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HomeMy WebLinkAboutNCD122263825_19951215_JFD Electronics - Channel Master_FRBCERCLA SPD_NPDES Permit Application-OCRI I I I I I I I I I I I I I I I I I I 0 NPDES PERMIT APPLICATION REcc-•• •:o DEC 21 1995 SUPEAFU Nos1:cr,0N JFD ELECTRONICS/CHANNEL MASTER CERCLASITE OXFORD, NORTH CAROLINA December 15, 199 5 Prepared for: JFD Electronics/Channel Master 620 West Industry Drive Oxford, North Carolina 27565 Prepared by: Geraghty & Miller, Inc. CrossPointe II 2840 Plaza Place, Suite 3 50 Raleigh, North Carolina (919) 571-1662 GERAGHTY & MILLER. INC. 0 I I I I I I I I I I I I I I 'I I I I I t-...ortn CarOilna ut'pt. o; c.~1,ii~;11:1c::1~, r.cc:, .. ,,, G ·-·'-·--· .-,-.. ___ , _ .... _ Division or Environmental Management, P.O. Box 29535, Aalelgh, NC 27626-0535 NATIONAL POLL UT ANT 015CHAAGE ELIMINATION SYSTEM APPLICATION N\JM8£R APPLICATION FOR PEAMIT OISCHAAGE SHORT FORM C-GW F""~-.~_..-..._. Date Rtce1vt0 ,,,, l. I To be filed by persons engaged In groundwater remediat Ion pro Jects. ( DEM USE ONLY) Do not attempt to complete this form before reading accompanying Instructions. (Please print or type) 1. Name, address, location, 21'\d telephone number or racllity producing discharge A. Name JFD Electronics/Channel Master B. Malling address 1. Street address see Appendix A 2. City_________ 3. State _________ _ 4. ZIP _________ _ C. Loe at ion: 1. Street 620 west Industry Drive 2. City oxford 3.State Horth carolina 4_ County Granville D. TelephOne No. (_)-see Appendix A E. Nature or business Fonoerly manufactured television antennas 2. Fac111ty contact A. Name see Appendix A B. Title _______________ C. Telephone No. (_) ----- 3. The application Is for Ii) a new permit, Qpermlt renewal, □Permit modification. SIC I I l l ! llf known>. If application is ror renewal or modification, please Indicate permit number: NCOQ, ______ _ 4. Product(s) recovered __ So_l_v_en_t_s_·_c_on_t_a_m_i "_a_t_ed_9"""r_o_on_dva_t_e_r ________ _ [Diesel fuel, leaded or unleaded fuel, solvents, etc.) This application must also Include the following: Al A report or alternatives to surface water discharge as outlined by N.C. Permit and Engineering Unit's 0 Gu1dance for Evaluation or wastewater Disposal Alternatives: [Required by ISA NCAC 2H .0105 <c>l (See Appendix Bl B> An engineering proposal deta111ng the remediation project. [Required by ISA NCAC 2H .0105 (c)l (See enclosed Preliminary Design Report-Appendix C.I C> A listing or -atrf chemicals round in detectable amounts with the maximum observed concentration reportec1 The summary or analytical results containing this maximum value should also be submitted !i.e. the listing, not the graphical scan>. The most recent sample must be no older than one yeu l)fevlous to the date or this application. (See Appendix DI For fuel remediation projects, volatile organic compounds should be scanned along with any suSPected fuel additives. The following compounds should be Included: benzene•, toluene•, ·ethylbenzene•, xylene•, lead, methyl tert·butylether IMTBEl, dlbromoethane <EDBl, 1,2·dichloroethane, lsopropyl ether, naphthalene, phenol. • AA EPA approved methOd capable or detection levels to I ppb Should be used to detect these comooi.l\ds I I I I I I I I I I I I I I I I I I For solvents or unfdentfffed products, an EPA Method 624/625 analysts snovld be provided, wfth the 10 largest peaks. not fdentfffed as one or the targeted compounds IJld not present fn the proceoural blank, ldentHted and approximately QUantltated. [As per the same guidance stipulated on NCDEM's "Annual Pollutant Analysts Monitoring (APAM) ReQUlrement -Reporting Form A; Revised June 1990]. 1r metals or pesticides are suspected to be present, these st\ould be analyzed to the same detection level as presented In the NC APAM. Dl The removal errtclency or each compound detected ror the proposed project ShOuld be provided, 1f known. 5. Name or receiving water _-=.F.::ci:csh::.:ic;;;;n"'g_c::.:rc..:ec;:ek:c;._ ______________ _ Attach a USGS topographical map wfth all discharge pofnts clearly marked. 6. Is potential discharge directly to the receiving water? If not. state soecmcalll! the discharge pofnt. Dnrernerl tri bntary of the Fishing Creek. Mark clearly the pathway to the potential receiving water on the stte map. [This Includes tracing the pathway or the storm sewer to fts discharge pofnt. If a storm sewer fs the only vtable means or discharge.I 7. Amount or treated groundwater to be discharged fn gallons per operating day: Estimated average • 43,000 god; Maximum discharge = so ,ooo gpd e. Describe the duration and rreauency or the discharge <continuous, Intermittent, seasonal) Including the monthS or discharge, number or days per week or discharge. volume treated <monthly average flow fn gallons per day>. xear round -continuous; Monthly average= 43,000 gpd, I cert1ry that I am ram111ar wfth the Information contained fn the app11catlon and that to the best or my knowledge and belier such tnrormatfon ts true, complete, and accurate. Brian Keapner, The Uni.max Corp., Vice-President David Birk, Avnet, Inc., Senior Vice-President Date App 1tcat1on Stgned North Caro11na General Statute 143-215.6 (bl (2) provides that: Af"'I person who knowingly makes any false statement representatfon, or certlf1catlon fn any appllcatfon, record, rePol't. plan or other document ffles or reaulred to be maintained under Article 21 or regulations or the Environmental Management Commission fmplementfng that Article, or whO falsffles, tampers wfth or knowingly renders Inaccurate any recording or mon1torfng device or method reQufred to be operated or mafntafned under Article 21 or regulations or the Environmental Management Commtssfon tmplementtng that Article, shall be guflty or a misdemeanor punishable by a fine not to exceed S 10,000. or by Imprison- ment not to exceed sfx months, or by both. < 18 U.S.C. Section 1001 provides a punishment by a ffne of not more than S 10,000 or fmprfsonment not more than 5 years, or both, for a slmflar orrense.l I I I I I I I I I I I I I I I I I I I ~ ' 0 .. 0 ~ 6 :z Je < er C IOOOB::RH·==j•OOO~=~,OOOE::==JOOOE=~-E::=~"'°°E=:36000==~'000 SCALE 1: 24000 .n Contour Interval 10 Feet Datum is Mean Seo Level "' ~ r----------u_. s_. G_._s_. 7 1r. 5_M_in_u..:.te:........:.S_er..:.ie..:.s_O.:..x.:..f o.:..r..:.d:..· .:..N..:..C.:.. . ..;T..:.o!:.po:..:g;:.r~op::.:.h::.:ic:.....:O.::.uo:::d;::.r::::on::_:g~I e:::_. ___ "T"-__ ~ 0 FIGURE 8 < C .A.,. GERAGHTY Air' & MILLER, INC. 41' Environmental Seruices SITE LOCATION MAP JFO ELECTRONICS/CHANNEL MASTER OXFORD, NORTH CAROLINA 1 -- ---- - - owe DAT[: 1151,1AY9~ PRJCT NO.: NC0202.0eo fll( NO.: CHANN(L l[G[NO 0-OV[RfLOW PR[V[NTIQN fLOAT 6)-f'LOW SWITCH M SAr.APL[ PORT [)-(] CLOS[ VALVE [) CHECK VALVE [XJ GATE VALVE 0, PRESSURE GAUGE l2J TQTALll[R GROUNDWATER [XTRACTION WELL ,.,, GERAGHTY Al .. & MILLER, INC. .. Environm.ental Services - -- -- -- OR.A.WING: Pf 0-R CH[O<[D: N. SH( TTY APPROV(D: l. I.IQR[lZ FLOW "ETER ) AIR OUT WATER ',:,=z:'l _ IN ~ -"IST ELl"INATOR AIR IN AIR STRIPPER OBSERVATION PORT PROCESS FLOW DIAGRAM PRELIMINARY REMEDIAL DESIGN JFD ELECTRONICS/CHANNEL "ASTER OXFORD, NORTH CAROLINA EFFLUENT TO STORM SEWER - -- - ORAf"T[R: A. WARREN FIGURE 2 I I I I I APPENDIX A I MAILING ADDRESSES JFD ELECTRONICS/CHANNEL MASTER SITE I OXFORD, GRANVILLE COUNTY, NORTH CAROLINA I I I I I I I I I I I I I GERAGHTY & \1lLLER. !NC 0 I I I I I I I I I I I I I I I I I I I APPENDIX A MAILING ADDRESSES JFD ELECTRONICS/CHANNEL MASTER SITE OXFORD, GRANVILLE COUNTY, NORTH CAROLINA MAILING ADDRESSES A. B. Address and Contact for JFD Electronics: The Unimax Corporation 54 East 64th Street New York, NY 10021 Contact: Mr. Brian Kempner Vice President Telephone: (212) 755-8800 Address and Contact for Channel Master: AVNET, Inc. 80 Cutter Mill Road Great Neck, NY I I 02 I Contact: Ms. Lisa Palumbo Assistance General Counsel and Assistant Secretary Telephone: (516) 466-7000 GERAGHTY & /-.(ILLER. INC 0 I I I I I APPENDIXB I EVALUATION OF WASTEWATER DISPOSAL ALTERNATIVES JFD ELECTRONICS/CHANNEL MASTER NPL SITE I OXFORD, NORTH CAROLINA I I I I I I I I I I I I GERAGHTY C:1' MILLER. INC. 0 I I I I I I I I I I I I I I I I I I I I. APPENDIX B EVALUATION OF WASTEWATER DISPOSAL ALTERNATIVES JFD ELECTRONICS/CHANNEL MASTER NPL SITE OXFORD, NORTH CAROLINA GENERAL INFORMATION A. B. C. D. Fac.!_lity Name: County: Address: JFD Electronics/Channel Master NPL Site Granville 620 West Industry Drive, Oxford, North Carolina Report Preparer's Name: Nanjundeswar V. Shetty, P.E. No. 021028 Gregory Rorech, P.E. No. 021328 Report Preparer's Address: Geraghty & Miller, Inc., /GMCE, Inc. 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Description of the proposed Discharge Facility: Figure I presents the site location map for the JFD Electronics/Channel Master NPL site. The groundwater remedial design process is in progress under the United States Environmental Protection Agency (USEPA) supervision. A preliminary design report, representing 3 0 percent design, was submitted to USEPA in July 1995. Currently, the pre-final design (90 percent) is being prepared. The preliminary design proposed withdrawal of contaminated groundwater using a total of eight extraction wells with total extraction rate of approximately 30 gallons per minute (continuous). The extracted groundwater will be treated above ground using an air stripper to remove volatile organic compounds. The treated effluent is proposed to be discharged into an unnamed creek that runs along the eastern property boundary which ultimately discharges into the Fishing Creek ( see site map and process flow diagram in the enclosed preliminary design report). The proposed discharge to the surface water is from a groundwater treatment system. This is not a domestic wastewater treatment plant (WWTP). This is not a phased development project. I of3 GERAGHTY & MILLER. INC 0 I I I I I I I I I I I I I I I I I I II. APPENDIXB EVALUATION OF WASTEWATER DISPOSAL ALTERNATIVES JFD ELECTRONICS/CHANNEL MASTER NPL SITE OXFORD, NORTH CAROLINA EVALUATION OF ENVIRONMENTAL FEASIBILITY OF DISCHARGE ALTERNATIVES A. Environmental Feasibility of all three of the following non-discharge alternatives: 1. 2. Connection to Sewerage System: a. Existing Sewerage System: An existing sewer is located along the southern property boundary of the JFD Electronics/Channel Master site property. (2) (3) Sewer on the property is currently connected to the City of Oxford WWTP. City of Oxford has denied requests to discharge the effluent from the proposed groundwater treatment system. The discharge point ( unnamed tributary) is located on the JFD Electronics/Channel Master property. (4) see attached topographic map (Figure !). Subsurface Disposal System: Based on site investigation reports, the stratigraphy beneath the site property consists of overburden layer composed of shallow clayey fill on the site property, with alluvium in the southeast swale area. These clayey soils overlay a feldspathic sand saprolite that gradually grades in to a decomposed granitic rock that has volcanic inclusions. The total thickness of these overburden materials averages approximately 58 feet. Depths to groundwater approximately varies between 7 and IO feet below ground surface. As indicated above, the unsaturated soils at the site, typically consisting of low permeability clayey soils, are not very conductive. Due to low permeability soils, a large area is required to infiltrate the recovered groundwater without creating excessive mounding. Infiltration of treated groundwater upgradient of the contaminant plume is not feasible due to 2 of3 a:~~02.0IJ',1)(11~.....iu-..f, GERAGHTY & \·llLLER. lNC. 0 I I I I I I I I I I I I I I I I I I I m. B. APPENDIX B EVALUATION OF WASTEWATER DISPOSAL ALTERNATIVES JFD ELECTRONICS/CHANNEL MASTER NPL SITE OXFORD, NORTH CAROLINA limited area for locating the infiltration gallery. Therefore, subsurface disposal system is not a feasible option. 3. Spray Irrigation System: As indicated Section 11.A.2., the presence of low permeability clayey soils beneath the facility requires a large area for infiltrating the treated effluent through spray irrigation. Due to limited availability of the land area for spray irrigation, this is not a feasible option. None of the alternatives in Section II.A. is feasible. C. Environmental Feasibility of the Discharge to a Flowing Stream: An intermittent stream/tributary to the Fishing Creek flows along the eastern property boundary of the JFD Electronics/Channel Master site. The preliminary design report proposed disposal of the treated groundwater to this intermittent stream. Based on a conversation with United States Geological Survey, the intermittent stream appears to be a zero discharge stream. COST ESTIMATION AND COMPARISON This section is not completed since the alternatives in Section II. A. are not technically feasible. 3 of3 ~~~02.0ll"XII ~ _.,I ,.o.....,, GERAGHTY & MILLER. INC. 0 I I I I I APPENDIX C I PRELIMINARY DESIGN REPORT GROUNDWATER REMEDIATION I JFD ELECTRONICS/CHANNEL MASTER NPL SITE OXFORD, NORTH CAROLINA I I I I I I I I I I I I GERAGHTY & MILLER. INC. 0 I I I I I I I I I I I I I I I I I I I Source: APPENDIXD GROUNDWATER ANALYTICAL REPORT JFD ELECTRONICS/CHANNEL MASTER OXFORD, NORTH CAROLINA Tables 4-3 through 4-11 and the analytical reports, are from the Pre-Design Data Acquisition Report for JFD Electronics/Channel Master Site, submitted in June 1995. GERAGHTY & i\·IILLER. 1"1C. 0 ·---- -- -- - - - -- - - - -- - Page I of7 Table 4-3. Phase I Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: SMEOI JFD-CMMW0 1-00 I JFD-CMMW02-00 I CMMW02-001 (DL) JFD-CMMW03-001 Sample Date: 9/26/94 9/27/94 I0/12/94 I0/12/94 10/12/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Intermediate Intermediate Intermediate Intermediate Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: 8445225•1 S445255•t S445566A•t S445566A•4 S445566A•2 Concentration Unit: µg/L µg/L µg/L µg/L µg/L Benzene 10 U IOU IOU z IOU Bromodichloromethane 10 U IOU IOU z IOU Carbon Tetrachloride 10 U IOU 10 U z IOU Chlorobcn,,e:nc 10 U IOU 10 U z IOU Chloroform IOU IOU IOU z 21 l, 1-Dichloroethane IOU IOU IOU z IOU l, 1-Dichloroethene IOU IOU 21 z 2 1 1,2-Dichloroethene (total) IOU IOUJ 93 z 100 2,Hexanone 10 U IOU IOU z IOU Methylene chloride IOU IOU 10 U z IOU Tetrachloroethene 10 U IOU z 2600D z Toluene IOU 17U IOU z IOU I, I, I-Trichloroethane 10 U IOU 10 U z IOU Trichloroethene 10 U IOU z 7500 D z Vinyl chloride 10 U IOU 10 U z 11 µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. 1 Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated method blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0201.0J0\2281chaa\tebk4-J xbOOl/9'::, GERAGHTY 8 fVIILLER. INC. 0 - ---- ---- ---- --- - --Page 2 of7 Table 4-3. Phase I Groundwater Sample Quality TCL voe Data SU111l1131)', JFD Electronics/Channel Master, Inc., Oxford, Nonh Carolina. Sample Name: CMMW03--001 (DL) JFD-<::MMW04--00 I CMMW04--001 (DL) JFD-<::MMW05--00 I CMMW05--001 (DL) Sample Date: 10/12/94 10/11/94 10/11/94 10/13/94 10/13/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: lntenned.iate Intermediate Intermediate Intermediate Intermediate Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S445566A•5 S445540A•8 S44SS40A • II S445588A•I S445588A•8 Concentration Unit: µg/L µg/L µg/L µg/L µg/L Benzene z 10 U z I J z Bromodichloromethane z IOU z 10 UJ z Camon Tetrachloride z 10 U z 51 z Chlorobenzene z IOU z 10 UJ z Chloroform z IOU z 21 z I, 1-Dichloroethane z J3 z IOUJ z I, 1-Dichloroethene z 10 U z 29 J z 1,2-Dichloroethene (total) z 58 z z 710 DJ 2-Hexanone z IOU z 41 z Methylene chloride z 10 U z 34 UJ z Tetrachloroethene 1500 D z 440 DJ z 6500D Toluene z IOU z IOUJ z 1, 1, I-Trichloroethane z IOU z 61 z Trichloroethene 10000 D z 5600D z 35000 D Vinyl chloride z 21 z IOUJ z µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. · J Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated method blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0202 030\2281 chan\table4-l.xb\Yl 1/9, GERAGHTY {,r i\.111 .. LFR. INC. 0 -- - --- - -- ---- - - -- - - Page 3 of7 Table 4-3. Phase I Groundwater Sample Quality TCL voe Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMWOSR-00 I CMMWOSR-OOl(DL) JFD-CMMW06-00 I SMMW06-00 I (DL) JFD-CMMW07-001 Sample Date: 10/13/94 10/13/94 10/07/94 10/07/94 10/11/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Intermediate Intermediate Intermediate Intermediate Shallow Bedrock Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S445588A•2 S445588A•9 S445489•1 S445489•5 S445540A•7 Concentration Unit: µg/L µg/L µg/L (µg/L) µg/L Benzene 1000 Ul z IOUJ z IOU Bromodichloromethane IOOOUl z IOUJ z IOU Carbon Tetrachloride 1000 Ul z IOUJ z IOU Chlorobenzene 1000 UJ z 0.7 1 z IOU Chloroform 1000 Ul z IOUJ z 10 U l, 1-Dichloroethane 1000 Ul z I 1 z IOU l, 1-Dichloroethene 1000 Ul z 21 z IOU 1,2-Dichloroethene (total) 6701 z 161 z 21 2-Hexanone 1000 UJ z IOUJ z 10 U Methylene chloride 1000 UJ z 10 Ul z 2 1 Tetrachloroethene 6500 z z 220 D 22 U Toluene 1000 UJ z 16 Ul z IOU l, l, 1-Trichloroethane 1000 Ul z IOUJ z 10 U Trichlorocthene z 34000 D 561 z 32 U Vinyl chloride 1000 UJ z IOUJ z IIOU µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. 1 Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated method blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC020l.0)0U28J chan\tabk4-3.xk\YJ l/9l GERAGHTY & MILLER. INC. 0 -------------------Page 4 of7 Table 4-3. Phase I Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD.CMMW0S--00 I JFD.CMMW09--00 I JFD.CMMWI0--00 I CMMW I 0--00 I (DL) JFD.CMMW I I --00 I Sample Date: 9/27/94 9/28/94 10/13/94 10/13/94 9/29/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Bedrock Shallow Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: 5445255•2 S44527)•) 5445588A•7 5445588A•I I 5445311 •2 Concentration Unit: µg/L µg/L µg/L µg/L µg/L Benzene 10 U IOU 100 U z 10 U Bromodichloromethane IOU IOU 100 U z IOU Camon Tetrachloride 10 U 10 U 26 J z 0.6 J Chlorobenzene IOU IOU 100 U z IOU Chloroform 10 U IOU 91 z 10 U I, 1-Dichloroethane 10 U 10 U 100 U z 14 I, 1-Dichloroethene IOU 10 U 120 z 15 1,2-Dichloroethene (total) 10 U 10 U 610 z 28 2-Hexanone 10 U IOU 100 U z 10 U Methylene chloride 10 U 10 U 220 B z 21 Tetrachloroethene 10 U 10 U z 5300 DJ llO Toluene IOU IOU 100 U z 10 U I, I, I-Trichloroethane IOU 10 U 30 J z 5 J Trichloroethene IOU IOU z 160000 D 52 Vinyl chloride IOU 10 U 100 U z IOU µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. J Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated blank sample. Z . Compound concentration was not used. Sample data an: a combination of two analytical runs. NC0202 OJO',Jl81dian\table4-).xb\.V31/95 GERAGHTY & MILLER. INC. U - - - -- --- -- - -- - - -- - - Page S of7 Table 4-3. Phase I Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW12-001 CMMW12-001 (DL) JFD-CMMWl3-00I CMMWIJ-001 (DL) JFD-CMMWlJR-001 Sample Date: 9/29/94 9/29/94 10/11/94 10/11/94 10/11/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Top of Rock TopofRock Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S445311 •1 8445311•4 S44SS40A0 1 S44SS40A•9 S44SS40A0 2 Concentration Unit: µg/L (µg/L) µg/L (µg/L) µg/L Benzene 10 U z 10 U z IOU Bromodichloromethane 10 U z 10 U z IOU Camon Tetrachloride 10 U z 10 U z 10 U Chlorobenzcne IOU z 10 U z 10 U Chloroform IOU z 10 U z IOU I, 1-Dichloroethane IOU z 0.9 J z 0.8 J I, 1-Dichloroethene IOU z 7J z 61 1,2-Dichloroethene (total) I J z z 300 DJ z 2-Hexanone IOU z IOU z IOU Methylene chloride 2J z 10 U z 10 U Tetrachlorocthene IS U z z 2800 D z Toluene IOU z 17 U z 19 U I, I, I-Trichloroethane IOU z 10 U z IOU Trichloroethene z 610 D z 6600D z Vinyl chloride 10 U z 2J z 2J µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. J Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0201.0)0\.2lS!chan\table4-3.x.lsWl 119, GERAGHTY & MILLER. INC. -------------------Page 6 of7 Table 4-3. Phase I Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. I Sample Name: CMMWl3R-OOl(DL) JFD-CMMWl4-00I JFD-CMMWI S-00 I JFD-CMMWl6-00 I CMMWl6-00I (DL) Sample Date: 10/11/94 10/03/94 10/03/94 10/07/94 10/07/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Shallow Top of Rock Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S44SS40A*I0 S44S362*1 8445362*2 S44S489*2 S445489*6 Concentration Unit: (µg/L) µg/L µg/L µg/L (µg/L) Benzene z IOU 10 U 10 U z Bromodichloromethane z 10 U 2J 10 U z Carbon Tetrachloride z 10 U IOU 10 U z Chlorobenzene z IOU IOU 10 U z Chloroform z IOU 10 U IOU z I, 1-Dichloroethane z IOU IOU 0.6 J z I, 1-Dichloroethene z IOU 10 U 2J z 1,2-Dichloroethene (total) 290 DJ IOU 7J z 310 D 2-Hexanone z IOU IOU 10 U z Methylene chloride z IOU IOU 10 U z Tetrachloroethene 2600D IOU 18 U z SIO D Toluene z IOU IOU 38 z I, I, 1-Trichloroethane z IOU IOU 10 U z Trichloroethene 6100 D 10 U 190 z 330D Vinyl chloride z IOU IOU 93 z µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. J Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated method blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0202.030\1281chan~+J.xb\YJl/95 GERAGHTY f<i' MILLER. INC -- -- --- - - - - -- -- - - - - Page 7 of7 Table 4-3. Phase I Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford. North Carolina. Sample Name: JFD-CMMWI 7--001 JFD-CMMWI8--001 JFD-CMMW19--00I JFD-CMMW2 l--OO JFD-TW24--00 I TW24--00 I (DL) Sample Date: 10/11/94 10/07/94 10/05/94 10/05/94 10/05/94 10/05/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Deep Bedrock Shallow Bedrock Intermediate Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: S445540A•6 S445489•3 S445438C•5 S445438C•4 S445438C•i S445438C•6 Concentration Unit: µg/L µg/L µg/L µg/L µg/L (µg/L) Benzene IOU IOU IOU 2J IOU z Bromodichloromethane 10 U IOU IOU 10 U 10 U z Camon Tetrachloride IOU IOU IOU 10 U 10 U z Chlorobenzene 10 U IOU 10 U 20 IOU z Chloroform 10 U IOU IOU 10 U 10 U z I, 1-Dichloroethane IOU IOU IOU I J IOU z I, 1-Dichloroethene IOU IOU 10 U IOU IOU z 1,2-Dichloroethene (total) I J IOU 10 U 180 160 z 2-Hexanone IOU IOU 10 U IOU IOU z Methylene chloride IOU IOU 10 U IOU IOU z Tetrachloroethene 27 U IOU 10 U 100 z 850 D Toluene 10 U 140 10 U 10 U IOU z I, I, I-Trichloroethane IOU IOU 10 U 10 U 10 U z Trichloroethene 19 U IOU 10 U 72 99 z Vinyl chloride IOU IOU 10 U 10 U 10 U z µg/L Micrograms per liter. U Compound was not detected above the CRQL or was qualified as undetected due to blank contamination. J Estimated concentration (compound was detected between the MDL and CRQL and/or QC criteria were not met). D Compound was quantitated using a secondary dilution factor. B Compound was detected in the associated blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0'202.0J0\228 I chan\bbk,4.J.xb\Yll/91 GERAGHTY c<f MILLER. INC. 0 -------------------Page I of3 Table 4-4. Phase I Quality Control Sample TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99E-001 JFD-CMMW99E-002 CMMW99E-002(DL) JFD-CMMW99F-001 JFD-CMMW99F-002 JFD-CMMW99T-001 Sample Date: 10/11/94 10/13/94 10/13/94 10/11/94 10/13/94 9/26/94 Sample Type: Equipment Blank Equipment Blank Equipment Blank Field Blank Field Blank Trip Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: Concentration Unit: Acetone 1,2-Dichloropropane Methylene chloride Tetrachloroethene Toluene I, 1,2-Trichloroethane Trichloroethene µg/L Micrograms per liter. S445540A*4 µg/L 10 U IOU JOU 32 21 IOU 28 U Compound was not detected above the CRQL. S445588A*3 S445588A • 10 µg/L µg/L IOU z IOU z 5 BJ z 70 z 12 z 10 U z z 250 D 1 Estimated concentration (compound concentration is between the MDL and CRQL). D Compound was detected using a secondary dilution factor. B Compound was detected in the associated blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0202 030\228 I chal\tt.blo4-◄ xl,.\.YJ I '9' S445540A*3 S445588A*4 5445225*2 µg/L µg/L µg/L 12 B JOU IOU 0.7 J IOU IOU JOU 5 BJ IOU I 1 IOU WV 3 1 21 IOU 0.81 IOU 10 U 3 1 I 1 IOU GERAGHTY 8 l'v11Ll.U{. INC. -------------------Page 2 of3 Table 4-4. Phase I Quality Control Sample TCL VOC Data Summmy, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99T--001 JFD-CMMW99T--002 JFD-CMMW99T--003 JFD-CMMW99T--004 JFD-CMMW99T--OOS Sample Date: 10/11/94 9/27/94 9/28/94 9/29/94 10/03/94 Sample Type: Trip Blank Trip Blank Trip Blank Trip Blank Trip Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S44SS40A*S S44S2SS*3 S44S271*2 S445311 •3 S445362*3 Concentration Unit: µg/L µg/L µg/L µg/L µg/L Acetone IOU IOU 10 U 10 U 10 U 1,2-Dichloropropane IOU IOU 10 U 10 U 10 U Methylene Chloride IOU IOU 10 U IOU IOU Tetrachloroethene IOU 21 10 U IOU IOU Toluene 3 J 2 J 10 U SJ IOU I, 1,2-Trichloroethane IOU 10 U 10 U 10 U 10 U Trichloroethene IOU IOU IOU IOU 10 U µg/L Micrograms per liter. U Compound was not detected above the CRQL. J Estimated concentration (compound concentration is between the MDL and CRQL). D Compound was detected using a secondary dilution factor. B Compound was detected in the associated blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0202.030U28Jchan\t:abk-M.xb0011'95 GERAGHTY S' MII.LER. INC. 0 -------------------Page 3 of3 Table 4-4. Phase I Quality Control Sample TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99T-006 JFD-CMMW99T-007 JFD-CMMW99T-008 JFD-CMMW99T-O 10 JFD-CMMW99T-O 11 Sample Date: IO/OS/94 10/0S/94 10/07/94 10/12/94 10/13/94 Sample Type: Trip Blank Trip Blank Trip Blank Trip Blank Trip Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S44S438C0 2 S44S438C•3 5445489°4 S44SS66A03 S44SS88A0 S Concentration Unit: µg/L µg/L µg/L µg/L µg/L Acetone IOU IOU IOU 10 U 10 U 1,2-Dichloropropane IOU IOU IOU IOU IOU Methylene Chloride 2 J IOU 10 U 10 U 4 BJ Tetrachloroethene 3 J 2J 0.8 J 3J IOU Toluene 3 J 10 U 12 I J I J l, 1,2-Trichloroethane 10 U 10 U 10 U IOU 10 U Trichloroethene 10 U 10 U 10 U 10 J 10 U µg/L Micrograms per liter. U Compound was not detected above the CRQL. J Estimated concentration (compound concentration is between the MDL and CRQL). D Compound was detected using a secondary dilution factor. B Compound was detected in the associated blank sample. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NCOlOl 0l0\1111 than\t..bl.4-4.xbOOl /9' GERAGHTY 8 l'vllLU:R. INC. ·-- - - - - - - - ----- - - - - - Page I ofl Table 4-5. Phase I Groundwater Sample Quality TCL SVOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW0l-001 JFD-CMMW0S-001 JFD-CMMWI0-001 JFD-CMMWll-00 I JFD-CMMW13-00I JFD-CMMW IJR-00 I Sample Date: 10/12/94 10/13/94 10/13/94 9/29/94 10/11/94 10/11/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Intermediate Intermediate Shallow Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: S44SS66•t S44Ssss•1 S44SS88•2 S44SJ11C•t S44SS40•J S44SS40•4 Concentration Unit: µg/L µg/L µg/L µg/L µg/L µg/L 1,2-Dichlorobenzene 10 U IOU 10 U IOU IOU IOU 1,3-Dichlorobenzene 10 U IOU 10 U 10 U IOU IOU 1,4-Dichlorobenzene 10 U IOU O.S J IOU IOU IOU Naphthalene 10 U 10 U 0.6 J 10 U 10 U 10 U µg/L Micrograms per liter. U Compound was not detected above the CRQL. J Estimated concentration (compound concentration is between the MDL and CRQL). D Compound was detected using a secondary dilution factor. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NC0102.030\221l chan\lablc-4-,.U\Yl 1/9, GERAGHTY 8 MILLER. INC. 0 - - - -- - - - - -- -- - - -- - - Page 2 of2 Table 4-5. Phase I Groundwater Sample Quality TCL SVOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMWl4-00 I JFD-CMMWI6-001 JFD-CMMW2 l-OO I CMMW21--00I (DL) JFD-TW24-00 I Sample Date: 10/03/94 10/07/94 10/05/94 10/05/94 10/05/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Shallow Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S445362C*l S445489C*l S445438B*2 5445438B*J 5445438B*l Concentration Unit: µg/L µg/L µg/L µg/L µg/L 1,2-Dichlorobenzene IOU IOU z 210 D 10 U 1,3-Dichlorobenzene IOU IOU IOU z IOU I, 4-Dichlorobenzene IOU IOU 14 z IOU Naphthalene IOU IOU IOU z . 10 U µg/L Micrograms per liter. U Compound was not detected above the CRQL. J Estimated concentration (compound concentration is between the MDL and CRQL). D Compound was detected using a secondary dilution factor. Z Compound concentration was not used. Sample data are a combination of two analytical runs. NCOlOl.0».228Iehan\tablc4-S.xb001/9S GERAGHTY E,i' MILLER. INC -------------------Page I of5 Table 4~. Phase I Groundwater Sample Quality Total and Dissolved T AL Metal, Hexavalent Chromium, and Total/ Amenable Cyanide Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: Sample Date: Sample Type: Media: Zone: Laboratory: Lab ID: Concentration Unit: Aluminum Antimony Arsenic Barium Beryllium Calcium Hexavalent chromium Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel Potassium Silver Sodium Vanadium Zinc Cyanide (amenable) Cyanide (total) Total Dissolved Solids (mg/L) µg/L M;crograms per liter. mg/L Milligrams per liter. SMEOI 9/26/94 Monitor Well Groundwater Shallow Savannah S445225°1 µg/L 643 8.9U 1.4 U 40.5 U 0.22 U 9520 U JOU 11.3 U 1.6 U 10.3 U 1660 uu 5450 U 44.1 7.7U 810 U 2.3 U 11000 U 10.4 U 18 U 10 U 10 U NA JFD-CMMWO 1-00 I 9'17/94 Monitor Well Groundwater Intermediate Savannah S445255°1/S445255B•I µg/L J09U 8.9U 1.4 U 29.2 U 0.14 U JOJO() u 10 U 5.2 U 1.6 U 16 U 166 1.4 U 5080 U 7.9U 2.3 U 1270 U 2.3 U 12500 U 7.3 U 19.2 U JOU JOU 150 JFD-CMMWOJ-001 JFD-CMMW02-00I JFD-CMMW03-00J JFD-CMMW04-00I 9/27/94 10/12/94 10/12/94 10/11/94 Monitor Well Groundwater Intermediate Savannah 5445255•1 µg/L (Dissolved) NA NA NA NA NA NA NA NA NA NA 204 NA NA 9.0U NA NA NA NA NA NA NA NA Monitor Well Groundwater Intermediate Savannah S445566A0 1 µg/L 362 J 8.9U 1.4 U 32.2 U 0.21 U 31700U 10 UJ 3.3 U 1.6 U 6.9 U 495 J 1.5 U 13200 U 299 7.4 U 1580 U 2.3 U 20300 U 7.6 U 7.4 UJ JO u JOU NA Monitor Well Gr6undwater Intermediate Savannah S445566A*2 µg/L 143 UJ 8.9U 1.4 U 59.1 U 0.14 U 18200 U JOUJ 3.3 U 1.6 U 4.1 U 313 J 0.91 U 8870 U 385 7.6 U 1100 U 2.3 U 24100 U 6.4U 20.2 UJ JOU JO u NA Monitor Well Groundwater Intermediate Savannah S445540A0 8 µg/L 443 J 10.2 B 1.4 U 59.8 BJ 0.14 U 97400 U 50U 7.7B 3.0U 43.4 U 1050 J 1.8 UJ 55000 24.7 15.1 U 1820 U 2.3 U 33800 U 6.2 U 35.7 UJ 81 354 NA U Compound was not detected above the IDL or was qualified as undctccted due to blank contamination. B Compound coru:cntntion detected u bctwcon tho IDL and CRDL J Compound oonoentration dctcctcd is qualified as estimated (I). NA Compound was not analyzed. GERAGHTY 8 MILLER. INC. - -·-- - - - - - - - - - - - - - - - Page 2 of5 Table 4-6. Phase I Groundwater Sample Quality Total and Dissolved T AL Metal, Hexavalcnt Chromiwn, and Total/ Amenable Cyanide Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW05-00 I JFD-CMMW05R-001 JFD-CMMW06-00 I JFD-CMMW06-00 I JFD-CMMW07-00 I Sample Date: 10/13/94 10/13/94 10nt94 I0n/94 10/11/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Intermediate Intermediate Intermediate Intermediate Shallow Bedrock Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S445588A•! S445588A•2 S445489• 1/S455489B• I S445489•! S445540A•7 Concentration Unit: µg/L µg/L µg/L µg/L (Dissolved) µg/L Aluminum 57 UJ 50.4 UJ 98.7U NA 56UJ Antimony 8.9U 8.9U 8.9U NA 8.9U Arsenic 1.4 U 1.4 U 1.4 U NA 1.4 U Barium 53 U 52.1 U 14.5 U NA 40.7 U Beryllium 0.14 U 0.19 U 0.14 U NA 0.21 U Calcium IJOOOU 12800 U 47800 U NA 44900 U Hexavalent chromium 10 U 10 U 10 U NA 10 U Chromium 3.3 U 3.3 U 3.5 U NA 13.7 Cobalt 1.6 U 1.9 U 1.6 U NA 1.6 U Copper 3.1 U 2.8 U 7.5 U NA 3.1 U Iron 130 J 125 J 84.1 U 17.1 U 75.9 U Lead 0.91 U 0.91 U 0.91 U NA 0.91 U Magnesium 6930U 6820 U 32600 U NA 4340U Manganese 49.6 47.1 320 322 77.2 Nickel 3.9 U 3.6 U 2.3 U NA 5.4 U Potassium 895 U 868U 1230U NA 87200 U Silver 2.3 U 2.5 U 2.3 U NA 2.3 U Sodium 22300 U 21900 U 29500U NA 31500 U Vanadium 5.5 U 7.9U 3.7 U NA 2.4 U Zinc 5.3 U 12.9 U 16 U NA IO.I UJ Cyanide (amenable) IOU 10 U 10 U NA IOU Cyanide (total) 10 U IOU IOU NA IOU Total Dissolved Solids (mg/L) NA NA 400 NA µg/L Micrograms per liter. msfL Milligrams per liter. U Compound was not detcctcd above the IDL or wu qualified as omdctcdcd due to blank a>ntamination. B Compound concentration do:tc<ud is bctwa:n tho IDL and CRDI. J C-Ompound conccntmion do:tc<ud is qualifiod u cotimatod (1). NA Compound wu not analyz.cd. NC0'202.0»'228 I c.hanlrables/I' ABLE4-6.XLS/Y3J/9} GERAGHTY 8 MILLER. INC 0 --- - ---- - -- --- - -- - - Page 3 of5 Table 4-6. Phase I Groundwater Sample Quality Total and Dissolved T AL Metal, Hexavalent Chromium, and TotaV Amenable Cyanide Data Swnmary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW08-00 I JFD-CMMW09-00 I JFD-CMMWI 0-00 I JFD-CMMWI0-001 JFD-CMMWll-001 JFD-CMMW12-00I Sample Date: 9/27/94 9/28/94 10/18/94 10/18/94 9/29/94 9/29/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Bedrock Shallow Shallow Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: $445255•2 S445271 ., S445670•l/S445670B• I S445670•! S445311•2 $445311•1 Concentration Unit: µg/L µg/L µg/L µg/L (Dissolved) µg/L µg/L Aluminum 66.1 U 488 43401 25 UJ 958 67U Antimony 8.9U 8.9U 8.9U 8.9U 8.9U 8.9U Arsenic 1.4 U 2.1 U 1.4 U 2.4 U l.4U 1.4 U Barium 42.8 U 115 BJ 154 BJ 111 BJ 78.1 BJ 12.5 U Beryllium 0.14 U 0.14 U 1.7 U 1.6 U 0.14 U 0.14 U Calcium 10100 U 22700U 11100 U 9770 U 23900 U 16500 U Hexavalent chromium 10 U 10 U 10 U NA 12 10 U Chromium 11.3 U 3.7 U 20.7 3.3 U 3.3 U 3.3 U Cobalt 1.6 U 1.6 U 5.7 B 1.6 U 2.0U 1.6 U Copper 19.1 U 7.0U 14.1 U 4.9U 7.8U 3.6U Iron 134 U 827 11100 U 87.6 UJ 2010 45.9U Lead 2.6 U 0.95 U 5.9 2.6B 1.6 U 0.91 U Magnesium 5570 U 16000 U 8740 U 6620 U 17400 U 12100 U Manganese 4.9U 252 324 194 617 19.8 Nickel 6.6U 3.9 U 25.3 B 7.9U 5.5 U 2.3 U Potassium 1980 U 586 U 701 U 461 U 1060 U 1320 U Silver 2.3 U 2.3 U 2.3 U 2.3 U 2.3 U 2.3 U Sodium 9370 U 23600 U 42200 U 41000 U 22100 U 13400 U Vanadium 5.1 U 6.7U 33.8 BJ 7.8 U 10.4 U 6.9 U Zinc 15.2 U 15.9 U 32 UJ 4.5 UJ 17.1 U 11.8 U Cyanide (amenable) IOU IOU 10 U NA IOU 10 U Cyanide (total) 10 U 10 U IOU IOU IOU 10 U Total Dissolved Solids (mg/L) NA NA 320 NA NA µwt, Micrograms per liter. mgiL Milligrams per-liter. u Compound was not detected above the IDL or wu qualified u unddectcd due to blank contamination. 8 Compound ooncentntioo ddeaod ia bctwom the IDL and CRDL J Compound concentratioo ddeaod ia qualified u estimated (J). NA Compound wu not analyzed. GERAGHTY f<f MILLER. INC 0 NC0102.0)0(2281chanlllblc.rrABLE-4-6.XLSIYll/9~ -------------------Page 4 of S Table 4~. Phase I Groundwater Sample Quality Total and Dissolved TAL Metal, Hexavalent Chromium, and Total/Amenable Cyanide Data Sunuruuy, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMWl3-00 I JFD-CMMWl3-00I JFD-CMMWl3R-001 JFD-CMMWl3R-OO I JFD-CMMW14-00I Sample Date: 10/11/94 10/11/94 10/11/94 10/11/94 10/3/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Groundwater Groundwater Zone: Shallow Shallow Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S44SS40A • l/S44SS40C*2 S44SS40A*l S44SS40A*2 S44SS40A*2 S445362*1 Concentration Unit: µg/L µg/L (Dissolved) µg/L µg/L (Dissolved) µg/L Aluminum 899 J NA 1190 J NA 40,6 U Antimony 8.9 U NA 11.7 B NA 8.9U Arsenic 2.3 U NA 1.8 U NA 1.4 UJ Barium 194 BJ NA !SJ BJ NA 121 BJ Beryllium 0.14 U NA 0.47 U NA 0.14 U Calcium 27200 U NA 27800 U NA 49500 U Hexavalent chromium IOU NA 10 U NA IOU Chromium 4.3 B NA S.S B NA 3.3 U Cobalt 8.S U NA 8.8 U NA 1.6 U Copper 17.9 U NA 18.3 U NA 6.S U Iron 19601 61.2 UJ 2240 J 63.3 UJ 26.2 U Lead 0.91 U NA 0.91 U NA I.SU Magnesium 19600 U NA 20000 U NA 36600 U Manganese 2740 2760 2830 2860 11.7 U Nickel 31.8 BJ NA 29.8 BJ NA 2.3 U Potassium 1320U NA 1370 U NA 743 U Silver 2.3 U NA 2.3 U NA 2.3 U Sodium 153000 ·a NA 156000 NA 54900 U Vanadium 10.S U NA 10.3 U NA 9.1 U Zinc 27.6 UJ NA 1301 NA 10,8 U Cyanide (amenable) IOU NA 10 U NA 10 Cyanide (total) 10 U NA 10 U NA 10.2 Total Dissolved Solids (mg/L) sso NA µg,'l.. Micrograms per liter. mgt'L Milligrams per liter. U Compound wu not detected above the IDL or was qualified u unddcctcd due to blank oontaminalion. B Compound concentration de1«1ed is betwcm the IDL and CRDL J Compound ~on de1«1ed is qualified u cotimated (1). NA C-OmlXM,llld was not analyzed. NC0202.0»'22SI chan/tabla/J" ABLE4-6J(l.SIY.J I '9:1 GERAGHTY & MILLER. INC 0 -------------------Page 5 of5 Table 4~. Phase I Groundwater Sample Quality Total and Dissolved T AL Metal, Hexavalent Chromium, and Total/Amenable Cyanide Data Summary, JFD Electronics/Channel Master, Inc., Oxford, Nonh Carolina. Sample Name: JFD-CMMWl5-00I JFD-CMMWl6-001 JFD-CMMWI 7-00 I JFD-CMMWl8-00 I JFD-CMMWl9-00I JFD-CMMW2 I-OOI Sample Date: 10/3/94 I0n/94 10/11/94 I0n/94 10/5/94 10/5/94 Sample Type: Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Monitor Well Media: Groundwater Growulwater Groundwater Groundwater Growulwater Groundwater Zone: Top of Rock Shallow Deep Bedrock Shallow Bedrock Intermediate Shallow Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: S445362•2 S445489•2 S445540A•6 S445489•3 S445438A•2 S445438A•i Concentration Unit: µg/L µg/L µg/L µg/L µg/L µg/L Aluminum 72.5 U 323 289 J 155 U 110 UJ 306J Antimony 11.5 U 8.9U 8.9U 8.9 U 8.9U 8.9 U Arsenic 1.4 B 1.4 U 1.6 U 1.4 U 1.4 U 1.4 U Barium 28.6 U 43.2 U 80.6 BJ 51.7 U 28.5 U 69.7 J Beryllium 0.14 U 0.14 U 0.52 U 0.14 U 1.1 u I.I u Calcium 29400 U 53400 U 47600 U 37600 U 34400 U 45800 Hexavalent chromium IOU 10 U IOU 10 U 10 U JOU Chromium 3.3 U 3.3 U 9.8 B 4.0 U 3.3 U 3.3 U Cobalt 1.6 U 1.6 U 1.6 U 1.6 U 9.9 U 5.7 U Copper 2.8 U 4.7U 2.8 U 4.7U 9.6U 10.9 U Iron 39.6 U 385 294 J 60.6 U 183 J 520 J Lead 1.3U 0.91 U 0.91 U 0.91 U 2.9 U 4.9 U Magnesium 20800 U 42200 22900 U 22300 U 20500 U 33200 U Manganese 16.6 131 38.3 64.8 843 802 Nickel 2.6 U 2.3 U 7.6U 2.3 U 2.3 U 6.6U Potassium 1650 U 827 U 1910 U 1900 U 1210 U 1340 U Silver 2.3 U 2.3 U 2.3 U 2.3 U 2.3 U 2.3 U Sodium 14100 U 27700 U 16100 U 18000 29500 20800U Vanadium 2.4 U 5.6U 5U 2.4 U 5.6 U 5.6 U Zinc 35.7 U 12.2 U 23 UJ 33.9 U 12.7 UJ 32.5 UJ Cyanide (amenable) 11 18 u JO JO u 10 U 10 U Cyanide (total) 30.1 56 u JO ' IOU 10 U IOU Total Dissolved Solids (mg/L) NA NA NA NA NA NA µg/L Mia-og.ram, per lita-. mg/L Milligrams per liter. u Compound wu not dctcctcd above the IDL or wu qualified u undetcctod due to blank oonwnination. B Compound conccntratioo detected is between the IDL and CRDI.. J Compound concentration detected ia qualified u estimated (J). NA Compound WU no( a.naly1.od. NC0202.030t'2281chanltables/r ABLE-4-o.XLSIY3!/9j GERAGHTY & MILLER. INC n \,J ------------------- Table 4-7. Phase I Quality Control Sample Total and Dissolved T AL Metal Data Summary Associated with Groundwater Data, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99E-OO I JFD-CMMW99E-002 JFD-CMMW99F-00 I JFD-CMMW99F-002 Sample Date: 10/11/94 10/13/94 10/11/94 10/13/94 Sample Type: Equipment Blank Equipment Blank Field Blank Field Blank Media: Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Lab ID: S445540A*4 S445588A*3 S445540A*3 S445588A*4 Concentration Unit: µg/L µg/L µg/L µg/L Aluminum 34.5 B 15.5 U 19.4 B 17.6 B Barium 11.6 B 11 B 11.8 B 11 B Calcium 24800 24200 25400 24900 Iron 32.3 B 19.6 B 11.3 B 11.9 B Iron, Dissolved 12.2 B NA 9.9 B NA Lead 15.2 0.91 U 0.91 U 0.91 U Magnesium 7950 7530 8080 7750 Manganese 1.4B 0.94 U 0.94 U 0.94 U Manganese, Dissolved 3.5 B NA 0.94 U NA Potassium 2230B 2150 B 2230B 2260B Sodium 13000 12400 13300 12700 Zinc 10.7 B 20.8 7.7 B 34 Total Dissolved Solids (mg/L) NA NA SU NA µg/L Micrograms per liter. mg/L Milligrams per liter. U Compound was not detected above the IDL. B Compound concentration detected is between the IDL and CRDL. NA Compound was not analyzed. NC0202.0J0\228 I er-\table+ 7.xls\Y.I 1/95 GERAGHTY & MILLER. INC. 0 ------------------- Page I of3 Table 4-8. Geoprobe® Groundwater Sample Quality Site-Specific voe Data SUlllill31Y, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: GP-1-18 11 GP-1-24 Sample Date: 12/15/94 12/15/94 Sample Type: Geoprobe Geoprobe Media: Groundwater Groundwater Laboratory: ES! Mobile Lab ES! Mobile Lab Concentration Units: µg/L µg/L Chlorobenzene IOU IOU 1,2-Dichlorobenzene (total) 10 U IOU Tetrachloroethene IOU IOU Trichloroethene IOU 10 U Micrograms per liter. µg/L u Compound was not detected above the reporting limit. GP-2-16 GP-2-25.5 12/15/94 12/16/94 Geoprobe Geoprobe Groundwater Groundwater ES! Mobile Lab ES! Mobile Lab µg/L µg/L IOU IOU 32 30 51 13 3 J 6J J II Estimated concentration (compound was detected between the MDL and reporting limit). Sample GP-1-18 represents location GP-I and sample depth of 18 feet below land surface. NC0101.0lOl228 I chan-'table'-8.Jtb/~ 119'.5 GP-3-21 GP-4-15 12/16/94 12/15/94 Geoprobe Geoprobe Groundwater Groundwater ES! Mobile Lab ES! Mobile Lab µg/L µg/L IOU 10 U IOUI IOU 10 U IOU 10 U IOU GERAGHTY & MILLER. INC. 0 ------------------- Page 2 of3 Table 4-8. Geoprobe® Groundwater Sample Quality Site-Specific voe Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: GP-4-27 GP-S-16 Sample Date: 12/16/94 12/15/94 Sample Type: Geoprobe Geoprobe Media: Groundwater Groundwater Laboratory: ESI Mobile Lab ESI Mobile Lab Concentration Units: µg/L µg/L Chlorobenzene IOU IOU 1,2-Dichlorobenzene (total) 10 U 10 U Tetrachloroethene IOU 10 U Trichloroethene 10 U JJ Micrograms per liter. µg/L u Compound was not detected above the reporting limit. GP-S-16 (Dup) GP-S-27 12/1S/94 12/1S/94 Equip. Blank Equip. Blank Aqueous Aqueous ESI Mobile Lab ESI Mobile Lab µg/L µg/L IOU 10 U 10 U 10 U IOU IOU IOU 6J J I/ Estimated concentration (compound was detected between the MDL and reporting limit). Sample GP-1-18 represents location GP-I and sample depth of 18 feet below land surface. NC0202 0»"228ktwlltableA-8.xl:s/Y3Jl95 GP~l4 GP~-14(Dup) 12/20/941 12/20/94 Geoprobe Geoprobe Groundwater Groundwater ESI Mobile Lab ESI Mobile Lab µg/L µg/L 10 U 10 U 10 U 10 U 10 U IOU IOU IOU GERAGHTY & MILLER. INC. ft \,J ------------------- Page 3 of3 Table 4-8. Geoprobe® Groundwater Sample Quality Site-Specific VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: GP-6-22.5 GP-7-20 Sample Date: 12/20/94 12/16/94 Sample Type: Geoprobe Geoprobe Media: Groundwater Groundwater Laboratory: ES! Mobile Lab ES! Mobile Lab Concentration Units: µg/L µg/L Chlorobenzene 10 U IOU 1,2-Dichlorobenzene (total) 10 U IOU Tetrachloroethene 10 U 115 Trichloroethene 10 U SJ Micrograms per liter. µg/L u Compound was not detected above the reporting limit. GP-9-10 GP-9-24.5 12/20/94 12/20/94 Geoprobe Geoprobe Groundwater Groundwater ESI Mobile Lab ES! Mobile Lab µg/L µg/L IOU 25 10 U 21 10 U 10 U 10 U 10 U J II Estimated concentration (compound was detected between the MDL and reporting limit). Sample GP-1-18 represents location GP-I and sample depth of 18 feet below land surface. NCO?Ol.030122Bichan/table+l.xl.t/Y.Jl/9' GP-10-18.5 GP-11-22 12/19/94 12/19/94 Geoprobe Geoprobe Groundwater Groundwater ESI Mobile Lab ESI Mobile Lab µg/L µg/L 10 U 10 U IOU 10 U IOU 10 U IOU 10 U GERAGHTY & MILLER. INC. 0 - - ----- - - - - -- Table4-9. ~ Oroundwal« Split Sample QuaHty VOC Dou Canpoti,oa. JFD Eloctroruoo/ammcl Maota-, !no., Oxford, North Carolina. Sample Name: Sample Delo: S-l•Typc: Media: Llbonlory: LabID: Conoentntion Unita: -Carbon disulfide Chlorobcnzonc Chloroform 1,1-Dichlorocthanc 1,2-Dichlorocthanc 1,1-DichJorocthate citllnnl--1,2-Dichlorocthenc 1,2-Dichlon>propanc Ethylbcnzcnc T ctrachloroethcnc Toluene I, I, 1-TrichJorocthane TrichlOf'OCthcne Xylcncs Micrograma per liter. Compound WU not analyzed OP·2-2S.S 11 12/1 S/94 Oooprobc Clroundwat« Savomwt S446856•1 •8'L to u 10 31 to u IOU IOU IOU 30 11 IOU 20 0.71 IOU 14 3 1 OP·2-2'.S 12/IS/94 Oooprobc Clroundw,.., ES! Mobile Lab •8'L NA NA IOU NA NA NA NA 30 NA NA 13 IOU NA 61 NA OP-6--22.5 OP-6-22.5 OP-7-20 12'20194 12'20194 1Vl6/94 Oooprobc Oooprobc Oooprobc Oroundwal« Oroundwal« Oroundwal« Savannah ES! Mobile Lab Savomwt 5446912•1 5446856•2 ,8'L •8'L ,8'L IOU NA z IOU NA 10 U IOU IOU IOU IOU NA 91 IOU NA 31 10 U NA 21 IOU NA 22 10 U IOU 24 IOU NA IOU IOU NA 21 IOU to u z 21 10 U 3 1 10 U NA 14 10 U IOU 37 91 NA 83 •8'L NA u 1 Compound wu not dctcctcd above the: reporting limit/CRQL or wa qualified a undctoctcd due to blank oontamination. Ea:timatcd oonccntntion (oompoond wu dctoctod bctwocn the MDL and reporting liout/CRQL). D z " Sample oonoc:ntration wu quantinatcd using a IOOOOdary dilutioa. Compound oonocntration ll not ua.ablc. Sample rau.lt i1 a oombination oftwo analytioaJ rum. Sample GP-2-2S.S rcprcacnll location GP-2 md umplc depth of2S.S feet below land mrfaoc. OP-7-20 (DL) 12/16194 Oooprobc ~ -S446U6•4 •8'L 1700D z z z z z z z z z 410D z z z z --- -- - OP-7-20 OP-10-18.5 OP-10-18.S 12/16194 12/1919-4 12/19194 Oooprobc Oooprobc Oooprobc ~ ~ ~ ES! Mobile Lab Savomwt ES! Mobile Lab S4469t2•2 •8'L ,8'L •8'L NA 10 U NA NA to u NA IOU IOU IOU NA IOU NA NA IOU NA NA IOU NA NA 10 U NA IOU IOU IOU NA 10 U NA NA IOU NA 11S IOU IOU IOU IOU IOU NA IOU NA 81 IOU IOU NA 61 NA GERAGHTY & MILLER. INC. U ------------------- Page I of2 Table 4-10. Geoprobe® Quality Control Sample voe Data Summary, JFD Electronics/Channel Master, Inc., Oxford, Nonh Carolina. Sample Name: FB-1 FB-2 FB-3 FB-4 RB-I Sample Date: 12/15/94 12/16/94 12/19/94 12/19/94 12/15/94 Sample Type: Field Blank Field Blank Field Blank Field Blank Equip. Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: ES! Mobile Lab ES! Mobile Lab ES! Mobile Lab ES! Mobile Lab ES! Mobile Lab Lab ID: Concentration Units: µg/L µg/L µg/L µg/L µg/L Acetone NA NA NA NA NA Carbon disulfide NA NA NA NA NA Chlorobenzene 10 U IOU 10 U 10 U IOU 1,2-Dichloroethene (total) 10 U IOU 10 U 10 U IOU Tetrachloroethene IOU IOU IOU 10 U IOU I, I, I -Trichloroethane NA NA NA NA NA I, 1,2-Trichloroethane NA NA NA NA NA Trichloroethene IOU 10 U IOU IOU IOU µg/L Micrograms per liter. NA Compound was not analyzed. U Compound was not detected above the reporting lirnit/CRQL. J Estimated concentration (compound was detected between the MDL and CRQL). NC0102.0»'2281 charvtab4-I O.xb/Y3i/9j GERAGHTY 8 MILLE!{. INC ft \.J ------------------- Page 2 of2 Table 4-10. Geoprobe® Quality Control Sample VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: RB-2 RB-3 RB-4 TB-I TB-2 Sample Date: 12/16/94 12/19/94 12/19/94 12/15/94 12/19/94 Sample Type: Equip. Blank Equip. Blank Equip. Blank Equip. Blank Equip. Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: ESI Mobile Lab ES! Mobile Lab ES! Mobile Lab Savannah Savannah Lab ID: 5446856*3 5446912*3 Concentration Units: µg/L µg/L µg/L µg/L µg/L Acetone NA NA NA IOU 150 Carbon disulfide NA NA NA SJ 7J Chlorobenzene 10 U IOU 10 U IOU IOU 1,2-Dichloroethene (total) IOU 10 U IOU IOU 10 U Tetrachloroethene IOU 10 U 10 U IOU IOU I ,I, I-Trichloroethane IOU 10 U 10 U IOU 10 U I, 1,2-Trichloroethane NA NA NA 0.9 J IOU Trichloroethene NA NA NA 10 U 10 U µg/L Micrograms per liter. NA Compound was not analyzed. U Compound was not detected above the reporting limit/CRQL. J Estimated concentration (compound was detected between the MDL and CRQL). NC0202 030(2281 dianhab4-I OJds/Yl 1195 GERAGHTY & MILLER. INC. -------------------Page I of2 Table 4-11. Phase II Groundwater Sample Quality TCL VOC Data Surnmaty, JFD Electronics/Channel Master, Inc., Oxford, North Carolina . .. Sample Name: JFD-CMMW07-002 JFD-CMMW17-002 Sample Date: 3/10/95 3/14/95 Sample Type: Monitor Well Monitor Well Media: Groundwater GroWldwater Zone: Shallow Bedrock Deep Bedrock Laboratory: Savannah Savannah Lab ID: S551346•2 S551414•5 Concentration Unit: µg/L µg/L Acetone 81 IOU Benzene IOU IOU Carbon disulfide 10 U IOU cis/trans-1,2-Dichloroethane 11 10 U l, 1-Dichloroethene IOU IOU Tetrachloroethene 94 11 I, I, I-Trichloroethane 10 U IOU Trichloroethene 180 10 Toluene 10 U IOU Micrograms per liter. µg/L u Compound was not detected above the CRQL. JFD-CMMW 18-002 3/14/95 Monitor Well Groundwater Shallow Bedrock Savannah S55l414•7 µg/L 10 uJ" IOU IOU 10 U 10 U IOU 10 U 10 U IOU J B Estimated concentration (compound was detected between the MDL and CRQL). Compound was detected in the associated blank sample. II Sample was analyzed using USEPA SW-846 Method 8240. Duplicate sample criteria were not met. NC0202.020\22ll lchan\tab4-I l .xls001/95 JFD-CMMW18R-002 JFD-CMMWl 9-002 3/14/95 3/10/95 Monitor Well Monitor Well Groundwater Groundwater Shallow Bedrock Intermediate Savannah Savannah S5514t4•8 S551346•1 µg/L µg/L 55f' IOU IOU 10 U 10 U 10 U 10 U 10 U IOU IOU IOU 12 IOU 10 U IOU 10 U 10 U 10 U GERAGHTY C:<i' MILLER. INC V -------------------Page 2 of2 Table 4-11. Phase II Groundwater Sample Quality TCL VOC Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-{:MMW20--00 I 11 JFD-{:MMW22--00 I Sample Date: 3/17/95 3/17/95 Sample Type: Monitor Well Monitor Well Media: Groundwater Groundwater Zone: Shallow Shallow Laboratory: Savannah Savannah Lab ID: S551512D*I S551512*2 Concentration Unit: µg/L µg/L Acetone 25 U IOU Benzene SU IOU Carbon disulfide SU IOU cis/trans-1,2-Dichloroethane 14 IOU I, 1-Dichloroethene 11 10 U Tetrachloroethene 260 41 l, l, 1-Trichloroethene 6.9 10 U Trichloroethene 31 IOU Toluene SU 10 U Micrograms per liter. µg/L u Compound was not detected above the CRQL. JFD-{:MMW23-00 I 3/16/95 Monitor Well Groundwater Intermediate Savannah S551493*3 µg/L IOU IOU 10 U 31 IOU 94 IOU 24 21 1 B Estimated concentration (compound was detected between the MDL and CRQL). Compound was detected in the associated blank sample. II Sample was analyzed using USEPA SW-846 Method 8240. Duplicate sample criteria were not met. NC0l0l.020\2281 dlan\b.b4. I I .xla\5131f9j JFD-{:MMW24--00 I JFD-{:MMW25--00 I JFD-{:MMW26--00 I 3/16/95 3/15/95 3/15/95 Monitor Well Monitor Well Monitor Well Groundwater Groundwater Groundwater Intermediate Intermediate Intermediate Savannah Savannah Savannah S551493*2 S551458*2 S551458*3 µg/L µg/L µg/L IOU IOU IOU IOU IOU IOU 21 IOU IOU 10 U IOU 13 IOU IOU IOU IOU IOU 51 10 U 1IOU IOU IOU 10 U 91 IOU IOU IOU GERAGHTY 8 MILLER. INC ------------------- Page I of2 Table 4-12. Phase II Quality Control Sample TCL VOC Data Summary Associated with Groundwater Sample Data, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99E-001 JFD-CMMW99E--002 JFD-CMMW99E--004 JFD-CMMW99F--OO I JFD-CMMW99T--OO JFD-CMMW99T--002 Sample Date: 3nt95 3/13/95 3/13/95 3/13/95 3nt95 3/10/95 Sample Type: Equipment Blank Equipment Blank Equipment Blank Field Blank Trip Blank Trip Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Savannah Savannah Lab ID: S551245•J S5514J4•2 S5514J4•4 S5514J4•3 S5514J4•3 S551346•3 Concentration Units: µg/L µg/L µg/L µg/L µg/L µg/L Acetone 10 U IOU IOU 10 U 10 U 10 U Camon disulfide 10 U IOU SJ 10 U JOU 10 U Methylene chloride 10 U 51 IOU 10 U 10 U IOU Xylencs 2 J IOU IOU 10 U JOU 10 U µg/L Micrograms per liter. U Compound was not detected above the reporting limit. J Estimated concentration (compound was detected between the MDL and CRQL). GERAGHTY & MILLER. INC NC0202.0J412281 ~han/tab4-I 2.xW.Y31195 0 ------------------- Page 2 of2 Table 4-12. Phase II Quality Control Sample TCL VOC Data Swnma,y Associated with Groundwater Sample Data, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW99T -003 JFD-CMMW99T-004 JFD-CMMW99T-005 JFD-CMMW99T -006 JFD-CMMW99T-007 Sample Date: 3/13/95 3/14/95 3/15/95 3/16/95 3/17/95 Sample Type: Trip Blank Trip Blank Trip Blank Trip Blank Trip Blank Media: Aqueous Aqueous Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S551414*1 S551414*6 Concentration Units: µg/L µg/L µg/L µg/L µg/L Acetone 10 U IOU 10 U 61 10 U Carbon disulfide 10 U IOU 10 U IOU 10 U Methylene chloride 10 U IOU IOU 28 10 U Xylenes 10 U IOU IOU 10 U 10 U µg/L Micrograms per liter. U Compound was not detected above the reporting limit. J Estimated concentration (compound was detected between the MDL and CRQL). NC0202.0»'228lchanl'b.b4-lhW.YJl/9j GERAGHTY & MILLER. INC 0 -- ----- - - - --- - Table 4-13. Phase D Groundwaw Sample Quality Total and Diaolvcd T AL Metal Da!a Summary, lFD Elcctronic.-cbanncl M...,,., Inc., Oxfool, North Carolina. Location: Unimax Corp. Unimax Corp. Unimax Corp. Unimax Corp. Unimax Corp. Sample Name: JFD.CMMW020-001 11 JFD.CMMW22-00 I JFD.CMMW2M01° JFD.CMMW23--00 I JFD.CMMW24--00 I Sample Dale: 3/17/95 3/17/95 3/17195 3/16/95 3/16/95 Sample Type: Monitor Well Monitor Wc,11 Monitor" Well Monitor Well Monitor Well Media: Oroundwata' Oroondwaw Oroundwak:lr Groundwater Groundwater Zone: Shallow Shallow Shallow lntcnncdiatc, lntcnnodiate Laboratory: Savannah Savannah Savannah Savannah Savannah Lab ID: S551512D•I S5ll512B•2 S551512C•l SS51493•2 S551493A•t Concentration Unit µg/L µg/L µg/L (Dissolved) µg/L µg/L Aluminum 340 7580 42.4U 99.5UJ 1580) Ancnic IOU I.IU 1.1B I.JU I.SU Bariwn 37 42.8B 11.4U 10.8B 27.SB Beryllium s.ou 2.4U l.7U 1.5U l.9U Calcium 19000 21600 1noo 37800 23900 Chromium IOU 34.1 3.1 U 3.IU 3.IU Cobalt IOU 34.4B 2.8B 1.4B 5.8B Copper 2SU 17.8U 3.2U 3.2U 4.4U Iron 2801 14500 38.IU 33001 138UI Lead s.ou 2.8B 0.52 U 0.S2U 0.97U Magnesium 8800 13900 7n0 19900 15400 Manganese ISO 951 544 58.2 644 Mercury 0.20U 0.10B 0.11B 0.20B 0.20B Nickel 40U 27.4 3.6U 3.6U 3.6U Potassium IOOOU 1320B 675B 1510B 896B Silver IOU 1.7B 1.7 U l.7U l.7U Sodium 14000 8430 8040 14300 15200 Vanadium IOU 25.SB 2.8U 2.8U IO.SB Zinc 20U SS.2U 9.9U 37.JU IS.SU Micrograms per liter. µg/L u B Compound was not detected above the IDL {PQL for JFD.CMMW~ I) or wu qualified as undetected due to blank contamination. Compound concentration detected is betwoen the IDL and CRDL. I " n Compound concentration is qualified as estimated. Sample was analyzed using USEPA SW-846 Methods. Dissolved metal conccntratiom. Sample JFD-CMMW22~1 wu field filtered. l'fC0102.0JIUlll-•IJmUIJl1'' Unimax Corp. JFD.CMMW25--00 I 3115195 Monitor Well Oroundwatcr lntamcdiato Savannah S551458A•J µg/L 2040) 1.IU 101B 2.2U 20900 14.IJ 3.SB 8.IU 42801 0.52U 10300 163 0.20U 4.7B 1210B l.7U 12900 10.38 39.9U - --- Unimax Corp. Unimax Corp. JFD..CMMW2SR--001 JFD.CMMW26-00 I 3/1 S/95 3/15195 Monitor Well Monitor Well Groundwater Oroundwaa lntcrmcdiato Inicnnc,dialCI Savannah Savannah SSSl458A•4 S5l1458A•5 µg/L µg/L 17901 52.JUI I.IU 1.6U 103B 73.0B 1.9U 1.2U 21400 32600 IO.SJ 3.IU 2.8B 1.2U 8.5U 5.4U 39201 72.6UI 1.2U 0.86U 10600 17300 166 43.4 0.20U 0.20U S.4B 3.6U 1210B 1450B l.7U l.7U 13400 19200 10.38 4.78 47.2U 7.9U GERAGHTY & MILLER. INC. - 0 ------------------- Table 4-14. Phase II Quality Control Sample Total TAL Metal and Hexavalent Chromium Data Summary Associated with Groundwater Sample Data, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: CMMW99E--005 JFD..CMMW99F--002 JFD..CMMW99E--OO 1 Sample Date: 3/15/95 3/15/95 3n19s Sample Type: Equipment Blank Field Blank Equipment Blank Media: Aqueous Aqueous Aqueous Laboratory: Savannah Savannah Savannah Lab ID: S551458A•I S551458A•2 SSSl24SA•I Concentration Unit: µg/L µg/L µg/L Aluminum 25.9B 37.8B NA Arsenic 1.4B I.IU NA Barium 0.47U 1.7B NA Beryllium 0.60U 312B NA Calcium 273B 505B NA Copper 4.9B 4.5B NA Iron 40.9B 39.6B NA Magnesium 13.7B 172B NA Manganese 0.92B 3.3B NA Sodium 374B 530B NA Zinc 13.0B 7.0B NA Hexavalent chromium NA NA 2.IB µg/L Micrograms per liter. U Compound was not detected above the IDL. B Compound concentration detected is between the IDL and CRDL. NA Compound was not analyzed. NC0l02.0l0\2281chtn~!,4.xlaOOJl95 GERAGHTY 8 MILLER. INC I I I I I I I I I I I I I I I I I I I Page 1 of2 Table 4-15. Bio-Geochemical Parameter Data Summary, JFD Electronics/Channel Master, Inc., Oxford, North Carolina. Sample Name: JFD-CMMW09-002 JFD-CMMW13-002 JFD-CMMW22-001 Sample Date: 3/23/95 3/24/95 3/23/95 Sample Type: Monitor Well Monitor Well Monitor Well Media: Groundwater Groundwater Groundwater Zone: Shallow Shallow Shallow Laboratory: Savannah Savannah Savannah Lab!D: S551647•2 S551679•1 S551647•1 Concentration Unit: mg/L mg/L mg/L Total Dissolved Solids (160.1) 300 740 170 Biochemical Oxygen Demand ( 405. I) 2.0U 2.0U 2.0U Ammonium-N (FL-DER) 0.020 U 0.020 U 0.020U Nitrate-N (353 0.36 0.050 U 0.57 Nitrite-N (353 0.050 U 0.050 U 0.050 U Orthophosphate-P (365.1) 0.076 0.33 0.1 Chloride (325.2) 19 22 4.2 Alkalinity (to pH 4.5) as CaC0,(310.1) 160 160 100 Total Organic Carbon (415.1) 1.9 12 I.OU Chemical Oxyg~n Demand ( 4 IO .1) 20U 21 20U Sulfate (375.4) 29 99 6.2 Sulfide (376.2) 0.40 U 0.40U 0.40U Metals (6010) Iron 2.3 4.5 6.3 Iron (dissolved) 0.050 U 0.050 U 0.050 U Manganese 0.17 2.8 0.52 Manganese ( dissolved) 0.096 2.9 0.37 Volatile Oreanic Com(!Qunds (8240) (111!/L) cis-1,2-Dichloroethane NA 260 NA Tetrachloroethene NA 1200 NA Trichloroethane NA 4900 NA µg/L Micrograms per liter. mg/L Milligrams per liter. u Compound was not detected above the reporting limit. NA Compound was not analyzed. NC020l0».2281clwl~l5.xb\Yll/95 GERAGHTY & MILLER. INC I I I I I I I I I I I I I I I I I I I Page 2 of2 Table 4-15. Bio-Geochemical Parameter Data Swnrnary, JFD Electronics/Channel Master, Inc., Oxford, Nonh Carolina. Sample Name: JFD-CMMW09-002 Sample Date: Sample Type: Media: Zone: Laboratory: LabID: Concentration Unit: Camon dioxide Oxygen Nitrogen Methane Camon monoxide Micrograms per liter. Milligrams per liter. 3/23/95 Monitor Well Groundwater Shallow Microseeps PS 68 mg/I.. 58.9 4 14.9 0.2 U 0.3 U µg/L mg/I.. u NA Compound was not detected above the reporting limit Compound was not analyzed. NC0'202.030'1228 I dwi\tab4-15Jds00 l/9S JFD-CMMW13-002 3/24/95 Monitor Well Groundwater Shallow Microseeps _ PS 69 mg/I.. 132.3 2.1 10.6 0.2 U 0.3 U GERAGHTY & MILLER. INC. JFD-CMMW22-001 3/23/95 Monitor Well Groundwater Shallow Microseeps PS 67 mg/I.. 21.8 3.8 13.3 0.2 U 0.3 U 0 I I I I I I I I I I I I I I I I I I I _,.._x,cx.., LABORATORY REPORTS OF GROUND\VA TER SAMPLES FROM MONITORING WELL CMMW-10 I I I I I I I I I I I I I I I I I I I .5 L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savar,nah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S4-4:670 Revised: 10 J;,_~ 55 Received: 19 OC7 ~4 Mr. Leonard More~z Geraghty & Mille=, Inc., Enviro~~e~cal Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Projec~: NC0202. 02 o /Ox:ord/Channel Master /SDG#G:-soa Sampled By: Clie~t REPORT 0: RESULTS LOG NO SAMPLE DESC!E?TION , LIQUID s;_,!PLES ------------------------------------------------------------- 45670-1 JFD-CMMWl0-001 PARAMETER 45670-1 Paqe 1 DATE/ TIME SAMPLED S~Ge 10-18-94/1210 G1·S08 ------------------------------------------------------------------------------- TAL Metals. (CLP-3/90) Aluminum (CLP 3/90), ug/1 Antimony (CLP 3/90), ug/1 Barium (CLP 3/90), ug/1 Beryllium (CLP 3/90), ug/1 Cadmium (CLP 3/90), ug/1 Calcium (CLP 3/90), ug/1 Chromium (CLP 3/90), ug/1 Cobalt (CLP 3/90), ug/1 Copper (CLP 3/90), ug/1 Iron (CLP 3/90), ug/1 Magnesium (CLP 3/90), ug/1 Manganese (CLP 3/90), ug/1 Nickel (CLP 3/90), ug/1 Potassium (CLP 3/90), ug/1 Silver (CLP 3/90), ug/1 Sodium (CLP 3/90), ug/1 Vanadium (CLP 3/90), ug/1 Zinc (CLP 3/90), ug/1 Interference Check Sample Dilution Check Sample Date Analyzed Mercury (CLP 3/90) Mercury (CLP 3/90), ug/1 Date Analyzed 4340N* 8.90 154B 1.7B 2 .6U 11100 20.7 5.7B 14 .lB lllOON* 8740 324 25. 3B 701B 2 .3U 42200 33.SS 32.0 PASSED PASSED 10.31.94 o. o.;u 11.02.94 ------------------------------------------------------------------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I . s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG ~O: S4-~Soi0 Revised: 10 J;s ~5 Received: 19 cc, 94 Mr. Leonard Moretz Geraghty & Miller, Inc., Envi~o~rae~tal Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project: NC0202. 020/Oxfo:-d/Channel Mas~e::-/SDG=G:-s.n Sampled By: c:ce~t REPO~T OF RESULTS Pa;e 2 DATE/ LOG NO SAMPLE DESCRI?TION, LIQUID s.;.~?LES TIME SAM?:.ED ------------------------------------------------------------------------------------ 45670-1 JFD-CMM"~l0-001 PARAMETER Lead (CLP 3/90) Lead (CLP 3/90), ug/1 IR Post Digestion Spike Date Analyzed Selenium (CLP 3/90) Selenium (CLP 3/90), ug/1 t R Post Digestion Spike Date Analyzed Arsenic (CLP 3/90) Arsenic (CLP 3/90), ug/1 IR Post Digestion Spike Date Analyzed Thallium (CLP 3/90) Thallium (CLP 3/90), ug/1 IR Post Digestion Spike Date Analyzed 45670-1 5.9 104 I 10.28.94 13. 2U"'"N 83 \ 10.28.94 l.4U 108 t 10.28.94 1.3U 96 t 10.28.94 10-18-94/1210 G:-s.O0 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I - I I I I I I I I I I I I I . s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannae, GA 31404 • (9;2) 354-7858 • Fax (912) 352-0165 LOG NO: S4-,:,;o Revised: 10 J;.s 55 Received: 19 CC7 54 Mr. Leonard Moretz Geraghty & Miller, Inc., Enviror-~e~tal Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Projec~: NC0202.020/0xford/Channel Master/SDG#GX:.08 Sampled By: C~c~~t REPORT OF RESULTS Paqe 3 DATE/ LOG NO SAMPLE DESCRIPTION, LIQUID s;.MPLES TIME SAMPLED ------------------------------------------------------------- 45670-l JFD-CMMWl0-001 10-18-94/1210 ------------------------------------------------------------------------------------ PARAMETER --------------------------------------- TAL Metals (Dissolved) (CLP 3/90) Aluminum (Dissolved) (CLP 3/90), ug/1 Antimony (Dissolved) (CLP 3/90), ug/1 Barium (Dissolved) (CLP 3/90), ug/1 Beryllium (Dissolved) (CLP 3/90), ug/1 Cadmium (Dissolved) (CLP 3/90), ug/1 Calcium (Dissolved) (CLP 3/90), ug/1 Chromium (Dissolved) (CLP 3/90), ug/1 Cobalt (Dissolved) (CLP 3/90), ug/1 Copper (Dissolved) (CLP 3/90), ug/1 Iron (Dissolved) (CLP 3/90), ug/1 Magnesium (Dissolved) (CLP 3/90), ug/1 Manganese (Dissolved) (CLP 3/90), ug/1 Nickel (Dissolved) (CLP 3/90), ug/1 Potassium (Dissolved) (CLP 3/90), ug/1 Silver (Dissolved) (CLP 3/90), ug/1 Sodium (Dissolved) (CLP 3/90), ug/1 Vanadium (Dissolved) (CLP 3/90), ug/1 Zinc (Dissolved) (CLP 3/90), ug/1 Interference Check Sample Dilution Check Sample Date Analyzed Arsenic (CLP 3/90) Arsenic (Dissolved) (CLP 3/90), ug/1 \ R Post Digestion Spike Date Analyzed 45670-l 25.0B 8.9U lllB 1.6B 2.6U 9770 3. 3U 1.6U 4.9B 87.6B 6620 194 7.9B 461B 2 .3U 41000 7. SB 4.5B PASSED PASSED 10.31.94 2 .4B 104 \ 10.28.94 1 1 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I -s L SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRccne Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Ge=-aghty & Miller, Inc., Environme:1tal Services. 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG ::o: S4-45670 Revised: 10 J;._'i 95 Recei·:ed: 19 cc-;-S4 Project: NC02 02. 020/0x:c:-c/Channel Mas:er /SDG~S'.·S.·J8 Samp:ed By: c~:e~t REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID SA.~PLES ------------------------------------------------------------- 45670-1 JFD-CMMWl0-001 ------------------------------------------------------------- PARAMETER --------------------------------------- Lead (CLP 3/90) Lead (Dissolved) (CLP 3/90), ug/1 t R Post Digestion Spike Date Analyzed Mercury (CLP 3/90) Mercury (Dissolved) (CLP 3/90), ug/1 Date Analyzed Selenium (CLP 3/90) Selenium (Dissolved) (CLP 3/90), ug/1 t R Post Digestion Spike Date Analyzed Thallium (CLP 3/90) Thallium (Dissolved) (CLP 3/90), ug/1 t R Post Digestion Spike Date Analyzed Cyanide (CLP 3/90) Cyanide (CLP 3/90), ug/1 Date Analyzed Cyanide (Dissolved) (CLP 3/90) Cyanide (Dissolved) (CLP 3/90), ug/1 Date Analyzed Methcds: CLP 3/90 45670-1 2.6B 104 t 10.28.94 0 .04U 11.02.94 13.2U 101 t 10.28.94 l.3U 94 t 10.28.94 lOU 10.25.94 lOU 10.26.94 Final Page Of Report DATE/ TIME SA.'-1?:.ED 10-18-94/:210 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA l.alxnalo,y lid< O,dm No.I. 3_7-3."3 CHAIN-OF-CUSTODY RECORD Pnyo .. _L_ _____ of ____ / __ Projecl Number .}l_,~O_'2,_,;> __ l_. __ O_}_ b_ l'roj,x:I Locnlio11 (J,x. r,J(. J 1 ;J (-_ Laboralory ~_.__,,, .• , ,, r,_ h, ___ _b!_,6 __ Samplcr(s)/Affilialion .:er,,. ;::, -</;. • .~) k.<__,-,,; ··-(<" • ,..._ \ Date/Time &\MPLE IDENTITY Code Sampled Lab ID i......------ Sample Code: L = Liquid; S = Solid; A = Air I Relinquished by: --C' .n--'DJ,,., Organization: Received by: Organization: Relinquished b~-: . ,~. Organization: Received by: ~ .... JY-="\..-~~--q.,__,,s.Jb"'-'7~r.~=>-Organizalion: L-----""" Total No. ol Bollles/ Containers DatP. /{) I t ~ 15 't-Time_....;1:...1'-"'tP_,Q'--. __ __ Date 1 1 Time ______ _ Dale_/__./ ___ Time· _______ _ Daill Iv, L't, 2'1Time--9'. : 3 Y Seal lnlact? Yes No NIA Seal Intact? @ No NIA Special Instructions/Remarks: .. _ . -·--·-··--·-------.. ____ _ ___________________________________ --·-· _ . _ ........ ______ _ _________ _,,0!.L< ; Z,'f./...c hoiJ.-"5 +,-,,,.,.c +'<ic Cr.,."' _f-oC..::::. k~or~_Jt.....~------------ ____ (1J cf) 9--J ~It. t "L __ ~ Common Carrier fl) q_ ~cc-----D Lab Courier D Other SJ'fcrt ····-··-··-------------·--·----- Delivery Method: D In Person SN:Cl'Y -- -------------- - I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES . & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Envircn=:ental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: S4·45508 Received: 14 OC7 ~; Proje:::: NC0202.020/0x:-"rd/Channel Master/S!::G~GM?.C7 s~~pled By: Clie~: REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID S.0..'1PLES 45588-1 JFD·CMMW05·001 45588·2 JFD-CMMWl0-001 PARAMETER 45588·1 TCL Semivolatiles (CLP-3/90) Phenol, ug/1 bis(2-Chloroethyl)ether, ug/1 2-Chlorophenol, ug/1 1,3-Dichlorobenzene, ug/1 1,4-Dichlorobenzene, ug/1 1,2-Dichlorobenzene, ug/1 2-Methylphenol (o-cresol), ug/1 2,2'-0xybis(l·Chloropropane), ug/1 3-Methylphenol/4-Methylphenol(m&p-cresol), ug/1 N-Nitroso-di-n-propylamine, ug/1 Hexachloroethane, ug/1 Nitrobenzene, ug/1 Isophorone, ug/1 2-Nitrophenol, ug/1 2,4-Dimethylphenol, ug/1 bis(2-Chloroethoxy)methane, ug/1 2,4-Dichlorophenol, ug/1 1,2,4-Trichlorobenzene, ug/1 Naphthalene, ug/1 4·Chloroaniline, ug/1 Hexachlorobutadiene, ug/1 4-Chloro-3-methylphenol, ug/1 lOU lOU lOU lOU lOU lOU lOU 100 lOU lOU 100 lOU lOU lOU lOU lOU lOU 100 lOU lOU lOU lOU ---------- Page 1 DATE/ TIME SAMPLED SDG= 10-13-94/1305 10-13-94/1530 ·45588-2 lOU lOU 100 100 0.SJ lOU lOU lOU lOU 100 100 100 100 lOU lOU lOU lOU lOU 0.6J lOU lOU 100 G~C7 G~.07 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Envircnmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Received: 14 OC~ S~ Project: NC0202.020/0x~o~C/Channel Maste~/S~G~G~.07 Sampled By: Clce~c REPO"T OF RESULTS LOG NO SAMPLE DESCRIPTION , LIQUID SA:-!PLES 45588-1 JFD-Cl1MW05-001 45588-2 JFD-Cl1MW10-001 Paqe 2 DATE/ TIME SAMPLED s=G= 10-13-94/1305 10-13-94/1530 c;:~:7 G~.07 PARAMETER 45585-1 45588-2 2-Methylnaphthalene, ug/1 Hexachlorocyclopentadiene, ug/1 2,4,6-Trichlorophenol, ug/1 2,4,5-Trichlorophenol, ug/1 2-Chloronaphthalene, ug/1 2-Nitroaniline, ug/1 Dimethylphthalate, ug/1 Acenaphthylene, ug/1 2,6-Dinitrotoluene, ug/1 3-Nitroaniline, ug/1 Acenaphthene, ug/1 2,4-Dinitrophenol, ug/1 4-Nitrophenol, ug/1 Dibenzofuran, ug/1 2,4-Dinitrotoluene, ug/1 Diethylphthalate, ug/1 4-Chlorophenyl-phenyl ether, ug/1 Fluorene, ug/1 4-Nitroaniline, ug/1 4,6-Dinitro-2-methylphenol, ug/1 N-Nitrosodiphenylamine/Diphenylamine, ug/1 4-Bromophenyl-phenyl-ether, ug/1 Hexachlorobenzene, ug/1 ---------- l0U l0U 100 25U 100 250 l0U 100 100 250 100 250 250 l0U 100 100 100 100 250 250 100 100 100 ---------- -------------------- 100 l0U 100 250 100 250 100 l0U l0U 250 100 250 250 100 100 100 100 100 25U 25U 100 100 100 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 La~oche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352·0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Envircr...~ental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Received: 1, .CC? s~ Project:: NC0202. 02 a/Oxford/Channel Mas::er /SJG~G:-!?.G7 Sampled By: Clie~: REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQUID S.Cu'!PLES 45588-l JFD-Cl1MW05-00l 45588-2 JFD-Cl1MW10 -001 DATE/ TIME SA..'!?LED s::G:; 10-13-94/1305 10-13-94/1530 G!-!P.C-: G:-!?.~I PARAMETER 45588-1 45588-2 Pentachlorophenol, ug/1 Phenanthrene, ug/1 Anthracene, ug/1 Carbazole, ug/1 Di-n-butylphthalate, ug/1 Fluoranthene, ug/1 Pyrene, ug/1 Butylbenzylphthalate, ug/1 3,3'-Dichlorobenzidine, ug/1 Benzo(a)anthracene, ug/1 Chrysene, ug/1 bis(2-Ethylhexyl)phthalate, ug/1 Di-n-octylphthalate, ug/1 Benzo(b)fluoranthene, ug/1 Benzo(k)fluoranthene, ug/1 Benzo(a)pyrene, ug/1 Indeno(l,2,3-cd)pyrene, ug/1 Dibenz(a,h)anthracene, ug/1 Benzo(g,h,i)perylene, ug/1 Sur:cogate-2FP Sur:cogate-PHL Surrogate-NEZ Surrogate -2FBP 25U lOU lOU lOU lOU lOU lOU 100 100 100 100 100 100 100 100 100 100 100 100 67 \' 79 \ 77 % 68 % 25U 100 100 lOU 100 lOU lCU lOU lOU lOU lOU lOU lOU lOU 100 lOU lOU lOU lOU 64 \ 73 \ 77 \ 68 % Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savanr.ah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Received: 1.; CC:' ~-= Mr. Leonard Moretz Geraghty & Miller, Inc., Envircr.rr.e:1tal Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Proj ec;;: NC02 02. 02 0/0xford/Channel Master /S,;G#G:~07 Sampled By: Cl~e~: REPO?-T OF RESULTS LOG NO SAMPLE DESCRIPTION , LIQUID S.::...'!?LES 45588·1 JFD·O!MW05·001 45588·2 JFD-O!MWlO·OOl PARAMETER 45588·2 Surrogate·TBP Surrogate·TPH Surrogate·l,2-DCB-d4 Surrogate-2-Chlorophenol-d4 Date Extracted Date Analyzed Methods: CLP 3/90 87 % 77 \- 54 \- 72 \- 10.17.94 10.20.94 Final Page Of Report DATE/ TIME SAMFL:::O 10·13-94/1305 10·13·94/2530 ----------------------- 45588-2 84 % 72 % 51 \- 70 % 10.11.s.; 10.20.H Laboratories In Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA 1'1u1<x:I N111111>e, J.) ( () / C '. () l L"' l',ojccl l.cx::ilio11 0/\ (.',,,,) 1 ,IJ C. LnL>oralory __ S(.~ ~-':"~ "' .. ' \_.-._ h. ___ -~-._ (l..J. Snmplcr(s)/1\llilinlion rn_ n __ -____ <i-,.,.,.__ ___ _ 6, w -Cr, .. .,,.... SI\MPLE IDENTITY . Code Dale/Time Sampled Lab ID • ll "" CHAIN-OF-CUSTODY RECORD I_ . o1 I -------I--I-----I-----I---------J----1----1----1---------1----•---I------ Sample Code: L = Liquid; S = Solid; I\ = /\ir Relinquished by: -~T.-_i>-1~_.!=~'.'.>•c.!· ,,~~------ Received by: Organizalion: _d::.eIA.1·.!:,J-y. j mi It rr:.,_.,;f (U., Organizalion: lolal No. of Elollles/ Conlainers Oale./..Q_f /3.1!5. '(Time __ ,/_7'---='""0,<._ __ Dale ' ·' Time Seal Intact? Yes No N/A llcli11quisl1ccJ 'f!.-r-o,.-/,. __ /);-rf .. 8'_]"_---01gn11izalion: ~----- Rcco,vccJ by: -<7---/->'-~ (} .. "1. §' .£ _ _ Organizalion: f l-Ff__ _______ _ Dalo _ / / . Timo_ _ _____ Seal lnlacl? Date_/vll_S'.'Lf~Time f:] 7 (es> No N/A Special lnslruclions/11crnaiks: -----------------------~------------------------_____ ,(J_C!i:~ '. 12,'-{ /,r. }\o(~:,,s 7,-~ "•"-er t-i:... Pt1L::; L. /1...:.1tl::....:_r-.o,:{.,CJ..t__,:-i.::___ __________ _ Delivery Method: ------D In Person - - __________ _________ _ _ (1 I 1).5'7/~f t,t 2.. _________ _ D(1 Common Carrier _l!!,) ~:t-•_ _________ □ Lab Courier D Other _______________ _ s,1.c;a·y 51'f'OfY - - - - - - - - - - - -......... Lai>rnalory 1'1sl< Orclr.r No./ 3-:, 13 Proi":I Nornlx,r j(/ ( V l D l, o lo I 'ruiccl l.ucalion . C)J: f'o,, l , ,v <.... I I I '· , L I .;1 ,rn:11uy . ,..r ... r'•·"' ,in•· \ / . •~: 1.5_ Seu nplcr(s)//\llilinlion Dale/Time SAMPLE IDENTITY Code Sampled Lab ID !, -.. 3 _3 _-,:,1 ,. I<-·z. _r_,1,. ,._ J l- Sample Code: L = Liquid; S = Solid; I\ = Air Relinquished by: .....I;J1.1~2-!..;_-,__L_ ____ _ Received by: 3 ·3 7.. I '<.. :2 -~- Organization: _&..r_,:i__sl>'ly Organizalion: CHAIN-OF-CUSTODY RECORD ol I I !{' . $; ~ . ---· 4- Tolal No. of Bolllcs/ Conlainers Dale I c.> 11 '!..J "i!J. Time, _ __,_J~q~vc....=cD __ _ Dale ' ' Time, ______ _ Seal lnlact? Yes No N/A Date_/_ __ ./.....,,.; Time___________ ,.§_tal lntacl? Dale LQ.i.l.'!LJ ,J. Time 9: ] 7, ~ No NIA Delivery Method: Cl 111 Person \,\J Common Carrier .l~~-.,) ___ 5>!. ________ _ :"ol1:Clf"Y 0 Lab Courier 0 Other ____________ _ fJ'fClfY Sn, • ..,, ... 91,\7&11 ------------------- I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: S4·45670A Received: 19 OCT 94 Project: NC0202.020/Oxford/C~annel Master/SDG#GMR09 Sampled By: Client LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SA.'!PLES 45670A·l JFD·CMMWl0-001 PARAMETER 45670A·l Hexavalent Chromium (7196) Hexavalent Chromium (7196), ug/1 Date Analyzed Hexavalent Chromium (Dissolved) (7196) Hexavalent Chromium (7196), ug/1 Date Analyzed <10 .10.19.94 <10 10.19.94 Page l DATE/ TIME SAMPLED SDG# 10-18-94/1210 GMR09 I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue •Savannah.GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Environrne~tal Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: 54·45670~ Received: 19 CCT s; Project: NC0202. 020/Oxford/Chan:,el Mas::er /SDGaG:-so; Sampled By: Clie~: REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SDIISOL!D 45670A·2 Detection Limits 45670A-3 Method Blank Result 45670A·4 · Lab Control Sample (LCS) Result 45670A-5 LCS Expected Value 45670A-6 LCS \ Recovery PARAMETER 45670A·2 Hexavalent Chromium (7196) Hexavalent Chromium (7196), ug/1 10 Date Analyzed Hexavalent Chromium (Dissolved) (7196) Hexavalent Chromium (7196), ug/1 10 Date Analyzed Methods: SW-846 45670A-3 <10 10.19.94 <10 10.19.94 45670A-4 205 10.19.94 205 10.19.94 45670A-5 200 200 Page 2 SDG~ G:~os G:-S09 G:-S0S GMR09 GMR09 4 5670A· 6 102 \- 102 % I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project ,-NC0202. 020/0xford/Channel Mascer/SCG#G:-!:.:, Sample1 By: C~ie~: REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, QC RE?ORT FOR SOLID/SEMISOLID LCS % Recovery Limits 45670A· 7 45670A·8 45670A·9 45670A· 10 45670A· ll Matrix Spike (JFD-CMMW21·001) (S445438) Result MS Duplicate (JFD-CMMW21·001) (S445438) Result MS (JFD-CMMW21-001) Expected Value MS (JFD-CMMW21-001) t Recove:y PARAMETER 45670A•7 Hexavalent Chromium (7196) Hexavalent Chromium 80-120 \ (7196), ug/1 Date Analyzed Hexavalent Chromium (Dissolved) ( 7196) Hexavalent Chromium (7196) 80-120 t Methods: SW-846 45670A·8 176 10.06.94 45670A·9 176 10.06.94 G::-!:.C; G~-s.c= G:-SG: G:Q.G; G::-!:.0; 45670A-10 45670A-l: 200 I SL SAVANNAH LABORATORIES I & ENVIRONMENTAL SERVICES, INC. I I I I I I I I I I I I I I I I I 5102 LaRodle Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 M:. Leonard Moretz Geraghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: S4-45670A Received: 19 OC7 s~ Project: -NC0202.020/Oxfo=d/Channel ~_aster/SDG~G:-!?.09 Sampled By: Clie~t REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISO~ID 45670A-12 MSD (JFD-Cl-!MW21-001) \ Recovery 45670A-13 MS\ Recovery Limit 45670A-l4 MS\ RPO (Limit) G~OS G:-!?.OS G:~os PARAMETER 45670A-12 45670A-13 45670A-!4 Hexavalent Chromium (7196) Hexavalent Chromium (7196) 83 \ 85·115 \ 0(<20) \ Hexavalent Chromium (Dissolved) (7196) Hexavalent Chromium (7196) Methods: SW-846 Final Page Of Report Laboratories in Savannah. GA • Tallahassee, FL • Tampa. FL • Deerfield Beach. FL • Mobile. AL • New Orleans. LA - l.ai>rnalu1y ld1 01drn Nu../.L7.3.'3 CHAIN-OF-CUSTODY RECORD l'a[/O _____ _l ____ ol _ ··--/ .... l'mjccl N11111llcr A<" D ·z.._,._'"> 1.. O~~-o ··--__ 1'1ojecl 1.ocalion __ ___() )\ GJ.c.J, . ;.)_ ~-: __ . --·-· .. Sampler(s)/Nlilialion ..::r, t-;::, -· I&-• .~,\ ~;._(J,IJ ,._ (<i,. .... ~ \ Dale/Time SI\MPLE IDENTllY Code Sampled IO I Ji--1~ ,-z.,,, Lab ID '\ I I I l l \ I ./ , ..... 1-----1---1---+---t---f---t---l----l----l----l----l-~ ~1.........- ~ -----1--1----1---1~ -----.,............. TOfAL 1----'.7""1]1~--l----1----ll----l---t---l----1----1----1---+---l----l-----l ~ ~ Sample Code: L = Liquid: S = Solid; A = Air Relinquished by: -c• ,..__ 'I:,~.,"- Received by: Organization: Organization: nclinquishcd ~t--r: =,---{ _ Organization: . Received by: -0'-f.YJ. L_q_,-,._ ' L ~_b..J_Q Organization: ---5'J E5. Total No. of Bollles/ Containers Dale IQ I t f; 15 ~ _ Time,_....:....I _,_7_,,,r_,c1.:._ __ Dale I I Time Dale_/ /.. ... Time ____________ _ . Date...1'2.LJ'f..LJ.':{Time 9'~ f., __ _ Seal Intact? Yes No N/A Seal I nlaci? @ No N/A Special lnslruclions/Rcmarks: -------------------------::--·-------_,vo t< • Z,'{l,c hei.J,-> -{-,-,,..,_c .Cor c,..-"', f-oC.::;. L,.,, ~~"r,._·.,_,,,(.."'-------------- D;-ive_ry_M;;-hod-~---□-ln_P_e_r_so-n---~-C-o_m_m_o_n,_C_a_r,-ie_r _ _fl )--:~-¥-~----_-·_· •_·•· -... ---·---□~~-£~?ur:-'-~~t, ~h: . --. ·-· ~~en - - - - - ----· - - - - - - -·--···•• I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S4·45588A Received: 14 OCT 94 Mr. Leonard Moretz Geraghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project: NC0202.020/0x!ord/Channel Master/SDG#GMR08 Sampled By.: Client LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID S"''!PLES 45588A·l JFD·CMMW05-001 45588A-2 JFD·CMMW05R-001 45588A·3 JFD·CMMW99E-002 45588A·4 JFD·CMMW99F-002 PARAMETER Volatiles by GC/MS (CLP-3/90) Chloromethane, ug/1 Bromomethane, ug/1 Vinyl Chloride, ug/1 Chloroethane, ug/1 Methylene Chloride (Dichloromethane), ug/1 Acetone, ug/1 Carbon Disulfide, ug/1 1,1-Dichloroethene, ug/1 1,1-Dichloroethane, ug/1 Cis/Trans-1,2-Dichloroethene, ugJl Chloroform, ug/1 1,2-Dichloroethane, ug/1 2-Butanone (MEK), ug/1 1,1,1-Trichloroethane, ug/1 Carbon Tetrachloride, ug/1 Bromodichloromethane, ug/1 1,2-Dichloropropane, ug/1 cis-1,3-Dichloropropene, ug/1 Trichloroethene, ug/1 Dibromochloromethane, ug/1 45588A·l 100 lOU 7J lOU 34 100 lOU 29 lOU 760E 2J lOU lOU 6J SJ lOU 100 lOU 9600E lOU 45588A-2 10000 10000 10000 10000 10000 10000 10000 10000 10000 670J 1000 1000 1000 1000 1000 1000 1000 1000 36000E 10000 DATE/ TIME SAMPLED 10-13-94/1305 10-13-94/1305 10-13-94/1500 10-13-94/1305 45588A-3 lOU lOU lOU 100 SBJ lOU 100 100 100 100 100 100 lOU 100 100 100 100 100 230E 100 Pagel SDG# GMROS GMR06 GMROB GMROS 45588A-4 100 100 100 lOU SBJ 100 lOU lOU 100 100 lOU lOU lOU lOU lOU lOU lOU lOU lJ 100 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I -• I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG ~O: S4-45588A Recei-,ed: 14 OCT 94 Mr. Leonard Moretz Geraghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project: NC0202.020/0xford/Channel Mas:er/SDG~=oa Sarnp!ed By: Client LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SA.'IPLES 45588A-l JFD-CMMW05-001 45588A-2 JFD-CMMW05R-001 45588A-3 JFD-CMMW99E-002 45588A-4 JFD-CMMW99F-002 PARAMETER 1,1,2-Trichloroethane, ug/1 Benzene, ug/1 trans-1,3-Dichloropropene, ug/1 Bromoform, ug/1 4-Methyl-2-pentanone (MIBK), ug/1 2-Hexanone, ug/1 Tetrachloroethene, ug/1 l,l,2,2-Tetrachloroethane, ug/1 Toluene, ug/1 Chlorobenzene, ug/1 Ethylbenzene, ug/1 Styrene, ug/1 Xylenes, ug/1 Surrogate Toluene-dB Surrogate-· 4-Bromofluorobenzene Surrogate -l,2-Dichloroethane-d4 Date Analyzed 45588A-l ---------- 100 lJ lOU lOU lOU 4J 5200E 100 7J lOU lOU lOU 100 107 \- 99 \- 103 \- 10.17.94 45588A-2 ---------- lOOOU lOOOU lOOOU lOOOU lOOOU 10000 6500 lOOOU lOOOU lOOOU lOOOU lOOOU lOOOU 107 \- 102 \- 100 % 10.20.94 DATE/ TIME SAM? :.ED 10-13-94/1305 10-13-94/1305 10-13-94/1500 10-13 -94 /13 05 45588A-3 Page 2 SDG~ G..'8.08 GMR08 GMROS GMR08 45588A-4 -------------------- 100 100 100 100 100 lOU 100 100 lCO 100 100 100 70 100 100 100 12 2J 100 lOU 100 lOU 100 lOU 100 lOU 105 % 103 \- 102 % 107 % 101 % 103 \- 10.20.;.; 10.20.94 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue •Savannah.GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Envi~cnmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: S4-4o388~ Received: 14 CCT 94 Project: NC0202.020/0xford/Channel Master/SDG#=.os Sampled By: Ccie~t LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQU:D S,'..'IPLES 45588A·l JFD-01MW05·001 45588A-2 JFD-01MW05R-001 45588A-3 JFD-01MW99E-002 45588A-4 JFD-01MW99F-002 ------------------------------------------------------------- PARAMETER TAL Metals (CLP-3/90) Aluminum (CLP 3/90), ug/1 Antimony (CLP 3/90), ug/1 Barium (CLP 3/90), ug/1 Beryllium (CLP 3/90), ug/1 Cadmium (CLP 3/90), ug/1 Calcium (CLP 3/90), ug/1 Chromium (CLP 3/90), ug/1 Cobalt (CLP 3/90), ug/1 Copper (CLP 3/90), ug/1 Iron (CLP 3/90), ug/1 Magnesium (CLP 3/90), ug/1 Manganese (CLP 3/90), ug/1 Nickel (CLP 3/90), ug/1 Potassium (CLP 3/90), ug/1 Silver (CLP 3/90), ug/1 Sodium (CLP 3/90), ug/1 Vanadium (CLP 3/90), ug/1 Zinc (CLP 3/90), ug/1 Interference Check Sample Dilution Check Sample Date Analyzed ---------- 45588A-l 57.0BN* 8 .9U 53.0B 0 .14U 2.60 13000 3.30 l.6U 3.lB l30N* 6930 49.6 3.9B 895B 2.30 22300 5.5B 5.3B PASSED PASSED 10.26.94 ---------- .45588A·2 50.4BN* 8.9U 52.lB 0 .19B 2.60 12800 3 .30 1.9B 2.80 125N* 6820 47.1 3.6B 868B 2.5B 21900 7.9B 12.9B PASSED PASSED 10.26.94 ---------- DATE/ TIME SA.'IPLED 10-13-94/1305 10-13-94/1305 10-13-94/1500 10-13-94/1305 45588A·3 15.SUN* 8.90 11.0B 0 .140 2.60 24200 3.30 1. 60 2.80 19.6BN* 7530 0.940 2. 30 2150B 2.30 12400 2 .40 20.8 PASSED PASSED Page 3 =oa =.oa =.oa =oa 45588A·4 17. 63N* E.SU 1:.03 0.l4iJ 2. 60 2~500 3 .30 l. 60 2.SU 11.S3N• ":730 0.5·lU ~.30 22503 2. 3U 1~700 2.4U 34.0 p;..ssED PASS'.::!) 10.26.94 10.2:.s; -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Geraghty & Miller, Inc., Enviror-=:ental Se=-vices 2840 Plaza Place, Suite 350 Raleigh, NC 27612 LOG NO: S4·4:588A Received: 14 CCT 94 Projec~: NC0202.020/0xford/Channel Master/SDG~=os Sampled By: Client REPORT OF RESULTS LOG NO SAMPLE DESCRIPTION, LIQU!D SA.'!PLES 45588A·l JFD·CMMW05·00l 4558BA·2 JFD·CMMW05R-00l 45588A·3 JFD·CMMW99E·002 45588A·4 JFD·CMMW99F·002 PARAMETER Arsenic (CLP 3/90) Arsenic (CLP 3/90), ug/1 \-R Post Digestion Spike Date Analyzed Lead (CLP 3/90) Lead (CLP 3/90), ug/1 \-R Post Digestion Spike Date Analyzed Selenium (CLP 3/90) Selenium (CLP 3/90), ug/1 \-R Post Digestion Spike Date Analyzed Thallium (CLP 3/90) Thallium (CLP 3/90), ug/1 \-R Post Digestion Spike Date Analyzed Mercury (CLP 3/90) Mercury (CLP 3/90), ug/1 Date Analyzed Cyanide (CLP 3/90) Cyanide (CLP 3/90), ug/1 Date Analyzed ---------- 45588A·l 1.40 100 \- 10.19.94 0 .910 98 \- 10.19.94 13. 20WN 83 \- 10.20.94 1.30 96 \- 10.19.94 0.040 10.20.94 lOU 10.21.54 ---------- 45588A·2 1.40 101 \- 10.19.94 0 .910 97 \- 10.19.94 l3.2UWN 72 \- 10.20.94 1.30 99 \- 10.19.94 0.04U 10.20.94 100 10.21.94 ---------- Page 4 DATE/ TIME SAMPLED 10-13-94/1305 10·13-94/1305 10-13-94/1500 10-13-94/1305 =as 0!?.08 0!?.08 =os 45588A·3 45588A-4 1.40 1.40 115 \-10" \- 10.19.94 10.19.94 0 .910 0.910 100 \-56 \- 10.19.94 10.lS.9-! 2.6UWN 13. 2c;-.~ 45 \-73 \- 10.19.94 10.20.S-I l.3U l.3U 96 \-100 \- 10.19.94 10.lS .S-1 0.04U 0.040 10.20.94 10.20.9-1 lOU 100 10.21.94 10.21.54 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Recei·,e:i: 14 CCT 94 Mr. Leonard Moretz Geraghty & Miller, Inc., Enviror.mental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project: NC0202.020/0xford/Cha.-mel Master/SDG~=.oa -Sampled By: Client LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SA.'!PLES 45588A-5 JFD-CMMW99T-Oll 45588A-7 JFD-CMMWl0-001 DATE SAM?Ll:D 10-13-94 10-13-94 Page 5 =.oa =.oa PARAMETER 45588A-5 45588A-7 Volatiles by GC/MS (CLP-3/90) Chloromethane, ug/1 Bromomethane, ug/1 Vinyl Chloride, ug/1 Chloroethane, ug/1 Methylene Chloride (Dichloromethane), ug/1 Acetone, ug/1 Carbon Disulfide, ug/1 1,1-Dichloroethene, ug/1 1,1-Dichloroethane, ug/1 Cis/Trans-1,2-Dichloroethene, ug/1 Chloroform, ug/1 1,2-Dichloroethane, ug/1 2-Butanone (MEK), ug/1 1,1,1-Trichloroethane, ug/1 Carbon Tetrachloride, ug/1 Bromodichloromethane, ug/1 1,2-Dichloropropane, ug/1 cis-1,3-Dichloropropene, ug/1 Trichloroethene, ug/1 Dibromochloromethane, ug/1 1,1,2-Trichloroethane, ug/1 Benzene, ug/1 100 100 100 100 4BJ 100 100 100 100 100 100 100 100 100 lOU 100 100 100 100 100 100 100 ---------- 1000 1000 1000 1000 2203 1000 1000 120 1000 610 SJ 1000 1000 30J 25J 1000 1000 1000 76000~ 1000 1000 1000 -------------------- Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7858 • Fax (912) 352-0165- LOG NO: S4-45588A Received: 14 CCT 94 Mr. Leonard Moretz Geraghty & Mille:-, Inc., En-✓iror..mental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Project: NC0202.020/0xford/Channel Master/SDG;=.oa Sampled By: Client LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID S;.MPLES 45588A-5 JFD-CMMW99T-Oll 45588A-7 JFD-CMMWl0-001 DATE SAMPLED 10-13-94 10-13-94 PARAMETER 45588A-5 45588A-7 trans-1,3-Dichloropropene, ug/1 Bromoform, ug/1 4-Methyl-2-pentanone (MIBK), ug/1 2-Hexanone, ug/1 · Tetrachloroethene, ug/1 1,1,2,2-Tetrachloroethane, ug/1 Toluene, ug/1 Chlorobenzene, ug/1 · Ethylbenzene, ug/1 Styrene, ug/1 Xylenes, ug/1 Surrogate Toluene-dB Surrogate -4-Bromofluorobenzene Surrogate -l,2-Dichloroethane-d4 Date Analyzed 100 100 100 100 100 100 lJ 100 100 100 100 104 \- 104 \- 106 % 10.20.94 1000 1000 1000 lOOU 6000E 1000 lSJ lOOU 1000 1000 lOOU 103 \- 9 9 \- 105 \- 10.20.94 Page 6 SDG; Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL• Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354-7858 • Fax (912) 352-0165 LOG NO: S4-4SS88A Received: 14 CCT 94 Mr. Leonard Moretz Geraghty & Miller, Inc., Enviror.-ental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Projec~: NC0202.020/0xford/Channel Master/SDG~=os Sampled By: Client LOG NO REPOR"!" OF RESULTS SAMPLE DESCRIPTION, LIQUID SA.'!PLES 45588A-8 JFD-CMMWOS-001 (DL) 45588A-9 JFD-CMMWOSR-001 (DL) 45588A-10 JFD-CMMW99E-002 (DL) 45588A-ll JFD-CMMWl0-001 (DL) PARAMETER Volatiles by GC/MS (CLP-3/90) Chloromethane, ug/1 Bromomethane, ug/1 Vinyl Chloride, ug/1 Chloroethane, ug/1 Methylene Chloride (Dichloromethane), Acetone, ug/1 Carbon Disulfide, ug/1 l,l-Dichloroethene, ug/1 l,l-Dichloroethane, ug/1 Cis/Trans-1,2-Dichloroethene, ug/1 Chloroform, ug/1 l,2-Dichloroethane, ug/1 2-Butanone (MEK), ug/1 l,l,l-Trichloroethane, ug/1 Carbon Tetrachloride, ug/1 Bromodichloromethane, ug/1 l,2-Dichloropropane, ug/1 cis-1,3-Dichloropropene, ug/1 Trichloroethene, ug/1 Dibromochloromethane, ug/1 45588A-8 sooou 50000 50000 50000 ug/1 1600BDJ 50000 50000 50000 50000 710DJ 50000 50000 sooou sooou sooou 50000 50000 50000 35000D 50000 DATE SA.'!PLED 10-13-94 10-13-94 10-13-94 10-13-94 Page 7 =as G:-!P.08 =-OB =oa 45588A-9 45588A-10 45588A-ll 20000 20000 20000 20000 710BDJ 20000 20000 2000U 20000 690DJ 20000 20000 20000 20000 20000 20000 2000U 20000 34000D 20000 sou 100000 500 100000 500 100000 sou 100000 lBBDJ 4900BDJ 500 100000 500 100000 500 100000 500 100000 500 100000 500 100000 500 100000 500 lOOOOU 500 lOOOOU 500 100000 500 100000 500 100000 500 100000 250D 150000D sou 100000 Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA I I I I I I I I I I I I I I I I I I I SL SAVANNAH LABORATORIES & ENVIRONMENTAL SERVICES, INC. 5102 LaRoche Avenue •Savannah.GA 31404 • (912) 354-7858 • Fax (912) 352-0165 Mr. Leonard Moretz Ge~aghty & Miller, Inc., Environmental Services 2840 Plaza Place, Suite 350 Raleigh, NC 27612 Recei·;ed: 14 CCT 9-i Project: NC0202.020/0xford/Channel Mas~er/SDG=2<S.08 Sampled By: Clten~ LOG NO REPORT OF RESULTS SAMPLE DESCRIPTION, LIQUID SAMPLES 45588A-8 JFD-CMMWOS-001 (DL) 45588A-9 JFD-CMMWOSR-001 (DL) 45588A-l0 JFD-CMMW99E-002 (DL) 45588A-ll JFD-CMMWl0-001 (DL) PARAMETER l,1,2-Trichloroethane, ug/1 Benzene, ug/1 trans-l,3-Dichloropropene, ug/1 Bromoform, ug/1 4-Methyl-2-pentanone (MIBK), ug/1 2-Hexanone, ug/1 Tetrachloroethene, ug/1 l,l,2,2-Tetrachloroethane, ug/1 Toluene, ug/1 Chlorobenzene, ug/1 Ethylbenzene, ug/1 Styrene, ug/1 Xylenes, ug/1 Surrogate Toluene-dB Surrogate - 4 .-Bromofl uorobenzene Surrogate -l,2-Dichloroethane-d4 Date Analyzed Methods: CLP 3/90 45588A-8 ---------- 50000 50000 50000 50000 sooou 50000 6500D sooou 50000 50000 50000 50000 50000 104 % 103 t 109 t 10.20.94 455BBA-9 ---------- 20000 20000 20000 20000 20000 20000 6100D 20000 20000 20000 20000 20000 20000 105 t 103 t 107 t 10.20.94 Final Page Of Report DATE SA.'!?i.c:;:D 10-13-94 10-13-94 10-13-94 10-13-94 45588A-10 Paqe 8 8-!?.08 81:;.08 8-!?.0S 0!?.08 45588A-ll -------------------- 500 100000 500 100000 500 100000 500 100000 sou 100000 500 100000 75D 5300DJ sou 100000 14DJ 100000 sou 100000 sou 100000 500 100000 500 100000 105 \ 1~3 t 102 t 10, \ 107 t 106 \ 10.20.5~ 10.20.H Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA CHAIN-OF-CUSTODY RECORD l'nuo. ___ / ___ 01_/_ __ 1',uj,x;I Nu,nlior .Al CD 1 D ·l.. ___ o "Lo ______ _ I '1uj,x;I Lot:;ilio11 _ C)J:_to•_• l __ 1 _ ,\./_(__ _____________ _ l,JI.Jor alory 2-.>' '"'-~-u.::.J..L;..J:..:::.l.!.s __ s,1111plC1 (s)//\llili~lio11 __ _1__>1 · <-?_ __ :.-.. (, __ ,-"" ·-- ~ ~ vJ -r;..,.,." Dalell"imc SIIMPLE IDENTITY Code Sampled Lab ID ' /II-'•• I >-"1'1 3 !, 3 _3 I I/,:,;, -(ih~'"..,//C•-v1.•i L I "3 ·3 7- '-::.!, ?2 --2 ----------1---1-----1---- Sample Code: L = Liquid; S = Solid; A = Air Relinquished by: ....:T--,..O.L..J"2~.,~--~~~------ Reccived by: Organization: Organization: 1 l ~ ~ ----- --t-, - Tolal No. ol Bollles/ Conlainers &en. s.b1.y -t ,n i JJ t CJ :TA£., Dal<a I,, I I '],__J 'i'~_ Time, _ __,J'-q'-'p::..::D __ _ Dale 1 ' Time lOTAL (I"~) r-: ,") (· ) (~) (31 ~(-1:1-- r"" [.·> - Seal Intact? Yes No NIA ~I Intact? __ ~No NIA Sr,ecial l11structions/Rcmarkl(: .V.e{..!:..:_/l_~,.,_:f£..1' -h~ 7,.,,.,1<-1 1 "C "'' ~ ._ , ~Ck V<'~-r lf-·t·,.,__ L "·"'I'"'"!-' ---------L~ 0 +~ : ·7.. 'i J,('-/141) di" 5 ii n--<.. -f!,, r Cc t-1-, (JP C. :: L' /11 c•rrt-r: .. ________________ (:} I 'J) .. 5.3·, -/ t~ 'L --------------------------□ In Person ~ Common Carrier ...E!:JL..._1.~'-'----- 1 s,,:c,n 0 Lau Courier 0 Other _____ _ ~.l'(CJl'Y Delivery Melhod: - - - --------- - - - - - - - CHAIN-OF-CUSTODY RECORD l1:1qo I ____ of __ I _____ _ l',ojL'Cl Nu1111)e1 ))_(_'?.. ?9._·~.: .. 9. .. ?: .. ~~~------·-1 ---------------------------------------------. ------------------, /----,---,-S/\Ml'Ll: UOIILl_~/_CONIAlf~L:II IJESClllf'IION ------,-----JI I'1ojL'<:I Localirn I __ Qi\ __ (.'_,,.!_,)_ I -}./ __ <; _____ ------ L1lJoral01y SQ. vrA r, r\~--1:::,,__~. b :5 __ S;1111ple1{e:)/Alfili:ilio11 ____ rn-n _-G-,-,., ____ _ 6-l vJ -t,-1-.-►, .v _,._ .,V ,'1 r/ .ii :;'J I~ I" -V I { u' / " ,x· ,.il ,r " , V 11: ( 11 \v ~ .;. l :::.o :r q;: /.. t ;; ~ IJnlc/Timo ii' 0 o ' q, v {) / / 0 Q \., SIIMPLE IDENTITY Code Sampled Lab ID j y ty /;",o /-.. ~ 1,-,°' V , '' \ 1 i TOTAL Sample Code: L -Liquid; S -Solid; A = Air Tolal No_ of Bollles/ Conlainers Relinquished t,y: __-:r.,_,·I!'--=-__,;::,=., ,_,_ll_,__a,,______ Organization: tFete..1My. i {t1,0/« ,__;:f (U.< Dale_/.JLLf .3_/.!1-'(f ime,_~l_7~0~o~-- Received by: Organization: Date I I Time, ______ _ Seal Intact? Yes No NIA Rclinq_ uishecJ ~,7-~-/'J.-rru Organization: c 1 ,, Received by: -<7-t.liJ.&--q ':L'i'CT <!... Organization: ----L.Jc.~f::=-----L~------- Dato _ ..J __ /_Timo Dale /b/.L'f.il~Time -r.-17 Seal Intact? Ves> No N/A Special Instructions/Remarks: di. of-<... : 2 'f 1-r. b, o{): ,,._~1_,ZCj__t'-"~'=--'"CL<"--'---L='-r _+-_(.. ___ __,p---'t:7'--L--_-....,.L':'-'-. (t!.c::.P..:./'-(_,---""-f....::-i.:::...._ _________ _ ------0J!i2flL~,._/?=l'-~-~------ Delivery Method: - - - D In Person - - \)a Common Carrier µ) -f ~ • Sl'(C,,-Y -------D Lab Courier - - D Other ------c==:----Sl'(ClfY - - -