NCD980799019_19960201_Cherokee Oil_FRBCERCLA RA_CERCLA Removal Action-OCR

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CERCIA Removal Action
Cherokee Oil Site (Berryhill Location)
Charlotte, Mecklenburg County, North Carolina
Bulk Group Analytical
FEDERAL
PROGRAMS
® DIVISION
REGION IV TECHNICAL ASSISTANCE TEAM
-1, Note: This document contains most of the bulk group analytical
, however, it is not complete. For a complete version,
please contact Steve Spurlin, USEPA (Region IV).
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·. , .•• · •.•.•• ,; .. ,,t.'
A12c121v12D
-F"t 8 0 2 1996
AquaChem Environmental Laboratories, lnc~UP£RFuND
Data Qualifier Definitions S£cr,oN
U -Compound analyzed for but not detected.
E -Compound exceeded calibration range.
D -Compound analyzed at a secondary dilution factor.
J -Compound detected but below the contract required
detection limit. The value given was an estimate.
S -Spiked compound.
B -Compound was found in the Method Blank.
A -Suspected Aldo! condensation product.
Y -Indistinguishable isomer in tentatively identified
compounds.
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·1
* Note:
Bulk Group 03
Bulk Group Description: PCB Solid
Bolk Groups were named aeeordiog to preliminary hazardous
l'.ategorization test and may not eorrespood to what the material
was elassified as for disposal.
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Ii•)) 1 Aqua Chem
11176 Downs Road .
. Pineville, NC 28134
704/588-5076
. FAX [phone] I
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Certificate of Analysis
I_,·-.
:.:_;:
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Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG#: SR633080
Lab ID: AAI 1898
Sample ID:. BG-03
Parameter
) Total Organic Halide (TOX)
Paint Filter
Corrosivity
BTU
Flash Point
Reactive Cynide
Reactive Sulfide
PH
Result
ILi
Negative
6.88
2650
156
Negative
Negative
6.88
Detection
Limit
LO
0-14
70
0-14
Unit
ppm
s.u.
BTU/gal
Deg.F
ppm
ppm
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: 12-Jun-95
Approved By: -=~-"-'~-""""""'"'1"""'=-~-R~C~~ 6
Project Manager
Method Time Date Analyst
SM 506 17:00 05/30/95 JCH
SW846 10:00 05/28/95 TML
SW-846 #111 08:20 05/30/95 RCD
SW-846 #909 17:00 05/30/95 JCH
SW-846 #909 10:00 05/30/95 TML
SW846 9010 11:00 05/31/95 TML
SW846 9030 11:00 05/31/95 TML
SW846 9045 08:20 05/30/95 RCD
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1.
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·,
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
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Client:
Client#:
Contact:
SDG#:
Lab ID:
. Sample ID:
Parameter
OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
3080
Mr. Randy Bennett
SR633080
AAll898
BG-03
Result
If[) I PCB 1242
PCB 1248
u
u
u
u
u
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( 1--
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PCB 1254
PCB 1260
Toxaphene
Total Organic Halide (TOX)
Paint Filter
Corrosivity
BTU
Flash Point
Reactive Cynide
Reactive Sulfide
PH
I I.I
Negative
6.88
2650
156
Negative
Negative
6.88
Detection
Limit
1.0
0-14
70
0-14
Unit
ppb
ppb
ppb
ppb
ppb
ppm
s.u.
BTU/gal
Deg. F
ppm
ppm.
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Date:
Approved By:
Method
EPA 8080
EPA 8080
EPA 8080
EPA 8080
EPA 8080
SM506
SW846
SW-846 #II 1
SW-846 #909
SW-846 #909
SW846 9010
SW846 9030
SW846 9045
24-May-95
12-Jun-95
R~~~C
Project Manager
Time Date Analyst
18:52 06/07/95 RAG
18:52 06/07/95 RAG
18:52 06/07/95 RAG
18:52 06/07/95 RAG
18:52 06/07/95 RAG
17:00 05/30/95 JCH
10:00 05/28/95 TML
08:20 05/30/95 RCD
17:00 05/30/95 JCH
10:00 05/30/95 TML
11:00 05/31/95 TML
11:00 05/31/95 TML
08:20 05/30/95 RCD
I
I;;:, lJ\quaChem
I ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
· Pineville, NC 28134
704/588-5076
FAX [phone] I
I Certificate of Analysis
Client: OHM Corporation I
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240 l Tuckaseegee Road
Charlotte, NC
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
3080
Mr. Randy Bennett
SR633080
AA11898
BG-03
I"/) 4,4'-DDD
4,4-DDT
I Aldrin
Alpha-BHC
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Alpha-chlordane
Beta-BHC
Delta-BHC
Dieldrin
Endosulfan I
Endosulfan sulfate
Endrin
Endrin ketone
Gamma-BHC (Lindane)
Gamma-chlordane
Heptachlor
Heptachlor epoxide
Methoxychlor I PCB.1016
. . . . PCB 1221
r · .. • ;-, ,, __ ., PCB 1232
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Result
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Detection
Limit
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Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: 12-Jun-95
Approved By: ~/~ "/) -R~~"""e 'ri. "-1:~u"""rry-""'~v--
Projcct Manager
Method Time Date Analyst
EPA8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG.
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
EPA 8080 18:52 06/07/95 RAG
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1-~ AquaChem ! .-.
I 'ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076 I FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: ~-=~
Lab ID: AA11898 R6bert L. Curry Q
I Sample ID: BG-03 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst 1::-·,, Benzene 0.21 E 0.005 mg/L 1311/8260 11:13 06/01/95 DLC ,.-i -,
Carbon tetrachloride u 0.005 mg/L 1311/8260 11:13 06/01/95 . DLC
I Chlorobenzene u 0.005 mg/L 13 I 1/8260 11:13 06/01/95 DLC
Chloroform u 0.005 mg/L 1311/8260 II: 13 06/01/95 DLC
,I Methyl ethyl ketone 0.15 0.005 mg/L 1311/8260 11:13 06/01/95 DLC
Tetrachloroethylene 0.007 0.005 mg/L 1311/8260 11:13 06/01/95 DLC
Trichlorciethylene u 0.005 mg/L 1311/8260 II: 13 06/01/95 DLC
I Vinyl chloride u 0.005 mg/L 1311/8260 11:13 06/01/95 DLC
2,4,5-Trichlorophenol UD 0.20 mg/L 1311/8270 13:12 05/30/95 ANM
I 2,4,6-Trichlorophenol UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
2,4-Dinitrotoluene UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
Hexachlorobenzene -UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM ' I Hexachlorobutadiene UD 0.20 mg/L 1311/8270 13:12 05/30/95 ANM
Hexachloroethane UD 0.20 mg/L 1311/8270 13:12 05/30/95 ANM
I m-Cresol UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
Nitrobenzene UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
o-Crcsol UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM I p-Crcsol UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
;:. . _, Pentachlorophenol UD 0.20 mg/L 1311/8270 13:12 05/30/95 ANM ' 1.:-• Pyridine UD 0.20 mg/L 1311/8270 13: 12 05/30/95 ANM
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1-, Jr C . ,,/1 iflz4qua hem
I . ~ ENVIRONMENTAL LABORATORIES, INC .
11176 Downs Road
Pineville, NC 28134
704/588-5076
I FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date:
I SDG#: SR633080 Approved By:
Lab ID: AAll898
I Sample ID: BG-03 Project Manager
Detection
Parameter Result Limit Unit Method Time Date ,.~ : .'..) . u 0.005 mg/L 1311/6010 13:45 05/30/95 ,.~_i Arse_mc
Barium 8.8 0.1 mg/L 1311/6010 14:50 06/01/95
I Cadmium 0.03 0.01 mg/L 1311/6010 17:39 06/01/95
Chromium u 0.05 mg/L 1311/6010 17:39 06/01/95
Lead 0.14 0.05 mg/L 1311/6010 17:39 06/01/95
I Mercury u 0.0002 mg/L 1311/6010 10:30 06/02/95
Selenium u 0.005 mg/L 1311/6010 15:00 05/30/95
I Silver 0.02 0.01 mg/L 1311/6010 17:39 06/01/95
Chlorodane u 0.010 mg/L 13 ll/8080A 14:46 06/08/95
Endrin u 0.010 mg/L 13 l l/8080A 14:46 06/08/95 I Heptachlor u 0.010 mg/L 131118080A 14:46 06/08/95
Heptachlor epoxide u 0.010 mg/L 131118080A 14:46 06/08/95
I Lindane u 0.010 mg/L 131118080A 14:46 06/08/95
Methox·ychlor u 0.010 mg/L 13 l 1/8080A 14:46 06/08/95
I Toxaphene u 0.010 mg/L 1311/8080A 14:46 06/08/95
2,4,5-TP (Silvex) u 0.010 mg/L 1311/8150 14:26 06/06/95
2,4-D u 0.010 mg/L 1311/8150 14:26 06/06/95
I I, 1-Dichloroethylene u 0.005 mg/L 1311/8260 II: 13 06/01/95
. : 1,2-Dichloroethane u 0.005 mg/L 1311/8260 11: 13 06/01/95
'-I'-__, 1,4-Dichlorobenzene u 0.005 mg/L 1311/8260 11: 13 06/01/95
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305
99032
Analyst
KRR
RCD
RCD
RCD
RCD
TML
KRR
RCD
RAG
RAG
RAG
RAG
RAG
RAG
RAG
RAG
RAG
DLC
DLC
DLC
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Bulk Group 04
Balk Group Description: PCB Liquid
* Note: Bulk Groups were named aeeording to preliminary hazardous
eategorization test and may not eorrespond to what the material
was elassified as for disposal.
OCT 16 '95 14:56 TO 3911147 .~ FROM AquoCh•m Enuir. Lab T-572 P.02
PraliBiDary 11.eport
1 ... •
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:·~,-/
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LA~::~~.~~ .. ro ...... ,
11176 Downs Rood
Pfnevllle, NC 28134
704/588-5076
FAX [phone]M
Certificate of Analysis
--··-···--·--· --------
Client: OHM Corporation
240 I Tuckasecgee Road
Charlotte. NC
Client#: 381
Contact: Jack Kilbarger
Sample Date: 24-May-95
SDG #: SDG--000151
Lab Sample ID: LSID-000182
Sample ID: BG--04
Parameler Result
PCB 1016
!'CB 1221
PCB 1232
PCB 1242
PCB 1248
PCB 1254
PCB 1260
u
u
u
u
u
u
143
Reporting
Limit Unit
0 ppm
0 ppm
0 ppm
0 ppm
0 ppm
0 ppm
1 ppm
Page 1
North Carolina Certification Number: 30~
South Carolina Certification Number: 99031
Reulpt Date 04-0ct-95
Report Date: 16-0ct-95
Approved By: ~""""-· ....... , ~---~
~rry p
Project Manager
Method Time Date Analyst
EPA 8080 IU/10/95 MW
EPA 8080 10/10/95 MW
EPA 8080 10/10/95 MW
EPA 8080 10/10/95 MW
EPA 8080 10/10/95 MW
EPA8080 10/10/91 MW
EPA8080 ·. 10/10/95 MW
I
·.@! /A~:!~o'E,~~~,o,uoa,es, '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076 I FAX [phone]
Certificate of Analysis I
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I
Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
I"'~'\ ~4'..'.-:'
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Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA11899
Sample ID: BG-04
Parameter
) Butyl benzyl phthalate
Chrysene
Di-n-butyl phthalate
Di-n-octyl phthalate
Dibenzo(a,h)anthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno( 1,2,3-cd)pyrene
Isophorone
N-nitroso-di-n-propylamine
N-nitrosodiphenylamine
! Naphthalene
I!(_;) ·· Nitrobenzenc
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Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
1500
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
Receiwd Date:
Report Date:
Approved By:
Method
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
' EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
Time
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
Date Analyst
05/31/95 ANM
05/3 1/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
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••::)/:
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A~~~s,~.~~•omoa,es, '"
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: -~-8 Lab ID: AA11899 R6b~Cuny
I Sample ID: BG-04 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
Ii) i 4-Brnmophenyl phenyl ether UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
4-Chloro-3-methylphenol UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
I 4-Chloroaniline UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
4-Chlorophenyl phenyl ether UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
4-Methylphenol (p-cresol) UD 1000 ppb EPA 8270 16:27 05/31/95 ANM ,I 4-Nitroaniline UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
4-Niuophenol UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
I Acenaphthene UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
Acenaphthylene UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
I Benzo(a)anthracene UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
Benzo(a)p)Tene UD 1900 ppb EPA 8270 16:27 05/31/95 ANM
Benzo(b)fluoranthene UD 3000 ppb EPA 8270 16:27 05/31/95 ANM
I Benzo(ghi)perylene UD 2000 ppb EPA 8270 16:27 05/31/95 ANM
Benzo(k)fluoranthene UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
I Benzoic Acid UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
Benzyl alcohol UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
Bis(2-chloroethox1·) methane UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
I Bis(2-chloroethyl) ether UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
i Bis(2-chloroisopropyl) ether UD 1000 ppb EPA 8270 16:27 05/31/95 ANM
1-·· Bis(2-cthylhex-yl) phthalate UD 1900 ppb EPA 8270 16:27 05/31/95 ANM
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/A~~~o!E,~~~,oamm.,,o
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I
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Certificate of Analysis
Client: OHM Corporation
2401 Tuckaseegee Road
Charlotte, NC
I
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Client#: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA! 1899
Sample ID: BG-04
Parameter IJ}) ·· \ Pentachlorophenol
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Phenanthrene
Phenol
· Pyrene
Total Suspended Solids
Total Organic Halide (TOX)
Barium
Cadmium
Chromium
Copper
Iron
Lead
Nickel
Silver
Zinc
Arsenic
Mercury
Selenium
. , BTU
• •\~.:) Flash Point
I
Result
UD
UD
UD
UD
141000
u
69.6
1.15
3.68
77.2 D
2740 D
33.6
2.07
u
92.9D
0.340
UD
2.85 DE
8610
152
Detection
Limit
1000
1000
1000
1300
1.0
0.5
0.05
0.25
1.0
15
0.25
0.15
0.05
0.5
0.025
0,002
0.25
70
Unit
ppb
ppb
ppb
ppb
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
BTU/gal
Dcg.F
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receh·cd Date: 24-May-95
Report Date: 12-J -95
Project Manager
Method Time Date Analyst.
EPA 8270 16:27 05/31/95 ANM
EPA 8270 16:27 05/31/95 . ANM
EPA 8270 16:27 05/31/95 ANM
EPA 8270 16:27 05/31/95 ANM
SM209C 10:00 05/29/95 TML
SM506 17:00 05/30/95 JCH
SW 6010 14:50 06/01/95 RCD
SW 6010 18: 10 05/31/95 KRR
SW 6010 18:10 05/31/95 KRR
SW 6010 18:10 05/31/95 KRR
SW 6010 16:07 05/31/95 KRR
SW 6010 18·.12 06/01/95 RCD
SW 6010 18: 10 05/31/95 KRR
SW 6010 18:10 05/31/95 KRR
SW 6010 18:10 05/31/95 KRR
SW 7060 08:30 06/01/95 KRR
SW7470 10:30 06/02/95 TML
SW7740 09:20 06/01/95 KRR
SW-846 #909 17:00 05/30/95 JCH
SW-846 #909 10:00 05/30/95 TML
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1-~--. · .. -,.
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1,--:::,,
. -' ·~:2,::-'
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/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Dat,e: 12-Jun-95
SDG#: SR633080 Approved By: l{f~ Lab ID: AAll899 ifoi__ C;;ry~
Sample ID: BG-04 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
) Aluminium 603 D 50 ppm SW846 6010 08: 19 06/01/95
Antimony 0.07 0.05 ppm SW846 6010 11:10 05131/95
Beryllium u 0.25 ppm SW846 6010 16:07 05/31/95
Calcium !660D 25 ·ppm SW846 6010 16:07 05/31/95
Cobalt u 0.25 ppm SW846 6010 11: 15 05/31/95
Maganese 136 D 25 ppm SW846 6010 16:07 05/31/95
Magnesium 339 D 25 ppm SW846 6010 16:07 05/31/95
Potassium 206 0.5 ppm SW846 6010 07:37 06/01/95
Sodium · 2700D 50 ppm SW846 6010 09:50 06/01/95
Thallium 0.13 0.05 ppm SW846 6010 08:20 05/31/95
Vanadium 1.59 0.25 ppm SW846 6010 16:07 05/31/95
Reactive Cynide Negative ppm SW846 9010 11:00 05/31/95
Reactive Sulfide Negative ppm SW846 9030 11:00 05/31/95
pH 6.78 0-14 SU SW846 9040 08:20 05/30/95
305
99032
Analyst
KRR
KRR
KRR
KRR
RCD
KRR
KRR
KRR
KRR
KRR
KRR
TML
TML
RCD
I
I.
LA~~~o'E~,~~•oa..um, '"
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation I
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I
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240 I Tuckaseegee Road
Charlotte, NC
Client #: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA 11899
Sample ID: BG-04
Parameter Result IC?J) Percent Water 40.70
Total Dissolved Solids 5800
I Total Organic Carbon (TOC) 520,000
I, I, 1,2-Tetrachloroethane u
I, I, I-Trichloroethane 200,000 DE I I, 1,2,2-Tetrachloroethane u
I, I ,2-Trichloroethane u
I I, 1-Dichloroethane u
I, 1-Dichloroethene u
I 1,2-Dichloroethane u
1,2-Dichloropropane u
2-Butanone 87,000 D
I 2-Chloroethylvinyl ether u
2-Hexanone u
I 4-Methyl-2-Pentanone u
Acetone u
Benzene u
I Bromodichloromethane u
, Bromoform u .,~, Bromomethane u
I
Detection
Limit
5000
5000
10000
5000
5000
10000
5000
5000
12000
10000
5000
10000
16000
5000
5000
5000
10000
Unit
%
ppm
ppm
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receh·ed Date: 24-May-95
Report Date: 12-Jun-95
Approved By: ~ ·
R~.c;,J' 2}
Project Manager
Method Time Date Analyst
17:00 05/30/95 JCH
EPA 209A 16:25 05/30/95 . RCD
EPA 415.1 17:00 05/30/95 .JCH
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
' EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05130/95 DLC
EPA 8240 19:34 05130/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05130/95 DLC
EPA 8240 19:34 05/30/95 DLC
I
:'.?' 1
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/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I
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I
Client:
Client#:
Contact:
SDG#:
Lab ID:
OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
3080
Mr. Randy Bennett
SR633080
AA! 1899
Sample ID: BG-04
Parameter Ir~)_) Carbon disulfide
Carbon tetrachloride
Result
u
u
I Chlorobenzene·
Chlorodibromomethane
u
u
I Chloroethane
Chloroform
u
u
Chloromethane u
I cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
u
u
I Ethylbenzene
Methylene chloride
300,000 DE
u
R
Stryen~
Tetrachloroethene
u
u
Toluene 68,000 D
Detection
Limit
10000
5000
5000
10000
10000
5000
20000
5000
5000
5000
14000
10000
5000
5000
I Total Xylenes 4,200,000 DE 5000
trans-1,2-Dichloroethene u 5000
I trans-1,3-Dichloropropene
Trichlorocthene
u 5000
u 5000
,-· .. . ) Vinyl chloride 1\ _ _:,1., 1,2,4-Trichlorobenzene
u 10000
VD 1000
I
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Dat~:
Approved By:
Project Manager
Method Time Date Analyst
EPA 8240 19:34 05/30/95 DLC
. EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
' EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05130/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05130/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8240 19:34 05/30/95 DLC
EPA 8270 16:27 05/31/95 ANM
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1 __ ,,
l::r}
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l a•.,_-, ,, .• •. -. ·-~~:/
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I(_;__;)
I
/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
·FAX 704/588•2454
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#:
Contact:
SDG#:
Lab ID:
3080
Mr. Randy Bennett
SR633080
AA11899
Sample ID: BG-04
Parameter
: 1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphcnol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol (o-cresol)
2-Nitroanilinc
2-Nitrophcnol
3,3-Dichlorobenzidine
3-Nitroaniline
i 4,6-Dinitro-2-mcthylphcnol
4,6-Dinitro-o-crcsol
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date:
Approved By: '"~·zy
Project Manager
Method Time
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270 16:27
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
16:27
Date Analyst
05/31/95 ANM
05/31/9_5 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95 ANM
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
I
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Bulk Group 06
Bulk Group Description: Peroxide Liquid
* Note: Bulk Groups were named aeeording to preliminary hazardous
eategorization test and may not eorrespond to what the material
was elassified as for disposal.
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r~un HquaLiem Enutr. Lab T-386 P.02
Certificate of Analysis
Client: OHM Corporation North Carolina Certiflution Number: 2401 Tuckaseegee Road Soulh Carolina Certification Number: Charlotte, 1'C
Client II: 3080 Receh-ed Date: 02-Aug-9S Contact: Mr. Randy Bennett Report Date: 23-Aug-9S
SDG#: SY533080 Approved Ry:
Lab ID: AAl39S0 Robert L. Cuny Sample ID: BG-06 0772 Project Manager
Detection
Parameter Result Limit Unit Melilod nm. D111e
Dis(2-cthylhc~-yl) phlhalatc UD 5000 ppb EPA 8270 06:26 08/05/95
Butyl benzyl phthalate UD S000 ppb EPA 8270 06:26 08105/95
Ghry5Clle LID 5000 ppb EPA 8270 06:26 08/05/95
Di-n-butyl phthalate l! D sooo ppb EPA 8270 06:26 U!l/05195
Di-n-octyl phthalate UD 5000 ppb EPA8270 06:26 08,05/95
Dibe!IZO(ah)anthracene UD 5000 ppb EPA8270 06:26 08/05/95
Dibemofuran UD 5000 ppb EPA8270 06:26 08/05195
Diethylpbthalate UD 5000 ppb EPA8270 06:26 08/05195
DiruclhylphUlalatc UD S000 ppb EPA8270 06:26 08105195
Fluoranlhenc UD 5000 ppb EPA8270 06:26 08/05195
Fluorcne 11D 5000 ppb EPA8210 06·.26 08/05195
Hcxachlotobenzene UD 5000 ppb EPA8270 06:26 08/05195
HeJQlchlorobutadiene \;D 5000 ppb EPA 8270 06:26 08/05195
Hexachlorocyclopentadiene UD 5000 ppb EPA 8270 06:26 08105/9S
Hexachloroethane UD 5000 ppb EPA 8270 06:26 08105195
lndeno(l ,2,3-<:d)pyrcne UD 5000 ppb EPA 8270 06:26 08105/95
lsophoronc UD 5000 ppb EPA 8270 06:26 08/05i95
N-NiUoso-di-n-propylaminc UD 5000 ppb EPA8270 06:26 08/0S/95
N-NiUosodiphenylamine UD sooo ppb EPA8270 06:26 08105/95
NaphUialeue 1900 DJ sooo ppb EPA 8270 06:26 08/0S/95
305
99032
Aual1sl
ANM
ANM
ANM
A.11/M
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A,'IIM
A.'IM
ANM
ANM
ANM
HUu Ll '35 15:59 TO 39ill47 FROM AquaChem Eautr. Lab T-386 P,06 I
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I Certificate of Analysis
I Client: OHM Corporation Nonb Carolina Cenification 1'"umber: 305 2401 Tuckaseegee Road South Carolina Certification Sumber: 99032 Cllarlotte, NC
I Client#: 3080 Received Date: 02-Ang-95 Contact: Mr. Randy Bennen Report Date: 23-Aug-95
I SDG#: SVS33080 Approved By:
LabID: AA1J952 Rcben L. Curry
I Sample ID: B~ 0772 Project Maaager
Detectioo \ Parameter lwull Umit Unit Method Time Date Analyst I Arsenic I.OS 0.50 ppm SW 6010 09:35 08107/9S RCD Barium 17GOD 50 ppm SW60IO 11:05 08116/95 RCD
I Cadmium u 0.05 ppm SW60IO 10:45 08/0819S RCD Chromium 1.10 · 0.25 ppm SW6010 10:45 08108195 RCD Copper 0.15 0.10 ppm SW6010 10:45 0810819S RCD I Iron 8.10 o.os ppm SW60IO 08:35 08108/95 RCD Lead 0.36 0.2S ppm SW 60IO I0:45 08/08/95 RCD Nickel u 0.1S ppm SW6010 10:45 08/08/95 RCD ·1 Selenium 0.058 0.025 ppm SW60IO 10:50 08/07/95 RCD ' -' Silver u 0.05 ppm SW60IO 10:45 08/08/95 RCD I Zinc 1.06 0.05 ppm SW60IO l0:45 08/08/95 RCD Mercury u 0.002 ppm SW7470 08:10 08/16/95 RCD Aluminium u 0.5 ppm SW84G GOIO 08:JS 08116/95 RCD I AnLimony 0.012 0.050 ppm SW8466010 14:40 08107/95 RCD Beryllium u 0.05 ppm SW8466010 Oll:]5 08108/95 RCD
I Calcium 4,90 0.0S ppm SW846 6010 08:35 08108195 RCD Cobah u 0.0S ppm SW8466010 ll:30 . 08/07/95 RCD Magnesium 0.29 0.05 ppm SW8466010 08:35 08/08195 RCD I Manganese 0.37 0.0S ppm SW84660IO 08:35 0810819S RCD Potassium u ,.o ppm SW846 6010 12:10 08107/95 RCD
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FROM HquaCh~m E.ivir. Lab T-386 P.05
Certificate of Analysis
Client: OHM Corporation Nor1h Carolina Certification Number: 240 I Tuckaseegee Road South Carolina Certfflcation Number: Charlotte, NC
Client#: 3080 Received Date: 02-Aug-95 Contact: Mr. Randy Bennett Report Date: 23-Aug-95
SDG#: SV533080 Approved By:
Lab ID: AA139Sl Robert L. Curry Sample ID: BG--06 0772 Project Manager
Detection
Parameter Relllll Limit Unit Method Time Date
Chlorodibromomethane u 100000 ppb EPA 8240 11:14 08/04/95
Cbloroethsne u 100000 ppb EPA 8240 11:14 08/04195
Chloroform u 50000 ppb EPA 8240 ll:14 08/04/95
Chloromethane u 200000 ppb EPA 8240 11:14 08/04/95
cis-1,2-Dichloroethene u 50000 ppb EPA 8240 11:14 08/04195
cis-1,3-Dichloropropcnc u 50000 ppb EPA 8240 11:14 08/04/95
Ethylbcnzene 20,0000 J 50000 ppb EPA 8240 11:14 08/04/95
Methylene chloride u 140000 ppb EPA 8240 11:14 08/04/95
Stryene u 100000 ppb EPA 8240 II: 14 08/04/95
Tetrachlorocthcne 30,000 DJ 50000 ppb EPA 8240 11:14 08/04/95
Toluene 50,000 0 J 50000 ppb EPA 8240 11:14 08/04/95
Total Xylenes 270,000 0 50000 ppb EPA 8240 11: 14 08/04/95
trans-1,2-Dichloroethone u 50000 ppb EPA 8240 11:14 08/04/95
lrans· l ,3-Dichloropropcnc u 50000 ppb EPA 8240 11:14 08/04/95
Trichloroethcnc u 50000 ppb EPA 8240 11:14 08/04/95
Vinyl chloride u 100000 ppb EPA 8240 11:14 08i04/95
JOS
99032
Analyst
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
OLC
DLC
DLC
' -
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f'"-R□M AquaChl!'m Env tr. Lab T-386 P.04
Certificate of Analysis
Client: OHM Corporation North Carolina Certification !'lumber: 240 I Tw:kaseegee Road South Carolina Certification Number: Charlotte. NC
Olent#: 3080
Received Date: 02-Aug-95 Contart: Mr. Randy Bennett
Report Date: 23-Aug-95
SDG 11: SV533080 Approved B): Lab ID: AAl3951
Robcn L. Cuny Sample ID: BG-06 0772
Project Manager --·
Detection ParlUlteter Result Limit Unit Method Time Date I, I, 1,2-Teuechlorocthanc u 50000 ppb EPA 8240 11:14 08/04/95 1,1,l •Trichloroethanc u 50000 ppb EPA 8240 11:14 08/04195 I, 1,2,2-Tetrachloroetllane u 100000 ppb EPA 8240 11:14 08/04/95 I, 1,2-Trichloroethane u 50000 ppb EPA 8240 11:14 08104/95 I, 1-Dichloroetliane u 50000 ppb EPA 8240 11:14 08104/95 J, 1-Dichlorocthene u 100000 ppb EPA 8240 11:14 011104/95 l,2-D1chloroahane u 50000 ppb EPA 8240 11:14 08/04/95 1,2-DichlofO!)ropane u S0000 ppb EPA 8240 II :14 08/04/95 2-Butanonc u 120000 ppb EPA8240 11:14 08/04/95 2-Chloroetbylvinyl ether u 100000 ppb EPA 8240 II :14 Oll/04/95 2-Hexanone u 50000 ppb EPA 8240 11:14 08104/95 4-Metbyl-2-Pentanone u 100000 ppb EPA 8240 11:14 08104/95 Acetone 1,000,000 160000 ppb EPA 8240 11:14 08/04/95 Benzene u 50000 ppb EPA 8240 11:14 011/04.'95 Bromodicbloromethane u 50000 ppb EPA8240 11:14 08/04/95 Bromoform u 50000 ppb EPA8240 11:14 08/04/95 Bromomctbanc u 100000 ppb EPA8240 11:14 08/04/95 cart,on disulfide u 100000 ppb • EPA 8240 11:14 08/04195 Carl,on tetrachloride u 50000 ppb EPA 8240 11:14 08104/95 Chlorobc112.ene u 50000 ppb EPA 8240 11:14 08/04/95
J05
99032
Analyst
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
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r-,.,_ur1 HquaL..iem t::/1utr-. Lab T-386 P,03
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305 240 I Tuckaseegee Road South Carolina Cenificatioo Number: 99032 Charlotte, NC
Client#: 3080
Received Date: 02-Aug-95 Contact: Mr. Randy Bennen
Report Date: 23-Aug-95
SDG#: SV533080 Approved By: Lahm: AA13950 Robert L. Curry Sample ID: BG-06 0772
Project Manager
Detection Parameter Result Limit Unit Method Time Dare Analyst Nitrobcnzene UD 3000 ppb EPA 8270 06:26 08/05/95 ANM Pentachlorophenol UD 5000 ppb EPA 8270 06:26 08/05/95 ANM Phenanth<cnc UD 5000 ppb EPA8270 06:26 08105/95 ANM Phenol UD 5000 ppb EPA 8270 06:26 08/05/95 ANM Pyrene IJ D 5000 ppb EPA 8270 06:26 08/05/95 A.""M FlaahPoinl 80 80 Dcg.F SW-846 #909 08:30 08/15/95 RCD pH 7.13 0•14 SU SW8469040 09:20 08/17/95 RCD
HUu c'.3 '95 15:57 70 3911147 FROM AquaC,em Envir, Lab T-386 P, 02 i I
I . f ~
I ,
I ,
I Certificate of Analysis I
I Client: OHM Corporation North Carolina Certific.tlon Number. 305 I 240 I Tuckaseegee Road South Carolina Cenification Number: 99032 Charlotte, J\C -I Client#: 3080 Rcceind Date: 02-Aug-9S Contact: Mr. Randy Benneu Report Date: 23-Aug-9S
I SDG II: SV5J3080 Approved Ry, I Lab ID: AA139S0 Robert L. Cuny
I Sample ID: BG-06 0772 Project Manager I Detection
Parameter Result Limit Unit Method nm. D111c Ana1,., I Dis(2-cthylhcxyl) phthalatc UD 5000 ppb EPA 8270 06'.26 08/05/95 ANM I Butyl bcnzyl phthalate UD S000 ppb EPA 8270 06:26 08105/95 ANM
I Chrysene UD 5000 ppb EPA 8270 06:26 08/0'195 ANM I Di-n-butyl phthalate UD 5000 ppb EPA 8270 06:26 08/05/95 A.IIIM
Di-n-octyl phlhalate UD 5000 ppb EPA8270 06:26 08/05195 ANM I Dibcnzo(ah)anlhraccne UD 5000 ppb EPA 8270 06:26 08/05195 ANM I Dibcnzofuran UD 5000 ppb EPA8270 06:26 08/05/95 ANM
I Dietbylphthalate UD 5000 ppb EPA8270 06:26 08/05195 ANM I Dimclhylphlhalatc UD 5000 ppb EPA8270 06:26 08/05/95 ANM
Fluoranthene UD 5000 ppb EPA8270 06:26 08/05195 ANM
I Fluorcne IJ D 5000 ppb EPA 8270 06:26 08/05195 ANM I Hcxachlorobenzene UD 5000 ppb EPA8270 06:26 08/05195 ANM
Hcxachlorobutadicnc i; D 5000 ppb EPA8270 06:26 08/05195 ANM I I Hexachlorocyclopentadiene UD 5000 ppb EPA 8270 06'.26 08/05/95 ANM
Hexachloroethane UD 5000 ppb EPA R270 06:26 0810S/95 ANM
I lndcno( 1,2,3 -<:d)pyrene UD 5000 ppb EPA8270 06:26 0810S/95 ANM I Isophoronc UD 5000 ppb EPA8270 06:26 08/0S195 A.'™
N-Nitroso-di-n-propylamine UD 5000 ppb EPA 8270 06:26 08105/95 ANM I N-Nitrosod!phenylnminc UD sooo ppb EPA8270 06:26 08105!95 ANM I NaphU1akue 1900 DJ 5000 ppb EPA 8270 06:26 08/0S/9S ANM
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Bulk Group 22
Bulk Group Deseription: Organie Flammable
Neutral Liquid
* Note: Bulk Groups were named aeeordiug to preliminary hazardous
eategorization test and may not eorrespond to what the material
was classified as for disposal.
AUG 10 '95 15:26 TO 3911147
I
1.,7,,~
\):} .AquaChem I ENVIRONMENTAL LABORATORIES, INC,
I
11178 Downs Road ·
Pineville, NC 28134
704/588-5076
FAX 704/588·2454
FROM AquaCnem Enuir. Lab T-338 P.02
I Certificate of Analysis
I Client: OHM Corporation 1"orth Carolina Certification 1"wnber:
2401 Tuckllseegee Road South Carolina Certification Number:
I Charlotte. NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 10-Aug-95
I SDC#: SV203080 Approved By:
Lab ID: AA13851 Robert L. Curry
I Sample ID: BG-22 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
l{}dercent Water 2.77 % 09:00 08/02/95
Arsenic 0.45 D 0.125 mg/L 1311/6010 l0:30 08/03/95
I Barium 28.4 0.5 mg/L 1311/6010 10:55 08/03/95
Cadmium 0,90 0.05 mg/L 1311/6010 10:45 08/08/95
Chromium 4.75 0.25 mg/L 1311/6010 10:4S 08/08/95 I Lead 0.48 0.25 mg/L 1311/6010 10:45 08/08/95
Mercury 0.098 0.004 mg/L 1311/6010 08:30 , 08/10/95
I Selenium · u 0.025 mg/L 1311/6010 14:20 08/03/95
Silver u 0.05 mg/L 1311/6010 10:45 08/08/95
Total Dissolved Solids 3,000,000 62 ppm EPA 209A 14:00 08/03/95 I Total Organic Carbon (TOC) 850000 ppm EPA 415.1 13:00 08/03/95
1, 1, 1,2-Tetrachloroethane UD 50000 ppb EPA 8240 13:07 08/02/9S
I I, I, I-Trichloroethane 2,800,000 D E 50000 ppb EPA 8240 13:07 08/02/9~
l, 1,2,2-Tetrachloroetbanc UD 50000 ppb EPA 8240 13:07 08/02/95
1, 1,2-Trichloroethane UD S0000 ppb EPA 8240 13:07 08/02/95
I 1.1-Dichloroethane UD S0000 ppb EPA 8240 IJ:07 08/02/95
I, 1-Dichloroethcne UD 50000 ppb EPA 8240 13:07 08/02/95
I 1,2-Dichloroethane UD S0000 ppb EPA8240 13:07 08/02/95
1,2-Dichloropropane UD 50000 ppb EPA 8240 13:07 08/02/95
1: · >Butan0ne 150,000 D 60000 ppb EPA 8240 13:07 08/02/95 I\__, '
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305
99032
Analyst
JCH
RCD
RCD
RCD
RCD
RCD
KRR
RCD
RCD
DLC
JCH
ANM
ANM
ANM
Al'<'M
ANM
ANM
ANlvl
ANM
ANM
AUG 10 '35 15:27 TO 3311147
I
-'"'•~ ' ··<· AquoChem I ~ ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downs Road
Pineville, NC 28134
7041588-5076
FAX [phone]
FROM AquaChem Enuir. Lab T-338 P,83
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
I Charlotte, 1'iC
Client#: 3080 Received Date: 27•Jul-Y5
Contact: Mr. Randy Bennett Report Date: 10-Aug-95
I SDG II: SV2030BO Approved By:
Lab ID: AA13851 Robert L. Curry
I Sample ID: BG-22 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
1•~'.°i)chlorocthylvinyl ether UD 50000 ppb EPA 8240 13:07 08/02/95 '-·,.,, . .
2-Hexanone UD 50000 ppb EPA 8240 13:07 08/02/95
I 4-Methyl-2-pentanone 500,000 D 50000 ppb EPA 8240 13:07 08/02/95
Acetone UD 85000 ppb EPA 8240 13:07 08/02/95
Benzene S0,000 D 95000 ppb EPA 8240 13:07 08/02/95 I Bromodichloromethane UD 50000 ppb EPA 8240 !3:07 08/02/95
Bromofonn UD 50000 ppb _EPA 8240 13:07 08/02/95
I Bromomethane UD 50000 ppb EPA 8240 13:07 08/02/95.
Carbon disulfide UD 50000 ppb EPA 8240 13:07 08/02/95
Carbon tetrachloride UD 50000 ppb EPA 8240 13:07 · 08/02/95 I Chlorobenzene UD 50000 ppb EPA 8240 13:07 08/02/95
Chlorodibromomethane UD 50000 ppb EPA 8240 13:07 08/02/95
I Chlo,oethane UD 50000 ppb EPA 8240 13:07 08/02/95
Chloroform UD 50000 ppb EPA 8240 13:07 08/02/95
Chloromethane UD 55000 ppb EPA 8240 13:07 08/02/95
I cis~ l ,2~Dichloroethene UD 50000 ppb EPA 8240 13:07 08/02/95
cis-1,3-Dichloropropene UD 50000 ppb EPA 8240 13:07 08/02/95
I Ethylbenzene 1,400,000 DE 50000 ppb EPA 8240 13:07 08/02/95
Strycnc 190,000 D 50000 ppb EPA 8240 13:07 08/02/95
: . · · ,tracblorocthene UD 50000 ppb EPA 8240 13:07 08/02/9S l"j
I
305
99032
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A.NM
Ai"IM
ANM
ANM
A."IM
Ai"IM
ANM
ANM
ANM
AUG 10 '95 15:28 TO 3911147
I
•-~ -:{/ AquaChem I l:. ENVIRONMENTAL LABORATORIES, INC.
I
11176 Down• Ro&d
Plnevlllo, NC 28134
704/588-5078
FAA 7041588•2454
FROM AquaCnem Env,r. Lab T-338 P.04
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certiflcadon Number:
240 I Tuckaseegee Road South Carolina Certlffcallon Number:
I Charlotte, NC ?-
Clienl #: 3080 Ri!ceived Datt: 27-Jul-95
Contac1: \fr. Randy Bennett Report Date: 10-Ang-95
I SDG#: SV203080 Approved By:
Lab ID: AAl3851 Roben L. Curry
I Sample ID: BG-22 Project Manager
De1ection
Parameter Result Limit Unit l\lethod Time Date 1«".'.\ 520,000 D 50000 ppb 13:07 08/02/95 <~>·olucnc_ EPA 8240
Total Xylcnes 7,300,000 DE 50000 ppb EPA 8240 13:07 08/02/95
I trans-I ,2-Dichloroethene UD 50000 ppb EPA 8240 13:07 08/02/95
trans-1,3-Dichloropropene UD 50000 ppb EPA 8240 13:07. 08/02/95
Tri,:hloroethcnc UD 50000 ppb EPA 8240 13:07 08/02195 I Vinyl chloride UD 50000· ppb EPA 8240 13:07 08/02/95
1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 13:05 08/02/95
I 1,2-Dichlorobenzene UD 1000 ppb EPA 8270 13:05 08/02/95
1,3-Dichlorobenzene UD 1000 ppb EPA8270 13:05 08/02/95
1, 4-Dichlorobenzene UD 1000 ppb EPA 8270 13:05 08/02/95 I 2,45-Trichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
2,4,6-Trichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
I 2, 4-Dichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
2,4-Dimethylphenol UD 1000 ppb EPA 8270 13:05 08/02/95
2,4-Dinitrophenol UD 1000 ppb EPA 8270 13:05 08/02/95
I 2,4•Dinitrotoluene UD !000 ppb EPA 8270 13:0S 08/02/95
2,6•Dinitrotoluenc UD 1000 ppb EPA 8270 13:05 08/02/95
I 2-Chloronaphthalene UD 1000 ppb EPA 8270 13:05 08/02/95
2-Chlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
, . :-Methylnaphthalene .,,-/ UD 1000 ppb EPA 8270 13:05 08/02/95
I
305
99032
Analyst
A.'IM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A.\/M
ANM
ANM
ANM
AUG 10 '95 15:28 TD 39:1147
I
1---~ :, ••·· ~ >1
· ;.· .. A.quaChem I . (.:. ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downe Road
Plnevllle, NC 28134
704/588-5078
FAX [phone]
FROM AquaChem Eooir. Lab T-338 P.05
I Certificate of Analysis
I Client: OHM Corporation North Carolina Ccrtif'ication Numbu:
2401 Tuckaseegee Road South Carolina Certification Number:
I Charlotte, NC
Client Ir. 3080 Received Date: 27-Jul-95
Cootaci: Mr. Randy Bennett Report Date: I0,Aug-95
I SDG#: SV203080 Approved By:
Lab ID: AA138Sl Robert L. Curry
I Sample ID: BG-22 Project M1U1•ger
Detection
Parameter Result Limit Unit Method Time Date
l>J-Methylphenol (o-cresol) UD 1000 ppb EPA 8270 13:05 08/02/95
2-Nitroanillne UD 1000 ppb EPA 8270 13:05 · 08/02/95
I 2-Nitrophenol UD 1000 ppb EPA 8270 13:05 08/02/95
3-Nitroanilinc UD 1000 ppb EPA 8270 13:05 08/02/95
4,6-Dinitro-2-methylphenol UD 1000 ppb EPA 8270 13:05 08/02/95 I 4,6-Diuitro-o-.:resol UD 1000 ppb EPA 8270 13:0S 08/02/95
4-Bromophenyl phenyl ether UD 1000 ppb EPA 8270 13:05 08/02/95
I 4-Chloro-3-methylphenol UD 1000 ppb EPA 8270 13:05 08/02/95
4-chloroanilinc UD 1000 ppb EPA 8270 13:05 . 08/02/95
4-Chlorophenyl phenyl ether UD 1000 ppb EPA 8270 13:05 08/02/95
I 4-Methylphenol (p-cresol) UD IO00 ppb EPA 8270 13:05 08/02/95
4-Nitroaniline UD IO00 ppb EPA 8270 13:05 08/02/95
I 4-Nitrophenol UD 1000 ppb EPA 8270 13:05 08/02/95
Acenaphthene UD 1000 ppb EPA 8270 13:05 08/02/95
Acenaphthylene UD 1000 ppb EPA 8270 13:05 08/02/95
I Benzo(a)anthracene UD 1000 ppb EPA 8270 13:05 08/02/95
Benz.o(a)P)TODO UD 1000 ppb EPA 8270 13:05 08/02/95
I Benzo(b )fluoranthenc UD 1000 ppb EPA 8270 13:05 08/02/95
Benzo(ghl)perylene UD 1000 ppb EPA 8270 13:05 08/02/95
. .. · 3cnzo(k)fluora.nthene UD 1000 ppb EPA 8270 IJ:05 08/02/95 .\~/ '
I
305
99032
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 10 '95 15:29 TO 3911147
I
•---~ . \(: · .AquaChem . I l.:. ENVIRONMENTAL LABORATORIES, INC.
11176 Downo Road
Plnevllle, NC 28134
704/588-5076
FAX [phone]
FROM AquaChem Envir, Lab ___ T.:...-...:3:.:3c:8..:P..:·...:0;.:6 ______ _
I
I Certificate of Analysis
I Client: Om..! Corporation
2401 Tuckasecgee Road
I Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
I SDG#: SV203080
Lah ID: AAl385l
I Sample ID: BG-22
Detection
Parameter Resuh
·~~3is(2-chloroelhoxy) methane UD
Limit
1000
Bis(2-chloroelhyl) ether VD 1000
I Bis(2-chloroisopropyl) ether UD
Bis(2-cthylhcxyl) phlhalate UD
1000
1000
I Butyl benzyl phthalate UD
Chrysene VD
l000
1000
Di-n-butyl phthalate VD 1000
I Di-n-octyl phthalate VD
Dibenzo(ah)anthracenc VD
1000
1000
Dibenzofuran VD I Diethylphthalate VD
1000
1000
Dimethylphthalatc UD 1000
I Fluoranthene VD
Fluorene VD
1000
1000
Hex:ichlorobenzene VD 1000 I Hexachlorobutadiene UD 1000
Hcxachlorocyclopenladicne UD 1000
I Hexachloroethane UD
lndcno( 1,2,3-cd)pyrene VD
1000
1000
:: · ·: )ophorone 1---VD 1000,
I
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: 10-Aug-95
Approved By:
Robert L. Curry
Project Manager
Method lime Date Analyst
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 · 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 A.t'-M
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 A.,',M
EPA 8270 IJ:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:0S 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA8270 13:05 08/02/95 ANM
I
HUG 10 '95 15:30 TO 3911147 FROM Aqc•Chem Env(r. l•b T-338 P.07
I. )1_
l:::~~~~o~~A~~BORATOR1es, INC.
11176 Downs Road
I Plnavllla, NC 2813-4
704/588-5078
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation
I Client#:
240 I Tuckaseegee RDad
Charlotte, NC
Contact:
I SDG#:
Lab ID: I So.mpleID:
3080
Mr. Randy Bennett
SV203080
AA13851
BG-22
Parameter
l.:f,-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
I Naphthalene
Nitrobenzene
I Pentnchlorophenol
Phenanthrene
Phenol
I Pyrene
Total Suspended Solids
Total Organic Halide (TOX) I BTU
Flash Point
I
Resuh
UD
UD
UD
UD
UD
UD
UD
UD
300,000
u
15420
74
4.27
Detection
Limit Unit
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
I ppm
1.0 ppm
BTU/gal
70 Deg. F
0-14 SU
North Carolina Certification Number: 305
South Carolina Certiflcadon Number: 99031
Received Date:
Report Date:
27-Jul-95
10-Aug-95
Appro,i,d By: _________ _
RobenL. Curry
Project Muager
Method Time Date Analylt
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 B:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
SM209C 13:30 08/03/95 DLC
SM506 14:00 08/04/9.l /CH
SW-846 #909 08:00 08/02/95 /CH
SW-846 #909 10:15 08/10/95 KRR
SW846 9045 10:00 08/10/9.l KRR
I
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I
I
I
I
I
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I
* Note:
Bulk Group 15
Bulk Group Deseription: Sulfides
Bulik Groups were named aeeording to preliminary hazardous
eategorization test and may not correspond to what the material
was classified as for disposal.
I
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I
I
I
I
I
I
I
I
I
I
I
I • ·.1
\:_jl
l"r<Ul'l Hq~em 1:.nu l('. LcHl
Certificate of Analysis
Client: OHM Corporation
2401 Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG#: SV533080
Lab ID: AA13965
Sample ID: BG-15
Para.meter
Arsenic
Bariwn
Cadmiwn
Chromium
Lead
~ercury
Selenium
Silver
1,1-Dichloroethylene
1,2-Dichloroethanc
1,4-Dichlorobcnzcne
Benzene
Carbon tetrachloride
Chlorobcnzcnc
Chloroform
Methyl ethyl ketone·
Tetrachloroethylene
Trichloroclhylcoe
Vinyl chloride
2,4,S-Trichlorophcnol
~It
u
0.2
u
2000D
u
u
u
u
u.
u
u
u
u
u
u
0.450 E
u
u
u
u
Detection
Limit Unit
0.005 mg/L
0.1 mg/L
0.05 mg/L
250 mg/L
0.25 mg/L
0.0002 mg/L
0.005 mg/L
0.0S mg/L
0.005 ntg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
0,005 mg/L
0.005 mg/L
0.005 mg/L
0.005. mg/L
0.02 mg/L
North CarolinK Certl!lcatlon Number: 305
South Carolina Certlflcatlon Number: 99032
Received Date:
Report Date:
02-Aug-95
23-Aug-95
Appro,·ed By: _________ _
Robert L. Curry
Project Manager
Method Time Date Analyst
. 1311/6010 11:25 08/16/95 RCD
13lli6010 09:40 08/16/95 ·RCD
1311/6010 10:45 08/08/95 RCD
1311/6010 10:05 08/14/95 RCD
. J311160l0 10:45 08/08/95 RCD
1311/6010 08:10 08/16/95 RCD
1311/6010 12:30 08/16/95 RCD
1311/6010 10:45 08/08/95 RCD ' 1311/8260 23:51 08/16/95 DLC
1311/82fi0 23:51 08/16/95 DLC
1311/8260 23:51 08/16/95 DLC
1311/8260 23:51 08/16/95 DLC
1311/8260 23:51 Ul!/16/95 DLC
1311/8260 23:51 08/16195 DLC
1311/8260 23:51 08/16/95 DLC
1311/8260 23:51 08/16/95 DLC
1311/8260 23:51 08/16/95 DLC
~311/8260 23:51 08/16/95 DLC
1311/8260 23:51 08/16/95 DLC
1311/8270 20:13 08/10/95 ANM
I
Is"'
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I
.,.., ... "'-J .. .., .. ..., .... .., ,..., .., ........... , I 1'-VI I n"IY'-''-'''-"' ,_,,v ,, o '-'-""' I __,..,, I • ._..
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegce Road
Charlotte. NC
Client#: ]080
Contact: Mr. Randy Bennett
SDG#: SVS33080
Lab ID: AAl3965
Sample ID: BG-15
Parameter Result
2,4,6-TricWorophenol u
2,4-Dinitrotoluene u
Hexachlorobenzene u
Hexacblorobutadienc u
Hexacbloroethane u
m-Crcsol 0.011 J
Nitrobenzene u
o-Cresol 0.012 J
p-Cresol 0.012 J
Pentachlorophcnol u
Pyridine:: u
Sulfide PENDING
Total Organic Carbon (TOC) 1400
Total Organic Halide (TOX) <JO
Paint Filter Negative
Re.ctivity PENDING·
BTU ✓-1000
Flash Point <80
PH 7.H7
Detection
Limit Unit
0.02 mg/L
0.02 mg/L
0.02 mg/L
0.02 m~
0.02 mg/L
0.02 m~'L
0.02 m~'L
0.02 mg/L
0.02 mg/L
0.02 m~'L
0.02 mg/L
-0-ppm
I ppm
1.0 ppm
-0--0-
-0--0-
-0-□TU/gal
80 Deg.F
0-14 SU
North Carolina Certification Swnber: 305
Sonth Carolina Certification Nwnber: 99032
Rfcelved Date: 02-Aug-95
Reporc Date: 23-Aug-95
Approved By:
Robcn L. Curry
Project Manager
MetbOd Time Date Analyst
1311/8270 20:13 08/10195 ANM
131118270 20:13 08/10/95 .ANM
131118270 20:13 08/10/95 ANM
1311/8270 20:13 08/10195 ANM
1311/8270 20:13 08/10/95 ANM
1311/8270 20:13 08i10l9S ANM
1311/8270 20:13 08/10/95 ANM
1311/8270 20:13 08/10/95 ANM
1311/8270 20:13 08/10/95 ANM
1311/8270 20:13 08/10/95 . ANM
1311/8270 20:13 08/10/95 ANM
EPA 376. l -0· -0--0-
EPA 415.1 13:00 08/17/9:l JCH
SM506 13:00 08117/95 RCD
SW846 10:55 08/18/95 RCD
SW-846117.3 -0--0--o-
SW-846 11909 13 :OO 08/17/95 RCD
SW-846 #909 08:30 08/15/95 RCD
SW846 9045 09:20 08117/95 RCD
I
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Bulk Group 21
Bulk Group Description: Flammable Organic
Neutral Liquid
* Node: Bulk Groups were named aeeording to preliminary hazardous
categorization test and may not correspond to what the material
was classified as for disposal.
I
lr1,,
(-•. .::-1 I
I i!\~!!~!?~.~~'°"'°"'"· '"' 11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I
I
I
I
I
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: · Mr. Randy Bennett
SDG#:
Lab ID:
SR633080
AAll900
Sample ID: BG-21
Parameter JJ ·; Percent Water
Arsenic
Barium
Cadmium I
I
I
I
I
I
Chromium
Lead
Mercury
Selenium
Silver
Total Dissolved Solids
Total Organic Carbon (TOC)
I, I, 1,2-Tetrachloroethane
I, 1,1-Trichloroethane
I , 1,2 ,2-Tetrachloroethane
I, 1,2-Trichloroethane
1,1-Dichloroethane
I, 1-Dichloroethene I 1,2-Dichloroethane
•.,. 1,2-Dichloropropane -.. , I
( ·' 2-Butanone
I
Result
8.70
0.013
18.9D
1.65
1.10.
48.1
UD
u
0.10
14300
115,000
u
u
u
u
u
u
u
u
130,000 D
Detection
Limit
0.025
0.5
0.05
0.25
0.25
0.002
0.025
0.05
10000
10000
20000
10000
10000
20000
10000
10000
24000
Unit
%
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ppm
ppm
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: 12-Jun-95
Approved By: ~
R~ .Curry
Method
1311/6010
1311/6010
1311/60!0
1311/60!0
13 I 1/60!0
1311/6010
1311/6010
1311/60!0 .
EPA 209A
EPA 415.1
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
Project Manager
Time
17:00
13:45
14:50
17:43
17:43
17:43
10:30
15:00
17:43
16:25
17:00
21:42
21:42 ·
21:42
21:42
21:42
21:42
21:42
21 :42
21 :42
Date.
05/30/95
05130/95
Analyst,
JCH
KRR
06/01/95 · .. RCD
06/01/95 RCD
06/01/95 R<;D
06/01195
06/02/95
05/30/95
06/01/95
05/30/95
05/30/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
RCD
TML
KRR
RCD
RCD
JCH
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
I
1
1
fJ)J lA~~~o5~,~~,oSAn>m, '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076 I F'AX 704/588-2454
I
I
I
I
Certificate of Analysis
I
Client:
Client#:
Contact:
SDG#:
Lab ID:
OHM Corporation
2401 Tuckaseegee Road
Charlotte, NC
3080
Mr. Randy Bennett
SR633080
AAll900
Sample ID: . BG-21
Parameter Result
Detection
Limit I© • ) 2-Chloroethylvinyl ether
2-Hexanone
u
u
u
20000
10000
20000
32000
10000
10000 .
10000
20000
20000
10000
10000
20000
20000
10000
40000
10000
10000
I 4-Methyl-2-Pentanone
Acetone u
u
u
u
u
u•·
u
u
u
u
u
u
u
u
Benzene I Bromodichloromethane
I
I
I
I
I
0 I
I
Bromoform
Bromomethane
Camon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
· Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
,. Ethylbeilzene~,s-=i'F:iff7i/'.'Zei?fi""50<i"ii6oi>'?:fil0000 ~~t.~:-~:~'l;i'~,'.-,?-i~ .. ~:~i~::tlt'l.ij;:_;,,:~1:.:.:.c!:~,!-::.-~~~~.,
Methylene chloride U 28000
) Stryene U 20000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Dat~:
24-May-95
12-Jun-95
/ ~~ Approved By: / C-?L, <......, -R~S:,c.~y. "'c=ur"ry.-c....,~=,::~_-),,..._ -
Method
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA_ 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
Project Manager
Time
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21:42
21 :42
21:42
21:42
21:42
21:42
21:42
21:42
Date
05/31/95
05/31/95
0_5/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/3 i/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
Analyst
DLC
DLC
DLC
DLC
DLC .
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
I
le-,
·:'/'.:."/
I
I
\ lA~~~E,~.~~•omos,es, "'
11176 Downs Road
Pineville, NC 28134
7041588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
11 Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Dat~: 12-Jun-95
Rtffif ~ , "z,··· I SDG#: SR633080 Approved By:
Lab ID: AA! 1900
I Sample ID: BG-21 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst.
IC) 1l£etrachloroeilieii'e~Ji.@¼~22~00 ~ 10000 ppb EPA 8240 21:42 05/31/95 DLC t:> .. "."'"-.:..==:... . ..-.-:-::-.. ~ ,,,6'$.::~~;'.E-?:';~.:1£,~~5::£::i':1~~·-~~-·-
~T&~f~~£I~~~lilll~,i~f~W10000 ppb EPA 8240 21:42 05/31/95 DLC
I /!ZJ£tal'2.CyleQ~1~~:~~~~-,;,.'{l;}\J,0s:~9.~Jl D 10000 ppb EPA 8240 21:42 05/31/95 DLC •--',.•••V • •· ....... -•~•••-~M•~•-•••------
trans-1,2-Dichloroethene u 10000 ppb EPA 8240 21:42 05/31/95 DLC
I trans-1,3-Dichloropropene u 10000 ppb EPA 8240 21:42 05/31/95 DLC
Trichloroethene u 10000 ppb EPA 8240 21:42 05/31/95 DLC
Vinyl chloride u 20000 ppb EPA 8240 21:42 05/31/95 DLC
II 1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
1,2-Dichlorobenzene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
1,3-Dichlorobenzene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM I 1,4-Dichlorobenzene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
2,4,5-Trichlorophenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I 2,4,6-Trichlorophenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
2,4-Dichlorophenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I 2,4-Dimethylphenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
2,4-Dinitrophenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
2,4-Dinitrotoluene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM I 2,6-Dinitrotoluene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
(;<) ) 2-Chloronaphthalene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM I'-'-' · 2-Chlorophenol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I
I
.(?:'!.
I
I
l A~~~o~,~.~~aomoa,es, ""
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
Client: OHM Corporation I 240 I Tuckaseegee Road
Charlotte, NC
I
I
I
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
3080
Mr. Randy Bennett
SR633080
AAll900
BG-21
lcD ! 2-Methylnaphthalene
2-Methylphenol (o-cresol)
I
I
I
I
I
I
2-Nitroaniline
2-Nitropheriol
3,3-Dichlorophenol
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4,6-Dinitro-o-cresol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-chloroaniline
4-~hlorophenyl phenyl ether
4-Methylphenol (p-cresol)
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene I Benzo(a)anthracene
. :·--.) . Benzo(a)pyrene
···.._c,') Benzo(b)fluoranthene
I
Result
UD
UD
UD
UD
UD
UD
UD
UD
.. uo··
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date_: 12-Jun-95
Approved By: -~-,--=· .. •· ..,··~'--'-....._-•'"''=-'"'·~-R~{ oi; 0
Project Manager
Method Time Date . Analyst,
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ·. ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM •.
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM.
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31/95 ANM
EPA 8270 15:04 05/31195 ANM
EPA 8270 15:04 05/31/95 ANM
I
I,= /A~~:;.,5!'.'z~,omos,es, '" ·-:-\?,} . 1 -~-
I 11176 Downs Road
Pineville, NC 28134
704/588-5076
I FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: ~--. Lab ID: AAll900 R~~ •Curry ,3
I Sample ID: . BG-21 Project Manager
Detection
Paramet_er Result Limit Unit Method Time Date Anal~·st 12' ) ) Benzo(ghi)perylene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Benzo(k)fluoranthene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I Benzoic acid UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Benzyl alcohol UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I
Bis(2-chloroethoxy) methane UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Bis(2-chloroethyl) ether UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Bis(2-chloroisopropyl) ether UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I Bis(2-cthylhexyl) phthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Butyl benzyl phthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM ' Chrysene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM I Di-n-butyl phthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Di-n-octyl phthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I Dibenzo(ah)anthracene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Dibenzofuran UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I Diethylphthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Dimethylphthalate UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
Fluoranthene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I_ Fluorene UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
-Hexachlorobenzene UD 1000 ppb EPA 8270 15:04 05/31/95 , ANM .. i
) Hexachlorobutadiene Iv' UD 1000 ppb EPA 8270 15:04 05/31/95 ANM
I
'
I
I
I
I
I
I
I
17'.:.; :.,x_;l
I
I
I
I
I
I
\ lA~!!~oE~,~~'°'"°""· '"' 11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG#: SR633080
Lab ID: AA11900
Sample ID: . BG-21
Parameter
:1 Hexachlorocyclopentadiene
Hexachloroethane
Indeno( 1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylarnine
Naphthalene
Nitro benzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Total Suspended Solids
Total Organic Halide (TOX)
BTU
Flash Point
pH
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
386000
u
14100
>220
8.70
Detection
Limit
l000
l000
l000
l000
l000
l000
l000
1000
l000
l000
l000
l000
1.0
70
0-14
Unit
ppb
ppb
ppb
'ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppm
ppm
BTU/gal
Deg. F
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Dat_e:
Approved By:
Method
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
SM209C
SM506
SW-846 #909
SW-846 #909
SW846 9040
24-May-95
12-Jun-95
R'll:~f
Project Manager
Time Date Analyst
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05131/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
15:04 05/31/95 ANM
10:00 05/29/95 TML
17:00 05/30/95 JCH
17:00 05/30/95 JCH
10:00 05/30/95 TML
08:20 05/30/95 RCD
HULJ J.l::'J '':1:::1 l:'l:.i:.'b IU ,S'jlll4"f FROM AquaC.,em Envir. Lab T-338 P.02
I
•
I"'>-~ ';:::a l, Aqua Chem I . ENVIRONMENTAL LABORATORIES, INC. 11176 Downs Road
Pineville, NC 28134
I 7041588•5076
FAX [phone]·2454
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305 2401 Tuck;,seegee Road South Carolina Certification Nnmber: 99032 Charlotte, NC
I Client II: 3080 Received Date: 27-Jul-95 Contact: Mr. Randy Bennett Report Date: IO•Aug-95
I soc#: SV203080 Approved By:
Lab ID: AA138SJ Robert L. Curry I SamplelD: BG-22 Project Manager
Detection
Parameter Reslllt Limit Unit Method Time Date Analyst t ·'\ 2.77 % 09:00 08/02/95 JO!
· :: -·ercent Water -::.;..,~
Arsenic• 0.45D 0.125 mg/L 1311/6010 I0:30 08/03/95 RCD.
I Barium 28.4 0,5 mg/L 1311/6010 10:55 08/03/95 RCD Cadmium 0.90 0,05 mg/L 1311/6010 10:45 08/08/95 RCD Chromium 4.75 0.25 mg/L 1311/6010 10:45 08/08/95 RCD I Lead 0.48 0,25 mg/L 13ll/6UIU 10:45 08/0H/95 RCD
Mercuzy 0.098 0,004 mg/L 1311/6010 08:30 08/10/9S I<RR
I Selenium· u 0.025 mg/L 1311/6010 14:20 08/0319S RCD Silver u 0.05 mg/L 1311/6010 10:45 08108/95 RCD
Total Dissolved Solids 3,000,000 62 ppm EPA209A '14:00 08/03/95 DLC I Total Organic Caibon (TOC) 850000 ppm EPA 415.l 13:00 08/03/95 JQI 1,1,1,2-Tetrachloroethane UD 50000 ppb EPA 8240 13:07 08/02/95 ANM 1, l, I· Trichloroethane 2,800,000 D E 50000 ppb EPA 8240 13:07 08/02/95 ANM I l, 1,2,2-Tetrachloroethanc UD 50000 ppb EPA 8240 13:07 08/02/95 ANM I, 1,2-Trichloroethane UD 50000 ppb EPA 8240 13:07 08/02/95 ANM
I I, 1-Dichloroethane UD 50000 ppb EPA 8240 JJ:07 08102195 ANM I, 1-Dichloroethenc UD 50000 ppb EPA 8240 13:07 08/02/95 ANM 1,2-DichJoroethane UD 50000 ppb EPA8240 13:07 08/02/95 ANM I 1,2-Dichloropropane UD 50000 ppb EPA 8240 13:07 08/02195 A.'<M ':',-Butan0ne 150,000 D 60000 ppb EPA 8240 13:07 08/02/95 ANM '-> : I
I
AUG 10 '95 15:27 TO 3911147
I
I,\ Jf_
,
2
~'i~~O~~A~~BORATORIES, INC,
11178 Downs Road
I
Plnevllle, NC 28134
704.'588-5076
FAX [phone]
FROM AquaChem Enuir, L•b T-338 P.m
•
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
I Client#:
Charlotte, NC
3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 10-Aug-95
I SDG#: SV203080 Approved By:
Lab ID: AAl3851 Robert L. Curry I Sample ID: BG-22 Project Manager
Defection
Parameter Result Limit Unit Method Time Date
l}'Jchlorocthyhinyl ether UD 50000 ppb EPA 8240 13:07 08/02/95
2-Hexanone UD 50000 ppb EPA 8240 13:07 08/0219S
I 4-Methyl-2-pentanone 500,000 D 50000 ppb EPA 8240 13:07 08/02/9S
Acetone uo 85000 ppb EPA 8240 13:07 08/02/95
Benzene S0,000O 9S000 ppb EPA 8240 13:07 08/02/95 I Bromodichloromethane UD 50000 ppb EPA 8240 13:07 08/02/9S
Bromoform UD 50000 ppb .EPA 8240 13:07 08/02/95
I Bromomcthane UD 50000 ppb EPA 8240 13:07 08/02/95
Carbon disulfide UD 50000 ppb EPA 8240 13:07 08/02/95
Carbon tetrachloride UD 50000 ppb EPA 8240 '13:07 08/02/9S
I Chlorobenzene UD 50000 ppb EPA 8240 13:07 08/02/95
Chlorodibromomethane UD 50000 ppb EPA 8240 13:07 08/02/95
I Chloroethane UD 50000 ppb EPA 8240 13:07 08/02/95
Chloroform UD 50000 ppb EPA 8240 13:07 08/02/95
Chloromethane UD S5000 ppb EPA 8240 13:07 08/02/95
I cis~l12~Dichloroethene UD 50000 ppb EPA 8240 13:07 08/02/95
cis-1,3-Dichloropropene UD 50000 ppb EPA 8240 13:07 08/02/95
I Ethylbenzene 1,400,000 DE 50000 ppb EPA 8240 13:07 08/02/95
Strycnc 190,000 D soooo ppb EPA 8240 13:07 08/02/95
;trachlorocthene UD 50000 ppb EPA 8240 13:07 08/02/95 ,~ '
I
305
99032
Analyst
ANM
ANM
ANM
A..'IM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A,','M
A..'IM
ANM
ANM
A.'IM
ANM
ANM
ANM
A.'-M
I
I,,,~
{f/' Aqua Chem I l:. ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downs Road
Pineville, NC 28134
704/588-5078
FAX 704/588•2454
rt<.Jl'I Hquai...:1em c.n_v \r. L~o 1-.J.JO r-, l(J"-o
I Certificate of Analysis
I Client: OHM Corporation Nonh Clll'Ollna Certlficadon Number:
2401 Tuclcaseegee Road South Carolina Certification Number:
I Client#:
Charlotte, NC
3080 Received Dau: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 10-Aug-95
I SDG#: SV20JOBO ApprO\·ed By:
Lab ID: AA13851 Roben L. Curry I SampleID: BG-22 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
f)oluenc 520,000 D 50000 ppb EPA 8240 13:07 08/02/95
Total Xylcnes 7,300,000 DE 50000 ppb EPA 8240 13:07 08/02/95
I trans-1,2-Dich!oroethene UD 50000 ppb EPA 8240 13:07 08/02/95
trans-1,3-Dichloropropene UD 50000 ppb EPA 8240 13:07 08/02/95
Trichloroethcne UD 50000 ppb EPA 8240 13:07 08/02/95
I Vinyl chloride UD 50000 ppb EPA 8240 13:07 08/02/95
.1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 13:05 08/02/95
I 1,2-Dicblorobenzene UD 1000 ppb EPA8270 13:05 08/0219S
1,3-Dichlorobcnzcne UD 1000 ppb EPA 8270 13;05 08/02/95
1,4-Dichlorobenzene UD 1000 ppb EPA 8270 ' 13:05 08/02/95
I 2,4,;. Trichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
2,4,6-Trichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
I 2, 4-Dichlorophenol UD 1000 ppb EPA 8270 13:05 08/02/95
2,4-Dimethylphenol UD 1000 ppb EPA 8270 13:0S 08/02/95
2,4-Dinitrophenol UD 1000 ppb EPA 8270 13:0S 08/02/9S
I 1,4•Dinitrotoluene UD !000 ppb EPA 8270 13:05 08/0219, .
2,6-Dinitrotolucnc UD 1000 ppb EPA 8270 13:05 08/02/95
I 2-Chlorcnaphthalene UD 1000 ppb EPA 8270 13:0S 08/02/95
2-Chlorcphenol UD 1000 ppb EPA 8270 13:05 08/02/9S
: ,-Methylnaphthalene UD 1000 I'-'/ ppb EPA 8270 13:05 08/02/95
I
305
99032
Analyst
A..'1/M
ANM_
ANM
ANM
ANM
ANM
ANM
ANM
A..'IM
A..'1/M
ANM
ANM
\
ANM
ANM
ANM
ANM
A..'IM
A."IM
ANM
ANM
AUG 10 '95.15:28 TO 39:1147
I
I.,~"~
S/ AquaChem I l.:. ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downs Road
Plnevllle, NC 28134
7041588-5076
FAX [phone]
FROl1 AquoChem Eou1r. L•b
I Certificate of Analysis
I Client: OHM Corporation North Cnrolina Ccrtif"lcation Number:
2401 Tuckaseegee Road South Carolina Certification Number:
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: lO•Ang-95
I SDG#: SV203080 Approved By:
Lab ID: AA13851 Robert L. Curry
I Sample ID: BG-22 Project M11Dager
Detection
Parameter Reswt Limit Unit Method Time Date
l\~:)-Methylphenol (o-<:resol) UD 1000 ppb EPA 8270 13:05 08/02195
2-Niuoaniline UD 1000 ppb EPA 8270 13:05 08/02/95
I 2•Niuophenol UD 1000 ppb EPA 8270 13:05 08/02/95
3-Nitroani!inc UD 1000 ppb EPA 8270 13:05 08/02/95
4,6-Dinitro-2-methylphenol UD 1000 . ppb EPA 8270 13:05 08/02/95 I 4,6-Dinitro-o-<;rcsol UD 1000 ppb EPA 8270 13:05 08/02/95
4-Bromophenyl phenyl ether UD 1000 ppb EPA 8270 13:05 08/02195
I 4-Chloro-3-methylphenol UD 1000 ppb EPA 8270 13:05 08/02/95
4-<:hloroanilinc UD 1000 ppb EPA 8270 13:05 08/02/95
4-Chlorophenyl phenyl ether UD 1000 ppb EPA 8270 ' 13:05 08102195
I 4-Methylphenol (p-cresol) UD 1000 ppb EPA 8270 13:05 08/02/95
4-Nitroaniline UD l000 ppb EPA 8270 13:05 08102/95
I 4-Niuophenol UD 1000 ppb EPA 8270 13:05 08/02195
Acenaphthene UD 1000 ppb EPA 8270 13:05 08/02195
Acenaphthylene UD 1000 ppb EPA 8270 13:05 08102195
I Benzo(a)anthracene UD 1000 ppb EPA 8270 13:05 08/02/95
Benzo(a)pyrene UD 1000 ppb EPA 8270 13:05 08/02/95
I Benzo(b )lluoranthcnc UD 1000 ppb EPA 8270 13:05 08102195
Benzo(ghi)pcrylene UD 1000 ppb EPA 8270 13:05 08/02/9S
:· ,'3cnzo(k)lluom,thenc UD 1000 ppb EPA 8270 IJ:05 08/02195 .~ '
I
305
99032
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 10 '95 15:2'3 TD 3911147
I
·•:->-~ ·tt. Aqua Chem I l.:. ENVIRONMENTAL LABORATORIES, INC.
11176 Dcwna Road
Plnevllle, NC 28134
704/588-5076
FAX [phone]
FROM Aq u acne m En v \ r. Lab __ 1c..-..:;_j.;;__jtj;:_/-'.c.· .;;_<lb;:_ _____ _
I
I Certificate of Analysis
I Client: OHM Corporation
2401 Tuckasecgee Road
I Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
I SDG#: SV203080
Lab ID: AA13851
I Sample ID: BG-22
Parameter Result
lf~)is(2-chloroethoxy) methane UD
Bis(2-<:hloroethyl) ether UD
I Bis(2-chloroisopropyl) ether UD
Bis(2-ethylhcxyl) phthalate UD
I Butyl benzyl phthalatc UD
Cluysene UD
Di-n-butyl phthalate UD
I Di-n-octyl phthalate UD
Dibenzo(ah)anthracenc UD
Dibenzofuran UD
I Diethylphthalate UD
Dimcdtylphthalatc UD
I Fluoranthene UD
Fluorcne UD
Hcxachlorobenzene UD
I Hexacblorobutadiene UD
Hexachlorocyclopentadiene UD
I Hexachloroetlume UD
Indcno(l,2,3-cd}pyrene UD
.-. i ; : ·.sophoronc 10• UD
I
Detection
Limit Unit
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
l00Q ppb
North Carolina Certification Number: J05
South Carolina Certification Number: 990Jl
Received Date: 27-Jul-95
Report Date: 10-Aug-9S
Approved By: .
Robert L. Curry
Project Manager
Method lime Date Analyst
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:0S 08/02/95 ANM
EPA 3270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270' 13:05 08/02/9S ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/9, ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/9S . ANM
EPA 8270 13:05 08/02/9S ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 IJ:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA 8270 13:05 08/02/95 ANM
EPA8270 i 13:05 08/02/95 ANM
AUG 10 '95 15:30 TO 3911147
I
:;z:;, L!'~~~!?~!~ ....... ,,,. ,~
11176 Downs Road
Pineville, NC 28134
I 704158&-5076
FAX ~/588-2454
' FROM AqcaChem Env ir. Lob T-338 P.07
I Certificate of Analysis
OHM Corporation I Client:
I Client#:
2401 Tuckaseegee Road
Charlotte, NC
Contact:
I SDG#:
Lab ID:
3080
Mr. Randy Bennett
SV203080
AAl3851
1 Sample ID: BG-22
ParB111eter
IQ-Nitroso-di-n-propylamine
N-Nitrosodiphcnylamine
I
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I
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I
Naphthalene
Nitrobenzene
Pentnchlorophenol
Phenanthrenc
Phenol
Pyrene
Total Suspended Solids
Total Organic Halide (TOX)
BTU
Flash Point
PH
\S! ••
I
ResuH
UD
UD
UD
UD
UD
UD
UD
UD
300,000
u
15420
;4
4.27
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
I
1.0
70
0-14
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppm
ppm
BTU/gal
Deg. F
SU
North Carolina Certification Number: 3-0!1
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: 10-Aug-95
Method
EPA 8270
EPA 8270
EPA 8270
EPA8270
EPA 8270
EPA 8270 ·
EPA 8270
EPA 8270
SM209C
SM506
Robert L. Curry
Project M11nager
Time Date
13:05 08/02/95
13:05 08/02/95
13:05 08/fu/95
13:05 08/02/95
13:05 08/02/95
13:05 08/02/95
13:05 08/02/95
13:05 08/02/95
13:30 08/03/95
14:00 08/04/95
SW-846 #909 08:00 08/02/95
SW-846 #909 10:15 08/10/95
SW846 9045 10:00 08/10/95
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
DLC
!CH
JCH
KRR
KRR
,<Ulj 23 ''35 16; 03 TO 3'3l ll47 FROM AquaCnem Enuir, Lab T-386 P, '.4
I
•-. _;.~·-'~
I
I
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Oien!#: 3080 Received Date: 02-Aug-95
Contact: Mr. Randy Bennett RA!port Date: 23-Aug-95
I SDG#: SV533080 Approved By:
Lab ID: AAIJ956 Robert L. Curry
I Sample ID: BG-36 Project .Manager
Detection
Parameter &suit Limit Unit Method Time Date Analy!t .,,,.,,
Arsenic u 0.02S ppm SW60IO 09:35 08/07/9S RCD _:.:.,j Bariwn 0,5 0,5 SW60IO 09:40 08/16/95 RCD ppm
I Cadmium o.os 0.05 ppm SW6010 10:45 08/08/95 RCD
Chromium u 0.25 PPl\1 SW 6010 I0:45 08/08/95 RCD
Copper 1.75 0.10 ppm SW6010 10:45 08/08/95 RCD
I Iron 109 5 ppm SW6010 08:35 08/08/95 RCD
Lead 0.65 0.25 ppm SW60!0 10:45 08/08/95 RCD
I ;-;ickel 1.35 0.15 ppm SW6010 10:45 08/08/95 RCD
Selenium 0.074 0.025 ppm SW6010 10:50 08/07/95 RCD
Silver u 0,05 ppm SW6010 10:45 08/08/95 RCD
I Zinc 295D 5 ppm SW60IO 10:05 08/14/95 RCD
Mercwy u 0.002 ppm SW7470 08:10 08/16/95 RCD
Aluminium 18 0.5 ppm SW846 6010 08:35 08/16/95 RCD I Antimony u 0.010 ppm SW846 6010 14:40 08/07/95 RCD
Beryllium u 0.05 ppm SW846 6010 08:35 08/08/95 RCD
I Calcium 14.4 0.05 ppm SW846 60!0 08:35 0R/0R/95 RCD
Cobalt 8.40 0.05 ppm SW846 6010 11:30 08/07/95 RCD
Magnesium 3.71 0.05 ppm SW846 60l0 08:35 08/08/95 RCD I Manganese 5.12 0.05 ppm SW846 60l0 08:35 08/08/95 RCD
Potassiwn u 5.0 ppm SW846 6010 12:10 08/07/95 RCD ·-~-'
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HUb 23 •g5 16:04 TD 3glll47 FROM RquaChem Envtr. Lab T-386 P. 15
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number:
2401 Tuckaseegee Road South Carolina Certification Number:
Charlotte, NC
Client Ir. 3080 Rceci,cd Date: 02-Aug-95
Contact: Mr. Randy Bennett Report Date: 23-Aug-95
SDG#: SV511080 Approved By:
Lah ID: AA13956 Robert L. Curry
Sample ID: BG-36 Project Manager
Oetectlon. -----
Parameter Result Limit Unit Method Ti.me Dale
Sodium 81 2.5 ppm SW846 6010 15:30 08/15/95
Thallium u 0.050 ppm SW846 6010 08:40 08/07/95
Vanadium 0.40 0.05 ppm SW846 6010 08:35 08/08195
305
99032
Awilyn
RCD
RCD
RCD
I
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I
I'_~·\ :-; _;,
I
I
I
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I
rr<UM Aqu~Chem En•J Ir. Lab _ _;T_-_::3.;:.8-,;_, .:.p.:.·.;:.1.;:.2 __ _
Certificate of Analysis
Client: . OHM Corporation
240 I Tuckaseegee Road
Charlotte. NC
Client#: 1080
Contact: Mr. Randy Bennett
SDG#: SV533080
Lab ID: AAJ3962
Sample ID: BG-36
Parameter
Oxidation Potential
Percent Water
Total Dissolved Solids
Acidity
Chloride
Nitrate
Nitrite
Total Phosphorus
Sulfate
Total Organic Carbon (fOC)
1.2 .4-Trichlorobenzene
1.2-Dichlorobenzene
1,3-Dichlorobenzcnc
1, 4-Dichlorobenzene
2,4,5-Trichlorophenol
2 ,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimcthylphenol
2.4-Dinitrophenol
2, 4-D initrotol uene
Re.ru.lt
490
5.50
340,000
Can Not Test
Can Not Test
Can Not Test
Can Not Test
Can Not Test
Can Not Test
800,000
u
u
u
u
u
u
u
u
u
u
Detection
Limit Unit
--0-mv
-0-½
62 ppm
--0-ppm ..
-0-ppm
-0-ppm
-0-ppm
--0-ppm
-0-ppm
1 ppm
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
-~000 ppb
5000 ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Date:
Method
. -0-
-0·
EPA 209A
EPA 305.1
EPA325.3
EPA352.l
EPA 354.1
EPA 365.3
EPA 375.4
EPA 415.1
EPA 8270
EPA 8270
EPA 8270
EPA 8270
. EPA 8270
EPA 8270
EPA 8270
),PA 8270
EPA 8270
EPA 8270
02-Aug-95
. 23-Aug-95
Robert L. Cuny
Project Manager
Time Date
13:00 08/17/95
13:00 08/17/95
14:00 08/03/95
--0---0-
--0--0-
-0--0-
--0· -0-
--0---0-
-0--0-
13:00 08/17/95
07:46 08105/95
07:46 08/05/95
07:46 08/05/95
07:46 08105/95
07:46 08/05/95
07:46 08/05/95
07:46 08/05195
07:46 08/05/95
07:46 08/05/95
07:46 08105/95
Analyrt
/CH
/CH
DLC
--0-
-0-
--0-
--0-
--0-
-0-
JCH
A..'IM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
HUll d,j '':I::, Lb:1:::, IU .::i':11114"( t-r<uri HquaChem 1::.nu 1 r. LaO !-.:itff I"', l.:i
I
1,-. ·."•,;·:
I
I
I Certificate of Analysis
I Client: OHM Cu!pOration North Carolina Certificotion Number: 305
240 l Tuckaseegee Road South Carolina Certification Number: 99032
Charlone. NC
I Client#: 3080 Ra:eived Date: 02-Aug-95
Contact: Mr. Randy Bennett Report Date: . 23-Aug-95
I SDG#: SVS33080 Approved By:
Lab ID: AAl3962 Robert L. Curry
I Sample ID: BG-36 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst 1:,:1 2,6-Dinitrotoluene u 5000 ppb EPA 8270 07:46 08/05/95 ANM ~.;/ 2-Chloronaphthalene u 5000 ppb EPA 8270 07:46 08/05/9:l ANM
I 2-Chlorophenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
2-Methylnaphthalene lJ 5000 ppb, EPA 8270 07:46 08/05/95 ANM
2-Methylphenol (o-cresol) u 5000 ppb. EPA 8270 07:46 08/05/95 ANM
I 2-Nitroanilinc u 5000 ppb EPA 8270 07:46 08/05/9:l ANM
2-Nitrophenol u 5000 ppb EPA 8270 07:46 08/05195 ANM
I 3-Nitroaniline u 5000 ppb EPA 8270 07:46 08/05/95 ANM
4,6-Dinitro-2-methylphenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
4,6-Dinitro-o-cresol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
I 4-Bromophenyl phenyl ether u 5000 ppb EPA 8270 07:46 0810S/9S ANM
4-Chloro-3-methylphenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
4-chloroaniline u 5000 ppb EPA 8270 07:46 08/05/95 ANM I 4-Chlorophenyl phenyl ether u 5000 ppb EPA 8270 07:46 08/05/95 ANM
4-Methylphenol (p-cresol) u 5000 ppb EPA 8270 07:46 08/05/95 ANM
I 4-Nitroaniline u 5000 ppb EPA 8270 07:46 08/05/95 ANM
1-Nitrophenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Accnaphlhenc u 5000 ppb EPA 8270 07:46 08/05/95 ANM I ,
Acenaphlhylene u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Benzo(a)anthraccnc u 5000 ppb EPA 8270 07:46 08/05/95 A.."hl .~/
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I
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I
RUG 23 '95 16:lb TD 3911147 l"t<U['l HqU.!IChem t:.:)')lr. LaO r-:scrr P. :_4
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG#: SV533080
Lab ID: AAl3962
Sample ID: BG-36
Plll'amctcr R1:3ult
Benzo(a)pyrene u
Ber.zo(b)fluoranthene u
Bcnzo(ghi)perylene u
Benzo(k)fluoranthene u
Bis(2-ehloroethoxy) methane u
Bis(2-<:hlorocthyl) ether u
Bis(2-<:hloroisopropyl) ether u
Bis(2-etllylhexyl) phthalate u
Butyl bcnzyl phthalalC u
Chrysene u
Di-n-butyl phthalate u
D1-n-octyl phthalate u
Dibenzo(ah)anthracene u
Dibenzofuran u
Diethylphthalate u
Dimethylphthalate u
Fluoranthene u
Fluorenc u
Hexachlorobcnzcne u
Hexachlorobutadiene u
Detection
Limit
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
sooo
5000
5000
5000
Unit
ppb
ppb
ppb
ppb I
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 02-Aug-95
Rt:port Date: . 23-Aug-95
Approved By:
Robert L. Cuny
Project Manager
Method nme Date Analyst
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08105/95 ANM
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 A,','M
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 A.'IM
EPA 8270 07:46 08/05/95 ANM
EPA 82'70 07:46 08/05/95 ANM
EPA 8270 07:46 08/0"9:J ANM
EPA 8270 07:46 08/05/95 A.'IM
EPA 8270 07:46 08/05/95 A.'IM
EPA 8270 07:46 08/0~/95 ANM
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 ANM
EPA 8270 07:46 08/05/95 A.'illl
,EPA 8270 07:46 08/05/95 AN~f
EPA 8270 07:46 08105/9S ANIII
EPA 8270 07:46 08/05/9S M'M
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-;··. i
~•.;_: -
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AUG 23 '95 16:17 TO 3911147 FROM Aqu•Chemc...;::;E __ nu_i;.;.r..;..._L_a_b __ r_-_3_8_7_P_._1_5 ______ _
Certificate of Analysis
Client: OHM Corporation North Cllrollna Certification Number: 305 240 I Tuckaseegee Read South Carolina Certification Number: 99032 Charlotte, NC
Client#: 3080 Received Date: 02-Aug-95 Contact: MI. Randy llennett Report Date: 21-Aug-95
SDG#: SV533080 Approved By:
Lab ID: AA!3962 Roben L. Curry
Sample ID: BG-36 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
Hexachlorocyclopentadiene u 5000 ppb . EPA 8270 07:-lo 08/05/95 ANM
Hexachloroethane u 5000 ppb EPA 8270 07:46 08/05/95 ANM
lndeno( 1,2, 3-cd)p}TCOC u 5000 ppb EPA 8270 07:¼ 08105/95 ANM
lsophorone u 5000 ppb•. EPA 8270 07:46 08/05/95 ANM
N-Nitroso-<li-n-propylarnine u 5000 ppb. · EPA 8270 07:46 08/05/95 ANM
N-Nitrosodiphenylaminc u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Naphthalene u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Nitrobenzene u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Pentachlorophenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Phcrumthrenc u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Phenol u 5000 ppb EPA 8270 07:46 08/05/95 ANM
Pyrene u 5000 ppb EPA 8270 07:46 08/0,/95 ANM
Total Suspended Solids 370,000 I ppm SM209C I 1:30 08/07/95 DLC
Total Orgrutic Halide (TOX) <IO 1.0 ppm SM506 13:00 08/17/95 JCH
Flash Point <80 80 Deg. F SW-846 #<J09 08:30 08/15/95 RCD
pH 1.37 0-14 SU SW846 9040 09:20 08/17/95 RCD
AUG 23 '95 15;17 TO 3911147 FROM Aquacnem t:.n.,:u:.:1.:..r.:.., _:L~•~b:___:..,-.::.:i:=tJ.:.·'..:'"'..:·.:l:.:b _____ _ I
I
·i-<'\:
I
I
I Certificate of Analysis
I Client: OHM Corporation North Carolina Cenifkation Number: 305 240 I Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 02-Aug-95
Contact: Mr. Randy Bennett Report Date: . 23-Aug-95
I SDG#: SV533080 ApproYed By:
Lahm: AA13963 Robert L. Cu!T)'
I Sample ID: BG-36 Project Manager
Detection
Parameter Result Limn Unit Method Time Date Analyst ·-·---.,., I, I, 1,2-Tetrachloroethane u S0000 ppb EPA8240 12:07 08/04/95 DLC . -' · .. ·· ·:
I, I, 1-Trichloroothane u 50000 · ppb EPA 8240 12:07 08/04195 DLC
I I, 1,2,2-Tctrachloroelhanc u 100000 ppb EPA 8240 12:07 08104/9S DLC
J ,l,l•Trichloroethane u 50000 ppb' EPA 8240 12:07 08/04/9S DLC
I, 1-Dichloroethane u 50000 ppb ·. EPA 8240 12:07 08/04/95 DLC I 1,1-Dichloroethene u 100000 ppb EPA 8240 12:07 08/04/95 DLC
1,2-Dichloroethane 130,000D 50000 ppb EPA 8240 12:07 08/04/95 DLC
I 1.2-Dichloropropane u 50000 ppb EPA8240 12:07 08/04/95 DLC
2-Butanone u 120000 ppb EPA 8240 12:07 08/04/95 DLC
2-Chlorocthylvinyl ether u 100000 ppb EPA 8240 12:07 08/04/95 DLC
I 2-H=one u 50000 ppb EPA 8240 12:07 08/04/95 DLC
4-Melhyl-2-Pentanone 210,000 D 100000 ppb EPA 8240 12:07 08/04/95 DLC
I Acetone u 160000 ppb EPA 8240 12:07 08/04/95 DLC
Benzene u 50000 ppb EPA 8240 12:07 08/04/95 DLC
Bromodichloromethane u 50000 ppb EPA 8240 12:07 08/04/95 DLC
I Bromoform u S0000 ppb EPA 8240 12:07 08/04/95 DLC
Bromomethane u 100000 ppb EPA 8240 12:07 · 08/04/95 DLC
I Oubon disulfide u )00000 ppb .,EPA 8240 12:07 08/04/95 DLC
Carbon teuachloride u 50000 ppb EPA 8240 12:07 08/04/95 DLC
Chlorobenzene u 50000 ppb EPA 8240 12:07 08/04195 DLC I'·-·
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·-~-,
l;,_j
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1
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·-.. ___ ,,.
<=lUG 23 '95 15: 18 TO 391U47 FROM AquaChem E~utr, Lab T-387 P. 17
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegce Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG #: SV533080
Lab ID: AAl3963
Sample ID: BG-36
Parameter
Cblorodibromomethane
Chloroethanc
Chloroform
Cbloromethane
:is-1,2-Dicbloroethene
cis-1,3-Dichloropropene
Ethylbenune
Methylene chloride
Stryene
Tetra.:hloroethene
Toluene
Total Xytenes
trans-1.2-Dichloroethene
trans• l ,3-Dichloropropene
Trichloroethene
Vinrl chloride
Rc,ult
u
lJ
u
u
u
u
70,000 D
u
u
30,000 DJ
100,000 D
420,000 D
u
u
u
u
Detection
Limit Unit
100000 ppb
· 100000 ppb
50000 ppb
200000 ppb
50000 ppb.
50000 ppb
50000 ppb
140000 ppb
100000 ppb
50000 ppb
50000 ppb
50000 ppb
50000 ppb
~0000 ppb
50000 ppb
100000 ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Date:
ApproYed By:
Method
EPA8240
EPA 8240
EPA8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
•,
02-Aug-95
23-Aug-95
Robert L. Curry
Project Mwiager
Time Date
12:07 08/04/95
12:07 08/04/95
12:07 · 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 08/04/95
12:07 OK/04/95
12:07 08/04/95
12:07 08/04/95
12:07 UIS/04/95
12:07 08/04/95
12:07 08/04/95
Analyst
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
DLC
,.....,v ., ~~ 4~•~ IU ~~~~1~( r~□M RquoChem Enu,r. Lob T-693 P.01
I
I .:.Y>
"·· ~-
I 'R,-e\;,vi
I
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305 240 I Tuckaseegee Road South Carolina Certification Number: 99032 Charlotte, NC
I Client#: 381 Receipt D11te 30-0ct-95 Contact: Jack Kilbarger
Report Date: 17-Nov-95 I
Sample Date: 30-0ct-95
I SDG#: . SDG-000315 Approved By:
Lab Sample ID: LSID--001188 Kenneth R. Richardson Sample ID: BG-41 Project MllDager l:J Reporting • .· ..
-..'.:.·. P11J111Deter Rtsult Limit . Method Date Analyst Unit Tune
I I, 1,1-Trichloroethane u s ppb EPA8240 11/3/95 DLW I, 1,2,2-Tetrachloroethane u s ppb EPA 8240 11/3/95 DLW I, 1,2-Trichlorocthane u s . ppb EPA 8240 11/3/95 DLW I I, 1-Dichloroelhane u s ppb EPA 8240 11/3/95 DLW l, 1-Dichlorocthcnc u 5 ppb EPA8240 11/3/95 DLW 1,2-Dichloroelhanc u 5 ppb EPA 8240 11/3/95 DLW I 1,2-Dichloroethcne u s ppb EPA8240 . 11/3/95 DLW 1,2-Dichloropropanc u s ppb EPA8240 11/3/95 DLW 2-Butanone u 10 ppb EPA 8240 11/3/95 DLW I 2-Hexanone u 10 ppb EPA 8240 11/3195 DLW 4-Methyl-2-peutanone u 10 ppb ·EPA 8240 11/3/95 DLW I. Acetone u 10 ppb EPA 8240 11/3/95 DLW Benzene u. s ppb EPA 8240 11/3/95 DLW Bromodichloromcthanc u 5 ppb EPA 8240 11/3/95 DLW I Bromoform u 5 ppb EPA8240 11/3/95 DLW Bromomethanc u 10 ppb EPA8240 11/3/95 DLW Carbon Disulfide u 5 ppb EPA8240 ll/3195 DLW I Camon Tetrachloride u 5 ppb EPA 8240 11/3/95 DLW Chloroben:zeno u 5 ppb EPA82~0 11/3/?5 DLW ,. \Z,) Chloroctllane u 10 ppb EPA8240 11/3/95 DLW I ·_ Chlorofonn u s ppb EPA8240 11/3/95 DLW
I Paae l
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I<:.:__,
I
r~u~ Hqua~nem ~nvlr. Lab T-693 P,02
Certificate of Analysls
Client:
Cllenl#:
Contact:
Sample Date:
SDG#:
OHM Corporation
240 I Tuckasecgee Road
Charlotte, NC
381
Jack Kilbarger
30-0ct-95
SDG-000315
Lab Sample ID: LSID-001188
Sample ID: EG-41
Parameter Result
2,4-Dinitrophenol u
2,4-Dinitrotoluene u
2,6-Dinitrotolue.ne u
2-Cb!oronaphthalene u
2-Chlorophenol u
2-Mcthlyphenol (o-;;re,;ol) u
2-Mcthy!naphthalene u
2-Ni troanlline u
2-Nitrophenol u
3,3-Dichlorobenzidine u
3-Nitroaniline u
4,6-Dinitro-2-methylphenol u
4-Bromophenyl phenyl ether u
4-Ch!omnilinc u
4-Chloro-3-mcthylphenol u
4-Chlorophcnyl phenyl ether u
4-Mclhylphenol (p-crcsol) u
4-Nitroanillnc u
4-Nltrophenol u
Accnaphthcnc u
Acenaphthylene u
Reporting
Limit Unit
5000 ppb
500() ppb,
S000 ppb
S000 ppb
5000 ppb
5000 ppb
5000 ppb
S000 ppb
5000 ppb
5000 ppb
5000 ppb
12500 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
12500 ppb
5000 . ppb
5000 ppb
Pa2e .1
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date 30-<xt-95
Report Date: I 7-Nov-95
Approved By:
Kenneth R. Rlchanbon
Project Manager
Method Time Date
EPA8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA8270 11/8/95
EPA8270 11/8/95
EPA8270 1118/95
EPA8270 11/8/95
EPA 8270 I 1/8/95
EPA 8270 I 1/8/95
EPA 8270 11/8/95
EPA 8270 1118/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8195
EPA 8270 1118/95
EPA8270 I 118/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA8270 11/8/95
Analyst
DLW
DLW
DLW
DLW
DLW
DLW·
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DT,W
DLW
DLW
DLW
DLW
DLW
I
I
I
-1
I
I
I •:._:_:_.)
~✓
I
I
I
I
I
I
I .,~)
I
Certificate ~f Analysis
Client:
Oient 1#:
Contact:
Sample Date:
SDG#:
OH!\,! Co!J)Oration
2~01 Tuckaseegee Road
Charlotte, NC
JK!
Jack Kilbargcr
30-0ct-95
SDG--000315
Lab Sample ID: LS!D--001188
Sample ID: BG-41
Parameter Result
Anthraccne u
Benzo(a)anthracene u
Benzo (a) pyrene u
Benzo (b) fluoranthenc u
Benzo (ghi) perylcnc u
Bcnzo (k) fluoranthcnc u
Bcnzoic acid u
Bcnzyl alcohol u
Bis (2-<:hloroethoxy) methane u
Bis (2-<:hloroethyl) ether u
Bis (2-<:hloroisoprobyl) ether u
Bis (2-othylhcxyl) phthalate u
Butyl benzyl phthalate u
Chryseno u
Di-a-butyl phthalatc u
Di•n-octylphthalatc u
Dibe112o (ah) anthrdl.'CllC u
Dlbenzofuran u
Dicthylphthalatc u
Dlmethy!phthalatc u
Fluoranthcnc u
Reporting
Limit Unit
S000 ppb
5000 ppb
5000 ppb'
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
50-00 ppb
5000 ppb
5000 ppb
5000 PJX>
5000 ppb
5000 ppb
5000 ppb
5000 ppb
Pue 4
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date 30-0ct-95
Report Date: 17-Nov-9S
Approved By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA 8270 1118/95
EPA 8270 1118/95
EPA 8270 1118/95
EPA 8270 11/8/95
EPA 8270 11/8/9S
.EPA 8270 11/8/95
EPA8270 1118/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8195
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 1118195
EPA 8270 1118/95
EPA 8270 l l/8/95
EPA8270 1118195
EPA 8270 11/8/95
EPA 8270 11/8/95
Analyst
DLW.
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
'
I
le . .. ,
I
I
I
I
I
I
I
Ii\ ::.··J <.'i/
I
I
I
I
I
I
I
~ ...
• I'-
I
Certificate of Analysis.
Client:
Client#:
Contact:
Sample Date:
SDG#:
OHM Corporation
240 l Tuckaseegee Road
Charlotte, NC
3g1
Jack Kilbarger
30-0ct-95
SDG-000315
Lab Sample ID: LSID--001188
Sample ID: BG-41
Parameter Result
Fluorene u
Hexachlorobell7.ene u
Hexachlorobutadiene u
He.'<achlorocyclopentadiene u
Hexachloroethanc u
Indcno (1,2,3~) pyrcne u
lsophoronc u
N-Nitroso-dl-n-propylarnlne u
N-Nitrosodipbenylamine u
. Naphthalene u
Nitrobcnzene u
Pentachlorophenol u
Phenanthrenc u
Phenol u
Pyrene u
Reportlng
Limit
5000
5000
5000
5000
5000
SOOD
5000
5000
5000
5000
5000
sooo
sooo
5000
5000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Caroliu Certification Number: JOS
South Carolina Certifkatlon Number: 99031
Receipt Date 30-0ct-95
Report Date: 17-Nov·9S
Approved By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA 827() 1118/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8195
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA8270 1118/95
EPA 8270 11/8/95
EPA 8270 1118195
EPA 8270 11/8195
EPA 8270 11/8195
EPA 8270 11/8/95
EPA 8270 11/8195
EPA 8270 11/8/95
EPA 8270 11/8/95
Analyst
DLW
DLW
DLW
DLW,
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
I
I
I
I
I
I
I
I
I
I
I
I
. r ~un HCI u a1...nem :::t:.:.,_n u:::._1:.,.r..:.•....::.L•:.:•:.__:,_1 -..::b:.;;':l;;:;l.,:P.,:•.;:l:l:l;;;.. ______ _
Certificate of Analysis
Client: OHM Corporation
240 l Tuckaseegee Road
Charlotte, NC
Client#: 381
Contact: Jack Kilbarger
Sample Date:. 30-0ct-95
SDG #: SDG-000315
Lab Sample ID: LSID-001189
Sample ID: BG-41
. Parameter
Percent Water
Density
British Themutl Unit
TOC
Total Organic Halides
Result
98.6
1.041
lOOOU
6450
lOOOU
Reportl112
Limit Unit
0 percent
0
1000 ppni
0 ppm
1000 ppm
Pa2e 6
North Carolina Certification Number. 305
South Carolina Certification Number: 99032
Receipt Date 30-0ct-95
Report Date: 11:Nov-95
Approved By:
Kenneth R. Richardton
Project Manager
Method Time Date
ASSTM D1298.85
ASTMD20l5
EPA415.l
EPA 9020
Analyst
JCH
JCH
JCH
JCH
JCH
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
r"un M~U(ll,,,flCIII c::;.riy \ro LOD
Certificate of Analysis
Client:
Client#:
Contact:
Sample Date:
SDG#:
OHM Corporation
2401 Tuckasecgce Road
Charlotte, NC
381
Jack Kilbarger
30-0ct-95
SDG-000315
Lab Sample ID: LS!D-001190
Sample ID: BO-41
Parameter Result
Arsenic 1.14
pH II.SO
Alkalinity 241000 D
Aluminum UD
Antimony u
Barium UD
Beryllium UD
Cadmium UD
Calcium 4.50D
Chromium 0.45D
Cobalt UD
Iron 12.7D
Magnesium 0.0SD
Manganese 2.60D
Nickel 67.0D
Potassium 4300D
Silver 0.l0D
Sodium 2790DE
Vanadium UD
Zinc 85.SD
Lead 1.10D
Reporting
Limit Unit
0.00S ppm
0 Sil
1000 ppm,
o.s ppm
0.32 ppm
o.s ppm
0.0S ppm
0 ppm
0.05 ppm
0.25 ppm
0.05 ppm
0.0S ppm
O.OS ppm
0.05 ppm
l.S ppm
so ppm
0.05 ppm
5 ppm
0.05 ppm
o.s ppm
0.25 ppm
Pa2e 7
North Carolina Certification Number: 305
South Carolina Certification Number. 99032
Rtteipt Date 30-0ct-95
Report Date: 17-Nov-95
Approved By:
Kenneth R. Rlchardson
Project Manager
Method. Time Date
EPA 7470 11110/95
E?A 150.1 11 :30 10/31/95
EPA3l0.l 14:25 10131195
EPA 6010 11:00 11/10/9S
EPA6010 11/10195
EPA6010 13:55 11/9/95 .
EPA60!0 9:05 11/10195
EPA6010 11:05 1119/95
EPA 6010 9:05 11/10/95
EPA 6010 11:0S 11/9/95
EPA6010 12:35 11/10/95
E?A 6010 9:05 11110/9S
EPA6010 9:05 11110/95
EPA 6010 9:05 11110/95
EPA6010 11:05 11/9/95
EPA6010 15:55 11/9/95
EPA6010 11:05 11/9/95
EPA6010 16:35 11/9/95
EPA 6010 9:05 11/10/95
EPA6010 11 :03 11/9/95
EPA 7470 11:0S 11/9/95
Analyst
DLW
RCD
RCD
RCD
DLW
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
·RCD
RCD
RCD
RCD
'
I
1, . .:.:
' .-.... -. 1•,,,·
I
I
I
I
I
I
l)J
I
I
I
I
I
I
I ,~·
I
. Certificate of Analysis
Client:
Client#:
Contact:
OHM Corporation
2401 Tuckaseegee Road
Charlone, NC
381
Jack Kilbarger
Sample Date: 30-0ct-95
SDG #: SDG-000315
Lab Sample ID: LSID--001190
Sample ID: BG-41
Parameter Remit
Mercury
Selenium
Thallium
Flash Point
u
3.21
14.8
141
Reporting
· Limit Unit
0.006 ppm
0.32 ppm,
0.32 ppm.
70 deg.F
Pue R
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date 30-0ct-95
Report Date: 17-Nov-95
Approved By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA 7470 1111019S
EPA 7470 11/9/95
EPA 7470 11/10/95
SW-846 #9095 11:10 10/31/95
Analyst
DL\Y
DLW
DLW
RCD '
AU5 10 '95 15:30 TO 3911147
I
I,~ r·.', A.quaChem . I l,,:, ENVIRONMENTAL LABORATORIES, INC.
I
Tl 176 Downe Road
Plnevllle, NC 28134
704/588-5076
FAX [phone]
FROM AquaChem E.,vir. Lab T-338 P,1<18
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 2401 Tuckaseegee Road South Carolina Certification Number:
I Client#:
Charlotte, NC
3080 Recdved Date: 27-Jul-95 Contact: Mr. Randy Bennett Report Date: IO-Aug-95
lsnG~ SV213080 Approved By:
Lab ID: AA!3852 Rohen L. Curry
ISampleID: BG-41 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
IJxidation Potential 356 mv 11:00 08/09/9j
Per<ent Water 36,14 % 09:00 08/02/95
I Total Dissolved Solids 390,000 62 ppm EPA 209A 14:00 08/03/95
Alkalinity Can Not Test 2 ppm EPA 310.1
Total Organic Carbon (TOC) 410000 ppm EPA 415.1 13:00 08/03/95
I l,l,l,2-Tctra<;bloroethane UD 5000 ppb EPA 8240 14:03 08/02/95
I, I.I-Trichloroethane UD 5000 ppb EPA 8240 14:03 08/02/9S
I l,l,2,2-Tetrachlorocthanc UD 5000 ppb EPA 8240 14:03 08/02195
I, 1,2-Trichlorocthanc UD 5000 ppb EPA 8240 14:03 08/02195
' I, 1-Dichlorocthane 11,000 D S000 ppb EPA 8240 14:03 08/0219S
• 1.1-Dichloroethene UD 5000 ppb EPA 8240 14:03 08/02/95
1,2-Dichloroethanc UD 5000 ppb EPA 8240 14:03 08/02195
11,2-Dichloropropanc UD 5000 ppb EPA 8240 14:03 08/02/95
2-Butanone 26.000 6000 ppb EPA 8240 14:03 08/02195
2-Chlorocthylvinyl ether UD 5000 ppb EPA 8240 14:03 08/02/95
12-Hexanone UD 5000 ppb EPA 8240 14:03 08/02195
4-Methyl-2-pentanone 12,000 D 5000 ppb EPA 8240 14:03 08/02195
1 Acetone UD 8500 ppb EPA 8240 14:03 08/02195
Benzene UD 9500 ppb EPA 8240 14:03 08/02195
•.. -omod!chloromethane UD 5000 ppb EPA 8240 14:03 08/02/95 IJ
••
305
99032
Analyst
JCH
JCH.
DLC
JCH
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A."IM
ANM
ANM
ANM
ANM
RUG 10 '95 15;31 TO 3911147
I
I:>~ ,\/ Aqua Chem I l.:. ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Plnevllle, NC 28134
7041588-5076
FAX [phone]•2454
FROM RqcaChem Enu\r. Lab T-338 P.09
I
I Certificate of Analysis
OHM Corporation I Client:
lc11ent#:
240 I Tuck:tseegee Road
Charlotte, NC
Contact:
ls»G 11,
Lab ID:
ISampleID:
Parameter
1:-.)omoform
.~~ .
3080
Mr. Randy Bennett
SV213080
AAJ3852
BG-41
Bromomethanc I Carbon disulfide
Carbcn tetrachloride
Chlorcbcnzcnc I Chlorodibromomethane
Chloroethane I Chloroform
Chloromcthane
cis-1,2-Dichloroethene I cis-1,3-Dichloropropene
Ethylbenzene
1 Stryene
Tetrachloroethene
Toluene I Total Xylenes ·
trans-1,2-Dichloroethene
1 trans-1,3-Dichloropropene
Trichlorocthene
· :"nyl chloride I_>
I
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
DeteetiOll
Limit
5000
5000
5000
5000
5000
5000
5000
S000
S500
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: IO-Aug-95
Approved Dy: ____ _
Robert L. Cuny
Project Manager
Method Time Date
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/9S
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/9S
EPA 8240 14:03 08/02/9S
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA8240 14:03 08/02/95
EPA 8240 14:03 08/02195
EPA 8240 14:0J 08/02/95
EPA 8240 14:03 08/02/95
EPA8240 14:03 08/02/95
EPA 8240 14:03 08/02/95
EPA 8240 14:03 08/02/9S
EPA 8240 14:03 08/02/9S
EPA 8240 14:03 08/02/95
Analy!I
ANM
ANM.
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
Al'iM
AUG 10 '35 15:32 TO 39:1147
I
,>. k '?:1 A.quaChem I ~ ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downs Road
Plnevlllo, NC ~8134
704/588,5076
FAX [phone]
FROM AquaChem Env\r. Lab T-338 P. ,0
I Cer.tificate of Analysis
I Client: OHM Corporation North Carolina Ccnirication Number:
2401 Tuckaseegee Road Soutb Carolina Cer1ification Number:
I Client#:
Charlotte, NC
3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Repor1 Da1e: 10-Aug-95
I SDG#: SV213080 Approved By:
Lab ID: AAl3852 Robert L. Curry I Sample ID: BG-41 Project Manager
Detection
Parameter Result Limit Unit Method Time Date
l>'i.,2,4-Trichlorobenune UD 100 ppb EPA 8270 14:30 08/02/95 . ' _ .. ., .
1,2-Dichlorobenzene UD 100 ppb EPA 8270 14:30 08/02/95
I 1,3-Dichlorobenzene UD 100 ppb EPA 8270 14:30 08/02/95
1,4-Dichlorobenzene UD 100 ppb EPA 8270 14:30 08/02195
2, 4, 5-Trichlcrophenol UD 100 ppb EPA 8270 14:30 08/02/95 I 2,4,6-Trichlorophcnol UD 100 ppb EPA 8270 14:30 08/02/95
2,4-Dichlorophenol UD 100 ppb EPA 8270 14:30 08/02/95
I 2,4-Dimethylphenol UD 100 ppb EPA 8270 14:30 0810219S
2,4-Dinitrophenol UD 100 ppb EPA 8270 14:30 08/02/95
2,4-Dinitrotolucne UD 100 ppb EPA 8270 14:30 08/02/95 I 2,6-Dinitrotoluene UD 100 ppb EPA 8270 14:30 · 08/02/95
2-Chloronaphthalene UD 100 ppb EPA 8270 14:30 0810219S
I 2-Chloropbcnol UD 100 ppb EPA 8270 14:30 08102195
2-Methylnaphthalene UD 100 Wb EPA 8270 14:30 08/02/95
2-Mcthylpbenol (o-cresol) un 100 ppb EPA 8270 14:30 08102/95
I 2-Nitroaniline UD 100 ppb EPA 8270 14:30 08102/95
2-Nitrophcnol UD 100 ppb EPA 8270 14:30 08102/95
I 3-Nitroaniline UD 100 ppb EPA 8270 14:30 0810219S
4,6-Dinitro-2-methylphcnol UD 100 ppb EPA 8270 14:30 08/02/95
-'.,6-Dinitr()-0-(resol UD l00 ppb EPA 8270 14:30 08/02195
-· I'
I
305
99032
Analyst
ANM
ANM
A.NM
ANM
ANM
ANM
ANM
A.NM
A.."'IM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 18 '95 15:32 ,O 3911147
I
I .. ~ t? .Aqua Chem · I l.:. ENVIRONMENTAL LABORATORIES, INC.
I
11176 Downs Roacl
Plnevlllo, NC 28134
704/588·5076
FAX [phone]
FROM AquaChem Eou \c. Lab T-338 P. 11
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number:
2401 Tuckaseegee Road South Carolina Certification Number:
I Charlotte, NC
Client#: 3080 Recdved Date: 27-Jul-95
Cootact: Mr. Randy Bennett Report Date: IO•Aug-95
I SDG If: SV213080 Approved By:
Lab ID: AAl3852 Robert L. Curry
I Sample ID: BG-41 Project Manager
Detection
Parameter Result Limit lnit Method Tbne Date
1:)-Bromophenyl phenyl ether UD 100 ppb EPA 8270 14:30 08/02/95
4-Chloro-3-mc:thylpbcool UD 100 ppb EPA 8270 14:30 08/02/95
I 4-dtloroaniline UD 100 ppb EPA 8270 14:30 08/02/95
4-Chlorophenyl phenyl ether UD 100 ppb EPA 8270 14:30 08/02/95
4-Methylphenol (p-eresol) UD 100 ppb EPA 8270 14:30 08/02/95 I 4-Nitroaniline UD 100 ppb EPA 8270 14·.30 08/02195
4-Nitrophcncl UD 100 ppb EPA 8270 14:30 08/02/95
I Acenaphthcne UD 100 ppb EPA 8270 14:30 08102/95
Accnaphthylcnc UD 100 ppb EPA 8270 14:30 · 08/02195
Benzo(a)anthracene UD 100 ppb EPA 8270 14:30 08/02/95 I Benzo(a)pyrcne UD 100 ppb EPA 8270 . 14:30 08/02/95
Benzo(b)fluoranthene UD 100 ppb EPA 8270 14:30 08/02/95
I Denzo(ghi)perylcne UD 100 ppb EPA 8270 14:30 08/02/95
Benzo(k)fluoranthcnc UD 100 ppli EPA 8270 14:30 08/02/95
. Bis(2<hloroethoxy) methane UD 100 ppb EPA 8270 14:30 08/02195 I Bis(2<hloroethyl) ether UD 100 ppb EPA 8270 14:30 08102/95
Bis(2<hloroisopropyl) ether UD 100 ppb EPA 8270 14:30 08102/9:l
I Bis(2~thylhcxyl) phthalate UD 100 ppb EPA 8270 14:30 08102/95
Butyl benql phthalate UD 100 ppb EPA 8270 14:30 08/02/95
~luyscnc UD 100 ppb EPA 8270 14:30 08/02195 1-::.1
I
305
99032
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 10 '95 15:33 TO 3911147
I
I~.~ <x: Aqua Chem. I ENVIRONMENTAL LABORATORIES, INC.
11178 Downs Road
Plnevllfe, NC 28134
7041588-5078
FAX 704/588·2454
FROM AqwaChem Er,vir. Lab T-338 P. 12
I
I Certificate of Analysis
OHM Corporation I Client:
I Client#:
2401 Tuckaseegec Road
Charlotte, NC
3080
Contact: Mr. Randy Bennett
I SDG#: SV213080
AAl3852 Lab ID: I Sample ID: BG-41
Parameter
l)/li-o-butyl phthalate
" ·Di-n-octyl phtbalate
I Diben,.o{ah)anthracene
Dibenzofuran
I
Diethylphthalate
Dimethylphtbalate
Fluoranthene
I Fluorene
Hexachloroben:ane
Hexachlorobutadiene
I Hexachlorocyclopentadiene
Hcxachlorocthanc
I I ndeno(l ,2 ,3-<:d)pyrene
lsophorone
N-Nitroso-di-n-propylamine I N-Nitrosodiphcnylamine
Naphthalene
'
I Nitroben,ene
Pentachlorophcnol
. '~enanthrene l(c_j
I
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
uo
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Date:
Approved By:
Method
EPA 8270
EPA 8270
EPA 8270
EPA8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
27-Jul-95
10-Aug-95
---
Robert L. Cuny
Project Manager
Time Date
14:30 08/02/95
14:30 08/02195
14:30 08/02/95
14:JO 08/02/95
14:30 08/02/95
14:30 08102/95
· 14:30 08/02/9S
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
14:30 08/02/95
Analyst
··•·-
ANM
ANM.
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 10 '95 15:33 TO 3911147
I
1.,•~-. }T_
I /.:~~~~O~at~A~~ATORIES, INC.
11115 Downs Road
Plnevllle, NC 28134
7D41588-5078 I FAX [phone]
FROM AquaChem Eovir. Lab T-338 P, "3
I Certificate of Analysis
I Oient: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client II: 3080 Rtteived ·Date; 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 10-Aug-95
I SDG/1: SV2l3080 Approved By:
Lab ID: AA13852 Robert L. Curry
S:unple ID: BG-41 Projed Manager I Detection
Parameter Reoutt Limit Unit Method Time Date Analyst .-. 1oc· \enol UD 100 ppb EPA 8270 14:30 08/0219S ANM •• ·1
·-c_fyrcne UD 100 ppb EPA 8270 14:30 08/02195 ANM
I Total SUSJ)Cnded Solids 45,000 ppm SM209C 13:30 08/03/95 DLC
Total Organic Halide (TOX) u . 1.0 ppm SM 506 14:00 08/04/95 JCH
Barium u 0.5 ppm SW 6010 10:55 08/03/95 RCD
I Cadmium 0.05 0.05 ppm SW 6010 10:45 08/08/95 RCD
Chromium 0.40 0.25 ppm SW 6010 10:45 08/08/95 RCD
Copper u 0.02 ppm SW 6010 10:45 08/08/95 RCD I Iron 4.65 0.0S ppm SW 6010 14:30 08/02195 RCD
Nickel .U O.Q3 ppm SW 6010 '10:45 08/08/95 RCD
I Silver u 0.05 ppm SW 6010 10:45 08/08/95 RCD
Zinc 73 0.50 ppm SW 6010 10:45 08/08/95 RCD
Arn:nic 0.07S 0.02S ppm SW7060 10:30 08/03/9S RCD I Lead 6.30 0.25 ppm SW 7421 10:45 08/08195 RCD
Mcixury u 0.004 ppm SW 7471 08:30 08/10/95 KRR
I Selenium 0.013 0.02S ppm SW 7740 14:20 08/03/9S RCD
Flash Point 78 70 Dcg.F SW-l!46 #909 10: 15 08/10/95 KRR
Aluminium u 0.5 ppm SW846 60IO 09:40 08/04/9j RCD I Aotimony u 0.050 ppm SW8466010 14:40 08/07/9S Ren ,. ,ryllium u 0.05 SW846 6010 14:30 08/02/95 RCD ppm ~:
I
I
AUG 10 '95 15:34 TO 39"1147
I
1
1 u,iAi'!.~E~.~r!'"'"'·""· '"' 11176 Downs Road
PIMvllle, NC 28134
704/588-5076 I FAX [phone]
FROM AqvaChem Envir. Lab T-338 P. "4
I Certificate of Analysis
I Client:
I Client#:
Contact:
I SDG#:
Lab ID:
I
Sample ID:
Pa.rameter
···:· \ 1 ··;·_-~_}alcium __ ,.. .
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Cobalt
Magnesiwn
Manganese
Potassium
Sodiwn
Thalliwn
Vanadium
PH
OHM Corporation
240 l Tockaseegee Road
Charlotte, NC
3080
Mr. Randy Bennett
SV2!3080
AA13852
BG-41
Result
2.60
u
1.90
0.75
3240
5800D
u
u
13.03
Detection
Limit Unit
0.05 ppm
0.05 ppm
0.05 ppm
0.05 ppm
50 ppm
500 ppm
0.050 ppm
0.25 ppm
0-14 SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: IO-Aug-95
Approved By: _________ _
Robert L. Cuny
Project Manager
Method Time Date Analyst
.SW846 6010 14:JO 08/02195 RCD
SW8466010 11:30 08/07/95 RClJ
SW846 6010 14:JO 08102/95 RCD
SW846 6010 14:JO 08102/95 RCD
SW846 6010 14:05 08/07195 RCD
SW846 6010 14:20 08103195 RCD
SW846 6010 08:40 08107/95 RCD
SW846 6010 14:JO 08/02/95 RCD
SW846 9045 10:03 08110/95 KRR
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I l\.
)
Bulk Group 4 7
Bulk Group Description: W /S Acid l.,iquid
(Chlorinated Oxidizer
• Note: Bulk Groups were named aeeordiog to preliminary hazardous
categorization test and may not correspond to what the material
was classified as for disposal.
I
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"-..,'
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I
/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11178 Down• Road .
Plnevllle, NC 28134
704/588-5078
FAX [phone]
FROM AqeaChem Envir. Lab T-543 P,07
Certificate of Analysis
Client: OHM Corporation North Carolina Certlflca1fon Number: 305 2401 Tuckaseegee Rood South Carolina Certiflcatfoa Number: 99032 Charlotte, NC
Client#: 3080 Retelved Date: 24-May-95 Coatlic1: Mr. Randy Bennett Report Date: IO-Oct-95
SDG#: SR633080 Approved By: ;_Ufi-~ 0 Lab ID: AAl190l
Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
N-nitroso-di-n-propylamine UD 1000 ppb EPA 8270 17:51 05/31/95 ANM N :rutrosodipbenylamine UD 1000 ppb EPA 8270 17:51 05/31/95 ANM Naphthalene UD 1000 ppb EPA 8270 . 17:51 OS/31/95 ANM Nitro~• UD 1000 ppb EPA 8270 17:51 05/31/95 ANM Pcntachlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM Phenanthrene UD 1000 . ppb EPA 8270 17:51 05/31/95 M"M Phenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM Pyrcnc UD 1300 .. ppb EPA 8270 17:51 OS/31/95 ANM Total Suspended Solids 7280 ppm SM209C 10:00 05/29/95 TML Total Organic Halide (TOX) u 1.0 ppm SM506 17:00 05/30/95 JCH O:tidation Potential 42L31 +\-10 mv SM2310B 15:30 06/06/95 JOI Arsenic u 0.025 ppm SW6010 08:30 06/01/95 KRR Barium u 0,5 wm SW 6010 14:50 06/01/95 RCD Cadmium 1.26 0.05 ppm SW6010 18:10 0S/31/95 KRR Chromium 139D 25 ppm SW6010 18:10 .0S/31/95 KRR Copper 256D 10 ppm SW6010 18:10 0'131/95 KRR Iron 10900DE IS wm SW60!0 16:07 05/3U95 KRR Lead 3.6S 0.2S ppm ·s SW6010 18:26 06/01/95 RCD Nickel 415 D 15 ppm SWGOlO 18:10 05/31/95 KRR Silver u o.o, ppm SW6010 18:10 05/31/9, KRR
I
/Aqua Chem
ENVIRONMENTAL LABORAT.ORIES, INC. 11176 Dawna Road
Pfnovllle, NC 28134
704/588-8076
FAX [phone]
FROM AquaChom Enuir. Lab T-543 P.08
I
I
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I
I
Certificate of Analysis
I
I
I
I
I
I
1.
Client:
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Plll'ameter
Zinc
Mercu.ry
Selenium
Flash Point
Aluminium
Antimony
Beryllium
Calcium
Cobalt
Magnesium
Manganese
Potassium
Sodium
Thallium
Vanadium
pH
·-I
I
OHM Corporation
240 I 1i1ckaseegee Road
Charlotte, NC
3080
Mr. Randy Bennett
SR633080
AA11901
BG-47
Result
. 7840DE
UD
0.195
>220 ·
44.4
0.18
u
70.S D
u
10.7
387D
58. l
2050D
1.15D
2.11
0.1 U
Detection
Limit
s
0.002
0.025
7.0
0.5
0.05
0.25
25
0.25
0.25
25
0.5
. so
0.50
0.25
0.1
Unit
ppm
ppm·
ppm
Deg.F.
ppm
ppm
ppm
ppm
ppm.
ppm
ppm
ppm
ppm
ppm
ppm
SU
North Carolina Certlflcatloo Number: 305
South Carolina Certlflcatioo Number: 99032
Received Date:
Report Date:
Approved By:
Method
SW6010
SW7470
SW7740
24-May-95
I0-Oct-95 E,·=o-Rort.uny.
Project Manager
Time Date Analyst
18:10 05/31/95 KRR
10:30 06/02/95 TM!..
09:20 06/01/95 Krul·
SW-846 #909 10:00 05/30/95 TML
SW846 6010 08:19 06/01/95 KRR
SW8466010 11:10 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW8466010 16:07 05/31/95 KRR
SW8466010 11:15 05/31/95 RCD
SW8466010 16:07 05/31195 !<RR
SW8466010 16:07 05/31/95 !<RR
SW846 6010 07:37 06/01/95 KRR
SW846 6010 09:50 06/01/95 KRR
SW8466010 08:20 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW846 9040 08:20 05/30/95 RCD
..
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I
lA~~C?,~,~~'°"''•'"'• '"c 11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]•2454
FROM AquaChem Envir, Lab T-54:J P.02
Revised Report
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckasecgee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Received Date: 24-May-9S
Contact: Mr. Randy Bennett Report Date: I0-Oct-95
~-SDG#: SR633080 Approved By: C, Lab ID: AAll901 L CUllY
Sample ID: BG-47 Project Ma!Uger
Detection
l'arl!Deler Result Limit Unit Method Time Date Analyst
Percent Water 96.10 .Q. % .(). 17:00 05/30195 JCH
Total Dissolved Solids 4200 I ppm EPA 209A 16:25 05130/95 RCD
Chloride 55 5 ppm EPA32B 10:15 05/30/95 . RCD
Nitrate+ Nitrite 17,6 5.0 ppm EPA 353.3 12:05 05/30/95 RCD
Total Phosphorus 2.35 ,10 ppm· . EPA 365.3 10:30 05130/95 RCD
Sulfate 710 I ppm EPA 375.4 09:50 05/31/95 RCD
Total Organic Camon (TOC) 810 ppm EPA415.I 17;00 OS/30/95 . JCH
!, I, 1,2-Tetrachloroethane UD 500 ppb EPA8240 02:53 06i01/95 DLC
1,1, 1-Trichloroelhanc UD 500 ppb EPA 8240 02:53 06i01/9S DLC
1.1,2,2~retrachloroethane UD 1000 ppb EPA 8240 02:53 06/01/95 DLC
I, 1,2-Trich!oroethane UD 500 ppb EPA8240 02:53 06/01/95 DLC
1, 1-Dichlorocthane UD 500 ppb EPA8240 02:53 06/01/95 DLC
1, 1-Dichloroelhene UD 1000 ppb EPA 8240 02:53 06/0li95 DLC
I, 2-Dichloroethane UD 500 ppb EPA8240 02:53 06/01/95 DLC
1,2-Dichloropropane UD 500 pph EPA8240 02:53 06/01/95 DLC
2-BulallOne UD 1200 ppb EPA:8240 02:53 06101/95 DLC
2-Chloroethylvinyl ether UD 1000 ppb EPA8240 02:53 06/01/95 DLC
2-Hexaaonc UD 500 ppb , EPA 8240 02:53 06/01/95 DLC
4-M:thyl-2-Pentanone UD 1000 ppb EPA 8240 02:53 06101/95 DLC
Acetone UD 1600 ppb EPA 8240 02:53 06/01/95 DLC
<
U(; I l<l '95 1:18: 2'3 TO 39: 1147 FROM AqvaChem Envir. Lab T-543 P.1:13 I
I".;>,
~quaChem ·o , •.• :
I ENVIRONMENTAL LABORATORIES, INC. 11178 Dowria Road .
Plnevllle, NC 28134
I 7(W583-5078 .
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305 2401 Tuckaseegee Road South Carolina Certification N11D1ber: 99032 Charlotte, NC I Client#: 3080 Rei:eived Date: 24-May-95 Contact: Mr. Randy Bennett Report Date: 10-0ct-95
I SDG#: SR633080 Approved By: Rtl:;;•t> Lab ID: AAl190I
I Sample ID: BG-47 Projm Manager
Detection
Parameter Result Llmlt Unit Method Time Date Analyst ,-~ -.-.. , Benzene UD 500 . EPA 8240 02:53 06/01/95 .:, _:) ppb DLC :_::_,,:
Bromodichloromethane UD 500 ppb EPA8240 02:53 06/01/95 DLC ,I Bromofonn UD 500 ppb EPA8240 02:53 06/01/95 DLC
Bromomethane UD 1000 ppb • EPA8240 02:53 06/01195 DLC Carbon clisulfide UD 1000 ppb · EPA8240 02:53 06/01/95 DLC I Carbon tetrachloride UD 500 ppb EPA8240 02:53 06/01/95 DLC Chlorobenzene UD 500 ppb EPA8240 02:53 06/01/95 DLC
I Chlorodibromcmethane UD 1000 ppb EPA8240 02:53 06/01/95 DLC
Chloroethane UD 1000 ppb EPA8240 02:53 06/01/95 DLC
Chlorofonn UD 500 ppb EPA8240 02:53 06/01/95 DLC I Chloromethane UD 2000 ppb EPA8240 02:53 06/01/95 DLC
cis-1,2-Dichloroethene UD 500 ppb EPA8240 02:53 06/01/95 DLC
I cis-1,3-Dichloropropenc UD 500 ppb EPA 82-10 02:53 06/01/95 DLC
Etbylbenzcne UD 500 ppb EPA 8240 02:53 06/01/95 DLC
Methylene chloride UD 1400 ppb EPA8240 02:53 06/01195 DLC I Sllycnc UD l000 ppb EPA8240 02:53 06/01/95 DLC Tctrachloroethcnc UD soo ppb EPA8240 02:Sl 06/01/95 DLC
Toluene UD 500 ppb ·s EPA 8240 02:53 06/01/95 DLC I Total Xylenes UD 500 ppb EPA8240 02:53 06/01/95 DLC
': ! traru-1,2-Dichlorocthcne UD 500 ppb EPA8240 02:Sl 06/01/95 DLC Is_/
I
-~· •Y ..I..J •.JO•..x.J ,U .,;l':l'•J.J.""tf ~KUl'l HqwaLhem t:.nu lr. Lab T-543 P,04
I
··"' . ,<·:,\ lAquaChem -;: •. ~ :-.. :: ·-:•::..."
I ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Plnevllle, NC 28134
I 704/588-15076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 3-05
2401 Tuck,sseegee Road South Carolina Certifica1ion Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 1!iz: .. I SDGII: SR633080 Approved By:
Lab ID: AAl1901 .Curry 0
I Sample ID: BG-17 Project Manager ..
Detection
Parameter Result Limit Unit Method Time Date Analyst .,7-_ tnw,-1,3-Dichloropropcnc UD S00 02:53 06/01/95 : .:' i ppb EPA8240 DLC -..~·.:~'
'frichlorocthene UD 500 ppb EPA8240 02:53 06/01/95 DLC
I Vinyl chloride UD 1000 ppb EPA8240 02:53 06/01/9S DLC
1,2,4-Trichlorobenzene UD 1000 ppb,_ EPAH270 17:51 0~/3J/95 A.\IM
1,2-Dichlorobenzene UD 1000 ppb EPA 8270 17:51 OS/31/95 A.'<M ·1 I ,3-Dichlorobcnzenc UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
1,4-Dichlorobenzene UD 1000 ppb EPA 8270 17:51 05/31/9S ANM
I 2, 4,5-Trichlorophenol UD 1000 ppb EPA8270 · 17:51 05/31/9S ANM
2, 4,6-Trichlorophenol UD 1000 ppb EPA 8270 17:51 05131/95 ANM
2,4-Dichlorophcnol UD 1000 ppb EPA 8270 17:51 OS/31/95 ANM
I 2,4-Dimethylphenol UD 1000 ppb EPA 8270 17:51 05/3119, ANM
2,4-Dinitrcphenol UD 1000 ppb EPA 8270 17:51 05/31/9S ANM
2,4-0initrotolucnc UD 1000 ppb EPA 8270 17:51 05/31/9S · ANM I 2,6-0initrotoluenc UJJ 1000 ppb EPA 8270 17:51 05/31/9S ANM
2-Chloronaphthalene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 2-Chlorophcnol UD 1000 ppb EPA 8270 17:51 0.1/31/95 ANM
2-Methylnaphthalcnc UD 1000 ppb EPA 8270 17:S I 05/3119S ANM
2-Methylphcnol (CK:resol) UD 1000 ppb , EPA 8270 17:51 05/31/95 ANM I 2-Nitroanilinc l,1) 1000 ppb EPA 8270 17:51 05/31/95 ANM
2-Nitrophenol UD 1000 ppb EPA 8270 I 7:5 I 05/31/95 A."IM I'-'
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Aqua Chem
eNVIRONMENTAL LABORATORIES, INC.
11178 Downe Road
Plnovllle, NC 28134
7041588-5076
FAX 704/~86-24e4
FRDr·1 Aq"aChem Env i r. Lab T-54::l P.05
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#:
Cootac't:
SDG II:
Lab ID:
3080
Mr. Randy Bennett
SR.633080
AA11901
Sample ID: BG-17
Parameter
3,3-Dichlorobenzidine
3-Nitroani!ine
4,6-Dinitro-2-methylphencl
4 ,6-Dinitro-o-crcsol
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Methylphenol {p-msol)
4-Nitroaniline
4-Nitrophenol
Acenaphlhcnc:
Accnaphthylcne
Benzo(a)anthracene
Bcnzo(a)pyrcnc
Bcnzo(bJfluoranthene
Benzo(ghi)perylene
Bcnzo(k)fluoranthene
Bcnzoic Acid
Benzyl alcohol
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
lJD
LU
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1900 ·
3000
2000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb,
ppb.
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certifica1ion Number: 305
Sooth Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date:
-~10 -95 ,.
Appro,·ed By: .,l--~~¥,.,6,~-""· ""7.'i"",.--
Robe . Curry V
Method
EPA8270
EPA 8270
EPA8270
EPA 8270
. EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
. EPA 8270
EPA 8270
EPA 8270
s EPA 8270
EPA R270
EPA 8270
Project Manager
. Time
17:51
17:S1
17:51
17:51
17:Sl
17:51
17:51
17:S1
1751
17:51
17:51
17:51
17:51
17:51
17:51
17:51
17:51
17:51
17:51
17:51
Date
05/31/9S
0S/31/95
05/31/95
05/31/95
05/31/9S
05131/95
05131/95
05131/95
05131/95
051:ll/95
05131/95
05131/95
05131/9S
0S/31195
0:5/31/95
051:l 1195
05/31195
05/31195
0513119:5
05/31195
Analyst
ANM
ANM
A.'lM
A.'lM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
A]l,11,1
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
uc, l~ ·~5 ~8:Jl TO 39:1147 FROM Aqo•Cnem Eov ir. L•b T-543 P, 06 I
le-,
/A~!',~!?,~.~~"'""0'"'· '"'
\\~:)
,.;_,.•
I 11178 Dawna Raad
I Pineville, NC 28134
704/588-5076
FAX 704/sa&-2454
I Certificate of Analysis
I Client: OHM Corporation ~lorth Carolina Certification Number: 3-05
240 l Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Rl:l:elved Date: 24-i\fay-95 .
Contact: Mr. Randy Bennett Repor1 Date: IO-Oct-95
I SDG_#: SRG33080 Approved By: ~-3--Lab ID: AA11901
I Sample ID: BG-47 Project Mnnager
Detection
Parameter Result Limit Unit Method Time. Date Analyst I) Bis(2-<:hloro,:thoxy) methane UD 1000 ppb EPA 8270 ·17:51 05131/95 ANM .
Bis(2-<:hloroethyl) ether UD 1000 ppb EPA 8270 17:51 05131/95 .A.'lM
I Bis(2-<:hloroisopropyl) ether UD 1000 ppb EPA 8270 17:51 05131/95 ANM
Bi,(2-<:thylhexyl) phthnlate UD 1900 ppb EPA 8270 17:51 05/31195 ANM
Bulyl beiuyl phthalate UD 1500 ppb · EPA 8270 17:51 05131195 ANM I Chrysene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Di-n-butyl phthalate UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Di-n-«tyl phthalate IJD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Dibcnzo(a,h)autlu=e UD 1000 ppb EPA 8270 17:51 05/31195 ANM
Dibenzofuran UD 1000 ppb EPA 8270 17:51 05/31195 ANM
I Diethylphthalate UD 1000 ppb EPA 8270 17:51 05131/95 ANM
Dimelhylphthalate UD 1000 ppb EPA 8270 17:51 05/31195 ANM
I Fluoranthene !JD 1000 ppb EPA 8270. 17:51 05131/95 A.'lM
Fluorene UD 1000 ppb EPA 8270 17:.H 05131195 ANM
Hexachlorobenzenc UD 1000 ppb EPA 8270 17:51 05/31195 ANM
I Hcxachlorobu1adienc UD 1000 ppb EPA 8270 17:51 OS/31/95 ANM
Hexachlorocyclopentadiene IJD 1000 ppb EPA 8270 17:51 05131195 ANM
I Hexachlaroethanc UD 1000 ppb < EPA S270 17:51 o,n1/9s ANM
Indcno(l ,2,3-<:d)pyrcoe UD 1000 ppb EPA 8270 17:Sl 05131195 ANM
l -lsophoronc !JD 1000 ppb EPA 8270 11:,1 OS/31195 ANM 1-
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IA.qua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pinevllle, NC 28134
704/588-5076
FAX [phone]
i
NC
SC
Certification Number:
Certification Number:
Date of Report:
Date Received:
Client:' OHM Corporation Services, Corp.
5335 Triangle Parkway
Norcross, Ga 30092
Contact: Mr. Cary Sherman
Customer Number: 3080
Laboratory Report
LAB ID: AA11901
SAMPLE ID: BG-47
ANALYSIS: Oxidation Potential (Acidity)
\
June 7, 1995
May 24, 1995
305
99032
167 Milligrams KOH per gram of oil (equivalent to 3.4 N. acid)
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I
/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2-10 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: ~✓-7-Lab ID: AAll901 Rclb'1cur;
I Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst I",·, ) 2-Nitrophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM ·.: .. _:,
._:_,
3,3--Dichlorobenzidine UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 3-Nitroaniline UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4,6-Dinitro-2-methylphenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 4,6-Dinitro-o-cresol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4-Bromophenyl phenyl ether UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4-Chloro-3-methylphenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 4-Chloroaniline UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4-Ch!orophenyl phenyl ether UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 4-Methylphenol (p-cresol) UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4-Nitroaniline UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
4-Nitrophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Acenaphthene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
·Acenaphthylene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Benzo(a)anthracene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Benzo(a)pyrene UD 1900 ppb EPA 8270 17:51 05/31/95 ANM
Benzo(b)fluoranthcne UD 3000 ppb EPA 8270 17:51 05/31/95 ANM I Benzo(ghi)perylene UD 2000 ppb EPA 8270 17:51 05/31/95 ANM
. 1 Benzo(k)fluoranthcne UD 1000 ppb EPA 8270 17:51 05/31/95 ANM 1~-' Benzoic Acid UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
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l Aqua Ch em
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95 /)
I SDG#: SR633080 Approved By: ~-2?? Lab ID: AAII901 Robert Cuny
I Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
·~) I Benzyl alcohol VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Bis(2-chloroethox-y) methane VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Bis(2-chloroethyl) ether VD 1000 ppb EPA 8270 17:51 05/31/95 _ANM
Bis(2-chloroisopropyl) ether VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Bis(2-ethylhex,·I) phthalate VD 1900 ppb EPA 8270 17:51 05/31/95 ANM I Butyl benzyl phthalate VD 1500 ppb EPA 8270 17:51 05/31/95 ANM
Chrysene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Di-n-butyl phthalate VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Di-n-octyl phthalate VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Iiibenzo(a,h)anthracene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Dibenzofuran VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Diethylphthalate VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I ' Dimethylphthalate VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Fluoranthene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Fluorene _VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Hexachlorobenzene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
Hexachlorobutadiene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I Hexachlorocyclopentadiene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
, __ --:· ; ) Hexachloroethane VD 1000 ppb EPA 8270 17:51 05/31/95 ANM 10 Indeno(l ,2,3-cd)pyrene VD 1000 ppb EPA 8270 17:51 05/31/95 ANM
·,;,
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I
b\qua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Appro,·ed By: ~ Lab ID: AA11901 Ro~Curry
I Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date IS'.; ~--· Isophorone UD 1000 ppb EPA 8270 17:51 05/31/95
N-nitroso-di-n-propylamine UD 1000 ppb EPA 8270 17:51 05/31/95 .
I N-nitrosodiphenylamine UD 1000 ppb EPA 8270 17:51 05/31/95
Naphthalene UD 1000 ppb EPA 8270 17:51 05/31/95
Nitro benzene UD 1000 ppb EPA 8270 17:51 05/31/95 I Pentachlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95
Phenanthrene UD 1000 ppb EPA 8270 17:51 05/31/95
I Phenol UD 1000 ppb EPA 8270 17:51 05/31/95
Pyrene UD 1300 ppb EPA 8270 17:51 05/31/95
'
I Total Suspended Solids 7280 ppm SM 209C 10:00 05/29/95
Total Organic Halide (TOX) u 1.0 ppm SM506 17:00 05/30/95
Arsenic u 0.025 ppm SW 6010 08:30 06/01/95
I Barium u 0.5 ppm SW 6010 14:50 06/01/95
Cadmium 1.26 0.05 ppm SW 6010 18:10 05/31/95
I Chromium 139 D 25 ppm SW 6010 18:10 05/31/95
Copper 256 D 10 ppm SW 6010 18:10 05/31/95
Iron 10900 DE 15 ppm SW 6010 16:07 05/31/95
I Lead 3.65 0.25 ppm SW 6010 18:26 06/01/95
( .. , ; Nickel 415 D 15 ppm SW 6010 18:10 05/31/95 IV Silver u 0.05 ppm SW 6010 18:10 05/31/95
I
305
99032
if
Analyst
ANM
ANM
-ANM
ANM
ANM
' ANM
ANM
ANM
ANM
TML
JCH
KRR ' RCD
KRR
KRR
KRR
KRR
RCD
KRR
KRR
I
It-=\\
I l A~~~o'9,~~~•omomes. '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
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I
I
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I
Certificate of Analysis
Client: OHM Corporation
2401 Tuckaseegee Road
Charlotte, NC
Client #: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA11901
Sample ID: BG-4 7
Parameter_ Result 1~-. -':-.")' Zmc ..,__... . 7840 DE
Mercury UD
I Selenium
Flash Point
0.195
>220
I Aluminium
Antimony
44.4
0.18
Beryllium u
I Calcium
Cobalt
70.5 D
u
I Maganese
Magnesium
387 D
10.7
Potassium 58.1
I Sodium
Thallium
2050 D
1.15 D
I Vanadium
pH
2.11
u
I
.½)}
I
Detection
Limit
5
0.002
0.025
· 70
0.5
0.05
0.25
25
0.25
25
0.25
0.5
50
0.50
0.25
0-14
Unit
ppm
ppm
ppm
Deg. F
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Recei\'ed Date:
Report Date:
24-May-95
12-Jun-95
Approved By: ~~
---,I'~++,-,,_r-----,, ur7'--<-ry ~hr-=-+--3
Project Manager
Method Time Date Analyst
SW 6010 18:10 05/31/95 KRR
SW 7470 10:30 06/02/95 TML
SW7740 09:20 06/01/95 KRR
SW-846 #909 10:00 05/30/95 TML
SW846 6010 08:19 06/01/95 KRR
SW846 6010 11:10 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW846 6010 11: 15 05/31/95 RCD
' SW846 6010 16:07 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW846 6010 07:37 06/01/95 KRR
SW846 6010 09:50 06/01/95 KRR
SW846 6010 08:20 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR
SW846 9040 08:20 05/30/95 RCD
I
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'-:-··--~ ~··· . ': '.;_: .
I 11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I Charlone, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Appro\'ed By: ~4frc ..
Lab ID: AA11901 R;b; urry 0
I Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date. Analyst, I"· -~-. '-~:: ) Oxidation Potential See Attached
Percent Water 96.10 % 17:00 05/30/95, JCH
I Total Dissolved Solids 4200 ppm EPA 209A 16:25 05/30/95 RCD
Chloride 55 5 ppm EPA 325.3 10:15 05/30/95 RCD
I Nitrate + Nitrite 17.6 5.0 ppm EPA 353.3 12:05 05/30/95 RCD
Total Phosphorus 2.35 .10 ppm EPA 365.3 10:30 05/30/95 RCD
Sulfate 710 I ppm EPA 375.4 09:50 05/31/95 RCD I Total Organic Carbon (TOC) 810 ppm EPA 415.1 17:00 05/30/95 JCH
I, I, 1,2-Tetrachloroethane UD 500 ppb EPA 8240 02:53 06/01/95 DLC
I I, 1,1-Trichloroethane UD 500 ppb EPA 8240 02:53 06/01/95 DLC
I, 1,2,2-Tetrachloroethane UD 1000 ppb EPA 8240 02:53 06/01/95 DLC
I I, 1,2-Trichloroethane UD 500 ppb EPA 8240 02:53 06/01/95 DLC ' I, 1-Dichloroethane UD 500 ppb EPA 8240 02:53 06/01/95 DLC
I, 1-Dichloroethcne UD 1000 ppb EPA 8240 02:53 06/01/95 DLC
I 1,2-Dichloroethane UD 500 ppb EPA 8240 02:53 06/01/95 DLC
1,2-Dichloropropane UD 500 ppb EPA 8240 02:53 06/01/95 DLC
I 2-Butanone UD 1200 ppb EPA 8240 02:53 06/01/95 DLC
2-Chloroethylvinyl ether UD 1000 ppb EPA 8240 02:53 06/01/95 DLC
I \ 2-Hexanone UD 500 ppb EPA 8240 02:53 06/01/95 DLC l\c_:/ )
· 4-Methyl-2-Pentanone UD 1000 ppb EPA 8240 02:53 06/01/95 DLC
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I
··'.':.. I; lJ\quaChem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I
I
I
I
I
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client #: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AAl1901
Sample ID: BG-47
Parameter
I}). i Acetone
Benzene
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Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Ethyl benzene
Methylene chloride
Stryene
Tetrachloroethene
, , Toluene
.,_). Total Xylenes
I
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit Unit
1600 ppb
500 ppb
500 ppb
500 ppb
1000 ppb
1000 ppb
500 ppb
500 ppb
1000 ppb
1000 . ppb
500 ppb
2000 ppb
500 ppb
500 ppb
500 ppb
1400 ppb
1000 ppb
500 ppb
500 ppb
500 ppb
North Carolina Certification Number: 305
South Carolina Certification Nuinber: 99032
Received Date:
Report Date:
Method
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
24-May-95
12-Jun-95 v ,✓,e:;rry~~ --~<'--~~ ?/
Project Manager
Time Date Analyst.
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC ' 02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 , DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
02:53 06/01/95 DLC
I
1,-•c•
lA~!!~o~~!~ao,.,om,,,o 1-' ·\ · l ') •~' .;,,/)
11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 l Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: R~'<ZJ Lab ID: AA11901
I Sample ID: BG-47 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst 1.,-,," -:."':.>1 i trans-1,2-Dichloroethene UD 500 ppb EPA 8240 02:53 06/01/95 DLC .:;,;.;;.:'
trans-1,3-Dichloropropene UD 500 ppb EPA 8240 02:53 06/01/95 DLC
I Trichloroethene UD 500 ppb EPA 8240 02:53 06/01/95. DLC
Vinyl chloride UD 1000 ' ·, ppb EPA 8240 02:53 06/01/95 DLC
I 1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
1,2-Dichlorobenzene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
1,3-Dichlorobenzene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM I 1,4-Dichlorobenzene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
2, 4,5-Trichlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 2,4,6-Tri,chlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
· 2,4-Dichlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 2,4-Dimethylphenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
2,4-Dinitrophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
2,4-Dinitrotoluene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 2,6-Dinitrotoluene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
2-Chloronaphthalene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
I 2-Chlorophenol UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
2-Methylnaphthalene UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
) 2-Methylphenol (o-cresol) UD 1000 ppb EPA 8270 17:51 05/31/95 ANM .~ 2-Nitroaniline UD 1000 ppb EPA 8270 17:51 05/31/95 ANM
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Bulk Group 48
Bulk Group De§eription: Acidic Liquid
Oxidizer
* Note: Bulk Groups were named aeeording to prelillllinary Daazardous
eategorization test and may not eorrespond to what the material
was elassified as for disposal.
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~~UM Hqua~nem ~nutr. Lib T-693 P.08
Certificate of A~alysis
Client:
Client#:
Contact:
Sample Date:
SDG#:
OHM Corporation
240 I Tuckascegce Road
Charlotte, NC
381
Jack Kilbarger
30-0ct-95
SDG-000315
Lab Sample ID: LSID-001191
Sample ID: BG-48
Parameter Result
I, I. I• Trichloroethane u
I, 1.2,2-Teliachloroethane u
U,2-Trichloroethane u
I, 1-Dichlorocthane u
I, 1-Dichloroethcnc u
1,2-Diohlorocthanc u
1,2-Dichloroethcnc u
1,2-Dichloropropane u
2-BUlailone u
2-Hcxanonc u
4-Methyl-2-pentanonc u
Acetone u
Benzene u
· Bromodichlorornethane u
Bromoform u
Bromomclhanc u
Ca,bon Disulfide u
Caibon Tetrachloride u
Chlurubcna:nc u
Chloroethane u
Chloroform u
Reporling
Limit Unit
s ppb
s ppb
s ppb
s ppb
s ppb
5 ppb
5 ppb
s ppb
10 ppb
10 ppb
10 ppb
10 ppb
5 ppb
5 ppb
5 ppb
10 ppb
5 ppb
5 ppb
s ppb
10 ppb
s ppb
Pa1111 9
Norlh Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date 30-0ct-95
Report Date: 17-Nov-9S
Approved By:
Kenneth R. RichardSlln
Project Manager
Method Time Date . Analyst
EPA8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA 8240 11/3/95 DLW,.
EPA8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA8240 11/3/9S DLW
EPA8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA 8240 1113195 DLW
EPA 8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA 8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA8240 11/3195 DLW
EPA 8240 11/3195 DLW
EPA8240 11/3/95 DLW
EPA8240 11/3/95 DLW
EPA 82◄0 · 11/3/95 . DLW
EPA 8240 11/3/95 DLW
EPA8240 11/3/95 DLW
NOV 17 '95 10:29 TO 3911147 FROM AquaChem Envir, Lab T-693 P,09
I
·~ ,s;
I f?e.1:~
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certif'ication Nwnber: 305
240 I Tuckascegee Road Sooth Carolina CertifiCAtion Number: 99032
I Charlotte, NC
Olent#: 381 Receipt Date 30-0ct-95
Contact: Jack Kilbarger Report Date: 17-Nov-95 I
Saotple Date: 30-0ct-95
I SDG#: S00-000315 Approved By:
Lab Sample ID:LSID-001191 · Kenneth R. Richardson
Sample ID: BG-48 Projed Manager I"~ Reportine: J Parameter Result Limit Unit Method Time Dale Analyst
I Chlorornethane u 10 ppb EPA8240 ll/3/95 DLW
cis-1,3-0ichloropropene u s ·.ppb EPA 8240 11/3/95 DLW
Dibromochloromethane u. s ppb EPA 8240 11/3/95 DLW I Etbylbenzene u 5 .· ppb EPA 8240 11/3195 DLW '
Methylene Chloride u s ppb EPA 8240 11/3/95 DLW
I Styrene u 5 ppb EPA 8240 11/3/95 DLW
Tetra.hloroethene u 5 ppb EPA8240 11/3/95 DLW
Toluene u s ppb EPA 8240 ll/3/95 DLW
I Total Xylenes u s ppb EPA 8240 11/3/95 DLW
trans-1,3-Dichloropropene u s ppb EPA8240 ll/3/95 DLW
Trichloroethene u 10 ppb EPA 8240 11/3/95 DLW
I Vwyl Acetate u 10 ppb EPA 8240 11/3/95 DLW
Vinyl Chloride u 10 ppb EPA 8240 11/3/95 DLW
1,2,4-Tricltlorobenzene u 5000 ppb EPA 8270 11/8/95 DLW I 1,2-Dichlorobenzcnc u 5000 ppb EPA 8270 11/8/95 DLW
· 1,3-Diehlorobcnzene u 5000 ppb EPA 8270 11/8195 DLW
1,4-Dichlorobenzcnc u 5000 ppb EPA 8270 11/8195 DLW I 2,4,5-Trichlorophenol u 5000 ppb EPA8270 11/8/95 DLW
2,4,6-Trichlorophcnol u 5000 ppb EPA 8270 11/8195 DLW .~;_) 2,4-Dithloropheool u 5000 ppb EPA 8270 11/8/95 DLW
2, 4-Dlmcthylphenol u 5000 ppb EPA 8270 11/8195 DLW
I PallC 10
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NUV 1( '95 H):~ TO. 3911147 FROM Aqua.Chem Enuir, Lab T-693 P. 10
Certifi~ate of Analysis
Client:
Client 1#:
Contact:
Sample Date:
SDG/1:
OHM Corporation
240 I Tuclcaseegee Road
Chartoite, NC
381
Jack Kllbarger
30-0ct-95
SDG-000315
Lab Sample ID: LSID--001191
Sample ID: BG-48
Parameter Result
2,4-Dinitrophenol u
2,4-Dinitrotolnene ·U
2.6-Dinitrotolnene t:
2-Chloronaphthalene u
2-Chlorophenol u
2-Melhlyphcnol {o-crcsol) u
2-Methylnaphthalene u
2-Nilroanilinc u
2-Nitrophenol u
3,3-Dichlorobcnzidiru: u
3-Nitroaniline u
4,6-Dinitro-2-methylphenol u
4-Bromophenyl phenyl ether u
4-Chloraniline u
4-Chloro-3-methylphcnol u
4-Chlorophenyl phenyl ether u
4-Mcthylphcool (p-creool) u
4-Nitroanilinc u
4-Nitrophenol u
A~hthcnc u
Acenaphthylenc u
Reporting
Umlt Unit
5000 ppb
5000 ppb'
5000 ppb .
5000. ppb
5000 ppb
5000 ppb
5000 ppb
sooo ppb
5000 ppb
5000 ppb
5000 ppb
12500 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
12500 ppb
5000 ppb
5000 ppb
Pue 11
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date 30-0ct-95
Report Date: I 7-Nov-95
Approved By:
Kenneth R. Rlclu.rdJod
Project Manager
Method Time Date
. EPA 8270 11/8/95
EPA8270 11/8/95
EPA 8270 11/8/9S
EPA 8270 11/8/95
EPA8270 11/819S
EPA 8270 1118195
EPA 8270 11/8195
EPA8270 11/8/95
EPA 8270 1118195
EPA 8270 11/8195
EPA 8270 1118195
EPA 8270 1118195
EPA 8270 1118195
EPA 8270 11/8195
EPA 8270 11/8195
EPA 8270 11/8195
EPA 8270 1118195
EPA8270 IL'S/95
EPA8270 11/8195
EPA8270 lliS/95
EPA8270 11/8/95
Analyst
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
I •~ ay:
I
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t ' j
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I
Certificate of Analysis
Client:
Client#:
Contact:
Sample Date:
SDG#:
OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
381
Jack Kilbarger
30-0ct-95
SDG-000315
Lab Sample ID: LSID--001191
Sample ID: BG-48
Parameter Result
Anthracene u
Benzo (a) anthracene u
Benzo (a) pyrene u
Bcnzo (b) fluoranthene u
Bcnzo (ghi) pe,ylcnc u
Bcnzo (k) fluoranthcnc u
Bcnzoic acid u
Benzyl alcohol u
Bis (2<hloroethoxy) methane u
Bis (2-chloroethyl) ether u
Bis (2<hloroisoprobyl) ether u
Bis (2-<:thylhcxyl) phthalate u
. Butyl benzyl phthalate u
Chrysene u
Di-n-butyl phthalatc u
Di-n-octylphthalate u
Dibenzo (ah) anthraccnc u
DibenzoJ\Jran u
Dlelhylphthalalc u
Dimetllylphthalate u
Fluoranthenc u
Reporting
Limit Unit
5000 ppb
sooo ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
S000 ppb
5000 ppb
5000 ppb
5000 .ppb
5000 ppb .
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
Pa11e 12
North CaroUna Certlncatlon Number: 305
South Carolina Certiricatlon Number: 99032
Receipt Date 30-0ct-95
Report Date: 17-Nov-95
Approved By:
Kenneth R. Richardson
Project Manager
Method Time · Date
EPA 8270 11/8/95
EPA8270 11/8/95
EPA 8270 11/8/9S
EPA 8270 1118/95
EPA 8270 11/8/95
EPA 8270 1118/95
EPA8270 I 1/8195
EPA 8270 l 1/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA 8270 ll/8/95
EPA 8270 11/8/95
EPA 8270 1118/95
EPA 8270 11/8/95
EPA 8270 1118195
EPA 8270 11/8/95
EPA 8270 11/8195
EPA 8270 11/8195
EPA 8270 11/8195
EPA 8270 11/8/95
.A■alyst
DLW ·
DLW
DLW
DLW'·
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
· DLW
DLW
DLW
I
1 ..
•:-~::_.:!';
I
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I
NOV 17 '95 10:31 TO 3911147 FROM AquaChe111 t:.nu,r. Lab T-693 P.12
..
Certificate of AnaJysis
Client:
Client#:
Contact:
Sample Date:
SDG#:
OHM Corporation
240 l Tuckaseegee Road
Charlotte, NC
381
Jack Kilbargcr
30-0ct-95
SDG--00031 S
Lab Sample ID: LSID-001191
Sample ID: BG-48
Parameter Result
Fluorene u
Hexachlorobenzene u
Hexachlorobutadiene u
Hexnchlorocyclopentadiene u
Hexachlorocthanc u
lndcno (l,2,3-cd) pyrcnc u
l,uphoronc u
N-Nitroso-di-n-propylamine u
N-Nltrosodlphenylamine u
Naphibalcnc 5400
Nitroben1.ene u
Pc:nlBCh!oroph:nol u
. Phcnantbrenc u
Phenol u
Pyrenc u
Reporting
Limit Unit
5000. ppb
S000 ppb
S000 ppb'
S000 ppb
5000 ppb
S000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
5000 ppb
Paae 11
North Carolina Certification Number: 305
South Carolina Certlflcatlon Number: 99032
Receipt Dt.te 30-0ct-95
Report Date: l 7-Nov-95
Appro,·cd By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA8270 11/819S
EPA8270 11/8/95
EPA 8270 11/8/9S
EPA 8270 11/8/95
EPA 8270 11/8/95
EPA8270 11/8/95
EPA8270 11/8195
EPA8270 11/8/95
EPA8270 11/8/95
EPA 8270 11/8/95
EPA 8270 1118195
EPA8270 11/8/95
EPA8270 11/8195
EPA8270 11/8195
EPA 8270 11/8/95
Analyst
DLW
DLW
DLW
DLW ,
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
DLW
I
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I
I
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I
ID
I
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I
I ...,~,J '•..::•-=-"-------
Certificate of Analysis
Clfent: OHM Corporation
240 I Tuckascegee Road
Charlotte, NC
Client#: 381
Contact: JackKilbarger
Sample Date: 30-0ct-95
SDG#: SDG-000315
Lab Sample ID: LSID--001192
Sample ID: BG-48
Parame1er
Percent Water
Density
British Thennal Unit
roe
Total Organic Halides
Result .
94.6
1.124
IOOOU
22600
IOOOU
Reporting
Limit Unit
·o percent
0
l000 ppm
0 ppm
1000 ppm
Pue 14
North Carolina Certificadon Number: 305
South Carolina Cert111cadon Number: 9903;
Receipt Date 30-0ct-9S ·
Report Date: 17-Nov-95
Approved B1:
Kenneth R. RlchardJon
Project Manager
Method Time Date
ASSTM D 1298.SS
ASTMD20l5
EPA415.l
EPA9020
Analyst
JCH
JCH
JCH
JCH
JCH
,....,..,. .. , ~,J _.W•-,,._, ,J.., ...... --.,
I·
I-;_·:.<'~ ,,:,
I Pre/,'~
I Certificate of Analysis
Client: OHM <'.orporation North Carolina Certification :"llumber: 305 I 240 I Tuckaseegee Road South Carolina Certification Number: 99032 · Charlotte, NC
I Client#: 381 J . Receipt Date 30-0ct-95
Contact: Jack Kilbargcr Report Date: 17-Nov-95
I Sample Date: 30-0ct-95
SDGII: SDG-000315 Approved By:
I Lab Sampl~ ID: LSID--001193 Kenneth R. Richardson
Sample ID: BG-48 Project Manager r·•. Reporting
' J Parameter Result Llmit Unit Method Time Date Analyst .:_;;-'
Arr.enic 0.615 0.005 ppm EPA 7470 I 1/10/95 DLW
I pH 2,07 0 5U EPA ISO.I 11:30 10/31/95 RCD Acidity 504000D 6000 ppm EPA305.l 14:50 10/31/95 RCD Aluminum 33.4D O.S ppm· EPA6010 11:00 11/10/95 RCD I Antimony u 0 ppm EPA6010 11/10/95 DLW Barium 1.3D o.s ppm EPA6010 13:55 11/9/95 RCD BcryUium L'D 0.05 ppm EPA6010 9:05 11/10/95 RCD I <'Jldmium 0.15D 0.05 ppm ill'AGOIO I I :05 11/9/95 RCD Calcium 202DE O,S ppm EPA6010 9:05 11/10/95 RCD Chromium 6.45D 0.25 ppm EPA6010 11:05 ll/9/95 RCD I Cooalt L'D 0.05 ppm EPA6010 12:35 11/10/95 RCD Iron 540DE 0.5 ppm EPA6010 9:05 11/10/95 RCD
I Magnesium 33.4D 0,5 ppm EPA 6010 9:05 11/10/95 RCD Manganese 37.9D 0,5 ppm EPA6010 9:05 11/10/95 RCD Nickel 351DE 1.5 ppm EPA 6010 11:05 11/9/95 RCD
I Potamum 38,5D · s ppm EPAGOIO 15:'5 I 1/9195 RCD Silver 0.15D 0.05 ppm EPA6010 11:05 11/9195 RCD Sodium 355D s ppm EPA6010 16:35 11/9/95 RCD
I Vanadium 0.50D 0.05 ppm EPA601U 9:05 11/10/'JS RCD Ziric 124SDE o,s ppm EPA'6010 11:05 11/9/95 RCD ,~, Lead 3,60D U.25 ppm EPA 7470 11:0S 11/9,'95 RCD
Paae 15
I Puc 16
I
•.,:-:c,.~
•
?~;, l Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I
I
I
I
I
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG#: SV223080
Lab ID: Ml3853
Sample ID: BG-48
l(~t~arameter
s_~'' Oxidation Potential
I
I
I
I
I
I
I
Percent Water
Total Dissolved Solids
Acidity
Chloride
Nitrate
Nitrite
. Total Phosphorus
Sulfate
Total Organic Carbon (TOC)
l, l, 1,2-Tetrachloroethane
1,1, !-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
l, 1-Dichloroethene
1,2-Dichloroethane
... 1,2-Dichloropropane ' . -,
1(--.,; 2-Butanone .
· 2-Chloroethylvmyl ether
I
Detection
Result Limit
490
78.60
100,000 62
2.50
Can Not Test
Can Not Test
Can Not Test
Can Not Test
Can Not Test
120000
U D 200000
U D 200000
UD 200000
U D 200000
U D 200000
U D 200000
U D 200000
UD 200000
U D 240000
U D 200000
. Unit
mv
%
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
Received Date: 27-Jul-95
Report Date: I -Aug-95
Project Manager
Method Time
11:00
09:00
EPA 209A 14:00
EPA 305.1 10:06
EPA 325.3
EPA 352.1
EPA 354.1
EPA 365.3
EPA 375.4
EPA 415.1
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA8240
EPA 8240
EPA 8240
EPA 8240
EPA8240
EPA 8240
13:00
14:59
14:59
14:59
14:.59
14:59
14:59
14:59
14:59
14:59
14:59
Date · Analyst
08/09/95 . JCH
08/02/95 JCH
08/03/95 DLC
08/10/95 KRR
08/03/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
JCH
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
I
•-~-Jf_ .
l;:6
; ~~~~O~M:N~A~~BORATORIES, INC.
11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I
I
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
I Contact: Mr. Randy Bennett Report Date: 15-Aug-95
SDG#: SV223080
I Lab ID: AAl3853 Ke eth R Richardson
Sample ID: BG-48 Project Manager
Detection I 't7arameter Result Limit Unit Method Time Date Analyst -· . UD 200000 14:59 08/02/95 2-Hexanone ppb EPA 8240 ANM
I 4-Methyl-2-pentanone UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
Acetone .UD 340000 ppb ·. EPA 8240 14:59 08/02/95 ANM
Benzene UD 380000 ppb · EPA 8240 14:59 08/02/95 ANM I Bromodichloromethane UD 200000 ppb EPA 8240 14:59 08/02/95 ANM'·
Bromoform UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I Bro mo methane UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
Carbon disulfide UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I Carbon tetrachloride UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
Chlorobenzene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
Chlorodibromomethane UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I Chloroethane UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
Chloroform UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I Chloromethane UD 220000 ppb EPA 8240 14:59 08/02/95 ANM
cis-1,2-Dichloroethene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
cis-1,3-Dichloropropene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I Ethylbenzene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
.-• Stryene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
l"--)Tetrachloroethene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
• Toluene UD 200000 ppb EPA 8240 14:59 08/02/95 ANM
I
I
Ir?~-'·
-:;:s AquaChem I f ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I
I Client:
Certificate of Analysis
OHM Corporation North Carolina Ce"rtification Number:
240 I Tuckaseegee Road South Carolina Certification Number:
.Client#:
Charlotte, NC
3080 Received Date: 27-Jul-95
1 C.ontact: Mr. Randy Bennett Report Date: J5-Aug-95
SDG#: SV223080 I Lab ID: AA13853
Sample ID: BG-48 Project Manager
Detection
1·;,::=::ameter Result Limit Unit Method Time Date 0"
Total Xylenes UD 200000 ppb EPA 8240 14:59 08/02/95
I trans-1,2-Dichloroethene .UD 200000 ppb EPA8240 14:59 08/02/95
trans-1,3-Dichloropropene UD 200000 ppb EPA 8240 14:59 08/02/95
Trichloroethene UD 200000 ppb EPA8240 14:59 08/02/95
I Vinyl chloride UD 200000 ppb EPA8240 14:59 08/02/95
1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 15:53 08/02/95
I 1,2-Dichlorobenzene UD 1000 ppb EPA 8270 15:53 08/02/95
1,3-Dichlorobenzene UD 1000 ppb EPA 8270 15:53 08/02/95
1,4-Dichlorobenzene UD 1000 ppb EPA 8270 15:53 08/02/95 I 2, 4,5-Trichlorophenol UD 1000 ppb EPA 8270 15:53 08/02/95
2,4,6-Trichlorophenol UD 1000 ppb EPA 8270 15:53 08/02/95
I 2,4-Dichlorophenol UD 1000 ppb EPA 8270 15:53 08/02/95
2,4-Dimethylphenol UD 1000 ppb EPA 8270 15:53 08/02/95
I 2,4-Dinitrophenol UD 1000 ppb EPA 8270 15:53 08/02/95
2,4-Dinitrotoluene UD 1000 ppb EPA 8270 15:53 08/02/95
2,6-Dinitrotoluene UD 1000 ppb EPA 8270 15:53 08/02/95
I 2-Chloronaphthalene UD 1000 ppb EPA 8270 15:53 08/02/95
•0 -Chlorophenol UD 1000 ppb EPA 8270 15:53 , 08/02/95 I~ k1e1hylnaphthalene UD 1000 ppb EPA 8270 15:53 08/02/95
2-Methylphenol (o-cresol) UD 1000 ppb EPA 8270 15:53 08/02/95
I
305
99032
Analyst
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
.,;:;1 .. ·
I
I. l A~!!~o5~~~•omos,es, '"'
\:i)-;·
I
11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I
I
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
I Contact: Mr. Randy Bennett Report Date: 15-Aug-95
Approved B : SDG#: SV223080
I Lab ID: AAl3853
Sample ID: BG-48 Project Manager
Detection
1·::\Parameter Result Limit Unit Method Time Date Analyst
•-...:.~~-
: 2-Nitioaniline UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I 2-Nitrophenol UD 1000 ppb EPA 8270 15:53 08/02/95 · ANM
3-Nitroaniline UD 1000 ppb, EPA 8270 15:53 08/02/95 ANM
4,6-Dinitro-2-methylphenol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM I 4 ,6-Dinitro-o-cresol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
4-Bromophenyl phenyl ether UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I 4-Chloro-3-methylphenol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
4-chloroaniline UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
4-Chlorophenyl phenyl ether UD 1000 ppb EPA 8270 15:53 08/02/95 ANM I 4-Methylpheriol (p-cresol) UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
4-Nitroaniline .UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I 4-Nitrophenol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Acenaphthene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Acenaphthylene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Benzo(a)anthracene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Benzo(a)pyrene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Benzo(b)fluoranthene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Benzo(ghi)perylene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM 1t-j Benzo(k)fluoranthene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
· Bis(2-chloroethoxy) methane UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I
I
•= ~ f:!:1 {_A.qua Chem I ENVIRONMENTAL LABORATORIES, INC.
/ 11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: I SDG#: SV223080
I Lab ID: AA13853
Sample ID: BG-48 Project Manager
Detection
_ l(?\Pararneter Result Limit Unit Method Time Date 'Analyst
/"'-.;...~
1000 15:53 08/02/95 ,_. Bis(2-chloroethyl) ether UD ppb EPA 8270 ANM
I Bis(2-chloroisopropyl) ether UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Bis(2-ethylhexyl) phthalate UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Butyl benzyl phthalate UD 1000 ppb' EPA 8270 15:53 08/02/95 ANM
I Chrysene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Di-n-butyl phthalate UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Di-n-octyl phthalate UD 1000 ppb EPA 8270 15:53 · 08/02/95 ANM
Dibenzo(ah)anthracene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Dibenzofuran UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Diethylphthalate UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Dimethylphthalate .UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Fluoranthene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Fluorene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Hexachlorobenzene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM I Hexachlorobutadiene UD . 1000 ppb EPA 8270 15:53 08/02/95 ANM
Hexachlorocyclopentadiene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Hexachloroethane UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Indeno( 1,2,3-cd)pyrene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM (. ·.-·\
;(;:;.-; Isophorone UD 1000 ppb EPA 8270 15:53 08/02/95 ANM I'·· N-Nitroso-di-n-propylamine UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I
I
1-~ .. ·'.: ..,,.\
<s AquaChem I f...:. ENVIRONMENTAL LABORATORIES, INC.
---11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 15-Aug-95 I SDG#: SV223080 Approyed Bv:
I Lab ID: AAl3853 Kenn R. Richardson
Sample ID: BG-48 Project Manager
Detection
1:7\Parameter Result Limit Unit Method Time Date Analyst • < . _ . .,
--, N-Nitiosodiphenylamine UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Naphthalene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
Nitrobenzene UD 1000 ppb, EPA 8270 15:53 08/02/95 ANM
Pentachlorophenol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Phenanthrene UD 1000 ppb EPA 8270 15:53 08/02/95 ANM'
Phenol UD 1000 ppb EPA 8270 15:53 08/02/95 ANM
I Pyrene UD/ 1000· ppb EPA 8270 15:53 08/02/95 ANM
Total Suspended Solids 200,000 1 ppm SM209C 13:30 08/03/95 DLC
Total Organic Halide (fOX) u 1.0 ppm SM 506' 14:00 08/04/95 JCH
I Barium 1.7 0.5 ppm SW 6010 10:55 08/03/95 RCD
Cadmium 0.25 0.05 ppm SW 6010 10:45 08/08/95 RCD
I Chromium 20.8 0.25 ppm SW 6010 10:45 08/08/95 RCD
Copper 83D 1.0 ppm SW 6010 10:05 08/14/95 RCD
Iron 1850D 5.0 ppm SW 6010 09:15 08/03/95 RCD I Nickel 310D 15 ppm SW 6010 14:10 08/14/95 RCD
Silver u 0.05 ppm SW 6010 10:45 08/08/95 .RCD
1. Zinc 2015D 5 ppm SW 6010 10:05 08/14/95 RCD
Arsenic 0.055 0.025 ppm SW7060 10:30 08/03/95 RCD
. ) L d 160D 2.5 SW 7421 10:05 08/14/95 RCD .....:..,.,,-ea. ppm I-·· Mercury u 0.004 ppm SW 7471 08:30 08/10/95 KRR
I
I
I, ... ]l_
l;/}~~~~O~N~:~BORATORIES, INC ..
11176 Downs Road
I Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
I Client#:
1 Contact:
SDG#:
I Lab ID:
Sample ID:
ITJarameter
Selenium
I Flash Point
Aluminium
I Antimony
Beryllium
Calcium
I Cobalt
Magnesium
I Manganese
Potassium
Sodium
I Thallium
Vanadium
I PH
I
I
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
3080
Mr. Randy Bennett
SV223080
AAl3853
BG-48
Detection
Result Limit ·unit
0.007 0.025 ppm
80 70 Deg. F.
20.8 0.5 ppm1
u 0.050 ppm•
u 0.05 ppm
750D 5.0 ppm
u 0.05 ppm.
240D 0.5 ppm
43.5 0.25 ppm
33.7 5.0 ppm
300D 50 ppm
u 0.050 ppm
0.35 0.25 ppm
2.50 0-14 SU
Received Date: 27-Jul-95
Report Date: -Aug-95
Approved
e eth R. Richardson
Project Manager
Method Time Date
SW7740 14:20 08/03/95
SW-846 #909 10:15 08/10/95
SW846 6010 09:40 08/04/95
. SW846 6010 14:40 08/07/95
SW846 6010 14:30 08/02/95
SW846 6010 09:15 08/03/95
SW846 6010 11:30 08/07/95
SW846 6010 09:15 08/03/95
SW846 6010 14:30 08/02/95
SW846 6010 12:10 08/07/95
SW846 6010 14:20 08/03/95
SW846 6010 08:40 08/07/95
SW846 6010 14:30 08/02/95
SW846 9045 10:06 08/10/95
Analyst
RCD
··KRR
RCD
RCD
RCD,
RCD
RCD
RCD
RCD
RCD
RCD
RCD
RCD
KRR
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Bulk Group 49
Bulk Group Description: Organie Flammable
Liquid Chlorinated
* Note: Bulk Groups were named aeeording to preliminary hazardous
eategorization test and may not eorrespond to what the material
was elassified as for disposal.
I
·.I}A~:!~01£?,,~,~~,omom. "c
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I Certificate of Analysis
OHM Corporation I Client:
lclient #:
240 I Tuckaseegee Road
Charlotte, NC
Contact:
lsDG#:
Lab ID:
.Sample ID:
3080
Mr. Randy Bennett
SV243080
AAl3855
BG-49
Parameter I' 0
\rcent Water .....,.:_.) .
Arsenic I Barium
Cadmium·
I Chromium
Lead
Mercury I Selenium
Silver
I Total Dissolved Solids
Total Organic Carbon (TOC)
1, I, 1,2-Tetrachloroethane
11,1,1-Trichloroethane
I, 1,2,2-Tetrachloroethane
11,1,2-Trichloroethane
1, 1-Dichloroethane
I
1, 1-Dichloroethene
1,2-Dichloroethane
.. '. ,2-Dichloropropane
-.:-L· utanone I,. /B
I
Detection
Result Limit
0.86
0.30D 0.125
32.7 0.5
0.40 0.05
10.4 0.25
169D 2.5
u 0.004
u 0.025
u 0.05
7,800,000 62
960000
UD 45450
1,500,000 DE 45450
UD ·45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
3,300,000 DE 54540
Unit
%
mg/L
mg/L
mg/L ·.
mg/L
mg/L
mg/L
mg/L
mg/L
ppm
ppm
ppb
ppb
ppb
ppb
ppb
ppb
ppb
pp~
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receiyed Date: 27-Jul-95
Report Date: . l 5-Aug-9,-5_ "_.::::.:::_-°"-~--
Project Manager
Method Time Date Analyst
09:00 08/02/95 JCH
1311/6010 10:30 08/03/95 RCD
1311/6010 10:55 08/03/95 RCD
1311/6010 10:45 08/08/95 RCD
1311/6010 10:45 08/08/95 RCD
1311/6010 10:05 08/14/95 RCD
1311/6010 08:30 08/10/95 KRR
1311/6010 14:20 08/03/95 RCD
1311/6010 10:45 08/08/95 RCD
EPA209A 14:00 08/03/95 DLC
EPA 415.1 13:00 08/03/95 JCH
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 · 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
I
,,~quoChem .
1-/, ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I Ce~tificate of Analysis
OHM Corporation llient:
llient #:
240 I Tuckaseegee Road
Charlotte, NC
Contact:
IDG#:
Lab ID:
.ample ID:
3080
Mr. Randy Bennett
SV243080
AAl3855
BG-49
.rarameter •
l__':fhloroethylvinyl ether
2-Hexanone
14-Methyl-2-pentanone ·
Acetone
~enzene
llaromodichloromethane
Bromoform 1B romomethane
Carbon disulfide
•
Carbon tetrachloride
Chlorobenzene
. Chlorodibromomethane
IChloroethane
Chloroform
I
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
IEthylbenzene
· :' ,thylene chloride
.• :;,J•ene
I
Detection
Result Limit
UD 45450
UD 45450
3,400,000 DE 45450
UD 77265
UD 86355
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 45450
UD 49995
UD 45450
UD 45450
2,500,000 D E 45450
UD 63630
UD 45450
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: 5-Aug-95
Kenn th R. Richardson
Project Manager
Method Time Date Analyst
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA8240 18:10 08/02/95 ANM
EPA8240 18: 10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA8240 18:10 08/02/95 ANM·
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18:10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
EPA 8240 18: 10 08/02/95 ANM
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I
Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date:
I ' SDG#: SV243080
Lab ID: AAl3855
I Sample ID: BG-49 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
·~)Tetrachloroethene 1,900,000 DE 45450 ppb . EPA 8240 18: 10 08/02/95 ANM -..;:,_.• .
Toluene 2,400,000 DE 45450 ppb EPA 8240 18:10 08/02/95 ANM
I Total Xylenes 13,000,000 D 45450 ppb EPA 8240 18:10 08/02/95 ANM
trans-1,2-Dichloroethene UD 45450 ppb' EPA 8240 18:10 08/02/95 ANM
I trans-1,3-Dichloropropene UD 45450 ppb . EPA 8240 18:10 08/02/95 ANM
Trichloroethene 330,000 D 45450 ppb EPA8240 18:10 08/02/95 ANM
Vinyl chloride UD 45450 ppb EPA 8240 18:10 08/02/95 ANM
I 1,2, 4-Trichlorobenzene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
1,2-Dichlorobenzene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I 1,3-Dichlorobenzene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
1,4-Dichlorobenzene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
2,4,5-Trichlorophenol UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I 2,4,6-Trichlorophenol UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
2,4-Dichlorophenol UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I 2,4-Dimethylphenol UD .1000 ppb EPA 8270 20:05 08/02/95 ANM
2,4-Dinitrophenol UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I 2,4-Dinitrotoluene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
2,6-Dinitrotoluene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
(/ .. ,2-Chloronap~.thalene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM 10 2-Chlorophenol UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I
I
I.~, Jh C
l:t:} ~~~~ONMEN~:~BORATORIES, INC.
I
'
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
Client: OHM Corporation I 240 I Tuckaseegee Road
Charlotte, NC
I Client#:
Contact:
3080
Mr. Randy Bennett
I SDG#: SV243080
Lab ID: AA13855
I Sample ID: BG-49
Parameter . Result
l't) 2-Methylnaphthalene UD
"'-·'' .
2-Methylphenol (o-cresol) UD
I 2-Nitroaniline UD
2-Nitrophenol UD
I 3-Nitroaniline UD
4,6-Dinitro-2-methylphenol UD
4 ,6-Dinitro--0-cresol UD
I 4-Bromophenyl phenyl ether UD
4-Chloro-3-methylphenol UD
I 4-chloroaniline UD
4-Chlorophenyl phenyl ether UD
4-Methylphenol (p-cresol) ·UD
I 4-Nitroaniline UD
4-Nitrophenol UD
I Acenaphthene UD
Acenaphthylene UD
Benzo(a)anthracene UD I Benzo(a)p}Tene UD
1;. : ... __ Benzo(b)fluoranthene UD
,-~) Benzo(ghi)perylene UD
I
.
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb
' ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date:
Project Manager
Method Time Date Analyst
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
' EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
I
·~ 1r} l A~~~06EN~A:~BORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
I Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 5-Aug-95
I SDG#: SV243080
Lab ID: AA13855
I Sample ID: BG-49
Detection
Parameter . Result Limit Unit Method Time Date Analyst It:) Benzo(k)fluoranthene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Bis(2-chloroethoxy) methane UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Bis(2-chloroethyl) ether UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Bis(2-chloroisopropyl) ether UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Bis(2-ethylhexyl) phthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Butyl benzyl phthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Chrysene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Di-n-butyl phthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Di-n-octyl phthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Dibenzo(ah)anthracene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Dibenzofuran UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Diethylphthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Dimethylphthalate UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Fluoranthene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Fluorene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Hexachlorobenzene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I Hexachlorobutadiene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
Hexachlorocyclopentadiene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
V: ·. , Hexachloroethane UD 1000 ppb EPA 8270 20:05 08/02/95 ANM f :.c::_) Indeno( 1,2,3-cd)pyrene UD 1000 ppb EPA 8270 20:05 08/02/95 ANM
I
I
I,
afb,
I
I
I
I
I
I
LA~~~os~.~~oo,m,,,,. '"
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
'
Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckasecgee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date:
SDG#: SV243080
Lab ID: AAl3855
Sample ID: BG-49 Project Manager
Detection
Parameter . Result Limit Unit Method Time Date l:0 I~ophorone UD
UD
UD
UD
UD
UD
UD
UD
UD
460,000
u
1000 ppb EPA 8270
Analyst
20:05 08/02/95 ANM
I
I
I
I
I
I
I
N-Nitroso-di-n-propylarnine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
Total Suspended Solids
Total Organic Halide (TOX)
BTU
Flash Point
PH
· 16120
>200
4.85
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
1000 ppb
I ppm
1.0 ppm
BTU/gal
70 Deg.F
0-14 SU
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
'· EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
EPA 8270 20:05 08/02/95 ANM
SM209C 13:30 08/03/95 DLC
SM506 14:00 08/04/95 JCH
SW-846 #909 08:00 08/02/95 JCH
SW-846 #909 10: 15 08/10/95 KRR
SW846 9045 09:55 08/10/95 KRR
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Bulk Group 51
Bulk Group Description: Neutral Solid
• Note: Bulk Groups were named aeeording to preliminary hazardous
eategorization test and may not correspond to what the material
was classified as for disposal.
I
I
.. /AquaChem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina· Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
I SDG#: SR633080 Approved By: ~ Lab ID: AAll902
I Sample ID: BG-51 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
l',s) ) Arsenic 0.012 0.005 mg/L 1311/6010 13:45 05/30/95 KRR .:· ..
~~
Barium 1.4 0.1 mg/L 1311/6010 14:50 06/01/95 RCD
I Cadmium 0.01 0.01 mg/L 1311/6010 17:48 06/01/95 RCD
Chromium 1.73 0.05 mg/L 1311/6010 17:48 06/01/95 RCD
Lead 1.83 0.05 mg/L 1311/6010 17:48 06/01/95 RCD I MercUI}' u 0.0002 mg/L 1311/6010 10:30 06/02/95 TML
Selenium u 0.005 mg/L 1311/6010 15:00 05/30/95 KRR
I Silver 0.01 0.01 mg/L 1311/6010 17:48 06/01/95 RCD
Chlorodane u 0.010 mg/L 131118080A 12:43 06/08/95 RAG
I Emlrin u 0.010 mg/L 1311/8080A 12:43 06/08/95 RAG
Heptachlor u 0.010 mg/L 1311/8080A 12:43 06/08/95 RAG
Heptachlor epoxide u 0.010 mg/L 13 I l/8080A 12:43 06/08/95 RAG
I ' Lindane u 0.010 mg/L 131118080A 12:43 06/08/95 RAG
· Methoxychlor u 0.010 mg/L 1311/8080A 12:43 06/08/95 RAG
I Toxaphene u 0.010 mg/L 1311/8080A 12:43 06/08/95 RAG
2,4,5-TP (Silvex) u 0.010 mg/L 1311/8150 14:07 06/06/95 RAG
2,4-D u 0.010 mg/L 1311/8150 14:07 06/06/95 RAG I 1, 1-Dichloroethylene u 0.250 mg/L 1311/8260 17:38 06/01/95 DLC
I 1,2-Dichloroethane u 0.250 mg/L 13 I 1/8260 17:38 06/01/95 DLC 10/ 1,4-Dichlorobenzcne u 0.250 mg/L 1311/8260 17:38 06/01/95 DLC
I
I
LA~~~o~~!~oomom '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I
I
I
I
I
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
Charlotte, NC
3080
Mr. Randy Bennett
SR633080
AAll902
BG-51
ie5) 1 Benzene
I
I
I
I
I
I
Carbon tetrachloride
Chlorobenzene
Chloroform
Methyl ethyl ketone
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
2, 4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
m-Cresol
Nitrobenzene
o-Cresol I p-Cresol
,·, . , ) Pentachlorophenol
•. ~_:./ ' Pyridine
I
Result
u
u
.U
u
u
u
u
u
UD
UD
UD
UD
UD
UD
0.087 DJ
UD
0.050 DJ
0.087 DJ
UD
UD
Detection
Limit
0,250
0.250
0.250
0.250
0.250
0,250
0,250
0.250
0,10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.10.
0. 10
Unit
mg/L
mg/L
mg/L
ing/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Received Date:
Report Date,:
Approved By:
24-May-95
12-Jun-95
~···o
Project Manager
Method Time Date Analyst.
1311/8260 17:38
1311/8260 17:38
1311/8260
1311/8260
1311/8260
1311/8260
1311/8260
1311/8260
1311/8270
1311/8270
1311/8270
1311/8270
1311/8270
1311/8270
1311/8270
1311/8270
1311/8270 ,
1311/8270
1311/8270
1311/8270
17:38
17:38
. 17:38
17:38
17:38
17:38
11:39
11:39
11:39
11:39
11:39
11:39
11:39
11 :39
11:39
11 :39
11:39
11:39
06/01/95 DLC
06/01/95 DLC
06/01/95
06/01/95
06/01/95
06/01/95
06/01/95
06/01/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
06/02/95
DLC
DLC
DLC
DLC
DLC
DLC
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
I
' A~~~ol!?.~;~,omoa,e, '"c
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I
I
I
I
I
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
I
I
I
I
I
Client#:
Contact:
SDG#:
Lab ID:
3080
Mr. Randy Bennett
SR633080
AA11902
Sample ID: -BG-51
Parameter
·,i Total Organic Carbon (TOC)
Total Organic Halide (TOX)
Paint Filter
Corrosivity
BTU
Flash Point
Reactive Cynide
Reactive Sulfide
PH
I
1·:~•·J
I
Result
115,000
<1.0
Positive
12.35
2640
>220
Negative
Negative
12.35
Detection
Limit
1.0
0-14
70
0-14
Unit
ppm
ppm
s.u.
BTU/gal
Deg. F
ppm
ppm
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: 12-Jun-95
Method Time Date Analyst
EPA 415.1 17:00 05/30/95 JCH
SM506 17:00 05/30/9_5 JCH
SW846 10:00 05/28/95 TML
SW-846 #111 08:20 05/30/95 RCD
SW-846 #909 17:00 05/30/95 JCH
SW-846 #909 10:00 05/30/95 TML
SW846 9010 11:00 05/31/95 TML
SW846 9030 11:00 05/31/95 TML
SW846 9045 08:20 05/30/95 RCD
'
HUll .::::..=i "':IJ lb:...J4 ,IJ . .)'jl.ll'-4( l""t(Ul"I Hqua1,,.,:1em ~.,v\r, L..ao 1--.Jo::i r-. t:r.1. .
••••
I,~ LA~~~os.~!~""'""· ,so .{)
11178 Downs Road
I
Plnavllle, NC 28134
704/583-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolin• Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I
Charlot1e, NC
Client#: 3080 Rtceived Date: 27-Jul-95
Contact: Mr. Randy Bennett Rfport Date: 22-Aug-95
I SDG/1: SV233080 Approved By: &:F· 0 Lab ID: AA!3854
I Sample ID: BG--61 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst 1-~~ Percent Water 86.10 '% 09:00 08/02/95 JCH ·(-:i
.;:.::.:,./ Cyanide u 0.025 EPA 335.2 17:00 08/17/95 DRW ppm
I Sulfide 131 5.0 ppm EPA 376.l 17:00 08/17/95 DRW
Total Organic Carbon (TOC) 85000 1 ppm EPA-US.I 13:00 08/03/95 JCH.
I
!, l, l,2-Tetrachlorocthane UD 38460 ppb" EPA8240 B:56 08/02/95 ANM
I l ,l,1-Trichlorocthane 180,000 D 38460 ppb EPA8240 1S:S6 08/02/95 ANM
l, l,2,2-Tetrachlorocthane UD 38460 ppb EPA8240 15:56 08/02/95 ANM
I l, !,2-Trichlorocthane UD . 38460 ppb EPA 8240 15:56 08/02/95 ANM
I, 1-Dichloroethane UD 38460 ppb EPA 8240 1':56 08/02/9S ANM
l, 1-Dichloroethene UD 38460 ppb EPA8240 15:56 08/02/95 ANM
I 1,2-Dichloroethanc UD 38460 ppb EPA 8240 ' 15:56 08/02/95 ANM
1,2-Dichloropropane UD 38460 ppb EPA 8240 15:56 08/02195 ANM
I
2-Butanone 120,C00 D 46152 ppb EPA8240 15:56 08/02195 ANM
2-Chlorocthylvinyl ether UD 38460 ppb EPA 8240 15:56 08/02195 A,'IM
2-Hexanone UD 38460 ppb EPA 8240 15:56 08102195 ANM
I 4-Methyl-2-pentanone UD 38460 ppb EPA 8240 15:56 · 08102/95 ANM
Acetone UD 65382 ppb EPA 8240 15:56 08/02/95 ANM
Benzene UD 73074 ppb EPA 8240 15:56 08/02195 ANM
I Bromodichloromethane UD 38460 ppb EPA 8240 15:56 08/02195 ANM
Bromafonn un· 38460 ppb EPA 8240 15:56 08/02/95 ANM .,~;
I
HUb ~~ •~~ 16:.54 TO 3~ill47 FROM AquoChem Envtr. Lab T-38':i P.02
I
Ir}
~~!!,~o~!'~~O"roru" '"° ~~·-
I · 11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation Nonh Carolina Certification Number: JOS
240 I Tuckascegee Road South Carolina Certifica1ioo Number: 99032
Charlene, NC
I Client#: 3080 Received Date: 27-Jul-95
Conlact: Mr. Randy Bennett Report Date: 22-Aug-95 r
I SDG#: SV233080 Approved By: (!lF------Lab ID: AAl3854 ~llITY 0
I Sample ID: BG-61 Project Manaaer
Detection
Parameter &suit Limit Unit Method Time Date AnalySI
1r) Bromoroethane UD 38460 ppb EPA 8240 15:56 08/02/95 ANM ~-" Carbon disulfide UD . 38460 ppb EPA 8240 15:56 08/02/95 ANM
I Carbon teuachloride UD 38460 ppb EPA 8240 15:56 08/02/95 ANM
Chlorobenzene UD 38460 ppb, EPA 8240 15:56 08/02/95 ANM
Chlorodibromoroethane UD 38460 ppb' EPA8240 15:56 08/02/95 ANM
I Chloroethane UD 38460 ppb EPA 8240 15:56 08/02/95 ANM
Chloroform UD 38460 ppb EPA 8240 15:56 08/02/95 ANM
Chloromethane UD 42306 ppb EPA 8240 15:56 08/02/95 ANM I cis-1,2-Dichloroethene UD 38460 ppb EPA 8240 15:56 08/02/95 ANM
cis-1,3-Dichloropropene UD 38460 ppb EPA 8240 15:56 08/02/95 · ANM
I Ethylbenzene UD 38460 ppb EPA 8240 15:56 08/02i9S ANM
Methylene chloride UD 53844 ppb EPA 8240 15:56 08/02/95 ANM
Stryene U.D 38460 ppb EPA 8240 15:56 08/02/95 A.'IM
I Tetrachloroethene 41,000 0 38460 ppb EPA 8240 15:56 08/02/95 ANM
Toluene 76,000D 38460 ppb EPA 8240 15:56 08/02195 ANM
I Total Xylencs 170,000 D 38460 ppb EPA 8240 15:56 08102/95 ANM
trans-1,2-Dichloroethenc UD 38460 ppb EPA 8240 15:56 08102/95 ANM
trans-1,3-Oichloropropenc uo 38460 ppb EPA 8240 15:56 08/02195 A.'IM
I Trichloroethene uo 38460 ppb EPA 8240 15:56 08/02/95 ANM
Vinyl chloride UD 38460 ppb i!PA8240 15:56 08/02/95 ANM ,· ! 1-Y
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/Aqua Chem
ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
1-..:,ilj'j t"', 1:1~
Certificate of Analysis
Client: OHM Corporation
240 l Tuckaseegee Road
Charlotte, NC
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
3080
Mr. Randy Bennett
SV233080
AA13854
BG-61
1,2,4-Tricblorobcnzcnc
1,2--Dichlorobc:nzcne
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4,6: Trichlorophcnol
2,4-Dichlorophenol
2,4-Dimethylphcnol
2,4-Dinitrophenol
2,4-Dinitrotolucnc
2,6-Dinilrotoluenc
2-Cbloronaphtbalcne
2-Chlorophenol
2-Mcthylnaphlhaleue
2-Methylphenol (o-cresol)
2-Nitroaniline
2-Nitrophcnol
3-Nitroaniline
4.6-Dinitro-2-r.iethylphcnol
4,6-Dinitro--0-cresol
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
1000
Unit
ppb
ppb
ppb
ppb,
ppb.
ppb
ppb
ppb
ppb
ppb
ppb
ppb
?Pb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certificatioo Number. 305
South Carolina Certification Number: 99032
Received Date: 27-Jul-95
Report Date: 22-Aug-95
Approved By: -·-/<..£?~~;..~~~=""?:;:::,i,,--
~,; 'J
Method
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA82'70
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA8270
EPA 8270
Project Manager
Time Date
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
17:17
08/02/95
08/02/9S
08/02/9S
08/02/95
08/02/95
08/02/9S
08/02/95
08/02/95
08/02/95
08/02/95
08/02/9S
08/02/95
08/02/95
08/02/95
08/02/9S
08/02/95
08/02/95
08/02/95
08/02/95
08/02/95
Analyst
'ANM
ANM
ANM
-ANM
ANM
AM,,! '
AM,,!
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
AUG 23 '95 16;35 TO 39!1147 FROM Aqt.;aC:'lem Enu ir. Lab T-389 P.04
I
I,"
lA~!!,~,l!?~.~r:i.,,,,.,,,,.,, '"' . • ,, .. :~
11176 Downs Road
I Pineville, NC 28134
704/5118-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99031 •
I
Charlotte, NC
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Dale: . 22-Aug-95
I SDG#: SV233080 Approved By: UdZ2.
0 La.b ID: AA13854 ~
I Sample ID: BG-i;I Project Manager
Det«tion
Parameter Iwult Limit Unit Method Time Date Analyst .-. . · .\ 4-Bromophenyl phenyl ether UD 1000 ppb EPA82i0 17: l7 08/02/95 A.'IM" .. • I
:.J 4-Chloro-3-mcthylphenol UD -1000 ppb EPA 8270 !?:Ji 08/02/95 _ANM
I 4-chloroaniline UD 1000 ppb EPA8270 1'7:17 08/02/95 ANM
4-Chlorophenyl phenyl ether UD 1000 ppb, EPA8270 17:17 08/02/95 ANM
4-Mcthylphcnol (p-crcsol) UD 1000 ppb. . EPA 8270 17: Ii 08/02/95 ANM
I 4-Nitroanilinc UD 1000 ppb EPA 82i0 17:17 08/02/95 ANM '
4-Nitrophcnol UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Accnaphthene UD 1000 ppb EPA8270 17:17 08102/95 Amil
Acenaphthylene UD 1000 ppb EPA8270 17:17 08/02/95 ANM
Bcnzo(a)anthraccne UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Benzo(a)pyrcne UD 1000 ppb EPA 8270 17:17 08/02/95 A.,'1/M
ae·nzO(b)fluoranthene UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
I Benzo(ghi)pcrylcnc UD 1000 ppb EPA8270 17:17 08102/9S ANM
Benzo(k)lluoranthenc UD l000 ppb EPA8270 17:17 08/02/95 ANM
Bis(2-chloroetlloxy) methane UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Bis(2-chloroethyl) ether UD 1000 ppb EPA 8270 17:17 08/02/9S ANM
Bis(2-chloroisopropyl) ether UD l000 ppb EPA8270 17:17 08/02/9S ANM
Bis(2-ethylhcxyl) phthalate UD 1000 ppb EPAS270 17:17 08/02195 ANM I Butyl bcnzyl phthalate UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
Chrysene UD l000 ppb EPA8270 17:17 08/02/95 ANM
1-
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,AUG 23 '95 16:36 TO 3911147
I
FROM Hcp.;aChem Enu \r. Lab T-389 P, 05
I_,
lA~:!~oE~,~~,omoa,., ,.c
,";-. ::~~, .... _-.-::
.,.,''c" 1-
11178 Downs Road
I
Pineville, NC 281 :14
704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 30S
240 I Tuckaseegee Road South Carolina Certification Number: 99032
·1 Charlotte, NC
Client#: 3080 Received Date: 27-Iul-95
Contact: Mr. Randy Bennett Report Date: ~--I SDG#: SV233080 Approved By: 0 Lab ID: AAl3854 ~ ~ .
I Sample ID: BG-61 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
IS"i'-; Di-n-bul)'l phtbalate UD 1000 ppb EPA8270 17:17 08/02/95 ANM ·,-.. :, ,·;,,./ Di'n--0s"tyl phthalate UD 1000 ppb EPA 8270 17:17 08/02195 ANM
I
Dibcnzo(ah)anthraccne UD 1000 ppb E?A8270 17:17 08/02/95 ANM
Dibcnzofuran UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
Diethylphthalate UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
I Dimethylphthalate UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
Fluoranthene UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Fluorene UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
Hexachlorobenzenc UD 1000 ppb EPA8270 17:17 08/02/95 ANM
Hexachlorobutadicne UD 1000 ppb ( EPA8270 17:17 08/02/95 ANM
I Hcxachlorocyclopentadiene UD 1000 ppb EPA8270 17:17 08/02/95 ANM
Hcxachlorocthanc UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
I lndcno(l,2,3-cd)pyrene UD 1000 ppb EPA8270 17:17 08/02/95 A..'<M
lsophorone UD 1000 ppb EPA8270 17:17 08J02/95 ANM
N-Ni!Ioso-di-n-propylaininc UD !000 ppb EPA 8270 17:17 08/02/95 ANM
I N-NiUosodiphenylamine UD 1000 ppb EPA 8270 17:17 08/02/95 ANM
Naphthalene UD 1000 ppb EPA8270 17:17 08/02/95 ANM
Nitrobcnzcnc UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Pentachlorophcnol UD 1000 ' 17:17 08102/95 ANM ppb EPA 8270
Phenanthrenc UD IOOO ppb EPA8270 17:17 08/02/95 ANM
1--
I
HUll .1..5 ·~::i lb:,.H 1U .j':,!,.114'( FROM AquaChem Env,r. L•b T-389 P.06
I
I.cc,
/A~~~,!?.,):,~~ao,.,om~ '"" ~~tr
I 11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckascegee Road South Carolina Certification Number: 99032
Charloue, NC
I Client II: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennett Report Date: 22-Aug-95
I SDG#: SV233080 Approved By: ~~4~27 Lab ID: AAl3854 R'&c ' ' ·,
S•mple ID: BG-61 Project Manager I Detection
Parameter Rc1ult Umit Unit Method Time Date Anal1st
E' Phenol UD 1000 ppb EPA 8270 17:17 08i02/9S ANM .,
/ Pyrcne UD 1000 ppb EPA8270 17:17 08/02/95 ANM
I Barium 15.2 o.s ppm SW 6010 10:55 08103/95 RCD
Cadmium 0.80 0,05 ppm SW 6010 10:45 08/08195 RCD
Chromium 37D 2.5 ppm· SW 6010 10:05 08/14/95 RCD
I Copper 31D 1.0 ppm SW 6010 10:05 08/14195 RCD
Iron 3500 0.5 ppm SW 6010 09:15 08103/95 RCD
Nickel 96D 1.5 ppm SW 6010 14:10 08/14/95 RCD I Silver u 0.05 ppm SW6010 10:45 08/08/95 RCD
Zinc 365D 5 ppm SW 6010, 10:05 08/14195 RCD
I Arsenic 0.160 0.02S ppm SW7060 10:30 08/03/95 RCD
Lead 104D 2.5 ppm SW7421 10:05 08/14/95 RCD
Mercu,y 0.038 0.004 ppm SW 7471 08:30 08/10195 KRR
I Selenium 0.013 0.015 ppm SW7740 14:20 · 08103/95 RCD
Paint Filter Positive SW 846 10:55 08116/95 RCD
I BTU <1000 BTU/gal SW-846 #909 08:00 08102195 JCH
Flash Point 80 70 Dcg.F SW-846 #909 10:15 08/10/95 KRR
Aluminium 63.S 0.S ppm SW846 6010 09:40 08/04/95 RCD
I Antimony 2.4 1.0 ppm SW846 6010 14:40 08/07/95 RCD
Berylliwn u o.o, ppm SW846 6010 14:30 08/02195 RCD r}
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l_j
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A~!!~~~.~~,oAA,o,m, ,c
11176 Downs Road
Plnevllle, NC ~8134
704/SB&-5076
FAX [phone]
FROM AquaC~em E~ui~. Lab T-389 P.07
Certificate of Analysis
Client: OHM Corporation North Carolina Certifkation Number: 305
240 I Tuckaseegee Road South Carolina Certification Number. 99032
Charlotte, NC '
Client#: 3080 Received Date: 27-Jul-95
Contact: Mr. Randy Bennen Report Date: , 22-Aug-95
SDG#: SV233080 Approved By: ~~---' Lab ID: AA13854 Rol5"er!L rry ;;
Sample ID: BG-61 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
Calcium 1600 0.S ppm. SW8466010 09:15 08/03/95 RCD
Cobalt li 0.05 ppm SW8466010 11:30 08/07/95 RCD
Magnesium 24,8 0.05 ppm SW8466010 14:30 08/02/95 RCD
Mangan= 470D 0.5 PPII! SW846 6010 09:15 08/03195 RCD
Potas.sium 482 5,0 ppm• SW846 6010 12:10 08/07195 RCD
Sodium 1140D so ppm SW846 6010 14:::o 08/03/95 RCD ' Thallium u 0.050 ppm SW846 6010 08:40 08107/95 RCD
Vanadium 0,50 0.25 ppm SW846 6010 14:30 08/02/95 RCD
PH 8.39 0-14 SU SW846 9045 09:45 08/10/95 ICRR
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* Note:
Bulk Group 67
Bulk Group Description: Solids
Bulk Groups were uamed aeeording to preliminary hazardous
eategorization test and may not eorrespond to what the material
was classified as for disposal.
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Certificate of Analysis
l ·Y-):·.:_ ... <..:..
I
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Client: OHM Corporation
240 l Tuckaseegee Road
Charlotte, NC
Client#: 30&0
Contact: Mr. Randy Bennett
SDG/1: SV533080
Lab ID: AA 13 964
Sample ID: BG-o7
Parameter
Arsenic
Bariwn
Cadmium
Chromium
Lead
Mercury
Solcniwn
Silver
Result
0.021
5.2
1.90
42D
1650
u
u
u I 1,1-Dichloroethylene 0.027
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I
1,2-Dichlorocthanc
1,4-Dichlorobenzcne
Benzene
Carbon tetrachloride
Chlorobenzcne
Chlorofonn
Methyl ethyl ketone
T etrachloroethylcno
Trichloroctl1yl0Dc
Vinyl chloride
2.~.5-Trichlorophenol
1.308
0.220 E
II.IE
3.00E
u
u
3.6E
0.360 E
0.040
OU
UD
Detection
Limit Unit
o.oos mg/L
0.1 mg,'L
0,05 mg/L
2.5 mg,'L
2.5 mg/L
0.0002 mg/L
0.005 mg/L
0.05 mg/L
0.005 mgiL
0.005 mg/L
0.005 mg/L
o.oos mg/L
0.005 mg/L
0.005 mg/L
0005 mg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
0.005 mg/L
1.00 mg/L
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Re(eived Date: 02-Aug-95
Repon Date: .23-Aug-95
Approved By:
Robert L. Curry
Project Manager
Method Time Date Analyst
1311/6010 11:25 08/16/95 RCD
1311/6010 09:40 0&/16/95 RCD
1311/6010 10:45 08/08/95 RCD.
1311/6010 10:05 08/14/95 RCD
1311/6010 10:05 08/14195 RCD
1311/6010 08:10 08/16/95 RCD
13 ll/6010 12:30 08/16/95 RCD
1311/6010 10:45 08/08/95 RCD
1311/8260 21:SI . 08/15/9j ANM
1311/8260 ' 2Ul 08/15/95 ANM
1311/8260 21:51 08/15195 ANM
1311/8260 21:51 08/15/95 ANM
1311/8260 2UI 08/15/95 ANM
1311/8260 21:51 08/15/95 ANM
1311/8260 21:51 08/15/95 ANM
1311/8260 21:51 08/15/95 ANM
1311/8260 2Ul 08/15/95 ANM
1,311/8260 2Ul 08/15/95 ANM
1311/8260 21:51 08115/95 ANM
1311/8270 14:09 08/14/95 ANM
I
ID;
I:;,·/
rt-<UM Aq_L'~~nem ~_n_u_,r_._L_•_b __ T-_3 __ a_,_P_. _1=' ___ _
Certificate of Analysis
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Client: OHM Corporation North Carolina Certification Number: 305 2401 Tuckaseegee Road South Carolina Certification Number: 99032
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
Charlone, NC
3080
Mr. Randy Bennett
SV533080
AA13964
BG-67
I /] 2,4.6-Trichlorophenol
·-2,4-Dinitrotoluene
I Hexachlorobenzenc
Hexlll:hlorobutadiene
Hexachloroethane
I m-Cresol
Nitroben:£cne
I o-Cresol
p-Cresol
Penlachlorophcnol
I Pyridine
Total Organic Carbon (TOC)
Total Organic Halide (TOX) I Paint Filter
Reactivity
I BTU
Flash Point
PH
I
IC
I
Detection
Result Limit
UD 1.00
UD 1.00
CD 1.00
UD 1.00
UD 1.00
UD 1.00
UD 1.00
UD LOO
UD LOO
UD LOO
VD LOO
640,000
<10 LO
Negative -0·
P!:NDING -0·
10.200 -0-
<80 80
6.14 0-14
Uoit
mg/L
mg/L
mg/I..
mg/L,
mg/L
mg,L
mg/L
mg/L
mg/I..
mg/L
mg/L
ppm
ppm
-0·
-0-
BTU/gal
Deg. F
SU
Received Date:
RtPorl Date:
Approved By:
02-Aug-95
23-Aug-95
Robert L. Curry
Project Manager
Method TlDle Date
1311/8270 14:09 08/14/95
l311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
13 !118270 14:09 08/1♦/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
1311/8270 14:09 08/14/95
EPA415.I 13:00 08/1 i/95
SMS06 13:00 08/17/95
SW846 10:55 08/18/95
SW-846 #7.3 -0-

-
0
-
SW-846 #909 13:00 08/17/95
SW-846 #909 08:30 08/15/95
SW846 9045 . 09:20 08/17/9S
Analyst
ANM
ANM
ANM.
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
JCH
RCD
RCD
-0·
RCD
RCO
RCD
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Bulk Group 66
Bulk Group Description: Organic Solid
* Note: Bulk Groups were named aeeording to preliminary hazardous
categorization test and may not correspond to what the material
was classified as for disposal.
I
I;~•·, ·, ,ll\qudChem ·! I
I ENVIRONMENTAL LABORATORIES, INC,
11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date:
I SDG#: SR633080 Approved By:
Lab ID: AA11903 R
I Sample ID:· BG-66
Detection
Parameter Result Limit Unit Method Time Date Analyst r~ i'J ) Arsenic 0.078 D 0.010 mg/L. 1311/6010 13:45 05/30/95 KRR ~·
Barium 4.6 0.1 mg/L 1311/6010 14:50 06/01/95 RCD
I Cadmium u 0.01 mg/L 1311/6010 17:53 06/01/95. RCD
Chromium u 0.05 mg/L 1311/6010 17:53 06/01/95 RCD
I Lead 0.14 0.05 mg/L· 1311/6010 17:53 06/01/95 RCD
Selenium u 0.005 mg/L 1311/6010 15:00 05/30/95 KRR
Silver 0.02 0,01 mg/L 1311/6010 17:53 06/01/95 RCD
I Chlorodane u 0.010 mg/L 131118080A 13:27 06/08/95 RAG
Endrin u 0.010 mg/L 131118080A 13:27 06/08/95 RAG
I Heptachlor l/ 0.010 mg/L 1311/8080A 13:27 06/08/95 RAG
Heptachlor epoxide u 0.010 mg/L 131118080A 13:27 06/08/95 RAG
Lindane u 0.010 mg/L 1311/8080A 13:27 06/08/95 RAG
I Methox-ychlor u 0,010 mg/L 131118080A 13:27 06/08/95 RAG
Toxaphene u 0.010 mg/L 131118080A 13:27 06/08/95 RAG
I 2,4,5-TP (Silvex) u 0.010 mg/L 1311/8150 13:46 06/06/95 RAG
2,4-D u 0.010 mg/L 1311/8150 13:46 06/06/95 RAG
I, 1-Dichloroethylene u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
I 1,2-Dichloroethane u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
.:.·) ) 1,4-Dichlorobcnzene u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC 1~ · Benzene 0,086 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
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le-: ~ .. ;_.;•
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) lA~!!~o'!?.~,~~•o"''°'"' '"c
11176 Downs Road
Pineville, NC 28134
704/588-5076
· FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-J"
SDG#: SR633080 Approved By: ~ Lab ID: AAll903 RQbe'~urry~
Sample ID:· BG-66 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
} Carbon tetrachloride u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
Chlorobenzene u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
Chloroform u 0.005 mg/L 13 I 1/8260 19:47 06/01/95 · DLC
Methyl ethyl ketone 0.025 0.005 \ mg/L 1311/8260 19:47 06/01/95 DLC
Tetrachloroethylene 0.007 0.005 mg/L 1311/8260 19:47 06/01/95 DLC '· Trichloroethylene 3.09 D 0.25 mg/L 13 I 1/8260 19:47 06/01/95 DLC
Vinyl chloride u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
2, 4,5-Trichlorophenol UD 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
2,4,6-Trichlorophenol UD 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
2,4-Dinitrotoluene UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Hexachlorobenzene UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Hexachlorobutadiene . UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Hexachloroethane UD 0.IO mg/L 13 I 1/8270 13:02 06/02/95 ANM
m-Cresol 0.120 D 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
Nitrobenzene UD 0.IO mg/L 13 I 1/8270 13:02 06/02/95 ANM
o-Cresol 0.100 D 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
p-Cresol 0.120 D 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Pentachlorophcnol UD 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
Pyridine UD 0.IO mg/L 1311/8270 13:02 06/02/95 ANM
Total Organic Carbon (TOC) 320,000 ppm EPA 415.1 17:00 05/30/95 JCH
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1 lA~!!~o9~,~~ao,uo,.,, '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076
. FAX [phone]
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr_ Randy Bennett
SDG#: SR633080
Lab ID: AAI 1903
Sample ID:-BG-66
Parameter Result
Total Organic Halide (TOX) 8.6
Paint Filter Positive
Co_rrosivity 7.19
BTU 6750
Flash Point 64
Reactive Cynide u
Reactive Sulfide u
PH 7.19
Detection
Limit Unit
LO ppm
0-14 s.u.
BTU/gal
60 Deg.F
ppm
0.1 ppm
0-14 SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receh·ed Date: 24-May-95
Report Date: 12-Jun-95
Appro,•ed By: ~~
Project Manager
Method Time Date Anal);st
SM506 17:00 05/30/95 JCH
SW846 10:00 05/28/95 TML
SW-846 #111 08:20 05/30/95 · RCD
SW-846 #909 17:00 05/30/95 JCH
SW-846 #909 10:15 05/31/95 TML
'· SW846 9010 11:00 05/31/95 TML
SW846 9030 I 1:00 05/31/95 TML
SW846 9045 08:20 05/30/95 RCD
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101 :· -.. -
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lA~!!~o~,~.~~•oamm,,.,
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Receh·ed Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-J~
SDG#: SR633080 Approved By: ~-Lab ID: AAll903 R~luny~
Sample ID: BG-66 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
Carbon tetrachloride u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
Chlorobenzene u • 0.005 mg/L 13 I 1/8260 19:47 06/01/95 DLC
Chloroform u 0.005 mg/L 13 I 1/8260 19:47 06/01/95 ·.DLC
Methyl ethyl ketone 0.025 0.005 mg/L 13 I 1/8260 19:47 06/01/95 DLC
Tetrachloroethylene 0.007 0.005 mg/L 13 I 1/8260 19:47 06/01/95 DLC
' Trichloroethylene 3.09 D 0.25 mg/L 13 I 1/8260 19:47 06/01/95 DLC
Vinyl chloride u 0.005 mg/L 1311/8260 19:47 06/01/95 DLC
2,4,5-Trichlorophenol UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
2,4,6-Trichlorophenol UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
' 2,4:Dinitrotoluene UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Hexachlorobenzene UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Hexachlorobutadiene UD 0.10 mg/L 13 I 1/8270 13:02 06/02/95 ANM
Hexachloroethane UD 0.10 mg/L . 1311/8270 13:02 06/02/95 ANM
m-Cresol 0.120 D 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Nitrobenzene UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
o-Cresol 0.100 D 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
p-Cresol 0.120 D 0. 10 mg/L 1311/8270 13:02 06/02/95 ANM
Pentachlorophenol UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Pyridine UD 0.10 mg/L 1311/8270 13:02 06/02/95 ANM
Total Organic Carbon (TOC) 320,000 ppm EPA 415.1 17:00 05/30/95 JCH
I
I. })A Ch ,_-a,,! z....:' qua em
I ENVIRONMENTAL LABORATORIES, INC.
· · 11176 Downs Road
Pineville, NC 28134
704/588-5076 I FAX [phone]
I Certificate of Analysis
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Client: OHM Corporation
2401 Tuckaseegee Road
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA! 1903
Sample ID: BG-66
Parameter
Total Organic Halide (TOX)
Paint Filter
Corrosivity
BTU
Flash Point
Reactive C)nide
Reactive Sulfide
PH
Result
8.6
Positive
7.19
6750
64
u
u
7.19
Detection
Limit
1.0
0-14
60
0.1 ·
0-14
Unit
ppm
s.u.
BTU/gal
Deg.F
ppm
ppm
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: 12-Jun-95
Approved By: ~ R~rry z>
Project Manager
Method Time Date Analyst
SM506 17:00 05/30/95 JCH
SW846 10:00 05/28/95 TML
SW-846 #111 08:20 05/30/95 -RCD
SW-846 #909 17:00 05/30/95 JCH
SW-846 #909 IO: 15 05/31/95. TML
SW846 9010 11:00 05/31/95 ' TML
SW846 9030 11:00 05/31/95 TML
SW846 9045 08:20 05/30/95 RCD
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Bulk Gromp 70
Bulk Gn-01111.p Description: Water Solublle Neu.ttn-aH:
• Note: Rnllk. Groups were named aeeoralling to preliminary hazaJl"doos
eategorization test and may not eorrespond to what t.he materiiml
was elassil!ied as for disposal.
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/A~~~o5~,~'.:!',o .. ro,.,,. '"c
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 12-Jun-95
SDG#: SR633080 Approved By: #(~·c Lab ID: AAll904
Sample ID: BG-70 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst;
Percent Water 85.70 % 17:00 05/30/95 JCH
Total Organic Carbon (TOC) 86,000 ppm EPA415.l 17:00 05/30/95 JCH
1, I, 1,2-Tetrachloroethane u 500 ppb EPA 8240 ·10:07 06/01/95 DLC
1, I, 1-Trichloroethane u 500 ppb EPA 8240 10:07 06/01/95 DLC
1, 1,2,2-Tetrachloroethane u 1000 ppb EPA 8240 · 10:07 06/01/95 DLC
I, 1,2-Trichloroethane u 500 ppb EPA 8240 10:07 06/01/95 DLC
I, 1-Dichloroethane u 500 ppb EPA 8240 · 10:07 06/01/95 DLC
I, 1-Dichloroethene u 1000 ppb . EPA 8240 10:07 06/01/95 DLC
1,2-Dichloroethane u 500 ppb EPA 8240 10:07 06/01/95 DLC
1,2-Dichloropropane u 500 ppb EPA 8240 10:07 06/01/95 DLC
2-Butanone u 1200 ppb EPA 8240 10:07 06/01/95 DLC
2-Chloroethylvinyl ether u 1000 ppb EPA 8240 10:07 06/01/95 DLC
2-Hexanone u 500 ppb EPA 8240 10:07 06/01/95 DLC
4-Methyl-2-Pentanone 1910D 1000 ppb EPA 8240 10:07 06/01/95 DLC
Acetone u 1600 ppb EPA 8240 10:07 06/01/95 DLC
Benzene u 500 ppb EPA 8240 10:07 06/01/95 DLC
Bromodichloromethane u 500 ppb EPA 8240 10:07 06/01/95 DLC
Bromoform u 500 ppb EPA 8240 10:07 06/01/95 DLC
Bromomethane u 1000 ppb EPA 8240 10:07 06/01/95 DLC
Carbon disulfide 2230 D 1000 ppb EPA 8240 10:07 06/01/95 DLC
/
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' lA~~~o':9,~,~~,oSAros,es, '"'
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Dat_e: 12-JM
SDG#: SR633080 Approved By: L~«-Lab ID: AA! 1994 Rob&! _. urry 0
Sample ID: · BG-70 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst
•. I Carbon tetrachloride u 500 · ppb EPA 8240 10:07 06/01/95 DLC
Chlorobenzene u 500 ppb EPA 8240 10:07 06/01/95 DLC
Chlorodibromomethane u 1000 ppb EPA 8240 10:07 06/01/95 DLC
Chloroethane u 1000 'ppb EPA 8240 10:07 06/01/95 DLC
Chloroform u 500 ppb EPA 8240 10:07 06/01/95 DLC
Chloromethane u 2000 ppb EPA 8240 10:07 06/01/95 DLC
cis-1,2-Dichloroethene u 500 ppb EPA 8240 10:07 06/01/95 DLC
cis-1,3-Dichloropropene u 500 ppb EPA 8240 10:07 06/01/95 DLC
Ethylbenzene 1650 D 500 ppb EP18240 10:07 06/01/95 DLC
Methylene chloride u 1400 ppb EPA 8240 10:07 06/01/95 DLC
Stryene 1560 D 1000 ppb EPA 8240 10:07 06/01/95 DLC
Tetrachloroethene u 500 ppb EPA 8240 10:07 06/Pl/95 DLC
Toluene 2330 D 500 ppb EPA 8240 10:07 06/01/95 DLC
Total Xylenes 5940 D 500 ppb EPA 8240 10:07 06/01/95 DLC
trans-1,2-Dichloroethene u 500 ppb EPA 8240 10:07 06/01/95 DLC
trans-I, 3-Dichloropropene u 500 ppb EPA 8240 10:07 06/01/95 DLC
Trichloroethene u 500 ppb EPA 8240 10:07 06/01/95 DLC
Vinyl chloride u 1000 ppb EPA 8240 10:07 06/01195 DLC
) 1,2,4-Trichlorobenzene UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
1,2-Dichlorobenzene UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
I
I,. ) lA~~"~E~.'z~,o,m,.,,. '"' •.".·,":' -~ <;:::.·
I 11176 Oown.s Road
Pineville, NC 28134
I 704/588-5076
· FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
2-lOI Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Receh·ed Date: 24-May-95
Contact: Mr. Randy Bennett Report D~te: 12-Jun-95
I SDG#: SR633080 ApproYed By: ~ Lab ID: AAll904 Ro'fu~rryrp
I Sample ID: BG-70 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analpt 1~ ' UD 19:16 05/31/95 ~->-) 1,3-Dichlorobenzene 1000 ppb EPA 8270 ANM
1,4-Dichlorobenzene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I 2,4,5-Trichlorophenol UD 1000 ppb EPA 8270 19:16 05/31/95 . ANM
2,4,6-Trichlorophenol UD 1000 ' ppb EPA 8270 19:16 05/31/95 ANM
I 2,4-Dichlorophenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
'· 2,4;Dimethylphenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
2,4-Dinitrophenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I 2,4-Dinitrotoluene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
2,6-Dinitrotoluene UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
I 2-Chloronaphthalene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
2-Chlorophenol UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
2-Methylnaphµialene UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
I 2-Methylphenol (o-cresol) UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
2-Nitroaniline UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I 2-Nitrophenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
3,3-Dichlorobenzidine UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
3-Nitroaniline UD 1000 ppb EPA 8270 19:16 05/31195 ANM I 4,6-Dinitro-2-methylphenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
} ) 4,6-Dinitro-o-cresol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM IJ · 4-Bromophenyl phenyl ether UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
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11§ lA~~~o~,~.~~aoaAro"~•.c
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
I
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I
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
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Client#:
Contact:
SDG#:
Lab ID:
3080
Mr. Randy Bennett
SR633080
AAll904
Sample ID: BG-70
Parameter
j 4-Chloro-3-methylphenol
4-Chloroaniline
4-Chiorophenyl phenyl ether
4-Methylphenol (p--cresol)
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphtli.ylene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b )fluoranthene
Benzo(ghi)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
Bis(2--chloroethoxy) methane
Bis(2--chloroethyl) ether I Bis(2--chloroisopropyl) ether
l
\c:,:./ ) Bis(2-ethylhexyl) phthalate
. Butyl bcnzyl phthalate
I
Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit
1000
1000
1000
1000
1000
1000
1000
1000
1000
1900
3000
2000
1000
1000
1000
1000
1000
1000
1900
1500
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date:
Report Oat~:
24-May-95
12-Ju~
Approved By: ~~~""7r"
-R-o?-.""~e~"'-"'_ "'u"rry,__.===~t,'
Method
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270,
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
Project Manager
Time
19:16
19:16
19:16
19:16
19:16
19: 16
19:16
19: 16
19: 16
19: 16
19:16
19:16
19:16
19:16
19:16
19:16
19:16
19:16
19:16
19:16
Date
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
05/31/95
Analys)
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM
ANM.
ANM
ANM
I
•·~ ... _ ·: ,,;{/
I
1 1A~~~o5~.:~,o,no,,,,. "'
11176 Downs Road
Pineville, NC 28134
7041588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 l Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date'. 12-Jun-95
I SDG#: SR633080 Approved By: ~---Lab ID: AAl 1904 ~~/
I Sample ID: BG-70 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst, .~-\ . lJ , Chrysene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Di-n-butyl phthalate UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I Di-n-octyl phthalate UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Dibenzo(a,h)anthracene UD 1000 ppb EPA 8270 19:16 05131195 ANM
I D ibenzofuran UD 1000 ppb EPA 8270 19:16 05/31/95 ANM .
Diethylphthalate UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Dimethylphthalate UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I Fluoranthene UD 1000 ppb EPA 8270 19:16 05131/95 ANM
Fluorene UD 1000 ppb EPA,8270 19:16 05/31/95 ANM
I Hexachlorobenzene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Hexachlorobutadiene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Hexachlorocyclopentadiene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I Hexachloroethane UD 1000 ppb EPA 8270 19: 16 05/31/95 ANM
Indeno( 1,2,3-cd)p)Tene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I Isophorone UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
N-nitroso-<li-n-propylamine UD 1000 . ppb EPA 8270 19: 16 05/31/95 ANM
N-nitrosodiphenylamine UD 1000 ppb EPA 8270 19:16 05/31/95 ANM I Naphthalene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
(>,) Nitrobenzene UD 1000 ppb EPA8270 19:16 05/31/95 ANM
' ,::. .. ::/. Pentachlorophcnol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
"
I
I
-~'"· #\.qua Chem ! :;:.~~ ... ,)! .;: :, ..
I ENVIRONMENTAL LABORATORIES, INC.
11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis'
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
I Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date:
I SDG#: SR633080 Approved By:
Lab ID: AA11904 /,.
I Sample ID: BG-70 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst a-3., Phenanthrene UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
Phenol UD 1000 ppb EPA 8270 19:16 05/31/95 ANM
I Pyrene UD 1300 ppb EPA 8270 19:16 05/31/95 ·ANM
Barium 187 E 0.5 ppm SW 6010 14:50 06/01/95 RCD
I Cadmium 0.65 0.05 ppm SW 6010 18:10 05/31/95 KRR
' Chromium 22.1 0.25 ppm SW 6010 18:10 05/31/95 KRR
Copper 117 D 1.0 ppm SW 6010 18:10 05/31/95 KRR
I Iron 1560D 15 ppm SW 6010 16:07 05/31/95 KRR
Lead 12.9 0.25 ppm SW 6010 18:31 06/01/95 RCD
I Nickel 27D 15 ppm SW 6010 18:10 05/31/95 KRR
Silver u 0.05 ppm SW 6010 18:10 05/31/95 KRR
Zinc 91.9 D 0.51 ppm SW 6010 18:10 05/31/95 KRR
I Arsenic 2.10 D 0.025 ppm SW 7060 08:30 06/01/95 KRR
Mercury UD 0.002 ppm SW 7470 10:30 06/02/95 TML
I Selenium 0.100 0.025 ppm SW7740 09:20 06/01/95 KRR
Paint Filter Positive SW846 10:00 05/28/95 TML
I BTU llOO BTU/gal SW-846 #909 17:00 05/30/95 JCH
Flash Point >220 70 Deg.F SW-846 #909 IO: I 5 05/31/95 TML
1 .._: ~\ Aluminium 807 D 50 ppm SW846 6010 08:19 06/01/95 KRR
1'-----" Antimony u 0.05 ppm SW846 6010 11: IO 05/31/95 KRR
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A~~~!?,~,~~•oa.rnmes "c.
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone]
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Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#:
Contact:
SDG#:
Lab ID:
3080
Mr. Randy Bennett
SR633080
AA! 1904
Sample ID: BG-70
Parameter-I 1)) Beryllium
Calcium
I Cobalt
Maganese
I Magnesium
Potassium
Sodium
I Thallium
Vanadium
I •ReactiYe Cynide
Reactiye Sulfide
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pH
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I ... Iv)
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Result
u
871 D
Detection
Limit
0.25
25
U 0.25
115 D 25
156 D 25
1120 D 5.0 ·
12000DE 50
U 0.05
1.46 0.25
Negative
Negative
12.98 0-14
Unit
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
SU
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date:
Project Manager
Method Time Date Analyst
SW846 6010 16:07 05/31/95 KRR
SW846 6010 16:07 05/31/95 . KRR
SW846 6010 11:15 05/31/95 RCD
SW846 60IO 16:07 05/31/95 KRR
SW846 6010 16:07 05/31/95 KRR • SW846 6010 07:37 06/01/95 KRR
SW846 60IO 09:50 06/01/95 KRR
SW846 60IO 08:20 05/31/95 KRR
SW84(> 6010 16:07 05/31/95 KRR
SW846 90IO 11:00 05/31/95 TML
SW846 9030 I 1:00 05/31/95 TML
SW846 9040 08:20 05/30/95 RCD
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Bulk Group 71
Bulk Group Description: Aquatic Rase/
Neutral Solid
* Note: Bolk Groups were named aeeor:ding fu preliminary hazardous
eategorization test and may not eorrespond to what the material
was elassified· as for disposal;
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I~ .. ) /A~!!~o~~~~aoamm" '" •!" •:{/
11176 Downs Road
Pineville, NC 28134
I 704/588-5076
FAX [phone]
I Certificate of Analysis
I Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
I
Charlotte, NC
Client#: 3080 Received Date: 24-May-95
Contact: Mr. Randy Bennett Report Date: 5
I SDG#: SR633080 Approved By:
Lab ID: AAll905
I Sample ID: BG-71 Project Manager
Detection
Parameter Result Limit Unit Method Time Date Analyst ,~ . ':_:;~ ) Arsenic 0.014 0.005 mg/L 1311/6010 13:45 05/30/95 KRR '•::J
Barium 0.5 0.1 mg/L 1311/6010 14:50 06/01/95 RCD I Cadmium 0.02 0.01 mg/L 13II/6010 17:58 06/01/95 RCD .
Chromium 0.31 0.05 mg/L 1311/6010 17:58 06/01/95 RCD
I Lead u 0.05 mg/L 1311/6010 17:58 06/01/95 RCD
Mercury u 0.0002 mg/L 1311/6010 10:30 06/02/95 TML
Selenium u 0.005 mg/L 13il/6010 15:00 05/30/95 KRR I Silver u 0.01 mg/L 1311/6010 17:58 06/01/95 RCD
Chlorodane u 0.010 mg/L 1311/8080A 14:08 06/08/95 RAG
I Endrin u 0.010 mg/L 131 l/8080A 14:08 06/08/95 RAG
Heptachlor u 0.010 mg/L 1311/8080A 14:08 06/08/95 RAG
Heptachlor epoxide u 0.010 mg/L 1311/8080A 14:08 , 06/08/95 RAG, I Lindane u 0.010 mg/L 1311/8080A 14:08 06/08/95 RAG
Methoxychlor u 0.010 mg/L 1311/8080A 14:08 06/08/95 RAG
I Toxaphene u 0.010 mg/L 13 l l/8080A 14:08 06/08/95 RAG
2,4,5-TP (Silvex) u 0.010 mg/L 1311/8150 13:25 06/06/95 RAG
I 2,4-D u 0.010 mg/L 1311/8150 13:25 06/06/95 RAG
I, 1-Dichloroethylene UD 0.500 mg/L 1311/8260 12:35 06/06/95 DLC
I , •1 ) 1,2-Dichloroethane UD 0.500 mg/L 13 II/8260 12:35 06/06/95 DLC .~; · 1,4-Dichlorobenzene UD 0,500 mg/L 1311/8260 12:35 06/06/95 DLC
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lA~!~:o~.?,~,~~,os,rnm ,.c
11176 Downs Road
Pineville, NC 28134
704/588-5076
FAX [phone] I
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I
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I
Certificate of Analysis
Client: OHM Corporation
240 I Tuckaseegee Road
Charlotte, NC
Client#:
Contact:
SDG#:
Lab ID:
Sample ID:
Parameter
3080
Mr. Randy Bennett
SR633080
AA! 1905
BG-71
1.-.
{:) _) Benzene
Carbon tetrachloride
I Chlorobenzene
Chloroform
I Methyl ethyl ketone
Tetrachloroethylene
Trichloroethylene
I Vinyl chloride
2,4,5-Trichlorophenol
I 2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Hexachlorobenzene
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Hexachlorobutadiene
Hexachloroethane
I m-Cresol
Nitrobenzene
o-Cresol
I p-Cresol
I.,:.·.··. , Pentachlorophenol · _ _. .. JI
~--Pyridine
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Result
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
UD
Detection
Limit Unit
0.500 mg/L
0,500 mg/L
0.500 mg/L
0.500 mg/L
0.500 mg/L
0,500 mg/L
0.500 . mg/L
0.500 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0,10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
0.10 mg/L
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Received Date: 24-May-95
Report Date: ,
Method Time Date Analyst .
1311/8260 12:35 06/06/95 DLC
1311/8260 12:35 06/06/95 ·. DLC
13 I 1/8260 12:35 06/06/95 DLC
1311/8260 12:35 06/06/95 DLC
13 I 1/8260 12:35 06/06/95 DLC
1311/8260 12:35 06/06/95 DLC
13 I 1/8260 12:35 06/06/95 DLC
1311/8260 12:35 06/06/95 DLC
1311/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
1311/8270 · 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
13 I 1/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
13 I 1/8270 14:26 06/02/95 ANM
1311/8270 14:26 06/02/95 ANM
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zA~~~oi!?,~.~~.o, .. o,,,,,,"
11176 Downs Road
Pineville, NC. 28134
704/588-5076
FAX [phone]
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 3080
Contact: Mr. Randy Bennett
SDG #: SR633080
Lab ID: AA 11905
Sample ID: BG-71
Parameter Result
Detection
Limit
·✓
Unit
Receiyed Date: 24-May-95 ......... , ~
Approved By:, . . ~
. 'b .Curry
Project Manager
Method ' Time Date ID ) Total Organic Carbon (TOC)
Total Organic Halide (TOX)
20,800
u LO
ppm EPA 415.1
ppm SM506
Analyst
17:00 05/30/95 JCH ·
17:00 05/30/95 JCH
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Paint Filter
Corrosivity
Flash Point
Reactive Cynide
Reactive Sulfide
PH
Negative
7.39 0-14
>220 70
Negative
Negative
7.39 0-14
SW846 10:00 05/28/95 ·. TML
S.u. SW-846 #I 11 08:20 05/30/95 RCD
Deg. F SW-846 #909 10:15 05/31/95 TML
' ppm SW846 9010 11:00 05/31/95 TML
ppm SW846 9030 11:00 05/31/95 TML
SU SW846 9045 08:20 05/30/95 RCD