NCD122263825_20110528_JFD Electronics - Channel Master_FRBCERCLA SPD_Industrial Users Reports 2008 - 2011-OCR

AECOM
May 18, 2011
Mr. Larry Thomas
City Engineer
City of Oxford
P.O. Box 1307
AECOM
8540 Colonnade Center Drive Suite 306
Raleigh, NC 27615
Oxford, North Carolina 27565
Subject: Industrial Users Report for May 2011
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 60160750
Dear Mr. Thomas,
919.872.6600 tel
919.872.7996 fax
SUPERFUND SECTION
On behalf of The Unimax Corporation and Avnet, Inc., AECOM North Carolina, Inc. (AECOM) is
submitting the Quarterly Industrial User Permit report for the months of February, March, and April
2011. This report is prepared in accordance with permit requirements for the discharge of treated
groundwater at the above referenced site.
If you have any questions, please contact Gerald Hornaday at 919-239-7148.
Yours sincerely,
/: J.i _.,. .. ;' .'I f--,.1,p,11,1.,;,r /f,<1r,;,,,,1/l.f'fl,1.,,,-.,
Gerald Hornad£y, P.E. /
Project Engineer
Enclosure
}~)AJ
Matthew J. Zenker, Ph.D., P.E.
Project Engineer
cc: Steve Kempf -Utilities and Industries Management Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Robert West, RPM -USEPA Superfund
Bill Doucette -Permittee Representative (electronic mail)
File
6016075.108
INDUSTRIAL USER REPORTING FORM
1.U. PERMIT NO:_--'G"'-0,,..,0'--'1 _____ DISCHARGE NO: ___ ....,0"'0-'-1 _____ _
MONTHS: February, March, and April YEAR: ----'2"'0"-1'""'1 _____ _
1.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERATOR IN RESPONSIBLE CHARGE (ORC): AECOM North Carolina Inc.
LABORATORY PERFORMING ANALYSIS: Test America Inc.
PERSON(S) COLLECTING SAMPLES: Luke Kemp (AECOM). Aaron Hill (EFM, Inc.)
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box I 307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. [gJ
(Compliant)
All monthly averages and/or other limitations do not meet permit monitoring requirements. D
(Noncomplianl)
If the facility is noncompliant, please comment on corrective actions being taken in respect lo
cquiprr_ient, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete lo the best of my knowledge:
Signature of Permittce Representative
William H. Doucette, Jr., Ph.D.
May 18,201 I
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.U. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
1.U. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
PERSON(S) COLLECTING SAMPLES:
PARAMETER
Daily Average Flow (MGD)
Telrach1oroelhylene
1, 1-0lchloroethane
cis-1,2 Dichloroethene
Chlorobenzene
Toluene
1, 1-Dlchloroelhylene
trans-1,2 Dichloroelhyl.ene
Trichloroethene
Vinyl Chloride
Cyanide (lo1al)
pH
Temperature
Monitoring requirement only
MGD Million Gallons per day.
µg/L Micrograms per liter.
mg/L Milligrams per liter.
SU Standard Uni1s.
'C Degrees Centigrade.
G001
001
February, March, and April
2011
JFD Electronics/Channel Master NPL Site
Granville
AECOM North Carolina, Inc.
TestAmerica
Luke Kemp (AECOM), Aaron Hill (EFM Inc.)
PERMIT LIMITS
Dally Maximum
O.D40
0.05
5.0 to 10.0
40
UNITS
MGO
µg/L
j.JglL
µg/L
µg/L
µg/L
µgll
µgll
µg/L
µg/L
mg/L
SU
oc
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
< Compound was not detected above the quantitation limit
NS Not sampled
G:\Env\JFDCHANN\NC0202.170\C,Iy of Ox!ord\lURTable May 2011.xls\Table 1\5/1712011
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335.2
Field
Field
QUARTERLY MEASUREMENT
DATES
2/812011 3121/2011 4127/2011
0.014 0.020 0.020
NS NS <1.0
NS NS ..:1.0
NS NS ..:1.0
NS NS ..:1.0
NS NS ..:1,0
NS NS ..:1.0
NS NS <1.0
NS NS ..:1.0
NS NS <1.0
NS NS ..:0.0050
8.01 7.69 7.69
14.8 17.8 19,3
Test America
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-67821-1
Job Description: JFD/Oxford
For:
AECOM, Inc.
8540 Colonnade Center Drive
Suite 306
Raleigh, NC 27615
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
05/13/2011
Apprnvl!d Jo, rol11a$11
Kalhl)ln Sm,th
Pmiect Manager I
5/1312011 3.55 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report. ·
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah. GA 31404
Tel [phone] Fax [phone] www testamericainc com
Page 1 of 61
Comments
No additional comments.
Receipt
Job Narrative
680-67821-1
All samples were received in good condition within temperature requirements.
GC/MS VOA
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted.
Page 2 of 61
Client: AECOM, Inc.
Description
Matrix: Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Amenable
Distillation, Cyanide
Cyanide, Total
Distillation, Cyanide
TOG
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Job Number: 680-67821-1
Lab Location Method Preparation Method
TAL SAV SW846 8260B
TAL SAV SW846 5030B
TAL SAV MCAWW335.1
TALSAV Distill/CN
TAL SAV MCAWW 335.4
TAL SAV Distill/CN
TAL SAV MCAWW415.1
MCA\/1/W = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Savannah Page 3 of 61
METHOD/ ANALYST SUMMARY
Client: AECOM, Inc. Job Number: 680-67821-1
Method Analyst Analyst ID
SW846 82608 Cowart, Judson WJC
MCAWW 335.1 McDonald, Debbie DAM
MCAWW 335.4 McDonald, Debbie DAM
MCAWW 415.1 Holmes, Tinita TH
TestAmerica Savannah
Page 4 of 61
SAMPLE SUMMARY
Client: AECOM, Inc. Job Number: 680-67821-1
Date/Time Date/Time
Lab Samele ID Client Samele ID Client Matrix Sameled Received
680-67821-1 Trip Blank Water 04/26/2011 0000 04/28/2011 1003
680-67821-2 CMMW-26 Water 04/26/2011 1010 04/28/2011 1003
680-67821-3 CMMW-24 Water 04/26/2011 1015 04/28/2011 1003
680-67821-4 CMMW-22A Water 04/26/2011 1130 04/28/2011 1003
680-67821-5 CMMW-19 Water 04/26/2011 1250 04/28/2011 1003
680-67821,6 CMMW-15 Water 04/26/2011 1252 04/28/2011 1003
680-67821-7 CMMW-25 Water 04/26/2011 1342 04/28/2011 1003
680-67821-8 CMMW-03 Water 04/26/2011 1433 04/28/2011 1003
680-67821-9 CMMW-18 Water 04/26/2011 1520 04/28/2011 1003
680-67821-10 CMMW-02 Water 04/26/2011 1545 04/28/2011 1003
680-67821-11 CMMW-21 Water 04/26/2011 1650 04/28/2011 1003
680-67821-12 CMMW-20 Water 04/26/2011 1812 04/28/2011 1003
680-67821-13 FB-01 Water 04/26/2011 0930 04/28/2011 1003
680-67821-14 EB-01 Water 04/26/2011 1035 04/28/2011 1003
680-67821-15 CMMW-17 Water 04/26/2011 0730 04/28/2011 1003
680-67821-16 CMMW-07 Water 04/26/2011 0740 04/28/2011 1003
680-67821-17 CMMW-23 Water 04/26/2011 0800 04/28/2011 1003
680-67821-18 CMMW-04 Water 04/26/2011 0915 04/28/2011 1003
680-67821-19 DUP-01 Water 04/26/2011 0000 04/28/2011 1003
680-67821-20 CMMW-10 Water 04/26/2011 1035 04/28/2011 1003
680-67821-21 CMMW-05 Water 04/26/2011 1155 04/28/2011 1003
680-67821-22 SYS-EFF Water 04/26/2011 1215 04/28/2011 1003
680-67821-23 SYS-INF Water 04/26/2011 1230 04/28/2011 1003
680-67821-24 PW-1 Water 04/26/2011 1245 04/28/2011 1003
680-67821-25 PW-2 Water 04/26/2011 1300 04/28/2011 1003
680-67821-26 PW-3 Water 04/26/2011 1315 04/28/2011 1003
680-67821-27 PW-4 Water 04/26/2011 1330 04/28/2011 1003
680-67821-28 PW-5 Water 04/26/2011 1345 04/28/2011 1003
TestAmerica Savannah Page 5 of 61
Analytical Data
Client: AECOM, Inc. Job Number: 680-67821-1
Client Sample ID: SYS-EFF
Lab Sample ID:
Client Matrix:
680-67821-22
Water
Analysis Method: 82608
Prep Method: 50308
Dilution: 1.0
Analysis Date: 05/0712011
Prep Date: 0510712011
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroelhane
Chloroform
Chtoromethane
cis-1,2-Dichloroethene
cis-1,3-0ich!oropropene
Oichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1 , 1 -Dich1oroethene
1,2-0ichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (Ml8K)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-0ichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
0006
0006
Date Sampled: 04/26120111215
Date Received: 04/2812011 1003
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch:
Prep Batch:
680-202174
NIA
Result (ug/L)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
93
102
102
Page 27 of 61
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSA
a122.d
5 ml
5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Qualifier Acceptance Limits
70-130
70 -130
70 -130
Client: AECOM, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
SYS-EFF
680-67821-22
Water
Result
0.0050
Analysis Batch: 680-202076
Prep Batch: 680-201928
TestAmerica Savannah
General Chemistry
Qua! Units
U mg/L
Analysis Date: 0510612011 0623
Prep Date: 0510512011 0600
Page 37 of 61
RL
0.0050
Analytical Data
Job Number: 680-67821-1
Date Sampled: 04126120111215
Date Received: 0412812011 1003
Oil
1.0
Method
335.4
DATA REPORTING QUALIFIERS
Client: AECOM, Inc. Job Number: 680-67821-1
Lab Section Qualifier Description
GC/MS VOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u Indicates the analyte was analyzed for but not detected.
TestAmerica Savannah
Page 44 of 61
Client: AECOM, Inc.
Method Blank -Batch: 680-202174
Lab Sample 10: MB 680-202174110
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05106/2011
Prep Date: 05/06/2011
Leach Date: NIA
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chiaro benzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1612
1612
Analysis Batch: 680-202174
NIA Prep Batch:
leach Batch:
Units:
NIA
ug/l
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1 0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
90
101
103
Page 45 of 61
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Quality Control Results
Method: 82608
Preparation: 50308
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Job Number: 680-67821-1
MSA
aq068.d
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
70-130
70 -130
70 -130
Quality Control Results
Client: AECOM, Inc. Job Number: 680-67821-1
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report• Batch: 680-202174
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 680-20217417
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/06/2011 1449
Prep Date: 05/06/2011 1449
Leach Date: N/A
LCSD Lab Sample ID: LCSD 680-202174/8
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/06/2011
Prep Date: 05/06/2011
Leach Date: N/A
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomelhane
1, 1-Dich!oroelhane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Melhyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrach!oroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
TestAmerica Savannah
1509
1509
Analysis Balch:
Prep Bate~:
Leach Batch:
Units:
Analysis Batch:
Prep Batch:
leach Batch:
Units:
% Rec.
LCS LCSD
95 100
108 107
93 95
71 72
89 83
103 102
94 94
83 83
77 69
102 100
85 81
102 102
104 105
107 107
109 112
99 98
81 75
114 115
94 94
109 110
82 79
125 126
110 114
93 93
98 100
89 89
100 100
79 74
95 98
102 100
105 109
96 97
88 84
93 94
LCS % Rec
Page 46
680-202174 Instrument ID: MSA
N/A lab Fite ID: aq064.d
N/A Initial WeighWo1ume: 5 ml
ug/L Final WeighWolume: 5 ml
680-202174 Instrument ID: MSA
N/A lab File ID: aq065.d
N/A Initial WeighWolume: 5 ml
ug/L Final WelghWolume: 5 ml
Limit RPD RPO Limit LCS Qual LCSD Qual
26-180 5 50
70 -130 0 30
70 -130 3 30
23 -165 1 50
54 -132 6 30
70 -130 1 30
70 -130 0 30
70 -130 0 50
56 -152 11 40
70 -130 2 30
70 -130 4 30
70 -130 0 30
70 -130 1 30
70-130 0 30
70-130 3 30
70 -130 1 30
66-131 7 30
70 -130 30
70 -130 30
42 -185 30
67 -130 4 30
49 -172 0 30
70 • 130 3 30
70 -130 30
70 -130 3 30
70 -130 30
70 -130 1 30
70 -130 6 30
70 -130 3 50
70 -130 2 30
70 -130 3 30
70 -130 2 30
67 -134 4 30
70-130 1 30
LCSO % Rec Acceptance Limits
of 61
Client: AECOM, Inc.
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
LCS % Rec
104
96
107
LCSD % Rec
103
97
108
Page 47 of 61
Quality Control Results
Job Number: 680-67821-1
Acceptance Limits
70 -130
70 -130
70 -130
Client: AECOM, Inc.
Method Blank -Batch: 680-202321
Lab Sample ID: MB 680-202321/26
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/07/2011
Prep Date: 05/07/2011
Leach Date: N/A
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-0ich!oropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichtoroethene
1,2-Dich!oropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichlciropropene
1, 1, 1-Trichtoroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1747
1747
Analysis Batch: 680-202321
N/A Prep Batch:
Leach Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
100
114
101
Page 48 of 61
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Quality Control Results
Job Number: 680-67821-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
MSP
pq147.d
5 ml
5 ml
Acceptance Limits
70 -130
70 -130
70 -130
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Quality Control Results
Client: AECOM, Inc. Job Number: 680-67821-1
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-202321
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 680-202321/23 Analysis Batch: 680-202321 Instrument ID: MSP
Client Matrix: Water Prep Batch: N/A Lab File 1D: pq143.d
Dilution: 1.0 Leach Batch: N/A Initial Weight/Volume: 5 ml
Analysis Date: 05/07/2011 1620 Units: ug/L Final WeighWolume: 5 ml
Prep Date: 05/07/2011 1620
Leach Date: N/A
LCSD Lab Sample ID: LCSD 680-202321/24 Analysis Batch: 680-202321 Instrument ID: MSP
Client Matrix: Water Prep Batch: N/A Lab File ID: pq144.d
Dilution: 1.0 Leach Batch: N/A Initial Weight/Volume: 5 ml
Analysis Date: 05/07/2011 1642 Units: ug/L Final Weight/Volume: 5 ml
Prep Date: 05/07/2011 1642
Leach Date: N/A
%Rec.
Analyte LCS LCSD Limit RPO RPO Limit LCS Qual LCSD Qual
Acetone 107 110 26 -180 2 50
Benzene 98 98 70 -130 0 30
Bromoform 121 123 70-130 30
Bromomethane 93 71 23 -165 27 50
Carbon disulfide 118 117 54 -132 1 30
Carbon tetrachloride 104 101 70 -130 3 30
Chlorobenzene 105 107 70 -130 2 30
Chlorodibromomethane 105 105 70 -130 0 50
Chloroethane 103 98 56 -152 4 40
Chloroform 111 109 70 -130 2 30
Chloromethane 107 108 70 -130 2 30
cis-1,2-Dichloroethene 110 109 70-130 2 30
cis-1,3-Dichloropropene 104 104 70-130 30
Dichlorobromomethane 103 102 70 -130 30
1, 1-Dichloroethane 108 107 70-130 1 30
1,2-Dichloroethane 97 94 70-130 3 30
1, 1-Dichloroethene 116 113 66 -131 3 30
1,2-Dichloropropane 97 97 70 -130 0 30
Ethyl benzene 106 107 70 -130 2 30
2-Hexanone 101 103 42 -185 30
Methylene Chloride 113 112 67 -130 2 30
2-Butanone (MEK) 100 99 49 -172 30
4-Methyl-2-pentanone (MIBK) 95 94 70 -130 30
Styrene 111 112 70-130 30
1, 1,2,2-Tetrachloroethane 110 109 70-130 30
Tetrachloroethene 109 110 70-130 30
Toluene 102 103 70-130 30
trans-1,2-Dichloroethene 113 111 70 -130 2 30
trans-1,3-Dichloropropene 103 101 70 -130 1 50
1, 1 , 1-T richloroethane 114 112 70 -130 1 30
1, 1,2-Trichloroethane 101 101 70 -130 0 30
T richloroethene 104 105 70 -130 1 30
Vinyl chloride 104 104 67 -134 0 30
Xytenes, Total 108 110 70-130 2 30
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
TestAmerica Savannah Page 49 of 61
Client: AECOM, Inc.
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerlca Savannah
LCS % Rec
107
114
104
LCSD % Rec
108
110
104
Page 50 of 61
Quality Control Results
Job Number: 680-67821-1
Acceptance Limits
70 -130
70 -130
70 -130
Client: AECOM, Inc.
Method Blank -Batch: 680-202352
Lab Sample ID: MB 680-202352/10
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/09/2011
Prep Date: 05/09/2011
Leach Date: N/A
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chtorodibromomethane
Chtoroethane
Chloroform
Ch1oromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-0ichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Melhyl-2-penlanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trlchloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1730
1730
Analysis Batch: 680-202352
N/A Prep Batch:
Leach Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
96
101
99
Page 51 of 61
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Quality Control Results
Job Number: 680-67821-1
Method: 82608
Preparation: 50308
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
MSA
aq078.d
5 ml
5 ml
Acceptance Limits
70 -130
70 -130
70 -130
RL
25
1.0
1.0
1 0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Quality Control Results
Client: AECOM, Inc. Job Number: 680-67821-1
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-202352
Method: 82608
Preparation: 50308
LCS Lab Sample ID: LCS 680-202352/7
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/09/2011 1603
Prep Date: 05/09/2011 1603
Leach Date: N/A
LCSD Lab Sample ID: LCSD 680-202352/8
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/09/2011
Prep Date: 05/09/2011
Leach Date: NIA
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chtoroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Oichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichtoroethene
1,2-Dich!oropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichtoroethene
trans-1,3-Dichloropropene
1 , 1 , 1-T rich!oroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
TestAmerlca Savannah
1623
1623
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
% Rec.
LCS LCSD
55 63
100 102
108 114
79 82
116 109
110 109
97 100
91 95
101 93
99 101
104 103
103 105
96 99
105 105
104 106
95 96
99 104
102 105
96 99
63 66
92 98
71 74
94 96
97 99
100 104
103 107
97 98
89 92
93 95
102 105
101 104
101 101
98 100
98 100
LCS% Rec
Page 52
680-202352 Instrument ID: MSA
N/A Lab File ID: aq074.d
N/A Initial WeighWolume: 5 ml
ug/L Final WeighWolume: 5 ml
680-202352 Instrument ID: MSA
N/A Lab File ID: aq075.d
N/A Initial WeighWolume: 5 ml
ug/L Final WeighWolume: 5 ml
Limit RPD RPO Limit LCS Qual LCSDQual
26 -180 13 50
70-130 2 30
70 -130 5 30
23 -165 4 50
54 -132 6 30
70 -130 1 30
70-130 3 30
70-130 4 50
56-152 8 40
70 -130 2 30
70 -130 1 30
70 -130 2 30
70-130 3 30
70 -130 0 30
70-130 2 30
70 -130 1 30
66-131 5 30
70 -130 3 30
70 -130 3 30
42 -185 4 30
67 -130 6 30
49 -172 4 30
70 -130 1 30
70 -130 2 30
70 -130 3 30
70 -130 3 30
70 -130 1 30
70 -130 4 30
70 -130 3 50
70 -130 2 30
70 -130 3 30
70-130 0 30
67 -134 2 30
70 -130 3 30
LCSD % Rec Acceptance Limits
of 61
Client: AECOM, Inc.
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
LCS % Rec
106
98
105
LCSD % Rec
110
102
106
Page 53 of 61
Quality Control Results
Job Number: 680-67821-1
Acceptance Limits
70 -130
70 -130
70-130
Client: AECOM, Inc.
Method Blank -Batch: 680-201930
Lab Sample ID: MB 680-201930/1-A
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/06/2011 0720
Prep Date: 05/05/2011 0638
Leach Date: N/A
Analyte
Cyanide, Amenable
Duplicate• Batch: 680-201930
Lab Sample ID:
Client Matrix:
Dilution:
Analysis Date:
Prep Date:
Leach Date:
Analyte
Cyanide, Amenable
680-67821-19
Water
1.0
05/06/2011 0720
05/05/2011 0638
N/A
TestAmerica Savannah
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
Result
680-202077
680-201930
N/A
mg/L
0.0050
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
680-202077
680-201930
N/A
mg/L
Sample ResulVQual
0.041
Page 54 of 61
Qual
u
Result
0.0425
Quality Control Results
Job Number: 680-67821-1
Method: 335.1
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Method: 335, 1
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
RPO
4
LACHAT1
N/A
50 ml
50 ml
RL
0.0050
LACHAT1
N/A
50 ml
50 ml
Limit
20
Qual
Client: AECOM, Inc.
Method Blank -Balch: 680-201928
Lab Sample ID:
Client Matrix:
Dilution:
Analysis Date:
Prep Date:
MB 680-201928/1-A
Water
1.0
05/06/2011 0616
05/05/2011 0600
Leach Date: NIA
Analyte
Cyanide, Total
Analysis Batch: 680-202076
680-201928
N/A
Prep Batch:
Leach Batch:
Units: mg/L
Result
0.0050
High Level Control Sample -Batch: 680-201928
Lab Sample ID:
Client Matrix:
Dilution:
Analysis Date:
Prep Date:
HLCS 680-201928/4-A
Water
1.0
05/06/2011 0619
05/05/2011 0600
Leach Date: NIA
Analyte
Cyanide, Total
Lab Control Sample/
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
Spike Amount
0.0751
680-202076
680-201928
N/A
mg/L
Result
0.0754
Lab Control Sample Duplicate Recovery Report -Batch: 680-201928
LCS Lab Sample ID: LCS 680-201928/2-A Analysis Batch: 680-202076
Client Matrix: Water Prep Batch: 680-201928
Dilution: 1.0 Leach Batch: N/A
Analysis Date: 05/06/2011 0617 Units: mg/L
Prep Date: 05/05/2011 0600
Leach Date: N/A
LCSD Lab Sample ID: LCSD 680-201928/3-A Analysis Batch: 680-202076
Client Matrix: Water Prep Batch: 680-201928
Dilution: 1.0 Leach Batch: NIA
Analysis Date: 05/06/2011 0618 Units: mg/L
Prep Date: 05/05/2011 0600
·Leach Date: N/A
% Rec.
Analyte LCS LCSD Limit
Cyanide, Tota\ 103 107 90-110
TestAmerica Savannah Page 55 of 61
Quat
u
Quality Control Results
Job Number: 680-67821-1
Method: 335.4
Preparation: Distill/CN
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Method: 335.4
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
% Rec. Limit
100
Method: 335.4
Preparation: Distill/CN
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
RPO RPO Limit
4 20
LACHAT1
CN0506Z.FDT
50 ml
50 ml
RL
0.0050
LACHAT1
CN0506Z.FDT
50 ml
50 ml
Qual
LACHAT1
CN0506Z.FDT
50 ml
50 ml
LACHAT1
CN0506Z.FDT
50 ml
50 ml
LCS Qual LCSDQual
Client: AECOM, Inc.
Duplicate -Batch: 680-201928
Lab Sample ID: 680-67821-19
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/06/2011 0622
Prep Date: 05/05/2011 0600
Leach Date: NIA
Analyte
Cyanide, Total
TestAmerica Savannah
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
680-202076
680-201928
N/A
mg/l
Sample ResulUQual
0.083
Page 56 of 61
Result
0.0810
Quality Control Results
Job Number: 680-67821-1
Method: 335.4
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
RPO
2
LACHAT1
CN0506Z.FDT
50 ml
50 ml
Limit
20
Qual
Client: AECOM, Inc.
Method Blank· Batch: 680-201943
Lab Sample ID:
Client Matrix:
Dilution:
Analysis Date:
MB 680-20194312
Water
1.0
05/04/2011 0952
Prep Date: N/A
Leach Date: N/A
Analyte
Total Organic Carbon
Lab Control Sample• Batch: 680-201943
Lab Sample ID: LCS 680-201943/4
Client Matrix: Water
Dilution: 1.0
Analysis Date: 05/04/2011 1116
Prep Date: NIA
Leach Date: N/A
Analyte
Total Organic Carbon
TestAmerica Savannah
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
Result
1.0
Analysis Batch:
Prep Batch:
Leach Batch:
Units:
Spike Amount
20.0
680-201943
N/A
NIA
mg/l
680-201943
NIA
NIA
mg/L
Result
18.8
Page 57 of 61
Qual
u
Quality Control Results
Method: 415.1
Preparation: N/A
Instrument ID:
Lab File 10:
Initial WeighWolume:
Final WeighWolume:
Method: 415.1
Preparation: NIA
Instrument ID:
Lab File 10:
Initial WeighWolume:
Final WeighWo!ume:
Job Number: 680-67821-1
TOC3
TOC050411.txt
25 ml
25 ml
Rl
1.0
TOC3
TOC050411 . txt
25 ml
25 ml
% Rec. Limit Qual
94 80 · 120
Test America
THE LEADER IN ENVIRONMENTAL TESTING
Cl.JENT: Ll&coM
R>YORTTOc G,i1t,,/J 4.,.,...,.J°'1
ADDRESS~ c..:,/0 ....,.c.J{_ C,;};;:,D.-. .5 l-l 3<J,(,
/I<-:t ,~r S
PHONE· Cl I~ .""7l ..<.<-= FAX:
PROH':CT NAME· ' uA> / o'!( .c.. "i •rl 1.1.0,\-PROJECT NUMBER:
k..-th l l SAMPLl-1) HY: ~J
" CUENr SAMPLE SAMPLING 3~ ,._,~ IDENTIFICATION DATE/flME ~!::
<,tnf11W-0 i;-l'-1 l-1 /i, -\\ c;S 3 ,
l.f ';a/i, -3 , SYS -~r=f /?IS l
'l S'( s ---JN F' i ·pft, -/)~v ·3 i
'"(>w-I ' ~1i, -iJ '{f' 3 I '
' !>vJ -:i I~ ).,f, -11..,, 3 I •
Pw-3 f 1, 'T:-,A' -n,-r 3 l
'
' r'\N-lj ll ,,!,-f]?o 3 \
• Pw-<{ I~ :i1 /,_ (?'-{'j 3 I
I
'
'" Rl'l,l'.\\Hl IIV; ,4 __ . 41/ ~ Pllli'd ',J,>,\ll · FIRM
R/"1.1~\l,))JIJ\":
r111,T \lAJ..11". FlRM
MllllTl(lN,\I. Rl'M.\ltKS·
11720 North Creelr. Pkwy N Suite 400. B01hcll. WA 98011-8244 , 425-420-9.~00 FAX [phone] §
11922 E. First Ave, SpokallC, WA 99206-5302 . 509-924-9_200 FAX [phone]
~5 SW Nimbus Ave.Beaverton, OR 97008-7145 503-906-9200 FAX [phone]
2000 W International Airport Rd Ste AI0, Anchorage, AK 99502-1119 907-563-9,;m FAX [phone]
CHAIN OF CUSTODY REPORT Work Order#·
!NVOICETO: )o._~ TURNAROUND REQUEST
lri Hu.'>i~ D•,-:. •
◊r&ilnic &: lnorsaoic An:tly~s
~000000 □
P.O. NUMBER: STD. Petroleum Hydrucarbon A1mly~c,
PRESERVATIVE 00000 □ I ,w
REQUESTED ANALYSES I OTHER I S~dfy:
• T""'"""'"d k<'quut• ku 1!"111 Jfml<imd "~'-' """"' 1(1,rh Cbw,:,·,.
MATRIX #OF LOCATION/ TA
(W,S.0) CONT. COMMENTS WOID
l.v 3
w 1f
w l
J
vJ L
'·
\r-' '-f
~ 4 . v,J '
w <.
.
DATE: qp.; fl RtoCEJVl'Jl HY; ~cl f,;e
t">Alt:,
·nME-J7tJO PRINT NAM(:, rlRM· flME: -= DATE· Rt.CfJVl:;I) SY: om,Q(./•Q'a /
TIMC: f'RtNTNAME:·h, f\-+h o n r.,, ri r.--41,.i,M m =:AV "llMC: 1nn::a-
.J J . 13.~ ok_,;,J uJ ·.
Login Sample Receipt Checklist
Client AECOM, Inc.
Login Number: 67821
List Number: 1
Creator: Daughtry, Beth
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COG is present.
COG is filled out in ink and legible.
COG is filled out with all pertinent information.
Is the Field Sampler's name present on COG?
There are no discrepancies between the sample IDs on the containers and
the COC.
S.imptes are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, inct. any requested
MSIMSDs
VOA sample vials d6 not have headspace or bubble is <6mm (1/4") in
diameter.
Multiphasic samples are not present.
Samples do nol require splitting or compositing.
Residual Chlorine Checked.
Answer
NIA
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
NIA
TestAmerica Savannah Page 61 of 61
Job Number: 680-67821-1
List Source: TestAmerica Savannah
Comment
AECOM
August 11, 2010
Mr. Larry Thomas
City Engineer
City of Oxford
P 0. Box 1307
Oxford, North Carolina 27565
AECOM
·8540 Colonnade Center Drive Suite 306
Raleigh, NC 27615
Subject: Industrial Users Report for August 2010
919.872.6600
919 872.7996
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 60160750
Dear Mr. Thomas,
tel
fax
On behalf of The Unimax Corporation and Avnet, Inc, AECOM North Carolina, Inc. (AECOM) is
submitting the Quarterly Industrial User Permit report for the months of May, June, and July 2010.
This report is prepared in accordance with permit requirements for the discharge of treated
groundwater at the above referenced site.
If you have any questions, please contact us at 919-872-6600.
Yours sincerely,
~~1/k~47
Gerald Hornaday, P.E.
Project Engineer
Enclosure
cc:
for Nanjun V Shelly, P.E.
Project Manager
Steve Kempf -Utilities and Industries Management Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Robert West, RPM -USEPA Superfund
File
INDUSTRIAL USER REPORTING FORM
I.U. PER.MJT NO: _ _,G""0"-"0'-'-1 _____ DISCHARGE NO: ___ ~0~0~1 _____ _
MONTHS: May, June, and July 2010 YEAR: 2010
l.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERATOR IN RESPONS[BLE CHARGE (ORC): AECOM North Carolina Inc.
LABORATORY PERFORMING ANALYSIS: Test America Inc.
PERSON(S) COLLECTING SAMPLES: Chris Brownfield (AECOM), Luke Kemp (AECOM)
and Gerald Hornaday (AECOM)
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box l 307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet pennit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet pennit monitoring requirements. D
(Noncompliant)
If the facility is noncompliant, please comment on cmTective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best of my knowledge:
Signature of Pennittee Representative
William H. Doucette, Jr., Ph.D ..
August 11, 20 l 0
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.LI. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
I.LI. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
PERSON(S) COLLECTING SAMPLES:
G001
001
May, June, and July 2q 10
2010
JFD Electronics/Channel Master NPL Site
Granville
AECOM Nor1h Carolina, Inc.
T estAmerica
Chris Brownfield (AECOM), Luke Kemp (AECOM). and Gerald Hornaday (AECOM)
PARAMETER PERMIT LIMITS UNITS SAMPLE LAB QUARTERLY MEASUREMENT
Daily Maximum TYPE METHOD DATES
5/2512010 6/25/2010 7/2812010
Daily Average Flow (MGD) 0.040 MGD Meter Field 0.019 0.022 0.021
Tetrachloroethylene fig/L Grab 8260 NS NS <1.0
1, 1•Dichloroethane µglL Grab 8260 NS NS <1.0
cis•1,2 Dichloroethene µglL Grab 8260 NS NS <LO
Chlorobenzene µg/L Grnb 8260 NS NS <1.0
Toluene fJg/L Grab 8260 NS NS <1.0
1, 1 •Dichloroethylene µgll Grab 8260 NS NS <1.0
trans•1,2 Dichloroethylene µg/L Grab 8260 NS NS <1.0
Trichloroethene pgll Grab 8260 NS NS <1.0
Vinyl Chloride µgll Grab 8260 NS NS <1.0
Cyanide (total) 0.05 mgll Grab 335.2 NS NS <0.005
pH 5.0 to 10.0 SU Grab Field 7.36 7.97 8.07
Temperature 40 'C Grab Field 19.5 20,1 21.9
Monitoring requirement only.
MGD Million Gallons per day.
µgil Micrograms per liter.
mglL Milligrams per liter.
SU Standmd Units.
'C Degrees Centigrade
< Compound was not detected above the quantitation limit.
NS Not sampled
G \Eri,'JFDCHANN\NC0202.170\City ol Oxlord\lURTa~e Al.!gllSt 2010 ,ls\Table '>\8/1012010
THE LEADER :N Eh'\IIKOt~MEt✓TAL TESTit~G
ANALYTICAL REPORT
Job Number: 680-59926-1
Job Description: Channel Master
For:
AECOM, Inc.
8540 Colonnade Center Drive
Suite 306
Raleigh, NC 27615
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
08/06/2010
Appmv&CI for rAlnase
Kathryn Sm1lh
Project Man11g,er I
6/612010 2"40 PM
The test results in this report meet NE LAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www testamericainc com
Page 1 of 16
Comments
No additional comments.
Receipt
Job Narrative
680-59926-1
AU samples were received in good condition within temperature requirements.
GC/MS VOA
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted.
Page 2 of 16
Client AECOM, Inc.
Description
Matrix Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Total
Distillation, Cyanide
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Lab Location
TAL SAV
TAL SAV
TAL SAV
TAL SAV
Job Number: 680-59926-1
Method Preparation Method
SW846 8260B
SW846 5030B
MCAWW335.4
Distill/CN
MCAVWv = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Savannah
Page 3 of 16
Client: AECOM, Inc.
Method
SW846 8260B
MCAWW 335.4
TestAmerica Savannah
METHOD /ANALYST SUMMARY
Analyst
Lanier, Carolyn
McDonald, Debbie
Page 4 of 16
Job Number: 680-59926-1
Analyst ID
CL
DAM
SAMPLE SUMMARY
Client: AECOM, Inc. Job Number: 680-59926-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-59926-1 Effluent Water 0712812010 1640 0713012010 0901
680-59926-2 Trip Blank Water 0712812010 0000 07130/2010 0901
TestAmerica Savannah
Page 5 of 16
Analytical Data
Client: AECOM, Inc. Job Number: 680-59926-1
Client Sample ID: Effluent
Lab Sample ID:
Client Matrix·
680-59926-1
Water
Method: 82608
Prepara\ion: 50308
Dilution: 1.0
Date Analyzed: 08/05/2010
Date Prepared: 08/05/2010
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chiaro methane
cis-1,2-Dichloroethene
cis-1,3-0ichloropropene
Dichtorobromomethane
1, 1-Dichloroethane
1,2-0ichloroethane
1, 1-Dichloroethene
1,2-0ichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-0lchloroethene
trans-1,3-0ichloropropene
1, 1 , 1-T richloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1849
1849
Date Sampled: 07/28/2010 1640
Date Received: 07/30/2010 0901
82608 Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-176479
Result (ug/l) Qualifier
25 u
1.0 u
1.0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
'1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
10 u
5.0 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
2.0 u
%Rec Qualifier
99
98
103
Page 6 of 16
Instrument ID:
Lab File ID:
Initial WeightNolume:
Final WeighWolume:
MSP2
p0024.d
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance limits
75 -120
75 -121
75 -120
Analytical Data
Client: AECOM, Inc. Job Number: 680-59926-1
Client Sample ID: Trip Blank
Lab Sample 10:
Client Matrix:
680-59926-2
Water
Method: 8260B
Preparation: 5030B
Dilution: 1.0
Date Analyzed: 08/05/2010
Date Prepared: 08/05/2010
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroelhene
cis-1,3-0ichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-0ichloroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-~8 (Surr)
TestAmerlca Savannah
1820
1820
Date Sampled: 07/28/2010 0000
Date Received: 07/30/2010 0901
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-176479
Result (ug/L)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
100
96
102
Page 7 of 16
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSP2
p0022 d
5 ml
5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Qualifier Acceptance Limits
75 -120
75-121
75 -120
Client: AECOM, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
Effluent
680-59926-1
Water
Result
0.0050
Analysis Batch: 680-176048
Prep Batch: 680-175914
TestAmerica Savannah
General Chemistry
Qual Units
U mg/L
Date Analyzed: 08/03/2010 0629
Date Prepared: 08/02/2010 0712
Page 8 of 16
RL
0.0050
Analytical Data
Job Number: 680-59926-1
Date Sampled: 07/28/2010 1640
Date Received: 07/30/2010 0901
Oil
1.0
Method
335.4
DATA REPORTING QUALIFIERS
Client: AECOM, Inc. Job Number: 680-59926-1
Lab Section Qualifier Description
GCIMS VOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u Indicates the analyte was analyzed for but not detected.
TestAmerica Savannah
Page 9 of 16
Quality Control Results
Client: AECOM, Inc. Job Number: 680-59926-1
Method Blank · Batch: 680-176479 Method: 8260B
Preparation: 50308
Lab Sample 10: MB 680-176479117 Analysis Batch: 680-176479 Instrument ID· MSP2
Client Matrix: Water Prep Batch: N/A Lab File ID: pq234.d
Dilution· 1.0 Units: ug/l Initial WeighWolume: 5 ml
Date Analyzed: 0810512010 1254 Final WeighWolume: 5 ml
Date Prepared: 0810512010 1254
Analyte Result Qual Rl
Acetone 25 u 25
Benzene 1.0 u 1.0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1.0 u 1.0
Chlorobenzene 1.0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1.0 u 1.0
Chloroform 1.0 u 1.0
Chiaro methane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-0ichloropropene 1.0 u 1.0
Oichlorobromomethane 1.0 u 1.0
1, 1-Dichloroethane 1.0 u 1.0
1,2-Dichloroethane 1.0 u 1.0
1, 1-Dichloroethene 1.0 u 1.0
1,2-0ichloropropane 1.0 u 1.0
Ethyl benzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2-Tetrachloroethane 1.0 u 1.0
T etrachloroethene 1.0 u 1.0
Toluene 1.0 u 1.0
trans-1,2-0ichloroethene 1.0 u 1.0
trans-1,3-0ichloropropene 1.0 u 1.0
1 , 1, 1-T richloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroelhene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 103 75 -120
Oibromofluoromethane 102 75-121
Toluene-dB (Surr) 103 75 -120
TestAmerica Savannah Page 10 of 16
Client AECOM, inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-176479
LCS Lab Sample ID: LCS 680-176479/15
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 08/05/2010 1120
Date Prepared: 08/05/2010 1120
LCSD Lab Sample ID: LCSD 680-176479/18
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 08/05/2010 2048
Date Prepared: 08/05/2010 2048
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chlorcimethane
cis• 1,2•Dichloroethene
cis• 1,3•Dichloropropene
Dichtorobromomethane
1 , 1 •0ichloroethane
1,2•Dichloroethane
1, 1 ·Dichloroethene
1,2•Dichloropropane
Ethylbenzene
2.Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2·Tetrachloroethane
T etrachloroethene
Toluene
trans• 1,2•Dichloroethene
trans• 1,3-Dichloropropene
1, 1, 1 ·Trichloroethane
1, 1,2·Trichloroelhane
Trichloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-176479
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-176479
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
97 101 17 -175
103 106 77 -119
103 90 62 · 133
111 80 12 -184
110 102 55 -131
101 85 71 -135
105 103 85 -116
96 87 75 -133
108 107 40 -165
105 104 82 -120
102 91 48 · 142
108 103 69-134
106 106 76 -126
109 106 78 -127
108 105 74 -127
98 107 66-132
115 102 62 -141
103 105 73 -124
107 103 86 -116
99 100 34 -161
102 104 70 -125
97 101 33 -157
101 108 40-151
108 104 82 -122
102 101 69-129
111 99 76 -126
102 104 81 -117
107 103 72 -131
109 106 73 -128
113 103 76 -127
99 103 75 -121
106 105 84 -115
108 97 59 -144
Page a of 16
RPO
4
2
14
33
7
17
2
10
11
5
1
3
3
8
12
2
3
2
3
7
4
12
2
4
3
9
4
1
10
Quality Control Results
Job Number: 680-59926-1
Method: 82606
Preparation: 50306
Instrument ID:
Lab File lD:
MSP2
pq228.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSP2
Lab File ID: pq236.d
5 ml
5 ml
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Qual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Dual
Client AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-176479
LCS Lab Sample ID: LCS 680-176479/15
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 08/05/2010 1120
Date Prepared'. 08/05/2010 1120
LCSD Lab Sample ID: LCSD 680-176479/18
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Xylenes, Tota!
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB {Surr)
1.0
08/05/2010 2048
08/05/2010 2048
TestAmerica Savannah
Analysis Batch: 680-176479
"Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-176479
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
105 101 84-118
RPD
4
LCS % Rec LCSD % Rec
105 102
105 103
103 106
Page 12 of 16
Quality Control Results
Job Number: 680-59926-1
Method: 8260B
Preparation: 50308
Instrument ID: MSP2
Lab File ID: pq228 d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: MSP2
Lab File ID: pq236.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
RPO Limit LCS Qual
30
Acceptance Limits
75 -120
75-121
75 -120
LCSD Qual
Client: AECOM, inc
Method Blank -Batch: 680-175914
Lab Sample 10: MB 680-175914/1-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 08/03/2010 0629
Date Prepared: 08/02/2010 0712
Analyte
Cyanide, Total
Lab Control Sample/
Analysis Batch: 680-176048
Prep Batch: 680-175914
Units: mg/L
Result
0.0050
Lab Control Sample Duplicate Recovery Report -Batch: 680-175914
LCS Lab Sample ID: LCS 680-175914/2-A
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
1.0
08/03/2010 0629
08/02/2010 0712
LCSD Lab Sample ID: LCSD 680-175914/3-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 08/03/2010 0629
Date Prepared:
Analyte
Cyanide, Total
08/02/2010 0712
TestAmerlca Savannah
Analysis Batch: 680-176048
Prep Batch: 680-175914
Units: mg/L
Analysis Batch: 680-176048
Prep Batch: 680-175914
Units: mg/L ·
LCS
101
%Rec.
LCSD Limit
110 90-110
Page 13 of 16
Qual
u
RPO
8
Quality Control Results
Job Number: 680-59926-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: LATCHAT
Lab File 10: N/A
Initial WeightNolume: 50 ml
Final WeighWolume: 50 ml
RL
0.0050
Method: 335.4
Preparation: Distill/CN
Instrument 10: LA TC HAT
Lab File ID: N/A
Initial WeighWolume:
Final WeighWolume:
50 ml
50 ml
Instrument ID: LA TCHAT
Lab File ID: NIA
Initial WeightNotume:
Final WeightNolume:
50 ml
50 ml
RPO Limit LCS Qual LCSD Qual
20
Client: AECOM, Inc.
Matrix Spike/
Matrix Spike Duplicate Recovery Report • Batch: 680-175914
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
MSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Cyanide, Total
TestAmerica Savannah
680-59926-1
Water
1.0
0810312010 0629
0810212010 0712
680-59926-1
Water
1.0
08/03/2010 0629
08102/2010 0712
Analysis Batch: 680-176048
Prep Batch: 680-175914
Analysis Batch: 680-176048
Prep Batch: 680-175914
MS
102
% Rec.
MSD Limit
94 90 -110
Page 14 of 16
RPD
7
Quality Control Results
Job Number: 680-59926-1
Method: 335.4
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
LATCHAT
NIA
Initial WeighWolume:
Final WeighWolume:
50 ml
50 ml
Instrument ID: LATCHAT
Lab File ID: NIA
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPO Limit MS Qual
20
MSD Qual
Serial Number O 3 2 6 3 9
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ¢ TestAmerlca Savannah Website: .www'.testamericainc.con1
Test America
5102 La Roche Avenue Phone: [phone]
Savannah, GA 31404 Fax_: [phone]
0 Alternate Laboratory Name/Location
Phone:
THE LEADER IN ENVIRONMENT AL TESTING
Fax:
P~ECT REFERENCE /J J . f) PROJECT NO. PROJECT L~)TION · MATRIX REQUIRED ANALYSIS
PAGE @I -OF I
-. ·11 .... -• bOI l (j7';;0 (STATE) ,\ /' _ TYPE
I -
TAL (LAB) PROJECT MANAGER P.O. NUMBER CONTRACT NO. ~ I
STANDARD REPORT
/( < . t,..P ~ ~: DELIVERY <;17
""'
,NT~PM ./ ~ENT PHONE CLIENT FAX ~ z ~-~ "' DATE DUE
,_ --,t,., 11) .;;31· )Ii../? ,?1f-3'?,;1.-n,1 ~ ::; -~ "-J .
. 5l
l
'B ~3 EXPEDITED REPORT
CLIENT NAME CLIENT E-MAIL ·~ _j 'O<=:j C)
/t ft: .. ,J/Y/ t' '·,II,(!--• ,J, Al ~t.!,,. f Q
DELIVERY
!'-0 0 ~f
(SURCHARGE)
C~AOOAE~ (J,_ ,&,,~ ' DC '6: g 8 1-----DATE DUE
, ::S-"l-6 . Ade. ,:., · . , SQ_ Jot, D. IL :. l . /..X.. ~ "' ~ ~ " i -~ IJ~JlRE~ El IV, ,TiVE, NUMBER OF COOLERS SUBMITTED
COMPANY CONTRACTING THIS WORK (rr applicable) ::,i_? & I .S "' ~ lJl PER SHIPMENT: (
~ ~ DC 0
"' SAMPLE
0 ! :, => ::, DC
lQ DATE TIME
SAMPLE IDENTIFICATION 8 Sl g< NUMBER OF CONTAINERS SUBMITTED REMARKS
.
p,/,9$/2 o /6:'l-6 9VJ/. --r--~ 1;:: =, vtA: I ,El>Df PDF. . I,
' I
I
0
,_.
"
' .
'
RELINQUISHED BY: (SlGNATURE) DATE TIME RaJNQUISHE~~ DATE TIME RELINQUISHED BY: (SlGW,nJRE) DATE TIME
i/-:n • 11 .I •~ "1--rJ ?/2.tJ/;o /,{, :s 0
RECEIVED BY: lSIGNATURE) J }? TIME RECEIVED BY: (Sl<lNATUREJ ( u;&,TE ' TIME RECEIVED BY: <S!GNATUAE) DATE TIME
/!~ A_/J./ __ •A ,(, -?,/2 C jJ,,).o , I
I LABORATORY USE ONLY .
RECEIVED FOR L.ABOAATOAY BY: n7~1io TIME CUSTODY INTACT CUSTODY SAVANNAt L4.BORATORY REMARKS Tcn,p
(SIGNATURE) YES 0 SEAL NO. LOGNO. ~~\)-
11~.+h n. I)(\( 1r:h111, r, C\ If'; I NO 0 5C\C\cl '" ,n C)
.I I
TAL8240-680 {1207)
Login Sample Receipt Check List
Client: AECOM, Inc.
Login Number: 59926
Creator: Daughtry, Beth
List Number: 1
Question
Radioactivity either was not measured or, if measured, is at or below
background
The cooler's custody seal, if present, is intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperati.ire is recorded.
COC is present.
COG is filled out in ink and legible.
COG is filled out with an pertinent infonnation.
Is the Field Sampler's name present on COC?
There are no discrepancies between the sample IDs on the containers and
the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified
There is sufficient vol. for all requested analyses,incl. any requested
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
needs
Multiphasic samples are not present.
Samples do not require splitting or compositing.
TestAmcrica Savannah
T /F/ NA
N/A
True
True
True
True
True
True
True
True
False
False
True
True
True
True
True
True
True
True
True
True
N/A
N/A
Page 16 of 16
Job Number: 680-59926-1
List Source: TestAmerlca Savannah
Comment
Rec'd Trip Blk -not listed on COC
£COM
May 11, 2010
AECOM
8540 Colonnade Center Drive, Suite 306
Raleigh, NC 27615
'
919.872.6600
919.872.7996
tel
fax
Mr. Larry Thomas
City Engineer
City of Oxford
P.O. Box 1307 SUPERFUND SECTION _______ ..:...;...:.;.:,J
Oxford, North Carolina 27565
Subject: Industrial Users Report for May 2010
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 1 0140-029
Dear Mr. Thomas,
On behalf of The Unimax Corporation and Avnet, Inc., AECOM North Carolina, Inc. (AECOM) is
submitting the Quarterly Industrial User Permit report for the months of February, March, and April
201 0. This report is prepared in accordance with permit requirements for the discharge of treated
groundwater at the above referenced site.
If you have any questions, please contact us at 919-872-6600.
Yours sincerely,
(i.~~
Project Engineer
Enclosure
cc:
~0}/4;:o,~
Nanjun V. Shetty, P.E.
Project Manager
Steve Kempf. Utilities and Industries Management Corporation (w/o lab attachment)
S. Alan Lazar • Avnet, Inc. (w/o lab attachment)
Steve Earp • Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Robert West, RPM -USEPA Superfund
File
To enhance and sustain the world's built, natural and social environments
INDUSTRIAL USER REPORTING FORM
1.U. PERMIT NO: __ G=0=0~1 _____ DISCHARGE NO: ___ ....,0ce0..!.1 _____ _
MONTHS: _ _,_F-"e""b;.,ru"'a"-ry..,_.-"M"'a"'-rc""h-'-"-'. a"'n-"'d'-'AC!Jp"'r-"-il-=2""0-"1 De.__ YEAR: 201 0
1.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERA TOR IN RESPONS1BLE CHARGE (ORC): --~A~E=C"-'O""'M'-'-'-'N"'ort'""h~C=a=r=ol=in""a~l~nc=·---
LABORA TORY PERFORMING ANALYSIS: _ __,_T-"e,,,stc.!.A.,,_m~e"'-r"'ic,,_a...,l"-'nc"-'.---------
PERSON(S) COLLECTING SAMPLES: ___ _;C:e:h.!!.r""is...eB,,_,ro"-'w,.,.n"'fi""el""d.'-'('-'A"'-EC"'-O"'-'-"M,._) ____ _
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet permit monitoring requirements. 0
(Noncompliant)
lf the facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best of my knowledge:
Signature of Pennittee Representative
William H. Doucette, Jr., Ph.D ..
5/13/10
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.U. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
I.U. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
G001
001
February, March, and April 2010
2010
JFD Electronics/Channel Master NPL Site
Granville
AECOM North Carolina, Inc.
TestAmerica
PERSON($) COLLECTING SAMPLES: Chris Brownfield (AECOM), Gerald Hornaday (AECOM), and Jeff Leaver (Environmental Field Management)
PARAMETER PERMIT LIMITS UNITS SAMPLE LAB QUARTERLY MEASUREMENT
Daily Maximum TYPE METHOD DATES
2122/2010 3123/2010 4/2012010
Daily Average Flow (MGO) 0.040 MGD Meter Field 0 019 0.022 0.021
Tetrachloroethylene µg/L Grab 8260 NS NS <1.0
1, 1-Dichloroethane µg/l Grab 8260 NS NS <1.0
cis-1,2 Dichloroethene µg/l Grab 8260 NS NS <1.0
Chlorobenzene µg/L Grab 8260 NS NS <1.0
Toluene µg/L Grab 8260 NS NS <1.0
1, 1-0ichloroethylene µg/L Grab 8260 NS NS <1 0
trans-1,2 Oichloroethylene µg/L Grab 8260 NS NS <1.0
Trichloroelhene µg/L Grab 8260 NS NS <1.0
Vinyl Chloride µg/L Grab 8260 NS NS <1.0
Cyanide (total) 0.05 mglL Grab 335.2 NS NS 0.0057
pH 5.0 lo 10.0 SU Grab Field 8.31 8.43 8.07
Temperature 40 oc Grab Field 11.8 16.0 17.0
Monitoring requirement only.
MGD Million Gallons per day
µg/L Micrograms per liter
mg/L Milligrams per liter.
SU Standard Units oc Degrees Centigrade.
< Compound was not detected above the quantitation limit
NS Not sampled
G·\Env\JFDCHANNINC0202.170\Cily of Oxford\lURTable Feb 2010 xls\Table 1\5/1012{)10
Test America
THE LEADER IN EN.VlRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-56925-1
Job Description: Channel Master
For:
AECOM, Inc.
8540 Colonnade Center Drive
Suite 306
Raleigh, NC 27615
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
05/07/2010
Appro\19d lo, r&leas&
Katnryn Sm,th
Project Manager I
517/2010 4:04 PM
The test results in this report meet NE LAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel (912) 354•7858 Fax [phone] www tsstaroericainc com
Page 1 of 60
Comments
No additional comments.
Receipt
Job Narrative
680-56925-1
All samples were received in good condition within temperature requirements.
GC/MS VOA
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted.
Page 2 of 60
Client: AECOM, Inc.
Description
Matrix Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Amenable
Distillation, Cyanide
Cyanide, Total
Distillation, Cyanide
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Job Number: 680-56925-1
Lab Location Method Preparation Method
TAL SAV SW846 82608
TAL SAV SW846 50308
TAL SAV MCAWW335.1
TAL SAV Distill/CN
TAL SAV MCAWW335.4
TAL SAV Oisti!I/CN
MCAWvV = "Methods For Chem.ica\ Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Savannah
Page 3 of 60
METHOD /ANALYST SUMMARY
Client: AECOM, Inc. Job Number 680-56925-1
Method Analyst Analyst ID
SW846 8260B Bearden, Robert RB
SW846 8260B Cowart, Judson WJC
SW846 8260B Lanier, Carolyn CL
MCAWW 335.1 McDonald, Debbie DAM
MCAWW 335.4 McDonald, Debbie DAM
TestAmerica Savannah
Page 4 of 60
SAMPLE SUMMARY
Client: AECOM, Inc. Job Number: 680-56925-1
DatefTime Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-56925-1 EB EB-01 Water 04/19/2010 1025 04/21/2010 0917
680-56925-2FB FB-01 Water 04/19/2010 1045 04/21/2010 0917
680-56925-3 CMMW-22A Water 04/19/2010 1230 04/21/2010 0917
680-56925-4 CMMW-26 Water 04/19/2010 1250 04/21/2010 0917
680-56925-5 CMMW-24 Water 04/19/2010 1535 04/21/2010 0917
680-56925-6 CMMW-15 Water 04/19/2010 1650 04/21/2010 0917
680-56925-7 CMMW-20 Water 04/19/2010 1850 04/21/2010 0917
680-56925-8 CMMW-19 Water 04/19/2010 1930 04/21/2010 0917
680-56925-9 CMMW-21 Water 04/19/2010 2005 04/21/2010 0917
680-56925-10 CMMW-17 Water 04/20/2010 0720 04/21/2010 0917
680-56925-11 CMMW-07 Water 04/20/2010 0730 04/21/2010 0917
680-56925-12 CMMW-23 Water 04/20/2010 1025 04/21/2010 0917
680-56925-13 CMMW-04 Water 04/20/2010 1040 04/21/2010 0917
680-56925-14FD Dup01 Water 04/20/2010 0000 04/21/2010 0917
680-56925-15 CMMW-10 Water 04/20/2010 1115 04/21/2010 0917
680-56925-16 CMMW-05 Water 04/20/2010 1330 04/21/2010 0917
680-56925-17 SYS EFF Water 04/20/2010 1210 04/21/2010 0917
680-56925-18 SYS INF Water 04/20/2010 1225 04/21/2010 0917
680-56925-19 PW-1 Water 04/20/2010 1240 04/21/2010 0917
680-56925-20 PW-2 Water 04/20/2010 1255 04/21/2010 0917
680-56925-21 PW-3 Water 04/20/2010 1310 04/21/2010 0917
680-56925-22 PW-4 Water 04/20/2010 1325 04/21/2010 0917
680-56925-23 PW-5 Water 04/20/2010 1345 04/21/2010 0917
680-56925-24TB Trip Blank Water 04/20/2010 0000 04/21/2010 0917
TestAmerica Savannah .
Page 5 of 60
Analytical Data
Client: AECOM, Inc Job Number: 680-56925-1
Client Sample ID: SYS EFF
Lab Sample 10·
Client Matrix·
680-56925-17
Water
Method: 82608
Preparation: 50308
Dilution: 10
Date Analyzed· 04/22/2010 0020
Date Prepared: 04/22/2010 0020
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TcstAmerica Savannah
Date Sampled: 04/20/2010 1210
Date Received: 04/21/2010 0917
82608 Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-166350
Result (ug/l)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1 0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
93
102
93
Page 22 of 60
Instrument ID:
Lab File 10;
Initial WeighWolume:
Fina! WeighWolume:
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSA2
a352.d
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Qualifier Acceptance Limits
75 -120
75 -121
75 -120
Analytical Data
Client AECOM, Inc Job Number: 680-56925-1
Client Sample ID: Trip Blank
Lab Sample ID:
Client Matrix:
680-56925-24TB
Water
Method:
Preparation:
Dilution:
82608
5030B
1.0
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
04/26/2010 0025
04/26/2010 0025
Chiaro benzene
Ch\orodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-0ichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1 , 1,2-T richloroethane
Trichloroethene
Vinyl chloride
Xytenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8 (Surr)
TestAmerica Savannah
Date Sampled: 04/20/2010 0000
Date Received: 04/21/2010 0917
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-166756
Result (u9/l)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
97
103
96
Page 29 of 60
Instrument ID:
Lab File 10:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSA
a413.d
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1 0
1 0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1 0
1.0
1.0
2.0
Qualifier Acceptance Limits
75 -120
75 -121
75 -120
Client AECOM, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
SYS EFF
680-56925-17
Water
Result
0.0057
Analysis Batch: 680-167074
Prep Batch: 680-166926
TestAmerica Savannah
General Chemistry
Qual Units
mg/L
Date Analyzed: 04/29/2010 0721
Date Prepared: 04/28/2010 0615
Page 32 of 60
RL
0.0050
Analytical Data
Job Number 680-56925-1
Date Sampled: 04/20/2010 1210
Date Received: 04/21/2010 0917
Oil Method
1.0 335.4
Client AECOM, Inc.
Lab Section Qualifier
GC/MS VOA
u
General Chemistry
u
TestAmerica Savannah
DATA REPORTING QUALIFIERS
Job Number: 680-56925-1
Description
Indicates the analyte was analyzed for but not detected.
LCS or LCSD exceeds the control limits
Indicates the analyte was analyzed for but not detected.
Page 39 of 60
Quality Control Results
Client AECOM, Inc Job Number: 680-56925-1
Surrogate Recovery Report
8260B Volatile Organic Com11ounds {GC/MS)
•
Client Matrix: Water
BFB DBFM TOL
Lab Sample ID Client Sample ID %Rec %Rec %Rec
680-56925-1 EB-01 95 101 98
680-56925-2 FB-01 97 99 100
680-56925-3 CMMW-22A 92 100 94
680-56925-4 CMMW-26 98 105 97
680-56925-5 CMMW-24 93 99 99
680-56925-6 CMMW-15 95 99 99
680-56925-7 CMMW-20 100 96 98
680-56925-8 CMMW-19 97 103 97
680-56925-9 CMMW-21 98 98 97
680-56925-10 CMMW-17 91 102 95
680-56925-11 CMMW-07 98 97 99
680-56925-12 CMMW-23 99 95 99
680-56925-13 CMMW-04 98 101 96
680-56925-14 Dup01 98 98 97
680-56925-15 CMMW-10 100 96 99
680-56925-16 CMMW-05 99 99 97
680-56925-17 SYS EFF 93 102 93
680-56925-18 SYS INF 96 97 93
680-56925-19 PW-1 93 88 103
680-56925-20 PW-2 92 87 99
680-56925-21 PW-3 91 88 102
680-56925-22 PW-4 97 97 102
680-56925-23 PW-5 93 85 99
680-56925-24 Trip Blank 97 103 96
MB 680-166349/9 98 96 98
MB 680-166350/8 90 99 95
MB 680-166756/24 99 100 99
MB 680-166896/7 96 95 102
MB 680-167117/7 96 97 99
Surrogate Acceptance Limits
BFB = 4-Bromofluorobenzene 75-120
DBFM = Oibromofluoromethane 75-121
TOL = Toluene-d8 (Surr) 75-120
TestAmerica Savannah
Page 40 of 60
Client: AECOM, Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
LCS 680-16634916
LCS 680-16635015
LCS 680-166756121
LCS 680-166896/4
LCS 680-16711714
LCSD 680-16634917
LCSD 680-16635016
LCSD 680-166756122
LCSD 680-16689615
LCSD 680-16711715
Surrogate
BFB = 4-Bromofluorobenzene
DBFM = Oibromofluoromethane
TOL = Toluene-dB (Surr)
TestAmerica Savannah
BFB
%Rec
95
92
99
103
102
95
93
102
106
101
DBFM TOL
%Rec %Rec
96 94
94 91
101 98
95 105
95 99
95 94
94 90
95 91
94 102
97 102
Acceptance Limits
75-120
75-121
75-120
Page 41 of 60
Quality Control Results
Job Number: 680-56925-1
Quality Control Results
Client: AECOM, Inc. Job Number 680-56925-1
Method Blank -Batch: 680-166349 Method: 8260B
Preparation: 50308.
Lab Sample ID: MB 680-166349/9 Analysis Batch: 680-166349 Instrument ID: MSA
Client Matrix: Water Prep Batch: N/A Lab File 10: aq167.d
Dilution: 1 0 Units: ug/L Initial WeighVVolume: 5 ml
Date Analyzed· 04/21/2010 1652 Final WeighWolume: 5 ml
Date Prepared: 04/21/2010 1652
Analyte Result Qual Rl
Acetone 25 u 25
Benzene 1.0 u 1.0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1.0 u 1 0
Chlorobenzene 1.0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1.0 u 1 0
Chloroform 1.0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-Dichloropropene 1.0 u 1.0
Dichlorobromomethane 1.0 u 1.0
1, 1-0ichloroethane 1.0 u 1.0
1 ,2-Dichloroethane 1.0 u 1.0
1, 1-0ichloroethene 1.0 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethylbenzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2-Tetrachloroethane 1.0 u 1.0
Tetrachloroethene 1.0 u 1.0
Toluene 1.0 u 1.0
trans-1,2-Dichloroethene 1.0 u 1.0
trans-1,3-Dichloropropene 1.0 u 1.0
1, 1, 1-Trichloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroethene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate %Rec Acceptance Limits
4-Bromofluorobenzene 98 75-120
Dibromofluoromethane 96 75-121
Toluene-d8 (Surr) 98 75 -120
TestAmerica Savannah Page 42 of 60
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166349
LCS Lab Sample ID: LCS 680-166349/6
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 0412112010 1456
Date Prepared: 0412112010 1456
LCSD Lab Sample ID: LCSD 680-16634917
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/21/2010 1525
Date Prepared 0412112010 1525
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1 , 1-Dfchloroethene
1,2-0ichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-166349
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166349
Prep Batch: N/A
Units: ug/L
%Rec.
LCS LCSD Limit
159 112 17 -175
98 98 77-119
93 93 62 -133
55 63 12 -184
136 126 55 -131
85 86 71 -135
99 99 85 -116
82 82 75 -133
90 93 40 -165
98 98 82 -120
80 77 48 -142
92 94 69 -134
104 105 76 -126
100 99 78 -127
99 100 74 -127
92 94 66-132
116 100 62 -141
104 103 73 -124
104 104 86 -116
101 102 34 -161
107 104 70 -125
102 103 33 -157
92 94 40-151
101 101 82 -122
95 96 69-129
99 102 76 -126
97 98 81-117
91 94 72 -131
102 102 73-128
100 101 76 -127
91 89 75 -121
95 94 84-115
73 72 59 -144
Page 43 of 60
RPD
35
0
0
13
8
1
0
4
0
4
2
0
2
15
1
0
1
3
2
0
1
3
4
2
1
2
Quality Control Results
Job Number. 680-56925-1
Method: 82608
Preparation: 5030B
Instrument ID:
Lab File ID:
MSA
aq159.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSA
Lab Fite 10: aq161.d
5 ml
5 ml
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Qual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Qual
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166349
LCS Lab Sample ID: LCS 680-166349/6
Client Matrix: Water
Dilution· 1.0
Date Analyzed: 04/21/2010 1456
Date Prepared: 04/21/2010 1456
LCSD Lab Sample ID LCSD 680-166349/7
Client Matrix: Water
DilutiOff 1.0
Date Analyzed:
Date Prepared:
Anatyte
Xylenes, Total
Surrogate
4-Bromonuorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
04/21/2010 1525
04/21/2010 1525
TestAmerica Savannah
Analysis Batch: 680-166349
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-166349
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
102 101 84 -118
RPO
LCS % Rec LCSD % Rec
95 95
96 95
94 94
Page 44 of 60
Quality Control Results
Job Number 680-56925-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File 10·
MSA
aq159.d
lnitial WeighWolume:
Final Weight(Volume:
Instrument ID: MSA
Lab File ID: aq161.d
5 ml
5 ml
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Qual LCSD Qual
30
Acceptance Limits
75 -120
75 -121
75 -120
Quality Control Results
Client: AECOM, Inc Job Number: 680-56925-1
Method Blank -Batch: 680-166350 Method: 82606
Preparation: 50308
Lab Sample ID: MB 680-16635018 Analysis Batch: 680-166350 Instrument ID: MSA2
Client Matrix: Water Prep Batch: N/A Lab File ID: aq168.d
Dilution: 1.0 Units: ug/L Initial WeighWolume: 5 ml
Date Analyzed: 0412112010 1707 Final WeighWolume: 5 ml
Date Prepared: 04/2112010 1707
Analyte Result Qua1 Rl
Acetone 25 u 25
Benzene 1.0 u 1.0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1.0 u 1.0
Chlorobenzene 1.0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1.0 u 1.0
Chloroform 1.0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-Dichloropropene 1.0 u 1.0
Dichlorobromomethane 1.0 u 1.0
1, 1-0ichloroethane 1.0 u 1.0
1,2-Dichloroethane 1.0 u 1.0
1, 1-Dichloroethene 1.0 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethylbenzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
· 4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2-Tetrachloroethane 1.0 u 1.0
Tetrachloroethene 1.0 u 1.0
Toluene 1.0 u 1.0
trans-1,2-Dichloroethene 1.0 u 1.0
trans-1,3-Dichloropropene 1.0 u 1.0
1, 1, 1-Trichloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroethene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 90 75 -120
Dibromofluoromethane 99 75 -121
Toluene-dB (Surr) 95 75 -120
TestAmerica Savannah Page 45 of 60
Client AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166350
LCS Lab Sample ID: LCS 680-166350/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed· 04/21/2010 1511
Date Prepared: 04/21/2010 1511
LCSD Lab Sample ID: LCSD 680-166350/6
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
1.0
04/21/2010 1540
04/21/2010 1540
Chlorodibromomethane
Ch1oroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-0ichloroethane
1,2-0ichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Melhyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-.166350
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166350
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
98 94 17 -175
101 101 77-119
89 91 62 -133
73 91 12 -184
127 126 55 -131
87 88 71 -135
95 99 85 -116
82 82 75 -133
97 105 40-165
95 97 82 -120
92 91 48 -142
91 92 69 -134
105 106 76 -126
97 98 78 -127
99 100 74 -127
92 90 66 -132
93 92 62 -141
100 103 73 -124
103 106 86 -116
99 103 34 -161
108 111 70 -125
97 103 33-157
95 97 40 -151
98 102 82 -122
95 97 69 -129
99 103 76 -126
97 98 81-117
88 89 72 -131
90 91 73-128
98 100 76 -127
92 94 75 -121
96 97 84-115
.84 85 59 -144
Page 46 of 60
RPO
5
1
2
23
1
0
4
0
8
2
2
2
0
1
2
0
3
3
4
3
5
2
4
4
1
3
3
1
0
Quality Control Results
Job Number: 680-56925-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
MSA2
aq160.d
Initial WeighWolume:
Final WeighWolume·
Instrument ID: MSA2
Lab File 10: aq162.d
Initial WeighWolume·
Final WeighWolume:
5 ml
5 ml
5 ml·
5 ml
RPO Limit LCS Qual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Qual
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166350
LCS Lab Sample ID: LCS 680-166350/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed 0412112010 1511
Date Prepared: 0412112010 1511
LCSD Lab Sample ID LCSD 680-16635016
Client Matrix: Water
Dilution
Date Analyzed:
Date Prepared
Analyte
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1.0
0412112010 1540
04/2112010 1540
TestAmerica Savannah
Analysis Batch: 680-166350
Prep Batch: N/A
Units ug/L
Analysis Batch: 680-166350
Prep Batch: N/A
Units: ug/L
% Rec
LCS LCSD Limit
97 100 84 -118
RPO
4
LCS % Rec LCSD % Rec
92 93
94 94
91 90
Page 47 of 60
Quality Control Results
Job Number 680-56925-1
Method: 8260B
Preparation: 5030B
Instrument ID
Lab File ID:
MSA2
aq160.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSA2
Lab File ID: aq162:d
Initial WeighWolume·
Final WeighWolume.
5 ml
5 ml
5 ml
5 ml
RPO Limit LCS Qual
30
Acceptance Limits
75 -120
75 -121
75-120
LCSD Qual
Quality Control Results
Client: AECOM, Inc Job Number 680-56925-1
Method Blank -Batch: 680-166756 Method: 8260B
Preparation: 5030B
Lab Sample ID: MB 680-166756/24 Analysis Batch: 680-166756 Instrument ID: MSA
Client Matrix: Water Prep Batch: N/A Lab File ID: aq206.d
Dilution· 1.0 Units: ug/l Initial WeighWolume: 5 ml
Date Analyzed: 04/26/2010 0006 Final We1ghWolume· 5 ml
Date Prepared: 04/26/2010 0006
Analyte Result Qual Rl
Acetone 25 u 25
Benzene 1.0 u 1 0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1.0 u 1.0
Chiaro benzene 1.0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1 0 u 1.0
Chloroform 1.0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-Dichloropropene 1.0 u 1 0
Dichlorobromomethane 1.0 u 1.0
1, 1-0ichloroethane 1.0 u 1.0
1,2-Dichloroethane 1.0 u 1.0
1, 1-Dichloroethene 1.0 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethyl benzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2•pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2•Tetrachloroethane 1.0 u 1.0
Tetrachloroethene 1.0 u 1.0
Toluene 1.0 u 1 0
trans• 1,2•Dichloroethene 1.0 u 1.0
trans-1,3•Dichloropropene 1.0 u 1.0
1, 1, 1. Trichloroethane 1.0 u 1.0
1, 1,2· Trichloroethane 1.0 u 1.0
Trichloroethene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4•Bromofluorobenzene 99 75 -120
Dibromofluoromethane 100 75-121
Toluene.dB (Surr) 99 75-120
TestAmerica Savannah Page 48 of 60
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report-Batch: 680-166756
LCS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 680-166756/21
Water
1.0
04/25/2010 2247
04/25/2010 2247
LCSD Lab Sample ID: LCSD 680-166756/22
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared·
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chiaro benzene
1 0
04/25/2010 2307
04/25/2010 2307
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1 ,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-penta_none· (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
T richloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-166756
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166756
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
103 95 17 -175
105 90 77 -119
108 115 62 -133
42 39 12-184
107 93 55-131
95 87 71 -135
101 101 85 -116
95 96 75 -133
85 67 40 -165
99 95 82 -120
60 55 48 -142
100 94 69 -134
113 97 76 -126
106 103 78 -127
102 95 74 -127
98 92 66-132
110 105 62-141
108 93 73 -124
109 103 86 -116
116 124 34 -161
93 80 70 -125
110 106 33-157
104 107 40-151
106 109 82 -122
111 119 69 -129
107 105 76 -126
100 90 81 -117
103 100 72 -131
110 99 73-128
107 99 76 -127
93 95 75 -121
100 95 84-115
72 64 59 -144
Page 49 of 60
RPO
7
15
7
6
14
8
0
0
24
4
8
5
15
3
7
7
5
15
5
6
15
4
2
3
7
3
11
3
11
7
2
5
11
Quality Control Results
Job Number 680-56925-1
Method: 82608
Preparation: 5030B
Instrument ID:
Lab File ID
MSA
aq202.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSA
Lab File 10: aq203.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
5 ml
5 ml
RPO Limit LCS Qual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Qual
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report• Batch: 680-166756
LCS lab Sample ID:
Client Matrix:
Dilution·
Date Analyzed
Date Prepared:
LCS 680-166756/21
Water
1.0
04/2512010 2247
0412512010 2247
LCSD Lab Sample ID: LCSD 680-166756122
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
1.0
04/2512010 2307
0412512010 2307
TestAmerica Savannah
Analysis Batch: 680-166756
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166756
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
108 103 84-118
RPD
4
LCS % Rec LCSD % Rec
99 102
101 95
98 91
Page 50 of 60
Quality Control Results
Job Number 680-56925-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
MSA
aq202.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSA
Lab File ID: aq203.d
5 ml
5 ml
Initial WeighWolume:
Final WeighWolume·
5 ml
5 ml
RPD Limit LCS Qual LCSD Qual
30
Acceptance Limits
75 -120
75-121
75 -120
Client AECOM, Inc
Method Blank -Batch: 680-166896
Lab Sample \D: MB 680-166896/7
Client Matrix·
Dilution:
Date Analyzed:
Date Prepared:
Anatyte
Acetone
Benzene
· Bromoform
Bromomethane
Carbon disulfide
Water
1.0
04/27/2010
04/27/2010
Carbon tetrachloride
Chlorobenzene
Ch1orodibromomethane
Chloroethane
Chlorciform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1 ,2-Dichloroethane
1, 1-0ichloroethene
1 ,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichforoethane
1, 1,2-Trichloroethane
T richloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1150
1150
Analysis Batch: 680-166896
Prep Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1 0
2.0
1.0
1 0
1.0
1.0
1.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
96
95
102
Page 51 of 60
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Quality Control Results
Job Number: 680-56925-1
Method: 8260B
Preparation: 50308
Instrument ID: MSP2
Lab File ID: pq176.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 • 121
75 -120
Client AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166896
LCS Lab Sample ID: LCS 680-16689614
Client Matrix· Water
Dilution: 1.0
Date Analyzed: 0412712010 1012
Date Prepared: 04/2712010 1012
LCSD Lab Sample ID: LCSD 680-16689615
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
1.0
0412712010 1042
04/27/2010 1042
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachtoroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-_Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-166896
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166896
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
80 77 17 -175
95 96 77 • 119
104 108 62 -133
149 160 12 -184
74 74 55-131
104 103 71 · 135
98 104 85-116
106 111 75 -133
75 73 40 -165
96 95 82 -120
88 87 48 -142
84 84 69-134
117 116 76-126
113 111 78 -127
90 87 74 -127
109 107 66 -132
77 77 62 -141
109 105 73 -124
105 107 86 -116
107 112 34 -161
81 79 70 • 125
92 89 33 -157
113 110 40-151
101 104 82 -122
105 108 69-129
95 99 76-126
100 100 81-117
78 79 72 -131
124 116 73 -128
102 104 76 -127
106 105 75 -121
93 96 84 -115
77 74 59 -144
Page 52 of 60
RPD
4
0
4
8
1
6
4
2
2
0
2
4
2
0
4
2
4
2
3
2
3
2
4
0
1
7
3
3
4
Quality Control Results
Job Number 680-56925-1
Method: 8260B
Preparation: 50308
Instrument ID:
Lab File ID:
MSP2
pq168.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSP2
Lab File ID: pq170.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
5 ml
5 ml
RPO Limit LCS Oual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Oual
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report-Batch: 680-166896
LCS Lab Sample ID: LCS 680-166896/4
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
LCSD Lab Sample ID
Client Matnx:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1.0
04/27/2010 1012
04/27/2010 1012
LCSD 680-166896/5
Water
1.0
04/27/2010 1042
04/27/2010 1042
TestAmerica Savannah
Analysis Batch: 680-166896
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-166896
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
102 106 84-118
RPD
4
LCS % Rec LCSD % Rec
103 106
95 94
105 102
Page 53 of 60
Quality Control Results
Job Number 680-56925-1
Method: 82608
Preparation: 50308
lnstrument ID:
Lab File ID:
MSP2
pq168.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSP2
Lab File ID: pq170.d
5 ml
5 ml
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Qual
30
Acceptance Limits
75 -120
75 -121
75 -120
LCSD Qual
Quality Control Results
Client AECOM, Inc. Job Number 680-56925-1
Method Blank -Batch: 680-167117 Method: 82608
Preparation: 50308
Lab Sample ID: MB680-167117/7 Analysis Batch: 680-167117 Instrument ID: MSP
Client Matrix: Water Prep Batch: NIA Lab File ID: pq195.d
Dilution: 1.0 Units: ug/l Initial WeighWolume: 5 ml
Date Analyzed 0412912010 1108 Final WeighWolume: 5 ml
Date Prepared: 04/29/2010 1108
Analyte Result Qual Rl
Acetone 25 u 25
Benzene 1.0 u 1.0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 20
Carbon tetrachloride 1.0 u 1 0
Chlorobenzene 1 0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1.0 u 1.0
Chloroform 1.0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-0ichloroethene 1.0 u 1.0
cis-1 :3-Dichloropropene 1.0 u 1.0
Dichlorobromomethane 1.0 u 1.0
1, 1-Dichloroethane 1.0 u 1.0
1,2-Dichloroethane 1.0 u 1.0
1 , 1-0ichloroethene 1.0 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethylbenzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2-Tetrachloroethane 1.0 u 1.0
Tetrachloroethene 1.0 u 1.0
Toluene 1.0 u 1.0
trans-1,2-Dichloroethene 1.0 u 1.0
trans-1,3-Dichloropropene 1.0 u 1.0
1, 1, 1-Trichloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroethene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xyl~nes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 96 75 -120
Dibromofluoromethane 97 75 -121
Toluene-dB (Surr) 99 75 -120
TestAmerica Savannah Page 54 of 60
Client: AECOM, Inc
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report• Batch: 680-167117
LCS Lab Sample ID:
Client Matrix·
Dilution:
Date Analyzed:
Date Prepared:
LCS 680-167117/4
Water
1.0
04/29/2010 0908
04/29/2010 0908
LCSD Lab Sample ID: LCSD 680-167117/5
Client Matrix: Water
Dilution· 1.0
Date Analyzed: 04/29/2010 0938
Date Prepared: 04/29/2010 0938
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chiaro benzene
Ch!orodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1 , 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
TestAmerica Savannah
Analysis Batch: 680-167117
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-167117
Prep Batch: N/A
Units· ug/L
% Rec.
LCS LCSD Limit
84 85 17 -175
97 98 77-119
92 90 62 -133
115 115 12 -184
89 91 55-131
101 103 71 -135
98 99 85 -116
105 102 75 -133
110 101 40 -165
99 100 82 -120
113 108 48 -142
93 93 69-134
109 106 76 -126
102 103 78 -127
94 91 74 -127
106 108 66 -132
88 90 62 -141
101 102 73 -124
104 104 86 -116
95 96 34 -161
97 93 70 -125
87 85 33 -157
97 100 40 -151
102 103 82 -122
99 102 69-129
96 100 76-126
100 97 81 -117
90 89 72 -131
112 109 73 -128
102 106 76 -127
99 101 75 -121
91 95 84 -115
95 95 59-144
Page 55 of 60
RPO
2
2
2
0
3
2
0
2
8
0
4
1
2
2
3
1
2
1
0
2
4
2
3
1
3
5
3
2
4
1
4
1
Quality Control Results
Job Number: 680-56925-1
Method: 8260B
Preparation: 50308
Instrument ID:
Lab File ID:
MSP
pq187.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSP
Lab File ID pq189.d
5 ml
5 ml
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Qual
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
50
LCSD Dual
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-167117
LCS Lab Sample 10:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCS 680-167117/4
Water
1.0
04/29/2010 0908
04/29/2010 0908
LCSD Lab Sample ID LCSD 680-167117/5
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1.0
04/29/2010 0938
04/29/2010 0938
TestAmerica Savannah
Analysis Batch: 680-167117
Prep Batch: N/A
Units· ug/L
Analysis Batch: 680-167117
Prep Batch: N/A
Units: ug/L
% Rec
LCS LCSD Limit
103 103 84 -118
RPD
LCS % Rec LCSD % Rec
102 101
95 97
99 102
Page 56 of 60
Quality Control Results
Job Number: 680-56925-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
MSP
pq187.d
Initial WeighWolume:
Final WeighWolume:
Instrument ID: MSP
Lab File ID: pq189.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
5 ml
5 ml
RPD Limit LCS Qual LCSD Qual
30
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-166925
Lab Sample ID: MB 680-166925/1-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/29/201 0 0728
Date Prepared: 04/28/2010 0615
Analyte
Cyanide, Amenable
Duplicate. Batch: 680-166925
Lab Sample ID: 680-56925-13
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/29/2010 0728
Date Prepared: 04/28/2010 0615
Analyte
Cyanide, Amenable
TestAmerica Savannah
Analysis Batch: 680-167075
Prep Batch: 680-166925
Units mg/L
Result
0.0050
Analysis Batch: 680-167075
Prep Batch: 680-166925
Units: mg/L
Sample ResulVQual
0.0050 u
Page 57 of 60
Oual
u
Result
0.0050
Quality Control Results
Job Number: 680-56925-1
Method: 335.1
Preparation: Distill/CN
Instrument 10: LATCHAT
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
Method: 335.1
Prepara'tion: Distill/CN
Instrument ID: LATCHAT
Lab File 10: N/A
RL
0.0050
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPD Limit
NC 20
Qual
u
Client: AECOM, Inc
Method Blank -Batch: 680-166926
Lab Sample ID: MB 680-16692611-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/29/2010 0721
Date Prepared: 04/2812010 0615
Analysis Batch: 680-'167074
Prep Batch: 680-166926
Units: mg/L
Analyte Result
Cyanide, Total 0.0050
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-166926
LCS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed·
Date Prepared:
LCSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
LCS 680-16692612-A
Water
1.0
04/2912010 0721
04/2812010 0615
LCSD 680-166926/3-A
Water
1.0
04/29/2010 0721
04/2812010 0615
Analysis Batch: 680-167074
Prep Batch: 680-166926
Units: mg/L
Analysis Batch: 680-167074
Prep Batch: 680-166926
Units: mg/L
% Rec.
LCS LCSD Limit
Quality Control Results
Job Number: 680-56925-1
Method: 335.4
Preparation: Oistill/CN
Instrument ID:
Lab File ID:
LATCHAT
NIA
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
Qual RL
U 0.00~
RPO
Method: 335.4
Preparation: Distill/CN
Instrument ID: LATCHAT
Lab File ID: NIA
Initial We~ghWolume:
Final WeightNolume:
50 ml
50 ml
Instrument ID
Lab File ID:
LA TC HAT
NIA
Initial WeighWolume:
Final WeighWolume:
50 ml
50 ml
RPO Limit LCS Qual LCSD Qual
Cyanide, Total 99 101 90 -110 2 20
Duplicate -Balch: 680-166926
Lab Sample ID: 680~56925-13
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/29/2010 0721
Date Prepared: 04/28/2010 0615
Analyte
Cyanide, Total
TestAmerica Savannah
Analysis Batch: 680-167074
Prep Batch: 680-166926
Units: mg/L
Sample ResulVOual
0.10
Page 58 of 60
Result
0.102
Method: 335.4
Preparation: Distill/CN
Instrument ID: LATCHAT
Lab File ID: NIA
Initial WeighWolume:
Final WeighWolume:
RPO Limit
2 20
50 ml
50 ml
Qual
..,
" IQ " "' 0
a
"'
"' 0
Chain of
Custody Record
TAL·◄124 {1007}
C/len'A
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Address J //_IJ.r-1.
<lt;tJo f' I '• (,.:.,,, !Jr',<, >.H_ 5~ Nt .
C,,y fl n --IA IN~ )z;,ct7<,I\
3.~7o:;:~r:,.rareJ ( N c)
ConlmcJ/Plin:llase Order/Ouoft9 No,
Sainple 1.0. No. and Description Date
(Conteiner.; tor eec/1 sample may be combined on one line}
r. M vVI W-0 Y t.1/:)(,\10
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r .A'\l\#\\IJ-11'1
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...
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¼~ 1...\.\ '
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'"n7~\f 1l L ·•~1
Temperature on Receipt __ _ Test America
Drinking Water? Ves □ Nol!J THE LEADER IN ENVIRONMENTAL TESTING
Project Manag~ \\e,-1'-0 ~n~~ Dar:/-, ,I Che in of Custody Number
C q) 1.16757
Telsphone Number (Area Codo}/Fax Number V lab Number ,::) q,o._ '61 l -Co(,,o i) . Page of
SIie Con/EC! Lab Contact Analysis (Attach list ,r
more space is needed}
Corn8r/Wayb17! Number E
3¥
Special Instructions/
Containers & '-; Conditions of Receipt
MalnX Preservatives F-I 1 Time l i i; ; ii ~Ii ,g " ~ ~ ~ ·S ~ ,)l ,§ ~ ~~ ' ' ~
10'{0 i ' '{_ )( "'-y:.., -~ 'I. 'I,. 1-X:
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-''J X /110 ~ ~
1315 V Ii ,/
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INS ))( 1, 'f-,
-1,,, I'' I'
Possible Hazard ldentifit:4/ion I Sample Disposal (A lee may Do assessed 1/ samples are retained
0 Non-Hazard 0 Flammable 0 Skin tmranr 0 Poisons ~ Unknown O Retum To Client r)}::j;;sposaf By Lab 0 Arch!V0 For ____ Monfhs tonger than I month)
Tum Around Trme Reqwrod OC Req1Hremen/s (SpectlyJ
D 24Hours O 48Hours O ?Days O t40ays O 2I Days
!. Relinquished By
Time
2 Relinquished By ] Time
Time
:J Relinquished By Time 3.R~
Time
Comments 0. 2."c,..
DfSTRIBUTION: WHITE. R6/umed to Clienl with Report; CANARY -Stays wi/h the Sampta; PINK -Field Copy
~COM
November 11, 2009
Mr. Larry Thomas
City Engineer
City of Oxford·
P.O. Box 1307
Oxford, North Carolina 27565
AECOM
7041 Old Wake Forest Road, Suite 103
Raleigh, NC 27616
Subject: Industrial Users Report for November 2009
919.872.6600
919.872.7996
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 10140-029
Dear Mr. Thomas,
tel
fax
On behalf of The Unimax Corporation and Avnet, Inc., AECOM North Carolina, Inc. (AECOM) is
submitting the Quarterly Industrial User Permit report for the months of August, September and
October 2009. This report is prepared in accordance with permit requirements for the discharge of
treated groundwater at the above referenced site.
If you have any questions, please contact us at 919-872-6600.
Yours sincerely,
~uedl(~
Gerald Hornaday, P.E.
Project Engineer
Enclosure
cc:
Nanjun V. Shetty, P.E.
Project Manager
Steve Kempf -Utilities and Industries Manangement Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Robert West, RPM -US EPA Superfund
File
To enhance and sustain the world's built, natural and social environments
INDUSTRIAL USER REPORTING FORM
I.U. PERMIT NO: _ _,G""0"-'0'-'-1 _____ DISCHARGE NO: ___ ...,0""0_,__1 _____ _
MONTHS: August, September and October YEAR: 2009
1.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERA TOR fN RESPONSIBLE CHARGE (ORC): AECOM North Carolina Inc.
LABORATORY PERFORMfNG ANALYSIS: _ __,_T-"'e,,_,st'"'-A.,,_m'-"e"'-r"'icsca ._,l,..,,nc"'-.---------
PERSON(S) COLLECTING SAMPLES: Joe Ladd, (AECOM), Aaron Hill (EFM, Inc.)
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet pennit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet permit monitoring requirements. D
(Noncompliant)
If the facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best of my knowledge:
Signature of Pennittee Representative
Nanjun Shetty, P.E.
i"""""'\o\cham,l...,._.,-\o6n,~g_,,.n'd]1I0-02960:llll\a0ini,tl~\821lJn1~(1n,l)\82l.,.,.,....,..,,_u\oo,?009\ul...,,,,,..2{1]9doc,
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
1.U. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
1.U. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE (_'.;HARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
PERSON(S) COLLECTING SAMPLES:
PARAMETER
Dally Average Flow (MGD)
Tetrachloroethylene
1,1-0ichloroethane
cis-1,2 Dlchloroethene
Chlorobenzene
Toluene
1, 1-Dlchloroethylene
trans-1,2 Dichloroethylene
Trlchloroethene
Vinyl Chloride
Cyanide (total)
pH
Temperature
Monitoring requirement only
MGD Million Gallons per day.
µgll Micrograms per liter.
mg/l Milligrams per liter.
SU Standard Units.
•c Degrees Centigrade.
G001
001
August. September and October
2009
JFD Electronics/Channel Master NPL Site
Granville
AECOM North Carolina, Inc
Tes\America
Joe Ladd (AECOM)
PERMIT LIMITS
Daily Maximum
O.D40
0.05
5.0to 10.0
40
UNITS
MGD
µgll
µg/L
µg/l
µg/l
µg/L
µgtl
µg/l
µgll
µgll
mg/l
SU
•c
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
< Compound was not detected above the quantitation limit.
NS Not sampled
G:1Eov'JFDCHANN\NC0202. 1 701Co1y ot O•for~\IURTable Nov 2009.,ls\Table \\11/512009
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335.2
Field
Field
QUARTERLY MEASUREMENT
DATES
8120/2009 9/14/2009 1011612009
0.018 0.019 O.D18
NS NS <:1,0
NS NS <:1,0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <:1,0
NS NS <:1,0
NS NS <1.0
NS NS <1.0
NS NS 0.0074
8.22 8.46 8.28
21.2 20.3 16.3
Test America
THE LEADER IN ENV\RONMENTAL TEST\NG
ANALYTICAL REPORT
Job Number: 680-51739-1
Job Description: JFD/Oxford
For:
AECOM, Inc.
7041 Old Wake Forest Road
Suite 103
Raleigh, NC 27616
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
10/30/2009
Approvoo 10, release
Kathryn Sm,tt,
Proiecl Man.agar I
1 0130/2009 1 :23 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www testamericainc com
Page 1 of 55
Comments
No additional comments.
Receipt
Job Narrative
680-51739-1
All samples were received in good condition within temperature requirements.
GC/MS VOA
No analytical or quality issues were noted.
General Chemistry
Method(s) 335.4: The matrix spike/ matrix spike duplicate (MS/MSD) recoveries for batch 151760 were outside control limits. The
associated laboratory control sample (LCS) recovery met acceptance criteria.
No other analytical or quality issues were noted.
VOA Prep
No analytical or quality issues were noted.
Page 2 of 55
Client: AECOM, Inc.
Description
Matrix Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Amenable
Distillation, Cyanide
Cyanide, Total
Distillation, Cyanide
TOG
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Job Number: 680-51739-1
Lab Location Method Preparation Method
TAL SAY SW846 8260B
TAL SAY SW846 5030B
TAL SAY MCAWW335.1
TAL SAY Distill/CN
TAL SAY MCAWW 335.4
TAL SAY Distill/CN
TAL SAY MCAWW415.1
MCA WW= "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Savannah
Page 3 of 55
METHOD/ ANALYST SUMMARY
Client: AECOM, Inc. Job Number: 680-51739-1
Method Analyst Analyst ID
SW846 82606 Bearden, Robert RB
MCAWW 335.1 Johnson, Brad BJ
MCAWW 335.4 Johnson, Brad BJ
MCAWW 415.1 Brazell, Connie CB
TestAmerica Savannah
Page 4 of 55
SAMPLE SUMMARY
Client: AECOM, Inc. Job Number: 680-51739-1
Date/Time Date/Time
Lab Sample ID Client Sample ID Client Matrix Sampled Received
680-51739-1 FB FBD1 Water 10/15/2009 1005 10/17/2009 1040
68D-51739-2EB EB01 Water 10/15/2009 1015 10/17/2009 1040
680-51739-3 CMMW-26 Water 10/15/2009 1105 . 10/17/2009 1040
680-51739-4 CMMW-22A Water 10/15/2009 1225 10117/2009 1040
680-51739-5 CMMW-19 Water 10/15/2009 1312 10/17/2009 1040
680-51739-6 CMMW-21 Water 10/1512009 1539 10/17/2009 1040
680-51739-7 CMMW-20 Water 10/15/2009 1658 10/17/2009 1040
680-51739-8 CMMW-24 Water 10/15/2009 1757 10/17/2009 1040
680-51739-9 CMMW-23 Water 10/16/2009 0950 10/17/2009 1040
680-51739-1 D CMMW-17 Water 10/1612009 0810 10/17/2009 1040
680-51739-11 CMMW-07 Water 10/16/2009 0820 10/17/2009 1040
680-51739-12 CMMW-15 Water 10/16/2009 1 054 10/17/2009 1040
680-51739-13 SYS EFF Water 10/16/2009 1037 10/17/2009 1040
680-51739-14 SYS INF Water 10/16/2009 1045 10/17/2009 1040
680-51739-15 CMMW-04 Water 10/16/2009 1205 10/17/2009 1040
680-51739-16 CMMW-10 Water 10/16/2009 1303 10/17/2009 1040
680-51739-17 CMMW-05 Water 10/1612009 1409 10/17/2009 1040
680-51739-18 POW-1 Water 10/16/2009 1453 10/17/2009 1040
680-51739-19 IW-1 Water 10/16/2009 1552 10/17/2009 1040
680-51739-20FD DUP-01 Water 10/16/2009 DODD 10/17/2009 1040
680-51739-21TB TRIP BLANK Water 10/16/2009 DODO 10/17/2009 1040
TestAmerica Savannah
Page 5 of 55
Analytical Data
Client: AECOM, Inc. Job Number: 680-51739-1
Client Sample ID: SYS EFF
Lab Sample ID:
Client Matrix:
680-51739-13
Water
Method: 8260B
Preparation· 5030B
Dilution: 1.0
Date Analyzed: 10/2412009
Date Prepared: 1012412009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
Tetrachloroethene
Toluene
trans-1,2-DichJoroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1318
1318
Date Sampled: 10/16/2009 1037
Date Received: 10/17/2009 1040
82608 Volatile Organic Compounds (GCIMS)
Analysis Batch: 680-151452
Result ( ug/l I
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
105
101
103
Page 18 of 55
Instrument ID
Lab File 10:
Initial Weight/Volume:
Final Weight/Volume-
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSO2
02216.d
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.D
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.,0
1.0
1.0
1.0
1.0
1.0
2.0
Qualifier Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
SYS EFF
680-51739-13
Water
Result
0.0074
Analysis Batch: 680-151157
Prep Batch: 680-150999
TestAmerica Savannah
General Chemistry
Qual Units RL
mg/L 0.0050
Date Analyzed: 10/21/2009 1421
Date Prepared: 10/20/2009 1303
Page 27 of 55
Analytical Data
Job Number: 680-51739-1
Date Sampled: 10/16/2009 1037
Date ReceiVed: 10/17/2009 1040
Oil Method
1.0 335.4
DATA REPORTING QUALIFIERS
Client: AECOM, Inc. Job Number: 680-51739-1
Lab Section Qualifier Description
GC/MS VOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u Indicates the analyte was analyzed for but not detected.
TeslAmerica Savannah
Page 34 of 55
Client: AECOM, Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample 10 Client Sample 10
680-51739-1 FB01
680-51739-2 EB01
680-51739-3 CMMW-26
680-51739-4 CMMW-22A
680-51739-5 CMMW-19
680-51739-6 CMMW-21
680-51739-7 CMMW-20
680-51739-8 CMMW-24
680-51739-9 CMMW-23
680-51739-10 CMMW-17
680-51739-11 CMMW-07
680-51739-12 CMMW-15
680-51739-13 SYS EFF
680-51739-14 SYS INF
680-51739-15 CMMW-04
680-51739-16 CMMW-10
680-51739-17 CMMW-05
680-51739-18 POW-1
680-51739-19 IW-1
680-51739-20 DUP-01
680-51739-21 TRIP BLANK
MB 680-151404/11
MB 680-151405/11
MB 680-151452/11
MB 680-151533/9
LCS 680-151404/4
LCS 680-151405/8
LCS 680-151452/8
LCS 680-151533/6
Surrogate
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-dB (Surr)
TestAmerica Savannah
BFB DBFM TOL
¾Rec ¾Rec ¾Rec
108 108 107
106 109 108
106 104 101
106 106 104
107 102 103
106 101 103
108 101 104
105 102 104
104 103 104
109 99 106
108 101 102
107 102 101
105 101 103
105 105 104
102 103 103
105 105 102
104 106 103
108 111 105
104 111 105
108 103 107
107 108 106
107 103 105
106 104 102
109 111 103
113 109 110
99 98 102
108 106 110
113 105 112
107 109 114
Acceptance Limits
75-120
75-121
75-120
Page 35 of 55
Quality Control Results
Job Number: 680-51739-1
Client: AECOM, Inc.
Surrogate Recovery Report
82608 Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
LCSD 680-151404/5
LCSD 680-151405/9
L CSD 680-151452/9
LCSD 680-151533/7
Surrogate
Client Sample ID
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-dB (Surr)
TestAmerica Savannah
BFB
%Rec
105
112
103
105
DBFM
%Rec
101
105
101
107
TOL
%Rec
110
109
103
110
Acceptance Limits
75-120
75-121
75-120
Page 36 of 55
Quality Control Results
Job Number: 680-51739-1
Client: AECOM, Inc.
Method Blank -Batch: 680-151404
Lab Sample ID: MB 680-151404/11
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/23/2009
Date Prepared: 10/23/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dich1oroethene
cis-1,3-Dichloropropene
Oichlorobromomethane
1, 1-Dichloroethane
1,2-0ichforoethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methy!-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1 , 1 , 1-T richloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1224
1224
Analysis Batch: 680-151404
Prep Batch: N/A
Units: ug/L
Result
25
1.0
. 1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
107
103
105
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 37 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - 0
Lab File ID: oq849.d
Initial WeighWolume: 5 ml
Final WeighWolume· 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75-121
75-120
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151404
LCS Lab Sample ID: lCS 680-151404/4
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/2312009 0938
Date Prepared: 10/23/2009 0938
LCSD Lab Sample ID: lCSD 680-151404/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/23/2009 1028
Date Prepared· 10/23/2009 1028
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dich1oroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (~EK)
4-Methyl-2-pentanone (M!BK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-151404
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-151404
Prep Batch: N/A
Units: ug/L
%Rec.
lCS lCSD Limit
89 98 17 -175
101 108 77 -119
94 101 62 -133
77 92 12 -184
81 83 55-131
98 105 71-135
98 104 85-116
106 113 75 -133
106 125 40 -165
96 101 82 -120
99 103 48 -142
97 103 69 -134
105 112 76 -126
103 108 78 -127
96 103 74 -127
103 110 66-132
83 87 62 -141
103 110 73 -124
103 108 86 -116
111 118 34 -161
84 87 70 -125
101 110 33 -157
110 120 40 -151
105 109 82 -122
109 115 69 -129
105 107 76 -126
103 109 81 -117
104 104 72 -131
109 116 73 -128
106 113 76 -127
104 109 75 -121
104 110 84-115
Calculations are performed before rounding to avoid round-off errors in calculated results
TestAmerica Savannah Page 38 of 55
RPD
11
8
8
18
2
6
5
6
16
5
4
6
6
5
7
6
5
7
4
6
4
9
9
3
5
2
5
1
6
6
4
6
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 50308
Instrument 10:
lab File 10:
GC/MS Volatiles - 0
oq839.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles - 0
lab File ID: oq841.d
Initial WeighWolume:
Final WeighWolume:
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 ml
5 ml
LCS Qual lCSDQual
Client AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151404
LCS Lab Sample ID:
Client Matrix·
Dilution:
Date Analyzed:
Date Prepared:
LCSO Lab Sample ID·
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
lCS 680-151404/4
Water
1.0
10/23/2009 0938
10/23/2009 0938
lCSD 680-151404/5
Water
1.0
10/23/2009 1028
10/23/2009 1028
Analysis Batch: 680-151404
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151404
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSO Limit
108 115 59 -144
104 109 84 -118
RPO
7
4
Surrogate LCS % Rec LCSD % Rec
4-Bromofluorobenzene
Oibromofluoromelhane
Toluene-dB (Surr)
99
98
102
105
101
110
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 39 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument JO·
Lab File ID:
GC/MS Volatiles - 0
oq839.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles - 0
Lab File ID: oq841.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
RPO Limit LCS Qua!
50
30
Acceptance Limits
75-120
75-121
75 -120
LCSO Qual
Client: AECOM, Inc.
Method Blank -Batch: 680-151405
Lab Sample ID: MB 680-151405/11
Client Matrix: Waler
Dilution: 1.0
Date Analyzed: 10/23/2009
Date Prepared· 10/23/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone {MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
T richloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1238
1238
Analysis Batch: 680-151405
Prep Batch: NIA
Units· ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
106
104
102
Qua1
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 40 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - 0 C2
Lab File 10: oq850.d
lrnlial WeighWo1ume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75-121
75 -120
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151405
LCS Lab Sample ID: LCS 680-151405/8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 1012312009 1042
Date Prepared: 10/2312009 1042
LCSD Lab Sample ID: LCSD 680-151405/9
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/2312009 1111
Date Prepared: 10/2312009 1111
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1 , 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dich!oroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-151405
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151405
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
107 124 17 • 175
107 106 77-119
99 101 62 • 133
101 99 12 • 184
96 91 55 • 131
107 106 71 • 135
105 107 85 • 116
98 100 75 · 133
100 92 40 • 165
105 106 82 · 120
106 96 48 · 142
103 104 69-134
113 114 76 · 126
109 111 78-127
105 103 74 • 127
109 109 66 -132
92 87 62 · 141
109 108 73 • 124
110 113 86 • 116
116 131 34 • 161
101 101 70 · 125
114 120 33-157
120 124 40-151
113 118 82 • 122
113 121 69 · 129
111 109 76 • 126
109 109 81 · 117
110 105 72 · 131
115 118 73 • 128
110 108 76 • 127
107 106 75 • 121
109 106 84-115
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 41 of 55
RPD
14
1
2
2
5
1
2
2
8
0
10
1
2
2
5
. 1
3
12
1
5
3
4
7
2
0
4
2
2
1
2
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 50308
Instrument ID:
Lab File 10:
GC/MS Volatiles - 0 C2
oq842.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles - 0 C2
Lab File ID· oq844.d
Initial WeighWolume:
Final WeighWolume:
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 ml
5 ml
LCS Qual LCSD Oual
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151405
LCS Lab Sample ID: LCS 680-151405/8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/23/2009 1042
Date Prepared:
LCSD Lab Sample ID:
Client Matrix:
Dilution-
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
10/23/2009 1042
LCSD 680-151405/9
Water
1.0
10/23/2009 1111
10/23/2009 1111
Analysis Batch: 680-151405
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151405
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
110 101 59 -144
111 115 84 -118
RPD
8
4
Surrogate LCS % Rec LCSD % Rec
4-Bromofluorobenzene
Dibromofluoromethane
Toluene•d8 (Surr)
108
106
110
112
105
109
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 42 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles - 0 C2
oq842.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
Instrument ID:
Lab File ID:
GC/MS Volatiles - 0 C2
oq844.d
Initial WeighWolume:
Final WeightNolume:
5 ml
5 ml
RPO Limit LCS Qual
50
30
Acceptance Limits
75 -120
75 -121
75 -120
LCSD Oual
Quality Control Results
Client: AECOM, Inc. Job Number: 680-51739-1
Method Blank -Batch: 680-151452 Method: 8260B
Preparation: 5030B
Lab Sample ID: MB 680-151452111 Analysis Batch: 680-151452 Instrument ID: GC/MS Volatiles -0 C2
Client Matrix: Water Prep Batch: NIA Lab File ID: oq864.d
Dilution: 1.0 Units: ug/L Initial WeighWolume: 5 ml
Date Analyzed: 10124/2009 1121 Final WeighWolume: 5 ml
Date Prepared: 10124/2009 1121
Analyte Result Qual RL
Acetone 25 u 25
Benzene 1.0 u 1.0
Bromoform 1.0 u 1.0
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1.0 u 1.0
Chlorobenzene 1.0 u 1.0
Chlorodibromomethane 1.0 u 1.0
Chloroethane 1.0 u 1.0
Chloroform 1.0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-Dichloropropene 1.0 u 1.0
Dich!orobromomethane 1.0 u 1.0
1, 1-Dichloroethane 1.0 u 1.0
1,2-Dichloroethane 1.0 u 1.0
1, 1-Dichloroethene 1.0 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethyl benzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2-Tetrach1oroethane 1.0 u 1.0
Tetrachloroethene 1.0 u 1.0
Toluene 1.0 u 1.0
trans-1,2-Dichloroethene 1.0 u 1.0
trans-1,3-Dichloropropene 1.0 u 1.0
1, 1, 1-Trichloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroethene 1.0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 109 75 • 120
Dibromofluoromethane 111 75 -121
Toluene-dB (Surr) 103 75 -120
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 43 of 55
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151452
LCS Lab Sample ID: LCS 680-151452/8
Client' Matrix: Water
Dilution· 1.0
Date Analyzed: 10/24/2009 0925
Date Prepared: 10/24/2009 0925
LCSD Lab Sample ID: LCSD 680-151452/9
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chtorobenzene
1.0
10/24/2009 0954
10/24/2009 0954
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis•1,2-Dichloroethene
cis•1,3•Dichloropropene
Dich!orobromomethane
1, 1-Dichtoroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1.1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-151452
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-151452
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
106 102 17 -175
108 102 77-119
102 94 62 -133
108 107 12 -184
98 90 55 -131
109 103 71 -135
111 102 85-116
100 95 75 -133
120 98 40 -165
106 99 82 -120
110 98 48 · 142
105 100 69 · 134
115 107 76 -126
112 104 78 • 127
103 98 74 -127
111 105 66-132
92 84 62 • 141
109 103 73 · 124
114 106 86-116
118 111 34 · 161
105 94 70 -125
112 104 33 -157
120 113 40 -151
121 108 82 -122
121 107 69 -129
115 109 76 • 126
113 103 81 -117
111 105 72 -131
117 110 73 -128
110 104 76 -127
109 103 75 -121
108 104 84-115
Calculations are performed bef~re rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 44 of 55
RPO
4
6
8
1
8
6
9
5
20
6
12
6
7
8
6
5
9
5
8
7
11
8
6
11
12
5
9
6
7
5
6
5
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles - 0 C2
oq856.d
Initial WeighWolume:
Final Weight/Volume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles - 0 C2
Lab Fi(e ID: oq858.d
Initial Weight/Volume:
Final Weight/Volume:
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 ml
5 ml
LCS Qual LCSD Oual
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151452
LCS Lab Sample ID LCS 680-151452/8
Client Matrix· Water
01lution:
Date Analyzed:
Date Prepared:
1.0
10/24/2009 0925
10/24/2009 0925
LCSD Lab Sample ID: LCSD 680-151452/9
Client Matrix: Water
Dilution:
Date Analyzed·
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
1.0
10/24/2009 0954
10/24/2009 0954
Analysis Batch: 680-151452
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151452
Prep Batch: N/A
Units: ug/L
% Rec.
lCS LCSD Limit
114 101 59 -144
115 105 84 -118
RPD
12
9
Surrogate LCS % Rec LCSD % Rec
4-Bromofiuorobenzene
Dibromofluoromethane
Toluene-dB {Surr)
113
105
112
103
101
103
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 45 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID
Lab File ID:
GC/MS Volatiles - 0 C2
oq856.d
Initial Weight/Volume:
Fina! Weight/Volume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles -0 C2
lab File ID: oq858.d
Initial Weight/Volume:
Final Weight/Volume:
5 ml
5 ml
RPO Limit lCS Qua!
50
30
Acceptance Limits
75 -120
75 -121
75 -120
lCSD Qua!
Quality Control Results
Client: AECOM, Inc. Job Number: 680-51739-1
Method Blank · Batch: 680-151533 Method: 8260B
Preparation: 5030B
Lab Sample 10: MB 680-151533/9 Analysis Batch: 680-151533 Instrument ID: GC/MS Volatiles -0 C2
Client Matrix· Water Prep Batch: NIA Lab File ID: oq898.d
Dilution: 1.0 Units: ug/L Initial WeighWolume: 5 ml
Date Analyzed: 10/26/2009 1107 Final WeighWolume: 5 ml
Date Prepared: 10126/2009 1107
Analyte Result Qual Rl
Acetone 25 u 25
Benzene 10 u 1.0
Bromoform 1.0 u 10
Bromomethane 1.0 u 1.0
Carbon disulfide 2.0 u 2.0
Carbon tetrachloride 1 0 u 1.0
Chlorobenzene 1 0 u 1.0
Chlorodibromomethane 1 0 u 1.0
Chtoroethane 1.0 u 1.0
Chloroform 1 0 u 1.0
Chloromethane 1.0 u 1.0
cis-1,2-Dichloroethene 1.0 u 1.0
cis-1,3-Dichloropropene 1.0 u 1.0
Dichlorobromomethane 1.0 u 1.0
1, 1-0ichloroethane 1.0 u 1.0
1 ,2-Dichloroethane 1.0 u 1 0
1, 1-Dichloroethene 10 u 1.0
1,2-Dichloropropane 1.0 u 1.0
Ethylbenzene 1.0 u 1.0
2-Hexanone 10 u 10
Methylene Chloride 5.0 u 5.0
2-Butanone (MEK) 10 u 10
4-Methyl-2-pentanone (MIBK) 10 u 10
Styrene 1.0 u 1.0
1, 1,2,2· Tetrachloroethane 1.0 u 1.0
T eti-achloroethene 1.0 u 1.0
Toluene 1 0 u 1.0
trans-1,2-Dichloroethene 1 0 u 1.0
trans-1,3-Dichloropropene 1.0 u 1 0
1, 1, 1-Trichloroethane 1.0 u 1.0
1, 1,2-Trichloroethane 1.0 u 1.0
Trichloroethene 1 0 u 1.0
Vinyl chloride 1.0 u 1.0
Xylenes, Total 2.0 u 2.0
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 113 75 -120
Dibromofluoromethane 109 75-121
Toluene-d8 {Surr) 110 75 -120
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 46 of 55
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151533
LCS Lab Sample ID: LCS 680-151533/6
Client Matrix: Water
Dilution: 1.0
Date AnalYzed:
Date Prepared:
10/26/2009 0911
1012612009 0911
LCSD Lab Sample ID: LCSO 680-15153317
Client Matrix: Water
Dilution
Date Analyzed:
Date Prepared·
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
1.0
10/2612009 0939
10/2612009 0939
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1 , 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Bulanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dich/oropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-151533
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151533
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
108 107 17 -175
102 102 77-119
89 91 62 -133
95 86 12 -184
103 96 55 -131
105 104 71 -135
102 99 85 -116
87 92 75 -133
89 71 40 -165
109 106 82 -120
107 98 48 -142
104 102 69 -134
109 112 76 -126
108 106 78 -127
103 102 74 -127
100 100 66 -132
93 91 62 -141
102 103 73 -124
107 105 86-116
98 102 34 -161
109 102 70-125
98 96 33 -157
108 108 40 -151
109 106 82 -122
103 102 69 -129
103 105 76 -126
114 108 81 -117
107 106 72 -131
111 115 73 -128
110 107 76 -127
101 104 75 -121
102 103 84-115
Calculations are periormed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 47 of 55
RPO
1
0
2
10
7
1
3
5
22
2
9
2
3
2
2
0
3
2
4
7
2
0
3
1
2
5
1
3
3
3
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles -0 C2
oq890.d
lnitial Weight/Volume:
Final WeighWolume:
5 ml
5 ml
Instrument ID:
Lab File ID:
GC/MS Volatiles • 0 C2
oq892.d
Initial Weight/Volume:
Final Weight/Volume:
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 ml
5 ml
LCS Oual LCSO Oual
Client: AECOM, Inc,
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-151533
LCS Lab Sample ID: LCS 680-151533/6
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared·
1.0
1 0/26/2009 0911
10/26/2009 0911
LCSD Lab Sample ID: LCSD 680-151533/7
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared
Analyte
Vinyl chloride
Xylenes, Total
1.0
10/26/2009 0939
10/26/2009 0939
Analysis Batch: 680-151533
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-151533
Prep Batch: NIA
Units: ug/l
% Rec.
LCS LCSD Limit
109 99 59 -144
108 104 84-118
RPO
9
3
Surrogate LCS % Rec LCSD % Rec
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
107
109
114
105
107
110
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 48 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 8260B
Preparation: 5030B
Instrument 10:
Lab File ID:
GC/MS Volatiles -0 C2
oq890 d
Initial WeighWolume:
Final Weighvyolume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles - 0 C2
Lab File ID: oq892.d
Initial WeightNotume:
Final WeighWolume:
5 ml
5 ml
RPO Limit LCS Qual
50
30
Acceptance Limits
75 • 120
75-121
75 -120
LCSD Qua!
Client: AECOM, Inc.
Method Blank -Batch: 680-150999
Lab Sample ID: MB 680-150999/1-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/21/2009 1406
Date Prepared: 10/20/2009 1256
Analyte
Cyanide, Amenable
Analysis Batch: 680-151146
Prep Batch: 680-1 50999
Units: mg/L
Result
0.0050
Qual
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 49 of 55
Quality Control Results
Job Number: 680-51739-1
Method: 335.1
Preparation: Distill/CN
Instrument 10:
Lab File ID:
QuickChem 8000
N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RL
0.0050
Client: AECOM, Inc.
Method Blank -Batch: 680-150999
Lab Sample 10: MB 680-150999/1-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/2112009 1421
Date Prepared: 10/2012009 1256
Analysis Batch: 680-151157
Prep Batch: 680-150999
Units: mg/L
Analyte Result
Cyanide, Total 0.0050
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-150999
LCS Lab Sample 10:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Cyanide, Total
LCS 680-150999/2-A
Water
1.0
10/21/2009 1421
10/20/2009 1256
LCSD 680-150999/3-A
Water
1.0
10121/2009 1421
10/2012009 1256
Analysis Batch: 680-151157
Prep Batch: 680-150999
Units: mg/L
Analysis Batch: 680-151157
Prep Batch: 680-150999
Units: mg/L
% Rec.
LCS LCSD Limit
102 109 90 -110
Quality Control Results
Job Number: 680-51739-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: QuickChem 8000
Lab File 10: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
Qua! RL
U 0.0050
RPO
7
Method: 335.4
Preparation: DistilllC~
Instrument ID:
Lab File ID:
QuickChem 8000
NIA
Initial WeighWolume: 50 ml
50 ml Final WeighWolume·
Instrument ID:
Lab File ID:
QuickChem 8000
NIA
Initial WeighWolume:
Final WeighWolume:
50 ml
50 ml
RPD Limit LCS Qual LCSO Qual
20
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 50 of 55
Client: AECOM, Inc.
Method Blank· Batch: 680-151834
Lab Sample ID: MB 680-151834/1
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/28/2009
Date Prepared: NIA
Anatyte
Total Organic Carbon
TOC Result 1
TOC Result 2
TOC Result 3
Lab Control Sample/
1910
Analysis Batch: 680-151834
Prep Batch: N/A
Units: mg/L
Result
1.0
1.0
1.0
1.0
Lab Control Sample Duplicate Recovery Report• Batch: 680-151834
LCS Lab Sample ID: LCS 680-151834/2
Client Matrix: Water
Dilution: 1 0
Dale Analyzed: 10/28/2009 1941
Date Prepared NIA
LCSD Lab Sample ID: LCSD 680-151834/3
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/28/2009 1954
Date Prepared: NIA
Analyte
Total Organic Carbon
TOC Result 1
TOC Result 2
TOC Result 3
Analysis Batch: 680-151834
Prep Batch: N/A
Units: mg/L
Analysis Batch: 680-151834
Prep Batch: N/A
Units: mg/L
% Rec.
LCS LCSD Limit
100 99 BO -120
100 99 BO -120
100 98 BO -120
99 98 BO -120
Quat
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results
TestAmerica Savannah Page 51 of 55
RPO
1
2
Quality Control Results
Job Number: 680-51739-1
Method: 415.1
Preparation; NIA
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 25 ml
Final WeighWolume: 25 ml
Method: 415,1
Preparation: N/A
RL
1.0
1.0
1.0
1.0
Instrument ID:
Lab File 10:
No Equipment Assigned
NIA
Initial Weight/Volume:
Fina! Weight/Volume:
25 ml
25 ml
Instrument ID: No Equipment Assigned
Lab File ID NIA
Initial Weight/Volume:
Final Weight/Volume:
RPO Limit
25
25
25
25
25 ml
25 ml
LCS Qual LCSD Qual
Client: AECOM, Inc.
Matrix Spike/
Matrix Spike Duplicate Recovery Report -Batch: 680-151834
MS Lab Sample ID: 680-51739-16
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/28/2009 2223
Date Prepared: N/A
MSD Lab Sample ID: 680-51739-16
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/28/2009 2237
Date Prepared: N/A
Analyte
Total Organic Carbon
TOC Result 1
TOC Result 2
TOG Result 3
Analysis Batch: 680-151834
Prep Batch: N/A
Analysis Batch: 680-151834
Prep Batch: N/A
% Rec.
MS MSD Limit
96 94 80 -120
96 94 BO -120
95 94 80 -120
95 93 80 -120
Calculations are performed before rounding to avoid round•off errors in calculated results.
TestAmerica Savannah Page 52 of 55
RPO
2
2
2
Quality Control Results
Job Number: 680-51739-1
Method: 415.1
Preparation: N/A
Instrument ID:
Lab File ID:
No Equipment Assigned
N/A
Initial WeighWolume·
Final WeighWolume:
25 ml
25 ml
Instrument ID·
Lab File 10:
No Equipment Assigned
N/A
Initial WeightNolume: 25 ml
Final WeighWolume· 25 ml
RPO Limit MS Qual MSD Qual
25
25
25
25
Client: AECOM, Inc.
Method Blank· Batch: 680-151989
Lab Sample ID: MB 680-15198911
Client Matrix: Water
Dilution-1.0
Date Analyzed: 1012912009
Date Prepared: NIA
Analyte
Total Organic Carbon
TOC Result 1
TOG Result 2
TOC Result 3
Lab Control Sample/
1647
Analysis Batch: 680-151989
Prep Batch: NIA
Units: mg/L
Result
1.0
1.0
1.0
1.0
Lab Control Sample Duplicate Recovery Report_-Batch: 680-151989
LCS Lab Sample ID: LCS 680-15198912
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10129/2009 1704
Date Prepared: NIA
LCSD Lab Sample ID: LCSD 680-151989/3
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/29/2009 1718
Date Prepared: NIA
Analyte
Total Organic Carbon
TOG Result 1
TOG Result 2
TOG Result 3
Analysis Batch: 680-151989
Prep Batch: N/A
Units: mg/L
Analysis Batch: 680-151989
Prep Batch: N/A
Units: mg/L
%Rec.
LCS LCSD Limit
96 96 80-120
96 97 80 • 120
95 96 80-120
96 95 80 -120
Qual
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 53 of 55
RPD
0
Quality Control Results
Job Number: 680-51739-1
Method: 415,1
Preparation: NIA
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 25 ml
Final WeighWolume· 25 ml
Method: 415,1
Preparation: N/A
RL
1.0
1.0
1.0
1.0
Instrument ID:
Lab File ID:
No Equipment Assigned
N/A
!niti.3I Weight/Volume:
Final Weight/Volume:
25 ml
25 ml
Instrument ID:
Lab File ID:
No EquiPment Assigned
N/A
Initial Weight/Volume:
Final Weight/Volume:
RPO Limit
25
25
25
25
25 ml
25 ml
LCS Qual LCSD Qual
Serial Number O 214 9 2
ANALYSIS REQUEST ANO CHAIN OF CUSTODY RECORD <}§ TestAmerlca Savannah Website: www.testamericainc.com
Test America 5102 la Roche Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
0 Alternate Laboratory Name/Location
Phone:
THE LEADER IN ENVIRONMENTAL TESTING Fax:
PROJECT~iERENCI' l PROJECT NO. PROJECT LOCATION MATRIX PAGE I I :3' ."\Pi) 0. ✓ (STATE) t-J(, lYPE REQUIRED ANALYSIS
TAL (LAB) PROJECT MANAGER P.O. NUMBER CONTRACT NO. ~ STANDARD REPORT ¢ ~ <Ii DELIVERY
CLIENT .(~j) PM _j,.,__ CLIENT PHONE CUENTFAX <3 1z" ~l a w DATE DUE r _... ~or-.,._.,. .... 9 t'\.ll-,:t.E.6oO "' "' ~ Q @ EXPEDITED REPORT CUENTNAME CLIENT E-MAIL _, ~~ C) A_h, ·-a) Q DELIVERY ;;; (SURCHARGE) <:> 9 0 s ~ CLIENT AD~lESS il'l\lG: f;;~ (1j. RJ,e.h Ne,
a:ia: 6 0 DATE DUE
170-11 nl uJ l7~10 0 w u, J CT~~ "' NUMBER OF COOLERS SUBMITTED COMPANY CONTRACTING THIS WORK (ii applicable) 1 WI~~ => ,"'·\, -~·,,,~ ,;;: .c, r::_ f '/ft. ~\i'[~r, 0 1-w' .'i"~'' 1,,,,·.;': PEA SHIPMENT: t:: (/) cc w t-;;,,qr"--'·· ~ "' => 0 ::, I ~ ,1
SAMPLE a: @ 0 SI '.:.! :::J ::i ~8 NUMBER OF CONTAINERS SUBMITTED REMARKS SAMPLE lOENTIRCATION 000
"' DATE TIME Cl « <n « z
i,h~tq LOOS (,"501 G ~ 3
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AEUNOUISHED w (SIGNATU~\J ~~E TIME RELINQUISHED BY: (SIGNATURE) DATE TIME AEUNOUlSHEO BY: (SIGNATURE) DATE TIME
\. r. , \0 ,i,,\q \100
RECEIVED BY:~'.£ DATE TIME RECEIVED SY: (SIGNATURE) DATE TJME RECEIVED BY: (SIGNATURE) DATE TIME
• LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY: DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS
(SKlN>T~ ,.jc:.1-.. \o }H \"'1 YES C) SEAL NO. LOG NO.
\o"t» NO C) i..10-) n1'I ~-s·c.
TAL824O·60O (1?07)
Serial Number Q 214 91
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ~ TestAmertca Savannah Website: www.testamericainc.com
TestAmerica 5102 laRoche Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
0 Alternate Lab9falory Name/Locatioi:i
Phone:
THE LEADER IN ENVIRONMENT AL TESTING FalC:
p~~1Eo~t,J
PROJECT NO. PROJECT LijATION MATRIX PAGE~ I :)OF (STATE) (_, TYPE REQUIRED ANALYSIS
TAL (LAS) PROJECT MANAGER P.0.NUMBER CONTRACT NO.
-~ ,1 STANDARD REPORT
l'c: DELIVERY ex,
f~E::r ~~~ 1~ L .• CLIENlHONE CUENT FAX i 'z' w 1~ DATE DUE C\\O\ i1~-<,(i60 2l g .:!, <ll
CrNAME u CLIENT E-MAIL Q, 5 \J EXPEDITED REPORT
a, J 0 OEUVERY 0 . "•.Jrl'/\ ~ Q ~ 0 (SURCHARGE) "' C, C, ~ 1--CLIENT ADDA~ij _.\t /;<trt" RJ. Q 0.J .. t,le, ~lG,ll, er er ~ 5 °"' ~ 0 DATE DUE ,o~\ C r.l .• 0 w u, J ~ -
u r"' "' ·l->,:_~J~: NUMBER OF COOLERS SUBMITTED COMPANY CONTRACTING THIS WORK (ii applicab!e) ~ m 5 ~,,y !@'.:::l E ii /t \( ', 1 i\/t:r PER SHIPMENT; 00~~ w ( ;_;.,,r ~ ·1 ,. ·,
SAMPLE ~ @ 0
SAMPLE IDENTIFICATION ~::, :::J a: z NUMBER OF CONTAINERS SUBMITTED 000 " g REMARKS
"' DATE TIME u.:"'
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1\r \o\1w\~ nou
AECEIVE°0I~E) DATE TIME RECEIVED BY: (S!GNAJURE1 DATE TIME RECEIVED BY: (SIGNATVRE) DATE TIME
LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY: DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS
{SIGNATURE)
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YES 0 SEAL NO. LOG NO.
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TAL8240-680{1207)
AECOM North Carolina, Inc.
7041 Old Wake Forest Road, Suite 103, Raleigh, NC 27616-3013
T 919.872.6600 F 919.872.7996 www.aecom.com
August4.2009
Mr. Larry Thomas
City Engineer
City of Oxford
P.O. Box 1307
Oxford, North Carolina 27565
Subject: Industrial Users Report for August 2009
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 10140-029
Dear Mr. Thomas,
AECOM
On behalf of The Unimax Corporation and Avnet, Inc., AECOM North Carolina, Inc. (AECOM) is
submitting the Quarterly Industrial User Permit report for the months of May, June and July 2009. This
report is prepared in accordance with permit requirements for the discharge of treated groundwater at
the above referenced site.
If you have any questions, please contact us at 919-872-6600.
Yours sincerely,
~d~
Project Engineer
Enclosure
cc:
~ ~~oe1
Nanjun V. Shetty, P.E.
Project Manager
Steve Kempf -Utilities and Industries Manangement Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Robert West, RPM -USEPA Superfund
File
J:\Projects\C\Channel Master\O&M Jul09_Jun10(10140-029 &
030)\8.0 Project Documents\8.20 Proj Report (Final)\8.21 Quarterly
IU Reports\Aug 2009\IUR letter Aug 2009.doc
AECOM Environment
INDUSTRIAL USER REPORTING FORM
1.U. PERMJT NO: G001 _ DISCHARGE NO: ___ ~0~0~1 _____ _
MONTHS: May, June and July YEAR: 2009
I.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERA TOR IN RESPONSIBLE CHARGE (ORC): AECOM North Carolina Inc.
LABORATORY PERFORMING ANALYSIS: _ __,_T.,,_es,,,.,t_,_A""m"'e"'ri""ca"'-'-'ln"'c"'". _______ _
PERSON(S) COLLECTING SAMPLES: -~J=o=e=La=d=d~f~A=EC~O~M~l _________ _
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet pem1it monitoring requirements. D
(Noncompliant)
If the facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best of my knowledge:
\ .. )~"1{1)~~
Signature of Pem1ittee Repn-sentative
William H. Doucette, Jr., Ph.D.
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
1.U. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
1.U. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
PERSON(S) COLLECTING SAMPLES;
PARAMETER
Dally Average Flow (MGD)
Tetrachtoroethylene
1, 1-Dlchloroethane
cis-1,2 Dlchloroethene
Chlorobenzene
Toluene
1, 1-Dichloroethylene
trans-1,2 Dichloroethylene
Trichloroethene
Vinyl Chloride
Cyanide (total)
pH
Temperature
Monitoring requirement only.
MG□ Million Gallons per day.
µg/L Micrograms per liter.
mglL Milligrams per liter.
SU Standard Umts. •c Degrees Centigrade.
G001
001
May, June and July
2009
JFD Electronics/Channel Master NPL Site
Granville
AECOM North Carolina. Inc.
TestAmerica
Joe Ladd {AECOM)
PERMIT LIMITS
Daily Maximum
0.040
0.05
5.0 to 10.0
40
UNITS
MGD
µg/L
µgll
µgll
µgll
µgll
µgll
µg/L
µg/L
µg/L
mg/L
SU
·c
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
< Compound was not detected above the quantitation limit
NS Not sampled
G \Env\JFOCHANNV.C0202. 1 70\City ol OdortlllURTable Aug 2009.xls\Table 118/4/2009
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335 2
Field
Field
QUARTERLY MEASUREMENT
DATES
512112009 6/2512009 7123/2009
0.022 0.019 0.019
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1,0
NS NS 0.0012
8.11 8.27 8.1
18.5 20.3 22.2
July 2009 Analytical Data
J:\Projects\C\Channel Master\O&M Jul09_Jun10(10140-029 &
030)\8.0 Project Documents\8.20 Proj Report (Final)\8.21 Quarterly
IU Reports\Aug 2009\IUR Letter Aug 2009.doc
AECOM Environment I AECOM
Test America
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-49307-1
Job Description: Channel Master
For:
AECOM, Inc.
7041 Old Wake Forest Road
Suite 103
Raleigh, NC 27616
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
07/31/2009
Approved 10! r,ilease
Kalhtyn Smith
PmJect Manager I
713112009 3·14 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
iestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www testamedcainc com
Page 1 of 14
Client: AECOM, Inc.
Description
Matrix: Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Total
Distillation, Cyanide
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Lab Location Method
TAL SAV
TAL SAV
TAL SAV
TAL SAV
SW846 82608
MCAWW335.4
Job Number: 680-49307-1
Preparation Method
SW846 50308
Distill/CN
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Savannah
Page 2 of 14
Client AECOM, Inc.
Method
SW846 8260B
MCAWW 335.4
T estAmerica Savannah
METHOD/ ANALYST SUMMARY
Analyst
Lanier, Carolyn
McDonald, Debbie
Page 3 of 14
Job Number: 680-49307-1
Analyst ID
CL
OM
Client: AECOM, Inc.
Lab Sample ID
680-49307-1
680-49307-2
Client Sample ID
July 09 Eff.
Trip Blank
TestAmerica Savannah
SAMPLE SUMMARY
Client Matrix
Water
Water
Page 4 of 14
Date/Time
Sampled
07/23/2009 1630
07/23/2009 0000
Job Number: 680-49307-1
Date/Time
Received
07/25/2009 0900
07/25/2009 0900
Client AECOM, Inc.
Client Sample ID: July 09 Elf.
Lab Sample ID:
Client Matrix:
680-49307-1
Water
Method: 82608
Preparation: 50308
Dilution: 1.0
Date Analyzed: 07/30/2009
Date Prepared: 07/30/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropr6pene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2 ,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bfomofluofobenzene
Oibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1922
1922
Analytical Data
Job Number: 680-49307 -1
Date Sampled: 07/23/2009 1630
Date Received: 07/25/2009 0900
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch 680-144262
Result (ug/L)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
96
100
109
Page 5 of 14
Instrument ID:
Lab File ID:
Initial WeighWolume:
Final WeighWolume:
Qualifier
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
MSA
a4839.d
5 ml
5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Qualifier Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Client Sample ID: Trip Blank
Lab Sample ID:
Client Matrix:
680-49307-2
Water
Method: 8260B
Preparation: 5030B
Dilution: 10
Date Analyzed: 07/30/2009
Date Prepared: 07/30/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-=-sromof1Uorobenz8ne
Dibromofluoromethane
T oluene-d8 (Surr)
TestAmerica Savannah
1951
1951
Analytical Data
Job Number: 680-49307-1
Date Sampled: 07/23/2009 0000
Date Received 07/25/2009 0900
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-144262
Result (ug/L)
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
1.0
2.0
%Rec
97
100
110
Page 6 of 14
Instrument ID: MSA
Lab File ID: a4841.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Qualifier RL
u 25
u 1.0
u 1.0
u 1.0
u 2.0
u 10
u 10
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 10
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 10
u 5.0
u 10
u 10
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 1.0
u 2.0
Qualifier Acceptance Limits
75 • 120
75 -121
75 -120
Client: AECOM, Inc.
Client Sample ID: July 09 Eff.
Lab Sample ID
Client Matrix:
Analyte
Cyanide, Total
680-49307-1
Water
General Chemistry
Result Qual Units
0.012 mg/L
Analysis Batch: 680-143972 Date Analyzed: 07/29/2009 0813
Prep Batch: 680-143835 Date Prepared: 07/28/2009 0805
TestAmerica Savannah Page 7 of 14
Analytical Data
Job Number: 680-49307-1
Date Sampled: 07/23/2009 1630
Date Received: 07/25/2009 0900
RL
0.0050
Dil
1.0
Method
335.4
DATA REPORTING QUALIFIERS
Client: AECOM, Inc. Job Number: 680-49307-1
Lab Section Qualifier Description
GC/MS VOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u Indicates the analyte was analyzed for but not detected.
TestAmerica Savannah
Page 8 of 14
Client: AECOM, Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
680-49307-1 July 09 Eff.
680-49307-2 Trip Blank
MB 680-144262/20
LCS 680-144262/17
LCSD 680-144262/18
Surrogate
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-dB (Surr)
TestAmerica Savannah
BFB
%Rec
96
97
101
102
101
DBFM TOL
%Rec %Rec
100 109
100 110
96 108
96 109
94 107
Acceptance Limits
75-120
75-121
75-120
Page 9 of 14
Quality Control Results
Job Number: 680-49307-1
Client: AECOM, Inc.
Method Blank -Batch: 680-144262
Lab Sample ID: MB 680-144262120
Client Matrix· Water
Dilution: 1.0
Date Analyzed: 07130/2009 1209
Date Prepared: 07/30/2009 1209
Analyte
Acetone
Benzene
Bromoform
Brom a methane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Oichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2•Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,1, 1-Trichloroethane
1 , 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4•Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
Analysis Batch: 680-144262
Prep Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
1.0
10
1.0
1.0
10
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
101
96
108
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 10 of 14
Quality Control Results
Job Number: 680-49307-1
Method: 82606
Preparation: 50306
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq935.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-144262
LCS Lab Sample ID: LCS.680-144262/17
Client Matrix: Water
Dilution: 10
Date Analyzed: · 07/30/2009 1005
Date Prepared 07/30/2009 1005
LCSD Lab Sample ID: LCSD 680-144262/18
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 07/30/2009 1035
Date Prepared: 07/30/2009 1035
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1, 2-Trichloroethane
Trichloroethene
Analysis Batch: 680-144262
Prep Batch N/A
Units: ug/L
Analysis Batch: 680-144262
Prep Batch: N/A
Units: ug/L
%Rec.
LCS LCSD Limit
75 84 17 -175
105 101 77 -119
104 107 62 -133
81 87 12 -184
80 81 55 -131
102 99 71 -135
100 100 85 -116
111 110 75 -133
90 88 40 -165
100 98 82 -120
76 78 48 -142
90 94 69 -134
116 110 76 -126
117 113 78 · 127
91 90 74 -127
104 102 66 · 132
83 86 62 · 141
104 105 73 · 124
109 108 86 · 116
98 99 34 -161
89 87 70 -125
76 87 33 · 157
103 101 40 · 151
104 103 82 • 122
95 95 69 -129
98 97 76 • 126
108 106 81 -117
90 94 72 · 131
97 95 73 • 128
102 100 76 · 127
102 103 75 · 121
106 103 84 • 115
Quality Control Results
Job Number: 680-49307-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - A
Lab File ID: aq927.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq929.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO RPO Limit LCS Qual LCSD Qual
11 50
4 30
3 30
7 50
0 30
3 30
0 30
1 30
2 50
2 30
3 50
4 30
5 30
4 30
30
2 30
3 30
0 30
1 30
2 30
3 30
14 30
2 30
0 30
1 30
2 30
3 30
5 30
2 30
2 30
1 30
3 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 11 of 14
Client: AECOM, Inc.
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report -Batch: 680-144262
LCS Lab Sample ID: LCS 680-144262/17
Client Matrix
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
07/30/2009 1005
07/30/2009 1005
LCSD Lab Sample ID: LCSD 680-144262/18
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
07/30/2009 1035
07/30/2009 1035
Analysis Batch: 680-144262
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-144262
Prep Batch: N/A
Units: ug/L
% Rec.
Quality Control Results
Job Number: 680-49307-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq927.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq929.d
Initial WeighWolume: 5 ml,
Final WeighWolume: 5 ml
Analyte LCS LCSD Limit RPO RPO Limit LCS Qual LCSD Qual
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
84
107
82
106
LCS % Rec
102
96
109
59 -144 2
84-118 0
LCSD % Rec
101
94
107
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 12 of 14
50
30
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-143835
Lab Sample ID MB 680-143835/1-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 07/29/2009 0813
Date Prepared: 07/28/2009 0805
Analyte
Cyanide, Total
Analysis Batch: 680-143972
Prep Batch: 680-143835
Units: mg/L
Result
0.0050
Lab Control Sample -Batch: 680-143835
Lab Sample ID: LCS 680-143835/2-A
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Cyanide, Total
Matrix Spike/
Water
1.0
07/29/2009 0813
07/28/2009 0805
Analysis Batch: 680-143972
Prep Batch: 680-143835
Units: mg/L
Spike Amount
0.0301
Result
0.0316
Matrix Spike Duplicate Recovery Report -Batch: 680-143835
MS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
680-49307-1
Water
1.0
07/29/2009 0813
07/28/2009 0805
MSD Lab Sample ID: 680-49307-1
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Cyanide, Total
Water
1.0
07/29/2009 0813
07/28/2009 0805
Analysis Batch: 680-143972
Prep Batch: 680-143835
Analysis Batch: 680-143972
Prep Batch: 680-143835
% Rec.
MS MSD Limit
98 94 90 -110
Qual
u
Quality Control Results
Job Number: 680-49307-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RL
0.0050
Method: 335.4
Preparation: Distill/CN
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
%Rec. Limit Qual
105 90 -110
Method: 335.4
Preparation: Distill/CN
Instrument ID:
Lab File ID:
QuickChem 8000
N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPD
3
RPD Limit
20
MS Oual MSD Qual
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 13 of 14
Serial Number O 14 4 2 6
ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD cj> TestAmerica Savannah Website: www.testamericainc.com
Test America 5102 LaAocne Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
0 Alternate Laboratory Name/Location
Phone:
THE LEADER IN ENVIRONMENTAL TESTING Fax:
PROJECTt,E[~~:: I ,., _, . PROJECT NO. PROJECT LOCATION MATRIX REQUIRED ANALYSIS PAGE l I OF ( (STATE) !JII, TYPE
TAL (LAB) Pf'E~ MANAGER PO.NUMBER CONTRACT NO. ~----;:, ["\ STANDARD REPORT ~ ;-H,. I'! • ]! DELIVERY g----
CUE?:ITE) PM LL t;iTPHONE Cl:tr ~ 'z V) ~-w"' DATE DUE r(V}/111 ,,,n· ,,..J,....,1 'if"JJ .( , 1r··, ( j ,q 'l-fJ'i ii, ;,; 6~i ',~, I l"CUElff E·MAIL ~ 8. "'.'.} EXPEDITED REPORT CUEJNAME ..i ,,. \j DELIVERY C) a, Q O"' I-. F/f AU/I n.~~~ IA J,,.,..,,.,.~.AJ-d;,('::J.r,.• < (SURCHARGE) --a: Cl 0~ ~ '" 5 <"\ CLIEN1' ADDRESS .,. ' a: I ii' ~ ' f!,.,j ) I ':; O<> "" DATE DUE l"')l'>J.l.l ,-,,,../ ; I J,._ ~ ,2/"J(p/l Ow -' • v' -,_ ' ~~ ~ "' NUMBER OF COOLERS SUBMITTED COMPANY CONTRACTING THIS WORK (iJ appf,cable) • . ~~ 11•0\"Fi ~~~:i :c:;:.~_ f ;~: r \'.\/ ;~_,.''f('j ,r1fl t: "' PER SHIPMENT:
"' => ~ "'"' L,,i '"' .~; ;;
SAMPlE ~@ § ~ ,. => ~~ NUMBER OF CONTAINERS SUBMITTED REMARKS SAMPLE IDENTIFICATION oo g -DATE TIME U< <Z
V-J<: o9 fl. 'f.r-,1,.J,, o9 ftfl 1-I)( ,z I , ,,,.l)i) t ,'IPF? 1,
... I h , I, ~ ' ... .,..,-A,,
.. -· I ' ·--·-· ---· ···----·.
0
...
.
RELINQ\JJ"'li, BY: ISZAE) . DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME
. ' ,,,? ,,,, ,./_f' 7-.?.ro'1 I 'Jero
AECEI\J rY: (OONA'ruRE) ' DATE TIME RECEIVED BY: (SIGNATURE) DATE TIME RECEIVED BY: (&GNATURE} DATE TIME
.
..
LABORATqRY USE ONLY
RECEIVED FOR LABORATORY BY: DATE TIME CUSTODY INTACT cusroofc SAVANNAH LABORATORY REMARKS
{SIGNATUAEJ Ji,,,,1<;:c.,._, 7/z,;/o<i YES C) SEAL NO?· LOG NO.
o9o;, NO C) \ e,.,.,. '{~07 '-\,.1·~ ,•.
a
TAL..8240-680 (1207)
AECOM Environment
7041 Old Wake Forest Road, Suite 103, Raleigh, NC 27616-3013
T 919.872.6600 F 919.872.7996 www.aecom.com
May 7, 2009
Mr. Larry Thomas
City Engineer
City of Oxford
P.O. Box 1307
Oxford, North Carolina 27565
RE: Industrial Users Report for May 2009
SUPERFUND SECTION
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 10140-025
Dear Mr. Thomas:
AECOM
On behalf of The Unimax Corporation and Avnet, Inc., ENSR Consulting and Engineering (NC), Inc.
(AECOM Environment) is submitting the Quarterly Industrial User Permit report for the months of
February, March, and April 2009. This report is prepared in accordance with permit requirements for the
discharge of treated groundwater at the above referenced site.
If you have any questions, please contact us at
[phone].
Sincerely,
Gfl:=t~
Project Engineer
Enclosure
William H. Doucette, Jr., Ph.D.
Senior Program Manager
cc: Steve Kempf -United and Industries Monument Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Ken Lucas, RPM -USEPA Superfund
Nanjun Shetty, P.E. -AECOM
File
AECOM Environment
INDUSTRIAL USER REPORTING FORM
l. U. PERMIT NO: _ __,,G=0.,,_01'--------DISCHARGE NO: ___ --"-00"'-1'----------
MONTHS: February, March, and April YEAR: 2009
I.U. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERA TOR IN RESPONSIBLE CHARGE (ORC): AECOM North Carolina, lnc.{formerly ENSR)
LABORATORY PERFORMING ANALYSIS: -----'T-"'e""st'-'-A_,,_m,.,.,e'-'-r""ica"'-'--'ln"'c"-. ________ _
PERSON(S) COLLECTING SAMPLES: Joe Ladd {AECOM). Aaron Hill {EFM. Inc.
CHECK BLOCK If ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. l?s:]
(Compliant)
All monthly averages and/or other limitations do not meet pennit monitoring requirements. D
(Noncompliant)
If the facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best.of my knowledge:
\,j JM. c~ -ti I -
Signature of Pennittee Representativ
William H. Doucette, Jr., Ph.D.
Date:
TABLE 1. GROUNDWATER REMEDIAT.ION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.LI. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
I.LI. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
G001
001
February, March. and April
2009
JFD Electronics/Channel Master NPL Site
Granville
AECOM North Carolina, Inc. (formerly ENSR)
TestAmerica
PERSON(S) COLLECTING SAMPLES: Joe Ladd (AECOM), Aaron Hill (Environmental Field Mgmt, Inc)
PARAMETER
Daily Average Flow (MGO)
Tetrachloroethylene
1, 1 •Dlchloroethane
cls-1,2 Dlchloroethene
Chlorobenzene
Toluene
1, 1•Dich1oroethylene
trans•1,2 Dichloroethylene
Trichloroethane
Vinyl Chloride
Cyanide (total)
pH
Temperature
Monitoring requirement only.
MGD Million Gallons per day.
µg/L Micrograms per liter.
mg/L Milligrams per liter.
SU Standard Units.
°C Degrees Centigrade.
PERMIT LIMITS
Dally Maximum
0.040
0.05
5.010 10.0
40
Compound was not detected above the quantitation limit
NS Not sampled
G:\EnvUFOCHANN\NC0202.170\C,ty of Oxlord\lURTable May 2009.1ls\Table 1\Sn/2009
UNITS
MGD
µgtl
µg/L
µgll
µg/L
µg/L
µg/L
µgll
µg/L
µg/L
mg/L
SU
•c
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335.2
Field
Field
QUARTERLY MEASUREMENT
OATES
2/1812009 3/26/2009 4/6/2009
0.020 0.019 0.019
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1,0
NS NS <1.0
NS NS <1.0
NS NS 1.1
NS NS <1.0
NS NS 0.0081
8.43 8,35 7.81
14.4 16.9 17,1
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-46224-1
Job Description: Channel Master
For:
AECOM, Inc.
7041 Old Wake Forest Road
Suite 103
Raleigh, NC 27616
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
04/20/2009
Approved !<>r release
Kathryn Sm1tt1
Project Manager I
4120/2009 4·35 PM
The test results in this report meet NE LAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; AROEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
OEQ: 30690; LA OHH: LA080008; ME: 2008022; MO: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC OWQ: 269; NC OHHS: 13701; PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA: WV DEP: 094; WV
_DHHR: 9950 C; WI ONR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www.testamericaioc com
Page 1 of 68
Client: AECOM, Inc.
Client Sample ID:
Lab Sample ID:
Client Matrix:
SYSEFF
680-46224-11
Water
Method: 8260B
Preparation: 5030B
Dilution: 1.0
Dale Analyzed: 04/15/2009
Date Prepared: 04/15/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfid~
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-0ichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroelhane
T etrachloroethene
Toluene
trans-1,2-Dich!oroethene
trans-1,3-Dich!oropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
T estAmerica Savannah
1712
1712
Analytical Data
Job Number: 680-46224-1
Date Sampled: 04/06/2009 0845
Date Received: 04/08/2009 0858
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-135248 Instrument ID: GC/MS Volatiles -0
Lab File ID: 08765.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Result (ug/L) Qualifier RL
25 u 25
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
2.0 u 2.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
10 u 10
5.0 u 5.0
10 u 10
10 u 10
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u 1.0
1.0 u l.O
1.0 u 1.0
2.0 u 2.0
%Rec Acceptance Limits
92 75 -120
107 75 -121
102 75 -120
Page 15 of 68
Client: AECOM, Inc
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
SYS EFF
680-46224-11
Water
Result
0.0081
Anly Batch: 680-135403
Prep Batch: 680-135285
TestAmerica Savannah
General Chemistry
Oual Units
mg/L
Date Analyzed 04/17/2009 0806
Date Prepared: 04/16/2009 0631
Page 32 of 68
Analytical Data
Job Number: 680-46224-1
Date Sampled: 04/06/2009 0845
Date Received: 04/08/2009 0858
RL Oil Method
0.0050 1.0 335.4
Client: AECOM, inc.
Surrogate Recovery Report
82608 Volatile Organic Compounds (GC/MS)
Client Matrix: Water
BFB DBFM TOL
Lab Sample ID Client Sample ID · %Rec %Rec %Rec
680-46224-1 CMMW-26 90 109 106
680-46224-2 CMMW-22A 91 107 106
680-46224-3 CMMW-15 90 106 99
680-46224-4 CMMW-19 95 107 104
680-46224-5 CMMW-23 96 101 104
680-46224-6 CMMW-21 96 99 · 103
680-46224-7 CMMW-04 92 104 102
680-46224-8 DUP01 92 106 102
680-46224-9 CMMW-20 92 109 106
680-46224-10 CMMW-17 94 107 103
680-46224-11 SYS EFF 92 107 102
680-46224-12 SYS INF 94 107 101
680-46224-13 PW-1 94 107 106
680-46224-14 PW-2 94 107 100
680-46224-14 DL PW-2 DL 101 99 106
680-46224-15 PW-3 97 96 103
680-46224-16 PW-4 91 106 105
680-46224-17 PW-5 94 104 105
680-46224-18 CMMW-24 90 105 100
680-46224-19 EB01 90 108 100
680-46224-20 FB01 90 106 100
680-46224-21 CMMW-07 99 80 105
680-46224-22 CMMW-10 94 83 104
680-46224-23 CMMW-05 93 92 104
680-46224-24 IW-1 89 92 100
680-46224-25 POW-1 99 83 103
680-46224-26 TRIP BLANK 88 96 100
MB 680-135129/7 92 105 102
MB 680-135172/2 91 111 105
Surrogate Acceptance Limits
BFB = 4-Bromofluorobenzene 75-120
DBFM = Oibromofluorbmethane 75-121
TOL = Toluene-dB (Surr) 75-120
TestAmerica Savannah
Page 36 of 68
Quality Control Results
Job Number: 680-46224-1
Client: AECOM, Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
MB 680-135248/9
MB 680-135330/8
MB 680-135332/16
MB 680-135495/7
MB 680-135496/7
MB 680-135497/16
LCS 680-135129/4
LCS 680-135172/7
LCS 680-135248/6
LCS 680-135330/5
LCS 680-135332/13
LCS 680-135495/4
LCS 680-135496/4
LCS 680-135497/4
LCSD 680-135129/5
LCSD 680-135172/1
LCSD 680-135248/7
LCSD 680-135330/6
LCSD 680-135332/14
LCSD 680-135495/5
LCSD 680-135496/5
LCSD 680-135497/5
Surrogate
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
T0L = Toluene-dB (Surr)
TestAmerica Savannah .
BFB
%Rec
93
92
94
95
93
91
99
100
96
103
97
97
101
100
95
102
98
96
104
104
99
102
DBFM T0L
%Rec · %Rec
106 103
94 103
96 102
109 102
106 100
112 103
96 99
99 99
103 95
96 100
92 98
100 97
104 97
106 98
97 100
101 100
101 95
94 95
88 103
104 102
102 98
106 100
Acceptance Limits
75-120
75-121
75-120
Page 37 of 68
Quality Control Results
Job Number: 680-46224-1
Client: AECOM, Inc.
Method Blank -Batch: 680-135129
Lab Sample ID: MB 680-13512917
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 0411412009
Dale Prepared: 04/14/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2:-Dichloropropane
Ethylbenzene
2-Hexanone
1112
1112
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-d8 (Surr)
Analysis Batch: 680-135129
Prep Batch: NIA
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
92
105
102
Oual.
u
u
u
u
u
u
u·
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
. T estAmerica Savannah Page 38 of.68
Quality Control Results
Job Number 680-46224-1
Method: 82608
Preparation: 50308
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq723.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc,
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135129
LCS Lab Sample ID: LCS 680-135129/4
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1,0
04/14/2009 0832
04/14/2009 0832
LCSD Lab Sample ID: LCSD 680-135129/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Water
1,0
04/14/2009 0901
04/14/2009 0901
Chlorodibromomethane
Chloroethane
Chloroform
Ch!oromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Oichlorobromomethane
1, 1-Oichloroethane
1,2-Oichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-T-richloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-135129
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135129
Prep Balch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
96 93 17-175
96 97 77-119
118 113 62 -133
170 170 12-184
81 83 55-131
95 97 71 -135
97 93 85-116
109 105 75 -133
84 85 40 -165
97 96 82 -120
96 98 48 -142
98 99 69 -134
107 108 76 -126
104 101 78 -127
96 98 74 -127
96 97 66 -132
91 91 62-141
96 96 73 -124
100 98 86-116
100 93 34 -161
96 96 70 -125
96 97 33 -157
95 97 40 -151
102 100 82 -122
99 95 69 -129
99 98 76 -126
97 99 81-117
91 92 72 -131
112 112 73 -128
94 95 76 -127
93 96 75 -121
92 95 84-115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - 0
Lab File ID: oq713,d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles -0
Lab Fite ID: oq715,d
initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
RPO RPO Limit LCS Oual LCSD Oual
3 50
30
4 30
o 50
2 30
2 30
4 30
4 30
1 50
1 30
2 50
1 30
1 30
3 30
2 30
1 30
0 30
0 30
3 30
'6 30
o 30
30
1 30
2 30
4 30
2 30
2 30
1 30
o 30
2 30
3 30
4 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 39 of 68
Client: AECOM, Inc,
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135129
LCS Lab Sample ID: LCS 680-135129/4
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared·
Water
1,Q
04/14/2009 0832
04/14/2009 0832
LCSD Lab Sample ID: LCSD 680-135129/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, To1al
Surrogate
Water
1,Q
04/14/2009 0901
04/14/2009 0901
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
Analysis Batch: 680-135129
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135129
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
94 95 59 -144
101 97 84 -118
RPD
1
3
LCS % Rec LCSD % Rec
99 95
96 97
99 100
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 40 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 82608
Preparation: 50308
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq713,d
Initial WeightNolume: · 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq715,d
Initial Weight/Volume: 5 ml
Final Weigh!Nolume: 5 ml
RPD Limit LCS Qual LCSD Qual
50
30
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-135172
Lab Sample ID: MB 680-135172/2
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009
Date Prepared: 04/14/2009
Analyle
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dich\orobromomethane
1, 1-Dichloroethane
1 ,2-0ich!oroethane
1, 1-Dichloroeth€ne
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
1126
1126
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
Analysis Balch: 680-135172
Prep Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
91
111
105
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are periormed before rounding to avoid round-off errors in calculated results.
T estAmerica Savannah Page 41 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq724 d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Accepta_nce Limits
75 -120
75-121
75 -120
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report• Batch: 680-135172
LCS Lab Sample ID: LCS 680-135172/7
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/14/2009 0846
04/14/2009 0846
LCSD Lab Sample ID: LCSD 680-135172/1
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Water
1.0
04/14/2009 0915
04/14/2009 0915
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
. Elhylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
T richloroethene
Analysis Batch: 680-135172
Prep Balch N/A
Units: ug/L
Analysis Balch: 680-135172
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
85 91 17-175
98 98 77-119
99 98 62 -133
162 170 12-184
86 88 55-131
94 96 71 -135
98 100 85-116
113 110 75, 133
110 113 40 -165
99 100 82 -120
106 108 48 -142
98 101 69 -134
109 108 76 -126
101 101 78 -127
101 100 74 -127
96 97 66 -132
93 99 62 -141
94 95 73 -124
104 105 86 -116
99 98 34-161
96 99 70 -125
94 96 33 -157
98 98 40 -151
104 107 82 -122
96 99 69 -129
104 106 76 -126
100 101 81-117
97 98 72 -131
109 108 73 -128
93 94 76 -127
94 94 75 -121
101 102 84 -115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq714.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq716.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
RPD RPD Limit LCS Qual LCSD Qual
7 50
30
1 30
5 50
2 30
2 30
2 30
3 30
2 50
1 30
2 50
4 30
1 30
0 30
30
1 30
5 30
30
30
1 30
3 30
2 30
0 30
3 30
4 30
2 30
30
30
30
30
30
30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 42 of 68
Client: AECOM. Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135172
LCS Lab Sample ID: LCS 680-13517217
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/14/2009 0846
04/14/2009 0846
LCSD Lab Sample ID: LCSD 680-135172/1
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
Water
1.0
04/14/2009 0915
04/14/2009 0915
Analysis Batch: 680-135172
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135172
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
100 103 59 -144
104 105 84 -118
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq714.d
Initial WeightNolume: 5 ml
Final WeightNolume: 5 ml
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq716.d
Initial WeightNolume: 5 ml
Final WeighWolume: 5 ml
RPD RPD Limit LCS Oual LCSD Qual
3 50
30
Surrogate LCS % Rec LCSD % Rec Acceptance Limlts
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
100
99
99
102
101
100
Calculations are performed before rounding to avoid round-off errors in calculated results.
TeslAmerica Savannah Page 43 of 68
75 -120
75-121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-135248
Lab Sample ID: MB 680-135248/9
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/15/2009
Date Prepared: 04/15/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromoriiethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-0ichloroe\hane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
1124
1124
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl. chloride
Xylenes, Total
Surrogate
4-Brornofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
Analysis Batch: 680-135248
Prep Batch: NIA
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
93
106
103
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 44 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq735.d
Initial. WeightNolume: 5 ml
Final WeightNolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0'
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135248
LCS Lab Sample ID: LCS 680-135248/6 Analysis Batch: 680-135248
Client Matrix: Waler Prep Batch: NIA
Dilution: 1.0 Units: ugll
Date Analyzed: 04/15/2009 0912
Date Prepared: 04/15/2009 0912
LCSD Lab Sample ID:.LCSD 680-135248/7 Analysis Batch: 680-135248
Client Matrix: Water Prep Batch: NIA
Dilution: 1.0 LI.nits: ug/L
Date Analyzed: 04/15/2009 0941
Date Prepared: 04/15/2009 0941 ·
% Rec.
Analyte LCS LCSD Limit
Acetone 101 100 17-175
Benzene 93 94 77-119
Bromoform 120 119 62 -133
Bromomethane 172 174 12-184
Carbon disulfide 86 85 55 -131
Carbon tetrachloride 91 91 71 -135
Chlorobenzene 96 97 85 -116
Chlorodibromomethane 108 108 75 -133
Chloroethane 98 93 40 -165
Chloroform 99 100 82 -120
Chloromethane 103 100 48 • 142
cis-1,2-Dichloroethene 104 103 69 -134
cis-1,3-Dichloropropene 104 104 76 -126
Dichlorobromomethane 98 101 78 • 127
1, 1-Dichloroethane 100 100 74 -127
1,2-Dichloroethane 90 92 66 -132
1, 1 ·Dichloroethene 96 96 62 -141
1,2-Dichloropropane 93 93 73 · 124
Ethylbenzene 99 100 86 -116
2·Hexanone 97 100 34-161
Methylene Chloride 102 101 70 · 125
2-Butanone (MEK) 99 100 33 -157
4-Methyl-2-pentanone (MIBK) 91 93 40 · 151
Styrene 100 101 82 • 122
1, 1,2,2-Tetrachloroethane 99 100 69 -129
Tetrachloroethene 104 104 76 -126
Toluene 93 95 81 -117
trans•1,2·Dichloroethene 96 95 72 -131
trans• 1,3•Dichloropropene 105 106 73 -128
1, 1, 1 ·Trichloroethane 89 92 76 • 127
1, 1,2· Trichloroethane 91 92 75 -121
Trichloroethene 89 90 84 -115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GCIMS Volatiles -0
Lab File ID: oq727.d
Initial WeighWolume: 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles· 0
Lab File ID: oq729.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
RPD RPD Limit LCS Oual LCSD Oual
1 50
2 30
30
50
30
30
1 30
0 30
6 50
1 30
2 50
1 30
0 30
3 30
o 30
3 30
1 30
0 30
1 30
3 30
0 30
1 30
2 30
30
30
30
2 30
1 30
2 30
3 30
30
30
Calculations are performed before rounding to avoid round.off errors in calculated results.
TestAmerica Savannah Page 45 of 68
Quality Control Results
Client: AECOM, Inc. Job Number 680-46224-1
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135248
Method: 82608
Preparation: 50308
LCS Lab Sample ID: LCS 680-135248/6
Client Matrix:
Dilution:
Water
1.0
Dale Analyzed:
Date Prepared:
04/15/2009 0912
04/15/2009 0912
LCSD Lab Sample ID: LCSD 680-135248/7
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
Surrogate
Water
1.0
04/15/2009
04/15/2009
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
0941
0941
Analysis Batch: 680-135248
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135248
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
102 101 59 -144
99 100 84-118
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq727.d
Initial WeighWolume: 5 ml
Final WeightNolume: 5 ml
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq729.d
Initial Weight/Volume: 5 ml
Final WeightNolume: 5 ml
RPO RPO Limit LCS Oual LCSD Qual
2
50
30
LCS % Rec LCSD % Rec Acceptance Limits
96
103
95
98
101
95
75 -120
75 -121
75 -120
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 46 of 68
Client: AECOM, Inc.
Method Blank· Batch: 680-135330
Lab Sample ID: MB 680-135330/8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009
Date Prepared: 04/14/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dich\oroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
1420
1'420
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene·
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
Analysis Batch: 680-135330
Prep Batch: NIA
Units:. ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
92
94
103
Qual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 47 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - A
Lab File ID: aq767.d
Initial WeighWolume: 5 ml
Final WeightNolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135330
LCS Lab Sample ID: LCS 680-135330/5 Analysis Batch: 680-135330
Client Matrix: Water Prep Batch: NIA
Dilution: 1 0 Units: ug/L
Date Analyzed: 04/14/2009 1211
Date Prepared: 04/14/2009 1211
_,,,,, ___ , __ , ____
LCSD Lab Sample ID: LCSD 680-13533016 Analysis Batch: 680-135330
Client Matrix: Water Prep Batch: N/A
Dilution: 1.0 Units: ug/L
Date Analyzed: 04/14/2009 1253
Date Prepared: 04/14/2009 1253
% Rec.
Analyte LCS LCSD Limit
Acetone 91 87 17-175
Benzene 96 92 77-119
Brornoform 92 85 62 -133
Bromomethane 102 100 12 -184
Carbon disulfide 85 91 55 -131
Carbon tetrachloride 114 101 71 -135
Chlorobenzene 105 95 85 -116
Chlorodibromomethane 106 106 75 -133
Chloroethane 92 103 40 -165
Chloroform 101 95 82 -120
Chlorornethane 92 90 48 -142
cis-1,2-0ichloroethene 88 88 69 -134
cis-1,3-Dichloropropene 104 99 76 -126
Dichlorobromomethane 104 101 78 -127
1, 1-Dichloroethane 94 92 74 -127
1,2-Dichloroethane 106 103 66 -132
1, 1-Dichloroethene 81 86 62 -141
1,2-Dichloropropane 100 95 73 -124
Ethyl benzene 110 97 86 -116
2-Hexanone 99 93 34 -161
Methylene Chloride 94 91 70 -125
2-Butanone (MEK) 83 104 33 -157
4-Methyl-2-pentanone (MIBK) 94 95 40 -151
Styrene 105 98 82 -122
1, 1,2,2-Tetrachloroethane 93 94 69 -129
Tetrachloroethene 113 99 76 -126
Toluene 106 97 81-117
trans-1,2-Dichloroethene 81 89 72 -131
trans-1,3-Dichloropropene 105 99 73 -128
1, 1, 1-Trichloroethane 106 97 76 -127
1, 1,2-Trichloroethane 101 95 75 -121
Trichloroethene 108 95 84 -115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq759.d
Initial WeightNo!ume: 5 ml
Final Weight/Volume: 5 ml
--·---·--··
. Instrument ID: GC/MS Volatiles -A
Lab File ID: aq761.d
Initial WeightNolume: 5 ml
Final Weight/Volume: 5 ml
RPO RPO Limit . LCS Qual LCSD Qual
4 50
4 30
7 30
2 50
6 30
12 30
10 30
0 30
11 50
7 30
2 50
0 30
5 30
3 30
3 30
3 30
5 30
5 30
13 30
7 30
3 30
23 30
30
7 30
30
13 30
9 30
8 30
5 30
9 30
6 30
12 30
Calculations are periormed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 48 of 68
Client: AECOM, Inc.
Lab Control Spike/
Quality Control Results
Job Number: 680-46224-1
Lab Control Spike Duplicate Recovery Report• Batch: 680-135330
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 680-135330/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009 1211
Date Prepared: 04/1412009 1211
LCSD Lab Sample ID: LCSD 680-135330/6
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
VinYI chloride
Xylenes. Total
Surrogate
Water
1.0
04/14/2009
04/14/2009
4-Brornofluorobenzene
Dibromof!uoromethane
Toluene-dB (Surr)
1253
1253
Analysis Batch: 680-135330
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-135330
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
101 87 59 -144
108 95 84 -118
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq759.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq761.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
RPD RPO Limit LCS Qual LCSD Qual
15 50
12 30
LCS % Rec LCSD % Rec Acceptance Limits
103 96 75 -120
96 94 75-121
100 95 75 -120
Calculations are performed before rounding to avoid round-off errors in calculated results.
T estAmerica Savannah Page 49 of 68
Client: AECOM, Inc.
Method Blank· Batch: 680-135332
Lab Sample ID: MB 680-135332/16
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Water
1.0
04/15/2009 1327
04/15/2009 1327
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dlchloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1 ,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Viny! chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
T oluene-d8 (Surr)
Analysis Batch: 680-135332
Prep Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1,0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
94
96
102
Oual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are periormed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 50 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - A
Lab File ID: aq781.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1,0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Lab Control Spike/
Quality Control Results
Job Number: 680-46224-1
Lab Control Spike Duplicate Recovery Report -Batch: 680-135332
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 680-135332/13 Analysis Batch: 680-135332 Instrument 10: GC/MS Volatiles - A
Client Matrix: Water Prep Batch: NIA Lab File ID: aq773.d
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5 ml
Date Analyzed: 04/15/2009 1131 Final Weight/Volume: 5 ml
Date Prepared: 04/15/2009 1131
-·--~·-------
LCSD Lab Sample ID: LCSD 680-135332114 Analysis Batch: 680-135332 Instrument ID: GC/MS Volatiles - A
Client Matrix: Water Prep Balch: NIA Lab File ID: aq775.d
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5 ml
Date Analyzed: 04/15/2009 1200 Final Weight/Volume: 5 ml
Date Prepared: 04115/2009 1200
% Rec.
Analyte LCS LCSD Limit RPO RPO Limit LCS Qual LCSD Qual
Acetone 98 97 17-175 1 50
Benzene 87 93 77-119 6 30
Bromoform 96 96 62 -133 1 30
Bromomethane 75 100 12-184 29 50
Carbon disulfide 70 75 55 -131 6 30
Carbon tetrachloride 122 124 71 -135 2 30
Chlorobenzene 96 100 85 -116 4 30
Chlorodibromomethane 110 112 75 -133 2 30
Chloroethane 92 87 40 -165 5 50
Chloroform 92 96 82-120 5 30
Chloromethane 81 82 48 -142 1 50
cis-1,2-Dichloroethene 78 82 69 -134 5 30
cis-1,3-0ichloropropene 106 106 76 -126 0 30
Dichlorobromomethane 109 112 78 -127 2 30
1, 1-Dichloroethane 83 87 74 -127 5 30
1,2-Dichloroethane 115 . 112 66 -132 2 30
1, 1-0ichloroethene 65 69 62-141 5 30
1,2-Dlchloropropane 97 100 73 -124 4 30
Ethylbenzene 98 105 86-116 6 30
2-Hexanone 100 104 34-161 4 30
· Methylene Chloride 82 89 70 -125 7 30
2-Butanone (MEK) 81 83 33 -157 2 30
4-Methyl-2-pentanone (MIBK) 102 101 40 -151 1 30
Styrene 97 100 82 -122 3 30
1, 1,2,2-T etrachloroethane 90 93 69 -129 3 30
T etrachloroethene 100 105 76 -126 5 30
Toluene 102 107 81 -117 5 30
trans-1,2-Dlchloroethene 70 73 72 -131 5 30
trans-1,3-Dichloropropene 107 111 73 -128 4 30
1, 1, 1-T richloroethane 117 117 76 -127 0 30
1, 1,2-Trichloroethane 102 104 75 -121 2 30
Trichloroethene 102 106 84-115 5 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 51 of 68
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135332
LCS Lab Sample ID: LCS 680-135332/13
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/15/2009 1131
04/15/2009 1131
LCSD Lab Sample ID: LCSD 680-135332/14
Client Matrix: Waler
Dilution: 1.0
Date Analyzed: 04/15/2009 1200
Dale Prepared: 04/15/2009 1200
Analysis Batch: 680-135332
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135332
Prep Batch: N/A
Units: ug/L
% Rec.
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles - A
Lab File ID: aq773.d
Initial WeighWo!ume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: GC/MS Volatiles - A
Lab File 10: aq775.d
Initial WeighWolume: 5 ml
Fi~al WeighWolume: 5 ml
Analyte LCS LCSD Limit RPO RPO Limit LCS Oual LCSD Qua!
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
85
97
88
102
LCS % Rec
97
92
98
59 -144 4
84 -118 5
LCSD % Rec
104
88
103
Calcu!ations are pertormed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 52 of 68
50
30
Acceptance Limits
75 -120
75-121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-135495
Lab Sample ID: MB 680-135495/7
Client Matrix·
Dilution:
Date Analyzed:
Water
1.0
04/17/2009 0928
Date Prepared: 04/17/2009 0928
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-T richloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8 (Surr)
Analysis Batch: 680-135495
Prep Batch: N/A
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
95
109
102
Oual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page _53 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq761.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1 0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Quality Control Results
Cl.ient: AECOM, Inc. Job Number: 680-46224-1
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135495
Method: 8260B
Preparation: 5030B
LCS Lab Sample ID: LCS 680-135495/4 Analysis Batch: 680-135495 Instrument ID: GC/MS Volatiles -0
Client Matrix: Water Prep Batch: N/A Lab File ID: oq757.d
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5 ml
Date Analyzed: 04/1712009 0809 Final WeighWolume: 5 ml
Date Prepared: 04/1712009 0809
__ ,, ____ , ____ ,,_,__ -------, __ ,, ____ ------________ ,, _________ ,_,,_,,,,,,.,., __ ,_,,,,_, __ ,,,_, __ ,,,_, ___ , _
LCSD Lab Sample ID: LCSD 680-135495/5 Analysis Batch: 680-135495 Instrument ID: GC/MS Volatiles -0
Client Matrix: Water Prep Batch: NIA Lab File ID: oq758.d
Dilution: 1.0 Units: ug/L Initial Weight/Volume: 5 ml
Date Analyzed: 04/17/2009 0829 Final Weight/Volume: 5 ml
Date Prepared: 04/17/2009 0829
% Rec.
Analyte LCS LCSD Limit RPO RPO Limit LCS Qual LCSD Qual
Acetone 96 102 17-175 7 50
Benzene 95 99 77-119 4 30
Bromoform 124 129 62 -133 4 30
Bromomethane 172 182 12 -184 6 50
Carbon disulfide 82 86 55-131 4 30
Carbon tetrachloride 94 99 71 -135 5 30
Chlorobenzene 98 103 85 -116 5 30
Chlorodibromomethane 113 115 75 -133 2 30
Chloroethane 95 99 40 -165 4 50
Chloroform 98 101 82 -120 3 30
Chloromethane 99 102 48 -142 3 50
cis-1,2-Dichloroethene 100 105 69 -134 5 30
cis-1,3-Dichloropropene 107 110 76 -126 3 30
Dichlorobromomethane 101 108 78 -127 6 30
1, 1-Dichloroethane 97 100 74 -127 3 30
·1,2-Dichloroethane 92 98 66 -132 7 30
1, 1-Dichloroethene 93 97 62-141 4 30
1,2-Dichloropropane 95 99 73 -124 4 30
Ethylbenzene 99 104 86-116 5 30
2-Hexanone 99 99 34 -161 0 30
Methylene Chloride 99 102 70 -125 3 30
2-Butanone (MEK) 97 97 33 -157 0 30
4-Methyl-2-pentanone (MIBK) 94 98 40 -151 4 30
Styrene 103 109 82 -122 5 30
1, 1,2,2-T etrachloroethane 100 105 69 -129 5 30
T etrachloroethene 104 107 76 -126 3 30
Toluene 96 99 81-117 4 30
trans-1,2-Dichloroethene 92 96 72 -131 5 30
trans-1,3-Dichloropropene 110 116 73 -128 5 30
1, 1, 1-Trichloroethane 92 97 76 -127 5 30
1, 1,2-Trich!oroethane 96 98 75 -121 2 30
Trichloroethene 91 96 84-115 6 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 54 of 68
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135495
LCS Lab Sample ID: LCS 680-135495/4
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04117 /2009 0809
04/1712009 0809
LCSD Lab Sample ID: LCSD 680-135495/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
Surrogate
Water
1.0
04/1712009 0829
04/17/2009 0829
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
Analysis Batch: 680-135495
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-135495
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
102 105 59 -144
101 105 84 -118
RPD
3
4
LCS % Rec LCSD % Rec
97 104
100 104
97 102
Calculations are performed before rounding to avoid round-off errors in calculated results.
T estAmerica Savannah Page 55 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq757.d
Initial WeighWolume: 5 ml
Fin"al Welght/Volume: 5 ml
Instrument ID: GC/MS Volatiles - O
Lab File ID: oq758.d
Initial WeightNolume: 5 ml
Final Weight/Volume: 5 ml
RPD Limit LCS Oual LCSD Oual
50
30
Acceptance Limits
75 -120
75-121
75 -120
Client: AECOM. Inc.
Method Blank -Batch: 680-135496
Lab Sample ID MB 680-135496/7
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/16/2009 1134
Date Prepared: 04/16/2009 1134
Analyte
Analysis Batch: 680-135496
Prep Batch: N/A
Units: ug/L
Result Qual --------------·-·------------------Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroetharle
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-0ichloroethane
1,2-0ichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichtoroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Vinyl chl~ride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
25 u
1.0 u
1.0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
10 u
5.0 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
2.0 u
% Rec
93
106
100
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 56 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq753.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135496
LCS Lab Sample ID: LCS 680-135496/4
Client Matrix:
Dilution:
Date Analyzed
Water
1.0
04/16/2009 0904
Date Prepared: 04/16/2009 0904
LCSD Lab Sample ID: LCSD 680-135496/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Water
1.0
04/16/2009 0933
04/1612009 0933
Chlorodibromomethane
Chloroethane·
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1 -Oichloroethane
1,2-0ichloroethane
1, 1-Dich!oroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MtBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-135496
Prep Batch: NIA
Units: ug/L
Analysis Batch: 680-135496
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
103 101 17-175
95 95 77 -119
123 122 62 -133
166 164 12-184
88 85 55 -131
94 94 71 -135
101 100 85 -116
111 111 75 -133
98 93 40 -165
101 100 82 • 120
102 100 48 -142
104 102 69 -134
105 106 76 -126
101 98 78 -127
101 100 74 -127
91 93 66 -132
98 97 62 -141
93 95 73 -124
104 102 86 -116
101 100 34 -161
103 101 70 -125
99 99 33 -157
94 96 40 -151
106 104 82 -122
102 103 69 -129
108 105 76 • 126
97 96 81 • 117
97 94 72 -131
109 108 73 -128
93 93 76 -127
93 96 75 -121
95 94 84 -115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GCIMS Volatiles• 0
Lab File ID: oq745.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq747.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPD RPD Limit LCS Oual LCSD Oual
3 50
0 30
30
1 50
3 30
0 30
1 30
1 30
5 50
1 30
2 50
2 30
0 30
3 30
2 30
30
1 30
2 30
30
30
1 30
0 30
2 30
30
1 30
3 30
0 30
2 30
0 30
0 30
3 30
2 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 57 of 68
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135496
LCS Lab Sample ID: LCS 680-135496/4
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/16/2009 0904
04/16/2009 0904
LCSD Lab Sample ID: LCSD 680-135496/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
Water
1.0
04/16/2009 0933
04/16/2009 0933
Analysis Batch: 680-135496
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135496
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
104 101 59 -144
104 102 84 -118
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0
Lab File ID:· oq745.d
RPO
3
2
Initial Weighl/Volume: 5 ml
Final WeighWolume: 5 ml
Instrument ID: GC/MS Volatiles -0
Lab File ID: oq747.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO Limit LCS Dual LCSD Qual
50
30
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene
Oibromofluoromethane
Toluene-dB (Surr)
101
104
97
99
102
98
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 58 of 68
75 • 120
75-121
75 -120
Client: AECOM, Inc.
Method Blank· Batch: 680-135497
Lab Sample ID: MB 680-135497/16
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/16/2009
Date Prepared: 04/16/2009
Analyle
Acetone
Benzene
Bromofor'm
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
1148
1148
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-T etrachloroethane
T etrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
T oluene-dS (Surr)
Analysis Batch: 680-135497
Prep Batch NIA
Units: ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
% Rec
91
112
103
Qua!
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
T estAmerica Savannah Page 59 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq754.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
. 10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2,0
Acceptance Limits
75 • 120
75 -121
75 -120
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135497
LCS Lab Sample ID: LCS 680-135497/4 Analysis Batch: 680-135497
Client Matrix: Water Prep Batch: NIA
Dilution: 1.0 Units: ug/L
Date Analyzed: 04/16/2009 0918
Date Prepared: 04/1612009 0918
LCSD Lab Sample ID: LCSD 680-135497/5 Analysis Batch: 680-135497
Client Matrix: Water Prep Batch: NIA
Dilution: 1.0 Units: ug/L
Date Analyzed: 04/16/2009 094 7
Date Prepared: 04/16/2009 0947
% Rec.
Analyte LCS LCSD Limit
Acetone 96 96 17 -175
Benzene 97 100 77 -119
Bromoform 101 102 62 -133
Bromomethane 162 171 12-184
Carbon disulfide 91 94 55 -131
Carbon tetrachloride 92 94 71 -135
Chlorobenzene 100 103 85 -116
Chlorodibromomethane 114 116 75 -133
Chloroethane 128 122 40 -165
Chloroform 102 105 82 -120
Chloromethane 11 o 113 48 -142
cis-1,2-Dichloroethene 104 106 69 -134
cis-1,3-Dichloropropene 104 106 76 -126
Oichtorobromomethane 98 100 78 -127
1, 1-Dichloroethane 102 105 74-127
1,2-Dichloroethane 92 93 66 -132
1, 1-Dich\oroethene 101 102 62 -141
1,2-Dichloropropane 92 96 73 -124
Ethylbenzene 104 107 86 -116
2-Hexanone 101 102 34 -161
Methylene Chloride 103 103 70 -125
2-Butanone (MEK) 97 99 33 -157
4-Methyl-2-pentanone (MIBK) 96 97 40 -151
Styrene 105 107 82 -122
1, 1,2,2-Tetrachloroethane 100 102 69 -129
Tetrachloroethene 110 112 76 -126
Toluene 98 100 81-117
trans-1,2-Dichloroethene 100 103 72 -131
trans-1,3-Dichloropropene 106 106 73 -128
1, 1, 1-Trichloroethane 92 94 76 -127
1, 1,2-Trichloroethane 95 95 75 -121
Trichloroethene 99 106 84 -115
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq746.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
--------··-
Instrument 10: GCIMS Volatiles -0 C2
Lab File ID: oq748.d
Initial WeighWolume: 5 ml
Final WeighWolume: 5 ml
RPO RPO Limit LCS Oual LCSD Qual
o 50
3 30
1 30
6 50
3 30
3 30
3 30
2 30
4 50
2 30
2 50
30
30
1 30
3 30
2 30
30
4 30
3 30
o 30
1 30
3 30
30
1 30
2 30
2 30
3 30
3 30
o 30
2 30
o 30
7 30
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 60 of 68
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-135497
LCS Lab Sample ID: LCS 680-135497/4
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/16/2009 0918
04/16/2009 0918
LCSD Lab Sample ID: LCSD 680-135497/5
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Water
1.0
04/16/2009 0947
04/16/2009 094 7
Analysis Batch: 680-135497
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-135497
Prep Batch: N/A
Units: ug/L
% Rec.
Quality Control Results
Job Number: 680-46224-1
Method: 8260B
Preparation: 50308
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq746.d
Initial Weight/Volume: 5 ml
Final Weight/Volume: 5 ml
Instrument ID: GC/MS Volatiles -0 C2
Lab File ID: oq7 48.d
Initial W_eight/Volume: 5 ml
Final WeighVVolume: 5 ml
Analyte LCS LCSD Limit RPO RPO Limit LCS Qual LCSD Qual
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
T oluene-d8 (Surr)
104
106
105
107
LCS % Rec
100
106
98
59 -144 1
84-118 2
LCSD % Rec
102
106
100
Calculations are periormed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 61 of 68
50
30
Acceptance Limits
75 -120
75-121
75 -120
Client: AECOM, Inc.
Method Blank -Batch: 680-135284
Lab Sample ID: MB 680-135284/1-A
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Water
1.0
04/17/2009 0814
04/16/2009 0600
Cyanide, Amenable
Duplicate -Batch: 680-135284
Lab Sample ID: 680-46224-8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/17/2009 0814
Date Prepared: 04/16/2009 0600
Analyte
Cyanide, Amenable
Analysis Batch: 680-135404
Prep Batch: 680-135284
Units: mg/L
Result
0.0050
Analysis Batch: 680-135404
Prep Batch: 680-135284
Units: mg/L
Qual
u
Sample ResulUQual Result
0.029 0.0291
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 62 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 335.1
Preparation: Distill/CN
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RL
0.0050
Method: 335.1 .
Preparation: Distill/CN
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPD Limit
0 20
Oual
Client: AECOM, inc.
Method Blank· Batch: 680-135285
Lab Sample ID: MB 680-135285/1-A
Client Matrlx: Water
Dilution: 1 .0
Date Analyzed: 04/17/2009 0806
Date Prepared: 04/16/2009 0631
Analyte
Cyanide, Total
Lab Control Spike -Batch: 680-135285
Lab Sample ID: LCS 680-135285/2-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/17/2009 0806
Date Prepared: 04/16/2009 0631
Analyte
Cyanide, Total
Matrix Spike/
Analysis Batch: 680-135403
Prep Batch: 680-135285
Units: mg/L
Result
0 0050
Analysis Balch: 680-135403
Prep Balch: 680-135285
Units: mg/L
Spike Amount Result
0.0301 0.0302
Matrix Spike Duplicate Recovery Report -Batch: 680-135285
MS Lab Sample ID: 680-46224-16
Client Matrix: Water
Dilution: 1.0
Date. Analyzed: 04/17/2009 0806
Date Prepared: 04/16/2009 0631
MSD Lab Sample ID: 680-46224-16
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/17/2009 0806
Date Prepared: 04/16/2009 0631
Analyte
Cyanide, Total
Analysis Batch: 680-135403
Prep Batch: 680-135285
Analysis Batch: 680-135403
Prep Batch: 680-135285
% Rec.
MS MSD Limit
100 96 90 -110
Qual
u
Quality Control Results
Job Number: 680-46224-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume· 50 ml
Final WeighWolume: 50 ml
RL
0.0050
Method: 335.4
Preparation: Distill/CN
Instrument ID: No Equipment Assigned
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
% Rec. Limit Qual
100 90 -110
Method: 335.4
Preparation: Distill/CN
Instrument ID:
Lab File ID:
No Equipment Assigned
N/A
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
Instrument ID: No Equipment Assigned
Lab File ID: N/A
RPO
4
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPO Limit MS Qual MSD Qual
20
Calculations are performed before rounding to avoid round~off errors in calculated results.
TestAmerica Savannah Page 63 of 68
Client: AECOM, Inc.
Duplicate -Batch: 680-135285
Lab Sample ID: 680-46224-8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/17/2009 0806
Date Prepared: 04/17/2009 0743
Analyte
Cyanide, Total
Analysis Batch: 680-135403
Prep Batch: 680-135285
Units: mg/L
Sample Resull/Qual
0.10
Result
0.103
Calculations are performed before rounding to avoid round•off errors in calculated results.
TestAmerica Savannah Page 64 of 68
Quality Control Results
Job Number: 680-46224-1
Method: 335.4
Preparation: Distill/CN
Instrument 10: No Equipment Assigned
Lab File ID: NIA
Initial WeighWolume: 50 ml
Final WeighWolume: 50 ml
RPO Limit
20
Qual
Client: AECOM, Inc.
Method Blank -Batch: 680-135236
Lab Sample ID: MB 680-135236/2
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009
Date Prepared: N/A
Analyte
Toti31 Organic Carbon
TOC Result 1
TOC Result 2
TOC Result 3
Lab Control Spike/
1113
Analysis Batch: 680-135236
Prep Batch: N/A
Units: mg/L
Result
1.0
1.0
1.0
1.0
Lab Control Spike Duplicate Recovery Report -Batch: 680-135236
LCS Lab Sample ID: LCS 680-135236/4
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009 1147
Date Prepared: N/A
LCSD Lab Sample ID: LCSD 680-135236/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 04/14/2009 1200
Date Prepared: N/A
Analyt~
Total Organic Carbon
TOC Result 1
TOC Result 2
TOC Result 3
Analysis Batch: 680-135236
Pr_ep Batch: N/A
Units: mg/L
Analysis Batch: 680-135236
Prep Batch: N/A
Units: mg/L
% Rec.
LCS LCSD Limit
100 99 80 -120
100 99 80 -120
99 99 80 -120
100 99 80·-120
Ouat
u
u
u
u
Quality Control Results
Job Number: 680-46224-1
Method: 415.1
Preparation: N/A
Instrument !O: Total Organic Carbon Anal~
Lab File ID: N/A
Initial WeighWolume: 25 ml
Final Weight/Volume: 25 ml
Method: 415.1
Preparation: N/A
RL
1.0
1.0
1.0
1.0
· Instrument ID: Total Organic Carbon Anal:
RPD
1
0
2
Lab File ID: N/A
Initial Weight/Volume: 25 ml
Final Weight/Volume: 25 ml
Instrument ID:
Lab File ID:
Total Organic Carbon An,
N/A
Initial Weight/Volume: 25 ml
Final Weight/Volume: 25 ml
RPD Limit LCS Oual
25
25
25
25
LCSD Oual
Calculations are performed before rounding to avoid round-off errors in calcu!ated.results.
TestAmerica Savannah Page 65 of 68
Testi~merica
Client Name AfCoVVl Client#: -----Addresa: JQ<:\\ o\J wo:14-: h,r<,1-,
CitytState/ZipCode: ~½, N<-..l._'7(p ('f'
ProjectManager ~ .µ.,J"°(l,J?
Telephone Number: 9\C\-n~-(;.G,oo Fax: _______ _
To 88Sist ue In using the proper analytlcaJ melhods.
is this wori< being conducted for regulatory purposes?
Compliance Monitoring
ProjedName:.~'.JI:....,_,&c..1-.=ox:....:..,;,:.;_;'a:...~------
Project#: _________________ _
Site/Location ID:--"'(;)'-'K"-¼-"'-t..;;;J.,;..,.. ___ ~_ State: _;_lv.::....,G"-·---
Report To:_·.,.6"-"·e~·;JJ.:.:..::.:.......1f:\,,""'-,-.,...="'""]~:.:.+------
Invoice To:--'----''--------• _________ _ Sampler Name: (~nt Name)_:::::'-->''r.--'-""'f--"_-,,.,,,~\\,f-'_'.\._\ ______________ _
sampler Signsture: _~...::::-=...:=:=--~---;:;:;:::;:;;::;:==::;:======;;====:....---=°"::o;l•:#::.::,;:::======:..:,P_:0#::,;: =~-----Matrix Preservation & # of Containe
~T f=-Standard
_ Rush (surcharges may apply)
Dam N8"ded: _____ _
~ Fax RHults: y N <Q
~
"' "' SAMPLE ID
0 ..
. "' a,
-!
(Bstch QC)
Level3
Level4
Other:_;_ __
REMARKS
"' ~ CQ
II)
"' ._,
0
"'
"' a,
Testi~merica
Client#: -----
City/State/Zip Code:~, Ne,, 'J., 7<ti I 4,
c1~t ~::,:' •• /t:(coM
Add=:'7o<./~IJ uJ..k,Fo,_.,r lt ·
Project Manager: ~ kk,,.-t'lo.~
TalephoneNumbec C\\"l -'31~-<J~ooJ' Fax:_· ______ _
Sampler Name: (Prim Name)-~?'·..,..,~=· _,·'-',C-"=''-',l~")J.i',,_\::..· ______________ _
Sam,,.er Signature· {.k. k:fl
Matrix Preservation & # of Container
TAT _r..._ Standard
_ Rush (surcharges may apply)
Date Needed: _____ _
Fax R89ulta: Y N
SAMPLE ID
/100 V
£°Bo(
10,..ol\/
To aaalsl us In using the proper analytlcal methods,
is this work being oonductoo for regulatory purposes?
Corrl)lian~ Monitoring
Project Nanw> . J"Pf.) [ O?({;J
Project#: _______________ _
Site/Location ID: _,,Q&"-"--'ill'l~""..l,,_ ____ State Ne
Report To: _,,G.:;;:@=='-· .1.µ.,.o'-'r'-"'=~~==A-· _______ _
Invoice To:_:::fcl:::!~5':_ ____________ _
Quote#·
Anar~For:
I
I
, y\., oeuvernoaes
_None
_Level2
(Botch QC)
_Level3
_Level4
Other: __ _
REMARKS
1.1/7(9 I_, 70" L. .. ·. ·-~)/✓ -L.
081.e: Time: ill-f/fltl1 Date:
Date: Time: Data:
0 "'
"' a,
Testi~merica
c1~n-1 ~::'"A'~wtM
Addresa· '?~Ml,J~~~(.; .--,..iS: P,J,,
CrtylStalelZip Code V\ :i0 (..:-1 (tl~
Proiect Manager (;.u,,., ~r-",),a _
Telephone NumberC\\5-i[]?.-yl;oo Fax: _______ _
To auist us ln using the praper anatytlcal methods.
is this work being conducted for regulatory purposes?
Compliance Monitoring
Client#: ____ _
Project Name if~ t 0£ -6 ~P
Project#:.~--~--------------
Site/Localion ID: o-'((,:c;;;;,:: StatelJC,.,.::'-=----
Report To Ge1ocll tk""'--a •1 lnvoic.e To: -"-"'
Sampler Name: (PrinlName)_A.:.,l.u\,.._· w.;,•.~.,._~l.,..il-----------------
S&mpler Signature·_W==\\=:)IJJ=---,=;;:;:=.:;~==::::::;::::~==:;::=_== -. =;_ __ _:o:uo;t•:#;·;;;:;;:::=========:..:,P_:OII::,;· ===,------
Matrix Preservatlon & # c, ContainAr Anet ze For:
~Standard
_ Rush (surcharges may apply) " l u i l :;
U) U) s
SAMPLE ID ~ ~ ;Ji
Date Needed: _____ _
Fax RetiultB: Y N
0
:r: 0 5i
~1i1i I
u.\t,\w -l O '-\' · 'l rnnc. 1/ ')< I(
1y1.,, Oen~era0tes
_None
_Level2
, (Betel! QCJ
_Level3
_level4
Other: __ _
REMARKS
1---'-r··e.M~"11..l::...·-"!'0..,___i; __ -+-+-14'~!-"~-">04+-++--l--l--l~-z."+-+--1-4-l-..4--'-li<_---+--+-+--+--+-_j:..-i--4---1-----
"'.kl.) -\ · I v: 1-r.w.. -r::1.15
-0.0:~1(µrliirr~,~TS_,
In_-,,_-___ -,_,-_,-~---1(1"1):--. --;1T:~~:-1yn-1--T l.,';-j;i\:r-1ii'\'\nL-__ -_ -::,100==. =-11~-~;.~z-::..;::;·~"-' s.:r---~----:---,r.,.-•• -. -,,~-.--.---:--1 !ltr:Tu1!(2t:f;&p: ·• . ·-··.
Special ln9tructlon1;
µ:R~el~I ~~~c_: _______ _j!:D~at~e: __ .j.;nc!!,m~e"":--~~~1l'.::...L"'-,L.:.-:C::!:'...~-_..j~1,!::/_11_'[)_7_..ji!.t<,!!!Ve'.!!!e-:..Sr{_·_~j°:f'fl\,U,PJ'.l(~,~yTe~t,~~•'.ica: Y. N
Relinquished B : Date: Time: Time:
o ... TEMP
AECOM Environment
704i Old Wake Fores! Road, Suiie 103, Raleigh, NC 27616·3013
T 919.872.6600 F 919.872.7996 www.aecom.com
February 4, 2009
Mr. Larry Thomas
City Engineer
City of Oxford
P 0. Box 1307
Oxford, North Carolina 27565
RE: Industrial Users Report for February 2009
I 1€! «; {~ ll If /fE
FEB 1 02009 I
SUPERFUNO SECTION
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 10140-025
Dear Mr. Thomas:
On behalf of The Unimax Corporation and Avnet, Inc., ENSR Consulting and Engineering (NC), Inc.
(AECOM Environment) is submitting the Quarterly Industrial User Permit report for the months of
November and December, 2008 and January 2009. This report is prepared in accordance with permit
requirements for the discharge of treated groundwater at the above referenced site.
If you have any questions, please contact us at
[phone].
Sincerely,
G~~H
Project Engineer
Enclosure
William H. Doucette, Jr., Ph.
Senior Program Manager
cc: Steve Kempf -United and Industries Monument Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Ken Lucas, RPM -USEPA Superfund
Nanjun Shelly, P.E. -AECOM
File
AECOM Environment
INDUSTRIAL USER REPORTING FORM
IU. PERMITNO G001 D1SCHARGENO ___ ~0~0~1 _____ _
MONTHS: November. December and January YEAR: 2008 -2009
LU. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERATOR IN RESPONSIBLE CHARGE (ORC): ENSR Consulting & Engineering (NC). Inc.
LABORATORY PERFORI\11NG ANALYSIS: Test America (Formerly STL-Savannah)
PERSON(S) COLLECTING SAMPLES Joe Ladd (ENSR)
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet permit monitoring requirements. D
(Noncompliant)
lfthe facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets ifnecessary)
I certify that this Report is accurate and
complete to the best of my knowledge:
Signature of Permittee Represen alive
William H. Doucctte,,Jr., PhD.
/I~-),_ 7<, P.->
~'l{lln\pn,,,cl\.~\~erlir.<-1s\2009\!o!,2009\u"lannlob?009.lloc
2-lf" 2oo°f
Date:
TABLE 1. GROUNDWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.LI. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
I.LI. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS·
PERSON($) COLLECTING SAMPLES:
PARAMETER
Daily Average Flow (MGD)
Tetrachloroethylene.
1, 1-Dichloroethane
cis-1,2 Dichloroethene
Chlorobenzene
Toluene
1, 1-Dichloroethylene
trans-1,2 Dichlorocthylene
Trichloroethene
Vinyl Chloride
Cyanide (total)
pH
Temperature
Monitoring requirement only.
MGD Million Gallons per day.
µgll Micrograms per liter.
rng/L Milligrams per liter.
SU Standard Units. •c Degrees Centigrade
G001
001
November, December and January
2008 -2009
JFD Electronics/Channel Master NPL Site
Granville
ENSR Consulting and Engineering (NC), Inc
Tes\America
Joe Ladd (ENSR)
PERMIT LIMITS
Daily Maximum
0.040
0.05
5.0 to 10.0
40
UNITS
MGD
µg/L
µg/L.
µg/L
µg/L
µgll
µgll
µg!L
µg/L
µgll
mglL
SU
•c
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab.
Grab
Grab
Grab
Grab
Grab
Grab
Compound was not detected above the quantitalion limit.
NS Not sampled
G.\Env\JFDCHANN\NC0202.170\Cily of Oxlord\lURTable Fen 2009.xls\Table 1\2/3/2009
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335.2
Field
Field
QUARTERLY MEASUREMENT
DATES
1112012006 12/2212008 1/812009
0.018 0.019 0 020
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS 1.1
NS NS <1.0
NS NS 0.0068
7.96 8.54 8.76
16.3 21.5 14.2
ANALYTICAL REPORT
Job Number: 680-43787-1
Job Description: Channel Master
For:
AECOM, Inc.
7041 Old Wake Forest Road
Suite 103
Raleigh, NC 27616
Attention: Mr. Gerald Hornaday
I t_oJ;{I\ ~/I __
Kathryn Smith
Project Manager I
[e-mail]
01/16/2009
/\ppm~ed tor ielease.
Kathryn Sm,tt,
Proj0c1 Manager 1
1/16/20094:35PM
The test results in this report meet NE LAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEO: 88-0692; AROOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
OEQ: 30690; LA OHH: LA080008; ME: 2008022; MO: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC OWO: 269; NC DHHS: 13701;.PA: 68-00474; PR: GA00006; RI: LA000244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI ONR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax (_912) 352-0165 www testamericainc com
Page 1 of 14
Client: AECOM, Inc.
Description
Matrix Water
Volatile Organic Compounds (GCIMS)
Purge and Trap
Cyanide, Total
Distillation, Cyanide
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Lab Location
TAL SAV
TAL SAV
TAL SAV
TAL SAV
Method
SW846 82608
MCAVVW 335.4
Job Number: 680-43787-1
Preparation Method
SW846 50308
Distilt/CN
MCA WW= "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions,
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates
TestAmerica Savannah
Page 2 of 14
Client: AECOM, Inc
Method
SW846 8260B
MCAWW 335.4
TestAmerica Savannah
METHOD / ANALYST SUMMARY
Analyst
Lui, Chung
McDonald, Debbie
Page 3 of 14
Job Number: 680-43787-1
Analyst ID
CL
OM
Client: AECOM, Inc.
Lab Sample ID
680-43787-1
680-43787-2
TestAmerica Savannah
Client Sample ID
Effluent
Trip Blank
SAMPLE SUMMARY
Client Matrix
Water
Water
Page 4 of 14
Date/Time
Sampled
01/08/2009 1430
01/08/2009 0000
Job Number 680-43787-1
Date/Time
Received
01/0912009 0858
01/09/2009 0858
Analytical Data
Client: AECOM, Inc Job Number: 680-43787-1
Client Sample ID: Effluent
Lab Sample ID·
Client Matrix:
680-43787-1
Water
Method·
Preparation:
Dilution
Date Analyzed·
Date Prepared··
Analyte
Acetone
Benzene
Bromoform
· Bromomethane
Carbon disulfide
8260B
5030B
1.0
01/1212009
01112/2009
Carbon tetrachloride
Chlorobenzene
Ch!orodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-0ichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1, 3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-BromoHuorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1514
1514
82608 Volatile Organic Compounds (GC/MS)
Analysi~ Batch: 680-127227
Result (ug/L) Qualifier
25 u
1.0 u
1.0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
10 u
5.0 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.1
1.0 u
2.0 u
1%Rec
92
104
102
Page 5 of 14
Date Sampled: 01/08/2009 1430
01109/2009 0858 Date Received:
Instrument ID:
Lab File ID
GC/MS Volatiles - P
p0049.d
Initial WeightNolume:
Final WeighWolume:
5 ml
5 ml
Rl
25
1.0
-1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Analytical Data
Client: AECOM, Inc Job Number 680-43787-1
Client Sample ID: Trip Blank
Lab Sample ID:
Client Matrix·
680-43787-2
Water
Method: 8260B
Preparation: 5030B
Dilution· 1.0
Date Analyzed: 01112/2009
Date Prepared: 01/12/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Ch\oroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichlo,roethane
1,2-Dichloroethane
1, 1-Dich\oroethene
1,2-Dichloropropane
Ethytbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-8 romofl u o roben zen e
Dibromofluoromethane
T oluene-d8 (Surr)
TestAmerica Savannah
1445
1445
8260B Volatile Organi~ Compounds (GC/MS)
Analysis Batch: 680-127227
Result (ug/L) Qualifier
25 u
1.0 u
1 0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 0 u
1.0 u
1.0 u
1 0 u
1.0 u
1 0 u
1 0 u
1 0 u
1.0 u
1.0 u
10 u
50 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1 0 u
1.0 u
1.0 u
1.0 u
1.0 u
2.0 . u
%Rec
94
105
100
Page 6 of 14
Date Sampled:
Date Received:
0110812009 0000
01/09/2009 0858
Instrument 10:
Lab File 10:
GC/MS Volatiles - P
p0047.d
Initial WeighWolume:
Final WeightNO\ume:
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Client Sample ID:
Lab Sample 10
Client Matrix:
Ana\yte
Cyanide, Total
Effluent
660-43767-1
Water
Anly Batch
Result
0.0068
660-127496
Prep Batch: 680-127299
TestAmerica Savannah
General Chemistry
Oual Units
mg/L
Date Analyzed 01115120D9 0911
Date Prepared: 01/13/2009 0945
Page 7 of 14
Analytical Data
Job Number· 680-43787-1
Date Sampled
Date Received:
RL
0.0050
01/0812009 1430
01/09/2009 0656
Oil Method
1.0 335.4
DATA REPORTING QUALIFIERS
Client AECOM, Inc. Job Number: 680-43787-1
Lab Section Qualifier Description
GC/MSVOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u lndicates the analyte was analyzed for but not detected
TestAmerica Savannah
Page 8 of 14
Client AECOM, Inc.
Surrogate Recovery Report
82608 Volatile Organic Compounds {GC/MS)
Client Matrix: Water
Lab Sample ID
680-43787-1
680-43787-2
MB 680-127227/7
LCS 680-127227 /4
LCSD 680-127227/5
Surrogate
Client Sample ID
Effluent
Trip Blank
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
TestAmerica Savannah
BFB
%Rec
92
94
93
93
101
DBFM TOL
%Rec %Rec
104 102
105 100
109 101
115 101
114 103
Acceptance Limits
75-120
75-121
75-120
Page 9 of 14
Quality Control Results
Job Number 680-43787-1
Client· AECOM, Inc.
Method Blank -Batch: 680-127227
lab Sample ID: MB 680-127227/7
Client Matrix Water
Dilution: 1.0
Date Analyzed: 01/12/2009
Date Prepared: 01/12/2009
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-0ichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dich!oroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trich!oroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
1144
1144
Analysis Batch: 680-127227
Prep Batch: NIA
Units· ug/L
Result
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
10
1.0
1.0
1.0
1.0
1.0
1.0
2.0
%Rec
93
109
101
Calculations are performed before rounding to avoid round-off errors in calculated results
TestAmerica Savannah Page 10 of 14
Oual
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
QuaHty Control Results
Job Number 680-43787-1
Method: 82608
Preparation: 50308
Instrument ID: GC/MS Volatiles - P
Lab File ID pq059.d
Initial WeightNolume: 5 ml
Final WeightNolume. 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 · 120
Client: AECOM, Inc.
Lab Control Spike/
Lab Control Spike.Duplicate Recovery Report-Batch: 680-127227
LCS Lab Sample ID: LCS 680-127227/4
Client Matrix· Water
Dilution: 1.0
Date Analyzed· 01/1212009 1011
Date Prepared· 01/12/2009 1011
LCSD Lab Sample ID: LCSD 680-127227/5
Client Matrix: Water
Dilution: 1.0
Date Analyzed:
Date Prepared:
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
01/12/2009 1045
01/12/2009 1045
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-0ichloroethene
cis-1,3-0ichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methy_l-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1 ,2-Trichloroethane
Trichloroethene
Analysis Batch: 680• 127227
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-127227
Prep Batch: N/A
Units: ug/L
% Rec
LC$ LCSD Limit
102 103 17 -175
98 101 77 -119
109 117 62 -133
137 148 12 -184
128 118 55-131
110 109 71 -135
97 98 85 -116
97 105 75 -133
129 125 40 -165
116 112 82 -120
136 136 48 -142
114 110 69 -134
104 111 76 -126
102 107 78 -127
112 107 74 -127
95 98 66-132
95 86 62 -141
100 104 73 -124
98 99 86 -116
97 105 34 -161
114 114 70 -125
103 107 33 -157
94 101 40 -151
97 101 82 -122
89 97 69 -129
94 96 76 -126
103 104 81 -117
101 95 72 -131
104 112 73 -128
101 99 76 -127
94 101 75-121
101 103 84-115
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 11 of 14
RPD
2
3
7
8
9
7
3
3
0
4
7
5
5
3
10
3
2
8
0
4
7
4
9
2
1
7
7
2
7
2
Quality Control Results
Job Number: 680-43787-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles - P
pq053.d
Initial WeighWolume·
Final Weight/Volume:
5 ml
5 ml
Instrument ID: GCIMS Volatiles - P
Lab File ID: pq055.d
Initial WeighWo!ume:
Final Weight/Volume
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 mL
· 5 ml
LCS Oual LCSO Qual
Client: AECOM, Inc,
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-127227
LCS Lab Sample 10:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCSD Lab Sample 10:
Client Matrix·
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
lCS 680-127227/4
Water
1.0
01/12/2009 1011
01/12/2009 1011
lCSD 680-127227/5
Water
1.0
01/12/2009 1045
01/12/2009 1045
Analysis Batch: 680·127227
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-127227
Prep Batch: NIA
Units· ugll
% Rec
lCS lCSD Limit
129 116 59 -144
98 100 84 -118
RPD
10
2
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8 (Surr)
LCS % Rec LCSD % Rec
93 101
115 114
101 103
Calculations are Performed before rounding to avoid round-off errors in calculated results
TestAmerica Savannah Page 12 of 14
Quality Control Results
Job Number 680-43787-1
Method: 82608
Preparation: 5030B
Instrument JD·
lab File ID:
GC/MS Volatiles· P
pq053.d
Initial WeighWolurne:
Final WeightNolume
5 ml
5 ml
Instrument ID· GCIMS Volatiles -P
Lab File ID: pq055.d
Initial WeighWolume:
Final WeighW0lume:
5 ml
5 ml
RPO Limit LCS Qual LCSD Qual
50
30
Acceptance Limits
75 -120
75 -121
75 -120
Client: AECOM, Inc.
Method Blank· Batch: 680-127299
Lab Sample ID: MB 680-127299/1-A
Client Matrix: Water
Dilution: 1 .0
Date Analyzed· 01/15/2009 0911
Date Prepared· 01/13/2009 0945
Analyte
Cyanide, Total
Lab Contrc;,I Spike/
Analysis Batch: 680-127496
Prep Batch: 680-127299
Units: mg/L
Result
0.0050
Lab Control Spike Duplicate Recovery Report -Batch: 680-127299
LCS Lab Sample ID: LCS 680-12729912-A
Client Matrix: Water
Dilution:
Date Analyzed·
Date Prepared:
1.0
01/1512009 0911
01/13/2009 0945
LCSD Lab Sample ID: LCSD 680-127299/3-A
Client Matrix: Water
Dilution:
Date Analyzed·
Date Prepared:
Analyte
Cyanide, Total
1.0
01/15/2009 0911
01/1312009 0945
Analysis Batch: 680-127496
Prep Batch: 680-127299
Units: mgll
Analysis Batch: 680-127496
Prep Batch: 680-127299
Units: mg/l
LCS
94
% Rec
LCSD
90
limit
90 · 110
Oual
u
Calculations are performed before rounding to avoid round-off errors 1n calculated results.
TestAmerica Savannah Page 13 of 14
RPO
4
Quality Control Results
Job Number: 680-43787-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: No Equipment Assigned
Lab File ID· N/A
Initial WeightNolume: 50 ml
Final WeightNolume: 50 ml
RL
0 0050
Method: 335.4
Preparation: Oistill/CN
lnstrument 10 No Equipment Assigned
lab File ID: N/A
Initial WeightNolume:
Final WeightNolume:
50 ml
50 ml
Instrument ID: No Equipment Assigned
lab File ID: N/A
Initial WeighWolume:
Final WeightNolume:
50 ml
50 ml
RPO Limit LCS Qual LCSO Qual
20
Serial Number O O 4 0 3 7
ANALYSIS R_EQUEST AND CHAIN OF CUSTODY RECORD <JS TestAmerica s·av_a.nnah Website: www.testamericainc.com
Test America 5102 La Roche Avenue Phone: [phone]
Savannah, GA 31404 Fax: [phone]
C) Alternale L_aboratory Name/Location
Phone·
THE LEADER '1N ENVIRONMENTAL TEST IN~ Fa;,:;
PROJECT REFERENCE
1
/ /Yh t PAOJ~714.o. PROJECT LOCATION MATRIX REQUIRED ANALYSIS PAGE I I OF I /'Ah~,/.,, , r /0 o-(STATE) TYPE .
T AL (LAB) PZ'ECT MANAGER PO. NUMBER CONTRACT NO. ~ STANDARD REPORT
' <;,u,J/A. I" ~ DELIVERY w >-'
CLIENT ~ PM . //4 . t,,CL~)TPHONE CUrTFAY. 0 z :i. ~ -~ ~-
w DATE DUE emlol orJl/ada1/ 1 'ltC/ &'72-l,,/,()C; ( '!11 f-'12--099/f cl Sl J ?
CLIEITT NA. . . : . . l CLIENT E-MAIL . . : s "' EXPEDITED REPORT _; 0 m Q 0 ' ~M ' DELIVERY
"· -1,J • ha,.--,rnd."' ,/4) a ecc-wt .c(/111 "' ,_'.) i :t~ . e c,C1'V1 "' (SURC_HARG~) (!) 0 0 ~~ cu)4 AODRESS /, ln.L Fr,, )-?,-,J . }( q J,,IC.J, "' a' ~ ~ (... . DATE DUE let: J'7wlf/ 0 w '76 I /'!1d . t ✓~ . G' !;, " "' NUMBER OF COOLERS SUBMITTED COMPAN.Y.COtJ"fRACTJNG THIS WORK (if applicabl~} -·i "' lli ~~ x "'·fl:'.lv '.If..,.,~!"".. f:,'"""' !~f1. _11 ' ;<,. 1-r:1;;7. tj'~;· "' "' 0w,:-1 1f.,,,..'t:", :;;,-.~, ~~ rr,~ ';., . ,.~ f,, ,if!\ ' \ PER SHIPMEMT / {. -' l co 0 ~ 9 '" fJ.,,,..,, ~5{ f, •. ,, r, Ii. .J !l(h f1 t ·~ .. ii,,}-· v71e @ 0 i . SAMPLE " co ::; a: SAMPLE IDENTIFICATION 8 '.? g 4' NUMBER OF CO,NTAINERS SUBMITTED REMARKS DATE TIME z .. -
I -<;( oY /1.)-:?-'J £fl'/ve11r G X " I 'f-ci)t) r ·PQF~2-
H 4. '17:,•r, 11./,111/c , ,<l, -
J
.
RELINQUISHED BY: (StGNATUAE) DATE T!ME Ai: [SHED 2.(S!GW.TIJRE) DATE TIME RELINQUISHED BY: (S!GNATURE) DATE TIME
I, , RN/'tJ /-'fi-09 1'7:d-{J
RECn,BY[:ZRE) DATE TIME RE~I D BY: {SIGNATURE.)-OATE T!ME RECEIVED BY .. (SIGNATURE) DATE TIME
.~ .. ""''' /-',;.fJ°f 1-f HJ
// ·.,.-, LABORATORY USE ONLY
RE< ~FOR~fK?} OATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS
{SI~ ~ YES 0 SEAL NO. LOG NO. ~TFMP ✓ . 'VJ1oc;ocr Oi!'>3 NO 0 'nY0C/3171 01b \ ,•
L \ TAL8240-680 (1207)
ENSR Consulting and Engineering (NC), Inc.
7041 Old Wake Forest Road, Suite 103, Raleigh, North Carolina 27616
T 919 872 6600 F 919 872 7996 www.ensr.aecom.com
November 3, 2008
Mr. Larry Thomas
City Engineer
City of Oxford
P .0. Box 1307
Oxford, North Carolina 27565
RE: Industrial Users Report for November 2008
JFD Electronics/Channel Master NPL Site, Oxford, North Carolina
Project No. 1 0140-025
Dear Mr. Thomas:
ENSR A[COM
On behalf of The Unimax Corporation and Avnet, Inc., ENSR Consulting and Engineering (NC), Inc, is
submitting the Quarterly Industrial User Permit report for the months of August, September and
October 2008. This report reflects the new effluent monitoring frequency of once per quarter, which
began in January 2008 when the renewed permit went into effect, and is prepared in accordance with
permit requirements for the discharge of treated groundwater at the above referenced site.
If you have any questions, please contact us at [phone].
Sincerely,
ENSR Consulting and Engineering (NC), Inc.
Ge{;Y~~
Project Engineer
Enclosure
\J ·
William H. Doucette, Jr., Ph.D.
Senior Program Manager
cc: Steve Kempf -United and Industries Monument Corporation (w/o lab attachment)
S. Alan Lazar -Avnet, Inc. (w/o lab attachment)
Steve Earp -Smith Helms Muliss & Moore (w/o lab attachment)
David Mattison -NCDENR Superfund
Ken Lucas, RPM -USEPA Superfund
Nanjun Shelly, P.E. -ENSR
File
S:\PUBSIPAOJECnC\ChannelMaster\Ouarterly IUReports\2008\Nov 2008\IUR Letter Nov 2008.doc
INDUSTRIAL USER REPORTING FORM
I.U. PERMIT NO:_-'G=0,,_.,0'--'1 _____ DISCHARGE NO: ___ ...,0=0_,_1 _____ _
MONTHS: _.!.,.A,,,u .... g,,,us,,.t'-', S""e"'p,cte,,,,m-"b,,,ee.,.r...,a,,_n,,,d...,O"'c"'to,,,b,,,e,,_r ____ YEAR: ----~2=0~0=8 __ _
LU. NAME: JFD Electronics/Channel Master CLASS: COUNTY: Granville
OPERATOR IN RESPONSIBLE CHARGE (ORC): ENSR Consulting & Engineering (NC), Inc.
LABORATORY PERFORMING ANALYSIS: Test America (Formerly STL-Savannah)
PERSON(S) COLLECTING SAMPLES: Joe Ladd (ENSR)
CHECK BLOCK IF ORC HAS CHANGED 0
SEND REPORT TO: City Engineer
City of Oxford
P.O. Box 1307
Oxford, NC 27565
Facility Status: (Please check one of the following)
All monthly averages and/or other limitations do meet permit monitoring requirements. ~
(Compliant)
All monthly averages and/or other limitations do not meet permit monitoring requirements. D
(Noncompliant)
If the facility is noncompliant, please comment on corrective actions being taken in respect to
equipment, operation, maintenance, etc. and a time table for improvements to be made.
(Attach additional sheets if necessary)
I certify that this Report is accurate and
complete to the best of my knowledge: /_
~. ,: )f'i /I-S"-2ocl8
=L.Jl.4,.6..,th,e..l..._:_:,1-<r.L!,~=_:_:.1-1':!'.Jl" -----------
Signature of Permittee Representa · e Date:
William H. Doucette, Jr., Ph.D.
1\p,.l,1wro,e1\c\i:hlrn!rMS1r~rlr,npon,l]IIIIB\ro,1il08\u-kmocl?Ollilrh:
TABLE 1. GROU~DWATER REMEDIATION SYSTEM DISCHARGE MONITORING REPORT, CITY OF OXFORD, NORTH CAROLINA
I.U. PERMIT NO:
DISCHARGE NO:
MONTHS:
YEAR:
I.LI. NAME:
COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC):
LABORATORY PERFORMING ANALYSIS:
PERSON(S) COLLECTING SAMPLES:
PARAMETER
Daily Average Flow (MGO)
Tetrachloro'ethylene
1,1-Dichloroethane
cis-1,2 Dichloroelhene
Chlorobenzene
Toluene
1, 1-0ichloroethylene
trans-1,2 Dichloroethylene
Trichloroethene
Vinyl Chloride
Cyanide (total)
pH
Temperature
Monitoring requirement only.
MGD Million Gallons per day.
µg/L Micrograms per liter.
mg/L Milligrams per Iller.
SU Standard Units ~c Degrees Centigrade.
G001
001
August, September and October
2008
JFD Electronics/Channel Master NPL Site
Granville
ENSR Consulting and Engineering (NC), Inc
TestAmerica
Joe Ladd (ENSR)
PERMIT LIMITS
Daily Maximum
0.040
0.05
5.0 to 10.0
40
UNITS
MGD
µgtl
µgll
µg/L
µg/L
µg/L
µg/L
µgll
µgll
µg/l
mgll
SU
•c
SAMPLE
TYPE
Meter
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
< Compound was not detected above the quantitat1on limit
NS Not sampled
G 1Env\JFDCHANN\NC0202.1701C,ty ol Oxlon:I\IURTable Nov 2008.xls\Table 1110/'2812008
LAB
METHOD
Field
8260
8260
8260
8260
8260
8260
8260
8260
8260
335.2
Field
Field
QUARTERLY MEASUREMENT
DATES
8/27/2008 9/15/2008 10115/2008
0.019 0.016 0.013
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS <1.0
NS NS 0.012
8.63 8.47 8.36
20.2 21.8 21.3
Test America
THE LEADER !N ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 680-41442-1
Job Description: Channel Master
For:
ENSR International
7041 Old Wake Forest Road
Suite 103
Raleigh, NC 27616
Attention: Mr. Gerald Hornaday
Kathryn Smith
Project Manager I
[e-mail]
10/28/2008
Ai:,proved tor raloase
Kathryn sm,th
ProJect Manager I
10/21112008 3.59 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This report
may not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to the
person who signed this report. ·
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; CA: 03217CA; CO; CT:
PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KY UST; LA
DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; Ml: 9925; MS; NFESC: 249; NV: GA00006;
NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244; SC:
98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WV
DHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel [phone] Fax [phone] www testamericainc.com
Pagel of 14
Client: ENSR International
Description
Matrix Water
Volatile Organic Compounds (GC/MS)
Purge and Trap
Cyanide, Total
Distillation, Cyanide
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
METHOD SUMMARY
Lab Location
TAL SAV
TAL SAV
TAL SAV
TAL SAV
Method
SW846 8260B
MCAWW335.4
Job Number: 680-41442-1
Preparation Method
SWB46 5030B
OistiU/CN
MCAWW = "Methods For Chemical Analysts Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Savannah
Page 2 of 14
Client: ENSR International
Method
SW846 82608
MCAWW 335.4
TestAmerica Savannah
METHOD/ ANALYST SUMMARY
Analyst
Sokolin, Eleina
McDonald, Debbie
Page 3 of 14
Job Number: 680-41442-1
Analyst ID
ES
DM
Client: ENSR International
Lab Sample ID
680-41442-1
680-41442-2
TestAmerica Savannah
Client Sample ID
OCT EFFLUENT
TRIP BLANK
SAMPLE SUMMARY
Client Matrix
Water
Water
Page 4 of 14
Date/Time
Sampled
10/15/2008 1550
1011 5/2008 0000
Job Number: 680-41442-1
Date/Time
Received
10117/2008 0907
10/17/2008 0907
Client: ENSR International
Client Sample ID:
Lab Sample ID:
Client Matrix:
OCT EFFLUENT
680-41442-1
Water
Method: 82608
Preparation: 50308
Dilution: 1.0
Date Analyzed: 10/21/2008
Date Prepared: 10/21/2008
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-0ichloroethene
1,2-0ichloropropane
Ethylbenzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-penlanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-0ichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1704
1704
82608 Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-120524
Result (ug/L) Qualifier
25 u
1.0 u
1.0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
10 u
5.0 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
2.0 u
%Rec
91
97
104
Page 5 of 14
Analytical Data
Job Number: 680-41442-1
Date Sampled·
Date Received:
10/15/2008. 1550
10/17/2008 0907
Instrument 1D:
Lab File ID:
GC/MS Volatiles - A
a295.d
Initial WeighWo!ume: 5 ml
5 ml Final WeighWolume:
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: ENSR International
Client Sample ID:
Lab Sample ID·
Client Matrix:
TRIP BLANK
680-41442-2
Water
Method: 8260B
Preparation: 5030B
Dilution: 1.0
Date Analyzed: 10/21/2008
Date Prepared: 10/21/2008
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
TestAmerica Savannah
1724
1724
8260B Volatile Organic Compounds (GC/MS)
Analysis Batch: 680-120524
Result (ug/l) Qualifier
25 u
1.0 u
1.0 u
1.0 u
2.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
10 u
5.0 u
10 u
10 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
1.0 u
2.0 u
%Rec
92
97
102
Page 6 of 14
Analytical Data
Job Number: 680-41442-1
Date Sampled: 10/15/2008 0000
10/17/2008 0907 Date Received:
Instrument ID:
Lab File ID:
GC/MS Volatiles - A
a296.d
Initial WeightNolume:
Final WeightNolume:
5 ml
5 ml
Rl
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: ENSR International
Client Sample ID:
Lab Sample ID:
Client Matrix:
Analyte
Cyanide, Total
OCT EFFLUENT
680-41442-1
Water
Anly Batch:
Result
· 0.012
680-120779
Prep Batch: 680-120486
TestAmerica Savannah
General Chemistry
Oual Units
mg/L
Date Analyzed 10/24/2008 1215
Date Prepared: 10/22/2008 0800
Page 7 of 14
Analytical Data
Job Number: 680-41442-1
Date Sampled:
Date Received:
RL
0.0050
10/15/2008 1550
10/17/2008 0907
Oil Method
1.0 335.4
DATA REPORTING QUALIFIERS
Client: ENSR International Job Number: 680-41442-1
Lab Section Qualifier Description
GC/MS VOA
u Indicates the analyte was analyzed for but not detected.
General Chemistry
u Indicates the analyte was analyzed for but not detected.
TestAmerica Savannah
Page 8 of 14
Client: ENSR International
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID
680-41442-1
680-41442-2
MB 680-120524/5
LCS 680-120524/7
LCSD 680-120524/8
Surrogate
Client Sample ID
OCT EFFLUENT
TRIP BLANK
BFB = 4~Bromofluorobenzene
OBFM = Oibromofluoromethane
TOL = Toluene-dB (Surr)
TestAmerica Savannah
BFB
%Rec
91
92
91
88
92
DBFM TOL
%Rec %Rec
97 104
97 102
100 102
95 108
93 107
Acceptance Limits
75-120
75-121
75-120
Page 9 of 14
Quality Control Results
Job Number: 680-41442-1
Client: ENSR lnternat,onal
Method Blank -Batch: 680-120524
Lab Sample ID: MB 680-12052415 Analysis Batch: 680-120524
Client Matrix: Water Prep Batch: NIA
Dilution: 1.0 Units: ug/L
Date Analyzed: 10/2112008 1136
Date Prepared: 10/21/2008 1136
Analyte Result Qua!
Acetone 25 u
Benzene 1.0 u
Bromoform 1.0 u
Bromomethane 1.0 u
Carbon disulfide 2.0 u
Carbon tetrachloride 1.0 u
Chlorobenzene 1.0 u
Chlorodibromomethane 1.0 u
Chloroethane 1.0 u
Chloroform 1.0 u
Chloromethane 1.0 u
cis-1,2-Dichloroethene 1.0 u
cis-1,3-Dichloropropene 1.0 u
Oichlorobromomethane 1.0 u
1, 1-Dichloroethane 1.0 u
1,2-Dichtoroethane 1.0 u
1, 1-0ichloroethene 1.0 u
1,2-Dichloropropane 1.0 u
EthyJbenzene 1.0 u
2-Hexanone 10 u
Methylene Chloride 5.0 u
2-Butanone (MEK) 10 u
4-Methyl-2-pentanone (MIBK) 10 u
Styrene 1.0 u
1, 1,2,2· T etrachloroethane 1.0 u
Tetrachloroethene 1.0 u
Toluene 1.0 u
trans-1,2-Dichloroethene 1.0 u
trans-1,3-Dichloropropene 1.0 u
1, 1, 1-Trichloroethane 1.0 u
1, 1,2-Trichloroethane 1.0 u
Trichloroethene 1.0 u
Vinyl chloride 1.0 u
Xy!enes, Total 2.0 u
Surrogate % Rec
4-Bromofluorobenzene 91
Dibromofluoromethane 100
Toluene-dB (Surr) 102
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 10 of 14
Quality Control Results
Job Number: 680-41442-1
Method: 8260B
Preparation: 5030B
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq094.d
Initial WeighUVolume: 5 ml
Final WeighWolume: 5 ml
RL
25
1.0
1.0
1.0
2.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
10
5.0
10
10
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
Acceptance Limits
75 -120
75 -121
75 -120
Client: ENSR International
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-120524
LCS Lab Sample ID: LCS 680-120524/7
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/21/2008 1203
Date Prepared: 10/21/2008 1203
···-·-
LCSD Lab Sample ID: LCSD 680-120524/8
Client Matrix: Water
Dilution: 1.0
Date Analyzed: 10/21/2008 1222
Date Prepared: 10/21/2008 1222
Analyte
Acetone
Benzene
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dichlorobromomethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
1,2-Dichloropropane
Ethyl benzene
2-Hexanone
Methylene Chloride
2-Butanone (MEK)
4-Methyl-2-pentanone (MIBK)
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-0ichloropropene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Analysis Batch: 680-120524
Prep Batch: N/A
Units: ug/L
Analysis Batch: 680-120524
Prep Batch: N/A
Units: ug/L
% Rec.
LCS LCSD Limit
86 92 17 -175
102 103 77 -119
69 73 62 -133
150 151 12 -184
94 89 55 -131
89 89 71 -135
98 99 85-116
85 90 75 -133
87 85 40 -165
97 94 82 -120
72 69 48 -142
90 86 69 -134
105 106 76 -126
100 102 78 -127
85 81 74 -127
108 111 66 -132
80 76 62 -141
109 109 73 -124
97 98 86 -116
90 98 34 -161
93 89 70 -125
93 95 33 -157
99 107 40 -151
96 95 82 -122
93 98 69 -129
99 99 76 -126
105 108 81 -117
89 86 72 -131
103 106 73 -128
97 98 76 -127
105 109 75 -121
110 109 84-115
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 11 of 14
RPD
7
0
6
1
6
0
5
3
3
5
5
1
2
4
2
5
0
1
9
4
2
8
1
6
0
2
3
4
1
3
Quality Control Results.
Job Number: 680-41442-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles - A
aq095.d
Initial Weight/Volume:
Final Weight/Volume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq096.d
Initial WeighVVolume:
Final Weight/Volume:
RPO Limit
50
30
30
50
30
30
30
30
50
30
50
30
. 30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
5 ml
5 ml
LCS Qual LCSD Qual
Client: ENSR International
Lab Control Spike/
Lab Control Spike Duplicate Recovery Report -Batch: 680-120524
LCS Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
LCSD Lab Sample ID:
Client Matrix:
Dilution:
Date Analyzed:
Date Prepared:
Analyte
Vinyl chloride
Xylenes, Total
LCS 680-120524/7
Water
1.0
10/21/2008 1203
10/21/2008 1203
LCSD 680-120524/8
Water
1.0
10/21/2008 1222
10/21/2008 1222
Analysis Batch: 680-120524
Prep Batch: N/ A
Units: ug/L
Analysis Batch: 680-120524
Prep Batch: NIA
Units: ug/L
% Rec.
LCS LCSD Limit
82 79 59 -144
95 94 84 -118
RPO
4
Surrogate LCS % Rec LCSO % Rec
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-dB (Surr)
88
95
108
92
93
107
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 12 of 14
Quality Control Results
Job Number: 680-41442-1
Method: 8260B
Preparation: 5030B
Instrument ID:
Lab File ID:
GC/MS Volatiles - A
aq095.d
Initial WeightNolume:
Final WeighWolume:
5 ml
5 ml
Instrument ID: GC/MS Volatiles -A
Lab File ID: aq096.d
Initial WeighWolume:
Final WeighWolume:
5 ml
5 ml
RPO Limit LCS Qual
50
30
Acceptance Limits
75 -120
75 -121
75 -120
LCSD Qual
Client: ENSR International
Method Blank -Batch: 680-120486
Lab Sample ID: MB 680-120486/1-A
Client Matrix· Water
Dilution: 1.0
Date Analyzed: 10/24/2008 1215
Date Prepared: 10/22/2008 0800
Analy1e
Cyanide, Total
Lab Control Spike/
Analysis Batch: 680-120779
Prep Batch: 680-120486
Units: mg/L
Result
0.0050
Lab Control Spike Duplicate Recovery Report -Batch: 680-120486
LCS Lab Sample ID: LCS 680-120486/2-A
Client Matrix: Water
Dilution:
Date Analyzed:
Date Prepared:
1.0
10/24/2008 1215
10/22/2008 0800
LCSD Lab Sample ID: LCSD 680-120486/3-A
Client Matrix: Water
Dilution: 1.0
Date Analyzed:
Date Prepared:
Analyte
Cyanide, Total
10/24/2008 1215
10/22/2008 0800
Analysis Batch: 680-120779
Prep Batch: 680-120486
Un.its: mg/L
Analysis Batch: 680-120779
Prep Batch: 680-120486
Units: mg/L
% Rec.
LCS LCSD Limit
92 90 90-110
Oual
u
Calculations are performed before rounding to avoid round-off errors in calculated results.
TestAmerica Savannah Page 13 of 14
RPO
2
Quality Control Results
Job Number: 680-41442-1
Method: 335.4
Preparation: Distill/CN
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume: 50 ml
Final WeightNolume: 50 ml
Method: 335.4
Preparation: Distill/CN
RL
0.0050
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume:
Final WeightNolume:
50 ml
50 ml
Instrument ID: QuickChem 8000
Lab File ID: N/A
Initial WeighWolume:
Final WeighWolume:
50 ml
50 ml
RPO Limit LCS Qual LCSD Qual
20
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ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD
Serial Number 7 8 5 4 8
c=~S'rl Savannah
S l 02 LcRoche Avenue
Savannah. GA 3 l 4(M
Websire: ww\v.st~inc.com
P~1one: 1912) 354-7858
fax: i912I 352-0165
Phone:
Fax:
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