NCD122263825_19991020_JFD Electronics - Channel Master_FRBCERCLA SAP QAPP_Annual Groundwater Sampling Results-OCR

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ARCADIS GERAGHTY&MILLER
Mr. McKenzie Mallary
U.S. Environmental Protection Agency
Region IV
I 00 Alabama Street, SW
Atlanta, GA 30303-3104
Subject:z
RECEI\/ED
OCT 28 1999
3UPERFUND SECTlO~1
Annual Groundwater Sampling Results, JFD Electronics/Channel Master NPL Site, Oxford, North Carolina.
Dear Mr. Mallary:
ARCADIS Geraghty & Miller, Inc., (ARCADIS Geraghty & Miller) collected a round of groundwater samples at selected wells at the JFD Electronics/Channel t-.faster site. The purpose of this sampling was to evaluate if the plume has migrated farther at the above-referenced facility. This report summarizes the procedure used to collect the groundwater samples and discusses the anal)1ical results.
SUMMARY OF FIELD ACTIVITIES AND RESULTS
The field activities were conducted by ARCADIS Geraghty & Miller personnel during the period of March 2, 1999, and March 4, 1999. These activities include
groundwater level measurements and groundwater sampling of 12 monitor wells. The following sections describe various field activities and provide a summary of sampling infom1ation.
Field Activities
Depth-to-water measurements were collected from all on-site and off-site monitor
wells, with the exception of wells CMMW05 and CMMWI0, on March 2, 1999. Wells CMMW05 and CMMWI0 were buried under a layer of gravel and required a magnetic detector to locate them; therefore, water levels from wells CMM\V IO and CMMW05 were collected on March 3 and 4, 1999, respectively. The water-level
measurements were collected using an electronic water-level probe.
Groundwater samples were collected on March 2 through 4, 1999. The groundwater sampling activity was performed in accordance with the Remedial Design Work Plan prepared by ARCADIS Geraghty & Miller in 1993. A low-flow sampling
methodology was employed for well sampling in an effort to obtain groundwater samples with low turbidity and to minimize volatilization. The monitor wells sampled include CMMW04, CMMW0\ CMMW07: CMMWI0·, CMMWl5·, CMMWI7:
CMMWI9: CMMW20: CMMW21; CMMW2i, CMMW2{ and CMMW26: ll1csc 12 monitor wells were purged and sampled using peristaltic pumps with dedicated
Our ref.:
g:\g&m\:iprojcct~fdchann\nc0202.190\rcport~1sarnp•rpl.dl)c\20-Oct-99
ARCAOIS Geraghty & Miller, Jnc.
2301 Rexwood1 Drive
Suite 102
Raleigh
North Carolina 27607
Tel 919 782 S511
Fax [phone]
ENVIRONMENTAL
Raleigh, NC.
20 October! 999
Contact:
William H. Doucette, Jr.,
Ph.D., P.G.
Extemion:
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ARCADIS GERAGHTY & MILLER
tubing. The deep monitor wells were sampled using decontaminated electric
submersible pumps. Approximately three well volumes of water were purged from
each well, except for well Cl'v!MWI 7, prior to sampling. The recharge rate of well
CMMW-17 was very low and the well was dry after purging 1.07 well volumes.
Therefore, this well was left overnight to be recharged and was sampled the next day
(within 24 hours). During purging of monitor wells, pH, specific conductance, and
temperature were measured and recorded using portable meters calibrated in the field.
This information was recorded on a groundwater sampling log. Copies of the
groundwater san1pling logs are enclosed as Attachment I. Purge water and equipment
decontamination water (investigative-derived waste) generated during sampling were
placed in the existing storage container at the site for future disposal.
Once collected, the groundwater samples were placed in appropriately labeled and
preserved, laboratory-supplied containers, packed on ice in a cooler, and shipped to
Savannah Laboratories and Environmental Services, Inc., Savannah, Georgia, for
analysis. A chain-of-custody form was used to maintain a complete record of all
personnel that had contact with the samples. Copies of the chain-of-custody records
arc enclosed with the laboratory anal:,tical reports in Attachment 2.
Results
The depth-to-water measurements were converted to groundwater elevations using the
well survey data. Table I presents the depth-to-water measurement and groundwater
elevation. Figure I presents the groundwater elevation contour map with general
groundwater flow direction. Based on this map, the groundwater flow direction is
toward the southeast on the JFD Electronics/Channel Master property and casU
northeast on the off-site property. The groundwater flow pattern is similar to those
previously observed.
All groundwater samples collected at the site were submitted for analysis of volatile
organic compounds (VOCs) using U.S. Environmental Protection (USEPA) Method
8260. In addition, the groundwater san1ple from monitor well CMl\1\V04 was
analyzed for total and amemble cyanide (USEP A 90 I 0). Upon receipt of completed
laboratory amlyscs, ARCADIS Geraghty & Miller validated the data using Level II
Data Quality objectives. A summary of laboratory anal)1ical results is presented in
Table 2.
Based on the anal)tical results described in Table 2, the VOC concentrations in on-site
monitor wells vary slightly from the previous sampling events, with the exception of
monitor wells CMiv!W05. As sho"n in Figure 2, monitor wells CMtv!W05 had total
trichlorocthcne (TCE) concentrations of 180,000 micrograms per liter (ftg/L). This
concentration is significantly higher than that detected historically in well CMMW05
(sec Figure 2). The reason for this increase is unknO\\TI at this time.
Our ref.:
g:\ g&m '.,project~ f dchannlncO 2 0 2 . l 901rcp.:i rt.~l.c;;unp•rvt.doc\2 0-Oct -9 9
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ARCADIS GERAGHTY&MILLER
The total VOC concentrations in the groundwater samples collected from off-site
monitor wells CMMW04, CMMW21, CMMW07, CMMW17, CMMW19,
CMMW21, CMMW22, CMMW24, and CMMW26 did not vary significantly from
the previous sampling results.
Since the historical data indicate the presence of cyanide, monitor well CMMW04 was
also sampled for total and amenable cyanide analyses. The total and amenable
cyanide concentrations detected in this well were qualified as estimated at 250J ftg/L
each, respectively. The previously-measured total and amenable cyanide
concentrations (February 25, 1998) in the groundwater sample from this well were
240 and JO µg/L, respectively.
Summary
To evaluate if the groundwater contamination has migrated farther, a round of
groundwater samples was collected from representative monitor wells at the facility in
March 1999. The groundwater sampling results indicate that the dissolved
contaminant concentrations in the perimeter monitor wells have not changed
significantly since the last sampling event conducted in February 1998. However,
significantly higher concentrations of total VOCs were observed in monitor well
CMMW05 (hot-spot well). Since no significant changes in contaminant
concentrations were observed in the perimeter monitor wells, the contaminant plume
docs not appear to have migrated farther.
If you have any questions or need additional infom1ation, please contact us at
[phone].
Sincerely,
ARCADIS Geraghty & Miller, Inc.
~i~-~ouc~e~~
Associate/Project Coordinator
for the Responsible Party
Attachments
/1 ~
Nanjun Y. Shetty, P.E.
Senior Engineer/Project Manager
c,,;.,, Brian Kempner, The UNIMAX Corporation
S. Alan Lazar, AVNET, Inc.
Our ref.:
Greg Rorech, ARCADIS Geraghty & l'vliller (Tampa)
David Mattison, NCDENR
g: \g&m1~1 proj cct~ f dchannlncO::? O::?. I 901,cpo,t.,;\ump-rpt. d0c\10-O~-i-99
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ARCADIS GERAGHTY & MILLER
TABLES
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I AR CAD IS GERAGHTY & MILLER
I Table I. Water-Level Elevations, March 2, 1999, JFD Electronics/Channel Maser Site, Oxford,
North Carolina.
I Measuring Point Depth Groundwater
Monitor Elevation to Water Elevation
Well ID (fl msl) (fl toe) (fl msl)
I
CMMW0l 478.18 9.54 468.64
I CMMW02 466.24 6.41 459.83
CMMW03 466.23 8.16 458.07
I CMMW04 463.60 8.06 455.54
CMMW05 469.99 7.75 11 462.24
CMMW06 459.03 6.54 452.49
I CMMW07 463.60 5.15 458.45
CMMW08 476.74 8.36 468.38
I Ct-.lMW09 472.68 7.4 7 11 465.21
CMM\Vl0 469. 71 7.46 462.25
CMM\Vll 466.69 6.45 460.24
I CMMWl2 466.78 6.39 460.39
CMMWl3 463.68 3.97 459. 71
CMMWl4 468.40 9.60 458.80
I CMMWl5 468. I 7 9.41 458.76
CMMW16 458.02 4.72 453.30
I CMMW17 460. l 5 5.51 454.64
CMMW18 455.58 4.20 451.38
CMMW19 456.48 7.48 449.00
I CMMW20 469.37 13.79 455.58
CMMW21 456.22 3.27 452.95
CMMW22 456.12 4.24 451.88
I CMMW23 447.64
CMMW24 445.58 4.54 441.04
I CMt'vfW25 466.96 7.36 459.60
CMMW26 468.44 7 02 461.42
1W-24 463 .88 5.91 457.97
I SME-01 477.80 7.86 469.94
OW-1 466.14 8.00 458.14
I fl toe Feet below top of casing.
fl msl Feet above mean sea level.
I ]/ Data collected on March 4, 1999.
'1 Data collected on March 3, 1999.
I g:\aproj.:ct1nc0:202. I 30\tabks\Gw _ ckv.xls\ 1 0/20/99
-- -- - --- - -- - ----Table 2. Groundwater Sample Quality YOC and Cyanide Data Summary, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Sample Name: C1'.1MW-04 • C1'1MW-05, CMMW-07 •
Sample Date: 3/4/99 3/4/99 3/4/99
Sample Type: Monitor Well Monitor Well Monitor Well
Media: Groundwater Groundwater Groundwater
Zone: Intermediate Intermediate Shallow Bedrock
Laboratory: Savannah Savannah
Lab ID: S9-ll456*12 S9-ll456*13
Concentration Unit: 11g/L 11g/L
Volatile Organic Cornnouncls
(USEPA Method 8260)
Carbon tetrachloride <50 <100
Chlorobcnzene <50 <100
Chloroform <50 <100
l, 1-Dichlorocthane <50 <100
l, 1-Dichlorocthene <50 <100
cis-1,2-Dichlorocthene 85 • 740,
trans-1,2-Dichloroethene <50 <100
Methylene chloride <250 250J 11 •
Tetrachlorocthene 380 · 14,000D
l, l, !-Trichloroethane <50 <100
Trichlorocthene 5,800 • 180,000D ·
Cyanide
(USEPA Method 9010)
Total 250J 21 • NA
Amenable 250J 21 • NA
Micrograms per liter. 11g/L
<
J
D
Compound was not detected above the quantitation limit.
Compound concentration is qualified as estimated.
Compound \Vas quantitatcd using a secondary dilution factor.
Savannah
S9-l 1456*2
11g/L
<l.0
<l.0
<l.0
<l.0
<l.O
61 •
<l.0
<5.0
58 ·
<1.0
3401l ·
NA
NA
REP-I* ,
3/4/99
Monitor Well
Groundwater
Shallow Bedrock
Savannah
S9-ll456*14
µg/L
<2.0
<2.0
<2.0
<2.0
<2.0
63 ·
<2.0
<10
62 •
<2.0
340 •
NA
NA
I/ Estimated concentration (compound was detected between the MDL and the Quantitation Limit).
CMMW-10 · CMlvfW-15 •
3/3/99 . 3/4/99
Monitor Well Monitor Well
· · Groundwater Groundwater
Shallow Top of Rock
Savannah Savannah
S9-l 1427*9 S9-l 1456* l
11g/L 11g/L
<2,000 <2.0
<2,000 <2.0
<2,000 <2.0
<2,000 <2.0
<2,000 <2.0
<2,000 7.7 ·
<2,000 <2.0
<10,000 <10
3,800 · 18 •
<2,000 <2.0
140,000 • 300 •
NA NA
NA NA
2/
•
Compound concentration is qualified as estimated because the matrix spike/matrix spike duplicate sample recoveries were not met.
Field replicate of groundwater sample CMMW-07 .
NA Compound was not analyzed.
--Page I of 2
CMMW-17 •
3/3/99
Monitor Well
Groundwater
Deep Bedrock
Savannah
S9-l 1427*7
11g/L
<l.0
<l.0
<l.0
<l.0
<l.0
5.8 ·
<l.0
<5.0
31 ·
<l.0
48 •
NA
NA
AR CAD Is GERAGHTY & MILLER
-
- -- ----- - -- -- - -
Table 2. Groundwater Sample Quality VOC and Cyanide Data Summary, JFD Electronics/Channel Master Sile, Oxford, North Carolina.
Sample Name: CMMW-19 • CMMW-20 •
Sample Date: 3/3/99 JRiW -shhr,J
Sample Type: Monitor Well Monitor Well
Media: Ground waler Groundwater
Zone: Intermediate Shallow
Laboratory: Savannah Savannah
Lab ID: S9-l 1427*6 S9-I 1427*4
Concentration Unit: 11g/L 11g/L
Volatile Organic ComQounds
(USEPA Method 8260)
Carbon tetrachloride <I.0 <IO
Chlorobcnzene <1.0 <IO
Chloroform <1.0 <10
I, 1-Dichlorocthane <1.0 <10
I, 1-Dichloroethene <I.0 32·
cis-1,2-Dichloroethene 1.3 • 28 ·
trans-1,2-Dichloroethene <1.0 <IO
Methylene chloride <5.0 <50
Tetrachloroethene 36 • 1,000 •
l, l, I-Trichloroethane <1.0 <10
Trichlorocthcnc 12 . 70 •
Cyanide
(USEPA Method 9010)
Total NA NA
Amenable NA NA
µg/L Micrograms per liter.
<
J
D
Compound was not detected above the quantitation limit.
Compound concentration is qualified as estimated.
Compound was quantitatcd using a secondary dilution factor.
CMMW-21 • CMMW-22 -
"3Qf'J<f!/$/'J'1 3/2/99
Monitor Well Monitor Well
Ground waler Groundwater
Shallow Shallow
Savannah Savannah
S9-Il427*5 S9-l 1427*2
Jlg/L 11g/L
<5.0 <I.0
8.1 , <I.0
<5.0 <1.0
<5.0 <1.0
<5.0 <1.0
200 • <1.0
<5.0 <1.0
<25 <5.0
320· 2.3 •
<5.0 <1.0
89 -<1.0
NA NA
NA NA
II Estimated concentration (compound was detected between the MDL and the Quanlilation Limit).
CMMW-24-
3/2/99
Monitor Well
Groundwater
lntem1ediate
Savannah
S9-11427* I
11g/L
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<I.0
<1.0
<1.0
NA
NA
21
• Compound concentration is qualified as estimated because the matrix spike/matrix spike duplicate sample recoveries were not met.
Field replicate of groundwater sample CMMW-07 .
NA Compound was not analyzed.
-- -
Page 2 of 2
CMMW-26 -
3/3/99
Monitor Well
Groundwater
lntennediale
Savannah
S9-l 1427*8
11g/L
<1.0
<1.0
<1.0
<1.0
<I.0
70-
I. 7 •
<5.0
120·
<1.0
10 •
NA
NA
ARCADIS GERAGHTY&MILLER
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ARCADIS GERAGHTY&MILLER
FIGURES
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CONCRETE
PAD
ARCADIS GERAGHTY&MILLER
2301 Rex .. oods Drive
Suite 102 RALEIGH, NC 27607
Tel• 9191792-5511 Fox• 919/782-5905
PRJT MANAGER,
L. MORETZ
CHECKED BY•
A. PINNIX
REFERENCE: BECHTEL FIGURE 1-3
FS REPORT, APRIL 1992.
0 200 FEET
DU,'A?
DRAFTER•
A. NORTON
DRA\o/ING,
\./L3-99
DATE•
13DCT99
PROJECT NUMBER• NC000202.0190
JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
GROUNDWATER ELEVATION CONTOURS
AND GENERALIZED FLOW DIRECTIONS
MARCH 2, 1999
FlGURE:
1
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j
-®-
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TVOC
1-~~o :J--1 (p_~-
1 . / G)SM
I
42,257 J 93,390J I6,74IJ
I
10-3-94 2-21-97 '1 2-26-98 '1 3-3-99 J/
TCE 160,000 240,000 II0,000D 140,000
5,300J 8,500 3,800 3,800
I66,3I5J 248,500 II4,570J 143,800
I94,990J -"-Y ~-I CMMW02 '::;: .,,. -CMMW07 •
i.---,,:.r CMMW17 CMMW11 CMMW12.
~~·.
~ k() '\
-\
10-3-94 2-19-97 J/ 2-26-98'1 3-4-99 '1
TCE 190 270 260D 300
PCE I8U 20 20 18
TVOC I99J 645J 288 326 [ ~~ VA
"'~ ~c,J__~_~v~_,,_0,-+..--"-'----.,,
'/ ~ \. 10-11-94 2-21-97,; 2-27-98'1 3-L-99 '1 ~ -, , "-~ TCE 5,600 5,600 4,600D 5,800
PCE 440J 370 390 380
-
'-'
C MMW24 -
=::=::=--J's \r ---:z_ -
>-\1 J --->-£---~. ~ '-A_,'
/ /
TCE
PCE -"?-TVOC
TCE
PCE
KEY TO DATA BOX
3-15-95
TCE IOU
PCE IOU
TVOC 2J
ND
J
(µg/L)
1/
2/
3/
u
D
Date Sorn pl ed
Trichloroeth one (µg/L)
thane (µg/L) Tetrachloroe
Total Vo!otil
Com ounds p e( ~JLtc
Not Detected
Estimated Concentration
micrograms per liter
Analyzed by USEPA
Method 601
Analyzed by USEPA
SW-846 Method 8240
Analyzed by USEPA
SW-846 Method 8260
Compound Not Detected
Compound Was Quantitoted
Using a Secondary Dilution
Factor
3-16-95 2-19-97 J/ 2-25-98 '1 3-2-99 J/
ND 0.5IJ ND ND
ND ND ND ND
2J 0.5IJ ND ND
10-5-9!.. 3-10-95 2-20-97'1 2-25-98'1 3-3-99 J/
2J IOU 9.3 II 12
IOU IOU 28 44 36
CMMW:6 "o~O CMMW21 CMMW22 I'-'' ' '
TVOC 2J ND 38J 56.4 49.3
0t..?-i'l c,olJ' .
l ·~ t:~~ ~
3-15-95 2-19-97'1 2-25-98 '1 3-3-99 J/
TCE 9J 9.2 8.7 10
PCE 51 57 78D 120
TVOC 73J 88 133 202
ARCADIS GERAGHTY&MILLER
2301 Rexwoods Drive
Suite 102 RALEIGH, NC 27607
Tel• 919/782-5511 ra.x1 919/782-5905
'
10-11-94 3-14-95
TCE I9U 10
PCE 27U II
TVOC IJ 21
~
CRISEX 3UILDING
PRJT MANAGER,
L MORETZ
5-16-9511 2-21-97 J/
26 27
78 28
114 61
3-17-95 '1
TCE 31
PCE 260
TVOC 323
CHECKED BY•
N. SHETTY
REFERENCE: BECHTEL FIGURE 1-3
FS REPORT, APRIL 1992.
2-27-98J/ 3-3-99 J/
9. 7 48
6.3 31
31 85
2-19-97 '1 2-25-98 '1
49 55D
680 740D
793 858
CMMW20
TCE
PCE
TVOC
10-11-94
32U
22U
4J
DRAFTER,
A. NORTON
DRAVING,
~ 3-17-95 2-19-97J/
( "' ~
~\
II
(lW-24 I
TCE IOU 0.22J
PCE 4J 2.6
TVOC 4J 3J
0-5-94 2-25-98'1 3-2-99 '1
3-2-99 J/ TCE 72 8ID 89
70 PCE 100 220D 320
1,000 TVOC 375J 502 617
1,130
3-10-95 2-20-9721 2-26-98 '1 3-l-99 '1
180 130 IOODJ 340D
94 33 40 58
362J 540J 172 459
PROJECT NUMBER• NC000202.0190
G\J-DS99 JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
0 200 FEET DATE,
l3□CT99
2-25-98'1 3-2-99 J/
ND ND
2.7 2.3
2. 7 2.3
~
LEGEND
FENCE
CULVERT
SHALLOW WELL
INTERMEDIATE WELL
SHALLOW BEDROCK WELL
DEEP BEDROCK WELL
TOP OF ROCK WELL
DRAINAGE CREEK
PROPERTY LINE
TREE LINE
RAILROAD CMMWO 1 RI WELL/RD WELL
P.W-1 A
OW-1 [:.ii
PUMPING WELL
OBSERVATION WELL
GROUNDWATER VOLATILE ORGANIC
COMPOUND DATA SUMMARY
FIGURE:
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ARCADIS GERAGHTY&MILLER
ATTACHMENT I
Groundwater Sampling Logs
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ARCADIS
GERAGHTY & MILLER
HATER S7'-'1PLING LOG
Project/No. C:.HA/J!J{i HaS'!e,/
;i/,./11
J,-. NcJ!2z.o z . /'!CJ
Page / of _J_
Site LDcation ~Os4m::L,~:L_--,--------------------
Site/Well No. U1HtJ-zt Rep./Field Bla.nk No. 715-I
Ended /C: 9CJ Weather ,;,_,~.,7 1
5:5-,,.:::-Sampling Began ///Z
Description of P.easuring Point (MP) _Ti.~O=-'""'---------------
HP Elev2.tion Water Level Elevation
F.eight of MP
Depth of Well Below MP tfO.Q
Held Depth to Water Below MP
Water Column in Well 3{. ,;c
X CJ./(p ---
Casing Di2..meter Gal. /ft.
Gallons in Well "';'ii. = 5-? 9
Ei.'c.cu2.tion Volume
G2.llons
pE
Spec. Conductance
Temp,crature t9/°F)
s,nnol inq
Color <..leer Odor -'.C::..C:C:::.,_ ___ _
Comrnents:
X
0 ? /0
<, 'I e G-7-/ (,.(;j
.)c)c) -z,:;, J . -u; I
/r':,.s /&-0 /G.'f._
Data/Field
Spec. Cond. (u..'iilios/cm) ZGZ.... pH &-01
--------
If
(o.r.y
-z.cz.
ft-r
I Z.. 'lo
Sampling Met hod _7.-~r::.,,,.'.::'.:"."_'..:.,-,.::.C':.:'.":'::'-:....'....P,:..·c.::r--.c+:------------------
Co n ta in er Type (L-3b l'.._G&M __ ) Analyses
8zc:o
Rem2rks:
GN...J\T
3, -'.zfJ ,,,, c //a fs
1-V, • -0.00
1-\':" -O.C"J
z--0.1G
2-\':· -o.:-iJ
::i· -0.37
3-\':" -0.'."'.-0
Preserv2tive
'z'.' G /;;c:.1
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ARCADIS
GERAGHTY & MILLER
WATE-""l. S1'-"'-iPLING LOG
Project/No. c.HA/JA!ft. Has/?,/ /JaJz.oz. /9CJ Date 3 /c. /fy
Site Location ~0,.4'.l<Gd_..1!!.L---------------------
Site/1-iell No. c'..Mt-f(,l_ 22. Rep./Field Blank No.
1-ieather juv1vi, c;;o· r-Sampling Began /7,.?-=
I -,..... / Description of Measuring Point (HP) '---''--
HP Elevation Water Level Elevation
Evecuction
F.eight of HP
Depth of 1-iell Below HP
Held
1-iet
___ Depth to Water Below HP
Water Column in Well
Casing Diameter
Gallons in Well
EV?..cuation Volume
Gallons
:z
X
Gal./ft.
0 "', <-/
ze:,_ 7-c.
X C?/(p
332
G B jj_
Ended l'(~o
-------
~y,
pF. (,, 1/ {t,/f, G,7-s. C.5t; \
Spec. Conductance
Te::iperature t§/oF)
('}_'j_
Jtj_l
/'-14-
Li-1-
/j_~ i~~
/5', '1 ,r z.
&rnolina Data/Field P~ramPter~
Color ( /c,,, Odor -"--'='-----
NA Appea ranee (,/<o, ~~-'----------
Co mrr rents:
Spec, Cond. (wnhos/ cm) / 4 j
Sampling Method
Analyses
8zc:o
Remarks:
Container Type (Lab ..K_G&M __ )
.3, -f0 .,,, !. Va I<,
1-\.'•" -0.03
1-\.':" -O.c:J
I\HL (AS:rx::; VCU/!.t!cS
Z---0.16 3·
2-\':" -O.::"t3 3-\':"
Preservative
...!/ c /11 t: 1
..(· -0.(-.S
G· -1.-.0
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~ Page _L_ of _I_
ARCADIS WATE.....:Z S1'-1.fPLING LOG
GERAGHTY & MILLER
Project/No. C.HA/J!!ft. Hast?,! A)o:Jzoz. /90 Date 3 / 2-/ f9'
Site Location ~O~b,:,L.JYJ:..._ ___________________ _
Site/Well No. (J·1M(,)-f1: Rep./Field Blank No. _______ _
Weather Sc.,,v,,v 0> .. c_ Sampling Began I>'-// Ended / S;;,,; <..-. ;, / 5/'ir
Description of Measuring Point (M?) _-.J_-~o~-c_=------------
MP Elevation Water Level Elevation ----------------
Eyccnction Peta
Eeight of MP
Depth of Well Belo,; M? /lo.a
Held
Wet
Depth to Water Below HP
Water Column in Well = /o'I .1;
313/J"l
1335
Casing Diameter -e::_
G2llons in Well
EVccuation Volume
Gallons
pH
S!)€c. Conductance
Temperature ~/oF)
Gal. /ft. X cJ./(p
= (0-1-c
X
0 f /0 /f,
~-(;p1 8.Q_> 1?> 8.22'
~31 Z'/._L/ C°L/._c.. ~
!_2-1-/1.f L6-i /f:.,.G
sanoliua Datc/fiPld P~ramPtPr0
Color ~C~k_{µ," ___ _ Odor /JA Appearance C/<or -=-'--------
Comments:
S!)€c. Cond. (umhos/ on) 4/f, PH 8-cJ <---"----
Sampling Method
l•J1alyses
f3zc:o
Remarks:
Container Type (L2b -1\G&H __ )
3, · z0 .,,, L V« I:,
Preservative
q c; /11c1
,~ .S~ ,,,,./c 3/!tilt ' W /J;pcs.,(, ,~
' E, ... .1/r,.....
Sampling Personnel: Lu.~~
1,HL C,AS:UG VC\.UHS
1-V• • -O.OS
C C-1
.· 7.' -O.IG J·
".1-\'·" -02-J 3-V:"
{).;t ,.,.,,._..__
-0.J)
-0. ~0
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~ Page of _L_
ARCADIS WATER SlL"!PLING LOG
GERAGHTY & MILLER
Project/No. t.HA/JIJ{c. Ha;,li,/ A)aJz.oz. /90
Site Location -'=Oa.t=,L....f!f..l.---------------==,-------,-----
Site/Well No. <'.'.M,'-'iW. zC. Rep./Field Blank No. T8,-/.
Weather (/4._,c./.,, f;G •r Sampling Began /..53:S Ended /C,!:CJ
/7 Description of Measuring Point (H?) -~-'--1--::_o=-..::,.._ __________ _
MP Elevation Water Level Elevation
Evacuation Data
Height of HP
Depth of Well Eelow HP
Held ___ Depth to Water Below MP
Wet Water Column in Well
Casing Diameter
G-2.llons in Well
EVccuation Volurae
Gallons
Gal. /ft. X
X 3,
0 ,,;,2-
pH -:;. & "l: G.'7..3
C?/(p
5 28
/ (.
&,q]_
Spec. Conductance
Temperature {§/of)
53l
/!'\,~
";>i/
J1 1
3"\5
11c, z..
Color C(_~ O<l or ,-.J r>i Appe a ran c e U---t---A -----'=------
Comments:
Spec. Cond. (lLSlhos/on) S"i <; pH
Sarapling Method
Analyses
8zco
Remarks:
Container Type (wb j(_G&M __ )
3 -z0 .,,, !. Va I:,
\',ell CAs:UG VQ._V,.,SS
1-\',"' -a.OS
1.l'•' -OCJ
2"' -0.lG
2-\':"' -0~3
3--0.37
J..\½"' -0.~,1
Preservative
_'LG l11t1
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ARCADIS
GERAGHTY & MILLER
Project/No. c.HA/JAJ(t. Ha;;/<,/ A)o:Jz,oz. /'lo Date 3 /~ /fy
Site Location ~0:::ct:IDJL/:LJ..----------------=,---~----
Site/Well No. (.l'-tN(.) .;0 Rep./Field Blank No. ,-5-/ /F./J-(
-ju~,= Sampling Began 17/5" Ended / 1 '/£ Weather {Jo~.l,
I
Description of Measuring Point (HP) ~G) C.. __ ...:.._ ________ _
HP Elevation Water Level Elevation
F.eight of HP
Depth of Well Below H?
Held
Wet
Depth to water Below HP
Water Column in Well
Casing Diameter z:_
Gallons in Well
EVccuction Volume
Gallons
pF.
X
Gal./ft.
3
0 /. C
r, :--/e <.;16
7-, '-16
= io.~r
X CJ./(p
= /.G'?
f;.o
3, %?.,._
(. .3:j
Spec. Conductance
Temperature e9/°FJ
3<,~ 302 300
/J.'-{ /3,.1_ I -:,,L,
--------
/o
G~e
l."18
fj.o
Color (_ (,:ol' O<lo r _,.,/.,..,_).,_AL____ Appearance ---'-(_,k,"'""-·""C ______ _
Comments:
Spec. Cond. (um.hos/on) -Z.'7' 8
Sampling Method
l-.nalyses
f3zco
Remarks:
GM..JF1.
Container Type (Lab LG&M __ J
3, · </4J .,,,t: Va is
1-Y,' -0.Oi
1_v.· -OC'J
\',cU. CA$UG VO.lMSS
Z---0.16 3'
~-\':" -O_:iti .3--\':"
-0.37
-o.~.J
Preservative
i/ % Ille.I
,· -0.65
6" - 1 . .0
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ARCADIS
GERAGHTY & MILLER
WATER SA..>.J:PLING LOG
Project/No. C.HA/J/J,ft. Has-ti,/ Ncoz.oz. /'/O
Site Location _0'=4.tmd........l!L'-----------------------
Site/;.;e11 No. LMMe,J. ;;!CJ Rep./Field Blank No.
Date 3(f/fy
-,-cs-t
1-iea ther rcA/7 s ,., 1./.5. C Sampling Began oBzo·
' . Ended O'rZO
Description of Measuring Point (HP) TcJC ----'------------
HP Elevation Water Level Elevation --------
Eyacuation Data
Height of HP
Depth of 1-iell Below HP
Held
Wet
Depth to Water Below HP
Water Column in Well
Casing Diameter z.. Gal./.ft.
Gallons in Well
E'-'c.Cuc.tion Volume X :::,
Gallons 0 i-;-
pFi s-13 ;, 11__
Spec. Conductance ZZ(/.. ZZ'f._
Tem_cerature t9/0F) ;;; <} lfZ
Color (Ice.,-
Comments:
X
15.11
cJ.((p
/. 71
s. 37
2..; -;Jo
( 0'( c:;03
zz.1
15.1/
zzz.
11. I
Spec. Cond. (umhos/cm) Z 2 ~ pH ____ _
Sampling Method
0920
Analyses
8zco
-------------------------
Container Type (Lab J._G&H __ ) Preserv2.ti ve
.> -z0 .,,, t V« /,, 't'. ('. /;; (,/
Remarks:
Sam P 1 in g Pc rs on n e 1 : .G._.L4, 1/,,Ly'"'''c.......J{Jc=c(,c.:.:.,_tf,_,'.-"'·"°-"-(d-½--, ____,0.cc( l<c.:.c"-<7z_"-{v-"fi.."-s:,::,✓,~,'='-'='-------
-I
V, 1: LL CJ,$ r ,>G VCt lf1,.(SS
G,",J.JFT. Z--0.16 3· -0.37
".\i.-_ o '."':i 3-\':" -o . .::,J
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WJ Page __j___ of _/_
ARCADIS
GERAGHTY & MILLER
WATE....-.:Z SJ. .. MPLING LOG
Project/No. cHA/JIJ{t. Has-/?,/ Na:Jz.02. /90
Site Location __,,,O:'..U=L....=----------------------
Site/Well No. C:.Hr'q,.,. 21
Weather Yu,/i.., ,s"""'' ) y;· E
Rep./Field Blank No. TR -I • --'-'-L...-'-. ___ _
r I
Ended /0 -:zo
Description of Measuring
HP Elevation
Sampling Began Ol3o
Point (H?J JO(_ -~----'"----------
--------Water Level Elevation
Eyccuation Pete
Eeight of MP
Depth of Well Below HP
Wet ---
Depth to Water Below MP
Water Column in Well
Gesing Dia.meter
Gallons in Well
Evacuation Volume
Gallons
pfi
Spec. Conductance
Temperature (:9/°F)
Gal./ft.
0 z_z5
&.7.3
'i3t
f '-/, 3
/8 ()
samolincr Data/Field P~r~rnPter~
(ozo
Color </L'c:,,r
Corn.rnents:
Appearance (/«-r
Spec. Cond. (wnhos/on) 1/G:f,
Sampling Method _________________________ _
pH 6-Zi
Analyses
8zc:o
Rem2rks:
GA.L....,1--7"_
Container Type (Lab').4_G&M __ )
.:S -51:'.J ""!. V« Is
1-\'," -0.Cti
1-\':' -O.CJ
W(LL CtG nG VCt U,.((S
2· -0.1G 3-
:?·\':' -0.:-G J..\':'
-0.37
-05)
Preservative
'z'.'. ~( /;;{,I
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~ Page __ I_ of I
ARCADIS
GERAGHTY & MILLER
WATER S.l-..MPLING LOG
Project/No. t.HA/J/Jtt. Mq,&,/ A)CCJz.oz. /9<.J Date 3 / °:s/ fy
Site Location ~0':C,.(.W:oi.......JJ!.1-----------------------
Site/Well No. CMMld •f<t
Ended / z' • Weather ,fodiy.Su""i', .:f:5" F
Description of Heasuring
Rep./Field Blank No.
Sampling Began /0'/o
Point (H?) ~(._ ~-~~-----------
HP Elevation Water Level Elevation
Eyecuetion Det~
Fieight of HP
Depth of Well Below HP
Held ___ Depth to water Below HP
Wet Water Column in Well
Casing Diameter "'--Gal. /ft -
Gallons in Well
Evc.cuation Volume x ,"]
Gallons
pH
Spec. Conductance
Ter.iperature ~/oFJ
0
(~-~
t-/15
16-if
~
G 81
l/Zi
/(;6
qo.o
= 32: ,72'.:
X cJ./(p
?. 2a
= 15-(, 0
/o, zr;
&-Ci
1/1
!& C,
/~.0
(",0
'1Zd
/<c,.J
I Z 10
S0molinq Dete/Field P~remeter~
Color Odor Appearance -------
Comrne n ts :
Spec. Cond. (um.hos/on) ':z'.ZO pH G.f)c)
Sampling Method
Analyses
f3zco
Remarks:
G.,\.L.1r-l.
Container Type (Lab _l_G&M __ )
3, -92) .,,, t Va is
1-Y,' -a.OS
1.tV -O.CJ
WEU 0.S:>.l'.3 VO.UMS'.'i
Z' -0.16 3-
2·\-':-. -02ti 3-v-:•
-0.37
-0.~-0
----------
Preserv2.tive
t/ ~( /;; c. I
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~ P2.ge __l_ of L
ARCADIS
GERAGHTY & MILLER
WATE....""Z SJL"-PLING LOG
Project/No. t..HAIJ/Jfi Ha,k,/ A)aJz.oz. 190 D2.te 3 /y /79
Site Loc2.tion --°"O~(~f,ilor:~JL.-~!J~<----------------tT------
Site/WellJ.o. (Hnt,J· 07 Rep./Field Blank No. -pl&& -J f)J-z_
• (.l{ >'31!7 • • heather i Ii" qJ ·-€>-f:P>e•e· Gor Sampling Began !:l,20 Ended fSLO
' Description of Measuring Point (M?) -~/_0-"-(,,_ __________ _
M? Elevation Water Level Elevation
EY?.!CUation
F.eight of MP
Depth of Well Below HP
Held ___ Depth to water Below HP
Wet W2.ter Column in Well
Casing Diameter
Gallons in Well
Evacu2.tion Volume
Gallons
pF.
Sp€c. Conductance
Temperature t9/0F)
Gal./ft.
0
o/.½
£GI
/G-3
--------
7:7-0
= 11• 8~
X CJ./(p
//.5
Color (__/cc:,-Odor U6 -1'>,'-'-'-----Appearance ((=.,... ~=....c..:. _____ _
. Pc17· I Comments: {"""//,-,~,P 4:1:1,,.(c. ::.<-, .. ,?~
Spec. Cond. (umhos/~) r/20 pH lo. 9D T (e)/°F) /z.o
Sampling Method
J.J1alyses
8zc:o
Remarks:
G"1...JFl'.
Container Type (Lab _i_G&M __ )
.3, · z0 ,,,, c Va Is
"HL CA$t1G VQU,.(E5
1·\.'• • -Q_Oj
1.\';" -O.CJ
z---0.1G
2·)':" .. 0.:))
:i· -O.:J7
3-\':" -O.~O
Preservative
'IC: /11t:.1
~--0.65
G" -l.H
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~ Page _1_ of L
ARCADIS
GERAGHTY & MILLER
WATER SA.."'-U'LING LOG
Project/No. C:.HA/JAJ{i. Hasti,/ NcXJz.oz. {'lo Date 3 / t{ / fy
Site Location ~0=".1'.ru:cL.....l!f.1----------------------
Site/Well No. Ll'il-1.w -06 Rep. /Field Blank No. z::i<, -2. --L....<..:>---'==-----
Weather Su.,_,,, 0.;,J1 '50~G Samp ling Began /2 zo Ended I .3 .So
I I I I
Description of Measuring Point (H?)
HP Elevc.tion Water Level Elevation --------
Evacuation Data
Eeight of H?
Depth of Well Below MP
Held
Wet
Depth to water Below MP
Water Column in Well
Casing Diameter
GGllons in Well
Evacuation Volur.ie
Gallons
pE
Spec. Conductance
Teroperature /§!°F)
L Gal./ft. x
x __ _
0 /2 2
c,,. z~
/1{)
15,&
le.!, c. 2a
lr<.-
15. '1
_>i MP, -;;:,C:
I Z,50
Co 1 or --'("-. '--!<...:" ,,.c______ 0d or
Comments:
_.:__f.J~A--'----Appearance --=-(L/c-c.,,--'--------
Spec. Cond. (umhos/cm) /'jc, pH-----T(Ef:>/oF) -1-/z"-',_,o/ __ _
Sar.ipling Method
Analyses
8zc:o
Remarks:
Container Type (Lab 1-_G&M_~)
.) · z,:} Wll Va/:,
J.y.· -O.o.3
1•\':" -O.CJ
V.cU CAS:r x:; va. V!.tSS
:Z--0.16
2-\':" -02ti
3· -0.37
3-\':" -O.'.:•J
Preseri.12.tive
<z:'. % /11c:.1
-C. ... O.G.J
6" -, .~7
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~ Page _L_ of _I_
ARCADIS
GERAGHTY & MILLER
WATLP.. SJI.MPLING LOG
Project/No. c.HAiJIJfi. l-1a;:f2,/ /Ja::Jz.oz. /90 Date 3/'(/77'.
Site Location ~O~.t=>i_.l!L!~--------------=-------~ Rep./Field Blank No. TD -z. Site/Well No. LMM£,J. o'-/ --------
Weather ~Sllc~-,~•~,,~•,..._,,~?~•~1-_-___ _ Sampling Began /CJ/Z Ended / Z.c C -----I_. /
Description of Measuring Point (1-f?) -~~~«.~-----------
1-:P Elevation _______ _ Water Level Elevation
Evccuntion Date
Eeight of MP
Depth of Well Below MP
Wet
Held ___ Depth to water Below MP
Water Column in Well = <-/Z.1'-{ IZ OQ
Gal./ft. X CJ./(p
(,.87
X ~ = 20.c;
Casing Diameter Z
Gallons in Well
Evacuation Volume
Gallons 0 k'i· 1 Ho z!o
pE
Spec. Conductance
Temperature t9/~F)
(.;!,,,,,
'/. 7 -..,
11/b
(.,.(;'J
5_z,5
if&
/''1/ffe C,, //
1:11.s 'I tz
Nr, /'t'_.?,
5arnolina Pntn/field Pcrnm 0 ter~
~
~ ~
Color {(cc,,,-• Odor _µk.,__A,__ ___ Appea ranee _.:,:.{._0>_v-____ _
Comments: Iv-, s .. 1/;h, /,,J,~t< {F',,''°) /,,cJ /(c,it, 1c,,X/, +,r,J--f LJ:JL <.-<{(.G3
Spec.Cond. (umhos/cm) t.j17 pH(,.(( T(©/°F) /'(.8
Sampling Method
J..nalyses
8zc:o
Remarks:
Container Type (Lab !_G&M __ )
.> -'(cJ ,,,, 1. V., Is
W'ELL CA$UG VClllk~
,.;-,· -o.c,;
L~V .,. 0.CJ
2· -0.tG
~-\': • ... 0 :.•ti
3· -0.37
3-\':" -o.:v
P reserva ti ve
t/ ~( ///_,,._{.:__I __
Iv-. u /./ & , Ii /2 -i-,
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~
ARCADIS
GERAGHTY & MILLER
SA.."'-!PLING LOG
Project/No. c.HA/J!Jfi !1a,12,/ /JCX!Z.OZ. i'IO
Page __ ,_. of I
Date 3 /--/ /fy
Site Location O ~=ia.....1.!LL.-----------------
S it e /We 11 No. ct-/"1 t,J -/1, Rep. /Field Blank No.
Sampling Began Of.£!:, Ended 09 fl'..
Description of Measuring Point (M?)
MP Elevation Water Level Elevation --------
Height of MP
Depth of Well Below HP
Held
h'et
___ Depth to Water Below MP
Water Column in Well
Casing Di2.meter
Gallons in Well
E'-'c.Cuction Volume
Gallons
pH
Spec. Conductance
Temperature (§/°F)
Gal./ft. x
X
0 ,.,.,
e,11:b .Z&
"258
//,3
So
(o'f
302
No
cJ./(p
8. O'z:
c.'/3
--------
2'/5
c.1.1
27'C
lt/Z.
Color (lea,· Odor --'f\,-"-'-'-,/2-'----___ Appearance _C.'--'(.~c'-"c.:.,.· ..--______ _
comments:
Spec. Cond. (wnhos/cm) -z-;,c. pH {,. Z o/
Sampling Method _________________________ _
Analyses
3zc:o
Remarks:
C.'•UcT
container Type (Lcb l_G&H __ )
3 -fO ..,,,L Va 0
Preservative
£ '( /;; c::. I
\>ell CJ\s:tlG VO.. VMSS
Z--0.16 3• -0.37
I'\<'."\
--------. · ... :S,:A~t.11a~~-\~c ; '.,, .. )(;'_i[]i,bor~.--i.o_·_ .. ry_·._·.;.:.Tci:ik:6;c1_~r .•. N~.•-· ----'.-,'--. :;,'Jllla!Environme'.i!,~1.5:_~;;;c,/r... ; , • < '., . -------••··.·•··.·• \· iCHAIN~OF-CUSTODY·· RECORD . ' .
· ... · Project Number 'itVC6'z.oz. o .· 0 )/i'i,:•i:::.
·" . ··-~-·~~==~~~~~----:·,·:.J;:}?Jf,:'.:}\·\ ·
. SA.MPLE IDENTITY:i'-;Code'• \Sampled .:·,•, . ' . . . . . . ,,-•··.•. ~--. ' ,.,,.. .. . .
, -C.f:,.r,-;,,w~z.#..:,1. /Lt'· ..
BfliJ\,< ~j '\t.;// · ..
; iJ.:i/'•>•tt:\ '/C;i: .
t:rh'V'?.i cX: >(tf •·
- -
Total. No.· of· Bottles/.:
..-.. ·,·.•.•·• ... o.·. li .. d,·,;·,.·.·•.·.A.••·.•••.··•:=., .. ·.,,A.,. i.•.r ... •.•.•.· . i• ·.:: Containers · .. _.,_,~-, ·:,:\~ :','::,,: :; ..
Relinquish~d by:'•',/ '/ /i:.,~ , . . Organization: -'----'-;_.::.=-"'-:...:...:;..:,=-,1./~· -·-'--'...:.'.:..,__'--_> •:·Date•. 3 (:YI 're Time . · /8 ,, .
,Receivedby•i'...:. .:_<.,_/...:.·•'c..·'_' ··-·------'--'----·-••_.,-,:Organization: . . :,, . ,... . ·:· Date . Time,_·------'-'-------
Relinquished by:_"_·---------'----c,--Organization:· ___ ·_•,_·.'-· _·_.c.·~\~------... Date,_· ___c.1___,___-'Time, _______ _
'Receivedby: ·· · Organization:.· Date Time,_i_~-----
.·. D 'Lab Co~rier D Other __ ·
- -
- - - - ---- -------. CHAIN-OF-CUSTODY RECORD· -_ ~lalll"UC.KJ-\Unl I ... _
·;_---_.:/'.•Ali,'&-MII:.EER''INC· :: :'.
· · SAMPLE IDENTIT'l'!? Code °<:,';iSarripled
•
Reliriquistied, by:-,jc...' ,L' '-/-t'.L<..,,..,,C=:...:....c====:;"-··.-...:•' ;c,·· :_:': : o;ganization: ---~4-"="~;1~-,,~·:_, ~G~<~'~~-.:.c.,' -~l~l"':·)~"~(_'·h_.~:~-'~!,-._.,,._--'. Date 3 1 i_ I 11 Time,_·_,/~'l'-'q-""--L) ___ _
:Received:"tJ;/:'--' --· . -, ,_"_Organization:·,, __ ,. _-,;:--.,,(--,,-J"·•.'"'-.. _,,-,,,._ '-: ---'.:Date-. -·-Time•----'--'-'-
RelinquishecJ"by:':' : Organization:; ·. Date : Time,_·-----'---_:_-
Received by: · · f Organization: · . Date Time_-__ _:_ ___ _
--
TOfAL
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ARCADIS GERAGHTY&MILLER
ATTACHMENT 2
Laboratory Analytical Reports
Our r,f.:
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc. P.O. Box 31388
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Raleigh, NC 27622 Requisition: SQ98-0553
Contract No.: JFD Channel Master CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324 REPORT OF RESULTS Page 1
DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
11427-1
11427-2
11427-3
11427-4
11427-5
PARAMETER
CMMW-24
CMMW,-22
TB-1
CMMW-20
CMMW-21
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane, ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
11427-1 11427-2 11427-3
:.
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<1.0 <1.0 <1.0
<5.0 <5.0 <5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<l. 0
<l. 0
<25
<l. 0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
03-02-99/1240
03-02-99/1450
03-02-99
03-03-99/0920
03-03-99/1020
11427-4 11427-5
<10 <5.0
<10 <5.0
<10 <5 .0
<10 <5.0
<50 <25
<250
<10
32
<10
28
<10
<10
<10
<100
<10
<10
<10
<120
<5.0
<5.0
<5. 0
200
<5. 0
<5.0
<5.0
<50
<5.0
<5.0
<5.0
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190
Sampled By: Client
Code: 153590324
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------
11427-1
11427-2
11427-3
11427-4
11427-5
CMMW-24
CMMW-22
TB-1
CMMW-20
CMMW-21
03-02-99/1240
03 -02 -99 /1450
03-02-99
03-03-99/0920
03-03-99/1020
- ------------------ - - - -------------------- - ----------- - ----------------- -----------------
PARAMETER 11427-1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, ug/1
Surrogate Toluene-dB
<l. 0
<1.0
<1.0
<l. 0
<1.0
<1.0
<1.0
<l. 0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
9 2 %-
Surrogate -4-Bromofluorobenzene 90 %
Surrogate -Dibromofluoromethane 88 %
Analysis Date 03.10.99
Batch ID 100310
Dilution Factor 1. 0
11427-2 11427-3
--------------------
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
2.3 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<2.0 <2.0
92 % 92 %
90 % 90 %
88 % 88 %
03.10.99 03.10.99
100310 100310
1. 0 1.0
--------------------
11427-4 11427-5
--------------------
<10 <5.0
<10 <5.0
<10 <5.0
70 89
<10 <5.0
<10 <5.0
<10 <5.0
<10 <5.0
<10 <5.0
<100 <50
<100 <50
1000 320
<10 <5.0
<10 8.1
<10 <5.0
<10 <5.0
<20 <10
88 % 92 %
88 % 88 %
92 % 90 %
03.12.99 03.10.99
100312 100310
10.0 5.0
--------------------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS Page 3
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
11427-6 CMMW-19
11427-7 CMMW-17
11427-8 CMMW-26
11427-9 CMMW-10
11427-10 FB-1
DATE/
TIME SAMPLED
03-03-99/1210
03-03-99/1335
03-03-99/1650
03-03-99/1745
03-03-99/1730
------------ - ------ - - - ------------------ - ------ ------------------------------------------
PARAMETER 11427-6
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane, ug/1 <1.0
Vinyl chloride, ug/1 <1.0
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1.0
1,1-Dichloroethene, ug/1 <1.0
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 1.3
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2-Butanone (MEK), ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <1.0
Bromodichloromethane, ug/1 <1.0
11427-7
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
5.8
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
11427-8
<l. 0
<l.O
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
70
1.7
<1.0
<1.0
<10
<1.0
<1.0
<1.0
11427-9
<2000
<2000
<2000
<2000
<10000
<50000
<2000
<2000
<2000
<2000
<2000
<2000
<2000
<20000
<2000
<2000
<2000
11427-10
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<l.O
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LT0#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS Page 4
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
11427-6 CMMW-19
11427-7 CMMW-17
11427-8 CMMW-26
11427-9 CMMW-10
11427-10 FB-1
PARAMETER 11427-6
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
<1.0
<1.0
<1.0
12
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
36
<1.0
<1.0
<1.0
<1.0
<2.0
92 %-
90 %
Surrogate -Dibrornofluorornethane 86 %
Analysis Date 03.11.99
Batch ID 100311
Dilution Factor 1.0
11427-7 11427-8
--------------------
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
48 10
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<l.O <1.0
<10 <10
<10 <10
31 120
<1.0 <1.0
<l.O <1.0
<1.0 <1.0
<1.0 <1.0
<2.0 <2.0
94 % 90 %
88 % 88 %
90 % 88 %
03.10.99 03.11.99
100310 100311
1.0 1.0
--------------------
DATE/
TIME SAMPLED
03-03-99/1210
03-03-99/1335
03-03-99/1650
03-03-99/1745
03-03-99/1730
11427-9 11427-10
--------------------
<2000 <1.0
<2000 <1.0
<2000 <1.0
140000 <1.0
<2000 <1.0
<2000 <1.0
<2000 <1.0
<2000 <1.0
<2000 <1.0
<20000 <10
<20000 <10
3800 <1.0
<2000 <1.0
<2000 <1.0
<2000 <1.0
<2000 <1.0
<4000 <2.0
92 % 92 %
90 % 90 %
90 % 88 %
03.12.99 03.10.99
100312 100310
2000.0 1.0
--------------------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LT0#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------------- ---------------- ----------- - -------- ------------ --- ----------------- -----.
11427-11 Method Blank
11427-19 Method Blank
11427-20
11427-12
11427-21
Method Blank
Lab Control Standard% Recovery
Lab Control Standard% Recovery
------- ----- ---------- - ------------------------------------------------------------------
PARAMETER 11427-11 11427-19 11427-20 11427-12 11427-21
--------------------------------------------------------------------- ----------
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane, ug/1 <1.0
Vinyl chloride, ug/1 <1.0
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1.0
1,1-Dichloroethene, ug/1 <1.0
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 <1.0
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2-Butanone (MEK), ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <1.0
Bromodichloromethane, ug/1 <1.0
<1.0
<l. 0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
106 % 109 %
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------------------------------------------------------------------------------------
11427-11 Method Blank
11427-19 Method Blank
11427-20
11427-12
11427-21
Method Blank
Lab Control Standard% Recovery
Lab Control Standard% Recovery
----- ------- ------- - - - - ----------- ----- -------------- ------------------ ------------------
PARAMETER 11427-11
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, ug/1
Surrogate Toluene-dB
<1.0
<1.0
<l. 0
<1.0
<l. 0
<l. 0
<1.0
<l.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
90 %-
Surrogate -4-Bromofluorobenzene 90 %
Surrogate -Dibromofluoromethane 88 %-
Analysis Date 03.10.99
Batch ID
Dilution Factor
100310
1. 0
11427-19
----------
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<l. 0
<2.0
92 %
92 %
84 %
03 .11.99
100311
1.0
----------
11427-20
----------
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
92 %
88 %
92 %
03.12.99
100312
1. 0
----------
11427-12 11427-21
105 %
105 %
105 %-
100 %-
91 %
87 %
89 %-
03 .10. 99
100310
1. 0
115 %
117 %-
114 %
110 %
91 %-
91 %-
84 %
03.11.99
100311
1.0
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9·11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11427-22
11427-13
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
PARAMETER
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
11427-22
116 %
113 %
112 %
109 %
106 %
91 %
Surrogate -4-Brornofluorobenzene
Surrogate -Dibromofluoromethane 91 %
89 %
Analysis Date 03.12.99
Batch ID 100312
Dilution Factor 1.0
11427-13
46-147 %
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
03.10.99
100310
1.0
----------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P . O . Box 313 8 8
Raleigh, NC 27622
LOG NO: S9-11427
Received: 04 MAR 99
Reported: 16 MAR 99
Revised: 24 MAR 99
Client PO. No.: LT0#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 153590324
REPORT OF RESULTS . Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------------------------------------------------------------------------------------
11427-14 MS% Recovery (Batch)
11427-15 MSD % Recovery (Batch)
11427-16 Precision (%RPO) MS/MSD
11427-17 MS Accuracy Advisory Limit (%R)
11427-18 MS Precision Advisory Limit (%RPO)
----------- - --------------- ---------- ---------- - ---------------- ----
PARAMETER
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
11427-14
114 %
116 %
116 %
114 %
110 %
92 %
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane 88 %
90 %
Analysis Date 03.11.99
Batch ID 100311
Dilution Factor 1. 0
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
11427-15 11427-16 11427-17
112 % 2 % 46-147 %
110 % 5 % 56-143 %
108 % 7 % 62-135 %
108 % 5 % 68-131 %
106 % 4 % 72 -12 7 %
90 % 77-122 %
89 % 74-126 %
90 % 70-130 %
03 .11.99 03.11.99
100311 100311
1. 0 1.0
-------------------- ----------
11427-18
0-30 %
0-35 %
0-37 %
0-33 %
0-22 %
----------
COMMENT: All associated QA/QC samples were within the SL quality control
requirements.
Angie s'i:.ewart, Project Manager
Final Page Of Report
-------------------..AD"GERAGHTY A"'& MILLER, INC. Laboratory Task Order No. CHAIN-OF-CUSTODY RECORD Page_/~of __
JJ!l!JJIEn\'ironmental Sen•ices
Project Number fj<-CJ202. 0/90
Project Location O xf'o L J, IJ C
Laboratory Se< l.{_0/.1V1c{ h Labs
Sampler(s)/AHiliation (a/,,;.,, lJ/,:jfc/J
_Js:_rc""'z /1'.f"~ I
DatefTime
SAMPLE IDENTITY Code Sampled Lab ID
Cf.-1 Mw · <-L/ L y Ari!, ,.., 0
J-1 /'1/) · < 2 L-3'~'l'l5ZJ
TB·/ -
l. .,..,,.(7 'H•
(.Hh() ·<?O l. ~13/Jl o
<..,Ml-1t)·Z/ .~/.l .,
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(MMW·/7 L. ~f.J I 1 I 7./o
c.,t--1 MW -/1 l. 313if§3~
(/c,/1-1()·2.G L , Ul!f C..x:,
c. t--, /.1 v -10 L, 31:J/n, -:;.Ii£
Fi3 -I I 31 .Jtr 1 17.:P
Sample Code: L = Liquid; S = Solid;
1 -
Relinquished by: If "7/ /c..-~~
Received by: //' // ~ , , ,
Relinquished by:
Received by:
Special lnstructio __ amarks:
....L. C{"(y'
I
,
A = Air
I SAMPLE BOTTLE / CONTAINER DESCRIPTION I
V V <'\ I '\.." ( !
rv'-')'-' !
'-'"~ I ~~~ I
ri5' ~" )-i TOTAL
.3 I 3 ;
3 ! $
' 3 i 3
3 i 3
3 ' 3 I
3 I 3
-3 I 3
3 I 3 I
.3 i ~
3 i 3 I
I
i
I ' !
I
I Total No. of Bottles/ I 3<::i I Containers
Organization: A,cocP.5 C:.c~I; ~ h ;/(0, Date-3 I ,:'.) I 'tJ Time 18 11 ~I Intact?
Organization: 2 le; <; I Date 'I '1 / '"' ime ,:Z,'uL No N/A
✓
Organization: i Date I I Time Seal Intact?
Organization: I Date I I Time Yes No N/A
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
lt_iCEIVED
MAR 2 5 1999
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]l~~e;ld:ll~aeraghty&Miller
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190
Sampled By: Client
Code: 173090324
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
11456-1
11456-2
11456 -2-DL
11456-12
11456-13
CMMW-15
CMMW-07
CMMW-07
CMMW-04
CMMW-05
03-04-99/0955
03-04-99/1030
03-04-99/1030
03-04-99/1200
03-04-99/1350
---------------------------------------------------------------------·
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane, ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, U:9/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
11456-1
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2.0
7.7
<2.0
<2.0
<2.0
<20
<2.0
<2.0
<2.0
11456-2 11456-2-DL
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<5.0 <10
<25 <50
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
56 61
<l. 0 <2.0
<1.0 <2.0
<l. 0 <2.0
<10 <20
<1.0 <2.0
<l. 0 <2.0
<1.0 <2.0
--------------------
11456-12 11456-13
<50 <100
<50 <100
<50 <100
<50 <100
<250 250J
<1200 <2500
<50 <100
<50 <100
<50 <100
85 740
<50 <100
<50 <100
<50 <100
<500 <1000
<50 <100
<50 <100
<50 <100
--------------------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 2
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
11456-1
11456-2
11456-2-DL
11456-12
11456-13
CMMW-15
CMMW-07
CMMW-07
CMMW-04
CMMW-05
PARAMETER 11456-1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
<2.0
<2.0
<2.0
300
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
18
<2.0
<2.0
<2.0
<2.0
<4.0
9 0 %
88 %-
Surrogate -Dibromofluoromethane 92 %
Analysis Date 03.08.99
Batch ID 100308
Dilution Factor 2.0
11456-2 11456-2-DL
--------------------
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
310E 340
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<l.O <2.0
<1.0 <2.0
<10 <20
<10 <20
56 58
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<2.0 <4.0
90 % 92 %
88 % 88 %
94 % 94 %
03.08.99 03.09.99
100308 100309
1.0 2.0
--------------------
DATE/
TIME SAMPLED
03-04-99/0955
03-04-99/1030
03-04-99/1030
03-04-99/1200
03-04 -99 /1350
11456-12 11456-13
--------------------
<50 <100
<50 <100
<50 <100
5800 130000E
<50 <100
<50 <100
<50 <100
<50 <100
<50 <100
<500 <1000
<500 <1000
380 11000
<50 <100
<50 <100
<50 <100
<50 <100
<100 <200
90 % 92 %
86 % 86 %
96 % 92 %
03.08.99 03.08.99
100308 100308
50.0 100.0
--------------------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Raleigh, NC 27622 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------------
11456-13-DL CMMW-05 03-04-99/1350
11456-14 REP-1 03-04-99
11456-15 TB-1 03-04-99
-----------------------------------------------------------------------------------------
PARAMETER 11456-13-DL 11456-14 11456-15
-----------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <2000
Bromomethane, ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
·Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
<2000
<2000
<2000
<10000
<50000
<2000
<2000
<2000
<2000
<2000
<2000
<2000
<20000
<2000
<2000
<2000
<2000
<2000
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2.0
63
<2.0
<2.0
<2.0
<20
<2.0
<2.0
<2.0
<2.0
<2.0
<1.0
<l.0
<l. 0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
-----------------------------------------------------------------
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------------
11456-13-DL CMMW-05 03-04-99/1350
11456-14 REP-1 03-04-99
11456-15 TB-1 03-04-99
-----------------------------------------------------------------------------------------
PARAMETER 11456-13-DL
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone
(MIBK) , ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Analysis Date
Batch ID
Dilution Factor
<2000
180000
<2000
<2000
<2000
<2000
<2000
<20000
<20000
14000
<2000
<2000
<2000
<2000
<4000
92 %
92 %
94 %
03.09.99
100309
2000.0
11456-14
<2,0
340
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
62
<2.0
<2.0
<2.0
<2.0
<4.0
90 %
86 %
94 %
03.08.99
100308
2.0
11456-15
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
92 %
88 %
92 %
03.08.99
100308
1. 0
-----------------------------------------------------------------
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SL SAVANNAH LABORATORIES
• & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S9·11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098·A
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0190
Sampled By: Client
Code: 173090324
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
----------------------------------------------------------------------------------------·
11456·3 CMMW-04 03·04·99/1200
-----------------------------------------------------------------------------------------
PARAMETER 11456·3
Cyanide, Total (9010), mg/1 0.25
Prep Date 03.08.99
Analysis Date 03.15.99
Batch ID 0308T
Dilution Factor 2.0
Cyanide, Amenable (9010), mg/1 0.25
Prep Date 03.08.99
Analysis Date 03.15.99
Batch ID 0308T
Dilution Factor 2.0
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5702 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11456-4 Method Blank
Method Blank 11456-16
11456-5
11456-17
11456-6
Lab Control Standard% Recovery
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
PARAMETER
Vol~tiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane, ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
11456-4
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
11456-16
<1.0
<1.0
<1.0
<l. o
<5.0
<25
<1.0
<l. o
<l. o
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
11456-5 11456-17 11456-6
104 % 105 % 46-147 %
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------------
11456-4 Method Blank
11456-16
11456-5
11456-17
11456-6
Method Blank
Lab Control Standard% Recovery
Lab Control Standard% Recovery
LCS Accuracy Control Limit {%R)
-----------------------------------------------------------------------
PARAMETER 11456-4 11456-16 11456-5 11456-17 11456-6
-------------------------------------------------------------------------------
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene1 ug/1
Dibromochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
cis-1,3-Dichloropropene, ug/1 <1.0
Bromoform, ug/1 <1.0
2-Hexanone, ug/1 <10
4-Methyl-2-pentanone (MIBK), ug/1 <10
Tetrachloroethene, ug/1 <1.0
Toluene, ug/1 <1.0
Chlorobenzene, ug/1 <1.0
Ethylbenzene, ug/1 <1.0
Styrene, ug/1 <1.0
Xylenes, ug/1 <2.0
Surrogate Toluene-dB 90 %
Surrogate -4-Bromofluorobenzene 86 %
Surrogate -Dibromofluoromethane 92 %
Analysis Date 03.08.99
Batch ID 100308
Dilution Factor 1.0
<l. 0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<l. 0
<2.0
92 %
8 8 %
90 %
03.09.99
100309
1.0
98 %
98 %
96 %
94 %
92 %
86 %
92 %
03.08.99
100308
1.0
----------
103 %
102 %
100 %
97 %
91 %
87 %
91 %
03.09.99
100309
1.0
----------
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190
Sampled By: Client
Code: 173090324
REPORT OF RESULTS Page 8
LOG NO
11456-4
11456-16
11456-5
11456-17
11456-6
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
--------------------------------------------------
Method Blank
Method Blank
Lab Control Standard% Recovery
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
DATE/
TIME SAMPLED
-------- ------ -------- - ---- - ------ - - - ---------------------- ------------
PARAMETER
Cyanide, Total (9010), mg/1
Prep Date
Analysis Date
Batch ID
Dilution Factor
Cyanide, Amenable (9010), mg/1
Prep Date
Analy"sis Date
Batch ID
Dilution Factor
11456-4
<0.0050
03.08.99
03.15.99
0308T
1.0
<0.0050
03.08.99
03.15.99
0308T
1. 0
11456-16 11456-5
90 %-
03.08.99
03.10.99
0308T
1. 0
11456-17 11456-6
85-115 %
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SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S9-11456
Received: OS MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LT0#113098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190
Sampled By: Client
Code: 173090324
Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
11456-7 MS% Recovery(Batch)
11456-8 MSD % Recovery(Batch)
11456-9 MS Accuracy Advisory Limit (%R)
11456-10 Precision (%RPO) MS/MSD
11456-11 MS Precision Advisory Limit (%RPD)
PARAMETER
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
11456-7
110 %
100 %
100 %-
100 %-
96 %
91 %-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane 94 %
85 %
Analysis Date 03.16.99
Batch ID 100316
Dilution Factor
Cyanide, Total (9010), rng/1
Prep Date
Analysis Date
Batch ID
Dilution Factor
1.0
0 %-
03.08.99
03.10.99
0308T
1. 0
11456-8
120 %-
130 %-
110 %
110 %
110 %-
90 %
87 %
89 %-
03.16.99
100316
1. 0
0 %-
03.08.99
03.10.99
0308T
1.0
11456-9
46-147 %
56-143 %
62-135 %
68-131 %
72-127 %
67-134 %-
67-132 %-
64-142 %-
75-125 %-
11456-10
8.7 %
26 %
9.5 %
9.5 %-
14 %-
1.1 %-
2.3 %-
5.5 %-
03.16.99
100316
1. 0
0 %
03.08.99
03.10.99
0308T
1.0
11456-11
<30 %
<3 5 %
<37 %
<33 %
<22 %
<30 %
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I
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 La Roche Avenue • Savannah. GA 31404 • [phone] • Fax [phone]
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27622
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S9-11456
Received: 05 MAR 99
Reported: 23 MAR 99
Revised: 24 MAR 99
Client PO. No.: LTO#ll3098-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190
Sampled By: Client
Code: 173090324
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------------------------------------------------------------------------------------·
----------------------------------------------------------------------------------------·
PARAMETER
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
J = Estimated result between the reporting limit (RL) and the method detection
limit (MDL) .
E = Result is above the upper calibration limit; therefore, dilution is
required.
Angie Stewart, Project Manager
Final Page Of Report
-------------------.'@YGERAGHTY
AP'& MILLER, INC. Laboratory Task Order No.___ CHAIN-OF-CUSTODY RECORD Page_~_ot_l_
J1!liiJ/ £11 i'i ron men ta I Services
Project Number N<-0 2 6 2-C-d~z:_o_-__ _
Project Location VI c=: ✓-=<d~·~!V~C~--­
Laboratory ~-·~. /, C..e,h5 ~·~,-~-----
Sampler(s)/ Affiliation / (/1,.,..,:5 ""-
Lwi:J=£ ,ce._;1 __
Date/Time
SIIMPLE IDENTITY Code Sampled Lab ID
(Mn,,:,-/;:; L R/'/t<rf
r;~ ,;,;
/nr-1w-01 L :-:,./1//t?
/ (.) :~o
/Hf'lc.J.O'f l. ~/1//fl . ,z.v-
IMMw ·o'{ l J/-1/f/
!?."'°
(. f'.-< ,.., 0-o...S L 51r~'{,5c,
Pc..,.., -I l_ 3/t//77
Tl<,-/ L -
Sample Code: L = Liquid; S = Solid; A = Air
I
3
3
1_
3
3
SAMPLE BOTTLE / CONTAINER DESCRIPTION
Total No. of Bottles/
Containers
I
TOTAL
~----~
Date_3__J_f_j_J_7_ Time~/ '~(=CC~>-c----eal Intact?
Date J / < l£1Time 7f .' VO \.Yes 1No N/A
Relinquished by: ___________ Organization: ___________ _ Date t t Time s;al Intact?
Received by: Organization: Date t t Time Yes No NIA
Special Instructions/Remarks:--------------------------------------------
,--, I -'-,....,_