NCD980557656_19970829_NC State University (Lot 86 Farm Unit 1)_FRCBERCLA SAP QAPP_Task 2 - Bioattenuation Screening Analysis Groundwater Natural Attenuation Demonstration (Revision 0)-OCR

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TASK 2 -BIOATTENUATION SCREENING ANALYSIS
GROUNDWATER NATURAL ATTENUATION DEMONSTRATION
LOT 86 SUPERFUND SITE
Submitted to:
North Carolina State University
Environment, Health & Safety Center
Campus Box 8007
Raleigh, North Carolina 27695-7212
NCSU No. 218-75-99-0000
7721 Six Forks Road, Suite 136
Raleigh, North Carolina 27615
(9 I 9) 676-0665
August 29, 1997
Revision 0
Project 97 I 91
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RECEIVED
JAN 3 0 1998
TASK 2-BIOATTENUATION SCREENING a:M'aElYSlsSECTION
GROUNDWATER NATURAL ATTENUATION DEMONSTRATION
LOT 86 SUPERFUND SITE
August 29, 1997
Submitted to:
North Carolina State University
Environment, Health & Safety Center
Campus Box 8007
Raleigh, North Carolina 27695-7212
Prepared by:
GEI Consultants, Inc.
7721 Six Forks Road, Suite 136
Raleigh, North Carolina 27615
[phone]
Project 97191
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EXECUTIVE SUMMARY
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997
North Carolina State University (NCSU) engaged GEi Consultants, Inc. (GEi) to evaluate the
potential for natural attenuation processes to remediate groundwater affected by release of
chlorinated volatile organic compounds (VOCs) from the Lot 86 Superfund Site in Raleigh, North
Carolina. The predominant compounds found in groundwater at the site are chloroform, methylene
chloride, benzene, carbon tetrachloride, and trichlorocthene.
The U.S. Environmental Protection Agency (EPA) has issued a Record of Decision (ROD) tha.t calls
for NCSU to pump contaminated groundwater until prescribed groundwater remedial objectives are
achieved. The ROD allows deferring implementation of groundwater pumping for two years, during
which time NCSU may submit information to EPA providing evidence that groundwater
contamination is being reduced by naturally-occurring processes. If the evidence is persuasive, EPA
will consider changing the 'selected groundwater remedy.
The scope of the groundwater natural attenuation project includes the following tasks: 1 A) preparing
work plans for groundwater sampling and analysis; 1B) collecting and analyzing groundwater
samples from 24 existing monitoring wells; and 2) applying the results of the analyses to a
Bioattenuation Screening Process contained in a draft document developed by the U.S. Air Force,
Technical Protocol for Evaluating Natural Attenuation of Chlorinated Solvents in Groundwater (the
Technical Protocol). The Bioattenuation Screening Process is an initial step that allows investigators
to determine, with minimal investment in data collection, whether natural bioattenuation is likely
to be a viable remedial alternative. The process uses a scoring system in which parameters are
awarded points based on their potential for enhancing conditions for natural attenuation and on
indications that natural attenuation is occurring. If the screening score for the site indicates that
natural attenuation appears to viable, NCSU may proceed with the following additional tasks: 3)
simulating contaminant transport and bioattenuation using a two-dimensional computer model,
BIOPLUMEII; and 4) preparing documentation presenting a weight-of-evidence demonstration that
natural attenuation is capable of achieving remedial objectives for the site.
GEi has completed tasks I A through 2 above. This report presents the results of the application of
the Bioattenuation Screening Process using the results of the analyses of groundwater samples. The
samples were categorized into the following zones for conducting the screening: wells in the most
contaminated portion of the aquifer; wells in the dissolved contaminant plume downgradient of the
most contaminated portion of the aquifer; and wells upgradient of the source area and lateral to the
contaminant plume. Results of the analyses were sorted according to the zones, and a representative
result was determined for each parameter of analysis for each zone. The representative results were
then applied to the scoring system, and a total site biodegradation score was determined.
The total site biodegradation score indicates there is adequate evidence of biodegradation of
chlorinated organics at the site to warrant more detailed evaluation of natural attenuation including
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 ii
bioattenuation. The conditions expressed in the results for dissolved oxygen, dissolved hydrogen,
total organic carbon, BTEX (benzene, toluene, ethylbenzene, and xylenes), nitrate, sulfate,
alkalinity,· and chloride concentrations, and pH, indicate that bioattenuation of chlorinated
compounds. should be occurring in the zone of the highest groundwater contaminant
concentrations.
Apparently conflicting with otherwise strong evidence that bioattenuation is occurring, products
of bioattenuation of chlorinated compounds (such as the dissolved gases methane, ethane, and
ethene) and intermediate "daughter-product" chlorinated compounds (such as dichloroethenes,
vinyl chloride, chloroethane, and chlorobenzene) were, with a few exceptions, absent in
groundwater at the site. Additional investigation or inquiry may be warranted to account for this
apparent conflict.
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TABLE OF CONTENTS
EXECUTIVE SUMMARY
LIST OF TABLES
LIST OF FIGURES
LIST OF APPENDICES
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997
l. INTRODUCTION ...................................................... l
l. l Purpose and Scope .................................................. l
l .2 Authorization ...................................................... 2
2. SITE BACKGROUND ................................................... 3
3. THE TECHNICAL PROTOCOL FOR EVALUATING
NATURAL ATTENUATION ............................................. 5
3.l Overview of Natural Attenuation ...................................... 5
3.2 Natural Attenuation of Chlorinated Aliphatic Hydrocarbons ................. 5
3.3 Demonstration of Natural Attenuation of Chlorinated Aliphatic Hydrocarbons ... 6
3.4 The Technical Protocol's Bioattenuation Screening Process ................. 7
4. GROUNDWATER SAMPLING AND ANALYSES CONDUCTED
FOR BIOATIENUATION SCREENING .................................... 9
5. APPLICATION OF THE BIOA TTENUA TION
SCREENING PROCESS TO THE SITE .................................... 11
6. EVALUATION OF THE RESULTS ....................................... 13
7. CONCLUSIONS ....................................................... 17
REFERENCES ........................................................... 20
REFERENCES
TABLES
FIGURES
APPENDICES C:\DOCS2\PROJECTS\9719 l\REl'OR 1\A TTENUA.Rl'l\cf
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LIST OFT ABLES
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, I 997
1. Groundwater Potentiometric Surface and Monitoring Well Screen Elevations
2. Groundwater Quality Data Sorted and Reduced by Biodegradation Zone
· 3. Bioattenuation Score Sheet Completed for the Site
LIST OF FIGURES
1. Bioattenuation Screening Process Flow Chart
2. Site Map, Groundwater Contours, and Biodegradation Zones
LIST OF APPENDICES
A. Results of Task 1 B Groundwater Sampling and Analysis
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 I
I. INTRODUCTION
1.1 Purpose and Scope
North Carolina State University (NCSU) is evaluating the potential for natural attenuation processes
to remediate groundwater affected by release of chlorinated volatile organic compounds (VOCs)
from the Lot 86 Superfund Site in Raleigh, North Carolina. The predominant compounds found in
groundwater at the site are chloroform, methylene chloride, benzene, carbon tetrachloride, and
trichloroethene.
The U.S. Environmental Protection Agency (EPA) has issued a Record of Decision (ROD) that calls
for NCSU to pump contaminated groundwater until prescribed groundwater remedial objectives are
achieved. The ROD allows deferring implementation of groundwater pumping for two years, during
which time NCSU may submit information to EPA providing evidence that groundwater
contamination is being reduced by naturally-occurring processes. If the evidence is persuasive, EPA
will consider changing the selected groundwater remedy.
NCSU, under contract with GEi Consultants, Inc. (GEi), is evaluating whether subsurface conditions
at the site are conducive to natural attenuation and whether there is evidence that natural attenuation
is in process. The basis for the evaluation procedure is a Bioattenuation Screening Process contained
in a draft document developed by the U.S. Air Force, Technical Protocol.for Evaluating Natural
Attenuation of Chlorinated Solvents in Groundwater (the Technical Protocol). The natural
attenuation demonstration project for the Lot 86 Superfund Site is organized as follows:
Task IA
Task 1 B
Task 2
Task 3
Task4
Sampling and Analysis, Health and Safety, and Quality Assurance
Project Plan
Sampling and Analysis Implementation
Screening Analysis
Modeling
Complete Natural Attenuation Demonstration
Task I A was completed with submission of the Sampling and Analysis Plan (GEi, 1997a), the
Quality Assurance Project Plan (GEi, 1997b), and the Health and Safety Plan (appended to the
Sampling and Analysis Plan), all dated May 9, 1997. Task I B was completed with submission of
a report dated August 5, 1997 (GEi, 1997c), consisting of data tables providing results of field
measurements and laboratory analyses conducted on groundwater samples from the site, as
recommended by the Technical Protocol for evaluating natural attenuation of chlorinated compounds
in groundwater.
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 2
Task 2 has been completed by evaluating whether biodegradation of chlorinated compounds is
occurring per the Bioattenuation Screening Process (summarized in Section 3.4 of this report and
described,in detail in Section 2.2.2 of the Technical Protocol), using the data collected under Task
I B. The results of this evaluation, which are presented in this report, provide a basis for deciding
whether natural attenuation has at least the potential to reduce concentrations of chlorinated
compounds in groundwater to below remedial objectives before transported contaminants reach
receptors. If such potential is demonstrated, NCSU may choose to proceed with more in-depth
· evaluation of natural attenuation at the site, including: I) two-dimensional modeling of contaminant
transport in groundwater (Task 3) and, 2) using a weight-of-evidence approach, demonstrate that
natural attenuation processes will reduce contaminant concentrations such that remedial objectives
will be achieved without active groundwater remediation (Task 4).
1.2 Authorization
This work was authorized by NCSU Purchase Order No. P00655490, dated March 25, 1997.
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2. SITE BACKGROUND
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 3
The North Carolina State University (NCSU) Lot 86 Superfund Site received solvents, pesticides,
heavy metals, acids, and some low-level radioactive laboratory wastes from 1969 to 1980. The
wastes were placed in 22 ten-foot-deep trenches of various lengths, totaling 2,000 feet. Groundwater
in the area of the site contains volatile organic compounds (VOCs), principally chloroform,
methylene chloride, benzene, carbon tetrachloride, and trichloroethene. Lower concentrations of
semi-volatile organic compounds and pesticides also have been detected in groundwater.
Contaminant concentrations are higher in the shallow aquifer than in the bedrock aquifer and
decrease with distance from the site.
NCSU's Department of Marine, Earth, and Atmospheric Sciences began monitoring the site in 1981.
The site was proposed for listing on the National Priorities List (NPL) in October 1984 and was
listed on the NPL in June 1986. The U.S. Environmental Protection Agency (EPA) began
investigating the site in 1987, and NCSU began a remedial investigation/feasibility study (Rl/FS)
of the site in I 992.
The RI focused on confirming the findings of earlier groundwater investigations, using
methodologies that conformed to EPA Region IV protocols (Brown and Caldwell, 1994 ). The FS
examined a range of relatively conventional site remediation approaches, including, for groundwater,
institutional action, groundwater treatment, and biotreatment, and, for subsurface soils, institutional
action, containment and capping, soil vapor extraction, incineration, and low-temperature thermal
desorption. The evaluation of alternatives in the FS did not demonstrate that one alternative was
preferable to the others (Brown and Caldwell, 1995).
Following completion of the RI/FS, NCSU in 1995 undertook an additional investigation to evaluate
the content of the waste in the trenches, obtain updated groundwater quality data, and model the
transport and biodegradation of four primary groundwater contaminants. The investigation
detern1ined the following: I) free and containerized liquid-phase chemical wastes remain in the
trenches; 2) the wastes in the trenches continue to serve as a significant source of contaminants that
can be released to groundwater; 3) after the source materials have been removed or stabilized, it is
possible that the groundwater contaminant plume could be adequately controlled by natural
biodegradation processes; and 4) the extent of the plume would be significantly larger than observed
if not for the attenuating effects of contaminant biodegradation (S&ME, 1996). Based on the these
findings, NCSU in 1996 evaluated natural attenuation as a remedial approach (NCSU, 1996a) and
prepared a revised FS that examined, among other alternatives, in-place stabilization of the trench
materials and natural attenuation of groundwater contaminants (NCSU, 1996b). The earlier FS did
not examine either of these alternatives, and the revised FS ranked these alternatives highest among
all the alternatives.
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, I 997 4
EPA issued its Record of Decision (ROD) for the site in September 1996 (EPA, 1996). The ROD
calls for the response action for groundwater to be pumped and treated until groundwater remedial
objectives are attained throughout the contaminant plume. This action was estimated to require 30
years. The ROD allows delay of the groundwater remedy for two years (until September 1998),
during which time EPA will consider new evidence that NCSU may submit demonstrating that
"reduction of groundwater contamination is occurring at the site by means of natural processes. If
analytical results such as but not limited to a decrease of groundwater contamination or the existence
of breakdown products of the original contaminants is presented, EPA will consider a change in
remedy." The North Carolina Division of Waste Management concurred with this approach,
provided that natural attenuation is evaluated using appropriate guidance, such as that developed by
the U.S. Air Force Center for Environmental Excellence, Technical Protocol for Evaluating Natural
Attenuation of Chlorinated Solvents in Ground Water (Draft-Revision 1) (the Technical Protocol)
(Wiedemeier et al., 1996).
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3.
3.1
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 5
THE TECHNICAL PROTOCOL FOR EVALUATING NATURAL ATTENUATION
Overview of Natural Attenuation
EPA defines natural attenuation as:
... naturally-occurring processes in soil and groundwater environments that act without
human intervention to reduce the mass, toxicity, mobility, volume, or concentration of
contaminants in those media. These in-situ processes include biodegradation, dispersion,
dilution, admrption, volatiliza(ion and chemical or biological stabilization or destruction
of contaminants.
While various mechanisms can reduce contaminant concentrations, EPA's preferred objective· for
site remediation is contaminant destruction, as opposed to dilution or transfer of contaminants from
one medium to another (e.g., from groundwater to soil via sorption). Consequently, to achieve
acceptance of natural attenuation, it is desirable to demonstrate that contaminants are being
transfom1ed to less toxic compounds as part of the attenuation.
Transformation of chemicals in the environment can occur through both chemical (abiotic) and
biological (biotic) processes. In-situ abiotic processes are difficult to manage and often produce only
partial transformation that can result in new compounds more troublesome than those initially
present. In-situ biotic processes, while not fully understood, have been shown to be capable of
accomplishing complete mineralization of chlorinated aliphatic hydrocarbons (CAHs), destroying
them and preventing their migration off-site.
3.2 Natural Attenuation of Chlorinated Aliphatic Hydrocarbons
Biotic transformation of organic compounds in the environment can occur under either aerobic or
anaerobic conditions if the necessary microbial population and nutrients necessary for their growth
are present in an environment that the microorganisms find habitable. The products of such
transformations depend on the specific microbes, the energy sources available, the specific
contaminants present, and whether the environment is aerobic or anaerobic and oxidizing or
reducing.
Aerobic conditions generally promote biological oxidation of the compounds in the presence of
electron acceptors such as oxygen, nitrate, iron (Ill), and sulfate. Here, the process is fairly simple,
with the microbes using carbon-containing compounds as "food" (i.e., they oxidize it) while
"breathing" (i.e., reducing) the electron acceptor. Because highly chlorinated hydrocarbons, such
as tetrachloroethene (PCE) and trichloroethene (TCE), are also relatively highly oxidized
compounds, they are not readily used as primary substrates in aerobic processes and are resistant to
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 6
this process. In years past, it was assumed that these compounds were resistant to biological
transformation.
It is now understood that, in subsurface environments where anaerobic conditions exist, CAHs can
be biologically transformed through reductive dechlorination. This is a step-wise process where
chlorine substitutes are removed from the core molecule and replaced by hydrogen. It has been
shown that, in this process, the highly chlorinated CAI-ls act as an alternate electron acceptor during
the biological oxidation of a primary substrate such as natural organics or anthropogenic
hydrocarbons that may be present. In the absence of these primary substrates, anaerobic
dechlorination will not occur, which explains why degradation occurs at some but not all sites. The
. more highly chlorinated species, being better electron acceptors, will degrade most readily,
producing lesser-chlorinated compounds. These products can in tum be further dechlorinated by the
microbial population, but at much slower rates. Thus; anaerobic transformation of PCE will
sequentially produce TCE, 1, 1-dichloroethene (DCE), vinyl chloride (VC), and ethene. Reductive
dechlorination is the most common naturally occurring process causing the degradation of the more
highly chlorinated CAHs, such as PCE, TCE, chloroform, and carbon tetrachloride, dissolved in
groundwater (Wiedemeier et al., 1996) .
Production of lesser-chlorinated intermediates that are less susceptible to electron-acceptor reactions
(reductive dechlorination) can result in a buildup of these species and can be troublesome if the
process stalls at this stage because some of these "daughter" products, such as VC, are more toxic
and more mobile than the parent compounds. Under some conditions, such as the leading edges of
contaminant plumes where oxygen has infiltrated, aerobic conditions exist and aerobic microbes can
then use daughter products as energy sources, converting them to less toxic compounds at a much
faster rate than the sequential reductive dechlorination process would. Hence, plumes that start
under anaerobic conditions with carbon sources available then transition into aerobic conditions that
can effectively contain CAH contamination (Wiedemeier et al. 1996).
3.3 Demonstration of Natural Attenuation of Chlorinated Aliphatic Hydrocarbons
To address problems associated with past operations at its installations, the U.S. Air Force Center
for Environmental Excellence (AFCEE) funded studies that have significantly advanced the science
of natural attenuation of CAI-ls. The studies culminated in publication in November 1996 of the
Technical Protocol. This document presents technical procedures and guidance for data collection
and analysis by which to evaluate the fate in groundwater of CAI-ls and determine not only whether
concentrations are being reduced by degradation, dilution, or transfer of media, but also whether any
degradation that occurs is by biotic or abiotic processes. The Technical Protocol therefore provides
a starting basis for collecting data for demonstrating natural attenuation. ·It must then be enhanced
by a thorough understanding of the specific site and specific needs for decision making.
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3.4
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 7
The Technical Protocol's Bioattenuation Screening Process
The Technical Protocol first provides a screening process by which to assess whether natural
bioattenuation is likely to be significant component to contaminant remediation. The screening
process, represented in Figure 1 (excerpted from the Technical Protocol), compares rates of
contaminant transport with estimates ofbiodegradation rates to predict whether biodegradation alone
has potential to achieve remedial objectives. The first step in the process (Step 1: Determine if
Biodegradation is Occurring) uses a scoring system where specific parameters are awarded points
based on their potential for enhancing conditions for natural attenuation and on indications that
natural attenuation is occurring. The process calls for sampling groundwater from monitoring wells
that are representative of the contaminant transport system and analyzing the samples for specific
parameters. Per the Technical Protocol, the wells should be selected to represent the following zones
of the transport system:
1)
2)
3)
The most contaminated portion of the aquifer (generally the source area where nonaqueous-
phase liquid [NAPL] is present or has been present).
The dissolved contaminant plume downgradient of the source area.
The non-contaminated portion of the aquifer downgradient of the dissolved contaminant.
plume.
4) The non-contaminated portion of the aquifer upgradient of the source area and lateral to the
contaminant plume.
After groundwater samples from selected monitoring wells have been analyzed for ·specified
parameters, the Technical Protocol calls for evaluating whether biodegradation is occurring by
applying a scoring system that uses the results of the analyses as the basis for awarding points for
each parameter. The scoring system lists the parameters, criteria for scoring, and potential points
associated with each parameter. The criteria for scoring vary among the parameters, but are of the
following three types:
• Threshold concentrations for the parameter in the most contaminated portion of the aquifer
(Zone 1, above).
• Concentrations in Zone 1 relative to background (Zone 4) concentrations.
• Demonstration that a compound in the dissolved contaminant plume is a product of
biodegradation of a source compound (i.e., the compound found is a "daughter" product of
a "parent" compound from the source area).
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Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997 8
The scoring system emphasizes biodegradation of the parent compounds PCE, TCE, DCE, I, I,!-
trichloroethane (I, I, l-TCA), and dichlorobenzenes (several of which are in groundwater at the site)
to intermediate daughter products TCE, DCE, VC, and chloroethane and ultimate products chloride,
methane, ethcne, and carbon dioxide. Other parent ·CQ!]1pounds and daughter products in
groundwater at the site, such as chloroform, carbon tetrachloride, and methylene chloride, arc not
specifically addressed in the scoring system.
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4.
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 9
GROUNDWATER SAMPLING AND ANALYSES CONDUCTED FOR
BIOATTENUATION SCREENING
In June I 997, GEi conducted a program of groundwater sampling and analysis at the site (Task I B)
to obtain data for supporting· application of the Initial Site Screening procedure in the Technical
Protocol. Twenty-four monitoring wells, shown on Figure 2, were designated by NCSU for the
following field measurements and analyses of groundwater samples in a field laboratory and a fixed-
base laboratory:
FIELD MEASUREMENTS
Dissolved oxygen
Oxidation-reduction potential
Depth/elevation of potentiometric surface
FIELD LABORATORY ANALYSIS
Dissolved hydrogen
FIXED-BASE LABORATORY ANALYSES
Total iron
Dissolved iron
Total manganese
Dissolved manganese
Total alkalinity
Chloride
Volatile organic compounds
Conductivity
Temperature
pH
Dissolved ethane
Dissolved ethene
Dissolved methane
Nitrate nitrogen
Total organic carbon
Sulfate
Field measurements were conducted by GEi; field laboratory analyses were conducted by Turner,
Hart & Hickman, P.C., of Baton Rouge, Louisiana; and fixed-base laboratory analyses are conducted
by Pace Analytical Services, Inc., of Huntersville, North Carolina, and Minneapolis, Minnesota.
The results of these measurements (except depth/elevation of the piezometric surface) and analyses
are summarized in tables provided in Appendix A and in a separate report prepared by GEi (GEi,
1997c). Consistent with results from previous investigations of the site, the predominant volatile
organic compounds in groundwater are as follows:
•
•
CAHs: chloroform, methylene chloride, carbon tetrachloride, tctrachloroethene,
trichloroethene, 1,2-dichloropropane, and chlorobcnzene.
Non-CAHs: toluene, benzene, xylenes, and 1,2-dibromomethane .
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Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997 10
Concentrations of individual compounds in parts per million (milligrams per liter, or mg/L) are
prevalent in samples from monitoring wells immediately downgradient (northwest) of the source
burial trenches (e.g., monitoring well MW02) and approximately 125 feet downgradient of the
source at the downgradient limit of the site's monitoring well network (e.g., MW12). Volatile
organic compounds were either not detected o~ were detected at concentrations below remedial
objectives of the ROD in the upgradient background wells (MW32, MW33, MW34S, and MW34D)
and in wells MW 10 and MWl 3 within the conta'minant plume.
Three bedrock wells within the contaminant plume were sampled. Bedrock groundwater at wells
MW38 and MW35D was not affected by VOC contaminant migration (the sample from well MW38
contained l ug/L of chloroform). However, six CAHs were detected in the sample from well
MW36D at concentrations above remedial objectives.
Figure 2 provides GEi's interpretation of the potentiometric surface of shallow groundwater (the
water table) at the site,_ based on measurements of depth to groundwater in 18 shallow monitoring
wells in June 1997. As has been shown in previous investigations, shallow groundwater flow across
and downgradient from the site is northwesterly.
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 11
5. APPLICATION OF THE BIOATTENUATION SCREENING PROCESS TO THE
SITE
GEi applied results of the groundwater sampling and analysis to the biodegradation scoring system
in the Technical Protocol in the following manner:
I) Select biodegradation zones. Based on the location of the source voes, the confirmed
northwesterly direction of groundwater flow (shown on Figure 2), site hydrostratigraphy (as·
described in prior site investigations and as evident from boring log summaries),
groundwater table and well screen elevations (Table l ), and the concentrations of eAHs
detected (tabulated in Appendix A), the 24 monitoring wells sampled were categorized into
zones representative of the contaminant flow system, as described in the Technical Protocol,
as follows .
Zone Description Monitoring Wells
Wells in the most contaminated portion MW02, MW03, MW06, MW07, MW08,
of the aquifer. MW12, MWl6, MW36S, MW37
2 Wells in the dissolved contaminant MW04, MWI0, MW! I, MW13, MWIS,
plume downgradient of the most MW17, MW27, MW35S
contaminated portion of the aquifer.
3 Wells downgradient of the dissolved None
contaminant plume.
4 Wells upgradicnt of the source area or MW32, MW33, MW34S
lateral to the contaminant plume.
5 None of the above (bedrock wells). MW34D, MW35D, MW36D, MW38
GEi's estimate of the general locations of Zones 1, 2, and 4 are shown on Figure 2. Wells
MW04, MW! I, and MW27, while appearing to be hydraulically upgradient of or lateral to
the source area and contaminant plume, are included in Zone 2 because samples from these
wells contained voes detected in wells clearly hydraulically downgradient of the source.
These wells could be influenced by local variations in hydraulic gradient caused by
groundwater "mounding" around the source area and/or by diffusion of voes from the
source area. In this context, GE!' s determination of which wells to categorize as
downgradient wells considered both hydraulic gradient and voe-concentration gradient.
Also, because eAH are present at the most downgradient wells, GEi considers there to be
no wells qualifying for Zone 3 (downgradient of the dissolved plume). The wells selected
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2)
3)
4)
Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997 12
for Zone 5 are deep, bedrock wells and are grouped separately because they are not
hydrostratigraphically consistent with the shallow, saprolite wells in Zones I, 2, and 4.
Reduce data for each biodegradation zone. Results for the analyses for each parameter were
compiled and sorted by zone and parameter. For each parameter within each zone, the
minimum value, the maximum value, the average value, and the median value were
identified. The median parameter values were selected as the best representation of
groundwater conditions in each zone for application in the biodegradation scoring system.
The resulting sorted and reduced data for each zone are shown in Table 2.
Analytical results reported as "not detected at or above the laboratory's reporting limit" (i.e.,
those with a "U" qualifier in the data tables in Appendix A) are treated as non-values in
determining the minimum, maximum, average, and median values shown on Table 2. As
alternative conventions for representing "not-detected" values, GEi also considered using
zero, the reporting limit, or one-half the reporting limit. While any of these approaches
introduces a high or low bias to the minimum, average, and median values for parameters
with a mix of detected and not-detected values, this decision did not affect the scoring of any
of individual parameters. In deciding how to score parameters that included not-detected
results, GEi placed primary emphasis on the median values, but also recognized a not-
detected result to be a possible value in the range of zero to the specific reporting limit.
Evaluate the presence of daughter products. The possible presence of daughter products in
either Zone I or Zone 2 was evaluated from the analytical results. Records of waste disposal
at the site were reviewed in an attempt to identify specific CAHs known to be present in or
absent from the source area. Because records of waste disposal did not conclusively exclude
compounds such as TCE, 1,2-DCE, chlorofonn, methylene chloride, I, 1-DCE, and
chlorobenzene as buried wastes (parent compounds), and because few daughter products
were detected in groundwater samples collected from the site, no scoring points for the
presence of daughter products were awarded.
_Apply the biodegradation scoring system. The median parameter concentrations in Zone
I and median background (Zone 4) concentrations for alkalinity and chloride were applied
to the scoring system. The completed scoresheet is included as Table 3.
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6. EVALUATION OF THE RESULTS
Task 2 -Bioattenuation Screening Analysis
North Carolina.State University
August 29, 1997 13
· The total score for the biodegradation screening using Zone I results is 17 points. The Technical
Protocol provides the following guidance for interpreting the total score:
Total Score
0 to 5
6 to 14
15 to 20
>20
Strength of Evidence for
Biodegradation of CAHs
Inadequate evidence
Limited evidence
Adequate evidence
· Strong evidence
On this basis, there is "adequate evidence" that natural biodegradation of CAHs is occurring at the
site. The Technical Protocol further states that if"the score totals 15 or more points, it is likely that
biodegradation is occurring, and the investigation should proceed" to groundwater flow and transport
modeling.
The following is GEi's assessment of the contribution of each parameter to the strength of evidence
for biodegradation of CAHs at the site. The parameters on the scoresheet are grouped into the
following categories for this assessment: favorable indications, non-favorable indications, and
parameters not included in the analyses. "Range" and "Median" values are for Zone I.
Dissolved oxygen Range: 0.23 to 1.42 mg/L Median: 0.37 mg/L Score: 3 of -3 or 3 points
DO concentrations in this range indicate that anaerobic conditions conducive to biotic reductive dechlorination
predominate in Zone I. The Zone 4 (upgradient) median DO concentration is 6.4 mg/L, indicating depletion of
DO across Zone I. The Zone 2 (farther downgradient) median DO concentration is 6.2 mg/L, indicating aerobic
conditions, and aerobic attenuation processes may occur downgradient of Zone I.
Nitrate Range: 0.053 to 8.8 mg/L Median: 0.87 mg/L Score: 2 of0 or 2 points
Nitrate is a highly oxidized compound that will competitively exclude CAHs as electron acceptors ifit were present
in the system at concentrations higher than I rng/L. Denitrification appears to not be competing with reductive
chlorination in Zone I.
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Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997 14
Sulfate Range: 5.4 to 12 mg/L Median: 8.7 mg/L Score: 2 of0 or2 points
Sulfate is a highly oxidized compound that can competitively exclude CAHs as electron acci::ptors ifit were present
in the system at concentrations higher than 20 mg/L, and sulfate was not detected above 5 mg/Lat seven of nine
wells in Zone I. No sulfate concentration in Zone I is above 20 mg/L. Sulfate reduction appears to not be
competing With reductive dechlorination in Zone I.
pM Range: 4.9 to 6.7 Median: 5.7 Score: 0 of0 or-2 points
Groundwater with pH in the range of 5 ot 9 is generally conducive to biotic reductive dechlorination.
Total organic carbon Range: 6.2 to 210 mg/L Median: 54 mg/L Score: 2 of0 or 2 points
These TOC concentrations indicate that electron donors and primary substrates, which provide carbon and energy
for reductive dechlorination, appear to be sufficient and are not limiting the rate ofbiodcgradation in Zone 1.
BTEX Range: I. 7 to 24 mg/L Median: 8.3 mg/L Score: 2 of 0 or 2 points
BTEX hydrocarbons provide a source of carbon for microbial growth during reductive dechlorination. Chlorinated
solvent plumes where sufficient anthropogenic carbon (e.g., BTEX) is available for growth (Type I Behavior, as
described in the Technical Protocol) will result in the most predictably rapid and extensive degradation of the more
highly-chlorinated contaminants, such as PCE, TCE, carbon tetrachloride, chloroform, and DCE. Based on the
BTEX concentrations alone, anthropogenic carbon sources for dechlorination are not limiting the rate of
biodegradation in Zone I.
Alkalinity Range: 2 to 49 mg/L Median: 19 mg/L Score: I of 0 or I point
Background (Zone 4) alkalinity results range from less than I mg/L to 26 mg/L. Because of the limited number
of background samples (3) and highly variable alkalinity results for upgradient wells, GEi evaluated alkalinity
results in shallow wells across the site (Zones 2 and 4) relative to alkalinity results in Zone I. The median
alkalinity for all shallow wells (11) outside of Zone I is 6 mg/L. The median alkalinity for shallow wells in Zone
I is 19 mg/I. GEi concludes the conditions of alkalinity in Zone I are significantly elevated relative to conditions
of alkalinity outside of Zone I. Alkalinity of groundwater is important in the maintenance ofpM by buffering the
system against acids produced in biological (aerobic or anaerobic) degradation.
Chloride Range: 4 to 63 mg/L Median: 24 mg/L Score: 2 of0 or 2 points
The median chloride concentration for Zone 4 (background) is 2.1 mg/L. The chloride concentration in Zone I
is more than IO times the background concentration. In reductive dechlorination reactions, chloride is released
to groundwater. Elevated chloride concentrations in Zone I is direct evidence of reductive dechlorination activity.
Dissolved hydrogen Range: 2.1 to 129.3 nM Median: I 8.8 nM Score: 3 of 0 or 3 points
The dissolved hydrogen concentrations indicate the dominant terminal electron accepting process for Zone I is
methanogenesis or sulfate reduction. Sulfate reducers and methanogens are relatively inefficient in utilizing
hydrogen. The most rapid rate of reductive dechlorination affecting the widest range of chlorinated CAHs is
reported to occur under sulfate-reducing or methanogenic conditions, which are indicated by the Zone I dissolved
hydrogen concentrations.
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 15
lrou (Il) Range: 0.49 to 0.97 mg/L Median: 0._73 mg/L Score: 0 of0 or 3 points
The ratio of ferrous iron (II) (dissolved iron) to ferric iron (Ill) (total iron) is generally high in Zone I, indicating
that much of the available iron (Ill) has been reduced to iron.(11) and that reducing conditions exist in Zone I. The
median iron (II) concentration in Zone I is low (below I mg/L) because of the low availability of iron in the
system.·
Methane Range: Not detected Median: Not calculable Score: 0 of 0 or 3 points
The absence of dissolved methane in Zone I is in conflict with strong evidence (e.g., dissolved oxygen and
dissolved hydrogen concentrations) that methanogcnesis, which produces methane, is occurring in Zone I.
ORP Range: 30 to 284 mV Median: 250 mV Score:0 of 0, I or 2 points
ORP is a measure of electron activity and indicates the relative tendency of a solution to accept or transfer
electrons. Some biological processes operate only within a certain range of ORP conditions. Lower ORP values
indicate stronger reducing conditions. The high positive ORP values for Zone I arc in conflict with strong
evidence provided by other rarameters that reducing conditions exist in Zone I. In addition, conflicts _between
the ORP and dissolved oxygen data sets cause GEi to question the accuracy and representativeness of the ORP data
set. For example, ORP values higher than I 00 m V are not plausible where DO values are less than 0.5 mg/L. A
second set ofORP readings for the 24 wells was collected by GEi's subcontractor, retained to conduct on-site 11eld
laboratory analyses for dissolved hydrogen, at the same time that GEi collected ORP readings; these readings are
not included in the data in Appendix A. While the subcontractor's ORP readings indicate stronger reducing
conditions in Zone I than the readings taken by GEi, there also are conflicts between ORP and dissolved oxygen
values in the subcontractor's data. Because of the uncertainty about the ORP values, 0 points are awarded for
ORP.
Temperature Range: 16.6 to I 9.2°C Median: I 6.1 °C Score: 0 of I point
The dechlorination process would be accelerated if temperatures were above 20°C.
Ethane/cthene Range: Nol detected Median: Not calculable Score:0 of 0, 2 or 3 points
The absence of dissolved ethane and ethene is in conflict with strong evidence that reducing conditions exist in
Zone I and that reductive dechlorination is occurring. Under reducing conditions (Type I behavior), the lesser-
chlorinated degradation products may be reduced through vinyl chloride to ethene, ethane, or methane. However,
under these conditions alone, the destruction of the degradation products is slow, and vinyl c·hloride tends to
accumulate.
Daughter products Score: 0 points
Records of waste disposal for the site are not sufficiently specific regarding the content of the waste to identify or
eliminate specific compounds in the waste as "parent" compounds. In addition, because the compounds identified
in the scoring system as daughter products generally were not detected in the wells in Zones I and 2, specific
daughter products could not be identified. The absence of daughter products is unexpected and in conflict with
indications from other parameters that reductive dechlorination is occurring.
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Sulfide
Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 16
Availability of sulfur in the system is generally low, based on sulfate concentrati6ns. Arl elevation of
sulfate/sulfide ratios can provide evidence of conditions conducive to reductive dechlorination. Groundwater
samples were not analyzed for sulfide.
Carbon dioxide
The presence of carbon dioxide can provide evidence of biological activity and correlates to the alkalinity of the
system. Groundwater samples were not analyzed for carb~n dioxide.
Volatile fatty acids
The presence of volatile fatty acids provides evidence of available electron donors and is an additional indicator
of anaerobic conditions. Groundwater samples were not analyzed for fatty acids.
Other parameters for which analyses were conducted, but are not part of the scoring system, are as
follows:
•
•
Total and dissolved manganese: The inorganic manganese (Mn) data for the site suggest
concentrations of the metal are elevated in Zone 1 (median total Mn concentration of7.3 mg/L)
relative to Zone 2 (median total Mn concentration of0.07 mg/L) and Zone 4 (median total Mn
concentration of0.02 mg/L). The elevated concentrations of Mn in Zone I wells are as reduced
or dissolved Mn(+2). This indicates reducing conditions in Zone I.
Total and dissolved iron: The iron data indicate that ferric iron (III) concentrations are
generally low overall, with the highest concentrations reported in upgradient (background)
wells. No reduced ferrous iron (II) was detected in any Zone 2 or Zone 4 well. Conversely, in
two of the Zone I wells, nearly all of the detectable iron was in the reduced, or dissolved, iron
(II) state. Three wells of Zone I had low ferric .iron (Ill) concentrations, with no ferrous iron
(II), and four wells in Zone I had no detectable iron concentrations. Much of the available iron
(lll) in Zone I has been reduced to iron (II), indicating that reducing conditions exist in Zone
I.
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7. CONCLUSIONS
Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997 17
The biodegradation score based on the results of groundwater sampling and analysis performed
according to the Technical Protocol indicates that there is adequate evidence ofbiodegradation of
chlorinated organics at the site to warrant more detailed evaluation of natural attenuation. The
conditions expressed in the results for dissolved oxygen, dissolved hydrogen, total organic carbon,
BTEX, nitrate, sulfate, alkalinity, chloride, and pl-I, indicate that reductive dechlorination of the more
highly chlorinated CAI-ls should be occurring in Zone 1, the zone of the highest groundwater
contaminant concentrations. Downgradient from Zone I, conditions are aerobic and favorable for
continued biodegradation by aerobic oxidation or cometabolism of intermediate daughter products,
such as the dichloroethenes, 1,2-dichloroethane, methylene chloride, and vinyl chloride.
In apparent conflict with strong favorable indications from the above parameters, data for the
following parameters appear to indicate that biodegradation of CAI-ls is not occurring or that
conditions are not favorable for biodegradation: intermediate daughter products, metabolic end-
product gases, and ORP. Discussion of each follows.
Intermediate daughter products. Few intermediate daughter products were detected in groundwater
samples collected from the site. Except for elevated chloride concentrations in Zone 1, direct
evidence of products of biodegradation, including the presence of intermediate daughter products
is weak or lacking. For example, dechlorination of PCE and TCE produces 1,2-DCE, 1, 1-DCE, and
vinyl chloride, none of which was detected to a significant extent.
The issue of parent versus daughter products is particularly problematic for interpreting the VOC
data for the site. Compounds that are dechlorination daughters of PCE and carbon tetrachloride,
including TCE, chloroform, and methylene chloride, are found in groundwater in Zone 1 in high
concentrations. However, what proportions, if any, of the specific concentrations found are
attributable to degradation versus direct input to the system from the source is not known.
Compounds that are distinctly derived from degradation of CAI-Is, such as cis-1,2-DCE, vinyl
chloride, or chloroethane, are not found in the VOC data. Source compounds PCE and carbon
tetrachloride are widely detected in Zone I in part-per-million concentrations and are not detected
in Zone 2 wells. Detectable concentrations of PCE and carbon tetrachloride and a greater
distribution of TCE, chloroform, and methylene chloride would be expected in Zone 2 in lieu of
attenuation by biodegradation, based on the concentrations found, distances from the source, and the
amount of time since the waste was placed at the site.
It is possible that daughter products are present, but were not detected and reported in the analyses
because of high concentrations of parent VOCs, the need for the laboratory to dilute the samples, and
the resulting elevated laboratory reporting limits. The laboratory reported peaks in volatile organic
GC/MS analysis that were positively identified by characteristic ion scans, but were quantified to
less than the sample reporting limit (laboratory "J" values). A detailed, coordinated review of the
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Task 2 -Bioattenuation Screening Analysis
North Carolina State University
August 29, 1997 18
data by GEi and the laboratory may reveal the presence of additional daughter products at
concentrations below the laboratory's reporting limit.
Metabolic end-product gases (methane, ethane, ethene, and carbon dioxide). None of these dissolved
gases was detected in the groundwater samples (carbon dioxide was not included in the analyses).
As a result, direct evidence of these metabolic end products is lacking. Methane would be expected
if dechlorination were occurring, and ethene would be present under strongly reducing conditions
ofmethanogenesis ofalkenes. It is possible that the analytical holding time (14 days) established
for the unpreserved samples enabled the gases, if present in the samples when collected, to be
biologically transformed or lost, causing them to not be detected in the analysis. Resampling of
selected monitoring wells, followed by rapid-turnaround analyses for these dissolved gases, could
resolve this apparent conflict.
ORP. Contradictions between the ORP and dissolved oxygen data sets cause GEi to suspect the
accuracy and representativeness of the ORP data. The common platinum electrode used in
measuring ORP is not completely responsive to several soluble-phase redox couples that are
common in groundwater, including sulfate/sulfide, carbon dioxide/methane, and nitrate/nitrogen.
Additionally, the electrode systems can be readily impaired or fouled. Resampling selected wells
for measuring ORP could resolve this apparent contradiction, but may not be necessary considering
the evidence afforded by the data as a whole, particularly hydrogen and dissolved oxygen results.
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REFERENCES
Task 2 -Bioattcnuation Screening Analysis
North Carolina State University
August 29, 1997
Brown and Caldwell (1994). Remedial Investigation Report, Lot 86 Site, North Carolina State
University, Raleigh, North Carolina. June I 0, 1994.
Brown and Caldwell (1995). Revised Feasibility Study Report, Lot 86 Site, North Carolina State
University, Raleigh, North Carolina. January 1995.
EPA (1996). Record of Decision, NC State University Lot 86 Superfund Site. September 30, 1996.
GEi Consultants, Inc. (1997a). Sampling and Analysis Plan, Lot 86 Superfund Site, Raleigh, North
Carolina (Revision 0). May 9, 1997. ·
GEi Consultants, Inc. (1997b). Quality Assurance Project Plan, Lot 86 Superfund Site, Raleigh,
North Carolina (Revision 0). May 9, 1997
GEi Consultants, Inc. (1997c). Results of Task I B Groundwater Sampling and Analysis,
Groundwater Natural Attenuation Demonstration, Lot 86 Superfund Site. August 5, 1997.
NCSU (1996a). Preliminary Evaluation of Natural Attenuation as a Remedial Approach for the
North Carolina State University Lot 86 Site (Draft). February 1996.
NCSU (1996b). Revised Feasibility Study, North Carolina State University Lot 86 Site (Draft).
February I 996.
S&ME (1996). Limited Site Assessment and Source Characterization Report for North Carolina
State University, Lot 86 Site. January 24, 1996.
Wiedemeier et al. (1996). Technical Protocol for Evaluating Natural Attenuation of Chlorinated
Solvents in Ground Water (Draft-Revision I). November 1996.
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TABLE 1 -POTENTIOMETRIC SURFACE
Lot 86 Superfund Site
Raleigh, North Carolina
Page 1 of 1
·4<,gL~ "'.-', i'..W!'. .:::t;ffo'Jf0fJRis'0~~!s &i,: G rci1.1 n d JS 1.1 rfa ce"!i '~Potentiometric;Surfac:e~ Yt;'JffO'p!of:!-SCr88h_it!'.V ·sottcim'ot;Sc:reerf•
., __ ,. ' •• <\ ' ·, •'. i' :· ·:.' • '." ',1 ;; •. , •. , '';'·_--•. ~-)'.. .. _/Mk :;,·• )' ,•-·;-f"," · • __ ;~'.:i , _,;( ~. · 'F :~. __ ,. 1V\;"; ··.·-,. :.-,-.. ! • , \ ~'_; __ -.. ~., ;•.:••~,1'.:<z-'-.',_., ~--'"'.1.:•-~ ;,01),~-:· .. ,,..-,.,\;.,' ! Y<i'· ·:,Elevat,on{3)'",; · ~y wem ' ' a;, ~El{ivatiol1(1 )'. 1?: ~: !\~.,-. ·-:~:;.:'t'.' .-:: 'f5. :'..'.~·. ft'., l)!-<~---f·;, '0, ''Elevation(1) •,. ~.:
~·:,:,~'.,){f ''j',.J 'r;;;,
: " ·,., "·Elevation(2)(-·· ,. • .. :
>~-~ .;::1 ~i:;::tl{~~!)'1i:,/ ~(:??:_;;~;
'.~·• Elevation(3)'-:·, ~{rt l 1f~~t)£J~j::;;}~i;; '_'."!,1':·_ T, +i~•,,_,,,.,.,,...t "\.: :A•'.;_l · )'
f.,11:.•l -~:l:-.;<,t. t.d!.,k'.i';,_,:,, -~0... ::A.i. :Jwiiu ,l1,.,.d:1fo. .. ~e.t ,:h. ~t,:,,L ,,,,,~0 / ,,t,:'t, "~-•· , ,),V"' .,0 ,,. .. ~\ ,:;g ,jli,,i!(feet)tla1•,~ ,. : , .. ,.·.£,,;.,~ ~~· ,Ai< ,1' .. ~~:-,
MW01
MW02
MW03
MW04
MW06
MW07
MW08
MW10
MW11
MW12
MW13
MW15
MW16
MW17
MW27
MW30
MW32
MW33
MW34D
MW34S
MW35D
MW35S
MW36D
MW36S
MW37
MW38
Notes:
1.
2.
3.
439.30 437.73 407.22 400.53 395.53
445.17 443.93 410.15 401.23 396.23
445.39 443.58 409.39 411.18 406.18
454.32 452.54 413.19 405.54 400.54
438.61 436.36 407.26 402.86 397.86
441.94 440.09 408.79 401.29 396.29
447.85 445.91 409.90 397.91 392.91
438.09 435.60 403.93 398.60 393.60
430.01 429.56 410.42 405.56 · 400.56
427.24 426.18 407.04 397.18 392.18
423.82 423.73 400.17 394.73 389.73
432.38 431.67 399.32 397.67 392.67
427.94 427.61 409.48 399.61 394.61
425.09 424.02 404.14 398.02 393.02
448.26 447.22 412.83 407.22 402.22
440.86 438.17 415.70 399.17 398.17
438.15 436.21 410.50 411.41 401.41
441.38 438.42 410.36 378.42 368.42
440.13 437.66 413.86 322.16 312.16
439.57 437.53 416.97 397.53 387.53
444.69 441.99 406.09 304.99 294.99
443.12 441.57 403.94 401.57 391.57
442.87 439.75 408.02 335.45 325.45
442.71 439.64 407.89 399.64 389.64
440.88 438.70 407.93 398.70 388.70
445.38 442.47 410.06 345.37 335.37
Riser and ground surface elevations were surveyed in July 1997 by Murphy Hobson Sacks, of
Raleigh, North Carolina. Elevations are referenced to National Geodetic Vertical Datum (NGVD) of
1929 based on the North Carolina Geodetic Survey Station "East Base". Riser means the top of the
internal sleeve located inside the outer protective well casing.
Potentiometric surface elevations are calculated from depth-to-groundwater measurements by
GEi Consultants, Inc. (GEi) during the period from June 8 through June13, 1997.
Top-of-screen and bottom-of-screen elevations are calculated from ground surface based on the Well
Construction Record completed by the drilling contractor for issue to the Division of Environmental
Management, Groundwater Section, North Carolina Department of Natural Resources and Community
Development, provided by NCSU.
GEi Consultants, lnC Project 97191 August 1997
--· -- - -- - - -- - - - --TABLE 2 -GROUNDWATER QUALITY DATA SORTED AND REDUCED BY BIODEGRADATION ZONE
Lot 86 Superfund Site
Raleigh, North Carolina
--
Zone 1 -Wells in the Most Contaminated Portion of the Aquifer Page 1 Of 4
MW02 8.8 0.053 <0.05 40 42 <5 0.29 <8.6 <15 <16 6.2 16.2 230 49 63 18.8
MW3 0.053 0.54 0.49 6.9 7.3 <5 0.53 <8.6 <15 <16 6.67 18.7 45
MW6 <0.05
MW07 <0.05
MW08 0.78
MW12 0.95
MW16 <0.05
MW36S <0.05
MW37 <0.05
0.22 <5 16.6 250
<0.05
<0.05
0.97
<0.05
0.053
<0.05 18 18
<0.05 4.1 4
<0.05 0.085 0.087
<0.05 4.6 4.7
0.97 15 15
<0.05 9.9 10
<0.05 7.3 7.3
<5
<5
<5
5.4
<5
0.37 <6.6 <15 <16 6.66
0.53 <8.6 <15 <16 5.7
0.29 <8.6 <15 <16 5.6
1.42 <8.6 <15 <16 4.9
0.23 <8.6 <15 <16 6.4
0.33 <8.6 <15 <16 5.7
0.47 <8.6 <15 <16 5.7
<0.05 12 18.4 284
17.7
18.1
16.8
19.2
274
261
30
282
246
35 4 21.6
28 53 2.1
19 24 22.2
6 6.3 5.61
2 32 8.71
39 10 12.5
19 14 30.6
17 27 129.3
Min 0.053 0.053 0.49 0.085 0.087 5.4 0.23 NC NC NC 4.9 16.6 30 2 4 2.1
Max 8.8 0.97 0.97 40 42 12 1.42 NC NC NC 6.67 19.2 284 49 63 129.3
Average 2.65 0.37 0.73 11.77 12.04 8.7 0.50 NC NC NC 5.95 17.9 211 24 25.9 27.9
Median 0.87 0.22 0.73 7.3 7.3 8.7 0.37 NC NC NC 5.70 18.1 250 19 24.0 18.8
Score 2 NA 0 NA NA 2 3 0 0 0 0 0 0 1 2 3
MW02 210 7500 13000 700 1600 1200 24000 1000 2000 <250 <500 900 <500 <250 <250 65
MW3 18 7900 3500 160 380 320 12260 87 4800 18 <10 370 <10 34 47 2
MW6 31 1300 140 24 84 220 1768 700 1200 <100 <200 90 <200 <100 <100 220
MW07 54 6100 420 380 1000 410 8310 550 1400
MWOB 6.2 5300 430 <500 230 190 6150 <500 550
<250
<500
<500
<1000
560
MW12 69 12000 7800 490 1500 810 22600 <500 1100
<500
MW16 73 3300 9400 380 1300 630 15010 1800 3400
<500
<500
<1000 450
MW36S 140 7500 300 <500 160 310 8270 <500 1900
MW37 18 6900 700 <500 350 220 8170 220 680
<500
<1000
<500
<1000
400
<1000
<500
<500
<500
<1000
<250 <250
<1000
<500
<500
<500
<250
<500
<500
<1000
<1000
<500
<500
<500
<500
<500
<1000 <500
<500
<500
<500
100
Min 6.2 1300 140 24 84 190 1768 87 550 18 NC 90 NC 34 47 2
Max 210 12000 13000 700 1600 1200 24000 1800 4800 18 NC 900 NC 34 47 220
Average 69 6422 3966 356 734 479 11838 726 1892 18 NC 462 NC 34 47 97
Median 54 6900 700 380 380 320 8310 625 1400 NC NC 425 NC NC NC 83
Score 2 NA NA NA NA NA 2 NA 0 0 0 0 0 0 0 NA
!Total Score: 17
See notes on page 4 of 4.
GEi Consultants, Inc Project 97191 August 1997
-
---- -- - --- - - -
TABLE 2 • GROUNDWATER QUALITY DATA SORTED AND REDUCED BY BIODEGRADATION
Lot 86 Superfund Site
Raleigh, North Carolina
Zone 2 • Wells in the Contaminant Plume Downgradient of Zone 1
MVV04 0.28 0.53 <0.05 0.019 <0.01 <5 6.80 <8.6 <15 <16 5.64 17.9 296
MW10 1.4 0.27 <0,05 0.062 0.06 <5 9.24 <8.6 <15 <16 5.00 18.3 354
MW11 0.72 <0.05 <:0.05 0.068 0.053 <5 4.06 <8.6 <15 <16 5.68 15.9 442
MW13 9 <0.05 <0.05 1.5 1.6 <5 6.27 <8.6 <15 <16 4.67 17.1 327
MW15 0.41 0.32 <0.05 0.099 0.099 <5 7.11 <8.6 <15 <16 5.37 20.6 349
MW17 0.59 0.47 <0.05 0.073 0.063 <5 6.04 <8.6 <15 <16 5.25 19.9 339
MVY27 0.71 9.3 <0.05 0.47 0.05 <5 5.33 <8.6 <15 <16 5.78 19.6 319
MV\135S 0.87 0.76 <0.05 0.025 0.011 <5 3.21 <8.6 <15 <16 5.34 16.3 298
Min 0.28 0.27 NC 0.019 0.011 NC 3.21 NC NC NC 4.67 15.9 296
Max 9 9.3 NC 1.5 1.6 NC 9.24 NC NC NC 5.78 20.6 442
Average 1.75 1.94 NC 0.290 0.277 NC 6.0 NC NC NC 5.34 18.2 341
Median 0.72 0.50 NC 0.071 0.060 NC 6.2 NC NC NC 5.36 18.1 333
- -
Page 2 of 4
3 1.9 t.53
2 3.5 5.96
12 2.8 1.07
8.9 12.3
7 4 0.756
2 3.7 3.24
7 3.5 3.08
6 2.6 2.6
1 1.9 0.756
12 8.9 12.3
5 3.9 3.82
5 3.5 2.84
Mv\/04 0.95 <5 <5 <5 <5 <5 <5 7.7 13 <5 <10 <5 <10 <5 <5 <5
MW10 1.2 <5 1.3 <5 <5 <5 1.3 <5 <5 <5 <10 <5 <10 <5 <5 <5
MW11 <5 2.7 23 2.6 84 <5 109.6 30 12 <5 <10 <5 <10 <5 <5 <5
MW13 2.8 <5 1.3 <5 <5 <5 1.3 <5 <5 <5 <10 <5 <10 <5 <5 3.4
MW15 1.1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 <10 <5 <5 <5
MW17 12 13 <5 <5 <5 25 <5 <5 <5 <10 <5 <10 <5 <5 <5
MVY27 1.9 <5 <5 <5 <5 <5 <5 <5 1.3 <5 <10 <5 <10 <5 <5 <5
MW35S 1.2 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 <10 <5 <5 <5
Min 0.95 12 1.3 NC 84 NC 1.3 7.7 1.3 NC NC NC NC NC NC 3.4
Ma, 2.8 23 13 NC 84 NC 109.6 30 13 NC NC NC NC NC NC 3.4
Average 1.6 18 4.6 NC 84 NC 34.3 18.9 8.8 NC NC NC NC NC NC 3.4
Median 1.2 18 2.0 NC NC NC 13.2 18.9 12.0 NC NC NC NC NC NC NC
See notes on page 4 of 4.
GEi Consu'ltants, Inc. Project 97191
- --
August 1997
- - - -- - ---- --- - -
TABLE 2 -GROUNDWATER QUALITY DATA SORTED AND REDUCED BY BIODEGRADATION ZONE
Lot 86 Superfund Site
Raleigh, North Carolina
Zone 4 -Wells Upgradient of or Lateral to the Plume
-
Page 3 of 4
MvV32 0.2 2.3 <0.05 0.024 0.01 <5 6.4 <8.6 <15 <16 5.03 19 306 6 3.5 16
Mv\'33 <0.05 0.31 <0.05 0.012 <0.0.1 <5 4.89 <B.6 <15 <16 5.85 17 225 26 2.1 1.43
MW34S <0.05 1.7 <0.05 0.015 <0.01 <5 6.83 <8.6 <15 <16 5.68 15.8 301 <1 1.6 1.85
Min 0 0.31 NC 0.012 0 NC 4.89 NC NC NC 5.03 15.8 225 6 1.6 1.43
Ma, 0.2 2.3 NC 0.024 0.01 NC 6.83 NC NC NC 5.85 19 306 26 3.5 16
Average NC 1.44 NC 0.017 NC NC 6.04 NC NC NC 5.52 17.3 277 16 2.4 6.43
Median NC 1.7 NC 0,015 NC NC 6.4 NC NC NC 5.68 17.0 301 NC 2.1 1.85
Mv\'32 0.84 <5 <5 <5 <5 <5 <S 1 .2 <5 <5 <10 <5 <10 <S <5 <5
Mv\"33 0.67 <5 1.4 <5 <5 <5 1.4 <5 <5 <5 <10 <5 <:10 <5 <5 <5
MW34S <5 <5 <5 <S <5 <S <5 <5 <5 <10 <5 <10 <5 <5 <5
M<a 0.67 NC 1.4 NC NC NC 1.4 1.2 NC NC NC NC NC NC NC NC
Ma, 1 NC 1.4 NC NC NC 1.4 1.2 NC NC NC NC NC NC NC NC
Average 0.84 NC 1.4 NC NC NC 1.4 1.2 NC NC NC NC NC NC NC NC
Median 0.84 NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC
See notes on page 4 of 4.
GEi Consultants, Inc Project 97191
- --
August 1997
-- -
Zone 5 -Bedrock Wells
- ------ --
TABLE 2 • GROUNDWATER QUALITY DATA SORTED AND REDUCED BY BIODEGRADATION ZONE
Lot 86 Superfund Site
Raleigh, North Carolina
--
Page 4 of 4
MVl/340 <0.05 2.1 <0.05 0.25 0.072 <5 0.18 <8.6 <15 <16 10.62 15.8 -86 97 1.9 318
MW35D <0.05 0.7 <0.05 0.062 0.035 <5 6.15 <8.6 <15 <16 6.42 16.6 182 43 1.6 141.3
MW36D 0.06 0.093 <0.05 <0.01 <0.01 <5 2.3 <8.6 <15 <18 6.69 17.3 117 77 1.9 10.6
MW38 <0.05 <0.05 <0.05 0.019 0.028 7.9 1.23 <8.6 <15 <16 6.68 16.9 77 91 2.1 75.8
Min 0.06 0.093 NC 0.019 0.028 7.9 0.18 NC NC NC 6.42 15.8 -86 43 1.6 10.6
Max 0.06 • 2.1 NC 0.25 0.072 7.9 6,15 NC NC NC 10.62 17.3 182 97 2.1 318
Average 0.06 0.96 NC 0.110 0.045 7.9 2.47 NC NC NC 7.60 16.7 66 77 1.9 136.4
Median NC 0.70 NC 0.062 0.035 NC 1.77 NC NC NC 6.69 16.8 97 84 1.9 108.6
1,'!l~!,9rga~i~ '.::"'.0i"}.;" ·~:d rt;-·~:-[~';';'.
h • Cart:iOn.~J. -,Benzene.'{; Toluene ::.Ji~~:.,.),:; ~.;. :·ugll~. '.-:<~ ~: Ug/L-::
,":~-~\ Y,,p_ • --~"f:: ~"'"{¼ 1t~ii; ~;'t'.,:':~"Y tY:'.V:0%4; ;·•i:,1flr ~::1•;f'!_;~\:">";'i:1:ol :l!?·J,~; f.,r:.t;-;::i+":~~ jJff(;f;-1>;;::)iL'.f --.. ,~]~r': :,t'.PA·/:f f;..1T2!~~
Ethylbenzene m;p.-xy1ene o-Xytene -'~BTEX.:_" fPCE'.°;, ,·rce~ cis-J:2°DCE ~VC::f ChlOl'l)benzene Ch!oroethane i,1;1~oce 1;_1;1-TGA ,;,-,DCBs_•·
·~~,,uQl'0q :i ~~:::'t,Qn?.;; t!UQift-s;;iiQ11.~: ->~Q~~ iauQliY:: /\:).1g/L~ ;~ '-.uQ/l~ ·, 2iu'o11Pi-~~ ~-iik;-iioll..~ :.,;ugJL: ¾iutifL~:i :,;Udif:-:
MW340 0,98 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 <10 <5 <5 <5
MW350 0.67 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 <10 <5
MW36D 0.89 <5 <5 <5 <5 <5 <5 9.3 9.1 <5 <10 <5 <10 <5
MW38 1.3 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 <10 <5
Min 0.67 NC NC NC NC NC NC 9.3 9.1 NC NC NC NC NC
Mox 1.3 NC NC NC NC NC NC 9.3 9.1 NC NC NC NC NC
Average 0.96 NC NC NC NC NC NC 9.3 9.1 NC NC NC NC NC
Median 0.94 NC NC NC NC NC NC NC NC NC NC NC NC NC
Notes:
1. Concentrations reported are for groundwater samples collected at the NCSU Lot 86 Site by GEi Consultants, Inc, during the period trom June 8, 1997 through June 12, 1997.
2. Minimum, average and median values are determined for detected result only.
3. Only Zone 1 values are scored in the Bioattenuation Screening Process, with Zone 1 values used for background per the Technical Protocol.
Abbreviations:
<~
NC
NA
BTEX
PCE
TCE
cis-1,2-DCE
vc
1.1-DCE
1,1,1-TCA
Tota! DCBs
GEi Consuftants, Inc.
the parameter was not detected above the associated reporting limit.
not calculable.
not app!lcable in the scoring.
the sum of benzene, toluene, elhylbenzene, and xylenes concentrations.
tetrach!oroelhene.
trichloroethene.
cis-1,2-dichloroelhene.
vinyl chloride.
1.1-dichloroethene.
1, 1.1-trichloroethane.
the sum of 1.2-dichlOrobenzene, 1,3-dichlorobenzene, and 1,4-dichlorobenzene concentrations
Pro1ect 97191
<5 <5
<5 <5
<5 <5
NC NC
NC NC
NC NC
NC NC
- --
Augus11S97
I
I TABLE 3 -BIOATTENUATION SCORESHEET COMPLETED FOR THE SITE
Lot 86 Superfund Site
I
Raleigh, North Carolina
Page I of2
I
I Oxygen' <0.5 mg/L Tolerated, suppresses the.reductive pathway at 3 3
higher concentrations
I Oxygen* >I mg/L VC may be oxidized aerobically -3
Nitrate* <I mg/L At higher concentrations may compete with 2 2 ✓
I reductive pathway
Iron II' >I mg/L Reductive pathway possible 3 0
I Sulfate• <20 mg/L At higher concentrations may compete with 2 2 I
reductive pathway
Sulfide' >I mg/L Reductive pathway possible 3
I Methane* <0.5 mg/L VC oxidizes 0 0
>0.5 mg/L Ultimate reductive daughter product, VC 3
I accumulates
Oxidation Reduction <50 millivolts Reductive pathway possible 0
Potential' (ORP) (mV) Reductive pathway likely 2
I <-100 mV
pH' 5<pH < 9 Optimal range for reductive pathway 0 0
I 5> pH >9 Outside optimal range for reductive pathway -2
TOC > 20 mg/L Carbon and energy source: drives 2 2 ✓-
dechlorination; can be natural or anthropogenic
I Temperature* > 20°c At T>20°C biochemical process is accelerated 0
Carbon Dioxide >2x background Ultimate oxidative daughter product
I Alkalinity >2x background Results from interaction of carbon dioxide with
aquifer inincrals
.-o
I Chloride' >2x background Daughter product of organic chorine 2 2 /
Hydrogen >I nM Reductive pathway possible, VC may 3 3 /
accumulate
I Hydrogen <I nM VC oxidized 0
I Volatile Fatty Acids > 0.1 mg/L Intermediates resulting from biodegradation of 2
aromatic compounds; carbon and energy source
BTEX' >0.1 mg/L Carbon and energy source; drives 2 2 ✓
I dechlorination
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TABLE 3 -BIOA TTENUA TION SCORESHEET COMPLETED FOR THE SITE
Lot 86 Supcrfund Site
!'CE'
TCE'
DCE*
vc•
Ethenc/Ethane
Ch loroethane•
I, I, 1-
Trich lorocthane*
1,2-
dichlorobenzene*
1,3-
dichlorobenzenc*
1,4-
dichlorobenzene*
Chlorobenzenc*
1,1-DCE*
Raleigh, North Carolina
>0.01 mg/L
>0.1 mg/L
Material released
Material released
Daughter product of PCE
Material released
Daughter product of TCE
If cis is greater than 80% of total DCE, it is
likely a daughter product ofTCE
Material released
Daughter product of DCE
Daughter product of VC/ethene
Daughter product of YC under reducing
conditions
Material released
Material released
Material released
Material released
Material released or daughter product of
dichlorobenzene
Daughter product of TCE or chemical reaction
of 1,1,1,-TCA
TOTAL LOT 86 SITE SCORE
Footnotes:
*Required analysis (per the Technical Protocol).
0
0
2"
0
2·
0
2·
2
3
2
0
0
0
0
Page 2 of2
0
0
0
0
0
0
0
0
0
0
0
0
17
a/ Points awarded only if it can be shown that the compound is a daughter product (i.e., not a constituent of the source
NAPL).
Notes:
Base scoreshcet after the Tcchn ical Protocol.
~ GEI ConsultanL~Inc. Project 97191 August 1997
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AnalyZe Available SIie Data
to Determine if Biodegradation l(C----1 Collect More Screening Data
is Geo.ming
Noor
Insufficient
Data
Determine Groundwater Flow and
Solute Transport Parameter.; using
Site-Specific Data; Porosity and
Disper.;ivity May.be Estimated
Estimate Biodegradation
Rate Constant
Compare the Rate of Transport
to the Rate of Attenuation using
Analytical Solute Transport Model
No
No
Yes
Engineered
Remediation Required,
Implement Other
Protocols
No Evaluate use of Selected Proceed to
Additional Remedial Options
along with Natural Attenuation Rgure 2.1
Yes
Perform Site Characterization
to Support Natural Attenuation
Proceed to
Figure 2.1
Source:
Wiedemeier et al., 1996.
~1-----__:_-----,-~-------.....,.-----------i
~ North Carolina State. University Groundwater Natural ~ Raleigh, North Carolina Attenuation Demonstration
;;;-l--------------1 Lot 86 Superfund Site
Raleigh, North Carolina
GEi Consultants, Inc. Project 97191
BIOATTENUATION
SCREENING PROCESS
FLOW CHART
August 1997 Fig. 1
' II.
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0 ~
~ m
~ ' m ~ ' m
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()'° . Ix ...
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./
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·--ZONE 2
f "Sf 1triur f 5,~f ,~;ts··
!&
<:-\\-:·:\,i~{ ~ ogggggpo~~,, (409.90) J.:t:~t \ 0f fgg{iggJogf~• :\oo(;og(;g og . ·.· .. _·. :-·I
LOT 86
SUPERFUND SITE
' ' ' ' ' '
MW30 ,1'\
( 415. 1oi'f"
'
MW34S
~416.97}
• MW340~
' " " " ' " ,r_,
0
+MW32
(410.50)
North Carolina State University
Raleigh, North Carolina
G EI Consultants, Inc.
LEGEND:
_,.h_ MW07 . MONITORING WELL, WELL NUMBER.
'f'{40e.79) ANO WATER TABLE ELEVATION (6/97)
WATER TABLE ELEVATION CONTOUR (6/97)
APPROXIMATE WASTE BURIAL AREA
NOTES:
1. ELEVATIONS ARE NGVD 1929 BASED ON NORTH
CAROLINA GEODETIC SURVEY STATION "EAST BASE".
2. BIODEGRADATION ZONES ARE AS FOLLOWS:
ZONE 1-MOST CONTAMINATED AREA
ZONE 2-DISSOLVED CONTAMINATED PLUME
DOWNGRADIENT OF ZONE 1
ZONE 4-UPGRADIENT AND LATERAL TO THE
CONTAMINANT PLUME
3. SITE PLAN BASED ON SURVEY DRAWING "wELL
AND FEATURE LOCATIONS" BY MURPHY HOBSON
SACKS DATED JULY 29, 1997.
4. WASTE BURIAL AREA LOCATIONS PER BROWN
AND CALDWELL, JUNE 10, 1994.
5. WATER TABLE ELEVATIONS BASED ON MONITORING
WELL ELEVATIONS PER MURPHY HOBSON SACKS
ANO MEASUREMENTS BY GEi CONSULTANTS
DURING JUNE 8-13, 1997.
6. WATER LEVELS IN BEDROCK MONITORING WELLS
MW34D, MW35D, AND MW38 WERE NOT USED TO
CONSTRUCT WATER TABLE ELEVATION CONTOURS.
7. MONITORING WELLS IN ADDITION TO THOSE SHOWN
ON THIS FIGURE EXIST AT THE SITE, BUT WERE
NOT USED IN THIS INVESTIGATION.
0 80 160
SCALE, FEET
Groundwater Natural
Attenuation Demonstration
Lot 86 Superfund Site
Raleigh, North Carolina
SITE MAP, GROUNDWATER
CONTOURS, AND
BIODEGRADATION ZONES
Project 97191 August 1997 Fig. 2
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TABLE 1
Results of Fixed-Base Laboratory Analyses
-------------------
SAMPLE NAME SAMPLED
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191. MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119452 WATER Iron 200.7
920119452 WATER Iron, Dissolved 200.7
920119452 WATER Manganese 200.7
920119452 WATER Manganese, Dissolved 200.7
920119452 WATER Alkalinity, Total 310.1
920119452 WATER Chloride 325.3
920119452 WATER Sulfate 375.2
920119452 WATER Ethane 3810
920119452 WATER Ethene 3810 .
920119452 WATER Methane 3810
920119452 WATER Nitrogen, Nitrate 4500°NO3 F
920119452 WATER Total Organic Carbon 5310C
920119452 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119452 WATER 1, 1, 1-Trichloroethane 8260
920119452 WATER 1, 1,2,2-Tetrachloroethane 8260
920119452 WATER 1, 1,2-Trichloroethane 8260
920119452 WATER 1, 1-Dichloroethane 8260
920119452 WATER 1, 1-Dichloroethene 8260
920119452 WATER 1, 1-Dichloropropene 8260
920119452 WATER 1,2,3-Trichlorobenzene 8260
920119452 WATER 1,2,3-Trichloropropane 8260
920119452 WATER 1,2,4-Trichlorobenzene 8260
920119452 WATER 1,2,4-Trimethylbenzene 8260
920119452 WATER 1,2-Dibromo-3-chloropropane 8260
920119452 WATER 1,2-Dibromoethane 8260
920119452 WATER 1,2-Dichlorobenzene 8260
920119452 WATER 1,2-Dichloroethane 8260
920119452 WATER 1,2-Dichloropropane 8260
920119452 WATER 1,3,5-Trimethylbenzene 8260
920119452 WATER 1,3-Dichlorobenzene 8260
920119452 WATER 1,3-Dichloropropane 8260
920119452 WATER 1,4-Dichlorobenzene 8260
Page 1 of 78
UNITS CONC QUAL OIL
mg/L 0.053 1
mg/L 0.050 u 1
mg/L 40 1
mg/L 42 1
mg/L 49 1
mg/L 63 10
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 8.8 10
mg/L 210 4
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 200 J 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 70 J 50
ug/L 250 u 50
ug/L 65000 50
ug/L 65 J 50
ug/L 235 J 50
ug/L 20000 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 165 J 50
ug/L 250 u 50
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site_
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119452 WATER 2,2-Dichloropropane 8260
920119452 WATER 2-Chlorotoluene 8260
920119452 WATER 4-Chlorotoluene 8260
920119452 WATER Benzene 8260
920119452 WATER Bromobenzene 8260
920119452 WATER Bromochloromethane 8260
920119452 WATER Bromodichloromethane 8260
920119452 WATER Bromoform 8260
920119452 WATER Bromomethane 8260
920119452 WATER Carbon Tetrachloride 8260
920119452 WATER Chlorobenzene 8260
920119452 WATER Chlorodibromomethane 8260
920119452 WATER Chloroethane 8260
920119452 WATER Chloroform 8260
920119452 WATER Chloromethane 8260
920119452 WATER cis-1,2-Dichloroethene 8260
920119452 WATER Dibromomethane 8260
920119452 WATER Dichlorodifiuoromethane 8260
920119452 WATER Ethyl benzene 8260
920119452 WATER Hexachlorobutadiene 8260
920119452 WATER lsopropylbenzene 8260
920119452 WATER m-Xylene and p-Xylene 8260
920119452 WATER Methylene chloride 8260
920119452 WATER n-Butylbenzene 8260
920119452 WATER n-Propylbenzene 8260
920119452 WATER Naphthalene 8260
920119452 WATER a-Xylene 8260
920119452 WATER p-lsopropyltoluene 8260
920119452 WATER sec-Butyl benzene 8260
920119452 WATER Styrene 8260
920119452 WATER tert-Butylbenzene 8260
920119452 WATER Tetrachloroethene 8260
Page 2 of 78
UNITS CONG QUAL OIL
ug/L 500 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 7500 50
ug/L 105 J 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 2600 50
ug/L 900 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 81000 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 55 J 50
ug/L 700 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 1600 50
ug/L 9500 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 1200 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 1000 50
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 MW02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119452 WATER Toluene 8260
920119452 WATER trans-1,2-Dichloroethene 8260
920119452 WATER Trichloroethene 8260
920119452 WATER Trichlorofiuoromethane 8260
920119452 WATER Vinyl Chloride 8260
920119436 WATER Iron 200.7
920119436 WATER Iron, Dissolved 200.7
920119436 WATER Manganese 200.7
920119436 WATER Manganese, Dissolved 200.7
920119436 WATER Alkalinity, Total 310.1
920119436 WATER Chloride 325.3
920119436 WATER Sulfate 375.2
920119436 WATER Ethane 3810
920119436 WATER Ethene 3810
920119436 WATER Methane 3810
920119436 WATER Nitrogen, Nitrate 4500-NO3 F
920119436 WATER Total Organic Carbon 5310C
920119436 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119436 WATER 1, 1, 1-Trichloroethane 8260
920119436 WATER 1, 1,2,2-Tetrachloroethane 8260
920119436 WATER 1, 1,2-Trichloroethane 8260
920119436 WATER 1, 1-Dichloroethane 8260
920119436 WATER 1 , 1-Dichloroethene 8260
920119436 WATER 1, 1-Dichloropropene 8260
920119436 WATER 1,2,3-Trichlorobenzene 8260
920119436 WATER 1,2,3-Trichloropropane 8260
920119436 WATER 1,2,4-Trichlorobenzene 8260
920119436 WATER 1,2,4-Trimethylbenzene 8260
920119436 WATER 1,2-Dibromo-3-chloropropane 8260
920119436 WATER 1,2-Dibromoethane 8260
Page 3 of 78
UNITS CONC QUAL OIL
ug/L 13000 50
ug/L 250 u 50
ug/L 2000 50
ug/L 250 u 50
ug/L 500 u 50
mg/L 0.054 1
mg/L 0.050 u 1
mg/L 41 1
mg/L 43 1
mg/L 50 ' 1
mg/L 50 •. 5
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u . 1
ug/L 8.6 u 1
mg/L 8.5 10
mg/L 190 2
ug/L 5.0 u 1
ug/L 31 1
ug/L 6.4 1
ug/L 180 1
ug/L 7.5 1
ug/L 19 . 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 130 j 100
ug/L 10 u 1
ug/L 56 1
ug/L 330 j 100
ug/L 56000 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697. 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
--~---Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119436 WATER 1,2-Dichlorobenzene 8260
920119436 WATER 1,2-Dichloroethane 8260
920119436 WATER 1,2-Dichloropropane 8260
920119436 WATER 1,3,5-Trimethylbenzene 8260
920119436 WATER 1,3-Dichlorobenzene 8260
920119436 WATER 1,3-Dichloropropane 8260
920119436 WATER 1,4-Dichlorobenzene 8260
920119436 WATER 2,2-Dichloropropane 8260
920119436 WATER 2-Chlorotoluene 8260
920119436 WATER 4-Chlorotoluene 8260
920119436 WATER Benzene 8260
920119436 WATER Bromobenzene 8260
920119436 WATER Bromochloromethane 8260
920119436 WATER Bromodichloromethane 8260
920119436 WATER Bromoform 8260
920119436 WATER Bromomethane 8260
920119436 WATER Carbon Tetrachloride 8260
920119436 WATER Chlorobenzene 8260
920119436 WATER Chlorodibromomethane 8260
920119436 WATER Chloroethane 8260
920119436 WATER Chloroform 8260
920119436 WATER Chloromethane 8260
920119436 WATER cis-1,2-Dichloroethene 8260
920119436 WATER Dibromomethane 8260
920119436 WATER Dichlorodifluoromethane 8260
920119436 WATER Ethylbenzene 8260
920119436 WATER Hexachlorobutadiene 8260
920119436 WATER lsopropylbenzene 8260
920119436 WATER m-Xylene and p-Xylene 8260
920119436 WATER Methylene chloride 8260
920119436 WATER n-Butylbenzene 8260
920119436 WATER n-Propylbenzene 8260
Page 4 of 78
UNITS CONG QUAL OIL ..
ug/L 51 1
ug/L 180 1
ug/L 18000 1
ug/L 30 1
ug/L 5.0 u 1
ug/L 150 J 100
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 6500 1
ug/L 81 1
ug/L 5.0 u 1
ug/L 5.2 1
ug/L 4.8 J 1
ug/L 10 u 1
ug/L 2500 1
ug/L 810 1
ug/L 1.4 J 1
ug/L 10 u 1
ug/L 70000 1
ug/L 10 u 1
ug/L 8.9 1
ug/L 22 1
ug/L 24 1
ug/L 640 1
ug/L 10 u ., 1
ug/L 16 1
ug/L 1500 1
ug/L 9000 1
ug/L 5.0 u 1
ug/L 12 1
August 4, 1997
- - --· --- - - - - - - - - - - - -
SAMPLE NAME -SAMPLED
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 FD02 0697 06/12/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed'.Base Laboratory Analyses
Lot 86 Superfund Site .
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119436 WATER Naphthalene 8260
920119436 WATER a-Xylene 8260
920119436 WATER p-lsopropyltoluene 8260
920119436 WATER sec-Butylbenzene 8260
920119436 WATER Styrene 8260
920119436 WATER tert-Butylbenzene 8260
920119436 WATER Tetrachloroethene 8260
920119436 WATER Toluene 8260
920119436 WATER trans-1,2-Dichloroethene 8260 -
920119436 WATER Trichloroethene 8260
920119436 WATER Trichlorofiuoromethane 8260
920119436 WATER Vinyl Chloride 8260
920118472 WATER Iron 200.7
920118472 WATER Iron, Dissolved 200.7
920118472 WATER Manganese 200.7
920118472 WATER Manganese, Dissolved 200.7
920118472 WATER Alkalinity, Total 310.1
920118472 WATER Chloride 325.3
920118472 WATER Sulfate 375.2
920118472 WATER Ethane 3810
920118472 WATER Ethene 3810
920118472 WATER Methane 3810
920118472 WATER Nitrogen, Nitrate 4500-NO3 F
920118472 WATER Total Organic Carbon 5310C
920118472 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118472 WATER 1, 1, 1-Trichloroethane 8260
920118472 WATER 1, 1,2,2-Tetrachloroethane 8260
920118472 WATER 1, 1,2-Trichloroethane 8260
920118472 WATER 1, 1-Dichloroethane 8260
920118472 WATER 1, 1-Dichloroethene 8260
Page 5 of 78
UNITS CONC QUAL OIL
ug/L 22 1
ug/L 1200 1
ug/L 2.1 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 820 1
ug/L 12000 1
ug/L 5.0 u 1
ug/L 1900 1
ug/L 33 1
ug/L 1.2 J 1
mg/L 0.54 1
mg/L 0.49 1
mg/L 6.9 1
mg/L 7.3 1
mg/L 35 1
mg/L 4.0 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.053 1
mg/L 18 1
ug/L 5.0 u 1
ug/L 47 1
ug/L 230 J 100
ug/L 41 1
ug/L 5.6 1
ug/L 34 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raieiyh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118472 WATER 1, 1-Dichloropropene 8260
920118472 WATER 1,2,3-Trichlorobenzene 8260
920118472 WATER 1,2,3-Trichloropropane 8260
920118472 WATER 1,2,4-Trichlorobenzene 8260
920118472 WATER 1,2,4-Trimethylbenzene 8260
920118472 WATER 1,2-Dibromo-3-chloropropane 8260
920118472 WATER 1,2-Dibromoethane 8260
920118472 WATER 1,2-Dichlorobenzene 8260
920118472 WATER 1,2-Dichloroethane 8260
920118472 WATER 1,2-Dichloropropane 8260
920118472 WATER 1,3,5-Trimethylbenzene 8260
920118472 WATER 1,3-Dichlorobenzene 8260
920118472 WATER 1,3-Dichloropropane 8260
920118472 WATER 1,4-Dichlorobenzene 8260
920118472 WATER 2,2-Dichloropropane 8260
920118472 WATER 2-Chlorotoluene . 8260
920118472 WATER 4-Chlorotoluene 8260
920118472 WATER Benzene 8260
920118472 WATER Bromobenzene 8260
920118472 WATER Bromochloromethane 8260
920118472 WATER Bromodichloromethane 8260
920118472 WATER Bromoform 8260
920118472 WATER Bromomethane 8260
920118472 WATER Carbon Tetrachloride 8260
920118472 WATER Chlorobenzene 8260
920118472 WATER Chlorodibromomethane 8260
920118472 WATER Chloroethane 8260
920118472 WATER Chloroform 8260
920118472 WATER Chloromethane 8260
920118472 WATER cis-1,2-Dichloroethene 8260
920118472 WATER Dibromomethane 8260
920118472 WATER Dichlorodifluoromethane 8260
Page 6 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 190 J 100
ug/L 5.0 u 1
ug/L 720 1
ug/L 2 J 1
ug/L 220 J 100
ug/L 4000 1
ug/L 74 1
ug/L 5.0 u 1
ug/L 5.8 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 7900 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 8.3 1
ug/L 4.6 J 1
ug/L 10 u 1
ug/L 1600 1
ug/L 370 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 60000 1
ug/L 10 u 1
ug/L 18 1
ug/L 5.0 u 1
ug/L 24 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW3 0697 06/11/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04· 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
-• Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118472 WATER Ethyl benzene 8260
920118472 WATER Hexachlorobutadiene 8260
920118472 WATER lsopropylbenzene 8260
920118472 WATER m-Xylene and p-Xylene 8260
920118472 WATER Methylene chloride 8260
920118472 WATER n-Butylbenzene 8260
920118472 WATER n-Propylbenzene 8260
920118472 WATER Naphthalene 8260
920118472 WATER a-Xylene 8260
920118472 WATER p-lsopropyltoluene 8260
920118472 WATER sec-Butylbenzene 8260
920118472 WATER Styrene 8260
920118472 WATER tert-Butylbenzene 8260
920118472 WATER Tetrachloroethene 8260
920118472 WATER Toluene 8260
920118472 WATER trans-1,2-Dichloroethene 8260
920118472 WATER Trichloroethene 8260
920118472 WATER Trichlorofluoromethane 8260
920118472 WATER Vinyl Chloride 8260
920116798 WATER Iron 200.7
920116798 WATER Iron, Dissolved 200.7
920116798 WATER Manganese 200.7
920116798 WATER Manganese, Dissolved 200.7
920116798 WATER Alkalinity, Total 310.1
920116798 WATER Chloride 325.3
920116798 WATER Sulfate 375.2
920116798 WATER Ethane 3810
920116798 WATER Ethene 3810
920116798 WATER Methane 3810
920116798 WATER Nitrogen, Nitrate 4500-NO3 F
Page 7 of 78
UNITS CONG QUAL OIL
ug/L 160 1
ug/L 10 u 1
ug/L 11 1
ug/L 380 1
ug/L 8300 1
ug/L 5.0 u 1
ug/L 14 1
ug/L 40 1
ug/L . 320 1
ug/L 3.8 J 1
ug/L 3.1 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 87 1
ug/L 3500 1
ug/L 2.1 J 1
ug/L 4800 1
ug/L 26 1
ug/L 10 u 1
mg/L 0.53 1
mg/L 0.050 u 1
mg/L 0.019 1
mg/L 0.010 u 1
mg/L 3.0 1
mg/L . 1.9 1
mg/L 5 •. u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.28 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 · 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697-06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 .0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
SAMPLE NO.
920116798
920116798
920116798
920116798
920116798
I l"\t Ra; C', ,,...,..,-f, ,.,.,.,r Ci♦,.,, ._..,~ vv ...,,..,.., ...... , ,u, ,u vnw
Raleigh, North Carolina
MATRIX COMPOUND/PARAMETER
WATER Total Organic Carbon
WATER 1, 1, 1,2-Tetrachloroethane
WATER 1, 1, 1-Trichloroethane
WATER 1, 1,2,2-Tetrachloroethane
WATER 1, 1,2-Trichloroethane
920116798 · WATER 1, 1-Dichloroethane
920116798 WATER 1, 1-Dichloroethene
920116798 WATER 1, 1-Dichloropropene
920116798 WATER 1,2,3-Trichlorobenzene
920116798 WATER 1,2,3-Trichloropropane
920116798 WATER 1,2,4-Trichlorobenzene
920116798 WATER 1,2,4-Trimethylbenzene
920116798 WATER 1,2-Dibromo-3-chloropropane
920116798 WATER 1,2-Dibromoethane
920116798 WATER 1,2-Dichlorobenzene
920116798 WATER 1,2-Dichloroethane
920116798 WATER 1,2-Dichloropropane
920116798 WATER 1,3,5-Trimethylbenzene
920116798 WATER 1,3-Dichlorobenzene
920116798 WATER 1,3-Dichloropropane
920116798 WATER 1,4-Dichlorobenzene
920116798 WATER 2,2-Dichloropropane
920116798 WATER 2-Chlorotoluene
920116798 WATER 4-Chlorotoluene
920116798 WATER Benzene
920116798 WATER Bromobenzene
920116798 WATER Bromochloromethane
920116798 WATER Bromodichloromethane
920116798 WATER Bromoform
920116798 WATER Bromomethane
920116798 WATER Carbon Tetrachloride
920116798 WATER Chlorobenzene
Page 8 of 78
METHOD
5310C
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
UNITS CONG QUAL OIL
mg/L 0.95 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 12 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1 .
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 72 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW04 0697 06/10/97
97191 MW6 0697 06/1 i/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
I nt RR ~11p.:i.rf11nri ~ita.
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116798 WATER Chlorodibromomethane 8260
920116798 WATER Chloroethane 8260
920116798 WATER Chloroform 8260
920116798 WATER Chloromethane 8260
920116798 WATER cis-1,2-Dichloroethene 8260
920116798 WATER Dibromomethane 8260
920116798 WATER Dichlorodifiuoromethane 8260
920116798 WATER Ethyl benzene 8260
920116798 WATER Hexachlorobutadiene 8260
920116798 WATER lsopropylbenzene 8260
920116798 WATER m-Xylene and p-Xylene 8260
920116798 WATER Methylene chloride 8260
920116798 WATER n-Butylbenzene 8260
920116798 WATER n-Propylbenzene 8260
920116798 WATER Naphthalene 8260
920116798 WATER o-Xylene 8260
' 920116798 WATER p-lsopropyltoluene 8260
920116798 WATER sec-Butylbenzene 8260
920116798 WATER Styrene 8260
920116798 WATER tert-Butylbenzene 8260.
920116798 WATER Tetrachloroethene 8260
920116798 WATER Toluene 8260
920116798 WATER trans-1,2-Dichloroethene 8260
920116798 WATER Trichloroethene 8260
920116798 WATER Trichlorofiuoromethane 8260
920116798 WATER Vinyl Chloride 8260
920118480 WATER Iron 200.7
920118480 WATER Iron, Dissolved 200.7
920118480 WATER Manganese 200.7
920118480 WATER Manganese, Dissolved 200.7
Page 9 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 2800 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 7.7 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 13 1
ug/L 1.5 J 1
ug/L 10 u 1
mg/L 0.22 1
mg/L 0.050 u 1
mg/L 18 1
mg/L 18 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
. 97191 MW6 0697 06/11/97
97191 MW6 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Sit~
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118480 WATER Alkalinity, Total 310.1
920118480 WATER Chloride 325.3
920118480 WATER Sulfate 375.2
920118480 WATER Ethane 3810
920118480 WATER Ethene 3810
920118480 WATER Methane 3810
920118480 WATER Nitrogen, Nitrate 4500-NO3 F
920118480 WATER Total Organic Carbon 5310C
920118480 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118480 WATER 1, 1, 1-Trichloroethane 8260
920118480 WATER 1, 1,2,2-Tetrachloroethane 8260
920118480 WATER 1, 1,2-Trichloroethane 8260
920118480 WATER 1, 1-Dichloroethane 8260
920118480 WATER 1, 1-Dichloroethene 8260
920118480 WATER 1, 1-Dichloropropene 8260
920118480 WATER 1,2,3-Trichlorobenzene 8260
920118480 WATER 1,2,3-Trichloropropane 8260
920118480 WATER 1,2,4-Trichlorobenzene 8260
920118480 WATER 1,2,4-Trimethylbenzene 8260
920118480 WATER 1,2-Dibromo-3-chloropropane 8260
920118480 WATER 1,2-Dibromoethane 8260
920118480 WATER 1,2-Dichlorobenzene 8260
920118480 WATER 1,2-Dichloroethane 8260
920118480 WATER 1,2-Dichloropropane 8260
920118480 WATER 1,3,5-Trimethylbenzene 8260
920118480 WATER 1,3-Dichlorobenzene 8260
920118480 WATER 1,3-Dichloropropane 8260
920118480 WATER 1,4-Dichlorobenzene 8260
920118480 WATER 2,2-Dichloropropane 8260
920118480 WATER 2-Chlorotoluene 8260
920118480 WATER 4-Chlorotoluene 8260
920118480 WATER Benzene 8260
Page 10 of 78
UNITS CONG QUAL DIL
mg/L 28 1 .
mg/L 53 5
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 31 2
ug/L 100 u 20
ug/L 30 J 20
ug/L 52 J 20
ug/L 100 u 20
ug/L 38 J 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 200 u 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 700 20
ug/L 220 20
ug/L 150 20
ug/L 3400 20
ug/L 20 J 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 200 u 20
ug/L 100 u 20
ug/L 100 u 20
ug/L 1300 20
August 4, 1997
- --- - - - - - - - - - -·-- - - -TABLE 1 -Results of Fixed-Base Laboratory Analyses
I nt AR C:11norf1 ,nrl C:ito -~-~-....... ,.. .... , , ................. ....
Raleigh, North Carolina
SAMPLE NAME SAMPLED SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD UNITS CONC QUAL OIL
97191 MW6 0697 06/11/97 920118480 WATER Bromobenzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Bromochloromethane 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Bromodichloromethane 8260 ug/L 610 20
97191 MW6 0697 06/11/97 920118480 WATER Bromoform 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Bromomethane 8260 ug/L 200 u 20
97191 MW6 0697 06/11/97 920118480 WATER Carbon Tetrachloride 8260 ug/L 2000 20
97191 MW6 0697 06/11/97 920118480 WATER Chlorobenzene 8260 ug/L 90 J 20
97191 MW6 0697 06/11/97 920118480 WATER Chlorodibromomethane 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Chloroethane 8260 ug/L 200 u 20
97191 MW6 0697 06/11/97 920118480 WATER Chloroform 8260 ug/L 50000 20
97191 MW6 0697 06/11/97 920118480 WATER Chloromethane 8260 ug/L 200 u 20
97191 MW6 0697 06/11/97 920118480 WATER cis-1,2-Dichloroethene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Dibromomethane 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Dichlorodifluoromethane 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Ethyl benzene 8260 ug/L 24 J 20
97191 MW6 0697 06/11/97 920118480 WATER Hexachlorobutadiene 8260 ug/L 200 u 20
97191 MW6 0697 06/11/97 920118480 WATER lsopropylbenzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER m-Xylene and p-Xylene 8260 ug/L 84 J 20
97191 MW6 0697 06/11/97 920118480 WATER Methylene chloride 8260 ug/L 3300 20
97191 MW6 0697 06/11/97 920118480 WATER n-Butylbenzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER n-Propylbenzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Naphthalene 8260 ug/L 200 u 20
97191 MW6 0697 06/11/97 920118480 WATER o-Xylene 8260 ug/L 220 20
97191 MW6 0697 06/11/97 920118480 WATER p-lsopropyltoluene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER sec-Butyl benzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Styrene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER tert-Butylbenzene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Tetrachloroethene 8260 ug/L 700 20
97191 MW6 0697 06/11/97 920118480 WATER Toluene 8260 ug/L 140 20
97191 MW6 0697 06/11/97 920118480 WATER trans-1,2-Dichloroethene 8260 ug/L 100 u 20
97191 MW6 0697 06/11/97 920118480 WATER Trichloroethene 8260 ug/L 1200 20
97191 MW6 0697 06/11/97 920118480 WATER Trichlorofluoromethane 8260 ug/L 100 u 20
August 4, 1997
Project 97191 Page 11 of 78
-------------------
SAMPLE NAME SAMPLED
97191 MW6 0697 06/11/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
SAMPLE NO.
920118480
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
920119444
I .... ~ oa: C', , ... ,....+, , ... ...1 c-:~ .... .._..,~ vv vup,;;11u1 ,u vnc:
Raleigh, North Carolina
MATRIX COMPOUND/PARAMETER
WATER Vinyl Chloride
WATER Iron
WATER Iron, Dissolved
WATER Manganese
WATER Manganese, Dissolved
WATER Alkalinity, Total
WATER Chloride
WATER Sulfate
WATER Ethane
WATER Ethene
WATER Methane
WATER Nitrogen, Nitrate
WATER Total Organic Carbon
WATER 1, 1, 1,2-Tetrachloroethane
WATER 1, 1, 1-Trichloroethane
WATER 1, 1,2,2-Tetrachloroethane
WATER 1, 1,2-Trichloroethane
WATER 1, 1-Dichloroethane
WATER 1, 1-Dichloroethene
WATER 1, 1-Dichloropropene
WATER 1,2,3-Trichlorobenzene
WATER 1,2,3-Trichloropropane
WATER 1,2,4-Trichlorobenzene
WATER 1,2,4-Trimethylbenzene
WATER 1,2-Dibromo-3-chloropropane
WATER 1,2-Dibromoethane
WATER 1,2-Dichlorobenzene
WATER 1,2-Dichloroethane
WATER 1,2-Dichloropropane
WATER 1,3,5-Trimethylbenzene
Page 12 of 78
METHOD
8260
200.7
200.7
200.7
200.7
310.1
325.3
375.2
3810
3810
3810
4500-NO3 F
5310C
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
UNITS CONG QUAL DIL
ug/L 200 u 20
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 4.1 1
mg/L 4.0 1
mg/L 19 1
mg/L 24 1
mg/L 12 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 54 4
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 440 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 250 . u 50
ug/L 260 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 550 50
ug/L 1600 50
ug/L 250 u 50
ug/L 110 J 50
ug/L 9600 50
ug/L 250 u 50
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0691 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
97191 MW07 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Let 36 Supeifund Slte
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119444 WATER 1,3-Dichlorobenzene 8260
920119444 WATER 1, 3-Dichloropropane 8260
920119444 WATER 1,4-Dichlorobenzene 8260
920119444 WATER 2,2-Dichloropropane 8260
920119444 WATER 2-Chlorotoluene 8260
920119444 WATER 4-Chlorotoluene 8260
920119444 WATER Benzene 8260
920119444 WATER Bromobenzene 8260
920119444 WATER Bromochloromethane 8260
920119444 WATER Bromodichloromethane 8260
920119444 WATER Bromoform 8260
920119444 WATER Bromomethane 8260
920119444 WATER Carbon Tetrachloride 8260
920119444 WATER Chlorobenzene 8260
920119444 WATER Chlorodibromomethane 8260
920119444 WATER Chloroethane 8260
920119444 WATER Chloroform 8260
920119444 WATER Chiaro methane 8260
920119444 WATER cis-1,2-Dichloroethene 8260
920119444 WATER Dibromomethane 8260
920119444 WATER Dichlorodifluoromethane 8260
920119444 WATER Ethylbenzene 8260
920119444 WATER Hexachlorobutadiene 8260
920119444 WATER lsopropylbenzene 8260
920119444 WATER m-Xylene and p-Xylene 8260
920119444 WATER Methylene chloride 8260
920119444 WATER n-Butylbenzene 8260
920119444 WATER n-Propylbenzene 8260
920119444 WATER Naphthalene 8260
920119444 WATER a-Xylene 8260
920119444 WATER p-lsopropyltoluene 8260
920119444 WATER sec-Butyl benzene 8260
Page 13 of 78
UNITS CONG QUAL DIL
ug/L 250 u 50
ug/L 95 J 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 6100 50
ug/L 250 u 50
ug/L 250 u· 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 155 J 50
ug/L 2000 50
ug/L 560 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 78000 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 85 J 50
ug/L 380 50
ug/L 500 u 50
ug/L 250 u 50
ug/L 1000 50
ug/L 14000 50
ug/L 250 u 50
ug/L 250 u 50
ug/L 500 u 50
ug/L 410 50
ug/L 250 u 50
ug/L 250 u 50
August 4, 1997
-------------------TABLE 1 -Results of Fixed-Base Laboratory Analyses
Raleigh, North Carolina
SAMPLE NAME SAMPLED SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD UNITS CONC QUAL OIL
97191 MW07 0697 06/12/97 920119444 WATER Styrene 8260 ug/L 250 u 50
97191 MW07 0697 06/12/97 920119444 WATER tert-Butylbenzene 8260 ug/L 250 u 50
97191 MW07 0697 06/12/97 920119444 WATER Tetrachloroethene 8260 ug/L 550 50
97191 MW07 0697 06/12/97 920119444 WATER Toluene 8260 ug/L 420 50
97191 MW07 0697 06/12/97 920119444 WATER trans-1,2-Dichloroethene 8260 ug/L 250 u 50
97191 MW07 0697 06/12/97 920119444 WATER Trichloroethene 8260 ug/L 1400 50
97191 MW07 0697 06/12/97 920119444 WATER Trichlorofluoromethane 8260 ug/L 250 u 50
97191 MW07 0697 06/12/97 920119444 WATER Vinyl Chloride 8260 ug/L 500 u 50
I
97191 MW08 0697 06/12/97 920119525 WATER Iron 200.7 mg/L 0.050 u 1
97191 MW08 0697 06/12/97 920119525 WATER Iron, Dissolved 200.7 mg/L 0.050 u 1
97191 MW08 0697 06/12/97 920119525 WATER Manganese 200.7 mg/L 0.085 1
97191 MW08 0697 06/12/97 920119525 WATER Manganese, Dissolved 200.7 mg/L 0.087 1
97191 MW08 0697 06/12/97 920119525 WATER Alkalinity, Total 310.1 mg/L 6.0 1
97191 MW08 0697 06/12/97 920119525 WATER Chloride 325.3 mg/L 6.3 1
97191 MW08 0697 06/12/97 920119525 WATER Sulfate 375.2 mg/L 5 u 1
97191 MW08 0697 06/12/97 920119525 WATER Ethane 3810 ug/L 16 u 1
97191 MW08 0697 06/12/97 920119525 WATER Ethene 3810 ug/L 15 u 1
97191 MW08 0697 06/12/97 920119525 WATER Methane 3810 ug/L 8.6 u 1
97191 MW08 0697 06/12/97 920119525 WATER Nitrogen, Nitrate 4500-NO3 F mg/L 0.78 1
97191 MW08 0697 06/12/97 920119525 WATER Total Organic Carbon 5310C mg/L 6.2 1
97191 MW08 0697 06/12/97 920119525 WATER 1, 1, 1,2-Tetrachloroethane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1, 1-Trichloroethane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1,2,2-Tetrachloroethane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1,2-Trichloroethane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1-Dichloroethane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1-Dichloroethene 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1, 1-Dichloropropene 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1,2,3,Trichlorobenzene 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1,2,3-Trichloropropane 8260 ug/L 500 u 100
97191 MW08 0697 06/12/97 920119525 WATER 1,2,4-Trichlorobenzene 8260 ug/L 1000 u 100
August 4, 1997
Project 97191 Page 14 of 78
-------------------
SAMPLE NAME SAMPLED
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 M'{\108 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Supeifund Site
Raleigh, North Carolin_a
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119525 WATER 1,2,4-Trimethylbenzene 8260
920119525 WATER 1,2-Dibromo-3-chloropropane 8260
920119525 WATER 1,2-Dibromoethane 8260
920119525 WATER 1,2-Dichlorobenzene 8260
920119525 WATER 1,2-Dichloroethane 8260
920119525 WATER 1,2-Dichloropropane 8260
920119525 WATER 1,3,5-Trimethylbenzene 8260
920119525 WATER 1,3-Dichlorobenzene 8260
920119525 WATER 1,3-Dichloropropane 8260
920119525 WATER 1,4-Dichlorobenzene 8260
920119525 WATER 2,2-Dichloropropane 8260
920119525 WATER 2-Chlorotoluene 8260
920119525 WATER 4-Chlorotoluene 8260
920119525 WATER Benzene 8260
920119525 WATER Bromobenzene 8260
920119525 WATER Bromochloromethane 8260
920119525 WATER Bromodichloromethane 8260
920119525 WATER Bromoform 8260
920119525 WATER Bromomethane 8260
920119525 WATER Carbon Tetrachloride 8260
920119525 WATER Chlorobenzene 8260
920119525 WATER Chlorodibromomethane 8260
920119525 WATER Chloroethane 8260
920119525 WATER Chloroform 8260
920119525 WATER Chloromethane 8260
920119525 WATER cis-1,2-Dichloroethene 8260
920119525 WATER Dibromomethane 8260
920119525 WATER Dichlorodifiuoromethane 8260
920119525 WATER Ethylbenzene 8260
920119525 WATER Hexachlorobutadiene 8260
920119525 WATER lsopropylbenzene 8260
920119525 WATER m-Xylene and p-Xylene 8260
Page 15 of78
UNITS CONC QUAL OIL
ug/L 500 u 100
ug/L 500 u 100
ug/L 5700 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 2000 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 5300 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 750 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 43000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L . 500 u 100
ug/L 500 u 100
ug/L . 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 230 J 100
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW08 0697 06/12/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
~ot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119525 WATER Methylene chloride 8260
920119525 WATER n-Butylbenzene 8260
920119525 WATER n-Propylbenzene 8260
920119525 WATER Naphthalene 8260
920119525 WATER o-Xylene 8260
920119525 WATER p-lsopropyltoluene 8260
920119525 WATER sec-Butylbenzene 8260
920119525 WATER Styrene 8260
920119525 WATER tert-Butylbenzene 8260
920119525 WATER Tetrachloroethene 8260
920119525 WATER Toluene 8260
920119525 WATER trans-1,2-Dichloroethene 8260
920119525 WATER Trichloroethene 8260
920119525 WATER Trichlorofluoromethane 8260
920119525 WATER Vinyl Chloride 8260
920116755 WATER Iron 200.7
920116755 WATER Iron, Dissolved 200.7
920116755 WATER Manganese 200.7
920116755 WATER Manganese, Dissolved 200.7
920116755 WATER Alkalinity, Total 310.1
920116755 WATER Chloride 325.3
920116755 WATER Sulfate 375.2
920116755 WATER Ethane 3810
920116755 WATER Ethene 3810
920116755 WATER Methane 3810
920116755 WATER Nitrogen, Nitrate 4500-NO3 F
920116755 WATER Total Organic Carbon 5310C
920116755 WATER 1, 1, 1,2-Tetrachloroethane 8260
920116755 WATER 1, 1, 1-Trichloroethane 8260
920116755 WATER 1, 1,2,2-Tetrachloroethane 8260
Page 16 of 78
UNITS CONG QUAL OIL
ug/L 6300 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 190 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 430 J 100
ug/L 500 u 100
ug/L 550 100
ug/L 500 u 100
ug/L 1000 u 100
mg/L 0.27 1
mg/L 0.050 u 1
mg/L 0.062 1
mg/L 0.060 1
mg/L 2.0 1
mg/L 3.5 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 1.4 10
mg/L 1.2 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116755 WATER 1, 1,2-Trichloroethane 8260
920116755 WATER 1, 1-Dichloroethane 8260
920116755 WATER 1, 1-Dichloroethene 8260
920116755 WATER 1, 1-Dichloropropene 8260
920116755 WATER 1,2,3-Trichlorobenzene 8260
920116755 WATER 1,2,3-Trichloropropane 8260
920116755 WATER 1,2,4-Trichlorobenzene 8260
920116755 WATER 1,2,4-Trimethylbenzene 8260
920116755 WATER 1,2-Dibromo-3-chloropropane 8260
920116755 WATER 1,2-Dibromoethane 8260
920116755 WATER 1,2-Dichlorobenzene 8260
920116755 WATER 1,2-Dichloroethane 8260
920116755 WATER 1,2-Dichloropropane 8260
920116755 WATER 1,3,5-Trimethylbenzene 8260
920116755 WATER 1,3-Dichlorobenzene 8260
920116755 WATER 1,3-Dichloropropane 8260
920116755 WATER 1,4-Dichlorobenzene 8260
920116755 WATER 2,2-Dichloropropane 8260
920116755 WATER 2-Chlorotoluene 8260
920116755 WATER 4-Chlorotoluene 8260
920116755 WATER Benzene 8260
920116755 WATER Bromobenzene 8260
920116755 WATER Bromochloromethane 8260
920116755 WATER Bromodichloromethane 8260
920116755 WATER Bromoform 8260
920116755 WATER Bromomethane 8260
920116755 WATER Carbon Tetrachloride 8260
920116755 WATER Chlorobenzene 8260
920116755 WAtt:R Chlorodibromomethane 8260
920116755 WATER Chloroethane 8260
920116755 WATER Chloroform 8260
920116755 WATER Chloromethane 8260
Page 17 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.Q u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
- - - - - - - - - - - - - --l!!!!!!!I l!!!!!!!I ~ ==
SAMPLE NAME SAMPLED
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10· 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW10 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116755 WATER cis-1,2-Dichloroethene 8260
920116755 WATER Dibromomethane 8260
920116755 WATER Dichlorodifluoromethane 8260
920116755 WATER Ethylbenzene 8260
920116755 WATER Hexachlorobutadiene 8260
920116755 WATER lsopropylbenzene 8260
920116755 WATER m-Xylene and p-Xylene 8260
920116755 WATER Methylene chloride 8260
920116755 WATER n-Butylbenzene . 8260
920116755 WATER n-Propylbenzene 8260
920116755 WATER Naphthalene 8260
920116755 WATER a-Xylene 8260
920116755 WATER p-lsopropyltoluene 8260
920116755 WATER sec-Butylbenzene 8260
920116755 WATER Styrene 8260
920116755 WATER tert-Butylbenzene 8260
920116755 WATER Tetrachloroethene 8260
920116755 WATER Toluene 8260
920116755 WATER trans-1,2-Dichloroethene 8260
920116755 WATER Trichloroethene 8260
920116755 WATER T richlorofl uoromethane 8260
920116755 WATER Vinyl Chloride 8260
920116801 WATER Iron 200.7
920116801 WATER Iron, Dissolved 200.7
920116801 WATER Manganese 200.7
920116801 WATER Manganese, Dissolved 200.7
920116801 WATER Alkalinity, Total 310.1
920116801 WATER Chloride 325.3
920116801 WATER Sulfate 375.2
920116801 WATER Ethane 3810
Page 18 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L. 5.0 u 1
ug/L 1.3 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 0.068 1
mg/L 0.053 1
mg/L 12 1
mg/L 2.8 1
mg/L 5 u 1
·ug/L 16 u 1
August 4, 1997
- - - - - - - - - - - - -11!!!!!!!1 l!!!!!!I . !!!!!I -== ==a
SAMPLE NAME SAMPLED
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116801 WATER Ethene 3810
920116801 WATER Methane 3810
920116801 WATER Nitrogen, Nitrate 4500-NO3 F
920116801 WATER Total Organic Carbon 5310C
920116801 WATER 1, 1, 1,2-Tetrachloroethane 8260
920116801 WATER 1, 1, 1-Trichloroethane 8260
920116801 WATER 1, 1,2,2-Tetrachloroethane 8260
920116801 WATER 1, 1,2-Trichloroethane 8260
920116801 WATER 1, 1-Dichloroethane 8260
920116801 WATER 1, 1-Dichloroethene 8260
920116801 WATER 1, 1-Dichloropropene 8260
920116801 WATER 1,2,3-Trichlorobenzene 8260
920116801 WATER 1,2,3-Trichloropropane 8260
920116801 WATER 1,2,4-Trichlorobenzene 8260
920116801 WATER 1,2,4-Trimethylbenzene 8260
920116801 WATER 1,2-Dibromo-3-chloropropane 8260
920116801 WATER 1,2-Dibromoethane 82~0
920116801 WATER 1,2-Dichlorobenzene 8260
920116801 WATER 1,2-Dichloroethane 8260
920116801 WATER 1,2-Dichloropropane 8260
920116801 WATER 1,3,5-Trimethylbenzene 8260
920116801 WATER 1,3-Dichlorobenzene 8260
920116801 WATER 1,3-Dichloropropane. 8260
920116801 WATER 1,4-Dichlorobenzene 8260
920116801 WATER 2,2-Dichloropropane 8260
920116801 WATER 2-Chlorotoluene 8260
920116801 WATER 4-Chlorotoluene 8260
920116801 WATER Benzene 8260
920116801 WATER Bromobenzene 8260
920116801 WATER Bromochloromethane 8260
920116801 WATER Bromodichloromethane 8260
920116801 WATER Bromoform 8260
Page 19 of 78
UNITS CONC QUAL OIL
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.72 1
mg/L 2.7 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 4.9 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 1
ug/L 5.0 U· 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 23 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - - - - - - - - - - - --I!!!!!!! !!!!!I !=i == m::liliil
SAMPLE NAME SAMPLED
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW11 0697 06/10/97
97191 MW12 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116801 WATER Bromomethane 8260
920116801 WATER Carbon Tetrachloride 8260
920116801 WATER Chlorobenzene 8260
920116801 WATER Chlorodibromomethane 8260
920116801 WATER Chloroethane 8260
920116801 WATER Chloroform 8260
920116801 WATER Chloromethane 8260
920116801 WATER cis-1,2-Dichloroethene 8260
920116801 WATER Dibromomethan·e 8260
920116801 WATER Dichlorodifluoromethane 8260
920116801 WATER Ethylbenzene 8260
920116801 WATER Hexachlorobutadiene 8260
920116801 WATER lsopropylbenzene 8260
920116801 WATER m-Xylene and p-Xylene 8260
920116801 WATER Methylene chloride 8260
920116801 WATER n-Butylbenzene 8260
920116801 WATER n-Propylbenzene 8260
920116801 WATER Naphthalene 8260
920116801 WATER a-Xylene 8260
920116801 WATER p-lsopropyltoluene 8260
920116801 WATER sec-Butylbenzene 8260
920116801 WATER Styrene 8260
920116801 WATER tert-Butylbenzene 8260
920116801 WATER Tetrachloroethene 8260
920116801 WATER Toluene 8260
920116801 WATER trans-1,2-Dichloroethene 8260
920116801 WATER Trichloroethene 8260
920116801 WATER Trichlorofluoromethane 8260
920116801 WATER Vinyl Chloride 8260
920119517 WATER Iron 200.7
Page 20 of 78
UNITS CONG QUAL OIL
ug/L 10 u 1
ug/L 23 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 4700 1
ug/L 10 u 1
ug/L 5.0, u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 84 1
ug/L 8.2 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 30 1
ug/L 2.6 J 1
ug/L 5.0 u 1
ug/L 12 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.050 u 1
August 4, 1997
- - - - - - - - - - - - -l!!!!!!!I l!!!!!!I l!!!!I == ~ ca;;
SAMPLE NAME SAMPLED
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 -06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfun_d Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119517 WATER Iron, Dissolved 200.7
920119517 WATER Manganese 200.7
920119517 WATER Manganese, Dissolved 200.7
920119517 WATER Alkalinity, Total 310.1
920119517 WATER Chloride 325.3
920119517 WATER Sulfate 375.2
920119517 WATER Ethane 3810
920119517 WATER Ethene 3810
920119517 WATER Methane 3810
920119517 WATER Nitrogen, Nitrate 4500-NO3 F
920119517 WATER Total Organic Carbon 5310C
920119517 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119517 WATER 1, 1, 1-Trichloroethane 8260
920119517 WATER 1, 1,2,2-Tetrachloroethane 8260
920119517 WATER 1, 1,2-Trichloroethane 8260
920119517 WATER 1, 1-Dichloroethane 8260
920119517 WATER 1, 1-Dichloroethene 8260
920119517 WATER 1, 1-Dichloropropene 8260
920119517 WATER 1,2,3-Trichlorobenzene 8260
920119517 WATER 1,2,3-Trichloropropane 8260
920119517 WATER 1,2,4-Trichlorobenzene 8260
920119517 WATER 1,2,4-Trimethylbenzene 8260
920119517 WATER 1,2-Dibromo-3-chloropropane 8260
920119517 WATER 1,2-Dibromoethane 8260
920119517 WATER 1,2-Dichlorobenzene 8260
920119517 WATER 1,2-Dichloroethane 8260
920119517 WATER 1,2-Dichloropropane 8260
920119517 WATER 1,3,5-Trimethylbenzene 8260
920119517 WATER 1,3-Dichlorobenzene 8260
920119517 WATER 1,3-Dichloropropane 8260
920119517 WATER 1,4-Dichlorobenzene 8260
920119517 WATER 2,2-Dichloropropane 8260
Page 21 of 78
UNITS CONG QUAL OIL
mg/L 0.050 u 1
mg/L 4.6 1
mg/L , 4.7 1
mg/L 2.0 1
mg/L 32 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.95 1
mg/L 69 4
ug/L 500 u 100
ug/L 500 u 100
ug/L 140 J 100
ug/L 6300 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 2000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 4700 100
ug/L 6300 100
ug/L 500 u 100
ug/L 320 J 100
ug/L 39000 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
August 4, 1997
- - - - - - - - - - - - -11!!!!!!1 I!!!! 1!!!!!11 == == i:aa
SAMPLE NAME SAMPLED
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119517 WATER 2-Chlorotoluene 8260
920119517 WATER 4-Chlorotoluene 8260
920119517 WATER Benzene 8260
920119517 WATER Bromobenzene 8260
920119517 WATER Bromochloromethane 8260
920119517 WATER Bromodichloromethane 8260
920119517 WATER Bromoform 8260
920119517 WATER Bromomethane 8260
920119517 WATER Carbon Tetrachloride 8260
920119517 WATER Chlorobenzene 8260
920119517 WATER Chlorodibromomethane 8260
920119517 WATER Chloroethane 8260
920119517 WATER Chloroform 8260
920119517 WATER Chloromethane 8260
920119517 WATER cis-1,2-Dichloroethene 8260
920119517 WATER Dibromomethane 8260
920119517 WATER Dichlorodifluoromethane 8260
920119517 WATER Ethylbenzene 8260
920119517 WATER Hexachlorobutadiene 8260
920119517 WATER lsopropylbenzene 8260
920119517 WATER m-Xylene and p-Xylene 8260
920119517 WATER Methylene chloride 8260
920119517 WATER n-Butylbenzene 8260
920119517 WATER n-Propylbenzene 8260
920119517 WATER Naphthalene 8260
920119517 WATER a-Xylene 8260
920119517 WATER p-lsopropyltoluene . 8260
920119517 WATER sec-Butylbenzene 8260
920119517 WATER Styrene 8260
920119517 WATER tert-Butylbenzene 8260
920119517 WATER Tetrachloroethene 8260
920119517 WATER Toluene 8260
Page 22 of 78
UNITS CONC QUAL DIL
ug/L 500 u 100
ug/L 500 u 100
ug/L 12000 100
ug/L 110 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 4700 100
ug/L 450 J 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 65000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 490 J 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 1500 100
ug/L 6900 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 810 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 7800 100
August 4, 1997
- - - - - - - - - - - - -l!!!!!!!I !!!!!I I!!!!! == m::;; lililii
SAMPLE NAME SAMPLED
97191 MW12 0697 06/12/97
97191 MW12 0697 06/12/97
97191 MW12 0697 06112/97
97191 MW12 0697 06112197
97191 FD01 0697 06112197
97191 FD01 0697 06/12/97
9719_1 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12197
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12197
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12197
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119517 WATER trans-1,2-Dichloroethene 8260
920119517 WATER Trichloroethene 8260
920119517 WATER Trichlorofluoromethane 8260
920119517 WATER Vinyl Chloride 8260
920119487 WATER Iron 200.7
920119487 WATER Iron, Dissolved 200.7
920119487 WATER Manganese 200.7
920119487 WATER Manganese, Dissolved 200.7
920119487 WATER Alkalinity, Total 310.1
920119487 WATER Chloride 325.3
920119487 WATER Sulfate 375.2
920119487 WATER Ethane 3810
920119487 WATER Ethene 3810
920119487 WATER Methane 3810
920119487 WATER Nitrogen, Nitrate 4500-NO3 F
920119487 WATER Total Organic Carbon 5310C
920119487 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119487 WATER 1, 1, 1-Trichloroethane 8260
920119487 WATER 1, 1,2,2-Tetrachloroethane 8260
920119487 WATER 1, 1,2-Trichloroethane 8260
920119487 WATER 1, 1-Dichloroethane 8260
920119487 WATER 1, 1-Dichloroethene 8260
920119487 WATER 1, 1-Dichloropropene 8260
920119487 WATER 1,2,3-Trichlorobenzene 8260
920119487 WATER 1,2,3-Trichloropropane 8260
920119487 WATER 1,2,4-Trichlorobenzene 8260
920119487 WATER 1,2,4-Trimethylbenzene 8260
920119487 WATER 1,2-Dibromo-3-chloropropane 8260
920119487 WATER 1,2-Dibromoethane 8260
920119487 WATER 1,2-Dichlorobenzene 8260
Page 23 of 78
UNITS CONC QUAL OIL
ug/L 500 u 100
ug/L 1100 100
ug/L 500 u 100
ug/L 1000 u 100
mg/L 0.050 u 100
mg/L 0.050 u 100
mg/L 4.5 100
mg/L 4.6 100
mg/L 4.0 100
mg/L 32 100
mg/L 5 u 100
ug/L 16 u 100
ug/L 15 u 100
ug/L 8.6 u 100
mg/L 0.94 100
mg/L 75 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 140 J 100
ug/L 5900 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1900 100
ug/L 1000 u 100
ug/L 110 J 100
ug/L 4400 100
ug/L 6500 100
ug/L 500 u 100
August 4, 1997
- - - - - - - - - - - - -1!!!11!! I!!!! l!!il!!=i == == liiiiilli
SAMPLE NAME SAMPLED
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 · 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119487 WATER 1,2-Dichloroethane 8260
920119487 WATER 1,2-Dichloropropane 8260
920119487 WATER 1,3,5-Trimethylbenzene 8260
920119487 WATER 1, 3-Dichlorobenzene 8260
920119487 WATER 1,3-Dichloropropane 8260
920119487 WATER 1,4-Dichlorobenzene 8260
920119487 WATER 2,2-Dichloropropane 8260
920119487 WATER 2-Chlorotoluene 8260
920119487 WATER 4-Chlorotoluene 8260
920119487 WATER Benzene 8260
920119487 WATER Bro mo benzene 8260
920119487 WATER Bromochloromethane 8260
920119487 WATER Bromodichloromethane 8260
920119487 WATER Bromoform 8260
920119487 WATER Bromomethane 8260
920119487 WATER Carbon Tetrachloride 8260
920119487 WATER Chlorobenzene 8260
920119487 WATER Chlorodibromomethane 8260
920119487 WATER Chloroethane 8260
920119487 WATER Chloroform 8260
920119487 WATER Chloromethane 8260.
920119487 WATER cis-1,2-Dichloroethene 8260
920119487 WATER Dibromomethane 8260
920119487 WATER Dichlorodifluoromethane 8260
920119487 WATER Ethylbenzene 8260
920119487 WATER Hexachlorobutadiene 8260
920119487 WATER lsopropylbenzene 8260
920119487 WATER m-Xylene and p-Xylene 8260
920119487 WATER Methylene chloride 8260
920119487 WATER n-Butylbenzene 8260
920119487 WATER n-Propylbenzene 8260
920119487 WATER Naphthalene 8260
Page 24 of 78
UNITS CONG QUAL OIL
ug/L 310 J 100
ug/L 34000 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 510 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 12000 100
ug/L 130 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 4900 100
ug/L 490 J 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 60000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 550 100
ug/L 1000 u 100
ug/L 500 u 100 /
ug/L 1700 100
ug/L 6800 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
August 4, 1997
- - - - - - - - - - - - -l!!!!!!!I I!!!!!! ~ == -llliiil
SAMPLE NAME SAMPLED
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 FD01 0697 06/12/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119487 WATER a-Xylene 8260
920119487 WATER p-lsopropyltoluene 8260
920119487 WATER sec-Butylbenzene 8260
920119487 WATER Styrene 8260
920119487 WATER tert-Butylbenzene 8260
920119487 WATER Tetrachloroethene 8260
920119487 WATER Toluene 8260
920119487 WATER trans-1,2-Dichloroethene 8260
920119487 WATER Trichloroethene 8260
920119487 WATER Trichlorofluoromethane 8260
920119487 WATER Vinyl Chloride 8260
920114345 WATER Iron 200.7
920114345 WATER Iron, Dissolved 200.7
920114345 WATER Manganese 200.7
920114345 WATER Manganese, Dissolved 200.7
920114345 WATER Alkalinity, Total 310.1
920114345 WATER Chloride 325.3
920114345 WATER Sulfate 375.2
920114345 WATER Ethane 3810
920114345 WATER Ethene 3810
920114345 WATER Methane 3810
920114345 WATER Nitrogen, Nitrate 4500-NO3 F
920114345 WATER Total Organic Carbon 5310C
920114345 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114345 WATER 1, 1, 1-Trichloroethane 8260
920114345 WATER 1, 1,2,2-Tetrachloroethane 8260
920114345 WATER 1, 1 ,2-Trichloroethane 8260
920114345 WATER 1, 1-Dichloroethane 8260
920114345 WATER 1, 1-Dichloroethene 8260
920114345 WATER 1, 1-Dichloropropene 8260
Page 25 of 78
UNITS CONC QUAL OIL
ug/L 840 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 7600 100
ug/L 50_0. u 100
ug/L 1100 100
ug/L 500 u 100
ug/L 1000 u 100
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 1.5 1
mg/L 1.6 1
mg/L 1.0 1
mg/L 8.9 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 9.0 10
mg/L 2.8 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
SAMPLE NAME SAMPLED
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
9719.1 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114345 WATER 1,2,3-Trichlorobenzene 8260
920114345 WATER 1,2,3-Trichloropropane 8260
920114345 WATER 1,2,4-Trichlorobenzene 8260
920114345 WATER 1,2,4-Trimethylbenzene 8260
920114345 WATER 1,2-Dibromo-3-chloropropane 8260
920114345 WATER 1,2-Dibromoethane 8260
920114345 WATER 1,2-Dichlorobenzene 8260
920114345 WATER 1,2-Dichloroethane 8260
920114345 WATER 1,2-Dichloropropan·e 8260
920114345 WATER 1, 3,5-T rimethylbenzene 8260
920114345 WATER 1,3-Dichlorobenzene 8260
920114345 WATER 1,3-Dichloropropane 8260
920114345 WATER 1,4-Dichlorobenzene 8260
920114345 WATER 2,2-Dichloropropane 8260
920114345 WATER 2-Chlorotoluene 8260
920114345 WATER 4-Chlorotoluene 8260
920114345 WATER Benzene 8260
920114345 WATER Bromobenzene 8260
920114345 WATER Bromochloromethane 8260
920114345 WATER Bromodichloromethane 8260
920114345 WATER Bromoform 8260
920114345 WATER Bromomethane 8260
920114345 WATER Carbon Tetrachloride 8260
920114345 WATER Chlorobenzene 8260
920114345 WATER Chlorodibromomethane 8260
920114345 WATER Chloroethane 8260
920114345 WATER Chloroform 8260
920114345 WATER Chloromethane 8260
920114345 WATER cis-1,2-Dichloroethene 8260
920114345 WATER Dibromomethane 8260
920114345 WATER Dichlorodifluoromethane 8260
920114345 WATER Ethylbenzene 8260
Page 26 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 3.4 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
SAMPLE NAME SAMPLED
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW13 0697 06/08/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114345 WATER Hexachlorobutadiene 8260
920114345 WATER lsopropylbenzene 8260
920114345 WATER m-Xylene and p-Xylene 8260
920114345 WATER Methylene chloride 8260
920114345 WATER n-Butylbenzene 8260
920114345 WATER n-Propylbenzene 8260
920114345 WATER Naphthalene 8260
920114345 WATER a-Xylene 8260
920114345 WATER p-lsopropyltoluene 8260
920114345 WATER sec-Butylbenzene 8260
920114345 WATER Styrene 8260
920114345 WATER tert-Butylbenzene 8260
920114345 WATER Tetrachloroethene 8260
920114345 WATER Toluene 8260
920114345 WATER trans-1,2-Dichloroethene 8260
920114345 WATER Trichloroethene 8260
920114345 WATER Trichlorofiuoromethane 8260
920114345 WATER Vinyl Chloride 8260
920116780 WATER Iron 200.7
920116780 WATER Iron, Dissolved 200.7
920116780 WATER Manganese 200.7
920116780 WATER Manganese, Dissolved 200.7
920116780 WATER Alkalinity, Total 310.1
920116780 WATER Chloride 325.3
920116780 WATER Sulfate 375.2
920116780 WATER Ethane 3810
920116780 WATER Ethene 3810
920116780 WATER Methane 3810
920116780 WATER Nitrogen, Nitrate 4500-NO3 F
920116780 WATER Total Organic Carbon 5310C
Page 27 of 78
UNITS CONC QUAL OIL
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 ·U 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1.3 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.32 1
mg/L 0.050 u 1
mg/L 0.099 1
mg/L 0.099 1
mg/L 7.0 1
mg/L 4.0 1
mg/L 5 u· 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.41 1
mg/L 1. 1 1
August 4, 1997
- -·-- - - - - - - - - - - --!!!!!!I ==i liiliil
SAMPLE NAME SAMPLED
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97 .
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/i 0/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116780 WATER 1, 1, 1,2-Tetrachloroethane 8260
920116780 WATER 1, 1, 1-Trichloroethane 8260
920116780 WATER 1, 1,2,2-Tetrachloroethane 8260
920116780 WATER 1, 1,2-Trichloroethane 8260
920116780 WATER 1, 1-Dichloroethane 8260
920116780 WATER 1, 1-Dichloroethene 8260
920116780 WATER 1, 1-Dichloropropene 8260
920116780 WATER 1,2,3-Trichlorobenzene 8260
920116780 WATER 1,2,3-Trichloropropane 8260
920116780 WATER 1,2,4-Trichlorobenzene 8260
920116780 WATER 1,2,4-Trimethylbenzene 8260
920116780 WATER 1,2-Dibromo-3-chloropropane 8260
920116780 WATER 1,2-Dibromoethane 8260
920116780 WATER 1,2-Dichlorobenzene 8260
920116780 WATER 1,2-Dichloroethane 8260
920116780 WATER 1,2-Dichloropropane 8260
920116780 WATER 1,3,5-Trimethylbenzene 8260
920116780 WATER 1,3-Dichlorobenzene 8260
920116780 WATER 1,3-Dichloropropane 8260
920116780 WATER 1,4-Dichlorobenzene 8260
920116780 WATER 2,2-Dichloropropane 8260
920116780 WATER 2-Chlorotoluene 8260
920116780 WATER 4-Chlorotoluene 8260
920116780 WATER Benzene 8260
920116780 WATER Bromobenzene 8260
920116780 WATER Bromochloromethane 8260
920116780 WATER Bromodichloromethane 8260
920116780 WATER Bromoform 8260
920116780 WATER Bromomethane 8260
920116780 WATER Carbon Tetrachloride 8260
920116780 WATER Chlorobenzene 8260
920116780 WATER Chlorodibromomethane 8260
Page 28 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u < ' ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - --·· ---- - - - - - - --1!!!!!!11 =a -
SAMPLE NAME SAMPLED
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15. 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191· MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW15 0697 06/10/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MVl/16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116780 WATER Chloroethane 8260
920116780 WATER Chloroform 8260
920116780 WATER Chloromethane 8260
920116780 WATER cis-1,2-Dichloroethene 8260
920116780 WATER Dibromomethane 8260
920116780 WATER Dichlorodifluoromethane 8260
920116780 WATER Ethylbenzene 8260
920116780 WATER Hexachlorobutadiene 8260
920116780 WATER lsopropylbenzene 8260
920116780 WATER m-Xylene and p-Xylene 8260
920116780 WATER Methylene chloride 8260
920116780 WATER n-Butylbenzene 8260
920116780 WATER n-Propylbenzene 8260
920116780 WATER Naphthalene 8260
920116780 WATER a-Xylene 8260
920116780 WATER p-lsopropyltoluene 8260
920116780 WATER sec-Butylbenzene 8260
920116780 WATER Styrene 8260
920116780 WATER tert-Butylbenzene 8260
920116780 WATER Tetrachloroethene 8260
920116780 WATER Toluene 8260
920116780 WATER trans-1,2-Dichloroethene 8260
920116780 WATER Trichloroethene 8260
920116780 WATER Trichlorofluoromethane 8260
920116780 WATER Vinyl Chloride 8260
920119509 WATER Iron 200.7
920119509 WATF=R Iron, Dissolved 200.7
920119509 WATER Manganese 200.7
920119509 WATER Manganese, Dissolved 200.7
920119509 WATER Alkalinity, Total 310.1
Page 29 of 78
UNITS CONC QUAL OIL
ug/L 10 u 1
ug/L 30 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0. u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.97 1
mg/L 0.97 1
mg/L 15 1
mg/L 15 1
mg/L 39 1
August 4, 1997
SAMPLE NAME SAMPLED
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119509 WATER Chloride 325.3
920119509 WATER Sulfate 375.2
920119509 WATER Ethane 3810
920119509 WATER Ethene 3810
920119509 WATER Methane 3810
920119509 WATER Nitrogen, Nitrate 4500-NO3 F
920119509 WATER Total Organic Carbon 5310C
920119509 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119509 WATER 1, 1, 1-Trichloroethane 8260
920119509 WATER 1, 1,2,2-Tetrachloroethane 8260
920119509 WATER 1, 1,2-Trichloroethane 8260
920119509 WATER 1, 1-Dichloroethane 8260
920119509 WATER 1, 1-Dichloroethene 8260
920119509 WATER 1,1-Dichloropropene 8260
920119509 WATER 1,2,3-Trichlorobenzene 8260
920119509 WATER 1,2,3-Trichloropropane 8260
920119509 WATER 1,2,4-Trichlorobenzene 8260
920119509 WATER 1,2,4-Trimethylbenzene 8260
920119509 WATER 1,2-Dibromo-3-chloropropane 8260
920119509 WATER 1,2-Dibromoethane 8260
920119509 WATER 1,2-Dichlorobenzene 8260
920119509 WATER 1,2-Dichloroethane 8260
920119509 .. WATER 1,2-Dichloropropane 8260
920119509 WATER 1,3,5-Trimethylbenzene 8260
920119509 WATER 1,3-Dichlorobenzene 8260
920119509 WATER 1,3-Dichloropropane 8260
920119509 WATER 1,4-Dichlorobenzene 8260
920119509 WATER 2,2-Dichloropropane 8260
920119509 WATER 2-Chlorotoluene 8260
920119509 WATER 4-Chlorotoluene 8260
920119509 WATER Benzene 8260
920119509 WATER Bromobenzene 8260
Page 30 of 78
UNITS CONG QUAL OIL
mg/L 10 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 73 1
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 390 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L . 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 5300 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 4400 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 3300 100
ug/L 500 u 100
August 4, 1997
- - - - - - - --· - - - - - - -l!!!!!!!!!!!I == -
SAMPLE NAME SAMPLED
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 .0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
97191 MW16 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119509 WATER Bromochloromethane 8260
920119509 WATER Bromodichloromethane 8260
920119509 WATER Bromoform 8260
920119509 WATER· Bromomethane 8260
920119509 WATER Carbon Tetrachloride 8260
920119509 WATER Chlorobenzene 8260
920119509 WATER Chlorodibromomethane 8260
920119509 WATER Chloroethane 8260
920119509 WATER Chloroform 8260
920119509 · WATER Chloromethane 8260
920119509 WATER cis-1,2-Dichloroethene 8260
920119509 WATER Dibromomethane 8260 ·
920119509 WATER Dichlorodifluoromethane 8260
920119509 WATER Ethylbenzene 8260
· 920119509 WATER Hexachlorobutadiene 8260
920119509 WATER lsopropylbenzene 8260
920119509 WATER m-Xylene and p-Xylene 8260
920119509 · WATER Methylene chloride 8260
920119509 WATER n-Butylbenzene 8260
920119509 WATER n-Propylbenzene 8260
920119509 WATER Naphthalene 8260
920119509 WATER o-Xylene 8260
920119509 WATER p-lsopropyltoluene 8260
920119509 WATER sec-Butylbenzene 8260
920119509 WATER Styrene 8260
920119509 WATER tert-Butylbenzene 8260
920119509 WATER Tetrachloroethene 8260
920119509 WATER Toluene 8260
920119509 WATER trans-1,2-Dichloroethene 8260
920119509 WATER Trichloroethene 8260 ·
920119509 WATER Trichlorofluoromethane 8260
920119509 WATER Vinyl Chloride 8260
Page 31 of 78
UNITS CONG QUAL DIL
ug/L 500 U, 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 1100 100
ug/L 400 J 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 35000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 380 J 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 1300 100
ug/L 1400 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 630 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1800 100
ug/L 9400 100
ug/L 500 u 100
ug/L 3400 100
ug/L 500 u 100
ug/L 1000 u 100
August 4, 1997
·-- - - - - - - - - - - - - --!!!!I == liliiiil
SAMPLE NAME
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
9.7191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
97191 MW17 0697
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLED SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
06/10/97 920116763 WATER Iron 200.7
06/10/97 920116763 WATER Iron, Dissolved 200.7
06/10/97 920116763 WATER Manganese 200.7
06/10/97 920116763 WATER Manganese, Dissolved 200.7
06/10/97 920116763 WATER Alkalinity, Total 310.1
06/10/97 920116763 WATER Chloride 325.3
06/10/97 920116763 WATER Sulfate 375.2 ·
06/10/97 920116763 WATER Ethane 3810
06/10/97 920116763 WATER Ethene 3810
06/10/97 920116763 WATER Methane 3810
06/10/97 920116763 WATER Nitrogen, Nitrate 4500-NO3 F
06/10/97 920116763 WATER Total Organic Carbon 5310C
06/10/97 920116763 WATER 1, 1, 1,2-Tetrachloroethane 8260
06/10/97 920116763 WATER 1, 1, 1-Trichloroethane 8260
06/10/97 920116763 WATER 1, 1,2,2-Tetrachloroethane 8260
06/10/97 920116763 WATER 1, 1,2-Trichloroethane 8260
06/10/97 920116763 WATER 1, 1-Dichloroethane 8260
06/10/97 920116763 WATER 1, 1-Dichloroethene 8260
06/10/97 920116763 WATER 1, 1-Dichloropropene 8260
06/10/97 920116763 WATER 1,2,3-Trichlorobenzene 8260
06/10/97 920116763 WATER 1,2,3-Trichloropropane 8260
06/10/97 920116763 WATER 1,2,4-Trichlorobenzene 8260
06/10/97 920116763 WATER 1,2,4-Trimethylbenzene 8260
06/10/97 920116763 WATER 1,2-Dibromo-3,chloropropane 8260
06/10/97 920116763 WATER 1,2-Dibromoethane 8260
06/10/97 920116763 WATER 1,2-Dichlorobenzene 8260
06/10/97 920116763 WATER 1,2-Dichloroethane 8260
06/10/97 920116763 WATER 1,2-Dichloropropane 8260
06/10/97 920116763 WATER 1,3,5-Trimethylbenzene 8260
06/10/97 920116763 WATER 1, 3-Dichlorobenzene 8260
Page 32 of 78
UNITS CONC QUAL DIL
mg/L 0.47 1
mg/L 0.050 u 1
mg/L 0.073 1
mg/L 0.063 1
mg/L 2.0 1
mg/L 3.7 1
ing/l 5 u 1
ug/L 16 u 1
· ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.59 .. 1
mg/L 1.0 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 9.7 -1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-- -·-- - - - --- - - - --!!ml ;a; -
SAMPLE NAME SAMPLED
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17. 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/91
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116763 WATER 1,3-Dichloropropane 8260
920116763 WATER 1,4-Dichlorobenzene 8260
920116763 WATER 2,2-Dichloropropane 8260
920116763 WATER 2-Chlorotoluene 8260
920116763 WATER 4-Chlorotoluene 8260
920116763 WATER Benzene 8260
920116763 WATER Bromobenzene 8260
920116763 WATER Bromochloromethane 8260
920116763 · WATER Bromodichloromethane 8260
920116763 WATER Bromoform 8260
920116763 WATER Bromomethane 8260
920116763 WATER Carbon Tetrachloride 8260
920116763 WATER Chlorobenzene 8260
920116763 WATER Chlorodibromomethane 8260
920116763 WATER Chloroethane 8260
920116763 WATER Chloroform 8260
920116763 WATER Chloromethane 8260
920116763 WATER cis-1,2-Dichloroethene 8260
920116763 WATER Dibromomethane 8260
920116763 WATER Dichlorodifluoromethane 8260
920116763 WATER Ethylbenzene 8260
920116763 WATER Hexachlorobutadiene 8260
920116763 WATER lsopropylbenzene 8260
920116763 WATER m-Xylene and p-Xylene 8260
920116763 WATER Methylene chloride 8260
920116763 WATER n-Butylbenzene 8260
920116763 WATER n-Propylbenzene 8260
920116763 WATER Naphthalene 8260
920116763 WATER o-Xylene 8260
920116763 WATER p-lsopropyltoluene 8260
920116763 WATER sec-Butylbenzene 8260
920116763 WATER Styrene 8260
Page 33 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 12 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 9.0 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0. u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-- - ---- - - - - - - - --1!!!!!!!1 !!!I ;a;;
SAMPLE NAME SAMPLED
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW17 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
. 97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 M\JV27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Supeliund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116763 WATER tert-Butylbenzene 8260
920116763 WATER Tetrachloroethene 8260
920116763 WATER Toluene 8260
920116763 WATER trans-1,2-Dichloroethene 8260
920116763 WATER Trichloroethene 8260
920116763 WATER Trichlorofluoromethane 8260
920116763 WATER Vinyl Chloride 8260
920116771 WATER Iron 200.7
920116771 WATER Iron, Dissolved 200.7
920116771 WATER Manganese 200.7
920116771 WATER Manganese, Dissolved 200.7
920116771 WATER Alkalinity, Total 310.1
920116771 WATER Chloride 325.3
920116771 WATER Sulfate 375.2
920116771 WATER Ethane 3810
920116771 WATER Ethene 3810
920116771 WATER Methane 3810
920116771 WATER Nitrogen, Nitrate 4500-NO3 F
920116771 WATER Total Organic Carbon 5310C
920116771 WATER 1, 1, 1,2-Tetrachloroethane 8260
920116771 WATER 1, 1, 1-Trichloroethane 8260
920116771 WATER 1, 1,2,2-Tetrachloroethane 8260
920116771 WATER 1, 1,2-Trichloroethane 8260
920116771 WATER 1, 1-Dichloroethane 8260
920116771 WATER 1, 1-Dichloroethene 8260
920116771 WATER 1, 1-Dichloropropene 8260
920116771 WATER 1,2,3-Trichlorobenzene 8260
920116771 WATER 1,2,3-Trichloropropane 8260
920116771 WATER 1,2,4-Trichlorobenzene 8260
920116771 WATER 1,2,4-Trimethylbenzene 8260
Page 34 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 13 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 9.3 1
mg/L 0.050 u 1
mg/L 0.47 1
mg/L · 0.050. -1
mg/L 7.0 1
mg/L 3.5 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0:71 1
mg/L 1.9 1
ug/L 50 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u ' I
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
- - - - - - - - - - - - - - - -I!!!!! == ..
SAMPLE NAME SAMPLED
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 . 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
9719.1 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MVV27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116771 WATER 1,2-Dibromo-3-chloropropane 8260
920116771 WATER 1,2-Dibromoethane 8260
920116771 WATER 1,2-Dichlorobenzene 8260
920116771 WATER 1,2-Dichloroethane 8260
920116771 WATER 1,2-Dichloropropane 8260
920116771 WATER 1,3,5-Trimethylbenzene 8260
920116771 WATER 1,3-Dichlorobenzene 8260
920116771 WATER 1,3-Dichloropropane 8260
920116771 WATER 1,4-Dichlorobenzene 8260
920116771 WATER 2,2-Dichloropropane 8260
920116771 WATER 2-Chlorotoluene 8260
920116771 WATER 4-Chlorotoluene 8260
920116771 WATER Benzene 8260
920116771 WATER Bromobenzene 8260
920116771 WATER Bromochloromethane 8260
920116771 WATER Bromodichloromethane 8260
920116771 WATER Bromoform 8260
920116771 WATER Bromomethane 8260
920116771 WATER Carbon Tetrachloride 8260
920116771 WATER Chlorobenzene 8260
920116771 WATER Chlorodibromomethane 8260
920116771 WATER Chloroethane 8260
920116771 WATER Chloroform 8260
920116771 WATER Chloromethane 8260
920116771 WATER cis-1,2-Dichloroethene 8260
920116771 WATER Dibromomethane 8260
920116771 WATER Dichlorodifluoromethane 8260
920116771 WATER Ethyl benzene 8260
920116771 WATER Hexachlorobutadiene 8260
920116771 WATER lsopropylbenzene 8260
920116771 WATER m-Xylene and p-Xylene 8260
920116771 WATER Methylene chloride 8260
Page 35 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
-ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 2.6 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 8.7 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 LJ_ 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- ----- ---- - - - - - - --I!!!!!!==
SAMPLE NAME SAMPLED
97191 M\/V2.7 0697 06/10/97
97191 MVV2.7 0697 06/10/97
97191 MVV2.7 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW27 0697 06/10/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116771 WATER n-Butylbenzene 8260
920116771 WATER n-Propylbenzene 8260
920116771 WATER Naphthalene 8260
920116771 WATER a-Xylene 8260
920116771 WATER p-lsopropyltoluene 8260
920116771 WATER sec-Butyl benzene 8260
920116771 WATER Styrene 8260
920116771 WATER tert-Butylbenzene 8260
920116771 WATER Tetrachloroethene 8260
920116771 WATER Toluene 8260
920116771 WATER trans-1,2-Dichloroethene 8260
920116771 WATER Trichloroethene 8260
920116771 WATER Trichlorofluoromethane 8260
920116771 WATER Vinyl Chloride --8260 -
-
920114914 WATER Iron 200.7
920114914 WATER Iron, Dissolved 200.7
920114914 WATER Manganese 200.7
920114914 WATER Manganese, Dissolved 200.7
920114914 WATER Alkalinity, Total 310.1
920114914 WATER Chloride 325.3
920114914 WATER Sulfate 375.2
920114914 WATER Ethane 3810
920114914 WATER Ethene 3810
920114914 WATER Methane 3810
920114914 WATER Nitrogen, Nitrate 4500-NO3 F
920114914 WATER Total Organic Carbon 5310C
920114914 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114914 WATER 1, 1, 1-Trichloroethane 8260
920114914 WATER 1, 1,2,2-Tetrachloroethane 8260
920114914 WATER 1, 1,2-Trichloroethane 8260
Page 36 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1.3 J 1
ug/L 5.0 u 1
Ug/L 10 u 1
mg/L 2.3 1
mg/L 0.050 u 1
mg/L 0.024 1
mg/L 0.010 1
mg/L 6.0 1
mg/L 3.5 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.20 1
mg/L 0.84 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-----------------~-
SAMPLE NAME SAMPLED
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697. 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97.
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114914 WATER 1, 1-Dichloroethane 8260
920114914 WATER 1, 1-Dichloroethene 8260
920114914 WATER 1, 1-Dichloropropene 8260
920114914 WATER 1,2,3-Trichlorobenzene 8260
920114914 WATER 1,2,3-Trichloropropane 8260
920114914 WATER 1,2,4-Trichlorobenzene 8260
920114914 WATER 1,2,4-Trimethylbenzene 8260
920114914 WATER 1,2-Dibromo-3-chloropropane 8260
920114914 WATER 1,2-Dibromoethane 8260 -
920114914 WATER 1,2-Dichlorobenzene 8260
920114914 WATER 1,2-Dichloroethane 8260
920114914 WATER 1,2-Dichloropropane 8260
920114914 WATER 1,3,5-Trimethylbenzene 8260
920114914 WATER 1,3-Dichlorobenzene 8260
920114914 WATER 1,3-Dichloropropane 8260
920114914 WATER 1,4-Dichlorobenzene 8260
920114914 WATER 2 ,2-Dichloropropane 8260
920114914 WATER 2-Chlorotoluene 8260
920114914 WATER 4-Chlorotoluene 8260
920114914 WATER Benzene 8260
920114914 WATER Bromobenzene 8260
920114914 WATER Bromochloromethane 8260
920114914 WATER Bromodichloromethane 8260
920114914 WATER Bromoform 8260
920114914 WATER Bromomethane 8260
920114914 WATER Carbon Tetrachloride 8260
920114914 WATER Chlorobenzene 8260
920114914 WATER Chlorodibromomethane 8260
920114914 WATER Chloroeihane 8260
920114914 WATER Chloroform 8260
920114914 WATER Chloromethane 8260
920114914 WATER cis-1,2-Dichloroethene 8260
Page 37 of 78
UNITS CONG QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
· ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
--·----------------
SAMPLE NAME SAMPLED
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW32 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114914 WATER Dibromomethane 8260
920114914 WATER Dichlorodifluoromethane 8260
920114914 WATER Ethylbenzene 8260
920114914 WATER Hexachlorobutadiene 8260
920114914 WATER lsopropylbenzene 8260
920114914 WATER m-Xylene and p-Xylene 8260
920114914 WATER Methylene chloride 8260
920114914 WATER n-Butylbenzene 8260
920114914 WATER n-Propylbenzene 8260
920114914-WATER Naphthalene 8260
920114914 WATER a-Xylene 8260
920114914 WATER p-lsopropyltoluene 8260
920114914 WATER sec-Butylbenzene 8260
920114914 WATER Styrene 8260
920114914 WATER tert-Butylbenzene 8260
920114914 WATER Tetrachloroethene 8260
920114914 WATER Toluene 8260
920114914 WATER trans-1,2-Dichloroethene 8260
920114914 WATER Trichloroethene 8260
920114914 WATER Trichlorofluoromethane 8260
920114914 WATER Vinyl Chloride 8260
920114892 WATER Iron 200.7
920114892 WATER Iron, Dissolved 200.7
920114892 WATER Manganese 200.7
920114892 WATER Manganese, Dissolved 200.7
920114892 WATER Alkalinity, Total 310.1
920114892 WATER Chloride 325.3
920114892 WATER Sulfate 375.2
920114892 WATER Ethane 3810
920114892 WATER Ethene 3810
Page 38 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
. ug/L 5.0 -U 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1.2 j 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.31 1
mg/L 0.050 u 1
mg/L 0.012 1
mg/L 0.010 u 1
mg/L 26 1
mg/L 2.1 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
August 4, 1997
11!11 -- - - - ----- - - - - - - - --
SAMPLE NAME SAMPLED
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0691 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114892 WATER Methane 3810
920114892 WATER Nitrogen, Nitrate 4500-N03 F
920114892 WATER Total Organic Carbon 5310C
920114892 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114892 WATER 1, 1, 1-Trichloroethane 8260
920114892 WATER 1, 1,2,2-Tetrachloroethane 8260
920114892 WATER 1, 1,2-Trichloroethane 8260
920114892 WATER 1, 1-Dichloroethane 8260
920114892 WATER 1, 1-Dichloroethene 8260
920114892 WATER 1, 1-Dichloroproperie 8260
920114892 WATER 1,2,3-Trichlorobenzene 8260
920114892 WATER 1,2,3-Trichloropropane 8260
920114892 WATER 1,2,4-Trichlorobenzene 8260
920114892 WATER 1,2,4-Trimethylbenzene 8260
920114892 WATER 1,2-Dibromo-3-chloropropane 8260
920114892 WATER 1,2-Dibromoethane 8260
920114892 WATER 1,2-Dichlorobenzene 8260
920114892 WATER 1,2-Dichloroethane 8260
920114892 WATER 1,2-Dichloropropane 8260
920114892 WATER 1,3,5-Trimethylbenzene 8260
920114892 WATER 1,3-Dichlorobenzene 8260
920114892 WATER 1, 3-Dichloropropane 8260
920114892 WATER 1,4-Dichlorobenzene 8260
920114892 WATER 2,2-Dichloropropane 8260
920114892 WATER 2-Chlorotoluene 8260
920114892 WATER 4-Chlorotoluene 8260
920114892 WATER Benzene 8260
920114892 WATER Bromobenzene 8260
920114892 WATER Bromochloromethane 8260
920114892 WATER Bromodichloromethane 8260
920114892 WATER Bromoform 8260
920114892 WATER Bromomethane 8260
Page 39 of 78
UNITS CONC QUAL OIL
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 0.67 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ugll 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-- - - - ---·-- - - - - - - - - -
SAMPLE NAME SAMPLED
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97 -
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW33 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114892 WATER Carbon Tetrachloride 8260
920114892 WATER Chlorobenzene 8260
920114892 WATER Chlorodibromomethane 8260
920114892 WATER Chloroethane 8260
920114892 WATER Chloroform 8260
920114892. WATER Chloromethane 8260
920114892 WATER cis-1,2-Dichloroethene 8260
920114892 WATER Dibromomethane 8260
920114892 WATER Dichlorodifluoromethane 8260
920114892 WATER Ethylbenzene 8260
920114892 WATER Hexachlorobutadiene 8260
920114892 WATER lsopropylbenzene 8260
920114892 WATER m-Xylene and p-Xylene 8260
920114892 WATER Methylene chloride 8260
920114892 WATER n-Butylbenzene 8260
920114892 WATER n-Propylbenzene 8260
920114892 WATER Naphthalene 8260
920114892 WATER a-Xylene 8260
920114892 WATER p-lsopropyltoluene 8260
920114892 WATER sec-Butyl benzene 8260
920114892 WATER Styrene 8260
920114892 WATER tert-Butylbenzene 8260
920114892 WATER Tetrachloroethene 8260
920114892 WATER Toluene 8260
920114892 WATER trans-1,2-Dichloroethene 8260
920114892 WATER Trichloroethene 8260
920114892 WATER Trichlorofluoromethane 8260
920114892 WATER Vinyl Chloride 8260
920114922 WATER Iron 200.7
920114922 WATER I ran, Dissolved 200.7
Page 40 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1.4 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 1.7 1
mg/L 0.050 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114922 WATER Manganese 200.7
920114922 WATER Manganese, Dissolved 200.7
920114922 WATER Alkalinity, Total 310.1
920114922 WATER Chloride 325.3
920114922 WATER Sulfate 375.2
920114922 WATER Ethane 3810
920114922 WATER Ethene 3810
920114922 WATER Methane 3810
920114922 WATER Nitrogen, Nitrate 4500-NO3 F
920114922 WATER Total Organic Carbon 5310C
920114922 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114922 WATER 1, 1, 1-Trichloroethane 8260
920114922 WATER 1, 1,2,2-Tetrachloroethane 8260
920114922 WATER 1, 1,2-Trichloroethane 8260
920114922 WATER 1, 1-Dichloroethane 8260
920114922 WATER 1, 1-Dichloroethene 8260
920114922 WATER 1, 1-Dichloropropene 8260
920114922 WATER 1,2,3-Trichlorobenzene 8260
920114922 WATER 1,2,3-Trichloropropane 8260
920114922 WATER 1,2,4-Trichlorobenzene 8260
920114922 WATER 1,2,4-Trimethylbenzene 8260
920114922 WATER 1,2-Dibromo-3-chloropropane 8260
920114922 WATER 1,2-Dibromoethane 8260
920114922 WATER 1,2-Dichlorobenzene 8260
920114922 WATER 1,2-Dichloroethane 8260
920114922 WATER 1,2-Dichloropropane 8260
920114922 WATER 1,3,5-Trimethylbenzene 8260
920114922 WATER 1,3-Dichlorobenzene 8260
920114922 WATER 1,3-Dichloropropane 8260
920114922 WATt::R 1,4-Dichlorobenzene 8260
920114922 WATER 2,2-Dichloropropane 8260
920114922 WATER 2-Chlorotoluene 8260
Page 41 of 78
UNITS. CONG QUAL DIL
mg/L 0.015 1
mg/L 0.010 u 1
mg/L 1.0 u 1
mg/L 1.6 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 1.0 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
--- - - ---------- - - - - --
SAMPLE NAME SAMPLED
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697' 06/09/97
97191 MW34S -0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO_ MATRIX COMPOUND/PARAMETER METHOD
920114922 WATER 4-Chlorotoluene 8260
920114922 WATER Benzene 8260
920114922 WATER Bromobenzene 8260
920114922 WATER Bromochloromethane 8260
920114922 WATER Bromodichloromethane 8260
920114922 WATER Bromoform 8260
920114922 WATER Bromomethane 8260
920114922 WATER Carbon Tetrachloride 8260
920114922 WATER Chlorobenzene 8260
920114922 WATER Chlorodibromomethane 8260
920114922 WATER Chloroethane 8260
920114922 WATER Chloroform 8260
920114922 WATER Chloromethane 8260
920114922 WATER cis-1,2-Dichloroethene 8260
920114922 WATER Dibromomethane 8260
920114922 WATER Dichlorodifluoromethane 8260
920114922 WATER Ethylbenzene 8260
920114922 WATER Hexachlorobutadiene 8260
920114922 WATER lsopropylbenzene 8260
920114922 WATER m-Xylene and p-Xylene 8260
920114922 WATER Methylene chloride 8260
920114922 WATER n-Butylbenzene 8260
920114922 WATER n-Propylbenzene 8260
920114922 WATER Naphthalene 8260
920114922 WATER a-Xylene 8260
920114922 WATER p-lsopropyltoluene 8260
920114922 WATER sec-Butylbenzene 8260
920114922 WATER Styrene 8260
920114922 WATER tert-Butylbenzene 8260
920114922 WATER Tetrachloroethene 8260
920114922 WATER Toluene 8260
920114922 WATER trans-1,2-Dichloroethene 8260
Page 42 of 78
UNITS CONC QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5,0 u 1
ug/L 10 u 1
ug/L 5,0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5,0 u 1
ug/L 10 u 1
ug/L 5,0 u· 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5,0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5,0 u 1
ug/L 5,0 u 1
ug/L 5,0 u 1
ug/L 5,0 u 1
ug/L · 5,0 u 1
ug/L 5,0 u 1
August 4, 1997
-----· ·-- --·-- - - - - - - --
SAMPLE NAME SAMPLED
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34S 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D· 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW340 0697 06/09/97
97191 MW340 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW340 0697 · 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW340 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW340 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114922 WATER Trichloroethene 8260
920114922 WATER Trichlorofiuoromethane 8260
920114922 WATER Vinyl Chloride 8260
920114930 WATER Iron 200.7
920114930 WATER Iron, Dissolved 200.7
920114930 WATER Manganese 200.7
920114930 WATER Manganese, Dissolved 200.7
920114930 WATER Alkalinity, Total 310.1
920114930 WATER Chloride 325.3
920114930 WATER Sulfate 375.2
920114930 WATER Ethane 3810
920114930 WATER Ethene 3810
920114930 WATER Methane 3810
920114930 WATER Nitrogen, Nitrate 4500-N03 F
920114930 WATER Total Organic Carbon 5310C
920114930 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114930 WATER 1, 1, 1-Trichloroethane 8260
920114930 WATER 1, 1,2,2-Tetrachloroethane 8260
920114930 WATER 1, 1,2-Trichloroethane 8260
920114930 WATER 1, 1-Dichloroethane 8260
920114930 WATER 1, 1-Dichloroethene 8260
920114930 WATER 1, 1-Dichloropropene 8260
920114930 WATER 1,2,3-Trichlorobenzene 8260
920114930 WATER 1,2,3-Trichloropropane 8260
920114930 WATER 1,2,4-Trichlorobenzene 8260
920114930 WATER 1,2,4-Trimethylbenzene 8260
920114930 WATER 1,2-Dibromo-3-chloropropane 8260
920114930 WAIER 1,2-Dibromoethane 8260
920114930 WATER 1,2-Dichlorobenzene 8260
920114930 WATER 1,2-Dichloroethane 8260
Page 43 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 2.1 1
mg/L 0.050 u 1
mg/L 0.25 1
mg/L 0.072 1
mg/L 97 1
mg/L 1.9 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 0.98 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1 .
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114930 WATER 1,2-Dichloropropane 8260
920114930 WATER 1,3,5-Trimethylbenzene 8260
920114930 WATER 1,3-Dichlorobenzene 8260
920114930 WATER 1,3-Dichloropropane 8260
920114930 WATER 1,4-Dichlorobenzene 8260
920114930 WATER 2 ,2-Dichloropropane 8260
920114930 WATER 2-Chlorotoluene 8260
920114930 WATER 4-Chlorotoluene . 8260
920114930 WATER Benzene 8260
920114930 . WATER Bromobenzene 8260
920114930 WATER Bromochloromethane 8260
920114930 WATER Bromodichloromethane 8260
920114930 WATER Bromoform 8260
920114930 WATER Bromomethane 8260
920114930 WATER Carbon Tetrachloride 8260
920114930 WATER Chlorobenzene 8260
920114930 WATER Chlorodibromomethane 8260
920114930 WATER Chloroethane 8260
920114930 WATER Chloroform 8260
920114930 WATER Chloromethane 8260
920114930 WATER cis-1,2-Dichloroethene 8260
920114930 WATER Dibromomethane 8260
920114930 WATER Dichlorodifluoromethane 8260
920114930 WATER Ethyl benzene 8260
920114930 WATER Hexachlorobutadiene 8260
920114930 WATER lsopropylbenzene 8260
920114930 WATER m-Xylene and p-Xylene 8260
920114930 WATER Methylene chloride 8260
920114930 WATER n-Butylbenzene 8260
920114930 WATER n-Propylbenzene 8260
920114930 WATER Naphthalene 8260
920114930 WATER a-Xylene 8260
Page 44 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L · 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
--------~----------
SAMPLE NAME SAMPLED
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW34D 0697 06/09/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97 ·
97191 MW35S 0697 •. 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 •. 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97i91 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114930 WATER p-lsopropyltoluene 8260
920114930 WATER sec-Butylbenzene 8260
920114930 WATER Styrene 8260
920114930 WATER tert-Butylbenzene 8260
920114930 WATER Tetrachloroethene 8260
920114930 WATER Toluene 8260
920114930 WATER trans-1,2-Dichloroethene 8260
920114930 WATER Trichloroethene 8260
920114930 WATER Trichlorofluoromethane 8260
920114930 WATER Vinyl Chloride 8260
920118448 WATER Iron 200.7
920118448 WATER Iron, Dissolved 200.7
920118448 WATER Manganese 200.7
920118448 WATER Manganese, Dissolved 200.7
920118448 WATER Alkalinity, Total 310.1
920118448 WATER Chloride 325.3
920118448 WATER Sulfate 375.2
920118448 WATER Ethane 3810
920118448 WATER Ethene 3810
920118448 WATER Methane 3810
920118448 WATER Nitrogen, Nitrate 4500-NO3 F
920118448 WATER Total Organic Carbon 5310C
920118448 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118448 WATER 1, 1, 1-Trichloroethane 8260
920118448 WATER 1, 1,2,2-Tetrachloroethane 8260
920118448 WATER 1, 1,2-Trichloroethane 8260
920118448 WATER 1, 1-Dichloroethane 8260
920118448 WATER 1, 1-Dichloroethene 8260
920118448 WATER 1, 1-Dichloropropene 8260
920118448 WATER 1,2,3-Trichlorobenzene 8260
Page 45 of 78
UNITS CONG QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u· 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.76 1
mg/L 0.050 u 1
mg/L 0.025 1
mg/L 0.011 1
mg/L 6.0 1
mg/L 2.6 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.87 1
mg/L 1.2 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - -----· ------ - - - - - - - - -
SAMPLE NAME SAMPLED
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06111/97
97191 MW35S 0697 06111/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06111/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 · MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06111/97
97191 MW35S 0697 06111/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118448 WATER 1,2,3-Trichloropropane 8260
920118448 WATER 1,2,4-Trichlorobenzene 8260
920118448 WATER 1,2,4-Trimethylbenzene 8260
920118448 WATER 1,2-Dibromo-3-chloropropane 8260
920118448 WATER 1,2-Dibromoethane 8260
920118448 WATER 1,2-Dichlorobenzene 8260
920118448 WATER 1,2-Dichloroethane 8260
920118448 WATER 1,2-Dichloropropane 8260
920118448 WATER 1,3,5-Trimethylbenzene 8260
920118448 WATER 1,3°Dichlorobenzene 8260
920118448 WATER 1,3-Dichloropropane 8260
920118448 WATER 1,4-Dichlorobenzene 8260
920118448 WATER 2,2-Dichloropropane 8260
920118448 WATER 2-Chlorotoluene 8260
920118448 WATER 4-Chlorotoluene 8260
920118448 WATER Benzene 8260
920118448 WATER Bromobenzene 8260
920118448 WATER Bromochloromethane 8260
920118448 WATER Bromodichloromethane 8260
920118448 WATER Bromoform 8260
920118448 WATER Bromomethane 8260
920118448 WATER Carbon Tetrachloride 8260
920118448 WATER Chlorobenzene . 8260
920118448 WATER Chlorodibromomethane 8260
920118448 WATER Chloroethane 8260
920118448 WATER Chloroform 8260
920118448 WATER Chloromethane 8260
920118448 WATER cis-1,2-Dichloroethene 8260
920118448 WATER Dibromomethane 8260
920118448 WATER Dichlorodifiuoromethane 8260
920118448 WATER Ethyl benzene 8260
920118448 WATER Hexachlorobutadiene 8260
Page 46 of 78
UNITS CONC QUAL DIL
ug/L 5.0 u 1 ' ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1"
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 U· 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 . u 1
ug/L 5.0 u 1
ug/L 5.0 .· u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5,0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35S 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 069/ 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118448 WATER lsopropylbenzene 8260
920118448 WATER m-Xylene and p-Xylene 8260
920118448 WATER Methylene chloride 8260
920118448 WATER n-Butylbenzene 8260
920118448 WATER n-Propylbenzene 8260
920118448 WATER Naphthalene 8260
920118448 WATER o-Xylene 8260
920118448 WATER p-lsopropyltoluene 8_260
920118448 WATER sec-Butylbenzene 8260
920118448 WATER Styrene 8260
920118448 WATER tert-Butylbenzene 8260
920118448 WATER Tetrachloroethene 8260
920118448 WATER Toluene 8260
920118448 WATER trans-1,2-Dichloroethene 8260
920118448 WATER Trichloroethene 8260
920118448 WATER T richlorofluoromethane 8260
920118448 WATER Vinyl Chloride 8260
920118464 WATER Iron 200.7
920118464 WATER Iron, Dissolved 200.7
920118464 WATER Manganese 200.7
920118464 WATER Manganese, Dissolved 200.7
920118464 WATER Alkalinity, Total 310.1
920118464 WATER Chloride 325.3
920118464 WATER Sulfate 375.2
920118464 WATER Ethane 3810
920118464 WATER Ethene 3810
920118464 WATER Methane 3810
920118464 WATER Nitrogen, Nitrate 4500-NO3 F
920118464 WATER Total Organic Carbon 5310C
920118464 WATER 1, 1, 1,2-Tetrachloroethane 8260
Page 47 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 9.6 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 . u 1
ug/L 5.0 u 1
ug/L · 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.70 1
mg/L 0.050 u 1
mg/L 0.062 1
mg/L 0.035 1
mg/L 43 1
mg/L 1.6 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 0.67 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11 /97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118464 WATER 1, 1, 1-Trichloroethane 8260
920118464 WATER 1, 1,2,2-Tetrachloroethane 8260
920118464 WATER 1, 1 ,2-Trichloroethane 8260
920118464 WATER 1, 1-Dichloroethane 8260
920118464 WATER 1, 1-Dichloroethene 8260
920118464 WATER 1, 1-Dichloropropene 8260
920118464 WATER 1,2,3-Trichlorobenzene 8260 ·
920118464 WATER 1,2,3-Trichloropropane 8260
920118464 WATER 1,2,4-Trichlorobenzene 8260
920118464 · WATER 1,2,4-Trimethylbenzene 8260
920118464 WATER 1,2-Dibromo-3-chloropropane 8260
920118464 WATER 1,2-Dibromoethane 8260
920118464 WATER 1,2-Dichlorobenzene 8260
920118464 WATER 1,2-Dichloroethane 8260
920118464 WATER 1,2-Dichloropropane 8260
920118464 WATER 1,3,5-Trimethylbenzene 8260
920118464 WATER 1,3-Dichlorobenzene 8260
920118464 WATER 1,3-Dichloropropane 8260
920118464 WATER 1,4-Dichlorobenzene 8260
920118464 WATER 2,2-Dichloropropane 8260
920118464 WATER 2-Chlorotoluene 8260
920118464 WATER 4-Chlorotoluene 8260
920118464 WATER Benzene 8260
920118464 WATER Bromobenzene 8260
920118464 WATER Bromochloromethane 8260
920118464 WATER Bromodichloromethane 8260
920118464 WATER Bromoform 8260
920118464 WATER Bromomethane 8260
920118464 WATER Carbon Tetrachloride 8260
920118464 WATER Chlorobenzene 8260
920118464 WATER Chlorodibromomethane 8260
920118464 WATER Chloroethane 8260
Page 48 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
. ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11 /97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW35D 0697 06/11/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118464 WATER Chloroform 8260
920118464 WATER Chloromethane 8260
920118464 WATER cis-1,2-Dichloroethene 8260
920118464 WATER Dibromomethane 8260
920118464 WATER Dichlorodifluoromethane 8260
920118464 WATER Ethylbenzene 8260
920118464 WATER Hexachlorobutadiene 8260
920118464 WATER lsopropylbenzene 8260
920118464 WATER m-Xylene and p-Xylene 8260
920118464 WATER Methylene chloride 8260
920118464 WATER n-Butylbenzene 8260
920118464 WATER n-Propylbenzene 8260
920118464 WATER Naphthalene 8260
920118464 WATER o-Xylene 8260
920118464 WATER p-lsopropyltoluene 8260
920118464 WATER sec-Butyl benzene 8260
920118464 WATER Styrene 8260
920118464 WATER tert-Butylbenzene 8260
920118464 WATER Tetrachloroethene 8260
920118464 WATER Toluene 8260
920118464 WATER trans-1,2-Dichloroethene 8260
920118464 WATER Trichloroethene 8260
920118464 WATER Trichlorofiuoromethane 8260
920118464 WATER Vinyl Chloride 8260
920119479 WATER Iron 200.7
920119479 WATER Iron, Dissolved 200.7
920119479 WATER Manganese 200.7
920119479 WATER Manganese, Dissolved 200.7
920119479 WATER Alkalinity, Total 310.1
920119479 WATER Chloride 325.3
Page 49 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
. ug/L 5,0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 9.9 1
mg/L 10 1
mg/L 19 1
mg/L 14 1
August 4, 1997
--------------------
SAMPLE NAME SAMPLED
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697. 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97'
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119479 WATER Sulfate 375.2
920119479 WATER Ethane 3810
920119479 WATER Ethene 3810
920119479 WATER Methane 3810
920119479 WATER Nitrogen, Nitrate 4500-NO3 F
920119479 WATER Total Organic Carbon 5310C
920119479 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119479 WATER 1, 1, 1-Trichloroethane 8260
920119479 WATER 1, 1,2,2-Tetrachloroethane 8260
920119479 WATER 1, 1,2-Trichloioethane 8260
920119479 WATER 1, 1-Dichloroethane 8260
920119479 WATER 1, 1-Dichloroethene 8260
920119479 WATER 1, 1-Dichloropropene 8260
920119479 WATER 1,2,3-Trichlorobenzene 8260
920119479 WATER 1,2,3-Trichloropropane 8260
920119479 WATER 1,2,4-Trichlorobenzene 8260
920119479 WATER 1,2,4-Trimethylbenzene 8260
920119479 WATER 1,2-Dibromo-3-chloropropane 8260
920119479 WATER 1,2-Dibromoethane 8260
920119479 WATER 1,2-Dichlorobenzene 8260
920119479 WATER 1,2-Dichloroethane 8260
920119479 WATER 1,2-Dichloropropane 8260
920119479 WATER 1,3,5-Trimethylbenzene 8260
920119479 WATER 1,3-Dichlorobenzene 8260
920119479 WATER 1,3-Dichloropropane 8260
920119479 WATER 1,4-Dichlorobenzene 8260
920119479 WATER 2,2-Dichloropropane 8260
920119479 WATER 2-Chlorotoluene 8260
920119479 WATER 4-Chlorotoluene 8260
920119479 WATER Benzene 8260
920119479 WATER Bromobenzene 8260
920119479 WATER Bromochloromethane 8260
Page 50 of 78
UNITS CONG QUAL DIL
mg/L 5.4 1
ug/L 16 ·u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 140 4
ug/L 200 J 100
ug/L 500 u 100
ug/L 200 J 100
ug/L 220 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 7000 100
ug/L 500 u 100
ug/L 1000 100
ug/L 2000 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 7500 100
ug/L 500 u 100
ug/L 500 u 100
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/12/97
97191 MW36S 0697 06/i2/97
97191 MW36S 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119479 WATER Bromodichloromethane 8260
920119479 WATER Bromoform 8260
920119479 WATER Bromomethane 8260
920119479 WATER Carbon Tetrachloride 8260
920119479 WATER Chlorobenzene 8260
920119479 WATER Chlorodibromomethane 8260
920119479 WATER Chloroethane 8260
920119479 WATER Chloroform 8260
920119479 WATER Chloromethane 8260
920119479 WATER cis-1,2-Dichloroethene 8260
920119479 WATER Dibromomethane 8260
920119479 WATER Dichlorodifluoromethane 8260
920119479 WATER Ethylbenzene 8260
920119479 WATER Hexachlorobutadiene 8260
920119479 WATER lsopropylbenzene 8260
920119479 WATER m-Xylene and p-Xylene 8260
920119479 WATER Methylene chloride 8260
920119479 WATER n-Butylbenzene 8260
920119479 WATER n-Propylbenzene 8260
920119479 WATER Naphthalene 8260
920119479 WATER a-Xylene 8260
920119479 WATER p-lsopropyltoluene 8260
920119479 WATER sec-Butyl benzene 8260
920119479 WATER Styrene 8260
920119479 WATER tert-Butylbenzene 8260
920119479 WATER Tetrachloroethene 8260
920119479 WATER Toluene 8260
920119479 WATER trans-1,2-Dichloroethene 8260
920119479 WATER Trichloroethene 8260
920119479 WATER Trichlorofluoromethane 8260
920119479 WATER Vinyl Chloride 8260
Page 51 of 78
UNITS CONG QUAL OIL
ug/L 3700 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 1800 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 34000 100
. ug/L --1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 160 J 100
ug/L 8800 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 310 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 300 J 100
ug/L 500 u 100
ug/L 1900 100
ug/L 500 u 100
ug/L 1000 u 100
August 4, 1997
_ __, ________________ _
SAMPLE NAME SAMPLED
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191" MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118456 WATER Iron 200.7
920118456 WATER Iron, Dissolved 200.7
920118456 WATER Manganese 200.7
920118456 WATER Manganese, Dissolved 200.7
920118456 WATER Alkalinity, Total 310.1
920118456 WATER Chloride 325.3
920118456 WATER Sulfate 375.2
920118456 WATER Ethane 3810
920118456 WATER Ethene 3810
920118456 WATER Methane 3810
920118456 WATER Nitrogen, Nitrate 4500-NO3 F
920118456 WATER Total Organic Carbon 5310C
920118456 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118456 WATER 1, 1, 1-Trichloroethane 8260
920118456 WATER 1, 1,2,2-Tetrachloroethane 8260
920118456 WATER 1, 1,2-Trichloroethane 8260
920118456 WATER 1, 1-Dichloroethane 8260
920118456 WATER 1, 1-Dichloroethene 8260
920118456 WATER 1, 1-Dichloropropene 8260
920118456 WATER 1,2,3-Trichlorobenzene 8260
920118456 WATER 1,2,3-Trichloropropane 8260
920118456 WATER 1,2,4-Trichlorobenzene 8260
920118456 WATER 1,2,4-Trimethylbenzene 8260
920118456 WATER 1,2-Dibromo-3-chloropropane 8260
920118456 WATER 1,2-Dibromoethane 8260
920118456 WATER 1,2-Dichlorobenzene 8260
920118456 WATER 1,2-Dichloroethane 8260
920118456 WATER 1,2-Dichloropropane 8260
920118456 WATER 1,3,5-Trimethylbenzene 8260
920118456 WATER 1,3-Dichlorobenzene 8260
920118456 WATER 1,3-Dichloropropane 8260
Page 52 of 78
UNITS CONG QUAL DIL
mg/L 0.093 1
mg/L 0.050 u 1
mg/L 0.010 u 1
mg/L 0.010 u 1
· mg/L 77 1
mg/L 1.9 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.06 1
mg/L 0.89 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 6.5 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 8.2 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - - - --· - - - - - --- - - - - -
SAMPLE NAME SAMPLED
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 _ 06/11/97 .
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118456 WATER 1,4-Dichlorobenzene 8260
920118456 WATER 2,2-Dichloropropane 8260
920118456 WATER 2-Chlorotoluene 8260
920118456 WATER 4-Chlorotoluene 8260
920118456 WATER Benzene 8260
920118456 WATER Bromobenzene 8260
920118456 WATER Bromochloromethane 8260
920118456 WATER Bromodichloromethane 8260
920118456 WATER Bromoform 8260
920118456 WATER Bromomethane 8260
920118456 WATER Carbon Tetrachloride 8260
920118456 WATER Chlorobenzene 8260
920118456 WATER Chlorodibromomethane 8260
920118456 WATER Chloroethane 8260
920118456 WATER Chloroform 8260
920118456 WATER Chloromethane 8260
920118456 WATER cis-1,2-Dichloroethene 8260
920118456 WATER Dibromomethane 8260
920118456 WATER Dichlorodifluoromethane 8260
920118456 WATER Ethylbenzene 8260
920118456 WATER Hexachlorobutadiene 8260
920118456 WATER lsopropylbenzene 8260
920118456 WATER m-Xylene and p-Xylene 8260
920118456 WATER Methylene chloride 8260
920118456 WATER n-Butylbenzene 8260
920118456 WATER n-Propylbenzene 8260
920118456 WATER Naphthalene 8260
920118456 WATER o-Xylene 8260
920118456 WATER p-lsopropyltoluene 8260
920118456 WATER sec-Butylbenzene 8260
920118456 WATER Styrene 8260
920118456 WATER tert-Butylbenzene 8260
Page 53 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 •. u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 12 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 270 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 6.3 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW36D 0697 06/11/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118456 WATER Tetrachloroethene 8260
920118456 WATER Toluene 8260
920118456 WATER trans-1,2-Dichloroethene 8260
920118456 WATER Trichloroethene 8260
920118456 WATER T richlorofluoromethane 8260
920118456 WATER Vinyl Chloride 8260
920119460 WATER Iron 200.7
920119460 WATER Iron; Dissolved 200.7
920119460 WATER Manganese 200.7
920119460 WATER Manganese, Dissolved 200.7
920119460 WATER Alkalinity, Total 310.1
920119460 WATER Chloride 325.3
920119460 WATER Sulfate 375.2
920119460 WATER Ethane 3810
920119460 WATER Ethene 3810
920119460 WATER Methane 3810
920119460 WATER Nitrogen, Nitrate 4500-NO3 F
920119460 WATER Total Organic Carbon 5310C
920119460 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119460 WATER 1, 1, 1-Trichloroethane 8260
920119460 WATER 1, 1,2,2-Tetrachloroethane 8260
920119460 WATER 1, 1,2-Trichloroethane 8260
920119460 WATER 1, 1-Dichloroethane 8260
920119460 WATER 1, 1-Dichloroethene 8260
920119460 WATER 1, 1-Dichloropropene 8260
920119460 WATER 1,2,3-Trichlorobenzene 8260
920119460 WATER 1,2,3-Trichloropropane 8260
920119460 WATER 1,2,4-Trichlorobenzene 8260
920119460 WATER 1,2,4-Trimethylbenzene 8260
920119460 WATER 1,2-Dibromo-3-chloropropane 8260
Page 54 of 78
UNITS CONC QUAL DIL
ug/L 9.3 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 9.1 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.053 1
mg/L 0.050 u 1
mg/L 7.3 1
mg/L 7.3 1
mg/L 17 1
mg/L 27 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 18 1
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/.97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119460 WATER 1,2-Dibromoethane 8260
920119460 WATER 1,2-Dichlorobenzene 8260
920119460 WATER 1,2-Dichloroethane 8260
920119460 WATER 1,2-Dichloropropane 8260
920119460 WATER 1,3,5-Trimethylbenzene 8260
920119460 WATER 1,3-Dichlorobenzene 8260
920119460 WATER 1,3-Dichloropropane 8260
920119460 WATER 1,4-Dichlorobenzene 8260
920119460 WATER 2,2-Dichloropropane 8260 -
920119460 WATER 2-Chlorotoluene 8260
920119460 WATER 4-Chlorotoluene 8260
920119460 WATER Benzene 8260
920119460 WATER Bromobenzene 8260
920119460 WATER Bromochloromethane 8260
920119460 WATER Bromodichloromethane 8260
920119460 WATER Bromoform 8260
920119460 WATER Bromomethane 8260
920119460 WATER Carbon Tetrachloride 8260
920119460 WATER Chlorobenzene 8260
920119460 WATER Chlorodibromomethane 8260
920119460 WATER Chloroethane 8260
920119460 WATER Chloroform 8260
920119460 WATER Chloromethane 8260
920119460 WATER cis-1,2-Dichloroethene 8260
920119460 WATER Dibromomethane 8260
920119460 WATER Dichlorodifiuoromethane 8260
920119460 WATER Ethylbenzene 8260
920119460 WATER Hexachlorobutadiene 8260
920119460 WATER lsopropylbenzene 8260
920119460 WATER m-Xylene and p-Xylene 8260
920119460 WATER Methylene chloride 8260
920119460 WATER n-Butylbenzene 8260
Page 55 of 78
UNITS CONG QUAL OIL
ug/L 500 u 100
ug/L 500 u 100
ug/L 110 J 100
ug/L 520 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 100 J 100
. ug/L -1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 6900 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 4300 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 45000 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 1000 u 100
ug/L 500 u 100
ug/L 350 J 100
ug/L 8100 100
ug/L 500 u 100
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697. 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/.12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW37 0697 06/12/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119460 WATER n-Propylbenzene 8260
920119460 WATER Naphthalene 8260
920119460 WATER o-Xylene 8260
920119460 WATER p-lsopropyltoluene 8260
920119460 WATER sec-Butylbenzene 8260
920119460 WATER Styrene 8260
920119460 WATER tert-Butylbenzene 8260
920119460 WATER Tetrachloroethene 8260
920119460 WATER Toluene 8260
920119460 WATER trans-1,2-Dichloroethene 8260
920119460 WATER Trichloroethene 8260
920119460 WATER Trichlorofluoromethane 8260
920119460 WATER Vinyl Chloride 8260
920118499 WATER Iron 200.7
920118499 WATER Iron, Dissolved 200.7
920118499 WATER Manganese 200.7
920118499 WATER Manganese, Dissolved 200.7
920118499 WATER Alkalinity, Total 310.1
920118499 WATER Chloride 325.3
920118499 WATER Sulfate 375.2
920118499 WATER Ethane 3810
920118499 WATER Ethene 3810
920118499 WATER Methane 3810
920118499 WATER Nitrogen, Nitrate 4500-NO3 F
920118499 WATER Total Organic Carbon 5310C
920118499 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118499 WATER 1, 1, 1-Trichloroethane 8260
920118499 WATER 1, 1,2,2-Tetrachloroethane 8260
920118499 WATER 1, 1,2-Trichloroethane 8260
920118499 WATER 1, 1-Dichloroethane 8260
Page 56 of 78
UNITS CONC QUAL DIL
ug/L 500 u 100
ug/L 1000 u 100
ug/L 220 J 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 500 u 100
ug/L 220 J 100
ug/L . 700 100
ug/L 500 u 100
ug/L 680 100
ug/L 500 u 100
ug/L 1000 u 100
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 0.019 1
mg/L 0.028 1
mg/L 91 1
mg/L 2.1 1
mg/L 7.9 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
mg/L 0.05 u 1
mg/L 1.3 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
--- - - -------- - - - - - - - -
SAMPLE NAME SAMPLED
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697-06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0597 06/11/9/
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118499 WATER 1, 1-Dichloroethene 8260
920118499 WATER 1, 1-Dichloropropene 8260
920118499 WATER 1,2,3-Trichlorobenzene 8260
920118499 WATER 1,2,3-Trichloropropane 8260
920118499 WATER 1,2,4-Trichlorobenzene 8260
920118499 WATER 1,2,4-Trimethylbenzene 8260
920118499 WATER 1,2-Dibromo-3-chloropropane 8260
920118499 WATER 1,2-Dibromoethane 8260
920118499 WATER 1,2-Dichlorobenzene 8260
920118499 WATER 1,2-Dichloroethane 8260
920118499 WATER 1,2-Dichloropropane 8260
920118499 WATER 1,3,5-Trimethylbenzene 8260
920118499 WATER 1,3-Dichlorobenzene 8260
920118499 WATER 1,3-Dichloropropane 8260
920118499 WATER 1,4-Dichlorobenzene 8260
920118499 WATER 2,2-Dichloropropane 8260
920118499 WATER 2-Chlorotoluene 8260
920118499 WATER 4-Chlorotoluene 8260
920118499 WATER Benzene 8260
920118499 WATER Bromobenzene 8260
920118499 WATER Bromochloromethane 8260
920118499 WATER Bromodichloromethane 8260
920118499 WATER Bromoform 8260
920118499 WATER Bromomethane 8260
920118499 WATER Carbon Tetrachloride 8260
920118499 WATER Chlorobenzene 8260
920118499 WATER Chlorodibromomethane 8260
920118499 WATER Chloroethane 8260
920118499 WATER Chloroform 8260
920118499 WATER Chloromethane 8260
920118499 WATER cis-1,2-Dichloroethene 8260
920118499 WATER Dibromomethane 8260
Page 57 of 78
UNITS CONC QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0-u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 1 J 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 . MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 MW38 0697 06/11/97
97191 EB01 · 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118499 WATER Dichlorodifluoromethane 8260
920118499 WATER Ethylbenzene 8260
920118499 WATER Hexachlorobutadiene 8260
920118499 WATER lsopropylbenzene 8260
920118499 WATER m-Xylene and p-Xylene 8260
920118499 WATER Methylene chloride 8260
920118499 WATER n-Butylbenzene 8260
920118499 WATER n-Propylbenzene . 8260
920118499 WATER Naphthalene 8260
920118499 · WATER o-Xylene 8260
920118499 WATER p-lsopropyltoluene 8260
920118499 WATER sec-Butyl benzene 8260
920118499 WATER Styrene 8260
920118499 WATER tert-Butylbenzene 8260
920118499 WATER Tetrachloroethene 8260
920118499 WATER Toluene 8260
920118499 WATER trans-1,2-Dichloroethene 8260
920118499 WATER Trichloroethene 8260
920118499 WATER Trichlorofluorometharie 8260
920118499 WATER Vinyl Chloride 8260
920114906 WATER Iron 200.7
920114906 WATER Iron, Dissolved 200.7
920114906 WATER Manganese 200.7
920114906 WATER Manganese, Dissolved 200.7
920114906 WATER Alkalinity, Total 310.1
920114906 WATER Chloride 325.3
920114906 WATER Sulfate 375.2
920114906 WATER Ethane 3810
920114906 WATER Ethene 3810
920114906 WATER Methane 3810
Page 58 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L. 10 u -1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.073 1
mg/L 0.050 u 1
mg/L 0.010 u 1
mg/L 0.010 u 1
mg/L 20 1
mg/L 1 u 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 15 u 1
ug/L 8.6 u 1
August 4, 1997
-----------~-------
SAMPLE NAME SAMPLED
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 · 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER · METHOD
920114906 WATER Nitrogen, Nitrate 4500-NO3 F
920114906 WATER Total Organic Carbon 5310C
920114906 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114906 WATER 1, 1, 1-Trichloroethane 8260
920114906 WATER 1, 1,2,2-Tetrachloroethane 8260
920114906 WATER 1, 1 ,2-Trichloroethane 8260
920114906 WATER 1, 1-Dichloroethane 8260
920114906 WATER 1, 1-Dichloroethene 8260
920114906 WATER 1, 1-Dichloropropene 8260
920114906 WATER 1,2,3-Trichhrobenzene 8260
920114906 WATER 1,2,3-Trichloropropane 8260
920114906 WATER 1,2,4-Trichlorobenzene 8260
920114906 WATER 1,2,4-Trimethylbenzene 8260
920114906 WATER 1,2-Dibromo-3-chloropropane 8260
920114906 WATER 1,2-Dibromoethane 8260
920114906 WATER 1,2-Dichlorobenzene 8260
920114906 WATER 1,2-Dichloroethane 8260
920114906 WATER 1,2-Dichloropropane 8260
920114906 WATER 1,3,5-Trimethylbenzene 8260
920114906 WATER 1,3-Dichlorobenzene 8260
920114906 WATER 1,3-Dichloropropane 8260
920114906 WATER 1,4-Dichlorobenzene 8260
920114906 WATER 2,2-Dichloropropane 8260
920114906 WATER 2-Chlorotoluene 8260
920114906 WATER 4-Chlorotoluene 8260
920114906 WATER Benzene 8260
920114906 WATER Bromobenzene 8260
920114906 WATER Bromochloromethane 8260
920114906 WATER Bromodichlorornethane 8260
920114906 WATER Bromoform 8260
920114906 WATER Bromomethane 8260
920114906 WATER Carbon Tetrachloride 8260
Page 59 of 78
UNITS CONG QUAL OIL
mg/L 0.05 u 1
mg/L 0.93 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191-· EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB01 0697 06/09/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114906 WATER Chlorobenzene 8260
920114906 WATER Chlorodibromomethane 8260
920114906 WATER Chloroethane 8260
920114906 WATER Chloroform 8260
920114906 WATER Chloromethane 8260
920114906 WATER cis-1,2-Dichloroethene 8260
920114906 WATER Dibromomethane 8260
920114906 WATER Dichlorodifluoromethane 8260
920114906 WATER Ethylbenzene 8260
92011<\906 WATER Hexachlorobutadiene 8260
920114906 WATER lsopropylbenzene 8260
920114906 WATER m-Xylene and p-Xylene 8260
920114906 WATER Methylene chloride 8260
920114906 WATER n-Butylbenzene 8260
920114906 WATER n-Propylbenzene 8260
920114906 WATER Naphthalene 8260
920114906 WATER o-Xylene 8260
920114906 WATER p-lsopropyltoluene 8260
920114906 WATER sec-Butyl benzene 8260
920114906 WATER Styrene 8260
920114906 WATER tert-Butylbenzene 8260
920114906 WATER Tetrachloroethene 8260
920114906 WATER Toluene 8260
920114906 WATER trans-1,2-Dichloroethene 8260
920114906 WATER Trichloroethene 8260
920114906 WATER Trichlorofluoromethane 8260
920114906 WATER Vinyl Chloride 8260
920114906 WATER Trichlorofluoromethane 8260
920114906 WATER Vinyl Chloride 8260
920118421 WATER 1, 1, 1,2-Tetrachloroethane 8260
Page 60 of 78
UNITS CONC QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
--ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 ·U 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B· 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11 /97
97191 EB02B 0697 06/11/97
-97191 EB02B 0697. 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/_97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB028 0697 06/11/97
97191 EB028 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB028. 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB028 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB028 0697 06/11/97
97191 EB028 0697 06/11/97
97191 E802B 0697 06/11/97
97191 EB028 0697 06/11/97
97191 EB028 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118421 WATER 1, 1, 1-Trichloroethane 8260
920118421 WATER 1, 1,2,2-Tetrachloroethane 8260
920118421 WATER 1, 1,2-Trichloroethane 8260
920118421 WATER 1, 1-Dichloroethane 8260
920118421 WATER 1, 1-Dichloroethene 8260
920118421 WATER 1, 1-Dichloropropene 8260
920118421 WATER 1,2,3-Trichlorobenzene 8260
920118421 WATER 1,2,3-Trichloropropane 8260
920118421 WATER 1,2,4-Trichlorobenzene 8260
920118421 WATER l,2,4-Trimethylbenzene 8260
920118421 WATER 1,2-Dibromo-3-chloropropane 8260
920118421 WATER 1,2-Dibromoethane 8260
920118421 WATER 1,2-Dichlorobenzene 8260
920118421 WATER 1,2-Dichloroethane 8260
920118421 WATER 1,2-Dichloropropane 8260
920118421 WATER 1,3,5-Trimethylbenzene 8260
920118421 WATER 1,3-Dichlorobenzene 8260
920118421 WATER 1,3-Dichloropropane 8260
920118421 WATER 1,4-Dichlorobenzene 8260
920118421 WATER 2,2-Dichloropropane 8260
920118421 WATER 2-Chlorotoluene 8260
920118421 WATER 4-Chlorotoluene 8260
920118421 WATER Benzene 8260
920118421 WATER Bromobenzene 8260
920118421 WATER Bromochloromethane 8260
920118421 WATER Bromodichloromethane 8260
920118421 WATER Bromoform 8260
920118421 WATER Bromomethane 8260
920118421 WATER Carbon Tetrachloride 8260
920118421 WATER Chlorobenzene 8260
920118421 WATER Chlorodibromomethane 8260
920118421 WATER Chloroethane 8260
Page 61 of 78
UNITS CONG QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
.. ug/L 10 u-- . 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11 /97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97 .
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB02B 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118421 WATER Chloroform 8260
920118421 WATER Chloromethane 8260
920118421 WATER cis-1,2-Dichloroethene 8260
920118421 WATER Dibromomethane 8260
920118421 WATER Dichlorodifluoromethane 8260
920118421 WATER Ethyl benzene 8260
920118421 WATER Hexachlorobutadiene 8260
920118421 WATER lsopropylbenzene 8260
920118421 WATER m-Xylene and p-Xylene 8260
920118421-WATER Methylene chloride 8260
920118421 WATER n-Butylbenzene 8260
920118421 WATER n-Propylbenzene 8260
920118421 WATER Naphthalene 8260
920118421 WATER o-Xylene 8260
920118421 WATER p-lsopropyltoluene 8260
920118421 WATER sec-Butylbenzene 8260
920118421 WATER Styrene 8260
920118421 WATER tert-Butylbenzene 8260
920118421 WATER Tetrachloroethene 8260
920118421 WATER Toluene 8260
920118421 WATER trans-1,2-Dichloroethene 8260
920118421 WATER Trichloroethene 8260
920118421 WATER Trichlorofluoromethane 8260
920118421 WATER Vinyl Chloride 8260
920118430 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118430 WATER 1, 1, 1-Trichloroethane 8260
920118430 WATER 1, 1,2,2-Tetrachloroethane 8260
920118430 WATER 1, 1,2-Trichloroethane 8260
920118430 WATER 1, 1-Dichloroethane 8260
920118430 WATER 1, 1-Dichloroethene 8260
Page 62 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u .. 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- ----- - - - - - - - - - - - - - - -
SAMPLE NAME SAMPLED
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11 /97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118430 WATER 1, 1-Dichloropropene 8260
920118430 WATER 1,2, 3-Trichlorobenzene 8260
920118430 WATER 1,2,3-Trichloropropane 8260
920118430 WATER 1,2,4-Trichlorobenzene 8260
920118430 WATER 1,2,4-Trimethylbenzene 8260
920118430 WATER 1,2-Dibromo-3-chloropropane 8260
920118430 WATER 1,2-Dibromoethane 8260
920118430 WATER 1,2-Dichlorobenzene 8260
920118430 WATER 1,2-Dichloroethane 8260
920118430 . WATER 1',2-Dichloropropane 8260
920118430 WATER 1,3,5-Trimethylbenzene 8260
920118430 WATER 1,3-Dichlorobenzene 8260
920118430 WATER 1,3-Dichloropropane 8260
920118430 WATER 1,4-Dichlorobenzene 8260
920118430 WATER 2,2-Dichloropropane 8260
920118430 WATER 2-Chlorotoluene 8260
920118430 WATER 4-Chlorotoluene 8260
920118430 WATER Benzene 8260
920118430 WATER Bromobenzene 8260
920118430 WATER Bromochloromethane 8260
920118430 WATER Bromodichloromethane 8260
920118430 WATER Bromoform 8260
920118430 WATER Bromomethane 8260
920118430 WATER Carbon Tetrachloride 8260
920118430 WATER Chlorobenzene 8260
920118430 WATER Chlorodibromomethane 8260
920118430 WATER Chloroethane 8260
920118430 WATER Chloroform 8260
920118430 WATER Ch!oromethane 8260
920118430 WATER cis-1,2-Dichloroethene 8260
920118430 WATER Dibromomethane 8260
920118430 WATER Dichlorodifluoromethane 8260
Page 63 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u ~ 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 .U 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06/11/97
97191 EB03P 0697 06111197
97191 · EB03P 0697 06111197
97191 EB03P 0697 06111197
97191 EB03P 0697 06111197
97191 EB03P 0697 06111197
97191 EB03P 0697 06/11197
97191 EB03P 0697 06111/97
97191 EB03P 0697 06111/97
97191 EB03P 0697 06/11197
97191 EB03P 0697 06/11197
97191 EB04 0697 06/12197
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06112197
97191 EB04 0697 06/12197
97191 EB04 0697 06112/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site_
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118430 WATER Ethylbenzene 8260
920118430 WATER Hexachlorobutadiene 8260
920118430 WATER lsopropylbenzene 8260
920118430 WATER m-Xylene and p-Xylene 8260
920118430 WATER Methylene chloride 8260
920118430 WATER n-Butylbenzene 8260
920118430 WATER n-Propylbenzene 8260
920118430 WATER Naphthalene 8260
920118430 WATER a-Xylene 8260.
920118430 WATER p-lsopropyltoluene 8260
920118430 WATER sec-Butyl benzene 8260
920118430 WATER Styrene 8260
920118430 WATER tert-Butylbenzene 8260
920118430 WATER Tetrachloroethene 8260
920118430 WATER Toluene 8260
920118430 WATER trans-1,2-Dichloroethene 8260
920118430 WATER Trichloroethene 8260
920118430 WATER Trichloroftuoromethane 8260
920118430 WATER Vinyl Chloride 8260
920119495 WATER Iron 200.7
920119495 WATER Iron, Dissolved 200.7
920119495 WATER Manganese 200.7
920119495 WATER Manganese, Dissolved 200.7
920119495 WATER Alkalinity, Total 310.1
920119495 WATER Chloride 325.3
920119495 WATER Sulfate 375.2
920119495 WATER Ethane 3810
920119495 WATER Ethene 3810
920119495 WATER Methane 3810
920119495 WATER Nitrogen, Nitrate 4500-NO3 F
Page 64 of 78
UNITS CONG QUAL DIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 1.6 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5,0 u-1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
mg/L 0.050 u 1
mg/L 0.050 u 1
mg/L 0.010 u 1
mg/L 0.010 u 1
mg/L 1.0 1
mg/L 1 u 1
mg/L 5 u 1
ug/L 16 u 1
ug/L 27 1
ug/L 8.6 u 1
mg/L 0.05 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697· 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 f;B04 0697. 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 . EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04. 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119495 WATER Total Organic Carbon 5310C
920119495 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119495 WATER 1, 1, 1-Trichloroethane 8260
920119495 WATER 1, 1,2,2-Tetrachloroethane 8260
920119495 WATER 1, 1,2-Trichloroethane 8260
920119495 WATER 1, 1-Dichloroethane 8260
920119495 WATER 1, 1-Dichloroethene 8260
920119495 WATER 1, 1-Dichloropropene 8260
920119495 WATER 1,2,3-Trichlorobenzene 8260
920119495 WATER 1,2,3-Trichloropropane 8260
920119495 WATER 1,2,4-Trichlorobenzene 8260
920119495 WATER 1,2,4-Trimethylbenzene 8260
920119495 WATER 1,2-Dibromo-3-chloropropane 8260
920119495 WATER 1,2-Dibromoethane 8260
920119495 WATER 1,2-Dichlorobenzene 8260
920119495 WATER 1,2-Dichloroethane 8260
920119495 WATER 1,2-Dichloropropane 8260
920119495 WATER 1,3,5-Trimethylbenzene 8260
920119495 WATER 1,3-Dichlorobenzene 8260
920119495 WATER 1,3-Dichloropropane 8260
920119495 WATER 1,4-Dichlorobenzene 8260
920119495 WATER 2,2-Dichloropropane 8260
920119495 WATER 2-Chlorotoluene 8260
920119495 WATER 4-Chlorotoluene 8260
920119495 WATER Benzene 8260
920119495 WATER Bromobenzene 8260
920119495 WATER Bromochloromethane 8260
920119495 WATER Bromodichloromethane 8260
920119495 WATER Bromoform 8260
920119495 WATER Bromomethane 8260
920119495 WATER Carbon Tetrachloride 8260
920119495 WATER Chlorobenzene 8260
Page 65 of 78
UNITS CONC QUAL OIL
mg/L 0.92 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L -5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 2.3 j 1
ug/L 2.1 j 1
ug/L 5.0 u 1
ug/L 13 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 8.4 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1.9 j 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 8.4 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 EB04 0697 06/12/97
97191 WX0608 0697 06/08/97
97191 VVX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119495 WATER Chlorodibromomethane 8260
920119495 WATER Chloroethane 8260
920119495 WATER Chloroform 8260
920119495 · WATER Chloromethane 8260
920119495 WATER cis-1,2-Dichloroethene 8260
920119495 WATER Dibromomethane 8260
920119495 WATER Dichlorodifiuoromethane 8260
920119495 WATER Ethyl benzene 8260
920119495 WATER Hexachlorobutadiene 8260 .
920119495 WATER lsopropylbenzene 8260
920119495 WATER m-Xylene and p-Xylene 8260
920119495 WATER Methylene chloride 8260
920119495 WATER n-Butylbenzene 8260
920119495 WATER n-Propylbenzene 8260
920119495 WATER Naphthalene 8260
920119495 WATER a-Xylene 8260
920119495 WATER p-lsopropyltoluene 8260
920119495 WATER sec-Butylbenzene 8260
920119495 WATER Styrene 8260
920119495 WATER tert-Butylbenzene 8260
920119495 WATER Tetrachloroethene 8260
920119495 WATER Toluene 8260
920119495 WATER trans-1,2-Dichloroethene 8260
920119495 WATER Trichloroethene ' 8260
920119495 WATER Trichlorofiuoromethane 8260
920119495 WATER Vinyl Chloride 8260
920114353 WATER 1, 1, 1,2-Tetrach!oroethane 8260
920114353 WATER 1, 1, 1-Trichloroethane 8260
920114353 WATER 1, 1,2,2-Tetrachloroethane 8260
920114353 WATER 1, 1,2-Trichloroethane 8260
Page 66 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 160 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L. . 10 u . 1
ug/L 5.0 u 1
ug/L 1.5 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 1.6 . J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 15 1
ug/L 3 J 1
ug/L 5.0 u 1
ug/L 16 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114353 WATER 1, 1-Dichloroethane 8260
920114353 WATER 1, 1-Dichloroethene 8260
920114353 WATER 1, 1-Dichloropropene 8260
920114353 WATER 1,2,3-Trichlorobenzene 8260
920114353 WATER 1,2,3-Trichloropropane 8260
920114353 WATER 1,2,4-Trichlorobenzene 8260
920114353 WATER 1,2,4-Trimethylbenzene 8260
920114353 WATER 1,2-Dibromo-3-chloropropane 8260
920114353 WATER 1,2-Dibromoethane 8260
920114353 WATER 1,2-Dichlorobenzene 8260
920114353 WATER 1,2-Dichloroethane 8260
920114353 WATER 1,2-Dichloropropane 8260
920114353 WATER 1,3,5-Trimethylbenzene 8260
920114353 WATER 1, 3-Dichlorobenzene 8260
920114353 WATER 1,3-Dichloropropane 8260
920114353 WATER 1,4-Dichlorobenzene 8260
920114353 WATER 2,2-Dichloropropane 8260
920114353 WATER 2-Chlorotoluene 8260
920114353 WATER 4-Chlorotoluene 8260
920114353 WATER Benzene 8260
920114353 WATER Bromobenzene 8260
920114353 WATER Bromochloromethane 8260
920114353 WATER Bromodichloromethane 8260
920114353 WATER Bromoform 8260
920114353 WATER Bromomethane 8260
920114353 WATER Carbon Tetrachloride 8260
920114353 WATER Chlorobenzene 8260
920114353 WATER Chlorodibromomethane 8260
920114353 WATER Chloroethane 8260
920114353 WATER Chloroform 8260
920114353 WATER Chloromethane 8260
920114353 WATER cis-1,2-Dichloroethene 8260
Page 67 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
.. ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1 .
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0608 0697 06/08/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114353 WATER Dibromomethane 8260
920114353 WATER Dichlorodifiuoromethane 8260
920114353 WATER Ethyl benzene 8260
920114353 WATER Hexachlorobutadiene 8260
920114353 WATER lsopropylbenzene 8260
920114353 WATER m-Xylene and p-Xylene 8260
920114353 WATER Methylene chloride 8260
920114353 WATER n-Butylbenzene 8260
920114353 WATER n-Propylbenzene 8260
920114353 · WATER Naphthalene 8260
920114353 WATER o-Xylene 8260
920114353 WATER p-lsopropyltoluene 8260
920114353 WATER sec-Butylbenzene 8260
920114353 WATER Styrene 8260
920114353 WATER tert-Butylbenzene 8260
920114353 WATER Tetrachloroethene 8260
920114353 WATER Toluene 8260
920114353 WATER trans-1,2-Dichloroethene 8260
920114353 WATER Trichloroethene 8260
920114353 WATER T rich lorofi uoromethane 8260
920114353 WATER Vinyl Chloride 8260
920114957 WATER 1, 1, 1,2-Tetrachloroethane 8260
920114957 WATER 1, 1, 1-Trichloroethane 8260
920114957 WATER 1, 1,2,2-Tetrachloroethane 8260
920114957 WATER 1, 1,2-Trichloroethane 8260
920114957 WATER 1, 1-Dichloroethane 8260
920114957 WATER 1, 1-Dichloroethene 8260
920114957 WATER 1, 1-Dichloropropene 8260
920114957 WATER 1,2,3-Trichlorobenzene 8260
920114957 WATER 1,2,3-Trichloropropane 8260
Page 68 of 78
UNITS CONC QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 3.7 J 1
ug/L 5.0 u 1
ug/L 5.0 .u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - --· -

-

-

-

-
--

-
--

-

-

-
-· -
SAMPLE NAME SAMPLED
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191. WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 _ 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191. WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 . 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 VVX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114957 WATER 1,2,4-Trichlorobenzene 8260
920114957 WATER 1,2,4-Trimethylbenzene 8260
920114957 WATER 1,2-Dibromo-3-chloropropane 8260
920114957 WATER 1,2-Dibromoethane 8260
920114957 WATER 1,2-Dichlorobenzene 8260
920114957 WATER 1,2-Dichloroethane 8260
920114957 WATER 1,2-Dichloropropane 8260
920114957 WATER 1, 3,5-Trimethylbenzene 8260
920114957 WATER 1,3-Dichlorobenzene 826_0
920114957 WATER 1 ;3-Dichloropropane 8260
920114957 WATER 1,4-Dichlorobenzene 8260
920114957 WATER 2,2-Dichloropropane 8260
920114957 WATER 2-Chlorotoluene 8260
920114957 WATER 4-Chlorotoluene 8260
920114957 WATER Benzene 8260
920114957 WATER Bromobenzene 8260
920114957 WATER Bromochloromethane 8260
920114957 WATER Bromodichloromethane 8260
920114957 WATER Bromoform 8260
920114957 WATER Bromomethane 8260
920114957 WATER Carbon Tetrachloride 8260
920114957 WATER Chlorobenzene 8260
920114957 WATER Chlorodibromomethane 8260
920114957 WATER Chloroethane 8260
920114957 WATER Chloroform 8260
920114957 WATER Chloromethane 8260
920114957 WATER cis-1,2-Dichloroethene 8260
920114957 WATER Dibromomethane 8260
920114957 WATER Dichlorodiftuoromethane 8260
920114957 WATER Ethylbenzene 8260
920114957 WATER Hexachlorobutadiene 8260
920114957 WATER lsopropylbenzene 8260
Page 69 of 78
UNITS CONG QUAL DIL
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
-ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u· 1
u9/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1 -
August 4, 1997
.. --· - - - - - - - - - - - - - - - -
SAMPLE NAME SAMPLED
97191 WX.0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0f;97 0697 . 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0697 0697 06/09/97
97191 WX.0697 0697 06/09/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
. 97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 VVX0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
97191 WX.0610 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920114957 WATER m-Xylene and p-Xylene 8260
920114957 WATER Methylene chloride 8260
920114957 WATER n-Butylbenzene 8260
920114957 WATER n-Propylbenzene 8260
920114957 WATER Naphthalene 8260
920114957 WATER a-Xylene 8260
920114957 WATER p-lsopropyltoluene 8260
920114957 WATER sec-Butyl benzene 8260
920114957 WATER Styrene 8260
.. 920114957 WATER tert-Butylbenzene 8260
920114957 WATER Tetrachloroethene 8260
920114957 WATER Toluene 8260
920114957 WATER trans-1,2-Dichloroethene 8260
920114957 WATER Trichloroethene 8260
920114957 WATER Trichlorofluoromethane 8260
920114957 WATER Vinyl Chloride 8260
920116810 WATER 1, 1, 1,2-Tetrachloroethane 8260
920116810 WATER 1, 1, 1-Trichloroethane 8260
920116810 WATER 1, 1,2,2-Tetrachloroethane 8260
920116810 WATER 1, 1 ,2-Trichloroethane 8260
920116810 WATER 1, 1-Dichloroethane 8260
920116810 WATER 1, 1-Dichloroethene 8260
920116810 WATER 1, 1-Dichloropropene 8260
920116810 WATER 1,2,3-Trichlorobenzene 8260
920116810 WATER 1,2,3-Trichloropropane 8260
920116810 WATER 1,2,4-Trichlorobenzene 8260
920116810 WATER 1,2,4-Trimethylbenzene 8260
920116810 WATER 1,2-Dibromo-3-chloropropane 8260
920116810 WATER 1,2-Dibromoethane 8260
920116810 WATER 1,2-Dichlorobenzene 8260
Page 70 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 3.3 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L · 50· u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - - ----- - - - - - - - - - - - -
SAMPLE NAME SAMPLED
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX061.0 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 -wxo510 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 W';(06-W 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116810 WATER 1,2-Dichloroethane 8260
920116810 WATER 1,2-Dichloropropane 8260
920116810 WATER 1,3,5-Trimethylbenzene 8260
920116810 WATER 1,3-Dichlorobenzene 8260
920116810 WATER 1,3-Dichloropropane 8260
920116810 WATER 1,4-Dichlorobenzene 8260
920116810 WATER 2,2-Dichloropropane 8260
920116810 WATER 2-Chlorotoluene 8260
920116810 WATER 4-Chlorotoluene 8260
-920116810 WATER Benzene 8260
920116810 WATER Bromobenzene 8260
920116810 WATER Bromochloromethane 8260
920116810 WATER Bromodichloromethane 8260
920116810 WATER Bromoform 8260
920116810 WATER Bromomethane 8260
920116810 WATER Carbon Tetrachloride 8260
920116810 WATER Chlorobenzene 8260
920116810 WATER Chlorodibromomethane 8260
920116810 WATER Chloroethane 8260
920116810 WATER Chloroform 8260
920116810 WATER Chloromethane 8260
920116810 WATER cis-1,2-Dichloroethene 8260
920116810 WATER Dibromomethane 8260
920116810 WATER Dichlorodifluoromethane 8260
920116810 WATER Ethylbenzene 8260
920116810 WATER Hexachlorobutadiene 8260
920116810 WATER lsopropylbenzene 8260
920116810 WATER m-Xylene and p-Xylene 8260
920116810 WATER Methylene chloride 8260
920116810 WATER n-Butylbenzene 8260
920116810 WATER n-Propylbenzene 8260
920116810 WATER Naphthalene 8260
Page 71 of 78
UNITS CONG QUAL DIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 -u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 3.4 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0_610 0697 06/10/97
97191 WX0610 0697 06/10/97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX061i 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920116810 WATER o-Xylene 8260
920116810 WATER p-lsopropyltoluene 8260
920116810 WATER sec-Butyl benzene 8260
920116810 WATER Styrene 8260
920116810 WATER tert-Butylbenzene 8260
920116810 WATER Tetrachloroethene 8260
920116810 WATER Toluene 8260
920116810 WATER trans-1,2-Dichloroethene 8260
920116810 WATER Trichloroethene 8260
· 920116810 WATER Tricnlorofluoromethane 8260
920116810 WATER Vinyl Chloride 8260
920118510 WATER 1, 1, 1,2-Tetrachloroethane 8260
920118510 WATER 1, 1, 1-Trichloroethane 8260
920118510 WATER 1, 1,2,2-Tetrachloroethane 8260
920118510 WATER 1, 1,2-Trichloroethane 8260
920118510 WATER 1, 1-Dichloroethane 8260
920118510 WATER 1, 1-Dichloroethene 8260
920118510 WATER 1, 1-Dichloropropene 8260
920118510 WATER 1,2,3-Trichlorobenzene 8260
920118510 WATER 1,2,3-Trichloropropane 8260
920118510 WATER 1,2,4-Trichlorobenzene 8260
920118510 WATER 1,2,4-Trimethylbenzene 8260
920118510 WATER 1,2-Dibromo-3-chloropropane 8260
920118510 WATER 1,2-Dibromoethane 8260
920118510 WATER 1,2-Dichlorobenzene 8260
920118510 WATER 1,2-Dichloroethane 8260
920118510 WATER 1,2-Dichloropropane 8260
920118510 WATER 1,3,5-Trimethylbenzene 8260
920118510 WATER 1,3-Dichlorobenzene 8260
920118510 WATER 1,3-Dichloropropane 8260
Page 72 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L ·. 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- -·-- - - - - - --- - - - - - - -
SAMPLE NAME SAMPLED
97191 WX0611 0697 06/11/97
. 97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11 /97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/i i/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COM POUND/PARAMETER METHOD
920118510 WATER 1,4-Dichlorobenzene 8260
920118510 WATER 2,2-Dichloropropane 8260
920118510 WATER 2-Chlorotoluene 8260
920118510 WATER 4-Chlorotoluene 8260
920118510 WATER Benzene 8260
920118510 WATER Bromobenzene 8260
920118510 WATER Bromochloromethane 8260
920118510 WATER Bromodichloromethane 8260
920118510 WATER Bromoform 8260
920118510 WATER Bromo·methane ' 8260
920118510 WATER Carbon Tetrachloride 8260
920118510 WATER Chlorobenzene 8260
920118510 WATER Chlorodibromomethane 8260
920118510 WATER Chloroethane 8260
920118510 WATER Chloroform 8260
920118510 WATER Chloromethane 8260
920118510 WATE.R cis-1,2-Dichloroethene 8260
920118510 WATER Dibromomethane 8260
920118510 WATER Dichlorodifluoromethane 8260
920118510 WATER Ethyl benzene 8260
920118510 WATER Hexachlorobutadiene 8260
920118510 WATER lsopropylbenzene 8260
920118510 WATER m-Xylene and p-Xylene 8260
920118510 WATER Methylene chloride 8260
920118510 WATER n-Butylbenzene 8260
920118510 WATER n-Propylbenzene 8260
920118510 WATER Naphthalene 8260
920118510 WATER a-Xylene 8260
920118510 WATER p-lsopropyltoluene 8260
920118510 WATER sec-Butylbenzene 8260
920118510 WATER Styrene 8260
920118510 WATER tert-Butylbenzene 8260
Page 73 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0611 0697 06/11/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 \IVX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920118510 WATER Tetrachloroethene 8260
920118510 WATER Toluene 8260
920118510 WATER trans-1,2-Dichloroethene 8260
920118510 WATER Trichloroethene 8260
920118510 WATER Trichlorofluoromethane 8260
920118510 WATER Vinyl Chloride 8260
920119649 WATER 1, 1, 1,2-Tetrachloroethane 8260
. 920119649 -WATER 1, 1, 1-Trichloroethane 8260
920119649 WATER 1, 1,2,2-Tetrachloroethane 8260
920119649 WATER 1, 1 ,2-Trichloroethane 8260
920119649 WATER 1, 1-Dichloroethane 8260
920119649 WATER 1, 1-Dichloroethene 8260
920119649 WATER 1, 1-Dichloropropene 8260
920119649 WATER 1,2,3-Trichlorobenzene 8260
920119649 WATER 1,2,3-Trichloropropane 8260
920119649 WATER 1,2,4-Trichlorobenzene 8260
920119649 WATER 1,2,4-Trimethylbenzene 8260
920119649 WATER 1,2-Dibromo-3-chloropropane 8260
920119649 WATER 1,2-Dibromoethane 8260
920119649 WATER 1,2-Dichlorobenzene 8260
920119649 WATER 1,2-Dichloroethane 8260
920119649 WATER 1,2-Dichloropropane 8260
920119649 WATER 1,3,5-Trimethylbenzene 8260
920119649 WATER 1,3-Dichlorobenzene 8260
920119649 WATER 1,3-Dichloropropane 8260
920119649 WATER 1,4-Dichlorobenzene 8260
920119649 WATER 2,2-Dichloropropane 8260
920119649 WATER 2-Chlorotoluene 8260
920119649 WATER 4-Chlorotoluene 8260
920119649 WATER Benzene 8260
Page 74 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 1.1 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5,0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
- - - - -·-- - - - - - - - - - - - -
SAMPLE NAME SAMPLED
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 . 06/12/97 ·
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 VVX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
97191 WX0612 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119649 WATER Bromobenzene 8260
920119649 WATER Bromochloromethane 8260
920119649 WATER Bromodichloromethane 8260
920119649 WATER Bromoform 8260
920119649 WATER Bromomethane 8260
920119649 WATER Carbon Tetrachloride 8260
920119649 WATER Chlorobenzene 8260
920119649 WATER Chlorodibromomethane 8260
920119649 WATER Chloroethane 8260
920119649 WATER Chloroform 8260
920119649 WATER Chloromethane 8260
920119649 WATER cis-1,2-Dichloroethene 8260
920119649 WATER Dibromomethane 8260
920119649 WATER Dichlorodifluoromethane 8260
920119649 WATER Ethylbenzene 8260
920119649 WATER Hexachlorobutadiene 8260
920119649 WATER lsopropylbenzene 8260
920119649 WATER m-Xylene and p-Xylene 8260
920119649 WATER Methylene chloride 8260
920119649 WATER n-Butylbenzene 8260
920119649 WATER n-Propylbenzene 8260
920119649 WATER Naphthalene 8260
920119649 WATER o-Xylene 8260
920119649 WATER p-lsopropyltoluene 8260
920119649 WATER sec-Butylbenzene 8260
920119649 WATER Styrene 8260
920119649 WATER tert-Butylbenzene 8260
920119649 WATER Tetrachloroethene 8260
920119649 WATER Toluene 8260
920119649 WATER trans-1,2-Dichloroethene 8260
920119649 WATER Trichloroethene 8260
920119649 WATER Trichlorofluoromethane 8260
Page 75 of 78
UNITS CONG QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 ,. u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 WX0612 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 DI01 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 DI01 0697 06/12/97
97191 0101 0697 06/12/97
97191 DI01 0697 06/12/97
97191 DI01 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119649 WATER Vinyl Chloride 8260
920119541 WATER 1, 1, 1,2-Tetrachloroethane 8260
920119541 WATER 1, 1, 1-Trichloroethane 8260
920119541 WATER 1, 1,2,2-Tetrachloroethane 8260
920119541 WATER 1, 1,2-Trichloroethane 8260
920119541 WATER 1, 1-Dichloroethane 8260
920119541 WATER 1, 1-0ichloroethene 8260
920119541 WATER 1, 1-0ichloropropene 8260
920119541 WATER 1.2,3-Trichlorobenzene 8260
920119541 WATER 1,2,3-Trichloropropane 8260
920119541 WATER 1,2,4-Trichlorobenzene 8260
920119541 WATER 1,2,4-Trimethylbenzene 8260
920119541 WATER 1,2-0ibromo-3-chloropropane 8260
920119541 WATER 1,2-Dibromoethane 8260
920119541 WATER 1,2-0ichlorobenzene 8260
920119541 WATER 1,2-Dichloroethane 8260
920119541 WATER 1,2-0ichloropropane 8260
920119541 WATER 1,3,5-Trimethylbenzene 8260
920119541 WATER 1, 3-0ichlorobenzene 8260
920119541 WATER 1,3-0ichloropropane 8260
920119541 WATER 1,4-Dichlorobenzene 8260
920119541 WATER 2,2-Dichloropropane 8260
920119541 WATER 2-Chlorotoluene 8260
920119541 WATER 4-Chlorotoluene 8260
920119541 WATER Benzene 8260
920119541 WATER Bromobenzene 8260
920119541 WATER Bromochloromethane 8260
920119541 WATER Bromodichloromethane 8260
920119541 WATER Bromoform 8260
920119541 WATER Bromomethane 8260
Page 76 of 78
UNITS CONC QUAL OIL
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u -· 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L o.O u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
-------------------
SAMPLE NAME SAMPLED
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 D101 0697 06/12/97
97191 D101 0697 06/12/97
97191 0101 0697 06/12/97 .
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/J 2/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 D101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
97191 0101 0697 06/12/97
Project 97191
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
SAMPLE NO. MATRIX COMPOUND/PARAMETER METHOD
920119541 WATER Carbon Tetrachloride 8260
920119541 WATER Chlorobenzene 8260
920119541 WATER Chlorodibromomethane 8260
920119541 WATER Chloroethane 8260
920119541 WATER Chloroform 8260
920119541 WATER Chloromethane 8260
920119541 WATER cis-1,2-Dichloroethene 8260
920119541 WATER Dibromomethane 8260
920119541 WATER Dichlorodifluoromethane 8260 -.
920119541 WATER Ethylbenzene 8260
920119541 WATER Hexachlorobutadiene 8260
920119541 WATER lsopropylbenzene 8260
920119541 WATER m-Xylene and p-Xylene 8260
920119541 WATER Methylene chloride 8260
920119541 WATER n-Butylbenzene 8260
920119541 WATER n-Propylbenzene 8260
920119541 WATER Naphthalene 8260
920119541 WATER a-Xylene 8260
920119541 WATER p-lsopropyltoluene 8260
920119541 WATER sec-Butylbenzene 8260
920119541 WATER Styrene 8260
920119541 WATER tert-Butylbenzene 8260
920119541 WATER Tetrachloroethene 8260
920119541 WATER Toluene 8260
920119541 WATER trans-1,2-Dichloroethene 8260
920119541 WATER Trichloroethene 8260
920119541 WATER Trichlorofluoromethane 8260
920119541 WATER Vinyl Chloride 8260
Page 77 of 78
UNITS CONC QUAL OIL
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
ug/L 5.0 u 1
ug/L 1 J 1
ug/L 5.0 · u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 1. 1 J 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 5.0 u 1
ug/L 10 u 1
August 4, 1997
---- - - - ---- - - - - - - - - - -
Notes:
TABLE 1 -Results of Fixed-Base Laboratory Analyses
Lot 86 Superfund Site
Raleigh, North Carolina
1) Sample 97191 FD01 0697 is a duplicate of sample 97191 MW12 0697.
Sample 97191 FD02 0697 is a duplicate of sample 97191 MW02 0697.
2) Samples with "EB" suffixes are equipment blanks.
3) Samples with "WX" suffixes are trip blanks.
4) Sample 97191 DI01 0697 is a sample of laboratory-provided deionized water used for equipment blanks.
Abbreviations:
CONG Concentration of compound/parameter or, where a "U" is entered in the "QUAL" column, the laboratory's reporting limit
QUAL Qualifying note.
OIL Dilution factor.
u Compound/parameter was_not detected at or above the laboratory's reporting limit in the "CONG" column.
j Compoundlparamenter was detected at an estimated concentration below the laboratory's reporting limit
ug/L Micrograms per liter_
mg/L Milligrams per liter.
Project 97191 Page 78 of 78
August 4, 1997
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I
TABLE2
Summary of Results of Fixed-Base Laboratory Analyses
Mobile Laboratory Analyses, and Field-Measured Parameters
I
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I
I
I
I
I
I
I
I
I
u
I
I
I
I
I
I.
I
SAMPLE
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
MW02
FD02
FD02
FD02
FD02
FD02
FD02
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory An'alyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
Iron 200.7 mg/L 0.053
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 40
Manganese, Dissolved 200.7 mg/L 42
Alkalinity, Total 310.1 mg/L 49
Chloride 325.3 mg/L 63
Sulfate 375.2 mg/L. 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen. Nitrate 4500-NO3 F mg/L 8.8
Total Organic Carbon · 5310C mg/L 210
1, 1,2-Trichordethane 8260 ug/L 200
1,2,4-Trimethylbenzene 8260 ug/L 70
1,2-Dibromoethane 8260 ug/L 65000
1.2-Dichlorobenzene 8260 ug/L 65
1,2-Dichloroethane 8260 ug/L 235
1,2-Dichloropropane 8260 ug/L 20000
1,3-Dichloropropane 8260 ug/L 165
Benzene 8260 ug/L 7500
Bromobenzene 8260 ug/L 105
Carbon Tetrachloride 8260 ug/L 2600
Chlorobenzene 8260 ug/L 900
Chloroform 8260 ug/L 81000
Dichlorodifluoromethane 8260 ug/L 55
Ethylbenzene 8260 ug/L 700
m-Xylene and p-Xylene 8260 ug/L 1600
Methylene chloride 8260 ug/L 9500
a-Xylene 8260 ug/L 1200
Tetrachloroethene 8260 ug/L 1000
Toluene 8260 ug/L 13000
T richloroethene 8260 ug/L 2000
Disolved Hydrogen Note 1 nM 18.8
Disolved Oxygen Note 2 mg/L 0.29
Oxidation°Reduction Potential Note 3 mV 230
pH Note 4 pH units 6.2
Conductivity Note 5 us 422
Temperature Note 6 C 18.2
Iron 200.7 mg/L 0.054
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 41
Manganese, Dissolved 200.7 mg/L 43
Alkalinity, Total 310.1 mg/L 50
Chloride 325.3 mg/L 50
Page 1 of 18
OUAL OIL
1
u 1
1
1
1
10
u 1
u 1
u 1
u 1
10
4
J 50
J 50
500
J 50
J 50
500
J 50
50
J 50
50
50
500
J 50
50
50
500
50
50
500
50
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
5
August 4, 1997
I
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I
I
I
I
I
I
D
I
I
I
I
I
I
I
11 I
I
SAMPLE
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
FD02
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
Sulfate ' 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 8.5
Total Organic Carbon 5310G mg/L 190
1, 1, 1-Trichlor.oethane 8260 ug/L 31
1, 1,2,2-Tetrachloroethane 8260 ug/L 6.4
1, 1,2-Trichloroethane 8260 ug/L 180
1, 1-Dichloroethane 8260 ug/L 7.5
1, 1-Dichloroethene 8260 ug/L 19
1,2,3-Trichloropropane 8260 ug/L 130
1,2,4-Trimethylbenzene 8260 ug/L 56
1,2-Dibromo-3-chloropropane 8260 ug/L 330
1,2-Dibromoethane 8260 ug/L 56000
1,2-Dichlorobenzene 8260 ug/L 51
1,2-Dichloroethane 8260 ug/L 180
1,2-Dichloropropane 8260 ug/L 18000
1,3,5-Trimethylbenzene 8260 ug/L 30
1,3-Dichloropropane 8260 ug/L 150
Benzene 8260 ug/L 6500
Bromobenzene 8260 ug/L 81
Bromodichloromethane 8260 ug/L 5.2
Bromoform 8260 ug/L 4.8
Carbon Tetrachloride 8260 ug/L 2500
Chlorobenzene 8260 ug/L 810
Chlorodibromoethane 8260 ug/I 1.4
Chloroform 8260 ug/L 70000
cis-1,2-Dichloroethene 8260 ug/L 8.9
Dibromomethane 8260 ug/L 22
Dichlorodifluoromethane 8260 ug/L 24
Ethyl benzene 8260 ug/L 640
lsopropylbenzene 8260 ug/L 16
m-Xylene and p-Xylene 8260 ug/L 1500
Methylene chloride 8260 ug/L 9000
n-Propylbenzene 8260 ug/L 12
Naphthalene 8260 ug/L 22
o-Xylene 8260 ug/L 1200
p-lsopropyltoluene 8260 ug/L 2.1
Tetrachloroethene 8260 ug/L 820
Toluene 8260 ug/L 12000
Trichloroethene 8260 ug/L 1900
Trichlorofiuoromethane 8260 ug/L 33
Vinyl Chloride 8260 ug/L 1.2
Page 2 of 18
QUAL OIL
u 1
u 1
u 1
u 1
10
2
1
1
1
1
1
J 100
1
J 100
500
1
1
500
1
J 100
1
1
1
J 1
20
100
J 1
500
1
1
1
100
1
100
500
1
1
100
J 1
100
100
20
1
J 1
August 4, 1997
I
I
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I
I
I
I
I
I
I
D
I
I
I
I
I
I
SAMPLE
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
· MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
. MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
MW3
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
' Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD
Iron 200.7
Iron, Dissolved 200.7
Manganese 200.7
Manganese, Dissolved 200. 7-
Alkalinity, Total 310.1
Chloride 325.3
Sulfate 375.2
Ethane 3810
Ethene 3810
Methane 3810
Nitrogen, Nitrate 4500-NO3 F
Total Organic,Carbon 5310C
1, 1, 1-T richloroethane 8260
1, 1,2,2-Tetrachloroethane 8260
1, 1,2-Trichloroethane 8260
1, 1-Dichloroethane 8260
1, 1-Dichloroethene 8260
1,2,4-Trimethylbenzene 8260
1,2-Dibromoethane 8260
1,2-Dichlorobenzene 8260
1,2-Dichloroethane 8260
1,2-Dichloropropane 8260
1,3,5-Trimethylbenzene 8260
1,3-Dichloropropane 8260
Benzene 8260
Bromodichloromethane 8260
Bromoform 8260
Carbon Tetrachloride 8260
Chlorobenzene 8260
Chloroform 8260
cis-1,2-Dichloroethene 8260
Dichlorodifluoromethane 8260
Ethyl benzene 8260
lsopropylbenzene 8260
m-Xylene and p-Xylene 8260
Methylene chloride 8260
n-Propylbenzene 8260
Naphthalene ' 8260
o-Xylene ' 8260
p-lsopropyltoluene 8260
sec-Butylbenzene 8260
Tetrachloroethene 8260
Toluene 8260
trans-1,2-Dichloroethene 8260
Trichloroethene 8260
Trichlorofluoromethane 8260
Page 3 of 18
UNITS CONC
mg/L 0.54
mg/L 0.49
mg/L 6.9
mg/L 7.3
mg/L 35
mg/L 4.0
mg/L 5
ug/L 16
ug/L 15
ug/L 8.6
mg/L 0.053
mg/L 18
ug/L 47
ug/L 230
ug/L 41
ug/L 5.6
ug/L 34
ug/L 190
ug/L 720
ug/L 2
ug/L 220
ug/L 4000
ug/L 74
ug/L 5.8
ug/L 7900
ug/L 8.3
ug/L 4.6
ug/L 1600
ug/L 370
ug/L 60000
ug/L 18
ug/L 24
ug/L 160
ug/L 11
ug/L 380
ug/L 8300
ug/L 14
ug/L 40
ug/L 320
ug/L 3.8
ug/L 3.1
ug/L 87
ug/L 3500
ug/L 2.1
ug/L 4800
ug/L 26
QUAL OIL
1
1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
1
J 100
1
1
1
J 100
100
J 1
J 100
100
1
1
100
1
J 1
100
J 100
500
1
1
1
1
1
100
1
1
J 100
J 1
J 1
1
100
J 1
100
1
August 4, 1997
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I
I
I
I
I
I
R
I
I
I
I
I
I
SAMPLE
MW3
MW3
MW3
MW3
MW3
MW3
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04 .
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW04
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Disolved Hydrogen Note 1 nM 21.6
Disolved Oxygen Note 2 mg/L 0.53
Oxidation-Reduction Potential Note 3 mV 45
pH Note 4 pH units 6.67
Conductivity. Note 5 us 92.5
Temperature Note 6 C 18.7
Iron 200.7 mg/L 0.53
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.019
Manganese, Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 3.0
Chloride 325.3 mg/L 1.9
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.28
Total Organic Carbon 5310G mg/L 0.95
1,2-Dichloropropane 8260 ug/L 12
Carbon Tetrachloride 8260 ug/L 72
Chloroform 8260 ug/L 2800
Tetrachloroethene 8260 ug/L 7.7
Trichloroethene 8260 ug/L 13
Trichlorofiuoror'nethane 8260 ug/L 1.5
Disolved Hydrogen Note 1 nM 1.53
Disolved Oxygen Note 2 mg/L 6.8
Oxidation-Reduction Potential Note 3 mV 296
pH Note 4 pH units 5.64
Conductivity Note 5 us 18.36
Temperature Note 6 C 17.9
Iron 200.7 mg/L 0.22
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 18
Manganese, Dissolved 200.7 mg/L 18
Alkalinity, Total . 310.1 mg/L 28
Chloride 325.3 mg/L 53
Sulfate . 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L · 31
Page 4 of 18
QUAL OIL
1
NA
NA
NA
NA
NA
1
u 1
1
u 1
1
1
u 1
u 1
u 1
u 1
1
1
1
1
1
1
1
J 1
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
5
u 1
u 1
u 1
u 1
u 1
2
August 4, 1997
I
I
I
I
I
I
I
I
I
.I
I
u
I
I
I
I
I
I
I
SAMPLE
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW6
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
1, 1, 1-Trichloroethane 8260 ug/L 30
1, 1,2,2-Tetrachloroethane 8260 ug/L 52
1, 1-Qichloroethane 8260 ug/L 38
1,2-Dibromoethane 8260 ug/L 700
1,2-Dichlorobenzene 8260 ug/L 220
1,2-Dichloroethane 8260 ug/L 150
1,2-Dichloropmpane 8260 ug/L 3400
1,3,5-Trimethylbenzene 8260 ug/L 20
Benzene 8260 ug/L 1300
Bromodichloromethane 8260 ug/L 610
Carbon Tetrachloride 8260 ug/L 2000
Chlorobenzene 8260 ug/L 90
Chloro_form 8260 ug/L 50000
Ethyl benzene• 8260 ug/L 24
m-Xylene and:p-Xylene 8260 ug/L 84
Methylene chloride 8260 ug/L 3300
o-Xylene 8260 ug/L 220
Tetrachloroethene 8260 ug/L 700
Toluene 8260 ug/L 140
Trichloroethene 8260 ug/L 1200
Disolved Hydrogen Note 1 nM 2.1
Disolved Oxygen Note 2 mg/L 0.37
Oxidation-Reduction Potential Note 3 mV 250
pH Note 4 pH units 6.66
Conductivity Note 5 us 262
Temperature Note 6 C 16.6
Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 4.1
Manganese, Dissolved 200.7 mg/L 4.0
Alkalinity, Total 310.1 mg/L 19
Chloride 325.3 mg/L 24
Sulfate 375.2 mg/L 12
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L 54
1, 1,2-Trichloroethane 8260 ug/L 440
1,2,3-Trichloropropane 8260 ug/L 260
1,2-Dibromo-3-chloropropane 8260 ug/L 550
1,2-Dibromoethane 8260 ug/L 1600
1,2-Dichloroethane 8260 ug/L 110
1,2-Dichloropropane 8260 ug/L 9600
Page 5 of 18
QUAL OIL
J 20
J 20
J 20
20
20
20
20
J 20
20
20
20
J 20
20
J 20
J 20
20
20
20
20
20
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
1
u 1
u 1
u 1
u 1
4
50
50
50
50
J 50
50
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW07
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
MW08
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
1,3-Dichloropropane 8260 ug/L 95
Benzene 8260 ug/L 6100
Bromomethane 8260 ug/L 155
Carbon Tetrachloride 8260 ug/L 2000
Chlorobenzene 8260 ug/L 560
Chloroform 8260 ug/L 78000
Dichlorodifiuoromethane 8260 ug/L 85
Ethyl benzene 8260 ug/L 380
m-Xylene and p-Xylene 8260 ug/L 1000
Methylene chloride 8260 ug/L 14000
a-Xylene 8260 ug/L 410
Tetrachloroethene 8260 ug/L 550
Toluene 8260 ug/L 420
Trichloroethene 8260 ug/L 1400
Disolved Hydrogen Note 1 nM 22.2
Disolved Oxygen Note 2 mg/L 0.53
Oxidation-Reduction Potential Note 3 mV 284
pH Note 4 pH units 5.7
Conductivity Note 5 us 167.3
Temperature Note 6 C 18.4
Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.085
Manganese, Dissolved 200.7 mg/L 0.087
Alkalinity, Total 310.1 mg/L 6.0
Chloride 325.3 mg/L 6.3
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.78
Total Organic Carbon 5310C mg/L 6.2
1,2-Dibromoethane 8260 ug/L 5700
1,2-Dichloropropane 8260 ug/L 2000
Benzene 8260 ug/L 5300
Carbon Tetrachloride 8260 ug/L 750
Chloroform 8260 ug/L 43000
m-Xylene and p-Xylene 8260 ug/L 230
Methylene chloride 8260 ug/L 6300
a-Xylene 8260 ug/L 190
Toluene 8260 ug/L 430
T richloroethene 8260 ug/L 550
Disolved Hydrogen Note 1 nM 5.61
Disolved Oxygen Note 2 mg/L 0.29
Page 6 of 18
QUAL OIL
J 50
50
J 50
50
50
50
J 50
50
50
50
50
50
50
50
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
100
100
100
100
100
J 100
100
J 100
J 100
100
1
NA
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW08
MW08
MW08
MW08
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW10
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
MW11
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
Oxidation-Reduction Potential Note 3 mV 274
pH Note 4 pH units 5.6
Conductivity Note 5 us 38.7
Temperature Note 6 C 17.7
Iron 200.7 mg/L 0.27
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.062
Manganese, Dissolved 200.7 mg/L 0.060
Alkalinity, Total 310.1 mg/L 2.0
Chloride 325.3 mg/L 3.5
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 1.4
Total Organic Carbon 5310C mg/L 1.2
Toluene 8260 ug/L 1.3
Disolved Hydrogen Note 1 nM 5.96
Disolved Oxygen Note 2 mg/L 9.24
Oxidation-Reduction Potential Note 3 mV 354
pH Note 4 pH units 5
Conductivity Note 5 us 34.2
Temperature Note 6 C 18.3
Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.068
Manganese, Dissolved 200.7 mg/L 0.053
Alkalinity, Total 310.1 mg/L 12
Chloride 325.3 mg/L 2.8
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.72
Total Organic Carbon 5310C mg/L 2.7
1,2,4-Trimethylbenzene 8260 ug/L 4.9
1,2-Dichloropropane 8260 ug/L 5.0
Benzene 8260 ug/L 23
Carbon Tetrachloride 8260 ug/L 23
Chloroform 8260 ug/L 4700
m-Xylene and p-Xylene 8260 ug/L 84
Methylene chloride 8260 ug/L 8.2
Page 7 of 18
QUAL OIL
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
10
1
J 1
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
J 1
1
1
1
1
1
1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW11
MW11
MW11
· MW11
MW11
MW11
MW11
MW11
MW11
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
MW12
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Tetrachloroethene 8260 ug/L 30
Toluene 8260 ug/L 2.6
Trichloroethene 8260 ug/L 12
Disolved Hydrogen Note 1 nM 1.07
Disolved Oxygen Note 2 mg/L 4.06
Oxidation-Reduction Potential Note 3 mV 442
pH Note 4 pH units 5.68
Conductivity Note 5 us 38.1
Temperature Note 6 C 15.9
Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 4.6
Manganese, Dissolved 200.7 mg/L 4.7
Alkalinity, Total 310.1 mg/L 2.0
Chloride 325.3 mg/L 32
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.95
Total Organic Carbon 5310C mg/L 69
1, 1,2,2-Tetrachloroethane 8260 ug/L 140
1, 1,2-Trichloroethane 8260 ug/L 6300
1,2,3-Trichloropropane 8260 ug/L 2000
1,2-Dibromo-3-chloropropane 8260 ug/L 4700
1,2-Dibromoethane . 8260 ug/L 6300
1,2-Dichloroethane 8260 ug/L 320
1,2-Dichloropropane 8260 ug/L 39000
Benzene 8260 ug/L 12000
Bromobenzene 8260 ug/L 110
Carbon Tetrachloride 8260 ug/L 4700
Chlorobenzene 8260 ug/L 450
Chloroform . 8260 ug/L 65000
Ethyl benzene 8260 ug/L 490
m-Xylene and p-Xylene 8260 ug/L 1500
Methylene chloride 8260 ug/L 6900
o-Xylene 8260 ug/L 810
Toluene 8260 ug/L 7800
Trichloroethene 8260 ug/L 1100
Disolved Hydrogen Note 1 nM 8.71
Disolved Oxygen Note 2 mg/L 1.42
Oxidation-Reduction Potential Note 3 mV 261
pH Note 4 pH units 4.9
Conductivity Note 5 us 139.4
Page 8 of 18
QUAL OIL
1
J 1
1
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
4
J 100
100
100
100
100
J 100
100
100
J 100
100
J 100
100
J 100
100
100
100
100
100
1
NA
NA
NA
NA
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW12
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD0_1
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
FD01
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Temperature Note 6 C 18.1
' Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 4.5
Manganese, Dissolved 200.7 mg/L 4.6
Alkalinity, Total 310.1 mg/L 4.0
Chloride 325.3 mg/L 32
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.94
Total Organic Carbon 5310C mg/L 75
1, 1,2,2-Tetrachloroethane 8260 ug/L 140
1, 1,2-Trichloroethane 8260 ug/L 5900
1,2,3-Trichloropropane 8260 ug/L 1900
1,2,4-Trimethylbenzene 8260 ug/L 110
1,2-Dibromos3-chloropropane 8260 ug/L 4400
1,2-Dibromoethane 8260 ug/L 6500
1,2-Dichloroethane 8260 ug/L 310
1,2-Dichloropropane 8260 ug/L 34000
1,3-Dichloropropane 8260 ug/L 510
Benzene 8260 ug/L 12000
Bromobenzene 8260 ug/L 130
Carbon Tetrachloride 8260 ug/L 4900
Chlorobenzene 8260 ug/L 490
Chloroform ; 8260 ug/L 60000
Ethylbenzene 8260 ug/L 550
m-Xylene and p-Xylene 8260 ug/L 1700
Methylene chloride 8260 ug/L 6800
a-Xylene 8260 ug/L 840
Toluene 8260 ug/L 7600
Trichloroethene 8260 ug/L 1100
:
Iron 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 1.5
Manganese, Dissolved 200.7 mg/L 1.6
Alkalinity, Total 310.1 mg/L 1.0
Chloride 325.3 mg/L 8.9
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Page 9 of 18
QUAL OIL
NA
u 100
u 100
100
100
100
100
u 100
u 100
u 100
u 100
100
100
J 100
100
100
J 100
100
100
J 100
100
100
100
J 100
100
J 100
100
100
100
100
100
100
100
u 1
u 1
1
1
1
1
u 1
u 1
u 1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW13
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW15
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 9.0
Total Organic Carbon 5310C mg/L 2.8
1,3-Dichlorobenzene 8260 ug/L 3.4
Toluene 8260 ug/L 1.3
Disolved Hydrogen Note 1 nM 12.3
Disolved-Oxygen Note 2 mg/L 6.27
Oxidation-Reduction Potential Note 3 mV 327
pH Note4 pH units 4.67
Conductivity Note 5 us 115.4
Temperature, Note 6 C 17.1
Iron 200.7 mg/L 0.32
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.099
Manganese,· Dissolved 200.7 mg/L 0.099
Alkalinity, Total 310.1 mg/L 7.0
Chloride 325.3 mg/L 4.0
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.41
Total Organic Carbon 5310C mg/L 1. 1
Chloroform _ 8260 ug/L 30
Disolved Hydrogen Note 1 nM 0.756
Disolved Oxygen Note 2 mg/L 7.11
Oxidation-Reduction Potential Note 3 mV 349
pH Note 4 pH units 5.37
Conductivity Note 5 us 26.7
Temperature Note 6 C 20.6
Iron 200.7 mg/L 0.97
Iron, Dissolved 200.7 mg/L 0.97
Manganese _ 200.7 mg/L 15
Manganese, Dissolved 200.7 mg/L 15
Alkalinity, Total 310.1 mg/L 39
Chloride 325.3 mg/L 10
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L 73
Page 10 of 18
QUAL OIL
u 1
10
1
J 1
J 1
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
1
1
NA
NA
NA
NA
NA
1
1
1
1
1
1
u 1
u 1
u 1
u 1
u 1
4
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW16
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
MW17
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
1, 1,2-Tricholorethane 8260 ug/L 390
1,2-Dibromoethane 8260 ug/L 5300
1,2-Dichloropropane 8260 ug/L . 4400
Benzene 8260 ug/L 3300
Carbon Tetrachloride 8260 ug/L 1100
Chlorobenzene 8260 ug/L 400
Chloroform 8260 ug/L 35000
Ethylbenzene 8260 ug/L 380
m-Xylene and p-Xylene 8260 ug/L 1300
Methylene chloride 8260 ug/L 1400
a-Xylene 8260 ug/L 630
Tetrachloroethene 8260 ug/L 1800
Toluene 8260 ug/L 9400
Trichloroethene 8260 ug/L 3400
Dissoved Hydrogen Note 1 nM 12.5
Dissoved Oxygen Note 2 mg/L 0.23
Oxidation-Reduction Potential Note 3 • mV 30
pH Note 4 pH units 6.4
Conductivity · Note 5 us 114.7
Temperature Note 6 C 16.8
.
Iron 200.7 mg/L 0.47
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.073
Manganese, Dissolved 200.7 mg/L 0.063
Alkalinity, Total 310.1 mg/L 2.0
Chloride 325.3 mg/L 3.7
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.59
Total Organic Carbon 5310C mg/L 1.0
1,2-Dichloropropane 8260 ug/L 9.7
Benzene 8260 ug/L 12
Chloroform 8260 ug/L 9.0
Toluene 8260 ug/L 13
Disolved Hydrogen Note 1 nM 3.24
Disolved Oxygen Note 2 mg/L 6.04
Oxidation-Reduction Potential Note 3 mV 339
pH Note 4 pH units 5.25
Conductivity Note 5 us 29.5
Temperature Note 6 C 19.9
Page 11 of18
QUAL DIL
J 100
100
100
100
100
J 100
100
J 100
100
100
100
100
100
100
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW27
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW32
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUN.D/PARAMETER METHOD UNITS CONC
Iron 200.7 mg/L 9.3
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.47
Manganese, Dissolved 200.7 mg/L 0.050
Alkalinity, Total 310.1 mg/L 7.0
Chloride 325.3 mg/L 3.5
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.71
Total Organic Carbon 5310C mg/L 1.9
Carbon Tetrachloride 8260 ug/L 2.6
Chloroform , 8260 ug/L 8.7
Trichloroethene 8260 ug/L 1.3
Disolved Hydrogen Note 1 nM 308
Disolved Oxygen Note 2 mg/L 5.33
Oxidation-Reduction Potential Note 3 mV 319
pH Note 4 pH units 5.78
Conductivity· Note 5 us 37.7
Temperature Note 6 C 19.6
Iron 200.7 mg/L 2.3
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.024
Manganese, Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 6.0
Chloride 325.3 mg/L 3.5
Sulfate ' 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Total Organic Carbon 5310C mg/L 0.84
Iron 200.7 mg/L 2.3
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.024
Manganese, Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 6.0
Chloride 325.3 mg/L 3.5
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.20
Total Organic Carbon 5310C mg/L 0.84
Page 12 of 18
QUAL OIL
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
J 1
1
J 1
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW32
MW32
MW32
MW32
MW32
MW32
MW32
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW33
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
MW34S
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONG
Tetrachloroethene 8260 ug/L 1.2
Disolved Hydrogen Note 1 nM 16
Disolved Oxygen Note 2 mg/L 6.4
Oxidation-Reduction Potential Note 3 mV 306
pH Note 4 pH units 5.03
Conductivity Note 5 us 33.1
Temperature Note 6 C 19
Iron 200.7 mg/L 0.31
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.012
Manganese, Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 26
Chloride ' 325.3 mg/L 2.1
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L 0.67
Toluene 8260 ug/L 1.4
Disolved Hydrogen Note 1 nM 1.43
Disolved Oxygen Note 2 mg/L 4.89
Oxidation-Reduction Potential Note 3 mV 225
pH Note 4 pH units 5.85
Conductivity Note 5 us 66.2
Temperature. Note 6 C 17
Iron 200.7 mg/L 1.7
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.015
Manganese, Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 1.0
Chloride 325.3 mg/L 1.6
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L 1.0
Disolved Hydrogen Note 1 nM 1.85
Disolved Oxygen Note 2 mg/L 6.83
Oxidation-Reduction Potential Note 3 mV 301
pH Note 4 pH units 5.68
Page 13 of 18
QUAL OIL
J 1
1
NA
, NA
NA
NA
NA
1
u 1
1
u 1
1
1
u 1
u 1
u 1
u 1
u 1
1
J 1
1
NA
NA
NA
NA
NA
1
u 1
1
u 1
u 1
1
u 1
u 1
u 1
u 1
u 1
1
NA
NA
NA
NA
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
SAMPLE
MW34S
MW34S
MW34D
MW34D
MW34D
MW34D
MW340
MW340
MW34D
MW340
MW34D
MW34D
MW340
MW340
MW34D
MW340
MW34D
MW340
MW34D
MW340
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35S
MW35D
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Conductivity Note 5 us 40.5
Temperature Note 6 C 15.8
Iron 200.7 mg/L 2.1
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.25
Manganese, Dissolved 200.7 mg/L 0.072
Alkalinity, Total 310.1 mg/L 97
Chloride ' 325.3 mg/L 1.9
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic Carbon 5310C mg/L 0.98
Disolved Hydrogen Note 1 nM 318
Disolved Oxygen Note 2 mg/L 0.18
Oxidation-Reduction Potential Note 3 mV -86
pH Note 4 pH units 10.62
Conductivity' Note 5 us 212
Temperature Note 6 C 15.8
Iron 200.7 mg/L 0.76
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.025
Manganese, Dissolved 200.7 mg/L 0.011
Alkalinity, Total 310.1 mg/L 6.0
Chloride 325.3 mg/L 2.6
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.87
Total Organic Carbon 5310C mg/L 1.2
Methylene chloride 8260 ug/L 9.6
Disolved Hydrogen Note 1 nM 2.6
Disolved Oxygen Note 2 mg/L 3.21
Oxidation-Reduction Potential Note 3 mV 298
pH Note 4 pH units 5.34
Conductivity ' Note 5 us 34
Temperature Note 6 C 16.3
Iron 200.7 mg/L 0.70
Page 14 of 18
QUAL OIL
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
u 1
1
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
1
1
1
1
NA
NA
NA
NA
NA
1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
••
I
I
I
.:1
I
I
SAMPLE
MW350
MW350
MW35D
MW35D
MW350
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Iron, Dissolved 200.7 mg/L 0.050
M.anganese 200.7 mg/L 0.062
Manganese, •Dissblved 200.7 mg/L 0.035
Alkalinity, Total 310.1, mg/L 43
Chloride 325.3 mg/L · 1.6
MW35D .· Sulfate 375.2 mg/L 5
MW35D Ethane 3810 ug/L 16
MW35D Ethene 3810 ug/L 15
MW35D Methane 3810 ug/L 8.6
MW350 Nitrogen, Nitrate 4500-N03 F mg/L 0.05
MW35D Total Organic Carbon 5310C mg/L 0.67
MW350 Disolved Hydrogen Note 1 nM 141.3
MW350 Disolved Oxygen Note 2 mg/L 6.15
MW350 Oxidation-Reduction Potential Note 3 mV 182
MW350 pH Note 4 pH units 6.42
MW350 Conductivity Note 5 us 82.3
MW350 Temperature Note 6 C 16.6
MW36S Iron 200.7 mg/L 0.050
MW36S Iron, Dissolved 200.7 mg/L 0.050
MW36S Manganese 200.7 mg/L 9.9
MW36S Manganese, Dissolved 200.7 mg/L 10
MW36S Alkalinity, Total 310.1 mg/L 19
MW36S Chloride 325.3 mg/L 14
MW36S Sulfate 375.2 mg/L 5.4
MW36S Ethane 3810 ug/L 16
MW36S Ethene 3810 ug/L 15
MW36S Methane 3810 ug/L 8.6
MW36S Nitrogen, Nitrate 4500-N03 F mg/L 0.05
MW36S Total Organic Carbon 5310C mg/L 140
MW36S 1, 1,2,2-Tetrachloroethane 8260 ug/L 200
MW36S 1, 1,2-Trichloroethane 8260 ug/L 220
MW36S 1,2-Dibromoethane 8260 ug/L 7000
MW36S 1,2-Dichloroethane 8260 ug/L 1000
MW36S 1,2-Dichloropropane 8260 ug/L 2000
MW36S Benzene 8260 ug/L 7500
MW36S Bromodichloromethane 8260 ug/L 3700
MW36S Carbon Tetrachloride 8260 ug/L 1800
MW36S Chloroform 8260 ug/L 34000
MW36S m-Xylene and p-Xylene 8260 ug/L 160
MW36S Methylene chloride 8260 ug/L 8800
MW36S a-Xylene 8260 ug/I 310
MW36S Toluene 8260 ug/L 300
MW36S Trichloroethene 8260 ug/L 1900
MW36S Disolved Hydrogen Note 1 nM 30.6
Project 97191 Page 15 of 18
QUAL OIL
u 1
1
1
1
1
u 1
u 1
u 1
u 1
u 1
1
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
1
u 1
u 1
u 1
u 1
4
J 100
J 100
100
100
100
100
100
100
100
J 100
100
J 100
J 100
100
1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
•· I
i -. I
' -
I
I
SAMPLE
MW36S
MW36S
MW36S
MW36S
MW36S
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW36D
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
Disolved Oxygen Note 2 mg/L 0,33
Oxidation-Reduction Potential Note 3 mV 282
pH Note 4 pH units 5,7
Conductivity Note 5 us 92.6
Temperature Note 6 C 17.7
Iron 200.7 mg/L 0.093
Iron, Dissolved 200.7 mg/L 0.050
Manganese' 200.7 mg/L 0.010
Manganese,' Dissolved 200.7 mg/L 0.010
Alkalinity, Total 310.1 mg/L 77
Chloride 325.3 mg/L 1.9
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.06
Total Organic Carbon 5310C mg/L 0.89
1,2-Dibromoethane 8260 ug/L 6.5
1,2-Dichloropropane 8260 ug/L 8.2
Carbon Tetrachloride 8260 ug/L 12
Chloroform 8260 ug/L 270
Methylene chloride 8260 ug/L 6.3
Tetrachloroethene 8260 ug/L 9.3
Trichloroethene 8260 ug/L 9.1
Disolved Hydrogen Note 1 nM 10.6
Disolved Oxygen Note 2 mg/L 2.3
Oxidation-Reduction Potential Note 3 mV 117
pH Note 4 pH units 6.69
Conductivity Note 5 us 169
Temperature Note 6 C 17.3
Iron 200.7 mg/L 0.053
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 7.3
Manganese, Dissolved 200.7 mg/L 7.3
Alkalinity, Total 310.1 mg/L 17
Chloride 325.3 mg/L 27
Sulfate 375.2 mg/L 5
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/I 8.6
Nitrogen, Nitrate 4500-NO3 F mg/L 0.05
Total Organic ,Carbon 5310C mg/L 18
Page 16 of 18
QUAL OIL
NA
NA
NA
NA
NA
1
u 1
u 1
u 1
1
1
u 1
u 1
u 1
u 1
1
1
1
1
1
1
1
1
1
1
NA
NA
NA
NA
NA
1
u 1
1
1
1
1
u 1
u 1
u 1
u 1
u 1
1
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
' I
I
SAMPLE
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW37
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
MW38
Project 97191
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mobile Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
COMPOUND/PARAMETER METHOD UNITS CONC
1,2-Dichloroethane 8260 ug/L 110
1,2-Dichloropropane 8260 ug/L 520
Bezene ' 8260 ug/L 6900
Carbon Tetrachloride 8260 ug/L 4300
Chlorobenzene 8260 ug/L 100
Chloroform 8260 ug/L 45000
m-Xylene and p-Xylene 8260 ug/L 350
Methylene chloride 8260 ug/L 8100
o-Xylene 8260 ug/L 220
Tetrachloroethene 8260 ug/L 220
Toluene 8260 ug/L 700
Trichloroethene 8260 ug/L 680
Disolved Hydrogen Note 1 nM 129.3
Disolved Oxygen Note 2 mg/L 0.47
Oxidation-Reduction Potential Note 3 mV 246
pH Note 4 pH units 5.7
Conductivity Note.5 us 134.9
Temperature, Note 6 C 19.2
Iron ' 200.7 mg/L 0.050
Iron, Dissolved 200.7 mg/L 0.050
Manganese 200.7 mg/L 0.019
Manganese, Dissolved 200.7 mg/L 0.028
Alkalinity, Total 310.1' mg/L 91
Chloride 325.3 mg/L 2.1
Sulfate 375.2 mg/L • 7.9
Ethane 3810 ug/L 16
Ethene 3810 ug/L 15
Methane 3810 ug/L 8.6
Nitrogen, Nitrate 4500-N03 F mg/L 0.05
Total Organic Carbon 5310C mg/L 1.3
Chloroform 8260 ug/L 1
Disolved Hydrogen Note 1 nM 75.8
Disolved Oxygen Note 2 mg/L 1.23
Oxidation-Reduction Potential Note 3 mV 77
pH Note 4 pH units 6.68
Conductivity Note 5 us 213
Temperature Note 6 C 16.9
Page 17 of 18
QUAL OIL
J 100
100
100
100
J 100
100
J. 100
100
J 100
J 100
100
100
1
NA
NA
NA
NA
NA
u 1
u 1
1
1
1
1
1
u 1
u 1
u 1
u 1
1
J 1
1
NA
NA
NA
NA
NA
August 4, 1997
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
~
TABLE 2 -Summary of Results of Fixed-Base Laboratory Analyses,
Mob!le Laboratory Analyses, and Field-Measured Parameters
Lot 86 Superfund Site
Raleigh, North Carolina
1. Dissolved hvdroaen analvsis conducted in an on-site mobile laboratorv usina a aas chromatoaraoh and a reducina aas
gas detector.
2. Dissolved oxvaen was measured in the field usina a direct readina dissolved oxvnen meter and aalvanic dissolved
oxvaen probe.
3. Oxidation-reduction potential was measured in the field usina a direct-readino oxidation-reduction oot1::mtial meter
aaainst a silver/silver chloride reference electrode.
4. oH was measured in the field usina a oH meter with automatic temperature compensation.
5. Conductivitv was measured in the field usina a direct readinq conductivity meater.
6. Temoerature was measured in the field usina a oH meter.
7. See Table 1 for the followino results not shown on this summarv table: Method 8260 oarameters not detected at
concentrations above the reoortino limit.
8. See Table 1 for results for the followina samoles not shown on this summarv table: trio blanks, eauioment blanks,
and deionized water sample.
Ab!;m~vi~tiQos;
CONC Concentration of comoound/oarameter or, where a "U" is entered in the "QUAL" column, the
laboratorv's reoortina limit.
QUAL Qualifvina note.
DIL Dilution factor.
u Comoound/oarameter was not detected at or above the laboratorv's reoortina limit in the "CONC"
column. '
J Compound/parameter was detected at an estimated concentration below the laboratorv's reoortina limit.
uq/L Micrograms per liter.
mall Milliqrams per liter.
nM Nanomolar
mV Millivolts
us Microsiemens
C Dearees centiarade
Project 97191 Page 18 of 18 August 4, 1997