NCD122263825_20000721_JFD Electronics - Channel Master_FRBCERCLA SAP QAPP_Soil Sampling Results-OCR

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ARCADIS GERAGHTY & MILLER
Ms. Samantha Urquhart-Foster
U.S. Environmental Protection Agency
61 Forsyth Street, SW
Atlanta, Georgia 30303-8960
Subject:
r-cEIVED
AUG -12000
SUPERFUND SECTION
Soil Sampling Results,. JFD Electronics/Channel Master NPL Site,
Oxford, North Carolina.
ARCADIS Geraghty & Miller Project No. NC0202.0210.00001
Dear Ms. Urquhart-Foster:
ARCADIS Geraghty & Miller of North Carolina, Inc., (ARCADIS Geraghty &
Miller) collected surficial soil samples at the JFD Electronics/Channel Master site to
further delineate impacted areas slated for excavation and treatment. The soil
sampling was performed in two phases due to delays in obtaining access agreements
from Norfolk Southern Corporation (NSC). The first phase consisted of sampling
on-site grids. Results of these samples were summarized in a letter dated June 30,
2000. The second phase consisted of collecting soil samples from grids in the NSC
right-of-way. This report summarizes the procedures used to collect the soil samples
and discusses the analytical results for both on-site and off-site samples. This letter
also addresses comments from Mr. David Mattison of the North Carolina
Department of Environment and Natural Resources (NCDENR). Finally,
recommendations have been made concerning the proposed remedial action of the
surficial soils.
SUMMARY OF FIELD ACTIVITIES AND RESULTS
The soil sampling activities were conducted by ARCADIS Geraghty & Miller
personnel on May 24 and 25, and July 6, 2000. These activities included collecting
and compositing surficial soil samples from 22 square grids at three different depth
intervals. The following sections describe the field activities and summarize the
sampling program.
Field Activities
The soil samples were collected in accordance with the procedures described in the
Construction Quality Assurance (CQA) Plan (ARCADIS Geraghty and Miller,
March 2000). The grid system was established by an ARCADIS Geraghty & Miller
survey crew. A detailed description of these locations is presented as Figure I. A
total of twenty-two 50 foot by 50 foot grids were staked at each node and in the
center of each grid. Due to access restrictions and site features several grids were
combined as shown on Figure I. The portions of grids I and 3 on the Avnet
property were combined, sampled, and labeled grid I. The remaining portions of
these two grids on the railroad property were combined, sampled, and labeled grid 3.
The portions of grids 12 and 15 north of the railroad were combined, sampled, and
labeled grid 12. The remaining portions of these two grids, however, were not
Our ref.:
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ARCAOIS Geraghty & Miller of
North Carolina, Inc.
2301 Rexwoods Drive
Suite 102
Raleigh
North Carolina 27607
Tel [phone]
Fax [phone]
ENVIRONMENTAL
Raleigh, NC
21 July 2000
Contact:
William H. Doucette, Jr.,
Ph.D.,P.G.
Extension:
256
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ARCADIS GERAGHTY&MILLER
sampled because they lie beneath the rip-rap covered embankment upon which the
railroad tracks are located. Therefore, a total of21 grid composites were sampled.
Grid 21 was sampled on May 25 and July 6, 2000. Based on the June 15, 2000
meeting with the United States Environmental Protection Agency (USEPA) and
NCDENR, grid 21 was resampled on July 6, 2000 to verify whether metals and
cyanide were present at concentrations above RLs at this location.
Shallow soil samples were collected from grid locations at three depth intervals:
0 to 0.5, 0.5 to I, and I to 1.5 feet below land surface (ft bis). A clean dedicated
stainless steel hand-held auger was used to collect the soil subsamples at each depth
interval within each of the grids. The procedures followed are described below:
I. Leaves, gravel, grass, rocks, and surface debris were cleared from each sampling
area;
2. The bucket auger was advanced to the desired shallow depth interval of0 to 0.5
ft bis at the grid center point;
3. The soil was removed from the terminal ends to prevent potential cross-
contamination and the soil sample was placed in a clean stainless steel bowl;
4. Steps 2 and 3 were repeated for the grid intersection/node soil subsample
locations. Uniform soil volumes were collected from each of the soil subsample
locations;
5. The composite soil sample was thoroughly mixed after all subsample locations
had·been sampled. Typical grids consisted of 5 subsamples, with the exception
of locations where a building or fence prevented collection of a subsample at a
grid node. Table I indicates the number of subsamples obtained at each grid;
6. The composite soil samples were placed in clean and labeled laboratory-
provided sample containers for analysis of hexavalent chromium (USEP A
Method 7196), and antimony and nickel (USEPA Method 6010). Composite
soil samples collected from grids 6, 8, 9, 13, 16, 18, 21, and 22 also were
analyzed for total and amenable cyanide (USEPA Methods 9013/9010); and
7. The intermediate depth, 0.5 to I ft bis, and deeper depth, I to 1.5 ft bis, interval
soil samples also were collected following the procedures outlined in Steps 2
through 6. These composite soil samples were collected with the use of clean
dedicated stainless steel hand-held bucket augers.
8. The equipment used was dedicated to the three depth intervals sampled and was
cleaned in accordance with the procedures described in the CQA Plan between
the different grid locations. Equipment rinsate blank samples EB-0 I through
EB-09 also were collected to verify that the equipment was properly cleaned.
Once collected, the composite soil samples were packed on ice in coolers and
shipped via express courier to STL Savannah Laboratories, Savannah, Georgia, for
analysis. Chain-of-custody forms were included to maintain a complete record of all
personnel that had contact with the samples. Copies of the chain-of-custody records
are enclosed with the laboratory analytical reports in Attachment I.
STL Savannah Laboratories initially was instructed to perform Level II analysis of
all composite samples collected from the shallow (0 to 0.5 ft bis) and intermediate
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ARCAD!S GERAGHTY&MILLER
(0.5 to I ft bis) depths. The deeper depth I to 1.5 ft bis interval composite samples
were held pending the analytical results of the overlying composite samples
collected. Based on these data, ARCADIS Geraghty & Miller instructed STL
Savannah Laboratories to perform Level II analysis on the deeper composite
samples (I to 1.5 ft bis) at grid locations where the intermediate depth (0.5 to I ft
bis) composite samples exceeded remediation levels (RLs). A complete set of
composite samples representing all three depths collected at each grid also was sent
to STL Savannah Laboratories for CLP confirmatory analysis. These samples were
held pending the Level II results. Twenty-five percent of soil samples with
constituents of concern below RLs were selected for CLP analysis. The CLP data
for the selected samples below remediation goals will be provided when all CLP
data are available.
Results
The analytical results are summarized in Table I and the laboratory reports are
included as Attachment I. The RLs for the constituents of concern in milligrams per
kilogram on a dry weight basis (mg/kg.dw), are as follows:
Hexavalent chromium
Antimony
Nickel
Total cyanide
Amenable cyanide
310
25
1,100
590
30
Grids 8, 9, 11, 14, 18, and 22 contained soils impacted above RLs. The analytical
data for these six grids are summarized in Figure I.
Nickel was detected in grid 8 within the O to 0.5 ft bis and 0.5 to I ft bis intervals at
4,300 mg/kg.dw and 3,600 mg/kg.dw, respectively. Total cyanide was detected in
the 0.5 to I ft bis interval at 590 mg/kg.dw and amenable cyanide was estimated in
the Oto 0.5 ft bis interval at 64 mg/kg.dw. No other constituents were detected
above RLs at these two depth intervals and no constituents were detected above
remedial levels within the I to 1.5 ft bis depth interval in grid 8.
Within the O to 0.5 ft bis depth interval in grid 9, nickel was estimated at 1,500
mg/kg.dw. Amenable cyanide was detected in the 0.5 to I ft bis depth interval at 30
mg/kg.dw. Due to an oversight, the composite sample collected from the I to 1.5 ft
bis depth interval was not analyzed. Therefore, it is assumed that the soils at this
depth interval exceed the RLs.
Within the 0.5 to I ft bis depth interval in grid 11, nickel was estimated at 1,400
mg/kg.dw. No other constituents were detected above RLs within that depth interval
in grid 11. Additionally, no constituents were detected above remedial levels within
the O to 0.5 and I to 1.5 ft bis depth intervals within this grid .
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AR CAD IS GERAGHTY & MILLER
Within the 0.5 to 1 ft bls depth interval in grid 14, nickel was detected at 1,200
mg/kg.dw. No other constituents were detected above RLs within that depth interval
in grid 14. Additionally, no constituents were detected above RLs within the Oto
0.5 and 1 to 1.5 ft bls depth intervals within this grid.
Nickel was estimated in grid 18 within the Oto 0.5 ft bls depth interval at 1,600
mg/kg.dw and detected in the 0.5 to 1 ft bls and 1 to 1.5 ft bls depth intervals at
1,800 mg/kg.dw and 1,100 mg/kg.dw, respectively. Total cyanide was detected in
the 0.5 to I ft bls depth interval at 620 mg/kg.dw and amenable cyanide was
detected in the I to 1.5 ft bls depth interval at 210 mg/kg.dw. No other constituents
were detected above RLs within this grid.
Nickel was detected in grid 22 within the Oto 0.5 foot bls depth interval at 1,700
mg/kg.dw. No other constituents were detected above RLs within that depth interval
and no constituents were detected above remedial levels within the 0.5 to I ft bls
depth interval in grid 22.
Conclusions
Based on the analytical result presented above, ARCADJS Geraghty and Miller
identified only 6 surficial soil grids to be excavated for treatment and disposal
during the implementation of the soil/sludge remedial action. The total volume of
fOil associated with these grids is estimated to be between 600 and 700 cubic yards.
Therefore, as stated in the Explanation of Significant Difference (ESD), the most
cost effective remedy for these soils is off-site treatment and disposal to a permitted
facility for the following grids:
• Within grid 8, soil should be excavated for treatment to a depth of I ft bis.
• Soil should be excavated for treatment to a depth of 1.5 ft bls within grid 9.
• Within grid 11, soil should be excavated for treatment to a depth of I ft bis.
• Soil should be excavated for treatment to a depth of I ft bls within grid 14.
• Soil should be excavated for treatment to a depth of at least 1.5 ft bis within
grid 18. Grid 18 overlays the sludge drying bed (SOB) area of excavation.
Therefore, soils at a depth greater than I ft bis may be removed during SOB
excavation activities.
• Finally, soil should be excavated for treatment to a depth of0.5 ft bis within
grid 22.
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ARCADIS GERAGHTY& MILLER
If you have any questions or need additional information, please contact us at (919) 782-55 I I.
Sincerely,
ARCADIS Geraghty & Miller of North Carolina, Inc.
V'--C. -st ~=yr,"V
Jeffrey S. Hall, E.I.
Staff Engineer
~~~~t~
Associate Vice President/ .
Project Coordinator for the Responsible Party
/srd
Attachments
Coplesc ·Brian Kempner, The UNIMAX Corporation
S. Alan Lazar, AVNET, Inc.
Our ref.:
David Mattison, NCDENR
Nan jun Shetty, ARCADIS Geraghty & Miller
Michelle Pahr, ARCADIS Geraghty & Miller
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TABLES
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AR CAD IS GERAGHTY & MILLER
Table I. Summary o~ Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID:
Sample ID: GI (0 -0.5)
STL Savannah Laboratory ID: 03436-1
Depth Interval (ft bis): 0 -0.5
Number of Subsamples: 5
Date Sampled: 5/25/00
R'erriedi.itiifa·.
Constituents (mg/kg.dw) ~::~~:n~~V~iWtt
Hexavalent Chromium (USEPA 7196A) 0.54 ,
Antimony (USEPA 6010) <4.1 ·
Nickel (USEPA 6010) 35.
Total Cyanide (USEPA 9010) NS
Amenable Cyanide (USEPA 9010) NS
ft bis
NA
NS
mgikg.dw
< I -~f'.~!L"i; _ _t:·Lt,t;:~; I
Feet below land surface.
Not analyzed.
Not sampled.
Milligrams per kilogram on a dry weight basis.
Constituent was not detected above the quantitation limit.
Cons1i1uent Concentration exceeds Remediation Level.
Grid I
GI (0.5 -I) GI (I -1.5) G2 (0 -0.5)
03436-2 03382-1
0.5 - I I -1.5 0-0.5
5 5 5
5/25100 5125100 5/24/00
0.6 · NA 0.63 ·
<2.0 • NA < 2.3.
39 , NA 1I0J11
•
NS NS NS
NS NS NS
90 · NA 86
J" ," Constituent concentration is qualified as estinuited because the MS/1\,tSD relative percent difference was outside QC limits.
Constituent concentration is qualiffod as estimated because 1he field replicate sampl~ criteria were not met
g:\env\j fdchann\nc202.21 O\ Tables\grid _samples_ new I .xis\ 7 / 19/00
Grid 2
G2 (0.5 -I) G2 (I -\.5) G3 (0 -0.5)
03382-2 04471-1
0.5 - I . I -1.5 0 -0.5
5 5 5
5/24/00 5/24/00 7/6/00
0.55 · NA <0.45 ·
< 2.3 · NA <2.1.
1311 NA 190.
NS NS NS
NS NS NS
88 · NA 88 ·
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Grid 3
G3 (0.5 -I) G3 (I -1.5)
04471-2
0.5 - I I -1.5
5 5
7/6/00 7/6/00
<0.43 • NA
<2.2 · NA
9.8 NA
NS NS
NS NS
92 · NA
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ARCADIS GERAGHTY&MILLER
Table I. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID:
Sample TD: G4 (0 -0.5)
STL Savannah Laboratory ID: 03382-3
Depth Interval (f\ bis): 0-0.5
Number of Subsamples: 5
Date Sampled: 5/24/00
Re"fue"diiitiOri
Constituents (mg/kg.dw) 2~i~f~te·~e1t: ,i;
Hexavalent Chromium (USEPA 7196A) < 0.49 ·
Antimony (USEPA 6010) < 2.2
Nickel (US EPA 60 I 0) 94J"
ft bis
NA
NS
mglkg.dw
< I,,,'!' c-.cc."' :·H
Feet below land surface.
Not analy-l.Cd.
Not sampled
Milligrams per kilogram on a dry weight basis.
Conslituent was not detecced above the quantitation limit.
Constituent Concentration e~ceeds Remediation Level.
Grid4
G4 (0.5 -1) G4 (1 -1.5) G5 (0 -0.5)
03382-4 03382-5
0.5 -I I -1.5 0-0.5
5 5 5
5/24/00 5/24/00 5/24/00
0.52 · NA <0.47 ·
< 2.4. NA < 2.4 .
45 NA 490Jll'
NS NS NS
NS NS NS
85 · NA 85
J"
J"
Constituent concentra1ion is qualified as estimated because the MS/MSD relative percent difference was outside QC limits.
Constituent concentration is qualified as estimated because the field replicate sample criteria were not mel
g:\env\jfdchann\nc202 .210\ T ables\grid _samples_ new l .. ds\ 7 /19/00
Grid 5
G5 (0.5 -I) G5(1-l.5) G6 (0 -0.5)
03382-6 04471-7
0.5 -I I -1.5 0 -0.5
5 5 5
5/24/00 5/24/00 7/6/00
< 0.46 · NA <0.43 ·
< 2.3 NA <2.0 .
180 NA 88 ·
NS NS 9.0 ·
NS NS <I.I
87 NA 91
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Grid 6
G6 (0.5 -I) G6(1-l.5)
04471-8
0.5 -1 I -1.5
5 5
7/6/00 7/6/00
<0.43 · NA
<2.2 -NA
74 NA
14 · NA
<I.I. NA
91 NA
-- - -- - -- -- -
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ARCADIS GERAGHTY&MILLER
Table I. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid JD:
Sample ID:
STL Savannah Laboratory ID:
Depth Interval (ft bis):
Number of Subsamples:
Constituents (mg/kg.dw)
Hexavalent Chromium (USEPA 7196A)
Antimony (USEPA 6010)
Nickel (USEPA 6010)
Total Cyanide (USEPA 9010)
Amenable Cyanide (USEPA 90 I 0)
Percent Solids
ft bis
NA
Feet below land surface.
Not analy-.1:ed.
Not sampled.
Date Sampled:
Reffiedi.itiOil ii)Htt~i'.elillh
G7 (0 -0.5)
03382-7
0 -0.5
5
5/24/00
0.50 ·
< 2.5 ·
8IJ110
NS
NS
80 ·
NS
mg/kg.dw
< I; ;¾E8';~\~i~'¾tf; I
Milligrams per kilogram on a dry weight basis.
Constituent was no! de1ected above the quantitation limit
Cons1i1uent Concentration exceeds Remediation Level.
Grid 7
G7 (0.5 -!)
03382-8
0.5 -I
5
5/24/00
0.46 ·
< 2.3·
80
NS
NS
88 ·
G7 (I -1.5)
I -1.5
5
5/24/00
NA
NA
NA
NS
NS
NA
G8 (0 -0.5)
04471-9
0 -0.5
5
7/6/00
<0.48·
19 ·
:·~:tJf:: 590_i;:!,'.-'f'
,'·;;¥ 64J,,0:
82 ·
1"
J"
Constituent concentration is qualified as estimated because the MS/MSD relative percent difference was outside QC limits.
Constituent concentration is qualified as estimated because the tield replicate samplt: criteria were not mcL
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Grid 8
G8 (0.5 -I)
04471-10
0.5 -I
5
7/6/00
110 '
20J~G
82 ·
G8(1-l.5)
004471A-2
I -1.5
5
7/6/00
<0.45 ·
<2.3 ·
510 ,
88 ·
G9 (0 -0.5)
03382-9/51
0-0.5
5
5/24/00
0.62
<4.9-·
Grid 9
G9 (0.5 -I)
03382-10/52
0.5 -I
5
5/24/00
0.65 ·
< 2.3 ·
640
500 · 200 ·
21 . l·e1:• 30,,,,.~ ,1
82 , 86 ·
G9 (I -1.5)
I -1.5
5
5/24/00
NA
NA
NA
NA
NA
NA
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ARCADIS GERAGHTY&MILLER
Table 1. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID: Grid 10 Grid 11
Sample ID: GI0 (0 -0.5) G\0 (0.5 -I) G\0(1-1.5) GI I (0 -0.5) GI I (0.5 -I)
STL Savannah Laboratory IO: 03382-15
Depth Interval (ft bis): 0 -0.5
Number of Subsamples: 5
Date Sampled: 5/24/00
ReiiieOi3tiOri~
Constituents {mg/kg.dw) !~;/E~;~~i:iftff
Hexavalent Chromium (USEPA 7196A) 0.55 ·
Antimony (USEPA 6010) ;'.'.-;-,;a;;'"·'I < 2.4 •
Nickel (USEPA 6010) l~/;~'i'[,~J~ 340J" •
Total Cyanide (USEPA 9010) NS
Amenable Cyanide (USEPA 9010) )I@t~~l/l!I NS
ft bis
NA
NS
mgtl.:g.dw
<
Feet below land surface.
Not analyzed
Not sampled.
Milligrams per kilogram on a dry weight basis.
Constituent was not detected above the quantitation limiL
Constituent Concentration exceeds Remediation Level.
03382-16 03382-13
0.5 - I I -1.5 0 -0.5
5 5 5
5/24/00 5/24/00 5/24/00
< 0.46 · NA < 0.47 ·
<2.1 NA < 2.3.
91 NA 600J11 , I
NS NS NS
NS NS NS
87 NA 86
Conslituent concentration is qlllllified as estimated because the MS/MSD relative percent difference was outside QC limits.
Constituent concentration is qualified as estimated because the field replicate sample criteria were not met.
•
g:\env\j fdchann\nc202 .2 I 0\ Tables\b>rid _samples_ new I . :it ls\ 7 / 19/00
03382-14
0.5 - I
5
5/24/00
< 0.47 ·
< 2.4·
:1;400Jf.:;;I
NS
NS
85
Gil (1-1.5) G\2 (0-0.5)
033828-1 04471-3
I -1.5 0 -0.5
5 5
5/24/00 7/6/00
<0.46 · <0.44
<2.3 · <2.2
77. 30
NS NS
NS NS
87, 90
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Grid 12
G\2(0.5-1) G\2 (1 -1.5)
04471-4
0.5 - 1 1 -1.5
5 5
7/6/00 7/6/00
<0.43 · NA
<2.2 · NA
14 NA
NS NS
NS NS
92 NA
- - - -- -- - -
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ARCADIS GERAGHTY&MILLER
Table l. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID:
Sample I D:
STL Savannah Laboratory I D:
Depth Interval (ft bl s):
Number
Constituents (mg/kg.dw)
Hexavalent Chromium (USEPA 7196A)
Antimony (USEP A 6010)
Nickel (USEPA 6010)
Total Cyanide (USEPA 9010)
Amenable Cyanide (US EPA 90 I 0)
Percent Solids
ft bis
NA
Feet below land surface.
Not analyzed.
Not sampled.
of Subsampl es:
Date Sampl ed:
Remediation J~l~IJV~i fi,J}
Gl3 (0 -0.5)
03382-17/44
0 -0.5
5
5/24/00
< 0.47 ·
< 2.4 •
570J11
90 '
2.8 ·
85 ,
NS
mg/kg.dw
<
Milligrams per kilogram on a dry weight basis.
Constituent was not detected above the quantitation limit.
Constituent Concentration e)(Ceeds Remediation level.
Grid 13 Grid 14
G13(0.5-I) Gl3(1-l.5) Gl4 (0 -0.5) Gl4 (0.5 -I)
03382-18/45 04471-5 04471-6
0.5 -I I -1.5 0 -0.5 0.5 -I
5 5 5 5
5/24/00 5/24/00 7/6/00 7/6/00
< 0.47 · NA <0.48 <0.47 •
<2.1 NA 4.9 10
580 NA 450 · 1~~}f:l_;700t;~ I
110 NA NS NS
13 NA NS NS
85 · NA 82 85
1 •.1•:; ,-,,•n,;:· ··,==:I
1"
1"
Constituent concen1ratio11 is qualified as estimated because the MSll\.-tSD relative percent difference was outside QC limits.
Consti1uent concentraticm is (1ualified as estimated because the field replicate sample criteri<1 were not met.
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Grid 15 (Combined w/ Grid 12)
Gl4 (I -1.5) Gl5 (0 -0.5) · Gl5 (0.5 -1) Gl5 (I -1.5)
04471A-I.
I -1.5 0 -0.5 -0.5 -·! 1 -1.5 ·
5 .. 7/6/00 7/6/00 7/6100 7/6/00 ·
<0.47 •
<2.4
290
NS
NS
85
-
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l!!!!!l!!I 11!!!!!!1 l!!!i!!I ==
ARCADIS GERAGHTY&MILLER
Table 1. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid. ID: Grid 16 Grid 17
Sample ID: 016 (0 -0.5) 016(0.5-1) 016(1-1.5) 017 (0-0.5) 017(0.5-1)
STL Savannah Laboratory ID:
Depth Interval (ft b Is):
Number of Subsamp Jes:
Constituents (mg/kg.dw)
Hexavalent Chromium (USEPA 7 I 96A)
Antimony (USEPA 6010)
Nickel (USEPA 6010)
Total Cyanide (USEPA 9010)
Amenable Cyanide (USEP A 90 I 0)
Percent Solids
ft bis
NA
Feet below land surface.
Not analyzed.
Not sampled.
Date Sampl ed:
ReniediatiOn i,?tii:i,~1}~1{
03382-21/53
0 -0.5
4
5/24/00
< 0.49 ·
< 2.2 ·
230J11 •
22.
2.5 ·
82
NS
mgfkg.dw
<
Milligrams per kilogram on a dry weight basis.
Constituent was not detected above the quantitation limit.
Constituent Concentration tllceeds Remediation Level.
03382-22/54 03382-19
0.5 - I I -1.5 0 -0.5
4 4 5
5/24/00 5/24/00 5/24/00
< 0.47 · NA < 0.47
< 2.1 ~ NA < 2.3
130 NA 640J"
17 · NA NS
2.0 NA NS
85 -NA 86
Constituent concentration is qualified as estimated because 1he MS/MSD relative pen:enl difference was outside QC limits.
Constituent concentration is qualified as estimated because the field replicate sample criteria were not met.
g:\env\j fdchann\nc202 .2 I O\Tabtes\grid _samples_ new I .Ills\ 7 I I 9/00
03382-20
0.5 - I
5
5/24/00
< 0.47 ·
<2.1
510
NS
NS
85 ·
G17(1-1.5)
I -1.5
5
5/24/00
NA
NA
NA
NS
NS
NA
Grid 18
GI 8 (0 -0.5) GI 8 (0.5 -I)
03382-23/46 03382-24/47
0 -0.5 0.5 - I
5 5
5/24/00 5/24/00
G!8(1-l.5)
033828-2/3
I -1.5
5
5/24/00
0.68 , 0.97 · <0.48 ·
.< 12 · <2.4 .
ISO • ';;1/:620/te 220
<1.3-<l.2 ;;,Tf210,:
79 81 82 •
--
Page 6 of8
- - - - -- - -- -
l!!!!!!!I l!!!!!!!I l!!!!!I
ARCADIS GERAGHTY&MILLER
Table I. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID: Grid 19 Grid 20
Sample ID: GI 9 (0 -0.5) 019(0.5-1) Gl9(1-l.5) 020 (0 -0.5) 020 (0.5 -I)
STL Savannah Laboratory ID:
Depth Interval (ft bis):
Number of Subsamples:
Constituents (mg/kg.dw)
Hexavalent Chromium (USEPA 7196A)
Antimony (USEP A 60 I 0)
Nickel (USEP A 60 I 0)
Total Cyanide (USEPA 9010)
Amenable Cyanide (USEPA 9010)
Percent Solids
ft bis
NA
Feet below land surface.
Not analyzed.
Not sampled.
Date Sampled:
ReinediatiOn, itf~~rtJJ;r~~ff
04471-11
0 -0.5
5
7/6/00
<0.46 •
2.9
380
51 ·
<1.2 .
86 •
NS
mg/kg.dw
<
Milligrams per kilogram on a <lry weight basis.
Constituent was not detected above the quantitation limi1.
Constituent Concentration exceeds Remediation Level.
04471-12 03436-7
0.5 -I I -1.5 0 -0.5
5 5 5
7/6/00 7/6/00 5/25100
<0.49 · NA <0.45
4.2 NA < 2.1
600 NA 320
140 , NA llO ·
<l.2' NA 7.9J.U,:-
81 NA 88
I :,0.:··:?~t<(n~:c~=,:1
J" ," Cous1ituent concentration is qualified as estimated because tl1e MS/MSD relative percent difference was outside QC limits.
Constituem concentration is qualified as estimated because the field replicate sample criteria were not met.
g:\env\j fdchann\nc202.2 l 0\ Tables\grid _samples_ new I .xis\ 7 / 19/00
03436-8
0.5 -I
5
5/25/00
< 0.44 •
< 2.0 •
90 ·
8.5J.u0
1.JJ"'..:•
90 ·
020 (I -1.5) 02 I (0 -0.5)
03436-28
I -1.5 0 -0.5
5 5
5/25/00 5/25/00
NA < 0.52 ·
NA <2.4·
NA 610 ·
NA 190
NA < l.O
NA 77
liiliill liiiiiiil
Page 7 of8
Grid 21
021 (0.5 -I) 021 (I -1.5)
03436-29
0.5 -I I -1.5
5 5
5/25/00 5/25/00
< 0.49 · NA
<2.2 NA
79 NA
41 • NA
3.8 · NA
82 · NA
- - - - --l!!!!!!!!I l!!!!!!!!!I I!!!!!! l!!!!!I l!!!!!I l!!!!!I l!!!!!I
ARCADIS GERAGHTY&MILLER
Table I. Summary of Analytical Results for Surficial Soil Samples, Soil/Sludge Remediation, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Grid ID: Grid 21 (Resampled) Grid 22
Sample ID: G21 (0 -0.5) G21 (0.5 -I) G21 (I -1.5) G22 (0 -0.5) G22 (0.5 -I)
STL Savannah Laboratory ID:
Depth lnterv_al (ft bis):
Number of Subsamples:
Constituents (mg/kg.dw)
Hexavalent Chromium (USEPA 7196A)
Antimony (USEP A 60 I 0)
Nickel (USEPA 6010)
Total Cyanide (USEPA 9010)
Amenable Cyanide (USEPA 9010)
Percent Solids
ft bis
NA
Feet below land surface.
Not analyzed.
Not sampled.
Dale Sampled:
04471-13
0 -0.5
5
7/6/00
<0.51 '
6.2 ,
1,000 ·
50 - .
<1.3.
78
NS
mg/1.g.dw
<
Milligrams per kilogram on a dry weight basis.
Constituent was not detected above the quantitation limit.
Constituent Concentration exceeds Remediation Level.
04471-14 03436-30
0.5 -I I -1.5 0 -0.5
5 5 4
7/6/00 7/6/00 5/25/00
<0.51 • NA < 0.56
5.6 NA <5.1
710 NA '''i":'i.,' I', 1oo_r/'Jli
39 NA 110
<l.3 NA <1.0
77 NA 72
Constituent concentration is qualified as estimated because the MSfl..ISD relative percent difference was outside QC limits.
Cons1iwen1 concentration is qualified as estimated because the field replicate sample criteria were not met.
g;\env\jfdchann\nc202.2 J 0\ Tables\grid _samples_ new I .xis\ 711 9100
03436-31
0.5 -I
4
5/25/00
< 0.56
< 2.6
740
57
1.0
71
G22 (I -1.5)
I -1.5
4
5/25/00
NA
NA
NA
NA
NA
NA
==
Page 8 of8
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ARCADIS GERAGHTY & MILLER
FIGURES
g: \en v\j f dchann \ncO 20 2 .21 O\report\soi l _sludge samp ling\report \samp-rptv2. doc \21 -J ul-00
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I Grid ID:
De th Interval ft bis : 0 -0.5 0.5 -I
I Number of Subsam Jes: 5 5
Date Sam led: 5/24/00 5/24/00
Hexavalent Chromium 0.62 0.65
Antimonv < 4.9 < 2.3
. Nickel 640
Total C ·anide 500 200
-Amenable Cvanide 27
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De th Interval (ft bis): 0 -0.5
Number of Subsarn !es: 5
·· Date Sam led: 7/6/00
Hexavalcnt Chromium <0.48
I Antimonv 19 16J
·· Nickel
· Total Cvanide
Amenable Cvanide
I
I ARCADIS GERAGHTY & MILLER
2301 Re-xwoocis Drive-of North Carolina, Inc.
Suite 102 RALEIGH, NC 27607
I Tel: [phone] Fa.x: 919/782-5905
I • 1.5
5
5/24/00
NA
NA
5
7/6/00
<0.45
<2.3
510
100
16J
PRJT MANAGER,
N. SHETTY
NOTES:
Grid IO: Grid 22
De th Interval (ft bis): 0 -0.5 0.5 - I
Number of Subsam les: 4 4
Date Sam led: 5/25/00 5/25/00
<0.56 < 0.56
<5.1 < 2.6
$.~r100:~}r 740
110 57
Amenable Cvanide <1.0 1.0
Grid 18
0 -0.5 0.5 - I
5 5
5/24/00 5/24/00
0.68 0.97
I -l.5
4
5/25/00
NA
NA
NA
NA
NA
Legend
®
+
ft bis
NA
NS
<
D2
Grid Number
Grid Node
Combined Grid
Constituents Detected Above
Remediation Levels Within Grid
Feet Below Land Surface
Not Analyzed
Not Sampled
Consituent Not Detected Above
the Quantitation Limit
l-~'.f,100 <a;;: j Constituent Concentration
Exceeds Remediation Level
Constituent Concentration ts
Qualified As Estimated Because
the MS/MS□ Relative Percent
Difference Was Outside QC
Limits.
Amenable C anide < 1.3 < 1.2 ~2109!1~
Constituent Concentration Is
Qualified As Estimated Because
the Field Replicate Sample
Criteria Were Not Met.
Grid ID: Grid 14
I . De th Interval ft bis): 0 -0.5 0.5 -I
, c;:z •-, f0 /f';"~"'~"';";"~e:::;:,:..,~:::he,me,mecie,uccmc... __ +-..:..,:';;"-+-'-:cc"--
NumberofSubsam !cs: 5 5
7/6/00 7/6/00
< 0.48 < 0.47
4.9 10
f Total Cvanide
.;-: /~. Amenable Cvanide
CHECKED BY:
M. PAHR
Nickel 450 :'~;tf•200~-
Total Cvanide NS NS
.-. Amenable Cvanide NS NS
0 -0.5
5
5/24/00
< 0.47
< 2.3
600J
NS
NS
DRAFTER•
J. HALL
DRA\JING:
RESULTS
DAT[,
19JUL00
Grid 11
0.5 -I I . 1.5
5 5
5/24/00 5/24/00
< 0.47 <0.46
< 2.4 <2.3
:;:{t;400 ... ~, 77
NS . NS
NS · NS
PROJECT NUMBER• NC0002!0.000J
JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
I . 1.5
5
7/6/00
<0.47
<2.4
290
NS
NS
All Results Are Given In
Milligrams Per Killogram On A
Ory Weight Basis
o· 60' 120· --~-~-~--1 I ■■ -----~'
SCALE: FEET
CONSTITUENTS DETECTED ABOVE
REMEDIATION LEVELS IN
SURFICIAL SOILS
FIGURE:
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ARCADIS GERAGHTY&MILLER
ATTACHMENT I
Laboratory Analytical Reports
g:\env\jf dchann \nc0202 .21 O\report\soil _ sludge sampling\report\samp-rptv2.doc\3 l -J ul-00
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ARCADIS GERAGHTY&MILLER
Data Review
The purpose of this section is to evaluate the field and laboratory analytical data (STL Savannah
Laboratories Logs No. S0-03382 [A, B, D, and E], S0-03436 [A], and S0-04471 [Al) for the
completeness of data package deliverables (Reporting Level II}. The composite soil and associated QC
sample data were validated following the rules set forth in the Functional Guidelines for Evaluating
Inorganic Analyses (USEPA, 1994). Additionally, all field records were reviewed to verify the
completion of required documentation.
Field Quality Assurance Components
All field activities were appropriately documented in the sampling logbook. The composite soil and QC
samples collected on May 24-25 and July 6, 2000 for analysis ofhexavalent chromium, antimony, nickel,
and amenable and total cyanide, were appropriately labeled, stored in sample containers on ice, and sent
via a courier to STL Savannah Laboratories, Savannah, Georgia. Equipment Rinsate blank samples (EB-
O I through EB-09) were collected in association with the composite soil samples. Additionally, field
replicate samples REP-0 I (G 11 [0-0.5]), REP-02 (G 11 [0.5-1]), REP-03 (G 11 [1-1.5]), REP-04 (G20 [0-
05]), REP-05 (G20 (0.5-1]), REP-06 (sample not analyzed), REP-07 (GS (0-05]), REP-08 (G8 (0.5-1]),
and REP-09 (GS [ 1-1.5]) were collected to assess data precision.
Composite soil samples G7 (0-0.5), G8 (1-1.5), GI I (0.5-1), GlS (1-1.5), G20 (0.5-1), G21 (0-0.5), G21
(0.5-1 }, G22 (0-0.5) were selected for matrix spike (MS)/MS duplicate (MSD) analysis.
Analytical Quality Assurance Components
All composite soil samples and associated QC samples collected on May 24-25 and July 6, 2000 were
analyzed within the required holding time periods. Deviations from QC standards are discussed below.
With the exception of the deviations reported herein, all sample QC parameters were within established
control limits or did not result in data qualification. The attached data are valid and usable within the
confines of this review.
Hexavalent Chromium (USEPA Method 7196A)
The required quantitation limits were reported. This compound was not detected in the associated method
blank and equipment rinsate blank QC samples. The field duplicate sample criteria were not met for
composite soil samples GS (0.5-1) and REP-08. The hexavalent chromium data for these two samples,
therefore, are qualified as estimated and flagged "J" if detected and "<J" if nondetected. No other
deviations resulting in data qualification were noted.
g: \en v\j f dchann \nc0202.2 l O\report\soi I_ sludge sampling\rcport\samp•rptv2.doc\3 I • J uJ.QO
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AR CAD IS GERAGHTY & MILLER
Antimony and Nickel (USE PA Method 601 OB)
The required quantitation limits were reported with the exception of several samples which were diluted
because of elevated concentrations or matrix interferences. These two metals were not detected in the
associated method blank and equipment rinsate blank QC samples. Because the MS/MSO recoveries for
antimony were below the lower QC limits in QC batches ID 0601A and 0601B (Log No. S0-033S2) and
053 IA (Log no. S0-03436), the associated samples were redigested using the optional digestion
technique described in section 7.5 ofUSEPA Method 3050B and reanalyzed as part of QC batch ID
06070 (Log No. S0-033S20) and 0607C (Log No. S0-03436A). The initial sample data for QC batches
0601A, 0601B, and 053 IA, therefore, were not used. The following samples had nickel MS/MSO
recoveries and/or relative percent differences (RPOs) outside QC limits: G7 (0-0.5) -RPO of35% and
REP-03 -MSO %R 151 and RPO of 56%. The nickel data associated with samples G7 (0-0.5) and REP-
03, therefore, were qualified as estimated and flagged "J" and "-J/<J," respectively. Additional samples
with nickel MS/MSO recoveries and/or RPDs outside QC limits, however, were not qualified because
the initial sample concentration exceeded the spike concentration added by a factor of 4 or greater: G 11
(0.5-1)-0/0 %R; G20 (0-0.5) -141/153 %R; GIS (1-1.5)-no recoveries; G21 (0.5-1)-no MSO
recovery and RPO; and G21 (0-0.5) and G21 (1-1.5) -no recoveries and RPO. The field duplicate
sample criteria for primary/replicate samples G 11 (0.5-1)/REP-02 (nickel) and GS (0.5-1)/ REP-OS
(antimony) were not met. The data for these samples, therefore, are qualified as estimated and flagged
"J" if detected and "<J" if nondetected. No other deviations resulting in data qualification were noted.
Amenable and Total Cyanide (USEPA Method 9010
The required quantitation limits were reported with the exception of several samples which were diluted
because of elevated concentrations. These two compounds were not detected in the associated method
blank and equipment rinsate blank QC samples. The following samples, which had total cyanide
MS/MSO recoveries and relative percent differences (RPOs) outside QC limits, were not qualified
because the initial sample concentration exceeded the spike concentration added by a.factor of 4 or
greater: GS (1-1.5), GIS (1-1.5), G20 (0.5-1), G21 (0.5-1), G21 (0.5-1), and G22 (0-0.5). The field
duplicate sample criteria for primary/replicate samples GS (0-0.5)/REP-07 (amenable cyanide), GS (0.5-
1)/REP-OS (amenable cyanide), GS (1-1.5)/REP-09 (amenable cyanide), G20 (0-0.5)/REP-04 (amenable
cyanide), and G20 (0.5-1)/ REP-05 (amenable and total cyanide) were not met. The data for these
samples, therefore, are qualified as estimated and flagged "J" if detected and "<J" if nondetected. No
other deviations resulting in data qualification were noted.
Reference
United States Environmental Protection Agency (USEPA), 1994a. National Functional Guidelines for
Evaluating Inorganic Analyses, Office of Solid Waste and Emergency Response, Contract
Laboratory Program. EPA-540-R/94-013. February.
Our ref.:
g: \env\j f dchann \nc0202.2 I 0\report\soil _ s Judge sampling\report\samp-rptv2.doc \3 1-J ul-00
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S.a v a n.n a·h
l:aboratorie's
,_.., .. a ..... ,,..,,i.ao,,.,,,.,,.,._ 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
July 17, 2000
Mr. Mark Radecke
Arcadis Geraghty & Miller
230 I Rexwoods Drive, Suite 102
Raleigh, NC 27607
Mr. Radecke,
RECEIVED
JUL 1 8 2000
ARCADIS Geraghty & Miller
Samples received May 25 (S003382) and May 26, 2000 (S003436) at STL
Savannah from the JFD Channel Master site contracted through Arcadis Geraghty and
Miller were digested and analyzed according to SW846 Method 3050B and 6010B for '
antimony. Low percent recoveries were observed for the matrix spikes. STL Savannah
reanalyzed all of the antimony samples utilizing the optional digestion technique
described in Section 7.5 of SW846 Method 3050B An increase in the matrix spike
recoveries was observed. Both sets of data were supplied to the client.
Sincerely,
~s~Pmj,e< Mm~e,
STL Savannah
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S,a via n1n·a h
L"abOratorie·s
._ .. .._,,,, ... i.....,....,inc, 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LT0#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
-------------------------------------------------------------------------
03382-1
03382-2
03382-3
03382-4
03382-5
G2
G2
G4
G4
GS
(0-0.5)
(0.5-1.0)
(0-0.5)
(0.5-1.0)
(0-0.5)
05-24-00/08:20
05-24-00/08:40
05-24-00/09:01
05-24-00/09:15
05-24-00/09:30
------------------------------------------------------------------- ------
PARAMETER
-----------------------------
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03382-1
----------
0.63
1
05.30.00
06.01.00
0530A
<2.3
1
06.01.00
06.02.00
0601A
110
1
06.01.00
06.02.00
0601A
86
03382-2
----------
0.55
1
05. 30. 00
06.01.00
0530A
<2.1
1
06.01.00
06.02.00
0601A
130
1
06.01.00
06.02.00
0601A
88
03382-3 03382-4 03382-5
------------------------------
<0.49 0.52 <0.47
1 1 1
05.30.00 05.30.00 05.30.00
06.01.00 06.01.00 06.01.00
0530A 0530A 0530A
<2.2 <2.1 <2.4
1 1 1
06.01.00 06.01.00 06.01.00
06.02.00 06.02.00 06.02.00
0601A 0601A 0601A
94 45 490
1 1 1
06.01.00 06.01.00 06.01.00
06.02.00 06.02.00 06.02.00
0601A 0601A 0601A
85 85
-------------------------------------------------------------------------------
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S a ,v,:a, n -~:.a~h
tabor:ator-ies 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO~052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 101s □067
Page 2
DATE/
LOG NO
03382-6
03382-7
03382-8
03382-9
03382-10
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
--------------------------------------------------
GS (0.5-1.0)
G7 (0-0.5)
G7 (0.5-1.0)
G9 (0-0.5)
G9 (0.5-1.0)
----------------------------------------------- ---
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03382-6
<0.46
1
05.30.00
06.01.00
0530A
<2.3
1
06.01.00
06.02.00
0601A
180
1
06.01.00
06.02.00
0601A
87
03382-7 03382-8
a.so 0.46
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530A 0530A
<2.3 <2.3
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601A
81 80
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601A
80 88
05-24-00/09:40
05-24-00/10:00
05-24-00/10:05
05-24-00/10:25
05-24-00/10:45
03382-9 03382-10
0.62 0.65
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530A 0530A
<4.4*F65 <2.1
2 1
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601A
1500 640
2 1
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601A
82 86
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s·av,a n,n ah
l!aborSto'ritiS ; 102 LaRoche Avenue • Savannah, GA 31404 • (912) 3;4-7s;s · Fax (912) 3;2-016; · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 3
DATE/
LOG NO
03382-11
03382-12
03382-13
03382-14
03382-15
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
REP-01
TIME SAMPLED
05-24-00
05-24-00
05-24-00/11:10
05-24-00/11:20
05-24-00/11:45
PARAMETER
REP-02
Gll (0-0.5)
Gll (0.5-1.0)
Gl0 (0-0.5)
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03382-11
<0.48
1
05.30.00
06.01.00
0530A
<2.4
1
06.01.00
06.02.00
0601A
600
1
06.01.00
06.02.00
0601A
84
03382-12
0 .91
1
05.30.00
06.01.00
0530A
<2.4
1
06.01.00
06.02.00
0601A
670
1
06.01.00
06.02.00
0601A
85
03382-13 03382-14
<0.47 <0.47
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530A 0530B
<2.3 <4.7*F65
1 2
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601B
600 1400
1 2
06.01.00 06.01.00
06.02.00 06.02.00
0601A 0601B
86 85
03382-15
0.55
1
05.30.00
06.01.00
0530A
<2.1
1
06.01.00
06.02.00
0601B
340
1
06.01.00
06.02.00
060J.B
85
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S,a v a n,n1 a·ih
t3bcir3toi:ies 5102 LaRoche Avenue · Savannah, GA 31404 , [phone] • Fax [phone] • www.stlsavlab.com
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03382-16
03382-17
03382-18
03382-19
03382-20
PARAMETER
Gl0
Gl3
Gl3
Gl7
Gl7
(0.5-1.0)
(0-0.5)
(0.5-1.0)
(0-0.5)
(0.5-1.0)
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03382-16 03382-17
<0.46 <0.47
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530A 0530A
<2 .1 <2.1
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
91 570
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
87 85
03382-18
<0.47
1
05.30.00
06.01.00
0530A
<2.1
1
06.01.00
06.02.00
0601B
580
1
06.01.00
06.02.00
0601B
85
05-24-00/12:00
05-24-00/13:40
05-24-00/13:58
05-24-00/14:20
05-24-00/14:35
03382-19 03382-20
<0.47 <0 .47
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530A 0530B
<2.3 <2.4
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
640 510
1 1
06 .01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
86 85
------------------------------------------------- ------------------------------
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S-a' v-a: n. n;:a;h
tab'ol'.ator.ieS 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03382-21
03382-22
03382-23
03382-24
PARAMETER
Gl6 (0-0 .5)
Gl6 (0.5-1.0)
Gl8 (0-0.5)
Gl8 (0.5-1.0)
-----------------------------
Hexavalent Chromium (7196A),
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nicke-1 (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
-----------------------------
----------
mg/kg dw
----------
03382-21 03382-22
--------------------
<0.49 <0.47
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530B 0530B
<2.2 <2.4
1 1
06.01.00 06 .01.00
06.02.00 06.02.00
0601B 0601B
230 130
1 1
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
82 85
--------------------
05-24-00/15:00
05-24-00/15:05
05-24-00/15:40
05-24-00
03382-23 03382-24
--------------------
0.68 0.97
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530B 0530B
<13*F65 <ll*F65
5 5
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
1600 1800
5 5
06.01.00 06.01.00
06.02.00 06.02.00
0601B 0601B
79 81
--------------------
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S a.v·a·n/n a·,h
E3bo·rato~r.ieS
,-...,o,s.,,,,.,,.,,,uoo., __ ..,. 5102 LaRoche Avenue· Savannah, GA 31404 · (912) 3.54-7858 · Fax [phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 6
DATE/
TIME SAMPLED
03382-25 EB-01 05-24-00/13:30
03382-26 EB-02 05-24-00/13:33
PARAMETER
Hexavalent Chromium (7196A), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/1
Dilution Fac~or
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382-25
<0.010
1
06 .01.00
06.01.00
0601C
<0.020
1
05.25.00
05.26.00
052SL
<0.040
1
05.25.00
05.26.00
0525L
03382-26
<0.010
1
06 .01.00
06. 01. 00
0601C
<0.020
1
05.25.00
05.26.00
052SL
<0.040
1
05.25.00
05.26.00
0525L
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S.atv a n'n•a,h
l;;ali'Oratoi'.iE!'S
........... s ..... ,, ........... .,... ..... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.c_om
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN oo
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 7
DATE/
TIME SAMPLED
------------------------------------------------------------------------------------
03382-27 EB-03 05-24-00/13:35
--------------------------------------------------- ---------------------------------
PARAMETER 03382-27
--------------------------------------- -------------------- ---------- ----------
Hexavalent Chromium (7196A), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-------------------------------------------------
<0.010
1
06.01.00
06.01.00
0601C
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S.a·v a,n·n'a,'h
t'abO'r:·at(i'f.ie's 5102 LaRoche Avenue• Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com . .,_ .. ......,, ................. ...
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
CC: Mr. Mark Radecke
Client PO. No.: LTOij052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 1.01.50067
Page 8 REPORT OF RESULTS
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
03382-28
03382-29
03382-30
03382-31.
03382-32
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (601.0), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (601.0), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382-28
<0.40
l.
05.30.00
06.01..00
0530A
<2.0
l.
06 .01..00
06.02.00
0601.A
<4.0
l.
06.01..00
06.02.00
0601.A
03382-29
1.08 %
l.
05.30.00
06.01..00
0530A
98 %
l.
06.01.00
06.02.00
0601.A
03382-30
80-1.20 %
75-1.25 %
1.02 % 75-1.25 %
l.
06.01.00
06.02.00
0601.A
03382-31.
98 %
1
06.01.00
06.02.00
0601.A
1.02 'Ir
l.
06.01.00
06.02.00
0601.A
03382-32
0 %
0 %
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s:a:-v·am'n a-h t·aOcfr:3tO·r:1Et's 5102 LaRocheAvenue • Savannah, GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 9
DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03382-33
03382-39
03382-40
03382-55
03382-56
LCS Precision Control Limit (Advisory) 'lrRPD Method Blank
Lab Control Standard 'Ir Recovery
Lab Control Standard Duplicate 'Ir Recovery
Precision ('lrRPD) of LCS/LCSD
PARAMETER 03382-33 03382-39
Hexavalent Chromium <0 .40 (7196A) , mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), 'Ir <20 % Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), % <20 'Ir
Dilution Factor
Prep Date
Analysis Date
Batch ID
1
05.30.00
06.01.00
0530B
<2.0
1
06.01.00
06.02.00
0601B
<4 .0
l
06.01.00
06.02.00
0601B
03382-40
107 'Ir
1
05.30.00
06.01.00
0530B
101 %
l
06.01.00
06.02.00
0601B
104 'Ir
l
06.01.00
06.02.00
0601B --------------------
03382-55 03382-56
100 % 1.0 %
1
06.01.00
06.02.00
0601B
104 'Ir 0 %
1
06_.01.00
06.02.00
0601B
----------
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S a'v·a',_n, n,a,h
l::ab'o'ratO~i&S 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr_ Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: OS JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382-34 Matrix Spike%-Recovery (G7 0-0.5)
03382-35 Matrix Spike Duplicate%-Recovery (G7 0-0.5)
03382-36 MS Accuracy Advisory Limit (%-R)
03382-37 Precision ('lrRPD) MS/MSD (G7 0-0.5)
03382-38
PARAMETER
MS Precision Advisory Limit ('lrRPD)
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), %-
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), %-
Dilution Factor
Prep Date
Analysis Date
Batch ID -----------------------------
03382-34
90 %-
1
05_30.00
06.01.00
0530A
31 %*F73
1
06.01.00
06_02.00
0601A
75 %-
1
06_01.00
06.02.00
0601A
----------
03382-35
89 'Ir
1
05.30.00
06.01.00
0530A
32 %-*F73
1
06.01.00
06.02.00
0601A
107 %-
1
06.01.00
06.02.00
0601A
----------
03382-36
80-120 %-
75-125 %-
75-125 %-
----------
03382-37
1.1 'Ir
3.2 %-
35 %-*F79
----------
03382-38
<20 %-
<20 %-
----------
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s. a.-y.:a.:n~n:.at.~ Labor-ator.1es 5!02LaRocheAvenue · Savannah,GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 10150067
REPORT OF RESULTS Page 11
LOG NO
03382-41
03382-42
03382-43
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
Matrix Spike% Recovery (Gll 0.5-1.0)
Matrix Spike Duplicate% Recovery (Gll 0.5-1.0)
Precision (%RPO) MS/MSD (Gll 0.5-1.0)
------------------------------------------------------------------------------------
PARAMETER 03382-41 03382-42 03382-43
Hexavalent Chromium (7196A), mg/kg dw 84 % 85 % 1.2 %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010),
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
%
1
05.30.00
06.01.00
0530B
31 %*F73
2
06.01.00
06.02.00
0601B
0 %-*F61
2
06.01.00
06.02.00
0601B
1
05.30.00
06.01.00
0530B
30 %*F73
2
06. 01. 00
06.02.00
0601B
0 '1r*F61
2
06.01.00
06.02.00
0601B
3.3 %
0 %
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s·a v. a,•n•n ah
l!abO'rcitOries
,-...,.,s ..... r,.,...__,no 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 12
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- ---------- ----------------- ----------------------- -----------------------
03382-48
03382-49
03382-50
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
------------------------------------------------------------------------------------
PARAMETER
-------------------------------------------------
Hexavalent Chromium (7196A), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-------------------------------------------------
03382-48 03382-49 03382-50
<0.010 101 % 85-115 %
1 1
06.01.00
06.01.00
0601C
<0.020
1
05.25.00
05.26.00
0525L
06.01.00
06.01.00
0601C
100 %
1
05.25.00
05.26.00
0525L
75-125 %
<0.040 103 t· 75-125 %
1 1
05.25.00 05.25.00
05.26.00 05.26.00
0525L 0525L
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
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S' a 1.v. a.n n.a 'h
l:!afiora·to-rie's 5102 LaRoche Avenue· Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: OS JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 13
DATE/
LOG NO
03382-44
03382-45
03382-46
03382-47
03382-51
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
--------------------------------------------------
G13 (0-0. 5)
G13 (0.5-1.0)
G18 (0-0.5)
G18 (0.5-1.0)
G9 (0-0.5)
------------- ---------- ---------------------------
PARAMETER 03382-44
Cyanide, Total (9010), mg/kg dw 90
Dilution Factor 10
Prep Date 05.31_00
Analysis Date 05.31.00
Batch ID 0531S
Cyanide, Amenable
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
(9010), mg/kg dw 2.8
10
05.31.00
OS. 31. 00
0531T
85
03382-45
----------
110
10
05.31.00
05.31.00
0531S
13
10
05.31.00
05.31.00
0531T
85
03382-46
----------
150
20
05.31.00
05.31.00
0531S
<1.3
20
05.31.00
05.31.00
0531T
79
05-24-00/13:40
05-24-00/13 :58
05-24-00/15:40
05-24-00
05-24-00/10:25
03382-47 03382-51
--------------------
620 500
so so
05.31.00 06.02.00
05.31.00 06.02.00
0531S 0602T
<1.2 27
50 50
05.31.00 06.02.00
05.31.00 06.02.00
0531T 0602T
81 82
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s·a1v·a,rr n.a h
t'abOratOf.ie·s
•--.. S-T.-~-n.0.,. 5102 LaRoche Avenue• Savannah, GA 31404 · [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun S_hetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382
Received: 25 MAY 00
Reported: OS JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 10150067
Page 14
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03382-52
03382-53
03382"'54
G9 (0.5-1.0)
Gl6 (0-0.s)·
Gl6 (0.5-1.0)
05-24-00/10:45
05-24-00/15:00
05-24-00/15:05
----------- -------------------------------------------------- -----------------------
PARAMETER
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382-52
--------------------
200
so
06.02.00
06.02.00
0602T
30
so
06.02.00
06.02.00
0602T
03382-53 03382-54
--------------------
22 17
5 5
06.02.00 06.02.00
06.02.00 06.02.00
0602T 0602T
2.5 2.0
5 5
06.02.00 06.02.00
06.02.00 06.02.00
0602T 0602T
Percent Solids 86 82 85
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I
I
I
I
I
I
I
I
,
I
I
I
I
s; a~v; a,n:n~a• h
l!.3bOiato-ririS ..... ..,. ........ ,,... ...... _..., 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fa.x [phone] · www.stlsavlab.com
LOG NO: S0-03382
Received: 25 MAY 00
Reported: 05 JUN 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31.388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.02l.0
Sampled By: Client
Code: l.0l.50067
Page l.5
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03382-52
03382-53
03382-54
G9 ( 0. 5 -1. 0)
Gl.6 (0-0.5)
Gl.6 (0.5-l..0)
05-24-00/l.0:45
05-24-00/l.5:00
05-24-00/15:05
------------------------------------------------------------------------------------
PARAMETER 03382-52 03382-53
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, IIB, and III.
MS/MSD FOR G7 (0-0.5) failed to meet advisory criteria for Nickel and
Antimony due to matrix interference. The Nickel concentration was Bl
mg/kg dw and Antimony <2.3 mg/kg dw. The spiked amount was 56.8 mg/kg
dw for both Nickel and Antimony.
MS/MSD for Gll (0.5-l..0) failed advisory criteria for Nickel and
Antimony due to the abundance of analyte. The total Nickel
concentration was l.400 mg/kg dw and Antimony was <4.7 mg/kg dw. The
spiked amount for Nickel and Antimony was 58.8 mg/kg dw for both Nickel
and Antimony.
03382-54
*F61 = The recoveries of the matrix spikes are outside advisory limits due to
the abundance of the target analyte in the sample.
*F65 = Elevated detection limits were reported due to sample matrix.
interference which required sample or extract dilution.
*F73 = Matrix spike recoveries were outside advisory limits due to matrix
interference present in the sample.
*F79 = Matrix spike recoveries were outside advisory limits due to
non-homogeneity of the sample.
~-- --ARCADIS GERAGHTY & MILLER --------------Laboratory Task Order No./P.O. No. ()(2.,~Qt>-.$ CHAIN-OF-CUSTODY RECORD Page _L of.....2,_
Project Number/Name NC:L"b~ 2-<...'1... 0'2-.IQ I ANALYSIS/ METHOD/ SIZE I
I
Project Location "JF-.D le. t'l Q.>;.f:c,:W"> 'd' . .J
j j '.f }r.,.
Laboratory Sn... S'A""'?~'J Al-t Lb!\C .p...Y .i -< :.i
Project Manager iY SH:=='f ( "J" '.} J'j
Sampler(s)/ Affiliation ·;rc:-FF ........._L '--ei.e---1.L~ ' .r , , f.tl r'-. "-"'"' C.U<-EC C. ;.,,,u:.-.1) ;".) CJ~ , -<
Datemme .., ... :{
Sample ID/Location Matrix Sampled Lab ID "ii .. Remarks Total
"'°Li O -Q. S) 5 5,~ .. "L'f .-Ob ,:z..c I I
' 5 --Z..'i -= G z. ( lJ, .S" -I, "J 5 >':' 240 I I
G-2 (,.c,.-1,Sl ..) s·•-'l...'i--o, \ I c:·,..,c
(..:..U f 0-C, !;) 5 s -u,-0, l I CJ· c:
C,-'-j (c,,S-1.c,) s s-2;:'I-= '-IS I I
G-Y I I. c,. -I ,) s 5-~\/•C-0 . ' ~· I I
&S (o-o.s) .s 5 .. ".':.= I I
G-5 iu.s--1.t:i, .5 :S ·-1.>, _,._, I _.-(t. ~;,h.-I ·4.-_;o
&S (i,(.;-/.S) s 5--z..,, -"'-> I ('.. (?"__A',., i ,,,u . ' . . . .-.•
( u-o,S\
. = . ~:} :/., G'.-7 5 5-2..¼-= I I 10,1..-0 . ~' ~
C:-7 fo. S··J.0} s S;;;;-;..~;? I
.:__,.,-".•·;,:· I .(__··
0 C:-7 (i.i:,-1->) 5 s-1.1-= ·,c.,.: 1..S I i
G-a. io-~.-;.) $ s -;v-1 -c--> c,~~ I I
c,:.c, (c,,s-1.'.,) 5 5·-L'i•C> I I i"o\ "-" .
G-9 (1,<.:. -1,S") s "5-L¼-<,O \ ~'--i 6 ' :;.3.525c::_. I ,oi.~·'4 ...
Sample Matrix: L = Liquid; s Solid; A Air Total No. of Bottles/ iS = = Containers
Relinquished by: 1..1-..,\,, ... x. 'l:'. /'2-....L.--"" Organization: l«LCZ l 5s!:; •'-' Date .s l <-'I l C?..>-Time ,i:crt. Seal Intact?
Received by: · '1,·
, ,, ,. , \J./ ';..--lZ. :;/ oc Time 9.'1:> ~ No Organization: s G.-...:.-~--Date N/A , ,
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special Instructions/Remarks: I '· . ~r,.-c·-o.-..i,,d --1-. "rn-··-. --. ' --.·,---..... -= (">if:-_
~L ~ -h,..... N,,,_._J.J:;, c.f -½,-5~i~ c\--,p:llis ~pi.-,,... col Ir: ch!.d
i lecl--.;. 7 o ·-o ;s.· fvt._. '><A
Delivery Method: D In Person Carrier &;n e-:x,
SPECIFY
D Lab Courier □Other _______ _
SPECIFY AG 05-0597
~----ARCADIS GERAGHTY & MILLER --------------Laboratory Task Order No./P.O. No. OS'2.7.,= sf\ CHAIN-OF-CUSTODY RECORD Page ----1,,:_ ot----3-
Project Number/Name >-J C:.qy-c ·LO 7 o~, c
Project Location JF-J:> /w-, oi-ce, ,u-, / ;..,i,:;_
Project Manager ,-.; . Jj . ., .. ¾
Sampler(s)/Affiliation
Sample ID/Location
fl-t.-P--o;
~ fl-t.;,-P-·<).;,
G--11 / o-c. S)
G-11 (o.S-1.c)
€, G-tl (1..:,-1,s)
G--1 o /o-a.,;)
(;-1,:, (o. s-1,c)
@ G-tc i /,c-L!>)
® V>-<:3
GU ( ~-O•S)
e 6,-1.J (1.0-l,S)
\ tt, \ 1 . lD~ ~ J .
,...__ ~o~~ r,..,.__c...,i.$)
Daterrirhe
Matrix Sampled Lab ID
j S-2-'I -u'-'
.s 5--Z...'t-= ·-
5 S" .. "L.\J -«> ·11: I~
s 5-"1-'t-(5:) • f • ! ;, ....
s S"--Z...'1-<'.o I I c-t.S
s S-1.i,,/-c..~
)/\..'l$
.s 5-111·=
12.!'-0
s S--Z..'t,.,u
1 l, c, '-
L S"-1.>i-o.
,--:r· . .,.,:;;,.
L S-2-'i-<:k ' -.,;,
L S-tiJ-""" ;,.,,_~
s 5..:-i.r,-eou ·~•-'I(;,
s S--Ul-,:;t,
/~;.::11
5 '5-2..'t-"<>
I 'ti OS
Sample Matrix: L = Liquid; S = Solid; A = Air
(
I
I
I
i
I
/ ANALYSIS/ METHOD/ SIZE
I
I
Remarks Total
I
I
I
Total No. of Bottles/ i 5
Containers
Relinquished by: \..>--\.~C. 'i:' _ n 1 ,~
Received by: c ' •~ .{,,,,_,,,-? .
Organization: _ _,A-~"---C~-_A_T>_,-'_s~· ~E-~,q,,,_· ~M~--Date S / <--':J I"'° Time -~17?....,,~<!1'.'-=-_ ~I Intact?
Organization: 5':·[2... -,5,-,_µ Date 'L ,z..5) O O Time C/, '() ('es j No N/A
I V
Relinquished by: ___________ Organization: ____________ Date I I Time _____ 1 Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special Instructions/Remarks: I 1......,re.eJ,, ... •~ -a,,..o·._:j-...1 . 1 -' -11
'
1\ CD • + i b; 9 .J:L< Db...J...l ~
Delivery Method: □ In Person [ll'Common Carrier Rn t£:7"
SPECIFY
□ Lab Courier □Other ___ ==----
5PEcJFv AG 0S-0597
-~ - --ARCAD/S GERAGHTY & MILLER --------------Laboratory Task Order No./P.O. No. on 3(/lj--8 CHAIN-OF-CUSTODY RECORD Page 2--of---3.....
Project Number/Name µc:.ovo 'Z-<,'?..-C>·.1..1 c
Project Location 7"Fo / en Ql'f'c-tt..o , ,-..c.._
I ANALYSIS/ METHOD/ SIZE
Laboratory ::>~ s~~"'"',J.. L...loc~~
Project Manager ,-.i. J.b~
Sampler(s)/A ffil iation
Sample ID/Location
Bntt.l-.
Sample Matrix: L ; .Liquid; S ; Solid; A ; Air
Remarks Total
I
I
I
Total No. of Bottles/ 9
Containers
l
I
l
I
I
I
Relinquished by: V...1,-L 't: ,, ...,L_.r -.,;;t _.l('-j .i _/\ I
Organization:_""M-"=<:.""'"-"'-"l::>"-1.s=...__:<\'..:':f/rµo=-----Date 5 t?...'i IC'<> Time--1.I..>~...!,',>,==----Seal Intact? Organization: 5 7l-.5:&.-J DatP .,-IV P O Time _ ___,9~. _.'I,,:>_, c@:; No NIA
Received by: ' • '-"'
" ll ll Relinquished by: __________ Organization: ___________ Date _ _,_, _ _,_, __ Time_____ Seal Intact? Received by: Organization: Date 1 1 Time _____ , Yes No N/A Special Instructions/Remarks·: i \..;,,)-ec,.,K ·-1 ---.. o· ... "--' ! I I l -J l (J
"'~ .11:-'-· ...J ._k ,l Ii .t · \..I \ ~
Delivery Method: D In Person
•
1)3 Common Carrie r _ _,_F'e:-=D::_c..e:),>=-------
spEc1Fv
. l I • ~ -, • • f • (,.;t\ • 4-<......-• -_, l -~ . ..____ t' I --a 1 -c~ \ . ~
D Lab Courier □Other ___ ==----sPEcJFv
-- - - ------- -
., ;
r
-----4/
-
.-. {
-- - ---
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s·a v.,a n:n a h
t3bor8fofies 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com '""''""'"'_,, ................ , ....
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382A
Received: 05 JUN 00
Reported: 07 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 09350067
Page 1
DATE/
LOG NO
03382A-l
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
G7 (0-0.5)
TIME SAMPLED
--------·---------------
05-24-00/10:00
PARAMETER 03382A-1
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<2.3
1
06.06.00
06.06.00
0606B
-------------------------------------------------------------------------------
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S a,v:ain::n a!h
Laborator.ies 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0·03382A
Received: 05 JUN 00
Reported: 07 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 09350067
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382A·2
· 03382A·3
03382A·4
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
------------------------------------------------------------------------------------
PARAMETER
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382A·2 03382A-3 03382A·4
<2.0 99 % 75-125 %
1 1
06.06.00 06.06.00
06.06.00 06.06.00
0606B 0606B
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I
s,.a·v,a: n1 n 1a~h
tahOra'tOrie·s
'"""""''"S-T,onoL.aoorOIGOH,IOC. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382A
Received: 05 JUN 00
Reported: 07 JUN oo
Client PO. No.: LT0#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 09350067
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382A-8
03382A-9
03382A-10
03382A-ll
Matrix Spike% Recovery (G7 0-0.5)
Matrix Spike Duplicate% Recovery (G7 0-0.5)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD (G7 0,0.5)
03382A-12 MS Precision Advisory Limit (%RFD)
------------------------------------------------------------------------------------
PARAMETER
Antimony (6010), %
Dilution Factor
Prep Date
Analysi's Date
Batch ID
03382A-8 03382A-9 03382A-10
------------------------------
86 'Ir 86 %-75-125 'Ir
1 1
06.06.00 06.06.00
06.06.00 06.06.00
0606B 0606B
------------------------------
Final Page Of Report
03382A-11 03382A-12
--------------------
o % <20 %-
--------------------
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S,a.v,a1n:n·a1h
1:.'a bO r 3t0 ~ie·s 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED ------------------------------------------------------------------------------------
03382B-l Gll (1-1.5)
03382B-2 Gl8 (1-1.5)
PARAMETER
-----.------------------------
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium (7196A) ,
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
mg/kg dw
03382B-l
<2.3
1
06.07.00
06.07.00
0607B
77
1
06.07.00
06.07.00
0607Z
<0.46
1
06.06.00
06.07.00
0606A
87
05-24-00/11:25
05-24-00
03382B-2
<2.4
1
06.07.00
06.07.00
0607B
1100
1
06.07.00
06.07.00
0607Z
<0 .48
1
06.06.00
06.07.00
0606A
82
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I
S ,a, v/a·· n, n· a, h
l!i:ib0r.at0f:i8S 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
--------------------------------------------------------- -- -------------------------
03382B-3 Gl8 (1-1.5) 05-24-00
PARAMETER 03382B-3
--------------------------------------- ----------------------------------------
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
220
1
06.07.00
06.07.00
0607T
210
50
06.07.00
06.07.00
0607T
82
-------------------------------------------------------------------------------
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S a1 vla n, n: a· h
t:8b0r:atori8s 5102 LaRoche Avenue· Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03382B-15 EB-03 05-24-00/13:35
------------------------------------------------------------------------------------
PARAMETER 03382B-15
-------------------------------------------------------------------------------
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.020
1
06.07.00
06:08.00
0607H
<0.040
1
06.07.00
06.08.00
0607H
----------------------------------------------------------- --------------------
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S,a:,v,a n~11,atJ:1
Laborator:ies 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03382B-16
03382B-17
03382B-18
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
------------------------------------------------------------------------------------
PARAMETER
-------------------------------------------------
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382B-16 03382B-17 03382B-18
<0.020 98 % 75-125 %
1 1
06.07.00 06.07.00
06.08.00 06.08.00
0607H 0607H
<0.040
1
06.07.00
06.08.00
0607H
101 %
1
06.07.00
06.08.00
0607H
75-125 %
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S,,ai v ·a1 n~. n, a. h
t:.:atiO ra tO r,ieS 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 5
DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
Method Blank
Lab Control Standard%-Recovery
LCS Accuracy Control Limit (%-R)
03382B-4
03382B-5
03382B-6
03382B-7
03382B-8
Lab Control Standard Duplicate%-Recovery
Precision (%-RPD) of LCS/LCSD
PARAMETER 03382B-4
_Antimony (6010), mg/kg dw
Dilution Factor
<2 .0
1
06.07.00
06.07.00
0607B
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw <4 .0 Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable
Dilution Factor
Prep Date
Analysis Date
Batch ID
1
06.07.00
06.07.00
0607Z
(9010), mg/kg dw <1.0
1
06.07.00
06.07.00
0607T
03382B-5
95 %-
1
06.07.00
06.07.00
0607B
104 %-
1
06.07.00
06.07.00
0607Z
03382B-6 03382B-7 03382B-8
75-125 %-
75-125 %-
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S'a,,v a·n·n·a•h
L3bO'rtftories 5102 L~Roche Avenue· Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382B-4
03382B-5
03382B-6
03382B-7
03382B-8
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
03382B-4 03382B-5 03382B-6
--- --------------------------------------------------------
Cyanide, Total (9010), mg/kg dw -<1.0 97 % 90-110 %
Dilution Factor l l
Prep Date 06.07.00 06.07.00
Analysis Date 06.07.00 06.07.00
Batch ID 0607T 0607T
Hexavalent Chromium <0.40 102 % 85-115 %
(7196A), mg/kg dw
Dilution Factor l l
Prep Date 06.06.00 06.06.00
Analysis Date 06.07.00 06.07.00
Batch ID 0606A 0606A
--- ----- ---------------------------------------------------
03382B-7 03382B-8
--------------------
94 % 3.1 %
l
06.07.00
06.07.00
0607T
---------- ----------
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S,arwa,mn:a-h
labo·r-atOiiE!S 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
033828-9 LCS Precision Control Limit (Advisory) %RPO
------------------------------------------------------------------------------------
PARAMETER 03382B-9
Antimony (6010), %
Nickel (6010), %
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010),
I Hexavalent Chromium (7196A), mg/kg dw
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S'mv,a nc,n:a!h
t'ab"Oi:citar.ie'S 5102LaRocheAvenue • Savannah,GA31404 · [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTO#052300B
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382B-10
03382B-ll
03382B-12
03382B-13
03382B-14
Matrix Spike% Recovery (Gl8 1-1.5)
Matrix Spike Duplicate % Recovery (Gl8 1-1.·5)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD (Gl8 1-1.5)
MS Precision Advisory Limit (%RFD)
PARAMETER 03382B-10 03382B-ll 03382B-12 03382B-13 03382B-14
----------------------------------------------------------- ---------- ----------
Antimony (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010),
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
90 %
1
06.07.00
06.07.00
0607B
*F61
2
06.07.00
06.07.00
0607Z
64 %
50
06.08.00
06.08.00
0608T
----------
89 'Ir
1
06.07.00
06.07.00
0607B
*F61
2
06.07.00
06.07.00
0607Z
65 %
50
06.08.00
06.08.00
0608T
----------
75-125 %
75-125 %
75-125 %
----------
1.1 % <20 'I'
3.9 % <20 %
1.6 % <20 %
--------------------
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~a1,v .a.n:n}_a:·~
l:abor:atar.1es 5102 LaRocheAvenue • Savannah, GA 31404 • [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202_0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03382B-10 Matrix Spike% Recovery (Gl8 1-1.5)
03382B-ll Matrix Spike Duplicate% Recovery (Gl8 1-1.5)
03382B-12 MS Accuracy Advisory Limit ('lrR)
03382B-13 Precision (%RPO) MS/MSD (Gl8 1-1.5)
03382B-14 MS Precision Advisory Limit (%RPO)
------------------------------------------------------------------------------------
PARAMETER 03382B-10 03382B-ll 03382B-12 03382B-13 03382B-14
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
111 %
5
06.06.00
06.07.00
0606A
110 %
5
06.06.00
06.07.00
0606A
85-115 % 0.90 'Ir <30 %
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,S:.,a: y, ~ n::._n:aiJi
l.t'abocatories
•""''''°"'"'°"""T,,,.._...,,,.,n,1,., 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
· Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382B
Received: 06 JUN 00
Reported: 09 JUN 00
Client PO. No.: LTO*052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03382B-10 Matrix Spike% Recovery (G18 1-1.5)
03382B-ll Matrix Spike Duplicate% Recovery (Gl8 1-1.5)
03382B-12 MS Accuracy Advisory Limit (%R)
03382B-13 Precision (%RPO) MS/MSD (GlB 1-1.5)
03382B-14 MS Precision Advisory Limit (%RPO)
PARAMETER 03382B-10 03382B-11 03382B-12 03382B-13 03382B-14
MS/MSD was performed on sample S003382B-2 (G18 (1-1.5)) to
generate precision data.
MS/MSD for nickel failed advisory limits due to abundance of analyte
present in the sample. The sample contained 1100 mg/kg dw of nickel and
the spike level was 61 mg/kg dw. Precision data for nickel was
calculated from the MS/MSD results of 1500 mg/kg dw and 1490 mg/kg dw.
MS/MSD for cyanide failed advisory limits due to abundance of analyte
present in the sample. The sample contained 220 mg/kgdw total cyanide
and the spike level was 4.9 mg/kg dw.
The alternate digestion procedure in SW846, Method 350B, Section 7.5 was
utilized to determine antimony data.
*F61 = The recoveries of the matrix spikes are outside advisory limits due to
the abundance of the target analyte in the sample.
Final Page Of Report
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s;a·,v,.~1 n1,ra:a.~
labor.ator:les 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382O
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 1
LOG NO
033820-1
033820-2
033820-3
033820-4
033820-5
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
G2 (0-0 .5)
G2 (0.5-1.0)
G4 (0-0.5)
G4 (0.5-1.0)
GS (0-0.5)
--------------------------------------------------
PARAMETER 033820-1 033820-2 033820-3
-----------------------------------------------------------
Antimony (6010), mg/kg dw <2.3 <2.3 <2.2
Dilution Factor 1 1 1
Prep Date 06.07.00 06.07.00 06.07.00
Analysis Date 06.08.00 06.08.00 06.08.00
Batch ID 0607D 0607D 06070
Percent Solids 86 88 81 -----------------------------------------------------------
DATE/
TIME SAMPLED
05-24-00/08:20
05-24-00/08:40
05-24-00/09:01
05-24-00/09:15
05-24-00/09:30
03382D-4 033820-5
--------------------
<2.4 <2.4
1 1
06.07.00 06.07.00
06.08.00 06.08.00
06070 06070
85 85
---------- ----------
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S,a v·a,n.n1a:h
t::'8bO'f3t01'.iE!S . .......,,,,._,.,, ........... ., ......... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTOj0S2300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 2
DATE/
LOG NO
03382D-6
03382D-7
03382D-8
03382D-9
03382D-10
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
GS (0.5-1.0)
G7 (0-0.5)
G7 (0.5-1.0)
G9 (0-0.5)
G9 (0.5-1.0)
PARAMETER 03382D-6
---------------------------------------
Antimony (6010), mg/kg dw <2.3
Dilution Factor 1
Prep Date 06.07.00
Analysis Date 06.08.00
Batch ID 0607D
Percent Solids 87
---------------------------------------
03382D-7 03382D-8
--------------------
<2.5 <2.3
1 1
06.07.00 06.07.00
06.08.00 06.08.00
0607D 0607D
BO BB
--------------------
05-24-00/09:40
05-24-00/10:00
05-24-00/10:05
05-24-00/10:25
05-24-00/10:45
03382D-9 03382D-10
--------------------
<4.9*F65 <2.3
2 1
06.07.00 06.07.00
06.09.00 06.08.00
0607D 0607D
82 86
--------------------
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S'a,,v: a, rr-'nia.h
l:.'aboratories ,a.,,,...,.,,.,..,,r,.n,l.-.•""'"·"" 5102 LaRoche Avenue· Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 3
DATE/
LOG NO
03382D·ll
03382D-12
03382D-13
03382D-14
033820-15
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
REP-01
TIME SAMPLED
05-24-00
05-24-00
05-24-00/11:10
05-24-00/11:20
05-24-00/11 :45
PARAMETER
REP-02
Gll (0-0.5)
Gll (0.5·1.0)
Gl0 (0-0.5)
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03382D-ll 03382D-12
--------------------
<2.2 <2.1
1 1
06.07.00 06.07.00
06.08.00 06.08.00
0607D 0607D
84 85
03382D-13 03382D-14 03382D-15
------------------------------
<2.3 <2.4 <2.4
1 1 1
06.07.00 06.07.00 06.07.00
06.08.00 06.08.00 06.08.00
0607C 0607C 0607C
86 85 85
--------------------------------------------------------------------- ----------
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s·a.v~al.nrn,a;h
L:clbOr'atO'rieS
,_,.,5....,,,..,.L.u><w•ION1.1no. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
- -----------------------------------------------------------------------------------
03382D-16 05-24-00/12:00 Gl0 (0.5-1.0)
03382D-17 05-24-00/13:40 Gl3 ( 0-0. 5)
03382D-18 05-24-00/13:58 Gl3 (0.5-1.0)
03382D-19 05-24-00/14:20 Gl7 (0-0.5)
03382D-20 05-24-00/14:35 Gl7 (0.5-1.0)
------------------------------------------------------------------------------------
PARAMETER 03382D-16 03382D-17 03382D-18 03382D-19 03382D-20
-------------------------------------------------------------------------------
Antimony (6010), mg/kg dw <2.1 <2.4 <2.1 <2.3 <2.1
Dilution Factor l l l l l
Prep Date 06.07.00 06.07.00 06.07.00 06.07.00 06.07.00
Analysis Date 06.08.00 06.08.00 06.08.00 06.08.00 06.08.00
Batch ID 0607C 0607C 0607C 0607C 0607C
Percent Solids 87 85 85 86 85
----------------------------------------------------------- --------------------
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S.a,v,a n:n·a;h t:3 b O ~a to~r i es ,...,..,..,.s.,. .. r...,,~,,,,,,.o,,., ""'-5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
05-24-00/15:00
05-24-00/15:05
05-24-00/15:40
05-24-00
----------- --------------------------------------------------
03382D-21 G16 (0-0.5)
03382D-22 G16 (0 .5-1.0)
03382D-23 G18 (0-0.5)
03382D-24 G18 (0.5-1.0)
----------------- -------------------------------- -----------------------------------
PARAMETER 03382D-21 03382D-22 03382D-23 03382D-24
-------------------------------------------------------------------------------
Antimony (6010), mg/kg dw <2.2 <2.1 <12*F65 <4.9*F65
Dilution Factor 1 1 5 2
Prep Date 06.07.00 06.07.00 06.07.00 06.07.00
Analysis Date 06.08.00 06.08.00 06.08.00 06.08.00
Batch ID 0607C 0607C 0607C 0607C
Percent Solids 82 85 79 81
-------------------------------------------------------------------------------
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S,a.v a,:nm a,h
ltab-Oi'.atoiies 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 6
SAMPLE DESCRIPTION, LIQUID SAMPLES LOG NO
03382D-25
03382D-26
--------------------------------------------------
EB-01
EB-02
--------------------------------------------------
PARAMETER
-------------------------------------------------
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
--------------------------------------- ----------
03382D-25
----------
<0.020
1
06.07.00
06.08.00
0607H
----------
DATE/
TIME SAMPLED
05-24-00/13:30
05-24-00/13:33
03382D-26
--------------------
<0.020
1
06.07.00
06.08.00
0607H
--------------------
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s: a11v· ai n' maih
t3bC)r8.tO'iies 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTOj052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------03382D-27
03382D-28
03382D·29
03382D-33
03382D-34
Method Blank
Lab Control Standard 'Ir Recovery
LCS Accuracy Control Limit ('1-R)
Method Blank
Lab Control Standard 'Ir Recovery
- ------------------------------------------------------------ -----------------------
PARAMETER 03382D-33 03382D·34 03382D-27 03382D-28 03382D-29
An,timony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
----------
<2. 0
1
06.07.00
06.08.00
0607D
----------
----------
99 "' 1
06.07.00
06.08.00
0607D
----------
----------
75-125 "'
06.07.00
06.08.00
----------
<2.0
1
06.07.00
06.08.00
0607C
100 %-
1
06.07.00
06.08.00
0607C
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S a·v a•.n:n ah
C:abo'r.atOr.ies 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN oo
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 11210069
REPORT OF RESULTS Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382D-37
03382D-38
03382D-39
03382D-40
Matrix Spike t Recovery (G7 0-0.5)
Matrix Spike Duplicate t Recovery (G7 0-0.5)
MS Accuracy Advisory Limit (tR)
Precision (tRPD) MS/MSD (G7 0-0.5)
03382D-41 MS Precision Advisory Limit (tRPD)
------------------------------------------------------------------------------------
PARAMETER 03382D-37 03382D-38 03382D-39 03382D-40 03382D-41
--------------------------------------------------------------------- ----------
Antimony (6010) , t 87 t 84 t 75-125 % 3.1 % <20 %
Dilution Factor 1 1
Prep Date 06.07.00 06.07.00
Analysis Date 06.08.00 06.08.00
Batch ID 0607D 0607D ----------------------------------------------------------- --------------------
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s, a1v-,a.n•n_aJ!
tabor.ator.ies ,..,._,o1s-mr,.,,,.....,,.,...,1no:. 5102 LaRoche Avenue· Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN oo
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 9
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
----------------------------------------------------------------------------- -------
03382D-42
03382D-43
03382D-44
Matrix Spike % Recovery (Gll 0.5-1.0)
Matrix Spike Duplicate% Recovery (Gll 0.5-1.0)
Precision (%RPO) MS/MSD (Gll 0.5-1.0)
------------------------------------------------------------------------------------
PARAMETER 03382D-42 03382D-43 03382D-44
Antimony (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
92 \-
1
06.07.00
06.08.00
0607C
89 \-
1
06.07.00
06.08.00
0607C
3. 3 \-
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Sta:v\ai,n n; ai h
l!:alfo~r.3tcir.r8'S 5102 LaRocheAvenue · Savannah, GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382D
Received: 25 MAY 00
Reported: 09 JUN 00
Client PO. No.: LTO#052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03382D-45
03382D-46
03382D-47
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
PARAMETER 03382D-45 03382D-46 03382D-47
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.020
1
06.07.00
06.08.00
0607H
98 %
1
06.07.00
06.08.00
0607H
75-125 %
-------------------------------------------------------------------------------
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, I.IB, and III.
Alternate digestion procedure in SW846, Method 3050B, Section 7.5 was
utilized for determining the antimony data.
*F65 = Elevated detection limits were reported due to sample matrix
interference which required sample or extract dilution.
Final Page Of Report
·---ARCADIS GERAGHTY & MILLER ---------------Laboratory Task Order NoJP.O. No. 6(2,3oc,-$, CHAIN-OF-CUSTODY RECORD Page _J_ of--3-
Project Number/Name NC:®"' Z.a-t-oz..10 I
Project Location -~:T~i=c~n'--f-/~c~t:1~~0,X=·=fu=-"LD='--f-/ --
Laboratory_~S-'--n...=-__,,.5~· "'=w "'"''-"~'-',.,=--"'"'-"H'-,.Lo.<huR,..,.$' __ _
~ .v .:11,~
.1) _y ✓ r-~ :,., Project Manager r,,. 51-\...-rrt !)' }J'
Sampler(s)/Affiliation ';Tefi= J..f:-a-LL ' L..l '-PLe-1.e,._.J ;:-/ I
rt. P..A-O~~(AiLC•1)1~ ..., .fj .i(
Date/Time c? <' J' <\; <r ~ Sample ID/Location Matrix Sampled Lab ID • ,
ANALYSIS/ METHOD/ SIZE I
Remarks Total
t.\ G-f -, ..s s---~-i-= l I
.c:, f--'---''2.=----'-'''-· <>_· ___ ,_, .:..s..,_ '--+---==----+-=1"1.,,_., "'o=-----+----+--.:.-+---+----1------l----+---+---------+-.:__-c:.u o-o, ~) s s-,i'~;;10> l I
) t-C-_7'---'--'(,1_. o_•-_1 -~>_,_:) __ -t--_,s-'----t--5_.i'""k=l'_,_,~ ..... -t----t-------,-1 -+---+---+----+----t----t-----------+--'i"----1
G-"\ (o-o.-,,) 5 5,"1,;1;.'l' I I
~ L..cc--q"--!__.L I,:_··...:."_-~' ·-=-.s:-L_1 _ _L__::s::.__L___1_~-~o'-Cc::" V<l!]I-c.o'---L_ _ _L__l.:....__j_ __ __1_ __ __j_ __ --1 __ --1...::·'---):=::::.·-=CJ__:D~3=-= .5::_.:cf~C:::-----,--+--'l'---
Total No. of Bottles/ JS
Containers ~~-
Sample Matrix: L = Liquid; S = Solid; A = Air
Relinquished by: \A.-\""'-~ 't:: ri7., '
• -"l .I. 1 I \.h/ Received by:
, I
Organization: Aft.c.~t~ ~ .......
Organization: .5-f,=-$-,, Date S / c.'J / =~
Date !;,-tZ "Ji oiJ
Relinquished by: ___________ Organization: ____________ Date 1 1
Received by: Organization: Date 1 1
Special Instructions/Remarks: I ,. £11"1 L __ T-,. Li..J I , -·
Time Ix·~°""
Time 9.',::,
Time ____ _
Time
Seal Intact?
@ No NIA
Seal Intact?
Yes No NIA
Delivery Method: □ In Person Common Carrier f'.g:p e--y, □ Lab Courier □Other
SPfflFY ----==-,-----
·---ARCADIS GERAGHTY & MILLER ---------------Laboratory Task Order No./P.O. No. OS::z:z.,-;c-,1\ CHAIN-OF-CUSTODY RECORD Page~ ot-4--
Project Number/Name ~~_n_rr-.•~2 O"UC I ANALYSIS/ METHOD I SIZE I
Project Location Jf'.;I;! /c_~ 0i f 0~ & /1....D ,.. J....)'-,. ,v • '.l . .).
Laboratory S.L , ►--o--._..A.,. L-.¼ :// :1," ~ijj} Project Manager tJ . .11-, ~:tr:; .J..( '\./ . 1 E ~
Sampler(s)/Affiliation ::J:. ~ . 1,::,, f'l.. '<co:, //!•¼f; ,-.,., (L,,,:~ FCM>LS) c;°/JJ4f fJf Datem e
Sample ID/Location Matrix Sampled Lab ID Remarks Total
f!-c.--P-0/ 5 5-L't-b:> i I -e..1,,-P•-<n-.J S-"2.-'t -v. I I
IZ-ts-P--u 3. .s S-"L-'t--=-I I ·-
G-11 Io-O,SJ s S"-"UJ -= I I~ lb I l
Git (a,s-,.c) S' S-"L't-Ou l I H!..,,..
G-l l ( I. <:,-J.-S) .s $"-"L>;-CO I I Ii •~S
(;.-10 'o-o.~) s 'S-U/-~~ i d{:t\\. i II'-"$ ~,"'-'1',,._ ::i"_ -5-"lJl-e<:> /'I ,11'~ (;-le, O, S-1. c) s I' 1(-s:, t . ··• ~1 ,, ,.., I
G-to / 1,c,-LS) 5 s--z..'t-<-<> I '-\~( ·. ,~r,\~ I I Z.; o.S
=-01 L $"-L'i-o.,
. •1~-11. c:. I ''·).Y1f ,t; ',-,,,. .(. I
S"-l..'i-al ~;" :>r.· E""'--en... L 1-,-...: .... I ~;'"-' I
El!>-Q3 L S-"Lli-""" I I ·,-,. ~ ~
6-13 6-<>· s) 5 s-_i.o;-= I I /:}'~ C,
c;.13 O,S-1,0) .s S--1..l/-,,,, /1,;c;t I I
G-n (1.0 -1.S) '5-Z...'I--=-( ' _,,::; ,<J()J.:SY' L--s l't10C I
Sample Matrix: L ; Liquid; s ; Solid; A; Air Total No. of Bottles/ iS" Containers
Relinquished by: U--1.~C: 'i:'. /7 -' P Organization: ;:,.-ru::: A'C, l $ fr-.:} M Date ~-1.J <-0 Time 1?, llJt, fe-BI Intact? R . db ~, LS ✓ ,✓ c;-11--.:s-~ =i 7 ~oc'.'.> 9.'/) ece1ve y: ( -Organization: Date Time No N/A I ll
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special Instructions/Remarks: I ~i(_. I ---Ql'OU·-_ _J ' ·' I ' -'' " ' . ,, ---. I ,.14 c, ' . ' --1-<...c --' _O ' <l ~»-t:,-=p\..,.,, C .,I lg .;.l,,: ,.I ode -e.-d
Delivery Method: D In Person ~Common Carrier A=> <£:"¥' D Lab Co~rier □Other _______ _
SPECIFY
~
;
~
r------------------ARcAms GERAGHTY & MILLER Laboratory Task Order No./P.O. No. on 3,(11:>-5 CHAIN-OF-CUSTODY RECORD Page~ ot--3-
Project Number/Name JUC:.OUU 2.-<n--C ·.i_ 1 C I ANALYSIS/ METHOD/ SIZE
Project Location ::reoLC/"l Q~~ ,i ,-...c_ #(/?
Laboratory :,TL {'5:-.uo..""""'~ l....lo~ (J} >
1Y '
Project Manager ,-J -J:bi:!;t;j"
Sampler(s}/Affiliation M-12+-o~ ::I H""4--J' l:t. )-?!
(.,u. p; •• I• 7/t.C.>'O<-") rf/'J Dateffime
Sample ID/Location Matrix Sampled Lab ID
Gn /o-as) s :,-VI-= 1-i·.Z..:S I
6-17 /o.S-1-o) 5 s--1..~-= l i~ I
G-17 /i.~-1-S) s S-1..-'·1-a:> f 4 · u.; I
C-IC, <.1-C, '.:i) s S"-U/-""' i-,h. --I
G-''-o.S-1,e) :s S-;}~:IZ"' I
G-1t /.<:,-I, S) s 5'-;;-;'C~ I
G--i ~ (i -(), >) 5 .5-~-:~ I
G--1~ / o, ( -1. o) s s-....,-«> i
&l'K ( J. u ·-I ,SJ -5 S-1..4-.:0 I
'{"'e---[3.ott;L_ I...
'
Sa_mple Matrix: L = Liquid; S = Solid; A= Air
Relinquished by: '""-1 .,.,..L '2.l'J ' -Organization: /,,,fl.. C.A-1:) I.,; 6:€} "" ... 4 .,,(',. .J'_/~ _J /1 Organization: 5.TL ~a,.) Received by:
'' ,, l,j
Relinquished by: Organization:
Received by: Organization:
Special Instructions/Remarks: i \..u.~ _... ----Q\J ~ ' ' I • "I _I -1 I .I .. ,,.,... ..J -1, •• • I . .. , '' --... , -' . .1 , _ _;_ •
' I I
J_,,..l~ c; 1 l!' ( I i .s:) ~
Delivery Method: □ In Person fiii Common Ca rrier_..,_F'eD-=-=::__.I!<)'>_· "------
sPEc1FY
•·. ......
'' ' ~ c_
~ '.;;. ,•· .
" "~/! _:Jc, .,,
. .
-Date :5 I ?...'1 I er<,
Date :J lz5 l:?"
Date I I
Date I I
,_. ' , • I ~ -• I ·~ -.._._,
Q
□ Lab Courier
I
Remarks Total
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,,..,_
,:;,· 0 ::>::Jo
Total No. of Bottles/ °I Containers
Time 1)1, C'<, Seal Intact?
Time 'i: ,::r ~ No N/A
Time Seal Intact?
Time Yes No NIA
I ' .., (~ . .,-... -I-<---,_ -I ' -~ -_,_
~ I~ J
□Other _______ _
SPECIFY
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S a,u.a "·'!ah L:.:aboratories ,_.,_,_.__, .... ;102LaRocheAvenue • Savannah,GA31404 • (912)3;4-7858 · Fax[phone]; • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller,-Inc.
P.O. Box 31388
LOG NO: S0-03382E
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LT0#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 144000615
REPORT OF RESULTS Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03382E-l REP-03 05-24-00
------------------------------------------------------------------------------------
PARAMETER 03382E-l
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<2.3
1
06.12.00
06.14.00
0612D
80
1
06.08.00
06.09.00
0608B
<0.46
1
06.12.00
06.14.00
0612B
Percent Solids 87
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Sa vra n n ah
Lab"or3toiies 5102LaRocheAvenue • Savannah,GA31404 • [phone] • Fm,[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03382E
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LT0#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 144000615
REPORT OF RESULTS Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
03382E-2
03382E-3
03382E-4
03382E-5
03382E-6
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010) , mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
03382E-2
<2.0
1
06.12.00
06.14.00
0612D
<4. 0
1
06.08.00
06.09.00
0608B
<0.40
1
06.12.00
06.14.00
0612B
03382E-3
95 %
1
06.12.00
06.14.00
0612D
103 %
1
06.08.00
06.09.00
0608B
100 %
1
06.12.00
06.14.00
0612B
03382E-4
75-125 %
75-125 %
80-120 %
-----------------------------------------------------------
03382E-5 03382E-6
·104 % 0.97 %
1
06.08.00
06.09.00
0608B
--------------------
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s:a v·a n.n a,h
t.:'3:b'ciratoriEi's
·--·-.. , .... ..-.lno. ;102 LaRoche Avenue · Savannah, GA 31404 • (912) 3;4-7858 • Fax [phone]; · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03382E
Received: 07 JUN 00
Reported:.15 JUN 00
Client PO. No.: LTO*052300B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 144000615
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
033828-7 LCS Precision Control Limit (Advisory) %RPD
PARAMETER 033828-7
Antimony (6010), t
Nickel (6010), %
Hexavalent Chromium (7196A), mg/kg dw
<20 %
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5:·a~v a1 rt n ah
t::abOra"tOries 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc_
P.O. Box 31388
LOG NO: S0-03382E
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 144000615
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03382E-8 Matrix Spike% Recovery (Batch)
03382E-9 Matrix Spike Duplicate% Recovery (Batch)
03382E-10 MS Accuracy Advisory Limit (%R)
03382E-ll Precision (%RPD) MS/MSD (Batch)
03382E-12 MS Precision Advisory Limit (%RPD)
--------------------------------------------------
PARAMETER
Antimony (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), \-
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
03382E-8 03382E-9 03382E-10
------------------------------
88 % 85 % 75-125 %
1 1
06.12.00 06.12.00
06.14.00 06.14.00
0612D 0612D
85 % 151 %X 75-125 %
1 1
06.08.00 06.08.00
06.09.00 06.09.00
0608B 0608B
100 % 101 !r 80-120 %
1 1
06.12.00 06.12.00
06.14.00 06.14.00
0612B 0612B
------------------------------
03382E-ll 03382E-12
3.5 % <20 %
56 \-X <20 %
1.0 \-<30 %
--------------------
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S a·v/a n n ah
t.aborataries ;102 LaRoche Avenue • Savannah, GA 31404 • (912) 3;4-7858 • Fax [phone]; • www.stlsavlab.com
LOG NO: S0-03382E
Received: 07 JUN oo
Reported: 15 JUN 00 Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Client PO. No:: LT0ll052300B
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 144000615
REPORT OF RESULTS Page 5
DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03382E-8
03382E-9
03382E-10
03382E-ll
03382E-12
PARAMETER
Matrix Spike% Recovery (Batch)
Matrix Spike Duplicate% Recovery (Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD (Batch)
MS Precision Advisory Limit (%RPD)
03382E-8 03382E-9 03382E-10 03382E-ll 03382E-12
X = MSD percent recovery failed advisory limits due to matrix
interference. The sample concentration was 80mg/kg dw and the spike level was 50mg/kg.
All other QA/QC samples were within the STL Savannah quality control
requirements.
Final Page Of Report
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s·a,v.a1n1·n1a,h
t"ab'o'1r·atol".ies
, _ _.s ... m,,.,.._........,.~,nc 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page l
DATE/
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436-1
03436-2
Gl (0-0.5)
Gl (0.5-1.0)
05-25-00/09:15
05-25-00/09:20
------------------------------------------------------------------------------------
PARAMETER 03436-1 03436-2
Hexavalent Chromium (7196A), mg/kg dw 0.54 0.60
Dilution Factor l l
Prep Date
Analysis Date
Batch ID
Antimony (6010),
Dilution Factor
Prep Date
Analysis Date
Batch ID
mg/kg dw
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
05.30.00
06.01.00
0530B
<2.3
l
05.31.00
06.01.00
0531A
35
l
05.31.00
06.01.00
0531A
05.30.00
06.01.00
0530B
<2.0
l
05.31.00
06.01.00
0531A
39
1
05.31.00
06.01.00
0531A
Percent Solids 88 90
RECEIVED
JUN 1 I.. 2000
ARCADfS Geraghty & Miller
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s.a·_~1a:ra:.n ~,,h Cab or.atones 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03436
Received: 26 MAY 00
Reported: OS JUN 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436-7
03436-8
03436-28
03436-29
03436-30
G20
G20
G21
G21
G22
(0-0 .5)
(0_5-1.0)
(0-0.5)
(0.5-1.0)
(0-0.5)
05-25-00/10:04
05-25-00/10:15
05-25-00/10:35
05-25-00/10:40
05-25-00/11: 00
------------------------------------------------------------------------------------
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
03436-7
----------
<0_45
1
05.30.00
06.01.00
0530B
<2.3
1
05.31.00
06.01.00
0531A
320
1
05_31.00
06.01.00
0531A
----------
03436-8 03436-28 03436-29 03436-30
----------------------------------------
<0.44 <0.52 <0.49 <0.56
1 1 1 1
05.30.00 05.30.00 05.30.00 05.30_00
06_01.00 06_01.00 06.01.00 06.01.00
0530B 0530B 0530B 0530B
<2.0 <2.4 <2-2 <5.6*F65
1 1 1 2
05.31.00 05.31.00 05.31.00 05.31.00
06.01.00 06_01.00 06.01.00 06.01.00
0531A 0531A 0531A 0531A
90 610 79 1700
1 1 1 2
05.31.00 05.31.00 05.31.00 05 .31.00
06.01.00 -06_01.00 06_01.00 06.01.00
0531A 0531A 0531A 0531A
----------------------------------------
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S•,a, v:·a.n·n;a,h
Lab0r'a't0ri8S ;102 LaRoche Avenue• Savannah, GA 31404 · (912) 3;4-7858 · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: OS JUN 00
Client PO. No.: LT0#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
G20
G20
G21
G21
G22
(0-0.5)
(0.5-1.0)
(0-0.5)
(0.5-1.0)
(0-0.5)
05-25-00/10:04
05-25-00/10:15
05-25-00/10:35
05-25-00/10:40
05-25-00/11:00
------------------------------------------------------------------------------------
PARAMETER 03436-7
Cyanide, Amenable (9010), mg/kg dw 7.9
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
10
05.31.00
05.31.00
0531T
110
10
05.31.00
05.31.00
0531S
88
03436-8
----------
1.3
2
05.31.00
05.31.00
0531T
8.5
2
05.31.00
05.31.00
0531S
90
03436-28 03436-29 03436-30
------------------------------
<1.0 3.8 <1.0
50 5 so
06.02.00 06.02.00 06.02.00
06.02.00 06.02.00 06.02.00
0602T 0602T 0602T
190 41 110
50 5 so
06.02.00 06.02.00 06.02.00
06.02.00 06.02.00 06 .. 02. 00
0602T 0602T 0602T
77 82 72
----------------------------------------------------------- --------------------
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S-a v a-.n,n,a h
L'ab-Oratorit!S 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN oo
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436-31 G22 (0.5-1.0)
PARAMETER 03436-31
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.56
1
05.30.00
06.01.00
0530B
<2.6
1
05.31.00
06.01.00
0531A
740
1
05.31.00
06.01.00
0531A
1.0
5
06.02.00
06.02.00
0602T
05-25-00/11:05
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S)1,W~ 'n ·l'!~_a,~h
L1aborator.1es
•-i,s.-.T .... .--.... 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTOj021199-A
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03436-31 G22 (0.5-1.0) 05-25-00/11:05
----------------------.--------------------------------------------------------------
PARAMETER 03436-31
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
57
5
06.02.00
06.02.00
0602T
71
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s·a v a n·n a.h t:a b(fratC:ir'i e·s 5102 LaRoche Avenue · Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN oo
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03436-9 REP-04 05-25-00
03436-10 REP-OS 05-25-00
PARAMETER
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03436-9 03436-10
11 7 .o
10 2
05.31.00 05.31.00
05.31.00 05.31.00
0531T 0531T
100 15
10 2
05.31.00 05.31.00
05.31.00 05.31.00
0531S 0531S
87 90
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S a·v ain.n:a;h
l[cib'(frat(lr.it?S
• .,,.,,...,s.-,,r,.,,,,,...,.,.,,.,,1n< ; 102 LaRoche Avenue • Savannah, GA 31404 • (912) 3;4-7858 · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
03436·11 EB-04
03436-12 EB-05
03436-13 EB-06
PARAMETER
Cyanide, Amenable (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
----------
--------------------------------------- ----------
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO~021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 7
DATE/
03436-11
----------
<0.010
1
05.31.00
05.31.00
0531T
<0.010
1
05.31.00
05.31.00
0531S
----------
TIME SAMPLED
05-25-00/09:40
05-25-00/09:43
05-25-00/09:45
03436-12 03436-13
---------- ----------
<0.010 <0.010
1 1
05 .31. 00 05.31.00
05 .31.00 05.31.00
0531T 0531T
<0.010 <0.010
1 1
05.31.00 05.31.00
05 .31. 00 05.31.00
0531S 0531S
--------------------
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S a,v a·n n1a•h Labor.atahes ,...,...,oos, .. mr,.,,,.....,,,... .. .,,._ 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCJ\DIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 8
DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03436-14
03436-15
03436-16
03436-17
03436-18
PARAMETER
Method Blank
Lab Control Standard ls Recovery
LCS Accuracy Control Limit (%-R)
Lab Control Standard Duplicate ls Recovery Precision (%-RPD) of LCS/LCSD
03436-14 03436-15 03436-16 --------------------

-
-
-
-
-
-
-
-
-
-
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.40 107 l, 80-120 l,
1 1
05.30.00 05.30.00
06.01.00 06.01.00
0530B 0530B
<2. 0 99 l, 75-125 l,
1 1
05.31.00 05 .31.00
06.01.00 06.01.00
0531A 0531A
<4.0 103 ls 75-125 ls
1 1
05.31.00 05.31.00
06.01.00 06.01.00
0531A 0531A
03436-17
100 ls
1
05.31.00
06.01.00
0531A
03436-18
l. 0 l,
104 ls 0.97 ls
1
05.31.00
06.01.00
0531A
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Sra,,v, a•n n· ah
t.£8bo-rat0rieS 5102 LaRoche Avenue , Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
CC: Mr. Mark Radecke
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 9
LOG NO
03436-14
03436-15
03436-16
03436-17
03436-18
REPORT OF RESULTS
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate t Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER 03436-14 03436-15 03436-16 03436-17 03436-18
Cyanide, Amenable (9010), mg/kg dw <1.0
1
05.31.00
05.31.00
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
0531T
<1.0
1
05.31.00
05.31.00
0531S
95 % 85-115 %
1
05.31.00
05.31.00.
0531S
102 %
1
05.31.00
05.31.00
0531S
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
7.1 %
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s a,v,a n n:a.1h
L::abOr:atO'~ie"S 5102 LaRoche Avenue· Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO~021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
03436-19 LCS Precision Control Limit (Advisory) %RPO
PARAMETER 03436-19
Hexavalent Chromium (7196A), mg/kg dw
Antimony (6010), %
Nickel (6010), %
Cyanide, Amenable (9010), mg/kg dw
<20 %
<20 %
Cyanide, Total (9010), mg/kg dw <30 t
------------------------------------------------- -------------------- ----------
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
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S a/v a,'n n a,h
l:!abO'ratOFi8'S 5102 LaRoche Avenue· Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LT0#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 11
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED ------------------------------------------------------------------------------------
03436-32 Matrix Spike 'Ir Recovery
03436-33 Matrix Spike Duplicate 'Ir Recovery
03436-34 MS Accuracy Advisory Limit ('lrR)
03436-35 Precision ('lrRPD) MS/MSD
MS Precision Advisory Limit ('lrRPD) 03436-36
PARAMETER
--------------------------------------------------
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), 'Ir
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), 'Ir
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
03436-32
84 'Ir
1
05.30.00
06.01.00
0530B
30 'lr*F73
1
05.31.00
06.01.00
0531A
141 'lr*F61
1
05.31.00
06.01.00
0531A
----------
03436-33
86 'Ir
1
05.30.00
06.01.00
0530B
27 'lr*F73
1
05.31.00
06.01.00
0531A
153 'lr*F61
1
05.31.00
06.01.00
0531A
----------
03436-34
80-120 'Ir
75-125 'Ir
75-125 %-
----------
03436-35 03436-36
1.1 'Ir <30-'Ir
11 'Ir <20 'Ir
8.2 'Ir <20 'Ir
--------------------
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S a\vra• "~" a h taborator:ies 5102 LaRoche Avenue· Savannah, GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 12
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03436-20 Matrix Spike\-Recovery [G20 (0.5-1.0)]
03436-21 Matrix Spike Duplicate\-Recovery [G20
(0.5-1.0)]
03436-22 MS Accuracy Advisory Limit (%R)
03436-23 Precision (\-RPD) MS/MSD [G20 (0.5-1.0)]
03436-24 MS Precision Advisory Limit (\-RPD)
------------------------------------------------------------------------------------
PARAMETER 03436-20 03436-21 03436-22 03436-23 03436-24 ---------------------------------------
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010), mg/kg dw *F61 *F61 75-125 \-*F61 <30 %
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S a:.v·a n·n:a,h llaD'o·r·atOr:ieS • ...,..,.or,.,,.mr,.,.uoo,,.,,.,_,,.._ 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
· Received: 26 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#021199·A
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 13
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
-----------. -------------------------------------------------------------------------
03436-37
03436-38
03436·40
Matrix Spike% Recovery [G22 (0·0.5)]
Matrix Spike Duplicate% Recovery [G22 (0·0.5)]
Precision (%RPO) MS/MSD [G22 (0·0.5)]
---------------------------------------------------- --------------------------------
PARAMETER 03436·37 03436·38 03436·40
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010), mg/kg dw *F61 *F61 *F61
------------------------------------------------- ------------------------------
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S:a,~v:,~·n 91_a.h L'aboratories ,_,._,.r .... ~ ..... 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03436
Received: 26 MAY 00
Reported: 05 JUN oo
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 15240065
REPORT OF RESULTS Page 14
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- -------------------------------------------------------------------------
03436-25
03436-26
03436-27
Method Blank
Lab Control Standard\-Recovery
LCS Accuracy Control Limit (\-R)
------------------------------------------------------------------------------------
PARAMETER
-------------------------------------------------
Cyanide, Amenable (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03436-25 03436-26 03436-27
<0.010
1
05.31.00
05.31.00
0531T
<0.010
1
05.31.00
05.31.00
0531S
95 \-
1
05.31.00
05 .31.00
0531S
85-ll5 \-
--------------------------------------- ---------- ------------------------------
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S·a:v"a_ n,ni a~h
l'.!'abo'r:atofies 5102 LaRoche Avenue· Savannah, GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436
Received: 26 MAY 00
Reported: OS JUN 00
Client PO. No.: LT0#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 15240065
Page 15
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436-25
03436-26
03436-27
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
03436-25 03436-26 03436-27
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, IIB, and III.
All other QA/QC were within established control limits.
Antimony MS/MSD failed advisory limits due to matrix interference. The
sample contained <2.3 mg/kg dw Sb and the spike level was SO mg/kg.
Nickel MS/MSD failed advisory limits due to abundance of target analyte
present in the sample. The sample concentration was 320 mg/kg dw and the
spike level was 50 mg/kg.
Cyanide MS/MSD failed advisory limits for sample G20 (0.5-1.0)-and G22
0-0.5) due to abundance of target analyte. The spike concentration for
cyanide is 4.0 mg/kg.
*F61 = The recoveries of the matrix spikes are outside advisory limits due to
the abundance of the target analyte in the sample.
*F65 = Elevated detection limits were reported due to sample matrix
interference which required sample or extract dilution.
*F73 = Matrix spike recoveries were outside advisory limits due to matrix
interference present in the sample.
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, nl;J!_UfllUn cui~e remov1m ,or nec1p1ems n:corns
_ S,;, .-1 ':;.:· · .~.) ! .) FedEx Tracking Number
:Ompany
1dress
\-'"fnal Billing Reference
816911438041
Phone
&
,.
-------------------~
ARC/. ..> GERAGHTY & l,11LL:R Laboratory Task Order No./P.O. J\ ;$~=-.c. CHAIN-OF-CUSTODY RECORD PagL ,---of....:z.._
------Project Number/Name t,/LOL<"t,Z,cn c ;:,.1 c
/~. i ANALYSIS/ METHOD/ SIZE
ProJ·ect Location :JED/ flcr c M C?-rn-el r>C -(._ ' l ~ i
Laboratory_~S .... TI.u...-.:¾=v.uo,.,o=cuccci,..,l.,=~~l~,~k....,5~--
Project Manager N· s l. trj
Sampler(s)/ A ffi I iation ~ f!-;arn ~ ! • c.:: ::I~
L.:J .. PL<...~ C ...,._c..,,..-., ..r)
Date/Time
Sample ID/Location Matrix Sampled Lab ID
&-1 /o-o.~) I s ! r-2.s-= "L' ~
G-1 / o ,-1,o) I ' S"-1f,-'-"" ::. •Z e
G-1 /10 I, S") I s i S:U-= a,z.L
{;-'LC' ( 6 -0, S) I ' ',-ZS-= .s ' ' I J ,..,, C -_;
~20 / 6,S-/.c:,). i s I 5-l.S-~ I /Oi/C:
I ,-z.s-= (,,-?..C / f_c, -1.(') s I i i,,; I "i;
~E"P-C'f I s I 5--1..s-= -
f-'.c-?-CS i s 5--1..s--= I -' S--z. S-<= I P-c?--Oo I $ I -
! ,-·u..c. ce-o-i L "-'• -
ct,-cS I s--i.,-=
I L. Ci: -..:i
e'e-Ob i L ,-u-cc
' "''"" G-7-1 / o-c. J'\ I ,--z..r-= s ' lC,., 't" -, I I s--zs-= G-z...1 /o.;-1. d 5 I,.., . ._,,,.._
. .
I . . \ . /
·._./
,I' .KJ; V / (j . .::! ~ 9-,? . ._;' f.. d'
,'f... ft ,,.g'.J ... :f 1.t . .g-s ... -'l' , "k
r cf --<''"' ·:·...U tc:f..._;,; f: ~ -r~ , , o, , of ... ,:, :/"-'''J!r.;:.,3 <-;·_,,J<-?,;,}q · 'J)ft-..., ~ "I'<'-' "i<s "I< (.I 7 ·
t r
I ' I ;
'/ I/ I
/~-X~: I / I
A"r,Z;.. I .· I .• I I / I ' I I
. I ' .. · -
-r· /
I
/ I/'_,,
I 1 /
, '/ I
, ' I , , /
/ ;
t I
Remarks Total
z:..
L
-.. 2..
2-
z.
z.
I
I
I
I
I
I
2..
L
I s S-}S'-CAI> /,/ ( -z_ p r_, I fl o-I. SJ I Total No. of Bottles/ 2. 'J --.
Sample Matrix: l -liquid; s -Solid; A -Air Containers
Relinquished by: l>--1~12-"<'r.:J. I ' Organization: ~=-s ~ /::'.> Date S" l~S l ~1 Time /3!a,. Seal Intact?
Received by: /<C. \~ -Organization: _5.tL5+\--Jc.aL..-Date , l z, I ao Time q,; )o Yes No N/A
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A -Special Instructions/Remarks: ~.L.A...J ,.,, ,-t-/r1ll'i 1 -f • ,...__ 'I I ' A,, ,-. t • -' . ., -~ . I I u
.C, i·o I i >,£RI.I-=r:➔,e-,-, e·1";0c· r, ~ :-::;, ;o,,-e n• s -...l -~J
- - - - - - -------· - - - - - - -(~
ARCJ ) GERAGff,y & MILLER Laboratory Task Order No./P.O. ~ :, Si 3C?-O CHAIN-OF-CUSTODY RECORD Pag,. ~ of ___b_
Project Number/Name -~N~c._._-4~_,.__-,_,__,7-c=e?-'--'o'"'-"2.."1-'o'---_
Project Location __ ::r~F=~,"f)-~ ... F~I Le ... c-c,/<-c.=""'-'-----"c."':,c:cK=1-:;::, 1 ,-.,,c:,
Project Manager _ _J::,/-J~-.-!J~~l--::,·;,c%~t---------
Sa mp I e r(s)/ A ff i Ii at ion _J4"-L> ~.1:i?l;,3.:.--'' ,;,< ,.. ~,,.___:;r,L_. -11-4-.L/=bte!.,;_
Date/fime
Sample ID/Location Matrix Sampled Lab ID
s I s-1.s-e,;;;, I 1,-r,0
s I S"-tl-= ! II· CS
&,.0 G ?,,1,, ( 1. o-L c) s I S"-"l.S-c-" ' Ii· C;;
I ~,---..c:::::.,, ~ L-. i . i !
I
I
!
•
I
I
I
I
I
Sample Matrix: L = Liquid; S -Solid; A = Air
I ANALYSIS/ METHOD/ SIZE
I I
I
Relinquished by: ~ x;_g 1_-e. Organization:_f;.4-MitSd.".:OW>.S.'+>>Jl..:"";:_-'c-:::'=-:fc!:/--"H"---Date S:: /-z-5
Received by:~r:_c.. __ ..::;--;i.:~~-------Organization: HL-&,<,l...i-Date > / 2£ '= / C'C
Relinquished by: Organization: ____________ Date _ _,_, _ _,_, __
Received by: Organization: Date _ _,_, _ _,_, __
Special Instructions/Remarks: :t±:<:! u:J J J c; ::e ) r , p I J-c 1. -,? o--\= 4<> f;z) u...L,,.;J
Au, ,;:,,rl,-. -::::,::.. • 0 ,., or; e, ... 1 _J ::nr::r--e----
-,/.A G"L:,: / 0-o, s:) G--Z.2.. { ,_ 's:)
11
Q
"-'TL,,
r1i h,
Remarks Total
-z...
Total No. of Bonles/
Containers
Time -1.i-"!,,.,,_,=cc· ,,,__
Time _9.t..=-= .=..$.:..."--
Time ____ _
Time ____ _
Seal Intact?
Yes No N/A
Seal Intact?
Yes No N/A
o• f \
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I
RECEIVED
JUN 1 2 2000 $,a ,y a~"· n~_a)'!
L:abatator1es ,_.,s-,,r, ... ..__,.,_1nc 5102 LaRoche Avenue · Savannah, GA 31404 · [phone] • Fax [phone] • WJVWi[lS§Wel(lill AR lS-Gerag ·'f
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436A
Received: 26 MAY 00
Reported: 08 JUN 00
Client PO. No.: LTO#052300-B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
03436A-l Gl (0-0.5)
03436A-2 Gl (0.5-1.0)
-------------------------------------------------------------
PARAMETER
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
03436A-l
<4.l*F65
2
06.07.00
06.08.00
0607C
88
05-25-00/09:15
05-25-00/09:20
03436A-2
<2.0
1
06.07.00
06.08.00
0607C
90
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I
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I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
S a, v a n n,'a'.h 1.!:'abOratOf.ieS
.-..,,o111o...,,,.,.u.., ... ,,.., .. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436A
Received: 26 MAY 00
Reported: 08 JUN 00
Client PO. No.: LTO#052300-B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436A-3 05-25-00/10:04 G20 (0-0.5)
03436A-4 05-25-00/10:15 G20 (0.5-1.0)
03436A-5 05-25-00/10:35 G21 (0-0. 5)
03436A-6 05-25-00/10:40 G21 (0.5-1.0)
03436A-7 05-25-00/11:00 G22 (0-0.5)
------------------------------------------------------------------------------------
PARAMETER 03436A-3 03436A-4 03436A-5 0343 6A-6 03436A-7
-------- -----------------------------------------------------------------------
Antimony (6010), mg/kg dw <2.1 <2.0 <2.4 <2.2 <5.l*F65
Dilution Factor l l l l 2
Prep Date 06.07.00 06.07.00 06.07.00 06.07.00 06.07.00
Analysis Date 06.08.00 06.08.00 06.08.00 06.08.00 06.08.00
Batch ID 0607C 0607C 0607C 0607C 0607C
Percent Solids 88 90 77 82 72 -------------------------------------------------------------------------------
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I
S,a1v a n-n.a•h l:abo'r3torie"s
'"N""°"'S..0mTt ... L.>o0,-."1< 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADI_S Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436A
Received: 26 MAY 00
Reported: 08 JUN 00
Client 'po_ No.: LTO#052300-B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03436A-8 G22 (0.5-1.0) 05-25-00/11:05
PARAMETER 03436A-8
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
<2.6
1
06.07.00
06.08.00
0607C
71
----------------------------------------------------------- --------------------
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I
s·a;v a1n,n\a1h
Uab6{at0f.iE!S 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03436A
Received: 26 MAY 00
Reported: 08 JUN 00
Client PO. No.: LTO#052300-B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03436A-9
03436A-10
03436A-ll
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
PARAMETER 03436A-9 03436A-10 03436A-ll
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<2.0
1
06.07.00
06.08.00
0607C
100 %
1
06.07.00
06.08.00
0607C
75-125 %
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
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SYaiV/1a: n,:r.a h
L::.aborator.les 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
LOG NO: S0-03436A
Received: 26 MAY 00
Reported: 08 JUN 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Client PO. No.: LTO#052300-B
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 11210069
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
03436A-15
03436A-16
03436A-17
03436A-18
03436A-19
Matrix Spike%-Recovery (G22 0-0.5)
Matrix Spike Duplicate%-Recovery (G22 0-0.5)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD (G22 0-0.5)
MS Precision Advisory Limit (%-RPD)
PARAMETER 03436A-15 03436A-16 03436A-17 03436A-18 03436A-19
Antimony (6010), %-
Dilution Factor
Prep Date
Analysis Date
Batch ID
95 %-
2
06.07.00
06.08.00
0607C
92 %-75-125 %-
5
06.07.00
06.08.00
0607C
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, IIB, and III.
3. 2 %-
Alternate digest suggested in SW846, Method 3050B, Section 7.5 was
utilized to obtain antimony results and QA/QC.
*F65 = Elevated detection limits were reported due to sample matrix
interference which required sample or extract dilution.
Final Page Of Report
<20 %-
- - - - ---- ------ - - --0.'
ARC,L. J GERAGHTY & 1,11LLER Laboratory Task Order No./P.O. I\ 1S:Do::,-.C
------
CHAIN-OF-CUSTODY RECORD
' Pag~ .---of...2-.....
' N CQ:L. ~ 7,.c,7 Q L-l o I h
; );· i
Project Location :TED I flu· c M cr,0 frvl., t->C _, '. ! / ~ ;J [ c3 / r 1 .'-' •" r
:;; s::... ' l,.._ ( • r ·,,. //1 :f, > J-1 ;. J ,~ ...,. 1'l .> ...:I _ _,. .J~/~
:Q-,,o..,c:,a...-,-1o > \ ___ ,,., / J1.f"u• / fv ,u-··f I fu,,-.. 0·",/'' ✓ I ju" jJ' <•9/ f
Project Manager N · ,J' · ':Cj I./ /,. ! CJ I (: :!'J.J / 1"' {. J'
Sampler(s)/Affiliation t:'::::: t'-:!n?=, ·,:;: ::y tt,,--u. , ,:J I{ , ,..g, .., , ~ f:t ·-D , -'t , v Jt,
L;...> '· PL~I..Lc,,-., C ,-..,-_c.,,,.-r, '-0 ( '-i ' ~ '-, ,u [ if ..., 1 'j f .! ~ -f bl.
.if -..,,j) c;' :., \ 3 .._,5; '_;\ J s' ::, '} ti f-j) .!o':J f-. y -< '/ ')' -? c..., ' < ..!f °I < u ~ Q • '
Project Number/Name ANALYSIS/ METHOD/ SIZE
Laboratory
Sample ID/Location Matrix
Date/Time
Sampled Lab ID Remarks Total
s I 5"-2.5-o-<>
<a,o( I r /
s I S"-:¥,-'-"-' •2 e I ; I i
@~G-_,1-i/~1_. o~--'-· _S)~----c-----,~-'-7~-t---+---+---t--~t--,---;----+----+--------_---+_L=----J
c;.{c' (6-o,s) \ 2.
s
I
i S:,U-00> q,z.l
' S"-ZS-=
,1 1/
/
I 5 I , ,..... e-..; Y(~· ,.(~ I /
r: . .-z.c(6,S-J.<>) ( I s I 5-?.S-c.-:>
IO ,1< ,!"',,z.. I / ,
I s i
I
s:--z.s--= lr,:I~ I I /
I s I :5--'t.S-GO ; -I s I
y'tS"-=
I 5 I
5-.,_ 5-=> -
L ,--is-<.:..
, G, ! ., ..
E13-o.S L. . ' :s-·cr-=
9:'-'3
I '
' L ,-u-= j "l:'<<
s ! s--~s-oe / , ,
I I ' lC ., -r I
5 ! S'-~s--o<:> / I
;
1r,·""r,,.. t j
s I 5-~5'--CA-l I (
--.
Sample Matrix: L = Liquid; S = Solid; · A = Air
Relinquished by: V--\ ~a,_~ r-2 1 • Organization:...L&-c='°""'p.,,..,.,._,~C?e;~,,;'-"b:l.._ ___ Date S I JS 1,,...,
Received by: 1<4=--i '--\ -Organization: 9rL ,s.+v~ Date 5" I 2< I 00
z.
z.
I
I
\
'2..
L
2.
Total No. of Bottles/ 2 ':{
Containers
Time _,_1,,3:..:.!.=a::.=--
Time _ __,'1_'-'-1_0 __
Seal Intact?
Yes No N/A
Relinquished by: ___________ Organization: ____________ Date _ _,_, _ _,_, __ Time-----
Received by: Organization: Date ' ' Time-----
Seal Intact?
Yes No N/A -, -· Special Instructions/Remarks: i-i .A ...J -" i J .-, -/ r 1 ° i • &
I ,,.o:;;:. I I . J A,, ... I -,
4:U. c;..tf,.,.,, ck, f i..~,o .I i -:;--ee4::: :::::r:._o,., coo-·,,.. rt
. I
=;-, ........... ~-I -. h;:-l""L'") .J I \..__ ...... '-
u
-
- - - - --- -------· --- - - - -(.~
ARC/ ) GERAGfiTY & MILLER Laboratory Task Order No./P.O. ~ ::is23,:,o-O CHAIN-OF-CUSTODY RECORD Pag, ~ of__k_
· Project Number/Name Ne 01 :v -z...c2 o 2..1 o I ANALYSIS/ METHOD/ SIZE I
Project Location -::r F 1') El~ C /_ C.,..., Id I
) G:-C~>-.DtNC:. 0 r 'w· :/
Laboratory ~"'< ~S-'Sdl.!.::"~ L,.b c:,uJ-e ~' A z~"' -J+--.:r:s: ~ --1' CJf,,,
Project Manager N--:f ](;1.t~J
Sampler(s)/Affil iation 4 JI 0.-, \ < r, ::r. 1-!,..l/ _,. ._J-J . ' ::, 'l ?-.!:;"":--_v
Date/Time t-; -l;...ei. ~ :.; f~ i!.
Sample ID/Location Matrix Sampled Lab ID 'V . cy< ' Remarks Total
G---z..z. fo-c-r) s I s-1.s-= I I I f I ,·r,0 --z_
G-l-c. ( o. ,-1 -cJ s ! s---..S-= ll · cS I l ' .: <....
~ Gz:i. ( ,.o-/. ,) s I S" -"l.S-c-" Ii [ / I 11 • 0~ -z....
~, .... -tcaa....~ ~ L--I . I !
I I
I ! .
f
I . ' ' -
I I I -'
;
I > ' '
I I ' !
I I ' I !
I i • Total No. of Bottles/ G, Sample Matrix: L -Liquid; s -Solid; A -Air Containers
Relinquished by: ~ '2(} i -;e, Organization: ~~IS: ~"" Date ::.: IV:. I=. Time j~;c...::::::,. Seal Intact?
Received by: [: l.----. Organization: • r L-S-, lJ.._ Date S"" I z• I <'c Time <J.: $0 Yes No NIA
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date ( I Time Yes No NIA
Special Instructions/Remarks: .-~-1 .. ,,..... I. .J ' -r,..,.--. ll l _j '' :, . .. ' " tL., ,...J '' I I u
~D l..:.... ee ! e. ::C,. < o o-r: e,
,/-A ½cc• olr G-z..7 /o o, s:)
...J ::n r:::r:...e-::--::::n-r:::b:'2+ ct: -0
<f G-'2-2. ( I -I c:)
ill b i C -,.Yi d~
I
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I
S:a' v•a~n1,n 1a• h
l::a b Or at Of i es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 163800717
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
04471-1 G3 (0-0.5)
04471-2 G3 (0.5-1.0)
04471-3 G12 (0-0.5)
04471-4 G12 (0.5-1.0)
04471-5 G14 (0-0.5)
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
04471-1 04471-2
--------------------
<0.45 <0.43
1 1
07.10.00 07.10.00
07.11.00 07 .11. 00
0710B 0710B
<2.1 <2.2
1 1
07.11.00 07.11.00
07 .11. 00 07.11.00
0711I 0711I
190 9.8
1 1
07.10.00 07.10.00
07.11.00 07 .11.00
0710D 0710D
88 92
04471-3
----------
<0.44
1
07.10.00
07 .11.00
0710B
<2.2
1
07.11.00
07.11.00
0711I
30
1
07.10.00
07.11.00
0710D
90
07-06-00/09:25
07-06-00/09:25
07-06-00/11:15
07-06-00/11:20
07-06-00/11:30
04471-4 04471-5
---------- ----------
<0.43 <0.48
1 1
07.10.00 07.10.00
07 .11.00 07 .11.00
0710B 0710B
<2.2 4.9
1 1
07.11.00 07.11.00
07.11.00 07.11.00
0711I 0711I
14 450
1 1
07.10.00 07.10.00
07 .11. 00 07.11.00
0710D 0710D
92 82
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I
I
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I
I
~ al_v..,a. n_..n .a.h
Laboratories 5102 La.Roche Avenue• Savannah, GA 31404 • [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
04471-6 Gl4 (0.5-1.0) 07-06-00/12:00
PARAMETER 04471-6
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0 .47
1
07.10.00
07.11.00
0710B
10
2
07.11.00
07.11.00
0711!
1200
5
07.10.00
07.11.00
0710D
Percent Solids 85
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I
I
I
I
S1,.a v atn1 n ah
Labor'atorie's 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 163800717
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
04471-7
044 71-8
04471-9
04471-10
04471-11
G6 (0-0.5)
G6 (0.5-1.0)
GB (0-0.5)
GB (0 .5-1.0)
Gl9 (0-0.5)
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
04471-7
<0.43
1
07.10.00
07.11.00
0710B
<2.0
l
07.11.00
07.11.00
0711I
88
l
07.10.00
07 .11.00
0710D
----------
04471-8 04471-9
<0.43 <0.48
1 1
07.10.00 07.10.00
07.11.00 07.11.00
0710B 0710B
<2.2 19
l 5
07.11.00 07.11.00
07 .11.00 07.11.00
07llI 07llI
74 4300
l 5
07.10.00 07.10.00
07.11.00 07.11.00
0710D 0710D
--------------------
07-06-00/09:55
07-06-00/10:05
07-06-00/10:35
07-06-00/10:40
07-06-00/12:30
04471-10 04471-11
7.7 <0.46
1 l
07.10.00 07.10.00
07.11.00 07.11.00
0710B 0710B
16 2.9
5 2
07 .11.00 07 .11.00
07.11.00 07.12.00
0711I 071lI
3600 380
5 l
07.10.00 07.10.00
07.11.00 07.11.00
0710D 0710D
--------------------
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Sa v,a n,n.a h
l!8b0rator,ie's 5102LaRocheAvenue • Savannah, GA31404 · [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00-0232
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 163800717
Page 4
DATE/
LOG NO
04471-7
04471-8
04471-9
04471-10
04471-11
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
G6 (0-0.5)
TIME SAMPLED
07-06-00/09:55
07-06-00/10:05
07-06-00/10:35
07-06-00/10:40
07-06-00/12:30
G6 (0.5-1.0)
GS (0-0.5)
GS (0.5-1.0)
Gl9 (0-0.5)
PARAMETER 04471-7
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
<1.1
2
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010),
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
07.10.00
07.11.00
0710S
mg/kg dw 9.0
2
07.10.00
07.11.00
0710S
91
04471-8
<1.1
2
07.10.00
07.11.00
0710S
14
2
07.10.00
07.11.00
0710S
91
04471-9
64
200
07.10.00
07 .11.00
0710S
590
200
07.10.00
07.11.00
0710S
82
04471-10 04471-11
---------- ----------
20 <l. 2
20 50
07.10.00 07.10.00
07.11.00 07.11.00
0710S 0710S
110 51
20 50
07.10.00 07.10.00
07.11.00 07.11.00
0710S 0710S
82 86
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S_a,v.a·n n~a h
LaboratcirieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 5
LOG NO
04471-12
04471-13
04471-14
04471-15
04471-16
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
G19 (0.5-1.0)
G21 (0-0.5)
G21 (0.5-1.0)
REP-07
REP-08
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
044 71-12 044 71-13 04471-14
-------------------- ----------
<0.49 <0.51 <0.51
1 1 1
07.10.00 07.10.00 07.10.00
07.11.00 07.11.00 07.11.00
0710B 0710B 0710B
4.2 6.2 5.6
2 1 1
07 .11.00 07.11.00 07 .11.00
07.12.00 07.11.00 07 .11.00
0711I 0711I 0711I
600 1000 710
1 5 1
07.10.00 07.10.00 07.10.00
07 .11.00 07.11.00 07.11.00
0710D 0710D 0710D
------------------------------
DATE/
TIME SAMPLED
07-06-00/12:35
07-06-00/13:10
07-06-00/13:15
07-06-00
07-06-00
04471-15 04471-16
<0.47 <0.48
1 1
07.10.00 07.10.00
07.11.00 07.11.00
0710B 0710B
22 22
5 5
07.11.00 07.11.00
07.12.00 07.12.00
0711I 0711I
3400 4100
5 5
07.10.00 07.10.00
07.11.00 07.11.00
0710D 0710D
--------------------
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SJa1 v•a1 n• n a h
Laboratories 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Recefved: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 6
LOG NO
04471-12
044 71-13
044 71-14
04471-15
04471-16
SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
Gl9 (0.5-1.0)
G21 (0-0.5)
G21 (0. 5-1. 0)
REP-07
REP-08
PARAMETER 04471-12 044 71-13 04471-14
-----------------------------------------------------------
Cyanide, Amenable (9010), mg/kg dw <1.2 <1.3 <1.3
Dilution Factor 50 20 10
Prep Date 07.10.00 07.10.00 07.10.00
Analysis Date 07 .11.00 07.11.00 07 .11.00
Batch ID 0710S 0710S 0710S
Cyanide, Total (9010) , mg/kg dw 140 50 39
Dilution Factor 50 20 10
Prep Date 07.10.00 07.10.00 07.10.00
Analysis Date 07.11.00 07 .11.00 07.11.00
Batch ID 0710S 0710S 0710S
Percent Solids 81 78 77
------------------------------------------------- ----------
DATE/
TIME SAMPLED
07-06-00/12:35
07-06-00/13:10
07-06-00/13 :15
07-06-00
07-06-00
04471-15 044 71-16
--------------------
150 <1.2
200 25
07.10.00 07.10.00
07.11.00 07 .11.00
0710S 0710S
650 89
200 25
07.10.00 07.10.00
07.11.00 07.11.00
0710S 0710T
83 82
--------------------
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S,a .v,1a1,n, n_.a,h L'a'bor·ati:irieS 51021.aRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL oo
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
07-06-00/10:05
07-06-00/10:15
04471-17
044 71-18
PARAMETER
EB-07
EB-08
Cyanide, Amenable (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010),
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), rng/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
rng/1
04471-17
<0.010
1
07.10.00
07.11.00
0710T
<0.010
1
07.10.00
07.11.00
0710T
<0.020
1
07.10.00
07.11.00
07101
<0.040
1
07.10.00
07 .11. 00
07101
04471-18
<0.010
1
07.10.00
07 .11.00
0710T
<0.010
1
07.10.00
07.11.00
0710T
<0.020
1
07.10.00
07.11.00
07101
<0.040
1
07.10.00
07 .11.00
07101
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S a1.v,a1,n1n:a h
L'aboratcfries • .......,,,,.-.,r,.,.~ .... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
07-06-00/10:05
07-06-00/10:15
04471-17
04471-18
PARAMETER
EB-07
EB-08
Hexavalent Chromium (7196A), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471-17
<0.010
1
07.07.00
07.07.00
0707A
044 71-18
<0.010
1
07.07.00
07.07.00
0707A
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Sa v a]n n a'h r:"abOratCiries
• ...,...,,.._,,,r,.,ol.obora""1H,"" 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163 80071 7
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION ,. LIQUID SAMPLES TIME SAMPLED
04471-19 EB-09 07-06-00/10:45
PARAMETER 04471-19
Hexavalent Chromium (7196A), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.010
1
07.07.00
07.07.00
0707A
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S'.a,v1•a·n.n a·h
taboi'.'8torie·s 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By:_ Client
Code: 163800717
REPORT OF RESULTS Page 10
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
Method Blank
Lab Control Standard%-Recovery
LCS Accuracy Control Limit (%R)
04471-20
04471-21
04471-22
04471-23
04471-24
Lab Control Standard Duplicate% Recovery
Precision (%-RPD) of LCS/LCSD
PARAMETER
Hexavalent Chromium
(7196A), mg/kg dw
Dilution F'?-ctor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471-20 04471-21
<0 .40 97 %
1 1
07.10.00 07.10.00
07.11.00 07 .11. 00
0710B 0710B
<2.0 98 %-
1 1
07.11.00 07.11.00
07.11.00 07.11.00
07111 07111
044 71-22
80-120 %-
75-125 %-
Nickel (6010), mg/kg dw
Dilution Factor
<4.0 105 %-75-125 %-
Prep Date
Analysis Date
Batch ID
1 1
07.10.00 07.10.00
07.11.00 07.11.00
0710D 0710D
04471-23
98 %-
1
07.10.00
07.11.00
0710B
99 %-
1
07.11.00
07.11.00
07111
04471-24
1. 0 %-
1. 0 %-
106 %-0.95 %-
1
07.10.00
07.11.00
0710D
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S,a v,a n1n,a,h
l.!abo'r8tories 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 11
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
04471-20
04471-21
04471-22
04471-23
04471-24
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
PARAMETER
Cyanide, Amenable
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471-20
(9010), mg/kg dw <1.0
1
07.10.00
07.11.00
0710T
Cyanide, Total (9010), mg/kg dw <1.0
Dilution Factor 1
Prep Date 07.10.00
Analysis Date 07.11.00
Batch ID 0710S
04471-21
97 %
1
07.10.00
07.11.00
0710S
04471-22
75-125 %
--------------------------------------- ---------- ----------
04471-23 044 71-24
97 % 0 %
1
07.10.00
07.11.00
0710S
---------- ----------
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s·a·vta11n n ah
Labo'ratOr.i~s ·-"'_,_........,,,.,..., 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 12
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
04471-25 LCS Precision Control Limit (Advisory) %RPO
PARAMETER 04471-25.
Hexavalent Chromium (7196A), mg/kg dw
Antimony (6010), %
Nickel (6010), %
Cyanide, Amenable (9010), mg/kg dw
<30 %
<20 %-
<20 %
Cyanide, Total (9010), mg/kg dw <30 %
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s·,a,v an n a.h
l:aboratories ._,,.....,_r_, __ ..,_ 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO~021199-A
Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163 800717
REPORT OF RESULTS Page 13
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
04471-37 Matrix Spike% Recovery [G21 (0.5-1.0)]
04471-38 Matrix Spike Duplicate% Recovery [G21
(0.5-1.0)]
04471-39 Matrix Spike% Recovery [G21 (0-0.5)]
04471-40 Matrix Spike Duplicate% Recovery [G21 (0-0.5)]
PARAMETER
Antimony (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium
Dilution Factor
Prep Date
Analysis Date
Batch ID
----------
(7196A), mg/kg dw
04471-37 04471-38
--------------------
92 % 93 %
1 1
07.11.00 07.11.00
07.11.00 07 .'11. 00
0711I 0711I
124 % *F61
1 1
07.10.00 07.10.00
07.11.00 07.11.00
0710D 0710D
84 % 88 %
5 5
07.12.00 07.12.00
07.13.00 07.13.00
0712B 0712B
04471-39
----------
96 %
1
07.11.00
07.11.00
0711I
*F61
5
07.10.00
07 .11.00
0710D
87 %
5
07.12.00
07.13.00
0712B
04471-40
43· %
2
07.11.00
07.11.00
0711I
*F61
5
07.10.00
07 .11.00
0710D
88 %
5
07.12.00
07.13.00
0712B
I Cyanide, Amenable (9010), mg/kg dw
I
I
Cyanide, Total (9010), mg/kg dw *F61 *F61 *F61 *F61
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Sa,van,nifh
L.'ab0r21tories 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
04471-28
04471-29
04471-30
04471-33
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTO#021199-A
P .0. Box 31388
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 14
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
MS Accuracy Advisory Limit (%R)
Precision ('lrRPD) MS/MSD [G21 (0.5-1.0)]
MS Precision Advisory Limit ('lrRPD)
Precision ('lrRPD) MS/MSD [G21 (0-0.5)]
PARAMETER 04471-28 04471-29 04471-30 04471-33
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010), mg/kg dw
Hexavalent Chromium (7196A), mg/kg dw
Antimony (6010), 'Ir
75-125 %
80-120 %
75-125 'Ir
*F61
4.7 %
1.1 'Ir
<30 'Ir *F61
<30 % 1.1 %
<20 'Ir 76 'Ir
Nickel ( 6010) , % 75 -125 'Ir *F61 <20 'Ir *F61
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Sa v:a n n1a·h
L:aborator,ies 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LT0#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 15
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank 04471-34
04471-35
04471-36
04471-41
04471-42
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER
Cyanide, Amenable (9010), mg/1
Cyanide, Total (9010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471-34
<0.010
1
07.10.00
07.11.00
0710T
Hexavalent Chromium (7196A), mg/1 <0.010
Dilution Factor 1
Prep Date 07.07.00
Analysis Date 07.07.00
Batch ID
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
0707A
<0.020
1
07.10.00
07 .11.00
07101
044 71-35
95 %
1
07.10.00
07.11.00
0710T
100 %
1
07.07.00
07.07.00
0707A
102 %-
1
07.10.00
07 .11.00
07101
04471-36
85-115 %-
85-115 %
75-125 %
DATE/
TIME SAMPLED
04471-41
101 %-
1
07.07.00
07.07.00
0707A
101 %
1
07.10.00
07.11.00
07101
04471-42
1.0 %
0.99 %
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s:a .v a n n:a.lh
Labof'.·atorieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com .-.... .. -.r,.,.'--"'-,ln<.
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199cA
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 16
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04471-34 Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
04471-35
04471-36
04471-41
04471-42
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER 04471-34 044 71-35 04471-36
-----------------------------------------------------------
Nickel (6010) , mg/1 <0.040 106 % 75-125 %
Dilution Factor 1 1
Prep Date 07.10.00 07.10.00
Analysis Date 07.11.00 07.11.00
Batch ID 07101 0710I
-----------------------------------------------------------
04471-41 04471-42
---------- ----------
105 % 0.95 %
1
07.10.00
07.11.00
0710I
--------------------
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S a,via,n n,a h
L:3bor.itor'.i'es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471
Received: 07 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0232
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163800717
REPORT OF RESULTS Page 17
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04471-34 Method Blank
04471-35
04471-36
04471-41
04471-42
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
04471-34 044 71-35 04471-36 04471-41
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, IIB, and III.
S004471-14 MSD and S004471·13 MS/MSD failed to meet advisory limits due
to abundance of nickel present in the sample. S004471-13 sample result
was l000mg/kg dw and the spike level was 64mg/kg dw. Sample S004471-14
sample result was 710mg/kg dw and the spike level was 64.9mg/kg dw.
04471-42
Cyanide MS/MSD failed advisory limits due to abundance of analyte.
S004471-13 sample result was S0mg/kg dw and the spike level was 5.lmg/kg
dw. S004471-14 sample result was 39mg/kg dw and the spike level was 5.
2mg/kg dw.
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
*F61 = The recoveries of the matrix spikes are outside advisory limits due to
the abundance of the target analyte in the sample.
ffll ------- ------ - - - - -ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. 05'2. '!w--13 CHAIN-OF-CUSTODY RECORD Page _I_ of __6.__
Project Number/Name ,-IC--O\. '"C2..-C..'"'2, C ~I Cl I ANALYSIS/ METHOD/ SIZE I
Project Location JFD e\ec / C /'\ o,cfo"-D, N<:... AY. I., :i % jJ i ,.V ' ~ ,;I 'JI(.;
V -> ·• Y"-».. Laboratory sn .... SO....vu...-,.._c..i.t.... ~-....,.~ 1/; I/_, "/ 1/' "1:
Project Manager ,-J . .s ...,_--,-,--':i I'-< -4.. ~ 1/... ;; v _,_ '} \ 1f~; .f' "'1'/' iJ
Sampler(s)/Affiliation f:')_ IL= \:3:L<-€ :J'. ~ 1/4/t,;/ CJ t."4 1-1-f' 4, i,i' 4 M, Pe>W\. • c ~ 4) //J.;'0~Y-,'f tf f-~'r"9,,/J;~ "j} Datemme
Sample ID/Location Matrix Sampled Lab ID Remarks Total
G-3 i o -c.~) 5 7-(..-c,,,
G:W' I I
C-3 {u,J--1.c.) s 1-G·-~ I I C: : ,. t""
~ G,3 / l,G -I SI s 7-G-... ~ I I q,\IC,
. G0 C. -, u-o.,;J s 'ci~<~ I I
C-{, 1o,S-1.o) s ,,r:,.,x, o: ,,... l j
f;: r:..r. 1.0-1,sil s "1-E,-u. I I i ": 1<
EB-cY"t-L 1-t:.-i:N iC,,-,,-I ' I .l,
e,;-0'11 L. 7-G-<r<,
JCJI-$ I i I 3
G-7! i o-os\ s ,-G-~
10 I'-<" I i . , 7 .-C:-l'/4\ G-'8 lo.S-1.c,l s I. C; 1../C. ) ·-fl ~~ I
p G-'Z ft.o-)S'\ s 7-c;-,.o ' ~£1 MC-ril 10:'l't . . I
~P--1::,'l 1-G·<'C> I n"<&. '17 -i :; ~
el}·-09 7-G-<'.,<, I i 3 i.. fO;-,.S I
/ZcP -.:.,q .s ., -(;,-,.;<, ' I -
(:ii f?_a"--c,'1 5 ·,-l:-C't:. I f -
Sample Matrix: L = Liquid; S = Solid; A = Air Total No. of Bottles/ 7-1 Containers
Relinquished by: ✓ -¾i ..,..CE. (jb~..L..,._~ Organization: /',/'J.J::.A-D ,.s 6--(i_cM Date 1/ f, l ,~ Time Seal Intact?
Received by: {~ -~•,. Organization: YZ:.t.a ~,[GI Date .-, l i l ,-.-:1 Time ;r· ..\'U 6No N/A ,
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special lnstruct1ons/Remarks: I W ~ ~ :1,lrf:"t •'-Oc.·Jt,<d ·::b,.:ns> -H::s--:,,.J AU ~;.-, ---1 d ,,., b:t+, q \..➔ ;:::d--,, @ r,,-d Cl ::k e1 ~....,, l t7'
cl ::H,;.. t:::,h,·~Ur.-,,...,.,,. ,l·r4,t.. o::. ,; "Q, C----+?\l~c,&-f•.J ~ ew--\o 6 ..... d I.a· ,-,1.:c.,-. ('SJ>er-,d;::: Ar-1ld1=-:r-J Anc.l,,?r-, c::r,-o'} ~r'l-
Delivery Method: D In Person IB!Common Carrier Ac"? E..z;. □ Lab Courier □Other _______ _
SPECIFY _ , ....-jPEJ-IFY
-- -- ------ - -
liiiiil -
ARCADIS GERAGHTY & MILLER Laboratory Task Order No.IP.a. No. osz..:i:cc--.13 CHAIN-OF-CUSTODY RECORD Page__)___ of :;._
Project Number/Name t:! LOl.-::Q 2..Qj_ O Ll C I ANALYSIS/ METHOD/ SIZE I
Project Location ;:TF-.D cis:ct: /c_n C)<.C::-0~ ✓;-..1c... 1 I fl/J .,.,
->
Laboratory ;:iTL ~~vc:...~::n~a.~ L.,.L>.,..~ IJ. . u
/J . S<te 'I '1 4-~ //,.,? ..,
Project Manager [ \ £ \I-'
Sampler(s)/Affiliation J!,:.&ni:CCI.~ . t::1, ,::\-~ .. l!J .lk" t! £ -vi ' ,.f.4, ;,
-;r U-U ( ....... C...-0 ·".) ;,;/ /.t.l( ~o:/~'-A Datemme
Sample ID/Location Matrix Sampled Lab ID ' 'Y 0' Remarks Total
G1z..(o-c:, . .s) s ·7--,. a, ,, ,, .< I I
G'-1 "I-/ 0,,; __ ,. <>) 5 ,-,-C, I I II !l.c
G-1 z.. I 1.c,-1. s·1 s ..,_ c-c;;:, I I I I ;·1...,
~I 'f /o-lL ,:) 5 ,-<:--a, I I i\ ).$6
G-14 (o,r-1.cJ s 1--'f-<-s. I ! (.() I I
G-1'1 (1.~-1.s) .5 ·, ... -o, I I jZ..~ i l...
G-tc; I a -c..~J 5 7•6-C<> \ I 12:~w
G-t<j• fo.s-i.o} 5 '1-6·-C-, It.:~ I I
G'J'i (1.0-/,$) s •,f·¼ ~b I I
G-2.. I lo-o, ~) s 7-~-= I I i 3;,1,;,
(;-2.l (c,, ,-1:u) 'i ,-<--= I 1tS -!t I 13i IS :;;a,-. ,--,.,
GZ-1 /1.u-1S) -S 7-\,-.:0 I ~~ I; I 15;/.~
T· -_.e,.ttt._ L ~ l1 -
Sample Matrix: L Liquid; s Solid; A Air Total No. of Bottles/ IL = = = Containers
Relinquished b}". ~-e_ 5..-o~c:..... Organization: t,r11-.c•'"" ;S ~-M Date ·7 l (, l c.'"t""",. Time IC;~!:;. Seal Intact?
Organization: 5 .r,_.J -c:; cl~ Date 7. l -Z fCr!J Time -:v .. rv G'No NIA Received by: l . Y, ..-.
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special Instructions/Remarks: I it. .a.:a,k: --f\ i C!o D c..,,.c,v ; ... ~ .-h..."""""e -~··-' A-<.-1 J_",,,. .. ~ d -. I· • ac.J wt&@ ,......d ·p ~ £)•I') ~kb
Delivery Method: D In Person ~Common Carrier F'<..-o E><; □ Lab Courier □Other ___ ~~---
sPEctFY SPECIFY
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S a1v a1n n,a h
L:'a bci rato ri e· s •-•-T-~.""-5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 16390071 7
REPORT OF RESULTS Pagel
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
04471A-l Gl4 (1.0-1.5)
PARAMETER 04471A-l
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Percent Solids
<0.47
l
07.14.00
07.16.00
0714B
<2.4
l
07.13.00
07.17.00
0713A
290
1
07.13.00
07.17.00
0713C
85
07-06-00/12:12
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S1a v _a ,n n•a,h
Laboratories 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.:. JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 2
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES
04471A-2 GS (1.0-1.5)
04471A-3 REP-09
PARAMETER
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471A-2
<0 .45
1
07.14.00
07.16.00
0714B
<2.3
1
07.13.00
07.17.00
0713A
510
1
07.13.00
07.17.00
0713C
16
10
07.13.00
07.14.00
0713T
DATE/
TIME SAMPLED
07-06-00/10:48
07-06-00
04471A-3
<0.45
1
"07.14.00
07.16.00
0714B
<2.2
1
07.13.00
07.17.00
0713A
680
1
07.13.00
07.17.00
0713C
6.0
10
07.13.00
07.14.00
0713T
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S1a,v;ain n.a,h
L:aboratories .......... -1, ... ~ ..... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 163900717
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME SAMPLED
04471A-2 GB (1.0-1.5) 07-06-00/10:48
04471A-3 REP-09 07-06-00
PARAMETER 04471A-2 04471A-3
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
100
10
07.13.00
07.14.00
0713T
90
1
07.13.00
07.14.00
0713T
Percent Solids 88 89
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S,a v,~,n;n,a,h
L:abol".atories
•-OI-T•-'-"-.'"e. 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL oo
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 4
LOG NO
04471A-4
04471A-5
044 71A-6
04471A-7
04471A-8
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
PARAMETER
Hexavalent·Chromium
(7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
04471A-4 044 71A-5
<0.40 86 %
1 1
07.14.00 07.14.00
07.16.00 07.16.00
0714B 0714B
<2.0 93 %
1 1
07.13.00 07.13.00
07.17.00· 07.17.00
0713A 0713A
<4 .0 102 %-
1 1
07.13.00 07.13.00
07.17.00 07.17.00
07l.3C 0713C
04471A-6
80-120 %
75-125 %
75-125 %-
------------------------------------------------------------
0447l.A-7 04471A-8
104 % 1.9 %
].
07 .13 .00
07.17.00
0713C
---------- ----------
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Sa v a.n·,n a1h taboiatoi'ies 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0210
Sampled By: Client
Code: 163900717
Page 5
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
-----------------------------------------------------------------------------------
04471A-4
04471A-5
04471A-6
04471A-7
04471A-8
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
PARAMETER 04471A-4 04471A-5 04471A-6 04471A-7 044 71A-8
--------------------------------------- ------------------------------ ----------
Cyanide, Amenable (9010), mg/kg dw <1.0
1
07.13.00
07.14.00
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
0713T
<1.0
1
07.13.00
07.14.00
0713T
94 %
1
07.13.00
07.14.00
0713T
75-125 % 91 %
1
07.13.00
07.14.00
0713T
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
3.2 %
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S a v ain· n:a·h
l!:a borciti:::ii-ie's 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 6
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
-----------------------------------------------------------------------------------
044 71A-9 LCS Precision Control Limit (Advisory) %RPO
-----------------------------------------------------------------------------------
PARAMETER 04471A-9
Hexavalent Chromium (7196A), mg/kg dw
Antimony (6010), %
Nickel (6010), %
Cyanide, Amenable (9010), mg/kg dw
<20 %
Cyanide, Total (9010), mg/kg dw <30 %
These test results meet all the requirements of NELAC. All questi.ons
regarding this test report should be directed to the STL Project Manager
who signed this test report.
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s·a•v a nin.a h
Eabo'iatories 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr_ Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
04471A-10 Matrix Spike% Recovery [GB (1.0-1.5)]
04471A-11 Matrix Spike Duplicate% Recovery [GB (1.0-1.5)]
------------------------------------------------------------------------------------
PARAMETER 04471A-10 04471A-11
------------------------------------------------- ------------------------------
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Hexavalent Chromium (7196A), mg/kg dw
Dilution Factor
Prep Date
Analysis Date
Batch ID
Antimony (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
*F61
10
07.13.00
07.14.00
0713T
87 %
1
07.14.00
07_16.00
0714B
88 %
1
07.13.00
07.17.00
0713A
*F61
1
07.13.00
07.17.00
0713C
*F61
10
07.13_00
07.14.00
0713T
87 %
1
07.14.00
07.16.00
0714B
83 %
1
07.13.00
07.17.00
0713A
*F61
1
07.13.00
07.17.00
0713C
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s·a;v ~ n~n;a)!
taborator:ies 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Client PO. No.: LT0#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
------------------------------------------------------------------------------------
04471A-12 MS Accuracy Advisory Limit (%R)
04471A-13 Precision (%RPO) MS/MSD [GB (1.0-1.5)]
04471A-14 MS Precision Advisory Limit (%RPO)
------------------------------------------------------------------------------------
PARAMETER 04471A-12 04471A-13 04471A-14
-------------------------------------------------------------------------------
Cyanide, Amenable (9010), mg/kg dw
Cyanide, Total (9010), mg/kg dw
Hexavalent Chromium (7196A), mg/kg dw
Antimony (6010), %
75-125 %
80-120 %
75-125 %
*F61 <30 %
0 'I;
5.8 %
Nickel (6010), % 75-125 % *F61 <20 %
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S1a:v,a 1n'n ah
La"borcitOries 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO: S0-04471A
Received: 12 JUL 00
Reported: 17 JUL 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ98-0553
LOG NO
04471A-12
04471A-13
04471A-14
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210
Sampled By: Client
Code: 163900717
REPORT OF RESULTS Page 9
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID TIME SAMPLED
-------------------------------------------------------------------------
MS Accuracy Advisory Limit (%R)
Precision (%RFD) MS/MSD [GS (1.0-1.5)]
MS Precision Advisory Limit (%RFD)
------------------------------------------------------------------------------------
PARAMETER 04471A-12 04471A-13
--------------------------------------- ------------------------------
SW-846, Test Methods for Evaluating Solid Waste, Third Edition,
September 1986, and Updates I, II, IIA, IIB, and III.
044 71A-14
Total cyanide MS/MSD percent recoveries were outside advisory limits due
to abundance of analyte present in the sample. The total cyanide
concentration in the sample was l00mg/kg dw and the spike level was 4.
Smg/kg dw.
Nickel MS/MSD percent recoveries were outside advisory limits due to the
abundance of analyte present in the sample. The nickel concentration in
the sample was Sl0mg/kg dw and the spike level was 59mg/kg dw.
All other QA/QC were within STL Savannah control limits.
*F61 ~ The recoveries of the matrix spikes are outside advisory limits due to
the abundance of the target analyte in the sample.
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STL SAVANNAH LABS 912 352 0155
Savannoh
Lat'.Joratorie.s
......... ._,..,.,-.. n:. 5102 bRoche Avenue , Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
I,OG NO: S0-04471C
Received: 19 JUL 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LT0#052300-B
P.O. Bo,c 31388
Raleigh, NC 27612 Requisition: SQ00-0232
Coneract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0210/JFD CHANNEL MASTER/JFD02
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
Sampled By: Client
Code: 152600721
Page 1
DATE/
TIME SAMPLED
0447lC·1 EB-09 07-06-00/10:45
P,ARf\METER
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Oat.a
baton l:D
0447lC-l
<0.020
1
07.10.00
07.11.00
0710:J:
<0. 040
l
07.10.00
07.11.00
07lOI
I Cyanide, Total (9010)
cyanide, Amenable (9010)
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JUL-21-2000 16:04
'r,;;ff ~~
STL SAVANNAH LABS 912 352 0165 P.03/04
$,a v a n n ~ h
lfabotatories 5102 l.aRoche Avenue • S•vannah, GA 31404 • [phone] • Fax [phone] • www.srJsavlab.com
Mr. Nanj un Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO. S0-04471C
Received: 19 JUL 00
CC: Mr. Mark Radecl<e Project:
Client PO. No.: LT0~052300·B
Requisition, SQ00-0232
Contract No.: JFD Channel Master
NC000202.0210/JFD CHANNEL Ml>STER/JFD02
Sampled By. Client
code: 1S2600721
REPORT OF RESULTS Page 2
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED ---------------.. ------------·-------------------------------------------·-----------
04471C-2
04471C-3
04471C-4
04471C-5
04471C-6
Metnod Blank
Lab Control Standard t Recovery
Lab Control Stanaard Duplicate t Recovery
LCS Accuracy Control Limit ( tR)
Precision (\RPD) of LCS/LCSD --------------.. -----------------------------.. --.. -------------
PARAMETER
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/l
•o~lutiori Factor
Prep Date
Analysis Date
!latch ID
Cyanide, Total (9010)
Cyanide, Amenable (9010)
04471C·2
----------
<0.020
1
07.10.00
07 .11.00
onor
<O. 040
1
07.10.00
07.11.00
Q710I
04471C·3 04471C-4
--------------------
102 %-101 t
1 1
07.10.00 07.10.00
07.11.00 07.11.00
07101 0710I
106 \-105 1r
l 1
07.10.00 07.10.00
07.11.00 07.11.00
0710I 0710I
04471C-5
75-125 t
75-125 'I,
04471C-6
0.99 t
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JUL-21-2000 16:05 STL SAVANNAH LABS 912 352 0165 P.04/04
savannah
Laboratories 5102 LaRocbc Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.s"tlsavlab.com
LOG NO: S0-04471C
Received: 19 JUL oo
Mr. Nanjun Shetty
AR.CADIS Geraghty & Miller, Inc.
F.0. Box 31388
Raleigh, NC 27612
cc: Mr. Mark Radecke Project:
Client PO. No.: LT0#052300·B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
NC000202.02l0/JFD CH11NNEL MASTl!R/JFD02
Sampled By: Client
Code: 152600721
REPORT OF RESULTS Page 3
DAT!!/
LOG NO SAMPLE DESCRIPTION, QC RBFORT FOR LIQUID SAMl'Ll!S TIMI! SAMPLED
04471C-7 LCS Precision Control Limit (Advisory) %RPD
PARAM!lTER 04471C-7
Antimony (6010), t
Nickel (6010), t
Cyanide, Total (9010)
Cyanide, Amenable (9010)
<20:.
<20 \'
TOTAL P.04
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JUL-26-2000 17:01
Savannah
Laboratories
a rlh;ision ot68'ffll1 Tr111t Laborilttlril!s, loo.
STL SAVANNAH LABS 912 352 0165
STL Savannah Laboratories
5102 LaAcche Avenue
Savannah, Georgia 31404
Tel: [phone]
Fax: [phone]
P.01/05
FACSIMlL~ CUV .ti:KS.ii.i!:Er
From: ROSE WADLEY
Date:
.t" 21.l.. tt: ...
Phnne #:.<ll?.. 1.<;'1~'7~5ll _ ...
Fa:t #: 912-3:5.Z-0l 6:5
# of Pages Including This Sheet: ...5
Co.11,Gdenti11.lity 'N'otice: Th• inkm\Mion CQnbiaed in th• Fae11m!ll~ ,:an.u.g~ ii privil•s~rl •?1d ,.,.. .. _tl_,;1.'r!!:!:b.l i~~~ti<111, in.mc.de~-~12.Li\,fo~ .. ..i:., .. l".f,o. ,
('fJ~• ..... ~.,..•~• Tf ti,• ..,..,,-1,..,. f'lf ~hi. m••tca~ .. ;., n.-., fh• ; .. -.1...t ...,.;!";,,.,,t_ nr thl'! ~11'1'.':f~L'! I'll' il!l'!nr Tl"'A!'rm11.ihl• '"' ri•liu-it tn tlil'I inti!ndcd
recipient. you arc hcrctty ncdfkd that any dtueminatioft, dim'bution OM~yir.g-0! tlli! ~!:".:n-.:::.!~:ti~ !: !~.:tlr p~!=.i'Ji?:d, !! ~au ha.v~
received. thl11 1;0!?ll!:'.lllii:2tio~ Ul ~~r. p!e?te noti..fy U! m?Inedb.!~L'! h~ r•l~hnn~ 11.nri ,:-il~ue re?Um the ~n~,.,111 mr.u11r""' 1111 ~r tlir. llhnva :i.ddrc.ss
. vie. the U.S. Postal SctVicc. · ·
' /lllrt at
Severn Thi: Se.rv!= Ir1C
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JUL-26-2000 17=02 STL SAVANNAH LABS
Mr. Nanjun Shetty
An.CAJ:>:t:J C:fcl."a.':,ihLy & Mll.J.~.1. , l:ui..;.
P.O. Box 31388
Raleigh, NC 27612
cc: Mr. Mark Radecke Project:
912 352 0165
LOG NO: S0-04471C
ReC".P..i ,u,,.d ~ -tLJl'l!.~O
Reported: 26 JUL 00
Requisition: SQ00-0232
Contract No.: JFD Channel Master
NC000202.02l0/JFD CHJ\NNEL lli!ASTER/JFD02
Sampled By: Client
Code: 164500726
REPORT OF RESULTS Pagel
DATE/
LOG NO SAMPLE DESCRIPTION , .LIQUID SAMPLES TIMS SAHl'I.EI)
0447lC-l llB-09 07-06-00/10:45 ----------------------------------·-------------------------------------------------
PARAMETER 0447l.C•l
Antimony (6010), mg/1
Dilution Factor
Prep Date
Analye:i.e Date = l!J
Nickel (6010), mg/1
Oilution Fact:or
.R.u.a..L :t :,..1. I:, .ug. i..t:
Bo.tch IO . . Cyanrde, Total (9012)
Total Cyanide, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010)
Cyanide (Amenable), mg/-3.
Dilution Factor
Prep Date
Analysis Date
Satc:h ID
<0. 020
l
07.10.00
07.lLOO
07tOT
<0.040
l
U/ . .1.l.UU
07lOI
<:0.010
1
07.20.00
07.25.00
07209
... o-.ore
l
07.20.00
07.25.00
0720S
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Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-0447lC
Received: 19 JDL oo
Reported: 26 JUL oo
Client PO. No.: LTO#052300-B
Raleigh, NC 27612 Requisition: SQ00-0232
Contraot No. : JFD Channel Master
p..,.'""j~l"'t-. nr..nnn?Jl'l._a.2..Ln.l-Im .OJ~ns.TERlilED02.
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTIO~,
Method Blank 04471C-2
04471C-3
04471C-8
01.<t.'11C-H
0447lC-6
Lab Control Standard % Recovery_
Lab Control Standard Duplicate% Recovery
LCS l\ocur~---:,,r r~~---.-., T~-~ ... (9.-'C}
Precision (%RPD) of LCS/LCSD
PAH.AMJ:n'.b::H.
Antimony (6010), mg/1
Dilution Factor
~rep Oate
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep oate
Analysis Dat:e
Batch J:D
~lde, Total (9012)
Tot~1 Cy1;1.nide, mg/1
D:i.l.uti.on t'et..Q~o:r
Prep Date
Analysis Date
Batch ID
04471C·< U4471C-3 ____ ._ ....... .. .... -----~ -
<:0.020 102 %
l 1
07.10.00 07.10.00
07.11.00 07 .11. 00
07J.0I 0710I
<0. 040 106 t
1 1
o·,.io.oo 01.~o.o·u
07.ll.00 07.J.1.00
071"U.l ln:.t.0.L
~0.01.0 115 ~
l. l.
07.20.00 07.20.00
07.25.00 07.25.00
0720S 07209
Sampled By: Client
code: 164500726
Page 2
DAT!l/
101 \-. 75-125 \-
l
0 .99 %
07.10.00
07.ll.00
0710:I
105 % 75-125 " 0.95 t
l
l.n. J.\J-. U{F
07 .11. 00
0710
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JUL-26-2000 17:03 STL SAVANNAH LABS 912 352 0165 P.04/05
.a £ E
' !!!! !S --5 E! ""= 1t,t♦.:e1t.M 5102LaRochcAv-.nue • Savannah,GA31404 • [phone] • Fax.(912)35_2-0165 • www.sUsav~o·.co~
Mr. Nanjun Shetty
ARCJIDIS Geraghty & Miller, Inc.
P.O. Box 3l.388
Raleigh, NC 276l.2
LOG NO: S0·04471C
Rt:!Llt:Sivt,tl: J'"J_ (TTTI.,.n.n
Reported: 26 JUL 00
C.lient PO. No.: L'l'O#O~~~UU-li -
Requisition: SQ00-0232
Coneract No.~ JED ~hannel Master
i..;C..:: Mr. --t!lark kadet:k.e ....... P:z:oJ~t::L:·:-HC000.2"02:·0.2.1:0tJFD·C'rlH.NiffiL 1•%N.STE1'/.;'r.'.CC2
REPOR'l' OP RESULTS
Sampled By: Client
Code: 164500726
Page 3
r:>A=,'-
LOG NO QC !"~!."'OR'I'-· POR--L~D-.£.7\MN.SS ... ";?;:IME.-SU\MP.LE!I --------------------------------------------------------------------------
Method Blank
Lab Control seandard t Recovery
04471C-2
04471C-3
04471C-8
04471C•S
04471C-6
Lab control Standard Duplicate t Recovery
LCS Accuracy Control Limit ( %R)
Precision (tRPD) of LCS/LCSD
PARAMETER
Cyanide, Amenable (~010)
Cy,lllide (Amenable), mg/l
Dilution Factor
Prep Date
Analysis .ua.t:e
Batch ID
•
04471C-2 ,. _________
<0.010
1
07.20.00
07.25.00
0720S
----------
O-i¼7l.C-J 04471C a
----------------~---
115 t
1
07.24.00
07 . .2.,. 00-
0720S --------------------
0-1i7l.C 5 C!i71C £
--------------------
---·----------------
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JUL-26-2000 17:03 STL SAVANNAH LABS 912 3S2 016S P.0S/0S
5102 I.aRocht:--Avcnuc , Sa\.'nn11.'lh, ti,4~ 31404 • (912) 3~4-7A'.i8 • Fax [phone] • www-.stlsavtao.com
---· ---··---· ~-----------. . ·--
Mr. Nanjun Shetty
ARCADJ:S Gt;,::t.c:t.~hLy & t,til.1ci-, Inc.
P.O. Box 31388
R~io•~~. Nr ~~~,?.
CC: Mr. Mark Radecl<e Project:
LOG NO, S0-04471C
Received, 19 JUL oo
Reported, 26 JUL oo
Cl.ient PO ... N,-, • T,'"Niil:ni;,:~nn-B
Requisition: SQ00-0232
Contract No.: JFD Channel Master
NC000202. 021-01~· CHAI..tra!. !-1ASTER/ J!1DC2
Sami;>led By: Client
Code, 164500726
REPOR'l' OF RESULTS Page 4
DATE/
LOG NO SAMPLE DE:SCR:I.PTION , QC REI"ORT FOR LIQUID S?JdPLES "T'TM"J.: ~nM'PT.~n
·------------------------.. ----------------------------------------------------------
0447lC•7 LCS Precision Control ~imit (AUvl~v~y} ~RP~
-------------------------------------------------------------------------------------
PARAMETER 04471C·7
Antimony (6010),
Nickel (6010),
Cyanide, Total (9012)
Total Cyanide
Cyanide, Amenal:lle (9010)
Cyanide (Amenable)
<20 \-
• SW·84G, Test Methods for Bvaluating Solid Waste, Third Edition,
-September 1.986, and Updates ~:I,-Il:A; I:CD, and III.
I r ~sl<ir~
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Final Page Of Report
TOTAL P.05