts Creek, Stewarts Creek, Irwin Creek and Sugar Creek were calculated using values taken from two reports: (I) USGS Open File Report 83-211 titled "Drainage Areas of Selected Sites on Streams in North Carolina" and (2) USGS Water-Supply Paper 2403 titled "Low-Flow Characterisitics of Streams in North Carolina". The drainage area values from report (1) were multiplied by the mean annual runoff values from plate I of report (2) to estimate the mean annula flow in cubic feet per second. (I) Stewarts Creek Trib at Charlotte 1.52 sq. miles x I. I cubic feet per second/ square mile= 1.672 cubic feet per second. (2) Stewarts Creek at Mth at Charlotte I 1.5 sq. miles x I. I cubic feet per second/ square mile= 12.65 cubic feet per second. (3) Irwin Creek at Barringer Drive at Charlotte 26.0 sq. miles x I. I cubic feet per second/ square mile = 28.6 cubic feet per second. (4) Sugar Creek at State Line at Pineville 69.4 sq, miles x I. 1 cubic feet per second/ square mile = 76.34 cubic feet per second. !!\ii!T!!!ii i\!!!!!!!!!!!!!!!;·· . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . :::::::::::::: :::: :::::::::::::::: .................................. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . •·ii' .................. . I...YiTi !? ?Ti/TT ••••••.=I ••• ' lllf 1::11 I I :,11::1: 1:11:11 :::::::::::::: :::: :::::::::::::::: !!?!!!?!!! !iii !!!!??!!!? ill: :/iii I I :::::::::::::: :::: :::::::::::::::: .................. ·········· 11111 • 111• 11111 :::::::::::::: :::; :::::::::::::::: ··········•"' .... ················ IWWii: : i 1 \\'.?\\\\))\'. \iii)\\???\/ 111•1111 1 111• 1 11 :::::::::::::: :::: :::::::::::::::: . . . .. ... . . . . . . . .................. . . . . . . . . . . . . . ' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1::::: : I i : :::::::::::::: :::: :::::::::::::::: .............. ·---·········•······ ·············· ................... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . :1::: i: I :: .. ::::::::;: :::: :::::::::::::::: ........................... .............. .... .............. . a,: ••••rn1 •· ;::::::::::::: :::· ............... . . . . . . . . . . . . . . . . . . . . . . ............. ·············· ............. ·1= ...... , :: !!ii!!!! ii!!!!! ................... .............. .. ........... .. . .............. ·1········ ... . .. . ......... .. .. .. ......... . .. .. ........ .. . . .......... . . . ......... .. .. .. ......... . .. . .......... . .. . ....... .. ............. .. ·1········. . .. ...... . . . ....... . . .. ...... . . . ....... . . . . . . . . . . . . . ........ . .. . . . . . . . . . ....... . 1:: . . . . . . . . . . . . . . . . . . . . . . . . ............. ............. ............. •••• •••••••• •••••••• :: ii:i!\I! !iii!!!: ............ . . . . . . . . . . . . . . ., ........ .. ................. .. 1!1 H ! ············· . . ... •• U;S;. GEOLOGICAL SURVEY OPEN-FILE REPORT 83-21 l · ~--., ~-~ - : : : : : : : : ; : : : :: : : : : :: : : : : : ·:::::: :: : : : : ; : ; : ; :: : : :: : :':: ::: :·:;:: :: :; : : :: :: : :":::: . ::::::::::::::::::::::::::::::::::::::::::::::::::;::::::::::; DRAINAGE AREAS OF •• j • . ,•. '. ' ' ' .. _·,·? '._.) ,. . . . '·: ... ,•. . ', ;..;}'. .. . . . . ' :': ::::::: i I: i:: i l ~; :: :·t?-/ :·:::·::~:r:i::: :: i::: : : ................. . ... :;::::::::::::· . : : ............. . ............ ~:~:-; . .......... . .......... . .......... . . .......... . .......... . .......... . .......... ~~ .. ............ . .. ............. . .. .............. .. .. . ............... . ... . ··············--~?:": ..... . ................. . ....... . ::::::::::::::::.:::_::::::::::::::::::::;::::::::: ·.::: . SELECTED SITES ·-oN STREAMS·;_ 1 :': IN NORTH CAROLINA Prepared in cooperation with the North Carolina Department of Natural Resources and Community Development / · ... ·' ,' . ,' .- ~•ff ,· 1·1;·; ... ...... _.,. .. •:~ I': -~-I I .~;' I 1: .. I: I I I I: I,,, i,:c..:;, 1: .. ~ I,,, . -,. 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WEST CHARLOTTE lo.EST CHARLOTTE lo.EST CHARLOTTE !,,('ST FOAT Mill IS. C CHARLOTT!". WEST FORT MILL (S.(: 20 35052£ 80S358 FORT Mill. (S.C.) 20 350510 805405 F"ORT MILL <S.C,) 20 350437 805424 FOOT MILL (S,C. J 20 35153() 804731 DERITA 20 351.SOR 80483f. .lERITA 20 351444 20 351250 20 351147 20 3511:lO 01 35103'3 20 351'+03 02 351405 01 351 327 Cl! 351407 20 351306 20 3$1?2(; 03 351216 01 351047 20 3'.-0"~2'.~ 01 3S0'3S'1 20 3S0-32i? OJ 3S0-3J 3 01 350"~19 20 3S0905 01 3S08S.:-:' 01 35082l'. 20 3507()<; 0:l 3SOSOf. 03 350'+'+(1 20 35040.~ 11 3Sl !):! 20 3510)> ,"0 3SJ?ll 20 350':lSO 20 3510 .. 5 804852 SOSOJ l 805020 805036 80S04R 804609 804€,J 9 804f-Ol 8D47i'6 804744 B0481f. 804835 8049<+6 805106 80\ill2 8051 l l 8051 IB f!05a!Cl SO<;to:?7 e1051i''.;I 1105201 80C,20~, 805.'!SB 8053!0 805353 80'•?1 '3 f!043l2 F.0442.R 804417 804037 CHARLOTTE': F.AST CHARLOTT[-" FAST C:HARLOTTF. FAST CHARL.OTTF EASf CHARI.OTTF FA'11 CHAALOTTF. F.AST CHARl.OTTF. 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I I I I I I I t' I I I I I I .. I I Memo Date: August 4, 1995 To: File From: Douglas Moore 4 ~ Environmental Chemist NC Superfund Section Topic: Fisheries in Stewart Creek Cherokee Oil Company 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCD 980 799 019 On Friday, August 4, 1995, I spoke with Tony Roux, Environmental Specialist with the Mecklenburg County Department of Environmental Protection (MCDEP) -Water Quality Section (704) 336-5500. Mr. Roux stated that in October 1991, MCDEP conducted a survey of fish populations in Stewarts Creek, including the segment downstream of the subject site. The results of their survey found 8 different fish species, including sunfish, largemouth bass and bream in Stewarts Creek at the Morehead Street bridge. This point is approximately 0.5 miles downstream of the site PPE. Mr. Roux also indicated that MCDEP found discarded bait buckets at the Morehead Street bridge in Stewarts Creek, suggesting that people routinely attempted to catch fish at this location. With regard to the unnamed tributary of Stewarts Creek south of Freedom Road, Mr. Roux stated that the segment is probably large enough to have fish present, but believes that people probably do not attempt to catch fish due to inaccessibility. Mr. Roux indicated that MCDEP has visited the subject site numerous times in response to complaints about spills and contaminated runoff leaving the site. Mr. Roux indicated that the runoff usually originated from leaks in a containment wall located along the south boundary of the site. The runoff was particular bad during storm events. The runoff passed through and under' the containment wall, travelled south across the Suburban Propane property and entered a storm grate located on Suburban Propane's parking lot. The storm grate is connected to an underground sewer which directs the runoff south to an outfall on the unnamed tributary of Stewarts Creek (UT). MCDEP has collected samples of the runoff from the site as well as samples from a storm sewer outfall in the UT. These samples indicate that site runoff has resulted in contamination of the UT possibly down to Stewarts Creek. Mr. Roux believes that the analytical results of the samples would be able to demonstrate a release from the site to the UT. I ~ I I ; I I I I I - I I I I I 1.-: 1.,:-,• . • ,, I MEMO Date: To: From: Topic: March 15, 1994 File Douglas Moore &~~- Environmental Chemist NC Superfund Section Fishery and Recreational use along Irwin and Sugar Creeks Cherokee Oil Site 925 South Summit Avenue Ch2,rlotte, Mecklenburg Co., N. C. USEPA ID: NCD 986 190 239 On this day, I spoke with Wayne Chapman, State Fisheries Biologist, District 6, Wildlife Resources Commission (1-704-982-9255) regarding fishery and recreational use of Irwin and Sugar Creeks within 15 miles downstream of the subject site. Mr. Chapman visited the area near the site in response to an October 1990 fish kill. He stated that Irwin Creek is inaccessible from Wilkinson Boulevard down to West Boulevard, particularly near the site as most of the Creek has been culverted due to the 1-77 and I-74 interchange. He recalled that there were fish in Irwin Creek near the site but that due to the inaccessibility of Irwin Creek in this segment, no evidence was found that fishing occurs in this. area. He stated that there are signs of fishing along Irwin Creek at the West Boulevard bridge, at the Remount Road bridge and along Revolution Park adjacent to Irwin Creek. He believes that fishing occurs from West Boulevard downstream to the Clanton Road bridge. He stated that fishing and wading occurs in this segment due to its accessibility from housing complexes near Remount Road and along Revolution Park. He stated that fish are available for consumption-in this segment and believes that fish are regularly harvested for this purpose. He stated that Ir.,.ln Creek becomes more inaccessible below the Clanton Road bridge and he thinks that Irwin Creek is inaccessible and not actively fished from the Clanton Road bridge downstream to the Yorkmont Road bridge. Mr. Chapman believes that Sugar Creek is fished from the Yorkmont Road bridge and below due to the size of the stream and numerous bridge crossings along the stretch down to the end of the 15 mile surface water pathway distance. He believed that fish are harvested for human consumption in Sugar Creek. \cherokee\fishery Ref. 30 ., ~ [ir; MOUNTAIN ISLAND LA~ E, N.~ CHARLOTTE SE CHARLOTTE 1000 0 1000 ' SCALE 124000 0 ,000 3000 ""' 0 -6000 I MILE 7000 FEET l KILOMETER NATIONAL WETLANDS INVENTORY SPECIAL NOTE • UNITED STATES DEPARTMENT OF THE INTERIOR SYMBOLOOY EXAMPLE SYSTEM I SUBSYSTEM / _,..,,-CLASS EM~ SUBCLASS. WATER REGIME NOTES TO THE USER • Welland, which have been field examined are indicated on the mitp by an asterisk c•1. • Additions or corrections 10 1he wetlands information displayed on this map are solicited. Please forward such information to the address indicated. • Subsy,:tems, Classes, Subclasses, and Water Regimes in Italics were developad specifically for NATIONAL WETLANDS INVENTORY mapping, , 35" 15' •1 I ir•~·r ~u·s:,·3,_' MOUNTAIN ISLAND LAKE, N.C. D 1 acre D 10acres □ 20 IICrel This document was prepared primarily by tt&reotCOPlc analysis of high altitude aerial photographs, Wetlands were id.,tified on the photographs based on vegetation. visible hydrok,gy, and geography in accordllneu with CleHiflca• tion of Wllt1andt and Deepwater Habftatl of the UnlMd States (FWS/08S • 79/31 Dec&mber 1979). The aerial photographs typ«:ally reflect conditions during the specif"ie year and season when they were taken. In addition, there is a margin of error Inherent in the use of the aerial photographs. Thus. a detailed on the ground and historical analysis of a single site mav resutt in a reviskm of the wetland boundariEtS established through photographic interpretation_. In addition, some•mall wettends end thote obscured by den59 forest cover may not be included on this document. UPLAND (NON-WETLAND) • Some areas design11ted as R4S8, R4SBW, OR R4SBJ (INTERMITTENT STREAMS) may not meet the defini- tion of wetland. • This map uses the class Unconsolidated Shore (US). SYSTEM SUBSYSTEM CLH& - SYSTEM ACREAGE GUIDE Other information including a narrative report concerning the wetland resources depicted on this document maybe available. For information, contact: · Reg_iollal Director (ARDE) Region IV ·u.s .. Fish and Wildlife Service 75 Spring Street S.W. Atlante, Georgie 30303 1 -SUBTIDAL M-MARINE Federal, State and IOC$1 regulatory agencies wtth jurisdfc- tion aYffr wetlands may define and describe wetlands in a different manner than that used in tht8 inventory. There is no attempt, in either the design or products of this inven- to,y, to define the limhs of proprietary jurisdiction of any Federal, State or local government or to establish the geographical scope of the regulatOfY programs of govern- ment agencies. PeNOn1 lntendino to engage fn actilitift: ffl\l'olving modification• within or 41djacent to wwttand ■ren •hould •eek the advlceof appropriate Federal, Stat• or local agencies concerning specified 1111..,cy regulato,y . ;--"::i,'!S:,,,S l's•-~ pr.);,ric1;cry ~urist:::tiu;;a tha1 ;r.a--, ;;:fwt such activities. 2 -INTERTIDAL \ ___ ---;R20WH l (LINEAR DEEPWATER HABITAT) O -Primarily represents upland ereas, but may ,ncluda tmc!auified w~II!~ iuch ff m@f"'·~-X,i!ied ere!!, rt:n photo-identifiable areH and/or unin1en1ion"a1 omissions. On earlier NWI maps that class was designated Beach/ Bar (BB}, .or Flat (FL). Sutx:lasses remain the same in both versions. AERIAL PHOTOGRAPHY OATE,2.../___/.83 SCALE, 1:58 000 TYPE, __ C_I_R __ DATE: __J__!_. __ SCALE, ------ TYPE, E -ESTUARINE 1 -S-UBT!OA!. 2 -INTERTIDAL '-· U.S. DEPARTMENT OF THE INTERlOR FISH AND WILDLIFE SERVICE 1991 SYSTEM SUBSYSTEM RB-ROCK U:1-UNCORSOI.IOATEO-Ml -AOUAT1C Bf.I> RF -REEF ON-OPENWArE".11'/ AB-AOUATIC BEO Rr -REEF RS -ROCIO' SHORE us -l)NCONSOIJOAT!I) 118 ;_ IIOOC. UI -UNCOHIOUDATED Al -AOI.IA,TIC BED IIF-11£9" OW-Qll'EN WA"11/ AB -AOUA11C Bf.0 Al':... REEF SIi -STMAMBED FIS -ROCJ(Y US -UNCONSOLIOAT"f.0 EM -EMERGEllil SS -· SCAU8-Sl«U8 ,o -· ,oRf:STEO CL ... BOTIOM 90TIOM V""-' Bott"'" ,_ l Rubble 1 Cobbtlt·G..-1 , ..... '""' •0fll9ni,; I Alge! 1 Coral J AooCed vna.,m 3 Wo,m '""""'"' -1 Algal 1 eo..t 3 R-.d Vaeuler 3 Worm 6 ~s.,,,,,._,,.,,, R-RIVERINE , ...... , ...... SHOM 1 Cobble-Gr....t 2 S•nd '""" 4 O'lJ-ln"' IIOTI0M . IIOTIOM I Alp! 2 Mullll'IC 3 AolKed Vneul■r 3 Worm 4 Floslin9 Vftcu,_ s U"ntno-s,._,,,,., e /Jn/1_,, Sud~■ 1 -LIMNETIC --1Alpl 2M~~E 3 R-edv..cui., 3 Worm • F1M1,,. Vn,:u1., S Utll.rio_, S""'-rg,Hlf IJ UM-Surl11tt • ' .j_ L -LACUSTRINE'' 1 Cobbl.,.G, ..... , lS.nd ,. ... ,o,_o:: SHORE ...... 2 Rubbltt" 6HOFIE I Cobble-G,.,.091 ,,... '""" • Orvan•c 2 -LITTORAL 1 ~11en1 \ Broad-Le..-1<:1 2 Nonpenottent OK,duou9 2 Nffdle-Lu•f'<l D~ld,..:,,n 3 Btoad·Lene<I E-11'..en 4 Nee-dle·L■BY9d E..ergr....,, '"" I Oftlduou• 1 fttrg,er:n I Broed L..._i Dftduou9 lNoedlt,-l.a.-1 Oecoduou■ :3 llroad-le8W!d £.,.,,,, .... 4 ,-,clle-Le-.:1 E-v,Men ''"" Ill 0-C,,,,._,s 1Eu;fl'~" SYSTl!M SUBSYST!M SUBSYSTEM 1 -TIDAL 2 -LOWER PERENNIAL 3 -UPPER PERENNIAL 4 -INTERMITTENT US -UNCONSOUOATEO 6 -UNKNOWN PERENNIAL r::IN -OHN WAITll'I u,,,.,_,,,tm.., SYSTEM C\AU RB -r:IOCK VII -VNCONSOUOATEO BOTT01¥1 1 C<,bblp-Grlv•t 2 S1nd '""" 4 O•g■nic '"""""' 2 flubb"' 3 Cobble--Gr■~el .... ,..., e Org■mc 7 V"'9ffl.red AB -AOUA TIC BEO I Alpl 2 Aquatic" Mou 3 Roo-ted V...:ui.r 4 FID!n,r,v v1scu1..- S u,v"°""' •-• I tklinc-S""- It$ -ROOCY SMOf!E , ...... "'"'"" """'' 1 Cobble-Gr-' , .... ,..., ·--·-- -STREAMBEO 11, lomned 10 TIOAL •nd 1"1ERMITTENT SUBsYSTEMS. and ,::omp,i91!1 ,,_ only ct.ASS iro the lfrfltRMITTENT SUIISVSTEM ••EMERGENT ~ l,m,ted lo TIDAL and LOWEii ~IIENNIAL SUBSYSTEMS n,.. remaining Ct.ASS£$ .,e lound 11• en SUBSYSTEMS AS -flOCK BOTTOM UII-UNCONSOUOATEO AB -AQUATIC SEO '"""' 2 Aubbllt eonoM 1 CObblt·G•aw!-1 , .... '""" 4 Ot11•noc ·-2 Aqutilc Mou 3RoaffldVNCUlel' 4Floll1•,i,aV..w,_. II, t/nlltNIIWI ,....,,.,,, I Uni-..,...,, Surl1'Cf- P -PALUSTAINE IJS -UNCONSOI.IOATEO Ml_ MOSS-LIC1-IEN EM -EMERGENT SS -SCfMI-SHRV9 F0 -FORESTED tJoN -Of>EN WATElf, SHOAE Un.!,_,, BOff(>l'lt I Cabble-G,....,I , .... '""" • 0•11•no: I V99'1'11tld lltoad-l.Nwd ,......,, 2,._....·Ltiwd OKICluou1 31f!Nld L.--f ,..,_ 4 Needle-1.elM!d h•'I'"'" '°"' t 0,,1,,um,t t 1.,.,,,,_ I a,,,..u_.,......i DecduDus 2 NNdlol-Le.-1 D-:iduou, 3 "*·i..-ecl e__..... 4N-.~E .. ,~ ""' I l?ec,Wo,n, 1r...,,v_,. Ra-ltOCK IIOTTOM ua -UHCONSOUOAtEO .... -AQUATIC r:,N-Ofl'ENWAr!"R Unl-·-RB -JIOO: 90TT~M ue -UNCONSOUOo\TtO A8 ·-AQUATIC RS -ROCKY SHORE US -UNCONSOUOATEO EM -EMERGENT OW-OPEN WATt/111 UM,,.,...,,Borrom I -,._ BOTTOM IED 1 Cabbl•·Gr-1 ..... , .... • Oti,a""' 1 ..... , ,,_ 80TTOM l Cobble-Gr..-e-1 .. .. '""' • Ort-nic ... IA .. 2AquM,cMoN, 3 R........t Vncula, 4Fio.i,.,.vneui.- 5 vnt ....... s.....,.,.,_ IUM......,SINf- MODIFIERS 1a-., 2Ru- '"°"' 1 Cllttble,G•-,s,.. , .... ,,,_ IV ... lllted In ordlir to fl'IOrt adeq1H11ely dncrobe _ .. ,.. ■nd ~ "-bit■n -or fflOl'e of the -rag,rM, -tar eheffl•tt!"'f'. soil. or Nl«..i l'IOdof,.,. ,...y be applied at !he cttss or ~ left! "' !he l'l,e-,ari;hy Th,e farmed modiflllf ~ ■190 be 11PPlied 10 the ecotogic■I ,v,ii.m WATER REGIME WATER CHEMISTRY SOIL Non-Tidal Tidal ., Coastal Halinity Inland l•Hnity pH Modifiers for A T■mpo,~ty~ H l'etmene•1t1y Flooded W.ht~ffottd«I •sf~-l!IMlt_ ~ I H.,,,.,hal,,,_ '"'-'-'-all Fresh Water I 0,111'""' • SaTurtM J ..,..,_,, flooded l Su1Moa..1 "Rs--llod91 •· 2 Eu"91•ne l!IE.rul .... .... n M,n@l'■t C ......... -ll Mr/ic,elly FloodN M ln119ute,1yf--3 • ' Semipar_.,. .... y ... J M_.,.,,,_ ,.,.i,Jh/ 9M .. ou1,,.. tC.CVnneu1,,1 D .S..o,,9#rF_,../ w..........,, N R-aulM-ty Fboclal ·v ,....,.....,,.roa1 ii f'o!Whal•NI 0 FrMh I All,al1n,p w.JI O,■"'" flDollllllT ........... ,. ... .,., ... .., ,loodltd """-·--' SlfUOIIIHl'rF,,,,,.,,1 v s.i-.i-s..-......,._, ·-~ ,.,__, ,_., ,,_ . ' ..,...,_1,-Floodad l ""-''™'•"'"' G 1Nennm•N'¥E....,_ E..-,t ,.._,_ •n.,u -.. ,..,.,,... .,. """-' ,u-d •n 11 11~1,in liilJll1111'1,llllllil lilltUf;, .,,i,...i .· . 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'~1 ~ '' """ ,,,' EASn ____ , ____ 7/_~ P5SIA, , ,r-· -• NE ---.,----=-' ~]~ -----••'L•-~~ <l 7' 30;; '20 ;,i <tll<; 'itHr~s~r\.," o~•,,•1-. n•"rf :'171-S'f, .,1p,.~ 35"1:J' 80°45' SVMBOLOGY EXAMPLE SYSTEM I SUBSYSTEM / .-,CLASS L2EM2F "' SUBCLA5$ WATER REGIME NOTES TO THE USER • Wetlands which ha\le been field examined are Indicated on the map by an asterisk 1•1. • Additions or corrections to the wetlands information displayed on this maP are solicited. Please fo;werd such inforrnat1on to the address indicated. • Subsystems, Classes, Subdasses. and Water Regimes in ltelics were ctevewed specifically for NATIONAL WETLANDS INVENTORY mapping. '11 5Z?JOO'" E DERITA, N.C. D 1 acre D 10acrn ACREAGE GUIDE □ 20ac,es This document was prepared primarity by stereoscopic analysis of high altitude aerial photographs. Wetlands were identified on the photographs based on vegetation, visible hydrology, and geography in accordance with c1 ... mca-tion of Wetlands and Deepwater Habitltt of the United Statn (FWS/08S • 79/31 December 1979). The aerial photographs typically reflect conditions during the specific year and season when they were taken. In addition. there is a margin of error inherent in the use of the aerial photographs. Thus. a detailed on the ground and historical analysis of a single site may result In a revision of the wetland boundaries established through photographic interpretation. In addition, some small wetlands and those obscured by dense forest cover mev not be included on this document. UPLAND (NON•WETLAND1 • Some areas designated as R4SB. R4SBW. OR R4SBJ (INTEftMITTENT STREAMS) may not meet the defini• tion of wetland. SYSTEM SUBSYSTEM CLASS 5ubi:;'-• SYSTEM Other information including a narrative report concerning the wetland resources depicted on this document may be available. For information, contact: Regional Director (ARDE) Region IV U.S. Fish and Wildlife Service 75 Spring Street S.W. Atlanta, Georgia 30303 M-MARINE Federal, State and local regulatory agencies with jurisdic-tion over wetlands may define and describe wetlands in a different manner than that used in this im,entory. There is no attempt, in either the design or products ol this Inven-tory, to define the limits of proprietary jurisdiction of any Federal. State or local government or to establish the ,geographical scope of the regulatory programs of govern-ment agencies. P•nona lntanding to eng.-ge In acttvitin involving modifications within or adjacent 10 wetland ., .. , should seek the advice of appropriate Faderal, Stat• or local agenciH concerning speclfied -aency ,-gulatory programs and proprletary jurisdictions th■t may lffect auch activities. "------R20WH / (LINEAR DEEPWATER HABITAT) O -Primarily represents upland areas. but may include unclassified wetlands such as man•modified areas. non photo-identifiable areas and/or unintentional omissions. • This map uses the class Unconsoltdated Shore (US). On earlier NWI maps that class was designated Beach/ ear !9B), or Flat (FL). Subclasses remain the same in both versions. AERIAL PHOTOGRAPHY OATE,~---J83 SCALE: f:58 QQQ TYPE, CIR DATE: ___/_____.I. __ SCALE; TYPE, E -ESTUARINE U.S. DEPARTMENT OF THE INTERIOR FISH AND WILDLIFE SERVICE Prepared by N•tlonal Wetlands Inventory 1991 SYSTEM 1 -SUBTIDAL 2 -INTERTIDAL 1 -SU_BTIOAL 2 -INTERTIDAL SUBSYSTEM RD -i!OCII( \)8-i.,'NCONSOLIDATfD ..,_8 -AQUATIC 8EO "f -ll'eEF ON-OP!NWArERI" BOTTOM 80TTOM Uni"""'n Bom,m 1 ~rock 2 Rubbl" 1 C-le-G,....,I 2 Sand "'"" • Organic: 1 A'9II 3 P.ooled VHC1Jllr SUfM,-r, $<.ll)m!O'genr l Coral 3Wo,.., A8 -AQUAnc 8£D AF -REEF RS -ROCKY Sl-fORE 1 Algal 1 Coul 3 Rooietl Vncular 3 Wnrm S UnA-rno,o,n Subm~ 1 8-ock 2 Rubblft R -RIVERINE US -UNCONSOLIOATEO SHO'lf 1 C,;,bl;,le-G,..,.,, 2 s,md '""" 4 Or91n,c RB-ROCI( VII -UNCOl'tSOUDATED A8 -AOU ... TtC BEO RF -Rl:Ef r:,,N -OF"!N WArERI u,,t..-Bor,om BOTTOM BOTTOM , ...... ,.,.,,. I Collble·G•riel lS.m '""" 4 Orflnic: 1 Alp1 J Mollutt: 3 Roo!ed v..r:u .. r 3 Worm • Fkw11,no Vneul .. su .. ,..,...s.,,,,,,.,.,.,,, ll/.mlnr,wnSu,tn,r 1 -LIMNETIC Al -AQUATIC BED Rf -REEF Sl:I -STM€AM8ED 11S -AOCK'f' 1 ..,_IQIII 2 MollulC 3 A-ed Vncul■r 3 Worm 411 flosltng Vncul• su,...-s.-~ II Uni.no""" s,,,,_ L -LACUSTRINE 1 Cubb!e Q . .,,,,,1 2 S1nd , ... ,t 0•1J,11no: '"""' : ....... oc:1< 2 Rubble US -UNCONSOt.lDAT!D EHi ·-EMERGENT SS -SCRUB-SHF!Ui '"""' j ColJbla·\afWel """' , ... 4 Qrga-n,e I Pe~ i ri:•oad·lu,,..S 2 """-'islenl ~,duo~ 2 --L-Oeeduous 3 B•md·Leav<ed E,r,e19,..,n ,tN&e,dle-Le-£_gr..,n , .. ., 6 OM,dw,,s 1 Ew,g,Hn 2 -LITTORAL fO -FORESTED ,a.--•-~ l)e<:lduous 2""""""-L-,,d O<>elduous l llroed·L"aved beryr"n ,t """9dla· Leor,,,d £...,'II'"'"" ·-&0«"1<1ous 7 E•~gtHn CLASI -SYSTEM SUBSYSTEM SUBSYSTEM 1 -TIOAl 2 -LOWER PERENNIAL 3 -UPPER PERENNIAL 4 -INTERMITTENT 6 -UNKNOWN PERENNIAL a.us ....... SYSTEM CIASS -· Rfl -ROCK 1 !Jl!droel< 2Flcu-VB -UNCONSOLIDATED BOTTOM 1 Cabble-Gravel 2 Sand ' ... 4 CJrv.l™c 'SB -ST!IEAMBED ·--2 RUbble 3 Cl:lbblo-G,_t 4 S•nd , ... -& O<gank: 7 V"!19191ed AB -AQUATIC BED I Aig.l 2 Aqu,iuc Mon 3 Rooled Vn.eular & floatm(II Vascular 5 Unfoawn s,,,,,,,,.,,..,.,,, 15 Ut>lnown Svrl«• RS -ROCic:Y SHORE I 88drOCk ,,,,,_ -STREAMflEO ,s l,miled to TIDAL 1nd INTERMITTENT Sll!JSYSTI:MS. and compr,.11~ only Ct.ASS "'Tl>e ll'fff:RM!nffil SUBSYSTEM ••EMERGENT is 1trn,1ed to TIDAL 1ml LOWER PEREfOIMAL SU9sYSTEMS. Tl,e ,...,1inin9 CLASSES •e lc.,nd ,n ,n SVIIS'fSTEMS P -PALUSTRINE US -UNC()NSOUOATED '"""' 1 Cobble--G,_1 , Som ,...., ·~ic ·--"EM -EMERGHIT 2 Noollf'rS.~lenl CN'l-0/>ENWATERI Unktto""" Bfflom AB -ROCK BOTTOM UB -UN<:ONSOUD..._TED ,1,B -"'OUATIC BED f!DTTOM IJS -ut.CON'SOllOATED Ml. -MOSS-LICHEN eM -EMERGENT SS -SCRUB-SHAUii FO -FoP:£SttD ON-0/>EN WArFRI u,,t...,wn Botro,,, \ lle<koc~ 2 Rubble 1 eott,1e·G<1•n,I 2 S•l'ld 3 Mud • Qryl<>n'.: 1 Algal 2 Aquauc Most l Rooted Vpcul,r ◄ FloW<•ntl V1~cuilr !) u,,t""""" sutim.,,,.n1 A Ur!Aili!ll,/l !llffJEJ SHORE 1 Cobble Grawl 2 Sand , ... • Organ,c sv.-i.i'l'd ' .... 2 Lo:hen ·--2 1'1onpa,r .. .,_ I a.o.d-.___, ........ J,.....i.--, -· llrold-~ f¥1!1'"" .. N .............. hlfifllll ,., .. IOKwciu, 1 E-,,,"" 1 Braed-LHW<I D.e>OIIOUS 2 N ....... ·L"-" 0.ClduOut 3 9'Dld-l•ewd f_.,...., • N.,..e-L..aved E-vr"" ·-~ (lflf~lllll ,,_ RB -ROCK 80TTOM U8-UMCONSOUOAT£D AB-,l,QIJAflC ON-OPfN wArtR, u..na..., Battom 11!1 -ROCK ,OTTOM UB -UNCONSOUOATEO AB -AQUA.TIC AS -ROCKY SHORE US -uttc0"1SOUOATEO EM -EMERGEHT OW-OPEN WArER, BOTTOM 8EO IIOTTOM !IED SHORE f/nlm,wt> Sorrom ·-· ,._ I Collble•Gr ... e! 2 s,nc1 '""" •o,ea...e ·-2 A.CIIM1icMa111 3 Root.It \tneulll' • 11oettne v-..:-u1., S {/,It-5,,,,.,_...., 6 un,1-,_, S!#ff1e9 ....... ,._ 1 Cobble-G<_,,.. 2 s,nc1 lMoo • Orpnic 1 Algal 1 B-..Ck l ,lloqi,Mic Ma111 2 Rut>bla l Ro,:,Nd VNcular 4 flo,ohng Va..;ular !i Ut>lnown S.,,,,._1/Mf -e UrttllOWtl Surl.n MODIFIERS 1 Cobble-Gr-I ,. .. , .... C OrlJ,llnC: S Ve,getfted In OfOlf lo mot■ Nellull•IV dffctibe w«land and clllftlonl., hllb,tltl -or more ol the -1..-"'9ime, -1er cheml1,try, soil. or 91)Kill modifiers ma, be '1)111;.,d Ill lhe cl•U or I-lewel ,n 11te hier,rchy. The larmad modifier may also be applied to the«:olo9ie•I gy9tem WATER REGtME WATER CHEMISTRY SOIL Non-Tidal Tidal Coastal Halinity Inland Salinity pH Modihrs for A T,...,.,._,,t-, Floadtd H Perrnener,1ly FloOdN K Arf~ffr floodH • S T...-.0,,,1,v•Todal IH_IIII_ 7-an Fresh Watet I O,pn,c 9 Sl1urfted J 1m .. ,mn,..,,1y Fl!lllded l Sublodll • A S.nonal·Todll 2 EUNI"" II E,,,..iM .... n M....,r•I C S.-11¥ Flooded K M1!1c,.II'( F'-'-d M lrr9tUl1rly hpMed •T s,,......,,,,..,.nt,Todll l Mn,,,..1•1'11 tfJrffl111t) IM-t Cl<cu.-U,rJI D S-anaRr Flooded/ W lnl.,.moll-lJ N Re,gulafl'( Fiood9<1 • V A,tm11n1ml·ldal 4 Polyhll•""' ··-'AIU!,ne _, 0,,-wd flooded 1.....,,,"' P lrre,gula1ly FioodoO'd U untr,own s Moo..,.,.. .... E S••-"r FINdlfl, 't Se1u<ef•M!:..,ipenNn11n11 &Oh9oh,~,_ ''""""' !IM60!!11 0 Jtttt, r r!"""""::1~ (t ftltllillltllr I ~'":r'IJ7 q,,i; , ltllfllHI ·lhi!U ,wjpf li1111fnes *'' onl, u-i"' v--1•11y ,nllue-nced, lrnhwal., --""7".77' . .1: 1--.'. ,,::,;•ri:-,:~ ., .,. : ,,; , ,_. ;·r,:· .".";--.--;. :f~:--:-;-;--,--; 1. t .:• .• "' ~i :1.; , .. · .. •· . 'c: ':': -,;. -,; --, ;.T, ,, -·,;~, -;-r'~ • -,,T -,,~,-'. 1 ;-' ,, J ·:1-2 Nanllf"Stslenl SPECIAL MODIFIERS ·-t, (J,bd.'ltnpaundtHJ d 1'1,r..lfr "'"""'IDircMd ' Art.tc:,11 Suba1t•1e f F1r'"9d ' Spa,/ • &cavn~ CIAU -- E ----:--L-_ ~ SYSTEM CHARLOTTE WEST, N.C. CHARLOTT[ SE CHARLOTTE SCALE 124 000 T _ -1~~ ·r·-D -~-==~7..: __ =r - 0 0/)(J 2000 _l(X)r 15000 :ooo FUT !-cl -j , -r _F-~-~----·--------__ -,=:=,,.-~ _:_:_ • 0 ·1::::-=:-:=:--_:::L-"' __ . ~=-::-..----:--=:J D 10acrH ACREAGE GUIDE I "'L:::lo'Ef[~ =~ □ 20acras Other information including a narrative report concerning the wetland resources depicted on this document may be available. For information, contact: Regional Director (ARDE) Region IV U.S. Fish and Wildlife Service 75 Spring Street S.W. Atla11ta. Georgia 30303 M-MARINE NATIONAL WETLANDS ll\iVE1~0RY Ul\!ITEO STATES DEPARTMENT OF THE INT!:RIOR SPECIAL NOTE This document was prepared primarily by stereoscopic ana,ysis of high altitude aerial phOtographs. Wetlands were identified on the photographs based on vegetation. visible hydrology. and geography in accordance with Clnsiftea- tion o1 Wetlands and Deepwater Habitat, of the United States iFWS10BS • 79131 December 1979)_ The aerial photographs typically reflect conditions during the specific year and season when they were taken. In addition, there is a margin of error inherent in the use of the aerial photographs Thus, a detailed on the ground and historical analysis of a single sile may result in a revision of the wetland boundaries established through photographic interpretation .. In addition, some small wetlands and those obscured by dense forest cover may not be included on this document. FeC:eral. State and local regulatory agencies with jurisdic- tion over wetlands may define and describe wetlands in a different manner than that used in this inventory. There is no attempt, in either the design or products of this inven. tory, to define the limits of proprietary jurisdiction of any Federal, State or local government or to establish the geographical scope of the regulatory programs of govern. ment agencies. P&rsons int&nding to engage In activities involving modifications within or adjacent to wetland . areas should seek the advice of appropriate Federal, State or focal agencies concerning specified agency regulatory r-rn~--111ms and ,,,oprietary jurisdictions that may affect tuch activities. SYMBOLOGY EXAMPLE SYSTEM I SUBSYSTEM /,.,,.-<CLASS 12EM2F / " SUBCLASS WATER REGIME UPLAND (NON.WETLAND, D -Primarily represents upland areas, but may include unclassified wetlends tuch n man•modified areas, non piioto-iudllc:•;;.,,;:;i'tl or~ill>I ord/1,n urill'ii.1ctl,kF1111: v;.1i:t,-ior,;;. NOTES TD THE USER • Wetlands which have been field examined are indicated on the map by an asterisk 1•1 • Additions or corrections to the wetlands information displayed on this map are solicited. Please forward such information to the address indicated. • Subsystems. Classes, Sutx:lasses, and Water Regimes in h.afics were developed specifically for NATIONAL WETLANDS INVENTORY mapping. • Some areas designated as R4SB, R4SBW, OR R4SBJ (INTERMITTENT STREAMS) may not meet the defini- tion of wetland. • This map uses the class Unconsolidated Shore lUS). On earlier NWI maps that class was designated Beach/ Bar (BBJ. or Flat {FL) Sutx:lasses remain the same in both versions. AERIAL PHOTOGRAPHY DATE: 3 / 183 DATE: __J____j_ __ SCALE, 1:58 000 SCALE: CIR E -ESTUARINE ~lF"(' FHIC:," '""''"""'·-' ~• PINEVIL~£ 2 7 Ml J. POCK Hill. SC ;,n .,,,·f "" "!Ill ~35D07'30" so 0 52'30'' CHARLOTTE WEST, N.C. U.S. DEPARTMENT OF THE INTERIOR FISH AND WILDLIFE SERVICE Pr,apared by National Wetlands Inventory 1991 SYSTEM SUBSYSTEM 1 -SUBTIDAL 2 -INTERTIDAL 1 -SUBTIDAL 2 -INTERTIDAL SUBSYSTEM CLASS ......... SYSTEM Rfl -ROCK UII -UMCONSOLIOATEO AB --AQUATIC BED RF -l'lrEf rm -Of'fN w,VfR, llfilftlM tltHIUM lllflnrnt.,lfntlnm I ~•ock "2 Rutlbl,- 1 Cobbl<!•Gr...,el 's,,oo '...,, 4 Qrg1n,c 1 Al!l•l 3 Aoolod VHcul .. 5 Untnown Sut,me,~nr 1 eo,11 3Wo,m AB --M)L/ATlf; ll~P RF REff 1 Alg~I 1 Corlll 3 Roo,...i V.ncul_, l Worm S Un/mown Submlff~nf R-RIVERINE flli ROrMY !'ilt/'ll!f I Blldroct 2 Rubt,lo, II~ U/rjf;ONflOI tnATfO SHC)Rf I Cohhl,--Gra~~I 2 SAnd '""" 4 O•,g1n,c 1'111 ltOCIC UII UHCONIOllOAUD All AOUAflC 1,D ~, ~~t, aN -(Jf(N WA7lfl' l)Mn~" 60110m IOTTOM IOTTOM , ....... 2Rubt,•., I Cllbbla-GrllWII 2S.M '""' 4 0-;tnic I AJval 2 Mi:111u-, J Ror.o!MI V~ul1, 3 Warm 4 ~to.,1,ng VIK1,1 .. , s vn,1,..,_, s,,,,,.,.,flfffl 6 VI# -n S1,1rl.c:e 1 -LIMNETIC AB AQUATIC BED AF --AHF I A~I Z Moll1,1.,; J R--ed Vneula, l Worm ◄ floel,,. Vncul11 S :,nt"°""' Subm.,,~nt 6 UnAnown SurlltCf' L -LACUSTRINE SI -StAfAMBfO RS -AOCICY I Cotible-G,..,~1 2 S■n<I '""" 4 Organ,c SMOAE ,..,, ... 2 Rubble US UNCONC:OL1DATEO EM • EMERGENT SS SCRU9-SHRU8 S>IORE 1 Cobbla-G,1t1el 2 Sand , .... 4 O,gani<: 1 Pe,-ttstenl I 8ro■r:He8YII<! Z N.i:,np,r,rs1su,n1 ~e,duous Z~le- DPelduous 3 B•oad Lesve<l E""''ll'ff" 4 --Lea-.fll Edrgt""""' .. , ... 6 0..c,d,.,(,uJ 7 E ""''T""" 2 -LITTORAL ,0 FORESTED I B,oa(!,L01.-.II<! ClttlffllOllS 2 ,._,Mlle•Lei,yll<! Dec.,uous 3 8'o■d·le­ Eve,,-n • -le-le8Yed EVP,g<ttn ' -6 D«,du<XJS 7 Ew,rg,...,,, SUBSYSTEM 1 -TIDAL 2 -LOWER PERENNIAL 3 -UPPER PERENNIAL 4 -INTERMITTENT 5 -UNKNOWN PER EN NIAL CLASS SYSTEM CLASS ........ 1 BU<oo:;t 2 Rubble UB -UNCONSOLIDATED BOTTOM 1 Cobhl,.-G,nwl 2 Sand '""" 4 Org1n,c ·se -STREAMBED 1 Bedrod 2 Rubbll 3 Cobblti-G,~VPI 4 S1nd '""" 6 Qrg1n1e 7 Vev~a1e<1 AB -AQUATIC BEO 1 Algll 2 Aqua!..: Most 3 "11a!ed VHCular 4 flOMl"V V■scul,,.,. s un,1-,.,,...,, SvbmMflM'r 6 Unlnown SurlHe RS -ROCl!::Y SHORE 1 Bed,ock 2 Rul>ble 'STIIEAM8ED 1& l1m,1MI to TIDAL Ind INTERMITTI'NT SUBSYSTEMS. l!'ld compr,..s the only Cl.ASS m 1"1, INTERMITTENT SUBSYSTEM ••EMERGENT 11' lim1Ted to TIDAL and LOWfR PERENNIAL SU8SYSTI:MS The ,1m11n"'!I CLASSES .,., found'" 111 SUaSYSTEMS P -PALUSTRINE US -UNCONSOLIDATED SHORE 1 Cobblt!-Grr,el 2 s,oo """' 4 0",l&ni,: 5V1111911~ .. EM -EMERGENT CNI -OPCN W,IITERI Un~rn,w,1 lla1n,m 118 •· ROCIC 90TTQM UB-IJNCONSOUD.A.TED AB -AQUATIC BED BOTTOM US -UNCONSOLIDATED ML -MOSS-LICHEN EM -EMERGENT SS -SCRUB-SHRUI! fO -FORESTED ~-OP£N WA7£RI U~nownlton"'" I Cobl,J,,-GrlYIII , s.~-' "'" 4 O,gan,t ,.,,., 2 hi"-"'lk MON l~V-..ltir .$ Floll1ing Vacul• 5 u,,tno..., Sut,me,gent e u,,tno..., suma Sl1ORE 1 t,,bhl1-Gr8YII l:S•nd , .... ,t Orgeni,: s veo,n11N1 I Ptrtestenl 2 Nonptt1,11e~1 1 llroad l.1!1¥"<1 :-eeotlu"us 2 Nffdl•-Le•~ OK.,uou, 3 llroed-1.eaYed f.d",l""'n 4 N91dlt•l.ell¥M hero,"" """ 110.r~s 1c.., •• ,, I 8,,.,,1 l"-Dot<s'.·,'-"'s : i,., .... ;,~ t.,_,_i ~>d1,11>,11 3 Brl>lld-ltav..d Eve•~n .. Nefldlt-l•-Edrg,_ ,~., 6Dtu,d;JOU$ ,,,,,,,.., f'tfl-AOCIC BOTTOM , ....... Z ll11bblt ue -UNCOHSOLIOATEO All -AQUATIC BOTTOM BEO 1 Collblti-Gr~ 2 ""' , .... , Or;anic 1 A.1g,1 2 Aquatic Motl 3 Rooted Vnc1,11., 4 Fl0Wtt"9V.-r:11lar s /Jn/1,_,, s,,,,,,,.,.,.11, S un•nawn Surt•e OW-OPEN WATER Unilnown BofPom 118 -AOC!{ 80TTOM ue -UNCONSOLIOATEO AB ·-AOUAflC RS·· ROCKY SHOR_E BOTTOM BED 1 Cobblt-Grltlal 2 Sand , .... 4 0rglni<: MODIFIERS 1 ~ 1 Bldmd 2 Aq,l■!IC Moss 2 Rubble 1 Rcot8d VHcula, <1 F1o111,no Vascular S Unilno ... n S~ge,m 6 UM,,.....,.Su,fKP US -UNCONSOLIDto.TED EM -EMERGENT OW -OPllV WATER. SHORE u,i,1-...,...,, 8aflom 1 CobhlP-Gr~ ,,_ '""" • Qrg1n,c 5 Vf'V"l&ted 1'1 order 10 more adaqa11ery dH,;nbt -land and <11Npw11., haMau oM o, more of 1he w11er '""ll'ffllf. -1er chemitiry, so,!, 0< soe,c,1! mod,hef1. trlllV be al)l"l,ed II lhe ciHI or lower lenl m ti. h,erarch; Thi! 1.,med moc1,r,1r may atso be ~h&r:110 The K<:1'°91Cal ,v,1em WATER REGIME WATER CHEMISTRY SOIL SPECIAL MODIFIERS Non-Tidal Ttd1I Coastal Halinltv Inland Salinity pH Modifiers for • r,e,_.,,,., F-H P<e,,...,.,-Cnlt-,, F•~ ' ,1,,r,~"'1 :1.;nd#!tl . :; Cempr,ra.·y-T!dal I Hw,erl,ah"" 7t-!-,p,,rs~1•,.,. eill fresh WatM 0f!li"IC ' IIP;W., " O•H /mpt,4,ndt,d • • s .. ,.,,.,..i ' m,.,,.,~i.nl'lo fioootd ' Subtldll ., s.....,,..1.t1d•I 2 fi,t,11,ne 8 E~l,,,• " M,ne,al ' P,.-,,,.!IJ Or••-C),tcht,d ' "'1~,c,,1 S11t..t•1•e ' S.-•llt-l'locidll<! ' .A.rMi,:,a•lv Fkiodlld M l•'<1911larlyE--., s • ..._,,,,.,...,nt-Tidll 3 M..-1,,.. /Br1dusl'l/ 9 MmMal,ne e Acid ' ·~-• ,_, 0 ~#-"r Flooded w h'\ttrmMtenll,· N R'911ll•'lo FloOOad ·v ~rrnanen•-Todlrl 4 Pulyhal,ne DF,tth 1 C1rc1,1mne11t-al . Eo, ... ,ei, weno,,,,.,,., Flooded Tami,o,lf"!' • lr1.-g1,1ia,-i,,, Flooded u (ln.l...,... .. 5 Mf'lnhal,ne ,Alllal,ne ' s,,,,_.,,..,:,-,.,, ' Sawnrled Sem,pe,mantrn' 6 01,oor,■1, .... s.,.,.,.., ,_, Of'"" ' Seffl.-,,.,.,.mly l'loaded ' tnt..m,n..,11y G lnNtrm111en1,-, E ._..,. E~--Pe<--nent "f""se -• '""'"'" -onty uSf'd"' ,,,,,._ 11dall-, ,nl~ !,"'1..,.ltt< ~•rns . Cl.AH - SYSTEM SUBSYSTEM CLASS I CHARLOTTE EAST, N.C. 80°"'?'.30" J5° is:: ,\;,(t:-'J f 12']0' ~ ~',,. . ., ' : UC [,'. (/J~ ;'' •-hJI "" '" ,s u• 0~ .. t ' ' • ~ ;. : c,;c· '.:'(·: FTFT i \.;;. I ,.. , : (''. ' -~-, ,-,\'' ( . \ CHARLOTTE SE CHARLOTTE l 1000 0 100] D 1 acre SCALE 1:24000 0 WYJ le«' '()00 C D 10acres ACREAGE GUIDE SOOD , -,' R:'J•.'I '~' " -r-:-, .. ' " \ ti;~---· <i ·. "!"' Ji\J---.~l'i,, sooo 7000 F[[T l KILOMETER D 20 ■crn I Ml\.( NATIONAL WETLANDS INVENTORY UNITED STATES DEPARTMENT OF THE 11,.TERIOH SPECIAL NOTE This document was prepared primarily by stereoscopic analysis of high altitude aerial photographs. Wetlands were identified on the photographs based on vegetation, visible hydrology, and geography in accordance with Clauifica• tion of Wetland• and Deepwater H1bitab of the United St1te1 (FWS/OBS -79/31 December 1979). The aerial photographs tvpically reflect conditions during the specific year and season when they were taken. In addition, there is a m~rgin of error inherent in the use of the aerial photograplis. Thus, a detailed on the ground and historical analysis of a single site may result in a revision of the wetland boundaries established through photographic in1erpre1a11on. In addition, some small wetlands and those obscured by dense forest cover may not be included on th-,; document. SYMBOLDGY EXAMPLE SYSTEM I SUBSYSTEM I /_,.,--CLASS L2EM2F ---✓ / "suBCLASS, WATER REGIME UPLAND fNON•WETLANDi NOTES TO THE USER • Wetlands which have been field examined are indicated on the map by an asterisk i-1. • Additions or correction's to the wetlands information displayed on this map are solicited. Please forward such information to the address indicated • Subsystems, Classes, Subclasses, and Water Regimes in ltalif:$ were developed spe-cificall-i: for NATIONAL WETLANDS INVENTORY mapping. • Some areas designated as R4SB, R4SBW, OR R4SBJ (INTERMITTENT STREAMS) may not meet the defini- tion of wetland. • This map uses the class Unconsolid11ted Shore (USI. On earlier NWI maps that class was designated Beach/ Bar (BB), or Flat (FL}. Subclasses remain the same in both versions. 12'30" ''94 CHARLOTTE EAST, N.C. Other information including a narrative report concerning the wetland resources depicted on this document may be available. For information, contact: Federal. Slate and local regulatory agencies with jurisdic- tion over wetlands may define and describe wetlands in a different manner than that used in this inventory. There is no attemp1. in either the design or products of this inven-tory, to define the limits of proprietary jurisdiction of any Federal, State or local government or to establish the geographical scope of the regulatory programs of govern-ment agencies. Persons intending to engage In Ktfvitin involving modiftCatlons within or adjacent to wetland area, thoufd seek the advice of appropw-iete Fed-.1. State or lou: agencle1 concerning specified tgency regulatory ~• ... 2• 1"""" '°"',d ,~::,~1e'!::""; ::.::'1:t!!.;::tfo;" :~ ... ,;·Nif 41(iwci such 1ctivities. \ ____________ R20WH / !LINEAR DEl:PWATER HABITAT) U.S. DEPARTMENT OF THE INTERIOR FISH ANO WILDLIFE SERVICE SYSTEM SUBSYSTEM CLASS Subclall SYSTEM Re1;1ional Director (AROE) Region IV U.S. Fish and Wildlife Service 75 Spring Street S. W. Atlanta, Georgia 30303 1 -SUBTIDAL M-MARINE Rfl -ROCK U8 -UNCONSOLIDATED AB -AQUATIC BED Rf -REEF ON-Ol'EN WATE", BOTTOM BOTTOM un.1:,,,_,, Bottom 1 Bedroct 2 Rubble 1 Cobb~·Gravel , "'"' 3 Mud • Organic 1 Algal 3 Rooted Vascular 5Unenown S"""1r,g,,m 1 Coral lWorm 2 -INTERTIDAL AB -AOU-.TIC BED 1 Algal 1 Coral 3 Roo111d Vnw'-• l Wu!-m 5(.1,M.,.,,..,,5~ 1 Bedrock 2 Rubb"1 R -RIVERINE US -UNCONSQLIDA.n"O 51-fORE l Co!lhl.-G, .... .-1 2 Sand 3 M,,a 4 Org•n,c Prepared by NattOnal Wetland■ Inventory AERIAL PHOTOGRAPHY 0-Primarily represents upl•nd areas. but may include ~.-..:;;.,;.;a;:i,;,ii "-N~iidnQs suci't as man,m:;cfifie<I areu. n\lfl photo-identifiablf! aree>, uid/or unir.tfiaitior,tii omi~slons. DATE,~__/. 83 TYPE: 1-<;A nnn CIR e -ESTUARINE 1 -SUBTIDAL 1991 DATE· __/__J_ __ 2 -INTERTIDAL RB -IIOCK US -UNCONSOUOATtO AB -AQUATIC 8~0 RF-REEF CN'l-0/lfllfWArER' ,\B · A,QIJ.UIC BED RF -REEF SB · STFIEAMBED RS -IIIOCkY US UIIICONSOLIOATEO EM -EMt:P;GENT SS SCRU9-SHRUB SHORE 80TTOM 80TTOM 1 Bldrock l Rubb'!, I Collble•G,...el ,,_ '""' • o,,,- I ~I 2 MolluE l Rooted Vn,::ular 3 Worm 4 flDllll"f Ynculet S Unt,.,...., S"""-~nr II Ur,1,,.,wn Sllrlau 1 -LIMNETIC u,,.o;_,,Bot,um 1 Algal 2 Moll!Jsc J Rtl0!9d Vncu!ar 3 Wo<m 4 fl0ltl1nt Va.eu1a, S Untnown Sut,n,e,ge~ 6 Unfn.,...., Surl11tt L -lACUSTRINE SHORE I !led•ocl 2 Rubble T Cobtk-Q,...,I ,. .... '""' 4 O,;an,e 2 -LITTORAL l Pers,~nt 1 Br<>ld·lea.-NI 2 NonpersIsten1 DoN:odtnUs l~Le"'"~ Q.ec,duo..., 3 BrOlld-ler,ed E""'II'"" • Ne,,<1lo--t ... ....i E..,,;,een , .... 6 0..C,duot,J 1 c ... ,g,- f0 . FORESTED 1 B•otd•le- DoN:lduous 2 "'-tle·Leaw<t Dec:lduous l llrOl<l-l•- E""'ll''""" • Ho,edlo,·l.e.....,. E""''9'ffn , .... 8lh,;,duoi,s 7(~n SUBSYSTEM 1 -TIOAL 2 -LOWER PERENNIAL. 3 -UPPER PERENNIAL 4 -INTERMITTENT 5 -UNKNOWN PERENNIAL CLASS Subcln1 SYSTEM CU.IS ......... RB -l'IOCk 1 Bedrock 2 Rubble UB -UNCOP'fSOLIOATEO BOTTOM 1 Cobble•Gt1ve1 2 Sand '""' " Or;tnie 'Sfl -STREAMaEO '"""' l•Rtfflble 3 Cobbl,,.G,,w1 .,_ '""' & Orgarne 7\1"119'11,Md AB -AQUATIC BED I Aim-1 2 AqrnHic Moss 3 Roollld 1/acui.r • f..,.."'11 vncular ~ u,,1,nown ·--eu,,.t-$tJrl- FIS -ROCKY SHOIIE , ...... 2 Rubble "STRE.t.MaEO ,s r,m~ed to TIDAl,L 1...i INTERMITTENT SU85'1'ST1:MS. •nd CO<T>IM"•MI lhe only CLASS .-. the INTERMITTENT SU8SVSTEM ••EMrnGENT •• limttM 10 TIDAL •nd LOWER ptRENNIAL SUBSYSTEMS TM rematn,nv CUSSES are lound ;,. 111 SUBSYSTEMS P -PALUSTRINE US -U~SOl1D"TED SMOAE . 1 Cobbftt.G,...i , ""' 3 ""' 4 Or119r,ic: S \11991.iM "fM -EMERGENT 2 No,,r,,,r,<!l!ent ~-oP!NWATf11, UM,.,_ •011"'" R8 -· ROCM, BOTTOM UB -UNCONSOUOATED AB -AQUATIC BED US -UNCONSOUOATEO Ml -MOSS·UCHEN EM -EMEIIIGENT SS-SCl'IUB-SHRUB FO -FORESTEO ON -OPEN WATEJt' Unl<nrwm Bom,,., 1 Be<troc• 2 ~ubble BOTTOM 1 A/;111 2Aq.,.,,ocMoP 3 Aoot«I' V"c-ulM at FID111,rtu v .. cul., s tmt-s~~ & Uno1:,.,....,s.,,r11u SH~E 1 Cobble-Gt...el ,,,.~ '""' at O,11,noc 5 Yeg,,,iaH!d , .... 2 lOCN!n I <.•Old-l...,.J O.clduoul 2 Nffdla-Ler,ed 0.c.,uou, 3 8,0lld-lllll\liod htfl•Hn atN....ne-t~ E-G""'" s .... l5{)ttl<h,r,u5 1c ... ,"" I l!m94-lffWICI °"<=odVOUS 2 N~edlti>LIIW!I Oectduout J ll•IMd-l1n9d E""'lf'IMI ~ N&edl•·Llr,ed E""tllfNA , .... 8 Oft<dl,INI 7 f~;g,ttn RB-ROCI( eonoM , ...... lRubb11 ua -UNCOHSOllOATEO AB -AQUATIC BOTTOM aEO 1 Algal 2 AQve1,c Mou 3111"""-<IVNcular 4 Floel,ng v-ular &~S~ 0 UM,-SvrlKII ~-Ol'ENWATfR Un.t"'"""' llaUom RB ·-AOC!t BOTTOM ·-"' ,, .... UB -UHCONSOLIOATEO AB -AOIJATIC BOTTOM BEO RS -ROCICV SflQRE I Cotib11-G,11nt 2 S4ncl 1 A'9al I Bl!'dtoi:k '""' I 0,ga.,,c 2 .._u,1,c Moes 2 lllubble 3 ROl>led Vn<:ula, at Fro.1,ng Vncul• SUnfnawnS~g,,ttf e Unfn.,wn surt,.,,.. MODIFIERS US -Uf,ICONSOUOATEO EM EMERGENT ~ -Ol'EN WAT(R: SHORE Un4nown Bmtom , Cobble-G,aver '"'"' '""' at 0.,.n,c S Veg,«Med 2 Nonpe,!.OSlenl In o,~ to more ld&qua1ety de9c,itll! Wl!!tland ind dleJrwM• h1b,1a1s one or moll! of 1ht! _1., r1111irne, -t•• chamlslry, aoil. or speei•t modif,.,s m11y t-1ppfiltd 81 the clan OI' I-,.._..1 ,n 11,. h,1r■rthV Th• f11rml'd modll1•1 mty IIIO M apot+fd !o the ~olog!CII &yltlm WATER REQIME WATER CHEMISTRY SOIL -SPECIAL MODIFIERS Non-Tidal " -' Tid•I Cont■! Halinlry Inland Salinity pH Modifiers for • r,.._......,Flooded H Pe,-,...,.,,,i, Floodld • hfifici■"r F~ ., r...._a,v-Tldll '1-t,c,t,, ......... 11-fyp,,,ul,ne all Frnh W•t., 0'9■IIOC • s,,,,,_, 11 o,,,.,,.,,,,_aunded • • ktutll.cl ' 1,.1erm~11n1tr Floodld L Sulmda1 ., S.,noi,-1 fo<:!11 2 Euh~,,.. II Eu1111lme " M,Mrll ' ,.,,,,,.,,, o,,,fl#d o,,thflJ ' Amfo<:11I Subtltlll C $ellO!'l,IIIJ Ploodld IC An,!1c11tly flondad M lr,eguFa,i.,. hoo91d . ' S ■ ITliP9f""'"""'·TKhll 3 Mm>hlt,1'11 /tJrlld.,shJ 9 M,ooul,ne .... ' f■rmood • ,,,.,, 0 s...,_,,., ,laad«f W lnle,m~1em1V N R~ul■•tyF~ ., Pe,,...,...,.,. Tldal atl'l;,1~1,,,. OFrnh 1 Circumn11t11111 . E•c■vlted WlllftJr1,,_, Ftoodld h"'llOl'try • lrr1tgUl11l~f~ U Un.llOw,, S Mesoha1,no, , Allll,nl ' $11"01111~ Flooded ' !l.i11ra11111 Swm~rm.ne"' e Ol'l""lline S..w.,,, ,_, DFruh ' s.m...-,iv floodld l ,,.,H,..~teffllV G ln'8r"""""f¥Eq,ol,O<I E~ ·l'ef-maMffl ·n,ue _.,, •911•~ ••e only uSo!'d m ,,,,.._ !.dllly ,nfl""r>c■<I fr--■1"' 11'(51-■ SYSTEM SUBSYSTEM - SYSTEM SUBSYSTEM CLASS ....... I ,_ I I I I I I I " I I I I I I .. I I Soil survey <)f Mecklenburg County, North Carolina United States Department of Agriculture SoH Conservation Service ·in cooperation with Mecklenburg County Board of Commissioners and North Carolina Agricultural Experiment Station I I. ;-~ i*;·, MECKLENBURG COUNTY, NORTH CAROLINA 7/1) and common medium distin6f''·oliv·e yellow (2.5YR 6/6) mottles; moderate fine angular blocky structure; very firm, plastic, slightly sticky; few fine pores; thin continuous clay films on faces of peds; few fine pebbles; strongly acid; gradual wavy bound- ary. B23t-28 to 37 inches; reddish yellow (7.5YR 6/8) clay; many medium distinct light gray (5Y 7 /2) mottles; weak fine angular blocky structure; very firm, plastic, slightly sticky; very strongly acid; abrupt smooth boundary. Cr-37 to 50 inches; mottled yellow and gray saprolite that crushes to silt; 75 percent by volume brittle slate fragments; very strongly acid; abrupt boundary. R-50 to 52 inches; hard slate rock. ''L ·I . ThhicknOessthoft thbe dclaykey B horfizon is less 7 than 30 inc es. ep o e roe ranges rom 48 to 2 inches. ,,,., Heaction in the B horizon is strongly acid or very strongly :,:..);::_ ac1he Ap horizon is yellowish brown, pale brown, or grayish brown. The B1 horizon is strong brown, brownish yellow, or · light yellowish brown silt loam or silty clay loam. The B2t •1 horizon is strong brown, reddish yellow, or yellowish brown clay or silty clay. Mottles of chroma 2 or less ·•~:.·· ange from few to common in the lower B2t horizon. The ' horizon, if present, is clay loam or silty clay loam. , The C horizon is mottled yellow and gray silt loam or ,,,1 silt. It is 15 to 80 percent weathered slate fragments in i'I ::~:::~::: series 'i./:' ·The Mecklenburg series consists of well drained, ·• slowly permeable soils that formed in residuum from . basic igneous and metamorphic rocks. These soils are ~W;,.' on broad ridges and side slopes. Slope ranges from 2 to "-•·· 15 percent. .I.. Typical pedon of Mecklenburg fine sandy loam, 2 to 8 percent slopes, approximately 9 miles southwest of ;J .. ' Charlotte on N.C. 49, 0.8 mile south on State Road i'•· .1,.. 1122, 40 feet west of road: :_, :, ·Ap-0 to 7 inches; dark reddish brown (5YR 3/4) fine ~if} . -' sandy loam; moderate fine granular structure; friable; r1··· ·. few fine roots; few fine pores; common fine manga-i ; · nese concretions; neutral; clear smooth boundary. j/iii;:B21t-7 to 15 inches; yellowish red (5YR 4/6) clay; '#if •_ moderate fine subangular blocky structure; very firm, JI;:;' sticky, pla.stic; common fine roots; few fine pores; ! •: ·· common fine manganese concretions; common thin \,·,~ ' distinct continuous clay films on faces of peds; neu-:r.~f'". '''"'',. tral; gradual wavy boundary. ,. 2t-15 to 22 inches; yellowish red (5YR 4/6) clay; . common medium distinct strong brown (7.5YR 5/8) ~.... mottles; moderate fine subangular blocky structure; I: t very firm, plastic; few fine roots; common light and I 41 , , . .'¥: ·• ' . ,. ;_, · dark colored minerals; thin continuous clay films on faces of peds; common fine manganese concre- tions; slightly acid; gradual wavy boundary. B3-22 to 34 inches; yellowish red (5YR 4/6) clay; many coarse distinct strong brown (7.5YR 5/8) mottles; weak fine subangular blocky structure; firm; few fine manganese concretions; common pockets of sapro- lite; few fine flakes of mica; slightly acid; gradual wavy boundary. C1 -34 to 45 inches; mottled strong brown (7.5YR 5/8) and yellowish red (5YR 4/6) saprolite that crushes to clay loam; massive; friable, sligl1tly sticky, slightly plastic; common fine flakes of mica; slightly acid; diffuse boundary. C2-45 to 65 inches; very dark grayish brown (2.5Y 3/2) and light olive brnwn (2.5Y 5/4) saprolite that crushes to loam; massive; friable; few pockets of strong brown ,clay in upper 10 inches; common fine flakes of mica; neutral. Thickness of the clayey B horizon is less than 32 inches. Depth to bedrock ranges from 48 to 60 inches. Reaction in the B horizon ranges from medium acid to neutral. The Ap horizon is reddish brown, dark reddish brown, brown, or yellowish red. The B2t horizon is red or yellowish red and has few to common brown to red mottles in the lower part. The B3 horizon, if present, is strong brown or yellowish red. The C horizon is commonly variegated red, yellow, brown, gray, and black saprolite that crushes to loam, sandy loam, sandy clay loam, or clay loam. Monacan series The Monacan series consists of somewhat poorly drained, moderately permeable soils that formed in recent alluvium. These soils are on flood plains adjacent to streams. The width of the flood plain varies. Map units are commonly long and narrow. Slope ranges from 0 to 2 percent. Typical pedon of Monacan loam in Long Creek Com- munity, 700 feet south Beatties Ford Road bridge, 250 feet east of the channel of Long Creek in pasture: Ap--0 to 7 inches; brown (7.5YR 4/4) loam; moderate medium granular structure; friable; many fine roots; neutral; clear smooth boundary. B1-7 to 14 inches; yellowish red (5YR 4/6) loam; common fine distinct light olive brown and brownish yellow mottles; weak fine subangular blocky struc- ture; friable; common fine roots; . common medium pores; neutral; clear smooth boundary. B21-14 to 21 inches; brown (7.5YR 4/4) silty clay loam; common medium distinct olive gray (5Y 5/2) mot- tles; weak fine subangular blocky structure; friable; common fine roots; common• medium pores; few I '-I I I I I I I 42 black organic specks; neutral; clear smooth bound-ary. B22-21 to 25 inches; dark brown (1 0YR 4/3) fine sandy loam; ma·ny medium distinct gray (SY 5/1) mottles; weak· medium subangular blocky structure; friable; few fine roots; common medium pores; · neutral; abrupt smooth boundary. B23g-25 to 33 inches; dark gray (N 4/0) sandy clay loam; many coarse distinct yellowish brown (1 0YR 5/4) mottles; weak medium subangular blocky struc-ture; firm; common medium pores;. neutral; clear smooth boundary. B24g-33 to 43 inches; gray (5Y 5/1) sandy clay loam; common fine distinct dark yellowish brown mottles; weak medium subangular blocky structure; friable; few fine pores; neutral; gradaul wavy boundary. B25g-43 to 65 inches; light gray (SY 6/ 1) sandy clay; common fine distinct dark yellowish brown and common medium distinct gray (N 5/0) mottles; mas-sive that parts to weak medium subangular blocky structure; very firm; some large pockets of gray sandy loam; many brown and black specks; neutral. Loamy layers extend to· a depth of more than 60 inches. Depth to bedrock is more than 60 inches. The B horizon ranges from strongly acid to neutral. The Ap horizon is brown, dark brown, or dark grayish brown . .. -. . The B1 horizon is yellowish red or brown loam or clay loam. The B2 horizon is strong brown, brown, dark brown, or yellowish brown in the upper part and brown, · light gray, gray, or dark gray in the lower part. Texture is I I I I fine sandy loam, sandy clay loam, silty clay loam, clay · loam, or sandy clay. Clayey textures are below 40 inches. The C horizon, if present, is stratified with textures ranging from loamy sand to clay. Pacolet series The Pacolet series consits of well drained, moderately permeable soils that formed in residuum from acid ig-neous and metamorphic rock. Slope ranges from 15 to 45 percent. Typical pedon of Pacolet sandy loam, 25 to 45 percent slopes, near Lake Wylie, 3/8 mile south of N.C. 49 on State Road 1109, 3.25 miles southwest on State Road 1102, 50 feet east of road in woods, about 350 feet past I junction of State Road 1101: 01-1 inch to 0; undecomposed and partly decomposed hardwood litter. I · A 1-0 to 3 inches; very dark grayish brown (1 0YR 3/2) sandy loam; moderate fine granular structure; friable; many medium roots; medium acid; clear smooth boundary. I _ 821-3 to 17 inches; red (2.5YR 4/6) clay; moderate .. medium s_ubangular blocky structure; firm; few fine I -L~SZiti,:Willliil.iffil\l, cs Hi& l&u+.IW:.l'Wiiifulifotii&W.tA SOIL SURVEY roots; common fine flakes of mica; common fA · ·. crystals of feldspar; strongly acid; gradual w;fl/' boundary. B3-17 to 31 inches; red (2.5YR 4/8) clay loam; weak fine subangular blocky structure; friable; common fine flakes of mica; common pockets of saprolite in lower pari-, strongly acid; gradual wavy boundary. C1-31 to 41 inches; mottled red (2.5YR 4/8) and yel-lowish red (5YR 5/8) saprolite that crushes to sandy loam; massive; friable; many fine flakes of mica; very strongly acid; gradual wavy boundary. C2-41 to 65 inches; mottled red (2.5YR 4/8), yellow (10YR 7/6), yellowish red (5YR 5/8), and reddish yellow (7.5YR 7 /6) saprolite that crushes to sandy loam; many fine flakes of mica; very strongly acid. The thickness of the clayey 8 horizon is less than 24 inches. Depth to bedrock is more than 60 inches. Reac-tion ranges from medium acid to very strongly acid in the B horizon. There are few to many flakes of mica through-out most subsurface horizons. The A 1 horizon is very dark grayish brown, dark gray-ish brown, or very dark gray. There are A2 horizons in some pedons. The 81 horizon, if present, is yellowish red or red sandy clay loam or clay loam. The B2t horizon is red clay or clay loam. The lower B2t horizon has yellow mottles in some pedons. The 83 horizon is red or yellowA ish red clay loam or sandy clay loam. ., The C horizon is variegated red, yellow, brown, and pink saprolite that crushes to loam; clay loam, or sandy loam. Vance series The va·nce series consists of well drained, slowly per-meable soils that formed in residuum from acid igneous and metamorphic rock. These soils are on broad ridges and side slopes. Slope ranges from 2 to 15 percent. Typical pedon of Vance sandy loam, 2 to 8 percent slopes, 0.4 mile east of N.C. 115 on State Road 2457 (Alexanderana Road), 100 feet south in field (0.6 mile southeast of North Mecklenburg High School): Ap-0 to 8 inches; yellowish brown (10YR 5/4) sandy loam; moderate medium granular structure; friable; many fine and medium roots; many medium pores; few earthworm casts; slightly acid; abrupt smooth boundary. B21 t-8 to 17 inches; strong brown (7.5YR 5/6) clay; moderate coarse prismatic structure parting to strong medium and coarse subangular blocky; very firm, sticky, plastic; common fine roots; common fine pores; thin continuous clay films on faces of peds; few earthworm casts; strongly acid; clear smooth boundary. 8221-17 to 26 inches; strong brown (7.5YR 5/6) clay;. common medium prominent red (2.5YR 4.18) and ""'*' - U.S. IJEPAHTMENT OF AGH ICULTliHE SOIL CONSERVATION SERVICE ,:11 . ' -... . ,: ~~!~ceB "'""' ' -.-::.,..~!5;::S~g :,,.,_3',;r,/, • 1" ·t ' ~ Mt.i::.'1 "" • . ,,-, . .. -. -, "'I ,· ~--'-.;,_ -:, ~-..,~., ~... . .r.-.. l ?A ~-·;.t;;;; %',·. •f:Z, rJ-:'7~\";! IIO -•. 1--~..:1:=r::-·,·~--- ~ k -I" SHEET NUMBER 6 MECKLENBURG COUNTY, NORTH CAROLINA I It I I I I I I I I I I I I I U. S. DEPARTMENT OF AGRICULTURE Soil Conservation Service Technical Guide Section ll-Ac2 June 1991 HYDRIC SOILS Mecklenburg County, North Carolina Hydric codes (HCJ: I • 2 • 3 • Vegetation codes (VCJ: 1 • 2 • Hydric soils, only.because of saturation for a significant period during the growing season: Hydric soils that are frequently flooded for long or very long periods during the growing season; and Hydri c soils that are ponded for 1 ong or very long periods during the growing season. Hydric soils that support woody vegetation unper natural conditions; and Hydric soils that do not support woody vegetation unde~ natural conditions. IMPORTANT NOTES: (I) Hydric soils in this county cannot be fanned under natural conditions withoUt removing woody vegetation or hydrology manipulation. (2) Some map units and included soils listed as hydric soils in this county may not meet the definition of hydric soils and wetlands because the hydrology has been altered through drainage or other.manipulations. A. Map units that are all hydric soils or have hydric soils as a major component. Map Unit Symbol NONE HC VC Hap Unit Name B. Map units with inclusions of hydric soils or have wet spots. Map Unit Symbol Map Unit Name HeB J,A Ho Helena sandy loam, 2 to 8 percent slopes Iredell fine sandy loam, 0 to 1 percent slopes Monacan loam Hydric Inclusion poorly drained soils poorly drained soi 1 s poorly drained soils . HC VC Nonnal location Inclusion depressi ans a 1 ong dra i nage.,.ays depressions depressions adjoining uplands sides lopes • • ,~, -. U.S. ARMY CORPS OF ENGINEERS Wilmington District I Action ID: /996 oo .3b'i< County: . ,,..,..El.!K 1...£.N 50f...6-- Notification of Jurisdictional Determination I Property owner/Authorized Agent NC-D 2:v'T:.S t:o,,J o ,=. I Address SUP!!.&!=-oJND S1£.c.',t.<.>..J,. An-,,J ~ /./ 01 o !3E../....l-'l'./J ?-.oAJJ RA LJSrC..-lf ) I Telephone Number 9 / 9 -7 .3 3 -2:;J O I ,X 3 i ,;( Size and Location of Property(walerbody, Highway name/number, town, etc.) A D."I -Ml::L£ LCJIIJl.,_ .Se'.,6-ME.A.i r Of-AN uAJ/JAMl!D I 5'rEvJA&rs c.g.UK 8t!..nJ~.E.v 8'1!.?-F-yif-C.U f!.oAD AA.JD [HE. C6JJ"l=Ll)J:.NCT. Iwd•)::)'1tW:5h'fl:.WAl-r.5(. II cf._a.K,l .So\.lrH AAirl PAP..ALt...cl-TT) Ff.EEDoltA /l.OAD A.,..... I n 1catc ,ichoflhc o owmgappy: C.->-IA/?..i...or,J!.. I ,, • There arc wetlands on the above described property which we strongly suggest should be delineated and surveyed. The su1veyed wetland lines musl be verified by our staff before the Corps will make a final jurisdictional determination on your properly. • Because of the size of your properly and our present workload, our identification and delineation of your wetlands cannot be accomplished in a timely manner. You may wish to employ a consultant to obtain a more timely delineation of the wetlands. Once your consultant has flagged a wetland line on the properly, Corps staff will review il, and, if il is accurate. we strongly recommend that you have the iine surveyed for final approval by the Corps. The Corps will nol make a final jurisdictional determination on your property I I I without an approved survey. • The wetlands on your lot have been delineated, and the limits of Corps jurisdiction have been explained to you. Unless there is a change in the law or our published regulations, this determination may be relied upon for a period not to exceed three years from the date of this notification. G)rhere are no wetlands present on the above described property which are subject to Lhe permit requirements of Section 404 of the Clean Water Act (33 USC 1344). Unless there is a change in the law or our. published regulations, this determination may be relied upon for a period not to exceed three years from the date of this notification. ,t+E. C~NN~L. r .S A f!..E.i:Ni.A nED WA~P-. oJ: TH! U.5 , • The project is localed in one of the 20 Coastal Counties. You should contact the nearest Stale Office of I Coastal Management lo determine their requirements. Placement of dredged or fill material in wetlands on this property without a Department of the Army permit is in most cases a violation of Section 301 of the Clean Water Act (33 USC 1311). A permit is I not required for work on the property restricted entirely to existing high ground. If you have any questions regarding the Corps of Engineers regulatory program, please contact ~=,,~v'?-:\l LvAJD at 7oq-::i.. 71-L.fll'.5"7 I Property owner/Authorized Agent Signature -----~----------------- Project Manager Signature /2,t;:; .,., IN, .Q ate I// o 7 / 9 S-Expiration Date _l_l /,__o_7+/_9~[( ______ _ URVEYrPLA~ OR FIELD SKETCH OF DESCRIBED PROPERTY AND THE WETLAND · I DELINEATION FORM MUST BE ATTACHED TO THE YELLOW (FILE) COPY OF THIS FORM. I CESA W Form Sr.t:, IOCT92 l~C SUPERFUND SECTION Fax:'019-733-4811 Au 1 '95 ,I, ¼ ,r-4'1, -/1( .,,:--·. ' :Ill \ ,{',, --\....: l .. 11~ ' .. ~~'i.r-,,._'.:.1,/ ·1· "",~ ,:!Sf~,;,' --~-~'%, ,,, .;;~-·'t·' \ 4,;r/ ·1· r /. ea 1;;f \, /' ~~ / I (:\._:, \ ..__ /\ . -, .. ;11 0~~i~ , ~;_,.;;!!/' ! '\,\}~: -/I '.j~~~~i( I,,, "r , , ,, ,_;,., ~&~ ... 1,111 ,' ·--~ ,.' :,, · ··./"-~ :!iii \\ \' --. .,.,:__: ·<::...::·· • { ' ~II<''''\ . , I~~,. ,,:_ - \\~ ~-" . ✓ P.02/0) • I I I I ~ I I Memo Date: August 20, 1996 To: File From: Douglas Moore 4 ~ Environmental Chemist NC Superfund Section Re: Natural Heritage Program Trip report Cherokee Oil Company site 1201 Berryhill Road Charlotte, Mecklenburg Co., NC US EPA ID: NCO 980 799 019 On Tuesday, August 20, 1996, Doug Moore reviewed the 1:24000 scale Charlotte East, Charlotte West, Derita and Mountain Island Lake topographic quadrangle maps located in the North Carolina Natural Heritage program files for occurences of significantly rare, threatened, or endangered plant or animal species along the 15 mile downstream distance and within a 4 mile radius of the subject site. The review included a check for registered natural areas. There were no observations of significantly rare, threatened, or endangered plant or animal species in the unnamed tributary to Stewarts Creek or Stewarts Creek, extending frm the site PPE downstream to the confluence withi Irwin Creek. A review of the topo maps identified two historic observations of the endangered mussel, Lasmigona decorata, or Carolina Heelsplitter, in Irwin and Sugar Creek within 15 miles downstream of the site. The closest observation was located near the confluence of Irwin and Sugar Creeks, approximately 4.6 miles downstream of the site. The last reported observation was in the 1870's. A survey of the Irwin and Sugar Creek drainage conducted in the 1980's by Brunswick College professor Eugene Keferl did not locate any observations of the mussels in these two creeks. No observations of endangered, threatened or significantly rare plant or animal species were identified within a 4 mile radius of the subject site. Likewsie, there are no registered natural areas within a 4 mile radius of the site. ]/;. ~/ y I •• g I I Ref. 38 i;S':J U.S. Fish & Wildlife Service Asheville Field Office 100 Otis Street Room 224 Asheville, NC 28801 The Einal Report on a Status Survey o.f the Carolina Heelsplitter, Lasmigona decorata and the Carolina Elktoe, Alasmidonta robusta Prepared by Eugene P. Keferl Department of Natural Sciences and Mathematics Brunswick College Bruriswick, Georgia 31523 and Rowland M. Shelley North Carolina State Museum of Natur~l Science Raleigh, North Carolina 27611 Prepared For U. S. Department of the Interior Fish and Wildlife Service and North Carolina State Museum of Natural Science 9 July 1988 ' I ,. altered by some form of urbanizati~n. Seven species of naiades were collected in the Saluda River system, most from areas just below impoundments on the Saluda River and in the Ninety Six -~ creek drainage. See Tables 1 and 4 for a summary of the Mollusca collected in the Saluda River System. Lasmigona decorata was found in three separate drainages; Waxhaw creek, a small tributary of the Catawba River; Goose ~reek, a small tributary Rocky River of the Pee Dee River system; and the Lynches River, a larger tributary of the Pee Dee River system. All three streams have their headwaters in Union County, North Carolina, which is adjacent to and southeast of Mecklenburg County. Mecklenburg county is the source of most of the historical records. Of the 196 different sites on 92 streams and rivers in the Catawba River system examiP-ed (see Figures 3 and 4), only WaxhaW' creek has a population of L. decorata (See Figure 8). See Table 1 and Appendix I for a summary of the collections from the Catawba River system. Naiades were found in only eighteen (20%) of the 92 streams and rivers, and in just three.above Charlotte, Mecklenburg County. With the exception of a few populations in lower Mecklenburg and those in Union Counties, most of the naiades in the Catawba River system occur in South Carolina. The chances of finding populations of 1_,._ decorata in the Catawba River system above Charlotte are remote, since the entire basin j. /· 10 has been greatly altered by man. Channelization, dredging, damming, agricultural run off, siltation, sand mining, and .i increased runoff due to urbanization are very ev,ident throughout the system. We doubt that the Corbicula invasion has been a factor in the decline of the naiades in this river system. Considering that there were no traces of old shells, these streams probably have not had naiades in them for a long time. Besides, just 49% of the streams examined had Corbicula. Most streams with good naiad populations also had Corbicula. Waxhaw Creek Waxhaw Creek is a small narrow, meandering tributary of the _I Catawba River draining Union County, North Carolina and a small "J • ' ' ! ::)part of Lancaster County, South Carolina. It originates in 11 southwestern of Union County (See Figure 8), approximately 13 kms 11 southwest of Monroe and it flows southwestward to the Catawba I River about 13 kms northwest of 'Lancaster. It is about 3 6 kms ' I long. Most of Waxhaw Creek flows through an agricultural area, and at the-present time, it appears relatively undisturbed. The I _stream is bordered by wooded vegetation on seventy-five percent I of its length. It is characterized by numerous fallen trees and sunken logs, and consequently has many long pooled areas. I The waters remained cool most of the summer. The turbidity I was usually moderate to high, clearing only in late summer. of the banks are moderately steep with exposed ciay, so a little ! Most 11 I II I ·Element Occu,·rence Recore! LASMIGONA DECORATA 08/13/91 1,..-,_denti fie r-s: .":/ Elcode EOI! State: _ EOCODE: IM8IV22040*004*NC IDENT: Y l SCOMNAME: CAROLINA HEELSPLITTER II ELEMENT RANKS: GRANK: Gl NRANK: NATION: US SITECODE: I Locators: SITENAME: SURVEYSITE: PRECISION: G QUADNAME: CHARLOTTE fiEST FORT MILi_ QUAD MARG DOT TEN CODE: NUM: NUM: TEN: 3508028 2 3508018 l LAT: 350812N S: LONG: 0805455W N: DIRECTIONS: SUGAR CREEK. LJTERSHED: 03050103 Status: • SURVEYDATE: 1987 EORANK: X E: W: LAST08S: EORANKDATE: 91-08-13 FONUM: .i SRANK:· Sl FIRST08S: COUNTY- CODE: NCMECK EORANKCOM: KEFERL ·, DECQRATA AND FOUND THIS STREAM. SEARCHED LONG CREEK DURING THE STATUS SURVEY NO EVIDENCE THAT THEY STILL SURVIVE IN FOR L. EODATA: l SPECIMEN FROM THIS CREEK IS DEPOSITED NATURAL SCIENCES AT PHILADELPHIA. IN THE ACADEMY OF Descr~ption: GENDESC: MEDIUM-SIZED PIEDMONT STREAM WHOSE HEADWATERS ARE LOCATED IN THE WESTERN PART OF CHARLOTTE. ::i,IELEV: ~rot~~i;~~; ~ORELAND: a.~GMTCOM: t,, Jn COM : IJwnershio: WNER: IOWNERCOM: ~ i . SIZE: MANAME: CONTAINED: MOREPROT: MOREMGMT: TNCINVOLVE: OWNERINFO: l • ) 1.-~ .. • ''Ld e n t 1 f :t_§.C.'?. : Element Occurrence Record LASMIGONA DECORAT~ 08/ 13/91 I Elcode EOtt State: EOCODE: IMBIV22040*003*NC I DENT: Y NRANK: FONUM: SCOMNAME: CAROLINA HEELSPLITTER l ELEMENT ~ANKS: _GRANK: Gl l_l,oca to rs: !NATION: us SITECODE: lsrTENAME: SURI/EYSITE: I IPRECISION: G iQlJADNAME: f HARLDTT E WEST ' LAT: 351135N I LONG: 0805441W I QUAD CODE: 3508028 S: N: E: W: ~IRECTIONS: IRWIN CREEK. ;'JTERSH ED: 03050103 ~tatus: MARG DOT TEN NUM: NUM: TEN: 1 DRANK: X EORANKDATE: 91-08-13 SR~,NK: Sl FIRSTOBS: COU~!TY- CODE: NCMECK tSURVEYDATE: 1987 LASTOBS: 1870' S ORANKCOM: KEFERL SEARCHED IRWIN CREEK DURING THE STATUS SURVEY FOR L. DECORATA AND FOUND NO EVIDENCE THAT THEY STILL SURVIVE IN lfHIS STREAM. ' ~ODATA: THIS WAS THE LOCATION OF A SYNTYPE OF L. DECORATA. 9 I esc r i t ~QD.: SPECIMENS ARE DEPOSITED IN THE ACADEMY OF NATURAL SCIENCES AT PHILADELPHIA. ENDESC: SMALL PIEDMONT STREAM WHQSE HEADWATERS ARE LOCATED IN THE WESTERN PART OF CHARLOTTE. tLEI/: Protection: I MACODE: ( ORELAND: ()TCOM: tROTCOM: (,)wnershig_: IJWNER: IJWNERCOM: SIZE: MANAME: CONTAINED: MOREPROT: MOREMGMT: TNCINVOLVE: mmERil~FO: i I i i i I G.ita•ba River-Fishing Creek Pond G.ine Creek Ca.p Creek Waxha, Creek Tilelve Mile Creek East Fork Twelve Mi le Creek West Fork Twelve Mile Creek Six Mi le Creek Sugar Creek Unnalled Tributary Steele Creek McAlpine Creek McMu I I en Creek Fourm i 1 e Cree!'. frvins Creek G.l•pbe 11 Creek Little Sugar Creel Briar Creek Kings Br~nch Ir.ir. Creek I~ Coffey Creek Cata,ba River-Lake Wyiie Big Allison Creek Beaverdam Creek Crowders _Creek I I I I Sooth Crowders Creel: Cataoba Creek South Fork G.ltawba River Long Creek I Little Long Creek Hoyle Creek Beaverdam Creek Indian Creek Hoo,ards Creek Clark Creek Mai den Creek Pott Creek Jacob Fork Henry Fork Paw Creek I . Lo~: c;~~ch Gutter.Branch I . Mcinture Creel _ ... Dutch.ans Creek (,·J South Prong Staale, I' Ki I I ians Creek LeePers Creef Reed Creak I Creek North ·carol ina Collections In The CATAWBA RIVER SYSTEl'I Species Collected For The North Carolina State Museum \ i:,,.>' c. ~~ Anodon ta imbecillis <J Alasmidonta varicosa ------------------- J Dead Page 3 .\ Lasm19ona decor a ta 0 Strophitus undulatus ----------------------------- 1 Alive, 1/2 Dead \( Vi llosa·.~ delumbis 'Z.. Vil losa constricta ----------------------- 10 Alive, 2 Dead 1 Alive 2 Alive Alive Alive I '-I I I I I I I ,,. I) I I I I I •• I I MEMO Date: To: From: Topic: 06/07/93 File Douglas Moore &_f,,A,u.~ Environmental Chemist NC Superfund Section Irwin/Sugar Creek endangered species Cherokee Oil Site NCO 986 190 239 Ref. 39 on Friday, June 4,1993, I spoke with Dr.Eugene Keferl of Brunswick College (l-912-264-7233). Dr.Keferl had coauthored a study of endangered freshwater mollusks in Mecklenburg County and parts of South Carolina. Dr.Keferl stated that they studied many of the drainages in Mecklenburg County for endangered mollusks including Lasmigona decorata. They studied the Irwin and Sugar Creek drainages from above Charlotte down to the Catawba River in 1986-1987. No mollusks were found in Irwin Creek or Sugar Creek to the Catawba River. \cherokee\mollusk I • I I I I I I I ,. I I I I I I .. I I Site Name: Site Number: Cherokee Oil Company NCD 980 799 019 Site Location: Charlotte, Mecklenburg County, N.C. Date: Latitude: 35 14 19.0 Longitude: 80 52 30.0 August 18, 1995 Calculation Results Population Distance from Site Location Per Ring Cumulative 0 to 1/4 mile 786 786 > 1/4 to 1/2 mile 1,396 2,182 > 1/2 to 1 mile 8,815 10,997 >I to 2 miles 24,582 35,579 >2 to 3 miles 36,343 71,922 >3 to 4 miles 35,143 107,065 Number of Households Per Ring Cumulative 329 329 505 834 3,057 3,891 9,850 13,741 . I 5,045 28,786 15,226 44,012 Note: The populations and number of households within,specified target distance rings were calculated for the NC Superfund Section by the NC State Center for Geographic Information and Analysis using the 1990 US Census data. These values were calculated by summing the population and the number of households data for each census block located within each target ring. For census blocks lying only partially within the ring, the per cent area of the block within the ring was multiplied by the population and household densities of the block. -I I I I I I •• I I I I I I I •• I · UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 4 · REcF:,. ,. ;i::· :-., MAR O 8 1996 Mr. Dwayne Alexander Vice President Rhyne, Alexander, Mattox 1100 South Tryon Street Suite 205 Charlotte, NC 28203-4239 3◄5 COURTLANO'STREET. N.E. ATLANTA. GEORGIA 30365 MAR 1 3 1996 Realty Co. RE: EPA information related to property at 2401 Tuckaseegee Road owned by Mr. Gene Miller Dear Mr. Alexander: This letter is to provide additional infonnation you requested related to the environmental condition of the above referenced property. Aa you are aware, the u. S. Environmental Protection Agenc:y,,(EPA) EmE!rgency Response & Removal Branch (ERRB) ·uti·lized th~ pr?pe;i::t}f, il.f! a. teml?orary staging area fo7 dr~a·during the._ !>UP;El.rfund :z:emC>val . ac:tion .for the· Cherokee Oil· SJ.ta_ across the street. · .. ·· ... •· " .. • . · . . After.ERRB_disposed of the drums. and their contents offsite, the top 3'td 4.inches of soil was removed from the drum staging area . This soil was tested (see attached analytical;samples CO-WS-20 & CO-WS-20), and EPA detennined that the soil was not.hazardous. The soil was utilized to backfill and grade areas of the Cherokee site across the street. After removing the top layer of soil; the property was divided into four (4) areas or grids for the purpose of collecting samples to confinn that no significant contamination remained. The location of grids 1, 2, 3, and 4, and their associated sample identification are shown in Figure 1. The grid areas cover all areas of the property that EPA conducted waste handling activities. The samples were collected per EPA protocol, and the results are attached. The results indicate that no significant contamination remains on the property. To restore the site to its original condition, a minimum of 3 to 4 inches of clean topsoil was spread across the staging area and t.he area was seeded. Although not needed, this soil serves as an additional barrier between the surface and the former staging area after scraping. As I.have indicated to you, EPA does not provide any kind of certificatio.n or "clean bill oi; heal th'·' for any property we are involvedwith'rio matter what the. circumstances; however; I ·can say that·basE!don the EPA sample_results and my knowledge of the I •• I I I I I .,_ activities EPA conducted on this property, the property poses no environmental or health threats. Of course, in the very unlikely circumstance that another source of contamination was disc.overed on the property (i.e. buried drums), EPA would re-evaluate the potential threats . · EPA ERRB plans no additional activities on the property with the exception of reseeding in the spring if necessary. The North Carolina Department of Environment, Health and Natural Resources (NCDEHNR) plans to conduct an investigation of the site which may or may not include the drum staging area. The NCDEHNR has been provided with the sample data and fully understands the circumstances associated with the drum staging area. I suggest you contact Mr. Doug Moore of NCDEHNR at 919/733-2801 X315 for information regarding their investigation. I hope this information will be of assistance, and as I've stated previously, I would be glad to discuss·, the site with any party who has a concern. I you wish to discuss the information, please call at 404/347-3931 X6135. ! Sincerely, I I js~r. •• I I I I I I I •• I On-Scene Coordinator Attachment(s) cc: Gene Miller w/o attachments Doug Moore, NCDEHNR w/o attachments -j-· • L. • - - '-' I·· - I ., ..... Drum &rree-r I ,- ' i --- /»V•·/J!l••' I I i I. I ' ' _'f ; • -- ' i .... ! -- \ -· -i -I ' .. -l- i. i i i ! - ~j -- ··-! - 1----! ' i ~-·! I-I l ---i---i --I -1 I I I ..1_ -! I 1- ' I I I I I -I ! I I I i I ! ----1--· I - -✓ ! ! i.. ' I - i . ' ••'.: . ' ' I- ' ' --j --; --i ' __ _J I k' --L 1.- [ i I--I , I ' ' I· -· 1-· i ' I !. I ' -I ---' ' !.,.-_ ! _.. ' - - - - - -,--_ ~ell,{ lt1vu\{l "<----· -~ <!l.'t>n!('clinlion + , ,_ :G" Se .s Corp. O • O.H. MATERIALS CORP. • P.O. BOX 551 • FINDLAY, OH 45839-0551 J _.J PROJECT NAME CllENrS REPRESENTATIVE ¼vt Sn,,,):,_ ci I z ::E w ,_ 7 8 9 10 ffi 3 4 SAMPLE NUMBER ITEM NUMBER DATE a. a, ::E < TIME O er 0 CJ IPRoJecr LocAr10N i_J.oO Dri,,,..,.. > ~. [L,,,lo.J+, r•J,C... J'l.JO'b SAMPLE DESCRIPTION (INCLUDE MATRIX AND POINT OF SAMPLE) c,~,; --/ .J!:r""v•-l'o~\ (,,_ "~ lo.,. ')'-e_ r___;,J"ljj l,,,f,r, , • : I I .. f;, .1 ! .,, ( ,.I, ">. ( t ,Ip /.._,.~ J-fi L.J :~I .I-~ I Sc. , ·- Dr-• -2.1,1. -fl.c, k .,., I L:4~ .I' TRANSFERS RELINQUISHED BY TRANSFERS ACCEPTED BY DATE 419-423-3526 ANALYSIS DESIRED {JNDICATE SEPAnATE CONTAINERS) -0 - - - •• LAB COPY Form 0019 Field Technical Serv·1ces 1614 2 8 Rev 08/89 REMARKS CEC-07-1995 17:34 FROM SAVet-!NAH LABS TO 9'. 7043911147 P.02 SL SAVANNAH LABORATORIES & ENV/RONM.NTAL SERV/Clis:, INC. I 1. I 5102 LaAoche Avenue• &vannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I I I ll.r. John Rhyne CHM Corporacion 5335 Trianglo Pkwy. Suite 450 Nor~roaa, ca 30092 CC: Jack Kilbarger P..!l~ORT OF P..!lSOLTS LCG NO: S5-56748 Received: OS DEC 95 Reporttd: 07 DEC 95 Purchase Order: 1016477 Project: 16817 Cherokee Oil sampled ay: ~lient DATE/ LOG NC 56746-1 S'718-l 56748-3 56748·4 56748-5 SAMPLE DESCRIPT.ON, SOLID OR SEMISOLID SAMPLES TIME SAMPLED I I \\., CO-WS-33 \,,:'-.: ,. CO-WG-)1. , ' , .. -.,:....__ CO-WS-35 " " 2 CO·WS-36 ,, '·' A. CO•WS-37 " I PAAAMETI.:R S6H8 ·1 •• I I I I I I I· • I I l,2-Dichloropropane, ug/kg dw <5.7 trans· 1, 3 •Dichlorop:-opene, <;i. 7 ug/kg dw Tric.~loroethene, ug/kg ~w <5.7 Dibromochloromethane, ug/kg dw <5.7 l,l,2-Trichloroethane, ug/kg dw <5.7 Benzene, ug/kg dw <5. 7 .cis-1,3-Diohloropropene, ug/kg dw <5.7 srorno:o:rm, ug/~g aw <5.7 2-Hexanone, ug/kg dw <28 4 .. MAt:hyl .. :i.-J.")P.T"lt.:.nr,ni:,, c?.~ (MIBK), ug/kg dw Tetraohloroethene, ug/kg dw 15 Toluene, ug/kg dw 7 .6 Chlorobenzene, ug/kg dw <5.7 ~s:hylbQn%QrlQ, ug/,:g dv •. 9 Styrene, ug/kg dw <5 .7 Xyl11nes, ug/l::g dw 52 Surrogate Toluene•d8 96 t Surrogate -4·Brcxnofluoroben•ene 95 t Currogata -l,~-Di~hloroeth-.no-d• ~S \ Oats Analyzed l2.06.9S :i6748-2 ---. --.. --- -<6. 0 <6.0 <6.0 <6.0 <6.0 -<6. 0 <6.0 <•. 0 <3 C c~n <6.0 <6.0 <6.0 --:=' .o <6.0 26 96 t 100 % 102 ' 12.06.95 ---------- ~674:9-3 ---------- <750 <750 "'1,0 <750 <750 <750 <750 <7SU <3800 c3aoo <750 <750 <750 ;:750 c750 <750 100 t 99 t 88 .. 12.07.95 -.... ---.. -.... l2•04·9S/lSOO 12-04-H/1440 12-04·95/l420 12·04·95/1450 12-0f-95/1430 5(;740-4 <6.1 <6.1 <5.1 <6.1 <6.1 <6.1 <6.l <li.l <30 <30 <6.1 <6.1 <6.l <,.1 <6.1 c6.l 1:0 t 1:22 t 1!6 "' 12,07.95 5G?49 5 -<7. s <7.5 ~7.5 <7. 5 <7.5 c7.5 <7.5 <7.S <37 <37 <7.5 <7.5 <7.5 <7.~ <7.5 <7. 5 98 t 94 t p, \ 12.07.95 ............... -...... ----.. - CEC -07-1995 1 7: 35 FROM SRlJf'NNRH LABS TD 9: 7043911147 P.03 I s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC . •• I I I I I I I •• ,' I I I I I I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 l'.r. John R.".!yne CHM Co:r:poro.tion 5335 Triangle Pk"Y. Suite 450 Norcro~s, GA 30092 CC: Jack Kilharger R,E PORT OF RE SUL TS too NO: S5•56748 Received: 05 DEC 9S Reported: 07 DEC 95 ~ureh~3e Order: 101S177 Project: 16817 Cherokee Oil Saa1pl~d Ely: Cl:.er.tc Pac;e 3 DATE/ LCG N'O SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED ------··-----------------------------------------------------................................. . 56748·1 56748-2 56746·3 S674S·4 56748·5 CO-WS-33 CO-WS-34 CO•WS-35 CO·WS-36 CO-WS-3 7 TCL Sernivolatiles (8270) Phenol, ug/kg dw bis(2·Chloroethyl)ether, ug/kg 3-Chlorophcnol, ug/kg dw 1,3-Dic:hlorobenzene, ug/kg dw l,4-Dichlorobenzene, ug/kg dw 1,2-Dichlorobenzene, ug/kg dw 2·Methylphenol (o-cresol), · ug,/kg dw 2,2'-0xybia(l·Chloropropane ) (b:.s-2•chloroisoProPYl ether), ug/kg dw 3·Methylphenol/4•Methylphen ol(m&p•crasol), ug/kg dw N·Nitra•o·di-n•propylamine, ug/kg dw Hexachlcroethane, ug/kg dw Nitrooenzene, ug/kg dw lsophorone, ug/kg dw 2-Nitro~he~ol, ug/kg dw <380 dW <380 <3SO <380 420 <380 <380 <380 <380 "380 <380 <380 <380 <380 ----······ <400 <400 <400 <400 <'400 <400 <400 <400 <400 <400 <400 <400 <400 <400 .. .. .. .. . .. -... - <400 <400 <400 <400 <400 c400 <400 <400 <400 c400 <400 <400 c400 c400 . -----.. -.. - 12-04-95/1500 D-04•95/1440 l2·04·95/l420 12·04-95/l450 12·04 ·95/l4JO <400 <400 <{00 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <400 <430 <430 <130 <430 <430 <430 <430 d30 d30 d3C <430 <43C <430 c430 ............. . --. -....... CEC -07-1995 l 7: 35 FROM SAVF'NolAH LABS TO 917043911147 P.04 I s L SAVANNAH LABORATORIES . & !NVIAONMENTAL SmVICES. INC . •• I 5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354•7858 • Fax (912) 352-0165 I I Mr. Jchn Rhyr." OJ.fM ("orporAt:ion 5335 Triangle Pkwy. suite 450 Norcro5u, GA 30092 CC: Jack Kilbarger REPORT CF RESULTS LOO NO: S5·!6748 Received: 05 DEC 95 Reported: 07 DEC 95 Purchagg Ordgr: 101•477 ?roject: 16817 Cherokee Oil S""°"lcd By: Client Page 4 DATE/ I L03 110 56748-1 56748 ·:l 56748-3 56748·4 56748-5 SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TlM:E SAMPLED I I CO·WS-33 CO-WS-34 CO·WS-35 CO·WS-36 CO•llS-37 PAAAMETER 56748-1 I 2,4•Dimethylphenol, ug/kg dw bis (2 ·Chloroethoxy) tr,etnane, I • ug/kg dw · 2, 4 •Ilichloror,h,.:,r,l, ug/1'9' dv · l, 2,4-Trichlorobenzene, ug/kg dw I I I I I Naphthal~ne, ug/kg dw 4-Chloroaniline, ug/kg dv Hexachlorobutadiene, ug/kg dw 4-Chloro•J-methylphGnol, ug/kg dw 2-Methylnaphthalene, ug/kg dw Hexachlorocyclopentadiene, ug/kg dw 2,4,6-Trichlorophenol, ug/k1, dw 2,4,5-Trichlorophcnol, Ui/kg dw 2·Chloronaphthalene,·ug/kg dw 2-Nitroa.~iline, ug/kg dw Dimethylphthalate, ug/kg dw Acenaphthylene, ug/kg dw 3-Nitro...,"'liline, u9/k!i:f l,lw ' Acanaphthen*, ug/kg dw .............................. ·--------- I •• I <380 <380 d80 <380 <380 <750 <380 <380 560 <380 <3.80 .._JQO <380 <1900 <380 <380 <HOO <380 56748-2 56748-3 ........ --.... ----.. ------- <400 <400 <400 <400 .-:400 r:400 <400 <400 dOO <400 <800 <800 <400 <400 <100 <100 440 <400 <400 <400 <400 <400 ... _.,oo ._400 <400 <400 <2000 <2000 <400 <400 <400 <400 <2000 <2000 <400 <400 ·-·----------------·- 12·04·95/lSCO 12·04·95/1440 12·04·95/1420 12-04 ·95/H50 ~2-04-95/J.4~0 56743-~ 56748 •5 <400 <430 <400 <430 .-:4 00 o,430 <400 <430 <400 <430 <800 <860 <400 <430 <100 <130 <400 <430 <400 c430 <400 <430 ..;4 00 .;:430 <400 <430 <2100 <2200 <400 <430 c400 c430 <2l00 <2.100 <400 c430 ---------· .. --.... --.... I LaboratoriH In S11Y11nm1h, GA • r,11,h .. He, FL • Tampa, FL• Dnrfltld S.ach, FL • Mob/I&. AL • New Orl&ana. LA I •• I I I I I I I CEC-07-1995 :7:36 FROM SAVeNNAH LABS TO . 9: 7043911147 P.05 SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC . 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John R.'iyne OHM: Co,:poration 5335 Triangle Pkwy. Suite 450 Norcrosa, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS LOG NO: Reeeived: Reporttd: s,-55748 05 DEC: 9, 07 DEC 95 P-...i;cha.se O..-dei;; l0lH77 Projeet: 16817 Cherokee Oil Sampled My: ~lient DAT!l/ LCG ~0 56743·1 56749·2 56746-3 56749·4 56743-5 SAMPLE DESCRI;T!ON, SOLID OR SEMISOLID SA..'lPLllS CO-WS-33 TIME SAMl'LBD 12·04·95/1500 12-04-95/lU0 12·04 ·95/1420 l2·0-4·9S/l450 12-04-95/1430 CO-WS •l4 CO-WS-35 CO-WS-36 CO-WS-37 2,4-Dinitrophenol, ug/kg dw 4•Nitrophenol, ug/kg dw $671.$-l -----·--·· <1900 <1900 56718·:l __ .. _______ <iOOO <2000 56748·3 56748·4 56748-5 ------------------------------ <2000 <:llOO <2200 <2000 <2100 <2200 I • Diben~ofuran, ug/kg-dw J,1-0initrotoluene, ug/Kg dw · 2,6-Dinitrotoluene, ug/kg dw <380 -<~60 <380 <400 <iOO <400 <400 <400 <00 ,400 ,-i.oo ,430 <400 <400 <430 I I I I I I I Diethylphthalate, ug/kg dw 4·Ch1orophenylpheny1 ether, ug/kg d" Fluo•ene, u9/k9 Uw 4•Nitroaniline, ug/kg dw 4,6•Dinitro•2•methylphenol, ug/kg dw N-Nitrosodiphenylarnine/Diph enylamine, ug/kg d" 4-B~omophenyl phenyl ether, ug/kg dw Hexachlorober.:ene, ug/k9 dw Pen~achlorophenol, ug/kg dw ~henantru:ene, ug/~g dw Anthraeene, ug/kg dw ·-·····------·· ...................... .. <380 <400 <380 <400 <360 <400 <1900 <2000 <1900 <2000 <380 <400 <380 <400 <380 <400 <1900 <2COO 890 <400 <380 <400 ---------· ---------- c40C <400 <430 <400 <400 <430 <400 <400 <430 <2000 <2100 <2200 <2000 <2100 <2200 <400 <400 <430 <400 <40il <430 <400 <400 <430 <2000 <2100 <2200 <400 <400 <no <400 <400 <430 ------------------------------ L.abof'ltorfes In Savannah, GA • Ta//ahas:s:ott, FL • T11mp11, FL• Deorfl•ld B••ch, FL • Mobll•. Al • N•w Orl••n•, LA I •• I I I I I I I •• I I I I I I CEC-07-1995 :7:J_? FROM SAVR-WH LABS SL SAVANNAH LABORATORIES & !NV/RONMENTAL SERVICES, INC. TO 9:704391114? p .1?6 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John Rhyne OHM C'crporation 5335 Triari9le Pkwy. Suite iSO Ncrcro5s, GA 30092 CC: Jack Kilbarger REPORT OF REStT.LTS LOG NO: S5-56748 Raceived: 05 DEC 95 Reported: 07 DE: 95 Purchaao Crdar: ioi,477 Project: 16817 Derokee 0:1 ~<=pled Dy: Client Pag~ 6 DATE/ LOG NO. 56748-l 56748-2 56748-3 56748-4 ,eHa-5 SAMi'LE DESCRIPTION, SOLID ~R SEMISOLID SJ..'!J>LES co-ws-n TIME SAMl'U::, 12-04-95/1500 12-04-95/lH0 12-04-95/1420 12-04-95/1450 l2·0,·95/l4J0 CO•WS-34 CO·IIS-35 CO-WS-36 CO-WS-37 PARAMETE;>. 5674R·l Di-n-butyl?hthalate, ug/kg dw <380 ,·1uoranthene, ug/Kg dw 820 Pyrene, ug/kg dw 600 llutylh<>n>.ylphth,_1,.t<>, u;:;/k!J dw ~30 3,3'-Dichlorobenzidine, ug/kg dw <750 Beru:o(a)a.nthracene, ug/kg dw <380 bis(2-Ethylhexyl)phthalate, 5600 ug/k.g dw Ch:r:y~ono, •~g/J-.g dw 3 9 0 Di•n'octylphthalate, ug/kg dw <380 aeozo (b) fl•Joranthene, ug/k9' dw s10 Benzo(k)fluoranthone, ug/kg dw <380 Benzo(a)pyrone, ug/k.g dw <380 Indeno(l,2,3-cd)pyrene, ug/kg aw ,380 Dibenzo(a,h)a.nthracene, ug/kg dw <380. Benzo(g,h,i)pexylene, ug/kg dw <380 Carbasole, U9'/kg dw <380 Sun:ogate -Phenol d5 92 t Sur~ogate,-2-~luu•vphenol Surrogate 2,4,6-Tribromophenol Surrogate -Nitrobenzene -dS Surrogate 2-Pluorobiphenyl Surrogate Terphenyl • d14 79 105 74 t tia.ce xx-crac,;ed Dat@e Analy~ed 1:..os.lls 12.06.95 S~74~-2 ______ ,.., __ <,00 <400 <400 <400 <800 <400 4400 <"-4.00 <400 <400 <400 <400 <400 <400 <400 <400· 77 t 6ti t 65 t 240 " 66 t 60 " 12.05,95 12.06.95 . -..... -...... - %74B-3 5,574,8-4 5-748-5 .. ----... -----.... --... -.. --.. ---. --.. <400 <400 <BO <400 <400 <430 <400 <400 <430 <400 <400 <~JO <800 <800 <860 <400 <400 <430 2300 <1700 <2200 <~00 <iOO ~430 <400 <400 <430 <400 <400 <430 "'400 <400 <430 <400 <400 <430 <400 <400 <430 <400 <400 <430 <400 <400 <430 <400 <400 <430 75 t 66 t 77 t ~~ t ,s t 51 t 56 t 44 t 32 t ~n " 56 t 54 • 78 t 72 t 64 ' 58 t 52 t 45 % 12.05.95 12,05.ll5 12.05,95 12.06.95 12.06.95 12.06.95 ----------.... -. ----.. . ----.... ~ --• .• I LaboratorlH In Sev,nn11h, GA • T11//ehnue, FL • Tampa, FL • Oetrfltld BNCh. FL • Mob/ft, AL • New Or/e,nt, LA I cEC-07-1995 :?:JS FROM SAIJR--INAH LABS TO 9: 70<lJ911147 P.07 SL SAVANNAH LABORATORIES & l!NVIRONM~NTAL S~VIC~, INC . I •• I 5102 LaRoche Avenue • Savannah. GA 31404 • (9 12) 354-7858 • F~x (ll1::>) ~!'i?-0165 I I Mr. John Rhyna OHM Corporation 5335 Trianile Pk..,./. Suitt 4S0 Norcro~~. GA J0093 CC: Jack Kilbarger I.<lG NO: S5-5674Q RecoivQd: 05 DAC 95 R~portad: 07 DEC 95 Furcha~e Ord~r: 1016477 Project: 16817 Cherokee Oil San,pled By: Client I REPORT OP RESU:t.TS DATE/ LCG NO S.AM.PLE DBSCRIPTION, SOLID OR SEMISOLID SAMl'L!S TIMB SAMPLED I 55748·1 CO-WS-33 SC7i0-~ CO-WS-34 56748-3 CO-WS-35 I 56748-4 CO-WS-36 56748•5 CO-WS-37 I p AAA. '1K TE R. Arsenic • Arsenic (6010), mg/kg dw I . Date Analyzed oarium (&010) I I I I I I Ba.r:.u.'!\ (60:0), mg/ks dW D.:lt".~ An~lyi.9cl Ca::!m:. urn ( 6 0 l O) Cad!:lium (6010), mg/kg dw Date Analyzed Chromium (6010) Chromium (,010), mg/~g dv Date Analy•ed Mercury Merc:ur-1 (7470/7471), mg/kg dw Datt Analysed -Siilvor (COlO} Silver (6010), mg/kg d·• Date Analysed Selenium Selenium (6010), mg/kg dw t>a.te Allaly , .. <J ------······· ... --.--................ . I . • I 12-04-~S/1500 12•04·95/J.HO 12·04-95/14:lO 12·04·95/HSO 12-04-95/1430 5614~-l 5~74a-2 56748·3 56748•4 56743·5 15 12.06.95 l. l 12.06.95 Sl 12.06.95 0.1: 13.06.95 <1.1 12,06.95 18 17 12.06.95 U .06 .95 97 110 12.00.95 l~.OG.95 <0.60 <0.60 12.06.9S 12.06.95 4G Je 12.05.95 12.06.95 0.11 0.071 12.06.95 12.06.95 <l.2 <1.2 12,06.9S 12.06.95. <12 <12 l~.U~.95 12.06.95 n 12.06.95 130 1a.o •. n <0.61 12.06.95 H 12.06.95 0.077 12.06.95 <1.2 12.06.95 <:H*F65 12.06.95 17 12.06.95 77 12.0G.95 <0.7S 12.06.95 2, 12.06.95 0,091 12.06.95 <l.S 12.06.95 <30•F6s l~.06.95 I ulx,r,torioa In Sorenneh, OA • T11//11honn, f'L • T•mp•, l'L • DefKfleld l!Jeacl'I, l'L • Mo/Jlle, AL • New Orleans, LA I •• I I I I I I I i:EC-07-1995 : 7: 39 FROM SAV~ LABS TO 9: 7043911147 P.00 SL SAVANNAH LABORATORIES & fNVIRONlll!HTAL SERVICES, INC . 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354•7858 • Fax (912) 352-0165 Mr. John Rhyne = Corpor:i.tJ.on 5335 Trianile Pkwy. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS LOG NO: SS-56748 Receiv•d: 05 DEC 95 Reported: 07 DEC 95 Project: 16817 Cherokee Oil SampleQ Hy: Clienc DATE/ LOG NO 56748-1 56748•2 56748-3 56748-4 ~6-t4ij•5 SAMPLE DESCRIPT!ON, SOLID OR SEMISOLID SAMPLES CO·WS-33 TIME SAMPLED 12 • 04 ·95/1500 12-0,-95/lUO 12·04•95/1420 12 • 04 ·95/1450 12·04-95/1430 CO-WS-34 CO-WS•3S CO•WS•36 CO·WS-37 SG748·l 56718-J 5G718-1 SG71S·S --------------.......... ---------.. Lead (6010) Lead [6010), mg/kg dw 110 140 75 62 150 I • Date Analyzed Porc•nt Solidc (lG0.3), I 12.06,95 12.06.95 12.06.95 12.06.95 12.06.95 00 83 83 82 57 --------.. ·--·---------------- I I I I I I •• I ----------. ... -.... --.. -.. ---·--·---................ .... -.. -......... I ~boratorle1 In S11v1nn1h, QA • T11/ah11u ... FL • Tamp11, FL • DHrll-1d it.1teh, l'L • Moh/I,., 4L • N"w o,t.,.n11, LA [f:C-07-1995 : 7: 39 FROM SRlJR-lflAH LABS TO 917043911147 P.09 I s L SAVANNAH LABORATORIES & fNVIRONM~NTAL SliRVICl.f:, INC . •• I 5102 LaRoche Avenue• Savannah, G~. 31404 • (912) 354-7858 • Fax (912) 352-0165 I I Mr. Jol-.n Rhyne OHM Cory0.c.: ct 1,.l VIJ 5335 Triangle Pkwy. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger P..:POP.T 0>" RESULTS LOG NO: S5·56748 Receiv9d: 05 Die 95 Reported: 07 DEC 95 »urchase order: 1016477 Project: :6817 Cherokee Oil Sampled By:, Client Page 9 DATE/ I LCXJ NO SA!-'.?LE DSSCRI?TION, SOLID OR SEMISOLID SAMPLES TIME SAMP!,EO I I I PARAMETER Volatiles by GC/MS (8240) Chlorometha.ne, ug/kg d·~ sromorncth.1ne 1 ug/kg dv Vinyl chloride, ug/kg dw C~loroethane, ug/kg dw •• I Methylene chloride IDich:oromethar.e), ug/kg dw Acetone, ug/kg dw C~rbor. disul!lUK, vH/~g dw l,l•Dichloroethene, ug/kg dw l,1-Dichloroethane, ug/kg cw Cis/Tra.ns•c,2-Dichloroethene, ug/kg dw Chloroform, ug/kg dw I I I I I i, :l-Dichlorocch.:l.nc., ug/kg dw 2·Buta.none (MEK), 'ug/kg dw l,l,l•Trichloro<>thiu:"', ug/kg dw Carbor. tetrachloride, ug/kg dw Bromodichlorcmethane, ug/kg dw 1,1,2,2-Tetraehloroethane, ug/kg dw 1,2-Diehloropropane, ug/kg dw trans-l,J-Dichlorepr0Pene, ug/k~ dw Trichloroethene, ug/kg dw Dibro:r.ochloromethane, ug/kg a·~ l,l,2-Trichloroethane, ug/kg dw Benzene, ug/kg dw •• I 56748-6 <1700 c:.1700 <l 700 <1700 <840 <8400 <840 <840 <840 <840 <840 <840 20000 \_/- "=94 0 <840 <840 <840 <840 <840 <840 <840 <840 <840 I Laboratori•• In Satv,innah, GA • Ta//ah,uaee, FL • Tampa, FL • Oaarlfald /)each, FL • Mob/le, AL • New Orleans, LA J:EC-07-1995 l7: 48 FROM SAVl'NNAH LABS TD 9, 7043911147 P. 10 I s L SAVANNAH LABORATORIES ·& l!NVIRONMl!NTAL SERVICES, INC . •• I 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354•7858 • Fax (912) 352-0165 I I Mr. John Rhyne OHM Cnrri(:rr~ t \ or. 5335 Triangle Pkwy. Suite ,so Norcross, GA 3009, CC: Jack Kilbarger REPORT OF RESOLTS LOG NO: Received: Report•d: S5·55748 05 DEC 95 07 DEC 95 ~urch~3C Order: 1015~77 Project: 16817 Cherokee Oil Sampl~<l By; Cll,.HI. Pac;e 10 DATE/ I LOG NO SAMPLE DESCRlPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED I 56748-6 CO•WS•38 12·04·95/1530 .. ,. .. ______ ,._ .......... __ .................................................... ________ .,,. ................................... .. PARAMETER I I 1• I I I I I I cis-l., J-Oichloi:opL:Vp1:mld, ug/kg clw Bromofor:n, ug/kg dw 2-Hexancne, ug/kg dw 4-Methyl-2-pentanone IMIBK), ug/kg dw Tetrachloroethene, ug/kg dw Toluene, ug/kg dw Chloroben7ene, ug/kg dw Ethylben~"n", t1r;;/,g dv Styrene, ug/kg dw Xylenes, ug/kg dw Surrogate Toluene•d8 Surrogate• 4-Bro:nofluorobenzene S\.l~rogato • l,~•Diohlorocth.:2.nc d4 Oate Analyzed •• I 56748-6 <~-10 <840 <9400 <8400 <840 7400 <840 2800 <840 1700 109 'I' 109. t 1J3 ~ 12.06.95 ------.. ------------- I Laboratorlot In Savannah, GA • T1//1haUff, FL • Tampa, FL • Deerfield Bffeh, FL • Mobile, AL • Now Orleans. LA I •• I I I I I I I i:£C -07-1 935 , 7: 40 FROM SAVeN-IAH LABS SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICl!S. INC . TO 917043911147 P.11 5102 LaRoche Avenue• Savannah. GA 31404 • (9~2) 354-785a • Fax (912) 352-0165 Mr. John Rhyne OHM Corpor:i.tion 5335 Tri&ngle Pk·,y. Suite 450 Norcross, GA 30092 CC: Jack K.ilbarger REPORT OF RESULTS LOG ~O: SS-56748 Receivgd: 05 DEC 95 Reported: 07 DEC 35 Pui·c.:h,rne Order: 10164 77 ;reject: 16817 Cherokee Oil Sampled ay: Client DATE/ LOO NO SAMPLE DESCRIPTION, SOLID OR SElilSOLID SAMPLES TIME SAMPLED 56748·6 CO•WS•38 P AAJi.'il!TiR ·,-ci.. ,ernivolatil<!s (8270) Phenol, ·..tg/kg d•M hiA(,-8hloroethyl)ethor, ug/kg dw 2-Chlcrophenol, ug/kg dw 1,3-Dichlorobenzene, ug/kg dw l2·04·95/l530 5674$-6 <89CO •• l,4-Dichlorobenzene, ug/kg dw l,2-Dicillorobenzene, ug/kg dw 2-Mo~hylphenol (o-crc3ol), ug/kg dY 2,2'-Cxybis(l-Chlorcpropane) ,<8~00 <8900 <8900 <8300 <8900 <89 co <8900 I I I I I I (bis•2•c.~loroisoprcpyl ether), ug/kg dw 3•Metbylphenol/t·Methylphenol(m&p•cresol), N•Nitroso-di•n·propylamine, ug/kg dw Hexaciilor=th<ine, ug/kg dw Nitrobenzene, ug/kg dw ~sophorone, ug/k~ dw ~-Nitrophenol, ug/kg dw 2,4·Dime:hylphenol, ug/kg dw bis(2·Chloroe~noxy)methane, ug/Xg aw 2,4-Dichlorophenol, ug/kg dw l.2,4-TrichlorobenzanA, ug/kg dw Naphthalen~, ug/kg dw 4-Chloroa.niline, ug/kg dw Hexach10::ooutadiene, ug/kg dw 4•Chloro·3•methylphenol, ug/kg dw ................... _.,.., ........... ,. ___ ............ . •• I ug/kg dw <8900 <8300 <a9oo <8900 <8900 <8900 <8300 <8.900 <8900 ~8900 <8900 <18000 <8900 <8900 I laboratoriH In S•v•nr1•h, GA • T•llahauGa, FL • T11mptt, Ft • O.•rllold &ach, FL • Mob//•, AL • New Orleans, LA ~Rf CEC-07-1995 :7:~l FROM SAVJ'.l,NAH LABS TO 9'. 7043911147 P.12 I SL SAVANNAH LABORATORIES & l!NVl"ONMt!NTAL /Jt!/11.VICl:5, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354,7A.~R • Fa• (912) 352-0165 Ml:'. John Rhyne OHM Corporation 5335 Triangle Pk.,,./. suite 450 Norerosc, GJ\. 20092 CC: Jack Kilbarger REPORT OF RESULTS LOG NO: 95-56748 Receivod, 05 DSC S5 Reported: 07 DEC 95 Purcilase Order: 1016477 Project: 16817 Cherokee Oil Sampled By: Client Paga 12 DATE/ I I I I LCG NO SAM9LE DESCR!?TION, SOLID OR SiiMISOLID SAMPLES TI:-m SAMPLED 56'740·6 CO-WS-38 12-04-35/1530 I I PMAME1'5R --•••r•••-•-····•••••••-•----.............. . 2-Methylnaphthalene, ug/kg dw Hexachlorocyclopentadiene, ug/kg dw :l,4,6·-rrichloropnenol, ug/kg dw 2,4,5-Trichlorophenol, ug/kg dw 2 -C~lt"')rcnr1ph th~ lg,nq, u!j/k:g dw 2·Nitroanilir.e, ug/kg dw I • Di~athylphthalate, ug/kg dw Acer.aphthylene, ug/kg dw 3-Nitroaniline, ug/kg dw I I I I I I J>.cg~aph~hene, vg/kg dw 2,4-Dinitrophenol, ug/kg dw 4-NitropheDol, ug/ks dw Dibenzofuran, ug/kg dw 2,4-Dicitrotcluene, u9/kg dw 2,~•Dinit~ot0luene, ug/kg Cw Diethylphthalata, ug/kg dw 4·ChlorophenylpheDy1 et:her, ug/kg dw Fluorene, ug/kg dw 4-Nitroani:ine, ug/kg dw 4, 6-D.i.uit:c:i:;,•2•methylpht:nol, ug/X.g Q.w N•Nitrcsod~phenylamine/Oiphenyla.~ine, ug/kg dw 4·llromophenyl i;,heDyl ether. vq/kg dw Hexac:r.lorobenzene, ug/kg dw Pentachlorophenol, ug/kg dw ---------------------------------~--------------- I • •• 56748-6 10000 <3900 <9900 <8900 <8900 <4SOOO <8900 <8900 <45000 .;8?00 <4 6000 <46000 <8900 <8900 <e,oo 18000 <8900 <8900 <46000 <ibUCO <8900 <~9CO <8900 <46000 I Laoo,.10,;.,,, in s, .. ann11h, GA • Tal/11h1tSSH, FL. • T1mp11, FL • Dff/1/Q/CI ao,cn, FL • Mobilt, AL • /WW Ortun,, L.A I •• I I I I I I I 1• I I I I I I CEC-07-1995 : c: c2 FROM SAV!flNAH LABS ·s L SAVANNAH LABORATORIES & fNVtRONMl!NTAL SERVICES, INC . TO 9: 7043911147 P.13 5102 L.aRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John R.'1.yne (;HM CnrporP.t!.on 5335 Triangle Pkwy. Suite 450 Norcross, GA 30092 CC: Jack Kilbarger REPORT OF RESULTS LOG NO: SS-56748 Received: 05 DEC 55 Reported: 07 DEC 95 Purch~oc Order, iOi6477 Project: 16817 Cherokee Oil Sampled Dy: Cll,;,nl Pa.;re 13 DA'rE/ LOG NO SAMPLE DESCRI?TlON, SOLID OR SEMISOLID SAMPLES TIME SAMPLED S6748-6 CO·WS-38 12·04·SS/l530 P.P.!JJU1ETER 56748-6 Pl1~u(l.!1thx-e;-1e, ug/kg-d.w Anthracene, u9/k9 dw Di·n•butylphthalate, ug/kg dw Fluoranthene, ug/kg dw Pyrene, ug/kg dw aucylbenzylphthalate, ug/kg dw 3,3'-Dic.hlo~benzidine, ug/kg dw BAnzn {;i) Ar'lthr~cen~, w:r/kg d.w bis(2·Bthylhexyl)phthalate, ug/kg dw Chrysene, ug/kg dw Di-n-octylphthalate, ug/~g dw Be:uo lb) fluoranthene, ug/kg dw Ben:o(k}£luor~thc:ne, 1,.1g/kg dw Benzola)py:-ene, ug/kg dw Indeno(l,2,3•cd)pyrene, ug/kg dw Dibenzo(a,h)anthracene, ug/kg dw Benzo(g,h,i)peryl•n•, ug/kg dw Carba&ole, ug/kg dw Surrogata Phenol dS Sur=ogate 2·Fluoror,henol Sur~ogate 2,4,5-Trib=ophenol Sur=ogate Nitrobenzene • dS Su<cu~dl~ z-~luorobiphcnyl Sur=osate Terphenyl • d14 Date Extract9d Date Analyzed <8900 d900 3,000 <8900 <2900 93000 <18000 <Q900 120000 <8900 <8900 <8900 ,e,oo <8900 <8900 <8900 <8900 <8'00 •F33 •F33 •F33 •F33 •F~~ •F33 l~.0<;.~<; 12.07,95 •• I L.boratorlH In Sa,annah, GA • Tal/ahlllSH, FL • Tampa, FL • Dffffrl/eld Beach, FL • Mob/Ir,, AL • Nr,w Orleans, LA I I •• I I I rEC-07·-1995 l 7: 42 FROM SAVfNNAH LABS TO 917043911147 P.14 SL SAVANNAH LABORATORIES ii ENVIRONMl!NTAL 31!/f.V/C/!3, INC . 5102 Wciche Avenue• Savannah. GA 31404 • (912) 354-7858 • F:ix (91'.) 352-0165 Mr. John Rhyne OHM Corporation 5335 Triangle Pkwy. Suite 450 Norcrogs, Ch i009~ CC: Jack Kilbarger REPORT OF RXS1'1il"S LCXl NO: S5•5674i Rcooived, OS ~EC 95 Reported: 07 DEC 95 Purchase Order: 1016477 Project: l68l7 Cherokee Oil Sampl~d By: Client Pa51e 14 DATE/ I LCG NO SAMPLE DESCRIPTION, SCLIO OR SEMISOLID SIIMPLES Til\!l! SAMPLED I 56748•6 CO-WS·3S PARAMETER 56748-6 I I •• I I I I I I Percent Solids (160,3), t •• I 74 i2-04-95/1530 I Ul~retorfN In Sa,11nn11h, GA • Ta/lafla1ser,; fL • Tampl, fL •· DHrtle/d Soacfl, FL • Mob/It, AL • New Or/11n1, L.A I •• I I I I I I I •• I I I I I I CEC-07-1 995 17: 4] FROM SAVl'N'IRH LABS TO 9,704]5111~7 P.15 SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC . 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John Rhyne OIIM Corporation 5335 Triangle Pk"')'. Suite 450 _Norcross, GA 30092 LOG ~O: S5·56748 Recoived: 05 DEC 95 Rgpor~od: 07 02C 95 P1.1:rchaae Order: 10U477 CC: Jack Kilbarger Project: 16817 Cherokee Oil ~ampled By: ~l:ent REPORT OF RESULTS LCG NO SAMPLE DESCRI?TION, QC REPORT FOR SOLID/SEMISOLID ---------------------........... __________________ ,__., _____ ., __ ,.,. ...... ---------------------- M~thod Blank S6748·7 56748·8 56748·9 Lah C<>nt.rnl 8t~nd,,.rd (LCS) t Recovery/Dupli~ata LCS \-RPO PARAMETER Vol~tileg by CC/MS (8240) Chloromethane, ug/kg dw Bromo:uethane, ug/kg dw vinyl chloride, ug/kg dw Chlcroethane, ug/kg dw Methylene chloride (Cichlororneth.u::e), ug/kg dw Acetor.e, ug/kg dw Car~n disulfide, ug/kg dw l,l·Dichloroethene, ug/kg dw l,1-Dichloroethane, ug/kg dw C:iB/Trans · i, 2-Dic:hlc.,~i:,sthene, ug/kg cl.w Chloroform, ug/kg dw l,2·Dichloroethane, ug/kg dw 2•Butanone (MEK), ug/kg dw l,l,l-Trichloroathar.e, ug/kg dw carbon cecrac:hloride, ug/kg dw Bromodichloromethan•, ug/kg dw l.l.2,2·Tetrachloroathanf!, ug/kg rlw l,2-0ichloropropane, ug/kg dw trans-1,3-Dichloropropene, ug/kg dw ,Trich.oroetnene, ug/kg dv Oibromoc.~loromathane, ug/kg dw 56748·7 <10 <10 <10 <10 c;.5.0 <25 <5.0 <5.0 <5 .o <5.0 <5.0 <5.0 <2S <5.0 <5 .0 <5,0 ,s .0 <5.0 <5.0 <5.0 <5.0 -----------·---------· 56748·8 S6748 ·9 134/136 t 1 \- 124/120 t •• I I L.aboratorlH in S"vannah, GA • Ta//aha1Na, FL • Tampa, FL • O.erflald 8e110h, FL • Mob/lo, AL • Now Orl•"1t, LA I •• i I I I I I I I 1• I I I I I I CEC-07-1995 1?:44 FRCl'1 SRVfN'<AH LABS TO 917043911147 P. 16 SL SAVANNAH LABORATORIES & INVIAONUIINTAL SliRVIC", INC . 5102 LaRoc/1e Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0166 LOO NO Mr. John Rhyn" OHM Cuz.yQ:ra~ion 5335 .Triang-lt Pkwy. Suite 450 NorcrOS$, GA 30092 CC: Jack Kilbarger LOG iqo, S5·!6748 Received: OS OiC 95 Reported: 07 DBC 95 Purchase Order: 1016477 Project: 16817 Cherokee Oil Srunpled By: Cl-ient Sk'!PLE DESCRIPTION, QC REPOR~ FOR SOLIO/SE~ISOLID ............. ------········ .. --------·····-··· ................................................... .. 56748-7 56748-8 56748-9 Method Blank Lab Cont~ol Se:>n&rd (LCS) t Re~ovo:i:y/Ouplieate LCS \' Fi.PD PAAA.'!ETER 56748-7 1 1 1,~ Trichloroethaiie, u~/kg dw Benzene, ug/kg dw cis·l,3-Dichloroproper.e, ug/kg dw Bromofo:nn, ug/kg dw ••Hexanone, ug/kg dw 4-McLh,rl·2•;,,.utanone IMIBIC), ug/kg dw Tetra.chloroethene, ug/kg dw Toluene, ug/kg dw Chlorobenzene, ug/kg cw Ethylber.zene, ug/kg dw ·styrene, ug /kg clw Xylenes, ug/kg dw Surrog;it:/1! .. To1,,1,,.n9-d8 Surrogate• 4•Brano!l~oroi,.nzena Surrogate.-l,2·Dichloroethane•d4 Date Analyzed <!'-0 <S.O <5,0 <5.0 <2!:i <i~ <5.0 <'i.O <5.0 <S.0 <5.0 <5.0 ;; t 104 t 94 t 12.06.95 56748-8 56748·9 128/l28 \' 0 t D0/1?.6 t S t l3,/130 t 2 t a.;a, t 100/96 t 92/94 t 12.04.95 •• I I Uborator/et In Sav:onn;oh, QA • T;,/1;,haoHe, FL • Tl!mpa, FL • C>oerl/eld Beoolt, FL • Mob/le, AL • New Or/Nne, LA r:EC -07-1 995 l7: 44 FROM SAV~NAH LABS TO 9;7043911147. P.17 ·s L SAVANNAH LABORATORIES & ~NVIRONMfNTAL SERVICES, INC . I •• I 5102 LaRoche AvMue •Savannah.GA 31404 • (912) 354-7858 • Fax (912) 352-0165 I Mr. John Rhyne OHM Cox;,oro.tion 5335 Trianglt Pkwy. Suite ,so Norcross, GA 30092 LOG NO: S5·56748 Receivtd: 05 DSC 95 Reportod: 07 Die 95 Purchase o.,·ae.c: 101.5..i 77 I CC: Jack Kilbarger Project: l6Bl7 Cherokeo Oil Sampled ay: Clie~~ I I I I LOG NO S6748•7 56748-8 56746-9 REPORT OF RES!JLTS SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID -. -.... ------.......... ---.. ----------........ · ... ---..... -.... -.. -Method alank Lah Control Standard (LC:S) t R.,r,c,v,0ry/nup1; c~t" LCS t RPD PAR.A.'IETl,R 56748·7 .... ---.. -.. ----. ----.......... -----. ---... --.... --...... ---- - ---------.. TC".T, $','lmfvcl~t.iles, (B270) Phe~ol, ug/kg dw <330 bis(2·Chloroethyl)ether, ug/kg dw <330 2-Cllorophenol, ug/kg dw <330 •• I 1,3•Dichlcrobenzene, ug/kg dw <330 1,4-0ichlorobenaone, ug/kg dw ~330 l,2-Dichlorobenzene, ug/kg dw <330 2-Methylphenol (o•crei;ol), ug/kg dw <330 2,2'-0xybis(l·Chloroprcpane) c330 (bis-2-chlcroisopropyl ether), ug/kg dw I I I I I J -Methylphenol/4 ·Methylphenol (,n&p · """~vl) , 1,1!,'/lc!,' r.lw <33 0 N•Nitroso-di-n-propylamine, ug/kg dw <330 Hexachloroethane, ug/kg dw <330 Nitrobenzene, ug/kg dw <330 Isophorone, ·ug/kg dw <330 2•NlL.rvyb.,w.>l, ug/1<9" dlr dJO 2,4-Dimethylphenol, ug/kg dw <330 bis(2-Chloroethc:,ey)~ethane, ug/kg dw ,~10 2,4-Dichlorophenol, ug/kg dw <330 l,2,4·Trichlorobenzene, ug/kg dw <330 Naphthalene, ug/kg dw <330 4-Chlorcaniline, ug/kg dw <660 I . • I '• Page 17 56748-8 56748·9 67/76 t 12 % 67/73 t 8 t 70/70 \ 0 \ 70/76 t 8 % 65/70 % 7 % Laboratories In Savannah, GA • Tlt//11h11ssH, FL • T•mpa. FL • Doorll•ld Bo,,ch, FL • Moblt., AL • N•w Or/oant, LA I I •• I I I I I I I SA\i"'~IRH L.PBS SL SAVANNAH LABORATORIES & fNVIRONltf!NTAL SERVICES, INC . 9, 7043911147 P, 18 5102 LaRocht Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LCC NO 5674,-7 56746-$ 56749-9 Mr. John_ R."lyne CHM Corpor~t:inn 5335 Triangle ~kwy. Suite 450 Norcross, GA 30092 LCG NO: S5·56748 Received: 05 DSC 95 Reported: 07 OBC 95 PurchagG Ordor, 101G477 CC: Jack Kilbarger Project: 16817 Cherokee Oil So.mpled ey: Client REPORT Ol' RESULTS: SAM?Li DESCRI?TION, QC REPORT l'OR SOLID/SEMISOLID Method Blank Lab Control Standard (LCS) ~ Recove,:y/OuPlicate LCS \-RPD Page lS ........................................ -------------·------------·-----------·---------------.... P;>.RAMETE1' 56748•7 S6748•8 S6748·9 8 ' •• I Hexachlorobutadiene, ug/kg dw 4-C.oloro-3-methylphencl, ug/kg dw 2-Methylnaphthalene, ug/kg dw Mexachlorocyclopentadiene, ug/kg ctw 2,4,6·Trichlorophenol, ug/kg dw 2,4,5-Trichloror,h~nnl, \lg/kg dw 2-Chloronaphthalene, ug/kg dw 2-Nitroaniline, ug/kg dw Dcmethylphthalate, ug/kg dw Acenaphthyler.e, ug/kg dw 3•Nitroanilir.9, ug/Y.g dw Acenaphthene, ug/kg dw 2,4-Dinitrophenol, ug/kg dw 4-NitrophGnol, ug/kg dw OibenzofurM, ug/kg dw ~,4-0initrotol~ene, ug/kg dw 2,6-Dinitrotoluene, ug/kg dw Oie~hylphthalate, ug/kg dw 4·Chlorophenylphenyl Qther, ug/kg dw Fluortne, ug/kg dw d30 <330 <330 <330 <330 -.no <330 <1700 <330 <330 sl.700 <330 <1700 <1700 <330 I I I I •-Nitroo.niline, ~9/h9 dw 4,6-0initro-_2-methylphanol, ug/kg dw I •• I <330 <llO <330 <330 <330 <1700 <1700 70/76 \- 73/7~ t 82/&8' ----... --... 8 ' 7 ' Liibor,torl•• In s,v,nnah, GA • T11/1hnno, FL • Tampa, Fl. • O..rll.id s .. ch, Fl • Mob/le, AL • New Or/NnS, LA I I •• I I I I I I I •• I I I I I I I r:EC-07-1995 17:45 FROM SAUA'INAH LABS SL SAVANNAH LABORATORIES & tiNVIRONMliNTAI. CERVICQ; INC . TO • 9,7043911147 P.19 5102 l.4Roche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John Rhyne OHM C:oq,oration 5335 Tri-.rl!,le Pkwy. Suita 450 Norcross, GA 30092 LOO NO: S5-567i8 Received: os o~c 9s Reported: 07 DEC 95 Purchase oraer: lOl,477 CC: Jacl< ~ilbarger Project: 16817 Cherokee Oil Sampled By: Client Rli:PORT O, RE~ULTS :LOG NO se;4a-1 5'718-8 5€748·9 SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID Method Blar.k Lo.l:> Control Cto.ndard {LCS) ~ Recovery/r,,,,plicate LCS t RPO PARk'!ETER N-Ni tro~o-diphenylNnine/D.i.pl..:u::uyld.!ttiu1;1 1 ;,ig /kg d.w 4 • Bromophe:1yl pheny: ethe,:-, ug/kg d,.. Hexachlorobenzene, uq/kq dw Pentachlorophenol, ug/kg dw Phenanthi:-ene, ug/kg dw Arithi;-acene, ug/k9 dw Di-n•butylphthalate, ug/kg dw Fluoranthe:1e, u~/kg dw Pyrene, ug/kg dw _Butylbenzylphthalate, ug/kg dw ,,,:•oicn1oro0enzidine, ug/kg dw Benzo{a)anthracene, ug/kg dw bis(2·E~hylh&xyl)phthal~te, ug/~g dw Chrysene, ug/kg dw r:i-n•octylphthalate, ug/l<g dw Benzo{b)!luoranthene, ug/kg dw Benao(k)!luoranthene, ug/kg dw Bcn1o{~)pyrcno, ~9/k9 dw Indeno{l,2,3•cd)pyrene, ug/kg d~ Diben,o(a,h)anthracene, ug/kg dw ien,o(g,h,i)perylene, ug/l<g dw Car~a:ole, ug/kg dw 56748-7 <330 <330 <330 <l 700 <330 <:l3o <330 d'lO '<330 <330 <HO <330 .no <330 <330 <330 <330 ,330 <330 <330 <330 <330 l'"gc 19 56748•8 56748-9 48/48 \-0 \- 65/65 t L.abor;,tori,u In Savannah, GA • TallahN~H, Ft. ~ Tampa, Fl. • Oeerffeld Ba.ch, Fl. • Mob/le, Al. • New OrlHn~, I.A I •• I I 1. I I I I I I I I I TO 9: 7043911147 P.20 SL SAVANNAH LABORATORIES & i.NVIRONfrlliNTAL $~V/Cli$, INC • 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John Rhyne OHM Corporation 5335 Trilllgli Pkwy, Suite 450 Norcro&s, GA 30092 LCG NO: S5-56748 Received: 05 DBC 95 Reported: 07 DiC 95 Purchase oroer: 1016477 CC: Jack Kilbarger Project: 16817 Cherokee Oil Sampled By: Clienc UX3 NO SAMPLB DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID 56748•7 Method Blank 5~748-8 Lah Co~trol St:u,c!a,.rd (LCS) ~ na~overy/Duplicate 56748-9 LCS t RPO PAAAMBTER 56748•7 £~rro9<1te Phenol d:; Surrogate 2-Fluorophenol Surrogate 2,4,6-Tribromophenol Surrogate Nitrobencene • dS Surrogate 2-?luorobiphtnyl -'"'-"·"·'\l"tv Terphenyl • dl4 Date Extracted Date Analyiac:1 Ar.enic Arsenic (6010), mg/kg c:lw i.>at:e Analy;go Barium (6010) Barium (,010), mg/kg dw Date Malyzed Cadmium (6010) Cai;lmium (6010), mg/kg dw Date Analyzed Chromi\ml (iOlO) Chromium (6010), mg/kg dv Date Analyzed Me~cury Mercury (7470/7471), mg/kg dw 0'10C An;ilyHd --·•····-·-------•· ................ ------··-- ---------- 82 t 73 t 85 " 70 t 76 t 7U " 12.05.95 J?..06.95 <10 12,06.95 <l.. 0 12.06,95 <0.!0 12.06.95 <1.0 12.06.95 <0.010 1~.06.'5 -------------------- 56748·8 55748 ·9 ---------- 73/73 t 70/73 t 82/85 t 65/70 t 70/76 t 7U/7~ t 12.05.95 1, .06.9!' 103/99 t LO t 12.06.95 96/9J t J.~ t 12.06.95 !Ol/98 t 3. 0 t 12.06.9S 99/% t 3.l t !2.06.95 96/102 t 6.1 t 12.os.,s -----·--·--..... -.... -.. 1. I I L11boratorfN In ,11v11nn11h, CA • T11//M:,etJce, FL • Tempe, FL • Daerllald Saech, FL • Mobila, AL • Naw Orlaarra, LA I •• I I I I I I I I I I I I I CE,:-07-1 595 :7: ,l? FROM SAVf'.l,IHAH LABS •s L SAVANNAH LABORATORIES & t.NVIRONM!HTAL $.RV/Cl,$, INC, TD 9: 7043911147 P.21 5102 LaRoct;e Avenue • Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. John Rhyn• OMM Cv::r.1,,1u:r;·,tion SJJS Tria~gle Pkwy. ~uit• 450 Norcros~. GA 3009, T,()G NO'. Received: Reported: s~-,~1•~ OS Di:C 95 07 DEC 95 c~-Jack Kilbarger Project: 16817 Chercl<.ee Oil Sampled By: Clie~t PJ!PORT OF PESULTS I.QG NO SAMPL3 D&SCRIPTION, QC REPORT FOR SOLID/SEMISOLID Mw\.bw 111-uls 56748·7 5•748-8 56748 • 9 Lal, Control Standard (LC.S) % l\eoov,:xy/Ouplic"to LCS t RPD PARAMETBR Silver (60iO) Silver (6010), mg.lkg clv Data hlaly:ed Salen:.urn seltnium (6010), ing/kg dw Date Analyzed v .... a ,,010) Lead (6010), inci/:~c; dw Data 1'naly:ed ...... ~-----------····· ----....... Memods: E~A sw-a4b 56748•7 ·---·-----.. .. .. .. ---.... ---.... -.... -- ,1.0 12.06.95 <lO i2.06.35 <5.0 12.06.95 ----------.. -.. --. --. --...... -... - 56748•8 56748-9 -...... -----.. -.. --..... -... 99/% '" 3 . , ' 12.06.95 96/94 t 2.1 t l.2.os.,s 99/98 t l.O ' 12.06.9~ ---.. --... -.. -.. ----.... -- •F33 = Cont~ol limics ar~ eata.bli~hed only for s~riogace coocent~ation levels sp■cifiod by V.PJ>. mAt:h<><1". 111-,c ... us<> th<! sample """ dilut"d prior to analyaia, &crrogate recoveri~s are not reported. •F65 •·Elevated detection limits wen reported due to sample matrix inte;i;fei·ence whl.ci"J. L·•'-l'•d.t.vcl ttample or excract ttilution. Steven J. White, Project Mar:ag~r Q.iPt Final Pa911 Of Report •• I L,,boratorl•t /11 Sav1nn1h, QA • Ta//,haa,eo, FL • Tampa, FL • OHrll•ld B11~h, FL • Mobile, AL • New Orfe:,na, I.A ' . I TOTAL P. 21 "' ··ti:~ ,._ -:Jr><•~~l{., · 1.~ ,it!;li&:,'li'h p~, ,!'f .4ir:•;,t'-"f'~', .,.I •. ;".·"··· .. I .-:,~ ·•ffi ;:; t-.r1~?1;z;i .... ..,.: "'~;;,.-;,-!~~t'~;~,~~: ,, •• l)\ .. • ''flj'' .•• ~/,\., ;,,"",iiJt~ . J;:f ~~ -~k rc.,. ij ·:., :··);i~:'d.: ' j ~- ; ' i : (. Jone then 8. Howea Secretary Department of Enviran'Del\t, Health~ and Natural Reaourcea Willi,.. L: Neyer Director , Division of Solid llute Management Jamee A. Carter Chief Hazardous Waste Section 200 copies of this pblic doclll'le!lt were printed at a cost of S3,700 or $18.50 per copy. Revhed JDnUary 1, 1996 ·IIOOI ............. . ,II005 ••• ;: ••••••••• ,oota.,,., ........ . ,D006 •••• , ••••..••• ,0019.. •• : ••••••••• ~D020 •• :.: ••••••••• OOZt., •••••••••••• 22 •••• ! ........ . D007 •••• ! ........ . D023 ••• :: ••••••••• OOZ4.'; •• ! ........ . ~0025:; .. : ........ . "'0026.; •• ~ •.••••••• 0016.! •••••••••••• 0021:::~~ ....... .. 002&.-: .. : ........ . 0029: ... ~ .. : ..... . -••" I W,Ni:!·~········· 0012: ••••••••••••• DQJ1~:~:: ........ . DOJ2::1:;·~ ....... . DOJJ::;:·: ... : .... . 0034!~::::;.~ .... . D008~:;~;~···!·~··· 0013 •••••••••••••• IMMW~~-;:: ....... . 0014 •• : ••••• · •••.•• D035.:.:: ........ . 0036.: ........... . D037~~-.~: .. ~ ..... . DOl8~!:.;., ...... . iloto.:::.-.~ ...... . 0011.::: .. : ...... . DOJ9.: ..•......... 0015.: ••• :: •• : •••• D040.~ ••••• :: ..••• ,0041;;;:.: ....... . 0042.:::.: ....... . 0017 •••••••••••••• 0043:~ ••. ~: .•..... L' :· Table J • Maxin.JD Concentration of Contanfnanta for Toxicity 011recterl1tlc Contamfnent Arsenic ••••••••••••••••••••••••••••••••••••• Barlun •••••••••••••••••••••••••••••••••••••• Benzene ••••••••••••••••••••••••••••••••••••• tadnii.n •••••••••••••••••••••••••••••••• ~ •••• Carbon Tetrachloride ••••••••••••• : •••••••••• Ollordane ..•••••••••••••••••••••••••••••••• ; 01lorobenzene •••••••••••••••••••••• ~ ••• ~ •••• Chloroform •••••••••••••••••••••••••• ~: ••. ~ ••• O,romfun .•••••••••••••••••••••••••• ~ •••••••• o·Cresol ••••••••••••••••••••••••• ~ ;~ •• ~-: ••• a,,,Cresol •••••••• : •••••••••••• : ••••••• ; •••••• p-Cresol •••••••••••••••••••••••••••• :.~ ••••• Cresol •.•••••••••••••••••••••••••• :.:.;:.: •• 2,4-0 •••••••••• ; • : ••••••••••••••• : : • ~.:; :~ •• 1.4·01ch lorobenzeno ......• ; ••... ; ••. : .. :.::: 1,2-Di ch loroethane ................ ~ •••• ~ ~: ~: 1.l·Oichloroethylene ••••••••••• : ••••• :.: ••• 2,4-Dlni trotoluene ........ ; ... ~ ... :~ .. :.:. :: Endrin ••••.••• : •••••••••••••••••••••••• :.; •• Heptachlor (and tta epoxlde) .•..•.••.. :,:.:. Hexachlorobenzene. ~ ............. : .: ~. ;~ ~; ! ; : : . HexachlorobJtadi ene •••••••• ~ ••••• :. :· ~. ~. ~. ~ ~ Hexach loroethane .................... :;:.: ~ :-! Lead ••••••••••••• ••; ••• ;•••:•;•••••••;;•••;; Llndana •••• : •• :: •••• ; ••••••••••••••••• : ••••• Mercury ••••••••••••••••••••••••••••• : •• :.:~. Nethoxychlor ••••••••••••••••••••• ~ •••• ~.: .;. Methyl ethyl ketone •••••••••••••••• : •• : •• ; •• Ni trobenzene •••••••••••••• -•••••••••• ;. : •• ~-~. Pentachlorophenol ••••••••••• ; ••••• ; • ;; ••• : ; • Py 'd" , •· r1 ~ne·•····•••···•••····•••···••····•~··· Selen11.1n •••••••••••••••••••••••••••••••••••• Silver •••.••••••••• ~ ••••••••••• ~ •••••• :.~: •• Tetrachloroethylene ................... ~~:·· Toxaphene ••••••••••••••••••••••••••••••••••• Trichloroethylene •••••••••••••••••••••••• ~;. 2 ,4 ,5· Tr f chlorophenol .............. : .... :: ~. 2,4,6· Trf chlorophenol ••••••••••••• ! ~~ .... i; • 2.4.5·TP Silwx ........... ; ........ ,, ... ; .. Vinyl chloride.: ................. ~ •• ~~ .. ;; .. CAS N.2 7440·38·Z 7440·39·3 . 71,43·Z 7440·43·9 . 56·23·5 57·74·9. 108·90·7 ·67·66·3 . 7440·47·3 095·48·7 · 108·39·4 106·44·5 ::;;94:75:7: __ ;: 106·46·7 r • 107·06·2 . . 75·35·4·-· ·::121-14-z ·• r-~ 72-20-1 ?1 ·+., 76·44,8.,, 118·74·1 > .. 87·68·3 . :. 67-n·1 '.7439·92·1 . 58·89·9 . . 7439·97·6 r · , . n-43·5 . · 78·93·3 98·95·3 ·,: 87·86·5 , 110·86·1 '7782;49·2 7440-22·4 127·18·4 8001·35·2 ., •• 79·01·6 ', . 95·95·4 , . Yt "., 88•06·2 ~ · 93-n-1 , .; 75·01 :4 '· <J>;:,.,;.,~ I ; • .• 1· . e waste nuJter. · · . ,-·-t• ;:, ~-:-t abstracts service rud:>er. · 1.,.1 ••• • .: • . _ ion limit is greeter then the calculated regulatory level •. The Reaulatory Level (rqi/l) 5.0 100.0 0.5 1.0 0.5 . 0.03 100.0 6.0 4 5.0 4200.0 4200.0 4200.0 200.0 10.0 7.5 0.5 30.7 o. 13 ·. 0.02 30.D08 0.13 · 0.5 3.0 5.0 0.4 0.2 10.0 200.0 2.0 100.0 ' l5.0 1.0 5.0 0.7 0.5 0.5 400.0 2.0 1.0 0.2 4ffA'!'!ttiiton limit therefore becomes the regulatory level. · • ,..If ct;, at-, and p-Cresol concentretlona· camot be dtfferentl1ted,: the total cresol (0026) ~tr~tiOf'I is used. The regulatory level of total cr8aot la 200 IIV/l • . I Rule .0006 • 20 , I !, ' •• I I I I I I I ··• I I I I I I •• I I- .( ,IV ~~V\1 ,_Jo,_(_ F-~ \) /JP . f•l-t.a~-e. f'.55 -1,;. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY ~'( lttt-< ?«- REGION IV · ~--=--· / /. -RE c,,. 'r L? r b v-e_ Y--34 s COURTLAND STREET. N.E. ,£,, · <~ () ATLANTA. GEORGIA 3036s -= 1/tJ;, <'."'1T;,,~~ TV r +,{-£A i 7 -47~· tv s~ -e LNOV 1.6 1994 ~DN-C? {s'b f MEMORANDUM SUBJECT: Guidance on Residential Lead-Based Paint, Lead-Coritaminated Dust, and Lead Contaminated Soil and Revised Interim Soil Lead Guidance for CERCLA Sites and RCRA-Corrective-Actiori' Facilft~ies -. FROM: TO: . Al Hanke, Chief n~ State Programs Section Jr State Directors State Authorization Contacts RPS Unit Chiefs RCS Unit-Chiefs The following documents are enclosed for your information. • Guidance on Residential Lead-Based Paint, Lead-Contaminated Dust, and Lead Contaminated Soil • Revised Interim Soil Lead Guidance for CERCLA Sites and RCRA Corrective Action Facilities If. you have any questions, please contact Margaret Meares at (404) 347-2234 vmx 6994. Attachment I •• I I I I I I I •• I I I I I I •• I I it may well be the result of soil being tracked into the house from outside, Also, if paint is in sbund condition and soil · concentrations are low but the interior dust concentrations are high, it is possible that other sources, such as dust carried home from lead-related work, ar~ present. T~rough a systematic process of elimination, many of the sources of lead in house dust can often be determined. While a detailed discussion .on how to perform these types of assessments is outside the scope of this guidance, these issues will be •ddressed ·by certification procedures and training requirements for parties involved in lead-based-paint activities (which includes abatement, inspection and risk assessment) .currently. being developed under section 4 02 of TSCA. . . . . .. . ... .. . -... -.. -. -.. - To ensure that excessive exposures are not being-caused by the amount of dust in the house, the Agency recommends that efforts always be made to minimize _dust in residences, even after paint and dust sources have been addressed through any needed interim control and/or abatement activities. A key component of these effoits is the need to maintain a residence in a cleanable state (i.e., in such a condition that it can be effectively cleaned by the occupant using reasonable cleaning procedures). For example, water-damaged or worn wood flooring may have a rough surface with ~revices from which dust cannot be readily removed through routine wet mopping. Such surfaces should either be replaced or repaired so :hat they are cleanable. Likewise, it is important that the residence be effectively and regularly cleaned and that exposures to anv i~terior du-t be minimized. Recommended activities to reduce ~nterior dust lead levels and associated exposures include: mopping floors, window ledges, and accessible surfaces with a warm detergent solution; washing pacifiers aod bottles if they fall_ on the floor; washing toys and stuffed anim.als regularly; and ensuring that children wash their hands before meals, naps, and bedtime. These activities, as well as the importance of nutrition and other factors relevant to children's -risk from lead exposure, should always be stressed as part of public education and awareness programs, regardless of the measured lead concentration in any one medium. Lead-Contaminated Soil Lead-contaminated exterior bare soil is of concern both as a direct source of exposure through inadvertent ingestion due to children's normal hand-to-mouth activity, and as a contributor to indoor dust lead levels (e.g., when tracked into a .residence from outside). Common sources of lead in residential soil include deteriorating exterior lead-based paint and historical airborne . deposition onto the soil surface as the result of point source· emissions or leaded gasoline. These sources have added substantially to the naturally occurring lead in soils, which 8 I I I I I •• I I I I I I •• I I generally range from~ -50 parts per million'. Also, industrial sources such as smelters, recycling facilities, and mining activities can result in lead contamination at residential areas. This adds difficulty in relating lead levels in soil to potential health effects because lead from different sources may pose different levels of potential hazard. One apparent difference is the extent to which ingested lead originating from different sources is taken up into th~ body-~that is, the bioavailability of the lead ... Decisionmakers should consider this and any other available information when implementing the recommendations contained in this guidance, particularly where non-paint sources of lead are involved. That is, if the soil is contarr.inated by lead. from other sources, rather than lead-based _ paint, decisionmakers should investigate the types of lead compounds present and their.unique characteristics. Agency guidance on consideration of bioavailability of lead in risk assessment can be found in the Guidance Manual for.the Integrated Exposure Uptake Biokinetic Model for Lead in Children (available from National Technical-Information Service, U.S .. Dept. of Commerce, Attn: Sales, Springfield, VA 22169 (703/487-4650), as document number PB 93-963510). s· ll lead concentrations in the Unit:d States vary wic:eiy, from less than one to tens of thousands of parts per million (ppm). Thi~ range of concentrations and attendant.potential exposure levels indicates that it is appropriate to develop a scaled strategy of risk reduction activi'::ies, depending upon the concentra_tions at particular locations and oth·er site-specific factor,. The Agency's recommendations for response acti 'ties at varyin~ soil lead concentrations are as follows. The Ag~ncy is recommending that (depending upon use patterns, populations at risk, and other factors), when lead concentrations are observed that exceed 400 ppm in bare soil, further-evaluation should be undertaken and_physical exposure- reduction activities, commensurate with the expected degree of risk, are appropriate .1 The Agency believes that. the 400 ppm 'U.S. Environmental Protection Agency (1989) Review of the National Ambient Air Quality Standards for Lead: Exposure Analysis Methodology and Validation. U.S. EPA Office of Air Quality Planning and Stahdards, RTP, NC. EPA-450/2-89/011. 'The selection of 400 ppm in this guidance is based upon two decisions. The first is that the level should help in reducing the threat that environmental lead poses to the public. ln this guidance, EPA estimates that beginning exposure reduction activity at 400 ppm will help ensure that·a typical child or group of children exposed to lead would have an estimated ris~ bf no more than 5% of .eAceeding a blood lead level of 10 µg/dl. This benchmark may change in the future section 403 rulP.making. 9 I. I •• I I I I I I I •• I I I I I I •• I I The second decision is to use the best available tool for ass~ssing the relationshi~ between children"s blood lead levels and environmental lead levels. Current research indicates that young children are particularly sensit~ve to the effects of lead and require specific attention in the development of lead · · standards. A .level that is protective for young children is expected to be protective.for older population subgroups .. In the same environmental' setting, pregnant women would be expected to have blood lead levels low~r than would young children, and this may further limit fetal exposures. The Ag~ncy has examined both epidemiological studies and modeling approaches for this purpose. Both of these will be further evaluated as part of .the effort to develop section 403 rulemaking. However, given the need to issue guidance at this time, the. Agency is choosing to base the guidance on the Integrated Exposure Uptake Biokinetic (IEUBK) .model, which EPA designed tO evaluate exposures to children in a residential setting. In general the model generates:a probability distribution .of blood lead :...?vels for a typical child, or group of children, exposed to a particular soil lead concentration and concurrent lead levels from other sources. The spread of the distribution reflects the observed variability of blood lead· levels· in several communities. This variability arises from several sources, including behavioral and cultural factors. The identification of lead levels from other sources (due to air, water, diet, etc.) is an essentia·1 part of characterizing the appropriate blood lead distribution for~ specific neighborhood or site. For the purpose of deriving the 400 ppm value used in this guidance, the background lead exposure inputs to the_IEUBK.model ·were determined using national averages, where suitable·, or typical values. Thus, the estimated level of 400 ppm is associated with an expected ,,.typical" response to these exposures, and should not be taken to indicate that a certain level of. risk (e.g., exactly 5% of children exceeding 10 µg/dl blood lead) will be observed in a specific community (e.g., in a blood lead survey). Because a child's exposure to lead involves a complex array of variables, because there is population sampling variability, arid beciuse there is variability in environmental lead measurements and background levels of lead in food and drinking water, results from the model may differ from results of blood lead screening of children in a community. Extensive field · evaluation of the model is in progress and-the model will be evaluated further.once these efforts are completed. EPA may base: the future ·~ectiOn 403 rulemaking on ~he model once these 10 1/ •• I I I I I I I •• I I I I I I •• I I level s.erves as a reasonable current. be.:1chrnark for the purposes of this guidance. Therefore, the Agency recommends that further evaluation and appropriate exposure-reduction activities be undertaken when soil lead concentrations exceed 40D ppm at areas expected or intended to be used by children.' (Recommendations for soil sampling and analysis are attached.) Further evaluation activities may include blood lead screening of children and others in the community. When soil lead levels exceed 400 ppm and children are likely to be present, exposure-reduction responses should focus on interim controls designed to change use patterns and create barriers between children and contaminated soil. This involves taking steps to. keep children. away. from certain--areas -and to · · - reduce exposure to bare soil in accessible areas. As an example of changing the use pattern, thorny shrubs can be planted to keep children from playing around houses that.have elevated soil lead concentrations immediately next to the house. Also, play equipment can be moved from bare soil contaminated areas to encourage children to pl~y elsewhere or, for more highly contaminated areas, access can be restricted by fencing. As an example .of the use of barriers to reduce exposure, grass or other groundcover can be ~stat"ished and maintained or the area can be covered with mulch or g~3vel. While the effectiveness of many of these interim control actions cannot yet be quantified, the Agency believes that they can reduce exposure. However, whenever interim controls are used, their condition should be monitored to ensure continued effectiveness. For example, the condition' of plants, groundcover, ... 2tc., that serve as use-modifying and barrier-type elements sr ,uld be visually inspected to ensu~c, that they have become well established and remain effective at · preventing exposure in accordance with the upcoming HUD Guidelines.·. · Within the range of 40D -SOOD ppm, the degree of risk reduction activity should be commensurate with the expected risk posed by the bare soil, considering both the severity of exposure (as reflected by the soil lead concentration) and the likelihood of children's exposure. At concentrations· in the lower segment evaluations have been completed, or on another methodology. '4D0 ppm is also used as the residential soil lead screening level for corrective Action under the Resource Conservation and Recovery Act (RCRA) · and cleanups under the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) in the Office of Solid Waste and Emergency Response (OSWER) Interim Soil Directive .. OSWER's screening level is not a "cleanup standard,• nor automatically a •cleanup goal." Rather, it is a level of contamination above which there is enough concern to warrant site-specific study of risks. 11 I •• I I I I I I I •• I I I I I I •• I I of this rc•nge (e.g., between 400 ppm and 2000 p:-,ml, emphasis should be placed on reducing exposures through interim controls at those areas expected or intended to be used· by children, 1 f the area is not frequented by children, these exposure reduction activities may be less rigorous. Where bare-s6il lead levels are found to be 2000 parts per million or more, interim controls should be implemented even if the area is not frequented by children. · Increasingly aggressive exposure-reduction activities are warranted at higher soil lead levels; with·very high levels indicating that soil abatement maybe necessary. For purposes of prioritizing abatements, the Agency recommends soil abatement ·when lead ·levels are found at 5000 parts per million_ or more in residential bare soil. Appropriate activities at this level of lead concentration may include removal and replacement of the soil,. the use of more permanent covers (e.g., paving), or other activities. Of course, state and local agencies should consider any other factors that affect the actual risks and benefits of. abatement when determining whether abatements may be necessary at lower levels, including, for example, prevalence of elevated - blood lead levels in children. The Agency is suggesting 5or J ppm for this hi_gher level because of the need to prioritize the types of activities that can often be resource intensive. Factors considered in the choice of this level include the risk reduction that may be achieved by different measures and the resources needed to reduce those risks .. Consequently, this level is designed to indicate where there is a relatively highe·· certainty that abatement or other extreme activities would be appropriate from a risk reduction and resource prioritization perspectiv~. Based upon estimates of residential soil lead distributions (from HUD, 1990), 5000 'ppm would target the soil at an estimated 1/2'< of U.S. homes. B~cause of the likelihood that lead-contaminated soil will have previously contributed lead to interior dust, specialized cleaning is ·recommended for the interior of residences to meet dust clearance levels after soil abatement or interim control activities have been conducted. The Agency's recommendations for residential lead- contaminated soil are summarized in Table I. 12 ... - ------- - - -- - - -- --• • • Tahle !--EPA Rccommendalion, for Response Aclivilie, for Residenlial l.cad-Conlaminaled llare Soil llare Soil Lead Area of Concern Concenlration (ppm) Recommended Respon,e Activities - Interim controls lo change use pallern, and establish harrlen between children and conlilminalcd ~oil, including: , ► planling ground cover or shrubbery to reduce eiposure lo bare soil. Areas expeded lo be used hy children, 400 -5000 ·,;. moving play equipment away from cont:uninaled bare soil, including: ► restricting access 1hrough posting, fencing. or otheractions, and ► residential baclcyard,. ► conlrol further contamination of area. ► daycare and !!Chool yards, Monitor condition of interim controls. ► playgrounds, Public notice of contaminated common arcu by local agency. ► public parks. and AJalemenl of soil, including:· ► other areas where children gather_ > 5000 ► removal and replacement of contaminated soil. and i,. permanent barders. Public notice of contaminated common area., by local agency. lnlerim controls lo change ii~ patterns and eslabli<h barriers belween children and contaminaled soil. including: ► planting g·ro_und_ cover or shrubbery to reduce c~posu~ to bare soi1. ► moving play equipment away from contaminated bare soil, 2000 • 5000 ► restricting access through posting. fencing, or other actions, an~ ► control further contamination of area. Areas where contact by children is less \fonitor conditil .. r interim control!. likely or infrequent Public notice of contaminated common area., by local agency. Abatement of soil, Including: > 5000 ► removal and replacement of contaminated soil. and· ► pernuncnt barriers. Public notice of contaminated common arcu by local agency. 13