NCD980557656_20060630_NC State University (Lot 86 Farm Unit 1)_FRCBERCLA SAP QAPP_Analytical Sampling Data 1983 - 2006-OCR

NC STATE UNIVERSITY
[) ~ @ I• 11 \VI ~ ~ ENVIRONMENTAL HEAL THAND SAFETY CENTER
NOTE n JUL O 5 2006
To: David Mattison
S>~ From: Duane Knudson S_LIPERFUND SECTION Date: .June 30, 2006
Sub_jcct: CLot 86 Ricliland Creek Water and Sediment Sampling /
David
I managed to find the lab data reports and sampling location map for the samples
collected from the unnamed tributary to Richland Creek. Samples were collected in April
2001.
As is shown, we did not find volatile organics at above detection levels.
-.
If you need anything else, or if you have any questions on this, please let me know .
Duane Knudson
Environmental Affairs Manager
NC State University
Box 8007
Raleigh, NC 27695
919-515-6859
919-515-6307-FAX
duane _ [e-mail]
. '• I
Lab Report
5/15/01
Compuchem
Bill Scott
501 Madison Ave
Cary, NC 27513
•
,M CA.A-t--1 -.,. -uJ c,oh. r--
•
Fun Service Analytical & Environmental Solutions
Page 1 of 12
Customer Project ID: NCSU
Customer Sample ID: BACKGROUND
Prism Samole ID: AC05988
Loi:iin Group: 935984
Sample Collection Date/Time: 4/27/01
Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
DICHLORODIFLUOROMETHANE
CHLOROMETHANE
VINYL CHLORIDE
BROMOMETHANE
CHLOROETHANE
TRICHLOROFLUOROMETHANE
1, 1-DICHLOROETHENE
METHYLENE CHLORIDE
trans-1,2-DICHLOROETHENE
1, 1-DICHLOROETHANE
2,2-DICHLOROPROPANE
cis-1 ,2-DICHLOROETHENE
CHLOROFORM
BROMOCHLOROMETHANE
1, 1, 1-TRICHLOROETHANE
1, 1-DICHLOROPROPENE
CARBON TETRACHLORIDE
BENZENE
1 ,2-DICHLOROETHANE
TRICHLOROETHENE
1 ,2-DICHLOROPROPANE
BROMODICHLOROMETHANE
DIBROMOMETHANE
TOLUENE
1, 1,2-TRICHLOROETHANE
TETRACHLOROETHENE
1 ,3-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
1,2-DIBROMOETHANE (EDS)
CHLOROBENZENE
TEST
RESULT UNITS
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected . ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
· Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
REPORTING METHOD
LIMIT REFERENCE
0.5
0.5
0.5
0.5
0.5
0.5
0.5
2.0
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0,5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
62300
DATE/TIME
STARTED ANALYST
5111101 05:03 CMS
5111101 05:03 CMB
5111101 05:03 CMS
5111101 05:03 CMB
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 . CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMB
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMS
5111101 05:03 CMB
NC Certification No. 402 -SC Certification Nu, 99012 -NC Drinkin~ Water Cert. No, 37735 FL Certification No. EB7519
449 Springbrook Road..,. P.O. Box 240543 ..,. Charlotte, NC 28224-0543
Phone: [phone] ... Toll Free Numher: 1-R00/529-6364 ... Fn: 704/:i:i2~-04'l9
Lab Report • •
Full Service Analytical & Environmental Solutions
5/15/01 Page 2 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: BACKGROUND
501 Madison Ave Prism Samole ID: AC05988
Cary, NC 27513 LoQin Group: 935984
Sample Collection Datefrime: 4/27/01
/1A cJ.." i Y-.-uJ,,,._ .µ_;-Lab Submittal Datefrime: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATErrlME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ETHYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
1, 1, 1,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
TOTAL XYLENES Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
STYRENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
ISOPROPYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
SROMOFORM Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
1, 1,2,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
1,2,3-TRICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
n-PROPYLBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
BROMOBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
1,3,5-TRIMETHYLBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
2-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
4-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
tert-BUTYLBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
1,2,4-TRI METHYLBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
sec-BUTYLBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
p-lSOPROPYL TOLUENE Not detected ug/L 0.5• 6230D 5/11/01 05:03 CMB
1,3-DICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
1,4-DICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
n-BUTYLBENZENE Not detected · ug/L 0.5 6230D 5/11/01 05:03 CMS
1,2-DICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
1,2-DIBROMO-3-CHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
1,2,4-TRICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
HEXACHLOROBUTADIENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
NAPHTHALENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
1,2,3-TRICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
MTBE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMB
IPE Not detected ug/L 0.5 6230D 5/11/01 05:03 CMS
NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road...,, P.O. Box 240543 ...,, Charlotte, NC 28224-0543
Phone: [phone]...,,. Toll Free Number: 1-800/529-6364 .._ Fax: [phone]
Lab Report
5/15/01
Compuchem
Bill Scott
501 Madison Ave
Cary, NC 27513
•
'
•
Full Service Analytical & Environmental Solutions
Page 3 of 12
Customer Project ID: NCSU
Customer Sample ID: BACKGROUND
Prism Sample ID: AC05988
Loc:iin Group: 9359G4
Sample Collection DatefTime: 4/27/01
Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Sample Comments:
TEST
RESULT
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD
UNITS LIMIT REFERENCE
DATE/TIME
STARTED ANALYST
NC Certification No. 402 • SC Certification No. 99012 • NC DrinkinQ Water Cert. No. 37735 • FL Certification No. E87519
449 Springbrook Road .._ P.O. Box 240543 .._ Charlotte, NC 28224-0543
Phone: [phone] ... Toll Free Number: 1-800/529-6364 .._ Fax: [phone]
Lab Report • •
Full Service Analytical & Environmental Solutions
5/15/01 Page 4 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: MIDDLE
501 Madison Ave Prism Samole ID: AC05989
Cary, NC 27513 Looin Group: 9359G4
Sample Collection Date/Time: 4/27/01
MJ ~'-,. -JJ J-.1. r Lab Submittal Date/Time: 5/1 /01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOO DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
DICHLORODIFLUOROMETHANE Not detected ug/L 0.5 62300 5/11/01 06:01 CMS
CHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
VINYL CHLORIDE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
BROMOMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
CHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
TRICHLOROFLUOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1, 1-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
METHYLENE CHLORIDE Not detected ug/L 2.0 6230D 5/11/01 06:01 CMS
trans-1,2-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1, 1-DICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
2,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
cis-1,2-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
CHLOROFORM Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
BROMOCHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1, 1, 1-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1, 1-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
CARBON TETRACHLORIDE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
BENZENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1,2-DICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
TRICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMB
BROMODICHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
DIBROMOMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
TOLUENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1, 1,2-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
TETRACHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1,3-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
DIBROMOCHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
1,2-DIBROMOETHANE (EDS) Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
CHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 06:01 CMS
NC Certification No. 402 •· SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road...._ P.O. Box 240543 .... Charlotte, NC 28224-0543
Phone: [phone]...,. Toll Free Number: 1-800/529-6364 .... Fax: [phone]
Lab Report • •
Full Service Analytical & Environmental Solutions
5/15/01
Compuchem
Bill Scott
501 Madison Ave
Cary, NC 27513
rM a.~"' ,...,. ~ w vJ-u
Page 5 of 12
Customer Project ID: NCSU
Customer Sample ID: MIDDLE
Prism Samole ID: AC05989
LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
Lab Submittal Date/Time: 5/1 /01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
ETHYLBENZENE
1, 1, 1,2-TETRACHLOROETHANE
TOTAL XYLENES
STYRENE
ISOPROPYLBENZENE
BRO MO FORM
1, 1,2,2-TETRACHLOROETHANE.
1.2,3-TRICHLOROPROPANE
n-PROPYLBENZENE
BROMOBENZENE
1,3,5-TRIMETHYLBENZENE
2-CHLOROTOLUENE
4-CHLOROTOLUENE
tert-BUTYLBENZENE
1,2,4-TRIMETHYLBENZENE
sec-BUTYLBENZENE
p-lSOPROPYL TOLUENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
n-BUTYLBENZENE
1,2-DICHLOROBENZENE
1,2-DIBROMO-3-CHLOROPROPANE
1,2,4-TRICHLOROBENZENE
HEXACHLOROBUTADIENE
NAPHTHALENE
1,2,3-TRICHLOROBENZENE
CIS-1,3-DICHLOROPROPENE
TRANS-1,3-DICHLOROPROPENE
MTBE
IPE
TEST
RESULT UNITS
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
Not detected ug/L
REPORTING METHOD
LIMIT REFERENCE
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
o:5
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
6230D
DATErrJME
STARTED
5/11/01 06:01
5/11 /01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
5/11/01 06:01
ANALYST
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMS
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMB
CMS
CMB
CMB
CMB
CMB
CMB
CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road...,_ P.O. Box 240543 ...,_ Charlotte, NC 28224-0543
Phnne: 704/52()-6::\64 ..._ Toll FrPe N11mher: 1-ROO/~?.Q-i.ll.4 ... F::1Y: 70.d/.c;?5-040Q
Lab Report • •
Full Service Analytical & Environments! Solutions
5/15/01 Page 6 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: MIDDLE
501 Madison Ave Prism Sample ID: AC05989
Cary, NC 27513 LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Sample Comments:
TEST
RESULT
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD
UNITS LIMIT REFERENCE
DATEfTIME
STARTED ANALYST
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water.Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road .._ P.O. Box 240543 .._ Charlotte, NC 28224-0543
Phone: [phone] .._ Toll Free Number: 1-800/529-6364 .._ Fax: [phone]
Lab Report • •
Full Service Analytical & Environmental Solutfons
5/15/01 Page 7 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: CONFLUENCE
501 Madison Ave Prism Sample ID: AC05990
Cary, NC 27513 LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
.M Q,,. \t,. 1 '1-~ \..NJ_ -Vt Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
DICHLORODIFLUOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
CHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
VINYL CHLORIDE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
BROMOMETHANE Not detected ugll 0.5 6230D 5/11/01 06:58 CMB
CHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
TRICHLOROFLUOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1, 1-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11 /01 06:58 CMB
METHYLENE CHLORIDE Not detected ug/L 2.0 6230D 5/11/01 06:58 CMB
trans-1,2-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1, 1-DICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
2,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
cis-1,2-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
CHLOROFORM Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
BROMOCHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1, 1, 1-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1, 1-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
CARBON TETRACHLORIDE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
BENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1,2-DICHLOROETHANE Not detected ugll 0.5 6230D 5/11/01 06:58 CMB
TRICHLOROETHENE Not dete.cted ug/L 0.5 6230D 5/11/01 06:58 CMB
1,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
BROMODICHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
DIBROMOMETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
TOLUENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
1, 1,2-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
TETRACHLOROETHENE Not detected ugll 0.5 6230D 5/11/01 06:58 CMB
1,3-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
DIBROMOCHLOROMETHANE Not detected ugll 0.5 6230D 5/11/01 06:58 CMB
1,2-DIBROMOETHANE (EDB) Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
CHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC Drinking Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road ... P.O. Box 240543 ... Charlotte, NC 28224-0543
Phone: [phone] .,o,. Toll Free Number: 1-800/529-6364 .,o,. Fax: [phone]
Lab Report • •
Full Service Analytlca1 & Environmental Solutions
5/15/01 Page 8 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: CONFLUENCE
501 Madison Ave ·Prism Samole ID: AC05990
Cary, NC 27513 LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
,A,{ cJ.. I-,'-f_ -VJ ~.L' Lab Submittal Date/Time: 5/1 /01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ETHYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1, 1, 1,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
TOTAL XYLENE$ Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
STYRENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
ISOPROPYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
SROMOFORM Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1, 1,2,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2,3-TRICHLOROPROPANE Not detected ug/L 0.5 · 6230D 5/11/01 06:58 CMS
n-PROPYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
SROMOSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,3,5-TRIME_THYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
2-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
4-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMB
tert-SUTYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2,4-TRIMETHYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
sec-SUTYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
p-lSOPROPYLTOLUENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,3-DICHLOROSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,4-DICHLOROSENZENE Not detected ug/L 0.5 62300 5/11/01 06:58 CMS
n-SUTYLSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2-DICHLOROSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2-DISROMO-3-CHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2,4-TRICHLOROSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
HEXACHLOROSUTADIENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
NAPHTHALENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
1,2,3-TRICHLOROSENZENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
CIS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 62300 5/11/01 06:58 CMS
· TRANS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
MTSE Not detected ug/L 0.5 6230D 5/11/01 06:58 CMS
IPE Not detected ug/L 0.5 62300 5/11/01 06:58 CMS
NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinA Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road .a.. P.O. Box 240543 .... Charlotte, NC 28224-0543
Phone: [phone] .a.. Toll Free Number: I-800/529-6364 .a.. Fax: [phone]
Lab Report
5/15101
Compuchem
Bill Scott
501 Madison Ave
Cary, NC 27513
• •
Full Service Analytical & Environmental Solutions
Customer Project ID: NCSU
Customer Sample ID: CONFLUENCE
Prism Samole ID: AC05990
Loqin Group: 9359G4
Sample Collection Date/Time: 4127101
Page 9 of 12
Lab Submittal Date/Time: 511101 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Sample Comments:
TEST
RESULT
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD
UNITS LIMIT REFERENCE
DATEfTIME
STARTED ANALYST
NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinA Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road .,.,, P.O. Box 240543 .,.,, Charlotte, NC 28224-0543
Phone, 704/529-6364..,. Toll Free Number: 1-8001529-6364.,.,, Fax: [phone]
Lab Report • •
, Full Service Analytlcal & Environmental SolutiOns
5/15/01 Page 10 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: TRIP BLANK
501 Madison Ave Prism Sample ID: AC05994
Cary, NC 27513
Lo!lin Grouo: 9359G4
Sample Collection Date/Time' 4/27/01
,v1 "'-\.i-''f -w(,\. .\.-{, t-Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATErrlME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
DICHLORODIFLUOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
CHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
VINYL CHLORIDE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
BROMOMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
CHLOROETHANE Not detected ug/L 0.5 6230D 5/11/0102:11 CMB
TRICHLOROFLUOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1, 1-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
METHYLENE CHLORIDE Not detected ug/L 2.0 6230D 5/11/0102:11 CMB
trans-1 :2-DICHLOROETH ENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1, 1-DICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
2,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/0102:11 CMB
cis-1,2-DICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
CHLOROFORM Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
BROMOCHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1, 1, 1-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1, 1-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
CARBON TETRACHLORIDE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
BENZENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1,2-DICHLOROETHANE Not detected . ug/L 0.5 6230D 5/11/01 02:11 CMB
TRICHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1,2-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
BROMODICHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
DIBROMOMETHANE Not detected ug/L 0.5 6230D 5/11/0102:11 CMB
TOLUENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1, 1,2-TRICHLOROETHANE Not detected ug/L 0.5 6230D 5/11/0102:11 CMB
TETRACHLOROETHENE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1,3-DICHLOROPROPANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
DIBROMOCHLOROMETHANE Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
1,2-DIBROMOETHANE (EDB) Not detected ug/L 0.5 6230D 5/11/01 02:11 CMB
CHLOROBENZENE Not detected ug/L 0.5 6230D 5/11/01 02: 11 CMB
NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinA Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road..,, P.O. Box 240543 ..,, Charlotte, NC 28224-0543
Phone: [phone] ..,, Toll Free Number: 1-800/529-6364..,, Fax: [phone]
Lab Report • •
Full Service Analytical & Environmental Solutions
5/15/01 Page 11 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: TRIP BLANK
501 Madison Ave Prism Sample ID: AC05994
Cary, NC 27513 LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
Me.\.+t-i'-/-w o... .\-.1. r Lab Submittal Date/Time: 5/1/01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ETHYLBENZENE Not detected ug/L 0.5 6230D 511110102:11 CMB
1, 1, 1,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
TOTAL XYLENES Not detected · ug/L 0.5 6230D 5111101 02:11 CMB
STYRENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
ISOPROPYLBENZENE Not detected ug/L 0.5 6230D 511110102:11 CMB
BROMOFORM, Not detected ug/L 0.5 6230D 511110102:11 CMB
1, 1,2,2-TETRACHLOROETHANE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
1,2,3-TRICHLOROPROPANE Not detected ug/L 0.5 6230D 5111101 02: 11 CMB
n-PROPYLBENZENE Not detected ug/L 0.5 6230D 511.1101 02:11 CMB
BROMOBENZENE Not detected ug/L 0.5 6230D 511110102:11 CMB
1,3,5-TRIMETHYLBENZENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
2-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
4-CHLOROTOLUENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
tert-BUTYLBENZENE Not detected ug/L 0.5 6230D 511110102:11 CMB
1,2,4-TRIMETHYLBENZENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
sec-BUTYLBENZENE Not detected ug/L 0.5 6230D 5111/01 02:11 CMB
p-lSOPROPYL TOLUENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
1,3-DICHLOROBENZENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
1,4-DICHLOROBENZENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
n-BUTYLBENZENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
1,2-DICHLOROBENZENE Not detected ug/L 0,5 6230D 5111101 02:11 CMB
1,2-DIBROM0-3-CHLOROPROPANE Not detected ug/L 0.5 6230D 5111/01 02:11 CMB
1,2,4-TRICHLOROBENZENE Not detected ug/L 0.5 6230D 511110102:11 CMB
HEXACHLOROBUTADIENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
NAPHTHALENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
1,2,3-TRICHLOROBENZENE Not detected ug/L 0.5 6230D 5/11101 02:11 CMB
CIS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
TRANS-1,3-DICHLOROPROPENE Not detected ug/L 0.5 62300 511110102:11 CMS
MTBE Not detected ug/L 0.5 6230D 5111/01 02:11 CMB
IPE Not detected ug/L 0.5 6230D 5111101 02:11 CMB
NC Certification No, 402 -SC Certification No, 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road• P.O. Box 240543 • Charlotte, NC 28224-0543
Phone: [phone] ..,,. Tn11 Free Numher: 1-R00/529-6364 .._ Fax: [phone]
Lab Report • •
Full Service Analytical & Environmental Solutions
5/15/01 Page 12 of 12
Compuchem Customer Project ID: NCSU
Bill Scott Customer Sample ID: TRIP BLANK
501 Madison Ave Prism Samele ID: AC05994
Cary, NC 27513 LoQin Group: 9359G4
Sample Collection Date/Time: 4/27/01
Lab Submittal Date/Time: 5/1 /01 10:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
Sample Comments:
TEST
RESULT
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD
UNITS LIMIT REFERENCE
DATEfTIME
STARTED ANALYST
NC Certification No. 402 -SC Certification No. 99012 -NC DrinkinQ Water Cert. No. 37735 -FL Certification No. E87519
449 Springbrook Road..,,. P.O. Box 240543 ... Charlotte, NC 28224-0543
Phone: [phone]...,. Toll Free Number: I-800/529-6364...,. Fax: [phone]
SUBCONTRACT CHAIN-OF-CUSTODY RECORD
COMPU HEM Project Name: Samples shipped to: -.., ,., .i~.,,.._,,, CompuChem point-of-contact: (4) ~ /.l
a tlivi.~inn of L1t,crtr Aruly11ul Corp. NC.Sl 1 Contact \-l.-.111, t,_ ,,,. , "-
~-, ........ C
IAI -1 '\v,u --rh T Address: ,; 1 'I' c . V el • Phone: [phone] X "/@Cr .. •. , ·. .=,c-,.::,,t Fax: (919) 379-IU<'fn '
501 Madison Avenue Keport style: . I I,
Cary, NC 27513 ~.if,\;.--'·'~~ ..... tt\l--1'>-.,'lrr. .. ,I r'none: (((61.J) c~n. ~ c,M, Sampling complete? Yor N (see Note 1)
1-800-833-5097 Disk requirementf'..., fl Q_ Project Locale (stale) Project-specific (PS) or Batch (B) QC?
□VA 01 1. slUnace vvater 6. np t:Hanl', □vA#Z A. m..,I + Ice t-. Ice unly BOX #3 BOX#4 BOX#S
2. Ground Water 7. Oil B. HN03 + Ice G. Other F-Filtered H-High C-CLP T-TCLP
3. Leachate 8. Waste C. NaOH + Ice H. NaHSO4 + Ice U-Unfiltered M-Medium S-SW-846
·4. Rinsate 9. Other 0. H2S04 + lee I. ZnAc+NaOH + Ice L-Low W-CWA 600-series
5. Soil / Sediment I Sludge E. Unpreserved J. Methanol 0-Other
Box#1 Box #2 Box #3 Box #4 Box #5 PARAMETERS ·
I
" ru ~ u u
i:;::_ C 0 I-0 ii:' Remarks / Comments
~ ru C u ~ .0
Sample ID > ::, rn ::, -~ ru 0 ru -" ~ ..., 0 (see Notes 2 & 3)
>-~ " ru " tf1 -X ru ~ t3 0 m .E 0
ru ru -~ ~ ru ~ ro ;;; E ;;; ~ ~ a. .; 0 ru en ~ X ~ ~ .::i CCN
0 ,= ::; a. u:: w ::; ,. ::,
( --?,, ol, (\ rr,c,M ,r ""' t:' u.. L A 3 .J (',,t'.,~
( 1\.. t'rl.~ \ ~ w A, C I.A. L u 3 .J fiS~{
I C..t-m \' l HA O l t,' ii.. p u L--n 3 .J 059qc,
( ""'-, \, ) r r " ,~,.{} So f:' Ll L-(\ ) '
-'\ r./ ✓-/00 oS99&1 (rl,u)
J .so f: u L n I Dj( n\ 'Oo.· i<.t<, C\\~l /I;. n/~/n
l',\,'Ai, Q 0 ' .I\ I 01 int. GS'l<r;;J J • V •
< C',~ ~o 'f LA v u I ' h"~' ~ .J (\/Fr.,..., osciq3
-,-,,·, ~l(\MV 101\ F l A L n ~ ✓ "'/An\ o S99l..j
~
Clients Special Instructions: Temperature •c
Lab: Received in good condition? y or N Describe any problems:
#1 Relinquished by:(sig) / ,/. --'J:fg Date: 1//311/q #2 ~lin~uished by:(sig) Date: Relinquished by:(sig) Date:
Company Name: /: .... ~ -/ L Time:ff/qf) Company Name: Time: Company Name: Time:
#1 Received by:(sig) ''/'.: I., -;;.ate: 5-/ -o/ #2 Received by:{sig) Date: #2 Received by:(sig) Date:
Company Name: j),,..,_ '.-vvt-Time:/riYJ Company Name: Time: Company Name: Time:
Note ( 1) If "N" lab should batch samples to a wall remainder of project -maximizing batch size and minimizing OC ratio; if ".Y" lab should begin processing batches now. L{ JJ<-1&~
m, ' Note (2) Samples should be stored 60 days after date report a !ed at no extra cha ge
Nole (3) All lab copies of data should be retained f0r a minimum of 3 years.
Note (4) Please call poinl--ol-eontact to verity receipt of samples. Revision 0 2-10-99
• •
FORM 1
VOLATILE ORGANICS.ANALYSIS DATA SHEET
CL.I ENT SAMP~ NO.
OS9"
CONFLUENCE
Lab Name: COMPUCHEM Cotitract:
Lab Code: LIBRTY Case No.: SAS No.: SDG No.: Al991
Matrix: (soil/water) SOIL /5Q.J.:~e" f Lab Sample ID: Al991-3
Sample wt/vol: 5.0 (g/mL) G
LOW
Lab File ID: Al991-3A52
Level: (low/med)
% Moisture: riot dee:· 23
GC Column: EQUITY624--1.D; .. 0 .. 53 (mm)
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Extract Volume: (uL) ----Soil Aliquot Volume:
CAS NO. COMPOUND.
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodiflaoromethane
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromometharie·
75-00-3---------Chloroethane
75-69-4~----~---Trichlorofluoromethane
75-35•4---------1,1-Dichloroethene
75~09-2---------Methylene Chloride
156-60-5--------trans-l,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether
75-34~3---------1,1-Dichloroethane ·
--
108-20-3--------Isopropyl ether
594-20-7--------2,.2-Dichloropropane
156-59-2--------cis-l,2-Dichloroethene
74-97-5---------Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride ·
563-58-6--------1,l-dichloropropene
71-43-2---------Benzene
107-06-2--------1,2-Dichloroethane
79-01~6--------~Trichloroethene
78-87-5~--------l,2-Dichloropropane
74-95-3---------Dibromomethane
75-27-4---------Bromodichloromethane
10061-01-5------cis-l,3-Dichloropropene
108-88-3--------Toluene ·
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
FORM I VOA
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
6
Q
u
u u
u u
u
u u u u u u u u u u u u u u u u u u u u u u u u u u
u
13.
• FORM 1
VOLATILE-ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
<!'599.'3
CONFLUENCE
Lab Name:_ .COMPUCHEM
Lab Code: LIBRTY Case No.:
Contract:
SAS No.: SDG No.: Al991
Lab Sample ID: Al991-.3 Matrix: (soil/water) SOIL / S ~A :.IA~ AT
Sample wt/vol: 5.0 (g/mL) G
LOW
Lab File ID: Al991-3A52
Level: (low/med)
% Moisture: not dee. 23
Date Received: 05/03/01
Dat·e Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY624 ID: 0.53 .. -:-.------~": .. ;· .... --· (mm)
Soil Extract Volume: ____ (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-90-7------~-chlorobenzene '
630-20-6-------~1,l,l,2-Tetra6hloroethane
lo0-41-4--------Ethylbenzene --
100-42-5--------Styrene
75-25-2---------Bromoform
98-82-8---------Isopropyl Benzene
108-86-1--------Bromobenzene
96-18-4---------1,2,3-Trichloropropane
79-34-5-----c---l,l,2,2-Tetrachloroethane_-_
103-65-1--------n-Propyl.Benzene
95-49-8---------2-Chlorotoluene
106-43-4~-------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert-Butyl Benzene
95-63-6---------1,2,4-Trimethyl Benzene
135-98-8--------sec-Butyl Benzene
541-73-1--~-----l,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--------n-Butyl Benzene
96-12 -.8.-- - - - - - --1, 2 -Di_bromo-3 -chloropropane
120-82-1~-------l,2,4-Trichlorobenzene -
87-68-3---------Hexachlorobutadiene
91-20-3---------Naphthalene
87-61-6---------1,2,3-Trichlorobenzene
1330-20-7--~----Xylene (total)
FORM I VOA
Q
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
-6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
C u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
14
• FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET o5""'\ 9. 2,,,
MIDDLE
Lab Name: COMPUCHEM Contract:
Lab Code: LIBRTY Case No.: SAS No.: SDG No.: Al991
Matrix:. (soil/water).SOIL /f..12d.,JV'~J\-\ Lab Sample ID: Al991-2
Sample wt/vol: . 5.0 (g/mL).G
LOW
Lab File ID: Al991-2A52
Level: (low/med)
% Moisture: not dee. 24
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
· GC Column: EQUITY624 ID.: 0. 53 (mm).
~ .-.-·---·-, _:
Soil Extract Volume: (uL) ----
. CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodifluoromethane
74-87-3---------Chloromethane ..
75-01-4-------~-vinyl Chloride
74-83-9---------Bromomethane
75~00-3---------Chloroethane
75-69-4---------Trichlorofluoromethane
75-35-4------~--l,l-Dichloroethene
75-09-2---------Methylene Chloride
156-60-5---:~---trans-l,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether --
75-34-3---------1,1-Dichloroethane
108-20-3--------Isopropyl ether
594-20-7--------2,2-Dichloropropane
156-59-2--------cis-l,2-Dichloroethene
74-97-5---------Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
563-58-6--------1,l-dichloropropene
· 71-43-2------~--Benzene
107-06-2--------1,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5~~-------l,2-Dichloropropane
74-95-3----~----Dibromomethane
75-27-4---------Bromodichloromethane
10061-01-5------cis-l,3-Dichloropropene
108-88~3--------Toluene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane .--
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
FORM I VOA
Q
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7, u
7 u
7 u
. 7 u
7 u
7 u
7 u
7 u
7 u .7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
15
• •
FORM 1· CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET 0$"ctC,, 'l...
MIDDLE
Lab Name: COMPUCHEM . Contract:
Lab Code: LIBRTY Case No.: SAS No.: SDG No.: Al991
.·Matrix: ·(soil/water) SOIL/512..d,~evi-t-Lab. Sample ID:Al991-2
Sample wt/vol_: 5.0 (g/mL) G
LOW
Lab File ID: ... : Al991_-2A52
Level: (low/med)
% Moisture: not dee. 24
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil A:iquot Volume:
GC Column: EQUITY-6-2-4-ll.s.-O.53 (mm)
Soil Extract Volume: (uL) -~--
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) -UG/KG
108-90-7--------Chlorobenzene·
630~20-6--------1,1,1,2-Tetrachloroethane
100-41-4--------Ethylbenzene · --
100-42-5--------Styrene
75-25-2---------Bromoform
98-82-8~-•----~--rsopropyl Benzene
108-86-1--------Bromobenzene
96-18-4----~----1~2,3-Trichloropropane -
79-34-5---------1,1,2,2-Tetrachloroethane
103-65-1--------n-Propyl Benzene --
95-49-8---------2-Chlorotoluene
106-43-4--------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert-Butyl Benzene .
95-63-6---------1,2,4-Trimethyl Benzene
135~98-8-------~sec-Butyl Benzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenz~ne
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--~-----n,Butyl Benzene
96-12cs---------l,2-Dibromo-3-Chloropropane
120-82-1--------1,2,4-Trichlorobenzene -
87-68~3---------Hexachlorobutadiene
91-20 .. ~ 3--

-

-

-

-

-

-
-Naphthalene
87-61~6---------1,2,3-Trichlorobenzene
1330-20-7-------Xylene (total)
.
FORM I VOA
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FORM 1 CLIENT SAMPLE NO.
. VOLATILE ORGANICS ANALYSIS DATA SHEET -o 5qa, 0\
BACKGROUND
Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Contract:
SAS No.:
Matrix: (soil/water) SOIL/S..eJ:111\~"\t
SDG No. : Al991
Lab Sample ID: Al991-l
Sample wt/vol: .5.0 (g/mL)•G Lab File ID: Al991ClA52
Level: (low/med) LOW
% Moisture: not dee. 25
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot.Volume:
GC Column: .EQUITY6.2A-:L!=);__0.53 (mm)
Soil Extract Volume: ____ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND . (ug/L or ug/Kg) UG/KG Q
75-71-8---------Dichlorodifluo.romethane 7 u
74 -87-3 --·--

-

-

-

-
-Chloromethane 7 u
75-01-4---------Vinyl Chloride 7 u
74-83-9---------Bromomethane 7 u
75-00-3---------Chloroethane 7 u
75-69-4---------Trichlorofluoromethane 7 u
75-35-4---------1,l-Dichloroethene 7 u
75-09-2----C----Methylene Chloride 7 u
156-60-5--------trans~l,2-Dichloroethene 7 u
1634-04-4-------Methyl-tert-butyl ether --7 u
75-34-)------c--l,l-Dichloroethane 7 u
108-20-3--------Isopropyl ether 7 u
594-20-7--------2,2-Dichloropropane 7 u
156-59-2--------cis-l,2-Dichloroethene 7 u
74 -91.c5_ -

-

-

-

-

-

-
-Bromochloromethane 7 u
67-66-3---------Chloroform _ 7 u
71-55-6---------1,1,l-Trichloroethane 7 u
56-23-5---------Carbon Tetrachloride 7 u
563-58-6--------1,l-dichloropropene 7 u
71-43-2---------Benzene 7 u
107-06-2--------1,2-Dichloroethane 7 u
79-01-6~~-------Trichloroethene 7 u
78-87-5---------1,2-Dichloropropane 7 u
74-95-.3 -

-

-

-

-

-

-

-
-Dibromomethane 7 u
75-27-4---------Bromodichloromethane 7 u
10061-01-5------cis-l,3-Dichloropropene 7 u
108-88-3--------Toluene 7 u
10061-02-6------trans-l,3-Dichloropropene 7 u·
79-00-5---------1,1,2-Trichloroethane --7 u
127-18-4--------Tetrachloroethene 7 u
142-28-9--------1,3-Dichloropropane 7 u
124-48-1--------Dibromochloromethane 7 u
106-93-4--------1,2-Dibromoethane 7 u
FORM I VOA
11
• •
FORM 1·
VOLATILE-ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO. o_s-qq o\
BACKGROUND
Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Contract:
SAS No.:
Matrix: (soil/water) SOIL /<;.~J:M{/\-\-
SDG No.: Al991
Lab Sample ID: A1991-1
Sample wt/vol:·_ 5. O (g/mL) G Lab File ID: A1991-1A52
Level: (low/med) LOW
% Moisture: riot dee. 25
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY624-:ill.c, .. 0.53 (mm)
Soil Extract Volume: · (uL) ----
CAS NO. COMPOUND
CO~CENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-90-7--------Chlorobenzene·
630-20-6--------1 1 1 2-Tetrachloroethane , , , ----
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2°--------Bromoform
98-82-8-c---~---Isopropyl Benzene
108-86-1~-------Bromobenzene
96-18-4--~------l,2,3-Trichloropropane
79-34-5---------1,1,2,2-Tetrachloroethane
103-65-1--------n-Propyl Benzene --
95-49-8---------2-Chlorotoluene
106-43-4--------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert0 Butyl Benzene
95°63-6---------1,2,4-Trimethyl Benzene
135-98-8--------sec-Butyl Benzene --
541-73-1--------1,3-Dichlorobenzene .
106-46-7--------1,4-Dichlorobenzene
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--------n-Butyl Benzene
96-12-8---------1,2-Dibromo-3-Chloropropane_
120-82-1--------1,2,4-Trichlorobenzene
87-68-3---------Hexachlorobutadiene
91-20-3---~-----Naphthalene
87-61-6---------1;2,3-Trichlorobenzene
1330-20-7-------Xylene (total)
FORM I VOA
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North Carolina Department of Environment and Natural Resources
Dexter R. Matthews, Director
Mr. Michael Townsend
Remedial Project Manager
Division of Waste Management
November 30, 2005
Superfund Remedial & Site Evaluation Branch
Waste Management Division
US EPA Region IV
61 Fors~h Street, 11 th Floor
Atlanta, Georgia 30303
RE: Draft Results of Data Acquisition Activities Report for Aquifer Testing
North Carolina State University Lot 86 NPL Site
Raleigh, Wake County
Dear Mr. Townsend:
Michael. F. Easley, Governor
William G. Ross Jr., Secretary
The North Carolina Department of Environment and Natural Resources (NC DENR) Superfund
Section has received and reviewed the Draft Results of Data Acquisition Activities Report for Aquifer
Testing for the North Carolina State University (NCSU) Lot 86 National Priority List Site. The NC
DENR Superfund Section offers the attached comments.
The NC DENR Superfund Section appreciates the opportunity to comment on this document. If you
have any questions or comments, please feel free to contact me at [phone].
Attachment
Sincerely,
David B. Mattison
Environmental Engineer
NC DENR Superfund Section
cc: Mr. Rick Bolich, NC DENR Aquifer Protection Section
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone [phone] I FAX [phone] I Internet http://wastenotnc.org
An Equal Opportunity I Affirmative Action Employer-Printed on Dual Purpose Recycted Paper
Mr. Michael Townsend
November 30, 2005
Page 1
• •
Draft Results of Data Acquisition Activities Report for Aquifer Testing
North Carolina State University Lot 86 NPL Site
Table of Contents
I. Please correct the Table of Contents to indicate that Figure 14 is actually entitled "Site
Map with Monitoring Well Locations". Furthermore, Figure 14-Well Construction
Schematic-RW-1 and Figure 15 -Well Construction Schematic-PW-I, PW-2, PW-3, as
given in the Table of Contents, were inadvertently omitted. Please correct these
oversights.
2. Please .correct the Table of Contents to reflect Appendix F -Step-Drawdown Test Data
and Appendix G -Pumping Test Data.
Section 3.1.3.2 Slug Testing Procedures
3. Although the reasons for not conducting falling and/or rising head slug tests could be
ascertained with some difficulty for groundwater monitoring wells MW-12D, MW-41, and
MW-43D, the reason for not conducting a rising head slug test at monitoring well MW-34SR
could not be determined (although the reason for not conducting the falling head slug test
could be determined from information provided in the fourth paragraph of Section 3.1.3.2).
Please revise Section 3.1.3.2 and Table 3 to more clearly present the reasons for not
conducting various falling and/or rising head slug tests, including at groundwater monitoring
well MW-34SR.
Section 3.1.3.3 Slug Test Data Analysis
4. In accordance with the slug test data presented in Appendix A, please correct the first
sentence of the first bullet item in the second paragraph of Section 3.1.3.3 to state "Shallow
wells: K for falling head tests ranged from 0.2524 ft/day to 0.7452 ft/day and K for rising
head tests ranged from 0.0161 ft/day (MW3A) to 0.6067 ft/day."
Section 3.2.2.4 \Veil Construction
5. Please correct the fourth sentence of the first paragraph of Section 3.2.2.4 to state "The
extraction well (RW-1) was constructed of four-inch diameter stainless steel well materials
whereas two-inch diameter polyvinyl chloride (PVC) well materials were used for
construction of the monitoring wells (PW-I through PW-3)."
6. Please correct the third sentence of the second paragraph of Section 3.2.2.4 to state "The
monitoring wells PW-I through PW-3 were also completed at grade by setting 8" diameter
bolt-down, watertight manholes around each wellhead."
• •
Mr. Michael Townsend
November 30, 2005
Page2
Section 3.2.4.2 Initial Pilot Study
7. The closing parenthesis was inadvertently omitted from the end of the first sentence of the
third paragraph of Section 3.2.4.2. Please correct this oversight.
Section 3.2.4.3.2 Conducting the Test
8. Please correct the third sentence of the second paragraph of Section 3.2.4.3.2 to state "The
manual water le.vel readings for these wells are provided in Table 4."
Section 3.2.5.1 Aquifer Parameters
9. In accordance with the information presented in Table 3, please correct the second and third
bullet points in the second paragraph of Section 3.2.5.1 to state the following:
• "Horizontal hydraulic conductivity (K): ranged from 0.4446 ft/day (PW-2) to
0.8194 ft/day (PW-3), ·
• Vertical hydraulic conductivity (Kv): ranged from 0.0351 ft/day (PW-2) to
1.0443 ft/day (PW-3),".
I 0. . In accordance with the information presented in Table 3, please correct the fifth bullet point
in the second paragraph of Section 3.2.5.1 to state the following:
• "Specific yield (Sy): ranged from 0.0091 ft/day (PW-2) to 0.0170 ft/day (MW-
12)."
11. Please correct the spelling of the word "significant" in the second sentence of the third
paragraph of Section 3.2.5.1.
Section 5.0 Summary and Conclusions
12. Please correct the fifth sentence of the second paragraph of Section 5.0 to state "Most of the
difference in the average K values between the shallow and intermediate zones was
accounted for by K values for two of the intermediate wells (MW3B and MW41I) that were
generally about an order of magnitude or so lower than the K values for the remainder of the
intermediate wells."
13. Upon recalculating the statistical evaluation of specific yield and storativity (see Comment
#17 and Comment #19), please revise the values given for specific yield and storativity in the
second sentence of the fourth paragraph of Section 5.0.
Mr. Michael Townsend
November 30, 2005
Page3
•
Table 1 Well and Groundwater Elevation Data
•
14. Please correct the spelling of the word "Elevation" in the column heading "Top of Casing
Elevation (ft)" of Table I. Furthermore, please define the abbreviations "TOS" and "TD"
used in Table I.
Table 3 Aquifer Testing Data Analysis Summary
15. . In accordance with the slug test data presented in Appendix A, please correct Table 3 to
indicate that the hydraulic conductivity at groundwater monitoring well MW-3A during the
rising head slug test was 0.0161 feet per day (ft/day).
16. In accordance with the pumping test data presented in Appendix G, please correct Table 3 to
indicate that during the aquifer pumping test the horizontal hydraulic conductivity is 0.4446
ft/day and the specific yield is 0.0091 at groundwater observation well PW-2.
17. In accordance with the revisions noted in Comment #16, please recalculate the arithmetic
mean, geometric mean and standard deviation associated with the values determined for
specific yield in Table 3.
18. In accordance with the revisions noted in Comment #16, please recalculate the storativity
associated with observation well PW-2 in Table 3.
19. In accordance with the revision noted in Comment #18, please recalculate the arithmetic
mean, geometric mean and standard deviation associated with the values determined for
storativity in Table 3.
20. In accordance with the pumping test data presented in Appendix G, please correct Table 3 to
indicate that during the aquifer pumping test the horizontal hydraulic conductivity at
groundwater observation well PW-3 is 0.8193 ft/day.
NORTH CAROLINA STATE UNIVERSITY
ENVIRONMENTAL HEAL TH AND SAFETY CENTER
NOTE
To:
Subject:
Date:
David Mattison
Lot 86 Surface Water and Sediment Sampling Procedure
April 24, 2001
Notes & Information
David:
•
Attached for your review arc two copies of the sampling and analysis procedure for the surface water and
sediment samples to be collected from Richland Creek.
Duane Knudson
Environmental Affairs Manager
[phone]
(919) 5 15-6307 fax
duane [e-mail]
•
NC STATE•UNIVERS'i'r.v,·:
' " • l ' , '~ ~
Michael Townsend
North Carolina State Universil land·
grant university and a constituent institution
of The University of North Carolina
An Equal Opportunity/Affinnative Action Employer
http:/ /www2. ncsu .edu/ncsu/ehs/
April I 0, 200 I
Superfund Branch, Waste Management Division
US·EPA Region IV
Atlanta Federal Center
I 00 Alabama Street, SW
Atlanta, GA 30303-3104
Dear Mr. Towns.end:
Office of Finance and Business
Business Division
Environmental Health & Safety Ce
Campus Box 8007
Raleigh, North Carolina 27695-8007
Director
Environmental Affairs
Industrial Hygiene
Health and Safety
Radiation Protection
{Fax)
919.515.42,
919.515.68:
919.515.68[
919.515.68:
919.515.28,
919.515.63(
Submitted with this letter are five copies of the sampling and analysis and quality assurance plans
for the spring 200 I groundwater sampling at Lot 86.
As we discussed, companion plans for surface water and sediment sampling for the potentially
affected areas of Richland Creek are being prepared ..
If there are any questions or comments on this, please let me know.
s~
Duane·A. Knudson
cc: ~CDENR (2 copies)
David Rainer (w/o enclosures)
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. -:<,-' ··: '. '::,:".:.' qbjectives.of the:s.~!jipEI)g_an~ \mily~is of.sed.i.ni~!]t _an_d surface \Yater ·sainplesfrorn near_,':;.'.,:-~.".; i', .. :
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.,, ••• ,-.·,· ~ t'~ ._;-,:.:.:.:r ,•-::<:·, .. ,:.'.:.::;-.'
;, -,_.; :.L: ;:;: :/>~b~~~~e.nt, ib::i?}iecti~f ~nd ~ilJ ~~'.ir~n~_P9~:~f rr_on'i /h~}jt~. t<i ¢q~ii~¢~~n:: '1.~§:' ;iiher -_ ':f. , _: .. :: · -
. · · · ·,./· ·. ·by samplmg or laboratory personnel:'In keepmg with Cham-of-Custody·requirements,all-. '· ,··/.:;:, :
; ••: /(i->" \( ~amples ircinsp,orted io the laboratory, wi!i" be ide~tifi~cl jn. ;~cord_an~e. 0iih s·~ctions .4.4;·2 •. . \:;:: '.i '.\
· .. ''-'\:,,;:1;:~?;1~r-~:1:i"j,;:~~st~!e~-~~<;r~:; .,.· ·. -~ .:; ... , .. ·.· ... ::.\i_::~ );,ji~fr::::::;/,\ ::::.:':\'.:/s,r;-"·· .::i.;>· .·•.•··· .•···.·.: ::.:?~:: '..: .·::-'' ·.;•::,:::· , ... · .
. /-'· . \::::Subsequent to;the·collectlon.·or.a san'iplefror.n an1/·g1yen:loc(!hon·(we)l)/ ea~lfcgntamer· .. ... .. .. . . ,····,, ,. ',., .. ,,:<"'-" -~ .... • .. ,-•. -•, ·.··-.'•:•;·.:·,;· .:;.• ·.·. ',•:.-·.;.•···:•::;~,--,··: -,.,,..' ... -·,_ .. ,,;,·,, '::·•-... ../ -. ,•,,,·.-_,-.• ,•,_· ·_ ..•. -.... , ,;•:"'·•'.'':,:.·•,·',"·. '1~• ,. <, .. ··._ ·:.:::0w1lI:be placed on ice ma cooler withm mmutes·ofcollect1on: Samples will be secured m ,:;.•:; ,,.
. :'. :'} -:•;; t99Jefs••~i_ih·}juffi6i~pf ·~iiiou~i• 6(jc'~'/t~·;~riJlYr~; pr6p~i. p;es~ryati6p;ia:~g;\~~ll;;; {{ __ ·:;::_ ):, C•
.. ·· ·•·.·•/', ;}-rii:tcessary,be se9ure:d\vithin the cooler(sY utili#ili;bubb.le w.r~p oi;fqain packing/at .the ;< . · .,, .. ' _
•~,, '.,'•··;:,.,1,'•J',·.',"',• ,,,_.· .• ·,.,•· ~:·•:.~(_'·,,-.. ,,,•,'_ ·,f"::•·,·-:-· ·_-·-. ,-;•.:,,,,'.·•·. '··• ,'.· ".,>•'"•,•'··• '··'C),-,.•.,;._, :,,~, ,,,.;;-'·. --.••-~•''·,, ', , .-·. ::· •·.;-,_--,;:' discretion p_tthe ,sampling personnel or .CompuChem: Care will be taken to ensure that_" -· ·:'• ·· _.-,_,,.
· ~'.;·'i. ,_:, ~n~,sa~ple_s r~;1ich ~ .temperatu~e·wi,i~h\½,il\ cau1e th~ .. ·sari!pl~(_§)tb'free~e/ .. /,."• '<, ... • ';/;}t\, ·:•-:•:-·::, ,,
· •. i_;,_;_-·: /:\,.!:'._:
• • FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET -o 5:qq 0\
BACKGROUND
Contract: Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No. : Al991
Lab Sample ID: Al991-l
Sample wt/vol: 5. 0 (g/mL) G. Lab File ID: Al991~1A52
Level: (low/med) LOW
% Moisture: not dee. 25
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY62;4_ .. ~J?:._0._53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodifluoromethane
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-69-4---------Trichlorofluoromethane
75-35-4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride
156-60-5--------trans-l,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether
75-34-3---------1,1-Dichloroethane
--
108-20-3--------Isopropyl ether
594-20-7--------2,2-Dichloropropane
156-59-2--------cis-l,2-Dichloroethene
74-97.-5--

-

-

-

-

-

-
-Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
563-58-6--------1,l-dichloropropene
71-43-2---------Benzene
107-06-2--------1,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
74-95-3---------Dibromomethane
75-27-4---------Bromodichloromethane
10061-01-5------cis-l,3-Dichloropropene
108-88-3--------Toluene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --.
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
FORM I VOA
Q
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u·
7 u
7 u
7 u
7 u
7 u
11
• • • FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET 0.59q Q\
BACKGROUND
Contract: Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No.: Al991
Lab Sample ID: Al991-l
Sample wt/vol: 5. 0 (g/mL) G
LOW
Lab File ID: Al991-1A52
Level: (low/med)
% Moisture: not dee. 25
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY624-IDo, .. 0 .. 53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
108-90-7--------Chlorobenzene ·
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
630-20-6--------1 1 1 2-Tetrachloroethane ' ' ' -·-
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
98-82-8---------Isopropyl Benzene
108-86-1--------Bromobenzene
96-18-4---------1,2,3-Trichloropropane
79-34-5---------1,1,2,2-Tetrachloroethane __
103-65-1--------n-Propyl Benzene
95-49-8---------2-Chlorotoluene
106-43-4--------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert"Butyl Benzene
95-63-6---------1,2,4-Trimethyl Benzene
135-98-8--------sec-Butyl Benzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--------n-Butyl Benzene ·
96-12-BC--------l,2-Dibr?mo-3-Chloropropane_
120-82-1--------1,2,4-Trichlorobenzene
87-68-3---------Hexachlorobutadiene
91-20-3---------Naphthalene
87-61-6---------1;2,3-Trichlorobenzene
1330-20-7-------Xylene (total)
FORM I VOA
Q
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
12
•• • FORM 1 CLIENT SAMPLE NO,
VOLATILE ORGANICS ANALYSIS DATA SHEET c)_Q:\, '\. 2_
MIDDLE
Contract: Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
Matrix:. (soil/water) SOIL
SAS No.: SDG No. : A1991
Lab Sample ID: Al991-2
Sample wt/vol: 5. 0 (g/mL) G
LOW
Lab File ID: A1991-2A52
Level: (low/med)
% Moisture: not dee. 24
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY624 ID: 0.53 (mm)
Soil Extract Volume:_ (uL) ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
75-71-8--

-

-

-

-

-

-
-Dichlorodiflu.o_romethane
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-69-4---------Trichlorofluoromethane
75-35-4------~--l,l-Dichloroethene
75-09-2--~------Methylene Chloride
156-60-5--~-----trans-l,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether --
75-34-3---------1,1-Dichloroethane
108-20-3--------Isopropyl ether
594-20-7--------2,2-Dichloropropane
156-59-2--------cis-l,2-Dichloroethene
74-97-5---------Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
563-58-6--------1,l-dichloropropene
71-43-2---------Benzene
107-06-2--------1,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5~~-------l,2-Dichloropropane
74-95-3----~----Dibromomethane
75-27-4---------Bromodichloromethane
10061-01-5------cis-l,3-Dichloropropene
108-88-3--------Toluene
10061-02-6------trans-1,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
FORM I VOA
Q
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7, u
7 u
7 u
. 7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
15
• • FORM 1 CLIENT SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
.Lab Name: COMPUCHEM
Lab Code: LIBRTY Case No.:
. Matrix: (soil/water) SOIL
Sample wt/vol:
Level: (low/med)
5.0 (g/mL) G
LOW
% Moisture: not dee. 24
Contract:
SAS No.:
Lab
Lab
Date
Date
os::cic,, -z..
MIDDLE
SDG No.: Al991
Sample ID: Al991-2
File ID: Al991-2A52
Received: 05/03/01
Analyzed: 05/09/01
GC Column: EQUITY6-24 -sID., .,0. 53 (mm)
Soil Extract Volume: ____ (uL)
Dilution Factor: 1.0
Soil A:iquot Volume:
CAS NO. COMPOUND
108-90-7--------Chlorobenzene·
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
630-20-6--------1,l,l,2-Tetrachloroethane_·_
100-41-4--------Ethylbenzene
100-42-5--------Styrene
75-25-2---------Bromoform
98-82-8---------Isopropyl Benzene
108-86-1--------Bromobenzene
96-18-4---------1,2,3-Trichloropropane
79-34-5---------1,1,2,2-Tetrachloroethane
103-65-1--------n-Propyl Benzene --
95-49-8---------2-Chlorotoluene
106-43-4--------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert-Butyl Benzene
95-63-6---------1,2,4-Trimethyl Benzene
135~98-8--------sec-Butyl Benzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--------n-Butyl Benzene
96-12"8---------1,2-Dibromo-3-Chloropropane
120-82-1--------1,2,4-Trichlorobenzene -
87-68~3---------Hexachlorobutadiene
91-20~3---------Naphthalene
87-61-6---------1,2,3-Trichlorobenzene
1330-20-7-------Xylene (total)
FORM I VOA
Q
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
7 u
16
• • FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMP:f NO.
a S9 °' -CONFLUENCE
Lab Name: COMPUCHEM Contract:
Lab Code: LIBRTY
Matrix: (soil/water)
Case No.:
SOIL
SAS No.: SDG No. : A1991
Lab Sample ID: A1991-3
Sample wt/vol: 5.0 (g/mL) G Lab File ID: A1991-3A52
Level: (low/med·) LOW
% Moisture: not dee. 23
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY6Z4--I0·;.0 .. 53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
75-71-8---------Dichlorodifluoromethane
74-87-3---------Chloromethane
75-01-4---------Vinyl Chloride
74-83-9---------Bromomethane
75-00-3---------Chloroethane
75-69-4---------Trichlorofluoromethane
75-35~4---------1,1-Dichloroethene
75-09-2---------Methylene Chloride
156-60-5--------trans-1,2-Dichloroethene
1634-04-4-------Methyl-tert-butyl ether --
75-34-3---------1,1-Dichloroethane
108-20-3--------Isopropyl ether
594-20-7--------2,2-Dichloropropane
156-59-2--------cis-1,2-Dichloroethene
74-97-5---------Bromochloromethane
67-66-3---------Chloroform
71-55-6---------1,1,1-Trichloroethane
56-23-5---------Carbon Tetrachloride
563-58-6--------1,1-dichloropropene
71-43-2---------Benzene
107-06-2--------1,2-Dichloroethane
79-01-6---------Trichloroethene
78-87-5---------1,2-Dichloropropane
74-95-3---------Dibromomethane
75-27-4---------Bromodichloromethane
10061-01-5------cis-l,3-Dichloropropene
108-88-3--------Toluene
10061-02-6------trans-l,3-Dichloropropene
79-00-5---------1,1,2-Trichloroethane --
127-18-4--------Tetrachloroethene
142-28-9--------1,3-Dichloropropane
124-48-1--------Dibromochloromethane
106-93-4--------1,2-Dibromoethane
FORM I VOA
Q
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
13
.-. • FORM 1
VOLATILE ORGANICS ANALYSIS DATA SHEET
CLIENT SAMPLE NO.
<.'.) 5 9.9. 3.
CONFLUENCE
Contract: Lab Name: .COMPUCHEM
Lab Code: LIBRTY Case No.:
Matrix: (soil/water) SOIL
SAS No.: SDG No. : Al991
Lab Sample .ID: Al991-3
Sample wt/vol: 5.0 (g/mL) .G. Lab File ID: Al991-3A52
Level: (low/med) LOW
% Moisture: not dee. 23
Date Received: 05/03/01
Date Analyzed: 05/09/01
Dilution Factor: 1.0
Soil Aliquot Volume:
GC Column: EQUITY~.f-~.,tP..:.o.: 53 (mm)
Soil Extract Volume: (uL) ----
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG
108-90-7--------Chlorobenzene
630-20-6--------1,l,l,2-Tetrachloroethane
100-41-4--------Ethylbenzene --
100-42-5--------Styrene
75-25-2---------Bromoform
98-82-8---------Isopropyl Benzene
108-86-1--------Bromobenzene
96-18-4---------1,2,3-Trichloropropane
79-34-5---------1,1,2,2-Tetrachloroethane
103-65-1--------n-Propyl Benzene --
95-49-8---------2-Chlorotoluene
106-43-4--------4-Chlorotoluene
108-67-8--------1,3,5-Trimethyl Benzene
98-06-6---------tert-Butyl Benzene
95-63-6---------1,2,4-Trimethyl Benzene
135-98-8--------sec-Butyl Benzene
541-73-1--------1,3-Dichlorobenzene
106-46-7--------1,4-Dichlorobenzene
99-87-6---------p-Isopropyl Toluene
95-50-1---------1,2-Dichlorobenzene
104-51-8--------n-Butyl Benzene
96-12-.8--

-

-

-

-

-

-
-1, 2-Dibromo-3-Chloropropane
120-82-1°-------1,2,4-Trichlorobenzene -
87-68-3--

-

-

-

-

-
-·-Hexachlorobutadiene
91-20-3---------Naphthalene
87-61-6---------1,2,3-Trichlorobenzene
1330-20-7--~----Xylene (total)
.
FORM I VOA
Q
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
G u
6 u
6 u
6 u
6 u
6 u
6 u
6 u
14
V
Box 8208
• North Carolina State University·
Department of Marine, Earth and
Atmospheric Sciences
College of Physical and Mathematical Sciences
RfCEIVtt,
JAN 19 1990
SUPERFUND SECTION
Haleigh, NC 27695.8208
[phone] January 18, 1990
T01 Charlotte Varlashkin
Division of Solid Waste Management
N,C, Superfund Section
From, Charles w. W~.Jl J~
Subject, NCSU Lot 86 Site Chemical Analyses
Enclosed are computer printouts of the analytical data that
we have for the Volatile Organics at the Lot 86 site. Data
from the most recent sampling events are still being worked
on inihe GC laboratory. The data on the computer printouts
are those obtained in the NCSU GC/MS laboratory.
If you have any questions, please give me a call,
Enc,
cc1 Bruce Mac Donald
North Carolina State University is a land-grant university and a constituent institution of The University of North Carolina.
1
Ddte:,
0 :::1 J :~1 .. t:1 ~:.',;
0325n85
0'-1-() 1 .. 8~5
0722.B5
l C.1.0Lt" B'.7.~
O:l 21. 86
()E!t.:!1':1 p 86
0513 .. 86
07 l.f.J" 86
0917 .. 06
1120. E16
O::l :l 13. ff7
051 li-.. 87
0(:306.87
0203 .. 88
07lf.?." t3U
l.020.8S
O'.'..i3l. 8'?
07f27" 89
l·Je 11 Il8
2
::r u. 1 :l. t:~. ·n
Da,y
1. l ,:'::!E~
ll.80
l :I. ff?
l C:?.99
J.(+3L1.
11-,132
1 ~5 :I. 8
l 59'+
1C'.>5El
l ?E?.1
1 78~5
:l 'iO::l
1960
E?.0'-t'·I·
222'.S
2 :~_I !:'.J ~'.i
21-1-8~:':i
;;_~f:.>t+7
27(:)5
•
::l 4
Diethyl Chloro-
Ethe·1-1·orm
0,. O~)e,' l " 71 f.:'.
On038 2 .. 111
0 .. 000 0" '7E!O
0 .. 021 0.66f:J
0 .. 01.3 l .. 07(2
0 H 008 0 H 71 ~:;
0. 0 l O O .. f::,59
0 .. 005 l .. O~i:-3
0 .. 008 l .. 056
O .. 003 :I. • ::JEI?
0.0:1.0 (l,.980
() H 000 0 ,0 68'~/
().(l(l'J (),.t:jl'78
(}" ()()() 1) n l {:1Lt
o. oo;~~ o. 7.::.,~i
0 .. 007 l .. ()E~B
On007 1. .. 51.3
0 H 000 (?. n '•t73
0 .. 000 0.000
CCl'1
-0,. lOL,j,
0.1C.~4
0 .. 070
o,. 0:-33
0 .. 077
0 .. 067
0.062
0 .. 092
(l n (l6Lt
0" (lf.~?,2
0.058
O.,OOE:l
() ■ ()7C/
0" 0'+3
0 .. 086
0. 07t:
(),, 1.61
0. 1 F:}6
0,. 000
•
6 7 8
Benzene Tri Cl Di Cl
0.000 0.206 0.000
0.063 0.249 0.024
0.000 0.09() 0.000
0 .. 000 0.088 0.000
0.000 0.139 0.000
0.000 0.108 0.000
0.000 0.121 0.000
0"001 ().166 0 .. 004
0.000 0.150 0.000
0.000 C> .. 198 0.000
0.002 0.149 0.000
c:).000 0.143 0.000
0.000 0.164 0.000
0 .. 000 0.117 0 .. 000
0 .. 000 0.166 0.009
On002 0.139 0.0(>0
0.004 0.242 0.024
0.000 0.358 0.047
0.000 0.0!)0 0.000
1
Date
0313.85
0325n85
0401.85
0722.85
1204.85
0121.86
0226.86
0513.86
0716.86
0917.86
1120.86
0318.87
0514.87
0806.87
0203.88
0712.88
1020.88
0331.89
0727.89
Well #8 •
2 9 10
Julian Tri Cl Tat Cl
Day Ethane Ethene
1168 0.000 0.136
1180 0.000 0.092
1187 0.000 0.100
1299 0.000 0.06()
1434 0.000 0.138
1482 0.000 0.105
1518 0.000 0.135
l.594 0.000 0.273
1658 0.000 0.121
1721 0.000 0.147
1785 0.(>00 0.108
1903 0.001 0.115
1960 0.002 0.132
2044 0.()01 0~167
2225 0.002 0.163
2385 0.000 0.101
2485 1).012 0.123
2647 0.014 (1.236
•
1 2 3 . 4
Date Julian Diethyl Di Cl
Day Ether Metha~1e
0606.85 1253 0.055 0.00()
0716.85 1293 0.048 0.000
1212.85 1442 0.024 0.()00
013().86 1491 0.011 0.000
0304.86 1524 0.039 0.000
0520.86 1601 0.010 0.000
0730.86 1672 0.01() 0.000
0917.86 1721 0.000 0.00()
1120.86 1785 0.009 0~072
0408.87 1924 0.000 0.000
0414.87 1930 0.004 o.oc,o
0721.87 2028 0.010 0.011
1120.87 2150 0.040 0.060
03()9.88 2260 0.045 0.705
0804.88 2408 0.432 0.052
Ch lDf'Ci"··
-rei·1··m
0. 211
0 .. 8~59
0 .. ~50(:_,
0.619
0 .1390
1.219
1. 687
l "09L1,
0 .. 709
l "l:,'+'7
l ., 68L~
t.:! .. 196
l.'+7f3
L+" /.~96
•
6
CCl.i+
0 .. 09~:::j
o. 122
0 .. ~~r.?.:::1
o .. r~1t+
O.C:!19
0. 3'-i'?
0.5lt.~
0.'769
O .. 2f.~ l
0 .. 2!:-J8
0 .. ~ili-0
() n ftCJ6
O.~SlO
0. 23C?.
0 .. 36t+
7 8
Eiec1zef1t~ Tr· i Cl
Etherie
0.000 0 .. 030
0. 000 0. Oi:?.7
0 .. 000 OH05L+
0 H 000 0 "()3~':i
0.,000 (),,()l~8
0 .. 000 0 .. 062
0 .. 000 0 .. 0 1::;1
0 .. 000 0 .. 089
0 .. 000 0 .. 067
0 .. 000 0 .. 063
(i" (l()() () n l 4Lt·
0 .. 000 0 .. 133
0 .. Or.'.:>3 0 .. l 66
(),, ()bf+ ()" J l+C/
0 .. 17~:3 O.,E73
Ot:106 .. B~i
0716 .. 1:l~i
l.212 .. 1:1'.'j
0130 .. f.:16
030'+ .. f36
0520 .. t16
07::.~o .. 86
091.'7.86
:I. :l.E~O,.f.:16
01to0 .. a?
()lj, 1 t+ • f:1 ')'
0721 .. 1:17
l lf.:~O,, 87
o:301?" 88
0801..~,, 88
l·Jel 1 16
2
,Jul :i. a.n
Day
12~;::1
1293
:J.f+l+2
1 t+9 l
l :'::i2t.+
1601
167E'
l 7E.:!. 1
1 '71:.l'.5
1 '~f f.:!l-t
1 "r'.:lO
2028
E:~ l '.:~O
C.~2f:10
f.~t+08
F·· 1--1 ~\ •
9 10 11 12
Toluene Tri Cl Tet Cl Di Dr
Ethane Ethene Etha11e
0.000 0.010 0 .. 000 0 .. 00(1
0.000 0.000 0.018 0.000
0.000 0 .. 051 0 .. 0£~9 0.(>00
0.000 0.000 0.000 0.000
0.000 0.000 0.046 0.000
0.000 0.000 0.068 0.000
0.()00 0.000 0.069 0.000
0.000 l).000 0.271 0.000
0.000 0.000 0.041 0.000
0.000 0.000 0.257 0.000
0.000 0.000 0.()88 ().,000
0.000 0.000 0 .. 090 0.001
0.000 0 .. 000 0.121 0.0()8
0.003 0~000 0.092 0.006
0 .. 012 0.002 0.102 0.(>26
1 ::1
Cl BE:n:.:-!
0 .. 000
0 .. 000
0 .. 000
0.000
0.000
0.000
0 .. 000
0"000
0 .. 000
0 .. 000
0 .. 000
0.001
o .. oo::!
O .. ()Of+
0 .. 015
l ,,
Xyle!nE•
0 .. 000
0.000
0 .. 000
0 .. 000
0 .. 000
0.000
0 .. 000
0 .. ()00
() .. 000
0 .. 000
0 .. 000
0 .. 000
0. 00.lt
0.004
0 .. 0::10
l
Oiite
0606 .. 8~:;
07l6,,8~3
1212"~3::;
01.:CIO .. El6
030't. 86
O~'.i20 .. 86
07:30.86
O''i'l.7 .. 86
1120 .. !:16
()l+(l8" f:17
()l.i, 1 l,t ~ f:1'7
O?E!l .8'/
l 120.8'7
0309 .. fJB
080lt., BB
.Jul iar1
Day
:I. t:~5:3
1293
1 '-tltE~
l <19 l
1 ::H?.Lt
1601
16'72
l '72 l
l 7f:l5
:l 9(:~l~
1';,::w
2o;~~t➔
21~i0
2E.!60
2'+0[~
Fil~
l ~:i
X y 1 E'l"rf.-:'
0 .. 000
0., 000
0~000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0~000
0 .. 000
0~000
0 .. 000
0 .. 002
0 .. OO~J
0 .. 02'-t
•
l.
Dt"..1te
0909.86
11l.1 .. El6
0128 .. !:37
01.t0ln8'7
100::?.aB'7
0309.8l:I
01304. 88
l Of::!'/ .. EJEI
0lJC~3 • Be;
1
Dato,,
l. l l l .. 86
()ltO 1 n 87
0'7E!l. .. 87
1 :l 20. 8'7
0309 .. BE.~
OE~O'+ .. EiB
l.027.88
0~~>23. 8G
ltlel l #27 I
2 '.3
Jul ia::\n ChlDi"Cr-
Day ·form
171'.3 On0:32
1776 On028
18~:;.::. 0 .. 010
l 917 0,. OC~B
2101 0 .. 000
2260 0 .. 0 :I. :-J
Et+08 0 a 008
2'·~9F.~ 0 "0 l '.]
f.;'.731 0 n 009
2 3 4
Julian Diethyl Di Cl
Day Ether Metha11e
1776 0 .. 000 0 .. 000
1917 0 .. 011 OnOOO
2028 ONOOO 0 .. 000
2150 0.000 Oal)OO
226() 0.000 0.000
2408 0 .. 000 0 .. 0()0
2492 0.000 0.0()0
2731 0 .. 021 1),,035
Ch lCti'"'O""
t·or·m
0 .. 000
0 .. 000
0 .. ()00
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 006
6
Ben:•":.f.~nt?
0 .. 000
0.000
0 .. 000
0 .. 000
0.000
0.000
0.000
0 .O:'.iO
1
Date
0219.85
0917.85
0613.86
0408.87
1002.87
0420.88
0719.88
1027.88
0331N89
Well #4
2 3 4
Julian Di Cl Chloro-
Day Methar1e for·m
1146 0.000 0.0()0
1356 0.000 0.000
1625 0.000 0.000
192'~ 0.002 0.000
2101 0.000 0.000
2302 0.000 0.002
2392 0.000 0.000
2lt92 0.000 0.003
2647 0~000 0.000
CC14
0.00()
O.OOl)
0.000
0.003
0.005
0.008
0.()00
0.006
0.000
•
1
Di::\tE2
1024. 8'►
0325 .8~i
0401.B~i
09(.7~L1-.. El'.:'.i
1 ;;:?.O~i. E3~5
01.E.!l .. 86
0225 .. 86
0513~86
0'716. f36
091 '7 .. tl6
:l. i.~O~:i. 8(.:}
020l+ "B7
0318 .. 87
O~il'+ .. B?
1002.87
0 lf.20 .. 8f::J
Ol;2i:-!., Bt:J
1.022 .. f:18
l✓ell #2
,~
,Jul iitn
Da,y
:t.028
l J.80
11 fl?
l~'l63
1'-~'.:3~::;
J.ltf3~?.
1 ~i J 7
1. ~/9lt
:t 6~38
J.'721
1£100
l f:31'.::i 1
1903
1960
210:l
i::21 l
E~~365
f:.~t+tl:=.~i
1 ~:-;
Eth Eic~nz
0 .. 030
0 .. 070
0.030
0.077
0 .. 0'73
0,, l ()8
0. 1. 't=i
0. 064,
0 .. (llf'-7
0. 2'+ 1
0 .. ::i'-t~S
0 .. l 10
0. 10'.3
0.218
0 .. 248
0 .. 2'+7
0. 3-:-. .i1:3
O.t+?t+
16
Xylt::nE!
0. :I. :I. 0
0 .. 5:::JO
0" 100
0.431
o .. c,~:=.;o
0 .. '70f.-J
0 .. 7~~:JE?.
0 .. 589
0 .. 440
l .. '.343
3 .. '.35:3
0 .. ~it3'7
0" ~36 :I.
0.'rf:>4
1. 170
1 .252
l .. 8/~lt
t?. a 09/:?.
17
Xylr:?ne
0 .. OElO
(>., lL1-0
0.090
0 .. 147
0 .. 162
0" l t:i9
() .. 209
o .. U.2
0 .. 4lt0
0 .. E.!60
0.611
0. J. Ell
!) ":t CJLt
O .. :JO:CI
0 .. 4't7
0 .. 43-'+
0 .. 6r..77
0 .. 790
•
:l
Da. tE:!
l Of.::!t+" Bl+
032:::1 ~ 8~.S
OL+O 1.. 85
092Lt .. B5
l205 .. f35
0121.f.16
022~5 n 86
o~::; 1 ::.1. El6
0716.86
0'-71 '7. 86
120'.:i. Ei6
Ot.~Ot+. 87
03 lf:.~,, El'?
0'.51'+ a 87
:I. OOE:' .. ff/
0 :I. 20 .131:!
06E.~i.::.! .. E\(:3
:l 02/?. .. fJB
I ,, '"
~Tul:i.an
Dc,y
1. O[c!B
11 FJO
1. l !37
1'.363
l ,,3:5
1 lt82
1 '.'; l '7
1~.i94
1. 6'."iB
1 "?E! 1
lUOO
:U361
190:1
J.i:,'160
21.0J
E~P 11
E!365
E~t+!:3!5
ft. 8
C/ 1 ()
Di Cl C:H:3
Pr·opane Pentano~1e
0 .. 000 0.000
O .. l c;o O. 100
0 .. 000 OnOOO
()" 1 S,1lt O" ()()()
0 .. 077 0.000
0. t.~21 0 .. 309
0.1~53 On253
0.000 0 .. 280
0 a ::.~::..'.J4 0 a ~i09
0. 221 0. 301+
0 .. 386 0 .. 65~~
0. 121:! 0., 1 'i?
0.153 0.161.
o .. 3:3? o. c:i2::i
O.lL,t:, O.lEIB
0 " 000 0 . !:.i :t t'.)
0. ?Ot;. ::.i. ;;:!(TEI
1 ., :39(3 L~ n (}f+6
l.l
·ro 1 u1-:-::-nf2
0 .. 290
~i .. Lt60
6 .. 900
:3 "?::i?
~3~7'+:::1
f.:) .,'.375
6 .. 23?
:➔ • ?El'i
2.flOO
j_Li..,fl76
i?. El • '7'.3 i.c
6 .. 7'.53
ti .. t+Ol+
12.,.21
t:3."73',
1 i.:J. "2lt0
23 .. '799
•
12
Tet C:l
Ethf2\'li:2
o .. 1.2~5
0. :l'iO
0 .. 360
0. 169
0 .. 2;~!,8
0.3H:
0 .. ~32(.-:,
0 .. 000
0 ~ 59i.~
l. l.27
O .. :l8~'::i
0 .. 22''7
0.383
0 .. 46i::!
0Alt19
0 .. 521
0 A '.3~i8
13
Di Br·
Etharie
0 .. 000
0 .. 010
0 .. 000
0 .. OE?.~:.i
0 .. OC.~6
0,.0:32
0,, 0~30
0 .. 000
0" 0'+5
0 .. 000
0 .. 000
0 .. 054
0 .. 0'+2
O.llEI
0,, 1 '.:!4
0. 139
0,,301.
0 .. '.3L•3
14
C: 1 Ben,:
0 .. 020
0 .. 040
0 .. 030
0 .. ()l,t'J
0 .. Ot2:J
0 .. 06r..l
0 .. O(::,~i
0 .. 083
0 .. 039
o .. 1'+7
0 .. '.':!'',El
0" 06F3
0 .. 06'1
O .. l ltf.?.
0 .. 153
0 .. l Lt:-::1
o .. ;:?.12
0 A E?.2,..;.f
1
D,;1i.;e
1024 .. 8'+
0325 .. 8~:;
()lp) l .. 8~5
0 1"1f~'+ .. 8~:i
lE'.!05 .. 85
Olf~1 .. c.16
OE~E.\~.:i., D.!J
05:1.:3,,Dt..,
0716,, E36
0917 .. 86
l (~0~~ .. E1l:i
Of.~04 .. ff7
<X:118. El?
0~31'+ .. 8'7
1002.87
0120 .. 88
06E'.i~ .. 8B
102C:. GE3
,Julian
Day
1028
1 :lBO
11 B7
:l ::IL;::3
1 t+::~~3
1L1-8f.7.
l!:il'7
:l. ~)9lt
1651:3
:l '721
lEIOO
:l f.16 l
190cl
11..f60
2101
2f., :l 1
23,S~5 c:,.~a5
3 t.t
Di.rathyl. Di. Cl.
Et;t~1e·1-l"'IE•thar·re
3,. 550 0 .. :➔ l 0
'7 .. '750 0 .. :370
3 .. 080 0 .. 000
6 .. 34~3 l .. 02:3
2. 62E3 0 .. 166
6 .. 09'7 0 .. 048
'+ .. 609 1 0 .. :::12.5
:l. .. 0~18 0 .. 319
J.O .. EJ6B 0 .. '7'+0
:1.0 .. l,tltl 1 .. '+98
J. 1. .. 500 2 .. '.53E?.
l ., :~t:,f:, 0 .. lt30
'.3.12'7 0 .. 69S
5 .. 678 2 .. O~ir3
1 . 843 l ., 138
2. 46'-r 1 • '.31 ~i
5.1El''r 4.231
8 .. 63lt t+,. 396
C:h lerr·er .....
fc,r·m
0,, 000
20 .. '+~iO
E~2 .. C:iOO
12. 1 ::;t,
l .. C~l~l+
19. 3'.3B
l~i .. 98(~
U .. '723
l C\" 000
::'~?,, l G'·t
lOE!.'711
1 :3 .. (3?8
l+l-1-" L.~l:,CJ
:;39. 837
18 .. 959
20 .. 8'70
33.19'.3
'+ 1 "o::~3
•
6
CC: l '-1-
l .. 150
1 .. C:)90
2.390
:l.389
1 .926
l .51''7
1 • 9;5 l.
f~-~i0'7
/:'?. n ()()()
1 .. (>'.3:3
:1.0 .. C?E~l
l .. ~::i:3:l
l.,, :CIJ.E'
2 .. 9'7 :l
l "9L1-l.
l .. l S'3
l. .. 277
1 .. 0'-t7
7 B
IJE·ir1zc~ne T·1-i Cl
0 .. 000 O .. E!20
3 .. 960 0 .. 4:1.0
3 .. 770 0" 7~.50
2 .. 573 0 ., :3~:iE➔
C:'. .. l ~iO O .. '.:'.l70
~:3 .. 6:34 0. 472
'.].,058 (),.l1-6l
1 ., Lt :l O O • 286
l .. l~OO O .. '.:'!80
6.i'213:,l O."l:l:l
1. E! .. C)E.'.9 l "i:,26
E:~.8::.;7 O.t+:51
f.?. .. Of::l6 0 .. ;_~!86
7 .. E\75 :l • ()l+'.:~
t+.:l.ltf.3 (),,E}:l.~5
l► .. E!'•~3 0 .. 732
7 .. Li-69 l. .. 0'.3cl
l O .. <~->:38 l • 28'+
1
Date
1127.84
0806.85
1001.85
1212.85
0130.86
0306.86
0520.86
0522.86
0716.86
0910.86
1205.86
0128.87
0325.87
0618.87
1015.87
0120.88
0622.88
1013.88
Well 5
2
Juliari
Day
1314
1370
1442
1491
1601
1603
1658
1714
1800
1854
1910
1995
211'~
2211
241)5
2478
-File 8 •
9 10 11 12
TolLlene Tet Cl Eth Benz Xylene
Ethene
0.000
0.000
0.000
0.000
0.000
·0.000
0.000
0.000
OuOOO
0.000
0.000
0.0()0
0.002
0.004
0.0(>7
0.018
0.005
0.011
0.000
0.00()
0.0()0
0.004
0.003
0.006
0.006
0.000
0,,002
0.015
0.016
0.01't
0.013
0.025
0.017
0.034
0.000
0.022
0.000
0.000
0.00•)
0.000
o.oc,o
0.000
0.000
0.000
0.000
0.000
().000
0.002
0.002
0.001
0.005
0.002
0.000
0.000
0.000
0.001)
0.00()
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0()0
0.003
0.004
0.1)05
0.015
0.027
0.003
0.015
13
Xyler1e
0.000
0.000
(1.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
0.000
0.035
0.003
0.018
14
Di Cl
Be\·iz
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o"ooo
0.000
0.000
0.000
0.000
0.000
0.019
0.004
0.006
1
Date
1127.84
1)806.85
1001"85
1212.85
0130.86
0306.86
0520.86
0522.86
0716.86
0910.86
1205.86
0128.87
0325.87
0618.87
1015.8'7
0120.88
0622"88
1013.88
Well 5
2
Julian
Day
1314
1370
1442
1491
1601
1603
1658
1714
1800
1854
1910
1995
2114
2211
2405
2478
• File A
3 4
Diethyl Di Cl
Ether Metha)1e
0.000 0.000
0.000 0.000
0.000 0.0(>0
0.007 0"000
0.017 0.000
0.044 0.000
0.038 0.000
0.121 0.000
0"021 0.000
0.061 0.053
0.078 0.515
1)"028 0.038
0.085 0.113
0.047 0.042
0.046 0.067
0.094 0.101
0.072 0,,074
0.343 0.072
Chloro-
form
0.280
0.199
0.462
1.386
1.398
1.788
2.721
9.050
1.304
14.623
8.231
4.9l•3
8.727
5.415
3.841
5.351
4.6£~9
11.204
•
6
CC14
0.020
0.026
0.057
0.166
0.160
0.178
0.019
0.276
0.153
0.688
0.376
0.846
0.453
0.385
0.567
0.264
0.521
7 8
Ber12er1e Tri Cl
Ethe)1e
0.000 0.020
0.000 0.014
0.0()0 0.023
0.000 0.005
0.000 0.052
0.000 !).063
0.000 0.254
0.000 0.114
0.Ct00 0.l.9(1
1).000 0.058
0.000 0.058
0.000 0.051
0.000 0.063
0.116 0.059
0.165 0.063
0.01)0 0.785
0.021 0.020
• • Well 5B File B
1 2 9
Date Juliar1 Tet Cl
Day Ethene
0606.85 1253 0.000
0806.85 1314 0.000
1002.85 1370 0.006
1212.85 14lt2 0.009
0130.86 1491 0"007
0306n86 1526 0.008
0520,,86 1601 0,,008
0730.86 1672 0.115
0910.86 1714 0.010
1205.86 1800 0.039
()128.87 1854 0.004
0325.87 1910 0.006
0611.87 1988 0.008
0618.87 1995 0.008
0721.87 2028 0.008
1015.87 2114 0.000
0120,,88 2211 0.008
0622.88 2365 o.,)06
1013.88 2478 0.006
0210.89 2598 0.006
•
1,-JE,l. l. SB Fi le ?\
1 (7~ 3 Ii
Date Julian Diethyl Di Cl
D;::,y E:thF:i-ME•thC:1i"rE
0606.85 1253 0.045 0.000
0806.85 1314 0.000 0.000
1002.85 1370 0.055 0.000
1212.85 14'~2 0.089 0.000
0130.86 1491. 0.044 0,,000
0306.86 1526 0.066 0.000
0520.86 1601 0.149 0~000
0730.86 1672 0.060 0.000
0910.86 1714 0.026 0.000
1205.86 1800 0.114 0.000
0128.87 1854 0.008 0.000
0325 .. 87 1910 0.010 0.002
0611.87 1988 0.016 0,159
0618.87 1995 0.(111 0.000
0721.87 2028 0.008 0.,001
1015.87 2114 0.000 0.000
0120.88 2211 0.005 0.001
(1622~88 2365 0.006 0.010
1013,,88 2478 0.005 0.000
0210.89 2598 (>.000 1).000
Ch lerr·o-"
f'orm
0 .. 895
0 .. 000
0. ~il1-9
0. 7(7~.5
0.737
0. f..)t.t l
2. 3'•'7
0. r..;iiy(:3
0.69\S
2 ",:y99
0.249
() n 3(31
0 .. 595
0. :~1•::?2
(),,1.'.J,70
0 "3~31
0. 46'-f
0.517
0 .. '.36~!
O.f311·
•
6 7 B
CC14 Tri Cl Tri Cl
Ethc:i .. rr~ Eth1::-,nc·
0.115 0,,(130 0.000
().000 1).000 0.000
0.1'75 0 .. 022 0.000
0.326 0 .. 024 0.000
(l,,228 0.022 0.000
0.205 0 .. 019 0.,000
0.988 0.041 0.000
0.605 0 .. 034 0.000
0.082 0.020 0.000
1.775 0 .. 815 0.00()
0 .. ].20 0 .. 009 0.00(1
0.247 0.011 0.000
0.309 0 .. 018 0.000
0.31'.:l 0.01'7 0.000
0.363 0 .. 017 0.000
0.217 0.012 0 .. 000
0,,301 0.015 0 .. 0()1
0.263 0.015 0.015
0.357 0.011 0.001
0.542 0 .. 020 0.000
• WF.,l. J. 5A Fi. le C
l 2
Di~i t F:.• ,J1.J l i ii:i n
DE1y
0606.85 1253
0730. 8'.5 1307
l.018.1:15 1387
0522.86 1603
09 l. 0 .. l:16 17 l ,.,.
0:32~:S. 87 :t t:J 1 o
06lB .. B7 l.995
lOl~i.87 21 llf
01E'.O .. f~JB E:C:!1 l
062(::~ .. f3fJ 1.?.36~')
l.OJ.3.f.clfl i~L1713
0210.89 259El
Xy l E,n,a
0 .. 000
0.000
0 .. 000
0.000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 001
0 .. 003
0 .. 000
0 .. 000
•
:I.
Date
0606 .. 85
1)730. 8~j
l O :I. El" £1~5
05E~2 .. f:~6
091.0 .. 86
061.8.i:17
101'.5 .. f.l?
01.PO .. l-38
0622. f.lEl
lOt ::I .. EJ8
Of-~l0 .. 89
;_:~
,Jul i.i::i.n
Day
125'.:I
1:307
1 :3f::)'7
160:3
l.71.L+
:l C/10
j_ 9r::,'.;5
i~'.:l.ll-t
C!.f.:'.~ l l
247!:I
E!598
9 10 11
Toluerie Tet Cl Di Br·
EthE•1·1E.• EthDr11::::
0.000 0 .. 000 0.000
0.000 0 .. 003 0.000
0.000 6.500 0.0()0
0.000 O.(>OO 0.000
0.000 0.000 0 .. 000
0.000
0 .. 002
() n 00'.3
0 ,, 00'+
0 .. 007
o .. oo~;
0.000
0 .. 002
0 .. 009
0 .. O:l 1
0" 01 :I.
0,, 01t:~
O.Ol.2
0 .. 013
0.000
0.001
0 .. 003
0 .. 003
0,.002
0 .. 000
0 .. 000
12 1:J
Cl E<,:,1·,c, E:th Be:mz
0 .. 000
0 .. 000
0 .. 000
() .. 000
0 .. 000
0 .. 000
0 .. 002
0 .. 0 1)3
o .. oo;~J
0 .. 003
0 .. 000
0 .. 000
0 .. 000
0.000
0 .. 000
0.000
0.000
0.000
0 .. 000
0 .. 000
o .. oo;J
0 .. 000
0 .. 000
.0 .. 000
:[Lf
X y 1 E·: n<-t:
0,.000
0.000
0 .. 000
0.,000
0 .. 000
0. Oi)O
0.000
0.000
0,, ()0 l
0 .. 002
0,,000
0 .. 0()0
1 2 3 4
Date Julian Diethyl Di Cl
Day Ether Methane
i);!11)r~1 ., B~i 12~.13 0 .. 130 0. 000
0'730"85 1307 0.095 0.000
1018n85 1387 n .. PP5 0.000
()522.86 1603 0 .. 234 0.000
0910.86 1714 0.132 0.0()0
()325.87 1910 0.057 0.021
0618"87 1995 0.051 0.005
1015.87 2114 0.030 0.035
0120.88 2211 0.029 0.026
0622.88 2365 0.057 0.125
1013.88 2478 0 .. 060 0.034
0210.89 2598 0.000 O.i)Ol)
Ch loco-·
fc,·1-m
'7. ,.,.1, 0
3 .. 270
5. 7'r~6
31.618
U .. 216
c!.Ul :l
3.376
Lt ,.()98
3 .. E?.EJO
::i. 325
t+ "7CJ(i'
? .. 39:t
6
CCJA
0 .. 070
0 .. 09~i
0.23Lt
0 .. 6L~9
O .. Oti'7
0 .. :l't'-?
0.'·tO:I.
0 .. 31 ,.,.
0. 631.1
0 .. 000
'7 El
Flt7~n=•~E:rH-:0 Tei Cl
E t.:h0?-·1··1t:?
0,, 03~i O. l.~'.3(2
0 .. 007 0 .. f2!::.'iEl
0 .. 000 0. t.+09
0 .. 000 (J. ~":i99
() • ()(l() (l n '.'.;1~)7
()" 000 0 .. :!. f.?.O
0" 000 0 .. E.'.!86
0 .. 010 O .. /.'."l9,:1
0 ., 000 0. E!f:!.6
0" 0:'.5 :l O. :~C~(=>
0.07'.] O .. i.:!16
1,.()lt3 0.,:312
1
Date
1130.84
0722.85
0522.86
0909.86
1111.86
0128.87
0325.87
0618.87
1120.87
0309.88
0712.88
0719.88
1101.88
0407.89
Well #3
Julian
Day
1065
1299
1603
1713
1776
1854
1910
1995
21.50
2260
2385
2392
2497
2654
9
Toluene
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
0.000
0.002
0.003
0.003
0.000
10
Tet Cl
Ethene
0.000
O.OIJO
0.000
0.002
0.000
0.003
0.003
0.007
0.007
0.006
0.()08
0.010
0.012
1
Date
11 cJ(l .. El'+
0722. B~i
()~)22 n f:36
090'?. 1::16
11 l. l. .86
0128.87
0::-125. El?
0618. ff/
1 l.,~0 .. 8'/
031)9. f313
0712 .. 88
0'719.88
l l. 0 l. • f3E!
0'1-0'7. 89
l,le 11 413
2
J"ulian
DE1y
106~)
1299
l t,o:;3
1 71'.3
l.'7'76
HJ~;Lf
1910
1995
C21 ~50
1?.2CJ0
238t5
f.:!392
2'+9'7
E!6~ilt
3 4
Di.ethyl Di. Cl.
E:'.threr M,ethc\ne
OnOOO 0 .. 001)
0.004 OnOOO
OnOOO OnOOO
On008 OnOOO
0.012 0 .. 000
0.009 0,,000
0 .. 005 0 .. 000
0 .. 026 0 .. ()0ft
0.026 O .. OlO
0 .. 015 0.022
0,,27~i OnOLi-2
0. 162 0" O~if.~
0. f.?.~l'J O. O~i4
0. 583 0. 08f.)
~ d
Ch 101-0-
1~ c, r· ffr
0,, O~!O
() .. C~5t.,
0,.2t,O
1 .. 22E:
3 .. 012
1 .. ::=:i62
:l.nL~f+l~
P "8::10
l..930
2.l'?'-7
8 .. Ot+O
3.0l.El
10.262
(_.
6
CC:1.4
0 .. 000
0 .. 052
0 .. 035
0.038
(),. 1.LJ,(l
0,,083
0.0'??
0 n 1 '72
0" l. '.~'•
0"077
0 .. 1. :t t+
0 .. 1 :l?
o .. 1.6?
o .. :1.50
'7 8
BE~n:-~er1E•:! Tr·j, Cl
EthE!"i .. lE~
0 .. 030 0.000
0 .. 000 0"009
0 .. 000 O .. Ot.'-J-0
0 .. 000 0" 0~:.:.>.9
0 .. 000 0 .. 0~57
0 "000 0" (){.t '7
0"000 OnOr.·•9
0" 1.)00 0" i.:!i.~~8
o,, o:~,r.~ o .. 090
0,.010 o .. :1.01::i
0 .. 1. 6t:l O .. J. tJ6
0 .. 163 0 .. :1.'79
O .. E!lO O .. r'::!67
() .. E'.i.::!13 On2:I.E:l
• Well #1.P, Fi.lee l}
1 2 21 22 23
Date Julian Tri Me Eth Me Tri Me
DEiy Bc:nz Df.?l"1Z Bc-:c1:2.
0606a85 1253 O.QQQ O.QQQ O.QQQ
0730.85 1307 0.1)01) 0.000 0.000
0523u86 16!)4 0.000 OuOOO 0.000
0916.86 1'720 0.000 0.000 0.000
0204»87 1861 o.c,oo 0.000 0.000
0401.87 1917 0.000 O.OOc) 0.000
0709.87 2016 0.000 0.000 OuOOO
1015.87 2114 0.000 0.023 0.0'►8
0120.88 221J 0.015 0.017 0.045
0622.88 2365 0.014 0.016 0.043
0719.88 2392 0.000 OuOOO 0.031
1013.88 2478 0.000 0.000 0.000
0210.s9 2s9s 0.000 0.000 0 .. 000
•
D,. Cl Tc i. Mee
Ber1z BE!Ctz
0.000 0.000
0. 000 0 .. 0()0
0 ■ ()(H) 0 .. (l(l()
0.000 0 .. 000
0.000 0 .. 000
0.000 0,,000
0.000 0 .. 000
O. 000 0 .. OC.!7
O .. 020 0,. Of.~'.::!
0.01'·7 0 .. 021
0 .. 000 0 .. 000
0 .. 000 0 .. 000
0. 000 0. 00()
0606 .. 85
0'730 .. n::i
O~iE~3 .. f:16
0916"8(")
020l~,. 8'7
0',01 .. 8'7
0709 .. 87
10l5flf.:17
0120.~38
06P2.88
0719 .. EJEl
tO:l:3 .. 8I3
Ot.:::I.O .. f:39
•
Fi.le C
2 l ~3
.Julian Di BfM
D<::1'y' EthE1nf:::
lE?.'.::i'.'.:i 7 .. 61.0
1 :::.107 't .. 't::17
1.60'+ 2 .. 303
1 ''?20 2.101
1 ell, l O. 8''i>'7
1917 l..380
2016 l. l.Ell
21 :I.,, :I. • 030
2:,! ll O .. 7'+'r
2:36~:3 0. 670
E~~J9E?. 0 .. ltf+!:i
f,?.Lt'78 0. 363
E~~59El O. Oi:!8
liS .l 7
C:l E<c;;r,z Eth De,nz
0 .. 000
0 .. 122
0"0'79
0 .. 1 7/.:.)
On 1.06
0 .. 1.0B
0 .. 210
(l.,;397
0 .. 2'.31
o .. 18:':i
0. :l ?'.3
0. 19 l
LEJlc!
1 • 07Z1
0 .. 9L~l~
1., 178
o .. 5:1_;:)
0 .. 56:l
O .. B3'·1·
l "0'-tf:!
0 .. 79~1
0.736
0 n ~:-:i5()
0" ~i72
(l,. lt92
•
U3
XylE:nf.0
4. :,so
r.: .. 52~/
2 .. '1·1B
2 .. 9::;c.,
l "E'!.7f:3
1 .. c!'i'El
J .. 9~;9
2. Li-:l 9
1 .. 999
1 . 783
1 • ::1s::1
:I.. 43'.3
l .. 2'7'.:,
:l 9 f~O
Xy 1 ens, Eth Mc2
Ber1l".
2 .. 290 0,.000
l .. :3'.'.:iB O. 000
l. .. Oli-8 0 .. 000
1 " J /+(.'.?. 0 .. 000
0 .. 673 0 .. 000
0,. 7'-? :t O. 000
J .. oc:) 1. o .. ooo
l .. 361 O~OLt?
1." JOB O" 03l,
1 n (}()'7 (J ~ ()'.3'7
(l n 'Jf)() 0" (J()()
0 .. 8:t6 OnOOO
0 .. 766 0 .. 000
:l
Dod;e
0730.85
O~iE!~~~ .. Fl6
0916 .. 8t-.J
OPOt.+,, B'?
()f,t() :t .. 87
0709 .. 07
l.Ol5 .. El7
0120 .. EIB
0622 .. 88
0719 .. f.18
1013.08
OE.!l.O .. 09
,,Jell #1A
Julit::\n
D;oy
lE!'.7:i3
130'7
l t·)Ol+
17E~O
l Ei6 l
19:l7
£:~O l 6:)
c:~ 1 1 I.'.~
2;:::!l l
2:::~(-:,5
C.?.~:192
2'-t 7f3
E!5-:-1f:l
•
9
Di Cl
Prc,pant?
l?.9'70
8" , .. :~12
6 .. '+'.]6
Lt• t:)li,''71
1. 76::!
3 .. 39:3
2 .. 82'+
2n21CJ
2 n f.':!3()
2 .. 52~3
2 .. OOf::!
2 .. 30Et
:I. "5t+B
10 11
E<c C:12 CHcl
Methane Pentanone
0 .. 00(1
0 .. 06E~
0 .. 000
0 .. 000
0 .. 000
0 .. ~l06
0,.2]c:I
0 .. 3(10
0. 31.EI
0 .. 3:l'i'
0 .. F.:~70
0 .. '.39'.3
(I .. '.:;136
2 .. 9BO
0 .. 266
U .. 1:102
0 .. 802
0 .. f~75
()" lt8:~{
0 ~ £+30
0. 135
O,,P70
0.87:l
O .. Ei'+2
l • U:3(i
0 .. 996
•
:t C!
Toluene
6 .. "?E!O
3. 2~~0
3. '-flf6
3.61B
l • EIOO
Lt. f.ti+t+
::.~. 60(2
3.9[!tjl
'+ • 7fl6
3. El'-76
/.7 n '7(}''7
lt" 2tl0
:l 3
Tri. Cl
Etha·ne
2 n (Jl.f()
1. 037
0 .. 4L~:3
0" 3E~9
(),. 1.L~l~
0,. f..?.~~j()
0 .. l~~l
0.1E:t,
o .. o:=;B
0" 0~:!lt
, 0 .. 000
0.000
0 .. 000
:l'+
Tet Cl
Et he·n1.-2
0~000
0. ()29
() n O::.:J~j
o q o~:;1
0~029
,~},.n3'":i
0 ~ 06E.'.
0 .. 077
0" ()'}'/..~
0 .. 06(""J
OnOt.1.'7
0 .. 000
OnOOO
1
Date
0606.85
0730.85
0523n86
0916.86
0204.87
0401.87
0709.87
1015.87
0120.88
0622.88
0719.88
1013.88
0210.89
Well #1A
2
Julian
Day
1253
1307
1604
1720
1861
1917
2016
2114
2211
2365
2392
2'~78
2598
• File A
3 4
Diethyl Di Cl
Ether· Metha)1e
68n94Q 68.940
35.260 0.000
54.042 26.24·0
2l►.4O9 1.£►04
5.640 0.992
10.106 1.971
9.735 3.031
4.608 2.5't1
3.677 2.360
4.623 2.896
4.550 0.8,~7
6.110 4.809
5.209 4.112
Chloro-
81.850
3.937
73.212
27.389
50.896
33.214
37.125
34.827
33.102
26.312
40.939
30.929
•
6
CC14
0.600
0.717
1.914
0.324
2.097
3.759
2.586
2.668
2.802
2.476
2.092
3.682
2.946
7 8
Berizer1e Tri Cl
Ethene
l(l.420 2.671
14.056 2.054
7.308 1.075
15.725 1.582
15.076 1.295
22.831 1.282
16.908 0.807
22.877 0.653
19.704 0.476
24.966 0.525
20.9()0 0.416
1
Date
0606.85
0730.85
1214.85
0121.86
0205.86
0513.86
0730.86
0916.86
1120.86
0204.87
0401.87
0709.87
0721.87
1015.87
0120.88
0622.88
1013.88
0210.89
Well #18
~ C
Julian
Day
1253
1307
1444
1482
1497
1594
1672
1720
1785
1861
1917
2016
2028
2114
2211
2365
2478
2598
• File D
21
Di Cl
Benz
0.000
0.000
0.000
0,,000
0.000
0.000
0"000
0.0()0
0.000
0.000
0.000
0.000
0.000
0.000
0.007
0.019
0.000 o.oo,)
22
T~i Me
Benz
o.ocio
0.000
0.000
0.000
0.000
0.000
0.000
0.001)
0.000
0.000
().000
0.000
0.00()
0.000
0,,005
0.011
0.000
0.000
•
1
Dc:1. tr::
0606.cJS
07'.:.~o n 8~:i
121'>.8~i
01E:l .S6
0205nEl6
o~:i :l 3. 8<:)
0'730.86
()'116.86
1 lE!0.86
Oi.:~OL1-. 87
0401.G?
0'7<YI. l:.l'7
071:! l. 8'7
101:5.87
01.E.~(l,, Ba
062F~ .. 88
l.Ol::J.BEI
0210.8CJ
J·u.J.ian
D2.y
l F.~:'::iZ➔
1::10'7
l ltt+4
:tt+82
l '+97
1'.'.':i94
'J.67(:
1720
178\:i
lfl61
1917
2016
202B
2 l 1 .::+
2,? l 1
2365
E!'+'7f3
• Fi le C
15 16
C 1 Benz Eth BPn-::~
0.000
0.0:30
0 .. 035
0.000
0., O:'.i5
0.000
0 .. 000
0 .. 0/::,2
0 .. 000
0 .. 000
0 .. O~:JO
0.038
0.043
0 .. O'-t't
0.041
0 .. 024
0.000
().,()ll1-
O. l '/3
0 .. 131
o .. 107
0. 1'>7
O .. ll+l+
(l "4Lt()
0 .. 06tJ
0.179
O .. OB5
0 .. 06.f:-J
0 .. 082
0 .. 081.
0. (::,C/9
0.08'.3
0.083
(} n ()i+6
0 .. O'+B
0 .. Oi::"?3
17
Xyleme
0 .. 603
0. 4:31+
0" 1+84·
0 .. '+0:3
0., l~()3
0 .. 369
() n ft72
0. l,35
(l,, f+ll-5
0 .. c~or.;;
O .. E!39
0 .. 281
0.337
O .. ft92
0 .. E'.92
o .. 195
0,. (.~ll-5
0. l '77
•
:I. tl
XyJF.,n<?
0 .. E!El2
o .. 1.90
o .. 161
0,, :lt.1-B
0. 169
0.21'+
0 .. tt.1-2
O .. E?.13
0. lOO
0 .. 09B
o .. 108
0" l l ,,
0" l (llt
0" 1.0:1.
0" 0[-:,'7
0 .. 078
l Ci
Eth Me
Df:.?fiZ
0,,000
(l,.()(i()
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0" 00()
0 .. 000
0 .. 000
0 .. 000
0,,000
0 .. 000
0 "000
0 .. 000
0" 011
0"000
0 .. 000
0 .. 000
20
Tt·i Mc:~
Etf.::n;•~
0"000
opooo
0 .. 000
0 .. 000
0,,000
0~000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
o .. 000
0.000
0 .. 000
0 .. 000
0 .. ()10
0"000
0,,000
0 .. 000
1
Dt::t t ~:•:t
0606 .. 8'.'.:"j
0730.85
li.:!lt.i .. 8~:i
0121.86
0(.~0~1 II f:31'::i
0~51:3.86
0'7'.:10 .. 86
0916.86
l li.cO. 86
OE!OLt. f37
OL,O l. .. 8'7
0'709.8'/
07E!l. 87
101~:5.87
01E(0 .. 88
O,:':,E!E~. !:3f3
lOl. 3. f.!8
0/:~lO .. fJ9
Well ttl.B
Jul i.Etr"1
Dc1y
l i:?.t::i3
130'7
l l..t t+ t.t
148(.7~
Jl.+97
:t '.591..t
1672
1720
l 7B'.5
:lB6:!.
19 l '7
i~Olt,
20E~8
211 lt
2211
E-2:36~~;
247B
•
Fi.le B
9
Di CJ.
F'i-opane
~'3" 6CJ~)
1 .063
0 .. l+l'7
1. 281
l .. 0:1.'7
1.43B
0 .. ?'79
o. 7~JO
l. .. 01+3
0.379
0 .. t.+70
0.420
0. '+4'.,l
0. 183
0. 34-4
O .. P33
0 .. 3f.~3
() .. (H)()
10
C:H,J
F'entanoc1e
0 .. 000
0. 21+8
0 .. 000
OmOOO
0 .. l 3~.~;
0 .. 000
(l,.000
0 .. 000
0 .. 000
0 .. 000
() ~ (ll-i,t:)
0.033
0 .. Ot+1
0.000
0 .. 016
0 .. 0'...18
0 .. 067
0 .. 000
11
2" 70:::.)
1 n 158
0" 61 l
0.833
0 .. '.:i~J7
0 .. 6:llt
0 .. 3:1. '?
0 .. 388
0,, 2~:il+
0. 132
0" :-3'?'7
0.1'-71
O .. i:~09
0.085
0" :I. J. I.,
O .. OB~i
o .. 0'71.
0 .. 02Lt
•
12
Tr• i. C:J.
Etha.nE?
(),, ~:lO~i
0. 115
0.000
0. 1 :I.'+
0.030
0.,000
0.048
0,,000
0.000
0 .. 04~:i
0. 0'.35
On030
OMOlO
0 .. OC.'.!l
O.Olt:)
O. l.'-1-9
0. 1 lt2
13
Ted; C: J.
Ethene
o .. 100
0. 11 B
o .. l.76
0. 171
O .. E.!~39
0.,:30;,?.
o .. 19 l
0 .. 263
0" l. 1. '7
0 .. 136
0 .. 098
0. 136
0 .. 231+
0 M ;:=:t~9
0 n l8(l
0.1C~1
0 .. 000
0 .. 000
1 t.1-
D 1 E<1-
Ethi=1ne
0 .. 9E'.O
i.) • :3 f~8
() .. E!OC/
0 .. 3l18
0., }~~"7Li,
0 .. 000
0. 183
0 .. 000
0. 08::i
0 .. 07'.:)
0 M 0130
0 .. OClE➔
0. Olt9
0,,06f.'?.
0~033
0 .. 000
0 .. 000
l
Dat:E-:
06(16 .. 05
0730 .8!:::i
12lLt.,f:l::i
O:lf.~1 .. f.36
0205.F36
O~.~-; 13" 136
07::10. 06
0916.06
l 1E10 .. f:1f:.)
020lt "87
Ot+O l .. El'?
0709 .8'7
072.1. .. Wl
1015.87
Olf.:'~O .. l-38
0(::l,:~E.! .. Ell:3
l. Ol. 3. 00
c1i:::10 .. ai:-;
C> , ..
J'1..1.l i~in
1307
l l+l+t+
l Ltf.:lf..'.:
1'+97
l :=.:_,;91.+
1672
l ?i.?.O
l 70'.:;
l Bl, 1
l ''117
2016
20E.?.B
(~:lllt
2r:. t l
2'+ 70
i.:~1591:3
• Fi 1E: A
3
Di.c,,thyl
7 .. 06~:'.j
3. 6~!:3
l .090
4. 5~:5lt
2. 92::1
~5 .. 110
3 .. 599
2,. l,t87
l1, .. 09E1
1 .. '+57
1. ., l'.'.!i..~l+
1.61'15
l "627
1.13~2;
0 .. '?99
l ., 1 :':i:':.'.I
l. .. 93/➔
1 "69<:i
4
Di. Cl
l"'lr:!thc,·11e.
0 .. 000
0.000
O .. F.~19
0 .. 000
0 .. 03'.l
0 .. 622
0 ":~i9lt
0 .. :s~":i2
0 .. 63f'!.
0 .. ~59fJ
0 "f..'12Lt
l .. 6,b9
0 .. 495
0 .. t+El2
1 .. 129
l • E~LtO
0" ?(SEl
Chlorc,•M•
t"errm
;.:.:_!() .. 9~i0
9 .. 19f!.
11 .. .::,.,.~a
l [~ .. E!:::l2
f.:!:'I. :307
l d. l OC/
l'.'i .. '.o<lf:3
l l1," 9Lt9
'7 .. 50~.:i
11., .• J.J."I
6 .. 533
10 .. 'JE:'.l
9.493
7 .. 6E''.J
~~j" Lttf8
l. l. ::365
l i.:: • 7 i.7~ Ei
•
6
C:CJ.L+
0 .. 000
0.51l+
l "::11.+;.~
0" 9E~9
l .. 473
l.. l. 61'1
0 .. 6l+9
l. .. 199
1. .. r.:.!9 l
0 .. '7(.}.8
1. "39'.::i
l .223
0.'1-4?
0 .. 970
1 . l ~39
7 El
Dt-::1n2E-:~n£-:: Tc i C: 1
EthE•ne
'7 .. ElLi-0
2. 59'+
l "~:57a
E~ .. 679
2 .. 726
3. f3l+L+
l "7l~i-t
F:!. .. ~:'.it.1 t
l .. 943
i?. .. 6Cle
2 .. C~20
1 .. 8~:i.:S
C?. n 791..1.
0 .. 770
()" '.3L~~:i
0 .. '.:163
0. 41 "?
(l.,Lt-70
O .. '?]:t
o .. 1..~70
0 .. :;).t+~ii
0 .. 295
0" f+]'/
0. t+O~:"i
0,. 3;7~!0
0 • r.~0'.3
O .. E!9i:-i
0" ::.~?:::~
1
Da t f:?
0'.313 .. BS
o::32~::i .. B~:i
Ol.tOl .. 85
0'730 .. 8~:i
120'·t ., 8~:i
OlE~C~ .. 86
0225 .. Bt-:i
051. ~~,. 8l.1
O~.:.t 16 .. {-3,:J
0716.86
l 1.C~O. 86
01.~0t+" 87
0401.. 87
o?o•::,t M ~3?
1015.87
Otf=0.8B
0622 .. BE)
Julian
Day
1028
.1. l ~:iC~
1168
11.BO
118?
J.30?
l'+'.3'+
l '+83
1 :~ 17
:1.594
:I. ~.59~5
1.65El
:I. '/E!O
1785
:I. fJli :l
191. '7
(;~() 16
C'.lll~
i:-~C! 11
E?.::165
•
:1.5 :l?
Cl Benz Eth Benz Xylerie
0. 160
0 .. E~60
() n 3f:.)0
0 .. 200
0 .. 2'+0
0 .. 26'/
0 .. 5~:3c_:,
()., l~()7
0 .. 000
0 .. 000
0 .. (:)31:3
0 .. 2l+'7
0 .. ~~i9~i
0 . .'+67
0 .. 30:=;
0 .. :-U.2
0 .. ::i :l Li-
C.:! .. r...'!a3
0 .. 571
0 .. 576
l "700
J. • fJOO
'.:l .. c,~30
2 .. aoo
2 .. 000
:3 .. E~Ol
2 .. 702
'.:l .. l O~::;
0.742
~] "~.)Pf::1
1. n 606
3 .. 036
1 • 3::39
l . t+fl'J
l .. '?09
'..:i. 1.13
:l.7~:i:l
l. 771
l~" ;~30
5 .. i:~50
1.0,, 200
6. ::100
7 .. 000
4.600
!3 .. 4-1.'.:!~:i
6 .. l.20
6 .. f30'.7.i
2.062
7,. 91.+'-Y'
3.0B8
6 .. 31~1
7.90?
:3. 100
3 .. 6~:'i6
t,t ~ 1E'.?
3 .. 061+
Lt .. 16~5
t+ .. lC:iB
•
1 El
Xy l enf:?
t': .. 320
2. ,mo
:➔• 260
0 .. 000
;:_;., l'-tO
2 .. E~58
3. ~:.'.i0•:1
1 .. 591
'.'.':i ~ OEJ 1
l. • 9bl1
:::1 u 1 ''/9
::➔ .. 6'74
t . '/6:)0
2.1.l.O
E.!. ltt+l►
O .. H!'.:I
Ft
Br~ B~~:•n-:.'.
(l., 3'70
0.350
0 .. Lt05
0 .. 840
0 .. ::l70
0.245
0 .. l'?C-~
0 .. 262
O .. E'.E\9
0 .. 000
0 .. 000
0 .. 000
(l,,000
0 .. lE?.~_:i
O .. lL1f.!
0" 167
0 .. l El:,
0 .. 1(:>lt
0 .. l76
l
[),,,t,:,,
0~::11. :::J,. G'.:i
0325.85
0'+0 l .. B~i
07'.~JO .. El~~!
1204-,, 8~3
0122.86
02!72~j" 86
O~:i1'.::l.B6
O~'il. 6 .. B6
071(-,. 8(::i
()<;, 16 "E16
11E~O .. Bf.:)
0204.87
0'+0 :t .. 87
()'}()'} n f:J'/
101~5 .. 87
0120"88
06(.?2 .. BG
We J. J. tr l
r..:
Ju 1 :i. E1rl
Day
102C.~
l 1 ~.:ii.:?.
J. l 6El
:1.180
118"7
:!.]07
l. t+ '.JI+
1 '+B3
l.517
l ~5'-tL+
1.595
16:iB
1.71.:?.0
l.f36 l.
:l '"i 17
E.:1.016
E-?.11 ft
221.l.
[~.'.3(7,~:j
9
Di CJ.
F'r·eipc,i·,r2
C:1.0 .. 700
l lJ .• 7()0
ElE! .. 200
0 .. 000
l+O .. 900
Pl.600
l 7 .. l1,'79
27.83B
C~'.6,. :-:187
3.677
'..10.lle4
21. 6~1f3
l 'i,. ~:'.i9f.?.
E'.8. B~J?
'7 .. '71.'7
l E'. .. 390
:I.;::!" 1. 1.~9
7 .. 590
7.270
10 .. 0tllt
10
·ro l UE'.'riE:
:::1 .. 61.+0
6 .. 3(':J()
J.L+" f:.l()(l
10 .. 730
7 .. '.::lOO
~::in '-/00
7. 31+'..l
7.329
'"1 .. C~'?~:i
E.! H i:.?. l ,.:_;,
l cl. 6'7f3
7. 8['lc'i
l O .. ;;J?f::)
:I 1 • 498
4.71'.:.15
1_7 .. 021
7 .. C:!76
10.372
7. '+131.
•
11 :t fl
Tr·i. Cl Di Cl
EthanE": F'r·opane
6 .. ~i30 O .. LtOO
7 .. :3PO O .. ltP()
:I. '7 .. 1. 00 l .. P~lO
9 .. 730 0 .. 610
'7., 000 0., 500
~::i. ~:iOO O "t.~'.:30
::; "8E'~O Ou t+OO
5 u F.:~c; 1 0. 000
6 .. :1.00 o .. ~:i68
O .. B:!.'7 0 .. 000
6 .. 661 0 .. 000
3i:.=~" 597 0" 000
:::J .. 06~3 0 .. :::iOO
3. 4(3~3 0 ~ 000
l .. 30'.3 0 .. 000
2 .. 097 0" C.~09
l .. t+~':19 O .. J. ~-=;a
:L .. 09(.:! 0 .. 14~::,
0.963 0.117
0" (307 0 ~ :l. 3(.:'~
l:3
TF:t Cl.
Ether·1E•
0 .. 000
0 .. 000
0,,000
Ou050
0., (ll+O
0 ., O'.~.~(l
0 .. 000
0. 10B
0. l '79
0,,000
0 .. 206
(l. 1'-18
0 .. :I. '.::l~.:i
(),. 000
0. 0'7~:l
0 .. 072
0. l Ofl
o .. :tt+f?.
O .. lt+lt
0,, 10(:,
l l+
Di. E<c
Ethd"r"1e
S.860
:l l .. 000
1 1 • l '.50
14 .. ElOO
13" 6'.:ll.
1.0 .. 0'+9
12 .. 660
P .. 6EiEl
l 6 .. 921
{::)" :l 5'.:."S
B .. '.:.=_;~_'."i l
'?" 1.,:,17
3.?l.3
3 .. :=:i9l
lJ . ., 66fJ
L~ "006
~:3 .. EJ'.:i5
1
Dat,0
l Of.7~l1." Ell.+
022::~ .. 8~3
0::11. :] -(~~5
03;.::!:i .. a~:;
OL+O l .. 8!.:i
0730 .. 8'.:i
1 c.:.'. o t+ .. u~:_;
01E~f~ .. 86
0225 .. 86
05 l 3 -Bf:)
O~-~ 16" Elti
0716.86
<Y,1.6 .. 86
l lE:~O .. 1:36
OE'.Ot+ .. 87
0401 .. 8'7
070,,, .. ff/
10:lc:, .. ffl
Olf.'.:O" BB
06C~2 .. 8El
•
l·k:11 #1
2 3
,Juli.an Di.ethyl
D:xy E:t:hc,;·
1 02£1 0 .. 000
:l 152 40 .. 100
1 lfJEl O .. 000
11r10 o .. ooo
118'7 80.000
1307 78 .. '+00
li.~3lt 91.~ .. 01.~l
1'-~83 146 .. 1~::i:3
l 5 l '7 1 E.?.O .. 83E:
l:':i9t.~ 9 .. 00:1.
1 :':i9'.:_:J 377" 6BB
1658 99.884
1720 122 .. 030
l '7fl~ii 136 .. 6f3i.~
1 Ei6 l E~ l "8B2
l'?l? 37.861
E.!O l 6 t+ 7 .. ~::i:::l 1
21 l'• :l6.21l,
2211 15 .. 446
C?3f.:.,~5 19. r;o5
Di. Cl
l"'lr::-:-t:h1::1l'"rEf
0 .. :-120
1 .. 200
0 .. 810
l .. '.JOO
0 .. 000
0" (?96
o .. 108
() a F.'~69
0" '·79f3
3 .. '.:;r::;,t+
L+ • 1 9'7
t.+ .. 1.76
·7 .. :3;.:.:a
2 ~ E(9:..i
t+ .. 8'72
'7 .. lB:':.'i
I+ .. ~::i~.53
l~,. '732
6.fl37
~ ,.,
Ch lc,i-c,-
·fc,·, .. m
0,,000
113 .. 000
;7_:_)97 .. 000
1.) -000
201.000
89.000
19~3 .. E.~~:i7
:l fl 1 • 079
l96n 1.5E~
6\:;. 31.L+
'+'-t-6" E56L~
l?fl.274
26 l .. 031
fl8. 7,2::1
125.669
116 .. ,?c;::3
a~::i. 9'.36
'T?. '743
1°1:s .. :l 06
•
6
CC14
0 n lt70
l.250
l .. 640
i.=~ .. 700
1 .. 000
1 n 200
3 .. 6!:il
f.?.. 8 :l ::.~
=➔.610
1. ~i0'.:3
2'.:.L ::;197
2.917
l .. E!OLt
5.059
6 .. ::_;97
3 .. 77'7
3.612
3 n J ~:.; :I
7
Elt·~nzE~nt~
::1.010
7 ~ i~OO
:,16. 700
::le:J .. 000
1.3.500
:l.ft .. 800
l l~ ,, (~!'70
c~2.1~:,1
21;. d 687
'.~) ,, L.;-9 ~-'.~
1.El,. CJEJc.:.\
26. 9'+8
31 .. :Cl7EI
Lt;:~" 2'.5L-1
l '+ .. 7El7
PB .. 61l;
3~:i,. lt~'=i".7
2E?. n 35]
:":3(.7~ n '.3 :J. CJ
8
T.-i. CJ
Ethr::r1<::!
::l H l E'.O
6.'.390
l :.:l .. 000
i..=:'.t-t .. 000
7. 1-,.00
9,, 7::.1~5
£1. :t D2
8 .. 599
E!'7 .. (>JE~
7 .. 00:3
t.1 n (-:,5~i
\::1. ~::_; :l ·=;,
4 .. 1.53
tr • 90't
Li-" f.:)09
'.3. 903
3,, 05f.J
c.:~ .. ['.) f.1 0
We l. l. ti l 2
1 2
D~~\tE: Jul 1.E.in
D1;.1y
0:l.(.:'.4,,£4:::-.i l 120
03E!~5 "(-3~:i t 1 EiO
0703.85 1280
1212 .. 85 j_t.~lt-f!.
1 E:! 1 l• h [3~::i 11.+LJ.I.+
() :t::lO. 86 1 '+91
030t+" E1<::i l ~SE!t+
O~:ii.'.:O. 86 160 l
07::l0.86 1672
09 :I. '7. f36 1 '7P l
11 E!O .. 86 l '785
03113. 87 1 903
Oei l 4· .. G7 l 9/.710
070,;:, . 87 201 (s
0806.87 2044
Qt,tC?O. ElB i.'.~'.'.:lOE!
0806 .. 8fJ (".:4 l 0
l OE?.O .. 88 C~L+t)5
1 C'.07. fJE~ E~~~i~l~:J
0511.89 2688
•
15 16 17
Xylene Xylene Eth Me
0.000 0.000 0 .. 000
0 .. 000 0.000 0.000
0.000 0.000 0 .. 000
0.000 0 .. 000 0.000
0 .. 000 0.00() 0.000
0.000 0.000 0.000
0.0()0 0 .. 000 0,,000
0 .. 000 0.000 0.000
0.000 0.000 0 .. 000
0 .. 000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0,.000 0.00()
0.001 Q,.001 0.000
0 .. 001 0.001 0,.000
0.002 0.003 (),.000
0.000 0.003 0.000
0.002 0 .. 000 (> .. 003
0.014 0.009 0.000
0.002 0.002 0 .. 000
•
18 19
Di. CJ. Di. E<r Cl
Benz F')·c1pBr1e
0 .. 000 0 .. 000
0.,000 0 .. 000
0 .. 000 0 .. 000
0 .. 000 0 .. 000
0 .. 000 0 .. 000
0 • ()()() (\ a 0()0
0 .. 000 0 .. 000
0.000 OaOOO
0 .. 000 0 .. 000
(). 000 0 "000
0.000 0 .. 000
0.000 0.000
0 .. 000 0,,000
0.000 0 .. 000
0 .. 000 0 .. 000
0 .. 000 0 .. 000
OaOOl 0 .. 000
(),.00:l 0,.00(l
0.000 0 .. 008
OQOOO 0.007
1 Date 0124.85 0325.85 0703.85 1212n85 1214.85 0130.86 0304.86 0520.86 0730.86 0917.86 1120.86 0318.87 0514.87 0709.87 0806.87 0420.88 0806.88 1020.88 1207.88 0511.89 • He J. J. # l 2 2 9 Julian Di Cl Day Propane 1120 0.487 1180 0.308 l.280 0.176 1442 0.143 1444 0.068 1491 0.220 1524 On252 1601 0.216 1672 0.402 1721 0.364 1785 0.887 1903 0.152 1960 0.283 2016 0.837 2044 0.127 2302 2.093 2410 l.497 21.+f:1 ~:_:; 2'.5:J:J 2681::1 1 "70<':-J 1 • 1.f37 0. ~j84 • 10 11 12 Toluene Tri Cl I)i Br E·thane Ethane 0.000 0.132 0.015 0.000 0.082 0.012 0.000 0.064 0.008 0.000 0.072 0.011 0.000 0.039 0.006 0.000 0.085 0.011 0.002 0.081 ().009 0.000 0.112 0.013 0.000 0.095 0.012 0.000 0.091 0.014 0.000 0.200 0.030 0.000 0.052 0.006 0.002 0.111 0.016 0.003 0.235 0.041 0.002 0,,092 0.018 0.005 0.428 0.057 0.005 0.383 0.068 0 .. 000 0.005 o.oo::?. 0,, l+'.:5E'. 0. :12? 0 H '.3f..-?.2 O .. 0'-?1 0.076 0. Ol,::'i 13 14 Cl Beriz Eth Benz o.oc,o 0.000 0.000 0 .. 000 0.000 0.000 0.0()0 0 .. 000 0.000 0 .. 000 0~000 0 .. 000 0.000 0.002 0 .. 001 0.003 0.003 0.005 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.(10() 0.000 0.000 0 .. 000 0 .. 000 0.001 (),,()01 0.002 0.002 0.001 0.004 0 .. 001
• Well #12
1 2 3 4
Date Julian Diethyl Di Cl
Day Ethe)· Metha~,e
0124.85 1120 0.383 0.000
0325.85 1180 0.153 0.000
0703.85 1280 0.040 0.000
1212.85 1442 0.023 0.000
1214.85 1444 0.041 0.0(>0
0130.86 1491 0.040 0.000
0304.86 1524 0.030 0.0()()
0520.86 1601 0.058 0.003
0730.86 1672 0.099 0.00()
0917.86 1'721 0.000 0.000
1120.86 1785 0.230 0.000
0318.87 1903 0.025 0.003
0514.87 1960 0.052 0.004
0709.87 2016 0.218 0.016
0806.87 2044 0.022 0.002
0420.88 2302 0.561 0.014
0806.88 2410 0.470 0.006
1020.88 2485 0.810 0.032
1207.88 2533 0.945 0.086
0511.89 2688 0.142 0.128
Chloro·-
0.285
0.206
0.101
0.200
0.105
0.159
0.158
0.213
0.276
0.243
0.547
0.137
0.256
0.503
0.113
0.648
0.585
0.829
0.820
0.388
•
6
CC14
0.012
0.015
0.004
0.023
0.012
0.010
0.014
0.020
0.(123
0.030
0.031
0.018
0.022
0.045
0.023
0.045
0.041
0.061
().069
0.030
7 8
Berizene Tri Cl
Ethene
0.000 0.000
0.,000 0"03~
0.000 0,,023
0.000 0.035
0.000 0.022
0.001 0.030
o.c)02 0.035
0.005 0.0,~3
0.004 0.057
0.000 0.064
0.016 0.(198
0.003 0.032
o.oos o.c,53
0.016 ().122
0~003 0.078
0.041 0.169
0.030 0.098
0.042 0.134
0.051 0.126
0.015 0.098
J.
Date
0 l :::~t.~" f::l~::i
0219.85
o::--:JC~5 .. 8~3
070~:3. a~.~i
061.9.86
1205.G6
031.cl.8'7
0411 . 8'7
0709 .. :.:3'7
1 oot:~ .. fJ7
0203. fJ8
Ottf.7.'.0 .. !3Et
07 l 9 .. flll
1020. 813
l E!OB .. f.~lEl
0~311.89
E~
Julian
Day
:l. l E?.O
1 :lL,6
1. 1 ao
:t,2130
1631.
:lE:lOO
J.703
1727
E.!O l 6
E!10:l
2225
(!.'.30i:.~
f!cl92
E!~:_:_i3t.+
261313
•
3
Ch loi-o-·
forHm
0 .. 02E3
0 .. 015
0 .. 02ft
0.017
0 .. 2E.!O
1. .. 027
0" 1. (:?.~.:;
0.095
(l .. ;:.~61..i·
0 .. 303
0.292
0 .. ;_;:.~(?9
0 .. L~O~i
0.693
0 .. 6!'::J'."}
0. 23lt
•
4 5 6
CC14 Tri Cl Tet Cl
Ethene Ethene
0.0()() ().()00 0.000
0 .. 000 0 .. 000 0.000
0 .. 000 0.000 0.000
0.001) 0.000 0.000
0.000 0.000 0 .. 000
0.013 0.000 0.000
0.,007 0 .. 000 0 .. 002
0 .. 003 0.000 0.003
0.003 0.000 0.003
0.004 0.000 0.004
0.004 0.000 0.003
0.,003 0 .. 001 0.01:,3
0.000 0.000 0.002
0.004 0.005 0.003
0.()00 0.000 0,,004
0.002 0.001 0.004
:I. Da tE• 1127.84 0325.85 0924.85 1204u85 0121.86 0225.86 0513,,86 0730.86 0916.86 1120.86 0204.87 0218.87 0514.87 0806.87 0127.88 0407.89 l• .. lp]. l 'lt7 7 ~ Julian Dciy 1062 1180 1363 1l~34 1482 1517 1594 1672 1720 1785 1861 1875 1960 2044 2218 2654 • 15 T.,,1; CJ. Ethene 0. 00() o. oo:.~ 0.01'+ 0 .. 01.:~:3 0 .. 024 0.032 0 .. OE:\'.~:i 0.059 0 .. 092 0.065 0.083 0. QL+5 0. 06:)9 0. 0'-78 o. :1.c11 0 .. 103 16 Di Br Ethane 0.010 1).014 0.376 0.043 0.036 0.099 0.041 0.031 0.000 0.316 0.119 0.051 0.675 0.778 0.031 0.034 • 17 18 19 Cl Benz Eth Benz Xylene 0.000 0.000 0.014 0.000 0.000 0.007 0.0()0 0.000 0.010 0.065 0.018 0.014 0.082 0.130 0.061 0.0't6 0.000 0.000 0.034 0.005 0.000 0.012 0.000 0.010 0.005 0.085 0.024 0.018 0.143 On182 0.042 0.026 0.000 0.000 0.079 0.013 0,,000 0.031 0.000 0.076 0.045 0.262 0.1~12 0.068 0.426 0.554 0.478 0.511 20 XylE:nf:? 0~000 () ~ 000 0 n Ot+ l (l u ()(){.; 0,. 000 0.017 0 .. 000 0 .. 0'.B On022 0. 10:l 0 .. 0:39 0 .. 02'7 0,. lEiB 0 n 2f.:>5 0.1.J.3 0.1.l.l
1
Date
1127.84
0325.85
0924.85
1204.85
0121.86
0225.86
0513.86
0730.86
0916.86
1120.86
02()4.87
0218.87
0514.87
0806~87
0127.88
0407.89
• Well #7
2 9
Julian Tri Cl
Day Ethene
1062 0.000
1180 0.006
1363 0.054
1434 0.041
1482 0.035
15:l7 0.042
1594 0.()25
1672 0.135
1720 0.124
1785 0.163
1861 0.117
1875 0.067
1960 0.173
20l►4 0.227
2218 0.309
2654 0.l~06
•
10 11 12
Di Cl CH3 Toluene
Propane Pentanone
0.000 0.000 0.000
0.206 0.000 0.020
1.621 0.000 0.297
0.328 0.000 0.130
0.210 0.000 0.071.
o.,~15 0.000 o,.196
0.097 0.000 0.164
0.156 0.000 0.499
(1.120 0.000 0.2,~9
1.676 0.000 1.882
0.447 0.000 0.678
0.188 0.007 0.£~42
2.26s o .. os,~ 2.ss1
0.958 0.027 4.154
0.,128 0.012 1.795
0.384 0.178 1.116
13
Tri Cl
Ethane
0.000
0.000
0.277
0.017
0.012
0.054
(1.015
0.000
o.cioo
0.192
0.051
0.025
0.524
0.710
0"()08
0.000
14
Di Cl
P1·opsr1e
0.130
0~000
0.053
0.000
0.000
1).016
0.000
0.000
0.000
O.Oi)O
0.000
0.0()5
0.076
0.058
().000
0.000
:I.
Da tc;,
1 :I.E!7" Ei!.+
0:3[~~:i .. 8~5
092l+ .. 85
1 E!.0'+ .. 3;5
OJ.E'.!l .. 8fJ
0225.86
0~,13.86
07::➔0" [36
0916.86
t lC~0.86
()E!.Ot.+ .. [)7
0218.13'7
051.Lt.,f'.37
OD()f.:>" B?
0 l (2'7" f3El
0407~89
i:.~
Julii::tn
Day
106:)E!
l lGO
1.363
:I. .:+:3'+
1 '+fli'.'.
1517
1 '.:i9L+
:tt:1?f.?.
1720
1785
lf::16 l
1E37~i
F/60
20L+f.t
2E! l E~
2654
•
Oice>thyl
Etht?"1·
OnOOO
()" ~-3C/l,t
(),.l+31-?
O .. Lt84
0,, E?.'.:l 1.
O.E-~15
0 .. 1. '+~5
0 .. ,;i6'.]
l .. O~:i9
l • 7Lt9
O .. f:i9'.'.:l
0 .. 212
l. 774
1 .. O~iO
4.049
'+ Di. Cl
Mt:!thr.ttY-ie
0 .. 0 i.7.~~:;
0 . 0lt5
0 .. 1.53
0 .. OE~Lt
(>" OO:':i
0 .. 016
0" ()l+6
0,. :l 9lt
0 .. :I.BO
0 .. 377
0,, '.::10~:_;
0 .. 05~::i
0,.5lt2
0 .. 390
2.779
•
1-Pentene C:hlcrc-
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 000
0 .. 012
0" 0'7~i
0 .. 01G
o .. 0::10
0 .. 000
t·ot·m
O .. '::iF:.'.O
C! .. ~i:31
2 .. 902
f.t .. 39(:,
3 .. 209
3. 107
B .. 376
8 .. 005
l :l .. 337
6 .. ::_;91
cl.312
l 2,. lJ.~jl~
9.706
19 .. 010
7
C:CJ.L+
0 .. 3El0
0 .. 6or~
0 .. 962
0 ~ (;,2::J
0 .. 901
1 • 07 :l
l .. 056
1 ,, 9(.?.t+
() .. 36l~
1 .. 276
1 .. 107
0 .. ?i=~ 1
1. 3E12
l .. O''?l+
l .. OL~f))
1 .. 083
f.➔
Br2n:;:.~c~nf::!
0" 00()
0. 00(.7~
0 .. 2t.)O
0. 0(~:3
0 .. 000
0 .. 700
0 .. 1.07
0.3'79
2.72cl
1 .. ::101
0.676
E~ .. 71.~::.1
E?. .. ,6l1.f+
2 .. 600
1
D;;d; e
1126. 84
03E.!5,, f:3~5
09:::!.5 a 8~5
1212 .. 85
01'.'.:lO .. Elf::i
0::104 .. 1:16
05E!O" t36
07;;30,, f:16
09l6a86
l l E~O .. El6
()2()L~ ,. 8'}
OLtO:I.. 87
O~:i l Lt .. f.3'7
l OOE!" c17
0127.88
071 E~ .. i3E:l
• Well #6 Fi.le C
2
,Julian Di Be
Di:':l.\' Ethc1i·1E•
1.061 2 .. 800
1. lBO
1 '.](:,4
14'+2
l '1''? 1
:1.~:_;24.
1 c,O 1
l67E?.
1720
l 78~~;
1 B'._:,:.;(:_;,
1917
1760
f..?.1.01
2E:18
2~JD'.5
2,, 5~30
l.,t ,, 003
2. ~iOO
0" 7313
2,. L+[.~8
l ":::s:'::iEl
::1 .. 027
(J,, 85L+
l. 071
l .. '+9 l
1 .. 25'1.
0. ff7'+
1 .. 002
1 n '.Jf:.i'i.:?.
1 l, j •*'/
. '
Cl Benz Eth Benz
0 .. 000
0 .. 000
o. oc:?
0.000
0 .. 0:1.'.3
0 .. 04[-?.
0 .. 000
0 .. 000
0. :t 19
0 .. 000
0 h 101
O.lL>7
0 .. 12/:i
0. 170
0 .. 2:llt
0 .. E!C:)f:.~
0 .. 160
0 .. 1.50
0 .. 2'.:.i'-t
0 .. 249
0,.071
O.L1-lO
o .. ]'·t·l
0 .. 694
0. :::127
0 .. 3C:l 1
0 .. 625
()" l~CJI.~
0. '-tf:.)'-?
0.551
0 .. 6:if:Jl+
•
:LB
Xylt!~ne
0 .. 370
0 .. 300
O .. 6~:;E!
Or.7El5
0 .. 1'71
0 .. 929
0 .. 898
l "6136
2 .. 5?0
l .597
:l.:l1?
l .. 701..1.
:1. ,.L~~:i1
1. "'+21
o .. ~i69
l .. ??'.:i
19
XylE)ne
0 ~ E~OO
0 .. l SiO
o .. :m::i
0"41.3
0 .. 07/:)
0.592
0 .. 7:31
0 n CJ~~/c:J
0.887
l .. l l 0
::i • 1 or~
0 ~ ~)69
O.,B37
0 .. ?013
l. 021
l ,. 1.7~ ~) El
1
Date
1126.84
0325.85
0925q85
1212.85
0130.86
0304.86
0520.86
0730.86
0916.86
1120.86
0204.87
0401.87
0514.87
1002.87
0127.88
1)712.88
Well #6
2
Julian
Day
1061
118()
1364
1442
1491
1524
1601
1672
1720
1785
1859
1917
1960
2101
2218
2385
• •
File B
9 10 11 12
Di Cl Br· Cl CH3 Toluene
Pr·opane Methane Pental1one
4.150 0.00() 0.330 16.850
9.800 0.000 1.880 14.900
7.3f1 0.215 0.786 26.471
2.902 0.000 0.000 5.641
1.346 0.()()0 0.286 5.783
4.585 0.000 1.343 14.636
4.227 0.000 0.474 12.580
8.440 0.000 0.913 12.529
9.124 0.000 0.665 24.924
8.538 0.000 0.605 11.565
2.847 0.609 0.165 17.820
31.750 2-'•92 0.579 23.318
3.118 0.705 0.225 9.338
1.384 7.285 0.068 5.481
2.379 0.998 0.127 4.033
3.847 1.507 0.787 4.061
13
Tri Cl
Ethar1e
0.255
0.270
0.516
0,,301
0.124
0.418
0.218
0.000
(1.635
0.000
0.177
0.572
0.242
0.102
0.088
0.084
14
Tet Cl
Etherie
0.000
0.000
0.000
0.000
0.007
0.260
0.000
0.000
0.056
0.000
0.039
0.00()
0,,000
0.095
0.103
0.081
1
De:\ t f2
1126. El4
0 ~:3 ~?. ~:i .. 8 ~-~j
09E?.5 .. 8t::i
01.30 .. 86
030i.t. 86
05E~O .. 06
0730. 8l;
09 lb" €~l6
1120.86
0204 .. f::l?
0'+01 .. B?
051.L+n87
100~'.'.!. 0'7
0 12'7. 8f.l
07 l E:!. f3B
~Je l l tt6
2
J·ulia.n
Dr.:ty
1061
l 100
13lA
1 l.t '·t C!.
l.'+91
1 ~52Lt
1601
1672
1'7E'.O
l '785
1859
1717
1960
E.'.101
221.8
C~3t~5
• Fi. le~ A
3
Di.r,thyl
Etht:!r'
10.650
E!f?.. 800
t:>5 It 800
16. 176
l l . cl61
E~6. 158
Co~ t..t ,, 6 ~:l ::1
("~lt .. 918
::11.1::13
35. '7fl0
6. clOfJ
7'+ .. 777
11 .. 294
5. ::i85
'+
Di. Cl
0. ~:iOO
o .. 100
2 .. f:101
0. C~B9
0., 0()0
0.000
1 .. ,,0::1
2.340
1 • ::iDEl
3 .. 116
l .. o::;9
1 1 ,, L1-(l(:)
2.443
:I. .. :·;~:10
2. 05Z1
:::➔.c'i21
~ ,.!
Chloro-
fc,i .. m
::ll .. 500
lt~.'~j., 300
103 .. '+67
E.'3. '79'7
6'7. 1'786
1 E:!;~~'.., 6(~.'. l
1'.:,9.1Lf7
l 7:j., :36E~
1 :::{~i .. l 60
67. 82'.'I
5t:,:~.:; .. 19'+
99" ()5Lt
~it> .. 72El
76.2:lt,
•
l,
CC).{+
0. l 9'.:i
0 N ::39()
0 .. 969
0 .. 000
O .. '.:llfJ
1 . o:::; 1
2" OL+:J
c~. '+3o
O.'.JJ.'7
1., :tC17
l "'JL,O
l :l ,. Of~l+
l .. 687
l~., 006
1.962
:t .,86E!
7
Bt::nZf?.ne
9El. 500
1 E!9 .. 000
109 .. 802
36 .. f25E!
i.7.\0,, Bl1, :1.
lt5Q 150
L1. E5 n l l ::::i
85 .. 795
92.91.5
6'7 "3lt0
2'+. fJ4Lf
5" 3E.!B
8
T;-i CJ.
E:thE!l"'1€-:~
1 .. 000
1. 620
E! .. 612
l .. 0 lE!
2 .833
:.~1 .. {.~f:33
5.2:t:~)
6 .. 09~~3
Lt" l.r()f.t
3. lf1lt
~3. :34.9
2 .. f:l69
2 n (SOE3
1
DF.1 tE•
0909b86
1 l 1 l ~ 86
0 l i:1 fJ. 8'7
0325.87
061D.ff7
11E0.8'7
0'.:309 .. f.lfJ
071 E~ .. 138
1027 .. f:18
0Lt07. (:jfy
• l,Je 11 11'3Et
2 3 4
Julian Diethyl Di Cl
Day Ether Me·thane
1713 0.008 0.010
17'76 1.3D1 0 .. 335
1854 0.032 0.016
1910 0.04~ 0.013
1995 0 .. 019 0 .. 012
2150 0.013 0.018
2260 0 .. 004 0 .. 009
2385 0.006 0.01)5
2492 0.002 0.003
2654 OnOOC> 0 .. 000
Chlor-o---·
·f"ocm
0. 1.61
::l. 4f3'7
0 .. 277
0 .. '+B9
0. t+f:.?.fJ
0.177
o .. 2~::;o
0. l i:~4
0. Obt:l
•
b
C:C:].li
0.000
0" 1 ?i.7!
().,018
0.005
O .. Ol+:J
0.010
0 .. 00'.:I
0.006
0 .. 000
0" OE:El
'7 8
BE-:n·z.E:nt:.:: Tc i C 1
Ethr2r11::::
0.057 0 .. 005
l ,, ~::J60 0 . :t. '.:.~r..-?
0 .. 195 0.0.1.0
O .. Ot+:=J O .. Olf:?.
0 .. 01.E! O .. Ol'.3
0 .. 018 0.008
0 .. Of.:~O O. 0 l l
0. 003 0., 00ft
O.OOE! 0 .. 003
0 .. ()00 0" 0 l l
l
Da t,,,
or:,,09. a,b
1 l 11 • 86
01. f.!1:1 .. i:1'7
032~i M 8~?
oc., 18" E➔7
111.~0.B''?
0309 .. EJEl
071 ,,:?. H 8(3
l.Oc!7. El8
OL+0'7 u B•::y
•
2 3 4
Julian Diethyl Di Cl
Day Ether Methane
1713 0.008 0.010
1776 1.381 0.335
1854 0.032 0.016
1910 0.045 0.013
1995 0.019 0.012
2150 0.013 0.018
2260 0.004 0.009
2385 0.01)6 0.005
2492 0.002 0.003
2654 0.000 OuC)QO
L7-' • .. J
Ch lor-o·""
form
0 .. 161
3.487
(l" f~(:yr:;
0. 48':;>
()" ltf.':!t{
o .. 199
0. E.~50
0. li.:~Lt
0 .. 068
0 "6~5..'t
•
CC14
0.000
0. 172
0 .. 0:1.f:l
0. 00~5
0., Ot+:::l
0. 010
0 .. 00::1
0.006
0.000
0., ()f'}.fJ
7 8
BE~nzene ·re i Cl
Ethe:-nE•
o,, o~:i'7 o. oo;:_:;
1.360 0.1371
On iC/~:i (),.()J()
0.043 0.012
O.Oli.'.·.! O .. Ol~:l
0.018 0.008
0 n (Jf.'.:)() ()" C) J. :I.
0. oo:] 0 .. OOlt
0.002 0 .. 00'..3
0 .. 000 0"011
:l
Da t,2
0909.Bb
1 1 1 :t ,, ~31.'J
0 lf!.8 .. E17
0325.f37
0618.87
O?E?.1 .. 13'7
11PO .. B7
0309. 8f3
0'712 .. Bll
102?. 13El
01+07 .. E!''i'
viel.l #3?\
2 3 4
Julian Diethyl Di Cl
Day Ether Methane
1713 0 .. 019 0.00'7
1'776 0.01.1 0 .. 000
1854 0 .. (>01 0.000
1910 0.000 0 .. 016
1995 0 .. 000 0 .. 000
2028 0 .. 001 0 .. 002
2150 0 .. 000 0 .. 007
2260 0.001 0 .. 001
2385 0.000 0.000
2492 OuOOO 0.000
2654 0.0()0 0.000
r.::· ,_,
Ch l or·o .. ···
foi· .. m
0. 05El
0. 0~~_;7
0,,02'7
O .. Ot+:3
0" 0Ltr3
0 .. 1C~:l
(l .. O:::lL1,
O .. Olt~:.i
0.032
0. ()L~O
0., f?'+'-?
•
,'.::) 7
C:C:J.L, Tri C:l
Ethe.rH,?
0 .. 000 0 .. 001
0 . 000 0 .. 00()
OnOOE! 0 .. 001
0 .. 00'+ 0 .. 001
0.005 0.002
0.009 0 .. 003
0,, 00:::1 0 .. OOE!
0 .. 002 0 .. 002
0 .. 000 0.001
0. 000 0. OOE?.
O .. Olt:l 0 .. 006
8
To 1 ut:::•ne
() n ()(l()
o.ouo
0 .. 0(>0
0 .. 000
0.000
0,. 0()0
0 .. 000
0 .. 000
0.000
0.001
0 .. 000
C. "pcp;.rtTn-:nt of Hum.an Resources
vi.sion of Hc:i.lth Services
. Suf!ctFU.#0 ·
•. SAMPLE ANALYSES REQU. State Laboratory of Public Health
. IO£~ rr9P.MJ·•)i>·lll"x 28047
/ / ,.. ) I CJ l..J ~ ~9g;,lff-'(,w~:n£7~7{
cc Number _·_C-Jt......!Ld-:_.=cD::.__~_-L·...,o~O_S_,_s_-i_/_:::.0_'.:)_tJ_ Field Sample Number -71'"· -;---_1·_;,1.-!''f,_J_A __ N-'--'2_:J'-1""9c:!9.:::.D __ _
ame of .Site ---=-/V,--=-_C:,.__,,"----'-S'-'-f-'q'-'/'-~_,,_e_· _______ ~· ·: ·.site Locilion --,:..·1-:f2':.'Q.~~~~1:·:ti-..!1i~;R::@J~~M[,,!••---
ollected By ....::cC..:'...:V,:._.ad..L;-1.1!,!Q_.,152./Li-ut ,_,· f"l'-L--IDli __ L/+--.,1-l_ Date Collected ....l.!ad,..c;.j....Ll.c:..f.--'l$='-'~--Time '.'o ()
.,.,:·:z::;,.; ___ ,,.:.~~_r s,..a.;,'.:':~::.:;::h=-~=-:=at.,,c.r""'--=(l_) __ --_°'--~n--"~_;~:.:'.".'·b:",;~""(=5-"'~ ~""-""· -===,,=M"" .. :"';~=~--"'-hf,,.~,;;,';..,d .. ~;.;g=-=
1
,"'!Co-.;:;;:m;;;;m~' ~"'en"',~""
1
·=v)l-
0
=·~=-~,.,-~--,:=·~=~---I/--~~..:.;. .. ~
_._· Surface Water (2) ___ Liquid (6)·
---Soil (3)
__ Other (4)
__ Sludge (7)
__ Other (8)
E.xtractables
Parameter
_Ar.scnic
__ Barium
_· Gdmium
_Chromium
_Lead
_Mercury
__,.._S~J~.~iu_!I'l._. _
_ -Silver
Results rng/1 Para.meter
__ Arsenic
__ Barium
__ Gdmiurn
__ Chloride
__ Chromi,:;m
__ Copper
__ Fluoride
__ lron
_wd
__ Mangan=:
__ Mercury
__ Nitrate
__ Selenium
Result> mg/1
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
_Ph
__ Conductivity
__ ms
_TOC
Results mg/1
ORGANIC CHEMISTRY
Results mg/1
, __ Acid:B/N Ext.
TOX ✓ ol ·, b ! ,.JJ>.J! e:..ir=----
MICROBIOLOGY
Para.meter
__ (MF) Coliform Colonies/!OOmls
__ (MPN) Coliform Colonies/lOOmls ·
Parameter.
_. _EDB
___ PCB's
__ Pe.rroleum
_ . _Endrin
__ Lindane
)are Rccciv,;d __ ,._,I J"-"-d-e_:D,:__·_,,f{,__q_,_,_,,X-"'./3=----------
Resulu mg/ 1
I . Paramete,;
_:_ Gross Alpha
__ Gross &ta
Para.meter
__ Methoxychlor
__ Toxaph=e ·
_2,4-D
Rcsulumg/1
--2,4,5-TP (silvc:x) _____ _
RADIOCHEMISTRY
Results PCi/1
Date Reported -::::::--:-,,_-_l__,1_-_f;._:o:::....._-______ _
fr. -
· )arc Exrrac,ed ----------~--~---Dare Analy:cd _ _,_l_-fw6c.....·9~D";;--,,71~1l~r:;-;:;=-----.....:..-
~
·7J. 11 /1 od 903767
· ".cponcd By J'(Jf?'Y/ J...": I'-"' Lab Number -------,-------'--
. 3 {,,, -
>HS110l/RcviKd7/85) ~'[{/ 7 7 °I0:377;2-
C. Dcpurmcnt of Hum:rn Resources
vision of Hc..i.lth Services • S v()S-/Fu;'i/J:) •
SA1viPLE ANALYSES REQUEST
Concentrate
' Time d-', O ()
~-.---------~~
·------~-~~==---:-~---= _:
Cornrnenu
""'r-,,e:~of-5a :11 pie~,,.,_,,.._
·-::nyonmenta1.
__ Groundwater (1)
~-Surface Water (2)
__ SDil (3)
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
\tV~,:5 + t i-d~ e,; I c.o 1tttrtv, ,'l-y wejf
__ Other (4)
Extractables
Parameter
__ Ar~nic
__ Barium
_· Cadmium
_Chromium
_Lod
__ Mercury
____,.. Sdl:".nium_ ·-
_-Silver
Parameter
Results mg/1
Re•ults mg/1
-:u MICROBIOLOGY
Para.meter
__ (MF) Coliform Colonics/lOOmls
___ (MPN) Coliform Colonies/lOOmls ·
INORGANIC CHEMJSTRY
Parameter
__ Arsenic
' __ Barium
__ Cadmium
: __ Chloride
__ Chromium
__ Copper
__ fluoride
__ lron
_Lead
__ Mang.an=
__ Mercury
__ Nitrate _
__ Selenium
Results mg/1
ORGANIC CHEMISTRY
Par.uneter_
_, _EDB
__ PCB's
__ Perroleum
__ Endrin
__ Linda.ne
Results mg/1
s:o,aao¢
P a.rame cc,;
_._Gross Alpha
__ Gross Bera
JAN 2 31990
SUPERFUND SECTION
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
__ Ph
__ Conductivity
__ TDS
_TOC
Parameter
Result< mg/1
Raulumg/1
__ Methoxychlor < 0, Q(J/
__ Toxaph=e · <o.oo.;z
_ 2,4-D L-CJ.Ci(!) I
--2,4,5-TP (silvcx) _<..:,..,:O:.:.•.:::Q')=.J\,___ _
RADIOCHEMISTRY
Results PCi/1
C. Dep~r~'c::nt of Human Resources
vision o( Hei.lth Scrvicci;
•. ~V(}Ef?FV/10 ·
. SAMPLE ANALYSES REQuet·
:pe of Sample:
"!iLC: --••
Envirrenta.l _ Concentra tc
__ Solid (5)
-eommenu -
VV' e.s i .,.. , cl ~ e. ~ Co v.1 IV)
__ Liquid (6)
\/. Groundwater ( 1)
_._· Surface Warer (2)
___ Soil (3) ---Sludge (7) f le c, se CJ no lyu, Pov Q :tl-2 /I -:i'.Q~ r, /11,s
__ Othc:r (BJ +lie CP"4fO<hJ:, L·..s +eJ., .pleasQ..., f2..n5{re.,
--Other (4)
Extractable,;
Parameter
_AtS<:nic
._Bariurh
_· Cadmium
_Chromium
_Lead
1 __ Mercury ·
1_........_Sclenium __ _
_ .Silver
Results mg/1
,--------------.,
Results mg/1
. _ Acid:B/N Ext
TOX T d I·< h [ '.LA.IL Cwfc._ __ _
v
MICROBIOLOGY
Par-a.meter
__ (MF) Coliform Colonies/lOOrnls
: __ (MPN) Coiiforrn Colonies/lOOmls ·
I c.o.,bo,d<-i-ra. t,A/o,;de_J;iPr-oeo~l}/ f ro1e,e~ e__,,JJ,.4,es
INORGANIC CHEMISTRY lJ lc.j k ~1te.s q n" l..>o I r,c./vJe.j_,
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
_' -.Chromi,.;m
__ Copper
_._fluoride
__ lron
-· _Lead
__ Manganese
__ Mercury
__ Nitrate
_,_Selenium
Resulu mg/1
ORGANIC CHEMISTRY
Parameter.
_EDB
__ PCB's
__ Perroleum
__ Endrin
__ Lindane
Results mg/1
Parametc,
__ Gross Alpha
__ Gross &:ta
Total
Parameter Results mg/1
_ Silver iCJ) cc IC:' r,,.:;;1 H;n C-ill'"llf-!!---
--Sulfat~ (I; (l;.U_"(J'--'-lb_lb{I ___ _
__ 2inc
__ Ph
--eo nd '8Ut'BIT-UND•-:SrF(F.i~TF1,f3,!!~ll--i ---__ ms ..
_TOC
Parameter
__ Methoxychlor
__ Toxaphcne ·
--2,4-D
Results mg/1
--2,4,5-TP (silvex) _____ _
RADIOCHElv!ISTRY
Results PCi/ 1
)arc Rcccivc;d __ _clJ.._-,.JcsDc._·_.,Z:w9uJ\LU.A.L-__ ;__ _____ _ Date Rc;:,orred --=::-:---------------pr: .
· )are Exrractcd -------------~---Dace Analy:cd _ _,/,:.-.,_lf:,=-'t~Qcc:72~1-fur ________ ~ _
".cporrcd By ______________ Lab Number --~S ..... O~J~7'-'6=9=---,-------""--
C. 0cp-J,rtmcnt o{Hum;rn Resources
vision of Hctlth Service.£
ce Number
• SAMPLE ANALYSES REQUEST
State Laboratory of Public Hohl
P. 0. Box 2804"
306 N. Wilmington Strcc
R,.lcigh, 2761
----. ~=== ·--
Snvrmental
··:.JJ_ Groundwater (1)
_._· Surface Water (2)
__ Soil (3)
Concentrate
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Otha (8)
Coromenu
,/1../~ 6 t Y-I clj Q '.:2__ . C..0 _'1m, l,.Uf_, fl .
__ Other (4)
Extractables
Parameter
__ Arsenic
__ Barium
_· Cadmium
_Chromium
_Lead
_Mercury
----S~.k.riiuJ.11.:_ ·-
_-Silver
.-
P;i.rametc:r
·~
Pan.meter
Results mg/1
.
Results mg/ 1
MICROBIOLOGY
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonies/lOOmls ·
INORGA .. 1''1C CHEMISTRY
Parameter
__ Arsenic
, __ Barium
, __ Cadmium
__ Chloride
, __ Chrorni;,rn
' __ .Copper
__ Fluoride
__ Iron
_Lead
__ Manganese
__ Mercury
__ Nitrate
__ Selenium
Result< mg/1
ORGANIC CHEMJSTRY
Parameter_
_EDB
__ PCB's
__ Perro le um
__ Endrin
__ Lindane
Results mg/1
<a.0001
<o.aoost
P=amete,;
_._Gross Alpha
__ Gross Bcca
R !EC !EJ V t!DJ
JAN 2 J 1990
SUPERFUNO SECTION
Total
Parameter
__ Silver
__ Sulfates
__ line
_Ph
__ Conductivity
__ TDS
_TOC
Parameter
__ Methoxychlor
__ Toxaph=c ·
_2,4-D
__ 2,4,5-TP (silve:x)
RADIOCHEMISTRY
Results mg/1
. Reau.Its mg/1
<o, oo/.
<a.op.;z
0-001
Results PCi/ 1
C.'Dcp2rm·.~nt of Hurru.n Resources
visi~n of Heilth Sc-rvica
· · S"uPcf?FU.tVk'.J ·
.SAMPLE ANALYSES REQue
tc Number
,pc of Sample: ~----·--. .,. ~:..:.,_
Envirrental Concen.trate
-¥-Grouhdv.:atcr ( 1)
~-· Surface Water (2)
__ Soil (3)
--Solid (5)
__ Liquid (6)
--Sludge (7) f fr c, se o no ly:M' Po v a 1:c,J /I ::i:QJ() n J,1,s
__ Othcr(SJ +he corv,fOvoJ:, i,'ss+e.J, .pleos-Q_ E..n;;:1,c
__ Other (4)
Extractables
Parameter
._Arsenic
_Barium
_· Cadmium
_Chromium
_Lead
._Mercury
----S~J~.~iu_rn __ _
_ ,Silver
. _ Acid:B/N Ext.
Results mg/1
Results mg/1
TOX .✓ oh·<" ~ '{! ~-.i.t..,L r .... r ___ _
-'-'JA-"'-'.LI<.AkJ.!Mlu:f .... ; ---'----
MICROBIOLOGY
Pan.meter
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonics/lOOmls ·
cec,bo,dd·ro. <-Alo,;de_,/ pt-oeo~i/ f ro;eAe°"/ e..,fJ,,ciAe.s
INORGANIC CHEMlSTRY ~ e_ 1 k e /\ e..s q rr /, l~ o ; >ic / vJ eJ,
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromi,.;m
0._.Copper
__ Fluoride
__ lron
_Lead
--Manganese
__ Mercury
__ Nitrate
_. _ Selenium
Results mg/1
ORGANIC CHEMISTRY
Para.meter.
_. _EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
. Results mg/ 1
Parametei;
__ Gross Alpha
__ Gross Beta
Total
Parameter Results mg/1
_ $ilvqgCC\ERVHFCibll[)f---_ __ su1at~J.. u v_ib_9'_'"" ____ _
--Zinc JAN 2 3 ;,;~9n9;';;'.!1------
__ Ph
-Conc!~m~ND SS!:-~lrlCT-1H!Of.l-N ---_ ms ..
_TOC
Parameter
__ Methoxychlor
__ T oxaph=e ·
-. _2,4-D
Results tng/1
__ 2.4,5-TP (silvex) _____ _
RADIOCHEMISTRY
Results PCi/1
,
1
)ace Received / :l-,;)Q-89 h$6 Date Re;xmcd _______________ _
P'f' .
1· )ate Extracted------------'--~---Date Anali~.ed _ _:_l·_l=--'e"-'---''i""D'--ztu'-'"''"'r _______ _;__
I. 90,37',i
I ".eportcd By Lab Number ----'--------,-------'-
' I >HS }\OJ (RcviKd 7/85)
C. 0cpJ,rtmcnr of Hum:rn Resources
vision of Hc:2\th Services
s; v/8"tFu,A/j) •
SAMPLE ANALYSES REQUEST
State Laboratory of Public Hccaltl·
P. 0. Box 2804i
306 N · Wilmington Strcc
;.--/ ~ , '.l R,lcigh, 27611
_c1'--:2:~D~~--'----"0C-"O"--S_..')_7__:((J~=>_v_ F1dd Sample Number -----:~)l;--9~l.,-'-'--;-J __ -,--.. __ _
cc Number
-/I ,,c: ,: f c, 1-e ' · ---------:--· ~l.l~,, !.~&-~1· ~:t-'"1 _____ _
~me: of.Site __ ./-'-V_,_ ,_="'---'--l<---<---'-"--'-'----------~-:-Site Loci::ion /[.,,_ . 5_ 'l
ollccred By ~c_,~V~ci~i~-)=q~s=/~ir~,~· f)__,____ lD/1 __ L/_,__,,~l_ Date Colleaed Id--// 8:-/ (S .. Time -:;), ; 0 0
':::.rCy'nmcnta.l. Concentrate
__ Groundwater ( 1) __ Solid (5)
~-· Surface Wates (2)
__ Soil (3)
__ Other (4)
__ Liquid (6)
__ Slu0dge (7)
___ Ot~cr (8)
Coro.menu
Fq r'.1115 Com/I)· ve )/
SUPERFUND SECTION
INORGANIC CHEMISTRY
Extractables
Parameter
__ Arsenic
_Bariurh
_· Cadmium
_Chromium
, _Lead
._ Mercury
---..SfJs.~iu_!:l.:_ __
_-Silver
Parameter
-. -
Pa"C"a.meter
Results mg/1
Remits mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/lOOmls
• __ (MPN) Coliform Colonies/lOOmls ·
Parameter
__ Arsenic
__ Barium
__ Cadmium
__ Chloride
__ Chromium
__ .Copper
__ Fluoride
__ Iron
_L.c.ld
__ Mangan=
__ Mercury
__ Nirratc·.
__ Selenium
Result, mg/1
Total
Parameter
__ Silver
__ Sulfates
__ Zinc
__ Ph
__ Conductivity
_ms
__TOC
Resulu mg/ 1
ORGA.N"IC CHEMISTRY
Parameter_
_EDB
__ PCB's
__ Pcrrolcurn
__ Endrin
__ Lind.ane
. Result,; mg/ 1
<o.ooo/
<:0,0004
Par.unecex;
_. _ Gros.s Alpha
__ Gross &:t>.
Para=eter
__ Methoxychlor
__ Toxaph=e ·
-2,4-D
__ 2,4,5-TP (silvcx)
RA.DlOCHEMJSTRY
Reoula mg/1
<:a.oat
Results PCi/1
Date Rqxmcd .
.1-)aJ__; Pi,3 } lJjJll
Dace An.al\=d r"J-2?-5[,9PdJ,t1) l-¥-90W 1-fJJo
-903772 ';,1t,
..
.-DIVISION OF HE..!-.LT:: S:C:RVIC:C:S
· .. · /) -.:. SOLI.AND HAZARDOUS \./ASTE l-'J.J,AG::J-f£K.BRA.NCR • ?_r-_3
S VI' ~t} Chain of Cus:od" Reco:::-d RlE.CJEJVltV-
Hazardous \./aste M.aterials JAN 2 :.11990
SUPERFUND SECTION
Loca:icn o: Sampling: Generator Transporter __ Treatme.nt Facili-.
__ Storage Facility __ Disposal Facility __ Landfill
~ Other : _ ____:::S::..__,,.V'-P-J?.,__1 .Lt _.-fi-"1'-'l\'-'J"-----"-/Vi-'-·--'~-c'.'.,=-cs""'-1 ;_k.....__, ----/
Company I s Name'---'N~_·_:c:::::.___::S:::....,f,c,Cl:!..LH_.__ _________ T elephone ( ___ ) _______ _
Address ,q__ C{ /e · ----'-....:....::::..,_..!.-'=..L.:.1---''-1-----------------------------
c olle c tor ' s N amec.....,,(~A a ... (ul~r:i...fkus;,...~t,{,-"'9'-'-(J.I./4,,.i.s,.,,A.af,.,_,·~r\-----T el eyhone ( 7 IC( ) 7 3 ,s -;J SJo /
;Signature
Date Sas pl ed. __ ___:._-1-l ..s.P--<..;;..1-/ ,.,d..,..Q.L../-/-'~"-[1---------T ime Sampled / 4; 0 o -16 ; CJ a
( , I
Type O:: pr O Ce s s Gene~ at ing wast ec......,,_,5_,c),<_·.Lt-"· vc.,C_i,a....,.l...,~'t----'(___>=-.'-')..,_c.J.M.,_,_,.._/.,._12 ... 6,_,,k.c..C .... <2c...·, .>.S!.../,l...~-::;-),JC,O'-=-e.,,,sc;./:_,-._c .././....!. ✓-~<'.'.;;,i
. Field I:iio~ation
119'-/) __
Chs.in · o:: ·Posiiessicin:
1.
inc:i'usiv~ dates
2.
signature
LfuyMg a_J) ~I
title inclusive dates
3.
signature title inclusive dates
Res~:is reported
sigr-12. ture rir::l.e dc.::e
Ins ::-uc r::ions: Complete 2.11 2pplic2.b_le in£ cn::c. tion including signatures, and
submit ~ith ·Bnelysis reques= fon::s.
DIVISION OF EU-"-rs S:::RVICE:S
SOLID AND HAZARDOUS WASTE: PJ~AGDENT BR.ANCE
-~ 'l"-J'/'''}'' .... · .ceipt for S2li:'Jles "-.. F "' ,. , •· 1 -·. ,-4 -~--~--.I: l! , ... "'"' ... J l' f • The samples described.belo~ ~ere collected in connection ~ith the administration,
enforcement, and.-doc\1Ille-b1t.~ftion of the:
( ) >r.fd...,l-1? Or1''1H1'l";: · North Caroliria-'Baza'rd·oJk· \..'aste Management Rules, 10 NCAC-lOF
() North Carolina Solid ~aste Management Rules, 10 NCAC lOG
() Comprehensive Enviroill!lental Response,.Compensation and Liability Act (CERCI.A)
() Toxic Substances Control Act (TSCA). 15 U.S.C. §2601,.~~-, specifically
Section 11.of TSCA, 15 U.S.C. § 2610.
Inspecto~•s Name Inspector's Address
Name of Finn Fin: Address.
Finn _Ow--ner, Opei·a ::or, or Agent
-
SAHPLE COLLECTED SAMPLE TYPE
NUMBER DATE TlliE WATER SOIL
!
-.. -'
.. '
·-.
'
Receipt for the sample(s) described.
above is hereby ack.no~ledged:
Signature of Inspector
Title
OTIIER
-· ----~
Title
DUPLICATE SAMPLES S.AMPLE LOCATION
Ori-i:REDI ACCEPTED! REJECTED 1. ON-SITE OFF-SITE
..
\' .,;..· ' ' .
I
I
I . ·,
' •,
I
I . '
.
I
I I
· Receipt/rejection of duplic2. te or split
s2.1:1ples is hereby acknmdedged·:
S igr-,c. -::u:-e cf Firm 0--w-ner, Ope:-2 tor, or Age·
COH½ENTS __ --, ___________________________________ _
BASE/NEUTRAL AND ACID
EXTRACTABLE$
COMPOUND
N nitrosodirrethvlamine
bis(2-chloroethvllether
2-chlornnhenol
ohenol
1.3-dichlorobenzene
1.4-dichlorobenzene
1.2-dichlorobenzene
bis(2-chloroi llether
hexachloroethane
N-ni troso-di -n-llrrwwlami ne
nltrobenzene
isnnhorone
2-nitrnnhenol
2.4-dirrethvlohenol
bis(2-chloroethoxvlrrethane
2 4-d i ch 1 oropheno l
l 2.4-trichlorobenzene
n°nhthalene
hexachlorobutadiene
4-chloro-{1)-Cresol
hexachlorocvcl~ntadiene
2.4 6-trichlorophenol
2-chloronaohthalene
acenaohthvlene
dirrethvl ohthalate
2 6-dinitrotoluene
acenanhthene
2.4-dinitrnnhenol
2.4-dinitrotoluene
4-ni trophenol
fluorene
4-chlornnhenvlohenvlether
diethvl ohthalate
4.6-dlnitro-o-cresol
diohenvlamine
azobenzene
4-bronoohenvlohenvlether
hexachlorobenzene
DPntachlornnhenol
ohenanthrene
anthracene
dibutvl ohthalate
fl uoranthene
• • STATE LABORATORY OF PUBLIC HEALTH DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
LAB NO q/J.r1h, SI QI) "f I II-; qo-r7'"'
FIELD# JJQiJJ 1/o/'I~ I l'IU :/
TYPE ( ) r / ) ( I l ( l
UNITS luo/ 1 ,.,_ .. n/] ,_ r .. n/J>......._, .. n/ l .. n/ka
JI\/ .., .. 0 J -' -I
S0/doSO
10.1 "':,o .,oh,.~o
/0/"30
. ,
50 1 i,.,:-,,
J,
/r>f.330 ,.~, .. ~~
so, /t,,:fO
l/1 /:J"fO
~, ~ • I \. ,
ml)L
J -Estimated value. H,.o/S0/1 ...
K -Actual value is known to be less tha~ value given.
RIECIE~VIED
JAN 2 3 1990
SUPERFUNO SECTION
( l ( l
.. n/ 1 .. n/ka ,on/ 1 ,on/ka
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nurber
NA -Not analyzed.
is the Mininun Detection Limit. m'])L ---
1/ -Tentative identification. fl -On NRDC List of Priority Pollutants.
N.C. V,fo,u.,-i_on 06 HeaLth Se1tv-i_c.v.,
VHS 3068-0 (4/86 LaboJuUo~y)
-
BASE/NEUTRAL ANO ACID
EXTRACT ABLES
CXJMPOONO
• • RIECIE~VIED
STATE LABOOA!OHY OF PUBLIC HEALlH , DIVISION OF HEALTH SERVICES, N.C. OEPAR!MEN! OF HUMAN RESOURCESAN 2 ,3 1990 P.O. BOX 28047 -306 N. WILM!NG!ON, Sl., RALEIGH, N.C. 27611
OHGANIC OlEM!CAL ANALYSIS SUPERFUND SECTION
LA8 NO Q11~ 171/)Y <./t}-=l 770 Q,-,~77_1
FIELD # 1/ 'di /l'-J'Y-1 '1/(j</-_'J'
TYPE ( ) ( I ) I . I ) ( ) ( ) I )
UNITS uo/1 'r.,n/1 ~ /uo/1 .. .-.... .. n/ j .. n/ko ""/ I ""/ko .. n/ I ""/kn
nvrene Jo/:i::i,,, / i I -
benzidioe --/.,.,-0
butvl benzvl phthalate IOI ?30
benz(a)anthracene
chrvsene . ,
3 3-dichlorobenzidine .so, lt,J,o
bis(2-ethvlhexvllnhthalate 1()/330
di-n-octvl ohthalate 10/.s.::/o
benzofblfluoranthene so/J1,,,;r,
benzo(klfluoranthene
benzo(a)nvrene
i ndeno ( l . 2. 3--<:dl nvrene
dibenzo(a.h)anthracene
benzo(o h il=rvlene ' , I/ ,/ ' /
aniline I_< 0 ,,,_ ro I 1/4..., IL,
benzoic acid
benzvl alcohol
4--<:h loroani line .. "'· dibenzofuran /0 /~,n
2-,rethvln,nhthalene
2-,rethvlphenol
4-thvlohenol ,J,
2-nitroaniline s-ol,t-<o
3-ni troa.ni line
4-ni troani line .
2 4 5-trichloroohenol ,, . , ' , '
m1)L
J -Estif1'3ted value. H2.0/ St:JI/...
K -Actual value is known tO be less than value given.
L -Actual value is known to be greater than value given.
U -Material was analyzed for but not detected. The nLITOer 1s the Hininun Detection Limit.
NA -Not analyzed.
1/ -Tentative identification.
~/ -On NROC List of Priority Pollutants.
N. C. D,i.v,0,,i.on o 6 Hea.Uh SVtv,i.ev.,
VHS 3068-0 14/86 Laboll.LLto~y)
• • . STATE LABOMTORY Of f'U8LIC HEAL TH
DIVISION Of HEALTH SERVICES, N.C. O[f'Nl!MENI Of HUIV\N RESOOHCESJAN 2 'J J99Q
P.O. 80X 28047 -306 N. IIILMINGION, SI., RALEIGH, N.C. 27&11 •
ORGANIC Q<EMICAL ANALYSIS SUPERFUND SECTION
PURGEA8 L E CO'il'OUNOS LAB NO °'0~'7•·7 qo-;,,71oc, '10377/
FIELD# I ,r,1.1-'{ ':; II q IL "1 11q4~
001/'00NO TYPE ( I ' ( I l ( I ) ( ) ( ) ( )
UNITS a.671') .. n/ka Vu<i/ I iln/ka /i,n/ l~,a/ka .. n/1 .. n/ka ua/1 .. n/ka ··-I I ""/ka
ch lorO"N?thane 10 , .. .,h LA--IA-.,
brcm::m?thane ,o·.
dichlorodifluorcrnethane 5
vinvl chloride JC
chloroethane 1n
methvlene chloride ,; ,
trichlorofluoronethane
ethene. 1 1-dichloro
ethane 1 1-<lichloro-
1.2-trans-dichloroethene
chloroform
ethane 1 2-<li ch Toro-
ethane. 1 1 1-trichloro-
carbontetrachloride
brorodichlororethane
or~ane. 1 2-<lichloro-
1 3-trans-dkhlo, i ne
trichloroethvlene
ch lorodibro,orethane
benzene
ethane 1. 1.2-trichloro-
1.3~is-dichlo ne
2-chloroethvl vinvl ether C
brmoform ,c
ethane. 1 1 2 2-tetrachloro-~
ethene. tetrachloro--
toluene
ch lore.benzene
ethvlben,ene • I .,7 ,v /
acetone /0 IA--IA.-/.,A-
2-0utJnOn(' IC
c.arbondi su 1f i de ,,
2-hexanone /(0
4-,nethvl-2-ntanone ,,...,
stvrene ,-
vinvl acct.He ,o
xvlenes lf«taf) ;;-
1LL-rl ;,,..v,...~., l .,-,.,
,(. " .\ -"·--Jo.~:,; ' . / . /
I
11'"1 l)L'/'"
J -Estimated value.
K -Actual value is known to be less than value given.
l -Actual value· is known to be greater than value given.
U -llaterial was analy,ed for but not detected. The nuroer is the ~ininun Q!,tection !_imit. -''/H./J L
NA -Not analyzed.
1/ -Tentative identification. !I -On NROC List of Priority Pollutants.
~.C. Division of llealth Services
011S 3068-0 (4/86 Laboratory)
. Qep~rtrr.ient of Environmental, Health, and Natural Resources/Superfund Section
State Inactive Hazardous Sites Inventory •
February 1990 . • State Inactive Hazardous Sites Inventory
State Priority List (SPL) Sites
U.S. EPA N.C. Superfund Site Name Oty County
ID Number ID Number
-NCIJ024462327 SIS600100068 ACADEMY STEEL DRUM MATTHEWS MECKLENBURG
.-,;c00031s2s42 SIS840100072 ALCOA BADIN DUMP BADEN STANLEY
·-NCD002464691 SIS110100012 ALLIANCE CAROLINA TOOL AND MOLD ARDEN BUNCOMBE
-NCD119168813 SIS600100081 ANILOX ROLL COMPANY CHARLOTTE MECKLENBURG
-NCD980557557 SIS760100086 ASHEBORO LANDFILL ASHEBORO RANDOLPH
-NCIJ070619663 SIS110100087 ASHEVILLE DYEING AND FINISHING SWANNANOA BUNCOMBE
-NONCD0000025 SIS390000817 ATHOL BURN SITE BUTNER GRANVILLE
-NCIJ072003635 SIS390100089 ATHOL MANUFACTURING COMPANY BUTNER GRANVILLE
-NCIJ051853547 SIS920100090 AUSTIN FOODS CARY WAKE
""!'lCIJ071567374 SIS410100003 BILL MARTIN LIVESTOCK GREENSBORO GUILFORD
-NCIJ048184451 SIS970100037 BURLINGTON HOME CHAIR RONDA WILKES
-NCIJ096158696 SIS410100107 BURLINGTON INDUSTRIES, INC. GREENSBORO GUILFORD
-NCD003216397 SIS340100108 BURLINGTON INDUSTRIES, INC. KERNERSVILLE FORSYTH
-NCD980557664 SIS920100014 BURLINGTON INDUSTRIES, INC. RALEIGH WAKE
-NCD981022288 SIS600100113 C&T REFINERY CHARLOTTE MECKLENBURG
-NCD003184710 SIS100100651 CAROLINA CREOSOTING CORPORATION LELAND BRUNSWICK
-NCD981015886 SIS110100652 CAROLINA PRODUCTION FINISHING ASHEVILLE BUNCOMBE
--NCIJ003200854 SIS420100140 CAROLINA WOOD PRESERVING CO. SCOTLAND NK HALIFAX
....i.NC0065288847 SIS460100144 CF NITROGEN, INCORPORATED WINTON HERTFORD
-NCIJ044447639 SIS600100029 CROWN CENTRAL PETROLEUM CORP. PAW CREEK MECKLENBURG
-NCIJ006991210 SIS650100181 DE POORTERE CORPORATION WILMINGTON NEW HANOVER
-NCIJ040047 466 SIS920100194 EAST CAROLINA METAL TREAT, INC. RALEIGH WAKE
-NC0004520136 SIS730100195 EATON CORPORATION ROXBORO PERSON
-NC0062566047 SIS230100209 FASCO INDUSTRIES, INCORPORATED SHELBY CLEVELAND
-NCIJ000605303 SIS240100214 FEDERAL PAPER BOARD COMPANY RIEGEL WOOD COLUMBUS
-NC0067191262 SIS980100016 FIRESTONE TIRE AND RUBBER COMPANY WILSON WILSON
-NCD980503056 SIS650100222 FLEMINGTON LANDFILL WILMINGTON NEW HANOVER
-NCIJ093340487 SIS600100228 FLORIDA STEEL CORPORATION CHARLOTTE MECKLENBURG
-NCIJ071579528 SIS990100226 FORBUSH METAL YADKINVILLE YADKIN
-NCD991277922 SIS360100030 GASTON COUNTY DYEING MACHINE CO. STANLEY GASTON
-NCD003149291 SIS360100034 GASTON COUNTY DYEING MACHINE CO. MOUNT HOLLY GASTON
-NCD0513229B0 SIS600100232 GENERAL ELECTRIC COMPANY CHARLOTTE MECKLENBURG
-NCIJ093137636 SIS100100239 GENERAL WOOD PRESERVING CO., INC. LrLAND BRUNSWICK
-NCD980843460 SIS600100066 GRANT CREEK-WWW "'6• le, i,,'qh f T"• { N ,./ / 1•t'ft.LISBURY ROWAN
-NCD98055769B SIS740100058 GREENVILLE CITY LANDFILL GREENVILLE PITT
~CIJ024459471 SIS240100255 GUYTON BATTERY SERVICE CHADBOURN COLUMBUS
-NCD108702606 SIS600100063 HARTSOE BATTERY KANNAPOLIS ROWAN
-NCD980483275 SIS420100011 HELENA CHEMICAL COMPANY BENFIELD HALIFAX
-i.cD9B1021915 SIS430100295 J STREET FLYASH DISPOSAL ERWIN HARNETT
-NCD981031693 SIS620100040 KEENER LANDFILL CLINTON SAMPSON
Page t
., , . l[]_J . Su Pc1r r-u/!IJJ
C. Ocp:i.rnncm of Hurrun Roou:-cc.s • ·~ _ --
vision of Holth Snviccs . SAMPLE ANALYSES REQ~T State Laboratory of Public He
P. 0, Box 28
306 N. Wilmington S:
'c ~,'men ta] .
___ Groundwater (!)
-~-Surface Water (2)
__ Soil (3)
__ Other (4)
Con.c~ntratc
__ Solid (5)
___ Liquid (6)
__ Sludge (7)
__ Otha (8)
R,Jeigh, 2'i
SUPERFUl\!D ,SECTIOl\t
INORGANIC CHEMISTRY
Extractables
Parameter
crcury
S<;_ls,~iu.rn_. _
_ ,Silver
Results mg/I Parameter
_· _Arsenic
!di,rium _v_ r Ca-drnium
_,,Chloride
_v'_ r Chromium
__ Copper
__ fluoride
~on _Lead
Result> mg/I
<:::,, 0, I
<, o,oo<
< o,o/
Total
Para.meter
~ilver
__ Sulfates
__ line
_Ph
__ Conductivity __ ms
_TOC
Rcsulu mg/1
ORGANIC CHEMISTRY
Parameter
,_, _ P& T:GC/MS
__ Acid:B/N Ext.
_TOX
Results mg/1
' ------"-~--------
MICROBIOLOGY
Para.meter
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Parameter
_EDB
__ PCB's
::..!.__Pecroleum
, __ Endrin
__ Lindane ·
)ate Rccc:fv<:d _________________ _
).:uc Extracted---------------'----
,;:-:,..,..._"r:r,....4 Rv __________________ _
Result,; mg/ l
P;;rn..metet;
__ Gross Alpha
__ Gross Beta
Parameter
__ Methoxychlor
__ Toxaph=e
_2,4-D
Rcaulu mg/l
--2,4,5-TP (silvo:) _____ _
RADIOCHEMJSTRY
Results PCi/1
Date Rcpon:ed ---':l!./4"-"~9-''t,o'---------c-
Date Analy:cd -----==----------
Lab NumL_ _______ :::_· __,_•-._,_.,v·_.,_'J•_',_·',..-l,·.:_ . .:_(..:,'_· :: . ..:,_, ----'-OCT ._,l 1-i ,:_J
@)
C. Dcp2rnncnt of Hum.2n Resources
vision of Holth Services
• ~u(}6ff~
_ SAMPLE ANALYS~~QuWr
cc Numbcr
( 1)
-~-Surface Water (2)
--Soil (3)
__ Other (4)
Concentrate.
__ Solid (5)
__ Liquid (6)
__ Sludge (7)
__ Other (8)
INORGANIC CHEMlSTRY
Extractables
Parametc:r Rcsult6 mg/ 1
crcury
Sfk.~iu_!Tl. ·
1 Silver
I _-_ -------------
1 '
I ---------------
1 ---------------
Parameter
____ P&T:GC/MS
_ Acid:B/N Ext
_TOX
Panni.ctcr
Rc.ult6 mg/1
MICROBIOLOGY
__ (MF) Coliform Colonics/lOOmls
__ (MPN) Coliform Colonics/lOOmls
Pa.ram c. cer
~An;eni c ✓Ba. -V num
__ Cadmium
_J2hlorid_e
_,/_ r Chromium
__ Copper
__ Fluoride
1~d
_).i.anganesc
_V_ M Mrrer;,cury
___Nirrace ·
__ v "Scl·enium
Results mg/1
ORGANIC CHEMISTRY
Para.meter.
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindane
Result, mg/ 1
P=ete,;
__ Gross Alpha
__ Gross Bera
""=="--I Comroenu
c.A S <'-d-c.o w2 lfl. we I (
. 1AM 1 1 1nnn
""' i.iiru1vD Stt:TION
Total
Para.meter ,·
__ Silver
__ Sulfates
__ Zinc.
_Ph
__ Conductivity
__ ms
_TOC
Parameter
__ Mcthoxychlor
__ Toxaph=c
_2,4-D
--2,4,5-TP (silvcx)
RADIOCHEMISTRY
Rcsulu mg/1
Rcsulumg/1
Resulu PCi/1
).re Rccdv~d ------------------Date Reported -~--t-'i-z'y'-'B---=o'------------'----
),rc Extracted Date Aru.iyeed ________________ _
. . : . if 9.) . .
C .. Dcp:i.r~~n .Re:,.;ourccs
,:ision of Holth Services • 5 v (}blf /-UH •
SAMPLE ANALYSES REQUEST
Commenu €~mental
___ Groundwater (1)
Concentrate
__ Solid (5)
___ Liquid (6)
__ Sludge (7)
--<1 . ft GM /II. U/() ({
~-Surface Water (2)
__ Soil (3) .....
__ Other (4) __ Otha (8) lb JAN 11 1990
Extra eta bl cs
P2rameter
ariurn .
-+-,~dmium
Parameter
·-. _ P& T:GC/MS
__ Acid:B/N Ext.
_TOX
Para.merer
Resu Its mg/ 1
Results mg/1
MICROBIOLOGY
__ (MF) Coliform Colonies/lOOmls
__ (MPN) Coliform Colonics/lOOmls
INORGANIC CHEMISTRY SUPERFIJl\lD SECTION
Parameter
~~-enic
~num
__ Cadmium
_,.e:hloride _✓_('!Chromium
__ Copper
__ Fluoride
7fon _· Le.,d
~anese
__ Mercury
_N1crare _v_ c; s,cleniwn
Total
0, I
< 0,06C __ Zinc
__ Ph
< 0, CJ I __ Conductivity __ ms
_·_TOC
,<o.oos::
zo.ooo:L-
ORGANIC CHEMISTRY
Parameter.
_EDB
__ PCB's
__ Petroleum
__ Endrin
__ Lindanc
Resuln =g/1 Parameter
__ Methoxychlor
__ Toxaph=e
_2,4-D
--2,4,5-TP (si\vc:x)
RADIOCHEMISTRY
Results mg/1
<O,<J~
Rcsults PCi/ l
__ Gross Alpha
__ Gross Beta
Lab Number
. ., NORTH CAROLINA STA1Rle!~VID
Department of Public Safety MAR O 7 1990
Box 7220
Raleigh. NC 27695-7220
Telephone: [phone]
SUPERFUND SECTION /
_ _,::,"-·,+l""L'--'__,_(l_D _____ Date
To, __ r'-l"""', 01....11."-"'f~l.l....l.m-~...,.,.1 '~'""'_;,___~=I b=~Q=, Q=~=,.v.. __ _
FROM: __ ___.ts~. u:t-ci:.e ,._, 1,:.1.r.~ __ ,._[Y,._J,.,Ll=Q .c:d,._,19-="'-s.sGo:.• C.,._·.,,,cti:..• ____ _
ACT!ON REQUESTED ON ATTACHED:
Ncite and return
/ For your information
(need not return)
__ Pleasl(handle
__ Please answer; furnish me copy
__ As you requested
__ Route to the following
__ Please draft reply for my signature
(return attachments)
__ Please give me your comments
(return attachments)
__ Requires your approval
__ Return for filing
__ Please see me
•
,~ .... ...,-~.,,,.,-t~1•1~ 11:~I • •
IEA LABORATORY RESULTS
IEA Project #: 614-004
Client Name: NCSU-Oept. of Marine, Earth & Atmosphere
Date
Sample# Client ID Para.meter Results Analyzed
========================================================================================
1 90-HSE 11 Cyanide <0.01 mg/L 01/25/90
2 2200 Trenton Rd. cyanide <0.01 mg/L 01/25/90
3 90-Medlin-1 . Cyanide .. <0.01 mg/L 01/25/90
1 90-HSE 11 Total Phenols <0.005 mg/L 02/01/90
2 2200 Trenton Rd. Total Phenols <0.005 mg/L 02/01/90
3 90-Medlin-1 Total Phenols <0.005 mg/L --... .. 02/01/90
1 90-HSE 11 Arsenic <0.005 mg/L 02/01/90
2 2200 Trenton Rd. Arsenic <0.005 mg/L 02/01/90
3 90-Medlin-1 Arsenic <0.005 mg/L 02/01/90
1 90-HSE 11 Cadmium <0.01 mg/L 02/05/90
2 2200 Trenton Rd. Cadmium <0.01 mg/L 02/05/90
3 90-Medlin-1 Cadmium <0.01 mg/L 02/05/90
1 90-HSE 11 Chromium <0.03 mg/L 02/05/90
2 2200 Trenton Rd. Chromium <0.03 mg/L 02/05/90
3 90-Medlin-1 Chromium <0.03 mg/L 02/05/90
1 90-HSE 11 Mercury <0.0005 mg/L 02/13/90
2 2200 Trenton Rd. Mercury <0.0005 mg/L 02/13/90
3 90-Medlin-1 Mercury <0.0005 mg/L 02/13/90
1 90-HSE 11 Lead <0.005 mg/L 02/02/90
2 2200 Trenton Rd. Lead <0.005 mg/L 02/02/90
3 90-Medlin-1 Lead <0.005 mg/L 02/02/90
1 90-HSE 11 Selenium <0.01 mg/L 02/02/90
2 2200 Trenton Rd. Selenium <0.01 mg/L 02/02/90
3 90-Medlin-1 Selenium <0.01 mg/L 02/02/90
1 90-HSE 11 Silver <0.05 mg/L 02/05/90
2 2200 Trenton Rd. Silver ;<0.05 mg/L 02/05/90
3 90-Medlin-1 Silver <0.05 mg/L 02/05/90
l 90-HSE 11 Beryllium <0.01 mg/L 02/05/90
2 2200 Trenton Rd. Beryllium <0.01 mg/L 02/05/90
3 90-Medlin-l Beryllium <0.01 mg/L 02/05/90
1 90-HSE 11 Thallium <0.005 mg/L 02/01/90
2 2200 Trenton Rd. Thallium <0.005 mg/L 02/01/90 3 90-Medlin-l Thallium <0.005 mg/L 02/01/90
1 90-HSE 11 Copper <0.02 mg/L 02/05/90 2 2200 Trenton Rd. Copper <0.02 mg/L 02/05/90 3 90-Medlin-1 Copper <0.02 mg/L 02/05/90 l 90-HSE 11 Zinc 0.16 mg/L 02/05/90
2 2200 Trenton Rd. Zinc 0.10 mg/L 02/05/90 3 90-Medlin-l Zinc 1.5 mg/L 02/05/90 l 90-HSE 11 Antimony <0.20 mg/L 02/05/90 2 2200 Trenton Rd. Antimony <0.20 mg/L 02/05/90 3 90-Medlin-1 Antimony <0.20 mg/L 02/05/90 l 90-HSE 11 Nickel <0.03 mg/L 02/05/90 2 2200 Trenton Rd. Nickel <0.03 mg/L 02/05/90 3 90-Medlin-l Nickel <0.03 mg/L 02/05/90
•"114%~81tR-tltlltilllifflllwWJ 'lliMIBJ-~~-•it
l1h;I7'1 • •
IEA Sample Number:
Sample Identification:
Date Analyzed:
GC/MS PURGEABLES
EPA METHOD 624 COMPOUNDS
614-004--1
90-HSE 11
01/29/90 By: Casto
Quantitation
Limit
Number Compound (ug/L)
1 Benzene 5
2 Bromodichloromethane· .. 5
3 Bromoform 5
4 Bromomethane 10
5 Carbon tetrachloride 5
6 Chlorobenzene 5
7 Chloroethane 10
8 2-Chloroethylvinyl ether 5
9 Chloroform 5
10 Chloromethane 10
11 Dibromochloromethane 5
12 1,2-Dichlorobenzene 5
13 1,3-Dichlorobenzene 5
14 1,4-Dichlorobenzene 5
15 1,1-Dichloroethane 5
16 1,2-Dichloroethane 5
17 1,1-Dichloroethene 5
18 Total-1,2-Dichloroethene 5
19 1,2-Dichloropropane 5
20 cis-1,3-Dichloropropene 5
21 trans-1,3-Dichloropropene 5
22 Ethylbenzene 5
23 Methylene chloride 5
24 1,1,2,2-Tetrachloroethane 5
25 Tetrachloroethene i 5
26 Toluene 5
27 1,1,1-Trichloroethane 5
28 1,1,2-Trichloroethane 5
29 Trichloroethene 5
30 Trichlorofluoromethane 5
31 Vinyl Chloride 10
Comments:
BQL = Below Quantitation Limit
FORM 624 Rev. 101989
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL ···
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
WMWliMtlt~-7titUNI/WM-B'9~.-
1~·'1 • •.
GC/MS PURGEABLES
EPA METHOD 624 COMPOUNDS
IEA Sample Number: 614-004-2
Sample Identification: 2200 Trenton Rd.
01/29/90 Date Analyzed:
Number Compound
1 Benzene
2 Bromodichloromethane
3 Bromoform
4 Bromomethane
5 carbon tetrachloride
6 Chlorobenzene
7 Chloroethane
8 2-Chloroethylvinyl ether
9 Chloroform
10 Chloromethane
11 Dibromochloromethane
12 1,2-Dichlorobenzene
13 1,3-Dichlorobenzene
14 1,4-Dichlorobenzene
15 1,1-Dichloroethane
16-1,2-Dichloroethane
17 1,1-Dichloroethene
18 Total-1,2-Dichloroethene
19 1,2-Dichloropropane
20 c is-1, 3-Dichloropropent~
21 trans-1,3-DichloropropHne
22 Ethylbenzene
23 Methylene chloride
24 1,1,2,2-Tetrachloroethane
25 Tetrachloroethene
26 Toluene
27 1,1,1-Trichloroethane
28 1,1,2-Trichloroethane
29 Trichloroethene
30 Trichlorofluoromethane
31 Vinyl Chloride
Comments:
BQL = Below Quantitation Limit
FORM 624 Rev. 101989
By: Casto
Quantitation
Limit
(ug/L)
5
5
5
10
5
5
10
5
5
10
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
10
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL''·
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
l'ltfirliilM'ilt:awq"Mf.WiNNl\~M .. 1~~UNMW®M.ffiiM m • •
IEA Sample Number:•
Sample Identification:
Date Analyzed:
GC/MS PURGEABLES
EPA METHOD 624 COMPOUNDS
614-004-3
90-Medlin-l
01/29/90 By: Casto
Quantitation
Limit
Number Compound (ug/L)
1 Benzene 5
2 Brornodichlorometharie 5
3 Bromoform 5
4 Bromomethane 10
5 Carbon tetrachloride 5
6 Chlorobenzene 5
7 Chloroethane 10
8 2-Chloroethylvinyl ether 5
9 Chloroform 5
10 Chloromethane 10
11 Dibrornochloromethane 5
12 1,2-Dichlorobenzene 5
13 1,3-Dichlorobenzene 5
14 1,4-Dichlorobenzene 5
15 1,1-Dichloroethane 5
16 1,2-Dichloroethane 5
17 1,1-Dichloroethene 5
18 Total-1,2-Dichloroethene 5
19 1,2-Dichloropropane 5
20 cis-1,3-Dichloropropene 5
21 trans-1,3-Dichloropropene 5
22 Ethylbenzene 5
23 Methylene chloride 5
24 1,1,2,2-Tetrachloroethane 5
25 Tetrachloroethene 5
26 Toluene 5
27 1,1,1-Trichloroethane 5
28 1,1,2-Trichloroethane 5
29 Trichloroethane 5
30 Trichlorofluoromethane 5
31 Vinyl Chloride 10
Comments:
BQL Below Quantitation Limit
FORM 624 Rev. 101989
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL'-.
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
llill~lllllilllit\\f.,"1B11Wl~Wtti& ... ~MR®t~
l~I • •
IEA Sample Number:
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
Sample Identification:
614-004--1
90-HSE 11
01/30/90
02/14/90
Date Extracted:
Date Analyzed: By: Schemmer
Quantitation
Limit
Number Compound (ug/L)
\
1 Acenaphthene 10
2 Acenaphthylene 10
3 Anthracene 10
4 Benzo(a)anthracene 10
5 Benzo(a)pyrene 10
6 Benzo(b)fluoranthene 10
7 Benzo(g,h,i)perylene 10
8 Benzo(k)fluoranthene 10
9 bis(2-Chloroethoxy)methane 10
10 bis(2-Chloroethyl)ether 10
11 bis(2-Chloroisopropyl)ether 10
12 bis(2-Ethylhexyl)phthalate 10
13 4-Bromophenyl phenyl ether 10
14 Benzyl butyl phthalate 10
15 2-Chloronaphthalene 10
16 4-Chlorophenyl phenyl ether 10
17 Chrysene 10
18 Dibenzo(a,h)anthracene 10
19 1,2-Dichlorobenzene 10
20 1,3-Dichlorobenzene 10
21 1,4-Dichlorobenzene 10
22 3,3'-Dichlorobenzidine 10
23 Diethyl phthalate 10
24 Dimethyl phthalate 10
25 Di-n-butylphthalate 10
26 2,4-Dinitrotoluene 10
27 2,6-Dinitrotoluene 10
28 Di-n-octylphthalate 10
29 Fluoranthene 10
30 Fluorene 10
31 Hexachlorobenzene 10
32 Hexachlorobutadiene 10
33 Hexachlorocyclopentadiene 10
34 Hexachloroethane 10
35 Indeno(l,2,3-cd)pyrene 10
36 Isophorone 10
37 Naphthalene 10
FORM 625B ( 1) Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
i BQL
BQL
BQL
BQL
BQL
BQL
,. BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
IEA Sample Number:
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
Sample Identification:
614-004--l
90-HSE .l1
01/30/90
02/14/90
Date Extracted:
Date Analyzed: By: Schemmer
Quantitation
Limit
Number Compound (ug/L)
'· 38 Nitrobenzene lO
39 N-Nitroso-di-n-propylamine 10
40 N-Nitrosodiphenylamine 10
41 Phenanthrene 10
42 Pyrene 10
43 1,2,4-Trichlorobenzene 10
44 Benzidine so
45 N-Nitrosodimethylamine 10
Comments:
. BQL ; Below Quantitation Limit
FORM 625B (2) Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
IWttMttttFt11WIIW~•~.,,,,,,,,,,,,~Vli
i~I • •
GC/MS ACID EXTRACTABLES
EPA METHOD 625 COMPOUNDS
IEA Sample Number: 614-004-1
90-HSE 11
01/30/90
02/14/90
Sample Identification:
Date Extracted:
Date Analyzed:
Number Compound
\
1 4-Chloro-3-methylphenol
2 2-Chlorophenol
3 2,4-Dichlorophenol
4 2,4-Dimethylphenol
5 2,4-Dinitrophenol
6 2-Methyl-4,6-dinitrophenol
7 2-Nitrophenol
8 4-Nitrophenol
9 Pentachlorophenol
10 Phenol
11 2,4,6-Trichlorophenol
Comments:
By: Schemmer
Quantitation
Limit
(ug/L)
.10
10
10
10
50
50
10
50
50
10
10
BQL ; Below Quantitation Limit
FORM 625A Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL --, ..
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
/
1111.-11111m·-~11.1u~11i1,,19,,,,,w111:ffilildlD1Dl~ll
~I • . •
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
IEA Sample Number: 614-004-2
Sample Identification: 2200 Trenton Rd,
01/30/90
02/14/90
Date Extracted:
Date Analyzed:
Number
l
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
Compc;,und
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)ftuoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Benzyl butyl phthalate
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
Di-n-butylphthalate
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
Naphthalene
FORM 625B (1) Rev. 050589
By: O'Toole
Quantitation
Limit
(ug/L)
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL.
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
IEA Sample Number:
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
614-004-2
Sample Identification: 2200 Trenton Rd.
01/30/90
02/14/90
Date Extracted:
Date Analyzed: By: O'Toole
Quantitation
Limit
Number Compound (ug/L)
'\
38 Nitrobenzene 10
39 N-Nitroso-di-n-propylamine 10
40 N-Nitrosodiphenylamine 10
41 Phenanthrene 10
42 Pyrene 10
43 1,2,4-Trichlorobenzene 10
44 Benzidine 50
45 N-Nitrosodimethylamine 10
Comments:
BQL ~ Below Quantitation Limit
FORM 625B (2) Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
:l,IIIN~,!811\lliMl-:\IIW'U. 'lltrlJ!'1~1Ri/llllllitt!UMMtM
11;r::1 • •
.,
GC/MS ACID EXTRACTABLES
EPA METHOD 625 COMPOUNDS
IEA Sample Number: 614-004-2
Sample Identification:
Date Extracted:
2200 Trenton Rd.
01/30/90
Date Analyzed: 02/14/90 By: O'Toole
Quantitation
Limit
Number Compound (ug/L)
' 1 4-Chloro-3-methylphenol 10
2 2-Chlorophenol 10
3 2,4-Dichlorophenol 10
4 2,4-Dirnethylphenol 10
5 2,4-Dinitrophenol so
6 2-Methyl-4,6-dinitrophenol 50
7 2-Nitrophenol 10
8 4-Nitrophenol 50
9 Pentachlorophenol 50
10 Phenol 10
11 2,4,6-Trichlorophenol 10
Comments:
BQL = Below Quantitation Limit
FORM 625A Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL ~ .......
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
-----.--~.-~~~&~ 1~1 •· •
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
IEA Sample Number: 614-004-3
90-Medlin-l
01/30/90
02/14/90
Sample Identification:
Date Extracted:
Date Analyzed:
Number
l
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
Compound
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl)ether
bis(2-Chloroisopropyl)ether
bis(2-Ethylhexyl)phthalate
4-Bromophenyl phenyl ether
Benzyl butyl phthalate
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenzo(a,h)anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
Di-n-butylphthalate
·2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(l,2,3-cd)pyrene
Isophorone
Naphthalene
FORM 625B (l) Rev. 050589
By: O'Toole
Quantitation
Limit
(ug/L)
10
10
10
10
10
10
10
10
10
10
10
10
10
-10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Results
Concentration
(ug/L)
. BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
•• ,.,,,,,,,,,.~,.!BJ,'Na~lffii~~~¥'':WWWII
1r;r:@1 • · •
IEA Sample Number:
GC/MS BASE/NEUTRAL EXTRACTABLES
EPA METHOD 625 COMPOUNDS
Sample Identification:
614-004-3
90-Medlin-l
01/30/90
02/14/90
Date Extracted:
Date Analyzed: By: O'Toole
Quantitation
Limit
Number Compound (ug/L)
' 38 Nitrobenzene 10
39 N-Nitroso-di-n-propylamine 10
40 N-Nitrosodiphenylamine 10
41 Phenanthrene 10
42 Pyrene 10
43 1,2,4-Trichlorobenzene 10
44 Benzidine 50
45 N-Nitrosodimethylamine 10
Comments:
BQL ; Below Quantitation Limit
FORM 625B (2) Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
GC/MS ACID EXTRACTABLES
EPA METHOD 625 COMPOUNDS
IEA Sample Number:
sample Identification:
614-004-3
90-Medlin-1
01/30/90
02/14/90
Date Extracted:
Date Analyzed:
Number Compound
' 1 4-Chloro-3-methylphenol
2 2..:chlorophenol
3 2,4-Dichlorophenol
4 2,4-Dimethylphenol
5 2,4-Dinitrophenol
6 2-Methyl-4,6-dinitrophenol
7 2-Nitrophenol
8 4-Nitrophenol
9 Pentachlorophenol
10 Phenol
11 2,4,6-Trichlorophenol
Comments:
By: O'Toole
Quantitation
Limit
(ug/L)
10
10
10
10
50
50
10
50
50
10
10
BQL = Below Quantitation Limit
FORM 625A Rev. 050589
Results
Concentration
(ug/L)
BQL
BQL --..
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
-~....,ft,ll)~ .. g)iq,JDE!'B4¥W~Mlllil
1rr;'J • •
IEA Sample Number:
Sample Identification:
Date Analyzed:
PESTICIDES/ PCBs
SW-846 METHOD 8080
614-004-1
90-HSE 11
02/03/90 By: Hollenbach/Austin
Quantitation Results
Number
1
2
Compound
alpha-BHC
beta-BHC
3 delta-BHC
4 gamma-BHC (Lindane)
5 Heptachlor
6 Aldrin
7 Heptachlor epoxide
8 Endosulfan I
9 Dieldrin
10 4,4'-DDE
11 Endrin
12 Endoeulfan II
13 4,4'-DDD
14 Endosulfan sulfate
15 4, 4' -DDT
16 Methoxychlor
17 Toxaphene
18 Aroclor 1016
19 Aroclor 1221
20 Aroclor 1232
21 Aroclor 1242
22 Aroclor 1248
23 Aroclor 1254
24 Aroclor 1260
25 Chlordane (technical)
26 Endrin aldehyde
Additional Compounds:
27
28
29
Comments:
Endrin ketone
alpha-Chlordane
gamma-Chlordane
BQL; Below Quantitation Limit
FORM 8080 Rev. 052589
Limit
(ug/L)
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.05
0.10
0.10
0.10
0.10
0.10
0.10
0.10
0.50
1.0
0.50
0.50
0.50
0.50
0.50
1.0
1.0
0.50
0.10
0.10
0.50
0.50
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
i BQL
BQL
BQL
IEA Sample Number:
PESTICIDES/ PCBs
SW-846 METHOD 8080
614-004-2
Sample Identification: 2200 Trenton Rd.
Date Analyzed: 02/03/90 By: Hollenbach/Austin
Quantitation Results
Number
1
2
3
Compound
alpha-BHC
beta-BHC
delta-BHC
4 gamma-BHC (Lindane)
5 Heptachlor
6 Aldrin
7 Heptachlor epoxide
8 Endosulfan I
9 Dieldrin
10 4,4'-DDE
11 Endrin
12 Endosulfan II
13 4,4'-DDD
14 Endosulfan sulfate
15 4,4'-DDT
16 -Methoxychlor
17 Toxaphene
18 Aroclor 1016
19 Aroclor 1221
20 Aroclor 1232
21 Aroclor 1242
22 Aroclor 1248
23 Aroclor 1254
24 Aroclor 1260
25 Chlordane (technical)
26 Endrin aldehyde
Additional Compounds:
27
28
29
comments:
Endrin ketone
alpha-Chlordane
gamma-Chlordane
BQL ~ Below Quantitation Limit
FORM 8080 Rev. 052589
Limit
(ug/L)
0.05
o.os
0.05
o.os
0.05
0.05
0.05
0.05
0.10
0.10
0.10
0.10
0.10
0.10
0.10
a.so
1.0
a.so
0.50
a.so
a.so
a.so
1.0
1.0
a.so
0.10
0.10
a.so
a.so
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
•~·•--•R111ur11""ifflW'i.w~~w-'t1~WMw:
l!:rrl • . •
IEA Sample Number:
Sample Identification:
Date Analyzed:
PESTICIDES/ PCBs
SW-846 METHOD 8080
614-004-3
90-Medlin-1
02/03/90 Sy: Hollenbach/Austin
Quantitation Results
Number
1
2
Compound
alpha-BHC'
beta-BHC
3 delta-BHC
4 gamma-BHC (Lindane)
5 Heptachlor
6 Aldrin
· 7 Heptachlor epoxide
8 Endosulfan I
9 Dieldrin
10 4,4'-DDE
11 Endrin
12 Endosulfan II
13 4, 4' -DOD
14 Endosulfan sulfate
15 4,4'-DDT
16 Methoxychlor
17 Toxaphene
18 Aroclor 1016
19 Aroclor 1221
20 Aroclor 1232
21 Aroclor 1242
22 Aroclor 1248
23 Aroclor 1254
24 Aroclor 1260
25 Chlordane (technical)
26 Endrin aldehyde
Additional CompoundJ,
27
28
29
Comments:
Endrin ketone
alpha-Chlordane
gamma-Chlordane
BQL = Below Quantitation Limit
FORM 8080 Rev. 052589
Limit
(ug/L)
0,05
0,05
o.os
o.os
o.os
D.05
o.os
o.os
0.10
0.10
0.10
0.10
0.10
0.10
0.10
o.so
1.0
a.so
o.so
0.50
a.so
a.so
1.0
l.O
o.so
0.10
0.10
o.so
a.so
Concentration
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
•• North Carolina Department of Human Resour·ces Division of Health Services
Laboratory Section
P .0. Box 28047, Raleigh, N. C. 27611 -
Environmental Sciences Analysis Report
Name of OWner, Patient
or Supply: ...,r>,.,,j"'C"'S='-"'U'--________ _
Address:(.,\~,--'\(_ t\o:.I \ ) N C.2,L)
County: Wc;..\<-"-
Report to:-'='-'---'--"""--'-'-''-'---'--'.u...'-'+-----
Addres s: _-£-...L;Hd-~~µ;J.1¥"'---h-'"'-.__-
Date
Collected . By: __::i..<.!._L;.....'-'=::s._.!...b'---<'-----
Analysis Desired: vOC:s s1.1c.h c~:-,±o\ 11e.r1el pc..r'1>-d',-ox_,,_,-,e./-lc:r
Laboratory Sample Sample Description or Remarks Number Number Results In
\
0 02r.:::07 .... , ... ~ . .,; ~ ~c.s 1 1 A c; c G 1 ·-1 LJ-SU. ATTACHW SHEETl!:l .
Nr \!\SGfG)-14
' \ -
~ 1,,--,-, ,. r-, "' -' \ \, , I < •V
• -~ -V \. ,... )\_/I )\:::'....J Li J J ' -~ , SO ,... -') 8 NG U'l3G c B )--' 02. SU ATTACHED SHEET(S)
., .«(.;,~\_; '
'
• NC<;\) 6G:i( 8)-~D2 . . . . .
.
.
Date Received )5 -;J!:)·89 .'<(1, Date Reported __ ..,,.-'---i-"'-'---"'-,f-----
Date Extracted-'.'--------------Date Analyzed . ..:\f__,/JG.<..LJ'P'~L,.,-'f-'2!:.:<..J.-:::;fL.:...:L---..,,.--
Repor tad By: -W~~L...£.E~:::::.:.:::::..:=~-
DHS Form 2364 Revised (5/89) Laboratory
..
• •
STATE LABOAATORY Of PUBLIC ATH • · D ON o EALTH SERVICES, N. C. DEPARTIIE9f' HUS RESOURCES
ooratory No.
· r.O. BOX·28047 -306.N. WILMINGTON ST, RALEIGH, N.C. 27611 9'02 :fo'J . PURGEABLE COMPOUNDS Date of Analysis ___.~c=,/4'-"-'-'f'---_
COMPOUND. µg/1 · COMPOUND . --
Di ch lorodi fluoranethane . , Ch 1 orobenzene Ch16roiettiane Ethvlbenzene ,Vi nvl .•Ch Jori de 1 1 1 2-Tetrachloroethane Braranethane ,,. . ·+>-.
' · o-Xvlene -Ch 1 oroottiane •' ·. ·.·.·'4 .. -~{,: .·. ' .. m-Xvlene Tri ch lorofluoranethane. . ,
0-Xvlene ✓1; 1~Dich 1oroetnv1ene •···· ... ~. , .. ,, .. ,,
Stvrene· Hethvleiii('Chloride, .' ':. /{,.,, qq4 .. ·' Bromofonn tert-BtJtvl Hethvl Ether . . I;·, I ]benzene (Transl l .2-0ich loroethvlene ,· 1 1 2 2-Tetrachloroethane I 1 ether .. .. \ '. e•.-• ·= ,_._, ·-Braoobenzene l . 1.:.iii'i:ti l oroethane'.~•-• ';'· •-· .. ' n-Pr:oovlbenzene 2-0i dilii . "•) ~ V': -.. . ·2 ne . 1 2 3-Trichlornnrnnane · (Ci s);•f;21:oich loroethvlene· ,. :'·, ·'· I . :'-., ~•,A .2~1orotoluene . . / ?. r, K . . 1 Chlorofonn 1.3 5 Trimeth.vlbenzene (BCH) Brcmochloranethane ' ' 11 4-ailorotoluene ✓l ·l. l-Trichloroethane CTertl Butvl Benzene 1, 1-Dichlo ne ' v' Pentach loroethane ✓Cartxini' Tetrachloride ' t:' ~ /') 1,2,4-Trimeth~lbenzene --✓Benzene ' '''"'" · (Seel Butvl Benzene ✓1 2-Dichloroethane .' ' J o-I 1 toluene ✓Tri ch loroethvlene ,' 2.j 52 ' l 2-0ichlo, ne ~/ (' q9 ... l 3-Dichlorobenzene
• ✓l. 4-0ich lorobenzene Branodichloranethane ' A _ n-BtJtvlbenzene• Di braroi,ethane V 1 ·2-0ichlorobenzene Toluene . " ·,;74 . ' ,.rs is li'-2. Ch lon:ii 1 Ether l l 2-Trich loroethane .. ' 'I r~ ;J'.f 1.2-0itiroro-3 Chloroorooane -
C ':19. Tetrachlciroethene
l .3-0ichlo: .... ·ne _, --.: ... J.).:~· . "l .2A:'.Trichloroberizene
·Hexachlorobutadiene Dibronochloranethane -v N•nhthalene· 1.2-0ibronr:iethane CEOBl .. I, r, LJ..rf· . " l.2:3~Trichlorobenzene l -Ch lorohexane' ,. I) . .. .. . ~i-J:½Lf.etk . IL} ,, C/'J._
'' .. . -. . ' ·-----·--·
' ' . . IIDL .. lliniM Detection Limit for·water (EPA Method 502.2), is 1.0 µg/1.
J .. Estimated value. K .. Actual value is kriown to.be _less than. value given. . L .. Actual value is· known to be·greater-than value given. U -llaterial was analyzed for but not detected. NA -Not analyzed ... · 1/ -Tentative identification.· ✓ -Re~u I a led ·voc 1 Tr1halonethane· : ~, ....
N.C. Division of Health Services OHS 3068-0 ( 1/89 Laboratory)
µg/1 -
) '7 ,::.
3 '1. ., ,
J ,L '<7 ..
' ' .
,/ j :3/./1
A
I" "
LL
7
'~. "i
I
•"
'
L
11 I I
STATE LABORATORY OF PUBLIC HEALTH
. IJ09l047 -306 N._ WILMINGTON ST, ~H, . 27611
,oratory, No.
DI.ON -EALTH SERVICES, N.C. DEPART11E!--HU.RESOORCES
{JrJ,2_501 . PURGEABLE COMPOUNDS · _ Date of Analysis
' -C(l,HPOUND µg/1 COMPOUND
.
-tlichlorodifluoranethane. I Ch 1 orobenzene ·
Chlciranethane Ethvlbenzene
>'Vinvl I Chloride 1 -l l 2 Tetrachloroethane
eraii'i,;,thdne n.:xvlene
Chloroethane >
m-Xvlene
Trichlorofluoranethane o~Xvlene
✓1.1-0ichloroethvlene stvrene
Hethvlene Chlor.ide Braoofonn -
tert--Butvl' Methvl Ether I ]benzene
/Transl 1.2-0ichloroethvlene 1 1 2 2-Tetrachloroethane
I l ·ether Braoobenzene
1 1-Dichloroethane· n-P......;.., !benzene
2.2-Dichlo ne I 1,2,3-Trichloi:QQrwane
(Cisl 1.2-0ichloroethvlene . 2--Chlorotoluene
Chloroform 1 3.5-Trimethvlbenzene
\BC/1) Brcmochloranethane 4--Ch lorotoluene
✓l :1 1-Trichloroethane /Tertl Butvl Benzene 1. 1 Dich lo, ne Pentachloroethane ✓Cdrbon Tetrachloride 1,2,4-Trimeth~lbenzene --✓Benzene (Seel Butyl Benzene ✓1,2-Dichloroethane n-1 !toluene ✓Trichloroethvlene 1 3-0ichlorobenzene 1 2-Dichlo ne ✓l 4-0ichlorobenzene Bratndichloranethane n--Butvlbenzene Dibraranethane 1.2-0i ch lorobenzene Toluene ..L.r-~ (!.P , /Bis' 2 Chloroi l Ether 1.1.2-Trichloroethane . 1.2-0ibraoo 3 Chlo, ne -
Tetrachloroethene l 2 4-Trichlorobenzene 1.3-Dlchlo~-ne Hexachlorobutadiene Dibrarochloranethane N•~hthalene·
1 .2-Dibmroettiane (EDBl 1.2.3-Trichlorobenzene
1-Ch 1 orohexane -
-,t1.U ,/ .,IL . . J.rv...c.e....., --'f -
--
IIOL --Hininun Detection Limit for water (EPA Method 502.2), is 1.0 µg/1.
J -Estimated value.
K -Actual value is known to be less than value given. L --Actual value is known to be greater than value given. U -Material was analyzed for but not detected. NA -Not analyzed.
1/ -Tentative identification. ✓ .. Re~ulated voe
I -Tri ha lane thane
N.C. Division -of Health Services OHS 3068-0 ( 1/89 Laboratory)
µg/1
I
~
-ir11 ft e__
>
.
/